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3412_Forsyth_OldSalisburyRoad_CDLF_May2020GW_FID1416615_20200622
r1 [:]PaperReport ❑Electronic Data Email CD (data loaded: Yes / No Doc/Event #: 1-tENR USE ONLY: NC DENR Environmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. Solid Waste Monitoring Data Submittal Information Name of entity submitting data (laboratory, consultant, facility owner): HDR Engineering, Inc. of the Carolinas Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Eric A. E-mail: eric.wright@hdrinc.com Facility name: Facility Address: [Old Salisbury Road landfill 3336 Old Salisbury Road Winston-Salem, NC 27127 Phone: 704-338-6719 NC Landfill Rule: Actual sampling dates (e.g., Facility Permit # (.0500 or .1600) October 20-24, 2006) 34-12 .0500 May 5-8, 2020 Environmental Status: (Check all that apply) ❑ Initial/Background Monitoring �X Detection Monitoring Lhl Assessment Monitoring Corrective Action of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells X❑ Groundwater monitoring data from private water supply wells Leachate monitoring data ❑ Surface water monitoring data Methane gas monitoring data Corrective action data (specify) Other(specify) Notification attached? No. No groundwater or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or INC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. ❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Certification To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Eric A. Wright Project Engineer 704-338-6719 Facility Representative Name (Print) Title (Area Code) Telephone Number Digitally signed by Eric Wright am wo020 Af !al `.% Date: 2020.06,22 13:47:17-04'00' \A RR SEAL 019027 6/22/2020 �• '•.. ... rf/I '' fA NtQ,,,r Signature Date 440 South Church Street Suite 1000 Charlotte NC 28202 Facility Representative Address F-0116 NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 This page intentionally left blank. FYZ k A. . .1 Winston-Salem/ Forsyth County 1 liieliofiac HDR Project No. 10125427 Assessment Monitoring Report Groundwater and Surface Water Sampling Event — May 2020 Old Salisbury Road Landfill NCDEQ Permit NO. 34-12 Forsyth County, North Carolina June 2020 IIIfill,�` t ,IS,tiQ�N k.�,��G � •. Q r • SEAL ' r 019027 This page intentionally left blank. Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Contents Contents 1 General..................................................................................................................................3 1.1 Facility Background........................................................................................................3 1.2 Regulatory Authority.......................................................................................................3 1.3 Assessment Monitoring..................................................................................................3 1.4 Geologic Characteristics.................................................................................................5 1.4.1 Regional Geologic and Hydrogeologic Setting........................................................5 1.4.2 Site Specific Topography and Drainage..................................................................5 1.4.3 Site Specific Hydrogeology.....................................................................................5 2 Monitoring Network................................................................................................................6 3 Data Collection......................................................................................................................8 3.1 Water Level Measurements............................................................................................8 3.2 Groundwater Flow..........................................................................................................9 3.3 Sample Collection and Analysis.....................................................................................9 4 Analytical Results................................................................................................................11 4.1 Groundwater.................................................................................................................11 4.2 Surface Water...............................................................................................................12 4.3 Assessment Monitoring................................................................................................12 4.4 Landfill Gas...................................................................................................................12 5 Summary.............................................................................................................................13 6 Recommendations...............................................................................................................13 Tables Table 1 Existing groundwater monitoring well details...................................................................6 Table 2 Sampling parameters and schedule................................................................................7 Table 3 Groundwater elevations...................................................................................................8 Table 4 Interwell flow velocities....................................................................................................9 Table5 Lab detections................................................................................................................10 Table6 Gas readings..................................................................................................................12 Figures Figure 1 Groundwater contours and sample locations.................................................................4 Figure 2 Historical groundwater elevations...................................................................................8 Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Contents Figure 3 MW-2R groundwater detections...................................................................................11 Appendices Appendix A — Summary of Monitoring Results Appendix B — Laboratory Reports Appendix C — Field Data Appendix D — Electronic Files Acronyms 2B 15A NCAC Subchapter 02B — Surface Water and Wetlands Standards 2L 15A NCAC Subchapter 02L — Groundwater Classification and Standards fag/L micrograms per liter EPA United States Environmental Protection Agency FID File Identification MCL Maximum contaminant level MDL method detection limit NCDEQ North Carolina Department of Environmental Quality' ND not detected in sample NE standard not established NS not sampled NTU Nephelometric turbidity units PCB polychlorinated biphenyl PCE tetrachloroethene PRL practical reporting limit PVC polyvinyl chloride SVOC semi -volatile organic compound VOC volatile organic compound USGS U.S. Geological Survey Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� General 1 General HDR Engineering, Inc. of the Carolinas (HDR), on behalf of Winston-Salem/Forsyth County Utilities (the City), is submitting this assessment monitoring report for the Old Salisbury Road C&D Landfill (OSR) located in Forsyth County, North Carolina. 1.1 Facility Background OSR covers approximately 56 acres within a 140-acre tract north of Friedberg Church Road and west of Old Salisbury Road in Forsyth County, North Carolina. The Forsyth/Davidson County line borders the site to the south (Figure 1). The facility was issued a permit to operate on July 3, 1996 and opened in August of the same year. 1.2 Regulatory Authority OSR is currently operating under North Carolina Department of Environmental Quality (NCDEQ) facility permit number 34-12, dated February 28, 2020 (FID 1389508). Groundwater monitoring and reporting requirements are outlined in items 14 to 21 of the permit. North Carolina Solid Waste Management (SWM) Rules 15A NCAC 13B .0544(b) and .0544(c) define the requirements applicable to groundwater and surface water monitoring plans for OSR, respectively. The groundwater monitoring plan (FID 1388728) dated January 2020, was approved by NCDEQ on February 28, 2020. 1.3 Assessment Monitoring OSR is in assessment monitoring due to exceedances of groundwater quality standards, as specified in 15 NCAC 02L .0202 (2L Standards), for benzene and tetrachloroethene (PCE) detected in well MW-2R in 2011. On December 9, 2011, an assessment monitoring plan for MW-2R was submitted in accordance with 15A NCAC 13B. The assessment monitoring plan can be summarized as: • Groundwater monitoring wells MW-1 R, MW-2R, MW-4R and MW-15 will be sampled semi-annually for Appendix I and the previously detected Appendix II constituents; • All fourteen groundwater monitoring wells (including MW-1 R, MW-2R, MW-4R and MW- 15) will be sampled during every other fall event (odd years) for the entire Appendix II constituent list. • Additional Appendix II constituents detected during these events will be added to the sampling program for subsequent semi-annual events. LEGEND EXISTING CONTOURS — PROPERTY BOUNDARY PERMIT/PHASE BOUNDARY — — 735 — — GROUNDWATER CONTOURS SURVEY BOUNDARY EXISTING ABANDONED 'FE�h CountMONITORING County WELLS (MW d[ OW)n METHANE PROBES (MM) 1� T SW-1 SURFACE WATER Location Mop No mao APPROXIMATE GROUNDWATER FLOW — — NOTES �MM-9 1. THE SITE TOPOGRAPHIC INFORMATION PROVIDED BY CARTOGRAPHIC AERIAL MAPPING INC. FOR \f W-10 MW-10j,p � MM-10 2019. SURVEYING COMPANY DATED JAN. 5 2019. ® SW-2 2. PROPERTY BOUNDARY TAKEN FROM DATA �; SUPPLIED BY BRADY SURVEYING, INC. DATED SURVEY BOUNDARY oso MARCH 14, 1994. 733.78 >� 00 L) 3. GROUNDWATER ELEVATIONS ARE IN MEAN SEA MW-14 LEVEL, MEASURED ON MAY 4, 2020 (SHOWN II NEXT TO WELL LABEL). 740.00 MW-9 I1 \ 72922 4. MW-15 IS NOT USED TO DEVELOP THE ^�0 1 _ >� MW-11 GROUNDWATER SURFACE SHOWN DUE TO IT BEING INSTALLED IN BEDROCK. > a° 790 — r\ >RS\ \ ono �MIM-11 MM- ® 753.13 1 _ \ \ �\ \\\\\ I SCALE IN FEET MW-6 770 I'llr'll \ \ —780— — i1 >So \ 734.52 200 100 0 200 400 / S790 oo ° \ \ MW-12 1 "=400' 810 830 LANDFILL PERMIT BOUNDARY 830 1 V — 760V \ \ I : MM-12 a 00 \ MM \ {�} 743.36 I PROPERTY LINE ,? �� \ R 11765 \ \ \ MW-13 / n� ,moo \\\\�\ / \ � 763.59 / ,'ISO/ \ \� -4 MW-3R _ �7g0 765.04 61W�6R 80\0MW-15 SW-1 MM-6 °o _ / �o MML1 I ®� W �775 ,MW M778.53 1W-2RB �Oo 771.15 S 110 MW-7 — 800 810 —765- 8220 \ 830 I i 830 790 Ao I 'moo 810800 I \1vIM— so � �� ea Y'C 800 763.11 \j� g3o MW-4R \ \ 830\ {� 803.60 19 ��g \ \ MW-1R \ soo \ MM-21)� MM-4S� MM-4D MM-3 775.06 -MW-SR — — PROJECTTITLE OLD SALISBURY ROAD C & D LANDFILL SHEET TITLE GROUNDWATER CONTOURS AND SAMPLE LOCATIONS PROJECT NUMBER 10125427 PROJECT MANAGER M. PLUMMER, P.E. DATE MAY 2020 REFERENCE SHEET LAYOUT 2 REFERENCE DOCUMENT OOD-03 EXHIBIT NUMBER FIGURE 1 Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� General 1.4 Geologic Characteristics This section paraphrases the descriptions in the original July 2003 Ground Water Monitoring Plan and the 2003 Design Hydrogeologic Investigation Report. 1.4.1 Regional Geologic and Hydrogeologic Setting Per the 1985 Geologic Map of North Carolina, OSR is located in the Charlotte Belt of the Piedmont Physiographic Province. This province is characterized by metamorphic and igneous plutonic rocks, which have been extensively weathered and eroded, forming an undulating topography. Subsurface conditions generally consist of topsoil underlain by residual soils, saprolite, partially weathered rock (PWR), and bedrock. There is generally a gradual transition between material types with varying thickness. Bedrock in the Charlotte Belt is characterized by numerous plutons with granitic to gabbroic composition that have intruded gneiss, schist, metavolcanic rocks, and metamorphosed mafic complexes (basalt, gabbro, and ultramafic rocks). Typically, bedrock is overlain by PWR and highly weathered bedrock (saprolite). Saprolite retains some of the original (relict) structural features of the parent rock and varies in thickness from a few feet to over 100 feet. The near surface residual soils are formed by physical and chemical weathering of the saprolite and usually do not retain the relict structural features. Groundwater is present within fractures and joints in the bedrock and within the pore spaces of the overlying-saprolite and residual soils. Groundwater is primarily recharged by precipitation and commonly located within the saprolite layer. Groundwater moves laterally toward streams and surface water bodies and generally follows the surface topography. 1.4.2 Site Specific Topography and Drainage Surface drainage at OSR is primarily controlled by a north -northwestern trending ridge within the property. This ridge directs the majority of surface runoff north to South Fork Muddy Creek; however, smaller components of runoff are directed to the northeast, west, and southwest into tributaries of South Fork Muddy Creek. A small area on the southeast portion of the site drains south into Miller Creek. Both the South Fork Muddy Creek and Miller Creek flow west where they converge with Muddy Creek and eventually discharge to the Yadkin River. 1.4.3 Site Specific Hydrogeology As documented in the Design Hydrogeological Investigation Report submitted by HDR on December 2, 2003, the uppermost aquifer underlying the facility is comprised of three stratigraphic units. The downward progression of the three units is saprolite transitioning into PWR, then bedrock. Groundwater flows through pore spaces within the saprolite and PWR, while groundwater flow through the bedrock is primarily through fractures. OSR was constructed within the unconsolidated micaceous silty sands and sandy silts produced by the in -situ weathering of the granodioritic parent rock. There is no evidence of discrete flow patterns resulting from relict quartz veins, dikes, healed fractures, or strong preferential Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Monitoring Network alignment of minerals (i.e., foliation). In general, groundwater flows from areas of higher elevation to areas of lower elevation and generally mimics surface topography. 2 Monitoring Network The monitoring network consists of 14 groundwater wells and 4 surface water sampling locations. Sampling of monitoring wells and surface water locations is conducted on a semi- annual basis, as summarized in Table 1. Groundwater monitoring well MW-1 R is located hydraulically upgradient of the landfill and is considered as the background well for the site. Upstream surface water (SW-1) and downstream surface water (SW-2) samples are obtained from the adjacent stream to the east. Two surface water samples (SW-3 and SW-4) are obtained from the drainage channel in the vicinity of MW- 2R. Surface water sampling location SW-3 is located south of the entrance road near MW-2R; while SW-4 is located on the north side of the entrance road, downstream of SW-3. Table 1 Existing groundwater monitoring well details Depth to Top Of NC State NC State Well Top of Screened Casing Ground OSR LF Plane Plane Diameter Well Depth Screen Screened Interval Elevation Elevation WELL Installed Northing Easting (inches) (ft bgs) (ft bgs) Interval (ft) Geology (ft MSL) (ft MSL) MW-1R 12/27/1995 820,411 1,622,983 2 60 45 15 Granitic saprolite 836.42 833.40 MW-2R 12/29/1995 820,974 1,622,722 2 23 8 15 Granitic saprolite 785.22 781.81 MW-3R 7/7/1999 821,237 1,621,463 2 27 12 15 Granitic saprolite 776.60 772.90 MW-4R 12/28/1995 820,435 1,621,428 2 20 5 15 Granitic saprolite 767.96 765.70 MW-5R 12/29/1995 820,137 1,622,130 2 32 17 15 Granitic saprolite 784.36 782.30 MW-7 12/28/1995 820,886 1,621,424 2 48 33 15 Granitic saprolite 803.66 802.10 MW-8 7/7/1999 821,930 1,621,485 2 27 12 15 Granitic saprolite 762.50 759.80 MW-9 8/11/2004 822,311 1,621,986 2 60 45 15 Sand 790.28 788.04 MW-10 8/10/2004 822,626 1,622,699 2 21 6 15 Sand 738.21 735.70 MW-11 8/10/2004 822,307 1,622,838 2 20 5 15 Sand 732.59 730.35 MW-12 8/9/2004 821,844 1,622,955 2 16 6 10 Silt 739.07 736.41 MW-13 8/9/2004 821,500 1,622,915 2 20 5 15 Sand 751.23 749.19 MW-14 8/11/2004 822,420 1,622,260 2 60 45 15 Sand 783.88 781.44 MW-15 4/6/2012 821,083 1,622,884 2 48 33.2 15 Bedrock 802.85 800.58 Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Monitoring Network The sampling plan for OSR is provided in Table 2. Table 2 Sampling parameters and schedule Method Parameter(s)' Frequency Monitoring wells Surface water EPA 300.0 Sulfate 2x/year All All EPA 6010 Trace metals 2x/year All All EPA 7470 Mercury 2x/year All All EPA 8081 Pesticides: all Fall of odd years All None (2021) Pesticides recently detected: 2x/year MW-1 R, MW- None 4,4'-DDD, 4,4'-DDT, aldrin, alpha-BHC, 2R, MW-4, MW- delta-BHC, endosulfan I, endosulfan II, 7, MW-10 & endrin, endrin aldehyde, heptachlor, MW-15 heptachlor epoxide & methoxychlor EPA 8082 PCBs: all Fall of odd years IM None -M (2021) EPA 8151 Herbicides: all Fall of odd years All None (2021) Herbicides previously detected: 2x/year MW-1 R, MW- None 2,4,5-TP (Silvex), 2,4-D 2R, MW-4R & MW-15 EPA 8260 App I VOCs + tetrahydrofuran 2x/year All All Appendix II VOCs Fall of odd years All None (2021) Appendix II VOCs recently detected: 2x/year None dichlorodifluoromethane 1,1 1,4-dioxane 2x/year All All EPA 8270 SVOCs: All Fall of odd years All None (2021) SVOCs recently detected: 2x/year MW-1 R, MW- SW-2 benzo(a)anthracene, bis(2- 2R, MW-4R-, ethyl hexyl)phthalate, chrysene, MW-3R & MW- dibenz(a,h)anthracene, & indeno(1,2,3- 15 cd)pyrene SM 2320B Alkalinity 2x/year All All SM 2540C Total dissolved solids 2x/year All All SM 4500 Chloride, cyanide, sulfide 2x/year All All Field Temperature, specific conductance, 2x/year All All dissolved oxygen, redox, turbidity, pH Field Total well depth, static water level 2x/year All NA NA — Not applicable Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Data Collection 3 Data Collection 3.1 Water Level Measurements On May 4, 2020, static groundwater level measurements were obtained from the 14 existing groundwater monitoring wells, MW-1 R through MW-15 (MW-6 was abandoned). Groundwater depths were measured to the nearest 0.01 foot from the top of the PVC casing prior to purging each well. Depth to water data is used to calculate static groundwater elevations (Table 3). Historic groundwater elevations are depicted on Figure 2. Table 3 Groundwater elevations Well ID Nov-17 May-18 Nov-18 May-19 Nov-19 May-20 MW-1 R 801.59 800.85 801.34 802.55 803.08 803.60 MW-2R 777.00 777.39 777.75 778.47 777.35 778.53 MW-3R 756.20 757.57 760.08 762.49 759.64 763.59 MW-4R 759.04 759.60 759.94 762.32 761.04 763.11 MW-5R 772.94 773.35 773.56 774.95 773.89 775.06 MW-7 767.01 766.57 767.21 769.41 769.81 771.15 MW-8 744.95 746.60 747.73 752.07 746.75 753.13 MW-9 737.45 736.82 736.80 738.65 739.68 740.00 MW-10 726.09 726.57 726.70 727.98 726.64 727.78 MW-11 728.22 728.81 729.27 728.96 728.98 729.22 MW-12 733.77 734.46 734.60 734.13 734.26 734.52 MW-13 742.19 742.75 743.34 743.15 742.87 743.36 MW-14 731.91 731.68 731.94 733.39 733.30 733.78 MW-15 763.48 763.71 764.08 765.11 763.87 765.04 ID - identification ft - feet MSL - mean sea level bgs - below ground surface ��l��rrr�����rr��rrr�rr■ ����r. � 3 . � a..i..j.■► �a�.,+rt..1.��►.�►�.►�..,tdia�la..iwlwiaelw►wi�<"t.. �.,� o ., -will lllll�`�'•' r. ��rlrlrll�iiilAIL iiiiiii�ii��ii�iii�li� Figure 2 Historical groundwater elevations 8 Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Data Collection 3.2 Groundwater Flow Hydraulic gradients were calculated between representative well pairs located in the general direction of groundwater flow. The flow velocities have been calculated based on the historic average hydraulic conductivity (0.466 ft./day) for the PWR material and an effective porosity (25 percent), as presented in Table 2-9 of the December 2003 OSR Design Hydrogeologic Investigation Report for the landfill. Table 4 presents the resulting flow velocities. The minimum and maximum values are based on the historic data collected from the site beginning in May 2003. HDR estimates a travel time of about four years between MW-2R and MW-15, based on the estimated flow rate of 49 ft/yr and a distance of 195 feet. Table 4 Interwell flow velocities Based on Flow Velocity Historic (ft./yr.) Record Nov May Nov May Nov May Nov May Min. Max. 2016 2017 2017 2018 2018 2019 2019 2020 MW-1 R to MW-4R 17 19 19 18 19 18 18 18 18 18 MW-1 R to MW-2R 22 28 27 26 27 26 26 26 28 28 MW-2R to MW-13 41 44 42 42 42 42 42 43 42 43 MW-13 to MW-10 9 10 9 9 10 10 10 9 10 9 MW-2R to MW-15 46 49 47 47 47 48 48 47 47 47 3.3 Sample Collection and Analysis HDR collected samples from the 14 wells and 4 surface water locations between May 5 and 8, 2020. Low -flow sampling techniques were used to purge groundwater from each well until stabilization of field parameters (pH, conductivity, redox, temperature, turbidity, and dissolved oxygen) occurred. Samples were collected from each of the groundwater wells using the dedicated QEDTM MicroPurge® pumps that were installed in August 2004, except MW-15, which is sampled with a variable speed submersible pump. Field parameters were recorded and are presented in Appendix B. Groundwater samples were labeled with the project name, sample ID, date, and time the sample was collected. This same information was recorded on a chain -of -custody form. The samples were placed in a cooler with ice, then transported under chain -of -custody procedures to Pace Analytical Services, LLC (Pace) in Huntersville, North Carolina (NC Cert. # 5342) for analysis. 9 Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report �J�` Data Collection Table 5 Lab detections MW- MW- MW- MW- 2L units Row s 1R 2R 3R 4R E l� 1000 250000 pg/L SulfateII_ 1 EPA 6010D im���mm Equip MW- ment 5R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 SWA SW-2 SW-3 SW-4 Blank 275000 1 10 21000 700 NE 2 pg/L Cadmium NE 1 pg/L Cobalt 010 10 NE 1 - 25 11 NE NE •/L SodiumIILLLiLII.w.....III�CLII1CilJI�I�IILSLL✓II�IIII�IISilJIIIISII�III�IIICJ4J111�11551YIIJiiYlllllllll, NE 1 • 1 NE 1 EPA 7470A �������� 1 • 12.1 11 2740 23700 2560 25700 1650 6410 ��������i 29.7 13.6 88.8 ___ :1 113 165 ; �_ 7.0 74900 1080 11300 5640 1080 ®_® 69.9 lllllllll.11llllll.®IIIIIIII.11llllll.IIIIIII,IIIIIII,IIIIIII,®llllllll.IIIIIIII,IIIllllll,11111111111111111111111111111111111111111111111111111111111,111111111, 111111111111111111111111111111IIIIIIII, S.S 11111111111111111111111111IIIIIIIIl,1111111111IIIIIIII,111111111111111111111111111111111111111111111111111111111111111,11111111, 11 EPA 6260D 3.3 �■�lll�l�l�r I_®_®____ ��� 1.6 �i�������� • NE 1,1 Chloroethane NE 111111111,111!11�1,111�111111111, 1 • _ _ _ ®III...allllllll,llllllllll11111111111®111111111111111111,1111111111,111111111111111111111111111111111111111111111111111111111111111111111111111111111111®IIIIIIIII, NE 1.1 DichlorodifluoromethaneIIIII■IIIIII♦IIIIII■IIIII■®_®-IIIIIII♦IIIIII■IIIIII■®IIIIII■IIII■IIIII■IIIII■IIIII■IIIIII■ • 1 500 10 NE 11 - 0.7 I7 pg/L Tetrachloroethene1.1 1000 NE 1 - SM • 3.4 111111111111111111111®11111111111111111,1111111111,111111111111111111111111111111111IIIIIIII,111111111111111111111111111111111111111111111111, 111111111, IIIIIII,IIIIIII, IIIIIIII,IIIIIII,®111111111111111,111111111111111111,11111111,11111111,IIIIIIII,11111111,111111.1111111,1111111,1111111, 11111111, IIIIIII,IIIIIII, IIIIIIII,IIIIIII, 4.7 111111111111111,111111111111111111.11111111,11111111,IIIIIIII,IIIIIIII,111111.1111111,1111111,1111111, 11111111, IIIII■IIIII■IIIIII■IIIIIII,®IIII■IIIII■®IIIIII■IIIIII■IIIIII■IIIIII■IIIIIII♦IIII■IIIII■IIIII■IIIII■IIIIII■ 1111111,11111111,1111111,1111111,111111111111111,111111111111111111,11111111,11111111,®IIIIIIII,IIIIII.IIIIIII,IIIIIII,IIIIIII, ®IIIIIII,®IIIIIII,I®�IIIIIII,®IIIIIIII.IIIIIIII, IIIIIIII, IIIIIIII, IIIIIIII,®111111111111111,1111111,®IIIIIIII, ®1111111,11111111,1111111,1111111,111111111111111,11111111111IIIIIIII,11111111,11111111,11111111,1111111111111111111111111111111111111111111, 11111111, 0.99 ______-________IIIII■IIIIII■ 11.1 NE pg/L• .. • SM 2540C NE 1000 DissoNed Solids SM 4500-CI-E 1111 1111 . •Chloride SM 4500-S2D NE NE pg/L Sulfide EPA 8270E 11 NE 1 _ _ _ EPA 8260D Mod. Field feet Static Water Level 1114YI111LL114GY�ICtlLYII4IY�ICYIIYLW �11.'i'i`W' IlSlllJllll'L'JIIIIIIIII, 840000= 854000 [M[MM[M 11600001= 612000 Illll�l�l�ll�ll��ll�ll�lml�l�l�l�ll�� IIIIII■IIIII■IIIII■IIIIII■IIIII■IIIII■IIII■IIIII■IIIIIII■IIIIIII♦IIIIII■IIIIII■IIIIII■IIIIII■_©IIIII■IIIII■IIIIII■ 11111111,1111111,1111111,11111111,1111111,1111111,111111111111111,111111111111111111,11111111,11111111,11111111,11111111,111111,®IIIIIII,IIIIIII,IIIIIIII, IIIIIIII,IIIIIII�' �� �1 �IIIIIIII, Note - To distinguish non detections (ND) from not sampled (NS), refer to complete laboratory analysis. This table represents both ND and NS as blanks. 10 Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Analytical Results 4 Analytical Results Historical concentrations are presented in Appendix A. A copy of the laboratory report is provided in Appendix B. Field parameters recorded prior to sample collection are presented in Appendix C. Other field data sheets are also provided in Appendix C. A Microsoft Excel file containing the analytical data in NCDEQ electronic data deliverable format is included as part of Appendix D. 4.1 Groundwater During this sampling event, 36 detections exceeded the 2L Standards. These exceedances consisted of 12 parameters at 11 well locations. Concentrations of constituents detected during this sampling event are presented in Table 5. In 2011, MW-2R concentrations of benzene and PCE above 2L Standards triggered assessment monitoring. The trends of detected constituents in MW-2R are shown on Figure 3. In general, concentrations of detected constituents have decreased since the November 2019 sampling event, with the exception of cobalt and chloride. Recent MW-2R Groundwater Detections OSR Construction & Demolition Landfill Permit 34-12 1000000 100000 10000 w u c 100 v 10 0.1 1� 11 1`Z 1b '\1 15 16 11 1$ 1g 2� 71 yat` ,Jam ,Jai ,Jai .Jai .Jai ,Jam ,Jai ,Jai .Jai .Jai ,Jai 1 1 NV 1 1 1 '� 1 1 Date Collected Figure 3 MW-2R groundwater detections tTotal Dissolved Solids tAlkalinity, Total as CaCO3 —Sulfate —Sodium —k--Chloride $-Manganese ---iron X Methane Barium —@—Tetrahydrofuran f Cobalt © Selenium ♦ Antimony O Thallium —*--Methylene Chloride 81,4-Dioxane(p-Dioxane) —X--Benzene —Chromium X Lead —*—Vanadium —6—Tetrachloroethene tVinyl chloride ■ bis(2-Ethylhexyl)phthalate ■ Cadmium ■ 4,4'-DDT Heptachlor 1 Chloromethane O delta-BHC X Aldrin E alpha-BHC X Nitrogen, Ammonia 11 Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Analytical Results 4.2 Surface Water Surface water analytical results were compared to 15A NCAC 02B (213 Standards). The 2B Standards do not provide criteria for alkalinity or iron, so the EPA's Nationally Recommended Water Quality Criteria for Class C freshwater (Class C Standards) was applied. There were no 2B exceedances; however, all locations exceeded the Class C standards for alkalinity and iron. Two semi -volatile organic compounds (dibenz(a,h)anthracene and indeno(1,2,3-cd)pyrene) were detected in the sample from SW-2. These compounds were last detected in MW-3R, which is located on the opposite (west) side of the landfill, during the November 2015 event. 4.3 Assessment Monitoring Appendix II pesticides (heptachlor and heptachlor epoxide) that were previously detected in 2012 were not detected during this event. Two Appendix II constituents (dibenz(a,h)anthracene and indeno(1,2,3-cd)pyrene) were detected in the surface water sample from SW-2 during this event. Dibenz(a,h)anthracene and indeno(1,2,3-cd)pyrene are polycyclic aromatic hydrocarbons (PAHs) found in fossil fuels and are also products of incomplete combustion. Note that these constituents were not detected in groundwater samples collected from wells MW-1 R, MW-2R, MW-4R, MW-3R, and MW-15 during the current monitoring event. Other Appendix II constituents were last detected during the November 2017 sampling event. 4.4 Landfill Gas Landfill gas is measured at MW-2R and wells in the vicinity of MM-1 during each groundwater sampling event. The results indicate the presence of carbon dioxide above ambient levels in MM-1 during each of the last four monitoring events. Note that the City is responsible for quarterly sampling of all methane monitoring wells and the related reporting, which is not included in this document. Gas readings taken during this event are presented in Table 6. Table 6 Gas readings Date ID # HZS ppm CH4 M COZ M OZ M) 26-Nov-18 MM-1 0.0% 26-Nov-18 MW-1 R 0.0% 0.1 % 20.2% 26-Nov-18 MW-2R 0.0% 0.6% 22.6% 26-Nov-18 MW-13 0.0% 0.2% 19.9% 26-Nov-18 MW-15 0.0% 0.2% 19.8% 6-May-19 MM-1 0.0% 6-May-19 MW-1 R 0.0% 0.0% 20.0% 6-May-19 MW-2R 0.0% 0.0% 19.7% 6-May-19 MW-13 0.0% 0.0% 20.1% 6-May-19 MW-15 0.0% 0.3% 19.4% 12-Nov-19 MM-1 0.0% 12-Nov-19 MW-1 R 0.0% 0.0% 21.1 % 12-Nov-19 MW-2R 0.0% 0.0% 21.0% 12-Nov-19 MW-13 0.0% 0.0% 21.1 % 12-Nov-19 MW-15 0.0% 0.2% 20.7% 4-May-20 MM-1 1 0.0% •' .', 4-May-20 MW-1 R 0 0.0% 0.1 % 20.9% 4-May-20 MW-2R 0 0.0% 0.1 % 20.7% 4-May-20 MW-13 0 0.1 % 0.1 % 20.9% 4-May-20 MW-15 0 0.0% 0.2% 21.2% Highlighted cells are outside of normal atmospheric ranges 12 Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Summary 5 Summary • During this sampling event, 36 detections (12 parameters at 11 well locations) exceeded the 2L Standards in groundwater samples. In general, the quantity of detections and magnitude of concerntrations are consistent with results from previous events. • Of the 12 parameters detected above 2L Standards, concentrations of seven parameters (sulfate, iron, vanadium, benzene, methylene chloride, PCE, and vinyl chloride) generally decreased since the November 2019 monitoring event, while concentrations of five parameters (cobalt, manganese, mercury, TDS, and 1,4-dioxane) generally increased since the last monitoring event. • No target analytes were detected above the 2B Standards in surface water samples collected during this monitoring event. However, two Appendix II constituents (dibenz(a,h)anthracene and indeno(1,2,3-cd)pyrene) were detected above the laboratory reporting limit in the sample collected from SW-2. • Results of limitied landfill gas monitoring conducted during this event indicate that the concentration of carbon dioxide in MM-1 exceeded ambient levels and is consistent with previous readings at this monitoring location. Methane concentrations in the wells and monitoring points did not exceed the lower explosive limit (LEL) of 5.0% during this event. 6 Recommendations Based on the results of groundwater, surface water, and landfill gas monitoring conducted during this semi-annual event, no changes to the OSR Assessment Monitoring Plan are recommended at this time. 13 Winston-Salem/Forsyth County Utilities Old Salisbury Road Landfill Assessment Monitoring Report ��� Recommendations This page intentionally left blank. 14 Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report Appendix A — Summary of Monitoring Results Appendix Monitoring Summary Groundwater Detections by Well Location Historical Detections by Date Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix A — Summary of Monitoring Results This page intentionally left blank. Al Facility Permit 34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard 50 pg/L 2,4,5-T 50 pg/L MW- 70 pg/L 2,4-D 70 pg/L MW- 70 pg/L MW-1 0.3 pg/L Pentac li 0.3 pg/L Equip 40 pg/L Endosu 40 pg/L MW- 40 pg/L MW-1 0.008 pg/L Heptac 0.008 pg/L MW-1 0.004 pg/L Heptac 0.004 pg/L MW-1 NE pg/L 2,4-Din NE pg/L MW- NE pg/L 2,6-Din NE pg/L MW- 200 pg/L Benzo( 200 pg/L MW- 1000 pg/L Butylbe 1000 pg/L MW-15 pg/L Dibenz 0.005 pg/L MW- 0.005 pg/L SW-2 100 pg/L Di-n-oc 100 pg/L MW- 100 pg/L MW-1 0.05 pg/L Indeno( 0.05 pg/L MW- 0.05 pg/L _ SW-2 6 pg/L L11Dic 6 pg/L MW- 6 pg/L MWFA - 0.4 pg/L 1,2-Dic 0.4 pg/L MW- 6 pg/L 1,4-Dic 6 pg/L MW- 3 pg/L 1,4-Dio 3 pg/L MW- 3 pg/L MW- 3 pg/L MW- 3 pg/L MW-1 3 pg/L MW-1 3 pg/L SW-2 3 pg/L SW-3 3 pg/L SW-4 o >+ M M j O z rn >, N o j O z o >, N ^ N 0 ti O z ti (B (0 O z co (0 LO O z LO v O z v CU • .• - . ment Blank 0 NONE • 0.12 l epoxide MEME A MEN 0.17 0 0.09 • • - - N ZEN trotoluen - - M M M M MNE 1 2ylphthalate ■ MEN • • - - 1.1 mop • • - - ______� ___ ID �. . 0 • o( thane ID ane p-Dioxane) —ME 3.9 3.7 4.7 4 5.1ol 6.6 7.9 6.4 8.5 10.3 5.3 E M 6.6 6.5 0 1 W-S GW Revised.xlsb 1 of 4 Al 40 pg/L 40 pg/L 40 pg/L 40 pg/L NE pg/L NE pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 6000 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 1 pg/L 700 pg/L 700 pg/L 3000 pg/L 3000 pg/L 3000 pg/L 70 pg/L 70 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard 2-Hexanone 0.72 0.69 0.96 _ MW-10 SW-2 1.8 SW-4 3.1 4-Methyl-2-pentanone (MIBK) 2.5 5.6 2.2 MW-10 0.65 1.7 1.1 2.8 2.6 Acetone Equipment Blank 10.2 18.3 M W-2 R 10.3 MW-3R 21.4 MW-4R 11 M W-5R 18.4 MW-7 15.7 MW-8 15.8 MW-10 16.4 13.7 12.1 22.5 14.1 11.8 MW-11 21.1 MW-12 12.1 MW-13 17.3 MW-14 14.7 MW-15 13.2 SW-1 11.2 SW-2 12.9 SW-3 16.2 SW-4 16 Benzene MW-2R MW-4R 0.38 0.42 0.28 MW-5R 0.28 MW-7 0.48 0.6 0.68 0.37 0.41 0.39 0.38 0.43 0.42 0.26 0.29 MW-10 0.56 0.78 0.33 0.55 0.55 0.57 0.52 0.83 0.46 0.44 MW-12 0.29 0.25 0.33 SW-3 0.73 0.42 0.54 0.32 SW-4 0.25 Carbon Disulfide MW-10 I 2.1 2 5.2 Chloroethane MW-2R _ 2.1 MW-7 0.85 Chloroform MW-15 0.45 0.44 0.44 0.4 0.44 0.7 0.44 0.26 0.49 Chloromethane MW-2R 0.25 MW-7 0.13 M W-11 0.23 SW-2 0.12 W-S GW Revised.xlsb 2 of 4 Al 70 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L 70 pg/L 1000 pg/L 1000 pg/L 1000 pg/L 1000 pg/L 1000 pg/L 1000 pg/L 600 pg/L 600 pg/L 600 pg/L 500 pg/L 500 pg/L 500 pg/L 500 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 3 pg/L 500 pg/L 500 pg/L 500 pg/L 500 pg/L 500 pg/L 500 pg/L 0.7 pg/L 0.7 pg/L 0.7 pg/L 0.7 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard cis- 1,2-Dichloroethene 1.1 0.9 0.85 0.71 0.38 0.2 MW-1 R 1.2 0.76 0.62 MW-2R 0.84 0.95 0.67 0.38 0.55 0.66 0.6 0.51 0.47 0.26 0.5 0.38 MW-7 0.91 1.4 1.5 0.86 0.85 1.1 1.1 1.1 1.1 0.77 0.8 0.73 0.73 0.37 MW-10 0.23 0.27 0.23 0.2 0.33 0.35 MW-12 0.4 0.23 SW-2 0.33 SW-3 0.26 SW-4 0.32 Dichlorodifluoromethane MW-2R _ 0.26 MW-7 0.52 0.62 1 MW-9 1.1 0.9 1.4 0.99 1.2 1.7 1.2 1.5 0.88 0.76 MW-12 0.23 MW-14 2.4 4.5 3 2.4 3 3.6 3.9 3.6 2.3 3.6 2.1 Ethylbenzene 0.38 MW-1 R MW-10 0.41 0.53 0.55 0.4 1 0.73 m&p-Xylene MW-5R 0.73 MW-7 0.72 0.93 1 1.1 1.7 1.6 1.4 1.2 2.2 MW-10 0.68 1.3 1.1 1.2 2.1 Methylene Chloride _ Equipment Blank 2.4 MW-1 R MW-2R 1.1 MW-3R MW-4R MW-5R MW-7 1.7 MW-8 MW-10 MW-11 MW-12 MW-14 MW-15 SW-1 SW-2 SW-3 SW-4 o-Xylene _ MW-2R MW-5R 0.45 MW-7 0.46 0.54 0.68 0.59 0.65 0.62 0.68 MW-10 0.34 0.84 0.28 0.53 0.78 1.1 0.97 M W-11 0.27 Tetrachloroethene MW-2R :: MW-7 MW-14 1 0.53 0.48 0.52 1.8 0.84 1.5 1.1 0.68 1.2 1.1 2.3 1.3 2.3 2.3 2.9 2.11 2.9 1.1 2.8 1.2 1.4 2 2 1.6 2.4 2 1 1.2 0.33 0.31 0.46 0.63 0.47 0.27 0.4 0.36 2.1 0.43 0.85 0.65 0.48 0.61 W-S GW Revised.xlsb 3 of 4 Al Facility Permit 34-12 Old Salisbury Road Landfill (C&D) OSR Concern (Multiple Items) Selected groundwater detections of concern within the last 6 years Qualifier (Multiple Items) Highlighted cells are at or above the current standard NE pg/L Tetrahydrofuran NE pg/L Equipment Blank NE pg/L MW-2R 38.6 NE pg/L MW-4R 11.4 NE pg/L MW-7 70.5 NE pg/L MW-10 130 NE pg/L MW-11 NE pg/L MW-12 NE pg/L MW-15 8.9 NE pg/L SW-2 NE pg/L SW-3 NE pg/L SW-4 9.1 600 pg/L Toluene 600 pg/L MW-2R 600 pg/L MW-5R 600 pg/L MW-10 600 pg/L MW-11 600 pg/L MW-12 600 pg/L MW-13 600 pg/L SW-2 3 pg/L Trichloroethene 3 pg/L MW-1 R 3 pg/L MW-2R 1.1 3 pg/L MW-7 2000 pg/L Trichlorofluoromethan 2000 pg/L MW-2R 2000 pg/L MW-7 5.6 2000 pg/L MW-9 1.3 2000 pg/L MW-10 2000 pg/L MW-12 2000 pg/L MW-14 1 2000 pg/L MW-15 2000 pg/L SW-4 88 pg/L Vinyl acetate 88 pg/L MW-2R 0.03 pg/L Vinyl chloride 0.03 pg/L MW-2R 500 pg/L Xylenes (Total) 500 pg/L MW-10 e 83 51.3 45.4 46 59.1 28 36.3 8.6 11.4 9.3 77.9 80.4 50.5 24.9 20.1 141 113 169 192 135 131 182 4.5 5.9 8.2 9.2 14.8 61.3 6.1 3.4 6.7 13.7 5.7 1.7 0.26 0.35 0.27 1 0.74 0.58 1.1 0.97I 0.9I 0.93I 0 .3 0.93I 1 1.5 4 2 1.2 1.2 1.6 1.6 0.86 1.7 1.3 1.3 1.4 1.2 0.81 1 0.89 1.4 0.52 1.5 0.92 0.86 0.79 0.8 0.87 0.21 0.42 0.22 0.71 0.32 2 1.1 3.2 39.1 49.6 35.8 34.6 79.2 72.6 13.6 3.5 7 5.8 15.9 11.8 32 21.7 13.5 17.7 14.1 8.8 5.2 237 6.1 120 145 106 18.6 11.4 26.8 12.4 12 16.8 27.3 19.8 16.9 15.5 21.4 18.4 6.3 3.3 10.2 9.7 3.5 3.6 4.1 4.4 0.27 0.52 0.63 1.2 0.71 0.71 0.66 1 0.79 1.5 0.85 2.4 0.71 3.7 0.91 1.5 0.92 1.4 0.79 1.2 0.62 1.4 1 1.3 1.1 0.98 0.96 0.47 0.2 1 2.8 1.4 0.82 0.22 0.32 0.75 0.58 1.1 0.54 0.59 0.57 0.34 2.1 4.4 5.1 4.8 4.4 3.9 5.3 0.27 W-S GW Revised.xlsb 4 of 4 A2 NE pg/L 10 pg/L 700 pg/L 0.05 pg/L 4 pg/L 3 pg/L 700 pg/L 250000 pg/L 10 pg/L 5 pg/L 70 pg/L 70 pg/L 600 pg/L 300 pg/L 15.0 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L 600 pg/L 500000 pg/L 3 pg/L 1000 pg/L 6 pg/L 350 pg/L 0.4 pg/L 6 pg/L 3 pg/L 50 pg/L 70 pg/L NE pg/L NE pg/L 4000 pg/L 40 pg/L 0.1 pg/L 6000 pg/L 0.002 pg/L NE pg/L 0.006 pg/L 1 pg/L 10 pg/L 700 pg/L 1 pg/L 3 pg/L 2 pg/L 250000 pg/L 3000 pg/L 70 pg/L 3 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.019 pg/L 1000 pg/L 2 pg/L 2 pg/L 0.008 pg/L 300 pg/L 15 pg/L 500 pg/L 50 pg/L 1 pg/L NS pg/L 40 pg/L 3 pg/L 6 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Value Column Historical Labels detections by well location Row Labels -MW-1R AL Alkalinity, Total as CaCO3 86600 84000 83800 84100 76100 71400 68600 64300 54900 48100 39600 Arsenic 5.8 Barium 290 290 285 284 263 260 272 241 228 207 164 Benzo(a)anthracene Beryllium 0.5 bi s (2-Ethylhexyl) phtha late Carbon Disulfide Chloride 9050 9150 9770 8920 9040 9290 8860 9630 9000 8510 7640 Chromium 4 Chrysene cis-1,2-Dichloroethene 1.2 1.1 0.9 0.85 0.71 0.76 0.62 0.38 0.2 Cyanide Ethylbenzene 0.38 Iron 111 43.1 54.8 96.2 78.8 82.8 Lead Manganese 31.41 24.71 19.5 16.7 17.6 11.8 12.5 7.3 7.2 2.8 Mercury 0.57 0.34 0.23 Methylene Chloride 2.3 Nickel 1.5 Selenium Silver Sodium 16800 16300 15800 16500 15500 15200 15800 14600 13300 13200 11600 Sulfate 1380 1080 1070 1700 Toluene Total Dissolved Solids 172000 180000 202000 164000 166000 153000 165000 154000 138000 78000 133000 Trichloroethene 0.65 Zinc 4.3 5.2 5.1 5 5.5 5.7 5.6 MW-2R 1,1-Dichloroethane 0.46 0.6 0.43 0.39 0.54 0.48 0.48 0.53 0.49 1,1-Dichloroethene 1,2-Dichloroethane 0.24 1,4-Dichlorobenzene 0.56 0.45 0.41 0.37 0.46 0.39 0.38 1,4-Dioxane (p-Dioxane) 2.3 2.1 2,4,5-TP (Silvex) 0.072 0.14 2,4-D 0.43 2,4-Dinitrotoluene 5.9 2,6-Dinitrotoluene 8.1 2-Butanone (MEK) 2-Hexanone 4,4'-DDT Acetone 10.3 Aldrin Alkalinity, Total as CaCO3 688000 736000 577000 573000 663000 670000 587000 571000 482000 440000 358000 alpha-BHC Antimony Arsenic Barium 309 359 260 258 289 1 323 323 272 324 279 287 Benzene bi s (2-Ethylhexyl) phtha late Cadmium 0.66 Chloride 64300 52500 42300 34500 42200 47600 50400 47600 47700 48700 44200 Chloroethane Chloroform Chloromethane 0.25 Chromium 3.3 2.7 2.8 2.6 cis-1,2-Dichloroethene 0.84 0.95 0.67 0.38 0.55 0.66 0.6 0.511 0.47 0.26 Cobalt 1 Copper 18.6 9.6 2.6 6.3 Cyanide 4.1 5 5.1 7.5 delta-BHC Dichlorodifluoromethane 0.26 Endrin Endrin aldehyde Heptachlor Iron • .•1 o•o .� l -we .0 Lead 3.2 3.3 m&p-Xylene Manganese e o e e i•ii ELTeMe EME0 Mercury Methane Methoxychlor Methylene Chloride 1.1 1.3 2.3 Naphthalene Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 NE pg/L 10 pg/L 700 pg/L 0.05 pg/L 4 pg/L 3 pg/L 700 pg/L 250000 pg/L 10 pg/L 5 pg/L 70 pg/L 70 pg/L 600 pg/L 300 pg/L 15.0 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L 600 pg/L 500000 pg/L 3 pg/L 1000 pg/L 6 pg/L 350 pg/L 0.4 pg/L 6 pg/L 3 pg/L 50 pg/L 70 pg/L NE pg/L NE pg/L 4000 pg/L 40 pg/L 0.1 pg/L 6000 pg/L 0.002 pg/L NE pg/L 0.006 pg/L 1 pg/L 10 pg/L 700 pg/L 1 pg/L 3 pg/L 2 pg/L 250000 pg/L 3000 pg/L 70 pg/L 3 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.019 pg/L 1000 pg/L 2 pg/L 2 pg/L 0.008 pg/L 300 pg/L 15 pg/L 500 pg/L 50 pg/L 1 pg/L NS pg/L 40 pg/L 3 pg/L 6 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Row Labels Historical detections by well location MW-1R Alkalinity, Total as CaCO3 37600 30000 28100 29800 26300 27100 27500 Arsenic Barium 142 124 106 109 91.7 93.8 82.6 Benzo(a)anthracene Beryllium bis(2-Ethylhexyl)phthalate 2.4 Carbon Disulfide Chloride 7090 5600 5880 5910 5320 5350 Chromium Chrysene 1.5 cis-1,2-Dichloroethene Cyanide 4.4 Ethylbenzene Iron 85.8 52.9 Lead Manganese 2.9 Mercury Methylene Chloride Nickel Selenium Silver Sodium 10600 10800 9940 9080 9180 9440 7670 Sulfate 1720 Toluene Total Dissolved Solids 120000 91000 103000 84000 95000 93000 95000 Trichloroethene Zinc MW-2R 1.1 1,1-Dichloroethane 1.1 0.83 1.3 1.2 1.2 1.2 1,1-Dichloroethene 36.6 38.7 1,2-Dichloroethane 1,4-Dichlorobenzene 0.4 1,4-Dioxane (p-Dioxane) 2,4,5-TP (Silvex) 0.23 2,4-D 1.1 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Butanone (MEK) 2-Hexanone 0.48 4,4'-DDT Acetone 20.3 3.7 Aldrin Alkalinity, Total as CaCO3 453000 344000 349000 363000 277000 196000 219000 165000 alpha-BHC Antimony Arsenic Barium 339 324 3111 3241 335 366 351 Benzene 1.1 bis(2-Ethylhexyl)phthalate Cadmium Chloride 49800 50500 56700 50000 64000 61500 62400 39900 Chloroethane 2.1 Chloroform 0.16 0.26 Chloromethane Chromium 3.4 cis-1,2-Dichloroethene 0.5 0.38 0.411 0.26 0.25 0.331 0.46 Cobalt 9.6 Copper Cyanide 4.2 delta-BHC D ich to rod iflu orom etha ne Endrin 0.27 Endrin aldehyde 0.23 0.2E Heptachlor Iron •O •:� Lead m&p-Xylene 0.66 Manganese EW 1 I Mercury Methane 1280 Methoxychlor 0.83 Methylene Chloride Naphthalene 0.86 1.3 1.6 1.9 84.71 85.41 1 85.3 1.41 0.961 1 1.4 0.51 1.1 0. 0.74 0.29 103 1.2 92.8 0.48 1 80.-1 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 74.3 85 90.3 105 8 0.05 pg/L Benzo(a)anthracene 4 pg/L Beryllium 3 pg/L bis(2-Ethylhexyl)phthalate 700 pg/L Carbon Disulfide 250000 pg/L Chloride 10 pg/L Chromium 0.88 0.64 0.49 5 pg/L Chrysene 70 pg/L cis-1,2-Dichloroethene 70 pg/L Cyanide 600 pg/L Ethylbenzene 300 pg/L Iron 15.0 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver 0.62 0.43 NE pg/L Sodium 250000 pg/L Sulfate 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 3 pg/L Trichloroethene 1000 pg/L Zinc MW-2R 6 pg/L 1,1-Dichloroethane 350 pg/L 1,1-Dichloroethene 0.4 pg/L 1,2-Dichloroethane 6 pg/L 1,4-Dichlorobenzene 3 pg/L 1,4-Dioxane (p-Dioxane) 50 pg/L 2,4,5-TP (Silvex) 70 pg/L 2,4-D NE pg/L 2,4-Dinitrotoluene NE pg/L 2,6-Dinitrotoluene 4000 pg/L 2-Butanone (MEK) 40 pg/L 2-Hexanone 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone 0.002 pg/L Aldrin NE pg/L Alkalinity, Total as CaCO3 0.006 pg/L alpha-BHC 1 pg/L Antimony 10 pg/L Arsenic 700 pg/L Barium 88.5 98.8 102 107 T 1 pg/L Benzene 3 pg/L bis(2-Ethylhexyl)phthalate 2 pg/L Cadmium 250000 pg/L Chloride 3000 pg/L Chloroethane 70 pg/L Chloroform 3.4 3 pg/L Chloromethane 10 pg/L Chromium 1.6 0.5 0.79 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.019 pg/L delta-BHC 1000 pg/L Dichlorodifluoromethane 2 pg/L Endrin 2 pg/L Endrin aldehyde 0.008 pg/L Heptachlor 300 pg/L Iron 15 pg/L Lead 500 pg/L m&p-Xylene 50 pg/L Manganese 1 pg/L Mercury NS pg/L Methane 40 pg/L Methoxychlor 3 pg/L Methylene Chloride 6 pg/L Naphthalene Highlighted cells are at or above the current standard. Blank cells indicate either INS or ND. W-S GW Revised.xlsb 94 90 5.5 96.3 460 120 100 1 3.5 1 4.31 2.3 55 60 56 140 1 1.9 2.2 2.1 8.9 A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 150 110 130 150 160 100 290 100 180 224 0.05 pg/L Benzo(a)anthracene 4 pg/L Beryllium 3 pg/L bis(2-Ethylhexyl)phthalate 700 pg/L Carbon Disulfide 28 23 250000 pg/L Chloride 10 pg/L Chromium 6.6 5.2 7.8 3 6 5 pg/L Chrysene 70 pg/L cis-1,2-Dichloroethene 70 pg/L Cyanide 600 pg/L Ethylbenzene 300 pg/L Iron 15.0 pg/L Lead 12 6 50 pg/L Manganese 1 pg/L Mercury 0.2 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 3 pg/L Trichloroethene 1000 pg/L Zinc MW-2R 6 pg/L 1,1-Dichloroethane 350 pg/L 1,1-Dichloroethene 0.4 pg/L 1,2-Dichloroethane 6 pg/L 1,4-Dichlorobenzene 3 pg/L 1,4-Dioxane (p-Dioxane) 50 pg/L 2,4,5-TP (Silvex) 70 pg/L 2,4-D NE pg/L 2,4-Dinitrotoluene NE pg/L 2,6-Dinitrotoluene 4000 pg/L 2-Butanone (MEK) 86 40 pg/L 2-Hexanone 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone 0.002 pg/L Aldrin NE pg/L Alkalinity, Total as CaCO3 0.006 pg/L alpha-BHC 1 pg/L Antimony 10 pg/L Arsenic 700 pg/L Barium 61 180 120 150 190 340 200 160 350 1 pg/L Benzene 3 pg/L bis(2-Ethylhexyl)phthalate 2 pg/L Cadmium 250000 pg/L Chloride 3000 pg/L Chloroethane 70 pg/L Chloroform 3 pg/L Chloromethane 10 pg/L Chromium 3.9 3 7.8 NMI 4 9 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.019 pg/L delta-BHC 1000 pg/L Dichlorodifluoromethane 2 pg/L Endrin 2 pg/L Endrin aldehyde 0.008 pg/L Heptachlor 300 pg/L Iron 15 pg/L Lead 6.5 6.9 14 8 500 pg/L m&p-Xylene 50 pg/L Manganese 1 pg/L Mercury 0.4 NS pg/L Methane 40 pg/L Methoxychlor 3 pg/L Methylene Chloride 79 6 pg/L Naphthalene Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 100 pg/L NS pg/L 500 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L 0.7 pg/L NE pg/L 0.2 pg/L 600 pg/L 500000 pg/L 3 pg/L 2000 pg/L 0.3 pg/L 88 pg/L 0.03 pg/L 500 pg/L 1000 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 200 pg/L 4 pg/L 3 pg/L 2 pg/L 700 pg/L 250000 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.005 pg/L 0.05 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L 2000 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 0.1 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 1000 pg/L 2 pg/L 250000 pg/L 3 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.019 pg/L 42 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Value Column Historical Labels detections by well location Row Labels Nickel 21.1 21.1 13.4 16.1 16.8 20.3 17 18.5 17.9 18 17 Nitrogen, Ammonia o-Xylene Selenium 6.1 Silver Sodium 65600 71900 57300 64400 73200 77600 72400 70200 61500 61400 51400 Sulfate 76400 111000 85100 95900 105000 122000 110000 121000 115000 115000 98400 Sulfide 80.1 Tetrachloroethene It : 38.6 83 51.3 45.4 46 59.1 28 Tetrahydrofuran 36.3 39.1 49.6 35.8 34.6 Thallium Toluene 0.27 Total Dissolved Solids me 33M woollue ..M M��� 0.71 0.66 0.79 Trichloroethene 1.1 1.1 0.97 0.9 0.93 1.3 0.93 1 1.2 Trichlorofluoromethane 1.5 0.71 1 1.5 Vanadium Vinyl acetate 2 Vinyl chloride Xylenes (Total) Zinc 24.5 18 5.8 8.7 MW-3R Acetone 21.4 Alkalinity, Total as CaCO3 70900 69800 488000 192000 115000 78900 114000 133000 87800 102000 107000 Arsenic 6.4 5.7 9 5.5 3.9 3.3 Barium 257 286 320 275 234 278 309 297 278 271 214 Benzo(g,h,i)perylene 1 Beryllium 0.35 bi s (2-Ethylhexyl) phtha late Cadmium Carbon Disulfide Chloride 3320 2000 44600 2660 2180 2650 2520 2050 2470 2990 2990 Chromium Cobalt if Copper 6.2 Cyanide 6.4 5 4.4 4.7 Dibenz(a,h)anthracene Indeno(1,2, 3-cd )pyrene Iron �� •�� �� :�� •�:�� �� �� �� �� �� .010 Lead 3.4 4.9 3.4 3.4 3.5 3.8 2.7 Manganese •,�.� .:�� �� •:� Mercury 0.65 Methylene Chloride 2.3 Nickel 1.2 Selenium 6.3 5 5.5 Silver Sodium 2150 2520 2540 2770 2680 2380 2240 2450 2310 2590 Sulfate 801 771 1210 1300 691 1530 1800 2200 3000 Tin 4.8 Total Dissolved Solids 146000 179000 M 213000 177000 164000 133000 168000 188000 137000 182000 Vanadium Zinc 8.7 MW-4R 2.4 1,4-Dioxane (p-Dioxane) 4,4'-DDT Acetone 11 Alkalinity, Total as CaCO3 517000 384000 129000 291000 101000 461000 315000 454000 99000 144000 117000 Arsenic Barium 176 166 216 222 270 198 343 255 210 184 306 Benzene 0.38 Butylbenzylphthalate 1.7 Cadmium Chloride 42100 34000 2220 25200 12500 49200 35800 58400 13800 16900 22200 Chloromethane Chromium 6.4 3.2 1 3.2 Cobalt Copper 2.7 5 2.8 Cyanide 4.2 delta-BHC Endosulfan II Iron 214 292 Lead Manganese �:� •� :� Mercury Methylene Chloride 2.9 Nickel 8 7.4 8.4 5 4.1 7.5 5.8 8 3.2 3.7 2.8 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 100 pg/L Nickel 25.9 20.6 27.1 20.7 21.8 22.3 NS pg/L Nitrogen, Ammonia 500 pg/L o-Xylene 0.33 0.31 0.54 0.54 0.63 1 20 pg/L Selenium 16.5 20 pg/L Silver 5.2 NE pg/L Sodium 58300 59700 46200 45700 43400 38400 250000 pg/L Sulfate 117000 136000 128000 115000 79500 95000 NE pg/L Sulfide 0.7 pg/L Tetrachloroethene 79.2 72.6 99.6 111 93.2 152 NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 600 pg/L Toluene 500000 pg/L Total Dissolved Solids . • • 0 0 8 . 3 pg/L Trichloroethene 0.85 0.71 0.89 0.68 0.77 0.82 2000 pg/L Trichlorofluoromethane 2.4 3.7 12 12.1 16.9 20.9 0.3 pg/L Vanadium 88 pg/L Vinyl acetate 0.03 pg/L Vinyl chloride 500 pg/L Xylenes (Total) 0.98 1.6 1000 pg/L Zinc 16.8 12.2 21.1 24.5 35.2 MW-3R 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 177000 155000 155000 175000 142000 150000 10 pg/L Arsenic 8.9 700 pg/L Barium 221 205 201 216 173 228 200 pg/L Benzo(g,h,i)perylene 4 pg/L Beryllium 3 pg/L bis(2-Ethylhexyl)phthalate 2 pg/L Cadmium 700 pg/L Carbon Disulfide 250000 pg/L Chloride 2940 3260 3620 3860 3920 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 10.4 7.1 8.1 9.1 6.5 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron • o 15 pg/L Lead 2.7 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 2770 250000 pg/L Sulfate 3740 4230 3400 5070 5420 6860 2000 pg/L Tin 5.8 500000 pg/L Total Dissolved Solids 191000 187000 193000 175000 172000 168000 0.3 pg/L Vanadium 1000 pg/L Zinc 10.5 MW-4R 3 pg/L 1,4-Dioxane (p-Dioxane) 0.1 pg/L 4,4'-DDT 11111111111MI 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 286000 222000 224000 203000 174000 64300 1 10 pg/L Arsenic 700 pg/L Barium 305 264 296 375 400 407 1 pg/L Benzene 0.42 0.28 0.27 1000 pg/L Butylbenzylphthalate 2 pg/L Cadmium 250000 pg/L Chloride 50500 29700 36500 33700 34500 33200 3 pg/L Chloromethane 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 4.3 5.9 0.019 pg/L delta-BHC . 42 pg/L Endosulfan II 0.12 300 pg/L Iron 126 89.5 158 1451 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 7.2 5.3 0.12 1.2 0.84 31800 27200 96300 197 274 98000 0.88 20.1 33.3 155000 237 180000 0.67 31.61 36.11 21.91 22.2 301 0 0.6 4 314 0.82 0.45 26.1 1 55.9 334 1.3 5.4 4.8 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND W-S GW Revised.xlsb A2 100 pg/L NS pg/L 500 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L 0.7 pg/L NE pg/L 0.2 pg/L 600 pg/L 500000 pg/L 3 pg/L 2000 pg/L 0.3 pg/L 88 pg/L 0.03 pg/L 500 pg/L 1000 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 200 pg/L 4 pg/L 3 pg/L 2 pg/L 700 pg/L 250000 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.005 pg/L 0.05 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L 2000 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 0.1 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 1000 pg/L 2 pg/L 250000 pg/L 3 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.019 pg/L 42 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location Row Labels Nickel Nitrogen, Ammonia o-Xylene Selenium Silver 0.58 1.2 0.93 Sodium Sulfate Sulfide Tetrachloroethene Tetrahydrofuran Thallium Toluene Total Dissolved Solids Trichloroethene T ri ch lorofl uo ro metha ne Vanadium Vinyl acetate Vinyl chloride Xylenes (Total) Zinc MW-3R Acetone Alkalinity, Total as CaCO3 Arsenic 7.4 8.4 Barium 252 231 293 273 310 230 290 300 300 340 270 200 220 13 370 400 Benzo(g,h,i)perylene Beryllium b is(2-Ethyl hexyl )p htha late Cadmium Carbon Disulfide 3.3 Chloride Chromium 0.63 2.3 3.7 2.3 Cobalt Copper Cyanide Di benz(a, h)anthracene I ndeno(1,2,3-cd)pyrene Iron Lead 14 Manganese Mercury Methylene Chloride Nickel Selenium 11.8 4.9 18.1 Silver 0.29 1.5 0.87 Sodium Sulfate Tin Total Dissolved Solids Vanadium Zinc MW-4R 1,4-Dioxane (p-Dioxane) 4,4'-DDT Acetone Alkalinity, Total as CaCO3 Arsenic 9.2 Barium 58.3 263 172 287 200 220 220 180 150 140 380 97 94 86 61 Benzene B utylbenzylp htha late Cadmium Chloride Chloromethane Chromium 1.2 0.58 0.4 2.6 5.5 5 Cobalt Copper Cyanide delta-BHC Endosulfan II Iron Lead 5.3 6 Manganese Mercury Methylene Chloride Nickel Highlighted cells are at or above the current standard. Blank cells indicate either INS or ND. W-S GW Revised.xlsb A2 100 pg/L NS pg/L 500 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L 0.7 pg/L NE pg/L 0.2 pg/L 600 pg/L 500000 pg/L 3 pg/L 2000 pg/L 0.3 pg/L 88 pg/L 0.03 pg/L 500 pg/L 1000 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 200 pg/L 4 pg/L 3 pg/L 2 pg/L 700 pg/L 250000 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.005 pg/L 0.05 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L 2000 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 0.1 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 1000 pg/L 2 pg/L 250000 pg/L 3 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.019 pg/L 42 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location -. Nickel Nitrogen, Ammonia o-Xylene Selenium Silver 6 Sodium Sulfate Sulfide Tetrachloroethene Tetrahydrofuran Thallium Toluene Total Dissolved Solids Trichloroethene T ri ch lorofl uo ro metha ne Vanadium Vinyl acetate Vinyl chloride Xylenes (Total) Zinc MW-3R Acetone Alkalinity, Total as CaCO3 Arsenic 5.9 Barium 300 52 Ww E. 1 620 Wloffi W011MVA111 Benzo(g,h,i)perylene Beryllium b is(2-Ethyl hexyl )p htha late Cadmium Carbon Disulfide Chloride Chromium 9 Cobalt Copper Cyanide Di benz(a, h)anthracene I ndeno(1,2,3-cd)pyrene Iron Lead Manganese Mercury 0.2 0.7 Methylene Chloride Nickel Selenium Silver Sodium Sulfate Tin Total Dissolved Solids Vanadium Zinc MW-4R 1,4-Dioxane (p-Dioxane) 4,4'-DDT Acetone Alkalinity, Total as CaCO3 Arsenic 7.5 Barium 350 570 650 280 595 :. Benzene B utylbenzylp htha late Cadmium Chloride Chloromethane Chromium Cobalt Copper Cyanide delta-BHC Endosulfan II Iron Lead 8.1 9.5 12 Manganese Mercury 0.36 0.21 0.3 Methylene Chloride Nickel Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L NE pg/L 0.2 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 4 pg/L 3 pg/L 2 pg/L 700 pg/L 250000 pg/L 3 pg/L 10 pg/L 1 pg/L 70 pg/L 300 pg/L 15 pg/L 500 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 500 pg/L 20 pg/L NE pg/L 250000 pg/L 600 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 10 pg/L 700 pg/L 10 pg/L 15 pg/L 1 pg/L 200 pg/L 6 pg/L 3 pg/L 0.1 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 4 pg/L 0.019 pg/L 700 pg/L 250000 pg/L 3000 pg/L 3 pg/L 10 pg/L 70 pg/L 70 pg/L 1000 pg/L 0.002 pg/L 40 pg/L 0.004 pg/L 300 pg/L 15 pg/L 500 pg/L 50 pg/L 1 pg/L 3 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Value Column Historical Labels detections by well location Row Labels Selenium Silver Sodium 73800 62300 71200 42600 17800 65500 42100 71000 14500 23800 23000 Sulfate 162000 122000 163000 104000 50300 179000 125000 193000 48700 70300 72700 Sulfide 105 Tetrahydrofuran 11.4 8.6 11.4 9.3 13.6 3.5 7 5.8 Thallium 0.029 Total Dissolved Solids 167000 496000 241000 161000 304000 :. Vanadium Zinc 5.4 5.9 5.2 �19.09 5.8 8.6 8.4 17.8 5.9 7.5 MW-5R Acetone 18.4 Alkalinity, Total as CaCO3 35700 34300 29200 35600 33600 33500 32300 32700 30800 32300 28600 Arsenic Barium 56.5 58.3 55.8 59.8 52.5 53.2 57.1 55.9 55.9 92.7 54 Benzene 0.28 Beryllium 0.2 bi s (2-Ethylhexyl) phtha late Cadmium Carbon Disulfide Chloride 14500 14800 15600 15100 15200 16200 15100 16400 15300 16200 15700 Chloromethane Chromium 6.8 5.6 5.4 5.5 5.3 owalm 4.6 5.8 5.1 4.8 Cobalt Cyanide 7.2 4.4 Iron 211 218 63.5 88.2 37.9 68.4 87.8 .40 113 Lead m&p-Xylene 0.73 Manganese 3 4.2 Mercury 0.69 Methylene Chloride Nickel 1.6 o-Xylene 0.45 Silver Sodium 17100 14100 13000 14600 12800 13500 13900 14200 13100 11300 13100 Sulfate 7770 8380 8620 8090 8220 7830 7740 8450 7620 7430 8000 Toluene 1.7 Total Dissolved Solids 163000 169000 175000 156000 164000 144000 156000 145000 154000 104000 166000 Vanadium Zinc 7.3 MW-6R Arsenic Barium Chromium Lead Mercury MW-7 1,1,1-Trichloroethane 1,1-Dichloroethane 0.9 1.3 1.3 1.3 1.1 1.6 1.4 1.3 1.5 1.2 0.91 1.1 1,4-Dioxane (p-Dioxane) 2.2 1.8 2 4,4'-DDD Acetone 15.7 Alkalinity, Total as CaCO3 71600 82700 54200 78500 75900 80400 85000 80100 71700 67300 64100 Arsenic Barium 136 163 168 161 158 152 163 140 129 140 122 Benzene 0.48 0.6 0.68 0.37 0.41 0.39 0.38 0.43 0.42 0.26 0.29 Beryllium 0.78 0.61 0.62 2.1 0.58 beta-BHC Carbon Disulfide Chloride 5910 7500 6470 6580 6490 7390 5290 4820 4430 6050 4340 Chloroethane 0.85 Chloromethane 0.13 Chromium cis-1,2-Dichloroethene 0.91 1.4 1.5 0.86 0.85 1.1 1.1 1.1 1.1 0.77 0.8 0.73 Cyanide Dichlorodifluoromethane 0.52 0.62 1 Dieldrin Endosulfan 1 0.15 Heptachlor epoxide Iron 21.5 35 25 25.2 Lead m&p-Xylene 1 0.721 0.93 1 1.1 1.7 1.6 1.4 1.2 2.2 1.8 0.84 1.5 Manganese 44 43.8 43 35.6 28.8 33.6 27.1 Mercury 1 Methylene Chloride 1.7 2.1 Highlighted cells are at or above the current standard. Blank cells indicate either INS or ND. W-S GW Revised.xlsb A2 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L NE pg/L 0.2 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 4 pg/L 3 pg/L 2 pg/L 700 pg/L 250000 pg/L 3 pg/L 10 pg/L 1 pg/L 70 pg/L 300 pg/L 15 pg/L 500 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 500 pg/L 20 pg/L NE pg/L 250000 pg/L 600 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 10 pg/L 700 pg/L 10 pg/L 15 pg/L 1 pg/L 200 pg/L 6 pg/L 3 pg/L 0.1 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 4 pg/L 0.019 pg/L 700 pg/L 250000 pg/L 3000 pg/L 3 pg/L 10 pg/L 70 pg/L 70 pg/L 1000 pg/L 0.002 pg/L 40 pg/L 0.004 pg/L 300 pg/L 15 pg/L 500 pg/L 50 pg/L 1 pg/L 3 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location Row Labels Selenium 11.5 Silver 0. Sodium 55400 39700 42600 42600 43600 40400 35300 Sulfate 143000 85200 113000 97600 73600 98700 61800 Sulfide Tetrahydrofuran 15.9 11.8 11.7 8.5 13.5 8.8 Thallium Total Dissolved Solids . • 445000 496000 413000 435000 374000 345000 Vanadium Zinc 7.2 13.6 MW-5R Acetone Alkalinity, Total as CaCO3 24000 31900 31700 34800 31200 134000 32800 Arsenic Barium 58.2 54.4 53.9 57.7 53.4 57.5 85.2 6 38 2.4 3 4.2 .7 53 54.3 66.8 7.6 5.8 5 8.6 i7 1 0.161 1 0.46 82 3.8 3.4 04 100 99.3 104 12.5 0.55 0.65 71 1.4 Highlighted cells are at or above the current standard. Blank cells indicate either INS or ND. W-S GW Revised.xlsb i7 1 0.161 1 0.46 82 3.8 3.4 04 100 99.3 104 12.5 0.55 0.65 71 1.4 Highlighted cells are at or above the current standard. Blank cells indicate either INS or ND. W-S GW Revised.xlsb 71 1.4 Highlighted cells are at or above the current standard. Blank cells indicate either INS or ND. W-S GW Revised.xlsb A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-5R 6000 pg/L Acetone 2.6 0.94 NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 52.6 56.1 57.5 70.6 5 1 pg/L Benzene 4 pg/L Beryllium 3 pg/L bis(2-Ethylhexyl)phthalate 2 pg/L Cadmium 700 pg/L Carbon Disulfide 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 5.2 5.3 5.6 8.4 6: 1 pg/L Cobalt 70 pg/L Cyanide 300 pg/L Iron 15 pg/L Lead 500 pg/L m&p-Xylene 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 500 pg/L o-Xylene 20 pg/L Silver 0.28 0.78 0.56 NE pg/L Sodium 250000 pg/L Sulfate 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-6R 10 pg/L Arsenic 700 pg/L Barium 10 pg/L Chromium 15 pg/L Lead 1 pg/L Mercury MW-7 200 pg/L 1,1,1-Trichloroethane 6 pg/L 1,1-Dichloroethane 3 pg/L 1,4-Dioxane (p-Dioxane) 0.1 pg/L 4,4'-DDD 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 86.9 99 95.7 101 8 1 pg/L Benzene 4 pg/L Beryllium 0.019 pg/L beta-BHC 700 pg/L Carbon Disulfide 250000 pg/L Chloride 3000 pg/L Chloroethane 3 pg/L Chloromethane 10 pg/L Chromium 0.91 7.3 70 pg/L cis-1,2-Dichloroethene 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 0.002 pg/L Dieldrin 40 pg/L Endosulfan 1 0.004 pg/L Heptachlor epoxide 300 pg/L Iron 15 pg/L Lead 500 pg/L m&p-Xylene 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride Highlighted cells are at or above the current standard. Blank cells indicate either INS or ND. W-S GW Revised.xlsb 58 6.2 76 5.1 80 5 76 7.3 65 8.7 72 65 7.4 150 61 9.5 5.1 28 25 24 41 1F 2.2 2.4 3.2 7 8.6 11801111111 130 21 5.3 6 131 7. 4.1 A2 Facility Permit 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-5R 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 1 pg/L Benzene 4 pg/L Beryllium 3 pg/L bis(2-Ethylhexyl)phthalate 2 pg/L Cadmium 700 pg/L Carbon Disulfide 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 1 pg/L Cobalt 70 pg/L Cyanide 300 pg/L Iron 15 pg/L Lead 500 pg/L m&p-Xylene 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 500 pg/L o-Xylene 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 0.3 pg/L Vanadium 1000 pg/L Zinc MW-6R 10 pg/L Arsenic 700 pg/L Barium 10 pg/L Chromium 15 pg/L Lead 1 pg/L Mercury MW-7 200 pg/L 1,1,1-Trichloroethane 6 pg/L 1,1-Dichloroethane 3 pg/L 1,4-Dioxane (p-Dioxane) 0.1 pg/L 4,4'-DDD 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 1 pg/L Benzene 4 pg/L Beryllium 0.019 pg/L beta-BHC 700 pg/L Carbon Disulfide 250000 pg/L Chloride 3000 pg/L Chloroethane 3 pg/L Chloromethane 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 0.002 pg/L Dieldrin 40 pg/L Endosulfan 1 0.004 pg/L Heptachlor epoxide 300 pg/L Iron 15 pg/L Lead 500 pg/L m&p-Xylene 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 41 Old Salisbury Road Landfill (C&D) MUM o o M rn iremrMtrordn"OVIMM• rn rn Co rn t- rn rn co rn • to rn � p z � p z T (6 2 U O > (6 2 U O � 820 1000 • 29 38 96 170 16 70 43 96 on on 16 29 69 31 20 19 10 �� 21 1400 12 18 1.4 .� 12 .� 33 20 .� 14 •� 10 t.� •� 960 1300 1200 1800 750 970 1930 62 190 350 430 410 180 21 28 30 36 38 53 23 17 10milli ■ 1.4 _ Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 100 pg/L 500 pg/L 20 pg/L NE pg/L 250000 pg/L 0.7 pg/L NE pg/L 500000 pg/L 3 pg/L 2000 pg/L 500 pg/L 1000 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 4 pg/L 250000 pg/L 10 pg/L 70 pg/L 100 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 20 pg/L NE pg/L 250000 pg/L 500000 pg/L 1000 pg/L NE pg/L 10 pg/L 700 pg/L 4 pg/L 3 pg/L 250000 pg/L 10 pg/L 70 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 20 pg/L NE pg/L 250000 pg/L 500000 pg/L 2000 pg/L 1000 pg/L 3 pg/L 40 pg/L NE pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 4 pg/L 2 pg/L 700 pg/L 250000 pg/L 10 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 40 pg/L 600 pg/L 0.008 pg/L 0.004 pg/L 300 pg/L 15 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Value Column CD Historical Labels detections by well location Row Labels Nickel 1.3 o-Xylene 0.46 0.54 0.68 0.59 0.65 0.62 0.68 0.46 0.63 0.47 0.27 0.4 Silver Sodium 16200 18400 17500 17700 16600 15300 17800 16200 16400 15700 16300 Sulfate 10400 13000 12800 12700 14200 13400 6720 3800 2930 10100 1850 Tetrachloroethene 0.48 Tetrahydrofuran 70.5 77.9 80.4 50.5 24.9 20.1 32 21.7 13.5 17.7 14.1 Total Dissolved Solids 165000 168000 192000 171000 181000 175000 175000 153000 137000 78000 145000 Trichloroethene 0.58 Trichlorofluoromethane 5.6 4 2 1.2 1.2 1.6 1.6 0.91 1.5 0.92 1.4 0.79 Xylenes (Total) Zinc 5 6 9 5 8.9 5.7 5.2 6.8 MW-8 Acetone 15.8 Alkalinity, Total as CaCO3 25000 25300 26600 24200 27000 28200 20800 25800 24800 23200 20000 Arsenic Barium 52.9 50.9 47.8 36 41.2 46.5 42.9 44 38.3 34.4 30 Beryllium 0.41 Chloride 4090 3860 4290 3110 3660 3860 3060 2670 1960 2040 1960 Chromium 5.6 4 3.5 2.6 4.9 4.1 Cyanide 9.9 4.3 5.1 Di-n-octylphthalate 5.6 Iron 125 27 42.4 39.3 37.6 48.6 54 Lead Manganese 4.2 3.3 4 4.4 3.6 3 2.7 2.9 3.3 3.4 Mercury Methylene Chloride 1.1 Silver Sodium 12900 10800 9620 8300 8810 9860 9240 9700 8280 7940 6940 Sulfate 9360 7860 6560 1060 2980 4740 2700 4090 1630 1350 1860 Total Dissolved Solids 93000 78000 170000 68000 75000 82000 67000 67000 87000 79000 61000 Zinc 5.3 7.1 MW-9 Alkalinity, Total as CaCO3 33900 39000 29700 33500 31800 27900 25400 23300 21200 23400 18900 Arsenic Barium 238 203 217 215 193 196 207 195 197 186 182 Beryllium 0.28 bi s (2-Ethylhexyl) phtha late Chloride 6370 4190 6830 5330 4830 4430 4610 4360 6850 4710 4290 Chromium 4.2 7.2 Cyanide 4.7 Dichlorodifluoromethane 1.1 0.9 1.4 0.99 1.2 1.7 1.2 1.5 0.88 0.76 Iron 43.5 91.4 148 250 35.3 166 149 128 Lead Manganese 5.1 5.3 7.1 10.7 4.2 10.6 4.6 8.5 6.3 4 3.5 Silver Sodium 16200 23400 14100 15700 14300 14900 15400 15700 14200 14500 14500 Sulfate 3610 960 3440 1110 2030 Total Dissolved Solids 130000 157000 190000 139000 133000 136000 141000 135000 103000 142000 134000 Trichlorofluoromethane 1.3 0.86 1.7 1.3 1.3 1.4 1.2 1.4 1 1.3 1.1 0.98 Zinc 5.1 MW-10 1,4-Dioxane (p-Dioxane) 2-Hexanone 0.72 0.69 0.96 4-Methyl-2-pentanone (MIBK) 0.65 1.7 1.1 2.8 2.5 2.6 5.6 Acetone 16.4 13.7 12.1 22.5 14.1 11.8 Alkalinity, Total as CaCO3 635000 726000 506000 652000 506000 520000 446000 626000 29000 48200 47300 Arsenic 2.6 5.2 Barium 66 111 65.6 83.1 94.7 106 221 148 292 241 660 Benzene 0.56 0.78 0.33 0.55 0.55 0.57 0.52 0.83 0.46 Beryllium 3.2 1.9 2.8 Cadmium 0.62 Carbon Disulfide 2.1 2 5.2 Chloride 63100 71800 65100 88500 158000 163000 :��� 202000 9640 47400 51800 Chromium 4 5.6 4.1 4.6 4.2 6.4 9.1 3.5 6.7 cis-1,2-Dichloroethene 0.23 0.27 0.23 0.2 0.33 Cobalt Copper 3.1 16.4 6.3 3.8 Cyanide 4.3 4.8 5.4 4.1 9.8 Endosulfan 1 0.17 Ethylbenzene 0.41 0.53 0.55 0.4 1 Heptachlor r' Heptachlor epoxide r' Iron o •I EWAj M� 1 .11 WI I Lead 3.7 2.6 3.9 4.1 2.6 8.5 11.6 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 100 Ng/L 500 Ng/L 20 Ng/L NE Ng/L 250000 Ng/L 0.7 Ng/L NE Ng/L 500000 Ng/L 3 Ng/L 2000 Ng/L 500 Ng/L 1000 Ng/L 6000 Ng/L NE Ng/L 10 Ng/L 700 Ng/L 4 Ng/L 250000 Ng/L 10 Ng/L 70 Ng/L 100 Ng/L 300 Ng/L 15 Ng/L 50 Ng/L 1 Ng/L 3 Ng/L 20 Ng/L NE Ng/L 250000 Ng/L 500000 Ng/L 1000 Ng/L NE Ng/L 10 Ng/L 700 Ng/L 4 Ng/L 3 Ng/L 250000 Ng/L 10 Ng/L 70 Ng/L 1000 Ng/L 300 Ng/L 15 Ng/L 50 Ng/L 20 Ng/L NE Ng/L 250000 Ng/L 500000 Ng/L 2000 Ng/L 1000 Ng/L 3 Ng/L 40 Ng/L NE Ng/L 6000 Ng/L NE Ng/L 10 Ng/L 700 Ng/L 1 Ng/L 4 Ng/L 2 Ng/L 700 Ng/L 250000 Ng/L 10 Ng/L 70 Ng/L 1 Ng/L 1000 Ng/L 70 Ng/L 40 Ng/L 600 Ng/L 0.008 Ng/L 0.004 Ng/L 300 Ng/L 15 Ng/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well to Row Labels Nickel o-Xylene 0.36 0.27 Silver Sodium 16600 14200 13000 14300 13900 13700 Sulfate 1360 2090 Tetrachloroethene Tetrahydrofuran 8.8 5.2 13.7 24.2 26 18.9 Total Dissolved Solids 138000 126000 116000 108000 111000 109000 Trichloroethene Trichlorofluoromethane 1.2 0.62 0.47 0.25 0.29 Xylenes (Total) 1.2 0.79 Zinc MW-8 Acetone Alkalinity, Total as CaCO3 22800 21300 19700 22800 19500 20100 Arsenic 2.6 Barium 38 30.7 25.4 28.5 26.9 27.5 Beryllium Chloride 1350 1800 1510 2070 1860 Chromium Cyanide Di-n-octylphthalate Iron 136 61.5 60.8 57.8 Lead Manganese 19.9 6.8 Mercury Methylene Chloride Silver Sodium 7810 6160 5580 6120 6980 6250 Sulfate 2100 Total Dissolved Solids 64000 50000 61000 51000 58000 52000 Zinc 15.2 MW-9 Alkalinity, Total as CaCO3 18300 18300 18400 21700 17200 20100 Arsenic 3.5 Barium 193 168 170 174 142 142 Beryllium bi s (2-Ethylhexyl) phth a late Chloride 3610 3610 3950 4300 3560 Chromium Cyanide Dichlorodifluoromethane 0.28 0.28 Iron 55.9 136 Lead Manganese 7.6 6.9 16.6 Silver Sodium 14600 12400 13500 12900 13100 12600 Sulfate 2100 3200 Total Dissolved Solids 141000 107000 124000 100000 118000 123000 Trichlorofluoromethane 0.96 0.47 0.69 0.36 0.49 Zinc 5.3 MW-10 1,4-Dioxane (p-Dioxane) 2-Hexanone 4-Methyl-2-pentanone (MIE 2.2 Acetone Alkalinity, Total as CaCO3 42200 31400 26700 32100 25500 413000 Arsenic Barium 262 132 112 115 101 96.5 Benzene 0.44 Beryllium 1.4 Cadmium Carbon Disulfide Chloride 2220 1820 1790 2040 1800 Chromium cis-1,2-Dichloroethene 0.35 Cobalt Copper Cyanide Endosulfan I Ethylbenzene 0.73 Heptachlor Heptachlor epoxide Iron . 1 84.3 92.8 218 55.1 Lead 4.1 cation 0.39 0.84 0.23 0.56 12000 124000 0.34 0.48 3.8 19600 24.4 27.3 26.8 28.8 0.96 0.62 1.4 151 7 0.1 5410 81000 45.4 17400 141 153 157 134 0.43 0.27 11900 128000 0.42 0.26 21700 91.3 80.7 38.9 46.6 0.63 27.2 0.16 128 0.32 39.1 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location 100 pg/L Nickel 500 pg/L o-Xylene 20 pg/L Silver 0.42 0.96 0.66 NE pg/L Sodium 250000 pg/L Sulfate 0.7 pg/L Tetrachloroethene NE pg/L Tetrahydrofuran 500000 pg/L Total Dissolved Solids 3 pg/L Trichloroethene 2000 pg/L Trichlorofluoromethane 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-8 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 25 32.8 24 26.6 31 4 pg/L Beryllium 250000 pg/L Chloride 10 pg/L Chromium 0.78 0.97 0.42 70 pg/L Cyanide 100 pg/L Di-n-octylphthalate 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 0.1 3 pg/L Methylene Chloride 20 pg/L Silver 0.15 0.13 0.16 NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 1000 pg/L Zinc MW-9 NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 173 124 124 117 141 4 pg/L Beryllium 3 pg/L bis(2-Ethylhexyl)phthalate 250000 pg/L Chloride 10 pg/L Chromium 7.6 0.47 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 20 pg/L Silver 0.18 0.36 0.22 0.32 NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 1000 pg/L Zinc MW-10 3 pg/L 1,4-Dioxane (p-Dioxane) 40 pg/L 2-Hexanone NE pg/L 4-Methyl-2-pentanone (MI 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 38.9 41.9 42 40.8 5; 1 pg/L Benzene 4 pg/L Beryllium 2 pg/L Cadmium 700 pg/L Carbon Disulfide 250000 pg/L Chloride 10 pg/L Chromium 0.65 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 40 pg/L Endosulfan 1 600 pg/L Ethylbenzene 0.008 pg/L Heptachlor 0.004 pg/L Heptachlor epoxide 300 pg/L Iron 15 pg/L Lead Highlighted cells are at or above the current standard. Blank cells indicate either INS or ND. W-S GW Revised.xlsb 29 140 71 1001 10C 6.8 52 77 48 3.2 3.8 2 6.7 A2 Facility Permit 100 pg/L Nickel 500 pg/L o-Xylene 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 0.7 pg/L Tetrachloroethene NE pg/L Tetrahydrofuran 500000 pg/L Total Dissolved Solids 3 pg/L Trichloroethene 2000 pg/L Trichlorofluoromethane 500 pg/L Xylenes (Total) 1000 pg/L Zinc MW-8 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 4 pg/L Beryllium 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L Cyanide 100 pg/L Di-n-octylphthalate 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 1000 pg/L Zinc MW-9 NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 4 pg/L Beryllium 3 pg/L bis(2-Ethylhexyl)phthalate 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 1000 pg/L Zinc 3 pg/L 1,4-Dioxane (p-Dioxane) 40 pg/L 2-Hexanone NE pg/L 4-Methyl-2-pentanone (MIE 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 1 pg/L Benzene 4 pg/L Beryllium 2 pg/L Cadmium 700 pg/L Carbon Disulfide 250000 pg/L Chloride 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 40 pg/L Endosulfan I 600 pg/L Ethylbenzene 0.008 pg/L Heptachlor 0.004 pg/L Heptachlor epoxide 300 pg/L Iron 15 pg/L Lead Old Salisbury Road Landfill (C&D) Historical detections by well location Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 500 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 500 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L NE pg/L 0.2 pg/L 2000 pg/L 600 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 500 pg/L 1000 pg/L 0.1 pg/L 6000 pg/L NE pg/L 700 pg/L 200 pg/L 4 pg/L 250000 pg/L 3 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 500 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L NE pg/L 0.2 pg/L 600 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 200 pg/L 4 pg/L 250000 pg/L 3 pg/L 10 pg/L 70 pg/L 1 pg/L 70 pg/L 1000 pg/L 100 pg/L 0.05 pg/L 300 pg/L 50 pg/L 3 pg/L 100 pg/L 20 pg/L NE pg/L 250000 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Value Column Historical Labels detections by well location -.w Lab m&p-Xylene 0.68 1.3 1.1 1.2 2.1 0.68 1.2 Manganese •1 Mercury 0.12 0.12 0.29 Methylene Chloride 2.8 1.2 Nickel 7.9 11 7.2 11.1 8.5 7.6 6.9 10.7 4.7 3.9 5.9 o-Xylene 0.34 0.84 0.28 0.53 0.78 1.1 0.97 1 2.1 0.43 0.85 Selenium 12 Silver Sodium 148000 138000 136000 151000 157000 138000 123000 184000 10300 19800 14100 Sulfate 235000 64100 002ol 15800 63600 8770 Sulfide 242 192 347 240 127 Tetrahydrofuran 130 141 113 169 192 135 131 182 237 6.1 120 145 Thallium 0.043 Tin 7.1 3.1 8.5 Toluene 0.26 0.35 0.27 0.63 Total Dissolved Solids 1. NT4 M1. 311000 403000 279000 1. 1 .Main 0118LIM Main 1. Trich to roflu orom etha ne Vanadium Xylenes (Total) 1.1 Zinc 5.4 5.1 34 27.2 21.2 MW-11 4,4'-DDT Acetone 21.1 Alkalinity, Total as CaCO3 127000 102000 154000 161000 130000 130000 135000 107000 104000 127000 132000 Barium 98.1 91.6 100 95.8 82.8 89.8 102 93.1 103 97.2 93.7 Benzo(g,h,i)perylene Beryllium 0.23 Chloride 11000 11400 12300 11800 12500 13000 13500 14500 14500 14900 14400 Chloromethane 0.23 Chromium Cobalt Copper 2.8 Cyanide 41 4.4 1 4.1 4.2 Iron �� . �� •-�� .10 Lead 2.9 Manganese e WON •e Elff.wel I I ••� Mercury Methylene Chloride 1.4 o-Xylene 0.27 Selenium 5.6 Silver Sodium 12400 13500 12800 13600 12000 12300 11700 12000 11200 12000 9460 Sulfate 22800 23900 22300 20700 15300 16200 14100 17100 15200 19100 15300 Sulfide 56.8 53.8 Tetrahydrofuran 4.5 Thallium Toluene 1 Total Dissolved Solids 230000 240000 236000 237000 232000 218000 226000 189000 236000 281000 239000 Vanadium Zinc 4.2 777 MW-12 2.6 I 1 1 1,4-Dioxane (p-Dioxane) Acetone 12.1 Alkalinity, Total as CaCO3 333000 150000 176000 117000 65800 73800 64500 72900 55900 41000 19200 Arsenic Barium 224 146 200 132 82.8 84.2 113 144 190 95.7 60.9 Benzene 0.29 0.25 0.33 Benzo(g,h,i)perylene Beryllium 0.88 Chloride 29500 17600 34000 14400 11100 10400 19700 23300 26000 9000 8070 Chloromethane Chromium cis-1,2-Dichloroethene 0.4 0.23 Cobalt Cyanide 4.8 5.3 Dichlorodifluoromethane 0.23 Di-n-octylphthalate 5.6 Indeno(1,2, 3-cd )pyrene Iron •L-111 NEW 175 125 274 Manganese ME wine OWN 49.6 9.7 Methylene Chloride 2 2 Nickel 10.6 4.3 6.2 3.3 4.4 6.2 5.5 3.2 Silver Sodium 28600 17400 20700 17600 13400 13200 1620C 19200 19200 13700 11200 Sulfate 227000 99500 149000 91700 64300 62400 86100 129000 169000 70800 73600 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 500 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 500 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L NE pg/L 0.2 pg/L 2000 pg/L 600 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 500 pg/L 1000 pg/L 0.1 pg/L 6000 pg/L NE pg/L 700 pg/L 200 pg/L 4 pg/L 250000 pg/L 3 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 500 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L NE pg/L 0.2 pg/L 600 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 200 pg/L 4 pg/L 250000 pg/L 3 pg/L 10 pg/L 70 pg/L 1 pg/L 70 pg/L 1000 pg/L 100 pg/L 0.05 pg/L 300 pg/L 50 pg/L 3 pg/L 100 pg/L 20 pg/L NE pg/L 250000 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location -.w Lab m&p-Xylene 1.1 CD Manganese 10.9 7.9 5.1 6.8 Mercury 0.33 0.51 Methylene Chloride 7 Nickel o-Xylene 0.65 Selenium Silver 0.12 0.19 Sodium 6860 5280 Sulfate Sulfide 260 Tetrahydrofuran 106 18.6 5 Thallium Tin Toluene Total Dissolved Solids 86000 63000 66000 46000 63000 49000 89000 Trichlorofluoromethane 0.2 0.33 0.38 0.49 0.68 0.52 Vanadium Xylenes (Total) Zinc 6.2 MW-11 4,4'-DDT 0.05 Acetone Alkalinity, Total as CaCO3 143000 175000 161000 189000 153000 120000 122000 Barium 96.8 94.3 87.8 87 76.8 70.3 57.5 56.2 48.1 37.6 31.8 Benzo(g,h,i)perylene 1.3 Beryllium Chloride 15000 12400 14000 14200 12900 10800 8480 Chloromethane Chromium Cobalt Copper Cyanide Iron 110 [111MISY11111 111184*11111110 Lead 3.6 Manganese I I •.� :•1 � WON EKFWII Mercury Methylene Chloride o-Xylene Selenium Silver 1.2 0.48 0.5 Sodium 10000 8490 9070 8290 8770 7460 6480 Sulfate 12800 10700 10400 11000 10400 9700 7590 Sulfide 130 Tetrahydrofuran 4.4 12.1 Thallium Toluene Total Dissolved Solids 228000 207000 236000 228000 220000 161000 165000 Vanadium Zinc 92 MW-12 1,4-Dioxane (p-Dioxane) Acetone Alkalinity, Total as CaCO3 40500 45500 39300 29600 40200 37200 40200 Arsenic 2.7 Barium 59.2 61.1 47.6 50.1 50.5 46.9 60.1 39.1 44.9 40.6 38 Benzene Benzo(g,h,i)perylene 1.2 Beryllium Chloride 8240 6180 6230 5820 4900 8200 8030 Chloromethane 0.21 Chromium 2.6 1.1 2.4 cis-1,2-Dichloroethene Cobalt Cyanide D ich to rod iflu orom etha ne Di-n-octylphthalate Indeno(1,2, 3-cd )pyrene Iron 253 Manganese 14.6 13.2 33.6 15.7 OWN Methylene Chloride Nickel 4.1 Silver 0.7 0.2 0.39 Sodium 12800 11000 10500 11100 11000 11600 9980 Sulfate 328001 480001 274001 518001 24200 20500 15300 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 500 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 500 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L NE pg/L 0.2 pg/L 2000 pg/L 600 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 500 pg/L 1000 pg/L 0.1 pg/L 6000 pg/L NE pg/L 700 pg/L 200 pg/L 4 pg/L 250000 pg/L 3 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 500 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L NE pg/L 0.2 pg/L 600 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 1 pg/L 200 pg/L 4 pg/L 250000 pg/L 3 pg/L 10 pg/L 70 pg/L 1 pg/L 70 pg/L 1000 pg/L 100 pg/L 0.05 pg/L 300 pg/L 50 pg/L 3 pg/L 100 pg/L 20 pg/L NE pg/L 250000 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Row Labels m&p-Xylene Manganese Mercury Methylene Chloride Nickel o-Xylene Selenium Silver Sodium Sulfate Sulfide Tetrahydrofuran Thallium Tin Toluene Total Dissolved Solids T ri ch lorofluo ro metha ne Vanadium Xylenes (Total) Zinc MW-11 M CD Historical co (D co CD detections I-- (D CD w (D by well CD location M (D 0.2 -W 7 6.2 �' ce) CD C0 N CD C14 (D 4,4'-DDT Acetone Alkalinity, Total as CaCO3 Barium 28.4 28.6 29.2 23.1 25 24 26 27 24 28 47 Benzo(g,h,i)perylene Beryllium Chloride Chloromethane Chromium 3.9 3.3 Cobalt Copper Cyanide Iron Lead Manganese Mercury Methylene Chloride o-Xylene Selenium 8.7 Silver 0.79 0.41 0.39 Sodium Sulfate Sulfide Tetrahydrofuran Thallium Toluene Total Dissolved Solids Vanadium Zinc MW-12 1,4-Dioxane (p-Dioxane) Acetone Alkalinity, Total as CaCO3 Arsenic Barium 34.5 57.9 60.5 47.3 31 66 55 77 50 77 74 Benzene Benzo(g,h,i)perylene Beryllium Chloride Chloromethane Chromium 2 1.8 4 2.1 cis-1,2-Dichloroethene Cobalt Cyanide Dichlorod ifluoromethane Di-n-octylphthalate I ndeno(1,2,3-cd)pyrene Iron Manganese Methylene Chloride Nickel Silver 0.37 0.15 0.26 Sodium Sulfate Highlighted cells are at or above the current standard. Blank cells indicate either INS or ND. W-S GW Revised.xlsb A2 NE pg/L 0.2 pg/L 600 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 350 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 0.005 pg/L 0.05 pg/L 200 pg/L 4 pg/L 250000 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.005 pg/L 0.05 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 100 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L NE pg/L 2000 pg/L 600 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 4 pg/L 3 pg/L 250000 pg/L 3 pg/L 10 pg/L 1000 pg/L 70 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L NE pg/L 250000 pg/L 0.7 pg/L 0.2 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Value Column CD Historical Labels detections by well location 10 -. Tetrahydrofuran 5.9 11.4 26.8 12.4 Thallium 0.021 Toluene 0.74 Total Dissolved Solids 369000 5W 1. 301000 218000 219000 288000 286000 382000 234000 163000 Trichlorofluoromethane 0.81 1 0.89 1.4 0.52 1 2.8 1.4 0.82 0.22 Vanadium Zinc MW-13 1,1-Dichloroethene Acetone 17.3 Alkalinity, Total as CaCO3 66400 58500 52800 52800 47200 44600 42400 42300 41000 37100 36900 Arsenic 2.6 Barium 196 156 138 124 114 116 120 91.6 210 71.5 89.3 Benzo(a)pyrene Be nzo(b)flu ora nthe ne Benzo(g,h,i)perylene Beryllium 0.72 0.78 0.6 0.69 0.63 0.52 2.2 0.68 0.66 Chloride 8400 6310 6290 5120 4790 4770 4310 4100 4590 3270 3760 Chromium 3.8 2.9 Cobalt Copper 8.5 Cyanide 5 Dibenz(a,h)anthracene Indeno(1,2, 3-cd )pyrene Iron 80.8 87.9 42.3 71.8 108 193 58 of Lead 8 2.9 Manganese 27.4 6.9 5.2 9.8 7.4 17.9 9.7 26.7 41.2 Mercury 0.52 Nickel 1.5 6.4 Silver Sodium 12600 11500 9940 10900 9540 9740 10000 9380 9420 12200 10700 Sulfate 6520 5450 5910 5650 4510 4960 5670 5390 7280 10100 9330 Sulfide Tetrahydrofuran Tin 2.5 Toluene 0.58 Total Dissolved Solids 126000 115000 115000 111000 107000 90000 89000 79000 145000 110000 107000 Trichlorofluoromethane Vanadium Zinc 5.7 12.8 40.5 8.6 7.9 MW-14 Acetone 14.7 Alkalinity, Total as CaCO3 65500 66600 64900 67100 61800 63500 55300 59700 50400 51500 45200 Arsenic 5.1 Barium 241 238 234 246 212 214 221 188 188 183 179 Beryllium 0.81 0.61 0.83 0.59 0.54 0.6 0.57 0.83 0.63 0.54 bi s (2-Ethylhexyl) phtha late Chloride 3730 3710 3870 3840 3930 3620 3260 3410 3470 3930 3510 Chloromethane Chromium Copper Cyanide 4.3 5.3 Dichlorodifluoromethane 2.4 4.5 3 2.4 3 3.6 3.9 3.6 2.3 3.6 2.1 Iron 40.3 36.2 124 93.9 134 123 Jill M. Lead Manganese 38.3 17.4 18.4 18.1 13.7 21.6 25.7 Mercury Methylene Chloride 1.6 Nickel 3.9 6 4.4 6.3 2.6 2.7 2.8 2.8 Silver Sodium 17900 18600 17400 18600 16900 17100 16900 16200 15400 15800 14500 Sulfate 663 1400 1080 1790 Tetrachloroethene 0.53 0.48 0.52 0.61 Thallium 0.048 Total Dissolved Solids 150000 152000 163000 154000 152000 142000 130000 118000 85000 135000 131000 Trichlorofluoromethane 1 1.5 0.92 0.86 0.79 0.8 0.87 0.75 0.58 1.1 0.54 0.59 Vanadium Zinc 5.31 6.3 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 NE pg/L 0.2 pg/L 600 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 350 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 0.005 pg/L 0.05 pg/L 200 pg/L 4 pg/L 250000 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.005 pg/L 0.05 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 100 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L NE pg/L 2000 pg/L 600 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 4 pg/L 3 pg/L 250000 pg/L 3 pg/L 10 pg/L 1000 pg/L 70 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L NE pg/L 250000 pg/L 0.7 pg/L 0.2 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Historical detections by well location -. Tetrahydrofuran Thallium Toluene Total Dissolved Solids 135000 149000 126000 138000 127000 130000 124000 Trichlorofluoromethane 0.32 Vanadium Zinc 30.8 MW-13 1,1-Dichloroethene Acetone Alkalinity, Total as CaCO3 36200 46400 43200 58700 43900 52200 44500 Arsenic Barium 130 77.1 106 176 279 144 139 164 176 126 Benzo(a)pyrene Be nzo(b)flu ora nthe ne Benzo(g,h,i)perylene 1.5 Beryllium 1.2 2.4 3.5 1.4 2.3 Chloride 5870 3880 5700 3820 6150 5380 Chromium 3 7.1 5.5 3.9 4 1.7 Cobalt Copper 3.8 7.6 6.9 6.1 Cyanide Dibenz(a,h)anthracene Indeno(1,2, 3-cd )pyrene Iron 232 • 1 EgMe • . I 1� .1 Lead 5.4 6.5 7.5 6.4 4.3 Manganese 34.1 48.8 Mercury Nickel Silver 0.72 0.4 Sodium 10700 11200 11700 19100 14600 16700 20200 Sulfate 8660 8680 9360 7820 9770 9420 9460 Sulfide 151 106 178 Tetrahydrofuran 18.6 Tin Toluene Total Dissolved Solids 119000 113000 114000 87000 144000 110000 159000 Trichlorofluoromethane Vanadium Zinc 13.7 17.2 37.3 51 20 31.6 MW-14 Acetone Alkalinity, Total as CaCO3 42300 37400 32800 35600 28900 30100 30400 Arsenic Barium 193 163 140 254 160 122 143 125 129 130 Beryllium 0.6 bi s (2-Ethylhexyl) phtha late Chloride 3720 3630 4100 4290 4790 Chloromethane 0.24 Chromium 4.5 6.6 6 1.8 2.3 3 Copper 4.8 9.5 5.8 Cyanide 6 D ich to rod iflu orom etha n e Iron 05 . f 142 Eramej Lead Manganese NEWAIJ 40.2 Mercury Methylene Chloride Nickel Silver 5.3 8.6 13.7 12.5 0.74 0.39 Sodium 14400 12800 12300 13500 15000 14300 12700 Sulfate Tetrachloroethene Thallium Total Dissolved Solids 1�13.3 124000 123000 102000 127000 145000 138000 Trichlorofluoromethane 0.34 Vanadium Zinc 11.7 27.4 231 12 19.8 117 0.8 0.41 18.6 242 7.2 0.54 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 Facility Permit NE pg/L Tetrahydrofuran 0.2 pg/L Thallium 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc MW-13 350 pg/L 1,1-Dichloroethene 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 0.005 pg/L Benzo(a)pyrene 0.05 pg/L Benzo(b)fluoranthene 200 pg/L Benzo(g,h,i)perylene 4 pg/L Beryllium 250000 pg/L Chloride 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 100 pg/L Nickel 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate NE pg/L Sulfide NE pg/L Tetrahydrofuran 2000 pg/L Tin 600 pg/L Toluene 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc MW-14 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 10 pg/L Arsenic 700 pg/L Barium 4 pg/L Beryllium 3 pg/L bis(2-Ethylhexyl)phthalate 250000 pg/L Chloride 3 pg/L Chloromethane 10 pg/L Chromium 1000 pg/L Copper 70 pg/L Cyanide 1000 pg/L Dichlorodifluoromethane 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 20 pg/L Silver NE pg/L Sodium 250000 pg/L Sulfate 0.7 pg/L Tetrachloroethene 0.2 pg/L Thallium 500000 pg/L Total Dissolved Solids 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc 0 Old Salisbury Road Landfill (C&D) Historical detections by well location 88.71 64.61 85.61 791 62 0.21 7.3 97.9 583 186 0.4 IM 4.1 ).461 0.56 130 1.7 0.1 0.48 5 59 46 57 160 2 4.8 9.2 11 8.3 210 460 250 1 6.6 5.2 13 ! 170 3.2 8 Highlighted cells are at or above the current standard. Blank cells indicate either INS or ND. W-S GW Revised.xlsb A2 350 pg/L 70 pg/L 0.1 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 4 pg/L 250000 pg/L 70 pg/L 10 pg/L 1000 pg/L 70 pg/L 300 pg/L 15 pg/L 50 pg/L 3 pg/L 100 pg/L NE pg/L 250000 pg/L NE pg/L NE pg/L 0.2 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Value Row Labels MW-15 Column Historical Labels detections by well location 1,1-Dichloroethene 2,4-D 0.27 4,4'-DDD Acetone 13.2 Alkalinity, Total as CaCO3 96500 91300 74200 89900 112000 110000 98100 101000 104000 103000 91500 Arsenic 4.5 Barium 23.8 13.5 29.8 24.4 11.4 17.1 22.7 14 11 74 105 Beryllium 0.22 Chloride 55500 72100 115000 128000 89700 89800 104000 98000 94000 113000 98200 Chloroform 0.45 0.44 0.44 0.4 0.44 0.7 0.44 0.26 Chromium 5.4 7.6 Copper 2.5 3 2.6 7.1 8.8 Cyanide 4.2 Iron IIIIIIIIIIIIIM 227 off .1 0.1 Lead 1 6 6.8 Manganese Methylene Chloride 2.4 Nickel 1.6 2.7 3.9 4.3 Sodium 19700 19900 23000 26100 20500 19800 21600 20200 20100 21800 20300 Sulfate 38300 40600 45900 49900 54600 59600 58300 58700 63700 70000 65400 Sulfide Tetrahydrofuran 8.9 8.2 9.2 14.8 12 16.8 27.3 19.8 16.9 Thallium 0.049 Total Dissolved Solids 269000 311000 448000 395000 369000 370000 410000 371000 418000 362000 360000 Trichlorofluoromethane 0.21 0.42 0.22 0.71 2.1 4.4 5.1 4.8 4.4 Vanadium Zinc 5.1 5.1 5.8 6.6 7.1 16.2 6.3 5.9 35.4 49 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 350 pg/L 70 pg/L 0.1 pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 4 pg/L 250000 pg/L 70 pg/L 10 pg/L 1000 pg/L 70 pg/L 300 pg/L 15 pg/L 50 pg/L 3 pg/L 100 pg/L NE pg/L 250000 pg/L NE pg/L NE pg/L 0.2 pg/L 500000 pg/L 2000 pg/L 0.3 pg/L 1000 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value Row Labels MW-15 Historical detections by we 1,1-Dichloroethene 3.1 2,4-D 4,4'-DDD 0.062 Acetone Alkalinity, Total as CaCO3 54700 96600 64300 78900 77600 75300 Arsenic 7.1 5.7 Barium 41.5 8.6 23.8 59.6 143 115 Beryllium Chloride 146000 83400 124000 124000 143000 60600 Chloroform 0.49 0.77 0.63 0.49 1.4 Chromium 6.7 7.2 Copper 10.5 Cyanide 5.2 Iron 233 292 239 1 11 Mtollifill Lead 9.5 7.6 Manganese 33 34.7 14 . Methylene Chloride Nickel Sodium 24000 24200 25300 26700 21200 16300 Sulfate 43800 59500 53200 41200' 35600 25800 Sulfide 100 Tetrahydrofuran 15.5 21.4 14.7 7.4 6.3 Thallium Total Dissolved Solids 464000 373000 410000 442000 298000 260000 Trichlorofluoromethane 3.9 5.3 7.6 4.3 8.1 7.3 Vanadium Zinc 5.31 17.1 22.7 45.6 51.1 II location Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 6000 pg/L NE pg/L 10 pg/L 700 pg/L 4 pg/L 2 pg/L 250000 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 2 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 40 pg/L NE pg/L NE pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 0.05 pg/L 0.005 pg/L 0.05 pg/L 200 pg/L 0.5 pg/L 4 pg/L 3 pg/L 250000 pg/L 3 pg/L 10 pg/L 5 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.005 pg/L 0.05 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L NE pg/L 600 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Value Column Historical Labels detections by well location Row Labels SW-1 Acetone 11.2 Alkalinity, Total as CaCO3 40100 15900 22300 27400 49200 43600 33200 57400 27700 35100 44500 Arsenic 8.5 3.6 Barium 25.6 120 109 47 68.2 47.5 86.8 65.9 69.5 65 72.2 Beryllium 0.54 Cadmium Chloride 12100 35100 55400 18300 29700 35700 49200 26800 26000 21600 31500 Chromium 3.8 Cobalt Copper 5.5 8.6 3.9 Cyanide 4.4 4.7 Endrin Iron • •:� .-� .I •�� �,� ..� I Lead 3.4 Manganese 48.5 -me Mercury Methylene Chloride 2 Nickel 2.5 Selenium Silver Sodium 10400 17000 19400 11800 15600 17000 23000 14200 13000 12800 16000 Sulfate 533 7890 7970 4140 2060 2730 2530 3410 4320 4460 3690 Sulfide 52.1 Total Dissolved Solids 76000 143000 174000 106000 131000 123000 143000 116000 118000 113000 140000 Vanadium Zinc 16.1 5.2 10.1 7.2 7.5 SW-2 1,4-Dioxane (p-Dioxane) 2.2 2.7 1.3 2-Hexanone 1.8 3, 3'-Dichlorobenzid ine 3-Methylchola nth rene Acetone 12.9 Alkalinity, Total as CaCO3 78800 74900 54900 62600 56000 57600 46200 58800 32300 43200 33200 Arsenic 3.7 Barium 100 110 85.6 78.8 74.2 65.4 77.5 108 73.1 70 0 Benzo(a)anthracene Benzo(a)pyrene Be nzo(b)flu ora nthe ne Benzo(g,h,i)perylene Be nzo(k)fl uo ra nthene Beryllium 3.7 bi s (2-Ethylhexyl) phtha late Chloride 19300 20200 19400 12800 13500 15200 13800 6190 9720 12500 4050 Chloromethane 0.12 Chromium 2.8 3.8 1 Chrysene cis-1,2-Dichloroethene 0.33 Cobalt Copper 2.2 4.1 81.6 Cyanide 4.2 Dibenz(a,h)anthracene Indeno(1,2, 3-cd )pyrene Iron �� :•I 1 �I I 1 •1 Ms It 1 1 .oil Lead 2.7 Manganese .:� .1 Mercury 0.2 Methylene Chloride Nickel 1.6 16.4 Selenium Silver Sodium 14200 14500 12300 11900 11300 11600 1160 110200 8420 11300 8390 Sulfate 19300 16600 13500 20000 11100 9920 10900 6270 17100 11600 7280 Sulfide Tetrahydrofuran 61.3 Toluene 0.52 Total Dissolved Solids 171000 166000 182000 144000 135000 125000 129000 106000 113000 105000 125000 Vanadium Zinc 51 249 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 Facility Permit Old Salisbury Road Landfill (C&D) Historical detections by well location fL units Row Labels SW-1 6000 pg/L Acetone 2.2 NE pg/L Alkalinity, Total as CaCO3 63700 45200 72700 58000 79700 47200 19600 10 pg/L Arsenic 5.9 700 pg/L Barium 276 65.8 71.1 58.9 63.3 70.4 42.5 4 pg/L Beryllium 1.1 2 pg/L Cadmium 0.7 250000 pg/L Chloride 19500 23700 18100 20600 19700 25300 19100 10 pg/L Chromium 1 pg/L Cobalt 1000 pg/L Copper 16.4 70 pg/L Cyanide 2 pg/L Endrin 0.08 300 pg/L Iron ��� :�� .•�� �� �� •� 15 pg/L Lead •. 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 8.7 20 pg/L Selenium 7 20 pg/L Silver NE pg/L Sodium 12500 14500 13000 12400 15500 14300 9390 250000 pg/L Sulfate 3130 2820 2190 2700 2090 NE pg/L Sulfide 500000 pg/L Total Dissolved Solids 122000 126000 125000 104000 131000 98000 140000 0.3 pg/L Vanadium 1000 pg/L Zinc 69.8 SW-2 3 pg/L 1,4-Dioxane (p-Dioxane) 40 pg/L 2-Hexanone NE pg/L 3,3'-Dichlorobenzidine 3.6 NE pg/L 3-Methylcholanthrene 2.9 6000 pg/L Acetone 4 NE pg/L Alkalinity, Total as CaCO3 2390 41300 48900 48600 44700 44200 26100 10 pg/L Arsenic 6.2 700 pg/L Barium 171 59.7 50.1 51.7 46.5 53.4 81 0.05 pg/L Benzo(a)anthracene 0.005 pg/L Benzo(a)pyrene 0.05 pg/L Benzo(b)fluoranthene 200 pg/L Benzo(g,h,i)perylene 1.8 0.5 pg/L Benzo(k)fluoranthene 4 pg/L Beryllium 0.64 3 pg/L bis(2-Ethylhexyl)phthalate 1.1 250000 pg/L Chloride 28200 10700 11600 10800 10300 11300 10900 3 pg/L Chloromethane 10 pg/L Chromium 3.2 5 pg/L Chrysene 1.1 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper 3.2 70 pg/L Cyanide 0.005 pg/L Dibenz(a,h)anthracene 0.05 pg/L Indeno(1,2,3-cd)pyrene 300 pg/L Iron ENLI IO W'a [gill M 15 pg/L Lead 7.4 50 pg/L Manganese 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 3.1 20 pg/L Selenium 20 pg/L Silver NE pg/L Sodium 17600 9840 10300 9160 9990 9890 8650 250000 pg/L Sulfate 5620 12700 5490 5090 4240 6180 38300 NE pg/L Sulfide 142 NE pg/L Tetrahydrofuran 18.4 600 pg/L Toluene 500000 Ng/L Total Dissolved Solids 117000 120000 114000 91000 101000 101000 189000 0.3 pg/L Vanadium 1000 pg/L Zinc 28 13.5 0.4 49.2 0.2 61 57.6 3.7 92.5 77.7 0.28 59.4 0.2 0.62 1 52.1 0.081 1 0.36 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 6000 pg/L NE pg/L 10 pg/L 700 pg/L 4 pg/L 2 pg/L 250000 pg/L 10 pg/L 1 pg/L 1000 pg/L 70 pg/L 2 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L 500000 pg/L 0.3 pg/L 1000 pg/L 3 pg/L 40 pg/L NE pg/L NE pg/L 6000 pg/L NE pg/L 10 pg/L 700 pg/L 0.05 pg/L 0.005 pg/L 0.05 pg/L 200 pg/L 0.5 pg/L 4 pg/L 3 pg/L 250000 pg/L 3 pg/L 10 pg/L 5 pg/L 70 pg/L 1 pg/L 1000 pg/L 70 pg/L 0.005 pg/L 0.05 pg/L 300 pg/L 15 pg/L 50 pg/L 1 pg/L 3 pg/L 100 pg/L 20 pg/L 20 pg/L NE pg/L 250000 pg/L NE pg/L NE pg/L 600 pg/L 500000 pg/L 0.3 pg/L 1000 pg/L Facility Permit Old Salisbury Road Landfill (C&D) Value -. SW-1 Historical detections Acetone 22.7 Alkalinity, Total as CaCO3 Arsenic Barium 45.6 78.2 79.7 70.3 88 5 Beryllium Cadmium Chloride Chromium 0.61 0.67 1.2 0.61 Cobalt Copper Cyanide Endrin Iron Lead Manganese Mercury Methylene Chloride Nickel Selenium Silver 0.39 0.37 0.51 Sodium Sulfate Sulfide Total Dissolved Solids Vanadium Zinc SW-2 1,4-Dioxane (p-Dioxane) 2-Hexanone 3,3'-Dichlorobenzidi ne 3-M ethylcho la nth re ne Acetone Alkalinity, Total as CaCO3 Arsenic 5.5 Barium 46.3 50.6 50.6 49.4 300 4 Benzo(a)anthracene Benzo(a)pyrene Benzo (b )fl uo ra nthene Benzo(g,h,i)perylene Benzo (k)flu ora nthe ne Beryllium b is(2-Ethyl hexyl )p htha late Chloride Chloromethane Chromium 0.42 Chrysene cis-1,2-Dichloroethene Cobalt Copper Cyanide Di benz(a, h)anthracene I ndeno(1,2,3-cd)pyrene Iron Lead 11 Manganese Mercury Methylene Chloride Nickel Selenium Silver 0.5 0.26 0.26 Sodium Sulfate Sulfide Tetrahydrofuran Toluene Total Dissolved Solids Vanadium Zinc Highlighted cells are at or above the current standard. Blank cells indicate either INS or ND. W-S GW Revised.xlsb A2 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Historical detections by well location SW-3 3 pg/L 1,4-Dioxane (p-Dioxane) 1 1.3 40 pg/L 3&4-Methylphenol(m&p Cresol) 0.1 pg/L 4,4'-DDD 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 330000 360000 473000 181000 356000 700 pg/L Barium 169 189 273 122 223 1 pg/L Benzene 0.73 250000 pg/L Chloride 19600 26100 28000 12000 22300 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 42 pg/L Endosulfan II 300 pg/L Iron I s [sit] 15 pg/L Lead 50 pg/L Manganese 1 pg/L Mercury 0.18 3 pg/L Methylene Chloride 100 pg/L Nickel 4 6.9 3.9 NE pg/L Sodium 22500 27200 34000 16900 27000 250000 pg/L Sulfate 28600 29600 43600 16000 18500 NE pg/L Sulfide 54 NE pg/L Tetrahydrofuran 6.1 3.4 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 421000 415000 ..: 241000 413000 0.3 pg/L Vanadium 1000 pg/L Zinc 7.1 SW-4 350 pg/L 1,1-Dichloroethene 3 pg/L 1,4-Dioxane (p-Dioxane) 40 pg/L 2-Hexanone 0.1 pg/L 4,4'-DDD 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 281000 207000 265000 145000 211000 700 pg/L Barium 170 215 382 124 138 1 pg/L Benzene 0.25 250000 pg/L Chloride 42200 44300 18700 24800 29800 70 pg/L Chloroform 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 0.32 1 pg/L Cobalt 1000 pg/L Copper 5.8 70 pg/L Cyanide 4.1 42 pg/L Endosulfan II 2 Ng/L Endrin aldehyde 300 pg/L Iron 15 pg/L Lead 3.6 50 pg/L Manganese • . 3 pg/L Methylene Chloride 100 pg/L Nickel 4.8 4.4 2.6 NE pg/L Sodium 31400 29100 22000 20000 23400 250000 pg/L Sulfate 68200 52500 17400 27500 24400 NE pg/L Tetrahydrofuran 9.1 6.7 13.7 5.7 500000 pg/L Total Dissolved Solids 471000 392000 444000 236000 327000 2000 pg/L Trichlorofluoromethane 0.3 pg/L Vanadium 1000 pg/L Zinc 14.4 90.1 6.9 16.2 000 251000 520000 161000 210000 118000 217 173 270 114 152 105 0.42 800 18400 34000 10500 16300 27000 3.4 0.26 4.4 4.6 6 3.6 6.8 2.8 2.8 1 24600 38460 14700 20900 18260 15200 18500 11400 27000 17000 6.3 3.3 2.8 321000 231000 300000 233000 9.6 13.6 5K 16 192000 187000 240000 148000 187000 242000 110 121 128 113 115 187 36800 27400 27900 20300 19800 19000 5.6 1.2 2.5 3.6 25600 23400 26000 16900 20200 23800 26700 18200 28600 16600 24900 23500 3.5 3.6 4.1 17000 289000 325000 229000 267000 371000 0.32 8.31 1 1 1 1 7.31 1 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A2 Facility Permit SW-3 Old Salisbury Road Landfill (C&D) Historical detections by well location 3 pg/L 1,4-Dioxane (p-Dioxane) 40 pg/L 3&4-Methylphenol(m&p Cr 3. 0.1 pg/L 4,4'-DDD 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone NE pg/L Alkalinity, Total as CaCO3 389000 259000 5160C 700 pg/L Barium 206 181 34 1 pg/L Benzene 0.54 0.32 0.8 250000 pg/L Chloride 27000 16900 348C 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 42 pg/L Endosulfan II 300 pg/L Iron name OR-MUNKLULS 15 pg/L Lead 50 pg/L Manganese out e E 1 pg/L Mercury 3 pg/L Methylene Chloride 100 pg/L Nickel 4.8 1 NE pg/L Sodium 29900 29900 411C 250000 pg/L Sulfate 16800 26300 6250 NE pg/L Sulfide NE pg/L Tetrahydrofuran 10.2 9.7 18. 2000 pg/L Tin 500000 pg/L Total Dissolved Solids 473000 319000 Me 0.3 pg/L Vanadium 1000 pg/L Zinc 10. SW-4 350 pg/L 1,1-Dichloroethene _ 3 pg/L 1,4-Dioxane (p-Dioxane) 40 pg/L 2-Hexanone 0.1 pg/L 4,4'-DDD 0.1 pg/L 4,4'-DDT 6000 pg/L Acetone 0.079 100 317000 221000 160C 185 315 179 1 0.34 0.25 D00 24300 22800 209 0.0711 0.085' . � . 11 M ie mums 25000 33800 21300 1 20100 36400 26400 1 5.1 4.8 4.5 27000 432000 329000 22 0.062 NE pg/L Alkalinity, Total as CaCO3 140000 158000 152000 147000 220000 158000 131C 700 pg/L Barium 82.8 126 101 106 151 136 1 1 pg/L Benzene 250000 pg/L Chloride 24300 30800 31000 26900 28800 30900 23E 70 pg/L Chloroform 0.97 10 pg/L Chromium 70 pg/L cis-1,2-Dichloroethene 1 pg/L Cobalt 1000 pg/L Copper 70 pg/L Cyanide 42 pg/L Endosulfan II 2 pg/L Endrin aldehyde 300 pg/L Iron 15 pg/L Lead 50 pg/L Manganese 3 pg/L Methylene Chloride 100 pg/L Nickel NE pg/L Sodium 17800 24400 201C 250000 pg/L Sulfate 17600 23500 230C NE pg/L Tetrahydrofuran 4.4 500000 pg/L Total Dissolved Solids 222000 257000 27000 2000 pg/L Trichlorofluoromethane 0.27 0.2 0.3 pg/L Vanadium 1000 pg/L Zinc 0.066 0.061 29000 2001 32300 2361 349000 27201 1 1 1 Highlighted cells are at or above the current standard. Blank cells indicate either NS or ND. W-S GW Revised.xlsb A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Method (Multiple Surface water detections within the last 6 years Qualifier (Multiple Items) 2B units Max of Result 2000 pg/L Acetone 11.2 20000 pg/L Alkalinity, Total as CaCO3 40100 15900 22300 27400 49200 43600 33200 57400 27700 35100 44500 63700 45200 150 pg/L Arsenic 8.5 3.6 5.9 21000 pg/L Barium 25.6 120 109 47 68.2 47.5 86.8 65.9 69.5 65 72.2 276 65.8 6.5 pg/L Beryllium 0.54 1.1 NE pg/L Cadmium 0.7 230000 pg/L Chloride 12100 35100 55400 18300 29700 35700 49200 26800 26000 21600 31500 19500 23700 11 pg/L Chromium 3.8 13 NE pg/L Cobalt 9 NE pg/L Copper 5.5 8.6 3.9 16.4 5 pg/L Cyanide 4.4 4.7 1000 pg/L Iron 1550 6980 889 1840 6560 4900 5040 5660 5520 9830 8870 155000 8210 NE pg/L Lead 3.4 18.3 NE pg/L Manganese 255 149 48.5 135 926 461 804 1050 465 688 1160 1760 749 11000 pg/L Methylene Chloride 2 25 pg/L Nickel 2.5 8.7 NE pg/L Selenium 7 NE pg/L Sodium 10400 17000 19400 11800 15600 17000 23000 14200 13000 12800 16000 12500 14500 250000 pg/L Sulfate 533 7890 7970 4140 2060 2730 2530 3410 4320 4460 3690 3130 2820 NE pg/L Sulfide 52.1 NE pg/L Total Dissolved Solids 76000 143000 174000 106000 131000 123000 143000 116000 118000 113000 140000 122000 126000 NE pg/L Vanadium 9.2 4.3 37 NE pg/L Zinc 16.1 5.2 10.1 7.2 7.5 69.8 NE pg/L 1,4-Dioxane (p-Dioxane) 2.2 2.7 1.3 NE pg/L 2-Hexanone 1.8 2000 pg/L Acetone 12.9 20000 pg/L Alkalinity, Total as CaCO3 78800 74900 54900 62600 56000 57600 46200 58800 32300 43200 33200 2390 41300 150 pg/L Arsenic 3.7 17 6.2 21000 pg/L Barium 100 110 85.6 78.8 74.2 65.4 77.5 108 73.1 70 700 171 59.7 6.5 pg/L Beryllium 3.7 0.64 230000 pg/L Chloride 19300 20200 19400 12800 13500 15200 13800 6190 9720 12500 4050 28200 10700 NE pg/L Chloromethane 0.12 11 pg/L Chromium 2.8 3.8 40.3 3.2 NE pg/L cis-1,2-Dichloroethene 0.33 NE pg/L Cobalt 5.9 4.4 NE pg/L Copper 2.2 4.1 81.6 3.2 5 pg/L Cyanide 4.2 5 pg/L Dibenz(a,h)anthracene 2 NE pg/L Indeno(1,2,3-cd)pyrene 2.2 1000 pg/L Iron 4030 8890 4370 4140 2540 1740 1790 29900 1510 2070 226000 75000 2130 NE pg/L Lead 2.7 75 7.4 NE pg/L Manganese 1040 825 680 615 397 196 304 1160 317 291 1020 1010 219 0.012 pg/L Mercury 0.2 11000 pg/L Methylene Chloride 3.1 25 pg/L Nickel 1.6 16.4 3.1 NE pg/L Sodium 14200 14500 12300 11900 11300 11600 11600 10200 8420 11300 8390 17600 9840 250000 pg/L Sulfate 19300 16600 13500 20000 11100 9920 10900 6270 17100 11600 7280 5620 12700 NE pg/L Sulfide 142 110000 pg/L Tetrahydrofuran 61.3 18.4 11 pg/L Toluene 0.52 NE pg/L Total Dissolved Solids 171000 166000 182000 144000 135000 125000 129000 106000 113000 105000 125000 117000 120000 NE pg/L Vanadium 2.4 3.2 127 11.6 NE pg/L Zinc 5 249 28 6/10/2020 1 of 2 A3 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Method (Multiple Surface water detections within the last 6 years Qualifier (Multiple Items) 2B L NE pg/L 1.3 1,4-Dioxane (p-Dioxane) 2000 pg/L Acetone 16.2 20000 pg/L Alkalinity, Total as CaCO3 330000 360000 473000 181000 356000 477000 251000 520000 161000 210000 118000 389000 259000 21000 pg/L Barium 169 189 273 122 223 217 173 270 114 152 105 206 181 1.19 pg/L Benzene 0.73 0.42 0.54 0.32 230000 pg/L Chloride 19600 26100 28000 12000 22300 33800 18400 34000 10500 16300 27000 27000 16900 11 pg/L Chromium 3.4 NE pg/L cis-1,2-Dichloroethene 0.26 NE pg/L Cobalt 4.2 12.6 5.3 7.2 3 6.8 3.4 14.8 NE pg/L Copper 4.4 5 pg/L Cyanide 4.6 6 1000 pg/L Iron 7910 5650 13000 2500 13100 1720 8240 10500 3390 4160 4940 5270 8890 NE pg/L Lead 2.7 NE pg/L Manganese 3280 5130 7890 2130 6310 7340 4750 8350 2310 3860 1420 5080 4320 0.012 pg/L Mercury 0.18 11000 pg/L Methylene Chloride 1 25 pg/L Nickel 4 6.9 3.9 5.5 3.6 6.8 2.8 2.8 4.8 NE pg/L Sodium 22500 27200 34000 16900 27000 35500 24600 38400 14700 20900 18200 29900 29900 250000 pg/L Sulfate 28600 29600 43600 16000 18500 33800 15200 18500 11400 27000 17000 16800 26300 NE pg/L Sulfide 54 110000 pg/L Tetrahydrofuran 6.1 3.4 6.3 3.3 10.2 9.7 NE pg/L Tin 2.8 NE pg/L Total Dissolved Solids 421000 415000 668000 241000 413000 600000 321000 623000 231000 300000 233000 473000 319000 NE pg/L Vanadium 2 2.5 5.6 9.7 NE pg/L Zinc 7.1 9.6 13.6 NE pg/L 6.6 6.5 1,4-Dioxane (p-Dioxane) NE pg/L 2-Hexanone 3.1 2000 pg/L Acetone 16 20000 pg/L Alkalinity, Total as CaCO3 281000 207000 265000 145000 211000 192000 187000 240000 148000 187000 242000 140000 158000 21000 pg/L Barium 170 215 382 124 138 110 121 128 113 115 187 82.8 126 1.19 pg/L Benzene 0.25 230000 pg/L Chloride 42200 44300 18700 24800 29800 36800 27400 27900 20300 19800 19000 24300 30800 11 pg/L Chromium 4.7 NE pg/L cis-1,2-Dichloroethene 0.32 NE pg/L Cobalt 6.4 2.6 11.6 5.9 NE pg/L Copper 5.8 5 pg/L Cyanide 4.1 5.6 1000 pg/L Iron 5580 17400 38700 3890 3020 802 1480 1520 1520 2240 9220 638 2520 NE pg/L Lead 3.6 NE pg/L Manganese 4510 2960 7710 1470 3580 1020 2900 2930 1930 2550 5050 739 2250 11000 pg/L Methylene Chloride 1.2 25 pg/L Nickel 4.8 4.4 2.6 2.5 3.6 NE pg/L Sodium 31400 29100 22000 20000 23400 25600 23400 26000 16900 20200 23800 17800 24400 250000 pg/L Sulfate 68200 52500 17400 27500 24400 26700 18200 28600 16600 24900 23500 17600 23500 110000 pg/L Tetrahydrofuran 9.1 6.7 13.7 5.7 3.5 3.6 4.1 4.4 NE pg/L Total Dissolved Solids 471000 392000 444000 236000 327000 317000 289000 325000 229000 267000 371000 222000 257000 NE pg/L Trichlorofluoromethane 0.32 0.27 NE pg/L Vanadium 7.6 4.5 3.5 5.9 NE pg/L Zinc 14.4 90.1 6.9 8.3 7.3 6/10/2020 2 of 2 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 2 pg/L 10 pg/L 1 pg/L 300 pg/L 50 pg/L 100 pg/L NE pg/L 2000 pg/L 0.3 pg/L 1 pg/L 6 pg/L 6 pg/L 1 pg/L 3000 pg/L 70 pg/L 1000 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L 2000 pg/L 0.03 pg/L 3 pg/L NE pg/L 500000 pg/L 250000 pg/L NE pg/L i May-20 feet Field Static Water Level pg/L EPA 300.0 Sulfate EPA 601 OD Arsenic Barium Beryllium Cadmium Chromium Cobalt Iron Manganese Nickel Sodium Tin Vanadium EPA 7470A Mercury EPA 8260D 1,1-Dichloroethane 1,4-Dichlorobenzene Benzene Chloroethane cis-1,2-Dichloroethene Dichlorodifluoromethane m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride EPA 8260D Mod. 1,4-Dioxane (p-Dioxane) SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-S2D Sulfide November-19 feet Field Static Water Level 32.82 6.69 13.01 4.85 9.3 32.51 9.37 50.28 10.43 3.37 4.55 7.87 50.1 37.81 76400 801 162000 7770 10400 9360 $I$ 22800 227000 6520 38300 5.8 290 309 257 176 56.5 136 52.9 238 66 98.1 224 196 241 23.8 0.72 0.62 6.8 5.6 4 29.7 1 r •r: 211 125 43.5 2740 23700 25.1 80.8 31.4 1 21.1 � �:� 8 5.1 00 7.9 0 4 � 10.6 27.4 3.9 16800 65600 2150 73800 17100 16200 12900 16200 148000 12400 28600 12600 17900 19700 4.8 7.1 0.65 0.69 0.52 0.66 0.46 0.9 0.56 0.48 0.56 0.29 0.85 1.2 0.84 0.91 0.52 1.1 2.4 0.72 0.46 0.34 0.53 38.6 11.4 70.5 130 8.9 1.1 5.6 1.3 1 1 2.2 86600 688000 70900 517000 35700 71600 25000 33900 635000 127000 333000 66400 65500 96500 172000 . ���� 146000 111 163000 165000 93000 130000 :110� 230000 ��� 126000 150000 269000 9050 64300 3320 42100 14500 5910 4090 63707 11000 29500 8400 3730 55500 80.1 242 66.72 15.74 33.96 13.87 20.93 67.7 31.66 101.3 23.17 7.2 9.75 16.76 101.22 77.94 6/10/2020 1 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date Units Concentration 2L r . r . r ./L r r rNE pg/L r • . r pg/L r 11 . r . NE pg/L 600 r . r MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX • 300.0 .. 601 r ■ Cadmium Chromium Copper-®-----®----®_- Sodium EPA r . 8260D cis- 1,2-Dichloroethene®�----®--------_- Chloride - - .. Tetrahydrofuran .. .. 8260D Mod. ■ . ■ . ---------------_- ---------------_- ------------®-_- -------------_- 27.1 11.5 72.6 ----- 11.4 1.9 ----_- 6180 78700 1020 4490 24100 937 ��-_- 12700 6180 901 ©- 95.4 31400 1570 1500 58.8 143 -��------®-----_- 3 1.6 1.8 5.1 ---- 4 1.3 1.6 -- 1.5 _- ---------------_- 1.5EPA --------------_- 3.9 -------_- 4 ---- 4.8 --------_- ------��----_- 1.2 -----------�-_- ----®-----���--_- ----------®-_- 1.3EPA -------------_- 3.7 - 4 7.9 ----_- 6/10/2020 2 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date NE pg/L 84000 736000 69800 384000 34300 82700 25300 39000 726000 102000 150000 58500 66600 91300 Alkalinity, Total as CaCO3 500000 pg/L 250000 pg/L 70 pg/L NE pg/L 250000 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 50 pg/L 100 pg/L NE pg/L 0.3 pg/L 1000 pg/L 1 pg/L 3 pg/L SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide SM 4500-S2D Sulfide pmhos/cm Field Field Specific Conductance deg C Field Field Temperature May-19 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX pg/L EPA 300.0 Sulfate EPA 601 OD Barium Beryllium Chromium Cobalt Copper Iron Manganese Nickel Sodium Vanadium Zinc EPA 7470A Mercury EPA 8260E Mod. 1,4-Dioxane (p-Dioxane) 7 180000 :��� 179000 ��� 169000 168000 78000 157000 :���� 240000 369000 115000 152000 311000 9150 52500 2000 34000 14800 7500 3860 4190 71800 11400 17600 6310 3710 72100 6.4 192 221.9 1450 375.6 967 175.7 221.5 83 198.2 184.8 354.6 531.8 144.9 192.4 507.6 13 13.7 14.5 16.1 15.7 13.1 14.5 13.7 16.2 14.8 15.2 14.2 14.2 16.3 100.3 20.5 43.18 16.43 28.22 102.35 32.3 154.41 31.02 11.22 15.15 24.42 151.2 113.25 120 42 54 40 60 96 54 120 42 40 31.28 40 120 96 2.31 1.78 3.85 1.58 11.68 0.94 12.52 11.94 4.17 6.8 4.97 8.11 3.07 3.65 3.37 11.71 59.87 19.46 7.55 0.94 3.05 9.06 23.79 12.98 2.42 4.17 3 24.7 10.46 12.09 12.43 12 11.42 10.47 10.24 10.26 12.49 11.57 11.53 10.45 10.25 12.15 -193 -333.4 -293.4 -297.8 -81.6 -165.9 -65.1 -47.7 -603.7 -608.2 -469.8 -402.2 -219.3 -111.2 85100 1210 163000 8620 12800 6560 235000 22300 149000 5910 45900 285 260 320 216 55.8 168 47.8 217 65.6 100 200 138 234 29.8 0.61 0.6 0.61 5.4 3.5 9.6 19.5 . • 13.4 i •: 8.4 63.5 3.3 148 7.1 �� 7.2 • • 1 �:$ 6.2 5.2 42.3]17400 0 15800 57300 2540 71200 13000 17500 9620 14100 136000 12800 20700 9940 23000 5.2 18 5.9 5.1 2.31 2 6/10/2020 3 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date Units Concentration 2L 6000 ./L 3 pg/L 1 ./L NE pg/L 00000 .TotalDissolved 0000 ./L r ./L NE pg/L MW-1R ---------------_- MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank EPA MOD Acetone---------------_� Methylene Chloride------ Tetrachloroethene Alkalinity, Total as CaCO3 . .s Chloride_- Cyanide Sulfide Field Field Specific Conductance deg C Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX Field Field Specific Conductance deg C Field 2.3 ---------_- 4.3 --------_- 1.4 -----------�-_- 1150000 1040000 1110000 1710000 ----®----------_- 6/10/2020 4 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date 2L Units Concentration 1111 . 1000 ./L 11 . 1 . NE pg/L 1 .• 111 . 3 pg/L 11 . 1.7 pg/L .11 . MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX .. 300.0 .. 601 1 ■ Copper-----------_- Manganese Sodium Vanadium---- EPA 1 .EPA 8151 EPA 8260B ■ • - - Dichlorodifluoromethane Methylene Chloride------ o-Xylene-------------_- Tetrachloroethene Toluene ---------------_- •11 11 1'111 :1.1 - 11 1.1 - 357000 1 11 11 ®. 1 - ••11 _- --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- 15.91 11.3 35 ----- 22 2090 90800 475 5030 28200 371 653 8920 7940 584 24700 1620 336 170 115 _- 11 .••1llllllllllll,•••. .11 •.11111111111111111111111 11 11 11 111 .11 .11 1.11 :.11 1llllllllllllllll,- 4.8 ----------_- ---------------_- ®-11111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- --11111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- --llllllllllllllllllll,11111111111111111111111111111111111111111,111111111111111111111®11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- 1.7 -----------_- --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111�111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111®111111111111111111111111111111111111,- 5.7 --------_- 0.88 -------------_- --------------_- 6/10/2020 5 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date 2000 pg/L 88 pg/L 3 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L NE pg/L 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L 1.2 1.3 LIATIM i 1 0.86 0.21 Trichlorofluoromethane Vinyl acetate _ EPA 8260E Mod. 1,4-Dioxane (p-Dioxane) SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide SM 4500-S2D Sulfide pmhos/cm Field Field Specific Conductance deg C Field Field Temperature May-18 feet Field Static Water Level Total Well Depth mg/1 Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX pg/L EPA 300.0 Sulfate EPA 6010 Arsenic Barium Beryllium Chromium Cobalt Copper Iron Lead Manganese Nickel 2 7 2.1 2.4 84100 573000 192000 291000 35600 78500 24200 33500 652000 161000 117000 52800 67100 89900 164000 .111 213000 496000 156000 171000 68000 139000 jEfLf 237000 301000 111000 154000 395000 8920 34500 2660 25200 15100 6580 3110 5330 88500 11800 14400 5120 3840 128000 678 4.1 5 4.3 4 53.8 218.7 1145 426 671 170.1 238.2 54.1 152.3 1866 346.4 426 124.8 178 699 13.5 14 14.9 14.7 13.8 7.3 14.6 14.5 13 13.4 14.8 14.2 13.6 15.5 71.02 15.65 38.14 16.68 21.98 74.1 31.8 106.92 23.28 7.57 9.22 16.97 104.4 78.28 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 1.09 0.71 1.1 0.21 5.49 1.2 5.49 6.55 0.13 1.53 0.36 4.06 5.48 2.01 0.8 1.34 5.46 60.65 1.08 0.57 0.78 2.67 8.15 4.77 1.61 1.55 2.9 5.13 5.5 6.2 6.3 6 5.9 5.5 5.4 5.6 6.3 6 5.9 5.6 5.5 6.2 199.4 4.1 -52.1 198.8 194.1 203.4 237.7 185 -105.9 -5.1 196.2 256.7 200.4 68 105000 691 50300 8220 14200 2980 1 111 15300 64300 4510 54600 5.7 263 289 234 270 52.5 158 41.2 193 94.7 82.8 82.8 114 212 11.4 2.1 0.63 0.59 6.4 5.3 2.6 4.1 5 3 111 .0 4.9 • : 88.2 35 39.3 35.3 3.9 Be 175 108 124 17.6 1 16.8 of 4.1 43.8 4.4 4.2 of 8.5 . I 7.4 17.4 2.6 ;; 6/10/2020 6 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date NE pg/L 0.3 pg/L 1000 pg/L 0.2 pg/L 1 pg/L 6 pg/L 6 pg/L 40 pg/L NE pg/L 6000 pg/L 1 pg/L 70 pg/L 70 pg/L 1000 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L 2000 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L NE pg/L 15500 73200 2680 17800 12800 16600 8810 14300 157000 12000 13400 9540 16900 20500 Sodium Vanadium Zinc EPA 6020B Thallium EPA 7470 Mercury EPA 8260 1,1-Dichloroethane 1,4-Dichlorobenzene 2-Hexanone 4-Methyl-2-pentanone (MIBK) Acetone Benzene Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide SM 4500-S2D Sulfide pmhos/cm Field Field Specific Conductance °C Field Field Temperature December-17 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity 5 19.9 9 6.6 0.029 0.34 0.39 1.1 0.41 0.72 1.7 16.4 0.41 0.55 0.45 0.71 0.55 0.85 0.23 1.2 3 1.7 0.68 1.7 2.4 0.65 0.78 461 24.9 192 5.9 14.8 0.93 1.2 1.3 0.89 0.79 0.42 76100 663000 115000 101000 33600 75900 27000 31800 506000 130000 65800 47200 61800 112000 166000 :::I11 177000 250000 164000 181000 75000 133000 1I11 232000 218000 107000 152000 369000 9040 42200 2180 12500 15200 6490 3660 4830 158000 12500 11100 4790 3930 89700 5 4.8 4.41 4.8 4.2 1051 240 221.7 1391 423.5 343.9 176.7 234.9 70.7 155.8 1840 349.9 304.2 121.8 183.9 641 22 17.2 18.7 18.2 17.3 17.8 16.5 18.9 17.4 17.9 17 16.2 19.1 16.9 35.1 8.3 21.15 9.44 11.5 37 18.55 52.94 12.18 4.14 5.46 9.09 52.09 39.58 60 21 27 20 50 48 27 60 21 20 15.7 20 60 48 3.3 0.4 0.5 0.6 5.1 1 4.5 6.2 0.1 0.1 0.3 1.3 2.9 2.3 2.8 2.41 9.4 9.6 4.2 3.5 9.7 9.6 7.8 9.8 9.7 9.71 7.4 2.7 6/10/2020 7 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date Units Concentration 21 pg/L 1 . 111 . 600 . 11 . 11 . 1 . NE pg/L .11 .. 0.03 ■ MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Std. Units Field Field pH mv �, ■ • ' 8260 Carbon Disulfide ■ . - - . • • - • - - Chloride . - - .. - - - _ Tetrahydrofuran - Field- - Field Field Temperature feet FieldStatic Water Level Total Well Depth Field Oxygen, Dissolved NTU Fiel • • Std. Units Field Field pH mv Field ■ • ------- �llllllllll� 11 111111111�111111111111111111111111111111111�111111111•..�w..®lllllllllll�..w..11llllllll�lllllllll®' r---�,---- llllllll®' IIIIIIIII�IIIIIIIII4:C41111111111111111,- r-_- ---------------_- 2.5700 -----------_- --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111�111111111111111,- --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111®lllllllllllllllllllll,11111111111111111111111111111111111111111,111111111111111111111111111111111111�111111111111111111111111111111111111,- --------------_- --IIIIIIIIIIIIIIIIIIII,IIIIIIIIIIIIIIIIIIII1llllllllllllllllllll,IIIIIIIIIIIIIIIIIIII111111111111111111OJllllllllllllllllllll1llllllllllllllllllll,®11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- --------®-----_- 5.7 --------_- 1.5 -------------_- 1.4Field -------------_- --llllllllllllllllllll,-11111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- ��llllllll®"' IIIIIIIIIIIWii:l®11111111111111111111111111111®' ' ®lllllllll®' ' ' llllllllllll�lllllllll..�w.11l E=II ' IIIIIIIIIWEi7111111111�1111111111111®' lllllllllllllll,- --11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- --11111111111111111111,11111111111�111111111111�1111111111111111111111111111111111�11111111111111111111111111111111� --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- ®®llllllllllllllllmllllllllllllllllmllllllllllllllllllll1IIIIIIIIIIIIIIIIIiL®llllllllllllllllm®llllllllllllllllm®llllllllllllllllmllllllllllllllllmllllllll�lllllllllllllll,- --11111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- --------T-------_- ®�lllllllllllllll®' 11111111111�11111111111�111111111111111111111111111111111111�1111111111111111:�i7111111111111111�1111111111111111�111111111111111�111111111111®' lllllllllllllll�lllllllllllllll�lllllllll�lllllllllllllll,- --11111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- ®' ' �IIIIIIIi�JlllllllllllillllllllllllliQi�llllllllllllllllllll1®lllllllll�" llllllll®1' ' llllllllllllllllllllllllll�lllllllllll�lllllllll.a mow.' ®lllllllllll®' lllllllllllllll,- 6/10/2020 8 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L NE pg/L 0.3 pg/L 1000 pg/L 1 pg/L 50 pg/L 70 pg/L 0.3 pg/L 6 pg/L 6 pg/L NE pg/L 6000 pg/L 1 pg/L 70 pg/L 70 pg/L 1000 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L 2000 pg/L 0.03 pg/L 1000 pg/L NE pg/L 500000 pg/L 250000 pg/L NE pg/L EPA 300.0 Sulfate EPA 6010 Arsenic Barium Beryllium Chromium Cobalt Iron Lead Manganese Nickel Sodium Vanadium Zinc EPA 7470 Mercury EPA 8151 2,4,5-TP (Silvex) 2,4-D Pentachlorophenol EPA 8260 1,1-Dichloroethane 1,4-Dichlorobenzene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride EPA 8270 Butylbenzylphthalate SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-S2D Sulfide pmhos/cm Field Field Specific Conductance 122000 179000 7830 13400 4740 64100 16200 62400 4960 59600 9 260 323 278 198 53.2 152 46.5 196 106 89.8 84.2 116 214 17.1 0.52 0.54 4 2.7 3.2 1 4.9 7.2 4.6 3.8 3.2 43.1 1 1 11 3.4 37.9 25 37.6 166 1 11 125 193 93.9 1 1 11.8 1 11 20.3 1 1 1 7.5 4.2 43 3.6 10.6 :11 7.6 1 17.9 18.4 15200 77600 2380 65500 13500 15300 9860 14900 138000 1230C 13200 9740 17100 19800 539 5.8 5 5.3 7.1 0.23 0.072 0.27 0.018 0.48 1.4 0.46 1.1 12.1 0.38 0.52 0.44 0.62 0.6 1.1 0.23 1.2 3.9 1.4 1.1 0.68 0.97 28 20.1 131 0.93 1.5 1.6 1.2 0.52 0.87 0.71 1.7 71400 670000 78900 461000 33500 80400 28200 27900 520000 130000 73800 44600 63500 110000 153000 ME :111 164000 .. 111 144000 175000 82000 136000 IN 1111 218000 219000 90000 142000 370000 9290 47600 2650 49200 16200 7390 3860 4430 163000 13000 10400 4770 3620 89800 127 208.3 1393 394.2 1209 176.8 288.4 77.4 160 1989 348.31 299.8 111.4 172.7 624 6/10/2020 9 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date Units Concentration 2L 1111 . 1 1 . 1 . 11 . 1 . NE pg/L 1 . 1 . 1 ./L .111 . pg/L 600 ./L 11 . 500 . MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Field Field Temperature feet Field Static = Water Level :.®wwwwwww®wwwww�� Field Oxygen,DissolvedNTU FieldTurbidityStd. Units FieldField. mv Field .. .. 300.0 - .. 6010 Cobalt Manganese Sodium' EPA .1 1,2-Dichloroethane Acetone Carbon Disulfide Ethylbenzene--------------_- - - o-Xylene--------------_- Trichloroethene SM 1 ���w�����■�������� �wwwwwww�wwwww�� ��wwwwwww�wwwww�� ��wwwwwww�wwwww�� ��wwwwwww�wwwww�� ��wwwwwww�wwwww�� ---------------_- 1111 - 111 ----- 333000 11 ----_- --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- -®-®-----®�----_- --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,®11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- 20.6 3870 - - 59.9 302 ----- ----- 21.8 2400 -----_- 26700 ----_- 9200 - 801 ----- 8390 1720 ----_- 1 1 llllllllllllllllllll, 1 1 llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111, 1 1 1 1 1 11111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- --------- 1 1 -----_- --------- 2.7 -----_- ---------------_- -------------_- -----®®----_- 2.1700 -------------_- ---------®-----_- -®llllllllllllllllllll,®11111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,®®11111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- -�llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- ---------------_- 6/10/2020 10 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date Units Concentration 2L pg/L MW-2R 111 MW-3R llllllllllllllll■ MW-4R 111 MW-5R llllllllllllllll■lllllllllllllll■llllllllllllllll■lllllllllllllll■llllllllllllllll■ MW-6R MW-7 MW-8 MW-9 MW-10 ' ' . 111 MW-11 111 MW-12 llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■lllllllllll■— MW-13 MW-14 MW-15 Trip Blank Equipment Blank _MW-1R Alkalinity, • TotalNE 11111 ./L 1111 . 11 . 1 . 1000 . 300 . 1 ... 11 ./L pg/L 1 . 2000 . 1 .111 . SM 1 — Total Dissolved . . SM 11 Chloride Field Field Specific Conductance Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX .. 300.0 EPA 6010 Cobalt • • - . • Manganese NickelNE Sodium:11 ' 8260 Acetone --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111,- --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- 796000 — 552000 ----- 1150000----_— 318000 11 ----_— --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,— --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,— ®—llllllllllllll<�111111111111111111111®11111111111111111111111111111111111�' lllllllllll�llllllllllllll'�111111111111111111111,111111111111111111111®llllllllllllll�....®®lllllllllllllll,— --llllllllllllllllllll,11111111111111111111111111111111111111111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,— 11.5 --------------�_� �— --®------------_ 89300 ——®---- 714 1740 _® 18.2 ®— 6460 --- 51.9 ©�-- 134 �� 359 _- —�— •11 — :11� 11 -- . 11 1111 .•11 .11 _- --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,111111111111111111111 1 1 111111111111111111111 1 1 1 1• ---------------_� ---- 4.4 --------- 5 _— ---------------_— 6/10/2020 11 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date 70 pg/L 70 pg/L 1000 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 2000 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 300 pg/L 15 pg/L i 0.4 Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichlorofluoromethane SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide Nmhos/cm Field Field Specific Conductance °C Field Field Temperature November-16 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX pg/L EPA 300.0 Sulfate EPA 6010 Arsenic Barium Beryllium Chromium Cobalt Iron Lead 0.38 1.1 7 1.5 3.6 1.2 0.46 0.61 32 11.4 12 0.91 1.4 1 0.75 2.1 68600 114000 32300 85000 20800 25400 64500 42400 55300 98100 165000 133000 156000 175000 67000 141000 288000 89000 130000 410000 8860 2520 15100 5290 3060 4610 19700 4310 3260 104000 4.4 4.4 9.9 4.3 209.7 392.9 175.5 2207. 68.1 159 367.4 116.5 173.7 690 20.3 20.4 21.2 19.7 17 19.8 17.4 16.9 18.4 17.6 68.82 16.64 2047. 17.87 22.26 36.41 34.35 104.13 24.2 8.77 10.74 18.41 103.03 39.3 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 1.52 1.18 2.9 3.5 5.73 1.2 7.7 8.26 1.16 4.39 1.34 4.6 4 3.19 0.72 1.51 5.3 7.03 0.31 0.25 0.31 4.61 6.38 5.81 2.97 7.23 1.95 44.5 5.6 6.2 6.3 6.1 5.9 5.6 5.7 5.5 6.2 6 5.9 5.7 5.6 6.4 137.2 24.1 -61.4 176.7 242.9 152 217.5 272 62.3 16.7 175.1 241.4 270.5 177.6 1380 121000 1530 193000 8450 3800 4090 17100 129000 5390 1400 58700 3.9 2.6 241 272 297 2551 55.9 140 44 195 148 93.1 144 91.6 188 14 0.58 0.57 2.8 1 5.8 4.1 6.4 96.2 •: :. � � � 3.5 11 214 149 2.6 NEW, Me 274 123 6/10/2020 12 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date 50 pg/L 100 pg/L 20 pg/L NE pg/L 0.3 pg/L 1000 pg/L 0.008 pg/L 0.004 pg/L 6 pg/L 6 pg/L NE pg/L 6000 pg/L 1 pg/L 700 pg/L 70 pg/L 3 pg/L 70 pg/L 1000 pg/L 600 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L 7.3 18.5 8 35.6 2.7 8.5 � 10.7 I 6.2 26.7 13.7 Manganese Nickel Selenium Sodium Vanadium Zinc EPA 8081 Heptachlor Heptachlor epoxide EPA 8260 1,1-Dichloroethane 1,4-Dichlorobenzene 4-Methyl-2-pentanone (MIBK) Acetone Benzene Carbon Disulfide Chloroform Chloromethane cis-1,2-Dichloroethene Dichlorodifluoromethane Ethylbenzene m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide pmhos/cm Field Field Specific Conductance °C Field Field Temperature June-16 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved 5 14600 70200 2450 71000 14200 16200 9700 15700 184000 12000 19200 9380 16200 20200 5.7 8.4 7.3 5.7 5.1 12.8 6.3 0.53 1.5 ]714.1 0.39 25.4 0.381 0.42 0.83 5.2 0.44 0.4 0.2 0.47 1.1 0.33 0.62 0.88 2.3 0.38 0.55 2.2 2.1 0.63 2.1 1 0.48 39.1 13.6 21.7 237 26.8 16.8 1.2 1.5 1 2.8 0.58 4.4 64300 571000 133000 454000 32700 80100 25800 23300 626000 107000 72900 42300 59700 101000 154000 � 168000 g.X4,111SUI 145000 153000 67000 135000 Ciffl 11OI 189000 286000 79000 118000 371000 9630 47600 2050 58400 16400 4820 2670 4360 202000 14500 23300 4100 3410 98000 5.4 202.8 1262 380.4 1204 176 203.1 73.7 167.8 2535 355 463.1 106.2 158.6 609.9 16.6 15.9 15 16 16.3 15.3 16.5 17.1 17.2 16.1 16.7 16.4 17.1 15.2 34.65 7.68 36.15 60 20 48 1.7 0.2 0.3 6/10/2020 13 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date 2L Units Concentration 3 pg/L 1111 . 1 ./L 1 ./L 11 . 1 . 100 . 1 ./L pg/L 2000 . 1 ./L 1000 . 40 ' • . 1 . MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank NTU Field Turbidity Std. Units Field Field pH mv Field REDOX • 8260 Methylene Chloride------ Field Field Specific Conductance Field Temperature feet Field Static Water- - - • 300.0 EPA 6010 Arsenic--®------®-----_- Chromium •.. Manganese SeleniumNE Sodium11 Vanadium EPA 7470 .. 8081 •- • 8260 ■ • - - ---------------_- 3.7Field --------_- �®' lllllllll�® 1 1 : 11111111111111111111111111111®'' lllllllll�llllllll�llllllllll�®llllllllllll`�n'lllllllllll®"' llllllll�lllllllll...��.11lllllllllllll,- ---------------_- 1:1 111 :11 •: 11�-��- :11 11 .•111 �- . 11 _- 4.7 -------------_- --11111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,®11111111111111111111111111111111111111111,®®111111111111111111111111111111111111,- - 18 10.2 10.5 ----- 3.1 -----_- 13.6 --_- 4360 77200 1550---� ------ 11800 19.1 29400 --�--_- 312 11000 312 ® 10900 6800 515 ®------®�®-_- 530 1820 90.8 284 116 . 11� 11 11 - .•11 ®' '1 11 1 11 11 11� 'II 1 11 ---------®--®--_� 4.2 4.2 ---- 20 -- 22.6 -----®--®--�-®_� --11111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,®11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- ---------------_- --llllllllllllllllllll,11111111111111111111111111111111111111111,111111111111111111111®11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- ---------------_- --llllllllllllllllllll,11111111111111111111111111111111111111111,111111111111111111111®11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- 1.7 ------------_- --IIIIIIIIIIIIIIIIIIII,IIIIIIIIIIIIIIIIIIII1llllllllllllllllllll,IIIIIIIIIIIIIIIIIIII1llllllllllllllllllll,IIIIIIIIIIIIIIIIIIII1llllllllllllllllllll,IIIIIIIIIIIIIIIIIIIII,IIIIIIIIIIIIIIIIIIII1llllllllllllllllllll,IIIIIIIIIIIIIIIIIIII1llllllllllllllllllll,IIIIIIIIIIIIIIII:QIlllllllllllllll,- 6/10/2020 14 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date Units Concentration 2L 111 . MW-1R --llllllllllllllll■lllllllllllllll■llllllllllllllll■lllllllllllllll■llllllllllllllll■lllllllllllllll■llllllllllllllll■lllllllllllllllll■lllllllllllllll■llllllllllllllll■lllllllllllllll■lllllllllllllll®' MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 lllllllllllllll■lllllllllll■- Trip Blank Equipment Blank Dichlorodifluoromethane 11 . 11 . 1 . 111 . 0.03 pg/L 11111 ./L 1111 . 1 . - - Chloride - - .. - - - • chloride •• -- SIM 1 : Alkalinity, • TotalNE SIM 1 Total Dissolved . . SM 11 Chloride SIM 1 1 CyanideField feet Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX Field Field Specific Conductance Field Field Temperature feet Field :. = DeFielpth Oxygen,NTU FieldTurbidity��©wwwwww�wwwww�� ® --------------_- 4.4 3.4 3.2 - 9.5 6 1.3 -------------_- -----®--®-®®_- 0.72 -------------_- ---------------_- �•11 111 :11 ••111 1:11 - 11:11 11 •111 1111 •11 111 1�11 1111 _- ---------------_- :111 769000 ::111 111111 - 111 111 1 111 111 .111 111 111 111 :111 _- --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- •111 11� :11 11 -�� 11 .111 �� •'lll _- --11111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,111111111111111111111----_- -®��---®-®®----_- --®1 "" ------------_- ■�w�■ww�w■��w■�www�� ®�ww®wwww�®wwww�� ®©w®wwwww�ww®ww�� 6/10/2020 15 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date Units Concentration 2L 1111 . 1 . 1 . 11 . 1 .Manganese• 11 . 1 . NE pg/L 1 2000 . 1 ./L 0.008 ./L 0.004 1 . .111 . 1 . .11 ./L 3 pg/L 11 . 17 pg/L .11 . MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Std. Units Field Field pH mv Field REDOX .. 300.0 .. 6010 Cobalt Copper . Sodium1 Vanadium EPA 1 .. 8081 Heptachlor Heptachlor epoxide • 8260 Acetone Ethylbenzene Methylene Chloride-®®--- o-Xylene-------------_- Tetrachloroethene Toluene ---------------_- 1 1 111 11 1 11 �- 1 11 �� • .11 11 1:11 1 11 1:1 1111 _- ---------------_- ------------®-®_- ---------®----®_- 17.4 9.1 28.3 2.5 ---- 3.1 2.9 ----_- 3080 682008200 31==== 3690 34600� 790 466 8180 = �_ 9010 7100 407 1890 -�®� ----� 587 2020 62.11 69.3 297 _- ---- ----- • ----_- 1 • 1 1 lllllllllll� : 1 1 1 1- 1 1 llllllllll� 1 1 •: 1 1 11 1 1 1lllllllllllllll,- ---------- 8.8 --------------_- 11.9 9.9- 3.7---- 5.6 3.5- 2.6- 18.9_- ---------------_- --11111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,®11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- ---------------_- 0.12 --------- 0.093 -----_- ---------------_- --------------_- --------------_- 1.5 -------------_- --------------�_- ---------®-----_- 3.9 --®-©---_® 0.95 -------------_- -------------_- 6/10/2020 16 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date 2000 pg/L 0.03 pg/L NE pg/L NE pg/L 200 pg/L 0.005 pg/L 100 pg/L 0.05 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L 250000 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 1 1.4 1.1 i 0.82 0.54 4.8 Trichlorofluoromethane Vinyl chloride _ EPA 8270 2,4-Dinitrotoluene 2,6-Dinitrotoluene Benzo(g,h,i)perylene Dibenz(a,h)anthracene Di-n-octylphthalate Indeno(1,2,3-cd)pyrene SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide Nmhos/cm Field Field Specific Conductance .0 Field Field Temperature May-15 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX pg/L EPA 300.0 Sulfate EPA 6010 Barium Beryllium Chromium Cobalt Copper Iron Lead 7 5.9 8.1 1 5.6 5.6 48100 440000 102000 144000 32300 67300 23200 23400 48200 127000 41000 37100 51500 103000 78000 .�.1 WM 131000 161000 104000 78000 79000 142000 403000 281000 234000 110000 135000 362000 8510 48700 2990 16900 16200 6050 2040 4710 47400 14900 9000 3270 3930 113000 7.5 5.1 4.7 9.8 4.2 5.3 5 5.3 163.2 1044 211.4 395.9 164.5 196.6 58.4 151.5 365.1 400.8 281.5 108.9 152.1 596.2 16 15.9 15.2 15.5 15.9 15.3 15.6 15.9 16.5 15.8 16.2 16.2 16.3 15.6 71.44 16.32 42.18 18.28 21.85 75.46 16.85 53.36 23.35 8.07 9.8 8.98 52.23 39.21 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 4.5 1.6 2 2.5 6.8 0.4 5.7 6.3 1.5 0.3 5.4 2.7 5.2 2 1.2 8.8 6.2 12.2 2.2 1.2 2.3 1.4 246.4 8 7.7 32.7 26.1 81.7 5.5 6.1 6.1 5.9 5.9 5.6 5.7 5.5 5.2 6 6 5.7 5.6 6.2 265.1 15.4 -1.1 262.81 244.4 228.8 255.2 206.8 244.7 -34.3 230.6 218.91 221.2 176 1700 98400 3000 72700 8000 1850 1860 2030 8770 15300 73600 9330 1790 65400 164 287 214 306 54 122 30 182 660 93.7 60.9 89.3 179 105 2.8 0.66 0.54 4.8 6.7 2.9 7.6 6.3 1 3.81 1 8.8 .0 3.31 2.71 2921 113 1 54 1 1 11.61 2.91 2.9 . 1 6.8 6/10/2020 17 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date 50 pg/L 100 pg/L NE pg/L 0.2 pg/L 0.3 pg/L 1000 pg/L 1 pg/L 50 pg/L 70 pg/L 6 pg/L 40 pg/L NE pg/L 1 pg/L 70 pg/L 3 pg/L 70 pg/L 600 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 600 pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L 500000 pg/L 250000 pg/L 17 • : 2.8 27.1 3.4 3.5 i 5.9 9.7 41.2 25.7 2.8 4.3 7 Manganese Nickel Sodium Thallium Vanadium Zinc EPA 7470 Mercury EPA 8151 2,4,5-TP (Silvex) 2,4-D EPA 8260 1,1-Dichloroethane 2-Hexanone 4-Methyl-2-pentanone (MIBK) Benzene Chloroform Chloromethane cis-1,2-Dichloroethene Ethylbenzene m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Toluene Trichloroethene Trichlorofluoromethane Vinyl chloride SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride Nmhos/cm Field Field Specific Conductance •C Field Field Temperature November-14 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field 11600 51400 23000 13100 16300 6940 14500 14100 9460 11200 10700 14500 20300 8.7 7.5 6.8 21.2 7.9 49 0.29 0.14 0.43 0.49 1.1 0.96 5.6 0.29 0.46 0.26 0.13 0.73 1 1.5 1.2 2.3 2.1 1.5 1.8 0.4 0.85 34.6 5.8 14.1 145 16.9 0.63 0.79 1.5 0.79 0.98 0.22 0.59 4.4 39600 358000 107000 117000 28600 64100 20000 18900 47300 132000 19200 36900 45200 91500 133000 EM 111 182000 304000 166000 145000 61000 134000 279000 239000 163000 107000 131000 360000 7640 44200 2990 22200 15700 4340 1960 4290 51800 14400 8070 3760 3510 98200 153.1 985 363.4 422 175.1 194.8 50.9 148.3 297.2 407.8 234.3 115 150.1 611 18 13.7 15 13.3 14.7 16.7 16.1 17.5 17.1 13.4 14.9 18.7 17.1 17.3 69.7 17.18 21.87 18.4 22.36 36.9 37.58 104.74 24.68 5.4 10.76 18.48 103.8 79 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 1 0.5 6.3 0.5 5 0.5 2.3 8.3 0.5 0.5 0.5 3.8 1.25 6/10/2020 18 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L NE pg/L 0.3 pg/L 1000 pg/L 1 pg/L 6 pg/L 6 pg/L NE pg/L 1 pg/L 3000 pg/L 70 pg/L 600 pg/L 500 pg/L 3 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L =I 1.7 NLTITYAI.� 3.53 M LY11291.0 5.2 I LIATZE I 1.M 10 M LTIT9611.0 3.6 I JAYA-Mm LTATAY� 1.2 I LIATE*-� 9.1 JILTITZIM 2 I JAY5 i 98 9.9 5.2 152 7.8 20.1 Turbidity Std. Units Field Field pH mV Field REDOX pg/L EPA 300.0 Sulfate EPA 6010 Arsenic Barium Beryllium Chromium Cobalt Copper Iron Lead Manganese Nickel Sodium Vanadium Zinc EPA 7470 Mercury EPA 8260 1,1-Dichloroethane 1,4-Dichlorobenzene 4-Methyl-2-pentanone (MIBK) Benzene Chloroethane cis-1,2-Dichloroethene Ethylbenzene m&p-Xylene Methylene Chloride o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide SM 4500-S2D 7 5.6 6.1 6 5.9 6 5.6 5.7 5.5 5.1 5.9 5.9 5.6 5.6 6.2 194 38 13 158 198 184 224 252 198 -61 101 232 242 182 1720 117000 3740 143000 8180 1360 2100 12800 32800 8660 43800 2.6 3.5 142 339 221 305 58.2 111 38 193 262 96.8 59.2 130 193 41.5 1.4 1.2 0.6 3.4 4.8 3 4.5 9.6 3.8 4.8 85.8 1 2.7 126 221 76.5 55.9 .1 4.1 233 2.9 •:: 2.6 22.9 19.9 7.6 1 33 25.9 7.2 4.1 5.3 10600 58300 2770 55400 13700 16600 7810 14600 6860 10000 12800 10700 14400 24000 16.8 7.2 5.3 6.2 13.7 13.3 5.3 0.33 1.1 1.3 0.4 2.2 0.42 0.44 2.1 0.5 0.73 0.35 0.73 1.1 1.1 0.33 2.9 0.36 0.65 79.2 15.9 8.8 106 15.5 0.85 2.4 1.2 0.96 0.57 3.9 37600 453000 177000 286000 24000 62400 22800 18300 42200 143000 40500 36200 42300 54700 120000 . 111 191000 gWA1el 163000 138000 64000 141000 86000 228000 135000 119000 119000 464000 7090 49800 2940 50500 15500 4300 1350 3610 2220 15000 8240 5870 3720 146000 4.41 4.21 10.4 4.3 5.1 6/10/2020 19 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date Concentration 2L Units NE pg/L 1111 . 1 ./L 1 . 11 . 1 .Manganese 11 . NE pg/L 1000 . 1 ./L 1 ./L 11 . 1 . MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Sulfide Field Field Specific Conductance Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX EPA 300.0 .. 6010 Arsenic--------------_- Cobalt - Sodium EPA 1 EPA .1 Chloroform--------------�_- cis- 1,2-Dichloroethene Chloride . - - .. - - - ---------------_- _- ---------------_- 5.4 -------------_- ----®----------_- 22.8 1650 - 38200 46.6 -----------_- ®----- 33400 348 -� 79501 9260 llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- 1960 1: 1 1 • 1 1 llllllllllllllllllll, ' 1 1 . 1 1 111111111111111111111 1 1 lllllllllll....... ' 1 1 lllllllllllllllllllll,llllllllll� 1 1 1 1 1 : 1 1 1 1 ----®-------®®-_- --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- 1.8 ------------_- -�llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111�11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- -�llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- 3.7 -------------®- 1.8 -------------_- 6/10/2020 20 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date 2000 pg/L NE pg/L 500000 pg/L 250000 pg/L 250000 pg/L 700 pg/L 1 pg/L 300 pg/L 50 pg/L 100 pg/L NE pg/L 0.3 pg/L 1000 pg/L 50 pg/L 70 pg/L 6 pg/L 1 pg/L 70 pg/L 70 pg/L 1000 pg/L 3.7 0.62 0.47 i 0.2 0.32 0.34 5.3 Trichlorofluoromethane SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride Nmhos/cm Field Field Specific Conductance °C Field Field Temperature November-13 feet Field Static Water Level Total Well Depth mg/1 Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX pg/L EPA 300.0 Sulfate EPA 6010 Barium Cobalt Iron Manganese Nickel Sodium Vanadium Zinc EPA 8151 2,4,5-TP (Silvex) 2,4-D EPA 8260 1,1-Dichloroethane Benzene Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane 30000 344000 155000 222000 31900 51900 21300 18300 31400 175000 45500 46400 37400 96600 91000 � 187000 445000 167000 126000 50000 107000 63000 207000 149000 113000 124000 373000 5600 50500 3260 29700 13900 3600 1800 3610 1820 12400 6180 3880 3630 83400 137 1040 367 715 194 171 64 155 86 430 243 149 156 623 18.4 19.6 18.7 14.8 14.7 17.2 16 17.7 15 14.4 15 16.6 17.7 17.8 71.87 16.65 45.08 18.63 22.73 76.44 36.08 106.03 24.77 9.1 10.56 18.83 104.66 79.28 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 8.7 0.9 0.7 7.5 5.6 0.5 10.2 9.2 2.2 0.5 6.5 1.3 6.5 2.8 1 3 1 12 3 2 5 11 4 8 9 123 250 21 5.6 5.6 5.9 5.8 5.9 5.5 5.4 5.2 5.2 5.9 5.8 5.4 5.4 6.2 228 68 -8 207 239 200 357 363 327 -66 189 280 355 241 128000 3400 113000 8310 10400 27400 9360 53200 106 311 201 296 53.9 98.8 25.4 170 112 87.8 47.6 106 140 23.8 6 89.5 136 136 84.3 11 253 1 239 1 27.1 • • • 1 5.3 19.4 6.8 6.9 7.9 1 48.8 1 14 9940 46200 42600 13800 13000 5580 13500 9070 10500 11700 12300 25300 12.2 17.1 0.23 1.1 1.3 0.9 0.27 0.77 0.41 0.54 0.28 6/10/2020 21 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date 3 pg/L 6 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L 2000 pg/L 0.03 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L 250000 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L i Methylene Chloride Naphthalene o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Vinyl chloride SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide pmhos/cm Field Field Specific Conductance .0 Field Field Temperature May-13 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX pg/L EPA 300.0 Sulfate EPA 6010 Barium Beryllium Chromium Cobalt Copper Iron Lead Manganese 0.86 0.54 99.6 11.7 13.7 5 14.7 0.89 121 0.47 0.69 0.33 7.6 1 28100 349000 155000 224000 31700 51600 19700 18400 26700 161000 39300 43200 32800 64300 103000 ow 193000 496000 154000 116000 61000 124000 66000 236000 126000 114000 123000 410000 5880 56700 3620 36500 15200 5160 1510 3950 1790 14000 6230 5700 4100 124000 7.1 5.9 6 5.2 104 840 316 678 168 144 48 138 63 385 153 115 123 614 18.3 13.8 15.9 17.2 17.4 16.5 15.1 16.3 16.7 16.7 17.1 14.8 16.7 17 73 15.54 21.94 17.53 21.44 38.62 31.43 106.24 23.65 8.13 9.59 17.62 104.48 78.61 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 8.3 1.9 6 2.7 7.1 0.9 7.2 7.4 3.1 6.4 9.3 1.3 6.4 2.5 1 1 1 36 1 1 1 44 1 6 5 587 446 190 5.6 5.81 5.8 5.6 6 5.3 5.51 5 5.2 6.21 5.8 5.6 5.5 6.1 263 10 21 246 274 211 260 282 267 -22 185 204 254 224 115000 5070 97600 11200 2100 3200 11000 51800 7820 41200 009 324 216 375 57.7 115 28.5 174 115 87 50.1 176 254 59.6 2.4 7.1 6.6 7.6 9.5 �1 158 126 61.5 92.8 . 1 • 6.5 =1 2 1 . 1 • . 1 24.9 16.6 M.1 13.2 .1 6/10/2020 22 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date 100 pg/L NE pg/L 2000 pg/L 0.3 pg/L 1000 pg/L 6 pg/L 40 pg/L 6000 pg/L 1 pg/L 70 pg/L 70 pg/L 500 pg/L 3 pg/L 6 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L 2000 pg/L 500 pg/L NE pg/L 500000 pg/L 250000 pg/L 70 pg/L 20.7 8.6 Nickel Sodium Tin Vanadium Zinc EPA 8260 1,1-Dichloroethane 2-Hexanone Acetone Benzene Chloroform cis-1,2-Dichloroethene m&p-Xylene Methylene Chloride Naphthalene o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Xylenes (Total) SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E Cyanide pmhos/cm Field Field Specific Conductance •C Field Field Temperature November-12 feet Field Static Water Level Total Well Depth mg/1 Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field 9080 45700 42600 13000 14300 6120 12900 8290 11100 19100 13500 26700 77 5.8 21.1 10.5 13.6 37.3 27.4 22.7 1.2 0.84 0.48 20.3 0.63 0.26 0.72 0.96 ..3 0.54 0.27 111 8.5 24.2 7.4 0.68 12.1 0.25 0.36 0.38 4.3 1.2 29800 363000 175000 203000 34800 63500 22800 21700 32100 189000 29600 58700 35600 78900 84000 •101 175000 413000 131000 108000 51000 100000 46000 228000 138000 87000 102000 442000 5910 50000 3860 33700 16200 5340 2070 4300 2040 14200 5820 3820 4290 124000 8.1 5 68 802 217 382 116 106 31 88 43 400 197 136 81 403 20.9 19.7 15.7 15.6 15.2 16.3 17.5 18.1 16.3 14.7 14.7 16.5 18.2 17.9 72.24 17.78 45.36 19.26 22.81 77.49 37.56 105.53 25.13 8.94 10.71 18.71 104.68 79.91 60 21 27 20 30 48 27 60 21 20 15.58 20 60 50.85 5.5 1.5 1.2 2.3 6.4 1.8 9.8 7.3 4.4 0.9 3 2.3 6.4 2.3 1 1 25 14 14 7 1 1 1 25 1 605 329 456 5.7 5.8 5.6 5.7 5.8 5.4 5.7 5.5 5 6.1 5.9 5.51 5.5 6.5 6/10/2020 23 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date 250000 pg/L 10 pg/L 700 pg/L 4 pg/L 10 pg/L 1 pg/L 1000 pg/L 300 pg/L 15 pg/L 50 pg/L 100 pg/L NE pg/L 0.3 pg/L 1000 Ng/L 0.1 pg/L 0.002 pg/L 42 pg/L 2 pg/L 2 pg/L 0.004 pg/L 6 pg/L 1 pg/L 3000 pg/L 70 pg/L 70 pg/L 1000 pg/L 3 pg/L 6 pg/L 500 pg/L 0.7 pg/L NE pg/L 3 pg/L 2000 pg/L 500 pg/L 0.05 pg/L 3 pg/L 5 pg/L NE pg/L 500000 pg/L 250000 pg/L 236 77 16 181 245 197 260 352 i 366 -61 150 246 365 160 REDOX pg/L EPA 300.0 Sulfate EPA 6010 Arsenic Barium Beryllium Chromium Cobalt Copper Iron Lead Manganese Nickel Sodium Vanadium Zinc EPA 8081 4,4'-DDD Dieldrin Endosulfan II Endrin Endrin aldehyde Heptachlor epoxide EPA 8260 1,1-Dichloroethane Benzene Chloroethane Chloroform cis-1,2-Dichloroethene Dichlorodifluoromethane Methylene Chloride Naphthalene o-Xylene Tetrachloroethene Tetrahydrofuran Trichloroethene Trichlorofluoromethane Xylenes (Total) EPA 8270 Benzo(a)anthracene bis(2-Ethylhexyl)phthalate Chrysene SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride SM 4500-CN-E 7 79500 5420 73600 8400 2090 10400 24200 9770 35600 7.1 91.7 335 173 40C 53.4 95.1 26.9 142 101 76.8 50.5 279 160 143 3.5 6 6.7 6.9 5.8 10.5 i 102 60.8 218 411 I 7.5 I 11 9.5 21.8 .0 17.4 5.1 33.6 13.7 9180 43400 43600 14500 13900 6980 13100 5280 8770 11000 14600 15000 21200 24.5 15.2 92 30.8 51 23 45.6 0.062 1 0.12 0.27 0.23 1.2 1.2 1.3 0.16 0.49 0.25 0.62 0.28 1.6 0.63 93.2 13.5 26 6.3 0.77 16.9 0.29 0.49 0.49 8.1 0.98 0.79 2.4 1.5 1.1 1 26300 277000 142000 174000 31200 51900 19500 17200 25500 153000 40200 43900 28900 77600 95000 . 111 172000 435000 157000 111000 58000 118000 63000 220000 127000 144000 127000 298000 5320 64000 39201 345001 16100 3810 1860 3560 1800 12900 4900 6150 4790 143000 6/10/2020 24 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date Units Concentration 2L 1 . pg/L 1111 . 1 . 11 . 11 . 1 . 100 . 1 ./L pg/L 1 1000 . 1 . 1.1 pg/L 0.002 ./L 0.006 . 0.019 MW-1R --®lllllllllllllll■llllllllllllllll■lllllllllllllll■llllllllllllllll■lllllllllllllll■llllllllllllllll■lllllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■llllllllllllllll■lllllllllll■- MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Cyanide SM 11 ■ SulfideNE Field Field Specific Conductance Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX ' 300.0 .. 6010 Cobalt14.81 Manganese SilverNE Sodium_- EPA 8081 - ■ ■ ■ 4,4'-DDT Aldrin - ------------�- 1 1 _- ---------------_- 111 ®" '1 •: 11�----- 11 1 11 �- :11 _- ---------------_- --------------®_- 16.4 21.5 -----------_- 3190 41500--�-® 26300 539 3760 1140 10000 _- -®-----------®-_- 8280 9310 370 --�--- 1580 ® 91.5 170, 327 ------------ 7.2 - 23.4 -®----------�-®_- ---------------_- ------ 0.13 --------_- 0.54 - 0.14 ------ 1 1 0.12 0.12 -------------_- 0.18 - 0.069 -----------_- 6/10/2020 25 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date Units Concentration 2L 0.008 ./L 0.004 ./L 1 . 11 . 1 ./L 111 . 11 . 0.005 . 11 . 0.005 . 0.05 ./L pg/L 11111 .TotalDissolved 1111 ./L pg/L MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Heptachlor Heptachlor epoxide • • 8260 Chloride3.2 Naphthalene o-Xylene-------------_- Tetrachloroethene . . . . - - - -• • 1 - - - - - - - ■ . - - - lndeno(1,2,3-cd)pyrene----------- SIM 1 : Alkalinity, • TotalNE SIM • 1 • . SM 11 Chloride_- SIM 11 SIM 411 ■NE Sulfide Field Field Specific Conductance Field Field Temperature 1 feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field 0.48 ------ 0.066 --------_- -------------_- ---------------_- 1.5 -------------_- -------------_- 1.7 -------------_- ------------®_- -------------_- ---------------_- ------------ 1.1 --_- ----------®®®--_- -- 5.5 ------------ 1.2 1.2 1.5 --_- ---------------_- 11 •.111 1111 . 11 111 - 1 11 1 11 1 11 111 1111 11 11 1 11 11 _- ---------------_- 111 531000 .:111 •111 ••111 - 1.111 111 111 ••111 111 1111 1111 111 .1111 _- --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- ---� _---------_� 6/10/2020 26 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date 250000 pg/L 700 pg/L 10 pg/L 1 pg/L 300 pg/L 50 pg/L NE pg/L 0.3 pg/L 1000 pg/L NE pg/L 500000 pg/L 250000 pg/L 250000 pg/L 2 40 90 i Turbidity Std. Units Field Field pH mV Field REDOX pg/L EPA 300.0 Sulfate EPA 6010 Barium Chromium Cobalt Iron Manganese Sodium Vanadium Zinc SM 2320B Alkalinity, Total as CaCO3 SM 2540C Total Dissolved Solids SM 4500-CI-E Chloride Nmhos/cm Field Field Specific Conductance °C Field Field Temperature November-11feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mV Field REDOX pg/L EPA 300.0 Sulfate 7 5.8 5.9 5.7 218 175 200 61800 7020 82.6 328 85.2 15 7670 35300 43.5 13300 15.3 27500 143000 32800 95000 345000 139000 16400 97 177 r 15.4 15.2 36.52 16.58 44.06 11.1 77.6 17.03 52.19 12.24 7.38 9.19 17.83 52.08 21 27 48 27 60 21 20 15.58 20 60 1.7 3.1 4 5.8 6.8 4.5 0.6 2 6.9 6.2 1 4 3 4 1 2 37 54 223 154 5.9 6 5.8 5.6 5.6 5.6 6.3 6 5.9 5.8 95 71 207 206 205 223 -148 216 239 218 96300 7590 15300 9460 6/10/2020 27 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date Units Concentration 2L 1 . 111 .Copper--------- 11 . 1 .Manganese 11 . NE pg/L 1 ./L 1000 . .111 . • 1 . 11 . 11 . 1 . NE pg/L 11111 •Total MW-1R --llllllllllllllll■lllllllllllllll■llllllllllllllll■lllllllllllllll■llllllllllllllll■lllllllllllllll■llllllllllllllll■lllllllllllllllll■lllllllllllllll■llllllllllllllll■lllllllllllllll■llllllllllllllll■lllllllllllllll■lllllllllll■- MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank .. 6010 Cobalt-_- . - Sodium Vanadium • 8260 11,11-Dichloroethane Acetone - - Chloride . - - .. - - - 1• • romethane SM . Alkalinity, • SM 1 ■ - • SM 11 Field Specific Conductance Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity ------------® 11.8 ---------- -_- • -_- 2980 40300 ----®- 424 23000 3030 614 22050 -_- 7920 7310 ---®�-� 1250 58.3 140 71 -_- -------------_- : 11 llllllllllllllllllll,11111111111111111111111111111111111111111,111111111111111111111 111 lllllllllll.�a... 11 lllllllllllllllllllll,lllllllllllllllllllll.r.•'.' 1 11 11 111111111111111111111111111111111111,- 10.8 -®-----®----�®-_- ---------------_- -®llllllllllllllllllll,11111111111111111111111111111111111111111,111111111111111111111®11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- -®-------------�® 2 -------------_- -------------_- -®-------------_- 3.5 -------------_ 3.2 1.8 -------------_- ---------------_- '111 11111111111111111111111111111111111111111111,111111111111111111111 11 •.11 •11 11 111 •1 11 " 11 1. 11111111111111111111111111111111111111,- ---------------_- '':111 :1111-11111111111111111111,111111111111111111111 'lll 111 :111 :•111 111 •111 •111 :111111111111111111111111111111111111111,- ---------------_Field - 6/10/2020 28 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date INS pg/L NE pg/L 1 pg/L 0.7 pg/L NE pg/L NS pg/L NE pg/L 250000 pg/L 700 pg/L 10 pg/L 20 pg/L 200 pg/L =I M VITYA.� M L111291 .0 1 M VITZE I M L'I'M Za I JAIIIII-I M klklfr� I JAIAI-� M kT&I= I M L1115 i Std. Units _Field Field pH my Field REDOX pg/L EPA 350.1 Nitrogen, Ammonia EPA 6010 Sodium EPA 8260 Benzene Tetrachloroethene Tetrahydrofuran RSK 175 Methane SM 2320B Alkalinity, Total as CaCO3 SM 4500-CI-E Chloride Nmhos/cm Field Field Specific Conductance °C Field Field Temperature May-11 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX pg/L EPA 6010 Barium Chromium Silver EPA 8260 1,1,1-Trichloroethane 5.8 88 0.12 27200 274 1280 165000 39900 698 19.1 35.93 8.17 20.56 8.34 10.44 37.99 15.08 51.11 11.72 4 4.91 8.85 51.45 60 21 27 20 19.56 48 27 60 21 20 15.58 20 60 6.3 3.9 6.3 5.3 9 3.2 8.7 7.3 7.1 4.3 7.4 5.2 7.8 55 57 70 96 85 40 18 1 4 23 25 177 39 5.8 5.9 6.2 5.7 6.1 5.6 5.1 5.6 5.5 6.2 6 5.6 5.5 263 71 43 271 141 245 272 265 279 -36 188 245 272 84.7 273 301 126 63.7 104 27.3 153 80.7 56.2 39.1 164 125 1.4 5.4 1.3 7.6 0.96 0.63 2.6 3.9 1.8 0.51 2.5 0.6 0.88 0.57 0.84 0.1 0.43 0.12 1.2 0.7 0.72 0.74 0.82 6/10/2020 29 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date Units Concentration 2L .111 . 1 . 3 pg/L 11 . 1 ./L 1 ./L 3 pg/L MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Acetone Methylene Chloride o-Xylene------------_- Tetrachloroethene Field Field Specific Conductance Field Temperature November-10feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field TurbidityStd. Units Field Field pH mv Field REDOX .. 6010 Silver-®�---------_- EPA .1 Methylene Chloride Field Field Specific Conductance Field Field Temperature --------------_- 1.3 -------------_- -------------_- 4.1 -------------_- 1.4Field -------------_- ©�' IIIIIIIIIIIIIIIImlllllllllllllllliiL©111111111111111111111®llllllllllllllllllll�llllllllllllllllllll�llllllllllllllll�llllllllllllllllmllllllllllllllllllll� 11 llllllllllllllllmllllllllllllllllllll1111111111111111,- ---------------_- ---------------_- 4.2 -------------_- 6/10/2020 30 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date 2000 pg/L 10 pg/L 700 pg/L 2 pg/L 10 pg/L 20 pg/L I M LIITYA.� M 1,111291.0 1 M LITZE I.M M LIM-1.0 I M VAII-I M tu, J, ILT&JIIIIIIIIIIIIIII I jj 11115 i April-10 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX pg/L EPA 8260 Trichlorofluoromethane Nmhos/cm Field Field Specific Conductance °C Field Field Temperature March-10 feet Field Static Water Level Total Well Depth mg/I Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH my Field REDOX pg/L EPA 6010 Arsenic Barium Cadmium Chromium Silver EPA 8260 7 7.15 21 2.7 2 5.46 -7 21.9 255 14.3 36.62 7.16 18.22 8.22 9.99 38.71 13.23 51.31 11.18 3.55 4.15 8.05 51.21 60 21 27 20 30 48 27 60 21 20 15.58 20 60 5.9 4.8 3.7 4.4 6.1 2.2 7.2 8.5 7.4 1.9 6.8 5.4 7.9 2 4 6 45 3 2 7 6 2 13 31 11 29 5.74 5.31 5.61 5.56 5.96 5.55 5.21 5.32 5.18 5.97 5.73 5.5 5.35 262 191 31 262 260 213 303 309 300 -60 197 237 292 4 4.2 3.4 2.7 85.3 103 314 55.9 54.3 99.3 28.8 134 46.6 37.6 40.6 126 130 0.82 1.4 1.2 1.3 5 1.4 2.4 1.7 3 0.29 0.67 0.45 0.46 0.56 0.27 0.481 0.2 0.4 0.39 6/10/2020 31 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date Concentration 21 Units 2000 . MW-1R -®-------------_- MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank .. .. Field Field Specific Conductance Field Field Temperature November-09feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX Field Field Specific Conductance Field Field Temperature ' " Field Static Water Level Total Well Depth Field Oxygen, Dissolved NTU Field Turbidity Std. Units Field Field pH mv Field REDOX .. 6010 ----_-------_-®-7-_- � �� ��r m--� � mrfeet 1-_- ---------------_- 6/10/2020 32 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date Units Concentration 2L pg/L 1 •/L pg/L MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank ' 8260700 Carbon Disulfide Methylene _Field SpecificField FieldField Temperature 'feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved Std. Units Field Field pH mv Field REDOX EPA 6010 Silver-��-------_- ' 8260700 Carbon Disulfide Field Field Specific Conductance Field Field Temperature 1 feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved Std. Units Field Field pH ---------------_- --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111111111111111111111111,111111111111111111111®- --11111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- ��llllllllllllll�" --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- ---------------_- ---------------_- 6/10/2020 33 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date Units Concentration 2L 1 ./L 1 ./L 1 •/L 1 ./L MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank mv Field REDOX .. 6010 Arsenic-------------®-_- Selenium-------------_- ' 8260 ChloroformField Field_ConductanceField Temperature Field March-i:-llllllllllllllllllll,11111111111111111111111111111111111111111,1111111111111111111111111111111111�1111111111111111111111111��11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- .. Field Static Water Level Total Well Depth Field Oxygen, Dissolved Std. Units Field Field pH mv Field REDOX .. 6010 Selenium--®------------_- EPA 1 ' 8260 Field Field Specific Conductance Field Field Temperature ---------------_- ------------- 26.2 -_- ---------------_- -®-------------_- --11111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- ��llllllllllllll�" llllllllllllll�llllllllllllll�' 111111111111111111111®®®®®IIIIIIIIIIIIIIIW' llllllllllllllll�®111111111111111111111111111111111111,- --11111111111111111111,11111111111111111111111111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,11111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111,111111111111111,- --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111,111111111111111,- ®®llllllllllllllllmllllllllllllllllmllllllllllllllllllll1IIIIIIIIIIIIIIIIIiL®llllllllllllllllm®llllllllllllllllmlllllllll®'llllllllllllllllmllllllllllllllllmllllllllllllllllllll1111111111111111,- --11111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- --11111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- ��lllllllllll®' 11' lllllllllll®' lllllllllll®' ' 111111111111111111111111111111111111111111111�111111111111�" llllllllllll®' ®®lllllllllll�llllllllllll`w '+' 111111111111111111111111111111111111,- --11111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- --11111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- ---------------_- ---------------_- ---------------_- 6/10/2020 34 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date Units Concentration 2L 1 . 1 . 4 111 . 11 . 1 . MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank feet Fiel Static Water Level Total Well Depth Field Oxygen, Dissolved Std. Units Field Field pH mv Field REDOX - Field Field Specific Conductance Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved Std. Units Field Field pH mv Field REDOX • - Field Field Specific Conductance --11111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111 1 1 �' 111111111111111111111111111111111111,- --®------------_- -------��-��-®-_- ---------------_� --11111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111®111111111111111111111111111111111111,- -- 24 ------------_- 6/10/2020 35 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date Units Concentration 2L r . r r r r . MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Field Field Temperature feet Field Static Water Level Total Well Depth Field Oxygen, Dissolved Std. Units Field Field pH mv Field REDOX Barium Cadmium-- Field Field Specific Conductance Field Field Temperature November-05 EPA 6010 EPA 7470 EPA 8260 Chloromethane -------------�-■- 2 ------------■- ------------ 35 -■- ------------- 23 -■- 15 �■ ��7���■ I� 1�■i 5.4 ----------■- --------------■- ®--------------■- 6/10/2020 36 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date Units Concentration 2L 1 ./L 10 pg/L . 1 ./L 11pg/L 1 ./L 1 . 1 ./L 11 . 1 . 11 . 1 ./L MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Arsenic----®----------_- Chromium •IL (blank)700 Chromium . Barium Chromium • pgIL Chromium Chromium 14 --llllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,11111111111111111111111111111111111-�a..11lllllllllllllllmlllllllllllllllli�lllllllllllllllllli711111111111111�.....11llllllllllllWJllllllllllllllllllll1111111111111111,- 14 13 ®llllllllllllll,...11lllllllllll�lllllllllllllllll�' llllllllllllllllmllllllllllllll�.....11lllllllllllir.a••'llllllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- 14 18 ®® ®-- 26 28 41 -------_- -------_- 150 ®-------_- 22 ----- 24 -------__- ��S ---- 2.7 ----------_- 17 -------_- ---®--®�JJ------__- 11®llllllllllllllll®" llllllllllllllllm' lllllllllllllllli�llllllllllllll�...11lllllllllllllliiLllllllllllllllllllll,lllllllllllllllllllll,11111111111111111111111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- --®------------_- 1l llllllllllllll.....11llllllllllllllm' llllllllllllll�n...11llllllllllll�.....11llllllllllllllmllllllllllllll�n�..11llllllllllllllllll,lllllllllllllllllllll,llllllllllllllllllll111111111111111111111,11111111111111111111111111111111111111111,111111111111111111111111111111111111,- 23 26 23 -------_- -- 21 -----------_- 6/10/2020 37 of 39 A4 Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) I Historical detections by date 2L Units i pg/L r r r 00 pg/L r pg/L r 00 10 pg/L r r . r 0 r . r 3 pg/L 6000 r . r pg/L 1 . Concentration MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Arsenic pgIL Barium Chromium Chromium Methylene Chloride Carbon Disulfide 16 17 36 ------_- ------_- ------_- ®: r 22 16 900 19 95 35 36 � 140 ® 95 38 1300 2700 270 94 36 150 ------_- -- 18-- 16 46 ------_- ------_- 950 50 38 53 49 1300 210I 26 2600 92 210-------_- ------_- -- �� 31 -©- 41500�lllllllllllllllllllll�ll 82 45 89 2600 4200r 580--�- 65 400-------_- ------_- --®®-----------_- ® 14 24 40 860 60 40-®--------_- 29 ��--------_- 62 --------_- --------------_- ®i --- 13 ®i 13 - - 950 110 50 10 38 16 10 - 960 190 30 10 --------_- -------_- -------_- -------_- --------------_- 11 -------------_- 1100 1400 2000 1300700 --------_- 12 210 68 77 39 300 76 96 29 12 - 350 36 --------_- --------_- 6/10/2020 38 of 39 A4 1 pg/L 10 pg/L 700 pg/L 10 pg/L 15 pg/L 700 pg/L 10 pg/L 15 pg/L 1 pg/L 700 pg/L 2 pg/L 10 pg/L 15 pg/L 20 pg/L 700 pg/L 10 pg/L 15 pg/L 1 pg/L 4000 pg/L 700 pg/L 2 pg/L 700 pg/L 10 pg/L 15 pg/L 1 pg/L Facility Permit 34-12 Old Salisbury Road Landfill (C&D) Qualifier (Multiple items) Historical detections by date ration Concent MW-1R MW-2R MW-3R MW-4R MW-5R MW-6R MW-7 MW-8 MW-9 MW-10 MW-11 MW-12 MW-13 MW-14 MW-15 Trip Blank Equipment Blank Arsenic BariumMercury Chromium49 Lead- ��� 34 19 860 25 32 850 130 43 820� 170 69 33 20 1200 430 38 --------_- --------_- --------_- • Barium������ Chromium11 Lead® 43 31 16 26 55 29 16 31 14 1800 410 53Mercury -------_- -------_- -------_- Barium Cadmium 3 800 ----- ®.'r ®iM 750 -------_- -------_- romium Lead 28 27 - 70 21 180 23Silver -------_- -------_- Barium®. Chromium Lead r 790 20 15 720 47 16 43 20Mercury 10 ��--------_- 970 21 --------_- Barium Cadmium--- 1230� 7Carbon 1000 - 1400 1930--------_- --------_- Disulfide M Chromium Lead Mercury - 1.8 12 26 �� 15 21 17 1.7 96 19 ®i . 12 28 18 17 1.4 1.4 -------_- -------_- -------_- 6/10/2020 39 of 39 This page intentionally left blank. Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix B — Laboratory Reports Appendix Laboratory Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix B — Laboratory Reports This page intentionally left blank. leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 June 09, 2020 Mark Filardi HDR 440 S. Church St Suite 900 Charlotte, NC 28202 RE: Project: OSR LANDFILL GW Pace Project No.: 92477011 Dear Mark Filardi: Enclosed are the analytical results for sample(s) received by the laboratory on May 08, 2020. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace National - Mt. Juliet • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Herring kevin.herring@pacelabs.com 1(704)875-9092 HORIZON Database Administrator Enclosures cc: Charles Gruenberg REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 155 lacieAnalyfica(' www,pacelabs.com Pace Analytical Services, LLC 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: OSR LANDFILL GW Pace Project No.: 92477011 Pace Analytical Services National 12065 Lebanon Road, Mt. Juliet, TN 37122 Alabama Certification #: 40660 Alaska Certification 17-026 Arizona Certification #: AZ0612 Arkansas Certification #: 88-0469 California Certification #: 2932 Canada Certification #: 1461.01 Colorado Certification #: TN00003 Connecticut Certification #: PH-0197 DOD Certification: #1461.01 EPA# TN00003 Florida Certification #: E87487 Georgia DW Certification #: 923 Georgia Certification: NELAP Idaho Certification #: TN00003 Illinois Certification #: 200008 Indiana Certification #: C-TN-01 Iowa Certification #: 364 Kansas Certification #: E-10277 Kentucky UST Certification #: 16 Kentucky Certification #: 90010 Louisiana Certification #: A130792 Louisiana DW Certification #: LA180010 Maine Certification #: TN0002 Maryland Certification #: 324 Massachusetts Certification #: M-TNO03 Michigan Certification #: 9958 Minnesota Certification #: 047-999-395 Mississippi Certification #: TN00003 Missouri Certification #: 340 Montana Certification M CERT0086 Nebraska Certification #: NE-OS-15-05 Pace Analytical Services Charlotte 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 Louisiana/NELAP Certification # LA170028 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 CERTIFICATIONS Nevada Certification #: TN-03-2002-34 New Hampshire Certification #: 2975 New Jersey Certification #: TNO02 New Mexico DW Certification New York Certification #: 11742 North Carolina Aquatic Toxicity Certification #: 41 North Carolina Drinking Water Certification #: 21704 North Carolina Environmental Certificate #: 375 North Dakota Certification #: R-140 Ohio VAP Certification #: CL0069 Oklahoma Certification #: 9915 Oregon Certification #: TN200002 Pennsylvania Certification #: 68-02979 Rhode Island Certification #: LA000356 South Carolina Certification #: 84004 South Dakota Certification Tennessee DW/Chem/Micro Certification #: 2006 Texas Mold Certification #: LAB0152 Texas Certification #: T 104704245-17-14 USDA Soil Permit #: P330-15-00234 Utah Certification #: TN00003 Vermont Dept. of Health: ID# VT-2006 Virginia Certification #: VT2006 Virginia Certification #: 460132 Washington Certification #: C847 West Virginia Certification #: 233 Wisconsin Certification #: 9980939910 Wyoming UST Certification #: via A21-A 2926.01 A21-A-ISO 17025 Certification #: 1461.01 A21-A-ISO 17025 Certification #: 1461.02 AIHA-LAP/LLC EMLAP Certification #:100789 South Carolina Certification #: 99006001 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: OSR LANDFILL GW Pace Project No.: 92477011 Lab ID Sample ID Matrix Date Collected Date Received 92477011001 MW-8 Water 05/04/2014:30 05/08/20 17:07 92477011002 MW-9 Water 05/05/20 08:45 05/08/20 17:07 92477011003 MW-14 Water 05/05/2010:25 05/08/20 17:07 92477011004 SW-3 Water 05/05/2015:25 05/08/20 17:07 92477011005 MW-11 Water 05/06/20 09:25 05/08/20 17:07 92477011006 MW-12 Water 05/06/2011:25 05/08/20 17:07 92477011007 MW-13 Water 05/06/2012:55 05/08/20 17:07 92477011008 MW-5R Water 05/07/2014:20 05/08/20 17:07 92477011009 SW-4 Water 05/08/2013:15 05/08/20 17:07 92477011010 SW-1 Water 05/08/2013:50 05/08/20 17:07 92477011011 TRIP BLANK Water 05/08/20 00:00 05/08/20 17:07 92477008001 MWA R Water 05/06/20 14:15 05/08/20 17:07 92477008002 FIELD BLANK Water 05/06/20 15:08 05/08/20 17:07 92477008003 MW-4R Water 05/07/2012:35 05/08/20 17:07 92477008004 MW-2R Water 05/08/20 08:45 05/08/20 17:07 92477008005 MW-15 Water 05/08/2011:50 05/08/20 17:07 92477008006 EQBL Water 05/08/2012:40 05/08/20 17:07 92477013001 MW-10 Water 05/05/2012:35 05/08/20 17:07 92477013002 MW-7 Water 05/07/2010:35 05/08/20 17:07 92477016001 SW-2 Water 05/05/2014:35 05/08/20 17:07 92477016002 MW-3R Water 05/07/20 08:55 05/08/20 17:07 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: OSR LANDFILL GW 92477011 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92477011001 MW-8 EPA 601 OD DS 18 PASI-A EPA 7470A SOO 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 RED 1 PASI-A SM 4500-S2D-2011 LMS1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 4500-CN-E-2011 CJL 1 PASI-A 92477011002 MW-9 EPA 601 OD DS 18 PASI-A EPA 7470A SOO 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 RED 1 PASI-A SM 4500-S2D-2011 LMS1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 4500-CN-E-2011 CJL 1 PASI-A 92477011003 MW-14 EPA 601 OD DS 18 PASI-A EPA 7470A SOO 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 RED 1 PASI-A SM 4500-S2D-2011 LMS1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 4500-CN-E-2011 CJL 1 PASI-A 92477011004 SW-3 EPA 601 OD DS 18 PASI-A EPA 7470A SOO 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 RED 1 PASI-A SM 4500-S2D-2011 LMS1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR LANDFILL GW Pace Project No.: 92477011 Analytes Lab ID Sample ID Method Analysts Reported Laboratory EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 4500-CN-E-2011 CJL 1 PASI-A 92477011005 MW-11 EPA 601 OD DS 18 PASI-A EPA 7470A SOO 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 RED 1 PASI-A SM 4500-S2D-2011 LMS1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 4500-CN-E-2011 CJL 1 PASI-A 92477011006 MW-12 EPA 601 OD DS 18 PASI-A EPA 7470A SOO 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 RED 1 PASI-A SM 4500-S2D-2011 LMS1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 4500-CN-E-2011 CJL 1 PASI-A 92477011007 MW-13 EPA 601 OD DS 18 PASI-A EPA 7470A SOO 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 RED 1 PASI-A SM 4500-S2D-2011 LMS1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 4500-CN-E-2011 CJL 1 PASI-A 92477011008 MW-5R EPA 601 OD DS 18 PASI-A EPA 7470A SOO 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR LANDFILL GW Pace Project No.: 92477011 Lab ID Sample ID Method Analysts Analytes Reported Laboratory SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 RED 1 PASI-A SM 4500-S2D-2011 LMS1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 4500-CN-E-2011 CJL 1 PASI-A 92477011009 SW-4 EPA 601 OD DS 18 PASI-A EPA 7470A SOO 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 RED 1 PASI-A SM 4500-S2D-2011 LMS1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 4500-CN-E-2011 CJL 1 PASI-A 92477011010 SW-1 EPA 601 OD DS 18 PASI-A EPA 7470A SOO 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 RED 1 PASI-A SM 4500-S2D-2011 LMS1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 4500-CN-E-2011 DMN 1 PASI-A 92477011011 TRIP BLANK EPA 8260D CL 53 PASI-C 92477008001 MWA R EPA 8151 LEL 3 PAN EPA 8081 B SEM 14 PASI-C EPA 601OD SH1 18 PASI-A EPA 7470A SOO 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 RED 1 PASI-A SM 4500-S2D-2011 LMS1 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR LANDFILL GW Pace Project No.: 92477011 Analytes Lab ID Sample ID Method Analysts Reported Laboratory EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 4500-CN-E-2011 CJL 1 PASI-A 92477008002 FIELD BLANK EPA 8151 RP 3 PAN EPA 8081 B SEM 14 PASI-C EPA 601OD SH1 18 PASI-A EPA 7470A SOO 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 RED 1 PASI-A SM 4500-S2D-2011 LMS1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 4500-CN-E-2011 CJL 1 PASI-A 92477008003 MW-4R EPA 8151 RP 3 PAN EPA 8081 B SEM 14 PASI-C EPA 601OD SH1 18 PASI-A EPA 7470A SOO 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 RED 1 PASI-A SM 4500-S2D-2011 LMS1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 4500-CN-E-2011 CJL 1 PASI-A 92477008004 MW-2R EPA 8151 RP 3 PAN EPA 8081 B SEM 14 PASI-C EPA 601OD KQ, SH1 18 PASI-A EPA 7470A SOO 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 ECH 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR LANDFILL GW Pace Project No.: 92477011 Lab ID Sample ID Method Analysts Analytes Reported Laboratory SM 2540C-2011 RED 1 PASI-A SM 4500-S2D-2011 LMS1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 4500-CN-E-2011 CJL 1 PASI-A 92477008005 MW-15 EPA 8151 RP 3 PAN EPA 8081 B SEM 14 PASI-C EPA 601OD SH1 18 PASI-A EPA 7470A SOO 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 RED 1 PASI-A SM 4500-S2D-2011 LMS1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 4500-CN-E-2011 CJL 1 PASI-A 92477008006 EQBL EPA 8151 RP 3 PAN EPA 8081 B SEM 14 PASI-C EPA 601 OD DS 18 PASI-A EPA 7470A SOO 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 RED 1 PASI-A SM 4500-S2D-2011 LMS1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 4500-CN-E-2011 CJL 1 PASI-A 92477013001 MW-10 EPA 8081 B SEM 14 PASI-C EPA 601 OD DS 18 PASI-A EPA 7470A SOO 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 ECH 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR LANDFILL GW Pace Project No.: 92477011 Lab ID Sample ID Method Analysts Analytes Reported Laboratory SM 2540C-2011 RED 1 PASI-A SM 4500-S2D-2011 LMS1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 4500-CN-E-2011 CJL 1 PASI-A 92477013002 MW-7 EPA 8081 B SEM 14 PASI-C EPA 601 OD DS 18 PASI-A EPA 7470A SOO 1 PASI-A EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 RED 1 PASI-A SM 4500-S2D-2011 LMS1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 4500-CN-E-2011 DMN 1 PASI-A 92477016001 SW-2 EPA 601 OD DS 18 PASI-A EPA 7470A SOO 1 PASI-A EPA 8270E PKS 11 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 RED 1 PASI-A SM 4500-S2D-2011 LMS1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A SM 4500-CN-E-2011 CJL 1 PASI-A 92477016002 MW-3R EPA 601 OD DS 18 PASI-A EPA 7470A SOO 1 PASI-A EPA 8270E PKS 8 PASI-C EPA 8260D CL 53 PASI-C EPA 8260D Mod. LMB 3 PASI-C SM 2320B-2011 ECH 1 PASI-A SM 2540C-2011 RED 1 PASI-A SM 4500-S2D-2011 LMS1 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A SM 4500-CI-E-2011 MDW 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: OSR LANDFILL GW Pace Project No.: 92477011 Analytes Lab ID Sample ID Method Analysts Reported Laboratory SM 4500-CN-E-2011 DMN 1 PASI-A PAN = Pace National - Mt. Juliet PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-8 Lab ID: 92477011001 Collected: 05/04/20 14:30 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 05/14/20 01:51 05/19/20 19:37 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 19:37 7440-38-2 Barium 52.9 ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 19:37 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 05/14/20 01:51 05/19/20 19:37 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 05/14/20 01:51 05/19/20 19:37 7440-43-9 Chromium 5.6 ug/L 5.0 3.7 1 05/14/20 01:51 05/19/20 19:37 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 05/14/20 01:51 05/19/20 19:37 7440-48-4 Copper ND ug/L 5.0 4.3 1 05/14/20 01:51 05/19/20 19:37 7440-50-8 Iron 125 ug/L 50.0 41.5 1 05/14/20 01:51 05/19/20 19:37 7439-89-6 Lead ND ug/L 5.0 4.5 1 05/14/20 01:51 05/19/20 19:37 7439-92-1 Manganese ND ug/L 5.0 3.4 1 05/14/20 01:51 05/19/20 19:37 7439-96-5 Nickel ND ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 19:37 7440-02-0 Selenium ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 19:37 7782-49-2 Silver ND ug/L 5.0 2.5 1 05/14/20 01:51 05/19/20 19:37 7440-22-4 Sodium 12900 ug/L 5000 611 1 05/14/20 01:51 05/19/20 19:37 7440-23-5 Tin ND ug/L 5.0 4.7 1 05/14/20 01:51 05/19/20 19:37 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 05/14/20 01:51 05/19/20 19:37 7440-62-2 Zinc ND ug/L 10.0 9.5 1 05/14/20 01:51 05/19/20 19:37 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene Date: 06/09/2020 08:57 AM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 05/20/2017:30 05/21/2011:27 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 6.2 1 05/18/20 17:22 67-64-1 0.90 1 05/18/20 17:22 107-13-1 0.15 1 05/18/20 17:22 71-43-2 0.34 1 05/18/20 17:22 74-97-5 0.26 1 05/18/20 17:22 75-27-4 0.62 1 05/18/20 17:22 75-25-2 0.62 1 05/18/20 17:22 74-83-9 3.3 1 05/18/20 17:22 78-93-3 0.40 1 05/18/20 17:22 75-15-0 0.22 1 05/18/20 17:22 56-23-5 0.23 1 05/18/20 17:22 108-90-7 0.49 1 05/18/20 17:22 75-00-3 2.3 1 05/18/20 17:22 67-66-3 0.39 1 05/18/20 17:22 74-87-3 0.26 1 05/18/20 17:22 96-12-8 0.41 1 05/18/20 17:22 124-48-1 0.26 1 05/18/20 17:22 106-93-4 0.46 1 05/18/20 17:22 74-95-3 0.29 1 05/18/20 17:22 95-50-1 0.26 1 05/18/20 17:22 106-46-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. IK,v2 IK Page 11 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-8 Lab ID: 92477011001 Collected: 05/04/20 14:30 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.54 1 05/18/2017:22 110-57-6 IH ND ug/L 1.0 0.23 1 05/18/2017:22 75-71-8 IK ND ug/L 1.0 0.27 1 05/18/2017:22 75-34-3 ND ug/L 1.0 0.34 1 05/18/2017:22 107-06-2 ND ug/L 1.0 0.24 1 05/18/2017:22 75-35-4 ND ug/L 1.0 0.29 1 05/18/2017:22 156-59-2 ND ug/L 1.0 0.25 1 05/18/2017:22 156-60-5 ND ug/L 1.0 0.19 1 05/18/2017:22 78-87-5 ND ug/L 1.0 0.30 1 05/18/2017:22 10061-01-5 ND ug/L 1.0 0.31 1 05/18/2017:22 10061-02-6 ND ug/L 1.0 0.26 1 05/18/2017:22 100-41-4 ND ug/L 5.0 0.57 1 05/18/2017:22 591-78-6 ND ug/L 20.0 12.5 1 05/18/2017:22 74-88-4 ND ug/L 5.0 3.7 1 05/18/2017:22 75-09-2 ND ug/L 5.0 4.5 1 05/18/2017:22 108-10-1 ND ug/L 1.0 0.27 1 05/18/2017:22 100-42-5 ND ug/L 1.0 0.34 1 05/18/2017:22 630-20-6 ND ug/L 1.0 0.22 1 05/18/2017:22 79-34-5 ND ug/L 1.0 0.16 1 05/18/2017:22 127-18-4 ND ug/L 10.0 1.9 1 05/18/2017:22 109-99-9 ND ug/L 1.0 0.24 1 05/18/2017:22 108-88-3 ND ug/L 1.0 0.18 1 05/18/2017:22 71-55-6 ND ug/L 1.0 0.24 1 05/18/2017:22 79-00-5 ND ug/L 1.0 0.22 1 05/18/2017:22 79-01-6 ND ug/L 1.0 0.31 1 05/18/2017:22 75-69-4 IK ND ug/L 1.0 0.35 1 05/18/2017:22 96-18-4 ND ug/L 2.0 1.4 1 05/18/2017:22 108-05-4 ND ug/L 1.0 0.24 1 05/18/2017:22 75-01-4 IK ND ug/L 2.0 0.41 1 05/18/2017:22 179601-23-1 ND ug/L 1.0 0.22 1 05/18/2017:22 95-47-6 93 % 70-130 1 05/18/2017:22 460-00-4 103 % 70-130 1 05/18/2017:22 17060-07-0 103 % 70-130 1 05/18/2017:22 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 1.2 1 05/14/20 22:59 123-91-1 95 % 50-150 1 05/14/20 22:59 17060-07-0 108 % 50-150 1 05/14/20 22:59 2037-26-5 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 25000 ug/L 5000 5000 1 05/12/2019:49 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 12 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-8 Parameters Lab ID: 92477011001 Collected: 05/04/20 14:30 Report Results Units Limit MDL DF Received: 05/08/20 17:07 Matrix: Water Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville Total Dissolved Solids 93000 ug/L 25000 25000 1 05/11/20 23:02 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 05/11/20 23:27 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 9360 ug/L 1000 500 1 05/14/2011:21 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 4090 ug/L 1000 500 1 05/12/2019:16 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 05/13/20 09:08 05/14/20 14:21 57-12-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 13 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-9 Lab ID: 92477011002 Collected: 05/05/20 08:45 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 05/14/20 01:51 05/19/20 19:40 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 19:40 7440-38-2 Barium 238 ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 19:40 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 05/14/20 01:51 05/19/20 19:40 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 05/14/20 01:51 05/19/20 19:40 7440-43-9 Chromium ND ug/L 5.0 3.7 1 05/14/20 01:51 05/19/20 19:40 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 05/14/20 01:51 05/19/20 19:40 7440-48-4 Copper ND ug/L 5.0 4.3 1 05/14/20 01:51 05/19/20 19:40 7440-50-8 Iron 43.5J ug/L 50.0 41.5 1 05/14/20 01:51 05/19/20 19:40 7439-89-6 Lead ND ug/L 5.0 4.5 1 05/14/20 01:51 05/19/20 19:40 7439-92-1 Manganese 5.1 ug/L 5.0 3.4 1 05/14/20 01:51 05/19/20 19:40 7439-96-5 Nickel ND ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 19:40 7440-02-0 Selenium ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 19:40 7782-49-2 Silver ND ug/L 5.0 2.5 1 05/14/20 01:51 05/19/20 19:40 7440-22-4 Sodium 16200 ug/L 5000 611 1 05/14/20 01:51 05/19/20 19:40 7440-23-5 Tin ND ug/L 5.0 4.7 1 05/14/20 01:51 05/19/20 19:40 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 05/14/20 01:51 05/19/20 19:40 7440-62-2 Zinc ND ug/L 10.0 9.5 1 05/14/20 01:51 05/19/20 19:40 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene Date: 06/09/2020 08:57 AM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 05/20/2017:30 05/21/2011:29 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 6.2 1 05/18/20 19:48 67-64-1 0.90 1 05/18/20 19:48 107-13-1 0.15 1 05/18/20 19:48 71-43-2 0.34 1 05/18/20 19:48 74-97-5 0.26 1 05/18/20 19:48 75-27-4 0.62 1 05/18/20 19:48 75-25-2 0.62 1 05/18/20 19:48 74-83-9 3.3 1 05/18/20 19:48 78-93-3 0.40 1 05/18/20 19:48 75-15-0 0.22 1 05/18/20 19:48 56-23-5 0.23 1 05/18/20 19:48 108-90-7 0.49 1 05/18/20 19:48 75-00-3 2.3 1 05/18/20 19:48 67-66-3 0.39 1 05/18/20 19:48 74-87-3 0.26 1 05/18/20 19:48 96-12-8 0.41 1 05/18/20 19:48 124-48-1 0.26 1 05/18/20 19:48 106-93-4 0.46 1 05/18/20 19:48 74-95-3 0.29 1 05/18/20 19:48 95-50-1 0.26 1 05/18/20 19:48 106-46-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. IK,v2 IK Page 14 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-9 Lab ID: 92477011002 Collected: 05/05/20 08:45 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.54 1 05/18/2019:48 110-57-6 IH 1.1 ug/L 1.0 0.23 1 05/18/2019:48 75-71-8 IK ND ug/L 1.0 0.27 1 05/18/2019:48 75-34-3 ND ug/L 1.0 0.34 1 05/18/2019:48 107-06-2 ND ug/L 1.0 0.24 1 05/18/2019:48 75-35-4 ND ug/L 1.0 0.29 1 05/18/2019:48 156-59-2 ND ug/L 1.0 0.25 1 05/18/2019:48 156-60-5 ND ug/L 1.0 0.19 1 05/18/2019:48 78-87-5 ND ug/L 1.0 0.30 1 05/18/2019:48 10061-01-5 ND ug/L 1.0 0.31 1 05/18/2019:48 10061-02-6 ND ug/L 1.0 0.26 1 05/18/2019:48 100-41-4 ND ug/L 5.0 0.57 1 05/18/2019:48 591-78-6 ND ug/L 20.0 12.5 1 05/18/2019:48 74-88-4 ND ug/L 5.0 3.7 1 05/18/2019:48 75-09-2 ND ug/L 5.0 4.5 1 05/18/2019:48 108-10-1 ND ug/L 1.0 0.27 1 05/18/2019:48 100-42-5 ND ug/L 1.0 0.34 1 05/18/2019:48 630-20-6 ND ug/L 1.0 0.22 1 05/18/2019:48 79-34-5 ND ug/L 1.0 0.16 1 05/18/2019:48 127-18-4 ND ug/L 10.0 1.9 1 05/18/2019:48 109-99-9 ND ug/L 1.0 0.24 1 05/18/2019:48 108-88-3 ND ug/L 1.0 0.18 1 05/18/2019:48 71-55-6 ND ug/L 1.0 0.24 1 05/18/2019:48 79-00-5 ND ug/L 1.0 0.22 1 05/18/2019:48 79-01-6 1.3 ug/L 1.0 0.31 1 05/18/2019:48 75-69-4 IK ND ug/L 1.0 0.35 1 05/18/2019:48 96-18-4 ND ug/L 2.0 1.4 1 05/18/2019:48 108-05-4 ND ug/L 1.0 0.24 1 05/18/2019:48 75-01-4 IK ND ug/L 2.0 0.41 1 05/18/2019:48 179601-23-1 ND ug/L 1.0 0.22 1 05/18/2019:48 95-47-6 97 % 70-130 1 05/18/2019:48 460-00-4 104 % 70-130 1 05/18/2019:48 17060-07-0 102 % 70-130 1 05/18/2019:48 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 1.2 1 05/14/20 23:58 123-91-1 97 % 50-150 1 05/14/20 23:58 17060-07-0 89 % 50-150 1 05/14/20 23:58 2037-26-5 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 33900 ug/L 5000 5000 1 05/15/20 20:43 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 15 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-9 Parameters Lab ID: 92477011002 Collected: 05/05/20 08:45 Report Results Units Limit MDL DF Received: 05/08/20 17:07 Matrix: Water Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville Total Dissolved Solids 130000 ug/L 25000 25000 1 05/12/20 16:31 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 05/12/20 20:03 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate ND ug/L 1000 500 1 05/14/20 04:28 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 6370 ug/L 1000 500 1 05/12/2019:46 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 05/13/20 09:43 05/14/20 14:48 57-12-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 16 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-14 Lab ID: 92477011003 Collected: 05/05/20 10:25 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 05/14/20 01:51 05/19/20 19:43 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 19:43 7440-38-2 Barium 241 ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 19:43 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 05/14/20 01:51 05/19/20 19:43 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 05/14/20 01:51 05/19/20 19:43 7440-43-9 Chromium ND ug/L 5.0 3.7 1 05/14/20 01:51 05/19/20 19:43 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 05/14/20 01:51 05/19/20 19:43 7440-48-4 Copper ND ug/L 5.0 4.3 1 05/14/20 01:51 05/19/20 19:43 7440-50-8 Iron ND ug/L 50.0 41.5 1 05/14/20 01:51 05/19/20 19:43 7439-89-6 Lead ND ug/L 5.0 4.5 1 05/14/20 01:51 05/19/20 19:43 7439-92-1 Manganese 113 ug/L 5.0 3.4 1 05/14/20 01:51 05/19/20 19:43 7439-96-5 Nickel 3.9J ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 19:43 7440-02-0 Selenium ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 19:43 7782-49-2 Silver ND ug/L 5.0 2.5 1 05/14/20 01:51 05/19/20 19:43 7440-22-4 Sodium 17900 ug/L 5000 611 1 05/14/20 01:51 05/19/20 19:43 7440-23-5 Tin ND ug/L 5.0 4.7 1 05/14/20 01:51 05/19/20 19:43 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 05/14/20 01:51 05/19/20 19:43 7440-62-2 Zinc ND ug/L 10.0 9.5 1 05/14/20 01:51 05/19/20 19:43 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene Date: 06/09/2020 08:57 AM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 05/20/2017:30 05/21/2011:31 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 6.2 1 05/18/20 20:07 67-64-1 0.90 1 05/18/20 20:07 107-13-1 0.15 1 05/18/20 20:07 71-43-2 0.34 1 05/18/20 20:07 74-97-5 0.26 1 05/18/20 20:07 75-27-4 0.62 1 05/18/20 20:07 75-25-2 0.62 1 05/18/20 20:07 74-83-9 3.3 1 05/18/20 20:07 78-93-3 0.40 1 05/18/20 20:07 75-15-0 0.22 1 05/18/20 20:07 56-23-5 0.23 1 05/18/20 20:07 108-90-7 0.49 1 05/18/20 20:07 75-00-3 2.3 1 05/18/20 20:07 67-66-3 0.39 1 05/18/20 20:07 74-87-3 0.26 1 05/18/20 20:07 96-12-8 0.41 1 05/18/20 20:07 124-48-1 0.26 1 05/18/20 20:07 106-93-4 0.46 1 05/18/20 20:07 74-95-3 0.29 1 05/18/20 20:07 95-50-1 0.26 1 05/18/20 20:07 106-46-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. IK,v2 IK Page 17 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-14 Lab ID: 92477011003 Collected: 05/05/20 10:25 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.54 1 05/18/20 20:07 110-57-6 IH 2.4 ug/L 1.0 0.23 1 05/18/20 20:07 75-71-8 IK ND ug/L 1.0 0.27 1 05/18/20 20:07 75-34-3 ND ug/L 1.0 0.34 1 05/18/20 20:07 107-06-2 ND ug/L 1.0 0.24 1 05/18/20 20:07 75-35-4 ND ug/L 1.0 0.29 1 05/18/20 20:07 156-59-2 ND ug/L 1.0 0.25 1 05/18/20 20:07 156-60-5 ND ug/L 1.0 0.19 1 05/18/20 20:07 78-87-5 ND ug/L 1.0 0.30 1 05/18/20 20:07 10061-01-5 ND ug/L 1.0 0.31 1 05/18/20 20:07 10061-02-6 ND ug/L 1.0 0.26 1 05/18/20 20:07 100-41-4 ND ug/L 5.0 0.57 1 05/18/20 20:07 591-78-6 ND ug/L 20.0 12.5 1 05/18/20 20:07 74-88-4 ND ug/L 5.0 3.7 1 05/18/20 20:07 75-09-2 ND ug/L 5.0 4.5 1 05/18/20 20:07 108-10-1 ND ug/L 1.0 0.27 1 05/18/20 20:07 100-42-5 ND ug/L 1.0 0.34 1 05/18/20 20:07 630-20-6 ND ug/L 1.0 0.22 1 05/18/20 20:07 79-34-5 0.53.11 ug/L 1.0 0.16 1 05/18/20 20:07 127-18-4 ND ug/L 10.0 1.9 1 05/18/20 20:07 109-99-9 ND ug/L 1.0 0.24 1 05/18/20 20:07 108-88-3 ND ug/L 1.0 0.18 1 05/18/20 20:07 71-55-6 ND ug/L 1.0 0.24 1 05/18/20 20:07 79-00-5 ND ug/L 1.0 0.22 1 05/18/20 20:07 79-01-6 1.0 ug/L 1.0 0.31 1 05/18/20 20:07 75-69-4 IK ND ug/L 1.0 0.35 1 05/18/20 20:07 96-18-4 ND ug/L 2.0 1.4 1 05/18/20 20:07 108-05-4 ND ug/L 1.0 0.24 1 05/18/20 20:07 75-01-4 IK ND ug/L 2.0 0.41 1 05/18/20 20:07 179601-23-1 ND ug/L 1.0 0.22 1 05/18/20 20:07 95-47-6 96 % 70-130 1 05/18/20 20:07 460-00-4 103 % 70-130 1 05/18/20 20:07 17060-07-0 102 % 70-130 1 05/18/20 20:07 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 1.2 1 05/15/20 00:18 123-91-1 96 % 50-150 1 05/15/20 00:18 17060-07-0 92 % 50-150 1 05/15/20 00:18 2037-26-5 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 65500 ug/L 5000 5000 1 05/15/20 20:50 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 18 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-14 Parameters Lab ID: 92477011003 Collected: 05/05/20 10:25 Report Results Units Limit MDL DF Received: 05/08/20 17:07 Matrix: Water Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville Total Dissolved Solids 150000 ug/L 25000 25000 1 05/12/20 16:31 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 05/12/20 20:04 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate ND ug/L 1000 500 1 05/14/20 05:58 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 3730 ug/L 1000 500 1 05/12/2019:47 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 05/13/20 09:43 05/14/20 14:44 57-12-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 19 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: SW-3 Lab ID: 92477011004 Collected: 05/05/20 15:25 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 05/14/20 01:51 05/19/20 19:46 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 19:46 7440-38-2 Barium 169 ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 19:46 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 05/14/20 01:51 05/19/20 19:46 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 05/14/20 01:51 05/19/20 19:46 7440-43-9 Chromium ND ug/L 5.0 3.7 1 05/14/20 01:51 05/19/20 19:46 7440-47-3 Cobalt 4.2J ug/L 5.0 3.6 1 05/14/20 01:51 05/19/20 19:46 7440-48-4 Copper ND ug/L 5.0 4.3 1 05/14/20 01:51 05/19/20 19:46 7440-50-8 Iron 7910 ug/L 50.0 41.5 1 05/14/20 01:51 05/19/20 19:46 7439-89-6 Lead ND ug/L 5.0 4.5 1 05/14/20 01:51 05/19/20 19:46 7439-92-1 Manganese 3280 ug/L 5.0 3.4 1 05/14/20 01:51 05/19/20 19:46 7439-96-5 Nickel ND ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 19:46 7440-02-0 Selenium ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 19:46 7782-49-2 Silver ND ug/L 5.0 2.5 1 05/14/20 01:51 05/19/20 19:46 7440-22-4 Sodium 22500 ug/L 5000 611 1 05/14/20 01:51 05/19/20 19:46 7440-23-5 Tin ND ug/L 5.0 4.7 1 05/14/20 01:51 05/19/20 19:46 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 05/14/20 01:51 05/19/20 19:46 7440-62-2 Zinc ND ug/L 10.0 9.5 1 05/14/20 01:51 05/19/20 19:46 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene Date: 06/09/2020 08:57 AM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville 0.18J ug/L 0.20 0.12 1 05/20/20 17:30 05/21 /20 11:34 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 6.2 1 05/18/20 20:25 67-64-1 0.90 1 05/18/20 20:25 107-13-1 0.15 1 05/18/20 20:25 71-43-2 0.34 1 05/18/20 20:25 74-97-5 0.26 1 05/18/20 20:25 75-27-4 0.62 1 05/18/20 20:25 75-25-2 0.62 1 05/18/20 20:25 74-83-9 3.3 1 05/18/20 20:25 78-93-3 0.40 1 05/18/20 20:25 75-15-0 0.22 1 05/18/20 20:25 56-23-5 0.23 1 05/18/20 20:25 108-90-7 0.49 1 05/18/20 20:25 75-00-3 2.3 1 05/18/20 20:25 67-66-3 0.39 1 05/18/20 20:25 74-87-3 0.26 1 05/18/20 20:25 96-12-8 0.41 1 05/18/20 20:25 124-48-1 0.26 1 05/18/20 20:25 106-93-4 0.46 1 05/18/20 20:25 74-95-3 0.29 1 05/18/20 20:25 95-50-1 0.26 1 05/18/20 20:25 106-46-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. IK,v2 IK Page 20 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: SW-3 Lab ID: 92477011004 Collected: 05/05/20 15:25 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.54 1 05/18/20 20:25 110-57-6 IH ND ug/L 1.0 0.23 1 05/18/20 20:25 75-71-8 IK ND ug/L 1.0 0.27 1 05/18/20 20:25 75-34-3 ND ug/L 1.0 0.34 1 05/18/20 20:25 107-06-2 ND ug/L 1.0 0.24 1 05/18/20 20:25 75-35-4 ND ug/L 1.0 0.29 1 05/18/20 20:25 156-59-2 ND ug/L 1.0 0.25 1 05/18/20 20:25 156-60-5 ND ug/L 1.0 0.19 1 05/18/20 20:25 78-87-5 ND ug/L 1.0 0.30 1 05/18/20 20:25 10061-01-5 ND ug/L 1.0 0.31 1 05/18/20 20:25 10061-02-6 ND ug/L 1.0 0.26 1 05/18/20 20:25 100-41-4 ND ug/L 5.0 0.57 1 05/18/20 20:25 591-78-6 ND ug/L 20.0 12.5 1 05/18/20 20:25 74-88-4 ND ug/L 5.0 3.7 1 05/18/20 20:25 75-09-2 ND ug/L 5.0 4.5 1 05/18/20 20:25 108-10-1 ND ug/L 1.0 0.27 1 05/18/20 20:25 100-42-5 ND ug/L 1.0 0.34 1 05/18/20 20:25 630-20-6 ND ug/L 1.0 0.22 1 05/18/20 20:25 79-34-5 ND ug/L 1.0 0.16 1 05/18/20 20:25 127-18-4 ND ug/L 10.0 1.9 1 05/18/20 20:25 109-99-9 ND ug/L 1.0 0.24 1 05/18/20 20:25 108-88-3 ND ug/L 1.0 0.18 1 05/18/20 20:25 71-55-6 ND ug/L 1.0 0.24 1 05/18/20 20:25 79-00-5 ND ug/L 1.0 0.22 1 05/18/20 20:25 79-01-6 ND ug/L 1.0 0.31 1 05/18/20 20:25 75-69-4 IK ND ug/L 1.0 0.35 1 05/18/20 20:25 96-18-4 ND ug/L 2.0 1.4 1 05/18/20 20:25 108-05-4 ND ug/L 1.0 0.24 1 05/18/20 20:25 75-01-4 IK ND ug/L 2.0 0.41 1 05/18/20 20:25 179601-23-1 ND ug/L 1.0 0.22 1 05/18/20 20:25 95-47-6 97 % 70-130 1 05/18/20 20:25 460-00-4 105 % 70-130 1 05/18/20 20:25 17060-07-0 102 % 70-130 1 05/18/20 20:25 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 1.2 1 05/15/20 00:38 123-91-1 97 % 50-150 1 05/15/20 00:38 17060-07-0 95 % 50-150 1 05/15/20 00:38 2037-26-5 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 330000 ug/L 5000 5000 1 05/15/20 21:01 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 21 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: SW-3 Parameters Lab ID: 92477011004 Collected: 05/05/20 15:25 Report Results Units Limit MDL DF Received: 05/08/20 17:07 Matrix: Water Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville Total Dissolved Solids 421000 ug/L 25000 25000 1 05/12/20 16:32 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 05/12/20 20:05 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 28600 ug/L 1000 500 1 05/14/20 06:13 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 19600 ug/L 1000 500 1 05/13/20 20:16 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 05/13/20 09:43 05/14/20 14:45 57-12-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 22 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-11 Lab ID: 92477011005 Collected: 05/06/20 09:25 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 05/14/20 01:51 05/19/20 19:49 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 19:49 7440-38-2 Barium 98.1 ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 19:49 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 05/14/20 01:51 05/19/20 19:49 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 05/14/20 01:51 05/19/20 19:49 7440-43-9 Chromium ND ug/L 5.0 3.7 1 05/14/20 01:51 05/19/20 19:49 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 05/14/20 01:51 05/19/20 19:49 7440-48-4 Copper ND ug/L 5.0 4.3 1 05/14/20 01:51 05/19/20 19:49 7440-50-8 Iron 23700 ug/L 50.0 41.5 1 05/14/20 01:51 05/19/20 19:49 7439-89-6 Lead ND ug/L 5.0 4.5 1 05/14/20 01:51 05/19/20 19:49 7439-92-1 Manganese 1650 ug/L 5.0 3.4 1 05/14/20 01:51 05/19/20 19:49 7439-96-5 Nickel ND ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 19:49 7440-02-0 Selenium ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 19:49 7782-49-2 Silver ND ug/L 5.0 2.5 1 05/14/20 01:51 05/19/20 19:49 7440-22-4 Sodium 12400 ug/L 5000 611 1 05/14/20 01:51 05/19/20 19:49 7440-23-5 Tin ND ug/L 5.0 4.7 1 05/14/20 01:51 05/19/20 19:49 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 05/14/20 01:51 05/19/20 19:49 7440-62-2 Zinc ND ug/L 10.0 9.5 1 05/14/20 01:51 05/19/20 19:49 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene Date: 06/09/2020 08:57 AM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville 1.6 ug/L 0.20 0.12 1 05/20/20 17:30 05/21 /20 11:41 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 6.2 1 05/19/20 08:22 67-64-1 0.90 1 05/19/20 08:22 107-13-1 0.15 1 05/19/20 08:22 71-43-2 0.34 1 05/19/20 08:22 74-97-5 0.26 1 05/19/20 08:22 75-27-4 0.62 1 05/19/20 08:22 75-25-2 0.62 1 05/19/20 08:22 74-83-9 3.3 1 05/19/20 08:22 78-93-3 0.40 1 05/19/20 08:22 75-15-0 0.22 1 05/19/20 08:22 56-23-5 0.23 1 05/19/20 08:22 108-90-7 0.49 1 05/19/20 08:22 75-00-3 2.3 1 05/19/20 08:22 67-66-3 0.39 1 05/19/20 08:22 74-87-3 0.26 1 05/19/20 08:22 96-12-8 0.41 1 05/19/20 08:22 124-48-1 0.26 1 05/19/20 08:22 106-93-4 0.46 1 05/19/20 08:22 74-95-3 0.29 1 05/19/20 08:22 95-50-1 0.26 1 05/19/20 08:22 106-46-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. IK,v2 IK Page 23 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-11 Lab ID: 92477011005 Collected: 05/06/20 09:25 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.54 1 05/19/20 08:22 110-57-6 IH ND ug/L 1.0 0.23 1 05/19/20 08:22 75-71-8 IK ND ug/L 1.0 0.27 1 05/19/20 08:22 75-34-3 ND ug/L 1.0 0.34 1 05/19/20 08:22 107-06-2 ND ug/L 1.0 0.24 1 05/19/20 08:22 75-35-4 ND ug/L 1.0 0.29 1 05/19/20 08:22 156-59-2 ND ug/L 1.0 0.25 1 05/19/20 08:22 156-60-5 ND ug/L 1.0 0.19 1 05/19/20 08:22 78-87-5 ND ug/L 1.0 0.30 1 05/19/20 08:22 10061-01-5 ND ug/L 1.0 0.31 1 05/19/20 08:22 10061-02-6 ND ug/L 1.0 0.26 1 05/19/20 08:22 100-41-4 ND ug/L 5.0 0.57 1 05/19/20 08:22 591-78-6 ND ug/L 20.0 12.5 1 05/19/20 08:22 74-88-4 v2 ND ug/L 5.0 3.7 1 05/19/20 08:22 75-09-2 ND ug/L 5.0 4.5 1 05/19/20 08:22 108-10-1 v1 ND ug/L 1.0 0.27 1 05/19/20 08:22 100-42-5 ND ug/L 1.0 0.34 1 05/19/20 08:22 630-20-6 ND ug/L 1.0 0.22 1 05/19/20 08:22 79-34-5 ND ug/L 1.0 0.16 1 05/19/20 08:22 127-18-4 ND ug/L 10.0 1.9 1 05/19/20 08:22 109-99-9 ND ug/L 1.0 0.24 1 05/19/20 08:22 108-88-3 ND ug/L 1.0 0.18 1 05/19/20 08:22 71-55-6 ND ug/L 1.0 0.24 1 05/19/20 08:22 79-00-5 ND ug/L 1.0 0.22 1 05/19/20 08:22 79-01-6 ND ug/L 1.0 0.31 1 05/19/20 08:22 75-69-4 IK ND ug/L 1.0 0.35 1 05/19/20 08:22 96-18-4 ND ug/L 2.0 1.4 1 05/19/20 08:22 108-05-4 v1 ND ug/L 1.0 0.24 1 05/19/20 08:22 75-01-4 IK ND ug/L 2.0 0.41 1 05/19/20 08:22 179601-23-1 ND ug/L 1.0 0.22 1 05/19/20 08:22 95-47-6 98 % 70-130 1 05/19/20 08:22 460-00-4 115 % 70-130 1 05/19/20 08:22 17060-07-0 105 % 70-130 1 05/19/20 08:22 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 1.2 1 05/15/20 03:15 123-91-1 91 % 50-150 1 05/15/20 03:15 17060-07-0 102 % 50-150 1 05/15/20 03:15 2037-26-5 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 127000 ug/L 5000 5000 1 05/15/20 22:10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 24 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-11 Parameters Lab ID: 92477011005 Collected: 05/06/20 09:25 Report Results Units Limit MDL DF Received: 05/08/20 17:07 Matrix: Water Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville Total Dissolved Solids 230000 ug/L 25000 25000 1 05/12/20 23:19 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 05/12/20 20:09 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 22800 ug/L 1000 500 1 05/14/20 06:28 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 11000 ug/L 1000 500 1 05/13/20 20:17 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 05/18/2013:47 05/19/2011:49 57-12-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 25 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-12 Lab ID: 92477011006 Collected: 05/06/20 11:25 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 05/14/20 01:51 05/19/20 19:52 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 19:52 7440-38-2 Barium 224 ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 19:52 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 05/14/20 01:51 05/19/20 19:52 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 05/14/20 01:51 05/19/20 19:52 7440-43-9 Chromium ND ug/L 5.0 3.7 1 05/14/20 01:51 05/19/20 19:52 7440-47-3 Cobalt 11.0 ug/L 5.0 3.6 1 05/14/20 01:51 05/19/20 19:52 7440-48-4 Copper ND ug/L 5.0 4.3 1 05/14/20 01:51 05/19/20 19:52 7440-50-8 Iron 2560 ug/L 50.0 41.5 1 05/14/20 01:51 05/19/20 19:52 7439-89-6 Lead ND ug/L 5.0 4.5 1 05/14/20 01:51 05/19/20 19:52 7439-92-1 Manganese 6410 ug/L 5.0 3.4 1 05/14/20 01:51 05/19/20 19:52 7439-96-5 Nickel 10.6 ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 19:52 7440-02-0 Selenium ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 19:52 7782-49-2 Silver ND ug/L 5.0 2.5 1 05/14/20 01:51 05/19/20 19:52 7440-22-4 Sodium 28600 ug/L 5000 611 1 05/14/20 01:51 05/19/20 19:52 7440-23-5 Tin ND ug/L 5.0 4.7 1 05/14/20 01:51 05/19/20 19:52 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 05/14/20 01:51 05/19/20 19:52 7440-62-2 Zinc ND ug/L 10.0 9.5 1 05/14/20 01:51 05/19/20 19:52 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene Date: 06/09/2020 08:57 AM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 05/20/2017:30 05/21/2011:43 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 0.29J ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 6.2 1 05/19/20 08:41 67-64-1 0.90 1 05/19/20 08:41 107-13-1 0.15 1 05/19/20 08:41 71-43-2 0.34 1 05/19/20 08:41 74-97-5 0.26 1 05/19/20 08:41 75-27-4 0.62 1 05/19/20 08:41 75-25-2 0.62 1 05/19/20 08:41 74-83-9 3.3 1 05/19/20 08:41 78-93-3 0.40 1 05/19/20 08:41 75-15-0 0.22 1 05/19/20 08:41 56-23-5 0.23 1 05/19/20 08:41 108-90-7 0.49 1 05/19/20 08:41 75-00-3 2.3 1 05/19/20 08:41 67-66-3 0.39 1 05/19/20 08:41 74-87-3 0.26 1 05/19/20 08:41 96-12-8 0.41 1 05/19/20 08:41 124-48-1 0.26 1 05/19/20 08:41 106-93-4 0.46 1 05/19/20 08:41 74-95-3 0.29 1 05/19/20 08:41 95-50-1 0.26 1 05/19/20 08:41 106-46-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. IK,v2 IK Page 26 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-12 Lab ID: 92477011006 Collected: 05/06/20 11:25 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.54 1 05/19/20 08:41 110-57-6 IH ND ug/L 1.0 0.23 1 05/19/20 08:41 75-71-8 IK ND ug/L 1.0 0.27 1 05/19/20 08:41 75-34-3 ND ug/L 1.0 0.34 1 05/19/20 08:41 107-06-2 ND ug/L 1.0 0.24 1 05/19/20 08:41 75-35-4 ND ug/L 1.0 0.29 1 05/19/20 08:41 156-59-2 ND ug/L 1.0 0.25 1 05/19/20 08:41 156-60-5 ND ug/L 1.0 0.19 1 05/19/20 08:41 78-87-5 ND ug/L 1.0 0.30 1 05/19/20 08:41 10061-01-5 ND ug/L 1.0 0.31 1 05/19/20 08:41 10061-02-6 ND ug/L 1.0 0.26 1 05/19/20 08:41 100-41-4 ND ug/L 5.0 0.57 1 05/19/20 08:41 591-78-6 ND ug/L 20.0 12.5 1 05/19/20 08:41 74-88-4 v2 ND ug/L 5.0 3.7 1 05/19/20 08:41 75-09-2 ND ug/L 5.0 4.5 1 05/19/20 08:41 108-10-1 v1 ND ug/L 1.0 0.27 1 05/19/20 08:41 100-42-5 ND ug/L 1.0 0.34 1 05/19/20 08:41 630-20-6 ND ug/L 1.0 0.22 1 05/19/20 08:41 79-34-5 ND ug/L 1.0 0.16 1 05/19/20 08:41 127-18-4 ND ug/L 10.0 1.9 1 05/19/20 08:41 109-99-9 ND ug/L 1.0 0.24 1 05/19/20 08:41 108-88-3 ND ug/L 1.0 0.18 1 05/19/20 08:41 71-55-6 ND ug/L 1.0 0.24 1 05/19/20 08:41 79-00-5 ND ug/L 1.0 0.22 1 05/19/20 08:41 79-01-6 ND ug/L 1.0 0.31 1 05/19/20 08:41 75-69-4 IK ND ug/L 1.0 0.35 1 05/19/20 08:41 96-18-4 ND ug/L 2.0 1.4 1 05/19/20 08:41 108-05-4 v1 ND ug/L 1.0 0.24 1 05/19/20 08:41 75-01-4 IK ND ug/L 2.0 0.41 1 05/19/20 08:41 179601-23-1 ND ug/L 1.0 0.22 1 05/19/20 08:41 95-47-6 95 % 70-130 1 05/19/20 08:41 460-00-4 111 % 70-130 1 05/19/20 08:41 17060-07-0 103 % 70-130 1 05/19/20 08:41 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 10.3 ug/L 2.0 1.2 1 05/15/20 03:35 123-91-1 95 % 50-150 1 05/15/20 03:35 17060-07-0 95 % 50-150 1 05/15/20 03:35 2037-26-5 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 333000 ug/L 5000 5000 1 05/15/20 22:22 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 27 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-12 Parameters Lab ID: 92477011006 Collected: 05/06/20 11:25 Report Results Units Limit MDL DF Received: 05/08/20 17:07 Matrix: Water Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville Total Dissolved Solids 812000 ug/L 50000 50000 1 05/12/20 23:19 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 05/12/20 20:09 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 227000 ug/L 5000 2500 5 05/14/2013:44 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 29500 ug/L 1000 500 1 05/13/20 20:18 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 05/18/2013:47 05/19/2011:50 57-12-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 28 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-13 Lab ID: 92477011007 Collected: 05/06/20 12:55 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 05/14/20 01:51 05/19/20 19:56 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 19:56 7440-38-2 Barium 196 ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 19:56 7440-39-3 Beryllium 0.72J ug/L 1.0 0.70 1 05/14/20 01:51 05/19/20 19:56 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 05/14/20 01:51 05/19/20 19:56 7440-43-9 Chromium ND ug/L 5.0 3.7 1 05/14/20 01:51 05/19/20 19:56 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 05/14/20 01:51 05/19/20 19:56 7440-48-4 Copper ND ug/L 5.0 4.3 1 05/14/20 01:51 05/19/20 19:56 7440-50-8 Iron 80.8 ug/L 50.0 41.5 1 05/14/20 01:51 05/19/20 19:56 7439-89-6 Lead ND ug/L 5.0 4.5 1 05/14/20 01:51 05/19/20 19:56 7439-92-1 Manganese 27.4 ug/L 5.0 3.4 1 05/14/20 01:51 05/19/20 19:56 7439-96-5 Nickel ND ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 19:56 7440-02-0 Selenium ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 19:56 7782-49-2 Silver ND ug/L 5.0 2.5 1 05/14/20 01:51 05/19/20 19:56 7440-22-4 Sodium 12600 ug/L 5000 611 1 05/14/20 01:51 05/19/20 19:56 7440-23-5 Tin ND ug/L 5.0 4.7 1 05/14/20 01:51 05/19/20 19:56 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 05/14/20 01:51 05/19/20 19:56 7440-62-2 Zinc ND ug/L 10.0 9.5 1 05/14/20 01:51 05/19/20 19:56 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene Date: 06/09/2020 08:57 AM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville 0.52 ug/L 0.20 0.12 1 05/20/20 17:30 05/21 /20 11:45 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 6.2 1 05/19/20 08:59 67-64-1 0.90 1 05/19/20 08:59 107-13-1 0.15 1 05/19/20 08:59 71-43-2 0.34 1 05/19/20 08:59 74-97-5 0.26 1 05/19/20 08:59 75-27-4 0.62 1 05/19/20 08:59 75-25-2 0.62 1 05/19/20 08:59 74-83-9 3.3 1 05/19/20 08:59 78-93-3 0.40 1 05/19/20 08:59 75-15-0 0.22 1 05/19/20 08:59 56-23-5 0.23 1 05/19/20 08:59 108-90-7 0.49 1 05/19/20 08:59 75-00-3 2.3 1 05/19/20 08:59 67-66-3 0.39 1 05/19/20 08:59 74-87-3 0.26 1 05/19/20 08:59 96-12-8 0.41 1 05/19/20 08:59 124-48-1 0.26 1 05/19/20 08:59 106-93-4 0.46 1 05/19/20 08:59 74-95-3 0.29 1 05/19/20 08:59 95-50-1 0.26 1 05/19/20 08:59 106-46-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. IK,v2 IK Page 29 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-13 Lab ID: 92477011007 Collected: 05/06/20 12:55 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.54 1 05/19/20 08:59 110-57-6 IH ND ug/L 1.0 0.23 1 05/19/20 08:59 75-71-8 IK ND ug/L 1.0 0.27 1 05/19/20 08:59 75-34-3 ND ug/L 1.0 0.34 1 05/19/20 08:59 107-06-2 ND ug/L 1.0 0.24 1 05/19/20 08:59 75-35-4 ND ug/L 1.0 0.29 1 05/19/20 08:59 156-59-2 ND ug/L 1.0 0.25 1 05/19/20 08:59 156-60-5 ND ug/L 1.0 0.19 1 05/19/20 08:59 78-87-5 ND ug/L 1.0 0.30 1 05/19/20 08:59 10061-01-5 ND ug/L 1.0 0.31 1 05/19/20 08:59 10061-02-6 ND ug/L 1.0 0.26 1 05/19/20 08:59 100-41-4 ND ug/L 5.0 0.57 1 05/19/20 08:59 591-78-6 ND ug/L 20.0 12.5 1 05/19/20 08:59 74-88-4 v2 ND ug/L 5.0 3.7 1 05/19/20 08:59 75-09-2 ND ug/L 5.0 4.5 1 05/19/20 08:59 108-10-1 v1 ND ug/L 1.0 0.27 1 05/19/20 08:59 100-42-5 ND ug/L 1.0 0.34 1 05/19/20 08:59 630-20-6 ND ug/L 1.0 0.22 1 05/19/20 08:59 79-34-5 ND ug/L 1.0 0.16 1 05/19/20 08:59 127-18-4 ND ug/L 10.0 1.9 1 05/19/20 08:59 109-99-9 ND ug/L 1.0 0.24 1 05/19/20 08:59 108-88-3 ND ug/L 1.0 0.18 1 05/19/20 08:59 71-55-6 ND ug/L 1.0 0.24 1 05/19/20 08:59 79-00-5 ND ug/L 1.0 0.22 1 05/19/20 08:59 79-01-6 ND ug/L 1.0 0.31 1 05/19/20 08:59 75-69-4 IK ND ug/L 1.0 0.35 1 05/19/20 08:59 96-18-4 ND ug/L 2.0 1.4 1 05/19/20 08:59 108-05-4 v1 ND ug/L 1.0 0.24 1 05/19/20 08:59 75-01-4 IK ND ug/L 2.0 0.41 1 05/19/20 08:59 179601-23-1 ND ug/L 1.0 0.22 1 05/19/20 08:59 95-47-6 97 % 70-130 1 05/19/20 08:59 460-00-4 118 % 70-130 1 05/19/20 08:59 17060-07-0 103 % 70-130 1 05/19/20 08:59 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 1.2 1 05/15/20 03:54 123-91-1 95 % 50-150 1 05/15/20 03:54 17060-07-0 94 % 50-150 1 05/15/20 03:54 2037-26-5 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 66400 ug/L 5000 5000 1 05/15/20 22:43 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 30 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-13 Parameters Lab ID: 92477011007 Collected: 05/06/20 12:55 Report Results Units Limit MDL DF Received: 05/08/20 17:07 Matrix: Water Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville Total Dissolved Solids 126000 ug/L 25000 25000 1 05/12/20 23:19 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 05/12/20 20:09 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 6520 ug/L 1000 500 1 05/14/20 06:58 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 8400 ug/L 1000 500 1 05/13/20 20:18 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 05/18/2013:47 05/19/2011:51 57-12-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 31 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-5R Lab ID: 92477011008 Collected: 05/07/20 14:20 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 05/14/20 01:51 05/19/20 19:59 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 19:59 7440-38-2 Barium 56.5 ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 19:59 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 05/14/20 01:51 05/19/20 19:59 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 05/14/20 01:51 05/19/20 19:59 7440-43-9 Chromium 6.8 ug/L 5.0 3.7 1 05/14/20 01:51 05/19/20 19:59 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 05/14/20 01:51 05/19/20 19:59 7440-48-4 Copper ND ug/L 5.0 4.3 1 05/14/20 01:51 05/19/20 19:59 7440-50-8 Iron 211 ug/L 50.0 41.5 1 05/14/20 01:51 05/19/20 19:59 7439-89-6 Lead ND ug/L 5.0 4.5 1 05/14/20 01:51 05/19/20 19:59 7439-92-1 Manganese ND ug/L 5.0 3.4 1 05/14/20 01:51 05/19/20 19:59 7439-96-5 Nickel ND ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 19:59 7440-02-0 Selenium ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 19:59 7782-49-2 Silver ND ug/L 5.0 2.5 1 05/14/20 01:51 05/19/20 19:59 7440-22-4 Sodium 17100 ug/L 5000 611 1 05/14/20 01:51 05/19/20 19:59 7440-23-5 Tin ND ug/L 5.0 4.7 1 05/14/20 01:51 05/19/20 19:59 7440-31-5 Vanadium 5.5 ug/L 5.0 3.9 1 05/14/20 01:51 05/19/20 19:59 7440-62-2 Zinc ND ug/L 10.0 9.5 1 05/14/20 01:51 05/19/20 19:59 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene Date: 06/09/2020 08:57 AM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville 0.69 ug/L 0.20 0.12 1 05/20/20 17:30 05/21 /20 11:48 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 6.2 1 05/19/20 06:39 67-64-1 0.90 1 05/19/20 06:39 107-13-1 0.15 1 05/19/20 06:39 71-43-2 0.34 1 05/19/20 06:39 74-97-5 0.26 1 05/19/20 06:39 75-27-4 0.62 1 05/19/20 06:39 75-25-2 0.62 1 05/19/20 06:39 74-83-9 3.3 1 05/19/20 06:39 78-93-3 0.40 1 05/19/20 06:39 75-15-0 0.22 1 05/19/20 06:39 56-23-5 0.23 1 05/19/20 06:39 108-90-7 0.49 1 05/19/20 06:39 75-00-3 2.3 1 05/19/20 06:39 67-66-3 0.39 1 05/19/20 06:39 74-87-3 0.26 1 05/19/20 06:39 96-12-8 0.41 1 05/19/20 06:39 124-48-1 0.26 1 05/19/20 06:39 106-93-4 0.46 1 05/19/20 06:39 74-95-3 0.29 1 05/19/20 06:39 95-50-1 0.26 1 05/19/20 06:39 106-46-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. IH,IK,L1 Page 32 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-5R Lab ID: 92477011008 Collected: 05/07/20 14:20 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.54 1 05/19/20 06:39 110-57-6 L1,v1 ND ug/L 1.0 0.23 1 05/19/20 06:39 75-71-8 ND ug/L 1.0 0.27 1 05/19/20 06:39 75-34-3 ND ug/L 1.0 0.34 1 05/19/20 06:39 107-06-2 ND ug/L 1.0 0.24 1 05/19/20 06:39 75-35-4 ND ug/L 1.0 0.29 1 05/19/20 06:39 156-59-2 ND ug/L 1.0 0.25 1 05/19/20 06:39 156-60-5 ND ug/L 1.0 0.19 1 05/19/20 06:39 78-87-5 ND ug/L 1.0 0.30 1 05/19/20 06:39 10061-01-5 ND ug/L 1.0 0.31 1 05/19/20 06:39 10061-02-6 ND ug/L 1.0 0.26 1 05/19/20 06:39 100-41-4 ND ug/L 5.0 0.57 1 05/19/20 06:39 591-78-6 ND ug/L 20.0 12.5 1 05/19/20 06:39 74-88-4 ND ug/L 5.0 3.7 1 05/19/20 06:39 75-09-2 ND ug/L 5.0 4.5 1 05/19/20 06:39 108-10-1 ND ug/L 1.0 0.27 1 05/19/20 06:39 100-42-5 ND ug/L 1.0 0.34 1 05/19/20 06:39 630-20-6 ND ug/L 1.0 0.22 1 05/19/20 06:39 79-34-5 ND ug/L 1.0 0.16 1 05/19/20 06:39 127-18-4 ND ug/L 10.0 1.9 1 05/19/20 06:39 109-99-9 ND ug/L 1.0 0.24 1 05/19/20 06:39 108-88-3 ND ug/L 1.0 0.18 1 05/19/20 06:39 71-55-6 ND ug/L 1.0 0.24 1 05/19/20 06:39 79-00-5 ND ug/L 1.0 0.22 1 05/19/20 06:39 79-01-6 ND ug/L 1.0 0.31 1 05/19/20 06:39 75-69-4 ND ug/L 1.0 0.35 1 05/19/20 06:39 96-18-4 ND ug/L 2.0 1.4 1 05/19/20 06:39 108-05-4 IK ND ug/L 1.0 0.24 1 05/19/20 06:39 75-01-4 ND ug/L 2.0 0.41 1 05/19/20 06:39 179601-23-1 ND ug/L 1.0 0.22 1 05/19/20 06:39 95-47-6 98 % 70-130 1 05/19/20 06:39 460-00-4 95 % 70-130 1 05/19/20 06:39 17060-07-0 100 % 70-130 1 05/19/20 06:39 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 1.2 1 05/15/2015:08 123-91-1 98 % 50-150 1 05/15/2015:08 17060-07-0 94 % 50-150 1 05/15/2015:08 2037-26-5 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 35700 ug/L 5000 5000 1 05/16/20 02:33 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 33 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-5R Parameters Lab ID: 92477011008 Collected: 05/07/20 14:20 Report Results Units Limit MDL DF Received: 05/08/20 17:07 Matrix: Water Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville Total Dissolved Solids 163000 ug/L 25000 25000 1 05/12/20 23:20 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 05/12/20 20:44 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 7770 ug/L 1000 500 1 05/14/20 07:13 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 14500 ug/L 1000 500 1 05/13/20 20:19 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 05/18/2013:48 05/19/2012:21 57-12-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 34 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: SW-4 Lab ID: 92477011009 Collected: 05/08/20 13:15 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 05/14/20 01:51 05/19/20 20:08 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 20:08 7440-38-2 Barium 170 ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 20:08 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 05/14/20 01:51 05/19/20 20:08 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 05/14/20 01:51 05/19/20 20:08 7440-43-9 Chromium ND ug/L 5.0 3.7 1 05/14/20 01:51 05/19/20 20:08 7440-47-3 Cobalt 6.4 ug/L 5.0 3.6 1 05/14/20 01:51 05/19/20 20:08 7440-48-4 Copper ND ug/L 5.0 4.3 1 05/14/20 01:51 05/19/20 20:08 7440-50-8 Iron 5580 ug/L 50.0 41.5 1 05/14/20 01:51 05/19/20 20:08 7439-89-6 Lead ND ug/L 5.0 4.5 1 05/14/20 01:51 05/19/20 20:08 7439-92-1 Manganese 4510 ug/L 5.0 3.4 1 05/14/20 01:51 05/19/20 20:08 7439-96-5 Nickel ND ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 20:08 7440-02-0 Selenium ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 20:08 7782-49-2 Silver ND ug/L 5.0 2.5 1 05/14/20 01:51 05/19/20 20:08 7440-22-4 Sodium 31400 ug/L 5000 611 1 05/14/20 01:51 05/19/20 20:08 7440-23-5 Tin ND ug/L 5.0 4.7 1 05/14/20 01:51 05/19/20 20:08 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 05/14/20 01:51 05/19/20 20:08 7440-62-2 Zinc ND ug/L 10.0 9.5 1 05/14/20 01:51 05/19/20 20:08 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene Date: 06/09/2020 08:57 AM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 05/20/2017:30 05/21/2011:50 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 0.25J ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 6.2 1 05/19/20 04:09 67-64-1 0.90 1 05/19/20 04:09 107-13-1 0.15 1 05/19/20 04:09 71-43-2 0.34 1 05/19/20 04:09 74-97-5 0.26 1 05/19/20 04:09 75-27-4 0.62 1 05/19/20 04:09 75-25-2 0.62 1 05/19/20 04:09 74-83-9 3.3 1 05/19/20 04:09 78-93-3 0.40 1 05/19/20 04:09 75-15-0 0.22 1 05/19/20 04:09 56-23-5 0.23 1 05/19/20 04:09 108-90-7 0.49 1 05/19/20 04:09 75-00-3 2.3 1 05/19/20 04:09 67-66-3 0.39 1 05/19/20 04:09 74-87-3 0.26 1 05/19/20 04:09 96-12-8 0.41 1 05/19/20 04:09 124-48-1 0.26 1 05/19/20 04:09 106-93-4 0.46 1 05/19/20 04:09 74-95-3 0.29 1 05/19/20 04:09 95-50-1 0.26 1 05/19/20 04:09 106-46-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. IH,IK,L1 Page 35 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: SW-4 Lab ID: 92477011009 Collected: 05/08/20 13:15 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.54 1 05/19/20 04:09 110-57-6 L1,v1 ND ug/L 1.0 0.23 1 05/19/20 04:09 75-71-8 ND ug/L 1.0 0.27 1 05/19/20 04:09 75-34-3 ND ug/L 1.0 0.34 1 05/19/20 04:09 107-06-2 ND ug/L 1.0 0.24 1 05/19/20 04:09 75-35-4 0.32J ug/L 1.0 0.29 1 05/19/20 04:09 156-59-2 ND ug/L 1.0 0.25 1 05/19/20 04:09 156-60-5 ND ug/L 1.0 0.19 1 05/19/20 04:09 78-87-5 ND ug/L 1.0 0.30 1 05/19/20 04:09 10061-01-5 ND ug/L 1.0 0.31 1 05/19/20 04:09 10061-02-6 ND ug/L 1.0 0.26 1 05/19/20 04:09 100-41-4 ND ug/L 5.0 0.57 1 05/19/20 04:09 591-78-6 ND ug/L 20.0 12.5 1 05/19/20 04:09 74-88-4 ND ug/L 5.0 3.7 1 05/19/20 04:09 75-09-2 ND ug/L 5.0 4.5 1 05/19/20 04:09 108-10-1 ND ug/L 1.0 0.27 1 05/19/20 04:09 100-42-5 ND ug/L 1.0 0.34 1 05/19/20 04:09 630-20-6 ND ug/L 1.0 0.22 1 05/19/20 04:09 79-34-5 ND ug/L 1.0 0.16 1 05/19/20 04:09 127-18-4 9.11 ug/L 10.0 1.9 1 05/19/20 04:09 109-99-9 ND ug/L 1.0 0.24 1 05/19/20 04:09 108-88-3 ND ug/L 1.0 0.18 1 05/19/20 04:09 71-55-6 ND ug/L 1.0 0.24 1 05/19/20 04:09 79-00-5 ND ug/L 1.0 0.22 1 05/19/20 04:09 79-01-6 ND ug/L 1.0 0.31 1 05/19/20 04:09 75-69-4 ND ug/L 1.0 0.35 1 05/19/20 04:09 96-18-4 ND ug/L 2.0 1.4 1 05/19/20 04:09 108-05-4 IK ND ug/L 1.0 0.24 1 05/19/20 04:09 75-01-4 ND ug/L 2.0 0.41 1 05/19/20 04:09 179601-23-1 ND ug/L 1.0 0.22 1 05/19/20 04:09 95-47-6 98 % 70-130 1 05/19/20 04:09 460-00-4 94 % 70-130 1 05/19/20 04:09 17060-07-0 100 % 70-130 1 05/19/20 04:09 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 6.6 ug/L 2.0 1.2 1 05/15/2015:28 123-91-1 97 % 50-150 1 05/15/2015:28 17060-07-0 91 % 50-150 1 05/15/2015:28 2037-26-5 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 281000 ug/L 5000 5000 1 05/16/20 02:39 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 36 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: SW-4 Parameters Lab ID: 92477011009 Collected: 05/08/20 13:15 Report Results Units Limit MDL DF Received: 05/08/20 17:07 Matrix: Water Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville Total Dissolved Solids 471000 ug/L 25000 25000 1 05/12/20 23:43 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 05/12/20 20:48 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 68200 ug/L 1000 500 1 05/14/20 07:28 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 42200 ug/L 2000 1000 2 05/13/20 20:39 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 05/18/2013:48 05/19/2012:22 57-12-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 37 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: SW-1 Lab ID: 92477011010 Collected: 05/08/20 13:50 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 05/14/20 01:51 05/19/20 20:12 7440-36-0 Arsenic 8.5J ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 20:12 7440-38-2 Barium 25.6 ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 20:12 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 05/14/20 01:51 05/19/20 20:12 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 05/14/20 01:51 05/19/20 20:12 7440-43-9 Chromium ND ug/L 5.0 3.7 1 05/14/20 01:51 05/19/20 20:12 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 05/14/20 01:51 05/19/20 20:12 7440-48-4 Copper ND ug/L 5.0 4.3 1 05/14/20 01:51 05/19/20 20:12 7440-50-8 Iron 1550 ug/L 50.0 41.5 1 05/14/20 01:51 05/19/20 20:12 7439-89-6 Lead ND ug/L 5.0 4.5 1 05/14/20 01:51 05/19/20 20:12 7439-92-1 Manganese 255 ug/L 5.0 3.4 1 05/14/20 01:51 05/19/20 20:12 7439-96-5 Nickel ND ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 20:12 7440-02-0 Selenium ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 20:12 7782-49-2 Silver ND ug/L 5.0 2.5 1 05/14/20 01:51 05/19/20 20:12 7440-22-4 Sodium 10400 ug/L 5000 611 1 05/14/20 01:51 05/19/20 20:12 7440-23-5 Tin ND ug/L 5.0 4.7 1 05/14/20 01:51 05/19/20 20:12 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 05/14/20 01:51 05/19/20 20:12 7440-62-2 Zinc ND ug/L 10.0 9.5 1 05/14/20 01:51 05/19/20 20:12 7440-66-6 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene Date: 06/09/2020 08:57 AM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 05/20/2017:30 05/21/2011:53 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 6.2 1 05/19/20 03:50 67-64-1 0.90 1 05/19/20 03:50 107-13-1 0.15 1 05/19/20 03:50 71-43-2 0.34 1 05/19/20 03:50 74-97-5 0.26 1 05/19/20 03:50 75-27-4 0.62 1 05/19/20 03:50 75-25-2 0.62 1 05/19/20 03:50 74-83-9 3.3 1 05/19/20 03:50 78-93-3 0.40 1 05/19/20 03:50 75-15-0 0.22 1 05/19/20 03:50 56-23-5 0.23 1 05/19/20 03:50 108-90-7 0.49 1 05/19/20 03:50 75-00-3 2.3 1 05/19/20 03:50 67-66-3 0.39 1 05/19/20 03:50 74-87-3 0.26 1 05/19/20 03:50 96-12-8 0.41 1 05/19/20 03:50 124-48-1 0.26 1 05/19/20 03:50 106-93-4 0.46 1 05/19/20 03:50 74-95-3 0.29 1 05/19/20 03:50 95-50-1 0.26 1 05/19/20 03:50 106-46-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. IH,IK,L1 Page 38 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: SW-1 Lab ID: 92477011010 Collected: 05/08/20 13:50 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.54 1 05/19/20 03:50 110-57-6 L1,v1 ND ug/L 1.0 0.23 1 05/19/20 03:50 75-71-8 ND ug/L 1.0 0.27 1 05/19/20 03:50 75-34-3 ND ug/L 1.0 0.34 1 05/19/20 03:50 107-06-2 ND ug/L 1.0 0.24 1 05/19/20 03:50 75-35-4 ND ug/L 1.0 0.29 1 05/19/20 03:50 156-59-2 ND ug/L 1.0 0.25 1 05/19/20 03:50 156-60-5 ND ug/L 1.0 0.19 1 05/19/20 03:50 78-87-5 ND ug/L 1.0 0.30 1 05/19/20 03:50 10061-01-5 ND ug/L 1.0 0.31 1 05/19/20 03:50 10061-02-6 ND ug/L 1.0 0.26 1 05/19/20 03:50 100-41-4 ND ug/L 5.0 0.57 1 05/19/20 03:50 591-78-6 ND ug/L 20.0 12.5 1 05/19/20 03:50 74-88-4 ND ug/L 5.0 3.7 1 05/19/20 03:50 75-09-2 ND ug/L 5.0 4.5 1 05/19/20 03:50 108-10-1 ND ug/L 1.0 0.27 1 05/19/20 03:50 100-42-5 ND ug/L 1.0 0.34 1 05/19/20 03:50 630-20-6 ND ug/L 1.0 0.22 1 05/19/20 03:50 79-34-5 ND ug/L 1.0 0.16 1 05/19/20 03:50 127-18-4 ND ug/L 10.0 1.9 1 05/19/20 03:50 109-99-9 ND ug/L 1.0 0.24 1 05/19/20 03:50 108-88-3 ND ug/L 1.0 0.18 1 05/19/20 03:50 71-55-6 ND ug/L 1.0 0.24 1 05/19/20 03:50 79-00-5 ND ug/L 1.0 0.22 1 05/19/20 03:50 79-01-6 ND ug/L 1.0 0.31 1 05/19/20 03:50 75-69-4 ND ug/L 1.0 0.35 1 05/19/20 03:50 96-18-4 ND ug/L 2.0 1.4 1 05/19/20 03:50 108-05-4 ND ug/L 1.0 0.24 1 05/19/20 03:50 75-01-4 ND ug/L 2.0 0.41 1 05/19/20 03:50 179601-23-1 ND ug/L 1.0 0.22 1 05/19/20 03:50 95-47-6 98 % 70-130 1 05/19/20 03:50 460-00-4 94 % 70-130 1 05/19/20 03:50 17060-07-0 100 % 70-130 1 05/19/20 03:50 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 1.2 1 05/15/2015:48 123-91-1 116 % 50-150 1 05/15/2015:48 17060-07-0 88 % 50-150 1 05/15/2015:48 2037-26-5 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 40100 ug/L 5000 5000 1 05/16/20 02:56 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 39 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: SW-1 Parameters Lab ID: 92477011010 Collected: 05/08/20 13:50 Report Results Units Limit MDL DF Received: 05/08/20 17:07 Matrix: Water Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville Total Dissolved Solids 76000 ug/L 25000 25000 1 05/12/20 23:43 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 05/12/20 20:48 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 533J ug/L 1000 500 1 05/14/20 07:43 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 12100 ug/L 1000 500 1 05/13/20 20:21 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 05/20/2010:03 05/20/2017:20 57-12-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 40 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: TRIP BLANK Lab ID: 92477011011 Collected: 05/08/20 00:00 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 6.2 1 05/19/20 02:54 67-64-1 ND ug/L 10.0 0.90 1 05/19/20 02:54 107-13-1 ND ug/L 1.0 0.15 1 05/19/20 02:54 71-43-2 ND ug/L 1.0 0.34 1 05/19/20 02:54 74-97-5 ND ug/L 1.0 0.26 1 05/19/20 02:54 75-27-4 ND ug/L 1.0 0.62 1 05/19/20 02:54 75-25-2 ND ug/L 2.0 0.62 1 05/19/20 02:54 74-83-9 ND ug/L 5.0 3.3 1 05/19/20 02:54 78-93-3 ND ug/L 2.0 0.40 1 05/19/20 02:54 75-15-0 ND ug/L 1.0 0.22 1 05/19/20 02:54 56-23-5 ND ug/L 1.0 0.23 1 05/19/20 02:54 108-90-7 ND ug/L 1.0 0.49 1 05/19/20 02:54 75-00-3 ND ug/L 5.0 2.3 1 05/19/20 02:54 67-66-3 ND ug/L 1.0 0.39 1 05/19/20 02:54 74-87-3 ND ug/L 5.0 0.26 1 05/19/20 02:54 96-12-8 ND ug/L 1.0 0.41 1 05/19/20 02:54 124-48-1 ND ug/L 1.0 0.26 1 05/19/20 02:54 106-93-4 ND ug/L 1.0 0.46 1 05/19/20 02:54 74-95-3 ND ug/L 1.0 0.29 1 05/19/20 02:54 95-50-1 ND ug/L 1.0 0.26 1 05/19/20 02:54 106-46-7 ND ug/L 1.0 0.54 1 05/19/20 02:54 110-57-6 ND ug/L 1.0 0.23 1 05/19/20 02:54 75-71-8 ND ug/L 1.0 0.27 1 05/19/20 02:54 75-34-3 ND ug/L 1.0 0.34 1 05/19/20 02:54 107-06-2 ND ug/L 1.0 0.24 1 05/19/20 02:54 75-35-4 ND ug/L 1.0 0.29 1 05/19/20 02:54 156-59-2 ND ug/L 1.0 0.25 1 05/19/20 02:54 156-60-5 ND ug/L 1.0 0.19 1 05/19/20 02:54 78-87-5 ND ug/L 1.0 0.30 1 05/19/20 02:54 10061-01-5 ND ug/L 1.0 0.31 1 05/19/20 02:54 10061-02-6 ND ug/L 1.0 0.26 1 05/19/20 02:54 100-41-4 ND ug/L 5.0 0.57 1 05/19/20 02:54 591-78-6 ND ug/L 20.0 12.5 1 05/19/20 02:54 74-88-4 ND ug/L 5.0 3.7 1 05/19/20 02:54 75-09-2 ND ug/L 5.0 4.5 1 05/19/20 02:54 108-10-1 ND ug/L 1.0 0.27 1 05/19/20 02:54 100-42-5 ND ug/L 1.0 0.34 1 05/19/20 02:54 630-20-6 ND ug/L 1.0 0.22 1 05/19/20 02:54 79-34-5 ND ug/L 1.0 0.16 1 05/19/20 02:54 127-18-4 ND ug/L 10.0 1.9 1 05/19/20 02:54 109-99-9 ND ug/L 1.0 0.24 1 05/19/20 02:54 108-88-3 ND ug/L 1.0 0.18 1 05/19/20 02:54 71-55-6 ND ug/L 1.0 0.24 1 05/19/20 02:54 79-00-5 ND ug/L 1.0 0.22 1 05/19/20 02:54 79-01-6 ND ug/L 1.0 0.31 1 05/19/20 02:54 75-69-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. IH,IK,L1 L1,v1 Page 41 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: TRIP BLANK Lab ID: 92477011011 Collected: 05/08/20 00:00 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,2,3-Trichloropropane ND ug/L 1.0 0.35 1 05/19/20 02:54 96-18-4 Vinyl acetate ND ug/L 2.0 1.4 1 05/19/20 02:54 108-05-4 IK Vinyl chloride ND ug/L 1.0 0.24 1 05/19/20 02:54 75-01-4 m&p-Xylene ND ug/L 2.0 0.41 1 05/19/20 02:54 179601-23-1 o-Xylene ND ug/L 1.0 0.22 1 05/19/20 02:54 95-47-6 Surrogates 4-Bromofluorobenzene (S) 100 % 70-130 1 05/19/20 02:54 460-00-4 1,2-Dichloroethane-d4 (S) 93 % 70-130 1 05/19/20 02:54 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 05/19/20 02:54 2037-26-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 42 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MWAR Lab ID: 92477008001 Collected: 05/06/20 14:15 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Chlorinated Herb. (GC) 8151 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND ug/L 2.00 0.547 1 05/13/20 18:19 05/15/20 21:28 94-75-7 2,4,5-TP (Silvex) ND ug/L 2.00 0.335 1 05/13/20 18:19 05/15/20 21:28 93-72-1 Surrogates 2,4-DCAA (S) 74.8 % 14.0-158 1 05/13/20 18:19 05/15/20 21:28 19719-28-9 8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Aldrin ND ug/L 0.050 0.022 1 05/12/20 21:32 05/14/20 14:42 309-00-2 M1,R1 alpha-BHC ND ug/L 0.050 0.019 1 05/12/20 21:32 05/14/20 14:42 319-84-6 M1 delta-BHC ND ug/L 0.050 0.020 1 05/12/20 21:32 05/14/20 14:42 319-86-8 M1 4,4'-DDD ND ug/L 0.050 0.0069 1 05/12/20 21:32 05/14/20 14:42 72-54-8 M1 4,4'-DDT ND ug/L 0.050 0.018 1 05/12/20 21:32 05/14/20 14:42 50-29-3 M1 Endosulfan I ND ug/L 0.050 0.0094 1 05/12/20 21:32 05/14/20 14:42 959-98-8 M1 Endosulfan 11 ND ug/L 0.050 0.0065 1 05/12/20 21:32 05/14/20 14:42 33213-65-9 M1 Endrin ND ug/L 0.050 0.0089 1 05/12/20 21:32 05/14/20 14:42 72-20-8 M1 Endrin aldehyde ND ug/L 0.050 0.013 1 05/12/20 21:32 05/14/20 14:42 7421-93-4 M1 Heptachlor ND ug/L 0.050 0.016 1 05/12/20 21:32 05/14/20 14:42 76-44-8 M1,R1 Heptachlor epoxide ND ug/L 0.050 0.0097 1 05/12/20 21:32 05/14/20 14:42 1024-57-3 M1,R1 Methoxychlor ND ug/L 0.15 0.033 1 05/12/20 21:32 05/14/20 14:42 72-43-5 M1 Surrogates Tetrachloro-m-xylene (S) 64 % 10-130 1 05/12/20 21:32 05/14/20 14:42 877-09-8 Decachlorobiphenyl (S) 133 % 10-130 1 05/12/20 21:32 05/14/20 14:42 2051-24-3 S3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 05/14/20 01:51 05/21/20 03:26 7440-36-0 Arsenic 5.8J ug/L 10.0 4.7 1 05/14/20 01:51 05/21/20 03:26 7440-38-2 Barium 290 ug/L 5.0 3.5 1 05/14/20 01:51 05/21/20 03:26 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 05/14/20 01:51 05/21/20 03:26 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 05/14/20 01:51 05/21/20 03:26 7440-43-9 Chromium ND ug/L 5.0 3.7 1 05/14/20 01:51 05/21/20 03:26 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 05/14/20 01:51 05/21/20 03:26 7440-48-4 Copper ND ug/L 5.0 4.3 1 05/14/20 01:51 05/21/20 03:26 7440-50-8 Iron ND ug/L 50.0 41.5 1 05/14/20 01:51 05/21/20 03:26 7439-89-6 Lead ND ug/L 5.0 4.5 1 05/14/20 01:51 05/21/20 03:26 7439-92-1 Manganese 31.4 ug/L 5.0 3.4 1 05/14/20 01:51 05/21/20 03:26 7439-96-5 Nickel ND ug/L 5.0 3.5 1 05/14/20 01:51 05/21/20 03:26 7440-02-0 Selenium ND ug/L 10.0 4.7 1 05/14/20 01:51 05/21/20 03:26 7782-49-2 Silver ND ug/L 5.0 2.5 1 05/14/20 01:51 05/21/20 03:26 7440-22-4 Sodium 16800 ug/L 5000 611 1 05/14/20 01:51 05/21/20 03:26 7440-23-5 Tin ND ug/L 5.0 4.7 1 05/14/20 01:51 05/21/20 03:26 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 05/14/20 01:51 05/21/20 03:26 7440-62-2 Zinc ND ug/L 10.0 9.5 1 05/14/20 01:51 05/21/20 03:26 7440-66-6 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 43 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MWAR Lab ID: 92477008001 Collected: 05/06/20 14:15 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury 3.3 ug/L 0.20 0.12 1 05/15/2011:45 05/15/2018:09 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)anthracene ND ug/L 10.0 1.5 1 05/12/20 18:13 05/19/20 20:31 56-55-3 Chrysene ND ug/L 10.0 1.4 1 05/12/20 18:13 05/19/20 20:31 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 1.6 1 05/12/20 18:13 05/19/20 20:31 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 6.0 2.0 1 05/12/20 18:13 05/19/20 20:31 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 1.7 1 05/12/20 18:13 05/19/20 20:31 193-39-5 Surrogates Nitrobenzene-d5 (S) 91 % 13-130 1 05/12/20 18:13 05/19/20 20:31 4165-60-0 2-Fluorobiphenyl (S) 98 % 13-130 1 05/12/20 18:13 05/19/20 20:31 321-60-8 Terphenyl-d14 (S) 116 % 25-130 1 05/12/20 18:13 05/19/20 20:31 1718-51-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 05/19/20 08:04 67-64-1 Acrylonitrile ND ug/L 10.0 0.90 1 05/19/20 08:04 107-13-1 Benzene ND ug/L 1.0 0.15 1 05/19/20 08:04 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 05/19/20 08:04 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 05/19/20 08:04 75-27-4 Bromoform ND ug/L 1.0 0.62 1 05/19/20 08:04 75-25-2 Bromomethane ND ug/L 2.0 0.62 1 05/19/20 08:04 74-83-9 IK,v2 2-Butanone (MEK) ND ug/L 5.0 3.3 1 05/19/20 08:04 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 05/19/20 08:04 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 05/19/20 08:04 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 05/19/20 08:04 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 05/19/20 08:04 75-00-3 IK Chloroform ND ug/L 5.0 2.3 1 05/19/20 08:04 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 05/19/20 08:04 74-87-3 IK 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 05/19/20 08:04 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 05/19/20 08:04 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 05/19/20 08:04 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 05/19/20 08:04 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.29 1 05/19/20 08:04 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 05/19/20 08:04 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 05/19/20 08:04 110-57-6 IH Dichlorodifluoromethane ND ug/L 1.0 0.23 1 05/19/20 08:04 75-71-8 IK 1,1-Dichloroethane ND ug/L 1.0 0.27 1 05/19/20 08:04 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.34 1 05/19/20 08:04 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 05/19/20 08:04 75-35-4 cis-1,2-Dichloroethene 1.2 ug/L 1.0 0.29 1 05/19/20 08:04 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.25 1 05/19/20 08:04 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.19 1 05/19/20 08:04 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 0.30 1 05/19/20 08:04 10061-01-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 44 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MWAR Lab ID: 92477008001 Collected: 05/06/20 14:15 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) i:Y�*111 e7 �, Riy&i I �, 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 20.0 ND ug/L 5.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 97 % 70-130 116 % 70-130 103 % 70-130 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 97 % 50-150 95 % 50-150 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 86600 ug/L 5000 Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville 172000 ug/L 25000 Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville ND ug/L 100 0.31 1 05/19/20 08:04 10061-02-6 0.26 1 05/19/20 08:04 100-41-4 0.57 1 05/19/20 08:04 591-78-6 12.5 1 05/19/20 08:04 74-88-4 v2 3.7 1 05/19/20 08:04 75-09-2 4.5 1 05/19/20 08:04 108-10-1 v1 0.27 1 05/19/20 08:04 100-42-5 0.34 1 05/19/20 08:04 630-20-6 0.22 1 05/19/20 08:04 79-34-5 0.16 1 05/19/20 08:04 127-18-4 1.9 1 05/19/20 08:04 109-99-9 0.24 1 05/19/20 08:04 108-88-3 0.18 1 05/19/20 08:04 71-55-6 0.24 1 05/19/20 08:04 79-00-5 0.22 1 05/19/20 08:04 79-01-6 0.31 1 05/19/20 08:04 75-69-4 IK 0.35 1 05/19/20 08:04 96-18-4 1.4 1 05/19/20 08:04 108-05-4 v1 0.24 1 05/19/20 08:04 75-01-4 IK 0.41 1 05/19/20 08:04 179601-23-1 0.22 1 05/19/20 08:04 95-47-6 1 05/19/20 08:04 460-00-4 1 05/19/20 08:04 17060-07-0 1 05/19/20 08:04 2037-26-5 1.2 1 05/15/20 02:56 123-91-1 1 05/15/20 02:56 17060-07-0 1 05/15/20 02:56 2037-26-5 5000 1 05/15/20 21:55 25000 1 F�i][i>il REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 05/12/20 23:18 05/12/20 20:08 18496-25-8 Page 45 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MWAR Parameters Lab ID: 92477008001 Collected: 05/06/20 14:15 Report Results Units Limit MDL DF Received: 05/08/20 17:07 Matrix: Water Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate ND ug/L 1000 500 1 05/14/20 09:22 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 9050 ug/L 1000 500 1 05/12/2019:39 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 05/13/20 09:43 05/14/20 14:56 57-12-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 46 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: FIELD BLANK Lab ID: 92477008002 Collected: 05/06/20 15:08 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Chlorinated Herb. (GC) 8151 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND ug/L 2.00 0.547 1 05/13/20 18:19 05/15/20 21:44 94-75-7 2,4,5-TP (Silvex) ND ug/L 2.00 0.335 1 05/13/20 18:19 05/15/20 21:44 93-72-1 Surrogates 2,4-DCAA (S) 64.9 % 14.0-158 1 05/13/20 18:19 05/15/20 21:44 19719-28-9 8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Aldrin ND ug/L 0.050 0.022 1 05/12/20 21:32 05/14/20 15:26 309-00-2 alpha-BHC ND ug/L 0.050 0.019 1 05/12/20 21:32 05/14/20 15:26 319-84-6 delta-BHC ND ug/L 0.050 0.020 1 05/12/20 21:32 05/14/20 15:26 319-86-8 4,4'-DDD ND ug/L 0.050 0.0069 1 05/12/20 21:32 05/14/20 15:26 72-54-8 4,4'-DDT ND ug/L 0.050 0.018 1 05/12/20 21:32 05/14/20 15:26 50-29-3 Endosulfan I ND ug/L 0.050 0.0094 1 05/12/20 21:32 05/14/20 15:26 959-98-8 Endosulfan 11 ND ug/L 0.050 0.0065 1 05/12/20 21:32 05/14/20 15:26 33213-65-9 Endrin ND ug/L 0.050 0.0089 1 05/12/20 21:32 05/14/20 15:26 72-20-8 Endrin aldehyde ND ug/L 0.050 0.013 1 05/12/20 21:32 05/14/20 15:26 7421-93-4 Heptachlor ND ug/L 0.050 0.016 1 05/12/20 21:32 05/14/20 15:26 76-44-8 Heptachlor epoxide ND ug/L 0.050 0.0097 1 05/12/20 21:32 05/14/20 15:26 1024-57-3 Methoxychlor ND ug/L 0.15 0.033 1 05/12/20 21:32 05/14/20 15:26 72-43-5 Surrogates Tetrachloro-m-xylene (S) 104 % 10-130 1 05/12/20 21:32 05/14/20 15:26 877-09-8 Decachlorobiphenyl (S) 116 % 10-130 1 05/12/20 21:32 05/14/20 15:26 2051-24-3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 05/14/20 01:51 05/21/20 03:30 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 05/14/20 01:51 05/21/20 03:30 7440-38-2 Barium ND ug/L 5.0 3.5 1 05/14/20 01:51 05/21/20 03:30 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 05/14/20 01:51 05/21/20 03:30 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 05/14/20 01:51 05/21/20 03:30 7440-43-9 Chromium ND ug/L 5.0 3.7 1 05/14/20 01:51 05/21/20 03:30 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 05/14/20 01:51 05/21/20 03:30 7440-48-4 Copper ND ug/L 5.0 4.3 1 05/14/20 01:51 05/21/20 03:30 7440-50-8 Iron ND ug/L 50.0 41.5 1 05/14/20 01:51 05/21/20 03:30 7439-89-6 Lead ND ug/L 5.0 4.5 1 05/14/20 01:51 05/21/20 03:30 7439-92-1 Manganese ND ug/L 5.0 3.4 1 05/14/20 01:51 05/21/20 03:30 7439-96-5 Nickel ND ug/L 5.0 3.5 1 05/14/20 01:51 05/21/20 03:30 7440-02-0 Selenium ND ug/L 10.0 4.7 1 05/14/20 01:51 05/21/20 03:30 7782-49-2 Silver ND ug/L 5.0 2.5 1 05/14/20 01:51 05/21/20 03:30 7440-22-4 Sodium ND ug/L 5000 611 1 05/14/20 01:51 05/21/20 03:30 7440-23-5 Tin ND ug/L 5.0 4.7 1 05/14/20 01:51 05/21/20 03:30 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 05/14/20 01:51 05/21/20 03:30 7440-62-2 Zinc ND ug/L 10.0 9.5 1 05/14/20 01:51 05/21/20 03:30 7440-66-6 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 47 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: FIELD BLANK Lab ID: 92477008002 Collected: 05/06/20 15:08 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 05/15/2011:45 05/15/2018:11 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)anthracene ND ug/L 10.0 1.5 1 05/12/20 18:13 05/19/20 20:56 56-55-3 Chrysene ND ug/L 10.0 1.4 1 05/12/20 18:13 05/19/20 20:56 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 1.6 1 05/12/20 18:13 05/19/20 20:56 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 6.0 2.0 1 05/12/20 18:13 05/19/20 20:56 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 1.7 1 05/12/20 18:13 05/19/20 20:56 193-39-5 Surrogates Nitrobenzene-d5 (S) 93 % 13-130 1 05/12/20 18:13 05/19/20 20:56 4165-60-0 2-Fluorobiphenyl (S) 94 % 13-130 1 05/12/20 18:13 05/19/20 20:56 321-60-8 Terphenyl-d14 (S) 130 % 25-130 1 05/12/20 18:13 05/19/20 20:56 1718-51-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 05/19/20 01:37 67-64-1 Acrylonitrile ND ug/L 10.0 0.90 1 05/19/20 01:37 107-13-1 Benzene ND ug/L 1.0 0.15 1 05/19/20 01:37 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 05/19/20 01:37 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 05/19/20 01:37 75-27-4 Bromoform ND ug/L 1.0 0.62 1 05/19/20 01:37 75-25-2 Bromomethane ND ug/L 2.0 0.62 1 05/19/20 01:37 74-83-9 IK,v2 2-Butanone (MEK) ND ug/L 5.0 3.3 1 05/19/20 01:37 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 05/19/20 01:37 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 05/19/20 01:37 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 05/19/20 01:37 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 05/19/20 01:37 75-00-3 IK Chloroform ND ug/L 5.0 2.3 1 05/19/20 01:37 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 05/19/20 01:37 74-87-3 IK 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 05/19/20 01:37 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 05/19/20 01:37 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 05/19/20 01:37 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 05/19/20 01:37 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.29 1 05/19/20 01:37 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 05/19/20 01:37 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 05/19/20 01:37 110-57-6 IH Dichlorodifluoromethane ND ug/L 1.0 0.23 1 05/19/20 01:37 75-71-8 IK 1,1-Dichloroethane ND ug/L 1.0 0.27 1 05/19/20 01:37 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.34 1 05/19/20 01:37 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 05/19/20 01:37 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.29 1 05/19/20 01:37 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.25 1 05/19/20 01:37 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.19 1 05/19/20 01:37 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 0.30 1 05/19/20 01:37 10061-01-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 48 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: FIELD BLANK Lab ID: 92477008002 Collected: 05/06/20 15:08 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) i:Y�*111 e7 �, Riy&i I �, 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 20.0 ND ug/L 5.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 97 % 70-130 102 % 70-130 102 % 70-130 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 98 % 50-150 91 % 50-150 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville ND ug/L 5000 Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville ND ug/L 25000 Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville ND ug/L 100 0.31 1 05/19/20 01:37 10061-02-6 0.26 1 05/19/20 01:37 100-41-4 0.57 1 05/19/20 01:37 591-78-6 12.5 1 05/19/20 01:37 74-88-4 v2 3.7 1 05/19/20 01:37 75-09-2 4.5 1 05/19/20 01:37 108-10-1 v1 0.27 1 05/19/20 01:37 100-42-5 0.34 1 05/19/20 01:37 630-20-6 0.22 1 05/19/20 01:37 79-34-5 0.16 1 05/19/20 01:37 127-18-4 1.9 1 05/19/20 01:37 109-99-9 0.24 1 05/19/20 01:37 108-88-3 0.18 1 05/19/20 01:37 71-55-6 0.24 1 05/19/20 01:37 79-00-5 0.22 1 05/19/20 01:37 79-01-6 0.31 1 05/19/20 01:37 75-69-4 IK 0.35 1 05/19/20 01:37 96-18-4 1.4 1 05/19/20 01:37 108-05-4 v1 0.24 1 05/19/20 01:37 75-01-4 IK 0.41 1 05/19/20 01:37 179601-23-1 0.22 1 05/19/20 01:37 95-47-6 1 05/19/20 01:37 460-00-4 1 05/19/20 01:37 17060-07-0 1 05/19/20 01:37 2037-26-5 1.2 1 05/14/20 22:39 123-91-1 1 05/14/20 22:39 17060-07-0 1 05/14/20 22:39 2037-26-5 5000 1 05/15/20 22:05 25000 1 F�i][i>il REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 05/12/20 23:18 05/12/20 20:08 18496-25-8 Page 49 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: FIELD BLANK Parameters Lab ID: 92477008002 Collected: 05/06/20 15:08 Report Results Units Limit MDL DF Received: 05/08/20 17:07 Matrix: Water Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate ND ug/L 1000 500 1 05/14/2010:07 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride ND ug/L 1000 500 1 05/12/2019:40 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 05/18/2013:47 05/19/2011:48 57-12-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 50 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-4R Lab ID: 92477008003 Collected: 05/07/20 12:35 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Chlorinated Herb. (GC) 8151 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND ug/L 2.00 0.547 1 05/13/20 18:19 05/15/20 22:00 94-75-7 2,4,5-TP (Silvex) ND ug/L 2.00 0.335 1 05/13/20 18:19 05/15/20 22:00 93-72-1 Surrogates 2,4-DCAA (S) 58.4 % 14.0-158 1 05/13/20 18:19 05/15/20 22:00 19719-28-9 8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Aldrin ND ug/L 0.050 0.022 1 05/12/20 21:32 05/14/20 16:39 309-00-2 alpha-BHC ND ug/L 0.050 0.019 1 05/12/20 21:32 05/14/20 16:39 319-84-6 delta-BHC ND ug/L 0.050 0.020 1 05/12/20 21:32 05/14/20 16:39 319-86-8 4,4'-DDD ND ug/L 0.050 0.0069 1 05/12/20 21:32 05/14/20 16:39 72-54-8 4,4'-DDT ND ug/L 0.050 0.018 1 05/12/20 21:32 05/14/20 16:39 50-29-3 Endosulfan I ND ug/L 0.050 0.0094 1 05/12/20 21:32 05/14/20 16:39 959-98-8 Endosulfan 11 ND ug/L 0.050 0.0065 1 05/12/20 21:32 05/14/20 16:39 33213-65-9 Endrin ND ug/L 0.050 0.0089 1 05/12/20 21:32 05/14/20 16:39 72-20-8 Endrin aldehyde ND ug/L 0.050 0.013 1 05/12/20 21:32 05/14/20 16:39 7421-93-4 Heptachlor ND ug/L 0.050 0.016 1 05/12/20 21:32 05/14/20 16:39 76-44-8 Heptachlor epoxide ND ug/L 0.050 0.0097 1 05/12/20 21:32 05/14/20 16:39 1024-57-3 Methoxychlor ND ug/L 0.15 0.033 1 05/12/20 21:32 05/14/20 16:39 72-43-5 Surrogates Tetrachloro-m-xylene (S) 134 % 10-130 1 05/12/20 21:32 05/14/20 16:39 877-09-8 S3 Decachlorobiphenyl (S) 107 % 10-130 1 05/12/20 21:32 05/14/20 16:39 2051-24-3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 05/14/20 01:51 05/21/20 03:34 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 05/14/20 01:51 05/21/20 03:34 7440-38-2 Barium 176 ug/L 5.0 3.5 1 05/14/20 01:51 05/21/20 03:34 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 05/14/20 01:51 05/21/20 03:34 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 05/14/20 01:51 05/21/20 03:34 7440-43-9 Chromium ND ug/L 5.0 3.7 1 05/14/20 01:51 05/21/20 03:34 7440-47-3 Cobalt 88.8 ug/L 5.0 3.6 1 05/14/20 01:51 05/21/20 03:34 7440-48-4 Copper ND ug/L 5.0 4.3 1 05/14/20 01:51 05/21/20 03:34 7440-50-8 Iron 1080 ug/L 50.0 41.5 1 05/14/20 01:51 05/21/20 03:34 7439-89-6 Lead ND ug/L 5.0 4.5 1 05/14/20 01:51 05/21/20 03:34 7439-92-1 Manganese 1080 ug/L 5.0 3.4 1 05/14/20 01:51 05/21/20 03:34 7439-96-5 Nickel 8.0 ug/L 5.0 3.5 1 05/14/20 01:51 05/21/20 03:34 7440-02-0 Selenium ND ug/L 10.0 4.7 1 05/14/20 01:51 05/21/20 03:34 7782-49-2 Silver ND ug/L 5.0 2.5 1 05/14/20 01:51 05/21/20 03:34 7440-22-4 Sodium 73800 ug/L 5000 611 1 05/14/20 01:51 05/21/20 03:34 7440-23-5 Tin ND ug/L 5.0 4.7 1 05/14/20 01:51 05/21/20 03:34 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 05/14/20 01:51 05/21/20 03:34 7440-62-2 Zinc ND ug/L 10.0 9.5 1 05/14/20 01:51 05/21/20 03:34 7440-66-6 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 51 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-4R Lab ID: 92477008003 Collected: 05/07/20 12:35 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 05/15/2011:45 05/15/2018:14 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)anthracene ND ug/L 10.0 1.5 1 05/12/20 18:13 05/19/20 21:22 56-55-3 Chrysene ND ug/L 10.0 1.4 1 05/12/20 18:13 05/19/20 21:22 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 1.6 1 05/12/20 18:13 05/19/20 21:22 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 6.0 2.0 1 05/12/20 18:13 05/19/20 21:22 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 1.7 1 05/12/20 18:13 05/19/20 21:22 193-39-5 Surrogates Nitrobenzene-d5 (S) 99 % 13-130 1 05/12/20 18:13 05/19/20 21:22 4165-60-0 2-Fluorobiphenyl (S) 99 % 13-130 1 05/12/20 18:13 05/19/20 21:22 321-60-8 Terphenyl-d14 (S) 111 % 25-130 1 05/12/20 18:13 05/19/20 21:22 1718-51-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 05/19/20 05:43 67-64-1 Acrylonitrile ND ug/L 10.0 0.90 1 05/19/20 05:43 107-13-1 Benzene ND ug/L 1.0 0.15 1 05/19/20 05:43 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 05/19/20 05:43 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 05/19/20 05:43 75-27-4 Bromoform ND ug/L 1.0 0.62 1 05/19/20 05:43 75-25-2 Bromomethane ND ug/L 2.0 0.62 1 05/19/20 05:43 74-83-9 IH,IK,L1 2-Butanone (MEK) ND ug/L 5.0 3.3 1 05/19/20 05:43 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 05/19/20 05:43 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 05/19/20 05:43 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 05/19/20 05:43 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 05/19/20 05:43 75-00-3 Chloroform ND ug/L 5.0 2.3 1 05/19/20 05:43 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 05/19/20 05:43 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 05/19/20 05:43 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 05/19/20 05:43 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 05/19/20 05:43 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 05/19/20 05:43 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.29 1 05/19/20 05:43 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 05/19/20 05:43 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 05/19/20 05:43 110-57-6 L1,v1 Dichlorodifluoromethane ND ug/L 1.0 0.23 1 05/19/20 05:43 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.27 1 05/19/20 05:43 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.34 1 05/19/20 05:43 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 05/19/20 05:43 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.29 1 05/19/20 05:43 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.25 1 05/19/20 05:43 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.19 1 05/19/20 05:43 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 0.30 1 05/19/20 05:43 10061-01-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 52 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-4R Lab ID: 92477008003 Collected: 05/07/20 12:35 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) i:Y�*111 e7 �, Riy&i I �, 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 20.0 ND ug/L 5.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 11.4 ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 98 % 70-130 95 % 70-130 99 % 70-130 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 4.7 ug/L 2.0 100 % 50-150 90 % 50-150 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 517000 ug/L 5000 Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville 854000 ug/L 50000 Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville ND ug/L 100 0.31 1 05/19/20 05:43 10061-02-6 0.26 1 05/19/20 05:43 100-41-4 0.57 1 05/19/20 05:43 591-78-6 12.5 1 05/19/20 05:43 74-88-4 3.7 1 05/19/20 05:43 75-09-2 4.5 1 05/19/20 05:43 108-10-1 0.27 1 05/19/20 05:43 100-42-5 0.34 1 05/19/20 05:43 630-20-6 0.22 1 05/19/20 05:43 79-34-5 0.16 1 05/19/20 05:43 127-18-4 1.9 1 05/19/20 05:43 109-99-9 0.24 1 05/19/20 05:43 108-88-3 0.18 1 05/19/20 05:43 71-55-6 0.24 1 05/19/20 05:43 79-00-5 0.22 1 05/19/20 05:43 79-01-6 0.31 1 05/19/20 05:43 75-69-4 0.35 1 05/19/20 05:43 96-18-4 1.4 1 05/19/20 05:43 108-05-4 IK 0.24 1 05/19/20 05:43 75-01-4 0.41 1 05/19/20 05:43 179601-23-1 0.22 1 05/19/20 05:43 95-47-6 1 05/19/20 05:43 460-00-4 1 05/19/20 05:43 17060-07-0 1 05/19/20 05:43 2037-26-5 1.2 1 05/15/20 18:45 123-91-1 1 05/15/20 18:45 17060-07-0 1 05/15/20 18:45 2037-26-5 5000 1 05/18/20 19:36 50000 1 F�i][i>il REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 05/12/20 23:20 05/12/20 20:43 18496-25-8 M1 Page 53 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-4R Parameters Lab ID: 92477008003 Collected: 05/07/20 12:35 Report Results Units Limit MDL DF Received: 05/08/20 17:07 Matrix: Water Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 162000 ug/L 3000 1500 3 05/15/2011:10 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 42100 ug/L 2000 1000 2 05/12/2019:50 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 05/18/2013:48 05/19/2012:16 57-12-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 54 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-2R Lab ID: 92477008004 Collected: 05/08/20 08:45 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Chlorinated Herb. (GC) 8151 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND ug/L 2.00 0.547 1 05/13/20 18:19 05/15/20 22:16 94-75-7 2,4,5-TP (Silvex) ND ug/L 2.00 0.335 1 05/13/20 18:19 05/15/20 22:16 93-72-1 Surrogates 2,4-DCAA (S) 272 % 14.0-158 1 05/13/20 18:19 05/15/20 22:16 19719-28-9 ST 8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Aldrin ND ug/L 0.050 0.022 1 05/12/20 21:32 05/14/20 18:21 309-00-2 alpha-BHC ND ug/L 0.050 0.019 1 05/12/20 21:32 05/14/20 18:21 319-84-6 delta-BHC ND ug/L 0.050 0.020 1 05/12/20 21:32 05/14/20 18:21 319-86-8 4,4'-DDD ND ug/L 0.050 0.0069 1 05/12/20 21:32 05/14/20 18:21 72-54-8 4,4'-DDT ND ug/L 0.050 0.018 1 05/12/20 21:32 05/14/20 18:21 50-29-3 Endosulfan I ND ug/L 0.050 0.0094 1 05/12/20 21:32 05/14/20 18:21 959-98-8 Endosulfan 11 ND ug/L 0.050 0.0065 1 05/12/20 21:32 05/14/20 18:21 33213-65-9 Endrin ND ug/L 0.050 0.0089 1 05/12/20 21:32 05/14/20 18:21 72-20-8 Endrin aldehyde ND ug/L 0.050 0.013 1 05/12/20 21:32 05/14/20 18:21 7421-93-4 Heptachlor ND ug/L 0.050 0.016 1 05/12/20 21:32 05/14/20 18:21 76-44-8 Heptachlor epoxide ND ug/L 0.050 0.0097 1 05/12/20 21:32 05/14/20 18:21 1024-57-3 Methoxychlor ND ug/L 0.15 0.033 1 05/12/20 21:32 05/14/20 18:21 72-43-5 Surrogates Tetrachloro-m-xylene (S) 84 % 10-130 1 05/12/20 21:32 05/14/20 18:21 877-09-8 Decachlorobiphenyl (S) 130 % 10-130 1 05/12/20 21:32 05/14/20 18:21 2051-24-3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 05/14/20 01:51 05/21/20 03:37 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 05/14/20 01:51 05/21/20 03:37 7440-38-2 Barium 309 ug/L 5.0 3.5 1 05/14/20 01:51 05/21/20 03:37 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 05/14/20 01:51 05/21/20 03:37 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 05/14/20 01:51 05/21/20 03:37 7440-43-9 Chromium ND ug/L 5.0 3.7 1 05/14/20 01:51 05/21/20 03:37 7440-47-3 Cobalt 29.7 ug/L 5.0 3.6 1 05/14/20 01:51 05/21/20 03:37 7440-48-4 Copper ND ug/L 5.0 4.3 1 05/14/20 01:51 05/21/20 03:37 7440-50-8 Iron 3650 ug/L 50.0 41.5 1 05/14/20 01:51 05/21/20 03:37 7439-89-6 Lead ND ug/L 5.0 4.5 1 05/14/20 01:51 05/21/20 03:37 7439-92-1 Manganese 11300 ug/L 25.0 17.2 5 05/14/20 01:51 05/22/20 12:35 7439-96-5 Nickel 21.1 ug/L 5.0 3.5 1 05/14/20 01:51 05/21/20 03:37 7440-02-0 Selenium ND ug/L 10.0 4.7 1 05/14/20 01:51 05/21/20 03:37 7782-49-2 Silver ND ug/L 5.0 2.5 1 05/14/20 01:51 05/21/20 03:37 7440-22-4 Sodium 65600 ug/L 5000 611 1 05/14/20 01:51 05/21/20 03:37 7440-23-5 Tin ND ug/L 5.0 4.7 1 05/14/20 01:51 05/21/20 03:37 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 05/14/20 01:51 05/21/20 03:37 7440-62-2 Zinc ND ug/L 10.0 9.5 1 05/14/20 01:51 05/21/20 03:37 7440-66-6 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 55 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-2R Lab ID: 92477008004 Collected: 05/08/20 08:45 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 05/15/2011:45 05/15/2018:16 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)anthracene ND ug/L 10.0 1.5 1 05/12/20 18:13 05/19/20 21:47 56-55-3 Chrysene ND ug/L 10.0 1.4 1 05/12/20 18:13 05/19/20 21:47 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 1.6 1 05/12/20 18:13 05/19/20 21:47 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 6.0 2.0 1 05/12/20 18:13 05/19/20 21:47 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 1.7 1 05/12/20 18:13 05/19/20 21:47 193-39-5 Surrogates Nitrobenzene-d5 (S) 83 % 13-130 1 05/12/20 18:13 05/19/20 21:47 4165-60-0 2-Fluorobiphenyl (S) 90 % 13-130 1 05/12/20 18:13 05/19/20 21:47 321-60-8 Terphenyl-d14 (S) 125 % 25-130 1 05/12/20 18:13 05/19/20 21:47 1718-51-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 05/19/20 06:01 67-64-1 Acrylonitrile ND ug/L 10.0 0.90 1 05/19/20 06:01 107-13-1 Benzene 3.4 ug/L 1.0 0.15 1 05/19/20 06:01 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 05/19/20 06:01 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 05/19/20 06:01 75-27-4 Bromoform ND ug/L 1.0 0.62 1 05/19/20 06:01 75-25-2 Bromomethane ND ug/L 2.0 0.62 1 05/19/20 06:01 74-83-9 IH,IK,L1 2-Butanone (MEK) ND ug/L 5.0 3.3 1 05/19/20 06:01 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 05/19/20 06:01 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 05/19/20 06:01 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 05/19/20 06:01 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 05/19/20 06:01 75-00-3 Chloroform ND ug/L 5.0 2.3 1 05/19/20 06:01 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 05/19/20 06:01 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 05/19/20 06:01 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 05/19/20 06:01 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 05/19/20 06:01 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 05/19/20 06:01 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.29 1 05/19/20 06:01 95-50-1 1,4-Dichlorobenzene 0.56.11 ug/L 1.0 0.26 1 05/19/20 06:01 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 05/19/20 06:01 110-57-6 L1,v1 Dichlorodifluoromethane ND ug/L 1.0 0.23 1 05/19/20 06:01 75-71-8 1,1-Dichloroethane 0.46.11 ug/L 1.0 0.27 1 05/19/20 06:01 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.34 1 05/19/20 06:01 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 05/19/20 06:01 75-35-4 cis-1,2-Dichloroethene 0.84.11 ug/L 1.0 0.29 1 05/19/20 06:01 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.25 1 05/19/20 06:01 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.19 1 05/19/20 06:01 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 0.30 1 05/19/20 06:01 10061-01-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 56 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-2R Lab ID: 92477008004 Collected: 05/08/20 08:45 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) i:Y�:f11 e7 �, Riy&i I �, 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 20.0 ND ug/L 5.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 1.1 ug/L 1.0 38.6 ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 1.1 ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 0.991 ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 99 % 70-130 94 % 70-130 99 % 70-130 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 3.9 ug/L 2.0 100 % 50-150 96 % 50-150 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 688000 ug/L 5000 Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville 840000 ug/L 50000 Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville 80.1J ug/L 100 0.31 1 05/19/20 06:01 10061-02-6 0.26 1 05/19/20 06:01 100-41-4 0.57 1 05/19/20 06:01 591-78-6 12.5 1 05/19/20 06:01 74-88-4 3.7 1 05/19/20 06:01 75-09-2 4.5 1 05/19/20 06:01 108-10-1 0.27 1 05/19/20 06:01 100-42-5 0.34 1 05/19/20 06:01 630-20-6 0.22 1 05/19/20 06:01 79-34-5 0.16 1 05/19/20 06:01 127-18-4 1.9 1 05/19/20 06:01 109-99-9 0.24 1 05/19/20 06:01 108-88-3 0.18 1 05/19/20 06:01 71-55-6 0.24 1 05/19/20 06:01 79-00-5 0.22 1 05/19/20 06:01 79-01-6 0.31 1 05/19/20 06:01 75-69-4 0.35 1 05/19/20 06:01 96-18-4 1.4 1 05/19/20 06:01 108-05-4 IK 0.24 1 05/19/20 06:01 75-01-4 0.41 1 05/19/20 06:01 179601-23-1 0.22 1 05/19/20 06:01 95-47-6 1 05/19/20 06:01 460-00-4 1 05/19/20 06:01 17060-07-0 1 05/19/20 06:01 2037-26-5 1.2 1 05/15/20 14:29 123-91-1 1 05/15/20 14:29 17060-07-0 1 05/15/20 14:29 2037-26-5 5000 1 05/18/20 19:45 50000 1 F�i][i>il REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 05/12/20 23:42 05/12/20 20:47 18496-25-8 Page 57 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-2R Parameters Lab ID: 92477008004 Collected: 05/08/20 08:45 Report Results Units Limit MDL DF Received: 05/08/20 17:07 Matrix: Water Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 76400 ug/L 1000 500 1 05/14/2010:36 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 64300 ug/L 3000 1500 3 05/12/2019:41 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 05/18/2013:48 05/19/2012:19 57-12-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 58 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-15 Lab ID: 92477008005 Collected: 05/08/20 11:50 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Chlorinated Herb. (GC) 8151 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND ug/L 2.00 0.547 1 05/15/20 18:43 05/17/20 15:31 94-75-7 2,4,5-TP (Silvex) ND ug/L 2.00 0.335 1 05/15/20 18:43 05/17/20 15:31 93-72-1 Surrogates 2,4-DCAA (S) 62.8 % 14.0-158 1 05/15/20 18:43 05/17/20 15:31 19719-28-9 8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Aldrin ND ug/L 0.050 0.022 1 05/12/20 21:32 05/14/20 18:36 309-00-2 alpha-BHC ND ug/L 0.050 0.019 1 05/12/20 21:32 05/14/20 18:36 319-84-6 delta-BHC ND ug/L 0.050 0.020 1 05/12/20 21:32 05/14/20 18:36 319-86-8 4,4'-DDD ND ug/L 0.050 0.0069 1 05/12/20 21:32 05/14/20 18:36 72-54-8 4,4'-DDT ND ug/L 0.050 0.018 1 05/12/20 21:32 05/14/20 18:36 50-29-3 Endosulfan I ND ug/L 0.050 0.0094 1 05/12/20 21:32 05/14/20 18:36 959-98-8 Endosulfan 11 ND ug/L 0.050 0.0065 1 05/12/20 21:32 05/14/20 18:36 33213-65-9 Endrin ND ug/L 0.050 0.0089 1 05/12/20 21:32 05/14/20 18:36 72-20-8 Endrin aldehyde ND ug/L 0.050 0.013 1 05/12/20 21:32 05/14/20 18:36 7421-93-4 Heptachlor ND ug/L 0.050 0.016 1 05/12/20 21:32 05/14/20 18:36 76-44-8 Heptachlor epoxide ND ug/L 0.050 0.0097 1 05/12/20 21:32 05/14/20 18:36 1024-57-3 Methoxychlor ND ug/L 0.15 0.033 1 05/12/20 21:32 05/14/20 18:36 72-43-5 Surrogates Tetrachloro-m-xylene (S) 125 % 10-130 1 05/12/20 21:32 05/14/20 18:36 877-09-8 Decachlorobiphenyl (S) 138 % 10-130 1 05/12/20 21:32 05/14/20 18:36 2051-24-3 S3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 05/14/20 01:51 05/21/20 03:41 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 05/14/20 01:51 05/21/20 03:41 7440-38-2 Barium 23.8 ug/L 5.0 3.5 1 05/14/20 01:51 05/21/20 03:41 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 05/14/20 01:51 05/21/20 03:41 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 05/14/20 01:51 05/21/20 03:41 7440-43-9 Chromium ND ug/L 5.0 3.7 1 05/14/20 01:51 05/21/20 03:41 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 05/14/20 01:51 05/21/20 03:41 7440-48-4 Copper ND ug/L 5.0 4.3 1 05/14/20 01:51 05/21/20 03:41 7440-50-8 Iron ND ug/L 50.0 41.5 1 05/14/20 01:51 05/21/20 03:41 7439-89-6 Lead ND ug/L 5.0 4.5 1 05/14/20 01:51 05/21/20 03:41 7439-92-1 Manganese 165 ug/L 5.0 3.4 1 05/14/20 01:51 05/21/20 03:41 7439-96-5 Nickel ND ug/L 5.0 3.5 1 05/14/20 01:51 05/21/20 03:41 7440-02-0 Selenium ND ug/L 10.0 4.7 1 05/14/20 01:51 05/21/20 03:41 7782-49-2 Silver ND ug/L 5.0 2.5 1 05/14/20 01:51 05/21/20 03:41 7440-22-4 Sodium 19700 ug/L 5000 611 1 05/14/20 01:51 05/21/20 03:41 7440-23-5 Tin ND ug/L 5.0 4.7 1 05/14/20 01:51 05/21/20 03:41 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 05/14/20 01:51 05/21/20 03:41 7440-62-2 Zinc ND ug/L 10.0 9.5 1 05/14/20 01:51 05/21/20 03:41 7440-66-6 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 59 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-15 Lab ID: 92477008005 Collected: 05/08/20 11:50 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury ND ug/L 0.20 0.12 1 05/20/2017:30 05/21/2011:17 7439-97-6 M1 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)anthracene ND ug/L 10.0 1.5 1 05/12/20 18:13 05/19/20 22:13 56-55-3 Chrysene ND ug/L 10.0 1.4 1 05/12/20 18:13 05/19/20 22:13 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 1.6 1 05/12/20 18:13 05/19/20 22:13 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 6.0 2.0 1 05/12/20 18:13 05/19/20 22:13 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 1.7 1 05/12/20 18:13 05/19/20 22:13 193-39-5 Surrogates Nitrobenzene-d5 (S) 91 % 13-130 1 05/12/20 18:13 05/19/20 22:13 4165-60-0 2-Fluorobiphenyl (S) 86 % 13-130 1 05/12/20 18:13 05/19/20 22:13 321-60-8 Terphenyl-d14 (S) 110 % 25-130 1 05/12/20 18:13 05/19/20 22:13 1718-51-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 05/19/20 06:20 67-64-1 Acrylonitrile ND ug/L 10.0 0.90 1 05/19/20 06:20 107-13-1 Benzene ND ug/L 1.0 0.15 1 05/19/20 06:20 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 05/19/20 06:20 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 05/19/20 06:20 75-27-4 Bromoform ND ug/L 1.0 0.62 1 05/19/20 06:20 75-25-2 Bromomethane ND ug/L 2.0 0.62 1 05/19/20 06:20 74-83-9 IH,IK,L1 2-Butanone (MEK) ND ug/L 5.0 3.3 1 05/19/20 06:20 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 05/19/20 06:20 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 05/19/20 06:20 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 05/19/20 06:20 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 05/19/20 06:20 75-00-3 Chloroform ND ug/L 5.0 2.3 1 05/19/20 06:20 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 05/19/20 06:20 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 05/19/20 06:20 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 05/19/20 06:20 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 05/19/20 06:20 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 05/19/20 06:20 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.29 1 05/19/20 06:20 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 05/19/20 06:20 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 05/19/20 06:20 110-57-6 L1,v1 Dichlorodifluoromethane ND ug/L 1.0 0.23 1 05/19/20 06:20 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.27 1 05/19/20 06:20 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.34 1 05/19/20 06:20 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 05/19/20 06:20 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.29 1 05/19/20 06:20 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.25 1 05/19/20 06:20 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.19 1 05/19/20 06:20 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 0.30 1 05/19/20 06:20 10061-01-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 60 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-15 Lab ID: 92477008005 Collected: 05/08/20 11:50 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) i:Y�*111 e7 �, Riy&i I �, 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 20.0 ND ug/L 5.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 8.91 ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 99 % 70-130 96 % 70-130 100 % 70-130 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 111 % 50-150 87 % 50-150 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 96500 ug/L 5000 Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville 269000 ug/L 25000 Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville ND ug/L 100 0.31 1 05/19/20 06:20 10061-02-6 0.26 1 05/19/20 06:20 100-41-4 0.57 1 05/19/20 06:20 591-78-6 12.5 1 05/19/20 06:20 74-88-4 3.7 1 05/19/20 06:20 75-09-2 4.5 1 05/19/20 06:20 108-10-1 0.27 1 05/19/20 06:20 100-42-5 0.34 1 05/19/20 06:20 630-20-6 0.22 1 05/19/20 06:20 79-34-5 0.16 1 05/19/20 06:20 127-18-4 1.9 1 05/19/20 06:20 109-99-9 0.24 1 05/19/20 06:20 108-88-3 0.18 1 05/19/20 06:20 71-55-6 0.24 1 05/19/20 06:20 79-00-5 0.22 1 05/19/20 06:20 79-01-6 0.31 1 05/19/20 06:20 75-69-4 0.35 1 05/19/20 06:20 96-18-4 1.4 1 05/19/20 06:20 108-05-4 IK 0.24 1 05/19/20 06:20 75-01-4 0.41 1 05/19/20 06:20 179601-23-1 0.22 1 05/19/20 06:20 95-47-6 1 05/19/20 06:20 460-00-4 1 05/19/20 06:20 17060-07-0 1 05/19/20 06:20 2037-26-5 1.2 1 05/15/20 14:48 123-91-1 1 05/15/20 14:48 17060-07-0 1 05/15/20 14:48 2037-26-5 5000 1 05/16/20 00:48 25000 1 F�i][i>il REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 05/12/20 23:43 05/12/20 20:47 18496-25-8 Page 61 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-15 Parameters Lab ID: 92477008005 Collected: 05/08/20 11:50 Report Results Units Limit MDL DF Received: 05/08/20 17:07 Matrix: Water Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 38300 ug/L 1000 500 1 05/14/2010:51 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 55500 ug/L 2000 1000 2 05/12/2019:51 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 05/18/2013:48 05/19/2012:20 57-12-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 62 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: EQBL Lab ID: 92477008006 Collected: 05/08/20 12:40 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual Chlorinated Herb. (GC) 8151 Analytical Method: EPA8151 Preparation Method: 8151A Pace National - Mt. Juliet 2,4-D ND ug/L 2.00 0.547 1 05/15/20 18:43 05/17/20 15:47 94-75-7 2,4,5-TP (Silvex) ND ug/L 2.00 0.335 1 05/15/20 18:43 05/17/20 15:47 93-72-1 Surrogates 2,4-DCAA (S) 53.8 % 14.0-158 1 05/15/20 18:43 05/17/20 15:47 19719-28-9 8081 OC Pesticides RVE Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Aldrin ND ug/L 0.050 0.022 1 05/12/20 21:32 05/14/20 18:50 309-00-2 alpha-BHC ND ug/L 0.050 0.019 1 05/12/20 21:32 05/14/20 18:50 319-84-6 delta-BHC ND ug/L 0.050 0.020 1 05/12/20 21:32 05/14/20 18:50 319-86-8 4,4'-DDD ND ug/L 0.050 0.0069 1 05/12/20 21:32 05/14/20 18:50 72-54-8 4,4'-DDT ND ug/L 0.050 0.018 1 05/12/20 21:32 05/14/20 18:50 50-29-3 Endosulfan I ND ug/L 0.050 0.0094 1 05/12/20 21:32 05/14/20 18:50 959-98-8 Endosulfan 11 ND ug/L 0.050 0.0065 1 05/12/20 21:32 05/14/20 18:50 33213-65-9 Endrin ND ug/L 0.050 0.0089 1 05/12/20 21:32 05/14/20 18:50 72-20-8 Endrin aldehyde ND ug/L 0.050 0.013 1 05/12/20 21:32 05/14/20 18:50 7421-93-4 Heptachlor ND ug/L 0.050 0.016 1 05/12/20 21:32 05/14/20 18:50 76-44-8 Heptachlor epoxide ND ug/L 0.050 0.0097 1 05/12/20 21:32 05/14/20 18:50 1024-57-3 Methoxychlor ND ug/L 0.15 0.033 1 05/12/20 21:32 05/14/20 18:50 72-43-5 Surrogates Tetrachloro-m-xylene (S) 92 % 10-130 1 05/12/20 21:32 05/14/20 18:50 877-09-8 Decachlorobiphenyl (S) 109 % 10-130 1 05/12/20 21:32 05/14/20 18:50 2051-24-3 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 05/14/20 01:51 05/19/20 19:17 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 19:17 7440-38-2 Barium ND ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 19:17 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 05/14/20 01:51 05/19/20 19:17 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 05/14/20 01:51 05/19/20 19:17 7440-43-9 Chromium ND ug/L 5.0 3.7 1 05/14/20 01:51 05/19/20 19:17 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 05/14/20 01:51 05/19/20 19:17 7440-48-4 Copper ND ug/L 5.0 4.3 1 05/14/20 01:51 05/19/20 19:17 7440-50-8 Iron ND ug/L 50.0 41.5 1 05/14/20 01:51 05/19/20 19:17 7439-89-6 Lead ND ug/L 5.0 4.5 1 05/14/20 01:51 05/19/20 19:17 7439-92-1 Manganese ND ug/L 5.0 3.4 1 05/14/20 01:51 05/19/20 19:17 7439-96-5 Nickel ND ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 19:17 7440-02-0 Selenium ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 19:17 7782-49-2 Silver ND ug/L 5.0 2.5 1 05/14/20 01:51 05/19/20 19:17 7440-22-4 Sodium ND ug/L 5000 611 1 05/14/20 01:51 05/19/20 19:17 7440-23-5 Tin ND ug/L 5.0 4.7 1 05/14/20 01:51 05/19/20 19:17 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 05/14/20 01:51 05/19/20 19:17 7440-62-2 Zinc ND ug/L 10.0 9.5 1 05/14/20 01:51 05/19/20 19:17 7440-66-6 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 63 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: EQBL Lab ID: 92477008006 Collected: 05/08/20 12:40 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville Mercury 0.66 ug/L 0.20 0.12 1 05/20/2017:30 05/21/2011:24 7439-97-6 8270E RVE Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte Benzo(a)anthracene ND ug/L 10.0 1.5 1 05/12/20 18:13 05/19/20 22:38 56-55-3 Chrysene ND ug/L 10.0 1.4 1 05/12/20 18:13 05/19/20 22:38 218-01-9 Dibenz(a,h)anthracene ND ug/L 10.0 1.6 1 05/12/20 18:13 05/19/20 22:38 53-70-3 bis(2- Ethyl hexyl)phthalate ND ug/L 6.0 2.0 1 05/12/20 18:13 05/19/20 22:38 117-81-7 Indeno(1,2,3-cd)pyrene ND ug/L 10.0 1.7 1 05/12/20 18:13 05/19/20 22:38 193-39-5 Surrogates Nitrobenzene-d5 (S) 112 % 13-130 1 05/12/20 18:13 05/19/20 22:38 4165-60-0 2-Fluorobiphenyl (S) 95 % 13-130 1 05/12/20 18:13 05/19/20 22:38 321-60-8 Terphenyl-d14 (S) 127 % 25-130 1 05/12/20 18:13 05/19/20 22:38 1718-51-0 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 6.2 1 05/19/20 03:31 67-64-1 Acrylonitrile ND ug/L 10.0 0.90 1 05/19/20 03:31 107-13-1 Benzene ND ug/L 1.0 0.15 1 05/19/20 03:31 71-43-2 Bromochloromethane ND ug/L 1.0 0.34 1 05/19/20 03:31 74-97-5 Bromodichloromethane ND ug/L 1.0 0.26 1 05/19/20 03:31 75-27-4 Bromoform ND ug/L 1.0 0.62 1 05/19/20 03:31 75-25-2 Bromomethane ND ug/L 2.0 0.62 1 05/19/20 03:31 74-83-9 IH,IK,L1 2-Butanone (MEK) ND ug/L 5.0 3.3 1 05/19/20 03:31 78-93-3 Carbon disulfide ND ug/L 2.0 0.40 1 05/19/20 03:31 75-15-0 Carbon tetrachloride ND ug/L 1.0 0.22 1 05/19/20 03:31 56-23-5 Chlorobenzene ND ug/L 1.0 0.23 1 05/19/20 03:31 108-90-7 Chloroethane ND ug/L 1.0 0.49 1 05/19/20 03:31 75-00-3 Chloroform ND ug/L 5.0 2.3 1 05/19/20 03:31 67-66-3 Chloromethane ND ug/L 1.0 0.39 1 05/19/20 03:31 74-87-3 1,2-Dibromo-3-chloropropane ND ug/L 5.0 0.26 1 05/19/20 03:31 96-12-8 Dibromochloromethane ND ug/L 1.0 0.41 1 05/19/20 03:31 124-48-1 1,2-Dibromoethane (EDB) ND ug/L 1.0 0.26 1 05/19/20 03:31 106-93-4 Dibromomethane ND ug/L 1.0 0.46 1 05/19/20 03:31 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 0.29 1 05/19/20 03:31 95-50-1 1,4-Dichlorobenzene ND ug/L 1.0 0.26 1 05/19/20 03:31 106-46-7 trans-1,4-Dichloro-2-butene ND ug/L 1.0 0.54 1 05/19/20 03:31 110-57-6 L1,v1 Dichlorodifluoromethane ND ug/L 1.0 0.23 1 05/19/20 03:31 75-71-8 1,1-Dichloroethane ND ug/L 1.0 0.27 1 05/19/20 03:31 75-34-3 1,2-Dichloroethane ND ug/L 1.0 0.34 1 05/19/20 03:31 107-06-2 1,1-Dichloroethene ND ug/L 1.0 0.24 1 05/19/20 03:31 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 0.29 1 05/19/20 03:31 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 0.25 1 05/19/20 03:31 156-60-5 1,2-Dichloropropane ND ug/L 1.0 0.19 1 05/19/20 03:31 78-87-5 cis-1,3-Dichloropropene ND ug/L 1.0 0.30 1 05/19/20 03:31 10061-01-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 64 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: EQBL Lab ID: 92477008006 Collected: 05/08/20 12:40 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) i:Y�*111 e7 �, Riy&i I �, 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 ND ug/L 1.0 ND ug/L 5.0 ND ug/L 20.0 ND ug/L 5.0 ND ug/L 5.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 1.0 100 % 70-130 96 % 70-130 99 % 70-130 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte ND ug/L 2.0 95 % 50-150 94 % 50-150 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville ND ug/L 5000 Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville ND ug/L 25000 Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville ND ug/L 100 0.31 1 05/19/20 03:31 10061-02-6 0.26 1 05/19/20 03:31 100-41-4 0.57 1 05/19/20 03:31 591-78-6 12.5 1 05/19/20 03:31 74-88-4 3.7 1 05/19/20 03:31 75-09-2 4.5 1 05/19/20 03:31 108-10-1 0.27 1 05/19/20 03:31 100-42-5 0.34 1 05/19/20 03:31 630-20-6 0.22 1 05/19/20 03:31 79-34-5 0.16 1 05/19/20 03:31 127-18-4 1.9 1 05/19/20 03:31 109-99-9 0.24 1 05/19/20 03:31 108-88-3 0.18 1 05/19/20 03:31 71-55-6 0.24 1 05/19/20 03:31 79-00-5 0.22 1 05/19/20 03:31 79-01-6 0.31 1 05/19/20 03:31 75-69-4 0.35 1 05/19/20 03:31 96-18-4 1.4 1 05/19/20 03:31 108-05-4 IK 0.24 1 05/19/20 03:31 75-01-4 0.41 1 05/19/20 03:31 179601-23-1 0.22 1 05/19/20 03:31 95-47-6 1 05/19/20 03:31 460-00-4 1 05/19/20 03:31 17060-07-0 1 05/19/20 03:31 2037-26-5 1.2 1 05/15/20 12:11 123-91-1 1 05/15/20 12:11 17060-07-0 1 05/15/20 12:11 2037-26-5 5000 1 05/16/20 02:28 25000 1 F�i][i>il REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 05/12/20 23:43 05/12/20 20:48 18496-25-8 Page 65 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: EQBL Parameters Lab ID: 92477008006 Collected: 05/08/20 12:40 Report Results Units Limit MDL DF Received: 05/08/20 17:07 Matrix: Water Prepared Analyzed CAS No. Qual 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate ND ug/L 1000 500 1 05/14/2011:06 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride ND ug/L 1000 500 1 05/12/2019:43 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 05/18/2013:48 05/19/2012:21 57-12-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 66 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-10 Lab ID: 92477013001 Collected: 05/05/20 12:35 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Aldrin alpha-BHC delta-BHC 4,4'-DDD 4,4'-DDT Endosulfan I Endosulfan 11 Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Silver Sodium Tin Vanadium Zinc 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Date: 06/09/2020 08:57 AM Analytical Method: EPA 8081 B Preparation Method: EPA 351 OC Pace Analytical Services - Charlotte ND ug/L 0.050 0.022 1 05/12/2013:40 05/13/2019:20 309-00-2 ND ug/L 0.050 0.019 1 05/12/2013:40 05/13/2019:20 319-84-6 ND ug/L 0.050 0.020 1 05/12/2013:40 05/13/2019:20 319-86-8 ND ug/L 0.050 0.0069 1 05/12/2013:40 05/13/2019:20 72-54-8 ND ug/L 0.050 0.018 1 05/12/2013:40 05/13/2019:20 50-29-3 ND ug/L 0.050 0.0094 1 05/12/2013:40 05/13/2019:20 959-98-8 ND ug/L 0.050 0.0065 1 05/12/2013:40 05/13/2019:20 33213-65-9 ND ug/L 0.050 0.0089 1 05/12/2013:40 05/13/2019:20 72-20-8 L1 ND ug/L 0.050 0.013 1 05/12/2013:40 05/13/2019:20 7421-93-4 ND ug/L 0.050 0.016 1 05/12/2013:40 05/13/2019:20 76-44-8 ND ug/L 0.050 0.0097 1 05/12/2013:40 05/13/2019:20 1024-57-3 ND ug/L 0.15 0.033 1 05/12/2013:40 05/13/2019:20 72-43-5 21 % 10-130 1 05/12/2013:40 05/13/2019:20 877-09-8 92 % 10-130 1 05/12/2013:40 05/13/2019:20 2051-24-3 Analytical Method: EPA 601 OD Preparation Method: EPA 301 OA Pace Analytical Services -Asheville ND ug/L 5.0 3.0 1 05/14/20 01:51 05/19/20 20:15 7440-36-0 ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 20:15 7440-38-2 66.0 ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 20:15 7440-39-3 ND ug/L 1.0 0.70 1 05/14/20 01:51 05/19/20 20:15 7440-41-7 0.62J ug/L 1.0 0.40 1 05/14/20 01:51 05/19/20 20:15 7440-43-9 4.OJ ug/L 5.0 3.7 1 05/14/20 01:51 05/19/20 20:15 7440-47-3 12.1 ug/L 5.0 3.6 1 05/14/20 01:51 05/19/20 20:15 7440-48-4 ND ug/L 5.0 4.3 1 05/14/20 01:51 05/19/20 20:15 7440-50-8 2740 ug/L 50.0 41.5 1 05/14/20 01:51 05/19/20 20:15 7439-89-6 ND ug/L 5.0 4.5 1 05/14/20 01:51 05/19/20 20:15 7439-92-1 25700 ug/L 25.0 17.2 5 05/14/20 01:51 05/20/20 16:03 7439-96-5 7.9 ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 20:15 7440-02-0 ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 20:15 7782-49-2 ND ug/L 5.0 2.5 1 05/14/20 01:51 05/19/20 20:15 7440-22-4 148000 ug/L 25000 3050 5 05/14/20 01:51 05/20/20 16:03 7440-23-5 7.1 ug/L 5.0 4.7 1 05/14/20 01:51 05/19/20 20:15 7440-31-5 ND ug/L 5.0 3.9 1 05/14/20 01:51 05/19/20 20:15 7440-62-2 ND ug/L 10.0 9.5 1 05/14/20 01:51 05/19/20 20:15 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 05/20/2017:30 05/21/2011:55 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 6.2 1 05/19/20 01:56 67-64-1 ND ug/L 10.0 0.90 1 05/19/20 01:56 107-13-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 67 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-10 Lab ID: 92477013001 Collected: 05/05/20 12:35 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 0.56J ug/L 1.0 0.15 1 05/19/20 01:56 71-43-2 ND ug/L 1.0 0.34 1 05/19/20 01:56 74-97-5 ND ug/L 1.0 0.26 1 05/19/20 01:56 75-27-4 ND ug/L 1.0 0.62 1 05/19/20 01:56 75-25-2 ND ug/L 2.0 0.62 1 05/19/20 01:56 74-83-9 IK,v2 ND ug/L 5.0 3.3 1 05/19/20 01:56 78-93-3 ND ug/L 2.0 0.40 1 05/19/20 01:56 75-15-0 ND ug/L 1.0 0.22 1 05/19/20 01:56 56-23-5 ND ug/L 1.0 0.23 1 05/19/20 01:56 108-90-7 ND ug/L 1.0 0.49 1 05/19/20 01:56 75-00-3 IK ND ug/L 5.0 2.3 1 05/19/20 01:56 67-66-3 ND ug/L 1.0 0.39 1 05/19/20 01:56 74-87-3 IK ND ug/L 5.0 0.26 1 05/19/20 01:56 96-12-8 ND ug/L 1.0 0.41 1 05/19/20 01:56 124-48-1 ND ug/L 1.0 0.26 1 05/19/20 01:56 106-93-4 ND ug/L 1.0 0.46 1 05/19/20 01:56 74-95-3 ND ug/L 1.0 0.29 1 05/19/20 01:56 95-50-1 ND ug/L 1.0 0.26 1 05/19/20 01:56 106-46-7 ND ug/L 1.0 0.54 1 05/19/20 01:56 110-57-6 IH ND ug/L 1.0 0.23 1 05/19/20 01:56 75-71-8 IK ND ug/L 1.0 0.27 1 05/19/20 01:56 75-34-3 ND ug/L 1.0 0.34 1 05/19/20 01:56 107-06-2 ND ug/L 1.0 0.24 1 05/19/20 01:56 75-35-4 ND ug/L 1.0 0.29 1 05/19/20 01:56 156-59-2 ND ug/L 1.0 0.25 1 05/19/20 01:56 156-60-5 ND ug/L 1.0 0.19 1 05/19/20 01:56 78-87-5 ND ug/L 1.0 0.30 1 05/19/20 01:56 10061-01-5 ND ug/L 1.0 0.31 1 05/19/20 01:56 10061-02-6 ND ug/L 1.0 0.26 1 05/19/20 01:56 100-41-4 ND ug/L 5.0 0.57 1 05/19/20 01:56 591-78-6 ND ug/L 20.0 12.5 1 05/19/20 01:56 74-88-4 v2 ND ug/L 5.0 3.7 1 05/19/20 01:56 75-09-2 ND ug/L 5.0 4.5 1 05/19/20 01:56 108-10-1 v1 ND ug/L 1.0 0.27 1 05/19/20 01:56 100-42-5 ND ug/L 1.0 0.34 1 05/19/20 01:56 630-20-6 ND ug/L 1.0 0.22 1 05/19/20 01:56 79-34-5 ND ug/L 1.0 0.16 1 05/19/20 01:56 127-18-4 130 ug/L 10.0 1.9 1 05/19/20 01:56 109-99-9 ND ug/L 1.0 0.24 1 05/19/20 01:56 108-88-3 ND ug/L 1.0 0.18 1 05/19/20 01:56 71-55-6 ND ug/L 1.0 0.24 1 05/19/20 01:56 79-00-5 ND ug/L 1.0 0.22 1 05/19/20 01:56 79-01-6 ND ug/L 1.0 0.31 1 05/19/20 01:56 75-69-4 IK ND ug/L 1.0 0.35 1 05/19/20 01:56 96-18-4 ND ug/L 2.0 1.4 1 05/19/20 01:56 108-05-4 v1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 68 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-10 Lab ID: 92477013001 Collected: 05/05/20 12:35 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Vinyl chloride ND ug/L 1.0 0.24 1 05/19/20 01:56 75-01-4 IK m&p-Xylene ND ug/L 2.0 0.41 1 05/19/20 01:56 179601-23-1 o-Xylene 0.34.11 ug/L 1.0 0.22 1 05/19/20 01:56 95-47-6 Surrogates 4-Bromofluorobenzene (S) 95 % 70-130 1 05/19/20 01:56 460-00-4 1,2-Dichloroethane-d4 (S) 102 % 70-130 1 05/19/20 01:56 17060-07-0 Toluene-d8 (S) 103 % 70-130 1 05/19/20 01:56 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) 6.6 ug/L 2.0 1.2 1 05/15/20 00:58 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 107 % 50-150 1 05/15/20 00:58 17060-07-0 Toluene-d8 (S) 86 % 50-150 1 05/15/20 00:58 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 635000 ug/L 5000 5000 1 05/18/20 15:25 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville Total Dissolved Solids 1180000 ug/L 50000 50000 1 05/12/20 16:32 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide 242 ug/L 100 50.0 1 05/12/20 20:05 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 275000 ug/L 6000 3000 6 05/14/2013:59 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 63100 ug/L 3000 1500 3 05/13/20 20:40 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 05/13/20 09:43 05/14/20 14:49 57-12-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 69 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-7 Lab ID: 92477013002 Collected: 05/07/20 10:35 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8081 OC Pesticides RVE Aldrin alpha-BHC delta-BHC 4,4'-DDD 4,4'-DDT Endosulfan I Endosulfan 11 Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Surrogates Tetrachloro-m-xylene (S) Decachlorobiphenyl (S) 6010 MET ICP Antimony Arsenic Barium Beryllium Cadmium Chromium Cobalt Copper Iron Lead Manganese Nickel Selenium Silver Sodium Tin Vanadium Zinc 7470 Mercury Mercury 8260D MSV Low Level Landfill Acetone Acrylonitrile Date: 06/09/2020 08:57 AM Analytical Method: EPA 8081 B Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 0.050 0.022 1 05/12/20 21:32 05/14/20 16:54 309-00-2 ND ug/L 0.050 0.019 1 05/12/20 21:32 05/14/20 16:54 319-84-6 ND ug/L 0.050 0.020 1 05/12/20 21:32 05/14/20 16:54 319-86-8 ND ug/L 0.050 0.0069 1 05/12/20 21:32 05/14/20 16:54 72-54-8 ND ug/L 0.050 0.018 1 05/12/20 21:32 05/14/20 16:54 50-29-3 ND ug/L 0.050 0.0094 1 05/12/20 21:32 05/14/20 16:54 959-98-8 ND ug/L 0.050 0.0065 1 05/12/20 21:32 05/14/20 16:54 33213-65-9 ND ug/L 0.050 0.0089 1 05/12/20 21:32 05/14/20 16:54 72-20-8 ND ug/L 0.050 0.013 1 05/12/20 21:32 05/14/20 16:54 7421-93-4 ND ug/L 0.050 0.016 1 05/12/20 21:32 05/14/20 16:54 76-44-8 ND ug/L 0.050 0.0097 1 05/12/20 21:32 05/14/20 16:54 1024-57-3 ND ug/L 0.15 0.033 1 05/12/20 21:32 05/14/20 16:54 72-43-5 39 % 10-130 1 05/12/20 21:32 05/14/20 16:54 877-09-8 125 % 10-130 1 05/12/20 21:32 05/14/20 16:54 2051-24-3 Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Pace Analytical Services -Asheville ND ug/L 5.0 3.0 1 05/14/20 01:51 05/19/20 20:18 7440-36-0 ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 20:18 7440-38-2 136 ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 20:18 7440-39-3 ND ug/L 1.0 0.70 1 05/14/20 01:51 05/19/20 20:18 7440-41-7 ND ug/L 1.0 0.40 1 05/14/20 01:51 05/19/20 20:18 7440-43-9 ND ug/L 5.0 3.7 1 05/14/20 01:51 05/19/20 20:18 7440-47-3 ND ug/L 5.0 3.6 1 05/14/20 01:51 05/19/20 20:18 7440-48-4 ND ug/L 5.0 4.3 1 05/14/20 01:51 05/19/20 20:18 7440-50-8 ND ug/L 50.0 41.5 1 05/14/20 01:51 05/19/20 20:18 7439-89-6 ND ug/L 5.0 4.5 1 05/14/20 01:51 05/19/20 20:18 7439-92-1 69.9 ug/L 5.0 3.4 1 05/14/20 01:51 05/19/20 20:18 7439-96-5 ND ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 20:18 7440-02-0 ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 20:18 7782-49-2 ND ug/L 5.0 2.5 1 05/14/20 01:51 05/19/20 20:18 7440-22-4 16200 ug/L 5000 611 1 05/14/20 01:51 05/19/20 20:18 7440-23-5 ND ug/L 5.0 4.7 1 05/14/20 01:51 05/19/20 20:18 7440-31-5 ND ug/L 5.0 3.9 1 05/14/20 01:51 05/19/20 20:18 7440-62-2 ND ug/L 10.0 9.5 1 05/14/20 01:51 05/19/20 20:18 7440-66-6 Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 05/20/2017:30 05/21/2011:57 7439-97-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 6.2 1 05/19/20 06:57 67-64-1 ND ug/L 10.0 0.90 1 05/19/20 06:57 107-13-1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 70 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-7 Lab ID: 92477013002 Collected: 05/07/20 10:35 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 0.48J ug/L 1.0 0.15 1 05/19/20 06:57 71-43-2 ND ug/L 1.0 0.34 1 05/19/20 06:57 74-97-5 ND ug/L 1.0 0.26 1 05/19/20 06:57 75-27-4 ND ug/L 1.0 0.62 1 05/19/20 06:57 75-25-2 ND ug/L 2.0 0.62 1 05/19/20 06:57 74-83-9 IH,IK,L1 ND ug/L 5.0 3.3 1 05/19/20 06:57 78-93-3 ND ug/L 2.0 0.40 1 05/19/20 06:57 75-15-0 ND ug/L 1.0 0.22 1 05/19/20 06:57 56-23-5 ND ug/L 1.0 0.23 1 05/19/20 06:57 108-90-7 0.85J ug/L 1.0 0.49 1 05/19/20 06:57 75-00-3 ND ug/L 5.0 2.3 1 05/19/20 06:57 67-66-3 ND ug/L 1.0 0.39 1 05/19/20 06:57 74-87-3 ND ug/L 5.0 0.26 1 05/19/20 06:57 96-12-8 ND ug/L 1.0 0.41 1 05/19/20 06:57 124-48-1 ND ug/L 1.0 0.26 1 05/19/20 06:57 106-93-4 ND ug/L 1.0 0.46 1 05/19/20 06:57 74-95-3 ND ug/L 1.0 0.29 1 05/19/20 06:57 95-50-1 ND ug/L 1.0 0.26 1 05/19/20 06:57 106-46-7 ND ug/L 1.0 0.54 1 05/19/20 06:57 110-57-6 L1,v1 0.52J ug/L 1.0 0.23 1 05/19/20 06:57 75-71-8 0.901 ug/L 1.0 0.27 1 05/19/20 06:57 75-34-3 ND ug/L 1.0 0.34 1 05/19/20 06:57 107-06-2 ND ug/L 1.0 0.24 1 05/19/20 06:57 75-35-4 0.911 ug/L 1.0 0.29 1 05/19/20 06:57 156-59-2 ND ug/L 1.0 0.25 1 05/19/20 06:57 156-60-5 ND ug/L 1.0 0.19 1 05/19/20 06:57 78-87-5 ND ug/L 1.0 0.30 1 05/19/20 06:57 10061-01-5 ND ug/L 1.0 0.31 1 05/19/20 06:57 10061-02-6 ND ug/L 1.0 0.26 1 05/19/20 06:57 100-41-4 ND ug/L 5.0 0.57 1 05/19/20 06:57 591-78-6 ND ug/L 20.0 12.5 1 05/19/20 06:57 74-88-4 4.7J ug/L 5.0 3.7 1 05/19/20 06:57 75-09-2 ND ug/L 5.0 4.5 1 05/19/20 06:57 108-10-1 ND ug/L 1.0 0.27 1 05/19/20 06:57 100-42-5 ND ug/L 1.0 0.34 1 05/19/20 06:57 630-20-6 ND ug/L 1.0 0.22 1 05/19/20 06:57 79-34-5 ND ug/L 1.0 0.16 1 05/19/20 06:57 127-18-4 70.5 ug/L 10.0 1.9 1 05/19/20 06:57 109-99-9 ND ug/L 1.0 0.24 1 05/19/20 06:57 108-88-3 ND ug/L 1.0 0.18 1 05/19/20 06:57 71-55-6 ND ug/L 1.0 0.24 1 05/19/20 06:57 79-00-5 ND ug/L 1.0 0.22 1 05/19/20 06:57 79-01-6 5.6 ug/L 1.0 0.31 1 05/19/20 06:57 75-69-4 ND ug/L 1.0 0.35 1 05/19/20 06:57 96-18-4 ND ug/L 2.0 1.4 1 05/19/20 06:57 108-05-4 IK REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 71 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-7 Lab ID: 92477013002 Collected: 05/07/20 10:35 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Vinyl chloride ND ug/L 1.0 0.24 1 05/19/20 06:57 75-01-4 m&p-Xylene 0.72J ug/L 2.0 0.41 1 05/19/20 06:57 179601-23-1 o-Xylene 0.46J ug/L 1.0 0.22 1 05/19/20 06:57 95-47-6 Surrogates 4-Bromofluorobenzene (S) 99 % 70-130 1 05/19/20 06:57 460-00-4 1,2-Dichloroethane-d4 (S) 94 % 70-130 1 05/19/20 06:57 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 05/19/20 06:57 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) 2.2 ug/L 2.0 1.2 1 05/15/20 16:08 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 108 % 50-150 1 05/15/20 16:08 17060-07-0 Toluene-d8 (S) 100 % 50-150 1 05/15/20 16:08 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 71600 ug/L 5000 5000 1 05/16/20 03:03 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville Total Dissolved Solids 165000 ug/L 25000 25000 1 05/12/20 23:20 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 05/12/20 20:44 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 10400 ug/L 1000 500 1 05/14/20 09:59 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 5910 ug/L 1000 500 1 05/13/20 20:23 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 05/20/2010:03 05/20/2017:23 57-12-5 M1,R1 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 72 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: SW-2 Lab ID: 92477016001 Collected: 05/05/20 14:35 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 05/14/20 01:51 05/19/20 20:21 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 20:21 7440-38-2 Barium 100 ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 20:21 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 05/14/20 01:51 05/19/20 20:21 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 05/14/20 01:51 05/19/20 20:21 7440-43-9 Chromium ND ug/L 5.0 3.7 1 05/14/20 01:51 05/19/20 20:21 7440-47-3 Cobalt ND ug/L 5.0 3.6 1 05/14/20 01:51 05/19/20 20:21 7440-48-4 Copper ND ug/L 5.0 4.3 1 05/14/20 01:51 05/19/20 20:21 7440-50-8 Iron 4030 ug/L 50.0 41.5 1 05/14/20 01:51 05/19/20 20:21 7439-89-6 Lead ND ug/L 5.0 4.5 1 05/14/20 01:51 05/19/20 20:21 7439-92-1 Manganese 1040 ug/L 5.0 3.4 1 05/14/20 01:51 05/19/20 20:21 7439-96-5 Nickel ND ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 20:21 7440-02-0 Selenium ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 20:21 7782-49-2 Silver ND ug/L 5.0 2.5 1 05/14/20 01:51 05/19/20 20:21 7440-22-4 Sodium 14200 ug/L 5000 611 1 05/14/20 01:51 05/19/20 20:21 7440-23-5 Tin ND ug/L 5.0 4.7 1 05/14/20 01:51 05/19/20 20:21 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 05/14/20 01:51 05/19/20 20:21 7440-62-2 Zinc ND ug/L 10.0 9.5 1 05/14/20 01:51 05/19/20 20:21 7440-66-6 7470 Mercury Mercury 8270E RVE Benzo(a)anthracene Chrysene Dibenz(a,h)anthracene bis(2- Ethyl hexyl)phthalate Indeno(1,2,3-cd)pyrene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol (S) 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Date: 06/09/2020 08:57 AM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville ND ug/L 0.20 0.12 1 05/20/2017:30 05/21/2012:00 7439-97-6 Analytical Method: EPA 8270E Preparation Method: EPA 351 OC Pace Analytical Services - Charlotte ND ug/L 10.0 1.5 1 05/12/20 10:44 05/12/20 20:42 56-55-3 ND ug/L 10.0 1.4 1 05/12/20 10:44 05/12/20 20:42 218-01-9 2.OJ ug/L 10.0 1.6 1 05/12/20 10:44 05/12/20 20:42 53-70-3 ND ug/L 6.0 2.0 1 05/12/20 10:44 05/12/20 20:42 117-81-7 2.2J ug/L 10.0 1.7 1 05/12/20 10:44 05/12/20 20:42 193-39-5 67 % 13-130 1 05/12/20 10:44 05/12/20 20:42 4165-60-0 45 % 13-130 1 05/12/20 10:44 05/12/20 20:42 321-60-8 123 % 25-130 1 05/12/20 10:44 05/12/20 20:42 1718-51-0 43 % 10-130 1 05/12/20 10:44 05/12/20 20:42 13127-88-3 57 % 10-130 1 05/12/20 10:44 05/12/20 20:42 367-12-4 85 % 10-137 1 05/12/20 10:44 05/12/20 20:42 118-79-6 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 6.2 1 05/19/20 02:14 67-64-1 ND ug/L 10.0 0.90 1 05/19/20 02:14 107-13-1 ND ug/L 1.0 0.15 1 05/19/20 02:14 71-43-2 ND ug/L 1.0 0.34 1 05/19/20 02:14 74-97-5 ND ug/L 1.0 0.26 1 05/19/20 02:14 75-27-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. v2,v3 v1 Page 73 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: SW-2 Lab ID: 92477016001 Collected: 05/05/20 14:35 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Bromoform Bromomethane 2-Butanone (MEK) Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 1.0 0.62 1 05/19/20 02:14 75-25-2 ND ug/L 2.0 0.62 1 05/19/20 02:14 74-83-9 IK,v2 ND ug/L 5.0 3.3 1 05/19/20 02:14 78-93-3 ND ug/L 2.0 0.40 1 05/19/20 02:14 75-15-0 ND ug/L 1.0 0.22 1 05/19/20 02:14 56-23-5 ND ug/L 1.0 0.23 1 05/19/20 02:14 108-90-7 ND ug/L 1.0 0.49 1 05/19/20 02:14 75-00-3 IK ND ug/L 5.0 2.3 1 05/19/20 02:14 67-66-3 ND ug/L 1.0 0.39 1 05/19/20 02:14 74-87-3 IK ND ug/L 5.0 0.26 1 05/19/20 02:14 96-12-8 ND ug/L 1.0 0.41 1 05/19/20 02:14 124-48-1 ND ug/L 1.0 0.26 1 05/19/20 02:14 106-93-4 ND ug/L 1.0 0.46 1 05/19/20 02:14 74-95-3 ND ug/L 1.0 0.29 1 05/19/20 02:14 95-50-1 ND ug/L 1.0 0.26 1 05/19/20 02:14 106-46-7 ND ug/L 1.0 0.54 1 05/19/20 02:14 110-57-6 IH ND ug/L 1.0 0.23 1 05/19/20 02:14 75-71-8 IK ND ug/L 1.0 0.27 1 05/19/20 02:14 75-34-3 ND ug/L 1.0 0.34 1 05/19/20 02:14 107-06-2 ND ug/L 1.0 0.24 1 05/19/20 02:14 75-35-4 ND ug/L 1.0 0.29 1 05/19/20 02:14 156-59-2 ND ug/L 1.0 0.25 1 05/19/20 02:14 156-60-5 ND ug/L 1.0 0.19 1 05/19/20 02:14 78-87-5 ND ug/L 1.0 0.30 1 05/19/20 02:14 10061-01-5 ND ug/L 1.0 0.31 1 05/19/20 02:14 10061-02-6 ND ug/L 1.0 0.26 1 05/19/20 02:14 100-41-4 ND ug/L 5.0 0.57 1 05/19/20 02:14 591-78-6 ND ug/L 20.0 12.5 1 05/19/20 02:14 74-88-4 v2 ND ug/L 5.0 3.7 1 05/19/20 02:14 75-09-2 ND ug/L 5.0 4.5 1 05/19/20 02:14 108-10-1 v1 ND ug/L 1.0 0.27 1 05/19/20 02:14 100-42-5 ND ug/L 1.0 0.34 1 05/19/20 02:14 630-20-6 ND ug/L 1.0 0.22 1 05/19/20 02:14 79-34-5 ND ug/L 1.0 0.16 1 05/19/20 02:14 127-18-4 ND ug/L 10.0 1.9 1 05/19/20 02:14 109-99-9 ND ug/L 1.0 0.24 1 05/19/20 02:14 108-88-3 ND ug/L 1.0 0.18 1 05/19/20 02:14 71-55-6 ND ug/L 1.0 0.24 1 05/19/20 02:14 79-00-5 ND ug/L 1.0 0.22 1 05/19/20 02:14 79-01-6 ND ug/L 1.0 0.31 1 05/19/20 02:14 75-69-4 IK ND ug/L 1.0 0.35 1 05/19/20 02:14 96-18-4 ND ug/L 2.0 1.4 1 05/19/20 02:14 108-05-4 v1 ND ug/L 1.0 0.24 1 05/19/20 02:14 75-01-4 IK ND ug/L 2.0 0.41 1 05/19/20 02:14 179601-23-1 ND ug/L 1.0 0.22 1 05/19/20 02:14 95-47-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 74 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: SW-2 Lab ID: 92477016001 Collected: 05/05/20 14:35 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 8260D MSV SIM 1,4-Dioxane (p-Dioxane) Surrogates 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) 2320B Alkalinity Alkalinity, Total as CaCO3 2540C Total Dissolved Solids Total Dissolved Solids 4500S2D Sulfide Water Sulfide 300.0 IC Anions 28 Days Sulfate 4500 Chloride Chloride 450OCNE Cyanide, Total Cyanide Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 95 % 70-130 1 05/19/20 02:14 460-00-4 105 % 70-130 1 05/19/20 02:14 17060-07-0 101 % 70-130 1 05/19/20 02:14 2037-26-5 Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 2.2 ug/L 2.0 1.2 1 05/15/20 01:18 123-91-1 99 % 50-150 1 05/15/20 01:18 17060-07-0 104 % 50-150 1 05/15/20 01:18 2037-26-5 Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville 78800 ug/L 5000 5000 1 05/15/20 21:36 Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville 171000 ug/L 25000 25000 1 05/12/2016:32 Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville ND ug/L 100 50.0 1 05/12/20 20:06 18496-25-8 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville 19300 ug/L 1000 500 1 05/14/2010:44 14808-79-8 Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville 19300 ug/L 1000 500 1 05/13/20 20:26 16887-00-6 Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville ND ug/L 8.0 6.0 1 05/13/20 09:43 05/14/20 14:50 57-12-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 75 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-3R Lab ID: 92477016002 Collected: 05/07/20 08:55 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A Pace Analytical Services -Asheville Antimony ND ug/L 5.0 3.0 1 05/14/20 01:51 05/19/20 20:24 7440-36-0 Arsenic ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 20:24 7440-38-2 Barium 257 ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 20:24 7440-39-3 Beryllium ND ug/L 1.0 0.70 1 05/14/20 01:51 05/19/20 20:24 7440-41-7 Cadmium ND ug/L 1.0 0.40 1 05/14/20 01:51 05/19/20 20:24 7440-43-9 Chromium ND ug/L 5.0 3.7 1 05/14/20 01:51 05/19/20 20:24 7440-47-3 Cobalt 13.6 ug/L 5.0 3.6 1 05/14/20 01:51 05/19/20 20:24 7440-48-4 Copper ND ug/L 5.0 4.3 1 05/14/20 01:51 05/19/20 20:24 7440-50-8 Iron 74900 ug/L 50.0 41.5 1 05/14/20 01:51 05/19/20 20:24 7439-89-6 Lead ND ug/L 5.0 4.5 1 05/14/20 01:51 05/19/20 20:24 7439-92-1 Manganese 5640 ug/L 5.0 3.4 1 05/14/20 01:51 05/19/20 20:24 7439-96-5 Nickel ND ug/L 5.0 3.5 1 05/14/20 01:51 05/19/20 20:24 7440-02-0 Selenium ND ug/L 10.0 4.7 1 05/14/20 01:51 05/19/20 20:24 7782-49-2 Silver ND ug/L 5.0 2.5 1 05/14/20 01:51 05/19/20 20:24 7440-22-4 Sodium 2150J ug/L 5000 611 1 05/14/20 01:51 05/19/20 20:24 7440-23-5 Tin 4.8J ug/L 5.0 4.7 1 05/14/20 01:51 05/19/20 20:24 7440-31-5 Vanadium ND ug/L 5.0 3.9 1 05/14/20 01:51 05/19/20 20:24 7440-62-2 Zinc ND ug/L 10.0 9.5 1 05/14/20 01:51 05/19/20 20:24 7440-66-6 7470 Mercury Mercury 8270E RVE Benzo(a)anthracene Chrysene Dibenz(a,h)anthracene bis(2- Ethyl hexyl)phthalate Indeno(1,2,3-cd)pyrene Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) 8260D MSV Low Level Landfill Acetone Acrylonitrile Benzene Bromochloromethane Bromodichloromethane Bromoform Bromomethane 2-Butanone (MEK) Date: 06/09/2020 08:57 AM Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services -Asheville 0.65 ug/L 0.20 0.12 1 05/20/20 17:30 05/21 /20 12:02 7439-97-6 Analytical Method: EPA 8270E Preparation Method: EPA 3510C Pace Analytical Services - Charlotte ND ug/L 10.0 1.5 1 05/12/20 18:13 05/19/20 23:04 56-55-3 ND ug/L 10.0 1.4 1 05/12/20 18:13 05/19/20 23:04 218-01-9 ND ug/L 10.0 1.6 1 05/12/20 18:13 05/19/20 23:04 53-70-3 ND ug/L 6.0 2.0 1 05/12/20 18:13 05/19/20 23:04 117-81-7 ND ug/L 10.0 1.7 1 05/12/20 18:13 05/19/20 23:04 193-39-5 104 % 13-130 92 % 13-130 124 % 25-130 Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 25.0 ND ug/L 10.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 1.0 ND ug/L 2.0 ND ug/L 5.0 1 05/12/20 18:13 05/19/20 23:04 4165-60-0 1 05/12/20 18:13 05/19/20 23:04 321-60-8 1 05/12/20 18:13 05/19/20 23:04 1718-51-0 6.2 1 05/19/20 07:16 67-64-1 0.90 1 05/19/20 07:16 107-13-1 0.15 1 05/19/20 07:16 71-43-2 0.34 1 05/19/20 07:16 74-97-5 0.26 1 05/19/20 07:16 75-27-4 0.62 1 05/19/20 07:16 75-25-2 0.62 1 05/19/20 07:16 74-83-9 3.3 1 05/19/20 07:16 78-93-3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. IH,IK,L1 Page 76 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-3R Lab ID: 92477016002 Collected: 05/07/20 08:55 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Carbon disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane 1,2-Dibromo-3-chloropropane Dibromochloromethane 1,2-Dibromoethane (EDB) Dibromomethane 1,2-Dichlorobenzene 1,4-Dichlorobenzene trans-1,4-Dichloro-2-butene Dichlorodifluoromethane 1,1-Dichloroethane 1,2-Dichloroethane 1,1-Dichloroethene cis-1,2-Dichloroethene trans-1,2-Dichloroethene 1,2-Dichloropropene cis-1,3-Dichloropropene trans- 1,3-Dichloropropene Ethylbenzene 2-Hexanone lodomethane Methylene Chloride 4-Methyl-2-pentanone (MIBK) Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Tetrahydrofuran Toluene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Date: 06/09/2020 08:57 AM Analytical Method: EPA 8260D Pace Analytical Services - Charlotte ND ug/L 2.0 0.40 1 05/19/20 07:16 75-15-0 ND ug/L 1.0 0.22 1 05/19/20 07:16 56-23-5 ND ug/L 1.0 0.23 1 05/19/20 07:16 108-90-7 ND ug/L 1.0 0.49 1 05/19/20 07:16 75-00-3 ND ug/L 5.0 2.3 1 05/19/20 07:16 67-66-3 ND ug/L 1.0 0.39 1 05/19/20 07:16 74-87-3 ND ug/L 5.0 0.26 1 05/19/20 07:16 96-12-8 ND ug/L 1.0 0.41 1 05/19/20 07:16 124-48-1 ND ug/L 1.0 0.26 1 05/19/20 07:16 106-93-4 ND ug/L 1.0 0.46 1 05/19/20 07:16 74-95-3 ND ug/L 1.0 0.29 1 05/19/20 07:16 95-50-1 ND ug/L 1.0 0.26 1 05/19/20 07:16 106-46-7 ND ug/L 1.0 0.54 1 05/19/20 07:16 110-57-6 L1,v1 ND ug/L 1.0 0.23 1 05/19/20 07:16 75-71-8 ND ug/L 1.0 0.27 1 05/19/20 07:16 75-34-3 ND ug/L 1.0 0.34 1 05/19/20 07:16 107-06-2 ND ug/L 1.0 0.24 1 05/19/20 07:16 75-35-4 ND ug/L 1.0 0.29 1 05/19/20 07:16 156-59-2 ND ug/L 1.0 0.25 1 05/19/20 07:16 156-60-5 ND ug/L 1.0 0.19 1 05/19/20 07:16 78-87-5 ND ug/L 1.0 0.30 1 05/19/20 07:16 10061-01-5 ND ug/L 1.0 0.31 1 05/19/20 07:16 10061-02-6 ND ug/L 1.0 0.26 1 05/19/20 07:16 100-41-4 ND ug/L 5.0 0.57 1 05/19/20 07:16 591-78-6 ND ug/L 20.0 12.5 1 05/19/20 07:16 74-88-4 ND ug/L 5.0 3.7 1 05/19/20 07:16 75-09-2 ND ug/L 5.0 4.5 1 05/19/20 07:16 108-10-1 ND ug/L 1.0 0.27 1 05/19/20 07:16 100-42-5 ND ug/L 1.0 0.34 1 05/19/20 07:16 630-20-6 ND ug/L 1.0 0.22 1 05/19/20 07:16 79-34-5 ND ug/L 1.0 0.16 1 05/19/20 07:16 127-18-4 ND ug/L 10.0 1.9 1 05/19/20 07:16 109-99-9 ND ug/L 1.0 0.24 1 05/19/20 07:16 108-88-3 ND ug/L 1.0 0.18 1 05/19/20 07:16 71-55-6 ND ug/L 1.0 0.24 1 05/19/20 07:16 79-00-5 ND ug/L 1.0 0.22 1 05/19/20 07:16 79-01-6 ND ug/L 1.0 0.31 1 05/19/20 07:16 75-69-4 ND ug/L 1.0 0.35 1 05/19/20 07:16 96-18-4 ND ug/L 2.0 1.4 1 05/19/20 07:16 108-05-4 IK ND ug/L 1.0 0.24 1 05/19/20 07:16 75-01-4 ND ug/L 2.0 0.41 1 05/19/20 07:16 179601-23-1 ND ug/L 1.0 0.22 1 05/19/20 07:16 95-47-6 100 % 70-130 1 05/19/20 07:16 460-00-4 93 % 70-130 1 05/19/20 07:16 17060-07-0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 77 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: OSR LANDFILL GW Pace Project No.: 92477011 Sample: MW-3R Lab ID: 92477016002 Collected: 05/07/20 08:55 Received: 05/08/20 17:07 Matrix: Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Landfill Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Surrogates Toluene-d8 (S) 99 % 70-130 1 05/19/20 07:16 2037-26-5 8260D MSV SIM Analytical Method: EPA 8260D Mod. Pace Analytical Services - Charlotte 1,4-Dioxane (p-Dioxane) ND ug/L 2.0 1.2 1 05/15/20 16:27 123-91-1 Surrogates 1,2-Dichloroethane-d4 (S) 107 % 50-150 1 05/15/20 16:27 17060-07-0 Toluene-d8 (S) 88 % 50-150 1 05/15/20 16:27 2037-26-5 2320B Alkalinity Analytical Method: SM 2320B-2011 Pace Analytical Services -Asheville Alkalinity, Total as CaCO3 70900 ug/L 5000 5000 1 05/16/20 03:25 2540C Total Dissolved Solids Analytical Method: SM 2540C-2011 Pace Analytical Services -Asheville Total Dissolved Solids 146000 ug/L 25000 25000 1 05/12/20 23:20 4500S2D Sulfide Water Analytical Method: SM 4500-S2D-2011 Pace Analytical Services -Asheville Sulfide ND ug/L 100 50.0 1 05/12/20 20:45 18496-25-8 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Sulfate 801J ug/L 1000 500 1 05/14/2010:59 14808-79-8 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 3320 ug/L 1000 500 1 05/13/20 20:27 16887-00-6 450OCNE Cyanide, Total Analytical Method: SM 4500-CN-E-2011 Preparation Method: SM 4500-CN-E-2011 Pace Analytical Services -Asheville Cyanide ND ug/L 8.0 6.0 1 05/20/2010:03 05/20/2017:26 57-12-5 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 78 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 1474966 Analysis Method: EPA 8151 QC Batch Method: 8151A Analysis Description: Chlorinated Herb. (GC) 8151 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92477008001, 92477008002, 92477008003, 92477008004 METHOD BLANK: R3528604-1 Matrix: Water Associated Lab Samples: 92477008001, 92477008002, 92477008003, 92477008004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 2,4-D ug/L ND 2.00 0.547 05/15/20 15:27 2,4,5-TP (Silvex) ug/L ND 2.00 0.335 05/15/20 15:27 2,4-DCAA (S) % 58.2 14.0-158 05/15/20 15:27 METHOD BLANK: R3528716-1 Matrix: Water Associated Lab Samples: 92477008001, 92477008002, 92477008003, 92477008004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 2,4-D ug/L ND 2.00 0.547 05/16/20 11:36 2,4,5-TP (Silvex) ug/L ND 2.00 0.335 05/16/20 11:36 2,4-DCAA (S) % 57 14.0-158 05/16/20 11:36 LABORATORY CONTROL SAMPLE & LCSD: R3528716-2 R3528716-3 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers 2,4-D ug/L 5.00 2.68 2.69 53.6 53.8 50.0-120 0.372 20 2,4,5-TP (Silvex) ug/L 5.00 2.93 2.94 58.6 58.8 50.0-125 0.341 20 2,4-DCAA (S) % 59.6 60.4 14.0-158 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 79 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 1476953 Analysis Method: EPA 8151 QC Batch Method: 8151A Analysis Description: Chlorinated Herb. (GC) 8151 Laboratory: Pace National - Mt. Juliet Associated Lab Samples: 92477008005, 92477008006 METHOD BLANK: R3528967-1 Matrix: Water Associated Lab Samples: 92477008005, 92477008006 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 2,4-D ug/L ND 2.00 0.547 05/17/20 13:04 2,4,5-TP (Silvex) ug/L ND 2.00 0.335 05/17/20 13:04 2,4-DCAA (S) % 58.2 14.0-158 05/17/20 13:04 LABORATORY CONTROL SAMPLE & LCSD: R3528967-2 R3528967-3 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers 2,4-D ug/L 5.00 2.57 2.68 51.4 53.6 50.0-120 4.19 20 2,4,5-TP (Silvex) ug/L 5.00 3.00 3.05 60.0 61.0 50.0-125 1.65 20 2,4-DCAA (S) % 57.8 56.4 14.0-158 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 80 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541804 Analysis Method: EPA 7470A QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477008001, 92477008002, 92477008003, 92477008004 METHOD BLANK: 2886897 Matrix: Water Associated Lab Samples: 92477008001, 92477008002, 92477008003, 92477008004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury ug/L ND 0.20 0.12 05/15/2016:23 LABORATORY CONTROL SAMPLE: 2886898 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.6 102 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2886899 2886900 MS MSD 92476928018 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L ND 2.5 2.5 2.5 2.6 99 102 75-125 3 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 81 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 542610 Analysis Method: EPA 7470A QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477008005,92477008006,92477011001,92477011002,92477011003,92477011004,92477011005, 92477011006,92477011007,92477011008,92477011009,92477011010,92477013001,92477013002, 92477016001,92477016002 METHOD BLANK: 2890802 Matrix: Water Associated Lab Samples: 92477008005,92477008006,92477011001,92477011002,92477011003,92477011004,92477011005, 92477011006,92477011007,92477011008,92477011009,92477011010,92477013001,92477013002, 92477016001,92477016002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Mercury ug/L ND 0.20 0.12 05/21/2011:12 LABORATORY CONTROL SAMPLE: 2890803 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury ug/L 2.5 2.6 104 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2890804 2890805 MS MSD 92477008005 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Mercury ug/L ND 2.5 2.5 3.4 3.6 135 144 75-125 7 25 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 82 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541473 Analysis Method: EPA 6010D QC Batch Method: EPA 3010A Analysis Description: 6010 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477008001, 92477008002, 92477008003, 92477008004, 92477008005 METHOD BLANK: 2885497 Matrix: Water Associated Lab Samples: 92477008001, 92477008002, 92477008003, 92477008004, 92477008005 Blank Reporting Parameter Units Result Limit MDL Analyzed Antimony ug/L ND 5.0 3.0 05/21/20 02:09 Arsenic ug/L ND 10.0 4.7 05/21/20 02:09 Barium ug/L ND 5.0 3.5 05/21/20 02:09 Beryllium ug/L ND 1.0 0.70 05/21/20 02:09 Cadmium ug/L ND 1.0 0.40 05/21/20 02:09 Chromium ug/L ND 5.0 3.7 05/21/20 02:09 Cobalt ug/L ND 5.0 3.6 05/21/20 02:09 Copper ug/L ND 5.0 4.3 05/21/20 02:09 Iron ug/L ND 50.0 41.5 05/21/20 02:09 Lead ug/L ND 5.0 4.5 05/21/20 02:09 Manganese ug/L ND 5.0 3.4 05/21/20 02:09 Nickel ug/L ND 5.0 3.5 05/21/20 02:09 Selenium ug/L ND 10.0 4.7 05/21/20 02:09 Silver ug/L ND 5.0 2.5 05/21/20 02:09 Sodium ug/L ND 5000 611 05/21/20 02:09 Tin ug/L ND 5.0 4.7 05/21/20 02:09 Vanadium ug/L ND 5.0 3.9 05/21/20 02:09 Zinc ug/L ND 10.0 9.5 05/21/20 02:09 LABORATORY CONTROL SAMPLE: Parameter 2885498 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 530 106 80-120 Arsenic ug/L 500 531 106 80-120 Barium ug/L 500 529 106 80-120 Beryllium ug/L 500 521 104 80-120 Cadmium ug/L 500 527 105 80-120 Chromium ug/L 500 512 102 80-120 Cobalt ug/L 500 519 104 80-120 Copper ug/L 500 547 109 80-120 Iron ug/L 5000 4870 97 80-120 Lead ug/L 500 522 104 80-120 Manganese ug/L 500 513 103 80-120 Nickel ug/L 500 520 104 80-120 Selenium ug/L 500 532 106 80-120 Silver ug/L 250 257 103 80-120 Sodium ug/L 5000 5350 107 80-120 Tin ug/L 500 519 104 80-120 Vanadium ug/L 500 507 101 80-120 Qualifiers Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 83 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 LABORATORY CONTROL SAMPLE: 2885498 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Zinc ug/L 500 507 101 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2885499 2885500 MS MSD 92476856023 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 564 556 113 111 75-125 1 20 Arsenic ug/L 5AJ 500 500 566 560 112 111 75-125 1 20 Barium ug/L 46.9 500 500 607 598 112 110 75-125 2 20 Beryllium ug/L ND 500 500 551 541 110 108 75-125 2 20 Cadmium ug/L ND 500 500 568 560 114 112 75-125 1 20 Chromium ug/L ND 500 500 547 539 109 107 75-125 2 20 Cobalt ug/L ND 500 500 553 543 110 108 75-125 2 20 Copper ug/L ND 500 500 576 571 115 113 75-125 1 20 Iron ug/L 8530 5000 5000 14100 13800 111 105 75-125 2 20 Lead ug/L ND 500 500 545 539 109 108 75-125 1 20 Manganese ug/L 182 500 500 731 719 110 107 75-125 2 20 Nickel ug/L 5.4 500 500 559 553 111 109 75-125 1 20 Selenium ug/L ND 500 500 584 578 116 115 75-125 1 20 Silver ug/L ND 250 250 266 262 106 105 75-125 1 20 Sodium ug/L 3420J 5000 5000 9240 9050 116 113 75-125 2 20 Tin ug/L ND 500 500 549 540 110 108 75-125 2 20 Vanadium ug/L 14.4 500 500 557 543 108 106 75-125 3 20 Zinc ug/L ND 500 500 555 550 109 108 75-125 1 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 84 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541474 Analysis Method: EPA 6010D QC Batch Method: EPA 3010A Analysis Description: 6010 MET Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477008006, 92477011001, 92477011002, 92477011003, 92477011004, 92477011005, 92477011006, 92477011007, 92477011008, 92477011009, 92477011010, 92477013001, 92477013002, 92477016001, 92477016002 METHOD BLANK: 2885501 Matrix: Water Associated Lab Samples: 92477008006, 92477011001, 92477011002, 92477011003, 92477011004, 92477011005, 92477011006, 92477011007, 92477011008, 92477011009, 92477011010, 92477013001, 92477013002, 92477016001, 92477016002 Parameter Units Antimony ug/L Arsenic ug/L Barium ug/L Beryllium ug/L Cadmium ug/L Chromium ug/L Cobalt ug/L Copper ug/L Iron ug/L Lead ug/L Manganese ug/L Nickel ug/L Selenium ug/L Silver ug/L Sodium ug/L Tin ug/L Vanadium ug/L Zinc ug/L Blank Result Reporting Limit MDL Analyzed Qualifiers ND 5.0 3.0 05/19/2019:11 ND 10.0 4.7 05/19/2019:11 ND 5.0 3.5 05/19/2019:11 ND 1.0 0.70 05/19/2019:11 ND 1.0 0.40 05/19/2019:11 ND 5.0 3.7 05/19/2019:11 ND 5.0 3.6 05/19/2019:11 ND 5.0 4.3 05/19/2019:11 ND 50.0 41.5 05/19/2019:11 ND 5.0 4.5 05/19/2019:11 ND 5.0 3.4 05/19/2019:11 ND 5.0 3.5 05/19/2019:11 ND 10.0 4.7 05/19/2019:11 ND 5.0 2.5 05/19/2019:11 ND 5000 611 05/19/2019:11 ND 5.0 4.7 05/19/2019:11 ND 5.0 3.9 05/19/2019:11 ND 10.0 9.5 05/19/2019:11 LABORATORY CONTROL SAMPLE: Parameter 2885502 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Antimony ug/L 500 464 93 80-120 Arsenic ug/L 500 463 93 80-120 Barium ug/L 500 490 98 80-120 Beryllium ug/L 500 471 94 80-120 Cadmium ug/L 500 479 96 80-120 Chromium ug/L 500 485 97 80-120 Cobalt ug/L 500 475 95 80-120 Copper ug/L 500 488 98 80-120 Iron ug/L 5000 4750 95 80-120 Lead ug/L 500 471 94 80-120 Manganese ug/L 500 485 97 80-120 Nickel ug/L 500 473 95 80-120 Selenium ug/L 500 450 90 80-120 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 85 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 LABORATORY CONTROL SAMPLE: 2885502 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Silver ug/L 250 233 93 80-120 Sodium ug/L 5000 4910J 98 80-120 Tin ug/L 500 462 92 80-120 Vanadium ug/L 500 485 97 80-120 Zinc ug/L 500 456 91 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2885503 2885504 MS MSD 92477008006 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Antimony ug/L ND 500 500 497 484 99 97 75-125 3 20 Arsenic ug/L ND 500 500 490 475 97 94 75-125 3 20 Barium ug/L ND 500 500 516 503 103 100 75-125 2 20 Beryllium ug/L ND 500 500 497 488 99 98 75-125 2 20 Cadmium ug/L ND 500 500 505 494 101 99 75-125 2 20 Chromium ug/L ND 500 500 507 497 101 99 75-125 2 20 Cobalt ug/L ND 500 500 500 487 100 97 75-125 3 20 Copper ug/L ND 500 500 509 494 102 99 75-125 3 20 Iron ug/L ND 5000 5000 5010 4860 100 97 75-125 3 20 Lead ug/L ND 500 500 493 485 99 97 75-125 2 20 Manganese ug/L ND 500 500 508 498 102 100 75-125 2 20 Nickel ug/L ND 500 500 495 485 99 97 75-125 2 20 Selenium ug/L ND 500 500 501 490 100 98 75-125 2 20 Silver ug/L ND 250 250 237 232 95 93 75-125 2 20 Sodium ug/L ND 5000 5000 6140 50001 122 99 75-125 20 Tin ug/L ND 500 500 484 472 96 94 75-125 3 20 Vanadium ug/L ND 500 500 508 497 102 99 75-125 2 20 Zinc ug/L ND 500 500 485 476 97 95 75-125 2 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 86 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 542112 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92477011001, 92477011002, 92477011003, 92477011004 METHOD BLANK: 2888661 Matrix: Water Associated Lab Samples: 92477011001, 92477011002, 92477011003, 92477011004 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.34 05/18/20 11:33 1,1,1-Trichloroethane ug/L ND 1.0 0.18 05/18/20 11:33 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 05/18/20 11:33 1,1,2-Trichloroethane ug/L ND 1.0 0.24 05/18/20 11:33 1,1-Dichloroethane ug/L ND 1.0 0.27 05/18/20 11:33 1,1-Dichloroethene ug/L ND 1.0 0.24 05/18/20 11:33 1,2,3-Trichloropropane ug/L ND 1.0 0.35 05/18/20 11:33 1,2-Dibromo-3-chloropropane ug/L ND 5.0 0.26 05/18/20 11:33 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.26 05/18/20 11:33 1,2-Dichlorobenzene ug/L ND 1.0 0.29 05/18/20 11:33 1,2-Dichloroethane ug/L ND 1.0 0.34 05/18/20 11:33 1,2-Dichloropropane ug/L ND 1.0 0.19 05/18/20 11:33 1,4-Dichlorobenzene ug/L ND 1.0 0.26 05/18/20 11:33 2-Butanone (MEK) ug/L ND 5.0 3.3 05/18/20 11:33 2-Hexanone ug/L ND 5.0 0.57 05/18/20 11:33 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 4.5 05/18/20 11:33 Acetone ug/L ND 25.0 6.2 05/18/20 11:33 Acrylonitrile ug/L ND 10.0 0.90 05/18/20 11:33 Benzene ug/L ND 1.0 0.15 05/18/20 11:33 Bromochloromethane ug/L ND 1.0 0.34 05/18/20 11:33 Bromodichloromethane ug/L ND 1.0 0.26 05/18/20 11:33 Bromoform ug/L ND 1.0 0.62 05/18/20 11:33 Bromomethane ug/L ND 2.0 0.62 05/18/20 11:33 IK,v2 Carbon disulfide ug/L ND 2.0 0.40 05/18/20 11:33 Carbon tetrachloride ug/L ND 1.0 0.22 05/18/20 11:33 Chlorobenzene ug/L ND 1.0 0.23 05/18/20 11:33 Chloroethane ug/L ND 1.0 0.49 05/18/20 11:33 IK Chloroform ug/L ND 5.0 2.3 05/18/20 11:33 Chloromethane ug/L ND 1.0 0.39 05/18/20 11:33 IK cis-1,2-Dichloroethene ug/L ND 1.0 0.29 05/18/20 11:33 cis-1,3-Dichloropropene ug/L ND 1.0 0.30 05/18/20 11:33 Dibromochloromethane ug/L ND 1.0 0.41 05/18/20 11:33 Dibromomethane ug/L ND 1.0 0.46 05/18/20 11:33 Dichlorodifluoromethane ug/L ND 1.0 0.23 05/18/20 11:33 IK Ethylbenzene ug/L ND 1.0 0.26 05/18/20 11:33 lodomethane ug/L ND 20.0 12.5 05/18/20 11:33 m&p-Xylene ug/L ND 2.0 0.41 05/18/20 11:33 Methylene Chloride ug/L ND 5.0 3.7 05/18/20 11:33 o-Xylene ug/L ND 1.0 0.22 05/18/20 11:33 Styrene ug/L ND 1.0 0.27 05/18/20 11:33 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 87 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 METHOD BLANK: 2888661 Matrix: Water Associated Lab Samples: 92477011001, 92477011002, 92477011003, 92477011004 Blank Reporting Parameter Units Result Limit MDL Analyzed Tetrachloroethene ug/L ND 1.0 0.16 05/18/20 11:33 Tetrahydrofuran ug/L ND 10.0 1.9 05/18/20 11:33 Toluene ug/L ND 1.0 0.24 05/18/20 11:33 trans-1,2-Dichloroethene ug/L ND 1.0 0.25 05/18/20 11:33 trans- 1,3-Dichloropropene ug/L ND 1.0 0.31 05/18/20 11:33 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.54 05/18/20 11:33 Trichloroethene ug/L ND 1.0 0.22 05/18/20 11:33 Trichlorofluoromethane ug/L ND 1.0 0.31 05/18/20 11:33 Vinyl acetate ug/L ND 2.0 1.4 05/18/20 11:33 Vinyl chloride ug/L ND 1.0 0.24 05/18/20 11:33 1,2-Dichloroethane-d4 (S) % 98 70-130 05/18/20 11:33 4-Bromofluorobenzene (S) % 97 70-130 05/18/20 11:33 Toluene-d8 (S) % 101 70-130 05/18/20 11:33 LABORATORY CONTROL SAMPLE: 2888662 Parameter Qualifiers IH IK IK Spike LCS LCS % Rec Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 52.2 104 70-130 1,1,1-Trichloroethane ug/L 50 48.3 97 70-130 1,1,2,2-Tetrachloroethane ug/L 50 49.9 100 70-130 1,1,2-Trichloroethane ug/L 50 50.4 101 70-130 1,1-Dichloroethane ug/L 50 46.5 93 70-130 1,1-Dichloroethene ug/L 50 48.3 97 70-130 1,2,3-Trichloropropane ug/L 50 51.0 102 70-130 1,2-Dibromo-3-chloropropane ug/L 50 56.3 113 70-130 1,2-Dibromoethane (EDB) ug/L 50 52.0 104 70-130 1,2-Dichlorobenzene ug/L 50 51.9 104 70-130 1,2-Dichloroethane ug/L 50 46.2 92 70-130 1,2-Dichloropropane ug/L 50 49.2 98 70-130 1,4-Dichlorobenzene ug/L 50 51.6 103 70-130 2-Butanone (MEK) ug/L 100 102 102 64-135 2-Hexanone ug/L 100 104 104 66-135 4-Methyl-2-pentanone (MIBK) ug/L 100 107 107 70-130 Acetone ug/L 100 96.9 97 61-157 Acrylonitrile ug/L 250 236 95 61-143 Benzene ug/L 50 49.0 98 70-130 Bromochloromethane ug/L 50 47.2 94 70-130 Bromodichloromethane ug/L 50 53.1 106 70-130 Bromoform ug/L 50 53.3 107 70-130 Bromomethane ug/L 50 37.6 75 38-130IK,v3 Carbon disulfide ug/L 50 47.3 95 68-130 Carbon tetrachloride ug/L 50 51.8 104 70-130 Chlorobenzene ug/L 50 50.1 100 70-130 Chloroethane ug/L 50 33.4 67 37-142 IK Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 88 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 LABORATORY CONTROL SAMPLE: Parameter 2888662 Units Spike LCS Conc. Result Chloroform ug/L 50 Chloromethane ug/L 50 cis-1,2-Dichloroethene ug/L 50 cis-1,3-Dichloropropene ug/L 50 Dibromochloromethane ug/L 50 Dibromomethane ug/L 50 Dichlorodifluoromethane ug/L 50 Ethylbenzene ug/L 50 lodomethane ug/L 100 m&p-Xylene ug/L 100 Methylene Chloride ug/L 50 o-Xylene ug/L 50 Styrene ug/L 50 Tetrachloroethene ug/L 50 Tetrahydrofuran ug/L 500 Toluene ug/L 50 trans-1,2-Dichloroethene ug/L 50 trans- 1,3-Dichloropropene ug/L 50 trans-1,4-Dichloro-2-butene ug/L 50 Trichloroethene ug/L 50 Trichlorofluoromethane ug/L 50 Vinyl acetate ug/L 100 Vinyl chloride ug/L 50 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % LCS % Rec % Rec Limits Qualifiers 46.5 93 70-130 41.4 83 48-1301K 46.8 94 70-130 51.6 103 70-130 53.6 107 70-130 49.8 100 70-130 41.6 83 53-134 IK 47.1 94 70-130 75.3 75 40-130 95.0 95 70-130 44.2 88 67-132 48.1 96 70-131 51.9 104 70-130 51.1 102 69-130 467 93 62-130 47.5 95 70-130 47.6 95 70-130 52.4 105 70-130 65.0 130 35-1891H 48.4 97 70-130 45.3 91 63-1301K 111 111 55-143 49.5 99 70-131 IK 89 70-130 98 70-130 101 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2888663 MS 92476718010 Spike Parameter Units Result Conc. MSD Spike Conc. 2888664 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 21.3 20.5 106 103 73-134 3 30 1,1,1-Trichloroethane ug/L ND 20 20 20.1 20.7 101 103 82-143 3 30 1,1,2,2-Tetrachloroethane ug/L ND 20 20 21.2 22.1 106 111 70-136 4 30 1,1,2-Trichloroethane ug/L ND 20 20 19.7 19.7 98 98 70-135 0 30 1,1-Dichloroethane ug/L 4.8 20 20 26.5 27.0 108 111 70-139 2 30 1,1-Dichloroethene ug/L ND 20 20 23.1 23.3 116 117 70-154 1 30 1,2,3-Trichloropropane ug/L ND 20 20 21.1 21.6 106 108 71-137 2 30 1,2-Dibromo-3- ug/L ND 20 20 18.5 19.5 93 98 65-134 5 30 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 20 20 21.5 22.2 107 111 70-137 4 30 1,2-Dichlorobenzene ug/L ND 20 20 23.7 24.5 119 123 70-133 3 30 1,2-Dichloroethane ug/L ND 20 20 20.8 22.3 104 111 70-137 7 30 1,2-Dichloropropane ug/L 0.84J 20 20 23.6 24.0 114 116 70-140 2 30 1,4-Dichlorobenzene ug/L 4.1 20 20 27.7 28.7 118 123 70-133 4 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 89 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2888663 2888664 MS MSD 92476718010 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 2-Butanone (MEK) ug/L ND 40 40 39.6 41.1 99 103 60-139 4 30 2-Hexanone ug/L ND 40 40 44.4 45.8 111 114 65-138 3 30 4-Methyl-2-pentanone ug/L ND 40 40 41.4 40.8 104 102 65-135 1 30 (MIBK) Acetone ug/L ND 40 40 49.2 54.1 123 135 60-148 10 30 Acrylonitrile ug/L ND 100 100 104 104 104 104 64-147 0 30 Benzene ug/L 1.4 20 20 23.4 23.1 110 108 70-151 1 30 Bromochloromethane ug/L ND 20 20 19.6 20.4 98 102 70-141 4 30 Bromodichloromethane ug/L ND 20 20 19.6 20.1 98 100 70-138 2 30 Bromoform ug/L ND 20 20 18.1 18.4 90 92 63-130 2 30 Bromomethane ug/L ND 20 20 24.4 24.7 122 123 15-152 1 30 IH,v2 Carbon disulfide ug/L ND 20 20 21.7 21.2 109 106 69-149 2 30 Carbon tetrachloride ug/L ND 20 20 21.5 21.3 108 107 70-143 1 30 Chlorobenzene ug/L 8.2 20 20 32.2 31.5 120 116 70-138 2 30 Chloroethane ug/L ND 20 20 20.5 21.8 102 109 52-163 6 30 Chloroform ug/L ND 20 20 21.5 20.8 108 104 70-139 3 30 Chloromethane ug/L ND 20 20 18.8 18.1 94 91 41-139 4 30 cis-1,2-Dichloroethene ug/L 16.4 20 20 37.6 38.5 106 110 70-141 2 30 cis-1,3-Dichloropropene ug/L ND 20 20 19.9 20.4 100 102 70-137 2 30 Dibromochloromethane ug/L ND 20 20 20.4 21.2 102 106 70-134 4 30 Dibromomethane ug/L ND 20 20 20.7 20.4 103 102 70-138 1 30 Dichlorodifluoromethane ug/L ND 20 20 15.9 15.8 80 79 47-155 1 30 Ethylbenzene ug/L ND 20 20 22.3 22.9 111 114 66-153 3 30 lodomethane ug/L ND 40 40 23.3 24.5 58 61 20-138 5 30 m&p-Xylene ug/L ND 40 40 47.1 46.1 118 115 69-152 2 30 Methylene Chloride ug/L ND 20 20 24.9 24.9 125 125 42-159 0 30 o-Xylene ug/L ND 20 20 23.1 23.4 116 117 70-148 1 30 Styrene ug/L ND 20 20 18.6 16.9 93 85 70-135 10 30 Tetrachloroethene ug/L 8.1 20 20 31.7 31.4 118 117 59-143 1 30 Tetrahydrofuran ug/L ND 200 200 209 219 104 110 70-133 5 30 Toluene ug/L ND 20 20 20.6 20.0 103 100 59-148 3 30 trans-1,2-Dichloroethene ug/L ND 20 20 22.4 22.8 112 114 70-146 2 30 trans-1,3-Dichloropropene ug/L ND 20 20 19.1 19.7 96 98 70-135 3 30 trans-1,4-Dichloro-2-butene ug/L ND 20 20 21.7 21.8 108 109 47-135 1 30 IH Trichloroethene ug/L 5.0 20 20 27.1 27.0 111 110 70-147 0 30 Trichlorofluoromethane ug/L ND 20 20 18.9 18.3 95 92 70-148 3 30 Vinyl acetate ug/L ND 40 40 42.9 42.1 107 105 49-151 2 30 v1 Vinyl chloride ug/L 0.881 20 20 22.3 22.1 107 106 70-156 1 30 1,2-Dichloroethane-d4 (S) % 107 105 70-130 4-Bromofluorobenzene (S) % 104 99 70-130 Toluene-d8 (S) % 97 99 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 90 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 542117 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92477008002, 92477013001, 92477016001 METHOD BLANK: 2888703 Matrix: Associated Lab Samples: 92477008002, 92477013001, 92477016001 Blank Parameter Units Result Water Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.34 05/19/20 00:24 1,1,1-Trichloroethane ug/L ND 1.0 0.18 05/19/20 00:24 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 05/19/20 00:24 1,1,2-Trichloroethane ug/L ND 1.0 0.24 05/19/20 00:24 1,1-Dichloroethane ug/L ND 1.0 0.27 05/19/20 00:24 1,1-Dichloroethene ug/L ND 1.0 0.24 05/19/20 00:24 1,2,3-Trichloropropane ug/L ND 1.0 0.35 05/19/20 00:24 1,2-Dibromo-3-chloropropane ug/L ND 5.0 0.26 05/19/20 00:24 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.26 05/19/20 00:24 1,2-Dichlorobenzene ug/L ND 1.0 0.29 05/19/20 00:24 1,2-Dichloroethane ug/L ND 1.0 0.34 05/19/20 00:24 1,2-Dichloropropane ug/L ND 1.0 0.19 05/19/20 00:24 1,4-Dichlorobenzene ug/L ND 1.0 0.26 05/19/20 00:24 2-Butanone (MEK) ug/L ND 5.0 3.3 05/19/20 00:24 2-Hexanone ug/L ND 5.0 0.57 05/19/20 00:24 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 4.5 05/19/20 00:24 Acetone ug/L ND 25.0 6.2 05/19/20 00:24 Acrylonitrile ug/L ND 10.0 0.90 05/19/20 00:24 Benzene ug/L ND 1.0 0.15 05/19/20 00:24 Bromochloromethane ug/L ND 1.0 0.34 05/19/20 00:24 Bromodichloromethane ug/L ND 1.0 0.26 05/19/20 00:24 Bromoform ug/L ND 1.0 0.62 05/19/20 00:24 Bromomethane ug/L ND 2.0 0.62 05/19/20 00:24 Carbon disulfide ug/L ND 2.0 0.40 05/19/20 00:24 Carbon tetrachloride ug/L ND 1.0 0.22 05/19/20 00:24 Chlorobenzene ug/L ND 1.0 0.23 05/19/20 00:24 Chloroethane ug/L ND 1.0 0.49 05/19/20 00:24 Chloroform ug/L ND 5.0 2.3 05/19/20 00:24 Chloromethane ug/L ND 1.0 0.39 05/19/20 00:24 cis-1,2-Dichloroethene ug/L ND 1.0 0.29 05/19/20 00:24 cis-1,3-Dichloropropene ug/L ND 1.0 0.30 05/19/20 00:24 Dibromochloromethane ug/L ND 1.0 0.41 05/19/20 00:24 Dibromomethane ug/L ND 1.0 0.46 05/19/20 00:24 Dichlorodifluoromethane ug/L ND 1.0 0.23 05/19/20 00:24 Ethylbenzene ug/L ND 1.0 0.26 05/19/20 00:24 lodomethane ug/L ND 20.0 12.5 05/19/20 00:24 m&p-Xylene ug/L ND 2.0 0.41 05/19/20 00:24 Methylene Chloride ug/L ND 5.0 3.7 05/19/20 00:24 o-Xylene ug/L ND 1.0 0.22 05/19/20 00:24 Styrene ug/L ND 1.0 0.27 05/19/20 00:24 Qualifiers v1 I K,v2 IK IK IK v2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 91 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 METHOD BLANK: 2888703 Matrix: Associated Lab Samples: 92477008002, 92477013001, 92477016001 Blank Parameter Units Result Water Reporting Limit MDL Analyzed Tetrachloroethene ug/L ND 1.0 0.16 05/19/20 00:24 Tetrahydrofuran ug/L ND 10.0 1.9 05/19/20 00:24 Toluene ug/L ND 1.0 0.24 05/19/20 00:24 trans-1,2-Dichloroethene ug/L ND 1.0 0.25 05/19/20 00:24 trans- 1,3-Dichloropropene ug/L ND 1.0 0.31 05/19/20 00:24 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.54 05/19/20 00:24 Trichloroethene ug/L ND 1.0 0.22 05/19/20 00:24 Trichlorofluoromethane ug/L ND 1.0 0.31 05/19/20 00:24 Vinyl acetate ug/L ND 2.0 1.4 05/19/20 00:24 Vinyl chloride ug/L ND 1.0 0.24 05/19/20 00:24 1,2-Dichloroethane-d4 (S) % 102 70-130 05/19/20 00:24 4-Bromofluorobenzene (S) % 97 70-130 05/19/20 00:24 Toluene-d8 (S) % 102 70-130 05/19/20 00:24 LABORATORY CONTROL SAMPLE: 2888704 Parameter Qualifiers Z IK v1 IK Spike LCS LCS % Rec Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 55.7 111 70-130 1,1,1-Trichloroethane ug/L 50 52.5 105 70-130 1,1,2,2-Tetrachloroethane ug/L 50 53.5 107 70-130 1,1,2-Trichloroethane ug/L 50 54.0 108 70-130 1,1-Dichloroethane ug/L 50 51.7 103 70-130 1,1-Dichloroethene ug/L 50 53.0 106 70-130 1,2,3-Trichloropropane ug/L 50 55.2 110 70-130 1,2-Dibromo-3-chloropropane ug/L 50 58.4 117 70-130 1,2-Dibromoethane (EDB) ug/L 50 54.7 109 70-130 1,2-Dichlorobenzene ug/L 50 53.3 107 70-130 1,2-Dichloroethane ug/L 50 51.9 104 70-130 1,2-Dichloropropane ug/L 50 54.4 109 70-130 1,4-Dichlorobenzene ug/L 50 52.0 104 70-130 2-Butanone (MEK) ug/L 100 119 119 64-135 2-Hexanone ug/L 100 117 117 66-135 4-Methyl-2-pentanone (MIBK) ug/L 100 121 121 70-130 v1 Acetone ug/L 100 119 119 61-157 Acrylonitrile ug/L 250 259 104 61-143 Benzene ug/L 50 53.0 106 70-130 Bromochloromethane ug/L 50 48.8 98 70-130 Bromodichloromethane ug/L 50 56.4 113 70-130 Bromoform ug/L 50 56.0 112 70-130 Bromomethane ug/L 50 37.1 74 38-130lK,v3 Carbon disulfide ug/L 50 52.3 105 68-130 Carbon tetrachloride ug/L 50 55.3 111 70-130 Chlorobenzene ug/L 50 53.2 106 70-130 Chloroethane ug/L 50 37.6 75 37-142 IK Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 92 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 LABORATORY CONTROL SAMPLE: Parameter 2888704 Units Spike Conc. LCS LCS Result % Rec Chloroform ug/L 50 51.3 Chloromethane ug/L 50 47.6 cis-1,2-Dichloroethene ug/L 50 52.0 cis-1,3-Dichloropropene ug/L 50 55.3 Dibromochloromethane ug/L 50 56.6 Dibromomethane ug/L 50 51.6 Dichlorodifluoromethane ug/L 50 50.0 Ethylbenzene ug/L 50 50.6 lodomethane ug/L 100 78.8 m&p-Xylene ug/L 100 103 Methylene Chloride ug/L 50 48.7 o-Xylene ug/L 50 51.7 Styrene ug/L 50 54.8 Tetrachloroethene ug/L 50 52.4 Tetrahydrofuran ug/L 500 533 Toluene ug/L 50 51.1 trans-1,2-Dichloroethene ug/L 50 51.6 trans- 1,3-Dichloropropene ug/L 50 56.0 trans-1,4-Dichloro-2-butene ug/L 50 88.6 Trichloroethene ug/L 50 51.5 Trichlorofluoromethane ug/L 50 51.6 Vinyl acetate ug/L 100 120 Vinyl chloride ug/L 50 56.1 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % % Rec Limits Qualifiers 103 70-130 95 48-1301K 104 70-130 111 70-130 113 70-130 103 70-130 100 53-1341K 101 70-130 79 40-130 v3 103 70-130 97 67-132 103 70-131 110 70-130 105 69-130 107 62-130 102 70-130 103 70-130 112 70-130 177 35-1891H 103 70-130 103 63-1301K 120 55-143 v1 112 70-131 IK 96 70-130 99 70-130 103 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2888705 MS 92476718003 Spike Parameter Units Result Conc. MSD Spike Conc. 2888706 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 22.3 21.7 111 108 73-134 3 30 1,1,1-Trichloroethane ug/L ND 20 20 20.3 21.8 101 109 82-143 7 30 1,1,2,2-Tetrachloroethane ug/L ND 20 20 21.3 21.7 106 109 70-136 2 30 1,1,2-Trichloroethane ug/L ND 20 20 19.7 20.0 98 100 70-135 1 30 1,1-Dichloroethane ug/L ND 20 20 21.8 22.8 109 114 70-139 5 30 1,1-Dichloroethene ug/L ND 20 20 22.7 24.1 114 121 70-154 6 30 1,2,3-Trichloropropane ug/L ND 20 20 21.4 22.0 107 110 71-137 3 30 1,2-Dibromo-3- ug/L ND 20 20 18.7 18.4 94 92 65-134 2 30 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 20 20 21.5 22.1 107 111 70-137 3 30 1,2-Dichlorobenzene ug/L ND 20 20 24.1 25.8 121 129 70-133 7 30 1,2-Dichloroethane ug/L ND 20 20 21.5 22.3 108 111 70-137 3 30 1,2-Dichloropropane ug/L ND 20 20 22.3 22.6 112 113 70-140 1 30 1,4-Dichlorobenzene ug/L ND 20 20 24.2 23.9 121 120 70-133 1 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 93 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2888705 2888706 MS MSD 92476718003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 2-Butanone (MEK) ug/L ND 40 40 37.8 40.3 94 101 60-139 6 30 2-Hexanone ug/L ND 40 40 43.5 43.4 109 108 65-138 0 30 4-Methyl-2-pentanone ug/L ND 40 40 39.2 40.7 98 102 65-135 4 30 (MIBK) Acetone ug/L ND 40 40 38.9 42.2 97 106 60-148 8 30 Acrylonitrile ug/L ND 100 100 102 108 102 108 64-147 5 30 Benzene ug/L ND 20 20 21.7 23.1 109 115 70-151 6 30 Bromochloromethane ug/L ND 20 20 19.0 21.2 95 106 70-141 11 30 Bromodichloromethane ug/L ND 20 20 19.4 20.2 97 101 70-138 4 30 Bromoform ug/L ND 20 20 17.3 18.4 86 92 63-130 7 30 Bromomethane ug/L ND 20 20 24.9 26.3 124 131 15-152 5 30 IH,v3 Carbon disulfide ug/L ND 20 20 21.1 21.9 106 110 69-149 4 30 Carbon tetrachloride ug/L ND 20 20 20.7 21.2 104 106 70-143 2 30 Chlorobenzene ug/L ND 20 20 23.3 23.3 117 116 70-138 0 30 Chloroethane ug/L ND 20 20 20.3 22.0 102 110 52-163 8 30 Chloroform ug/L ND 20 20 21.2 22.3 106 112 70-139 5 30 Chloromethane ug/L ND 20 20 17.7 19.0 88 95 41-139 7 30 cis-1,2-Dichloroethene ug/L ND 20 20 21.4 22.5 107 112 70-141 5 30 cis-1,3-Dichloropropene ug/L ND 20 20 20.2 20.6 101 103 70-137 2 30 Dibromochloromethane ug/L ND 20 20 20.2 21.7 101 108 70-134 7 30 Dibromomethane ug/L ND 20 20 21.1 20.6 105 103 70-138 2 30 Dichlorodifluoromethane ug/L ND 20 20 15.7 16.7 78 83 47-155 6 30 Ethylbenzene ug/L ND 20 20 22.4 22.9 112 115 66-153 2 30 lodomethane ug/L ND 40 40 22.7 24.3 57 61 20-138 7 30 v3 m&p-Xylene ug/L ND 40 40 45.9 47.3 115 118 69-152 3 30 Methylene Chloride ug/L ND 20 20 24.5 24.5 122 123 42-159 0 30 o-Xylene ug/L ND 20 20 23.7 23.4 118 117 70-148 1 30 Styrene ug/L ND 20 20 23.2 22.9 116 114 70-135 1 30 Tetrachloroethene ug/L ND 20 20 21.7 21.6 109 108 59-143 1 30 Tetrahydrofuran ug/L ND 200 200 198 202 99 101 70-133 2 30 Toluene ug/L ND 20 20 20.3 21.3 101 106 59-148 5 30 trans-1,2-Dichloroethene ug/L ND 20 20 22.0 24.0 110 120 70-146 9 30 trans-1,3-Dichloropropene ug/L ND 20 20 19.4 19.7 97 98 70-135 1 30 trans-1,4-Dichloro-2-butene ug/L ND 20 20 20.5 19.2 103 96 47-135 7 30 IH Trichloroethene ug/L ND 20 20 21.7 21.5 109 107 70-147 1 30 Trichlorofluoromethane ug/L ND 20 20 18.0 18.5 90 93 70-148 3 30 Vinyl acetate ug/L ND 40 40 44.0 46.1 110 115 49-151 5 30 v1 Vinyl chloride ug/L ND 20 20 21.0 22.0 105 110 70-156 5 30 1,2-Dichloroethane-d4 (S) % 106 106 70-130 4-Bromofluorobenzene (S) % 96 99 70-130 Toluene-d8 (S) % 98 98 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 94 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 542119 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92477008001, 92477011005, 92477011006, 92477011007 METHOD BLANK: 2888719 Matrix: Water Associated Lab Samples: 92477008001, 92477011005, 92477011006, 92477011007 Blank Reporting Parameter Units Result Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.34 05/19/20 00:06 1,1,1-Trichloroethane ug/L ND 1.0 0.18 05/19/20 00:06 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 05/19/20 00:06 1,1,2-Trichloroethane ug/L ND 1.0 0.24 05/19/20 00:06 1,1-Dichloroethane ug/L ND 1.0 0.27 05/19/20 00:06 1,1-Dichloroethene ug/L ND 1.0 0.24 05/19/20 00:06 1,2,3-Trichloropropane ug/L ND 1.0 0.35 05/19/20 00:06 1,2-Dibromo-3-chloropropane ug/L ND 5.0 0.26 05/19/20 00:06 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.26 05/19/20 00:06 1,2-Dichlorobenzene ug/L ND 1.0 0.29 05/19/20 00:06 1,2-Dichloroethane ug/L ND 1.0 0.34 05/19/20 00:06 1,2-Dichloropropane ug/L ND 1.0 0.19 05/19/20 00:06 1,4-Dichlorobenzene ug/L ND 1.0 0.26 05/19/20 00:06 2-Butanone (MEK) ug/L ND 5.0 3.3 05/19/20 00:06 2-Hexanone ug/L ND 5.0 0.57 05/19/20 00:06 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 4.5 05/19/20 00:06 Acetone ug/L ND 25.0 6.2 05/19/20 00:06 Acrylonitrile ug/L ND 10.0 0.90 05/19/20 00:06 Benzene ug/L ND 1.0 0.15 05/19/20 00:06 Bromochloromethane ug/L ND 1.0 0.34 05/19/20 00:06 Bromodichloromethane ug/L ND 1.0 0.26 05/19/20 00:06 Bromoform ug/L ND 1.0 0.62 05/19/20 00:06 Bromomethane ug/L ND 2.0 0.62 05/19/20 00:06 Carbon disulfide ug/L ND 2.0 0.40 05/19/20 00:06 Carbon tetrachloride ug/L ND 1.0 0.22 05/19/20 00:06 Chlorobenzene ug/L ND 1.0 0.23 05/19/20 00:06 Chloroethane ug/L ND 1.0 0.49 05/19/20 00:06 Chloroform ug/L ND 5.0 2.3 05/19/20 00:06 Chloromethane ug/L ND 1.0 0.39 05/19/20 00:06 cis-1,2-Dichloroethene ug/L ND 1.0 0.29 05/19/20 00:06 cis-1,3-Dichloropropene ug/L ND 1.0 0.30 05/19/20 00:06 Dibromochloromethane ug/L ND 1.0 0.41 05/19/20 00:06 Dibromomethane ug/L ND 1.0 0.46 05/19/20 00:06 Dichlorodifluoromethane ug/L ND 1.0 0.23 05/19/20 00:06 Ethylbenzene ug/L ND 1.0 0.26 05/19/20 00:06 lodomethane ug/L ND 20.0 12.5 05/19/20 00:06 m&p-Xylene ug/L ND 2.0 0.41 05/19/20 00:06 Methylene Chloride ug/L ND 5.0 3.7 05/19/20 00:06 o-Xylene ug/L ND 1.0 0.22 05/19/20 00:06 Styrene ug/L ND 1.0 0.27 05/19/20 00:06 Qualifiers v1 I K,v2 IK IK IK v2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 95 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 METHOD BLANK: 2888719 Matrix: Water Associated Lab Samples: 92477008001, 92477011005, 92477011006, 92477011007 Blank Reporting Parameter Units Result Limit MDL Analyzed Tetrachloroethene ug/L ND 1.0 0.16 05/19/20 00:06 Tetrahydrofuran ug/L ND 10.0 1.9 05/19/20 00:06 Toluene ug/L ND 1.0 0.24 05/19/20 00:06 trans-1,2-Dichloroethene ug/L ND 1.0 0.25 05/19/20 00:06 trans- 1,3-Dichloropropene ug/L ND 1.0 0.31 05/19/20 00:06 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.54 05/19/20 00:06 Trichloroethene ug/L ND 1.0 0.22 05/19/20 00:06 Trichlorofluoromethane ug/L ND 1.0 0.31 05/19/20 00:06 Vinyl acetate ug/L ND 2.0 1.4 05/19/20 00:06 Vinyl chloride ug/L ND 1.0 0.24 05/19/20 00:06 1,2-Dichloroethane-d4 (S) % 99 70-130 05/19/20 00:06 4-Bromofluorobenzene (S) % 98 70-130 05/19/20 00:06 Toluene-d8 (S) % 101 70-130 05/19/20 00:06 LABORATORY CONTROL SAMPLE: 2888720 Parameter Qualifiers IH IK v1 IK Spike LCS LCS % Rec Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 55.6 111 70-130 1,1,1-Trichloroethane ug/L 50 53.1 106 70-130 1,1,2,2-Tetrachloroethane ug/L 50 53.0 106 70-130 1,1,2-Trichloroethane ug/L 50 53.6 107 70-130 1,1-Dichloroethane ug/L 50 51.4 103 70-130 1,1-Dichloroethene ug/L 50 53.5 107 70-130 1,2,3-Trichloropropane ug/L 50 55.8 112 70-130 1,2-Dibromo-3-chloropropane ug/L 50 59.6 119 70-130 1,2-Dibromoethane (EDB) ug/L 50 55.9 112 70-130 1,2-Dichlorobenzene ug/L 50 54.0 108 70-130 1,2-Dichloroethane ug/L 50 52.0 104 70-130 1,2-Dichloropropane ug/L 50 53.5 107 70-130 1,4-Dichlorobenzene ug/L 50 53.7 107 70-130 2-Butanone (MEK) ug/L 100 117 117 64-135 2-Hexanone ug/L 100 116 116 66-135 4-Methyl-2-pentanone (MIBK) ug/L 100 118 118 70-130 v1 Acetone ug/L 100 118 118 61-157 Acrylonitrile ug/L 250 259 104 61-143 Benzene ug/L 50 52.3 105 70-130 Bromochloromethane ug/L 50 51.0 102 70-130 Bromodichloromethane ug/L 50 55.7 111 70-130 Bromoform ug/L 50 56.4 113 70-130 Bromomethane ug/L 50 43.8 88 38-130IK,v3 Carbon disulfide ug/L 50 51.5 103 68-130 Carbon tetrachloride ug/L 50 55.3 111 70-130 Chlorobenzene ug/L 50 53.0 106 70-130 Chloroethane ug/L 50 38.9 78 37-142 IK Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 96 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 LABORATORY CONTROL SAMPLE: Parameter 2888720 Units Spike Conc. LCS LCS Result % Rec Chloroform ug/L 50 51.5 Chloromethane ug/L 50 47.3 cis-1,2-Dichloroethene ug/L 50 51.9 cis-1,3-Dichloropropene ug/L 50 54.7 Dibromochloromethane ug/L 50 57.5 Dibromomethane ug/L 50 50.8 Dichlorodifluoromethane ug/L 50 51.0 Ethylbenzene ug/L 50 51.2 lodomethane ug/L 100 81.6 m&p-Xylene ug/L 100 104 Methylene Chloride ug/L 50 48.9 o-Xylene ug/L 50 52.6 Styrene ug/L 50 55.3 Tetrachloroethene ug/L 50 53.5 Tetrahydrofuran ug/L 500 527 Toluene ug/L 50 50.0 trans-1,2-Dichloroethene ug/L 50 52.5 trans- 1,3-Dichloropropene ug/L 50 56.7 trans-1,4-Dichloro-2-butene ug/L 50 86.8 Trichloroethene ug/L 50 51.0 Trichlorofluoromethane ug/L 50 52.1 Vinyl acetate ug/L 100 120 Vinyl chloride ug/L 50 56.1 1,2-Dichloroethane-d4 (S) % 4-Bromofluorobenzene (S) % Toluene-d8 (S) % % Rec Limits Qualifiers 103 70-130 95 48-1301K 104 70-130 109 70-130 115 70-130 102 70-130 102 53-1341K 102 70-130 82 40-130 v3 104 70-130 98 67-132 105 70-131 111 70-130 107 69-130 105 62-130 100 70-130 105 70-130 113 70-130 174 35-1891H 102 70-130 104 63-1301K 120 55-143 v1 112 70-131 IK 107 70-130 99 70-130 102 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2888721 MS 92476718004 Spike Parameter Units Result Conc. MSD Spike Conc. 2888722 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 22.1 20.3 110 102 73-134 8 30 1,1,1-Trichloroethane ug/L ND 20 20 20.6 20.4 103 102 82-143 1 30 1,1,2,2-Tetrachloroethane ug/L ND 20 20 21.4 21.3 107 107 70-136 0 30 1,1,2-Trichloroethane ug/L ND 20 20 19.1 19.9 96 99 70-135 4 30 1,1-Dichloroethane ug/L ND 20 20 21.2 21.6 106 108 70-139 2 30 1,1-Dichloroethene ug/L ND 20 20 23.4 23.6 117 118 70-154 1 30 1,2,3-Trichloropropane ug/L ND 20 20 22.1 21.3 110 107 71-137 4 30 1,2-Dibromo-3- ug/L ND 20 20 19.5 19.7 97 98 65-134 1 30 chloropropane 1,2-Dibromoethane (EDB) ug/L ND 20 20 22.3 22.1 112 110 70-137 1 30 1,2-Dichlorobenzene ug/L ND 20 20 24.5 25.6 123 128 70-133 4 30 1,2-Dichloroethane ug/L ND 20 20 21.1 21.2 106 106 70-137 0 30 1,2-Dichloropropane ug/L ND 20 20 21.5 22.1 108 111 70-140 3 30 1,4-Dichlorobenzene ug/L ND 20 20 24.5 24.2 123 121 70-133 1 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 97 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2888721 2888722 MS MSD 92476718004 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 2-Butanone (MEK) ug/L ND 40 40 40.3 38.4 101 96 60-139 5 30 2-Hexanone ug/L ND 40 40 45.2 43.1 113 108 65-138 5 30 4-Methyl-2-pentanone ug/L ND 40 40 41.1 40.2 103 100 65-135 2 30 (MIBK) Acetone ug/L ND 40 40 40.7 41.0 102 103 60-148 1 30 Acrylonitrile ug/L ND 100 100 105 101 105 101 64-147 4 30 Benzene ug/L ND 20 20 22.0 22.2 110 111 70-151 1 30 Bromochloromethane ug/L ND 20 20 19.4 20.0 97 100 70-141 3 30 Bromodichloromethane ug/L ND 20 20 19.7 19.2 99 96 70-138 2 30 Bromoform ug/L ND 20 20 19.2 17.9 96 90 63-130 7 30 Bromomethane ug/L ND 20 20 22.7 24.6 114 123 15-152 8 30 IH,v3 Carbon disulfide ug/L ND 20 20 21.1 21.3 106 106 69-149 1 30 Carbon tetrachloride ug/L ND 20 20 21.2 21.5 106 108 70-143 2 30 Chlorobenzene ug/L ND 20 20 23.0 23.1 115 116 70-138 1 30 Chloroethane ug/L ND 20 20 22.9 21.3 114 106 52-163 7 30 Chloroform ug/L ND 20 20 21.3 21.0 106 105 70-139 1 30 Chloromethane ug/L ND 20 20 17.8 18.0 89 90 41-139 1 30 cis-1,2-Dichloroethene ug/L ND 20 20 21.6 21.4 108 107 70-141 1 30 cis-1,3-Dichloropropene ug/L ND 20 20 20.2 19.4 101 97 70-137 4 30 Dibromochloromethane ug/L ND 20 20 21.3 19.8 106 99 70-134 7 30 Dibromomethane ug/L ND 20 20 21.4 19.8 107 99 70-138 8 30 Dichlorodifluoromethane ug/L ND 20 20 15.8 15.8 79 79 47-155 0 30 Ethylbenzene ug/L ND 20 20 23.6 22.7 118 114 66-153 4 30 lodomethane ug/L ND 40 40 23.2 22.3 58 56 20-138 4 30 v3 m&p-Xylene ug/L ND 40 40 48.0 45.4 120 114 69-152 6 30 Methylene Chloride ug/L ND 20 20 23.3 23.4 117 117 42-159 0 30 o-Xylene ug/L ND 20 20 24.5 22.7 123 114 70-148 8 30 Styrene ug/L ND 20 20 24.1 23.7 121 119 70-135 2 30 Tetrachloroethene ug/L ND 20 20 23.6 22.4 118 112 59-143 5 30 Tetrahydrofuran ug/L ND 200 200 201 196 101 98 70-133 3 30 Toluene ug/L ND 20 20 20.5 20.2 102 101 59-148 1 30 trans-1,2-Dichloroethene ug/L ND 20 20 22.8 22.0 114 110 70-146 3 30 trans-1,3-Dichloropropene ug/L ND 20 20 19.2 19.7 96 99 70-135 2 30 trans-1,4-Dichloro-2-butene ug/L ND 20 20 21.5 21.3 108 107 47-135 1 30 IH Trichloroethene ug/L ND 20 20 21.9 21.7 109 108 70-147 1 30 Trichlorofluoromethane ug/L ND 20 20 18.4 18.7 92 94 70-148 2 30 Vinyl acetate ug/L ND 40 40 45.4 44.6 113 112 49-151 2 30 v1 Vinyl chloride ug/L ND 20 20 21.0 21.3 105 107 70-156 2 30 1,2-Dichloroethane-d4 (S) % 101 103 70-130 4-Bromofluorobenzene (S) % 99 99 70-130 Toluene-d8 (S) % 97 98 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 98 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 542188 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92477008003, 92477008004, 92477008005, 92477008006, 92477011008, 92477011009, 92477011010, 92477011011,92477013002,92477016002 METHOD BLANK: 2889063 Matrix: Water Associated Lab Samples: 92477008003, 92477008004, 92477008005, 92477008006, 92477011008, 92477011009, 92477011010, 92477011011, 92477013002, 92477016002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 0.34 05/19/20 02:17 1,1,1-Trichloroethane ug/L ND 1.0 0.18 05/19/20 02:17 1,1,2,2-Tetrachloroethane ug/L ND 1.0 0.22 05/19/20 02:17 1,1,2-Trichloroethane ug/L ND 1.0 0.24 05/19/20 02:17 1,1-Dichloroethane ug/L ND 1.0 0.27 05/19/20 02:17 1,1-Dichloroethene ug/L ND 1.0 0.24 05/19/20 02:17 1,2,3-Trichloropropane ug/L ND 1.0 0.35 05/19/20 02:17 1,2-Dibromo-3-chloropropane ug/L ND 5.0 0.26 05/19/20 02:17 1,2-Dibromoethane (EDB) ug/L ND 1.0 0.26 05/19/20 02:17 1,2-Dichlorobenzene ug/L ND 1.0 0.29 05/19/20 02:17 1,2-Dichloroethane ug/L ND 1.0 0.34 05/19/20 02:17 1,2-Dichloropropane ug/L ND 1.0 0.19 05/19/20 02:17 1,4-Dichlorobenzene ug/L ND 1.0 0.26 05/19/20 02:17 2-Butanone (MEK) ug/L ND 5.0 3.3 05/19/20 02:17 2-Hexanone ug/L ND 5.0 0.57 05/19/20 02:17 4-Methyl-2-pentanone (MIBK) ug/L ND 5.0 4.5 05/19/20 02:17 Acetone ug/L ND 25.0 6.2 05/19/20 02:17 Acrylonitrile ug/L ND 10.0 0.90 05/19/20 02:17 Benzene ug/L ND 1.0 0.15 05/19/20 02:17 Bromochloromethane ug/L ND 1.0 0.34 05/19/20 02:17 Bromodichloromethane ug/L ND 1.0 0.26 05/19/20 02:17 Bromoform ug/L ND 1.0 0.62 05/19/20 02:17 Bromomethane ug/L ND 2.0 0.62 05/19/20 02:17 Carbon disulfide ug/L ND 2.0 0.40 05/19/20 02:17 Carbon tetrachloride ug/L ND 1.0 0.22 05/19/20 02:17 Chlorobenzene ug/L ND 1.0 0.23 05/19/20 02:17 Chloroethane ug/L ND 1.0 0.49 05/19/20 02:17 Chloroform ug/L ND 5.0 2.3 05/19/20 02:17 Chloromethane ug/L ND 1.0 0.39 05/19/20 02:17 cis-1,2-Dichloroethene ug/L ND 1.0 0.29 05/19/20 02:17 cis-1,3-Dichloropropene ug/L ND 1.0 0.30 05/19/20 02:17 Dibromochloromethane ug/L ND 1.0 0.41 05/19/20 02:17 Dibromomethane ug/L ND 1.0 0.46 05/19/20 02:17 Dichlorodifluoromethane ug/L ND 1.0 0.23 05/19/20 02:17 Ethylbenzene ug/L ND 1.0 0.26 05/19/20 02:17 lodomethane ug/L ND 20.0 12.5 05/19/20 02:17 m&p-Xylene ug/L ND 2.0 0.41 05/19/20 02:17 Methylene Chloride ug/L ND 5.0 3.7 05/19/20 02:17 o-Xylene ug/L ND 1.0 0.22 05/19/20 02:17 IH,IK Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 99 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 METHOD BLANK: 2889063 Matrix: Water Associated Lab Samples: 92477008003, 92477008004, 92477008005, 92477008006, 92477011008, 92477011009, 92477011010, 92477011011,92477013002,92477016002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Styrene ug/L ND 1.0 0.27 05/19/20 02:17 Tetrachloroethene ug/L ND 1.0 0.16 05/19/20 02:17 Tetrahydrofuran ug/L ND 10.0 1.9 05/19/20 02:17 Toluene ug/L ND 1.0 0.24 05/19/20 02:17 trans-1,2-Dichloroethene ug/L ND 1.0 0.25 05/19/20 02:17 trans- 1,3-Dichloropropene ug/L ND 1.0 0.31 05/19/20 02:17 trans-1,4-Dichloro-2-butene ug/L ND 1.0 0.54 05/19/20 02:17 Trichloroethene ug/L ND 1.0 0.22 05/19/20 02:17 Trichlorofluoromethane ug/L ND 1.0 0.31 05/19/20 02:17 Vinyl acetate ug/L ND 2.0 1.4 05/19/20 02:17 Vinyl chloride ug/L ND 1.0 0.24 05/19/20 02:17 1,2-Dichloroethane-d4 (S) % 97 70-130 05/19/20 02:17 4-Bromofluorobenzene (S) % 99 70-130 05/19/20 02:17 Toluene-d8 (S) % 98 70-130 05/19/20 02:17 LABORATORY CONTROL SAMPLE: 2889064 Parameter v1 129 Spike LCS LCS % Rec Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 51.1 102 70-130 1,1,1-Trichloroethane ug/L 50 53.4 107 70-130 1,1,2,2-Tetrachloroethane ug/L 50 54.3 109 70-130 1,1,2-Trichloroethane ug/L 50 53.6 107 70-130 1,1-Dichloroethane ug/L 50 54.8 110 70-130 1,1-Dichloroethene ug/L 50 56.9 114 70-130 1,2,3-Trichloropropane ug/L 50 52.2 104 70-130 1,2-Dibromo-3-chloropropane ug/L 50 61.9 124 70-130 1,2-Dibromoethane (EDB) ug/L 50 54.5 109 70-130 1,2-Dichlorobenzene ug/L 50 52.6 105 70-130 1,2-Dichloroethane ug/L 50 51.2 102 70-130 1,2-Dichloropropane ug/L 50 52.6 105 70-130 1,4-Dichlorobenzene ug/L 50 53.5 107 70-130 2-Butanone (MEK) ug/L 100 107 107 64-135 2-Hexanone ug/L 100 103 103 66-135 4-Methyl-2-pentanone (MIBK) ug/L 100 103 103 70-130 Acetone ug/L 100 119 119 61-157 Acrylonitrile ug/L 250 258 103 61-143 Benzene ug/L 50 53.6 107 70-130 Bromochloromethane ug/L 50 59.4 119 70-130 Bromodichloromethane ug/L 50 54.5 109 70-130 Bromoform ug/L 50 55.5 111 70-130 Bromomethane ug/L 50 68.7 137 38-1301H,IK,L1 Carbon disulfide ug/L 50 60.7 121 68-130 Carbon tetrachloride ug/L 50 53.9 108 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 100 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 LABORATORY CONTROL SAMPLE: 2889064 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chlorobenzene ug/L 50 53.1 106 70-130 Chloroethane ug/L 50 49.1 98 37-142 Chloroform ug/L 50 55.1 110 70-130 Chloromethane ug/L 50 47.7 95 48-130 cis-1,2-Dichloroethene ug/L 50 54.8 110 70-130 cis-1,3-Dichloropropene ug/L 50 57.2 114 70-130 Dibromochloromethane ug/L 50 53.7 107 70-130 Dibromomethane ug/L 50 54.1 108 70-130 Dichlorodifluoromethane ug/L 50 55.9 112 53-134 Ethylbenzene ug/L 50 50.6 101 70-130 lodomethane ug/L 100 129 129 40-130 m&p-Xylene ug/L 100 101 101 70-130 Methylene Chloride ug/L 50 54.1 108 67-132 o-Xylene ug/L 50 51.9 104 70-131 Styrene ug/L 50 54.4 109 70-130 Tetrachloroethene ug/L 50 49.7 99 69-130 Tetrahydrofuran ug/L 500 524 105 62-130 Toluene ug/L 50 50.5 101 70-130 trans-1,2-Dichloroethene ug/L 50 56.1 112 70-130 trans- 1,3-Dichloropropene ug/L 50 60.3 121 70-130 trans-1,4-Dichloro-2-butene ug/L 50 116 231 35-189 L1,v1 Trichloroethene ug/L 50 50.9 102 70-130 Trichlorofluoromethane ug/L 50 51.3 103 63-130 Vinyl acetate ug/L 100 110 110 55-143 IK Vinyl chloride ug/L 50 60.9 122 70-131 1,2-Dichloroethane-d4 (S) % 98 70-130 4-Bromofluorobenzene (S) % 99 70-130 Toluene-d8 (S) % 102 70-130 MATRIX SPIKE SAMPLE: 2889066 92477052002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 22.1 110 73-134 1,1,1-Trichloroethane ug/L ND 20 22.9 114 82-143 1,1,2,2-Tetrachloroethane ug/L ND 20 23.5 118 70-136 1,1,2-Trichloroethane ug/L ND 20 22.6 113 70-135 1,1-Dichloroethane ug/L ND 20 25.1 126 70-139 1,1-Dichloroethene ug/L ND 20 26.1 130 70-154 1,2,3-Trichloropropane ug/L ND 20 22.8 114 71-137 1,2-Dibromo-3-chloropropane ug/L ND 20 20.2 101 65-134 1,2-Dibromoethane (EDB) ug/L ND 20 24.4 122 70-137 1,2-Dichlorobenzene ug/L ND 20 26.7 134 70-133 M1 1,2-Dichloroethane ug/L ND 20 24.2 121 70-137 1,2-Dichloropropane ug/L ND 20 25.2 126 70-140 1,4-Dichlorobenzene ug/L ND 20 25.5 128 70-133 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 101 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 MATRIX SPIKE SAMPLE: Parameter 2889066 Units 92477052002 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 2-Butanone (MEK) ug/L ND 40 42.8 107 60-139 2-Hexanone ug/L ND 40 47.1 118 65-138 4-Methyl-2-pentanone (MIBK) ug/L ND 40 43.5 109 65-135 Acetone ug/L ND 40 44.4 111 60-148 Acrylonitrile ug/L ND 100 110 110 64-147 Benzene ug/L ND 20 25.2 126 70-151 Bromochloromethane ug/L ND 20 22.1 110 70-141 Bromodichloromethane ug/L ND 20 21.5 108 70-138 Bromoform ug/L ND 20 19.4 97 63-130 Bromomethane ug/L ND 20 26.3 131 15-152 IH Carbon disulfide ug/L ND 20 23.9 119 69-149 Carbon tetrachloride ug/L ND 20 22.6 113 70-143 Chlorobenzene ug/L ND 20 25.2 126 70-138 Chloroethane ug/L ND 20 23.4 117 52-163 Chloroform ug/L ND 20 23.4 117 70-139 Chloromethane ug/L ND 20 21.0 105 41-139 cis-1,2-Dichloroethene ug/L ND 20 25.0 125 70-141 cis-1,3-Dichloropropene ug/L ND 20 22.4 112 70-137 Dibromochloromethane ug/L ND 20 21.2 106 70-134 Dibromomethane ug/L ND 20 24.4 122 70-138 Dichlorodifluoromethane ug/L ND 20 19.3 97 47-155 Ethylbenzene ug/L ND 20 25.1 126 66-153 Iodomethane ug/L ND 40 23.0 58 20-138 v3 m&p-Xylene ug/L ND 40 50.0 125 69-152 Methylene Chloride ug/L ND 20 26.8 134 42-159 o-Xylene ug/L ND 20 25.4 127 70-148 Styrene ug/L ND 20 25.9 129 70-135 Tetrachloroethene ug/L ND 20 23.5 117 59-143 Tetrahydrofuran ug/L ND 200 219 110 70-133 Toluene ug/L ND 20 22.6 113 59-148 trans-1,2-Dichloroethene ug/L ND 20 25.2 126 70-146 trans- 1,3-Dichloropropene ug/L ND 20 21.1 105 70-135 trans-1,4-Dichloro-2-butene ug/L ND 20 22.0 110 47-135 v1 Trichloroethene ug/L ND 20 23.6 118 70-147 Trichlorofluoromethane ug/L ND 20 20.7 103 70-148 Vinyl acetate ug/L ND 40 49.6 124 49-151 Vinyl chloride ug/L ND 20 24.5 122 70-156 1,2-Dichloroethane-d4 (S) % 105 70-130 4-Bromofluorobenzene (S) % 97 70-130 Toluene-d8 (S) % 98 70-130 SAMPLE DUPLICATE: 2889065 92477052001 Dup Max Parameter Units Result Result RPD RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 102 of 155 Pace Analytical Services, LLC lac, Analyilcal ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 SAMPLE DUPLICATE: 2889065 Parameter Units 92477052001 Result Dup Result RPD Max RPD Qualifiers 1,1,1-Trichloroethane ug/L ND ND 30 1,1,2,2-Tetrachloroethane ug/L ND ND 30 1,1,2-Trichloroethane ug/L ND ND 30 1,1-Dichloroethane ug/L ND ND 30 1,1-Dichloroethene ug/L ND ND 30 1,2,3-Trichloropropane ug/L ND ND 30 1,2-Dibromo-3-chloropropane ug/L ND ND 30 1,2-Dibromoethane (EDB) ug/L ND ND 30 1,2-Dichlorobenzene ug/L ND ND 30 1,2-Dichloroethane ug/L ND ND 30 1,2-Dichloropropane ug/L ND ND 30 1,4-Dichlorobenzene ug/L ND ND 30 2-Butanone (MEK) ug/L ND ND 30 2-Hexanone ug/L ND ND 30 4-Methyl-2-pentanone (MIBK) ug/L ND ND 30 Acetone ug/L ND ND 30 Acrylonitrile ug/L ND ND 30 Benzene ug/L ND ND 30 Bromochloromethane ug/L ND ND 30 Bromodichloromethane ug/L ND ND 30 Bromoform ug/L ND ND 30 Bromomethane ug/L ND ND 301H Carbon disulfide ug/L ND ND 30 Carbon tetrachloride ug/L ND ND 30 Chlorobenzene ug/L ND ND 30 Chloroethane ug/L ND ND 30 Chloroform ug/L ND ND 30 Chloromethane ug/L ND ND 30 cis-1,2-Dichloroethene ug/L ND ND 30 cis-1,3-Dichloropropene ug/L ND ND 30 Dibromochloromethane ug/L ND ND 30 Dibromomethane ug/L ND ND 30 Dichlorodifluoromethane ug/L ND ND 30 Ethylbenzene ug/L ND ND 30 lodomethane ug/L ND ND 30 v2 m&p-Xylene ug/L ND ND 30 Methylene Chloride ug/L ND ND 30 o-Xylene ug/L ND ND 30 Styrene ug/L ND ND 30 Tetrachloroethene ug/L ND ND 30 Tetrahydrofuran ug/L ND ND 30 Toluene ug/L ND ND 30 trans-1,2-Dichloroethene ug/L ND ND 30 trans- 1,3-Dichloropropene ug/L ND ND 30 trans-1,4-Dichloro-2-butene ug/L ND ND 30 v1 Trichloroethene ug/L ND ND 30 Trichlorofluoromethane ug/L ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 103 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 SAMPLE DUPLICATE: 2889065 92477052001 Dup Max Parameter Units Result Result RPD RPD Vinyl acetate ug/L ND ND 30 Vinyl chloride ug/L ND ND 30 1,2-Dichloroethane-d4 (S) % 96 109 4-Bromofluorobenzene (S) % 100 100 Toluene-d8 (S) % 99 97 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 104 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541676 Analysis Method: EPA 8260D Mod. QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92477008001,92477008002,92477011001,92477011002,92477011003,92477011004,92477011005, 92477011006,92477013001,92477016001 METHOD BLANK: 2886576 Matrix: Water Associated Lab Samples: 92477008001,92477008002,92477011001,92477011002,92477011003,92477011004,92477011005, 92477011006,92477013001,92477016001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 1.2 05/14/20 20:02 1,2-Dichloroethane-d4 (S) % 103 50-150 05/14/20 20:02 Toluene-d8 (S) % 100 50-150 05/14/20 20:02 LABORATORY CONTROL SAMPLE: 2886577 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane(p-Dioxane) ug/L 20 18.6 93 70-130 1,2-Dichloroethane-d4 (S) % 103 50-150 Toluene-d8(S) % 102 50-150 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2886859 2886860 MS MSD 92477011005 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane (p-Dioxane) ug/L ND 20 20 18.4 19.5 89 95 50-150 6 30 1,2-Dichloroethane-d4 (S) % 98 113 50-150 30 Toluene-d8 (S) % 95 106 50-150 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 105 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541677 Analysis Method: EPA 8260D Mod. QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92477011007 METHOD BLANK: 2886578 Matrix: Water Associated Lab Samples: 92477011007 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 1.2 05/14/20 20:22 1,2-Dichloroethane-d4 (S) % 99 50-150 05/14/20 20:22 Toluene-d8 (S) % 89 50-150 05/14/20 20:22 LABORATORY CONTROL SAMPLE: 2886579 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane (p-Dioxane) ug/L 20 19.2 96 70-130 1,2-Dichloroethane-d4 (S) % 105 50-150 Toluene-d8 (S) % 100 50-150 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2886857 2886858 MS MSD 92477011007 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane (p-Dioxane) ug/L ND 20 20 18.9 19.7 93 97 50-150 4 30 1,2-Dichloroethane-d4 (S) % 96 107 50-150 30 Toluene-d8 (S) % 96 83 50-150 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 106 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541824 Analysis Method: EPA 8260D Mod. QC Batch Method: EPA 8260D Mod. Analysis Description: 8260D MSV SIM Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92477008003, 92477008004, 92477008005, 92477008006, 92477011008, 92477011009, 92477011010, 92477013002,92477016002 METHOD BLANK: 2887087 Matrix: Water Associated Lab Samples: 92477008003, 92477008004, 92477008005, 92477008006, 92477011008, 92477011009, 92477011010, 92477013002,92477016002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 1,4-Dioxane (p-Dioxane) ug/L ND 2.0 1.2 05/15/20 11:31 1,2-Dichloroethane-d4 (S) % 98 50-150 05/15/20 11:31 Toluene-d8 (S) % 111 50-150 05/15/20 11:31 LABORATORY CONTROL SAMPLE: 2887088 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dioxane(p-Dioxane) ug/L 20 19.3 97 70-130 1,2-Dichloroethane-d4 (S) % 98 50-150 Toluene-d8(S) % 96 50-150 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2887460 2887461 MS MSD 92476968001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 1,4-Dioxane (p-Dioxane) ug/L ND 20 20 19.1 19.1 92 92 50-150 0 30 1,2-Dichloroethane-d4 (S) % 103 97 50-150 30 Toluene-d8 (S) % 91 104 50-150 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 107 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 540972 Analysis Method: EPA 8081 B QC Batch Method: EPA 3510C Analysis Description: 8081 OC Pesticides Red Vol Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92477013001 METHOD BLANK: 2883115 Associated Lab Samples: 92477013001 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed 4,4'-DDD ug/L ND 0.050 0.0069 05/13/20 19:49 4,4'-DDT ug/L ND 0.050 0.018 05/13/20 19:49 Aldrin ug/L ND 0.050 0.022 05/13/20 19:49 alpha-BHC ug/L ND 0.050 0.019 05/13/20 19:49 delta-BHC ug/L ND 0.050 0.020 05/13/20 19:49 Endosulfan I ug/L ND 0.050 0.0094 05/13/20 19:49 Endosulfan 11 ug/L ND 0.050 0.0065 05/13/20 19:49 Endrin ug/L ND 0.050 0.0089 05/13/20 19:49 Endrin aldehyde ug/L ND 0.050 0.013 05/13/20 19:49 Heptachlor ug/L ND 0.050 0.016 05/13/20 19:49 Heptachlor epoxide ug/L ND 0.050 0.0097 05/13/20 19:49 Methoxychlor ug/L ND 0.15 0.033 05/13/20 19:49 Decachlorobiphenyl (S) % 76 10-130 05/13/20 19:49 Tetrachloro-m-xylene (S) % 81 10-130 05/13/20 19:49 LABORATORY CONTROL SAMPLE: 2883116 Parameter 4,4'-DDD 4,4'-DDT Aldrin alpha-BHC delta-BHC Endosulfan I Endosulfan II Endrin Endrin aldehyde Heptachlor Heptachlor epoxide Methoxychlor Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Qualifiers Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers ug/L 0.25 0.31 124 49-130 ug/L 0.25 0.29 116 45-130 ug/L 0.25 0.17 69 25-130 ug/L 0.25 0.26 103 53-130 ug/L 0.25 0.27 106 54-130 ug/L 0.25 0.29 114 43-130 ug/L 0.25 0.30 119 64-130 ug/L 0.25 0.33 132 56-130 L1 ug/L 0.25 0.26 106 59-130 ug/L 0.25 0.21 86 37-130 ug/L 0.25 0.26 105 56-130 ug/L 0.75 0.81 108 46-130 % 123 10-130 % 94 10-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 108 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883117 2883118 MS MSD 92476875005 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 4,4'-DDD ug/L ND 0.25 0.25 0.24 0.33 95 132 28-130 33 30 M1,R1 4,4'-DDT ug/L ND 0.25 0.25 0.22 0.32 90 126 11-130 34 30 R1 Aldrin ug/L ND 0.25 0.25 0.15 0.27 59 107 10-130 58 30 R1 alpha-BHC ug/L ND 0.25 0.25 0.21 0.29 86 117 27-130 31 30 R1 delta-BHC ug/L ND 0.25 0.25 0.22 0.31 88 125 44-130 35 30 R1 Endosulfan I ug/L ND 0.25 0.25 0.25 0.34 99 134 10-139 30 30 Endosulfan II ug/L ND 0.25 0.25 0.23 0.33 93 131 36-130 34 30 M1,R1 Endrin ug/L ND 0.25 0.25 0.23 0.32 93 128 26-130 32 30 R1 Endrin aldehyde ug/L ND 0.25 0.25 0.21 0.30 85 120 19-160 34 30 R1 Heptachlor ug/L ND 0.25 0.25 0.19 0.28 75 113 25-130 41 30 R1 Heptachlor epoxide ug/L ND 0.25 0.25 0.22 0.30 89 120 18-130 29 30 Methoxychlor ug/L ND 0.75 0.75 0.66 0.92 88 122 10-130 32 30 R1 Decachlorobiphenyl (S) % 84 119 10-130 Tetrachloro-m-xylene (S) % 82 109 10-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 109 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541169 Analysis Method: EPA 8081 B QC Batch Method: EPA 3510C Analysis Description: 8081 OC Pesticides Red Vol Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92477008001, 92477008002, 92477008003, 92477008004, 92477008005, 92477008006, 92477013002 METHOD BLANK: 2884095 Matrix: Water Associated Lab Samples: 92477008001, 92477008002, 92477008003, 92477008004, 92477008005, 92477008006, 92477013002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers 4,4'-DDD ug/L ND 0.050 0.0069 05/14/20 21:17 4,4'-DDT ug/L ND 0.050 0.018 05/14/20 21:17 Aldrin ug/L ND 0.050 0.022 05/14/20 21:17 alpha-BHC ug/L ND 0.050 0.019 05/14/20 21:17 delta-BHC ug/L ND 0.050 0.020 05/14/20 21:17 Endosulfan I ug/L ND 0.050 0.0094 05/14/20 21:17 Endosulfan 11 ug/L ND 0.050 0.0065 05/14/20 21:17 Endrin ug/L ND 0.050 0.0089 05/14/20 21:17 Endrin aldehyde ug/L ND 0.050 0.013 05/14/20 21:17 Heptachlor ug/L ND 0.050 0.016 05/14/20 21:17 Heptachlor epoxide ug/L ND 0.050 0.0097 05/14/20 21:17 Methoxychlor ug/L ND 0.15 0.033 05/14/20 21:17 Decachlorobiphenyl (S) % 79 10-130 05/14/20 21:17 Tetrachloro-m-xylene (S) % 90 10-130 05/14/20 21:17 LABORATORY CONTROL SAMPLE: Parameter 2884096 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 4,4'-DDD ug/L 0.25 0.27 108 49-130 4,4'-DDT ug/L 0.25 0.30 120 45-130 Aldrin ug/L 0.25 0.17 67 25-130 alpha-BHC ug/L 0.25 0.24 94 53-130 delta-BHC ug/L 0.25 0.24 94 54-130 Endosulfan I ug/L 0.25 0.22 88 43-130 Endosulfan II ug/L 0.25 0.26 105 64-130 Endrin ug/L 0.25 0.25 99 56-130 Endrin aldehyde ug/L 0.25 0.26 104 59-130 Heptachlor ug/L 0.25 0.18 71 37-130 Heptachlor epoxide ug/L 0.25 0.22 89 56-130 Methoxychlor ug/L 0.75 0.78 104 46-130 Decachlorobiphenyl (S) % 94 10-130 Tetrachloro-m-xylene (S) % 92 10-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 110 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2884097 2884098 MS MSD 92477008001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 4,4'-DDD ug/L ND 0.5 0.5 0.92 1.1 185 217 28-130 16 30 M1 4,4'-DDT ug/L ND 0.5 0.5 1.1 1.2 219 243 11-130 10 30 M1 Aldrin ug/L ND 0.5 0.5 0.50 0.70 100 139 10-130 33 30 M1,R1 alpha-BHC ug/L ND 0.5 0.5 0.61 0.74 121 148 27-130 20 30 M1 delta-BHC ug/L ND 0.5 0.5 0.60 0.80 121 160 44-130 28 30 M1 Endosulfan I ug/L ND 0.5 0.5 0.65 0.84 131 168 10-139 25 30 M1 Endosulfan II ug/L ND 0.5 0.5 0.79 0.96 159 192 36-130 19 30 M1 Endrin ug/L ND 0.5 0.5 0.95 1.2 190 231 26-130 20 30 M1 Endrin aldehyde ug/L ND 0.5 0.5 1.2 1.3 239 261 19-160 9 30 M1 Heptachlor ug/L ND 0.5 0.5 0.71 1.0 142 204 25-130 36 30 M1,R1 Heptachlor epoxide ug/L ND 0.5 0.5 0.61 0.85 121 170 18-130 34 30 M1,R1 Methoxychlor ug/L ND 1.5 1.5 2.1 2.7 139 182 10-130 26 30 M1 Decachlorobiphenyl (S) % 120 145 10-130 SO Tetrachloro-m-xylene (S) % 119 136 10-130 SO Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 111 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 540969 Analysis Method: EPA 8270E QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92477016001 METHOD BLANK: 2883103 Associated Lab Samples: 92477016001 Parameter Units Matrix: Blank Result Water Reporting Limit MDL Analyzed Qualifiers Benzo(a)anthracene ug/L ND 10.0 1.5 05/12/20 19:51 bis(2-Ethylhexyl)phthalate ug/L ND 6.0 2.0 05/12/20 19:51 v1 Chrysene ug/L ND 10.0 1.4 05/12/20 19:51 Dibenz(a,h)anthracene ug/L ND 10.0 1.6 05/12/20 19:51 v2 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 1.7 05/12/20 19:51 2,4,6-Tribromophenol (S) % 63 10-137 05/12/20 19:51 2-Fluorobiphenyl (S) % 44 13-130 05/12/20 19:51 2-Fluorophenol (S) % 44 10-130 05/12/20 19:51 Nitrobenzene-d5 (S) % 62 13-130 05/12/20 19:51 Phenol-d6 (S) % 35 10-130 05/12/20 19:51 Terphenyl-d14 (S) % 108 25-130 05/12/20 19:51 LABORATORY CONTROL SAMPLE: Parameter 2883104 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Benzo(a)anthracene ug/L 50 39.9 80 50-130 bis(2-Ethylhexyl)phthalate ug/L 50 51.8 104 50-130 v1 Chrysene ug/L 50 40.1 80 50-130 Dibenz(a,h)anthracene ug/L 50 31.3 63 40-130 v3 Indeno(1,2,3-cd)pyrene ug/L 50 32.1 64 40-130 2,4,6-Tribromophenol (S) % 73 10-137 2-Fluorobiphenyl (S) % 53 13-130 2-Fluorophenol(S) % 46 10-130 Nitrobenzene-d5 (S) % 65 13-130 Phenol-d6 (S) % 37 10-130 Terphenyl-d14 (S) % 104 25-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883105 2883106 MS MSD 92477016001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Benzo(a)anthracene ug/L ND 50 50 41.3 34.7 83 69 50-130 17 30 bis(2- Ethyl hexyl)phthalate ug/L ND 50 50 53.8 45.1 105 87 50-130 17 30 v1 Chrysene ug/L ND 50 50 41.5 34.6 83 69 50-130 18 30 Dibenz(a,h)anthracene ug/L 2.OJ 50 50 34.6 28.3 65 53 40-130 20 30 v2,v3 Indeno(1,2,3-cd)pyrene ug/L 2.2J 50 50 34.3 30.1 64 56 40-130 13 30 2,4,6-Tribromophenol (S) % 77 8 10-137 SO Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 112 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883105 2883106 MS MSD 92477016001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 2-Fluorobiphenyl (S) % 60 43 13-130 2-Fluorophenol (S) % 59 4 10-130 SO Nitrobenzene-d5(S) % 73 51 13-130 Phenol-d6 (S) % 55 15 10-130 Terphenyl-d14(S) % 97 85 25-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 113 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541145 Analysis Method: EPA 8270E QC Batch Method: EPA 3510C Analysis Description: 8270E Water MSSV RVE Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92477008001, 92477008002, 92477008003, 92477008004, 92477008005, 92477008006, 92477016002 METHOD BLANK: 2883971 Matrix: Water Associated Lab Samples: 92477008001, 92477008002, 92477008003, 92477008004, 92477008005, 92477008006, 92477016002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Benzo(a)anthracene ug/L ND 10.0 1.5 05/13/20 21:17 bis(2-Ethylhexyl)phthalate ug/L ND 6.0 2.0 05/13/20 21:17 Chrysene ug/L ND 10.0 1.4 05/13/20 21:17 Dibenz(a,h)anthracene ug/L ND 10.0 1.6 05/13/20 21:17 Indeno(1,2,3-cd)pyrene ug/L ND 10.0 1.7 05/13/20 21:17 2,4,6-Tribromophenol (S) % 69 10-137 05/13/20 21:17 2-Fluorobiphenyl (S) % 71 13-130 05/13/20 21:17 2-Fluorophenol (S) % 56 10-130 05/13/20 21:17 Nitrobenzene-d5 (S) % 83 13-130 05/13/20 21:17 Phenol-d6 (S) % 42 10-130 05/13/20 21:17 Terphenyl-d14 (S) % 100 25-130 05/13/20 21:17 LABORATORY CONTROL SAMPLE: 2883972 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Benzo(a)anthracene ug/L 50 38.4 77 50-130 bis(2-Ethylhexyl)phthalate ug/L 50 42.5 85 50-130 Chrysene ug/L 50 38.8 78 50-130 Dibenz(a,h)anthracene ug/L 50 38.7 77 40-130 Indeno(1,2,3-cd)pyrene ug/L 50 39.1 78 40-130 2,4,6-Tribromophenol (S) % 37 10-137 2-Fluorobiphenyl (S) % 38 13-130 2-Fluorophenol(S) % 31 10-130 Nitrobenzene-d5 (S) % 44 13-130 Phenol-d6 (S) % 25 10-130 Terphenyl-d14 (S) % 75 25-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883973 2883974 MS MSD 92471460014 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Benzo(a)anthracene ug/L ND 50 50 45.8 46.4 92 93 50-130 1 30 bis(2- Ethyl hexyl)phthalate ug/L ND 50 50 52.6 54.2 105 108 50-130 3 30 Chrysene ug/L ND 50 50 44.9 45.2 90 90 50-130 1 30 Dibenz(a,h)anthracene ug/L ND 50 50 53.4 50.0 107 100 40-130 7 30 Indeno(1,2,3-cd)pyrene ug/L ND 50 50 54.1 50.1 108 100 40-130 8 30 2,4,6-Tribromophenol (S) % 22 26 10-137 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 114 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883973 2883974 MS MSD 92471460014 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual 2-Fluorobiphenyl (S) % 84 80 13-130 2-Fluorophenol(S) % 10 12 10-130 Nitrobenzene-d5(S) % 89 85 13-130 Phenol-d6 (S) % 29 30 10-130 Terphenyl-d14(S) % 104 106 25-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 115 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541022 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477011001 METHOD BLANK: 2883326 Matrix: Water Associated Lab Samples: 92477011001 Blank Reporting Parameter Units Result Limit Alkalinity, Total as CaCO3 ug/L ND 5000 LABORATORY CONTROL SAMPLE: 2883327 Spike LCS Parameter Units Conc. Result Alkalinity, Total as CaCO3 ug/L 50000 51700 MDL Analyzed Qualifiers 5000 05/12/2016:31 LCS % Rec % Rec Limits Qualifiers 103 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883328 2883329 MS MSD 92476084019 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 300 mg/L 50000 50000 340000 335000 81 70 80-120 2 25 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883913 2883914 MS MSD 92476084018 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 262 mg/L 50000 50000 311000 307000 99 90 80-120 2 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 116 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541634 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477008001, 92477008002, 92477008005, 92477011002, 92477011003, 92477011004, 92477011005, 92477011006,92477011007,92477016001 METHOD BLANK: 2886255 Matrix: Water Associated Lab Samples: 92477008001, 92477008002, 92477008005, 92477011002, 92477011003, 92477011004, 92477011005, 92477011006,92477011007,92477016001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 5000 05/15/20 20:10 LABORATORY CONTROL SAMPLE: 2886256 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 53000 106 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2886257 2886258 MS MSD 92476889005 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 29.3 mg/L 50000 50000 78600 78400 99 98 80-120 0 25 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2886259 2886260 MS MSD 92477011007 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 66400 50000 50000 117000 118000 101 103 80-120 1 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 117 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541813 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477008006, 92477011008, 92477011009, 92477011010, 92477013002, 92477016002 METHOD BLANK: 2886980 Matrix: Water Associated Lab Samples: 92477008006, 92477011008, 92477011009, 92477011010, 92477013002, 92477016002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 5000 05/16/20 01:08 LABORATORY CONTROL SAMPLE: 2886981 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 53000 106 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2886982 2886983 MS MSD 92477634001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 92.9 mg/L 50000 50000 143000 146000 100 106 80-120 2 25 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2886984 2886985 MS MSD 92477013002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 71600 50000 50000 121000 121000 99 99 80-120 0 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 118 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 542078 Analysis Method: SM 2320B-2011 QC Batch Method: SM 2320B-2011 Analysis Description: 2320E Alkalinity Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477008003, 92477008004, 92477013001 METHOD BLANK: 2888437 Matrix: Water Associated Lab Samples: 92477008003, 92477008004, 92477013001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Alkalinity, Total as CaCO3 ug/L ND 5000 5000 05/18/20 14:54 LABORATORY CONTROL SAMPLE: 2888438 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Alkalinity, Total as CaCO3 ug/L 50000 52400 105 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2888439 2888440 MS MSD 92477591001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 57.2 mg/L 50000 50000 108000 109000 102 104 80-120 1 25 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2888441 2888442 MS MSD 92477599002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Alkalinity, Total as CaCO3 ug/L 85.9 mg/L 50000 50000 137000 138000 102 104 80-120 1 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 119 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 540941 Analysis Method: SM 2540C-2011 QC Batch Method: SM 2540C-2011 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477011001 METHOD BLANK: 2883037 Matrix: Water Associated Lab Samples: 92477011001 Blank Reporting Parameter Units Result Limit Total Dissolved Solids ug/L ND 25000 LABORATORY CONTROL SAMPLE: 2883038 Spike LCS Parameter Units Conc. Result Total Dissolved Solids ug/L 250000 268000 SAMPLE DUPLICATE: 2883039 92477011001 Dup Parameter Units Result Result Total Dissolved Solids ug/L 93000 96000 MDL Analyzed Qualifiers 25000 05/11 /20 23:02 LCS % Rec % Rec Limits Qualifiers 107 90-110 Max RPD RPD Qualifiers 3 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 120 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541102 Analysis Method: SM 2540C-2011 QC Batch Method: SM 2540C-2011 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477011002, 92477011003, 92477011004, 92477013001, 92477016001 METHOD BLANK: 2883710 Matrix: Water Associated Lab Samples: 92477011002, 92477011003, 92477011004, 92477013001, 92477016001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Dissolved Solids ug/L ND 25000 25000 05/12/20 16:31 LABORATORY CONTROL SAMPLE: 2883711 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids ug/L 250000 250000 100 90-110 SAMPLE DUPLICATE: 2883712 92477011002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Dissolved Solids ug/L 130000 147000 12 25 SAMPLE DUPLICATE: 2883713 92476546010 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Dissolved Solids ug/L ND ND 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 121 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541184 Analysis Method: SM 2540C-2011 QC Batch Method: SM 2540C-2011 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477008001, 92477008002, 92477008003, 92477011005, 92477011006, 92477011007, 92477011008, 92477013002,92477016002 METHOD BLANK: 2884140 Matrix: Water Associated Lab Samples: 92477008001, 92477008002, 92477008003, 92477011005, 92477011006, 92477011007, 92477011008, 92477013002,92477016002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Dissolved Solids ug/L ND 25000 25000 05/12/20 23:18 LABORATORY CONTROL SAMPLE: 2884141 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids ug/L 250000 256000 102 90-110 SAMPLE DUPLICATE: 2884142 92477008001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Dissolved Solids ug/L 172000 167000 3 25 SAMPLE DUPLICATE: 2884143 92476968001 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Dissolved Solids ug/L ND ND 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 122 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541198 Analysis Method: SM 2540C-2011 QC Batch Method: SM 2540C-2011 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477008004, 92477008005, 92477008006, 92477011009, 92477011010 METHOD BLANK: 2884198 Matrix: Water Associated Lab Samples: 92477008004, 92477008005, 92477008006, 92477011009, 92477011010 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Total Dissolved Solids ug/L ND 25000 25000 05/12/20 23:41 LABORATORY CONTROL SAMPLE: 2884199 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Dissolved Solids ug/L 250000 252000 101 90-110 SAMPLE DUPLICATE: 2884200 92476969006 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Dissolved Solids ug/L 98000 93000 5 25 SAMPLE DUPLICATE: 2884201 92477008004 Dup Max Parameter Units Result Result RPD RPD Qualifiers Total Dissolved Solids ug/L 840000 840000 0 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 123 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 540866 Analysis Method: SM 4500-S2D-2011 QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477011001 METHOD BLANK: 2882755 Matrix: Water Associated Lab Samples: 92477011001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfide ug/L ND 100 50.0 05/11/20 23:12 LABORATORY CONTROL SAMPLE: 2882756 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 522 104 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2882759 2882760 MS MSD 92476669002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 486 491 97 98 80-120 1 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883033 2883034 MS MSD 92476714001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 486 445 97 89 80-120 9 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 124 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541111 Analysis Method: SM 4500-S2D-2011 QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477008001,92477008002,92477011002,92477011003,92477011004,92477011005,92477011006, 92477011007,92477013001,92477016001 METHOD BLANK: 2883751 Matrix: Water Associated Lab Samples: 92477008001,92477008002,92477011002,92477011003,92477011004,92477011005,92477011006, 92477011007,92477013001,92477016001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfide ug/L ND 100 50.0 05/12/20 20:02 LABORATORY CONTROL SAMPLE: 2883752 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 483 97 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883753 2883754 MS MSD 92477011002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 457 496 89 97 80-120 8 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883755 2883756 MS MSD 92477011003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 464 462 92 91 80-120 0 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 125 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541114 Analysis Method: SM 4500-S2D-2011 QC Batch Method: SM 4500-S2D-2011 Analysis Description: 4500S2D Sulfide Water Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477008003, 92477008004, 92477008005, 92477008006, 92477011008, 92477011009, 92477011010, 92477013002,92477016002 METHOD BLANK: 2883784 Matrix: Water Associated Lab Samples: 92477008003, 92477008004, 92477008005, 92477008006, 92477011008, 92477011009, 92477011010, 92477013002,92477016002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfide ug/L ND 100 50.0 05/12/20 20:40 LABORATORY CONTROL SAMPLE: 2883785 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfide ug/L 500 471 94 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883788 2883789 MS MSD 92476928038 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 352 351 70 70 80-120 0 10 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883798 2883799 MS MSD 92477008003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfide ug/L ND 500 500 242 259 48 51 80-120 7 10 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 126 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541452 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477008001, 92477008002, 92477008003, 92477008004, 92477008005, 92477008006, 92477011001 METHOD BLANK: 2885433 Matrix: Water Associated Lab Samples: 92477008001, 92477008002, 92477008003, 92477008004, 92477008005, 92477008006, 92477011001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfate ug/L ND 1000 500 05/14/20 04:12 LABORATORY CONTROL SAMPLE: 2885434 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate ug/L 50000 52200 104 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2885435 2885436 MS MSD 2631766002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L ND 50000 50000 53700 52000 107 104 90-110 3 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2885437 2885438 MS MSD 92476969001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 2520 50000 50000 62800 57600 121 110 90-110 9 10 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 127 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541453 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477011002,92477011003,92477011004,92477011005,92477011006,92477011007,92477011008, 92477011009,92477011010,92477013001,92477013002,92477016001,92477016002 METHOD BLANK: 2885439 Matrix: Water Associated Lab Samples: 92477011002,92477011003,92477011004,92477011005,92477011006,92477011007,92477011008, 92477011009,92477011010,92477013001,92477013002,92477016001,92477016002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Sulfate ug/L ND 1000 500 05/14/20 03:58 LABORATORY CONTROL SAMPLE: 2885440 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Sulfate ug/L 50000 51500 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2885441 2885442 MS MSD 92477011002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L ND 50000 50000 54800 52700 109 105 90-110 4 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2885443 2885444 MS MSD 92477013002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Sulfate ug/L 10400 50000 50000 63400 63100 106 105 90-110 0 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 128 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541126 Analysis Method: SM 4500-CI-E-2011 QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477011001 METHOD BLANK: 2883853 Matrix: Water Associated Lab Samples: 92477011001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Chloride ug/L ND 1000 500 05/12/2018:55 LABORATORY CONTROL SAMPLE: 2883854 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride ug/L 20000 20300 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883855 2883856 MS MSD 92476997002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 14.9 mg/L 10000 10000 25200 24500 103 96 90-110 3 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883857 2883858 MS MSD 92476997003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 2.5 mg/L 10000 10000 12500 12800 100 103 90-110 2 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 129 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541127 Analysis Method: SM 4500-CI-E-2011 QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477008001, 92477008002, 92477008003, 92477008004, 92477008005, 92477008006, 92477011002, 92477011003 METHOD BLANK: 2883859 Matrix: Water Associated Lab Samples: 92477008001, 92477008002, 92477008003, 92477008004, 92477008005, 92477008006, 92477011002, 92477011003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Chloride ug/L ND 1000 500 05/12/2019:18 LABORATORY CONTROL SAMPLE: 2883860 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride ug/L 20000 20300 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883861 2883862 MS MSD 92476908001 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 1130 mg/L 10000 10000 1140000 1130000 55 -2 90-110 1 10 M6 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883863 2883864 MS MSD 92476877005 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Chloride ug/L 6.3 mg/L 10000 10000 16500 16500 102 102 90-110 0 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 130 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541397 Analysis Method: SM 4500-CI-E-2011 QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477011004, 92477011005, 92477011006, 92477011007, 92477011008, 92477011009, 92477011010, 92477013001,92477013002,92477016001,92477016002 METHOD BLANK: 2885029 Matrix: Water Associated Lab Samples: 92477011004, 92477011005, 92477011006, 92477011007, 92477011008, 92477011009, 92477011010, 92477013001,92477013002,92477016001,92477016002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Chloride ug/L ND 1000 500 05/13/20 20:04 LABORATORY CONTROL SAMPLE: 2885030 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Chloride ug/L 20000 20100 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2885031 MS MSD 92476968002 Spike Spike Parameter Units Result Conc. Conc. Chloride ug/L ND 10000 10000 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2885033 MS MSD 92476969004 Spike Spike Parameter Units Result Conc. Conc. Chloride ug/L 9160 10000 10000 2885032 MS MSD MS MSD % Rec Max Result Result % Rec % Rec Limits RPD RPD Qual 9670 9960 94 97 90-110 3 10 2885034 MS MSD MS MSD % Rec Max Result Result % Rec % Rec Limits RPD RPD Qual 19500 19100 104 100 90-110 2 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 131 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541006 Analysis Method: SM 4500-CN-E-2011 QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 450OCNE Cyanide, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477011001 METHOD BLANK: 2883214 Matrix: Water Associated Lab Samples: 92477011001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide ug/L ND 8.0 6.0 05/14/2014:00 LABORATORY CONTROL SAMPLE: 2883215 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 100 100 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883216 2883217 MS MSD 2631659003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 81.1 ND 81 2 80-120 10 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883218 2883219 MS MSD 2631737002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 87.0 86.6 87 87 80-120 0 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 132 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 541007 Analysis Method: SM 4500-CN-E-2011 QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 450OCNE Cyanide, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477008001, 92477011002, 92477011003, 92477011004, 92477013001, 92477016001 METHOD BLANK: 2883224 Matrix: Water Associated Lab Samples: 92477008001, 92477011002, 92477011003, 92477011004, 92477013001, 92477016001 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide ug/L ND 8.0 6.0 05/14/2014:29 LABORATORY CONTROL SAMPLE: 2883225 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 101 101 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883226 2883227 MS MSD 92476638002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 72.0 67.4 72 67 80-120 7 10 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2883228 2883229 MS MSD 92476875005 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 85.6 70.8 86 71 80-120 19 10 M1,R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 133 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 542041 Analysis Method: SM 4500-CN-E-2011 QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 450OCNE Cyanide, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477008002, 92477011005, 92477011006, 92477011007 METHOD BLANK: 2888247 Matrix: Water Associated Lab Samples: 92477008002, 92477011005, 92477011006, 92477011007 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide ug/L ND 8.0 6.0 05/19/2011:26 LABORATORY CONTROL SAMPLE: 2888248 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 108 108 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2888249 2888250 MS MSD 92477191003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 51.9 46.3 50 44 80-120 11 10 M1,R1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2888251 2888252 MS MSD 92477192003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 58.1 61.7 56 60 80-120 6 10 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 134 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 542042 Analysis Method: SM 4500-CN-E-2011 QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 450OCNE Cyanide, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477008003, 92477008004, 92477008005, 92477008006, 92477011008, 92477011009 METHOD BLANK: 2888253 Matrix: Water Associated Lab Samples: 92477008003, 92477008004, 92477008005, 92477008006, 92477011008, 92477011009 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide ug/L ND 8.0 6.0 05/19/2011:54 LABORATORY CONTROL SAMPLE: 2888254 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 105 105 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2888255 2888256 MS MSD 2631793006 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 71.1 73.2 70 73 80-120 3 10 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2888257 2888258 MS MSD 2631794003 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 97.2 96.2 97 96 80-120 1 10 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 135 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: OSR LANDFILL GW Pace Project No.: 92477011 QC Batch: 542317 Analysis Method: SM 4500-CN-E-2011 QC Batch Method: SM 4500-CN-E-2011 Analysis Description: 450OCNE Cyanide, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92477011010, 92477013002, 92477016002 METHOD BLANK: 2889492 Matrix: Water Associated Lab Samples: 92477011010, 92477013002, 92477016002 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Cyanide ug/L ND 8.0 6.0 05/20/2017:25 LABORATORY CONTROL SAMPLE: 2889493 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Cyanide ug/L 100 96.1 96 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2889494 2889495 MS MSD 92477011010 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 93.1 89.5 93 90 80-120 4 10 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2889496 2889497 MS MSD 92477013002 Spike Spike MS MSD MS MSD % Rec Max Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual Cyanide ug/L ND 100 100 51.9 80.7 52 81 80-120 43 10 M1,R1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 136 of 155 Pace Analytical Services, LLC lac, Analyilcal ® 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: OSR LANDFILL GW Pace Project No.: 92477011 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. ANALYTE QUALIFIERS IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be considered an estimated value. IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be considered an estimated value. L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples may be biased high. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. R1 RPD value was outside control limits. SO Surrogate recovery outside laboratory control limits. S3 Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample. ST Surrogate recovery was above laboratory control limits. Results may be biased high. v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias. v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 137 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: OSR LANDFILL GW 92477011 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92477008001 MWA R 8151A 1474966 EPA 8151 1474966 92477008002 FIELD BLANK 8151A 1474966 EPA8151 1474966 92477008003 MW-4R 8151A 1474966 EPA8151 1474966 92477008004 MW-2R 8151A 1474966 EPA8151 1474966 92477008005 MW-15 8151A 1476953 EPA8151 1476953 92477008006 EQBL 8151A 1476953 EPA8151 1476953 92477008001 MWA R EPA 3510C 541169 EPA 8081 B 541496 92477008002 FIELD BLANK EPA 3510C 541169 EPA 8081 B 541496 92477008003 MW-4R EPA 3510C 541169 EPA 8081 B 541496 92477008004 MW-2R EPA 3510C 541169 EPA 8081 B 541496 92477008005 MW-15 EPA 3510C 541169 EPA 8081 B 541496 92477008006 EQBL EPA 3510C 541169 EPA 8081 B 541496 92477013001 MW-10 EPA 3510C 540972 EPA 8081 B 541219 92477013002 MW-7 EPA 3510C 541169 EPA 8081 B 541496 92477008001 MWA R EPA 3010A 541473 EPA 6010D 541491 92477008002 FIELD BLANK EPA 3010A 541473 EPA 6010D 541491 92477008003 MW-4R EPA 3010A 541473 EPA 6010D 541491 92477008004 MW-2R EPA 3010A 541473 EPA 6010D 541491 92477008005 MW-15 EPA 3010A 541473 EPA 6010D 541491 92477008006 EQBL EPA 3010A 541474 EPA 6010D 541492 92477011001 MW-8 EPA 3010A 541474 EPA 6010D 541492 92477011002 MW-9 EPA 3010A 541474 EPA 6010D 541492 92477011003 MW-14 EPA 3010A 541474 EPA 6010D 541492 92477011004 SW-3 EPA 3010A 541474 EPA 6010D 541492 92477011005 MW-11 EPA 3010A 541474 EPA 6010D 541492 92477011006 MW-12 EPA 3010A 541474 EPA 6010D 541492 92477011007 MW-13 EPA 3010A 541474 EPA 6010D 541492 92477011008 MW-5R EPA 3010A 541474 EPA 6010D 541492 92477011009 SW-4 EPA 3010A 541474 EPA 6010D 541492 92477011010 SW-1 EPA 3010A 541474 EPA 6010D 541492 92477013001 MW-10 EPA 3010A 541474 EPA 6010D 541492 92477013002 MW-7 EPA 3010A 541474 EPA 6010D 541492 92477016001 SW-2 EPA 3010A 541474 EPA 6010D 541492 92477016002 MW-3R EPA 3010A 541474 EPA 6010D 541492 92477008001 MWA R EPA 7470A 541804 EPA 7470A 541849 92477008002 FIELD BLANK EPA 7470A 541804 EPA 7470A 541849 92477008003 MW-4R EPA 7470A 541804 EPA 7470A 541849 92477008004 MW-2R EPA 7470A 541804 EPA 7470A 541849 92477008005 MW-15 EPA 7470A 542610 EPA 7470A 542745 92477008006 EQBL EPA 7470A 542610 EPA 7470A 542745 92477011001 MW-8 EPA 7470A 542610 EPA 7470A 542745 92477011002 MW-9 EPA 7470A 542610 EPA 7470A 542745 92477011003 MW-14 EPA 7470A 542610 EPA 7470A 542745 92477011004 SW-3 EPA 7470A 542610 EPA 7470A 542745 92477011005 MW-11 EPA 7470A 542610 EPA 7470A 542745 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 138 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: OSR LANDFILL GW 92477011 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92477011006 MW-12 EPA 7470A 542610 EPA 7470A 542745 92477011007 MW-13 EPA 7470A 542610 EPA 7470A 542745 92477011008 MW-5R EPA 7470A 542610 EPA 7470A 542745 92477011009 SW-4 EPA 7470A 542610 EPA 7470A 542745 92477011010 SW-1 EPA 7470A 542610 EPA 7470A 542745 92477013001 MW-10 EPA 7470A 542610 EPA 7470A 542745 92477013002 MW-7 EPA 7470A 542610 EPA 7470A 542745 92477016001 SW-2 EPA 7470A 542610 EPA 7470A 542745 92477016002 MW-3R EPA 7470A 542610 EPA 7470A 542745 92477008001 MW-1 R EPA 3510C 541145 EPA 8270E 541416 92477008002 FIELD BLANK EPA 3510C 541145 EPA 8270E 541416 92477008003 MW-4R EPA 3510C 541145 EPA 8270E 541416 92477008004 MW-2R EPA 3510C 541145 EPA 8270E 541416 92477008005 MW-15 EPA 3510C 541145 EPA 8270E 541416 92477008006 EQBL EPA 3510C 541145 EPA 8270E 541416 92477016001 SW-2 EPA 3510C 540969 EPA 8270E 541125 92477016002 MW-3R EPA 3510C 541145 EPA 8270E 541416 92477008001 MWA R EPA 8260D 542119 92477008002 FIELD BLANK EPA 8260D 542117 92477008003 MW-4R EPA 8260D 542188 92477008004 MW-2R EPA 8260D 542188 92477008005 MW-15 EPA 8260D 542188 92477008006 EQBL EPA 8260D 542188 92477011001 MW-8 EPA 8260D 542112 92477011002 MW-9 EPA 8260D 542112 92477011003 MW-14 EPA 8260D 542112 92477011004 SW-3 EPA 8260D 542112 92477011005 MW-11 EPA 8260D 542119 92477011006 MW-12 EPA 8260D 542119 92477011007 MW-13 EPA 8260D 542119 92477011008 MW-5R EPA 8260D 542188 92477011009 SW-4 EPA 8260D 542188 92477011010 SW-1 EPA 8260D 542188 92477011011 TRIP BLANK EPA 8260D 542188 92477013001 MW-10 EPA 8260D 542117 92477013002 MW-7 EPA 8260D 542188 92477016001 SW-2 EPA 8260D 542117 92477016002 MW-3R EPA 8260D 542188 92477008001 MWA R EPA 8260D Mod. 541676 92477008002 FIELD BLANK EPA 8260D Mod. 541676 92477008003 MW-4R EPA 8260D Mod. 541824 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 139 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: OSR LANDFILL GW 92477011 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92477008004 MW-2R EPA 8260D Mod. 541824 92477008005 MW-15 EPA 8260D Mod. 541824 92477008006 EQBL EPA 8260D Mod. 541824 92477011001 MW-8 EPA 8260D Mod. 541676 92477011002 MW-9 EPA 8260D Mod. 541676 92477011003 MW-14 EPA 8260D Mod. 541676 92477011004 SW-3 EPA 8260D Mod. 541676 92477011005 MW-11 EPA 8260D Mod. 541676 92477011006 MW-12 EPA 8260D Mod. 541676 92477011007 MW-13 EPA 8260D Mod. 541677 92477011008 MW-5R EPA 8260D Mod. 541824 92477011009 SW-4 EPA 8260D Mod. 541824 92477011010 SW-1 EPA 8260D Mod. 541824 92477013001 MW-10 EPA 8260D Mod. 541676 92477013002 MW-7 EPA 8260D Mod. 541824 92477016001 SW-2 EPA 8260D Mod. 541676 92477016002 MW-3R EPA 8260D Mod. 541824 92477008001 MWA R SM 2320E-2011 541634 92477008002 FIELD BLANK SM 2320B-2011 541634 92477008003 MW-4R SM 2320B-2011 542078 92477008004 MW-2R SM 2320B-2011 542078 92477008005 MW-15 SM 2320B-2011 541634 92477008006 EQBL SM 2320B-2011 541813 92477011001 MW-8 SM 2320B-2011 541022 92477011002 MW-9 SM 2320B-2011 541634 92477011003 MW-14 SM 2320B-2011 541634 92477011004 SW-3 SM 2320E-2011 541634 92477011005 MW-11 SM 2320B-2011 541634 92477011006 MW-12 SM 2320B-2011 541634 92477011007 MW-13 SM 2320B-2011 541634 92477011008 MW-5R SM 2320B-2011 541813 92477011009 SW-4 SM 2320E-2011 541813 92477011010 SW-1 SM 2320E-2011 541813 92477013001 MW-10 SM 2320B-2011 542078 92477013002 MW-7 SM 2320B-2011 541813 92477016001 SW-2 SM 2320E-2011 541634 92477016002 MW-3R SM 2320B-2011 541813 92477008001 MWA R SM 254OC-2011 541184 92477008002 FIELD BLANK SM 254OC-2011 541184 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 140 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: OSR LANDFILL GW 92477011 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92477008003 MW-4R SM 2540C-2011 541184 92477008004 MW-2R SM 254OC-2011 541198 92477008005 MW-15 SM 254OC-2011 541198 92477008006 EQBL SM 254OC-2011 541198 92477011001 MW-8 SM 2540C-2011 540941 92477011002 MW-9 SM 254OC-2011 541102 92477011003 MW-14 SM 254OC-2011 541102 92477011004 SW-3 SM 254OC-2011 541102 92477011005 MW-11 SM 2540C-2011 541184 92477011006 MW-12 SM 2540C-2011 541184 92477011007 MW-13 SM 2540C-2011 541184 92477011008 MW-5R SM 2540C-2011 541184 92477011009 SW-4 SM 254OC-2011 541198 92477011010 SW-1 SM 254OC-2011 541198 92477013001 MW-10 SM 2540C-2011 541102 92477013002 MW-7 SM 254OC-2011 541184 92477016001 SW-2 SM 2540C-2011 541102 92477016002 MW-3R SM 254OC-2011 541184 92477008001 MW-1R SM 4500-S2D-2011 541111 92477008002 FIELD BLANK SM 4500-S2D-2011 541111 92477008003 MW-4R SM 4500-S2D-2011 541114 92477008004 MW-2R SM 4500-S2D-2011 541114 92477008005 MW-15 SM 4500-S2D-2011 541114 92477008006 EQBL SM 4500-S2D-2011 541114 92477011001 MW-8 SM 4500-S2D-2011 540866 92477011002 MW-9 SM 4500-S2D-2011 541111 92477011003 MW-14 SM 4500-S2D-2011 541111 92477011004 SW-3 SM 4500-S2D-2011 541111 92477011005 MW-11 SM 4500-S2D-2011 541111 92477011006 MW-12 SM 4500-S2D-2011 541111 92477011007 MW-13 SM 4500-S2D-2011 541111 92477011008 MW-5R SM 4500-S2D-2011 541114 92477011009 SW-4 SM 4500-S2D-2011 541114 92477011010 SW-1 SM 4500-S2D-2011 541114 92477013001 MW-10 SM 4500-S2D-2011 541111 92477013002 MW-7 SM 4500-S2D-2011 541114 92477016001 SW-2 SM 4500-S2D-2011 541111 92477016002 MW-3R SM 4500-S2D-2011 541114 92477008001 MWA R EPA 300.0 Rev 2.1 1993 541452 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/09/2020 08:57 AM without the written consent of Pace Analytical Services, LLC. Page 141 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: OSR LANDFILL GW Pace Project No.: 92477011 Lab ID 92477008002 92477008003 92477008004 92477008005 92477008006 92477011001 92477011002 92477011003 92477011004 92477011005 92477011006 92477011007 92477011008 92477011009 92477011010 92477013001 92477013002 92477016001 92477016002 92477008001 92477008002 92477008003 92477008004 92477008005 92477008006 92477011001 92477011002 92477011003 92477011004 92477011005 92477011006 92477011007 92477011008 92477011009 92477011010 92477013001 92477013002 92477016001 92477016002 92477008001 92477008002 92477008003 92477008004 92477008005 92477008006 Sample ID FIELD BLANK MW-4R MW-2R MW-15 EQBL MW-8 MW-9 MW-14 SW-3 MW-11 MW-12 MW-13 MW-5R SW-4 SW-1 MW-10 MW-7 SW-2 MW-3R MWAR FIELD BLANK MW-4R MW-2R MW-15 EQBL MW-8 MW-9 MW-14 SW-3 MW-11 MW-12 MW-13 MW-5R SW-4 SW-1 MW-10 MW-7 SW-2 MW-3R MWA R FIELD BLANK MW-4R MW-2R MW-15 EQBL Date: 06/09/2020 08:57 AM QC Batch Method EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 SM 4500-CI-E-2011 SM 4500-CI-E-2011 SM 4500-CI-E-2011 SM 4500-CI-E-2011 SM 4500-CI-E-2011 SM 4500-CI-E-2011 SM 4500-CI-E-2011 SM 4500-CI-E-2011 SM 4500-CI-E-2011 SM 4500-CI-E-2011 SM 4500-CI-E-2011 SM 4500-CI-E-2011 SM 4500-CI-E-2011 SM 4500-CI-E-2011 SM 4500-CI-E-2011 SM 4500-CI-E-2011 SM 4500-CI-E-2011 SM 4500-CI-E-2011 SM 4500-CI-E-2011 SM 4500-CI-E-2011 SM 4500-CN-E-2011 SM 4500-CN-E-2011 SM 4500-CN-E-2011 SM 4500-CN-E-2011 SM 4500-CN-E-2011 SM 4500-CN-E-2011 QC Batch Analytical Method 541452 541452 541452 541452 541452 541452 541453 541453 541453 541453 541453 541453 541453 541453 541453 541453 541453 541453 541453 541127 541127 541127 541127 541127 541127 541126 541127 541127 541397 541397 541397 541397 541397 541397 541397 541397 541397 541397 541397 541007 542041 542042 542042 542042 542042 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. SM 4500-CN-E-2011 SM 4500-CN-E-2011 SM 4500-CN-E-2011 SM 4500-CN-E-2011 SM 4500-CN-E-2011 SM 4500-CN-E-2011 Analytical Batch 541295 542129 542130 542130 542130 542130 Page 142 of 155 leAnalyiical www.pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: OSR LANDFILL GW 92477011 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92477011001 MW-8 SM 4500-CN-E-2011 541006 SM 4500-CN-E-2011 541292 92477011002 MW-9 SM 4500-CN-E-2011 541007 SM 4500-CN-E-2011 541295 92477011003 MW-14 SM 4500-CN-E-2011 541007 SM 4500-CN-E-2011 541295 92477011004 SW-3 SM 4500-CN-E-2011 541007 SM 4500-CN-E-2011 541295 92477011005 MW-11 SM 4500-CN-E-2011 542041 SM 4500-CN-E-2011 542129 92477011006 MW-12 SM 4500-CN-E-2011 542041 SM 4500-CN-E-2011 542129 92477011007 MW-13 SM 4500-CN-E-2011 542041 SM 4500-CN-E-2011 542129 92477011008 MW-5R SM 4500-CN-E-2011 542042 SM 4500-CN-E-2011 542130 92477011009 SW-4 SM 4500-CN-E-2011 542042 SM 4500-CN-E-2011 542130 92477011010 SW-1 SM 4500-CN-E-2011 542317 SM 4500-CN-E-2011 542592 92477013001 MW-10 SM 4500-CN-E-2011 541007 SM 4500-CN-E-2011 541295 92477013002 MW-7 SM 4500-CN-E-2011 542317 SM 4500-CN-E-2011 542592 92477016001 SW-2 SM 4500-CN-E-2011 541007 SM 4500-CN-E-2011 541295 92477016002 MW-3R SM 4500-CN-E-2011 542317 SM 4500-CN-E-2011 542592 Date: 06/09/2020 08:57 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 143 of 155 Document Name: Document Revised: February 7, 2018 m aceAnalytical Sample Condition Upon Receipt(SOUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville [� Raleigh[] Mechanicsville❑ Sample. , . Client Name: ° Wp# : 92477011 � ' � Project q: ❑Courier: ❑Fed fx []UPS ❑U5P5 SClient 11111111111111111111111 Commercial ❑Pate ❑Other: �-� 92477011 Custody Seal Present? ❑Yes �O Seals Intact? []Yes E to gate/Initials Person Examining Contents: Packing Material: ❑Bubble Wrap eaubbie Bags []None ❑ Other 8101agical Tissue Frren? Thermometer: ❑Yes ❑❑ No N/A R • Gun ID: 92Ta61 Type of ice: wet ❑Blue [)None Cooler Temp [°CI: 0, C I, < Correction Factor: Add/subtract (°C) +0,1 ., Temp should be above freezing to 6°C Cooler Temp Corrected (°C}: `� • []Samples out of temp cr,teria. Samples on ice, cooling process has begun USDA Regulated Soil (g NIA, water sample) Did samples Orieirtate in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source linter F tionally, l�Yes W. ;—i� i °u.,..�W and m,e..,, m I r•-lu_. Cam ments/Dlscre ancy: Chain of Custody Present? Yes ❑No ❑N/A 1. Samples Arrived within Hold Time? es No QN/A 2. Short Hold Time Analysis (e72 hr.)? []Yes ErNo [-I N/A 3. Rush Turn Around Time Requested? []Yes a [I N/A 4. Sufficient Volume? EJYes ❑No ❑N/A S. Correct Containers Used? : es []No []N/A 6. -Pace Containers Used? 2fes ONO ❑N/A Containers Intact? W es� ❑No ❑N/A 7. Dissolved analysis: Samples Field Filtered? ❑Yes [:]No PN/A S. Sample Labels Match COQ es FINo F1NJA 9. i� } -Includes Date/Time/ID/Analysis Matrix: Heads ace in VOA Vials i>5-6mmi? ❑Ye io [_-]N/A 10. Trip Blank Present? es []No ❑NIA 11. Trip Blank Custody Seals Present? 2 Yes ❑No ❑N/A COMMENTS/SAMPLE DISCREPANCY CLIENT NOTIFICATION/RESCILUTiON Person contacted: Project Manager SCURF Review; Project Manager SRF Review: Date/Time: Lot ID of split containers: Date: Date: Field Data Required? []Yes []No Page 144 of 155 Document Name: Document Revised: February 7, 2018 m aecAnaJyrical sample Condition Upon Recel t(SiCUR) Page i of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Caroilnas Quallty Office *Check mark top half of box if pH and/or dechlorination is verified and within the acceptance range for preservation samples, Exceptions: VOA, C'oliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLNg "Bottom half of box is to list number of bottle Project # WO# : 92477011 Ph: KLH1 Due Date: 05/22/20 CLIENT: 92—HDR d a m m Q 7 �+ A a E Ln *V a m z v v m c 7 •+ a E a N 7 a m z a a m 7 a+ A a E a T > a m a ? y rs c V m W .-i > a ca N a D N Vu - a J E y� H` V7 C a m n v y ^' z 2 �• E o N Z a m _ o u V a, J ,n N a m ~ .N a OS ? m a, J E ,n N U a cc v m to •o d a=+ o E v y �i LL 7i U ? v 2 v C t 4 my ri a v _ u 2 91 a a - �. ri 47 a Q d Z y y n c d fl £ E o N 6 in l7 a H v = a v a N 2 M E a °: ..1 h rl 0 4 x a o N Z 5 E ¢ E o N lil m Lo a Q z u = z a E 4 J F o r"'i 4 m 0 a M V' a z _ lJ 2 4 O} J E x QI 0 0 a 2 ^ � vi 2 ¢ O J E q F Cf l7 2 CL C � ¢ O E q C1 l7 y v O 2 ¢ O E q 4 Q% C7 O = ? c 1 y Jr w a n •g .�-. Y Q 0 ? x m = a } = Y n h y " Y U' 7 a a z Y d W N J E N C, w 3 z a ro w, E N N a w 1� '" nN 2 Z a a c N M a m a Z a C A E ¢ E 0 6 O t.7 a ? o c J E N 7 �7 Jr a z v 2 c e ar D ¢ J £ 7 6 O1 4h a z j 3 \,A, 1 � 1 I N N\\ I 6 XX j \N\i- -TO_N L_\\4KX IN NN\ 11 r i X-11 T ? pH Adjustment log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added lot N Now Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out of hold, Incorrect preservative, out of temp, Incorrect containers. Page 145 of 155 PaceAnalyiica!' CHAIN -OF -CUSTODY 1 Analytical Request Document wrrw.—RUSCD. The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. aacuon A Section B Section C Required Client Information: Required Project Information: Invoice Information- Page: 1 Of T Company: HDR Report To: Mark Fllardi / Charies Gruenberg Attention: Address: 440 S. Church St Copy To: Company Name: Suite 900, Charlotte, NC 28202 Address Regulator A anc Email; mark.filardi hdrinc, corn Purchase Order It Pace Quote: Phone: (704)33M787 IFax Project Name, OSR Landfill GW Pace Project Mana er: ke vin.herring@paoelabs.com. 3 evin.herring pacelabs.com, State 1 Location Requested Due Date', 1project #: I Od 1 4 Pace Profile # 2588 NC R vested An lysis Filtered YIN ° 2 MATRIX coos o COLLECTED = Preservatives -� } Drinking Water Ow c U D W,I r WT U w�:Ia wm„r ww Protlud R SAMPLE ID S.Ws.W SL � '? START END ru `1 r Oil OL One Character per box. Wr Wa .. M C q — tA•Z, 0-9 1, -j ar AR Other OT Sample Ids must be unique Tows 15 o a 't F w c H v O o ? '� N" },r Q °a o m E3 o o g .0 V > V v m m v F DATE TIME DATE TIME Q O C N Z _ U = U Z N z N L 4 Q 9 cn O m N m Cn ❑ F ri3 v ?. cs J 2 v D= k 1 \ l =i 1 ziy" 3 I 2 M W— ' � ;��_LS U��s 93 111311 1 3 a ICI `' i G z" C' i �S 9 1 1 3 i 7 8 }a,SS [ ) 1 1 ' [ I I f 1 It; s M W —? c;— ijA6 1 1 i I E cSO� car ,2 ADDITIONAL COMMENTS RELINQUISHED BY 1 AFFILIATION DATE TIME ACCEPTED BY 1 AFFILIATION DATE TIME SAMPLE CONDITIONS I707 'I-c1 P. t SAMPLER NAME AND SIGNATURE ca v PRINT Name of SAMPLER: C�c ,.�,,i,� a. _ d m } o F-1 m o } } SIGNATURE of SAMPLER: ,y' DATE Signed- IL Document Name: Document Revised: February 7, 2018 m aceAnalytical Sample Condition Upon Recelpt(SCUR) Pagel of 2 Document No.: Issuing Authority: F-CAR-CS•033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville Ej� Raleigh[] Mechanicsville❑ SarnplUpon Receipt • Condition Client Name: � ,I ProJectsi: W0# : 92477008 Courier: ❑Fed Ex []UPS ❑US PS Client II I III I IIII I I I I I II III ❑ Commercial ❑Pace ❑Other: Custody Seal Present? ❑Yes fo Seals intact? ❑Yes QNo/ 82477008 / Date/Initlah Person Examining Contents: Packing Material: ❑Bubble Wrap v Bubble Bags ❑None ❑ Other Biological Tissue flltzen? Thermometer: � ❑Yes ❑No QN/A LIKRGunID: 92TO61. Type of Ice: [Iwet ❑3lue ❑None Cooler Temp (°C):JCorrection Factor: Add/Subtract(°Cj +0 �� Temp should be above freezing to VCCooler Temp Corrected (°Ci: / _ Jl _ 0 - / ❑5amples out of temp criteria. Samples on Ice, cooling process has begun USDA Regulated Soil N/A, water sample) Did samples originate in a quarantine tone within the United States: CA, NY, or SC (check maps)? old samples originate from a foreign source Jinternp,15naily, Dyes IJio a:.. o... n n. __ Comments/Dlscre ancy: Chain of Custody Present? 2Yes []No ❑N/A 1. Samples Arrived within Hold Time? 3s No ❑N/A 2. Shot Hold Time Analysis (<72 hr.)? ❑Yes No ❑N/A 3. Rush Turn Around Time Requested? ❑Yes No ❑N/A 4. Sufficlent Volume? " les []No ❑N/A 5. Correct Containers Used? IN ' ❑No ❑N/A 6. -Pace Containers Used? res [:]No ❑N/A Containers Intact? W es ❑No❑N//A 7. Dissolved analysis: Samples Field filtered? ❑Yes QNo j /A 8. Yes nNo N A 9. -Includes Date/Time/ID/Analysis Matrix: Heads ace in VOA Vials (>5-6mmi? (--]Yes 2f o ❑N A 10, Trip Blank Present? ❑Yes []No - N/A 11. Trip Blank Custody Seals Present? ❑Yes ❑No QI%A COMMENTS/SAMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time; Lot ID of split containers: Date: Date: Field Data Required? []Yes [—]No Page 147 of 155 Document Name: Document Revised: February 7, 2018 a aceAnalyfical Sample Condition Upon Recel t(SCUR) Page 1 of 2 Document No.: Issuing Authority, F-CAR•CS-033-Rev.06 Pace Carolinas Quality Office *Check mark top half of box if pH and/or dechlorination is verified and wlthin the acceptance range for preservation samples. Exceptlons: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg **Bottom half of box is to list number of bottle Project# WO# : 92477008 PM: KLH1 Due Dale: 05/22/20 CLIENT: 92—HDR ¢ O z z z ` N z a Z roW N N v Z m M v ? m ? J n = 2 � e`vCL M. a a is c n y Z „�, _ Z q `= Z C7 2 H Z a c a c CL c d a e O N = z = a z y OM z l7 p d V '� a j a O N z a E a a Z m en a Z 2 a O A a 7 ,� Lq 04 = z c 7 c o c. e u N u N u N V u N u N N N 4e i a 7 N Z 01 d Z J E () �. @ z o, C en = .�'. �+ Y a d a 4 'u @ a a y n E E ¢ E ¢ N O O } O i 6 a 'r'' w a 4 u E a N o _ E of N E ,n!y E a L, rl �_ ti o N ° _ E N M E J E O E E G ° v n E E N E a E O E O E O ,N-r V1 Z N Nv■ a a rl, .ry+ 0 ti L7 0 M I q T 7Q IfS N M �r NCL7� 7 Oa m go m m m 4 4 yw a m 0 a Vm G �' ✓ f J 5 ✓ Y ? X/ B 9 10 11 1!S!S111-T-t7t-� fft pH Adjustment Log for Preserved Samples $ample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot N Note: Whenever there is a discrepartcv affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office ii.e. Out of hold, incorrect preservative, out of temp, Incorrect containers. Page 148 of 155 F 31'Analytiml www.rA[russ.[rsw Section A Required Client Information: Company, HDR Address 440 S. Church Suite 900. Charlotte, NC 2820. Email: Due W F- 3 4 5 i] Section B Information: Filardi I Charles se Order#: Name: OSR Landfill GW #. MATRIX CODR a OV O1.1k..9 Water OW W.I.r WT O1 u U w�alr. water ww SAMPLE ID P ,VS P SoiVSolitl SL _ - 0.1 Or One Character per box. wipe WP STAR' tA-Z, 0-91 , -) Art AR Sample Ids must 6e unique Osxer� Os o 0 � a a a zi " DATL IL !r rL T G- �'f • �! t�s � L L- t -. ADDITIONAL COMMENTS CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately, Section C a Invoice Information; )erg Attention: Page : 1 Of 1 Company Name: manager kevin. #', 2588 ",gym RELINQUISHLD BYT AFFTCJATfO� (--I � &A z } N I� rn — m iu � c c a = > y U A } —.I I IML ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS %?c 4 �i tea) iPLER NAME AND SIGNATURE T Name of SAMPLER: U T5i- PRI14c SIGNATURE ct SAMPLER: �'" Document Name: Document Revised: February 7, 2018 a aceArralytrcal Sample Condition Upon Recelpt(SCUR) Page 1 of 2 Document No.: issuing Authority: F•CAR-CS•033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville BI Raleigh[] Mechanicsville❑ Sample Condition Client Name:uponReceiWO: 92477013 Courier: Project #: []Fed Ex ❑UPS ❑USPS lient 1111111111111111111111 ❑ Commercial ❑Pace 00ther: 92477013 Custody SeatPresent7 ❑Yes M to Seals intact? Dyes [ fo / Cate/initials Person Examintng Contents: ( l'� Packing Material: ❑Bubble Wrap Bubble Bags ❑None ❑ Other Biological Tissue F zen? Thermome❑Yes []NO N/A 5��92TO61 Type of Ice: [ wet ❑glue ❑None un ID: 2 Cooler Temp (°C): •• l Correction Factor: Add/Subtract [°Cj +_0 1_ Temp should be above freezing to 6°C Cooler Temp Corrected ('C): —i ❑Samples out of temp Criteria. Samples on Ice, coaling process has begun USDA Regulated Soil (0 N/A, water sample) Did ter samples on to in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (inionally, I�Ye's No—F... li— W—U —d D... — pi-17 { ivee Comma nts/Dlscre ancy: Chain of Custody Present? Yes ONO ❑N/A 1. Samples Arrived within Hold Time? es Na ❑N/A 2. Short Hold Time Analysis (02 hr.)? Dyes No []N/A 3, Rush Turn Around Time Requested? ❑Yes EJNo ❑N/A 4. Sufficient Volume? Yes ❑No []N/A 5. Correct Containers Used? -Pace Containers Used? IEK �,� Imes ❑No ❑No ❑N/A ❑N/A 6. Containers Intact? Yes [:]No ❑N/ 7. Dissolved analysis: Samples Field Filtered? ❑Y s ❑Na N/A S. Sample LabgIs Match COC? yes No nN JA 9. -Includes Date/Time/ID/Analysis Matrix: �'J I Heads ace in VOA Vials (>5-6mm)? [)Yes MNo ❑ A 10. Trip Blank present? Trip Blank Custody Seals Present? []Yes ❑Yes []No ❑No ' N/A N/A 11. COMMENTS/SAMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Project Manager SCURF Review: Project Manager SRF Review: Lot ID of split containers: Date: Date: field Data Required? []Yes ❑No Page 150 of 155 Document Name: Document Revised: February 7, 2018 eeARaV cal Sample Co Upon Recei t(SCUft) Page 1 of 2 Document No.: Document Issuing Authority: F-CAR-05-033-Rev.06 Pace Carolinas Quallty Office *Check mark top half of box if pH and/or dechlorination is Project # verified and within the acceptance range for preservation samples. Exceptions: VOA, Cali€arm, TOC, oil and Grease, DRO/8015 (water) DOC, LLHg "Bottom half of box is to list number of bottle WO# : 92477013 PM: KLH1 Duo Date: 05/22/20 CLIENT: 92-HDR « _ u v v v a u a J E n N v a m d N v V a J E a N em a. mo a w2 w U a J E o O ry a m a G = f1 d d m N v a N V J E yy7 N 6 m v a Q = V a J E a m rL m n Z aA mn � Z y J E .V a. m x O Z J E n a a m Z [ "vi v do CC G a 7 7 ]i " u Z v v C 7 E ¢ `v = M 0 a y x a U = E ¢ m - 14 (D d u a Z a `y E ¢ .-J E m l7 ¢ v Y vv1 nl S a E a v .y l7 d T v O s a 5 o H A m 0l0 d U It m a 4 J o N ran m ¢ U a O E c al Q 0 Q rn m ¢ O > E In l7 ] ¢ C C a O > E o a� t0 ] G Z O fir a O ] E—° m C7 0 ? Y M ur " v a s Q 0 ] Y ca 0 = 7 m G b rY7 ] Q Z u A fl N E u~i a m u a m E a N n a m a+ 61 ry 2 E o In m a m 2 n j E a J E 0 Q o O d ? 3 o c '„ N E N ��7 Vi ] 4 c -D ¢ E V Obi l7 0 X/ n 3 4 . . . . . . . . . . . . . . . . . . . . . 6 7 9 SO ii pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot t# Note: Whenever there is a discrepancy affecting North Carolina Compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e. Out nf hotd, Incorrect preservative, out of temp, Into rrettcontalners. Page 151 of 155 /.; a'aceMaJytical wWW.r�CELABs.rPM Section A Required Client Information: Company HDR Address: 440 S. Church St LU H 1 2 3 4 5 6 7 9 12 Fax Due Date: SAMPLE ID One Character per box. (A-Z, 0-9 1, -j Sample Ids must be unique Section B Required Project Information: Report To: Mark Filardi 1 Charles Purchase Order#� Project Name: OSR Landfill GW Project M TRIx CODE n _ a_ ° u Drinking Water Watn DW WT U m Wasin W.I., Ww Produd P _ S.&SOhd C11 SL aL START WrP' WP W Air AR ❑ Other OT O } Tr;sue TS X Q� J Q CHAIN -OF -CUSTODY 1 Analytical Request Document The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section C Invoice Information: Page ' 1 Of 1 jerq Attention. Company Name: Address: Regulatory q en Pace quote: . Pace Project Manager: kevin.herring pacelahs.com, State f Location Pace Profile #: 2588 NC TIME I DA = Preservatives Z } w J Jv END o a � F r O> V% L c m m C O a U C m y z == O O 4 TIME z U c'n ADDmoNALCOMMENTS RELINQUISHED BYI AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME li"4NZ 17C -7 SAMPLER NAME AND SIGNATURE PRINT Name of SAMPLER: '+ SIGNATURE of SAMPLER: "I DATE Signed- SAMPLE CONDITIONS U I o C 2 °f Document Name: Document Rev#sed: February 7, 2018 m /�alcehvyical Sample on Upon Recelpl(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS•033-Rev.06 Pace Carolinas Quality Office Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Huntersville ©� Raleigh❑ Met:hanlcsville❑ Sample Condition Client Name: Upon Receipt1_r i� Project # Courier: []Fed Ex 7 ❑UPS ❑USPS Erclient ❑ Commercial ❑Pace ❑Other: Custody Seal Present? ❑Yes [No Seals Intact? ❑Yes ETNo Patking Material: ❑Bubble Wrap QBubble Bags ❑None ❑ Other Thermometer' ff [I'M Gun ID: 92TO61 Type of Ice: ❑Wet []Blue � Cooler Temp (°C): ! p - --) Correction Factor: Add/Subtract J'Q +^0.� Cooler Temp Corrected (°C): i- 9 USDA Regulated Soil I N/A, water sample) Did samples o^rig'i ate in a quarantine zone within the United States CA, NY, or 5C (check maps)? I�Yes I�{Ne W0#:92477016 II I Ill I IIII I I ll I III III 92477016 Date/In[Vals Person EwsminingContents: Biological Tissue ozen? ❑None �" Dyes ❑No N/A Temp should be above freezing to VC ❑Samples out of temp criteria. Samples on ice, cooling process has begun Did samples originate from a foreign source lintern3tionally, Comments/alstre ancy: Chain of Custody Present? // Byes []ND ❑N/A 1. Samples Arrived within Hold Time? O/Yes ONo ❑N/A 2. Short Hold Tlme Analysis (<72 hr.)? ❑yes No ❑N/A 3. Rush Turn Around Time Requested? ❑Yes EK. []NIA 4. Sufficient Volume? ErYe ❑No ❑N/a 5. Correct Containers Used? Pace Containers Used? Y s (_ es ON. [-]No ❑ N/A ❑N/A 6. 7. Containers intact? Yes ❑No ❑N A Dissolved analysis: Samples Field Filtered? ❑Yes ❑No O N/A 8. es ElNo EINIA 9. -Includes Date/Time/ID/Analysls Matrix: �� 1 Heads ace in VOA Vials (>S-6mm)? ❑Yes LJNQ ❑ PYA 10. Trip Blank Present? Trip blank Custody Seals Present? ❑Yes Des ❑No [:]No N/A !/A 11. COMMENTS/SAMPLE DISCREPANCY Lot 10 of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Date/Time; Date: Date: Field Data Required? ❑Yes []No Page 153 of 155 Document Name: Document Revised: February 7, 2018 el?Anafyttal Sample Condition Upon Recel t(SCUR) Page 1 of 2 Document No.: Issuing Authority: F-CAR-CS-033-Rev.06 Pace Caroilnas QualltyOfflce *Check mark top half of box if pH and/or dechlorination is Project #; verified and within the acceptance range for preservation samples. Exceptions: VQA, Coliform, TOC, Oil and Grease, ORO/8015 (water) DOC, Ll **Bottom half of box is to list number of bottle W0#:92477016 PM. KLH1 Due Dale: 05/22/20 CLIENT: 92-HDR _ v N Z °� n C 7 A a J E eNn m v 41 2 n C 7 m c J E N 7 m v a di N a C N a J E 7 m Z a v 2 IV a G � Y d y m N V O N N V a J E v1 d Na v 6 m N V x `' Z 4 a J E N 2 a m Os DiS N $ Q Z y 4 J E N a m 'F7'� s - z O f0 ? - n J E ram+ U n m v m 3 N a E 4 u v y a CL c IU a ¢ v en 7 W Q N V O = v 'a E Q `m N T D Q = N °� w c C D a n E ¢ J i N kv Q N V _ a c O 4 S b E Q `m ,ti ti7 0 N V = ° O N 2 E ¢ E N 0 4 -- = z U r ? a E Q J E 0 N .,(. m O Q %V 4 Z �_ lJ x 4 E G S l7 O Q z z ^' ON �n A Z Q O 'J J E G Y�- ] Z CL C 7 Q O 7 E Q ] = O M T 6 O 7 E G l9 O ? W Y r'nr O �^ x y a ° a �p Q O ] m N m = q S � ag d o• N m 7 r I Q H b R m .Y E N m I \ z v a 'n E N a v< °' yj $ N 2 z V N T a E 4 m z 0 -0 N Z a a � y t E Q J E o N Q 0 Q = c O = c N a: O N ul ] z >• 01 2 a u E Q E ❑ C Q1u 0 8 1 X'1 ✓ v l 3 4 5 6 8 4 10 11 IN pH Adjustment Log for Preserved Samples Sample 10 Type of Pfeservative pH upon receipt Date preservation adjusted Time preservstlon adjusted Arno unt of Preservative added Lot N Note: Whenever there Is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office {i.e. Out of hold, Incorrect preservative, out of temp, Incorrect containers. Page 154 of 155 F aee,a,iarytkaf• CHAIN -OF -CUSTODY 1 Analytical Request Document wwrr.eruesron The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately. Section A Section 8 Section C of Required Client Information: Required Project Information: Invoice Information: Page 1 Of a Company: HDR ReportTo: Mark Filardi !Charles Gruenberg Attention: 1 Address: 440 S. Church St Copy To: Company Name; Suite 900. Charlotte, NC 28202 Address: Email, mark.filardi hdrin0.com Purchase Order#, Pace Quotes R ulato A e Phone: (704)338-6787 JFax Requested Due Date, Protect Name: OSR Landfill GW Pace Project Manager kevin.herring pace[a6s.com, State !Location Project #: Pace Profile #2568 NC Requested Anal sis Filtered Y!N — z MATRIx CODE COLLECTED Z Preservatives } Prinking Water W�Icr DW WT b V O SAMPLE ID W.,M. W..' S..VS.ONSoIitl WW P SL ! .. � +� � Z N aii aL " .J c� START END One Character per box. wyP WP a (A-Z 0-9! •' Air Pmmc AR p, 0 w C Samplo Ids must be unique Tlas m om ?, o o O x W ,V 4 �0 J PO c �_ Lu u = N C m J U b Q d Q N Q O Q G O N Z U m a O N r DATE TIME DATE TIME e = M= z w m m m r v 0 w � Sl'✓' � �'r � u�y �� �� I I S t 3 I i 1 1 3 a, I I I 3 4 S 6 7 8 9 10 11 12 ADDITIONAL COMMENTS RELINQUISHED BY 1 AFFILIATION DATE TIME ACCEPTED BY 1 AFFILIATION DATE TIME SAMPLE CONDITIONS / Por, t-?i!��� SAMPLER NAME AND SIGNATURE PRINT Name of SAMPLER: U o SIGNATURE of SAMPLER: JC�!, DATE Signed C' ?/J I J _� ter v+ w 1— m y m o y m r y This page intentionally left blank. Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix C — Field Data i dk 4 1 � . 1 i Appendix C — Field Data Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix C — Field Data This page intentionally left blank. 19 Location {N�'�M1 � �—�� Date PI- ect,client fad` 4fJ "� _ - — +'tcei To l��vi+�E H +•� '7 � 4 - A Vy �' + .� � ' � rP � 77 Ire t Ors/ -���;� - - cH If, Cap; ),, � 1� ��1 �I "C;r�Q Vi U • 1 le y a { IV7V o Z7roZ7 N��•—tR c5 �� � � ! � I 20 Location VU'° ^` Project / Client C :N Date cy� vo dr fr . .-.......... �.� �,, �! + c' Location S ^ S��t� +_ Date 65' b 7 "L� Project / Client (26K 22 Location w 1�� �_rj�lP'r. [C.AX, Dite OS � e-az Project r Client—C6L L�►113 G�W��� � 67I a) mA I # 1tC>_ isog ,tad g41,K. Location _ ��F"5 �►�1 10 j1 D1 atL,—c vtItC,Lt 3 Pro�erf I Clien!' _ i K 07w, � G 24 Location W' �d^ SDate Project / Client Mw� 14 n 13�- ti � C13xSF u t. — 10 I i - ss�0-1 Z-1 ,146 Location Project / Client 25 Date HYDROLOGIC DATA SHEET - DEPTH O5/01 II''r 1 R�+ N,, Ep178340 Timc StarlRtl' V ` 'L Time Fini,hi-d Personnel- VN..ies rn onJera Cinnati ira' I f /I! � . Well ID Depth to Total Water btoc) Depth M —4?, =-1a�65' q, 5' Depth to Total Well ID Water (btoc) Depth F�-- Version: 02/13/2020 Sheet t of 11111111111111IN Groundwater Sampling Form Sample ID: m�J ► R Site Information Site Name: OSR Landfill Project Number: 10178340 Site Location: Winston-Salem, NC Sampling Personnel: Charles Gruenberg Date: 0 �10 e d-G Weather: 41,,,A /t, r Well Information Well Diameter (in): Purge Equipment: 6-ee eci (ro zc,441 Po Screened Interval (ft): Type: Ilk L)l, g1(,)1,, Well Depth (ft): Wo 4 Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): Tubing Diameter (in): S /' " Water Column Thickness (ft): Well Volume (ft^3): , -g al. 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): a; SI yi TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) (+/- 0.3) pH (standard units) (±0.11)) TEMP. (C") (3%) COND. (PS/cm) (3%) DISSOLVED OXYGEN (mg/L) (10%) ORP (mV) (±10mV) TURBIDITY (NTUs) (SOY) COLOR/ ODOR (describe) 3 J�j v � Z -X) d '57, � . % U / 6, 1 7 e,a 6 ry A� � 1,531 i !r� I,x zz6 ll ��' �l 5,33, 1S•q 146,} �.3u rA �$�'1 Da ear 0'43 ilk k-4 :�66 S,d 9 IS, :�,16. 0, 61�� 131 I a. "3,G 36,0 V3,14 1-5,9 1,apvQ 6,91 u/rr� I��( Iy� 41 3oc �?�l�J. Sr1- rO AaC'l,/�J q ��.� 0,A,© 0.755 `IPd� 5 7 I r d � (Q �O O S,.4 yI 1� c 6 -1a5 1 /Oc' ' v �/ 0�.0 0,4 C �ea/ 135 4. a, as 1S,9 0.(,5 'd.'I ..1 0,°5,5 Cle-r 140- Ip0� 61.1 ,i,5 1S,j 6.5 --',w,U G-18 C1,*" lye l - 9 . C 3(S6 I S. S a1.2 .3 0.54 ()r b~-1- C (ea I`I it 1,J. I6.ri a 15,4 1 day C!•Sa �k. �►.L' C)r kv Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify 4; / L Sample Information Sample Number Collection Time Parameter Container Preservative My I 1 1 rl Soo M� A JA ysv0 ��,�o,•a4 �� 5v>~� AJ4 S.i�- I��,��'�� XSd HNJ� 10 `1 fi Sd rul N /A {lno N�aH ,� Sampled By: Charles Gruenberg Sample Time: j y15 Date Sampled: 5J04ZU�, Notes: Pumprate= o 13�,$— ^'�r.(Guri('5,q Sampler Signature: �$( ejtjC,'Ji!r tr j(!'ct 2�E AICA NSA A!/A Version: 02/13/2020 Sheet of a 1111111111111IN Groundwater Sampling Form Sample ID: rA 0w1 Site Information Site Name: OSR Landfill Project Number: 10178340 Site Location: Winston-Salem, NC Sampling Personnel: Charles Gruenberg Date: Ci Tj 1 i c=1c Weather: ��� ,. - 6L 1 Well Information Well Diameter (in): �„ � A Purge Equipment: C ea) txti to! 6 Screened Interval (ft): Pump Type: ,,I >�; ),�jlLb� ►r ��n Well Depth (ft): Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): Tubing Diameter (in): " " Water Column Thickness (ft): Well Volume (ft^3): 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter lnstrument(s):,Hz -YS1 TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) (+/- 0.3) pH (standard units) (±0.1) TEMP. (C°) (3%) COND. (µ5/cm) (3%) DISSOLVED OXYGEN (mg/L) (10%) ORP (mV) (±10mV) TURBIDITY (NTUs) (10%) COLOR/ ODOR (describe) t�a. la�l 3�9a !o •611— 1�9 } i� �., I o �l: 0PS3 0.1 a-o (; 1344 1146 T1 Q 1,19 , I 123, 4 " 0C-40 Cq0$ 0- ,,� t/�V /, �Pe 13,14 1 35� G �)r 5D '1-e D(, �.` � , 15 15o Q,-"y —I ,C, 0io4 0g61 ;� S, ISa ,), 13lry 1 35 ;1;, i o,o® C1ati� 0%,XG 15. 5 (0145 I So 1 � 3) 11 12,Co U �-3 - —16s v 10,04 C leke ,nsas 9,311 Cp.j 1 1 13o4 ISGC) 0,�4 —K.1 10,113 Cicci Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; O = Specify Sample Information Sample Number Collection Time Parameter Container Preservative Q iV/ rl Scsti IJ 1A SaGc °' C'S 46,1 C�� 14 Sampled By: Charles Gruenberg Sample Time: Date Sampled: G V/ -Lu2c, Sampler Signature: Notes: Pumprate= a,C M11_ n, rs IC I 'S ( 14 l;')`+2 $f i.., 1 C, 71 tVIA 4 CA � � u r►11►• �` �' `� I� ArSP� �►w s \�ur� C��.I N)A �!rk Version: 02/13/2020 Sheet � Of d, IIIIIIIIIIIIIIIN Groundwater Sampling Form Sample ID: M W -Aip, Purging Information (Page 2) TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH + T0.i4•S WATER (ft_bTOC) pH (standard units) (±0.1) TEMP.. CC) (3Y) COND. (PS/cm) (3Y) DISSOLVED OXYGEN (mB/L) (10%) ORP (mV) (±10mV) TURBIDITY (NTUs) (109�) COLOR/ ODOR (describe) 0, Clc�r G53 ��'W- C5� IS'o 11 f, tic G-30 "-14. , 0,60 cjosb , . alu �,' 5 . �5 tga y, y I �, 1 SG �.3d - J',1 Cli,f Version: 02/13/2020 Sheet I of )-, 111111113"R Groundwater Sampling Form Sample ID: Mw-,K Site Information Site Name: OSR Landfill Project Number: 10178340 :Site Location: Winston-Salem, NC Sampling Personnel: Charles Gruenberg Date: c> S& ( I o Weather: 1.�; ,,� - G" Well Information 'Well Diameter (in): ,L Purge Equipment: ru kk� 17, Screened Interval (ft): Pump Type: Old 1( r Net:! 919 0, joM 02 Well Depth (ft): Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): Tubing Diameter (in): .5 $ �� J Water Column Thickness (ft): 1`3, [ Q .- Well Volume (ft^3): 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; T = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): =54 SI r1� ,,% ry ` TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) pH (standard units) (±0.1) TEMP. (C,) (3%) COND. (PS/cm) (3%) DISSOLVED OXYGEN (mg/L) (10%) ORP (mV) (±10mV) TURBIDITY (NTUs) (10%) COLOR/ ODOR (describe) 5 5 0 360 17 ir. ��C/ ���1! I / a q "��r �lee,- 9 1.4, I' 3Go '353-A li.. 'Sa.y (, i9 Cle�r I'll, PLt 3CO 3��, y! �5 _yd= F `l@z !J, 3„ 7cirr ,S} 1 rely "3G1,� -Ky 065 I,J_ 6,0 36© 3Q5 (o, 19 1316 `3'5',ld 4,.55 -!q 'A- 55 ee,�- OW I., d, }, �, 3a6 3.. __ G, Al 15. 3�W! W G.ay �-35, 0 �! 94 CCet_ r- 0113 1,4, $-" '306 131,55 a. A -k 3,1- -�Pf.0 5.6 —3T.q tA,4w cICq/ C It 14 `i! 566 15,54C.>CS.9 S,1 - .9 5!3 Cj,, h1. 16, j 361 13.E &,d5 113�8 361,+ 5,06 1 -11.5 1 t[,q5 c-1ocr Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative I 5C3:J <;j $.I L�k N 1 dii— SA, C. V0C_If Sampled By: Charles Gruenberg Sample Time: o j s 5 Date Sampled: 6 5A A,4l0 Sampler Signature: k Notes: Pumprate= �3ce(,,) 6TT7 y (i, --Je 7V0C'f %,_,- A42, 51,1s iv, 1(41) W/1 Version: 02/13/2020 Sheet of FIN Groundwater Sampling Form Sample ID: P v-3A Information (Page 2) (Liters) CUMULATIVE VOLUME (Liters) DEPTHPurging TO .. (standard OXYGEN ,. TURBIDITYVOLUME ,, Version: 02/13/2020 Sheet of 0\ lm:)2 Groundwater Sampling Form Sample ID: M Q Site Information Site Name: OSR Landfill Project Number: 10178340 Site Location: Winston-Salem, NC Sampling Personnel: Charles Gruenberg Date: Weather: S,,. —Gr z, Well Information Well Diameter (in): �,i rJ ; : Purge Equipment: Screened Interval (ft): Cj —J,6 Pump Type: bl j,)„ pullp Well Depth (ft): -X6 Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): 1, 91 - 1 Tubing Diameter (in): Water Column Thickness (ft): I , 6 1 Well Volume (fta3): p � 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Hfaing3SI �Ir�a l i�� 1SL TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) (+/-0.3) pH (standard units) (±0.1) TEMP. (C°) (3%) COND. [PS/cm) (3%) DISSOLVED OXYGEN (mg/L) (10%) ORP (mV) (±10mV) TURBIDITY (NTUs) (10%) COLOR/ ODOR (describe) Ll 2'� ecf Il (0106 (3oS 11 list I,J, `1, 'mac! so 6,01 1315 1 115 0%5B( 1 b, y0 1- )11, clic"Or- uS5 I,r), G26 :;0 b 15.39 (.-,.04 13:5 11w G,3-1 6G19 G. &(r 110 30,o G.0 1 13,5 116-1- 0.(00 (,-�o4 ` .14 C-f e0v- 5(o (a. 61 13.5 I /T5 G,sy G.L,d 'i - Git,,/ q,!0 30o 'S,a I G. Oq 13,5 116a 0,56 c,.:9 4..pS C,w I a 1 I I , � (cl , � -saC Spa 6. 13, 5 l IQ' O . `( � L (vj, j 1 D- 5-1-r Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; O = Specify Sample Information Sample Number Collection Time Parameter Container Preservative 06-4-� I �k3 Tej 4114 LISoc 19P xs�h Af/It S-Ak 4 A K,,1;�i� C zro tj-,' , t� S�IG;d� l 1a V"o ACf i, j 10v, By: Charles Gruenberg EDatea Sample Time: pled: 6S%} 3 �,ya Sampler Signature: yf-t,4g4 Notes: Pumprate= 7GL S VO C ;i r,fsI;(;1rf �ti )Gsr Ic,�,^1 Cra� dvlA l� t rfL+c.*bef L CXj) Af(� Version: 02/13/2020 Sheet �— of d 02 Groundwater Sampling Form Sample ID: (VI v Purging Information (Page 2) j . (Liters) DEPTH (ft .. .. .�COLOR/ ,, :. 0. .D. Version: 02/13/2020 Sheet of I M tl,, - S HPGroundwater Sampling Form Sample ID: —Ply'" Site Information Site Name: OSR Landfill Project Number:10178340 Site Location: Winston-Salem, NC Sampling Personnel: Charles Gruenberg Date: () a-}j Weather: S`vn 1 -kjL-� Well Information Well Diameter (in): a,�`y j Purge Equipment:t� Crad,. j r;J Screened Interval (ft): Cp_ �j�} �- Pump Type: 04 4 4 6146 0 Well Depth (ft): Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): 9 ri1 Tubing Diameter (in): y Water Column Thickness (ft): PO, Well Volume (ft^3): 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): BSI fl kko b-Y TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) (+/-0.3) pH (standard units) (±0.1) TEMP. (C,) (3%) COND. (VS/cm) (3%) DISSOLVED OXYGEN (mg/L) (10%) ORP (mV) (±10mV) TURBIDITY (NTUs) (10%) COLOR/ ODOR (describe) 177IS5 © r 91 c 9 ISO i If, z► 9fa �4 [��� t � s.SJ, a65.I 5isG Ili.( 114 Sr Ads.' 0I;k Le 3. W �ca� • q 5. `�3 15. 1 I 6.6 5.5 1 I'5,0 ,5 S< 1 d,0 U• 6 u� J Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; O = Specify Sample Information Sample Number Collection Time Parameter Container Preservative S� 5W GM6A1 �i -?V 5s �f- ¢ Ik,[IIAL AS'o WA ��S ti l 1+ r Cn Sampled By: Charles Gruenberg Sample Time: Date Sampled: 0VC j-/ % LD Sampler Signature: co k}e Notes: Pumprate=(%j Version: 02/13/2020 Sheet � of HP Groundwater Sampling Form Sample ID: l'A w —+ Site Information Site Name: OSR Landfill Project Number: 10178340 Site Location: Winston-Salem, NC Sampling Personnel: Charles Gruenberg Date: �,/�, 3a�-v Weather: 1..--SGs Well Information Well Diameter (in): ;A Purge Equipment: (se,, c,,,44d [ fE Screened Interval (ft): Pump Type: aj �4'4.,d r-S V Well Depth (ft): Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): Tubing Diameter (in): A Water Column Thickness (ft): lr,,,4 I Well Volume (ft^3): ;lL, `j . 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Informat' n Parameter Instrument(s):_�YSI N►;�a� "��,J TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) (+/- 0.3) pH (standard units) (±0.1) TEMP. (C,) (3%) COND. (PS/cm) (3%) DISSOLVED OXYGEN (mg/L) (10%) ORP (mV) (±10mv) TURBIDITY (NTUs) (10%) COLOR/ ODOR (describe) 0994S((�� CI 0 � ';1 5 G,,� S,1 KDA I,�-S S,O mil l 6.1 0, a40 S, 3% IS. 1 IT1,9 0eJ q/7. 1 C(eM1� )953 M 1. kb Is,4 I do•y 0,94 1 od,0 G, 9 eler l5'- Olt "0 IS-4 6 ®- 6 64. "3 G. J 5 C c� 1do5 0,1 4,0 xv 0 C),l lyS.� 0,14 Lies (,0 V,� ye�j �(jfi ^",a,7-� 7ci,'T � le',ja,4, 0.To 1 J.4U 6-,r CIC,-/ 16 I J,5.'i i W. I 36 l4 . 1 0.,15 C 10I} 0,9 CS. 0,"34 a6i1, LI<<r I(JA1 o.Sl D—C4"�- trl�,;� Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative 163S -1-05 �1 spas ,1 fvr& IV, bit $a60 voc,f � 1 �Al Sampled By: Charles Gruenberg Sample Time: (� 3S Date Sampled: ]Sampler Signature: Notes: Pumprate= �,,.I�r (1 `i 5 $C$1 9� Pq tocif►l �� (X") Version: 02/13/2020 Sheet Z. of FNGroundwater Sampling Form Sample ID: (n k/'-- Purging Information (Page 2) TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) pH (standard units) (±0.1) TEMP. (°C) (3%) COND. (µ5/cm) (3%) DISSOLVED OXYGEN (mg/L) (10%) ORP (mV) (+10MV) TURBIDITY (NTUs) (10%) COLOR/ ODOR (describe) S�),G IS,y iq`Iro t version: 02/13/2020 Sheet ) of I F�2 Groundwater Sampling Form Sample ID: ! ' k/ 4 Site Information Site Name: OSR Landfill Project Number: 10178340 Site Location: Winston-Salem, NC Sampling Personnel: Charles Gruenberg Date: d 51,a j ,,.2a Weather: Well Information 'Well Diameter (in): Purge Equipment: Cfporrc 6y f 0 Screened Interval (ft): -�- �� Pump Type: /91ti Well Depth (ft): a. l Pump Depth (ft-bTOC): r Depth -to -Water (ft-bTOC): Tubing Diameter (in):J�B 'Water Column Thickness (ft): r f, 63 lWell Volume (ft^3): p 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s):, I J1 '.Lfe Ad TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) (+/-0.3) pH (standard units) (±0.1) TEMP. (C') (3%) COND. 41S/cm) (3%) DISSOLVED OXYGEN (mg/L) (10%) ORP (mV) (±10mV) TURBIDITY (NTUs) (10%) COLOR/ ODOR (describe) less v a and g'ST , I6,o `r, 74- Y 6.46 41 1340 110 I,D 10d 4.5( 1,43 1ka U,1 6,55 ').66,7 65 Cle41 �3`�5 f -U a„d a00 9rSS �,' [lD � �3•a (,.ab �,,4 I1�68 �f� 550 1-5 77. 30v •y5 15-S 415MIA 60 LIev 1-555 t,5 G..d Soo 1 „J.6 ts,[ qvi S.. S I- a, 0401 Cloy/ 110b 1 6,5 '306 9.61 4114 1S. 16.4 5a1-1- 304.5 G'Q3 t,1e41- 1401F I.5 ;,0 ?,od 1, qk 1 1150 IS. 01 oe 306, JL 1.49 0-tee„- 1410 (,5 1, 300 q,4.5 '1•'4, 15.d. q ,6 1 4,1 30 ,� cs.ta, C10'r- 1415 1•5 11,0 1,66 9.'i� f{," 15, t,` S,4 `3 6 C;, S Zia, ,,. (,APhL Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative �/� /" 1 I_ i_(� ( �V b 14 36 -70 7 PSI 5aa "� N �010 ./ o col �50.�1 IINa s 0 J C�916r �dl a�L N14 ,,,;Je of 14.SML Ne.o14 SDI At A11<,I;k;t .( a56Ac N 511 Vk1k f'o1 ue"c N„014;t zt �.6a VO(A Gr6j 46,,L GO I4-CL Sampled By: Charles Gruenberg I Sample Time: `13a Date Sampled: [)!5/0 -.2,0 1 Sampler Signature: A,e,,� II Notes: Pumprate= a a �`Jh � ►'L35 10 6 I S5® Version: 02/13/2020 Sheet 6 of KR Groundwater Sampling Form Sample ID: N1 V- I Site Information ;Site Name: OSR Landfill Project Number: 10178340 Site Location: Winston-Salem, NC Sampling Personnel: Charles Gruenberg -Date: 6 �/,s5 f.L61+ Weather: 0, , j . , Well Information 'Well Diameter (in): Purge Equipment: �� @�l, 6-e, e„ sal rr�s Screened Interval (ft): 5° 46,6 .�} Pump Type: apd;(,a1j)✓ 'Well Depth (ft): I• Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): c Cy . } Tubing Diameter (in): 3Ji" Y 'Water Column Thickness (ft): 1133, lWell Volume (ft^3): (� 5; 5 64 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; T = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): ar 1 14iLf6 �v TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) (+/- 0.3) pH (standard units) (±0.1) TEMP. (C°) (3%) COND. (PS/cm) (3%) DISSOLVED OXYGEN lm%) (10%) ORP (mV) (±10MV) TURBIDITY (NTUs) (10%) COLOR/ ODOR (describe) iv I 0 0 100 So..3, Lj,•• v Is, I%-1, I ,t'} �1 0.�' Cle, r- 0Cke 1,`D` d00 So.3S `t, 4+ I5.. 1. I1.5(1 9.dQ a.`y3a v`0 3�. C/le.f- .K5 I.0 yI.b/ AeV Aa0 5035 4. l7 1 '( 7./ isly $,6 1 ZJ4.to Ve C.+1QG.� 1.0 110 .100 50,36 `I.�}lrr_ ICS, i 1 d$•I cl. j -4,41,4 C�. 5 q C-jr�Rr y6 14$ 0 1r© G,0 --46 ?0.3T q q 15.4 10-6 q'00 a-�8• p 1.17 Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; O = Specify Sample Information Sample Number Collection Time Parameter Container Preservative T05 rol 566 MI / eWorlh 4s06 lidI �50 N I A a 11r6 ei `aS� JAI Ned 1+ d Z. �S rl maH 51G0 Voe- 40A,16 )t<l Sampled By: Charles Gruenberg Sample Time: U ' $ Date Sampled: Sampler Signature: P---, Notes: Pumprate= a00mL®,,, p 0 % IS V--� c version: 02/13/2020 Sheet of I IIIIIIIIIIIIN Groundwater Sampling Form Sample ID: J , /o Site Information Site Name: OSR Landfill Project Number: 10178340 Site Location: Winston-Salem, NC Sampling Personnel: Charles Gruenberg Date: 0 5 0 5 ,- a ;k0 Weather: R'o ' Well Information Well Diameter (in): �ks U Purge Equipment: Cr',�4 ,c &t,6,4'1 rro Screened Interval (ft): G, 0 - 1,1,0 Pump Type: OtJ;teli,) f31sd�v Well Depth (ft): 3,11 0 (- Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): 10l- Tubing Diameter (in): Water Column Thickness (ft): I G . lWell Volume (ft^3): f. 6 9 ag 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter lnstrument(s): SI- en,Cre ?tA/ ys TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) (+/- 0.3) pH (standard units) (±0.1) TEMP. (C,) (3%) COND. (µS/cm) (3Y) DISSOLVED OXYGEN (mg/L) (SOY) ORP (mV) (±10mV) TURBIDITY (NTUs) (SOY) COLOR/ ODOR (describe) [150 0 U 3a 6 )Q, d. I G. 11 1 J. d ) 0 5 & _S3 — 53.1} 11, - CIO,, 1s5 I.5 ) S -500 10.sl , ,b rvo -a. to - 3.1 ► , 11 c:lP,./ IJ.Go I,s 0 G 16," lull 1.41 _�d, ` , V CIPI/ 1aG5 I•S S 3co I'•1b,1 ("45 1 ,6 141b 0,91 —11.6 4.45 */ [a.10 I,5 6,0 300 o.$d `.�5 14,5 1115 p.50 - 3. 5,10 Clc,,f IJ•I5 1-5 -S Sao 6� L.A ,55 1}11 G.65 -t16 ,d4 I2.d 1;o 1, 9,0 'SGO 16, �5 14,5 116 Cf. Sl — S+p6 laa; 1,5 10.5 300 16, � 1 6.4 1 ,5 110 0, 5`� —,%% Ir4( ta3o 115 1 a,0 -lod 6 6. a _%1. a�r6 - CIQ� Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative F d3eclv Sand I WA- s�r�ktt1({ 4 S 0 r`f1 Q 1 L50 �pl� : aS�i M I NNd A- e J fs)in/ lLl 0.1& tI Sampled By: Charles Gruenberg Sample Time: 1','5 Date Sampled: G S GS .jaLd Sampler Signature: Notes: Pumprate= >OG M VM e t [ Sa �0 �, II f S�� �i��5 we, I'm tc bJ (al N//} Version: 02/13/2020 Sheet � of )- 11111111110)2 Groundwater Sampling Form Sample ID: ry- 1 I Site Information Site Name: OSR Landfill Project Number: 10178340 .Site Location: Winston-Salem, NC Sampling Personnel: Charles Gruenberg Date: % ,16 10 Weather: Z 1cj j / .C,. Well Information Well Diameter (in): ,� , 0 ;1 Purge Equipment: �p�,, c.� Cs-�� G>� ,�( re Screened Interval (ft): , p — Z .0 Pump Type: Ji" fc4 Jbir r . Well Depth (ft): a(j, Q Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): 15. Tubing Diameter (in): '�,� y z- � Water Column Thickness (ft): j Ig. 55 Well Volume (ftA3): 4 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): Kanxsa--,2YSL �C=a ' s TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) (+/-0.3) pH (standard units) (±0.1) TEMP. (C') (3%) COND. (µS/cm) (3%) DISSOLVED OXYGEN (10%) (m%) ORP (mV) (±30mV) TURBIDITY (NTUs) (10%) COLOR/ ODOR (describe) o-% 6 ^>, S6 `, 1400 "31 •5 S,So 10,4,6 Oec", .0-K5 1.6 U 0 '3151 S40 1+0 ads •( I. , b - $, T- i=54 Cl&', Di►oo ��o �.,o a�a 3,sd ,o g,� �,5) i' .� �S,o�1 c ►��� 0405 i , '3. ;.o 0 3. 5 r - NO M9 .5 -1. 0 " . 0 • � 9 GI,QGI (3�10 ko yqc ao(j "�, 55 .6 140 `i3,6 1 � fo, �, .� � C Iget- o`6i5 t,b S,b ei0 A 4 5,QL l s(1 '544- t,6 -3, + 'S o� Cl�dr 1.0 Gay d0 �a. a-1- S,6 1 ,6 3`i�,�, U, b ,0 •q 4 ls'6 1,0� .0 8 (� <S 5,('3 I`y�ob .- ,� -1, 5', Ci0c r JJ�� �3�9 /5�1 0%-315 1101 1,6 -,66 0t61 4, —4- 3.a 6 CIef Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time , Parameter Container Preservative p/1 0yv�5. 7hS �I oc n �} Srl e All(�I��i 1 to e-I N 4 So e.i h, A 0 15'r; ,� I airs / rl. �.SvI 1+.Aid TI or,I. ure, ,Na®1 MOW ¢ U Q 0 s Sampled By: Charles Gruenberg Sample Time: 1 Date Sampled: C6 dukd Sampler Signature: ACn! q� th Notes: Pumprate= aW,1/, l; C,�So k--, Version: 02/13/2020 Sheet I of HPGroundwater Sampling Form Sample ID: h �/-\l Purging Information (Page 2) VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED RGE. (MIATE .1mi WATE .. (standard units) TEMP. ( oc) COND.TO (PS/cm) I OXYGEN (mg/L) 0. (MV) TURBIDITY NTUs) (10% COLOR/ ... Version: 02/13/2020 Sheet of Groundwater Sampling Form Sample ID: PAO- Site Information Site Name: OSR Landfill Project Number: 10178340 Site Location: Winston-Salem, NC Sampling Personnel: Charles Gruenberg Date: OS d4Je7.63.6 Weather: n- 7o G Well Information 'Well Diameter (in): _J.,0 Purge Equipment: &etjrA �a�Lo7`fr61 �6 Screened Interval (ft): , b Pump Type: W ; C,,110),1 (V Well Depth (ft): Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): � , Tubing Diameter (in): /�$ `� Y ll j. ' Water Column Thickness (ft): 11,0 K Well Volume (ft^3): tt 3 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s):`�-5l (0 Tr6j ysr TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) (+/- 0.3) pH (standard units) (±0.1) TEMP. (C") (3%) COND. (PS/cm) (3%) DISSOLVED OXYGEN (m%) (10%) ORP (mV) (±10mV) TURBIDITY (NTUs) (10%) COLOR/ ODOR (describe) leAd 0 d a00 y=T, G-0 1160 66- 1 lq.� W4 ci2t,,_ 146 avd . 6, to 14,b lob 3. 0 % 1,44 aar to q 0ei I.1i -,deg 4eTj, 6,14 4e5 10--,�a a,% S1,0 4,56 e-'«,- 16-173 aeb aoa `,.4 6.15 11.6 (o. 301 4S.1 Cie., 103�- ro1.q O.�d 3e AQa `fie T3 , Ifp 1`i. 1814 1.0 41,l1 (�,445 -1,q6 cle.( 1041 4045 C).<� 5,0 4,4-4 d1e1 44C c,5 6. xoa 4,W G.1 14,.-jot 0 10511 0.1 `+. a6d 4 _,Tj 1 6, I ry' 16 . 06 �G, 0.44 CI oc,,- Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; O = Specify Sample Information Sample Number p Collection Time Parameter Container Preservative VIA Uct c wAl a -at- NA C A0bg � �� .l (Z�TI �9o1�4r!•hk U06 S Sampled By: Charles Gruenberg Isample Time: 1.15 Date Sampled: QS 66f ).Q Lu I Sampler Signature: C Notes: Pumprate= p� nllh /1 toiz Version: 02/13/2020 Sheet r, Of �kl Groundwater Sampling Form Sample ID: MU-11 Purging Information (Page 2) TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO ty,3 WATER (ft-bTOC) pH (standard units) + (_01) TEMP. CC) (3%) COND. (µS/cm) (3%) DISSOLVED OXYGEN (mg/L) (10%) ORP (mV) (±10mV) TURBIDITY (NTUs) (10%) COLOR/ ODOR (describe) rOi 0100 q.a_ Nv4) 4-13 &&li' I A 1G64 0` 1 5�� 3 ().60 *.Cr C�. i1 0 5 o" i q , l7 00 9,i6 �j b � e 1 p l a ®a y V �/51 1f 0.01 �� Qatr % /(1� u j�61 1113 15114 (6•0 �%w 14A toss a.-YA ss.`( o.00 Lleor 11l .I k�� o �1Y•9 (i.o� rrlegr Version: 02/13/2020 Sheet of Groundwater Sampling Form Sample ID: Site Information Site Name: OSR Landfill Project Number: 10178340 Site Location: Winston-Salem, NC Sampling Personnel: Charles Gruenberg Date: 0516G12-O LO Weather: �- s Well Information Well Diameter (in): Purge Equipment: Screened Interval (ft): 5rU Pump Type: ()Yj ,:" �w (,; I,) v" Well Depth (ft): ao,() Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): Tubing Diameter (in):/ Water Column Thickness (ft): Well Volume (ft^3): i . 9 `1 l 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s):" a�,1V51 N" ,4 SL TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) (+/-0/.3) pH (standard units) (±0.1) TEMP. (C°) (3%) COND. (µ5/cm) (3%) DISSOLVED OXYGEN (mg/L) (10%) ORP (mV) (±10mV) TURBIDITY (NTUs) (10%) COLOR/ ODOR (describe) r, HIV V , I S . ° I 14 Lo I>0 Jh6 S,31 10�. C'K0 4.a� 14, l�,�Ok,- �i 1�14 6� ad ci 7d p )e j �.� 14,1 1 >. 2 , 7 0.11 cr�Z� U4 013 �,,q �,iyz- IAA, 5, -ki i I .1 53.5 0.9. Cl�a� 1� GIq 31b add S11 6 1 5,X. 14.1 3,ij I i .3 in CIac.", M o,q 4.1 Aob -5I 545 14.3 1, 3,-S I i.,a-1, n, si Clexr (6�4 a►ri S,X asu& q.53, 4.J,3 I. 6,34 Ctocr 'J.h-k G.-Q G, 014 ," �. 5��� (4.1 113,j 6,qj 0.9g c j&�,- Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative T1JS �1 San,�l ill LI Aj 6G Lo RAM. Ifo %,10 NGI :Sampled By: Charles Gruenberg ISample Time: 1j s S Date Sampled: ISampler Signature: 4k Notes: Pumprate= �;o ,,I/r, e ('.(0 ,),Go Mlr., 0 tJ,j,�_ Version: 02/13/2020 Sheet ) of i FIN Groundwater Sampling Form Sample ID: MV -11 Site Information Site Name: OSR Landfill Project Number: 10178340 ,Site Location: Winston-Salem, NC Sampling Personnel: Charles Gruenberg Date: D 5 0 S% o J-o Weather: C GJ Well Information 'Well Diameter (in): a,6 Purge Equipment: 6-eo .t c :Screened Interval (ft): IS, 0 -- (,G , 0 Pump Type: OkJ;4js j J31; 1/ Well Depth (ft): (�b, o �+ Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): So. I Tubing Diameter (in): '>f ��� )�r .-I 'Water Column Thickness (ft): `f, S S( Well Volume (ft^3): S<jo $ 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): 44aaaa=Y!jI M ; c , 6 T N-J YST TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) (+/-0.3) pH (standard units) (±0.1) TEMP, (C") (3%) COND. (PS/cm) (3%) DISSOLVED OXYGEN (mg/L) (10%) ORP (mV) (±10mV) TURBIDITY (NTUs) (10%) COLOR/ ODOR (describe) �950 0 aao So. 3; y�`lo 15.y 14S.3 6, 13 a-:�,6 IG-16 c1e« 0955 Lo 1,0 �),o0 1;6.3G IS.; M.3 a. 14, XWC Go 3I Cltcr 1660 1 a,, 3" _r-01 44 Li. 9d► Is. 3 1%, .0 5 360.0 a 5.16 CIttr 100 ►,S $o 2,00 o.H3 4. ISm IU.3 1•44 3o3.I O.0 Cie,r to to I.S S, S �te,o So.yS 4 �d IS, 19�. b t.5 �aa.0 V. Sal Gets ►o15 1.5 1,p 1,00 so.`1 Is.y ►96.4 0. 9 Clett- Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative W-5 10S 01c1,4 J;06 �,1 N114 al d N1 4 4I K,I,'i, 3• "14 Ng /l e 'a`SG 14i 1 'I N( 014 01 �o ^1 ND �,► ;d bl Id- rI IVA04 4 p 0 L :1.6u 1w 40,1 LD W-1 :Sampled By: Charles Gruenberg Sample Time: 16 J, Date Sampled: 0 S a Sampler Signature: Notes: Pumprate= Jdr) C Cj 9So V 30c, Q I'vo Version: 02/13/2020 Sheet I of 4 1=)2 Groundwater Sampling Form Sample ID: fA v" (5 Site Information Site Name: OSR Landfill Project Number: 10178340 Site Location: Winston-Salem, NC Sampling Personnel: Charles Gruenberg Date: 6 /,� ,�� �� Weather: 5VIAA �_ SO Well Information Well Diameter (in): A .o j Purge Equipment: (� Screened Interval (ft): Pump Type: Well Depth (ft): Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): 15 444 Tubing Diameter (in): Water Column Thickness (ft): I C). ' Well Volume (ft^3): 1 Well Volume = (Total Depth - Static Water Le% Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = Purging Information Parameter Instrument(s): am SI TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) (+y/--�0.3) pH (standard units) (±0.11) TEMP. (C°) (3%) CW (µS/i (39 + .�y (0AI I • U 1.0 �).sb � I . I t,c 1;Sic V� � I . a.e0 m-0 l� 31,C, ,14 ( 1 N• 74 ick .4 A06 31,51 6,0 --, S� 1015 1.0 e 0 31.5W 0.14 I t ®�o ('a 5-1 l,^ v 2 J1.5 6,1 I T,9 46, 10,;5 I'd �a a ad --�C1,54 1D fj10 q5 106 ;q.56 o i 3igY 11110 LIL 15S . Je ? g1�• 1 �1 1 r0 yGi Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Su Sample Information Sample Number Collection Time Parameter I'ISU w; 60(v / 1114-0 s.,► 'fie Sampled By: Charles Gruenberg ISampleTime Date Sampled: 0 )-G ISampler Sign Notes: Pumprate= �Vy0 h(�ti C� S iSj ii�b,6) k Luc ple, C 10,10 %GGj 11016 �)40 Version: 02/13/2020 Sheet I)L of A- IMN Groundwater Sampling Form Sample ID: ('� l,.J- f 5 Purging Information (Page 2) PURGED (Liters) I CUMULATIVE VOLUMEVOLUME PURGED (Liters) • WATEFjjj .. units) CC) W/crn) • (mg/L) 0. (MV) TURBIDITY (NTUs) (10%) ODOR Version: 02/13/2020 Sheet of IIIIIIIIIIIIN Groundwater Sampling Form Sample ID: 5w— Site Information Site Name: OSR Landfill Project Number: 10178340 Site Location: Winston-Salem, NC Sampling Personnel: Charles Gruenberg Date: d g4 ,1u- Weather: �. (,(j Well Information Well Diameter (in): AIIA Purge Equipment: /V Screened Interval (ft): IL'MA Pump Type: Well Depth (ft): Pump Depth (ft-bTOC): ,N Depth -to -Water (ft-bTOC): Tubing Diameter (in): Water Column Thickness (ft): /- Well Volume (ft^3): 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; T = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s) a�x a, SI M(zr► Tov TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) (+/- 0.3) pH (standard units) (±0.1) TEMP. (C,) (3%) COND. (µS/cm) (3%) DISSOLVED OXYGEN (m%) (109'0) ORP (mV) (±10mV) TURBIDITY (NTUs) (10%) COLOR/ ODOR (describe) Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative J l t3156 1-05 1 N/ l S.o e -'T l. 4IV AI! %O.d + V O 6010 Z rC c �„' �� 15 w- N'' .lt % �(b UO( j k� / w 1i�1n� 1. 11R Rt. Sampled By: Charles Gruenberg Sample Time: 1 �.j0 Date Sampled: d d J,,, Sampler Signature: ^ kco-(-1c Notes: Pumprate= Version: 02/13/2020 Sheet t of FN Groundwater Sampling Form Sample ID: 51+/ a, Site Information Site Name: OSR Landfill Project Number: 10178340 Site Location: Winston-Salem, NC Sampling Personnel: Charles Gruenberg Date: OS/cS XoI6 Weather: 61,,,a Purging Information Parameter Instrument(s): 449"namY91- M ",10 TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) (+/- 0.3) pH (standard units) (±0.1C)1 TEMP. (C') (3%) COND. (PS/cm) (3%) DISSOLVED OXYGEN (m (10%) ) ORP (mV) (±10mV) TURBIDITY (NTUs) (10%) COLOR/ ODOR (describe) F 15. Q �J Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Cor ll Oo C Ia 4 1 ej ! Vo(_'t 4 r Go 10 ,/ 71 1 16a U0 C- J Sampled By: Charles Gruenberg Sample Time: 14 35 Date Sampled: 05 0 �o Sampler Signature: Notes: Pumprate= N/A Qwc fat? lj, o f Version: 02/13/2020 Sheet I of I FN Groundwater Sampling Form Sample ID: S�/'3 Site Information Site Name: OSR Landfill Project Number: 10178340 Site Location: Winston-Salem, NC Sampling Personnel: Charles Gruenberg Date: O j -U" Weather: ( LJ Well Information Well Diameter (in): Purge Equipment: AIZA Screened Interval (ft): Pump Type: A_ Well Depth (ft): Pump Depth (ft-bTOC): Depth -to -Water (ft-bTOC): Al A Tubing Diameter (in): AVIA Water Column Thickness (ft): Well Volume (ft^3): AI A 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; T = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s): =YS1 l"In) -Tlr(j Yr,t TIME VOLUME PURGED (Liters) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) (+/ 0 3) pH (standard units) (±0.1) TEMP. (C,) (3%) COND. (µ5/cm) (3%) DISSOLVED OXYGEN (mg/L) (10%) ORP (mV) (±10mV) TURBIDITY (NTUs) (10%) COLOR/ ODOR (describe) 110 1,65 —11 5 o &I Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative TO �� Soy 1 I V 4 too,I V 4 4,500 c4 (o A P, l M W 1p 0 pory 1S6 m 4 Al b [ a c a-S r- ( Al o l �.S �. I 614 ,lV� i/ pp 7& k Sampled By: Charles Gruenberg Sample Time: Date Sampled: v i,,riA Sampler Signature: Z;'c ot«h4 Notes: Pumprate= VIP- Version: 02/13/2020 Sheet J_ of Groundwater Sampling Form Sample ID: S h/ Site Information Site Name: OSR Landfill Project Number: 10178340 Site Location: Winston-Salem, NC Sampling Personnel: Charles Gruenberg Date: Weather: C4,,,d 'tom 66e Well Information Well Diameter (in): ,v 1A Purge Equipment: AIJA Screened Interval (ft): Pump Type: N A Well Depth (ft): , A Pump Depth (ft-bTOC): N Depth -to -Water (ft-bTOC): IVIA Tubing Diameter (in): WA 'Water Column Thickness (ft): !n / Well Volume (ft^3): , 1 Well Volume = (Total Depth - Static Water Level) * Well Capacity Well Capacity (gallons per feet): 0.75" = 0.02; 1" = 0.04; 1.25" = 0.06; 2" = 0.16; 3' = 0.37; 4" = 0.65; 5" = 1.02; 6" = 1.47 Purging Information Parameter Instrument(s):.Hi (`� ii�a `r (►L. TIME VOLUME PURGED (Liters) ) CUMULATIVE VOLUME PURGED (Liters) PURGE RATE (mL/min) DEPTH TO WATER (ft-bTOC) (+/- 0.3) pH (standard units) (±0.1) TEMP. (C°) (3Y) COND. (µ5/cm) (3Y) DISSOLVED OXYGEN (10�) (mg/L) ORP (mV) (±lOmV) TURBIDITY (NTUs) (109�°) COLOR/ ODOR (describe) Purging Equipment Codes (circle): B = Bailer; BP = Bladder Pump; ESP = Electric Submersible Pump; PP = Peristaltic Pump; 0 = Specify Sample Information Sample Number Collection Time Parameter Container Preservative S i �)5 ; S Al, So,I / /1. II �1a�Q 1I y+�/ ,I aSd ti l /V%A. [[ (` o _,,t C r,x I'll .j s4o Vo C rs cry J I c f 4 n l Sampled By: Charles Gruenberg Sample Time: I' Date Sampled: 0-r%LlfjJ-G Sampler Signature: 4(10, Notes: Pumprate= Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix D — Electronic Files Appendix D — Electronic Files Portable document format (PDF) of this report Electronic data deliverable (EDD) of groundwater results r i L J Winston-Salem/Forsyth County Utilities I Old Salisbury Road Landfill Assessment Monitoring Report ��� Appendix D — Electronic Files This page intentionally left blank. FN HDR Engineering, Inc. of the Carolinas 440 S Church Street, Suite 1000 Charlotte, NC 28202-2075 704.338.6700 NC License F0116 hdrinc.com © 2020 HDR, Inc., all rights reserved