RA-2695_16861_CA_O_20200206

February 6, 2020

Mr. Mark Petermann
NCDEQ, Division of Waste Management, UST Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Reference: Letter Report – Former Brown’s Service Station
29 Lewis Brown Road
Bennett, Chatham County, North Carolina
NCDEQ Incident: 16861
NCDEQ Contract: N17006
ECS Project: 49:6218-C

Dear Mr. Petermann:

As authorized by your acceptance of ECS Southeast, LLP (ECS) Task Authorization Request #4 (TAR #4)
dated November 20, 2019 and authorized on November 25, 2019, ECS has completed the Letter Report
for the Former Brown’s Service Station (Figure 1 and Figure 2). Included in this report is a description of the
field activities, the results obtained, and our conclusions and recommendations.

On December 18, 2019, ECS was contracted to collect a field blank and a groundwater sample from
water supply wells WSW-1 and WSW-2 for laboratory analyses. A summary of available water supply
well information is provided in Table 1 and locations of previously identified water supply wells is
depicted on Figure 3.

Laboratory analysis reported methyl tert butyl ether (MTBE) concentration above its North Carolina 2L
Groundwater Quality Standard (NC2LGWQS) but below its Gross Contamination Level (GCL) in the
groundwater sample collected from water supply well WSW-1. Laboratory analysis reported diisopropyl
ether and 1,2-dichloroethane at a concentration above its laboratory reporting limit but below its
NC2LGWQS in the groundwater sample collected from water supply well WSW-1.

Laboratory analysis reported ethanol at an estimated concentration, denoted with a “J” flag above the
laboratory reporting limit in the groundwater samples collected from water supply wells WSW-1, WSW-2,
and the Field Blank. Ethanol was not analyzed during the previous groundwater sampling events. The field
blank was collected using laboratory provided deionized water.

ECS inquired with the laboratory to determine if the ethanol detections were accurate. The laboratory
confirmed ethanol was reported with a J flag which indicates it is an estimated concentration reported
below the reporting limit. Therefore, it is possible the detection of ethanol was introduced in the
laboratory and/or in the field. Since only ethanol was reported in water supply well WSW-2 and the field
blank, it is ECS’s opinion the ethanol detections is considered to be a laboratory contaminant.

A summary of analytical results is provided in Table 2, and a copy of the laboratory analytical report as well
as chain of custody is attached. Based on the results of this groundwater sampling event and previous
SOURCE:
USGS TOPOGRAPHIC MAP
BENNETT
NC QUADRANGLE
DATED 1968
SCALE: 1” : 24,000”
FIGURE 1
SITE LOCATION MAP
FORMER BROWN’S SERVICE STATION
29 LEWIS BROWN ROAD
BENNETT, CHATHAM COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: 16861
ECS PROJECT: 49:6218-C
SITE
FIGURE 2
AERIAL SITE MAP
FORMER BROWN’S SERVICE STATION
29 LEWIS BROWN ROAD
BENNETT, CHATHAM COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: 16861
ECS PROJECT: 49:6218-C
SOURCE:
CHATHAM COUNTY GIS
DATED 2013
SCALE AS SHOWN
SITE
AGRICULTURAL
1 inch = 70 feet
WOODED UNDEVELOPED
AGRICULTURAL
Approximate
Location of the
Former Brown’s
Service Station
Building
LEGEND
Approximate Location of Former USTs
Approximate Location of Former
Dispenser Island
Water Supply Well Location
WSW-1
WSW-1
SOURCE:
CHATHAM COUNTY GIS
DATED 2013
SCALE AS SHOWN
FIGURE 3
WATER SUPPLY WELL LOCATION MAP
FORMER BROWN’S SERVICE STATION
29 LEWIS BROWN ROAD
BENNETT, CHATHAM COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: 16861
ECS PROJECT: 49:6218-C
LEGEND
Approximate Location of Water Supply Well
500 ft. Radius
1,000 ft.
Radius
SITE
WSW-2
WSW-1
1 inch = 400 feet
WSW-1
Water Supply Well ID Well Owner / Address Well Address Well Use Well Depth
(ft bgs)
Type of
Well
Approximate Distance
from Source Area of
Release (ft)
Mr. John Dooley (Subject Site)
6272 Carl Cox Road 29 Lewis Brown Road
North Carolina 27208 Bennett, North Carolina 27208
Mr. Aubra & Billy Davis
1471 Bennett-Siler City Road
Bennett, North Carolina 27208
Notes:
ft = feet
WSW-2
Sole-Source Unknown Drilled Approximately 175 ft west
Sole-Source Unknown Drilled Approximately 450 ft east
ft bgs = feet below the ground surface
Table 1
Water Supply Well Survey
Former Brown's Service Station
29 Lewis Brown Road
Bennett, Chatham County, North Carolina
ECS Project: 49:6218-C
NCDEQ Incident: 16861
WSW-1
1471 Bennett-Siler City Road
Bennett, North Carolina 27208
Sample ID Sample Date
2/15/2010 BRL 1.2 15.6 NA
10/31/2014 1.0 2.0 56.0 NA
7/17/2015 1.2 2.0 51.4 NA
4/12/2018 BRL 0.71 17 NA
11/1/2018 1.2 1.2 27.3 NA
7/10/2019 BRL 1.0 25 NA
12/18/2019 0.55 0.95 25 40 J
10/31/2014 BRL BRL BRL NA
7/17/2015 BRL BRL BRL NA
4/12/2018 BRL BRL BRL NA
11/1/2018 BRL BRL BRL NA
7/10/2019 BRL BRL BRL NA
12/18/2019 BRL BRL BRL 24 J
Field Blank 12/18/2019 BRL BRL BRL 34 J
20 70 20 4000
20,000 70,000 20,000 4,000,000
Notes:
NC2LGWQS = North Carolina 2L Groundwater Quality Standard as of April 1, 2013
GCL = NCDEQ's Gross Contamination Levels for Groundwater as of April 1, 2013
(µg/L) = Micrograms per Liter
BRL = Below Reporting Limit
Bold = Detected above the NC2LGWQS
NA = Not Analyzed
J = Detected but below the Reporting Limit; therefore, result is an estimated concentration
NCDEQ Incident: 16861
NC2LGWQS (µg/L)
GCL (µg/L)
ECS Project: 49:6218-B
Analytical Method
Contaminant of Concern 1,2-DichloroethaneDiisopropyl etherWSW-1
WSW-2 EthanolEPA Method 6200B (µg/L)Methyl-tert-butyl etherTable 2
Summary of Current and Historical Groundwater Analytical Results
Former Brown's Service Station
29 Lewis Brown Road
Bennett, Chatham County, North Carolina
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
December 30, 2019
Matt Gillis
ECS Southeast - Raleigh, NC
9001 Glenwood Avenue
Raleigh, NC 27617
Project Location: Bennett, NC
Client Job Number:
Project Number: 49:6218-C
Laboratory Work Order Number: 19L0903
Enclosed are results of analyses for samples received by the laboratory on December 19, 2019. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 22
Table of Contents
Table of Contents
Sample Summary 3
Hits Only Report 4
Case Narrative 5
Sample Results 6
19L0903-01 6
19L0903-02 8
19L0903-03 10
Sample Preparation Information 12
QC Data 13
Volatile Organic Compounds by GC/MS 13
B248979 13
Flag/Qualifier Summary 17
Certifications 18
Chain of Custody/Sample Receipt 20
Page 2 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
12/30/2019
ECS Southeast - Raleigh, NC
9001 Glenwood Avenue
Raleigh, NC 27617
ATTN: Matt Gillis
49:6218-C
19L0903
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Bennett, NC
WSW-1 19L0903-01 Water SM21-22 6200B
WSW-2 19L0903-02 Water SM21-22 6200B
Field Blank 19L0903-03 Field Blank SM21-22 6200B
[TOC_1]Sample Summary[TOC]
Page 3 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19L0903-01WSW-1
DL
1,2-Dichloroethane 0.55 0.50 g/L SM21-22 6200B0.41
Diisopropyl Ether (DIPE)0.95 0.50 g/L SM21-22 6200B0.17
Ethanol 40 50 g/L SM21-22 6200BJ11
Methyl tert-Butyl Ether (MTBE)25 0.50 g/L SM21-22 6200B0.25
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19L0903-02WSW-2
DL
Ethanol 24 50 g/L SM21-22 6200BJ11
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19L0903-03Field Blank
DL
Ethanol 34 50 g/L SM21-22 6200BJ11
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 4 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
[TOC_1]Case Narrative[TOC]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 5 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/19/2019
Work Order: 19L0903Sample Description:Project Location: Bennett, NC
Sample ID: 19L0903-01
Field Sample #: WSW-1
Sample Matrix: Water
Sampled: 12/18/2019 13:00
[TOC_2]19L0903-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 12/24/19 16:56 LBDg/L3.8 12/24/19SM21-22 6200B1Acetone
ND 0.50 12/24/19 16:56 LBDg/L0.18 12/24/19SM21-22 6200B1Benzene
ND 0.50 12/24/19 16:56 LBDg/L0.15 12/24/19SM21-22 6200B1Bromobenzene
ND 0.50 12/24/19 16:56 LBDg/L0.32 12/24/19SM21-22 6200B1Bromochloromethane
ND 0.50 12/24/19 16:56 LBDg/L0.16 12/24/19SM21-22 6200B1Bromodichloromethane
ND 0.50 12/24/19 16:56 LBDg/L0.46 12/24/19SM21-22 6200B1Bromoform
ND 2.0 12/24/19 16:56 LBDg/L0.78 12/24/19SM21-22 6200B1Bromomethane
ND 5.0 12/24/19 16:56 LBDg/L1.9 12/24/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 12/24/19 16:56 LBDg/L0.21 12/24/19SM21-22 6200B1n-Butylbenzene
ND 0.50 12/24/19 16:56 LBDg/L0.16 12/24/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 12/24/19 16:56 LBDg/L0.17 12/24/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 12/24/19 16:56 LBDg/L0.11 12/24/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 12/24/19 16:56 LBDg/L0.15 12/24/19SM21-22 6200B1Chlorobenzene
40 50 12/24/19 16:56 LBDg/L11 12/24/19SM21-22 6200B1JEthanol
ND 0.50 12/24/19 16:56 LBDg/L0.21 12/24/19SM21-22 6200B1Chlorodibromomethane
ND 1.0 12/24/19 16:56 LBDg/L0.35 12/24/19SM21-22 6200B1Chloroethane
ND 0.50 12/24/19 16:56 LBDg/L0.17 12/24/19SM21-22 6200B1Chloroform
ND 1.0 12/24/19 16:56 LBDg/L0.45 12/24/19SM21-22 6200B1Chloromethane
ND 0.50 12/24/19 16:56 LBDg/L0.12 12/24/19SM21-22 6200B12-Chlorotoluene
ND 0.50 12/24/19 16:56 LBDg/L0.14 12/24/19SM21-22 6200B14-Chlorotoluene
ND 0.50 12/24/19 16:56 LBDg/L0.19 12/24/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 12/24/19 16:56 LBDg/L0.16 12/24/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 12/24/19 16:56 LBDg/L0.12 12/24/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 12/24/19 16:56 LBDg/L0.13 12/24/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 12/24/19 16:56 LBDg/L0.26 12/24/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 12/24/19 16:56 LBDg/L0.16 12/24/19SM21-22 6200B11,1-Dichloroethane
0.55 0.50 12/24/19 16:56 LBDg/L0.41 12/24/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 12/24/19 16:56 LBDg/L0.32 12/24/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 12/24/19 16:56 LBDg/L0.13 12/24/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 12/24/19 16:56 LBDg/L0.31 12/24/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 12/24/19 16:56 LBDg/L0.20 12/24/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 12/24/19 16:56 LBDg/L0.11 12/24/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 12/24/19 16:56 LBDg/L0.20 12/24/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 12/24/19 16:56 LBDg/L0.16 12/24/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 12/24/19 16:56 LBDg/L0.13 12/24/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 12/24/19 16:56 LBDg/L0.23 12/24/19SM21-22 6200B1trans-1,3-Dichloropropene
0.95 0.50 12/24/19 16:56 LBDg/L0.17 12/24/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 12/24/19 16:56 LBDg/L0.13 12/24/19SM21-22 6200B1Ethylbenzene
ND 5.0 12/24/19 16:56 LBDg/L1.5 12/24/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 12/24/19 16:56 LBDg/L0.17 12/24/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 12/24/19 16:56 LBDg/L0.20 12/24/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
25 0.50 12/24/19 16:56 LBDg/L0.25 12/24/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 12/24/19 16:56 LBDg/L0.34 12/24/19SM21-22 6200B1Methylene Chloride
ND 5.0 12/24/19 16:56 LBDg/L1.7 12/24/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
[TOC_1]Sample Results[TOC]
Page 6 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/19/2019
Work Order: 19L0903Sample Description:Project Location: Bennett, NC
Sample ID: 19L0903-01
Field Sample #: WSW-1
Sample Matrix: Water
Sampled: 12/18/2019 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 12/24/19 16:56 LBDg/L0.31 12/24/19SM21-22 6200B1Naphthalene
ND 0.50 12/24/19 16:56 LBDg/L0.13 12/24/19SM21-22 6200B1n-Propylbenzene
ND 0.50 12/24/19 16:56 LBDg/L0.11 12/24/19SM21-22 6200B1Styrene
ND 0.50 12/24/19 16:56 LBDg/L0.22 12/24/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 12/24/19 16:56 LBDg/L0.18 12/24/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 12/24/19 16:56 LBDg/L0.14 12/24/19SM21-22 6200B1Toluene
ND 1.0 12/24/19 16:56 LBDg/L0.57 12/24/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 12/24/19 16:56 LBDg/L0.40 12/24/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 12/24/19 16:56 LBDg/L0.20 12/24/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 12/24/19 16:56 LBDg/L0.16 12/24/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 12/24/19 16:56 LBDg/L0.24 12/24/19SM21-22 6200B1Trichloroethylene
ND 0.50 12/24/19 16:56 LBDg/L0.33 12/24/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 1.0 12/24/19 16:56 LBDg/L0.25 12/24/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 12/24/19 16:56 LBDg/L0.18 12/24/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 12/24/19 16:56 LBDg/L0.14 12/24/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 12/24/19 16:56 LBDg/L10 12/24/19SM21-22 6200B1Vinyl Acetate
ND 0.50 12/24/19 16:56 LBDg/L0.45 12/24/19SM21-22 6200B1Vinyl Chloride
ND 1.0 12/24/19 16:56 LBDg/L0.30 12/24/19SM21-22 6200B1m+p Xylene
ND 0.50 12/24/19 16:56 LBDg/L0.17 12/24/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 99.0 12/24/19 16:5670-130
Toluene-d8 100 12/24/19 16:5670-130
4-Bromofluorobenzene 100 12/24/19 16:5670-130
Page 7 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/19/2019
Work Order: 19L0903Sample Description:Project Location: Bennett, NC
Sample ID: 19L0903-02
Field Sample #: WSW-2
Sample Matrix: Water
Sampled: 12/18/2019 13:15
[TOC_2]19L0903-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 12/24/19 17:27 LBDg/L3.8 12/24/19SM21-22 6200B1Acetone
ND 0.50 12/24/19 17:27 LBDg/L0.18 12/24/19SM21-22 6200B1Benzene
ND 0.50 12/24/19 17:27 LBDg/L0.15 12/24/19SM21-22 6200B1Bromobenzene
ND 0.50 12/24/19 17:27 LBDg/L0.32 12/24/19SM21-22 6200B1Bromochloromethane
ND 0.50 12/24/19 17:27 LBDg/L0.16 12/24/19SM21-22 6200B1Bromodichloromethane
ND 0.50 12/24/19 17:27 LBDg/L0.46 12/24/19SM21-22 6200B1Bromoform
ND 2.0 12/24/19 17:27 LBDg/L0.78 12/24/19SM21-22 6200B1Bromomethane
ND 5.0 12/24/19 17:27 LBDg/L1.9 12/24/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 12/24/19 17:27 LBDg/L0.21 12/24/19SM21-22 6200B1n-Butylbenzene
ND 0.50 12/24/19 17:27 LBDg/L0.16 12/24/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 12/24/19 17:27 LBDg/L0.17 12/24/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 12/24/19 17:27 LBDg/L0.11 12/24/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 12/24/19 17:27 LBDg/L0.15 12/24/19SM21-22 6200B1Chlorobenzene
24 50 12/24/19 17:27 LBDg/L11 12/24/19SM21-22 6200B1JEthanol
ND 0.50 12/24/19 17:27 LBDg/L0.21 12/24/19SM21-22 6200B1Chlorodibromomethane
ND 1.0 12/24/19 17:27 LBDg/L0.35 12/24/19SM21-22 6200B1Chloroethane
ND 0.50 12/24/19 17:27 LBDg/L0.17 12/24/19SM21-22 6200B1Chloroform
ND 1.0 12/24/19 17:27 LBDg/L0.45 12/24/19SM21-22 6200B1Chloromethane
ND 0.50 12/24/19 17:27 LBDg/L0.12 12/24/19SM21-22 6200B12-Chlorotoluene
ND 0.50 12/24/19 17:27 LBDg/L0.14 12/24/19SM21-22 6200B14-Chlorotoluene
ND 0.50 12/24/19 17:27 LBDg/L0.19 12/24/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 12/24/19 17:27 LBDg/L0.16 12/24/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 12/24/19 17:27 LBDg/L0.12 12/24/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 12/24/19 17:27 LBDg/L0.13 12/24/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 12/24/19 17:27 LBDg/L0.26 12/24/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 12/24/19 17:27 LBDg/L0.16 12/24/19SM21-22 6200B11,1-Dichloroethane
ND 0.50 12/24/19 17:27 LBDg/L0.41 12/24/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 12/24/19 17:27 LBDg/L0.32 12/24/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 12/24/19 17:27 LBDg/L0.13 12/24/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 12/24/19 17:27 LBDg/L0.31 12/24/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 12/24/19 17:27 LBDg/L0.20 12/24/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 12/24/19 17:27 LBDg/L0.11 12/24/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 12/24/19 17:27 LBDg/L0.20 12/24/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 12/24/19 17:27 LBDg/L0.16 12/24/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 12/24/19 17:27 LBDg/L0.13 12/24/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 12/24/19 17:27 LBDg/L0.23 12/24/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 12/24/19 17:27 LBDg/L0.17 12/24/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 12/24/19 17:27 LBDg/L0.13 12/24/19SM21-22 6200B1Ethylbenzene
ND 5.0 12/24/19 17:27 LBDg/L1.5 12/24/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 12/24/19 17:27 LBDg/L0.17 12/24/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 12/24/19 17:27 LBDg/L0.20 12/24/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 12/24/19 17:27 LBDg/L0.25 12/24/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 12/24/19 17:27 LBDg/L0.34 12/24/19SM21-22 6200B1Methylene Chloride
ND 5.0 12/24/19 17:27 LBDg/L1.7 12/24/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 8 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/19/2019
Work Order: 19L0903Sample Description:Project Location: Bennett, NC
Sample ID: 19L0903-02
Field Sample #: WSW-2
Sample Matrix: Water
Sampled: 12/18/2019 13:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 12/24/19 17:27 LBDg/L0.31 12/24/19SM21-22 6200B1Naphthalene
ND 0.50 12/24/19 17:27 LBDg/L0.13 12/24/19SM21-22 6200B1n-Propylbenzene
ND 0.50 12/24/19 17:27 LBDg/L0.11 12/24/19SM21-22 6200B1Styrene
ND 0.50 12/24/19 17:27 LBDg/L0.22 12/24/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 12/24/19 17:27 LBDg/L0.18 12/24/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 12/24/19 17:27 LBDg/L0.14 12/24/19SM21-22 6200B1Toluene
ND 1.0 12/24/19 17:27 LBDg/L0.57 12/24/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 12/24/19 17:27 LBDg/L0.40 12/24/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 12/24/19 17:27 LBDg/L0.20 12/24/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 12/24/19 17:27 LBDg/L0.16 12/24/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 12/24/19 17:27 LBDg/L0.24 12/24/19SM21-22 6200B1Trichloroethylene
ND 0.50 12/24/19 17:27 LBDg/L0.33 12/24/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 1.0 12/24/19 17:27 LBDg/L0.25 12/24/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 12/24/19 17:27 LBDg/L0.18 12/24/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 12/24/19 17:27 LBDg/L0.14 12/24/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 12/24/19 17:27 LBDg/L10 12/24/19SM21-22 6200B1Vinyl Acetate
ND 0.50 12/24/19 17:27 LBDg/L0.45 12/24/19SM21-22 6200B1Vinyl Chloride
ND 1.0 12/24/19 17:27 LBDg/L0.30 12/24/19SM21-22 6200B1m+p Xylene
ND 0.50 12/24/19 17:27 LBDg/L0.17 12/24/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 98.8 12/24/19 17:2770-130
Toluene-d8 99.8 12/24/19 17:2770-130
4-Bromofluorobenzene 96.8 12/24/19 17:2770-130
Page 9 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/19/2019
Work Order: 19L0903Sample Description:Project Location: Bennett, NC
Sample ID: 19L0903-03
Field Sample #: Field Blank
Sample Matrix: Field Blank
Sampled: 12/18/2019 12:00
[TOC_2]19L0903-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 12/24/19 16:25 LBDg/L3.8 12/24/19SM21-22 6200B1Acetone
ND 0.50 12/24/19 16:25 LBDg/L0.18 12/24/19SM21-22 6200B1Benzene
ND 0.50 12/24/19 16:25 LBDg/L0.15 12/24/19SM21-22 6200B1Bromobenzene
ND 0.50 12/24/19 16:25 LBDg/L0.32 12/24/19SM21-22 6200B1Bromochloromethane
ND 0.50 12/24/19 16:25 LBDg/L0.16 12/24/19SM21-22 6200B1Bromodichloromethane
ND 0.50 12/24/19 16:25 LBDg/L0.46 12/24/19SM21-22 6200B1Bromoform
ND 2.0 12/24/19 16:25 LBDg/L0.78 12/24/19SM21-22 6200B1Bromomethane
ND 5.0 12/24/19 16:25 LBDg/L1.9 12/24/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 12/24/19 16:25 LBDg/L0.21 12/24/19SM21-22 6200B1n-Butylbenzene
ND 0.50 12/24/19 16:25 LBDg/L0.16 12/24/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 12/24/19 16:25 LBDg/L0.17 12/24/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 12/24/19 16:25 LBDg/L0.11 12/24/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 12/24/19 16:25 LBDg/L0.15 12/24/19SM21-22 6200B1Chlorobenzene
34 50 12/24/19 16:25 LBDg/L11 12/24/19SM21-22 6200B1JEthanol
ND 0.50 12/24/19 16:25 LBDg/L0.21 12/24/19SM21-22 6200B1Chlorodibromomethane
ND 1.0 12/24/19 16:25 LBDg/L0.35 12/24/19SM21-22 6200B1Chloroethane
ND 0.50 12/24/19 16:25 LBDg/L0.17 12/24/19SM21-22 6200B1Chloroform
ND 1.0 12/24/19 16:25 LBDg/L0.45 12/24/19SM21-22 6200B1Chloromethane
ND 0.50 12/24/19 16:25 LBDg/L0.12 12/24/19SM21-22 6200B12-Chlorotoluene
ND 0.50 12/24/19 16:25 LBDg/L0.14 12/24/19SM21-22 6200B14-Chlorotoluene
ND 0.50 12/24/19 16:25 LBDg/L0.19 12/24/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 12/24/19 16:25 LBDg/L0.16 12/24/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 12/24/19 16:25 LBDg/L0.12 12/24/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 12/24/19 16:25 LBDg/L0.13 12/24/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 12/24/19 16:25 LBDg/L0.26 12/24/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 12/24/19 16:25 LBDg/L0.16 12/24/19SM21-22 6200B11,1-Dichloroethane
ND 0.50 12/24/19 16:25 LBDg/L0.41 12/24/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 12/24/19 16:25 LBDg/L0.32 12/24/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 12/24/19 16:25 LBDg/L0.13 12/24/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 12/24/19 16:25 LBDg/L0.31 12/24/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 12/24/19 16:25 LBDg/L0.20 12/24/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 12/24/19 16:25 LBDg/L0.11 12/24/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 12/24/19 16:25 LBDg/L0.20 12/24/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 12/24/19 16:25 LBDg/L0.16 12/24/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 12/24/19 16:25 LBDg/L0.13 12/24/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 12/24/19 16:25 LBDg/L0.23 12/24/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 12/24/19 16:25 LBDg/L0.17 12/24/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 12/24/19 16:25 LBDg/L0.13 12/24/19SM21-22 6200B1Ethylbenzene
ND 5.0 12/24/19 16:25 LBDg/L1.5 12/24/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 12/24/19 16:25 LBDg/L0.17 12/24/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 12/24/19 16:25 LBDg/L0.20 12/24/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 12/24/19 16:25 LBDg/L0.25 12/24/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 12/24/19 16:25 LBDg/L0.34 12/24/19SM21-22 6200B1Methylene Chloride
ND 5.0 12/24/19 16:25 LBDg/L1.7 12/24/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 10 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/19/2019
Work Order: 19L0903Sample Description:Project Location: Bennett, NC
Sample ID: 19L0903-03
Field Sample #: Field Blank
Sample Matrix: Field Blank
Sampled: 12/18/2019 12:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 12/24/19 16:25 LBDg/L0.31 12/24/19SM21-22 6200B1Naphthalene
ND 0.50 12/24/19 16:25 LBDg/L0.13 12/24/19SM21-22 6200B1n-Propylbenzene
ND 0.50 12/24/19 16:25 LBDg/L0.11 12/24/19SM21-22 6200B1Styrene
ND 0.50 12/24/19 16:25 LBDg/L0.22 12/24/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 12/24/19 16:25 LBDg/L0.18 12/24/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 12/24/19 16:25 LBDg/L0.14 12/24/19SM21-22 6200B1Toluene
ND 1.0 12/24/19 16:25 LBDg/L0.57 12/24/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 12/24/19 16:25 LBDg/L0.40 12/24/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 12/24/19 16:25 LBDg/L0.20 12/24/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 12/24/19 16:25 LBDg/L0.16 12/24/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 12/24/19 16:25 LBDg/L0.24 12/24/19SM21-22 6200B1Trichloroethylene
ND 0.50 12/24/19 16:25 LBDg/L0.33 12/24/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 1.0 12/24/19 16:25 LBDg/L0.25 12/24/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 12/24/19 16:25 LBDg/L0.18 12/24/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 12/24/19 16:25 LBDg/L0.14 12/24/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 12/24/19 16:25 LBDg/L10 12/24/19SM21-22 6200B1Vinyl Acetate
ND 0.50 12/24/19 16:25 LBDg/L0.45 12/24/19SM21-22 6200B1Vinyl Chloride
ND 1.0 12/24/19 16:25 LBDg/L0.30 12/24/19SM21-22 6200B1m+p Xylene
ND 0.50 12/24/19 16:25 LBDg/L0.17 12/24/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 99.0 12/24/19 16:2570-130
Toluene-d8 99.9 12/24/19 16:2570-130
4-Bromofluorobenzene 97.9 12/24/19 16:2570-130
Page 11 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B248979 12/24/1955.0019L0903-01 [WSW-1]
B248979 12/24/1955.0019L0903-02 [WSW-2]
B248979 12/24/1955.0019L0903-03 [Field Blank]
[TOC_1]Sample Preparation Information[TOC]
Page 12 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B248979 - SW-846 5030B
[TOC_3]B248979[TOC]
Blank (B248979-BLK1) Prepared & Analyzed: 12/24/19
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
[TOC_1]QC Data[TOC]
Page 13 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248979 - SW-846 5030B
Blank (B248979-BLK1) Prepared & Analyzed: 12/24/19
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 99.324.8
g/L 25.0 70-130Surrogate: Toluene-d8 10225.4
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 95.924.0
LCS (B248979-BS1) Prepared & Analyzed: 12/24/19
Acetone g/L50 100 70-13095.295.2
Benzene g/L0.50 10.0 70-13098.99.89
Bromobenzene g/L0.50 10.0 70-13096.09.60
Bromochloromethane g/L0.50 10.0 70-13010610.6
Bromodichloromethane g/L0.50 10.0 70-13010010.0
Bromoform g/L0.50 10.0 70-13095.19.51
Bromomethane g/L1.0 10.0 60-14093.09.30
2-Butanone (MEK)g/L5.0 100 70-130111111
n-Butylbenzene g/L0.50 10.0 70-13097.59.75
sec-Butylbenzene g/L0.50 10.0 70-13010110.1
tert-Butylbenzene g/L0.50 10.0 70-13097.79.77
Carbon Tetrachloride g/L0.50 10.0 70-13096.09.60
Chlorobenzene g/L0.50 10.0 70-13097.79.77
Ethanol g/L50 100 70-13088.188.1
Chlorodibromomethane g/L0.50 10.0 70-13010110.1
Chloroethane g/L0.50 10.0 60-14092.79.27
Chloroform g/L0.50 10.0 70-13091.69.16
Chloromethane g/L0.60 10.0 60-14010310.3
2-Chlorotoluene g/L0.50 10.0 70-13010210.2
4-Chlorotoluene g/L0.50 10.0 70-13097.99.79
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13010110.1
1,2-Dichlorobenzene g/L0.50 10.0 70-13098.99.89
1,3-Dichlorobenzene g/L0.50 10.0 70-13010010.0
1,4-Dichlorobenzene g/L0.50 10.0 70-13099.09.90
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14096.09.60
1,1-Dichloroethane g/L0.50 10.0 70-13010710.7
1,2-Dichloroethane g/L0.50 10.0 70-13095.69.56
1,1-Dichloroethylene g/L0.50 10.0 70-13094.89.48
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13010810.8
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13010310.3
1,2-Dichloropropane g/L0.50 10.0 70-13011211.2
1,3-Dichloropropane g/L0.50 10.0 70-13010310.3
2,2-Dichloropropane g/L0.50 10.0 70-13099.79.97
1,1-Dichloropropene g/L0.50 10.0 70-13010110.1
cis-1,3-Dichloropropene g/L0.50 10.0 70-13010210.2
trans-1,3-Dichloropropene g/L0.50 10.0 70-13010110.1
Page 14 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248979 - SW-846 5030B
LCS (B248979-BS1) Prepared & Analyzed: 12/24/19
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13011311.3
Ethylbenzene g/L0.50 10.0 70-13098.09.80
2-Hexanone (MBK)g/L5.0 100 70-130107107
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13098.49.84
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13097.29.72
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13098.39.83
Methylene Chloride g/L5.0 10.0 70-13011311.3
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-130114114
Naphthalene g/L0.50 10.0 70-13085.88.58
n-Propylbenzene g/L0.50 10.0 70-13097.59.75
Styrene g/L0.50 10.0 70-13099.69.96
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13010410.4
Tetrachloroethylene g/L0.50 10.0 70-13095.39.53
Toluene g/L0.50 10.0 70-13099.09.90
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13088.38.83
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13092.49.24
1,1,1-Trichloroethane g/L0.50 10.0 70-13099.09.90
1,1,2-Trichloroethane g/L0.50 10.0 70-13010610.6
Trichloroethylene g/L0.50 10.0 70-13096.79.67
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13090.99.09
1,2,3-Trichloropropane g/L0.50 10.0 70-13010310.3
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13090.99.09
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13095.09.50
Vinyl Acetate g/L20 100 70-130118118
Vinyl Chloride g/L0.50 10.0 60-14010610.6
m+p Xylene g/L1.0 20.0 70-13096.019.2
o-Xylene g/L0.50 10.0 70-13097.59.75
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 96.124.0
g/L 25.0 70-130Surrogate: Toluene-d8 10425.9
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 96.824.2
LCS Dup (B248979-BSD1) Prepared & Analyzed: 12/24/19
Acetone g/L50 100 2570-13098.2 3.0898.2
Benzene g/L0.50 10.0 2570-13098.7 0.2029.87
Bromobenzene g/L0.50 10.0 2570-13095.4 0.6279.54
Bromochloromethane g/L0.50 10.0 2570-130107 0.84610.7
Bromodichloromethane g/L0.50 10.0 2570-13098.5 2.019.85
Bromoform g/L0.50 10.0 2570-13094.0 1.169.40
Bromomethane g/L1.0 10.0 2560-14098.7 5.959.87
2-Butanone (MEK)g/L5.0 100 2570-130114 3.10114
n-Butylbenzene g/L0.50 10.0 2570-130100 2.6310.0
sec-Butylbenzene g/L0.50 10.0 2570-130102 0.59310.2
tert-Butylbenzene g/L0.50 10.0 2570-13099.3 1.629.93
Carbon Tetrachloride g/L0.50 10.0 2570-13095.9 0.1049.59
Chlorobenzene g/L0.50 10.0 2570-13095.9 1.869.59
Ethanol g/L50 100 2570-130102 15.0102
Chlorodibromomethane g/L0.50 10.0 2570-130102 1.1810.2
Chloroethane g/L0.50 10.0 2560-14090.4 2.519.04
Chloroform g/L0.50 10.0 2570-13092.6 1.099.26
Chloromethane g/L0.60 10.0 2560-14094.3 8.639.43
2-Chlorotoluene g/L0.50 10.0 2570-13099.3 2.689.93
4-Chlorotoluene g/L0.50 10.0 2570-13097.0 0.9249.70
Page 15 of 22
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248979 - SW-846 5030B
LCS Dup (B248979-BSD1) Prepared & Analyzed: 12/24/19
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130101 0.099110.1
1,2-Dichlorobenzene g/L0.50 10.0 2570-130102 2.7910.2
1,3-Dichlorobenzene g/L0.50 10.0 2570-130104 3.4310.4
1,4-Dichlorobenzene g/L0.50 10.0 2570-130101 2.4010.1
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14094.3 1.799.43
1,1-Dichloroethane g/L0.50 10.0 2570-130107 0.56010.7
1,2-Dichloroethane g/L0.50 10.0 2570-13095.0 0.6309.50
1,1-Dichloroethylene g/L0.50 10.0 2570-13093.7 1.179.37
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-130108 0.18510.8
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-130102 0.68110.2
1,2-Dichloropropane g/L0.50 10.0 2570-130111 1.0711.1
1,3-Dichloropropane g/L0.50 10.0 2570-130103 0.38810.3
2,2-Dichloropropane g/L0.50 10.0 2570-13099.6 0.1009.96
1,1-Dichloropropene g/L0.50 10.0 2570-13099.2 1.709.92
cis-1,3-Dichloropropene g/L0.50 10.0 2570-130102 0.097910.2
trans-1,3-Dichloropropene g/L0.50 10.0 2570-130103 1.7710.3
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130114 1.2311.4
Ethylbenzene g/L0.50 10.0 2570-13097.0 1.039.70
2-Hexanone (MBK)g/L5.0 100 2570-130109 2.34109
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-13099.0 0.6089.90
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-13099.0 1.839.90
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13097.4 0.9209.74
Methylene Chloride g/L5.0 10.0 2570-130114 1.6711.4
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-130114 0.262114
Naphthalene g/L0.50 10.0 2570-13099.6 14.99.96
n-Propylbenzene g/L0.50 10.0 2570-13097.7 0.2059.77
Styrene g/L0.50 10.0 2570-130101 1.1010.1
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130105 1.1510.5
Tetrachloroethylene g/L0.50 10.0 2570-13097.5 2.289.75
Toluene g/L0.50 10.0 2570-13097.1 1.949.71
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-13097.1 9.499.71
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13095.0 2.779.50
1,1,1-Trichloroethane g/L0.50 10.0 2570-13097.8 1.229.78
1,1,2-Trichloroethane g/L0.50 10.0 2570-130107 0.74910.7
Trichloroethylene g/L0.50 10.0 2570-13096.3 0.4159.63
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13089.7 1.338.97
1,2,3-Trichloropropane g/L0.50 10.0 2570-13098.0 4.889.80
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-13093.1 2.399.31
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-13093.7 1.389.37
Vinyl Acetate g/L20 100 2570-130119 1.31119
Vinyl Chloride g/L0.50 10.0 2560-140102 3.5510.2
m+p Xylene g/L1.0 20.0 2570-13094.0 2.1618.8
o-Xylene g/L0.50 10.0 2570-13095.5 2.079.55
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 97.324.3
g/L 25.0 70-130Surrogate: Toluene-d8 10125.3
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 96.324.1
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*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
FLAG/QUALIFIER SUMMARY
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
[TOC_1]Flag/Qualifier Summary[TOC]
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
[TOC_1]Certifications[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2022
M-MA100Massachusetts DEPMA 06/30/2020
PH-0567Connecticut Department of Publilc HealthCT 09/30/2021
10899 NELAPNew York State Department of HealthNY 04/1/2020
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2020
LAO00112Rhode Island Department of HealthRI 12/30/2019
652North Carolina Div. of Water QualityNC 12/31/2020
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E871027 NELAPFlorida Department of HealthFL 06/30/2020
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2020
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460217Commonwealth of VirginiaVA 12/14/2020
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2020
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2020
25703North Carolina Department of HealthNC-DW 07/31/2020
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2020
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