RA-2582_16143_CA_LAB_20100922_Pace Lab Report

October 04, 2010
LIMS USE: FR - LINDA BLALOCK
LIMS OBJECT ID: 9278272
9278272
Project:
Pace Project No.:
RE:
Ms. Linda Blalock
NCDENR - UST Section
1637 Mail Service Center
Raleigh, NC 276991637
16143 Agrotec
Dear Ms. Blalock:
Enclosed are the analytical results for sample(s) received by the laboratory on September 23, 2010.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory and
Organic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. All
Microbiological analyses were performed at the laboratory where the samples were received.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin for
Renee Spencer
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
9278272
16143 Agrotec
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078Louisiana/LELAP Certification #: 04034
New Jersey Certification #: NC012North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12Pennsylvania Certification #: 68-00784
South Carolina Certification #: 99006001South Carolina Drinking Water Cert. #: 99006003
Virginia Certification #: 00213Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84Louisiana DHH Drinking Water # LA 100031
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Connecticut Certification #: PH-0106Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030
New Jersey Certification #: NC011North Carolina Bioassay Certification #: 9
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40Pennsylvania Certification #: 68-03578South Carolina Bioassay Certification #: 99030002
South Carolina Certification #: 99030001Virginia Certification #: 00072
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE SUMMARY
Pace Project No.:
Project:
9278272
16143 Agrotec
Lab ID Sample ID Matrix Date Collected Date Received
9278272001 MW-2 Water 09/22/10 13:30 09/23/10 13:30
9278272002 MW-1 Water 09/22/10 14:00 09/23/10 13:30
9278272003 WSW-4 Water 09/22/10 15:10 09/23/10 13:30
9278272004 WSW-3 Water 09/22/10 15:35 09/23/10 13:30
9278272005 WSW-1 Water 09/22/10 16:00 09/23/10 13:30
9278272006 WSW-2 Water 09/22/10 16:20 09/23/10 13:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9278272
16143 Agrotec
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
9278272001 MW-2 MADEP EPH 5 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-AJMW
EPA 625 59 PASI-CBPJ
SM 6200B 64 PASI-CTLS
9278272002 MW-1 MADEP EPH 5 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-AJMW
EPA 625 59 PASI-CBPJ
SM 6200B 64 PASI-CTLS
9278272003 WSW-4 MADEP EPH 5 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-AJMW
EPA 625 59 PASI-CPPM
SM 6200B 64 PASI-CTLS
9278272004 WSW-3 MADEP EPH 5 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-AJMW
EPA 625 59 PASI-CPPM
SM 6200B 64 PASI-CTLS
9278272005 WSW-1 MADEP EPH 5 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-AJMW
EPA 625 59 PASI-CPPM
SM 6200B 64 PASI-CTLS
9278272006 WSW-2 MADEP EPH 7 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-AJMW
EPA 625 59 PASI-CPPM
SM 6200B 64 PASI-CTLS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:MW-2 Lab ID:9278272001 Collected:09/22/10 13:30 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 09/29/10 18:4309/29/10 09:00118118
Aliphatic (C19-C36)ND ug/L 1 09/29/10 18:4309/29/10 09:00118118
Aromatic (C11-C22)ND ug/L 1 09/29/10 18:4309/29/10 09:00118118
Nonatriacontane (S)73 %1 09/29/10 18:43 7194-86-709/29/10 09:0040-140
o-Terphenyl (S)78 %1 09/29/10 18:43 84-15-109/29/10 09:0040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 09/24/10 17:01100100
Aliphatic (C09-C12)ND ug/L 1 09/24/10 17:01100100
Aromatic (C09-C10)ND ug/L 1 09/24/10 17:01100100
2,5-Dibromotoluene (PID)(S)95 %1 09/24/10 17:0170-130
2,5-Dibromotoluene (FID)(S)107 %1 09/24/10 17:0170-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead 104 ug/L 1 10/01/10 07:04 7439-92-1 B09/24/10 10:505.0 4.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 09/24/10 20:05 83-32-909/23/10 11:306.2 3.5
Acenaphthylene ND ug/L 1 09/24/10 20:05 208-96-809/23/10 11:306.2 3.5
Anthracene ND ug/L 1 09/24/10 20:05 120-12-709/23/10 11:306.2 3.6
Benzo(a)anthracene ND ug/L 1 09/24/10 20:05 56-55-309/23/10 11:306.2 3.5
Benzo(a)pyrene ND ug/L 1 09/24/10 20:05 50-32-809/23/10 11:306.2 3.9
Benzo(b)fluoranthene ND ug/L 1 09/24/10 20:05 205-99-209/23/10 11:306.2 4.5
Benzo(g,h,i)perylene ND ug/L 1 09/24/10 20:05 191-24-209/23/10 11:306.2 3.9
Benzo(k)fluoranthene ND ug/L 1 09/24/10 20:05 207-08-909/23/10 11:306.2 3.8
4-Bromophenylphenyl ether ND ug/L 1 09/24/10 20:05 101-55-309/23/10 11:306.2 3.0
Butylbenzylphthalate ND ug/L 1 09/24/10 20:05 85-68-709/23/10 11:306.2 3.6
4-Chloro-3-methylphenol ND ug/L 1 09/24/10 20:05 59-50-709/23/10 11:306.2 3.5
bis(2-Chloroethoxy)methane ND ug/L 1 09/24/10 20:05 111-91-109/23/10 11:3012.5 7.2
bis(2-Chloroethyl) ether ND ug/L 1 09/24/10 20:05 111-44-409/23/10 11:306.2 6.0
bis(2-Chloroisopropyl) ether ND ug/L 1 09/24/10 20:05 108-60-109/23/10 11:306.2 5.0
2-Chloronaphthalene ND ug/L 1 09/24/10 20:05 91-58-709/23/10 11:306.2 4.5
2-Chlorophenol ND ug/L 1 09/24/10 20:05 95-57-809/23/10 11:306.2 5.5
4-Chlorophenylphenyl ether ND ug/L 1 09/24/10 20:05 7005-72-309/23/10 11:306.2 3.4
Chrysene ND ug/L 1 09/24/10 20:05 218-01-909/23/10 11:306.2 3.4
Dibenz(a,h)anthracene ND ug/L 1 09/24/10 20:05 53-70-309/23/10 11:306.2 3.6
3,3'-Dichlorobenzidine ND ug/L 1 09/24/10 20:05 91-94-109/23/10 11:3031.2 4.2
2,4-Dichlorophenol ND ug/L 1 09/24/10 20:05 120-83-209/23/10 11:306.2 5.1
Diethylphthalate ND ug/L 1 09/24/10 20:05 84-66-209/23/10 11:306.2 3.4
2,4-Dimethylphenol ND ug/L 1 09/24/10 20:05 105-67-909/23/10 11:3012.5 7.0
Dimethylphthalate ND ug/L 1 09/24/10 20:05 131-11-309/23/10 11:306.2 3.0
Di-n-butylphthalate ND ug/L 1 09/24/10 20:05 84-74-209/23/10 11:306.2 3.6
4,6-Dinitro-2-methylphenol ND ug/L 1 09/24/10 20:05 534-52-109/23/10 11:3025.0 9.8
2,4-Dinitrophenol ND ug/L 1 09/24/10 20:05 51-28-509/23/10 11:3062.5 12.5
2,4-Dinitrotoluene ND ug/L 1 09/24/10 20:05 121-14-209/23/10 11:306.2 3.2
2,6-Dinitrotoluene ND ug/L 1 09/24/10 20:05 606-20-209/23/10 11:306.2 3.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 5 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:MW-2 Lab ID:9278272001 Collected:09/22/10 13:30 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 1 09/24/10 20:05 117-84-009/23/10 11:306.2 3.6
bis(2-Ethylhexyl)phthalate ND ug/L 1 09/24/10 20:05 117-81-709/23/10 11:306.2 2.6
Fluoranthene ND ug/L 1 09/24/10 20:05 206-44-009/23/10 11:306.2 3.6
Fluorene ND ug/L 1 09/24/10 20:05 86-73-709/23/10 11:306.2 3.2
Hexachloro-1,3-butadiene ND ug/L 1 09/24/10 20:05 87-68-309/23/10 11:306.2 4.1
Hexachlorobenzene ND ug/L 1 09/24/10 20:05 118-74-109/23/10 11:306.2 3.2
Hexachlorocyclopentadiene ND ug/L 1 09/24/10 20:05 77-47-409/23/10 11:3012.5 4.6
Hexachloroethane ND ug/L 1 09/24/10 20:05 67-72-109/23/10 11:306.2 4.1
Indeno(1,2,3-cd)pyrene ND ug/L 1 09/24/10 20:05 193-39-509/23/10 11:306.2 3.8
Isophorone ND ug/L 1 09/24/10 20:05 78-59-109/23/10 11:3012.5 8.1
2-Methylnaphthalene ND ug/L 1 09/24/10 20:05 91-57-609/23/10 11:306.2 4.2
Naphthalene ND ug/L 1 09/24/10 20:05 91-20-309/23/10 11:306.2 4.8
Nitrobenzene ND ug/L 1 09/24/10 20:05 98-95-309/23/10 11:306.2 5.5
2-Nitrophenol ND ug/L 1 09/24/10 20:05 88-75-509/23/10 11:306.2 5.8
4-Nitrophenol ND ug/L 1 09/24/10 20:05 100-02-709/23/10 11:3062.5 2.5
N-Nitrosodimethylamine ND ug/L 1 09/24/10 20:05 62-75-909/23/10 11:306.2 3.9
N-Nitroso-di-n-propylamine ND ug/L 1 09/24/10 20:05 621-64-709/23/10 11:306.2 4.6
N-Nitrosodiphenylamine ND ug/L 1 09/24/10 20:05 86-30-609/23/10 11:3012.5 8.2
Pentachlorophenol ND ug/L 1 09/24/10 20:05 87-86-509/23/10 11:3031.2 2.0
Phenanthrene ND ug/L 1 09/24/10 20:05 85-01-809/23/10 11:306.2 3.4
Phenol ND ug/L 1 09/24/10 20:05 108-95-209/23/10 11:306.2 2.2
Pyrene ND ug/L 1 09/24/10 20:05 129-00-009/23/10 11:306.2 3.6
1,2,4-Trichlorobenzene ND ug/L 1 09/24/10 20:05 120-82-109/23/10 11:306.2 4.2
2,4,6-Trichlorophenol ND ug/L 1 09/24/10 20:05 88-06-209/23/10 11:3012.5 7.6
Nitrobenzene-d5 (S)51 %1 09/24/10 20:05 4165-60-009/23/10 11:3010-120
2-Fluorobiphenyl (S)55 %1 09/24/10 20:05 321-60-809/23/10 11:3015-120
Terphenyl-d14 (S)64 %1 09/24/10 20:05 1718-51-009/23/10 11:3011-131
Phenol-d6 (S)24 %1 09/24/10 20:05 13127-88-309/23/10 11:3010-120
2-Fluorophenol (S)39 %1 09/24/10 20:05 367-12-409/23/10 11:3010-120
2,4,6-Tribromophenol (S)57 %1 09/24/10 20:05 118-79-609/23/10 11:3010-137
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 09/30/10 04:07 71-43-20.50 0.50
Bromobenzene ND ug/L 1 09/30/10 04:07 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 09/30/10 04:07 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 09/30/10 04:07 75-27-40.50 0.50
Bromoform ND ug/L 1 09/30/10 04:07 75-25-20.50 0.50
Bromomethane ND ug/L 1 09/30/10 04:07 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 09/30/10 04:07 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 09/30/10 04:07 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 09/30/10 04:07 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 09/30/10 04:07 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 09/30/10 04:07 108-90-70.50 0.50
Chloroethane ND ug/L 1 09/30/10 04:07 75-00-31.0 1.0
Chloroform ND ug/L 1 09/30/10 04:07 67-66-30.50 0.50
Chloromethane ND ug/L 1 09/30/10 04:07 74-87-31.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 6 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:MW-2 Lab ID:9278272001 Collected:09/22/10 13:30 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
2-Chlorotoluene ND ug/L 1 09/30/10 04:07 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 09/30/10 04:07 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 09/30/10 04:07 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 09/30/10 04:07 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 09/30/10 04:07 106-93-40.50 0.50
Dibromomethane ND ug/L 1 09/30/10 04:07 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 09/30/10 04:07 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 09/30/10 04:07 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 09/30/10 04:07 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 09/30/10 04:07 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 09/30/10 04:07 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 09/30/10 04:07 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 09/30/10 04:07 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 09/30/10 04:07 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 09/30/10 04:07 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 09/30/10 04:07 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 09/30/10 04:07 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 09/30/10 04:07 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 09/30/10 04:07 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 09/30/10 04:07 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 09/30/10 04:07 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 09/30/10 04:07 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 09/30/10 04:07 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 09/30/10 04:07 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 09/30/10 04:07 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 09/30/10 04:07 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 09/30/10 04:07 1634-04-40.50 0.50
Naphthalene ND ug/L 1 09/30/10 04:07 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 09/30/10 04:07 103-65-10.50 0.50
Styrene ND ug/L 1 09/30/10 04:07 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 09/30/10 04:07 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 09/30/10 04:07 79-34-50.50 0.50
Tetrachloroethene ND ug/L 1 09/30/10 04:07 127-18-40.50 0.50
Toluene ND ug/L 1 09/30/10 04:07 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 09/30/10 04:07 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 09/30/10 04:07 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 09/30/10 04:07 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 09/30/10 04:07 79-00-50.50 0.50
Trichloroethene ND ug/L 1 09/30/10 04:07 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 09/30/10 04:07 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 09/30/10 04:07 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 09/30/10 04:07 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 09/30/10 04:07 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 09/30/10 04:07 75-01-41.0 1.0
m&p-Xylene ND ug/L 1 09/30/10 04:07 179601-23-11.0 1.0
o-Xylene ND ug/L 1 09/30/10 04:07 95-47-60.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 7 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:MW-2 Lab ID:9278272001 Collected:09/22/10 13:30 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
1,2-Dichloroethane-d4 (S)109 %1 09/30/10 04:07 17060-07-070-130
Dibromofluoromethane (S)95 %1 09/30/10 04:07 1868-53-770-130
4-Bromofluorobenzene (S)110 %1 09/30/10 04:07 460-00-470-130
Toluene-d8 (S)94 %1 09/30/10 04:07 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 8 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:MW-1 Lab ID:9278272002 Collected:09/22/10 14:00 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 09/29/10 18:43 P209/29/10 09:00111111
Aliphatic (C19-C36)ND ug/L 1 09/29/10 18:4309/29/10 09:00111111
Aromatic (C11-C22)ND ug/L 1 09/29/10 18:4309/29/10 09:00111111
Nonatriacontane (S)38 %1 09/29/10 18:43 7194-86-7 S009/29/10 09:0040-140
o-Terphenyl (S)36 %1 09/29/10 18:43 84-15-1 S009/29/10 09:0040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 09/24/10 17:26100100
Aliphatic (C09-C12)ND ug/L 1 09/24/10 17:26100100
Aromatic (C09-C10)ND ug/L 1 09/24/10 17:26100100
2,5-Dibromotoluene (PID)(S)96 %1 09/24/10 17:2670-130
2,5-Dibromotoluene (FID)(S)108 %1 09/24/10 17:2670-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead 9.9 ug/L 1 10/01/10 07:08 7439-92-1 B09/24/10 10:505.0 4.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 09/24/10 20:32 83-32-909/23/10 11:305.9 3.3
Acenaphthylene ND ug/L 1 09/24/10 20:32 208-96-809/23/10 11:305.9 3.3
Anthracene ND ug/L 1 09/24/10 20:32 120-12-709/23/10 11:305.9 3.4
Benzo(a)anthracene ND ug/L 1 09/24/10 20:32 56-55-309/23/10 11:305.9 3.3
Benzo(a)pyrene ND ug/L 1 09/24/10 20:32 50-32-809/23/10 11:305.9 3.6
Benzo(b)fluoranthene ND ug/L 1 09/24/10 20:32 205-99-209/23/10 11:305.9 4.2
Benzo(g,h,i)perylene ND ug/L 1 09/24/10 20:32 191-24-209/23/10 11:305.9 3.6
Benzo(k)fluoranthene ND ug/L 1 09/24/10 20:32 207-08-909/23/10 11:305.9 3.5
4-Bromophenylphenyl ether ND ug/L 1 09/24/10 20:32 101-55-309/23/10 11:305.9 2.8
Butylbenzylphthalate ND ug/L 1 09/24/10 20:32 85-68-709/23/10 11:305.9 3.4
4-Chloro-3-methylphenol ND ug/L 1 09/24/10 20:32 59-50-709/23/10 11:305.9 3.3
bis(2-Chloroethoxy)methane ND ug/L 1 09/24/10 20:32 111-91-109/23/10 11:3011.8 6.8
bis(2-Chloroethyl) ether ND ug/L 1 09/24/10 20:32 111-44-409/23/10 11:305.9 5.6
bis(2-Chloroisopropyl) ether ND ug/L 1 09/24/10 20:32 108-60-109/23/10 11:305.9 4.7
2-Chloronaphthalene ND ug/L 1 09/24/10 20:32 91-58-709/23/10 11:305.9 4.2
2-Chlorophenol ND ug/L 1 09/24/10 20:32 95-57-809/23/10 11:305.9 5.2
4-Chlorophenylphenyl ether ND ug/L 1 09/24/10 20:32 7005-72-309/23/10 11:305.9 3.2
Chrysene ND ug/L 1 09/24/10 20:32 218-01-909/23/10 11:305.9 3.2
Dibenz(a,h)anthracene ND ug/L 1 09/24/10 20:32 53-70-309/23/10 11:305.9 3.4
3,3'-Dichlorobenzidine ND ug/L 1 09/24/10 20:32 91-94-109/23/10 11:3029.4 4.0
2,4-Dichlorophenol ND ug/L 1 09/24/10 20:32 120-83-209/23/10 11:305.9 4.8
Diethylphthalate ND ug/L 1 09/24/10 20:32 84-66-209/23/10 11:305.9 3.2
2,4-Dimethylphenol ND ug/L 1 09/24/10 20:32 105-67-909/23/10 11:3011.8 6.6
Dimethylphthalate ND ug/L 1 09/24/10 20:32 131-11-309/23/10 11:305.9 2.8
Di-n-butylphthalate ND ug/L 1 09/24/10 20:32 84-74-209/23/10 11:305.9 3.4
4,6-Dinitro-2-methylphenol ND ug/L 1 09/24/10 20:32 534-52-109/23/10 11:3023.5 9.2
2,4-Dinitrophenol ND ug/L 1 09/24/10 20:32 51-28-509/23/10 11:3058.8 11.8
2,4-Dinitrotoluene ND ug/L 1 09/24/10 20:32 121-14-209/23/10 11:305.9 3.1
2,6-Dinitrotoluene ND ug/L 1 09/24/10 20:32 606-20-209/23/10 11:305.9 3.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 9 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:MW-1 Lab ID:9278272002 Collected:09/22/10 14:00 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 1 09/24/10 20:32 117-84-009/23/10 11:305.9 3.4
bis(2-Ethylhexyl)phthalate ND ug/L 1 09/24/10 20:32 117-81-709/23/10 11:305.9 2.5
Fluoranthene ND ug/L 1 09/24/10 20:32 206-44-009/23/10 11:305.9 3.4
Fluorene ND ug/L 1 09/24/10 20:32 86-73-709/23/10 11:305.9 3.1
Hexachloro-1,3-butadiene ND ug/L 1 09/24/10 20:32 87-68-309/23/10 11:305.9 3.9
Hexachlorobenzene ND ug/L 1 09/24/10 20:32 118-74-109/23/10 11:305.9 3.1
Hexachlorocyclopentadiene ND ug/L 1 09/24/10 20:32 77-47-409/23/10 11:3011.8 4.4
Hexachloroethane ND ug/L 1 09/24/10 20:32 67-72-109/23/10 11:305.9 3.9
Indeno(1,2,3-cd)pyrene ND ug/L 1 09/24/10 20:32 193-39-509/23/10 11:305.9 3.5
Isophorone ND ug/L 1 09/24/10 20:32 78-59-109/23/10 11:3011.8 7.6
2-Methylnaphthalene ND ug/L 1 09/24/10 20:32 91-57-609/23/10 11:305.9 4.0
Naphthalene ND ug/L 1 09/24/10 20:32 91-20-309/23/10 11:305.9 4.5
Nitrobenzene ND ug/L 1 09/24/10 20:32 98-95-309/23/10 11:305.9 5.2
2-Nitrophenol ND ug/L 1 09/24/10 20:32 88-75-509/23/10 11:305.9 5.4
4-Nitrophenol ND ug/L 1 09/24/10 20:32 100-02-709/23/10 11:3058.8 2.4
N-Nitrosodimethylamine ND ug/L 1 09/24/10 20:32 62-75-909/23/10 11:305.9 3.6
N-Nitroso-di-n-propylamine ND ug/L 1 09/24/10 20:32 621-64-709/23/10 11:305.9 4.4
N-Nitrosodiphenylamine ND ug/L 1 09/24/10 20:32 86-30-609/23/10 11:3011.8 7.8
Pentachlorophenol ND ug/L 1 09/24/10 20:32 87-86-509/23/10 11:3029.4 1.9
Phenanthrene ND ug/L 1 09/24/10 20:32 85-01-809/23/10 11:305.9 3.2
Phenol ND ug/L 1 09/24/10 20:32 108-95-209/23/10 11:305.9 2.1
Pyrene ND ug/L 1 09/24/10 20:32 129-00-009/23/10 11:305.9 3.4
1,2,4-Trichlorobenzene ND ug/L 1 09/24/10 20:32 120-82-109/23/10 11:305.9 4.0
2,4,6-Trichlorophenol ND ug/L 1 09/24/10 20:32 88-06-209/23/10 11:3011.8 7.2
Nitrobenzene-d5 (S)59 %1 09/24/10 20:32 4165-60-009/23/10 11:3010-120
2-Fluorobiphenyl (S)62 %1 09/24/10 20:32 321-60-809/23/10 11:3015-120
Terphenyl-d14 (S)71 %1 09/24/10 20:32 1718-51-009/23/10 11:3011-131
Phenol-d6 (S)26 %1 09/24/10 20:32 13127-88-309/23/10 11:3010-120
2-Fluorophenol (S)42 %1 09/24/10 20:32 367-12-409/23/10 11:3010-120
2,4,6-Tribromophenol (S)68 %1 09/24/10 20:32 118-79-609/23/10 11:3010-137
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 09/30/10 04:30 71-43-20.50 0.50
Bromobenzene ND ug/L 1 09/30/10 04:30 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 09/30/10 04:30 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 09/30/10 04:30 75-27-40.50 0.50
Bromoform ND ug/L 1 09/30/10 04:30 75-25-20.50 0.50
Bromomethane ND ug/L 1 09/30/10 04:30 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 09/30/10 04:30 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 09/30/10 04:30 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 09/30/10 04:30 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 09/30/10 04:30 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 09/30/10 04:30 108-90-70.50 0.50
Chloroethane ND ug/L 1 09/30/10 04:30 75-00-31.0 1.0
Chloroform ND ug/L 1 09/30/10 04:30 67-66-30.50 0.50
Chloromethane ND ug/L 1 09/30/10 04:30 74-87-31.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 10 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:MW-1 Lab ID:9278272002 Collected:09/22/10 14:00 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
2-Chlorotoluene ND ug/L 1 09/30/10 04:30 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 09/30/10 04:30 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 09/30/10 04:30 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 09/30/10 04:30 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 09/30/10 04:30 106-93-40.50 0.50
Dibromomethane ND ug/L 1 09/30/10 04:30 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 09/30/10 04:30 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 09/30/10 04:30 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 09/30/10 04:30 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 09/30/10 04:30 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 09/30/10 04:30 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 09/30/10 04:30 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 09/30/10 04:30 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 09/30/10 04:30 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 09/30/10 04:30 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 09/30/10 04:30 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 09/30/10 04:30 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 09/30/10 04:30 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 09/30/10 04:30 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 09/30/10 04:30 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 09/30/10 04:30 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 09/30/10 04:30 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 09/30/10 04:30 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 09/30/10 04:30 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 09/30/10 04:30 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 09/30/10 04:30 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 09/30/10 04:30 1634-04-40.50 0.50
Naphthalene ND ug/L 1 09/30/10 04:30 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 09/30/10 04:30 103-65-10.50 0.50
Styrene ND ug/L 1 09/30/10 04:30 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 09/30/10 04:30 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 09/30/10 04:30 79-34-50.50 0.50
Tetrachloroethene ND ug/L 1 09/30/10 04:30 127-18-40.50 0.50
Toluene ND ug/L 1 09/30/10 04:30 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 09/30/10 04:30 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 09/30/10 04:30 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 09/30/10 04:30 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 09/30/10 04:30 79-00-50.50 0.50
Trichloroethene ND ug/L 1 09/30/10 04:30 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 09/30/10 04:30 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 09/30/10 04:30 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 09/30/10 04:30 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 09/30/10 04:30 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 09/30/10 04:30 75-01-41.0 1.0
m&p-Xylene ND ug/L 1 09/30/10 04:30 179601-23-11.0 1.0
o-Xylene ND ug/L 1 09/30/10 04:30 95-47-60.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 11 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:MW-1 Lab ID:9278272002 Collected:09/22/10 14:00 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
1,2-Dichloroethane-d4 (S)110 %1 09/30/10 04:30 17060-07-070-130
Dibromofluoromethane (S)96 %1 09/30/10 04:30 1868-53-770-130
4-Bromofluorobenzene (S)111 %1 09/30/10 04:30 460-00-470-130
Toluene-d8 (S)96 %1 09/30/10 04:30 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 12 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:WSW-4 Lab ID:9278272003 Collected:09/22/10 15:10 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 09/29/10 19:1909/29/10 09:00104104
Aliphatic (C19-C36)ND ug/L 1 09/29/10 19:1909/29/10 09:00104104
Aromatic (C11-C22)ND ug/L 1 09/29/10 19:1909/29/10 09:00104104
Nonatriacontane (S)77 %1 09/29/10 19:19 7194-86-709/29/10 09:0040-140
o-Terphenyl (S)74 %1 09/29/10 19:19 84-15-109/29/10 09:0040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 09/24/10 17:51100100
Aliphatic (C09-C12)ND ug/L 1 09/24/10 17:51100100
Aromatic (C09-C10)ND ug/L 1 09/24/10 17:51100100
2,5-Dibromotoluene (PID)(S)98 %1 09/24/10 17:5170-130
2,5-Dibromotoluene (FID)(S)112 %1 09/24/10 17:5170-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead ND ug/L 1 10/01/10 07:11 7439-92-109/24/10 10:505.0 4.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 09/28/10 23:02 83-32-909/27/10 15:305.6 3.1
Acenaphthylene ND ug/L 1 09/28/10 23:02 208-96-809/27/10 15:305.6 3.1
Anthracene ND ug/L 1 09/28/10 23:02 120-12-709/27/10 15:305.6 3.2
Benzo(a)anthracene ND ug/L 1 09/28/10 23:02 56-55-309/27/10 15:305.6 3.1
Benzo(a)pyrene ND ug/L 1 09/28/10 23:02 50-32-809/27/10 15:305.6 3.4
Benzo(b)fluoranthene ND ug/L 1 09/28/10 23:02 205-99-209/27/10 15:305.6 4.0
Benzo(g,h,i)perylene ND ug/L 1 09/28/10 23:02 191-24-209/27/10 15:305.6 3.4
Benzo(k)fluoranthene ND ug/L 1 09/28/10 23:02 207-08-909/27/10 15:305.6 3.3
4-Bromophenylphenyl ether ND ug/L 1 09/28/10 23:02 101-55-309/27/10 15:305.6 2.7
Butylbenzylphthalate ND ug/L 1 09/28/10 23:02 85-68-709/27/10 15:305.6 3.2
4-Chloro-3-methylphenol ND ug/L 1 09/28/10 23:02 59-50-709/27/10 15:305.6 3.1
bis(2-Chloroethoxy)methane ND ug/L 1 09/28/10 23:02 111-91-109/27/10 15:3011.1 6.4
bis(2-Chloroethyl) ether ND ug/L 1 09/28/10 23:02 111-44-409/27/10 15:305.6 5.3
bis(2-Chloroisopropyl) ether ND ug/L 1 09/28/10 23:02 108-60-109/27/10 15:305.6 4.4
2-Chloronaphthalene ND ug/L 1 09/28/10 23:02 91-58-709/27/10 15:305.6 4.0
2-Chlorophenol ND ug/L 1 09/28/10 23:02 95-57-809/27/10 15:305.6 4.9
4-Chlorophenylphenyl ether ND ug/L 1 09/28/10 23:02 7005-72-309/27/10 15:305.6 3.0
Chrysene ND ug/L 1 09/28/10 23:02 218-01-909/27/10 15:305.6 3.0
Dibenz(a,h)anthracene ND ug/L 1 09/28/10 23:02 53-70-309/27/10 15:305.6 3.2
3,3'-Dichlorobenzidine ND ug/L 1 09/28/10 23:02 91-94-109/27/10 15:3027.8 3.8
2,4-Dichlorophenol ND ug/L 1 09/28/10 23:02 120-83-209/27/10 15:305.6 4.6
Diethylphthalate ND ug/L 1 09/28/10 23:02 84-66-209/27/10 15:305.6 3.0
2,4-Dimethylphenol ND ug/L 1 09/28/10 23:02 105-67-909/27/10 15:3011.1 6.2
Dimethylphthalate ND ug/L 1 09/28/10 23:02 131-11-309/27/10 15:305.6 2.7
Di-n-butylphthalate ND ug/L 1 09/28/10 23:02 84-74-209/27/10 15:305.6 3.2
4,6-Dinitro-2-methylphenol ND ug/L 1 09/28/10 23:02 534-52-109/27/10 15:3022.2 8.7
2,4-Dinitrophenol ND ug/L 1 09/28/10 23:02 51-28-509/27/10 15:3055.6 11.1
2,4-Dinitrotoluene ND ug/L 1 09/28/10 23:02 121-14-209/27/10 15:305.6 2.9
2,6-Dinitrotoluene ND ug/L 1 09/28/10 23:02 606-20-209/27/10 15:305.6 3.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 13 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:WSW-4 Lab ID:9278272003 Collected:09/22/10 15:10 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 1 09/28/10 23:02 117-84-009/27/10 15:305.6 3.2
bis(2-Ethylhexyl)phthalate ND ug/L 1 09/28/10 23:02 117-81-709/27/10 15:305.6 2.3
Fluoranthene ND ug/L 1 09/28/10 23:02 206-44-009/27/10 15:305.6 3.2
Fluorene ND ug/L 1 09/28/10 23:02 86-73-709/27/10 15:305.6 2.9
Hexachloro-1,3-butadiene ND ug/L 1 09/28/10 23:02 87-68-309/27/10 15:305.6 3.7
Hexachlorobenzene ND ug/L 1 09/28/10 23:02 118-74-109/27/10 15:305.6 2.9
Hexachlorocyclopentadiene ND ug/L 1 09/28/10 23:02 77-47-409/27/10 15:3011.1 4.1
Hexachloroethane ND ug/L 1 09/28/10 23:02 67-72-109/27/10 15:305.6 3.7
Indeno(1,2,3-cd)pyrene ND ug/L 1 09/28/10 23:02 193-39-509/27/10 15:305.6 3.3
Isophorone ND ug/L 1 09/28/10 23:02 78-59-109/27/10 15:3011.1 7.2
2-Methylnaphthalene ND ug/L 1 09/28/10 23:02 91-57-609/27/10 15:305.6 3.8
Naphthalene ND ug/L 1 09/28/10 23:02 91-20-309/27/10 15:305.6 4.2
Nitrobenzene ND ug/L 1 09/28/10 23:02 98-95-309/27/10 15:305.6 4.9
2-Nitrophenol ND ug/L 1 09/28/10 23:02 88-75-509/27/10 15:305.6 5.1
4-Nitrophenol ND ug/L 1 09/28/10 23:02 100-02-709/27/10 15:3055.6 2.2
N-Nitrosodimethylamine ND ug/L 1 09/28/10 23:02 62-75-909/27/10 15:305.6 3.4
N-Nitroso-di-n-propylamine ND ug/L 1 09/28/10 23:02 621-64-709/27/10 15:305.6 4.1
N-Nitrosodiphenylamine ND ug/L 1 09/28/10 23:02 86-30-609/27/10 15:3011.1 7.3
Pentachlorophenol ND ug/L 1 09/28/10 23:02 87-86-509/27/10 15:3027.8 1.8
Phenanthrene ND ug/L 1 09/28/10 23:02 85-01-809/27/10 15:305.6 3.0
Phenol ND ug/L 1 09/28/10 23:02 108-95-209/27/10 15:305.6 2.0
Pyrene ND ug/L 1 09/28/10 23:02 129-00-009/27/10 15:305.6 3.2
1,2,4-Trichlorobenzene ND ug/L 1 09/28/10 23:02 120-82-109/27/10 15:305.6 3.8
2,4,6-Trichlorophenol ND ug/L 1 09/28/10 23:02 88-06-209/27/10 15:3011.1 6.8
Nitrobenzene-d5 (S)33 %1 09/28/10 23:02 4165-60-009/27/10 15:3010-120
2-Fluorobiphenyl (S)33 %1 09/28/10 23:02 321-60-809/27/10 15:3015-120
Terphenyl-d14 (S)50 %1 09/28/10 23:02 1718-51-009/27/10 15:3011-131
Phenol-d6 (S)14 %1 09/28/10 23:02 13127-88-309/27/10 15:3010-120
2-Fluorophenol (S)21 %1 09/28/10 23:02 367-12-409/27/10 15:3010-120
2,4,6-Tribromophenol (S)26 %1 09/28/10 23:02 118-79-609/27/10 15:3010-137
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 09/30/10 04:53 71-43-20.50 0.50
Bromobenzene ND ug/L 1 09/30/10 04:53 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 09/30/10 04:53 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 09/30/10 04:53 75-27-40.50 0.50
Bromoform ND ug/L 1 09/30/10 04:53 75-25-20.50 0.50
Bromomethane ND ug/L 1 09/30/10 04:53 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 09/30/10 04:53 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 09/30/10 04:53 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 09/30/10 04:53 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 09/30/10 04:53 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 09/30/10 04:53 108-90-70.50 0.50
Chloroethane ND ug/L 1 09/30/10 04:53 75-00-31.0 1.0
Chloroform ND ug/L 1 09/30/10 04:53 67-66-30.50 0.50
Chloromethane ND ug/L 1 09/30/10 04:53 74-87-31.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 14 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:WSW-4 Lab ID:9278272003 Collected:09/22/10 15:10 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
2-Chlorotoluene ND ug/L 1 09/30/10 04:53 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 09/30/10 04:53 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 09/30/10 04:53 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 09/30/10 04:53 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 09/30/10 04:53 106-93-40.50 0.50
Dibromomethane ND ug/L 1 09/30/10 04:53 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 09/30/10 04:53 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 09/30/10 04:53 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 09/30/10 04:53 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 09/30/10 04:53 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 09/30/10 04:53 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 09/30/10 04:53 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 09/30/10 04:53 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 09/30/10 04:53 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 09/30/10 04:53 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 09/30/10 04:53 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 09/30/10 04:53 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 09/30/10 04:53 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 09/30/10 04:53 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 09/30/10 04:53 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 09/30/10 04:53 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 09/30/10 04:53 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 09/30/10 04:53 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 09/30/10 04:53 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 09/30/10 04:53 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 09/30/10 04:53 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 09/30/10 04:53 1634-04-40.50 0.50
Naphthalene ND ug/L 1 09/30/10 04:53 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 09/30/10 04:53 103-65-10.50 0.50
Styrene ND ug/L 1 09/30/10 04:53 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 09/30/10 04:53 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 09/30/10 04:53 79-34-50.50 0.50
Tetrachloroethene ND ug/L 1 09/30/10 04:53 127-18-40.50 0.50
Toluene ND ug/L 1 09/30/10 04:53 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 09/30/10 04:53 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 09/30/10 04:53 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 09/30/10 04:53 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 09/30/10 04:53 79-00-50.50 0.50
Trichloroethene ND ug/L 1 09/30/10 04:53 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 09/30/10 04:53 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 09/30/10 04:53 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 09/30/10 04:53 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 09/30/10 04:53 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 09/30/10 04:53 75-01-41.0 1.0
m&p-Xylene ND ug/L 1 09/30/10 04:53 179601-23-11.0 1.0
o-Xylene ND ug/L 1 09/30/10 04:53 95-47-60.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 15 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:WSW-4 Lab ID:9278272003 Collected:09/22/10 15:10 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
1,2-Dichloroethane-d4 (S)105 %1 09/30/10 04:53 17060-07-070-130
Dibromofluoromethane (S)88 %1 09/30/10 04:53 1868-53-770-130
4-Bromofluorobenzene (S)109 %1 09/30/10 04:53 460-00-470-130
Toluene-d8 (S)93 %1 09/30/10 04:53 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 16 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:WSW-3 Lab ID:9278272004 Collected:09/22/10 15:35 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 09/29/10 19:1909/29/10 09:00104104
Aliphatic (C19-C36)ND ug/L 1 09/29/10 19:1909/29/10 09:00104104
Aromatic (C11-C22)ND ug/L 1 09/29/10 19:1909/29/10 09:00104104
Nonatriacontane (S)69 %1 09/29/10 19:19 7194-86-709/29/10 09:0040-140
o-Terphenyl (S)76 %1 09/29/10 19:19 84-15-109/29/10 09:0040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 09/24/10 18:16100100
Aliphatic (C09-C12)ND ug/L 1 09/24/10 18:16100100
Aromatic (C09-C10)ND ug/L 1 09/24/10 18:16100100
2,5-Dibromotoluene (PID)(S)96 %1 09/24/10 18:1670-130
2,5-Dibromotoluene (FID)(S)109 %1 09/24/10 18:1670-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead ND ug/L 1 10/01/10 07:14 7439-92-109/24/10 10:505.0 4.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 09/28/10 23:30 83-32-909/27/10 15:305.4 3.0
Acenaphthylene ND ug/L 1 09/28/10 23:30 208-96-809/27/10 15:305.4 3.0
Anthracene ND ug/L 1 09/28/10 23:30 120-12-709/27/10 15:305.4 3.2
Benzo(a)anthracene ND ug/L 1 09/28/10 23:30 56-55-309/27/10 15:305.4 3.0
Benzo(a)pyrene ND ug/L 1 09/28/10 23:30 50-32-809/27/10 15:305.4 3.4
Benzo(b)fluoranthene ND ug/L 1 09/28/10 23:30 205-99-209/27/10 15:305.4 3.9
Benzo(g,h,i)perylene ND ug/L 1 09/28/10 23:30 191-24-209/27/10 15:305.4 3.4
Benzo(k)fluoranthene ND ug/L 1 09/28/10 23:30 207-08-909/27/10 15:305.4 3.3
4-Bromophenylphenyl ether ND ug/L 1 09/28/10 23:30 101-55-309/27/10 15:305.4 2.6
Butylbenzylphthalate ND ug/L 1 09/28/10 23:30 85-68-709/27/10 15:305.4 3.2
4-Chloro-3-methylphenol ND ug/L 1 09/28/10 23:30 59-50-709/27/10 15:305.4 3.0
bis(2-Chloroethoxy)methane ND ug/L 1 09/28/10 23:30 111-91-109/27/10 15:3010.9 6.3
bis(2-Chloroethyl) ether ND ug/L 1 09/28/10 23:30 111-44-409/27/10 15:305.4 5.2
bis(2-Chloroisopropyl) ether ND ug/L 1 09/28/10 23:30 108-60-109/27/10 15:305.4 4.3
2-Chloronaphthalene ND ug/L 1 09/28/10 23:30 91-58-709/27/10 15:305.4 3.9
2-Chlorophenol ND ug/L 1 09/28/10 23:30 95-57-809/27/10 15:305.4 4.8
4-Chlorophenylphenyl ether ND ug/L 1 09/28/10 23:30 7005-72-309/27/10 15:305.4 2.9
Chrysene ND ug/L 1 09/28/10 23:30 218-01-909/27/10 15:305.4 2.9
Dibenz(a,h)anthracene ND ug/L 1 09/28/10 23:30 53-70-309/27/10 15:305.4 3.2
3,3'-Dichlorobenzidine ND ug/L 1 09/28/10 23:30 91-94-109/27/10 15:3027.2 3.7
2,4-Dichlorophenol ND ug/L 1 09/28/10 23:30 120-83-209/27/10 15:305.4 4.5
Diethylphthalate ND ug/L 1 09/28/10 23:30 84-66-209/27/10 15:305.4 2.9
2,4-Dimethylphenol ND ug/L 1 09/28/10 23:30 105-67-909/27/10 15:3010.9 6.1
Dimethylphthalate ND ug/L 1 09/28/10 23:30 131-11-309/27/10 15:305.4 2.6
Di-n-butylphthalate ND ug/L 1 09/28/10 23:30 84-74-209/27/10 15:305.4 3.2
4,6-Dinitro-2-methylphenol ND ug/L 1 09/28/10 23:30 534-52-109/27/10 15:3021.7 8.5
2,4-Dinitrophenol ND ug/L 1 09/28/10 23:30 51-28-509/27/10 15:3054.3 10.9
2,4-Dinitrotoluene ND ug/L 1 09/28/10 23:30 121-14-209/27/10 15:305.4 2.8
2,6-Dinitrotoluene ND ug/L 1 09/28/10 23:30 606-20-209/27/10 15:305.4 3.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 17 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:WSW-3 Lab ID:9278272004 Collected:09/22/10 15:35 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 1 09/28/10 23:30 117-84-009/27/10 15:305.4 3.2
bis(2-Ethylhexyl)phthalate ND ug/L 1 09/28/10 23:30 117-81-709/27/10 15:305.4 2.3
Fluoranthene ND ug/L 1 09/28/10 23:30 206-44-009/27/10 15:305.4 3.2
Fluorene ND ug/L 1 09/28/10 23:30 86-73-709/27/10 15:305.4 2.8
Hexachloro-1,3-butadiene ND ug/L 1 09/28/10 23:30 87-68-309/27/10 15:305.4 3.6
Hexachlorobenzene ND ug/L 1 09/28/10 23:30 118-74-109/27/10 15:305.4 2.8
Hexachlorocyclopentadiene ND ug/L 1 09/28/10 23:30 77-47-409/27/10 15:3010.9 4.0
Hexachloroethane ND ug/L 1 09/28/10 23:30 67-72-109/27/10 15:305.4 3.6
Indeno(1,2,3-cd)pyrene ND ug/L 1 09/28/10 23:30 193-39-509/27/10 15:305.4 3.3
Isophorone ND ug/L 1 09/28/10 23:30 78-59-109/27/10 15:3010.9 7.1
2-Methylnaphthalene ND ug/L 1 09/28/10 23:30 91-57-609/27/10 15:305.4 3.7
Naphthalene ND ug/L 1 09/28/10 23:30 91-20-309/27/10 15:305.4 4.1
Nitrobenzene ND ug/L 1 09/28/10 23:30 98-95-309/27/10 15:305.4 4.8
2-Nitrophenol ND ug/L 1 09/28/10 23:30 88-75-509/27/10 15:305.4 5.0
4-Nitrophenol ND ug/L 1 09/28/10 23:30 100-02-709/27/10 15:3054.3 2.2
N-Nitrosodimethylamine ND ug/L 1 09/28/10 23:30 62-75-909/27/10 15:305.4 3.4
N-Nitroso-di-n-propylamine ND ug/L 1 09/28/10 23:30 621-64-709/27/10 15:305.4 4.0
N-Nitrosodiphenylamine ND ug/L 1 09/28/10 23:30 86-30-609/27/10 15:3010.9 7.2
Pentachlorophenol ND ug/L 1 09/28/10 23:30 87-86-509/27/10 15:3027.2 1.7
Phenanthrene ND ug/L 1 09/28/10 23:30 85-01-809/27/10 15:305.4 2.9
Phenol ND ug/L 1 09/28/10 23:30 108-95-209/27/10 15:305.4 2.0
Pyrene ND ug/L 1 09/28/10 23:30 129-00-009/27/10 15:305.4 3.2
1,2,4-Trichlorobenzene ND ug/L 1 09/28/10 23:30 120-82-109/27/10 15:305.4 3.7
2,4,6-Trichlorophenol ND ug/L 1 09/28/10 23:30 88-06-209/27/10 15:3010.9 6.6
Nitrobenzene-d5 (S)44 %1 09/28/10 23:30 4165-60-009/27/10 15:3010-120
2-Fluorobiphenyl (S)45 %1 09/28/10 23:30 321-60-809/27/10 15:3015-120
Terphenyl-d14 (S)68 %1 09/28/10 23:30 1718-51-009/27/10 15:3011-131
Phenol-d6 (S)19 %1 09/28/10 23:30 13127-88-309/27/10 15:3010-120
2-Fluorophenol (S)27 %1 09/28/10 23:30 367-12-409/27/10 15:3010-120
2,4,6-Tribromophenol (S)43 %1 09/28/10 23:30 118-79-609/27/10 15:3010-137
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 09/30/10 05:16 71-43-20.50 0.50
Bromobenzene ND ug/L 1 09/30/10 05:16 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 09/30/10 05:16 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 09/30/10 05:16 75-27-40.50 0.50
Bromoform ND ug/L 1 09/30/10 05:16 75-25-20.50 0.50
Bromomethane ND ug/L 1 09/30/10 05:16 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 09/30/10 05:16 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 09/30/10 05:16 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 09/30/10 05:16 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 09/30/10 05:16 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 09/30/10 05:16 108-90-70.50 0.50
Chloroethane ND ug/L 1 09/30/10 05:16 75-00-31.0 1.0
Chloroform ND ug/L 1 09/30/10 05:16 67-66-30.50 0.50
Chloromethane ND ug/L 1 09/30/10 05:16 74-87-31.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 18 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:WSW-3 Lab ID:9278272004 Collected:09/22/10 15:35 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
2-Chlorotoluene ND ug/L 1 09/30/10 05:16 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 09/30/10 05:16 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 09/30/10 05:16 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 09/30/10 05:16 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 09/30/10 05:16 106-93-40.50 0.50
Dibromomethane ND ug/L 1 09/30/10 05:16 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 09/30/10 05:16 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 09/30/10 05:16 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 09/30/10 05:16 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 09/30/10 05:16 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 09/30/10 05:16 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 09/30/10 05:16 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 09/30/10 05:16 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 09/30/10 05:16 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 09/30/10 05:16 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 09/30/10 05:16 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 09/30/10 05:16 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 09/30/10 05:16 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 09/30/10 05:16 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 09/30/10 05:16 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 09/30/10 05:16 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 09/30/10 05:16 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 09/30/10 05:16 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 09/30/10 05:16 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 09/30/10 05:16 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 09/30/10 05:16 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 09/30/10 05:16 1634-04-40.50 0.50
Naphthalene ND ug/L 1 09/30/10 05:16 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 09/30/10 05:16 103-65-10.50 0.50
Styrene ND ug/L 1 09/30/10 05:16 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 09/30/10 05:16 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 09/30/10 05:16 79-34-50.50 0.50
Tetrachloroethene ND ug/L 1 09/30/10 05:16 127-18-40.50 0.50
Toluene ND ug/L 1 09/30/10 05:16 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 09/30/10 05:16 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 09/30/10 05:16 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 09/30/10 05:16 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 09/30/10 05:16 79-00-50.50 0.50
Trichloroethene ND ug/L 1 09/30/10 05:16 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 09/30/10 05:16 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 09/30/10 05:16 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 09/30/10 05:16 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 09/30/10 05:16 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 09/30/10 05:16 75-01-41.0 1.0
m&p-Xylene ND ug/L 1 09/30/10 05:16 179601-23-11.0 1.0
o-Xylene ND ug/L 1 09/30/10 05:16 95-47-60.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 19 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:WSW-3 Lab ID:9278272004 Collected:09/22/10 15:35 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
1,2-Dichloroethane-d4 (S)111 %1 09/30/10 05:16 17060-07-070-130
Dibromofluoromethane (S)95 %1 09/30/10 05:16 1868-53-770-130
4-Bromofluorobenzene (S)111 %1 09/30/10 05:16 460-00-470-130
Toluene-d8 (S)95 %1 09/30/10 05:16 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 20 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:WSW-1 Lab ID:9278272005 Collected:09/22/10 16:00 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 09/29/10 19:5509/29/10 09:00105105
Aliphatic (C19-C36)ND ug/L 1 09/29/10 19:5509/29/10 09:00105105
Aromatic (C11-C22)ND ug/L 1 09/29/10 19:5509/29/10 09:00105105
Nonatriacontane (S)73 %1 09/29/10 19:55 7194-86-709/29/10 09:0040-140
o-Terphenyl (S)72 %1 09/29/10 19:55 84-15-109/29/10 09:0040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 09/24/10 18:41100100
Aliphatic (C09-C12)ND ug/L 1 09/24/10 18:41100100
Aromatic (C09-C10)ND ug/L 1 09/24/10 18:41100100
2,5-Dibromotoluene (PID)(S)101 %1 09/24/10 18:4170-130
2,5-Dibromotoluene (FID)(S)115 %1 09/24/10 18:4170-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead ND ug/L 1 10/01/10 07:17 7439-92-109/24/10 10:505.0 4.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 09/28/10 23:57 83-32-909/27/10 15:305.3 2.9
Acenaphthylene ND ug/L 1 09/28/10 23:57 208-96-809/27/10 15:305.3 2.9
Anthracene ND ug/L 1 09/28/10 23:57 120-12-709/27/10 15:305.3 3.1
Benzo(a)anthracene ND ug/L 1 09/28/10 23:57 56-55-309/27/10 15:305.3 2.9
Benzo(a)pyrene ND ug/L 1 09/28/10 23:57 50-32-809/27/10 15:305.3 3.3
Benzo(b)fluoranthene ND ug/L 1 09/28/10 23:57 205-99-209/27/10 15:305.3 3.8
Benzo(g,h,i)perylene ND ug/L 1 09/28/10 23:57 191-24-209/27/10 15:305.3 3.3
Benzo(k)fluoranthene ND ug/L 1 09/28/10 23:57 207-08-909/27/10 15:305.3 3.2
4-Bromophenylphenyl ether ND ug/L 1 09/28/10 23:57 101-55-309/27/10 15:305.3 2.5
Butylbenzylphthalate ND ug/L 1 09/28/10 23:57 85-68-709/27/10 15:305.3 3.1
4-Chloro-3-methylphenol ND ug/L 1 09/28/10 23:57 59-50-709/27/10 15:305.3 2.9
bis(2-Chloroethoxy)methane ND ug/L 1 09/28/10 23:57 111-91-109/27/10 15:3010.5 6.1
bis(2-Chloroethyl) ether ND ug/L 1 09/28/10 23:57 111-44-409/27/10 15:305.3 5.1
bis(2-Chloroisopropyl) ether ND ug/L 1 09/28/10 23:57 108-60-109/27/10 15:305.3 4.2
2-Chloronaphthalene ND ug/L 1 09/28/10 23:57 91-58-709/27/10 15:305.3 3.8
2-Chlorophenol ND ug/L 1 09/28/10 23:57 95-57-809/27/10 15:305.3 4.6
4-Chlorophenylphenyl ether ND ug/L 1 09/28/10 23:57 7005-72-309/27/10 15:305.3 2.8
Chrysene ND ug/L 1 09/28/10 23:57 218-01-909/27/10 15:305.3 2.8
Dibenz(a,h)anthracene ND ug/L 1 09/28/10 23:57 53-70-309/27/10 15:305.3 3.1
3,3'-Dichlorobenzidine ND ug/L 1 09/28/10 23:57 91-94-109/27/10 15:3026.3 3.6
2,4-Dichlorophenol ND ug/L 1 09/28/10 23:57 120-83-209/27/10 15:305.3 4.3
Diethylphthalate ND ug/L 1 09/28/10 23:57 84-66-209/27/10 15:305.3 2.8
2,4-Dimethylphenol ND ug/L 1 09/28/10 23:57 105-67-909/27/10 15:3010.5 5.9
Dimethylphthalate ND ug/L 1 09/28/10 23:57 131-11-309/27/10 15:305.3 2.5
Di-n-butylphthalate ND ug/L 1 09/28/10 23:57 84-74-209/27/10 15:305.3 3.1
4,6-Dinitro-2-methylphenol ND ug/L 1 09/28/10 23:57 534-52-109/27/10 15:3021.1 8.2
2,4-Dinitrophenol ND ug/L 1 09/28/10 23:57 51-28-509/27/10 15:3052.6 10.5
2,4-Dinitrotoluene ND ug/L 1 09/28/10 23:57 121-14-209/27/10 15:305.3 2.7
2,6-Dinitrotoluene ND ug/L 1 09/28/10 23:57 606-20-209/27/10 15:305.3 2.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 21 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:WSW-1 Lab ID:9278272005 Collected:09/22/10 16:00 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Di-n-octylphthalate ND ug/L 1 09/28/10 23:57 117-84-009/27/10 15:305.3 3.1
bis(2-Ethylhexyl)phthalate ND ug/L 1 09/28/10 23:57 117-81-709/27/10 15:305.3 2.2
Fluoranthene ND ug/L 1 09/28/10 23:57 206-44-009/27/10 15:305.3 3.1
Fluorene ND ug/L 1 09/28/10 23:57 86-73-709/27/10 15:305.3 2.7
Hexachloro-1,3-butadiene ND ug/L 1 09/28/10 23:57 87-68-309/27/10 15:305.3 3.5
Hexachlorobenzene ND ug/L 1 09/28/10 23:57 118-74-109/27/10 15:305.3 2.7
Hexachlorocyclopentadiene ND ug/L 1 09/28/10 23:57 77-47-409/27/10 15:3010.5 3.9
Hexachloroethane ND ug/L 1 09/28/10 23:57 67-72-109/27/10 15:305.3 3.5
Indeno(1,2,3-cd)pyrene ND ug/L 1 09/28/10 23:57 193-39-509/27/10 15:305.3 3.2
Isophorone ND ug/L 1 09/28/10 23:57 78-59-109/27/10 15:3010.5 6.8
2-Methylnaphthalene ND ug/L 1 09/28/10 23:57 91-57-609/27/10 15:305.3 3.6
Naphthalene ND ug/L 1 09/28/10 23:57 91-20-309/27/10 15:305.3 4.0
Nitrobenzene ND ug/L 1 09/28/10 23:57 98-95-309/27/10 15:305.3 4.6
2-Nitrophenol ND ug/L 1 09/28/10 23:57 88-75-509/27/10 15:305.3 4.8
4-Nitrophenol ND ug/L 1 09/28/10 23:57 100-02-709/27/10 15:3052.6 2.1
N-Nitrosodimethylamine ND ug/L 1 09/28/10 23:57 62-75-909/27/10 15:305.3 3.3
N-Nitroso-di-n-propylamine ND ug/L 1 09/28/10 23:57 621-64-709/27/10 15:305.3 3.9
N-Nitrosodiphenylamine ND ug/L 1 09/28/10 23:57 86-30-609/27/10 15:3010.5 6.9
Pentachlorophenol ND ug/L 1 09/28/10 23:57 87-86-509/27/10 15:3026.3 1.7
Phenanthrene ND ug/L 1 09/28/10 23:57 85-01-809/27/10 15:305.3 2.8
Phenol ND ug/L 1 09/28/10 23:57 108-95-209/27/10 15:305.3 1.9
Pyrene ND ug/L 1 09/28/10 23:57 129-00-009/27/10 15:305.3 3.1
1,2,4-Trichlorobenzene ND ug/L 1 09/28/10 23:57 120-82-109/27/10 15:305.3 3.6
2,4,6-Trichlorophenol ND ug/L 1 09/28/10 23:57 88-06-209/27/10 15:3010.5 6.4
Nitrobenzene-d5 (S)61 %1 09/28/10 23:57 4165-60-009/27/10 15:3010-120
2-Fluorobiphenyl (S)64 %1 09/28/10 23:57 321-60-809/27/10 15:3015-120
Terphenyl-d14 (S)80 %1 09/28/10 23:57 1718-51-009/27/10 15:3011-131
Phenol-d6 (S)25 %1 09/28/10 23:57 13127-88-309/27/10 15:3010-120
2-Fluorophenol (S)39 %1 09/28/10 23:57 367-12-409/27/10 15:3010-120
2,4,6-Tribromophenol (S)69 %1 09/28/10 23:57 118-79-609/27/10 15:3010-137
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 09/30/10 05:39 71-43-20.50 0.50
Bromobenzene ND ug/L 1 09/30/10 05:39 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 09/30/10 05:39 74-97-50.50 0.50
Bromodichloromethane 0.63 ug/L 1 09/30/10 05:39 75-27-40.50 0.50
Bromoform ND ug/L 1 09/30/10 05:39 75-25-20.50 0.50
Bromomethane ND ug/L 1 09/30/10 05:39 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 09/30/10 05:39 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 09/30/10 05:39 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 09/30/10 05:39 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 09/30/10 05:39 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 09/30/10 05:39 108-90-70.50 0.50
Chloroethane ND ug/L 1 09/30/10 05:39 75-00-31.0 1.0
Chloroform 39.9 ug/L 1 09/30/10 05:39 67-66-30.50 0.50
Chloromethane ND ug/L 1 09/30/10 05:39 74-87-31.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 22 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:WSW-1 Lab ID:9278272005 Collected:09/22/10 16:00 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
2-Chlorotoluene ND ug/L 1 09/30/10 05:39 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 09/30/10 05:39 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 09/30/10 05:39 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 09/30/10 05:39 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 09/30/10 05:39 106-93-40.50 0.50
Dibromomethane ND ug/L 1 09/30/10 05:39 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 09/30/10 05:39 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 09/30/10 05:39 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 09/30/10 05:39 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 09/30/10 05:39 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 09/30/10 05:39 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 09/30/10 05:39 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 09/30/10 05:39 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 09/30/10 05:39 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 09/30/10 05:39 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 09/30/10 05:39 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 09/30/10 05:39 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 09/30/10 05:39 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 09/30/10 05:39 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 09/30/10 05:39 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 09/30/10 05:39 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 09/30/10 05:39 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 09/30/10 05:39 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 09/30/10 05:39 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 09/30/10 05:39 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 09/30/10 05:39 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 09/30/10 05:39 1634-04-40.50 0.50
Naphthalene ND ug/L 1 09/30/10 05:39 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 09/30/10 05:39 103-65-10.50 0.50
Styrene ND ug/L 1 09/30/10 05:39 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 09/30/10 05:39 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 09/30/10 05:39 79-34-50.50 0.50
Tetrachloroethene ND ug/L 1 09/30/10 05:39 127-18-40.50 0.50
Toluene ND ug/L 1 09/30/10 05:39 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 09/30/10 05:39 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 09/30/10 05:39 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 09/30/10 05:39 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 09/30/10 05:39 79-00-50.50 0.50
Trichloroethene ND ug/L 1 09/30/10 05:39 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 09/30/10 05:39 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 09/30/10 05:39 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 09/30/10 05:39 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 09/30/10 05:39 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 09/30/10 05:39 75-01-41.0 1.0
m&p-Xylene ND ug/L 1 09/30/10 05:39 179601-23-11.0 1.0
o-Xylene ND ug/L 1 09/30/10 05:39 95-47-60.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 23 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:WSW-1 Lab ID:9278272005 Collected:09/22/10 16:00 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
1,2-Dichloroethane-d4 (S)107 %1 09/30/10 05:39 17060-07-070-130
Dibromofluoromethane (S)91 %1 09/30/10 05:39 1868-53-770-130
4-Bromofluorobenzene (S)108 %1 09/30/10 05:39 460-00-470-130
Toluene-d8 (S)96 %1 09/30/10 05:39 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 24 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:WSW-2 Lab ID:9278272006 Collected:09/22/10 16:20 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 10/01/10 01:5209/29/10 09:00104104
Aliphatic (C19-C36)ND ug/L 1 10/01/10 01:5209/29/10 09:00104104
Aromatic (C11-C22)ND ug/L 1 10/01/10 01:5209/29/10 09:00104104
Nonatriacontane (S)78 %1 10/01/10 01:52 7194-86-709/29/10 09:0040-140
o-Terphenyl (S)81 %1 10/01/10 01:52 84-15-109/29/10 09:0040-140
2-Fluorobiphenyl (S)103 %1 10/01/10 01:52 321-60-809/29/10 09:0040-140
2-Bromonaphthalene (S)105 %1 10/01/10 01:52 580-13-209/29/10 09:0040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 09/24/10 19:06100100
Aliphatic (C09-C12)ND ug/L 1 09/24/10 19:06100100
Aromatic (C09-C10)ND ug/L 1 09/24/10 19:06100100
2,5-Dibromotoluene (PID)(S)94 %1 09/24/10 19:0670-130
2,5-Dibromotoluene (FID)(S)108 %1 09/24/10 19:0670-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead ND ug/L 1 10/01/10 07:21 7439-92-109/24/10 10:505.0 4.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 09/29/10 17:57 83-32-909/28/10 13:305.3 3.0
Acenaphthylene ND ug/L 1 09/29/10 17:57 208-96-809/28/10 13:305.3 3.0
Anthracene ND ug/L 1 09/29/10 17:57 120-12-709/28/10 13:305.3 3.1
Benzo(a)anthracene ND ug/L 1 09/29/10 17:57 56-55-309/28/10 13:305.3 3.0
Benzo(a)pyrene ND ug/L 1 09/29/10 17:57 50-32-809/28/10 13:305.3 3.3
Benzo(b)fluoranthene ND ug/L 1 09/29/10 17:57 205-99-209/28/10 13:305.3 3.8
Benzo(g,h,i)perylene ND ug/L 1 09/29/10 17:57 191-24-209/28/10 13:305.3 3.3
Benzo(k)fluoranthene ND ug/L 1 09/29/10 17:57 207-08-909/28/10 13:305.3 3.2
4-Bromophenylphenyl ether ND ug/L 1 09/29/10 17:57 101-55-309/28/10 13:305.3 2.6
Butylbenzylphthalate ND ug/L 1 09/29/10 17:57 85-68-709/28/10 13:305.3 3.1
4-Chloro-3-methylphenol ND ug/L 1 09/29/10 17:57 59-50-709/28/10 13:305.3 3.0
bis(2-Chloroethoxy)methane ND ug/L 1 09/29/10 17:57 111-91-109/28/10 13:3010.6 6.2
bis(2-Chloroethyl) ether ND ug/L 1 09/29/10 17:57 111-44-409/28/10 13:305.3 5.1
bis(2-Chloroisopropyl) ether ND ug/L 1 09/29/10 17:57 108-60-109/28/10 13:305.3 4.3
2-Chloronaphthalene ND ug/L 1 09/29/10 17:57 91-58-709/28/10 13:305.3 3.8
2-Chlorophenol ND ug/L 1 09/29/10 17:57 95-57-809/28/10 13:305.3 4.7
4-Chlorophenylphenyl ether ND ug/L 1 09/29/10 17:57 7005-72-309/28/10 13:305.3 2.9
Chrysene ND ug/L 1 09/29/10 17:57 218-01-909/28/10 13:305.3 2.9
Dibenz(a,h)anthracene ND ug/L 1 09/29/10 17:57 53-70-309/28/10 13:305.3 3.1
3,3'-Dichlorobenzidine ND ug/L 1 09/29/10 17:57 91-94-109/28/10 13:3026.6 3.6
2,4-Dichlorophenol ND ug/L 1 09/29/10 17:57 120-83-209/28/10 13:305.3 4.4
Diethylphthalate ND ug/L 1 09/29/10 17:57 84-66-209/28/10 13:305.3 2.9
2,4-Dimethylphenol ND ug/L 1 09/29/10 17:57 105-67-909/28/10 13:3010.6 6.0
Dimethylphthalate ND ug/L 1 09/29/10 17:57 131-11-309/28/10 13:305.3 2.6
Di-n-butylphthalate ND ug/L 1 09/29/10 17:57 84-74-209/28/10 13:305.3 3.1
4,6-Dinitro-2-methylphenol ND ug/L 1 09/29/10 17:57 534-52-109/28/10 13:3021.3 8.3
2,4-Dinitrophenol ND ug/L 1 09/29/10 17:57 51-28-509/28/10 13:3053.2 10.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 25 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:WSW-2 Lab ID:9278272006 Collected:09/22/10 16:20 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
2,4-Dinitrotoluene ND ug/L 1 09/29/10 17:57 121-14-209/28/10 13:305.3 2.8
2,6-Dinitrotoluene ND ug/L 1 09/29/10 17:57 606-20-209/28/10 13:305.3 3.0
Di-n-octylphthalate ND ug/L 1 09/29/10 17:57 117-84-009/28/10 13:305.3 3.1
bis(2-Ethylhexyl)phthalate ND ug/L 1 09/29/10 17:57 117-81-709/28/10 13:305.3 2.2
Fluoranthene ND ug/L 1 09/29/10 17:57 206-44-009/28/10 13:305.3 3.1
Fluorene ND ug/L 1 09/29/10 17:57 86-73-709/28/10 13:305.3 2.8
Hexachloro-1,3-butadiene ND ug/L 1 09/29/10 17:57 87-68-309/28/10 13:305.3 3.5
Hexachlorobenzene ND ug/L 1 09/29/10 17:57 118-74-109/28/10 13:305.3 2.8
Hexachlorocyclopentadiene ND ug/L 1 09/29/10 17:57 77-47-409/28/10 13:3010.6 3.9
Hexachloroethane ND ug/L 1 09/29/10 17:57 67-72-109/28/10 13:305.3 3.5
Indeno(1,2,3-cd)pyrene ND ug/L 1 09/29/10 17:57 193-39-509/28/10 13:305.3 3.2
Isophorone ND ug/L 1 09/29/10 17:57 78-59-109/28/10 13:3010.6 6.9
2-Methylnaphthalene ND ug/L 1 09/29/10 17:57 91-57-609/28/10 13:305.3 3.6
Naphthalene ND ug/L 1 09/29/10 17:57 91-20-309/28/10 13:305.3 4.0
Nitrobenzene ND ug/L 1 09/29/10 17:57 98-95-309/28/10 13:305.3 4.7
2-Nitrophenol ND ug/L 1 09/29/10 17:57 88-75-509/28/10 13:305.3 4.9
4-Nitrophenol ND ug/L 1 09/29/10 17:57 100-02-709/28/10 13:3053.2 2.1
N-Nitrosodimethylamine ND ug/L 1 09/29/10 17:57 62-75-909/28/10 13:305.3 3.3
N-Nitroso-di-n-propylamine ND ug/L 1 09/29/10 17:57 621-64-709/28/10 13:305.3 3.9
N-Nitrosodiphenylamine ND ug/L 1 09/29/10 17:57 86-30-609/28/10 13:3010.6 7.0
Pentachlorophenol ND ug/L 1 09/29/10 17:57 87-86-509/28/10 13:3026.6 1.7
Phenanthrene ND ug/L 1 09/29/10 17:57 85-01-809/28/10 13:305.3 2.9
Phenol ND ug/L 1 09/29/10 17:57 108-95-209/28/10 13:305.3 1.9
Pyrene ND ug/L 1 09/29/10 17:57 129-00-009/28/10 13:305.3 3.1
1,2,4-Trichlorobenzene ND ug/L 1 09/29/10 17:57 120-82-109/28/10 13:305.3 3.6
2,4,6-Trichlorophenol ND ug/L 1 09/29/10 17:57 88-06-209/28/10 13:3010.6 6.5
Nitrobenzene-d5 (S)61 %1 09/29/10 17:57 4165-60-009/28/10 13:3010-120
2-Fluorobiphenyl (S)62 %1 09/29/10 17:57 321-60-809/28/10 13:3015-120
Terphenyl-d14 (S)71 %1 09/29/10 17:57 1718-51-009/28/10 13:3011-131
Phenol-d6 (S)2 %1 09/29/10 17:57 13127-88-3 S009/28/10 13:3010-120
2-Fluorophenol (S)35 %1 09/29/10 17:57 367-12-409/28/10 13:3010-120
2,4,6-Tribromophenol (S)67 %1 09/29/10 17:57 118-79-609/28/10 13:3010-137
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 09/30/10 06:02 71-43-20.50 0.50
Bromobenzene ND ug/L 1 09/30/10 06:02 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 09/30/10 06:02 74-97-50.50 0.50
Bromodichloromethane 3.1 ug/L 1 09/30/10 06:02 75-27-40.50 0.50
Bromoform 1.7 ug/L 1 09/30/10 06:02 75-25-20.50 0.50
Bromomethane ND ug/L 1 09/30/10 06:02 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 09/30/10 06:02 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 09/30/10 06:02 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 09/30/10 06:02 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 09/30/10 06:02 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 09/30/10 06:02 108-90-70.50 0.50
Chloroethane ND ug/L 1 09/30/10 06:02 75-00-31.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 26 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:WSW-2 Lab ID:9278272006 Collected:09/22/10 16:20 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Chloroform ND ug/L 1 09/30/10 06:02 67-66-30.50 0.50
Chloromethane ND ug/L 1 09/30/10 06:02 74-87-31.0 1.0
2-Chlorotoluene ND ug/L 1 09/30/10 06:02 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 09/30/10 06:02 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 09/30/10 06:02 96-12-81.0 1.0
Dibromochloromethane 3.6 ug/L 1 09/30/10 06:02 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 09/30/10 06:02 106-93-40.50 0.50
Dibromomethane ND ug/L 1 09/30/10 06:02 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 09/30/10 06:02 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 09/30/10 06:02 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 09/30/10 06:02 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 09/30/10 06:02 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 09/30/10 06:02 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 09/30/10 06:02 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 09/30/10 06:02 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 09/30/10 06:02 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 09/30/10 06:02 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 09/30/10 06:02 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 09/30/10 06:02 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 09/30/10 06:02 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 09/30/10 06:02 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 09/30/10 06:02 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 09/30/10 06:02 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 09/30/10 06:02 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 09/30/10 06:02 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 09/30/10 06:02 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 09/30/10 06:02 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 09/30/10 06:02 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 09/30/10 06:02 1634-04-40.50 0.50
Naphthalene ND ug/L 1 09/30/10 06:02 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 09/30/10 06:02 103-65-10.50 0.50
Styrene ND ug/L 1 09/30/10 06:02 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 09/30/10 06:02 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 09/30/10 06:02 79-34-50.50 0.50
Tetrachloroethene ND ug/L 1 09/30/10 06:02 127-18-40.50 0.50
Toluene ND ug/L 1 09/30/10 06:02 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 09/30/10 06:02 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 09/30/10 06:02 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 09/30/10 06:02 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 09/30/10 06:02 79-00-50.50 0.50
Trichloroethene ND ug/L 1 09/30/10 06:02 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 09/30/10 06:02 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 09/30/10 06:02 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 09/30/10 06:02 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 09/30/10 06:02 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 09/30/10 06:02 75-01-41.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 27 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9278272
16143 Agrotec
Sample:WSW-2 Lab ID:9278272006 Collected:09/22/10 16:20 Received:09/23/10 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
m&p-Xylene ND ug/L 1 09/30/10 06:02 179601-23-11.0 1.0
o-Xylene ND ug/L 1 09/30/10 06:02 95-47-60.50 0.50
1,2-Dichloroethane-d4 (S)105 %1 09/30/10 06:02 17060-07-070-130
Dibromofluoromethane (S)86 %1 09/30/10 06:02 1868-53-770-130
4-Bromofluorobenzene (S)110 %1 09/30/10 06:02 460-00-470-130
Toluene-d8 (S)90 %1 09/30/10 06:02 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 28 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9278272
16143 Agrotec
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/11325
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Associated Lab Samples:9278272001, 9278272002, 9278272003, 9278272004, 9278272005, 9278272006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:504315
Associated Lab Samples:9278272001, 9278272002, 9278272003, 9278272004, 9278272005, 9278272006
Matrix:Water
Analyzed
Aliphatic (C09-C18)ug/L ND 100 10/01/10 00:04
Aliphatic (C19-C36)ug/L ND 100 10/01/10 00:04
Aromatic (C11-C22)ug/L ND 100 10/01/10 00:04
2-Bromonaphthalene (S)%90 40-140 10/01/10 00:04
2-Fluorobiphenyl (S)%88 40-140 10/01/10 00:04
Nonatriacontane (S)%76 40-140 10/01/10 00:04
o-Terphenyl (S)%69 40-140 10/01/10 00:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
504316LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
504317
Aliphatic (C09-C18)ug/L 154300 51 40-14067202 27 50
Aliphatic (C19-C36)ug/L 306400 77 40-14085342 11 50
Aromatic (C11-C22)ug/L 547850 64 40-14082695 24 50
2-Bromonaphthalene (S)%80 40-14089
2-Fluorobiphenyl (S)%83 40-14090
Nonatriacontane (S)%73 40-14073
o-Terphenyl (S)%62 40-14078
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 29 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9278272
16143 Agrotec
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/4363
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples:9278272001, 9278272002, 9278272003, 9278272004, 9278272005, 9278272006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:502575
Associated Lab Samples:9278272001, 9278272002, 9278272003, 9278272004, 9278272005, 9278272006
Matrix:Water
Analyzed
Aliphatic (C05-C08)ug/L ND 100 09/24/10 14:56
Aliphatic (C09-C12)ug/L ND 100 09/24/10 14:56
Aromatic (C09-C10)ug/L ND 100 09/24/10 14:56
2,5-Dibromotoluene (FID)(S)%104 70-130 09/24/10 14:56
2,5-Dibromotoluene (PID)(S)%91 70-130 09/24/10 14:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
502576LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
502577
Aliphatic (C05-C08)ug/L 320300 107 70-130101304 5 25
Aliphatic (C09-C12)ug/L 364300 121 30-130119356 2 25
Aromatic (C09-C10)ug/L ND100 93 70-13090ND 25
2,5-Dibromotoluene (FID)(S)%94 70-13088
2,5-Dibromotoluene (PID)(S)%83 70-13077
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 30 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9278272
16143 Agrotec
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/7119
SM 3030C
EPA 200.7
200.7 MET 3030C
Associated Lab Samples:9278272001, 9278272002, 9278272003, 9278272004, 9278272005, 9278272006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:502321
Associated Lab Samples:9278272001, 9278272002, 9278272003, 9278272004, 9278272005, 9278272006
Matrix:Water
Analyzed
Lead ug/L 12.6 5.0 B10/01/10 06:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
502322LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 507500 101 85-115
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
502323MATRIX SPIKE SAMPLE:
MSSpike
Result
9278269001
Lead ug/L 510500 83 70-13096.5
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9278269002
502324SAMPLE DUPLICATE:
Lead ug/L 1340 0 201340
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 31 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9278272
16143 Agrotec
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/11266
EPA 625
EPA 625
625 MSS
Associated Lab Samples:9278272001, 9278272002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:501652
Associated Lab Samples:9278272001, 9278272002
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 09/24/10 13:18
2,4,6-Trichlorophenol ug/L ND 10.0 09/24/10 13:18
2,4-Dichlorophenol ug/L ND 5.0 09/24/10 13:18
2,4-Dimethylphenol ug/L ND 10.0 09/24/10 13:18
2,4-Dinitrophenol ug/L ND 50.0 09/24/10 13:18
2,4-Dinitrotoluene ug/L ND 5.0 09/24/10 13:18
2,6-Dinitrotoluene ug/L ND 5.0 09/24/10 13:18
2-Chloronaphthalene ug/L ND 5.0 09/24/10 13:18
2-Chlorophenol ug/L ND 5.0 09/24/10 13:18
2-Methylnaphthalene ug/L ND 5.0 09/24/10 13:18
2-Nitrophenol ug/L ND 5.0 09/24/10 13:18
3,3'-Dichlorobenzidine ug/L ND 25.0 09/24/10 13:18
4,6-Dinitro-2-methylphenol ug/L ND 20.0 09/24/10 13:18
4-Bromophenylphenyl ether ug/L ND 5.0 09/24/10 13:18
4-Chloro-3-methylphenol ug/L ND 5.0 09/24/10 13:18
4-Chlorophenylphenyl ether ug/L ND 5.0 09/24/10 13:18
4-Nitrophenol ug/L ND 50.0 09/24/10 13:18
Acenaphthene ug/L ND 5.0 09/24/10 13:18
Acenaphthylene ug/L ND 5.0 09/24/10 13:18
Anthracene ug/L ND 5.0 09/24/10 13:18
Benzo(a)anthracene ug/L ND 5.0 09/24/10 13:18
Benzo(a)pyrene ug/L ND 5.0 09/24/10 13:18
Benzo(b)fluoranthene ug/L ND 5.0 09/24/10 13:18
Benzo(g,h,i)perylene ug/L ND 5.0 09/24/10 13:18
Benzo(k)fluoranthene ug/L ND 5.0 09/24/10 13:18
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/24/10 13:18
bis(2-Chloroethyl) ether ug/L ND 5.0 09/24/10 13:18
bis(2-Chloroisopropyl) ether ug/L ND 5.0 09/24/10 13:18
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 09/24/10 13:18
Butylbenzylphthalate ug/L ND 5.0 09/24/10 13:18
Chrysene ug/L ND 5.0 09/24/10 13:18
Di-n-butylphthalate ug/L ND 5.0 09/24/10 13:18
Di-n-octylphthalate ug/L ND 5.0 09/24/10 13:18
Dibenz(a,h)anthracene ug/L ND 5.0 09/24/10 13:18
Diethylphthalate ug/L ND 5.0 09/24/10 13:18
Dimethylphthalate ug/L ND 5.0 09/24/10 13:18
Fluoranthene ug/L ND 5.0 09/24/10 13:18
Fluorene ug/L ND 5.0 09/24/10 13:18
Hexachloro-1,3-butadiene ug/L ND 5.0 09/24/10 13:18
Hexachlorobenzene ug/L ND 5.0 09/24/10 13:18
Hexachlorocyclopentadiene ug/L ND 10.0 09/24/10 13:18
Hexachloroethane ug/L ND 5.0 09/24/10 13:18
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 09/24/10 13:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 32 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9278272
16143 Agrotec
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:501652
Associated Lab Samples:9278272001, 9278272002
Matrix:Water
Analyzed
Isophorone ug/L ND 10.0 09/24/10 13:18
N-Nitroso-di-n-propylamine ug/L ND 5.0 09/24/10 13:18
N-Nitrosodimethylamine ug/L ND 5.0 09/24/10 13:18
N-Nitrosodiphenylamine ug/L ND 10.0 09/24/10 13:18
Naphthalene ug/L ND 5.0 09/24/10 13:18
Nitrobenzene ug/L ND 5.0 09/24/10 13:18
Pentachlorophenol ug/L ND 25.0 09/24/10 13:18
Phenanthrene ug/L ND 5.0 09/24/10 13:18
Phenol ug/L ND 5.0 09/24/10 13:18
Pyrene ug/L ND 5.0 09/24/10 13:18
2,4,6-Tribromophenol (S)%43 10-137 09/24/10 13:18
2-Fluorobiphenyl (S)%38 15-120 09/24/10 13:18
2-Fluorophenol (S)%21 10-120 09/24/10 13:18
Nitrobenzene-d5 (S)%33 10-120 09/24/10 13:18
Phenol-d6 (S)%13 10-120 09/24/10 13:18
Terphenyl-d14 (S)%54 11-131 09/24/10 13:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
501653LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 28.250 56 44-142
2,4,6-Trichlorophenol ug/L 39.950 80 37-144
2,4-Dichlorophenol ug/L 38.550 77 1-191
2,4-Dimethylphenol ug/L 36.550 73 32-119
2,4-Dinitrophenol ug/L 55.2250 22 1-181
2,4-Dinitrotoluene ug/L 42.350 85 39-139
2,6-Dinitrotoluene ug/L 40.450 81 50-158
2-Chloronaphthalene ug/L 37.550 75 60-118
2-Chlorophenol ug/L 34.550 69 23-134
2-Methylnaphthalene ug/L 34.150 68 25-150
2-Nitrophenol ug/L 35.250 70 29-182
3,3'-Dichlorobenzidine ug/L 66.1100 66 1-262
4,6-Dinitro-2-methylphenol ug/L 63.6100 64 1-181
4-Bromophenylphenyl ether ug/L 38.850 78 53-127
4-Chloro-3-methylphenol ug/L 83.0100 83 22-147
4-Chlorophenylphenyl ether ug/L 41.550 83 25-158
4-Nitrophenol ug/L 75.6250 30 1-132
Acenaphthene ug/L 40.850 82 47-145
Acenaphthylene ug/L 40.050 80 33-145
Anthracene ug/L 41.150 82 1-166
Benzo(a)anthracene ug/L 40.350 81 33-143
Benzo(a)pyrene ug/L 39.250 78 17-163
Benzo(b)fluoranthene ug/L 40.050 80 24-159
Benzo(g,h,i)perylene ug/L 40.050 80 1-219
Benzo(k)fluoranthene ug/L 40.350 81 11-162
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 33 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9278272
16143 Agrotec
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
501653LABORATORY CONTROL SAMPLE:
LCSSpike
bis(2-Chloroethoxy)methane ug/L 36.650 73 33-184
bis(2-Chloroethyl) ether ug/L 38.450 77 12-158
bis(2-Chloroisopropyl) ether ug/L 35.850 72 36-166
bis(2-Ethylhexyl)phthalate ug/L 35.950 72 8-158
Butylbenzylphthalate ug/L 35.250 70 1-152
Chrysene ug/L 39.850 80 17-168
Di-n-butylphthalate ug/L 38.350 77 1-118
Di-n-octylphthalate ug/L 34.450 69 4-146
Dibenz(a,h)anthracene ug/L 40.750 81 1-227
Diethylphthalate ug/L 40.050 80 1-114
Dimethylphthalate ug/L 38.750 77 1-112
Fluoranthene ug/L 43.250 86 26-137
Fluorene ug/L 42.650 85 59-121
Hexachloro-1,3-butadiene ug/L 22.350 45 24-116
Hexachlorobenzene ug/L 39.250 78 1-152
Hexachlorocyclopentadiene ug/L 27.650 55 25-150
Hexachloroethane ug/L 22.450 45 40-113
Indeno(1,2,3-cd)pyrene ug/L 39.650 79 1-171
Isophorone ug/L 39.450 79 21-196
N-Nitroso-di-n-propylamine ug/L 41.350 83 1-230
N-Nitrosodimethylamine ug/L 24.650 49 25-150
N-Nitrosodiphenylamine ug/L 40.550 81 25-150
Naphthalene ug/L 34.250 68 21-133
Nitrobenzene ug/L 35.250 70 35-180
Pentachlorophenol ug/L 51.0100 51 14-176
Phenanthrene ug/L 41.250 82 54-120
Phenol ug/L 16.950 34 5-112
Pyrene ug/L 38.150 76 52-115
2,4,6-Tribromophenol (S)%85 10-137
2-Fluorobiphenyl (S)%75 15-120
2-Fluorophenol (S)%43 10-120
Nitrobenzene-d5 (S)%71 10-120
Phenol-d6 (S)%29 10-120
Terphenyl-d14 (S)%76 11-131
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 34 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9278272
16143 Agrotec
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/11304
EPA 625
EPA 625
625 MSS
Associated Lab Samples:9278272003, 9278272004, 9278272005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:503641
Associated Lab Samples:9278272003, 9278272004, 9278272005
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 09/29/10 09:07
2,4,6-Trichlorophenol ug/L ND 10.0 09/29/10 09:07
2,4-Dichlorophenol ug/L ND 5.0 09/29/10 09:07
2,4-Dimethylphenol ug/L ND 10.0 09/29/10 09:07
2,4-Dinitrophenol ug/L ND 50.0 09/29/10 09:07
2,4-Dinitrotoluene ug/L ND 5.0 09/29/10 09:07
2,6-Dinitrotoluene ug/L ND 5.0 09/29/10 09:07
2-Chloronaphthalene ug/L ND 5.0 09/29/10 09:07
2-Chlorophenol ug/L ND 5.0 09/29/10 09:07
2-Methylnaphthalene ug/L ND 5.0 09/29/10 09:07
2-Nitrophenol ug/L ND 5.0 09/29/10 09:07
3,3'-Dichlorobenzidine ug/L ND 25.0 09/29/10 09:07
4,6-Dinitro-2-methylphenol ug/L ND 20.0 09/29/10 09:07
4-Bromophenylphenyl ether ug/L ND 5.0 09/29/10 09:07
4-Chloro-3-methylphenol ug/L ND 5.0 09/29/10 09:07
4-Chlorophenylphenyl ether ug/L ND 5.0 09/29/10 09:07
4-Nitrophenol ug/L 6.9J 50.0 09/29/10 09:07
Acenaphthene ug/L ND 5.0 09/29/10 09:07
Acenaphthylene ug/L ND 5.0 09/29/10 09:07
Anthracene ug/L ND 5.0 09/29/10 09:07
Benzo(a)anthracene ug/L 4.1J 5.0 09/29/10 09:07
Benzo(a)pyrene ug/L ND 5.0 09/29/10 09:07
Benzo(b)fluoranthene ug/L ND 5.0 09/29/10 09:07
Benzo(g,h,i)perylene ug/L ND 5.0 09/29/10 09:07
Benzo(k)fluoranthene ug/L ND 5.0 09/29/10 09:07
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/29/10 09:07
bis(2-Chloroethyl) ether ug/L ND 5.0 09/29/10 09:07
bis(2-Chloroisopropyl) ether ug/L ND 5.0 09/29/10 09:07
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 09/29/10 09:07
Butylbenzylphthalate ug/L 4.1J 5.0 09/29/10 09:07
Chrysene ug/L 4.5J 5.0 09/29/10 09:07
Di-n-butylphthalate ug/L ND 5.0 09/29/10 09:07
Di-n-octylphthalate ug/L ND 5.0 09/29/10 09:07
Dibenz(a,h)anthracene ug/L ND 5.0 09/29/10 09:07
Diethylphthalate ug/L ND 5.0 09/29/10 09:07
Dimethylphthalate ug/L ND 5.0 09/29/10 09:07
Fluoranthene ug/L ND 5.0 09/29/10 09:07
Fluorene ug/L ND 5.0 09/29/10 09:07
Hexachloro-1,3-butadiene ug/L ND 5.0 09/29/10 09:07
Hexachlorobenzene ug/L ND 5.0 09/29/10 09:07
Hexachlorocyclopentadiene ug/L ND 10.0 09/29/10 09:07
Hexachloroethane ug/L ND 5.0 09/29/10 09:07
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 09/29/10 09:07
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 35 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9278272
16143 Agrotec
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:503641
Associated Lab Samples:9278272003, 9278272004, 9278272005
Matrix:Water
Analyzed
Isophorone ug/L ND 10.0 09/29/10 09:07
N-Nitroso-di-n-propylamine ug/L ND 5.0 09/29/10 09:07
N-Nitrosodimethylamine ug/L ND 5.0 09/29/10 09:07
N-Nitrosodiphenylamine ug/L ND 10.0 09/29/10 09:07
Naphthalene ug/L ND 5.0 09/29/10 09:07
Nitrobenzene ug/L ND 5.0 09/29/10 09:07
Pentachlorophenol ug/L 4.8J 25.0 09/29/10 09:07
Phenanthrene ug/L ND 5.0 09/29/10 09:07
Phenol ug/L ND 5.0 09/29/10 09:07
Pyrene ug/L 2.9J 5.0 09/29/10 09:07
2,4,6-Tribromophenol (S)%63 10-137 09/29/10 09:07
2-Fluorobiphenyl (S)%61 15-120 09/29/10 09:07
2-Fluorophenol (S)%39 10-120 09/29/10 09:07
Nitrobenzene-d5 (S)%64 10-120 09/29/10 09:07
Phenol-d6 (S)%24 10-120 09/29/10 09:07
Terphenyl-d14 (S)%89 11-131 09/29/10 09:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
503642LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 25.350 51 44-142
2,4,6-Trichlorophenol ug/L 40.850 82 37-144
2,4-Dichlorophenol ug/L 37.250 74 1-191
2,4-Dimethylphenol ug/L 36.150 72 32-119
2,4-Dinitrophenol ug/L 50.5250 20 1-181
2,4-Dinitrotoluene ug/L 40.650 81 39-139
2,6-Dinitrotoluene ug/L 41.850 84 50-158
2-Chloronaphthalene ug/L 37.050 74 60-118
2-Chlorophenol ug/L 33.550 67 23-134
2-Methylnaphthalene ug/L 29.950 60 25-150
2-Nitrophenol ug/L 36.750 73 29-182
3,3'-Dichlorobenzidine ug/L 53.7100 54 1-262
4,6-Dinitro-2-methylphenol ug/L 55.1100 55 1-181
4-Bromophenylphenyl ether ug/L 39.950 80 53-127
4-Chloro-3-methylphenol ug/L 77.1100 77 22-147
4-Chlorophenylphenyl ether ug/L 40.450 81 25-158
4-Nitrophenol ug/L 58.5250 23 1-132
Acenaphthene ug/L 40.650 81 47-145
Acenaphthylene ug/L 39.650 79 33-145
Anthracene ug/L 41.850 84 1-166
Benzo(a)anthracene ug/L 38.550 77 33-143
Benzo(a)pyrene ug/L 37.550 75 17-163
Benzo(b)fluoranthene ug/L 37.650 75 24-159
Benzo(g,h,i)perylene ug/L 40.650 81 1-219
Benzo(k)fluoranthene ug/L 38.950 78 11-162
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 36 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9278272
16143 Agrotec
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
503642LABORATORY CONTROL SAMPLE:
LCSSpike
bis(2-Chloroethoxy)methane ug/L 34.750 69 33-184
bis(2-Chloroethyl) ether ug/L 36.050 72 12-158
bis(2-Chloroisopropyl) ether ug/L 32.450 65 36-166
bis(2-Ethylhexyl)phthalate ug/L 35.550 71 8-158
Butylbenzylphthalate ug/L 37.850 76 1-152
Chrysene ug/L 38.850 78 17-168
Di-n-butylphthalate ug/L 37.050 74 1-118
Di-n-octylphthalate ug/L 30.750 61 4-146
Dibenz(a,h)anthracene ug/L 40.550 81 1-227
Diethylphthalate ug/L 38.250 76 1-114
Dimethylphthalate ug/L 37.850 76 1-112
Fluoranthene ug/L 39.750 79 26-137
Fluorene ug/L 41.850 84 59-121
Hexachloro-1,3-butadiene ug/L 19.150 38 24-116
Hexachlorobenzene ug/L 40.450 81 1-152
Hexachlorocyclopentadiene ug/L 26.650 53 25-150
Hexachloroethane ug/L 16.8 L2503440-113
Indeno(1,2,3-cd)pyrene ug/L 39.450 79 1-171
Isophorone ug/L 38.050 76 21-196
N-Nitroso-di-n-propylamine ug/L 34.150 68 1-230
N-Nitrosodimethylamine ug/L 25.550 51 25-150
N-Nitrosodiphenylamine ug/L 41.950 84 25-150
Naphthalene ug/L 31.250 62 21-133
Nitrobenzene ug/L 35.350 71 35-180
Pentachlorophenol ug/L 50.3100 50 14-176
Phenanthrene ug/L 41.150 82 54-120
Phenol ug/L 15.950 32 5-112
Pyrene ug/L 44.850 90 52-115
2,4,6-Tribromophenol (S)%73 10-137
2-Fluorobiphenyl (S)%72 15-120
2-Fluorophenol (S)%42 10-120
Nitrobenzene-d5 (S)%71 10-120
Phenol-d6 (S)%26 10-120
Terphenyl-d14 (S)%88 11-131
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 37 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9278272
16143 Agrotec
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/11321
EPA 625
EPA 625
625 MSS
Associated Lab Samples:9278272006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:503973
Associated Lab Samples:9278272006
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 09/29/10 10:30
2,4,6-Trichlorophenol ug/L ND 10.0 09/29/10 10:30
2,4-Dichlorophenol ug/L ND 5.0 09/29/10 10:30
2,4-Dimethylphenol ug/L ND 10.0 09/29/10 10:30
2,4-Dinitrophenol ug/L ND 50.0 09/29/10 10:30
2,4-Dinitrotoluene ug/L ND 5.0 09/29/10 10:30
2,6-Dinitrotoluene ug/L ND 5.0 09/29/10 10:30
2-Chloronaphthalene ug/L ND 5.0 09/29/10 10:30
2-Chlorophenol ug/L ND 5.0 09/29/10 10:30
2-Methylnaphthalene ug/L ND 5.0 09/29/10 10:30
2-Nitrophenol ug/L ND 5.0 09/29/10 10:30
3,3'-Dichlorobenzidine ug/L ND 25.0 09/29/10 10:30
4,6-Dinitro-2-methylphenol ug/L ND 20.0 09/29/10 10:30
4-Bromophenylphenyl ether ug/L ND 5.0 09/29/10 10:30
4-Chloro-3-methylphenol ug/L ND 5.0 09/29/10 10:30
4-Chlorophenylphenyl ether ug/L ND 5.0 09/29/10 10:30
4-Nitrophenol ug/L 4.2J 50.0 09/29/10 10:30
Acenaphthene ug/L ND 5.0 09/29/10 10:30
Acenaphthylene ug/L ND 5.0 09/29/10 10:30
Anthracene ug/L ND 5.0 09/29/10 10:30
Benzo(a)anthracene ug/L 4.4J 5.0 09/29/10 10:30
Benzo(a)pyrene ug/L ND 5.0 09/29/10 10:30
Benzo(b)fluoranthene ug/L ND 5.0 09/29/10 10:30
Benzo(g,h,i)perylene ug/L ND 5.0 09/29/10 10:30
Benzo(k)fluoranthene ug/L ND 5.0 09/29/10 10:30
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/29/10 10:30
bis(2-Chloroethyl) ether ug/L ND 5.0 09/29/10 10:30
bis(2-Chloroisopropyl) ether ug/L ND 5.0 09/29/10 10:30
bis(2-Ethylhexyl)phthalate ug/L 3.3J 5.0 09/29/10 10:30
Butylbenzylphthalate ug/L 3.4J 5.0 09/29/10 10:30
Chrysene ug/L 4.8J 5.0 09/29/10 10:30
Di-n-butylphthalate ug/L ND 5.0 09/29/10 10:30
Di-n-octylphthalate ug/L ND 5.0 09/29/10 10:30
Dibenz(a,h)anthracene ug/L ND 5.0 09/29/10 10:30
Diethylphthalate ug/L ND 5.0 09/29/10 10:30
Dimethylphthalate ug/L ND 5.0 09/29/10 10:30
Fluoranthene ug/L ND 5.0 09/29/10 10:30
Fluorene ug/L ND 5.0 09/29/10 10:30
Hexachloro-1,3-butadiene ug/L ND 5.0 09/29/10 10:30
Hexachlorobenzene ug/L ND 5.0 09/29/10 10:30
Hexachlorocyclopentadiene ug/L ND 10.0 09/29/10 10:30
Hexachloroethane ug/L ND 5.0 09/29/10 10:30
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 09/29/10 10:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 38 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9278272
16143 Agrotec
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:503973
Associated Lab Samples:9278272006
Matrix:Water
Analyzed
Isophorone ug/L ND 10.0 09/29/10 10:30
N-Nitroso-di-n-propylamine ug/L ND 5.0 09/29/10 10:30
N-Nitrosodimethylamine ug/L ND 5.0 09/29/10 10:30
N-Nitrosodiphenylamine ug/L ND 10.0 09/29/10 10:30
Naphthalene ug/L ND 5.0 09/29/10 10:30
Nitrobenzene ug/L ND 5.0 09/29/10 10:30
Pentachlorophenol ug/L 3.1J 25.0 09/29/10 10:30
Phenanthrene ug/L ND 5.0 09/29/10 10:30
Phenol ug/L ND 5.0 09/29/10 10:30
Pyrene ug/L 3.0J 5.0 09/29/10 10:30
2,4,6-Tribromophenol (S)%62 10-137 09/29/10 10:30
2-Fluorobiphenyl (S)%67 15-120 09/29/10 10:30
2-Fluorophenol (S)%36 10-120 09/29/10 10:30
Nitrobenzene-d5 (S)%64 10-120 09/29/10 10:30
Phenol-d6 (S)%25 10-120 09/29/10 10:30
Terphenyl-d14 (S)%82 11-131 09/29/10 10:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
503974LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 19.3 L2503944-142
2,4,6-Trichlorophenol ug/L 31.350 63 37-144
2,4-Dichlorophenol ug/L 24.850 50 1-191
2,4-Dimethylphenol ug/L 23.950 48 32-119
2,4-Dinitrophenol ug/L 61.2250 24 1-181
2,4-Dinitrotoluene ug/L 31.450 63 39-139
2,6-Dinitrotoluene ug/L 33.550 67 50-158
2-Chloronaphthalene ug/L 34.250 68 60-118
2-Chlorophenol ug/L 22.350 45 23-134
2-Methylnaphthalene ug/L 22.750 45 25-150
2-Nitrophenol ug/L 24.550 49 29-182
3,3'-Dichlorobenzidine ug/L 52.7100 53 1-262
4,6-Dinitro-2-methylphenol ug/L 51.8100 52 1-181
4-Bromophenylphenyl ether ug/L 30.850 62 53-127
4-Chloro-3-methylphenol ug/L 49.0100 49 22-147
4-Chlorophenylphenyl ether ug/L 31.550 63 25-158
4-Nitrophenol ug/L 48.0J250 19 1-132
Acenaphthene ug/L 31.950 64 47-145
Acenaphthylene ug/L 31.450 63 33-145
Anthracene ug/L 32.550 65 1-166
Benzo(a)anthracene ug/L 30.050 60 33-143
Benzo(a)pyrene ug/L 29.950 60 17-163
Benzo(b)fluoranthene ug/L 31.450 63 24-159
Benzo(g,h,i)perylene ug/L 33.750 67 1-219
Benzo(k)fluoranthene ug/L 30.350 61 11-162
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 39 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9278272
16143 Agrotec
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
503974LABORATORY CONTROL SAMPLE:
LCSSpike
bis(2-Chloroethoxy)methane ug/L 29.950 60 33-184
bis(2-Chloroethyl) ether ug/L 26.250 52 12-158
bis(2-Chloroisopropyl) ether ug/L 24.950 50 36-166
bis(2-Ethylhexyl)phthalate ug/L 27.450 55 8-158
Butylbenzylphthalate ug/L 28.750 57 1-152
Chrysene ug/L 30.050 60 17-168
Di-n-butylphthalate ug/L 29.350 59 1-118
Di-n-octylphthalate ug/L 26.550 53 4-146
Dibenz(a,h)anthracene ug/L 33.550 67 1-227
Diethylphthalate ug/L 29.350 59 1-114
Dimethylphthalate ug/L 29.050 58 1-112
Fluoranthene ug/L 30.650 61 26-137
Fluorene ug/L 32.850 66 59-121
Hexachloro-1,3-butadiene ug/L 15.350 31 24-116
Hexachlorobenzene ug/L 31.050 62 1-152
Hexachlorocyclopentadiene ug/L 25.250 50 25-150
Hexachloroethane ug/L 17.2 L2503440-113
Indeno(1,2,3-cd)pyrene ug/L 32.850 66 1-171
Isophorone ug/L 25.750 51 21-196
N-Nitroso-di-n-propylamine ug/L 27.950 56 1-230
N-Nitrosodimethylamine ug/L 16.050 32 25-150
N-Nitrosodiphenylamine ug/L 32.550 65 25-150
Naphthalene ug/L 23.250 46 21-133
Nitrobenzene ug/L 23.950 48 35-180
Pentachlorophenol ug/L 44.2100 44 14-176
Phenanthrene ug/L 31.650 63 54-120
Phenol ug/L 11.450 23 5-112
Pyrene ug/L 30.350 61 52-115
2,4,6-Tribromophenol (S)%58 10-137
2-Fluorobiphenyl (S)%57 15-120
2-Fluorophenol (S)%25 10-120
Nitrobenzene-d5 (S)%46 10-120
Phenol-d6 (S)%17 10-120
Terphenyl-d14 (S)%61 11-131
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 40 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9278272
16143 Agrotec
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/12437
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:9278272001, 9278272002, 9278272003, 9278272004, 9278272005, 9278272006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:504566
Associated Lab Samples:9278272001, 9278272002, 9278272003, 9278272004, 9278272005, 9278272006
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 09/29/10 23:10
1,1,1-Trichloroethane ug/L ND 0.50 09/29/10 23:10
1,1,2,2-Tetrachloroethane ug/L ND 0.50 09/29/10 23:10
1,1,2-Trichloroethane ug/L ND 0.50 09/29/10 23:10
1,1-Dichloroethane ug/L ND 0.50 09/29/10 23:10
1,1-Dichloroethene ug/L ND 0.50 09/29/10 23:10
1,1-Dichloropropene ug/L ND 0.50 09/29/10 23:10
1,2,3-Trichlorobenzene ug/L ND 2.0 09/29/10 23:10
1,2,3-Trichloropropane ug/L ND 0.50 09/29/10 23:10
1,2,4-Trichlorobenzene ug/L ND 2.0 09/29/10 23:10
1,2,4-Trimethylbenzene ug/L ND 0.50 09/29/10 23:10
1,2-Dibromo-3-chloropropane ug/L ND 1.0 09/29/10 23:10
1,2-Dibromoethane (EDB)ug/L ND 0.50 09/29/10 23:10
1,2-Dichlorobenzene ug/L ND 0.50 09/29/10 23:10
1,2-Dichloroethane ug/L ND 0.50 09/29/10 23:10
1,2-Dichloropropane ug/L ND 0.50 09/29/10 23:10
1,3,5-Trimethylbenzene ug/L ND 0.50 09/29/10 23:10
1,3-Dichlorobenzene ug/L ND 0.50 09/29/10 23:10
1,3-Dichloropropane ug/L ND 0.50 09/29/10 23:10
1,4-Dichlorobenzene ug/L ND 0.50 09/29/10 23:10
2,2-Dichloropropane ug/L ND 0.50 09/29/10 23:10
2-Chlorotoluene ug/L ND 0.50 09/29/10 23:10
4-Chlorotoluene ug/L ND 0.50 09/29/10 23:10
Benzene ug/L ND 0.50 09/29/10 23:10
Bromobenzene ug/L ND 0.50 09/29/10 23:10
Bromochloromethane ug/L ND 0.50 09/29/10 23:10
Bromodichloromethane ug/L ND 0.50 09/29/10 23:10
Bromoform ug/L ND 0.50 09/29/10 23:10
Bromomethane ug/L ND 5.0 09/29/10 23:10
Carbon tetrachloride ug/L ND 0.50 09/29/10 23:10
Chlorobenzene ug/L ND 0.50 09/29/10 23:10
Chloroethane ug/L ND 1.0 09/29/10 23:10
Chloroform ug/L ND 0.50 09/29/10 23:10
Chloromethane ug/L ND 1.0 09/29/10 23:10
cis-1,2-Dichloroethene ug/L ND 0.50 09/29/10 23:10
cis-1,3-Dichloropropene ug/L ND 0.50 09/29/10 23:10
Dibromochloromethane ug/L ND 0.50 09/29/10 23:10
Dibromomethane ug/L ND 0.50 09/29/10 23:10
Dichlorodifluoromethane ug/L ND 0.50 09/29/10 23:10
Diisopropyl ether ug/L ND 0.50 09/29/10 23:10
Ethylbenzene ug/L ND 0.50 09/29/10 23:10
Hexachloro-1,3-butadiene ug/L ND 2.0 09/29/10 23:10
Isopropylbenzene (Cumene)ug/L ND 0.50 09/29/10 23:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 41 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9278272
16143 Agrotec
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:504566
Associated Lab Samples:9278272001, 9278272002, 9278272003, 9278272004, 9278272005, 9278272006
Matrix:Water
Analyzed
m&p-Xylene ug/L ND 1.0 09/29/10 23:10
Methyl-tert-butyl ether ug/L ND 0.50 09/29/10 23:10
Methylene Chloride ug/L ND 2.0 09/29/10 23:10
n-Butylbenzene ug/L ND 0.50 09/29/10 23:10
n-Propylbenzene ug/L ND 0.50 09/29/10 23:10
Naphthalene ug/L ND 2.0 09/29/10 23:10
o-Xylene ug/L ND 0.50 09/29/10 23:10
sec-Butylbenzene ug/L ND 0.50 09/29/10 23:10
Styrene ug/L ND 0.50 09/29/10 23:10
tert-Butylbenzene ug/L ND 0.50 09/29/10 23:10
Tetrachloroethene ug/L ND 0.50 09/29/10 23:10
Toluene ug/L ND 0.50 09/29/10 23:10
trans-1,2-Dichloroethene ug/L ND 0.50 09/29/10 23:10
trans-1,3-Dichloropropene ug/L ND 0.50 09/29/10 23:10
Trichloroethene ug/L ND 0.50 09/29/10 23:10
Trichlorofluoromethane ug/L ND 1.0 09/29/10 23:10
Vinyl chloride ug/L ND 1.0 09/29/10 23:10
1,2-Dichloroethane-d4 (S)%105 70-130 09/29/10 23:10
4-Bromofluorobenzene (S)%110 70-130 09/29/10 23:10
Dibromofluoromethane (S)%88 70-130 09/29/10 23:10
Toluene-d8 (S)%94 70-130 09/29/10 23:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
504567LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.150 108 60-140
1,1,1-Trichloroethane ug/L 47.350 95 60-140
1,1,2,2-Tetrachloroethane ug/L 51.850 104 60-140
1,1,2-Trichloroethane ug/L 49.250 98 60-140
1,1-Dichloroethane ug/L 37.150 74 60-140
1,1-Dichloroethene ug/L 38.150 76 60-140
1,1-Dichloropropene ug/L 39.550 79 60-140
1,2,3-Trichlorobenzene ug/L 58.650 117 60-140
1,2,3-Trichloropropane ug/L 48.450 97 60-140
1,2,4-Trichlorobenzene ug/L 47.850 96 60-140
1,2,4-Trimethylbenzene ug/L 64.550 129 60-140
1,2-Dibromo-3-chloropropane ug/L 55.750 111 60-140
1,2-Dibromoethane (EDB)ug/L 49.350 99 60-140
1,2-Dichlorobenzene ug/L 50.950 102 60-140
1,2-Dichloroethane ug/L 48.850 98 60-140
1,2-Dichloropropane ug/L 41.850 84 60-140
1,3,5-Trimethylbenzene ug/L 54.150 108 60-140
1,3-Dichlorobenzene ug/L 50.250 100 60-140
1,3-Dichloropropane ug/L 46.850 94 60-140
1,4-Dichlorobenzene ug/L 45.150 90 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 42 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9278272
16143 Agrotec
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
504567LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 35.950 72 60-140
2-Chlorotoluene ug/L 50.850 102 60-140
4-Chlorotoluene ug/L 53.350 107 60-140
Benzene ug/L 43.050 86 60-140
Bromobenzene ug/L 44.450 89 60-140
Bromochloromethane ug/L 37.150 74 60-140
Bromodichloromethane ug/L 52.550 105 60-140
Bromoform ug/L 55.650 111 60-140
Bromomethane ug/L 38.350 77 60-140
Carbon tetrachloride ug/L 57.050 114 60-140
Chlorobenzene ug/L 45.650 91 60-140
Chloroethane ug/L 44.950 90 60-140
Chloroform ug/L 45.850 92 60-140
Chloromethane ug/L 32.250 64 60-140
cis-1,2-Dichloroethene ug/L 36.250 72 60-140
cis-1,3-Dichloropropene ug/L 50.650 101 60-140
Dibromochloromethane ug/L 53.050 106 60-140
Dibromomethane ug/L 53.950 108 60-140
Dichlorodifluoromethane ug/L 39.850 80 60-140
Diisopropyl ether ug/L 37.450 75 60-140
Ethylbenzene ug/L 48.650 97 60-140
Hexachloro-1,3-butadiene ug/L 51.150 102 60-140
Isopropylbenzene (Cumene)ug/L 54.850 110 60-140
m&p-Xylene ug/L 109100 109 60-140
Methyl-tert-butyl ether ug/L 36.250 72 60-140
Methylene Chloride ug/L 48.550 97 60-140
n-Butylbenzene ug/L 52.550 105 60-140
n-Propylbenzene ug/L 50.950 102 60-140
Naphthalene ug/L 49.650 99 60-140
o-Xylene ug/L 58.750 117 60-140
sec-Butylbenzene ug/L 55.950 112 60-140
Styrene ug/L 47.950 96 60-140
tert-Butylbenzene ug/L 59.150 118 60-140
Tetrachloroethene ug/L 52.950 106 60-140
Toluene ug/L 44.650 89 60-140
trans-1,2-Dichloroethene ug/L 35.250 70 60-140
trans-1,3-Dichloropropene ug/L 53.850 108 60-140
Trichloroethene ug/L 52.150 104 60-140
Trichlorofluoromethane ug/L 38.450 77 60-140
Vinyl chloride ug/L 35.850 72 60-140
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%110 70-130
Dibromofluoromethane (S)%88 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 43 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9278272
16143 Agrotec
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
505586MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9277922001
505587
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 127 60-14099 25 3020ND25.5 19.9
1,1,1-Trichloroethane ug/L 20 115 60-14096 18 3020ND23.0 19.2
1,1,2,2-Tetrachloroethane ug/L 20 113 60-14088 25 3020ND22.5 17.6
1,1,2-Trichloroethane ug/L 20 108 60-14087 22 3020ND21.6 17.3
1,1-Dichloroethane ug/L 20 92 60-14074 21 3020ND18.4 14.9
1,1-Dichloroethene ug/L 20 100 60-14076 27 3020ND19.9 15.2
1,1-Dichloropropene ug/L 20 98 60-14079 22 3020ND19.7 15.8
1,2,3-Trichlorobenzene ug/L 20 119 60-14095 22 3020ND23.8 19.0
1,2,3-Trichloropropane ug/L 20 108 60-14093 15 3020ND21.7 18.6
1,2,4-Trichlorobenzene ug/L 20 104 60-14082 24 3020ND20.8 16.4
1,2,4-Trimethylbenzene ug/L 20 117 60-14092 24 3020ND23.4 18.5
1,2-Dibromo-3-chloropropane ug/L 20 128 60-14098 27 3020ND25.6 19.5
1,2-Dibromoethane (EDB)ug/L 20 114 60-14092 21 3020ND22.8 18.5
1,2-Dichlorobenzene ug/L 20 116 60-14095 20 3020ND23.3 19.0
1,2-Dichloroethane ug/L 20 116 60-14094 21 3020ND23.2 18.8
1,2-Dichloropropane ug/L 20 95 60-14074 26 3020ND19.0 14.7
1,3,5-Trimethylbenzene ug/L 20 128 60-140104 21 3020ND25.6 20.8
1,3-Dichlorobenzene ug/L 20 116 60-14095 21 3020ND23.3 18.9
1,3-Dichloropropane ug/L 20 106 60-14086 21 3020ND21.1 17.1
1,4-Dichlorobenzene ug/L 20 104 60-14085 20 3020ND20.9 17.0
2,2-Dichloropropane ug/L 20 77 60-14060 24 3020ND15.3 12.1
2-Chlorotoluene ug/L 20 123 60-140100 20 3020ND24.5 20.1
4-Chlorotoluene ug/L 20 127 60-140104 20 3020ND25.5 20.8
Benzene ug/L 20 104 60-14085 19 3020ND20.7 17.0
Bromobenzene ug/L 20 110 60-14089 21 3020ND22.0 17.8
Bromochloromethane ug/L 20 92 60-14071 26 3020ND18.5 14.2
Bromodichloromethane ug/L 20 115 60-14093 21 3020ND23.0 18.6
Bromoform ug/L 20 117 60-14095 20 3020ND23.4 19.0
Bromomethane ug/L 20 80 60-14070 13 3020ND16.0 14.0
Carbon tetrachloride ug/L 20 127 60-140108 16 3020ND25.5 21.6
Chlorobenzene ug/L 20 111 60-14092 19 3020ND22.2 18.3
Chloroethane ug/L 20 108 60-14087 22 3020ND21.6 17.4
Chloroform ug/L 20 110 60-14081 30 3020ND22.1 16.3
Chloromethane ug/L 20 84 60-14069 20 3020ND17.0 13.9
cis-1,2-Dichloroethene ug/L 20 91 60-14072 23 3020ND18.1 14.4
cis-1,3-Dichloropropene ug/L 20 89 60-14071 22 3020ND17.8 14.2
Dibromochloromethane ug/L 20 119 60-14095 23 3020ND23.9 18.9
Dibromomethane ug/L 20 117 60-14096 20 3020ND23.3 19.2
Dichlorodifluoromethane ug/L 20 115 60-14091 23 3020ND22.9 18.2
Diisopropyl ether ug/L 20 82 60-14063 25 3020ND16.3 12.7
Ethylbenzene ug/L 20 118 60-14096 20 3020ND23.5 19.3
Hexachloro-1,3-butadiene ug/L 20 118 60-140100 16 3020ND23.6 20.0
Isopropylbenzene (Cumene)ug/L 20 123 60-14096 24 3020ND24.6 19.2
m&p-Xylene ug/L 40 131 60-140109 18 3040ND52.5 43.7
Methyl-tert-butyl ether ug/L 20 87 60-14067 25 3020ND17.4 13.5
Methylene Chloride ug/L M0,R1207260-14049 38 3020ND14.4 9.9
n-Butylbenzene ug/L 20 117 60-14095 21 3020ND23.4 18.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 44 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9278272
16143 Agrotec
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
505586MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9277922001
505587
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
n-Propylbenzene ug/L 20 126 60-140102 21 3020ND25.3 20.5
Naphthalene ug/L R12010260-14073 34 3020ND20.5 14.6
o-Xylene ug/L 20 136 60-140108 23 3020ND27.4 21.8
sec-Butylbenzene ug/L 20 133 60-140108 21 3020ND26.6 21.5
Styrene ug/L 20 111 60-14092 19 3020ND22.3 18.4
tert-Butylbenzene ug/L M02014160-140113 22 3020ND28.1 22.5
Tetrachloroethene ug/L 20 127 60-140105 19 3020ND25.4 21.0
Toluene ug/L 20 104 60-14083 22 3020ND20.9 16.7
trans-1,2-Dichloroethene ug/L 20 87 60-14070 22 3020ND17.4 14.0
trans-1,3-Dichloropropene ug/L 20 105 60-14084 23 3020ND21.0 16.7
Trichloroethene ug/L 20 122 60-140100 19 3020ND24.3 20.1
Trichlorofluoromethane ug/L 20 101 60-14078 26 3020ND20.2 15.6
Vinyl chloride ug/L 20 88 60-14071 22 3020ND17.6 14.2
1,2-Dichloroethane-d4 (S)%103 70-130100
4-Bromofluorobenzene (S)%112 70-130113
Dibromofluoromethane (S)%91 70-13090
Toluene-d8 (S)%93 70-13093
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 45 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALIFIERS
Pace Project No.:
Project:
9278272
16143 Agrotec
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Re-extraction or re-analysis could not be performed due to insufficient sample amount.P2
RPD value was outside control limits.R1
Surrogate recovery outside laboratory control limits.S0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 46 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
9278272
16143 Agrotec
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
9278272001 OEXT/11325 GCSV/8461MW-2 MADEP EPH MADEP EPH
9278272002 OEXT/11325 GCSV/8461MW-1 MADEP EPH MADEP EPH
9278272003 OEXT/11325 GCSV/8461WSW-4 MADEP EPH MADEP EPH
9278272004 OEXT/11325 GCSV/8461WSW-3 MADEP EPH MADEP EPH
9278272005 OEXT/11325 GCSV/8461WSW-1 MADEP EPH MADEP EPH
9278272006 OEXT/11325 GCSV/8461WSW-2 MADEP EPH MADEP EPH
9278272001 GCV/4363MW-2 MADEP VPH
9278272002 GCV/4363MW-1 MADEP VPH
9278272003 GCV/4363WSW-4 MADEP VPH
9278272004 GCV/4363WSW-3 MADEP VPH
9278272005 GCV/4363WSW-1 MADEP VPH
9278272006 GCV/4363WSW-2 MADEP VPH
9278272001 MPRP/7119 ICP/6563MW-2 SM 3030C EPA 200.7
9278272002 MPRP/7119 ICP/6563MW-1 SM 3030C EPA 200.7
9278272003 MPRP/7119 ICP/6563WSW-4 SM 3030C EPA 200.7
9278272004 MPRP/7119 ICP/6563WSW-3 SM 3030C EPA 200.7
9278272005 MPRP/7119 ICP/6563WSW-1 SM 3030C EPA 200.7
9278272006 MPRP/7119 ICP/6563WSW-2 SM 3030C EPA 200.7
9278272001 OEXT/11266 MSSV/4041MW-2 EPA 625 EPA 625
9278272002 OEXT/11266 MSSV/4041MW-1 EPA 625 EPA 625
9278272003 OEXT/11304 MSSV/4059WSW-4 EPA 625 EPA 625
9278272004 OEXT/11304 MSSV/4059WSW-3 EPA 625 EPA 625
9278272005 OEXT/11304 MSSV/4059WSW-1 EPA 625 EPA 625
9278272006 OEXT/11321 MSSV/4063WSW-2 EPA 625 EPA 625
9278272001 MSV/12437MW-2 SM 6200B
9278272002 MSV/12437MW-1 SM 6200B
9278272003 MSV/12437WSW-4 SM 6200B
9278272004 MSV/12437WSW-3 SM 6200B
9278272005 MSV/12437WSW-1 SM 6200B
9278272006 MSV/12437WSW-2 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 10/04/2010 04:52 PM Page 47 of 47
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]