RA-2456_15929_CA_MRP_20141216_ECS Final Charles Berryman Report

9001 Glenwood Avenue, Raleigh, NC 27617 • T: 919-861-9910 • F: 800-327-5832 • www.ecslimited.com
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December 16, 2014

Mr. Mark Petermann
NCDENR, Division of Waste Management, UST Section
1637 Mail Service Center
Raleigh, North Carolina 27699-1637

Reference: Groundwater Monitoring Report – Charles Berryman Property
898 Old US Highway 1
Moncure, Chatham County, North Carolina
NCDENR Incident: 15929
NCDENR Contract: N14007i-C
ECS Project: 06:22078

Dear Mr. Petermann:

As authorized by your acceptance of ECS Carolinas, LLP (ECS) Task Authorization Request #1
dated October 6, 2014, ECS has completed the Groundwater Monitoring Report for the above-
referenced site. Included in this report is a description of the field activities, the results obtained, and
our conclusions and recommendations. Information regarding the owner of the former UST, current
property owner, contacts, consultant, laboratory, release information, and latitude and longitude are
presented below.

ECS appreciates the opportunity to provide our environmental consulting services to you on this
project. If you have any questions concerning this report or this project, please contact us at (919)
861-9910.

Sincerely,

ECS CAROLINAS, LLP
Matthew Gillis
Staff Environmental Project Manager

C. Brian Smith, P.G.
Manager of Environmental Services / Principal Geologist

Groundwater Monitoring Report – Charles Berryman Property
Moncure, Chatham County, North Carolina
NCDENR Incident: 15929
NCDENR Contract: N14007i-C
December 16, 2014

SITE INFORMATION

Date of Report: December 16, 2014

Facility I.D.: Unknown
UST Incident No.: 15929
Site Rank: High
Land Use Category: Residential – Currently Vacant Land

Site Name and Location: Charles Berryman Property
898 Old US Highway 1
Moncure, Chatham County, North Carolina

Location Method: Google Earth
Latitude and Longitude: 35.622880 North, 79.076813 West

Contacts

Owner of UST: Mr. Kevin Ronald Stone
901 Old US Highway 1
Moncure, North Carolina 27559
[phone]

Primary Contact: Mr. Kevin Ronald Stone
901 Old US Highway 1
Moncure, North Carolina 27559
[phone]

Consultant: ECS Carolinas, LLP
9001 Glenwood Avenue
Raleigh, North Carolina 27617
[phone]
Attn: Matthew Gillis

Laboratory: Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, North Carolina 28078
[phone]
NC Certification No. 12

Groundwater Monitoring Report – Charles Berryman Property
Moncure, Chatham County, North Carolina
NCDENR Incident: 15929
NCDENR Contract: N14007i-C
December 16, 2014

EXECUTIVE SUMMARY

The subject site is known as the Charles Berryman Property and is located at 898 Old US Highway
1 in Moncure, Chatham County, North Carolina (Figures 1 and 1A). The subject site is further
identified by Chatham County Geographic Information Systems (GIS) Parcel Identification
Number (PIN) 9678-71-1577.

On November 7, 2014, ECS collected five groundwater samples from monitoring wells MW-1
through MW-5 (Figure 2). Additionally, ECS collected one groundwater sample from water
supply well WSW-1 (Figure 6). Well construction and groundwater elevation details are
provided in Table 2.

Laboratory analysis of the groundwater samples collected from monitoring wells MW-1 through
MW-5 reported several targeted analytes at concentrations that exceed their respective North
Carolina 2L Groundwater Quality Standards (NC2LGWQS) but did not exceed their respective
Gross Contamination Levels (GCLs).

Laboratory analysis of the groundwater sample collected from monitoring well MW-5 reported 1,2-
dichloroethane at a concentration that exceeds its respective NC2LGWQS but did not exceed its
respective GCL.

The laboratory did not report targeted analytes at concentrations above the laboratory reporting
limits in the groundwater sample collected from water supply well WSW-1.

A summary of the laboratory analytical results is included in Tables 3 and 4.

The laboratory analytical data sheets and chain of custody records (COCs) are included in
Appendix A.
Groundwater Monitoring Report – Charles Berryman Property
Moncure, Chatham County, North Carolina
NCDENR Incident: 15929
NCDENR Contract: N14007i-C
December 16, 2014

TABLE OF CONTENTS
SITE HISTORY ............................................................................................................... 1 
FIELD ACTIVITIES ......................................................................................................... 3 
CONCLUSIONS .............................................................................................................. 4 
RECOMMENDATIONS ................................................................................................... 5 

FIGURES

Figure 1 Site Location Map
Figure 1A Site Location Map
Figure 2 Monitoring Well Location Map
Figure 3 Groundwater Elevation Map
Figure 4 Groundwater Concentration Map
Figure 5 Benzene Isoconcentration Map
Figure 6 Water Supply Well Location Map
TABLES

Table 1 UST Information
Table 2 Well Construction and Groundwater Elevation Details
Table 3 Summary of Current Groundwater Analytical Results
Table 4 Summary of Historical Groundwater Analytical Results
Table 5 Summary of Historical Soil Sample Analytical Results
Table 6 Water Supply Well Survey

APPENDICIES

Appendix A Laboratory Analytical Data Sheets and Chain of Custody Records
Appendix B ECS Personnel Field Notes
Appendix C Site Photographs
Groundwater Monitoring Report – Charles Berryman Property
Moncure, Chatham County, North Carolina
NCDENR Incident: 15929
NCDENR Contract: N14007i-C
December 16, 2014

1
SITE HISTORY

The subject site is known as the Charles Berryman Property and is located at 898 Old US Highway
1 in Moncure, Chatham County, North Carolina (Figures 1 and 1A). The subject site is further
identified by Chatham County GIS PIN 9678-71-1577.

According to information provided by the NCDENR, the site is a residential property with no
indications of a current/former gasoline retail facility. In 1992, the North Carolina Department of
Transportation (NCDOT) encountered an abandoned underground storage tank (UST) and
apparent petroleum-impacted soils during the installation of a fiber optic line. Since the UST
was encountered adjacent to a 6-inch PVC water line, water samples were collected from the
adjacent residences and analyzed for benzene, toluene, ethylbenzene, and xylenes (BTEX).
Laboratory analysis of the water samples did not report BTEX concentrations above laboratory
reporting limits. The UST was not removed by NCDOT at that time.

In January 1993, one hand auger boring was advanced to a depth of six feet below the ground
surface (ft bgs) between the UST and the Chatham County water line and soil samples were
collected from depths of three and five ft bgs for laboratory analysis. Laboratory results of the
soil sample (CMS-2) collected from five ft bgs interval reported total petroleum hydrocarbons
gasoline range organics (TPH-GRO) above the UST Section’s Action Level of 10 milligrams per
kilogram (mg/kg). The report recommended the removal of the UST. As part of the January
1993 assessment, a second area of suspected contamination was identified. The abandoned
country store (Dupree’s Grocery) had a fuel dispenser in front of the store and it was not known
if a UST remained at this facility. Two additional soil borings were advanced to a depth of six ft
bgs. Field observations of the soil samples collected from the two borings did not exhibit
petroleum impact and therefore, soil samples were not submitted to the laboratory for analysis.

In an effort to determine the existence of a gasoline station associated with the subject site,
historical aerial photographs from 1955, 1960, and 1991 were reviewed. The aerial photographs
depict the presence of two buildings on the property in 1955 and 1960, but only one building in
the 1991 aerial photograph.

In December 2009, a geophysical survey, consisting of an electromagnetic (EM) survey and a
ground penetrating radar (GPR) survey, was conducted near the suspected UST location and
adjacent area. Two anomalies, indicative of USTs, were identified during the geophysical
survey.

In April 2010, one 15,000-gallon gasoline UST (UST-1) and two 550-gallon gasoline USTs
(UST-2 and UST-3) were excavated and removed from the site. The fuel dispensing product
lines and vent lines were also removed at this time. During closure activities, approximately
144.60 tons of petroleum-impacted soils were removed from the vicinity of UST-1. Following
UST closure and soil excavation activities, confirmation soil samples were collected from the
vicinity of the USTs (two samples each beneath UST-2 and UST-3, and four soil samples from
the sidewalls of the UST-1 excavation). Laboratory analysis of soil sample UST-3B reported a
TPH diesel range organics (TPH-DRO) concentration of 10.3 mg/kg, exceeding the UST
Section’s Action Level of 10 mg/kg. Laboratory analysis of one of the four soil samples collected
from the UST-1 excavation reported targeted constituents at concentrations that exceed their
respective soil-to-groundwater maximum soil contaminant concentrations (MSCCs) but below
their respective residential MSCCs.
Groundwater Monitoring Report – Charles Berryman Property
Moncure, Chatham County, North Carolina
NCDENR Incident: 15929
NCDENR Contract: N14007i-C
December 16, 2014

2

In July 2011, a receptor survey was completed for the site. The receptor survey identified 22
water supply wells within 1,500 feet of the source area. Six of the 22 water supply wells (WSW-
5, WSW-8, WSW-9, WSW-10, WSW-19, and WSW-20) were determined to be used for potable
purposes; three of the 22 water supply wells (WSW-11, WSW-15, and WSW-16) were
determined to be used for non-potable purposes (irrigation); nine of the 22 water supply wells
(WSW-2, WSW-3, WSW-4, WSW-6, WSW-12, WSW-13, WSW-14, WSW-17, WSW-18, WSW-
20, and WSW-21) were determined to be inactive; and, the status/use of one of the 22 water
supply wells (WSW-1) could not be determined. Municipal water connections and fire hydrants
were identified throughout the search radius of the survey area and Chatham County Public
Works – Utilities and Water Division confirmed that municipal water is available to each property
within 1,500 feet of the site.

Between July 11 and 13, 2011, as part of a Limited Site Assessment (LSA), five groundwater
monitoring wells (MW-1 through MW-5) were installed and sampled at the site to assess
groundwater quality. Soil samples were collected for laboratory analysis using risk-based
parameters from the borings for monitoring wells MW-1 and MW-2. Laboratory analysis of the
soil samples reported targeted compounds at concentrations that exceed their respective
laboratory reporting limits, but below their respective MSCCs. Laboratory analysis of the
groundwater sample collected from each monitoring well reported targeted petroleum-related
compounds at concentrations that exceed their respective NC2LGWQS, but below their
respective GCLs. Groundwater was determined to be flowing to the south-southeast. The extent
of groundwater impact exceeding NC2LGWQS has not been defined.

SITE GEOLOGY AND HYDROGEOLOGY

As determined from the USGS Topographic Maps, Merry Oaks and Moncure, North Carolina
Quadrangles dated 1993 (Figure 1), the site is at an approximate elevation of 210 feet above
mean sea level. Surface runoff on the site is generally to the east.

The subject site is situated in the Piedmont Physiographic Province. The soils encountered in
this area are the residual product of in-place chemical weathering of rock presently underlying
the site and/or historic depositional events. In general, shallow unconfined groundwater
movement within the overlying soils is controlled largely by topographic gradients. However, as
the groundwater percolates downward, it becomes controlled by the subsurface geologic
conditions. Thus, the direction of groundwater movement in the deeper aquifers may not be
consistent with the reflecting topography.

In general, shallow unconfined groundwater movement within the overlying soils is controlled
largely by topographic gradients. Recharge occurs primarily by infiltration along higher
elevations and typically discharges into streams or other surface water bodies. The elevation of
the shallow water table is transient and can vary greatly with seasonal fluctuations in
precipitation. Movement of shallow groundwater is generally from higher to lower elevations.

Groundwater Monitoring Report – Charles Berryman Property
Moncure, Chatham County, North Carolina
NCDENR Incident: 15929
NCDENR Contract: N14007i-C
December 16, 2014

3

Water Supply Wells

Five previously identified water supply wells are located within 1,000 feet of the source area
(Figure 6). Water supply well questionnaires were mailed via United States Postal Service (USPS)
to the property owners of water supply wells WSW-1, WSW-3, WSW-5, WSW-8, and WSW-9
concerning the status of water supply wells on their property. ECS received written consent
from Ms. Marietta Dixon and ECS received verbal consent from Mrs. Marilyn Berryman to
collect groundwater samples from their water supply wells WSW-9 and WSW-5, respectively.
Both WSW-9 and WSW-5 were inoperable and not in use during the time of our site visit. Ms.
Berryman informed ECS that her residence utilizes the municipal water supply. ECS did not
receive verbal or written consent from Mr. Kenneth Jefferies to collect a groundwater sample
from water supply well WSW-8. Both WSW-1 and WSW-3, which are located on the Raymond
Judd Heirs property, are not in use and inoperable. ECS collected a grab groundwater sample
from WSW-1 using a bailer since the water supply well casing was exposed. The names and
addresses of the property owners with water supply wells located within 1,000 feet of the site
are included in Table 6.

FIELD ACTIVITIES

On November 7, 2014, ECS collected five groundwater samples from monitoring wells MW-1,
through MW-5 (Figure 2). Additionally, ECS collected one groundwater sample from water
supply well WSW-1 (Figure 6). Well construction and groundwater elevation details are
provided in Table 2.

Prior to monitoring well sampling activities, the static groundwater elevation was measured in each
monitoring well. Well construction details and groundwater elevation data is summarized in
Table 2 and shown on Figure 3. Based on the groundwater elevation data, groundwater at the
site generally flows to the east.

Purging and sampling were accomplished using a peristaltic pump and dedicated tubing.
Immediately after collection, the groundwater samples were transferred into sample containers
provided by the laboratory.

ECS utilized a bailer to collect a grab groundwater sample from water supply well WSW-1. ECS
collected the groundwater sample from WSW-1 and poured the groundwater into sample
containers provided by the laboratory.

The sample containers were labeled with ECS project number, sample identification, sample
date and time, and requested analytical analysis. The containers were placed into protective
packaging material and placed into a cooler with ice to maintain the samples at approximately
4 Celsius (C). The samples were submitted to Pace Analytical Services, Inc. located in
Huntersville, North Carolina for chemical analysis for volatile organic compounds (VOCs) using
EPA Method 6200B. ECS maintained proper COC procedures throughout the sample collection
and transportation process.

Groundwater Monitoring Report – Charles Berryman Property
Moncure, Chatham County, North Carolina
NCDENR Incident: 15929
NCDENR Contract: N14007i-C
December 16, 2014

4

LABORATORY ANALYTICAL RESULTS

Laboratory analysis of the groundwater samples collected from monitoring wells MW-1 through
MW-5 reported several targeted analytes at concentrations that exceed their respective
NC2LGWQS but did not exceed their respective GCLs.

Laboratory analysis of the groundwater sample collected from monitoring well MW-5 reported 1,2-
dichloroethane at a concentration that exceeds its respective NC2LGWQS but did not exceed its
respective GCL.

The laboratory did not report targeted analytes at concentrations above the laboratory reporting
limits in the groundwater sample collected from water supply well WSW-1.

A summary of the laboratory analytical results is included in Table 3 and shown on Figures 4 and 5.

A summary of historical groundwater analytical results is included in Table 4.

The laboratory analytical data sheets and COCs are included in Appendix A.

CONCLUSIONS

Based on the results of this Groundwater Sampling Event, ECS concludes the following:

 Based on closure samples collected during excavation activities performed in 2010, it is likely
that petroleum-impacted soils remain at the site;

 Laboratory analysis of the groundwater samples collected from monitoring wells MW-1 through
MW-4 reported several targeted analytes at concentrations that exceed their respective
NC2LGWQS but did not exceed their respective GCLs;

 Laboratory analysis of the groundwater sample collected from monitoring well MW-5 reported
1,2-dichloroethane at a concentration that exceeds its respective NC2LGWQS but did not
exceed its respective GCL; and

 The laboratory did not report targeted analytes at concentrations above the laboratory reporting
limits in the groundwater sample collected from water supply well WSW-1.

Groundwater Monitoring Report – Charles Berryman Property
Moncure, Chatham County, North Carolina
NCDENR Incident: 15929
NCDENR Contract: N14007i-C
December 16, 2014

5

RECOMMENDATIONS

 ECS recommends installing four monitoring wells at the subject site to define the lateral
extent of groundwater contamination. ECS recommends installing a monitoring well
approximately 75 feet west of MW-1, a monitoring well approximately 100 feet north of MW-
1 (Rays Supermarket), a monitoring well approximately 100 feet southwest of MW-4, and a
monitoring well approximately 75 feet east of MW-3;

 ECS recommends performing a survey at the subject site to determine the latitude and
longitude of the monitoring wells and the elevations of the top of each well’s casing;

 ECS recommends collecting groundwater samples from the monitoring wells and water
supply wells on a semi-annual basis; and

 ECS recommends that a copy of this report be submitted to the current property owner as
requested by Mr. Kevin Stone.

FIGURES
SOURCE:
USGS TOPOGRAPHIC MAPS
MERRY OAKS and MONCURE
NC QUADRANGLES
DATED 1993
SCALE: 1 : 24,000
FIGURE 1
SITE LOCATION MAP
CHARLES BERRYMAN PROPERTY
898 OLD US HIGHWAY 1
MONCURE, CHATHAM COUNTY,
NORTH CAROLINA
NCDENR INCIDENT: 15929
ECS PROJECT: 06:22078
SITE
FIGURE 1A
SITE LOCATION MAP
CHARLES BERRYMAN PROPERTY
898 OLD US HIGHWAY 1
MONCURE, CHATHAM COUNTY,
NORTH CAROLINA
NCDENR INCIDENT: 15929
ECS PROJECT: 06:22078
SOURCE:
CHATHAM COUNTY GIS
DATED 2013
SCALE AS SHOWN
SITE
SINGLE-FAMILY
RESIDENCES
1 inch = 100 feet
SINGLE-FAMILY
RESIDENCES
WOODED
UNDEVELOPED
LAND
SOURCE:
CHATHAM COUNTY GIS
DATED 2013
SCALE AS SHOWN
FIGURE 2
MONITORING WELL LOCATION MAP
CHARLES BERRYMAN PROPERTY
898 OLD US HIGHWAY 1
MONCURE, CHATHAM COUNTY,
NORTH CAROLINA
NCDENR INCIDENT: 15929
ECS PROJECT: 06:22078
LEGEND
Approximate Location of
Monitoring Well
Approximate Location of Former USTs
MW-1
MW-4
MW-1
Approximate Location
of Former USTs
MW-2
MW-5
MW-3
1 inch = 50 feet
Storage Shed
SOURCE:
CHATHAM COUNTY GIS
DATED 2013
SCALE AS SHOWN
FIGURE 3
GROUNDWATER ELEVATION MAP
CHARLES BERRYMAN PROPERTY
898 OLD US HIGHWAY 1
MONCURE, CHATHAM COUNTY,
NORTH CAROLINA
NCDENR INCIDENT: 15929
ECS PROJECT: 06:22078
MW-4
85.26
MW-1
85.54
MW-2
85.24
MW-5
84.21
MW-3
83.81
1 inch = 50 feet
LEGEND
Approximate Location of Monitoring Well
Groundwater Elevation
Groundwater Contour Line
Estimated Groundwater Contour Line
Estimated Direction of Groundwater Flow
84.21
85.00
MW-1
84.00
83.00
SOURCE:
CHATHAM COUNTY GIS
DATED 2013
SCALE AS SHOWN
FIGURE 4
GROUNDWATER CONCENTRATION MAP
CHARLES BERRYMAN PROPERTY
898 OLD US HIGHWAY 1
MONCURE, CHATHAM COUNTY,
NORTH CAROLINA
NCDENR INCIDENT: 15929
ECS PROJECT: 06:22078
MW-4
MW-1
Approximate Location
of Former USTs
MW-2
MW-5
MW-3
1 inch = 50 feet
LEGEND
Approximate Location of Monitoring Well
7.0 Concentration Above Laboratory Reporting
Limit (µg/L)
293 Bold Concentration Above the NC2LGWQS
(µg/L)
BRL Below Laboratory Reporting Limit
Benzene 738
Toluene 6.5
Ethylbenzene 67.2
Total Xylenes 188.6
MW-1
Benzene 103
Toluene 1.4
Ethylbenzene 48.1
Total Xylenes 67.7
Benzene 9.2
Toluene BRL
Ethylbenzene BRL
Total Xylenes BRLBenzene293
Toluene 2.8
Ethylbenzene 7.0
Total Xylenes 18.8
Benzene BRL
Toluene BRL
Ethylbenzene BRL
Total Xylenes BRL
SOURCE:
CHATHAM COUNTY GIS
DATED 2013
SCALE AS SHOWN
FIGURE 5
BENZENE ISOCONCENTRATION MAP
CHARLES BERRYMAN PROPERTY
898 OLD US HIGHWAY 1
MONCURE, CHATHAM COUNTY,
NORTH CAROLINA
NCDENR INCIDENT: 15929
ECS PROJECT: 06:22078
MW-4
293
MW-1
738
Approximate Location
of Former USTs
MW-2
103
MW-5
BRL
MW-3
9.2
1 inch = 50 feet
LEGEND
Approximate Location of Monitoring Well
Benzene Isoconcentration Contour (µg/L)
293 Bold Concentration Above the NC2LGWQS
BRL Below Laboratory Reporting Limit
MW-1
100
1
SOURCE:
CHATHAM COUNTY GIS
DATED 2013
SCALE AS SHOWN
FIGURE 6
WATER SUPPLY WELL LOCATION MAP
CHARLES BERRYMAN PROPERTY
898 OLD US HIGHWAY 1
MONCURE, CHATHAM COUNTY,
NORTH CAROLINA
NCDENR INCIDENT: 15929
ECS PROJECT: 06:22078
LEGEND
Approximate Location
of Water Supply Well
500 ft.
Radius 1,000 ft.
Radius
WSW-1
WSW-3
WSW-1
WSW-9
1 inch = 400 feet
WSW-5
WSW-8

TABLES
UST ID NumberLast ContentsPrevious ContentsCapacity (in Gallons)Construction DetailsTank DimensionsInstallation DateRemoval DateStatus1 Gasoline Gasoline 15,000 Unknown Unknown Unknown April 2010 Removed2 Gasoline Gasoline 550 Unknown Unknown Unknown April 2010 Removed3 Gasoline Gasoline 550 Unknown Unknown Unknown April 2010 RemovedMoncure, Chatham County, North CarolinaECS Project: 06:22078Table 1UST InformationCharles Berryman Property898 Old US Highway 1 NCDENR Incident: 15929
Monitoring Well IDDate MeasuredDate InstalledTotal Well Depth (ft. btoc)Well Casing Diameter (in)Screened Interval (ft. btoc)TOC Elevation *Depth to Groundwater (ft. btoc)Groundwater Elevation MW-1 7/13/2011 5/13/2009 31211-3199.6214.08 85.54MW-2 7/13/2011 5/14/2009 2929-2998.9913.75 85.24MW-3 7/13/2011 7/11/2011 27212-2798.0114.2 83.81MW-4 7/13/2011 5/14/2009 32217-3299.5414.28 85.26MW-5 7/13/2011 5/14/2009 35215-3598.6614.45 84.21ft. btoc = Feet Below Top of Casing Table 2Well Construction and Groundwater Elevation DetailsECS Project: 06:22078* = Survey Data according to concrete pad next to the telephone pole located at the northwestern corner of the property (100 foot site datum)Charles Berryman Property898 Old US Highway 1 Moncure, Chatham County, North CarolinaNCDENR Incident: 15929TOC = Top of Casing
Sample IDSample DateMW-111/7/20147386.5 67.2 188.6138 102117 7.9 22.1 28.6 5.7 4.6BRL0.83BRL21.1 1.6MW-211/7/20141031.4 48.1 67.7 13.347.784.2 7.3 16.4 25.3BRL3.6BRL BRL BRL3.1BRLMW-311/7/20149.2BRL BRL BRL3.5 2.7BRL BRL BRL BRL BRL BRL BRL BRL BRL0.54BRLMW-411/7/20142932.8 7.0 18.8 55.822.122.7 5.7 8.5 10.8BRL3.4 1.4BRL BRL11.9BRLMW-511/7/2014BRL BRL BRL BRL51.3BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL7.3BRLWSW-111/7/2014BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL1 600 600 500 70 6 400 400 70 70 70 70 70 70 3 0.4 0.65,000 260,000 84,500 85,500 70,000 6,000 28,500 25,000 25,000 30,000 6,900 8,500 15,000 70,000 3,000 400 600NC2LGWQS = North Carolina 2L Groundwater Quality Standard as of April 1, 2013 GCL = NCDENR's Gross Contamination Levels for Groundwater as of April 16, 2012VOCs = Volatile Organic CompoundsBold= Detected above the NC2LGWQS µg/L = Micrograms per LiterBRL = Below Reporting LimitTotal XylenesDiisopropyl etherTable 3Summary of Current Groundwater Analytical ResultsCharles Berryman Property898 Old US Highway 1 Moncure, Chatham County, North CarolinaNCDEBRL Incident: 159291,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzenen-PropylbenzeneECS Project: 06:22078Analytical MethodVOCs (6200B) (µg/L)Contaminant of Concern (µg/L)BenzeneTolueneEthylbenzeneNC2LGWS (µg/L)GCL (µg/L) ChloroformChloromethane1,2-Dichloroethane1,2-Dichloropropanen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneNaphthalene
Sample IDSample Date7/13/201173.1BRL1.5 22.5BRL87.6 725 4.6 2.5BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL2/28/20138604.4J 39 270BRL110 82130 7.2J 19 13BRL BRL BRL BRL4.4J 5.4JBRL BRL BRL BRL42BRL5.8J11/7/20147386.5 67.2 188.6BRL138 102117 7.9 22.1 28.6BRL BRL BRL BRL5.7 4.6BRL BRL0.83BRL21.1 1.6BRL7/13/201170.82.3 10.1 57.9 1.793.9 6.315.9BRL2.8 1.2BRL BRL BRL BRL BRL BRL BRL BRL BRL2.8BRL BRL BRL2/28/201382017 230750BRL94 93310 42 32 43BRL BRL BRL BRL7.6J 5.2JBRL BRL BRL BRL BRL BRL8.4J11/7/20141031.4 48.1 67.7BRL13.347.784.2 7.3 16.4 25.3BRL BRL BRL BRL BRL3.6BRL BRL BRL BRL3.1BRL BRL7/13/201164.4BRL BRL BRL BRL17 4.3BRL BRL2BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL2/28/201364BRL BRL0.13JBRL17 4.5BRL BRL1.8BRL BRL BRL BRL BRL0.35J 1.3 0.66BRL BRL BRL4.2BRL311/7/20149.2BRL BRL BRL BRL3.5 2.7BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL0.54BRL BRL7/13/2011153BRL8.6 17BRL46.321.836BRL916.9BRLBRL BRL BRL BRL BRL1.6BRL BRL BRL BRL BRL BRL2/28/20132,000BRL BRL48BRL420BRL11BRL6.38J 3.2JBRL BRL BRL BRL BRL BRL BRL BRL BRL BRL120 4JBRL11/7/20142932.8 7.0 18.8BRL55.822.122.7 5.7 8.5 10.8BRL BRL BRL BRL BRL3.4 1.4BRL BRL BRL11.9BRL BRL7/13/20118.7BRL BRL BRL BRL46.9BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL2/28/20131.1BRL BRL BRL BRL53BRL BRL BRL BRL BRL3.5JBRL BRL BRL BRL BRL BRL BRL BRL BRL7.8BRL BRL11/7/2014BRL BRL BRL BRL BRL51.3BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL7.3BRL BRL2/28/201311/7/2014BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLWSW-72/28/2013BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLWSW-82/28/2013BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLWSW-92/28/2013BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL0.41J 114.5BRL BRL BRL514BRL BRL BRL BRL1 600 600 500 20 70 6 400 400 70 70 6,000 NE NE 4 70 70 70 NE 70 3 0.4 0.6 255,000 260,000 84,500 85,500 20,000 70,000 6,000 28,500 25,000 25,000 30,000 6,000,000 NE NE 4,000 6,900 8,500 15,000 NE 70,000 3,000 400 600 11,700NC2LGWQS = North Carolina 2L Groundwater Quality Standard as of April 1, 2013 GCL = NCDENR's Gross Contamination Levels for Groundwater as of April 16, 2012VOCs = Volatile Organic CompoundsBOLD = Detected above the NC2LGWQS J = Detected but below the Reporting Limit; result is an estimated concentrationµg/L = Micrograms per LiterNE = Not EstablishedBRL = Below Reporting LimitContaminant of Concern (µg/L)NC2LGWS (µg/L)Not Sampled-Well InoperableGCL (µg/L) Moncure, Chatham County, North CarolinaECS Project: 06:22078BenzeneTolueneEthylbenzeneTotal XylenesTable 4Summary of Historical Groundwater Analytical ResultsCharles Berryman Property898 Old US Highway 1 VOCs (6200B) (µg/L)Analytical MethodNCDEBRL Incident: 15929Methyl-tert-butyl etherDiisopropyl etherNaphthalene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzeneChlorodibromomethaneChloroformChloromethane1,2-Dichloroethanen-PropylbenzeneAcetoneBromochloromethaneBromodichloromethaneBromoformn-ButylbenzeneMW-5WSW-11,2-Dichloropropanep-IsopropyltolueneMW-1MW-2MW-3MW-4sec-Butylbenzenetert-Butylbenzene
EPA Method 5030CMS-1 1/12/1993 3 9.93NS NS NSCMS-2 1/12/1993 5 218NS NS NSUST-3B 4/7/2010 Unknown 10.3NS NS NS11-13NS3.1 30.1 5.121-23NSBRL BRL BRL6-8NSBRL BRL BRL16-18NSBRL BRL BRL10 NA NA NANA 68 540 31NA 939 1,500 469MSCC = Maximum Soil Contaminant Concentrationmg/kg = milligram per kilogramBRL = Below Reporting Limitft bgs = feet below the ground surfaceNS = Not sampledNA = Not applicableMADEP VPHAnalytical MethodECS Project: 06:22078Table 5Summary of Historical Soil Sample Analytical ResultsCharles Berryman Property898 Old US Highway 1 Moncure, Chatham County, North CarolinaNCDENR Incident: 15929Depth Collected (ft bgs)Soil-to-Groundwater MSCC (mg/kg)C9-C18 AliphaticsResidential MSCC (mg/kg)TPH-GROUST Section's Action Level (mg/kg)SB-2 (MW-2)SB-1 (MW-1)7/12/20117/12/2011Contaminant of Concern (mg/kg)Sample ID Date CollectedC9-C22 AromaticsC5-C8 Aliphatics
Water Supply Well ID Well Owner / Address Well Address Well UseWell Depth (ft bgs)Type of WellApproximate Distance from Source Area of Release (ft)WSW-1Raymond Judd Heirs PO Box 145 Moncure, NC 27559890 Old US1 Moncure, NC 27559Not in use Unknown UnknownApproximately 120 ft southWSW-3Raymond Judd Heirs PO Box 145 Moncure, NC 27559890 Old US1 Moncure, NC 27559Not in use Unknown UnknownApproximately 200 ft southeastWSW-5Mr. and Mrs. Roy and Marilyn Berryman 981 Old US Highway 1 Moncure, NC 27559981 Old US 1 Moncure, NC 27559Not in use Unknown UnknownApproximately 575 ft east-northeastWSW-8Kenneth Jefferies 140 Moncure School Road Moncure, NC 27559140 Moncure School Road Moncure, NC 27559Unknown Approximately 80' UnknownApproximately 825 ft noth-northwestWSW-9Marietta M. Dixon 24 Fairview Cove Road Fairview, NC 28730145 Post Office Road Moncure, NC 27559UnknownDeep Well- owner not sure of totalUnknownApproximately 810 ft southwestft = feetft bgs = feet below the ground surfaceNCDENR Incident: 15929ECS Project: 06:22078Table 6Water Supply Well SurveyCharles Berryman Property898 Old US Highway 1Moncure, Chatham County, North Carolina

APPENDIX A
#=CL#
November 14, 2014
LIMS USE: FR - MATTHEW GILLIS
LIMS OBJECT ID: 92224834
92224834
Project:
Pace Project No.:
RE:
Matthew Gillis
ECS
9001 Glenwood Avenue
Raleigh, NC 27617
Charles Berryman Property
Dear Matthew Gillis:
Enclosed are the analytical results for sample(s) received by the laboratory on November 10, 2014.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
Enclosures
cc: Matthew Gillis, ECS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 30
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92224834
Charles Berryman Property
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 30
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92224834
Charles Berryman Property
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92224834001 MW-1
Benzene 738 ug/L 11/13/14 22:425.0SM 6200B
n-Butylbenzene 5.7 ug/L 11/13/14 10:340.50SM 6200B
sec-Butylbenzene 4.6 ug/L 11/13/14 10:340.50SM 6200B
Chloroform 0.83 ug/L 11/13/14 10:340.50SM 6200B
1,2-Dichloroethane 21.1 ug/L 11/13/14 10:340.50SM 6200B
1,2-Dichloropropane 1.6 ug/L 11/13/14 10:340.50SM 6200B
Diisopropyl ether 138 ug/L 11/13/14 10:340.50SM 6200B
Ethylbenzene 67.2 ug/L 11/13/14 10:340.50SM 6200B
Isopropylbenzene (Cumene)22.1 ug/L 11/13/14 10:340.50SM 6200B
Naphthalene 102 ug/L 11/13/14 10:342.0SM 6200B
n-Propylbenzene 28.6 ug/L 11/13/14 10:340.50SM 6200B
Toluene 6.5 ug/L 11/13/14 10:340.50SM 6200B
1,2,4-Trimethylbenzene 117 ug/L 11/13/14 10:340.50SM 6200B
1,3,5-Trimethylbenzene 7.9 ug/L 11/13/14 10:340.50SM 6200B
m&p-Xylene 120 ug/L 11/13/14 10:341.0SM 6200B
o-Xylene 68.6 ug/L 11/13/14 10:340.50SM 6200B
92224834002 MW-2
Benzene 103 ug/L 11/13/14 10:510.50SM 6200B
sec-Butylbenzene 3.6 ug/L 11/13/14 10:510.50SM 6200B
1,2-Dichloroethane 3.1 ug/L 11/13/14 10:510.50SM 6200B
Diisopropyl ether 13.3 ug/L 11/13/14 10:510.50SM 6200B
Ethylbenzene 48.1 ug/L 11/13/14 10:510.50SM 6200B
Isopropylbenzene (Cumene)16.4 ug/L 11/13/14 10:510.50SM 6200B
Naphthalene 47.7 ug/L 11/13/14 10:512.0SM 6200B
n-Propylbenzene 25.3 ug/L 11/13/14 10:510.50SM 6200B
Toluene 1.4 ug/L 11/13/14 10:510.50SM 6200B
1,2,4-Trimethylbenzene 84.2 ug/L 11/13/14 10:510.50SM 6200B
1,3,5-Trimethylbenzene 7.3 ug/L 11/13/14 10:510.50SM 6200B
m&p-Xylene 46.9 ug/L 11/13/14 10:511.0SM 6200B
o-Xylene 20.8 ug/L 11/13/14 10:510.50SM 6200B
92224834003 MW-3
Benzene 9.2 ug/L 11/13/14 11:080.50SM 6200B
1,2-Dichloroethane 0.54 ug/L 11/13/14 11:080.50SM 6200B
Diisopropyl ether 3.5 ug/L 11/13/14 11:080.50SM 6200B
Naphthalene 2.7 ug/L 11/13/14 11:082.0SM 6200B
92224834004 MW-4
Benzene 293 ug/L 11/13/14 22:582.0SM 6200B
sec-Butylbenzene 3.4 ug/L 11/13/14 11:240.50SM 6200B
tert-Butylbenzene 1.4 ug/L 11/13/14 11:240.50SM 6200B
1,2-Dichloroethane 11.9 ug/L 11/13/14 11:240.50SM 6200B
Diisopropyl ether 55.8 ug/L 11/13/14 11:240.50SM 6200B
Ethylbenzene 7.0 ug/L 11/13/14 11:240.50SM 6200B
Isopropylbenzene (Cumene)8.5 ug/L 11/13/14 11:240.50SM 6200B
Naphthalene 22.1 ug/L 11/13/14 11:242.0SM 6200B
n-Propylbenzene 10.8 ug/L 11/13/14 11:240.50SM 6200B
Toluene 2.8 ug/L 11/13/14 11:240.50SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 30
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92224834
Charles Berryman Property
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92224834004 MW-4
1,2,4-Trimethylbenzene 22.7 ug/L 11/13/14 11:240.50SM 6200B
1,3,5-Trimethylbenzene 5.7 ug/L 11/13/14 11:240.50SM 6200B
m&p-Xylene 6.9 ug/L 11/13/14 11:241.0SM 6200B
o-Xylene 11.9 ug/L 11/13/14 11:240.50SM 6200B
92224834005 MW-5
1,2-Dichloroethane 7.3 ug/L 11/13/14 18:470.50SM 6200B
Diisopropyl ether 51.3 ug/L 11/13/14 18:470.50SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92224834
Charles Berryman Property
Sample: MW-1 Lab ID: 92224834001 Collected: 11/07/14 12:41 Received: 11/10/14 14:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene 738 ug/L 11/13/14 22:42 71-43-25.0 10
Bromobenzene ND ug/L 11/13/14 10:34 108-86-10.50 1
Bromochloromethane ND ug/L 11/13/14 10:34 74-97-50.50 1
Bromodichloromethane ND ug/L 11/13/14 10:34 75-27-40.50 1
Bromoform ND ug/L 11/13/14 10:34 75-25-20.50 1
Bromomethane ND ug/L 11/13/14 10:34 74-83-95.0 1
n-Butylbenzene 5.7 ug/L 11/13/14 10:34 104-51-80.50 1
sec-Butylbenzene 4.6 ug/L 11/13/14 10:34 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/13/14 10:34 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/13/14 10:34 56-23-50.50 1
Chlorobenzene ND ug/L 11/13/14 10:34 108-90-70.50 1
Chloroethane ND ug/L 11/13/14 10:34 75-00-31.0 1
Chloroform 0.83 ug/L 11/13/14 10:34 67-66-30.50 1
Chloromethane ND ug/L 11/13/14 10:34 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/13/14 10:34 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/13/14 10:34 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/13/14 10:34 96-12-81.0 1
Dibromochloromethane ND ug/L 11/13/14 10:34 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/13/14 10:34 106-93-40.50 1
Dibromomethane ND ug/L 11/13/14 10:34 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/13/14 10:34 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/13/14 10:34 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/13/14 10:34 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/13/14 10:34 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/13/14 10:34 75-34-30.50 1
1,2-Dichloroethane 21.1 ug/L 11/13/14 10:34 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/13/14 10:34 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/13/14 10:34 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/13/14 10:34 156-60-50.50 1
1,2-Dichloropropane 1.6 ug/L 11/13/14 10:34 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/13/14 10:34 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/13/14 10:34 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/13/14 10:34 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/13/14 10:34 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/13/14 10:34 10061-02-60.50 1
Diisopropyl ether 138 ug/L 11/13/14 10:34 108-20-30.50 1
Ethylbenzene 67.2 ug/L 11/13/14 10:34 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/13/14 10:34 87-68-32.0 1
Isopropylbenzene (Cumene)22.1 ug/L 11/13/14 10:34 98-82-80.50 1
Methylene Chloride ND ug/L 11/13/14 10:34 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/13/14 10:34 1634-04-40.50 1
Naphthalene 102 ug/L 11/13/14 10:34 91-20-32.0 1
n-Propylbenzene 28.6 ug/L 11/13/14 10:34 103-65-10.50 1
Styrene ND ug/L 11/13/14 10:34 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/13/14 10:34 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/13/14 10:34 79-34-50.50 1
Tetrachloroethene ND ug/L 11/13/14 10:34 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92224834
Charles Berryman Property
Sample: MW-1 Lab ID: 92224834001 Collected: 11/07/14 12:41 Received: 11/10/14 14:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene 6.5 ug/L 11/13/14 10:34 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/13/14 10:34 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/13/14 10:34 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/13/14 10:34 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/13/14 10:34 79-00-50.50 1
Trichloroethene ND ug/L 11/13/14 10:34 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/13/14 10:34 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/13/14 10:34 96-18-40.50 1
1,2,4-Trimethylbenzene 117 ug/L 11/13/14 10:34 95-63-60.50 1
1,3,5-Trimethylbenzene 7.9 ug/L 11/13/14 10:34 108-67-80.50 1
Vinyl chloride ND ug/L 11/13/14 10:34 75-01-41.0 1
m&p-Xylene 120 ug/L 11/13/14 10:34 179601-23-11.0 1
o-Xylene 68.6 ug/L 11/13/14 10:34 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %11/13/14 10:34 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %11/13/14 10:34 460-00-470-130 1
Toluene-d8 (S)100 %11/13/14 10:34 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92224834
Charles Berryman Property
Sample: MW-2 Lab ID: 92224834002 Collected: 11/07/14 11:40 Received: 11/10/14 14:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene 103 ug/L 11/13/14 10:51 71-43-20.50 1
Bromobenzene ND ug/L 11/13/14 10:51 108-86-10.50 1
Bromochloromethane ND ug/L 11/13/14 10:51 74-97-50.50 1
Bromodichloromethane ND ug/L 11/13/14 10:51 75-27-40.50 1
Bromoform ND ug/L 11/13/14 10:51 75-25-20.50 1
Bromomethane ND ug/L 11/13/14 10:51 74-83-95.0 1
n-Butylbenzene ND ug/L 11/13/14 10:51 104-51-80.50 1
sec-Butylbenzene 3.6 ug/L 11/13/14 10:51 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/13/14 10:51 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/13/14 10:51 56-23-50.50 1
Chlorobenzene ND ug/L 11/13/14 10:51 108-90-70.50 1
Chloroethane ND ug/L 11/13/14 10:51 75-00-31.0 1
Chloroform ND ug/L 11/13/14 10:51 67-66-30.50 1
Chloromethane ND ug/L 11/13/14 10:51 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/13/14 10:51 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/13/14 10:51 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/13/14 10:51 96-12-81.0 1
Dibromochloromethane ND ug/L 11/13/14 10:51 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/13/14 10:51 106-93-40.50 1
Dibromomethane ND ug/L 11/13/14 10:51 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/13/14 10:51 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/13/14 10:51 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/13/14 10:51 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/13/14 10:51 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/13/14 10:51 75-34-30.50 1
1,2-Dichloroethane 3.1 ug/L 11/13/14 10:51 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/13/14 10:51 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/13/14 10:51 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/13/14 10:51 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/13/14 10:51 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/13/14 10:51 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/13/14 10:51 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/13/14 10:51 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/13/14 10:51 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/13/14 10:51 10061-02-60.50 1
Diisopropyl ether 13.3 ug/L 11/13/14 10:51 108-20-30.50 1
Ethylbenzene 48.1 ug/L 11/13/14 10:51 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/13/14 10:51 87-68-32.0 1
Isopropylbenzene (Cumene)16.4 ug/L 11/13/14 10:51 98-82-80.50 1
Methylene Chloride ND ug/L 11/13/14 10:51 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/13/14 10:51 1634-04-40.50 1
Naphthalene 47.7 ug/L 11/13/14 10:51 91-20-32.0 1
n-Propylbenzene 25.3 ug/L 11/13/14 10:51 103-65-10.50 1
Styrene ND ug/L 11/13/14 10:51 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/13/14 10:51 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/13/14 10:51 79-34-50.50 1
Tetrachloroethene ND ug/L 11/13/14 10:51 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92224834
Charles Berryman Property
Sample: MW-2 Lab ID: 92224834002 Collected: 11/07/14 11:40 Received: 11/10/14 14:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene 1.4 ug/L 11/13/14 10:51 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/13/14 10:51 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/13/14 10:51 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/13/14 10:51 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/13/14 10:51 79-00-50.50 1
Trichloroethene ND ug/L 11/13/14 10:51 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/13/14 10:51 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/13/14 10:51 96-18-40.50 1
1,2,4-Trimethylbenzene 84.2 ug/L 11/13/14 10:51 95-63-60.50 1
1,3,5-Trimethylbenzene 7.3 ug/L 11/13/14 10:51 108-67-80.50 1
Vinyl chloride ND ug/L 11/13/14 10:51 75-01-41.0 1
m&p-Xylene 46.9 ug/L 11/13/14 10:51 179601-23-11.0 1
o-Xylene 20.8 ug/L 11/13/14 10:51 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)95 %11/13/14 10:51 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %11/13/14 10:51 460-00-470-130 1
Toluene-d8 (S)101 %11/13/14 10:51 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92224834
Charles Berryman Property
Sample: MW-3 Lab ID: 92224834003 Collected: 11/07/14 10:51 Received: 11/10/14 14:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene 9.2 ug/L 11/13/14 11:08 71-43-20.50 1
Bromobenzene ND ug/L 11/13/14 11:08 108-86-10.50 1
Bromochloromethane ND ug/L 11/13/14 11:08 74-97-50.50 1
Bromodichloromethane ND ug/L 11/13/14 11:08 75-27-40.50 1
Bromoform ND ug/L 11/13/14 11:08 75-25-20.50 1
Bromomethane ND ug/L 11/13/14 11:08 74-83-95.0 1
n-Butylbenzene ND ug/L 11/13/14 11:08 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/13/14 11:08 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/13/14 11:08 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/13/14 11:08 56-23-50.50 1
Chlorobenzene ND ug/L 11/13/14 11:08 108-90-70.50 1
Chloroethane ND ug/L 11/13/14 11:08 75-00-31.0 1
Chloroform ND ug/L 11/13/14 11:08 67-66-30.50 1
Chloromethane ND ug/L 11/13/14 11:08 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/13/14 11:08 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/13/14 11:08 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/13/14 11:08 96-12-81.0 1
Dibromochloromethane ND ug/L 11/13/14 11:08 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/13/14 11:08 106-93-40.50 1
Dibromomethane ND ug/L 11/13/14 11:08 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/13/14 11:08 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/13/14 11:08 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/13/14 11:08 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/13/14 11:08 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/13/14 11:08 75-34-30.50 1
1,2-Dichloroethane 0.54 ug/L 11/13/14 11:08 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/13/14 11:08 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/13/14 11:08 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/13/14 11:08 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/13/14 11:08 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/13/14 11:08 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/13/14 11:08 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/13/14 11:08 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/13/14 11:08 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/13/14 11:08 10061-02-60.50 1
Diisopropyl ether 3.5 ug/L 11/13/14 11:08 108-20-30.50 1
Ethylbenzene ND ug/L 11/13/14 11:08 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/13/14 11:08 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/13/14 11:08 98-82-80.50 1
Methylene Chloride ND ug/L 11/13/14 11:08 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/13/14 11:08 1634-04-40.50 1
Naphthalene 2.7 ug/L 11/13/14 11:08 91-20-32.0 1
n-Propylbenzene ND ug/L 11/13/14 11:08 103-65-10.50 1
Styrene ND ug/L 11/13/14 11:08 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/13/14 11:08 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/13/14 11:08 79-34-50.50 1
Tetrachloroethene ND ug/L 11/13/14 11:08 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92224834
Charles Berryman Property
Sample: MW-3 Lab ID: 92224834003 Collected: 11/07/14 10:51 Received: 11/10/14 14:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 11/13/14 11:08 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/13/14 11:08 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/13/14 11:08 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/13/14 11:08 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/13/14 11:08 79-00-50.50 1
Trichloroethene ND ug/L 11/13/14 11:08 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/13/14 11:08 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/13/14 11:08 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/13/14 11:08 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/13/14 11:08 108-67-80.50 1
Vinyl chloride ND ug/L 11/13/14 11:08 75-01-41.0 1
m&p-Xylene ND ug/L 11/13/14 11:08 179601-23-11.0 1
o-Xylene ND ug/L 11/13/14 11:08 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %11/13/14 11:08 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %11/13/14 11:08 460-00-470-130 1
Toluene-d8 (S)101 %11/13/14 11:08 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92224834
Charles Berryman Property
Sample: MW-4 Lab ID: 92224834004 Collected: 11/07/14 13:36 Received: 11/10/14 14:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene 293 ug/L 11/13/14 22:58 71-43-22.0 4
Bromobenzene ND ug/L 11/13/14 11:24 108-86-10.50 1
Bromochloromethane ND ug/L 11/13/14 11:24 74-97-50.50 1
Bromodichloromethane ND ug/L 11/13/14 11:24 75-27-40.50 1
Bromoform ND ug/L 11/13/14 11:24 75-25-20.50 1
Bromomethane ND ug/L 11/13/14 11:24 74-83-95.0 1
n-Butylbenzene ND ug/L 11/13/14 11:24 104-51-80.50 1
sec-Butylbenzene 3.4 ug/L 11/13/14 11:24 135-98-80.50 1
tert-Butylbenzene 1.4 ug/L 11/13/14 11:24 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/13/14 11:24 56-23-50.50 1
Chlorobenzene ND ug/L 11/13/14 11:24 108-90-70.50 1
Chloroethane ND ug/L 11/13/14 11:24 75-00-31.0 1
Chloroform ND ug/L 11/13/14 11:24 67-66-30.50 1
Chloromethane ND ug/L 11/13/14 11:24 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/13/14 11:24 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/13/14 11:24 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/13/14 11:24 96-12-81.0 1
Dibromochloromethane ND ug/L 11/13/14 11:24 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/13/14 11:24 106-93-40.50 1
Dibromomethane ND ug/L 11/13/14 11:24 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/13/14 11:24 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/13/14 11:24 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/13/14 11:24 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/13/14 11:24 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/13/14 11:24 75-34-30.50 1
1,2-Dichloroethane 11.9 ug/L 11/13/14 11:24 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/13/14 11:24 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/13/14 11:24 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/13/14 11:24 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/13/14 11:24 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/13/14 11:24 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/13/14 11:24 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/13/14 11:24 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/13/14 11:24 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/13/14 11:24 10061-02-60.50 1
Diisopropyl ether 55.8 ug/L 11/13/14 11:24 108-20-30.50 1
Ethylbenzene 7.0 ug/L 11/13/14 11:24 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/13/14 11:24 87-68-32.0 1
Isopropylbenzene (Cumene)8.5 ug/L 11/13/14 11:24 98-82-80.50 1
Methylene Chloride ND ug/L 11/13/14 11:24 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/13/14 11:24 1634-04-40.50 1
Naphthalene 22.1 ug/L 11/13/14 11:24 91-20-32.0 1
n-Propylbenzene 10.8 ug/L 11/13/14 11:24 103-65-10.50 1
Styrene ND ug/L 11/13/14 11:24 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/13/14 11:24 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/13/14 11:24 79-34-50.50 1
Tetrachloroethene ND ug/L 11/13/14 11:24 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92224834
Charles Berryman Property
Sample: MW-4 Lab ID: 92224834004 Collected: 11/07/14 13:36 Received: 11/10/14 14:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene 2.8 ug/L 11/13/14 11:24 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/13/14 11:24 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/13/14 11:24 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/13/14 11:24 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/13/14 11:24 79-00-50.50 1
Trichloroethene ND ug/L 11/13/14 11:24 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/13/14 11:24 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/13/14 11:24 96-18-40.50 1
1,2,4-Trimethylbenzene 22.7 ug/L 11/13/14 11:24 95-63-60.50 1
1,3,5-Trimethylbenzene 5.7 ug/L 11/13/14 11:24 108-67-80.50 1
Vinyl chloride ND ug/L 11/13/14 11:24 75-01-41.0 1
m&p-Xylene 6.9 ug/L 11/13/14 11:24 179601-23-11.0 1
o-Xylene 11.9 ug/L 11/13/14 11:24 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)94 %11/13/14 11:24 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %11/13/14 11:24 460-00-470-130 1
Toluene-d8 (S)99 %11/13/14 11:24 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92224834
Charles Berryman Property
Sample: MW-5 Lab ID: 92224834005 Collected: 11/07/14 09:53 Received: 11/10/14 14:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 11/13/14 18:47 71-43-20.50 1
Bromobenzene ND ug/L 11/13/14 18:47 108-86-10.50 1
Bromochloromethane ND ug/L 11/13/14 18:47 74-97-50.50 1
Bromodichloromethane ND ug/L 11/13/14 18:47 75-27-40.50 1
Bromoform ND ug/L 11/13/14 18:47 75-25-20.50 1
Bromomethane ND ug/L 11/13/14 18:47 74-83-95.0 1
n-Butylbenzene ND ug/L 11/13/14 18:47 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/13/14 18:47 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/13/14 18:47 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/13/14 18:47 56-23-50.50 1
Chlorobenzene ND ug/L 11/13/14 18:47 108-90-70.50 1
Chloroethane ND ug/L 11/13/14 18:47 75-00-31.0 1
Chloroform ND ug/L 11/13/14 18:47 67-66-30.50 1
Chloromethane ND ug/L 11/13/14 18:47 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/13/14 18:47 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/13/14 18:47 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/13/14 18:47 96-12-81.0 1
Dibromochloromethane ND ug/L 11/13/14 18:47 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/13/14 18:47 106-93-40.50 1
Dibromomethane ND ug/L 11/13/14 18:47 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/13/14 18:47 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/13/14 18:47 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/13/14 18:47 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/13/14 18:47 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/13/14 18:47 75-34-30.50 1
1,2-Dichloroethane 7.3 ug/L 11/13/14 18:47 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/13/14 18:47 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/13/14 18:47 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/13/14 18:47 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/13/14 18:47 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/13/14 18:47 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/13/14 18:47 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/13/14 18:47 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/13/14 18:47 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/13/14 18:47 10061-02-60.50 1
Diisopropyl ether 51.3 ug/L 11/13/14 18:47 108-20-30.50 1
Ethylbenzene ND ug/L 11/13/14 18:47 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/13/14 18:47 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/13/14 18:47 98-82-80.50 1
Methylene Chloride ND ug/L 11/13/14 18:47 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/13/14 18:47 1634-04-40.50 1
Naphthalene ND ug/L 11/13/14 18:47 91-20-32.0 1
n-Propylbenzene ND ug/L 11/13/14 18:47 103-65-10.50 1
Styrene ND ug/L 11/13/14 18:47 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/13/14 18:47 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/13/14 18:47 79-34-50.50 1
Tetrachloroethene ND ug/L 11/13/14 18:47 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92224834
Charles Berryman Property
Sample: MW-5 Lab ID: 92224834005 Collected: 11/07/14 09:53 Received: 11/10/14 14:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 11/13/14 18:47 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/13/14 18:47 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/13/14 18:47 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/13/14 18:47 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/13/14 18:47 79-00-50.50 1
Trichloroethene ND ug/L 11/13/14 18:47 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/13/14 18:47 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/13/14 18:47 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/13/14 18:47 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/13/14 18:47 108-67-80.50 1
Vinyl chloride ND ug/L 11/13/14 18:47 75-01-41.0 1
m&p-Xylene ND ug/L 11/13/14 18:47 179601-23-11.0 1
o-Xylene ND ug/L 11/13/14 18:47 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)94 %11/13/14 18:47 17060-07-070-130 1
4-Bromofluorobenzene (S)93 %11/13/14 18:47 460-00-470-130 1
Toluene-d8 (S)101 %11/13/14 18:47 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92224834
Charles Berryman Property
Sample: WSW-1 Lab ID: 92224834006 Collected: 11/07/14 14:00 Received: 11/10/14 14:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 11/13/14 17:06 71-43-20.50 1
Bromobenzene ND ug/L 11/13/14 17:06 108-86-10.50 1
Bromochloromethane ND ug/L 11/13/14 17:06 74-97-50.50 1
Bromodichloromethane ND ug/L 11/13/14 17:06 75-27-40.50 1
Bromoform ND ug/L 11/13/14 17:06 75-25-20.50 1
Bromomethane ND ug/L 11/13/14 17:06 74-83-95.0 1
n-Butylbenzene ND ug/L 11/13/14 17:06 104-51-80.50 1
sec-Butylbenzene ND ug/L 11/13/14 17:06 135-98-80.50 1
tert-Butylbenzene ND ug/L 11/13/14 17:06 98-06-60.50 1
Carbon tetrachloride ND ug/L 11/13/14 17:06 56-23-50.50 1
Chlorobenzene ND ug/L 11/13/14 17:06 108-90-70.50 1
Chloroethane ND ug/L 11/13/14 17:06 75-00-31.0 1
Chloroform ND ug/L 11/13/14 17:06 67-66-30.50 1
Chloromethane ND ug/L 11/13/14 17:06 74-87-31.0 1
2-Chlorotoluene ND ug/L 11/13/14 17:06 95-49-80.50 1
4-Chlorotoluene ND ug/L 11/13/14 17:06 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 11/13/14 17:06 96-12-81.0 1
Dibromochloromethane ND ug/L 11/13/14 17:06 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 11/13/14 17:06 106-93-40.50 1
Dibromomethane ND ug/L 11/13/14 17:06 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 11/13/14 17:06 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 11/13/14 17:06 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 11/13/14 17:06 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 11/13/14 17:06 75-71-80.50 1
1,1-Dichloroethane ND ug/L 11/13/14 17:06 75-34-30.50 1
1,2-Dichloroethane ND ug/L 11/13/14 17:06 107-06-20.50 1
1,1-Dichloroethene ND ug/L 11/13/14 17:06 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 11/13/14 17:06 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 11/13/14 17:06 156-60-50.50 1
1,2-Dichloropropane ND ug/L 11/13/14 17:06 78-87-50.50 1
1,3-Dichloropropane ND ug/L 11/13/14 17:06 142-28-90.50 1
2,2-Dichloropropane ND ug/L 11/13/14 17:06 594-20-70.50 1
1,1-Dichloropropene ND ug/L 11/13/14 17:06 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 11/13/14 17:06 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 11/13/14 17:06 10061-02-60.50 1
Diisopropyl ether ND ug/L 11/13/14 17:06 108-20-30.50 1
Ethylbenzene ND ug/L 11/13/14 17:06 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 11/13/14 17:06 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 11/13/14 17:06 98-82-80.50 1
Methylene Chloride ND ug/L 11/13/14 17:06 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 11/13/14 17:06 1634-04-40.50 1
Naphthalene ND ug/L 11/13/14 17:06 91-20-32.0 1
n-Propylbenzene ND ug/L 11/13/14 17:06 103-65-10.50 1
Styrene ND ug/L 11/13/14 17:06 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 11/13/14 17:06 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 11/13/14 17:06 79-34-50.50 1
Tetrachloroethene ND ug/L 11/13/14 17:06 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92224834
Charles Berryman Property
Sample: WSW-1 Lab ID: 92224834006 Collected: 11/07/14 14:00 Received: 11/10/14 14:00 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 11/13/14 17:06 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 11/13/14 17:06 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 11/13/14 17:06 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 11/13/14 17:06 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 11/13/14 17:06 79-00-50.50 1
Trichloroethene ND ug/L 11/13/14 17:06 79-01-60.50 1
Trichlorofluoromethane ND ug/L 11/13/14 17:06 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 11/13/14 17:06 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 11/13/14 17:06 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 11/13/14 17:06 108-67-80.50 1
Vinyl chloride ND ug/L 11/13/14 17:06 75-01-41.0 1
m&p-Xylene ND ug/L 11/13/14 17:06 179601-23-11.0 1
o-Xylene ND ug/L 11/13/14 17:06 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)94 %11/13/14 17:06 17060-07-070-130 1
4-Bromofluorobenzene (S)92 %11/13/14 17:06 460-00-470-130 1
Toluene-d8 (S)100 %11/13/14 17:06 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92224834
Charles Berryman Property
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/29226
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92224834001, 92224834002, 92224834003, 92224834004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1328356
Associated Lab Samples:92224834001, 92224834002, 92224834003, 92224834004
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/13/14 07:46
1,1,1-Trichloroethane ug/L ND 0.50 11/13/14 07:46
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/13/14 07:46
1,1,2-Trichloroethane ug/L ND 0.50 11/13/14 07:46
1,1-Dichloroethane ug/L ND 0.50 11/13/14 07:46
1,1-Dichloroethene ug/L ND 0.50 11/13/14 07:46
1,1-Dichloropropene ug/L ND 0.50 11/13/14 07:46
1,2,3-Trichlorobenzene ug/L ND 2.0 11/13/14 07:46
1,2,3-Trichloropropane ug/L ND 0.50 11/13/14 07:46
1,2,4-Trichlorobenzene ug/L ND 2.0 11/13/14 07:46
1,2,4-Trimethylbenzene ug/L ND 0.50 11/13/14 07:46
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/13/14 07:46
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/13/14 07:46
1,2-Dichlorobenzene ug/L ND 0.50 11/13/14 07:46
1,2-Dichloroethane ug/L ND 0.50 11/13/14 07:46
1,2-Dichloropropane ug/L ND 0.50 11/13/14 07:46
1,3,5-Trimethylbenzene ug/L ND 0.50 11/13/14 07:46
1,3-Dichlorobenzene ug/L ND 0.50 11/13/14 07:46
1,3-Dichloropropane ug/L ND 0.50 11/13/14 07:46
1,4-Dichlorobenzene ug/L ND 0.50 11/13/14 07:46
2,2-Dichloropropane ug/L ND 0.50 11/13/14 07:46
2-Chlorotoluene ug/L ND 0.50 11/13/14 07:46
4-Chlorotoluene ug/L ND 0.50 11/13/14 07:46
Benzene ug/L ND 0.50 11/13/14 07:46
Bromobenzene ug/L ND 0.50 11/13/14 07:46
Bromochloromethane ug/L ND 0.50 11/13/14 07:46
Bromodichloromethane ug/L ND 0.50 11/13/14 07:46
Bromoform ug/L ND 0.50 11/13/14 07:46
Bromomethane ug/L ND 5.0 11/13/14 07:46
Carbon tetrachloride ug/L ND 0.50 11/13/14 07:46
Chlorobenzene ug/L ND 0.50 11/13/14 07:46
Chloroethane ug/L ND 1.0 11/13/14 07:46
Chloroform ug/L ND 0.50 11/13/14 07:46
Chloromethane ug/L ND 1.0 11/13/14 07:46
cis-1,2-Dichloroethene ug/L ND 0.50 11/13/14 07:46
cis-1,3-Dichloropropene ug/L ND 0.50 11/13/14 07:46
Dibromochloromethane ug/L ND 0.50 11/13/14 07:46
Dibromomethane ug/L ND 0.50 11/13/14 07:46
Dichlorodifluoromethane ug/L ND 0.50 11/13/14 07:46
Diisopropyl ether ug/L ND 0.50 11/13/14 07:46
Ethylbenzene ug/L ND 0.50 11/13/14 07:46
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92224834
Charles Berryman Property
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1328356
Associated Lab Samples:92224834001, 92224834002, 92224834003, 92224834004
Matrix: Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 11/13/14 07:46
Isopropylbenzene (Cumene) ug/L ND 0.50 11/13/14 07:46
m&p-Xylene ug/L ND 1.0 11/13/14 07:46
Methyl-tert-butyl ether ug/L ND 0.50 11/13/14 07:46
Methylene Chloride ug/L ND 2.0 11/13/14 07:46
n-Butylbenzene ug/L ND 0.50 11/13/14 07:46
n-Propylbenzene ug/L ND 0.50 11/13/14 07:46
Naphthalene ug/L ND 2.0 11/13/14 07:46
o-Xylene ug/L ND 0.50 11/13/14 07:46
sec-Butylbenzene ug/L ND 0.50 11/13/14 07:46
Styrene ug/L ND 0.50 11/13/14 07:46
tert-Butylbenzene ug/L ND 0.50 11/13/14 07:46
Tetrachloroethene ug/L ND 0.50 11/13/14 07:46
Toluene ug/L ND 0.50 11/13/14 07:46
trans-1,2-Dichloroethene ug/L ND 0.50 11/13/14 07:46
trans-1,3-Dichloropropene ug/L ND 0.50 11/13/14 07:46
Trichloroethene ug/L ND 0.50 11/13/14 07:46
Trichlorofluoromethane ug/L ND 1.0 11/13/14 07:46
Vinyl chloride ug/L ND 1.0 11/13/14 07:46
1,2-Dichloroethane-d4 (S)%95 70-130 11/13/14 07:46
4-Bromofluorobenzene (S)%95 70-130 11/13/14 07:46
Toluene-d8 (S)%100 70-130 11/13/14 07:46
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1328357LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.350 111 60-140
1,1,1-Trichloroethane ug/L 52.150 104 60-140
1,1,2,2-Tetrachloroethane ug/L 53.050 106 60-140
1,1,2-Trichloroethane ug/L 54.850 110 60-140
1,1-Dichloroethane ug/L 53.550 107 60-140
1,1-Dichloroethene ug/L 46.450 93 60-140
1,1-Dichloropropene ug/L 54.650 109 60-140
1,2,3-Trichlorobenzene ug/L 51.450 103 60-140
1,2,3-Trichloropropane ug/L 54.450 109 60-140
1,2,4-Trichlorobenzene ug/L 52.150 104 60-140
1,2,4-Trimethylbenzene ug/L 52.250 104 60-140
1,2-Dibromo-3-chloropropane ug/L 64.650 129 60-140
1,2-Dibromoethane (EDB)ug/L 54.750 109 60-140
1,2-Dichlorobenzene ug/L 51.850 104 60-140
1,2-Dichloroethane ug/L 46.850 94 60-140
1,2-Dichloropropane ug/L 52.050 104 60-140
1,3,5-Trimethylbenzene ug/L 52.250 104 60-140
1,3-Dichlorobenzene ug/L 51.550 103 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92224834
Charles Berryman Property
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1328357LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 53.850 108 60-140
1,4-Dichlorobenzene ug/L 51.450 103 60-140
2,2-Dichloropropane ug/L 44.550 89 60-140
2-Chlorotoluene ug/L 52.050 104 60-140
4-Chlorotoluene ug/L 51.150 102 60-140
Benzene ug/L 52.550 105 60-140
Bromobenzene ug/L 50.350 101 60-140
Bromochloromethane ug/L 53.250 106 60-140
Bromodichloromethane ug/L 50.450 101 60-140
Bromoform ug/L 45.050 90 60-140
Bromomethane ug/L 33.550 67 60-140
Carbon tetrachloride ug/L 54.650 109 60-140
Chlorobenzene ug/L 52.350 105 60-140
Chloroethane ug/L 43.550 87 60-140
Chloroform ug/L 48.350 97 60-140
Chloromethane ug/L 41.250 82 60-140
cis-1,2-Dichloroethene ug/L 53.550 107 60-140
cis-1,3-Dichloropropene ug/L 55.150 110 60-140
Dibromochloromethane ug/L 46.350 93 60-140
Dibromomethane ug/L 54.650 109 60-140
Dichlorodifluoromethane ug/L 43.250 86 60-140
Diisopropyl ether ug/L 51.150 102 60-140
Ethylbenzene ug/L 51.750 103 60-140
Hexachloro-1,3-butadiene ug/L 45.650 91 60-140
Isopropylbenzene (Cumene) ug/L 52.950 106 60-140
m&p-Xylene ug/L 102100 102 60-140
Methyl-tert-butyl ether ug/L 45.850 92 60-140
Methylene Chloride ug/L 48.950 98 60-140
n-Butylbenzene ug/L 50.850 102 60-140
n-Propylbenzene ug/L 51.250 102 60-140
Naphthalene ug/L 52.250 104 60-140
o-Xylene ug/L 50.750 101 60-140
sec-Butylbenzene ug/L 52.350 105 60-140
Styrene ug/L 56.650 113 60-140
tert-Butylbenzene ug/L 45.850 92 60-140
Tetrachloroethene ug/L 47.850 96 60-140
Toluene ug/L 50.950 102 60-140
trans-1,2-Dichloroethene ug/L 45.650 91 60-140
trans-1,3-Dichloropropene ug/L 56.550 113 60-140
Trichloroethene ug/L 51.050 102 60-140
Trichlorofluoromethane ug/L 37.250 74 60-140
Vinyl chloride ug/L 45.950 92 60-140
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92224834
Charles Berryman Property
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1328358MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92224566002
1328359
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 107 60-140101 520ND21.4 20.2
1,1,1-Trichloroethane ug/L M020-270 60-14015 3420194139 197
1,1,2,2-Tetrachloroethane ug/L 20 101 60-14095 520ND20.1 19.1
1,1,2-Trichloroethane ug/L 20 108 60-140101 6204.5 26.1 24.7
1,1-Dichloroethane ug/L E,M0,R12088460-140187 4420212389 250
1,1-Dichloroethene ug/L E,M0,R120116460-140261 5420194427 246
1,1-Dichloropropene ug/L 20 115 60-140109 520ND22.9 21.9
1,2,3-Trichlorobenzene ug/L 20 98 60-14093 520ND19.7 18.6
1,2,3-Trichloropropane ug/L 20 105 60-14097 820ND21.0 19.5
1,2,4-Trichlorobenzene ug/L 20 100 60-14095 520ND20.1 19.1
1,2,4-Trimethylbenzene ug/L 20 101 60-14093 820ND20.2 18.6
1,2-Dibromo-3-chloropropane ug/L 20 116 60-140111 520ND23.2 22.1
1,2-Dibromoethane (EDB) ug/L 20 102 60-14099 320ND20.3 19.7
1,2-Dichlorobenzene ug/L 20 103 60-14097 620ND20.6 19.4
1,2-Dichloroethane ug/L 20 96 60-14086 9205.5 24.7 22.6
1,2-Dichloropropane ug/L 20 102 60-14098 420ND20.3 19.6
1,3,5-Trimethylbenzene ug/L 20 92 60-14086 720ND18.5 17.2
1,3-Dichlorobenzene ug/L 20 105 60-140100 620ND21.1 19.9
1,3-Dichloropropane ug/L 20 103 60-14098 420ND20.6 19.7
1,4-Dichlorobenzene ug/L 20 105 60-14099 620ND20.9 19.7
2,2-Dichloropropane ug/L 20 111 60-140105 520ND22.2 21.0
2-Chlorotoluene ug/L 20 106 60-140101 620ND21.3 20.1
4-Chlorotoluene ug/L 20 104 60-14098 620ND20.9 19.6
Benzene ug/L 20 106 60-14099 620ND21.2 19.9
Bromobenzene ug/L 20 101 60-14095 620ND20.2 19.0
Bromochloromethane ug/L 20 112 60-140106 520ND22.5 21.3
Bromodichloromethane ug/L 20 93 60-14091 2201.0 19.6 19.2
Bromoform ug/L 20 86 60-14085 120ND17.2 16.9
Bromomethane ug/L M0205160-14063 2020ND10.7 13.1
Carbon tetrachloride ug/L 20 107 60-140107 0202.7 24.0 24.1
Chlorobenzene ug/L 20 106 60-140100 720ND21.3 19.9
Chloroethane ug/L 20 92 60-14087 620ND18.5 17.5
Chloroform ug/L 20 96 60-14092 3202.6 21.8 21.1
Chloromethane ug/L 20 83 60-14075 1020ND17.0 15.4
cis-1,2-Dichloroethene ug/L 20 114 60-140103 9202.2 25.1 22.8
cis-1,3-Dichloropropene ug/L 20 100 60-14096 520ND20.1 19.2
Dibromochloromethane ug/L 20 80 60-14077 4201.9 18.0 17.2
Dibromomethane ug/L 20 104 60-14096 720ND20.7 19.3
Dichlorodifluoromethane ug/L 20 83 60-14081 220ND16.6 16.3
Diisopropyl ether ug/L 20 101 60-14094 720ND20.1 18.9
Ethylbenzene ug/L 20 107 60-140101 520ND21.3 20.2
Hexachloro-1,3-butadiene ug/L 20 96 60-14095 120ND19.2 18.9
Isopropylbenzene (Cumene) ug/L 20 108 60-140103 520ND21.6 20.5
m&p-Xylene ug/L 40 103 60-14096 740ND41.1 38.5
Methyl-tert-butyl ether ug/L 20 89 60-14084 520ND17.8 16.9
Methylene Chloride ug/L 20 85 60-14076 1020ND16.9 15.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92224834
Charles Berryman Property
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1328358MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92224566002
1328359
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 107 60-140100 720ND21.4 20.0
n-Propylbenzene ug/L 20 108 60-140102 620ND21.7 20.4
Naphthalene ug/L 20 97 60-14090 720ND19.5 18.1
o-Xylene ug/L 20 100 60-14094 620ND20.0 18.8
sec-Butylbenzene ug/L 20 110 60-140104 620ND22.0 20.8
Styrene ug/L M0202960-14036 2220ND5.9 7.3
tert-Butylbenzene ug/L 20 95 60-14090 520ND19.0 18.1
Tetrachloroethene ug/L 20 102 60-14097 520ND20.7 19.6
Toluene ug/L 20 104 60-14097 720ND21.2 19.8
trans-1,2-Dichloroethene ug/L 20 102 60-14091 11200.82 21.2 19.0
trans-1,3-Dichloropropene ug/L 20 104 60-14098 620ND20.9 19.6
Trichloroethene ug/L 20 104 60-14096 7200.62 21.3 19.9
Trichlorofluoromethane ug/L 20 84 60-14080 520ND17.0 16.2
Vinyl chloride ug/L 20 93 60-14090 420ND18.7 18.0
1,2-Dichloroethane-d4 (S) %94 70-13093
4-Bromofluorobenzene (S) %99 70-13099
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92224834
Charles Berryman Property
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/29244
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92224834005, 92224834006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1329370
Associated Lab Samples:92224834005, 92224834006
Matrix: Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/13/14 16:33
1,1,1-Trichloroethane ug/L ND 0.50 11/13/14 16:33
1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/13/14 16:33
1,1,2-Trichloroethane ug/L ND 0.50 11/13/14 16:33
1,1-Dichloroethane ug/L ND 0.50 11/13/14 16:33
1,1-Dichloroethene ug/L ND 0.50 11/13/14 16:33
1,1-Dichloropropene ug/L ND 0.50 11/13/14 16:33
1,2,3-Trichlorobenzene ug/L ND 2.0 11/13/14 16:33
1,2,3-Trichloropropane ug/L ND 0.50 11/13/14 16:33
1,2,4-Trichlorobenzene ug/L ND 2.0 11/13/14 16:33
1,2,4-Trimethylbenzene ug/L ND 0.50 11/13/14 16:33
1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/13/14 16:33
1,2-Dibromoethane (EDB)ug/L ND 0.50 11/13/14 16:33
1,2-Dichlorobenzene ug/L ND 0.50 11/13/14 16:33
1,2-Dichloroethane ug/L ND 0.50 11/13/14 16:33
1,2-Dichloropropane ug/L ND 0.50 11/13/14 16:33
1,3,5-Trimethylbenzene ug/L ND 0.50 11/13/14 16:33
1,3-Dichlorobenzene ug/L ND 0.50 11/13/14 16:33
1,3-Dichloropropane ug/L ND 0.50 11/13/14 16:33
1,4-Dichlorobenzene ug/L ND 0.50 11/13/14 16:33
2,2-Dichloropropane ug/L ND 0.50 11/13/14 16:33
2-Chlorotoluene ug/L ND 0.50 11/13/14 16:33
4-Chlorotoluene ug/L ND 0.50 11/13/14 16:33
Benzene ug/L ND 0.50 11/13/14 16:33
Bromobenzene ug/L ND 0.50 11/13/14 16:33
Bromochloromethane ug/L ND 0.50 11/13/14 16:33
Bromodichloromethane ug/L ND 0.50 11/13/14 16:33
Bromoform ug/L ND 0.50 11/13/14 16:33
Bromomethane ug/L ND 5.0 11/13/14 16:33
Carbon tetrachloride ug/L ND 0.50 11/13/14 16:33
Chlorobenzene ug/L ND 0.50 11/13/14 16:33
Chloroethane ug/L ND 1.0 11/13/14 16:33
Chloroform ug/L ND 0.50 11/13/14 16:33
Chloromethane ug/L ND 1.0 11/13/14 16:33
cis-1,2-Dichloroethene ug/L ND 0.50 11/13/14 16:33
cis-1,3-Dichloropropene ug/L ND 0.50 11/13/14 16:33
Dibromochloromethane ug/L ND 0.50 11/13/14 16:33
Dibromomethane ug/L ND 0.50 11/13/14 16:33
Dichlorodifluoromethane ug/L ND 0.50 11/13/14 16:33
Diisopropyl ether ug/L ND 0.50 11/13/14 16:33
Ethylbenzene ug/L ND 0.50 11/13/14 16:33
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 22 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92224834
Charles Berryman Property
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 1329370
Associated Lab Samples:92224834005, 92224834006
Matrix: Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 11/13/14 16:33
Isopropylbenzene (Cumene) ug/L ND 0.50 11/13/14 16:33
m&p-Xylene ug/L ND 1.0 11/13/14 16:33
Methyl-tert-butyl ether ug/L ND 0.50 11/13/14 16:33
Methylene Chloride ug/L ND 2.0 11/13/14 16:33
n-Butylbenzene ug/L ND 0.50 11/13/14 16:33
n-Propylbenzene ug/L ND 0.50 11/13/14 16:33
Naphthalene ug/L ND 2.0 11/13/14 16:33
o-Xylene ug/L ND 0.50 11/13/14 16:33
sec-Butylbenzene ug/L ND 0.50 11/13/14 16:33
Styrene ug/L ND 0.50 11/13/14 16:33
tert-Butylbenzene ug/L ND 0.50 11/13/14 16:33
Tetrachloroethene ug/L ND 0.50 11/13/14 16:33
Toluene ug/L ND 0.50 11/13/14 16:33
trans-1,2-Dichloroethene ug/L ND 0.50 11/13/14 16:33
trans-1,3-Dichloropropene ug/L ND 0.50 11/13/14 16:33
Trichloroethene ug/L ND 0.50 11/13/14 16:33
Trichlorofluoromethane ug/L ND 1.0 11/13/14 16:33
Vinyl chloride ug/L ND 1.0 11/13/14 16:33
1,2-Dichloroethane-d4 (S)%94 70-130 11/13/14 16:33
4-Bromofluorobenzene (S)%93 70-130 11/13/14 16:33
Toluene-d8 (S)%101 70-130 11/13/14 16:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1329371LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 63.450 127 60-140
1,1,1-Trichloroethane ug/L 61.950 124 60-140
1,1,2,2-Tetrachloroethane ug/L 59.750 119 60-140
1,1,2-Trichloroethane ug/L 60.550 121 60-140
1,1-Dichloroethane ug/L 62.450 125 60-140
1,1-Dichloroethene ug/L 55.250 110 60-140
1,1-Dichloropropene ug/L 65.250 130 60-140
1,2,3-Trichlorobenzene ug/L 59.750 119 60-140
1,2,3-Trichloropropane ug/L 60.850 122 60-140
1,2,4-Trichlorobenzene ug/L 61.350 123 60-140
1,2,4-Trimethylbenzene ug/L 61.750 123 60-140
1,2-Dibromo-3-chloropropane ug/L 74.4 L350149 60-140
1,2-Dibromoethane (EDB)ug/L 62.550 125 60-140
1,2-Dichlorobenzene ug/L 59.750 119 60-140
1,2-Dichloroethane ug/L 52.850 106 60-140
1,2-Dichloropropane ug/L 60.050 120 60-140
1,3,5-Trimethylbenzene ug/L 62.050 124 60-140
1,3-Dichlorobenzene ug/L 60.850 122 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92224834
Charles Berryman Property
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1329371LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 61.350 123 60-140
1,4-Dichlorobenzene ug/L 59.450 119 60-140
2,2-Dichloropropane ug/L 64.650 129 60-140
2-Chlorotoluene ug/L 61.450 123 60-140
4-Chlorotoluene ug/L 59.950 120 60-140
Benzene ug/L 61.250 122 60-140
Bromobenzene ug/L 57.950 116 60-140
Bromochloromethane ug/L 63.150 126 60-140
Bromodichloromethane ug/L 56.950 114 60-140
Bromoform ug/L 51.050 102 60-140
Bromomethane ug/L 36.450 73 60-140
Carbon tetrachloride ug/L 64.150 128 60-140
Chlorobenzene ug/L 60.450 121 60-140
Chloroethane ug/L 50.050 100 60-140
Chloroform ug/L 56.650 113 60-140
Chloromethane ug/L 49.650 99 60-140
cis-1,2-Dichloroethene ug/L 62.750 125 60-140
cis-1,3-Dichloropropene ug/L 64.050 128 60-140
Dibromochloromethane ug/L 52.950 106 60-140
Dibromomethane ug/L 61.750 123 60-140
Dichlorodifluoromethane ug/L 53.050 106 60-140
Diisopropyl ether ug/L 59.050 118 60-140
Ethylbenzene ug/L 60.950 122 60-140
Hexachloro-1,3-butadiene ug/L 56.950 114 60-140
Isopropylbenzene (Cumene) ug/L 62.350 125 60-140
m&p-Xylene ug/L 120100 120 60-140
Methyl-tert-butyl ether ug/L 52.550 105 60-140
Methylene Chloride ug/L 56.950 114 60-140
n-Butylbenzene ug/L 62.250 124 60-140
n-Propylbenzene ug/L 60.950 122 60-140
Naphthalene ug/L 59.750 119 60-140
o-Xylene ug/L 59.150 118 60-140
sec-Butylbenzene ug/L 62.150 124 60-140
Styrene ug/L 65.550 131 60-140
tert-Butylbenzene ug/L 53.950 108 60-140
Tetrachloroethene ug/L 57.950 116 60-140
Toluene ug/L 59.350 119 60-140
trans-1,2-Dichloroethene ug/L 54.950 110 60-140
trans-1,3-Dichloropropene ug/L 65.350 131 60-140
Trichloroethene ug/L 59.150 118 60-140
Trichlorofluoromethane ug/L 42.650 85 60-140
Vinyl chloride ug/L 56.850 114 60-140
1,2-Dichloroethane-d4 (S)%91 70-130
4-Bromofluorobenzene (S)%100 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92224834
Charles Berryman Property
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1329372MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92224834006
1329373
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 122 60-140129 620ND24.4 25.9
1,1,1-Trichloroethane ug/L 20 122 60-140127 420ND24.3 25.4
1,1,2,2-Tetrachloroethane ug/L 20 115 60-140121 520ND23.1 24.2
1,1,2-Trichloroethane ug/L 20 118 60-140123 420ND23.5 24.5
1,1-Dichloroethane ug/L 20 124 60-140128 320ND24.8 25.6
1,1-Dichloroethene ug/L 20 114 60-140117 320ND22.7 23.3
1,1-Dichloropropene ug/L 20 131 60-140136 420ND26.1 27.2
1,2,3-Trichlorobenzene ug/L 20 116 60-140126 920ND23.2 25.3
1,2,3-Trichloropropane ug/L 20 119 60-140124 420ND23.8 24.7
1,2,4-Trichlorobenzene ug/L 20 116 60-140129 1020ND23.4 25.9
1,2,4-Trimethylbenzene ug/L 20 127 60-140135 620ND25.5 27.1
1,2-Dibromo-3-chloropropane ug/L M02013660-140147 820ND27.3 29.4
1,2-Dibromoethane (EDB) ug/L 20 120 60-140127 620ND24.0 25.5
1,2-Dichlorobenzene ug/L 20 121 60-140129 620ND24.2 25.8
1,2-Dichloroethane ug/L 20 101 60-140105 420ND20.1 21.0
1,2-Dichloropropane ug/L 20 117 60-140124 620ND23.5 24.9
1,3,5-Trimethylbenzene ug/L 20 128 60-140135 620ND25.6 27.1
1,3-Dichlorobenzene ug/L 20 124 60-140131 620ND24.8 26.3
1,3-Dichloropropane ug/L 20 120 60-140125 420ND24.1 25.1
1,4-Dichlorobenzene ug/L 20 119 60-140131 920ND24.2 26.5
2,2-Dichloropropane ug/L 20 113 60-140119 520ND22.6 23.8
2-Chlorotoluene ug/L 20 126 60-140136 720ND25.3 27.2
4-Chlorotoluene ug/L 20 123 60-140132 720ND24.6 26.5
Benzene ug/L 20 123 60-140128 420ND24.6 25.5
Bromobenzene ug/L 20 121 60-140126 420ND24.1 25.2
Bromochloromethane ug/L 20 127 60-140133 420ND25.5 26.5
Bromodichloromethane ug/L 20 105 60-140113 720ND21.0 22.5
Bromoform ug/L 20 93 60-14099 620ND18.6 19.7
Bromomethane ug/L 20 86 60-14080 820ND17.3 16.0
Carbon tetrachloride ug/L 20 127 60-140135 620ND25.4 27.1
Chlorobenzene ug/L 20 122 60-140128 520ND24.4 25.6
Chloroethane ug/L 20 109 60-140108 120ND21.7 21.6
Chloroform ug/L 20 110 60-140114 420ND22.0 22.9
Chloromethane ug/L 20 98 60-140100 220ND19.6 20.0
cis-1,2-Dichloroethene ug/L 20 124 60-140128 320ND24.8 25.5
cis-1,3-Dichloropropene ug/L 20 115 60-140122 620ND22.9 24.4
Dibromochloromethane ug/L 20 100 60-140107 720ND19.9 21.4
Dibromomethane ug/L 20 119 60-140124 520ND23.7 24.8
Dichlorodifluoromethane ug/L 20 115 60-140119 420ND23.0 23.8
Diisopropyl ether ug/L 20 114 60-140120 520ND22.8 23.9
Ethylbenzene ug/L 20 125 60-140130 420ND24.9 26.0
Hexachloro-1,3-butadiene ug/L 20 114 60-140125 920ND22.8 25.0
Isopropylbenzene (Cumene) ug/L 20 127 60-140134 520ND25.3 26.7
m&p-Xylene ug/L 40 120 60-140128 740ND47.9 51.4
Methyl-tert-butyl ether ug/L 20 98 60-140107 820ND19.7 21.3
Methylene Chloride ug/L 20 92 60-14095 320ND18.5 19.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92224834
Charles Berryman Property
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1329372MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92224834006
1329373
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 124 60-140134 820ND24.8 26.9
n-Propylbenzene ug/L 20 127 60-140137 820ND25.4 27.4
Naphthalene ug/L 20 116 60-140127 920ND23.3 25.6
o-Xylene ug/L 20 120 60-140125 520ND23.9 25.0
sec-Butylbenzene ug/L 20 130 60-140139 720ND26.0 27.9
Styrene ug/L 20 126 60-140132 520ND25.1 26.5
tert-Butylbenzene ug/L 20 113 60-140121 720ND22.6 24.2
Tetrachloroethene ug/L 20 118 60-140124 520ND23.6 24.9
Toluene ug/L 20 120 60-140124 420ND23.9 24.9
trans-1,2-Dichloroethene ug/L 20 110 60-140113 320ND22.0 22.6
trans-1,3-Dichloropropene ug/L 20 118 60-140125 620ND23.7 25.0
Trichloroethene ug/L 20 118 60-140122 420ND23.6 24.5
Trichlorofluoromethane ug/L 20 93 60-14096 320ND18.7 19.2
Vinyl chloride ug/L 20 116 60-140123 520ND23.2 24.5
1,2-Dichloroethane-d4 (S) %90 70-13089
4-Bromofluorobenzene (S) %96 70-13097
Toluene-d8 (S)%100 70-130100
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
Pace Analytical Services, Inc.
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Huntersville, NC 28078
[phone]
Page 26 of 30
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92224834
Charles Berryman Property
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits in
associated samples. Results unaffected by high bias.L3
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
Pace Analytical Services, Inc.
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[phone]
Page 27 of 30
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92224834
Charles Berryman Property
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92224834001 MSV/29226MW-1 SM 6200B
92224834002 MSV/29226MW-2 SM 6200B
92224834003 MSV/29226MW-3 SM 6200B
92224834004 MSV/29226MW-4 SM 6200B
92224834005 MSV/29244MW-5 SM 6200B
92224834006 MSV/29244WSW-1 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 11/14/2014 05:55 PM
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Page 28 of 30
Page 29 of 30
Page 30 of 30

APPENDIX B

APPENDIX C

SITE PHOTOGRAPHS
CHARLES BERRYMAN PROPERTY
898 OLD US HIGHWAY 1
MONCURE, CHATHAM COUNTY, NORTH CAROLINA
NCDENR INCIDENT: 15929
ECS PROJECT: 06:22078
Photograph 1: View of the subject site. View is to the southeast.
Photograph 2: View of the subject site. View is to the north
SITE PHOTOGRAPHS
CHARLES BERRYMAN PROPERTY
898 OLD US HIGHWAY 1
MONCURE, CHATHAM COUNTY, NORTH CAROLINA
NCDENR INCIDENT: 15929
ECS PROJECT: 06:22078
Photograph 3: View of the subject site. View is to the southwest.
Photograph 4: View of Ray’s Super Market adjacent to the north of the subject site.
SITE PHOTOGRAPHS
CHARLES BERRYMAN PROPERTY
898 OLD US HIGHWAY 1
MONCURE, CHATHAM COUNTY, NORTH CAROLINA
NCDENR INCIDENT: 15929
ECS PROJECT: 06:22078
Photograph 5: View of MW-2. View is to the north.
Photograph 6: View of WSW-1.