06016_Rad Spec_Tract F Post Const Sampling Approval Rpt&Approval 2014.07.18

1646 Mail Service Center, Raleigh, North Carolina 27699-1646
Phone: [phone] \ Internet: http://portal.ncdenr.org/web/wm
An Equal Opportunity \ Affirmative Action Employer – Made in part by recycled paper

North Carolina Department of Environment and Natural Resources

Pat McCrory
Governor
John E. Skvarla, III
Secretary

July 21, 2014
Sent Via Email

Leo Moretz
Hart & Hickman, PC
3334 Hillsborough Street
Raleigh, NC 27607
[e-mail]

Subject: Approval Post-Grading Sampling Report- Tract F
Radiator Specialty, Bryant Park
Charlotte, Mecklenburg County
Brownfields Project Number 06016-02-60

Dear Mr. Moretz:
On July 18, 2014, the North Carolina Brownfields Program (NCBP) received Bryant Park
Tract F Post-Construction Confirmation Sampling Report prepared by Hart & Hickman. The report
summarized the collection of post-grading sampling and other events. These activities are in
compliance and no further activities are necessary to meet the requirements of Land Use Restriction
Numbers 6 & 7 in the recorded Notice of Brownfields Property.

Be advised that this approval from the NCBP does not waive any applicable requirement to
obtain any necessary permits, licenses or certifications for the above listed activities nor does it
waive any requirement to comply with applicable law for such activities. If you have any questions
or comments, please contact me at 704/661-0330.

Sincerely,

Carolyn Minnich
Carolyn Minnich
Brownfields Project Manager
Division of Waste Management

ec: Bruce Nicholson, NCDENR
George Macon [e-mail]
Ron Weiner [e-mail]
Pete Lash [e-mail]
Chad Grubbs [e-mail]

Bryant Park Tract F
Post-Construction Confirmation
Sampling Report

2001 Suttle Avenue
Charlotte, North Carolina

H&H Job No. BTP-003
July 18, 2014

Via Email

July 18, 2014

NC DENR
Brownfields Section
Division of Waste Management
1314 Mallard Ridge Rd
Tega Cay, SC 29708

Attn: Ms. Carolyn Minnich

Re: Bryant Park Tract F
Post-Construction Confirmation
Sampling Report
2001 Suttle Avenue
Charlotte, North Carolina
H&H Job No. BTP-003

Dear Carolyn:

1.0 Introduction

On behalf of Suttle Avenue, LLC, Hart & Hickman, PC (H&H) is presenting this Post-
Construction Confirmation Sampling Report to document confirmation soil sampling activities at
the Bryant Park Tract F property located at 2001 Suttle Avenue in Charlotte, Mecklenburg
County, North Carolina. A site location map is provided as Figure 1. The purpose of the
sampling was to confirm that exposed shallow soils (up to 5 ft below ground surface (bgs)) do
not contain poly-chlorinated biphenyls (PCBs) above site-specific screening levels as outlined in
the approved Brownfields Agreement (BFA). A brief description of background information is
provided below.

Ms. Carolyn Minnich
July 18, 2014
Page 2
S:\AAA-Master Projects\Bryant Park (BTP-003) Tract F Update 2013\Post-Construction Sampling\Report\Final Bryant Park Post-Grading Sampling Report.docx

2.0 Background Information

The Phase III redevelopment area is comprised of the 2001 Suttle Avenue portion of the site
(historically referred to as Tract F) and the northern portion of the property located at
1900 Wilkinson Boulevard (historically referred to as Tract G). Tract F is located north of
Tract G (Figure 2). Phase III redevelopment involved site grading and construction of a charter
school, and surface parking lots.

Environmental conditions at the Brownfields property have been documented by data presented
in the Results of Site Assessment Activities prepared by Hart & Hickman, PC (August 19, 2002),
in the Supplemental Soil Sampling Activities report (February 20, 2007), and in the H&H
Additional Soil Sampling Activities (Tract F) report dated November 3, 2008. The data available
from the Phase III area is summarized and compared to current screening criteria in the Soil
Management Plan for “Areas of Known Contamination” dated July 18, 2013 (SMP). This SMP
was approved by DENR on July 19, 2013. The SMP required a work plan for sampling in areas
of exposed soils following the completion of grading activities. Therefore, H&H submitted a
Post-Construction Sampling and Analysis Plan dated January 22, 2014 (SAP) which was
subsequently approved by DENR on January 24, 2014. The scope of work described below
includes the sampling required in the SAP.

3.0 Scope of Work

Collection of Post-Grading Samples
H&H collected composite soil samples on May 30 and June 2, 2014 in accordance with the SAP.
The sample aliquots were collected using decontaminated stainless steel hand augers, composited
as detailed in the SAP, and placed into laboratory provided glassware. The samples were
immediately placed on ice and delivered to the laboratory under chain of custody protocol. The
composite samples were submitted to Pace Analytical Services, Inc. (Pace) in Huntersville,
North Carolina for laboratory analysis of PCBs by EPA Method 8082. The laboratory analytical
Ms. Carolyn Minnich
July 18, 2014
Page 3
S:\AAA-Master Projects\Bryant Park (BTP-003) Tract F Update 2013\Post-Construction Sampling\Report\Final Bryant Park Post-Grading Sampling Report.docx

results are summarized on Table 1 and the analytical data sheets are included in Appendix A.
According to the BFA, the total PCB concentration in exposed areas of soil to a depth of 5 ft bgs
must be below one (1) part per million PCBs. No PCB concentrations exceeded the 1 mg/kg
criteria except in two adjacent samples. PCB-1248 was detected at a concentration of
2.33 mg/kg in the 0-2 ft bgs composite sample from the designated “Area F” and at a
concentration 4.80 mg/kg in the 0-2 ft bgs composite sample from the designated “Area E”.
These contiguous areas are shown on Figure 2.

Additional Soil Excavation
Since the composite sampling data indicated the designated “Areas E and F” had concentrations
of PCBs in shallow (0-2 ft bgs) soil above the site specific screening criteria, H&H contacted
DENR regarding additional soil removal. In an emailed work plan, H&H indicated that the areas
of known soil contamination designated “Areas E and F” during the post-grading sampling
would be excavated and transported for off-site disposal, and would be backfilled with imported
fill from a known source. After backfilling, two additional composite samples for PCB analysis
would be collected from the backfilled excavated area at a 0-2 ft depth interval, which is
consistent with the sampling activities approved in the SAP. In an email dated June 30, 2014
DENR approved the proposed corrective action (Appendix B).

H&H contracted A&D Environmental Services (A&D) to excavate the impacted soil. On July 7
and 8, 2014 the PCB-containing soil from the areas designated “Areas E and F” was excavated,
loaded into dump trucks, and transported to the Republic landfill Services, Inc. (Republic)
landfill in Concord, NC. H&H provided oversight of the excavation, and confirmed the extent of
the excavation included Areas E and F, and field measured the dimensions of the excavation
which was 76 ft in length by 10 ft in width and 5 ft in depth. A total of 159.33 tons of soil was
removed and disposed at the Republic Services landfill in Concord, NC. Completed manifests
and weight tickets are provided in Appendix C.

Ms. Carolyn Minnich
July 18, 2014
Page 4
S:\AAA-Master Projects\Bryant Park (BTP-003) Tract F Update 2013\Post-Construction Sampling\Report\Final Bryant Park Post-Grading Sampling Report.docx

Upon completion of the excavation, A&D backfilled the excavation using clean fill from the
Martin-Marietta Aggregates Quarry located at 4551 Beatties Ford Rd in Charlotte, NC.

Backfill Analysis
In accordance with DENR requirements, H&H used a decontaminated hand auger to collect
additional composite samples in the backfilled excavation at a depth of 0-2 ft. The samples
(labeled as E-Backfill and F-Backfill) were collected in laboratory provided glassware, placed on
ice, and delivered to Pace under chain of custody protocol. The samples were submitted for
laboratory analysis of PCBs by EPA Method 8082. The analytical results of the two samples
collected indicated that no PCBs were detected above laboratory detection limits. Analytical
results are provided on Table 1 and laboratory results are provided in Appendix C.

4.0 Summary and Conclusion

Post-grading sampling indicated no PCBs above the site specific screening criteria, with the
exception of two locations. The soil within the areas of known soil contamination designated
“Areas E and F” was found to contain PCBs above 1 ppm. Therefore, in accordance with the
BFA, the impacted soil was excavated and removed from the site for disposal. The entire area of
known soil contamination was then backfilled with clean off-site fill to a depth of 5 ft bgs.
Additional confirmation samples collected from backfill placed in the excavation at “Areas E
and F” confirm no PCBs are present above site specific goals.

Based upon the post site grading confirmation sampling, the site is in compliance with BFA.
Therefore, on behalf of Suttle Avenue, LLC we request a letter from DENR confirming your
agreement that the BFA has been complied with and no further activities are necessary.

Ms. Carolyn Minnich
July 18, 2014
Page 5
S:\AAA-Master Projects\Bryant Park (BTP-003) Tract F Update 2013\Post-Construction Sampling\Report\Final Bryant Park Post-Grading Sampling Report.docx

We appreciate your expeditious responses and general assistance on this project. If you have any
questions, please contact me.

Sincerely,

Hart & Hickman, PC

Leonard Moretz, PG
Senior Project Manager

cc: Mr. George Macon, Merrifield Partners (1 copy by email)
Mr. Ron Weiner, Radiator Specialty Company (1 copy by email)
Mr. Pete Lash, Beacon Partners (1 copy by email)

Table 1
Summary of PCB in Soil Analtyical Results
Bryant Park-Tract F Post-Grading Sampling Plan
Charlotte, North Carolina
H&H Job No. BTP-003
PCBs (8082)
PCB-1248 (Aroclor
1248)
A1 (0-2') Comp 0-2' 5/30/2014 mg/kg <0.0420
A1 (3-5') Comp 3-5' 5/30/2014 mg/kg <0.0414
A2 (0-2') Comp 0-2' 5/30/2014 mg/kg <0.0399
A2 (3-5') Comp 3-5' 5/30/2014 mg/kg <0.0422
B (0-2') Comp 0-2' 5/30/2014 mg/kg <0.0401
C (0-2') Comp 0-2' 5/30/2014 mg/kg <0.0412
C (3-5') Comp 3-5' 5/30/2014 mg/kg 0.0425
D (0-2') Comp 0-2' 5/30/2014 mg/kg <0.0393
E (0-2') Comp 0-2' 6/2/2014 mg/kg 4.800
E-BACKFILL (0-2)0-2' 7/8/2014 mg/kg <0.0366
F (0-2') Comp 0-2' 6/2/2014 mg/kg 2.330
F-BACKFILL (0-2)0-2' 7/8/2014 mg/kg <0.0367
G (0-2') Comp 0-2' 6/2/2014 mg/kg 0.0744
H (0-2') Comp 0-2' 6/2/2014 mg/kg <0.0368
I (0-2') Comp 0-2' 6/2/2014 mg/kg <0.0393
J (0-2') Comp 0-2' 6/2/2014 mg/kg <0.0353
K (0-2') Comp 0-2' 6/2/2014 mg/kg 0.0945
L (0-2') Comp 0-2' 5/30/2014 mg/kg <0.0383
L (3-5') Comp 3-5' 5/30/2014 mg/kg <0.0409
M (0-2') Comp 0-2' 5/30/2014 mg/kg <0.373
M (3-5') Comp 3-5' 5/30/2014 mg/kg 0.502
N (0-2') Comp 0-2' 5/30/2014 mg/kg 0.101
O (0-2') Comp 0-2' 5/30/2014 mg/kg <0.0396
O (3-5') Comp 3-5' 5/30/2014 mg/kg <0.0384
P (0-2') Comp 0-2' 5/30/2014 mg/kg 0.331
Screening Criteria mg/kg 1.0
Notes:
SSSL = Site Specific Screening Level as defined by the Brownfields Agreement (BFA)
Only those compounds detected in at least one sample shown above
Bold indicates exceedance of SSSL
Method number follows parameter in parenthesis
Comp = Composite Sample
mg/kg = milligrams per kilogram
SSSL
Sample ID Sample Depth
(feet)Sample Date Units
S:\AAA-Master Projects\Bryant Park (BTP-003) Tract F Update 2013\Post-Construction Sampling\Soil Analytical Results7/17/2014
Table 1
Hart & Hickman, PC
SITE
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAPS
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
TITLE
PROJECT
SITE LOCATION MAP
SUTTLE AVE, LLC
2001 SUTTLE AVE
CHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
07-17-14 0
1BTP-003
2923 S. Tryon Street, Suite 100Charlotte, NC 28203
704.586.0007(p) 704.586.0373(f)
CHARLOTTE WEST, NC 1993
PHOTOREVISED: NO
CHARLOTTE EAST, NC 1967
PHOTOREVISED: 1988

Appendix A Laboratory Analytical Results
#=CL#
June 05, 2014
LIMS USE: FR - JOSELYN HARRIGER
LIMS OBJECT ID: 92203517
92203517
Project:
Pace Project No.:
RE:
Ms. Joselyn Harriger
Hart & Hickman
2923 S. Tryon St
Charlotte, NC 28203
BRYANT PARK
Dear Ms. Harriger:
Enclosed are the analytical results for sample(s) received by the laboratory on May 31, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 28
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92203517
BRYANT PARK
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 28
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92203517
BRYANT PARK
Lab ID Sample ID Matrix Date Collected Date Received
92203517001 A1 (0-2') COMP Solid 05/30/14 11:30 05/31/14 09:40
92203517002 A2 (0-2') COMP Solid 05/30/14 11:40 05/31/14 09:40
92203517003 A1 (3-5') COMP Solid 05/30/14 12:10 05/31/14 09:40
92203517004 A2 (3-5') COMP Solid 05/30/14 13:00 05/31/14 09:40
92203517005 B (0-2') COMP Solid 05/30/14 12:50 05/31/14 09:40
92203517006 C (0-2') COMP Solid 05/30/14 13:25 05/31/14 09:40
92203517007 C (3-5') COMP Solid 05/30/14 13:40 05/31/14 09:40
92203517008 D (0-2') COMP Solid 05/30/14 14:00 05/31/14 09:40
92203517009 L (0-2') COMP Solid 05/30/14 15:20 05/31/14 09:40
92203517010 M (0-2') COMP Solid 05/30/14 15:25 05/31/14 09:40
92203517011 O (0-2') COMP Solid 05/30/14 15:55 05/31/14 09:40
92203517012 N(0-2') COMP Solid 05/30/14 16:10 05/31/14 09:40
92203517013 P(0-2') COMP Solid 05/30/14 16:25 05/31/14 09:40
92203517014 L(3-5') COMP Solid 05/30/14 17:05 05/31/14 09:40
92203517015 O(3-5') COMP Solid 05/30/14 17:15 05/31/14 09:40
92203517016 M(3-5) COMP Solid 05/30/14 17:25 05/31/14 09:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 28
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92203517
BRYANT PARK
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92203517001 A1 (0-2') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CLLW
92203517002 A2 (0-2') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CLLW
92203517003 A1 (3-5') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CLLW
92203517004 A2 (3-5') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CLLW
92203517005 B (0-2') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CLLW
92203517006 C (0-2') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CLLW
92203517007 C (3-5') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CLLW
92203517008 D (0-2') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CLLW
92203517009 L (0-2') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CLLW
92203517010 M (0-2') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CLLW
92203517011 O (0-2') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CLLW
92203517012 N(0-2') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CLLW
92203517013 P(0-2') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CLLW
92203517014 L(3-5') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CLLW
92203517015 O(3-5') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CAES
92203517016 M(3-5) COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CAES
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203517
BRYANT PARK
Sample:A1 (0-2') COMP Lab ID:92203517001 Collected:05/30/14 11:30 Received:05/31/14 09:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 00:00 12674-11-205/31/14 12:5842.0 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 00:00 11104-28-205/31/14 12:5842.0 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 00:00 11141-16-505/31/14 12:5842.0 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 00:00 53469-21-905/31/14 12:5842.0 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/05/14 00:00 12672-29-605/31/14 12:5842.0 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 00:00 11097-69-105/31/14 12:5842.0 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 00:00 11096-82-505/31/14 12:5842.0 1
Surrogates
Decachlorobiphenyl (S)71 %06/05/14 00:00 2051-24-305/31/14 12:5821-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 21.4 %06/05/14 09:290.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203517
BRYANT PARK
Sample:A2 (0-2') COMP Lab ID:92203517002 Collected:05/30/14 11:40 Received:05/31/14 09:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 00:21 12674-11-205/31/14 12:5839.9 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 00:21 11104-28-205/31/14 12:5839.9 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 00:21 11141-16-505/31/14 12:5839.9 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 00:21 53469-21-905/31/14 12:5839.9 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/05/14 00:21 12672-29-605/31/14 12:5839.9 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 00:21 11097-69-105/31/14 12:5839.9 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 00:21 11096-82-505/31/14 12:5839.9 1
Surrogates
Decachlorobiphenyl (S)82 %06/05/14 00:21 2051-24-305/31/14 12:5821-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 17.2 %06/05/14 09:300.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203517
BRYANT PARK
Sample:A1 (3-5') COMP Lab ID:92203517003 Collected:05/30/14 12:10 Received:05/31/14 09:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 00:42 12674-11-205/31/14 12:5841.4 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 00:42 11104-28-205/31/14 12:5841.4 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 00:42 11141-16-505/31/14 12:5841.4 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 00:42 53469-21-905/31/14 12:5841.4 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/05/14 00:42 12672-29-605/31/14 12:5841.4 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 00:42 11097-69-105/31/14 12:5841.4 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 00:42 11096-82-505/31/14 12:5841.4 1
Surrogates
Decachlorobiphenyl (S)82 %06/05/14 00:42 2051-24-305/31/14 12:5821-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 20.3 %06/05/14 09:300.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203517
BRYANT PARK
Sample:A2 (3-5') COMP Lab ID:92203517004 Collected:05/30/14 13:00 Received:05/31/14 09:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 01:43 12674-11-205/31/14 12:5842.2 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 01:43 11104-28-205/31/14 12:5842.2 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 01:43 11141-16-505/31/14 12:5842.2 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 01:43 53469-21-905/31/14 12:5842.2 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/05/14 01:43 12672-29-605/31/14 12:5842.2 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 01:43 11097-69-105/31/14 12:5842.2 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 01:43 11096-82-505/31/14 12:5842.2 1
Surrogates
Decachlorobiphenyl (S)81 %06/05/14 01:43 2051-24-305/31/14 12:5821-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 21.8 %06/05/14 09:300.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203517
BRYANT PARK
Sample:B (0-2') COMP Lab ID:92203517005 Collected:05/30/14 12:50 Received:05/31/14 09:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 02:04 12674-11-205/31/14 12:5840.1 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 02:04 11104-28-205/31/14 12:5840.1 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 02:04 11141-16-505/31/14 12:5840.1 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 02:04 53469-21-905/31/14 12:5840.1 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/05/14 02:04 12672-29-605/31/14 12:5840.1 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 02:04 11097-69-105/31/14 12:5840.1 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 02:04 11096-82-505/31/14 12:5840.1 1
Surrogates
Decachlorobiphenyl (S)88 %06/05/14 02:04 2051-24-305/31/14 12:5821-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 17.7 %06/05/14 09:300.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203517
BRYANT PARK
Sample:C (0-2') COMP Lab ID:92203517006 Collected:05/30/14 13:25 Received:05/31/14 09:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 02:24 12674-11-205/31/14 12:5841.2 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 02:24 11104-28-205/31/14 12:5841.2 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 02:24 11141-16-505/31/14 12:5841.2 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 02:24 53469-21-905/31/14 12:5841.2 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/05/14 02:24 12672-29-605/31/14 12:5841.2 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 02:24 11097-69-105/31/14 12:5841.2 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 02:24 11096-82-505/31/14 12:5841.2 1
Surrogates
Decachlorobiphenyl (S)64 %06/05/14 02:24 2051-24-305/31/14 12:5821-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 19.9 %06/05/14 09:300.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203517
BRYANT PARK
Sample:C (3-5') COMP Lab ID:92203517007 Collected:05/30/14 13:40 Received:05/31/14 09:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 02:45 12674-11-205/31/14 12:5840.8 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 02:45 11104-28-205/31/14 12:5840.8 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 02:45 11141-16-505/31/14 12:5840.8 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 02:45 53469-21-905/31/14 12:5840.8 1
PCB-1248 (Aroclor 1248)42.5 ug/kg 06/05/14 02:45 12672-29-605/31/14 12:5840.8 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 02:45 11097-69-105/31/14 12:5840.8 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 02:45 11096-82-505/31/14 12:5840.8 1
Surrogates
Decachlorobiphenyl (S)87 %06/05/14 02:45 2051-24-305/31/14 12:5821-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 19.1 %06/05/14 09:300.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203517
BRYANT PARK
Sample:D (0-2') COMP Lab ID:92203517008 Collected:05/30/14 14:00 Received:05/31/14 09:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 03:06 12674-11-205/31/14 12:5839.3 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 03:06 11104-28-205/31/14 12:5839.3 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 03:06 11141-16-505/31/14 12:5839.3 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 03:06 53469-21-905/31/14 12:5839.3 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/05/14 03:06 12672-29-605/31/14 12:5839.3 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 03:06 11097-69-105/31/14 12:5839.3 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 03:06 11096-82-505/31/14 12:5839.3 1
Surrogates
Decachlorobiphenyl (S)82 %06/05/14 03:06 2051-24-305/31/14 12:5821-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 16.0 %06/05/14 09:300.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 12 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203517
BRYANT PARK
Sample:L (0-2') COMP Lab ID:92203517009 Collected:05/30/14 15:20 Received:05/31/14 09:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 03:26 12674-11-205/31/14 12:5838.3 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 03:26 11104-28-205/31/14 12:5838.3 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 03:26 11141-16-505/31/14 12:5838.3 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 03:26 53469-21-905/31/14 12:5838.3 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/05/14 03:26 12672-29-605/31/14 12:5838.3 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 03:26 11097-69-105/31/14 12:5838.3 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 03:26 11096-82-505/31/14 12:5838.3 1
Surrogates
Decachlorobiphenyl (S)85 %06/05/14 03:26 2051-24-305/31/14 12:5821-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 13.7 %06/05/14 09:300.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203517
BRYANT PARK
Sample:M (0-2') COMP Lab ID:92203517010 Collected:05/30/14 15:25 Received:05/31/14 09:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 10:37 12674-11-205/31/14 12:5837310
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 10:37 11104-28-205/31/14 12:5837310
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 10:37 11141-16-505/31/14 12:5837310
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 10:37 53469-21-905/31/14 12:5837310
PCB-1248 (Aroclor 1248)ND ug/kg 06/05/14 10:37 12672-29-605/31/14 12:5837310
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 10:37 11097-69-105/31/14 12:5837310
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 10:37 11096-82-505/31/14 12:5837310
Surrogates
Decachlorobiphenyl (S)0 %06/05/14 10:37 2051-24-3 D3,S405/31/14 12:5821-132 10
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 11.6 %06/05/14 09:310.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203517
BRYANT PARK
Sample:O (0-2') COMP Lab ID:92203517011 Collected:05/30/14 15:55 Received:05/31/14 09:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 04:07 12674-11-205/31/14 12:5839.6 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 04:07 11104-28-205/31/14 12:5839.6 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 04:07 11141-16-505/31/14 12:5839.6 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 04:07 53469-21-905/31/14 12:5839.6 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/05/14 04:07 12672-29-605/31/14 12:5839.6 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 04:07 11097-69-105/31/14 12:5839.6 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 04:07 11096-82-505/31/14 12:5839.6 1
Surrogates
Decachlorobiphenyl (S)85 %06/05/14 04:07 2051-24-305/31/14 12:5821-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 16.6 %06/05/14 09:310.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203517
BRYANT PARK
Sample:N(0-2') COMP Lab ID:92203517012 Collected:05/30/14 16:10 Received:05/31/14 09:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 04:28 12674-11-205/31/14 12:5838.9 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 04:28 11104-28-205/31/14 12:5838.9 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 04:28 11141-16-505/31/14 12:5838.9 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 04:28 53469-21-905/31/14 12:5838.9 1
PCB-1248 (Aroclor 1248)101 ug/kg 06/05/14 04:28 12672-29-605/31/14 12:5838.9 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 04:28 11097-69-105/31/14 12:5838.9 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 04:28 11096-82-505/31/14 12:5838.9 1
Surrogates
Decachlorobiphenyl (S)86 %06/05/14 04:28 2051-24-305/31/14 12:5821-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 15.2 %06/05/14 09:310.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203517
BRYANT PARK
Sample:P(0-2') COMP Lab ID:92203517013 Collected:05/30/14 16:25 Received:05/31/14 09:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 04:48 12674-11-205/31/14 12:5838.6 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 04:48 11104-28-205/31/14 12:5838.6 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 04:48 11141-16-505/31/14 12:5838.6 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 04:48 53469-21-905/31/14 12:5838.6 1
PCB-1248 (Aroclor 1248)331 ug/kg 06/05/14 04:48 12672-29-605/31/14 12:5838.6 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 04:48 11097-69-105/31/14 12:5838.6 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 04:48 11096-82-505/31/14 12:5838.6 1
Surrogates
Decachlorobiphenyl (S)83 %06/05/14 04:48 2051-24-305/31/14 12:5821-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 14.5 %06/05/14 09:310.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203517
BRYANT PARK
Sample:L(3-5') COMP Lab ID:92203517014 Collected:05/30/14 17:05 Received:05/31/14 09:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 05:09 12674-11-205/31/14 12:5840.9 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 05:09 11104-28-205/31/14 12:5840.9 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 05:09 11141-16-505/31/14 12:5840.9 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 05:09 53469-21-905/31/14 12:5840.9 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/05/14 05:09 12672-29-605/31/14 12:5840.9 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 05:09 11097-69-105/31/14 12:5840.9 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 05:09 11096-82-505/31/14 12:5840.9 1
Surrogates
Decachlorobiphenyl (S)83 %06/05/14 05:09 2051-24-305/31/14 12:5821-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 19.4 %06/05/14 09:310.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203517
BRYANT PARK
Sample:O(3-5') COMP Lab ID:92203517015 Collected:05/30/14 17:15 Received:05/31/14 09:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 05:29 12674-11-205/31/14 12:5838.4 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 05:29 11104-28-205/31/14 12:5838.4 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 05:29 11141-16-505/31/14 12:5838.4 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 05:29 53469-21-905/31/14 12:5838.4 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/05/14 05:29 12672-29-605/31/14 12:5838.4 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 05:29 11097-69-105/31/14 12:5838.4 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 05:29 11096-82-505/31/14 12:5838.4 1
Surrogates
Decachlorobiphenyl (S)82 %06/05/14 05:29 2051-24-305/31/14 12:5821-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 14.1 %06/04/14 16:440.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 28
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203517
BRYANT PARK
Sample:M(3-5) COMP Lab ID:92203517016 Collected:05/30/14 17:25 Received:05/31/14 09:15 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 05:50 12674-11-205/31/14 12:5839.8 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 05:50 11104-28-205/31/14 12:5839.8 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 05:50 11141-16-505/31/14 12:5839.8 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 05:50 53469-21-905/31/14 12:5839.8 1
PCB-1248 (Aroclor 1248)502 ug/kg 06/05/14 05:50 12672-29-605/31/14 12:5839.8 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 05:50 11097-69-105/31/14 12:5839.8 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 05:50 11096-82-505/31/14 12:5839.8 1
Surrogates
Decachlorobiphenyl (S)76 %06/05/14 05:50 2051-24-305/31/14 12:5821-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 17.1 %06/04/14 16:450.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
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[phone]
Page 20 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203517
BRYANT PARK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/28033
EPA 3546
EPA 8082
8082 GCS PCB
Associated Lab Samples:92203517001, 92203517002, 92203517003, 92203517004, 92203517005, 92203517006, 92203517007,
92203517008, 92203517009, 92203517010, 92203517011, 92203517012, 92203517013, 92203517014,
92203517015, 92203517016
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1211331
Associated Lab Samples:92203517001, 92203517002, 92203517003, 92203517004, 92203517005, 92203517006, 92203517007,
92203517008, 92203517009, 92203517010, 92203517011, 92203517012, 92203517013, 92203517014,
92203517015, 92203517016
Matrix:Solid
Analyzed
PCB-1016 (Aroclor 1016)ug/kg ND 33.0 06/04/14 22:18
PCB-1221 (Aroclor 1221)ug/kg ND 33.0 06/04/14 22:18
PCB-1232 (Aroclor 1232)ug/kg ND 33.0 06/04/14 22:18
PCB-1242 (Aroclor 1242)ug/kg ND 33.0 06/04/14 22:18
PCB-1248 (Aroclor 1248)ug/kg ND 33.0 06/04/14 22:18
PCB-1254 (Aroclor 1254)ug/kg ND 33.0 06/04/14 22:18
PCB-1260 (Aroclor 1260)ug/kg ND 33.0 06/04/14 22:18
Decachlorobiphenyl (S)%83 21-132 06/04/14 22:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1211332LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/kg 118167 71 49-110
PCB-1260 (Aroclor 1260)ug/kg 131167 78 50-110
Decachlorobiphenyl (S)%93 21-132
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1211333MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203517003
1211334
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
PCB-1016 (Aroclor 1016)ug/kg 209 72 49-15076 5 30209ND150159
PCB-1260 (Aroclor 1260)ug/kg 209 76 50-15078 3 30209ND158163
Decachlorobiphenyl (S)%79 21-13282
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
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Page 21 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203517
BRYANT PARK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/6645
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92203517001, 92203517002, 92203517003, 92203517004, 92203517005, 92203517006, 92203517007,
92203517008, 92203517009, 92203517010, 92203517011, 92203517012, 92203517013, 92203517014
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92203517001
1212572SAMPLE DUPLICATE:
Percent Moisture %20.2 6 2521.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92203638006
1212573SAMPLE DUPLICATE:
Percent Moisture %18.9 23 2515.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
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Page 22 of 28
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203517
BRYANT PARK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/6646
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92203517015, 92203517016
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92203107001
1212579SAMPLE DUPLICATE:
Percent Moisture %14.6 2 2514.8
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92203513002
1212580SAMPLE DUPLICATE:
Percent Moisture %17.0 R1272522.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
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Page 23 of 28
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92203517
BRYANT PARK
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
RPD value was outside control limits.R1
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
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Page 24 of 28
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92203517
BRYANT PARK
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92203517001 OEXT/28033 GCSV/17815A1 (0-2') COMP EPA 3546 EPA 8082
92203517002 OEXT/28033 GCSV/17815A2 (0-2') COMP EPA 3546 EPA 8082
92203517003 OEXT/28033 GCSV/17815A1 (3-5') COMP EPA 3546 EPA 8082
92203517004 OEXT/28033 GCSV/17815A2 (3-5') COMP EPA 3546 EPA 8082
92203517005 OEXT/28033 GCSV/17815B (0-2') COMP EPA 3546 EPA 8082
92203517006 OEXT/28033 GCSV/17815C (0-2') COMP EPA 3546 EPA 8082
92203517007 OEXT/28033 GCSV/17815C (3-5') COMP EPA 3546 EPA 8082
92203517008 OEXT/28033 GCSV/17815D (0-2') COMP EPA 3546 EPA 8082
92203517009 OEXT/28033 GCSV/17815L (0-2') COMP EPA 3546 EPA 8082
92203517010 OEXT/28033 GCSV/17815M (0-2') COMP EPA 3546 EPA 8082
92203517011 OEXT/28033 GCSV/17815O (0-2') COMP EPA 3546 EPA 8082
92203517012 OEXT/28033 GCSV/17815N(0-2') COMP EPA 3546 EPA 8082
92203517013 OEXT/28033 GCSV/17815P(0-2') COMP EPA 3546 EPA 8082
92203517014 OEXT/28033 GCSV/17815L(3-5') COMP EPA 3546 EPA 8082
92203517015 OEXT/28033 GCSV/17815O(3-5') COMP EPA 3546 EPA 8082
92203517016 OEXT/28033 GCSV/17815M(3-5) COMP EPA 3546 EPA 8082
92203517001 PMST/6645A1 (0-2') COMP ASTM D2974-87
92203517002 PMST/6645A2 (0-2') COMP ASTM D2974-87
92203517003 PMST/6645A1 (3-5') COMP ASTM D2974-87
92203517004 PMST/6645A2 (3-5') COMP ASTM D2974-87
92203517005 PMST/6645B (0-2') COMP ASTM D2974-87
92203517006 PMST/6645C (0-2') COMP ASTM D2974-87
92203517007 PMST/6645C (3-5') COMP ASTM D2974-87
92203517008 PMST/6645D (0-2') COMP ASTM D2974-87
92203517009 PMST/6645L (0-2') COMP ASTM D2974-87
92203517010 PMST/6645M (0-2') COMP ASTM D2974-87
92203517011 PMST/6645O (0-2') COMP ASTM D2974-87
92203517012 PMST/6645N(0-2') COMP ASTM D2974-87
92203517013 PMST/6645P(0-2') COMP ASTM D2974-87
92203517014 PMST/6645L(3-5') COMP ASTM D2974-87
92203517015 PMST/6646O(3-5') COMP ASTM D2974-87
92203517016 PMST/6646M(3-5) COMP ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/05/2014 02:09 PM
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Page 25 of 28
Page 26 of 28
Page 27 of 28
Page 28 of 28
#=CL#
June 06, 2014
LIMS USE: FR - JOSELYN HARRIGER
LIMS OBJECT ID: 92203638
92203638
Project:
Pace Project No.:
RE:
Ms. Joselyn Harriger
Hart & Hickman
2923 S. Tryon St
Charlotte, NC 28203
BRYANT PARK BTP-003
Dear Ms. Harriger:
Enclosed are the analytical results for sample(s) received by the laboratory on June 02, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 1 of 18
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92203638
BRYANT PARK BTP-003
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 2 of 18
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92203638
BRYANT PARK BTP-003
Lab ID Sample ID Matrix Date Collected Date Received
92203638001 F (0-2') COMP Solid 06/02/14 13:30 06/02/14 16:40
92203638002 E (0-2') COMP Solid 06/02/14 13:45 06/02/14 16:40
92203638003 G (0-2') COMP Solid 06/02/14 14:30 06/02/14 16:40
92203638004 H (0-2') COMP Solid 06/02/14 14:45 06/02/14 16:40
92203638005 I (0-2') COMP Solid 06/02/14 15:15 06/02/14 16:40
92203638006 K (0-2') COMP Solid 06/02/14 15:30 06/02/14 16:40
92203638007 J (0-2') COMP Solid 06/02/14 15:50 06/02/14 16:40
REPORT OF LABORATORY ANALYSIS
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Page 3 of 18
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92203638
BRYANT PARK BTP-003
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92203638001 F (0-2') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CLLW
92203638002 E (0-2') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CLLW
92203638003 G (0-2') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CLLW
92203638004 H (0-2') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CLLW
92203638005 I (0-2') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CLLW
92203638006 K (0-2') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CLLW
92203638007 J (0-2') COMP EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CZAK
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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[phone]
Page 4 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203638
BRYANT PARK BTP-003
Sample:F (0-2') COMP Lab ID:92203638001 Collected:06/02/14 13:30 Received:06/02/14 16:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 10:58 12674-11-206/02/14 18:4239110
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 10:58 11104-28-206/02/14 18:4239110
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 10:58 11141-16-506/02/14 18:4239110
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 10:58 53469-21-906/02/14 18:4239110
PCB-1248 (Aroclor 1248)2330 ug/kg 06/05/14 10:58 12672-29-606/02/14 18:4239110
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 10:58 11097-69-106/02/14 18:4239110
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 10:58 11096-82-506/02/14 18:4239110
Surrogates
Decachlorobiphenyl (S)0 %06/05/14 10:58 2051-24-3 S406/02/14 18:4221-132 10
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 15.6 %06/05/14 09:310.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/06/2014 04:56 PM
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Page 5 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203638
BRYANT PARK BTP-003
Sample:E (0-2') COMP Lab ID:92203638002 Collected:06/02/14 13:45 Received:06/02/14 16:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 11:18 12674-11-206/02/14 18:4299525
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 11:18 11104-28-206/02/14 18:4299525
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 11:18 11141-16-506/02/14 18:4299525
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 11:18 53469-21-906/02/14 18:4299525
PCB-1248 (Aroclor 1248)4800 ug/kg 06/05/14 11:18 12672-29-606/02/14 18:4299525
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 11:18 11097-69-106/02/14 18:4299525
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 11:18 11096-82-506/02/14 18:4299525
Surrogates
Decachlorobiphenyl (S)0 %06/05/14 11:18 2051-24-3 S406/02/14 18:4221-132 25
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 17.1 %06/05/14 09:310.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/06/2014 04:56 PM
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Page 6 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203638
BRYANT PARK BTP-003
Sample:G (0-2') COMP Lab ID:92203638003 Collected:06/02/14 14:30 Received:06/02/14 16:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 08:35 12674-11-206/02/14 18:4236.8 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 08:35 11104-28-206/02/14 18:4236.8 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 08:35 11141-16-506/02/14 18:4236.8 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 08:35 53469-21-906/02/14 18:4236.8 1
PCB-1248 (Aroclor 1248)74.4 ug/kg 06/05/14 08:35 12672-29-606/02/14 18:4236.8 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 08:35 11097-69-106/02/14 18:4236.8 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 08:35 11096-82-506/02/14 18:4236.8 1
Surrogates
Decachlorobiphenyl (S)86 %06/05/14 08:35 2051-24-306/02/14 18:4221-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 10.4 %06/05/14 09:310.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/06/2014 04:56 PM
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Page 7 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203638
BRYANT PARK BTP-003
Sample:H (0-2') COMP Lab ID:92203638004 Collected:06/02/14 14:45 Received:06/02/14 16:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 08:55 12674-11-206/02/14 18:4236.8 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 08:55 11104-28-206/02/14 18:4236.8 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 08:55 11141-16-506/02/14 18:4236.8 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 08:55 53469-21-906/02/14 18:4236.8 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/05/14 08:55 12672-29-606/02/14 18:4236.8 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 08:55 11097-69-106/02/14 18:4236.8 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 08:55 11096-82-506/02/14 18:4236.8 1
Surrogates
Decachlorobiphenyl (S)93 %06/05/14 08:55 2051-24-306/02/14 18:4221-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 10.3 %06/05/14 09:310.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/06/2014 04:56 PM
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Page 8 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203638
BRYANT PARK BTP-003
Sample:I (0-2') COMP Lab ID:92203638005 Collected:06/02/14 15:15 Received:06/02/14 16:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 09:15 12674-11-206/02/14 18:4239.3 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 09:15 11104-28-206/02/14 18:4239.3 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 09:15 11141-16-506/02/14 18:4239.3 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 09:15 53469-21-906/02/14 18:4239.3 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/05/14 09:15 12672-29-606/02/14 18:4239.3 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 09:15 11097-69-106/02/14 18:4239.3 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 09:15 11096-82-506/02/14 18:4239.3 1
Surrogates
Decachlorobiphenyl (S)80 %06/05/14 09:15 2051-24-306/02/14 18:4221-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 16.1 %06/05/14 09:310.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/06/2014 04:56 PM
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[phone]
Page 9 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203638
BRYANT PARK BTP-003
Sample:K (0-2') COMP Lab ID:92203638006 Collected:06/02/14 15:30 Received:06/02/14 16:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 09:36 12674-11-206/02/14 18:4238.8 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 09:36 11104-28-206/02/14 18:4238.8 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 09:36 11141-16-506/02/14 18:4238.8 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 09:36 53469-21-906/02/14 18:4238.8 1
PCB-1248 (Aroclor 1248)94.5 ug/kg 06/05/14 09:36 12672-29-606/02/14 18:4238.8 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 09:36 11097-69-106/02/14 18:4238.8 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 09:36 11096-82-506/02/14 18:4238.8 1
Surrogates
Decachlorobiphenyl (S)82 %06/05/14 09:36 2051-24-306/02/14 18:4221-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 15.0 %06/05/14 09:320.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/06/2014 04:56 PM
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[phone]
Page 10 of 18
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92203638
BRYANT PARK BTP-003
Sample:J (0-2') COMP Lab ID:92203638007 Collected:06/02/14 15:50 Received:06/02/14 16:40 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 06/05/14 09:56 12674-11-206/02/14 18:4235.3 1
PCB-1221 (Aroclor 1221)ND ug/kg 06/05/14 09:56 11104-28-206/02/14 18:4235.3 1
PCB-1232 (Aroclor 1232)ND ug/kg 06/05/14 09:56 11141-16-506/02/14 18:4235.3 1
PCB-1242 (Aroclor 1242)ND ug/kg 06/05/14 09:56 53469-21-906/02/14 18:4235.3 1
PCB-1248 (Aroclor 1248)ND ug/kg 06/05/14 09:56 12672-29-606/02/14 18:4235.3 1
PCB-1254 (Aroclor 1254)ND ug/kg 06/05/14 09:56 11097-69-106/02/14 18:4235.3 1
PCB-1260 (Aroclor 1260)ND ug/kg 06/05/14 09:56 11096-82-506/02/14 18:4235.3 1
Surrogates
Decachlorobiphenyl (S)84 %06/05/14 09:56 2051-24-306/02/14 18:4221-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 6.6 %06/06/14 16:380.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/06/2014 04:56 PM
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Page 11 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203638
BRYANT PARK BTP-003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/28054
EPA 3546
EPA 8082
8082 GCS PCB
Associated Lab Samples:92203638001, 92203638002, 92203638003, 92203638004, 92203638005, 92203638006, 92203638007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1212234
Associated Lab Samples:92203638001, 92203638002, 92203638003, 92203638004, 92203638005, 92203638006, 92203638007
Matrix:Solid
Analyzed
PCB-1016 (Aroclor 1016)ug/kg ND 33.0 06/04/14 05:36
PCB-1221 (Aroclor 1221)ug/kg ND 33.0 06/04/14 05:36
PCB-1232 (Aroclor 1232)ug/kg ND 33.0 06/04/14 05:36
PCB-1242 (Aroclor 1242)ug/kg ND 33.0 06/04/14 05:36
PCB-1248 (Aroclor 1248)ug/kg ND 33.0 06/04/14 05:36
PCB-1254 (Aroclor 1254)ug/kg ND 33.0 06/04/14 05:36
PCB-1260 (Aroclor 1260)ug/kg ND 33.0 06/04/14 05:36
Decachlorobiphenyl (S)%81 21-132 06/04/14 05:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1212235LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/kg 105167 63 49-110
PCB-1260 (Aroclor 1260)ug/kg 115167 69 50-110
Decachlorobiphenyl (S)%83 21-132
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1212236MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92203638001
1212237
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
PCB-1016 (Aroclor 1016)ug/kg M3198116149-1501051 10 30198ND22902080
PCB-1260 (Aroclor 1260)ug/kg 198 135 50-150146 8 30198ND266288
Decachlorobiphenyl (S)%102 21-132104
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/06/2014 04:56 PM
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[phone]
Page 12 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203638
BRYANT PARK BTP-003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/6644
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92203638007
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92203303001
1212555SAMPLE DUPLICATE:
Percent Moisture %21.9 23 2517.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92203525001
1212556SAMPLE DUPLICATE:
Percent Moisture %9.5 5 259.9
REPORT OF LABORATORY ANALYSIS
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Page 13 of 18
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92203638
BRYANT PARK BTP-003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/6645
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92203638001, 92203638002, 92203638003, 92203638004, 92203638005, 92203638006
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92203517001
1212572SAMPLE DUPLICATE:
Percent Moisture %20.2 6 2521.4
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92203638006
1212573SAMPLE DUPLICATE:
Percent Moisture %18.9 23 2515.0
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/06/2014 04:56 PM
Pace Analytical Services, Inc.
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Page 14 of 18
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92203638
BRYANT PARK BTP-003
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery was outside laboratory control limits due to matrix interferences.M3
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
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Page 15 of 18
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92203638
BRYANT PARK BTP-003
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92203638001 OEXT/28054 GCSV/17807F (0-2') COMP EPA 3546 EPA 8082
92203638002 OEXT/28054 GCSV/17807E (0-2') COMP EPA 3546 EPA 8082
92203638003 OEXT/28054 GCSV/17807G (0-2') COMP EPA 3546 EPA 8082
92203638004 OEXT/28054 GCSV/17807H (0-2') COMP EPA 3546 EPA 8082
92203638005 OEXT/28054 GCSV/17807I (0-2') COMP EPA 3546 EPA 8082
92203638006 OEXT/28054 GCSV/17807K (0-2') COMP EPA 3546 EPA 8082
92203638007 OEXT/28054 GCSV/17807J (0-2') COMP EPA 3546 EPA 8082
92203638001 PMST/6645F (0-2') COMP ASTM D2974-87
92203638002 PMST/6645E (0-2') COMP ASTM D2974-87
92203638003 PMST/6645G (0-2') COMP ASTM D2974-87
92203638004 PMST/6645H (0-2') COMP ASTM D2974-87
92203638005 PMST/6645I (0-2') COMP ASTM D2974-87
92203638006 PMST/6645K (0-2') COMP ASTM D2974-87
92203638007 PMST/6644J (0-2') COMP ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/06/2014 04:56 PM
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Page 16 of 18
Page 17 of 18
Page 18 of 18
#=CL#
July 11, 2014
LIMS USE: FR - CHAD GRUBBS
LIMS OBJECT ID: 92208192
92208192
Project:
Pace Project No.:
RE:
Mr. Chad Grubbs
Hart & Hickman
2923 South Tryon Street
Suite 100
Charlotte, NC 28203
BRYANT PARK BTP.003
Dear Mr. Grubbs:
Enclosed are the analytical results for sample(s) received by the laboratory on July 08, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 1 of 12
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92208192
BRYANT PARK BTP.003
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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Page 2 of 12
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92208192
BRYANT PARK BTP.003
Lab ID Sample ID Matrix Date Collected Date Received
92208192001 F-BACKFILL ( 0-2)Solid 07/08/14 10:45 07/08/14 12:17
92208192002 E-BACKFILL ( 0-2)Solid 07/08/14 11:05 07/08/14 12:17
REPORT OF LABORATORY ANALYSIS
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Page 3 of 12
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92208192
BRYANT PARK BTP.003
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92208192001 F-BACKFILL ( 0-2)EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CAES
92208192002 E-BACKFILL ( 0-2)EPA 8082 8 PASI-CRES
ASTM D2974-87 1 PASI-CAES
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 4 of 12
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92208192
BRYANT PARK BTP.003
Sample:F-BACKFILL ( 0-2)Lab ID:92208192001 Collected:07/08/14 10:45 Received:07/08/14 12:17 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 07/11/14 01:49 12674-11-207/09/14 10:0736.7 1
PCB-1221 (Aroclor 1221)ND ug/kg 07/11/14 01:49 11104-28-207/09/14 10:0736.7 1
PCB-1232 (Aroclor 1232)ND ug/kg 07/11/14 01:49 11141-16-507/09/14 10:0736.7 1
PCB-1242 (Aroclor 1242)ND ug/kg 07/11/14 01:49 53469-21-907/09/14 10:0736.7 1
PCB-1248 (Aroclor 1248)ND ug/kg 07/11/14 01:49 12672-29-607/09/14 10:0736.7 1
PCB-1254 (Aroclor 1254)ND ug/kg 07/11/14 01:49 11097-69-107/09/14 10:0736.7 1
PCB-1260 (Aroclor 1260)ND ug/kg 07/11/14 01:49 11096-82-507/09/14 10:0736.7 1
Surrogates
Decachlorobiphenyl (S)81 %07/11/14 01:49 2051-24-307/09/14 10:0721-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 10 %07/09/14 14:400.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/11/2014 03:22 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 5 of 12
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92208192
BRYANT PARK BTP.003
Sample:E-BACKFILL ( 0-2)Lab ID:92208192002 Collected:07/08/14 11:05 Received:07/08/14 12:17 Matrix:Solid
Results reported on a "dry-weight" basis
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPA 3546
PCB-1016 (Aroclor 1016)ND ug/kg 07/11/14 02:51 12674-11-207/09/14 10:0736.6 1
PCB-1221 (Aroclor 1221)ND ug/kg 07/11/14 02:51 11104-28-207/09/14 10:0736.6 1
PCB-1232 (Aroclor 1232)ND ug/kg 07/11/14 02:51 11141-16-507/09/14 10:0736.6 1
PCB-1242 (Aroclor 1242)ND ug/kg 07/11/14 02:51 53469-21-907/09/14 10:0736.6 1
PCB-1248 (Aroclor 1248)ND ug/kg 07/11/14 02:51 12672-29-607/09/14 10:0736.6 1
PCB-1254 (Aroclor 1254)ND ug/kg 07/11/14 02:51 11097-69-107/09/14 10:0736.6 1
PCB-1260 (Aroclor 1260)ND ug/kg 07/11/14 02:51 11096-82-507/09/14 10:0736.6 1
Surrogates
Decachlorobiphenyl (S)82 %07/11/14 02:51 2051-24-307/09/14 10:0721-132 1
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 9.7 %07/09/14 14:400.10 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/11/2014 03:22 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 12
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92208192
BRYANT PARK BTP.003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/28729
EPA 3546
EPA 8082
8082 GCS PCB
Associated Lab Samples:92208192001, 92208192002
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1237797
Associated Lab Samples:92208192001, 92208192002
Matrix:Solid
Analyzed
PCB-1016 (Aroclor 1016)ug/kg ND 33.0 07/10/14 11:52
PCB-1221 (Aroclor 1221)ug/kg ND 33.0 07/10/14 11:52
PCB-1232 (Aroclor 1232)ug/kg ND 33.0 07/10/14 11:52
PCB-1242 (Aroclor 1242)ug/kg ND 33.0 07/10/14 11:52
PCB-1248 (Aroclor 1248)ug/kg ND 33.0 07/10/14 11:52
PCB-1254 (Aroclor 1254)ug/kg ND 33.0 07/10/14 11:52
PCB-1260 (Aroclor 1260)ug/kg ND 33.0 07/10/14 11:52
Decachlorobiphenyl (S)%109 21-132 07/10/14 11:52
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1237798LABORATORY CONTROL SAMPLE:
LCSSpike
PCB-1016 (Aroclor 1016)ug/kg 123167 74 31-120
PCB-1260 (Aroclor 1260)ug/kg 150167 90 32-120
Decachlorobiphenyl (S)%112 21-132
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1237799MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92208192001
1237800
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
PCB-1016 (Aroclor 1016)ug/kg 186 67 49-15059 14 30186ND125108
PCB-1260 (Aroclor 1260)ug/kg 186 66 50-15063 5 30186ND122116
Decachlorobiphenyl (S)%76 21-13279
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/11/2014 03:22 PM
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[phone]
Page 7 of 12
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92208192
BRYANT PARK BTP.003
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
PMST/6784
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92208192001, 92208192002
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92207824001
1237662SAMPLE DUPLICATE:
Percent Moisture %23.1 4 2522.2
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92208326012
1237663SAMPLE DUPLICATE:
Percent Moisture %17.1 9 2518.6
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/11/2014 03:22 PM
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Huntersville, NC 28078
[phone]
Page 8 of 12
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92208192
BRYANT PARK BTP.003
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
LOD - Limit of Detection.
LOQ - Limit of Quantitation.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 07/11/2014 03:22 PM
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[phone]
Page 9 of 12
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92208192
BRYANT PARK BTP.003
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92208192001 OEXT/28729 GCSV/18173F-BACKFILL ( 0-2)EPA 3546 EPA 8082
92208192002 OEXT/28729 GCSV/18173E-BACKFILL ( 0-2)EPA 3546 EPA 8082
92208192001 PMST/6784F-BACKFILL ( 0-2)ASTM D2974-87
92208192002 PMST/6784E-BACKFILL ( 0-2)ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 10 of 12
Page 11 of 12
Page 12 of 12

Appendix B Corrective Action Correspondence
1
Joselyn Harriger
From:Chad Grubbs
Sent:Monday, June 30, 2014 5:32 PM
To:George Macon; Ron Weiner
Cc:Pete Lash; Matt Lucarelli; Walt Fisher; Curtis Trenkelbach; Chris Urquhart; Leo Moretz
Subject:Fwd: Bryant Park Site - Post Grading Sampling
Formal approval from DENR to excavate the area as we discussed.

Best Regards,
Chad

-------- Original Message --------
Subject: RE: Bryant Park Site - Post Grading Sampling
From: "Minnich, Carolyn" <[e-mail]>
To: Chad Grubbs <[e-mail]>
CC:
Chad: 

Thank you for talking with me.  I have reviewed the scope of work and attachments.  The work plan is acceptable.  If you 
have additional comments or questions, please contact me.   

Carolyn Minnich ------------------------------------------------------ 
Brownfields Project Manager NCDENR-DWM 
704/661-0330 www.ncbrownfields.org 
Come Clean Up With Us! ------------------------------------------------------ 
Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed
to third parties unless the content is exempt by statute or other regulation. 

From: Chad Grubbs [mailto:[e-mail]]
Sent: Monday, June 30, 2014 12:32 PM
To: Minnich, Carolyn
Subject: Bryant Park Site - Post Grading Sampling 

Hey Carolyn, 

I hope you are well.  I wanted to document our conversation last week about the post‐grading sampling and how we 
decided we could quickly address an area that was found to have PCBs above the action level of 1 mg/k.  I attached a 
table summarizing the recent data from the post‐grading confirmatory sampling and a figure from the approved Post‐
Grading Sampling Plan for ease of reference.  As we discussed, the sample results were below 1 mg/kg in all areas except 
for the areas defined as E & F (shown as one contiguous area).  You will note on the attached figure and table that PCBs 
were detected at 2.3 mg/kg and 4.8 mg/kg  at 0‐2 ft in this area.  To address these exceedances as quickly as possible, 
we discussed it was acceptable to excavate the designated “Area of Known Soil Contamination” (which is depicted as 
2
Areas E  & F and outlined in blue) to approximately 5 ft below ground surface and then backfill the entire area with clean 
imported fill.  We discussed  the excavation area will be approximately 75 feet long, 10 feet wide, and 5 ft deep (based 
on Figure 2 ).  We discussed collecting two additional composite samples for PCB analysis from the backfill after it has 
been placed (0‐2 ft depth interval to be consistent with previous sampling) to document no PCBs are above the action 
levels.  We discussed that no additional sampling will be required since the area of known soil contamination will be 
removed for offsite disposal.  We plan to send the soil to the Republic landfill in Concord, NC.  We did discuss with our 
client that they could do additional sampling to possibly reduce the area to be excavated but they prefer to move quickly 
to meet the schedule to occupy the building next month. 

We plan to start this excavation in the next few days so if you would please respond to this email that this plan is 
acceptable I would appreciate it.  H&H will prepare a final summary report with the results of the post‐grading sampling 
and will include a summary of this additional excavation as well. 

The entire team appreciated your input and assistance with this. 

Best Regards, 
Chad 

Chad Grubbs, PG, Project Manager 
Hart & Hickman, PC | 2923 South Tryon Street, Suite 100 | Charlotte, NC 28203 Direct 704-887-4604 | Mobile [phone] | Main 704-586-0007
www.harthickman.com 

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Appendix C Disposal Manifests and Weight Tickets