RA-2227_14098_CA_LSA_20171114

November 14, 2017 Mr. Mark Petermann
NCDEQ, Division of Waste Management, UST Section 1646 Mail Service Center Raleigh, North Carolina 27699-1646
Reference: Limited Site Assessment – Boulevard BP NW Corner of Clayton Avenue and North Madison Boulevard
Roxboro, Person County, North Carolina NCDEQ Incident No: 14098
UST No: RA-2227
NCDEQ Contract No: N17006 ECS Project No: 49:5108

Dear Mr. Petermann:
As authorized by your acceptance on August 24, 2017 of ECS Southeast, LLP (ECS) Task
Authorization Request Number (TAR No. 1) dated August 18, 2017, ECS has completed the Limited Site Assessment (LSA) Report for the above referenced site. Included in this report is a
description of the field activities, the results obtained, and our conclusions and recommendations. ECS appreciates the opportunity to provide our environmental consulting services to you on this
project. If you have any questions concerning this report or this project, please contact us. Sincerely,
ECS SOUTHEAST, LLP

Sarah Kordon John M. Stewart, P.G.
Environmental Scientist Principal Geologist [e-mail] [e-mail]
[phone] [phone]

Limited Site Assessment – Boulevard BP NW Corner of Clayton Avenue and North Madison Boulevard Roxboro, Person County, North Carolina NCDEQ Incident No: 14098
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SITE INFORMATION

Date of Report: November 14, 2017
Facility I.D.: 0-000352 UST Incident No.: 14098
UST No: RA-2227
Site Rank: 20/E Land Use Category: Commercial

Site Name and Location: Boulevard BP Property
NW Corner of Clayton Ave. and North Madison Blvd.
Roxboro, Person County, North Carolina
Latitude and Longitude: 36. 403282° North, -78. 979524° West
Contacts

Property Owner: H W O Newell PO BOX 1098 Roxboro, North Carolina 27573
Consultant: ECS Southeast, LLP 9001 Glenwood Avenue
Raleigh, North Carolina 27617 [phone]
Attn: Matthew Gillis
Laboratory: Pace Analytical Services, Inc. (Pace)
9800 Kincey Avenue, Suite 100
Huntersville, North Carolina 28078 [phone]
Laboratory I.D. # 37706

Limited Site Assessment – Boulevard BP NW Corner of Clayton Avenue and North Madison Boulevard Roxboro, Person County, North Carolina NCDEQ Incident No: 14098
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EXECUTIVE SUMMARY The subject site is known as the Boulevard BP and is located on the northwest corner of
Clayton Avenue and North Madison Boulevard in Roxboro, in Person County, North Carolina.
According to the Person County Geographic Information System (GIS) the parcel is identified as Parcel Identification Number (PIN) 0906-11-55-9764 and is developed with a 1,350 square foot
former service station currently occupied with a used tire store, office and automotive garage by the name of ‘Thrifty Tire’.

On September 18 and 19, 2017, Quantex, LLC. (Quantex) installed and ECS subsequently developed and sampled monitoring wells MW-1 through MW-4. ECS also collected three soil
samples from the soil borings located within the former gasoline UST location and within the
former dispenser. Borings were also drilled along the perimeter of the former gasoline UST location and near the former fuel dispensers. The samples were analyzed to determine the
extent of contaminated soils on the subject site. ECS conducted a receptor survey and surveyed the top of casing of the four monitoring wells.
The groundwater samples were submitted to Pace for chemical analysis for volatile organic compounds (VOCs) using Standard Method 6200B, semi-volatile organic compounds (SVOCs)
using EPA Method 625 BNA with 10 largest non-target peaks, and volatile petroleum
hydrocarbons (VPH) and extractable petroleum hydrocarbons (EPH) using the Massachusetts Department of Environmental Protection (MADEP) Methods. The soil samples were submitted
to Pace for chemical analysis for VOCs using EPA Method 8260, SVOCs using EPA Method
8270, and VPH and EPH using the MADEP Methods.
Based on the analytical results from the groundwater and soil samples, site observations, and
historical information available, ECS concludes the following:
• ECS identified four soil vapor extraction wells (SVE-1 through SVE-3) associated with the subject site;
• ECS did not identify water supply wells within 1,000 feet of the site;
• Municipal water supply is connected to the subject site and available to the surrounding
areas within 1,000 feet of the site;
• The groundwater flow direction is generally to the southwest across the site;
• Groundwater does not appear to be impacted to the north and appears nominally impacted to the east and far west (in the direction of groundwater flow) as laboratory
analysis of the groundwater collected from monitoring wells MW-2 and MW-4 reported
analytes at a concentration above their respective North Carolina 2L Groundwater Quality Standard (NC2LGWQS) and laboratory analysis of groundwater collected from
monitoring well MW-1 did not report any analytes above their respective laboratory
reporting limits;
• An unnamed, intermittent tributary of the Tanyard Branch is located off-site
approximately 110 feet south-southwest of the site and is not likely impacted as a possible receptor; and,
Limited Site Assessment – Boulevard BP NW Corner of Clayton Avenue and North Madison Boulevard Roxboro, Person County, North Carolina NCDEQ Incident No: 14098
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• The contaminant plume is delineated vertically and appears to be oriented to the southwest from the former gasoline UST basin, similar to the plume depicted in the 1995
SSE, therefore, ECS believes the plume has stabilized and is biodegrading.
Based on the conclusions of this Limited Site Assessment, ECS recommends:
• ECS recommends a Notice of Residual Petroleum (NRP) for perpetual land use
restrictions for soil and groundwater should be submitted for the site;
• ECS recommends that once the NRP has been recorded in the Person County Register
of Deeds, the NCDEQ should consider issuing a letter of No Further Action (NFA) and consider the site for closure;
• Should NCDEQ decide to close the site, ECS recommends abandoning the four onsite monitoring wells and three soil vapor extraction wells using a certified well contractor; and,
• ECS recommends that a copy of this report be submitted to the current property owner.

Limited Site Assessment – Boulevard BP NW Corner of Clayton Avenue and North Madison Boulevard Roxboro, Person County, North Carolina NCDEQ Incident No: 14098
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TABLE OF CONTENTS 1.0 SITE HISTORY ............................................................................................................... 7
2.0 SITE GEOLOGY AND HYDROGEOLOGY ..................................................................... 8
3.0 RECEPTOR INFORMATION .......................................................................................... 8
4.0 FIELD ACTIVITIES ........................................................................................................11
4.1 Monitoring Well Installation ..........................................................................................11
4.2 Soil Borings and Soil Sampling ....................................................................................12
4.3 Monitoring Well Sampling .............................................................................................12
4.4 Water Level Measurement.............................................................................................13
5.0 LABORATORY ANALYTICAL RESULTS ..........................................................................13
5.1 Soil Samples ..................................................................................................................13
5.2 Monitoring Well Samples ..............................................................................................13
6.0 CONCLUSIONS .............................................................................................................14
7.0 RECOMMENDATIONS ..................................................................................................15
FIGURES
Figure 1 Site Location Map
Figure 2 Historic Soil Boring Location Map Figure 3 Site Aerial Map
Figure 4 Adjacent Properties Map
Figure 5 Monitoring Well Location Map Figure 6 Groundwater Elevation Map
Figure 7 Soil Boring Location Map
Figure 8 Groundwater Concentration Map Figure 9 Estimated Area of Soils Exceeding Residential MSCCs
TABLES
Table 1 UST Information
Table 2 Summary of Historical Soil Analytical Results
Table 3 Adjacent Properties Table 4 Monitoring Well Construction and Groundwater Elevation Details
Table 5 Summary of Current Soil Analytical Results Table 6 Summary of Current Groundwater Analytical Results APPENDICES Appendix A Water Supply Well Questionnaires
Appendix B ECS Personnel Field Notes, Boring Log, and Sampling Sheets
Appendix C Monitoring Well Construction Forms Appendix D Site Photographs
Appendix E Laboratory Analytical Data Sheets and Chain of Custody (COC) Records
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1.0 SITE HISTORY The subject site is known as the Boulevard BP and is located on the northwest corner of
Clayton Avenue and North Madison Boulevard in Roxboro, in Person County, North Carolina
(Figure 1). According to the Person County GIS, the parcel is identified as PIN 0906-11-55-9764 and is developed with a 1,350 square foot former service station. According to information
provided to ECS by the North Carolina Department of Environment Quality (NCDEQ), the site historically operated as a gasoline service station owned by Little Huff, Inc. with three 2,000-gallon gasoline underground storage tanks (USTs) and one 550-gallon kerosene UST. The
USTs were reportedly removed from the site on September 8, 1994 (Table 1). In October of 1994, ENSCI Environmental, Inc. (ENSCI) conducted a UST Closure Assessment
at the site. ENSCI noted that the areas surrounding the site are served by municipal water supply. On September 8, 1994, ENSCI provided the NCDEQ with a report regarding the removal of the four USTs associated with the site. Notable odor or visible soil contamination
was reported in the vicinity of the three 2,000 gallon gasoline USTs removed from the basin southwest of the structure. The report noted that all USTs were removed from the site prior to
ENSCI personnel arriving. Free-product was not encountered. Soils excavated for the removal
of the USTs totaled approximately 32 cubic yards and composite soil samples collected did not reveal vapor concentrations of more than 40 parts per million (ppm) via Organic Vapor Analyzer
(OVA), Little Huff, Inc. choose to return the soils to the excavation. Based on the laboratory
results collected during removal activities from the former gasoline UST basin, the vertical impact of the soils appeared to be less than 18 feet in depth.
In April of 1995, ENSCI prepared a Site Assessment Report summarizing their soil assessment efforts and Site Sensitivity Evaluation (SSE). On December 5, 1994, ENSCI personnel
advanced nine soil borings to depths of 15 to 20 feet below ground surface (ft. bgs) with a Geoprobe sample equipped with hydraulic push. The locations of borings are shown on Figure 2. Samples were screened with OVA before being analyzed for the total petroleum
hydrocarbons (TPH) via EPA method 5030 and/or 3550. The nine soil samples were impacted in the area of the former dispensers extending to a depth of at least 9 ft. bgs. Considering the
extent of soils impacted above the 10 ppm minimum action limit for soils impacted by low boiling
point petroleum hydrocarbons (gasoline), level of water in a stream, Tanyard Branch, located approximately 110 feet north-northwest off of the site, lack of groundwater encounters, and
vertical extent of impacted soils, ENSCI generated a final cleanup level of 120 ppm for the site.
An estimated total of 114 cubic yards (including the 32 cubic yards returned during excavation) appear to have been impacted at the site above the action level of 120 ppm as calculated
through their SSE.
In August of 1995, ENSCI prepared a Soil Vapor Extraction (SVE) Pilot Test Report for Little
Huff, Inc., which found that the site was not suitable for SVE due to the observed lack of vapor flow during the pilot test and low vacuum pressures induced in the soil matrix. Groundwater was not reportedly encountered in any of the soil borings which were installed to a maximum depth
of 20 ft. bgs and groundwater was not encountered during the time of vapor sampling. For the purposes of this pilot test, three permanent monitoring wells were constructed with a truck mounted drill rig which advanced a 6 inch diameter auger to a depth of 14 or 15 ft. bgs. Soil
vapor extraction well SVE-1 and SVE-2 were used as piezometers and SVE-3 was used as an extraction well. Historical soil analytical results are included in Table 2.
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In October of 1995, ENSCI prepared a Corrective Action Plan (CAP) for Little Huff, Inc. ENSCI
reported that municipal water is supplied to the facility and the region by public water distribution systems from the City of Roxboro. Site reconnaissance within 1,500 foot radius of the site
revealed no private water supply wells. It was recommended that the 76 cubic yards of impacted
soils located near the former product dispensers be excavated horizontally 21.5 feet by 10.5 feet and vertically to 9 feet to mitigate the areas’ impact.
2.0 SITE GEOLOGY AND HYDROGEOLOGY

As determined from the USGS Topographic Maps, Roxboro, North Carolina Quadrangles dated 2013 (Figure 1), the site is at an approximate elevation of 645 feet above mean sea level. Historically, surface runoff on the site appeared to be generally to the south-southwest towards
Tanyard Branch, which is shown on Figure 3. The subject site is situated in the Piedmont Physiographic Province. The soils encountered in
this area are the residual product of in-place chemical weathering of rock presently underlying the site and/or historic depositional events. In general, shallow unconfined groundwater
movement within the overlying soils is controlled largely by topographic gradients. However, as
the groundwater percolates downward, it becomes controlled by the subsurface geologic conditions. Thus, the direction of groundwater movement in the deeper aquifers may not be
consistent with the reflecting topography.
In general, shallow unconfined groundwater movement within the overlying soils is controlled
largely by topographic gradients. Recharge occurs primarily by infiltration along higher elevations and typically discharges into streams or other surface water bodies. The elevation of the shallow water table is transient and can vary with seasonal fluctuations in precipitation.
Movement of shallow groundwater is generally from higher to lower elevations.
3.0 RECEPTOR INFORMATION
Risk Characterization
The answers in the following questionnaire will help with the assignment of the risk classification for the site.
Part I - Groundwater/Surface Water/Vapor Impacts
High Risk
1. Has the discharge or release contaminated any water supply well including any used for
non-drinking purposes? NO
2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the discharge or release? NO
3. Is a water supply well used for any purpose (e.g., irrigation, washing cars, industrial
cooling, filling swimming pools) located within 250 feet of the source area of the release or discharge? NO
4. Does the groundwater within 500 feet of the source area of the discharge or release
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have the potential for future use in that there is no other source of water supply other than the
groundwater? NO
According to the City of Roxboro Public Services, municipal water is connected to
the subject site and is available to properties within 1,000 feet of the site.
5. Do vapors from the discharge or release pose a threat of explosion because of accumulation of the vapors in a confined space or pose any other serious threat to
public health, public safety, or the environment? NO
6. Are there any other factors that would cause the discharge or release to pose an imminent danger to public health, public safety, or the environment? NO
Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the discharge or release? YES
An unnamed, intermittent tributary of the Tanyard Branch is located off-site approximately 110 feet south-southwest of the site.
8. Is the source area of the discharge or release located within a designated wellhead
protection area as defined in 42 USC 300h-7(e)? NO
The NCDEQ wellhead protection mapping tool indicated the subject site is not
located within a wellhead protection area. The link to the NCDEQ website is http://www.ncwater.org/?page=63.
9. Is the discharge or release located in the Coastal Plain Physiographic region as
designated on a map entitled “Geology of North Carolina” published by the Department in 1985?
NO
If YES, is the source area of the release located in an area in which there is recharge to an
unconfined or semi-confined deeper aquifer that is being used or may be used as a source of drinking water? NO
If YES, describe.
10. Do the levels of groundwater contamination for any contaminant exceed the gross contamination levels established by the Department of Environmental Quality? NO
Part II - Land Use
Property Containing Source Area of Discharge or Release
1. Does the property contain one or more primary or secondary residences (permanent or temporary)? NO
2. Does the property contain a school, daycare center, hospital, playground, park, recreation area, church, nursing home, or other place of public assembly? NO
Limited Site Assessment – Boulevard BP NW Corner of Clayton Avenue and North Madison Boulevard Roxboro, Person County, North Carolina NCDEQ Incident No: 14098
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3. Does the property contain a commercial (e.g., retail, warehouse, office/business space,
etc.) or industrial (e.g., manufacturing, utilities, industrial research and development, chemical/petroleum bulk storage, etc.) enterprise, an inactive commercial or industrial
enterprise, or is the land undeveloped? YES
The site currently operates as a used tire store, office and automotive garage.
4. Do children visit the property? YES
The site contains an automotive garage; it is unlikely that children visit.
5. Is access to the property reliably restricted consistent with its use (e.g., by fences, security personnel, or both)? NO
6. Does pavement, buildings, or other structures cap the contaminated soil? YES
Concrete and asphalt pavement cap the contaminated soil.
7. What is the zoning status of the property?
According to City of Roxboro Planning and Zoning Department the property is zoned ‘Highway Business’.
8. Is the use of the property likely to change in the next 20 years? NO
Part III - Property Surrounding Source Area of Discharge or Release
9. What is the distance from the source area of the release to the nearest primary or
secondary residence (permanent or temporary)?
A primary residence is located approximately 230 feet north-northwest of the source area.
10. What is the distance from the source area of the release to the nearest school, daycare
center, hospital, playground, park, recreation area, church, nursing home or other place of public assembly?
The First Pentecostal Church is located approximately 450 feet east of the subject site.
11. What is the zoning status of properties in the surrounding area?
According to City of Roxboro Planning and Zoning Department, properties located in
the vicinity of the site are designated as ‘Highway Business’.
12. Briefly characterize the use and activities of the land in the surrounding area.
The surrounding area is utilized for commercial purposes.
Water Supply Wells
On September 18 and 19, 2017, ECS performed a walking and vehicular reconnaissance of
properties within 1,000 feet of the site. ECS did not observe water supply wells within 1,000 feet
Limited Site Assessment – Boulevard BP NW Corner of Clayton Avenue and North Madison Boulevard Roxboro, Person County, North Carolina NCDEQ Incident No: 14098
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of the site (Figure 3). ECS contacted the City of Roxboro Public Services and according to
municipal records, municipal water supply wells are not located within 1,000 feet of the subject site. Additionally, water supply well surveys were mailed via United States Postal Service
(USPS) to the property owners located within 500 feet of the source area. ECS received
returned letters from Mr. Ray Patel of Timberland Motel at 720 N. Madison Blvd., Mr. Dale Norris of the ABC Store at 712 N. Madison Blvd., Mr. Ray Wilkins of Taylor Printing & Office
Supplies at 115 Clayton Avenue, Ms. Amy Roach of a residence at 214 Clayton Avenue, Ms. Lori Davis of a residence at 218 Clayton Avenue, and Ms. Renee Barker of a residence at 217 Clayton Avenue, which all indicated that the properties addressed do not contain water supply
wells and currently receive municipal water. ECS also received a returned letter from Mr. Ruffin Woody Jr. of the adjoining, northern vacant commercial parcel (legally addressed as N. Madison Blvd.), and he indicated 'unknown' regarding the presence of a supply well but noted that the
property was supplied with public water. ECS did not observe a supply well on his parcel on September 18, 2017. ECS did not receive a response letter from the Masouds, who own the restaurant at 625 N. Madison Blvd., but spoke with Mr. Masoud on September 18, 2017 and he
confirmed that no supply wells are present on this parcel. According to the property tax cards on Person County GIS, the surrounding areas are served by public utilities. Additionally, ECS
contacted the City of Roxboro Public Services and all additional properties are connected to
municipal water. Copies of completed questionnaires are included in Appendix A.
The names and addresses of the adjacent property owners are included in Table 3 and shown on
Figure 4.
Public Water Supplies
ECS contacted the City of Roxboro Public Services to inquire if municipal water is available for the subject site and surrounding area. According to the City of Roxboro Public Services
municipal water is connected to the subject site and properties within 1,000 feet of the site.
Surface Water
As determined from the USGS Topographic Map, Roxboro, North Carolina Quadrangle dated
2016 (Figure 1), the site is at an approximate elevation of 645 feet above mean sea level. Surface runoff on the site is generally to the south-southwest towards the Tanyard Branch.
Subsurface Structures ECS did not identify subsurface structures associated with the subject site.
Land Use
The subject site is developed with the current used tire store, office and automotive garage. The
surrounding area consists of commercial properties.
4.0 FIELD ACTIVITIES
4.1 Monitoring Well Installation
On September 18, 2017, Quantex, on behalf of ECS, installed four permanent groundwater monitoring wells: MW-1 through MW-4, as shown on Figure 5. Monitoring well MW-1 was installed near the northern-most gravel-covered area of the site. Monitoring well MW-2 was
installed in the asphalt near the former dispensers along the eastern side of the entrance to the
Limited Site Assessment – Boulevard BP NW Corner of Clayton Avenue and North Madison Boulevard Roxboro, Person County, North Carolina NCDEQ Incident No: 14098
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site. Monitoring well MW-3 was installed in the asphalt area concealing the former gasoline UST
basin. Monitoring well MW-4 was installed in the grassy area in the downgradient, southern portion of the property near Clayton Avenue. Monitoring well MW-3 was completed using augers
and air rotary and monitoring wells MW-1, MW-2, and MW-4 were installed utilizing augers with
a GeoProbe. Details regarding monitoring well construction and groundwater elevation are included in Table 4, and shown on Figure 5 and Figure 6. ECS personnel field notes, boring
logs, and forms are included in Appendix B. Monitoring Well Construction Records are included in Appendix C. ECS observed an aboveground storage tank (AST) without a cap in the northern, rear portion of the property containing an unknown amount of an unknown liquid.
Staining was not observed on the surrounding ground, as shown in the site photographs, included in Appendix D.
4.2 Soil Borings and Soil Sampling
On September 18, 2017, ECS, with Quantex drilled soil borings to collect soil samples, for risk-based analysis, along the perimeter of the former gasoline UST location and two soil samples
near the former fuel dispensers at depths of five, 10, and 15 ft bgs (18 total soil samples) to
determine the extent of contaminated soils on the subject site. Additionally, ECS also collected soil samples from a depth of five, 10 and 15 ft. bgs from the borings for monitoring well MW-2
(SB-3), located near the former dispensers, and MW-3 (SB-4), located near the former gasoline
UST basin (six total soil samples). The locations of the soil borings are shown on Figure 7. A soil boring log representative of site soils is included in Appendix B.
The sample containers were labeled with ECS project number, sample identification, sample
date and time, and requested analytical analysis. The containers were placed into protective packaging material and placed into a cooler with ice to maintain the samples at approximately
4°C (°Celsius). The soil samples were submitted to Pace in Huntersville, North Carolina for chemical analysis for VOCs using EPA Method 8260, SVOCs using EPA Method 8270, VPH
and EPH using MADEP Methods. ECS maintained proper COC procedures throughout the
sample collection and transportation process. The laboratory analytical data sheets and COCs are included in Appendix E.
4.3 Monitoring Well Sampling
On September 19, 2017, ECS collected a field blank and groundwater samples from monitoring
wells MW-1 through MW-4. Subsequently, ECS submitted the field blank and groundwater
samples to Pace.
Prior to monitoring well sampling activities, the static groundwater elevation was measured in
each monitoring well using a decontaminated water level meter. ECS allowed the monitoring wells to equilibrate. Prior to beginning groundwater sampling activities, ECS collected the field
blank at the site by pouring laboratory grade deionized water over the water level meter probe and into the appropriate laboratory prepared sample containers.
Purging and sampling of the monitoring wells was accomplished using a dedicated new, disposable polypropylene bailer and nylon cord. Following completion of the purging, the groundwater bailed to the surface was decanted directly into sample containers provided by the
laboratory. Each monitoring well was purged until the following geochemical field measurements had stabilized; temperature, pH, conductivity, and dissolved oxygen. ECS utilized an YSI model 556 MPS water quality meter calibrated using the manufacturers recommendations.

Limited Site Assessment – Boulevard BP NW Corner of Clayton Avenue and North Madison Boulevard Roxboro, Person County, North Carolina NCDEQ Incident No: 14098
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The bottles were labeled with ECS project number, sample identification, sample date and time,
and requested analytical analysis. The containers were placed into protective packaging
material and placed into a cooler with ice to maintain the samples at approximately 4° C. The
groundwater samples were submitted to Pace for chemical analysis for VOCs using Standard Method 6200B, SVOCs using EPA Method 625 BNA with 10 largest non-target peaks, and
VPH and EPH using the MADEP Methods. ECS maintained proper COC procedures throughout
the sample collection and transportation process. The laboratory analytical data sheets and COCs are included in Appendix E.

4.4 Water Level Measurement
On September 19, 2017, ECS surveyed the relative elevation of the top of each monitoring well
casing (MW-1 through MW-4). Each well was measured to the nearest 0.01 feet using a level
and rod. The elevations were measured relative to an arbitrary benchmark (Soil vapor extraction well SVE-1), which was assigned an elevation of 100 feet. The relative elevation of the top of
casing for each monitoring well and the measurement of the depth to groundwater surface from the top of the monitoring well casing were used to determine the relative elevation of groundwater at each monitoring well location. Based on the survey data, groundwater is flowing
in a semi-radial pattern to the north, northwest, west, and southwest toward Tanyard Branch. A summary of the groundwater elevation data and calculated flow direction is presented in Table 4
and displayed on Figure 6.
5.0 LABORATORY ANALYTICAL RESULTS
5.1 Soil Samples
Laboratory analysis reported C9-C22 Aromatics at a concentration above its Residential MSCC in soil sample SB-3A but below its industrial MSCC.

Laboratory analysis reported several targeted analytes above their respective Soil-to-Water MSCCs but below their respective residential MSCCs in each of the soil samples SB-1B, SB-
3A, SB-3B, SB-3C, SB-4C, and SB-5A.
Laboratory analysis reported several targeted analytes at concentrations above their respective
laboratory reporting limits but below their respective Soil-to-Water MSCCs in each of the soil
samples SB-1C, SB-2B, SB-2C, SB-4B, SB-5B, SB-5C, SB-6B, SB-6C, SB-7C, and SB-8B.
Laboratory analysis did not report targeted analytes above their respective laboratory reporting limits in the soil samples SB-1A, SB-2A, SB-4A, SB-6A, SB-7A, SB-7B, SB-8A, and SB-8C.
The laboratory analytical data sheets and COCs are included in Appendix E. A summary of current soil analytical results are included in Table 5. A summary of historic soil analytical results are included in Table 2.

5.2 Monitoring Well Samples
Laboratory analysis did not report targeted analytes above their respective laboratory reporting limits in the field blank or in the groundwater samples collected from monitoring well MW-1.
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Laboratory analysis reported chloroform, 1,3,5-Trimethylbenzene, 1,2,4-Trimethylbenzene, total
xylenes, and n-propylbenzene at a concentration above its laboratory reporting limit but below its NC2LGWQS in the groundwater collected from monitoring well MW-2.

Laboratory analysis of the groundwater sample collected from monitoring well MW-3 reported methyl-tert-butyl ether (MTBE), naphthalene, and C9-C22 Aromatics at a concentration above their
respective NC2LGWQS but below their respective Gross Contaminant Level (GCL), if applicable, and reported additional analytes at a concentration above their respective laboratory reporting limit but below their respective NC2LGWQS.
Laboratory analysis of the groundwater collected from MW-4 reported MTBE at a concentration above its laboratory reporting limit but below its NC2LGWQS.
A summary of current groundwater analytical results are included in Table 6 and displayed on Figure 8. The laboratory analytical data sheets and COCs are included in Appendix E.
6.0 CONCLUSIONS
Based on the analytical results from the groundwater and soil samples, site observations, and
historical information available, ECS concludes the following:
• ECS identified four soil vapor extraction wells (SVE-1 through SVE-3) associated with
the subject site;
• ECS did not identify water supply wells within 1,000 feet of the site;
• Municipal water supply is connected to the subject site and available to the surrounding
areas within 1,000 feet of the site;
• The groundwater flow direction is generally to the southwest across the site;
• Groundwater does not appear to be impacted to the north and appears nominally impacted to the east and far west (in the direction of groundwater flow) as laboratory analysis of the groundwater collected from monitoring wells MW-2 and MW-4 reported
analytes at a concentration above their respective NC2LGWQS and laboratory analysis of groundwater collected from monitoring well MW-1 did not report any analytes above
their respective laboratory reporting limits;
• An unnamed, intermittent tributary of the Tanyard Branch is located off-site
approximately 110 feet south-southwest of the site and is not likely impacted as a
possible receptor; and,
• The contaminant plume is delineated vertically and appears to be oriented to the
southwest from the former gasoline UST basin, similar to the plume depicted in the 1995 SSE, therefore, ECS believes the plume has stabilized and is biodegrading.

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7.0 RECOMMENDATIONS

Based on the conclusions of this Limited Site Assessment, ECS recommends:
• ECS recommends a NRP for perpetual land use restrictions for soil (See Figure 9) and groundwater should be submitted for the site;
• ECS recommends that once the NRP has been recorded in the Person County Register of Deeds, the NCDEQ should consider issuing an NFA and consider the site for closure;
• Should NCDEQ decide to close the site, ECS recommends abandoning the four onsite monitoring wells and three soil vapor extraction wells using a certified well contractor;
and,
• ECS recommends that a copy of this report be submitted to the current property owner.

FIGURES
SOURCE:

USGS Topographic Map
Roxboro, North Carolina 7.5-Minute Quadrangle 2013
FIGURE 1
SITE LOCATION MAP
BOULEVARD BP PROPERTY
NW CORNER OF CLAYTON AVE and
NORTH MADISON BLVD ROXBORO, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO: TF-14098
ECS PROJECT NO.: 49:5108 1 = 24,000
FORMER DISPENSER
FORMER
KEROSENE UST
SITE
SOURCE: ENSCI Environmental, Inc.
January 24, 1995

Samples collected during December of 1994.
FIGURE 2
HISTORIC SOIL BORING LOCATION MAP
BOULEVARD BP PROPERTY
NW CORNER OF CLAYTON AVE and
NORTH MADISON BLVD ROXBORO, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO: TF-14098
ECS PROJECT NO.: 49:5108 NOT TO SCALE
FORMER DISPENSER
FORMER
KEROSENE UST
SITE
SOURCE:

PERSON COUNTY GIS 2013
FIGURE 3
SITE AERIAL MAP
BOULEVARD BP PROPERTY
NW CORNER OF CLAYTON AVE and
NORTH MADISON BLVD ROXBORO, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO: TF-14098
ECS PROJECT NO.: 49:5108 1 inch = 400 feet
500 ft.
Radius
1,000 ft.
Radius
SITE
SOURCE:

PERSON COUNTY GIS 2013
FIGURE 4
ADJACENT PROPERTIES MAP
BOULEVARD BP PROPERTY
NW CORNER OF CLAYTON AVE and
NORTH MADISON BLVD ROXBORO, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO: TF-14098
ECS PROJECT NO.: 49:5108 1 inch = 60 feet
1
2
3
4
5
6
7
LEGEND

Property Number Corresponding
with Table 3

SOURCE:

GOOGLE EARTH 2016
FIGURE 5
MONITORING WELL LOCATION MAP
BOULEVARD BP PROPERTY
NW CORNER OF CLAYTON AVE and
NORTH MADISON BLVD ROXBORO, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO: TF-14098
ECS PROJECT NO: 49:5108 1 inch = 20 feet
LEGEND

APPROXIMATE SOIL VAPOR EXTRACTION WELL LOCATION

APPROXIMATE MONITORING WELL LOCATION (MW)

SUBJECT PROPERTY BOUNDARY
FORMER
DISPENSER
MW-3
MW-2
MW-1 FORMER
KEROSENE UST
FORMER GASOLINE USTS
SVE-3
SVE-2
SVE-1
MW-4
SOURCE:

GOOGLE EARTH 2016
FIGURE 6
GROUNDWATER ELEVATION MAP
BOULEVARD BP PROPERTY
NW CORNER OF CLAYTON AVE and
NORTH MADISON BLVD ROXBORO, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO: TF-14098
ECS PROJECT NO: 49:5108 1 inch = 20 feet
LEGEND
SOIL VAPOR EXTRACTION WELL LOCATION
MONITORING WELL LOCATION (MW)
WATER TABLE CONTOUR LINE
DIRECTION OF GROUNDWATER FLOW
GROUNDWATER ELEVATION (ft. btoc)
FORMER
DISPENSER
MW-3
92.87
MW-2
93.01
MW-1
92.63
MW-4
91.61
FORMER
KEROSENE UST
FORMER GASOLINE USTS
93
92
SOURCE:

GOOGLE EARTH 2016
FIGURE 7
SOIL BORING LOCATION MAP
BOULEVARD BP PROPERTY
NW CORNER OF CLAYTON AVE and
NORTH MADISON BLVD ROXBORO, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO: TF-14098
ECS PROJECT NO: 49:5108 1 inch = 20 feet
FORMER GASOLINE USTS
LEGEND

SOIL BORING LOCATION
FORMER
KEROSENE UST
FORMER DISPENSER SB-8
SB-7
SB-6
MW-3 /
SB-4
SB-5
SB-2
SB-1
MW-2 /
SB-3
SOURCE:

GOOGLE EARTH 2016
FIGURE 8
GROUNDWATER CONCENTRATION MAP
BOULEVARD BP PROPERTY
NW CORNER OF CLAYTON AVE and
NORTH MADISON BLVD ROXBORO, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO: TF-14098
ECS PROJECT NO: 49:5108 1 inch = 20 feet
LEGEND

APPROXIMATE MONITORING WELL LOCATION (MW)
23.6 CONCENTRATION REPORTED EXCEEDS NC2LGWQS (µg/L)
BELOW LABROTORY REPORTING LIMITS
*SVOC data not depicted for monitoring wells MW-3 & MW-4.
MW-3
MW-1
BRL
BRL
Chloroform 0.94
1,3,5-Trimethylbenzene 1.5
1,2,4-Trimethylbenzene 5.5
Total Xylenes 1.1
n-Propylbenzene 0.93
Naphthalene 33.5
Toluene 4.2
Diisopropyl ether 0.97
Ethylbenzene 62.7
Isopropylbenzene 7.6
Methyl-tert-butyl ether 23.6
1,2,4-Trimethylbenzene 20.8
Total Xylenes 46.6
n-Propylbenzene 10.2
C5-C8 Aliphatics 186
C9-C18 Aliphatics 67.7
C9-C22 Aromatics 229
MW-2
Methyl-tert-butyl ether 7.1
MW-4
SOURCE:

GOOGLE EARTH 2016
FIGURE 9
ESTIMATED AREA OF SOILS EXCEEDING
RESIDENTIAL MSCCs
BOULEVARD BP PROPERTY NW CORNER OF CLAYTON AVE and
NORTH MADISON BLVD
ROXBORO, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO: TF-14098
ECS PROJECT NO: 49:5108 1 inch = 20 feet
FORMER GASOLINE USTS
LEGEND
Soil Boring Location

Soil Sample reported above the Soil-to-Water Maximum Contaminant
Concentration and Residential Soil Cleanup Level (MSCC)
Estimated Area where Residual Soils exceed the residential MSCC based on
Laboratory Analysis
FORMER
KEROSENE UST
FORMER DISPENSER SB-8
SB-7
SB-6
MW-3 /
SB-4
SB-5
SB-2
SB-1 MW-2 /
SB-3
Estimated Area
where soils
exceed
residential
MSCCs
TABLES
UST ID
Number
Last
Contents
Capacity
(in Gallons)
Burial Depth
(Base of UST)
Tank
Dimensions
Installation
Date
Removal
Date Status
1 Gasoline 2,000 13 feet 12'x 5.4'Unknown Sept. 1994 Removed
2 Gasoline 2,000 13 feet 12'x 5.4'Unknown Sept. 1994 Removed
3 Gasoline 2,000 13 feet 12'x 5.4'Unknown Sept. 1994 Removed
4 Kerosene 550 13 feet 45.5" x 76"Unknown Sept. 1994 Removed
UST Information
Table 1
ECS Project: 49:5108
NCDEQ Incident: TF-14098
Roxboro, Person County, North Carolina
NW Corner of Clayton Avenue and North Madison Boulevard
Boulevard BP
PARAMETER
Sample ID SB-1 SB-2 SB-3 SB-4 SB-5 SB-6 SB-7*SB-8 SB-9 B-1 B-2 B-3 B-4 B-5 B-6 B-7 B-8 B-9
Collection Date
Sample Depth
(ft bgs)15 15 15 15 15 15 15 2 2 18-20 18-20 18-20 18-20 18-20 3-5 7-9 3-5 3-5
TPH - GRO 46 1,300 301 220 BDL BDL BDL 1,900 19 BDL BDL BDL BDL BDL BDL 170 BDL BDL 10
* = SB-7 was also analyzed using EPA Method 3550 and reported as 'BDL,' below detection limit.
Results presented in milligrams per kilogram (mg/kg), analogous to parts per million (ppm)
mg/kg = Milligrams per Kilogram
Reportedly, soil boring SB-1 through SB-9 were collected during UST closure and soil borings B-1 through B-9 were collected during additional assessment. Locations of borings are shown on Figure 2.
Bold = Detected above the appropriate Action Level at the time of assessment.
NCDEQ Incident: TF-14098
Table 2
Summary of Historical Sample Analytical Results
Boulevard BP
NW Corner of Clayton Avenue and North Madison Boulevard
Roxboro, Person County, North Carolina
EPA Method 5030 - Total Petroleum Hydrocarbons - Gasoline Range Organics (TPH - GRO)
NCDEQ = North Carolina Department of Environmental Quality
ECS Project: 49:5108
ANALYTICAL RESULTS
PREVIOUS
NCDEQ Action
Level
12/5/1994 (?)12/6/1994 (?)
Identification Number on
Figure 4 GIS PIN Parcel Address on Tax
Card Owner and Owner Address
Active City
Water
Account
Water Well On-
Site Current Use Description
1 0906-11-56-9042 N MADISON BLVD
WOODY W RUFFIN
PO BOX 381
ROXBORO NC 27573
YES Unknown*Vacant Retail Center
Wooded, Undeveloped Land
2 0906-11-65-2748 712 N MADISON BLVD
PC BOARD OF ALCOHOLIC CONTROL
712 N MADISON BLVD ROXBORO NC 27573 YES NO ABC Store
3 0906-11-65-2528 700 N MADISON BLVD
PRINCE ROXBORO FD LLC
909 S SALEM ST
APEX NC 27502
YES Unknown**Dollar Store
4 0906-11-65-0359 115 CLAYTON AVE
RAY WILKINS
PO BOX 681
ROXBORO NC 27573
YES NO Printing Company
5 0906-11-55-8553 625 N MADISON BLVD
EMAD H & NADIA N MASOUD
9 SHADOW MOSS PL
DURHAM NC 27705
YES NO ***Resturant
6 0906-11-55-7587 CLAYTON AVE
DONNA NEWELL
PO BOX 1098
ROXBORO NC 27573
--Private Paved Drive
7 0906-11-55-8788 208/210 CLAYTON AVE
NEWELL & SONS
PO BOX 1098 ROXBORO NC 27573 YES Unknown**Automotive Repair
*ECS received a response letter from Mr. Ruffin and he indicated 'unknown' regarding the presence of a supply well but noted that the property was supplied with public water. ECS did not observe a supply well on this parcel on September 18, 2017.
**ECS did not receive a response letter from Newell & Sons or the Dollar Store. ECS did not observe a supply well on these parcels on September 18, 2017.
***ECS did not receive a response letter from the Masouds but spoke with Mr. Masoud on September 18, 2017 and he confirmed that no supply wells are present on this parcel.
ECS Project: 49:5108
Table 3
Adjacent Properties
Boulevard BP
NW Corner of Clayton Avenue and North Madison Boulevard
Roxboro, Person County, North Carolina
NCDEQ Incident: TF-14098
Monitoring
Well ID
Date
Measured
Casing
Diameter
(I.D. in.)
Date Installed
Total Well
Depth
(ft. btoc)
Screen Interval
(ft. btoc)
Depth to
Groundwater
(ft. btoc)
TOC
Elevation *
Groundwater
Elevation (ft)
MW-1 9/19/2017 2 September 18, 2017 29 14-29 16.74 92.63 75.89
MW-2 9/19/2017 2 September 18, 2017 30 15-30 13.02 93.01 79.99
MW-3 9/19/2017 2 September 18, 2017 29 13-28 17.82 92.87 75.05
MW-4 9/19/2017 2 September 18, 2017 30 15-30 18.28 91.61 73.33
I.D. in. = Inside Diameter of Casing in Inches
ft. btoc = Feet Below Top of Casing
* = Survey Data obtained from survey activities conducted on September 19, 2017
MW = Monitoring Well
NM = Not Measured
TOC = Top of Casing
Table 4
Monitoring Well Construction and Groundwater Elevation Details
Boulevard BP
NW Corner of Clayton Avenue and North Madison Boulevard
Roxboro, Person County, North Carolina
NCDEQ Incident: TF-14098
ECS Project: 49:5108
PARAMETER
Sample ID SB-1A SB-1B SB-1C SB-2A SB-2B SB-2C SB-3A SB-3B SB-3C SB-4A SB-4B SB-4C SB-5A SB-5B SB-5C SB-6A SB-6B SB-6C SB-7A SB-7B SB-7C SB-8A SB-8B SB-8C
Collection Date
Sample Depth
(ft bgs)4-6.5 7-11 12.5-15 3.5-6 7-11 11.5-15 4-6 8-11 14-15 4-6 8-11 14-16 3.5-6 8-11 14-15.5 3.5-6 7.5-11 13-15 3.5-6 7.5-11.5 11.5-15 3.5-6 7-11 11.5-15
n-Butylbenzene BRL BRL BRL BRL BRL BRL 6.5 6.9 1.6 BRL BRL BRL BRL BRL 0.029 BRL BRL BRL BRL BRL BRL BRL BRL BRL 4.3 626 16,350
Methyl-tert-butyl ether BRL BRL BRL BRL 0.0066 0.026 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.091 350 3,100
sec-Butylbenzene BRL BRL BRL BRL BRL BRL 2.2 2.3 0.45 BRL BRL 0.21 BRL BRL 0.0068 BRL BRL BRL BRL BRL BRL BRL BRL BRL 3.3 626 16,350
Isopropylbenzene BRL BRL BRL BRL BRL BRL 2.9 2.9 0.62 BRL BRL BRL BRL BRL 0.0073 BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.7 1,564 40,880
Ethylbenzene BRL BRL 0.014 BRL BRL BRL 2.1 2.2 0.62 BRL BRL BRL BRL BRL 0.020 BRL BRL BRL BRL BRL BRL BRL BRL BRL 4.9 1,560 40,000
p-Isopropyltoluene BRL BRL BRL BRL BRL BRL 3.8 3.9 0.96 BRL BRL 0.28 BRL BRL 0.017 BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.12 100 4,000
Naphthalene BRL 0.29 0.087 BRL BRL 0.0056 5.4 5.6 2.1 BRL BRL 0.30 BRL BRL 0.080 BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.16 313 8,176
Acetone BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.13 BRL BRL BRL BRL BRL BRL BRL 0.11 BRL 24 14,000 360,000
n-Propylbenzene BRL 0.22 BRL BRL BRL BRL 12.6 12.3 2.7 BRL BRL 0.71 BRL BRL 0.038 BRL BRL BRL BRL BRL BRL BRL BRL BRL 1.7 626 16,350
1,2,4-Trimethylbenzene BRL 1.1 0.13 BRL 0.015 0.013 51.6 56.8 14 BRL 0.14 1.6 BRL 0.010 0.28 BRL 0.029 BRL BRL BRL BRL BRL BRL BRL 8.5 782 20,440
1,3,5-Trimethylbenzene BRL 0.41 0.032 BRL BRL BRL 17.2 18.9 4.4 BRL BRL 0.42 BRL BRL 0.086 BRL 0.0090 BRL BRL BRL BRL BRL BRL BRL 8.5 782 20,440
Total Xylenes BRL 0.94 0.17 BRL BRL BRL 6.9 7.5 1.9 BRL BRL BRL BRL BRL 0.12 BRL 0.013 BRL BRL BRL BRL BRL BRL BRL 4.6 3,129 81,760
All Other VOCs BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
1-Methylnaphthalene BRL 0.52 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.004 20 100
2-Methylnaphthalene BRL 1.1 BRL BRL BRL BRL BRL BRL 0.52 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 3.6 63 1,635
Naphthalene BRL 0.87 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.16 313 8,176
All other SVOCs BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
Aliphatics (C5-C8)BRL 184 BRL BRL BRL BRL 612 110 303 BRL 60.0 13.9 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 68 939 24,528
Aliphatics (C9-C18)BRL 101 BRL BRL BRL BRL 117 27.9 68.3 BRL 12.4 5.8 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 540 1,500 40,000
Aliphatics (C19-C36)BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 16.7 BRL BRL 36.2 BRL BRL BRL BRL BRL BRL 32.8 BRL BRL BRL Immobile 31,000 810,000
Aromatics (C9-C22)BRL 254 4.4 BRL BRL BRL 485 109 255 BRL 21.6 5.7 34.8 BRL BRL BRL BRL 17.9 BRL BRL 19.1 BRL BRL BRL 31 469 12,264
Results presented in milligrams per kilogram (mg/kg), analogous to parts per million (ppm)
mg/kg = Milligrams per Kilogram
BOLD = Detected above the Soil-to-Water Maximum Contaminant Concentration and Residential Soil Cleanup Level
Bold = Detected above the Action Level or Soil-to-Water Maximum Contaminant Concentration
Soil Boring SB-1A was collected from 5 ft. bgs. Soil Boring SB-1B was collected from 10 ft. bgs. Soil Boring SB-1C was collected from 15 ft. bgs….Etc.
Table 5
Summary of Current Soil Analytical Results
Boulevard BP
NW Corner of Clayton Avenue and North Madison Boulevard
Roxboro, Person County, North Carolina
NCDEQ Incident: TF-14098
ECS Project: 49:5108
ANALYTICAL RESULTS
Soil-to-Water
Maximum
Contaminant
Concentration
Residential
Soil Cleanup
Level
Industrial/
Commercial
Soil Cleanup
Level
NCDEQ = North Carolina Department of Environmental Quality
9/18/2017
Volatile Organic Compounds (VOCs) by EPA Method 8260
--
Semi-Volatile Organic Compounds (SVOCs) by EPA Method 8270
--
Extractable Petroleum Hydrocarbons & Volatile Petroleum Hydrocarbons (EPH/VPH) by MADEP
Sample Identification MW-1 MW-2 MW-3 MW-4
Sample Date
Naphthalene BRL BRL 33.5 BRL 6 6,000
Toluene BRL BRL 4.2 BRL 600 260,000
Diisopropyl ether BRL BRL 0.97 BRL 70 70,000
Ethylbenzene BRL BRL 62.7 BRL 600 84,500
Isopropylbenzene BRL BRL 7.6 BRL 70 25,000
Methyl-tert-butyl ether BRL BRL 23.6 7.1 20 20,000
Chloroform BRL 0.94 BRL BRL 70 70,000
1,3,5-Trimethylbenzene BRL 1.5 BRL BRL 400 25,000
1,2,4-Trimethylbenzene BRL 5.5 20.8 BRL 400 28,500
Total Xylenes BRL 1.1 46.6 BRL 500 85,500
n-Propylbenzene BRL 0.93 10.2 BRL 70 30,000
2,4-Dinitrotoluene BRL BRL BRL 6.0 NE NE
Naphthalene BRL BRL 22.4 BRL 6 6,000
C5-C8 Aliphatics BRL BRL 186 BRL 400 NE
C9-C18 Aliphatics BRL BRL 67.7 BRL 700 NE
C19-C36 Aliphatics BRL BRL BRL BRL 10,000 NE
C9-C22 Aromatics BRL BRL 229 BRL 200 NE
NC2LGWQS = North Carolina 2L Groundwater Quality Standard
GCL = Gross Contaminant Level
NE = No Standard Established
µg/L= micrograms per liter = ppb (parts per billion)
Bold = Concentration Exceeds NC2LGWQS
Roxboro, Person County, North Carolina
Boulevard BP
Summary of Current Groundwater Analytical Results
Table 6
NW Corner of Clayton Avenue and North Madison Boulevard
Extractable Petroleum Hydrocarbons & Volatile Petroleum Hydrocarbons (EPH/VPH) by MADEP
SVOCs by EPA Method 625BNA
VOCs by Standard Method 6200B
ECS Project: 49:5108
NCDEQ Incident: TF-14098
NC2LGWQS GCL09/19/17
APPENDIX A
APPENDIX B

APPENDIX C
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3106-A
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NA
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663 N. Madison Blvd., Roxboro, NC 27573
Person NA
36.403470 78.979502
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copy of this record has been provided to the well owner.



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James D. Barker
3106-A
Quantex, Inc.
NA
✔
9/18/17 MW-4
Blvd. BP Property NA
663 N. Madison Blvd., Roxboro, NC 27573
Person NA
36.403292 78.979586
✔
✔
1
30'
NA
~7"
Auger
23 24 Stiff Reddish Brown SILT + PWR
0152 Sch 40 PVC
15 30 2 0.010 Sch 40 PVC
0 12 Neat Cement 365lbs. pour
12 14 Bentonite 3/8" pellet 40 lbs. pour
14 30 #2 silica sand Pour
0 21 Reddish Brown SILT
21 30 stiff Reddish Brown SILT some clay + PWR
10/6/17
APPENDIX D

SITE PHOTOGRAPHS
BOULEVARD BP PROPERTY

NW CORNER OF CLAYTON AVE and NORTH MADISON BLVD
ROXBORO, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO: TF-14098
ECS PROJECT NO.: 49:5108

Photograph 1: View of the subject site – office and garage. View is to the west.

Photograph 2: View of the subject site - sign. View is to the south.

SITE PHOTOGRAPHS
BOULEVARD BP PROPERTY

NW CORNER OF CLAYTON AVE and NORTH MADISON BLVD
ROXBORO, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO: TF-14098
ECS PROJECT NO.: 49:5108

Photograph 3: View of the rear of the subject site. View is to the north.

Photograph 4: View of AST without a cap containing an unknown amount of an unknown liquid. View is to
the southwest.

SITE PHOTOGRAPHS
BOULEVARD BP PROPERTY

NW CORNER OF CLAYTON AVE and NORTH MADISON BLVD
ROXBORO, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO: TF-14098
ECS PROJECT NO.: 49:5108

Photograph 5: View of monitoring well MW-1. View is to the north.

Photograph 6: View of monitoring well MW-4. View is to the northeast.

SITE PHOTOGRAPHS
BOULEVARD BP PROPERTY

NW CORNER OF CLAYTON AVE and NORTH MADISON BLVD
ROXBORO, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO: TF-14098
ECS PROJECT NO.: 49:5108

Photograph 7: View of the former gasoline UST basin and monitoring well MW-3. View is to the north.

Photograph 8: View of monitoring well MW-3. View is to the west.

SITE PHOTOGRAPHS
BOULEVARD BP PROPERTY

NW CORNER OF CLAYTON AVE and NORTH MADISON BLVD
ROXBORO, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO: TF-14098
ECS PROJECT NO.: 49:5108

Photograph 9: View of the subject site from Tanyard Branch. View is to the east.

Photograph 10: View of former dispenser island and soil vapor extraction wells (SVE) SVE -1 through SVE-
3. View is to the north-northeast.

SITE PHOTOGRAPHS
BOULEVARD BP PROPERTY

NW CORNER OF CLAYTON AVE and NORTH MADISON BLVD
ROXBORO, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO: TF-14098
ECS PROJECT NO.: 49:5108

Photograph 11: View of the western adjoining property.

Photograph 12: View of the southern adjacent properties across Clayton Avenue.

SITE PHOTOGRAPHS
BOULEVARD BP PROPERTY

NW CORNER OF CLAYTON AVE and NORTH MADISON BLVD
ROXBORO, PERSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT NO: TF-14098
ECS PROJECT NO.: 49:5108

Photograph 13: View of adjacent southeast property across N. Madison Boulevard.

Photograph 14: View of the northern adjoining property.

APPENDIX E
#=CL#
September 27, 2017
LIMS USE: FR - MATTHEW GILLIS
LIMS OBJECT ID: 92356169
92356169
Project:
Pace Project No.:
RE:
Matthew Gillis
ECS
9001 Glenwood Avenue
Raleigh, NC 27617
BOULEVARD 495108
Dear Matthew Gillis:
Enclosed are the analytical results for sample(s) received by the laboratory on September 20, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
cc:Sarah Kordon, ECS Southeast
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 42
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 42
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92356169001 MW-2 MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 625 60 PASI-CBPJ
SM 6200B 63 PASI-CGAW
92356169002 MW-3 MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 625 64 PASI-CBPJ
SM 6200B 63 PASI-CZDO
92356169003 MW-4 MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 625 58 PASI-CBPJ
SM 6200B 63 PASI-CZDO
92356169004 MW-1 MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 625 61 PASI-CBPJ
SM 6200B 63 PASI-CZDO
92356169005 FIELD BLANK SM 6200B 63 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 42
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92356169001 MW-2
6.633:Benzene, 1-ethyl-2-methy 5.7J ug/L 09/23/17 01:42 NEPA 625
20.169:Unknown 11.5J ug/L 09/23/17 01:42EPA 625
20.563:Unknown 5.8J ug/L 09/23/17 01:42EPA 625
Chloroform 0.94 ug/L 09/26/17 16:290.50SM 6200B
n-Propylbenzene 0.93 ug/L 09/26/17 16:290.50SM 6200B
1,2,4-Trimethylbenzene 5.5 ug/L 09/26/17 16:290.50SM 6200B
1,3,5-Trimethylbenzene 1.5 ug/L 09/26/17 16:290.50SM 6200B
m&p-Xylene 1.1 ug/L 09/26/17 16:291.0SM 6200B
92356169002 MW-3
Aliphatic (C05-C08)186 ug/L 09/25/17 16:57 N250.0MADEP VPH
Aliphatic (C09-C12)67.7 ug/L 09/25/17 16:57 N250.0MADEP VPH
Aromatic (C09-C10)229 ug/L 09/25/17 16:57 N250.0MADEP VPH
Naphthalene 22.4 ug/L 09/23/17 02:115.0EPA 625
6.633:1,2,4-Trimethylbenzene 18.9J ug/L 09/23/17 02:11 NEPA 625
6.984:Indane 54.3J ug/L 09/23/17 02:11 NEPA 625
7.052:Benzene, 1,4-diethyl-16.6J ug/L 09/23/17 02:11 NEPA 625
7.332:Benzene, 4-ethyl-1,2-dim 20.9J ug/L 09/23/17 02:11 NEPA 625
7.565:Benzene, 1,2,4,5-tetrame 8.1J ug/L 09/23/17 02:11 NEPA 625
7.745:1H-Indene, 2,3-dihydro-4 8.6J ug/L 09/23/17 02:11 NEPA 625
7.811:3-Phenylbut-1-ene 22.9J ug/L 09/23/17 02:11 NEPA 625
Diisopropyl ether 0.97 ug/L 09/26/17 18:470.50SM 6200B
Ethylbenzene 62.7 ug/L 09/26/17 18:470.50SM 6200B
Isopropylbenzene (Cumene)7.6 ug/L 09/26/17 18:470.50SM 6200B
Methyl-tert-butyl ether 23.6 ug/L 09/26/17 18:470.50SM 6200B
Naphthalene 33.5 ug/L 09/26/17 18:472.0SM 6200B
n-Propylbenzene 10.2 ug/L 09/26/17 18:470.50SM 6200B
Toluene 4.2 ug/L 09/26/17 18:470.50SM 6200B
1,2,4-Trimethylbenzene 20.8 ug/L 09/26/17 18:470.50SM 6200B
m&p-Xylene 43.2 ug/L 09/26/17 18:471.0SM 6200B
o-Xylene 3.4 ug/L 09/26/17 18:470.50SM 6200B
92356169003 MW-4
2,4-Dinitrotoluene 6.0 ug/L 09/23/17 02:415.0EPA 625
20.321:Unknown 7.8J ug/L 09/23/17 02:41EPA 625
Methyl-tert-butyl ether 7.1 ug/L 09/26/17 19:040.50SM 6200B
92356169004 MW-1
19.351:Unknown 8.5J ug/L 09/23/17 03:11EPA 625
20.277:Unknown 12.6J ug/L 09/23/17 03:11EPA 625
20.653:Unknown 7.0J ug/L 09/23/17 03:11EPA 625
21.362:Unknown 10.1J ug/L 09/23/17 03:11EPA 625
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Sample:MW-2 Lab ID:92356169001 Collected:09/19/17 11:20 Received:09/20/17 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 09/26/17 02:13 N209/25/17 11:041001
Aliphatic (C19-C36)ND ug/L 09/26/17 02:13 N209/25/17 11:041001
Aromatic (C11-C22)ND ug/L 09/26/17 02:13 N209/25/17 11:041001
Surrogates
Nonatriacontane (S)59 %09/26/17 02:13 7194-86-709/25/17 11:0440-140 1
o-Terphenyl (S)74 %09/26/17 02:13 84-15-109/25/17 11:0440-140 1
2-Fluorobiphenyl (S)100 %09/26/17 02:13 321-60-809/25/17 11:0440-140 1
2-Bromonaphthalene (S)96 %09/26/17 02:13 580-13-209/25/17 11:0440-140 1
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)ND ug/L 09/25/17 16:29 N250.0 1
Aliphatic (C09-C12)ND ug/L 09/25/17 16:29 N250.0 1
Aromatic (C09-C10)ND ug/L 09/25/17 16:29 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)95 %09/25/17 16:29 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)91 %09/25/17 16:29 460-00-470-130 1
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
Acenaphthene ND ug/L 09/23/17 01:42 83-32-909/22/17 11:155.0 1
Acenaphthylene ND ug/L 09/23/17 01:42 208-96-809/22/17 11:155.0 1
Anthracene ND ug/L 09/23/17 01:42 120-12-709/22/17 11:155.0 1
Benzo(a)anthracene ND ug/L 09/23/17 01:42 56-55-309/22/17 11:155.0 1
Benzo(a)pyrene ND ug/L 09/23/17 01:42 50-32-809/22/17 11:155.0 1
Benzo(b)fluoranthene ND ug/L 09/23/17 01:42 205-99-209/22/17 11:155.0 1
Benzo(g,h,i)perylene ND ug/L 09/23/17 01:42 191-24-209/22/17 11:155.0 1
Benzo(k)fluoranthene ND ug/L 09/23/17 01:42 207-08-909/22/17 11:155.0 1
4-Bromophenylphenyl ether ND ug/L 09/23/17 01:42 101-55-309/22/17 11:155.0 1
Butylbenzylphthalate ND ug/L 09/23/17 01:42 85-68-709/22/17 11:155.0 1
4-Chloro-3-methylphenol ND ug/L 09/23/17 01:42 59-50-709/22/17 11:155.0 1
bis(2-Chloroethoxy)methane ND ug/L 09/23/17 01:42 111-91-109/22/17 11:1510.0 1
bis(2-Chloroethyl) ether ND ug/L 09/23/17 01:42 111-44-409/22/17 11:155.0 1
2-Chloronaphthalene ND ug/L 09/23/17 01:42 91-58-709/22/17 11:155.0 1
2-Chlorophenol ND ug/L 09/23/17 01:42 95-57-809/22/17 11:155.0 1
4-Chlorophenylphenyl ether ND ug/L 09/23/17 01:42 7005-72-309/22/17 11:155.0 1
Chrysene ND ug/L 09/23/17 01:42 218-01-909/22/17 11:155.0 1
Dibenz(a,h)anthracene ND ug/L 09/23/17 01:42 53-70-309/22/17 11:155.0 1
3,3'-Dichlorobenzidine ND ug/L 09/23/17 01:42 91-94-109/22/17 11:1525.0 1
2,4-Dichlorophenol ND ug/L 09/23/17 01:42 120-83-209/22/17 11:155.0 1
Diethylphthalate ND ug/L 09/23/17 01:42 84-66-209/22/17 11:155.0 1
2,4-Dimethylphenol ND ug/L 09/23/17 01:42 105-67-909/22/17 11:1510.0 1
Dimethylphthalate ND ug/L 09/23/17 01:42 131-11-309/22/17 11:155.0 1
Di-n-butylphthalate ND ug/L 09/23/17 01:42 84-74-209/22/17 11:155.0 1
4,6-Dinitro-2-methylphenol ND ug/L 09/23/17 01:42 534-52-109/22/17 11:1520.0 1
2,4-Dinitrophenol ND ug/L 09/23/17 01:42 51-28-509/22/17 11:1550.0 1
2,4-Dinitrotoluene ND ug/L 09/23/17 01:42 121-14-209/22/17 11:155.0 1
2,6-Dinitrotoluene ND ug/L 09/23/17 01:42 606-20-209/22/17 11:155.0 1
Di-n-octylphthalate ND ug/L 09/23/17 01:42 117-84-009/22/17 11:155.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Sample:MW-2 Lab ID:92356169001 Collected:09/19/17 11:20 Received:09/20/17 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
bis(2-Ethylhexyl)phthalate ND ug/L 09/23/17 01:42 117-81-709/22/17 11:155.0 1
Fluoranthene ND ug/L 09/23/17 01:42 206-44-009/22/17 11:155.0 1
Fluorene ND ug/L 09/23/17 01:42 86-73-709/22/17 11:155.0 1
Hexachloro-1,3-butadiene ND ug/L 09/23/17 01:42 87-68-309/22/17 11:155.0 1
Hexachlorobenzene ND ug/L 09/23/17 01:42 118-74-109/22/17 11:155.0 1
Hexachlorocyclopentadiene ND ug/L 09/23/17 01:42 77-47-409/22/17 11:1510.0 1
Hexachloroethane ND ug/L 09/23/17 01:42 67-72-109/22/17 11:155.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/23/17 01:42 193-39-509/22/17 11:155.0 1
Isophorone ND ug/L 09/23/17 01:42 78-59-109/22/17 11:1510.0 1
Naphthalene ND ug/L 09/23/17 01:42 91-20-309/22/17 11:155.0 1
Nitrobenzene ND ug/L 09/23/17 01:42 98-95-309/22/17 11:155.0 1
2-Nitrophenol ND ug/L 09/23/17 01:42 88-75-509/22/17 11:155.0 1
4-Nitrophenol ND ug/L 09/23/17 01:42 100-02-709/22/17 11:1550.0 1
N-Nitrosodimethylamine ND ug/L 09/23/17 01:42 62-75-909/22/17 11:155.0 1
N-Nitroso-di-n-propylamine ND ug/L 09/23/17 01:42 621-64-709/22/17 11:155.0 1
N-Nitrosodiphenylamine ND ug/L 09/23/17 01:42 86-30-609/22/17 11:1510.0 1
Pentachlorophenol ND ug/L 09/23/17 01:42 87-86-509/22/17 11:1510.0 1
Phenanthrene ND ug/L 09/23/17 01:42 85-01-809/22/17 11:155.0 1
Phenol ND ug/L 09/23/17 01:42 108-95-209/22/17 11:155.0 1
Pyrene ND ug/L 09/23/17 01:42 129-00-009/22/17 11:155.0 1
1,2,4-Trichlorobenzene ND ug/L 09/23/17 01:42 120-82-109/22/17 11:155.0 1
2,4,6-Trichlorophenol ND ug/L 09/23/17 01:42 88-06-209/22/17 11:1510.0 1
Surrogates
Nitrobenzene-d5 (S)75 %09/23/17 01:42 4165-60-009/22/17 11:1510-120 1
2-Fluorobiphenyl (S)77 %09/23/17 01:42 321-60-809/22/17 11:1515-120 1
Terphenyl-d14 (S)44 %09/23/17 01:42 1718-51-009/22/17 11:1511-131 1
Phenol-d6 (S)24 %09/23/17 01:42 13127-88-309/22/17 11:1510-120 1
2-Fluorophenol (S)36 %09/23/17 01:42 367-12-409/22/17 11:1510-120 1
2,4,6-Tribromophenol (S)95 %09/23/17 01:42 118-79-609/22/17 11:1510-137 1
Tentatively Identified Compounds
Benzene, 1-ethyl-2-methy 5.7J ug/L 09/23/17 01:42 611-14-3 N09/22/17 11:151
Unknown 11.5J ug/L 09/23/17 01:4209/22/17 11:151
Unknown 5.8J ug/L 09/23/17 01:4209/22/17 11:151
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 09/26/17 16:29 71-43-20.50 1
Bromobenzene ND ug/L 09/26/17 16:29 108-86-10.50 1
Bromochloromethane ND ug/L 09/26/17 16:29 74-97-50.50 1
Bromodichloromethane ND ug/L 09/26/17 16:29 75-27-40.50 1
Bromoform ND ug/L 09/26/17 16:29 75-25-20.50 1
Bromomethane ND ug/L 09/26/17 16:29 74-83-95.0 1
n-Butylbenzene ND ug/L 09/26/17 16:29 104-51-80.50 1
sec-Butylbenzene ND ug/L 09/26/17 16:29 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/26/17 16:29 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/26/17 16:29 56-23-5 M10.50 1
Chlorobenzene ND ug/L 09/26/17 16:29 108-90-70.50 1
Chloroethane ND ug/L 09/26/17 16:29 75-00-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Sample:MW-2 Lab ID:92356169001 Collected:09/19/17 11:20 Received:09/20/17 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Chloroform 0.94 ug/L 09/26/17 16:29 67-66-30.50 1
Chloromethane ND ug/L 09/26/17 16:29 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/26/17 16:29 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/26/17 16:29 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/26/17 16:29 96-12-81.0 1
Dibromochloromethane ND ug/L 09/26/17 16:29 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/26/17 16:29 106-93-40.50 1
Dibromomethane ND ug/L 09/26/17 16:29 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/26/17 16:29 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/26/17 16:29 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/26/17 16:29 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/26/17 16:29 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/26/17 16:29 75-34-30.50 1
1,2-Dichloroethane ND ug/L 09/26/17 16:29 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/26/17 16:29 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/26/17 16:29 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/26/17 16:29 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/26/17 16:29 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/26/17 16:29 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/26/17 16:29 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/26/17 16:29 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/26/17 16:29 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/26/17 16:29 10061-02-60.50 1
Diisopropyl ether ND ug/L 09/26/17 16:29 108-20-30.50 1
Ethylbenzene ND ug/L 09/26/17 16:29 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/26/17 16:29 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 09/26/17 16:29 98-82-80.50 1
Methylene Chloride ND ug/L 09/26/17 16:29 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 09/26/17 16:29 1634-04-40.50 1
Naphthalene ND ug/L 09/26/17 16:29 91-20-32.0 1
n-Propylbenzene 0.93 ug/L 09/26/17 16:29 103-65-10.50 1
Styrene ND ug/L 09/26/17 16:29 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/26/17 16:29 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/26/17 16:29 79-34-50.50 1
Tetrachloroethene ND ug/L 09/26/17 16:29 127-18-40.50 1
Toluene ND ug/L 09/26/17 16:29 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/26/17 16:29 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/26/17 16:29 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/26/17 16:29 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/26/17 16:29 79-00-50.50 1
Trichloroethene ND ug/L 09/26/17 16:29 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/26/17 16:29 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/26/17 16:29 96-18-40.50 1
1,2,4-Trimethylbenzene 5.5 ug/L 09/26/17 16:29 95-63-60.50 1
1,3,5-Trimethylbenzene 1.5 ug/L 09/26/17 16:29 108-67-80.50 1
Vinyl chloride ND ug/L 09/26/17 16:29 75-01-41.0 1
m&p-Xylene 1.1 ug/L 09/26/17 16:29 179601-23-11.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 7 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Sample:MW-2 Lab ID:92356169001 Collected:09/19/17 11:20 Received:09/20/17 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
o-Xylene ND ug/L 09/26/17 16:29 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)114 %09/26/17 16:29 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %09/26/17 16:29 460-00-470-130 1
Toluene-d8 (S)100 %09/26/17 16:29 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Sample:MW-3 Lab ID:92356169002 Collected:09/19/17 13:45 Received:09/20/17 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 09/26/17 02:41 N209/25/17 11:041001
Aliphatic (C19-C36)ND ug/L 09/26/17 02:41 N209/25/17 11:041001
Aromatic (C11-C22)ND ug/L 09/26/17 02:41 N209/25/17 11:041001
Surrogates
Nonatriacontane (S)40 %09/26/17 02:41 7194-86-709/25/17 11:0440-140 1
o-Terphenyl (S)79 %09/26/17 02:41 84-15-109/25/17 11:0440-140 1
2-Fluorobiphenyl (S)102 %09/26/17 02:41 321-60-809/25/17 11:0440-140 1
2-Bromonaphthalene (S)101 %09/26/17 02:41 580-13-209/25/17 11:0440-140 1
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)186 ug/L 09/25/17 16:57 N250.0 1
Aliphatic (C09-C12)67.7 ug/L 09/25/17 16:57 N250.0 1
Aromatic (C09-C10)229 ug/L 09/25/17 16:57 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)89 %09/25/17 16:57 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)86 %09/25/17 16:57 460-00-470-130 1
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
Acenaphthene ND ug/L 09/23/17 02:11 83-32-909/22/17 11:155.0 1
Acenaphthylene ND ug/L 09/23/17 02:11 208-96-809/22/17 11:155.0 1
Anthracene ND ug/L 09/23/17 02:11 120-12-709/22/17 11:155.0 1
Benzo(a)anthracene ND ug/L 09/23/17 02:11 56-55-309/22/17 11:155.0 1
Benzo(a)pyrene ND ug/L 09/23/17 02:11 50-32-809/22/17 11:155.0 1
Benzo(b)fluoranthene ND ug/L 09/23/17 02:11 205-99-209/22/17 11:155.0 1
Benzo(g,h,i)perylene ND ug/L 09/23/17 02:11 191-24-209/22/17 11:155.0 1
Benzo(k)fluoranthene ND ug/L 09/23/17 02:11 207-08-909/22/17 11:155.0 1
4-Bromophenylphenyl ether ND ug/L 09/23/17 02:11 101-55-309/22/17 11:155.0 1
Butylbenzylphthalate ND ug/L 09/23/17 02:11 85-68-709/22/17 11:155.0 1
4-Chloro-3-methylphenol ND ug/L 09/23/17 02:11 59-50-709/22/17 11:155.0 1
bis(2-Chloroethoxy)methane ND ug/L 09/23/17 02:11 111-91-109/22/17 11:1510.0 1
bis(2-Chloroethyl) ether ND ug/L 09/23/17 02:11 111-44-409/22/17 11:155.0 1
2-Chloronaphthalene ND ug/L 09/23/17 02:11 91-58-709/22/17 11:155.0 1
2-Chlorophenol ND ug/L 09/23/17 02:11 95-57-809/22/17 11:155.0 1
4-Chlorophenylphenyl ether ND ug/L 09/23/17 02:11 7005-72-309/22/17 11:155.0 1
Chrysene ND ug/L 09/23/17 02:11 218-01-909/22/17 11:155.0 1
Dibenz(a,h)anthracene ND ug/L 09/23/17 02:11 53-70-309/22/17 11:155.0 1
3,3'-Dichlorobenzidine ND ug/L 09/23/17 02:11 91-94-109/22/17 11:1525.0 1
2,4-Dichlorophenol ND ug/L 09/23/17 02:11 120-83-209/22/17 11:155.0 1
Diethylphthalate ND ug/L 09/23/17 02:11 84-66-209/22/17 11:155.0 1
2,4-Dimethylphenol ND ug/L 09/23/17 02:11 105-67-909/22/17 11:1510.0 1
Dimethylphthalate ND ug/L 09/23/17 02:11 131-11-309/22/17 11:155.0 1
Di-n-butylphthalate ND ug/L 09/23/17 02:11 84-74-209/22/17 11:155.0 1
4,6-Dinitro-2-methylphenol ND ug/L 09/23/17 02:11 534-52-109/22/17 11:1520.0 1
2,4-Dinitrophenol ND ug/L 09/23/17 02:11 51-28-509/22/17 11:1550.0 1
2,4-Dinitrotoluene ND ug/L 09/23/17 02:11 121-14-209/22/17 11:155.0 1
2,6-Dinitrotoluene ND ug/L 09/23/17 02:11 606-20-209/22/17 11:155.0 1
Di-n-octylphthalate ND ug/L 09/23/17 02:11 117-84-009/22/17 11:155.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Sample:MW-3 Lab ID:92356169002 Collected:09/19/17 13:45 Received:09/20/17 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
bis(2-Ethylhexyl)phthalate ND ug/L 09/23/17 02:11 117-81-709/22/17 11:155.0 1
Fluoranthene ND ug/L 09/23/17 02:11 206-44-009/22/17 11:155.0 1
Fluorene ND ug/L 09/23/17 02:11 86-73-709/22/17 11:155.0 1
Hexachloro-1,3-butadiene ND ug/L 09/23/17 02:11 87-68-309/22/17 11:155.0 1
Hexachlorobenzene ND ug/L 09/23/17 02:11 118-74-109/22/17 11:155.0 1
Hexachlorocyclopentadiene ND ug/L 09/23/17 02:11 77-47-409/22/17 11:1510.0 1
Hexachloroethane ND ug/L 09/23/17 02:11 67-72-109/22/17 11:155.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/23/17 02:11 193-39-509/22/17 11:155.0 1
Isophorone ND ug/L 09/23/17 02:11 78-59-109/22/17 11:1510.0 1
Naphthalene 22.4 ug/L 09/23/17 02:11 91-20-309/22/17 11:155.0 1
Nitrobenzene ND ug/L 09/23/17 02:11 98-95-309/22/17 11:155.0 1
2-Nitrophenol ND ug/L 09/23/17 02:11 88-75-509/22/17 11:155.0 1
4-Nitrophenol ND ug/L 09/23/17 02:11 100-02-709/22/17 11:1550.0 1
N-Nitrosodimethylamine ND ug/L 09/23/17 02:11 62-75-909/22/17 11:155.0 1
N-Nitroso-di-n-propylamine ND ug/L 09/23/17 02:11 621-64-709/22/17 11:155.0 1
N-Nitrosodiphenylamine ND ug/L 09/23/17 02:11 86-30-609/22/17 11:1510.0 1
Pentachlorophenol ND ug/L 09/23/17 02:11 87-86-509/22/17 11:1510.0 1
Phenanthrene ND ug/L 09/23/17 02:11 85-01-809/22/17 11:155.0 1
Phenol ND ug/L 09/23/17 02:11 108-95-209/22/17 11:155.0 1
Pyrene ND ug/L 09/23/17 02:11 129-00-009/22/17 11:155.0 1
1,2,4-Trichlorobenzene ND ug/L 09/23/17 02:11 120-82-109/22/17 11:155.0 1
2,4,6-Trichlorophenol ND ug/L 09/23/17 02:11 88-06-209/22/17 11:1510.0 1
Surrogates
Nitrobenzene-d5 (S)76 %09/23/17 02:11 4165-60-009/22/17 11:1510-120 1
2-Fluorobiphenyl (S)78 %09/23/17 02:11 321-60-809/22/17 11:1515-120 1
Terphenyl-d14 (S)54 %09/23/17 02:11 1718-51-009/22/17 11:1511-131 1
Phenol-d6 (S)23 %09/23/17 02:11 13127-88-309/22/17 11:1510-120 1
2-Fluorophenol (S)36 %09/23/17 02:11 367-12-409/22/17 11:1510-120 1
2,4,6-Tribromophenol (S)96 %09/23/17 02:11 118-79-609/22/17 11:1510-137 1
Tentatively Identified Compounds
1,2,4-Trimethylbenzene 18.9J ug/L 09/23/17 02:11 95-36-3 N09/22/17 11:151
Indane 54.3J ug/L 09/23/17 02:11 496-11-7 N09/22/17 11:151
Benzene, 1,4-diethyl-16.6J ug/L 09/23/17 02:11 105-05-5 N09/22/17 11:151
Benzene, 4-ethyl-1,2-dim 20.9J ug/L 09/23/17 02:11 934-80-5 N09/22/17 11:151
Benzene, 1,2,4,5-tetrame 8.1J ug/L 09/23/17 02:11 95-93-2 N09/22/17 11:151
1H-Indene, 2,3-dihydro-4 8.6J ug/L 09/23/17 02:11 824-22-6 N09/22/17 11:151
3-Phenylbut-1-ene 22.9J ug/L 09/23/17 02:11 934-10-1 N09/22/17 11:151
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 09/26/17 18:47 71-43-20.50 1
Bromobenzene ND ug/L 09/26/17 18:47 108-86-10.50 1
Bromochloromethane ND ug/L 09/26/17 18:47 74-97-50.50 1
Bromodichloromethane ND ug/L 09/26/17 18:47 75-27-40.50 1
Bromoform ND ug/L 09/26/17 18:47 75-25-20.50 1
Bromomethane ND ug/L 09/26/17 18:47 74-83-95.0 1
n-Butylbenzene ND ug/L 09/26/17 18:47 104-51-80.50 1
sec-Butylbenzene ND ug/L 09/26/17 18:47 135-98-80.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Sample:MW-3 Lab ID:92356169002 Collected:09/19/17 13:45 Received:09/20/17 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
tert-Butylbenzene ND ug/L 09/26/17 18:47 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/26/17 18:47 56-23-50.50 1
Chlorobenzene ND ug/L 09/26/17 18:47 108-90-70.50 1
Chloroethane ND ug/L 09/26/17 18:47 75-00-31.0 1
Chloroform ND ug/L 09/26/17 18:47 67-66-30.50 1
Chloromethane ND ug/L 09/26/17 18:47 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/26/17 18:47 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/26/17 18:47 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/26/17 18:47 96-12-81.0 1
Dibromochloromethane ND ug/L 09/26/17 18:47 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/26/17 18:47 106-93-40.50 1
Dibromomethane ND ug/L 09/26/17 18:47 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/26/17 18:47 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/26/17 18:47 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/26/17 18:47 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/26/17 18:47 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/26/17 18:47 75-34-30.50 1
1,2-Dichloroethane ND ug/L 09/26/17 18:47 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/26/17 18:47 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/26/17 18:47 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/26/17 18:47 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/26/17 18:47 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/26/17 18:47 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/26/17 18:47 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/26/17 18:47 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/26/17 18:47 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/26/17 18:47 10061-02-60.50 1
Diisopropyl ether 0.97 ug/L 09/26/17 18:47 108-20-30.50 1
Ethylbenzene 62.7 ug/L 09/26/17 18:47 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/26/17 18:47 87-68-32.0 1
Isopropylbenzene (Cumene)7.6 ug/L 09/26/17 18:47 98-82-80.50 1
Methylene Chloride ND ug/L 09/26/17 18:47 75-09-22.0 1
Methyl-tert-butyl ether 23.6 ug/L 09/26/17 18:47 1634-04-40.50 1
Naphthalene 33.5 ug/L 09/26/17 18:47 91-20-32.0 1
n-Propylbenzene 10.2 ug/L 09/26/17 18:47 103-65-10.50 1
Styrene ND ug/L 09/26/17 18:47 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/26/17 18:47 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/26/17 18:47 79-34-50.50 1
Tetrachloroethene ND ug/L 09/26/17 18:47 127-18-40.50 1
Toluene 4.2 ug/L 09/26/17 18:47 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/26/17 18:47 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/26/17 18:47 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/26/17 18:47 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/26/17 18:47 79-00-50.50 1
Trichloroethene ND ug/L 09/26/17 18:47 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/26/17 18:47 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/26/17 18:47 96-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Sample:MW-3 Lab ID:92356169002 Collected:09/19/17 13:45 Received:09/20/17 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
1,2,4-Trimethylbenzene 20.8 ug/L 09/26/17 18:47 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 09/26/17 18:47 108-67-80.50 1
Vinyl chloride ND ug/L 09/26/17 18:47 75-01-41.0 1
m&p-Xylene 43.2 ug/L 09/26/17 18:47 179601-23-11.0 1
o-Xylene 3.4 ug/L 09/26/17 18:47 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)111 %09/26/17 18:47 17060-07-070-130 1
4-Bromofluorobenzene (S)104 %09/26/17 18:47 460-00-470-130 1
Toluene-d8 (S)99 %09/26/17 18:47 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Sample:MW-4 Lab ID:92356169003 Collected:09/19/17 11:55 Received:09/20/17 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 09/26/17 03:08 N209/25/17 11:041001
Aliphatic (C19-C36)ND ug/L 09/26/17 03:08 N209/25/17 11:041001
Aromatic (C11-C22)ND ug/L 09/26/17 03:08 N209/25/17 11:041001
Surrogates
Nonatriacontane (S)53 %09/26/17 03:08 7194-86-709/25/17 11:0440-140 1
o-Terphenyl (S)78 %09/26/17 03:08 84-15-109/25/17 11:0440-140 1
2-Fluorobiphenyl (S)103 %09/26/17 03:08 321-60-809/25/17 11:0440-140 1
2-Bromonaphthalene (S)85 %09/26/17 03:08 580-13-209/25/17 11:0440-140 1
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)ND ug/L 09/25/17 17:25 N250.0 1
Aliphatic (C09-C12)ND ug/L 09/25/17 17:25 N250.0 1
Aromatic (C09-C10)ND ug/L 09/25/17 17:25 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)94 %09/25/17 17:25 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)90 %09/25/17 17:25 460-00-470-130 1
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
Acenaphthene ND ug/L 09/23/17 02:41 83-32-909/22/17 11:155.0 1
Acenaphthylene ND ug/L 09/23/17 02:41 208-96-809/22/17 11:155.0 1
Anthracene ND ug/L 09/23/17 02:41 120-12-709/22/17 11:155.0 1
Benzo(a)anthracene ND ug/L 09/23/17 02:41 56-55-309/22/17 11:155.0 1
Benzo(a)pyrene ND ug/L 09/23/17 02:41 50-32-809/22/17 11:155.0 1
Benzo(b)fluoranthene ND ug/L 09/23/17 02:41 205-99-209/22/17 11:155.0 1
Benzo(g,h,i)perylene ND ug/L 09/23/17 02:41 191-24-209/22/17 11:155.0 1
Benzo(k)fluoranthene ND ug/L 09/23/17 02:41 207-08-909/22/17 11:155.0 1
4-Bromophenylphenyl ether ND ug/L 09/23/17 02:41 101-55-309/22/17 11:155.0 1
Butylbenzylphthalate ND ug/L 09/23/17 02:41 85-68-709/22/17 11:155.0 1
4-Chloro-3-methylphenol ND ug/L 09/23/17 02:41 59-50-709/22/17 11:155.0 1
bis(2-Chloroethoxy)methane ND ug/L 09/23/17 02:41 111-91-109/22/17 11:1510.0 1
bis(2-Chloroethyl) ether ND ug/L 09/23/17 02:41 111-44-409/22/17 11:155.0 1
2-Chloronaphthalene ND ug/L 09/23/17 02:41 91-58-709/22/17 11:155.0 1
2-Chlorophenol ND ug/L 09/23/17 02:41 95-57-809/22/17 11:155.0 1
4-Chlorophenylphenyl ether ND ug/L 09/23/17 02:41 7005-72-309/22/17 11:155.0 1
Chrysene ND ug/L 09/23/17 02:41 218-01-909/22/17 11:155.0 1
Dibenz(a,h)anthracene ND ug/L 09/23/17 02:41 53-70-309/22/17 11:155.0 1
3,3'-Dichlorobenzidine ND ug/L 09/23/17 02:41 91-94-109/22/17 11:1525.0 1
2,4-Dichlorophenol ND ug/L 09/23/17 02:41 120-83-209/22/17 11:155.0 1
Diethylphthalate ND ug/L 09/23/17 02:41 84-66-209/22/17 11:155.0 1
2,4-Dimethylphenol ND ug/L 09/23/17 02:41 105-67-909/22/17 11:1510.0 1
Dimethylphthalate ND ug/L 09/23/17 02:41 131-11-309/22/17 11:155.0 1
Di-n-butylphthalate ND ug/L 09/23/17 02:41 84-74-209/22/17 11:155.0 1
4,6-Dinitro-2-methylphenol ND ug/L 09/23/17 02:41 534-52-109/22/17 11:1520.0 1
2,4-Dinitrophenol ND ug/L 09/23/17 02:41 51-28-509/22/17 11:1550.0 1
2,4-Dinitrotoluene 6.0 ug/L 09/23/17 02:41 121-14-209/22/17 11:155.0 1
2,6-Dinitrotoluene ND ug/L 09/23/17 02:41 606-20-209/22/17 11:155.0 1
Di-n-octylphthalate ND ug/L 09/23/17 02:41 117-84-009/22/17 11:155.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Sample:MW-4 Lab ID:92356169003 Collected:09/19/17 11:55 Received:09/20/17 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
bis(2-Ethylhexyl)phthalate ND ug/L 09/23/17 02:41 117-81-709/22/17 11:155.0 1
Fluoranthene ND ug/L 09/23/17 02:41 206-44-009/22/17 11:155.0 1
Fluorene ND ug/L 09/23/17 02:41 86-73-709/22/17 11:155.0 1
Hexachloro-1,3-butadiene ND ug/L 09/23/17 02:41 87-68-309/22/17 11:155.0 1
Hexachlorobenzene ND ug/L 09/23/17 02:41 118-74-109/22/17 11:155.0 1
Hexachlorocyclopentadiene ND ug/L 09/23/17 02:41 77-47-409/22/17 11:1510.0 1
Hexachloroethane ND ug/L 09/23/17 02:41 67-72-109/22/17 11:155.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/23/17 02:41 193-39-509/22/17 11:155.0 1
Isophorone ND ug/L 09/23/17 02:41 78-59-109/22/17 11:1510.0 1
Naphthalene ND ug/L 09/23/17 02:41 91-20-309/22/17 11:155.0 1
Nitrobenzene ND ug/L 09/23/17 02:41 98-95-309/22/17 11:155.0 1
2-Nitrophenol ND ug/L 09/23/17 02:41 88-75-509/22/17 11:155.0 1
4-Nitrophenol ND ug/L 09/23/17 02:41 100-02-709/22/17 11:1550.0 1
N-Nitrosodimethylamine ND ug/L 09/23/17 02:41 62-75-909/22/17 11:155.0 1
N-Nitroso-di-n-propylamine ND ug/L 09/23/17 02:41 621-64-709/22/17 11:155.0 1
N-Nitrosodiphenylamine ND ug/L 09/23/17 02:41 86-30-609/22/17 11:1510.0 1
Pentachlorophenol ND ug/L 09/23/17 02:41 87-86-509/22/17 11:1510.0 1
Phenanthrene ND ug/L 09/23/17 02:41 85-01-809/22/17 11:155.0 1
Phenol ND ug/L 09/23/17 02:41 108-95-209/22/17 11:155.0 1
Pyrene ND ug/L 09/23/17 02:41 129-00-009/22/17 11:155.0 1
1,2,4-Trichlorobenzene ND ug/L 09/23/17 02:41 120-82-109/22/17 11:155.0 1
2,4,6-Trichlorophenol ND ug/L 09/23/17 02:41 88-06-209/22/17 11:1510.0 1
Surrogates
Nitrobenzene-d5 (S)77 %09/23/17 02:41 4165-60-009/22/17 11:1510-120 1
2-Fluorobiphenyl (S)77 %09/23/17 02:41 321-60-809/22/17 11:1515-120 1
Terphenyl-d14 (S)69 %09/23/17 02:41 1718-51-009/22/17 11:1511-131 1
Phenol-d6 (S)24 %09/23/17 02:41 13127-88-309/22/17 11:1510-120 1
2-Fluorophenol (S)37 %09/23/17 02:41 367-12-409/22/17 11:1510-120 1
2,4,6-Tribromophenol (S)90 %09/23/17 02:41 118-79-609/22/17 11:1510-137 1
Tentatively Identified Compounds
Unknown 7.8J ug/L 09/23/17 02:4109/22/17 11:151
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 09/26/17 19:04 71-43-20.50 1
Bromobenzene ND ug/L 09/26/17 19:04 108-86-10.50 1
Bromochloromethane ND ug/L 09/26/17 19:04 74-97-50.50 1
Bromodichloromethane ND ug/L 09/26/17 19:04 75-27-40.50 1
Bromoform ND ug/L 09/26/17 19:04 75-25-20.50 1
Bromomethane ND ug/L 09/26/17 19:04 74-83-95.0 1
n-Butylbenzene ND ug/L 09/26/17 19:04 104-51-80.50 1
sec-Butylbenzene ND ug/L 09/26/17 19:04 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/26/17 19:04 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/26/17 19:04 56-23-50.50 1
Chlorobenzene ND ug/L 09/26/17 19:04 108-90-70.50 1
Chloroethane ND ug/L 09/26/17 19:04 75-00-31.0 1
Chloroform ND ug/L 09/26/17 19:04 67-66-30.50 1
Chloromethane ND ug/L 09/26/17 19:04 74-87-31.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Sample:MW-4 Lab ID:92356169003 Collected:09/19/17 11:55 Received:09/20/17 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
2-Chlorotoluene ND ug/L 09/26/17 19:04 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/26/17 19:04 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/26/17 19:04 96-12-81.0 1
Dibromochloromethane ND ug/L 09/26/17 19:04 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/26/17 19:04 106-93-40.50 1
Dibromomethane ND ug/L 09/26/17 19:04 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/26/17 19:04 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/26/17 19:04 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/26/17 19:04 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/26/17 19:04 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/26/17 19:04 75-34-30.50 1
1,2-Dichloroethane ND ug/L 09/26/17 19:04 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/26/17 19:04 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/26/17 19:04 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/26/17 19:04 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/26/17 19:04 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/26/17 19:04 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/26/17 19:04 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/26/17 19:04 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/26/17 19:04 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/26/17 19:04 10061-02-60.50 1
Diisopropyl ether ND ug/L 09/26/17 19:04 108-20-30.50 1
Ethylbenzene ND ug/L 09/26/17 19:04 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/26/17 19:04 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 09/26/17 19:04 98-82-80.50 1
Methylene Chloride ND ug/L 09/26/17 19:04 75-09-22.0 1
Methyl-tert-butyl ether 7.1 ug/L 09/26/17 19:04 1634-04-40.50 1
Naphthalene ND ug/L 09/26/17 19:04 91-20-32.0 1
n-Propylbenzene ND ug/L 09/26/17 19:04 103-65-10.50 1
Styrene ND ug/L 09/26/17 19:04 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/26/17 19:04 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/26/17 19:04 79-34-50.50 1
Tetrachloroethene ND ug/L 09/26/17 19:04 127-18-40.50 1
Toluene ND ug/L 09/26/17 19:04 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/26/17 19:04 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/26/17 19:04 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/26/17 19:04 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/26/17 19:04 79-00-50.50 1
Trichloroethene ND ug/L 09/26/17 19:04 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/26/17 19:04 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/26/17 19:04 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 09/26/17 19:04 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 09/26/17 19:04 108-67-80.50 1
Vinyl chloride ND ug/L 09/26/17 19:04 75-01-41.0 1
m&p-Xylene ND ug/L 09/26/17 19:04 179601-23-11.0 1
o-Xylene ND ug/L 09/26/17 19:04 95-47-60.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Sample:MW-4 Lab ID:92356169003 Collected:09/19/17 11:55 Received:09/20/17 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Surrogates
1,2-Dichloroethane-d4 (S)113 %09/26/17 19:04 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %09/26/17 19:04 460-00-470-130 1
Toluene-d8 (S)101 %09/26/17 19:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Sample:MW-1 Lab ID:92356169004 Collected:09/19/17 12:55 Received:09/20/17 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Water
Aliphatic (C09-C18)ND ug/L 09/26/17 03:35 N209/25/17 11:041001
Aliphatic (C19-C36)ND ug/L 09/26/17 03:35 N209/25/17 11:041001
Aromatic (C11-C22)ND ug/L 09/26/17 03:35 N209/25/17 11:041001
Surrogates
Nonatriacontane (S)47 %09/26/17 03:35 7194-86-709/25/17 11:0440-140 1
o-Terphenyl (S)59 %09/26/17 03:35 84-15-109/25/17 11:0440-140 1
2-Fluorobiphenyl (S)80 %09/26/17 03:35 321-60-809/25/17 11:0440-140 1
2-Bromonaphthalene (S)80 %09/26/17 03:35 580-13-209/25/17 11:0440-140 1
Analytical Method: MADEP VPHVPH NC Water
Aliphatic (C05-C08)ND ug/L 09/25/17 17:52 N250.0 1
Aliphatic (C09-C12)ND ug/L 09/25/17 17:52 N250.0 1
Aromatic (C09-C10)ND ug/L 09/25/17 17:52 N250.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)92 %09/25/17 17:52 460-00-470-130 1
4-Bromofluorobenzene (PID) (S)88 %09/25/17 17:52 460-00-470-130 1
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
Acenaphthene ND ug/L 09/23/17 03:11 83-32-909/22/17 11:155.0 1
Acenaphthylene ND ug/L 09/23/17 03:11 208-96-809/22/17 11:155.0 1
Anthracene ND ug/L 09/23/17 03:11 120-12-709/22/17 11:155.0 1
Benzo(a)anthracene ND ug/L 09/23/17 03:11 56-55-309/22/17 11:155.0 1
Benzo(a)pyrene ND ug/L 09/23/17 03:11 50-32-809/22/17 11:155.0 1
Benzo(b)fluoranthene ND ug/L 09/23/17 03:11 205-99-209/22/17 11:155.0 1
Benzo(g,h,i)perylene ND ug/L 09/23/17 03:11 191-24-209/22/17 11:155.0 1
Benzo(k)fluoranthene ND ug/L 09/23/17 03:11 207-08-909/22/17 11:155.0 1
4-Bromophenylphenyl ether ND ug/L 09/23/17 03:11 101-55-309/22/17 11:155.0 1
Butylbenzylphthalate ND ug/L 09/23/17 03:11 85-68-709/22/17 11:155.0 1
4-Chloro-3-methylphenol ND ug/L 09/23/17 03:11 59-50-709/22/17 11:155.0 1
bis(2-Chloroethoxy)methane ND ug/L 09/23/17 03:11 111-91-109/22/17 11:1510.0 1
bis(2-Chloroethyl) ether ND ug/L 09/23/17 03:11 111-44-409/22/17 11:155.0 1
2-Chloronaphthalene ND ug/L 09/23/17 03:11 91-58-709/22/17 11:155.0 1
2-Chlorophenol ND ug/L 09/23/17 03:11 95-57-809/22/17 11:155.0 1
4-Chlorophenylphenyl ether ND ug/L 09/23/17 03:11 7005-72-309/22/17 11:155.0 1
Chrysene ND ug/L 09/23/17 03:11 218-01-909/22/17 11:155.0 1
Dibenz(a,h)anthracene ND ug/L 09/23/17 03:11 53-70-309/22/17 11:155.0 1
3,3'-Dichlorobenzidine ND ug/L 09/23/17 03:11 91-94-109/22/17 11:1525.0 1
2,4-Dichlorophenol ND ug/L 09/23/17 03:11 120-83-209/22/17 11:155.0 1
Diethylphthalate ND ug/L 09/23/17 03:11 84-66-209/22/17 11:155.0 1
2,4-Dimethylphenol ND ug/L 09/23/17 03:11 105-67-909/22/17 11:1510.0 1
Dimethylphthalate ND ug/L 09/23/17 03:11 131-11-309/22/17 11:155.0 1
Di-n-butylphthalate ND ug/L 09/23/17 03:11 84-74-209/22/17 11:155.0 1
4,6-Dinitro-2-methylphenol ND ug/L 09/23/17 03:11 534-52-109/22/17 11:1520.0 1
2,4-Dinitrophenol ND ug/L 09/23/17 03:11 51-28-509/22/17 11:1550.0 1
2,4-Dinitrotoluene ND ug/L 09/23/17 03:11 121-14-209/22/17 11:155.0 1
2,6-Dinitrotoluene ND ug/L 09/23/17 03:11 606-20-209/22/17 11:155.0 1
Di-n-octylphthalate ND ug/L 09/23/17 03:11 117-84-009/22/17 11:155.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Sample:MW-1 Lab ID:92356169004 Collected:09/19/17 12:55 Received:09/20/17 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 625 Preparation Method: EPA 625625 MSSV
bis(2-Ethylhexyl)phthalate ND ug/L 09/23/17 03:11 117-81-709/22/17 11:155.0 1
Fluoranthene ND ug/L 09/23/17 03:11 206-44-009/22/17 11:155.0 1
Fluorene ND ug/L 09/23/17 03:11 86-73-709/22/17 11:155.0 1
Hexachloro-1,3-butadiene ND ug/L 09/23/17 03:11 87-68-309/22/17 11:155.0 1
Hexachlorobenzene ND ug/L 09/23/17 03:11 118-74-109/22/17 11:155.0 1
Hexachlorocyclopentadiene ND ug/L 09/23/17 03:11 77-47-409/22/17 11:1510.0 1
Hexachloroethane ND ug/L 09/23/17 03:11 67-72-109/22/17 11:155.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/23/17 03:11 193-39-509/22/17 11:155.0 1
Isophorone ND ug/L 09/23/17 03:11 78-59-109/22/17 11:1510.0 1
Naphthalene ND ug/L 09/23/17 03:11 91-20-309/22/17 11:155.0 1
Nitrobenzene ND ug/L 09/23/17 03:11 98-95-309/22/17 11:155.0 1
2-Nitrophenol ND ug/L 09/23/17 03:11 88-75-509/22/17 11:155.0 1
4-Nitrophenol ND ug/L 09/23/17 03:11 100-02-709/22/17 11:1550.0 1
N-Nitrosodimethylamine ND ug/L 09/23/17 03:11 62-75-909/22/17 11:155.0 1
N-Nitroso-di-n-propylamine ND ug/L 09/23/17 03:11 621-64-709/22/17 11:155.0 1
N-Nitrosodiphenylamine ND ug/L 09/23/17 03:11 86-30-609/22/17 11:1510.0 1
Pentachlorophenol ND ug/L 09/23/17 03:11 87-86-509/22/17 11:1510.0 1
Phenanthrene ND ug/L 09/23/17 03:11 85-01-809/22/17 11:155.0 1
Phenol ND ug/L 09/23/17 03:11 108-95-209/22/17 11:155.0 1
Pyrene ND ug/L 09/23/17 03:11 129-00-009/22/17 11:155.0 1
1,2,4-Trichlorobenzene ND ug/L 09/23/17 03:11 120-82-109/22/17 11:155.0 1
2,4,6-Trichlorophenol ND ug/L 09/23/17 03:11 88-06-209/22/17 11:1510.0 1
Surrogates
Nitrobenzene-d5 (S)86 %09/23/17 03:11 4165-60-009/22/17 11:1510-120 1
2-Fluorobiphenyl (S)75 %09/23/17 03:11 321-60-809/22/17 11:1515-120 1
Terphenyl-d14 (S)64 %09/23/17 03:11 1718-51-009/22/17 11:1511-131 1
Phenol-d6 (S)24 %09/23/17 03:11 13127-88-309/22/17 11:1510-120 1
2-Fluorophenol (S)38 %09/23/17 03:11 367-12-409/22/17 11:1510-120 1
2,4,6-Tribromophenol (S)92 %09/23/17 03:11 118-79-609/22/17 11:1510-137 1
Tentatively Identified Compounds
Unknown 8.5J ug/L 09/23/17 03:1109/22/17 11:151
Unknown 12.6J ug/L 09/23/17 03:1109/22/17 11:151
Unknown 7.0J ug/L 09/23/17 03:1109/22/17 11:151
Unknown 10.1J ug/L 09/23/17 03:1109/22/17 11:151
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 09/26/17 19:21 71-43-20.50 1
Bromobenzene ND ug/L 09/26/17 19:21 108-86-10.50 1
Bromochloromethane ND ug/L 09/26/17 19:21 74-97-50.50 1
Bromodichloromethane ND ug/L 09/26/17 19:21 75-27-40.50 1
Bromoform ND ug/L 09/26/17 19:21 75-25-20.50 1
Bromomethane ND ug/L 09/26/17 19:21 74-83-95.0 1
n-Butylbenzene ND ug/L 09/26/17 19:21 104-51-80.50 1
sec-Butylbenzene ND ug/L 09/26/17 19:21 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/26/17 19:21 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/26/17 19:21 56-23-50.50 1
Chlorobenzene ND ug/L 09/26/17 19:21 108-90-70.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 18 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Sample:MW-1 Lab ID:92356169004 Collected:09/19/17 12:55 Received:09/20/17 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Chloroethane ND ug/L 09/26/17 19:21 75-00-31.0 1
Chloroform ND ug/L 09/26/17 19:21 67-66-30.50 1
Chloromethane ND ug/L 09/26/17 19:21 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/26/17 19:21 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/26/17 19:21 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/26/17 19:21 96-12-81.0 1
Dibromochloromethane ND ug/L 09/26/17 19:21 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/26/17 19:21 106-93-40.50 1
Dibromomethane ND ug/L 09/26/17 19:21 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/26/17 19:21 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/26/17 19:21 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/26/17 19:21 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/26/17 19:21 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/26/17 19:21 75-34-30.50 1
1,2-Dichloroethane ND ug/L 09/26/17 19:21 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/26/17 19:21 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/26/17 19:21 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/26/17 19:21 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/26/17 19:21 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/26/17 19:21 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/26/17 19:21 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/26/17 19:21 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/26/17 19:21 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/26/17 19:21 10061-02-60.50 1
Diisopropyl ether ND ug/L 09/26/17 19:21 108-20-30.50 1
Ethylbenzene ND ug/L 09/26/17 19:21 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/26/17 19:21 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 09/26/17 19:21 98-82-80.50 1
Methylene Chloride ND ug/L 09/26/17 19:21 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 09/26/17 19:21 1634-04-40.50 1
Naphthalene ND ug/L 09/26/17 19:21 91-20-32.0 1
n-Propylbenzene ND ug/L 09/26/17 19:21 103-65-10.50 1
Styrene ND ug/L 09/26/17 19:21 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/26/17 19:21 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/26/17 19:21 79-34-50.50 1
Tetrachloroethene ND ug/L 09/26/17 19:21 127-18-40.50 1
Toluene ND ug/L 09/26/17 19:21 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/26/17 19:21 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/26/17 19:21 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/26/17 19:21 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/26/17 19:21 79-00-50.50 1
Trichloroethene ND ug/L 09/26/17 19:21 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/26/17 19:21 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/26/17 19:21 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 09/26/17 19:21 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 09/26/17 19:21 108-67-80.50 1
Vinyl chloride ND ug/L 09/26/17 19:21 75-01-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 19 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Sample:MW-1 Lab ID:92356169004 Collected:09/19/17 12:55 Received:09/20/17 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
m&p-Xylene ND ug/L 09/26/17 19:21 179601-23-11.0 1
o-Xylene ND ug/L 09/26/17 19:21 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)109 %09/26/17 19:21 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %09/26/17 19:21 460-00-470-130 1
Toluene-d8 (S)102 %09/26/17 19:21 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 20 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Sample:FIELD BLANK Lab ID:92356169005 Collected:09/19/17 10:35 Received:09/20/17 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 09/26/17 10:45 71-43-20.50 1
Bromobenzene ND ug/L 09/26/17 10:45 108-86-10.50 1
Bromochloromethane ND ug/L 09/26/17 10:45 74-97-50.50 1
Bromodichloromethane ND ug/L 09/26/17 10:45 75-27-40.50 1
Bromoform ND ug/L 09/26/17 10:45 75-25-20.50 1
Bromomethane ND ug/L 09/26/17 10:45 74-83-95.0 1
n-Butylbenzene ND ug/L 09/26/17 10:45 104-51-80.50 1
sec-Butylbenzene ND ug/L 09/26/17 10:45 135-98-80.50 1
tert-Butylbenzene ND ug/L 09/26/17 10:45 98-06-60.50 1
Carbon tetrachloride ND ug/L 09/26/17 10:45 56-23-50.50 1
Chlorobenzene ND ug/L 09/26/17 10:45 108-90-70.50 1
Chloroethane ND ug/L 09/26/17 10:45 75-00-31.0 1
Chloroform ND ug/L 09/26/17 10:45 67-66-30.50 1
Chloromethane ND ug/L 09/26/17 10:45 74-87-31.0 1
2-Chlorotoluene ND ug/L 09/26/17 10:45 95-49-80.50 1
4-Chlorotoluene ND ug/L 09/26/17 10:45 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 09/26/17 10:45 96-12-81.0 1
Dibromochloromethane ND ug/L 09/26/17 10:45 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 09/26/17 10:45 106-93-40.50 1
Dibromomethane ND ug/L 09/26/17 10:45 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 09/26/17 10:45 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 09/26/17 10:45 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 09/26/17 10:45 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 09/26/17 10:45 75-71-80.50 1
1,1-Dichloroethane ND ug/L 09/26/17 10:45 75-34-30.50 1
1,2-Dichloroethane ND ug/L 09/26/17 10:45 107-06-20.50 1
1,1-Dichloroethene ND ug/L 09/26/17 10:45 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 09/26/17 10:45 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 09/26/17 10:45 156-60-50.50 1
1,2-Dichloropropane ND ug/L 09/26/17 10:45 78-87-50.50 1
1,3-Dichloropropane ND ug/L 09/26/17 10:45 142-28-90.50 1
2,2-Dichloropropane ND ug/L 09/26/17 10:45 594-20-70.50 1
1,1-Dichloropropene ND ug/L 09/26/17 10:45 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 09/26/17 10:45 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 09/26/17 10:45 10061-02-60.50 1
Diisopropyl ether ND ug/L 09/26/17 10:45 108-20-30.50 1
Ethylbenzene ND ug/L 09/26/17 10:45 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 09/26/17 10:45 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 09/26/17 10:45 98-82-80.50 1
Methylene Chloride ND ug/L 09/26/17 10:45 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 09/26/17 10:45 1634-04-40.50 1
Naphthalene ND ug/L 09/26/17 10:45 91-20-32.0 1
n-Propylbenzene ND ug/L 09/26/17 10:45 103-65-10.50 1
Styrene ND ug/L 09/26/17 10:45 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 09/26/17 10:45 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 09/26/17 10:45 79-34-50.50 1
Tetrachloroethene ND ug/L 09/26/17 10:45 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 42
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Sample:FIELD BLANK Lab ID:92356169005 Collected:09/19/17 10:35 Received:09/20/17 10:20 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 09/26/17 10:45 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 09/26/17 10:45 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 09/26/17 10:45 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 09/26/17 10:45 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 09/26/17 10:45 79-00-50.50 1
Trichloroethene ND ug/L 09/26/17 10:45 79-01-60.50 1
Trichlorofluoromethane ND ug/L 09/26/17 10:45 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 09/26/17 10:45 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 09/26/17 10:45 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 09/26/17 10:45 108-67-80.50 1
Vinyl chloride ND ug/L 09/26/17 10:45 75-01-41.0 1
m&p-Xylene ND ug/L 09/26/17 10:45 179601-23-11.0 1
o-Xylene ND ug/L 09/26/17 10:45 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)107 %09/26/17 10:45 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %09/26/17 10:45 460-00-470-130 1
Toluene-d8 (S)100 %09/26/17 10:45 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
379189
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples:92356169001, 92356169002, 92356169003, 92356169004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2101288
Associated Lab Samples:92356169001, 92356169002, 92356169003, 92356169004
Matrix:Water
Analyzed
Aliphatic (C05-C08)ug/L ND 50.0 N209/25/17 16:01
Aliphatic (C09-C12)ug/L ND 50.0 N209/25/17 16:01
Aromatic (C09-C10)ug/L ND 50.0 N209/25/17 16:01
4-Bromofluorobenzene (FID) (S)%97 70-130 09/25/17 16:01
4-Bromofluorobenzene (PID) (S)%94 70-130 09/25/17 16:01
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2101289LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2101290
Aliphatic (C05-C08)ug/L 266 N23008970-13084252 5 25
Aliphatic (C09-C12)ug/L 281 N23009430-13093279 1 25
Aromatic (C09-C10)ug/L 77.4 N21007770-1307878.5 1 25
4-Bromofluorobenzene (FID) (S)%95 70-130100
4-Bromofluorobenzene (PID) (S)%91 70-13096
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
379319
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92356169001, 92356169005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2102068
Associated Lab Samples:92356169001, 92356169005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 09/26/17 09:03
1,1,1-Trichloroethane ug/L ND 0.50 09/26/17 09:03
1,1,2,2-Tetrachloroethane ug/L ND 0.50 09/26/17 09:03
1,1,2-Trichloroethane ug/L ND 0.50 09/26/17 09:03
1,1-Dichloroethane ug/L ND 0.50 09/26/17 09:03
1,1-Dichloroethene ug/L ND 0.50 09/26/17 09:03
1,1-Dichloropropene ug/L ND 0.50 09/26/17 09:03
1,2,3-Trichlorobenzene ug/L ND 2.0 09/26/17 09:03
1,2,3-Trichloropropane ug/L ND 0.50 09/26/17 09:03
1,2,4-Trichlorobenzene ug/L ND 2.0 09/26/17 09:03
1,2,4-Trimethylbenzene ug/L ND 0.50 09/26/17 09:03
1,2-Dibromo-3-chloropropane ug/L ND 1.0 09/26/17 09:03
1,2-Dibromoethane (EDB)ug/L ND 0.50 09/26/17 09:03
1,2-Dichlorobenzene ug/L ND 0.50 09/26/17 09:03
1,2-Dichloroethane ug/L ND 0.50 09/26/17 09:03
1,2-Dichloropropane ug/L ND 0.50 09/26/17 09:03
1,3,5-Trimethylbenzene ug/L ND 0.50 09/26/17 09:03
1,3-Dichlorobenzene ug/L ND 0.50 09/26/17 09:03
1,3-Dichloropropane ug/L ND 0.50 09/26/17 09:03
1,4-Dichlorobenzene ug/L ND 0.50 09/26/17 09:03
2,2-Dichloropropane ug/L ND 0.50 09/26/17 09:03
2-Chlorotoluene ug/L ND 0.50 09/26/17 09:03
4-Chlorotoluene ug/L ND 0.50 09/26/17 09:03
Benzene ug/L ND 0.50 09/26/17 09:03
Bromobenzene ug/L ND 0.50 09/26/17 09:03
Bromochloromethane ug/L ND 0.50 09/26/17 09:03
Bromodichloromethane ug/L ND 0.50 09/26/17 09:03
Bromoform ug/L ND 0.50 09/26/17 09:03
Bromomethane ug/L ND 5.0 09/26/17 09:03
Carbon tetrachloride ug/L ND 0.50 09/26/17 09:03
Chlorobenzene ug/L ND 0.50 09/26/17 09:03
Chloroethane ug/L ND 1.0 09/26/17 09:03
Chloroform ug/L ND 0.50 09/26/17 09:03
Chloromethane ug/L ND 1.0 09/26/17 09:03
cis-1,2-Dichloroethene ug/L ND 0.50 09/26/17 09:03
cis-1,3-Dichloropropene ug/L ND 0.50 09/26/17 09:03
Dibromochloromethane ug/L ND 0.50 09/26/17 09:03
Dibromomethane ug/L ND 0.50 09/26/17 09:03
Dichlorodifluoromethane ug/L ND 0.50 09/26/17 09:03
Diisopropyl ether ug/L ND 0.50 09/26/17 09:03
Ethylbenzene ug/L ND 0.50 09/26/17 09:03
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2102068
Associated Lab Samples:92356169001, 92356169005
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 09/26/17 09:03
Isopropylbenzene (Cumene)ug/L ND 0.50 09/26/17 09:03
m&p-Xylene ug/L ND 1.0 09/26/17 09:03
Methyl-tert-butyl ether ug/L ND 0.50 09/26/17 09:03
Methylene Chloride ug/L ND 2.0 09/26/17 09:03
n-Butylbenzene ug/L ND 0.50 09/26/17 09:03
n-Propylbenzene ug/L ND 0.50 09/26/17 09:03
Naphthalene ug/L ND 2.0 09/26/17 09:03
o-Xylene ug/L ND 0.50 09/26/17 09:03
sec-Butylbenzene ug/L ND 0.50 09/26/17 09:03
Styrene ug/L ND 0.50 09/26/17 09:03
tert-Butylbenzene ug/L ND 0.50 09/26/17 09:03
Tetrachloroethene ug/L ND 0.50 09/26/17 09:03
Toluene ug/L ND 0.50 09/26/17 09:03
trans-1,2-Dichloroethene ug/L ND 0.50 09/26/17 09:03
trans-1,3-Dichloropropene ug/L ND 0.50 09/26/17 09:03
Trichloroethene ug/L ND 0.50 09/26/17 09:03
Trichlorofluoromethane ug/L ND 1.0 09/26/17 09:03
Vinyl chloride ug/L ND 1.0 09/26/17 09:03
1,2-Dichloroethane-d4 (S)%100 70-130 09/26/17 09:03
4-Bromofluorobenzene (S)%99 70-130 09/26/17 09:03
Toluene-d8 (S)%102 70-130 09/26/17 09:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2102069LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.950 104 60-140
1,1,1-Trichloroethane ug/L 56.950 114 60-140
1,1,2,2-Tetrachloroethane ug/L 47.250 94 60-140
1,1,2-Trichloroethane ug/L 49.550 99 60-140
1,1-Dichloroethane ug/L 51.950 104 60-140
1,1-Dichloroethene ug/L 58.750 117 60-140
1,1-Dichloropropene ug/L 55.950 112 60-140
1,2,3-Trichlorobenzene ug/L 51.050 102 60-140
1,2,3-Trichloropropane ug/L 48.650 97 60-140
1,2,4-Trichlorobenzene ug/L 53.150 106 60-140
1,2,4-Trimethylbenzene ug/L 54.650 109 60-140
1,2-Dibromo-3-chloropropane ug/L 49.750 99 60-140
1,2-Dibromoethane (EDB)ug/L 51.850 104 60-140
1,2-Dichlorobenzene ug/L 50.450 101 60-140
1,2-Dichloroethane ug/L 47.950 96 60-140
1,2-Dichloropropane ug/L 51.050 102 60-140
1,3,5-Trimethylbenzene ug/L 55.950 112 60-140
1,3-Dichlorobenzene ug/L 50.350 101 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2102069LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 51.150 102 60-140
1,4-Dichlorobenzene ug/L 49.350 99 60-140
2,2-Dichloropropane ug/L 58.550 117 60-140
2-Chlorotoluene ug/L 52.750 105 60-140
4-Chlorotoluene ug/L 52.850 106 60-140
Benzene ug/L 51.250 102 60-140
Bromobenzene ug/L 51.450 103 60-140
Bromochloromethane ug/L 49.950 100 60-140
Bromodichloromethane ug/L 52.550 105 60-140
Bromoform ug/L 47.950 96 60-140
Bromomethane ug/L 43.250 86 60-140
Carbon tetrachloride ug/L 58.350 117 60-140
Chlorobenzene ug/L 51.050 102 60-140
Chloroethane ug/L 50.150 100 60-140
Chloroform ug/L 48.450 97 60-140
Chloromethane ug/L 38.250 76 60-140
cis-1,2-Dichloroethene ug/L 54.450 109 60-140
cis-1,3-Dichloropropene ug/L 54.350 109 60-140
Dibromochloromethane ug/L 52.050 104 60-140
Dibromomethane ug/L 49.150 98 60-140
Dichlorodifluoromethane ug/L 45.850 92 60-140
Diisopropyl ether ug/L 50.350 101 60-140
Ethylbenzene ug/L 54.350 109 60-140
Hexachloro-1,3-butadiene ug/L 56.650 113 60-140
Isopropylbenzene (Cumene)ug/L 56.250 112 60-140
m&p-Xylene ug/L 110100 110 60-140
Methyl-tert-butyl ether ug/L 51.050 102 60-140
Methylene Chloride ug/L 43.550 87 60-140
n-Butylbenzene ug/L 57.050 114 60-140
n-Propylbenzene ug/L 54.450 109 60-140
Naphthalene ug/L 51.850 104 60-140
o-Xylene ug/L 53.750 107 60-140
sec-Butylbenzene ug/L 56.950 114 60-140
Styrene ug/L 53.250 106 60-140
tert-Butylbenzene ug/L 45.750 91 60-140
Tetrachloroethene ug/L 51.550 103 60-140
Toluene ug/L 50.850 102 60-140
trans-1,2-Dichloroethene ug/L 54.450 109 60-140
trans-1,3-Dichloropropene ug/L 52.350 105 60-140
Trichloroethene ug/L 52.150 104 60-140
Trichlorofluoromethane ug/L 51.650 103 60-140
Vinyl chloride ug/L 54.050 108 60-140
1,2-Dichloroethane-d4 (S)%101 70-130
4-Bromofluorobenzene (S)%104 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2102070MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92356169001
2102071
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 115 60-140113 220ND23.0 22.5
1,1,1-Trichloroethane ug/L 20 126 60-140134 620ND25.3 26.8
1,1,2,2-Tetrachloroethane ug/L 20 98 60-14097 120ND19.7 19.5
1,1,2-Trichloroethane ug/L 20 102 60-140107 520ND20.5 21.5
1,1-Dichloroethane ug/L 20 107 60-140113 620ND21.3 22.6
1,1-Dichloroethene ug/L 20 121 60-140130 820ND24.1 26.0
1,1-Dichloropropene ug/L 20 114 60-140122 720ND22.8 24.4
1,2,3-Trichlorobenzene ug/L 20 108 60-140108 020ND21.7 21.6
1,2,3-Trichloropropane ug/L 20 106 60-140111 520ND21.2 22.2
1,2,4-Trichlorobenzene ug/L 20 108 60-140112 420ND21.6 22.5
1,2,4-Trimethylbenzene ug/L 20 116 60-140112 3205.5 28.8 28.0
1,2-Dibromo-3-chloropropane ug/L 20 106 60-140109 320ND21.1 21.8
1,2-Dibromoethane (EDB)ug/L 20 112 60-140113 120ND22.3 22.6
1,2-Dichlorobenzene ug/L 20 104 60-140108 420ND20.8 21.6
1,2-Dichloroethane ug/L 20 108 60-140114 520ND21.6 22.8
1,2-Dichloropropane ug/L 20 102 60-140108 620ND20.3 21.6
1,3,5-Trimethylbenzene ug/L 20 113 60-140113 1201.5 24.2 24.1
1,3-Dichlorobenzene ug/L 20 103 60-140107 420ND20.5 21.3
1,3-Dichloropropane ug/L 20 102 60-140105 320ND20.5 21.1
1,4-Dichlorobenzene ug/L 20 105 60-140107 220ND20.9 21.3
2,2-Dichloropropane ug/L 20 123 60-140130 620ND24.5 26.0
2-Chlorotoluene ug/L 20 103 60-140102 120ND20.5 20.4
4-Chlorotoluene ug/L 20 107 60-140110 220ND21.5 22.0
Benzene ug/L 20 106 60-140111 420ND21.3 22.2
Bromobenzene ug/L 20 107 60-140110 320ND21.5 22.1
Bromochloromethane ug/L 20 101 60-140108 720ND20.2 21.7
Bromodichloromethane ug/L 20 114 60-140119 520ND22.7 23.8
Bromoform ug/L 20 112 60-140101 1020ND22.3 20.1
Bromomethane ug/L 20 71 60-14083 1520ND14.3 16.5
Carbon tetrachloride ug/L M12014060-140147 420ND28.1 29.3
Chlorobenzene ug/L 20 109 60-140109 120ND21.9 21.7
Chloroethane ug/L 20 96 60-140103 720ND19.2 20.7
Chloroform ug/L 20 105 60-140109 4200.94 21.9 22.7
Chloromethane ug/L 20 99 60-140111 1120ND19.9 22.2
cis-1,2-Dichloroethene ug/L 20 109 60-140116 620ND21.9 23.3
cis-1,3-Dichloropropene ug/L 20 106 60-140109 320ND21.2 21.9
Dibromochloromethane ug/L 20 115 60-140111 420ND23.0 22.2
Dibromomethane ug/L 20 107 60-140113 620ND21.4 22.7
Dichlorodifluoromethane ug/L 20 97 60-140105 820ND19.4 21.1
Diisopropyl ether ug/L 20 102 60-140109 620ND20.5 21.7
Ethylbenzene ug/L 20 114 60-140115 120ND23.2 23.4
Hexachloro-1,3-butadiene ug/L 20 114 60-140120 520ND22.7 24.0
Isopropylbenzene (Cumene)ug/L 20 115 60-140113 220ND23.4 23.0
m&p-Xylene ug/L 40 117 60-140115 2401.1 47.7 46.9
Methyl-tert-butyl ether ug/L 20 99 60-140104 520ND20.2 21.2
Methylene Chloride ug/L 20 95 60-140100 420ND19.1 20.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2102070MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92356169001
2102071
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 112 60-140114 220ND22.4 22.9
n-Propylbenzene ug/L 20 106 60-140108 1200.93 22.2 22.5
Naphthalene ug/L 20 109 60-140110 120ND23.8 24.0
o-Xylene ug/L 20 114 60-140114 020ND22.8 22.9
sec-Butylbenzene ug/L 20 113 60-140114 120ND22.6 22.8
Styrene ug/L 20 111 60-140111 020ND22.1 22.2
tert-Butylbenzene ug/L 20 87 60-14093 720ND17.5 18.7
Tetrachloroethene ug/L 20 114 60-140111 220ND22.8 22.3
Toluene ug/L 20 109 60-140113 320ND21.9 22.6
trans-1,2-Dichloroethene ug/L 20 108 60-140115 620ND21.6 22.9
trans-1,3-Dichloropropene ug/L 20 108 60-140114 620ND21.6 22.9
Trichloroethene ug/L 20 115 60-140121 520ND22.9 24.2
Trichlorofluoromethane ug/L 20 128 60-140136 620ND25.7 27.2
Vinyl chloride ug/L 20 99 60-140108 820ND19.8 21.5
1,2-Dichloroethane-d4 (S)%108 70-130110
4-Bromofluorobenzene (S)%105 70-130102
Toluene-d8 (S)%98 70-13098
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
379454
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92356169002, 92356169003, 92356169004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2102958
Associated Lab Samples:92356169002, 92356169003, 92356169004
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 09/26/17 18:12
1,1,1-Trichloroethane ug/L ND 0.50 09/26/17 18:12
1,1,2,2-Tetrachloroethane ug/L ND 0.50 09/26/17 18:12
1,1,2-Trichloroethane ug/L ND 0.50 09/26/17 18:12
1,1-Dichloroethane ug/L ND 0.50 09/26/17 18:12
1,1-Dichloroethene ug/L ND 0.50 09/26/17 18:12
1,1-Dichloropropene ug/L ND 0.50 09/26/17 18:12
1,2,3-Trichlorobenzene ug/L ND 2.0 09/26/17 18:12
1,2,3-Trichloropropane ug/L ND 0.50 09/26/17 18:12
1,2,4-Trichlorobenzene ug/L ND 2.0 09/26/17 18:12
1,2,4-Trimethylbenzene ug/L ND 0.50 09/26/17 18:12
1,2-Dibromo-3-chloropropane ug/L ND 1.0 09/26/17 18:12
1,2-Dibromoethane (EDB)ug/L ND 0.50 09/26/17 18:12
1,2-Dichlorobenzene ug/L ND 0.50 09/26/17 18:12
1,2-Dichloroethane ug/L ND 0.50 09/26/17 18:12
1,2-Dichloropropane ug/L ND 0.50 09/26/17 18:12
1,3,5-Trimethylbenzene ug/L ND 0.50 09/26/17 18:12
1,3-Dichlorobenzene ug/L ND 0.50 09/26/17 18:12
1,3-Dichloropropane ug/L ND 0.50 09/26/17 18:12
1,4-Dichlorobenzene ug/L ND 0.50 09/26/17 18:12
2,2-Dichloropropane ug/L ND 0.50 09/26/17 18:12
2-Chlorotoluene ug/L ND 0.50 09/26/17 18:12
4-Chlorotoluene ug/L ND 0.50 09/26/17 18:12
Benzene ug/L ND 0.50 09/26/17 18:12
Bromobenzene ug/L ND 0.50 09/26/17 18:12
Bromochloromethane ug/L ND 0.50 09/26/17 18:12
Bromodichloromethane ug/L ND 0.50 09/26/17 18:12
Bromoform ug/L ND 0.50 09/26/17 18:12
Bromomethane ug/L ND 5.0 09/26/17 18:12
Carbon tetrachloride ug/L ND 0.50 09/26/17 18:12
Chlorobenzene ug/L ND 0.50 09/26/17 18:12
Chloroethane ug/L ND 1.0 09/26/17 18:12
Chloroform ug/L ND 0.50 09/26/17 18:12
Chloromethane ug/L ND 1.0 09/26/17 18:12
cis-1,2-Dichloroethene ug/L ND 0.50 09/26/17 18:12
cis-1,3-Dichloropropene ug/L ND 0.50 09/26/17 18:12
Dibromochloromethane ug/L ND 0.50 09/26/17 18:12
Dibromomethane ug/L ND 0.50 09/26/17 18:12
Dichlorodifluoromethane ug/L ND 0.50 09/26/17 18:12
Diisopropyl ether ug/L ND 0.50 09/26/17 18:12
Ethylbenzene ug/L ND 0.50 09/26/17 18:12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2102958
Associated Lab Samples:92356169002, 92356169003, 92356169004
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 09/26/17 18:12
Isopropylbenzene (Cumene)ug/L ND 0.50 09/26/17 18:12
m&p-Xylene ug/L ND 1.0 09/26/17 18:12
Methyl-tert-butyl ether ug/L ND 0.50 09/26/17 18:12
Methylene Chloride ug/L ND 2.0 09/26/17 18:12
n-Butylbenzene ug/L ND 0.50 09/26/17 18:12
n-Propylbenzene ug/L ND 0.50 09/26/17 18:12
Naphthalene ug/L ND 2.0 09/26/17 18:12
o-Xylene ug/L ND 0.50 09/26/17 18:12
sec-Butylbenzene ug/L ND 0.50 09/26/17 18:12
Styrene ug/L ND 0.50 09/26/17 18:12
tert-Butylbenzene ug/L ND 0.50 09/26/17 18:12
Tetrachloroethene ug/L ND 0.50 09/26/17 18:12
Toluene ug/L ND 0.50 09/26/17 18:12
trans-1,2-Dichloroethene ug/L ND 0.50 09/26/17 18:12
trans-1,3-Dichloropropene ug/L ND 0.50 09/26/17 18:12
Trichloroethene ug/L ND 0.50 09/26/17 18:12
Trichlorofluoromethane ug/L ND 1.0 09/26/17 18:12
Vinyl chloride ug/L ND 1.0 09/26/17 18:12
1,2-Dichloroethane-d4 (S)%110 70-130 09/26/17 18:12
4-Bromofluorobenzene (S)%101 70-130 09/26/17 18:12
Toluene-d8 (S)%100 70-130 09/26/17 18:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2102959LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 55.150 110 60-140
1,1,1-Trichloroethane ug/L 60.750 121 60-140
1,1,2,2-Tetrachloroethane ug/L 48.050 96 60-140
1,1,2-Trichloroethane ug/L 53.550 107 60-140
1,1-Dichloroethane ug/L 51.250 102 60-140
1,1-Dichloroethene ug/L 60.750 121 60-140
1,1-Dichloropropene ug/L 55.150 110 60-140
1,2,3-Trichlorobenzene ug/L 53.550 107 60-140
1,2,3-Trichloropropane ug/L 54.350 109 60-140
1,2,4-Trichlorobenzene ug/L 54.450 109 60-140
1,2,4-Trimethylbenzene ug/L 55.250 110 60-140
1,2-Dibromo-3-chloropropane ug/L 53.350 107 60-140
1,2-Dibromoethane (EDB)ug/L 54.850 110 60-140
1,2-Dichlorobenzene ug/L 52.350 105 60-140
1,2-Dichloroethane ug/L 54.350 109 60-140
1,2-Dichloropropane ug/L 50.450 101 60-140
1,3,5-Trimethylbenzene ug/L 55.550 111 60-140
1,3-Dichlorobenzene ug/L 52.450 105 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2102959LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 52.250 104 60-140
1,4-Dichlorobenzene ug/L 51.950 104 60-140
2,2-Dichloropropane ug/L 58.850 118 60-140
2-Chlorotoluene ug/L 52.350 105 60-140
4-Chlorotoluene ug/L 53.450 107 60-140
Benzene ug/L 51.150 102 60-140
Bromobenzene ug/L 51.650 103 60-140
Bromochloromethane ug/L 51.250 102 60-140
Bromodichloromethane ug/L 57.150 114 60-140
Bromoform ug/L 53.750 107 60-140
Bromomethane ug/L 42.150 84 60-140
Carbon tetrachloride ug/L 65.950 132 60-140
Chlorobenzene ug/L 52.550 105 60-140
Chloroethane ug/L 47.550 95 60-140
Chloroform ug/L 49.550 99 60-140
Chloromethane ug/L 46.750 93 60-140
cis-1,2-Dichloroethene ug/L 54.850 110 60-140
cis-1,3-Dichloropropene ug/L 56.550 113 60-140
Dibromochloromethane ug/L 56.350 113 60-140
Dibromomethane ug/L 55.750 111 60-140
Dichlorodifluoromethane ug/L 47.450 95 60-140
Diisopropyl ether ug/L 52.550 105 60-140
Ethylbenzene ug/L 54.950 110 60-140
Hexachloro-1,3-butadiene ug/L 57.550 115 60-140
Isopropylbenzene (Cumene)ug/L 57.450 115 60-140
m&p-Xylene ug/L 113100 113 60-140
Methyl-tert-butyl ether ug/L 52.450 105 60-140
Methylene Chloride ug/L 45.750 91 60-140
n-Butylbenzene ug/L 55.150 110 60-140
n-Propylbenzene ug/L 52.950 106 60-140
Naphthalene ug/L 54.150 108 60-140
o-Xylene ug/L 55.450 111 60-140
sec-Butylbenzene ug/L 55.450 111 60-140
Styrene ug/L 55.350 111 60-140
tert-Butylbenzene ug/L 45.550 91 60-140
Tetrachloroethene ug/L 54.150 108 60-140
Toluene ug/L 53.050 106 60-140
trans-1,2-Dichloroethene ug/L 53.850 108 60-140
trans-1,3-Dichloropropene ug/L 57.950 116 60-140
Trichloroethene ug/L 55.550 111 60-140
Trichlorofluoromethane ug/L 55.950 112 60-140
Vinyl chloride ug/L 52.750 105 60-140
1,2-Dichloroethane-d4 (S)%109 70-130
4-Bromofluorobenzene (S)%107 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2102960MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92356202003
2102961
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 200 112 60-140119 6200ND224237
1,1,1-Trichloroethane ug/L 200 129 60-140139 7200ND258277
1,1,2,2-Tetrachloroethane ug/L 200 95 60-140104 9200ND191209
1,1,2-Trichloroethane ug/L 200 107 60-140112 4200ND214223
1,1-Dichloroethane ug/L 200 110 60-140119 8200ND220237
1,1-Dichloroethene ug/L M120012860-140141 9200ND256281
1,1-Dichloropropene ug/L 200 116 60-140125 7200ND231249
1,2,3-Trichlorobenzene ug/L 200 107 60-140114 7200ND213228
1,2,3-Trichloropropane ug/L 200 109 60-140122 12200ND218244
1,2,4-Trichlorobenzene ug/L 200 112 60-140118 5200ND223235
1,2,4-Trimethylbenzene ug/L M12005360-14078 4200111012201270
1,2-Dibromo-3-chloropropane ug/L 200 104 60-140115 11200ND208231
1,2-Dibromoethane (EDB)ug/L 200 105 60-140116 10200ND210232
1,2-Dichlorobenzene ug/L 200 106 60-140111 4200ND213222
1,2-Dichloroethane ug/L 200 109 60-140119 8200ND218237
1,2-Dichloropropane ug/L 200 106 60-140113 6200ND213226
1,3,5-Trimethylbenzene ug/L 200 97 60-140112 5200395588619
1,3-Dichlorobenzene ug/L 200 106 60-140110 4200ND211219
1,3-Dichloropropane ug/L 200 102 60-140110 8200ND204221
1,4-Dichlorobenzene ug/L 200 100 60-140109 8200ND200218
2,2-Dichloropropane ug/L 200 114 60-140120 5200ND228240
2-Chlorotoluene ug/L 200 85 60-14085 0200ND170170
4-Chlorotoluene ug/L 200 106 60-140113 7200ND212227
Benzene ug/L 200 106 60-140112 52007.4 220 232
Bromobenzene ug/L 200 104 60-140114 9200ND207227
Bromochloromethane ug/L 200 102 60-140113 10200ND203225
Bromodichloromethane ug/L 200 116 60-140117 0200ND232233
Bromoform ug/L 200 89 60-14093 4200ND179186
Bromomethane ug/L M12005260-14064 21200ND104128
Carbon tetrachloride ug/L M120014160-140145 3200ND281291
Chlorobenzene ug/L 200 107 60-140115 8200ND213231
Chloroethane ug/L 200 103 60-140111 8200ND205223
Chloroform ug/L 200 103 60-140110 6200ND206220
Chloromethane ug/L 200 79 60-14092 15200ND159184
cis-1,2-Dichloroethene ug/L 200 115 60-140122 6200ND231245
cis-1,3-Dichloropropene ug/L 200 101 60-140111 9200ND203223
Dibromochloromethane ug/L 200 105 60-140107 2200ND209213
Dibromomethane ug/L 200 113 60-140116 3200ND225233
Dichlorodifluoromethane ug/L 200 102 60-140114 11200ND204228
Diisopropyl ether ug/L 200 106 60-140115 8200ND213231
Ethylbenzene ug/L 200 101 60-140114 6200250452479
Hexachloro-1,3-butadiene ug/L 200 118 60-140132 11200ND237263
Isopropylbenzene (Cumene)ug/L 200 115 60-140123 520093.9 324 340
m&p-Xylene ug/L 400 103 60-140119 7400495909970
Methyl-tert-butyl ether ug/L 200 98 60-140113 1320024.8 221 250
Methylene Chloride ug/L 200 98 60-140106 8200ND196213
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
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Page 32 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2102960MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92356202003
2102961
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L M120013360-140145 9200ND266289
n-Propylbenzene ug/L M12009460-140106 6200220408433
Naphthalene ug/L 200 106 60-140115 5200132343361
o-Xylene ug/L 200 113 60-140123 720068.9 295 315
sec-Butylbenzene ug/L 200 121 60-140132 9200ND241265
Styrene ug/L 200 110 60-140117 6200ND219233
tert-Butylbenzene ug/L 200 95 60-140102 7200ND189204
Tetrachloroethene ug/L 200 113 60-140122 7200ND226243
Toluene ug/L 200 106 60-140114 72005.8 219 234
trans-1,2-Dichloroethene ug/L 200 114 60-140120 5200ND228241
trans-1,3-Dichloropropene ug/L 200 108 60-140106 2200ND217213
Trichloroethene ug/L 200 118 60-140122 3200ND237244
Trichlorofluoromethane ug/L 200 122 60-140132 8200ND244265
Vinyl chloride ug/L 200 106 60-140124 15200ND212248
1,2-Dichloroethane-d4 (S)%106 70-130108
4-Bromofluorobenzene (S)%104 70-130105
Toluene-d8 (S)%99 70-13098
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
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Page 33 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
378722
EPA 625
EPA 625
625 MSS
Associated Lab Samples:92356169001, 92356169002, 92356169003, 92356169004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2098563
Associated Lab Samples:92356169001, 92356169002, 92356169003, 92356169004
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 09/22/17 18:47
2,4,6-Trichlorophenol ug/L ND 10.0 09/22/17 18:47
2,4-Dichlorophenol ug/L ND 5.0 09/22/17 18:47
2,4-Dimethylphenol ug/L ND 10.0 09/22/17 18:47
2,4-Dinitrophenol ug/L ND 50.0 09/22/17 18:47
2,4-Dinitrotoluene ug/L ND 5.0 09/22/17 18:47
2,6-Dinitrotoluene ug/L ND 5.0 09/22/17 18:47
2-Chloronaphthalene ug/L ND 5.0 09/22/17 18:47
2-Chlorophenol ug/L ND 5.0 09/22/17 18:47
2-Nitrophenol ug/L ND 5.0 09/22/17 18:47
3,3'-Dichlorobenzidine ug/L ND 25.0 09/22/17 18:47
4,6-Dinitro-2-methylphenol ug/L ND 20.0 09/22/17 18:47
4-Bromophenylphenyl ether ug/L ND 5.0 09/22/17 18:47
4-Chloro-3-methylphenol ug/L ND 5.0 09/22/17 18:47
4-Chlorophenylphenyl ether ug/L ND 5.0 09/22/17 18:47
4-Nitrophenol ug/L ND 50.0 09/22/17 18:47
Acenaphthene ug/L ND 5.0 09/22/17 18:47
Acenaphthylene ug/L ND 5.0 09/22/17 18:47
Anthracene ug/L ND 5.0 09/22/17 18:47
Benzo(a)anthracene ug/L ND 5.0 09/22/17 18:47
Benzo(a)pyrene ug/L ND 5.0 09/22/17 18:47
Benzo(b)fluoranthene ug/L ND 5.0 09/22/17 18:47
Benzo(g,h,i)perylene ug/L ND 5.0 09/22/17 18:47
Benzo(k)fluoranthene ug/L ND 5.0 09/22/17 18:47
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/22/17 18:47
bis(2-Chloroethyl) ether ug/L ND 5.0 09/22/17 18:47
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 09/22/17 18:47
Butylbenzylphthalate ug/L ND 5.0 09/22/17 18:47
Chrysene ug/L ND 5.0 09/22/17 18:47
Di-n-butylphthalate ug/L ND 5.0 09/22/17 18:47
Di-n-octylphthalate ug/L ND 5.0 09/22/17 18:47
Dibenz(a,h)anthracene ug/L ND 5.0 09/22/17 18:47
Diethylphthalate ug/L ND 5.0 09/22/17 18:47
Dimethylphthalate ug/L ND 5.0 09/22/17 18:47
Fluoranthene ug/L ND 5.0 09/22/17 18:47
Fluorene ug/L ND 5.0 09/22/17 18:47
Hexachloro-1,3-butadiene ug/L ND 5.0 09/22/17 18:47
Hexachlorobenzene ug/L ND 5.0 09/22/17 18:47
Hexachlorocyclopentadiene ug/L ND 10.0 09/22/17 18:47
Hexachloroethane ug/L ND 5.0 09/22/17 18:47
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 09/22/17 18:47
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
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Huntersville, NC 28078
[phone]
Page 34 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2098563
Associated Lab Samples:92356169001, 92356169002, 92356169003, 92356169004
Matrix:Water
Analyzed
Isophorone ug/L ND 10.0 09/22/17 18:47
N-Nitroso-di-n-propylamine ug/L ND 5.0 09/22/17 18:47
N-Nitrosodimethylamine ug/L ND 5.0 09/22/17 18:47
N-Nitrosodiphenylamine ug/L ND 10.0 09/22/17 18:47
Naphthalene ug/L ND 5.0 09/22/17 18:47
Nitrobenzene ug/L ND 5.0 09/22/17 18:47
Pentachlorophenol ug/L ND 10.0 09/22/17 18:47
Phenanthrene ug/L ND 5.0 09/22/17 18:47
Phenol ug/L ND 5.0 09/22/17 18:47
Pyrene ug/L ND 5.0 09/22/17 18:47
2,4,6-Tribromophenol (S)%88 10-137 09/22/17 18:47
2-Fluorobiphenyl (S)%67 15-120 09/22/17 18:47
2-Fluorophenol (S)%35 10-120 09/22/17 18:47
Nitrobenzene-d5 (S)%73 10-120 09/22/17 18:47
Phenol-d6 (S)%22 10-120 09/22/17 18:47
Terphenyl-d14 (S)%86 11-131 09/22/17 18:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2098564LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2098565
1,2,4-Trichlorobenzene ug/L 34.450 69 44-1427336.7 6 30
2,4,6-Trichlorophenol ug/L 47.050 94 37-14410251.1 8 30
2,4-Dichlorophenol ug/L 38.450 77 1-1918441.8 8 30
2,4-Dimethylphenol ug/L 38.650 77 32-1198040.2 4 30
2,4-Dinitrophenol ug/L 254250 102 1-181116291 14 30
2,4-Dinitrotoluene ug/L 48.250 96 39-13910250.8 5 30
2,6-Dinitrotoluene ug/L 45.950 92 50-1589648.1 5 30
2-Chloronaphthalene ug/L 41.050 82 60-1188843.8 7 30
2-Chlorophenol ug/L 34.750 69 23-1346934.3 1 30
2-Nitrophenol ug/L 42.050 84 29-1828843.8 4 30
3,3'-Dichlorobenzidine ug/L 72.8100 73 1-2628382.5 13 30
4,6-Dinitro-2-methylphenol ug/L 109100 109 1-181124124 13 30
4-Bromophenylphenyl ether ug/L 43.750 87 53-1279949.3 12 30
4-Chloro-3-methylphenol ug/L 83.1100 83 22-1478988.9 7 30
4-Chlorophenylphenyl ether ug/L 42.750 85 25-1589246.1 8 30
4-Nitrophenol ug/L 125250 50 1-13245113 10 30
Acenaphthene ug/L 41.350 83 47-1458843.8 6 30
Acenaphthylene ug/L 40.750 81 33-1458643.1 6 30
Anthracene ug/L 40.250 80 1-1668542.5 6 30
Benzo(a)anthracene ug/L 44.250 88 33-1439547.4 7 30
Benzo(a)pyrene ug/L 44.250 88 17-1639246.2 4 30
Benzo(b)fluoranthene ug/L 43.550 87 24-1599145.7 5 30
Benzo(g,h,i)perylene ug/L 42.550 85 1-2199346.5 9 30
Benzo(k)fluoranthene ug/L 45.650 91 11-1629547.6 4 30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2098564LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2098565
bis(2-Chloroethoxy)methane ug/L 40.850 82 33-1848542.7 5 30
bis(2-Chloroethyl) ether ug/L 36.550 73 12-1587537.4 3 30
bis(2-Ethylhexyl)phthalate ug/L 47.150 94 8-1589849.0 4 30
Butylbenzylphthalate ug/L 48.250 96 1-1529748.4 0 30
Chrysene ug/L 43.150 86 17-1689246.0 7 30
Di-n-butylphthalate ug/L 47.850 96 1-1189949.7 4 30
Di-n-octylphthalate ug/L 45.050 90 4-1469447.0 4 30
Dibenz(a,h)anthracene ug/L 43.350 87 1-2279446.9 8 30
Diethylphthalate ug/L 46.950 94 1-11410049.8 6 30
Dimethylphthalate ug/L 45.850 92 1-1129849.1 7 30
Fluoranthene ug/L 45.350 91 26-1379547.4 5 30
Fluorene ug/L 42.650 85 59-1219246.1 8 30
Hexachloro-1,3-butadiene ug/L 33.050 66 24-1167135.6 7 30
Hexachlorobenzene ug/L 41.650 83 1-1528844.2 6 30
Hexachlorocyclopentadiene ug/L 35.650 71 25-1507738.6 8 30
Hexachloroethane ug/L 24.850 50 40-1135427.0 9 30
Indeno(1,2,3-cd)pyrene ug/L 43.250 86 1-1719346.7 8 30
Isophorone ug/L 45.050 90 21-1969647.8 6 30
N-Nitroso-di-n-propylamine ug/L 39.950 80 1-2308643.1 8 30
N-Nitrosodimethylamine ug/L 26.450 53 25-1505125.4 4 30
N-Nitrosodiphenylamine ug/L 38.850 78 25-1508743.3 11 30
Naphthalene ug/L 34.350 69 21-1337336.3 6 30
Nitrobenzene ug/L 41.650 83 35-1808643.2 4 30
Pentachlorophenol ug/L 102100 102 14-176110110 8 30
Phenanthrene ug/L 40.250 80 54-1208642.9 7 30
Phenol ug/L 20.250 40 5-1123718.5 9 30
Pyrene ug/L 41.850 84 52-1158843.9 5 30
2,4,6-Tribromophenol (S)%97 10-137106
2-Fluorobiphenyl (S)%82 15-12087
2-Fluorophenol (S)%45 10-12041
Nitrobenzene-d5 (S)%85 10-12088
Phenol-d6 (S)%32 10-12028
Terphenyl-d14 (S)%85 11-13188
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 42
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
379198
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Associated Lab Samples:92356169001, 92356169002, 92356169003, 92356169004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2101354
Associated Lab Samples:92356169001, 92356169002, 92356169003, 92356169004
Matrix:Water
Analyzed
Aliphatic (C09-C18)ug/L ND 100 N209/25/17 23:30
Aliphatic (C19-C36)ug/L ND 100 N209/25/17 23:30
Aromatic (C11-C22)ug/L ND 100 N209/25/17 23:30
2-Bromonaphthalene (S)%95 40-140 09/25/17 23:30
2-Fluorobiphenyl (S)%110 40-140 09/25/17 23:30
Nonatriacontane (S)%68 40-140 09/25/17 23:30
o-Terphenyl (S)%78 40-140 09/25/17 23:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2101355LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2101356
Aliphatic (C09-C18)ug/L 164 N23005540-14074221 29 50
Aliphatic (C19-C36)ug/L 248 N24006240-14083330 28 50
Aromatic (C11-C22)ug/L 620 N28507340-14077657 6 50
2-Bromonaphthalene (S)%77 40-14067
2-Fluorobiphenyl (S)%95 40-14093
Nonatriacontane (S)%60 40-14082
o-Terphenyl (S)%75 40-14081
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 42
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92356169
BOULEVARD 495108
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The reported TIC has an 85% or higher match on a mass spectral library search.N
The lab does not hold NELAC/TNI accreditation for this parameter.N2
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 42
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92356169
BOULEVARD 495108
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92356169001 379198 379276MW-2 MADEP EPH MADEP EPH
92356169002 379198 379276MW-3 MADEP EPH MADEP EPH
92356169003 379198 379276MW-4 MADEP EPH MADEP EPH
92356169004 379198 379276MW-1 MADEP EPH MADEP EPH
92356169001 379189MW-2 MADEP VPH
92356169002 379189MW-3 MADEP VPH
92356169003 379189MW-4 MADEP VPH
92356169004 379189MW-1 MADEP VPH
92356169001 378722 378968MW-2 EPA 625 EPA 625
92356169002 378722 378968MW-3 EPA 625 EPA 625
92356169003 378722 378968MW-4 EPA 625 EPA 625
92356169004 378722 378968MW-1 EPA 625 EPA 625
92356169001 379319MW-2 SM 6200B
92356169002 379454MW-3 SM 6200B
92356169003 379454MW-4 SM 6200B
92356169004 379454MW-1 SM 6200B
92356169005 379319FIELD BLANK SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/27/2017 04:00 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 42
Page 40 of 42
Page 41 of 42
Page 42 of 42
#=CL#
November 01, 2017
LIMS USE: FR - MATTHEW GILLIS
LIMS OBJECT ID: 92355949
92355949
Project:
Pace Project No.:
RE:
Matthew Gillis
ECS
9001 Glenwood Avenue
Raleigh, NC 27617
Blvd B.P.
Dear Matthew Gillis:
Enclosed are the analytical results for sample(s) received by the laboratory on September 19, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Report revised 11/1/17 to change units at client request.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
cc:Sarah Kordon, ECS Southeast
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 165
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92355949
Blvd B.P.
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
Page 2 of 165
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92355949
Blvd B.P.
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92355949001 SB-1A MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949002 SB-1B MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949003 SB-1C MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949004 SB-2A MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949005 SB-2B MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949006 SB-2C MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949007 SB-3A MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949008 SB-3B MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 165
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92355949
Blvd B.P.
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949009 SB-3C MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949010 SB-4A MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949011 SB-4B MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949012 SB-4C MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949013 SB-5A MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949014 SB-5B MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949015 SB-5C MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 165
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92355949
Blvd B.P.
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
ASTM D2974-87 1 PASI-CKDF
92355949016 SB-6A MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949017 SB-6B MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949018 SB-6C MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949019 SB-7A MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949020 SB-7B MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949021 SB-7C MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949022 SB-8A MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949023 SB-8B MADEP EPH 7 PASI-CNU1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 165
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92355949
Blvd B.P.
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
92355949024 SB-8C MADEP EPH 7 PASI-CNU1
MADEP VPH 5 PASI-CWDV
EPA 8270 74 PASI-CBPJ
EPA 8260 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 165
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92355949
Blvd B.P.
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92355949001 SB-1A
Percent Moisture 23.6 %09/21/17 11:080.10ASTM D2974-87
92355949002 SB-1B
Aliphatic (C05-C08)184 mg/kg 09/21/17 16:06 N23.8MADEP VPH
Aliphatic (C09-C12)101 mg/kg 09/21/17 16:06 N23.8MADEP VPH
Aromatic (C09-C10)254 mg/kg 09/21/17 16:06 N23.8MADEP VPH
1-Methylnaphthalene 0.52 mg/kg 09/21/17 16:120.46EPA 8270
2-Methylnaphthalene 1.1 mg/kg 09/21/17 16:120.46EPA 8270
Naphthalene 0.87 mg/kg 09/21/17 16:120.46EPA 8270
Naphthalene 0.29 mg/kg 09/21/17 19:560.16EPA 8260
n-Propylbenzene 0.22 mg/kg 09/21/17 19:560.16EPA 8260
1,2,4-Trimethylbenzene 1.1 mg/kg 09/21/17 19:560.16EPA 8260
1,3,5-Trimethylbenzene 0.41 mg/kg 09/21/17 19:560.16EPA 8260
Xylene (Total)0.47 mg/kg 09/21/17 19:560.32EPA 8260
m&p-Xylene 0.47 mg/kg 09/21/17 19:560.32EPA 8260
Percent Moisture 28.3 %09/21/17 11:090.10ASTM D2974-87
92355949003 SB-1C
Aromatic (C09-C10)4.4 mg/kg 09/21/17 16:34 N23.2MADEP VPH
Ethylbenzene 0.014 mg/kg 09/21/17 20:160.0055EPA 8260
Naphthalene 0.087 mg/kg 09/21/17 20:160.0055EPA 8260
1,2,4-Trimethylbenzene 0.13 mg/kg 09/21/17 20:160.0055EPA 8260
1,3,5-Trimethylbenzene 0.032 mg/kg 09/21/17 20:160.0055EPA 8260
Xylene (Total)0.17 mg/kg 09/21/17 20:160.011EPA 8260
m&p-Xylene 0.16 mg/kg 09/21/17 20:160.011EPA 8260
o-Xylene 0.011 mg/kg 09/21/17 20:160.0055EPA 8260
Percent Moisture 16.5 %09/21/17 11:090.10ASTM D2974-87
92355949004 SB-2A
Percent Moisture 25.2 %09/21/17 11:090.10ASTM D2974-87
92355949005 SB-2B
Methyl-tert-butyl ether 0.0066 mg/kg 09/21/17 20:560.0050EPA 8260
1,2,4-Trimethylbenzene 0.015 mg/kg 09/21/17 20:560.0050EPA 8260
Percent Moisture 27.7 %09/21/17 11:090.10ASTM D2974-87
92355949006 SB-2C
Methyl-tert-butyl ether 0.026 mg/kg 09/21/17 21:150.0042EPA 8260
Naphthalene 0.0056 mg/kg 09/21/17 21:150.0042EPA 8260
1,2,4-Trimethylbenzene 0.013 mg/kg 09/21/17 21:150.0042EPA 8260
Percent Moisture 21.0 %09/21/17 11:090.10ASTM D2974-87
92355949007 SB-3A
Aliphatic (C05-C08)612 mg/kg 09/26/17 12:12 N215.0MADEP VPH
Aliphatic (C09-C12)117 mg/kg 09/26/17 12:12 N215.0MADEP VPH
Aromatic (C09-C10)485 mg/kg 09/26/17 12:12 N215.0MADEP VPH
n-Butylbenzene 6.5 mg/kg 09/21/17 21:350.33EPA 8260
sec-Butylbenzene 2.2 mg/kg 09/21/17 21:350.33EPA 8260
Ethylbenzene 2.1 mg/kg 09/21/17 21:350.33EPA 8260
Isopropylbenzene (Cumene)2.8 mg/kg 09/21/17 21:350.33EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 165
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92355949
Blvd B.P.
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92355949007 SB-3A
p-Isopropyltoluene 3.8 mg/kg 09/21/17 21:350.33EPA 8260
Naphthalene 5.4 mg/kg 09/21/17 21:350.33EPA 8260
n-Propylbenzene 12.6 mg/kg 09/21/17 21:350.33EPA 8260
1,2,4-Trimethylbenzene 51.6 mg/kg 09/22/17 14:253.3EPA 8260
1,3,5-Trimethylbenzene 17.2 mg/kg 09/22/17 14:253.3EPA 8260
Xylene (Total)6.9 mg/kg 09/21/17 21:350.66EPA 8260
m&p-Xylene 5.9 mg/kg 09/21/17 21:350.66EPA 8260
o-Xylene 0.94 mg/kg 09/21/17 21:350.33EPA 8260
Percent Moisture 24.4 %09/21/17 11:110.10ASTM D2974-87
92355949008 SB-3B
Aliphatic (C05-C08)110 mg/kg 09/21/17 18:54 N23.5MADEP VPH
Aliphatic (C09-C12)27.9 mg/kg 09/21/17 18:54 N23.5MADEP VPH
Aromatic (C09-C10)109 mg/kg 09/21/17 18:54 N23.5MADEP VPH
n-Butylbenzene 6.9 mg/kg 09/21/17 21:550.32EPA 8260
sec-Butylbenzene 2.3 mg/kg 09/21/17 21:550.32EPA 8260
Ethylbenzene 2.2 mg/kg 09/21/17 21:550.32EPA 8260
Isopropylbenzene (Cumene)2.9 mg/kg 09/21/17 21:550.32EPA 8260
p-Isopropyltoluene 3.9 mg/kg 09/21/17 21:550.32EPA 8260
Naphthalene 5.6 mg/kg 09/21/17 21:550.32EPA 8260
n-Propylbenzene 12.3 mg/kg 09/22/17 14:453.2EPA 8260
1,2,4-Trimethylbenzene 56.8 mg/kg 09/22/17 14:453.2EPA 8260
1,3,5-Trimethylbenzene 18.9 mg/kg 09/22/17 14:453.2EPA 8260
Xylene (Total)7.5 mg/kg 09/21/17 21:550.63EPA 8260
m&p-Xylene 6.5 mg/kg 09/21/17 21:550.63EPA 8260
o-Xylene 1.0 mg/kg 09/21/17 21:550.32EPA 8260
Percent Moisture 21.1 %09/21/17 11:110.10ASTM D2974-87
92355949009 SB-3C
Aliphatic (C05-C08)303 mg/kg 09/26/17 11:44 N25.1MADEP VPH
Aliphatic (C09-C12)68.3 mg/kg 09/26/17 11:44 N25.1MADEP VPH
Aromatic (C09-C10)255 mg/kg 09/26/17 11:44 N25.1MADEP VPH
2-Methylnaphthalene 0.52 mg/kg 09/21/17 18:380.42EPA 8270
n-Butylbenzene 1.6 mg/kg 09/21/17 14:430.14EPA 8260
sec-Butylbenzene 0.45 mg/kg 09/21/17 14:430.14EPA 8260
Ethylbenzene 0.62 mg/kg 09/21/17 14:430.14EPA 8260
Isopropylbenzene (Cumene)0.62 mg/kg 09/21/17 14:430.14EPA 8260
p-Isopropyltoluene 0.96 mg/kg 09/21/17 14:430.14EPA 8260
Naphthalene 2.1 mg/kg 09/21/17 14:430.14EPA 8260
n-Propylbenzene 2.7 mg/kg 09/21/17 14:430.14EPA 8260
1,2,4-Trimethylbenzene 14.0 mg/kg 09/22/17 13:071.1EPA 8260
1,3,5-Trimethylbenzene 4.4 mg/kg 09/21/17 14:430.14EPA 8260
Xylene (Total)1.9 mg/kg 09/21/17 14:430.29EPA 8260
m&p-Xylene 1.8 mg/kg 09/21/17 14:430.29EPA 8260
o-Xylene 0.17 mg/kg 09/21/17 14:430.14EPA 8260
Percent Moisture 21.7 %09/21/17 11:110.10ASTM D2974-87
92355949010 SB-4A
Percent Moisture 12.4 %09/21/17 11:110.10ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 165
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92355949
Blvd B.P.
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92355949011 SB-4B
Aliphatic (C19-C36)16.7 mg/kg 09/21/17 19:48 N213.0MADEP EPH
Aliphatic (C05-C08)60.0 mg/kg 09/21/17 20:17 N23.6MADEP VPH
Aliphatic (C09-C12)12.4 mg/kg 09/21/17 20:17 N23.6MADEP VPH
Aromatic (C09-C10)21.6 mg/kg 09/21/17 20:17 N23.6MADEP VPH
1,2,4-Trimethylbenzene 0.14 mg/kg 09/21/17 15:220.13EPA 8260
Percent Moisture 23.1 %09/21/17 11:120.10ASTM D2974-87
92355949012 SB-4C
Aliphatic (C05-C08)13.9 mg/kg 09/21/17 20:45 N23.0MADEP VPH
Aliphatic (C09-C12)5.8 mg/kg 09/21/17 20:45 N23.0MADEP VPH
Aromatic (C09-C10)5.7 mg/kg 09/21/17 20:45 N23.0MADEP VPH
sec-Butylbenzene 0.21 mg/kg 09/21/17 16:020.14EPA 8260
p-Isopropyltoluene 0.28 mg/kg 09/21/17 16:020.14EPA 8260
Naphthalene 0.30 mg/kg 09/21/17 16:020.14EPA 8260
n-Propylbenzene 0.71 mg/kg 09/21/17 16:020.14EPA 8260
1,2,4-Trimethylbenzene 1.6 mg/kg 09/21/17 16:020.14EPA 8260
1,3,5-Trimethylbenzene 0.42 mg/kg 09/21/17 16:020.14EPA 8260
Percent Moisture 19.3 %09/21/17 11:120.10ASTM D2974-87
92355949013 SB-5A
Aromatic (C11-C22)34.8 mg/kg 09/22/17 13:01 N212.6MADEP EPH
Percent Moisture 19.9 %09/21/17 11:120.10ASTM D2974-87
92355949014 SB-5B
Aliphatic (C19-C36)36.2 mg/kg 09/21/17 20:16 N213.1MADEP EPH
1,2,4-Trimethylbenzene 0.010 mg/kg 09/22/17 14:250.0061EPA 8260
Percent Moisture 24.5 %09/21/17 11:120.10ASTM D2974-87
92355949015 SB-5C
Acetone 0.13 mg/kg 09/25/17 20:260.089EPA 8260
n-Butylbenzene 0.029 mg/kg 09/25/17 20:260.0044EPA 8260
sec-Butylbenzene 0.0068 mg/kg 09/25/17 20:260.0044EPA 8260
Ethylbenzene 0.020 mg/kg 09/25/17 20:260.0044EPA 8260
Isopropylbenzene (Cumene)0.0073 mg/kg 09/25/17 20:260.0044EPA 8260
p-Isopropyltoluene 0.017 mg/kg 09/25/17 20:260.0044EPA 8260
Naphthalene 0.080 mg/kg 09/25/17 20:260.0044EPA 8260
n-Propylbenzene 0.038 mg/kg 09/25/17 20:260.0044EPA 8260
1,2,4-Trimethylbenzene 0.28 mg/kg 09/25/17 20:26 E0.0044EPA 8260
1,3,5-Trimethylbenzene 0.086 mg/kg 09/25/17 20:260.0044EPA 8260
Xylene (Total)0.12 mg/kg 09/25/17 20:260.0089EPA 8260
m&p-Xylene 0.085 mg/kg 09/25/17 20:260.0089EPA 8260
o-Xylene 0.032 mg/kg 09/25/17 20:260.0044EPA 8260
Percent Moisture 13.2 %09/21/17 11:120.10ASTM D2974-87
92355949016 SB-6A
Percent Moisture 18.3 %09/21/17 11:120.10ASTM D2974-87
92355949017 SB-6B
1,2,4-Trimethylbenzene 0.029 mg/kg 09/22/17 15:240.0060EPA 8260
1,3,5-Trimethylbenzene 0.0090 mg/kg 09/22/17 15:240.0060EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 165
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92355949
Blvd B.P.
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92355949017 SB-6B
Xylene (Total)0.013 mg/kg 09/22/17 15:240.012EPA 8260
m&p-Xylene 0.013 mg/kg 09/22/17 15:240.012EPA 8260
Percent Moisture 24.0 %09/21/17 11:120.10ASTM D2974-87
92355949018 SB-6C
Aromatic (C11-C22)17.9 mg/kg 09/22/17 13:56 N212.5MADEP EPH
Percent Moisture 20.1 %09/21/17 11:120.10ASTM D2974-87
92355949019 SB-7A
Percent Moisture 19.4 %09/21/17 11:120.10ASTM D2974-87
92355949020 SB-7B
Percent Moisture 25.7 %09/21/17 11:130.10ASTM D2974-87
92355949021 SB-7C
Aliphatic (C19-C36)32.8 mg/kg 09/25/17 17:34 N212.8MADEP EPH
Aromatic (C11-C22)19.1 mg/kg 09/25/17 17:34 N212.8MADEP EPH
Percent Moisture 22.9 %09/21/17 11:130.10ASTM D2974-87
92355949022 SB-8A
Percent Moisture 22.0 %09/21/17 11:130.10ASTM D2974-87
92355949023 SB-8B
Acetone 0.11 mg/kg 09/22/17 17:22 L10.10EPA 8260
Percent Moisture 24.7 %09/21/17 11:130.10ASTM D2974-87
92355949024 SB-8C
Percent Moisture 19.2 %09/21/17 11:130.10ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-1A Lab ID:92355949001 Collected:09/18/17 18:30 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/21/17 16:37 N209/21/17 08:0513.1 1
Aliphatic (C19-C36)ND mg/kg 09/21/17 16:37 N209/21/17 08:0513.1 1
Aromatic (C11-C22)ND mg/kg 09/21/17 16:37 N209/21/17 08:0513.1 1
Surrogates
Nonatriacontane (S)62 %09/21/17 16:37 7194-86-709/21/17 08:0540-140 1
o-Terphenyl (S)54 %09/21/17 16:37 84-15-109/21/17 08:0540-140 1
2-Fluorobiphenyl (S)90 %09/21/17 16:37 321-60-809/21/17 08:0540-140 1
2-Bromonaphthalene (S)90 %09/21/17 16:37 580-13-209/21/17 08:0540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/21/17 15:38 N209/21/17 10:453.5 1
Aliphatic (C09-C12)ND mg/kg 09/21/17 15:38 N209/21/17 10:453.5 1
Aromatic (C09-C10)ND mg/kg 09/21/17 15:38 N209/21/17 10:453.5 1
Surrogates
4-Bromofluorobenzene (FID) (S)104 %09/21/17 15:38 460-00-409/21/17 10:4570-130 1
4-Bromofluorobenzene (PID) (S)98 %09/21/17 15:38 460-00-409/21/17 10:4570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/21/17 15:13 83-32-909/20/17 18:120.43 1
Acenaphthylene ND mg/kg 09/21/17 15:13 208-96-809/20/17 18:120.43 1
Aniline ND mg/kg 09/21/17 15:13 62-53-309/20/17 18:120.43 1
Anthracene ND mg/kg 09/21/17 15:13 120-12-709/20/17 18:120.43 1
Benzo(a)anthracene ND mg/kg 09/21/17 15:13 56-55-309/20/17 18:120.43 1
Benzo(a)pyrene ND mg/kg 09/21/17 15:13 50-32-809/20/17 18:120.43 1
Benzo(b)fluoranthene ND mg/kg 09/21/17 15:13 205-99-209/20/17 18:120.43 1
Benzo(g,h,i)perylene ND mg/kg 09/21/17 15:13 191-24-209/20/17 18:120.43 1
Benzo(k)fluoranthene ND mg/kg 09/21/17 15:13 207-08-909/20/17 18:120.43 1
Benzoic Acid ND mg/kg 09/21/17 15:13 65-85-0 M109/20/17 18:122.2 1
Benzyl alcohol ND mg/kg 09/21/17 15:13 100-51-609/20/17 18:120.87 1
4-Bromophenylphenyl ether ND mg/kg 09/21/17 15:13 101-55-309/20/17 18:120.43 1
Butylbenzylphthalate ND mg/kg 09/21/17 15:13 85-68-709/20/17 18:120.43 1
4-Chloro-3-methylphenol ND mg/kg 09/21/17 15:13 59-50-709/20/17 18:120.87 1
4-Chloroaniline ND mg/kg 09/21/17 15:13 106-47-809/20/17 18:122.2 1
bis(2-Chloroethoxy)methane ND mg/kg 09/21/17 15:13 111-91-109/20/17 18:120.43 1
bis(2-Chloroethyl) ether ND mg/kg 09/21/17 15:13 111-44-409/20/17 18:120.43 1
2-Chloronaphthalene ND mg/kg 09/21/17 15:13 91-58-709/20/17 18:120.43 1
2-Chlorophenol ND mg/kg 09/21/17 15:13 95-57-809/20/17 18:120.43 1
4-Chlorophenylphenyl ether ND mg/kg 09/21/17 15:13 7005-72-309/20/17 18:120.43 1
Chrysene ND mg/kg 09/21/17 15:13 218-01-909/20/17 18:120.43 1
Dibenz(a,h)anthracene ND mg/kg 09/21/17 15:13 53-70-309/20/17 18:120.43 1
Dibenzofuran ND mg/kg 09/21/17 15:13 132-64-909/20/17 18:120.43 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 15:13 95-50-1 M109/20/17 18:120.43 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 15:13 541-73-109/20/17 18:120.43 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 15:13 106-46-709/20/17 18:120.43 1
3,3'-Dichlorobenzidine ND mg/kg 09/21/17 15:13 91-94-109/20/17 18:122.2 1
2,4-Dichlorophenol ND mg/kg 09/21/17 15:13 120-83-209/20/17 18:120.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-1A Lab ID:92355949001 Collected:09/18/17 18:30 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/21/17 15:13 84-66-209/20/17 18:120.43 1
2,4-Dimethylphenol ND mg/kg 09/21/17 15:13 105-67-909/20/17 18:120.43 1
Dimethylphthalate ND mg/kg 09/21/17 15:13 131-11-309/20/17 18:120.43 1
Di-n-butylphthalate ND mg/kg 09/21/17 15:13 84-74-209/20/17 18:120.43 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/21/17 15:13 534-52-109/20/17 18:120.87 1
2,4-Dinitrophenol ND mg/kg 09/21/17 15:13 51-28-5 M109/20/17 18:122.2 1
2,4-Dinitrotoluene ND mg/kg 09/21/17 15:13 121-14-209/20/17 18:120.43 1
2,6-Dinitrotoluene ND mg/kg 09/21/17 15:13 606-20-209/20/17 18:120.43 1
Di-n-octylphthalate ND mg/kg 09/21/17 15:13 117-84-009/20/17 18:120.43 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/21/17 15:13 117-81-709/20/17 18:120.43 1
Fluoranthene ND mg/kg 09/21/17 15:13 206-44-009/20/17 18:120.43 1
Fluorene ND mg/kg 09/21/17 15:13 86-73-709/20/17 18:120.43 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 15:13 87-68-309/20/17 18:120.43 1
Hexachlorobenzene ND mg/kg 09/21/17 15:13 118-74-109/20/17 18:120.43 1
Hexachlorocyclopentadiene ND mg/kg 09/21/17 15:13 77-47-409/20/17 18:120.43 1
Hexachloroethane ND mg/kg 09/21/17 15:13 67-72-109/20/17 18:120.43 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/21/17 15:13 193-39-509/20/17 18:120.43 1
Isophorone ND mg/kg 09/21/17 15:13 78-59-109/20/17 18:120.43 1
1-Methylnaphthalene ND mg/kg 09/21/17 15:13 90-12-009/20/17 18:120.43 1
2-Methylnaphthalene ND mg/kg 09/21/17 15:13 91-57-609/20/17 18:120.43 1
2-Methylphenol(o-Cresol)ND mg/kg 09/21/17 15:13 95-48-709/20/17 18:120.43 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/21/17 15:13 15831-10-409/20/17 18:120.43 1
Naphthalene ND mg/kg 09/21/17 15:13 91-20-309/20/17 18:120.43 1
2-Nitroaniline ND mg/kg 09/21/17 15:13 88-74-409/20/17 18:122.2 1
3-Nitroaniline ND mg/kg 09/21/17 15:13 99-09-209/20/17 18:122.2 1
4-Nitroaniline ND mg/kg 09/21/17 15:13 100-01-609/20/17 18:120.87 1
Nitrobenzene ND mg/kg 09/21/17 15:13 98-95-309/20/17 18:120.43 1
2-Nitrophenol ND mg/kg 09/21/17 15:13 88-75-509/20/17 18:120.43 1
4-Nitrophenol ND mg/kg 09/21/17 15:13 100-02-709/20/17 18:122.2 1
N-Nitrosodimethylamine ND mg/kg 09/21/17 15:13 62-75-909/20/17 18:120.43 1
N-Nitroso-di-n-propylamine ND mg/kg 09/21/17 15:13 621-64-709/20/17 18:120.43 1
N-Nitrosodiphenylamine ND mg/kg 09/21/17 15:13 86-30-609/20/17 18:120.43 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/21/17 15:13 108-60-1 M109/20/17 18:120.43 1
Pentachlorophenol ND mg/kg 09/21/17 15:13 87-86-509/20/17 18:122.2 1
Phenanthrene ND mg/kg 09/21/17 15:13 85-01-809/20/17 18:120.43 1
Phenol ND mg/kg 09/21/17 15:13 108-95-209/20/17 18:120.43 1
Pyrene ND mg/kg 09/21/17 15:13 129-00-009/20/17 18:120.43 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 15:13 120-82-109/20/17 18:120.43 1
2,4,5-Trichlorophenol ND mg/kg 09/21/17 15:13 95-95-409/20/17 18:120.43 1
2,4,6-Trichlorophenol ND mg/kg 09/21/17 15:13 88-06-209/20/17 18:120.43 1
Surrogates
Nitrobenzene-d5 (S)57 %09/21/17 15:13 4165-60-009/20/17 18:1223-110 1
2-Fluorobiphenyl (S)53 %09/21/17 15:13 321-60-809/20/17 18:1230-110 1
Terphenyl-d14 (S)77 %09/21/17 15:13 1718-51-009/20/17 18:1228-110 1
Phenol-d6 (S)54 %09/21/17 15:13 13127-88-309/20/17 18:1222-110 1
2-Fluorophenol (S)51 %09/21/17 15:13 367-12-409/20/17 18:1213-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-1A Lab ID:92355949001 Collected:09/18/17 18:30 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)63 %09/21/17 15:13 118-79-609/20/17 18:1227-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/21/17 19:36 67-64-10.096 1
Benzene ND mg/kg 09/21/17 19:36 71-43-20.0048 1
Bromobenzene ND mg/kg 09/21/17 19:36 108-86-10.0048 1
Bromochloromethane ND mg/kg 09/21/17 19:36 74-97-50.0048 1
Bromodichloromethane ND mg/kg 09/21/17 19:36 75-27-40.0048 1
Bromoform ND mg/kg 09/21/17 19:36 75-25-20.0048 1
Bromomethane ND mg/kg 09/21/17 19:36 74-83-90.0096 1
2-Butanone (MEK)ND mg/kg 09/21/17 19:36 78-93-30.096 1
n-Butylbenzene ND mg/kg 09/21/17 19:36 104-51-80.0048 1
sec-Butylbenzene ND mg/kg 09/21/17 19:36 135-98-80.0048 1
tert-Butylbenzene ND mg/kg 09/21/17 19:36 98-06-60.0048 1
Carbon tetrachloride ND mg/kg 09/21/17 19:36 56-23-50.0048 1
Chlorobenzene ND mg/kg 09/21/17 19:36 108-90-70.0048 1
Chloroethane ND mg/kg 09/21/17 19:36 75-00-30.0096 1
Chloroform ND mg/kg 09/21/17 19:36 67-66-30.0048 1
Chloromethane ND mg/kg 09/21/17 19:36 74-87-30.0096 1
2-Chlorotoluene ND mg/kg 09/21/17 19:36 95-49-80.0048 1
4-Chlorotoluene ND mg/kg 09/21/17 19:36 106-43-40.0048 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/21/17 19:36 96-12-80.0048 1
Dibromochloromethane ND mg/kg 09/21/17 19:36 124-48-10.0048 1
1,2-Dibromoethane (EDB)ND mg/kg 09/21/17 19:36 106-93-40.0048 1
Dibromomethane ND mg/kg 09/21/17 19:36 74-95-30.0048 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 19:36 95-50-10.0048 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 19:36 541-73-10.0048 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 19:36 106-46-70.0048 1
Dichlorodifluoromethane ND mg/kg 09/21/17 19:36 75-71-80.0096 1
1,1-Dichloroethane ND mg/kg 09/21/17 19:36 75-34-30.0048 1
1,2-Dichloroethane ND mg/kg 09/21/17 19:36 107-06-20.0048 1
1,1-Dichloroethene ND mg/kg 09/21/17 19:36 75-35-40.0048 1
cis-1,2-Dichloroethene ND mg/kg 09/21/17 19:36 156-59-20.0048 1
trans-1,2-Dichloroethene ND mg/kg 09/21/17 19:36 156-60-50.0048 1
1,2-Dichloropropane ND mg/kg 09/21/17 19:36 78-87-50.0048 1
1,3-Dichloropropane ND mg/kg 09/21/17 19:36 142-28-90.0048 1
2,2-Dichloropropane ND mg/kg 09/21/17 19:36 594-20-70.0048 1
1,1-Dichloropropene ND mg/kg 09/21/17 19:36 563-58-60.0048 1
cis-1,3-Dichloropropene ND mg/kg 09/21/17 19:36 10061-01-50.0048 1
trans-1,3-Dichloropropene ND mg/kg 09/21/17 19:36 10061-02-60.0048 1
Diisopropyl ether ND mg/kg 09/21/17 19:36 108-20-30.0048 1
Ethylbenzene ND mg/kg 09/21/17 19:36 100-41-40.0048 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 19:36 87-68-30.0048 1
2-Hexanone ND mg/kg 09/21/17 19:36 591-78-60.048 1
Isopropylbenzene (Cumene)ND mg/kg 09/21/17 19:36 98-82-80.0048 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-1A Lab ID:92355949001 Collected:09/18/17 18:30 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND mg/kg 09/21/17 19:36 99-87-60.0048 1
Methylene Chloride ND mg/kg 09/21/17 19:36 75-09-20.019 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/21/17 19:36 108-10-10.048 1
Methyl-tert-butyl ether ND mg/kg 09/21/17 19:36 1634-04-40.0048 1
Naphthalene ND mg/kg 09/21/17 19:36 91-20-30.0048 1
n-Propylbenzene ND mg/kg 09/21/17 19:36 103-65-10.0048 1
Styrene ND mg/kg 09/21/17 19:36 100-42-50.0048 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/21/17 19:36 630-20-60.0048 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/21/17 19:36 79-34-50.0048 1
Tetrachloroethene ND mg/kg 09/21/17 19:36 127-18-40.0048 1
Toluene ND mg/kg 09/21/17 19:36 108-88-30.0048 1
1,2,3-Trichlorobenzene ND mg/kg 09/21/17 19:36 87-61-60.0048 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 19:36 120-82-10.0048 1
1,1,1-Trichloroethane ND mg/kg 09/21/17 19:36 71-55-60.0048 1
1,1,2-Trichloroethane ND mg/kg 09/21/17 19:36 79-00-50.0048 1
Trichloroethene ND mg/kg 09/21/17 19:36 79-01-60.0048 1
Trichlorofluoromethane ND mg/kg 09/21/17 19:36 75-69-40.0048 1
1,2,3-Trichloropropane ND mg/kg 09/21/17 19:36 96-18-40.0048 1
1,2,4-Trimethylbenzene ND mg/kg 09/21/17 19:36 95-63-60.0048 1
1,3,5-Trimethylbenzene ND mg/kg 09/21/17 19:36 108-67-80.0048 1
Vinyl acetate ND mg/kg 09/21/17 19:36 108-05-40.048 1
Vinyl chloride ND mg/kg 09/21/17 19:36 75-01-40.0096 1
Xylene (Total)ND mg/kg 09/21/17 19:36 1330-20-70.0096 1
m&p-Xylene ND mg/kg 09/21/17 19:36 179601-23-10.0096 1
o-Xylene ND mg/kg 09/21/17 19:36 95-47-60.0048 1
Surrogates
Toluene-d8 (S)97 %09/21/17 19:36 2037-26-570-130 1
4-Bromofluorobenzene (S)100 %09/21/17 19:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %09/21/17 19:36 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 23.6 %09/21/17 11:080.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-1B Lab ID:92355949002 Collected:09/18/17 18:40 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/21/17 17:04 N209/21/17 08:0513.9 1
Aliphatic (C19-C36)ND mg/kg 09/21/17 17:04 N209/21/17 08:0513.9 1
Aromatic (C11-C22)ND mg/kg 09/21/17 17:04 N209/21/17 08:0513.9 1
Surrogates
Nonatriacontane (S)44 %09/21/17 17:04 7194-86-709/21/17 08:0540-140 1
o-Terphenyl (S)77 %09/21/17 17:04 84-15-109/21/17 08:0540-140 1
2-Fluorobiphenyl (S)108 %09/21/17 17:04 321-60-809/21/17 08:0540-140 1
2-Bromonaphthalene (S)105 %09/21/17 17:04 580-13-209/21/17 08:0540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)184 mg/kg 09/21/17 16:06 N209/21/17 10:453.8 1
Aliphatic (C09-C12)101 mg/kg 09/21/17 16:06 N209/21/17 10:453.8 1
Aromatic (C09-C10)254 mg/kg 09/21/17 16:06 N209/21/17 10:453.8 1
Surrogates
4-Bromofluorobenzene (FID) (S)189 %09/21/17 16:06 460-00-4 S509/21/17 10:4570-130 1
4-Bromofluorobenzene (PID) (S)112 %09/21/17 16:06 460-00-409/21/17 10:4570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/21/17 16:12 83-32-909/20/17 18:120.46 1
Acenaphthylene ND mg/kg 09/21/17 16:12 208-96-809/20/17 18:120.46 1
Aniline ND mg/kg 09/21/17 16:12 62-53-309/20/17 18:120.46 1
Anthracene ND mg/kg 09/21/17 16:12 120-12-709/20/17 18:120.46 1
Benzo(a)anthracene ND mg/kg 09/21/17 16:12 56-55-309/20/17 18:120.46 1
Benzo(a)pyrene ND mg/kg 09/21/17 16:12 50-32-809/20/17 18:120.46 1
Benzo(b)fluoranthene ND mg/kg 09/21/17 16:12 205-99-209/20/17 18:120.46 1
Benzo(g,h,i)perylene ND mg/kg 09/21/17 16:12 191-24-209/20/17 18:120.46 1
Benzo(k)fluoranthene ND mg/kg 09/21/17 16:12 207-08-909/20/17 18:120.46 1
Benzoic Acid ND mg/kg 09/21/17 16:12 65-85-009/20/17 18:122.3 1
Benzyl alcohol ND mg/kg 09/21/17 16:12 100-51-609/20/17 18:120.92 1
4-Bromophenylphenyl ether ND mg/kg 09/21/17 16:12 101-55-309/20/17 18:120.46 1
Butylbenzylphthalate ND mg/kg 09/21/17 16:12 85-68-709/20/17 18:120.46 1
4-Chloro-3-methylphenol ND mg/kg 09/21/17 16:12 59-50-709/20/17 18:120.92 1
4-Chloroaniline ND mg/kg 09/21/17 16:12 106-47-809/20/17 18:122.3 1
bis(2-Chloroethoxy)methane ND mg/kg 09/21/17 16:12 111-91-109/20/17 18:120.46 1
bis(2-Chloroethyl) ether ND mg/kg 09/21/17 16:12 111-44-409/20/17 18:120.46 1
2-Chloronaphthalene ND mg/kg 09/21/17 16:12 91-58-709/20/17 18:120.46 1
2-Chlorophenol ND mg/kg 09/21/17 16:12 95-57-809/20/17 18:120.46 1
4-Chlorophenylphenyl ether ND mg/kg 09/21/17 16:12 7005-72-309/20/17 18:120.46 1
Chrysene ND mg/kg 09/21/17 16:12 218-01-909/20/17 18:120.46 1
Dibenz(a,h)anthracene ND mg/kg 09/21/17 16:12 53-70-309/20/17 18:120.46 1
Dibenzofuran ND mg/kg 09/21/17 16:12 132-64-909/20/17 18:120.46 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 16:12 95-50-109/20/17 18:120.46 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 16:12 541-73-109/20/17 18:120.46 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 16:12 106-46-709/20/17 18:120.46 1
3,3'-Dichlorobenzidine ND mg/kg 09/21/17 16:12 91-94-109/20/17 18:122.3 1
2,4-Dichlorophenol ND mg/kg 09/21/17 16:12 120-83-209/20/17 18:120.46 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-1B Lab ID:92355949002 Collected:09/18/17 18:40 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/21/17 16:12 84-66-209/20/17 18:120.46 1
2,4-Dimethylphenol ND mg/kg 09/21/17 16:12 105-67-909/20/17 18:120.46 1
Dimethylphthalate ND mg/kg 09/21/17 16:12 131-11-309/20/17 18:120.46 1
Di-n-butylphthalate ND mg/kg 09/21/17 16:12 84-74-209/20/17 18:120.46 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/21/17 16:12 534-52-109/20/17 18:120.92 1
2,4-Dinitrophenol ND mg/kg 09/21/17 16:12 51-28-509/20/17 18:122.3 1
2,4-Dinitrotoluene ND mg/kg 09/21/17 16:12 121-14-209/20/17 18:120.46 1
2,6-Dinitrotoluene ND mg/kg 09/21/17 16:12 606-20-209/20/17 18:120.46 1
Di-n-octylphthalate ND mg/kg 09/21/17 16:12 117-84-009/20/17 18:120.46 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/21/17 16:12 117-81-709/20/17 18:120.46 1
Fluoranthene ND mg/kg 09/21/17 16:12 206-44-009/20/17 18:120.46 1
Fluorene ND mg/kg 09/21/17 16:12 86-73-709/20/17 18:120.46 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 16:12 87-68-309/20/17 18:120.46 1
Hexachlorobenzene ND mg/kg 09/21/17 16:12 118-74-109/20/17 18:120.46 1
Hexachlorocyclopentadiene ND mg/kg 09/21/17 16:12 77-47-409/20/17 18:120.46 1
Hexachloroethane ND mg/kg 09/21/17 16:12 67-72-109/20/17 18:120.46 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/21/17 16:12 193-39-509/20/17 18:120.46 1
Isophorone ND mg/kg 09/21/17 16:12 78-59-109/20/17 18:120.46 1
1-Methylnaphthalene 0.52 mg/kg 09/21/17 16:12 90-12-009/20/17 18:120.46 1
2-Methylnaphthalene 1.1 mg/kg 09/21/17 16:12 91-57-609/20/17 18:120.46 1
2-Methylphenol(o-Cresol)ND mg/kg 09/21/17 16:12 95-48-709/20/17 18:120.46 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/21/17 16:12 15831-10-409/20/17 18:120.46 1
Naphthalene 0.87 mg/kg 09/21/17 16:12 91-20-309/20/17 18:120.46 1
2-Nitroaniline ND mg/kg 09/21/17 16:12 88-74-409/20/17 18:122.3 1
3-Nitroaniline ND mg/kg 09/21/17 16:12 99-09-209/20/17 18:122.3 1
4-Nitroaniline ND mg/kg 09/21/17 16:12 100-01-609/20/17 18:120.92 1
Nitrobenzene ND mg/kg 09/21/17 16:12 98-95-309/20/17 18:120.46 1
2-Nitrophenol ND mg/kg 09/21/17 16:12 88-75-509/20/17 18:120.46 1
4-Nitrophenol ND mg/kg 09/21/17 16:12 100-02-709/20/17 18:122.3 1
N-Nitrosodimethylamine ND mg/kg 09/21/17 16:12 62-75-909/20/17 18:120.46 1
N-Nitroso-di-n-propylamine ND mg/kg 09/21/17 16:12 621-64-709/20/17 18:120.46 1
N-Nitrosodiphenylamine ND mg/kg 09/21/17 16:12 86-30-609/20/17 18:120.46 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/21/17 16:12 108-60-109/20/17 18:120.46 1
Pentachlorophenol ND mg/kg 09/21/17 16:12 87-86-509/20/17 18:122.3 1
Phenanthrene ND mg/kg 09/21/17 16:12 85-01-809/20/17 18:120.46 1
Phenol ND mg/kg 09/21/17 16:12 108-95-209/20/17 18:120.46 1
Pyrene ND mg/kg 09/21/17 16:12 129-00-009/20/17 18:120.46 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 16:12 120-82-109/20/17 18:120.46 1
2,4,5-Trichlorophenol ND mg/kg 09/21/17 16:12 95-95-409/20/17 18:120.46 1
2,4,6-Trichlorophenol ND mg/kg 09/21/17 16:12 88-06-209/20/17 18:120.46 1
Surrogates
Nitrobenzene-d5 (S)36 %09/21/17 16:12 4165-60-009/20/17 18:1223-110 1
2-Fluorobiphenyl (S)37 %09/21/17 16:12 321-60-809/20/17 18:1230-110 1
Terphenyl-d14 (S)78 %09/21/17 16:12 1718-51-009/20/17 18:1228-110 1
Phenol-d6 (S)41 %09/21/17 16:12 13127-88-309/20/17 18:1222-110 1
2-Fluorophenol (S)41 %09/21/17 16:12 367-12-409/20/17 18:1213-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-1B Lab ID:92355949002 Collected:09/18/17 18:40 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)63 %09/21/17 16:12 118-79-609/20/17 18:1227-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/21/17 19:56 67-64-13.2 25
Benzene ND mg/kg 09/21/17 19:56 71-43-20.16 25
Bromobenzene ND mg/kg 09/21/17 19:56 108-86-10.16 25
Bromochloromethane ND mg/kg 09/21/17 19:56 74-97-50.16 25
Bromodichloromethane ND mg/kg 09/21/17 19:56 75-27-40.16 25
Bromoform ND mg/kg 09/21/17 19:56 75-25-20.16 25
Bromomethane ND mg/kg 09/21/17 19:56 74-83-90.32 25
2-Butanone (MEK)ND mg/kg 09/21/17 19:56 78-93-33.2 25
n-Butylbenzene ND mg/kg 09/21/17 19:56 104-51-80.16 25
sec-Butylbenzene ND mg/kg 09/21/17 19:56 135-98-80.16 25
tert-Butylbenzene ND mg/kg 09/21/17 19:56 98-06-60.16 25
Carbon tetrachloride ND mg/kg 09/21/17 19:56 56-23-50.16 25
Chlorobenzene ND mg/kg 09/21/17 19:56 108-90-70.16 25
Chloroethane ND mg/kg 09/21/17 19:56 75-00-30.32 25
Chloroform ND mg/kg 09/21/17 19:56 67-66-30.16 25
Chloromethane ND mg/kg 09/21/17 19:56 74-87-30.32 25
2-Chlorotoluene ND mg/kg 09/21/17 19:56 95-49-80.16 25
4-Chlorotoluene ND mg/kg 09/21/17 19:56 106-43-40.16 25
1,2-Dibromo-3-chloropropane ND mg/kg 09/21/17 19:56 96-12-80.16 25
Dibromochloromethane ND mg/kg 09/21/17 19:56 124-48-10.16 25
1,2-Dibromoethane (EDB)ND mg/kg 09/21/17 19:56 106-93-40.16 25
Dibromomethane ND mg/kg 09/21/17 19:56 74-95-30.16 25
1,2-Dichlorobenzene ND mg/kg 09/21/17 19:56 95-50-10.16 25
1,3-Dichlorobenzene ND mg/kg 09/21/17 19:56 541-73-10.16 25
1,4-Dichlorobenzene ND mg/kg 09/21/17 19:56 106-46-70.16 25
Dichlorodifluoromethane ND mg/kg 09/21/17 19:56 75-71-80.32 25
1,1-Dichloroethane ND mg/kg 09/21/17 19:56 75-34-30.16 25
1,2-Dichloroethane ND mg/kg 09/21/17 19:56 107-06-20.16 25
1,1-Dichloroethene ND mg/kg 09/21/17 19:56 75-35-40.16 25
cis-1,2-Dichloroethene ND mg/kg 09/21/17 19:56 156-59-20.16 25
trans-1,2-Dichloroethene ND mg/kg 09/21/17 19:56 156-60-50.16 25
1,2-Dichloropropane ND mg/kg 09/21/17 19:56 78-87-50.16 25
1,3-Dichloropropane ND mg/kg 09/21/17 19:56 142-28-90.16 25
2,2-Dichloropropane ND mg/kg 09/21/17 19:56 594-20-70.16 25
1,1-Dichloropropene ND mg/kg 09/21/17 19:56 563-58-60.16 25
cis-1,3-Dichloropropene ND mg/kg 09/21/17 19:56 10061-01-50.16 25
trans-1,3-Dichloropropene ND mg/kg 09/21/17 19:56 10061-02-60.16 25
Diisopropyl ether ND mg/kg 09/21/17 19:56 108-20-30.16 25
Ethylbenzene ND mg/kg 09/21/17 19:56 100-41-40.16 25
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 19:56 87-68-30.16 25
2-Hexanone ND mg/kg 09/21/17 19:56 591-78-61.6 25
Isopropylbenzene (Cumene)ND mg/kg 09/21/17 19:56 98-82-80.16 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-1B Lab ID:92355949002 Collected:09/18/17 18:40 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND mg/kg 09/21/17 19:56 99-87-60.16 25
Methylene Chloride ND mg/kg 09/21/17 19:56 75-09-20.65 25
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/21/17 19:56 108-10-11.6 25
Methyl-tert-butyl ether ND mg/kg 09/21/17 19:56 1634-04-40.16 25
Naphthalene 0.29 mg/kg 09/21/17 19:56 91-20-30.16 25
n-Propylbenzene 0.22 mg/kg 09/21/17 19:56 103-65-10.16 25
Styrene ND mg/kg 09/21/17 19:56 100-42-50.16 25
1,1,1,2-Tetrachloroethane ND mg/kg 09/21/17 19:56 630-20-60.16 25
1,1,2,2-Tetrachloroethane ND mg/kg 09/21/17 19:56 79-34-50.16 25
Tetrachloroethene ND mg/kg 09/21/17 19:56 127-18-40.16 25
Toluene ND mg/kg 09/21/17 19:56 108-88-30.16 25
1,2,3-Trichlorobenzene ND mg/kg 09/21/17 19:56 87-61-60.16 25
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 19:56 120-82-10.16 25
1,1,1-Trichloroethane ND mg/kg 09/21/17 19:56 71-55-60.16 25
1,1,2-Trichloroethane ND mg/kg 09/21/17 19:56 79-00-50.16 25
Trichloroethene ND mg/kg 09/21/17 19:56 79-01-60.16 25
Trichlorofluoromethane ND mg/kg 09/21/17 19:56 75-69-40.16 25
1,2,3-Trichloropropane ND mg/kg 09/21/17 19:56 96-18-40.16 25
1,2,4-Trimethylbenzene 1.1 mg/kg 09/21/17 19:56 95-63-60.16 25
1,3,5-Trimethylbenzene 0.41 mg/kg 09/21/17 19:56 108-67-80.16 25
Vinyl acetate ND mg/kg 09/21/17 19:56 108-05-41.6 25
Vinyl chloride ND mg/kg 09/21/17 19:56 75-01-40.32 25
Xylene (Total)0.47 mg/kg 09/21/17 19:56 1330-20-70.32 25
m&p-Xylene 0.47 mg/kg 09/21/17 19:56 179601-23-10.32 25
o-Xylene ND mg/kg 09/21/17 19:56 95-47-60.16 25
Surrogates
Toluene-d8 (S)99 %09/21/17 19:56 2037-26-5 D370-130 25
4-Bromofluorobenzene (S)100 %09/21/17 19:56 460-00-470-130 25
1,2-Dichloroethane-d4 (S)99 %09/21/17 19:56 17060-07-070-132 25
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 28.3 %09/21/17 11:090.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-1C Lab ID:92355949003 Collected:09/18/17 18:55 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/25/17 16:39 N209/23/17 08:3712.0 1
Aliphatic (C19-C36)ND mg/kg 09/25/17 16:39 N209/23/17 08:3712.0 1
Aromatic (C11-C22)ND mg/kg 09/25/17 16:39 N209/23/17 08:3712.0 1
Surrogates
Nonatriacontane (S)59 %09/25/17 16:39 7194-86-709/23/17 08:3740-140 1
o-Terphenyl (S)55 %09/25/17 16:39 84-15-109/23/17 08:3740-140 1
2-Fluorobiphenyl (S)63 %09/25/17 16:39 321-60-809/23/17 08:3740-140 1
2-Bromonaphthalene (S)22 %09/25/17 16:39 580-13-2 S009/23/17 08:3740-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/21/17 16:34 N209/21/17 10:453.2 1
Aliphatic (C09-C12)ND mg/kg 09/21/17 16:34 N209/21/17 10:453.2 1
Aromatic (C09-C10)4.4 mg/kg 09/21/17 16:34 N209/21/17 10:453.2 1
Surrogates
4-Bromofluorobenzene (FID) (S)102 %09/21/17 16:34 460-00-409/21/17 10:4570-130 1
4-Bromofluorobenzene (PID) (S)95 %09/21/17 16:34 460-00-409/21/17 10:4570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/21/17 17:11 83-32-909/20/17 18:120.40 1
Acenaphthylene ND mg/kg 09/21/17 17:11 208-96-809/20/17 18:120.40 1
Aniline ND mg/kg 09/21/17 17:11 62-53-309/20/17 18:120.40 1
Anthracene ND mg/kg 09/21/17 17:11 120-12-709/20/17 18:120.40 1
Benzo(a)anthracene ND mg/kg 09/21/17 17:11 56-55-309/20/17 18:120.40 1
Benzo(a)pyrene ND mg/kg 09/21/17 17:11 50-32-809/20/17 18:120.40 1
Benzo(b)fluoranthene ND mg/kg 09/21/17 17:11 205-99-209/20/17 18:120.40 1
Benzo(g,h,i)perylene ND mg/kg 09/21/17 17:11 191-24-209/20/17 18:120.40 1
Benzo(k)fluoranthene ND mg/kg 09/21/17 17:11 207-08-909/20/17 18:120.40 1
Benzoic Acid ND mg/kg 09/21/17 17:11 65-85-009/20/17 18:122.0 1
Benzyl alcohol ND mg/kg 09/21/17 17:11 100-51-609/20/17 18:120.80 1
4-Bromophenylphenyl ether ND mg/kg 09/21/17 17:11 101-55-309/20/17 18:120.40 1
Butylbenzylphthalate ND mg/kg 09/21/17 17:11 85-68-709/20/17 18:120.40 1
4-Chloro-3-methylphenol ND mg/kg 09/21/17 17:11 59-50-709/20/17 18:120.80 1
4-Chloroaniline ND mg/kg 09/21/17 17:11 106-47-809/20/17 18:122.0 1
bis(2-Chloroethoxy)methane ND mg/kg 09/21/17 17:11 111-91-109/20/17 18:120.40 1
bis(2-Chloroethyl) ether ND mg/kg 09/21/17 17:11 111-44-409/20/17 18:120.40 1
2-Chloronaphthalene ND mg/kg 09/21/17 17:11 91-58-709/20/17 18:120.40 1
2-Chlorophenol ND mg/kg 09/21/17 17:11 95-57-809/20/17 18:120.40 1
4-Chlorophenylphenyl ether ND mg/kg 09/21/17 17:11 7005-72-309/20/17 18:120.40 1
Chrysene ND mg/kg 09/21/17 17:11 218-01-909/20/17 18:120.40 1
Dibenz(a,h)anthracene ND mg/kg 09/21/17 17:11 53-70-309/20/17 18:120.40 1
Dibenzofuran ND mg/kg 09/21/17 17:11 132-64-909/20/17 18:120.40 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 17:11 95-50-109/20/17 18:120.40 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 17:11 541-73-109/20/17 18:120.40 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 17:11 106-46-709/20/17 18:120.40 1
3,3'-Dichlorobenzidine ND mg/kg 09/21/17 17:11 91-94-109/20/17 18:122.0 1
2,4-Dichlorophenol ND mg/kg 09/21/17 17:11 120-83-209/20/17 18:120.40 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-1C Lab ID:92355949003 Collected:09/18/17 18:55 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/21/17 17:11 84-66-209/20/17 18:120.40 1
2,4-Dimethylphenol ND mg/kg 09/21/17 17:11 105-67-909/20/17 18:120.40 1
Dimethylphthalate ND mg/kg 09/21/17 17:11 131-11-309/20/17 18:120.40 1
Di-n-butylphthalate ND mg/kg 09/21/17 17:11 84-74-209/20/17 18:120.40 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/21/17 17:11 534-52-109/20/17 18:120.80 1
2,4-Dinitrophenol ND mg/kg 09/21/17 17:11 51-28-509/20/17 18:122.0 1
2,4-Dinitrotoluene ND mg/kg 09/21/17 17:11 121-14-209/20/17 18:120.40 1
2,6-Dinitrotoluene ND mg/kg 09/21/17 17:11 606-20-209/20/17 18:120.40 1
Di-n-octylphthalate ND mg/kg 09/21/17 17:11 117-84-009/20/17 18:120.40 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/21/17 17:11 117-81-709/20/17 18:120.40 1
Fluoranthene ND mg/kg 09/21/17 17:11 206-44-009/20/17 18:120.40 1
Fluorene ND mg/kg 09/21/17 17:11 86-73-709/20/17 18:120.40 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 17:11 87-68-309/20/17 18:120.40 1
Hexachlorobenzene ND mg/kg 09/21/17 17:11 118-74-109/20/17 18:120.40 1
Hexachlorocyclopentadiene ND mg/kg 09/21/17 17:11 77-47-409/20/17 18:120.40 1
Hexachloroethane ND mg/kg 09/21/17 17:11 67-72-109/20/17 18:120.40 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/21/17 17:11 193-39-509/20/17 18:120.40 1
Isophorone ND mg/kg 09/21/17 17:11 78-59-109/20/17 18:120.40 1
1-Methylnaphthalene ND mg/kg 09/21/17 17:11 90-12-009/20/17 18:120.40 1
2-Methylnaphthalene ND mg/kg 09/21/17 17:11 91-57-609/20/17 18:120.40 1
2-Methylphenol(o-Cresol)ND mg/kg 09/21/17 17:11 95-48-709/20/17 18:120.40 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/21/17 17:11 15831-10-409/20/17 18:120.40 1
Naphthalene ND mg/kg 09/21/17 17:11 91-20-309/20/17 18:120.40 1
2-Nitroaniline ND mg/kg 09/21/17 17:11 88-74-409/20/17 18:122.0 1
3-Nitroaniline ND mg/kg 09/21/17 17:11 99-09-209/20/17 18:122.0 1
4-Nitroaniline ND mg/kg 09/21/17 17:11 100-01-609/20/17 18:120.80 1
Nitrobenzene ND mg/kg 09/21/17 17:11 98-95-309/20/17 18:120.40 1
2-Nitrophenol ND mg/kg 09/21/17 17:11 88-75-509/20/17 18:120.40 1
4-Nitrophenol ND mg/kg 09/21/17 17:11 100-02-709/20/17 18:122.0 1
N-Nitrosodimethylamine ND mg/kg 09/21/17 17:11 62-75-909/20/17 18:120.40 1
N-Nitroso-di-n-propylamine ND mg/kg 09/21/17 17:11 621-64-709/20/17 18:120.40 1
N-Nitrosodiphenylamine ND mg/kg 09/21/17 17:11 86-30-609/20/17 18:120.40 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/21/17 17:11 108-60-109/20/17 18:120.40 1
Pentachlorophenol ND mg/kg 09/21/17 17:11 87-86-509/20/17 18:122.0 1
Phenanthrene ND mg/kg 09/21/17 17:11 85-01-809/20/17 18:120.40 1
Phenol ND mg/kg 09/21/17 17:11 108-95-209/20/17 18:120.40 1
Pyrene ND mg/kg 09/21/17 17:11 129-00-009/20/17 18:120.40 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 17:11 120-82-109/20/17 18:120.40 1
2,4,5-Trichlorophenol ND mg/kg 09/21/17 17:11 95-95-409/20/17 18:120.40 1
2,4,6-Trichlorophenol ND mg/kg 09/21/17 17:11 88-06-209/20/17 18:120.40 1
Surrogates
Nitrobenzene-d5 (S)41 %09/21/17 17:11 4165-60-009/20/17 18:1223-110 1
2-Fluorobiphenyl (S)37 %09/21/17 17:11 321-60-809/20/17 18:1230-110 1
Terphenyl-d14 (S)62 %09/21/17 17:11 1718-51-009/20/17 18:1228-110 1
Phenol-d6 (S)39 %09/21/17 17:11 13127-88-309/20/17 18:1222-110 1
2-Fluorophenol (S)41 %09/21/17 17:11 367-12-409/20/17 18:1213-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-1C Lab ID:92355949003 Collected:09/18/17 18:55 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)49 %09/21/17 17:11 118-79-609/20/17 18:1227-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/21/17 20:16 67-64-10.11 1
Benzene ND mg/kg 09/21/17 20:16 71-43-20.0055 1
Bromobenzene ND mg/kg 09/21/17 20:16 108-86-10.0055 1
Bromochloromethane ND mg/kg 09/21/17 20:16 74-97-50.0055 1
Bromodichloromethane ND mg/kg 09/21/17 20:16 75-27-40.0055 1
Bromoform ND mg/kg 09/21/17 20:16 75-25-20.0055 1
Bromomethane ND mg/kg 09/21/17 20:16 74-83-90.011 1
2-Butanone (MEK)ND mg/kg 09/21/17 20:16 78-93-30.11 1
n-Butylbenzene ND mg/kg 09/21/17 20:16 104-51-80.0055 1
sec-Butylbenzene ND mg/kg 09/21/17 20:16 135-98-80.0055 1
tert-Butylbenzene ND mg/kg 09/21/17 20:16 98-06-60.0055 1
Carbon tetrachloride ND mg/kg 09/21/17 20:16 56-23-50.0055 1
Chlorobenzene ND mg/kg 09/21/17 20:16 108-90-70.0055 1
Chloroethane ND mg/kg 09/21/17 20:16 75-00-30.011 1
Chloroform ND mg/kg 09/21/17 20:16 67-66-30.0055 1
Chloromethane ND mg/kg 09/21/17 20:16 74-87-30.011 1
2-Chlorotoluene ND mg/kg 09/21/17 20:16 95-49-80.0055 1
4-Chlorotoluene ND mg/kg 09/21/17 20:16 106-43-40.0055 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/21/17 20:16 96-12-80.0055 1
Dibromochloromethane ND mg/kg 09/21/17 20:16 124-48-10.0055 1
1,2-Dibromoethane (EDB)ND mg/kg 09/21/17 20:16 106-93-40.0055 1
Dibromomethane ND mg/kg 09/21/17 20:16 74-95-30.0055 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 20:16 95-50-10.0055 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 20:16 541-73-10.0055 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 20:16 106-46-70.0055 1
Dichlorodifluoromethane ND mg/kg 09/21/17 20:16 75-71-80.011 1
1,1-Dichloroethane ND mg/kg 09/21/17 20:16 75-34-30.0055 1
1,2-Dichloroethane ND mg/kg 09/21/17 20:16 107-06-20.0055 1
1,1-Dichloroethene ND mg/kg 09/21/17 20:16 75-35-40.0055 1
cis-1,2-Dichloroethene ND mg/kg 09/21/17 20:16 156-59-20.0055 1
trans-1,2-Dichloroethene ND mg/kg 09/21/17 20:16 156-60-50.0055 1
1,2-Dichloropropane ND mg/kg 09/21/17 20:16 78-87-50.0055 1
1,3-Dichloropropane ND mg/kg 09/21/17 20:16 142-28-90.0055 1
2,2-Dichloropropane ND mg/kg 09/21/17 20:16 594-20-70.0055 1
1,1-Dichloropropene ND mg/kg 09/21/17 20:16 563-58-60.0055 1
cis-1,3-Dichloropropene ND mg/kg 09/21/17 20:16 10061-01-50.0055 1
trans-1,3-Dichloropropene ND mg/kg 09/21/17 20:16 10061-02-60.0055 1
Diisopropyl ether ND mg/kg 09/21/17 20:16 108-20-30.0055 1
Ethylbenzene 0.014 mg/kg 09/21/17 20:16 100-41-40.0055 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 20:16 87-68-30.0055 1
2-Hexanone ND mg/kg 09/21/17 20:16 591-78-60.055 1
Isopropylbenzene (Cumene)ND mg/kg 09/21/17 20:16 98-82-80.0055 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-1C Lab ID:92355949003 Collected:09/18/17 18:55 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND mg/kg 09/21/17 20:16 99-87-60.0055 1
Methylene Chloride ND mg/kg 09/21/17 20:16 75-09-20.022 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/21/17 20:16 108-10-10.055 1
Methyl-tert-butyl ether ND mg/kg 09/21/17 20:16 1634-04-40.0055 1
Naphthalene 0.087 mg/kg 09/21/17 20:16 91-20-30.0055 1
n-Propylbenzene ND mg/kg 09/21/17 20:16 103-65-10.0055 1
Styrene ND mg/kg 09/21/17 20:16 100-42-50.0055 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/21/17 20:16 630-20-60.0055 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/21/17 20:16 79-34-50.0055 1
Tetrachloroethene ND mg/kg 09/21/17 20:16 127-18-40.0055 1
Toluene ND mg/kg 09/21/17 20:16 108-88-30.0055 1
1,2,3-Trichlorobenzene ND mg/kg 09/21/17 20:16 87-61-60.0055 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 20:16 120-82-10.0055 1
1,1,1-Trichloroethane ND mg/kg 09/21/17 20:16 71-55-60.0055 1
1,1,2-Trichloroethane ND mg/kg 09/21/17 20:16 79-00-50.0055 1
Trichloroethene ND mg/kg 09/21/17 20:16 79-01-60.0055 1
Trichlorofluoromethane ND mg/kg 09/21/17 20:16 75-69-40.0055 1
1,2,3-Trichloropropane ND mg/kg 09/21/17 20:16 96-18-40.0055 1
1,2,4-Trimethylbenzene 0.13 mg/kg 09/21/17 20:16 95-63-60.0055 1
1,3,5-Trimethylbenzene 0.032 mg/kg 09/21/17 20:16 108-67-80.0055 1
Vinyl acetate ND mg/kg 09/21/17 20:16 108-05-40.055 1
Vinyl chloride ND mg/kg 09/21/17 20:16 75-01-40.011 1
Xylene (Total)0.17 mg/kg 09/21/17 20:16 1330-20-70.011 1
m&p-Xylene 0.16 mg/kg 09/21/17 20:16 179601-23-10.011 1
o-Xylene 0.011 mg/kg 09/21/17 20:16 95-47-60.0055 1
Surrogates
Toluene-d8 (S)97 %09/21/17 20:16 2037-26-570-130 1
4-Bromofluorobenzene (S)102 %09/21/17 20:16 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %09/21/17 20:16 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.5 %09/21/17 11:090.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-2A Lab ID:92355949004 Collected:09/18/17 18:00 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/21/17 17:59 N209/21/17 08:0513.4 1
Aliphatic (C19-C36)ND mg/kg 09/21/17 17:59 N209/21/17 08:0513.4 1
Aromatic (C11-C22)ND mg/kg 09/21/17 17:59 N209/21/17 08:0513.4 1
Surrogates
Nonatriacontane (S)57 %09/21/17 17:59 7194-86-709/21/17 08:0540-140 1
o-Terphenyl (S)74 %09/21/17 17:59 84-15-109/21/17 08:0540-140 1
2-Fluorobiphenyl (S)97 %09/21/17 17:59 321-60-809/21/17 08:0540-140 1
2-Bromonaphthalene (S)91 %09/21/17 17:59 580-13-209/21/17 08:0540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/21/17 17:02 N209/21/17 10:453.3 1
Aliphatic (C09-C12)ND mg/kg 09/21/17 17:02 N209/21/17 10:453.3 1
Aromatic (C09-C10)ND mg/kg 09/21/17 17:02 N209/21/17 10:453.3 1
Surrogates
4-Bromofluorobenzene (FID) (S)100 %09/21/17 17:02 460-00-409/21/17 10:4570-130 1
4-Bromofluorobenzene (PID) (S)95 %09/21/17 17:02 460-00-409/21/17 10:4570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/25/17 13:29 83-32-909/20/17 18:124.4 10
Acenaphthylene ND mg/kg 09/25/17 13:29 208-96-809/20/17 18:124.4 10
Aniline ND mg/kg 09/25/17 13:29 62-53-309/20/17 18:124.4 10
Anthracene ND mg/kg 09/25/17 13:29 120-12-709/20/17 18:124.4 10
Benzo(a)anthracene ND mg/kg 09/25/17 13:29 56-55-309/20/17 18:124.4 10
Benzo(a)pyrene ND mg/kg 09/25/17 13:29 50-32-809/20/17 18:124.4 10
Benzo(b)fluoranthene ND mg/kg 09/25/17 13:29 205-99-209/20/17 18:124.4 10
Benzo(g,h,i)perylene ND mg/kg 09/25/17 13:29 191-24-209/20/17 18:124.4 10
Benzo(k)fluoranthene ND mg/kg 09/25/17 13:29 207-08-909/20/17 18:124.4 10
Benzoic Acid ND mg/kg 09/25/17 13:29 65-85-009/20/17 18:1221.8 10
Benzyl alcohol ND mg/kg 09/25/17 13:29 100-51-609/20/17 18:128.7 10
4-Bromophenylphenyl ether ND mg/kg 09/25/17 13:29 101-55-309/20/17 18:124.4 10
Butylbenzylphthalate ND mg/kg 09/25/17 13:29 85-68-709/20/17 18:124.4 10
4-Chloro-3-methylphenol ND mg/kg 09/25/17 13:29 59-50-709/20/17 18:128.7 10
4-Chloroaniline ND mg/kg 09/25/17 13:29 106-47-809/20/17 18:1221.8 10
bis(2-Chloroethoxy)methane ND mg/kg 09/25/17 13:29 111-91-109/20/17 18:124.4 10
bis(2-Chloroethyl) ether ND mg/kg 09/25/17 13:29 111-44-409/20/17 18:124.4 10
2-Chloronaphthalene ND mg/kg 09/25/17 13:29 91-58-709/20/17 18:124.4 10
2-Chlorophenol ND mg/kg 09/25/17 13:29 95-57-809/20/17 18:124.4 10
4-Chlorophenylphenyl ether ND mg/kg 09/25/17 13:29 7005-72-309/20/17 18:124.4 10
Chrysene ND mg/kg 09/25/17 13:29 218-01-909/20/17 18:124.4 10
Dibenz(a,h)anthracene ND mg/kg 09/25/17 13:29 53-70-309/20/17 18:124.4 10
Dibenzofuran ND mg/kg 09/25/17 13:29 132-64-909/20/17 18:124.4 10
1,2-Dichlorobenzene ND mg/kg 09/25/17 13:29 95-50-109/20/17 18:124.4 10
1,3-Dichlorobenzene ND mg/kg 09/25/17 13:29 541-73-109/20/17 18:124.4 10
1,4-Dichlorobenzene ND mg/kg 09/25/17 13:29 106-46-709/20/17 18:124.4 10
3,3'-Dichlorobenzidine ND mg/kg 09/25/17 13:29 91-94-109/20/17 18:1221.8 10
2,4-Dichlorophenol ND mg/kg 09/25/17 13:29 120-83-209/20/17 18:124.4 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-2A Lab ID:92355949004 Collected:09/18/17 18:00 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/25/17 13:29 84-66-209/20/17 18:124.4 10
2,4-Dimethylphenol ND mg/kg 09/25/17 13:29 105-67-909/20/17 18:124.4 10
Dimethylphthalate ND mg/kg 09/25/17 13:29 131-11-309/20/17 18:124.4 10
Di-n-butylphthalate ND mg/kg 09/25/17 13:29 84-74-209/20/17 18:124.4 10
4,6-Dinitro-2-methylphenol ND mg/kg 09/25/17 13:29 534-52-109/20/17 18:128.7 10
2,4-Dinitrophenol ND mg/kg 09/25/17 13:29 51-28-509/20/17 18:1221.8 10
2,4-Dinitrotoluene ND mg/kg 09/25/17 13:29 121-14-209/20/17 18:124.4 10
2,6-Dinitrotoluene ND mg/kg 09/25/17 13:29 606-20-209/20/17 18:124.4 10
Di-n-octylphthalate ND mg/kg 09/25/17 13:29 117-84-009/20/17 18:124.4 10
bis(2-Ethylhexyl)phthalate ND mg/kg 09/25/17 13:29 117-81-709/20/17 18:124.4 10
Fluoranthene ND mg/kg 09/25/17 13:29 206-44-009/20/17 18:124.4 10
Fluorene ND mg/kg 09/25/17 13:29 86-73-709/20/17 18:124.4 10
Hexachloro-1,3-butadiene ND mg/kg 09/25/17 13:29 87-68-309/20/17 18:124.4 10
Hexachlorobenzene ND mg/kg 09/25/17 13:29 118-74-109/20/17 18:124.4 10
Hexachlorocyclopentadiene ND mg/kg 09/25/17 13:29 77-47-409/20/17 18:124.4 10
Hexachloroethane ND mg/kg 09/25/17 13:29 67-72-109/20/17 18:124.4 10
Indeno(1,2,3-cd)pyrene ND mg/kg 09/25/17 13:29 193-39-509/20/17 18:124.4 10
Isophorone ND mg/kg 09/25/17 13:29 78-59-109/20/17 18:124.4 10
1-Methylnaphthalene ND mg/kg 09/25/17 13:29 90-12-009/20/17 18:124.4 10
2-Methylnaphthalene ND mg/kg 09/25/17 13:29 91-57-609/20/17 18:124.4 10
2-Methylphenol(o-Cresol)ND mg/kg 09/25/17 13:29 95-48-709/20/17 18:124.4 10
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/25/17 13:29 15831-10-409/20/17 18:124.4 10
Naphthalene ND mg/kg 09/25/17 13:29 91-20-309/20/17 18:124.4 10
2-Nitroaniline ND mg/kg 09/25/17 13:29 88-74-409/20/17 18:1221.8 10
3-Nitroaniline ND mg/kg 09/25/17 13:29 99-09-209/20/17 18:1221.8 10
4-Nitroaniline ND mg/kg 09/25/17 13:29 100-01-609/20/17 18:128.7 10
Nitrobenzene ND mg/kg 09/25/17 13:29 98-95-309/20/17 18:124.4 10
2-Nitrophenol ND mg/kg 09/25/17 13:29 88-75-509/20/17 18:124.4 10
4-Nitrophenol ND mg/kg 09/25/17 13:29 100-02-709/20/17 18:1221.8 10
N-Nitrosodimethylamine ND mg/kg 09/25/17 13:29 62-75-909/20/17 18:124.4 10
N-Nitroso-di-n-propylamine ND mg/kg 09/25/17 13:29 621-64-709/20/17 18:124.4 10
N-Nitrosodiphenylamine ND mg/kg 09/25/17 13:29 86-30-609/20/17 18:124.4 10
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/25/17 13:29 108-60-109/20/17 18:124.4 10
Pentachlorophenol ND mg/kg 09/25/17 13:29 87-86-509/20/17 18:1221.8 10
Phenanthrene ND mg/kg 09/25/17 13:29 85-01-809/20/17 18:124.4 10
Phenol ND mg/kg 09/25/17 13:29 108-95-209/20/17 18:124.4 10
Pyrene ND mg/kg 09/25/17 13:29 129-00-009/20/17 18:124.4 10
1,2,4-Trichlorobenzene ND mg/kg 09/25/17 13:29 120-82-109/20/17 18:124.4 10
2,4,5-Trichlorophenol ND mg/kg 09/25/17 13:29 95-95-409/20/17 18:124.4 10
2,4,6-Trichlorophenol ND mg/kg 09/25/17 13:29 88-06-209/20/17 18:124.4 10
Surrogates
Nitrobenzene-d5 (S)0 %09/25/17 13:29 4165-60-0 D3,S409/20/17 18:1223-110 10
2-Fluorobiphenyl (S)0 %09/25/17 13:29 321-60-8 S409/20/17 18:1230-110 10
Terphenyl-d14 (S)0 %09/25/17 13:29 1718-51-0 S409/20/17 18:1228-110 10
Phenol-d6 (S)0 %09/25/17 13:29 13127-88-3 S409/20/17 18:1222-110 10
2-Fluorophenol (S)0 %09/25/17 13:29 367-12-4 S409/20/17 18:1213-110 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-2A Lab ID:92355949004 Collected:09/18/17 18:00 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)0 %09/25/17 13:29 118-79-6 S409/20/17 18:1227-110 10
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/21/17 20:36 67-64-10.10 1
Benzene ND mg/kg 09/21/17 20:36 71-43-20.0051 1
Bromobenzene ND mg/kg 09/21/17 20:36 108-86-10.0051 1
Bromochloromethane ND mg/kg 09/21/17 20:36 74-97-50.0051 1
Bromodichloromethane ND mg/kg 09/21/17 20:36 75-27-40.0051 1
Bromoform ND mg/kg 09/21/17 20:36 75-25-20.0051 1
Bromomethane ND mg/kg 09/21/17 20:36 74-83-90.010 1
2-Butanone (MEK)ND mg/kg 09/21/17 20:36 78-93-30.10 1
n-Butylbenzene ND mg/kg 09/21/17 20:36 104-51-80.0051 1
sec-Butylbenzene ND mg/kg 09/21/17 20:36 135-98-80.0051 1
tert-Butylbenzene ND mg/kg 09/21/17 20:36 98-06-60.0051 1
Carbon tetrachloride ND mg/kg 09/21/17 20:36 56-23-50.0051 1
Chlorobenzene ND mg/kg 09/21/17 20:36 108-90-70.0051 1
Chloroethane ND mg/kg 09/21/17 20:36 75-00-30.010 1
Chloroform ND mg/kg 09/21/17 20:36 67-66-30.0051 1
Chloromethane ND mg/kg 09/21/17 20:36 74-87-30.010 1
2-Chlorotoluene ND mg/kg 09/21/17 20:36 95-49-80.0051 1
4-Chlorotoluene ND mg/kg 09/21/17 20:36 106-43-40.0051 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/21/17 20:36 96-12-80.0051 1
Dibromochloromethane ND mg/kg 09/21/17 20:36 124-48-10.0051 1
1,2-Dibromoethane (EDB)ND mg/kg 09/21/17 20:36 106-93-40.0051 1
Dibromomethane ND mg/kg 09/21/17 20:36 74-95-30.0051 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 20:36 95-50-10.0051 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 20:36 541-73-10.0051 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 20:36 106-46-70.0051 1
Dichlorodifluoromethane ND mg/kg 09/21/17 20:36 75-71-80.010 1
1,1-Dichloroethane ND mg/kg 09/21/17 20:36 75-34-30.0051 1
1,2-Dichloroethane ND mg/kg 09/21/17 20:36 107-06-20.0051 1
1,1-Dichloroethene ND mg/kg 09/21/17 20:36 75-35-40.0051 1
cis-1,2-Dichloroethene ND mg/kg 09/21/17 20:36 156-59-20.0051 1
trans-1,2-Dichloroethene ND mg/kg 09/21/17 20:36 156-60-50.0051 1
1,2-Dichloropropane ND mg/kg 09/21/17 20:36 78-87-50.0051 1
1,3-Dichloropropane ND mg/kg 09/21/17 20:36 142-28-90.0051 1
2,2-Dichloropropane ND mg/kg 09/21/17 20:36 594-20-70.0051 1
1,1-Dichloropropene ND mg/kg 09/21/17 20:36 563-58-60.0051 1
cis-1,3-Dichloropropene ND mg/kg 09/21/17 20:36 10061-01-50.0051 1
trans-1,3-Dichloropropene ND mg/kg 09/21/17 20:36 10061-02-60.0051 1
Diisopropyl ether ND mg/kg 09/21/17 20:36 108-20-30.0051 1
Ethylbenzene ND mg/kg 09/21/17 20:36 100-41-40.0051 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 20:36 87-68-30.0051 1
2-Hexanone ND mg/kg 09/21/17 20:36 591-78-60.051 1
Isopropylbenzene (Cumene)ND mg/kg 09/21/17 20:36 98-82-80.0051 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-2A Lab ID:92355949004 Collected:09/18/17 18:00 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND mg/kg 09/21/17 20:36 99-87-60.0051 1
Methylene Chloride ND mg/kg 09/21/17 20:36 75-09-20.021 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/21/17 20:36 108-10-10.051 1
Methyl-tert-butyl ether ND mg/kg 09/21/17 20:36 1634-04-40.0051 1
Naphthalene ND mg/kg 09/21/17 20:36 91-20-30.0051 1
n-Propylbenzene ND mg/kg 09/21/17 20:36 103-65-10.0051 1
Styrene ND mg/kg 09/21/17 20:36 100-42-50.0051 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/21/17 20:36 630-20-60.0051 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/21/17 20:36 79-34-50.0051 1
Tetrachloroethene ND mg/kg 09/21/17 20:36 127-18-40.0051 1
Toluene ND mg/kg 09/21/17 20:36 108-88-30.0051 1
1,2,3-Trichlorobenzene ND mg/kg 09/21/17 20:36 87-61-60.0051 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 20:36 120-82-10.0051 1
1,1,1-Trichloroethane ND mg/kg 09/21/17 20:36 71-55-60.0051 1
1,1,2-Trichloroethane ND mg/kg 09/21/17 20:36 79-00-50.0051 1
Trichloroethene ND mg/kg 09/21/17 20:36 79-01-60.0051 1
Trichlorofluoromethane ND mg/kg 09/21/17 20:36 75-69-40.0051 1
1,2,3-Trichloropropane ND mg/kg 09/21/17 20:36 96-18-40.0051 1
1,2,4-Trimethylbenzene ND mg/kg 09/21/17 20:36 95-63-60.0051 1
1,3,5-Trimethylbenzene ND mg/kg 09/21/17 20:36 108-67-80.0051 1
Vinyl acetate ND mg/kg 09/21/17 20:36 108-05-40.051 1
Vinyl chloride ND mg/kg 09/21/17 20:36 75-01-40.010 1
Xylene (Total)ND mg/kg 09/21/17 20:36 1330-20-70.010 1
m&p-Xylene ND mg/kg 09/21/17 20:36 179601-23-10.010 1
o-Xylene ND mg/kg 09/21/17 20:36 95-47-60.0051 1
Surrogates
Toluene-d8 (S)95 %09/21/17 20:36 2037-26-570-130 1
4-Bromofluorobenzene (S)97 %09/21/17 20:36 460-00-470-130 1
1,2-Dichloroethane-d4 (S)104 %09/21/17 20:36 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 25.2 %09/21/17 11:090.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-2B Lab ID:92355949005 Collected:09/18/17 18:10 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/21/17 18:26 N209/21/17 08:0513.8 1
Aliphatic (C19-C36)ND mg/kg 09/21/17 18:26 N209/21/17 08:0513.8 1
Aromatic (C11-C22)ND mg/kg 09/21/17 18:26 N209/21/17 08:0513.8 1
Surrogates
Nonatriacontane (S)55 %09/21/17 18:26 7194-86-709/21/17 08:0540-140 1
o-Terphenyl (S)67 %09/21/17 18:26 84-15-109/21/17 08:0540-140 1
2-Fluorobiphenyl (S)94 %09/21/17 18:26 321-60-809/21/17 08:0540-140 1
2-Bromonaphthalene (S)94 %09/21/17 18:26 580-13-209/21/17 08:0540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/21/17 17:30 N209/21/17 10:454.1 1
Aliphatic (C09-C12)ND mg/kg 09/21/17 17:30 N209/21/17 10:454.1 1
Aromatic (C09-C10)ND mg/kg 09/21/17 17:30 N209/21/17 10:454.1 1
Surrogates
4-Bromofluorobenzene (FID) (S)103 %09/21/17 17:30 460-00-409/21/17 10:4570-130 1
4-Bromofluorobenzene (PID) (S)97 %09/21/17 17:30 460-00-409/21/17 10:4570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/21/17 16:42 83-32-909/20/17 18:120.45 1
Acenaphthylene ND mg/kg 09/21/17 16:42 208-96-809/20/17 18:120.45 1
Aniline ND mg/kg 09/21/17 16:42 62-53-309/20/17 18:120.45 1
Anthracene ND mg/kg 09/21/17 16:42 120-12-709/20/17 18:120.45 1
Benzo(a)anthracene ND mg/kg 09/21/17 16:42 56-55-309/20/17 18:120.45 1
Benzo(a)pyrene ND mg/kg 09/21/17 16:42 50-32-809/20/17 18:120.45 1
Benzo(b)fluoranthene ND mg/kg 09/21/17 16:42 205-99-209/20/17 18:120.45 1
Benzo(g,h,i)perylene ND mg/kg 09/21/17 16:42 191-24-209/20/17 18:120.45 1
Benzo(k)fluoranthene ND mg/kg 09/21/17 16:42 207-08-909/20/17 18:120.45 1
Benzoic Acid ND mg/kg 09/21/17 16:42 65-85-009/20/17 18:122.3 1
Benzyl alcohol ND mg/kg 09/21/17 16:42 100-51-609/20/17 18:120.90 1
4-Bromophenylphenyl ether ND mg/kg 09/21/17 16:42 101-55-309/20/17 18:120.45 1
Butylbenzylphthalate ND mg/kg 09/21/17 16:42 85-68-709/20/17 18:120.45 1
4-Chloro-3-methylphenol ND mg/kg 09/21/17 16:42 59-50-709/20/17 18:120.90 1
4-Chloroaniline ND mg/kg 09/21/17 16:42 106-47-809/20/17 18:122.3 1
bis(2-Chloroethoxy)methane ND mg/kg 09/21/17 16:42 111-91-109/20/17 18:120.45 1
bis(2-Chloroethyl) ether ND mg/kg 09/21/17 16:42 111-44-409/20/17 18:120.45 1
2-Chloronaphthalene ND mg/kg 09/21/17 16:42 91-58-709/20/17 18:120.45 1
2-Chlorophenol ND mg/kg 09/21/17 16:42 95-57-809/20/17 18:120.45 1
4-Chlorophenylphenyl ether ND mg/kg 09/21/17 16:42 7005-72-309/20/17 18:120.45 1
Chrysene ND mg/kg 09/21/17 16:42 218-01-909/20/17 18:120.45 1
Dibenz(a,h)anthracene ND mg/kg 09/21/17 16:42 53-70-309/20/17 18:120.45 1
Dibenzofuran ND mg/kg 09/21/17 16:42 132-64-909/20/17 18:120.45 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 16:42 95-50-109/20/17 18:120.45 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 16:42 541-73-109/20/17 18:120.45 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 16:42 106-46-709/20/17 18:120.45 1
3,3'-Dichlorobenzidine ND mg/kg 09/21/17 16:42 91-94-109/20/17 18:122.3 1
2,4-Dichlorophenol ND mg/kg 09/21/17 16:42 120-83-209/20/17 18:120.45 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-2B Lab ID:92355949005 Collected:09/18/17 18:10 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/21/17 16:42 84-66-209/20/17 18:120.45 1
2,4-Dimethylphenol ND mg/kg 09/21/17 16:42 105-67-909/20/17 18:120.45 1
Dimethylphthalate ND mg/kg 09/21/17 16:42 131-11-309/20/17 18:120.45 1
Di-n-butylphthalate ND mg/kg 09/21/17 16:42 84-74-209/20/17 18:120.45 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/21/17 16:42 534-52-109/20/17 18:120.90 1
2,4-Dinitrophenol ND mg/kg 09/21/17 16:42 51-28-509/20/17 18:122.3 1
2,4-Dinitrotoluene ND mg/kg 09/21/17 16:42 121-14-209/20/17 18:120.45 1
2,6-Dinitrotoluene ND mg/kg 09/21/17 16:42 606-20-209/20/17 18:120.45 1
Di-n-octylphthalate ND mg/kg 09/21/17 16:42 117-84-009/20/17 18:120.45 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/21/17 16:42 117-81-709/20/17 18:120.45 1
Fluoranthene ND mg/kg 09/21/17 16:42 206-44-009/20/17 18:120.45 1
Fluorene ND mg/kg 09/21/17 16:42 86-73-709/20/17 18:120.45 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 16:42 87-68-309/20/17 18:120.45 1
Hexachlorobenzene ND mg/kg 09/21/17 16:42 118-74-109/20/17 18:120.45 1
Hexachlorocyclopentadiene ND mg/kg 09/21/17 16:42 77-47-409/20/17 18:120.45 1
Hexachloroethane ND mg/kg 09/21/17 16:42 67-72-109/20/17 18:120.45 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/21/17 16:42 193-39-509/20/17 18:120.45 1
Isophorone ND mg/kg 09/21/17 16:42 78-59-109/20/17 18:120.45 1
1-Methylnaphthalene ND mg/kg 09/21/17 16:42 90-12-009/20/17 18:120.45 1
2-Methylnaphthalene ND mg/kg 09/21/17 16:42 91-57-609/20/17 18:120.45 1
2-Methylphenol(o-Cresol)ND mg/kg 09/21/17 16:42 95-48-709/20/17 18:120.45 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/21/17 16:42 15831-10-409/20/17 18:120.45 1
Naphthalene ND mg/kg 09/21/17 16:42 91-20-309/20/17 18:120.45 1
2-Nitroaniline ND mg/kg 09/21/17 16:42 88-74-409/20/17 18:122.3 1
3-Nitroaniline ND mg/kg 09/21/17 16:42 99-09-209/20/17 18:122.3 1
4-Nitroaniline ND mg/kg 09/21/17 16:42 100-01-609/20/17 18:120.90 1
Nitrobenzene ND mg/kg 09/21/17 16:42 98-95-309/20/17 18:120.45 1
2-Nitrophenol ND mg/kg 09/21/17 16:42 88-75-509/20/17 18:120.45 1
4-Nitrophenol ND mg/kg 09/21/17 16:42 100-02-709/20/17 18:122.3 1
N-Nitrosodimethylamine ND mg/kg 09/21/17 16:42 62-75-909/20/17 18:120.45 1
N-Nitroso-di-n-propylamine ND mg/kg 09/21/17 16:42 621-64-709/20/17 18:120.45 1
N-Nitrosodiphenylamine ND mg/kg 09/21/17 16:42 86-30-609/20/17 18:120.45 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/21/17 16:42 108-60-109/20/17 18:120.45 1
Pentachlorophenol ND mg/kg 09/21/17 16:42 87-86-509/20/17 18:122.3 1
Phenanthrene ND mg/kg 09/21/17 16:42 85-01-809/20/17 18:120.45 1
Phenol ND mg/kg 09/21/17 16:42 108-95-209/20/17 18:120.45 1
Pyrene ND mg/kg 09/21/17 16:42 129-00-009/20/17 18:120.45 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 16:42 120-82-109/20/17 18:120.45 1
2,4,5-Trichlorophenol ND mg/kg 09/21/17 16:42 95-95-409/20/17 18:120.45 1
2,4,6-Trichlorophenol ND mg/kg 09/21/17 16:42 88-06-209/20/17 18:120.45 1
Surrogates
Nitrobenzene-d5 (S)56 %09/21/17 16:42 4165-60-009/20/17 18:1223-110 1
2-Fluorobiphenyl (S)44 %09/21/17 16:42 321-60-809/20/17 18:1230-110 1
Terphenyl-d14 (S)59 %09/21/17 16:42 1718-51-009/20/17 18:1228-110 1
Phenol-d6 (S)47 %09/21/17 16:42 13127-88-309/20/17 18:1222-110 1
2-Fluorophenol (S)51 %09/21/17 16:42 367-12-409/20/17 18:1213-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-2B Lab ID:92355949005 Collected:09/18/17 18:10 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)62 %09/21/17 16:42 118-79-609/20/17 18:1227-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/21/17 20:56 67-64-10.10 1
Benzene ND mg/kg 09/21/17 20:56 71-43-20.0050 1
Bromobenzene ND mg/kg 09/21/17 20:56 108-86-10.0050 1
Bromochloromethane ND mg/kg 09/21/17 20:56 74-97-50.0050 1
Bromodichloromethane ND mg/kg 09/21/17 20:56 75-27-40.0050 1
Bromoform ND mg/kg 09/21/17 20:56 75-25-20.0050 1
Bromomethane ND mg/kg 09/21/17 20:56 74-83-90.010 1
2-Butanone (MEK)ND mg/kg 09/21/17 20:56 78-93-30.10 1
n-Butylbenzene ND mg/kg 09/21/17 20:56 104-51-80.0050 1
sec-Butylbenzene ND mg/kg 09/21/17 20:56 135-98-80.0050 1
tert-Butylbenzene ND mg/kg 09/21/17 20:56 98-06-60.0050 1
Carbon tetrachloride ND mg/kg 09/21/17 20:56 56-23-50.0050 1
Chlorobenzene ND mg/kg 09/21/17 20:56 108-90-70.0050 1
Chloroethane ND mg/kg 09/21/17 20:56 75-00-30.010 1
Chloroform ND mg/kg 09/21/17 20:56 67-66-30.0050 1
Chloromethane ND mg/kg 09/21/17 20:56 74-87-30.010 1
2-Chlorotoluene ND mg/kg 09/21/17 20:56 95-49-80.0050 1
4-Chlorotoluene ND mg/kg 09/21/17 20:56 106-43-40.0050 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/21/17 20:56 96-12-80.0050 1
Dibromochloromethane ND mg/kg 09/21/17 20:56 124-48-10.0050 1
1,2-Dibromoethane (EDB)ND mg/kg 09/21/17 20:56 106-93-40.0050 1
Dibromomethane ND mg/kg 09/21/17 20:56 74-95-30.0050 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 20:56 95-50-10.0050 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 20:56 541-73-10.0050 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 20:56 106-46-70.0050 1
Dichlorodifluoromethane ND mg/kg 09/21/17 20:56 75-71-80.010 1
1,1-Dichloroethane ND mg/kg 09/21/17 20:56 75-34-30.0050 1
1,2-Dichloroethane ND mg/kg 09/21/17 20:56 107-06-20.0050 1
1,1-Dichloroethene ND mg/kg 09/21/17 20:56 75-35-40.0050 1
cis-1,2-Dichloroethene ND mg/kg 09/21/17 20:56 156-59-20.0050 1
trans-1,2-Dichloroethene ND mg/kg 09/21/17 20:56 156-60-50.0050 1
1,2-Dichloropropane ND mg/kg 09/21/17 20:56 78-87-50.0050 1
1,3-Dichloropropane ND mg/kg 09/21/17 20:56 142-28-90.0050 1
2,2-Dichloropropane ND mg/kg 09/21/17 20:56 594-20-70.0050 1
1,1-Dichloropropene ND mg/kg 09/21/17 20:56 563-58-60.0050 1
cis-1,3-Dichloropropene ND mg/kg 09/21/17 20:56 10061-01-50.0050 1
trans-1,3-Dichloropropene ND mg/kg 09/21/17 20:56 10061-02-60.0050 1
Diisopropyl ether ND mg/kg 09/21/17 20:56 108-20-30.0050 1
Ethylbenzene ND mg/kg 09/21/17 20:56 100-41-40.0050 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 20:56 87-68-30.0050 1
2-Hexanone ND mg/kg 09/21/17 20:56 591-78-60.050 1
Isopropylbenzene (Cumene)ND mg/kg 09/21/17 20:56 98-82-80.0050 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-2B Lab ID:92355949005 Collected:09/18/17 18:10 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND mg/kg 09/21/17 20:56 99-87-60.0050 1
Methylene Chloride ND mg/kg 09/21/17 20:56 75-09-20.020 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/21/17 20:56 108-10-10.050 1
Methyl-tert-butyl ether 0.0066 mg/kg 09/21/17 20:56 1634-04-40.0050 1
Naphthalene ND mg/kg 09/21/17 20:56 91-20-30.0050 1
n-Propylbenzene ND mg/kg 09/21/17 20:56 103-65-10.0050 1
Styrene ND mg/kg 09/21/17 20:56 100-42-50.0050 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/21/17 20:56 630-20-60.0050 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/21/17 20:56 79-34-50.0050 1
Tetrachloroethene ND mg/kg 09/21/17 20:56 127-18-40.0050 1
Toluene ND mg/kg 09/21/17 20:56 108-88-30.0050 1
1,2,3-Trichlorobenzene ND mg/kg 09/21/17 20:56 87-61-60.0050 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 20:56 120-82-10.0050 1
1,1,1-Trichloroethane ND mg/kg 09/21/17 20:56 71-55-60.0050 1
1,1,2-Trichloroethane ND mg/kg 09/21/17 20:56 79-00-50.0050 1
Trichloroethene ND mg/kg 09/21/17 20:56 79-01-60.0050 1
Trichlorofluoromethane ND mg/kg 09/21/17 20:56 75-69-40.0050 1
1,2,3-Trichloropropane ND mg/kg 09/21/17 20:56 96-18-40.0050 1
1,2,4-Trimethylbenzene 0.015 mg/kg 09/21/17 20:56 95-63-60.0050 1
1,3,5-Trimethylbenzene ND mg/kg 09/21/17 20:56 108-67-80.0050 1
Vinyl acetate ND mg/kg 09/21/17 20:56 108-05-40.050 1
Vinyl chloride ND mg/kg 09/21/17 20:56 75-01-40.010 1
Xylene (Total)ND mg/kg 09/21/17 20:56 1330-20-70.010 1
m&p-Xylene ND mg/kg 09/21/17 20:56 179601-23-10.010 1
o-Xylene ND mg/kg 09/21/17 20:56 95-47-60.0050 1
Surrogates
Toluene-d8 (S)97 %09/21/17 20:56 2037-26-570-130 1
4-Bromofluorobenzene (S)99 %09/21/17 20:56 460-00-470-130 1
1,2-Dichloroethane-d4 (S)102 %09/21/17 20:56 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 27.7 %09/21/17 11:090.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-2C Lab ID:92355949006 Collected:09/18/17 18:20 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/22/17 11:12 N209/21/17 08:0512.7 1
Aliphatic (C19-C36)ND mg/kg 09/22/17 11:12 N209/21/17 08:0512.7 1
Aromatic (C11-C22)ND mg/kg 09/22/17 11:12 N209/21/17 08:0512.7 1
Surrogates
Nonatriacontane (S)54 %09/22/17 11:12 7194-86-709/21/17 08:0540-140 1
o-Terphenyl (S)82 %09/22/17 11:12 84-15-109/21/17 08:0540-140 1
2-Fluorobiphenyl (S)112 %09/22/17 11:12 321-60-809/21/17 08:0540-140 1
2-Bromonaphthalene (S)109 %09/22/17 11:12 580-13-209/21/17 08:0540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/21/17 17:58 N209/21/17 10:452.9 1
Aliphatic (C09-C12)ND mg/kg 09/21/17 17:58 N209/21/17 10:452.9 1
Aromatic (C09-C10)ND mg/kg 09/21/17 17:58 N209/21/17 10:452.9 1
Surrogates
4-Bromofluorobenzene (FID) (S)97 %09/21/17 17:58 460-00-409/21/17 10:4570-130 1
4-Bromofluorobenzene (PID) (S)92 %09/21/17 17:58 460-00-409/21/17 10:4570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/22/17 17:47 83-32-909/20/17 18:124.1 10
Acenaphthylene ND mg/kg 09/22/17 17:47 208-96-809/20/17 18:124.1 10
Aniline ND mg/kg 09/22/17 17:47 62-53-309/20/17 18:124.1 10
Anthracene ND mg/kg 09/22/17 17:47 120-12-709/20/17 18:124.1 10
Benzo(a)anthracene ND mg/kg 09/22/17 17:47 56-55-309/20/17 18:124.1 10
Benzo(a)pyrene ND mg/kg 09/22/17 17:47 50-32-809/20/17 18:124.1 10
Benzo(b)fluoranthene ND mg/kg 09/22/17 17:47 205-99-209/20/17 18:124.1 10
Benzo(g,h,i)perylene ND mg/kg 09/22/17 17:47 191-24-209/20/17 18:124.1 10
Benzo(k)fluoranthene ND mg/kg 09/22/17 17:47 207-08-909/20/17 18:124.1 10
Benzoic Acid ND mg/kg 09/22/17 17:47 65-85-009/20/17 18:1220.7 10
Benzyl alcohol ND mg/kg 09/22/17 17:47 100-51-609/20/17 18:128.3 10
4-Bromophenylphenyl ether ND mg/kg 09/22/17 17:47 101-55-309/20/17 18:124.1 10
Butylbenzylphthalate ND mg/kg 09/22/17 17:47 85-68-709/20/17 18:124.1 10
4-Chloro-3-methylphenol ND mg/kg 09/22/17 17:47 59-50-709/20/17 18:128.3 10
4-Chloroaniline ND mg/kg 09/22/17 17:47 106-47-809/20/17 18:1220.7 10
bis(2-Chloroethoxy)methane ND mg/kg 09/22/17 17:47 111-91-109/20/17 18:124.1 10
bis(2-Chloroethyl) ether ND mg/kg 09/22/17 17:47 111-44-409/20/17 18:124.1 10
2-Chloronaphthalene ND mg/kg 09/22/17 17:47 91-58-709/20/17 18:124.1 10
2-Chlorophenol ND mg/kg 09/22/17 17:47 95-57-809/20/17 18:124.1 10
4-Chlorophenylphenyl ether ND mg/kg 09/22/17 17:47 7005-72-309/20/17 18:124.1 10
Chrysene ND mg/kg 09/22/17 17:47 218-01-909/20/17 18:124.1 10
Dibenz(a,h)anthracene ND mg/kg 09/22/17 17:47 53-70-309/20/17 18:124.1 10
Dibenzofuran ND mg/kg 09/22/17 17:47 132-64-909/20/17 18:124.1 10
1,2-Dichlorobenzene ND mg/kg 09/22/17 17:47 95-50-109/20/17 18:124.1 10
1,3-Dichlorobenzene ND mg/kg 09/22/17 17:47 541-73-109/20/17 18:124.1 10
1,4-Dichlorobenzene ND mg/kg 09/22/17 17:47 106-46-709/20/17 18:124.1 10
3,3'-Dichlorobenzidine ND mg/kg 09/22/17 17:47 91-94-109/20/17 18:1220.7 10
2,4-Dichlorophenol ND mg/kg 09/22/17 17:47 120-83-209/20/17 18:124.1 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-2C Lab ID:92355949006 Collected:09/18/17 18:20 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/22/17 17:47 84-66-209/20/17 18:124.1 10
2,4-Dimethylphenol ND mg/kg 09/22/17 17:47 105-67-909/20/17 18:124.1 10
Dimethylphthalate ND mg/kg 09/22/17 17:47 131-11-309/20/17 18:124.1 10
Di-n-butylphthalate ND mg/kg 09/22/17 17:47 84-74-209/20/17 18:124.1 10
4,6-Dinitro-2-methylphenol ND mg/kg 09/22/17 17:47 534-52-109/20/17 18:128.3 10
2,4-Dinitrophenol ND mg/kg 09/22/17 17:47 51-28-509/20/17 18:1220.7 10
2,4-Dinitrotoluene ND mg/kg 09/22/17 17:47 121-14-209/20/17 18:124.1 10
2,6-Dinitrotoluene ND mg/kg 09/22/17 17:47 606-20-209/20/17 18:124.1 10
Di-n-octylphthalate ND mg/kg 09/22/17 17:47 117-84-009/20/17 18:124.1 10
bis(2-Ethylhexyl)phthalate ND mg/kg 09/22/17 17:47 117-81-709/20/17 18:124.1 10
Fluoranthene ND mg/kg 09/22/17 17:47 206-44-009/20/17 18:124.1 10
Fluorene ND mg/kg 09/22/17 17:47 86-73-709/20/17 18:124.1 10
Hexachloro-1,3-butadiene ND mg/kg 09/22/17 17:47 87-68-309/20/17 18:124.1 10
Hexachlorobenzene ND mg/kg 09/22/17 17:47 118-74-109/20/17 18:124.1 10
Hexachlorocyclopentadiene ND mg/kg 09/22/17 17:47 77-47-409/20/17 18:124.1 10
Hexachloroethane ND mg/kg 09/22/17 17:47 67-72-109/20/17 18:124.1 10
Indeno(1,2,3-cd)pyrene ND mg/kg 09/22/17 17:47 193-39-509/20/17 18:124.1 10
Isophorone ND mg/kg 09/22/17 17:47 78-59-109/20/17 18:124.1 10
1-Methylnaphthalene ND mg/kg 09/22/17 17:47 90-12-009/20/17 18:124.1 10
2-Methylnaphthalene ND mg/kg 09/22/17 17:47 91-57-609/20/17 18:124.1 10
2-Methylphenol(o-Cresol)ND mg/kg 09/22/17 17:47 95-48-709/20/17 18:124.1 10
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/22/17 17:47 15831-10-409/20/17 18:124.1 10
Naphthalene ND mg/kg 09/22/17 17:47 91-20-309/20/17 18:124.1 10
2-Nitroaniline ND mg/kg 09/22/17 17:47 88-74-409/20/17 18:1220.7 10
3-Nitroaniline ND mg/kg 09/22/17 17:47 99-09-209/20/17 18:1220.7 10
4-Nitroaniline ND mg/kg 09/22/17 17:47 100-01-609/20/17 18:128.3 10
Nitrobenzene ND mg/kg 09/22/17 17:47 98-95-309/20/17 18:124.1 10
2-Nitrophenol ND mg/kg 09/22/17 17:47 88-75-509/20/17 18:124.1 10
4-Nitrophenol ND mg/kg 09/22/17 17:47 100-02-709/20/17 18:1220.7 10
N-Nitrosodimethylamine ND mg/kg 09/22/17 17:47 62-75-909/20/17 18:124.1 10
N-Nitroso-di-n-propylamine ND mg/kg 09/22/17 17:47 621-64-709/20/17 18:124.1 10
N-Nitrosodiphenylamine ND mg/kg 09/22/17 17:47 86-30-609/20/17 18:124.1 10
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/22/17 17:47 108-60-109/20/17 18:124.1 10
Pentachlorophenol ND mg/kg 09/22/17 17:47 87-86-509/20/17 18:1220.7 10
Phenanthrene ND mg/kg 09/22/17 17:47 85-01-809/20/17 18:124.1 10
Phenol ND mg/kg 09/22/17 17:47 108-95-209/20/17 18:124.1 10
Pyrene ND mg/kg 09/22/17 17:47 129-00-009/20/17 18:124.1 10
1,2,4-Trichlorobenzene ND mg/kg 09/22/17 17:47 120-82-109/20/17 18:124.1 10
2,4,5-Trichlorophenol ND mg/kg 09/22/17 17:47 95-95-409/20/17 18:124.1 10
2,4,6-Trichlorophenol ND mg/kg 09/22/17 17:47 88-06-209/20/17 18:124.1 10
Surrogates
Nitrobenzene-d5 (S)0 %09/22/17 17:47 4165-60-0 D3,S409/20/17 18:1223-110 10
2-Fluorobiphenyl (S)0 %09/22/17 17:47 321-60-8 S409/20/17 18:1230-110 10
Terphenyl-d14 (S)0 %09/22/17 17:47 1718-51-0 S409/20/17 18:1228-110 10
Phenol-d6 (S)0 %09/22/17 17:47 13127-88-3 S409/20/17 18:1222-110 10
2-Fluorophenol (S)0 %09/22/17 17:47 367-12-4 S409/20/17 18:1213-110 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-2C Lab ID:92355949006 Collected:09/18/17 18:20 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)0 %09/22/17 17:47 118-79-6 S409/20/17 18:1227-110 10
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/21/17 21:15 67-64-10.084 1
Benzene ND mg/kg 09/21/17 21:15 71-43-20.0042 1
Bromobenzene ND mg/kg 09/21/17 21:15 108-86-10.0042 1
Bromochloromethane ND mg/kg 09/21/17 21:15 74-97-50.0042 1
Bromodichloromethane ND mg/kg 09/21/17 21:15 75-27-40.0042 1
Bromoform ND mg/kg 09/21/17 21:15 75-25-20.0042 1
Bromomethane ND mg/kg 09/21/17 21:15 74-83-90.0084 1
2-Butanone (MEK)ND mg/kg 09/21/17 21:15 78-93-30.084 1
n-Butylbenzene ND mg/kg 09/21/17 21:15 104-51-80.0042 1
sec-Butylbenzene ND mg/kg 09/21/17 21:15 135-98-80.0042 1
tert-Butylbenzene ND mg/kg 09/21/17 21:15 98-06-60.0042 1
Carbon tetrachloride ND mg/kg 09/21/17 21:15 56-23-50.0042 1
Chlorobenzene ND mg/kg 09/21/17 21:15 108-90-70.0042 1
Chloroethane ND mg/kg 09/21/17 21:15 75-00-30.0084 1
Chloroform ND mg/kg 09/21/17 21:15 67-66-30.0042 1
Chloromethane ND mg/kg 09/21/17 21:15 74-87-30.0084 1
2-Chlorotoluene ND mg/kg 09/21/17 21:15 95-49-80.0042 1
4-Chlorotoluene ND mg/kg 09/21/17 21:15 106-43-40.0042 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/21/17 21:15 96-12-80.0042 1
Dibromochloromethane ND mg/kg 09/21/17 21:15 124-48-10.0042 1
1,2-Dibromoethane (EDB)ND mg/kg 09/21/17 21:15 106-93-40.0042 1
Dibromomethane ND mg/kg 09/21/17 21:15 74-95-30.0042 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 21:15 95-50-10.0042 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 21:15 541-73-10.0042 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 21:15 106-46-70.0042 1
Dichlorodifluoromethane ND mg/kg 09/21/17 21:15 75-71-80.0084 1
1,1-Dichloroethane ND mg/kg 09/21/17 21:15 75-34-30.0042 1
1,2-Dichloroethane ND mg/kg 09/21/17 21:15 107-06-20.0042 1
1,1-Dichloroethene ND mg/kg 09/21/17 21:15 75-35-40.0042 1
cis-1,2-Dichloroethene ND mg/kg 09/21/17 21:15 156-59-20.0042 1
trans-1,2-Dichloroethene ND mg/kg 09/21/17 21:15 156-60-50.0042 1
1,2-Dichloropropane ND mg/kg 09/21/17 21:15 78-87-50.0042 1
1,3-Dichloropropane ND mg/kg 09/21/17 21:15 142-28-90.0042 1
2,2-Dichloropropane ND mg/kg 09/21/17 21:15 594-20-70.0042 1
1,1-Dichloropropene ND mg/kg 09/21/17 21:15 563-58-60.0042 1
cis-1,3-Dichloropropene ND mg/kg 09/21/17 21:15 10061-01-50.0042 1
trans-1,3-Dichloropropene ND mg/kg 09/21/17 21:15 10061-02-60.0042 1
Diisopropyl ether ND mg/kg 09/21/17 21:15 108-20-30.0042 1
Ethylbenzene ND mg/kg 09/21/17 21:15 100-41-40.0042 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 21:15 87-68-30.0042 1
2-Hexanone ND mg/kg 09/21/17 21:15 591-78-60.042 1
Isopropylbenzene (Cumene)ND mg/kg 09/21/17 21:15 98-82-80.0042 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-2C Lab ID:92355949006 Collected:09/18/17 18:20 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND mg/kg 09/21/17 21:15 99-87-60.0042 1
Methylene Chloride ND mg/kg 09/21/17 21:15 75-09-20.017 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/21/17 21:15 108-10-10.042 1
Methyl-tert-butyl ether 0.026 mg/kg 09/21/17 21:15 1634-04-40.0042 1
Naphthalene 0.0056 mg/kg 09/21/17 21:15 91-20-30.0042 1
n-Propylbenzene ND mg/kg 09/21/17 21:15 103-65-10.0042 1
Styrene ND mg/kg 09/21/17 21:15 100-42-50.0042 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/21/17 21:15 630-20-60.0042 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/21/17 21:15 79-34-50.0042 1
Tetrachloroethene ND mg/kg 09/21/17 21:15 127-18-40.0042 1
Toluene ND mg/kg 09/21/17 21:15 108-88-30.0042 1
1,2,3-Trichlorobenzene ND mg/kg 09/21/17 21:15 87-61-60.0042 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 21:15 120-82-10.0042 1
1,1,1-Trichloroethane ND mg/kg 09/21/17 21:15 71-55-60.0042 1
1,1,2-Trichloroethane ND mg/kg 09/21/17 21:15 79-00-50.0042 1
Trichloroethene ND mg/kg 09/21/17 21:15 79-01-60.0042 1
Trichlorofluoromethane ND mg/kg 09/21/17 21:15 75-69-40.0042 1
1,2,3-Trichloropropane ND mg/kg 09/21/17 21:15 96-18-40.0042 1
1,2,4-Trimethylbenzene 0.013 mg/kg 09/21/17 21:15 95-63-60.0042 1
1,3,5-Trimethylbenzene ND mg/kg 09/21/17 21:15 108-67-80.0042 1
Vinyl acetate ND mg/kg 09/21/17 21:15 108-05-40.042 1
Vinyl chloride ND mg/kg 09/21/17 21:15 75-01-40.0084 1
Xylene (Total)ND mg/kg 09/21/17 21:15 1330-20-70.0084 1
m&p-Xylene ND mg/kg 09/21/17 21:15 179601-23-10.0084 1
o-Xylene ND mg/kg 09/21/17 21:15 95-47-60.0042 1
Surrogates
Toluene-d8 (S)96 %09/21/17 21:15 2037-26-570-130 1
4-Bromofluorobenzene (S)101 %09/21/17 21:15 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %09/21/17 21:15 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 21.0 %09/21/17 11:090.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-3A Lab ID:92355949007 Collected:09/18/17 11:20 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/22/17 11:39 N209/21/17 08:0513.6 1
Aliphatic (C19-C36)ND mg/kg 09/22/17 11:39 N209/21/17 08:0513.6 1
Aromatic (C11-C22)ND mg/kg 09/22/17 11:39 N209/21/17 08:0513.6 1
Surrogates
Nonatriacontane (S)52 %09/22/17 11:39 7194-86-709/21/17 08:0540-140 1
o-Terphenyl (S)82 %09/22/17 11:39 84-15-109/21/17 08:0540-140 1
2-Fluorobiphenyl (S)103 %09/22/17 11:39 321-60-809/21/17 08:0540-140 1
2-Bromonaphthalene (S)101 %09/22/17 11:39 580-13-209/21/17 08:0540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)612 mg/kg 09/26/17 12:12 N209/21/17 10:4515.0 4
Aliphatic (C09-C12)117 mg/kg 09/26/17 12:12 N209/21/17 10:4515.0 4
Aromatic (C09-C10)485 mg/kg 09/26/17 12:12 N209/21/17 10:4515.0 4
Surrogates
4-Bromofluorobenzene (FID) (S)169 %09/26/17 12:12 460-00-4 S509/21/17 10:4570-130 4
4-Bromofluorobenzene (PID) (S)115 %09/26/17 12:12 460-00-409/21/17 10:4570-130 4
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/21/17 17:40 83-32-909/20/17 18:120.44 1
Acenaphthylene ND mg/kg 09/21/17 17:40 208-96-809/20/17 18:120.44 1
Aniline ND mg/kg 09/21/17 17:40 62-53-309/20/17 18:120.44 1
Anthracene ND mg/kg 09/21/17 17:40 120-12-709/20/17 18:120.44 1
Benzo(a)anthracene ND mg/kg 09/21/17 17:40 56-55-309/20/17 18:120.44 1
Benzo(a)pyrene ND mg/kg 09/21/17 17:40 50-32-809/20/17 18:120.44 1
Benzo(b)fluoranthene ND mg/kg 09/21/17 17:40 205-99-209/20/17 18:120.44 1
Benzo(g,h,i)perylene ND mg/kg 09/21/17 17:40 191-24-209/20/17 18:120.44 1
Benzo(k)fluoranthene ND mg/kg 09/21/17 17:40 207-08-909/20/17 18:120.44 1
Benzoic Acid ND mg/kg 09/21/17 17:40 65-85-009/20/17 18:122.2 1
Benzyl alcohol ND mg/kg 09/21/17 17:40 100-51-609/20/17 18:120.88 1
4-Bromophenylphenyl ether ND mg/kg 09/21/17 17:40 101-55-309/20/17 18:120.44 1
Butylbenzylphthalate ND mg/kg 09/21/17 17:40 85-68-709/20/17 18:120.44 1
4-Chloro-3-methylphenol ND mg/kg 09/21/17 17:40 59-50-709/20/17 18:120.88 1
4-Chloroaniline ND mg/kg 09/21/17 17:40 106-47-809/20/17 18:122.2 1
bis(2-Chloroethoxy)methane ND mg/kg 09/21/17 17:40 111-91-109/20/17 18:120.44 1
bis(2-Chloroethyl) ether ND mg/kg 09/21/17 17:40 111-44-409/20/17 18:120.44 1
2-Chloronaphthalene ND mg/kg 09/21/17 17:40 91-58-709/20/17 18:120.44 1
2-Chlorophenol ND mg/kg 09/21/17 17:40 95-57-809/20/17 18:120.44 1
4-Chlorophenylphenyl ether ND mg/kg 09/21/17 17:40 7005-72-309/20/17 18:120.44 1
Chrysene ND mg/kg 09/21/17 17:40 218-01-909/20/17 18:120.44 1
Dibenz(a,h)anthracene ND mg/kg 09/21/17 17:40 53-70-309/20/17 18:120.44 1
Dibenzofuran ND mg/kg 09/21/17 17:40 132-64-909/20/17 18:120.44 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 17:40 95-50-109/20/17 18:120.44 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 17:40 541-73-109/20/17 18:120.44 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 17:40 106-46-709/20/17 18:120.44 1
3,3'-Dichlorobenzidine ND mg/kg 09/21/17 17:40 91-94-109/20/17 18:122.2 1
2,4-Dichlorophenol ND mg/kg 09/21/17 17:40 120-83-209/20/17 18:120.44 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-3A Lab ID:92355949007 Collected:09/18/17 11:20 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/21/17 17:40 84-66-209/20/17 18:120.44 1
2,4-Dimethylphenol ND mg/kg 09/21/17 17:40 105-67-909/20/17 18:120.44 1
Dimethylphthalate ND mg/kg 09/21/17 17:40 131-11-309/20/17 18:120.44 1
Di-n-butylphthalate ND mg/kg 09/21/17 17:40 84-74-209/20/17 18:120.44 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/21/17 17:40 534-52-109/20/17 18:120.88 1
2,4-Dinitrophenol ND mg/kg 09/21/17 17:40 51-28-509/20/17 18:122.2 1
2,4-Dinitrotoluene ND mg/kg 09/21/17 17:40 121-14-209/20/17 18:120.44 1
2,6-Dinitrotoluene ND mg/kg 09/21/17 17:40 606-20-209/20/17 18:120.44 1
Di-n-octylphthalate ND mg/kg 09/21/17 17:40 117-84-009/20/17 18:120.44 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/21/17 17:40 117-81-709/20/17 18:120.44 1
Fluoranthene ND mg/kg 09/21/17 17:40 206-44-009/20/17 18:120.44 1
Fluorene ND mg/kg 09/21/17 17:40 86-73-709/20/17 18:120.44 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 17:40 87-68-309/20/17 18:120.44 1
Hexachlorobenzene ND mg/kg 09/21/17 17:40 118-74-109/20/17 18:120.44 1
Hexachlorocyclopentadiene ND mg/kg 09/21/17 17:40 77-47-409/20/17 18:120.44 1
Hexachloroethane ND mg/kg 09/21/17 17:40 67-72-109/20/17 18:120.44 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/21/17 17:40 193-39-509/20/17 18:120.44 1
Isophorone ND mg/kg 09/21/17 17:40 78-59-109/20/17 18:120.44 1
1-Methylnaphthalene ND mg/kg 09/21/17 17:40 90-12-009/20/17 18:120.44 1
2-Methylnaphthalene ND mg/kg 09/21/17 17:40 91-57-609/20/17 18:120.44 1
2-Methylphenol(o-Cresol)ND mg/kg 09/21/17 17:40 95-48-709/20/17 18:120.44 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/21/17 17:40 15831-10-409/20/17 18:120.44 1
Naphthalene ND mg/kg 09/21/17 17:40 91-20-309/20/17 18:120.44 1
2-Nitroaniline ND mg/kg 09/21/17 17:40 88-74-409/20/17 18:122.2 1
3-Nitroaniline ND mg/kg 09/21/17 17:40 99-09-209/20/17 18:122.2 1
4-Nitroaniline ND mg/kg 09/21/17 17:40 100-01-609/20/17 18:120.88 1
Nitrobenzene ND mg/kg 09/21/17 17:40 98-95-309/20/17 18:120.44 1
2-Nitrophenol ND mg/kg 09/21/17 17:40 88-75-509/20/17 18:120.44 1
4-Nitrophenol ND mg/kg 09/21/17 17:40 100-02-709/20/17 18:122.2 1
N-Nitrosodimethylamine ND mg/kg 09/21/17 17:40 62-75-909/20/17 18:120.44 1
N-Nitroso-di-n-propylamine ND mg/kg 09/21/17 17:40 621-64-709/20/17 18:120.44 1
N-Nitrosodiphenylamine ND mg/kg 09/21/17 17:40 86-30-609/20/17 18:120.44 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/21/17 17:40 108-60-109/20/17 18:120.44 1
Pentachlorophenol ND mg/kg 09/21/17 17:40 87-86-509/20/17 18:122.2 1
Phenanthrene ND mg/kg 09/21/17 17:40 85-01-809/20/17 18:120.44 1
Phenol ND mg/kg 09/21/17 17:40 108-95-209/20/17 18:120.44 1
Pyrene ND mg/kg 09/21/17 17:40 129-00-009/20/17 18:120.44 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 17:40 120-82-109/20/17 18:120.44 1
2,4,5-Trichlorophenol ND mg/kg 09/21/17 17:40 95-95-409/20/17 18:120.44 1
2,4,6-Trichlorophenol ND mg/kg 09/21/17 17:40 88-06-209/20/17 18:120.44 1
Surrogates
Nitrobenzene-d5 (S)32 %09/21/17 17:40 4165-60-009/20/17 18:1223-110 1
2-Fluorobiphenyl (S)29 %09/21/17 17:40 321-60-8 S009/20/17 18:1230-110 1
Terphenyl-d14 (S)69 %09/21/17 17:40 1718-51-009/20/17 18:1228-110 1
Phenol-d6 (S)36 %09/21/17 17:40 13127-88-309/20/17 18:1222-110 1
2-Fluorophenol (S)36 %09/21/17 17:40 367-12-409/20/17 18:1213-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-3A Lab ID:92355949007 Collected:09/18/17 11:20 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)56 %09/21/17 17:40 118-79-609/20/17 18:1227-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/21/17 21:35 67-64-16.6 50
Benzene ND mg/kg 09/21/17 21:35 71-43-20.33 50
Bromobenzene ND mg/kg 09/21/17 21:35 108-86-10.33 50
Bromochloromethane ND mg/kg 09/21/17 21:35 74-97-50.33 50
Bromodichloromethane ND mg/kg 09/21/17 21:35 75-27-40.33 50
Bromoform ND mg/kg 09/21/17 21:35 75-25-20.33 50
Bromomethane ND mg/kg 09/21/17 21:35 74-83-90.66 50
2-Butanone (MEK)ND mg/kg 09/21/17 21:35 78-93-36.6 50
n-Butylbenzene 6.5 mg/kg 09/21/17 21:35 104-51-80.33 50
sec-Butylbenzene 2.2 mg/kg 09/21/17 21:35 135-98-80.33 50
tert-Butylbenzene ND mg/kg 09/21/17 21:35 98-06-60.33 50
Carbon tetrachloride ND mg/kg 09/21/17 21:35 56-23-50.33 50
Chlorobenzene ND mg/kg 09/21/17 21:35 108-90-70.33 50
Chloroethane ND mg/kg 09/21/17 21:35 75-00-30.66 50
Chloroform ND mg/kg 09/21/17 21:35 67-66-30.33 50
Chloromethane ND mg/kg 09/21/17 21:35 74-87-30.66 50
2-Chlorotoluene ND mg/kg 09/21/17 21:35 95-49-80.33 50
4-Chlorotoluene ND mg/kg 09/21/17 21:35 106-43-40.33 50
1,2-Dibromo-3-chloropropane ND mg/kg 09/21/17 21:35 96-12-80.33 50
Dibromochloromethane ND mg/kg 09/21/17 21:35 124-48-10.33 50
1,2-Dibromoethane (EDB)ND mg/kg 09/21/17 21:35 106-93-40.33 50
Dibromomethane ND mg/kg 09/21/17 21:35 74-95-30.33 50
1,2-Dichlorobenzene ND mg/kg 09/21/17 21:35 95-50-10.33 50
1,3-Dichlorobenzene ND mg/kg 09/21/17 21:35 541-73-10.33 50
1,4-Dichlorobenzene ND mg/kg 09/21/17 21:35 106-46-70.33 50
Dichlorodifluoromethane ND mg/kg 09/21/17 21:35 75-71-80.66 50
1,1-Dichloroethane ND mg/kg 09/21/17 21:35 75-34-30.33 50
1,2-Dichloroethane ND mg/kg 09/21/17 21:35 107-06-20.33 50
1,1-Dichloroethene ND mg/kg 09/21/17 21:35 75-35-40.33 50
cis-1,2-Dichloroethene ND mg/kg 09/21/17 21:35 156-59-20.33 50
trans-1,2-Dichloroethene ND mg/kg 09/21/17 21:35 156-60-50.33 50
1,2-Dichloropropane ND mg/kg 09/21/17 21:35 78-87-50.33 50
1,3-Dichloropropane ND mg/kg 09/21/17 21:35 142-28-90.33 50
2,2-Dichloropropane ND mg/kg 09/21/17 21:35 594-20-70.33 50
1,1-Dichloropropene ND mg/kg 09/21/17 21:35 563-58-60.33 50
cis-1,3-Dichloropropene ND mg/kg 09/21/17 21:35 10061-01-50.33 50
trans-1,3-Dichloropropene ND mg/kg 09/21/17 21:35 10061-02-60.33 50
Diisopropyl ether ND mg/kg 09/21/17 21:35 108-20-30.33 50
Ethylbenzene 2.1 mg/kg 09/21/17 21:35 100-41-40.33 50
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 21:35 87-68-30.33 50
2-Hexanone ND mg/kg 09/21/17 21:35 591-78-63.3 50
Isopropylbenzene (Cumene)2.8 mg/kg 09/21/17 21:35 98-82-80.33 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-3A Lab ID:92355949007 Collected:09/18/17 11:20 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene 3.8 mg/kg 09/21/17 21:35 99-87-60.33 50
Methylene Chloride ND mg/kg 09/21/17 21:35 75-09-21.3 50
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/21/17 21:35 108-10-13.3 50
Methyl-tert-butyl ether ND mg/kg 09/21/17 21:35 1634-04-40.33 50
Naphthalene 5.4 mg/kg 09/21/17 21:35 91-20-30.33 50
n-Propylbenzene 12.6 mg/kg 09/21/17 21:35 103-65-10.33 50
Styrene ND mg/kg 09/21/17 21:35 100-42-50.33 50
1,1,1,2-Tetrachloroethane ND mg/kg 09/21/17 21:35 630-20-60.33 50
1,1,2,2-Tetrachloroethane ND mg/kg 09/21/17 21:35 79-34-50.33 50
Tetrachloroethene ND mg/kg 09/21/17 21:35 127-18-40.33 50
Toluene ND mg/kg 09/21/17 21:35 108-88-30.33 50
1,2,3-Trichlorobenzene ND mg/kg 09/21/17 21:35 87-61-60.33 50
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 21:35 120-82-10.33 50
1,1,1-Trichloroethane ND mg/kg 09/21/17 21:35 71-55-60.33 50
1,1,2-Trichloroethane ND mg/kg 09/21/17 21:35 79-00-50.33 50
Trichloroethene ND mg/kg 09/21/17 21:35 79-01-60.33 50
Trichlorofluoromethane ND mg/kg 09/21/17 21:35 75-69-40.33 50
1,2,3-Trichloropropane ND mg/kg 09/21/17 21:35 96-18-40.33 50
1,2,4-Trimethylbenzene 51.6 mg/kg 09/22/17 14:25 95-63-63.3 500
1,3,5-Trimethylbenzene 17.2 mg/kg 09/22/17 14:25 108-67-83.3 500
Vinyl acetate ND mg/kg 09/21/17 21:35 108-05-43.3 50
Vinyl chloride ND mg/kg 09/21/17 21:35 75-01-40.66 50
Xylene (Total)6.9 mg/kg 09/21/17 21:35 1330-20-70.66 50
m&p-Xylene 5.9 mg/kg 09/21/17 21:35 179601-23-10.66 50
o-Xylene 0.94 mg/kg 09/21/17 21:35 95-47-60.33 50
Surrogates
Toluene-d8 (S)88 %09/21/17 21:35 2037-26-570-130 50
4-Bromofluorobenzene (S)114 %09/21/17 21:35 460-00-470-130 50
1,2-Dichloroethane-d4 (S)117 %09/21/17 21:35 17060-07-070-132 50
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 24.4 %09/21/17 11:110.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-3B Lab ID:92355949008 Collected:09/18/17 11:35 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/21/17 18:54 N209/21/17 08:0513.1 1
Aliphatic (C19-C36)ND mg/kg 09/21/17 18:54 N209/21/17 08:0513.1 1
Aromatic (C11-C22)ND mg/kg 09/21/17 18:54 N209/21/17 08:0513.1 1
Surrogates
Nonatriacontane (S)57 %09/21/17 18:54 7194-86-709/21/17 08:0540-140 1
o-Terphenyl (S)81 %09/21/17 18:54 84-15-109/21/17 08:0540-140 1
2-Fluorobiphenyl (S)116 %09/21/17 18:54 321-60-809/21/17 08:0540-140 1
2-Bromonaphthalene (S)114 %09/21/17 18:54 580-13-209/21/17 08:0540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)110 mg/kg 09/21/17 18:54 N209/21/17 10:453.5 1
Aliphatic (C09-C12)27.9 mg/kg 09/21/17 18:54 N209/21/17 10:453.5 1
Aromatic (C09-C10)109 mg/kg 09/21/17 18:54 N209/21/17 10:453.5 1
Surrogates
4-Bromofluorobenzene (FID) (S)175 %09/21/17 18:54 460-00-4 S509/21/17 10:4570-130 1
4-Bromofluorobenzene (PID) (S)113 %09/21/17 18:54 460-00-409/21/17 10:4570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/21/17 18:09 83-32-909/20/17 18:120.42 1
Acenaphthylene ND mg/kg 09/21/17 18:09 208-96-809/20/17 18:120.42 1
Aniline ND mg/kg 09/21/17 18:09 62-53-309/20/17 18:120.42 1
Anthracene ND mg/kg 09/21/17 18:09 120-12-709/20/17 18:120.42 1
Benzo(a)anthracene ND mg/kg 09/21/17 18:09 56-55-309/20/17 18:120.42 1
Benzo(a)pyrene ND mg/kg 09/21/17 18:09 50-32-809/20/17 18:120.42 1
Benzo(b)fluoranthene ND mg/kg 09/21/17 18:09 205-99-209/20/17 18:120.42 1
Benzo(g,h,i)perylene ND mg/kg 09/21/17 18:09 191-24-209/20/17 18:120.42 1
Benzo(k)fluoranthene ND mg/kg 09/21/17 18:09 207-08-909/20/17 18:120.42 1
Benzoic Acid ND mg/kg 09/21/17 18:09 65-85-009/20/17 18:122.1 1
Benzyl alcohol ND mg/kg 09/21/17 18:09 100-51-609/20/17 18:120.84 1
4-Bromophenylphenyl ether ND mg/kg 09/21/17 18:09 101-55-309/20/17 18:120.42 1
Butylbenzylphthalate ND mg/kg 09/21/17 18:09 85-68-709/20/17 18:120.42 1
4-Chloro-3-methylphenol ND mg/kg 09/21/17 18:09 59-50-709/20/17 18:120.84 1
4-Chloroaniline ND mg/kg 09/21/17 18:09 106-47-809/20/17 18:122.1 1
bis(2-Chloroethoxy)methane ND mg/kg 09/21/17 18:09 111-91-109/20/17 18:120.42 1
bis(2-Chloroethyl) ether ND mg/kg 09/21/17 18:09 111-44-409/20/17 18:120.42 1
2-Chloronaphthalene ND mg/kg 09/21/17 18:09 91-58-709/20/17 18:120.42 1
2-Chlorophenol ND mg/kg 09/21/17 18:09 95-57-809/20/17 18:120.42 1
4-Chlorophenylphenyl ether ND mg/kg 09/21/17 18:09 7005-72-309/20/17 18:120.42 1
Chrysene ND mg/kg 09/21/17 18:09 218-01-909/20/17 18:120.42 1
Dibenz(a,h)anthracene ND mg/kg 09/21/17 18:09 53-70-309/20/17 18:120.42 1
Dibenzofuran ND mg/kg 09/21/17 18:09 132-64-909/20/17 18:120.42 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 18:09 95-50-109/20/17 18:120.42 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 18:09 541-73-109/20/17 18:120.42 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 18:09 106-46-709/20/17 18:120.42 1
3,3'-Dichlorobenzidine ND mg/kg 09/21/17 18:09 91-94-109/20/17 18:122.1 1
2,4-Dichlorophenol ND mg/kg 09/21/17 18:09 120-83-209/20/17 18:120.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-3B Lab ID:92355949008 Collected:09/18/17 11:35 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/21/17 18:09 84-66-209/20/17 18:120.42 1
2,4-Dimethylphenol ND mg/kg 09/21/17 18:09 105-67-909/20/17 18:120.42 1
Dimethylphthalate ND mg/kg 09/21/17 18:09 131-11-309/20/17 18:120.42 1
Di-n-butylphthalate ND mg/kg 09/21/17 18:09 84-74-209/20/17 18:120.42 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/21/17 18:09 534-52-109/20/17 18:120.84 1
2,4-Dinitrophenol ND mg/kg 09/21/17 18:09 51-28-509/20/17 18:122.1 1
2,4-Dinitrotoluene ND mg/kg 09/21/17 18:09 121-14-209/20/17 18:120.42 1
2,6-Dinitrotoluene ND mg/kg 09/21/17 18:09 606-20-209/20/17 18:120.42 1
Di-n-octylphthalate ND mg/kg 09/21/17 18:09 117-84-009/20/17 18:120.42 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/21/17 18:09 117-81-709/20/17 18:120.42 1
Fluoranthene ND mg/kg 09/21/17 18:09 206-44-009/20/17 18:120.42 1
Fluorene ND mg/kg 09/21/17 18:09 86-73-709/20/17 18:120.42 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 18:09 87-68-309/20/17 18:120.42 1
Hexachlorobenzene ND mg/kg 09/21/17 18:09 118-74-109/20/17 18:120.42 1
Hexachlorocyclopentadiene ND mg/kg 09/21/17 18:09 77-47-409/20/17 18:120.42 1
Hexachloroethane ND mg/kg 09/21/17 18:09 67-72-109/20/17 18:120.42 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/21/17 18:09 193-39-509/20/17 18:120.42 1
Isophorone ND mg/kg 09/21/17 18:09 78-59-109/20/17 18:120.42 1
1-Methylnaphthalene ND mg/kg 09/21/17 18:09 90-12-009/20/17 18:120.42 1
2-Methylnaphthalene ND mg/kg 09/21/17 18:09 91-57-609/20/17 18:120.42 1
2-Methylphenol(o-Cresol)ND mg/kg 09/21/17 18:09 95-48-709/20/17 18:120.42 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/21/17 18:09 15831-10-409/20/17 18:120.42 1
Naphthalene ND mg/kg 09/21/17 18:09 91-20-309/20/17 18:120.42 1
2-Nitroaniline ND mg/kg 09/21/17 18:09 88-74-409/20/17 18:122.1 1
3-Nitroaniline ND mg/kg 09/21/17 18:09 99-09-209/20/17 18:122.1 1
4-Nitroaniline ND mg/kg 09/21/17 18:09 100-01-609/20/17 18:120.84 1
Nitrobenzene ND mg/kg 09/21/17 18:09 98-95-309/20/17 18:120.42 1
2-Nitrophenol ND mg/kg 09/21/17 18:09 88-75-509/20/17 18:120.42 1
4-Nitrophenol ND mg/kg 09/21/17 18:09 100-02-709/20/17 18:122.1 1
N-Nitrosodimethylamine ND mg/kg 09/21/17 18:09 62-75-909/20/17 18:120.42 1
N-Nitroso-di-n-propylamine ND mg/kg 09/21/17 18:09 621-64-709/20/17 18:120.42 1
N-Nitrosodiphenylamine ND mg/kg 09/21/17 18:09 86-30-609/20/17 18:120.42 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/21/17 18:09 108-60-109/20/17 18:120.42 1
Pentachlorophenol ND mg/kg 09/21/17 18:09 87-86-509/20/17 18:122.1 1
Phenanthrene ND mg/kg 09/21/17 18:09 85-01-809/20/17 18:120.42 1
Phenol ND mg/kg 09/21/17 18:09 108-95-209/20/17 18:120.42 1
Pyrene ND mg/kg 09/21/17 18:09 129-00-009/20/17 18:120.42 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 18:09 120-82-109/20/17 18:120.42 1
2,4,5-Trichlorophenol ND mg/kg 09/21/17 18:09 95-95-409/20/17 18:120.42 1
2,4,6-Trichlorophenol ND mg/kg 09/21/17 18:09 88-06-209/20/17 18:120.42 1
Surrogates
Nitrobenzene-d5 (S)31 %09/21/17 18:09 4165-60-009/20/17 18:1223-110 1
2-Fluorobiphenyl (S)20 %09/21/17 18:09 321-60-8 S009/20/17 18:1230-110 1
Terphenyl-d14 (S)73 %09/21/17 18:09 1718-51-009/20/17 18:1228-110 1
Phenol-d6 (S)32 %09/21/17 18:09 13127-88-309/20/17 18:1222-110 1
2-Fluorophenol (S)32 %09/21/17 18:09 367-12-409/20/17 18:1213-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 40 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-3B Lab ID:92355949008 Collected:09/18/17 11:35 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)56 %09/21/17 18:09 118-79-609/20/17 18:1227-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/21/17 21:55 67-64-16.3 50
Benzene ND mg/kg 09/21/17 21:55 71-43-20.32 50
Bromobenzene ND mg/kg 09/21/17 21:55 108-86-10.32 50
Bromochloromethane ND mg/kg 09/21/17 21:55 74-97-50.32 50
Bromodichloromethane ND mg/kg 09/21/17 21:55 75-27-40.32 50
Bromoform ND mg/kg 09/21/17 21:55 75-25-20.32 50
Bromomethane ND mg/kg 09/21/17 21:55 74-83-90.63 50
2-Butanone (MEK)ND mg/kg 09/21/17 21:55 78-93-36.3 50
n-Butylbenzene 6.9 mg/kg 09/21/17 21:55 104-51-80.32 50
sec-Butylbenzene 2.3 mg/kg 09/21/17 21:55 135-98-80.32 50
tert-Butylbenzene ND mg/kg 09/21/17 21:55 98-06-60.32 50
Carbon tetrachloride ND mg/kg 09/21/17 21:55 56-23-50.32 50
Chlorobenzene ND mg/kg 09/21/17 21:55 108-90-70.32 50
Chloroethane ND mg/kg 09/21/17 21:55 75-00-30.63 50
Chloroform ND mg/kg 09/21/17 21:55 67-66-30.32 50
Chloromethane ND mg/kg 09/21/17 21:55 74-87-30.63 50
2-Chlorotoluene ND mg/kg 09/21/17 21:55 95-49-80.32 50
4-Chlorotoluene ND mg/kg 09/21/17 21:55 106-43-40.32 50
1,2-Dibromo-3-chloropropane ND mg/kg 09/21/17 21:55 96-12-80.32 50
Dibromochloromethane ND mg/kg 09/21/17 21:55 124-48-10.32 50
1,2-Dibromoethane (EDB)ND mg/kg 09/21/17 21:55 106-93-40.32 50
Dibromomethane ND mg/kg 09/21/17 21:55 74-95-30.32 50
1,2-Dichlorobenzene ND mg/kg 09/21/17 21:55 95-50-10.32 50
1,3-Dichlorobenzene ND mg/kg 09/21/17 21:55 541-73-10.32 50
1,4-Dichlorobenzene ND mg/kg 09/21/17 21:55 106-46-70.32 50
Dichlorodifluoromethane ND mg/kg 09/21/17 21:55 75-71-80.63 50
1,1-Dichloroethane ND mg/kg 09/21/17 21:55 75-34-30.32 50
1,2-Dichloroethane ND mg/kg 09/21/17 21:55 107-06-20.32 50
1,1-Dichloroethene ND mg/kg 09/21/17 21:55 75-35-40.32 50
cis-1,2-Dichloroethene ND mg/kg 09/21/17 21:55 156-59-20.32 50
trans-1,2-Dichloroethene ND mg/kg 09/21/17 21:55 156-60-50.32 50
1,2-Dichloropropane ND mg/kg 09/21/17 21:55 78-87-50.32 50
1,3-Dichloropropane ND mg/kg 09/21/17 21:55 142-28-90.32 50
2,2-Dichloropropane ND mg/kg 09/21/17 21:55 594-20-70.32 50
1,1-Dichloropropene ND mg/kg 09/21/17 21:55 563-58-60.32 50
cis-1,3-Dichloropropene ND mg/kg 09/21/17 21:55 10061-01-50.32 50
trans-1,3-Dichloropropene ND mg/kg 09/21/17 21:55 10061-02-60.32 50
Diisopropyl ether ND mg/kg 09/21/17 21:55 108-20-30.32 50
Ethylbenzene 2.2 mg/kg 09/21/17 21:55 100-41-40.32 50
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 21:55 87-68-30.32 50
2-Hexanone ND mg/kg 09/21/17 21:55 591-78-63.2 50
Isopropylbenzene (Cumene)2.9 mg/kg 09/21/17 21:55 98-82-80.32 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 41 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-3B Lab ID:92355949008 Collected:09/18/17 11:35 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene 3.9 mg/kg 09/21/17 21:55 99-87-60.32 50
Methylene Chloride ND mg/kg 09/21/17 21:55 75-09-21.3 50
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/21/17 21:55 108-10-13.2 50
Methyl-tert-butyl ether ND mg/kg 09/21/17 21:55 1634-04-40.32 50
Naphthalene 5.6 mg/kg 09/21/17 21:55 91-20-30.32 50
n-Propylbenzene 12.3 mg/kg 09/22/17 14:45 103-65-13.2 500
Styrene ND mg/kg 09/21/17 21:55 100-42-50.32 50
1,1,1,2-Tetrachloroethane ND mg/kg 09/21/17 21:55 630-20-60.32 50
1,1,2,2-Tetrachloroethane ND mg/kg 09/21/17 21:55 79-34-50.32 50
Tetrachloroethene ND mg/kg 09/21/17 21:55 127-18-40.32 50
Toluene ND mg/kg 09/21/17 21:55 108-88-30.32 50
1,2,3-Trichlorobenzene ND mg/kg 09/21/17 21:55 87-61-60.32 50
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 21:55 120-82-10.32 50
1,1,1-Trichloroethane ND mg/kg 09/21/17 21:55 71-55-60.32 50
1,1,2-Trichloroethane ND mg/kg 09/21/17 21:55 79-00-50.32 50
Trichloroethene ND mg/kg 09/21/17 21:55 79-01-60.32 50
Trichlorofluoromethane ND mg/kg 09/21/17 21:55 75-69-40.32 50
1,2,3-Trichloropropane ND mg/kg 09/21/17 21:55 96-18-40.32 50
1,2,4-Trimethylbenzene 56.8 mg/kg 09/22/17 14:45 95-63-63.2 500
1,3,5-Trimethylbenzene 18.9 mg/kg 09/22/17 14:45 108-67-83.2 500
Vinyl acetate ND mg/kg 09/21/17 21:55 108-05-43.2 50
Vinyl chloride ND mg/kg 09/21/17 21:55 75-01-40.63 50
Xylene (Total)7.5 mg/kg 09/21/17 21:55 1330-20-70.63 50
m&p-Xylene 6.5 mg/kg 09/21/17 21:55 179601-23-10.63 50
o-Xylene 1.0 mg/kg 09/21/17 21:55 95-47-60.32 50
Surrogates
Toluene-d8 (S)86 %09/21/17 21:55 2037-26-570-130 50
4-Bromofluorobenzene (S)103 %09/21/17 21:55 460-00-470-130 50
1,2-Dichloroethane-d4 (S)113 %09/21/17 21:55 17060-07-070-132 50
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 21.1 %09/21/17 11:110.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 42 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-3C Lab ID:92355949009 Collected:09/18/17 11:45 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/22/17 12:07 N209/21/17 08:0512.8 1
Aliphatic (C19-C36)ND mg/kg 09/22/17 12:07 N209/21/17 08:0512.8 1
Aromatic (C11-C22)ND mg/kg 09/22/17 12:07 N209/21/17 08:0512.8 1
Surrogates
Nonatriacontane (S)45 %09/22/17 12:07 7194-86-709/21/17 08:0540-140 1
o-Terphenyl (S)71 %09/22/17 12:07 84-15-109/21/17 08:0540-140 1
2-Fluorobiphenyl (S)109 %09/22/17 12:07 321-60-809/21/17 08:0540-140 1
2-Bromonaphthalene (S)108 %09/22/17 12:07 580-13-209/21/17 08:0540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)303 mg/kg 09/26/17 11:44 N209/21/17 10:455.1 2
Aliphatic (C09-C12)68.3 mg/kg 09/26/17 11:44 N209/21/17 10:455.1 2
Aromatic (C09-C10)255 mg/kg 09/26/17 11:44 N209/21/17 10:455.1 2
Surrogates
4-Bromofluorobenzene (FID) (S)184 %09/26/17 11:44 460-00-4 S509/21/17 10:4570-130 2
4-Bromofluorobenzene (PID) (S)116 %09/26/17 11:44 460-00-409/21/17 10:4570-130 2
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/21/17 18:38 83-32-909/20/17 18:120.42 1
Acenaphthylene ND mg/kg 09/21/17 18:38 208-96-809/20/17 18:120.42 1
Aniline ND mg/kg 09/21/17 18:38 62-53-309/20/17 18:120.42 1
Anthracene ND mg/kg 09/21/17 18:38 120-12-709/20/17 18:120.42 1
Benzo(a)anthracene ND mg/kg 09/21/17 18:38 56-55-309/20/17 18:120.42 1
Benzo(a)pyrene ND mg/kg 09/21/17 18:38 50-32-809/20/17 18:120.42 1
Benzo(b)fluoranthene ND mg/kg 09/21/17 18:38 205-99-209/20/17 18:120.42 1
Benzo(g,h,i)perylene ND mg/kg 09/21/17 18:38 191-24-209/20/17 18:120.42 1
Benzo(k)fluoranthene ND mg/kg 09/21/17 18:38 207-08-909/20/17 18:120.42 1
Benzoic Acid ND mg/kg 09/21/17 18:38 65-85-009/20/17 18:122.1 1
Benzyl alcohol ND mg/kg 09/21/17 18:38 100-51-609/20/17 18:120.84 1
4-Bromophenylphenyl ether ND mg/kg 09/21/17 18:38 101-55-309/20/17 18:120.42 1
Butylbenzylphthalate ND mg/kg 09/21/17 18:38 85-68-709/20/17 18:120.42 1
4-Chloro-3-methylphenol ND mg/kg 09/21/17 18:38 59-50-709/20/17 18:120.84 1
4-Chloroaniline ND mg/kg 09/21/17 18:38 106-47-809/20/17 18:122.1 1
bis(2-Chloroethoxy)methane ND mg/kg 09/21/17 18:38 111-91-109/20/17 18:120.42 1
bis(2-Chloroethyl) ether ND mg/kg 09/21/17 18:38 111-44-409/20/17 18:120.42 1
2-Chloronaphthalene ND mg/kg 09/21/17 18:38 91-58-709/20/17 18:120.42 1
2-Chlorophenol ND mg/kg 09/21/17 18:38 95-57-809/20/17 18:120.42 1
4-Chlorophenylphenyl ether ND mg/kg 09/21/17 18:38 7005-72-309/20/17 18:120.42 1
Chrysene ND mg/kg 09/21/17 18:38 218-01-909/20/17 18:120.42 1
Dibenz(a,h)anthracene ND mg/kg 09/21/17 18:38 53-70-309/20/17 18:120.42 1
Dibenzofuran ND mg/kg 09/21/17 18:38 132-64-909/20/17 18:120.42 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 18:38 95-50-109/20/17 18:120.42 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 18:38 541-73-109/20/17 18:120.42 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 18:38 106-46-709/20/17 18:120.42 1
3,3'-Dichlorobenzidine ND mg/kg 09/21/17 18:38 91-94-109/20/17 18:122.1 1
2,4-Dichlorophenol ND mg/kg 09/21/17 18:38 120-83-209/20/17 18:120.42 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 43 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-3C Lab ID:92355949009 Collected:09/18/17 11:45 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/21/17 18:38 84-66-209/20/17 18:120.42 1
2,4-Dimethylphenol ND mg/kg 09/21/17 18:38 105-67-909/20/17 18:120.42 1
Dimethylphthalate ND mg/kg 09/21/17 18:38 131-11-309/20/17 18:120.42 1
Di-n-butylphthalate ND mg/kg 09/21/17 18:38 84-74-209/20/17 18:120.42 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/21/17 18:38 534-52-109/20/17 18:120.84 1
2,4-Dinitrophenol ND mg/kg 09/21/17 18:38 51-28-509/20/17 18:122.1 1
2,4-Dinitrotoluene ND mg/kg 09/21/17 18:38 121-14-209/20/17 18:120.42 1
2,6-Dinitrotoluene ND mg/kg 09/21/17 18:38 606-20-209/20/17 18:120.42 1
Di-n-octylphthalate ND mg/kg 09/21/17 18:38 117-84-009/20/17 18:120.42 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/21/17 18:38 117-81-709/20/17 18:120.42 1
Fluoranthene ND mg/kg 09/21/17 18:38 206-44-009/20/17 18:120.42 1
Fluorene ND mg/kg 09/21/17 18:38 86-73-709/20/17 18:120.42 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 18:38 87-68-309/20/17 18:120.42 1
Hexachlorobenzene ND mg/kg 09/21/17 18:38 118-74-109/20/17 18:120.42 1
Hexachlorocyclopentadiene ND mg/kg 09/21/17 18:38 77-47-409/20/17 18:120.42 1
Hexachloroethane ND mg/kg 09/21/17 18:38 67-72-109/20/17 18:120.42 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/21/17 18:38 193-39-509/20/17 18:120.42 1
Isophorone ND mg/kg 09/21/17 18:38 78-59-109/20/17 18:120.42 1
1-Methylnaphthalene ND mg/kg 09/21/17 18:38 90-12-009/20/17 18:120.42 1
2-Methylnaphthalene 0.52 mg/kg 09/21/17 18:38 91-57-609/20/17 18:120.42 1
2-Methylphenol(o-Cresol)ND mg/kg 09/21/17 18:38 95-48-709/20/17 18:120.42 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/21/17 18:38 15831-10-409/20/17 18:120.42 1
Naphthalene ND mg/kg 09/21/17 18:38 91-20-309/20/17 18:120.42 1
2-Nitroaniline ND mg/kg 09/21/17 18:38 88-74-409/20/17 18:122.1 1
3-Nitroaniline ND mg/kg 09/21/17 18:38 99-09-209/20/17 18:122.1 1
4-Nitroaniline ND mg/kg 09/21/17 18:38 100-01-609/20/17 18:120.84 1
Nitrobenzene ND mg/kg 09/21/17 18:38 98-95-309/20/17 18:120.42 1
2-Nitrophenol ND mg/kg 09/21/17 18:38 88-75-509/20/17 18:120.42 1
4-Nitrophenol ND mg/kg 09/21/17 18:38 100-02-709/20/17 18:122.1 1
N-Nitrosodimethylamine ND mg/kg 09/21/17 18:38 62-75-909/20/17 18:120.42 1
N-Nitroso-di-n-propylamine ND mg/kg 09/21/17 18:38 621-64-709/20/17 18:120.42 1
N-Nitrosodiphenylamine ND mg/kg 09/21/17 18:38 86-30-609/20/17 18:120.42 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/21/17 18:38 108-60-109/20/17 18:120.42 1
Pentachlorophenol ND mg/kg 09/21/17 18:38 87-86-509/20/17 18:122.1 1
Phenanthrene ND mg/kg 09/21/17 18:38 85-01-809/20/17 18:120.42 1
Phenol ND mg/kg 09/21/17 18:38 108-95-209/20/17 18:120.42 1
Pyrene ND mg/kg 09/21/17 18:38 129-00-009/20/17 18:120.42 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 18:38 120-82-109/20/17 18:120.42 1
2,4,5-Trichlorophenol ND mg/kg 09/21/17 18:38 95-95-409/20/17 18:120.42 1
2,4,6-Trichlorophenol ND mg/kg 09/21/17 18:38 88-06-209/20/17 18:120.42 1
Surrogates
Nitrobenzene-d5 (S)52 %09/21/17 18:38 4165-60-009/20/17 18:1223-110 1
2-Fluorobiphenyl (S)40 %09/21/17 18:38 321-60-809/20/17 18:1230-110 1
Terphenyl-d14 (S)76 %09/21/17 18:38 1718-51-009/20/17 18:1228-110 1
Phenol-d6 (S)52 %09/21/17 18:38 13127-88-309/20/17 18:1222-110 1
2-Fluorophenol (S)52 %09/21/17 18:38 367-12-409/20/17 18:1213-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 44 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-3C Lab ID:92355949009 Collected:09/18/17 11:45 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)70 %09/21/17 18:38 118-79-609/20/17 18:1227-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/21/17 14:43 67-64-12.9 25
Benzene ND mg/kg 09/21/17 14:43 71-43-20.14 25
Bromobenzene ND mg/kg 09/21/17 14:43 108-86-10.14 25
Bromochloromethane ND mg/kg 09/21/17 14:43 74-97-50.14 25
Bromodichloromethane ND mg/kg 09/21/17 14:43 75-27-40.14 25
Bromoform ND mg/kg 09/21/17 14:43 75-25-20.14 25
Bromomethane ND mg/kg 09/21/17 14:43 74-83-90.29 25
2-Butanone (MEK)ND mg/kg 09/21/17 14:43 78-93-32.9 25
n-Butylbenzene 1.6 mg/kg 09/21/17 14:43 104-51-80.14 25
sec-Butylbenzene 0.45 mg/kg 09/21/17 14:43 135-98-80.14 25
tert-Butylbenzene ND mg/kg 09/21/17 14:43 98-06-60.14 25
Carbon tetrachloride ND mg/kg 09/21/17 14:43 56-23-50.14 25
Chlorobenzene ND mg/kg 09/21/17 14:43 108-90-70.14 25
Chloroethane ND mg/kg 09/21/17 14:43 75-00-30.29 25
Chloroform ND mg/kg 09/21/17 14:43 67-66-30.14 25
Chloromethane ND mg/kg 09/21/17 14:43 74-87-30.29 25
2-Chlorotoluene ND mg/kg 09/21/17 14:43 95-49-80.14 25
4-Chlorotoluene ND mg/kg 09/21/17 14:43 106-43-40.14 25
1,2-Dibromo-3-chloropropane ND mg/kg 09/21/17 14:43 96-12-80.14 25
Dibromochloromethane ND mg/kg 09/21/17 14:43 124-48-10.14 25
1,2-Dibromoethane (EDB)ND mg/kg 09/21/17 14:43 106-93-40.14 25
Dibromomethane ND mg/kg 09/21/17 14:43 74-95-30.14 25
1,2-Dichlorobenzene ND mg/kg 09/21/17 14:43 95-50-10.14 25
1,3-Dichlorobenzene ND mg/kg 09/21/17 14:43 541-73-10.14 25
1,4-Dichlorobenzene ND mg/kg 09/21/17 14:43 106-46-70.14 25
Dichlorodifluoromethane ND mg/kg 09/21/17 14:43 75-71-80.29 25
1,1-Dichloroethane ND mg/kg 09/21/17 14:43 75-34-30.14 25
1,2-Dichloroethane ND mg/kg 09/21/17 14:43 107-06-20.14 25
1,1-Dichloroethene ND mg/kg 09/21/17 14:43 75-35-40.14 25
cis-1,2-Dichloroethene ND mg/kg 09/21/17 14:43 156-59-20.14 25
trans-1,2-Dichloroethene ND mg/kg 09/21/17 14:43 156-60-50.14 25
1,2-Dichloropropane ND mg/kg 09/21/17 14:43 78-87-50.14 25
1,3-Dichloropropane ND mg/kg 09/21/17 14:43 142-28-90.14 25
2,2-Dichloropropane ND mg/kg 09/21/17 14:43 594-20-70.14 25
1,1-Dichloropropene ND mg/kg 09/21/17 14:43 563-58-60.14 25
cis-1,3-Dichloropropene ND mg/kg 09/21/17 14:43 10061-01-50.14 25
trans-1,3-Dichloropropene ND mg/kg 09/21/17 14:43 10061-02-60.14 25
Diisopropyl ether ND mg/kg 09/21/17 14:43 108-20-30.14 25
Ethylbenzene 0.62 mg/kg 09/21/17 14:43 100-41-40.14 25
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 14:43 87-68-30.14 25
2-Hexanone ND mg/kg 09/21/17 14:43 591-78-61.4 25
Isopropylbenzene (Cumene)0.62 mg/kg 09/21/17 14:43 98-82-80.14 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 45 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-3C Lab ID:92355949009 Collected:09/18/17 11:45 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene 0.96 mg/kg 09/21/17 14:43 99-87-60.14 25
Methylene Chloride ND mg/kg 09/21/17 14:43 75-09-20.57 25
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/21/17 14:43 108-10-11.4 25
Methyl-tert-butyl ether ND mg/kg 09/21/17 14:43 1634-04-40.14 25
Naphthalene 2.1 mg/kg 09/21/17 14:43 91-20-30.14 25
n-Propylbenzene 2.7 mg/kg 09/21/17 14:43 103-65-10.14 25
Styrene ND mg/kg 09/21/17 14:43 100-42-50.14 25
1,1,1,2-Tetrachloroethane ND mg/kg 09/21/17 14:43 630-20-60.14 25
1,1,2,2-Tetrachloroethane ND mg/kg 09/21/17 14:43 79-34-50.14 25
Tetrachloroethene ND mg/kg 09/21/17 14:43 127-18-40.14 25
Toluene ND mg/kg 09/21/17 14:43 108-88-30.14 25
1,2,3-Trichlorobenzene ND mg/kg 09/21/17 14:43 87-61-60.14 25
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 14:43 120-82-10.14 25
1,1,1-Trichloroethane ND mg/kg 09/21/17 14:43 71-55-60.14 25
1,1,2-Trichloroethane ND mg/kg 09/21/17 14:43 79-00-50.14 25
Trichloroethene ND mg/kg 09/21/17 14:43 79-01-60.14 25
Trichlorofluoromethane ND mg/kg 09/21/17 14:43 75-69-40.14 25
1,2,3-Trichloropropane ND mg/kg 09/21/17 14:43 96-18-40.14 25
1,2,4-Trimethylbenzene 14.0 mg/kg 09/22/17 13:07 95-63-61.1 200
1,3,5-Trimethylbenzene 4.4 mg/kg 09/21/17 14:43 108-67-80.14 25
Vinyl acetate ND mg/kg 09/21/17 14:43 108-05-41.4 25
Vinyl chloride ND mg/kg 09/21/17 14:43 75-01-40.29 25
Xylene (Total)1.9 mg/kg 09/21/17 14:43 1330-20-70.29 25
m&p-Xylene 1.8 mg/kg 09/21/17 14:43 179601-23-10.29 25
o-Xylene 0.17 mg/kg 09/21/17 14:43 95-47-60.14 25
Surrogates
Toluene-d8 (S)99 %09/21/17 14:43 2037-26-570-130 25
4-Bromofluorobenzene (S)100 %09/21/17 14:43 460-00-470-130 25
1,2-Dichloroethane-d4 (S)128 %09/21/17 14:43 17060-07-070-132 25
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 21.7 %09/21/17 11:110.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 46 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-4A Lab ID:92355949010 Collected:09/18/17 12:15 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/25/17 17:07 N209/23/17 08:3711.7 1
Aliphatic (C19-C36)ND mg/kg 09/25/17 17:07 N209/23/17 08:3711.7 1
Aromatic (C11-C22)ND mg/kg 09/25/17 17:07 N209/23/17 08:3711.7 1
Surrogates
Nonatriacontane (S)50 %09/25/17 17:07 7194-86-709/23/17 08:3740-140 1
o-Terphenyl (S)6 %09/25/17 17:07 84-15-1 S209/23/17 08:3740-140 1
2-Fluorobiphenyl (S)10 %09/25/17 17:07 321-60-8 S209/23/17 08:3740-140 1
2-Bromonaphthalene (S)9 %09/25/17 17:07 580-13-2 S209/23/17 08:3740-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/26/17 11:16 N209/21/17 10:452.5 1
Aliphatic (C09-C12)ND mg/kg 09/26/17 11:16 N209/21/17 10:452.5 1
Aromatic (C09-C10)ND mg/kg 09/26/17 11:16 N209/21/17 10:452.5 1
Surrogates
4-Bromofluorobenzene (FID) (S)105 %09/26/17 11:16 460-00-409/21/17 10:4570-130 1
4-Bromofluorobenzene (PID) (S)101 %09/26/17 11:16 460-00-409/21/17 10:4570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/21/17 19:08 83-32-909/20/17 18:120.38 1
Acenaphthylene ND mg/kg 09/21/17 19:08 208-96-809/20/17 18:120.38 1
Aniline ND mg/kg 09/21/17 19:08 62-53-309/20/17 18:120.38 1
Anthracene ND mg/kg 09/21/17 19:08 120-12-709/20/17 18:120.38 1
Benzo(a)anthracene ND mg/kg 09/21/17 19:08 56-55-309/20/17 18:120.38 1
Benzo(a)pyrene ND mg/kg 09/21/17 19:08 50-32-809/20/17 18:120.38 1
Benzo(b)fluoranthene ND mg/kg 09/21/17 19:08 205-99-209/20/17 18:120.38 1
Benzo(g,h,i)perylene ND mg/kg 09/21/17 19:08 191-24-209/20/17 18:120.38 1
Benzo(k)fluoranthene ND mg/kg 09/21/17 19:08 207-08-909/20/17 18:120.38 1
Benzoic Acid ND mg/kg 09/21/17 19:08 65-85-009/20/17 18:121.9 1
Benzyl alcohol ND mg/kg 09/21/17 19:08 100-51-609/20/17 18:120.75 1
4-Bromophenylphenyl ether ND mg/kg 09/21/17 19:08 101-55-309/20/17 18:120.38 1
Butylbenzylphthalate ND mg/kg 09/21/17 19:08 85-68-709/20/17 18:120.38 1
4-Chloro-3-methylphenol ND mg/kg 09/21/17 19:08 59-50-709/20/17 18:120.75 1
4-Chloroaniline ND mg/kg 09/21/17 19:08 106-47-809/20/17 18:121.9 1
bis(2-Chloroethoxy)methane ND mg/kg 09/21/17 19:08 111-91-109/20/17 18:120.38 1
bis(2-Chloroethyl) ether ND mg/kg 09/21/17 19:08 111-44-409/20/17 18:120.38 1
2-Chloronaphthalene ND mg/kg 09/21/17 19:08 91-58-709/20/17 18:120.38 1
2-Chlorophenol ND mg/kg 09/21/17 19:08 95-57-809/20/17 18:120.38 1
4-Chlorophenylphenyl ether ND mg/kg 09/21/17 19:08 7005-72-309/20/17 18:120.38 1
Chrysene ND mg/kg 09/21/17 19:08 218-01-909/20/17 18:120.38 1
Dibenz(a,h)anthracene ND mg/kg 09/21/17 19:08 53-70-309/20/17 18:120.38 1
Dibenzofuran ND mg/kg 09/21/17 19:08 132-64-909/20/17 18:120.38 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 19:08 95-50-109/20/17 18:120.38 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 19:08 541-73-109/20/17 18:120.38 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 19:08 106-46-709/20/17 18:120.38 1
3,3'-Dichlorobenzidine ND mg/kg 09/21/17 19:08 91-94-109/20/17 18:121.9 1
2,4-Dichlorophenol ND mg/kg 09/21/17 19:08 120-83-209/20/17 18:120.38 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 47 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-4A Lab ID:92355949010 Collected:09/18/17 12:15 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/21/17 19:08 84-66-209/20/17 18:120.38 1
2,4-Dimethylphenol ND mg/kg 09/21/17 19:08 105-67-909/20/17 18:120.38 1
Dimethylphthalate ND mg/kg 09/21/17 19:08 131-11-309/20/17 18:120.38 1
Di-n-butylphthalate ND mg/kg 09/21/17 19:08 84-74-209/20/17 18:120.38 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/21/17 19:08 534-52-109/20/17 18:120.75 1
2,4-Dinitrophenol ND mg/kg 09/21/17 19:08 51-28-509/20/17 18:121.9 1
2,4-Dinitrotoluene ND mg/kg 09/21/17 19:08 121-14-209/20/17 18:120.38 1
2,6-Dinitrotoluene ND mg/kg 09/21/17 19:08 606-20-209/20/17 18:120.38 1
Di-n-octylphthalate ND mg/kg 09/21/17 19:08 117-84-009/20/17 18:120.38 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/21/17 19:08 117-81-709/20/17 18:120.38 1
Fluoranthene ND mg/kg 09/21/17 19:08 206-44-009/20/17 18:120.38 1
Fluorene ND mg/kg 09/21/17 19:08 86-73-709/20/17 18:120.38 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 19:08 87-68-309/20/17 18:120.38 1
Hexachlorobenzene ND mg/kg 09/21/17 19:08 118-74-109/20/17 18:120.38 1
Hexachlorocyclopentadiene ND mg/kg 09/21/17 19:08 77-47-409/20/17 18:120.38 1
Hexachloroethane ND mg/kg 09/21/17 19:08 67-72-109/20/17 18:120.38 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/21/17 19:08 193-39-509/20/17 18:120.38 1
Isophorone ND mg/kg 09/21/17 19:08 78-59-109/20/17 18:120.38 1
1-Methylnaphthalene ND mg/kg 09/21/17 19:08 90-12-009/20/17 18:120.38 1
2-Methylnaphthalene ND mg/kg 09/21/17 19:08 91-57-609/20/17 18:120.38 1
2-Methylphenol(o-Cresol)ND mg/kg 09/21/17 19:08 95-48-709/20/17 18:120.38 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/21/17 19:08 15831-10-409/20/17 18:120.38 1
Naphthalene ND mg/kg 09/21/17 19:08 91-20-309/20/17 18:120.38 1
2-Nitroaniline ND mg/kg 09/21/17 19:08 88-74-409/20/17 18:121.9 1
3-Nitroaniline ND mg/kg 09/21/17 19:08 99-09-209/20/17 18:121.9 1
4-Nitroaniline ND mg/kg 09/21/17 19:08 100-01-609/20/17 18:120.75 1
Nitrobenzene ND mg/kg 09/21/17 19:08 98-95-309/20/17 18:120.38 1
2-Nitrophenol ND mg/kg 09/21/17 19:08 88-75-509/20/17 18:120.38 1
4-Nitrophenol ND mg/kg 09/21/17 19:08 100-02-709/20/17 18:121.9 1
N-Nitrosodimethylamine ND mg/kg 09/21/17 19:08 62-75-909/20/17 18:120.38 1
N-Nitroso-di-n-propylamine ND mg/kg 09/21/17 19:08 621-64-709/20/17 18:120.38 1
N-Nitrosodiphenylamine ND mg/kg 09/21/17 19:08 86-30-609/20/17 18:120.38 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/21/17 19:08 108-60-109/20/17 18:120.38 1
Pentachlorophenol ND mg/kg 09/21/17 19:08 87-86-509/20/17 18:121.9 1
Phenanthrene ND mg/kg 09/21/17 19:08 85-01-809/20/17 18:120.38 1
Phenol ND mg/kg 09/21/17 19:08 108-95-209/20/17 18:120.38 1
Pyrene ND mg/kg 09/21/17 19:08 129-00-009/20/17 18:120.38 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 19:08 120-82-109/20/17 18:120.38 1
2,4,5-Trichlorophenol ND mg/kg 09/21/17 19:08 95-95-409/20/17 18:120.38 1
2,4,6-Trichlorophenol ND mg/kg 09/21/17 19:08 88-06-209/20/17 18:120.38 1
Surrogates
Nitrobenzene-d5 (S)53 %09/21/17 19:08 4165-60-009/20/17 18:1223-110 1
2-Fluorobiphenyl (S)54 %09/21/17 19:08 321-60-809/20/17 18:1230-110 1
Terphenyl-d14 (S)83 %09/21/17 19:08 1718-51-009/20/17 18:1228-110 1
Phenol-d6 (S)53 %09/21/17 19:08 13127-88-309/20/17 18:1222-110 1
2-Fluorophenol (S)49 %09/21/17 19:08 367-12-409/20/17 18:1213-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 48 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-4A Lab ID:92355949010 Collected:09/18/17 12:15 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)81 %09/21/17 19:08 118-79-609/20/17 18:1227-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/21/17 15:03 67-64-10.10 1
Benzene ND mg/kg 09/21/17 15:03 71-43-20.0052 1
Bromobenzene ND mg/kg 09/21/17 15:03 108-86-10.0052 1
Bromochloromethane ND mg/kg 09/21/17 15:03 74-97-50.0052 1
Bromodichloromethane ND mg/kg 09/21/17 15:03 75-27-40.0052 1
Bromoform ND mg/kg 09/21/17 15:03 75-25-20.0052 1
Bromomethane ND mg/kg 09/21/17 15:03 74-83-90.010 1
2-Butanone (MEK)ND mg/kg 09/21/17 15:03 78-93-30.10 1
n-Butylbenzene ND mg/kg 09/21/17 15:03 104-51-80.0052 1
sec-Butylbenzene ND mg/kg 09/21/17 15:03 135-98-80.0052 1
tert-Butylbenzene ND mg/kg 09/21/17 15:03 98-06-60.0052 1
Carbon tetrachloride ND mg/kg 09/21/17 15:03 56-23-50.0052 1
Chlorobenzene ND mg/kg 09/21/17 15:03 108-90-70.0052 1
Chloroethane ND mg/kg 09/21/17 15:03 75-00-30.010 1
Chloroform ND mg/kg 09/21/17 15:03 67-66-30.0052 1
Chloromethane ND mg/kg 09/21/17 15:03 74-87-30.010 1
2-Chlorotoluene ND mg/kg 09/21/17 15:03 95-49-80.0052 1
4-Chlorotoluene ND mg/kg 09/21/17 15:03 106-43-40.0052 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/21/17 15:03 96-12-80.0052 1
Dibromochloromethane ND mg/kg 09/21/17 15:03 124-48-10.0052 1
1,2-Dibromoethane (EDB)ND mg/kg 09/21/17 15:03 106-93-40.0052 1
Dibromomethane ND mg/kg 09/21/17 15:03 74-95-30.0052 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 15:03 95-50-10.0052 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 15:03 541-73-10.0052 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 15:03 106-46-70.0052 1
Dichlorodifluoromethane ND mg/kg 09/21/17 15:03 75-71-80.010 1
1,1-Dichloroethane ND mg/kg 09/21/17 15:03 75-34-30.0052 1
1,2-Dichloroethane ND mg/kg 09/21/17 15:03 107-06-20.0052 1
1,1-Dichloroethene ND mg/kg 09/21/17 15:03 75-35-40.0052 1
cis-1,2-Dichloroethene ND mg/kg 09/21/17 15:03 156-59-20.0052 1
trans-1,2-Dichloroethene ND mg/kg 09/21/17 15:03 156-60-50.0052 1
1,2-Dichloropropane ND mg/kg 09/21/17 15:03 78-87-50.0052 1
1,3-Dichloropropane ND mg/kg 09/21/17 15:03 142-28-90.0052 1
2,2-Dichloropropane ND mg/kg 09/21/17 15:03 594-20-70.0052 1
1,1-Dichloropropene ND mg/kg 09/21/17 15:03 563-58-60.0052 1
cis-1,3-Dichloropropene ND mg/kg 09/21/17 15:03 10061-01-50.0052 1
trans-1,3-Dichloropropene ND mg/kg 09/21/17 15:03 10061-02-60.0052 1
Diisopropyl ether ND mg/kg 09/21/17 15:03 108-20-30.0052 1
Ethylbenzene ND mg/kg 09/21/17 15:03 100-41-40.0052 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 15:03 87-68-30.0052 1
2-Hexanone ND mg/kg 09/21/17 15:03 591-78-60.052 1
Isopropylbenzene (Cumene)ND mg/kg 09/21/17 15:03 98-82-80.0052 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 49 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-4A Lab ID:92355949010 Collected:09/18/17 12:15 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND mg/kg 09/21/17 15:03 99-87-60.0052 1
Methylene Chloride ND mg/kg 09/21/17 15:03 75-09-20.021 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/21/17 15:03 108-10-10.052 1
Methyl-tert-butyl ether ND mg/kg 09/21/17 15:03 1634-04-40.0052 1
Naphthalene ND mg/kg 09/21/17 15:03 91-20-30.0052 1
n-Propylbenzene ND mg/kg 09/21/17 15:03 103-65-10.0052 1
Styrene ND mg/kg 09/21/17 15:03 100-42-50.0052 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/21/17 15:03 630-20-60.0052 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/21/17 15:03 79-34-50.0052 1
Tetrachloroethene ND mg/kg 09/21/17 15:03 127-18-40.0052 1
Toluene ND mg/kg 09/21/17 15:03 108-88-30.0052 1
1,2,3-Trichlorobenzene ND mg/kg 09/21/17 15:03 87-61-60.0052 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 15:03 120-82-10.0052 1
1,1,1-Trichloroethane ND mg/kg 09/21/17 15:03 71-55-60.0052 1
1,1,2-Trichloroethane ND mg/kg 09/21/17 15:03 79-00-50.0052 1
Trichloroethene ND mg/kg 09/21/17 15:03 79-01-60.0052 1
Trichlorofluoromethane ND mg/kg 09/21/17 15:03 75-69-40.0052 1
1,2,3-Trichloropropane ND mg/kg 09/21/17 15:03 96-18-40.0052 1
1,2,4-Trimethylbenzene ND mg/kg 09/21/17 15:03 95-63-60.0052 1
1,3,5-Trimethylbenzene ND mg/kg 09/21/17 15:03 108-67-80.0052 1
Vinyl acetate ND mg/kg 09/21/17 15:03 108-05-40.052 1
Vinyl chloride ND mg/kg 09/21/17 15:03 75-01-40.010 1
Xylene (Total)ND mg/kg 09/21/17 15:03 1330-20-70.010 1
m&p-Xylene ND mg/kg 09/21/17 15:03 179601-23-10.010 1
o-Xylene ND mg/kg 09/21/17 15:03 95-47-60.0052 1
Surrogates
Toluene-d8 (S)104 %09/21/17 15:03 2037-26-570-130 1
4-Bromofluorobenzene (S)96 %09/21/17 15:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)122 %09/21/17 15:03 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 12.4 %09/21/17 11:110.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 50 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-4B Lab ID:92355949011 Collected:09/18/17 12:25 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/21/17 19:48 N209/21/17 08:0513.0 1
Aliphatic (C19-C36)16.7 mg/kg 09/21/17 19:48 N209/21/17 08:0513.0 1
Aromatic (C11-C22)ND mg/kg 09/21/17 19:48 N209/21/17 08:0513.0 1
Surrogates
Nonatriacontane (S)63 %09/21/17 19:48 7194-86-709/21/17 08:0540-140 1
o-Terphenyl (S)71 %09/21/17 19:48 84-15-109/21/17 08:0540-140 1
2-Fluorobiphenyl (S)108 %09/21/17 19:48 321-60-809/21/17 08:0540-140 1
2-Bromonaphthalene (S)104 %09/21/17 19:48 580-13-209/21/17 08:0540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)60.0 mg/kg 09/21/17 20:17 N209/21/17 10:453.6 1
Aliphatic (C09-C12)12.4 mg/kg 09/21/17 20:17 N209/21/17 10:453.6 1
Aromatic (C09-C10)21.6 mg/kg 09/21/17 20:17 N209/21/17 10:453.6 1
Surrogates
4-Bromofluorobenzene (FID) (S)165 %09/21/17 20:17 460-00-4 S509/21/17 10:4570-130 1
4-Bromofluorobenzene (PID) (S)106 %09/21/17 20:17 460-00-409/21/17 10:4570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/21/17 19:37 83-32-909/20/17 18:120.43 1
Acenaphthylene ND mg/kg 09/21/17 19:37 208-96-809/20/17 18:120.43 1
Aniline ND mg/kg 09/21/17 19:37 62-53-309/20/17 18:120.43 1
Anthracene ND mg/kg 09/21/17 19:37 120-12-709/20/17 18:120.43 1
Benzo(a)anthracene ND mg/kg 09/21/17 19:37 56-55-309/20/17 18:120.43 1
Benzo(a)pyrene ND mg/kg 09/21/17 19:37 50-32-809/20/17 18:120.43 1
Benzo(b)fluoranthene ND mg/kg 09/21/17 19:37 205-99-209/20/17 18:120.43 1
Benzo(g,h,i)perylene ND mg/kg 09/21/17 19:37 191-24-209/20/17 18:120.43 1
Benzo(k)fluoranthene ND mg/kg 09/21/17 19:37 207-08-909/20/17 18:120.43 1
Benzoic Acid ND mg/kg 09/21/17 19:37 65-85-009/20/17 18:122.1 1
Benzyl alcohol ND mg/kg 09/21/17 19:37 100-51-609/20/17 18:120.85 1
4-Bromophenylphenyl ether ND mg/kg 09/21/17 19:37 101-55-309/20/17 18:120.43 1
Butylbenzylphthalate ND mg/kg 09/21/17 19:37 85-68-709/20/17 18:120.43 1
4-Chloro-3-methylphenol ND mg/kg 09/21/17 19:37 59-50-709/20/17 18:120.85 1
4-Chloroaniline ND mg/kg 09/21/17 19:37 106-47-809/20/17 18:122.1 1
bis(2-Chloroethoxy)methane ND mg/kg 09/21/17 19:37 111-91-109/20/17 18:120.43 1
bis(2-Chloroethyl) ether ND mg/kg 09/21/17 19:37 111-44-409/20/17 18:120.43 1
2-Chloronaphthalene ND mg/kg 09/21/17 19:37 91-58-709/20/17 18:120.43 1
2-Chlorophenol ND mg/kg 09/21/17 19:37 95-57-809/20/17 18:120.43 1
4-Chlorophenylphenyl ether ND mg/kg 09/21/17 19:37 7005-72-309/20/17 18:120.43 1
Chrysene ND mg/kg 09/21/17 19:37 218-01-909/20/17 18:120.43 1
Dibenz(a,h)anthracene ND mg/kg 09/21/17 19:37 53-70-309/20/17 18:120.43 1
Dibenzofuran ND mg/kg 09/21/17 19:37 132-64-909/20/17 18:120.43 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 19:37 95-50-109/20/17 18:120.43 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 19:37 541-73-109/20/17 18:120.43 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 19:37 106-46-709/20/17 18:120.43 1
3,3'-Dichlorobenzidine ND mg/kg 09/21/17 19:37 91-94-109/20/17 18:122.1 1
2,4-Dichlorophenol ND mg/kg 09/21/17 19:37 120-83-209/20/17 18:120.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 51 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-4B Lab ID:92355949011 Collected:09/18/17 12:25 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/21/17 19:37 84-66-209/20/17 18:120.43 1
2,4-Dimethylphenol ND mg/kg 09/21/17 19:37 105-67-909/20/17 18:120.43 1
Dimethylphthalate ND mg/kg 09/21/17 19:37 131-11-309/20/17 18:120.43 1
Di-n-butylphthalate ND mg/kg 09/21/17 19:37 84-74-209/20/17 18:120.43 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/21/17 19:37 534-52-109/20/17 18:120.85 1
2,4-Dinitrophenol ND mg/kg 09/21/17 19:37 51-28-509/20/17 18:122.1 1
2,4-Dinitrotoluene ND mg/kg 09/21/17 19:37 121-14-209/20/17 18:120.43 1
2,6-Dinitrotoluene ND mg/kg 09/21/17 19:37 606-20-209/20/17 18:120.43 1
Di-n-octylphthalate ND mg/kg 09/21/17 19:37 117-84-009/20/17 18:120.43 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/21/17 19:37 117-81-709/20/17 18:120.43 1
Fluoranthene ND mg/kg 09/21/17 19:37 206-44-009/20/17 18:120.43 1
Fluorene ND mg/kg 09/21/17 19:37 86-73-709/20/17 18:120.43 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 19:37 87-68-309/20/17 18:120.43 1
Hexachlorobenzene ND mg/kg 09/21/17 19:37 118-74-109/20/17 18:120.43 1
Hexachlorocyclopentadiene ND mg/kg 09/21/17 19:37 77-47-409/20/17 18:120.43 1
Hexachloroethane ND mg/kg 09/21/17 19:37 67-72-109/20/17 18:120.43 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/21/17 19:37 193-39-509/20/17 18:120.43 1
Isophorone ND mg/kg 09/21/17 19:37 78-59-109/20/17 18:120.43 1
1-Methylnaphthalene ND mg/kg 09/21/17 19:37 90-12-009/20/17 18:120.43 1
2-Methylnaphthalene ND mg/kg 09/21/17 19:37 91-57-609/20/17 18:120.43 1
2-Methylphenol(o-Cresol)ND mg/kg 09/21/17 19:37 95-48-709/20/17 18:120.43 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/21/17 19:37 15831-10-409/20/17 18:120.43 1
Naphthalene ND mg/kg 09/21/17 19:37 91-20-309/20/17 18:120.43 1
2-Nitroaniline ND mg/kg 09/21/17 19:37 88-74-409/20/17 18:122.1 1
3-Nitroaniline ND mg/kg 09/21/17 19:37 99-09-209/20/17 18:122.1 1
4-Nitroaniline ND mg/kg 09/21/17 19:37 100-01-609/20/17 18:120.85 1
Nitrobenzene ND mg/kg 09/21/17 19:37 98-95-309/20/17 18:120.43 1
2-Nitrophenol ND mg/kg 09/21/17 19:37 88-75-509/20/17 18:120.43 1
4-Nitrophenol ND mg/kg 09/21/17 19:37 100-02-709/20/17 18:122.1 1
N-Nitrosodimethylamine ND mg/kg 09/21/17 19:37 62-75-909/20/17 18:120.43 1
N-Nitroso-di-n-propylamine ND mg/kg 09/21/17 19:37 621-64-709/20/17 18:120.43 1
N-Nitrosodiphenylamine ND mg/kg 09/21/17 19:37 86-30-609/20/17 18:120.43 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/21/17 19:37 108-60-109/20/17 18:120.43 1
Pentachlorophenol ND mg/kg 09/21/17 19:37 87-86-509/20/17 18:122.1 1
Phenanthrene ND mg/kg 09/21/17 19:37 85-01-809/20/17 18:120.43 1
Phenol ND mg/kg 09/21/17 19:37 108-95-209/20/17 18:120.43 1
Pyrene ND mg/kg 09/21/17 19:37 129-00-009/20/17 18:120.43 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 19:37 120-82-109/20/17 18:120.43 1
2,4,5-Trichlorophenol ND mg/kg 09/21/17 19:37 95-95-409/20/17 18:120.43 1
2,4,6-Trichlorophenol ND mg/kg 09/21/17 19:37 88-06-209/20/17 18:120.43 1
Surrogates
Nitrobenzene-d5 (S)59 %09/21/17 19:37 4165-60-009/20/17 18:1223-110 1
2-Fluorobiphenyl (S)58 %09/21/17 19:37 321-60-809/20/17 18:1230-110 1
Terphenyl-d14 (S)75 %09/21/17 19:37 1718-51-009/20/17 18:1228-110 1
Phenol-d6 (S)57 %09/21/17 19:37 13127-88-309/20/17 18:1222-110 1
2-Fluorophenol (S)57 %09/21/17 19:37 367-12-409/20/17 18:1213-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 52 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-4B Lab ID:92355949011 Collected:09/18/17 12:25 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)74 %09/21/17 19:37 118-79-609/20/17 18:1227-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/21/17 15:22 67-64-12.7 25
Benzene ND mg/kg 09/21/17 15:22 71-43-20.13 25
Bromobenzene ND mg/kg 09/21/17 15:22 108-86-10.13 25
Bromochloromethane ND mg/kg 09/21/17 15:22 74-97-50.13 25
Bromodichloromethane ND mg/kg 09/21/17 15:22 75-27-40.13 25
Bromoform ND mg/kg 09/21/17 15:22 75-25-20.13 25
Bromomethane ND mg/kg 09/21/17 15:22 74-83-90.27 25
2-Butanone (MEK)ND mg/kg 09/21/17 15:22 78-93-32.7 25
n-Butylbenzene ND mg/kg 09/21/17 15:22 104-51-80.13 25
sec-Butylbenzene ND mg/kg 09/21/17 15:22 135-98-80.13 25
tert-Butylbenzene ND mg/kg 09/21/17 15:22 98-06-60.13 25
Carbon tetrachloride ND mg/kg 09/21/17 15:22 56-23-50.13 25
Chlorobenzene ND mg/kg 09/21/17 15:22 108-90-70.13 25
Chloroethane ND mg/kg 09/21/17 15:22 75-00-30.27 25
Chloroform ND mg/kg 09/21/17 15:22 67-66-30.13 25
Chloromethane ND mg/kg 09/21/17 15:22 74-87-30.27 25
2-Chlorotoluene ND mg/kg 09/21/17 15:22 95-49-80.13 25
4-Chlorotoluene ND mg/kg 09/21/17 15:22 106-43-40.13 25
1,2-Dibromo-3-chloropropane ND mg/kg 09/21/17 15:22 96-12-80.13 25
Dibromochloromethane ND mg/kg 09/21/17 15:22 124-48-10.13 25
1,2-Dibromoethane (EDB)ND mg/kg 09/21/17 15:22 106-93-40.13 25
Dibromomethane ND mg/kg 09/21/17 15:22 74-95-30.13 25
1,2-Dichlorobenzene ND mg/kg 09/21/17 15:22 95-50-10.13 25
1,3-Dichlorobenzene ND mg/kg 09/21/17 15:22 541-73-10.13 25
1,4-Dichlorobenzene ND mg/kg 09/21/17 15:22 106-46-70.13 25
Dichlorodifluoromethane ND mg/kg 09/21/17 15:22 75-71-80.27 25
1,1-Dichloroethane ND mg/kg 09/21/17 15:22 75-34-30.13 25
1,2-Dichloroethane ND mg/kg 09/21/17 15:22 107-06-20.13 25
1,1-Dichloroethene ND mg/kg 09/21/17 15:22 75-35-40.13 25
cis-1,2-Dichloroethene ND mg/kg 09/21/17 15:22 156-59-20.13 25
trans-1,2-Dichloroethene ND mg/kg 09/21/17 15:22 156-60-50.13 25
1,2-Dichloropropane ND mg/kg 09/21/17 15:22 78-87-50.13 25
1,3-Dichloropropane ND mg/kg 09/21/17 15:22 142-28-90.13 25
2,2-Dichloropropane ND mg/kg 09/21/17 15:22 594-20-70.13 25
1,1-Dichloropropene ND mg/kg 09/21/17 15:22 563-58-60.13 25
cis-1,3-Dichloropropene ND mg/kg 09/21/17 15:22 10061-01-50.13 25
trans-1,3-Dichloropropene ND mg/kg 09/21/17 15:22 10061-02-60.13 25
Diisopropyl ether ND mg/kg 09/21/17 15:22 108-20-30.13 25
Ethylbenzene ND mg/kg 09/21/17 15:22 100-41-40.13 25
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 15:22 87-68-30.13 25
2-Hexanone ND mg/kg 09/21/17 15:22 591-78-61.3 25
Isopropylbenzene (Cumene)ND mg/kg 09/21/17 15:22 98-82-80.13 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 53 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-4B Lab ID:92355949011 Collected:09/18/17 12:25 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND mg/kg 09/21/17 15:22 99-87-60.13 25
Methylene Chloride ND mg/kg 09/21/17 15:22 75-09-20.53 25
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/21/17 15:22 108-10-11.3 25
Methyl-tert-butyl ether ND mg/kg 09/21/17 15:22 1634-04-40.13 25
Naphthalene ND mg/kg 09/21/17 15:22 91-20-30.13 25
n-Propylbenzene ND mg/kg 09/21/17 15:22 103-65-10.13 25
Styrene ND mg/kg 09/21/17 15:22 100-42-50.13 25
1,1,1,2-Tetrachloroethane ND mg/kg 09/21/17 15:22 630-20-60.13 25
1,1,2,2-Tetrachloroethane ND mg/kg 09/21/17 15:22 79-34-50.13 25
Tetrachloroethene ND mg/kg 09/21/17 15:22 127-18-40.13 25
Toluene ND mg/kg 09/21/17 15:22 108-88-30.13 25
1,2,3-Trichlorobenzene ND mg/kg 09/21/17 15:22 87-61-60.13 25
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 15:22 120-82-10.13 25
1,1,1-Trichloroethane ND mg/kg 09/21/17 15:22 71-55-60.13 25
1,1,2-Trichloroethane ND mg/kg 09/21/17 15:22 79-00-50.13 25
Trichloroethene ND mg/kg 09/21/17 15:22 79-01-60.13 25
Trichlorofluoromethane ND mg/kg 09/21/17 15:22 75-69-40.13 25
1,2,3-Trichloropropane ND mg/kg 09/21/17 15:22 96-18-40.13 25
1,2,4-Trimethylbenzene 0.14 mg/kg 09/21/17 15:22 95-63-60.13 25
1,3,5-Trimethylbenzene ND mg/kg 09/21/17 15:22 108-67-80.13 25
Vinyl acetate ND mg/kg 09/21/17 15:22 108-05-41.3 25
Vinyl chloride ND mg/kg 09/21/17 15:22 75-01-40.27 25
Xylene (Total)ND mg/kg 09/21/17 15:22 1330-20-70.27 25
m&p-Xylene ND mg/kg 09/21/17 15:22 179601-23-10.27 25
o-Xylene ND mg/kg 09/21/17 15:22 95-47-60.13 25
Surrogates
Toluene-d8 (S)97 %09/21/17 15:22 2037-26-5 D370-130 25
4-Bromofluorobenzene (S)96 %09/21/17 15:22 460-00-470-130 25
1,2-Dichloroethane-d4 (S)113 %09/21/17 15:22 17060-07-070-132 25
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 23.1 %09/21/17 11:120.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 54 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-4C Lab ID:92355949012 Collected:09/18/17 12:35 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/22/17 12:34 N209/21/17 08:0512.4 1
Aliphatic (C19-C36)ND mg/kg 09/22/17 12:34 N209/21/17 08:0512.4 1
Aromatic (C11-C22)ND mg/kg 09/22/17 12:34 N209/21/17 08:0512.4 1
Surrogates
Nonatriacontane (S)66 %09/22/17 12:34 7194-86-709/21/17 08:0540-140 1
o-Terphenyl (S)67 %09/22/17 12:34 84-15-109/21/17 08:0540-140 1
2-Fluorobiphenyl (S)97 %09/22/17 12:34 321-60-809/21/17 08:0540-140 1
2-Bromonaphthalene (S)94 %09/22/17 12:34 580-13-209/21/17 08:0540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)13.9 mg/kg 09/21/17 20:45 N209/21/17 10:453.0 1
Aliphatic (C09-C12)5.8 mg/kg 09/21/17 20:45 N209/21/17 10:453.0 1
Aromatic (C09-C10)5.7 mg/kg 09/21/17 20:45 N209/21/17 10:453.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)130 %09/21/17 20:45 460-00-409/21/17 10:4570-130 1
4-Bromofluorobenzene (PID) (S)102 %09/21/17 20:45 460-00-409/21/17 10:4570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/21/17 20:06 83-32-909/20/17 18:120.41 1
Acenaphthylene ND mg/kg 09/21/17 20:06 208-96-809/20/17 18:120.41 1
Aniline ND mg/kg 09/21/17 20:06 62-53-309/20/17 18:120.41 1
Anthracene ND mg/kg 09/21/17 20:06 120-12-709/20/17 18:120.41 1
Benzo(a)anthracene ND mg/kg 09/21/17 20:06 56-55-309/20/17 18:120.41 1
Benzo(a)pyrene ND mg/kg 09/21/17 20:06 50-32-809/20/17 18:120.41 1
Benzo(b)fluoranthene ND mg/kg 09/21/17 20:06 205-99-209/20/17 18:120.41 1
Benzo(g,h,i)perylene ND mg/kg 09/21/17 20:06 191-24-209/20/17 18:120.41 1
Benzo(k)fluoranthene ND mg/kg 09/21/17 20:06 207-08-909/20/17 18:120.41 1
Benzoic Acid ND mg/kg 09/21/17 20:06 65-85-009/20/17 18:122.0 1
Benzyl alcohol ND mg/kg 09/21/17 20:06 100-51-609/20/17 18:120.81 1
4-Bromophenylphenyl ether ND mg/kg 09/21/17 20:06 101-55-309/20/17 18:120.41 1
Butylbenzylphthalate ND mg/kg 09/21/17 20:06 85-68-709/20/17 18:120.41 1
4-Chloro-3-methylphenol ND mg/kg 09/21/17 20:06 59-50-709/20/17 18:120.81 1
4-Chloroaniline ND mg/kg 09/21/17 20:06 106-47-809/20/17 18:122.0 1
bis(2-Chloroethoxy)methane ND mg/kg 09/21/17 20:06 111-91-109/20/17 18:120.41 1
bis(2-Chloroethyl) ether ND mg/kg 09/21/17 20:06 111-44-409/20/17 18:120.41 1
2-Chloronaphthalene ND mg/kg 09/21/17 20:06 91-58-709/20/17 18:120.41 1
2-Chlorophenol ND mg/kg 09/21/17 20:06 95-57-809/20/17 18:120.41 1
4-Chlorophenylphenyl ether ND mg/kg 09/21/17 20:06 7005-72-309/20/17 18:120.41 1
Chrysene ND mg/kg 09/21/17 20:06 218-01-909/20/17 18:120.41 1
Dibenz(a,h)anthracene ND mg/kg 09/21/17 20:06 53-70-309/20/17 18:120.41 1
Dibenzofuran ND mg/kg 09/21/17 20:06 132-64-909/20/17 18:120.41 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 20:06 95-50-109/20/17 18:120.41 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 20:06 541-73-109/20/17 18:120.41 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 20:06 106-46-709/20/17 18:120.41 1
3,3'-Dichlorobenzidine ND mg/kg 09/21/17 20:06 91-94-109/20/17 18:122.0 1
2,4-Dichlorophenol ND mg/kg 09/21/17 20:06 120-83-209/20/17 18:120.41 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 55 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-4C Lab ID:92355949012 Collected:09/18/17 12:35 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/21/17 20:06 84-66-209/20/17 18:120.41 1
2,4-Dimethylphenol ND mg/kg 09/21/17 20:06 105-67-909/20/17 18:120.41 1
Dimethylphthalate ND mg/kg 09/21/17 20:06 131-11-309/20/17 18:120.41 1
Di-n-butylphthalate ND mg/kg 09/21/17 20:06 84-74-209/20/17 18:120.41 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/21/17 20:06 534-52-109/20/17 18:120.81 1
2,4-Dinitrophenol ND mg/kg 09/21/17 20:06 51-28-509/20/17 18:122.0 1
2,4-Dinitrotoluene ND mg/kg 09/21/17 20:06 121-14-209/20/17 18:120.41 1
2,6-Dinitrotoluene ND mg/kg 09/21/17 20:06 606-20-209/20/17 18:120.41 1
Di-n-octylphthalate ND mg/kg 09/21/17 20:06 117-84-009/20/17 18:120.41 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/21/17 20:06 117-81-709/20/17 18:120.41 1
Fluoranthene ND mg/kg 09/21/17 20:06 206-44-009/20/17 18:120.41 1
Fluorene ND mg/kg 09/21/17 20:06 86-73-709/20/17 18:120.41 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 20:06 87-68-309/20/17 18:120.41 1
Hexachlorobenzene ND mg/kg 09/21/17 20:06 118-74-109/20/17 18:120.41 1
Hexachlorocyclopentadiene ND mg/kg 09/21/17 20:06 77-47-409/20/17 18:120.41 1
Hexachloroethane ND mg/kg 09/21/17 20:06 67-72-109/20/17 18:120.41 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/21/17 20:06 193-39-509/20/17 18:120.41 1
Isophorone ND mg/kg 09/21/17 20:06 78-59-109/20/17 18:120.41 1
1-Methylnaphthalene ND mg/kg 09/21/17 20:06 90-12-009/20/17 18:120.41 1
2-Methylnaphthalene ND mg/kg 09/21/17 20:06 91-57-609/20/17 18:120.41 1
2-Methylphenol(o-Cresol)ND mg/kg 09/21/17 20:06 95-48-709/20/17 18:120.41 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/21/17 20:06 15831-10-409/20/17 18:120.41 1
Naphthalene ND mg/kg 09/21/17 20:06 91-20-309/20/17 18:120.41 1
2-Nitroaniline ND mg/kg 09/21/17 20:06 88-74-409/20/17 18:122.0 1
3-Nitroaniline ND mg/kg 09/21/17 20:06 99-09-209/20/17 18:122.0 1
4-Nitroaniline ND mg/kg 09/21/17 20:06 100-01-609/20/17 18:120.81 1
Nitrobenzene ND mg/kg 09/21/17 20:06 98-95-309/20/17 18:120.41 1
2-Nitrophenol ND mg/kg 09/21/17 20:06 88-75-509/20/17 18:120.41 1
4-Nitrophenol ND mg/kg 09/21/17 20:06 100-02-709/20/17 18:122.0 1
N-Nitrosodimethylamine ND mg/kg 09/21/17 20:06 62-75-909/20/17 18:120.41 1
N-Nitroso-di-n-propylamine ND mg/kg 09/21/17 20:06 621-64-709/20/17 18:120.41 1
N-Nitrosodiphenylamine ND mg/kg 09/21/17 20:06 86-30-609/20/17 18:120.41 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/21/17 20:06 108-60-109/20/17 18:120.41 1
Pentachlorophenol ND mg/kg 09/21/17 20:06 87-86-509/20/17 18:122.0 1
Phenanthrene ND mg/kg 09/21/17 20:06 85-01-809/20/17 18:120.41 1
Phenol ND mg/kg 09/21/17 20:06 108-95-209/20/17 18:120.41 1
Pyrene ND mg/kg 09/21/17 20:06 129-00-009/20/17 18:120.41 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 20:06 120-82-109/20/17 18:120.41 1
2,4,5-Trichlorophenol ND mg/kg 09/21/17 20:06 95-95-409/20/17 18:120.41 1
2,4,6-Trichlorophenol ND mg/kg 09/21/17 20:06 88-06-209/20/17 18:120.41 1
Surrogates
Nitrobenzene-d5 (S)52 %09/21/17 20:06 4165-60-009/20/17 18:1223-110 1
2-Fluorobiphenyl (S)49 %09/21/17 20:06 321-60-809/20/17 18:1230-110 1
Terphenyl-d14 (S)69 %09/21/17 20:06 1718-51-009/20/17 18:1228-110 1
Phenol-d6 (S)51 %09/21/17 20:06 13127-88-309/20/17 18:1222-110 1
2-Fluorophenol (S)51 %09/21/17 20:06 367-12-409/20/17 18:1213-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 56 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-4C Lab ID:92355949012 Collected:09/18/17 12:35 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)71 %09/21/17 20:06 118-79-609/20/17 18:1227-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/21/17 16:02 67-64-1 M12.9 25
Benzene ND mg/kg 09/21/17 16:02 71-43-20.14 25
Bromobenzene ND mg/kg 09/21/17 16:02 108-86-10.14 25
Bromochloromethane ND mg/kg 09/21/17 16:02 74-97-50.14 25
Bromodichloromethane ND mg/kg 09/21/17 16:02 75-27-40.14 25
Bromoform ND mg/kg 09/21/17 16:02 75-25-20.14 25
Bromomethane ND mg/kg 09/21/17 16:02 74-83-90.29 25
2-Butanone (MEK)ND mg/kg 09/21/17 16:02 78-93-3 M12.9 25
n-Butylbenzene ND mg/kg 09/21/17 16:02 104-51-8 M10.14 25
sec-Butylbenzene 0.21 mg/kg 09/21/17 16:02 135-98-80.14 25
tert-Butylbenzene ND mg/kg 09/21/17 16:02 98-06-60.14 25
Carbon tetrachloride ND mg/kg 09/21/17 16:02 56-23-50.14 25
Chlorobenzene ND mg/kg 09/21/17 16:02 108-90-70.14 25
Chloroethane ND mg/kg 09/21/17 16:02 75-00-3 M10.29 25
Chloroform ND mg/kg 09/21/17 16:02 67-66-30.14 25
Chloromethane ND mg/kg 09/21/17 16:02 74-87-30.29 25
2-Chlorotoluene ND mg/kg 09/21/17 16:02 95-49-80.14 25
4-Chlorotoluene ND mg/kg 09/21/17 16:02 106-43-40.14 25
1,2-Dibromo-3-chloropropane ND mg/kg 09/21/17 16:02 96-12-8 M10.14 25
Dibromochloromethane ND mg/kg 09/21/17 16:02 124-48-10.14 25
1,2-Dibromoethane (EDB)ND mg/kg 09/21/17 16:02 106-93-40.14 25
Dibromomethane ND mg/kg 09/21/17 16:02 74-95-30.14 25
1,2-Dichlorobenzene ND mg/kg 09/21/17 16:02 95-50-10.14 25
1,3-Dichlorobenzene ND mg/kg 09/21/17 16:02 541-73-10.14 25
1,4-Dichlorobenzene ND mg/kg 09/21/17 16:02 106-46-70.14 25
Dichlorodifluoromethane ND mg/kg 09/21/17 16:02 75-71-80.29 25
1,1-Dichloroethane ND mg/kg 09/21/17 16:02 75-34-30.14 25
1,2-Dichloroethane ND mg/kg 09/21/17 16:02 107-06-20.14 25
1,1-Dichloroethene ND mg/kg 09/21/17 16:02 75-35-40.14 25
cis-1,2-Dichloroethene ND mg/kg 09/21/17 16:02 156-59-20.14 25
trans-1,2-Dichloroethene ND mg/kg 09/21/17 16:02 156-60-50.14 25
1,2-Dichloropropane ND mg/kg 09/21/17 16:02 78-87-50.14 25
1,3-Dichloropropane ND mg/kg 09/21/17 16:02 142-28-90.14 25
2,2-Dichloropropane ND mg/kg 09/21/17 16:02 594-20-70.14 25
1,1-Dichloropropene ND mg/kg 09/21/17 16:02 563-58-60.14 25
cis-1,3-Dichloropropene ND mg/kg 09/21/17 16:02 10061-01-50.14 25
trans-1,3-Dichloropropene ND mg/kg 09/21/17 16:02 10061-02-60.14 25
Diisopropyl ether ND mg/kg 09/21/17 16:02 108-20-30.14 25
Ethylbenzene ND mg/kg 09/21/17 16:02 100-41-40.14 25
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 16:02 87-68-30.14 25
2-Hexanone ND mg/kg 09/21/17 16:02 591-78-6 M11.4 25
Isopropylbenzene (Cumene)ND mg/kg 09/21/17 16:02 98-82-80.14 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 57 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-4C Lab ID:92355949012 Collected:09/18/17 12:35 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene 0.28 mg/kg 09/21/17 16:02 99-87-60.14 25
Methylene Chloride ND mg/kg 09/21/17 16:02 75-09-20.58 25
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/21/17 16:02 108-10-1 M11.4 25
Methyl-tert-butyl ether ND mg/kg 09/21/17 16:02 1634-04-40.14 25
Naphthalene 0.30 mg/kg 09/21/17 16:02 91-20-30.14 25
n-Propylbenzene 0.71 mg/kg 09/21/17 16:02 103-65-10.14 25
Styrene ND mg/kg 09/21/17 16:02 100-42-50.14 25
1,1,1,2-Tetrachloroethane ND mg/kg 09/21/17 16:02 630-20-60.14 25
1,1,2,2-Tetrachloroethane ND mg/kg 09/21/17 16:02 79-34-50.14 25
Tetrachloroethene ND mg/kg 09/21/17 16:02 127-18-40.14 25
Toluene ND mg/kg 09/21/17 16:02 108-88-30.14 25
1,2,3-Trichlorobenzene ND mg/kg 09/21/17 16:02 87-61-60.14 25
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 16:02 120-82-10.14 25
1,1,1-Trichloroethane ND mg/kg 09/21/17 16:02 71-55-60.14 25
1,1,2-Trichloroethane ND mg/kg 09/21/17 16:02 79-00-5 M10.14 25
Trichloroethene ND mg/kg 09/21/17 16:02 79-01-60.14 25
Trichlorofluoromethane ND mg/kg 09/21/17 16:02 75-69-4 M10.14 25
1,2,3-Trichloropropane ND mg/kg 09/21/17 16:02 96-18-4 M10.14 25
1,2,4-Trimethylbenzene 1.6 mg/kg 09/21/17 16:02 95-63-60.14 25
1,3,5-Trimethylbenzene 0.42 mg/kg 09/21/17 16:02 108-67-80.14 25
Vinyl acetate ND mg/kg 09/21/17 16:02 108-05-4 M11.4 25
Vinyl chloride ND mg/kg 09/21/17 16:02 75-01-40.29 25
Xylene (Total)ND mg/kg 09/21/17 16:02 1330-20-70.29 25
m&p-Xylene ND mg/kg 09/21/17 16:02 179601-23-10.29 25
o-Xylene ND mg/kg 09/21/17 16:02 95-47-60.14 25
Surrogates
Toluene-d8 (S)97 %09/21/17 16:02 2037-26-5 D370-130 25
4-Bromofluorobenzene (S)98 %09/21/17 16:02 460-00-470-130 25
1,2-Dichloroethane-d4 (S)118 %09/21/17 16:02 17060-07-070-132 25
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.3 %09/21/17 11:120.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 58 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-5A Lab ID:92355949013 Collected:09/18/17 15:25 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/22/17 13:01 N209/21/17 08:0512.6 1
Aliphatic (C19-C36)ND mg/kg 09/22/17 13:01 N209/21/17 08:0512.6 1
Aromatic (C11-C22)34.8 mg/kg 09/22/17 13:01 N209/21/17 08:0512.6 1
Surrogates
Nonatriacontane (S)76 %09/22/17 13:01 7194-86-709/21/17 08:0540-140 1
o-Terphenyl (S)95 %09/22/17 13:01 84-15-109/21/17 08:0540-140 1
2-Fluorobiphenyl (S)117 %09/22/17 13:01 321-60-809/21/17 08:0540-140 1
2-Bromonaphthalene (S)111 %09/22/17 13:01 580-13-209/21/17 08:0540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/21/17 21:13 N209/21/17 10:454.0 1
Aliphatic (C09-C12)ND mg/kg 09/21/17 21:13 N209/21/17 10:454.0 1
Aromatic (C09-C10)ND mg/kg 09/21/17 21:13 N209/21/17 10:454.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)104 %09/21/17 21:13 460-00-409/21/17 10:4570-130 1
4-Bromofluorobenzene (PID) (S)98 %09/21/17 21:13 460-00-409/21/17 10:4570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/22/17 18:17 83-32-909/20/17 18:124.1 10
Acenaphthylene ND mg/kg 09/22/17 18:17 208-96-809/20/17 18:124.1 10
Aniline ND mg/kg 09/22/17 18:17 62-53-309/20/17 18:124.1 10
Anthracene ND mg/kg 09/22/17 18:17 120-12-709/20/17 18:124.1 10
Benzo(a)anthracene ND mg/kg 09/22/17 18:17 56-55-309/20/17 18:124.1 10
Benzo(a)pyrene ND mg/kg 09/22/17 18:17 50-32-809/20/17 18:124.1 10
Benzo(b)fluoranthene ND mg/kg 09/22/17 18:17 205-99-209/20/17 18:124.1 10
Benzo(g,h,i)perylene ND mg/kg 09/22/17 18:17 191-24-209/20/17 18:124.1 10
Benzo(k)fluoranthene ND mg/kg 09/22/17 18:17 207-08-909/20/17 18:124.1 10
Benzoic Acid ND mg/kg 09/22/17 18:17 65-85-009/20/17 18:1220.5 10
Benzyl alcohol ND mg/kg 09/22/17 18:17 100-51-609/20/17 18:128.2 10
4-Bromophenylphenyl ether ND mg/kg 09/22/17 18:17 101-55-309/20/17 18:124.1 10
Butylbenzylphthalate ND mg/kg 09/22/17 18:17 85-68-709/20/17 18:124.1 10
4-Chloro-3-methylphenol ND mg/kg 09/22/17 18:17 59-50-709/20/17 18:128.2 10
4-Chloroaniline ND mg/kg 09/22/17 18:17 106-47-809/20/17 18:1220.5 10
bis(2-Chloroethoxy)methane ND mg/kg 09/22/17 18:17 111-91-109/20/17 18:124.1 10
bis(2-Chloroethyl) ether ND mg/kg 09/22/17 18:17 111-44-409/20/17 18:124.1 10
2-Chloronaphthalene ND mg/kg 09/22/17 18:17 91-58-709/20/17 18:124.1 10
2-Chlorophenol ND mg/kg 09/22/17 18:17 95-57-809/20/17 18:124.1 10
4-Chlorophenylphenyl ether ND mg/kg 09/22/17 18:17 7005-72-309/20/17 18:124.1 10
Chrysene ND mg/kg 09/22/17 18:17 218-01-909/20/17 18:124.1 10
Dibenz(a,h)anthracene ND mg/kg 09/22/17 18:17 53-70-309/20/17 18:124.1 10
Dibenzofuran ND mg/kg 09/22/17 18:17 132-64-909/20/17 18:124.1 10
1,2-Dichlorobenzene ND mg/kg 09/22/17 18:17 95-50-109/20/17 18:124.1 10
1,3-Dichlorobenzene ND mg/kg 09/22/17 18:17 541-73-109/20/17 18:124.1 10
1,4-Dichlorobenzene ND mg/kg 09/22/17 18:17 106-46-709/20/17 18:124.1 10
3,3'-Dichlorobenzidine ND mg/kg 09/22/17 18:17 91-94-109/20/17 18:1220.5 10
2,4-Dichlorophenol ND mg/kg 09/22/17 18:17 120-83-209/20/17 18:124.1 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 59 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-5A Lab ID:92355949013 Collected:09/18/17 15:25 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/22/17 18:17 84-66-209/20/17 18:124.1 10
2,4-Dimethylphenol ND mg/kg 09/22/17 18:17 105-67-909/20/17 18:124.1 10
Dimethylphthalate ND mg/kg 09/22/17 18:17 131-11-309/20/17 18:124.1 10
Di-n-butylphthalate ND mg/kg 09/22/17 18:17 84-74-209/20/17 18:124.1 10
4,6-Dinitro-2-methylphenol ND mg/kg 09/22/17 18:17 534-52-109/20/17 18:128.2 10
2,4-Dinitrophenol ND mg/kg 09/22/17 18:17 51-28-509/20/17 18:1220.5 10
2,4-Dinitrotoluene ND mg/kg 09/22/17 18:17 121-14-209/20/17 18:124.1 10
2,6-Dinitrotoluene ND mg/kg 09/22/17 18:17 606-20-209/20/17 18:124.1 10
Di-n-octylphthalate ND mg/kg 09/22/17 18:17 117-84-009/20/17 18:124.1 10
bis(2-Ethylhexyl)phthalate ND mg/kg 09/22/17 18:17 117-81-709/20/17 18:124.1 10
Fluoranthene ND mg/kg 09/22/17 18:17 206-44-009/20/17 18:124.1 10
Fluorene ND mg/kg 09/22/17 18:17 86-73-709/20/17 18:124.1 10
Hexachloro-1,3-butadiene ND mg/kg 09/22/17 18:17 87-68-309/20/17 18:124.1 10
Hexachlorobenzene ND mg/kg 09/22/17 18:17 118-74-109/20/17 18:124.1 10
Hexachlorocyclopentadiene ND mg/kg 09/22/17 18:17 77-47-409/20/17 18:124.1 10
Hexachloroethane ND mg/kg 09/22/17 18:17 67-72-109/20/17 18:124.1 10
Indeno(1,2,3-cd)pyrene ND mg/kg 09/22/17 18:17 193-39-509/20/17 18:124.1 10
Isophorone ND mg/kg 09/22/17 18:17 78-59-109/20/17 18:124.1 10
1-Methylnaphthalene ND mg/kg 09/22/17 18:17 90-12-009/20/17 18:124.1 10
2-Methylnaphthalene ND mg/kg 09/22/17 18:17 91-57-609/20/17 18:124.1 10
2-Methylphenol(o-Cresol)ND mg/kg 09/22/17 18:17 95-48-709/20/17 18:124.1 10
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/22/17 18:17 15831-10-409/20/17 18:124.1 10
Naphthalene ND mg/kg 09/22/17 18:17 91-20-309/20/17 18:124.1 10
2-Nitroaniline ND mg/kg 09/22/17 18:17 88-74-409/20/17 18:1220.5 10
3-Nitroaniline ND mg/kg 09/22/17 18:17 99-09-209/20/17 18:1220.5 10
4-Nitroaniline ND mg/kg 09/22/17 18:17 100-01-609/20/17 18:128.2 10
Nitrobenzene ND mg/kg 09/22/17 18:17 98-95-309/20/17 18:124.1 10
2-Nitrophenol ND mg/kg 09/22/17 18:17 88-75-509/20/17 18:124.1 10
4-Nitrophenol ND mg/kg 09/22/17 18:17 100-02-709/20/17 18:1220.5 10
N-Nitrosodimethylamine ND mg/kg 09/22/17 18:17 62-75-909/20/17 18:124.1 10
N-Nitroso-di-n-propylamine ND mg/kg 09/22/17 18:17 621-64-709/20/17 18:124.1 10
N-Nitrosodiphenylamine ND mg/kg 09/22/17 18:17 86-30-609/20/17 18:124.1 10
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/22/17 18:17 108-60-109/20/17 18:124.1 10
Pentachlorophenol ND mg/kg 09/22/17 18:17 87-86-509/20/17 18:1220.5 10
Phenanthrene ND mg/kg 09/22/17 18:17 85-01-809/20/17 18:124.1 10
Phenol ND mg/kg 09/22/17 18:17 108-95-209/20/17 18:124.1 10
Pyrene ND mg/kg 09/22/17 18:17 129-00-009/20/17 18:124.1 10
1,2,4-Trichlorobenzene ND mg/kg 09/22/17 18:17 120-82-109/20/17 18:124.1 10
2,4,5-Trichlorophenol ND mg/kg 09/22/17 18:17 95-95-409/20/17 18:124.1 10
2,4,6-Trichlorophenol ND mg/kg 09/22/17 18:17 88-06-209/20/17 18:124.1 10
Surrogates
Nitrobenzene-d5 (S)0 %09/22/17 18:17 4165-60-0 D3,S409/20/17 18:1223-110 10
2-Fluorobiphenyl (S)0 %09/22/17 18:17 321-60-8 S409/20/17 18:1230-110 10
Terphenyl-d14 (S)0 %09/22/17 18:17 1718-51-0 S409/20/17 18:1228-110 10
Phenol-d6 (S)0 %09/22/17 18:17 13127-88-3 S409/20/17 18:1222-110 10
2-Fluorophenol (S)0 %09/22/17 18:17 367-12-4 S409/20/17 18:1213-110 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 60 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-5A Lab ID:92355949013 Collected:09/18/17 15:25 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)0 %09/22/17 18:17 118-79-6 S409/20/17 18:1227-110 10
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/22/17 14:06 67-64-1 L10.10 1
Benzene ND mg/kg 09/22/17 14:06 71-43-20.0051 1
Bromobenzene ND mg/kg 09/22/17 14:06 108-86-10.0051 1
Bromochloromethane ND mg/kg 09/22/17 14:06 74-97-50.0051 1
Bromodichloromethane ND mg/kg 09/22/17 14:06 75-27-40.0051 1
Bromoform ND mg/kg 09/22/17 14:06 75-25-20.0051 1
Bromomethane ND mg/kg 09/22/17 14:06 74-83-90.010 1
2-Butanone (MEK)ND mg/kg 09/22/17 14:06 78-93-30.10 1
n-Butylbenzene ND mg/kg 09/22/17 14:06 104-51-80.0051 1
sec-Butylbenzene ND mg/kg 09/22/17 14:06 135-98-80.0051 1
tert-Butylbenzene ND mg/kg 09/22/17 14:06 98-06-60.0051 1
Carbon tetrachloride ND mg/kg 09/22/17 14:06 56-23-50.0051 1
Chlorobenzene ND mg/kg 09/22/17 14:06 108-90-70.0051 1
Chloroethane ND mg/kg 09/22/17 14:06 75-00-30.010 1
Chloroform ND mg/kg 09/22/17 14:06 67-66-30.0051 1
Chloromethane ND mg/kg 09/22/17 14:06 74-87-30.010 1
2-Chlorotoluene ND mg/kg 09/22/17 14:06 95-49-80.0051 1
4-Chlorotoluene ND mg/kg 09/22/17 14:06 106-43-40.0051 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/22/17 14:06 96-12-80.0051 1
Dibromochloromethane ND mg/kg 09/22/17 14:06 124-48-10.0051 1
1,2-Dibromoethane (EDB)ND mg/kg 09/22/17 14:06 106-93-40.0051 1
Dibromomethane ND mg/kg 09/22/17 14:06 74-95-30.0051 1
1,2-Dichlorobenzene ND mg/kg 09/22/17 14:06 95-50-10.0051 1
1,3-Dichlorobenzene ND mg/kg 09/22/17 14:06 541-73-10.0051 1
1,4-Dichlorobenzene ND mg/kg 09/22/17 14:06 106-46-70.0051 1
Dichlorodifluoromethane ND mg/kg 09/22/17 14:06 75-71-80.010 1
1,1-Dichloroethane ND mg/kg 09/22/17 14:06 75-34-30.0051 1
1,2-Dichloroethane ND mg/kg 09/22/17 14:06 107-06-20.0051 1
1,1-Dichloroethene ND mg/kg 09/22/17 14:06 75-35-40.0051 1
cis-1,2-Dichloroethene ND mg/kg 09/22/17 14:06 156-59-20.0051 1
trans-1,2-Dichloroethene ND mg/kg 09/22/17 14:06 156-60-50.0051 1
1,2-Dichloropropane ND mg/kg 09/22/17 14:06 78-87-50.0051 1
1,3-Dichloropropane ND mg/kg 09/22/17 14:06 142-28-90.0051 1
2,2-Dichloropropane ND mg/kg 09/22/17 14:06 594-20-70.0051 1
1,1-Dichloropropene ND mg/kg 09/22/17 14:06 563-58-60.0051 1
cis-1,3-Dichloropropene ND mg/kg 09/22/17 14:06 10061-01-50.0051 1
trans-1,3-Dichloropropene ND mg/kg 09/22/17 14:06 10061-02-60.0051 1
Diisopropyl ether ND mg/kg 09/22/17 14:06 108-20-30.0051 1
Ethylbenzene ND mg/kg 09/22/17 14:06 100-41-40.0051 1
Hexachloro-1,3-butadiene ND mg/kg 09/22/17 14:06 87-68-30.0051 1
2-Hexanone ND mg/kg 09/22/17 14:06 591-78-60.051 1
Isopropylbenzene (Cumene)ND mg/kg 09/22/17 14:06 98-82-80.0051 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 61 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-5A Lab ID:92355949013 Collected:09/18/17 15:25 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND mg/kg 09/22/17 14:06 99-87-60.0051 1
Methylene Chloride ND mg/kg 09/22/17 14:06 75-09-20.020 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/22/17 14:06 108-10-10.051 1
Methyl-tert-butyl ether ND mg/kg 09/22/17 14:06 1634-04-40.0051 1
Naphthalene ND mg/kg 09/22/17 14:06 91-20-30.0051 1
n-Propylbenzene ND mg/kg 09/22/17 14:06 103-65-10.0051 1
Styrene ND mg/kg 09/22/17 14:06 100-42-50.0051 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/22/17 14:06 630-20-60.0051 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/22/17 14:06 79-34-50.0051 1
Tetrachloroethene ND mg/kg 09/22/17 14:06 127-18-40.0051 1
Toluene ND mg/kg 09/22/17 14:06 108-88-30.0051 1
1,2,3-Trichlorobenzene ND mg/kg 09/22/17 14:06 87-61-60.0051 1
1,2,4-Trichlorobenzene ND mg/kg 09/22/17 14:06 120-82-10.0051 1
1,1,1-Trichloroethane ND mg/kg 09/22/17 14:06 71-55-60.0051 1
1,1,2-Trichloroethane ND mg/kg 09/22/17 14:06 79-00-50.0051 1
Trichloroethene ND mg/kg 09/22/17 14:06 79-01-60.0051 1
Trichlorofluoromethane ND mg/kg 09/22/17 14:06 75-69-40.0051 1
1,2,3-Trichloropropane ND mg/kg 09/22/17 14:06 96-18-40.0051 1
1,2,4-Trimethylbenzene ND mg/kg 09/22/17 14:06 95-63-60.0051 1
1,3,5-Trimethylbenzene ND mg/kg 09/22/17 14:06 108-67-80.0051 1
Vinyl acetate ND mg/kg 09/22/17 14:06 108-05-40.051 1
Vinyl chloride ND mg/kg 09/22/17 14:06 75-01-40.010 1
Xylene (Total)ND mg/kg 09/22/17 14:06 1330-20-70.010 1
m&p-Xylene ND mg/kg 09/22/17 14:06 179601-23-10.010 1
o-Xylene ND mg/kg 09/22/17 14:06 95-47-60.0051 1
Surrogates
Toluene-d8 (S)101 %09/22/17 14:06 2037-26-570-130 1
4-Bromofluorobenzene (S)100 %09/22/17 14:06 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %09/22/17 14:06 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.9 %09/21/17 11:120.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 62 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-5B Lab ID:92355949014 Collected:09/18/17 15:35 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/21/17 20:16 N209/21/17 08:0513.1 1
Aliphatic (C19-C36)36.2 mg/kg 09/21/17 20:16 N209/21/17 08:0513.1 1
Aromatic (C11-C22)ND mg/kg 09/21/17 20:16 N209/21/17 08:0513.1 1
Surrogates
Nonatriacontane (S)67 %09/21/17 20:16 7194-86-709/21/17 08:0540-140 1
o-Terphenyl (S)83 %09/21/17 20:16 84-15-109/21/17 08:0540-140 1
2-Fluorobiphenyl (S)108 %09/21/17 20:16 321-60-809/21/17 08:0540-140 1
2-Bromonaphthalene (S)93 %09/21/17 20:16 580-13-209/21/17 08:0540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/21/17 21:41 N209/21/17 10:453.7 1
Aliphatic (C09-C12)ND mg/kg 09/21/17 21:41 N209/21/17 10:453.7 1
Aromatic (C09-C10)ND mg/kg 09/21/17 21:41 N209/21/17 10:453.7 1
Surrogates
4-Bromofluorobenzene (FID) (S)103 %09/21/17 21:41 460-00-409/21/17 10:4570-130 1
4-Bromofluorobenzene (PID) (S)98 %09/21/17 21:41 460-00-409/21/17 10:4570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/21/17 20:35 83-32-909/20/17 18:120.44 1
Acenaphthylene ND mg/kg 09/21/17 20:35 208-96-809/20/17 18:120.44 1
Aniline ND mg/kg 09/21/17 20:35 62-53-309/20/17 18:120.44 1
Anthracene ND mg/kg 09/21/17 20:35 120-12-709/20/17 18:120.44 1
Benzo(a)anthracene ND mg/kg 09/21/17 20:35 56-55-309/20/17 18:120.44 1
Benzo(a)pyrene ND mg/kg 09/21/17 20:35 50-32-809/20/17 18:120.44 1
Benzo(b)fluoranthene ND mg/kg 09/21/17 20:35 205-99-209/20/17 18:120.44 1
Benzo(g,h,i)perylene ND mg/kg 09/21/17 20:35 191-24-209/20/17 18:120.44 1
Benzo(k)fluoranthene ND mg/kg 09/21/17 20:35 207-08-909/20/17 18:120.44 1
Benzoic Acid ND mg/kg 09/21/17 20:35 65-85-009/20/17 18:122.2 1
Benzyl alcohol ND mg/kg 09/21/17 20:35 100-51-609/20/17 18:120.87 1
4-Bromophenylphenyl ether ND mg/kg 09/21/17 20:35 101-55-309/20/17 18:120.44 1
Butylbenzylphthalate ND mg/kg 09/21/17 20:35 85-68-709/20/17 18:120.44 1
4-Chloro-3-methylphenol ND mg/kg 09/21/17 20:35 59-50-709/20/17 18:120.87 1
4-Chloroaniline ND mg/kg 09/21/17 20:35 106-47-809/20/17 18:122.2 1
bis(2-Chloroethoxy)methane ND mg/kg 09/21/17 20:35 111-91-109/20/17 18:120.44 1
bis(2-Chloroethyl) ether ND mg/kg 09/21/17 20:35 111-44-409/20/17 18:120.44 1
2-Chloronaphthalene ND mg/kg 09/21/17 20:35 91-58-709/20/17 18:120.44 1
2-Chlorophenol ND mg/kg 09/21/17 20:35 95-57-809/20/17 18:120.44 1
4-Chlorophenylphenyl ether ND mg/kg 09/21/17 20:35 7005-72-309/20/17 18:120.44 1
Chrysene ND mg/kg 09/21/17 20:35 218-01-909/20/17 18:120.44 1
Dibenz(a,h)anthracene ND mg/kg 09/21/17 20:35 53-70-309/20/17 18:120.44 1
Dibenzofuran ND mg/kg 09/21/17 20:35 132-64-909/20/17 18:120.44 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 20:35 95-50-109/20/17 18:120.44 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 20:35 541-73-109/20/17 18:120.44 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 20:35 106-46-709/20/17 18:120.44 1
3,3'-Dichlorobenzidine ND mg/kg 09/21/17 20:35 91-94-109/20/17 18:122.2 1
2,4-Dichlorophenol ND mg/kg 09/21/17 20:35 120-83-209/20/17 18:120.44 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 63 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-5B Lab ID:92355949014 Collected:09/18/17 15:35 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/21/17 20:35 84-66-209/20/17 18:120.44 1
2,4-Dimethylphenol ND mg/kg 09/21/17 20:35 105-67-909/20/17 18:120.44 1
Dimethylphthalate ND mg/kg 09/21/17 20:35 131-11-309/20/17 18:120.44 1
Di-n-butylphthalate ND mg/kg 09/21/17 20:35 84-74-209/20/17 18:120.44 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/21/17 20:35 534-52-109/20/17 18:120.87 1
2,4-Dinitrophenol ND mg/kg 09/21/17 20:35 51-28-509/20/17 18:122.2 1
2,4-Dinitrotoluene ND mg/kg 09/21/17 20:35 121-14-209/20/17 18:120.44 1
2,6-Dinitrotoluene ND mg/kg 09/21/17 20:35 606-20-209/20/17 18:120.44 1
Di-n-octylphthalate ND mg/kg 09/21/17 20:35 117-84-009/20/17 18:120.44 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/21/17 20:35 117-81-709/20/17 18:120.44 1
Fluoranthene ND mg/kg 09/21/17 20:35 206-44-009/20/17 18:120.44 1
Fluorene ND mg/kg 09/21/17 20:35 86-73-709/20/17 18:120.44 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 20:35 87-68-309/20/17 18:120.44 1
Hexachlorobenzene ND mg/kg 09/21/17 20:35 118-74-109/20/17 18:120.44 1
Hexachlorocyclopentadiene ND mg/kg 09/21/17 20:35 77-47-409/20/17 18:120.44 1
Hexachloroethane ND mg/kg 09/21/17 20:35 67-72-109/20/17 18:120.44 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/21/17 20:35 193-39-509/20/17 18:120.44 1
Isophorone ND mg/kg 09/21/17 20:35 78-59-109/20/17 18:120.44 1
1-Methylnaphthalene ND mg/kg 09/21/17 20:35 90-12-009/20/17 18:120.44 1
2-Methylnaphthalene ND mg/kg 09/21/17 20:35 91-57-609/20/17 18:120.44 1
2-Methylphenol(o-Cresol)ND mg/kg 09/21/17 20:35 95-48-709/20/17 18:120.44 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/21/17 20:35 15831-10-409/20/17 18:120.44 1
Naphthalene ND mg/kg 09/21/17 20:35 91-20-309/20/17 18:120.44 1
2-Nitroaniline ND mg/kg 09/21/17 20:35 88-74-409/20/17 18:122.2 1
3-Nitroaniline ND mg/kg 09/21/17 20:35 99-09-209/20/17 18:122.2 1
4-Nitroaniline ND mg/kg 09/21/17 20:35 100-01-609/20/17 18:120.87 1
Nitrobenzene ND mg/kg 09/21/17 20:35 98-95-309/20/17 18:120.44 1
2-Nitrophenol ND mg/kg 09/21/17 20:35 88-75-509/20/17 18:120.44 1
4-Nitrophenol ND mg/kg 09/21/17 20:35 100-02-709/20/17 18:122.2 1
N-Nitrosodimethylamine ND mg/kg 09/21/17 20:35 62-75-909/20/17 18:120.44 1
N-Nitroso-di-n-propylamine ND mg/kg 09/21/17 20:35 621-64-709/20/17 18:120.44 1
N-Nitrosodiphenylamine ND mg/kg 09/21/17 20:35 86-30-609/20/17 18:120.44 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/21/17 20:35 108-60-109/20/17 18:120.44 1
Pentachlorophenol ND mg/kg 09/21/17 20:35 87-86-509/20/17 18:122.2 1
Phenanthrene ND mg/kg 09/21/17 20:35 85-01-809/20/17 18:120.44 1
Phenol ND mg/kg 09/21/17 20:35 108-95-209/20/17 18:120.44 1
Pyrene ND mg/kg 09/21/17 20:35 129-00-009/20/17 18:120.44 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 20:35 120-82-109/20/17 18:120.44 1
2,4,5-Trichlorophenol ND mg/kg 09/21/17 20:35 95-95-409/20/17 18:120.44 1
2,4,6-Trichlorophenol ND mg/kg 09/21/17 20:35 88-06-209/20/17 18:120.44 1
Surrogates
Nitrobenzene-d5 (S)44 %09/21/17 20:35 4165-60-009/20/17 18:1223-110 1
2-Fluorobiphenyl (S)42 %09/21/17 20:35 321-60-809/20/17 18:1230-110 1
Terphenyl-d14 (S)84 %09/21/17 20:35 1718-51-009/20/17 18:1228-110 1
Phenol-d6 (S)44 %09/21/17 20:35 13127-88-309/20/17 18:1222-110 1
2-Fluorophenol (S)43 %09/21/17 20:35 367-12-409/20/17 18:1213-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 64 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-5B Lab ID:92355949014 Collected:09/18/17 15:35 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)76 %09/21/17 20:35 118-79-609/20/17 18:1227-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/22/17 14:25 67-64-1 L10.12 1
Benzene ND mg/kg 09/22/17 14:25 71-43-20.0061 1
Bromobenzene ND mg/kg 09/22/17 14:25 108-86-10.0061 1
Bromochloromethane ND mg/kg 09/22/17 14:25 74-97-50.0061 1
Bromodichloromethane ND mg/kg 09/22/17 14:25 75-27-40.0061 1
Bromoform ND mg/kg 09/22/17 14:25 75-25-20.0061 1
Bromomethane ND mg/kg 09/22/17 14:25 74-83-90.012 1
2-Butanone (MEK)ND mg/kg 09/22/17 14:25 78-93-30.12 1
n-Butylbenzene ND mg/kg 09/22/17 14:25 104-51-80.0061 1
sec-Butylbenzene ND mg/kg 09/22/17 14:25 135-98-80.0061 1
tert-Butylbenzene ND mg/kg 09/22/17 14:25 98-06-60.0061 1
Carbon tetrachloride ND mg/kg 09/22/17 14:25 56-23-50.0061 1
Chlorobenzene ND mg/kg 09/22/17 14:25 108-90-70.0061 1
Chloroethane ND mg/kg 09/22/17 14:25 75-00-30.012 1
Chloroform ND mg/kg 09/22/17 14:25 67-66-30.0061 1
Chloromethane ND mg/kg 09/22/17 14:25 74-87-30.012 1
2-Chlorotoluene ND mg/kg 09/22/17 14:25 95-49-80.0061 1
4-Chlorotoluene ND mg/kg 09/22/17 14:25 106-43-40.0061 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/22/17 14:25 96-12-80.0061 1
Dibromochloromethane ND mg/kg 09/22/17 14:25 124-48-10.0061 1
1,2-Dibromoethane (EDB)ND mg/kg 09/22/17 14:25 106-93-40.0061 1
Dibromomethane ND mg/kg 09/22/17 14:25 74-95-30.0061 1
1,2-Dichlorobenzene ND mg/kg 09/22/17 14:25 95-50-10.0061 1
1,3-Dichlorobenzene ND mg/kg 09/22/17 14:25 541-73-10.0061 1
1,4-Dichlorobenzene ND mg/kg 09/22/17 14:25 106-46-70.0061 1
Dichlorodifluoromethane ND mg/kg 09/22/17 14:25 75-71-80.012 1
1,1-Dichloroethane ND mg/kg 09/22/17 14:25 75-34-30.0061 1
1,2-Dichloroethane ND mg/kg 09/22/17 14:25 107-06-20.0061 1
1,1-Dichloroethene ND mg/kg 09/22/17 14:25 75-35-40.0061 1
cis-1,2-Dichloroethene ND mg/kg 09/22/17 14:25 156-59-20.0061 1
trans-1,2-Dichloroethene ND mg/kg 09/22/17 14:25 156-60-50.0061 1
1,2-Dichloropropane ND mg/kg 09/22/17 14:25 78-87-50.0061 1
1,3-Dichloropropane ND mg/kg 09/22/17 14:25 142-28-90.0061 1
2,2-Dichloropropane ND mg/kg 09/22/17 14:25 594-20-70.0061 1
1,1-Dichloropropene ND mg/kg 09/22/17 14:25 563-58-60.0061 1
cis-1,3-Dichloropropene ND mg/kg 09/22/17 14:25 10061-01-50.0061 1
trans-1,3-Dichloropropene ND mg/kg 09/22/17 14:25 10061-02-60.0061 1
Diisopropyl ether ND mg/kg 09/22/17 14:25 108-20-30.0061 1
Ethylbenzene ND mg/kg 09/22/17 14:25 100-41-40.0061 1
Hexachloro-1,3-butadiene ND mg/kg 09/22/17 14:25 87-68-30.0061 1
2-Hexanone ND mg/kg 09/22/17 14:25 591-78-60.061 1
Isopropylbenzene (Cumene)ND mg/kg 09/22/17 14:25 98-82-80.0061 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 65 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-5B Lab ID:92355949014 Collected:09/18/17 15:35 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND mg/kg 09/22/17 14:25 99-87-60.0061 1
Methylene Chloride ND mg/kg 09/22/17 14:25 75-09-20.024 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/22/17 14:25 108-10-10.061 1
Methyl-tert-butyl ether ND mg/kg 09/22/17 14:25 1634-04-40.0061 1
Naphthalene ND mg/kg 09/22/17 14:25 91-20-30.0061 1
n-Propylbenzene ND mg/kg 09/22/17 14:25 103-65-10.0061 1
Styrene ND mg/kg 09/22/17 14:25 100-42-50.0061 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/22/17 14:25 630-20-60.0061 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/22/17 14:25 79-34-50.0061 1
Tetrachloroethene ND mg/kg 09/22/17 14:25 127-18-40.0061 1
Toluene ND mg/kg 09/22/17 14:25 108-88-30.0061 1
1,2,3-Trichlorobenzene ND mg/kg 09/22/17 14:25 87-61-60.0061 1
1,2,4-Trichlorobenzene ND mg/kg 09/22/17 14:25 120-82-10.0061 1
1,1,1-Trichloroethane ND mg/kg 09/22/17 14:25 71-55-60.0061 1
1,1,2-Trichloroethane ND mg/kg 09/22/17 14:25 79-00-50.0061 1
Trichloroethene ND mg/kg 09/22/17 14:25 79-01-60.0061 1
Trichlorofluoromethane ND mg/kg 09/22/17 14:25 75-69-40.0061 1
1,2,3-Trichloropropane ND mg/kg 09/22/17 14:25 96-18-40.0061 1
1,2,4-Trimethylbenzene 0.010 mg/kg 09/22/17 14:25 95-63-60.0061 1
1,3,5-Trimethylbenzene ND mg/kg 09/22/17 14:25 108-67-80.0061 1
Vinyl acetate ND mg/kg 09/22/17 14:25 108-05-40.061 1
Vinyl chloride ND mg/kg 09/22/17 14:25 75-01-40.012 1
Xylene (Total)ND mg/kg 09/22/17 14:25 1330-20-70.012 1
m&p-Xylene ND mg/kg 09/22/17 14:25 179601-23-10.012 1
o-Xylene ND mg/kg 09/22/17 14:25 95-47-60.0061 1
Surrogates
Toluene-d8 (S)104 %09/22/17 14:25 2037-26-570-130 1
4-Bromofluorobenzene (S)99 %09/22/17 14:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)111 %09/22/17 14:25 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 24.5 %09/21/17 11:120.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 66 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-5C Lab ID:92355949015 Collected:09/18/17 15:45 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/22/17 13:29 N209/21/17 08:0511.4 1
Aliphatic (C19-C36)ND mg/kg 09/22/17 13:29 N209/21/17 08:0511.4 1
Aromatic (C11-C22)ND mg/kg 09/22/17 13:29 N209/21/17 08:0511.4 1
Surrogates
Nonatriacontane (S)63 %09/22/17 13:29 7194-86-709/21/17 08:0540-140 1
o-Terphenyl (S)71 %09/22/17 13:29 84-15-109/21/17 08:0540-140 1
2-Fluorobiphenyl (S)100 %09/22/17 13:29 321-60-809/21/17 08:0540-140 1
2-Bromonaphthalene (S)92 %09/22/17 13:29 580-13-209/21/17 08:0540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/21/17 22:09 N209/21/17 10:452.8 1
Aliphatic (C09-C12)ND mg/kg 09/21/17 22:09 N209/21/17 10:452.8 1
Aromatic (C09-C10)ND mg/kg 09/21/17 22:09 N209/21/17 10:452.8 1
Surrogates
4-Bromofluorobenzene (FID) (S)102 %09/21/17 22:09 460-00-409/21/17 10:4570-130 1
4-Bromofluorobenzene (PID) (S)97 %09/21/17 22:09 460-00-409/21/17 10:4570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/21/17 21:03 83-32-909/20/17 18:120.38 1
Acenaphthylene ND mg/kg 09/21/17 21:03 208-96-809/20/17 18:120.38 1
Aniline ND mg/kg 09/21/17 21:03 62-53-309/20/17 18:120.38 1
Anthracene ND mg/kg 09/21/17 21:03 120-12-709/20/17 18:120.38 1
Benzo(a)anthracene ND mg/kg 09/21/17 21:03 56-55-309/20/17 18:120.38 1
Benzo(a)pyrene ND mg/kg 09/21/17 21:03 50-32-809/20/17 18:120.38 1
Benzo(b)fluoranthene ND mg/kg 09/21/17 21:03 205-99-209/20/17 18:120.38 1
Benzo(g,h,i)perylene ND mg/kg 09/21/17 21:03 191-24-209/20/17 18:120.38 1
Benzo(k)fluoranthene ND mg/kg 09/21/17 21:03 207-08-909/20/17 18:120.38 1
Benzoic Acid ND mg/kg 09/21/17 21:03 65-85-009/20/17 18:121.9 1
Benzyl alcohol ND mg/kg 09/21/17 21:03 100-51-609/20/17 18:120.76 1
4-Bromophenylphenyl ether ND mg/kg 09/21/17 21:03 101-55-309/20/17 18:120.38 1
Butylbenzylphthalate ND mg/kg 09/21/17 21:03 85-68-709/20/17 18:120.38 1
4-Chloro-3-methylphenol ND mg/kg 09/21/17 21:03 59-50-709/20/17 18:120.76 1
4-Chloroaniline ND mg/kg 09/21/17 21:03 106-47-809/20/17 18:121.9 1
bis(2-Chloroethoxy)methane ND mg/kg 09/21/17 21:03 111-91-109/20/17 18:120.38 1
bis(2-Chloroethyl) ether ND mg/kg 09/21/17 21:03 111-44-409/20/17 18:120.38 1
2-Chloronaphthalene ND mg/kg 09/21/17 21:03 91-58-709/20/17 18:120.38 1
2-Chlorophenol ND mg/kg 09/21/17 21:03 95-57-809/20/17 18:120.38 1
4-Chlorophenylphenyl ether ND mg/kg 09/21/17 21:03 7005-72-309/20/17 18:120.38 1
Chrysene ND mg/kg 09/21/17 21:03 218-01-909/20/17 18:120.38 1
Dibenz(a,h)anthracene ND mg/kg 09/21/17 21:03 53-70-309/20/17 18:120.38 1
Dibenzofuran ND mg/kg 09/21/17 21:03 132-64-909/20/17 18:120.38 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 21:03 95-50-109/20/17 18:120.38 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 21:03 541-73-109/20/17 18:120.38 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 21:03 106-46-709/20/17 18:120.38 1
3,3'-Dichlorobenzidine ND mg/kg 09/21/17 21:03 91-94-109/20/17 18:121.9 1
2,4-Dichlorophenol ND mg/kg 09/21/17 21:03 120-83-209/20/17 18:120.38 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 67 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-5C Lab ID:92355949015 Collected:09/18/17 15:45 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/21/17 21:03 84-66-209/20/17 18:120.38 1
2,4-Dimethylphenol ND mg/kg 09/21/17 21:03 105-67-909/20/17 18:120.38 1
Dimethylphthalate ND mg/kg 09/21/17 21:03 131-11-309/20/17 18:120.38 1
Di-n-butylphthalate ND mg/kg 09/21/17 21:03 84-74-209/20/17 18:120.38 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/21/17 21:03 534-52-109/20/17 18:120.76 1
2,4-Dinitrophenol ND mg/kg 09/21/17 21:03 51-28-509/20/17 18:121.9 1
2,4-Dinitrotoluene ND mg/kg 09/21/17 21:03 121-14-209/20/17 18:120.38 1
2,6-Dinitrotoluene ND mg/kg 09/21/17 21:03 606-20-209/20/17 18:120.38 1
Di-n-octylphthalate ND mg/kg 09/21/17 21:03 117-84-009/20/17 18:120.38 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/21/17 21:03 117-81-709/20/17 18:120.38 1
Fluoranthene ND mg/kg 09/21/17 21:03 206-44-009/20/17 18:120.38 1
Fluorene ND mg/kg 09/21/17 21:03 86-73-709/20/17 18:120.38 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 21:03 87-68-309/20/17 18:120.38 1
Hexachlorobenzene ND mg/kg 09/21/17 21:03 118-74-109/20/17 18:120.38 1
Hexachlorocyclopentadiene ND mg/kg 09/21/17 21:03 77-47-409/20/17 18:120.38 1
Hexachloroethane ND mg/kg 09/21/17 21:03 67-72-109/20/17 18:120.38 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/21/17 21:03 193-39-509/20/17 18:120.38 1
Isophorone ND mg/kg 09/21/17 21:03 78-59-109/20/17 18:120.38 1
1-Methylnaphthalene ND mg/kg 09/21/17 21:03 90-12-009/20/17 18:120.38 1
2-Methylnaphthalene ND mg/kg 09/21/17 21:03 91-57-609/20/17 18:120.38 1
2-Methylphenol(o-Cresol)ND mg/kg 09/21/17 21:03 95-48-709/20/17 18:120.38 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/21/17 21:03 15831-10-409/20/17 18:120.38 1
Naphthalene ND mg/kg 09/21/17 21:03 91-20-309/20/17 18:120.38 1
2-Nitroaniline ND mg/kg 09/21/17 21:03 88-74-409/20/17 18:121.9 1
3-Nitroaniline ND mg/kg 09/21/17 21:03 99-09-209/20/17 18:121.9 1
4-Nitroaniline ND mg/kg 09/21/17 21:03 100-01-609/20/17 18:120.76 1
Nitrobenzene ND mg/kg 09/21/17 21:03 98-95-309/20/17 18:120.38 1
2-Nitrophenol ND mg/kg 09/21/17 21:03 88-75-509/20/17 18:120.38 1
4-Nitrophenol ND mg/kg 09/21/17 21:03 100-02-709/20/17 18:121.9 1
N-Nitrosodimethylamine ND mg/kg 09/21/17 21:03 62-75-909/20/17 18:120.38 1
N-Nitroso-di-n-propylamine ND mg/kg 09/21/17 21:03 621-64-709/20/17 18:120.38 1
N-Nitrosodiphenylamine ND mg/kg 09/21/17 21:03 86-30-609/20/17 18:120.38 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/21/17 21:03 108-60-109/20/17 18:120.38 1
Pentachlorophenol ND mg/kg 09/21/17 21:03 87-86-509/20/17 18:121.9 1
Phenanthrene ND mg/kg 09/21/17 21:03 85-01-809/20/17 18:120.38 1
Phenol ND mg/kg 09/21/17 21:03 108-95-209/20/17 18:120.38 1
Pyrene ND mg/kg 09/21/17 21:03 129-00-009/20/17 18:120.38 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 21:03 120-82-109/20/17 18:120.38 1
2,4,5-Trichlorophenol ND mg/kg 09/21/17 21:03 95-95-409/20/17 18:120.38 1
2,4,6-Trichlorophenol ND mg/kg 09/21/17 21:03 88-06-209/20/17 18:120.38 1
Surrogates
Nitrobenzene-d5 (S)59 %09/21/17 21:03 4165-60-009/20/17 18:1223-110 1
2-Fluorobiphenyl (S)56 %09/21/17 21:03 321-60-809/20/17 18:1230-110 1
Terphenyl-d14 (S)85 %09/21/17 21:03 1718-51-009/20/17 18:1228-110 1
Phenol-d6 (S)57 %09/21/17 21:03 13127-88-309/20/17 18:1222-110 1
2-Fluorophenol (S)56 %09/21/17 21:03 367-12-409/20/17 18:1213-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 68 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-5C Lab ID:92355949015 Collected:09/18/17 15:45 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)79 %09/21/17 21:03 118-79-609/20/17 18:1227-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 0.13 mg/kg 09/25/17 20:26 67-64-10.089 1
Benzene ND mg/kg 09/25/17 20:26 71-43-20.0044 1
Bromobenzene ND mg/kg 09/25/17 20:26 108-86-10.0044 1
Bromochloromethane ND mg/kg 09/25/17 20:26 74-97-50.0044 1
Bromodichloromethane ND mg/kg 09/25/17 20:26 75-27-40.0044 1
Bromoform ND mg/kg 09/25/17 20:26 75-25-20.0044 1
Bromomethane ND mg/kg 09/25/17 20:26 74-83-90.0089 1
2-Butanone (MEK)ND mg/kg 09/25/17 20:26 78-93-30.089 1
n-Butylbenzene 0.029 mg/kg 09/25/17 20:26 104-51-80.0044 1
sec-Butylbenzene 0.0068 mg/kg 09/25/17 20:26 135-98-80.0044 1
tert-Butylbenzene ND mg/kg 09/25/17 20:26 98-06-60.0044 1
Carbon tetrachloride ND mg/kg 09/25/17 20:26 56-23-50.0044 1
Chlorobenzene ND mg/kg 09/25/17 20:26 108-90-70.0044 1
Chloroethane ND mg/kg 09/25/17 20:26 75-00-30.0089 1
Chloroform ND mg/kg 09/25/17 20:26 67-66-30.0044 1
Chloromethane ND mg/kg 09/25/17 20:26 74-87-30.0089 1
2-Chlorotoluene ND mg/kg 09/25/17 20:26 95-49-80.0044 1
4-Chlorotoluene ND mg/kg 09/25/17 20:26 106-43-40.0044 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/25/17 20:26 96-12-80.0044 1
Dibromochloromethane ND mg/kg 09/25/17 20:26 124-48-10.0044 1
1,2-Dibromoethane (EDB)ND mg/kg 09/25/17 20:26 106-93-40.0044 1
Dibromomethane ND mg/kg 09/25/17 20:26 74-95-30.0044 1
1,2-Dichlorobenzene ND mg/kg 09/25/17 20:26 95-50-10.0044 1
1,3-Dichlorobenzene ND mg/kg 09/25/17 20:26 541-73-10.0044 1
1,4-Dichlorobenzene ND mg/kg 09/25/17 20:26 106-46-70.0044 1
Dichlorodifluoromethane ND mg/kg 09/25/17 20:26 75-71-80.0089 1
1,1-Dichloroethane ND mg/kg 09/25/17 20:26 75-34-30.0044 1
1,2-Dichloroethane ND mg/kg 09/25/17 20:26 107-06-20.0044 1
1,1-Dichloroethene ND mg/kg 09/25/17 20:26 75-35-40.0044 1
cis-1,2-Dichloroethene ND mg/kg 09/25/17 20:26 156-59-20.0044 1
trans-1,2-Dichloroethene ND mg/kg 09/25/17 20:26 156-60-50.0044 1
1,2-Dichloropropane ND mg/kg 09/25/17 20:26 78-87-50.0044 1
1,3-Dichloropropane ND mg/kg 09/25/17 20:26 142-28-90.0044 1
2,2-Dichloropropane ND mg/kg 09/25/17 20:26 594-20-70.0044 1
1,1-Dichloropropene ND mg/kg 09/25/17 20:26 563-58-60.0044 1
cis-1,3-Dichloropropene ND mg/kg 09/25/17 20:26 10061-01-50.0044 1
trans-1,3-Dichloropropene ND mg/kg 09/25/17 20:26 10061-02-60.0044 1
Diisopropyl ether ND mg/kg 09/25/17 20:26 108-20-30.0044 1
Ethylbenzene 0.020 mg/kg 09/25/17 20:26 100-41-40.0044 1
Hexachloro-1,3-butadiene ND mg/kg 09/25/17 20:26 87-68-30.0044 1
2-Hexanone ND mg/kg 09/25/17 20:26 591-78-60.044 1
Isopropylbenzene (Cumene)0.0073 mg/kg 09/25/17 20:26 98-82-80.0044 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 69 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-5C Lab ID:92355949015 Collected:09/18/17 15:45 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene 0.017 mg/kg 09/25/17 20:26 99-87-60.0044 1
Methylene Chloride ND mg/kg 09/25/17 20:26 75-09-20.018 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/25/17 20:26 108-10-10.044 1
Methyl-tert-butyl ether ND mg/kg 09/25/17 20:26 1634-04-40.0044 1
Naphthalene 0.080 mg/kg 09/25/17 20:26 91-20-30.0044 1
n-Propylbenzene 0.038 mg/kg 09/25/17 20:26 103-65-10.0044 1
Styrene ND mg/kg 09/25/17 20:26 100-42-50.0044 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/25/17 20:26 630-20-60.0044 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/25/17 20:26 79-34-50.0044 1
Tetrachloroethene ND mg/kg 09/25/17 20:26 127-18-4 L20.0044 1
Toluene ND mg/kg 09/25/17 20:26 108-88-30.0044 1
1,2,3-Trichlorobenzene ND mg/kg 09/25/17 20:26 87-61-60.0044 1
1,2,4-Trichlorobenzene ND mg/kg 09/25/17 20:26 120-82-10.0044 1
1,1,1-Trichloroethane ND mg/kg 09/25/17 20:26 71-55-60.0044 1
1,1,2-Trichloroethane ND mg/kg 09/25/17 20:26 79-00-50.0044 1
Trichloroethene ND mg/kg 09/25/17 20:26 79-01-60.0044 1
Trichlorofluoromethane ND mg/kg 09/25/17 20:26 75-69-40.0044 1
1,2,3-Trichloropropane ND mg/kg 09/25/17 20:26 96-18-40.0044 1
1,2,4-Trimethylbenzene 0.28 mg/kg 09/25/17 20:26 95-63-6 E0.0044 1
1,3,5-Trimethylbenzene 0.086 mg/kg 09/25/17 20:26 108-67-80.0044 1
Vinyl acetate ND mg/kg 09/25/17 20:26 108-05-40.044 1
Vinyl chloride ND mg/kg 09/25/17 20:26 75-01-40.0089 1
Xylene (Total)0.12 mg/kg 09/25/17 20:26 1330-20-70.0089 1
m&p-Xylene 0.085 mg/kg 09/25/17 20:26 179601-23-10.0089 1
o-Xylene 0.032 mg/kg 09/25/17 20:26 95-47-60.0044 1
Surrogates
Toluene-d8 (S)94 %09/25/17 20:26 2037-26-570-130 1
4-Bromofluorobenzene (S)101 %09/25/17 20:26 460-00-470-130 1
1,2-Dichloroethane-d4 (S)91 %09/25/17 20:26 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.2 %09/21/17 11:120.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 70 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-6A Lab ID:92355949016 Collected:09/18/17 16:15 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/21/17 20:43 N209/21/17 08:0512.2 1
Aliphatic (C19-C36)ND mg/kg 09/21/17 20:43 N209/21/17 08:0512.2 1
Aromatic (C11-C22)ND mg/kg 09/21/17 20:43 N209/21/17 08:0512.2 1
Surrogates
Nonatriacontane (S)61 %09/21/17 20:43 7194-86-709/21/17 08:0540-140 1
o-Terphenyl (S)66 %09/21/17 20:43 84-15-109/21/17 08:0540-140 1
2-Fluorobiphenyl (S)84 %09/21/17 20:43 321-60-809/21/17 08:0540-140 1
2-Bromonaphthalene (S)78 %09/21/17 20:43 580-13-209/21/17 08:0540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/21/17 22:37 N209/21/17 10:452.8 1
Aliphatic (C09-C12)ND mg/kg 09/21/17 22:37 N209/21/17 10:452.8 1
Aromatic (C09-C10)ND mg/kg 09/21/17 22:37 N209/21/17 10:452.8 1
Surrogates
4-Bromofluorobenzene (FID) (S)100 %09/21/17 22:37 460-00-409/21/17 10:4570-130 1
4-Bromofluorobenzene (PID) (S)96 %09/21/17 22:37 460-00-409/21/17 10:4570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/21/17 17:42 83-32-909/20/17 18:120.40 1
Acenaphthylene ND mg/kg 09/21/17 17:42 208-96-809/20/17 18:120.40 1
Aniline ND mg/kg 09/21/17 17:42 62-53-309/20/17 18:120.40 1
Anthracene ND mg/kg 09/21/17 17:42 120-12-709/20/17 18:120.40 1
Benzo(a)anthracene ND mg/kg 09/21/17 17:42 56-55-309/20/17 18:120.40 1
Benzo(a)pyrene ND mg/kg 09/21/17 17:42 50-32-809/20/17 18:120.40 1
Benzo(b)fluoranthene ND mg/kg 09/21/17 17:42 205-99-209/20/17 18:120.40 1
Benzo(g,h,i)perylene ND mg/kg 09/21/17 17:42 191-24-209/20/17 18:120.40 1
Benzo(k)fluoranthene ND mg/kg 09/21/17 17:42 207-08-909/20/17 18:120.40 1
Benzoic Acid ND mg/kg 09/21/17 17:42 65-85-009/20/17 18:122.0 1
Benzyl alcohol ND mg/kg 09/21/17 17:42 100-51-609/20/17 18:120.81 1
4-Bromophenylphenyl ether ND mg/kg 09/21/17 17:42 101-55-309/20/17 18:120.40 1
Butylbenzylphthalate ND mg/kg 09/21/17 17:42 85-68-709/20/17 18:120.40 1
4-Chloro-3-methylphenol ND mg/kg 09/21/17 17:42 59-50-709/20/17 18:120.81 1
4-Chloroaniline ND mg/kg 09/21/17 17:42 106-47-809/20/17 18:122.0 1
bis(2-Chloroethoxy)methane ND mg/kg 09/21/17 17:42 111-91-109/20/17 18:120.40 1
bis(2-Chloroethyl) ether ND mg/kg 09/21/17 17:42 111-44-409/20/17 18:120.40 1
2-Chloronaphthalene ND mg/kg 09/21/17 17:42 91-58-709/20/17 18:120.40 1
2-Chlorophenol ND mg/kg 09/21/17 17:42 95-57-809/20/17 18:120.40 1
4-Chlorophenylphenyl ether ND mg/kg 09/21/17 17:42 7005-72-309/20/17 18:120.40 1
Chrysene ND mg/kg 09/21/17 17:42 218-01-909/20/17 18:120.40 1
Dibenz(a,h)anthracene ND mg/kg 09/21/17 17:42 53-70-309/20/17 18:120.40 1
Dibenzofuran ND mg/kg 09/21/17 17:42 132-64-909/20/17 18:120.40 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 17:42 95-50-109/20/17 18:120.40 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 17:42 541-73-109/20/17 18:120.40 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 17:42 106-46-709/20/17 18:120.40 1
3,3'-Dichlorobenzidine ND mg/kg 09/21/17 17:42 91-94-109/20/17 18:122.0 1
2,4-Dichlorophenol ND mg/kg 09/21/17 17:42 120-83-209/20/17 18:120.40 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 71 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-6A Lab ID:92355949016 Collected:09/18/17 16:15 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/21/17 17:42 84-66-209/20/17 18:120.40 1
2,4-Dimethylphenol ND mg/kg 09/21/17 17:42 105-67-909/20/17 18:120.40 1
Dimethylphthalate ND mg/kg 09/21/17 17:42 131-11-309/20/17 18:120.40 1
Di-n-butylphthalate ND mg/kg 09/21/17 17:42 84-74-209/20/17 18:120.40 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/21/17 17:42 534-52-109/20/17 18:120.81 1
2,4-Dinitrophenol ND mg/kg 09/21/17 17:42 51-28-509/20/17 18:122.0 1
2,4-Dinitrotoluene ND mg/kg 09/21/17 17:42 121-14-209/20/17 18:120.40 1
2,6-Dinitrotoluene ND mg/kg 09/21/17 17:42 606-20-209/20/17 18:120.40 1
Di-n-octylphthalate ND mg/kg 09/21/17 17:42 117-84-009/20/17 18:120.40 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/21/17 17:42 117-81-709/20/17 18:120.40 1
Fluoranthene ND mg/kg 09/21/17 17:42 206-44-009/20/17 18:120.40 1
Fluorene ND mg/kg 09/21/17 17:42 86-73-709/20/17 18:120.40 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 17:42 87-68-309/20/17 18:120.40 1
Hexachlorobenzene ND mg/kg 09/21/17 17:42 118-74-109/20/17 18:120.40 1
Hexachlorocyclopentadiene ND mg/kg 09/21/17 17:42 77-47-409/20/17 18:120.40 1
Hexachloroethane ND mg/kg 09/21/17 17:42 67-72-109/20/17 18:120.40 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/21/17 17:42 193-39-509/20/17 18:120.40 1
Isophorone ND mg/kg 09/21/17 17:42 78-59-109/20/17 18:120.40 1
1-Methylnaphthalene ND mg/kg 09/21/17 17:42 90-12-009/20/17 18:120.40 1
2-Methylnaphthalene ND mg/kg 09/21/17 17:42 91-57-609/20/17 18:120.40 1
2-Methylphenol(o-Cresol)ND mg/kg 09/21/17 17:42 95-48-709/20/17 18:120.40 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/21/17 17:42 15831-10-409/20/17 18:120.40 1
Naphthalene ND mg/kg 09/21/17 17:42 91-20-309/20/17 18:120.40 1
2-Nitroaniline ND mg/kg 09/21/17 17:42 88-74-409/20/17 18:122.0 1
3-Nitroaniline ND mg/kg 09/21/17 17:42 99-09-209/20/17 18:122.0 1
4-Nitroaniline ND mg/kg 09/21/17 17:42 100-01-609/20/17 18:120.81 1
Nitrobenzene ND mg/kg 09/21/17 17:42 98-95-309/20/17 18:120.40 1
2-Nitrophenol ND mg/kg 09/21/17 17:42 88-75-509/20/17 18:120.40 1
4-Nitrophenol ND mg/kg 09/21/17 17:42 100-02-709/20/17 18:122.0 1
N-Nitrosodimethylamine ND mg/kg 09/21/17 17:42 62-75-909/20/17 18:120.40 1
N-Nitroso-di-n-propylamine ND mg/kg 09/21/17 17:42 621-64-709/20/17 18:120.40 1
N-Nitrosodiphenylamine ND mg/kg 09/21/17 17:42 86-30-609/20/17 18:120.40 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/21/17 17:42 108-60-109/20/17 18:120.40 1
Pentachlorophenol ND mg/kg 09/21/17 17:42 87-86-509/20/17 18:122.0 1
Phenanthrene ND mg/kg 09/21/17 17:42 85-01-809/20/17 18:120.40 1
Phenol ND mg/kg 09/21/17 17:42 108-95-209/20/17 18:120.40 1
Pyrene ND mg/kg 09/21/17 17:42 129-00-009/20/17 18:120.40 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 17:42 120-82-109/20/17 18:120.40 1
2,4,5-Trichlorophenol ND mg/kg 09/21/17 17:42 95-95-409/20/17 18:120.40 1
2,4,6-Trichlorophenol ND mg/kg 09/21/17 17:42 88-06-209/20/17 18:120.40 1
Surrogates
Nitrobenzene-d5 (S)59 %09/21/17 17:42 4165-60-009/20/17 18:1223-110 1
2-Fluorobiphenyl (S)55 %09/21/17 17:42 321-60-809/20/17 18:1230-110 1
Terphenyl-d14 (S)81 %09/21/17 17:42 1718-51-009/20/17 18:1228-110 1
Phenol-d6 (S)47 %09/21/17 17:42 13127-88-309/20/17 18:1222-110 1
2-Fluorophenol (S)46 %09/21/17 17:42 367-12-409/20/17 18:1213-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 72 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-6A Lab ID:92355949016 Collected:09/18/17 16:15 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)83 %09/21/17 17:42 118-79-609/20/17 18:1227-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/22/17 15:04 67-64-1 L10.12 1
Benzene ND mg/kg 09/22/17 15:04 71-43-20.0058 1
Bromobenzene ND mg/kg 09/22/17 15:04 108-86-10.0058 1
Bromochloromethane ND mg/kg 09/22/17 15:04 74-97-50.0058 1
Bromodichloromethane ND mg/kg 09/22/17 15:04 75-27-40.0058 1
Bromoform ND mg/kg 09/22/17 15:04 75-25-20.0058 1
Bromomethane ND mg/kg 09/22/17 15:04 74-83-90.012 1
2-Butanone (MEK)ND mg/kg 09/22/17 15:04 78-93-30.12 1
n-Butylbenzene ND mg/kg 09/22/17 15:04 104-51-80.0058 1
sec-Butylbenzene ND mg/kg 09/22/17 15:04 135-98-80.0058 1
tert-Butylbenzene ND mg/kg 09/22/17 15:04 98-06-60.0058 1
Carbon tetrachloride ND mg/kg 09/22/17 15:04 56-23-50.0058 1
Chlorobenzene ND mg/kg 09/22/17 15:04 108-90-70.0058 1
Chloroethane ND mg/kg 09/22/17 15:04 75-00-30.012 1
Chloroform ND mg/kg 09/22/17 15:04 67-66-30.0058 1
Chloromethane ND mg/kg 09/22/17 15:04 74-87-30.012 1
2-Chlorotoluene ND mg/kg 09/22/17 15:04 95-49-80.0058 1
4-Chlorotoluene ND mg/kg 09/22/17 15:04 106-43-40.0058 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/22/17 15:04 96-12-80.0058 1
Dibromochloromethane ND mg/kg 09/22/17 15:04 124-48-10.0058 1
1,2-Dibromoethane (EDB)ND mg/kg 09/22/17 15:04 106-93-40.0058 1
Dibromomethane ND mg/kg 09/22/17 15:04 74-95-30.0058 1
1,2-Dichlorobenzene ND mg/kg 09/22/17 15:04 95-50-10.0058 1
1,3-Dichlorobenzene ND mg/kg 09/22/17 15:04 541-73-10.0058 1
1,4-Dichlorobenzene ND mg/kg 09/22/17 15:04 106-46-70.0058 1
Dichlorodifluoromethane ND mg/kg 09/22/17 15:04 75-71-80.012 1
1,1-Dichloroethane ND mg/kg 09/22/17 15:04 75-34-30.0058 1
1,2-Dichloroethane ND mg/kg 09/22/17 15:04 107-06-20.0058 1
1,1-Dichloroethene ND mg/kg 09/22/17 15:04 75-35-40.0058 1
cis-1,2-Dichloroethene ND mg/kg 09/22/17 15:04 156-59-20.0058 1
trans-1,2-Dichloroethene ND mg/kg 09/22/17 15:04 156-60-50.0058 1
1,2-Dichloropropane ND mg/kg 09/22/17 15:04 78-87-50.0058 1
1,3-Dichloropropane ND mg/kg 09/22/17 15:04 142-28-90.0058 1
2,2-Dichloropropane ND mg/kg 09/22/17 15:04 594-20-70.0058 1
1,1-Dichloropropene ND mg/kg 09/22/17 15:04 563-58-60.0058 1
cis-1,3-Dichloropropene ND mg/kg 09/22/17 15:04 10061-01-50.0058 1
trans-1,3-Dichloropropene ND mg/kg 09/22/17 15:04 10061-02-60.0058 1
Diisopropyl ether ND mg/kg 09/22/17 15:04 108-20-30.0058 1
Ethylbenzene ND mg/kg 09/22/17 15:04 100-41-40.0058 1
Hexachloro-1,3-butadiene ND mg/kg 09/22/17 15:04 87-68-30.0058 1
2-Hexanone ND mg/kg 09/22/17 15:04 591-78-60.058 1
Isopropylbenzene (Cumene)ND mg/kg 09/22/17 15:04 98-82-80.0058 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 73 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-6A Lab ID:92355949016 Collected:09/18/17 16:15 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND mg/kg 09/22/17 15:04 99-87-60.0058 1
Methylene Chloride ND mg/kg 09/22/17 15:04 75-09-20.023 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/22/17 15:04 108-10-10.058 1
Methyl-tert-butyl ether ND mg/kg 09/22/17 15:04 1634-04-40.0058 1
Naphthalene ND mg/kg 09/22/17 15:04 91-20-30.0058 1
n-Propylbenzene ND mg/kg 09/22/17 15:04 103-65-10.0058 1
Styrene ND mg/kg 09/22/17 15:04 100-42-50.0058 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/22/17 15:04 630-20-60.0058 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/22/17 15:04 79-34-50.0058 1
Tetrachloroethene ND mg/kg 09/22/17 15:04 127-18-40.0058 1
Toluene ND mg/kg 09/22/17 15:04 108-88-30.0058 1
1,2,3-Trichlorobenzene ND mg/kg 09/22/17 15:04 87-61-60.0058 1
1,2,4-Trichlorobenzene ND mg/kg 09/22/17 15:04 120-82-10.0058 1
1,1,1-Trichloroethane ND mg/kg 09/22/17 15:04 71-55-60.0058 1
1,1,2-Trichloroethane ND mg/kg 09/22/17 15:04 79-00-50.0058 1
Trichloroethene ND mg/kg 09/22/17 15:04 79-01-60.0058 1
Trichlorofluoromethane ND mg/kg 09/22/17 15:04 75-69-40.0058 1
1,2,3-Trichloropropane ND mg/kg 09/22/17 15:04 96-18-40.0058 1
1,2,4-Trimethylbenzene ND mg/kg 09/22/17 15:04 95-63-60.0058 1
1,3,5-Trimethylbenzene ND mg/kg 09/22/17 15:04 108-67-80.0058 1
Vinyl acetate ND mg/kg 09/22/17 15:04 108-05-40.058 1
Vinyl chloride ND mg/kg 09/22/17 15:04 75-01-40.012 1
Xylene (Total)ND mg/kg 09/22/17 15:04 1330-20-70.012 1
m&p-Xylene ND mg/kg 09/22/17 15:04 179601-23-10.012 1
o-Xylene ND mg/kg 09/22/17 15:04 95-47-60.0058 1
Surrogates
Toluene-d8 (S)99 %09/22/17 15:04 2037-26-570-130 1
4-Bromofluorobenzene (S)101 %09/22/17 15:04 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %09/22/17 15:04 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 18.3 %09/21/17 11:120.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 74 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-6B Lab ID:92355949017 Collected:09/18/17 16:25 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/21/17 21:10 N209/21/17 08:0513.2 1
Aliphatic (C19-C36)ND mg/kg 09/21/17 21:10 N209/21/17 08:0513.2 1
Aromatic (C11-C22)ND mg/kg 09/21/17 21:10 N209/21/17 08:0513.2 1
Surrogates
Nonatriacontane (S)75 %09/21/17 21:10 7194-86-709/21/17 08:0540-140 1
o-Terphenyl (S)82 %09/21/17 21:10 84-15-109/21/17 08:0540-140 1
2-Fluorobiphenyl (S)104 %09/21/17 21:10 321-60-809/21/17 08:0540-140 1
2-Bromonaphthalene (S)91 %09/21/17 21:10 580-13-209/21/17 08:0540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/21/17 23:05 N209/21/17 10:453.5 1
Aliphatic (C09-C12)ND mg/kg 09/21/17 23:05 N209/21/17 10:453.5 1
Aromatic (C09-C10)ND mg/kg 09/21/17 23:05 N209/21/17 10:453.5 1
Surrogates
4-Bromofluorobenzene (FID) (S)121 %09/21/17 23:05 460-00-409/21/17 10:4570-130 1
4-Bromofluorobenzene (PID) (S)100 %09/21/17 23:05 460-00-409/21/17 10:4570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/21/17 18:12 83-32-909/20/17 18:120.43 1
Acenaphthylene ND mg/kg 09/21/17 18:12 208-96-809/20/17 18:120.43 1
Aniline ND mg/kg 09/21/17 18:12 62-53-309/20/17 18:120.43 1
Anthracene ND mg/kg 09/21/17 18:12 120-12-709/20/17 18:120.43 1
Benzo(a)anthracene ND mg/kg 09/21/17 18:12 56-55-309/20/17 18:120.43 1
Benzo(a)pyrene ND mg/kg 09/21/17 18:12 50-32-809/20/17 18:120.43 1
Benzo(b)fluoranthene ND mg/kg 09/21/17 18:12 205-99-209/20/17 18:120.43 1
Benzo(g,h,i)perylene ND mg/kg 09/21/17 18:12 191-24-209/20/17 18:120.43 1
Benzo(k)fluoranthene ND mg/kg 09/21/17 18:12 207-08-909/20/17 18:120.43 1
Benzoic Acid ND mg/kg 09/21/17 18:12 65-85-009/20/17 18:122.2 1
Benzyl alcohol ND mg/kg 09/21/17 18:12 100-51-609/20/17 18:120.87 1
4-Bromophenylphenyl ether ND mg/kg 09/21/17 18:12 101-55-309/20/17 18:120.43 1
Butylbenzylphthalate ND mg/kg 09/21/17 18:12 85-68-709/20/17 18:120.43 1
4-Chloro-3-methylphenol ND mg/kg 09/21/17 18:12 59-50-709/20/17 18:120.87 1
4-Chloroaniline ND mg/kg 09/21/17 18:12 106-47-809/20/17 18:122.2 1
bis(2-Chloroethoxy)methane ND mg/kg 09/21/17 18:12 111-91-109/20/17 18:120.43 1
bis(2-Chloroethyl) ether ND mg/kg 09/21/17 18:12 111-44-409/20/17 18:120.43 1
2-Chloronaphthalene ND mg/kg 09/21/17 18:12 91-58-709/20/17 18:120.43 1
2-Chlorophenol ND mg/kg 09/21/17 18:12 95-57-809/20/17 18:120.43 1
4-Chlorophenylphenyl ether ND mg/kg 09/21/17 18:12 7005-72-309/20/17 18:120.43 1
Chrysene ND mg/kg 09/21/17 18:12 218-01-909/20/17 18:120.43 1
Dibenz(a,h)anthracene ND mg/kg 09/21/17 18:12 53-70-309/20/17 18:120.43 1
Dibenzofuran ND mg/kg 09/21/17 18:12 132-64-909/20/17 18:120.43 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 18:12 95-50-109/20/17 18:120.43 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 18:12 541-73-109/20/17 18:120.43 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 18:12 106-46-709/20/17 18:120.43 1
3,3'-Dichlorobenzidine ND mg/kg 09/21/17 18:12 91-94-109/20/17 18:122.2 1
2,4-Dichlorophenol ND mg/kg 09/21/17 18:12 120-83-209/20/17 18:120.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 75 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-6B Lab ID:92355949017 Collected:09/18/17 16:25 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/21/17 18:12 84-66-209/20/17 18:120.43 1
2,4-Dimethylphenol ND mg/kg 09/21/17 18:12 105-67-909/20/17 18:120.43 1
Dimethylphthalate ND mg/kg 09/21/17 18:12 131-11-309/20/17 18:120.43 1
Di-n-butylphthalate ND mg/kg 09/21/17 18:12 84-74-209/20/17 18:120.43 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/21/17 18:12 534-52-109/20/17 18:120.87 1
2,4-Dinitrophenol ND mg/kg 09/21/17 18:12 51-28-509/20/17 18:122.2 1
2,4-Dinitrotoluene ND mg/kg 09/21/17 18:12 121-14-209/20/17 18:120.43 1
2,6-Dinitrotoluene ND mg/kg 09/21/17 18:12 606-20-209/20/17 18:120.43 1
Di-n-octylphthalate ND mg/kg 09/21/17 18:12 117-84-009/20/17 18:120.43 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/21/17 18:12 117-81-709/20/17 18:120.43 1
Fluoranthene ND mg/kg 09/21/17 18:12 206-44-009/20/17 18:120.43 1
Fluorene ND mg/kg 09/21/17 18:12 86-73-709/20/17 18:120.43 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 18:12 87-68-309/20/17 18:120.43 1
Hexachlorobenzene ND mg/kg 09/21/17 18:12 118-74-109/20/17 18:120.43 1
Hexachlorocyclopentadiene ND mg/kg 09/21/17 18:12 77-47-409/20/17 18:120.43 1
Hexachloroethane ND mg/kg 09/21/17 18:12 67-72-109/20/17 18:120.43 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/21/17 18:12 193-39-509/20/17 18:120.43 1
Isophorone ND mg/kg 09/21/17 18:12 78-59-109/20/17 18:120.43 1
1-Methylnaphthalene ND mg/kg 09/21/17 18:12 90-12-009/20/17 18:120.43 1
2-Methylnaphthalene ND mg/kg 09/21/17 18:12 91-57-609/20/17 18:120.43 1
2-Methylphenol(o-Cresol)ND mg/kg 09/21/17 18:12 95-48-709/20/17 18:120.43 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/21/17 18:12 15831-10-409/20/17 18:120.43 1
Naphthalene ND mg/kg 09/21/17 18:12 91-20-309/20/17 18:120.43 1
2-Nitroaniline ND mg/kg 09/21/17 18:12 88-74-409/20/17 18:122.2 1
3-Nitroaniline ND mg/kg 09/21/17 18:12 99-09-209/20/17 18:122.2 1
4-Nitroaniline ND mg/kg 09/21/17 18:12 100-01-609/20/17 18:120.87 1
Nitrobenzene ND mg/kg 09/21/17 18:12 98-95-309/20/17 18:120.43 1
2-Nitrophenol ND mg/kg 09/21/17 18:12 88-75-509/20/17 18:120.43 1
4-Nitrophenol ND mg/kg 09/21/17 18:12 100-02-709/20/17 18:122.2 1
N-Nitrosodimethylamine ND mg/kg 09/21/17 18:12 62-75-909/20/17 18:120.43 1
N-Nitroso-di-n-propylamine ND mg/kg 09/21/17 18:12 621-64-709/20/17 18:120.43 1
N-Nitrosodiphenylamine ND mg/kg 09/21/17 18:12 86-30-609/20/17 18:120.43 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/21/17 18:12 108-60-109/20/17 18:120.43 1
Pentachlorophenol ND mg/kg 09/21/17 18:12 87-86-509/20/17 18:122.2 1
Phenanthrene ND mg/kg 09/21/17 18:12 85-01-809/20/17 18:120.43 1
Phenol ND mg/kg 09/21/17 18:12 108-95-209/20/17 18:120.43 1
Pyrene ND mg/kg 09/21/17 18:12 129-00-009/20/17 18:120.43 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 18:12 120-82-109/20/17 18:120.43 1
2,4,5-Trichlorophenol ND mg/kg 09/21/17 18:12 95-95-409/20/17 18:120.43 1
2,4,6-Trichlorophenol ND mg/kg 09/21/17 18:12 88-06-209/20/17 18:120.43 1
Surrogates
Nitrobenzene-d5 (S)43 %09/21/17 18:12 4165-60-009/20/17 18:1223-110 1
2-Fluorobiphenyl (S)43 %09/21/17 18:12 321-60-809/20/17 18:1230-110 1
Terphenyl-d14 (S)73 %09/21/17 18:12 1718-51-009/20/17 18:1228-110 1
Phenol-d6 (S)36 %09/21/17 18:12 13127-88-309/20/17 18:1222-110 1
2-Fluorophenol (S)36 %09/21/17 18:12 367-12-409/20/17 18:1213-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 76 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-6B Lab ID:92355949017 Collected:09/18/17 16:25 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)75 %09/21/17 18:12 118-79-609/20/17 18:1227-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/22/17 15:24 67-64-1 L10.12 1
Benzene ND mg/kg 09/22/17 15:24 71-43-20.0060 1
Bromobenzene ND mg/kg 09/22/17 15:24 108-86-10.0060 1
Bromochloromethane ND mg/kg 09/22/17 15:24 74-97-50.0060 1
Bromodichloromethane ND mg/kg 09/22/17 15:24 75-27-40.0060 1
Bromoform ND mg/kg 09/22/17 15:24 75-25-20.0060 1
Bromomethane ND mg/kg 09/22/17 15:24 74-83-90.012 1
2-Butanone (MEK)ND mg/kg 09/22/17 15:24 78-93-30.12 1
n-Butylbenzene ND mg/kg 09/22/17 15:24 104-51-80.0060 1
sec-Butylbenzene ND mg/kg 09/22/17 15:24 135-98-80.0060 1
tert-Butylbenzene ND mg/kg 09/22/17 15:24 98-06-60.0060 1
Carbon tetrachloride ND mg/kg 09/22/17 15:24 56-23-50.0060 1
Chlorobenzene ND mg/kg 09/22/17 15:24 108-90-70.0060 1
Chloroethane ND mg/kg 09/22/17 15:24 75-00-30.012 1
Chloroform ND mg/kg 09/22/17 15:24 67-66-30.0060 1
Chloromethane ND mg/kg 09/22/17 15:24 74-87-30.012 1
2-Chlorotoluene ND mg/kg 09/22/17 15:24 95-49-80.0060 1
4-Chlorotoluene ND mg/kg 09/22/17 15:24 106-43-40.0060 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/22/17 15:24 96-12-80.0060 1
Dibromochloromethane ND mg/kg 09/22/17 15:24 124-48-10.0060 1
1,2-Dibromoethane (EDB)ND mg/kg 09/22/17 15:24 106-93-40.0060 1
Dibromomethane ND mg/kg 09/22/17 15:24 74-95-30.0060 1
1,2-Dichlorobenzene ND mg/kg 09/22/17 15:24 95-50-10.0060 1
1,3-Dichlorobenzene ND mg/kg 09/22/17 15:24 541-73-10.0060 1
1,4-Dichlorobenzene ND mg/kg 09/22/17 15:24 106-46-70.0060 1
Dichlorodifluoromethane ND mg/kg 09/22/17 15:24 75-71-80.012 1
1,1-Dichloroethane ND mg/kg 09/22/17 15:24 75-34-30.0060 1
1,2-Dichloroethane ND mg/kg 09/22/17 15:24 107-06-20.0060 1
1,1-Dichloroethene ND mg/kg 09/22/17 15:24 75-35-40.0060 1
cis-1,2-Dichloroethene ND mg/kg 09/22/17 15:24 156-59-20.0060 1
trans-1,2-Dichloroethene ND mg/kg 09/22/17 15:24 156-60-50.0060 1
1,2-Dichloropropane ND mg/kg 09/22/17 15:24 78-87-50.0060 1
1,3-Dichloropropane ND mg/kg 09/22/17 15:24 142-28-90.0060 1
2,2-Dichloropropane ND mg/kg 09/22/17 15:24 594-20-70.0060 1
1,1-Dichloropropene ND mg/kg 09/22/17 15:24 563-58-60.0060 1
cis-1,3-Dichloropropene ND mg/kg 09/22/17 15:24 10061-01-50.0060 1
trans-1,3-Dichloropropene ND mg/kg 09/22/17 15:24 10061-02-60.0060 1
Diisopropyl ether ND mg/kg 09/22/17 15:24 108-20-30.0060 1
Ethylbenzene ND mg/kg 09/22/17 15:24 100-41-40.0060 1
Hexachloro-1,3-butadiene ND mg/kg 09/22/17 15:24 87-68-30.0060 1
2-Hexanone ND mg/kg 09/22/17 15:24 591-78-60.060 1
Isopropylbenzene (Cumene)ND mg/kg 09/22/17 15:24 98-82-80.0060 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 77 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-6B Lab ID:92355949017 Collected:09/18/17 16:25 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND mg/kg 09/22/17 15:24 99-87-60.0060 1
Methylene Chloride ND mg/kg 09/22/17 15:24 75-09-20.024 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/22/17 15:24 108-10-10.060 1
Methyl-tert-butyl ether ND mg/kg 09/22/17 15:24 1634-04-40.0060 1
Naphthalene ND mg/kg 09/22/17 15:24 91-20-30.0060 1
n-Propylbenzene ND mg/kg 09/22/17 15:24 103-65-10.0060 1
Styrene ND mg/kg 09/22/17 15:24 100-42-50.0060 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/22/17 15:24 630-20-60.0060 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/22/17 15:24 79-34-50.0060 1
Tetrachloroethene ND mg/kg 09/22/17 15:24 127-18-40.0060 1
Toluene ND mg/kg 09/22/17 15:24 108-88-30.0060 1
1,2,3-Trichlorobenzene ND mg/kg 09/22/17 15:24 87-61-60.0060 1
1,2,4-Trichlorobenzene ND mg/kg 09/22/17 15:24 120-82-10.0060 1
1,1,1-Trichloroethane ND mg/kg 09/22/17 15:24 71-55-60.0060 1
1,1,2-Trichloroethane ND mg/kg 09/22/17 15:24 79-00-50.0060 1
Trichloroethene ND mg/kg 09/22/17 15:24 79-01-60.0060 1
Trichlorofluoromethane ND mg/kg 09/22/17 15:24 75-69-40.0060 1
1,2,3-Trichloropropane ND mg/kg 09/22/17 15:24 96-18-40.0060 1
1,2,4-Trimethylbenzene 0.029 mg/kg 09/22/17 15:24 95-63-60.0060 1
1,3,5-Trimethylbenzene 0.0090 mg/kg 09/22/17 15:24 108-67-80.0060 1
Vinyl acetate ND mg/kg 09/22/17 15:24 108-05-40.060 1
Vinyl chloride ND mg/kg 09/22/17 15:24 75-01-40.012 1
Xylene (Total)0.013 mg/kg 09/22/17 15:24 1330-20-70.012 1
m&p-Xylene 0.013 mg/kg 09/22/17 15:24 179601-23-10.012 1
o-Xylene ND mg/kg 09/22/17 15:24 95-47-60.0060 1
Surrogates
Toluene-d8 (S)101 %09/22/17 15:24 2037-26-570-130 1
4-Bromofluorobenzene (S)95 %09/22/17 15:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)118 %09/22/17 15:24 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 24.0 %09/21/17 11:120.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 78 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-6C Lab ID:92355949018 Collected:09/18/17 16:40 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/22/17 13:56 N209/21/17 08:0512.5 1
Aliphatic (C19-C36)ND mg/kg 09/22/17 13:56 N209/21/17 08:0512.5 1
Aromatic (C11-C22)17.9 mg/kg 09/22/17 13:56 N209/21/17 08:0512.5 1
Surrogates
Nonatriacontane (S)49 %09/22/17 13:56 7194-86-709/21/17 08:0540-140 1
o-Terphenyl (S)72 %09/22/17 13:56 84-15-109/21/17 08:0540-140 1
2-Fluorobiphenyl (S)115 %09/22/17 13:56 321-60-809/21/17 08:0540-140 1
2-Bromonaphthalene (S)106 %09/22/17 13:56 580-13-209/21/17 08:0540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/21/17 23:33 N209/21/17 10:453.5 1
Aliphatic (C09-C12)ND mg/kg 09/21/17 23:33 N209/21/17 10:453.5 1
Aromatic (C09-C10)ND mg/kg 09/21/17 23:33 N209/21/17 10:453.5 1
Surrogates
4-Bromofluorobenzene (FID) (S)101 %09/21/17 23:33 460-00-409/21/17 10:4570-130 1
4-Bromofluorobenzene (PID) (S)95 %09/21/17 23:33 460-00-409/21/17 10:4570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/21/17 18:42 83-32-909/20/17 18:120.41 1
Acenaphthylene ND mg/kg 09/21/17 18:42 208-96-809/20/17 18:120.41 1
Aniline ND mg/kg 09/21/17 18:42 62-53-309/20/17 18:120.41 1
Anthracene ND mg/kg 09/21/17 18:42 120-12-709/20/17 18:120.41 1
Benzo(a)anthracene ND mg/kg 09/21/17 18:42 56-55-309/20/17 18:120.41 1
Benzo(a)pyrene ND mg/kg 09/21/17 18:42 50-32-809/20/17 18:120.41 1
Benzo(b)fluoranthene ND mg/kg 09/21/17 18:42 205-99-209/20/17 18:120.41 1
Benzo(g,h,i)perylene ND mg/kg 09/21/17 18:42 191-24-209/20/17 18:120.41 1
Benzo(k)fluoranthene ND mg/kg 09/21/17 18:42 207-08-909/20/17 18:120.41 1
Benzoic Acid ND mg/kg 09/21/17 18:42 65-85-009/20/17 18:122.1 1
Benzyl alcohol ND mg/kg 09/21/17 18:42 100-51-609/20/17 18:120.83 1
4-Bromophenylphenyl ether ND mg/kg 09/21/17 18:42 101-55-309/20/17 18:120.41 1
Butylbenzylphthalate ND mg/kg 09/21/17 18:42 85-68-709/20/17 18:120.41 1
4-Chloro-3-methylphenol ND mg/kg 09/21/17 18:42 59-50-709/20/17 18:120.83 1
4-Chloroaniline ND mg/kg 09/21/17 18:42 106-47-809/20/17 18:122.1 1
bis(2-Chloroethoxy)methane ND mg/kg 09/21/17 18:42 111-91-109/20/17 18:120.41 1
bis(2-Chloroethyl) ether ND mg/kg 09/21/17 18:42 111-44-409/20/17 18:120.41 1
2-Chloronaphthalene ND mg/kg 09/21/17 18:42 91-58-709/20/17 18:120.41 1
2-Chlorophenol ND mg/kg 09/21/17 18:42 95-57-809/20/17 18:120.41 1
4-Chlorophenylphenyl ether ND mg/kg 09/21/17 18:42 7005-72-309/20/17 18:120.41 1
Chrysene ND mg/kg 09/21/17 18:42 218-01-909/20/17 18:120.41 1
Dibenz(a,h)anthracene ND mg/kg 09/21/17 18:42 53-70-309/20/17 18:120.41 1
Dibenzofuran ND mg/kg 09/21/17 18:42 132-64-909/20/17 18:120.41 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 18:42 95-50-109/20/17 18:120.41 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 18:42 541-73-109/20/17 18:120.41 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 18:42 106-46-709/20/17 18:120.41 1
3,3'-Dichlorobenzidine ND mg/kg 09/21/17 18:42 91-94-109/20/17 18:122.1 1
2,4-Dichlorophenol ND mg/kg 09/21/17 18:42 120-83-209/20/17 18:120.41 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 79 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-6C Lab ID:92355949018 Collected:09/18/17 16:40 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/21/17 18:42 84-66-209/20/17 18:120.41 1
2,4-Dimethylphenol ND mg/kg 09/21/17 18:42 105-67-909/20/17 18:120.41 1
Dimethylphthalate ND mg/kg 09/21/17 18:42 131-11-309/20/17 18:120.41 1
Di-n-butylphthalate ND mg/kg 09/21/17 18:42 84-74-209/20/17 18:120.41 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/21/17 18:42 534-52-109/20/17 18:120.83 1
2,4-Dinitrophenol ND mg/kg 09/21/17 18:42 51-28-509/20/17 18:122.1 1
2,4-Dinitrotoluene ND mg/kg 09/21/17 18:42 121-14-209/20/17 18:120.41 1
2,6-Dinitrotoluene ND mg/kg 09/21/17 18:42 606-20-209/20/17 18:120.41 1
Di-n-octylphthalate ND mg/kg 09/21/17 18:42 117-84-009/20/17 18:120.41 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/21/17 18:42 117-81-709/20/17 18:120.41 1
Fluoranthene ND mg/kg 09/21/17 18:42 206-44-009/20/17 18:120.41 1
Fluorene ND mg/kg 09/21/17 18:42 86-73-709/20/17 18:120.41 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 18:42 87-68-309/20/17 18:120.41 1
Hexachlorobenzene ND mg/kg 09/21/17 18:42 118-74-109/20/17 18:120.41 1
Hexachlorocyclopentadiene ND mg/kg 09/21/17 18:42 77-47-409/20/17 18:120.41 1
Hexachloroethane ND mg/kg 09/21/17 18:42 67-72-109/20/17 18:120.41 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/21/17 18:42 193-39-509/20/17 18:120.41 1
Isophorone ND mg/kg 09/21/17 18:42 78-59-109/20/17 18:120.41 1
1-Methylnaphthalene ND mg/kg 09/21/17 18:42 90-12-009/20/17 18:120.41 1
2-Methylnaphthalene ND mg/kg 09/21/17 18:42 91-57-609/20/17 18:120.41 1
2-Methylphenol(o-Cresol)ND mg/kg 09/21/17 18:42 95-48-709/20/17 18:120.41 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/21/17 18:42 15831-10-409/20/17 18:120.41 1
Naphthalene ND mg/kg 09/21/17 18:42 91-20-309/20/17 18:120.41 1
2-Nitroaniline ND mg/kg 09/21/17 18:42 88-74-409/20/17 18:122.1 1
3-Nitroaniline ND mg/kg 09/21/17 18:42 99-09-209/20/17 18:122.1 1
4-Nitroaniline ND mg/kg 09/21/17 18:42 100-01-609/20/17 18:120.83 1
Nitrobenzene ND mg/kg 09/21/17 18:42 98-95-309/20/17 18:120.41 1
2-Nitrophenol ND mg/kg 09/21/17 18:42 88-75-509/20/17 18:120.41 1
4-Nitrophenol ND mg/kg 09/21/17 18:42 100-02-709/20/17 18:122.1 1
N-Nitrosodimethylamine ND mg/kg 09/21/17 18:42 62-75-909/20/17 18:120.41 1
N-Nitroso-di-n-propylamine ND mg/kg 09/21/17 18:42 621-64-709/20/17 18:120.41 1
N-Nitrosodiphenylamine ND mg/kg 09/21/17 18:42 86-30-609/20/17 18:120.41 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/21/17 18:42 108-60-109/20/17 18:120.41 1
Pentachlorophenol ND mg/kg 09/21/17 18:42 87-86-509/20/17 18:122.1 1
Phenanthrene ND mg/kg 09/21/17 18:42 85-01-809/20/17 18:120.41 1
Phenol ND mg/kg 09/21/17 18:42 108-95-209/20/17 18:120.41 1
Pyrene ND mg/kg 09/21/17 18:42 129-00-009/20/17 18:120.41 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 18:42 120-82-109/20/17 18:120.41 1
2,4,5-Trichlorophenol ND mg/kg 09/21/17 18:42 95-95-409/20/17 18:120.41 1
2,4,6-Trichlorophenol ND mg/kg 09/21/17 18:42 88-06-209/20/17 18:120.41 1
Surrogates
Nitrobenzene-d5 (S)52 %09/21/17 18:42 4165-60-009/20/17 18:1223-110 1
2-Fluorobiphenyl (S)56 %09/21/17 18:42 321-60-809/20/17 18:1230-110 1
Terphenyl-d14 (S)90 %09/21/17 18:42 1718-51-009/20/17 18:1228-110 1
Phenol-d6 (S)44 %09/21/17 18:42 13127-88-309/20/17 18:1222-110 1
2-Fluorophenol (S)42 %09/21/17 18:42 367-12-409/20/17 18:1213-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 80 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-6C Lab ID:92355949018 Collected:09/18/17 16:40 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)89 %09/21/17 18:42 118-79-609/20/17 18:1227-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/22/17 15:44 67-64-1 L10.12 1
Benzene ND mg/kg 09/22/17 15:44 71-43-20.0062 1
Bromobenzene ND mg/kg 09/22/17 15:44 108-86-10.0062 1
Bromochloromethane ND mg/kg 09/22/17 15:44 74-97-50.0062 1
Bromodichloromethane ND mg/kg 09/22/17 15:44 75-27-40.0062 1
Bromoform ND mg/kg 09/22/17 15:44 75-25-20.0062 1
Bromomethane ND mg/kg 09/22/17 15:44 74-83-90.012 1
2-Butanone (MEK)ND mg/kg 09/22/17 15:44 78-93-30.12 1
n-Butylbenzene ND mg/kg 09/22/17 15:44 104-51-80.0062 1
sec-Butylbenzene ND mg/kg 09/22/17 15:44 135-98-80.0062 1
tert-Butylbenzene ND mg/kg 09/22/17 15:44 98-06-60.0062 1
Carbon tetrachloride ND mg/kg 09/22/17 15:44 56-23-50.0062 1
Chlorobenzene ND mg/kg 09/22/17 15:44 108-90-70.0062 1
Chloroethane ND mg/kg 09/22/17 15:44 75-00-30.012 1
Chloroform ND mg/kg 09/22/17 15:44 67-66-30.0062 1
Chloromethane ND mg/kg 09/22/17 15:44 74-87-30.012 1
2-Chlorotoluene ND mg/kg 09/22/17 15:44 95-49-80.0062 1
4-Chlorotoluene ND mg/kg 09/22/17 15:44 106-43-40.0062 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/22/17 15:44 96-12-80.0062 1
Dibromochloromethane ND mg/kg 09/22/17 15:44 124-48-10.0062 1
1,2-Dibromoethane (EDB)ND mg/kg 09/22/17 15:44 106-93-40.0062 1
Dibromomethane ND mg/kg 09/22/17 15:44 74-95-30.0062 1
1,2-Dichlorobenzene ND mg/kg 09/22/17 15:44 95-50-10.0062 1
1,3-Dichlorobenzene ND mg/kg 09/22/17 15:44 541-73-10.0062 1
1,4-Dichlorobenzene ND mg/kg 09/22/17 15:44 106-46-70.0062 1
Dichlorodifluoromethane ND mg/kg 09/22/17 15:44 75-71-80.012 1
1,1-Dichloroethane ND mg/kg 09/22/17 15:44 75-34-30.0062 1
1,2-Dichloroethane ND mg/kg 09/22/17 15:44 107-06-20.0062 1
1,1-Dichloroethene ND mg/kg 09/22/17 15:44 75-35-40.0062 1
cis-1,2-Dichloroethene ND mg/kg 09/22/17 15:44 156-59-20.0062 1
trans-1,2-Dichloroethene ND mg/kg 09/22/17 15:44 156-60-50.0062 1
1,2-Dichloropropane ND mg/kg 09/22/17 15:44 78-87-50.0062 1
1,3-Dichloropropane ND mg/kg 09/22/17 15:44 142-28-90.0062 1
2,2-Dichloropropane ND mg/kg 09/22/17 15:44 594-20-70.0062 1
1,1-Dichloropropene ND mg/kg 09/22/17 15:44 563-58-60.0062 1
cis-1,3-Dichloropropene ND mg/kg 09/22/17 15:44 10061-01-50.0062 1
trans-1,3-Dichloropropene ND mg/kg 09/22/17 15:44 10061-02-60.0062 1
Diisopropyl ether ND mg/kg 09/22/17 15:44 108-20-30.0062 1
Ethylbenzene ND mg/kg 09/22/17 15:44 100-41-40.0062 1
Hexachloro-1,3-butadiene ND mg/kg 09/22/17 15:44 87-68-30.0062 1
2-Hexanone ND mg/kg 09/22/17 15:44 591-78-60.062 1
Isopropylbenzene (Cumene)ND mg/kg 09/22/17 15:44 98-82-80.0062 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 81 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-6C Lab ID:92355949018 Collected:09/18/17 16:40 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND mg/kg 09/22/17 15:44 99-87-60.0062 1
Methylene Chloride ND mg/kg 09/22/17 15:44 75-09-20.025 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/22/17 15:44 108-10-10.062 1
Methyl-tert-butyl ether ND mg/kg 09/22/17 15:44 1634-04-40.0062 1
Naphthalene ND mg/kg 09/22/17 15:44 91-20-30.0062 1
n-Propylbenzene ND mg/kg 09/22/17 15:44 103-65-10.0062 1
Styrene ND mg/kg 09/22/17 15:44 100-42-50.0062 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/22/17 15:44 630-20-60.0062 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/22/17 15:44 79-34-50.0062 1
Tetrachloroethene ND mg/kg 09/22/17 15:44 127-18-40.0062 1
Toluene ND mg/kg 09/22/17 15:44 108-88-30.0062 1
1,2,3-Trichlorobenzene ND mg/kg 09/22/17 15:44 87-61-60.0062 1
1,2,4-Trichlorobenzene ND mg/kg 09/22/17 15:44 120-82-10.0062 1
1,1,1-Trichloroethane ND mg/kg 09/22/17 15:44 71-55-60.0062 1
1,1,2-Trichloroethane ND mg/kg 09/22/17 15:44 79-00-50.0062 1
Trichloroethene ND mg/kg 09/22/17 15:44 79-01-60.0062 1
Trichlorofluoromethane ND mg/kg 09/22/17 15:44 75-69-40.0062 1
1,2,3-Trichloropropane ND mg/kg 09/22/17 15:44 96-18-40.0062 1
1,2,4-Trimethylbenzene ND mg/kg 09/22/17 15:44 95-63-60.0062 1
1,3,5-Trimethylbenzene ND mg/kg 09/22/17 15:44 108-67-80.0062 1
Vinyl acetate ND mg/kg 09/22/17 15:44 108-05-40.062 1
Vinyl chloride ND mg/kg 09/22/17 15:44 75-01-40.012 1
Xylene (Total)ND mg/kg 09/22/17 15:44 1330-20-70.012 1
m&p-Xylene ND mg/kg 09/22/17 15:44 179601-23-10.012 1
o-Xylene ND mg/kg 09/22/17 15:44 95-47-60.0062 1
Surrogates
Toluene-d8 (S)101 %09/22/17 15:44 2037-26-570-130 1
4-Bromofluorobenzene (S)101 %09/22/17 15:44 460-00-470-130 1
1,2-Dichloroethane-d4 (S)109 %09/22/17 15:44 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 20.1 %09/21/17 11:120.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 82 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-7A Lab ID:92355949019 Collected:09/18/17 17:00 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/22/17 14:23 N209/21/17 08:0512.4 1
Aliphatic (C19-C36)ND mg/kg 09/22/17 14:23 N209/21/17 08:0512.4 1
Aromatic (C11-C22)ND mg/kg 09/22/17 14:23 N209/21/17 08:0512.4 1
Surrogates
Nonatriacontane (S)70 %09/22/17 14:23 7194-86-709/21/17 08:0540-140 1
o-Terphenyl (S)83 %09/22/17 14:23 84-15-109/21/17 08:0540-140 1
2-Fluorobiphenyl (S)107 %09/22/17 14:23 321-60-809/21/17 08:0540-140 1
2-Bromonaphthalene (S)109 %09/22/17 14:23 580-13-209/21/17 08:0540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/22/17 00:01 N209/21/17 10:453.0 1
Aliphatic (C09-C12)ND mg/kg 09/22/17 00:01 N209/21/17 10:453.0 1
Aromatic (C09-C10)ND mg/kg 09/22/17 00:01 N209/21/17 10:453.0 1
Surrogates
4-Bromofluorobenzene (FID) (S)100 %09/22/17 00:01 460-00-409/21/17 10:4570-130 1
4-Bromofluorobenzene (PID) (S)95 %09/22/17 00:01 460-00-409/21/17 10:4570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/21/17 21:32 83-32-909/20/17 18:120.41 1
Acenaphthylene ND mg/kg 09/21/17 21:32 208-96-809/20/17 18:120.41 1
Aniline ND mg/kg 09/21/17 21:32 62-53-309/20/17 18:120.41 1
Anthracene ND mg/kg 09/21/17 21:32 120-12-709/20/17 18:120.41 1
Benzo(a)anthracene ND mg/kg 09/21/17 21:32 56-55-309/20/17 18:120.41 1
Benzo(a)pyrene ND mg/kg 09/21/17 21:32 50-32-809/20/17 18:120.41 1
Benzo(b)fluoranthene ND mg/kg 09/21/17 21:32 205-99-209/20/17 18:120.41 1
Benzo(g,h,i)perylene ND mg/kg 09/21/17 21:32 191-24-209/20/17 18:120.41 1
Benzo(k)fluoranthene ND mg/kg 09/21/17 21:32 207-08-909/20/17 18:120.41 1
Benzoic Acid ND mg/kg 09/21/17 21:32 65-85-009/20/17 18:122.0 1
Benzyl alcohol ND mg/kg 09/21/17 21:32 100-51-609/20/17 18:120.82 1
4-Bromophenylphenyl ether ND mg/kg 09/21/17 21:32 101-55-309/20/17 18:120.41 1
Butylbenzylphthalate ND mg/kg 09/21/17 21:32 85-68-709/20/17 18:120.41 1
4-Chloro-3-methylphenol ND mg/kg 09/21/17 21:32 59-50-709/20/17 18:120.82 1
4-Chloroaniline ND mg/kg 09/21/17 21:32 106-47-809/20/17 18:122.0 1
bis(2-Chloroethoxy)methane ND mg/kg 09/21/17 21:32 111-91-109/20/17 18:120.41 1
bis(2-Chloroethyl) ether ND mg/kg 09/21/17 21:32 111-44-409/20/17 18:120.41 1
2-Chloronaphthalene ND mg/kg 09/21/17 21:32 91-58-709/20/17 18:120.41 1
2-Chlorophenol ND mg/kg 09/21/17 21:32 95-57-809/20/17 18:120.41 1
4-Chlorophenylphenyl ether ND mg/kg 09/21/17 21:32 7005-72-309/20/17 18:120.41 1
Chrysene ND mg/kg 09/21/17 21:32 218-01-909/20/17 18:120.41 1
Dibenz(a,h)anthracene ND mg/kg 09/21/17 21:32 53-70-309/20/17 18:120.41 1
Dibenzofuran ND mg/kg 09/21/17 21:32 132-64-909/20/17 18:120.41 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 21:32 95-50-109/20/17 18:120.41 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 21:32 541-73-109/20/17 18:120.41 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 21:32 106-46-709/20/17 18:120.41 1
3,3'-Dichlorobenzidine ND mg/kg 09/21/17 21:32 91-94-109/20/17 18:122.0 1
2,4-Dichlorophenol ND mg/kg 09/21/17 21:32 120-83-209/20/17 18:120.41 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 83 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-7A Lab ID:92355949019 Collected:09/18/17 17:00 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/21/17 21:32 84-66-209/20/17 18:120.41 1
2,4-Dimethylphenol ND mg/kg 09/21/17 21:32 105-67-909/20/17 18:120.41 1
Dimethylphthalate ND mg/kg 09/21/17 21:32 131-11-309/20/17 18:120.41 1
Di-n-butylphthalate ND mg/kg 09/21/17 21:32 84-74-209/20/17 18:120.41 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/21/17 21:32 534-52-109/20/17 18:120.82 1
2,4-Dinitrophenol ND mg/kg 09/21/17 21:32 51-28-509/20/17 18:122.0 1
2,4-Dinitrotoluene ND mg/kg 09/21/17 21:32 121-14-209/20/17 18:120.41 1
2,6-Dinitrotoluene ND mg/kg 09/21/17 21:32 606-20-209/20/17 18:120.41 1
Di-n-octylphthalate ND mg/kg 09/21/17 21:32 117-84-009/20/17 18:120.41 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/21/17 21:32 117-81-709/20/17 18:120.41 1
Fluoranthene ND mg/kg 09/21/17 21:32 206-44-009/20/17 18:120.41 1
Fluorene ND mg/kg 09/21/17 21:32 86-73-709/20/17 18:120.41 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 21:32 87-68-309/20/17 18:120.41 1
Hexachlorobenzene ND mg/kg 09/21/17 21:32 118-74-109/20/17 18:120.41 1
Hexachlorocyclopentadiene ND mg/kg 09/21/17 21:32 77-47-409/20/17 18:120.41 1
Hexachloroethane ND mg/kg 09/21/17 21:32 67-72-109/20/17 18:120.41 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/21/17 21:32 193-39-509/20/17 18:120.41 1
Isophorone ND mg/kg 09/21/17 21:32 78-59-109/20/17 18:120.41 1
1-Methylnaphthalene ND mg/kg 09/21/17 21:32 90-12-009/20/17 18:120.41 1
2-Methylnaphthalene ND mg/kg 09/21/17 21:32 91-57-609/20/17 18:120.41 1
2-Methylphenol(o-Cresol)ND mg/kg 09/21/17 21:32 95-48-709/20/17 18:120.41 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/21/17 21:32 15831-10-409/20/17 18:120.41 1
Naphthalene ND mg/kg 09/21/17 21:32 91-20-309/20/17 18:120.41 1
2-Nitroaniline ND mg/kg 09/21/17 21:32 88-74-409/20/17 18:122.0 1
3-Nitroaniline ND mg/kg 09/21/17 21:32 99-09-209/20/17 18:122.0 1
4-Nitroaniline ND mg/kg 09/21/17 21:32 100-01-609/20/17 18:120.82 1
Nitrobenzene ND mg/kg 09/21/17 21:32 98-95-309/20/17 18:120.41 1
2-Nitrophenol ND mg/kg 09/21/17 21:32 88-75-509/20/17 18:120.41 1
4-Nitrophenol ND mg/kg 09/21/17 21:32 100-02-709/20/17 18:122.0 1
N-Nitrosodimethylamine ND mg/kg 09/21/17 21:32 62-75-909/20/17 18:120.41 1
N-Nitroso-di-n-propylamine ND mg/kg 09/21/17 21:32 621-64-709/20/17 18:120.41 1
N-Nitrosodiphenylamine ND mg/kg 09/21/17 21:32 86-30-609/20/17 18:120.41 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/21/17 21:32 108-60-109/20/17 18:120.41 1
Pentachlorophenol ND mg/kg 09/21/17 21:32 87-86-509/20/17 18:122.0 1
Phenanthrene ND mg/kg 09/21/17 21:32 85-01-809/20/17 18:120.41 1
Phenol ND mg/kg 09/21/17 21:32 108-95-209/20/17 18:120.41 1
Pyrene ND mg/kg 09/21/17 21:32 129-00-009/20/17 18:120.41 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 21:32 120-82-109/20/17 18:120.41 1
2,4,5-Trichlorophenol ND mg/kg 09/21/17 21:32 95-95-409/20/17 18:120.41 1
2,4,6-Trichlorophenol ND mg/kg 09/21/17 21:32 88-06-209/20/17 18:120.41 1
Surrogates
Nitrobenzene-d5 (S)60 %09/21/17 21:32 4165-60-009/20/17 18:1223-110 1
2-Fluorobiphenyl (S)61 %09/21/17 21:32 321-60-809/20/17 18:1230-110 1
Terphenyl-d14 (S)78 %09/21/17 21:32 1718-51-009/20/17 18:1228-110 1
Phenol-d6 (S)59 %09/21/17 21:32 13127-88-309/20/17 18:1222-110 1
2-Fluorophenol (S)58 %09/21/17 21:32 367-12-409/20/17 18:1213-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 84 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-7A Lab ID:92355949019 Collected:09/18/17 17:00 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)75 %09/21/17 21:32 118-79-609/20/17 18:1227-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/22/17 16:03 67-64-1 L10.10 1
Benzene ND mg/kg 09/22/17 16:03 71-43-20.0052 1
Bromobenzene ND mg/kg 09/22/17 16:03 108-86-10.0052 1
Bromochloromethane ND mg/kg 09/22/17 16:03 74-97-50.0052 1
Bromodichloromethane ND mg/kg 09/22/17 16:03 75-27-40.0052 1
Bromoform ND mg/kg 09/22/17 16:03 75-25-20.0052 1
Bromomethane ND mg/kg 09/22/17 16:03 74-83-90.010 1
2-Butanone (MEK)ND mg/kg 09/22/17 16:03 78-93-30.10 1
n-Butylbenzene ND mg/kg 09/22/17 16:03 104-51-80.0052 1
sec-Butylbenzene ND mg/kg 09/22/17 16:03 135-98-80.0052 1
tert-Butylbenzene ND mg/kg 09/22/17 16:03 98-06-60.0052 1
Carbon tetrachloride ND mg/kg 09/22/17 16:03 56-23-50.0052 1
Chlorobenzene ND mg/kg 09/22/17 16:03 108-90-70.0052 1
Chloroethane ND mg/kg 09/22/17 16:03 75-00-30.010 1
Chloroform ND mg/kg 09/22/17 16:03 67-66-30.0052 1
Chloromethane ND mg/kg 09/22/17 16:03 74-87-30.010 1
2-Chlorotoluene ND mg/kg 09/22/17 16:03 95-49-80.0052 1
4-Chlorotoluene ND mg/kg 09/22/17 16:03 106-43-40.0052 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/22/17 16:03 96-12-80.0052 1
Dibromochloromethane ND mg/kg 09/22/17 16:03 124-48-10.0052 1
1,2-Dibromoethane (EDB)ND mg/kg 09/22/17 16:03 106-93-40.0052 1
Dibromomethane ND mg/kg 09/22/17 16:03 74-95-30.0052 1
1,2-Dichlorobenzene ND mg/kg 09/22/17 16:03 95-50-10.0052 1
1,3-Dichlorobenzene ND mg/kg 09/22/17 16:03 541-73-10.0052 1
1,4-Dichlorobenzene ND mg/kg 09/22/17 16:03 106-46-70.0052 1
Dichlorodifluoromethane ND mg/kg 09/22/17 16:03 75-71-80.010 1
1,1-Dichloroethane ND mg/kg 09/22/17 16:03 75-34-30.0052 1
1,2-Dichloroethane ND mg/kg 09/22/17 16:03 107-06-20.0052 1
1,1-Dichloroethene ND mg/kg 09/22/17 16:03 75-35-40.0052 1
cis-1,2-Dichloroethene ND mg/kg 09/22/17 16:03 156-59-20.0052 1
trans-1,2-Dichloroethene ND mg/kg 09/22/17 16:03 156-60-50.0052 1
1,2-Dichloropropane ND mg/kg 09/22/17 16:03 78-87-50.0052 1
1,3-Dichloropropane ND mg/kg 09/22/17 16:03 142-28-90.0052 1
2,2-Dichloropropane ND mg/kg 09/22/17 16:03 594-20-70.0052 1
1,1-Dichloropropene ND mg/kg 09/22/17 16:03 563-58-60.0052 1
cis-1,3-Dichloropropene ND mg/kg 09/22/17 16:03 10061-01-50.0052 1
trans-1,3-Dichloropropene ND mg/kg 09/22/17 16:03 10061-02-60.0052 1
Diisopropyl ether ND mg/kg 09/22/17 16:03 108-20-30.0052 1
Ethylbenzene ND mg/kg 09/22/17 16:03 100-41-40.0052 1
Hexachloro-1,3-butadiene ND mg/kg 09/22/17 16:03 87-68-30.0052 1
2-Hexanone ND mg/kg 09/22/17 16:03 591-78-60.052 1
Isopropylbenzene (Cumene)ND mg/kg 09/22/17 16:03 98-82-80.0052 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 85 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-7A Lab ID:92355949019 Collected:09/18/17 17:00 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND mg/kg 09/22/17 16:03 99-87-60.0052 1
Methylene Chloride ND mg/kg 09/22/17 16:03 75-09-20.021 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/22/17 16:03 108-10-10.052 1
Methyl-tert-butyl ether ND mg/kg 09/22/17 16:03 1634-04-40.0052 1
Naphthalene ND mg/kg 09/22/17 16:03 91-20-30.0052 1
n-Propylbenzene ND mg/kg 09/22/17 16:03 103-65-10.0052 1
Styrene ND mg/kg 09/22/17 16:03 100-42-50.0052 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/22/17 16:03 630-20-60.0052 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/22/17 16:03 79-34-50.0052 1
Tetrachloroethene ND mg/kg 09/22/17 16:03 127-18-40.0052 1
Toluene ND mg/kg 09/22/17 16:03 108-88-30.0052 1
1,2,3-Trichlorobenzene ND mg/kg 09/22/17 16:03 87-61-60.0052 1
1,2,4-Trichlorobenzene ND mg/kg 09/22/17 16:03 120-82-10.0052 1
1,1,1-Trichloroethane ND mg/kg 09/22/17 16:03 71-55-60.0052 1
1,1,2-Trichloroethane ND mg/kg 09/22/17 16:03 79-00-50.0052 1
Trichloroethene ND mg/kg 09/22/17 16:03 79-01-60.0052 1
Trichlorofluoromethane ND mg/kg 09/22/17 16:03 75-69-40.0052 1
1,2,3-Trichloropropane ND mg/kg 09/22/17 16:03 96-18-40.0052 1
1,2,4-Trimethylbenzene ND mg/kg 09/22/17 16:03 95-63-60.0052 1
1,3,5-Trimethylbenzene ND mg/kg 09/22/17 16:03 108-67-80.0052 1
Vinyl acetate ND mg/kg 09/22/17 16:03 108-05-40.052 1
Vinyl chloride ND mg/kg 09/22/17 16:03 75-01-40.010 1
Xylene (Total)ND mg/kg 09/22/17 16:03 1330-20-70.010 1
m&p-Xylene ND mg/kg 09/22/17 16:03 179601-23-10.010 1
o-Xylene ND mg/kg 09/22/17 16:03 95-47-60.0052 1
Surrogates
Toluene-d8 (S)97 %09/22/17 16:03 2037-26-570-130 1
4-Bromofluorobenzene (S)96 %09/22/17 16:03 460-00-470-130 1
1,2-Dichloroethane-d4 (S)105 %09/22/17 16:03 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.4 %09/21/17 11:120.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 86 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-7B Lab ID:92355949020 Collected:09/18/17 17:15 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/22/17 14:51 N209/21/17 08:0513.5 1
Aliphatic (C19-C36)ND mg/kg 09/22/17 14:51 N209/21/17 08:0513.5 1
Aromatic (C11-C22)ND mg/kg 09/22/17 14:51 N209/21/17 08:0513.5 1
Surrogates
Nonatriacontane (S)49 %09/22/17 14:51 7194-86-709/21/17 08:0540-140 1
o-Terphenyl (S)83 %09/22/17 14:51 84-15-109/21/17 08:0540-140 1
2-Fluorobiphenyl (S)112 %09/22/17 14:51 321-60-809/21/17 08:0540-140 1
2-Bromonaphthalene (S)112 %09/22/17 14:51 580-13-209/21/17 08:0540-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/22/17 00:29 N209/21/17 10:454.7 1
Aliphatic (C09-C12)ND mg/kg 09/22/17 00:29 N209/21/17 10:454.7 1
Aromatic (C09-C10)ND mg/kg 09/22/17 00:29 N209/21/17 10:454.7 1
Surrogates
4-Bromofluorobenzene (FID) (S)97 %09/22/17 00:29 460-00-409/21/17 10:4570-130 1
4-Bromofluorobenzene (PID) (S)93 %09/22/17 00:29 460-00-409/21/17 10:4570-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/21/17 17:12 83-32-909/20/17 18:120.44 1
Acenaphthylene ND mg/kg 09/21/17 17:12 208-96-809/20/17 18:120.44 1
Aniline ND mg/kg 09/21/17 17:12 62-53-309/20/17 18:120.44 1
Anthracene ND mg/kg 09/21/17 17:12 120-12-709/20/17 18:120.44 1
Benzo(a)anthracene ND mg/kg 09/21/17 17:12 56-55-309/20/17 18:120.44 1
Benzo(a)pyrene ND mg/kg 09/21/17 17:12 50-32-809/20/17 18:120.44 1
Benzo(b)fluoranthene ND mg/kg 09/21/17 17:12 205-99-209/20/17 18:120.44 1
Benzo(g,h,i)perylene ND mg/kg 09/21/17 17:12 191-24-209/20/17 18:120.44 1
Benzo(k)fluoranthene ND mg/kg 09/21/17 17:12 207-08-909/20/17 18:120.44 1
Benzoic Acid ND mg/kg 09/21/17 17:12 65-85-009/20/17 18:122.2 1
Benzyl alcohol ND mg/kg 09/21/17 17:12 100-51-609/20/17 18:120.88 1
4-Bromophenylphenyl ether ND mg/kg 09/21/17 17:12 101-55-309/20/17 18:120.44 1
Butylbenzylphthalate ND mg/kg 09/21/17 17:12 85-68-709/20/17 18:120.44 1
4-Chloro-3-methylphenol ND mg/kg 09/21/17 17:12 59-50-709/20/17 18:120.88 1
4-Chloroaniline ND mg/kg 09/21/17 17:12 106-47-809/20/17 18:122.2 1
bis(2-Chloroethoxy)methane ND mg/kg 09/21/17 17:12 111-91-109/20/17 18:120.44 1
bis(2-Chloroethyl) ether ND mg/kg 09/21/17 17:12 111-44-409/20/17 18:120.44 1
2-Chloronaphthalene ND mg/kg 09/21/17 17:12 91-58-709/20/17 18:120.44 1
2-Chlorophenol ND mg/kg 09/21/17 17:12 95-57-809/20/17 18:120.44 1
4-Chlorophenylphenyl ether ND mg/kg 09/21/17 17:12 7005-72-309/20/17 18:120.44 1
Chrysene ND mg/kg 09/21/17 17:12 218-01-909/20/17 18:120.44 1
Dibenz(a,h)anthracene ND mg/kg 09/21/17 17:12 53-70-309/20/17 18:120.44 1
Dibenzofuran ND mg/kg 09/21/17 17:12 132-64-909/20/17 18:120.44 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 17:12 95-50-109/20/17 18:120.44 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 17:12 541-73-109/20/17 18:120.44 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 17:12 106-46-709/20/17 18:120.44 1
3,3'-Dichlorobenzidine ND mg/kg 09/21/17 17:12 91-94-109/20/17 18:122.2 1
2,4-Dichlorophenol ND mg/kg 09/21/17 17:12 120-83-209/20/17 18:120.44 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 87 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-7B Lab ID:92355949020 Collected:09/18/17 17:15 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/21/17 17:12 84-66-209/20/17 18:120.44 1
2,4-Dimethylphenol ND mg/kg 09/21/17 17:12 105-67-909/20/17 18:120.44 1
Dimethylphthalate ND mg/kg 09/21/17 17:12 131-11-309/20/17 18:120.44 1
Di-n-butylphthalate ND mg/kg 09/21/17 17:12 84-74-209/20/17 18:120.44 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/21/17 17:12 534-52-109/20/17 18:120.88 1
2,4-Dinitrophenol ND mg/kg 09/21/17 17:12 51-28-509/20/17 18:122.2 1
2,4-Dinitrotoluene ND mg/kg 09/21/17 17:12 121-14-209/20/17 18:120.44 1
2,6-Dinitrotoluene ND mg/kg 09/21/17 17:12 606-20-209/20/17 18:120.44 1
Di-n-octylphthalate ND mg/kg 09/21/17 17:12 117-84-009/20/17 18:120.44 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/21/17 17:12 117-81-709/20/17 18:120.44 1
Fluoranthene ND mg/kg 09/21/17 17:12 206-44-009/20/17 18:120.44 1
Fluorene ND mg/kg 09/21/17 17:12 86-73-709/20/17 18:120.44 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 17:12 87-68-309/20/17 18:120.44 1
Hexachlorobenzene ND mg/kg 09/21/17 17:12 118-74-109/20/17 18:120.44 1
Hexachlorocyclopentadiene ND mg/kg 09/21/17 17:12 77-47-409/20/17 18:120.44 1
Hexachloroethane ND mg/kg 09/21/17 17:12 67-72-109/20/17 18:120.44 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/21/17 17:12 193-39-509/20/17 18:120.44 1
Isophorone ND mg/kg 09/21/17 17:12 78-59-109/20/17 18:120.44 1
1-Methylnaphthalene ND mg/kg 09/21/17 17:12 90-12-009/20/17 18:120.44 1
2-Methylnaphthalene ND mg/kg 09/21/17 17:12 91-57-609/20/17 18:120.44 1
2-Methylphenol(o-Cresol)ND mg/kg 09/21/17 17:12 95-48-709/20/17 18:120.44 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/21/17 17:12 15831-10-409/20/17 18:120.44 1
Naphthalene ND mg/kg 09/21/17 17:12 91-20-309/20/17 18:120.44 1
2-Nitroaniline ND mg/kg 09/21/17 17:12 88-74-409/20/17 18:122.2 1
3-Nitroaniline ND mg/kg 09/21/17 17:12 99-09-209/20/17 18:122.2 1
4-Nitroaniline ND mg/kg 09/21/17 17:12 100-01-609/20/17 18:120.88 1
Nitrobenzene ND mg/kg 09/21/17 17:12 98-95-309/20/17 18:120.44 1
2-Nitrophenol ND mg/kg 09/21/17 17:12 88-75-509/20/17 18:120.44 1
4-Nitrophenol ND mg/kg 09/21/17 17:12 100-02-709/20/17 18:122.2 1
N-Nitrosodimethylamine ND mg/kg 09/21/17 17:12 62-75-909/20/17 18:120.44 1
N-Nitroso-di-n-propylamine ND mg/kg 09/21/17 17:12 621-64-709/20/17 18:120.44 1
N-Nitrosodiphenylamine ND mg/kg 09/21/17 17:12 86-30-609/20/17 18:120.44 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/21/17 17:12 108-60-109/20/17 18:120.44 1
Pentachlorophenol ND mg/kg 09/21/17 17:12 87-86-509/20/17 18:122.2 1
Phenanthrene ND mg/kg 09/21/17 17:12 85-01-809/20/17 18:120.44 1
Phenol ND mg/kg 09/21/17 17:12 108-95-209/20/17 18:120.44 1
Pyrene ND mg/kg 09/21/17 17:12 129-00-009/20/17 18:120.44 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 17:12 120-82-109/20/17 18:120.44 1
2,4,5-Trichlorophenol ND mg/kg 09/21/17 17:12 95-95-409/20/17 18:120.44 1
2,4,6-Trichlorophenol ND mg/kg 09/21/17 17:12 88-06-209/20/17 18:120.44 1
Surrogates
Nitrobenzene-d5 (S)47 %09/21/17 17:12 4165-60-009/20/17 18:1223-110 1
2-Fluorobiphenyl (S)42 %09/21/17 17:12 321-60-809/20/17 18:1230-110 1
Terphenyl-d14 (S)76 %09/21/17 17:12 1718-51-009/20/17 18:1228-110 1
Phenol-d6 (S)33 %09/21/17 17:12 13127-88-309/20/17 18:1222-110 1
2-Fluorophenol (S)38 %09/21/17 17:12 367-12-409/20/17 18:1213-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 88 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-7B Lab ID:92355949020 Collected:09/18/17 17:15 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)72 %09/21/17 17:12 118-79-609/20/17 18:1227-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/22/17 16:23 67-64-1 L10.12 1
Benzene ND mg/kg 09/22/17 16:23 71-43-20.0062 1
Bromobenzene ND mg/kg 09/22/17 16:23 108-86-10.0062 1
Bromochloromethane ND mg/kg 09/22/17 16:23 74-97-50.0062 1
Bromodichloromethane ND mg/kg 09/22/17 16:23 75-27-40.0062 1
Bromoform ND mg/kg 09/22/17 16:23 75-25-20.0062 1
Bromomethane ND mg/kg 09/22/17 16:23 74-83-90.012 1
2-Butanone (MEK)ND mg/kg 09/22/17 16:23 78-93-30.12 1
n-Butylbenzene ND mg/kg 09/22/17 16:23 104-51-80.0062 1
sec-Butylbenzene ND mg/kg 09/22/17 16:23 135-98-80.0062 1
tert-Butylbenzene ND mg/kg 09/22/17 16:23 98-06-60.0062 1
Carbon tetrachloride ND mg/kg 09/22/17 16:23 56-23-50.0062 1
Chlorobenzene ND mg/kg 09/22/17 16:23 108-90-70.0062 1
Chloroethane ND mg/kg 09/22/17 16:23 75-00-30.012 1
Chloroform ND mg/kg 09/22/17 16:23 67-66-30.0062 1
Chloromethane ND mg/kg 09/22/17 16:23 74-87-30.012 1
2-Chlorotoluene ND mg/kg 09/22/17 16:23 95-49-80.0062 1
4-Chlorotoluene ND mg/kg 09/22/17 16:23 106-43-40.0062 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/22/17 16:23 96-12-80.0062 1
Dibromochloromethane ND mg/kg 09/22/17 16:23 124-48-10.0062 1
1,2-Dibromoethane (EDB)ND mg/kg 09/22/17 16:23 106-93-40.0062 1
Dibromomethane ND mg/kg 09/22/17 16:23 74-95-30.0062 1
1,2-Dichlorobenzene ND mg/kg 09/22/17 16:23 95-50-10.0062 1
1,3-Dichlorobenzene ND mg/kg 09/22/17 16:23 541-73-10.0062 1
1,4-Dichlorobenzene ND mg/kg 09/22/17 16:23 106-46-70.0062 1
Dichlorodifluoromethane ND mg/kg 09/22/17 16:23 75-71-80.012 1
1,1-Dichloroethane ND mg/kg 09/22/17 16:23 75-34-30.0062 1
1,2-Dichloroethane ND mg/kg 09/22/17 16:23 107-06-20.0062 1
1,1-Dichloroethene ND mg/kg 09/22/17 16:23 75-35-40.0062 1
cis-1,2-Dichloroethene ND mg/kg 09/22/17 16:23 156-59-20.0062 1
trans-1,2-Dichloroethene ND mg/kg 09/22/17 16:23 156-60-50.0062 1
1,2-Dichloropropane ND mg/kg 09/22/17 16:23 78-87-50.0062 1
1,3-Dichloropropane ND mg/kg 09/22/17 16:23 142-28-90.0062 1
2,2-Dichloropropane ND mg/kg 09/22/17 16:23 594-20-70.0062 1
1,1-Dichloropropene ND mg/kg 09/22/17 16:23 563-58-60.0062 1
cis-1,3-Dichloropropene ND mg/kg 09/22/17 16:23 10061-01-50.0062 1
trans-1,3-Dichloropropene ND mg/kg 09/22/17 16:23 10061-02-60.0062 1
Diisopropyl ether ND mg/kg 09/22/17 16:23 108-20-30.0062 1
Ethylbenzene ND mg/kg 09/22/17 16:23 100-41-40.0062 1
Hexachloro-1,3-butadiene ND mg/kg 09/22/17 16:23 87-68-30.0062 1
2-Hexanone ND mg/kg 09/22/17 16:23 591-78-60.062 1
Isopropylbenzene (Cumene)ND mg/kg 09/22/17 16:23 98-82-80.0062 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 89 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-7B Lab ID:92355949020 Collected:09/18/17 17:15 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND mg/kg 09/22/17 16:23 99-87-60.0062 1
Methylene Chloride ND mg/kg 09/22/17 16:23 75-09-20.025 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/22/17 16:23 108-10-10.062 1
Methyl-tert-butyl ether ND mg/kg 09/22/17 16:23 1634-04-40.0062 1
Naphthalene ND mg/kg 09/22/17 16:23 91-20-30.0062 1
n-Propylbenzene ND mg/kg 09/22/17 16:23 103-65-10.0062 1
Styrene ND mg/kg 09/22/17 16:23 100-42-50.0062 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/22/17 16:23 630-20-60.0062 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/22/17 16:23 79-34-50.0062 1
Tetrachloroethene ND mg/kg 09/22/17 16:23 127-18-40.0062 1
Toluene ND mg/kg 09/22/17 16:23 108-88-30.0062 1
1,2,3-Trichlorobenzene ND mg/kg 09/22/17 16:23 87-61-60.0062 1
1,2,4-Trichlorobenzene ND mg/kg 09/22/17 16:23 120-82-10.0062 1
1,1,1-Trichloroethane ND mg/kg 09/22/17 16:23 71-55-60.0062 1
1,1,2-Trichloroethane ND mg/kg 09/22/17 16:23 79-00-50.0062 1
Trichloroethene ND mg/kg 09/22/17 16:23 79-01-60.0062 1
Trichlorofluoromethane ND mg/kg 09/22/17 16:23 75-69-40.0062 1
1,2,3-Trichloropropane ND mg/kg 09/22/17 16:23 96-18-40.0062 1
1,2,4-Trimethylbenzene ND mg/kg 09/22/17 16:23 95-63-60.0062 1
1,3,5-Trimethylbenzene ND mg/kg 09/22/17 16:23 108-67-80.0062 1
Vinyl acetate ND mg/kg 09/22/17 16:23 108-05-40.062 1
Vinyl chloride ND mg/kg 09/22/17 16:23 75-01-40.012 1
Xylene (Total)ND mg/kg 09/22/17 16:23 1330-20-70.012 1
m&p-Xylene ND mg/kg 09/22/17 16:23 179601-23-10.012 1
o-Xylene ND mg/kg 09/22/17 16:23 95-47-60.0062 1
Surrogates
Toluene-d8 (S)101 %09/22/17 16:23 2037-26-570-130 1
4-Bromofluorobenzene (S)100 %09/22/17 16:23 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %09/22/17 16:23 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 25.7 %09/21/17 11:130.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 90 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-7C Lab ID:92355949021 Collected:09/18/17 17:25 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/25/17 17:34 N209/23/17 08:3712.8 1
Aliphatic (C19-C36)32.8 mg/kg 09/25/17 17:34 N209/23/17 08:3712.8 1
Aromatic (C11-C22)19.1 mg/kg 09/25/17 17:34 N209/23/17 08:3712.8 1
Surrogates
Nonatriacontane (S)60 %09/25/17 17:34 7194-86-709/23/17 08:3740-140 1
o-Terphenyl (S)75 %09/25/17 17:34 84-15-109/23/17 08:3740-140 1
2-Fluorobiphenyl (S)99 %09/25/17 17:34 321-60-809/23/17 08:3740-140 1
2-Bromonaphthalene (S)53 %09/25/17 17:34 580-13-209/23/17 08:3740-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/26/17 00:21 N209/25/17 10:304.1 1
Aliphatic (C09-C12)ND mg/kg 09/26/17 00:21 N209/25/17 10:304.1 1
Aromatic (C09-C10)ND mg/kg 09/26/17 00:21 N209/25/17 10:304.1 1
Surrogates
4-Bromofluorobenzene (FID) (S)98 %09/26/17 00:21 460-00-409/25/17 10:3070-130 1
4-Bromofluorobenzene (PID) (S)115 %09/26/17 00:21 460-00-409/25/17 10:3070-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/21/17 22:01 83-32-909/20/17 20:560.43 1
Acenaphthylene ND mg/kg 09/21/17 22:01 208-96-809/20/17 20:560.43 1
Aniline ND mg/kg 09/21/17 22:01 62-53-309/20/17 20:560.43 1
Anthracene ND mg/kg 09/21/17 22:01 120-12-709/20/17 20:560.43 1
Benzo(a)anthracene ND mg/kg 09/21/17 22:01 56-55-309/20/17 20:560.43 1
Benzo(a)pyrene ND mg/kg 09/21/17 22:01 50-32-809/20/17 20:560.43 1
Benzo(b)fluoranthene ND mg/kg 09/21/17 22:01 205-99-209/20/17 20:560.43 1
Benzo(g,h,i)perylene ND mg/kg 09/21/17 22:01 191-24-209/20/17 20:560.43 1
Benzo(k)fluoranthene ND mg/kg 09/21/17 22:01 207-08-909/20/17 20:560.43 1
Benzoic Acid ND mg/kg 09/21/17 22:01 65-85-009/20/17 20:562.1 1
Benzyl alcohol ND mg/kg 09/21/17 22:01 100-51-609/20/17 20:560.85 1
4-Bromophenylphenyl ether ND mg/kg 09/21/17 22:01 101-55-309/20/17 20:560.43 1
Butylbenzylphthalate ND mg/kg 09/21/17 22:01 85-68-709/20/17 20:560.43 1
4-Chloro-3-methylphenol ND mg/kg 09/21/17 22:01 59-50-709/20/17 20:560.85 1
4-Chloroaniline ND mg/kg 09/21/17 22:01 106-47-809/20/17 20:562.1 1
bis(2-Chloroethoxy)methane ND mg/kg 09/21/17 22:01 111-91-109/20/17 20:560.43 1
bis(2-Chloroethyl) ether ND mg/kg 09/21/17 22:01 111-44-409/20/17 20:560.43 1
2-Chloronaphthalene ND mg/kg 09/21/17 22:01 91-58-709/20/17 20:560.43 1
2-Chlorophenol ND mg/kg 09/21/17 22:01 95-57-809/20/17 20:560.43 1
4-Chlorophenylphenyl ether ND mg/kg 09/21/17 22:01 7005-72-309/20/17 20:560.43 1
Chrysene ND mg/kg 09/21/17 22:01 218-01-909/20/17 20:560.43 1
Dibenz(a,h)anthracene ND mg/kg 09/21/17 22:01 53-70-309/20/17 20:560.43 1
Dibenzofuran ND mg/kg 09/21/17 22:01 132-64-909/20/17 20:560.43 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 22:01 95-50-1 M109/20/17 20:560.43 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 22:01 541-73-1 L209/20/17 20:560.43 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 22:01 106-46-709/20/17 20:560.43 1
3,3'-Dichlorobenzidine ND mg/kg 09/21/17 22:01 91-94-109/20/17 20:562.1 1
2,4-Dichlorophenol ND mg/kg 09/21/17 22:01 120-83-209/20/17 20:560.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 91 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-7C Lab ID:92355949021 Collected:09/18/17 17:25 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/21/17 22:01 84-66-209/20/17 20:560.43 1
2,4-Dimethylphenol ND mg/kg 09/21/17 22:01 105-67-909/20/17 20:560.43 1
Dimethylphthalate ND mg/kg 09/21/17 22:01 131-11-309/20/17 20:560.43 1
Di-n-butylphthalate ND mg/kg 09/21/17 22:01 84-74-209/20/17 20:560.43 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/21/17 22:01 534-52-109/20/17 20:560.85 1
2,4-Dinitrophenol ND mg/kg 09/21/17 22:01 51-28-509/20/17 20:562.1 1
2,4-Dinitrotoluene ND mg/kg 09/21/17 22:01 121-14-209/20/17 20:560.43 1
2,6-Dinitrotoluene ND mg/kg 09/21/17 22:01 606-20-209/20/17 20:560.43 1
Di-n-octylphthalate ND mg/kg 09/21/17 22:01 117-84-009/20/17 20:560.43 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/21/17 22:01 117-81-709/20/17 20:560.43 1
Fluoranthene ND mg/kg 09/21/17 22:01 206-44-009/20/17 20:560.43 1
Fluorene ND mg/kg 09/21/17 22:01 86-73-709/20/17 20:560.43 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 22:01 87-68-309/20/17 20:560.43 1
Hexachlorobenzene ND mg/kg 09/21/17 22:01 118-74-109/20/17 20:560.43 1
Hexachlorocyclopentadiene ND mg/kg 09/21/17 22:01 77-47-409/20/17 20:560.43 1
Hexachloroethane ND mg/kg 09/21/17 22:01 67-72-109/20/17 20:560.43 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/21/17 22:01 193-39-509/20/17 20:560.43 1
Isophorone ND mg/kg 09/21/17 22:01 78-59-109/20/17 20:560.43 1
1-Methylnaphthalene ND mg/kg 09/21/17 22:01 90-12-009/20/17 20:560.43 1
2-Methylnaphthalene ND mg/kg 09/21/17 22:01 91-57-609/20/17 20:560.43 1
2-Methylphenol(o-Cresol)ND mg/kg 09/21/17 22:01 95-48-709/20/17 20:560.43 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/21/17 22:01 15831-10-409/20/17 20:560.43 1
Naphthalene ND mg/kg 09/21/17 22:01 91-20-309/20/17 20:560.43 1
2-Nitroaniline ND mg/kg 09/21/17 22:01 88-74-409/20/17 20:562.1 1
3-Nitroaniline ND mg/kg 09/21/17 22:01 99-09-209/20/17 20:562.1 1
4-Nitroaniline ND mg/kg 09/21/17 22:01 100-01-609/20/17 20:560.85 1
Nitrobenzene ND mg/kg 09/21/17 22:01 98-95-309/20/17 20:560.43 1
2-Nitrophenol ND mg/kg 09/21/17 22:01 88-75-509/20/17 20:560.43 1
4-Nitrophenol ND mg/kg 09/21/17 22:01 100-02-709/20/17 20:562.1 1
N-Nitrosodimethylamine ND mg/kg 09/21/17 22:01 62-75-909/20/17 20:560.43 1
N-Nitroso-di-n-propylamine ND mg/kg 09/21/17 22:01 621-64-709/20/17 20:560.43 1
N-Nitrosodiphenylamine ND mg/kg 09/21/17 22:01 86-30-609/20/17 20:560.43 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/21/17 22:01 108-60-1 M109/20/17 20:560.43 1
Pentachlorophenol ND mg/kg 09/21/17 22:01 87-86-509/20/17 20:562.1 1
Phenanthrene ND mg/kg 09/21/17 22:01 85-01-809/20/17 20:560.43 1
Phenol ND mg/kg 09/21/17 22:01 108-95-209/20/17 20:560.43 1
Pyrene ND mg/kg 09/21/17 22:01 129-00-009/20/17 20:560.43 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 22:01 120-82-109/20/17 20:560.43 1
2,4,5-Trichlorophenol ND mg/kg 09/21/17 22:01 95-95-409/20/17 20:560.43 1
2,4,6-Trichlorophenol ND mg/kg 09/21/17 22:01 88-06-209/20/17 20:560.43 1
Surrogates
Nitrobenzene-d5 (S)42 %09/21/17 22:01 4165-60-009/20/17 20:5623-110 1
2-Fluorobiphenyl (S)41 %09/21/17 22:01 321-60-809/20/17 20:5630-110 1
Terphenyl-d14 (S)61 %09/21/17 22:01 1718-51-009/20/17 20:5628-110 1
Phenol-d6 (S)42 %09/21/17 22:01 13127-88-309/20/17 20:5622-110 1
2-Fluorophenol (S)43 %09/21/17 22:01 367-12-409/20/17 20:5613-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 92 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-7C Lab ID:92355949021 Collected:09/18/17 17:25 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)53 %09/21/17 22:01 118-79-609/20/17 20:5627-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/22/17 16:43 67-64-1 L10.093 1
Benzene ND mg/kg 09/22/17 16:43 71-43-20.0047 1
Bromobenzene ND mg/kg 09/22/17 16:43 108-86-10.0047 1
Bromochloromethane ND mg/kg 09/22/17 16:43 74-97-50.0047 1
Bromodichloromethane ND mg/kg 09/22/17 16:43 75-27-40.0047 1
Bromoform ND mg/kg 09/22/17 16:43 75-25-20.0047 1
Bromomethane ND mg/kg 09/22/17 16:43 74-83-90.0093 1
2-Butanone (MEK)ND mg/kg 09/22/17 16:43 78-93-30.093 1
n-Butylbenzene ND mg/kg 09/22/17 16:43 104-51-80.0047 1
sec-Butylbenzene ND mg/kg 09/22/17 16:43 135-98-80.0047 1
tert-Butylbenzene ND mg/kg 09/22/17 16:43 98-06-60.0047 1
Carbon tetrachloride ND mg/kg 09/22/17 16:43 56-23-50.0047 1
Chlorobenzene ND mg/kg 09/22/17 16:43 108-90-70.0047 1
Chloroethane ND mg/kg 09/22/17 16:43 75-00-30.0093 1
Chloroform ND mg/kg 09/22/17 16:43 67-66-30.0047 1
Chloromethane ND mg/kg 09/22/17 16:43 74-87-30.0093 1
2-Chlorotoluene ND mg/kg 09/22/17 16:43 95-49-80.0047 1
4-Chlorotoluene ND mg/kg 09/22/17 16:43 106-43-40.0047 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/22/17 16:43 96-12-80.0047 1
Dibromochloromethane ND mg/kg 09/22/17 16:43 124-48-10.0047 1
1,2-Dibromoethane (EDB)ND mg/kg 09/22/17 16:43 106-93-40.0047 1
Dibromomethane ND mg/kg 09/22/17 16:43 74-95-30.0047 1
1,2-Dichlorobenzene ND mg/kg 09/22/17 16:43 95-50-10.0047 1
1,3-Dichlorobenzene ND mg/kg 09/22/17 16:43 541-73-10.0047 1
1,4-Dichlorobenzene ND mg/kg 09/22/17 16:43 106-46-70.0047 1
Dichlorodifluoromethane ND mg/kg 09/22/17 16:43 75-71-80.0093 1
1,1-Dichloroethane ND mg/kg 09/22/17 16:43 75-34-30.0047 1
1,2-Dichloroethane ND mg/kg 09/22/17 16:43 107-06-20.0047 1
1,1-Dichloroethene ND mg/kg 09/22/17 16:43 75-35-40.0047 1
cis-1,2-Dichloroethene ND mg/kg 09/22/17 16:43 156-59-20.0047 1
trans-1,2-Dichloroethene ND mg/kg 09/22/17 16:43 156-60-50.0047 1
1,2-Dichloropropane ND mg/kg 09/22/17 16:43 78-87-50.0047 1
1,3-Dichloropropane ND mg/kg 09/22/17 16:43 142-28-90.0047 1
2,2-Dichloropropane ND mg/kg 09/22/17 16:43 594-20-70.0047 1
1,1-Dichloropropene ND mg/kg 09/22/17 16:43 563-58-60.0047 1
cis-1,3-Dichloropropene ND mg/kg 09/22/17 16:43 10061-01-50.0047 1
trans-1,3-Dichloropropene ND mg/kg 09/22/17 16:43 10061-02-60.0047 1
Diisopropyl ether ND mg/kg 09/22/17 16:43 108-20-30.0047 1
Ethylbenzene ND mg/kg 09/22/17 16:43 100-41-40.0047 1
Hexachloro-1,3-butadiene ND mg/kg 09/22/17 16:43 87-68-30.0047 1
2-Hexanone ND mg/kg 09/22/17 16:43 591-78-60.047 1
Isopropylbenzene (Cumene)ND mg/kg 09/22/17 16:43 98-82-80.0047 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 93 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-7C Lab ID:92355949021 Collected:09/18/17 17:25 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND mg/kg 09/22/17 16:43 99-87-60.0047 1
Methylene Chloride ND mg/kg 09/22/17 16:43 75-09-20.019 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/22/17 16:43 108-10-10.047 1
Methyl-tert-butyl ether ND mg/kg 09/22/17 16:43 1634-04-40.0047 1
Naphthalene ND mg/kg 09/22/17 16:43 91-20-30.0047 1
n-Propylbenzene ND mg/kg 09/22/17 16:43 103-65-10.0047 1
Styrene ND mg/kg 09/22/17 16:43 100-42-50.0047 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/22/17 16:43 630-20-60.0047 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/22/17 16:43 79-34-50.0047 1
Tetrachloroethene ND mg/kg 09/22/17 16:43 127-18-40.0047 1
Toluene ND mg/kg 09/22/17 16:43 108-88-30.0047 1
1,2,3-Trichlorobenzene ND mg/kg 09/22/17 16:43 87-61-60.0047 1
1,2,4-Trichlorobenzene ND mg/kg 09/22/17 16:43 120-82-10.0047 1
1,1,1-Trichloroethane ND mg/kg 09/22/17 16:43 71-55-60.0047 1
1,1,2-Trichloroethane ND mg/kg 09/22/17 16:43 79-00-50.0047 1
Trichloroethene ND mg/kg 09/22/17 16:43 79-01-60.0047 1
Trichlorofluoromethane ND mg/kg 09/22/17 16:43 75-69-40.0047 1
1,2,3-Trichloropropane ND mg/kg 09/22/17 16:43 96-18-40.0047 1
1,2,4-Trimethylbenzene ND mg/kg 09/22/17 16:43 95-63-60.0047 1
1,3,5-Trimethylbenzene ND mg/kg 09/22/17 16:43 108-67-80.0047 1
Vinyl acetate ND mg/kg 09/22/17 16:43 108-05-40.047 1
Vinyl chloride ND mg/kg 09/22/17 16:43 75-01-40.0093 1
Xylene (Total)ND mg/kg 09/22/17 16:43 1330-20-70.0093 1
m&p-Xylene ND mg/kg 09/22/17 16:43 179601-23-10.0093 1
o-Xylene ND mg/kg 09/22/17 16:43 95-47-60.0047 1
Surrogates
Toluene-d8 (S)100 %09/22/17 16:43 2037-26-570-130 1
4-Bromofluorobenzene (S)100 %09/22/17 16:43 460-00-470-130 1
1,2-Dichloroethane-d4 (S)108 %09/22/17 16:43 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 22.9 %09/21/17 11:130.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 94 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-8A Lab ID:92355949022 Collected:09/18/17 17:30 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/25/17 18:02 N209/23/17 08:3712.6 1
Aliphatic (C19-C36)ND mg/kg 09/25/17 18:02 N209/23/17 08:3712.6 1
Aromatic (C11-C22)ND mg/kg 09/25/17 18:02 N209/23/17 08:3712.6 1
Surrogates
Nonatriacontane (S)69 %09/25/17 18:02 7194-86-709/23/17 08:3740-140 1
o-Terphenyl (S)59 %09/25/17 18:02 84-15-109/23/17 08:3740-140 1
2-Fluorobiphenyl (S)65 %09/25/17 18:02 321-60-809/23/17 08:3740-140 1
2-Bromonaphthalene (S)37 %09/25/17 18:02 580-13-2 S009/23/17 08:3740-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/26/17 00:49 N209/25/17 10:303.5 1
Aliphatic (C09-C12)ND mg/kg 09/26/17 00:49 N209/25/17 10:303.5 1
Aromatic (C09-C10)ND mg/kg 09/26/17 00:49 N209/25/17 10:303.5 1
Surrogates
4-Bromofluorobenzene (FID) (S)100 %09/26/17 00:49 460-00-409/25/17 10:3070-130 1
4-Bromofluorobenzene (PID) (S)120 %09/26/17 00:49 460-00-409/25/17 10:3070-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/21/17 22:59 83-32-909/20/17 20:560.43 1
Acenaphthylene ND mg/kg 09/21/17 22:59 208-96-809/20/17 20:560.43 1
Aniline ND mg/kg 09/21/17 22:59 62-53-309/20/17 20:560.43 1
Anthracene ND mg/kg 09/21/17 22:59 120-12-709/20/17 20:560.43 1
Benzo(a)anthracene ND mg/kg 09/21/17 22:59 56-55-309/20/17 20:560.43 1
Benzo(a)pyrene ND mg/kg 09/21/17 22:59 50-32-809/20/17 20:560.43 1
Benzo(b)fluoranthene ND mg/kg 09/21/17 22:59 205-99-209/20/17 20:560.43 1
Benzo(g,h,i)perylene ND mg/kg 09/21/17 22:59 191-24-209/20/17 20:560.43 1
Benzo(k)fluoranthene ND mg/kg 09/21/17 22:59 207-08-909/20/17 20:560.43 1
Benzoic Acid ND mg/kg 09/21/17 22:59 65-85-009/20/17 20:562.1 1
Benzyl alcohol ND mg/kg 09/21/17 22:59 100-51-609/20/17 20:560.85 1
4-Bromophenylphenyl ether ND mg/kg 09/21/17 22:59 101-55-309/20/17 20:560.43 1
Butylbenzylphthalate ND mg/kg 09/21/17 22:59 85-68-709/20/17 20:560.43 1
4-Chloro-3-methylphenol ND mg/kg 09/21/17 22:59 59-50-709/20/17 20:560.85 1
4-Chloroaniline ND mg/kg 09/21/17 22:59 106-47-809/20/17 20:562.1 1
bis(2-Chloroethoxy)methane ND mg/kg 09/21/17 22:59 111-91-109/20/17 20:560.43 1
bis(2-Chloroethyl) ether ND mg/kg 09/21/17 22:59 111-44-409/20/17 20:560.43 1
2-Chloronaphthalene ND mg/kg 09/21/17 22:59 91-58-709/20/17 20:560.43 1
2-Chlorophenol ND mg/kg 09/21/17 22:59 95-57-809/20/17 20:560.43 1
4-Chlorophenylphenyl ether ND mg/kg 09/21/17 22:59 7005-72-309/20/17 20:560.43 1
Chrysene ND mg/kg 09/21/17 22:59 218-01-909/20/17 20:560.43 1
Dibenz(a,h)anthracene ND mg/kg 09/21/17 22:59 53-70-309/20/17 20:560.43 1
Dibenzofuran ND mg/kg 09/21/17 22:59 132-64-909/20/17 20:560.43 1
1,2-Dichlorobenzene ND mg/kg 09/21/17 22:59 95-50-109/20/17 20:560.43 1
1,3-Dichlorobenzene ND mg/kg 09/21/17 22:59 541-73-1 L209/20/17 20:560.43 1
1,4-Dichlorobenzene ND mg/kg 09/21/17 22:59 106-46-709/20/17 20:560.43 1
3,3'-Dichlorobenzidine ND mg/kg 09/21/17 22:59 91-94-109/20/17 20:562.1 1
2,4-Dichlorophenol ND mg/kg 09/21/17 22:59 120-83-209/20/17 20:560.43 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 95 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-8A Lab ID:92355949022 Collected:09/18/17 17:30 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/21/17 22:59 84-66-209/20/17 20:560.43 1
2,4-Dimethylphenol ND mg/kg 09/21/17 22:59 105-67-909/20/17 20:560.43 1
Dimethylphthalate ND mg/kg 09/21/17 22:59 131-11-309/20/17 20:560.43 1
Di-n-butylphthalate ND mg/kg 09/21/17 22:59 84-74-209/20/17 20:560.43 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/21/17 22:59 534-52-109/20/17 20:560.85 1
2,4-Dinitrophenol ND mg/kg 09/21/17 22:59 51-28-509/20/17 20:562.1 1
2,4-Dinitrotoluene ND mg/kg 09/21/17 22:59 121-14-209/20/17 20:560.43 1
2,6-Dinitrotoluene ND mg/kg 09/21/17 22:59 606-20-209/20/17 20:560.43 1
Di-n-octylphthalate ND mg/kg 09/21/17 22:59 117-84-009/20/17 20:560.43 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/21/17 22:59 117-81-709/20/17 20:560.43 1
Fluoranthene ND mg/kg 09/21/17 22:59 206-44-009/20/17 20:560.43 1
Fluorene ND mg/kg 09/21/17 22:59 86-73-709/20/17 20:560.43 1
Hexachloro-1,3-butadiene ND mg/kg 09/21/17 22:59 87-68-309/20/17 20:560.43 1
Hexachlorobenzene ND mg/kg 09/21/17 22:59 118-74-109/20/17 20:560.43 1
Hexachlorocyclopentadiene ND mg/kg 09/21/17 22:59 77-47-409/20/17 20:560.43 1
Hexachloroethane ND mg/kg 09/21/17 22:59 67-72-109/20/17 20:560.43 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/21/17 22:59 193-39-509/20/17 20:560.43 1
Isophorone ND mg/kg 09/21/17 22:59 78-59-109/20/17 20:560.43 1
1-Methylnaphthalene ND mg/kg 09/21/17 22:59 90-12-009/20/17 20:560.43 1
2-Methylnaphthalene ND mg/kg 09/21/17 22:59 91-57-609/20/17 20:560.43 1
2-Methylphenol(o-Cresol)ND mg/kg 09/21/17 22:59 95-48-709/20/17 20:560.43 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/21/17 22:59 15831-10-409/20/17 20:560.43 1
Naphthalene ND mg/kg 09/21/17 22:59 91-20-309/20/17 20:560.43 1
2-Nitroaniline ND mg/kg 09/21/17 22:59 88-74-409/20/17 20:562.1 1
3-Nitroaniline ND mg/kg 09/21/17 22:59 99-09-209/20/17 20:562.1 1
4-Nitroaniline ND mg/kg 09/21/17 22:59 100-01-609/20/17 20:560.85 1
Nitrobenzene ND mg/kg 09/21/17 22:59 98-95-309/20/17 20:560.43 1
2-Nitrophenol ND mg/kg 09/21/17 22:59 88-75-509/20/17 20:560.43 1
4-Nitrophenol ND mg/kg 09/21/17 22:59 100-02-709/20/17 20:562.1 1
N-Nitrosodimethylamine ND mg/kg 09/21/17 22:59 62-75-909/20/17 20:560.43 1
N-Nitroso-di-n-propylamine ND mg/kg 09/21/17 22:59 621-64-709/20/17 20:560.43 1
N-Nitrosodiphenylamine ND mg/kg 09/21/17 22:59 86-30-609/20/17 20:560.43 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/21/17 22:59 108-60-109/20/17 20:560.43 1
Pentachlorophenol ND mg/kg 09/21/17 22:59 87-86-509/20/17 20:562.1 1
Phenanthrene ND mg/kg 09/21/17 22:59 85-01-809/20/17 20:560.43 1
Phenol ND mg/kg 09/21/17 22:59 108-95-209/20/17 20:560.43 1
Pyrene ND mg/kg 09/21/17 22:59 129-00-009/20/17 20:560.43 1
1,2,4-Trichlorobenzene ND mg/kg 09/21/17 22:59 120-82-109/20/17 20:560.43 1
2,4,5-Trichlorophenol ND mg/kg 09/21/17 22:59 95-95-409/20/17 20:560.43 1
2,4,6-Trichlorophenol ND mg/kg 09/21/17 22:59 88-06-209/20/17 20:560.43 1
Surrogates
Nitrobenzene-d5 (S)26 %09/21/17 22:59 4165-60-009/20/17 20:5623-110 1
2-Fluorobiphenyl (S)25 %09/21/17 22:59 321-60-8 S009/20/17 20:5630-110 1
Terphenyl-d14 (S)58 %09/21/17 22:59 1718-51-009/20/17 20:5628-110 1
Phenol-d6 (S)28 %09/21/17 22:59 13127-88-309/20/17 20:5622-110 1
2-Fluorophenol (S)27 %09/21/17 22:59 367-12-409/20/17 20:5613-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 96 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-8A Lab ID:92355949022 Collected:09/18/17 17:30 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)56 %09/21/17 22:59 118-79-609/20/17 20:5627-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/22/17 17:02 67-64-1 L10.12 1
Benzene ND mg/kg 09/22/17 17:02 71-43-20.0059 1
Bromobenzene ND mg/kg 09/22/17 17:02 108-86-10.0059 1
Bromochloromethane ND mg/kg 09/22/17 17:02 74-97-50.0059 1
Bromodichloromethane ND mg/kg 09/22/17 17:02 75-27-40.0059 1
Bromoform ND mg/kg 09/22/17 17:02 75-25-20.0059 1
Bromomethane ND mg/kg 09/22/17 17:02 74-83-90.012 1
2-Butanone (MEK)ND mg/kg 09/22/17 17:02 78-93-30.12 1
n-Butylbenzene ND mg/kg 09/22/17 17:02 104-51-80.0059 1
sec-Butylbenzene ND mg/kg 09/22/17 17:02 135-98-80.0059 1
tert-Butylbenzene ND mg/kg 09/22/17 17:02 98-06-60.0059 1
Carbon tetrachloride ND mg/kg 09/22/17 17:02 56-23-50.0059 1
Chlorobenzene ND mg/kg 09/22/17 17:02 108-90-70.0059 1
Chloroethane ND mg/kg 09/22/17 17:02 75-00-30.012 1
Chloroform ND mg/kg 09/22/17 17:02 67-66-30.0059 1
Chloromethane ND mg/kg 09/22/17 17:02 74-87-30.012 1
2-Chlorotoluene ND mg/kg 09/22/17 17:02 95-49-80.0059 1
4-Chlorotoluene ND mg/kg 09/22/17 17:02 106-43-40.0059 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/22/17 17:02 96-12-80.0059 1
Dibromochloromethane ND mg/kg 09/22/17 17:02 124-48-10.0059 1
1,2-Dibromoethane (EDB)ND mg/kg 09/22/17 17:02 106-93-40.0059 1
Dibromomethane ND mg/kg 09/22/17 17:02 74-95-30.0059 1
1,2-Dichlorobenzene ND mg/kg 09/22/17 17:02 95-50-10.0059 1
1,3-Dichlorobenzene ND mg/kg 09/22/17 17:02 541-73-10.0059 1
1,4-Dichlorobenzene ND mg/kg 09/22/17 17:02 106-46-70.0059 1
Dichlorodifluoromethane ND mg/kg 09/22/17 17:02 75-71-80.012 1
1,1-Dichloroethane ND mg/kg 09/22/17 17:02 75-34-30.0059 1
1,2-Dichloroethane ND mg/kg 09/22/17 17:02 107-06-20.0059 1
1,1-Dichloroethene ND mg/kg 09/22/17 17:02 75-35-40.0059 1
cis-1,2-Dichloroethene ND mg/kg 09/22/17 17:02 156-59-20.0059 1
trans-1,2-Dichloroethene ND mg/kg 09/22/17 17:02 156-60-50.0059 1
1,2-Dichloropropane ND mg/kg 09/22/17 17:02 78-87-50.0059 1
1,3-Dichloropropane ND mg/kg 09/22/17 17:02 142-28-90.0059 1
2,2-Dichloropropane ND mg/kg 09/22/17 17:02 594-20-70.0059 1
1,1-Dichloropropene ND mg/kg 09/22/17 17:02 563-58-60.0059 1
cis-1,3-Dichloropropene ND mg/kg 09/22/17 17:02 10061-01-50.0059 1
trans-1,3-Dichloropropene ND mg/kg 09/22/17 17:02 10061-02-60.0059 1
Diisopropyl ether ND mg/kg 09/22/17 17:02 108-20-30.0059 1
Ethylbenzene ND mg/kg 09/22/17 17:02 100-41-40.0059 1
Hexachloro-1,3-butadiene ND mg/kg 09/22/17 17:02 87-68-30.0059 1
2-Hexanone ND mg/kg 09/22/17 17:02 591-78-60.059 1
Isopropylbenzene (Cumene)ND mg/kg 09/22/17 17:02 98-82-80.0059 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 97 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-8A Lab ID:92355949022 Collected:09/18/17 17:30 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND mg/kg 09/22/17 17:02 99-87-60.0059 1
Methylene Chloride ND mg/kg 09/22/17 17:02 75-09-20.024 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/22/17 17:02 108-10-10.059 1
Methyl-tert-butyl ether ND mg/kg 09/22/17 17:02 1634-04-40.0059 1
Naphthalene ND mg/kg 09/22/17 17:02 91-20-30.0059 1
n-Propylbenzene ND mg/kg 09/22/17 17:02 103-65-10.0059 1
Styrene ND mg/kg 09/22/17 17:02 100-42-50.0059 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/22/17 17:02 630-20-60.0059 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/22/17 17:02 79-34-50.0059 1
Tetrachloroethene ND mg/kg 09/22/17 17:02 127-18-40.0059 1
Toluene ND mg/kg 09/22/17 17:02 108-88-30.0059 1
1,2,3-Trichlorobenzene ND mg/kg 09/22/17 17:02 87-61-60.0059 1
1,2,4-Trichlorobenzene ND mg/kg 09/22/17 17:02 120-82-10.0059 1
1,1,1-Trichloroethane ND mg/kg 09/22/17 17:02 71-55-60.0059 1
1,1,2-Trichloroethane ND mg/kg 09/22/17 17:02 79-00-50.0059 1
Trichloroethene ND mg/kg 09/22/17 17:02 79-01-60.0059 1
Trichlorofluoromethane ND mg/kg 09/22/17 17:02 75-69-40.0059 1
1,2,3-Trichloropropane ND mg/kg 09/22/17 17:02 96-18-40.0059 1
1,2,4-Trimethylbenzene ND mg/kg 09/22/17 17:02 95-63-60.0059 1
1,3,5-Trimethylbenzene ND mg/kg 09/22/17 17:02 108-67-80.0059 1
Vinyl acetate ND mg/kg 09/22/17 17:02 108-05-40.059 1
Vinyl chloride ND mg/kg 09/22/17 17:02 75-01-40.012 1
Xylene (Total)ND mg/kg 09/22/17 17:02 1330-20-70.012 1
m&p-Xylene ND mg/kg 09/22/17 17:02 179601-23-10.012 1
o-Xylene ND mg/kg 09/22/17 17:02 95-47-60.0059 1
Surrogates
Toluene-d8 (S)101 %09/22/17 17:02 2037-26-570-130 1
4-Bromofluorobenzene (S)97 %09/22/17 17:02 460-00-470-130 1
1,2-Dichloroethane-d4 (S)103 %09/22/17 17:02 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 22.0 %09/21/17 11:130.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 98 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-8B Lab ID:92355949023 Collected:09/18/17 17:45 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/25/17 18:29 N209/23/17 08:3713.3 1
Aliphatic (C19-C36)ND mg/kg 09/25/17 18:29 N209/23/17 08:3713.3 1
Aromatic (C11-C22)ND mg/kg 09/25/17 18:29 N209/23/17 08:3713.3 1
Surrogates
Nonatriacontane (S)81 %09/25/17 18:29 7194-86-709/23/17 08:3740-140 1
o-Terphenyl (S)58 %09/25/17 18:29 84-15-109/23/17 08:3740-140 1
2-Fluorobiphenyl (S)38 %09/25/17 18:29 321-60-8 S009/23/17 08:3740-140 1
2-Bromonaphthalene (S)13 %09/25/17 18:29 580-13-2 S009/23/17 08:3740-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/26/17 01:17 N209/25/17 10:303.5 1
Aliphatic (C09-C12)ND mg/kg 09/26/17 01:17 N209/25/17 10:303.5 1
Aromatic (C09-C10)ND mg/kg 09/26/17 01:17 N209/25/17 10:303.5 1
Surrogates
4-Bromofluorobenzene (FID) (S)99 %09/26/17 01:17 460-00-409/25/17 10:3070-130 1
4-Bromofluorobenzene (PID) (S)124 %09/26/17 01:17 460-00-409/25/17 10:3070-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/25/17 15:26 83-32-909/22/17 16:300.44 1
Acenaphthylene ND mg/kg 09/25/17 15:26 208-96-809/22/17 16:300.44 1
Aniline ND mg/kg 09/25/17 15:26 62-53-309/22/17 16:300.44 1
Anthracene ND mg/kg 09/25/17 15:26 120-12-709/22/17 16:300.44 1
Benzo(a)anthracene ND mg/kg 09/25/17 15:26 56-55-309/22/17 16:300.44 1
Benzo(a)pyrene ND mg/kg 09/25/17 15:26 50-32-809/22/17 16:300.44 1
Benzo(b)fluoranthene ND mg/kg 09/25/17 15:26 205-99-209/22/17 16:300.44 1
Benzo(g,h,i)perylene ND mg/kg 09/25/17 15:26 191-24-209/22/17 16:300.44 1
Benzo(k)fluoranthene ND mg/kg 09/25/17 15:26 207-08-909/22/17 16:300.44 1
Benzoic Acid ND mg/kg 09/25/17 15:26 65-85-009/22/17 16:302.2 1
Benzyl alcohol ND mg/kg 09/25/17 15:26 100-51-609/22/17 16:300.88 1
4-Bromophenylphenyl ether ND mg/kg 09/25/17 15:26 101-55-309/22/17 16:300.44 1
Butylbenzylphthalate ND mg/kg 09/25/17 15:26 85-68-709/22/17 16:300.44 1
4-Chloro-3-methylphenol ND mg/kg 09/25/17 15:26 59-50-709/22/17 16:300.88 1
4-Chloroaniline ND mg/kg 09/25/17 15:26 106-47-809/22/17 16:302.2 1
bis(2-Chloroethoxy)methane ND mg/kg 09/25/17 15:26 111-91-109/22/17 16:300.44 1
bis(2-Chloroethyl) ether ND mg/kg 09/25/17 15:26 111-44-409/22/17 16:300.44 1
2-Chloronaphthalene ND mg/kg 09/25/17 15:26 91-58-709/22/17 16:300.44 1
2-Chlorophenol ND mg/kg 09/25/17 15:26 95-57-809/22/17 16:300.44 1
4-Chlorophenylphenyl ether ND mg/kg 09/25/17 15:26 7005-72-309/22/17 16:300.44 1
Chrysene ND mg/kg 09/25/17 15:26 218-01-909/22/17 16:300.44 1
Dibenz(a,h)anthracene ND mg/kg 09/25/17 15:26 53-70-309/22/17 16:300.44 1
Dibenzofuran ND mg/kg 09/25/17 15:26 132-64-909/22/17 16:300.44 1
1,2-Dichlorobenzene ND mg/kg 09/25/17 15:26 95-50-109/22/17 16:300.44 1
1,3-Dichlorobenzene ND mg/kg 09/25/17 15:26 541-73-109/22/17 16:300.44 1
1,4-Dichlorobenzene ND mg/kg 09/25/17 15:26 106-46-709/22/17 16:300.44 1
3,3'-Dichlorobenzidine ND mg/kg 09/25/17 15:26 91-94-109/22/17 16:302.2 1
2,4-Dichlorophenol ND mg/kg 09/25/17 15:26 120-83-209/22/17 16:300.44 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 99 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-8B Lab ID:92355949023 Collected:09/18/17 17:45 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/25/17 15:26 84-66-209/22/17 16:300.44 1
2,4-Dimethylphenol ND mg/kg 09/25/17 15:26 105-67-909/22/17 16:300.44 1
Dimethylphthalate ND mg/kg 09/25/17 15:26 131-11-309/22/17 16:300.44 1
Di-n-butylphthalate ND mg/kg 09/25/17 15:26 84-74-209/22/17 16:300.44 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/25/17 15:26 534-52-109/22/17 16:300.88 1
2,4-Dinitrophenol ND mg/kg 09/25/17 15:26 51-28-509/22/17 16:302.2 1
2,4-Dinitrotoluene ND mg/kg 09/25/17 15:26 121-14-209/22/17 16:300.44 1
2,6-Dinitrotoluene ND mg/kg 09/25/17 15:26 606-20-209/22/17 16:300.44 1
Di-n-octylphthalate ND mg/kg 09/25/17 15:26 117-84-009/22/17 16:300.44 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/25/17 15:26 117-81-709/22/17 16:300.44 1
Fluoranthene ND mg/kg 09/25/17 15:26 206-44-009/22/17 16:300.44 1
Fluorene ND mg/kg 09/25/17 15:26 86-73-709/22/17 16:300.44 1
Hexachloro-1,3-butadiene ND mg/kg 09/25/17 15:26 87-68-309/22/17 16:300.44 1
Hexachlorobenzene ND mg/kg 09/25/17 15:26 118-74-109/22/17 16:300.44 1
Hexachlorocyclopentadiene ND mg/kg 09/25/17 15:26 77-47-409/22/17 16:300.44 1
Hexachloroethane ND mg/kg 09/25/17 15:26 67-72-109/22/17 16:300.44 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/25/17 15:26 193-39-509/22/17 16:300.44 1
Isophorone ND mg/kg 09/25/17 15:26 78-59-109/22/17 16:300.44 1
1-Methylnaphthalene ND mg/kg 09/25/17 15:26 90-12-009/22/17 16:300.44 1
2-Methylnaphthalene ND mg/kg 09/25/17 15:26 91-57-609/22/17 16:300.44 1
2-Methylphenol(o-Cresol)ND mg/kg 09/25/17 15:26 95-48-709/22/17 16:300.44 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/25/17 15:26 15831-10-4 L109/22/17 16:300.44 1
Naphthalene ND mg/kg 09/25/17 15:26 91-20-309/22/17 16:300.44 1
2-Nitroaniline ND mg/kg 09/25/17 15:26 88-74-409/22/17 16:302.2 1
3-Nitroaniline ND mg/kg 09/25/17 15:26 99-09-209/22/17 16:302.2 1
4-Nitroaniline ND mg/kg 09/25/17 15:26 100-01-609/22/17 16:300.88 1
Nitrobenzene ND mg/kg 09/25/17 15:26 98-95-309/22/17 16:300.44 1
2-Nitrophenol ND mg/kg 09/25/17 15:26 88-75-509/22/17 16:300.44 1
4-Nitrophenol ND mg/kg 09/25/17 15:26 100-02-709/22/17 16:302.2 1
N-Nitrosodimethylamine ND mg/kg 09/25/17 15:26 62-75-909/22/17 16:300.44 1
N-Nitroso-di-n-propylamine ND mg/kg 09/25/17 15:26 621-64-709/22/17 16:300.44 1
N-Nitrosodiphenylamine ND mg/kg 09/25/17 15:26 86-30-609/22/17 16:300.44 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/25/17 15:26 108-60-109/22/17 16:300.44 1
Pentachlorophenol ND mg/kg 09/25/17 15:26 87-86-509/22/17 16:302.2 1
Phenanthrene ND mg/kg 09/25/17 15:26 85-01-809/22/17 16:300.44 1
Phenol ND mg/kg 09/25/17 15:26 108-95-209/22/17 16:300.44 1
Pyrene ND mg/kg 09/25/17 15:26 129-00-009/22/17 16:300.44 1
1,2,4-Trichlorobenzene ND mg/kg 09/25/17 15:26 120-82-109/22/17 16:300.44 1
2,4,5-Trichlorophenol ND mg/kg 09/25/17 15:26 95-95-409/22/17 16:300.44 1
2,4,6-Trichlorophenol ND mg/kg 09/25/17 15:26 88-06-209/22/17 16:300.44 1
Surrogates
Nitrobenzene-d5 (S)17 %09/25/17 15:26 4165-60-0 S009/22/17 16:3023-110 1
2-Fluorobiphenyl (S)33 %09/25/17 15:26 321-60-809/22/17 16:3030-110 1
Terphenyl-d14 (S)70 %09/25/17 15:26 1718-51-009/22/17 16:3028-110 1
Phenol-d6 (S)31 %09/25/17 15:26 13127-88-309/22/17 16:3022-110 1
2-Fluorophenol (S)24 %09/25/17 15:26 367-12-409/22/17 16:3013-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 100 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-8B Lab ID:92355949023 Collected:09/18/17 17:45 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)76 %09/25/17 15:26 118-79-609/22/17 16:3027-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone 0.11 mg/kg 09/22/17 17:22 67-64-1 L10.10 1
Benzene ND mg/kg 09/22/17 17:22 71-43-20.0052 1
Bromobenzene ND mg/kg 09/22/17 17:22 108-86-10.0052 1
Bromochloromethane ND mg/kg 09/22/17 17:22 74-97-50.0052 1
Bromodichloromethane ND mg/kg 09/22/17 17:22 75-27-40.0052 1
Bromoform ND mg/kg 09/22/17 17:22 75-25-20.0052 1
Bromomethane ND mg/kg 09/22/17 17:22 74-83-90.010 1
2-Butanone (MEK)ND mg/kg 09/22/17 17:22 78-93-30.10 1
n-Butylbenzene ND mg/kg 09/22/17 17:22 104-51-80.0052 1
sec-Butylbenzene ND mg/kg 09/22/17 17:22 135-98-80.0052 1
tert-Butylbenzene ND mg/kg 09/22/17 17:22 98-06-60.0052 1
Carbon tetrachloride ND mg/kg 09/22/17 17:22 56-23-50.0052 1
Chlorobenzene ND mg/kg 09/22/17 17:22 108-90-70.0052 1
Chloroethane ND mg/kg 09/22/17 17:22 75-00-30.010 1
Chloroform ND mg/kg 09/22/17 17:22 67-66-30.0052 1
Chloromethane ND mg/kg 09/22/17 17:22 74-87-30.010 1
2-Chlorotoluene ND mg/kg 09/22/17 17:22 95-49-80.0052 1
4-Chlorotoluene ND mg/kg 09/22/17 17:22 106-43-40.0052 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/22/17 17:22 96-12-80.0052 1
Dibromochloromethane ND mg/kg 09/22/17 17:22 124-48-10.0052 1
1,2-Dibromoethane (EDB)ND mg/kg 09/22/17 17:22 106-93-40.0052 1
Dibromomethane ND mg/kg 09/22/17 17:22 74-95-30.0052 1
1,2-Dichlorobenzene ND mg/kg 09/22/17 17:22 95-50-10.0052 1
1,3-Dichlorobenzene ND mg/kg 09/22/17 17:22 541-73-10.0052 1
1,4-Dichlorobenzene ND mg/kg 09/22/17 17:22 106-46-70.0052 1
Dichlorodifluoromethane ND mg/kg 09/22/17 17:22 75-71-80.010 1
1,1-Dichloroethane ND mg/kg 09/22/17 17:22 75-34-30.0052 1
1,2-Dichloroethane ND mg/kg 09/22/17 17:22 107-06-20.0052 1
1,1-Dichloroethene ND mg/kg 09/22/17 17:22 75-35-40.0052 1
cis-1,2-Dichloroethene ND mg/kg 09/22/17 17:22 156-59-20.0052 1
trans-1,2-Dichloroethene ND mg/kg 09/22/17 17:22 156-60-50.0052 1
1,2-Dichloropropane ND mg/kg 09/22/17 17:22 78-87-50.0052 1
1,3-Dichloropropane ND mg/kg 09/22/17 17:22 142-28-90.0052 1
2,2-Dichloropropane ND mg/kg 09/22/17 17:22 594-20-70.0052 1
1,1-Dichloropropene ND mg/kg 09/22/17 17:22 563-58-60.0052 1
cis-1,3-Dichloropropene ND mg/kg 09/22/17 17:22 10061-01-50.0052 1
trans-1,3-Dichloropropene ND mg/kg 09/22/17 17:22 10061-02-60.0052 1
Diisopropyl ether ND mg/kg 09/22/17 17:22 108-20-30.0052 1
Ethylbenzene ND mg/kg 09/22/17 17:22 100-41-40.0052 1
Hexachloro-1,3-butadiene ND mg/kg 09/22/17 17:22 87-68-30.0052 1
2-Hexanone ND mg/kg 09/22/17 17:22 591-78-60.052 1
Isopropylbenzene (Cumene)ND mg/kg 09/22/17 17:22 98-82-80.0052 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 101 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-8B Lab ID:92355949023 Collected:09/18/17 17:45 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND mg/kg 09/22/17 17:22 99-87-60.0052 1
Methylene Chloride ND mg/kg 09/22/17 17:22 75-09-20.021 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/22/17 17:22 108-10-10.052 1
Methyl-tert-butyl ether ND mg/kg 09/22/17 17:22 1634-04-40.0052 1
Naphthalene ND mg/kg 09/22/17 17:22 91-20-30.0052 1
n-Propylbenzene ND mg/kg 09/22/17 17:22 103-65-10.0052 1
Styrene ND mg/kg 09/22/17 17:22 100-42-50.0052 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/22/17 17:22 630-20-60.0052 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/22/17 17:22 79-34-50.0052 1
Tetrachloroethene ND mg/kg 09/22/17 17:22 127-18-40.0052 1
Toluene ND mg/kg 09/22/17 17:22 108-88-30.0052 1
1,2,3-Trichlorobenzene ND mg/kg 09/22/17 17:22 87-61-60.0052 1
1,2,4-Trichlorobenzene ND mg/kg 09/22/17 17:22 120-82-10.0052 1
1,1,1-Trichloroethane ND mg/kg 09/22/17 17:22 71-55-60.0052 1
1,1,2-Trichloroethane ND mg/kg 09/22/17 17:22 79-00-50.0052 1
Trichloroethene ND mg/kg 09/22/17 17:22 79-01-60.0052 1
Trichlorofluoromethane ND mg/kg 09/22/17 17:22 75-69-40.0052 1
1,2,3-Trichloropropane ND mg/kg 09/22/17 17:22 96-18-40.0052 1
1,2,4-Trimethylbenzene ND mg/kg 09/22/17 17:22 95-63-60.0052 1
1,3,5-Trimethylbenzene ND mg/kg 09/22/17 17:22 108-67-80.0052 1
Vinyl acetate ND mg/kg 09/22/17 17:22 108-05-40.052 1
Vinyl chloride ND mg/kg 09/22/17 17:22 75-01-40.010 1
Xylene (Total)ND mg/kg 09/22/17 17:22 1330-20-70.010 1
m&p-Xylene ND mg/kg 09/22/17 17:22 179601-23-10.010 1
o-Xylene ND mg/kg 09/22/17 17:22 95-47-60.0052 1
Surrogates
Toluene-d8 (S)101 %09/22/17 17:22 2037-26-570-130 1
4-Bromofluorobenzene (S)99 %09/22/17 17:22 460-00-470-130 1
1,2-Dichloroethane-d4 (S)98 %09/22/17 17:22 17060-07-070-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 24.7 %09/21/17 11:130.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 102 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-8C Lab ID:92355949024 Collected:09/18/17 17:55 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: MADEP EPH Preparation Method: MADEP EPHMADEP EPH NC Soil
Aliphatic (C09-C18)ND mg/kg 09/25/17 18:56 N209/23/17 08:3712.5 1
Aliphatic (C19-C36)ND mg/kg 09/25/17 18:56 N209/23/17 08:3712.5 1
Aromatic (C11-C22)ND mg/kg 09/25/17 18:56 N209/23/17 08:3712.5 1
Surrogates
Nonatriacontane (S)62 %09/25/17 18:56 7194-86-709/23/17 08:3740-140 1
o-Terphenyl (S)62 %09/25/17 18:56 84-15-109/23/17 08:3740-140 1
2-Fluorobiphenyl (S)92 %09/25/17 18:56 321-60-809/23/17 08:3740-140 1
2-Bromonaphthalene (S)89 %09/25/17 18:56 580-13-209/23/17 08:3740-140 1
Analytical Method: MADEP VPH Preparation Method: MADEP VPHVPH NC Soil
Aliphatic (C05-C08)ND mg/kg 09/26/17 01:45 N209/25/17 10:303.5 1
Aliphatic (C09-C12)ND mg/kg 09/26/17 01:45 N209/25/17 10:303.5 1
Aromatic (C09-C10)ND mg/kg 09/26/17 01:45 N209/25/17 10:303.5 1
Surrogates
4-Bromofluorobenzene (FID) (S)100 %09/26/17 01:45 460-00-409/25/17 10:3070-130 1
4-Bromofluorobenzene (PID) (S)115 %09/26/17 01:45 460-00-409/25/17 10:3070-130 1
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Acenaphthene ND mg/kg 09/22/17 00:25 83-32-909/20/17 20:560.40 1
Acenaphthylene ND mg/kg 09/22/17 00:25 208-96-809/20/17 20:560.40 1
Aniline ND mg/kg 09/22/17 00:25 62-53-309/20/17 20:560.40 1
Anthracene ND mg/kg 09/22/17 00:25 120-12-709/20/17 20:560.40 1
Benzo(a)anthracene ND mg/kg 09/22/17 00:25 56-55-309/20/17 20:560.40 1
Benzo(a)pyrene ND mg/kg 09/22/17 00:25 50-32-809/20/17 20:560.40 1
Benzo(b)fluoranthene ND mg/kg 09/22/17 00:25 205-99-209/20/17 20:560.40 1
Benzo(g,h,i)perylene ND mg/kg 09/22/17 00:25 191-24-209/20/17 20:560.40 1
Benzo(k)fluoranthene ND mg/kg 09/22/17 00:25 207-08-909/20/17 20:560.40 1
Benzoic Acid ND mg/kg 09/22/17 00:25 65-85-009/20/17 20:562.0 1
Benzyl alcohol ND mg/kg 09/22/17 00:25 100-51-609/20/17 20:560.80 1
4-Bromophenylphenyl ether ND mg/kg 09/22/17 00:25 101-55-309/20/17 20:560.40 1
Butylbenzylphthalate ND mg/kg 09/22/17 00:25 85-68-709/20/17 20:560.40 1
4-Chloro-3-methylphenol ND mg/kg 09/22/17 00:25 59-50-709/20/17 20:560.80 1
4-Chloroaniline ND mg/kg 09/22/17 00:25 106-47-809/20/17 20:562.0 1
bis(2-Chloroethoxy)methane ND mg/kg 09/22/17 00:25 111-91-109/20/17 20:560.40 1
bis(2-Chloroethyl) ether ND mg/kg 09/22/17 00:25 111-44-409/20/17 20:560.40 1
2-Chloronaphthalene ND mg/kg 09/22/17 00:25 91-58-709/20/17 20:560.40 1
2-Chlorophenol ND mg/kg 09/22/17 00:25 95-57-809/20/17 20:560.40 1
4-Chlorophenylphenyl ether ND mg/kg 09/22/17 00:25 7005-72-309/20/17 20:560.40 1
Chrysene ND mg/kg 09/22/17 00:25 218-01-909/20/17 20:560.40 1
Dibenz(a,h)anthracene ND mg/kg 09/22/17 00:25 53-70-309/20/17 20:560.40 1
Dibenzofuran ND mg/kg 09/22/17 00:25 132-64-909/20/17 20:560.40 1
1,2-Dichlorobenzene ND mg/kg 09/22/17 00:25 95-50-109/20/17 20:560.40 1
1,3-Dichlorobenzene ND mg/kg 09/22/17 00:25 541-73-1 L209/20/17 20:560.40 1
1,4-Dichlorobenzene ND mg/kg 09/22/17 00:25 106-46-709/20/17 20:560.40 1
3,3'-Dichlorobenzidine ND mg/kg 09/22/17 00:25 91-94-109/20/17 20:562.0 1
2,4-Dichlorophenol ND mg/kg 09/22/17 00:25 120-83-209/20/17 20:560.40 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 103 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-8C Lab ID:92355949024 Collected:09/18/17 17:55 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Diethylphthalate ND mg/kg 09/22/17 00:25 84-66-209/20/17 20:560.40 1
2,4-Dimethylphenol ND mg/kg 09/22/17 00:25 105-67-909/20/17 20:560.40 1
Dimethylphthalate ND mg/kg 09/22/17 00:25 131-11-309/20/17 20:560.40 1
Di-n-butylphthalate ND mg/kg 09/22/17 00:25 84-74-209/20/17 20:560.40 1
4,6-Dinitro-2-methylphenol ND mg/kg 09/22/17 00:25 534-52-109/20/17 20:560.80 1
2,4-Dinitrophenol ND mg/kg 09/22/17 00:25 51-28-509/20/17 20:562.0 1
2,4-Dinitrotoluene ND mg/kg 09/22/17 00:25 121-14-209/20/17 20:560.40 1
2,6-Dinitrotoluene ND mg/kg 09/22/17 00:25 606-20-209/20/17 20:560.40 1
Di-n-octylphthalate ND mg/kg 09/22/17 00:25 117-84-009/20/17 20:560.40 1
bis(2-Ethylhexyl)phthalate ND mg/kg 09/22/17 00:25 117-81-709/20/17 20:560.40 1
Fluoranthene ND mg/kg 09/22/17 00:25 206-44-009/20/17 20:560.40 1
Fluorene ND mg/kg 09/22/17 00:25 86-73-709/20/17 20:560.40 1
Hexachloro-1,3-butadiene ND mg/kg 09/22/17 00:25 87-68-309/20/17 20:560.40 1
Hexachlorobenzene ND mg/kg 09/22/17 00:25 118-74-109/20/17 20:560.40 1
Hexachlorocyclopentadiene ND mg/kg 09/22/17 00:25 77-47-409/20/17 20:560.40 1
Hexachloroethane ND mg/kg 09/22/17 00:25 67-72-109/20/17 20:560.40 1
Indeno(1,2,3-cd)pyrene ND mg/kg 09/22/17 00:25 193-39-509/20/17 20:560.40 1
Isophorone ND mg/kg 09/22/17 00:25 78-59-109/20/17 20:560.40 1
1-Methylnaphthalene ND mg/kg 09/22/17 00:25 90-12-009/20/17 20:560.40 1
2-Methylnaphthalene ND mg/kg 09/22/17 00:25 91-57-609/20/17 20:560.40 1
2-Methylphenol(o-Cresol)ND mg/kg 09/22/17 00:25 95-48-709/20/17 20:560.40 1
3&4-Methylphenol(m&p Cresol)ND mg/kg 09/22/17 00:25 15831-10-409/20/17 20:560.40 1
Naphthalene ND mg/kg 09/22/17 00:25 91-20-309/20/17 20:560.40 1
2-Nitroaniline ND mg/kg 09/22/17 00:25 88-74-409/20/17 20:562.0 1
3-Nitroaniline ND mg/kg 09/22/17 00:25 99-09-209/20/17 20:562.0 1
4-Nitroaniline ND mg/kg 09/22/17 00:25 100-01-609/20/17 20:560.80 1
Nitrobenzene ND mg/kg 09/22/17 00:25 98-95-309/20/17 20:560.40 1
2-Nitrophenol ND mg/kg 09/22/17 00:25 88-75-509/20/17 20:560.40 1
4-Nitrophenol ND mg/kg 09/22/17 00:25 100-02-709/20/17 20:562.0 1
N-Nitrosodimethylamine ND mg/kg 09/22/17 00:25 62-75-909/20/17 20:560.40 1
N-Nitroso-di-n-propylamine ND mg/kg 09/22/17 00:25 621-64-709/20/17 20:560.40 1
N-Nitrosodiphenylamine ND mg/kg 09/22/17 00:25 86-30-609/20/17 20:560.40 1
2,2'-Oxybis(1-chloropropane)ND mg/kg 09/22/17 00:25 108-60-109/20/17 20:560.40 1
Pentachlorophenol ND mg/kg 09/22/17 00:25 87-86-509/20/17 20:562.0 1
Phenanthrene ND mg/kg 09/22/17 00:25 85-01-809/20/17 20:560.40 1
Phenol ND mg/kg 09/22/17 00:25 108-95-209/20/17 20:560.40 1
Pyrene ND mg/kg 09/22/17 00:25 129-00-009/20/17 20:560.40 1
1,2,4-Trichlorobenzene ND mg/kg 09/22/17 00:25 120-82-109/20/17 20:560.40 1
2,4,5-Trichlorophenol ND mg/kg 09/22/17 00:25 95-95-409/20/17 20:560.40 1
2,4,6-Trichlorophenol ND mg/kg 09/22/17 00:25 88-06-209/20/17 20:560.40 1
Surrogates
Nitrobenzene-d5 (S)28 %09/22/17 00:25 4165-60-009/20/17 20:5623-110 1
2-Fluorobiphenyl (S)26 %09/22/17 00:25 321-60-8 S009/20/17 20:5630-110 1
Terphenyl-d14 (S)44 %09/22/17 00:25 1718-51-009/20/17 20:5628-110 1
Phenol-d6 (S)26 %09/22/17 00:25 13127-88-309/20/17 20:5622-110 1
2-Fluorophenol (S)26 %09/22/17 00:25 367-12-409/20/17 20:5613-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 104 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-8C Lab ID:92355949024 Collected:09/18/17 17:55 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8270 Preparation Method: EPA 35468270 MSSV Microwave
Surrogates
2,4,6-Tribromophenol (S)45 %09/22/17 00:25 118-79-609/20/17 20:5627-110 1
Analytical Method: EPA 82608260/5035A Volatile Organics
Acetone ND mg/kg 09/22/17 17:42 67-64-1 L10.15 1
Benzene ND mg/kg 09/22/17 17:42 71-43-20.0075 1
Bromobenzene ND mg/kg 09/22/17 17:42 108-86-10.0075 1
Bromochloromethane ND mg/kg 09/22/17 17:42 74-97-50.0075 1
Bromodichloromethane ND mg/kg 09/22/17 17:42 75-27-40.0075 1
Bromoform ND mg/kg 09/22/17 17:42 75-25-20.0075 1
Bromomethane ND mg/kg 09/22/17 17:42 74-83-90.015 1
2-Butanone (MEK)ND mg/kg 09/22/17 17:42 78-93-30.15 1
n-Butylbenzene ND mg/kg 09/22/17 17:42 104-51-80.0075 1
sec-Butylbenzene ND mg/kg 09/22/17 17:42 135-98-80.0075 1
tert-Butylbenzene ND mg/kg 09/22/17 17:42 98-06-60.0075 1
Carbon tetrachloride ND mg/kg 09/22/17 17:42 56-23-50.0075 1
Chlorobenzene ND mg/kg 09/22/17 17:42 108-90-70.0075 1
Chloroethane ND mg/kg 09/22/17 17:42 75-00-30.015 1
Chloroform ND mg/kg 09/22/17 17:42 67-66-30.0075 1
Chloromethane ND mg/kg 09/22/17 17:42 74-87-30.015 1
2-Chlorotoluene ND mg/kg 09/22/17 17:42 95-49-80.0075 1
4-Chlorotoluene ND mg/kg 09/22/17 17:42 106-43-40.0075 1
1,2-Dibromo-3-chloropropane ND mg/kg 09/22/17 17:42 96-12-80.0075 1
Dibromochloromethane ND mg/kg 09/22/17 17:42 124-48-10.0075 1
1,2-Dibromoethane (EDB)ND mg/kg 09/22/17 17:42 106-93-40.0075 1
Dibromomethane ND mg/kg 09/22/17 17:42 74-95-30.0075 1
1,2-Dichlorobenzene ND mg/kg 09/22/17 17:42 95-50-10.0075 1
1,3-Dichlorobenzene ND mg/kg 09/22/17 17:42 541-73-10.0075 1
1,4-Dichlorobenzene ND mg/kg 09/22/17 17:42 106-46-70.0075 1
Dichlorodifluoromethane ND mg/kg 09/22/17 17:42 75-71-80.015 1
1,1-Dichloroethane ND mg/kg 09/22/17 17:42 75-34-30.0075 1
1,2-Dichloroethane ND mg/kg 09/22/17 17:42 107-06-20.0075 1
1,1-Dichloroethene ND mg/kg 09/22/17 17:42 75-35-40.0075 1
cis-1,2-Dichloroethene ND mg/kg 09/22/17 17:42 156-59-20.0075 1
trans-1,2-Dichloroethene ND mg/kg 09/22/17 17:42 156-60-50.0075 1
1,2-Dichloropropane ND mg/kg 09/22/17 17:42 78-87-50.0075 1
1,3-Dichloropropane ND mg/kg 09/22/17 17:42 142-28-90.0075 1
2,2-Dichloropropane ND mg/kg 09/22/17 17:42 594-20-70.0075 1
1,1-Dichloropropene ND mg/kg 09/22/17 17:42 563-58-60.0075 1
cis-1,3-Dichloropropene ND mg/kg 09/22/17 17:42 10061-01-50.0075 1
trans-1,3-Dichloropropene ND mg/kg 09/22/17 17:42 10061-02-60.0075 1
Diisopropyl ether ND mg/kg 09/22/17 17:42 108-20-30.0075 1
Ethylbenzene ND mg/kg 09/22/17 17:42 100-41-40.0075 1
Hexachloro-1,3-butadiene ND mg/kg 09/22/17 17:42 87-68-30.0075 1
2-Hexanone ND mg/kg 09/22/17 17:42 591-78-60.075 1
Isopropylbenzene (Cumene)ND mg/kg 09/22/17 17:42 98-82-80.0075 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 105 of 165
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92355949
Blvd B.P.
Sample:SB-8C Lab ID:92355949024 Collected:09/18/17 17:55 Received:09/19/17 13:30 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 82608260/5035A Volatile Organics
p-Isopropyltoluene ND mg/kg 09/22/17 17:42 99-87-60.0075 1
Methylene Chloride ND mg/kg 09/22/17 17:42 75-09-20.030 1
4-Methyl-2-pentanone (MIBK)ND mg/kg 09/22/17 17:42 108-10-10.075 1
Methyl-tert-butyl ether ND mg/kg 09/22/17 17:42 1634-04-40.0075 1
Naphthalene ND mg/kg 09/22/17 17:42 91-20-30.0075 1
n-Propylbenzene ND mg/kg 09/22/17 17:42 103-65-10.0075 1
Styrene ND mg/kg 09/22/17 17:42 100-42-50.0075 1
1,1,1,2-Tetrachloroethane ND mg/kg 09/22/17 17:42 630-20-60.0075 1
1,1,2,2-Tetrachloroethane ND mg/kg 09/22/17 17:42 79-34-50.0075 1
Tetrachloroethene ND mg/kg 09/22/17 17:42 127-18-40.0075 1
Toluene ND mg/kg 09/22/17 17:42 108-88-30.0075 1
1,2,3-Trichlorobenzene ND mg/kg 09/22/17 17:42 87-61-60.0075 1
1,2,4-Trichlorobenzene ND mg/kg 09/22/17 17:42 120-82-10.0075 1
1,1,1-Trichloroethane ND mg/kg 09/22/17 17:42 71-55-60.0075 1
1,1,2-Trichloroethane ND mg/kg 09/22/17 17:42 79-00-50.0075 1
Trichloroethene ND mg/kg 09/22/17 17:42 79-01-60.0075 1
Trichlorofluoromethane ND mg/kg 09/22/17 17:42 75-69-40.0075 1
1,2,3-Trichloropropane ND mg/kg 09/22/17 17:42 96-18-40.0075 1
1,2,4-Trimethylbenzene ND mg/kg 09/22/17 17:42 95-63-60.0075 1
1,3,5-Trimethylbenzene ND mg/kg 09/22/17 17:42 108-67-80.0075 1
Vinyl acetate ND mg/kg 09/22/17 17:42 108-05-40.075 1
Vinyl chloride ND mg/kg 09/22/17 17:42 75-01-40.015 1
Xylene (Total)ND mg/kg 09/22/17 17:42 1330-20-70.015 1
m&p-Xylene ND mg/kg 09/22/17 17:42 179601-23-10.015 1
o-Xylene ND mg/kg 09/22/17 17:42 95-47-60.0075 1
Surrogates
Toluene-d8 (S)103 %09/22/17 17:42 2037-26-570-130 1
4-Bromofluorobenzene (S)107 %09/22/17 17:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)142 %09/22/17 17:42 17060-07-0 S370-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 19.2 %09/21/17 11:130.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 106 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
378723
MADEP VPH
MADEP VPH
VPH NC Soil
Associated Lab Samples:92355949001, 92355949002, 92355949003, 92355949004, 92355949005, 92355949006, 92355949007,
92355949008, 92355949009, 92355949010, 92355949011, 92355949012, 92355949013, 92355949014,
92355949015, 92355949016, 92355949017, 92355949018, 92355949019, 92355949020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2098566
Associated Lab Samples:92355949001, 92355949002, 92355949003, 92355949004, 92355949005, 92355949006, 92355949007,
92355949008, 92355949009, 92355949010, 92355949011, 92355949012, 92355949013, 92355949014,
92355949015, 92355949016, 92355949017, 92355949018, 92355949019, 92355949020
Matrix:Solid
Analyzed
Aliphatic (C05-C08)mg/kg ND 2.5 N209/21/17 15:10
Aliphatic (C09-C12)mg/kg ND 2.5 N209/21/17 15:10
Aromatic (C09-C10)mg/kg ND 2.5 N209/21/17 15:10
4-Bromofluorobenzene (FID) (S)%104 70-130 09/21/17 15:10
4-Bromofluorobenzene (PID) (S)%98 70-130 09/21/17 15:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2098567LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2098568
Aliphatic (C05-C08)mg/kg 13.4 N2158970-1308913.4 0 25
Aliphatic (C09-C12)mg/kg 14.1 N2159430-1309514.3 1 25
Aromatic (C09-C10)mg/kg 4.0 N258070-130814.1 2 25
4-Bromofluorobenzene (FID) (S)%105 70-130101
4-Bromofluorobenzene (PID) (S)%100 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 107 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
379187
MADEP VPH
MADEP VPH
VPH NC Soil
Associated Lab Samples:92355949021, 92355949022, 92355949023, 92355949024
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2101275
Associated Lab Samples:92355949021, 92355949022, 92355949023, 92355949024
Matrix:Solid
Analyzed
Aliphatic (C05-C08)mg/kg ND 2.5 N209/25/17 15:33
Aliphatic (C09-C12)mg/kg ND 2.5 N209/25/17 15:33
Aromatic (C09-C10)mg/kg ND 2.5 N209/25/17 15:33
4-Bromofluorobenzene (FID) (S)%94 70-130 09/25/17 15:33
4-Bromofluorobenzene (PID) (S)%91 70-130 09/25/17 15:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2101276LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2101277
Aliphatic (C05-C08)mg/kg 13.0 N2158770-1308612.9 1 25
Aliphatic (C09-C12)mg/kg 13.5 N2159030-1309314.0 4 25
Aromatic (C09-C10)mg/kg 3.6 N257270-130763.8 5 25
4-Bromofluorobenzene (FID) (S)%100 70-13098
4-Bromofluorobenzene (PID) (S)%97 70-13094
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 108 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
378755
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92355949001, 92355949002, 92355949003, 92355949004, 92355949005, 92355949006, 92355949007,
92355949008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2098706
Associated Lab Samples:92355949001, 92355949002, 92355949003, 92355949004, 92355949005, 92355949006, 92355949007,
92355949008
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane mg/kg ND 0.0054 09/21/17 12:41
1,1,1-Trichloroethane mg/kg ND 0.0054 09/21/17 12:41
1,1,2,2-Tetrachloroethane mg/kg ND 0.0054 09/21/17 12:41
1,1,2-Trichloroethane mg/kg ND 0.0054 09/21/17 12:41
1,1-Dichloroethane mg/kg ND 0.0054 09/21/17 12:41
1,1-Dichloroethene mg/kg ND 0.0054 09/21/17 12:41
1,1-Dichloropropene mg/kg ND 0.0054 09/21/17 12:41
1,2,3-Trichlorobenzene mg/kg ND 0.0054 09/21/17 12:41
1,2,3-Trichloropropane mg/kg ND 0.0054 09/21/17 12:41
1,2,4-Trichlorobenzene mg/kg ND 0.0054 09/21/17 12:41
1,2,4-Trimethylbenzene mg/kg ND 0.0054 09/21/17 12:41
1,2-Dibromo-3-chloropropane mg/kg ND 0.0054 09/21/17 12:41
1,2-Dibromoethane (EDB)mg/kg ND 0.0054 09/21/17 12:41
1,2-Dichlorobenzene mg/kg ND 0.0054 09/21/17 12:41
1,2-Dichloroethane mg/kg ND 0.0054 09/21/17 12:41
1,2-Dichloropropane mg/kg ND 0.0054 09/21/17 12:41
1,3,5-Trimethylbenzene mg/kg ND 0.0054 09/21/17 12:41
1,3-Dichlorobenzene mg/kg ND 0.0054 09/21/17 12:41
1,3-Dichloropropane mg/kg ND 0.0054 09/21/17 12:41
1,4-Dichlorobenzene mg/kg ND 0.0054 09/21/17 12:41
2,2-Dichloropropane mg/kg ND 0.0054 09/21/17 12:41
2-Butanone (MEK)mg/kg ND 0.11 09/21/17 12:41
2-Chlorotoluene mg/kg ND 0.0054 09/21/17 12:41
2-Hexanone mg/kg ND 0.054 09/21/17 12:41
4-Chlorotoluene mg/kg ND 0.0054 09/21/17 12:41
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.054 09/21/17 12:41
Acetone mg/kg ND 0.11 09/21/17 12:41
Benzene mg/kg ND 0.0054 09/21/17 12:41
Bromobenzene mg/kg ND 0.0054 09/21/17 12:41
Bromochloromethane mg/kg ND 0.0054 09/21/17 12:41
Bromodichloromethane mg/kg ND 0.0054 09/21/17 12:41
Bromoform mg/kg ND 0.0054 09/21/17 12:41
Bromomethane mg/kg ND 0.011 09/21/17 12:41
Carbon tetrachloride mg/kg ND 0.0054 09/21/17 12:41
Chlorobenzene mg/kg ND 0.0054 09/21/17 12:41
Chloroethane mg/kg ND 0.011 09/21/17 12:41
Chloroform mg/kg ND 0.0054 09/21/17 12:41
Chloromethane mg/kg ND 0.011 09/21/17 12:41
cis-1,2-Dichloroethene mg/kg ND 0.0054 09/21/17 12:41
cis-1,3-Dichloropropene mg/kg ND 0.0054 09/21/17 12:41
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 109 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2098706
Associated Lab Samples:92355949001, 92355949002, 92355949003, 92355949004, 92355949005, 92355949006, 92355949007,
92355949008
Matrix:Solid
Analyzed
Dibromochloromethane mg/kg ND 0.0054 09/21/17 12:41
Dibromomethane mg/kg ND 0.0054 09/21/17 12:41
Dichlorodifluoromethane mg/kg ND 0.011 09/21/17 12:41
Diisopropyl ether mg/kg ND 0.0054 09/21/17 12:41
Ethylbenzene mg/kg ND 0.0054 09/21/17 12:41
Hexachloro-1,3-butadiene mg/kg ND 0.0054 09/21/17 12:41
Isopropylbenzene (Cumene)mg/kg ND 0.0054 09/21/17 12:41
m&p-Xylene mg/kg ND 0.011 09/21/17 12:41
Methyl-tert-butyl ether mg/kg ND 0.0054 09/21/17 12:41
Methylene Chloride mg/kg ND 0.021 09/21/17 12:41
n-Butylbenzene mg/kg ND 0.0054 09/21/17 12:41
n-Propylbenzene mg/kg ND 0.0054 09/21/17 12:41
Naphthalene mg/kg ND 0.0054 09/21/17 12:41
o-Xylene mg/kg ND 0.0054 09/21/17 12:41
p-Isopropyltoluene mg/kg ND 0.0054 09/21/17 12:41
sec-Butylbenzene mg/kg ND 0.0054 09/21/17 12:41
Styrene mg/kg ND 0.0054 09/21/17 12:41
tert-Butylbenzene mg/kg ND 0.0054 09/21/17 12:41
Tetrachloroethene mg/kg ND 0.0054 09/21/17 12:41
Toluene mg/kg ND 0.0054 09/21/17 12:41
trans-1,2-Dichloroethene mg/kg ND 0.0054 09/21/17 12:41
trans-1,3-Dichloropropene mg/kg ND 0.0054 09/21/17 12:41
Trichloroethene mg/kg ND 0.0054 09/21/17 12:41
Trichlorofluoromethane mg/kg ND 0.0054 09/21/17 12:41
Vinyl acetate mg/kg ND 0.054 09/21/17 12:41
Vinyl chloride mg/kg ND 0.011 09/21/17 12:41
Xylene (Total)mg/kg ND 0.011 09/21/17 12:41
1,2-Dichloroethane-d4 (S)%102 70-132 09/21/17 12:41
4-Bromofluorobenzene (S)%97 70-130 09/21/17 12:41
Toluene-d8 (S)%96 70-130 09/21/17 12:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2098707LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.062.06 103 74-137
1,1,1-Trichloroethane mg/kg 0.056.06 94 67-140
1,1,2,2-Tetrachloroethane mg/kg 0.061.06 102 72-141
1,1,2-Trichloroethane mg/kg 0.059.06 99 78-138
1,1-Dichloroethane mg/kg 0.053.06 88 69-134
1,1-Dichloroethene mg/kg 0.053.06 89 67-138
1,1-Dichloropropene mg/kg 0.057.06 96 69-139
1,2,3-Trichlorobenzene mg/kg 0.075.06 126 70-146
1,2,3-Trichloropropane mg/kg 0.065.06 109 69-144
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
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Page 110 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2098707LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 0.076.06 127 68-148
1,2,4-Trimethylbenzene mg/kg 0.070.06 117 74-137
1,2-Dibromo-3-chloropropane mg/kg 0.076.06 127 65-140
1,2-Dibromoethane (EDB)mg/kg 0.064.06 107 77-135
1,2-Dichlorobenzene mg/kg 0.067.06 112 77-141
1,2-Dichloroethane mg/kg 0.055.06 93 65-137
1,2-Dichloropropane mg/kg 0.059.06 99 72-136
1,3,5-Trimethylbenzene mg/kg 0.069.06 115 76-133
1,3-Dichlorobenzene mg/kg 0.067.06 111 74-138
1,3-Dichloropropane mg/kg 0.063.06 106 71-139
1,4-Dichlorobenzene mg/kg 0.067.06 112 76-138
2,2-Dichloropropane mg/kg 0.058.06 97 68-137
2-Butanone (MEK)mg/kg .1J.12 87 58-147
2-Chlorotoluene mg/kg 0.067.06 112 73-139
2-Hexanone mg/kg 0.13.12 111 62-145
4-Chlorotoluene mg/kg 0.068.06 114 76-141
4-Methyl-2-pentanone (MIBK)mg/kg 0.13.12 106 64-149
Acetone mg/kg .1J.12 87 53-153
Benzene mg/kg 0.059.06 98 73-135
Bromobenzene mg/kg 0.067.06 112 75-133
Bromochloromethane mg/kg 0.057.06 96 73-134
Bromodichloromethane mg/kg 0.059.06 99 71-135
Bromoform mg/kg 0.063.06 106 66-141
Bromomethane mg/kg 0.057.06 94 53-160
Carbon tetrachloride mg/kg 0.060.06 101 60-145
Chlorobenzene mg/kg 0.062.06 104 78-130
Chloroethane mg/kg 0.053.06 88 64-149
Chloroform mg/kg 0.056.06 94 70-134
Chloromethane mg/kg 0.052.06 86 52-150
cis-1,2-Dichloroethene mg/kg 0.057.06 95 70-133
cis-1,3-Dichloropropene mg/kg 0.063.06 105 68-134
Dibromochloromethane mg/kg 0.063.06 106 71-138
Dibromomethane mg/kg 0.061.06 102 74-130
Dichlorodifluoromethane mg/kg 0.048.06 81 40-160
Diisopropyl ether mg/kg 0.050.06 83 69-141
Ethylbenzene mg/kg 0.064.06 107 75-133
Hexachloro-1,3-butadiene mg/kg 0.070.06 117 68-143
Isopropylbenzene (Cumene)mg/kg 0.064.06 106 76-143
m&p-Xylene mg/kg 0.13.12 106 75-136
Methyl-tert-butyl ether mg/kg 0.054.06 91 68-144
Methylene Chloride mg/kg 0.046.06 77 45-154
n-Butylbenzene mg/kg 0.069.06 116 72-137
n-Propylbenzene mg/kg 0.066.06 111 76-136
Naphthalene mg/kg 0.082.06 136 68-151
o-Xylene mg/kg 0.063.06 106 76-141
p-Isopropyltoluene mg/kg 0.069.06 115 76-140
sec-Butylbenzene mg/kg 0.066.06 111 79-139
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 111 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2098707LABORATORY CONTROL SAMPLE:
LCSSpike
Styrene mg/kg 0.066.06 110 79-137
tert-Butylbenzene mg/kg 0.060.06 100 74-143
Tetrachloroethene mg/kg 0.053.06 89 71-138
Toluene mg/kg 0.061.06 102 74-131
trans-1,2-Dichloroethene mg/kg 0.053.06 89 67-135
trans-1,3-Dichloropropene mg/kg 0.063.06 105 65-146
Trichloroethene mg/kg 0.061.06 102 67-135
Trichlorofluoromethane mg/kg 0.054.06 90 59-144
Vinyl acetate mg/kg 0.11.12 90 40-160
Vinyl chloride mg/kg 0.052.06 87 56-141
Xylene (Total)mg/kg 0.19.18 106 76-137
1,2-Dichloroethane-d4 (S)%98 70-132
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2099718MATRIX SPIKE SAMPLE:
MSSpike
Result
92355949005
1,1,1,2-Tetrachloroethane mg/kg 0.025.028 90 70-130ND
1,1,1-Trichloroethane mg/kg 0.025.028 90 70-130ND
1,1,2,2-Tetrachloroethane mg/kg 0.025.028 90 70-130ND
1,1,2-Trichloroethane mg/kg 0.024.028 87 70-130ND
1,1-Dichloroethane mg/kg 0.022.028 80 70-130ND
1,1-Dichloroethene mg/kg 0.023.028 84 49-180ND
1,1-Dichloropropene mg/kg 0.025.028 89 70-130ND
1,2,3-Trichlorobenzene mg/kg 0.018.028 65 70-130ND
1,2,3-Trichloropropane mg/kg 0.024.028 88 70-130ND
1,2,4-Trichlorobenzene mg/kg 0.019.028 69 70-130ND
1,2,4-Trimethylbenzene mg/kg 0.027.028 41 70-1300.015
1,2-Dibromo-3-chloropropane mg/kg 0.024.028 86 70-130ND
1,2-Dibromoethane (EDB)mg/kg 0.026.028 95 70-130ND
1,2-Dichlorobenzene mg/kg 0.022.028 81 70-130ND
1,2-Dichloroethane mg/kg 0.023.028 85 70-130ND
1,2-Dichloropropane mg/kg 0.025.028 90 70-130ND
1,3,5-Trimethylbenzene mg/kg 0.026.028 78 70-130ND
1,3-Dichlorobenzene mg/kg 0.023.028 83 70-130ND
1,3-Dichloropropane mg/kg 0.026.028 93 70-130ND
1,4-Dichlorobenzene mg/kg 0.023.028 82 70-130ND
2,2-Dichloropropane mg/kg 0.025.028 90 70-130ND
2-Butanone (MEK)mg/kg .059J.055 85 70-130ND
2-Chlorotoluene mg/kg 0.025.028 90 70-130ND
2-Hexanone mg/kg .052J.055 94 70-130ND
4-Chlorotoluene mg/kg 0.025.028 91 70-130ND
4-Methyl-2-pentanone (MIBK)mg/kg .051J.055 93 70-130ND
Acetone mg/kg .11J.055 77 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
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Huntersville, NC 28078
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Page 112 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2099718MATRIX SPIKE SAMPLE:
MSSpike
Result
92355949005
Benzene mg/kg 0.025.028 91 50-166ND
Bromobenzene mg/kg 0.025.028 91 70-130ND
Bromochloromethane mg/kg 0.024.028 88 70-130ND
Bromodichloromethane mg/kg 0.025.028 91 70-130ND
Bromoform mg/kg 0.023.028 82 70-130ND
Bromomethane mg/kg 0.022.028 79 70-130ND
Carbon tetrachloride mg/kg 0.024.028 89 70-130ND
Chlorobenzene mg/kg 0.025.028 91 43-169ND
Chloroethane mg/kg 0.023.028 83 70-130ND
Chloroform mg/kg 0.025.028 92 70-130ND
Chloromethane mg/kg 0.022.028 80 70-130ND
cis-1,2-Dichloroethene mg/kg 0.025.028 89 70-130ND
cis-1,3-Dichloropropene mg/kg 0.024.028 89 70-130ND
Dibromochloromethane mg/kg 0.025.028 89 70-130ND
Dibromomethane mg/kg 0.024.028 87 70-130ND
Dichlorodifluoromethane mg/kg 0.023.028 82 70-130ND
Diisopropyl ether mg/kg 0.020.028 73 70-130ND
Ethylbenzene mg/kg 0.026.028 96 70-130ND
Hexachloro-1,3-butadiene mg/kg 0.019.028 69 70-130ND
Isopropylbenzene (Cumene)mg/kg 0.025.028 92 70-130ND
m&p-Xylene mg/kg 0.053.055 96 70-130ND
Methyl-tert-butyl ether mg/kg 0.025.028 66 70-1300.0066
Methylene Chloride mg/kg .022J.028 79 70-130ND
n-Butylbenzene mg/kg 0.024.028 88 70-130ND
n-Propylbenzene mg/kg 0.026.028 93 70-130ND
Naphthalene mg/kg 0.023.028 68 70-130ND
o-Xylene mg/kg 0.025.028 91 70-130ND
p-Isopropyltoluene mg/kg 0.025.028 90 70-130ND
sec-Butylbenzene mg/kg 0.025.028 92 70-130ND
Styrene mg/kg 0.024.028 85 70-130ND
tert-Butylbenzene mg/kg 0.023.028 82 70-130ND
Tetrachloroethene mg/kg 0.023.028 83 70-130ND
Toluene mg/kg 0.025.028 92 52-163ND
trans-1,2-Dichloroethene mg/kg 0.023.028 82 70-130ND
trans-1,3-Dichloropropene mg/kg 0.023.028 84 70-130ND
Trichloroethene mg/kg 0.025.028 91 49-167ND
Trichlorofluoromethane mg/kg 0.025.028 89 70-130ND
Vinyl acetate mg/kg .04J.055 72 70-130ND
Vinyl chloride mg/kg 0.023.028 82 70-130ND
1,2-Dichloroethane-d4 (S)%100 70-132
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%97 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 113 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92355877003
2099717SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg ND
1,1,1-Trichloroethane mg/kg ND
1,1,2,2-Tetrachloroethane mg/kg ND
1,1,2-Trichloroethane mg/kg ND
1,1-Dichloroethane mg/kg ND
1,1-Dichloroethene mg/kg ND
1,1-Dichloropropene mg/kg ND
1,2,3-Trichlorobenzene mg/kg ND
1,2,3-Trichloropropane mg/kg ND
1,2,4-Trichlorobenzene mg/kg ND
1,2,4-Trimethylbenzene mg/kg ND
1,2-Dibromo-3-chloropropane mg/kg ND
1,2-Dibromoethane (EDB)mg/kg ND
1,2-Dichlorobenzene mg/kg ND
1,2-Dichloroethane mg/kg ND
1,2-Dichloropropane mg/kg ND
1,3,5-Trimethylbenzene mg/kg ND
1,3-Dichlorobenzene mg/kg ND
1,3-Dichloropropane mg/kg ND
1,4-Dichlorobenzene mg/kg ND
2,2-Dichloropropane mg/kg ND
2-Butanone (MEK)mg/kg .0052J
2-Chlorotoluene mg/kg ND
2-Hexanone mg/kg ND
4-Chlorotoluene mg/kg ND
4-Methyl-2-pentanone (MIBK)mg/kg 0.075
Acetone mg/kg .023J
Benzene mg/kg NDND
Bromobenzene mg/kg ND
Bromochloromethane mg/kg ND
Bromodichloromethane mg/kg ND
Bromoform mg/kg ND
Bromomethane mg/kg ND
Carbon tetrachloride mg/kg ND
Chlorobenzene mg/kg ND
Chloroethane mg/kg ND
Chloroform mg/kg ND
Chloromethane mg/kg ND
cis-1,2-Dichloroethene mg/kg ND
cis-1,3-Dichloropropene mg/kg ND
Dibromochloromethane mg/kg ND
Dibromomethane mg/kg ND
Dichlorodifluoromethane mg/kg ND
Diisopropyl ether mg/kg ND
Ethylbenzene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg ND
Isopropylbenzene (Cumene)mg/kg ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 114 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92355877003
2099717SAMPLE DUPLICATE:
m&p-Xylene mg/kg ND
Methyl-tert-butyl ether mg/kg ND
Methylene Chloride mg/kg ND
n-Butylbenzene mg/kg ND
n-Propylbenzene mg/kg ND
Naphthalene mg/kg ND
o-Xylene mg/kg ND
p-Isopropyltoluene mg/kg ND
sec-Butylbenzene mg/kg ND
Styrene mg/kg ND
tert-Butylbenzene mg/kg ND
Tetrachloroethene mg/kg ND
Toluene mg/kg NDND
trans-1,2-Dichloroethene mg/kg ND
trans-1,3-Dichloropropene mg/kg ND
Trichloroethene mg/kg ND
Trichlorofluoromethane mg/kg ND
Vinyl acetate mg/kg ND
Vinyl chloride mg/kg ND
Xylene (Total)mg/kg NDND
1,2-Dichloroethane-d4 (S)%108 14103
4-Bromofluorobenzene (S)%101 9101
Toluene-d8 (S)%97 1097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 115 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
378788
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92355949009, 92355949010, 92355949011, 92355949012
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2098948
Associated Lab Samples:92355949009, 92355949010, 92355949011, 92355949012
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane mg/kg ND 0.0065 09/21/17 14:04
1,1,1-Trichloroethane mg/kg ND 0.0065 09/21/17 14:04
1,1,2,2-Tetrachloroethane mg/kg ND 0.0065 09/21/17 14:04
1,1,2-Trichloroethane mg/kg ND 0.0065 09/21/17 14:04
1,1-Dichloroethane mg/kg ND 0.0065 09/21/17 14:04
1,1-Dichloroethene mg/kg ND 0.0065 09/21/17 14:04
1,1-Dichloropropene mg/kg ND 0.0065 09/21/17 14:04
1,2,3-Trichlorobenzene mg/kg ND 0.0065 09/21/17 14:04
1,2,3-Trichloropropane mg/kg ND 0.0065 09/21/17 14:04
1,2,4-Trichlorobenzene mg/kg ND 0.0065 09/21/17 14:04
1,2,4-Trimethylbenzene mg/kg ND 0.0065 09/21/17 14:04
1,2-Dibromo-3-chloropropane mg/kg ND 0.0065 09/21/17 14:04
1,2-Dibromoethane (EDB)mg/kg ND 0.0065 09/21/17 14:04
1,2-Dichlorobenzene mg/kg ND 0.0065 09/21/17 14:04
1,2-Dichloroethane mg/kg ND 0.0065 09/21/17 14:04
1,2-Dichloropropane mg/kg ND 0.0065 09/21/17 14:04
1,3,5-Trimethylbenzene mg/kg ND 0.0065 09/21/17 14:04
1,3-Dichlorobenzene mg/kg ND 0.0065 09/21/17 14:04
1,3-Dichloropropane mg/kg ND 0.0065 09/21/17 14:04
1,4-Dichlorobenzene mg/kg ND 0.0065 09/21/17 14:04
2,2-Dichloropropane mg/kg ND 0.0065 09/21/17 14:04
2-Butanone (MEK)mg/kg ND 0.13 09/21/17 14:04
2-Chlorotoluene mg/kg ND 0.0065 09/21/17 14:04
2-Hexanone mg/kg ND 0.065 09/21/17 14:04
4-Chlorotoluene mg/kg ND 0.0065 09/21/17 14:04
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.065 09/21/17 14:04
Acetone mg/kg ND 0.13 09/21/17 14:04
Benzene mg/kg ND 0.0065 09/21/17 14:04
Bromobenzene mg/kg ND 0.0065 09/21/17 14:04
Bromochloromethane mg/kg ND 0.0065 09/21/17 14:04
Bromodichloromethane mg/kg ND 0.0065 09/21/17 14:04
Bromoform mg/kg ND 0.0065 09/21/17 14:04
Bromomethane mg/kg ND 0.013 09/21/17 14:04
Carbon tetrachloride mg/kg ND 0.0065 09/21/17 14:04
Chlorobenzene mg/kg ND 0.0065 09/21/17 14:04
Chloroethane mg/kg ND 0.013 09/21/17 14:04
Chloroform mg/kg ND 0.0065 09/21/17 14:04
Chloromethane mg/kg ND 0.013 09/21/17 14:04
cis-1,2-Dichloroethene mg/kg ND 0.0065 09/21/17 14:04
cis-1,3-Dichloropropene mg/kg ND 0.0065 09/21/17 14:04
Dibromochloromethane mg/kg ND 0.0065 09/21/17 14:04
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 116 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2098948
Associated Lab Samples:92355949009, 92355949010, 92355949011, 92355949012
Matrix:Solid
Analyzed
Dibromomethane mg/kg ND 0.0065 09/21/17 14:04
Dichlorodifluoromethane mg/kg ND 0.013 09/21/17 14:04
Diisopropyl ether mg/kg ND 0.0065 09/21/17 14:04
Ethylbenzene mg/kg ND 0.0065 09/21/17 14:04
Hexachloro-1,3-butadiene mg/kg ND 0.0065 09/21/17 14:04
Isopropylbenzene (Cumene)mg/kg ND 0.0065 09/21/17 14:04
m&p-Xylene mg/kg ND 0.013 09/21/17 14:04
Methyl-tert-butyl ether mg/kg ND 0.0065 09/21/17 14:04
Methylene Chloride mg/kg ND 0.026 09/21/17 14:04
n-Butylbenzene mg/kg ND 0.0065 09/21/17 14:04
n-Propylbenzene mg/kg ND 0.0065 09/21/17 14:04
Naphthalene mg/kg ND 0.0065 09/21/17 14:04
o-Xylene mg/kg ND 0.0065 09/21/17 14:04
p-Isopropyltoluene mg/kg ND 0.0065 09/21/17 14:04
sec-Butylbenzene mg/kg ND 0.0065 09/21/17 14:04
Styrene mg/kg ND 0.0065 09/21/17 14:04
tert-Butylbenzene mg/kg ND 0.0065 09/21/17 14:04
Tetrachloroethene mg/kg ND 0.0065 09/21/17 14:04
Toluene mg/kg ND 0.0065 09/21/17 14:04
trans-1,2-Dichloroethene mg/kg ND 0.0065 09/21/17 14:04
trans-1,3-Dichloropropene mg/kg ND 0.0065 09/21/17 14:04
Trichloroethene mg/kg ND 0.0065 09/21/17 14:04
Trichlorofluoromethane mg/kg ND 0.0065 09/21/17 14:04
Vinyl acetate mg/kg ND 0.065 09/21/17 14:04
Vinyl chloride mg/kg ND 0.013 09/21/17 14:04
Xylene (Total)mg/kg ND 0.013 09/21/17 14:04
1,2-Dichloroethane-d4 (S)%121 70-132 09/21/17 14:04
4-Bromofluorobenzene (S)%100 70-130 09/21/17 14:04
Toluene-d8 (S)%104 70-130 09/21/17 14:04
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2098949LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.062.061 102 74-137
1,1,1-Trichloroethane mg/kg 0.065.061 106 67-140
1,1,2,2-Tetrachloroethane mg/kg 0.056.061 92 72-141
1,1,2-Trichloroethane mg/kg 0.067.061 110 78-138
1,1-Dichloroethane mg/kg 0.065.061 106 69-134
1,1-Dichloroethene mg/kg 0.064.061 105 67-138
1,1-Dichloropropene mg/kg 0.063.061 104 69-139
1,2,3-Trichlorobenzene mg/kg 0.070.061 115 70-146
1,2,3-Trichloropropane mg/kg 0.066.061 109 69-144
1,2,4-Trichlorobenzene mg/kg 0.066.061 108 68-148
1,2,4-Trimethylbenzene mg/kg 0.064.061 105 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 117 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2098949LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane mg/kg 0.066.061 107 65-140
1,2-Dibromoethane (EDB)mg/kg 0.065.061 106 77-135
1,2-Dichlorobenzene mg/kg 0.065.061 106 77-141
1,2-Dichloroethane mg/kg 0.067.061 110 65-137
1,2-Dichloropropane mg/kg 0.068.061 111 72-136
1,3,5-Trimethylbenzene mg/kg 0.064.061 104 76-133
1,3-Dichlorobenzene mg/kg 0.063.061 104 74-138
1,3-Dichloropropane mg/kg 0.066.061 108 71-139
1,4-Dichlorobenzene mg/kg 0.064.061 104 76-138
2,2-Dichloropropane mg/kg 0.064.061 105 68-137
2-Butanone (MEK)mg/kg 0.14.12 111 58-147
2-Chlorotoluene mg/kg 0.063.061 103 73-139
2-Hexanone mg/kg 0.14.12 111 62-145
4-Chlorotoluene mg/kg 0.064.061 104 76-141
4-Methyl-2-pentanone (MIBK)mg/kg 0.14.12 112 64-149
Acetone mg/kg 0.19.12 152 53-153
Benzene mg/kg 0.065.061 106 73-135
Bromobenzene mg/kg 0.066.061 108 75-133
Bromochloromethane mg/kg 0.069.061 112 73-134
Bromodichloromethane mg/kg 0.066.061 108 71-135
Bromoform mg/kg 0.063.061 103 66-141
Bromomethane mg/kg 0.075.061 123 53-160
Carbon tetrachloride mg/kg 0.063.061 103 60-145
Chlorobenzene mg/kg 0.061.061 100 78-130
Chloroethane mg/kg 0.070.061 115 64-149
Chloroform mg/kg 0.067.061 109 70-134
Chloromethane mg/kg 0.075.061 122 52-150
cis-1,2-Dichloroethene mg/kg 0.067.061 109 70-133
cis-1,3-Dichloropropene mg/kg 0.070.061 115 68-134
Dibromochloromethane mg/kg 0.065.061 106 71-138
Dibromomethane mg/kg 0.066.061 108 74-130
Dichlorodifluoromethane mg/kg 0.061.061 100 40-160
Diisopropyl ether mg/kg 0.068.061 111 69-141
Ethylbenzene mg/kg 0.061.061 100 75-133
Hexachloro-1,3-butadiene mg/kg 0.062.061 102 68-143
Isopropylbenzene (Cumene)mg/kg 0.060.061 98 76-143
m&p-Xylene mg/kg 0.12.12 99 75-136
Methyl-tert-butyl ether mg/kg 0.068.061 111 68-144
Methylene Chloride mg/kg 0.072.061 117 45-154
n-Butylbenzene mg/kg 0.061.061 100 72-137
n-Propylbenzene mg/kg 0.062.061 101 76-136
Naphthalene mg/kg 0.074.061 120 68-151
o-Xylene mg/kg 0.061.061 99 76-141
p-Isopropyltoluene mg/kg 0.063.061 103 76-140
sec-Butylbenzene mg/kg 0.061.061 100 79-139
Styrene mg/kg 0.063.061 102 79-137
tert-Butylbenzene mg/kg 0.056.061 92 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 118 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2098949LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene mg/kg 0.053.061 86 71-138
Toluene mg/kg 0.066.061 108 74-131
trans-1,2-Dichloroethene mg/kg 0.066.061 108 67-135
trans-1,3-Dichloropropene mg/kg 0.069.061 112 65-146
Trichloroethene mg/kg 0.070.061 114 67-135
Trichlorofluoromethane mg/kg 0.069.061 113 59-144
Vinyl acetate mg/kg 0.096.12 78 40-160
Vinyl chloride mg/kg 0.071.061 116 56-141
Xylene (Total)mg/kg 0.18.18 99 76-137
1,2-Dichloroethane-d4 (S)%103 70-132
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%104 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2099745MATRIX SPIKE SAMPLE:
MSSpike
Result
92355949012
1,1,1,2-Tetrachloroethane mg/kg 0.61.58 105 70-130ND
1,1,1-Trichloroethane mg/kg 0.64.58 111 70-130ND
1,1,2,2-Tetrachloroethane mg/kg 0.60.58 103 70-130ND
1,1,2-Trichloroethane mg/kg 0.79 M1.58 137 70-130ND
1,1-Dichloroethane mg/kg 0.69.58 120 70-130ND
1,1-Dichloroethene mg/kg 0.64.58 111 49-180ND
1,1-Dichloropropene mg/kg 0.64.58 110 70-130ND
1,2,3-Trichlorobenzene mg/kg 0.69.58 118 70-130ND
1,2,3-Trichloropropane mg/kg 0.92 M1.58 159 70-130ND
1,2,4-Trichlorobenzene mg/kg 0.69.58 118 70-130ND
1,2,4-Trimethylbenzene mg/kg 2.2.58 99 70-1301.6
1,2-Dibromo-3-chloropropane mg/kg 1.8 M1.58 308 70-130ND
1,2-Dibromoethane (EDB)mg/kg 0.67.58 115 70-130ND
1,2-Dichlorobenzene mg/kg 0.64.58 111 70-130ND
1,2-Dichloroethane mg/kg 0.68.58 117 70-130ND
1,2-Dichloropropane mg/kg 0.62.58 106 70-130ND
1,3,5-Trimethylbenzene mg/kg 1.1.58 111 70-1300.42
1,3-Dichlorobenzene mg/kg 0.62.58 106 70-130ND
1,3-Dichloropropane mg/kg 0.64.58 111 70-130ND
1,4-Dichlorobenzene mg/kg 0.63.58 109 70-130ND
2,2-Dichloropropane mg/kg 0.67.58 115 70-130ND
2-Butanone (MEK)mg/kg 10.5 M11.2 911 70-130ND
2-Chlorotoluene mg/kg 0.67.58 117 70-130ND
2-Hexanone mg/kg 7.5 M11.2 652 70-130ND
4-Chlorotoluene mg/kg 0.75.58 130 70-130ND
4-Methyl-2-pentanone (MIBK)mg/kg 5.6 M11.2 483 70-130ND
Acetone mg/kg 7.7 M11.2 665 70-130ND
Benzene mg/kg 0.56.58 97 50-166ND
Bromobenzene mg/kg 0.72.58 125 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 119 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2099745MATRIX SPIKE SAMPLE:
MSSpike
Result
92355949012
Bromochloromethane mg/kg 0.67.58 116 70-130ND
Bromodichloromethane mg/kg 0.65.58 112 70-130ND
Bromoform mg/kg 0.59.58 102 70-130ND
Bromomethane mg/kg 0.67.58 115 70-130ND
Carbon tetrachloride mg/kg 0.53.58 92 70-130ND
Chlorobenzene mg/kg 0.63.58 109 43-169ND
Chloroethane mg/kg 0.33 M1.58 58 70-130ND
Chloroform mg/kg 0.66.58 114 70-130ND
Chloromethane mg/kg 0.71.58 122 70-130ND
cis-1,2-Dichloroethene mg/kg 0.68.58 118 70-130ND
cis-1,3-Dichloropropene mg/kg 0.59.58 102 70-130ND
Dibromochloromethane mg/kg 0.61.58 105 70-130ND
Dibromomethane mg/kg 0.56.58 97 70-130ND
Dichlorodifluoromethane mg/kg 0.59.58 101 70-130ND
Diisopropyl ether mg/kg 0.69.58 120 70-130ND
Ethylbenzene mg/kg 0.63.58 103 70-130ND
Hexachloro-1,3-butadiene mg/kg 0.57.58 99 70-130ND
Isopropylbenzene (Cumene)mg/kg 0.70.58 100 70-130ND
m&p-Xylene mg/kg 1.21.2 102 70-130ND
Methyl-tert-butyl ether mg/kg 0.71.58 123 70-130ND
Methylene Chloride mg/kg 0.61.58 106 70-130ND
n-Butylbenzene mg/kg 1.3 M1.58 233 70-130ND
n-Propylbenzene mg/kg 1.3.58 99 70-1300.71
Naphthalene mg/kg 0.90.58 103 70-1300.30
o-Xylene mg/kg 0.60.58 103 70-130ND
p-Isopropyltoluene mg/kg 0.79.58 88 70-1300.28
sec-Butylbenzene mg/kg 0.80.58 101 70-1300.21
Styrene mg/kg 0.63.58 109 70-130ND
tert-Butylbenzene mg/kg 0.54.58 93 70-130ND
Tetrachloroethene mg/kg 0.53.58 91 70-130ND
Toluene mg/kg 0.59.58 102 52-163ND
trans-1,2-Dichloroethene mg/kg 0.67.58 116 70-130ND
trans-1,3-Dichloropropene mg/kg 0.58.58 100 70-130ND
Trichloroethene mg/kg 0.63.58 110 49-167ND
Trichlorofluoromethane mg/kg 0.32 M1.58 56 70-130ND
Vinyl acetate mg/kg .65J M11.2 56 70-130ND
Vinyl chloride mg/kg 0.68.58 117 70-130ND
1,2-Dichloroethane-d4 (S)%120 70-132
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%94 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92355949010
2099744SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 120 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92355949010
2099744SAMPLE DUPLICATE:
1,1,1-Trichloroethane mg/kg NDND
1,1,2,2-Tetrachloroethane mg/kg NDND
1,1,2-Trichloroethane mg/kg NDND
1,1-Dichloroethane mg/kg NDND
1,1-Dichloroethene mg/kg NDND
1,1-Dichloropropene mg/kg NDND
1,2,3-Trichlorobenzene mg/kg NDND
1,2,3-Trichloropropane mg/kg NDND
1,2,4-Trichlorobenzene mg/kg NDND
1,2,4-Trimethylbenzene mg/kg NDND
1,2-Dibromo-3-chloropropane mg/kg NDND
1,2-Dibromoethane (EDB)mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,2-Dichloroethane mg/kg NDND
1,2-Dichloropropane mg/kg NDND
1,3,5-Trimethylbenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
1,3-Dichloropropane mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
2,2-Dichloropropane mg/kg NDND
2-Butanone (MEK)mg/kg NDND
2-Chlorotoluene mg/kg NDND
2-Hexanone mg/kg NDND
4-Chlorotoluene mg/kg NDND
4-Methyl-2-pentanone (MIBK)mg/kg NDND
Acetone mg/kg NDND
Benzene mg/kg NDND
Bromobenzene mg/kg NDND
Bromochloromethane mg/kg NDND
Bromodichloromethane mg/kg NDND
Bromoform mg/kg NDND
Bromomethane mg/kg NDND
Carbon tetrachloride mg/kg NDND
Chlorobenzene mg/kg NDND
Chloroethane mg/kg NDND
Chloroform mg/kg NDND
Chloromethane mg/kg NDND
cis-1,2-Dichloroethene mg/kg NDND
cis-1,3-Dichloropropene mg/kg NDND
Dibromochloromethane mg/kg NDND
Dibromomethane mg/kg NDND
Dichlorodifluoromethane mg/kg NDND
Diisopropyl ether mg/kg NDND
Ethylbenzene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg NDND
Isopropylbenzene (Cumene)mg/kg NDND
m&p-Xylene mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 121 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92355949010
2099744SAMPLE DUPLICATE:
Methyl-tert-butyl ether mg/kg NDND
Methylene Chloride mg/kg NDND
n-Butylbenzene mg/kg NDND
n-Propylbenzene mg/kg NDND
Naphthalene mg/kg NDND
o-Xylene mg/kg NDND
p-Isopropyltoluene mg/kg NDND
sec-Butylbenzene mg/kg NDND
Styrene mg/kg NDND
tert-Butylbenzene mg/kg NDND
Tetrachloroethene mg/kg NDND
Toluene mg/kg NDND
trans-1,2-Dichloroethene mg/kg NDND
trans-1,3-Dichloropropene mg/kg NDND
Trichloroethene mg/kg NDND
Trichlorofluoromethane mg/kg NDND
Vinyl acetate mg/kg NDND
Vinyl chloride mg/kg NDND
Xylene (Total)mg/kg NDND
1,2-Dichloroethane-d4 (S)%118 7122
4-Bromofluorobenzene (S)%98 1296
Toluene-d8 (S)%101 7104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 122 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
378935
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92355949013, 92355949014, 92355949016, 92355949017, 92355949018, 92355949019, 92355949020,
92355949021, 92355949022, 92355949023, 92355949024
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2099970
Associated Lab Samples:92355949013, 92355949014, 92355949016, 92355949017, 92355949018, 92355949019, 92355949020,
92355949021, 92355949022, 92355949023, 92355949024
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane mg/kg ND 0.0050 09/22/17 12:47
1,1,1-Trichloroethane mg/kg ND 0.0050 09/22/17 12:47
1,1,2,2-Tetrachloroethane mg/kg ND 0.0050 09/22/17 12:47
1,1,2-Trichloroethane mg/kg ND 0.0050 09/22/17 12:47
1,1-Dichloroethane mg/kg ND 0.0050 09/22/17 12:47
1,1-Dichloroethene mg/kg ND 0.0050 09/22/17 12:47
1,1-Dichloropropene mg/kg ND 0.0050 09/22/17 12:47
1,2,3-Trichlorobenzene mg/kg ND 0.0050 09/22/17 12:47
1,2,3-Trichloropropane mg/kg ND 0.0050 09/22/17 12:47
1,2,4-Trichlorobenzene mg/kg ND 0.0050 09/22/17 12:47
1,2,4-Trimethylbenzene mg/kg ND 0.0050 09/22/17 12:47
1,2-Dibromo-3-chloropropane mg/kg ND 0.0050 09/22/17 12:47
1,2-Dibromoethane (EDB)mg/kg ND 0.0050 09/22/17 12:47
1,2-Dichlorobenzene mg/kg ND 0.0050 09/22/17 12:47
1,2-Dichloroethane mg/kg ND 0.0050 09/22/17 12:47
1,2-Dichloropropane mg/kg ND 0.0050 09/22/17 12:47
1,3,5-Trimethylbenzene mg/kg ND 0.0050 09/22/17 12:47
1,3-Dichlorobenzene mg/kg ND 0.0050 09/22/17 12:47
1,3-Dichloropropane mg/kg ND 0.0050 09/22/17 12:47
1,4-Dichlorobenzene mg/kg ND 0.0050 09/22/17 12:47
2,2-Dichloropropane mg/kg ND 0.0050 09/22/17 12:47
2-Butanone (MEK)mg/kg ND 0.10 09/22/17 12:47
2-Chlorotoluene mg/kg ND 0.0050 09/22/17 12:47
2-Hexanone mg/kg ND 0.050 09/22/17 12:47
4-Chlorotoluene mg/kg ND 0.0050 09/22/17 12:47
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.050 09/22/17 12:47
Acetone mg/kg ND 0.10 09/22/17 12:47
Benzene mg/kg ND 0.0050 09/22/17 12:47
Bromobenzene mg/kg ND 0.0050 09/22/17 12:47
Bromochloromethane mg/kg ND 0.0050 09/22/17 12:47
Bromodichloromethane mg/kg ND 0.0050 09/22/17 12:47
Bromoform mg/kg ND 0.0050 09/22/17 12:47
Bromomethane mg/kg ND 0.010 09/22/17 12:47
Carbon tetrachloride mg/kg ND 0.0050 09/22/17 12:47
Chlorobenzene mg/kg ND 0.0050 09/22/17 12:47
Chloroethane mg/kg ND 0.010 09/22/17 12:47
Chloroform mg/kg ND 0.0050 09/22/17 12:47
Chloromethane mg/kg ND 0.010 09/22/17 12:47
cis-1,2-Dichloroethene mg/kg ND 0.0050 09/22/17 12:47
cis-1,3-Dichloropropene mg/kg ND 0.0050 09/22/17 12:47
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 123 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2099970
Associated Lab Samples:92355949013, 92355949014, 92355949016, 92355949017, 92355949018, 92355949019, 92355949020,
92355949021, 92355949022, 92355949023, 92355949024
Matrix:Solid
Analyzed
Dibromochloromethane mg/kg ND 0.0050 09/22/17 12:47
Dibromomethane mg/kg ND 0.0050 09/22/17 12:47
Dichlorodifluoromethane mg/kg ND 0.010 09/22/17 12:47
Diisopropyl ether mg/kg ND 0.0050 09/22/17 12:47
Ethylbenzene mg/kg ND 0.0050 09/22/17 12:47
Hexachloro-1,3-butadiene mg/kg ND 0.0050 09/22/17 12:47
Isopropylbenzene (Cumene)mg/kg ND 0.0050 09/22/17 12:47
m&p-Xylene mg/kg ND 0.010 09/22/17 12:47
Methyl-tert-butyl ether mg/kg ND 0.0050 09/22/17 12:47
Methylene Chloride mg/kg ND 0.020 09/22/17 12:47
n-Butylbenzene mg/kg ND 0.0050 09/22/17 12:47
n-Propylbenzene mg/kg ND 0.0050 09/22/17 12:47
Naphthalene mg/kg ND 0.0050 09/22/17 12:47
o-Xylene mg/kg ND 0.0050 09/22/17 12:47
p-Isopropyltoluene mg/kg ND 0.0050 09/22/17 12:47
sec-Butylbenzene mg/kg ND 0.0050 09/22/17 12:47
Styrene mg/kg ND 0.0050 09/22/17 12:47
tert-Butylbenzene mg/kg ND 0.0050 09/22/17 12:47
Tetrachloroethene mg/kg ND 0.0050 09/22/17 12:47
Toluene mg/kg ND 0.0050 09/22/17 12:47
trans-1,2-Dichloroethene mg/kg ND 0.0050 09/22/17 12:47
trans-1,3-Dichloropropene mg/kg ND 0.0050 09/22/17 12:47
Trichloroethene mg/kg ND 0.0050 09/22/17 12:47
Trichlorofluoromethane mg/kg ND 0.0050 09/22/17 12:47
Vinyl acetate mg/kg ND 0.050 09/22/17 12:47
Vinyl chloride mg/kg ND 0.010 09/22/17 12:47
Xylene (Total)mg/kg ND 0.010 09/22/17 12:47
1,2-Dichloroethane-d4 (S)%122 70-132 09/22/17 12:47
4-Bromofluorobenzene (S)%105 70-130 09/22/17 12:47
Toluene-d8 (S)%104 70-130 09/22/17 12:47
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2099971LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.055.049 113 74-137
1,1,1-Trichloroethane mg/kg 0.059.049 121 67-140
1,1,2,2-Tetrachloroethane mg/kg 0.048.049 97 72-141
1,1,2-Trichloroethane mg/kg 0.057.049 116 78-138
1,1-Dichloroethane mg/kg 0.058.049 119 69-134
1,1-Dichloroethene mg/kg 0.059.049 120 67-138
1,1-Dichloropropene mg/kg 0.062.049 125 69-139
1,2,3-Trichlorobenzene mg/kg 0.060.049 122 70-146
1,2,3-Trichloropropane mg/kg 0.057.049 117 69-144
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 124 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2099971LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 0.056.049 114 68-148
1,2,4-Trimethylbenzene mg/kg 0.054.049 110 74-137
1,2-Dibromo-3-chloropropane mg/kg 0.056.049 114 65-140
1,2-Dibromoethane (EDB)mg/kg 0.060.049 122 77-135
1,2-Dichlorobenzene mg/kg 0.055.049 112 77-141
1,2-Dichloroethane mg/kg 0.062.049 126 65-137
1,2-Dichloropropane mg/kg 0.057.049 115 72-136
1,3,5-Trimethylbenzene mg/kg 0.053.049 108 76-133
1,3-Dichlorobenzene mg/kg 0.053.049 109 74-138
1,3-Dichloropropane mg/kg 0.059.049 121 71-139
1,4-Dichlorobenzene mg/kg 0.055.049 113 76-138
2,2-Dichloropropane mg/kg 0.058.049 118 68-137
2-Butanone (MEK)mg/kg 0.12.098 125 58-147
2-Chlorotoluene mg/kg 0.053.049 108 73-139
2-Hexanone mg/kg 0.12.098 119 62-145
4-Chlorotoluene mg/kg 0.053.049 109 76-141
4-Methyl-2-pentanone (MIBK)mg/kg 0.12.098 119 64-149
Acetone mg/kg 0.16 L1.098 160 53-153
Benzene mg/kg 0.055.049 113 73-135
Bromobenzene mg/kg 0.056.049 113 75-133
Bromochloromethane mg/kg 0.062.049 127 73-134
Bromodichloromethane mg/kg 0.055.049 112 71-135
Bromoform mg/kg 0.058.049 118 66-141
Bromomethane mg/kg 0.070.049 143 53-160
Carbon tetrachloride mg/kg 0.052.049 107 60-145
Chlorobenzene mg/kg 0.055.049 112 78-130
Chloroethane mg/kg 0.066.049 134 64-149
Chloroform mg/kg 0.057.049 116 70-134
Chloromethane mg/kg 0.069.049 140 52-150
cis-1,2-Dichloroethene mg/kg 0.060.049 122 70-133
cis-1,3-Dichloropropene mg/kg 0.059.049 120 68-134
Dibromochloromethane mg/kg 0.059.049 121 71-138
Dibromomethane mg/kg 0.056.049 113 74-130
Dichlorodifluoromethane mg/kg 0.057.049 116 40-160
Diisopropyl ether mg/kg 0.062.049 126 69-141
Ethylbenzene mg/kg 0.055.049 112 75-133
Hexachloro-1,3-butadiene mg/kg 0.055.049 112 68-143
Isopropylbenzene (Cumene)mg/kg 0.054.049 110 76-143
m&p-Xylene mg/kg 0.11.098 111 75-136
Methyl-tert-butyl ether mg/kg 0.062.049 126 68-144
Methylene Chloride mg/kg 0.065.049 132 45-154
n-Butylbenzene mg/kg 0.053.049 107 72-137
n-Propylbenzene mg/kg 0.053.049 108 76-136
Naphthalene mg/kg 0.061.049 124 68-151
o-Xylene mg/kg 0.054.049 111 76-141
p-Isopropyltoluene mg/kg 0.054.049 110 76-140
sec-Butylbenzene mg/kg 0.053.049 107 79-139
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2099971LABORATORY CONTROL SAMPLE:
LCSSpike
Styrene mg/kg 0.058.049 118 79-137
tert-Butylbenzene mg/kg 0.047.049 96 74-143
Tetrachloroethene mg/kg 0.049.049 100 71-138
Toluene mg/kg 0.057.049 115 74-131
trans-1,2-Dichloroethene mg/kg 0.060.049 123 67-135
trans-1,3-Dichloropropene mg/kg 0.059.049 120 65-146
Trichloroethene mg/kg 0.062.049 126 67-135
Trichlorofluoromethane mg/kg 0.062.049 127 59-144
Vinyl acetate mg/kg 0.049.098 50 40-160
Vinyl chloride mg/kg 0.064.049 131 56-141
Xylene (Total)mg/kg 0.16.15 111 76-137
1,2-Dichloroethane-d4 (S)%113 70-132
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2101022MATRIX SPIKE SAMPLE:
MSSpike
Result
92356028001
1,1,1,2-Tetrachloroethane mg/kg 0.015.017 88 70-130ND
1,1,1-Trichloroethane mg/kg 0.016.017 96 70-130ND
1,1,2,2-Tetrachloroethane mg/kg 0.016.017 93 70-130ND
1,1,2-Trichloroethane mg/kg 0.014.017 83 70-130ND
1,1-Dichloroethane mg/kg 0.017.017 97 70-130ND
1,1-Dichloroethene mg/kg 0.016.017 91 49-180ND
1,1-Dichloropropene mg/kg 0.017.017 98 70-130ND
1,2,3-Trichlorobenzene mg/kg 0.011 M1.017 66 70-130ND
1,2,3-Trichloropropane mg/kg 0.015.017 88 70-130ND
1,2,4-Trichlorobenzene mg/kg 0.012 M1.017 67 70-130ND
1,2,4-Trimethylbenzene mg/kg 0.016.017 92 70-130ND
1,2-Dibromo-3-chloropropane mg/kg 0.017.017 96 70-130ND
1,2-Dibromoethane (EDB)mg/kg 0.015.017 88 70-130ND
1,2-Dichlorobenzene mg/kg 0.014.017 82 70-130ND
1,2-Dichloroethane mg/kg 0.016.017 91 70-130ND
1,2-Dichloropropane mg/kg 0.017.017 97 70-130ND
1,3,5-Trimethylbenzene mg/kg 0.016.017 95 70-130ND
1,3-Dichlorobenzene mg/kg 0.014.017 82 70-130ND
1,3-Dichloropropane mg/kg 0.016.017 91 70-130ND
1,4-Dichlorobenzene mg/kg 0.014.017 81 70-130ND
2,2-Dichloropropane mg/kg 0.016.017 93 70-130ND
2-Butanone (MEK)mg/kg .029J.035 84 70-130ND
2-Chlorotoluene mg/kg 0.016.017 92 70-130ND
2-Hexanone mg/kg .031J.035 90 70-130ND
4-Chlorotoluene mg/kg 0.016.017 91 70-130ND
4-Methyl-2-pentanone (MIBK)mg/kg .03J.035 88 70-130ND
Acetone mg/kg 0.19 M0.035 401 70-130ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 126 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2101022MATRIX SPIKE SAMPLE:
MSSpike
Result
92356028001
Benzene mg/kg 0.017.017 97 50-166ND
Bromobenzene mg/kg 0.016.017 94 70-130ND
Bromochloromethane mg/kg 0.016.017 93 70-130ND
Bromodichloromethane mg/kg 0.015.017 89 70-130ND
Bromoform mg/kg 0.016.017 91 70-130ND
Bromomethane mg/kg 0.015.017 88 70-130ND
Carbon tetrachloride mg/kg 0.016.017 96 70-130ND
Chlorobenzene mg/kg 0.016.017 93 43-169ND
Chloroethane mg/kg 0.015.017 89 70-130ND
Chloroform mg/kg 0.016.017 96 70-130ND
Chloromethane mg/kg 0.015.017 86 70-130ND
cis-1,2-Dichloroethene mg/kg 0.016.017 96 70-130ND
cis-1,3-Dichloropropene mg/kg 0.015.017 89 70-130ND
Dibromochloromethane mg/kg 0.015.017 85 70-130ND
Dibromomethane mg/kg 0.015.017 86 70-130ND
Dichlorodifluoromethane mg/kg 0.012 M1.017 69 70-130ND
Diisopropyl ether mg/kg 0.016.017 95 70-130ND
Ethylbenzene mg/kg 0.016.017 96 70-130ND
Hexachloro-1,3-butadiene mg/kg 0.013.017 78 70-130ND
Isopropylbenzene (Cumene)mg/kg 0.016.017 94 70-130ND
m&p-Xylene mg/kg 0.032.035 94 70-130ND
Methyl-tert-butyl ether mg/kg 0.015.017 86 70-130ND
Methylene Chloride mg/kg .016J.017 92 70-130ND
n-Butylbenzene mg/kg 0.015.017 87 70-130ND
n-Propylbenzene mg/kg 0.016.017 93 70-130ND
Naphthalene mg/kg 0.012 M1.017 68 70-130ND
o-Xylene mg/kg 0.016.017 95 70-130ND
p-Isopropyltoluene mg/kg 0.016.017 93 70-130ND
sec-Butylbenzene mg/kg 0.016.017 94 70-130ND
Styrene mg/kg 0.015.017 88 70-130ND
tert-Butylbenzene mg/kg 0.016.017 93 70-130ND
Tetrachloroethene mg/kg 0.013.017 75 70-130ND
Toluene mg/kg 0.016.017 96 52-163ND
trans-1,2-Dichloroethene mg/kg 0.016.017 93 70-130ND
trans-1,3-Dichloropropene mg/kg 0.015.017 85 70-130ND
Trichloroethene mg/kg 0.016.017 93 49-167ND
Trichlorofluoromethane mg/kg 0.014.017 82 70-130ND
Vinyl acetate mg/kg .012J M1.035 35 70-130ND
Vinyl chloride mg/kg 0.015.017 85 70-130ND
1,2-Dichloroethane-d4 (S)%96 70-132
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%99 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
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Huntersville, NC 28078
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Page 127 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92355949013
2101021SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg NDND
1,1,1-Trichloroethane mg/kg NDND
1,1,2,2-Tetrachloroethane mg/kg NDND
1,1,2-Trichloroethane mg/kg NDND
1,1-Dichloroethane mg/kg NDND
1,1-Dichloroethene mg/kg NDND
1,1-Dichloropropene mg/kg NDND
1,2,3-Trichlorobenzene mg/kg NDND
1,2,3-Trichloropropane mg/kg NDND
1,2,4-Trichlorobenzene mg/kg NDND
1,2,4-Trimethylbenzene mg/kg NDND
1,2-Dibromo-3-chloropropane mg/kg NDND
1,2-Dibromoethane (EDB)mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,2-Dichloroethane mg/kg NDND
1,2-Dichloropropane mg/kg NDND
1,3,5-Trimethylbenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
1,3-Dichloropropane mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
2,2-Dichloropropane mg/kg NDND
2-Butanone (MEK)mg/kg NDND
2-Chlorotoluene mg/kg NDND
2-Hexanone mg/kg NDND
4-Chlorotoluene mg/kg NDND
4-Methyl-2-pentanone (MIBK)mg/kg NDND
Acetone mg/kg .046JND
Benzene mg/kg NDND
Bromobenzene mg/kg NDND
Bromochloromethane mg/kg NDND
Bromodichloromethane mg/kg NDND
Bromoform mg/kg NDND
Bromomethane mg/kg NDND
Carbon tetrachloride mg/kg NDND
Chlorobenzene mg/kg NDND
Chloroethane mg/kg NDND
Chloroform mg/kg NDND
Chloromethane mg/kg NDND
cis-1,2-Dichloroethene mg/kg NDND
cis-1,3-Dichloropropene mg/kg NDND
Dibromochloromethane mg/kg NDND
Dibromomethane mg/kg NDND
Dichlorodifluoromethane mg/kg NDND
Diisopropyl ether mg/kg NDND
Ethylbenzene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg NDND
Isopropylbenzene (Cumene)mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 128 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92355949013
2101021SAMPLE DUPLICATE:
m&p-Xylene mg/kg NDND
Methyl-tert-butyl ether mg/kg NDND
Methylene Chloride mg/kg NDND
n-Butylbenzene mg/kg NDND
n-Propylbenzene mg/kg NDND
Naphthalene mg/kg NDND
o-Xylene mg/kg NDND
p-Isopropyltoluene mg/kg NDND
sec-Butylbenzene mg/kg NDND
Styrene mg/kg NDND
tert-Butylbenzene mg/kg NDND
Tetrachloroethene mg/kg NDND
Toluene mg/kg NDND
trans-1,2-Dichloroethene mg/kg NDND
trans-1,3-Dichloropropene mg/kg NDND
Trichloroethene mg/kg NDND
Trichlorofluoromethane mg/kg NDND
Vinyl acetate mg/kg NDND
Vinyl chloride mg/kg NDND
Xylene (Total)mg/kg NDND
1,2-Dichloroethane-d4 (S)%95 19109
4-Bromofluorobenzene (S)%97 8100
Toluene-d8 (S)%98 8101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 129 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
379248
EPA 8260
EPA 8260
8260 MSV 5035A Volatile Organics
Associated Lab Samples:92355949015
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2101667
Associated Lab Samples:92355949015
Matrix:Solid
Analyzed
1,1,1,2-Tetrachloroethane mg/kg ND 0.0057 09/25/17 14:30
1,1,1-Trichloroethane mg/kg ND 0.0057 09/25/17 14:30
1,1,2,2-Tetrachloroethane mg/kg ND 0.0057 09/25/17 14:30
1,1,2-Trichloroethane mg/kg ND 0.0057 09/25/17 14:30
1,1-Dichloroethane mg/kg ND 0.0057 09/25/17 14:30
1,1-Dichloroethene mg/kg ND 0.0057 09/25/17 14:30
1,1-Dichloropropene mg/kg ND 0.0057 09/25/17 14:30
1,2,3-Trichlorobenzene mg/kg ND 0.0057 09/25/17 14:30
1,2,3-Trichloropropane mg/kg ND 0.0057 09/25/17 14:30
1,2,4-Trichlorobenzene mg/kg ND 0.0057 09/25/17 14:30
1,2,4-Trimethylbenzene mg/kg ND 0.0057 09/25/17 14:30
1,2-Dibromo-3-chloropropane mg/kg ND 0.0057 09/25/17 14:30
1,2-Dibromoethane (EDB)mg/kg ND 0.0057 09/25/17 14:30
1,2-Dichlorobenzene mg/kg ND 0.0057 09/25/17 14:30
1,2-Dichloroethane mg/kg ND 0.0057 09/25/17 14:30
1,2-Dichloropropane mg/kg ND 0.0057 09/25/17 14:30
1,3,5-Trimethylbenzene mg/kg ND 0.0057 09/25/17 14:30
1,3-Dichlorobenzene mg/kg ND 0.0057 09/25/17 14:30
1,3-Dichloropropane mg/kg ND 0.0057 09/25/17 14:30
1,4-Dichlorobenzene mg/kg ND 0.0057 09/25/17 14:30
2,2-Dichloropropane mg/kg ND 0.0057 09/25/17 14:30
2-Butanone (MEK)mg/kg ND 0.11 09/25/17 14:30
2-Chlorotoluene mg/kg ND 0.0057 09/25/17 14:30
2-Hexanone mg/kg ND 0.057 09/25/17 14:30
4-Chlorotoluene mg/kg ND 0.0057 09/25/17 14:30
4-Methyl-2-pentanone (MIBK)mg/kg ND 0.057 09/25/17 14:30
Acetone mg/kg ND 0.11 09/25/17 14:30
Benzene mg/kg ND 0.0057 09/25/17 14:30
Bromobenzene mg/kg ND 0.0057 09/25/17 14:30
Bromochloromethane mg/kg ND 0.0057 09/25/17 14:30
Bromodichloromethane mg/kg ND 0.0057 09/25/17 14:30
Bromoform mg/kg ND 0.0057 09/25/17 14:30
Bromomethane mg/kg ND 0.011 09/25/17 14:30
Carbon tetrachloride mg/kg ND 0.0057 09/25/17 14:30
Chlorobenzene mg/kg ND 0.0057 09/25/17 14:30
Chloroethane mg/kg ND 0.011 09/25/17 14:30
Chloroform mg/kg ND 0.0057 09/25/17 14:30
Chloromethane mg/kg ND 0.011 09/25/17 14:30
cis-1,2-Dichloroethene mg/kg ND 0.0057 09/25/17 14:30
cis-1,3-Dichloropropene mg/kg ND 0.0057 09/25/17 14:30
Dibromochloromethane mg/kg ND 0.0057 09/25/17 14:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 130 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2101667
Associated Lab Samples:92355949015
Matrix:Solid
Analyzed
Dibromomethane mg/kg ND 0.0057 09/25/17 14:30
Dichlorodifluoromethane mg/kg ND 0.011 09/25/17 14:30
Diisopropyl ether mg/kg ND 0.0057 09/25/17 14:30
Ethylbenzene mg/kg ND 0.0057 09/25/17 14:30
Hexachloro-1,3-butadiene mg/kg ND 0.0057 09/25/17 14:30
Isopropylbenzene (Cumene)mg/kg ND 0.0057 09/25/17 14:30
m&p-Xylene mg/kg ND 0.011 09/25/17 14:30
Methyl-tert-butyl ether mg/kg ND 0.0057 09/25/17 14:30
Methylene Chloride mg/kg ND 0.023 09/25/17 14:30
n-Butylbenzene mg/kg ND 0.0057 09/25/17 14:30
n-Propylbenzene mg/kg ND 0.0057 09/25/17 14:30
Naphthalene mg/kg ND 0.0057 09/25/17 14:30
o-Xylene mg/kg ND 0.0057 09/25/17 14:30
p-Isopropyltoluene mg/kg ND 0.0057 09/25/17 14:30
sec-Butylbenzene mg/kg ND 0.0057 09/25/17 14:30
Styrene mg/kg ND 0.0057 09/25/17 14:30
tert-Butylbenzene mg/kg ND 0.0057 09/25/17 14:30
Tetrachloroethene mg/kg ND 0.0057 09/25/17 14:30
Toluene mg/kg ND 0.0057 09/25/17 14:30
trans-1,2-Dichloroethene mg/kg ND 0.0057 09/25/17 14:30
trans-1,3-Dichloropropene mg/kg ND 0.0057 09/25/17 14:30
Trichloroethene mg/kg ND 0.0057 09/25/17 14:30
Trichlorofluoromethane mg/kg ND 0.0057 09/25/17 14:30
Vinyl acetate mg/kg ND 0.057 09/25/17 14:30
Vinyl chloride mg/kg ND 0.011 09/25/17 14:30
Xylene (Total)mg/kg ND 0.011 09/25/17 14:30
1,2-Dichloroethane-d4 (S)%97 70-132 09/25/17 14:30
4-Bromofluorobenzene (S)%104 70-130 09/25/17 14:30
Toluene-d8 (S)%100 70-130 09/25/17 14:30
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2101668LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane mg/kg 0.063.056 112 74-137
1,1,1-Trichloroethane mg/kg 0.059.056 106 67-140
1,1,2,2-Tetrachloroethane mg/kg 0.057.056 102 72-141
1,1,2-Trichloroethane mg/kg 0.060.056 107 78-138
1,1-Dichloroethane mg/kg 0.059.056 105 69-134
1,1-Dichloroethene mg/kg 0.059.056 104 67-138
1,1-Dichloropropene mg/kg 0.061.056 108 69-139
1,2,3-Trichlorobenzene mg/kg 0.061.056 109 70-146
1,2,3-Trichloropropane mg/kg 0.062.056 111 69-144
1,2,4-Trichlorobenzene mg/kg 0.062.056 110 68-148
1,2,4-Trimethylbenzene mg/kg 0.064.056 113 74-137
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 131 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2101668LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane mg/kg 0.057.056 101 65-140
1,2-Dibromoethane (EDB)mg/kg 0.062.056 111 77-135
1,2-Dichlorobenzene mg/kg 0.063.056 112 77-141
1,2-Dichloroethane mg/kg 0.058.056 104 65-137
1,2-Dichloropropane mg/kg 0.063.056 112 72-136
1,3,5-Trimethylbenzene mg/kg 0.065.056 115 76-133
1,3-Dichlorobenzene mg/kg 0.060.056 106 74-138
1,3-Dichloropropane mg/kg 0.063.056 112 71-139
1,4-Dichlorobenzene mg/kg 0.059.056 105 76-138
2,2-Dichloropropane mg/kg 0.057.056 102 68-137
2-Butanone (MEK)mg/kg 0.13.11 112 58-147
2-Chlorotoluene mg/kg 0.062.056 110 73-139
2-Hexanone mg/kg 0.12.11 107 62-145
4-Chlorotoluene mg/kg 0.062.056 111 76-141
4-Methyl-2-pentanone (MIBK)mg/kg 0.13.11 114 64-149
Acetone mg/kg 0.13.11 118 53-153
Benzene mg/kg 0.061.056 108 73-135
Bromobenzene mg/kg 0.064.056 114 75-133
Bromochloromethane mg/kg 0.062.056 110 73-134
Bromodichloromethane mg/kg 0.061.056 109 71-135
Bromoform mg/kg 0.059.056 105 66-141
Bromomethane mg/kg 0.058.056 103 53-160
Carbon tetrachloride mg/kg 0.060.056 107 60-145
Chlorobenzene mg/kg 0.062.056 110 78-130
Chloroethane mg/kg 0.053.056 94 64-149
Chloroform mg/kg 0.060.056 107 70-134
Chloromethane mg/kg 0.050.056 88 52-150
cis-1,2-Dichloroethene mg/kg 0.060.056 107 70-133
cis-1,3-Dichloropropene mg/kg 0.064.056 114 68-134
Dibromochloromethane mg/kg 0.065.056 115 71-138
Dibromomethane mg/kg 0.057.056 101 74-130
Dichlorodifluoromethane mg/kg 0.039.056 70 40-160
Diisopropyl ether mg/kg 0.062.056 109 69-141
Ethylbenzene mg/kg 0.063.056 111 75-133
Hexachloro-1,3-butadiene mg/kg 0.065.056 115 68-143
Isopropylbenzene (Cumene)mg/kg 0.062.056 110 76-143
m&p-Xylene mg/kg 0.12.11 109 75-136
Methyl-tert-butyl ether mg/kg 0.060.056 106 68-144
Methylene Chloride mg/kg 0.056.056 100 45-154
n-Butylbenzene mg/kg 0.062.056 109 72-137
n-Propylbenzene mg/kg 0.062.056 110 76-136
Naphthalene mg/kg 0.067.056 119 68-151
o-Xylene mg/kg 0.062.056 110 76-141
p-Isopropyltoluene mg/kg 0.063.056 111 76-140
sec-Butylbenzene mg/kg 0.062.056 111 79-139
Styrene mg/kg 0.063.056 112 79-137
tert-Butylbenzene mg/kg 0.061.056 109 74-143
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 132 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2101668LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene mg/kg 0.038 L2.056 67 71-138
Toluene mg/kg 0.060.056 107 74-131
trans-1,2-Dichloroethene mg/kg 0.060.056 107 67-135
trans-1,3-Dichloropropene mg/kg 0.064.056 113 65-146
Trichloroethene mg/kg 0.066.056 117 67-135
Trichlorofluoromethane mg/kg 0.050.056 88 59-144
Vinyl acetate mg/kg 0.073.11 65 40-160
Vinyl chloride mg/kg 0.050.056 89 56-141
Xylene (Total)mg/kg 0.18.17 109 76-137
1,2-Dichloroethane-d4 (S)%95 70-132
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2102503MATRIX SPIKE SAMPLE:
MSSpike
Result
92356367001
1,1,1,2-Tetrachloroethane mg/kg 0.014.017 84 70-130ND
1,1,1-Trichloroethane mg/kg 0.015.017 89 70-130ND
1,1,2,2-Tetrachloroethane mg/kg 0.015.017 88 70-130ND
1,1,2-Trichloroethane mg/kg 0.014.017 80 70-130ND
1,1-Dichloroethane mg/kg 0.015.017 85 70-130ND
1,1-Dichloroethene mg/kg 0.015.017 88 49-180ND
1,1-Dichloropropene mg/kg 0.015.017 86 70-130ND
1,2,3-Trichlorobenzene mg/kg 0.0079 M1.017 47 70-130ND
1,2,3-Trichloropropane mg/kg 0.015.017 87 70-130ND
1,2,4-Trichlorobenzene mg/kg 0.0086 M1.017 50 70-130ND
1,2,4-Trimethylbenzene mg/kg 0.016.017 96 70-130ND
1,2-Dibromo-3-chloropropane mg/kg 0.015.017 88 70-130ND
1,2-Dibromoethane (EDB)mg/kg 0.015.017 87 70-130ND
1,2-Dichlorobenzene mg/kg 0.013.017 74 70-130ND
1,2-Dichloroethane mg/kg 0.015.017 91 70-130ND
1,2-Dichloropropane mg/kg 0.015.017 86 70-130ND
1,3,5-Trimethylbenzene mg/kg 0.016.017 94 70-130ND
1,3-Dichlorobenzene mg/kg 0.013.017 78 70-130ND
1,3-Dichloropropane mg/kg 0.015.017 88 70-130ND
1,4-Dichlorobenzene mg/kg 0.013.017 78 70-130ND
2,2-Dichloropropane mg/kg 0.015.017 88 70-130ND
2-Butanone (MEK)mg/kg .039J.034 115 70-130ND
2-Chlorotoluene mg/kg 0.015.017 91 70-130ND
2-Hexanone mg/kg .03J.034 88 70-130ND
4-Chlorotoluene mg/kg 0.015.017 89 70-130ND
4-Methyl-2-pentanone (MIBK)mg/kg .029J.034 86 70-130ND
Acetone mg/kg 0.11 M1.034 -142 70-1300.16
Benzene mg/kg 0.014.017 84 50-166ND
Bromobenzene mg/kg 0.015.017 89 70-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 133 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2102503MATRIX SPIKE SAMPLE:
MSSpike
Result
92356367001
Bromochloromethane mg/kg 0.015.017 91 70-130ND
Bromodichloromethane mg/kg 0.013.017 79 70-130ND
Bromoform mg/kg 0.013.017 78 70-130ND
Bromomethane mg/kg 0.015.017 90 70-130ND
Carbon tetrachloride mg/kg 0.014.017 81 70-130ND
Chlorobenzene mg/kg 0.014.017 84 43-169ND
Chloroethane mg/kg 0.016.017 96 70-130ND
Chloroform mg/kg 0.015.017 88 70-130ND
Chloromethane mg/kg 0.016.017 97 70-130ND
cis-1,2-Dichloroethene mg/kg 0.015.017 88 70-130ND
cis-1,3-Dichloropropene mg/kg 0.014.017 81 70-130ND
Dibromochloromethane mg/kg 0.014.017 81 70-130ND
Dibromomethane mg/kg 0.014.017 80 70-130ND
Dichlorodifluoromethane mg/kg 0.013.017 78 70-130ND
Diisopropyl ether mg/kg 0.015.017 88 70-130ND
Ethylbenzene mg/kg 0.015.017 87 70-130ND
Hexachloro-1,3-butadiene mg/kg 0.013.017 75 70-130ND
Isopropylbenzene (Cumene)mg/kg 0.014.017 84 70-130ND
m&p-Xylene mg/kg 0.030.034 88 70-130ND
Methyl-tert-butyl ether mg/kg 0.014.017 84 70-130ND
Methylene Chloride mg/kg .015J.017 88 70-130ND
n-Butylbenzene mg/kg 0.015.017 89 70-130ND
n-Propylbenzene mg/kg 0.016.017 94 70-130ND
Naphthalene mg/kg 0.0096 M1.017 56 70-130ND
o-Xylene mg/kg 0.015.017 86 70-130ND
p-Isopropyltoluene mg/kg 0.015.017 91 70-130ND
sec-Butylbenzene mg/kg 0.016.017 93 70-130ND
Styrene mg/kg 0.012.017 72 70-130ND
tert-Butylbenzene mg/kg 0.015.017 91 70-130ND
Tetrachloroethene mg/kg 0.0086 M0.017 51 70-130ND
Toluene mg/kg 0.015.017 88 52-163ND
trans-1,2-Dichloroethene mg/kg 0.015.017 89 70-130ND
trans-1,3-Dichloropropene mg/kg 0.014.017 80 70-130ND
Trichloroethene mg/kg 0.013.017 79 49-167ND
Trichlorofluoromethane mg/kg 0.016.017 96 70-130ND
Vinyl acetate mg/kg .016J M1.034 46 70-130ND
Vinyl chloride mg/kg 0.015.017 90 70-130ND
1,2-Dichloroethane-d4 (S)%110 70-132
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%101 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92356068002
2102502SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 134 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92356068002
2102502SAMPLE DUPLICATE:
1,1,1-Trichloroethane mg/kg NDND
1,1,2,2-Tetrachloroethane mg/kg NDND
1,1,2-Trichloroethane mg/kg NDND
1,1-Dichloroethane mg/kg NDND
1,1-Dichloroethene mg/kg NDND
1,1-Dichloropropene mg/kg NDND
1,2,3-Trichlorobenzene mg/kg NDND
1,2,3-Trichloropropane mg/kg NDND
1,2,4-Trichlorobenzene mg/kg NDND
1,2,4-Trimethylbenzene mg/kg NDND
1,2-Dibromo-3-chloropropane mg/kg NDND
1,2-Dibromoethane (EDB)mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,2-Dichloroethane mg/kg NDND
1,2-Dichloropropane mg/kg NDND
1,3,5-Trimethylbenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
1,3-Dichloropropane mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
2,2-Dichloropropane mg/kg NDND
2-Butanone (MEK)mg/kg .01JND
2-Chlorotoluene mg/kg NDND
2-Hexanone mg/kg NDND
4-Chlorotoluene mg/kg NDND
4-Methyl-2-pentanone (MIBK)mg/kg NDND
Acetone mg/kg 0.12ND
Benzene mg/kg NDND
Bromobenzene mg/kg NDND
Bromochloromethane mg/kg NDND
Bromodichloromethane mg/kg NDND
Bromoform mg/kg NDND
Bromomethane mg/kg NDND
Carbon tetrachloride mg/kg NDND
Chlorobenzene mg/kg NDND
Chloroethane mg/kg NDND
Chloroform mg/kg NDND
Chloromethane mg/kg NDND
cis-1,2-Dichloroethene mg/kg NDND
cis-1,3-Dichloropropene mg/kg NDND
Dibromochloromethane mg/kg NDND
Dibromomethane mg/kg NDND
Dichlorodifluoromethane mg/kg NDND
Diisopropyl ether mg/kg NDND
Ethylbenzene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg NDND
Isopropylbenzene (Cumene)mg/kg NDND
m&p-Xylene mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 135 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92356068002
2102502SAMPLE DUPLICATE:
Methyl-tert-butyl ether mg/kg NDND
Methylene Chloride mg/kg NDND
n-Butylbenzene mg/kg NDND
n-Propylbenzene mg/kg NDND
Naphthalene mg/kg NDND
o-Xylene mg/kg NDND
p-Isopropyltoluene mg/kg NDND
sec-Butylbenzene mg/kg NDND
Styrene mg/kg NDND
tert-Butylbenzene mg/kg NDND
Tetrachloroethene mg/kg NDND
Toluene mg/kg NDND
trans-1,2-Dichloroethene mg/kg NDND
trans-1,3-Dichloropropene mg/kg NDND
Trichloroethene mg/kg NDND
Trichlorofluoromethane mg/kg NDND
Vinyl acetate mg/kg NDND
Vinyl chloride mg/kg NDND
Xylene (Total)mg/kg NDND
1,2-Dichloroethane-d4 (S)%131 697
4-Bromofluorobenzene (S)%98 28102
Toluene-d8 (S)%100 2499
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 136 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
378645
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:92355949001, 92355949002, 92355949003, 92355949004, 92355949005, 92355949006, 92355949007,
92355949008, 92355949009, 92355949010, 92355949011, 92355949012, 92355949013, 92355949014,
92355949015, 92355949016, 92355949017, 92355949018, 92355949019, 92355949020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2098221
Associated Lab Samples:92355949001, 92355949002, 92355949003, 92355949004, 92355949005, 92355949006, 92355949007,
92355949008, 92355949009, 92355949010, 92355949011, 92355949012, 92355949013, 92355949014,
92355949015, 92355949016, 92355949017, 92355949018, 92355949019, 92355949020
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene mg/kg ND 0.33 09/21/17 14:15
1,2-Dichlorobenzene mg/kg ND 0.33 09/21/17 14:15
1,3-Dichlorobenzene mg/kg ND 0.33 09/21/17 14:15
1,4-Dichlorobenzene mg/kg ND 0.33 09/21/17 14:15
1-Methylnaphthalene mg/kg ND 0.33 09/21/17 14:15
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 09/21/17 14:15
2,4,5-Trichlorophenol mg/kg ND 0.33 09/21/17 14:15
2,4,6-Trichlorophenol mg/kg ND 0.33 09/21/17 14:15
2,4-Dichlorophenol mg/kg ND 0.33 09/21/17 14:15
2,4-Dimethylphenol mg/kg ND 0.33 09/21/17 14:15
2,4-Dinitrophenol mg/kg ND 1.7 09/21/17 14:15
2,4-Dinitrotoluene mg/kg ND 0.33 09/21/17 14:15
2,6-Dinitrotoluene mg/kg ND 0.33 09/21/17 14:15
2-Chloronaphthalene mg/kg ND 0.33 09/21/17 14:15
2-Chlorophenol mg/kg ND 0.33 09/21/17 14:15
2-Methylnaphthalene mg/kg ND 0.33 09/21/17 14:15
2-Methylphenol(o-Cresol)mg/kg ND 0.33 09/21/17 14:15
2-Nitroaniline mg/kg ND 1.7 09/21/17 14:15
2-Nitrophenol mg/kg ND 0.33 09/21/17 14:15
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 09/21/17 14:15
3,3'-Dichlorobenzidine mg/kg ND 1.7 09/21/17 14:15
3-Nitroaniline mg/kg ND 1.7 09/21/17 14:15
4,6-Dinitro-2-methylphenol mg/kg ND 0.67 09/21/17 14:15
4-Bromophenylphenyl ether mg/kg ND 0.33 09/21/17 14:15
4-Chloro-3-methylphenol mg/kg ND 0.67 09/21/17 14:15
4-Chloroaniline mg/kg ND 1.7 09/21/17 14:15
4-Chlorophenylphenyl ether mg/kg ND 0.33 09/21/17 14:15
4-Nitroaniline mg/kg ND 0.67 09/21/17 14:15
4-Nitrophenol mg/kg ND 1.7 09/21/17 14:15
Acenaphthene mg/kg ND 0.33 09/21/17 14:15
Acenaphthylene mg/kg ND 0.33 09/21/17 14:15
Aniline mg/kg ND 0.33 09/21/17 14:15
Anthracene mg/kg ND 0.33 09/21/17 14:15
Benzo(a)anthracene mg/kg ND 0.33 09/21/17 14:15
Benzo(a)pyrene mg/kg ND 0.33 09/21/17 14:15
Benzo(b)fluoranthene mg/kg ND 0.33 09/21/17 14:15
Benzo(g,h,i)perylene mg/kg ND 0.33 09/21/17 14:15
Benzo(k)fluoranthene mg/kg ND 0.33 09/21/17 14:15
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 137 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2098221
Associated Lab Samples:92355949001, 92355949002, 92355949003, 92355949004, 92355949005, 92355949006, 92355949007,
92355949008, 92355949009, 92355949010, 92355949011, 92355949012, 92355949013, 92355949014,
92355949015, 92355949016, 92355949017, 92355949018, 92355949019, 92355949020
Matrix:Solid
Analyzed
Benzoic Acid mg/kg ND 1.7 09/21/17 14:15
Benzyl alcohol mg/kg ND 0.67 09/21/17 14:15
bis(2-Chloroethoxy)methane mg/kg ND 0.33 09/21/17 14:15
bis(2-Chloroethyl) ether mg/kg ND 0.33 09/21/17 14:15
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 09/21/17 14:15
Butylbenzylphthalate mg/kg ND 0.33 09/21/17 14:15
Chrysene mg/kg ND 0.33 09/21/17 14:15
Di-n-butylphthalate mg/kg ND 0.33 09/21/17 14:15
Di-n-octylphthalate mg/kg ND 0.33 09/21/17 14:15
Dibenz(a,h)anthracene mg/kg ND 0.33 09/21/17 14:15
Dibenzofuran mg/kg ND 0.33 09/21/17 14:15
Diethylphthalate mg/kg ND 0.33 09/21/17 14:15
Dimethylphthalate mg/kg ND 0.33 09/21/17 14:15
Fluoranthene mg/kg ND 0.33 09/21/17 14:15
Fluorene mg/kg ND 0.33 09/21/17 14:15
Hexachloro-1,3-butadiene mg/kg ND 0.33 09/21/17 14:15
Hexachlorobenzene mg/kg ND 0.33 09/21/17 14:15
Hexachlorocyclopentadiene mg/kg ND 0.33 09/21/17 14:15
Hexachloroethane mg/kg ND 0.33 09/21/17 14:15
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 09/21/17 14:15
Isophorone mg/kg ND 0.33 09/21/17 14:15
N-Nitroso-di-n-propylamine mg/kg ND 0.33 09/21/17 14:15
N-Nitrosodimethylamine mg/kg ND 0.33 09/21/17 14:15
N-Nitrosodiphenylamine mg/kg ND 0.33 09/21/17 14:15
Naphthalene mg/kg ND 0.33 09/21/17 14:15
Nitrobenzene mg/kg ND 0.33 09/21/17 14:15
Pentachlorophenol mg/kg ND 1.7 09/21/17 14:15
Phenanthrene mg/kg ND 0.33 09/21/17 14:15
Phenol mg/kg ND 0.33 09/21/17 14:15
Pyrene mg/kg ND 0.33 09/21/17 14:15
2,4,6-Tribromophenol (S)%77 27-110 09/21/17 14:15
2-Fluorobiphenyl (S)%73 30-110 09/21/17 14:15
2-Fluorophenol (S)%69 13-110 09/21/17 14:15
Nitrobenzene-d5 (S)%70 23-110 09/21/17 14:15
Phenol-d6 (S)%71 22-110 09/21/17 14:15
Terphenyl-d14 (S)%85 28-110 09/21/17 14:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2098222LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.41.7 82 36-120
1,2-Dichlorobenzene mg/kg 1.31.7 77 41-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 138 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2098222LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichlorobenzene mg/kg 1.31.7 77 66-120
1,4-Dichlorobenzene mg/kg 1.31.7 77 42-120
1-Methylnaphthalene mg/kg 1.41.7 84 40-120
2,2'-Oxybis(1-chloropropane)mg/kg 1.11.7 67 17-120
2,4,5-Trichlorophenol mg/kg 1.51.7 91 37-120
2,4,6-Trichlorophenol mg/kg 1.41.7 84 40-120
2,4-Dichlorophenol mg/kg 1.41.7 84 33-120
2,4-Dimethylphenol mg/kg 1.51.7 88 36-120
2,4-Dinitrophenol mg/kg 7.48.4 89 22-121
2,4-Dinitrotoluene mg/kg 1.61.7 97 60-120
2,6-Dinitrotoluene mg/kg 1.61.7 93 54-120
2-Chloronaphthalene mg/kg 1.41.7 84 41-120
2-Chlorophenol mg/kg 1.31.7 80 39-120
2-Methylnaphthalene mg/kg 1.41.7 84 26-120
2-Methylphenol(o-Cresol)mg/kg 1.41.7 84 41-120
2-Nitroaniline mg/kg 3.03.3 90 45-120
2-Nitrophenol mg/kg 1.41.7 82 35-120
3&4-Methylphenol(m&p Cresol)mg/kg 1.41.7 83 35-120
3,3'-Dichlorobenzidine mg/kg 3.13.3 93 16-125
3-Nitroaniline mg/kg 3.03.3 90 45-120
4,6-Dinitro-2-methylphenol mg/kg 3.33.3 99 46-120
4-Bromophenylphenyl ether mg/kg 1.51.7 88 36-120
4-Chloro-3-methylphenol mg/kg 3.03.3 88 37-120
4-Chloroaniline mg/kg 2.63.3 78 35-120
4-Chlorophenylphenyl ether mg/kg 1.41.7 84 30-120
4-Nitroaniline mg/kg 3.23.3 97 48-120
4-Nitrophenol mg/kg 8.48.4 101 43-120
Acenaphthene mg/kg 1.41.7 85 46-120
Acenaphthylene mg/kg 1.51.7 87 46-120
Aniline mg/kg 1.31.7 75 33-120
Anthracene mg/kg 1.51.7 91 63-120
Benzo(a)anthracene mg/kg 1.51.7 88 61-120
Benzo(a)pyrene mg/kg 1.51.7 87 59-120
Benzo(b)fluoranthene mg/kg 1.41.7 84 55-120
Benzo(g,h,i)perylene mg/kg 1.51.7 92 57-120
Benzo(k)fluoranthene mg/kg 1.41.7 85 56-120
Benzoic Acid mg/kg 6.08.4 72 13-120
Benzyl alcohol mg/kg 2.63.3 79 34-120
bis(2-Chloroethoxy)methane mg/kg 1.51.7 88 21-120
bis(2-Chloroethyl) ether mg/kg 1.31.7 78 25-120
bis(2-Ethylhexyl)phthalate mg/kg 1.61.7 96 56-123
Butylbenzylphthalate mg/kg 1.61.7 94 57-120
Chrysene mg/kg 1.51.7 89 64-120
Di-n-butylphthalate mg/kg 1.81.7 107 58-120
Di-n-octylphthalate mg/kg 1.71.7 101 47-121
Dibenz(a,h)anthracene mg/kg 1.51.7 91 56-120
Dibenzofuran mg/kg 1.41.7 85 43-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 139 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2098222LABORATORY CONTROL SAMPLE:
LCSSpike
Diethylphthalate mg/kg 1.61.7 97 55-120
Dimethylphthalate mg/kg 1.61.7 99 54-120
Fluoranthene mg/kg 1.61.7 99 61-120
Fluorene mg/kg 1.51.7 89 51-120
Hexachloro-1,3-butadiene mg/kg 1.41.7 82 22-120
Hexachlorobenzene mg/kg 1.51.7 90 53-120
Hexachlorocyclopentadiene mg/kg 1.61.7 95 18-150
Hexachloroethane mg/kg 1.31.7 77 39-120
Indeno(1,2,3-cd)pyrene mg/kg 1.51.7 91 58-120
Isophorone mg/kg 1.51.7 89 38-120
N-Nitroso-di-n-propylamine mg/kg 1.41.7 86 30-120
N-Nitrosodimethylamine mg/kg 1.31.7 79 32-120
N-Nitrosodiphenylamine mg/kg 1.51.7 87 50-120
Naphthalene mg/kg 1.41.7 81 38-120
Nitrobenzene mg/kg 1.41.7 83 37-120
Pentachlorophenol mg/kg 3.23.3 94 10-120
Phenanthrene mg/kg 1.51.7 90 62-120
Phenol mg/kg 1.41.7 81 37-120
Pyrene mg/kg 1.41.7 85 63-120
2,4,6-Tribromophenol (S)%95 27-110
2-Fluorobiphenyl (S)%81 30-110
2-Fluorophenol (S)%79 13-110
Nitrobenzene-d5 (S)%79 23-110
Phenol-d6 (S)%80 22-110
Terphenyl-d14 (S)%85 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2098223MATRIX SPIKE SAMPLE:
MSSpike
Result
92355949001
1,2,4-Trichlorobenzene mg/kg 0.632.2 29 18-119ND
1,2-Dichlorobenzene mg/kg 0.64 M12.2 29 50-110ND
1,3-Dichlorobenzene mg/kg 0.642.2 29 27-110ND
1,4-Dichlorobenzene mg/kg 0.662.2 30 28-110ND
1-Methylnaphthalene mg/kg 0.772.2 35 24-116ND
2,2'-Oxybis(1-chloropropane)mg/kg ND M12.2 19 50-150ND
2,4,5-Trichlorophenol mg/kg 1.42.2 65 28-110ND
2,4,6-Trichlorophenol mg/kg 1.22.2 53 17-117ND
2,4-Dichlorophenol mg/kg 0.682.2 31 21-128ND
2,4-Dimethylphenol mg/kg 0.762.2 35 10-120ND
2,4-Dinitrophenol mg/kg ND M111010-107ND
2,4-Dinitrotoluene mg/kg 1.82.2 84 36-109ND
2,6-Dinitrotoluene mg/kg 1.82.2 80 32-110ND
2-Chloronaphthalene mg/kg 0.922.2 42 30-107ND
2-Chlorophenol mg/kg 0.592.2 27 14-106ND
2-Methylnaphthalene mg/kg 0.752.2 34 10-135ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
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Huntersville, NC 28078
[phone]
Page 140 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2098223MATRIX SPIKE SAMPLE:
MSSpike
Result
92355949001
2-Methylphenol(o-Cresol)mg/kg 0.652.2 30 10-124ND
2-Nitroaniline mg/kg 3.14.3 72 26-116ND
2-Nitrophenol mg/kg 0.632.2 29 28-103ND
3&4-Methylphenol(m&p Cresol)mg/kg 0.682.2 31 10-109ND
3,3'-Dichlorobenzidine mg/kg 3.74.3 81 10-150ND
3-Nitroaniline mg/kg 3.54.3 80 22-110ND
4,6-Dinitro-2-methylphenol mg/kg 1.54.3 35 13-121ND
4-Bromophenylphenyl ether mg/kg 1.72.2 76 31-109ND
4-Chloro-3-methylphenol mg/kg 2.54.3 58 13-128ND
4-Chloroaniline mg/kg 1.6J4.3 36 18-102ND
4-Chlorophenylphenyl ether mg/kg 1.42.2 66 29-112ND
4-Nitroaniline mg/kg 3.74.3 85 16-111ND
4-Nitrophenol mg/kg 4.811 43 14-135ND
Acenaphthene mg/kg 1.22.2 56 26-114ND
Acenaphthylene mg/kg 1.22.2 56 32-108ND
Aniline mg/kg 0.602.2 27 10-107ND
Anthracene mg/kg 1.82.2 83 32-111ND
Benzo(a)anthracene mg/kg 1.92.2 78 25-117ND
Benzo(a)pyrene mg/kg 1.92.2 81 25-106ND
Benzo(b)fluoranthene mg/kg 1.92.2 78 24-110ND
Benzo(g,h,i)perylene mg/kg 2.02.2 81 19-112ND
Benzo(k)fluoranthene mg/kg 1.92.2 77 24-114ND
Benzoic Acid mg/kg ND M111010-110ND
Benzyl alcohol mg/kg 1.24.3 28 24-106ND
bis(2-Chloroethoxy)methane mg/kg 0.692.2 32 13-119ND
bis(2-Chloroethyl) ether mg/kg 0.582.2 27 10-134ND
bis(2-Ethylhexyl)phthalate mg/kg 1.92.2 84 10-125ND
Butylbenzylphthalate mg/kg 1.92.2 83 18-110ND
Chrysene mg/kg 1.92.2 80 30-110ND
Di-n-butylphthalate mg/kg 2.12.2 96 19-112ND
Di-n-octylphthalate mg/kg 2.02.2 89 17-105ND
Dibenz(a,h)anthracene mg/kg 1.92.2 84 23-111ND
Dibenzofuran mg/kg 1.42.2 62 35-103ND
Diethylphthalate mg/kg 1.92.2 86 27-113ND
Dimethylphthalate mg/kg 1.82.2 83 26-111ND
Fluoranthene mg/kg 2.22.2 92 33-109ND
Fluorene mg/kg 1.52.2 70 32-113ND
Hexachloro-1,3-butadiene mg/kg 0.602.2 27 16-116ND
Hexachlorobenzene mg/kg 1.82.2 81 27-120ND
Hexachlorocyclopentadiene mg/kg 0.642.2 29 10-108ND
Hexachloroethane mg/kg 0.582.2 27 10-117ND
Indeno(1,2,3-cd)pyrene mg/kg 1.92.2 81 10-122ND
Isophorone mg/kg 0.952.2 44 28-114ND
N-Nitroso-di-n-propylamine mg/kg 0.752.2 34 27-113ND
N-Nitrosodimethylamine mg/kg 0.632.2 29 10-109ND
N-Nitrosodiphenylamine mg/kg 1.72.2 78 10-128ND
Naphthalene mg/kg 0.672.2 31 25-110ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 141 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2098223MATRIX SPIKE SAMPLE:
MSSpike
Result
92355949001
Nitrobenzene mg/kg 0.662.2 30 18-114ND
Pentachlorophenol mg/kg 2.74.3 60 10-122ND
Phenanthrene mg/kg 1.92.2 82 30-114ND
Phenol mg/kg 0.642.2 29 11-102ND
Pyrene mg/kg 2.12.2 86 25-116ND
2,4,6-Tribromophenol (S)%73 27-110
2-Fluorobiphenyl (S)%36 30-110
2-Fluorophenol (S)%24 13-110
Nitrobenzene-d5 (S)%27 23-110
Phenol-d6 (S)%25 22-110
Terphenyl-d14 (S)%79 28-110
Parameter Units
Dup
Result QualifiersRPDResult
92355949001
2098224SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
1-Methylnaphthalene mg/kg 0.61ND
2,2'-Oxybis(1-chloropropane)mg/kg NDND
2,4,5-Trichlorophenol mg/kg NDND
2,4,6-Trichlorophenol mg/kg NDND
2,4-Dichlorophenol mg/kg NDND
2,4-Dimethylphenol mg/kg NDND
2,4-Dinitrophenol mg/kg NDND
2,4-Dinitrotoluene mg/kg NDND
2,6-Dinitrotoluene mg/kg NDND
2-Chloronaphthalene mg/kg NDND
2-Chlorophenol mg/kg NDND
2-Methylnaphthalene mg/kg 1.3ND
2-Methylphenol(o-Cresol)mg/kg NDND
2-Nitroaniline mg/kg NDND
2-Nitrophenol mg/kg NDND
3&4-Methylphenol(m&p Cresol)mg/kg NDND
3,3'-Dichlorobenzidine mg/kg .13JND
3-Nitroaniline mg/kg NDND
4,6-Dinitro-2-methylphenol mg/kg NDND
4-Bromophenylphenyl ether mg/kg NDND
4-Chloro-3-methylphenol mg/kg NDND
4-Chloroaniline mg/kg NDND
4-Chlorophenylphenyl ether mg/kg NDND
4-Nitroaniline mg/kg NDND
4-Nitrophenol mg/kg NDND
Acenaphthene mg/kg NDND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
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Huntersville, NC 28078
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Page 142 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92355949001
2098224SAMPLE DUPLICATE:
Acenaphthylene mg/kg NDND
Aniline mg/kg NDND
Anthracene mg/kg NDND
Benzo(a)anthracene mg/kg .11JND
Benzo(a)pyrene mg/kg .1JND
Benzo(b)fluoranthene mg/kg .11JND
Benzo(g,h,i)perylene mg/kg NDND
Benzo(k)fluoranthene mg/kg .09JND
Benzoic Acid mg/kg NDND
Benzyl alcohol mg/kg NDND
bis(2-Chloroethoxy)methane mg/kg NDND
bis(2-Chloroethyl) ether mg/kg NDND
bis(2-Ethylhexyl)phthalate mg/kg NDND
Butylbenzylphthalate mg/kg NDND
Chrysene mg/kg .12JND
Di-n-butylphthalate mg/kg NDND
Di-n-octylphthalate mg/kg NDND
Dibenz(a,h)anthracene mg/kg NDND
Dibenzofuran mg/kg NDND
Diethylphthalate mg/kg NDND
Dimethylphthalate mg/kg NDND
Fluoranthene mg/kg NDND
Fluorene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg NDND
Hexachlorobenzene mg/kg NDND
Hexachlorocyclopentadiene mg/kg NDND
Hexachloroethane mg/kg NDND
Indeno(1,2,3-cd)pyrene mg/kg NDND
Isophorone mg/kg NDND
N-Nitroso-di-n-propylamine mg/kg NDND
N-Nitrosodimethylamine mg/kg NDND
N-Nitrosodiphenylamine mg/kg NDND
Naphthalene mg/kg 0.94ND
Nitrobenzene mg/kg NDND
Pentachlorophenol mg/kg NDND
Phenanthrene mg/kg NDND
Phenol mg/kg NDND
Pyrene mg/kg NDND
2,4,6-Tribromophenol (S)%50 2263
2-Fluorobiphenyl (S)%37 3653
2-Fluorophenol (S)%47 851
Nitrobenzene-d5 (S)%42 3057
Phenol-d6 (S)%45 1854
Terphenyl-d14 (S)%68 1277
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 143 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
378650
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:92355949021, 92355949022, 92355949024
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2098236
Associated Lab Samples:92355949021, 92355949022, 92355949024
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene mg/kg ND 0.33 09/21/17 10:12
1,2-Dichlorobenzene mg/kg ND 0.33 09/21/17 10:12
1,3-Dichlorobenzene mg/kg ND 0.33 09/21/17 10:12
1,4-Dichlorobenzene mg/kg ND 0.33 09/21/17 10:12
1-Methylnaphthalene mg/kg ND 0.33 09/21/17 10:12
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 09/21/17 10:12
2,4,5-Trichlorophenol mg/kg ND 0.33 09/21/17 10:12
2,4,6-Trichlorophenol mg/kg ND 0.33 09/21/17 10:12
2,4-Dichlorophenol mg/kg ND 0.33 09/21/17 10:12
2,4-Dimethylphenol mg/kg ND 0.33 09/21/17 10:12
2,4-Dinitrophenol mg/kg ND 1.7 09/21/17 10:12
2,4-Dinitrotoluene mg/kg ND 0.33 09/21/17 10:12
2,6-Dinitrotoluene mg/kg ND 0.33 09/21/17 10:12
2-Chloronaphthalene mg/kg ND 0.33 09/21/17 10:12
2-Chlorophenol mg/kg ND 0.33 09/21/17 10:12
2-Methylnaphthalene mg/kg ND 0.33 09/21/17 10:12
2-Methylphenol(o-Cresol)mg/kg ND 0.33 09/21/17 10:12
2-Nitroaniline mg/kg ND 1.7 09/21/17 10:12
2-Nitrophenol mg/kg ND 0.33 09/21/17 10:12
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 09/21/17 10:12
3,3'-Dichlorobenzidine mg/kg ND 1.7 09/21/17 10:12
3-Nitroaniline mg/kg ND 1.7 09/21/17 10:12
4,6-Dinitro-2-methylphenol mg/kg ND 0.66 09/21/17 10:12
4-Bromophenylphenyl ether mg/kg ND 0.33 09/21/17 10:12
4-Chloro-3-methylphenol mg/kg ND 0.66 09/21/17 10:12
4-Chloroaniline mg/kg ND 1.7 09/21/17 10:12
4-Chlorophenylphenyl ether mg/kg ND 0.33 09/21/17 10:12
4-Nitroaniline mg/kg ND 0.66 09/21/17 10:12
4-Nitrophenol mg/kg ND 1.7 09/21/17 10:12
Acenaphthene mg/kg ND 0.33 09/21/17 10:12
Acenaphthylene mg/kg ND 0.33 09/21/17 10:12
Aniline mg/kg ND 0.33 09/21/17 10:12
Anthracene mg/kg ND 0.33 09/21/17 10:12
Benzo(a)anthracene mg/kg ND 0.33 09/21/17 10:12
Benzo(a)pyrene mg/kg ND 0.33 09/21/17 10:12
Benzo(b)fluoranthene mg/kg ND 0.33 09/21/17 10:12
Benzo(g,h,i)perylene mg/kg ND 0.33 09/21/17 10:12
Benzo(k)fluoranthene mg/kg ND 0.33 09/21/17 10:12
Benzoic Acid mg/kg ND 1.7 09/21/17 10:12
Benzyl alcohol mg/kg ND 0.66 09/21/17 10:12
bis(2-Chloroethoxy)methane mg/kg ND 0.33 09/21/17 10:12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 144 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2098236
Associated Lab Samples:92355949021, 92355949022, 92355949024
Matrix:Solid
Analyzed
bis(2-Chloroethyl) ether mg/kg ND 0.33 09/21/17 10:12
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 09/21/17 10:12
Butylbenzylphthalate mg/kg ND 0.33 09/21/17 10:12
Chrysene mg/kg ND 0.33 09/21/17 10:12
Di-n-butylphthalate mg/kg ND 0.33 09/21/17 10:12
Di-n-octylphthalate mg/kg ND 0.33 09/21/17 10:12
Dibenz(a,h)anthracene mg/kg ND 0.33 09/21/17 10:12
Dibenzofuran mg/kg ND 0.33 09/21/17 10:12
Diethylphthalate mg/kg ND 0.33 09/21/17 10:12
Dimethylphthalate mg/kg ND 0.33 09/21/17 10:12
Fluoranthene mg/kg ND 0.33 09/21/17 10:12
Fluorene mg/kg ND 0.33 09/21/17 10:12
Hexachloro-1,3-butadiene mg/kg ND 0.33 09/21/17 10:12
Hexachlorobenzene mg/kg ND 0.33 09/21/17 10:12
Hexachlorocyclopentadiene mg/kg ND 0.33 09/21/17 10:12
Hexachloroethane mg/kg ND 0.33 09/21/17 10:12
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 09/21/17 10:12
Isophorone mg/kg ND 0.33 09/21/17 10:12
N-Nitroso-di-n-propylamine mg/kg ND 0.33 09/21/17 10:12
N-Nitrosodimethylamine mg/kg ND 0.33 09/21/17 10:12
N-Nitrosodiphenylamine mg/kg ND 0.33 09/21/17 10:12
Naphthalene mg/kg ND 0.33 09/21/17 10:12
Nitrobenzene mg/kg ND 0.33 09/21/17 10:12
Pentachlorophenol mg/kg ND 1.7 09/21/17 10:12
Phenanthrene mg/kg ND 0.33 09/21/17 10:12
Phenol mg/kg ND 0.33 09/21/17 10:12
Pyrene mg/kg ND 0.33 09/21/17 10:12
2,4,6-Tribromophenol (S)%64 27-110 09/21/17 10:12
2-Fluorobiphenyl (S)%68 30-110 09/21/17 10:12
2-Fluorophenol (S)%62 13-110 09/21/17 10:12
Nitrobenzene-d5 (S)%78 23-110 09/21/17 10:12
Phenol-d6 (S)%58 22-110 09/21/17 10:12
Terphenyl-d14 (S)%78 28-110 09/21/17 10:12
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2098237LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.21.7 72 36-120
1,2-Dichlorobenzene mg/kg 1.11.7 65 41-120
1,3-Dichlorobenzene mg/kg 1.1 L21.7 63 66-120
1,4-Dichlorobenzene mg/kg 1.11.7 65 42-120
1-Methylnaphthalene mg/kg 1.11.7 68 40-120
2,2'-Oxybis(1-chloropropane)mg/kg 0.801.7 48 17-120
2,4,5-Trichlorophenol mg/kg 1.41.7 83 37-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 145 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2098237LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol mg/kg 1.31.7 79 40-120
2,4-Dichlorophenol mg/kg 1.11.7 68 33-120
2,4-Dimethylphenol mg/kg 1.21.7 72 36-120
2,4-Dinitrophenol mg/kg 5.98.3 71 22-121
2,4-Dinitrotoluene mg/kg 1.41.7 84 60-120
2,6-Dinitrotoluene mg/kg 1.31.7 81 54-120
2-Chloronaphthalene mg/kg 1.21.7 71 41-120
2-Chlorophenol mg/kg 1.11.7 64 39-120
2-Methylnaphthalene mg/kg 1.11.7 68 26-120
2-Methylphenol(o-Cresol)mg/kg 1.21.7 74 41-120
2-Nitroaniline mg/kg 2.43.3 73 45-120
2-Nitrophenol mg/kg 1.21.7 72 35-120
3&4-Methylphenol(m&p Cresol)mg/kg 1.11.7 67 35-120
3,3'-Dichlorobenzidine mg/kg 2.13.3 65 16-125
3-Nitroaniline mg/kg 2.23.3 67 45-120
4,6-Dinitro-2-methylphenol mg/kg 3.13.3 93 46-120
4-Bromophenylphenyl ether mg/kg 1.41.7 83 36-120
4-Chloro-3-methylphenol mg/kg 2.63.3 78 37-120
4-Chloroaniline mg/kg 2.13.3 62 35-120
4-Chlorophenylphenyl ether mg/kg 1.21.7 75 30-120
4-Nitroaniline mg/kg 2.23.3 66 48-120
4-Nitrophenol mg/kg 6.88.3 82 43-120
Acenaphthene mg/kg 1.21.7 70 46-120
Acenaphthylene mg/kg 1.21.7 70 46-120
Aniline mg/kg 0.931.7 56 33-120
Anthracene mg/kg 1.21.7 74 63-120
Benzo(a)anthracene mg/kg 1.31.7 78 61-120
Benzo(a)pyrene mg/kg 1.31.7 78 59-120
Benzo(b)fluoranthene mg/kg 1.31.7 77 55-120
Benzo(g,h,i)perylene mg/kg 1.21.7 70 57-120
Benzo(k)fluoranthene mg/kg 1.31.7 79 56-120
Benzoic Acid mg/kg 4.88.3 58 13-120
Benzyl alcohol mg/kg 2.03.3 61 34-120
bis(2-Chloroethoxy)methane mg/kg 1.21.7 72 21-120
bis(2-Chloroethyl) ether mg/kg 1.11.7 64 25-120
bis(2-Ethylhexyl)phthalate mg/kg 1.41.7 82 56-123
Butylbenzylphthalate mg/kg 1.41.7 83 57-120
Chrysene mg/kg 1.31.7 77 64-120
Di-n-butylphthalate mg/kg 1.41.7 85 58-120
Di-n-octylphthalate mg/kg 1.31.7 76 47-121
Dibenz(a,h)anthracene mg/kg 1.21.7 72 56-120
Dibenzofuran mg/kg 1.21.7 70 43-120
Diethylphthalate mg/kg 1.41.7 85 55-120
Dimethylphthalate mg/kg 1.41.7 83 54-120
Fluoranthene mg/kg 1.31.7 77 61-120
Fluorene mg/kg 1.21.7 75 51-120
Hexachloro-1,3-butadiene mg/kg 1.31.7 78 22-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 146 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2098237LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene mg/kg 1.21.7 75 53-120
Hexachlorocyclopentadiene mg/kg 0.981.7 59 18-150
Hexachloroethane mg/kg 1.11.7 66 39-120
Indeno(1,2,3-cd)pyrene mg/kg 1.21.7 71 58-120
Isophorone mg/kg 1.31.7 79 38-120
N-Nitroso-di-n-propylamine mg/kg 1.21.7 70 30-120
N-Nitrosodimethylamine mg/kg 1.21.7 71 32-120
N-Nitrosodiphenylamine mg/kg 1.21.7 72 50-120
Naphthalene mg/kg 1.11.7 68 38-120
Nitrobenzene mg/kg 1.21.7 73 37-120
Pentachlorophenol mg/kg 2.63.3 79 10-120
Phenanthrene mg/kg 1.21.7 72 62-120
Phenol mg/kg 1.21.7 71 37-120
Pyrene mg/kg 1.21.7 73 63-120
2,4,6-Tribromophenol (S)%79 27-110
2-Fluorobiphenyl (S)%66 30-110
2-Fluorophenol (S)%63 13-110
Nitrobenzene-d5 (S)%72 23-110
Phenol-d6 (S)%63 22-110
Terphenyl-d14 (S)%74 28-110
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2098238MATRIX SPIKE SAMPLE:
MSSpike
Result
92355949021
1,2,4-Trichlorobenzene mg/kg 0.762.2 35 18-119ND
1,2-Dichlorobenzene mg/kg 0.78 M12.2 36 50-110ND
1,3-Dichlorobenzene mg/kg 0.782.2 36 27-110ND
1,4-Dichlorobenzene mg/kg 0.762.2 35 28-110ND
1-Methylnaphthalene mg/kg 0.952.2 44 24-116ND
2,2'-Oxybis(1-chloropropane)mg/kg 0.63 M12.2 29 50-150ND
2,4,5-Trichlorophenol mg/kg 1.42.2 67 28-110ND
2,4,6-Trichlorophenol mg/kg 1.22.2 57 17-117ND
2,4-Dichlorophenol mg/kg 1.02.2 47 21-128ND
2,4-Dimethylphenol mg/kg 0.972.2 45 10-120ND
2,4-Dinitrophenol mg/kg 5.610.8 52 10-107ND
2,4-Dinitrotoluene mg/kg 1.42.2 66 36-109ND
2,6-Dinitrotoluene mg/kg 1.32.2 61 32-110ND
2-Chloronaphthalene mg/kg 0.992.2 46 30-107ND
2-Chlorophenol mg/kg 0.782.2 36 14-106ND
2-Methylnaphthalene mg/kg 0.922.2 43 10-135ND
2-Methylphenol(o-Cresol)mg/kg 0.912.2 42 10-124ND
2-Nitroaniline mg/kg 2.54.3 57 26-116ND
2-Nitrophenol mg/kg 0.742.2 34 28-103ND
3&4-Methylphenol(m&p Cresol)mg/kg 0.932.2 43 10-109ND
3,3'-Dichlorobenzidine mg/kg 2.44.3 55 10-150ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 147 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2098238MATRIX SPIKE SAMPLE:
MSSpike
Result
92355949021
3-Nitroaniline mg/kg 2.64.3 60 22-110ND
4,6-Dinitro-2-methylphenol mg/kg 2.84.3 65 13-121ND
4-Bromophenylphenyl ether mg/kg 1.32.2 59 31-109ND
4-Chloro-3-methylphenol mg/kg 2.74.3 63 13-128ND
4-Chloroaniline mg/kg 1.8J4.3 41 18-102ND
4-Chlorophenylphenyl ether mg/kg 1.22.2 57 29-112ND
4-Nitroaniline mg/kg 2.84.3 66 16-111ND
4-Nitrophenol mg/kg 6.510.8 61 14-135ND
Acenaphthene mg/kg 1.22.2 54 26-114ND
Acenaphthylene mg/kg 1.22.2 53 32-108ND
Aniline mg/kg 0.642.2 30 10-107ND
Anthracene mg/kg 1.42.2 65 32-111ND
Benzo(a)anthracene mg/kg 1.32.2 62 25-117ND
Benzo(a)pyrene mg/kg 1.32.2 58 25-106ND
Benzo(b)fluoranthene mg/kg 1.22.2 57 24-110ND
Benzo(g,h,i)perylene mg/kg 1.32.2 59 19-112ND
Benzo(k)fluoranthene mg/kg 1.22.2 56 24-114ND
Benzoic Acid mg/kg 1.8J10.8 16 10-110ND
Benzyl alcohol mg/kg 1.64.3 36 24-106ND
bis(2-Chloroethoxy)methane mg/kg 0.792.2 37 13-119ND
bis(2-Chloroethyl) ether mg/kg 0.742.2 34 10-134ND
bis(2-Ethylhexyl)phthalate mg/kg 1.42.2 66 10-125ND
Butylbenzylphthalate mg/kg 1.42.2 66 18-110ND
Chrysene mg/kg 1.42.2 63 30-110ND
Di-n-butylphthalate mg/kg 1.52.2 72 19-112ND
Di-n-octylphthalate mg/kg 1.52.2 68 17-105ND
Dibenz(a,h)anthracene mg/kg 1.32.2 61 23-111ND
Dibenzofuran mg/kg 1.22.2 57 35-103ND
Diethylphthalate mg/kg 1.42.2 67 27-113ND
Dimethylphthalate mg/kg 1.32.2 62 26-111ND
Fluoranthene mg/kg 1.62.2 73 33-109ND
Fluorene mg/kg 1.32.2 60 32-113ND
Hexachloro-1,3-butadiene mg/kg 0.732.2 34 16-116ND
Hexachlorobenzene mg/kg 1.32.2 61 27-120ND
Hexachlorocyclopentadiene mg/kg 0.752.2 35 10-108ND
Hexachloroethane mg/kg 0.732.2 34 10-117ND
Indeno(1,2,3-cd)pyrene mg/kg 1.32.2 59 10-122ND
Isophorone mg/kg 0.892.2 41 28-114ND
N-Nitroso-di-n-propylamine mg/kg 0.842.2 39 27-113ND
N-Nitrosodimethylamine mg/kg 0.712.2 33 10-109ND
N-Nitrosodiphenylamine mg/kg 1.32.2 61 10-128ND
Naphthalene mg/kg 0.832.2 39 25-110ND
Nitrobenzene mg/kg 0.752.2 35 18-114ND
Pentachlorophenol mg/kg 2.64.3 61 10-122ND
Phenanthrene mg/kg 1.42.2 64 30-114ND
Phenol mg/kg 0.792.2 37 11-102ND
Pyrene mg/kg 1.62.2 72 25-116ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 148 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2098238MATRIX SPIKE SAMPLE:
MSSpike
Result
92355949021
2,4,6-Tribromophenol (S)%62 27-110
2-Fluorobiphenyl (S)%40 30-110
2-Fluorophenol (S)%33 13-110
Nitrobenzene-d5 (S)%32 23-110
Phenol-d6 (S)%36 22-110
Terphenyl-d14 (S)%62 28-110
Parameter Units
Dup
Result QualifiersRPDResult
92355949021
2098239SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene mg/kg NDND
1,2-Dichlorobenzene mg/kg NDND
1,3-Dichlorobenzene mg/kg NDND
1,4-Dichlorobenzene mg/kg NDND
1-Methylnaphthalene mg/kg NDND
2,2'-Oxybis(1-chloropropane)mg/kg NDND
2,4,5-Trichlorophenol mg/kg NDND
2,4,6-Trichlorophenol mg/kg NDND
2,4-Dichlorophenol mg/kg NDND
2,4-Dimethylphenol mg/kg NDND
2,4-Dinitrophenol mg/kg NDND
2,4-Dinitrotoluene mg/kg NDND
2,6-Dinitrotoluene mg/kg NDND
2-Chloronaphthalene mg/kg NDND
2-Chlorophenol mg/kg NDND
2-Methylnaphthalene mg/kg NDND
2-Methylphenol(o-Cresol)mg/kg NDND
2-Nitroaniline mg/kg NDND
2-Nitrophenol mg/kg NDND
3&4-Methylphenol(m&p Cresol)mg/kg NDND
3,3'-Dichlorobenzidine mg/kg NDND
3-Nitroaniline mg/kg NDND
4,6-Dinitro-2-methylphenol mg/kg NDND
4-Bromophenylphenyl ether mg/kg NDND
4-Chloro-3-methylphenol mg/kg NDND
4-Chloroaniline mg/kg NDND
4-Chlorophenylphenyl ether mg/kg NDND
4-Nitroaniline mg/kg NDND
4-Nitrophenol mg/kg NDND
Acenaphthene mg/kg NDND
Acenaphthylene mg/kg NDND
Aniline mg/kg NDND
Anthracene mg/kg NDND
Benzo(a)anthracene mg/kg NDND
Benzo(a)pyrene mg/kg NDND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
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Huntersville, NC 28078
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Page 149 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92355949021
2098239SAMPLE DUPLICATE:
Benzo(b)fluoranthene mg/kg NDND
Benzo(g,h,i)perylene mg/kg NDND
Benzo(k)fluoranthene mg/kg NDND
Benzoic Acid mg/kg NDND
Benzyl alcohol mg/kg NDND
bis(2-Chloroethoxy)methane mg/kg NDND
bis(2-Chloroethyl) ether mg/kg NDND
bis(2-Ethylhexyl)phthalate mg/kg NDND
Butylbenzylphthalate mg/kg NDND
Chrysene mg/kg .071JND
Di-n-butylphthalate mg/kg NDND
Di-n-octylphthalate mg/kg NDND
Dibenz(a,h)anthracene mg/kg NDND
Dibenzofuran mg/kg NDND
Diethylphthalate mg/kg NDND
Dimethylphthalate mg/kg NDND
Fluoranthene mg/kg NDND
Fluorene mg/kg NDND
Hexachloro-1,3-butadiene mg/kg NDND
Hexachlorobenzene mg/kg NDND
Hexachlorocyclopentadiene mg/kg NDND
Hexachloroethane mg/kg NDND
Indeno(1,2,3-cd)pyrene mg/kg NDND
Isophorone mg/kg NDND
N-Nitroso-di-n-propylamine mg/kg NDND
N-Nitrosodimethylamine mg/kg NDND
N-Nitrosodiphenylamine mg/kg NDND
Naphthalene mg/kg NDND
Nitrobenzene mg/kg NDND
Pentachlorophenol mg/kg NDND
Phenanthrene mg/kg NDND
Phenol mg/kg NDND
Pyrene mg/kg NDND
2,4,6-Tribromophenol (S)%42 2253
2-Fluorobiphenyl (S)%26 S04841
2-Fluorophenol (S)%30 3743
Nitrobenzene-d5 (S)%21 S06842
Phenol-d6 (S)%31 3142
Terphenyl-d14 (S)%43 3661
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 150 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
378862
EPA 3546
EPA 8270
8270 Solid MSSV Microwave
Associated Lab Samples:92355949023
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2099620
Associated Lab Samples:92355949023
Matrix:Solid
Analyzed
1,2,4-Trichlorobenzene mg/kg ND 0.33 09/22/17 11:38
1,2-Dichlorobenzene mg/kg ND 0.33 09/22/17 11:38
1,3-Dichlorobenzene mg/kg ND 0.33 09/22/17 11:38
1,4-Dichlorobenzene mg/kg ND 0.33 09/22/17 11:38
1-Methylnaphthalene mg/kg ND 0.33 09/22/17 11:38
2,2'-Oxybis(1-chloropropane)mg/kg ND 0.33 09/22/17 11:38
2,4,5-Trichlorophenol mg/kg ND 0.33 09/22/17 11:38
2,4,6-Trichlorophenol mg/kg ND 0.33 09/22/17 11:38
2,4-Dichlorophenol mg/kg ND 0.33 09/22/17 11:38
2,4-Dimethylphenol mg/kg ND 0.33 09/22/17 11:38
2,4-Dinitrophenol mg/kg ND 1.7 09/22/17 11:38
2,4-Dinitrotoluene mg/kg ND 0.33 09/22/17 11:38
2,6-Dinitrotoluene mg/kg ND 0.33 09/22/17 11:38
2-Chloronaphthalene mg/kg ND 0.33 09/22/17 11:38
2-Chlorophenol mg/kg ND 0.33 09/22/17 11:38
2-Methylnaphthalene mg/kg ND 0.33 09/22/17 11:38
2-Methylphenol(o-Cresol)mg/kg ND 0.33 09/22/17 11:38
2-Nitroaniline mg/kg ND 1.7 09/22/17 11:38
2-Nitrophenol mg/kg ND 0.33 09/22/17 11:38
3&4-Methylphenol(m&p Cresol)mg/kg ND 0.33 09/22/17 11:38
3,3'-Dichlorobenzidine mg/kg ND 1.7 09/22/17 11:38
3-Nitroaniline mg/kg ND 1.7 09/22/17 11:38
4,6-Dinitro-2-methylphenol mg/kg ND 0.67 09/22/17 11:38
4-Bromophenylphenyl ether mg/kg ND 0.33 09/22/17 11:38
4-Chloro-3-methylphenol mg/kg ND 0.67 09/22/17 11:38
4-Chloroaniline mg/kg ND 1.7 09/22/17 11:38
4-Chlorophenylphenyl ether mg/kg ND 0.33 09/22/17 11:38
4-Nitroaniline mg/kg ND 0.67 09/22/17 11:38
4-Nitrophenol mg/kg ND 1.7 09/22/17 11:38
Acenaphthene mg/kg ND 0.33 09/22/17 11:38
Acenaphthylene mg/kg ND 0.33 09/22/17 11:38
Aniline mg/kg ND 0.33 09/22/17 11:38
Anthracene mg/kg ND 0.33 09/22/17 11:38
Benzo(a)anthracene mg/kg ND 0.33 09/22/17 11:38
Benzo(a)pyrene mg/kg ND 0.33 09/22/17 11:38
Benzo(b)fluoranthene mg/kg ND 0.33 09/22/17 11:38
Benzo(g,h,i)perylene mg/kg ND 0.33 09/22/17 11:38
Benzo(k)fluoranthene mg/kg ND 0.33 09/22/17 11:38
Benzoic Acid mg/kg ND 1.7 09/22/17 11:38
Benzyl alcohol mg/kg ND 0.67 09/22/17 11:38
bis(2-Chloroethoxy)methane mg/kg ND 0.33 09/22/17 11:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 151 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2099620
Associated Lab Samples:92355949023
Matrix:Solid
Analyzed
bis(2-Chloroethyl) ether mg/kg ND 0.33 09/22/17 11:38
bis(2-Ethylhexyl)phthalate mg/kg ND 0.33 09/22/17 11:38
Butylbenzylphthalate mg/kg ND 0.33 09/22/17 11:38
Chrysene mg/kg ND 0.33 09/22/17 11:38
Di-n-butylphthalate mg/kg ND 0.33 09/22/17 11:38
Di-n-octylphthalate mg/kg ND 0.33 09/22/17 11:38
Dibenz(a,h)anthracene mg/kg ND 0.33 09/22/17 11:38
Dibenzofuran mg/kg ND 0.33 09/22/17 11:38
Diethylphthalate mg/kg ND 0.33 09/22/17 11:38
Dimethylphthalate mg/kg ND 0.33 09/22/17 11:38
Fluoranthene mg/kg ND 0.33 09/22/17 11:38
Fluorene mg/kg ND 0.33 09/22/17 11:38
Hexachloro-1,3-butadiene mg/kg ND 0.33 09/22/17 11:38
Hexachlorobenzene mg/kg ND 0.33 09/22/17 11:38
Hexachlorocyclopentadiene mg/kg ND 0.33 09/22/17 11:38
Hexachloroethane mg/kg ND 0.33 09/22/17 11:38
Indeno(1,2,3-cd)pyrene mg/kg ND 0.33 09/22/17 11:38
Isophorone mg/kg ND 0.33 09/22/17 11:38
N-Nitroso-di-n-propylamine mg/kg ND 0.33 09/22/17 11:38
N-Nitrosodimethylamine mg/kg ND 0.33 09/22/17 11:38
N-Nitrosodiphenylamine mg/kg ND 0.33 09/22/17 11:38
Naphthalene mg/kg ND 0.33 09/22/17 11:38
Nitrobenzene mg/kg ND 0.33 09/22/17 11:38
Pentachlorophenol mg/kg ND 1.7 09/22/17 11:38
Phenanthrene mg/kg ND 0.33 09/22/17 11:38
Phenol mg/kg ND 0.33 09/22/17 11:38
Pyrene mg/kg ND 0.33 09/22/17 11:38
2,4,6-Tribromophenol (S)%83 27-110 09/22/17 11:38
2-Fluorobiphenyl (S)%71 30-110 09/22/17 11:38
2-Fluorophenol (S)%65 13-110 09/22/17 11:38
Nitrobenzene-d5 (S)%77 23-110 09/22/17 11:38
Phenol-d6 (S)%62 22-110 09/22/17 11:38
Terphenyl-d14 (S)%83 28-110 09/22/17 11:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2099621LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene mg/kg 1.31.7 79 36-120
1,2-Dichlorobenzene mg/kg 1.21.7 70 41-120
1,3-Dichlorobenzene mg/kg 1.11.7 68 66-120
1,4-Dichlorobenzene mg/kg 1.11.7 69 42-120
1-Methylnaphthalene mg/kg 1.31.7 77 40-120
2,2'-Oxybis(1-chloropropane)mg/kg 0.881.7 53 17-120
2,4,5-Trichlorophenol mg/kg 1.71.7 103 37-120
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 152 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2099621LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol mg/kg 1.61.7 96 40-120
2,4-Dichlorophenol mg/kg 1.31.7 77 33-120
2,4-Dimethylphenol mg/kg 1.31.7 81 36-120
2,4-Dinitrophenol mg/kg 8.58.3 103 22-121
2,4-Dinitrotoluene mg/kg 1.61.7 98 60-120
2,6-Dinitrotoluene mg/kg 1.61.7 95 54-120
2-Chloronaphthalene mg/kg 1.61.7 94 41-120
2-Chlorophenol mg/kg 1.11.7 69 39-120
2-Methylnaphthalene mg/kg 1.21.7 74 26-120
2-Methylphenol(o-Cresol)mg/kg 1.41.7 82 41-120
2-Nitroaniline mg/kg 2.83.3 84 45-120
2-Nitrophenol mg/kg 1.31.7 80 35-120
3&4-Methylphenol(m&p Cresol)mg/kg 2.3 L11.7 140 35-120
3,3'-Dichlorobenzidine mg/kg 2.53.3 76 16-125
3-Nitroaniline mg/kg 2.83.3 85 45-120
4,6-Dinitro-2-methylphenol mg/kg 3.93.3 116 46-120
4-Bromophenylphenyl ether mg/kg 1.51.7 87 36-120
4-Chloro-3-methylphenol mg/kg 3.03.3 91 37-120
4-Chloroaniline mg/kg 2.43.3 73 35-120
4-Chlorophenylphenyl ether mg/kg 1.41.7 86 30-120
4-Nitroaniline mg/kg 2.93.3 86 48-120
4-Nitrophenol mg/kg 9.28.3 111 43-120
Acenaphthene mg/kg 1.41.7 83 46-120
Acenaphthylene mg/kg 1.41.7 82 46-120
Aniline mg/kg 1.01.7 63 33-120
Anthracene mg/kg 1.31.7 80 63-120
Benzo(a)anthracene mg/kg 1.41.7 85 61-120
Benzo(a)pyrene mg/kg 1.41.7 85 59-120
Benzo(b)fluoranthene mg/kg 1.51.7 90 55-120
Benzo(g,h,i)perylene mg/kg 1.31.7 81 57-120
Benzo(k)fluoranthene mg/kg 1.51.7 88 56-120
Benzoic Acid mg/kg 7.18.3 85 13-120
Benzyl alcohol mg/kg 2.33.3 68 34-120
bis(2-Chloroethoxy)methane mg/kg 1.31.7 80 21-120
bis(2-Chloroethyl) ether mg/kg 1.11.7 67 25-120
bis(2-Ethylhexyl)phthalate mg/kg 1.51.7 88 56-123
Butylbenzylphthalate mg/kg 1.51.7 93 57-120
Chrysene mg/kg 1.41.7 83 64-120
Di-n-butylphthalate mg/kg 1.51.7 93 58-120
Di-n-octylphthalate mg/kg 1.41.7 86 47-121
Dibenz(a,h)anthracene mg/kg 1.41.7 82 56-120
Dibenzofuran mg/kg 1.41.7 84 43-120
Diethylphthalate mg/kg 1.61.7 95 55-120
Dimethylphthalate mg/kg 1.61.7 94 54-120
Fluoranthene mg/kg 1.41.7 87 61-120
Fluorene mg/kg 1.41.7 86 51-120
Hexachloro-1,3-butadiene mg/kg 1.41.7 86 22-120
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 153 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2099621LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene mg/kg 1.31.7 80 53-120
Hexachlorocyclopentadiene mg/kg 1.31.7 81 18-150
Hexachloroethane mg/kg 1.21.7 72 39-120
Indeno(1,2,3-cd)pyrene mg/kg 1.31.7 81 58-120
Isophorone mg/kg 1.41.7 86 38-120
N-Nitroso-di-n-propylamine mg/kg 1.31.7 78 30-120
N-Nitrosodimethylamine mg/kg 1.21.7 72 32-120
N-Nitrosodiphenylamine mg/kg 1.31.7 78 50-120
Naphthalene mg/kg 1.21.7 75 38-120
Nitrobenzene mg/kg 1.31.7 77 37-120
Pentachlorophenol mg/kg 3.23.3 97 10-120
Phenanthrene mg/kg 1.31.7 79 62-120
Phenol mg/kg 1.41.7 82 37-120
Pyrene mg/kg 1.31.7 80 63-120
2,4,6-Tribromophenol (S)%96 27-110
2-Fluorobiphenyl (S)%80 30-110
2-Fluorophenol (S)%68 13-110
Nitrobenzene-d5 (S)%78 23-110
Phenol-d6 (S)%69 22-110
Terphenyl-d14 (S)%81 28-110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 154 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
378685
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Associated Lab Samples:92355949001, 92355949002, 92355949004, 92355949005, 92355949006, 92355949007, 92355949008,
92355949009, 92355949011, 92355949012, 92355949013, 92355949014, 92355949015, 92355949016,
92355949017, 92355949018, 92355949019, 92355949020
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2098374
Associated Lab Samples:92355949001, 92355949002, 92355949004, 92355949005, 92355949006, 92355949007, 92355949008,
92355949009, 92355949011, 92355949012, 92355949013, 92355949014, 92355949015, 92355949016,
92355949017, 92355949018, 92355949019, 92355949020
Matrix:Solid
Analyzed
Aliphatic (C09-C18)mg/kg ND 10 N209/21/17 15:15
Aliphatic (C19-C36)mg/kg ND 10 N209/21/17 15:15
Aromatic (C11-C22)mg/kg ND 10 N209/21/17 15:15
2-Bromonaphthalene (S)%90 40-140 09/21/17 15:15
2-Fluorobiphenyl (S)%92 40-140 09/21/17 15:15
Nonatriacontane (S)%55 40-140 09/21/17 15:15
o-Terphenyl (S)%62 40-140 09/21/17 15:15
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2098375LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2098376
Aliphatic (C09-C18)mg/kg ND N2108140-14071ND 50
Aliphatic (C19-C36)mg/kg 12.2 N213.3 91 40-1408010.6 14 50
Aromatic (C11-C22)mg/kg 25.4 N228.3 90 40-1408724.5 3 50
2-Bromonaphthalene (S)%104 40-140105
2-Fluorobiphenyl (S)%109 40-140109
Nonatriacontane (S)%79 40-14070
o-Terphenyl (S)%92 40-14089
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 155 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
379047
MADEP EPH
MADEP EPH
MADEP EPH NC Soil
Associated Lab Samples:92355949003, 92355949010, 92355949021, 92355949022, 92355949023, 92355949024
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2100693
Associated Lab Samples:92355949003, 92355949010, 92355949021, 92355949022, 92355949023, 92355949024
Matrix:Solid
Analyzed
Aliphatic (C09-C18)mg/kg ND 10.0 N209/25/17 12:33
Aliphatic (C19-C36)mg/kg ND 10.0 N209/25/17 12:33
Aromatic (C11-C22)mg/kg ND 10.0 N209/25/17 12:33
2-Bromonaphthalene (S)%71 40-140 09/25/17 12:33
2-Fluorobiphenyl (S)%70 40-140 09/25/17 12:33
Nonatriacontane (S)%49 40-140 09/25/17 12:33
o-Terphenyl (S)%41 40-140 09/25/17 12:33
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2100694LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2100695
Aliphatic (C09-C18)mg/kg ND N2106840-14069ND 50
Aliphatic (C19-C36)mg/kg 10.6 N213.3 79 40-1407910.5 1 50
Aromatic (C11-C22)mg/kg 22.0 N228.3 78 40-1407621.6 2 50
2-Bromonaphthalene (S)%93 40-14088
2-Fluorobiphenyl (S)%94 40-14089
Nonatriacontane (S)%41 40-14056
o-Terphenyl (S)%84 40-14084
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 156 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
378620
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92355949001, 92355949002, 92355949003, 92355949004, 92355949005, 92355949006
Parameter Units
Dup
Result QualifiersRPDResult
92355735001
2098029SAMPLE DUPLICATE:
Percent Moisture %79.8 080.0
Parameter Units
Dup
Result QualifiersRPDResult
92355837001
2098037SAMPLE DUPLICATE:
Percent Moisture %87.0 185.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 157 of 165
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92355949
Blvd B.P.
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
378637
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92355949007, 92355949008, 92355949009, 92355949010, 92355949011, 92355949012, 92355949013,
92355949014, 92355949015, 92355949016, 92355949017, 92355949018, 92355949019, 92355949020,
92355949021, 92355949022, 92355949023, 92355949024
Parameter Units
Dup
Result QualifiersRPDResult
92355949007
2098142SAMPLE DUPLICATE:
Percent Moisture %24.8 124.4
Parameter Units
Dup
Result QualifiersRPDResult
92355955001
2098143SAMPLE DUPLICATE:
Percent Moisture %21.2 522.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 158 of 165
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92355949
Blvd B.P.
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Analyte concentration exceeded the calibration range. The reported result is estimated.E
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associatedsamples may be biased high.L1
Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.L2
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
The lab does not hold NELAC/TNI accreditation for this parameter.N2
Surrogate recovery outside laboratory control limits.S0
Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re-analysis).S2
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated sample.S3
Surrogate recovery not evaluated against control limits due to sample dilution.S4
Surrogate recovery outside control limits due to matrix interferences (not confirmed by re-analysis).S5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 159 of 165
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92355949
Blvd B.P.
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92355949001 378685 379004SB-1A MADEP EPH MADEP EPH
92355949002 378685 379004SB-1B MADEP EPH MADEP EPH
92355949003 379047 379274SB-1C MADEP EPH MADEP EPH
92355949004 378685 379004SB-2A MADEP EPH MADEP EPH
92355949005 378685 379004SB-2B MADEP EPH MADEP EPH
92355949006 378685 379004SB-2C MADEP EPH MADEP EPH
92355949007 378685 379004SB-3A MADEP EPH MADEP EPH
92355949008 378685 379004SB-3B MADEP EPH MADEP EPH
92355949009 378685 379004SB-3C MADEP EPH MADEP EPH
92355949010 379047 379274SB-4A MADEP EPH MADEP EPH
92355949011 378685 379004SB-4B MADEP EPH MADEP EPH
92355949012 378685 379004SB-4C MADEP EPH MADEP EPH
92355949013 378685 379004SB-5A MADEP EPH MADEP EPH
92355949014 378685 379004SB-5B MADEP EPH MADEP EPH
92355949015 378685 379004SB-5C MADEP EPH MADEP EPH
92355949016 378685 379004SB-6A MADEP EPH MADEP EPH
92355949017 378685 379004SB-6B MADEP EPH MADEP EPH
92355949018 378685 379004SB-6C MADEP EPH MADEP EPH
92355949019 378685 379004SB-7A MADEP EPH MADEP EPH
92355949020 378685 379004SB-7B MADEP EPH MADEP EPH
92355949021 379047 379274SB-7C MADEP EPH MADEP EPH
92355949022 379047 379274SB-8A MADEP EPH MADEP EPH
92355949023 379047 379274SB-8B MADEP EPH MADEP EPH
92355949024 379047 379274SB-8C MADEP EPH MADEP EPH
92355949001 378723 378994SB-1A MADEP VPH MADEP VPH
92355949002 378723 378994SB-1B MADEP VPH MADEP VPH
92355949003 378723 378994SB-1C MADEP VPH MADEP VPH
92355949004 378723 378994SB-2A MADEP VPH MADEP VPH
92355949005 378723 378994SB-2B MADEP VPH MADEP VPH
92355949006 378723 378994SB-2C MADEP VPH MADEP VPH
92355949007 378723 378994SB-3A MADEP VPH MADEP VPH
92355949008 378723 378994SB-3B MADEP VPH MADEP VPH
92355949009 378723 378994SB-3C MADEP VPH MADEP VPH
92355949010 378723 378994SB-4A MADEP VPH MADEP VPH
92355949011 378723 378994SB-4B MADEP VPH MADEP VPH
92355949012 378723 378994SB-4C MADEP VPH MADEP VPH
92355949013 378723 378994SB-5A MADEP VPH MADEP VPH
92355949014 378723 378994SB-5B MADEP VPH MADEP VPH
92355949015 378723 378994SB-5C MADEP VPH MADEP VPH
92355949016 378723 378994SB-6A MADEP VPH MADEP VPH
92355949017 378723 378994SB-6B MADEP VPH MADEP VPH
92355949018 378723 378994SB-6C MADEP VPH MADEP VPH
92355949019 378723 378994SB-7A MADEP VPH MADEP VPH
92355949020 378723 378994SB-7B MADEP VPH MADEP VPH
92355949021 379187 379418SB-7C MADEP VPH MADEP VPH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 160 of 165
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92355949
Blvd B.P.
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92355949022 379187 379418SB-8A MADEP VPH MADEP VPH
92355949023 379187 379418SB-8B MADEP VPH MADEP VPH
92355949024 379187 379418SB-8C MADEP VPH MADEP VPH
92355949001 378645 378789SB-1A EPA 3546 EPA 8270
92355949002 378645 378789SB-1B EPA 3546 EPA 8270
92355949003 378645 378789SB-1C EPA 3546 EPA 8270
92355949004 378645 378789SB-2A EPA 3546 EPA 8270
92355949005 378645 378789SB-2B EPA 3546 EPA 8270
92355949006 378645 378789SB-2C EPA 3546 EPA 8270
92355949007 378645 378789SB-3A EPA 3546 EPA 8270
92355949008 378645 378789SB-3B EPA 3546 EPA 8270
92355949009 378645 378789SB-3C EPA 3546 EPA 8270
92355949010 378645 378789SB-4A EPA 3546 EPA 8270
92355949011 378645 378789SB-4B EPA 3546 EPA 8270
92355949012 378645 378789SB-4C EPA 3546 EPA 8270
92355949013 378645 378789SB-5A EPA 3546 EPA 8270
92355949014 378645 378789SB-5B EPA 3546 EPA 8270
92355949015 378645 378789SB-5C EPA 3546 EPA 8270
92355949016 378645 378789SB-6A EPA 3546 EPA 8270
92355949017 378645 378789SB-6B EPA 3546 EPA 8270
92355949018 378645 378789SB-6C EPA 3546 EPA 8270
92355949019 378645 378789SB-7A EPA 3546 EPA 8270
92355949020 378645 378789SB-7B EPA 3546 EPA 8270
92355949021 378650 378696SB-7C EPA 3546 EPA 8270
92355949022 378650 378696SB-8A EPA 3546 EPA 8270
92355949023 378862 378969SB-8B EPA 3546 EPA 8270
92355949024 378650 378696SB-8C EPA 3546 EPA 8270
92355949001 378755SB-1A EPA 8260
92355949002 378755SB-1B EPA 8260
92355949003 378755SB-1C EPA 8260
92355949004 378755SB-2A EPA 8260
92355949005 378755SB-2B EPA 8260
92355949006 378755SB-2C EPA 8260
92355949007 378755SB-3A EPA 8260
92355949008 378755SB-3B EPA 8260
92355949009 378788SB-3C EPA 8260
92355949010 378788SB-4A EPA 8260
92355949011 378788SB-4B EPA 8260
92355949012 378788SB-4C EPA 8260
92355949013 378935SB-5A EPA 8260
92355949014 378935SB-5B EPA 8260
92355949015 379248SB-5C EPA 8260
92355949016 378935SB-6A EPA 8260
92355949017 378935SB-6B EPA 8260
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 161 of 165
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92355949
Blvd B.P.
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92355949018 378935SB-6C EPA 8260
92355949019 378935SB-7A EPA 8260
92355949020 378935SB-7B EPA 8260
92355949021 378935SB-7C EPA 8260
92355949022 378935SB-8A EPA 8260
92355949023 378935SB-8B EPA 8260
92355949024 378935SB-8C EPA 8260
92355949001 378620SB-1A ASTM D2974-87
92355949002 378620SB-1B ASTM D2974-87
92355949003 378620SB-1C ASTM D2974-87
92355949004 378620SB-2A ASTM D2974-87
92355949005 378620SB-2B ASTM D2974-87
92355949006 378620SB-2C ASTM D2974-87
92355949007 378637SB-3A ASTM D2974-87
92355949008 378637SB-3B ASTM D2974-87
92355949009 378637SB-3C ASTM D2974-87
92355949010 378637SB-4A ASTM D2974-87
92355949011 378637SB-4B ASTM D2974-87
92355949012 378637SB-4C ASTM D2974-87
92355949013 378637SB-5A ASTM D2974-87
92355949014 378637SB-5B ASTM D2974-87
92355949015 378637SB-5C ASTM D2974-87
92355949016 378637SB-6A ASTM D2974-87
92355949017 378637SB-6B ASTM D2974-87
92355949018 378637SB-6C ASTM D2974-87
92355949019 378637SB-7A ASTM D2974-87
92355949020 378637SB-7B ASTM D2974-87
92355949021 378637SB-7C ASTM D2974-87
92355949022 378637SB-8A ASTM D2974-87
92355949023 378637SB-8B ASTM D2974-87
92355949024 378637SB-8C ASTM D2974-87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/01/2017 11:44 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 162 of 165
Page 163 of 165
Page 164 of 165
Page 165 of 165