RA-2071_12611_CA_MRP_20150121_ATC FINAL State Lead Report

Soil Assessment Report

Ferrell Residence
Incident #12611
5379 Wiggins Mill Road
Lucama, Wilson County, North Carolina
ATC Project No. 45.18514.3064

January 21, 2015
2725 East Millbrook Road
Suite 121
Raleigh, NC 27604
Tel: [phone]
Fax: [phone]
www.atcassociates.com
N.C. Engineering License No. C-1598

January 21, 2015

Mr. Mark Petermann
North Carolina Department of Environment and Natural Resources
Division of Waste Management
Underground Storage Tank Section
1637 Mail Service Center
Raleigh, North Carolina 27699-1637

Re: Soil Assessment Report
Ferrell Residence
5379 Wiggins Mill Road
Lucama, Wilson County, North Carolina
NCDENR Incident No. 12611
ATC Project No. 45.18514.3064

Dear Mr. Petermann:

ATC Associates of North Carolina, P.C. (ATC) is submitting the enclosed Soil and Groundwater
Assessment Report for the Ferrell Residence. The report presents investigative procedures, field
activities, and laboratory analytical results for assessment activities conducted in November 2014.
If you have any questions or require additional information, please contact our office at (919) 871-
0999.

Sincerely,

ATC Associates of North Carolina, P.C.

Elizabeth A. Allyn Gabriel Araos, P.E.
Project Scientist Senior Project Manager

Jeffrey A. Corson
Program Manager

TABLE OF CONTENTS

1. SITE IDENTIFICATION .........................................................................................1 
2.0 INTRODUCTION....................................................................................................2 
3.0 SITE DESCRIPTION .............................................................................................2 
3.1 Site Characterization ................................................................................2 
3.2 Site Background .......................................................................................3 
4.0 SOIL ASSESSMENT ACTIVITIES .....................................................................5 
5.0 CONCLUSIONS ......................................................................................................7 

TABLES
Table 1 Water Supply Well Information
Table 2 Soil Analytical Results

FIGURES
Figure 1 Site Topographic Map
Figure 2 Site Map
Figure 3 Potential Receptor Map
Figure 4 Soil Boring Location Map

APPENDICES
Appendix A Field Notes
Appendix B Soil Boring Logs
Appendix C Laboratory Analytical Results

Soil Assessment Report January 21, 2015
Ferrell Residence (Incident #12611) ATC Project No. 45.18514.3064
2
2.0 INTRODUCTION

ATC Associates of North Carolina, P.C. (ATC) has completed a Soil and Groundwater Assessment
Report for the Ferrell Residence. This report documents soil assessment event conducted at the site
in November 2014. The Soil Assessment Report is being performed based on a September 12, 2014
Task Authorization (TA-2) by the Trust Fund Branch of the Underground Storage Tank (UST)
Section, Division of Waste Management, North Carolina Department of Environment and Natural
Resources (NCDENR). The work is performed as part of the State Lead Contract #N14004i
between NCDENR and ATC.

3.0 SITE DESCRIPTION

3.1 Site Characterization

The Ferrell Residence site is located approximately 0.31 miles west of the junction of Scott Church
Road and Wiggins Mill Road in Lucama, Wilson County, North Carolina, and is currently
developed with a residential home. The former Barnes Store was located approximately 270 feet
east northeast of the Ferrell Residence and was used as a convenience store and petroleum retail
facility. Two 650-gallon USTs of unknown contents (assumed gasoline or diesel) and one 250-
gallon kerosene UST were located at the former Barnes Store. It is estimated that the USTs were
taken out of service in the early 1960’s; however, the exact year is unknown. The USTs were
removed from the former Barnes’s Store in 1995. The site is surrounded by properties used for
residential or agricultural purposes. Municipal water is available to the site and vicinity.

Seven water supply wells (WSW-1 through WSW-7) are located within 1,500 feet of the site, four
of which are within 1,000 feet of the site. Water supply well ownership information is included in
Table 1. A site topographic map is included as Figure 1 and a site map depicting monitoring well
locations and other pertinent site features is included as Figure 2. A Potential Receptor Map
showing water supply well locations is included as Figure 3.

Soil Assessment Report January 21, 2015
Ferrell Residence (Incident #12611) ATC Project No. 45.18514.3064
3
3.2 Site Background

In August 1994, the NCDENR Division of Environmental Management sampled potable wells
located at the Ferrell Residence (WSW-1) and Deans Residence (WSW-2). Water supply well
WSW-1 water supply well contained 1,2-dichloropropane at 0.39 micrograms per liter (µg/L),
xylenes at 1.2 µg/L, and naphthalene at 15 µg/L. Water supply well WSW-2 contained
chloroform at 0.69 µg/L and 1,2-dichloropropane at 0.59 µg/L.

ATEC Associates (ATEC) submitted an Initial Investigation Report to NCDENR on December
8, 1994. During the investigation, ATEC conducted a site reconnaissance and collected samples
from water supply wells WSW-1 through WSW-3. Based on the laboratory results, chloroform
was detected in WSW-2 at 4.2 µg/L. Based on the results, ATEC recommended UST closure at
the former Barnes Store.

On February 2, 1995, two 650-gallon USTs of unknown contents (although it is assumed they
formerly contained either gasoline or diesel) and one 250-gallon kerosene UST were removed
from the site. Soil samples collected during the UST closure indicated total petroleum
hydrocarbons (TPH) gasoline range organics (GRO) and diesel range organics (DRO) above the
NCDENR Action Level of 10 mg/kg. An Underground Storage Tank Closure Report was
submitted on March 17, 1995.

ATEC submitted at Subsurface Investigation Report on October 30, 1995, documenting the
installation of monitoring wells MW-1 through MW-4 and soil and groundwater sampling. Soil
samples collected from the MW-1 boring indicated a concentration of 88 mg/kg of TPH GRO.
In addition, the groundwater collected from MW-1 indicated concentrations of petroleum
impacts exceeding 2L Standard. Water supply well WSW-2 contained chloroform at a
concentration of 12.2 µg/L.

Mid-Atlantic Associates, P.A. (Mid-Atlantic) submitted a Report of Environmental Services on
October 11, 1996, documenting a comprehensive groundwater sampling event and slug testing
data. Mid-Atlantic performed a geoprobe investigation in December 1996 in order to delineate
Soil Assessment Report January 21, 2015
Ferrell Residence (Incident #12611) ATC Project No. 45.18514.3064
4
the groundwater plume. During the investigation, 13 shallow groundwater samples (GP-1S
through GP-13S) and six samples from the deeper aquifer (GP-3D, GP-4D, GP-5D, GP-11D,
and GP-12D) were collected. The sample collected from GP-10S exhibited concentrations
exceeding 2L Standard. The Geoprobe Investigation Report was submitted on January 29, 1997.

Between March 1997 and March 2002, eight groundwater sampling events were performed.
During a sampling event conducted in April 2000, monitoring well MW-2 could not be located
and was presumed to be destroyed.

A Mobile Multi-Phase Extraction (MMPE) event was performed of the site from June 9, 2003
through June 13, 2003. At the conclusion of the event, approximately 1,724 gallons of
petroleum impacted groundwater were recovered from monitoring well MW-1. A groundwater
sampling event was performed on July 9, 2003, to determine the effectiveness of the MMPE
event. Based on the results of the groundwater sampling event, an additional MMPE event was
performed from December 1, 2003 through December 5, 2003. At the conclusion of the event,
approximately 964 gallons of petroleum impacted water was recovered from MW-1. A sampling
event to monitor the effectiveness of the second MMPE event was performed on January 13,
2004.

A Soil Investigation, Monitoring Well Installation, and Groundwater Monitoring Report was
submitted in March 2005 and documented the advancement of 11 soil borings (SB-1 though SB-
11) at the former Barnes Store property, the installation of MW-2R, and a comprehensive
sampling event. Based on the analytical results, none of the soil borings had indicated petroleum
constituents and monitoring well MW-1 was the only impacted well.

A Soil Removal and Sampling and Groundwater Sampling Report was submitted in June 2006.
During the reporting period, approximately 165 tons of soil were removed from the site.
Following excavation, five soil samples were submitted for analysis of TPH GRO and TPH
DRO. Four of the samples indicated an exceedence of the corresponding Action Level. In
addition, a groundwater sample was collected from temporary well TW-1. Monitoring well
Soil Assessment Report January 21, 2015
Ferrell Residence (Incident #12611) ATC Project No. 45.18514.3064
5
MW-2R could not be located and was determined to be destroyed due to farming activities in the
area.

Between November 6, 2006 and November 1, 2007, three sampling events were performed at the
site. On February 19, 2008, four soil borings were advanced around the surrounding UST area.
Based on the soil analytical results, impacted soil appears to be delineated. In addition, an
updated receptor survey and groundwater sampling event were performed.

On August 19, 2009, monitoring well MW-5R was installed for horizontal delineation of the
groundwater plume. During the September 2009 sampling event, monitoring well MW-4 could
not be located and was presumed destroyed. Between November 19, 2008 and July 17, 2014,
nine groundwater sampling events have been performed at the site.

On August 13, 2015, ATC submitted a Federal/State-Lead Monitoring Report documenting the
completion of a sampling event. The laboratory analytical results indicated petroleum hydrocarbon
compounds at concentrations exceeding North Carolina 2L Groundwater Standards (2L Standards)
in monitoring well MW-1. ATC recommended continued sampling of the existing monitoring well
and proximal water supply wells and the completion of a limited soil assessment.

4.0 SOIL ASSESSMENT ACTIVITIES

ATC performed a limited soil assessment to determine if residual petroleum impacted soils
remained near the former UST basin. On November 26, 2014, ATC supervised Carolina Soil
Investigations, Inc. (CSI) during the advancement of nine soil borings (SB-1 through SB-9) above
the water table, approximately three feet below ground surface (bgs). Locations were based on
previously assessed areas as shown in the June 2006 Soil Removal and Sampling Report submitted
by Force Environmental Service Company. It should be noted that the historical soil results were
taken at depths approximately 10-13 feet bgs which are below the current and historical water tables
(4-5 feet bgs).
Soil Assessment Report January 21, 2015
Ferrell Residence (Incident #12611) ATC Project No. 45.18514.3064
6
The November 2014 and historical soil boring locations are shown on Figure 4. Soil analytical
results are included in Table 2. Field notes documenting the soil assessment are included as
Appendix A. Soil boring logs are included as Appendix B.

During advancement of each boring, ATC collected a soil sample at 3 feet bgs. Each sample was
then divided and placed into two separate Ziploc bags. One bag was placed in an ice-filled cooler
and the other was placed outside of the cooler to maximize volatilization. The soil sample that was
volatilized was then screened with a photoionization detector (PID). Each sample collected
indicated a PID reading of 0.0 parts per million and did not exhibit petroleum odors. Each sample
was placed in laboratory-approved containers, packed in ice and delivered under
chain-of-custody protocol to Contest Analytical Laboratory (Contest) in East Longmeadow,
Massachusetts for analysis of volatile organic compounds (VOCs) by EPA Method 8260B, semi-
volatile compounds by EPA Method 8270, volatile petroleum hydrocarbons (VPH) and extractable
petroleum hydrocarbons (EPH) by the Massachusetts Department of Environmental Protection
(MADEP) method.

Laboratory analytical results of the soil sampling event indicated no petroleum hydrocarbon
compounds detected above North Carolina Soil-to-Groundwater Maximum Soil Contaminant
Concentrations (MSCC). The following compounds were detected above the laboratory detection
limits in one or more soil samples: acetone, bis (2-Ethylhexyl) phthalate, C19-C36 Aliphatics,
phenanthrene, fluoranthene, pyrene.

As part of ATC’s quality assurance and quality control (QA and QC) measures, a data review of
the laboratory report was conducted. During the review, it was concluded that samples were
received by the laboratory in acceptable condition and properly preserved. The samples were
analyzed within the correct holding times, and the chain of custody was properly completed by
all parties. The laboratory QC report shows an internal blank was analyzed for each method that
was used for the original samples. The laboratory fortified blank (LFB) and laboratory control
sample (LCS) data results were also provided for each analytical method. Refer to the laboratory
reports in Appendix C for details regarding QA results for the laboratory samples and any noted
Soil Assessment Report January 21, 2015
Ferrell Residence (Incident #12611) ATC Project No. 45.18514.3064
7
exceptions. Overall, ATC concludes that the laboratory results are usable and any exceptions do
not significantly impact the conclusions presented in this report.

5.0 CONCLUSIONS

On behalf of the Trust Fund Branch of the UST Section, ATC has completed a Soil Assessment
Report documenting November 2014 assessment activities for the Ferrell Residence, located at
located at 5379 Wiggins Mill Road in Lucama, Wilson County, North Carolina. Results from
soil assessment activities indicated no petroleum hydrocarbon compounds were detected above
North Carolina Soil-to-Groundwater Maximum Soil Contaminant Concentrations (MSCC).
Furthermore, historical soil samples that indicated petroleum hydrocarbon impacts were collected at
depths approximately 10-13 feet bgs which are below the current and historical water table (4-5 feet
bgs) levels. Therefore, previously identified impacted soils are most likely associated with the
petroleum impacted groundwater. Based on the results of the current and historical soil
assessments, additional assessment and/or soil excavations are not warranted.

ATC recommends the following activities:
 Continued monitoring of the existing monitoring well network;
 Installation of a downgradient monitoring well approximately 50-75 feet south of MW-1
and two additional monitoring wells (replacement for monitoring wells MW-2 and MW-4).
 Installation of ORC socks in MW-1 to reduce the VOC concentrations; and
 Abandonment of two inactive water supply wells (WSW-1 and WSW-2) that may lower the
site risk.

TABLES
TABLE 1WATER SUPPLY WELL INFORMATIONFERRELL RESIDENCE5379 WIGGINS MILL ROADLUCAMA, WILSON COUNTY, NORTH CAROLINAINCIDENT #12611ATC PROJECT #45.18514.3064Well ID Property Owner(s) Property Address Owner Address Well Status UseMunicipal Water ConnectionDistance/Direction From Source (ft.)Up or Downgradient5379 Wiggins Mill Road 240 Polly Watson RoadLucama, NC 27581 Fremont, NC 278305366 Wiggins Mill Road 108 Wildwood Ave.Lucama, NC 27581 Rocky Mount, NC 278035356 Wiggins Mill Road 5356 Wiggins Mill RoadLucama, NC 27581 Lucama, NC 275815336 Wiggins Mill Road 240 Polly Watson RoadLucama, NC 27581 Fremont, NC 278305430 Wiggins Mill Road 5430 Wiggins Mill RoadLucama, NC 27581 Lucama, NC 275815421 Wiggins Mill Road 5421 Wiggins Mill RoadLucama, NC 27581 Lucama, NC 275815444 Wiggins Mill Road 5444 Wiggins Mill RoadLucama, NC 27581 Lucama, NC 27581Aycock Brothers of NC, LLCWSW-1Inactive YesNot in Use 250 SWInactive YesWSW-6 Lennie Edgar Bunn, Jr. Active NoWSW-5 Carl B. & Sherry S. EdwardsNot in UseTable adapted from Terraine Environmental Consulting, Monitoring Well Installation and Groundwater Monitoring Report, December 18, 2009. Property Owners and addresses udated 08/21/2012; New data from Wilson County, NC GIS Server.Russell W. & William R. BarnesWSW-2Inactive NoNot in UseIrrigationDrinkingActive YesWSW-4 Aycock Brothers of NC, LLC Active NoHerman L., Jr. & Linda H. BarnesWSW-3DrinkingWSW-7 Seth O. SmithActive YesIrrigation 1,400 SWCrossgradientUpgradientUpgradientUpgradientCrossgradientCrossgradientCrossgradient200 NW350 NE1,100 NE1,150 SW950 SW
TABLE 2SOIL ANALYTICAL RESULTSFerrell Residence5379 Wiggins Mill RoadLucama, North CarolinaIncident #12611SB-1 3 11/26/14 0<0.00059 <0.00068 <0.00068 <0.00199 0.02 J 0.25 J <0.17 <0.10 <0.13 <11 ND 17 NDSB-2 3 11/26/14 0<0.00059 <0.00068 <0.00068 <0.00199 <0.020 0.25 J <0.18 0.11 J <0.14 <9.8 ND <12 NDSB-3 3 11/26/14 0<0.00063 <0.00072 <0.00072 <0.00213 <0.021 0.24 J <0.18 <0.10 <0.14 <10 ND <12 NDSB-4 3 11/26/14 0<0.00073 <0.00084 <0.00084 <0.00253 <0.024 0.21 J 0.20 0.24 0.16 J <10 ND <12 NDSB-5 3 11/26/14 0<0.00089 <0.0010 <0.0010 <0.00309 <0.030 0.25 J <0.18 <0.11 <0.14 <12 ND <12 NDSB-6 3 11/26/14 0<0.00062 <0.00071 <0.00071 <0.00212 <0.021 0.23 J <0.18 <0.11 <0.14 <11 ND <12 NDSB-7 3 11/26/14 0<0.00059 <0.00067 <0.00067 <0.00199 <0.020 0.25 J <0.17 <0.10 <0.13 <9.9 ND <11 NDSB-8 3 11/26/14 0<0.00063 <0.00072 <0.00072 <0.00213 <0.021 0.22 J <0.18 <0.11 <0.14 <12 ND <12 NDSB-9 3 11/26/14 0<0.00058 <0.00066 <0.00066 <0.00198 <0.019 0.16 J <0.18 <0.11 <0.14 <12 ND <12 ND0.0056 4.3 4.9 4.6 24 6.6 290 56 270 68 540 ### 3118 1,200 1,560 3,129 14,000 46 620 469 469 939 1,500 31,000 469164 32,000 40,000 81,760 360,000 410 16,400 12,264 12,264 24,528 40,000 810,000 12,264Notes:1. Concentrations reported in milligrams per kilogram (mg/kg).2. "<" = not detected at or above the laboratory detection limit.3. Bold indicates concentrations above NCDENR Action Level.4. Final C9-C18 Aliphatics values are equal to (C9-C12 Aliphatics - C9-C10 Aromatics) + C9-C18 Aromatics.5. Final C9-C22 Aromatics are equal to C9-C10 Aromatics + C11-C22 Aromatics.6. J = Detected but below the reporting limit (lowest calibration standard); therefore, result is an estimated concentration.7. ### = Considered immobile.EthylbenzeneTotal XylenesDate SampledC5-C8 AliphaticsBis (2-Ethylhexyl) phthalateAcetone Fluoranthene PyreneIndustrial/Commerical MSCC8260BC9-C18 AliphaticsC9-C22 AromaticsSoil-to-Groundwater MSCCResidential MSCCC19-C36 Aliphatics8270CPhenantheneEPA Method:MADEP VPH and EPHSample Depth (feet) PID (ppm) Benzene Toluene

FIGURES
.

2725 E. Millbrook Road, Ste 121
Raleigh, NC 27604
[phone]
PROJECT NO: 45.18514.3064
DATE: 8/2014 REVIEWED BY: GA
Ferrell Residence – Incident #12611
5379 Wiggins Mill Road
Lucama, Wilson County, North Carolina
SOURCE: 1988 TOPOGRAPHIC MAP - MSRMAPS.COM.
SCALE: SEE ABOVE
FIGURE 1: SITE TOPOGRAPHIC MAP
N
SITE
2725 E. Millbrook Road, Ste 121
Raleigh, NC 27604
[phone]
PROJECT NO: 45.18514.3064
DATE: 8/2014 REVIEWED BY: GA
Ferrell Residence – Incident #12611
5379 Wiggins Mill Road
Lucama, Wilson County, North Carolina
SOURCE: Wilson County GIS
SCALE: 1” = 425’
FIGURE 3: POTENTIAL RECEPTOR MAP
Potable Water Supply Well
Irrigation Water Supply Well
Inactive Water Supply Well
500 Foot Radius From Source Area
1,000 Foot Radius From Source Area
N
WSW-7
WSW-6
WSW-2
WSW-1
Ferrell
Residence
(Site)Former Barnes
Store (Source
Area)
WSW-3
WSW-4
WSW-5

APPENDIX A

FIELD NOTES

APPENDIX B

SOIL BORING LOGS
12-29-2014 S:\Enviro\NCDENR State Lead Contract\Mark Sites\12611 - Ferrell Residence\Boring Logs\SB-1.borClient: NCDENR State Lead Program
ATC Project No. 045.18514.3064
Lucama, North Carolina
5379 Wiggins Mill Road
Ferrell Residence - Incident #12611
Terminated boring at 3 feet below ground surface.
BORING LOG: SB-1
(Page 1 of 1)
Date(s) Drilled : 11/26/14
Drilling Contractor : Carolina Soil Investigations
Drilling Method : Geoprobe
Boring Diameter : 4 Inches
Sampling Method : Macrocore
Sampling Interval : Continuous
Logged By : Jon Whitley
Depth In Feet0
1
2
3 USCSSW
SW GRAPHICDESCRIPTION
Red, light brown SAND, moderately sorted
Brown with dark brown spots, SAND, well sorted, dry
End of boring
PID
(ppm)
0.0
12-29-2014 S:\Enviro\NCDENR State Lead Contract\Mark Sites\12611 - Ferrell Residence\Boring Logs\SB-2.borClient: NCDENR State Lead Program
ATC Project No. 045.18514.3064
Lucama, North Carolina
5379 Wiggins Mill Road
Ferrell Residence - Incident #12611
Terminated boring at 3 feet below ground surface.
BORING LOG: SB-2
(Page 1 of 1)
Date(s) Drilled : 11/26/14
Drilling Contractor : Carolina Soil Investigations
Drilling Method : Geoprobe
Boring Diameter : 4 Inches
Sampling Method : Macrocore
Sampling Interval : Continuous
Logged By : Jon Whitley
Depth In Feet0
1
2
3 USCSOM
SW
SW GRAPHICDESCRIPTION
Grass and topsoil
Red, light brown SAND, moderately sorted
Light brown SAND, moderately sorted, dry
End of boring
PID
(ppm)
0.0
12-29-2014 S:\Enviro\NCDENR State Lead Contract\Mark Sites\12611 - Ferrell Residence\Boring Logs\SB-3.borClient: NCDENR State Lead Program
ATC Project No. 045.18514.3064
Lucama, North Carolina
5379 Wiggins Mill Road
Ferrell Residence - Incident #12611
Terminated boring at 3 feet below ground surface.
BORING LOG: SB-3
(Page 1 of 1)
Date(s) Drilled : 11/26/14
Drilling Contractor : Carolina Soil Investigations
Drilling Method : Geoprobe
Boring Diameter : 4 Inches
Sampling Method : Macrocore
Sampling Interval : Continuous
Logged By : Jon Whitley
Depth In Feet0
1
2
3 USCSOM
SW
SW GRAPHICDESCRIPTION
Grass and topsoil
Red, light brown SAND, moderately sorted
Light brown SAND, moderately sorted, dry
End of boring
PID
(ppm)
0.0
12-29-2014 S:\Enviro\NCDENR State Lead Contract\Mark Sites\12611 - Ferrell Residence\Boring Logs\SB-4.borClient: NCDENR State Lead Program
ATC Project No. 045.18514.3064
Lucama, North Carolina
5379 Wiggins Mill Road
Ferrell Residence - Incident #12611
Terminated boring at 3 feet below ground surface.
BORING LOG: SB-4
(Page 1 of 1)
Date(s) Drilled : 11/26/14
Drilling Contractor : Carolina Soil Investigations
Drilling Method : Geoprobe
Boring Diameter : 4 Inches
Sampling Method : Macrocore
Sampling Interval : Continuous
Logged By : Jon Whitley
Depth In Feet0
1
2
3 USCSOM
SW
SW GRAPHICDESCRIPTION
Grass and topsoil
Light brown SAND, moderately sorted
Brown SAND, moderately sorted, dry
End of boring
PID
(ppm)
0.0
12-29-2014 S:\Enviro\NCDENR State Lead Contract\Mark Sites\12611 - Ferrell Residence\Boring Logs\SB-5.borClient: NCDENR State Lead Program
ATC Project No. 045.18514.3064
Lucama, North Carolina
5379 Wiggins Mill Road
Ferrell Residence - Incident #12611
Terminated boring at 3 feet below ground surface.
BORING LOG: SB-5
(Page 1 of 1)
Date(s) Drilled : 11/26/14
Drilling Contractor : Carolina Soil Investigations
Drilling Method : Geoprobe
Boring Diameter : 4 Inches
Sampling Method : Macrocore
Sampling Interval : Continuous
Logged By : Jon Whitley
Depth In Feet0
1
2
3 USCSSW
SC GRAPHICDESCRIPTION
Red, light brown SAND, moderately sorted
Red CLAYEY SAND, poorly sorted, dry
End of boring
PID
(ppm)
0.0
12-29-2014 S:\Enviro\NCDENR State Lead Contract\Mark Sites\12611 - Ferrell Residence\Boring Logs\SB-6.borClient: NCDENR State Lead Program
ATC Project No. 045.18514.3064
Lucama, North Carolina
5379 Wiggins Mill Road
Ferrell Residence - Incident #12611
Terminated boring at 3 feet below ground surface.
BORING LOG: SB-6
(Page 1 of 1)
Date(s) Drilled : 11/26/14
Drilling Contractor : Carolina Soil Investigations
Drilling Method : Geoprobe
Boring Diameter : 4 Inches
Sampling Method : Macrocore
Sampling Interval : Continuous
Logged By : Jon Whitley
Depth In Feet0
1
2
3 USCSOM
SW
SW GRAPHICDESCRIPTION
Grass and topsoil
Red, light brown SAND, moderately sorted
Brown with dark brown streaks SAND, well sorted, dry
End of boring
PID
(ppm)
0.0
12-29-2014 S:\Enviro\NCDENR State Lead Contract\Mark Sites\12611 - Ferrell Residence\Boring Logs\SB-7.borClient: NCDENR State Lead Program
ATC Project No. 045.18514.3064
Lucama, North Carolina
5379 Wiggins Mill Road
Ferrell Residence - Incident #12611
Terminated boring at 3 feet below ground surface.
BORING LOG: SB-6
(Page 1 of 1)
Date(s) Drilled : 11/26/14
Drilling Contractor : Carolina Soil Investigations
Drilling Method : Geoprobe
Boring Diameter : 4 Inches
Sampling Method : Macrocore
Sampling Interval : Continuous
Logged By : Jon Whitley
Depth In Feet0
1
2
3 USCSOM
SW
SW GRAPHICDESCRIPTION
Grass and topsoil
Red, light brown SAND, moderately sorted
Brown with dark brown streaks SAND, well sorted, dry
End of boring
PID
(ppm)
0.0
12-29-2014 S:\Enviro\NCDENR State Lead Contract\Mark Sites\12611 - Ferrell Residence\Boring Logs\SB-8.borClient: NCDENR State Lead Program
ATC Project No. 045.18514.3064
Lucama, North Carolina
5379 Wiggins Mill Road
Ferrell Residence - Incident #12611
Terminated boring at 3 feet below ground surface.
BORING LOG: SB-8
(Page 1 of 1)
Date(s) Drilled : 11/26/14
Drilling Contractor : Carolina Soil Investigations
Drilling Method : Geoprobe
Boring Diameter : 4 Inches
Sampling Method : Macrocore
Sampling Interval : Continuous
Logged By : Jon Whitley
Depth In Feet0
1
2
3 USCSOM
SW
SW GRAPHICDESCRIPTION
Grass and topsoil
Red, light brown SAND, moderately sorted
Brown SAND, moderately sorted, dry
End of boring
PID
(ppm)
0.0
12-29-2014 S:\Enviro\NCDENR State Lead Contract\Mark Sites\12611 - Ferrell Residence\Boring Logs\SB-9.borClient: NCDENR State Lead Program
ATC Project No. 045.18514.3064
Lucama, North Carolina
5379 Wiggins Mill Road
Ferrell Residence - Incident #12611
Terminated boring at 3 feet below ground surface.
BORING LOG: SB-9
(Page 1 of 1)
Date(s) Drilled : 11/26/14
Drilling Contractor : Carolina Soil Investigations
Drilling Method : Geoprobe
Boring Diameter : 4 Inches
Sampling Method : Macrocore
Sampling Interval : Continuous
Logged By : Jon Whitley
Depth In Feet0
1
2
3 USCSOM
SW
SW GRAPHICDESCRIPTION
Grass
Light brown SAND, moderately sorted, dry
Light brown SAND, moderately sorted, dry
End of boring
PID
(ppm)
0.0

APPENDIX C

LABORATORY ANALYTICAL RESULTS

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
December 9, 2014
Ashley Winkelman
Cardno ATC Associates - Raleigh NC
2725 East Millbrook Road, Ste 121
Raleigh, NC 27604
Project Location: Ferrell Residence
Client Job Number:
Project Number: 045.18514.3064
Laboratory Work Order Number: 14L0056
Enclosed are results of analyses for samples received by the laboratory on December 1, 2014. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Lisa A. Worthington
Project Manager
Page 1 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
Table of Contents
Sample Summary 4
Case Narrative 6
Sample Results 10
14L0056-01 10
14L0056-02 17
14L0056-03 24
14L0056-04 31
14L0056-05 38
14L0056-06 45
14L0056-07 52
14L0056-08 59
14L0056-09 66
Sample Preparation Information 73
QC Data 75
Volatile Organic Compounds by GC/MS 75
B111082 75
Semivolatile Organic Compounds by GC/MS 80
B110780 80
B110838 84
Petroleum Hydrocarbons Analyses - EPH 90
B110844 90
Petroleum Hydrocarbons Analyses - VPH 93
B111275 93
Flag/Qualifier Summary 95
Certifications 96
Chain of Custody/Sample Receipt 101
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Table of Contents (continued)
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
12/9/2014
Cardno ATC Associates - Raleigh NC
2725 East Millbrook Road, Ste 121
Raleigh, NC 27604
ATTN: Ashley Winkelman
045.18514.3064
14L0056
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Ferrell Residence
SB-1 3 14L0056-01 Soil MADEP-EPH-04-1.1
MADEP-VPH-04-1.1
SM 2540G
SW-846 8260B
SW-846 8270D
SB-2 3 14L0056-02 Soil MADEP-EPH-04-1.1
MADEP-VPH-04-1.1
SM 2540G
SW-846 8260B
SW-846 8270D
SB-3 3 14L0056-03 Soil MADEP-EPH-04-1.1
MADEP-VPH-04-1.1
SM 2540G
SW-846 8260B
SW-846 8270D
SB-4 3 14L0056-04 Soil MADEP-EPH-04-1.1
MADEP-VPH-04-1.1
SM 2540G
SW-846 8260B
SW-846 8270D
SB-5 3 14L0056-05 Soil MADEP-EPH-04-1.1
MADEP-VPH-04-1.1
SM 2540G
SW-846 8260B
SW-846 8270D
SB-6 3 14L0056-06 Soil MADEP-EPH-04-1.1
MADEP-VPH-04-1.1
SM 2540G
SW-846 8260B
SW-846 8270D
SB-7 3 14L0056-07 Soil MADEP-EPH-04-1.1
MADEP-VPH-04-1.1
SM 2540G
SW-846 8260B
SW-846 8270D
SB-8 3 14L0056-08 Soil MADEP-EPH-04-1.1
MADEP-VPH-04-1.1
SM 2540G
SW-846 8260B
SW-846 8270D
[TOC_1]Sample Summary[TOC]
Page 4 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
12/9/2014
Cardno ATC Associates - Raleigh NC
2725 East Millbrook Road, Ste 121
Raleigh, NC 27604
ATTN: Ashley Winkelman
045.18514.3064
14L0056
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Ferrell Residence
SB-9 3 14L0056-09 Soil MADEP-EPH-04-1.1
MADEP-VPH-04-1.1
SM 2540G
SW-846 8260B
SW-846 8270D
Page 5 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
[TOC_1]Case Narrative[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
MADEP-VPH-04-1.1
Qualifications:
Soil/methanol ratio does not meet method specifications. Excess amount of soil. Sample was completely covered with methanol, but with
less than the method-specified amount.
Analyte & Samples(s) Qualified:
O-01
14L0056-02[SB-2 3], 14L0056-03[SB-3 3], 14L0056-04[SB-4 3], 14L0056-07[SB-7 3], 14L0056-09[SB-9 3]
Surrogate recovery is outside of control limits. Data validation is not affected since all associated results are less than the reporting limit and
bias is on the high side.Analyte & Samples(s) Qualified:
S-17
2,5-Dibromotoluene (FID)
14L0056-08[SB-8 3]
SW-846 8260B
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not
affected since all results are "not detected" for associated samples in this batch and bias is on the high side.
Analyte & Samples(s) Qualified:
L-02
Methyl tert-Butyl Ether (MTBE)
B111082-BS1, B111082-BSD1
tert-Butyl Ethyl Ether (TBEE)
B111082-BS1, B111082-BSD1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
1,3,5-Trimethylbenzene
B111082-BS1
2-Chlorotoluene
B111082-BS1
4-Chlorotoluene
B111082-BS1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
outside of control limits. Reduced precision anticipated for any reported result for this compound.
Analyte & Samples(s) Qualified:
L-07A
n-Propylbenzene
B111082-BS1
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
R-05
n-Propylbenzene
14L0056-01[SB-1 3], 14L0056-02[SB-2 3], 14L0056-03[SB-3 3], 14L0056-04[SB-4 3], 14L0056-05[SB-5 3], 14L0056-06[SB-6 3], 14L0056-07[SB-7 3],
14L0056-08[SB-8 3], 14L0056-09[SB-9 3], B111082-BLK1, B111082-BS1, B111082-BSD1
Continuing calibration did not meet method specifications and was biased on the low side for this compound. Increased uncertainty is
associated with the reported value which is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
V-05
1,2,3-Trichlorobenzene
14L0056-01[SB-1 3], 14L0056-02[SB-2 3], 14L0056-03[SB-3 3], 14L0056-04[SB-4 3], 14L0056-05[SB-5 3], 14L0056-06[SB-6 3], 14L0056-07[SB-7 3],
14L0056-08[SB-8 3], 14L0056-09[SB-9 3], B111082-BLK1, B111082-BS1, B111082-BSD1
1,2,4-Trichlorobenzene
14L0056-01[SB-1 3], 14L0056-02[SB-2 3], 14L0056-03[SB-3 3], 14L0056-04[SB-4 3], 14L0056-05[SB-5 3], 14L0056-06[SB-6 3], 14L0056-07[SB-7 3],
14L0056-08[SB-8 3], 14L0056-09[SB-9 3], B111082-BLK1, B111082-BS1, B111082-BSD1
Naphthalene
14L0056-01[SB-1 3], 14L0056-02[SB-2 3], 14L0056-03[SB-3 3], 14L0056-04[SB-4 3], 14L0056-05[SB-5 3], 14L0056-06[SB-6 3], 14L0056-07[SB-7 3],
14L0056-08[SB-8 3], 14L0056-09[SB-9 3], B111082-BLK1, B111082-BS1, B111082-BSD1
SW-846 8270D
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
2,4-Dinitrophenol
14L0056-09[SB-9 3], B110780-BLK1, B110780-BS1, B110780-BSD1
Benzoic Acid
14L0056-09[SB-9 3], B110780-BLK1, B110780-BS1, B110780-BSD1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
N-Nitrosodiphenylamine
B110838-BS1
Pentachloronitrobenzene
B110838-BS1
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.
Analyte & Samples(s) Qualified:
R-05
4,6-Dinitro-2-methylphenol
14L0056-09[SB-9 3], B110780-BLK1, B110780-BS1, B110780-BSD1
One associated surrogate standard recovery is outside of control limits but the other(s) is/are within limits. All recoveries are > 10%.
Analyte & Samples(s) Qualified:
S-07
2,4,6-Tribromophenol
14L0056-01[SB-1 3], B110838-BLK1, B110838-BS1, B110838-BSD1
p-Terphenyl-d14
14L0056-08[SB-8 3], B110838-BS1
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where %RSD is outside of method
specified criteria.
Analyte & Samples(s) Qualified:
V-04
2,4-Dinitrophenol
14L0056-01[SB-1 3], 14L0056-02[SB-2 3], 14L0056-03[SB-3 3], 14L0056-04[SB-4 3], 14L0056-05[SB-5 3], 14L0056-06[SB-6 3], 14L0056-07[SB-7 3],
14L0056-08[SB-8 3], 14L0056-09[SB-9 3]
Benzidine
14L0056-01[SB-1 3], 14L0056-02[SB-2 3], 14L0056-03[SB-3 3], 14L0056-04[SB-4 3], 14L0056-05[SB-5 3], 14L0056-06[SB-6 3], 14L0056-07[SB-7 3],
14L0056-08[SB-8 3], 14L0056-09[SB-9 3], B110780-BLK1, B110780-BS1, B110780-BSD1, B110838-BLK1, B110838-BS1, B110838-BSD1
Continuing calibration did not meet method specifications and was biased on the low side for this compound. Increased uncertainty is
associated with the reported value which is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
V-05
Benzidine
14L0056-01[SB-1 3], 14L0056-02[SB-2 3], 14L0056-03[SB-3 3], 14L0056-04[SB-4 3], 14L0056-05[SB-5 3], 14L0056-06[SB-6 3], 14L0056-07[SB-7 3],
14L0056-08[SB-8 3], 14L0056-09[SB-9 3], B110780-BLK1, B110780-BS1, B110780-BSD1, B110838-BLK1, B110838-BS1, B110838-BSD1
Hexachlorocyclopentadiene
B110780-BLK1, B110780-BS1, B110780-BSD1, B110838-BLK1, B110838-BS1, B110838-BSD1
Continuing calibration did not meet method specifications and was biased on the high side for this compound. Increased uncertainty is
associated with the reported value which is likely to be biased on the high side.
Analyte & Samples(s) Qualified:
V-06
2,4-Dinitrotoluene
B110780-BS1, B110780-BSD1, B110838-BS1, B110838-BSD1
2,6-Dinitrotoluene
B110780-BS1, B110780-BSD1, B110838-BS1, B110838-BSD1
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may be associated with reported
result.
Analyte & Samples(s) Qualified:
V-16
Pentachloronitrobenzene
14L0056-01[SB-1 3], 14L0056-02[SB-2 3], 14L0056-03[SB-3 3], 14L0056-04[SB-4 3], 14L0056-05[SB-5 3], 14L0056-06[SB-6 3], 14L0056-07[SB-7 3],
14L0056-08[SB-8 3], 14L0056-09[SB-9 3], B110780-BLK1, B110780-BS1, B110780-BSD1, B110838-BLK1, B110838-BS1, B110838-BSD1
Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not affected since sample result
was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-20
2,4-Dinitrophenol
14L0056-01[SB-1 3], 14L0056-02[SB-2 3], 14L0056-03[SB-3 3], 14L0056-04[SB-4 3], 14L0056-05[SB-5 3], 14L0056-06[SB-6 3], 14L0056-07[SB-7 3],
14L0056-08[SB-8 3], 14L0056-09[SB-9 3]
2,4-Dinitrotoluene
14L0056-01[SB-1 3], 14L0056-02[SB-2 3], 14L0056-03[SB-3 3], 14L0056-04[SB-4 3], 14L0056-05[SB-5 3], 14L0056-06[SB-6 3], 14L0056-07[SB-7 3],
14L0056-08[SB-8 3], 14L0056-09[SB-9 3], B110780-BLK1, B110838-BLK1
2,6-Dinitrotoluene
14L0056-01[SB-1 3], 14L0056-02[SB-2 3], 14L0056-03[SB-3 3], 14L0056-04[SB-4 3], 14L0056-05[SB-5 3], 14L0056-06[SB-6 3], 14L0056-07[SB-7 3],
14L0056-08[SB-8 3], 14L0056-09[SB-9 3], B110780-BLK1, B110838-BLK1
2-Nitroaniline
14L0056-01[SB-1 3], 14L0056-02[SB-2 3], 14L0056-03[SB-3 3], 14L0056-04[SB-4 3], 14L0056-05[SB-5 3], 14L0056-06[SB-6 3], 14L0056-07[SB-7 3],
14L0056-08[SB-8 3], 14L0056-09[SB-9 3]
4,6-Dinitro-2-methylphenol
14L0056-01[SB-1 3], 14L0056-02[SB-2 3], 14L0056-03[SB-3 3], 14L0056-04[SB-4 3], 14L0056-05[SB-5 3], 14L0056-06[SB-6 3], 14L0056-07[SB-7 3],
14L0056-08[SB-8 3], 14L0056-09[SB-9 3]
4-Nitroaniline
B110780-BLK1
4-Nitrophenol
14L0056-09[SB-9 3]
Benzo(g,h,i)perylene
14L0056-01[SB-1 3], 14L0056-02[SB-2 3], 14L0056-03[SB-3 3], 14L0056-04[SB-4 3], 14L0056-05[SB-5 3], 14L0056-06[SB-6 3], 14L0056-07[SB-7 3],
14L0056-08[SB-8 3], 14L0056-09[SB-9 3]
Dibenz(a,h)anthracene
14L0056-01[SB-1 3], 14L0056-02[SB-2 3], 14L0056-03[SB-3 3], 14L0056-04[SB-4 3], 14L0056-05[SB-5 3], 14L0056-06[SB-6 3], 14L0056-07[SB-7 3],
14L0056-08[SB-8 3], 14L0056-09[SB-9 3]
Pentachloronitrobenzene
14L0056-01[SB-1 3], 14L0056-02[SB-2 3], 14L0056-03[SB-3 3], 14L0056-04[SB-4 3], 14L0056-05[SB-5 3], 14L0056-06[SB-6 3], 14L0056-07[SB-7 3],
14L0056-08[SB-8 3], 14L0056-09[SB-9 3]
MADEP-EPH-04-1.1
SPE cartridge contamination with non-petroleum compounds, if present, is verified by GC/MS in each method blank per extraction batch and excluded from C 11-C22 aromatic
range fraction in all samples in the batch. No significant modifications were made to the method.
MADEP-VPH-04-1.1
No significant modifications were made to the method. All VPH samples were received preserved properly in methanol with a soil/methanol ratio of 1:1 +/- 25% completely
covered by methanol in the proper containers specified on the chain-of-custody form unless specified in this narrative.
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Daren J. Damboragian
Laboratory Manager
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-01
Field Sample #: SB-1 3
Sample Matrix: Soil
Sampled: 11/26/2014 09:50
[TOC_2]14L0056-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
0.020 0.085 12/5/14 11:26 MFFmg/Kg dry0.020 12/4/14SW-846 8260B1JAcetone
ND 0.0051 12/5/14 11:26 MFFmg/Kg dry0.0021 12/4/14SW-846 8260B1Acrylonitrile
ND 0.00085 12/5/14 11:26 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1Benzene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B1Bromobenzene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B1Bromochloromethane
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00051 12/4/14SW-846 8260B1Bromodichloromethane
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B1Bromoform
ND 0.0085 12/5/14 11:26 MFFmg/Kg dry0.0014 12/4/14SW-846 8260B1Bromomethane
ND 0.034 12/5/14 11:26 MFFmg/Kg dry0.015 12/4/14SW-846 8260B12-Butanone (MEK)
ND 0.034 12/5/14 11:26 MFFmg/Kg dry0.018 12/4/14SW-846 8260B1tert-Butyl Alcohol (TBA)
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1n-Butylbenzene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00085 12/4/14SW-846 8260B1sec-Butylbenzene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B1tert-Butylbenzene
ND 0.00085 12/5/14 11:26 MFFmg/Kg dry0.00051 12/4/14SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.0051 12/5/14 11:26 MFFmg/Kg dry0.0028 12/4/14SW-846 8260B1Carbon Disulfide
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B1Carbon Tetrachloride
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1Chlorobenzene
ND 0.00085 12/5/14 11:26 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1Chlorodibromomethane
ND 0.017 12/5/14 11:26 MFFmg/Kg dry0.0013 12/4/14SW-846 8260B1Chloroethane
ND 0.0034 12/5/14 11:26 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1Chloroform
ND 0.0085 12/5/14 11:26 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B1Chloromethane
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B12-Chlorotoluene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B14-Chlorotoluene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00093 12/4/14SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.00085 12/5/14 11:26 MFFmg/Kg dry0.00085 12/4/14SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00051 12/4/14SW-846 8260B1Dibromomethane
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B11,2-Dichlorobenzene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B11,3-Dichlorobenzene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B11,4-Dichlorobenzene
ND 0.0034 12/5/14 11:26 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.017 12/5/14 11:26 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B11,1-Dichloroethane
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B11,2-Dichloroethane
ND 0.0034 12/5/14 11:26 MFFmg/Kg dry0.00093 12/4/14SW-846 8260B11,1-Dichloroethylene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B11,2-Dichloropropane
ND 0.00085 12/5/14 11:26 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B11,3-Dichloropropane
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B12,2-Dichloropropane
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B11,1-Dichloropropene
ND 0.00085 12/5/14 11:26 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1cis-1,3-Dichloropropene
ND 0.00085 12/5/14 11:26 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1trans-1,3-Dichloropropene
ND 0.017 12/5/14 11:26 MFFmg/Kg dry0.0015 12/4/14SW-846 8260B1Diethyl Ether
[TOC_1]Sample Results[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-01
Field Sample #: SB-1 3
Sample Matrix: Soil
Sampled: 11/26/2014 09:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.00085 12/5/14 11:26 MFFmg/Kg dry0.00051 12/4/14SW-846 8260B1Diisopropyl Ether (DIPE)
ND 0.085 12/5/14 11:26 MFFmg/Kg dry0.049 12/4/14SW-846 8260B11,4-Dioxane
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B1Ethylbenzene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00085 12/4/14SW-846 8260B1Hexachlorobutadiene
ND 0.017 12/5/14 11:26 MFFmg/Kg dry0.0092 12/4/14SW-846 8260B12-Hexanone (MBK)
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.0034 12/5/14 11:26 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.017 12/5/14 11:26 MFFmg/Kg dry0.0060 12/4/14SW-846 8260B1Methylene Chloride
ND 0.017 12/5/14 11:26 MFFmg/Kg dry0.0064 12/4/14SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.0034 12/5/14 11:26 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1V-05Naphthalene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1R-05n-Propylbenzene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00051 12/4/14SW-846 8260B1Styrene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.00085 12/5/14 11:26 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B1Tetrachloroethylene
ND 0.0085 12/5/14 11:26 MFFmg/Kg dry0.0019 12/4/14SW-846 8260B1Tetrahydrofuran
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B1Toluene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00051 12/4/14SW-846 8260B1V-051,2,3-Trichlorobenzene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B1V-051,2,4-Trichlorobenzene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B11,3,5-Trichlorobenzene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00085 12/4/14SW-846 8260B11,1,1-Trichloroethane
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B11,1,2-Trichloroethane
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B1Trichloroethylene
ND 0.0085 12/5/14 11:26 MFFmg/Kg dry0.00093 12/4/14SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00093 12/4/14SW-846 8260B11,2,3-Trichloropropane
ND 0.0085 12/5/14 11:26 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B11,2,4-Trimethylbenzene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00051 12/4/14SW-846 8260B11,3,5-Trimethylbenzene
ND 0.0085 12/5/14 11:26 MFFmg/Kg dry0.00093 12/4/14SW-846 8260B1Vinyl Chloride
ND 0.0034 12/5/14 11:26 MFFmg/Kg dry0.0014 12/4/14SW-846 8260B1m+p Xylene
ND 0.0017 12/5/14 11:26 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 96.1 12/5/14 11:2670-130
Toluene-d8 96.8 12/5/14 11:2670-130
4-Bromofluorobenzene 89.1 12/5/14 11:2670-130
Page 11 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-01
Field Sample #: SB-1 3
Sample Matrix: Soil
Sampled: 11/26/2014 09:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.19 12/3/14 14:03 CMRmg/Kg dry0.097 12/2/14SW-846 8270D1Acenaphthene
ND 0.19 12/3/14 14:03 CMRmg/Kg dry0.093 12/2/14SW-846 8270D1Acenaphthylene
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.093 12/2/14SW-846 8270D1Acetophenone
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.29 12/2/14SW-846 8270D1Aniline
ND 0.19 12/3/14 14:03 CMRmg/Kg dry0.12 12/2/14SW-846 8270D1Anthracene
ND 0.75 12/3/14 14:03 CMRmg/Kg dry0.53 12/2/14SW-846 8270D1V-04, V-05Benzidine
ND 0.19 12/3/14 14:03 CMRmg/Kg dry0.088 12/2/14SW-846 8270D1Benzo(a)anthracene
ND 0.19 12/3/14 14:03 CMRmg/Kg dry0.068 12/2/14SW-846 8270D1Benzo(a)pyrene
ND 0.19 12/3/14 14:03 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Benzo(b)fluoranthene
ND 0.19 12/3/14 14:03 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-20Benzo(g,h,i)perylene
ND 0.19 12/3/14 14:03 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Benzo(k)fluoranthene
ND 1.1 12/3/14 14:03 CMRmg/Kg dry1.1 12/2/14SW-846 8270D1Benzoic Acid
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Bis(2-chloroisopropyl)ether
0.25 0.39 12/3/14 14:03 CMRmg/Kg dry0.087 12/2/14SW-846 8270D1JBis(2-Ethylhexyl)phthalate
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.096 12/2/14SW-846 8270D14-Bromophenylphenylether
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Butylbenzylphthalate
ND 0.19 12/3/14 14:03 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Carbazole
ND 0.75 12/3/14 14:03 CMRmg/Kg dry0.19 12/2/14SW-846 8270D14-Chloroaniline
ND 0.75 12/3/14 14:03 CMRmg/Kg dry0.16 12/2/14SW-846 8270D14-Chloro-3-methylphenol
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Chloronaphthalene
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Chlorophenol
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.13 12/2/14SW-846 8270D14-Chlorophenylphenylether
ND 0.19 12/3/14 14:03 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Chrysene
ND 0.19 12/3/14 14:03 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1V-20Dibenz(a,h)anthracene
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.090 12/2/14SW-846 8270D1Dibenzofuran
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Di-n-butylphthalate
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.077 12/2/14SW-846 8270D11,2-Dichlorobenzene
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.091 12/2/14SW-846 8270D11,3-Dichlorobenzene
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.096 12/2/14SW-846 8270D11,4-Dichlorobenzene
ND 0.19 12/3/14 14:03 CMRmg/Kg dry0.18 12/2/14SW-846 8270D13,3-Dichlorobenzidine
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12,4-Dichlorophenol
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Diethylphthalate
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.11 12/2/14SW-846 8270D12,4-Dimethylphenol
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Dimethylphthalate
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-204,6-Dinitro-2-methylphenol
ND 0.75 12/3/14 14:03 CMRmg/Kg dry0.39 12/2/14SW-846 8270D1V-04, V-202,4-Dinitrophenol
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1V-202,4-Dinitrotoluene
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1V-202,6-Dinitrotoluene
ND 0.76 12/3/14 14:03 CMRmg/Kg dry0.53 12/2/14SW-846 8270D1Di-n-octylphthalate
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.19 12/2/14SW-846 8270D11,2-Diphenylhydrazine (as Azobenzene)
ND 0.19 12/3/14 14:03 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Fluoranthene
ND 0.19 12/3/14 14:03 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Fluorene
Page 12 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-01
Field Sample #: SB-1 3
Sample Matrix: Soil
Sampled: 11/26/2014 09:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Hexachlorobenzene
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Hexachlorobutadiene
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.26 12/2/14SW-846 8270D1Hexachlorocyclopentadiene
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Hexachloroethane
ND 0.19 12/3/14 14:03 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Isophorone
ND 0.19 12/3/14 14:03 CMRmg/Kg dry0.074 12/2/14SW-846 8270D11-Methylnaphthalene
ND 0.19 12/3/14 14:03 CMRmg/Kg dry0.10 12/2/14SW-846 8270D12-Methylnaphthalene
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Methylphenol
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.22 12/2/14SW-846 8270D13/4-Methylphenol
ND 0.19 12/3/14 14:03 CMRmg/Kg dry0.085 12/2/14SW-846 8270D1Naphthalene
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.27 12/2/14SW-846 8270D1V-202-Nitroaniline
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.18 12/2/14SW-846 8270D13-Nitroaniline
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.20 12/2/14SW-846 8270D14-Nitroaniline
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Nitrobenzene
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Nitrophenol
ND 0.75 12/3/14 14:03 CMRmg/Kg dry0.68 12/2/14SW-846 8270D14-Nitrophenol
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1N-Nitrosodimethylamine
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1N-Nitrosodiphenylamine
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.12 12/2/14SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.091 12/2/14SW-846 8270D1V-16, V-20Pentachloronitrobenzene
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Pentachlorophenol
ND 0.19 12/3/14 14:03 CMRmg/Kg dry0.10 12/2/14SW-846 8270D1Phenanthrene
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.10 12/2/14SW-846 8270D1Phenol
ND 0.19 12/3/14 14:03 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Pyrene
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Pyridine
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.23 12/2/14SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.093 12/2/14SW-846 8270D11,2,4-Trichlorobenzene
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.20 12/2/14SW-846 8270D12,4,5-Trichlorophenol
ND 0.39 12/3/14 14:03 CMRmg/Kg dry0.25 12/2/14SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 89.0 12/3/14 14:0330-130
Phenol-d6 99.9 12/3/14 14:0330-130
Nitrobenzene-d5 94.1 12/3/14 14:0330-130
2-Fluorobiphenyl 104 12/3/14 14:0330-130
2,4,6-Tribromophenol 130 12/3/14 14:03S-0730-130
p-Terphenyl-d14 128 12/3/14 14:0330-130
Page 13 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-01
Field Sample #: SB-1 3
Sample Matrix: Soil
Sampled: 11/26/2014 09:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 11 12/5/14 12:11 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C9-C18 Aliphatics
17 11 12/5/14 12:11 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C19-C36 Aliphatics
ND 11 12/5/14 12:11 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
ND 11 12/5/14 12:11 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)71.2 12/5/14 12:1140-140
o-Terphenyl (OTP)91.9 12/5/14 12:1140-140
2-Bromonaphthalene 86.6 12/5/14 12:1140-140
2-Fluorobiphenyl 87.9 12/5/14 12:1140-140
Page 14 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-01
Field Sample #: SB-1 3
Sample Matrix: Soil
Sampled: 11/26/2014 09:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.15
Petroleum Hydrocarbons Analyses - VPH
ND 11 12/8/14 19:22 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11Unadjusted C5-C8 Aliphatics
ND 11 12/8/14 19:22 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C5-C8 Aliphatics
ND 11 12/8/14 19:22 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11Unadjusted C9-C12 Aliphatics
ND 11 12/8/14 19:22 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C9-C12 Aliphatics
ND 11 12/8/14 19:22 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)95.2 12/8/14 19:2270-130
2,5-Dibromotoluene (PID)79.4 12/8/14 19:2270-130
Page 15 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-01
Field Sample #: SB-1 3
Sample Matrix: Soil
Sampled: 11/26/2014 09:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
87.8 12/8/14 7:48 MRL% Wt 12/4/14SM 2540G1% Solids
Page 16 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-02
Field Sample #: SB-2 3
Sample Matrix: Soil
Sampled: 11/26/2014 10:15
[TOC_2]14L0056-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.085 12/5/14 11:54 MFFmg/Kg dry0.020 12/4/14SW-846 8260B1Acetone
ND 0.0051 12/5/14 11:54 MFFmg/Kg dry0.0021 12/4/14SW-846 8260B1Acrylonitrile
ND 0.00085 12/5/14 11:54 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1Benzene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B1Bromobenzene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B1Bromochloromethane
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00051 12/4/14SW-846 8260B1Bromodichloromethane
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B1Bromoform
ND 0.0085 12/5/14 11:54 MFFmg/Kg dry0.0014 12/4/14SW-846 8260B1Bromomethane
ND 0.034 12/5/14 11:54 MFFmg/Kg dry0.015 12/4/14SW-846 8260B12-Butanone (MEK)
ND 0.034 12/5/14 11:54 MFFmg/Kg dry0.018 12/4/14SW-846 8260B1tert-Butyl Alcohol (TBA)
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1n-Butylbenzene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00085 12/4/14SW-846 8260B1sec-Butylbenzene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B1tert-Butylbenzene
ND 0.00085 12/5/14 11:54 MFFmg/Kg dry0.00051 12/4/14SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.0051 12/5/14 11:54 MFFmg/Kg dry0.0028 12/4/14SW-846 8260B1Carbon Disulfide
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B1Carbon Tetrachloride
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1Chlorobenzene
ND 0.00085 12/5/14 11:54 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1Chlorodibromomethane
ND 0.017 12/5/14 11:54 MFFmg/Kg dry0.0013 12/4/14SW-846 8260B1Chloroethane
ND 0.0034 12/5/14 11:54 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1Chloroform
ND 0.0085 12/5/14 11:54 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B1Chloromethane
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B12-Chlorotoluene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B14-Chlorotoluene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00093 12/4/14SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.00085 12/5/14 11:54 MFFmg/Kg dry0.00085 12/4/14SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00051 12/4/14SW-846 8260B1Dibromomethane
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B11,2-Dichlorobenzene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B11,3-Dichlorobenzene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B11,4-Dichlorobenzene
ND 0.0034 12/5/14 11:54 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.017 12/5/14 11:54 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B11,1-Dichloroethane
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B11,2-Dichloroethane
ND 0.0034 12/5/14 11:54 MFFmg/Kg dry0.00093 12/4/14SW-846 8260B11,1-Dichloroethylene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B11,2-Dichloropropane
ND 0.00085 12/5/14 11:54 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B11,3-Dichloropropane
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B12,2-Dichloropropane
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B11,1-Dichloropropene
ND 0.00085 12/5/14 11:54 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1cis-1,3-Dichloropropene
ND 0.00085 12/5/14 11:54 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1trans-1,3-Dichloropropene
ND 0.017 12/5/14 11:54 MFFmg/Kg dry0.0015 12/4/14SW-846 8260B1Diethyl Ether
Page 17 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-02
Field Sample #: SB-2 3
Sample Matrix: Soil
Sampled: 11/26/2014 10:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.00085 12/5/14 11:54 MFFmg/Kg dry0.00051 12/4/14SW-846 8260B1Diisopropyl Ether (DIPE)
ND 0.085 12/5/14 11:54 MFFmg/Kg dry0.049 12/4/14SW-846 8260B11,4-Dioxane
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B1Ethylbenzene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00085 12/4/14SW-846 8260B1Hexachlorobutadiene
ND 0.017 12/5/14 11:54 MFFmg/Kg dry0.0092 12/4/14SW-846 8260B12-Hexanone (MBK)
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.0034 12/5/14 11:54 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.017 12/5/14 11:54 MFFmg/Kg dry0.0060 12/4/14SW-846 8260B1Methylene Chloride
ND 0.017 12/5/14 11:54 MFFmg/Kg dry0.0064 12/4/14SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.0034 12/5/14 11:54 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1V-05Naphthalene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1R-05n-Propylbenzene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00051 12/4/14SW-846 8260B1Styrene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.00085 12/5/14 11:54 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B1Tetrachloroethylene
ND 0.0085 12/5/14 11:54 MFFmg/Kg dry0.0019 12/4/14SW-846 8260B1Tetrahydrofuran
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B1Toluene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00051 12/4/14SW-846 8260B1V-051,2,3-Trichlorobenzene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B1V-051,2,4-Trichlorobenzene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B11,3,5-Trichlorobenzene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00085 12/4/14SW-846 8260B11,1,1-Trichloroethane
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B11,1,2-Trichloroethane
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B1Trichloroethylene
ND 0.0085 12/5/14 11:54 MFFmg/Kg dry0.00093 12/4/14SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00093 12/4/14SW-846 8260B11,2,3-Trichloropropane
ND 0.0085 12/5/14 11:54 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00068 12/4/14SW-846 8260B11,2,4-Trimethylbenzene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00051 12/4/14SW-846 8260B11,3,5-Trimethylbenzene
ND 0.0085 12/5/14 11:54 MFFmg/Kg dry0.00093 12/4/14SW-846 8260B1Vinyl Chloride
ND 0.0034 12/5/14 11:54 MFFmg/Kg dry0.0014 12/4/14SW-846 8260B1m+p Xylene
ND 0.0017 12/5/14 11:54 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 99.2 12/5/14 11:5470-130
Toluene-d8 97.3 12/5/14 11:5470-130
4-Bromofluorobenzene 95.8 12/5/14 11:5470-130
Page 18 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-02
Field Sample #: SB-2 3
Sample Matrix: Soil
Sampled: 11/26/2014 10:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.20 12/3/14 14:27 CMRmg/Kg dry0.098 12/2/14SW-846 8270D1Acenaphthene
ND 0.20 12/3/14 14:27 CMRmg/Kg dry0.095 12/2/14SW-846 8270D1Acenaphthylene
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.095 12/2/14SW-846 8270D1Acetophenone
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.30 12/2/14SW-846 8270D1Aniline
ND 0.20 12/3/14 14:27 CMRmg/Kg dry0.12 12/2/14SW-846 8270D1Anthracene
ND 0.76 12/3/14 14:27 CMRmg/Kg dry0.53 12/2/14SW-846 8270D1V-04, V-05Benzidine
ND 0.20 12/3/14 14:27 CMRmg/Kg dry0.089 12/2/14SW-846 8270D1Benzo(a)anthracene
ND 0.20 12/3/14 14:27 CMRmg/Kg dry0.069 12/2/14SW-846 8270D1Benzo(a)pyrene
ND 0.20 12/3/14 14:27 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Benzo(b)fluoranthene
ND 0.20 12/3/14 14:27 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-20Benzo(g,h,i)perylene
ND 0.20 12/3/14 14:27 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Benzo(k)fluoranthene
ND 1.2 12/3/14 14:27 CMRmg/Kg dry1.1 12/2/14SW-846 8270D1Benzoic Acid
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Bis(2-chloroisopropyl)ether
0.25 0.39 12/3/14 14:27 CMRmg/Kg dry0.088 12/2/14SW-846 8270D1JBis(2-Ethylhexyl)phthalate
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.097 12/2/14SW-846 8270D14-Bromophenylphenylether
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Butylbenzylphthalate
ND 0.20 12/3/14 14:27 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Carbazole
ND 0.76 12/3/14 14:27 CMRmg/Kg dry0.19 12/2/14SW-846 8270D14-Chloroaniline
ND 0.76 12/3/14 14:27 CMRmg/Kg dry0.16 12/2/14SW-846 8270D14-Chloro-3-methylphenol
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Chloronaphthalene
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Chlorophenol
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.13 12/2/14SW-846 8270D14-Chlorophenylphenylether
ND 0.20 12/3/14 14:27 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Chrysene
ND 0.20 12/3/14 14:27 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1V-20Dibenz(a,h)anthracene
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.091 12/2/14SW-846 8270D1Dibenzofuran
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Di-n-butylphthalate
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.079 12/2/14SW-846 8270D11,2-Dichlorobenzene
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.092 12/2/14SW-846 8270D11,3-Dichlorobenzene
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.097 12/2/14SW-846 8270D11,4-Dichlorobenzene
ND 0.20 12/3/14 14:27 CMRmg/Kg dry0.18 12/2/14SW-846 8270D13,3-Dichlorobenzidine
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12,4-Dichlorophenol
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Diethylphthalate
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.11 12/2/14SW-846 8270D12,4-Dimethylphenol
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Dimethylphthalate
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-204,6-Dinitro-2-methylphenol
ND 0.76 12/3/14 14:27 CMRmg/Kg dry0.39 12/2/14SW-846 8270D1V-04, V-202,4-Dinitrophenol
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1V-202,4-Dinitrotoluene
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1V-202,6-Dinitrotoluene
ND 0.77 12/3/14 14:27 CMRmg/Kg dry0.54 12/2/14SW-846 8270D1Di-n-octylphthalate
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.19 12/2/14SW-846 8270D11,2-Diphenylhydrazine (as Azobenzene)
ND 0.20 12/3/14 14:27 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Fluoranthene
ND 0.20 12/3/14 14:27 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Fluorene
Page 19 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-02
Field Sample #: SB-2 3
Sample Matrix: Soil
Sampled: 11/26/2014 10:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Hexachlorobenzene
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Hexachlorobutadiene
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.26 12/2/14SW-846 8270D1Hexachlorocyclopentadiene
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Hexachloroethane
ND 0.20 12/3/14 14:27 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Isophorone
ND 0.20 12/3/14 14:27 CMRmg/Kg dry0.075 12/2/14SW-846 8270D11-Methylnaphthalene
ND 0.20 12/3/14 14:27 CMRmg/Kg dry0.10 12/2/14SW-846 8270D12-Methylnaphthalene
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Methylphenol
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.22 12/2/14SW-846 8270D13/4-Methylphenol
ND 0.20 12/3/14 14:27 CMRmg/Kg dry0.087 12/2/14SW-846 8270D1Naphthalene
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.27 12/2/14SW-846 8270D1V-202-Nitroaniline
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.18 12/2/14SW-846 8270D13-Nitroaniline
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.20 12/2/14SW-846 8270D14-Nitroaniline
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Nitrobenzene
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Nitrophenol
ND 0.76 12/3/14 14:27 CMRmg/Kg dry0.69 12/2/14SW-846 8270D14-Nitrophenol
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1N-Nitrosodimethylamine
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1N-Nitrosodiphenylamine
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.12 12/2/14SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.092 12/2/14SW-846 8270D1V-16, V-20Pentachloronitrobenzene
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Pentachlorophenol
0.11 0.20 12/3/14 14:27 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1JPhenanthrene
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.10 12/2/14SW-846 8270D1Phenol
ND 0.20 12/3/14 14:27 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Pyrene
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Pyridine
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.23 12/2/14SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.095 12/2/14SW-846 8270D11,2,4-Trichlorobenzene
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.20 12/2/14SW-846 8270D12,4,5-Trichlorophenol
ND 0.39 12/3/14 14:27 CMRmg/Kg dry0.25 12/2/14SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 82.0 12/3/14 14:2730-130
Phenol-d6 92.4 12/3/14 14:2730-130
Nitrobenzene-d5 88.0 12/3/14 14:2730-130
2-Fluorobiphenyl 95.0 12/3/14 14:2730-130
2,4,6-Tribromophenol 123 12/3/14 14:2730-130
p-Terphenyl-d14 129 12/3/14 14:2730-130
Page 20 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-02
Field Sample #: SB-2 3
Sample Matrix: Soil
Sampled: 11/26/2014 10:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 12 12/5/14 12:32 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C9-C18 Aliphatics
ND 12 12/5/14 12:32 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C19-C36 Aliphatics
ND 12 12/5/14 12:32 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
ND 12 12/5/14 12:32 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)70.9 12/5/14 12:3240-140
o-Terphenyl (OTP)89.9 12/5/14 12:3240-140
2-Bromonaphthalene 83.6 12/5/14 12:3240-140
2-Fluorobiphenyl 84.0 12/5/14 12:3240-140
Page 21 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-02
Field Sample #: SB-2 3
Sample Matrix: Soil
Sampled: 11/26/2014 10:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Sample Flags: O-01
Soil/Methanol Preservation Ratio: 1.42
Petroleum Hydrocarbons Analyses - VPH
ND 9.8 12/8/14 19:58 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11Unadjusted C5-C8 Aliphatics
ND 9.8 12/8/14 19:58 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C5-C8 Aliphatics
ND 9.8 12/8/14 19:58 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11Unadjusted C9-C12 Aliphatics
ND 9.8 12/8/14 19:58 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C9-C12 Aliphatics
ND 9.8 12/8/14 19:58 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)112 12/8/14 19:5870-130
2,5-Dibromotoluene (PID)96.1 12/8/14 19:5870-130
Page 22 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-02
Field Sample #: SB-2 3
Sample Matrix: Soil
Sampled: 11/26/2014 10:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
86.2 12/8/14 7:48 MRL% Wt 12/4/14SM 2540G1% Solids
Page 23 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-03
Field Sample #: SB-3 3
Sample Matrix: Soil
Sampled: 11/26/2014 10:40
[TOC_2]14L0056-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.090 12/5/14 12:22 MFFmg/Kg dry0.021 12/4/14SW-846 8260B1Acetone
ND 0.0054 12/5/14 12:22 MFFmg/Kg dry0.0023 12/4/14SW-846 8260B1Acrylonitrile
ND 0.00090 12/5/14 12:22 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1Benzene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B1Bromobenzene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.0013 12/4/14SW-846 8260B1Bromochloromethane
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00054 12/4/14SW-846 8260B1Bromodichloromethane
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.0013 12/4/14SW-846 8260B1Bromoform
ND 0.0090 12/5/14 12:22 MFFmg/Kg dry0.0015 12/4/14SW-846 8260B1Bromomethane
ND 0.036 12/5/14 12:22 MFFmg/Kg dry0.016 12/4/14SW-846 8260B12-Butanone (MEK)
ND 0.036 12/5/14 12:22 MFFmg/Kg dry0.019 12/4/14SW-846 8260B1tert-Butyl Alcohol (TBA)
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1n-Butylbenzene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00090 12/4/14SW-846 8260B1sec-Butylbenzene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00081 12/4/14SW-846 8260B1tert-Butylbenzene
ND 0.00090 12/5/14 12:22 MFFmg/Kg dry0.00054 12/4/14SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.0054 12/5/14 12:22 MFFmg/Kg dry0.0030 12/4/14SW-846 8260B1Carbon Disulfide
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B1Carbon Tetrachloride
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1Chlorobenzene
ND 0.00090 12/5/14 12:22 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1Chlorodibromomethane
ND 0.018 12/5/14 12:22 MFFmg/Kg dry0.0014 12/4/14SW-846 8260B1Chloroethane
ND 0.0036 12/5/14 12:22 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1Chloroform
ND 0.0090 12/5/14 12:22 MFFmg/Kg dry0.00081 12/4/14SW-846 8260B1Chloromethane
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B12-Chlorotoluene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B14-Chlorotoluene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00099 12/4/14SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.00090 12/5/14 12:22 MFFmg/Kg dry0.00090 12/4/14SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00054 12/4/14SW-846 8260B1Dibromomethane
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B11,2-Dichlorobenzene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B11,3-Dichlorobenzene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B11,4-Dichlorobenzene
ND 0.0036 12/5/14 12:22 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.018 12/5/14 12:22 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B11,1-Dichloroethane
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B11,2-Dichloroethane
ND 0.0036 12/5/14 12:22 MFFmg/Kg dry0.00099 12/4/14SW-846 8260B11,1-Dichloroethylene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00081 12/4/14SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B11,2-Dichloropropane
ND 0.00090 12/5/14 12:22 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B11,3-Dichloropropane
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00081 12/4/14SW-846 8260B12,2-Dichloropropane
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00081 12/4/14SW-846 8260B11,1-Dichloropropene
ND 0.00090 12/5/14 12:22 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1cis-1,3-Dichloropropene
ND 0.00090 12/5/14 12:22 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1trans-1,3-Dichloropropene
ND 0.018 12/5/14 12:22 MFFmg/Kg dry0.0016 12/4/14SW-846 8260B1Diethyl Ether
Page 24 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-03
Field Sample #: SB-3 3
Sample Matrix: Soil
Sampled: 11/26/2014 10:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.00090 12/5/14 12:22 MFFmg/Kg dry0.00054 12/4/14SW-846 8260B1Diisopropyl Ether (DIPE)
ND 0.090 12/5/14 12:22 MFFmg/Kg dry0.052 12/4/14SW-846 8260B11,4-Dioxane
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B1Ethylbenzene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00090 12/4/14SW-846 8260B1Hexachlorobutadiene
ND 0.018 12/5/14 12:22 MFFmg/Kg dry0.0098 12/4/14SW-846 8260B12-Hexanone (MBK)
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.0036 12/5/14 12:22 MFFmg/Kg dry0.00081 12/4/14SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.018 12/5/14 12:22 MFFmg/Kg dry0.0064 12/4/14SW-846 8260B1Methylene Chloride
ND 0.018 12/5/14 12:22 MFFmg/Kg dry0.0069 12/4/14SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.0036 12/5/14 12:22 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1V-05Naphthalene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1R-05n-Propylbenzene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00054 12/4/14SW-846 8260B1Styrene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00081 12/4/14SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.00090 12/5/14 12:22 MFFmg/Kg dry0.00081 12/4/14SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B1Tetrachloroethylene
ND 0.0090 12/5/14 12:22 MFFmg/Kg dry0.0020 12/4/14SW-846 8260B1Tetrahydrofuran
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B1Toluene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00054 12/4/14SW-846 8260B1V-051,2,3-Trichlorobenzene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B1V-051,2,4-Trichlorobenzene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B11,3,5-Trichlorobenzene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00090 12/4/14SW-846 8260B11,1,1-Trichloroethane
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B11,1,2-Trichloroethane
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00081 12/4/14SW-846 8260B1Trichloroethylene
ND 0.0090 12/5/14 12:22 MFFmg/Kg dry0.00099 12/4/14SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00099 12/4/14SW-846 8260B11,2,3-Trichloropropane
ND 0.0090 12/5/14 12:22 MFFmg/Kg dry0.00081 12/4/14SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B11,2,4-Trimethylbenzene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00054 12/4/14SW-846 8260B11,3,5-Trimethylbenzene
ND 0.0090 12/5/14 12:22 MFFmg/Kg dry0.00099 12/4/14SW-846 8260B1Vinyl Chloride
ND 0.0036 12/5/14 12:22 MFFmg/Kg dry0.0015 12/4/14SW-846 8260B1m+p Xylene
ND 0.0018 12/5/14 12:22 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 101 12/5/14 12:2270-130
Toluene-d8 97.8 12/5/14 12:2270-130
4-Bromofluorobenzene 94.8 12/5/14 12:2270-130
Page 25 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-03
Field Sample #: SB-3 3
Sample Matrix: Soil
Sampled: 11/26/2014 10:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.20 12/3/14 14:52 CMRmg/Kg dry0.098 12/2/14SW-846 8270D1Acenaphthene
ND 0.20 12/3/14 14:52 CMRmg/Kg dry0.094 12/2/14SW-846 8270D1Acenaphthylene
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.094 12/2/14SW-846 8270D1Acetophenone
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.30 12/2/14SW-846 8270D1Aniline
ND 0.20 12/3/14 14:52 CMRmg/Kg dry0.12 12/2/14SW-846 8270D1Anthracene
ND 0.76 12/3/14 14:52 CMRmg/Kg dry0.53 12/2/14SW-846 8270D1V-04, V-05Benzidine
ND 0.20 12/3/14 14:52 CMRmg/Kg dry0.089 12/2/14SW-846 8270D1Benzo(a)anthracene
ND 0.20 12/3/14 14:52 CMRmg/Kg dry0.069 12/2/14SW-846 8270D1Benzo(a)pyrene
ND 0.20 12/3/14 14:52 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Benzo(b)fluoranthene
ND 0.20 12/3/14 14:52 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-20Benzo(g,h,i)perylene
ND 0.20 12/3/14 14:52 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Benzo(k)fluoranthene
ND 1.2 12/3/14 14:52 CMRmg/Kg dry1.1 12/2/14SW-846 8270D1Benzoic Acid
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Bis(2-chloroisopropyl)ether
0.24 0.39 12/3/14 14:52 CMRmg/Kg dry0.087 12/2/14SW-846 8270D1JBis(2-Ethylhexyl)phthalate
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.097 12/2/14SW-846 8270D14-Bromophenylphenylether
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Butylbenzylphthalate
ND 0.20 12/3/14 14:52 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Carbazole
ND 0.76 12/3/14 14:52 CMRmg/Kg dry0.19 12/2/14SW-846 8270D14-Chloroaniline
ND 0.76 12/3/14 14:52 CMRmg/Kg dry0.16 12/2/14SW-846 8270D14-Chloro-3-methylphenol
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Chloronaphthalene
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Chlorophenol
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.13 12/2/14SW-846 8270D14-Chlorophenylphenylether
ND 0.20 12/3/14 14:52 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Chrysene
ND 0.20 12/3/14 14:52 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1V-20Dibenz(a,h)anthracene
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.091 12/2/14SW-846 8270D1Dibenzofuran
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Di-n-butylphthalate
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.078 12/2/14SW-846 8270D11,2-Dichlorobenzene
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.092 12/2/14SW-846 8270D11,3-Dichlorobenzene
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.097 12/2/14SW-846 8270D11,4-Dichlorobenzene
ND 0.20 12/3/14 14:52 CMRmg/Kg dry0.18 12/2/14SW-846 8270D13,3-Dichlorobenzidine
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12,4-Dichlorophenol
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Diethylphthalate
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.11 12/2/14SW-846 8270D12,4-Dimethylphenol
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Dimethylphthalate
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-204,6-Dinitro-2-methylphenol
ND 0.76 12/3/14 14:52 CMRmg/Kg dry0.39 12/2/14SW-846 8270D1V-04, V-202,4-Dinitrophenol
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1V-202,4-Dinitrotoluene
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1V-202,6-Dinitrotoluene
ND 0.77 12/3/14 14:52 CMRmg/Kg dry0.53 12/2/14SW-846 8270D1Di-n-octylphthalate
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.19 12/2/14SW-846 8270D11,2-Diphenylhydrazine (as Azobenzene)
ND 0.20 12/3/14 14:52 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Fluoranthene
ND 0.20 12/3/14 14:52 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Fluorene
Page 26 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-03
Field Sample #: SB-3 3
Sample Matrix: Soil
Sampled: 11/26/2014 10:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Hexachlorobenzene
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Hexachlorobutadiene
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.26 12/2/14SW-846 8270D1Hexachlorocyclopentadiene
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Hexachloroethane
ND 0.20 12/3/14 14:52 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Isophorone
ND 0.20 12/3/14 14:52 CMRmg/Kg dry0.075 12/2/14SW-846 8270D11-Methylnaphthalene
ND 0.20 12/3/14 14:52 CMRmg/Kg dry0.10 12/2/14SW-846 8270D12-Methylnaphthalene
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Methylphenol
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.22 12/2/14SW-846 8270D13/4-Methylphenol
ND 0.20 12/3/14 14:52 CMRmg/Kg dry0.086 12/2/14SW-846 8270D1Naphthalene
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.27 12/2/14SW-846 8270D1V-202-Nitroaniline
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.18 12/2/14SW-846 8270D13-Nitroaniline
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.20 12/2/14SW-846 8270D14-Nitroaniline
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Nitrobenzene
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Nitrophenol
ND 0.76 12/3/14 14:52 CMRmg/Kg dry0.69 12/2/14SW-846 8270D14-Nitrophenol
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1N-Nitrosodimethylamine
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1N-Nitrosodiphenylamine
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.12 12/2/14SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.092 12/2/14SW-846 8270D1V-16, V-20Pentachloronitrobenzene
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Pentachlorophenol
ND 0.20 12/3/14 14:52 CMRmg/Kg dry0.10 12/2/14SW-846 8270D1Phenanthrene
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.10 12/2/14SW-846 8270D1Phenol
ND 0.20 12/3/14 14:52 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Pyrene
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Pyridine
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.23 12/2/14SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.094 12/2/14SW-846 8270D11,2,4-Trichlorobenzene
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.20 12/2/14SW-846 8270D12,4,5-Trichlorophenol
ND 0.39 12/3/14 14:52 CMRmg/Kg dry0.25 12/2/14SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 92.1 12/3/14 14:5230-130
Phenol-d6 101 12/3/14 14:5230-130
Nitrobenzene-d5 96.6 12/3/14 14:5230-130
2-Fluorobiphenyl 99.8 12/3/14 14:5230-130
2,4,6-Tribromophenol 121 12/3/14 14:5230-130
p-Terphenyl-d14 125 12/3/14 14:5230-130
Page 27 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-03
Field Sample #: SB-3 3
Sample Matrix: Soil
Sampled: 11/26/2014 10:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 12 12/5/14 12:53 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C9-C18 Aliphatics
ND 12 12/5/14 12:53 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C19-C36 Aliphatics
ND 12 12/5/14 12:53 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
ND 12 12/5/14 12:53 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)70.9 12/5/14 12:5340-140
o-Terphenyl (OTP)93.1 12/5/14 12:5340-140
2-Bromonaphthalene 92.2 12/5/14 12:5340-140
2-Fluorobiphenyl 93.2 12/5/14 12:5340-140
Page 28 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-03
Field Sample #: SB-3 3
Sample Matrix: Soil
Sampled: 11/26/2014 10:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Sample Flags: O-01
Soil/Methanol Preservation Ratio: 1.35
Petroleum Hydrocarbons Analyses - VPH
ND 10 12/8/14 20:34 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11Unadjusted C5-C8 Aliphatics
ND 10 12/8/14 20:34 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C5-C8 Aliphatics
ND 10 12/8/14 20:34 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11Unadjusted C9-C12 Aliphatics
ND 10 12/8/14 20:34 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C9-C12 Aliphatics
ND 10 12/8/14 20:34 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)117 12/8/14 20:3470-130
2,5-Dibromotoluene (PID)97.5 12/8/14 20:3470-130
Page 29 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-03
Field Sample #: SB-3 3
Sample Matrix: Soil
Sampled: 11/26/2014 10:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
85.8 12/8/14 7:48 MRL% Wt 12/4/14SM 2540G1% Solids
Page 30 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-04
Field Sample #: SB-4 3
Sample Matrix: Soil
Sampled: 11/26/2014 11:00
[TOC_2]14L0056-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.10 12/5/14 12:49 MFFmg/Kg dry0.024 12/4/14SW-846 8260B1Acetone
ND 0.0063 12/5/14 12:49 MFFmg/Kg dry0.0026 12/4/14SW-846 8260B1Acrylonitrile
ND 0.0010 12/5/14 12:49 MFFmg/Kg dry0.00073 12/4/14SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00073 12/4/14SW-846 8260B1Benzene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00084 12/4/14SW-846 8260B1Bromobenzene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.0015 12/4/14SW-846 8260B1Bromochloromethane
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1Bromodichloromethane
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.0015 12/4/14SW-846 8260B1Bromoform
ND 0.010 12/5/14 12:49 MFFmg/Kg dry0.0018 12/4/14SW-846 8260B1Bromomethane
ND 0.042 12/5/14 12:49 MFFmg/Kg dry0.018 12/4/14SW-846 8260B12-Butanone (MEK)
ND 0.042 12/5/14 12:49 MFFmg/Kg dry0.022 12/4/14SW-846 8260B1tert-Butyl Alcohol (TBA)
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00073 12/4/14SW-846 8260B1n-Butylbenzene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B1sec-Butylbenzene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00094 12/4/14SW-846 8260B1tert-Butylbenzene
ND 0.0010 12/5/14 12:49 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.0063 12/5/14 12:49 MFFmg/Kg dry0.0035 12/4/14SW-846 8260B1Carbon Disulfide
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00084 12/4/14SW-846 8260B1Carbon Tetrachloride
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00073 12/4/14SW-846 8260B1Chlorobenzene
ND 0.0010 12/5/14 12:49 MFFmg/Kg dry0.00073 12/4/14SW-846 8260B1Chlorodibromomethane
ND 0.021 12/5/14 12:49 MFFmg/Kg dry0.0016 12/4/14SW-846 8260B1Chloroethane
ND 0.0042 12/5/14 12:49 MFFmg/Kg dry0.00073 12/4/14SW-846 8260B1Chloroform
ND 0.010 12/5/14 12:49 MFFmg/Kg dry0.00094 12/4/14SW-846 8260B1Chloromethane
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00084 12/4/14SW-846 8260B12-Chlorotoluene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00084 12/4/14SW-846 8260B14-Chlorotoluene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0010 12/5/14 12:49 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1Dibromomethane
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00073 12/4/14SW-846 8260B11,2-Dichlorobenzene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00073 12/4/14SW-846 8260B11,3-Dichlorobenzene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00084 12/4/14SW-846 8260B11,4-Dichlorobenzene
ND 0.0042 12/5/14 12:49 MFFmg/Kg dry0.0013 12/4/14SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.021 12/5/14 12:49 MFFmg/Kg dry0.0014 12/4/14SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00073 12/4/14SW-846 8260B11,1-Dichloroethane
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.0014 12/4/14SW-846 8260B11,2-Dichloroethane
ND 0.0042 12/5/14 12:49 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B11,1-Dichloroethylene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00084 12/4/14SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00094 12/4/14SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.0014 12/4/14SW-846 8260B11,2-Dichloropropane
ND 0.0010 12/5/14 12:49 MFFmg/Kg dry0.00073 12/4/14SW-846 8260B11,3-Dichloropropane
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00094 12/4/14SW-846 8260B12,2-Dichloropropane
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00094 12/4/14SW-846 8260B11,1-Dichloropropene
ND 0.0010 12/5/14 12:49 MFFmg/Kg dry0.00073 12/4/14SW-846 8260B1cis-1,3-Dichloropropene
ND 0.0010 12/5/14 12:49 MFFmg/Kg dry0.00073 12/4/14SW-846 8260B1trans-1,3-Dichloropropene
ND 0.021 12/5/14 12:49 MFFmg/Kg dry0.0019 12/4/14SW-846 8260B1Diethyl Ether
Page 31 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-04
Field Sample #: SB-4 3
Sample Matrix: Soil
Sampled: 11/26/2014 11:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0010 12/5/14 12:49 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1Diisopropyl Ether (DIPE)
ND 0.10 12/5/14 12:49 MFFmg/Kg dry0.060 12/4/14SW-846 8260B11,4-Dioxane
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00084 12/4/14SW-846 8260B1Ethylbenzene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B1Hexachlorobutadiene
ND 0.021 12/5/14 12:49 MFFmg/Kg dry0.011 12/4/14SW-846 8260B12-Hexanone (MBK)
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00073 12/4/14SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00084 12/4/14SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.0042 12/5/14 12:49 MFFmg/Kg dry0.00094 12/4/14SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.021 12/5/14 12:49 MFFmg/Kg dry0.0074 12/4/14SW-846 8260B1Methylene Chloride
ND 0.021 12/5/14 12:49 MFFmg/Kg dry0.0080 12/4/14SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.0042 12/5/14 12:49 MFFmg/Kg dry0.00073 12/4/14SW-846 8260B1V-05Naphthalene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00073 12/4/14SW-846 8260B1R-05n-Propylbenzene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1Styrene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00094 12/4/14SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.0010 12/5/14 12:49 MFFmg/Kg dry0.00094 12/4/14SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.0014 12/4/14SW-846 8260B1Tetrachloroethylene
ND 0.010 12/5/14 12:49 MFFmg/Kg dry0.0023 12/4/14SW-846 8260B1Tetrahydrofuran
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00084 12/4/14SW-846 8260B1Toluene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1V-051,2,3-Trichlorobenzene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00084 12/4/14SW-846 8260B1V-051,2,4-Trichlorobenzene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00073 12/4/14SW-846 8260B11,3,5-Trichlorobenzene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B11,1,1-Trichloroethane
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.0013 12/4/14SW-846 8260B11,1,2-Trichloroethane
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00094 12/4/14SW-846 8260B1Trichloroethylene
ND 0.010 12/5/14 12:49 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B11,2,3-Trichloropropane
ND 0.010 12/5/14 12:49 MFFmg/Kg dry0.00094 12/4/14SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00084 12/4/14SW-846 8260B11,2,4-Trimethylbenzene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B11,3,5-Trimethylbenzene
ND 0.010 12/5/14 12:49 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B1Vinyl Chloride
ND 0.0042 12/5/14 12:49 MFFmg/Kg dry0.0018 12/4/14SW-846 8260B1m+p Xylene
ND 0.0021 12/5/14 12:49 MFFmg/Kg dry0.00073 12/4/14SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 98.3 12/5/14 12:4970-130
Toluene-d8 96.9 12/5/14 12:4970-130
4-Bromofluorobenzene 94.6 12/5/14 12:4970-130
Page 32 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-04
Field Sample #: SB-4 3
Sample Matrix: Soil
Sampled: 11/26/2014 11:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.20 12/3/14 15:16 CMRmg/Kg dry0.099 12/2/14SW-846 8270D1Acenaphthene
ND 0.20 12/3/14 15:16 CMRmg/Kg dry0.096 12/2/14SW-846 8270D1Acenaphthylene
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.096 12/2/14SW-846 8270D1Acetophenone
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.30 12/2/14SW-846 8270D1Aniline
ND 0.20 12/3/14 15:16 CMRmg/Kg dry0.12 12/2/14SW-846 8270D1Anthracene
ND 0.77 12/3/14 15:16 CMRmg/Kg dry0.54 12/2/14SW-846 8270D1V-04, V-05Benzidine
ND 0.20 12/3/14 15:16 CMRmg/Kg dry0.090 12/2/14SW-846 8270D1Benzo(a)anthracene
ND 0.20 12/3/14 15:16 CMRmg/Kg dry0.070 12/2/14SW-846 8270D1Benzo(a)pyrene
ND 0.20 12/3/14 15:16 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Benzo(b)fluoranthene
ND 0.20 12/3/14 15:16 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-20Benzo(g,h,i)perylene
ND 0.20 12/3/14 15:16 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Benzo(k)fluoranthene
ND 1.2 12/3/14 15:16 CMRmg/Kg dry1.1 12/2/14SW-846 8270D1Benzoic Acid
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Bis(2-chloroisopropyl)ether
0.21 0.40 12/3/14 15:16 CMRmg/Kg dry0.089 12/2/14SW-846 8270D1JBis(2-Ethylhexyl)phthalate
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.098 12/2/14SW-846 8270D14-Bromophenylphenylether
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Butylbenzylphthalate
ND 0.20 12/3/14 15:16 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Carbazole
ND 0.77 12/3/14 15:16 CMRmg/Kg dry0.19 12/2/14SW-846 8270D14-Chloroaniline
ND 0.77 12/3/14 15:16 CMRmg/Kg dry0.16 12/2/14SW-846 8270D14-Chloro-3-methylphenol
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Chloronaphthalene
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Chlorophenol
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.13 12/2/14SW-846 8270D14-Chlorophenylphenylether
ND 0.20 12/3/14 15:16 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Chrysene
ND 0.20 12/3/14 15:16 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1V-20Dibenz(a,h)anthracene
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.092 12/2/14SW-846 8270D1Dibenzofuran
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Di-n-butylphthalate
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.079 12/2/14SW-846 8270D11,2-Dichlorobenzene
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.093 12/2/14SW-846 8270D11,3-Dichlorobenzene
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.098 12/2/14SW-846 8270D11,4-Dichlorobenzene
ND 0.20 12/3/14 15:16 CMRmg/Kg dry0.18 12/2/14SW-846 8270D13,3-Dichlorobenzidine
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12,4-Dichlorophenol
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Diethylphthalate
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.11 12/2/14SW-846 8270D12,4-Dimethylphenol
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Dimethylphthalate
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-204,6-Dinitro-2-methylphenol
ND 0.77 12/3/14 15:16 CMRmg/Kg dry0.40 12/2/14SW-846 8270D1V-04, V-202,4-Dinitrophenol
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-202,4-Dinitrotoluene
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1V-202,6-Dinitrotoluene
ND 0.78 12/3/14 15:16 CMRmg/Kg dry0.54 12/2/14SW-846 8270D1Di-n-octylphthalate
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.19 12/2/14SW-846 8270D11,2-Diphenylhydrazine (as Azobenzene)
0.20 0.20 12/3/14 15:16 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Fluoranthene
ND 0.20 12/3/14 15:16 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Fluorene
Page 33 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-04
Field Sample #: SB-4 3
Sample Matrix: Soil
Sampled: 11/26/2014 11:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Hexachlorobenzene
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Hexachlorobutadiene
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.26 12/2/14SW-846 8270D1Hexachlorocyclopentadiene
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Hexachloroethane
ND 0.20 12/3/14 15:16 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Isophorone
ND 0.20 12/3/14 15:16 CMRmg/Kg dry0.076 12/2/14SW-846 8270D11-Methylnaphthalene
ND 0.20 12/3/14 15:16 CMRmg/Kg dry0.11 12/2/14SW-846 8270D12-Methylnaphthalene
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Methylphenol
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.22 12/2/14SW-846 8270D13/4-Methylphenol
ND 0.20 12/3/14 15:16 CMRmg/Kg dry0.088 12/2/14SW-846 8270D1Naphthalene
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.28 12/2/14SW-846 8270D1V-202-Nitroaniline
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.18 12/2/14SW-846 8270D13-Nitroaniline
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.20 12/2/14SW-846 8270D14-Nitroaniline
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Nitrobenzene
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Nitrophenol
ND 0.77 12/3/14 15:16 CMRmg/Kg dry0.70 12/2/14SW-846 8270D14-Nitrophenol
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1N-Nitrosodimethylamine
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1N-Nitrosodiphenylamine
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.093 12/2/14SW-846 8270D1V-16, V-20Pentachloronitrobenzene
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Pentachlorophenol
0.24 0.20 12/3/14 15:16 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Phenanthrene
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Phenol
0.16 0.20 12/3/14 15:16 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1JPyrene
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Pyridine
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.23 12/2/14SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.096 12/2/14SW-846 8270D11,2,4-Trichlorobenzene
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.21 12/2/14SW-846 8270D12,4,5-Trichlorophenol
ND 0.40 12/3/14 15:16 CMRmg/Kg dry0.26 12/2/14SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 90.6 12/3/14 15:1630-130
Phenol-d6 103 12/3/14 15:1630-130
Nitrobenzene-d5 97.0 12/3/14 15:1630-130
2-Fluorobiphenyl 102 12/3/14 15:1630-130
2,4,6-Tribromophenol 126 12/3/14 15:1630-130
p-Terphenyl-d14 122 12/3/14 15:1630-130
Page 34 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-04
Field Sample #: SB-4 3
Sample Matrix: Soil
Sampled: 11/26/2014 11:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 12 12/5/14 13:14 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C9-C18 Aliphatics
ND 12 12/5/14 13:14 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C19-C36 Aliphatics
ND 12 12/5/14 13:14 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
ND 12 12/5/14 13:14 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)73.3 12/5/14 13:1440-140
o-Terphenyl (OTP)89.3 12/5/14 13:1440-140
2-Bromonaphthalene 84.4 12/5/14 13:1440-140
2-Fluorobiphenyl 85.5 12/5/14 13:1440-140
Page 35 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-04
Field Sample #: SB-4 3
Sample Matrix: Soil
Sampled: 11/26/2014 11:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Sample Flags: O-01
Soil/Methanol Preservation Ratio: 1.41
Petroleum Hydrocarbons Analyses - VPH
ND 10 12/8/14 21:10 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11Unadjusted C5-C8 Aliphatics
ND 10 12/8/14 21:10 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C5-C8 Aliphatics
ND 10 12/8/14 21:10 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11Unadjusted C9-C12 Aliphatics
ND 10 12/8/14 21:10 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C9-C12 Aliphatics
ND 10 12/8/14 21:10 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)113 12/8/14 21:1070-130
2,5-Dibromotoluene (PID)99.8 12/8/14 21:1070-130
Page 36 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-04
Field Sample #: SB-4 3
Sample Matrix: Soil
Sampled: 11/26/2014 11:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
85.6 12/8/14 7:48 MRL% Wt 12/4/14SM 2540G1% Solids
Page 37 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-05
Field Sample #: SB-5 3
Sample Matrix: Soil
Sampled: 11/26/2014 11:25
[TOC_2]14L0056-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.13 12/5/14 13:17 MFFmg/Kg dry0.030 12/4/14SW-846 8260B1Acetone
ND 0.0076 12/5/14 13:17 MFFmg/Kg dry0.0032 12/4/14SW-846 8260B1Acrylonitrile
ND 0.0013 12/5/14 13:17 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B1Benzene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B1Bromobenzene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0018 12/4/14SW-846 8260B1Bromochloromethane
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B1Bromodichloromethane
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0018 12/4/14SW-846 8260B1Bromoform
ND 0.013 12/5/14 13:17 MFFmg/Kg dry0.0022 12/4/14SW-846 8260B1Bromomethane
ND 0.051 12/5/14 13:17 MFFmg/Kg dry0.022 12/4/14SW-846 8260B12-Butanone (MEK)
ND 0.051 12/5/14 13:17 MFFmg/Kg dry0.027 12/4/14SW-846 8260B1tert-Butyl Alcohol (TBA)
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B1n-Butylbenzene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0013 12/4/14SW-846 8260B1sec-Butylbenzene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B1tert-Butylbenzene
ND 0.0013 12/5/14 13:17 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.0076 12/5/14 13:17 MFFmg/Kg dry0.0042 12/4/14SW-846 8260B1Carbon Disulfide
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B1Carbon Tetrachloride
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B1Chlorobenzene
ND 0.0013 12/5/14 13:17 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B1Chlorodibromomethane
ND 0.025 12/5/14 13:17 MFFmg/Kg dry0.0019 12/4/14SW-846 8260B1Chloroethane
ND 0.0051 12/5/14 13:17 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B1Chloroform
ND 0.013 12/5/14 13:17 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B1Chloromethane
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B12-Chlorotoluene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B14-Chlorotoluene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0014 12/4/14SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.0013 12/5/14 13:17 MFFmg/Kg dry0.0013 12/4/14SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B1Dibromomethane
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B11,2-Dichlorobenzene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B11,3-Dichlorobenzene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B11,4-Dichlorobenzene
ND 0.0051 12/5/14 13:17 MFFmg/Kg dry0.0015 12/4/14SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.025 12/5/14 13:17 MFFmg/Kg dry0.0017 12/4/14SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B11,1-Dichloroethane
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0017 12/4/14SW-846 8260B11,2-Dichloroethane
ND 0.0051 12/5/14 13:17 MFFmg/Kg dry0.0014 12/4/14SW-846 8260B11,1-Dichloroethylene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0017 12/4/14SW-846 8260B11,2-Dichloropropane
ND 0.0013 12/5/14 13:17 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B11,3-Dichloropropane
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B12,2-Dichloropropane
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B11,1-Dichloropropene
ND 0.0013 12/5/14 13:17 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B1cis-1,3-Dichloropropene
ND 0.0013 12/5/14 13:17 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B1trans-1,3-Dichloropropene
ND 0.025 12/5/14 13:17 MFFmg/Kg dry0.0023 12/4/14SW-846 8260B1Diethyl Ether
Page 38 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-05
Field Sample #: SB-5 3
Sample Matrix: Soil
Sampled: 11/26/2014 11:25
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.0013 12/5/14 13:17 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B1Diisopropyl Ether (DIPE)
ND 0.13 12/5/14 13:17 MFFmg/Kg dry0.073 12/4/14SW-846 8260B11,4-Dioxane
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B1Ethylbenzene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0013 12/4/14SW-846 8260B1Hexachlorobutadiene
ND 0.025 12/5/14 13:17 MFFmg/Kg dry0.014 12/4/14SW-846 8260B12-Hexanone (MBK)
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.0051 12/5/14 13:17 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.025 12/5/14 13:17 MFFmg/Kg dry0.0090 12/4/14SW-846 8260B1Methylene Chloride
ND 0.025 12/5/14 13:17 MFFmg/Kg dry0.0097 12/4/14SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.0051 12/5/14 13:17 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B1V-05Naphthalene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B1R-05n-Propylbenzene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B1Styrene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.0013 12/5/14 13:17 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0017 12/4/14SW-846 8260B1Tetrachloroethylene
ND 0.013 12/5/14 13:17 MFFmg/Kg dry0.0028 12/4/14SW-846 8260B1Tetrahydrofuran
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B1Toluene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B1V-051,2,3-Trichlorobenzene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B1V-051,2,4-Trichlorobenzene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B11,3,5-Trichlorobenzene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0013 12/4/14SW-846 8260B11,1,1-Trichloroethane
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0015 12/4/14SW-846 8260B11,1,2-Trichloroethane
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B1Trichloroethylene
ND 0.013 12/5/14 13:17 MFFmg/Kg dry0.0014 12/4/14SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0014 12/4/14SW-846 8260B11,2,3-Trichloropropane
ND 0.013 12/5/14 13:17 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B11,2,4-Trimethylbenzene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.00076 12/4/14SW-846 8260B11,3,5-Trimethylbenzene
ND 0.013 12/5/14 13:17 MFFmg/Kg dry0.0014 12/4/14SW-846 8260B1Vinyl Chloride
ND 0.0051 12/5/14 13:17 MFFmg/Kg dry0.0022 12/4/14SW-846 8260B1m+p Xylene
ND 0.0025 12/5/14 13:17 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 100 12/5/14 13:1770-130
Toluene-d8 97.9 12/5/14 13:1770-130
4-Bromofluorobenzene 89.8 12/5/14 13:1770-130
Page 39 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-05
Field Sample #: SB-5 3
Sample Matrix: Soil
Sampled: 11/26/2014 11:25
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.20 12/3/14 15:39 CMRmg/Kg dry0.10 12/2/14SW-846 8270D1Acenaphthene
ND 0.20 12/3/14 15:39 CMRmg/Kg dry0.097 12/2/14SW-846 8270D1Acenaphthylene
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.097 12/2/14SW-846 8270D1Acetophenone
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.31 12/2/14SW-846 8270D1Aniline
ND 0.20 12/3/14 15:39 CMRmg/Kg dry0.12 12/2/14SW-846 8270D1Anthracene
ND 0.78 12/3/14 15:39 CMRmg/Kg dry0.55 12/2/14SW-846 8270D1V-04, V-05Benzidine
ND 0.20 12/3/14 15:39 CMRmg/Kg dry0.091 12/2/14SW-846 8270D1Benzo(a)anthracene
ND 0.20 12/3/14 15:39 CMRmg/Kg dry0.071 12/2/14SW-846 8270D1Benzo(a)pyrene
ND 0.20 12/3/14 15:39 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Benzo(b)fluoranthene
ND 0.20 12/3/14 15:39 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-20Benzo(g,h,i)perylene
ND 0.20 12/3/14 15:39 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Benzo(k)fluoranthene
ND 1.2 12/3/14 15:39 CMRmg/Kg dry1.1 12/2/14SW-846 8270D1Benzoic Acid
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Bis(2-chloroisopropyl)ether
0.25 0.40 12/3/14 15:39 CMRmg/Kg dry0.090 12/2/14SW-846 8270D1JBis(2-Ethylhexyl)phthalate
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.10 12/2/14SW-846 8270D14-Bromophenylphenylether
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Butylbenzylphthalate
ND 0.20 12/3/14 15:39 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Carbazole
ND 0.78 12/3/14 15:39 CMRmg/Kg dry0.20 12/2/14SW-846 8270D14-Chloroaniline
ND 0.78 12/3/14 15:39 CMRmg/Kg dry0.17 12/2/14SW-846 8270D14-Chloro-3-methylphenol
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.13 12/2/14SW-846 8270D12-Chloronaphthalene
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Chlorophenol
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.14 12/2/14SW-846 8270D14-Chlorophenylphenylether
ND 0.20 12/3/14 15:39 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Chrysene
ND 0.20 12/3/14 15:39 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1V-20Dibenz(a,h)anthracene
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.094 12/2/14SW-846 8270D1Dibenzofuran
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Di-n-butylphthalate
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.081 12/2/14SW-846 8270D11,2-Dichlorobenzene
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.095 12/2/14SW-846 8270D11,3-Dichlorobenzene
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.10 12/2/14SW-846 8270D11,4-Dichlorobenzene
ND 0.20 12/3/14 15:39 CMRmg/Kg dry0.18 12/2/14SW-846 8270D13,3-Dichlorobenzidine
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12,4-Dichlorophenol
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Diethylphthalate
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12,4-Dimethylphenol
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Dimethylphthalate
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1V-204,6-Dinitro-2-methylphenol
ND 0.78 12/3/14 15:39 CMRmg/Kg dry0.40 12/2/14SW-846 8270D1V-04, V-202,4-Dinitrophenol
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-202,4-Dinitrotoluene
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1V-202,6-Dinitrotoluene
ND 0.79 12/3/14 15:39 CMRmg/Kg dry0.55 12/2/14SW-846 8270D1Di-n-octylphthalate
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.19 12/2/14SW-846 8270D11,2-Diphenylhydrazine (as Azobenzene)
ND 0.20 12/3/14 15:39 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Fluoranthene
ND 0.20 12/3/14 15:39 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Fluorene
Page 40 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-05
Field Sample #: SB-5 3
Sample Matrix: Soil
Sampled: 11/26/2014 11:25
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Hexachlorobenzene
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Hexachlorobutadiene
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.27 12/2/14SW-846 8270D1Hexachlorocyclopentadiene
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Hexachloroethane
ND 0.20 12/3/14 15:39 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.12 12/2/14SW-846 8270D1Isophorone
ND 0.20 12/3/14 15:39 CMRmg/Kg dry0.077 12/2/14SW-846 8270D11-Methylnaphthalene
ND 0.20 12/3/14 15:39 CMRmg/Kg dry0.11 12/2/14SW-846 8270D12-Methylnaphthalene
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.13 12/2/14SW-846 8270D12-Methylphenol
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.22 12/2/14SW-846 8270D13/4-Methylphenol
ND 0.20 12/3/14 15:39 CMRmg/Kg dry0.089 12/2/14SW-846 8270D1Naphthalene
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.28 12/2/14SW-846 8270D1V-202-Nitroaniline
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.18 12/2/14SW-846 8270D13-Nitroaniline
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.21 12/2/14SW-846 8270D14-Nitroaniline
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Nitrobenzene
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Nitrophenol
ND 0.78 12/3/14 15:39 CMRmg/Kg dry0.71 12/2/14SW-846 8270D14-Nitrophenol
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1N-Nitrosodimethylamine
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.19 12/2/14SW-846 8270D1N-Nitrosodiphenylamine
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.095 12/2/14SW-846 8270D1V-16, V-20Pentachloronitrobenzene
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Pentachlorophenol
ND 0.20 12/3/14 15:39 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Phenanthrene
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Phenol
ND 0.20 12/3/14 15:39 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Pyrene
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Pyridine
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.24 12/2/14SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.097 12/2/14SW-846 8270D11,2,4-Trichlorobenzene
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.21 12/2/14SW-846 8270D12,4,5-Trichlorophenol
ND 0.40 12/3/14 15:39 CMRmg/Kg dry0.26 12/2/14SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 88.0 12/3/14 15:3930-130
Phenol-d6 96.5 12/3/14 15:3930-130
Nitrobenzene-d5 93.0 12/3/14 15:3930-130
2-Fluorobiphenyl 95.0 12/3/14 15:3930-130
2,4,6-Tribromophenol 116 12/3/14 15:3930-130
p-Terphenyl-d14 120 12/3/14 15:3930-130
Page 41 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-05
Field Sample #: SB-5 3
Sample Matrix: Soil
Sampled: 11/26/2014 11:25
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 12 12/5/14 13:35 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C9-C18 Aliphatics
ND 12 12/5/14 13:35 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C19-C36 Aliphatics
ND 12 12/5/14 13:35 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
ND 12 12/5/14 13:35 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)63.5 12/5/14 13:3540-140
o-Terphenyl (OTP)86.8 12/5/14 13:3540-140
2-Bromonaphthalene 86.8 12/5/14 13:3540-140
2-Fluorobiphenyl 88.0 12/5/14 13:3540-140
Page 42 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-05
Field Sample #: SB-5 3
Sample Matrix: Soil
Sampled: 11/26/2014 11:25
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.23
Petroleum Hydrocarbons Analyses - VPH
ND 12 12/8/14 21:46 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11Unadjusted C5-C8 Aliphatics
ND 12 12/8/14 21:46 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C5-C8 Aliphatics
ND 12 12/8/14 21:46 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11Unadjusted C9-C12 Aliphatics
ND 12 12/8/14 21:46 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C9-C12 Aliphatics
ND 12 12/8/14 21:46 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)116 12/8/14 21:4670-130
2,5-Dibromotoluene (PID)96.4 12/8/14 21:4670-130
Page 43 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-05
Field Sample #: SB-5 3
Sample Matrix: Soil
Sampled: 11/26/2014 11:25
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
84.4 12/8/14 7:48 MRL% Wt 12/4/14SM 2540G1% Solids
Page 44 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-06
Field Sample #: SB-6 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:00
[TOC_2]14L0056-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.089 12/5/14 13:45 MFFmg/Kg dry0.021 12/4/14SW-846 8260B1Acetone
ND 0.0053 12/5/14 13:45 MFFmg/Kg dry0.0022 12/4/14SW-846 8260B1Acrylonitrile
ND 0.00089 12/5/14 13:45 MFFmg/Kg dry0.00062 12/4/14SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00062 12/4/14SW-846 8260B1Benzene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00071 12/4/14SW-846 8260B1Bromobenzene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B1Bromochloromethane
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00053 12/4/14SW-846 8260B1Bromodichloromethane
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B1Bromoform
ND 0.0089 12/5/14 13:45 MFFmg/Kg dry0.0015 12/4/14SW-846 8260B1Bromomethane
ND 0.036 12/5/14 13:45 MFFmg/Kg dry0.016 12/4/14SW-846 8260B12-Butanone (MEK)
ND 0.036 12/5/14 13:45 MFFmg/Kg dry0.019 12/4/14SW-846 8260B1tert-Butyl Alcohol (TBA)
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00062 12/4/14SW-846 8260B1n-Butylbenzene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B1sec-Butylbenzene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00080 12/4/14SW-846 8260B1tert-Butylbenzene
ND 0.00089 12/5/14 13:45 MFFmg/Kg dry0.00053 12/4/14SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.0053 12/5/14 13:45 MFFmg/Kg dry0.0029 12/4/14SW-846 8260B1Carbon Disulfide
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00071 12/4/14SW-846 8260B1Carbon Tetrachloride
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00062 12/4/14SW-846 8260B1Chlorobenzene
ND 0.00089 12/5/14 13:45 MFFmg/Kg dry0.00062 12/4/14SW-846 8260B1Chlorodibromomethane
ND 0.018 12/5/14 13:45 MFFmg/Kg dry0.0013 12/4/14SW-846 8260B1Chloroethane
ND 0.0036 12/5/14 13:45 MFFmg/Kg dry0.00062 12/4/14SW-846 8260B1Chloroform
ND 0.0089 12/5/14 13:45 MFFmg/Kg dry0.00080 12/4/14SW-846 8260B1Chloromethane
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00071 12/4/14SW-846 8260B12-Chlorotoluene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00071 12/4/14SW-846 8260B14-Chlorotoluene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00098 12/4/14SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.00089 12/5/14 13:45 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00053 12/4/14SW-846 8260B1Dibromomethane
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00062 12/4/14SW-846 8260B11,2-Dichlorobenzene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00062 12/4/14SW-846 8260B11,3-Dichlorobenzene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00071 12/4/14SW-846 8260B11,4-Dichlorobenzene
ND 0.0036 12/5/14 13:45 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.018 12/5/14 13:45 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00062 12/4/14SW-846 8260B11,1-Dichloroethane
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B11,2-Dichloroethane
ND 0.0036 12/5/14 13:45 MFFmg/Kg dry0.00098 12/4/14SW-846 8260B11,1-Dichloroethylene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00071 12/4/14SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00080 12/4/14SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B11,2-Dichloropropane
ND 0.00089 12/5/14 13:45 MFFmg/Kg dry0.00062 12/4/14SW-846 8260B11,3-Dichloropropane
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00080 12/4/14SW-846 8260B12,2-Dichloropropane
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00080 12/4/14SW-846 8260B11,1-Dichloropropene
ND 0.00089 12/5/14 13:45 MFFmg/Kg dry0.00062 12/4/14SW-846 8260B1cis-1,3-Dichloropropene
ND 0.00089 12/5/14 13:45 MFFmg/Kg dry0.00062 12/4/14SW-846 8260B1trans-1,3-Dichloropropene
ND 0.018 12/5/14 13:45 MFFmg/Kg dry0.0016 12/4/14SW-846 8260B1Diethyl Ether
Page 45 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-06
Field Sample #: SB-6 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.00089 12/5/14 13:45 MFFmg/Kg dry0.00053 12/4/14SW-846 8260B1Diisopropyl Ether (DIPE)
ND 0.089 12/5/14 13:45 MFFmg/Kg dry0.051 12/4/14SW-846 8260B11,4-Dioxane
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00071 12/4/14SW-846 8260B1Ethylbenzene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B1Hexachlorobutadiene
ND 0.018 12/5/14 13:45 MFFmg/Kg dry0.0097 12/4/14SW-846 8260B12-Hexanone (MBK)
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00062 12/4/14SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00071 12/4/14SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.0036 12/5/14 13:45 MFFmg/Kg dry0.00080 12/4/14SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.018 12/5/14 13:45 MFFmg/Kg dry0.0063 12/4/14SW-846 8260B1Methylene Chloride
ND 0.018 12/5/14 13:45 MFFmg/Kg dry0.0068 12/4/14SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.0036 12/5/14 13:45 MFFmg/Kg dry0.00062 12/4/14SW-846 8260B1V-05Naphthalene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00062 12/4/14SW-846 8260B1R-05n-Propylbenzene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00053 12/4/14SW-846 8260B1Styrene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00080 12/4/14SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.00089 12/5/14 13:45 MFFmg/Kg dry0.00080 12/4/14SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B1Tetrachloroethylene
ND 0.0089 12/5/14 13:45 MFFmg/Kg dry0.0020 12/4/14SW-846 8260B1Tetrahydrofuran
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00071 12/4/14SW-846 8260B1Toluene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00053 12/4/14SW-846 8260B1V-051,2,3-Trichlorobenzene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00071 12/4/14SW-846 8260B1V-051,2,4-Trichlorobenzene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00062 12/4/14SW-846 8260B11,3,5-Trichlorobenzene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00089 12/4/14SW-846 8260B11,1,1-Trichloroethane
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B11,1,2-Trichloroethane
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00080 12/4/14SW-846 8260B1Trichloroethylene
ND 0.0089 12/5/14 13:45 MFFmg/Kg dry0.00098 12/4/14SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00098 12/4/14SW-846 8260B11,2,3-Trichloropropane
ND 0.0089 12/5/14 13:45 MFFmg/Kg dry0.00080 12/4/14SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00071 12/4/14SW-846 8260B11,2,4-Trimethylbenzene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00053 12/4/14SW-846 8260B11,3,5-Trimethylbenzene
ND 0.0089 12/5/14 13:45 MFFmg/Kg dry0.00098 12/4/14SW-846 8260B1Vinyl Chloride
ND 0.0036 12/5/14 13:45 MFFmg/Kg dry0.0015 12/4/14SW-846 8260B1m+p Xylene
ND 0.0018 12/5/14 13:45 MFFmg/Kg dry0.00062 12/4/14SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 99.4 12/5/14 13:4570-130
Toluene-d8 96.4 12/5/14 13:4570-130
4-Bromofluorobenzene 96.9 12/5/14 13:4570-130
Page 46 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-06
Field Sample #: SB-6 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.20 12/3/14 16:03 CMRmg/Kg dry0.099 12/2/14SW-846 8270D1Acenaphthene
ND 0.20 12/3/14 16:03 CMRmg/Kg dry0.096 12/2/14SW-846 8270D1Acenaphthylene
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.096 12/2/14SW-846 8270D1Acetophenone
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.30 12/2/14SW-846 8270D1Aniline
ND 0.20 12/3/14 16:03 CMRmg/Kg dry0.12 12/2/14SW-846 8270D1Anthracene
ND 0.77 12/3/14 16:03 CMRmg/Kg dry0.54 12/2/14SW-846 8270D1V-04, V-05Benzidine
ND 0.20 12/3/14 16:03 CMRmg/Kg dry0.090 12/2/14SW-846 8270D1Benzo(a)anthracene
ND 0.20 12/3/14 16:03 CMRmg/Kg dry0.070 12/2/14SW-846 8270D1Benzo(a)pyrene
ND 0.20 12/3/14 16:03 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Benzo(b)fluoranthene
ND 0.20 12/3/14 16:03 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-20Benzo(g,h,i)perylene
ND 0.20 12/3/14 16:03 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Benzo(k)fluoranthene
ND 1.2 12/3/14 16:03 CMRmg/Kg dry1.1 12/2/14SW-846 8270D1Benzoic Acid
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Bis(2-chloroisopropyl)ether
0.23 0.40 12/3/14 16:03 CMRmg/Kg dry0.089 12/2/14SW-846 8270D1JBis(2-Ethylhexyl)phthalate
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.098 12/2/14SW-846 8270D14-Bromophenylphenylether
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Butylbenzylphthalate
ND 0.20 12/3/14 16:03 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Carbazole
ND 0.77 12/3/14 16:03 CMRmg/Kg dry0.19 12/2/14SW-846 8270D14-Chloroaniline
ND 0.77 12/3/14 16:03 CMRmg/Kg dry0.16 12/2/14SW-846 8270D14-Chloro-3-methylphenol
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Chloronaphthalene
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Chlorophenol
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.13 12/2/14SW-846 8270D14-Chlorophenylphenylether
ND 0.20 12/3/14 16:03 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Chrysene
ND 0.20 12/3/14 16:03 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1V-20Dibenz(a,h)anthracene
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.092 12/2/14SW-846 8270D1Dibenzofuran
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Di-n-butylphthalate
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.079 12/2/14SW-846 8270D11,2-Dichlorobenzene
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.093 12/2/14SW-846 8270D11,3-Dichlorobenzene
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.098 12/2/14SW-846 8270D11,4-Dichlorobenzene
ND 0.20 12/3/14 16:03 CMRmg/Kg dry0.18 12/2/14SW-846 8270D13,3-Dichlorobenzidine
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12,4-Dichlorophenol
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Diethylphthalate
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.11 12/2/14SW-846 8270D12,4-Dimethylphenol
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Dimethylphthalate
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-204,6-Dinitro-2-methylphenol
ND 0.77 12/3/14 16:03 CMRmg/Kg dry0.40 12/2/14SW-846 8270D1V-04, V-202,4-Dinitrophenol
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-202,4-Dinitrotoluene
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1V-202,6-Dinitrotoluene
ND 0.78 12/3/14 16:03 CMRmg/Kg dry0.54 12/2/14SW-846 8270D1Di-n-octylphthalate
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.19 12/2/14SW-846 8270D11,2-Diphenylhydrazine (as Azobenzene)
ND 0.20 12/3/14 16:03 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Fluoranthene
ND 0.20 12/3/14 16:03 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Fluorene
Page 47 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-06
Field Sample #: SB-6 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Hexachlorobenzene
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Hexachlorobutadiene
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.26 12/2/14SW-846 8270D1Hexachlorocyclopentadiene
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Hexachloroethane
ND 0.20 12/3/14 16:03 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Isophorone
ND 0.20 12/3/14 16:03 CMRmg/Kg dry0.076 12/2/14SW-846 8270D11-Methylnaphthalene
ND 0.20 12/3/14 16:03 CMRmg/Kg dry0.11 12/2/14SW-846 8270D12-Methylnaphthalene
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Methylphenol
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.22 12/2/14SW-846 8270D13/4-Methylphenol
ND 0.20 12/3/14 16:03 CMRmg/Kg dry0.088 12/2/14SW-846 8270D1Naphthalene
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.28 12/2/14SW-846 8270D1V-202-Nitroaniline
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.18 12/2/14SW-846 8270D13-Nitroaniline
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.20 12/2/14SW-846 8270D14-Nitroaniline
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Nitrobenzene
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Nitrophenol
ND 0.77 12/3/14 16:03 CMRmg/Kg dry0.70 12/2/14SW-846 8270D14-Nitrophenol
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1N-Nitrosodimethylamine
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1N-Nitrosodiphenylamine
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.093 12/2/14SW-846 8270D1V-16, V-20Pentachloronitrobenzene
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Pentachlorophenol
ND 0.20 12/3/14 16:03 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Phenanthrene
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Phenol
ND 0.20 12/3/14 16:03 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Pyrene
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Pyridine
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.23 12/2/14SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.096 12/2/14SW-846 8270D11,2,4-Trichlorobenzene
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.21 12/2/14SW-846 8270D12,4,5-Trichlorophenol
ND 0.40 12/3/14 16:03 CMRmg/Kg dry0.26 12/2/14SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 91.8 12/3/14 16:0330-130
Phenol-d6 101 12/3/14 16:0330-130
Nitrobenzene-d5 96.2 12/3/14 16:0330-130
2-Fluorobiphenyl 97.6 12/3/14 16:0330-130
2,4,6-Tribromophenol 123 12/3/14 16:0330-130
p-Terphenyl-d14 126 12/3/14 16:0330-130
Page 48 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-06
Field Sample #: SB-6 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 12 12/5/14 13:56 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C9-C18 Aliphatics
ND 12 12/5/14 13:56 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C19-C36 Aliphatics
ND 12 12/5/14 13:56 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
ND 12 12/5/14 13:56 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)67.1 12/5/14 13:5640-140
o-Terphenyl (OTP)88.3 12/5/14 13:5640-140
2-Bromonaphthalene 90.7 12/5/14 13:5640-140
2-Fluorobiphenyl 90.7 12/5/14 13:5640-140
Page 49 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-06
Field Sample #: SB-6 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.22
Petroleum Hydrocarbons Analyses - VPH
ND 11 12/8/14 22:22 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11Unadjusted C5-C8 Aliphatics
ND 11 12/8/14 22:22 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C5-C8 Aliphatics
ND 11 12/8/14 22:22 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11Unadjusted C9-C12 Aliphatics
ND 11 12/8/14 22:22 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C9-C12 Aliphatics
ND 11 12/8/14 22:22 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)116 12/8/14 22:2270-130
2,5-Dibromotoluene (PID)95.7 12/8/14 22:2270-130
Page 50 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-06
Field Sample #: SB-6 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
85.1 12/8/14 7:48 MRL% Wt 12/4/14SM 2540G1% Solids
Page 51 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-07
Field Sample #: SB-7 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:20
[TOC_2]14L0056-07[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.084 12/5/14 14:12 MFFmg/Kg dry0.020 12/4/14SW-846 8260B1Acetone
ND 0.0050 12/5/14 14:12 MFFmg/Kg dry0.0021 12/4/14SW-846 8260B1Acrylonitrile
ND 0.00084 12/5/14 14:12 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1Benzene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00067 12/4/14SW-846 8260B1Bromobenzene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B1Bromochloromethane
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00050 12/4/14SW-846 8260B1Bromodichloromethane
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B1Bromoform
ND 0.0084 12/5/14 14:12 MFFmg/Kg dry0.0014 12/4/14SW-846 8260B1Bromomethane
ND 0.034 12/5/14 14:12 MFFmg/Kg dry0.015 12/4/14SW-846 8260B12-Butanone (MEK)
ND 0.034 12/5/14 14:12 MFFmg/Kg dry0.018 12/4/14SW-846 8260B1tert-Butyl Alcohol (TBA)
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1n-Butylbenzene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00084 12/4/14SW-846 8260B1sec-Butylbenzene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00075 12/4/14SW-846 8260B1tert-Butylbenzene
ND 0.00084 12/5/14 14:12 MFFmg/Kg dry0.00050 12/4/14SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.0050 12/5/14 14:12 MFFmg/Kg dry0.0028 12/4/14SW-846 8260B1Carbon Disulfide
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00067 12/4/14SW-846 8260B1Carbon Tetrachloride
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1Chlorobenzene
ND 0.00084 12/5/14 14:12 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1Chlorodibromomethane
ND 0.017 12/5/14 14:12 MFFmg/Kg dry0.0013 12/4/14SW-846 8260B1Chloroethane
ND 0.0034 12/5/14 14:12 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1Chloroform
ND 0.0084 12/5/14 14:12 MFFmg/Kg dry0.00075 12/4/14SW-846 8260B1Chloromethane
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00067 12/4/14SW-846 8260B12-Chlorotoluene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00067 12/4/14SW-846 8260B14-Chlorotoluene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00092 12/4/14SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.00084 12/5/14 14:12 MFFmg/Kg dry0.00084 12/4/14SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00050 12/4/14SW-846 8260B1Dibromomethane
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B11,2-Dichlorobenzene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B11,3-Dichlorobenzene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00067 12/4/14SW-846 8260B11,4-Dichlorobenzene
ND 0.0034 12/5/14 14:12 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.017 12/5/14 14:12 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B11,1-Dichloroethane
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B11,2-Dichloroethane
ND 0.0034 12/5/14 14:12 MFFmg/Kg dry0.00092 12/4/14SW-846 8260B11,1-Dichloroethylene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00067 12/4/14SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00075 12/4/14SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B11,2-Dichloropropane
ND 0.00084 12/5/14 14:12 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B11,3-Dichloropropane
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00075 12/4/14SW-846 8260B12,2-Dichloropropane
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00075 12/4/14SW-846 8260B11,1-Dichloropropene
ND 0.00084 12/5/14 14:12 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1cis-1,3-Dichloropropene
ND 0.00084 12/5/14 14:12 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1trans-1,3-Dichloropropene
ND 0.017 12/5/14 14:12 MFFmg/Kg dry0.0015 12/4/14SW-846 8260B1Diethyl Ether
Page 52 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-07
Field Sample #: SB-7 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.00084 12/5/14 14:12 MFFmg/Kg dry0.00050 12/4/14SW-846 8260B1Diisopropyl Ether (DIPE)
ND 0.084 12/5/14 14:12 MFFmg/Kg dry0.048 12/4/14SW-846 8260B11,4-Dioxane
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00067 12/4/14SW-846 8260B1Ethylbenzene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00084 12/4/14SW-846 8260B1Hexachlorobutadiene
ND 0.017 12/5/14 14:12 MFFmg/Kg dry0.0091 12/4/14SW-846 8260B12-Hexanone (MBK)
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00067 12/4/14SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.0034 12/5/14 14:12 MFFmg/Kg dry0.00075 12/4/14SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.017 12/5/14 14:12 MFFmg/Kg dry0.0059 12/4/14SW-846 8260B1Methylene Chloride
ND 0.017 12/5/14 14:12 MFFmg/Kg dry0.0064 12/4/14SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.0034 12/5/14 14:12 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1V-05Naphthalene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1R-05n-Propylbenzene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00050 12/4/14SW-846 8260B1Styrene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00075 12/4/14SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.00084 12/5/14 14:12 MFFmg/Kg dry0.00075 12/4/14SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B1Tetrachloroethylene
ND 0.0084 12/5/14 14:12 MFFmg/Kg dry0.0018 12/4/14SW-846 8260B1Tetrahydrofuran
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00067 12/4/14SW-846 8260B1Toluene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00050 12/4/14SW-846 8260B1V-051,2,3-Trichlorobenzene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00067 12/4/14SW-846 8260B1V-051,2,4-Trichlorobenzene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B11,3,5-Trichlorobenzene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00084 12/4/14SW-846 8260B11,1,1-Trichloroethane
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.0010 12/4/14SW-846 8260B11,1,2-Trichloroethane
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00075 12/4/14SW-846 8260B1Trichloroethylene
ND 0.0084 12/5/14 14:12 MFFmg/Kg dry0.00092 12/4/14SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00092 12/4/14SW-846 8260B11,2,3-Trichloropropane
ND 0.0084 12/5/14 14:12 MFFmg/Kg dry0.00075 12/4/14SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00067 12/4/14SW-846 8260B11,2,4-Trimethylbenzene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00050 12/4/14SW-846 8260B11,3,5-Trimethylbenzene
ND 0.0084 12/5/14 14:12 MFFmg/Kg dry0.00092 12/4/14SW-846 8260B1Vinyl Chloride
ND 0.0034 12/5/14 14:12 MFFmg/Kg dry0.0014 12/4/14SW-846 8260B1m+p Xylene
ND 0.0017 12/5/14 14:12 MFFmg/Kg dry0.00059 12/4/14SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 101 12/5/14 14:1270-130
Toluene-d8 97.8 12/5/14 14:1270-130
4-Bromofluorobenzene 93.4 12/5/14 14:1270-130
Page 53 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-07
Field Sample #: SB-7 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.19 12/3/14 16:27 CMRmg/Kg dry0.096 12/2/14SW-846 8270D1Acenaphthene
ND 0.19 12/3/14 16:27 CMRmg/Kg dry0.093 12/2/14SW-846 8270D1Acenaphthylene
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.093 12/2/14SW-846 8270D1Acetophenone
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.29 12/2/14SW-846 8270D1Aniline
ND 0.19 12/3/14 16:27 CMRmg/Kg dry0.12 12/2/14SW-846 8270D1Anthracene
ND 0.75 12/3/14 16:27 CMRmg/Kg dry0.52 12/2/14SW-846 8270D1V-04, V-05Benzidine
ND 0.19 12/3/14 16:27 CMRmg/Kg dry0.087 12/2/14SW-846 8270D1Benzo(a)anthracene
ND 0.19 12/3/14 16:27 CMRmg/Kg dry0.068 12/2/14SW-846 8270D1Benzo(a)pyrene
ND 0.19 12/3/14 16:27 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Benzo(b)fluoranthene
ND 0.19 12/3/14 16:27 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-20Benzo(g,h,i)perylene
ND 0.19 12/3/14 16:27 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Benzo(k)fluoranthene
ND 1.1 12/3/14 16:27 CMRmg/Kg dry1.1 12/2/14SW-846 8270D1Benzoic Acid
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Bis(2-chloroisopropyl)ether
0.25 0.39 12/3/14 16:27 CMRmg/Kg dry0.086 12/2/14SW-846 8270D1JBis(2-Ethylhexyl)phthalate
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.095 12/2/14SW-846 8270D14-Bromophenylphenylether
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Butylbenzylphthalate
ND 0.19 12/3/14 16:27 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Carbazole
ND 0.75 12/3/14 16:27 CMRmg/Kg dry0.19 12/2/14SW-846 8270D14-Chloroaniline
ND 0.75 12/3/14 16:27 CMRmg/Kg dry0.16 12/2/14SW-846 8270D14-Chloro-3-methylphenol
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Chloronaphthalene
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.11 12/2/14SW-846 8270D12-Chlorophenol
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.13 12/2/14SW-846 8270D14-Chlorophenylphenylether
ND 0.19 12/3/14 16:27 CMRmg/Kg dry0.12 12/2/14SW-846 8270D1Chrysene
ND 0.19 12/3/14 16:27 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1V-20Dibenz(a,h)anthracene
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.089 12/2/14SW-846 8270D1Dibenzofuran
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Di-n-butylphthalate
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.077 12/2/14SW-846 8270D11,2-Dichlorobenzene
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.091 12/2/14SW-846 8270D11,3-Dichlorobenzene
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.095 12/2/14SW-846 8270D11,4-Dichlorobenzene
ND 0.19 12/3/14 16:27 CMRmg/Kg dry0.18 12/2/14SW-846 8270D13,3-Dichlorobenzidine
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12,4-Dichlorophenol
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Diethylphthalate
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.11 12/2/14SW-846 8270D12,4-Dimethylphenol
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Dimethylphthalate
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-204,6-Dinitro-2-methylphenol
ND 0.75 12/3/14 16:27 CMRmg/Kg dry0.38 12/2/14SW-846 8270D1V-04, V-202,4-Dinitrophenol
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1V-202,4-Dinitrotoluene
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.12 12/2/14SW-846 8270D1V-202,6-Dinitrotoluene
ND 0.76 12/3/14 16:27 CMRmg/Kg dry0.53 12/2/14SW-846 8270D1Di-n-octylphthalate
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.18 12/2/14SW-846 8270D11,2-Diphenylhydrazine (as Azobenzene)
ND 0.19 12/3/14 16:27 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Fluoranthene
ND 0.19 12/3/14 16:27 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Fluorene
Page 54 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-07
Field Sample #: SB-7 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Hexachlorobenzene
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Hexachlorobutadiene
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.25 12/2/14SW-846 8270D1Hexachlorocyclopentadiene
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Hexachloroethane
ND 0.19 12/3/14 16:27 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Isophorone
ND 0.19 12/3/14 16:27 CMRmg/Kg dry0.074 12/2/14SW-846 8270D11-Methylnaphthalene
ND 0.19 12/3/14 16:27 CMRmg/Kg dry0.10 12/2/14SW-846 8270D12-Methylnaphthalene
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Methylphenol
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.21 12/2/14SW-846 8270D13/4-Methylphenol
ND 0.19 12/3/14 16:27 CMRmg/Kg dry0.085 12/2/14SW-846 8270D1Naphthalene
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.27 12/2/14SW-846 8270D1V-202-Nitroaniline
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.18 12/2/14SW-846 8270D13-Nitroaniline
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.20 12/2/14SW-846 8270D14-Nitroaniline
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Nitrobenzene
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.11 12/2/14SW-846 8270D12-Nitrophenol
ND 0.75 12/3/14 16:27 CMRmg/Kg dry0.67 12/2/14SW-846 8270D14-Nitrophenol
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1N-Nitrosodimethylamine
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1N-Nitrosodiphenylamine
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.12 12/2/14SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.091 12/2/14SW-846 8270D1V-20, V-16Pentachloronitrobenzene
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Pentachlorophenol
ND 0.19 12/3/14 16:27 CMRmg/Kg dry0.10 12/2/14SW-846 8270D1Phenanthrene
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.10 12/2/14SW-846 8270D1Phenol
ND 0.19 12/3/14 16:27 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Pyrene
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Pyridine
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.23 12/2/14SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.093 12/2/14SW-846 8270D11,2,4-Trichlorobenzene
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.20 12/2/14SW-846 8270D12,4,5-Trichlorophenol
ND 0.39 12/3/14 16:27 CMRmg/Kg dry0.25 12/2/14SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 95.2 12/3/14 16:2730-130
Phenol-d6 104 12/3/14 16:2730-130
Nitrobenzene-d5 104 12/3/14 16:2730-130
2-Fluorobiphenyl 103 12/3/14 16:2730-130
2,4,6-Tribromophenol 124 12/3/14 16:2730-130
p-Terphenyl-d14 128 12/3/14 16:2730-130
Page 55 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-07
Field Sample #: SB-7 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 11 12/5/14 14:17 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C9-C18 Aliphatics
ND 11 12/5/14 14:17 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C19-C36 Aliphatics
ND 11 12/5/14 14:17 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
ND 11 12/5/14 14:17 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)69.1 12/5/14 14:1740-140
o-Terphenyl (OTP)99.6 12/5/14 14:1740-140
2-Bromonaphthalene 93.1 12/5/14 14:1740-140
2-Fluorobiphenyl 92.6 12/5/14 14:1740-140
Page 56 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-07
Field Sample #: SB-7 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Sample Flags: O-01
Soil/Methanol Preservation Ratio: 1.33
Petroleum Hydrocarbons Analyses - VPH
ND 9.9 12/8/14 22:58 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11Unadjusted C5-C8 Aliphatics
ND 9.9 12/8/14 22:58 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C5-C8 Aliphatics
ND 9.9 12/8/14 22:58 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11Unadjusted C9-C12 Aliphatics
ND 9.9 12/8/14 22:58 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C9-C12 Aliphatics
ND 9.9 12/8/14 22:58 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)115 12/8/14 22:5870-130
2,5-Dibromotoluene (PID)91.6 12/8/14 22:5870-130
Page 57 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-07
Field Sample #: SB-7 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
88.3 12/8/14 7:48 MRL% Wt 12/4/14SM 2540G1% Solids
Page 58 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-08
Field Sample #: SB-8 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:40
[TOC_2]14L0056-08[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.090 12/5/14 14:40 MFFmg/Kg dry0.021 12/4/14SW-846 8260B1Acetone
ND 0.0054 12/5/14 14:40 MFFmg/Kg dry0.0022 12/4/14SW-846 8260B1Acrylonitrile
ND 0.00090 12/5/14 14:40 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1Benzene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B1Bromobenzene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.0013 12/4/14SW-846 8260B1Bromochloromethane
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00054 12/4/14SW-846 8260B1Bromodichloromethane
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.0013 12/4/14SW-846 8260B1Bromoform
ND 0.0090 12/5/14 14:40 MFFmg/Kg dry0.0015 12/4/14SW-846 8260B1Bromomethane
ND 0.036 12/5/14 14:40 MFFmg/Kg dry0.016 12/4/14SW-846 8260B12-Butanone (MEK)
ND 0.036 12/5/14 14:40 MFFmg/Kg dry0.019 12/4/14SW-846 8260B1tert-Butyl Alcohol (TBA)
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1n-Butylbenzene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00090 12/4/14SW-846 8260B1sec-Butylbenzene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00081 12/4/14SW-846 8260B1tert-Butylbenzene
ND 0.00090 12/5/14 14:40 MFFmg/Kg dry0.00054 12/4/14SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.0054 12/5/14 14:40 MFFmg/Kg dry0.0030 12/4/14SW-846 8260B1Carbon Disulfide
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B1Carbon Tetrachloride
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1Chlorobenzene
ND 0.00090 12/5/14 14:40 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1Chlorodibromomethane
ND 0.018 12/5/14 14:40 MFFmg/Kg dry0.0013 12/4/14SW-846 8260B1Chloroethane
ND 0.0036 12/5/14 14:40 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1Chloroform
ND 0.0090 12/5/14 14:40 MFFmg/Kg dry0.00081 12/4/14SW-846 8260B1Chloromethane
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B12-Chlorotoluene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B14-Chlorotoluene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00099 12/4/14SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.00090 12/5/14 14:40 MFFmg/Kg dry0.00090 12/4/14SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00054 12/4/14SW-846 8260B1Dibromomethane
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B11,2-Dichlorobenzene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B11,3-Dichlorobenzene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B11,4-Dichlorobenzene
ND 0.0036 12/5/14 14:40 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.018 12/5/14 14:40 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B11,1-Dichloroethane
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B11,2-Dichloroethane
ND 0.0036 12/5/14 14:40 MFFmg/Kg dry0.00099 12/4/14SW-846 8260B11,1-Dichloroethylene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00081 12/4/14SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B11,2-Dichloropropane
ND 0.00090 12/5/14 14:40 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B11,3-Dichloropropane
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00081 12/4/14SW-846 8260B12,2-Dichloropropane
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00081 12/4/14SW-846 8260B11,1-Dichloropropene
ND 0.00090 12/5/14 14:40 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1cis-1,3-Dichloropropene
ND 0.00090 12/5/14 14:40 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1trans-1,3-Dichloropropene
ND 0.018 12/5/14 14:40 MFFmg/Kg dry0.0016 12/4/14SW-846 8260B1Diethyl Ether
Page 59 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-08
Field Sample #: SB-8 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.00090 12/5/14 14:40 MFFmg/Kg dry0.00054 12/4/14SW-846 8260B1Diisopropyl Ether (DIPE)
ND 0.090 12/5/14 14:40 MFFmg/Kg dry0.052 12/4/14SW-846 8260B11,4-Dioxane
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B1Ethylbenzene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00090 12/4/14SW-846 8260B1Hexachlorobutadiene
ND 0.018 12/5/14 14:40 MFFmg/Kg dry0.0098 12/4/14SW-846 8260B12-Hexanone (MBK)
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.0036 12/5/14 14:40 MFFmg/Kg dry0.00081 12/4/14SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.018 12/5/14 14:40 MFFmg/Kg dry0.0064 12/4/14SW-846 8260B1Methylene Chloride
ND 0.018 12/5/14 14:40 MFFmg/Kg dry0.0068 12/4/14SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.0036 12/5/14 14:40 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1V-05Naphthalene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1R-05n-Propylbenzene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00054 12/4/14SW-846 8260B1Styrene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00081 12/4/14SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.00090 12/5/14 14:40 MFFmg/Kg dry0.00081 12/4/14SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B1Tetrachloroethylene
ND 0.0090 12/5/14 14:40 MFFmg/Kg dry0.0020 12/4/14SW-846 8260B1Tetrahydrofuran
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B1Toluene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00054 12/4/14SW-846 8260B1V-051,2,3-Trichlorobenzene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B1V-051,2,4-Trichlorobenzene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B11,3,5-Trichlorobenzene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00090 12/4/14SW-846 8260B11,1,1-Trichloroethane
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B11,1,2-Trichloroethane
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00081 12/4/14SW-846 8260B1Trichloroethylene
ND 0.0090 12/5/14 14:40 MFFmg/Kg dry0.00099 12/4/14SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00099 12/4/14SW-846 8260B11,2,3-Trichloropropane
ND 0.0090 12/5/14 14:40 MFFmg/Kg dry0.00081 12/4/14SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00072 12/4/14SW-846 8260B11,2,4-Trimethylbenzene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00054 12/4/14SW-846 8260B11,3,5-Trimethylbenzene
ND 0.0090 12/5/14 14:40 MFFmg/Kg dry0.00099 12/4/14SW-846 8260B1Vinyl Chloride
ND 0.0036 12/5/14 14:40 MFFmg/Kg dry0.0015 12/4/14SW-846 8260B1m+p Xylene
ND 0.0018 12/5/14 14:40 MFFmg/Kg dry0.00063 12/4/14SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 102 12/5/14 14:4070-130
Toluene-d8 97.1 12/5/14 14:4070-130
4-Bromofluorobenzene 95.4 12/5/14 14:4070-130
Page 60 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-08
Field Sample #: SB-8 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.20 12/3/14 16:51 CMRmg/Kg dry0.099 12/2/14SW-846 8270D1Acenaphthene
ND 0.20 12/3/14 16:51 CMRmg/Kg dry0.096 12/2/14SW-846 8270D1Acenaphthylene
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.096 12/2/14SW-846 8270D1Acetophenone
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.30 12/2/14SW-846 8270D1Aniline
ND 0.20 12/3/14 16:51 CMRmg/Kg dry0.12 12/2/14SW-846 8270D1Anthracene
ND 0.77 12/3/14 16:51 CMRmg/Kg dry0.54 12/2/14SW-846 8270D1V-04, V-05Benzidine
ND 0.20 12/3/14 16:51 CMRmg/Kg dry0.090 12/2/14SW-846 8270D1Benzo(a)anthracene
ND 0.20 12/3/14 16:51 CMRmg/Kg dry0.070 12/2/14SW-846 8270D1Benzo(a)pyrene
ND 0.20 12/3/14 16:51 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Benzo(b)fluoranthene
ND 0.20 12/3/14 16:51 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-20Benzo(g,h,i)perylene
ND 0.20 12/3/14 16:51 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Benzo(k)fluoranthene
ND 1.2 12/3/14 16:51 CMRmg/Kg dry1.1 12/2/14SW-846 8270D1Benzoic Acid
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Bis(2-chloroisopropyl)ether
0.22 0.40 12/3/14 16:51 CMRmg/Kg dry0.089 12/2/14SW-846 8270D1JBis(2-Ethylhexyl)phthalate
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.098 12/2/14SW-846 8270D14-Bromophenylphenylether
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Butylbenzylphthalate
ND 0.20 12/3/14 16:51 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Carbazole
ND 0.77 12/3/14 16:51 CMRmg/Kg dry0.19 12/2/14SW-846 8270D14-Chloroaniline
ND 0.77 12/3/14 16:51 CMRmg/Kg dry0.16 12/2/14SW-846 8270D14-Chloro-3-methylphenol
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Chloronaphthalene
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Chlorophenol
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.13 12/2/14SW-846 8270D14-Chlorophenylphenylether
ND 0.20 12/3/14 16:51 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Chrysene
ND 0.20 12/3/14 16:51 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1V-20Dibenz(a,h)anthracene
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.092 12/2/14SW-846 8270D1Dibenzofuran
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Di-n-butylphthalate
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.079 12/2/14SW-846 8270D11,2-Dichlorobenzene
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.093 12/2/14SW-846 8270D11,3-Dichlorobenzene
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.098 12/2/14SW-846 8270D11,4-Dichlorobenzene
ND 0.20 12/3/14 16:51 CMRmg/Kg dry0.18 12/2/14SW-846 8270D13,3-Dichlorobenzidine
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12,4-Dichlorophenol
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Diethylphthalate
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.11 12/2/14SW-846 8270D12,4-Dimethylphenol
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Dimethylphthalate
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-204,6-Dinitro-2-methylphenol
ND 0.77 12/3/14 16:51 CMRmg/Kg dry0.40 12/2/14SW-846 8270D1V-04, V-202,4-Dinitrophenol
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-202,4-Dinitrotoluene
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1V-202,6-Dinitrotoluene
ND 0.78 12/3/14 16:51 CMRmg/Kg dry0.54 12/2/14SW-846 8270D1Di-n-octylphthalate
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.19 12/2/14SW-846 8270D11,2-Diphenylhydrazine (as Azobenzene)
ND 0.20 12/3/14 16:51 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Fluoranthene
ND 0.20 12/3/14 16:51 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Fluorene
Page 61 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-08
Field Sample #: SB-8 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Hexachlorobenzene
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Hexachlorobutadiene
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.26 12/2/14SW-846 8270D1Hexachlorocyclopentadiene
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Hexachloroethane
ND 0.20 12/3/14 16:51 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Isophorone
ND 0.20 12/3/14 16:51 CMRmg/Kg dry0.076 12/2/14SW-846 8270D11-Methylnaphthalene
ND 0.20 12/3/14 16:51 CMRmg/Kg dry0.11 12/2/14SW-846 8270D12-Methylnaphthalene
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Methylphenol
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.22 12/2/14SW-846 8270D13/4-Methylphenol
ND 0.20 12/3/14 16:51 CMRmg/Kg dry0.088 12/2/14SW-846 8270D1Naphthalene
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.28 12/2/14SW-846 8270D1V-202-Nitroaniline
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.18 12/2/14SW-846 8270D13-Nitroaniline
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.20 12/2/14SW-846 8270D14-Nitroaniline
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Nitrobenzene
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Nitrophenol
ND 0.77 12/3/14 16:51 CMRmg/Kg dry0.70 12/2/14SW-846 8270D14-Nitrophenol
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1N-Nitrosodimethylamine
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1N-Nitrosodiphenylamine
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.093 12/2/14SW-846 8270D1V-16, V-20Pentachloronitrobenzene
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Pentachlorophenol
ND 0.20 12/3/14 16:51 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Phenanthrene
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Phenol
ND 0.20 12/3/14 16:51 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Pyrene
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Pyridine
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.23 12/2/14SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.096 12/2/14SW-846 8270D11,2,4-Trichlorobenzene
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.21 12/2/14SW-846 8270D12,4,5-Trichlorophenol
ND 0.40 12/3/14 16:51 CMRmg/Kg dry0.26 12/2/14SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 94.4 12/3/14 16:5130-130
Phenol-d6 103 12/3/14 16:5130-130
Nitrobenzene-d5 98.2 12/3/14 16:5130-130
2-Fluorobiphenyl 101 12/3/14 16:5130-130
2,4,6-Tribromophenol 127 12/3/14 16:5130-130
p-Terphenyl-d14 131 12/3/14 16:51*S-0730-130
Page 62 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-08
Field Sample #: SB-8 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 12 12/5/14 14:38 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C9-C18 Aliphatics
ND 12 12/5/14 14:38 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C19-C36 Aliphatics
ND 12 12/5/14 14:38 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
ND 12 12/5/14 14:38 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)66.9 12/5/14 14:3840-140
o-Terphenyl (OTP)89.4 12/5/14 14:3840-140
2-Bromonaphthalene 84.9 12/5/14 14:3840-140
2-Fluorobiphenyl 88.0 12/5/14 14:3840-140
Page 63 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-08
Field Sample #: SB-8 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Soil/Methanol Preservation Ratio: 1.09
Petroleum Hydrocarbons Analyses - VPH
ND 12 12/9/14 10:10 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11Unadjusted C5-C8 Aliphatics
ND 12 12/9/14 10:10 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C5-C8 Aliphatics
ND 12 12/9/14 10:10 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11Unadjusted C9-C12 Aliphatics
ND 12 12/9/14 10:10 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C9-C12 Aliphatics
ND 12 12/9/14 10:10 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)144 12/9/14 10:10*S-1770-130
2,5-Dibromotoluene (PID)127 12/9/14 10:1070-130
Page 64 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-08
Field Sample #: SB-8 3
Sample Matrix: Soil
Sampled: 11/26/2014 12:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
85.6 12/8/14 7:48 MRL% Wt 12/4/14SM 2540G1% Solids
Page 65 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-09
Field Sample #: SB-9 3
Sample Matrix: Soil
Sampled: 11/26/2014 13:00
[TOC_2]14L0056-09[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.083 12/5/14 15:07 MFFmg/Kg dry0.019 12/4/14SW-846 8260B1Acetone
ND 0.0050 12/5/14 15:07 MFFmg/Kg dry0.0021 12/4/14SW-846 8260B1Acrylonitrile
ND 0.00083 12/5/14 15:07 MFFmg/Kg dry0.00058 12/4/14SW-846 8260B1tert-Amyl Methyl Ether (TAME)
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00058 12/4/14SW-846 8260B1Benzene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00066 12/4/14SW-846 8260B1Bromobenzene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B1Bromochloromethane
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00050 12/4/14SW-846 8260B1Bromodichloromethane
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B1Bromoform
ND 0.0083 12/5/14 15:07 MFFmg/Kg dry0.0014 12/4/14SW-846 8260B1Bromomethane
ND 0.033 12/5/14 15:07 MFFmg/Kg dry0.015 12/4/14SW-846 8260B12-Butanone (MEK)
ND 0.033 12/5/14 15:07 MFFmg/Kg dry0.017 12/4/14SW-846 8260B1tert-Butyl Alcohol (TBA)
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00058 12/4/14SW-846 8260B1n-Butylbenzene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00083 12/4/14SW-846 8260B1sec-Butylbenzene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00075 12/4/14SW-846 8260B1tert-Butylbenzene
ND 0.00083 12/5/14 15:07 MFFmg/Kg dry0.00050 12/4/14SW-846 8260B1tert-Butyl Ethyl Ether (TBEE)
ND 0.0050 12/5/14 15:07 MFFmg/Kg dry0.0027 12/4/14SW-846 8260B1Carbon Disulfide
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00066 12/4/14SW-846 8260B1Carbon Tetrachloride
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00058 12/4/14SW-846 8260B1Chlorobenzene
ND 0.00083 12/5/14 15:07 MFFmg/Kg dry0.00058 12/4/14SW-846 8260B1Chlorodibromomethane
ND 0.017 12/5/14 15:07 MFFmg/Kg dry0.0012 12/4/14SW-846 8260B1Chloroethane
ND 0.0033 12/5/14 15:07 MFFmg/Kg dry0.00058 12/4/14SW-846 8260B1Chloroform
ND 0.0083 12/5/14 15:07 MFFmg/Kg dry0.00075 12/4/14SW-846 8260B1Chloromethane
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00066 12/4/14SW-846 8260B12-Chlorotoluene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00066 12/4/14SW-846 8260B14-Chlorotoluene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00091 12/4/14SW-846 8260B11,2-Dibromo-3-chloropropane (DBCP)
ND 0.00083 12/5/14 15:07 MFFmg/Kg dry0.00083 12/4/14SW-846 8260B11,2-Dibromoethane (EDB)
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00050 12/4/14SW-846 8260B1Dibromomethane
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00058 12/4/14SW-846 8260B11,2-Dichlorobenzene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00058 12/4/14SW-846 8260B11,3-Dichlorobenzene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00066 12/4/14SW-846 8260B11,4-Dichlorobenzene
ND 0.0033 12/5/14 15:07 MFFmg/Kg dry0.00099 12/4/14SW-846 8260B1trans-1,4-Dichloro-2-butene
ND 0.017 12/5/14 15:07 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B1Dichlorodifluoromethane (Freon 12)
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00058 12/4/14SW-846 8260B11,1-Dichloroethane
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B11,2-Dichloroethane
ND 0.0033 12/5/14 15:07 MFFmg/Kg dry0.00091 12/4/14SW-846 8260B11,1-Dichloroethylene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00066 12/4/14SW-846 8260B1cis-1,2-Dichloroethylene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00075 12/4/14SW-846 8260B1trans-1,2-Dichloroethylene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B11,2-Dichloropropane
ND 0.00083 12/5/14 15:07 MFFmg/Kg dry0.00058 12/4/14SW-846 8260B11,3-Dichloropropane
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00075 12/4/14SW-846 8260B12,2-Dichloropropane
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00075 12/4/14SW-846 8260B11,1-Dichloropropene
ND 0.00083 12/5/14 15:07 MFFmg/Kg dry0.00058 12/4/14SW-846 8260B1cis-1,3-Dichloropropene
ND 0.00083 12/5/14 15:07 MFFmg/Kg dry0.00058 12/4/14SW-846 8260B1trans-1,3-Dichloropropene
ND 0.017 12/5/14 15:07 MFFmg/Kg dry0.0015 12/4/14SW-846 8260B1Diethyl Ether
Page 66 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-09
Field Sample #: SB-9 3
Sample Matrix: Soil
Sampled: 11/26/2014 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.00083 12/5/14 15:07 MFFmg/Kg dry0.00050 12/4/14SW-846 8260B1Diisopropyl Ether (DIPE)
ND 0.083 12/5/14 15:07 MFFmg/Kg dry0.048 12/4/14SW-846 8260B11,4-Dioxane
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00066 12/4/14SW-846 8260B1Ethylbenzene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00083 12/4/14SW-846 8260B1Hexachlorobutadiene
ND 0.017 12/5/14 15:07 MFFmg/Kg dry0.0090 12/4/14SW-846 8260B12-Hexanone (MBK)
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00058 12/4/14SW-846 8260B1Isopropylbenzene (Cumene)
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00066 12/4/14SW-846 8260B1p-Isopropyltoluene (p-Cymene)
ND 0.0033 12/5/14 15:07 MFFmg/Kg dry0.00075 12/4/14SW-846 8260B1Methyl tert-Butyl Ether (MTBE)
ND 0.017 12/5/14 15:07 MFFmg/Kg dry0.0059 12/4/14SW-846 8260B1Methylene Chloride
ND 0.017 12/5/14 15:07 MFFmg/Kg dry0.0063 12/4/14SW-846 8260B14-Methyl-2-pentanone (MIBK)
ND 0.0033 12/5/14 15:07 MFFmg/Kg dry0.00058 12/4/14SW-846 8260B1V-05Naphthalene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00058 12/4/14SW-846 8260B1R-05n-Propylbenzene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00050 12/4/14SW-846 8260B1Styrene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00075 12/4/14SW-846 8260B11,1,1,2-Tetrachloroethane
ND 0.00083 12/5/14 15:07 MFFmg/Kg dry0.00075 12/4/14SW-846 8260B11,1,2,2-Tetrachloroethane
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.0011 12/4/14SW-846 8260B1Tetrachloroethylene
ND 0.0083 12/5/14 15:07 MFFmg/Kg dry0.0018 12/4/14SW-846 8260B1Tetrahydrofuran
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00066 12/4/14SW-846 8260B1Toluene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00050 12/4/14SW-846 8260B1V-051,2,3-Trichlorobenzene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00066 12/4/14SW-846 8260B1V-051,2,4-Trichlorobenzene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00058 12/4/14SW-846 8260B11,3,5-Trichlorobenzene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00083 12/4/14SW-846 8260B11,1,1-Trichloroethane
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00099 12/4/14SW-846 8260B11,1,2-Trichloroethane
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00075 12/4/14SW-846 8260B1Trichloroethylene
ND 0.0083 12/5/14 15:07 MFFmg/Kg dry0.00091 12/4/14SW-846 8260B1Trichlorofluoromethane (Freon 11)
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00091 12/4/14SW-846 8260B11,2,3-Trichloropropane
ND 0.0083 12/5/14 15:07 MFFmg/Kg dry0.00075 12/4/14SW-846 8260B11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00066 12/4/14SW-846 8260B11,2,4-Trimethylbenzene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00050 12/4/14SW-846 8260B11,3,5-Trimethylbenzene
ND 0.0083 12/5/14 15:07 MFFmg/Kg dry0.00091 12/4/14SW-846 8260B1Vinyl Chloride
ND 0.0033 12/5/14 15:07 MFFmg/Kg dry0.0014 12/4/14SW-846 8260B1m+p Xylene
ND 0.0017 12/5/14 15:07 MFFmg/Kg dry0.00058 12/4/14SW-846 8260B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 101 12/5/14 15:0770-130
Toluene-d8 93.3 12/5/14 15:0770-130
4-Bromofluorobenzene 93.9 12/5/14 15:0770-130
Page 67 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-09
Field Sample #: SB-9 3
Sample Matrix: Soil
Sampled: 11/26/2014 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.20 12/3/14 13:40 CMRmg/Kg dry0.10 12/2/14SW-846 8270D1Acenaphthene
ND 0.20 12/3/14 13:40 CMRmg/Kg dry0.098 12/2/14SW-846 8270D1Acenaphthylene
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.098 12/2/14SW-846 8270D1Acetophenone
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.31 12/2/14SW-846 8270D1Aniline
ND 0.20 12/3/14 13:40 CMRmg/Kg dry0.12 12/2/14SW-846 8270D1Anthracene
ND 0.79 12/3/14 13:40 CMRmg/Kg dry0.55 12/2/14SW-846 8270D1V-04, V-05Benzidine
ND 0.20 12/3/14 13:40 CMRmg/Kg dry0.092 12/2/14SW-846 8270D1Benzo(a)anthracene
ND 0.20 12/3/14 13:40 CMRmg/Kg dry0.072 12/2/14SW-846 8270D1Benzo(a)pyrene
ND 0.20 12/3/14 13:40 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Benzo(b)fluoranthene
ND 0.20 12/3/14 13:40 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-20Benzo(g,h,i)perylene
ND 0.20 12/3/14 13:40 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Benzo(k)fluoranthene
ND 1.2 12/3/14 13:40 CMRmg/Kg dry1.1 12/2/14SW-846 8270D1L-04Benzoic Acid
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Bis(2-chloroethoxy)methane
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Bis(2-chloroethyl)ether
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Bis(2-chloroisopropyl)ether
0.16 0.41 12/3/14 13:40 CMRmg/Kg dry0.091 12/2/14SW-846 8270D1JBis(2-Ethylhexyl)phthalate
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.10 12/2/14SW-846 8270D14-Bromophenylphenylether
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Butylbenzylphthalate
ND 0.20 12/3/14 13:40 CMRmg/Kg dry0.15 12/2/14SW-846 8270D1Carbazole
ND 0.79 12/3/14 13:40 CMRmg/Kg dry0.20 12/2/14SW-846 8270D14-Chloroaniline
ND 0.79 12/3/14 13:40 CMRmg/Kg dry0.17 12/2/14SW-846 8270D14-Chloro-3-methylphenol
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.13 12/2/14SW-846 8270D12-Chloronaphthalene
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Chlorophenol
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.14 12/2/14SW-846 8270D14-Chlorophenylphenylether
ND 0.20 12/3/14 13:40 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Chrysene
ND 0.20 12/3/14 13:40 CMRmg/Kg dry0.12 12/2/14SW-846 8270D1V-20Dibenz(a,h)anthracene
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.095 12/2/14SW-846 8270D1Dibenzofuran
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Di-n-butylphthalate
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.082 12/2/14SW-846 8270D11,2-Dichlorobenzene
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.096 12/2/14SW-846 8270D11,3-Dichlorobenzene
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.10 12/2/14SW-846 8270D11,4-Dichlorobenzene
ND 0.20 12/3/14 13:40 CMRmg/Kg dry0.19 12/2/14SW-846 8270D13,3-Dichlorobenzidine
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12,4-Dichlorophenol
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Diethylphthalate
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12,4-Dimethylphenol
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Dimethylphthalate
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1R-05, V-204,6-Dinitro-2-methylphenol
ND 0.79 12/3/14 13:40 CMRmg/Kg dry0.41 12/2/14SW-846 8270D1L-04, V-04, V-202,4-Dinitrophenol
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1V-202,4-Dinitrotoluene
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1V-202,6-Dinitrotoluene
ND 0.80 12/3/14 13:40 CMRmg/Kg dry0.56 12/2/14SW-846 8270D1Di-n-octylphthalate
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.20 12/2/14SW-846 8270D11,2-Diphenylhydrazine (as Azobenzene)
ND 0.20 12/3/14 13:40 CMRmg/Kg dry0.18 12/2/14SW-846 8270D1Fluoranthene
ND 0.20 12/3/14 13:40 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Fluorene
Page 68 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-09
Field Sample #: SB-9 3
Sample Matrix: Soil
Sampled: 11/26/2014 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.19 12/2/14SW-846 8270D1Hexachlorobenzene
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Hexachlorobutadiene
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.27 12/2/14SW-846 8270D1Hexachlorocyclopentadiene
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Hexachloroethane
ND 0.20 12/3/14 13:40 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1Indeno(1,2,3-cd)pyrene
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.12 12/2/14SW-846 8270D1Isophorone
ND 0.20 12/3/14 13:40 CMRmg/Kg dry0.078 12/2/14SW-846 8270D11-Methylnaphthalene
ND 0.20 12/3/14 13:40 CMRmg/Kg dry0.11 12/2/14SW-846 8270D12-Methylnaphthalene
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.13 12/2/14SW-846 8270D12-Methylphenol
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.23 12/2/14SW-846 8270D13/4-Methylphenol
ND 0.20 12/3/14 13:40 CMRmg/Kg dry0.090 12/2/14SW-846 8270D1Naphthalene
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.28 12/2/14SW-846 8270D1V-202-Nitroaniline
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.19 12/2/14SW-846 8270D13-Nitroaniline
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.21 12/2/14SW-846 8270D14-Nitroaniline
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Nitrobenzene
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.12 12/2/14SW-846 8270D12-Nitrophenol
ND 0.79 12/3/14 13:40 CMRmg/Kg dry0.71 12/2/14SW-846 8270D1V-204-Nitrophenol
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1N-Nitrosodimethylamine
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.19 12/2/14SW-846 8270D1N-Nitrosodiphenylamine
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.13 12/2/14SW-846 8270D1N-Nitrosodi-n-propylamine
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.096 12/2/14SW-846 8270D1V-16, V-20Pentachloronitrobenzene
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.16 12/2/14SW-846 8270D1Pentachlorophenol
ND 0.20 12/3/14 13:40 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Phenanthrene
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.11 12/2/14SW-846 8270D1Phenol
ND 0.20 12/3/14 13:40 CMRmg/Kg dry0.14 12/2/14SW-846 8270D1Pyrene
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.17 12/2/14SW-846 8270D1Pyridine
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.24 12/2/14SW-846 8270D11,2,4,5-Tetrachlorobenzene
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.098 12/2/14SW-846 8270D11,2,4-Trichlorobenzene
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.21 12/2/14SW-846 8270D12,4,5-Trichlorophenol
ND 0.41 12/3/14 13:40 CMRmg/Kg dry0.26 12/2/14SW-846 8270D12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 68.7 12/3/14 13:4030-130
Phenol-d6 78.3 12/3/14 13:4030-130
Nitrobenzene-d5 68.4 12/3/14 13:4030-130
2-Fluorobiphenyl 75.7 12/3/14 13:4030-130
2,4,6-Tribromophenol 93.4 12/3/14 13:4030-130
p-Terphenyl-d14 94.2 12/3/14 13:4030-130
Page 69 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-09
Field Sample #: SB-9 3
Sample Matrix: Soil
Sampled: 11/26/2014 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Petroleum Hydrocarbons Analyses - EPH
ND 12 12/5/14 14:59 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C9-C18 Aliphatics
ND 12 12/5/14 14:59 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C19-C36 Aliphatics
ND 12 12/5/14 14:59 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11Unadjusted C11-C22 Aromatics
ND 12 12/5/14 14:59 SCSmg/Kg dry 12/2/14MADEP-EPH-04-1.11C11-C22 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
Chlorooctadecane (COD)74.5 12/5/14 14:5940-140
o-Terphenyl (OTP)96.3 12/5/14 14:5940-140
2-Bromonaphthalene 93.9 12/5/14 14:5940-140
2-Fluorobiphenyl 92.9 12/5/14 14:5940-140
Page 70 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-09
Field Sample #: SB-9 3
Sample Matrix: Soil
Sampled: 11/26/2014 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Sample Flags: O-01
Soil/Methanol Preservation Ratio: 1.27
Petroleum Hydrocarbons Analyses - VPH
ND 12 12/8/14 23:34 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11Unadjusted C5-C8 Aliphatics
ND 12 12/8/14 23:34 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C5-C8 Aliphatics
ND 12 12/8/14 23:34 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11Unadjusted C9-C12 Aliphatics
ND 12 12/8/14 23:34 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C9-C12 Aliphatics
ND 12 12/8/14 23:34 EEHmg/Kg dry 12/8/14MADEP-VPH-04-1.11C9-C10 Aromatics
Surrogates % Recovery Recovery Limits Flag/Qual
2,5-Dibromotoluene (FID)120 12/8/14 23:3470-130
2,5-Dibromotoluene (PID)98.4 12/8/14 23:3470-130
Page 71 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/1/2014
Work Order: 14L0056Sample Description:Project Location: Ferrell Residence
Sample ID: 14L0056-09
Field Sample #: SB-9 3
Sample Matrix: Soil
Sampled: 11/26/2014 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
83.1 12/8/14 7:48 MRL% Wt 12/4/14SM 2540G1% Solids
Page 72 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 3546-MADEP-EPH-04-1.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B110844 12/02/1420.2 2.0014L0056-01 [SB-1 3]
B110844 12/02/1420.0 2.0014L0056-02 [SB-2 3]
B110844 12/02/1420.0 2.0014L0056-03 [SB-3 3]
B110844 12/02/1420.0 2.0014L0056-04 [SB-4 3]
B110844 12/02/1420.0 2.0014L0056-05 [SB-5 3]
B110844 12/02/1420.0 2.0014L0056-06 [SB-6 3]
B110844 12/02/1420.3 2.0014L0056-07 [SB-7 3]
B110844 12/02/1420.2 2.0014L0056-08 [SB-8 3]
B110844 12/02/1420.2 2.0014L0056-09 [SB-9 3]
Prep Method: MA VPH-MADEP-VPH-04-1.1
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B111275 12/08/1417.3 17.214L0056-01 [SB-1 3]
B111275 12/08/1421.3 18.014L0056-02 [SB-2 3]
B111275 12/08/1420.2 18.014L0056-03 [SB-3 3]
B111275 12/08/1421.2 18.214L0056-04 [SB-4 3]
B111275 12/08/1418.5 18.014L0056-05 [SB-5 3]
B111275 12/08/1418.3 17.814L0056-06 [SB-6 3]
B111275 12/08/1419.9 17.414L0056-07 [SB-7 3]
B111275 12/08/1416.3 17.414L0056-08 [SB-8 3]
B111275 12/08/1419.1 18.314L0056-09 [SB-9 3]
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]Batch Date
B110965 12/04/1414L0056-01 [SB-1 3]
B110965 12/04/1414L0056-02 [SB-2 3]
B110965 12/04/1414L0056-03 [SB-3 3]
B110965 12/04/1414L0056-04 [SB-4 3]
B110965 12/04/1414L0056-05 [SB-5 3]
B110965 12/04/1414L0056-06 [SB-6 3]
B110965 12/04/1414L0056-07 [SB-7 3]
B110965 12/04/1414L0056-08 [SB-8 3]
B110965 12/04/1414L0056-09 [SB-9 3]
Prep Method: SW-846 5035-SW-846 8260B
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B111082 12/04/146.73 10.014L0056-01 [SB-1 3]
B111082 12/04/146.84 10.014L0056-02 [SB-2 3]
B111082 12/04/146.46 10.014L0056-03 [SB-3 3]
B111082 12/04/145.58 10.014L0056-04 [SB-4 3]
B111082 12/04/144.66 10.014L0056-05 [SB-5 3]
B111082 12/04/146.61 10.014L0056-06 [SB-6 3]
B111082 12/04/146.76 10.014L0056-07 [SB-7 3]
B111082 12/04/146.50 10.014L0056-08 [SB-8 3]
B111082 12/04/147.26 10.014L0056-09 [SB-9 3]
[TOC_1]Sample Preparation Information[TOC]
Page 73 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 3546-SW-846 8270D
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B110780 12/02/1430.1 1.0014L0056-09 [SB-9 3]
Prep Method: SW-846 3546-SW-846 8270D
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B110838 12/02/1430.0 1.0014L0056-01 [SB-1 3]
B110838 12/02/1430.1 1.0014L0056-02 [SB-2 3]
B110838 12/02/1430.4 1.0014L0056-03 [SB-3 3]
B110838 12/02/1430.0 1.0014L0056-04 [SB-4 3]
B110838 12/02/1430.0 1.0014L0056-05 [SB-5 3]
B110838 12/02/1430.2 1.0014L0056-06 [SB-6 3]
B110838 12/02/1430.0 1.0014L0056-07 [SB-7 3]
B110838 12/02/1430.0 1.0014L0056-08 [SB-8 3]
Page 74 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B111082 - SW-846 5035
[TOC_3]B111082[TOC]
Blank (B111082-BLK1) Prepared & Analyzed: 12/05/14
Acetone mg/Kg wet0.10ND
Acrylonitrile mg/Kg wet0.0060ND
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010ND
Benzene mg/Kg wet0.0020ND
Bromobenzene mg/Kg wet0.0020ND
Bromochloromethane mg/Kg wet0.0020ND
Bromodichloromethane mg/Kg wet0.0020ND
Bromoform mg/Kg wet0.0020ND
Bromomethane mg/Kg wet0.010ND
2-Butanone (MEK)mg/Kg wet0.040ND
tert-Butyl Alcohol (TBA)mg/Kg wet0.040ND
n-Butylbenzene mg/Kg wet0.0020ND
sec-Butylbenzene mg/Kg wet0.0020ND
tert-Butylbenzene mg/Kg wet0.0020ND
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010ND
Carbon Disulfide mg/Kg wet0.0060ND
Carbon Tetrachloride mg/Kg wet0.0020ND
Chlorobenzene mg/Kg wet0.0020ND
Chlorodibromomethane mg/Kg wet0.0010ND
Chloroethane mg/Kg wet0.020ND
Chloroform mg/Kg wet0.0040ND
Chloromethane mg/Kg wet0.010ND
2-Chlorotoluene mg/Kg wet0.0020ND
4-Chlorotoluene mg/Kg wet0.0020ND
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020ND
1,2-Dibromoethane (EDB)mg/Kg wet0.0010ND
Dibromomethane mg/Kg wet0.0020ND
1,2-Dichlorobenzene mg/Kg wet0.0020ND
1,3-Dichlorobenzene mg/Kg wet0.0020ND
1,4-Dichlorobenzene mg/Kg wet0.0020ND
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040ND
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020ND
1,1-Dichloroethane mg/Kg wet0.0020ND
1,2-Dichloroethane mg/Kg wet0.0020ND
1,1-Dichloroethylene mg/Kg wet0.0040ND
cis-1,2-Dichloroethylene mg/Kg wet0.0020ND
trans-1,2-Dichloroethylene mg/Kg wet0.0020ND
1,2-Dichloropropane mg/Kg wet0.0020ND
1,3-Dichloropropane mg/Kg wet0.0010ND
2,2-Dichloropropane mg/Kg wet0.0020ND
1,1-Dichloropropene mg/Kg wet0.0020ND
cis-1,3-Dichloropropene mg/Kg wet0.0010ND
trans-1,3-Dichloropropene mg/Kg wet0.0010ND
Diethyl Ether mg/Kg wet0.020ND
Diisopropyl Ether (DIPE)mg/Kg wet0.0010ND
1,4-Dioxane mg/Kg wet0.10ND
Ethylbenzene mg/Kg wet0.0020ND
Hexachlorobutadiene mg/Kg wet0.0020ND
2-Hexanone (MBK)mg/Kg wet0.020ND
Isopropylbenzene (Cumene)mg/Kg wet0.0020ND
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040ND
[TOC_1]QC Data[TOC]
Page 75 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B111082 - SW-846 5035
Blank (B111082-BLK1) Prepared & Analyzed: 12/05/14
Methylene Chloride mg/Kg wet0.020ND
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020ND
Naphthalene mg/Kg wet0.0040 V-05ND
n-Propylbenzene mg/Kg wet0.0020 R-05ND
Styrene mg/Kg wet0.0020ND
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020ND
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010ND
Tetrachloroethylene mg/Kg wet0.0020ND
Tetrahydrofuran mg/Kg wet0.010ND
Toluene mg/Kg wet0.0020ND
1,2,3-Trichlorobenzene mg/Kg wet0.0020 V-05ND
1,2,4-Trichlorobenzene mg/Kg wet0.0020 V-05ND
1,3,5-Trichlorobenzene mg/Kg wet0.0020ND
1,1,1-Trichloroethane mg/Kg wet0.0020ND
1,1,2-Trichloroethane mg/Kg wet0.0020ND
Trichloroethylene mg/Kg wet0.0020ND
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010ND
1,2,3-Trichloropropane mg/Kg wet0.0020ND
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010ND
1,2,4-Trimethylbenzene mg/Kg wet0.0020ND
1,3,5-Trimethylbenzene mg/Kg wet0.0020ND
Vinyl Chloride mg/Kg wet0.010ND
m+p Xylene mg/Kg wet0.0040ND
o-Xylene mg/Kg wet0.0020ND
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 1080.0538
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 99.00.0495
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 98.30.0491
LCS (B111082-BS1) Prepared & Analyzed: 12/05/14
Acetone mg/Kg wet0.10 0.200 70-1601260.252
Acrylonitrile mg/Kg wet0.0060 0.0200 70-1301090.0219
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010 0.0200 70-1301270.0254
Benzene mg/Kg wet0.0020 0.0200 70-1301090.0219
Bromobenzene mg/Kg wet0.0020 0.0200 70-1301180.0237
Bromochloromethane mg/Kg wet0.0020 0.0200 70-1301140.0228
Bromodichloromethane mg/Kg wet0.0020 0.0200 70-1301180.0237
Bromoform mg/Kg wet0.0020 0.0200 70-1301140.0227
Bromomethane mg/Kg wet0.010 0.0200 40-13075.40.0151
2-Butanone (MEK)mg/Kg wet0.040 0.200 70-1601260.252
tert-Butyl Alcohol (TBA)mg/Kg wet0.040 0.200 40-1301250.249
n-Butylbenzene mg/Kg wet0.0020 0.0200 70-1301000.0201
sec-Butylbenzene mg/Kg wet0.0020 0.0200 70-1301040.0209
tert-Butylbenzene mg/Kg wet0.0020 0.0200 70-1601000.0200
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010 0.0200 L-0270-130136*0.0272
Carbon Disulfide mg/Kg wet0.0060 0.0200 70-1301100.0220
Carbon Tetrachloride mg/Kg wet0.0020 0.0200 70-1301150.0230
Chlorobenzene mg/Kg wet0.0020 0.0200 70-1301110.0223
Chlorodibromomethane mg/Kg wet0.0010 0.0200 70-1301150.0230
Chloroethane mg/Kg wet0.020 0.0200 70-1301080.0216
Chloroform mg/Kg wet0.0040 0.0200 70-1301140.0228
Chloromethane mg/Kg wet0.010 0.0200 70-13098.90.0198
2-Chlorotoluene mg/Kg wet0.0020 0.0200 L-0770-130147*0.0295
Page 76 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B111082 - SW-846 5035
LCS (B111082-BS1) Prepared & Analyzed: 12/05/14
4-Chlorotoluene mg/Kg wet0.0020 0.0200 L-0770-130144*0.0288
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020 0.0200 70-13088.00.0176
1,2-Dibromoethane (EDB)mg/Kg wet0.0010 0.0200 70-1301130.0225
Dibromomethane mg/Kg wet0.0020 0.0200 70-1301140.0227
1,2-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-1301040.0208
1,3-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-1301100.0219
1,4-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-1301040.0209
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040 0.0200 70-1301250.0249
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020 0.0200 J40-16072.10.0144
1,1-Dichloroethane mg/Kg wet0.0020 0.0200 70-1301120.0224
1,2-Dichloroethane mg/Kg wet0.0020 0.0200 70-1301170.0234
1,1-Dichloroethylene mg/Kg wet0.0040 0.0200 70-1301210.0241
cis-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 70-1301140.0227
trans-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 70-1301120.0224
1,2-Dichloropropane mg/Kg wet0.0020 0.0200 70-1301110.0222
1,3-Dichloropropane mg/Kg wet0.0010 0.0200 70-1301090.0217
2,2-Dichloropropane mg/Kg wet0.0020 0.0200 70-1301020.0204
1,1-Dichloropropene mg/Kg wet0.0020 0.0200 70-1301200.0239
cis-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 70-13098.30.0197
trans-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 70-1301100.0220
Diethyl Ether mg/Kg wet0.020 0.0200 70-1301220.0244
Diisopropyl Ether (DIPE)mg/Kg wet0.0010 0.0200 70-1301180.0236
1,4-Dioxane mg/Kg wet0.10 0.200 40-1601010.202
Ethylbenzene mg/Kg wet0.0020 0.0200 70-1301200.0239
Hexachlorobutadiene mg/Kg wet0.0020 0.0200 70-16088.60.0177
2-Hexanone (MBK)mg/Kg wet0.020 0.200 70-1601270.253
Isopropylbenzene (Cumene)mg/Kg wet0.0020 0.0200 70-1301250.0250
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020 0.0200 70-1301120.0225
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040 0.0200 L-0270-130138*0.0277
Methylene Chloride mg/Kg wet0.020 0.0200 40-1601060.0211
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020 0.200 70-1601170.234
Naphthalene mg/Kg wet0.0040 0.0200 V-0540-13067.60.0135
n-Propylbenzene mg/Kg wet0.0020 0.0200 L-07A, R-0570-130159*0.0317
Styrene mg/Kg wet0.0020 0.0200 70-1301170.0235
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020 0.0200 70-1301160.0231
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010 0.0200 70-1301230.0246
Tetrachloroethylene mg/Kg wet0.0020 0.0200 70-1301200.0239
Tetrahydrofuran mg/Kg wet0.010 0.0200 70-1301060.0212
Toluene mg/Kg wet0.0020 0.0200 70-1301020.0203
1,2,3-Trichlorobenzene mg/Kg wet0.0020 0.0200 V-0570-13072.40.0145
1,2,4-Trichlorobenzene mg/Kg wet0.0020 0.0200 V-0570-13072.40.0145
1,3,5-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-13080.90.0162
1,1,1-Trichloroethane mg/Kg wet0.0020 0.0200 70-1301060.0212
1,1,2-Trichloroethane mg/Kg wet0.0020 0.0200 70-1301090.0218
Trichloroethylene mg/Kg wet0.0020 0.0200 70-1301090.0219
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010 0.0200 70-1301190.0238
1,2,3-Trichloropropane mg/Kg wet0.0020 0.0200 70-1301290.0259
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010 0.0200 70-1301200.0239
1,2,4-Trimethylbenzene mg/Kg wet0.0020 0.0200 70-1301000.0200
1,3,5-Trimethylbenzene mg/Kg wet0.0020 0.0200 L-0770-130143*0.0285
Vinyl Chloride mg/Kg wet0.010 0.0200 40-1301010.0202
Page 77 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B111082 - SW-846 5035
LCS (B111082-BS1) Prepared & Analyzed: 12/05/14
m+p Xylene mg/Kg wet0.0040 0.0400 70-1301220.0486
o-Xylene mg/Kg wet0.0020 0.0200 70-1301220.0244
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 1040.0519
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 99.70.0498
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1060.0532
LCS Dup (B111082-BSD1) Prepared & Analyzed: 12/05/14
Acetone mg/Kg wet0.10 0.200 2570-160130 2.760.259
Acrylonitrile mg/Kg wet0.0060 0.0200 2570-130105 4.100.0210
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010 0.0200 2570-130120 5.420.0241
Benzene mg/Kg wet0.0020 0.0200 2570-130106 3.530.0211
Bromobenzene mg/Kg wet0.0020 0.0200 2570-130104 12.60.0209
Bromochloromethane mg/Kg wet0.0020 0.0200 2570-130108 5.140.0216
Bromodichloromethane mg/Kg wet0.0020 0.0200 2570-130112 5.200.0225
Bromoform mg/Kg wet0.0020 0.0200 2570-130118 3.970.0237
Bromomethane mg/Kg wet0.010 0.0200 2540-13079.0 4.660.0158
2-Butanone (MEK)mg/Kg wet0.040 0.200 2570-160129 1.960.257
tert-Butyl Alcohol (TBA)mg/Kg wet0.040 0.200 2540-130117 6.240.234
n-Butylbenzene mg/Kg wet0.0020 0.0200 2570-130102 1.190.0203
sec-Butylbenzene mg/Kg wet0.0020 0.0200 2570-130108 3.020.0215
tert-Butylbenzene mg/Kg wet0.0020 0.0200 2570-160103 2.950.0206
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010 0.0200 25 L-0270-130131 3.82*0.0262
Carbon Disulfide mg/Kg wet0.0060 0.0200 2570-130110 0.4540.0221
Carbon Tetrachloride mg/Kg wet0.0020 0.0200 2570-130110 4.270.0220
Chlorobenzene mg/Kg wet0.0020 0.0200 2570-130108 3.380.0215
Chlorodibromomethane mg/Kg wet0.0010 0.0200 2570-130112 2.290.0225
Chloroethane mg/Kg wet0.020 0.0200 2570-130106 1.680.0212
Chloroform mg/Kg wet0.0040 0.0200 2570-130110 3.300.0221
Chloromethane mg/Kg wet0.010 0.0200 2570-13099.1 0.2020.0198
2-Chlorotoluene mg/Kg wet0.0020 0.0200 2570-130116 23.50.0233
4-Chlorotoluene mg/Kg wet0.0020 0.0200 2570-130116 21.70.0231
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020 0.0200 2570-13097.2 9.940.0194
1,2-Dibromoethane (EDB)mg/Kg wet0.0010 0.0200 2570-130110 2.420.0220
Dibromomethane mg/Kg wet0.0020 0.0200 2570-130111 2.580.0222
1,2-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-130109 4.510.0218
1,3-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-130112 2.340.0225
1,4-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-130105 0.09560.0209
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040 0.0200 2570-130102 20.00.0204
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020 0.0200 25 J40-16072.8 0.9660.0146
1,1-Dichloroethane mg/Kg wet0.0020 0.0200 2570-130109 2.990.0217
1,2-Dichloroethane mg/Kg wet0.0020 0.0200 2570-130113 3.920.0225
1,1-Dichloroethylene mg/Kg wet0.0040 0.0200 2570-130120 0.7480.0240
cis-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 2570-130108 4.690.0217
trans-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 2570-130107 4.390.0214
1,2-Dichloropropane mg/Kg wet0.0020 0.0200 2570-130109 2.000.0218
1,3-Dichloropropane mg/Kg wet0.0010 0.0200 2570-130108 0.4610.0216
2,2-Dichloropropane mg/Kg wet0.0020 0.0200 2570-13096.2 6.050.0192
1,1-Dichloropropene mg/Kg wet0.0020 0.0200 2570-130116 2.890.0232
cis-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 2570-13094.7 3.730.0189
trans-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 2570-130106 3.520.0212
Diethyl Ether mg/Kg wet0.020 0.0200 2570-130118 3.420.0236
Diisopropyl Ether (DIPE)mg/Kg wet0.0010 0.0200 2570-130115 2.830.0230
Page 78 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B111082 - SW-846 5035
LCS Dup (B111082-BSD1) Prepared & Analyzed: 12/05/14
1,4-Dioxane mg/Kg wet0.10 0.200 5040-16093.5 7.950.187
Ethylbenzene mg/Kg wet0.0020 0.0200 2570-130114 4.450.0229
Hexachlorobutadiene mg/Kg wet0.0020 0.0200 2570-16090.8 2.450.0182
2-Hexanone (MBK)mg/Kg wet0.020 0.200 2570-160129 1.920.258
Isopropylbenzene (Cumene)mg/Kg wet0.0020 0.0200 2570-130106 16.70.0211
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020 0.0200 2570-130110 2.070.0220
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040 0.0200 25 L-0270-130131 5.80*0.0261
Methylene Chloride mg/Kg wet0.020 0.0200 2540-160100 5.350.0200
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020 0.200 2570-160115 1.300.231
Naphthalene mg/Kg wet0.0040 0.0200 25 V-0540-13067.2 0.5930.0134
n-Propylbenzene mg/Kg wet0.0020 0.0200 25 R-0570-130117 30.1 *0.0234
Styrene mg/Kg wet0.0020 0.0200 2570-130115 2.410.0229
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020 0.0200 2570-130113 2.540.0225
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010 0.0200 2570-130102 18.60.0204
Tetrachloroethylene mg/Kg wet0.0020 0.0200 2570-130116 2.540.0233
Tetrahydrofuran mg/Kg wet0.010 0.0200 2570-130114 7.190.0228
Toluene mg/Kg wet0.0020 0.0200 2570-130101 0.5930.0202
1,2,3-Trichlorobenzene mg/Kg wet0.0020 0.0200 25 V-0570-13073.6 1.640.0147
1,2,4-Trichlorobenzene mg/Kg wet0.0020 0.0200 25 V-0570-13072.8 0.5510.0146
1,3,5-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-13096.7 17.80.0193
1,1,1-Trichloroethane mg/Kg wet0.0020 0.0200 2570-130103 2.680.0206
1,1,2-Trichloroethane mg/Kg wet0.0020 0.0200 2570-130108 0.6440.0217
Trichloroethylene mg/Kg wet0.0020 0.0200 2570-130104 5.160.0208
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010 0.0200 2570-130118 1.100.0236
1,2,3-Trichloropropane mg/Kg wet0.0020 0.0200 2570-130109 17.10.0218
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010 0.0200 2570-130115 4.010.0230
1,2,4-Trimethylbenzene mg/Kg wet0.0020 0.0200 2570-130103 2.760.0206
1,3,5-Trimethylbenzene mg/Kg wet0.0020 0.0200 2570-130114 22.40.0228
Vinyl Chloride mg/Kg wet0.010 0.0200 2540-13099.5 1.400.0199
m+p Xylene mg/Kg wet0.0040 0.0400 2570-130116 4.630.0464
o-Xylene mg/Kg wet0.0020 0.0200 2570-130117 4.110.0234
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 1030.0514
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 99.90.0499
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 99.90.0500
Page 79 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Semivolatile Organic Compounds by GC/MS[TOC]
Batch B110780 - SW-846 3546
[TOC_3]B110780[TOC]
Blank (B110780-BLK1) Prepared & Analyzed: 12/02/14
Acenaphthene mg/Kg wet0.17ND
Acenaphthylene mg/Kg wet0.17ND
Acetophenone mg/Kg wet0.34ND
Aniline mg/Kg wet0.34ND
Anthracene mg/Kg wet0.17ND
Benzidine mg/Kg wet0.66 V-04, V-05ND
Benzo(a)anthracene mg/Kg wet0.17ND
Benzo(a)pyrene mg/Kg wet0.17ND
Benzo(b)fluoranthene mg/Kg wet0.17ND
Benzo(g,h,i)perylene mg/Kg wet0.17ND
Benzo(k)fluoranthene mg/Kg wet0.17ND
Benzoic Acid mg/Kg wet1.0 L-04ND
Bis(2-chloroethoxy)methane mg/Kg wet0.34ND
Bis(2-chloroethyl)ether mg/Kg wet0.34ND
Bis(2-chloroisopropyl)ether mg/Kg wet0.34ND
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 J0.20
4-Bromophenylphenylether mg/Kg wet0.34ND
Butylbenzylphthalate mg/Kg wet0.34ND
Carbazole mg/Kg wet0.17ND
4-Chloroaniline mg/Kg wet0.66ND
4-Chloro-3-methylphenol mg/Kg wet0.66ND
2-Chloronaphthalene mg/Kg wet0.34ND
2-Chlorophenol mg/Kg wet0.34ND
4-Chlorophenylphenylether mg/Kg wet0.34ND
Chrysene mg/Kg wet0.17ND
Dibenz(a,h)anthracene mg/Kg wet0.17ND
Dibenzofuran mg/Kg wet0.34ND
Di-n-butylphthalate mg/Kg wet0.34ND
1,2-Dichlorobenzene mg/Kg wet0.34ND
1,3-Dichlorobenzene mg/Kg wet0.34ND
1,4-Dichlorobenzene mg/Kg wet0.34ND
3,3-Dichlorobenzidine mg/Kg wet0.17ND
2,4-Dichlorophenol mg/Kg wet0.34ND
Diethylphthalate mg/Kg wet0.34ND
2,4-Dimethylphenol mg/Kg wet0.34ND
Dimethylphthalate mg/Kg wet0.34ND
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 R-05ND
2,4-Dinitrophenol mg/Kg wet0.66 L-04ND
2,4-Dinitrotoluene mg/Kg wet0.34 V-20ND
2,6-Dinitrotoluene mg/Kg wet0.34 V-20ND
Di-n-octylphthalate mg/Kg wet0.67ND
1,2-Diphenylhydrazine (as Azobenzene)mg/Kg wet0.34ND
Fluoranthene mg/Kg wet0.17ND
Fluorene mg/Kg wet0.17ND
Hexachlorobenzene mg/Kg wet0.34ND
Hexachlorobutadiene mg/Kg wet0.34ND
Hexachlorocyclopentadiene mg/Kg wet0.34 V-05ND
Hexachloroethane mg/Kg wet0.34ND
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17ND
Isophorone mg/Kg wet0.34ND
1-Methylnaphthalene mg/Kg wet0.17ND
2-Methylnaphthalene mg/Kg wet0.17ND
Page 80 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B110780 - SW-846 3546
Blank (B110780-BLK1) Prepared & Analyzed: 12/02/14
2-Methylphenol mg/Kg wet0.34ND
3/4-Methylphenol mg/Kg wet0.34ND
Naphthalene mg/Kg wet0.17ND
2-Nitroaniline mg/Kg wet0.34ND
3-Nitroaniline mg/Kg wet0.34ND
4-Nitroaniline mg/Kg wet0.34 V-20ND
Nitrobenzene mg/Kg wet0.34ND
2-Nitrophenol mg/Kg wet0.34ND
4-Nitrophenol mg/Kg wet0.66ND
N-Nitrosodimethylamine mg/Kg wet0.34ND
N-Nitrosodiphenylamine mg/Kg wet0.34ND
N-Nitrosodi-n-propylamine mg/Kg wet0.34ND
Pentachloronitrobenzene mg/Kg wet0.34 V-16ND
Pentachlorophenol mg/Kg wet0.34ND
Phenanthrene mg/Kg wet0.17ND
Phenol mg/Kg wet0.34ND
Pyrene mg/Kg wet0.17ND
Pyridine mg/Kg wet0.34ND
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34ND
1,2,4-Trichlorobenzene mg/Kg wet0.34ND
2,4,5-Trichlorophenol mg/Kg wet0.34ND
2,4,6-Trichlorophenol mg/Kg wet0.34ND
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 87.05.80
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 89.85.99
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 83.22.77
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 90.93.03
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 89.55.96
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 96.23.21
LCS (B110780-BS1) Prepared & Analyzed: 12/02/14
Acenaphthene mg/Kg wet0.17 1.67 40-14094.11.57
Acenaphthylene mg/Kg wet0.17 1.67 40-14098.91.65
Acetophenone mg/Kg wet0.34 1.67 40-14088.61.48
Aniline mg/Kg wet0.34 1.67 10-14042.10.702
Anthracene mg/Kg wet0.17 1.67 40-1401031.72
Benzidine mg/Kg wet0.66 1.67 V-04, V-0540-14050.80.846
Benzo(a)anthracene mg/Kg wet0.17 1.67 40-1401031.71
Benzo(a)pyrene mg/Kg wet0.17 1.67 40-1401021.70
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 40-14098.71.64
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 40-1401031.72
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 40-14096.81.61
Benzoic Acid mg/Kg wet1.0 1.67 L-04, J30-1308.96 *0.149
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 40-14089.31.49
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 40-14085.81.43
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 40-14072.81.21
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 40-1401051.75
4-Bromophenylphenylether mg/Kg wet0.34 1.67 40-14097.91.63
Butylbenzylphthalate mg/Kg wet0.34 1.67 40-14095.21.59
Carbazole mg/Kg wet0.17 1.67 40-1401081.80
4-Chloroaniline mg/Kg wet0.66 1.67 10-14055.50.925
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 30-13099.21.65
2-Chloronaphthalene mg/Kg wet0.34 1.67 40-14092.61.54
Page 81 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B110780 - SW-846 3546
LCS (B110780-BS1) Prepared & Analyzed: 12/02/14
2-Chlorophenol mg/Kg wet0.34 1.67 30-13092.91.55
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 40-14099.31.66
Chrysene mg/Kg wet0.17 1.67 40-1401031.72
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 40-1401081.80
Dibenzofuran mg/Kg wet0.34 1.67 40-1401081.80
Di-n-butylphthalate mg/Kg wet0.34 1.67 40-14098.71.64
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 40-14083.41.39
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 40-14079.81.33
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 40-14080.91.35
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 20-14059.20.987
2,4-Dichlorophenol mg/Kg wet0.34 1.67 30-1301001.67
Diethylphthalate mg/Kg wet0.34 1.67 40-14099.91.66
2,4-Dimethylphenol mg/Kg wet0.34 1.67 30-13088.91.48
Dimethylphthalate mg/Kg wet0.34 1.67 40-1401001.67
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 R-0530-13058.40.974
2,4-Dinitrophenol mg/Kg wet0.66 1.67 L-04, J30-13022.3 *0.372
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 V-0640-1401131.89
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 V-0640-1401141.90
Di-n-octylphthalate mg/Kg wet0.67 1.67 40-14091.81.53
1,2-Diphenylhydrazine (as Azobenzene)mg/Kg wet0.34 1.67 40-14092.41.54
Fluoranthene mg/Kg wet0.17 1.67 40-1401071.79
Fluorene mg/Kg wet0.17 1.67 40-1401041.73
Hexachlorobenzene mg/Kg wet0.34 1.67 40-1401061.76
Hexachlorobutadiene mg/Kg wet0.34 1.67 40-14087.71.46
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 V-0540-14063.01.05
Hexachloroethane mg/Kg wet0.34 1.67 40-14080.51.34
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 40-1401091.81
Isophorone mg/Kg wet0.34 1.67 40-14093.61.56
1-Methylnaphthalene mg/Kg wet0.17 1.67 40-14091.91.53
2-Methylnaphthalene mg/Kg wet0.17 1.67 40-14099.51.66
2-Methylphenol mg/Kg wet0.34 1.67 30-13084.31.40
3/4-Methylphenol mg/Kg wet0.34 1.67 30-13096.21.60
Naphthalene mg/Kg wet0.17 1.67 40-14089.11.48
2-Nitroaniline mg/Kg wet0.34 1.67 40-1401031.71
3-Nitroaniline mg/Kg wet0.34 1.67 30-14094.91.58
4-Nitroaniline mg/Kg wet0.34 1.67 40-1401151.91
Nitrobenzene mg/Kg wet0.34 1.67 40-14086.31.44
2-Nitrophenol mg/Kg wet0.34 1.67 30-13097.41.62
4-Nitrophenol mg/Kg wet0.66 1.67 30-1301131.88
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 40-14075.61.26
N-Nitrosodiphenylamine mg/Kg wet0.34 1.67 40-1401242.06
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 40-14084.01.40
Pentachloronitrobenzene mg/Kg wet0.34 1.67 V-1640-1401101.84
Pentachlorophenol mg/Kg wet0.34 1.67 30-13045.30.755
Phenanthrene mg/Kg wet0.17 1.67 40-1401041.73
Phenol mg/Kg wet0.34 1.67 30-13095.01.58
Pyrene mg/Kg wet0.17 1.67 40-14099.51.66
Pyridine mg/Kg wet0.34 1.67 30-14056.40.940
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 40-14097.51.63
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 40-14092.01.53
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 30-13098.31.64
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 30-13099.51.66
Page 82 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B110780 - SW-846 3546
LCS (B110780-BS1) Prepared & Analyzed: 12/02/14
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 95.06.33
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 99.46.63
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 91.83.06
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 1033.43
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 1177.82
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 1053.50
LCS Dup (B110780-BSD1) Prepared & Analyzed: 12/02/14
Acenaphthene mg/Kg wet0.17 1.67 3040-14089.2 5.351.49
Acenaphthylene mg/Kg wet0.17 1.67 3040-14093.2 5.931.55
Acetophenone mg/Kg wet0.34 1.67 3040-14083.8 5.641.40
Aniline mg/Kg wet0.34 1.67 5010-14037.8 10.80.630
Anthracene mg/Kg wet0.17 1.67 3040-14095.0 8.101.58
Benzidine mg/Kg wet0.66 1.67 30 V-04, V-0540-14047.9 5.840.798
Benzo(a)anthracene mg/Kg wet0.17 1.67 3040-14095.7 6.901.60
Benzo(a)pyrene mg/Kg wet0.17 1.67 3040-14095.2 7.051.59
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 3040-14092.2 6.791.54
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 3040-14095.5 7.891.59
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 3040-14091.2 5.941.52
Benzoic Acid mg/Kg wet1.0 1.67 50 L-04, J30-1305.68 44.8*0.0947
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 3040-14083.5 6.781.39
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 3040-14080.1 6.971.33
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 3040-14066.5 9.021.11
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 3040-14095.7 9.441.59
4-Bromophenylphenylether mg/Kg wet0.34 1.67 3040-14091.8 6.351.53
Butylbenzylphthalate mg/Kg wet0.34 1.67 3040-14087.0 9.071.45
Carbazole mg/Kg wet0.17 1.67 3040-14099.3 8.421.65
4-Chloroaniline mg/Kg wet0.66 1.67 3010-14052.0 6.550.866
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 3030-13092.0 7.511.53
2-Chloronaphthalene mg/Kg wet0.34 1.67 3040-14080.8 13.51.35
2-Chlorophenol mg/Kg wet0.34 1.67 3030-13087.5 5.971.46
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 3040-14093.6 5.971.56
Chrysene mg/Kg wet0.17 1.67 3040-14096.5 6.871.61
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 3040-14099.9 7.751.67
Dibenzofuran mg/Kg wet0.34 1.67 3040-140102 5.181.70
Di-n-butylphthalate mg/Kg wet0.34 1.67 3040-14090.1 9.071.50
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14081.5 2.331.36
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14079.5 0.4021.32
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14079.4 1.851.32
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 5020-14055.3 6.740.922
2,4-Dichlorophenol mg/Kg wet0.34 1.67 3030-13093.8 6.601.56
Diethylphthalate mg/Kg wet0.34 1.67 3040-14091.8 8.451.53
2,4-Dimethylphenol mg/Kg wet0.34 1.67 3030-13086.1 3.181.43
Dimethylphthalate mg/Kg wet0.34 1.67 3040-14092.8 7.531.55
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 30 R-0530-13042.4 31.7 *0.707
2,4-Dinitrophenol mg/Kg wet0.66 1.67 30 L-04, J30-13017.1 26.4*0.285
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 30 V-0640-140106 6.651.77
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 30 V-0640-140106 7.431.76
Di-n-octylphthalate mg/Kg wet0.67 1.67 3040-14083.1 9.971.38
1,2-Diphenylhydrazine (as Azobenzene)mg/Kg wet0.34 1.67 3040-14083.2 10.51.39
Fluoranthene mg/Kg wet0.17 1.67 3040-140100 7.151.67
Fluorene mg/Kg wet0.17 1.67 3040-14098.2 5.681.64
Page 83 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B110780 - SW-846 3546
LCS Dup (B110780-BSD1) Prepared & Analyzed: 12/02/14
Hexachlorobenzene mg/Kg wet0.34 1.67 3040-14098.9 6.671.65
Hexachlorobutadiene mg/Kg wet0.34 1.67 3040-14086.9 0.9401.45
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 30 V-0540-14060.2 4.581.00
Hexachloroethane mg/Kg wet0.34 1.67 3040-14078.9 1.981.32
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 3040-140102 5.931.71
Isophorone mg/Kg wet0.34 1.67 3040-14087.7 6.531.46
1-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14086.7 5.761.45
2-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14094.4 5.241.57
2-Methylphenol mg/Kg wet0.34 1.67 3030-13079.4 5.941.32
3/4-Methylphenol mg/Kg wet0.34 1.67 3030-13088.8 8.041.48
Naphthalene mg/Kg wet0.17 1.67 3040-14085.4 4.291.42
2-Nitroaniline mg/Kg wet0.34 1.67 3040-14095.1 7.821.59
3-Nitroaniline mg/Kg wet0.34 1.67 3030-14091.2 3.951.52
4-Nitroaniline mg/Kg wet0.34 1.67 3040-140107 6.891.78
Nitrobenzene mg/Kg wet0.34 1.67 3040-14082.1 4.991.37
2-Nitrophenol mg/Kg wet0.34 1.67 3030-13094.1 3.361.57
4-Nitrophenol mg/Kg wet0.66 1.67 5030-13099.3 13.01.65
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 3040-14073.8 2.381.23
N-Nitrosodiphenylamine mg/Kg wet0.34 1.67 3040-140115 7.251.92
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 3040-14076.7 9.181.28
Pentachloronitrobenzene mg/Kg wet0.34 1.67 30 V-1640-140105 5.271.74
Pentachlorophenol mg/Kg wet0.34 1.67 3030-13040.6 11.00.676
Phenanthrene mg/Kg wet0.17 1.67 3040-14097.1 6.881.62
Phenol mg/Kg wet0.34 1.67 3030-13088.6 6.951.48
Pyrene mg/Kg wet0.17 1.67 3040-14091.7 8.161.53
Pyridine mg/Kg wet0.34 1.67 3030-14056.2 0.3550.936
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 3040-14095.1 2.531.58
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 3040-14090.7 1.421.51
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 3030-13093.5 4.981.56
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 3030-13095.5 4.101.59
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 88.25.88
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 90.56.03
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 85.72.86
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 95.33.18
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 1107.34
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 95.13.17
Batch B110838 - SW-846 3546
[TOC_3]B110838[TOC]
Blank (B110838-BLK1) Prepared: 12/02/14 Analyzed: 12/03/14
Acenaphthene mg/Kg wet0.17ND
Acenaphthylene mg/Kg wet0.17ND
Acetophenone mg/Kg wet0.34ND
Aniline mg/Kg wet0.34ND
Anthracene mg/Kg wet0.17ND
Benzidine mg/Kg wet0.66 V-04, V-05ND
Benzo(a)anthracene mg/Kg wet0.17ND
Benzo(a)pyrene mg/Kg wet0.17ND
Benzo(b)fluoranthene mg/Kg wet0.17ND
Benzo(g,h,i)perylene mg/Kg wet0.17ND
Benzo(k)fluoranthene mg/Kg wet0.17ND
Benzoic Acid mg/Kg wet1.0ND
Bis(2-chloroethoxy)methane mg/Kg wet0.34ND
Page 84 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B110838 - SW-846 3546
Blank (B110838-BLK1) Prepared: 12/02/14 Analyzed: 12/03/14
Bis(2-chloroethyl)ether mg/Kg wet0.34ND
Bis(2-chloroisopropyl)ether mg/Kg wet0.34ND
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34ND
4-Bromophenylphenylether mg/Kg wet0.34ND
Butylbenzylphthalate mg/Kg wet0.34ND
Carbazole mg/Kg wet0.17ND
4-Chloroaniline mg/Kg wet0.66ND
4-Chloro-3-methylphenol mg/Kg wet0.66ND
2-Chloronaphthalene mg/Kg wet0.34ND
2-Chlorophenol mg/Kg wet0.34ND
4-Chlorophenylphenylether mg/Kg wet0.34ND
Chrysene mg/Kg wet0.17ND
Dibenz(a,h)anthracene mg/Kg wet0.17ND
Dibenzofuran mg/Kg wet0.34ND
Di-n-butylphthalate mg/Kg wet0.34ND
1,2-Dichlorobenzene mg/Kg wet0.34ND
1,3-Dichlorobenzene mg/Kg wet0.34ND
1,4-Dichlorobenzene mg/Kg wet0.34ND
3,3-Dichlorobenzidine mg/Kg wet0.17ND
2,4-Dichlorophenol mg/Kg wet0.34ND
Diethylphthalate mg/Kg wet0.34ND
2,4-Dimethylphenol mg/Kg wet0.34ND
Dimethylphthalate mg/Kg wet0.34ND
4,6-Dinitro-2-methylphenol mg/Kg wet0.34ND
2,4-Dinitrophenol mg/Kg wet0.66ND
2,4-Dinitrotoluene mg/Kg wet0.34 V-20ND
2,6-Dinitrotoluene mg/Kg wet0.34 V-20ND
Di-n-octylphthalate mg/Kg wet0.67ND
1,2-Diphenylhydrazine (as Azobenzene)mg/Kg wet0.34ND
Fluoranthene mg/Kg wet0.17ND
Fluorene mg/Kg wet0.17ND
Hexachlorobenzene mg/Kg wet0.34ND
Hexachlorobutadiene mg/Kg wet0.34ND
Hexachlorocyclopentadiene mg/Kg wet0.34 V-05ND
Hexachloroethane mg/Kg wet0.34ND
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17ND
Isophorone mg/Kg wet0.34ND
1-Methylnaphthalene mg/Kg wet0.17ND
2-Methylnaphthalene mg/Kg wet0.17ND
2-Methylphenol mg/Kg wet0.34ND
3/4-Methylphenol mg/Kg wet0.34ND
Naphthalene mg/Kg wet0.17ND
2-Nitroaniline mg/Kg wet0.34ND
3-Nitroaniline mg/Kg wet0.34ND
4-Nitroaniline mg/Kg wet0.34ND
Nitrobenzene mg/Kg wet0.34ND
2-Nitrophenol mg/Kg wet0.34ND
4-Nitrophenol mg/Kg wet0.66ND
N-Nitrosodimethylamine mg/Kg wet0.34ND
N-Nitrosodiphenylamine mg/Kg wet0.34ND
N-Nitrosodi-n-propylamine mg/Kg wet0.34ND
Pentachloronitrobenzene mg/Kg wet0.34 V-16ND
Page 85 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B110838 - SW-846 3546
Blank (B110838-BLK1) Prepared: 12/02/14 Analyzed: 12/03/14
Pentachlorophenol mg/Kg wet0.34ND
Phenanthrene mg/Kg wet0.17ND
Phenol mg/Kg wet0.34ND
Pyrene mg/Kg wet0.17ND
Pyridine mg/Kg wet0.34ND
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34ND
1,2,4-Trichlorobenzene mg/Kg wet0.34ND
2,4,5-Trichlorophenol mg/Kg wet0.34ND
2,4,6-Trichlorophenol mg/Kg wet0.34ND
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 93.26.22
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 96.36.42
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 85.82.86
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 1083.59
mg/Kg wet 6.67 S-0730-130Surrogate: 2,4,6-Tribromophenol 1369.06 *
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 1284.28
LCS (B110838-BS1) Prepared: 12/02/14 Analyzed: 12/03/14
Acenaphthene mg/Kg wet0.17 1.67 40-1401111.84
Acenaphthylene mg/Kg wet0.17 1.67 40-1401161.93
Acetophenone mg/Kg wet0.34 1.67 40-14086.61.44
Aniline mg/Kg wet0.34 1.67 10-14045.60.760
Anthracene mg/Kg wet0.17 1.67 40-1401232.05
Benzidine mg/Kg wet0.66 1.67 V-05, V-0440-14063.61.06
Benzo(a)anthracene mg/Kg wet0.17 1.67 40-1401252.08
Benzo(a)pyrene mg/Kg wet0.17 1.67 40-1401242.07
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 40-1401212.01
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 40-1401171.94
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 40-1401181.97
Benzoic Acid mg/Kg wet0.17 1.67 30-13036.20.603
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 40-14090.91.52
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 40-14074.11.24
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 40-14060.00.999
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 40-1401161.94
4-Bromophenylphenylether mg/Kg wet0.34 1.67 40-1401242.06
Butylbenzylphthalate mg/Kg wet0.34 1.67 40-1401131.88
Carbazole mg/Kg wet0.17 1.67 40-1401282.13
4-Chloroaniline mg/Kg wet0.66 1.67 10-14057.80.963
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 30-1301161.93
2-Chloronaphthalene mg/Kg wet0.34 1.67 40-14099.21.65
2-Chlorophenol mg/Kg wet0.34 1.67 30-13092.51.54
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 40-1401262.10
Chrysene mg/Kg wet0.17 1.67 40-1401242.07
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 40-1401262.10
Dibenzofuran mg/Kg wet0.34 1.67 40-1401312.18
Di-n-butylphthalate mg/Kg wet0.34 1.67 40-1401191.98
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 40-14075.71.26
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 40-14071.41.19
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 40-14072.81.21
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 20-14077.81.30
2,4-Dichlorophenol mg/Kg wet0.34 1.67 30-1301212.02
Diethylphthalate mg/Kg wet0.34 1.67 40-1401232.05
2,4-Dimethylphenol mg/Kg wet0.34 1.67 30-1301011.69
Page 86 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B110838 - SW-846 3546
LCS (B110838-BS1) Prepared: 12/02/14 Analyzed: 12/03/14
Dimethylphthalate mg/Kg wet0.34 1.67 40-1401242.06
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 30-13089.61.49
2,4-Dinitrophenol mg/Kg wet0.66 1.67 30-13046.90.781
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 V-0640-1401402.33
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 V-0640-1401362.27
Di-n-octylphthalate mg/Kg wet0.67 1.67 40-1401071.78
1,2-Diphenylhydrazine (as Azobenzene)mg/Kg wet0.34 1.67 40-14094.71.58
Fluoranthene mg/Kg wet0.17 1.67 40-1401332.21
Fluorene mg/Kg wet0.17 1.67 40-1401282.13
Hexachlorobenzene mg/Kg wet0.34 1.67 40-1401362.26
Hexachlorobutadiene mg/Kg wet0.34 1.67 40-14092.31.54
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 V-0540-14062.51.04
Hexachloroethane mg/Kg wet0.34 1.67 40-14069.21.15
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 40-1401272.12
Isophorone mg/Kg wet0.34 1.67 40-14094.71.58
1-Methylnaphthalene mg/Kg wet0.17 1.67 40-1401031.72
2-Methylnaphthalene mg/Kg wet0.17 1.67 40-1401111.84
2-Methylphenol mg/Kg wet0.34 1.67 30-13089.61.49
3/4-Methylphenol mg/Kg wet0.34 1.67 30-1301061.77
Naphthalene mg/Kg wet0.17 1.67 40-14091.21.52
2-Nitroaniline mg/Kg wet0.34 1.67 40-1401061.77
3-Nitroaniline mg/Kg wet0.34 1.67 30-1401031.72
4-Nitroaniline mg/Kg wet0.34 1.67 40-1401282.14
Nitrobenzene mg/Kg wet0.34 1.67 40-14079.61.33
2-Nitrophenol mg/Kg wet0.34 1.67 30-1301011.68
4-Nitrophenol mg/Kg wet0.66 1.67 30-1301282.14
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 40-14057.50.958
N-Nitrosodiphenylamine mg/Kg wet0.34 1.67 L-0740-140146*2.43
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 40-14080.11.34
Pentachloronitrobenzene mg/Kg wet0.34 1.67 L-07, V-1640-140143*2.38
Pentachlorophenol mg/Kg wet0.34 1.67 30-13088.81.48
Phenanthrene mg/Kg wet0.17 1.67 40-1401252.08
Phenol mg/Kg wet0.34 1.67 30-13096.11.60
Pyrene mg/Kg wet0.17 1.67 40-1401212.02
Pyridine mg/Kg wet0.34 1.67 30-14043.20.721
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 40-1401111.84
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 40-14096.51.61
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 30-1301262.10
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 30-1301262.11
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 89.05.94
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 1006.68
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 84.92.83
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 1193.96
mg/Kg wet 6.67 S-0730-130Surrogate: 2,4,6-Tribromophenol 16511.0 *
mg/Kg wet 3.33 S-0730-130Surrogate: p-Terphenyl-d14 1354.52 *
Page 87 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B110838 - SW-846 3546
LCS Dup (B110838-BSD1) Prepared: 12/02/14 Analyzed: 12/03/14
Acenaphthene mg/Kg wet0.17 1.67 3040-14094.8 15.41.58
Acenaphthylene mg/Kg wet0.17 1.67 3040-140101 13.51.69
Acetophenone mg/Kg wet0.34 1.67 3040-14081.6 5.921.36
Aniline mg/Kg wet0.34 1.67 5010-14044.3 2.940.738
Anthracene mg/Kg wet0.17 1.67 3040-140109 12.21.82
Benzidine mg/Kg wet0.66 1.67 30 V-04, V-0540-14057.2 10.60.954
Benzo(a)anthracene mg/Kg wet0.17 1.67 3040-140109 13.71.82
Benzo(a)pyrene mg/Kg wet0.17 1.67 3040-140111 11.41.85
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 3040-140108 10.71.81
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 3040-140102 13.01.71
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 3040-140108 9.341.79
Benzoic Acid mg/Kg wet1.0 1.67 50 J30-13044.9 21.40.748
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 3040-14085.1 6.631.42
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 3040-14075.1 1.231.25
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 3040-14060.7 1.161.01
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 3040-140105 9.591.76
4-Bromophenylphenylether mg/Kg wet0.34 1.67 3040-140107 14.01.79
Butylbenzylphthalate mg/Kg wet0.34 1.67 3040-140101 10.81.68
Carbazole mg/Kg wet0.17 1.67 3040-140114 11.61.89
4-Chloroaniline mg/Kg wet0.66 1.67 3010-14053.2 8.360.886
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 3030-130105 9.841.75
2-Chloronaphthalene mg/Kg wet0.34 1.67 3040-14089.6 10.21.49
2-Chlorophenol mg/Kg wet0.34 1.67 3030-13085.3 8.101.42
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 3040-140110 14.11.82
Chrysene mg/Kg wet0.17 1.67 3040-140110 12.21.83
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 3040-140110 13.11.84
Dibenzofuran mg/Kg wet0.34 1.67 3040-140113 14.61.88
Di-n-butylphthalate mg/Kg wet0.34 1.67 3040-140108 10.21.79
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14075.5 0.1591.26
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14072.2 1.141.20
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14072.7 0.1371.21
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 5020-14070.8 9.391.18
2,4-Dichlorophenol mg/Kg wet0.34 1.67 3030-130107 12.21.78
Diethylphthalate mg/Kg wet0.34 1.67 3040-140108 12.51.81
2,4-Dimethylphenol mg/Kg wet0.34 1.67 3030-13094.4 6.991.57
Dimethylphthalate mg/Kg wet0.34 1.67 3040-140106 15.21.77
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 3030-13078.0 13.81.30
2,4-Dinitrophenol mg/Kg wet0.66 1.67 3030-13041.8 11.50.696
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 30 V-0640-140121 14.52.01
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 30 V-0640-140120 13.01.99
Di-n-octylphthalate mg/Kg wet0.67 1.67 3040-140102 4.841.70
1,2-Diphenylhydrazine (as Azobenzene)mg/Kg wet0.34 1.67 3040-14088.9 6.361.48
Fluoranthene mg/Kg wet0.17 1.67 3040-140117 12.71.95
Fluorene mg/Kg wet0.17 1.67 3040-140110 14.71.84
Hexachlorobenzene mg/Kg wet0.34 1.67 3040-140117 14.81.95
Hexachlorobutadiene mg/Kg wet0.34 1.67 3040-14084.9 8.311.42
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 30 V-0540-14056.2 10.70.937
Hexachloroethane mg/Kg wet0.34 1.67 3040-14070.2 1.411.17
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 3040-140112 13.11.86
Isophorone mg/Kg wet0.34 1.67 3040-14089.1 6.111.49
1-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14092.0 11.51.53
2-Methylnaphthalene mg/Kg wet0.17 1.67 3040-140100 10.11.67
Page 88 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B110838 - SW-846 3546
LCS Dup (B110838-BSD1) Prepared: 12/02/14 Analyzed: 12/03/14
2-Methylphenol mg/Kg wet0.34 1.67 3030-13081.0 10.11.35
3/4-Methylphenol mg/Kg wet0.34 1.67 3030-13095.8 10.21.60
Naphthalene mg/Kg wet0.17 1.67 3040-14084.3 7.821.40
2-Nitroaniline mg/Kg wet0.34 1.67 3040-14098.9 7.101.65
3-Nitroaniline mg/Kg wet0.34 1.67 3030-14092.4 11.01.54
4-Nitroaniline mg/Kg wet0.34 1.67 3040-140113 12.61.88
Nitrobenzene mg/Kg wet0.34 1.67 3040-14076.6 3.791.28
2-Nitrophenol mg/Kg wet0.34 1.67 3030-13093.1 8.061.55
4-Nitrophenol mg/Kg wet0.66 1.67 5030-130118 8.821.96
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 3040-14061.6 6.921.03
N-Nitrosodiphenylamine mg/Kg wet0.34 1.67 3040-140127 13.22.12
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 3040-14075.2 6.361.25
Pentachloronitrobenzene mg/Kg wet0.34 1.67 30 V-1640-140125 13.52.08
Pentachlorophenol mg/Kg wet0.34 1.67 3030-13079.8 10.61.33
Phenanthrene mg/Kg wet0.17 1.67 3040-140109 13.31.82
Phenol mg/Kg wet0.34 1.67 3030-13089.4 7.161.49
Pyrene mg/Kg wet0.17 1.67 3040-140106 13.71.76
Pyridine mg/Kg wet0.34 1.67 3030-14045.8 5.660.763
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 3040-14097.2 13.01.62
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 3040-14087.8 9.471.46
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 3030-130108 14.91.80
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 3030-130107 16.51.79
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 82.45.49
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 89.05.93
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 78.42.61
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 1013.35
mg/Kg wet 6.67 S-0730-130Surrogate: 2,4,6-Tribromophenol 1369.06 *
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 1153.83
Page 89 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - EPH[TOC]
Batch B110844 - SW-846 3546
[TOC_3]B110844[TOC]
Blank (B110844-BLK1) Prepared: 12/02/14 Analyzed: 12/03/14
C9-C18 Aliphatics mg/Kg wet10ND
C19-C36 Aliphatics mg/Kg wet10ND
Unadjusted C11-C22 Aromatics mg/Kg wet10ND
C11-C22 Aromatics mg/Kg wet10ND
Acenaphthene mg/Kg wet0.10ND
Acenaphthylene mg/Kg wet0.10ND
Anthracene mg/Kg wet0.10ND
Benzo(a)anthracene mg/Kg wet0.10ND
Benzo(a)pyrene mg/Kg wet0.10ND
Benzo(b)fluoranthene mg/Kg wet0.10ND
Benzo(g,h,i)perylene mg/Kg wet0.10ND
Benzo(k)fluoranthene mg/Kg wet0.10ND
Chrysene mg/Kg wet0.10ND
Dibenz(a,h)anthracene mg/Kg wet0.10ND
Fluoranthene mg/Kg wet0.10ND
Fluorene mg/Kg wet0.10ND
Indeno(1,2,3-cd)pyrene mg/Kg wet0.10ND
2-Methylnaphthalene mg/Kg wet0.10ND
Naphthalene mg/Kg wet0.10ND
Phenanthrene mg/Kg wet0.10ND
Pyrene mg/Kg wet0.10ND
n-Decane mg/Kg wet0.10ND
n-Docosane mg/Kg wet0.10ND
n-Dodecane mg/Kg wet0.10ND
n-Eicosane mg/Kg wet0.10ND
n-Hexacosane mg/Kg wet0.10ND
n-Hexadecane mg/Kg wet0.10ND
n-Hexatriacontane mg/Kg wet0.10ND
n-Nonadecane mg/Kg wet0.10ND
n-Nonane mg/Kg wet0.10ND
n-Octacosane mg/Kg wet0.10ND
n-Octadecane mg/Kg wet0.10ND
n-Tetracosane mg/Kg wet0.10ND
n-Tetradecane mg/Kg wet0.10ND
n-Triacontane mg/Kg wet0.10ND
Naphthalene-aliphatic fraction mg/Kg wet0.10ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10ND
mg/Kg wet 5.00 40-140Surrogate: Chlorooctadecane (COD)82.24.11
mg/Kg wet 5.00 40-140Surrogate: o-Terphenyl (OTP)1055.23
mg/Kg wet 5.00 40-140Surrogate: 2-Bromonaphthalene 96.34.81
mg/Kg wet 5.00 40-140Surrogate: 2-Fluorobiphenyl 95.74.79
LCS (B110844-BS1) Prepared: 12/02/14 Analyzed: 12/03/14
Acenaphthene mg/Kg wet0.10 5.00 40-14092.64.63
Acenaphthylene mg/Kg wet0.10 5.00 40-14090.44.52
Anthracene mg/Kg wet0.10 5.00 40-1401055.27
Benzo(a)anthracene mg/Kg wet0.10 5.00 40-1401035.14
Benzo(a)pyrene mg/Kg wet0.10 5.00 40-14097.94.90
Benzo(b)fluoranthene mg/Kg wet0.10 5.00 40-14099.34.96
Benzo(g,h,i)perylene mg/Kg wet0.10 5.00 40-14092.74.64
Benzo(k)fluoranthene mg/Kg wet0.10 5.00 40-14097.24.86
Chrysene mg/Kg wet0.10 5.00 40-1401035.17
Page 90 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
Batch B110844 - SW-846 3546
LCS (B110844-BS1) Prepared: 12/02/14 Analyzed: 12/03/14
Dibenz(a,h)anthracene mg/Kg wet0.10 5.00 40-14090.14.50
Fluoranthene mg/Kg wet0.10 5.00 40-1401025.11
Fluorene mg/Kg wet0.10 5.00 40-14096.44.82
Indeno(1,2,3-cd)pyrene mg/Kg wet0.10 5.00 40-14076.23.81
2-Methylnaphthalene mg/Kg wet0.10 5.00 40-14088.44.42
Naphthalene mg/Kg wet0.10 5.00 40-14081.64.08
Phenanthrene mg/Kg wet0.10 5.00 40-14098.64.93
Pyrene mg/Kg wet0.10 5.00 40-1401035.14
n-Decane mg/Kg wet0.10 5.00 40-14067.53.38
n-Docosane mg/Kg wet0.10 5.00 40-1401045.20
n-Dodecane mg/Kg wet0.10 5.00 40-14078.23.91
n-Eicosane mg/Kg wet0.10 5.00 40-14099.74.99
n-Hexacosane mg/Kg wet0.10 5.00 40-1401025.12
n-Hexadecane mg/Kg wet0.10 5.00 40-1401015.03
n-Hexatriacontane mg/Kg wet0.10 5.00 40-1401025.08
n-Nonadecane mg/Kg wet0.10 5.00 40-1401045.20
n-Nonane mg/Kg wet0.10 5.00 30-14046.02.30
n-Octacosane mg/Kg wet0.10 5.00 40-14098.84.94
n-Octadecane mg/Kg wet0.10 5.00 40-1401035.15
n-Tetracosane mg/Kg wet0.10 5.00 40-1401015.07
n-Tetradecane mg/Kg wet0.10 5.00 40-14080.74.03
n-Triacontane mg/Kg wet0.10 5.00 40-1401015.04
Naphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
mg/Kg wet 5.00 40-140Surrogate: Chlorooctadecane (COD)98.24.91
mg/Kg wet 5.00 40-140Surrogate: o-Terphenyl (OTP)1175.84
mg/Kg wet 5.00 40-140Surrogate: 2-Bromonaphthalene 1025.11
mg/Kg wet 5.00 40-140Surrogate: 2-Fluorobiphenyl 1035.17
LCS Dup (B110844-BSD1) Prepared: 12/02/14 Analyzed: 12/03/14
Acenaphthene mg/Kg wet0.10 5.00 2540-14087.1 6.184.35
Acenaphthylene mg/Kg wet0.10 5.00 2540-14084.9 6.274.24
Anthracene mg/Kg wet0.10 5.00 2540-14098.8 6.564.94
Benzo(a)anthracene mg/Kg wet0.10 5.00 2540-14097.3 5.464.87
Benzo(a)pyrene mg/Kg wet0.10 5.00 2540-14093.4 4.714.67
Benzo(b)fluoranthene mg/Kg wet0.10 5.00 2540-14093.7 5.774.69
Benzo(g,h,i)perylene mg/Kg wet0.10 5.00 2540-14088.4 4.734.42
Benzo(k)fluoranthene mg/Kg wet0.10 5.00 2540-14092.6 4.834.63
Chrysene mg/Kg wet0.10 5.00 2540-14098.0 5.384.90
Dibenz(a,h)anthracene mg/Kg wet0.10 5.00 2540-14089.9 0.2164.49
Fluoranthene mg/Kg wet0.10 5.00 2540-14095.8 6.514.79
Fluorene mg/Kg wet0.10 5.00 2540-14090.8 5.984.54
Indeno(1,2,3-cd)pyrene mg/Kg wet0.10 5.00 2540-14073.8 3.313.69
2-Methylnaphthalene mg/Kg wet0.10 5.00 2540-14082.1 7.334.11
Naphthalene mg/Kg wet0.10 5.00 2540-14075.4 7.913.77
Phenanthrene mg/Kg wet0.10 5.00 2540-14092.5 6.434.62
Pyrene mg/Kg wet0.10 5.00 2540-14096.3 6.544.82
n-Decane mg/Kg wet0.10 5.00 2540-14059.8 12.12.99
n-Docosane mg/Kg wet0.10 5.00 2540-14097.9 6.024.89
n-Dodecane mg/Kg wet0.10 5.00 2540-14072.4 7.633.62
n-Eicosane mg/Kg wet0.10 5.00 2540-14094.1 5.784.71
n-Hexacosane mg/Kg wet0.10 5.00 2540-14097.2 5.254.86
Page 91 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - EPH - Quality Control
QUALITY CONTROL
Batch B110844 - SW-846 3546
LCS Dup (B110844-BSD1) Prepared: 12/02/14 Analyzed: 12/03/14
n-Hexadecane mg/Kg wet0.10 5.00 2540-14094.7 6.034.73
n-Hexatriacontane mg/Kg wet0.10 5.00 2540-14094.6 7.154.73
n-Nonadecane mg/Kg wet0.10 5.00 2540-14097.8 6.114.89
n-Nonane mg/Kg wet0.10 5.00 2530-14041.6 10.12.08
n-Octacosane mg/Kg wet0.10 5.00 2540-14093.2 5.824.66
n-Octadecane mg/Kg wet0.10 5.00 2540-14097.1 5.854.86
n-Tetracosane mg/Kg wet0.10 5.00 2540-14095.3 6.154.77
n-Tetradecane mg/Kg wet0.10 5.00 2540-14090.9 11.94.55
n-Triacontane mg/Kg wet0.10 5.00 2540-14095.2 5.714.76
Naphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
2-Methylnaphthalene-aliphatic fraction mg/Kg wet0.10 5.00 0-5ND
mg/Kg wet 5.00 40-140Surrogate: Chlorooctadecane (COD)90.34.52
mg/Kg wet 5.00 40-140Surrogate: o-Terphenyl (OTP)1065.29
mg/Kg wet 5.00 40-140Surrogate: 2-Bromonaphthalene 92.44.62
mg/Kg wet 5.00 40-140Surrogate: 2-Fluorobiphenyl 93.94.69
Page 92 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
[TOC_2]Petroleum Hydrocarbons Analyses - VPH[TOC]
Batch B111275 - MA VPH
[TOC_3]B111275[TOC]
Blank (B111275-BLK1) Prepared & Analyzed: 12/08/14
Unadjusted C5-C8 Aliphatics mg/Kg wet10ND
C5-C8 Aliphatics mg/Kg wet10ND
Unadjusted C9-C12 Aliphatics mg/Kg wet10ND
C9-C12 Aliphatics mg/Kg wet10ND
C9-C10 Aromatics mg/Kg wet10ND
Benzene mg/Kg wet0.050ND
Butylcyclohexane mg/Kg wet0.050ND
Decane mg/Kg wet0.050ND
Ethylbenzene mg/Kg wet0.050ND
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.050ND
2-Methylpentane mg/Kg wet0.050ND
Naphthalene mg/Kg wet0.50ND
Nonane mg/Kg wet0.050ND
Pentane mg/Kg wet0.050ND
Toluene mg/Kg wet0.050ND
1,2,4-Trimethylbenzene mg/Kg wet0.050ND
2,2,4-Trimethylpentane mg/Kg wet0.050ND
m+p Xylene mg/Kg wet0.10ND
o-Xylene mg/Kg wet0.050ND
mg/Kg wet 6.67 70-130Surrogate: 2,5-Dibromotoluene (FID)1067.09
mg/Kg wet 6.67 70-130Surrogate: 2,5-Dibromotoluene (PID)1157.68
LCS (B111275-BS1) Prepared & Analyzed: 12/08/14
Benzene mg/Kg wet0.0010 0.100 70-13087.90.0879
Butylcyclohexane mg/Kg wet0.0010 0.100 70-13081.50.0815
Decane mg/Kg wet0.0010 0.100 70-13093.70.0937
Ethylbenzene mg/Kg wet0.0010 0.100 70-13090.00.0900
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0010 0.100 70-13089.00.0890
2-Methylpentane mg/Kg wet0.0010 0.100 70-1301060.106
Naphthalene mg/Kg wet0.010 0.100 70-1301030.103
Nonane mg/Kg wet0.0010 0.100 30-13089.90.0899
Pentane mg/Kg wet0.0010 0.100 70-1301170.117
Toluene mg/Kg wet0.0010 0.100 70-13088.60.0886
1,2,4-Trimethylbenzene mg/Kg wet0.0010 0.100 70-13091.60.0916
2,2,4-Trimethylpentane mg/Kg wet0.0010 0.100 70-1301060.106
m+p Xylene mg/Kg wet0.0020 0.200 70-13090.60.181
o-Xylene mg/Kg wet0.0010 0.100 70-13089.80.0898
mg/Kg wet 0.0400 70-130Surrogate: 2,5-Dibromotoluene (FID)1270.0507
mg/Kg wet 0.0400 70-130Surrogate: 2,5-Dibromotoluene (PID)1210.0485
LCS Dup (B111275-BSD1) Prepared & Analyzed: 12/08/14
Benzene mg/Kg wet0.0010 0.100 2570-13086.5 1.650.0865
Butylcyclohexane mg/Kg wet0.0010 0.100 2570-13082.1 0.7640.0821
Decane mg/Kg wet0.0010 0.100 2570-13093.7 0.01920.0937
Ethylbenzene mg/Kg wet0.0010 0.100 2570-13088.7 1.520.0887
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0010 0.100 2570-13087.6 1.670.0876
2-Methylpentane mg/Kg wet0.0010 0.100 2570-130105 1.150.105
Naphthalene mg/Kg wet0.010 0.100 2570-130102 0.7680.102
Nonane mg/Kg wet0.0010 0.100 2530-13091.8 2.130.0918
Pentane mg/Kg wet0.0010 0.100 2570-130115 2.020.115
Toluene mg/Kg wet0.0010 0.100 2570-13087.0 1.740.0870
1,2,4-Trimethylbenzene mg/Kg wet0.0010 0.100 2570-13090.7 1.040.0907
Page 93 of 104 14L0056_2 Contest_Final 12 09 14 1752 12/09/14 17:53:11
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Petroleum Hydrocarbons Analyses - VPH - Quality Control
QUALITY CONTROL
Batch B111275 - MA VPH
LCS Dup (B111275-BSD1) Prepared & Analyzed: 12/08/14
2,2,4-Trimethylpentane mg/Kg wet0.0010 0.100 2570-130112 5.170.112
m+p Xylene mg/Kg wet0.0020 0.200 2570-13089.5 1.250.179
o-Xylene mg/Kg wet0.0010 0.100 2570-13088.5 1.540.0885
mg/Kg wet 0.0400 70-130Surrogate: 2,5-Dibromotoluene (FID)1080.0431
mg/Kg wet 0.0400 70-130Surrogate: 2,5-Dibromotoluene (PID)1130.0452
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FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits.
Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is
on the high side.
L-02
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD outside of control limits. Reduced precision anticipated for any reported result for
this compound.
L-07A
Soil/methanol ratio does not meet method specifications. Excess amount of soil. Sample was completely covered
with methanol, but with less than the method-specified amount.
O-01
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any
reported value for this compound.
R-05
One associated surrogate standard recovery is outside of control limits but the other(s) is/are within limits. All
recoveries are > 10%.
S-07
Surrogate recovery is outside of control limits. Data validation is not affected since all associated results are less
than the reporting limit and bias is on the high side.
S-17
Initial calibration did not meet method specifications. Compound was calibrated using a response factor where
%RSD is outside of method specified criteria.
V-04
Continuing calibration did not meet method specifications and was biased on the low side for this compound.
Increased uncertainty is associated with the reported value which is likely to be biased on the low side.
V-05
Continuing calibration did not meet method specifications and was biased on the high side for this compound.
Increased uncertainty is associated with the reported value which is likely to be biased on the high side.
V-06
Response factor is less than method specified minimum acceptable value. Reduced precision and accuracy may
be associated with reported result.
V-16
Continuing calibration did not meet method specifications and was biased on the high side. Data validation is not
affected since sample result was "not detected" for this compound.
V-20
[TOC_1]Flag/Qualifier Summary[TOC]
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
MADEP-EPH-04-1.1 in Soil
CT,NC,WA,ME,NH-PC9-C18 Aliphatics
CT,NC,WA,ME,NH-PC19-C36 Aliphatics
CT,NC,WA,ME,NH-PUnadjusted C11-C22 Aromatics
CT,NC,WA,ME,NH-PC11-C22 Aromatics
CT,NC,WA,ME,NH-PAcenaphthene
CT,NC,WA,ME,NH-PAcenaphthylene
CT,NC,WA,ME,NH-PAnthracene
CT,NC,WA,ME,NH-PBenzo(a)anthracene
CT,NC,WA,ME,NH-PBenzo(a)pyrene
CT,NC,WA,ME,NH-PBenzo(b)fluoranthene
CT,NC,WA,ME,NH-PBenzo(g,h,i)perylene
CT,NC,WA,ME,NH-PBenzo(k)fluoranthene
CT,NC,WA,ME,NH-PChrysene
CT,NC,WA,ME,NH-PDibenz(a,h)anthracene
CT,NC,WA,ME,NH-PFluoranthene
CT,NC,WA,MEFluorene
CT,NC,WA,ME,NH-PIndeno(1,2,3-cd)pyrene
CT,NC,WA,ME2-Methylnaphthalene
CT,NC,WA,ME,NH-PNaphthalene
CT,NC,WA,ME,NH-PPhenanthrene
CT,NC,WA,ME,NH-PPyrene
MADEP-VPH-04-1.1 in Soil
CT,NC,WA,ME,NH-PUnadjusted C5-C8 Aliphatics
CT,NC,WA,ME,NH-PC5-C8 Aliphatics
CT,NC,WA,ME,NH-PUnadjusted C9-C12 Aliphatics
CT,NC,WA,ME,NH-PC9-C12 Aliphatics
CT,NC,WA,ME,NH-PC9-C10 Aromatics
CT,NC,WA,ME,NH-PBenzene
CT,NC,WA,ME,NH-PEthylbenzene
CT,NC,WA,ME,NH-PMethyl tert-Butyl Ether (MTBE)
CT,NC,WA,ME,NH-PNaphthalene
CT,NC,WA,ME,NH-PToluene
CT,NC,WA,ME,NH-Pm+p Xylene
CT,NC,WA,ME,NH-Po-Xylene
SW-846 8260B in Soil
NCAcetone
NCAcrylonitrile
NCtert-Amyl Methyl Ether (TAME)
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCtert-Butyl Alcohol (TBA)
[TOC_1]Certifications[TOC]
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8260B in Soil
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCtert-Butyl Ethyl Ether (TBEE)
NCCarbon Disulfide
NCCarbon Tetrachloride
NCChlorobenzene
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromo-3-chloropropane (DBCP)
NC1,2-Dibromoethane (EDB)
NCDibromomethane
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCtrans-1,4-Dichloro-2-butene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiethyl Ether
NCDiisopropyl Ether (DIPE)
NC1,4-Dioxane
NCEthylbenzene
NCHexachlorobutadiene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
NC1,1,1,2-Tetrachloroethane
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8260B in Soil
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCTetrahydrofuran
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,3,5-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
SW-846 8270D in Soil
CT,NY,NH,ME,NC,VA,NJAcenaphthene
CT,NY,NH,ME,NC,VA,NJAcenaphthylene
NY,NH,ME,NC,VA,NJAcetophenone
NY,NH,ME,NC,VA,NJAniline
CT,NY,NH,ME,NC,VA,NJAnthracene
CT,NY,NH,ME,NC,VA,NJBenzidine
CT,NY,NH,ME,NC,VA,NJBenzo(a)anthracene
CT,NY,NH,ME,NC,VA,NJBenzo(a)pyrene
CT,NY,NH,ME,NC,VA,NJBenzo(b)fluoranthene
CT,NY,NH,ME,NC,VA,NJBenzo(g,h,i)perylene
CT,NY,NH,ME,NC,VA,NJBenzo(k)fluoranthene
NY,NH,ME,NC,VA,NJBenzoic Acid
CT,NY,NH,ME,NC,VA,NJBis(2-chloroethoxy)methane
CT,NY,NH,ME,NC,VA,NJBis(2-chloroethyl)ether
CT,NY,NH,ME,NC,VA,NJBis(2-chloroisopropyl)ether
CT,NY,NH,ME,NC,VA,NJBis(2-Ethylhexyl)phthalate
CT,NY,NH,ME,NC,VA,NJ4-Bromophenylphenylether
CT,NY,NH,ME,NC,VA,NJButylbenzylphthalate
NCCarbazole
CT,NY,NH,ME,NC,VA,NJ4-Chloroaniline
CT,NY,NH,ME,NC,VA,NJ4-Chloro-3-methylphenol
CT,NY,NH,NC,VA,NJ2-Chloronaphthalene
CT,NY,NH,ME,NC,VA,NJ2-Chlorophenol
CT,NY,NH,ME,NC,VA,NJ4-Chlorophenylphenylether
CT,NY,NH,ME,NC,VA,NJChrysene
CT,NY,NH,ME,NC,VA,NJDibenz(a,h)anthracene
CT,NY,NH,ME,NC,VA,NJDibenzofuran
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270D in Soil
CT,NY,NH,ME,NC,VA,NJDi-n-butylphthalate
NY,NH,ME,NC,VA,NJ1,2-Dichlorobenzene
NY,NH,ME,NC,VA,NJ1,3-Dichlorobenzene
NY,NH,ME,NC,VA,NJ1,4-Dichlorobenzene
CT,NY,NH,ME,NC,VA,NJ3,3-Dichlorobenzidine
CT,NY,NH,ME,NC,VA,NJ2,4-Dichlorophenol
CT,NY,NH,ME,NC,VA,NJDiethylphthalate
CT,NY,NH,ME,NC,VA,NJ2,4-Dimethylphenol
CT,NY,NH,ME,NC,VA,NJDimethylphthalate
CT,NY,NH,ME,NC,VA,NJ4,6-Dinitro-2-methylphenol
CT,NY,NH,ME,NC,VA,NJ2,4-Dinitrophenol
CT,NY,NH,ME,NC,VA,NJ2,4-Dinitrotoluene
CT,NY,NH,ME,NC,VA,NJ2,6-Dinitrotoluene
CT,NY,NH,ME,NC,VA,NJDi-n-octylphthalate
NY,NH,ME,NC,VA,NJ1,2-Diphenylhydrazine (as Azobenzene)
CT,NY,NH,ME,NC,VA,NJFluoranthene
NY,NH,ME,NC,VA,NJFluorene
CT,NY,NH,ME,NC,VA,NJHexachlorobenzene
CT,NY,NH,ME,NC,VA,NJHexachlorobutadiene
CT,NY,NH,ME,NC,VA,NJHexachlorocyclopentadiene
CT,NY,NH,ME,NC,VA,NJHexachloroethane
CT,NY,NH,ME,NC,VA,NJIndeno(1,2,3-cd)pyrene
CT,NY,NH,ME,NC,VA,NJIsophorone
NC1-Methylnaphthalene
CT,NY,NH,ME,NC,VA,NJ2-Methylnaphthalene
CT,NY,NH,ME,NC,VA,NJ2-Methylphenol
CT,NY,NH,ME,NC,VA,NJ3/4-Methylphenol
CT,NY,NH,ME,NC,VA,NJNaphthalene
CT,NY,NH,ME,NC,VA,NJ2-Nitroaniline
CT,NY,NH,ME,NC,VA,NJ3-Nitroaniline
CT,NY,NH,ME,NC,VA,NJ4-Nitroaniline
CT,NY,NH,ME,NC,VA,NJNitrobenzene
CT,NY,NH,ME,NC,VA,NJ2-Nitrophenol
CT,NY,NH,ME,NC,VA,NJ4-Nitrophenol
CT,NY,NH,ME,NC,VA,NJN-Nitrosodimethylamine
CT,NY,NH,ME,NC,VA,NJN-Nitrosodiphenylamine
CT,NY,NH,ME,NC,VA,NJN-Nitrosodi-n-propylamine
NCPentachloronitrobenzene
CT,NY,NH,ME,NC,VA,NJPentachlorophenol
CT,NY,NH,ME,NC,VA,NJPhenanthrene
CT,NY,NH,ME,NC,VA,NJPhenol
CT,NY,NH,ME,NC,VA,NJPyrene
CT,NY,NH,ME,NC,VA,NJPyridine
NC1,2,4,5-Tetrachlorobenzene
CT,NY,NH,ME,NC,VA,NJ1,2,4-Trichlorobenzene
CT,NY,NH,ME,NC,VA,NJ2,4,5-Trichlorophenol
CT,NY,NH,ME,NC,VA,NJ2,4,6-Trichlorophenol
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270D in Soil
NC2-Fluorophenol
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLCAIHA 02/1/2016
M-MA100Massachusetts DEPMA 06/30/2015
PH-0567Connecticut Department of Publilc HealthCT 09/30/2015
10899 NELAPNew York State Department of HealthNY 04/1/2015
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2015
LAO00112Rhode Island Department of HealthRI 12/30/2014
652North Carolina Div. of Water QualityNC 12/31/2014
MA007 NELAPNew Jersey DEPNJ 06/30/2015
E871027 NELAPFlorida Department of HealthFL 06/30/2015
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2015
C2065State of Washington Department of EcologyWA 02/23/2015
2011028State of MaineME 06/9/2015
460217Commonwealth of VirginiaVA 12/14/2014
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2015
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