RA-2071_12611_CA_MRP_20110630_Terraine GW Letter Rpt_unsigned

June 30, 2011

Mark Petermann, Hydrogeologist
Underground Storage Tank Section Division of Waste Management -- NCDENR
1637 Mail Service Center Raleigh, North Carolina 27699-1637

Reference: Ferrell Residence 5379 Wiggins Mill Road
Lucama, NC 27851 Wilson County
Incident # 12611
Subject: Groundwater Monitoring Results
Dear Mr. Petermann:
Terraine, Inc. (Terraine) has prepared this letter report to summarize the results of groundwater
monitoring activities at the Ferrell Residence site located at 5379 Wiggins Mill Road, Lucama, Wilson County, North Carolina.
On June 16, 2011, Terraine personnel mobilized to the site to collect groundwater samples from
monitoring wells MW-1, MW-3, and MW-5R. Groundwater elevation data are presented in Table 1. All groundwater samples were submitted under proper chain of custody control to Pace Analytical Laboratory
in Huntersville, North Carolina, for chemical analysis. Groundwater analytical data are summarized in Table 2. Tentatively identified compounds were detected in the groundwater samples collected from
monitoring wells MW-1, MW-3, and MW-5R. A complete laboratory report and chain of custody form for groundwater samples obtained are attached.
Immediately following sampling, a Universal Remediation, Inc., PRP® well boom was installed in
monitoring well MW-1. Well booms contain powdered beeswax, which stimulates rapid biodegradation of dissolved petroleum contaminants.
While on site, Terraine personnel observed that the house across the road (where monitoring well MW-3
is located) had been torn down. The house utilized water supply well WSW-2, which was also destroyed. Water supply well WSW-2 was the closest water supply well to the site.
Should you have any questions regarding any of this information, please contact me at 1-800-531-1242
ext. 706 or [e-mail].
Sincerely,

Karen Baer Project Manager
Terraine, Inc.
Groundwater Monitoring Results – 6/30/2011 Incident # 12611
Ferrell Residence Page 2
Lucama, NC Wilson County
Attachments: Table 1: Summary of Groundwater Elevation Data
Table 2: Summary of Groundwater Analytical Results
Site Photographs
Laboratory Report(s)
08/31/2010 11.01 83.02
12/21/2010 9.02 85.01
06/16/2011 8.82 85.21
08/31/2010 10.53 83.30
12/21/2010 8.36 85.47
06/16/2011 7.89 84.94
08/31/2010 9.97 83.52
12/21/2010 6.50 86.99
06/16/2011 6.25 87.24
Unknown 2 20
MW-5R 12/14/2009 93.49 15-25 2 25
Units measured in feet unless otherwise noted.
Groundwater elevation measurements based on an unknown benchmark.
GW - Groundwater
TOC - Top of Casing
MW-1 10/26/2009 94.03 Unknown 2 30
MW-3 10/26/2009 93.83
NCDENR Incident No. 12611
WELL ID INSTALL DATE TOC
ELEVATION
SCREEN
INTERVAL
WELL
DIAMETER
(INCHES)
TOTAL
DEPTH
WELL GAUGE
DATE
DEPTH TO
WATER FROM
TOC
GW
ELEVATION
Table 1
Summary of Groundwater Elevation Data
Ferrell Residence
5379 Wiggins Mill Road
Lucama, NC
Wilson County
Table 2
Summary of Groundwater Analytical Results
Ferrell Residence
5379 Wiggins Mill Road
Lucama, North Carolina
Wilson County
Incident No. 12611
Page 1 of 2
7/9/2003 140 400 220 890 6.2 ND NR 97 NR ND 4.4 ND NR NR ND NR NR 23 ND 4.4 77 17 15 NR NR NR NR NR NR NR NR NR
1/13/2004 260 560 480 1,880 19 3.3 NR 160 NR 28 9.1 ND NR NR ND NR NR 48 ND 10 340 59 29 NR NR NR NR NR NR NR NR NR
6/9/2004 440 2,000 850 5,500 ND ND NR 230 NR 130 8.5 ND NR NR ND NR NR 96 ND 8.3 730 290 45 NR NR NR NR NR NR NR NR NR
2/23/2005 760 3,500 1,500 9,600 ND ND NR 450 NR 230 ND ND NR NR ND NR NR 140 ND ND 1,800 ND 60 NR NR NR NR NR NR NR NR NR
5/24/2006 180 470 320 1,200 ND ND NR 110 NR ND ND ND NR NR ND NR NR 37 ND ND 310 110 21 NR NR NR NR NR NR NR NR NR
11/6/2006 240 520 240 860 ND ND NR 150 NR ND ND ND NR NR ND NR NR 40 ND ND 180 81 23 NR NR NR NR NR NR NR NR NR
5/22/2007 310 740 360 1,580 ND ND NR 130 NR ND ND ND NR NR ND NR NR 48 8 ND 300 110 25 NR NR NR NR NR NR NR NR NR
11/1/2007 95.8 125 114 213.9 ND ND NR 56.5 NR ND ND ND NR NR ND NR NR 18.6 1.7 ND 69.2 29.6 11.4 NR NR NR NR NR NR NR NR NR
2/19/2008 518 1,710 643 2,871 ND ND NR 222 NR ND ND ND NR NR ND NR NR 75.6 ND ND 549 191 192 NR NR NR NR NR NR NR NR NR
3/8/2008 439 1,910 806 3,540 0.85 ND NR 237 NR ND ND ND NR NR ND NR NR 118 ND ND 779 289 56.7 NR NR NR NR NR NR NR NR NR
11/19/2008 691 5,300 2,120 12,530 ND ND NR 881 NR ND ND ND NR NR ND NR NR 148 53 ND 2,610 855 72.4 NR NR NR NR NR NR NR NR NR
8/31/2010 106 450 519 2,010 ND ND ND 250 13.6 ND ND ND ND ND ND ND 16.7 72.8 7.5 ND 554 192 38.9 2,820 13,400 167 13,567 ND 1,840 228 2,068 15.9
12/21/2010 165 747 489 1,994 ND ND ND*193*25.8 ND ND ND ND ND ND ND ND 51.1 ND ND 394 146 26.1 ND*9,440 ND 9,440 ND ND 241 241 21.2
6/16/2011 181 987 636 2,407 ND ND ND*218*27.7 ND ND ND ND*ND*ND*ND ND*84.6 ND ND 599 215 38.1 4,840 16,700 ND 16,700 ND 2,100 373 2,473 12.9
7/9/2003 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
1/13/2004 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
6/9/2004 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
2/23/2005 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
5/24/2006 1.4 ND ND ND ND ND NR 10 NR ND 4.9 1.9 NR NR ND NR NR 1.1 NR ND ND ND 5.0 NR NR NR NR NR NR NR NR NR
11/6/2006 1.5 ND ND ND ND ND NR 5.8 NR ND 2.6 1.4 NR NR ND NR NR ND NR ND ND ND 3.5 NR NR NR NR NR NR NR NR NR
5/22/2007 0.55 ND ND ND ND ND NR 0.73 J NR ND 1.5 0.88 NR NR ND NR NR ND NR ND ND ND 1.4 NR NR NR NR NR NR NR NR NR
11/1/2007 ND ND ND ND ND ND NR ND NR ND 0.5 ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
2/19/2008 ND ND 0.50 ND ND ND NR ND NR ND 2.7 1.4 NR NR ND NR NR 0.55 NR ND ND ND ND NR NR NR NR NR NR NR NR NR
3/8/2008 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
11/18/2008 ND ND ND ND ND ND NR 3.7 NR ND 1.5 0.94 NR NR ND NR NR 2.7 NR 0.94 ND ND 1.3 NR NR NR NR NR NR NR NR NR
8/31/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 0.82 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 8.2
12/21/2010 ND ND ND ND ND ND ND*ND ND ND ND ND ND ND ND 0.51 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 12.9
6/16/2011 0.61 ND ND ND ND ND ND*ND ND ND 1.6 0.92 ND ND*ND ND ND ND ND ND ND ND 0.94 118 204 ND 204 ND 44.3 J ND 44.3 J 4.2 J
1 600 600 500 20 70 0.02 6 30 70 70 70 0.6 0.4 3 70 5 70 70 NE 400 400 70 400 NE NE 700 10,000 NE NE 200 15
Gross Contamination Level (GCL)5,000 260,000 84,500 85,500 20,000 70,000 50 6,000 12,500 6,900 8,500 15,000 NE 400 3,000 70,000 5,000 30,000 70,000 NE 28,500 25,000 25,000 NE NE NE NE NE NE NE NE 15,000
MW-1
MW-3
NDND
15A NCAC 2L.0202 Standard
ND ND ND NDND1.1 ND ND ND ND ND 0.56 ND 10.1ND
1,120 155 1,275Total C9-C18 Aliphatics7,171
ND ND
7,020 151.0 LeadC9-C12 AliphaticsC9-C18 AliphaticsC9-C10 AromaticsC11-C22 AromaticsTotal C9-C22 AromaticsMADEP VPH & EPH
ND ND NDNDND 1,3,5-TrimethylbenzeneXylenesEthylbenzeneTolueneBenzeneIsopropylbenzeneNaphthalenen-ButylbenzeneNDND
Sample DateWell ID
MTBE129NDNDEDBIPEp-Isopropyltoluene348Methylene Chloride1,2,4-Trimethylbenzene2-MethylnaphthaleneNDND185*ND 55.8 NDn-PropylbenzeneBromodichloromethaneChloroformDibromochloromethaneChloromethaneND sec-Butylbenzenetert-Butylbenzene9/10/2009 185 543 414 1,242 ND ND ND 4,140 C19-C36 AliphaticsC5-C8 AliphaticsND 26.9Styrene6.4ND 30.4
0.60 ND9/10/2009 ND ND ND ND NDND
Table 2
Summary of Groundwater Analytical Results
Ferrell Residence
5379 Wiggins Mill Road
Lucama, North Carolina
Wilson County
Incident No. 12611
Page 2 of 2
Total C9-C18 AliphaticsLeadC9-C12 AliphaticsC9-C18 AliphaticsC9-C10 AromaticsC11-C22 AromaticsTotal C9-C22 AromaticsMADEP VPH & EPH
1,3,5-TrimethylbenzeneXylenesEthylbenzeneTolueneBenzeneIsopropylbenzeneNaphthalenen-ButylbenzeneSample DateWell ID
MTBEEDBIPEp-IsopropyltolueneMethylene Chloride1,2,4-Trimethylbenzene2-Methylnaphthalenen-PropylbenzeneBromodichloromethaneChloroformDibromochloromethaneChloromethanesec-Butylbenzenetert-ButylbenzeneC19-C36 AliphaticsC5-C8 AliphaticsStyrene7/9/2003 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
1/13/2004 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
6/9/2004 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
2/23/2005 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
5/24/2006 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
11/6/2006 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
5/22/2007 ND ND ND ND ND ND NR ND NR ND ND ND NR NR 0.27 J NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
11/1/2007 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
2/19/2008 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
3/8/2008 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
11/18/2008 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
8/31/2010 ND ND ND ND ND ND ND ND 144 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
12/21/2010 ND ND ND ND ND ND ND*ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 25.8
6/16/2011 ND ND ND ND ND ND ND*ND ND ND ND ND ND ND*ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 20.5
6/9/2004 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
2/19/2008 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
11/18/2008 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
8/31/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
6/9/2004 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
2/19/2008 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
11/18/2008 ND ND ND ND ND ND NR ND NR ND ND ND NR NR ND NR NR ND NR ND ND ND ND NR NR NR NR NR NR NR NR NR
8/31/2010 ND ND ND ND ND ND ND ND ND ND ND ND 1.3 1.4 ND 1.3 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND
1 600 600 500 20 70 0.02 6 30 70 70 70 0.6 0.4 3 70 5 70 70 NE 400 400 70 400 NE NE 700 10,000 NE NE 200 15
Gross Contamination Level (GCL)5,000 260,000 84,500 85,500 20,000 70,000 50 6,000 12,500 6,900 8,500 15,000 NE 400 3,000 70,000 5,000 30,000 70,000 NE 28,500 25,000 25,000 NE NE NE NE NE NE NE NE 15,000
All results expressed in parts per billion (µg/L)Highlighted data shown in bold, italicized font indicate concentrations that meet or exceed the 2L Standards.* By analytical method SM 6200B VPH - Volatile Petroleum Hydrocarbons
ND - None Detected (below method detection limits)EDB - 1,2,-Dibromoethane ND* - None Detected (method detection limit above the 2L Standard)EPH - Extractable Petroleum Hydrocarbons
NE - No Standard Established J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit IPE - Diisopropyl ether
MTBE - Methyl tert-butyl ether MADEP - Massachusetts Department of Environmental Protection NR - Not reported in historical data tables
ND
12/21/2010 Not Sampled
WSW-2
12/21/2010 Not Sampled
WSW-3
ND
ND
ND ND
ND ND
MW-5R
ND
ND ND ND
ND
ND ND
ND
ND
ND
ND 93.4
ND
ND
Could Not Locate
ND
ND
ND
ND ND ND
ND ND ND
1.11.5
ND
ND
ND
NDND
ND
ND
NDNDNDNDNDNDNDND1.5 NDNDNDND9/10/2009 ND ND ND ND ND
ND
ND
ND ND
ND ND
ND
ND
ND
NDNDND
ND ND ND ND ND NDND
NDMW-5 9/10/2009 ND ND ND
ND9/10/2009 ND ND ND
ND ND ND ND ND
15A NCAC 2L.0202 Standard
ND
9/10/2009
ND
MW-4
ND
ND ND
ND ND
Site Photographs
Ferrell Residence
5379 Wiggins Mill Road
Lucama, NC
Wilson County
NCDENR Incident # 12611
View of the former store, facing south.1 of 3
View of the former on-site residence. The building and associated
water supply well (WSW-2) have been destroyed.
2 of 3
Site Photographs
Ferrell Residence
5379 Wiggins Mill Road
Lucama, NC
Wilson County
NCDENR Incident # 12611
Photo from December 2010, showing the previous location of water
supply well WSW-2.
3 of 3
June 28, 2011
LIMS USE: FR - LINDA BLALOCK
LIMS OBJECT ID: 9296540
9296540
Project:
Pace Project No.:
RE:
Ms. Linda BlalockNCDENR - UST Section1637 Mail Service CenterRaleigh, NC 276991637
12611 FERRELL RESIDENCE
Dear Ms. Blalock:
Enclosed are the analytical results for sample(s) received by the laboratory on June 17, 2011. The
results relate only to the samples included in this report. Results reported herein conform to themost current TNI standards, where applicable, unless otherwise narrated in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analytepage for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Renee Spencer
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078Louisiana/LELAP Certification #: 04034New Jersey Certification #: NC012North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12Pennsylvania Certification #: 68-00784South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003Virginia Certification #: 00213Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84Louisiana DHH Drinking Water # LA 100031West Virginia Certification #: 357
Asheville Certification IDs2225 Riverside Dr., Asheville, NC 28804Connecticut Certification #: PH-0106Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030New Jersey Certification #: NC011North Carolina Bioassay Certification #: 9North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40Pennsylvania Certification #: 68-03578South Carolina Bioassay Certification #: 99030002South Carolina Certification #: 99030001Virginia Certification #: 00072West Virginia Certification #: 356
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE SUMMARY
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Lab ID Sample ID Matrix Date Collected Date Received
9296540001 MW-1 Water 06/16/11 09:50 06/17/11 13:30
9296540002 MW-3 Water 06/16/11 09:15 06/17/11 13:30
9296540003 MW-5R Water 06/16/11 10:15 06/17/11 13:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
9296540001 MW-1 MADEP EPH 7 PASI-CRES
MADEP VPH 5 PASI-CKJM
EPA 200.7 1 PASI-AJMW
EPA 625 59 PASI-CPPM
SM 6200B 64 PASI-CAW
9296540002 MW-3 MADEP EPH 7 PASI-CRES
MADEP VPH 5 PASI-CKJM
EPA 200.7 1 PASI-AJMW
EPA 625 59 PASI-CPPM
SM 6200B 64 PASI-CAW
9296540003 MW-5R MADEP EPH 7 PASI-CRES
MADEP VPH 5 PASI-CKJM
EPA 200.7 1 PASI-AJMW
EPA 625 59 PASI-CPPM
SM 6200B 64 PASI-CAW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Sample:MW-1 Lab ID:9296540001 Collected:06/16/11 09:50 Received:06/17/11 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 06/24/11 19:30 N206/21/11 19:00100100
Aliphatic (C19-C36)ND ug/L 1 06/24/11 19:30 N206/21/11 19:00100100
Aromatic (C11-C22)373 ug/L 1 06/24/11 19:30 N206/21/11 19:00100100
Nonatriacontane (S)79 %1 06/24/11 19:30 7194-86-706/21/11 19:0040-140
o-Terphenyl (S)95 %1 06/24/11 19:30 84-15-106/21/11 19:0040-140
2-Fluorobiphenyl (S)123 %1 06/24/11 19:30 321-60-806/21/11 19:0040-140
2-Bromonaphthalene (S)139 %1 06/24/11 19:30 580-13-206/21/11 19:0040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)4840 ug/L 10 06/24/11 01:36 N2500150
Aliphatic (C09-C12)16700 ug/L 10 06/24/11 01:36 N2,NC500150
Aromatic (C09-C10)2100 ug/L 10 06/24/11 01:36 N2500150
2,5-Dibromotoluene (PID)(S)112 %10 06/24/11 01:3670-130
2,5-Dibromotoluene (FID)(S)116 %10 06/24/11 01:3670-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead 12.9 ug/L 1 06/22/11 17:44 7439-92-106/18/11 13:305.0 4.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 06/23/11 06:28 83-32-906/21/11 18:005.0 0.25
Acenaphthylene ND ug/L 1 06/23/11 06:28 208-96-806/21/11 18:005.0 0.21
Anthracene ND ug/L 1 06/23/11 06:28 120-12-706/21/11 18:005.0 0.14
Benzo(a)anthracene ND ug/L 1 06/23/11 06:28 56-55-306/21/11 18:005.0 0.33
Benzo(a)pyrene ND ug/L 1 06/23/11 06:28 50-32-806/21/11 18:005.0 0.30
Benzo(b)fluoranthene ND ug/L 1 06/23/11 06:28 205-99-206/21/11 18:005.0 0.28
Benzo(g,h,i)perylene ND ug/L 1 06/23/11 06:28 191-24-206/21/11 18:005.0 0.38
Benzo(k)fluoranthene ND ug/L 1 06/23/11 06:28 207-08-906/21/11 18:005.0 0.43
4-Bromophenylphenyl ether ND ug/L 1 06/23/11 06:28 101-55-306/21/11 18:005.0 0.82
Butylbenzylphthalate ND ug/L 1 06/23/11 06:28 85-68-706/21/11 18:005.0 0.79
4-Chloro-3-methylphenol ND ug/L 1 06/23/11 06:28 59-50-706/21/11 18:005.0 3.7
bis(2-Chloroethoxy)methane ND ug/L 1 06/23/11 06:28 111-91-106/21/11 18:0010.0 0.92
bis(2-Chloroethyl) ether ND ug/L 1 06/23/11 06:28 111-44-406/21/11 18:005.0 1.0
bis(2-Chloroisopropyl) ether ND ug/L 1 06/23/11 06:28 108-60-106/21/11 18:005.0 0.95
2-Chloronaphthalene ND ug/L 1 06/23/11 06:28 91-58-706/21/11 18:005.0 0.98
2-Chlorophenol ND ug/L 1 06/23/11 06:28 95-57-806/21/11 18:005.0 1.3
4-Chlorophenylphenyl ether ND ug/L 1 06/23/11 06:28 7005-72-306/21/11 18:005.0 0.87
Chrysene ND ug/L 1 06/23/11 06:28 218-01-906/21/11 18:005.0 0.21
Dibenz(a,h)anthracene ND ug/L 1 06/23/11 06:28 53-70-306/21/11 18:005.0 0.55
3,3'-Dichlorobenzidine ND ug/L 1 06/23/11 06:28 91-94-106/21/11 18:0025.0 2.1
2,4-Dichlorophenol ND ug/L 1 06/23/11 06:28 120-83-206/21/11 18:005.0 1.7
Diethylphthalate ND ug/L 1 06/23/11 06:28 84-66-206/21/11 18:005.0 0.58
2,4-Dimethylphenol ND ug/L 1 06/23/11 06:28 105-67-906/21/11 18:0010.0 1.2
Dimethylphthalate ND ug/L 1 06/23/11 06:28 131-11-306/21/11 18:005.0 0.76
Di-n-butylphthalate ND ug/L 1 06/23/11 06:28 84-74-206/21/11 18:005.0 0.75
4,6-Dinitro-2-methylphenol ND ug/L 1 06/23/11 06:28 534-52-106/21/11 18:0020.0 2.6
2,4-Dinitrophenol ND ug/L 1 06/23/11 06:28 51-28-506/21/11 18:0050.0 9.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 5 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Sample:MW-1 Lab ID:9296540001 Collected:06/16/11 09:50 Received:06/17/11 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
2,4-Dinitrotoluene ND ug/L 1 06/23/11 06:28 121-14-206/21/11 18:005.0 0.90
2,6-Dinitrotoluene ND ug/L 1 06/23/11 06:28 606-20-206/21/11 18:005.0 0.98
Di-n-octylphthalate ND ug/L 1 06/23/11 06:28 117-84-006/21/11 18:005.0 0.66
bis(2-Ethylhexyl)phthalate ND ug/L 1 06/23/11 06:28 117-81-706/21/11 18:005.0 0.79
Fluoranthene ND ug/L 1 06/23/11 06:28 206-44-006/21/11 18:005.0 0.21
Fluorene ND ug/L 1 06/23/11 06:28 86-73-706/21/11 18:005.0 0.21
Hexachloro-1,3-butadiene ND ug/L 1 06/23/11 06:28 87-68-306/21/11 18:005.0 0.94
Hexachlorobenzene ND ug/L 1 06/23/11 06:28 118-74-106/21/11 18:005.0 0.72
Hexachlorocyclopentadiene ND ug/L 1 06/23/11 06:28 77-47-406/21/11 18:0010.0 0.88
Hexachloroethane ND ug/L 1 06/23/11 06:28 67-72-106/21/11 18:005.0 1.1
Indeno(1,2,3-cd)pyrene ND ug/L 1 06/23/11 06:28 193-39-506/21/11 18:005.0 0.29
Isophorone ND ug/L 1 06/23/11 06:28 78-59-106/21/11 18:0010.0 0.89
2-Methylnaphthalene 27.7 ug/L 1 06/23/11 06:28 91-57-606/21/11 18:005.0 0.28
Naphthalene 149 ug/L 5 06/23/11 09:39 91-20-306/21/11 18:0025.0 1.7
Nitrobenzene ND ug/L 1 06/23/11 06:28 98-95-306/21/11 18:005.0 1.1
2-Nitrophenol ND ug/L 1 06/23/11 06:28 88-75-506/21/11 18:005.0 0.91
4-Nitrophenol ND ug/L 1 06/23/11 06:28 100-02-706/21/11 18:0050.0 4.1
N-Nitrosodimethylamine ND ug/L 1 06/23/11 06:28 62-75-906/21/11 18:005.0 0.91
N-Nitroso-di-n-propylamine ND ug/L 1 06/23/11 06:28 621-64-706/21/11 18:005.0 0.99
N-Nitrosodiphenylamine ND ug/L 1 06/23/11 06:28 86-30-606/21/11 18:0010.0 1.0
Pentachlorophenol ND ug/L 1 06/23/11 06:28 87-86-506/21/11 18:0025.0 4.6
Phenanthrene ND ug/L 1 06/23/11 06:28 85-01-806/21/11 18:005.0 0.22
Phenol ND ug/L 1 06/23/11 06:28 108-95-206/21/11 18:005.0 1.9
Pyrene ND ug/L 1 06/23/11 06:28 129-00-006/21/11 18:005.0 0.19
1,2,4-Trichlorobenzene ND ug/L 1 06/23/11 06:28 120-82-106/21/11 18:005.0 0.98
2,4,6-Trichlorophenol ND ug/L 1 06/23/11 06:28 88-06-206/21/11 18:0010.0 1.3
Nitrobenzene-d5 (S)73 %1 06/23/11 06:28 4165-60-006/21/11 18:0010-120
2-Fluorobiphenyl (S)71 %1 06/23/11 06:28 321-60-806/21/11 18:0015-120
Terphenyl-d14 (S)69 %1 06/23/11 06:28 1718-51-006/21/11 18:0011-131
Phenol-d6 (S)29 %1 06/23/11 06:28 13127-88-306/21/11 18:0010-120
2-Fluorophenol (S)44 %1 06/23/11 06:28 367-12-406/21/11 18:0010-120
2,4,6-Tribromophenol (S)120 %1 06/23/11 06:28 118-79-606/21/11 18:0010-137
6200B MSV Analytical Method: SM 6200B
Benzene 181 ug/L 5 06/24/11 09:58 71-43-22.5 2.5
Bromobenzene ND ug/L 5 06/24/11 09:58 108-86-12.5 2.5
Bromochloromethane ND ug/L 5 06/24/11 09:58 74-97-52.5 2.5
Bromodichloromethane ND ug/L 5 06/24/11 09:58 75-27-42.5 2.5
Bromoform ND ug/L 5 06/24/11 09:58 75-25-22.5 2.5
Bromomethane ND ug/L 5 06/24/11 09:58 74-83-925.0 5.0
n-Butylbenzene ND ug/L 5 06/24/11 09:58 104-51-82.5 2.5
sec-Butylbenzene ND ug/L 5 06/24/11 09:58 135-98-82.5 2.5
tert-Butylbenzene ND ug/L 5 06/24/11 09:58 98-06-62.5 2.5
Carbon tetrachloride ND ug/L 5 06/24/11 09:58 56-23-52.5 2.5
Chlorobenzene ND ug/L 5 06/24/11 09:58 108-90-72.5 2.5
Chloroethane ND ug/L 5 06/24/11 09:58 75-00-35.0 5.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 6 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Sample:MW-1 Lab ID:9296540001 Collected:06/16/11 09:50 Received:06/17/11 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Chloroform ND ug/L 5 06/24/11 09:58 67-66-32.5 2.5
Chloromethane ND ug/L 5 06/24/11 09:58 74-87-35.0 5.0
2-Chlorotoluene ND ug/L 5 06/24/11 09:58 95-49-82.5 2.5
4-Chlorotoluene ND ug/L 5 06/24/11 09:58 106-43-42.5 2.5
1,2-Dibromo-3-chloropropane ND ug/L 5 06/24/11 09:58 96-12-85.0 5.0
Dibromochloromethane ND ug/L 5 06/24/11 09:58 124-48-12.5 2.5
1,2-Dibromoethane (EDB)ND ug/L 5 06/24/11 09:58 106-93-42.5 2.5
Dibromomethane ND ug/L 5 06/24/11 09:58 74-95-32.5 2.5
1,2-Dichlorobenzene ND ug/L 5 06/24/11 09:58 95-50-12.5 2.5
1,3-Dichlorobenzene ND ug/L 5 06/24/11 09:58 541-73-12.5 2.5
1,4-Dichlorobenzene ND ug/L 5 06/24/11 09:58 106-46-72.5 2.5
Dichlorodifluoromethane ND ug/L 5 06/24/11 09:58 75-71-82.5 2.5
1,1-Dichloroethane ND ug/L 5 06/24/11 09:58 75-34-32.5 2.5
1,2-Dichloroethane ND ug/L 5 06/24/11 09:58 107-06-22.5 2.5
1,1-Dichloroethene ND ug/L 5 06/24/11 09:58 75-35-42.5 2.5
cis-1,2-Dichloroethene ND ug/L 5 06/24/11 09:58 156-59-22.5 2.5
trans-1,2-Dichloroethene ND ug/L 5 06/24/11 09:58 156-60-52.5 2.5
1,2-Dichloropropane ND ug/L 5 06/24/11 09:58 78-87-52.5 2.5
1,3-Dichloropropane ND ug/L 5 06/24/11 09:58 142-28-92.5 2.5
2,2-Dichloropropane ND ug/L 5 06/24/11 09:58 594-20-72.5 2.5
1,1-Dichloropropene ND ug/L 5 06/24/11 09:58 563-58-62.5 2.5
cis-1,3-Dichloropropene ND ug/L 5 06/24/11 09:58 10061-01-52.5 2.5
trans-1,3-Dichloropropene ND ug/L 5 06/24/11 09:58 10061-02-62.5 2.5
Diisopropyl ether ND ug/L 5 06/24/11 09:58 108-20-32.5 2.5
Ethylbenzene 636 ug/L 5 06/24/11 09:58 100-41-42.5 2.5
Hexachloro-1,3-butadiene ND ug/L 5 06/24/11 09:58 87-68-310.0 10.0
Isopropylbenzene (Cumene)38.1 ug/L 5 06/24/11 09:58 98-82-82.5 2.5
Methylene Chloride ND ug/L 5 06/24/11 09:58 75-09-210.0 10.0
Methyl-tert-butyl ether ND ug/L 5 06/24/11 09:58 1634-04-42.5 2.5
Naphthalene 218 ug/L 5 06/24/11 09:58 91-20-310.0 10.0
n-Propylbenzene 84.6 ug/L 5 06/24/11 09:58 103-65-12.5 2.5
Styrene ND ug/L 5 06/24/11 09:58 100-42-52.5 2.5
1,1,1,2-Tetrachloroethane ND ug/L 5 06/24/11 09:58 630-20-62.5 2.5
1,1,2,2-Tetrachloroethane ND ug/L 5 06/24/11 09:58 79-34-52.5 2.5
Tetrachloroethene ND ug/L 5 06/24/11 09:58 127-18-42.5 2.5
Toluene 987 ug/L 5 06/24/11 09:58 108-88-32.5 2.5
1,2,3-Trichlorobenzene ND ug/L 5 06/24/11 09:58 87-61-610.0 10.0
1,2,4-Trichlorobenzene ND ug/L 5 06/24/11 09:58 120-82-110.0 10.0
1,1,1-Trichloroethane ND ug/L 5 06/24/11 09:58 71-55-62.5 2.5
1,1,2-Trichloroethane ND ug/L 5 06/24/11 09:58 79-00-52.5 2.5
Trichloroethene ND ug/L 5 06/24/11 09:58 79-01-62.5 2.5
Trichlorofluoromethane ND ug/L 5 06/24/11 09:58 75-69-45.0 5.0
1,2,3-Trichloropropane ND ug/L 5 06/24/11 09:58 96-18-42.5 2.5
1,2,4-Trimethylbenzene 599 ug/L 5 06/24/11 09:58 95-63-62.5 2.5
1,3,5-Trimethylbenzene 215 ug/L 5 06/24/11 09:58 108-67-82.5 2.5
Vinyl chloride ND ug/L 5 06/24/11 09:58 75-01-45.0 5.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 7 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Sample:MW-1 Lab ID:9296540001 Collected:06/16/11 09:50 Received:06/17/11 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
m&p-Xylene 1640 ug/L 5 06/24/11 09:58 179601-23-15.0 5.0
o-Xylene 767 ug/L 5 06/24/11 09:58 95-47-62.5 2.5
1,2-Dichloroethane-d4 (S)123 %5 06/24/11 09:58 17060-07-070-130
Dibromofluoromethane (S)112 %5 06/24/11 09:58 1868-53-770-130
4-Bromofluorobenzene (S)93 %5 06/24/11 09:58 460-00-470-130
Toluene-d8 (S)101 %5 06/24/11 09:58 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 8 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Sample:MW-3 Lab ID:9296540002 Collected:06/16/11 09:15 Received:06/17/11 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 06/24/11 20:06 N206/21/11 19:00100100
Aliphatic (C19-C36)ND ug/L 1 06/24/11 20:06 N206/21/11 19:00100100
Aromatic (C11-C22)ND ug/L 1 06/24/11 20:06 N206/21/11 19:00100100
Nonatriacontane (S)85 %1 06/24/11 20:06 7194-86-706/21/11 19:0040-140
o-Terphenyl (S)79 %1 06/24/11 20:06 84-15-106/21/11 19:0040-140
2-Fluorobiphenyl (S)107 %1 06/24/11 20:06 321-60-806/21/11 19:0040-140
2-Bromonaphthalene (S)114 %1 06/24/11 20:06 580-13-206/21/11 19:0040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)118 ug/L 1 06/23/11 23:07 N250.0 15.0
Aliphatic (C09-C12)204 ug/L 1 06/23/11 23:07 N250.0 15.0
Aromatic (C09-C10)44.3J ug/L 1 06/23/11 23:07 N250.0 15.0
2,5-Dibromotoluene (PID)(S)122 %1 06/23/11 23:0770-130
2,5-Dibromotoluene (FID)(S)120 %1 06/23/11 23:0770-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead 4.2J ug/L 1 06/22/11 17:38 7439-92-106/18/11 13:305.0 4.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 06/23/11 06:55 83-32-906/21/11 18:005.0 0.25
Acenaphthylene ND ug/L 1 06/23/11 06:55 208-96-806/21/11 18:005.0 0.21
Anthracene ND ug/L 1 06/23/11 06:55 120-12-706/21/11 18:005.0 0.14
Benzo(a)anthracene ND ug/L 1 06/23/11 06:55 56-55-306/21/11 18:005.0 0.33
Benzo(a)pyrene ND ug/L 1 06/23/11 06:55 50-32-806/21/11 18:005.0 0.30
Benzo(b)fluoranthene ND ug/L 1 06/23/11 06:55 205-99-206/21/11 18:005.0 0.28
Benzo(g,h,i)perylene ND ug/L 1 06/23/11 06:55 191-24-206/21/11 18:005.0 0.38
Benzo(k)fluoranthene ND ug/L 1 06/23/11 06:55 207-08-906/21/11 18:005.0 0.43
4-Bromophenylphenyl ether ND ug/L 1 06/23/11 06:55 101-55-306/21/11 18:005.0 0.82
Butylbenzylphthalate ND ug/L 1 06/23/11 06:55 85-68-706/21/11 18:005.0 0.79
4-Chloro-3-methylphenol ND ug/L 1 06/23/11 06:55 59-50-706/21/11 18:005.0 3.7
bis(2-Chloroethoxy)methane ND ug/L 1 06/23/11 06:55 111-91-106/21/11 18:0010.0 0.92
bis(2-Chloroethyl) ether ND ug/L 1 06/23/11 06:55 111-44-406/21/11 18:005.0 1.0
bis(2-Chloroisopropyl) ether ND ug/L 1 06/23/11 06:55 108-60-106/21/11 18:005.0 0.95
2-Chloronaphthalene ND ug/L 1 06/23/11 06:55 91-58-706/21/11 18:005.0 0.98
2-Chlorophenol ND ug/L 1 06/23/11 06:55 95-57-806/21/11 18:005.0 1.3
4-Chlorophenylphenyl ether ND ug/L 1 06/23/11 06:55 7005-72-306/21/11 18:005.0 0.87
Chrysene ND ug/L 1 06/23/11 06:55 218-01-906/21/11 18:005.0 0.21
Dibenz(a,h)anthracene ND ug/L 1 06/23/11 06:55 53-70-306/21/11 18:005.0 0.55
3,3'-Dichlorobenzidine ND ug/L 1 06/23/11 06:55 91-94-106/21/11 18:0025.0 2.1
2,4-Dichlorophenol ND ug/L 1 06/23/11 06:55 120-83-206/21/11 18:005.0 1.7
Diethylphthalate ND ug/L 1 06/23/11 06:55 84-66-206/21/11 18:005.0 0.58
2,4-Dimethylphenol ND ug/L 1 06/23/11 06:55 105-67-906/21/11 18:0010.0 1.2
Dimethylphthalate ND ug/L 1 06/23/11 06:55 131-11-306/21/11 18:005.0 0.76
Di-n-butylphthalate ND ug/L 1 06/23/11 06:55 84-74-206/21/11 18:005.0 0.75
4,6-Dinitro-2-methylphenol ND ug/L 1 06/23/11 06:55 534-52-106/21/11 18:0020.0 2.6
2,4-Dinitrophenol ND ug/L 1 06/23/11 06:55 51-28-506/21/11 18:0050.0 9.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 9 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Sample:MW-3 Lab ID:9296540002 Collected:06/16/11 09:15 Received:06/17/11 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
2,4-Dinitrotoluene ND ug/L 1 06/23/11 06:55 121-14-206/21/11 18:005.0 0.90
2,6-Dinitrotoluene ND ug/L 1 06/23/11 06:55 606-20-206/21/11 18:005.0 0.98
Di-n-octylphthalate ND ug/L 1 06/23/11 06:55 117-84-006/21/11 18:005.0 0.66
bis(2-Ethylhexyl)phthalate ND ug/L 1 06/23/11 06:55 117-81-706/21/11 18:005.0 0.79
Fluoranthene ND ug/L 1 06/23/11 06:55 206-44-006/21/11 18:005.0 0.21
Fluorene ND ug/L 1 06/23/11 06:55 86-73-706/21/11 18:005.0 0.21
Hexachloro-1,3-butadiene ND ug/L 1 06/23/11 06:55 87-68-306/21/11 18:005.0 0.94
Hexachlorobenzene ND ug/L 1 06/23/11 06:55 118-74-106/21/11 18:005.0 0.72
Hexachlorocyclopentadiene ND ug/L 1 06/23/11 06:55 77-47-406/21/11 18:0010.0 0.88
Hexachloroethane ND ug/L 1 06/23/11 06:55 67-72-106/21/11 18:005.0 1.1
Indeno(1,2,3-cd)pyrene ND ug/L 1 06/23/11 06:55 193-39-506/21/11 18:005.0 0.29
Isophorone ND ug/L 1 06/23/11 06:55 78-59-106/21/11 18:0010.0 0.89
2-Methylnaphthalene ND ug/L 1 06/23/11 06:55 91-57-606/21/11 18:005.0 0.28
Naphthalene ND ug/L 1 06/23/11 06:55 91-20-306/21/11 18:005.0 0.34
Nitrobenzene ND ug/L 1 06/23/11 06:55 98-95-306/21/11 18:005.0 1.1
2-Nitrophenol ND ug/L 1 06/23/11 06:55 88-75-506/21/11 18:005.0 0.91
4-Nitrophenol ND ug/L 1 06/23/11 06:55 100-02-706/21/11 18:0050.0 4.1
N-Nitrosodimethylamine ND ug/L 1 06/23/11 06:55 62-75-906/21/11 18:005.0 0.91
N-Nitroso-di-n-propylamine ND ug/L 1 06/23/11 06:55 621-64-706/21/11 18:005.0 0.99
N-Nitrosodiphenylamine ND ug/L 1 06/23/11 06:55 86-30-606/21/11 18:0010.0 1.0
Pentachlorophenol ND ug/L 1 06/23/11 06:55 87-86-506/21/11 18:0025.0 4.6
Phenanthrene ND ug/L 1 06/23/11 06:55 85-01-806/21/11 18:005.0 0.22
Phenol ND ug/L 1 06/23/11 06:55 108-95-206/21/11 18:005.0 1.9
Pyrene ND ug/L 1 06/23/11 06:55 129-00-006/21/11 18:005.0 0.19
1,2,4-Trichlorobenzene ND ug/L 1 06/23/11 06:55 120-82-106/21/11 18:005.0 0.98
2,4,6-Trichlorophenol ND ug/L 1 06/23/11 06:55 88-06-206/21/11 18:0010.0 1.3
Nitrobenzene-d5 (S)70 %1 06/23/11 06:55 4165-60-006/21/11 18:0010-120
2-Fluorobiphenyl (S)71 %1 06/23/11 06:55 321-60-806/21/11 18:0015-120
Terphenyl-d14 (S)79 %1 06/23/11 06:55 1718-51-006/21/11 18:0011-131
Phenol-d6 (S)27 %1 06/23/11 06:55 13127-88-306/21/11 18:0010-120
2-Fluorophenol (S)41 %1 06/23/11 06:55 367-12-406/21/11 18:0010-120
2,4,6-Tribromophenol (S)112 %1 06/23/11 06:55 118-79-606/21/11 18:0010-137
6200B MSV Analytical Method: SM 6200B
Benzene 0.61 ug/L 1 06/24/11 04:38 71-43-20.50 0.50
Bromobenzene ND ug/L 1 06/24/11 04:38 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 06/24/11 04:38 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 06/24/11 04:38 75-27-40.50 0.50
Bromoform ND ug/L 1 06/24/11 04:38 75-25-20.50 0.50
Bromomethane ND ug/L 1 06/24/11 04:38 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 06/24/11 04:38 104-51-80.50 0.50
sec-Butylbenzene 1.6 ug/L 1 06/24/11 04:38 135-98-80.50 0.50
tert-Butylbenzene 0.92 ug/L 1 06/24/11 04:38 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 06/24/11 04:38 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 06/24/11 04:38 108-90-70.50 0.50
Chloroethane ND ug/L 1 06/24/11 04:38 75-00-31.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 10 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Sample:MW-3 Lab ID:9296540002 Collected:06/16/11 09:15 Received:06/17/11 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Chloroform ND ug/L 1 06/24/11 04:38 67-66-30.50 0.50
Chloromethane ND ug/L 1 06/24/11 04:38 74-87-31.0 1.0
2-Chlorotoluene ND ug/L 1 06/24/11 04:38 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 06/24/11 04:38 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 06/24/11 04:38 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 06/24/11 04:38 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 06/24/11 04:38 106-93-40.50 0.50
Dibromomethane ND ug/L 1 06/24/11 04:38 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 06/24/11 04:38 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 06/24/11 04:38 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 06/24/11 04:38 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 06/24/11 04:38 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 06/24/11 04:38 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 06/24/11 04:38 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 06/24/11 04:38 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 06/24/11 04:38 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 06/24/11 04:38 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 06/24/11 04:38 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 06/24/11 04:38 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 06/24/11 04:38 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 06/24/11 04:38 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 06/24/11 04:38 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 06/24/11 04:38 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 06/24/11 04:38 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 06/24/11 04:38 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 06/24/11 04:38 87-68-32.0 2.0
Isopropylbenzene (Cumene)0.94 ug/L 1 06/24/11 04:38 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 06/24/11 04:38 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 06/24/11 04:38 1634-04-40.50 0.50
Naphthalene ND ug/L 1 06/24/11 04:38 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 06/24/11 04:38 103-65-10.50 0.50
Styrene ND ug/L 1 06/24/11 04:38 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 06/24/11 04:38 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 06/24/11 04:38 79-34-50.50 0.50
Tetrachloroethene ND ug/L 1 06/24/11 04:38 127-18-40.50 0.50
Toluene ND ug/L 1 06/24/11 04:38 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 06/24/11 04:38 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 06/24/11 04:38 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 06/24/11 04:38 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 06/24/11 04:38 79-00-50.50 0.50
Trichloroethene ND ug/L 1 06/24/11 04:38 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 06/24/11 04:38 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 06/24/11 04:38 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 06/24/11 04:38 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 06/24/11 04:38 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 06/24/11 04:38 75-01-41.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 11 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Sample:MW-3 Lab ID:9296540002 Collected:06/16/11 09:15 Received:06/17/11 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
m&p-Xylene ND ug/L 1 06/24/11 04:38 179601-23-11.0 1.0
o-Xylene ND ug/L 1 06/24/11 04:38 95-47-60.50 0.50
1,2-Dichloroethane-d4 (S)124 %1 06/24/11 04:38 17060-07-070-130
Dibromofluoromethane (S)114 %1 06/24/11 04:38 1868-53-770-130
4-Bromofluorobenzene (S)91 %1 06/24/11 04:38 460-00-470-130
Toluene-d8 (S)99 %1 06/24/11 04:38 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 12 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Sample:MW-5R Lab ID:9296540003 Collected:06/16/11 10:15 Received:06/17/11 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 06/24/11 20:42 N206/21/11 19:00100100
Aliphatic (C19-C36)ND ug/L 1 06/24/11 20:42 N206/21/11 19:00100100
Aromatic (C11-C22)ND ug/L 1 06/24/11 20:42 N206/21/11 19:00100100
Nonatriacontane (S)79 %1 06/24/11 20:42 7194-86-706/21/11 19:0040-140
o-Terphenyl (S)75 %1 06/24/11 20:42 84-15-106/21/11 19:0040-140
2-Fluorobiphenyl (S)100 %1 06/24/11 20:42 321-60-806/21/11 19:0040-140
2-Bromonaphthalene (S)107 %1 06/24/11 20:42 580-13-206/21/11 19:0040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 06/23/11 23:32 N250.0 15.0
Aliphatic (C09-C12)ND ug/L 1 06/23/11 23:32 N250.0 15.0
Aromatic (C09-C10)ND ug/L 1 06/23/11 23:32 N250.0 15.0
2,5-Dibromotoluene (PID)(S)115 %1 06/23/11 23:3270-130
2,5-Dibromotoluene (FID)(S)116 %1 06/23/11 23:3270-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead 20.5 ug/L 1 06/22/11 17:50 7439-92-106/18/11 13:305.0 4.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 06/23/11 07:22 83-32-906/21/11 18:005.0 0.25
Acenaphthylene ND ug/L 1 06/23/11 07:22 208-96-806/21/11 18:005.0 0.21
Anthracene ND ug/L 1 06/23/11 07:22 120-12-706/21/11 18:005.0 0.14
Benzo(a)anthracene ND ug/L 1 06/23/11 07:22 56-55-306/21/11 18:005.0 0.33
Benzo(a)pyrene ND ug/L 1 06/23/11 07:22 50-32-806/21/11 18:005.0 0.30
Benzo(b)fluoranthene ND ug/L 1 06/23/11 07:22 205-99-206/21/11 18:005.0 0.28
Benzo(g,h,i)perylene ND ug/L 1 06/23/11 07:22 191-24-206/21/11 18:005.0 0.38
Benzo(k)fluoranthene ND ug/L 1 06/23/11 07:22 207-08-906/21/11 18:005.0 0.43
4-Bromophenylphenyl ether ND ug/L 1 06/23/11 07:22 101-55-306/21/11 18:005.0 0.82
Butylbenzylphthalate ND ug/L 1 06/23/11 07:22 85-68-706/21/11 18:005.0 0.79
4-Chloro-3-methylphenol ND ug/L 1 06/23/11 07:22 59-50-706/21/11 18:005.0 3.7
bis(2-Chloroethoxy)methane ND ug/L 1 06/23/11 07:22 111-91-106/21/11 18:0010.0 0.92
bis(2-Chloroethyl) ether ND ug/L 1 06/23/11 07:22 111-44-406/21/11 18:005.0 1.0
bis(2-Chloroisopropyl) ether ND ug/L 1 06/23/11 07:22 108-60-106/21/11 18:005.0 0.95
2-Chloronaphthalene ND ug/L 1 06/23/11 07:22 91-58-706/21/11 18:005.0 0.98
2-Chlorophenol ND ug/L 1 06/23/11 07:22 95-57-806/21/11 18:005.0 1.3
4-Chlorophenylphenyl ether ND ug/L 1 06/23/11 07:22 7005-72-306/21/11 18:005.0 0.87
Chrysene ND ug/L 1 06/23/11 07:22 218-01-906/21/11 18:005.0 0.21
Dibenz(a,h)anthracene ND ug/L 1 06/23/11 07:22 53-70-306/21/11 18:005.0 0.55
3,3'-Dichlorobenzidine ND ug/L 1 06/23/11 07:22 91-94-106/21/11 18:0025.0 2.1
2,4-Dichlorophenol ND ug/L 1 06/23/11 07:22 120-83-206/21/11 18:005.0 1.7
Diethylphthalate ND ug/L 1 06/23/11 07:22 84-66-206/21/11 18:005.0 0.58
2,4-Dimethylphenol ND ug/L 1 06/23/11 07:22 105-67-906/21/11 18:0010.0 1.2
Dimethylphthalate ND ug/L 1 06/23/11 07:22 131-11-306/21/11 18:005.0 0.76
Di-n-butylphthalate ND ug/L 1 06/23/11 07:22 84-74-206/21/11 18:005.0 0.75
4,6-Dinitro-2-methylphenol ND ug/L 1 06/23/11 07:22 534-52-106/21/11 18:0020.0 2.6
2,4-Dinitrophenol ND ug/L 1 06/23/11 07:22 51-28-506/21/11 18:0050.0 9.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 13 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Sample:MW-5R Lab ID:9296540003 Collected:06/16/11 10:15 Received:06/17/11 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
2,4-Dinitrotoluene ND ug/L 1 06/23/11 07:22 121-14-206/21/11 18:005.0 0.90
2,6-Dinitrotoluene ND ug/L 1 06/23/11 07:22 606-20-206/21/11 18:005.0 0.98
Di-n-octylphthalate ND ug/L 1 06/23/11 07:22 117-84-006/21/11 18:005.0 0.66
bis(2-Ethylhexyl)phthalate ND ug/L 1 06/23/11 07:22 117-81-706/21/11 18:005.0 0.79
Fluoranthene ND ug/L 1 06/23/11 07:22 206-44-006/21/11 18:005.0 0.21
Fluorene ND ug/L 1 06/23/11 07:22 86-73-706/21/11 18:005.0 0.21
Hexachloro-1,3-butadiene ND ug/L 1 06/23/11 07:22 87-68-306/21/11 18:005.0 0.94
Hexachlorobenzene ND ug/L 1 06/23/11 07:22 118-74-106/21/11 18:005.0 0.72
Hexachlorocyclopentadiene ND ug/L 1 06/23/11 07:22 77-47-406/21/11 18:0010.0 0.88
Hexachloroethane ND ug/L 1 06/23/11 07:22 67-72-106/21/11 18:005.0 1.1
Indeno(1,2,3-cd)pyrene ND ug/L 1 06/23/11 07:22 193-39-506/21/11 18:005.0 0.29
Isophorone ND ug/L 1 06/23/11 07:22 78-59-106/21/11 18:0010.0 0.89
2-Methylnaphthalene ND ug/L 1 06/23/11 07:22 91-57-606/21/11 18:005.0 0.28
Naphthalene ND ug/L 1 06/23/11 07:22 91-20-306/21/11 18:005.0 0.34
Nitrobenzene ND ug/L 1 06/23/11 07:22 98-95-306/21/11 18:005.0 1.1
2-Nitrophenol ND ug/L 1 06/23/11 07:22 88-75-506/21/11 18:005.0 0.91
4-Nitrophenol ND ug/L 1 06/23/11 07:22 100-02-706/21/11 18:0050.0 4.1
N-Nitrosodimethylamine ND ug/L 1 06/23/11 07:22 62-75-906/21/11 18:005.0 0.91
N-Nitroso-di-n-propylamine ND ug/L 1 06/23/11 07:22 621-64-706/21/11 18:005.0 0.99
N-Nitrosodiphenylamine ND ug/L 1 06/23/11 07:22 86-30-606/21/11 18:0010.0 1.0
Pentachlorophenol ND ug/L 1 06/23/11 07:22 87-86-506/21/11 18:0025.0 4.6
Phenanthrene ND ug/L 1 06/23/11 07:22 85-01-806/21/11 18:005.0 0.22
Phenol ND ug/L 1 06/23/11 07:22 108-95-206/21/11 18:005.0 1.9
Pyrene ND ug/L 1 06/23/11 07:22 129-00-006/21/11 18:005.0 0.19
1,2,4-Trichlorobenzene ND ug/L 1 06/23/11 07:22 120-82-106/21/11 18:005.0 0.98
2,4,6-Trichlorophenol ND ug/L 1 06/23/11 07:22 88-06-206/21/11 18:0010.0 1.3
Nitrobenzene-d5 (S)67 %1 06/23/11 07:22 4165-60-006/21/11 18:0010-120
2-Fluorobiphenyl (S)68 %1 06/23/11 07:22 321-60-806/21/11 18:0015-120
Terphenyl-d14 (S)69 %1 06/23/11 07:22 1718-51-006/21/11 18:0011-131
Phenol-d6 (S)27 %1 06/23/11 07:22 13127-88-306/21/11 18:0010-120
2-Fluorophenol (S)37 %1 06/23/11 07:22 367-12-406/21/11 18:0010-120
2,4,6-Tribromophenol (S)105 %1 06/23/11 07:22 118-79-606/21/11 18:0010-137
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 06/24/11 05:00 71-43-20.50 0.50
Bromobenzene ND ug/L 1 06/24/11 05:00 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 06/24/11 05:00 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 06/24/11 05:00 75-27-40.50 0.50
Bromoform ND ug/L 1 06/24/11 05:00 75-25-20.50 0.50
Bromomethane ND ug/L 1 06/24/11 05:00 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 06/24/11 05:00 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 06/24/11 05:00 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 06/24/11 05:00 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 06/24/11 05:00 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 06/24/11 05:00 108-90-70.50 0.50
Chloroethane ND ug/L 1 06/24/11 05:00 75-00-31.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 14 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Sample:MW-5R Lab ID:9296540003 Collected:06/16/11 10:15 Received:06/17/11 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Chloroform ND ug/L 1 06/24/11 05:00 67-66-30.50 0.50
Chloromethane ND ug/L 1 06/24/11 05:00 74-87-31.0 1.0
2-Chlorotoluene ND ug/L 1 06/24/11 05:00 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 06/24/11 05:00 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 06/24/11 05:00 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 06/24/11 05:00 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 06/24/11 05:00 106-93-40.50 0.50
Dibromomethane ND ug/L 1 06/24/11 05:00 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 06/24/11 05:00 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 06/24/11 05:00 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 06/24/11 05:00 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 06/24/11 05:00 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 06/24/11 05:00 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 06/24/11 05:00 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 06/24/11 05:00 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 06/24/11 05:00 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 06/24/11 05:00 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 06/24/11 05:00 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 06/24/11 05:00 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 06/24/11 05:00 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 06/24/11 05:00 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 06/24/11 05:00 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 06/24/11 05:00 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 06/24/11 05:00 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 06/24/11 05:00 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 06/24/11 05:00 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 06/24/11 05:00 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 06/24/11 05:00 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 06/24/11 05:00 1634-04-40.50 0.50
Naphthalene ND ug/L 1 06/24/11 05:00 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 06/24/11 05:00 103-65-10.50 0.50
Styrene ND ug/L 1 06/24/11 05:00 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 06/24/11 05:00 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 06/24/11 05:00 79-34-50.50 0.50
Tetrachloroethene ND ug/L 1 06/24/11 05:00 127-18-40.50 0.50
Toluene ND ug/L 1 06/24/11 05:00 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 06/24/11 05:00 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 06/24/11 05:00 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 06/24/11 05:00 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 06/24/11 05:00 79-00-50.50 0.50
Trichloroethene ND ug/L 1 06/24/11 05:00 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 06/24/11 05:00 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 06/24/11 05:00 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 06/24/11 05:00 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 06/24/11 05:00 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 06/24/11 05:00 75-01-41.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 15 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Sample:MW-5R Lab ID:9296540003 Collected:06/16/11 10:15 Received:06/17/11 13:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
m&p-Xylene ND ug/L 1 06/24/11 05:00 179601-23-11.0 1.0
o-Xylene ND ug/L 1 06/24/11 05:00 95-47-60.50 0.50
1,2-Dichloroethane-d4 (S)124 %1 06/24/11 05:00 17060-07-070-130
Dibromofluoromethane (S)113 %1 06/24/11 05:00 1868-53-770-130
4-Bromofluorobenzene (S)90 %1 06/24/11 05:00 460-00-470-130
Toluene-d8 (S)98 %1 06/24/11 05:00 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 16 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/14009
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Associated Lab Samples:9296540001, 9296540002, 9296540003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:624081
Associated Lab Samples:9296540001, 9296540002, 9296540003
Matrix:Water
Analyzed
Aliphatic (C09-C18)ug/L ND 100 N206/23/11 18:40
Aliphatic (C19-C36)ug/L ND 100 N206/23/11 18:40
Aromatic (C11-C22)ug/L ND 100 N206/23/11 18:40
2-Bromonaphthalene (S)%125 40-140 06/23/11 18:40
2-Fluorobiphenyl (S)%114 40-140 06/23/11 18:40
Nonatriacontane (S)%72 40-140 06/23/11 18:40
o-Terphenyl (S)%109 40-140 06/23/11 18:40
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
624082LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
624083
Aliphatic (C09-C18)ug/L 214 N23007140-14063190 12 50
Aliphatic (C19-C36)ug/L 379 N24009540-14084336 12 50
Aromatic (C11-C22)ug/L 678 N28508040-14067567 18 50
2-Bromonaphthalene (S)%84 40-14085
2-Fluorobiphenyl (S)%82 40-14073
Nonatriacontane (S)%77 40-14068
o-Terphenyl (S)%72 40-14058
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 17 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/5146
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples:9296540001, 9296540002, 9296540003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:624192
Associated Lab Samples:9296540001, 9296540002, 9296540003
Matrix:Water
Analyzed
Aliphatic (C05-C08)ug/L ND 50.0 N206/23/11 21:03
Aliphatic (C09-C12)ug/L 16.7J 50.0 N206/23/11 21:03
Aromatic (C09-C10)ug/L ND 50.0 N206/23/11 21:03
2,5-Dibromotoluene (FID)(S)%117 70-130 06/23/11 21:03
2,5-Dibromotoluene (PID)(S)%117 70-130 06/23/11 21:03
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
624193LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
624194
Aliphatic (C05-C08)ug/L 258 N23008670-13088265 3 25
Aliphatic (C09-C12)ug/L 298 N23009930-130103308 3 25
Aromatic (C09-C10)ug/L 95.6 N21009670-130101101 5 25
2,5-Dibromotoluene (FID)(S)%122 70-130111
2,5-Dibromotoluene (PID)(S)%121 70-130112
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 18 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/8571
SM 3030C
EPA 200.7
200.7 MET 3030C
Associated Lab Samples:9296540001, 9296540002, 9296540003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:622926
Associated Lab Samples:9296540001, 9296540002, 9296540003
Matrix:Water
Analyzed
Lead ug/L ND 5.0 06/22/11 17:31
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
622927LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 555500 111 85-115
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
622928MATRIX SPIKE SAMPLE:
MSSpike
Result
9296540002
Lead ug/L 526500 104 70-1304.2J
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9296540001
622929SAMPLE DUPLICATE:
Lead ug/L 15.8 20 2012.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 19 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/14001
EPA 625
EPA 625
625 MSS
Associated Lab Samples:9296540001, 9296540002, 9296540003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:623865
Associated Lab Samples:9296540001, 9296540002, 9296540003
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 06/22/11 21:18
2,4,6-Trichlorophenol ug/L ND 10.0 06/22/11 21:18
2,4-Dichlorophenol ug/L ND 5.0 06/22/11 21:18
2,4-Dimethylphenol ug/L ND 10.0 06/22/11 21:18
2,4-Dinitrophenol ug/L ND 50.0 06/22/11 21:18
2,4-Dinitrotoluene ug/L ND 5.0 06/22/11 21:18
2,6-Dinitrotoluene ug/L ND 5.0 06/22/11 21:18
2-Chloronaphthalene ug/L ND 5.0 06/22/11 21:18
2-Chlorophenol ug/L ND 5.0 06/22/11 21:18
2-Methylnaphthalene ug/L ND 5.0 06/22/11 21:18
2-Nitrophenol ug/L ND 5.0 06/22/11 21:18
3,3'-Dichlorobenzidine ug/L ND 25.0 06/22/11 21:18
4,6-Dinitro-2-methylphenol ug/L ND 20.0 06/22/11 21:18
4-Bromophenylphenyl ether ug/L ND 5.0 06/22/11 21:18
4-Chloro-3-methylphenol ug/L ND 5.0 06/22/11 21:18
4-Chlorophenylphenyl ether ug/L ND 5.0 06/22/11 21:18
4-Nitrophenol ug/L ND 50.0 06/22/11 21:18
Acenaphthene ug/L ND 5.0 06/22/11 21:18
Acenaphthylene ug/L ND 5.0 06/22/11 21:18
Anthracene ug/L ND 5.0 06/22/11 21:18
Benzo(a)anthracene ug/L ND 5.0 06/22/11 21:18
Benzo(a)pyrene ug/L ND 5.0 06/22/11 21:18
Benzo(b)fluoranthene ug/L ND 5.0 06/22/11 21:18
Benzo(g,h,i)perylene ug/L ND 5.0 06/22/11 21:18
Benzo(k)fluoranthene ug/L ND 5.0 06/22/11 21:18
bis(2-Chloroethoxy)methane ug/L ND 10.0 06/22/11 21:18
bis(2-Chloroethyl) ether ug/L ND 5.0 06/22/11 21:18
bis(2-Chloroisopropyl) ether ug/L ND 5.0 06/22/11 21:18
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 06/22/11 21:18
Butylbenzylphthalate ug/L ND 5.0 06/22/11 21:18
Chrysene ug/L ND 5.0 06/22/11 21:18
Di-n-butylphthalate ug/L ND 5.0 06/22/11 21:18
Di-n-octylphthalate ug/L ND 5.0 06/22/11 21:18
Dibenz(a,h)anthracene ug/L ND 5.0 06/22/11 21:18
Diethylphthalate ug/L ND 5.0 06/22/11 21:18
Dimethylphthalate ug/L ND 5.0 06/22/11 21:18
Fluoranthene ug/L ND 5.0 06/22/11 21:18
Fluorene ug/L ND 5.0 06/22/11 21:18
Hexachloro-1,3-butadiene ug/L ND 5.0 06/22/11 21:18
Hexachlorobenzene ug/L ND 5.0 06/22/11 21:18
Hexachlorocyclopentadiene ug/L ND 10.0 06/22/11 21:18
Hexachloroethane ug/L ND 5.0 06/22/11 21:18
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 06/22/11 21:18
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 20 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:623865
Associated Lab Samples:9296540001, 9296540002, 9296540003
Matrix:Water
Analyzed
Isophorone ug/L ND 10.0 06/22/11 21:18
N-Nitroso-di-n-propylamine ug/L ND 5.0 06/22/11 21:18
N-Nitrosodimethylamine ug/L ND 5.0 06/22/11 21:18
N-Nitrosodiphenylamine ug/L ND 10.0 06/22/11 21:18
Naphthalene ug/L ND 5.0 06/22/11 21:18
Nitrobenzene ug/L ND 5.0 06/22/11 21:18
Pentachlorophenol ug/L ND 25.0 06/22/11 21:18
Phenanthrene ug/L ND 5.0 06/22/11 21:18
Phenol ug/L ND 5.0 06/22/11 21:18
Pyrene ug/L ND 5.0 06/22/11 21:18
2,4,6-Tribromophenol (S)%85 10-137 06/22/11 21:18
2-Fluorobiphenyl (S)%62 15-120 06/22/11 21:18
2-Fluorophenol (S)%33 10-120 06/22/11 21:18
Nitrobenzene-d5 (S)%60 10-120 06/22/11 21:18
Phenol-d6 (S)%23 10-120 06/22/11 21:18
Terphenyl-d14 (S)%70 11-131 06/22/11 21:18
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
623866LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 30.850 62 44-142
2,4,6-Trichlorophenol ug/L 42.550 85 37-144
2,4-Dichlorophenol ug/L 39.650 79 1-191
2,4-Dimethylphenol ug/L 35.350 71 32-119
2,4-Dinitrophenol ug/L 102250 41 1-181
2,4-Dinitrotoluene ug/L 40.850 82 39-139
2,6-Dinitrotoluene ug/L 41.850 84 50-158
2-Chloronaphthalene ug/L 37.650 75 60-118
2-Chlorophenol ug/L 36.550 73 23-134
2-Methylnaphthalene ug/L 35.050 70 25-150
2-Nitrophenol ug/L 38.050 76 29-182
3,3'-Dichlorobenzidine ug/L 69.2100 69 1-262
4,6-Dinitro-2-methylphenol ug/L 73.0100 73 1-181
4-Bromophenylphenyl ether ug/L 41.950 84 53-127
4-Chloro-3-methylphenol ug/L 83.4100 83 22-147
4-Chlorophenylphenyl ether ug/L 40.750 81 25-158
4-Nitrophenol ug/L 87.4250 35 1-132
Acenaphthene ug/L 38.050 76 47-145
Acenaphthylene ug/L 35.550 71 33-145
Anthracene ug/L 39.950 80 1-166
Benzo(a)anthracene ug/L 37.950 76 33-143
Benzo(a)pyrene ug/L 36.450 73 17-163
Benzo(b)fluoranthene ug/L 35.550 71 24-159
Benzo(g,h,i)perylene ug/L 42.050 84 1-219
Benzo(k)fluoranthene ug/L 35.250 70 11-162
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 21 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
623866LABORATORY CONTROL SAMPLE:
LCSSpike
bis(2-Chloroethoxy)methane ug/L 37.150 74 33-184
bis(2-Chloroethyl) ether ug/L 34.450 69 12-158
bis(2-Chloroisopropyl) ether ug/L 35.650 71 36-166
bis(2-Ethylhexyl)phthalate ug/L 39.350 79 8-158
Butylbenzylphthalate ug/L 36.950 74 1-152
Chrysene ug/L 38.150 76 17-168
Di-n-butylphthalate ug/L 39.150 78 1-118
Di-n-octylphthalate ug/L 41.150 82 4-146
Dibenz(a,h)anthracene ug/L 41.650 83 1-227
Diethylphthalate ug/L 38.050 76 1-114
Dimethylphthalate ug/L 39.550 79 1-112
Fluoranthene ug/L 38.550 77 26-137
Fluorene ug/L 37.850 76 59-121
Hexachloro-1,3-butadiene ug/L 28.750 57 24-116
Hexachlorobenzene ug/L 43.450 87 1-152
Hexachlorocyclopentadiene ug/L 35.450 71 25-150
Hexachloroethane ug/L 24.050 48 40-113
Indeno(1,2,3-cd)pyrene ug/L 41.550 83 1-171
Isophorone ug/L 43.250 86 21-196
N-Nitroso-di-n-propylamine ug/L 41.750 83 1-230
N-Nitrosodimethylamine ug/L 24.250 48 25-150
N-Nitrosodiphenylamine ug/L 38.050 76 25-150
Naphthalene ug/L 32.050 64 21-133
Nitrobenzene ug/L 43.950 88 35-180
Pentachlorophenol ug/L 51.2100 51 14-176
Phenanthrene ug/L 38.050 76 54-120
Phenol ug/L 19.150 38 5-112
Pyrene ug/L 34.450 69 52-115
2,4,6-Tribromophenol (S)%104 10-137
2-Fluorobiphenyl (S)%76 15-120
2-Fluorophenol (S)%44 10-120
Nitrobenzene-d5 (S)%76 10-120
Phenol-d6 (S)%30 10-120
Terphenyl-d14 (S)%73 11-131
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 22 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/15786
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:9296540001, 9296540002, 9296540003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:625471
Associated Lab Samples:9296540001, 9296540002, 9296540003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 06/24/11 02:43
1,1,1-Trichloroethane ug/L ND 0.50 06/24/11 02:43
1,1,2,2-Tetrachloroethane ug/L ND 0.50 06/24/11 02:43
1,1,2-Trichloroethane ug/L ND 0.50 06/24/11 02:43
1,1-Dichloroethane ug/L ND 0.50 06/24/11 02:43
1,1-Dichloroethene ug/L ND 0.50 06/24/11 02:43
1,1-Dichloropropene ug/L ND 0.50 06/24/11 02:43
1,2,3-Trichlorobenzene ug/L ND 2.0 06/24/11 02:43
1,2,3-Trichloropropane ug/L ND 0.50 06/24/11 02:43
1,2,4-Trichlorobenzene ug/L ND 2.0 06/24/11 02:43
1,2,4-Trimethylbenzene ug/L ND 0.50 06/24/11 02:43
1,2-Dibromo-3-chloropropane ug/L ND 1.0 06/24/11 02:43
1,2-Dibromoethane (EDB)ug/L ND 0.50 06/24/11 02:43
1,2-Dichlorobenzene ug/L ND 0.50 06/24/11 02:43
1,2-Dichloroethane ug/L ND 0.50 06/24/11 02:43
1,2-Dichloropropane ug/L ND 0.50 06/24/11 02:43
1,3,5-Trimethylbenzene ug/L ND 0.50 06/24/11 02:43
1,3-Dichlorobenzene ug/L ND 0.50 06/24/11 02:43
1,3-Dichloropropane ug/L ND 0.50 06/24/11 02:43
1,4-Dichlorobenzene ug/L ND 0.50 06/24/11 02:43
2,2-Dichloropropane ug/L ND 0.50 06/24/11 02:43
2-Chlorotoluene ug/L ND 0.50 06/24/11 02:43
4-Chlorotoluene ug/L ND 0.50 06/24/11 02:43
Benzene ug/L ND 0.50 06/24/11 02:43
Bromobenzene ug/L ND 0.50 06/24/11 02:43
Bromochloromethane ug/L ND 0.50 06/24/11 02:43
Bromodichloromethane ug/L ND 0.50 06/24/11 02:43
Bromoform ug/L ND 0.50 06/24/11 02:43
Bromomethane ug/L ND 5.0 06/24/11 02:43
Carbon tetrachloride ug/L ND 0.50 06/24/11 02:43
Chlorobenzene ug/L ND 0.50 06/24/11 02:43
Chloroethane ug/L ND 1.0 06/24/11 02:43
Chloroform ug/L ND 0.50 06/24/11 02:43
Chloromethane ug/L ND 1.0 06/24/11 02:43
cis-1,2-Dichloroethene ug/L ND 0.50 06/24/11 02:43
cis-1,3-Dichloropropene ug/L ND 0.50 06/24/11 02:43
Dibromochloromethane ug/L ND 0.50 06/24/11 02:43
Dibromomethane ug/L ND 0.50 06/24/11 02:43
Dichlorodifluoromethane ug/L ND 0.50 06/24/11 02:43
Diisopropyl ether ug/L ND 0.50 06/24/11 02:43
Ethylbenzene ug/L ND 0.50 06/24/11 02:43
Hexachloro-1,3-butadiene ug/L ND 2.0 06/24/11 02:43
Isopropylbenzene (Cumene)ug/L ND 0.50 06/24/11 02:43
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 23 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:625471
Associated Lab Samples:9296540001, 9296540002, 9296540003
Matrix:Water
Analyzed
m&p-Xylene ug/L ND 1.0 06/24/11 02:43
Methyl-tert-butyl ether ug/L ND 0.50 06/24/11 02:43
Methylene Chloride ug/L ND 2.0 06/24/11 02:43
n-Butylbenzene ug/L ND 0.50 06/24/11 02:43
n-Propylbenzene ug/L ND 0.50 06/24/11 02:43
Naphthalene ug/L ND 2.0 06/24/11 02:43
o-Xylene ug/L ND 0.50 06/24/11 02:43
sec-Butylbenzene ug/L ND 0.50 06/24/11 02:43
Styrene ug/L ND 0.50 06/24/11 02:43
tert-Butylbenzene ug/L ND 0.50 06/24/11 02:43
Tetrachloroethene ug/L ND 0.50 06/24/11 02:43
Toluene ug/L ND 0.50 06/24/11 02:43
trans-1,2-Dichloroethene ug/L ND 0.50 06/24/11 02:43
trans-1,3-Dichloropropene ug/L ND 0.50 06/24/11 02:43
Trichloroethene ug/L ND 0.50 06/24/11 02:43
Trichlorofluoromethane ug/L ND 1.0 06/24/11 02:43
Vinyl chloride ug/L ND 1.0 06/24/11 02:43
1,2-Dichloroethane-d4 (S)%122 70-130 06/24/11 02:43
4-Bromofluorobenzene (S)%91 70-130 06/24/11 02:43
Dibromofluoromethane (S)%112 70-130 06/24/11 02:43
Toluene-d8 (S)%98 70-130 06/24/11 02:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
625472LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 45.550 91 60-140
1,1,1-Trichloroethane ug/L 51.250 102 60-140
1,1,2,2-Tetrachloroethane ug/L 47.150 94 60-140
1,1,2-Trichloroethane ug/L 46.950 94 60-140
1,1-Dichloroethane ug/L 51.350 103 60-140
1,1-Dichloroethene ug/L 48.650 97 60-140
1,1-Dichloropropene ug/L 46.750 93 60-140
1,2,3-Trichlorobenzene ug/L 47.050 94 60-140
1,2,3-Trichloropropane ug/L 44.050 88 60-140
1,2,4-Trichlorobenzene ug/L 46.050 92 60-140
1,2,4-Trimethylbenzene ug/L 47.450 95 60-140
1,2-Dibromo-3-chloropropane ug/L 44.750 89 60-140
1,2-Dibromoethane (EDB)ug/L 45.750 91 60-140
1,2-Dichlorobenzene ug/L 45.150 90 60-140
1,2-Dichloroethane ug/L 54.750 109 60-140
1,2-Dichloropropane ug/L 47.150 94 60-140
1,3,5-Trimethylbenzene ug/L 47.250 94 60-140
1,3-Dichlorobenzene ug/L 44.950 90 60-140
1,3-Dichloropropane ug/L 47.150 94 60-140
1,4-Dichlorobenzene ug/L 45.450 91 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 24 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
625472LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 45.750 91 60-140
2-Chlorotoluene ug/L 48.050 96 60-140
4-Chlorotoluene ug/L 48.650 97 60-140
Benzene ug/L 43.950 88 60-140
Bromobenzene ug/L 46.850 94 60-140
Bromochloromethane ug/L 45.950 92 60-140
Bromodichloromethane ug/L 47.950 96 60-140
Bromoform ug/L 40.550 81 60-140
Bromomethane ug/L 46.450 93 60-140
Carbon tetrachloride ug/L 46.550 93 60-140
Chlorobenzene ug/L 46.750 93 60-140
Chloroethane ug/L 58.950 118 60-140
Chloroform ug/L 53.250 106 60-140
Chloromethane ug/L 43.950 88 60-140
cis-1,2-Dichloroethene ug/L 47.350 95 60-140
cis-1,3-Dichloropropene ug/L 44.650 89 60-140
Dibromochloromethane ug/L 43.550 87 60-140
Dibromomethane ug/L 41.850 84 60-140
Dichlorodifluoromethane ug/L 45.750 91 60-140
Diisopropyl ether ug/L 49.750 99 60-140
Ethylbenzene ug/L 46.250 92 60-140
Hexachloro-1,3-butadiene ug/L 43.350 87 60-140
Isopropylbenzene (Cumene)ug/L 46.950 94 60-140
m&p-Xylene ug/L 92.9100 93 60-140
Methyl-tert-butyl ether ug/L 47.150 94 60-140
Methylene Chloride ug/L 52.750 105 60-140
n-Butylbenzene ug/L 50.650 101 60-140
n-Propylbenzene ug/L 48.850 98 60-140
Naphthalene ug/L 46.850 94 60-140
o-Xylene ug/L 46.250 92 60-140
sec-Butylbenzene ug/L 47.650 95 60-140
Styrene ug/L 47.550 95 60-140
tert-Butylbenzene ug/L 46.050 92 60-140
Tetrachloroethene ug/L 44.050 88 60-140
Toluene ug/L 43.250 86 60-140
trans-1,2-Dichloroethene ug/L 48.250 96 60-140
trans-1,3-Dichloropropene ug/L 46.550 93 60-140
Trichloroethene ug/L 46.150 92 60-140
Trichlorofluoromethane ug/L 54.450 109 60-140
Vinyl chloride ug/L 52.650 105 60-140
1,2-Dichloroethane-d4 (S)%114 70-130
4-Bromofluorobenzene (S)%95 70-130
Dibromofluoromethane (S)%111 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 25 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
626211MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9296539001
626212
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 67 60-14067 0 3020<0.50 13.4 13.4
1,1,1-Trichloroethane ug/L 20 90 60-14089 1 3020<0.50 18.0 17.8
1,1,2,2-Tetrachloroethane ug/L 20 73 60-14073 1 3020<0.50 14.7 14.5
1,1,2-Trichloroethane ug/L 20 72 60-14072 0 3020<0.50 14.4 14.4
1,1-Dichloroethane ug/L 20 90 60-14089 1 3020<0.50 18.0 17.7
1,1-Dichloroethene ug/L M0201160-14013 15 3020<0.50 2.2 2.6
1,1-Dichloropropene ug/L M0,R120560-1406 33 3020<0.50 0.93 1.3
1,2,3-Trichlorobenzene ug/L 20 65 60-14064 2 3020<2.0 13.1 12.9
1,2,3-Trichloropropane ug/L 20 68 60-14069 1 3020<0.50 13.6 13.8
1,2,4-Trichlorobenzene ug/L 20 65 60-14063 3 3020<2.0 13.1 12.6
1,2,4-Trimethylbenzene ug/L M020760-1409 24 3020<0.50 1.4 1.8
1,2-Dibromo-3-chloropropane ug/L 20 87 60-14081 7 3020<1.0 17.5 16.3
1,2-Dibromoethane (EDB)ug/L 20 69 60-14069 0 3020<0.50 13.8 13.9
1,2-Dichlorobenzene ug/L 20 70 60-14069 1 3020<0.50 13.9 13.9
1,2-Dichloroethane ug/L 20 94 60-14094 0 3020<0.50 18.8 18.9
1,2-Dichloropropane ug/L 20 76 60-14078 2 3020<0.50 15.3 15.5
1,3,5-Trimethylbenzene ug/L M020060-1401 3020<0.50 ND ND
1,3-Dichlorobenzene ug/L 20 69 60-14068 2 3020<0.50 13.8 13.5
1,3-Dichloropropane ug/L 20 72 60-14072 0 3020<0.50 14.4 14.5
1,4-Dichlorobenzene ug/L 20 73 60-14072 1 3020<0.50 14.7 14.5
2,2-Dichloropropane ug/L 20 73 60-14072 1 3020<0.50 14.6 14.4
2-Chlorotoluene ug/L 20 82 60-14080 3 3020<0.50 16.5 16.0
4-Chlorotoluene ug/L 20 82 60-14080 3 3020<0.50 16.5 16.1
Benzene ug/L 20 73 60-14073 1 3020<0.50 14.5 14.6
Bromobenzene ug/L 20 67 60-14064 5 3020<0.50 13.4 12.8
Bromochloromethane ug/L 20 77 60-14078 1 3020<0.50 15.4 15.6
Bromodichloromethane ug/L 20 74 60-14079 6 3020<0.50 15.1 16.1
Bromoform ug/L M0205060-14051 2 30202.1 12.2 12.4
Bromomethane ug/L 20 99 60-140104 4 3020<5.0 19.9 20.8
Carbon tetrachloride ug/L 20 77 60-14076 1 3020<0.50 15.5 15.3
Chlorobenzene ug/L 20 79 60-14076 3 3020<0.50 15.7 15.2
Chloroethane ug/L 20 116 60-140115 1 3020<1.0 23.2 23.1
Chloroform ug/L 20 93 60-14092 0 3020<0.50 18.5 18.4
Chloromethane ug/L 20 133 60-140129 3 3020<1.0 26.7 25.9
cis-1,2-Dichloroethene ug/L 20 85 60-14084 0 3020<0.50 16.9 16.9
cis-1,3-Dichloropropene ug/L M020660-1407 22 3020<0.50 1.2 1.5
Dibromochloromethane ug/L M0205960-14061 2 30201.0 12.9 13.2
Dibromomethane ug/L 20 70 60-14072 2 3020<0.50 14.1 14.4
Dichlorodifluoromethane ug/L 20 110 60-140109 1 3020<0.50 22.0 21.7
Diisopropyl ether ug/L 20 80 60-14079 1 3020<0.50 16.0 15.9
Ethylbenzene ug/L M020660-1408 27 3020<0.50 1.2 1.6
Hexachloro-1,3-butadiene ug/L 20 68 60-14065 5 3020<2.0 13.6 13.0
Isopropylbenzene (Cumene)ug/L M020560-1407 27 3020<0.50 1.1 1.4
m&p-Xylene ug/L M040160-1401 3040<1.0 ND ND
Methyl-tert-butyl ether ug/L 20 74 60-14073 1 3020<0.50 14.8 14.7
Methylene Chloride ug/L 20 85 60-14086 1 3020<2.0 17.1 17.3
n-Butylbenzene ug/L M020560-1406 15 3020<0.50 1.0 1.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 26 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
626211MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9296539001
626212
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
n-Propylbenzene ug/L M020660-1408 25 3020<0.50 1.2 1.5
Naphthalene ug/L M020360-1401 3020<2.0 ND ND
o-Xylene ug/L M020260-1403 3020<0.50 ND 0.66
sec-Butylbenzene ug/L M020660-1407 25 3020<0.50 1.1 1.4
Styrene ug/L M020060-1400 3020<0.50 ND ND
tert-Butylbenzene ug/L M020860-1409 15 3020<0.50 1.6 1.9
Tetrachloroethene ug/L 20 71 60-14069 3 3020<0.50 14.2 13.8
Toluene ug/L M0,R120560-1407 33 3020<0.50 1.0 1.5
trans-1,2-Dichloroethene ug/L 20 81 60-14081 1 3020<0.50 16.3 16.1
trans-1,3-Dichloropropene ug/L M020760-1408 19 3020<0.50 1.3 1.6
Trichloroethene ug/L 20 77 60-14075 3 3020<0.50 15.4 15.0
Trichlorofluoromethane ug/L 20 105 60-140104 1 3020<1.0 21.0 20.8
Vinyl chloride ug/L M020460-1405 3020<1.0 ND 1.1
1,2-Dichloroethane-d4 (S)%123 70-130126
4-Bromofluorobenzene (S)%91 70-13092
Dibromofluoromethane (S)%114 70-130116
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 27 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution ofthe sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
The lab does not hold TNI accreditation for this parameter.N2
Results acceptable because non-target analyte peak heights do not exceed the maximum calibrated upper range of thesystem per Section 9.5.8 of the MADEP VPH method.NC
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 28 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
9296540
12611 FERRELL RESIDENCE
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
9296540001 OEXT/14009 GCSV/10036MW-1 MADEP EPH MADEP EPH
9296540002 OEXT/14009 GCSV/10036MW-3 MADEP EPH MADEP EPH
9296540003 OEXT/14009 GCSV/10036MW-5R MADEP EPH MADEP EPH
9296540001 GCV/5146MW-1 MADEP VPH
9296540002 GCV/5146MW-3 MADEP VPH
9296540003 GCV/5146MW-5R MADEP VPH
9296540001 MPRP/8571 ICP/7922MW-1 SM 3030C EPA 200.7
9296540002 MPRP/8571 ICP/7922MW-3 SM 3030C EPA 200.7
9296540003 MPRP/8571 ICP/7922MW-5R SM 3030C EPA 200.7
9296540001 OEXT/14001 MSSV/5077MW-1 EPA 625 EPA 625
9296540002 OEXT/14001 MSSV/5077MW-3 EPA 625 EPA 625
9296540003 OEXT/14001 MSSV/5077MW-5R EPA 625 EPA 625
9296540001 MSV/15786MW-1 SM 6200B
9296540002 MSV/15786MW-3 SM 6200B
9296540003 MSV/15786MW-5R SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 06/28/2011 11:55 AM Page 29 of 29
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]