RA-2070_12610_CA_MRP_20110511_Terraine GW Letter

May 31, 2011

Mark Petermann, Hydrogeologist
Underground Storage Tank Section Division of Waste Management -- NCDENR
1637 Mail Service Center Raleigh, North Carolina 27699-1637

Reference: Former Four Corners Store 6154 West Mount Drive
Rocky Mount, NC 27803 Nash County
Incident # 12610
Subject: Groundwater Monitoring Results
Dear Mr. Petermann:
Terraine, Inc. (Terraine) has prepared this letter report to summarize the results of groundwater
monitoring activities at the Former Four Corners Store site located at 6154 West Mount Drive, Rocky Mount, Nash County, North Carolina.
On May 9, 2011, Terraine personnel mobilized to the site to collect groundwater samples from monitoring
wells MW-1, MW-1D, MW-2, MW-3, MW-4, MW-5, MW-6, and MW-7 and water supply well WSW-3 to evaluate current groundwater quality conditions. Water supply well WSW-3 could not be sampled
because the resident was not available. Monitoring wells MW-3 and MW-5 were not sampled for all analyses due to poor recharge. Groundwater elevation data are presented in Table 1. All groundwater
samples were submitted under proper chain of custody control to Pace Analytical Services, Inc., in Huntersville, North Carolina, for chemical analysis. Groundwater analytical data are summarized in Table
2. A complete laboratory report and chain of custody form for all groundwater samples obtained are attached.
Immediately following sampling, Universal Remediation, Inc., PRP® well booms were installed in
monitoring wells MW-1 and MW-5. Well booms contain powdered beeswax, which stimulates rapid biodegradation of dissolved petroleum contaminants.
Should you have any questions regarding any of this information, please contact me at 1-800-531-1242
ext. 706 or [e-mail].
Sincerely,

Karen Baer Project Manager
Terraine, Inc.
Groundwater Monitoring Results – 5/31/2011 Incident # 12610
Former Four Corners Store Page 2
Rocky Mount, NC Nash County
Attachments: Table 1: Summary of Groundwater Elevation Data
Table 2: Summary of Groundwater Analytical Results
Site Photographs
Laboratory Report(s)
5/13/2007 1.75 98.25
02/23/2010 0.90 99.10
10/6/2010 1.99 98.01
5/9/2011 1.84 98.16
5/13/2007 2.36 97.66
02/23/2010 0.15 99.87
10/06/2010 6.72 93.30
05/09/2011 9.90 90.12
5/13/2007 1.88 97.36
10/6/2010 2.07 97.17
5/9/2011 2.39 96.85
5/13/2007 2.22 97.82
02/23/2010 2.53 97.51
10/06/2010 1.84 98.20
05/09/2011 1.31 98.73
5/13/2007 2.47 98.49
10/6/2010 2.75 98.21
5/9/2011 2.70 98.26
5/13/2007 2.97 96.91
10/6/2010 4.73 95.15
5/9/2011 3.31 96.57
10/6/2010 2.25 98.74
5/9/2011 2.83 98.16
10/6/2010 6.34 92.87
5/9/2011 4.63 94.58
14
MW-7 9/15/2010 99.21 4-14 2 14
MW-6 9/15/2010 100.99 4 - 14 2
12
MW-5 5/23/2006 99.88 2 - 12 2 12
MW-4 5/23/2006 100.96 2 - 12 2
MW-3 5/23/2006 100.04 2 - 12 2
MW-2 10/25/2005 99.24 2 - 12 2
10/25/2005 100.00 3 - 13 2
MW-1D 10/25/2005 100.02 40 - 45 2
Units measured in feet unless otherwise noted.
Groundwater elevation measurements based on arbitrary top of casing (TOC) assignment of 100.00 feet for MW-1.
GW - Groundwater
TOTAL
DEPTH
INSTALL
DATEWELL ID
NCDENR Incident No. 12610
TOC
ELEVATION
SCREEN
INTERVAL
WELL
DIAMETER
(INCHES)
WELL
GAUGE
DATE
DEPTH TO
WATER
FROM TOC
GW
ELEVATION
13
45
12
12
MW-1
Nash County
Table 1Summary of Groundwater Elevation Data
Former Four Corners Store
6154 West Mount Drive
Rocky Mount, NC
Well ID Sample Date BenzeneTolueneEthylbenzeneXylenesMTBEIPEEDBNaphthalene 1,2,3-Trichlorobenzene1,2,4-Trimethylbenzene1,2-Dichloroethane1,3,5-TrimethylbenzeneBromomethaneChloromethaneIsopropylbenzene Methylene chloride n-Butylbenzenen-Propylbenzenesec-Butylbenzenetrans-1,3-Dichloropropene 3,3'-DichlorobenzidineBenzo(a)pyreneBenzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluoranthene bis(2-Ethylhexyl)phthalateDibenz(a,h)anthracene2-MethylnaphthaleneC5-C8 AliphaticsC9-C12 AliphaticsC9-18 AliphaticsC9-C18 Total AlphaticsC19-C36 AliphaticsC9-C10 AromaticsC11-C22 AromaticsC9-C22 Total AromaticsLead2/1/2006 1,600 1,500 1,900 6,100 ND ND ND 680 ND 2,400 ND 680 ND ND 100 ND ND 230 ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/24/2006 1,700 1,800 2,600 6,800 ND 100 ND 820 ND 2,400 ND 660 ND ND 120 ND ND 250 ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
9/7/2006 1,400 980 2,500 6,300 ND 65 ND 890 ND 2,500 ND 690 ND ND 130 ND ND 290 ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/22/2007 2,000 1,800 2,800 7,520 ND ND ND 920 ND 2,500 ND 750 ND ND 160 ND ND 360 ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
11/2/2007 1,540 1,710 2,520 8,281 ND ND ND 1,020 ND 2,990 ND 727 ND ND ND ND ND 325 ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/13/2008 1,030 3,620 2,810 9,750 ND ND ND 828 ND 2,930 ND 735 ND ND 163 ND ND 389 ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
7/1/2009 1,310 1,930 2,490 7,332 ND ND ND 766 ND 2,400 ND 607 ND ND ND ND 83.8 298 ND ND NA NA NA NA NA NA NA NA 1,510 3,860 NA 3,860 ND 181 NA 181 ND
12/10/2009 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA ND ND NA ND ND ND NA ND ND
2/23/2010 1,320 1,570 2,380 5,824 12 ND ND 706 ND 1,900 ND 524 ND ND 130 ND ND 285 12.6 25.7 ND ND ND ND ND ND ND ND 15,400 34,900 NA 34,900 ND 5,950 NA 5,950 5.0
10/6/2010 892 1,700 2,540 8,020 ND ND ND*1,200 57.2 3,530 ND*982 ND ND*133 55.0 ND 405 ND ND*ND ND*ND*ND ND ND*ND*199 13,100 81,600 945 82,545 ND 10,000 1,630 11,630 15.7
5/9/2011 990 2,480 2,390 8,070 ND ND ND*1,020 ††ND 2,500 ND*685 ND ND*94.7 ND 89.5 323 ND ND*28.8 J 18.8 J 15.3 J 17.2 J 16.7 J 124 14.6 J 785 18,100 79,500 4,200 83,700 ND 388 2,780 3,168 16.6
2/1/2006 ND 0.6 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/24/2006 260 14 94 120 2.7 2.8 ND 34 ND 140 5.0 8.3 ND ND 9.4 ND ND 11 ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
9/7/2006 ND ND ND ND 2.5 2.4 ND ND ND ND ND ND ND 12 ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/22/2007 ND 1.1 ND 0.31 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
11/2/2007 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/13/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
7/1/2009 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA ND ND NA ND ND ND NA ND ND
2/23/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA ND ND NA ND ND ND NA ND ND
10/6/2010 ND ND ND ND ND ND ND*ND ND ND ND*ND ND ND ND ND ND ND ND ND*ND ND*ND*ND ND ND*ND*ND ND ND ND ND ND ND ND ND 7.5
5/9/2011 523 20.5 184 336.7 10.4 4.3 ND*82.2 †ND 98.3 10.6 1.6 ND ND 18.0 ND ND 29.3 ND ND*ND ND ND ND ND 5.7 J ND 22.2 2,680 5,720 ND 5,720 ND 902 132 1,034 29.3
2/1/2006 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/24/2006 ND ND ND 1.1 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
9/7/2006 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/22/2007 ND ND ND ND ND ND ND .65 J ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
11/2/2007 ND ND ND ND 0.8 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/13/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
7/1/2009 NS NS NS NS NS NS NS NS NS NS NS NS ND NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/6/2010 ND ND ND ND ND ND ND*ND ND ND ND*ND ND ND ND ND ND ND ND ND*ND ND*ND*ND ND ND*ND*ND ND ND ND ND ND ND ND ND 11.8
5/9/2011 ND ND ND ND ND ND ND*ND ND 1.0 ND*ND ND ND ND ND ND ND ND ND*ND ND*ND*ND ND ND ND*ND ND ND ND ND ND ND ND ND 19.7
5/24/2006 1.9 ND ND ND 6.9 ND ND ND ND ND ND ND ND 7.7 ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
9/7/2006 ND ND ND ND 7.6 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/22/2007 0.34 J ND ND ND 12 1.8 ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
11/2/2007 ND ND ND ND 9.3 0.9 ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/13/2008 ND ND ND ND 3.2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
7/1/2009 ND ND ND ND 5 3.2 ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA ND ND NA ND ND ND NA ND 37.4
2/23/2010 ND ND ND ND 1.8 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA ND ND NA ND ND ND NA ND ND
10/6/2010 ND ND ND ND 0.57 ND ND*ND ND ND ND*ND ND ND ND ND ND ND ND ND*ND ND*ND*ND ND ND*ND*ND NA NA ND NA NA NA ND NA 32.3
5/9/2011 ND ND ND ND 0.59 ND ND*ND ND ND ND*ND ND ND ND ND ND ND ND ND*NA NA NA NA NA NA NA NA ND ND NA ND ND ND NA ND 75.1
5/24/2006 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
9/7/2006 ND ND ND ND ND ND ND ND ND ND ND ND ND 7.1 ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/22/2007 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
11/2/2007 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/13/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
7/1/2009 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA ND ND NA ND ND ND NA ND 64.5
10/6/2010 ND ND ND ND ND ND ND*ND ND ND ND*ND ND ND ND ND ND ND ND ND*ND ND*ND*ND ND ND*ND*ND ND ND ND ND ND ND ND ND 41.0
5/9/2011 ND ND ND ND ND ND ND*ND ND ND ND*ND ND ND ND ND ND ND ND ND*ND ND*ND*ND ND ND ND*ND ND ND ND ND ND ND ND ND 109
1 600 600 500 20 70 0.02 6 NE 400 0.4 400 NE 3 70 5 70 70 70 0.4 NE 0.005 0.05 200 0.5 3 0.005 30 400 NE NE 700 10,000 NE NE 200 15
5,000 260,000 84,500 85,500 20,000 70,000 50 6,000 NE 28,500 400 25,000 NE 3,000 25,000 5,000 6,900 30,000 8,500 400 NE 0.81 0.75 200 0.5 170 1.2 12,500 NE NE NE NE NE NE NE NE 15,000
All results expressed in µg/L (ppb)Values shown in bold, italicized, yellow highlighted font indicate concentrations that exceed the 2L Standards
ND - None Detected (below method detection limit)MADEP - Massachusetts Department of Environmental Protection
ND * - None Detected (method detection limit above the 2L Standard)VPH - Volatile Petroleum Hydrocarbons
NE - No Standard Established EPH - Extractable Petroleum Hydrocarbons
NA - Not Analyzed J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MTBE - Methyl tert-butyl ether † - By Method 6200B
IPE - Diisopropyl ether †† - By Method 625
EDB - 1,2-Dibromoethane NS - Not Sampled
MW-1
MW-1D
MW-2
MW-3
Table 2
MADEP VPH & EPH
Nash County
Rocky Mount, NC
6154 West Mount Drive
Former Four Corners Store
Summary of Groundwater Analytical Results
NCDENR Incident No. 12610
MW-4
15A NCAC 2L.0202 (2L) Standard
Gross Contamination Level (GCL)
Well ID Sample Date BenzeneTolueneEthylbenzeneXylenesMTBEIPEEDBNaphthalene 1,2,3-Trichlorobenzene1,2,4-Trimethylbenzene1,2-Dichloroethane1,3,5-TrimethylbenzeneBromomethaneChloromethaneIsopropylbenzene Methylene chloride n-Butylbenzenen-Propylbenzenesec-Butylbenzenetrans-1,3-Dichloropropene 3,3'-DichlorobenzidineBenzo(a)pyreneBenzo(b)fluorantheneBenzo(g,h,i)peryleneBenzo(k)fluoranthene bis(2-Ethylhexyl)phthalateDibenz(a,h)anthracene2-MethylnaphthaleneC5-C8 AliphaticsC9-C12 AliphaticsC9-18 AliphaticsC9-C18 Total AlphaticsC19-C36 AliphaticsC9-C10 AromaticsC11-C22 AromaticsC9-C22 Total AromaticsLead5/24/2006 14 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
9/7/2006 ND ND ND ND 15 ND ND ND ND ND ND ND ND 6.1 ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/22/2007 0.7 ND ND ND 10 0.7 ND ND ND ND 1.6 ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
11/2/2007 ND ND ND ND 6.8 0.8 ND ND ND ND 3.0 ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/13/2008 ND ND ND ND 11.5 ND ND ND ND ND 0.98 ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
7/1/2009 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
10/6/2010 ND ND ND ND 9.8 ND ND*ND ND ND 0.64 ND ND ND ND ND ND ND ND ND*ND ND*ND*ND ND*ND ND*ND NA NA ND NA NA NA ND NA NA
5/9/2011 ND ND ND ND 8.0 ND ND*ND ND ND ND ND ND ND ND ND ND ND ND ND*NA NA NA NA NA NA NA NA ND ND ND ND ND ND ND ND NA
10/6/2010 ND ND ND ND ND ND ND*ND ND ND ND*ND ND ND ND ND ND ND ND ND*ND ND*ND*ND ND*ND ND*ND ND ND ND ND ND ND ND ND 84.5
5/9/2011 ND ND ND ND ND ND ND*ND ND ND ND*ND ND ND ND ND ND ND ND ND*ND ND*ND*ND ND ND ND*ND ND ND ND ND ND ND ND ND 28.5
10/6/2010 ND ND ND ND ND ND ND*ND ND ND ND*ND ND ND ND ND ND ND ND ND*ND ND*ND*ND ND*ND ND*ND ND ND ND ND ND ND ND ND 78.1
5/9/2011 ND ND ND ND ND ND ND*ND ND ND ND*ND ND ND ND ND ND ND ND ND*ND ND*ND*ND ND*ND ND*ND ND ND ND ND ND ND ND ND 28.6
2/1/2006 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/24/2006 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
9/7/2006 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
11/7/2006 NS NS NS NS NS NS NS NS ND NS NS NS ND NS NS ND NS NS ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/22/2007 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
11/2/2007 NS NS NS NS NS NS NS NS ND NS NS NS ND NS NS ND NS NS ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/13/2008 NS NS NS NS NS NS NS NS ND NS NS NS ND NS NS ND NS NS ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
7/1/2009 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
2/23/2010 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA ND ND NA ND ND ND NA ND ND
10/6/2010 ND ND ND ND ND ND ND*ND ND ND ND*ND ND ND ND ND ND ND ND ND*ND ND*ND*ND ND*ND ND*ND ND ND ND ND ND ND ND ND ND
2/1/2006 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/24/2006 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
9/7/2006 ND ND ND ND ND ND ND ND ND ND ND ND ND 14 ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
11/7/2006 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/22/2007 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
11/2/2007 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/13/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
7/1/2009 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA ND ND NA ND ND ND NA ND ND
10/6/2010 ND ND ND ND ND ND ND*ND ND ND ND*ND ND ND ND ND ND ND ND ND*ND ND*ND*ND ND*ND ND*ND ND ND ND ND ND ND ND ND ND
2/1/2006 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/24/2006 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
9/7/2006 ND ND ND ND ND ND ND ND ND ND ND ND ND 5.4 ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
11/7/2006 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/22/2007 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
11/2/2007 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
5/13/2008 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA
7/1/2009 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA ND ND NA ND ND ND NA ND ND
2/23/2010 ND ND ND ND ND ND ND ND ND ND ND ND 1.3 J ND ND ND ND ND ND ND NA NA NA NA NA NA NA NA ND ND NA ND ND ND NA ND 12.3
10/6/2010 ND ND ND ND ND ND ND*ND ND ND ND*ND ND ND ND ND ND ND ND ND*ND ND*ND*ND ND*ND ND*ND ND ND ND ND ND ND ND ND 24.3
5/9/2011 NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS NS
1 600 600 500 20 70 0.02 6 NE 400 0.4 400 NE 3 70 5 70 70 70 0.4 NE 0.005 0.05 200 0.5 3 0.005 30 400 NE NE 700 10,000 NE NE 200 15
5,000 260,000 84,500 85,500 20,000 70,000 50 6,000 NE 28,500 400 25,000 NE 3,000 25,000 5,000 6,900 30,000 8,500 400 NE 0.81 0.75 200 0.5 170 1.2 12,500 NE NE NE NE NE NE NE NE 15,000
All results expressed in µg/L (ppb)Values shown in bold, italicized, yellow highlighted font indicate concentrations that exceed the 2L Standards
ND - None Detected (below method detection limit)MADEP - Massachusetts Department of Environmental Protection
ND * - None Detected (method detection limit above the 2L Standard)VPH - Volatile Petroleum Hydrocarbons
NE - No Standard Established EPH - Extractable Petroleum Hydrocarbons
NA - Not Analyzed J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MTBE - Methyl tert-butyl ether † - By Method 6200B
IPE - Diisopropyl ether †† - By Method 625
EDB - 1,2-Dibromoethane NS - Not Sampled
NCDENR Incident No. 12610
Gross Contamination Level (GCL)
MW-5
WSW-1
WSW-2
WSW-3
MW-6
MW-7
MADEP VPH & EPH
15A NCAC 2L.0202 (2L) Standard
Nash County
Rocky Mount, NC
Table 2 (continued)
Summary of Groundwater Analytical Results
Former Four Corners Store
6154 West Mount Drive
Site Photographs
Former Four Corners Store
6154 West Mount Drive
Rocky Mount, NC
Nash County
NCDENR Incident # 12610
View of the Former Four Corners Store, facing northwest.1 of 4
Abandoned building at Claude's ConstUuction. Monitoring wells MW-1
and MW-1D are near puddle to left of canopy.
2 of 4
Site Photographs
Former Four Corners Store
6154 West Mount Drive
Rocky Mount, NC
Nash County
NCDENR Incident # 12610
Fenced-in area of Claude's Construction.3 of 4
View of water supply well WSW-2, facing west.4 of 4
May 23, 2011
LIMS USE: FR - LINDA BLALOCK
LIMS OBJECT ID: 9293852
9293852
Project:
Pace Project No.:
RE:
Ms. Linda BlalockNCDENR - UST Section1637 Mail Service CenterRaleigh, NC 276991637
12610 FMR FOUR CORNERS STORE
Dear Ms. Blalock:
Enclosed are the analytical results for sample(s) received by the laboratory on May 10, 2011. The
results relate only to the samples included in this report. Results reported herein conform to themost current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Brandon Helton forRenee Spencer
[e-mail] Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
CERTIFICATIONS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078Louisiana/LELAP Certification #: 04034New Jersey Certification #: NC012North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12Pennsylvania Certification #: 68-00784South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003Virginia Certification #: 00213Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84Louisiana DHH Drinking Water # LA 100031West Virginia Certification #: 357
Asheville Certification IDs2225 Riverside Dr., Asheville, NC 28804Connecticut Certification #: PH-0106Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030New Jersey Certification #: NC011North Carolina Bioassay Certification #: 9North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40Pennsylvania Certification #: 68-03578South Carolina Bioassay Certification #: 99030002South Carolina Certification #: 99030001Virginia Certification #: 00072West Virginia Certification #: 356
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE SUMMARY
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Lab ID Sample ID Matrix Date Collected Date Received
9293852001 MW-1 Water 05/09/11 11:00 05/10/11 17:25
9293852002 MW-1D Water 05/09/11 10:45 05/10/11 17:25
9293852003 MW-2 Water 05/09/11 09:45 05/10/11 17:25
9293852004 MW-4 Water 05/09/11 11:20 05/10/11 17:25
9293852005 MW-6 Water 05/09/11 13:00 05/10/11 17:25
9293852006 MW-7 Water 05/09/11 12:30 05/10/11 17:25
9293852007 MW-3 Water 05/09/11 11:50 05/10/11 17:25
9293852008 MW-5 Water 05/09/11 09:15 05/10/11 17:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
9293852001 MW-1 MADEP EPH 7 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-AJMW
EPA 625 59 PASI-CBPJ
SM 6200B 64 PASI-CTLS
9293852002 MW-1D MADEP EPH 7 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-AJMW
EPA 625 59 PASI-CBPJ
SM 6200B 64 PASI-CTLS
9293852003 MW-2 MADEP EPH 7 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-AJMW
EPA 625 59 PASI-CBPJ
SM 6200B 64 PASI-CTLS
9293852004 MW-4 MADEP EPH 7 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-AJMW
EPA 625 59 PASI-CBPJ
SM 6200B 64 PASI-CTLS
9293852005 MW-6 MADEP EPH 7 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-AJMW
EPA 625 59 PASI-CBPJ
SM 6200B 64 PASI-CTLS
9293852006 MW-7 MADEP EPH 7 PASI-CRES
MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-AJMW
EPA 625 59 PASI-CBPJ
SM 6200B 64 PASI-CTLS
9293852007 MW-3 MADEP VPH 5 PASI-CAW
EPA 200.7 1 PASI-AJMW
SM 6200B 64 PASI-CTLS
9293852008 MW-5 MADEP EPH 7 PASI-CRES
MADEP VPH 5 PASI-CAW
SM 6200B 64 PASI-CTLS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-1 Lab ID:9293852001 Collected:05/09/11 11:00 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)4200 ug/L 5 05/17/11 09:19 N205/15/11 05:40538538
Aliphatic (C19-C36)ND ug/L 5 05/17/11 09:19 N205/15/11 05:40538538
Aromatic (C11-C22)2780 ug/L 2 05/17/11 09:19 N205/15/11 05:40215215
Nonatriacontane (S)0 %5 05/17/11 09:19 7194-86-7 S405/15/11 05:4040-140
o-Terphenyl (S)64 %2 05/17/11 09:19 84-15-105/15/11 05:4040-140
2-Fluorobiphenyl (S)118 %2 05/17/11 09:19 321-60-805/15/11 05:4040-140
2-Bromonaphthalene (S)128 %2 05/17/11 09:19 580-13-205/15/11 05:4040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)18100 ug/L 20 05/20/11 19:38 N2,NC600300
Aliphatic (C09-C12)79500 ug/L 20 05/20/11 19:38 N2,NC600300
Aromatic (C09-C10)388 ug/L 1 05/20/11 19:38 N2,NC30.0 15.0
2,5-Dibromotoluene (PID)(S)121 %1 05/20/11 19:3870-130
2,5-Dibromotoluene (FID)(S)125 %20 05/20/11 19:3870-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead 16.6 ug/L 1 05/11/11 22:16 7439-92-105/11/11 12:155.0 4.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 10 05/20/11 11:12 83-32-905/16/11 14:0058.1 2.9
Acenaphthylene ND ug/L 10 05/20/11 11:12 208-96-805/16/11 14:0058.1 2.4
Anthracene ND ug/L 10 05/20/11 11:12 120-12-705/16/11 14:0058.1 1.6
Benzo(a)anthracene ND ug/L 10 05/20/11 11:12 56-55-305/16/11 14:0058.1 3.8
Benzo(a)pyrene 18.8J ug/L 10 05/20/11 11:12 50-32-805/16/11 14:0058.1 3.5
Benzo(b)fluoranthene 15.3J ug/L 10 05/20/11 11:12 205-99-205/16/11 14:0058.1 3.3
Benzo(g,h,i)perylene 17.2J ug/L 10 05/20/11 11:12 191-24-205/16/11 14:0058.1 4.4
Benzo(k)fluoranthene 16.7J ug/L 10 05/20/11 11:12 207-08-905/16/11 14:0058.1 5.0
4-Bromophenylphenyl ether ND ug/L 10 05/20/11 11:12 101-55-305/16/11 14:0058.1 9.5
Butylbenzylphthalate ND ug/L 10 05/20/11 11:12 85-68-705/16/11 14:0058.1 9.2
4-Chloro-3-methylphenol ND ug/L 10 05/20/11 11:12 59-50-705/16/11 14:0058.1 43.0
bis(2-Chloroethoxy)methane ND ug/L 10 05/20/11 11:12 111-91-105/16/11 14:0011610.7
bis(2-Chloroethyl) ether ND ug/L 10 05/20/11 11:12 111-44-405/16/11 14:0058.1 11.6
bis(2-Chloroisopropyl) ether ND ug/L 10 05/20/11 11:12 108-60-105/16/11 14:0058.1 11.0
2-Chloronaphthalene ND ug/L 10 05/20/11 11:12 91-58-705/16/11 14:0058.1 11.4
2-Chlorophenol ND ug/L 10 05/20/11 11:12 95-57-805/16/11 14:0058.1 15.1
4-Chlorophenylphenyl ether ND ug/L 10 05/20/11 11:12 7005-72-305/16/11 14:0058.1 10.1
Chrysene ND ug/L 10 05/20/11 11:12 218-01-905/16/11 14:0058.1 2.4
Dibenz(a,h)anthracene 14.6J ug/L 10 05/20/11 11:12 53-70-305/16/11 14:0058.1 6.4
3,3'-Dichlorobenzidine 28.8J ug/L 10 05/20/11 11:12 91-94-105/16/11 14:0029124.4
2,4-Dichlorophenol ND ug/L 10 05/20/11 11:12 120-83-205/16/11 14:0058.1 19.8
Diethylphthalate ND ug/L 10 05/20/11 11:12 84-66-205/16/11 14:0058.1 6.7
2,4-Dimethylphenol ND ug/L 10 05/20/11 11:12 105-67-905/16/11 14:0011614.0
Dimethylphthalate ND ug/L 10 05/20/11 11:12 131-11-305/16/11 14:0058.1 8.8
Di-n-butylphthalate ND ug/L 10 05/20/11 11:12 84-74-205/16/11 14:0058.1 8.7
4,6-Dinitro-2-methylphenol ND ug/L 10 05/20/11 11:12 534-52-105/16/11 14:0023330.2
2,4-Dinitrophenol ND ug/L 10 05/20/11 11:12 51-28-505/16/11 14:00581105
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 5 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-1 Lab ID:9293852001 Collected:05/09/11 11:00 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
2,4-Dinitrotoluene ND ug/L 10 05/20/11 11:12 121-14-205/16/11 14:0058.1 10.5
2,6-Dinitrotoluene ND ug/L 10 05/20/11 11:12 606-20-205/16/11 14:0058.1 11.4
Di-n-octylphthalate ND ug/L 10 05/20/11 11:12 117-84-005/16/11 14:0058.1 7.7
bis(2-Ethylhexyl)phthalate 124 ug/L 10 05/20/11 11:12 117-81-705/16/11 14:0058.1 9.2
Fluoranthene ND ug/L 10 05/20/11 11:12 206-44-005/16/11 14:0058.1 2.4
Fluorene ND ug/L 10 05/20/11 11:12 86-73-705/16/11 14:0058.1 2.4
Hexachloro-1,3-butadiene ND ug/L 10 05/20/11 11:12 87-68-305/16/11 14:0058.1 10.9
Hexachlorobenzene ND ug/L 10 05/20/11 11:12 118-74-105/16/11 14:0058.1 8.4
Hexachlorocyclopentadiene ND ug/L 10 05/20/11 11:12 77-47-405/16/11 14:0011610.2
Hexachloroethane ND ug/L 10 05/20/11 11:12 67-72-105/16/11 14:0058.1 12.8
Indeno(1,2,3-cd)pyrene ND ug/L 10 05/20/11 11:12 193-39-505/16/11 14:0058.1 3.4
Isophorone ND ug/L 10 05/20/11 11:12 78-59-105/16/11 14:0011610.3
2-Methylnaphthalene 785 ug/L 10 05/20/11 11:12 91-57-605/16/11 14:0058.1 3.3
Naphthalene 1020 ug/L 10 05/20/11 11:12 91-20-305/16/11 14:0058.1 4.0
Nitrobenzene ND ug/L 10 05/20/11 11:12 98-95-305/16/11 14:0058.1 12.8
2-Nitrophenol ND ug/L 10 05/20/11 11:12 88-75-505/16/11 14:0058.1 10.6
4-Nitrophenol ND ug/L 10 05/20/11 11:12 100-02-705/16/11 14:0058147.7
N-Nitrosodimethylamine ND ug/L 10 05/20/11 11:12 62-75-905/16/11 14:0058.1 10.6
N-Nitroso-di-n-propylamine ND ug/L 10 05/20/11 11:12 621-64-705/16/11 14:0058.1 11.5
N-Nitrosodiphenylamine ND ug/L 10 05/20/11 11:12 86-30-605/16/11 14:0011611.6
Pentachlorophenol ND ug/L 10 05/20/11 11:12 87-86-505/16/11 14:0029153.5
Phenanthrene ND ug/L 10 05/20/11 11:12 85-01-805/16/11 14:0058.1 2.6
Phenol ND ug/L 10 05/20/11 11:12 108-95-205/16/11 14:0058.1 22.1
Pyrene ND ug/L 10 05/20/11 11:12 129-00-005/16/11 14:0058.1 2.2
1,2,4-Trichlorobenzene ND ug/L 10 05/20/11 11:12 120-82-1 D305/16/11 14:0058.1 11.4
2,4,6-Trichlorophenol ND ug/L 10 05/20/11 11:12 88-06-205/16/11 14:0011615.1
Nitrobenzene-d5 (S)0 %10 05/20/11 11:12 4165-60-0 S405/16/11 14:0010-120
2-Fluorobiphenyl (S)0 %10 05/20/11 11:12 321-60-805/16/11 14:0015-120
Terphenyl-d14 (S)0 %10 05/20/11 11:12 1718-51-005/16/11 14:0011-131
Phenol-d6 (S)0 %10 05/20/11 11:12 13127-88-305/16/11 14:0010-120
2-Fluorophenol (S)0 %10 05/20/11 11:12 367-12-405/16/11 14:0010-120
2,4,6-Tribromophenol (S)0 %10 05/20/11 11:12 118-79-605/16/11 14:0010-137
6200B MSV Analytical Method: SM 6200B
Benzene 990 ug/L 25 05/17/11 02:13 71-43-212.5 12.5
Bromobenzene ND ug/L 25 05/17/11 02:13 108-86-112.5 12.5
Bromochloromethane ND ug/L 25 05/17/11 02:13 74-97-512.5 12.5
Bromodichloromethane ND ug/L 25 05/17/11 02:13 75-27-412.5 12.5
Bromoform ND ug/L 25 05/17/11 02:13 75-25-212.5 12.5
Bromomethane ND ug/L 25 05/17/11 02:13 74-83-912525.0
n-Butylbenzene 89.5 ug/L 25 05/17/11 02:13 104-51-812.5 12.5
sec-Butylbenzene ND ug/L 25 05/17/11 02:13 135-98-812.5 12.5
tert-Butylbenzene ND ug/L 25 05/17/11 02:13 98-06-612.5 12.5
Carbon tetrachloride ND ug/L 25 05/17/11 02:13 56-23-512.5 12.5
Chlorobenzene ND ug/L 25 05/17/11 02:13 108-90-712.5 12.5
Chloroethane ND ug/L 25 05/17/11 02:13 75-00-325.0 25.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 6 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-1 Lab ID:9293852001 Collected:05/09/11 11:00 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Chloroform ND ug/L 25 05/17/11 02:13 67-66-312.5 12.5
Chloromethane ND ug/L 25 05/17/11 02:13 74-87-325.0 25.0
2-Chlorotoluene ND ug/L 25 05/17/11 02:13 95-49-812.5 12.5
4-Chlorotoluene ND ug/L 25 05/17/11 02:13 106-43-412.5 12.5
1,2-Dibromo-3-chloropropane ND ug/L 25 05/17/11 02:13 96-12-825.0 25.0
Dibromochloromethane ND ug/L 25 05/17/11 02:13 124-48-112.5 12.5
1,2-Dibromoethane (EDB)ND ug/L 25 05/17/11 02:13 106-93-412.5 12.5
Dibromomethane ND ug/L 25 05/17/11 02:13 74-95-312.5 12.5
1,2-Dichlorobenzene ND ug/L 25 05/17/11 02:13 95-50-112.5 12.5
1,3-Dichlorobenzene ND ug/L 25 05/17/11 02:13 541-73-112.5 12.5
1,4-Dichlorobenzene ND ug/L 25 05/17/11 02:13 106-46-712.5 12.5
Dichlorodifluoromethane ND ug/L 25 05/17/11 02:13 75-71-812.5 12.5
1,1-Dichloroethane ND ug/L 25 05/17/11 02:13 75-34-312.5 12.5
1,2-Dichloroethane ND ug/L 25 05/17/11 02:13 107-06-212.5 12.5
1,1-Dichloroethene ND ug/L 25 05/17/11 02:13 75-35-412.5 12.5
cis-1,2-Dichloroethene ND ug/L 25 05/17/11 02:13 156-59-212.5 12.5
trans-1,2-Dichloroethene ND ug/L 25 05/17/11 02:13 156-60-512.5 12.5
1,2-Dichloropropane ND ug/L 25 05/17/11 02:13 78-87-512.5 12.5
1,3-Dichloropropane ND ug/L 25 05/17/11 02:13 142-28-912.5 12.5
2,2-Dichloropropane ND ug/L 25 05/17/11 02:13 594-20-712.5 12.5
1,1-Dichloropropene ND ug/L 25 05/17/11 02:13 563-58-612.5 12.5
cis-1,3-Dichloropropene ND ug/L 25 05/17/11 02:13 10061-01-512.5 12.5
trans-1,3-Dichloropropene ND ug/L 25 05/17/11 02:13 10061-02-612.5 12.5
Diisopropyl ether ND ug/L 25 05/17/11 02:13 108-20-312.5 12.5
Ethylbenzene 2390 ug/L 25 05/17/11 02:13 100-41-412.5 12.5
Hexachloro-1,3-butadiene ND ug/L 25 05/17/11 02:13 87-68-350.0 50.0
Isopropylbenzene (Cumene)94.7 ug/L 25 05/17/11 02:13 98-82-812.5 12.5
Methylene Chloride ND ug/L 25 05/17/11 02:13 75-09-250.0 50.0
Methyl-tert-butyl ether ND ug/L 25 05/17/11 02:13 1634-04-412.5 12.5
Naphthalene 790 ug/L 25 05/17/11 02:13 91-20-350.0 50.0
n-Propylbenzene 323 ug/L 25 05/17/11 02:13 103-65-112.5 12.5
Styrene ND ug/L 25 05/17/11 02:13 100-42-512.5 12.5
1,1,1,2-Tetrachloroethane ND ug/L 25 05/17/11 02:13 630-20-612.5 12.5
1,1,2,2-Tetrachloroethane ND ug/L 25 05/17/11 02:13 79-34-512.5 12.5
Tetrachloroethene ND ug/L 25 05/17/11 02:13 127-18-412.5 12.5
Toluene 2480 ug/L 25 05/17/11 02:13 108-88-312.5 12.5
1,2,3-Trichlorobenzene ND ug/L 25 05/17/11 02:13 87-61-650.0 50.0
1,2,4-Trichlorobenzene ND ug/L 25 05/17/11 02:13 120-82-150.0 50.0
1,1,1-Trichloroethane ND ug/L 25 05/17/11 02:13 71-55-612.5 12.5
1,1,2-Trichloroethane ND ug/L 25 05/17/11 02:13 79-00-512.5 12.5
Trichloroethene ND ug/L 25 05/17/11 02:13 79-01-612.5 12.5
Trichlorofluoromethane ND ug/L 25 05/17/11 02:13 75-69-425.0 25.0
1,2,3-Trichloropropane ND ug/L 25 05/17/11 02:13 96-18-412.5 12.5
1,2,4-Trimethylbenzene 2500 ug/L 25 05/17/11 02:13 95-63-612.5 12.5
1,3,5-Trimethylbenzene 685 ug/L 25 05/17/11 02:13 108-67-812.5 12.5
Vinyl chloride ND ug/L 25 05/17/11 02:13 75-01-425.0 25.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 7 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-1 Lab ID:9293852001 Collected:05/09/11 11:00 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
m&p-Xylene 7050 ug/L 25 05/17/11 02:13 179601-23-125.0 25.0
o-Xylene 1020 ug/L 25 05/17/11 02:13 95-47-612.5 12.5
1,2-Dichloroethane-d4 (S)103 %25 05/17/11 02:13 17060-07-070-130
Dibromofluoromethane (S)100 %25 05/17/11 02:13 1868-53-770-130
4-Bromofluorobenzene (S)102 %25 05/17/11 02:13 460-00-470-130
Toluene-d8 (S)104 %25 05/17/11 02:13 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 8 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-1D Lab ID:9293852002 Collected:05/09/11 10:45 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 05/17/11 02:34 N205/15/11 05:40115115
Aliphatic (C19-C36)ND ug/L 1 05/17/11 02:34 N205/15/11 05:40115115
Aromatic (C11-C22)132 ug/L 1 05/17/11 02:34 N205/15/11 05:40115115
Nonatriacontane (S)79 %1 05/17/11 02:34 7194-86-705/15/11 05:4040-140
o-Terphenyl (S)56 %1 05/17/11 02:34 84-15-105/15/11 05:4040-140
2-Fluorobiphenyl (S)80 %1 05/17/11 02:34 321-60-805/15/11 05:4040-140
2-Bromonaphthalene (S)89 %1 05/17/11 02:34 580-13-205/15/11 05:4040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)2680 ug/L 10 05/19/11 03:36 N2300150
Aliphatic (C09-C12)5720 ug/L 10 05/19/11 03:36 N2300150
Aromatic (C09-C10)902 ug/L 10 05/19/11 03:36 N2300150
2,5-Dibromotoluene (PID)(S)97 %10 05/19/11 03:3670-130
2,5-Dibromotoluene (FID)(S)101 %10 05/19/11 03:3670-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead 29.3 ug/L 1 05/11/11 22:12 7439-92-105/11/11 12:155.0 4.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 05/19/11 22:48 83-32-905/16/11 14:005.8 0.29
Acenaphthylene ND ug/L 1 05/19/11 22:48 208-96-805/16/11 14:005.8 0.24
Anthracene ND ug/L 1 05/19/11 22:48 120-12-705/16/11 14:005.8 0.16
Benzo(a)anthracene ND ug/L 1 05/19/11 22:48 56-55-305/16/11 14:005.8 0.38
Benzo(a)pyrene ND ug/L 1 05/19/11 22:48 50-32-805/16/11 14:005.8 0.35
Benzo(b)fluoranthene ND ug/L 1 05/19/11 22:48 205-99-205/16/11 14:005.8 0.33
Benzo(g,h,i)perylene ND ug/L 1 05/19/11 22:48 191-24-205/16/11 14:005.8 0.44
Benzo(k)fluoranthene ND ug/L 1 05/19/11 22:48 207-08-905/16/11 14:005.8 0.50
4-Bromophenylphenyl ether ND ug/L 1 05/19/11 22:48 101-55-305/16/11 14:005.8 0.95
Butylbenzylphthalate ND ug/L 1 05/19/11 22:48 85-68-705/16/11 14:005.8 0.92
4-Chloro-3-methylphenol ND ug/L 1 05/19/11 22:48 59-50-705/16/11 14:005.8 4.3
bis(2-Chloroethoxy)methane ND ug/L 1 05/19/11 22:48 111-91-105/16/11 14:0011.6 1.1
bis(2-Chloroethyl) ether ND ug/L 1 05/19/11 22:48 111-44-405/16/11 14:005.8 1.2
bis(2-Chloroisopropyl) ether ND ug/L 1 05/19/11 22:48 108-60-105/16/11 14:005.8 1.1
2-Chloronaphthalene ND ug/L 1 05/19/11 22:48 91-58-705/16/11 14:005.8 1.1
2-Chlorophenol ND ug/L 1 05/19/11 22:48 95-57-805/16/11 14:005.8 1.5
4-Chlorophenylphenyl ether ND ug/L 1 05/19/11 22:48 7005-72-305/16/11 14:005.8 1.0
Chrysene ND ug/L 1 05/19/11 22:48 218-01-905/16/11 14:005.8 0.24
Dibenz(a,h)anthracene ND ug/L 1 05/19/11 22:48 53-70-305/16/11 14:005.8 0.64
3,3'-Dichlorobenzidine ND ug/L 1 05/19/11 22:48 91-94-105/16/11 14:0029.1 2.4
2,4-Dichlorophenol ND ug/L 1 05/19/11 22:48 120-83-205/16/11 14:005.8 2.0
Diethylphthalate ND ug/L 1 05/19/11 22:48 84-66-205/16/11 14:005.8 0.67
2,4-Dimethylphenol ND ug/L 1 05/19/11 22:48 105-67-905/16/11 14:0011.6 1.4
Dimethylphthalate ND ug/L 1 05/19/11 22:48 131-11-305/16/11 14:005.8 0.88
Di-n-butylphthalate ND ug/L 1 05/19/11 22:48 84-74-205/16/11 14:005.8 0.87
4,6-Dinitro-2-methylphenol ND ug/L 1 05/19/11 22:48 534-52-105/16/11 14:0023.3 3.0
2,4-Dinitrophenol ND ug/L 1 05/19/11 22:48 51-28-505/16/11 14:0058.1 10.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 9 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-1D Lab ID:9293852002 Collected:05/09/11 10:45 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
2,4-Dinitrotoluene ND ug/L 1 05/19/11 22:48 121-14-205/16/11 14:005.8 1.0
2,6-Dinitrotoluene ND ug/L 1 05/19/11 22:48 606-20-205/16/11 14:005.8 1.1
Di-n-octylphthalate ND ug/L 1 05/19/11 22:48 117-84-005/16/11 14:005.8 0.77
bis(2-Ethylhexyl)phthalate 5.7J ug/L 1 05/19/11 22:48 117-81-705/16/11 14:005.8 0.92
Fluoranthene ND ug/L 1 05/19/11 22:48 206-44-005/16/11 14:005.8 0.24
Fluorene ND ug/L 1 05/19/11 22:48 86-73-705/16/11 14:005.8 0.24
Hexachloro-1,3-butadiene ND ug/L 1 05/19/11 22:48 87-68-305/16/11 14:005.8 1.1
Hexachlorobenzene ND ug/L 1 05/19/11 22:48 118-74-105/16/11 14:005.8 0.84
Hexachlorocyclopentadiene ND ug/L 1 05/19/11 22:48 77-47-405/16/11 14:0011.6 1.0
Hexachloroethane ND ug/L 1 05/19/11 22:48 67-72-105/16/11 14:005.8 1.3
Indeno(1,2,3-cd)pyrene ND ug/L 1 05/19/11 22:48 193-39-505/16/11 14:005.8 0.34
Isophorone ND ug/L 1 05/19/11 22:48 78-59-105/16/11 14:0011.6 1.0
2-Methylnaphthalene 22.2 ug/L 1 05/19/11 22:48 91-57-605/16/11 14:005.8 0.33
Naphthalene 53.6 ug/L 1 05/19/11 22:48 91-20-305/16/11 14:005.8 0.40
Nitrobenzene ND ug/L 1 05/19/11 22:48 98-95-305/16/11 14:005.8 1.3
2-Nitrophenol ND ug/L 1 05/19/11 22:48 88-75-505/16/11 14:005.8 1.1
4-Nitrophenol ND ug/L 1 05/19/11 22:48 100-02-705/16/11 14:0058.1 4.8
N-Nitrosodimethylamine ND ug/L 1 05/19/11 22:48 62-75-905/16/11 14:005.8 1.1
N-Nitroso-di-n-propylamine ND ug/L 1 05/19/11 22:48 621-64-705/16/11 14:005.8 1.2
N-Nitrosodiphenylamine ND ug/L 1 05/19/11 22:48 86-30-605/16/11 14:0011.6 1.2
Pentachlorophenol ND ug/L 1 05/19/11 22:48 87-86-505/16/11 14:0029.1 5.3
Phenanthrene ND ug/L 1 05/19/11 22:48 85-01-805/16/11 14:005.8 0.26
Phenol ND ug/L 1 05/19/11 22:48 108-95-205/16/11 14:005.8 2.2
Pyrene ND ug/L 1 05/19/11 22:48 129-00-005/16/11 14:005.8 0.22
1,2,4-Trichlorobenzene ND ug/L 1 05/19/11 22:48 120-82-105/16/11 14:005.8 1.1
2,4,6-Trichlorophenol ND ug/L 1 05/19/11 22:48 88-06-205/16/11 14:0011.6 1.5
Nitrobenzene-d5 (S)64 %1 05/19/11 22:48 4165-60-005/16/11 14:0010-120
2-Fluorobiphenyl (S)65 %1 05/19/11 22:48 321-60-805/16/11 14:0015-120
Terphenyl-d14 (S)96 %1 05/19/11 22:48 1718-51-005/16/11 14:0011-131
Phenol-d6 (S)24 %1 05/19/11 22:48 13127-88-305/16/11 14:0010-120
2-Fluorophenol (S)40 %1 05/19/11 22:48 367-12-405/16/11 14:0010-120
2,4,6-Tribromophenol (S)73 %1 05/19/11 22:48 118-79-605/16/11 14:0010-137
6200B MSV Analytical Method: SM 6200B
Benzene 523 ug/L 5 05/17/11 06:02 71-43-22.5 2.5
Bromobenzene ND ug/L 1 05/15/11 16:18 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 05/15/11 16:18 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 05/15/11 16:18 75-27-40.50 0.50
Bromoform ND ug/L 1 05/15/11 16:18 75-25-20.50 0.50
Bromomethane ND ug/L 1 05/15/11 16:18 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 05/15/11 16:18 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 05/15/11 16:18 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 05/15/11 16:18 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 05/15/11 16:18 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 05/15/11 16:18 108-90-70.50 0.50
Chloroethane ND ug/L 1 05/15/11 16:18 75-00-31.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 10 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-1D Lab ID:9293852002 Collected:05/09/11 10:45 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Chloroform ND ug/L 1 05/15/11 16:18 67-66-30.50 0.50
Chloromethane ND ug/L 1 05/15/11 16:18 74-87-31.0 1.0
2-Chlorotoluene ND ug/L 1 05/15/11 16:18 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 05/15/11 16:18 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 05/15/11 16:18 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 05/15/11 16:18 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 05/15/11 16:18 106-93-40.50 0.50
Dibromomethane ND ug/L 1 05/15/11 16:18 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 05/15/11 16:18 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 05/15/11 16:18 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 05/15/11 16:18 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 05/15/11 16:18 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 05/15/11 16:18 75-34-30.50 0.50
1,2-Dichloroethane 10.6 ug/L 1 05/15/11 16:18 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 05/15/11 16:18 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 05/15/11 16:18 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 05/15/11 16:18 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 05/15/11 16:18 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 05/15/11 16:18 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 05/15/11 16:18 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 05/15/11 16:18 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 05/15/11 16:18 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 05/15/11 16:18 10061-02-60.50 0.50
Diisopropyl ether 4.3 ug/L 1 05/15/11 16:18 108-20-30.50 0.50
Ethylbenzene 184 ug/L 1 05/15/11 16:18 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 05/15/11 16:18 87-68-32.0 2.0
Isopropylbenzene (Cumene)18.0 ug/L 1 05/15/11 16:18 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 05/15/11 16:18 75-09-22.0 2.0
Methyl-tert-butyl ether 10.4 ug/L 1 05/15/11 16:18 1634-04-40.50 0.50
Naphthalene 82.2 ug/L 1 05/15/11 16:18 91-20-32.0 2.0
n-Propylbenzene 29.3 ug/L 1 05/15/11 16:18 103-65-10.50 0.50
Styrene ND ug/L 1 05/15/11 16:18 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 05/15/11 16:18 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 05/15/11 16:18 79-34-50.50 0.50
Tetrachloroethene ND ug/L 1 05/15/11 16:18 127-18-40.50 0.50
Toluene 20.5 ug/L 1 05/15/11 16:18 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 05/15/11 16:18 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 05/15/11 16:18 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 05/15/11 16:18 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 05/15/11 16:18 79-00-50.50 0.50
Trichloroethene ND ug/L 1 05/15/11 16:18 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 05/15/11 16:18 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 05/15/11 16:18 96-18-40.50 0.50
1,2,4-Trimethylbenzene 98.3 ug/L 1 05/15/11 16:18 95-63-60.50 0.50
1,3,5-Trimethylbenzene 1.6 ug/L 1 05/15/11 16:18 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 05/15/11 16:18 75-01-41.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 11 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-1D Lab ID:9293852002 Collected:05/09/11 10:45 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
m&p-Xylene 333 ug/L 1 05/15/11 16:18 179601-23-11.0 1.0
o-Xylene 3.7 ug/L 1 05/15/11 16:18 95-47-60.50 0.50
1,2-Dichloroethane-d4 (S)104 %1 05/15/11 16:18 17060-07-070-130
Dibromofluoromethane (S)101 %1 05/15/11 16:18 1868-53-770-130
4-Bromofluorobenzene (S)103 %1 05/15/11 16:18 460-00-470-130
Toluene-d8 (S)107 %1 05/15/11 16:18 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 12 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-2 Lab ID:9293852003 Collected:05/09/11 09:45 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 05/17/11 03:10 N205/15/11 05:40110110
Aliphatic (C19-C36)ND ug/L 1 05/17/11 03:10 N205/15/11 05:40110110
Aromatic (C11-C22)ND ug/L 1 05/17/11 03:10 N205/15/11 05:40110110
Nonatriacontane (S)81 %1 05/17/11 03:10 7194-86-705/15/11 05:4040-140
o-Terphenyl (S)60 %1 05/17/11 03:10 84-15-105/15/11 05:4040-140
2-Fluorobiphenyl (S)76 %1 05/17/11 03:10 321-60-805/15/11 05:4040-140
2-Bromonaphthalene (S)82 %1 05/17/11 03:10 580-13-205/15/11 05:4040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 05/19/11 04:26 N230.0 15.0
Aliphatic (C09-C12)ND ug/L 1 05/19/11 04:26 N230.0 15.0
Aromatic (C09-C10)ND ug/L 1 05/19/11 04:26 N230.0 15.0
2,5-Dibromotoluene (PID)(S)99 %1 05/19/11 04:2670-130
2,5-Dibromotoluene (FID)(S)94 %1 05/19/11 04:2670-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead 19.7 ug/L 1 05/11/11 22:09 7439-92-105/11/11 12:155.0 4.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 05/19/11 23:16 83-32-905/16/11 14:005.8 0.29
Acenaphthylene ND ug/L 1 05/19/11 23:16 208-96-805/16/11 14:005.8 0.24
Anthracene ND ug/L 1 05/19/11 23:16 120-12-705/16/11 14:005.8 0.16
Benzo(a)anthracene ND ug/L 1 05/19/11 23:16 56-55-305/16/11 14:005.8 0.38
Benzo(a)pyrene ND ug/L 1 05/19/11 23:16 50-32-805/16/11 14:005.8 0.35
Benzo(b)fluoranthene ND ug/L 1 05/19/11 23:16 205-99-205/16/11 14:005.8 0.33
Benzo(g,h,i)perylene ND ug/L 1 05/19/11 23:16 191-24-205/16/11 14:005.8 0.44
Benzo(k)fluoranthene ND ug/L 1 05/19/11 23:16 207-08-905/16/11 14:005.8 0.50
4-Bromophenylphenyl ether ND ug/L 1 05/19/11 23:16 101-55-305/16/11 14:005.8 0.95
Butylbenzylphthalate ND ug/L 1 05/19/11 23:16 85-68-705/16/11 14:005.8 0.92
4-Chloro-3-methylphenol ND ug/L 1 05/19/11 23:16 59-50-705/16/11 14:005.8 4.3
bis(2-Chloroethoxy)methane ND ug/L 1 05/19/11 23:16 111-91-105/16/11 14:0011.6 1.1
bis(2-Chloroethyl) ether ND ug/L 1 05/19/11 23:16 111-44-405/16/11 14:005.8 1.2
bis(2-Chloroisopropyl) ether ND ug/L 1 05/19/11 23:16 108-60-105/16/11 14:005.8 1.1
2-Chloronaphthalene ND ug/L 1 05/19/11 23:16 91-58-705/16/11 14:005.8 1.1
2-Chlorophenol ND ug/L 1 05/19/11 23:16 95-57-805/16/11 14:005.8 1.5
4-Chlorophenylphenyl ether ND ug/L 1 05/19/11 23:16 7005-72-305/16/11 14:005.8 1.0
Chrysene ND ug/L 1 05/19/11 23:16 218-01-905/16/11 14:005.8 0.24
Dibenz(a,h)anthracene ND ug/L 1 05/19/11 23:16 53-70-305/16/11 14:005.8 0.64
3,3'-Dichlorobenzidine ND ug/L 1 05/19/11 23:16 91-94-105/16/11 14:0029.1 2.4
2,4-Dichlorophenol ND ug/L 1 05/19/11 23:16 120-83-205/16/11 14:005.8 2.0
Diethylphthalate ND ug/L 1 05/19/11 23:16 84-66-205/16/11 14:005.8 0.67
2,4-Dimethylphenol ND ug/L 1 05/19/11 23:16 105-67-905/16/11 14:0011.6 1.4
Dimethylphthalate ND ug/L 1 05/19/11 23:16 131-11-305/16/11 14:005.8 0.88
Di-n-butylphthalate ND ug/L 1 05/19/11 23:16 84-74-205/16/11 14:005.8 0.87
4,6-Dinitro-2-methylphenol ND ug/L 1 05/19/11 23:16 534-52-105/16/11 14:0023.3 3.0
2,4-Dinitrophenol ND ug/L 1 05/19/11 23:16 51-28-505/16/11 14:0058.1 10.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 13 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-2 Lab ID:9293852003 Collected:05/09/11 09:45 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
2,4-Dinitrotoluene ND ug/L 1 05/19/11 23:16 121-14-205/16/11 14:005.8 1.0
2,6-Dinitrotoluene ND ug/L 1 05/19/11 23:16 606-20-205/16/11 14:005.8 1.1
Di-n-octylphthalate ND ug/L 1 05/19/11 23:16 117-84-005/16/11 14:005.8 0.77
bis(2-Ethylhexyl)phthalate ND ug/L 1 05/19/11 23:16 117-81-705/16/11 14:005.8 0.92
Fluoranthene ND ug/L 1 05/19/11 23:16 206-44-005/16/11 14:005.8 0.24
Fluorene ND ug/L 1 05/19/11 23:16 86-73-705/16/11 14:005.8 0.24
Hexachloro-1,3-butadiene ND ug/L 1 05/19/11 23:16 87-68-305/16/11 14:005.8 1.1
Hexachlorobenzene ND ug/L 1 05/19/11 23:16 118-74-105/16/11 14:005.8 0.84
Hexachlorocyclopentadiene ND ug/L 1 05/19/11 23:16 77-47-405/16/11 14:0011.6 1.0
Hexachloroethane ND ug/L 1 05/19/11 23:16 67-72-105/16/11 14:005.8 1.3
Indeno(1,2,3-cd)pyrene ND ug/L 1 05/19/11 23:16 193-39-505/16/11 14:005.8 0.34
Isophorone ND ug/L 1 05/19/11 23:16 78-59-105/16/11 14:0011.6 1.0
2-Methylnaphthalene ND ug/L 1 05/19/11 23:16 91-57-605/16/11 14:005.8 0.33
Naphthalene ND ug/L 1 05/19/11 23:16 91-20-305/16/11 14:005.8 0.40
Nitrobenzene ND ug/L 1 05/19/11 23:16 98-95-305/16/11 14:005.8 1.3
2-Nitrophenol ND ug/L 1 05/19/11 23:16 88-75-505/16/11 14:005.8 1.1
4-Nitrophenol ND ug/L 1 05/19/11 23:16 100-02-705/16/11 14:0058.1 4.8
N-Nitrosodimethylamine ND ug/L 1 05/19/11 23:16 62-75-905/16/11 14:005.8 1.1
N-Nitroso-di-n-propylamine ND ug/L 1 05/19/11 23:16 621-64-705/16/11 14:005.8 1.2
N-Nitrosodiphenylamine ND ug/L 1 05/19/11 23:16 86-30-605/16/11 14:0011.6 1.2
Pentachlorophenol ND ug/L 1 05/19/11 23:16 87-86-505/16/11 14:0029.1 5.3
Phenanthrene ND ug/L 1 05/19/11 23:16 85-01-805/16/11 14:005.8 0.26
Phenol ND ug/L 1 05/19/11 23:16 108-95-205/16/11 14:005.8 2.2
Pyrene ND ug/L 1 05/19/11 23:16 129-00-005/16/11 14:005.8 0.22
1,2,4-Trichlorobenzene ND ug/L 1 05/19/11 23:16 120-82-105/16/11 14:005.8 1.1
2,4,6-Trichlorophenol ND ug/L 1 05/19/11 23:16 88-06-205/16/11 14:0011.6 1.5
Nitrobenzene-d5 (S)66 %1 05/19/11 23:16 4165-60-005/16/11 14:0010-120
2-Fluorobiphenyl (S)70 %1 05/19/11 23:16 321-60-805/16/11 14:0015-120
Terphenyl-d14 (S)99 %1 05/19/11 23:16 1718-51-005/16/11 14:0011-131
Phenol-d6 (S)22 %1 05/19/11 23:16 13127-88-305/16/11 14:0010-120
2-Fluorophenol (S)38 %1 05/19/11 23:16 367-12-405/16/11 14:0010-120
2,4,6-Tribromophenol (S)64 %1 05/19/11 23:16 118-79-605/16/11 14:0010-137
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 05/15/11 16:41 71-43-20.50 0.50
Bromobenzene ND ug/L 1 05/15/11 16:41 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 05/15/11 16:41 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 05/15/11 16:41 75-27-40.50 0.50
Bromoform ND ug/L 1 05/15/11 16:41 75-25-20.50 0.50
Bromomethane ND ug/L 1 05/15/11 16:41 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 05/15/11 16:41 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 05/15/11 16:41 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 05/15/11 16:41 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 05/15/11 16:41 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 05/15/11 16:41 108-90-70.50 0.50
Chloroethane ND ug/L 1 05/15/11 16:41 75-00-31.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 14 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-2 Lab ID:9293852003 Collected:05/09/11 09:45 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Chloroform ND ug/L 1 05/15/11 16:41 67-66-30.50 0.50
Chloromethane ND ug/L 1 05/15/11 16:41 74-87-31.0 1.0
2-Chlorotoluene ND ug/L 1 05/15/11 16:41 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 05/15/11 16:41 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 05/15/11 16:41 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 05/15/11 16:41 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 05/15/11 16:41 106-93-40.50 0.50
Dibromomethane ND ug/L 1 05/15/11 16:41 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 05/15/11 16:41 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 05/15/11 16:41 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 05/15/11 16:41 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 05/15/11 16:41 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 05/15/11 16:41 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 05/15/11 16:41 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 05/15/11 16:41 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 05/15/11 16:41 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 05/15/11 16:41 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 05/15/11 16:41 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 05/15/11 16:41 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 05/15/11 16:41 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 05/15/11 16:41 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 05/15/11 16:41 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 05/15/11 16:41 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 05/15/11 16:41 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 05/15/11 16:41 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 05/15/11 16:41 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 05/15/11 16:41 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 05/15/11 16:41 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 05/15/11 16:41 1634-04-40.50 0.50
Naphthalene ND ug/L 1 05/15/11 16:41 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 05/15/11 16:41 103-65-10.50 0.50
Styrene ND ug/L 1 05/15/11 16:41 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 05/15/11 16:41 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 05/15/11 16:41 79-34-50.50 0.50
Tetrachloroethene ND ug/L 1 05/15/11 16:41 127-18-40.50 0.50
Toluene ND ug/L 1 05/15/11 16:41 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 05/15/11 16:41 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 05/15/11 16:41 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 05/15/11 16:41 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 05/15/11 16:41 79-00-50.50 0.50
Trichloroethene ND ug/L 1 05/15/11 16:41 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 05/15/11 16:41 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 05/15/11 16:41 96-18-40.50 0.50
1,2,4-Trimethylbenzene 1.0 ug/L 1 05/15/11 16:41 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 05/15/11 16:41 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 05/15/11 16:41 75-01-41.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 15 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-2 Lab ID:9293852003 Collected:05/09/11 09:45 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
m&p-Xylene ND ug/L 1 05/15/11 16:41 179601-23-11.0 1.0
o-Xylene ND ug/L 1 05/15/11 16:41 95-47-60.50 0.50
1,2-Dichloroethane-d4 (S)102 %1 05/15/11 16:41 17060-07-070-130
Dibromofluoromethane (S)99 %1 05/15/11 16:41 1868-53-770-130
4-Bromofluorobenzene (S)97 %1 05/15/11 16:41 460-00-470-130
Toluene-d8 (S)94 %1 05/15/11 16:41 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 16 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-4 Lab ID:9293852004 Collected:05/09/11 11:20 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 05/17/11 03:46 N205/15/11 05:40119119
Aliphatic (C19-C36)ND ug/L 1 05/17/11 03:46 N205/15/11 05:40119119
Aromatic (C11-C22)ND ug/L 1 05/17/11 03:46 N205/15/11 05:40119119
Nonatriacontane (S)61 %1 05/17/11 03:46 7194-86-705/15/11 05:4040-140
o-Terphenyl (S)56 %1 05/17/11 03:46 84-15-105/15/11 05:4040-140
2-Fluorobiphenyl (S)70 %1 05/17/11 03:46 321-60-805/15/11 05:4040-140
2-Bromonaphthalene (S)76 %1 05/17/11 03:46 580-13-205/15/11 05:4040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 05/17/11 07:27 N230.0 15.0
Aliphatic (C09-C12)ND ug/L 1 05/17/11 07:27 N230.0 15.0
Aromatic (C09-C10)ND ug/L 1 05/17/11 07:27 N230.0 15.0
2,5-Dibromotoluene (PID)(S)95 %1 05/17/11 07:2770-130
2,5-Dibromotoluene (FID)(S)92 %1 05/17/11 07:2770-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead 109 ug/L 1 05/11/11 22:20 7439-92-105/11/11 12:155.0 4.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 05/19/11 23:43 83-32-905/16/11 14:005.7 0.28
Acenaphthylene ND ug/L 1 05/19/11 23:43 208-96-805/16/11 14:005.7 0.24
Anthracene ND ug/L 1 05/19/11 23:43 120-12-705/16/11 14:005.7 0.16
Benzo(a)anthracene ND ug/L 1 05/19/11 23:43 56-55-305/16/11 14:005.7 0.38
Benzo(a)pyrene ND ug/L 1 05/19/11 23:43 50-32-805/16/11 14:005.7 0.34
Benzo(b)fluoranthene ND ug/L 1 05/19/11 23:43 205-99-205/16/11 14:005.7 0.32
Benzo(g,h,i)perylene ND ug/L 1 05/19/11 23:43 191-24-205/16/11 14:005.7 0.43
Benzo(k)fluoranthene ND ug/L 1 05/19/11 23:43 207-08-905/16/11 14:005.7 0.49
4-Bromophenylphenyl ether ND ug/L 1 05/19/11 23:43 101-55-305/16/11 14:005.7 0.93
Butylbenzylphthalate ND ug/L 1 05/19/11 23:43 85-68-705/16/11 14:005.7 0.90
4-Chloro-3-methylphenol ND ug/L 1 05/19/11 23:43 59-50-705/16/11 14:005.7 4.2
bis(2-Chloroethoxy)methane ND ug/L 1 05/19/11 23:43 111-91-105/16/11 14:0011.4 1.0
bis(2-Chloroethyl) ether ND ug/L 1 05/19/11 23:43 111-44-405/16/11 14:005.7 1.1
bis(2-Chloroisopropyl) ether ND ug/L 1 05/19/11 23:43 108-60-105/16/11 14:005.7 1.1
2-Chloronaphthalene ND ug/L 1 05/19/11 23:43 91-58-705/16/11 14:005.7 1.1
2-Chlorophenol ND ug/L 1 05/19/11 23:43 95-57-805/16/11 14:005.7 1.5
4-Chlorophenylphenyl ether ND ug/L 1 05/19/11 23:43 7005-72-305/16/11 14:005.7 0.99
Chrysene ND ug/L 1 05/19/11 23:43 218-01-905/16/11 14:005.7 0.24
Dibenz(a,h)anthracene ND ug/L 1 05/19/11 23:43 53-70-305/16/11 14:005.7 0.63
3,3'-Dichlorobenzidine ND ug/L 1 05/19/11 23:43 91-94-105/16/11 14:0028.4 2.4
2,4-Dichlorophenol ND ug/L 1 05/19/11 23:43 120-83-205/16/11 14:005.7 1.9
Diethylphthalate ND ug/L 1 05/19/11 23:43 84-66-205/16/11 14:005.7 0.66
2,4-Dimethylphenol ND ug/L 1 05/19/11 23:43 105-67-905/16/11 14:0011.4 1.4
Dimethylphthalate ND ug/L 1 05/19/11 23:43 131-11-305/16/11 14:005.7 0.86
Di-n-butylphthalate ND ug/L 1 05/19/11 23:43 84-74-205/16/11 14:005.7 0.85
4,6-Dinitro-2-methylphenol ND ug/L 1 05/19/11 23:43 534-52-105/16/11 14:0022.7 3.0
2,4-Dinitrophenol ND ug/L 1 05/19/11 23:43 51-28-505/16/11 14:0056.8 10.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 17 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-4 Lab ID:9293852004 Collected:05/09/11 11:20 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
2,4-Dinitrotoluene ND ug/L 1 05/19/11 23:43 121-14-205/16/11 14:005.7 1.0
2,6-Dinitrotoluene ND ug/L 1 05/19/11 23:43 606-20-205/16/11 14:005.7 1.1
Di-n-octylphthalate ND ug/L 1 05/19/11 23:43 117-84-005/16/11 14:005.7 0.75
bis(2-Ethylhexyl)phthalate ND ug/L 1 05/19/11 23:43 117-81-705/16/11 14:005.7 0.90
Fluoranthene ND ug/L 1 05/19/11 23:43 206-44-005/16/11 14:005.7 0.24
Fluorene ND ug/L 1 05/19/11 23:43 86-73-705/16/11 14:005.7 0.24
Hexachloro-1,3-butadiene ND ug/L 1 05/19/11 23:43 87-68-305/16/11 14:005.7 1.1
Hexachlorobenzene ND ug/L 1 05/19/11 23:43 118-74-105/16/11 14:005.7 0.82
Hexachlorocyclopentadiene ND ug/L 1 05/19/11 23:43 77-47-405/16/11 14:0011.4 1.0
Hexachloroethane ND ug/L 1 05/19/11 23:43 67-72-105/16/11 14:005.7 1.2
Indeno(1,2,3-cd)pyrene ND ug/L 1 05/19/11 23:43 193-39-505/16/11 14:005.7 0.33
Isophorone ND ug/L 1 05/19/11 23:43 78-59-105/16/11 14:0011.4 1.0
2-Methylnaphthalene ND ug/L 1 05/19/11 23:43 91-57-605/16/11 14:005.7 0.32
Naphthalene ND ug/L 1 05/19/11 23:43 91-20-305/16/11 14:005.7 0.39
Nitrobenzene ND ug/L 1 05/19/11 23:43 98-95-305/16/11 14:005.7 1.2
2-Nitrophenol ND ug/L 1 05/19/11 23:43 88-75-505/16/11 14:005.7 1.0
4-Nitrophenol ND ug/L 1 05/19/11 23:43 100-02-705/16/11 14:0056.8 4.7
N-Nitrosodimethylamine ND ug/L 1 05/19/11 23:43 62-75-905/16/11 14:005.7 1.0
N-Nitroso-di-n-propylamine ND ug/L 1 05/19/11 23:43 621-64-705/16/11 14:005.7 1.1
N-Nitrosodiphenylamine ND ug/L 1 05/19/11 23:43 86-30-605/16/11 14:0011.4 1.1
Pentachlorophenol ND ug/L 1 05/19/11 23:43 87-86-505/16/11 14:0028.4 5.2
Phenanthrene ND ug/L 1 05/19/11 23:43 85-01-805/16/11 14:005.7 0.25
Phenol ND ug/L 1 05/19/11 23:43 108-95-205/16/11 14:005.7 2.2
Pyrene ND ug/L 1 05/19/11 23:43 129-00-005/16/11 14:005.7 0.22
1,2,4-Trichlorobenzene ND ug/L 1 05/19/11 23:43 120-82-105/16/11 14:005.7 1.1
2,4,6-Trichlorophenol ND ug/L 1 05/19/11 23:43 88-06-205/16/11 14:0011.4 1.5
Nitrobenzene-d5 (S)61 %1 05/19/11 23:43 4165-60-005/16/11 14:0010-120
2-Fluorobiphenyl (S)67 %1 05/19/11 23:43 321-60-805/16/11 14:0015-120
Terphenyl-d14 (S)91 %1 05/19/11 23:43 1718-51-005/16/11 14:0011-131
Phenol-d6 (S)24 %1 05/19/11 23:43 13127-88-305/16/11 14:0010-120
2-Fluorophenol (S)40 %1 05/19/11 23:43 367-12-405/16/11 14:0010-120
2,4,6-Tribromophenol (S)62 %1 05/19/11 23:43 118-79-605/16/11 14:0010-137
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 05/15/11 17:04 71-43-20.50 0.50
Bromobenzene ND ug/L 1 05/15/11 17:04 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 05/15/11 17:04 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 05/15/11 17:04 75-27-40.50 0.50
Bromoform ND ug/L 1 05/15/11 17:04 75-25-20.50 0.50
Bromomethane ND ug/L 1 05/15/11 17:04 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 05/15/11 17:04 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 05/15/11 17:04 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 05/15/11 17:04 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 05/15/11 17:04 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 05/15/11 17:04 108-90-70.50 0.50
Chloroethane ND ug/L 1 05/15/11 17:04 75-00-31.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 18 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-4 Lab ID:9293852004 Collected:05/09/11 11:20 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Chloroform ND ug/L 1 05/15/11 17:04 67-66-30.50 0.50
Chloromethane ND ug/L 1 05/15/11 17:04 74-87-31.0 1.0
2-Chlorotoluene ND ug/L 1 05/15/11 17:04 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 05/15/11 17:04 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 05/15/11 17:04 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 05/15/11 17:04 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 05/15/11 17:04 106-93-40.50 0.50
Dibromomethane ND ug/L 1 05/15/11 17:04 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 05/15/11 17:04 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 05/15/11 17:04 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 05/15/11 17:04 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 05/15/11 17:04 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 05/15/11 17:04 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 05/15/11 17:04 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 05/15/11 17:04 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 05/15/11 17:04 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 05/15/11 17:04 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 05/15/11 17:04 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 05/15/11 17:04 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 05/15/11 17:04 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 05/15/11 17:04 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 05/15/11 17:04 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 05/15/11 17:04 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 05/15/11 17:04 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 05/15/11 17:04 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 05/15/11 17:04 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 05/15/11 17:04 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 05/15/11 17:04 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 05/15/11 17:04 1634-04-40.50 0.50
Naphthalene ND ug/L 1 05/15/11 17:04 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 05/15/11 17:04 103-65-10.50 0.50
Styrene ND ug/L 1 05/15/11 17:04 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 05/15/11 17:04 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 05/15/11 17:04 79-34-50.50 0.50
Tetrachloroethene ND ug/L 1 05/15/11 17:04 127-18-40.50 0.50
Toluene ND ug/L 1 05/15/11 17:04 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 05/15/11 17:04 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 05/15/11 17:04 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 05/15/11 17:04 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 05/15/11 17:04 79-00-50.50 0.50
Trichloroethene ND ug/L 1 05/15/11 17:04 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 05/15/11 17:04 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 05/15/11 17:04 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 05/15/11 17:04 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 05/15/11 17:04 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 05/15/11 17:04 75-01-41.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 19 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-4 Lab ID:9293852004 Collected:05/09/11 11:20 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
m&p-Xylene ND ug/L 1 05/15/11 17:04 179601-23-11.0 1.0
o-Xylene ND ug/L 1 05/15/11 17:04 95-47-60.50 0.50
1,2-Dichloroethane-d4 (S)106 %1 05/15/11 17:04 17060-07-070-130
Dibromofluoromethane (S)101 %1 05/15/11 17:04 1868-53-770-130
4-Bromofluorobenzene (S)96 %1 05/15/11 17:04 460-00-470-130
Toluene-d8 (S)94 %1 05/15/11 17:04 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 20 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-6 Lab ID:9293852005 Collected:05/09/11 13:00 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 05/17/11 04:22 N205/15/11 05:40118118
Aliphatic (C19-C36)ND ug/L 1 05/17/11 04:22 N205/15/11 05:40118118
Aromatic (C11-C22)ND ug/L 1 05/17/11 04:22 N205/15/11 05:40118118
Nonatriacontane (S)55 %1 05/17/11 04:22 7194-86-705/15/11 05:4040-140
o-Terphenyl (S)54 %1 05/17/11 04:22 84-15-105/15/11 05:4040-140
2-Fluorobiphenyl (S)80 %1 05/17/11 04:22 321-60-805/15/11 05:4040-140
2-Bromonaphthalene (S)85 %1 05/17/11 04:22 580-13-205/15/11 05:4040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 05/19/11 04:50 N230.0 15.0
Aliphatic (C09-C12)ND ug/L 1 05/19/11 04:50 N230.0 15.0
Aromatic (C09-C10)ND ug/L 1 05/19/11 04:50 N230.0 15.0
2,5-Dibromotoluene (PID)(S)92 %1 05/19/11 04:5070-130
2,5-Dibromotoluene (FID)(S)91 %1 05/19/11 04:5070-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead 28.5 ug/L 1 05/12/11 11:45 7439-92-105/11/11 12:155.0 4.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 05/20/11 00:11 83-32-905/16/11 14:005.7 0.28
Acenaphthylene ND ug/L 1 05/20/11 00:11 208-96-805/16/11 14:005.7 0.24
Anthracene ND ug/L 1 05/20/11 00:11 120-12-705/16/11 14:005.7 0.16
Benzo(a)anthracene ND ug/L 1 05/20/11 00:11 56-55-305/16/11 14:005.7 0.38
Benzo(a)pyrene ND ug/L 1 05/20/11 00:11 50-32-805/16/11 14:005.7 0.34
Benzo(b)fluoranthene ND ug/L 1 05/20/11 00:11 205-99-205/16/11 14:005.7 0.32
Benzo(g,h,i)perylene ND ug/L 1 05/20/11 00:11 191-24-205/16/11 14:005.7 0.43
Benzo(k)fluoranthene ND ug/L 1 05/20/11 00:11 207-08-905/16/11 14:005.7 0.49
4-Bromophenylphenyl ether ND ug/L 1 05/20/11 00:11 101-55-305/16/11 14:005.7 0.93
Butylbenzylphthalate ND ug/L 1 05/20/11 00:11 85-68-705/16/11 14:005.7 0.90
4-Chloro-3-methylphenol ND ug/L 1 05/20/11 00:11 59-50-705/16/11 14:005.7 4.2
bis(2-Chloroethoxy)methane ND ug/L 1 05/20/11 00:11 111-91-105/16/11 14:0011.4 1.0
bis(2-Chloroethyl) ether ND ug/L 1 05/20/11 00:11 111-44-405/16/11 14:005.7 1.1
bis(2-Chloroisopropyl) ether ND ug/L 1 05/20/11 00:11 108-60-105/16/11 14:005.7 1.1
2-Chloronaphthalene ND ug/L 1 05/20/11 00:11 91-58-705/16/11 14:005.7 1.1
2-Chlorophenol ND ug/L 1 05/20/11 00:11 95-57-805/16/11 14:005.7 1.5
4-Chlorophenylphenyl ether ND ug/L 1 05/20/11 00:11 7005-72-305/16/11 14:005.7 0.99
Chrysene ND ug/L 1 05/20/11 00:11 218-01-905/16/11 14:005.7 0.24
Dibenz(a,h)anthracene ND ug/L 1 05/20/11 00:11 53-70-305/16/11 14:005.7 0.63
3,3'-Dichlorobenzidine ND ug/L 1 05/20/11 00:11 91-94-105/16/11 14:0028.4 2.4
2,4-Dichlorophenol ND ug/L 1 05/20/11 00:11 120-83-205/16/11 14:005.7 1.9
Diethylphthalate ND ug/L 1 05/20/11 00:11 84-66-205/16/11 14:005.7 0.66
2,4-Dimethylphenol ND ug/L 1 05/20/11 00:11 105-67-905/16/11 14:0011.4 1.4
Dimethylphthalate ND ug/L 1 05/20/11 00:11 131-11-305/16/11 14:005.7 0.86
Di-n-butylphthalate ND ug/L 1 05/20/11 00:11 84-74-205/16/11 14:005.7 0.85
4,6-Dinitro-2-methylphenol ND ug/L 1 05/20/11 00:11 534-52-105/16/11 14:0022.7 3.0
2,4-Dinitrophenol ND ug/L 1 05/20/11 00:11 51-28-505/16/11 14:0056.8 10.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 21 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-6 Lab ID:9293852005 Collected:05/09/11 13:00 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
2,4-Dinitrotoluene ND ug/L 1 05/20/11 00:11 121-14-205/16/11 14:005.7 1.0
2,6-Dinitrotoluene ND ug/L 1 05/20/11 00:11 606-20-205/16/11 14:005.7 1.1
Di-n-octylphthalate ND ug/L 1 05/20/11 00:11 117-84-005/16/11 14:005.7 0.75
bis(2-Ethylhexyl)phthalate ND ug/L 1 05/20/11 00:11 117-81-705/16/11 14:005.7 0.90
Fluoranthene ND ug/L 1 05/20/11 00:11 206-44-005/16/11 14:005.7 0.24
Fluorene ND ug/L 1 05/20/11 00:11 86-73-705/16/11 14:005.7 0.24
Hexachloro-1,3-butadiene ND ug/L 1 05/20/11 00:11 87-68-305/16/11 14:005.7 1.1
Hexachlorobenzene ND ug/L 1 05/20/11 00:11 118-74-105/16/11 14:005.7 0.82
Hexachlorocyclopentadiene ND ug/L 1 05/20/11 00:11 77-47-405/16/11 14:0011.4 1.0
Hexachloroethane ND ug/L 1 05/20/11 00:11 67-72-105/16/11 14:005.7 1.2
Indeno(1,2,3-cd)pyrene ND ug/L 1 05/20/11 00:11 193-39-505/16/11 14:005.7 0.33
Isophorone ND ug/L 1 05/20/11 00:11 78-59-105/16/11 14:0011.4 1.0
2-Methylnaphthalene ND ug/L 1 05/20/11 00:11 91-57-605/16/11 14:005.7 0.32
Naphthalene ND ug/L 1 05/20/11 00:11 91-20-305/16/11 14:005.7 0.39
Nitrobenzene ND ug/L 1 05/20/11 00:11 98-95-305/16/11 14:005.7 1.2
2-Nitrophenol ND ug/L 1 05/20/11 00:11 88-75-505/16/11 14:005.7 1.0
4-Nitrophenol ND ug/L 1 05/20/11 00:11 100-02-705/16/11 14:0056.8 4.7
N-Nitrosodimethylamine ND ug/L 1 05/20/11 00:11 62-75-905/16/11 14:005.7 1.0
N-Nitroso-di-n-propylamine ND ug/L 1 05/20/11 00:11 621-64-705/16/11 14:005.7 1.1
N-Nitrosodiphenylamine ND ug/L 1 05/20/11 00:11 86-30-605/16/11 14:0011.4 1.1
Pentachlorophenol ND ug/L 1 05/20/11 00:11 87-86-505/16/11 14:0028.4 5.2
Phenanthrene ND ug/L 1 05/20/11 00:11 85-01-805/16/11 14:005.7 0.25
Phenol ND ug/L 1 05/20/11 00:11 108-95-205/16/11 14:005.7 2.2
Pyrene ND ug/L 1 05/20/11 00:11 129-00-005/16/11 14:005.7 0.22
1,2,4-Trichlorobenzene ND ug/L 1 05/20/11 00:11 120-82-105/16/11 14:005.7 1.1
2,4,6-Trichlorophenol ND ug/L 1 05/20/11 00:11 88-06-205/16/11 14:0011.4 1.5
Nitrobenzene-d5 (S)73 %1 05/20/11 00:11 4165-60-005/16/11 14:0010-120
2-Fluorobiphenyl (S)78 %1 05/20/11 00:11 321-60-805/16/11 14:0015-120
Terphenyl-d14 (S)98 %1 05/20/11 00:11 1718-51-005/16/11 14:0011-131
Phenol-d6 (S)25 %1 05/20/11 00:11 13127-88-305/16/11 14:0010-120
2-Fluorophenol (S)45 %1 05/20/11 00:11 367-12-405/16/11 14:0010-120
2,4,6-Tribromophenol (S)64 %1 05/20/11 00:11 118-79-605/16/11 14:0010-137
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 05/15/11 17:27 71-43-20.50 0.50
Bromobenzene ND ug/L 1 05/15/11 17:27 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 05/15/11 17:27 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 05/15/11 17:27 75-27-40.50 0.50
Bromoform ND ug/L 1 05/15/11 17:27 75-25-20.50 0.50
Bromomethane ND ug/L 1 05/15/11 17:27 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 05/15/11 17:27 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 05/15/11 17:27 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 05/15/11 17:27 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 05/15/11 17:27 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 05/15/11 17:27 108-90-70.50 0.50
Chloroethane ND ug/L 1 05/15/11 17:27 75-00-31.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 22 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-6 Lab ID:9293852005 Collected:05/09/11 13:00 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Chloroform ND ug/L 1 05/15/11 17:27 67-66-30.50 0.50
Chloromethane ND ug/L 1 05/15/11 17:27 74-87-31.0 1.0
2-Chlorotoluene ND ug/L 1 05/15/11 17:27 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 05/15/11 17:27 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 05/15/11 17:27 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 05/15/11 17:27 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 05/15/11 17:27 106-93-40.50 0.50
Dibromomethane ND ug/L 1 05/15/11 17:27 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 05/15/11 17:27 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 05/15/11 17:27 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 05/15/11 17:27 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 05/15/11 17:27 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 05/15/11 17:27 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 05/15/11 17:27 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 05/15/11 17:27 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 05/15/11 17:27 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 05/15/11 17:27 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 05/15/11 17:27 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 05/15/11 17:27 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 05/15/11 17:27 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 05/15/11 17:27 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 05/15/11 17:27 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 05/15/11 17:27 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 05/15/11 17:27 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 05/15/11 17:27 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 05/15/11 17:27 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 05/15/11 17:27 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 05/15/11 17:27 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 05/15/11 17:27 1634-04-40.50 0.50
Naphthalene ND ug/L 1 05/15/11 17:27 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 05/15/11 17:27 103-65-10.50 0.50
Styrene ND ug/L 1 05/15/11 17:27 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 05/15/11 17:27 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 05/15/11 17:27 79-34-50.50 0.50
Tetrachloroethene ND ug/L 1 05/15/11 17:27 127-18-40.50 0.50
Toluene ND ug/L 1 05/15/11 17:27 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 05/15/11 17:27 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 05/15/11 17:27 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 05/15/11 17:27 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 05/15/11 17:27 79-00-50.50 0.50
Trichloroethene ND ug/L 1 05/15/11 17:27 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 05/15/11 17:27 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 05/15/11 17:27 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 05/15/11 17:27 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 05/15/11 17:27 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 05/15/11 17:27 75-01-41.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 23 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-6 Lab ID:9293852005 Collected:05/09/11 13:00 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
m&p-Xylene ND ug/L 1 05/15/11 17:27 179601-23-11.0 1.0
o-Xylene ND ug/L 1 05/15/11 17:27 95-47-60.50 0.50
1,2-Dichloroethane-d4 (S)108 %1 05/15/11 17:27 17060-07-070-130
Dibromofluoromethane (S)105 %1 05/15/11 17:27 1868-53-770-130
4-Bromofluorobenzene (S)96 %1 05/15/11 17:27 460-00-470-130
Toluene-d8 (S)93 %1 05/15/11 17:27 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 24 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-7 Lab ID:9293852006 Collected:05/09/11 12:30 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 05/17/11 04:58 N205/15/11 05:40118118
Aliphatic (C19-C36)ND ug/L 1 05/17/11 04:58 N205/15/11 05:40118118
Aromatic (C11-C22)ND ug/L 1 05/17/11 04:58 N205/15/11 05:40118118
Nonatriacontane (S)78 %1 05/17/11 04:58 7194-86-705/15/11 05:4040-140
o-Terphenyl (S)60 %1 05/17/11 04:58 84-15-105/15/11 05:4040-140
2-Fluorobiphenyl (S)82 %1 05/17/11 04:58 321-60-805/15/11 05:4040-140
2-Bromonaphthalene (S)88 %1 05/17/11 04:58 580-13-205/15/11 05:4040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 05/19/11 05:15 N230.0 15.0
Aliphatic (C09-C12)ND ug/L 1 05/19/11 05:15 N230.0 15.0
Aromatic (C09-C10)ND ug/L 1 05/19/11 05:15 N230.0 15.0
2,5-Dibromotoluene (PID)(S)87 %1 05/19/11 05:1570-130
2,5-Dibromotoluene (FID)(S)85 %1 05/19/11 05:1570-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead 28.6 ug/L 1 05/11/11 22:49 7439-92-105/11/11 12:155.0 4.0
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
Acenaphthene ND ug/L 1 05/20/11 00:39 83-32-905/16/11 14:006.0 0.30
Acenaphthylene ND ug/L 1 05/20/11 00:39 208-96-805/16/11 14:006.0 0.25
Anthracene ND ug/L 1 05/20/11 00:39 120-12-705/16/11 14:006.0 0.17
Benzo(a)anthracene ND ug/L 1 05/20/11 00:39 56-55-305/16/11 14:006.0 0.39
Benzo(a)pyrene ND ug/L 1 05/20/11 00:39 50-32-805/16/11 14:006.0 0.36
Benzo(b)fluoranthene ND ug/L 1 05/20/11 00:39 205-99-205/16/11 14:006.0 0.33
Benzo(g,h,i)perylene ND ug/L 1 05/20/11 00:39 191-24-205/16/11 14:006.0 0.45
Benzo(k)fluoranthene ND ug/L 1 05/20/11 00:39 207-08-905/16/11 14:006.0 0.51
4-Bromophenylphenyl ether ND ug/L 1 05/20/11 00:39 101-55-305/16/11 14:006.0 0.98
Butylbenzylphthalate ND ug/L 1 05/20/11 00:39 85-68-705/16/11 14:006.0 0.94
4-Chloro-3-methylphenol ND ug/L 1 05/20/11 00:39 59-50-705/16/11 14:006.0 4.4
bis(2-Chloroethoxy)methane ND ug/L 1 05/20/11 00:39 111-91-105/16/11 14:0011.9 1.1
bis(2-Chloroethyl) ether ND ug/L 1 05/20/11 00:39 111-44-405/16/11 14:006.0 1.2
bis(2-Chloroisopropyl) ether ND ug/L 1 05/20/11 00:39 108-60-105/16/11 14:006.0 1.1
2-Chloronaphthalene ND ug/L 1 05/20/11 00:39 91-58-705/16/11 14:006.0 1.2
2-Chlorophenol ND ug/L 1 05/20/11 00:39 95-57-805/16/11 14:006.0 1.5
4-Chlorophenylphenyl ether ND ug/L 1 05/20/11 00:39 7005-72-305/16/11 14:006.0 1.0
Chrysene ND ug/L 1 05/20/11 00:39 218-01-905/16/11 14:006.0 0.25
Dibenz(a,h)anthracene ND ug/L 1 05/20/11 00:39 53-70-305/16/11 14:006.0 0.65
3,3'-Dichlorobenzidine ND ug/L 1 05/20/11 00:39 91-94-105/16/11 14:0029.8 2.5
2,4-Dichlorophenol ND ug/L 1 05/20/11 00:39 120-83-205/16/11 14:006.0 2.0
Diethylphthalate ND ug/L 1 05/20/11 00:39 84-66-205/16/11 14:006.0 0.69
2,4-Dimethylphenol ND ug/L 1 05/20/11 00:39 105-67-905/16/11 14:0011.9 1.4
Dimethylphthalate ND ug/L 1 05/20/11 00:39 131-11-305/16/11 14:006.0 0.90
Di-n-butylphthalate ND ug/L 1 05/20/11 00:39 84-74-205/16/11 14:006.0 0.89
4,6-Dinitro-2-methylphenol ND ug/L 1 05/20/11 00:39 534-52-105/16/11 14:0023.8 3.1
2,4-Dinitrophenol ND ug/L 1 05/20/11 00:39 51-28-505/16/11 14:0059.5 10.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 25 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-7 Lab ID:9293852006 Collected:05/09/11 12:30 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
2,4-Dinitrotoluene ND ug/L 1 05/20/11 00:39 121-14-205/16/11 14:006.0 1.1
2,6-Dinitrotoluene ND ug/L 1 05/20/11 00:39 606-20-205/16/11 14:006.0 1.2
Di-n-octylphthalate ND ug/L 1 05/20/11 00:39 117-84-005/16/11 14:006.0 0.79
bis(2-Ethylhexyl)phthalate ND ug/L 1 05/20/11 00:39 117-81-705/16/11 14:006.0 0.94
Fluoranthene ND ug/L 1 05/20/11 00:39 206-44-005/16/11 14:006.0 0.25
Fluorene ND ug/L 1 05/20/11 00:39 86-73-705/16/11 14:006.0 0.25
Hexachloro-1,3-butadiene ND ug/L 1 05/20/11 00:39 87-68-305/16/11 14:006.0 1.1
Hexachlorobenzene ND ug/L 1 05/20/11 00:39 118-74-105/16/11 14:006.0 0.86
Hexachlorocyclopentadiene ND ug/L 1 05/20/11 00:39 77-47-405/16/11 14:0011.9 1.0
Hexachloroethane ND ug/L 1 05/20/11 00:39 67-72-105/16/11 14:006.0 1.3
Indeno(1,2,3-cd)pyrene ND ug/L 1 05/20/11 00:39 193-39-505/16/11 14:006.0 0.35
Isophorone ND ug/L 1 05/20/11 00:39 78-59-105/16/11 14:0011.9 1.1
2-Methylnaphthalene ND ug/L 1 05/20/11 00:39 91-57-605/16/11 14:006.0 0.33
Naphthalene ND ug/L 1 05/20/11 00:39 91-20-305/16/11 14:006.0 0.40
Nitrobenzene ND ug/L 1 05/20/11 00:39 98-95-305/16/11 14:006.0 1.3
2-Nitrophenol ND ug/L 1 05/20/11 00:39 88-75-505/16/11 14:006.0 1.1
4-Nitrophenol ND ug/L 1 05/20/11 00:39 100-02-705/16/11 14:0059.5 4.9
N-Nitrosodimethylamine ND ug/L 1 05/20/11 00:39 62-75-905/16/11 14:006.0 1.1
N-Nitroso-di-n-propylamine ND ug/L 1 05/20/11 00:39 621-64-705/16/11 14:006.0 1.2
N-Nitrosodiphenylamine ND ug/L 1 05/20/11 00:39 86-30-605/16/11 14:0011.9 1.2
Pentachlorophenol ND ug/L 1 05/20/11 00:39 87-86-505/16/11 14:0029.8 5.5
Phenanthrene ND ug/L 1 05/20/11 00:39 85-01-805/16/11 14:006.0 0.26
Phenol ND ug/L 1 05/20/11 00:39 108-95-205/16/11 14:006.0 2.3
Pyrene ND ug/L 1 05/20/11 00:39 129-00-005/16/11 14:006.0 0.23
1,2,4-Trichlorobenzene ND ug/L 1 05/20/11 00:39 120-82-105/16/11 14:006.0 1.2
2,4,6-Trichlorophenol ND ug/L 1 05/20/11 00:39 88-06-205/16/11 14:0011.9 1.5
Nitrobenzene-d5 (S)73 %1 05/20/11 00:39 4165-60-005/16/11 14:0010-120
2-Fluorobiphenyl (S)77 %1 05/20/11 00:39 321-60-805/16/11 14:0015-120
Terphenyl-d14 (S)97 %1 05/20/11 00:39 1718-51-005/16/11 14:0011-131
Phenol-d6 (S)25 %1 05/20/11 00:39 13127-88-305/16/11 14:0010-120
2-Fluorophenol (S)46 %1 05/20/11 00:39 367-12-405/16/11 14:0010-120
2,4,6-Tribromophenol (S)74 %1 05/20/11 00:39 118-79-605/16/11 14:0010-137
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 05/15/11 17:50 71-43-20.50 0.50
Bromobenzene ND ug/L 1 05/15/11 17:50 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 05/15/11 17:50 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 05/15/11 17:50 75-27-40.50 0.50
Bromoform ND ug/L 1 05/15/11 17:50 75-25-20.50 0.50
Bromomethane ND ug/L 1 05/15/11 17:50 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 05/15/11 17:50 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 05/15/11 17:50 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 05/15/11 17:50 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 05/15/11 17:50 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 05/15/11 17:50 108-90-70.50 0.50
Chloroethane ND ug/L 1 05/15/11 17:50 75-00-31.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 26 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-7 Lab ID:9293852006 Collected:05/09/11 12:30 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Chloroform ND ug/L 1 05/15/11 17:50 67-66-30.50 0.50
Chloromethane ND ug/L 1 05/15/11 17:50 74-87-31.0 1.0
2-Chlorotoluene ND ug/L 1 05/15/11 17:50 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 05/15/11 17:50 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 05/15/11 17:50 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 05/15/11 17:50 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 05/15/11 17:50 106-93-40.50 0.50
Dibromomethane ND ug/L 1 05/15/11 17:50 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 05/15/11 17:50 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 05/15/11 17:50 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 05/15/11 17:50 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 05/15/11 17:50 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 05/15/11 17:50 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 05/15/11 17:50 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 05/15/11 17:50 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 05/15/11 17:50 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 05/15/11 17:50 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 05/15/11 17:50 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 05/15/11 17:50 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 05/15/11 17:50 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 05/15/11 17:50 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 05/15/11 17:50 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 05/15/11 17:50 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 05/15/11 17:50 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 05/15/11 17:50 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 05/15/11 17:50 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 05/15/11 17:50 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 05/15/11 17:50 75-09-22.0 2.0
Methyl-tert-butyl ether ND ug/L 1 05/15/11 17:50 1634-04-40.50 0.50
Naphthalene ND ug/L 1 05/15/11 17:50 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 05/15/11 17:50 103-65-10.50 0.50
Styrene ND ug/L 1 05/15/11 17:50 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 05/15/11 17:50 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 05/15/11 17:50 79-34-50.50 0.50
Tetrachloroethene ND ug/L 1 05/15/11 17:50 127-18-40.50 0.50
Toluene ND ug/L 1 05/15/11 17:50 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 05/15/11 17:50 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 05/15/11 17:50 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 05/15/11 17:50 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 05/15/11 17:50 79-00-50.50 0.50
Trichloroethene ND ug/L 1 05/15/11 17:50 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 05/15/11 17:50 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 05/15/11 17:50 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 05/15/11 17:50 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 05/15/11 17:50 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 05/15/11 17:50 75-01-41.0 1.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 27 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-7 Lab ID:9293852006 Collected:05/09/11 12:30 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
m&p-Xylene ND ug/L 1 05/15/11 17:50 179601-23-11.0 1.0
o-Xylene ND ug/L 1 05/15/11 17:50 95-47-60.50 0.50
1,2-Dichloroethane-d4 (S)105 %1 05/15/11 17:50 17060-07-070-130
Dibromofluoromethane (S)103 %1 05/15/11 17:50 1868-53-770-130
4-Bromofluorobenzene (S)96 %1 05/15/11 17:50 460-00-470-130
Toluene-d8 (S)89 %1 05/15/11 17:50 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 28 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-3 Lab ID:9293852007 Collected:05/09/11 11:50 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 05/19/11 05:40 N230.0 15.0
Aliphatic (C09-C12)ND ug/L 1 05/19/11 05:40 N230.0 15.0
Aromatic (C09-C10)ND ug/L 1 05/19/11 05:40 N230.0 15.0
2,5-Dibromotoluene (PID)(S)93 %1 05/19/11 05:4070-130
2,5-Dibromotoluene (FID)(S)92 %1 05/19/11 05:4070-130
200.7 MET ICP, 3030C Analytical Method: EPA 200.7 Preparation Method: SM 3030C
Lead 75.1 ug/L 1 05/11/11 22:24 7439-92-105/11/11 12:155.0 4.0
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 05/15/11 18:12 71-43-20.50 0.50
Bromobenzene ND ug/L 1 05/15/11 18:12 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 05/15/11 18:12 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 05/15/11 18:12 75-27-40.50 0.50
Bromoform ND ug/L 1 05/15/11 18:12 75-25-20.50 0.50
Bromomethane ND ug/L 1 05/15/11 18:12 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 05/15/11 18:12 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 05/15/11 18:12 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 05/15/11 18:12 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 05/15/11 18:12 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 05/15/11 18:12 108-90-70.50 0.50
Chloroethane ND ug/L 1 05/15/11 18:12 75-00-31.0 1.0
Chloroform ND ug/L 1 05/15/11 18:12 67-66-30.50 0.50
Chloromethane ND ug/L 1 05/15/11 18:12 74-87-31.0 1.0
2-Chlorotoluene ND ug/L 1 05/15/11 18:12 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 05/15/11 18:12 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 05/15/11 18:12 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 05/15/11 18:12 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 05/15/11 18:12 106-93-40.50 0.50
Dibromomethane ND ug/L 1 05/15/11 18:12 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 05/15/11 18:12 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 05/15/11 18:12 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 05/15/11 18:12 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 05/15/11 18:12 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 05/15/11 18:12 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 05/15/11 18:12 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 05/15/11 18:12 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 05/15/11 18:12 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 05/15/11 18:12 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 05/15/11 18:12 78-87-50.50 0.50
1,3-Dichloropropane ND ug/L 1 05/15/11 18:12 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 05/15/11 18:12 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 05/15/11 18:12 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 05/15/11 18:12 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 05/15/11 18:12 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 05/15/11 18:12 108-20-30.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 29 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-3 Lab ID:9293852007 Collected:05/09/11 11:50 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
Ethylbenzene ND ug/L 1 05/15/11 18:12 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 05/15/11 18:12 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 05/15/11 18:12 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 05/15/11 18:12 75-09-22.0 2.0
Methyl-tert-butyl ether 0.59 ug/L 1 05/15/11 18:12 1634-04-40.50 0.50
Naphthalene ND ug/L 1 05/15/11 18:12 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 05/15/11 18:12 103-65-10.50 0.50
Styrene ND ug/L 1 05/15/11 18:12 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 05/15/11 18:12 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 05/15/11 18:12 79-34-50.50 0.50
Tetrachloroethene ND ug/L 1 05/15/11 18:12 127-18-40.50 0.50
Toluene ND ug/L 1 05/15/11 18:12 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 05/15/11 18:12 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 05/15/11 18:12 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 05/15/11 18:12 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 05/15/11 18:12 79-00-50.50 0.50
Trichloroethene ND ug/L 1 05/15/11 18:12 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 05/15/11 18:12 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 05/15/11 18:12 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 05/15/11 18:12 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 05/15/11 18:12 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 05/15/11 18:12 75-01-41.0 1.0
m&p-Xylene ND ug/L 1 05/15/11 18:12 179601-23-11.0 1.0
o-Xylene ND ug/L 1 05/15/11 18:12 95-47-60.50 0.50
1,2-Dichloroethane-d4 (S)108 %1 05/15/11 18:12 17060-07-070-130
Dibromofluoromethane (S)103 %1 05/15/11 18:12 1868-53-770-130
4-Bromofluorobenzene (S)95 %1 05/15/11 18:12 460-00-470-130
Toluene-d8 (S)93 %1 05/15/11 18:12 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 30 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-5 Lab ID:9293852008 Collected:05/09/11 09:15 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)ND ug/L 1 05/17/11 05:33 N205/15/11 05:40116116
Aliphatic (C19-C36)ND ug/L 1 05/17/11 05:33 N205/15/11 05:40116116
Aromatic (C11-C22)ND ug/L 1 05/17/11 05:33 N205/15/11 05:40116116
Nonatriacontane (S)84 %1 05/17/11 05:33 7194-86-705/15/11 05:4040-140
o-Terphenyl (S)64 %1 05/17/11 05:33 84-15-105/15/11 05:4040-140
2-Fluorobiphenyl (S)84 %1 05/17/11 05:33 321-60-805/15/11 05:4040-140
2-Bromonaphthalene (S)90 %1 05/17/11 05:33 580-13-205/15/11 05:4040-140
VPH NC Water Analytical Method: MADEP VPH
Aliphatic (C05-C08)ND ug/L 1 05/19/11 06:05 N230.0 15.0
Aliphatic (C09-C12)ND ug/L 1 05/19/11 06:05 N230.0 15.0
Aromatic (C09-C10)ND ug/L 1 05/19/11 06:05 N230.0 15.0
2,5-Dibromotoluene (PID)(S)96 %1 05/19/11 06:0570-130
2,5-Dibromotoluene (FID)(S)93 %1 05/19/11 06:0570-130
6200B MSV Analytical Method: SM 6200B
Benzene ND ug/L 1 05/15/11 18:35 71-43-20.50 0.50
Bromobenzene ND ug/L 1 05/15/11 18:35 108-86-10.50 0.50
Bromochloromethane ND ug/L 1 05/15/11 18:35 74-97-50.50 0.50
Bromodichloromethane ND ug/L 1 05/15/11 18:35 75-27-40.50 0.50
Bromoform ND ug/L 1 05/15/11 18:35 75-25-20.50 0.50
Bromomethane ND ug/L 1 05/15/11 18:35 74-83-95.0 1.0
n-Butylbenzene ND ug/L 1 05/15/11 18:35 104-51-80.50 0.50
sec-Butylbenzene ND ug/L 1 05/15/11 18:35 135-98-80.50 0.50
tert-Butylbenzene ND ug/L 1 05/15/11 18:35 98-06-60.50 0.50
Carbon tetrachloride ND ug/L 1 05/15/11 18:35 56-23-50.50 0.50
Chlorobenzene ND ug/L 1 05/15/11 18:35 108-90-70.50 0.50
Chloroethane ND ug/L 1 05/15/11 18:35 75-00-31.0 1.0
Chloroform ND ug/L 1 05/15/11 18:35 67-66-30.50 0.50
Chloromethane ND ug/L 1 05/15/11 18:35 74-87-31.0 1.0
2-Chlorotoluene ND ug/L 1 05/15/11 18:35 95-49-80.50 0.50
4-Chlorotoluene ND ug/L 1 05/15/11 18:35 106-43-40.50 0.50
1,2-Dibromo-3-chloropropane ND ug/L 1 05/15/11 18:35 96-12-81.0 1.0
Dibromochloromethane ND ug/L 1 05/15/11 18:35 124-48-10.50 0.50
1,2-Dibromoethane (EDB)ND ug/L 1 05/15/11 18:35 106-93-40.50 0.50
Dibromomethane ND ug/L 1 05/15/11 18:35 74-95-30.50 0.50
1,2-Dichlorobenzene ND ug/L 1 05/15/11 18:35 95-50-10.50 0.50
1,3-Dichlorobenzene ND ug/L 1 05/15/11 18:35 541-73-10.50 0.50
1,4-Dichlorobenzene ND ug/L 1 05/15/11 18:35 106-46-70.50 0.50
Dichlorodifluoromethane ND ug/L 1 05/15/11 18:35 75-71-80.50 0.50
1,1-Dichloroethane ND ug/L 1 05/15/11 18:35 75-34-30.50 0.50
1,2-Dichloroethane ND ug/L 1 05/15/11 18:35 107-06-20.50 0.50
1,1-Dichloroethene ND ug/L 1 05/15/11 18:35 75-35-40.50 0.50
cis-1,2-Dichloroethene ND ug/L 1 05/15/11 18:35 156-59-20.50 0.50
trans-1,2-Dichloroethene ND ug/L 1 05/15/11 18:35 156-60-50.50 0.50
1,2-Dichloropropane ND ug/L 1 05/15/11 18:35 78-87-50.50 0.50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 31 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
ANALYTICAL RESULTS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Sample:MW-5 Lab ID:9293852008 Collected:05/09/11 09:15 Received:05/10/11 17:25 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
6200B MSV Analytical Method: SM 6200B
1,3-Dichloropropane ND ug/L 1 05/15/11 18:35 142-28-90.50 0.50
2,2-Dichloropropane ND ug/L 1 05/15/11 18:35 594-20-70.50 0.50
1,1-Dichloropropene ND ug/L 1 05/15/11 18:35 563-58-60.50 0.50
cis-1,3-Dichloropropene ND ug/L 1 05/15/11 18:35 10061-01-50.50 0.50
trans-1,3-Dichloropropene ND ug/L 1 05/15/11 18:35 10061-02-60.50 0.50
Diisopropyl ether ND ug/L 1 05/15/11 18:35 108-20-30.50 0.50
Ethylbenzene ND ug/L 1 05/15/11 18:35 100-41-40.50 0.50
Hexachloro-1,3-butadiene ND ug/L 1 05/15/11 18:35 87-68-32.0 2.0
Isopropylbenzene (Cumene)ND ug/L 1 05/15/11 18:35 98-82-80.50 0.50
Methylene Chloride ND ug/L 1 05/15/11 18:35 75-09-22.0 2.0
Methyl-tert-butyl ether 8.0 ug/L 1 05/15/11 18:35 1634-04-40.50 0.50
Naphthalene ND ug/L 1 05/15/11 18:35 91-20-32.0 2.0
n-Propylbenzene ND ug/L 1 05/15/11 18:35 103-65-10.50 0.50
Styrene ND ug/L 1 05/15/11 18:35 100-42-50.50 0.50
1,1,1,2-Tetrachloroethane ND ug/L 1 05/15/11 18:35 630-20-60.50 0.50
1,1,2,2-Tetrachloroethane ND ug/L 1 05/15/11 18:35 79-34-50.50 0.50
Tetrachloroethene ND ug/L 1 05/15/11 18:35 127-18-40.50 0.50
Toluene ND ug/L 1 05/15/11 18:35 108-88-30.50 0.50
1,2,3-Trichlorobenzene ND ug/L 1 05/15/11 18:35 87-61-62.0 2.0
1,2,4-Trichlorobenzene ND ug/L 1 05/15/11 18:35 120-82-12.0 2.0
1,1,1-Trichloroethane ND ug/L 1 05/15/11 18:35 71-55-60.50 0.50
1,1,2-Trichloroethane ND ug/L 1 05/15/11 18:35 79-00-50.50 0.50
Trichloroethene ND ug/L 1 05/15/11 18:35 79-01-60.50 0.50
Trichlorofluoromethane ND ug/L 1 05/15/11 18:35 75-69-41.0 1.0
1,2,3-Trichloropropane ND ug/L 1 05/15/11 18:35 96-18-40.50 0.50
1,2,4-Trimethylbenzene ND ug/L 1 05/15/11 18:35 95-63-60.50 0.50
1,3,5-Trimethylbenzene ND ug/L 1 05/15/11 18:35 108-67-80.50 0.50
Vinyl chloride ND ug/L 1 05/15/11 18:35 75-01-41.0 1.0
m&p-Xylene ND ug/L 1 05/15/11 18:35 179601-23-11.0 1.0
o-Xylene ND ug/L 1 05/15/11 18:35 95-47-60.50 0.50
1,2-Dichloroethane-d4 (S)106 %1 05/15/11 18:35 17060-07-070-130
Dibromofluoromethane (S)103 %1 05/15/11 18:35 1868-53-770-130
4-Bromofluorobenzene (S)97 %1 05/15/11 18:35 460-00-470-130
Toluene-d8 (S)93 %1 05/15/11 18:35 2037-26-570-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 32 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/13598
MADEP EPH
MADEP EPH
MADEP EPH NC Water
Associated Lab Samples:9293852001, 9293852002, 9293852003, 9293852004, 9293852005, 9293852006, 9293852008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:606674
Associated Lab Samples:9293852001, 9293852002, 9293852003, 9293852004, 9293852005, 9293852006, 9293852008
Matrix:Water
Analyzed
Aliphatic (C09-C18)ug/L ND 100 N205/16/11 18:11
Aliphatic (C19-C36)ug/L ND 100 N205/16/11 18:11
Aromatic (C11-C22)ug/L ND 100 N205/16/11 18:11
2-Bromonaphthalene (S)%84 40-140 05/16/11 18:11
2-Fluorobiphenyl (S)%78 40-140 05/16/11 18:11
Nonatriacontane (S)%68 40-140 05/16/11 18:11
o-Terphenyl (S)%72 40-140 05/16/11 18:11
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
606675LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
606676
Aliphatic (C09-C18)ug/L 200 N23006740-14072215 8 50
Aliphatic (C19-C36)ug/L 321 N24008040-14085341 6 50
Aromatic (C11-C22)ug/L 591 N28507040-14073618 5 50
2-Bromonaphthalene (S)%74 40-14079
2-Fluorobiphenyl (S)%77 40-14081
Nonatriacontane (S)%66 40-14069
o-Terphenyl (S)%69 40-14072
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 33 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/4996
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples:9293852004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:607095
Associated Lab Samples:9293852004
Matrix:Water
Analyzed
Aliphatic (C05-C08)ug/L ND 30.0 N205/16/11 21:29
Aliphatic (C09-C12)ug/L 16.8J 30.0 N205/16/11 21:29
Aromatic (C09-C10)ug/L ND 30.0 N205/16/11 21:29
2,5-Dibromotoluene (FID)(S)%107 70-130 05/16/11 21:29
2,5-Dibromotoluene (PID)(S)%110 70-130 05/16/11 21:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
607096LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
607097
Aliphatic (C05-C08)ug/L 285 N23009570-13091272 5 25
Aliphatic (C09-C12)ug/L 360 N230012030-130128385 7 25
Aromatic (C09-C10)ug/L 97.3 N21009770-1309897.5 0 25
2,5-Dibromotoluene (FID)(S)%93 70-13090
2,5-Dibromotoluene (PID)(S)%93 70-13090
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 34 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/5008
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples:9293852002, 9293852003, 9293852005, 9293852006, 9293852007, 9293852008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:608225
Associated Lab Samples:9293852002, 9293852003, 9293852005, 9293852006, 9293852007, 9293852008
Matrix:Water
Analyzed
Aliphatic (C05-C08)ug/L ND 30.0 N205/19/11 01:57
Aliphatic (C09-C12)ug/L 16.5J 30.0 N205/19/11 01:57
Aromatic (C09-C10)ug/L ND 30.0 N205/19/11 01:57
2,5-Dibromotoluene (FID)(S)%105 70-130 05/19/11 01:57
2,5-Dibromotoluene (PID)(S)%108 70-130 05/19/11 01:57
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
608226LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
608227
Aliphatic (C05-C08)ug/L 282 N23009470-13089266 6 25
Aliphatic (C09-C12)ug/L 346 N230011530-130116348 1 25
Aromatic (C09-C10)ug/L 98.0 N21009870-1309695.8 2 25
2,5-Dibromotoluene (FID)(S)%109 70-130100
2,5-Dibromotoluene (PID)(S)%104 70-13093
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 35 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
GCV/5017
MADEP VPH
MADEP VPH
VPH NC Water
Associated Lab Samples:9293852001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:609230
Associated Lab Samples:9293852001
Matrix:Water
Analyzed
Aliphatic (C05-C08)ug/L ND 30.0 N205/20/11 19:13
Aliphatic (C09-C12)ug/L 25.3J 30.0 N205/20/11 19:13
Aromatic (C09-C10)ug/L ND 30.0 N205/20/11 19:13
2,5-Dibromotoluene (FID)(S)%103 70-130 05/20/11 19:13
2,5-Dibromotoluene (PID)(S)%105 70-130 05/20/11 19:13
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
609231LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
609232
Aliphatic (C05-C08)ug/L 269 N23009070-13087261 3 25
Aliphatic (C09-C12)ug/L 331 N230011030-130123369 11 25
Aromatic (C09-C10)ug/L 95.6 N21009670-1309999.2 4 25
2,5-Dibromotoluene (FID)(S)%116 70-130113
2,5-Dibromotoluene (PID)(S)%121 70-130116
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 36 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MPRP/8342
SM 3030C
EPA 200.7
200.7 MET 3030C
Associated Lab Samples:9293852001, 9293852002, 9293852003, 9293852004, 9293852005, 9293852006, 9293852007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:604337
Associated Lab Samples:9293852001, 9293852002, 9293852003, 9293852004, 9293852005, 9293852006, 9293852007
Matrix:Water
Analyzed
Lead ug/L ND 5.0 05/11/11 21:28
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
604338LABORATORY CONTROL SAMPLE:
LCSSpike
Lead ug/L 557500 111 85-115
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
604339MATRIX SPIKE SAMPLE:
MSSpike
Result
9293788001
Lead ug/L 519500 102 70-1307.5
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
604341MATRIX SPIKE SAMPLE:
MSSpike
Result
9293720002
Lead ug/L 536500 107 70-130ND
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9293791001
604340SAMPLE DUPLICATE:
Lead ug/L 27.0 5 2028.5
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
9293852006
604342SAMPLE DUPLICATE:
Lead ug/L 28.7 0 2028.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 37 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
OEXT/13607
EPA 625
EPA 625
625 MSS
Associated Lab Samples:9293852001, 9293852002, 9293852003, 9293852004, 9293852005, 9293852006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:606934
Associated Lab Samples:9293852001, 9293852002, 9293852003, 9293852004, 9293852005, 9293852006
Matrix:Water
Analyzed
1,2,4-Trichlorobenzene ug/L ND 5.0 05/19/11 21:25
2,4,6-Trichlorophenol ug/L ND 10.0 05/19/11 21:25
2,4-Dichlorophenol ug/L ND 5.0 05/19/11 21:25
2,4-Dimethylphenol ug/L ND 10.0 05/19/11 21:25
2,4-Dinitrophenol ug/L ND 50.0 05/19/11 21:25
2,4-Dinitrotoluene ug/L ND 5.0 05/19/11 21:25
2,6-Dinitrotoluene ug/L ND 5.0 05/19/11 21:25
2-Chloronaphthalene ug/L ND 5.0 05/19/11 21:25
2-Chlorophenol ug/L ND 5.0 05/19/11 21:25
2-Methylnaphthalene ug/L ND 5.0 05/19/11 21:25
2-Nitrophenol ug/L ND 5.0 05/19/11 21:25
3,3'-Dichlorobenzidine ug/L ND 25.0 05/19/11 21:25
4,6-Dinitro-2-methylphenol ug/L ND 20.0 05/19/11 21:25
4-Bromophenylphenyl ether ug/L ND 5.0 05/19/11 21:25
4-Chloro-3-methylphenol ug/L ND 5.0 05/19/11 21:25
4-Chlorophenylphenyl ether ug/L ND 5.0 05/19/11 21:25
4-Nitrophenol ug/L ND 50.0 05/19/11 21:25
Acenaphthene ug/L ND 5.0 05/19/11 21:25
Acenaphthylene ug/L ND 5.0 05/19/11 21:25
Anthracene ug/L ND 5.0 05/19/11 21:25
Benzo(a)anthracene ug/L ND 5.0 05/19/11 21:25
Benzo(a)pyrene ug/L ND 5.0 05/19/11 21:25
Benzo(b)fluoranthene ug/L ND 5.0 05/19/11 21:25
Benzo(g,h,i)perylene ug/L ND 5.0 05/19/11 21:25
Benzo(k)fluoranthene ug/L ND 5.0 05/19/11 21:25
bis(2-Chloroethoxy)methane ug/L ND 10.0 05/19/11 21:25
bis(2-Chloroethyl) ether ug/L ND 5.0 05/19/11 21:25
bis(2-Chloroisopropyl) ether ug/L ND 5.0 05/19/11 21:25
bis(2-Ethylhexyl)phthalate ug/L ND 5.0 05/19/11 21:25
Butylbenzylphthalate ug/L ND 5.0 05/19/11 21:25
Chrysene ug/L ND 5.0 05/19/11 21:25
Di-n-butylphthalate ug/L ND 5.0 05/19/11 21:25
Di-n-octylphthalate ug/L ND 5.0 05/19/11 21:25
Dibenz(a,h)anthracene ug/L ND 5.0 05/19/11 21:25
Diethylphthalate ug/L ND 5.0 05/19/11 21:25
Dimethylphthalate ug/L ND 5.0 05/19/11 21:25
Fluoranthene ug/L ND 5.0 05/19/11 21:25
Fluorene ug/L ND 5.0 05/19/11 21:25
Hexachloro-1,3-butadiene ug/L ND 5.0 05/19/11 21:25
Hexachlorobenzene ug/L ND 5.0 05/19/11 21:25
Hexachlorocyclopentadiene ug/L ND 10.0 05/19/11 21:25
Hexachloroethane ug/L ND 5.0 05/19/11 21:25
Indeno(1,2,3-cd)pyrene ug/L ND 5.0 05/19/11 21:25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 38 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:606934
Associated Lab Samples:9293852001, 9293852002, 9293852003, 9293852004, 9293852005, 9293852006
Matrix:Water
Analyzed
Isophorone ug/L ND 10.0 05/19/11 21:25
N-Nitroso-di-n-propylamine ug/L ND 5.0 05/19/11 21:25
N-Nitrosodimethylamine ug/L ND 5.0 05/19/11 21:25
N-Nitrosodiphenylamine ug/L ND 10.0 05/19/11 21:25
Naphthalene ug/L ND 5.0 05/19/11 21:25
Nitrobenzene ug/L ND 5.0 05/19/11 21:25
Pentachlorophenol ug/L ND 25.0 05/19/11 21:25
Phenanthrene ug/L ND 5.0 05/19/11 21:25
Phenol ug/L ND 5.0 05/19/11 21:25
Pyrene ug/L ND 5.0 05/19/11 21:25
2,4,6-Tribromophenol (S)%60 10-137 05/19/11 21:25
2-Fluorobiphenyl (S)%54 15-120 05/19/11 21:25
2-Fluorophenol (S)%33 10-120 05/19/11 21:25
Nitrobenzene-d5 (S)%56 10-120 05/19/11 21:25
Phenol-d6 (S)%19 10-120 05/19/11 21:25
Terphenyl-d14 (S)%83 11-131 05/19/11 21:25
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
606935LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 23.950 48 44-142
2,4,6-Trichlorophenol ug/L 35.150 70 37-144
2,4-Dichlorophenol ug/L 31.050 62 1-191
2,4-Dimethylphenol ug/L 29.150 58 32-119
2,4-Dinitrophenol ug/L 66.7250 27 1-181
2,4-Dinitrotoluene ug/L 36.150 72 39-139
2,6-Dinitrotoluene ug/L 35.250 70 50-158
2-Chloronaphthalene ug/L 31.250 62 60-118
2-Chlorophenol ug/L 25.950 52 23-134
2-Methylnaphthalene ug/L 26.950 54 25-150
2-Nitrophenol ug/L 27.350 55 29-182
3,3'-Dichlorobenzidine ug/L 57.6100 58 1-262
4,6-Dinitro-2-methylphenol ug/L 52.1100 52 1-181
4-Bromophenylphenyl ether ug/L 35.050 70 53-127
4-Chloro-3-methylphenol ug/L 69.8100 70 22-147
4-Chlorophenylphenyl ether ug/L 35.950 72 25-158
4-Nitrophenol ug/L 63.0250 25 1-132
Acenaphthene ug/L 38.350 77 47-145
Acenaphthylene ug/L 34.850 70 33-145
Anthracene ug/L 40.150 80 1-166
Benzo(a)anthracene ug/L 35.250 70 33-143
Benzo(a)pyrene ug/L 31.850 64 17-163
Benzo(b)fluoranthene ug/L 33.650 67 24-159
Benzo(g,h,i)perylene ug/L 34.850 70 1-219
Benzo(k)fluoranthene ug/L 37.250 74 11-162
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 39 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
606935LABORATORY CONTROL SAMPLE:
LCSSpike
bis(2-Chloroethoxy)methane ug/L 29.650 59 33-184
bis(2-Chloroethyl) ether ug/L 28.150 56 12-158
bis(2-Chloroisopropyl) ether ug/L 27.750 55 36-166
bis(2-Ethylhexyl)phthalate ug/L 34.350 69 8-158
Butylbenzylphthalate ug/L 34.250 68 1-152
Chrysene ug/L 36.750 73 17-168
Di-n-butylphthalate ug/L 35.550 71 1-118
Di-n-octylphthalate ug/L 25.250 50 4-146
Dibenz(a,h)anthracene ug/L 33.450 67 1-227
Diethylphthalate ug/L 36.050 72 1-114
Dimethylphthalate ug/L 36.050 72 1-112
Fluoranthene ug/L 35.850 72 26-137
Fluorene ug/L 39.450 79 59-121
Hexachloro-1,3-butadiene ug/L 22.050 44 24-116
Hexachlorobenzene ug/L 37.750 75 1-152
Hexachlorocyclopentadiene ug/L 18.450 37 25-150
Hexachloroethane ug/L 20.350 41 40-113
Indeno(1,2,3-cd)pyrene ug/L 33.150 66 1-171
Isophorone ug/L 34.150 68 21-196
N-Nitroso-di-n-propylamine ug/L 27.650 55 1-230
N-Nitrosodimethylamine ug/L 18.750 37 25-150
N-Nitrosodiphenylamine ug/L 38.950 78 25-150
Naphthalene ug/L 27.350 55 21-133
Nitrobenzene ug/L 29.350 59 35-180
Pentachlorophenol ug/L 50.6100 51 14-176
Phenanthrene ug/L 38.950 78 54-120
Phenol ug/L 13.550 27 5-112
Pyrene ug/L 42.850 86 52-115
2,4,6-Tribromophenol (S)%71 10-137
2-Fluorobiphenyl (S)%69 15-120
2-Fluorophenol (S)%36 10-120
Nitrobenzene-d5 (S)%60 10-120
Phenol-d6 (S)%21 10-120
Terphenyl-d14 (S)%86 11-131
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
606936MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9293732014
606937
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/L 100 61 44-14256 7 30100<5.0 60.8 56.4
2,4,6-Trichlorophenol ug/L 100 77 37-14475 2 30100<10.0 76.6 74.7
2,4-Dichlorophenol ug/L 100 68 1-19164 7 30100<5.0 68.4 64.0
2,4-Dimethylphenol ug/L 100 63 32-11950 22 30100<10.0 63.0 50.4
2,4-Dinitrophenol ug/L 500 55 1-18151 8 30500<50.0 274 253
2,4-Dinitrotoluene ug/L 100 77 39-13979 2 30100<5.0 76.8 78.6
2,6-Dinitrotoluene ug/L 100 77 50-15877 1 30100<5.0 76.6 77.3
2-Chloronaphthalene ug/L 100 71 60-11868 4 30100<5.0 70.5 68.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 40 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
606936MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9293732014
606937
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Chlorophenol ug/L 100 59 23-13456 5 30100<5.0 59.0 56.3
2-Methylnaphthalene ug/L 100 64 25-15058 9 30100<5.0 63.6 58.1
2-Nitrophenol ug/L 100 61 29-18259 3 30100<5.0 60.9 59.0
3,3'-Dichlorobenzidine ug/L R1200421-26261 38 30200<25.0 83.3 122
4,6-Dinitro-2-methylphenol ug/L 200 64 1-18166 2 30200<20.0 128 131
4-Bromophenylphenyl ether ug/L 100 77 53-12777 1 30100<5.0 77.2 76.6
4-Chloro-3-methylphenol ug/L 200 80 22-14775 7 30200<5.0 161 150
4-Chlorophenylphenyl ether ug/L 100 79 25-15877 2 30100<5.0 78.7 76.9
4-Nitrophenol ug/L 500 52 1-13250 4 30500<50.0 262 251
Acenaphthene ug/L 100 84 47-14582 3 30100<5.0 84.1 82.0
Acenaphthylene ug/L 100 76 33-14574 2 30100<5.0 75.9 74.4
Anthracene ug/L 100 86 1-16686 1 30100<5.0 85.5 86.3
Benzo(a)anthracene ug/L 100 76 33-14380 5 30100<5.0 75.9 79.8
Benzo(a)pyrene ug/L 100 69 17-16370 2 30100<5.0 68.9 70.0
Benzo(b)fluoranthene ug/L 100 72 24-15972 0 30100<5.0 72.5 72.3
Benzo(g,h,i)perylene ug/L 100 80 1-21974 7 30100<5.0 79.9 74.4
Benzo(k)fluoranthene ug/L 100 79 11-16280 0 30100<5.0 79.4 79.6
bis(2-Chloroethoxy)methane ug/L 100 66 33-18462 6 30100<10.0 65.7 61.7
bis(2-Chloroethyl) ether ug/L 100 64 12-15861 5 30100<5.0 63.5 60.6
bis(2-Chloroisopropyl) ether ug/L 100 62 36-16659 6 30100<5.0 62.2 58.5
bis(2-Ethylhexyl)phthalate ug/L 100 75 8-15879 5 30100<5.0 75.3 79.4
Butylbenzylphthalate ug/L 100 74 1-15279 6 30100<5.0 74.0 78.7
Chrysene ug/L 100 79 17-16883 5 30100<5.0 79.1 83.1
Di-n-butylphthalate ug/L 100 76 1-11876 1 30100<5.0 75.6 76.3
Di-n-octylphthalate ug/L 100 55 4-14657 5 30100<5.0 54.9 57.4
Dibenz(a,h)anthracene ug/L 100 75 1-22771 5 30100<5.0 74.7 71.4
Diethylphthalate ug/L 100 77 1-11478 0 30100<5.0 77.4 77.5
Dimethylphthalate ug/L 100 77 1-11277 0 30100<5.0 77.2 77.2
Fluoranthene ug/L 100 74 26-13776 2 30100<5.0 74.3 76.1
Fluorene ug/L 100 86 59-12184 3 30100<5.0 86.1 83.7
Hexachloro-1,3-butadiene ug/L 100 62 24-11657 9 30100<5.0 61.7 56.5
Hexachlorobenzene ug/L 100 81 1-15282 1 30100<5.0 81.2 81.8
Hexachlorocyclopentadiene ug/L 100 48 25-15048 0 30100<10.0 47.7 47.7
Hexachloroethane ug/L 100 57 40-11351 12 30100<5.0 57.1 50.5
Indeno(1,2,3-cd)pyrene ug/L 100 74 1-17172 3 30100<5.0 74.4 71.9
Isophorone ug/L 100 76 21-19671 7 30100<10.0 76.4 71.0
N-Nitroso-di-n-propylamine ug/L 100 61 1-23058 6 30100<5.0 61.5 58.0
N-Nitrosodimethylamine ug/L 100 57 25-15052 10 30100<5.0 57.5 51.8
N-Nitrosodiphenylamine ug/L 100 82 25-15084 3 30100<10.0 82.0 84.3
Naphthalene ug/L 100 64 21-13360 6 30100<5.0 64.2 60.5
Nitrobenzene ug/L 100 66 35-18063 5 30100<5.0 66.4 62.9
Pentachlorophenol ug/L 200 60 14-17660 1 30200<25.0 120 120
Phenanthrene ug/L 100 84 54-12084 0 30100<5.0 83.6 83.8
Phenol ug/L 100 40 5-11241 0 30100<5.0 40.4 40.6
Pyrene ug/L 100 93 52-11597 4 30100<5.0 93.2 97.4
2,4,6-Tribromophenol (S)%79 10-13775
2-Fluorobiphenyl (S)%76 15-12071
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 41 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
606936MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9293732014
606937
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Fluorophenol (S)%53 10-12047
Nitrobenzene-d5 (S)%70 10-12063
Phenol-d6 (S)%37 10-12033
Terphenyl-d14 (S)%95 11-13194
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 42 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/15262
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:9293852002, 9293852003, 9293852004, 9293852005, 9293852006, 9293852007, 9293852008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:606649
Associated Lab Samples:9293852002, 9293852003, 9293852004, 9293852005, 9293852006, 9293852007, 9293852008
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 05/15/11 12:09
1,1,1-Trichloroethane ug/L ND 0.50 05/15/11 12:09
1,1,2,2-Tetrachloroethane ug/L ND 0.50 05/15/11 12:09
1,1,2-Trichloroethane ug/L ND 0.50 05/15/11 12:09
1,1-Dichloroethane ug/L ND 0.50 05/15/11 12:09
1,1-Dichloroethene ug/L ND 0.50 05/15/11 12:09
1,1-Dichloropropene ug/L ND 0.50 05/15/11 12:09
1,2,3-Trichlorobenzene ug/L ND 2.0 05/15/11 12:09
1,2,3-Trichloropropane ug/L ND 0.50 05/15/11 12:09
1,2,4-Trichlorobenzene ug/L ND 2.0 05/15/11 12:09
1,2,4-Trimethylbenzene ug/L ND 0.50 05/15/11 12:09
1,2-Dibromo-3-chloropropane ug/L ND 1.0 05/15/11 12:09
1,2-Dibromoethane (EDB)ug/L ND 0.50 05/15/11 12:09
1,2-Dichlorobenzene ug/L ND 0.50 05/15/11 12:09
1,2-Dichloroethane ug/L ND 0.50 05/15/11 12:09
1,2-Dichloropropane ug/L ND 0.50 05/15/11 12:09
1,3,5-Trimethylbenzene ug/L ND 0.50 05/15/11 12:09
1,3-Dichlorobenzene ug/L ND 0.50 05/15/11 12:09
1,3-Dichloropropane ug/L ND 0.50 05/15/11 12:09
1,4-Dichlorobenzene ug/L ND 0.50 05/15/11 12:09
2,2-Dichloropropane ug/L ND 0.50 05/15/11 12:09
2-Chlorotoluene ug/L ND 0.50 05/15/11 12:09
4-Chlorotoluene ug/L ND 0.50 05/15/11 12:09
Benzene ug/L ND 0.50 05/15/11 12:09
Bromobenzene ug/L ND 0.50 05/15/11 12:09
Bromochloromethane ug/L ND 0.50 05/15/11 12:09
Bromodichloromethane ug/L ND 0.50 05/15/11 12:09
Bromoform ug/L ND 0.50 05/15/11 12:09
Bromomethane ug/L ND 5.0 05/15/11 12:09
Carbon tetrachloride ug/L ND 0.50 05/15/11 12:09
Chlorobenzene ug/L ND 0.50 05/15/11 12:09
Chloroethane ug/L ND 1.0 05/15/11 12:09
Chloroform ug/L ND 0.50 05/15/11 12:09
Chloromethane ug/L ND 1.0 05/15/11 12:09
cis-1,2-Dichloroethene ug/L ND 0.50 05/15/11 12:09
cis-1,3-Dichloropropene ug/L ND 0.50 05/15/11 12:09
Dibromochloromethane ug/L ND 0.50 05/15/11 12:09
Dibromomethane ug/L ND 0.50 05/15/11 12:09
Dichlorodifluoromethane ug/L ND 0.50 05/15/11 12:09
Diisopropyl ether ug/L ND 0.50 05/15/11 12:09
Ethylbenzene ug/L ND 0.50 05/15/11 12:09
Hexachloro-1,3-butadiene ug/L ND 2.0 05/15/11 12:09
Isopropylbenzene (Cumene)ug/L ND 0.50 05/15/11 12:09
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 43 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:606649
Associated Lab Samples:9293852002, 9293852003, 9293852004, 9293852005, 9293852006, 9293852007, 9293852008
Matrix:Water
Analyzed
m&p-Xylene ug/L ND 1.0 05/15/11 12:09
Methyl-tert-butyl ether ug/L ND 0.50 05/15/11 12:09
Methylene Chloride ug/L ND 2.0 05/15/11 12:09
n-Butylbenzene ug/L ND 0.50 05/15/11 12:09
n-Propylbenzene ug/L ND 0.50 05/15/11 12:09
Naphthalene ug/L ND 2.0 05/15/11 12:09
o-Xylene ug/L ND 0.50 05/15/11 12:09
sec-Butylbenzene ug/L ND 0.50 05/15/11 12:09
Styrene ug/L ND 0.50 05/15/11 12:09
tert-Butylbenzene ug/L ND 0.50 05/15/11 12:09
Tetrachloroethene ug/L ND 0.50 05/15/11 12:09
Toluene ug/L ND 0.50 05/15/11 12:09
trans-1,2-Dichloroethene ug/L ND 0.50 05/15/11 12:09
trans-1,3-Dichloropropene ug/L ND 0.50 05/15/11 12:09
Trichloroethene ug/L ND 0.50 05/15/11 12:09
Trichlorofluoromethane ug/L ND 1.0 05/15/11 12:09
Vinyl chloride ug/L ND 1.0 05/15/11 12:09
1,2-Dichloroethane-d4 (S)%106 70-130 05/15/11 12:09
4-Bromofluorobenzene (S)%95 70-130 05/15/11 12:09
Dibromofluoromethane (S)%102 70-130 05/15/11 12:09
Toluene-d8 (S)%93 70-130 05/15/11 12:09
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
606650LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.850 98 60-140
1,1,1-Trichloroethane ug/L 51.250 102 60-140
1,1,2,2-Tetrachloroethane ug/L 45.650 91 60-140
1,1,2-Trichloroethane ug/L 51.650 103 60-140
1,1-Dichloroethane ug/L 50.650 101 60-140
1,1-Dichloroethene ug/L 51.550 103 60-140
1,1-Dichloropropene ug/L 48.150 96 60-140
1,2,3-Trichlorobenzene ug/L 44.950 90 60-140
1,2,3-Trichloropropane ug/L 46.450 93 60-140
1,2,4-Trichlorobenzene ug/L 40.150 80 60-140
1,2,4-Trimethylbenzene ug/L 48.350 97 60-140
1,2-Dibromo-3-chloropropane ug/L 50.350 101 60-140
1,2-Dibromoethane (EDB)ug/L 50.450 101 60-140
1,2-Dichlorobenzene ug/L 51.350 103 60-140
1,2-Dichloroethane ug/L 48.250 96 60-140
1,2-Dichloropropane ug/L 50.050 100 60-140
1,3,5-Trimethylbenzene ug/L 49.650 99 60-140
1,3-Dichlorobenzene ug/L 51.850 104 60-140
1,3-Dichloropropane ug/L 51.150 102 60-140
1,4-Dichlorobenzene ug/L 46.850 94 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 44 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
606650LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 37.950 76 60-140
2-Chlorotoluene ug/L 54.150 108 60-140
4-Chlorotoluene ug/L 53.750 107 60-140
Benzene ug/L 52.150 104 60-140
Bromobenzene ug/L 48.950 98 60-140
Bromochloromethane ug/L 49.250 98 60-140
Bromodichloromethane ug/L 52.250 104 60-140
Bromoform ug/L 50.050 100 60-140
Bromomethane ug/L 45.450 91 60-140
Carbon tetrachloride ug/L 54.950 110 60-140
Chlorobenzene ug/L 47.550 95 60-140
Chloroethane ug/L 49.650 99 60-140
Chloroform ug/L 48.750 97 60-140
Chloromethane ug/L 42.350 85 60-140
cis-1,2-Dichloroethene ug/L 50.350 101 60-140
cis-1,3-Dichloropropene ug/L 45.850 92 60-140
Dibromochloromethane ug/L 50.550 101 60-140
Dibromomethane ug/L 50.450 101 60-140
Dichlorodifluoromethane ug/L 45.450 91 60-140
Diisopropyl ether ug/L 49.450 99 60-140
Ethylbenzene ug/L 51.650 103 60-140
Hexachloro-1,3-butadiene ug/L 44.750 89 60-140
Isopropylbenzene (Cumene)ug/L 51.150 102 60-140
m&p-Xylene ug/L 112100 112 60-140
Methyl-tert-butyl ether ug/L 49.750 99 60-140
Methylene Chloride ug/L 49.150 98 60-140
n-Butylbenzene ug/L 43.550 87 60-140
n-Propylbenzene ug/L 53.750 107 60-140
Naphthalene ug/L 44.750 89 60-140
o-Xylene ug/L 48.650 97 60-140
sec-Butylbenzene ug/L 48.750 97 60-140
Styrene ug/L 48.550 97 60-140
tert-Butylbenzene ug/L 49.250 98 60-140
Tetrachloroethene ug/L 49.450 99 60-140
Toluene ug/L 51.250 102 60-140
trans-1,2-Dichloroethene ug/L 50.450 101 60-140
trans-1,3-Dichloropropene ug/L 46.850 94 60-140
Trichloroethene ug/L 50.450 101 60-140
Trichlorofluoromethane ug/L 49.650 99 60-140
Vinyl chloride ug/L 46.750 93 60-140
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%100 70-130
Dibromofluoromethane (S)%100 70-130
Toluene-d8 (S)%103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 45 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
607712MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9293843002
607713
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 86 60-14099 14 3020ND17.2 19.8
1,1,1-Trichloroethane ug/L 20 88 60-140102 15 3020ND17.6 20.5
1,1,2,2-Tetrachloroethane ug/L 20 77 60-14088 13 3020ND15.5 17.6
1,1,2-Trichloroethane ug/L 20 82 60-14092 12 3020ND16.3 18.3
1,1-Dichloroethane ug/L 20 88 60-140102 15 3020ND17.5 20.4
1,1-Dichloroethene ug/L 20 87 60-140103 18 3020ND17.3 20.7
1,1-Dichloropropene ug/L 20 78 60-14090 15 3020ND15.6 18.1
1,2,3-Trichlorobenzene ug/L 20 65 60-14074 14 3020ND13.0 14.9
1,2,3-Trichloropropane ug/L 20 79 60-14090 13 3020ND15.8 18.0
1,2,4-Trichlorobenzene ug/L 20 62 60-14073 16 3020ND12.5 14.6
1,2,4-Trimethylbenzene ug/L 20 77 60-14097 23 3020ND15.4 19.4
1,2-Dibromo-3-chloropropane ug/L 20 71 60-14082 14 3020ND14.2 16.5
1,2-Dibromoethane (EDB)ug/L 20 82 60-14095 15 3020ND16.4 18.9
1,2-Dichlorobenzene ug/L 20 80 60-14095 17 3020ND15.9 19.0
1,2-Dichloroethane ug/L 20 84 60-14095 13 3020ND16.7 19.0
1,2-Dichloropropane ug/L 20 76 60-14089 15 3020ND15.3 17.8
1,3,5-Trimethylbenzene ug/L 20 76 60-14093 20 3020ND15.3 18.7
1,3-Dichlorobenzene ug/L 20 84 60-140100 17 3020ND16.9 20.1
1,3-Dichloropropane ug/L 20 80 60-14094 16 3020ND16.0 18.8
1,4-Dichlorobenzene ug/L 20 79 60-14092 15 3020ND15.8 18.3
2,2-Dichloropropane ug/L 20 71 60-14092 25 3020ND14.3 18.4
2-Chlorotoluene ug/L 20 85 60-140102 19 3020ND16.9 20.4
4-Chlorotoluene ug/L 20 88 60-140105 18 3020ND17.6 21.0
Benzene ug/L 20 82 60-14096 16 3020ND16.4 19.3
Bromobenzene ug/L 20 79 60-14093 16 3020ND15.8 18.5
Bromochloromethane ug/L 20 85 60-14095 11 3020ND17.0 19.0
Bromodichloromethane ug/L 20 81 60-14093 13 3020ND16.3 18.6
Bromoform ug/L 20 79 60-14091 14 3020ND15.8 18.1
Bromomethane ug/L R1207160-14098 32 3020ND14.1 19.6
Carbon tetrachloride ug/L 20 89 60-140105 17 3020ND17.7 20.9
Chlorobenzene ug/L 20 83 60-14096 15 3020ND16.6 19.2
Chloroethane ug/L 20 83 60-14098 17 3020ND16.5 19.7
Chloroform ug/L 20 87 60-140100 14 3020ND17.4 19.9
Chloromethane ug/L 20 66 60-14079 17 3020ND13.2 15.8
cis-1,2-Dichloroethene ug/L 20 85 60-14098 15 3020ND16.9 19.6
cis-1,3-Dichloropropene ug/L M0205860-14070 18 3020ND11.7 14.0
Dibromochloromethane ug/L 20 81 60-14092 13 3020ND16.2 18.5
Dibromomethane ug/L 20 80 60-14091 13 3020ND16.0 18.1
Dichlorodifluoromethane ug/L 20 69 60-14078 12 3020ND13.9 15.7
Diisopropyl ether ug/L 20 75 60-14091 19 3020ND15.0 18.3
Ethylbenzene ug/L 20 87 60-140102 16 3020ND17.4 20.5
Hexachloro-1,3-butadiene ug/L M0205960-14076 24 3020ND11.9 15.1
Isopropylbenzene (Cumene)ug/L 20 78 60-14093 18 3020ND15.5 18.6
m&p-Xylene ug/L 40 93 60-140112 18 3040ND37.4 44.7
Methyl-tert-butyl ether ug/L 20 78 60-14091 15 3020ND15.6 18.2
Methylene Chloride ug/L 20 69 60-14083 19 3020ND13.7 16.6
n-Butylbenzene ug/L 20 68 60-14083 19 3020ND13.6 16.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 46 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
607712MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9293843002
607713
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
n-Propylbenzene ug/L 20 88 60-140105 17 3020ND17.6 20.9
Naphthalene ug/L M0205760-14071 22 3020ND11.3 14.2
o-Xylene ug/L 20 71 60-14086 18 3020ND14.3 17.2
sec-Butylbenzene ug/L 20 74 60-14091 20 3020ND14.8 18.1
Styrene ug/L 20 79 60-14094 17 3020ND15.8 18.8
tert-Butylbenzene ug/L 20 74 60-14090 19 3020ND14.8 18.0
Tetrachloroethene ug/L 20 89 60-140104 16 3020ND17.8 20.9
Toluene ug/L 20 82 60-14094 13 3020ND16.4 18.7
trans-1,2-Dichloroethene ug/L 20 86 60-140102 17 3020ND17.2 20.4
trans-1,3-Dichloropropene ug/L 20 71 60-14079 10 3020ND14.2 15.7
Trichloroethene ug/L 20 87 60-140100 14 3020ND17.3 19.9
Trichlorofluoromethane ug/L 20 85 60-14099 15 3020ND17.0 19.8
Vinyl chloride ug/L 20 68 60-14083 19 3020ND13.6 16.5
1,2-Dichloroethane-d4 (S)%99 70-130100
4-Bromofluorobenzene (S)%103 70-130100
Dibromofluoromethane (S)%99 70-13099
Toluene-d8 (S)%94 70-13095
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 47 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/15276
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:9293852001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:606862
Associated Lab Samples:9293852001
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 05/16/11 21:38
1,1,1-Trichloroethane ug/L ND 0.50 05/16/11 21:38
1,1,2,2-Tetrachloroethane ug/L ND 0.50 05/16/11 21:38
1,1,2-Trichloroethane ug/L ND 0.50 05/16/11 21:38
1,1-Dichloroethane ug/L ND 0.50 05/16/11 21:38
1,1-Dichloroethene ug/L ND 0.50 05/16/11 21:38
1,1-Dichloropropene ug/L ND 0.50 05/16/11 21:38
1,2,3-Trichlorobenzene ug/L ND 2.0 05/16/11 21:38
1,2,3-Trichloropropane ug/L ND 0.50 05/16/11 21:38
1,2,4-Trichlorobenzene ug/L ND 2.0 05/16/11 21:38
1,2,4-Trimethylbenzene ug/L ND 0.50 05/16/11 21:38
1,2-Dibromo-3-chloropropane ug/L ND 1.0 05/16/11 21:38
1,2-Dibromoethane (EDB)ug/L ND 0.50 05/16/11 21:38
1,2-Dichlorobenzene ug/L ND 0.50 05/16/11 21:38
1,2-Dichloroethane ug/L ND 0.50 05/16/11 21:38
1,2-Dichloropropane ug/L ND 0.50 05/16/11 21:38
1,3,5-Trimethylbenzene ug/L ND 0.50 05/16/11 21:38
1,3-Dichlorobenzene ug/L ND 0.50 05/16/11 21:38
1,3-Dichloropropane ug/L ND 0.50 05/16/11 21:38
1,4-Dichlorobenzene ug/L ND 0.50 05/16/11 21:38
2,2-Dichloropropane ug/L ND 0.50 05/16/11 21:38
2-Chlorotoluene ug/L ND 0.50 05/16/11 21:38
4-Chlorotoluene ug/L ND 0.50 05/16/11 21:38
Benzene ug/L ND 0.50 05/16/11 21:38
Bromobenzene ug/L ND 0.50 05/16/11 21:38
Bromochloromethane ug/L ND 0.50 05/16/11 21:38
Bromodichloromethane ug/L ND 0.50 05/16/11 21:38
Bromoform ug/L ND 0.50 05/16/11 21:38
Bromomethane ug/L ND 5.0 05/16/11 21:38
Carbon tetrachloride ug/L ND 0.50 05/16/11 21:38
Chlorobenzene ug/L ND 0.50 05/16/11 21:38
Chloroethane ug/L ND 1.0 05/16/11 21:38
Chloroform ug/L ND 0.50 05/16/11 21:38
Chloromethane ug/L ND 1.0 05/16/11 21:38
cis-1,2-Dichloroethene ug/L ND 0.50 05/16/11 21:38
cis-1,3-Dichloropropene ug/L ND 0.50 05/16/11 21:38
Dibromochloromethane ug/L ND 0.50 05/16/11 21:38
Dibromomethane ug/L ND 0.50 05/16/11 21:38
Dichlorodifluoromethane ug/L ND 0.50 05/16/11 21:38
Diisopropyl ether ug/L ND 0.50 05/16/11 21:38
Ethylbenzene ug/L ND 0.50 05/16/11 21:38
Hexachloro-1,3-butadiene ug/L ND 2.0 05/16/11 21:38
Isopropylbenzene (Cumene)ug/L ND 0.50 05/16/11 21:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 48 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:606862
Associated Lab Samples:9293852001
Matrix:Water
Analyzed
m&p-Xylene ug/L ND 1.0 05/16/11 21:38
Methyl-tert-butyl ether ug/L ND 0.50 05/16/11 21:38
Methylene Chloride ug/L ND 2.0 05/16/11 21:38
n-Butylbenzene ug/L ND 0.50 05/16/11 21:38
n-Propylbenzene ug/L ND 0.50 05/16/11 21:38
Naphthalene ug/L ND 2.0 05/16/11 21:38
o-Xylene ug/L ND 0.50 05/16/11 21:38
sec-Butylbenzene ug/L ND 0.50 05/16/11 21:38
Styrene ug/L ND 0.50 05/16/11 21:38
tert-Butylbenzene ug/L ND 0.50 05/16/11 21:38
Tetrachloroethene ug/L ND 0.50 05/16/11 21:38
Toluene ug/L ND 0.50 05/16/11 21:38
trans-1,2-Dichloroethene ug/L ND 0.50 05/16/11 21:38
trans-1,3-Dichloropropene ug/L ND 0.50 05/16/11 21:38
Trichloroethene ug/L ND 0.50 05/16/11 21:38
Trichlorofluoromethane ug/L ND 1.0 05/16/11 21:38
Vinyl chloride ug/L ND 1.0 05/16/11 21:38
1,2-Dichloroethane-d4 (S)%105 70-130 05/16/11 21:38
4-Bromofluorobenzene (S)%96 70-130 05/16/11 21:38
Dibromofluoromethane (S)%102 70-130 05/16/11 21:38
Toluene-d8 (S)%92 70-130 05/16/11 21:38
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
606863LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 52.350 105 60-140
1,1,1-Trichloroethane ug/L 52.650 105 60-140
1,1,2,2-Tetrachloroethane ug/L 47.650 95 60-140
1,1,2-Trichloroethane ug/L 52.950 106 60-140
1,1-Dichloroethane ug/L 51.650 103 60-140
1,1-Dichloroethene ug/L 50.250 100 60-140
1,1-Dichloropropene ug/L 46.650 93 60-140
1,2,3-Trichlorobenzene ug/L 47.550 95 60-140
1,2,3-Trichloropropane ug/L 45.850 92 60-140
1,2,4-Trichlorobenzene ug/L 43.250 86 60-140
1,2,4-Trimethylbenzene ug/L 50.750 101 60-140
1,2-Dibromo-3-chloropropane ug/L 49.150 98 60-140
1,2-Dibromoethane (EDB)ug/L 51.750 103 60-140
1,2-Dichlorobenzene ug/L 52.850 106 60-140
1,2-Dichloroethane ug/L 49.750 99 60-140
1,2-Dichloropropane ug/L 51.350 103 60-140
1,3,5-Trimethylbenzene ug/L 51.350 103 60-140
1,3-Dichlorobenzene ug/L 54.150 108 60-140
1,3-Dichloropropane ug/L 51.650 103 60-140
1,4-Dichlorobenzene ug/L 48.650 97 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 49 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
606863LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 51.250 102 60-140
2-Chlorotoluene ug/L 55.650 111 60-140
4-Chlorotoluene ug/L 56.650 113 60-140
Benzene ug/L 51.450 103 60-140
Bromobenzene ug/L 49.750 99 60-140
Bromochloromethane ug/L 49.050 98 60-140
Bromodichloromethane ug/L 54.650 109 60-140
Bromoform ug/L 51.150 102 60-140
Bromomethane ug/L 48.050 96 60-140
Carbon tetrachloride ug/L 56.050 112 60-140
Chlorobenzene ug/L 49.450 99 60-140
Chloroethane ug/L 48.650 97 60-140
Chloroform ug/L 50.550 101 60-140
Chloromethane ug/L 39.050 78 60-140
cis-1,2-Dichloroethene ug/L 49.050 98 60-140
cis-1,3-Dichloropropene ug/L 48.550 97 60-140
Dibromochloromethane ug/L 51.150 102 60-140
Dibromomethane ug/L 51.550 103 60-140
Dichlorodifluoromethane ug/L 36.850 74 60-140
Diisopropyl ether ug/L 48.350 97 60-140
Ethylbenzene ug/L 54.050 108 60-140
Hexachloro-1,3-butadiene ug/L 49.550 99 60-140
Isopropylbenzene (Cumene)ug/L 52.850 106 60-140
m&p-Xylene ug/L 118100 118 60-140
Methyl-tert-butyl ether ug/L 49.650 99 60-140
Methylene Chloride ug/L 46.650 93 60-140
n-Butylbenzene ug/L 47.650 95 60-140
n-Propylbenzene ug/L 56.550 113 60-140
Naphthalene ug/L 45.150 90 60-140
o-Xylene ug/L 50.350 101 60-140
sec-Butylbenzene ug/L 50.750 101 60-140
Styrene ug/L 51.650 103 60-140
tert-Butylbenzene ug/L 51.050 102 60-140
Tetrachloroethene ug/L 54.050 108 60-140
Toluene ug/L 52.250 104 60-140
trans-1,2-Dichloroethene ug/L 49.650 99 60-140
trans-1,3-Dichloropropene ug/L 50.150 100 60-140
Trichloroethene ug/L 53.050 106 60-140
Trichlorofluoromethane ug/L 50.750 101 60-140
Vinyl chloride ug/L 42.750 85 60-140
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%101 70-130
Dibromofluoromethane (S)%98 70-130
Toluene-d8 (S)%103 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 50 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
607718MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9294087002
607719
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 101 60-140114 12 3020ND20.2 22.8
1,1,1-Trichloroethane ug/L 20 103 60-140115 11 3020ND20.6 22.9
1,1,2,2-Tetrachloroethane ug/L 20 92 60-140103 11 3020ND18.5 20.5
1,1,2-Trichloroethane ug/L 20 100 60-140113 12 3020ND20.0 22.5
1,1-Dichloroethane ug/L 20 100 60-140114 13 3020ND20.0 22.8
1,1-Dichloroethene ug/L 20 101 60-140112 10 3020ND20.2 22.3
1,1-Dichloropropene ug/L 20 88 60-14098 11 3020ND17.5 19.6
1,2,3-Trichlorobenzene ug/L 20 69 60-14089 25 3020ND13.8 17.8
1,2,3-Trichloropropane ug/L 20 92 60-14099 8 3020ND18.4 19.8
1,2,4-Trichlorobenzene ug/L 20 64 60-14082 23 3020ND12.9 16.3
1,2,4-Trimethylbenzene ug/L 20 89 60-140105 16 3020ND17.9 21.0
1,2-Dibromo-3-chloropropane ug/L 20 78 60-14092 17 3020ND15.7 18.5
1,2-Dibromoethane (EDB)ug/L 20 96 60-140107 11 3020ND19.2 21.3
1,2-Dichlorobenzene ug/L 20 93 60-140109 15 3020ND18.7 21.8
1,2-Dichloroethane ug/L 20 96 60-140108 11 3020ND19.3 21.6
1,2-Dichloropropane ug/L 20 89 60-140105 17 3020ND17.7 21.1
1,3,5-Trimethylbenzene ug/L 20 90 60-140106 16 3020ND18.0 21.1
1,3-Dichlorobenzene ug/L 20 100 60-140114 14 3020ND20.0 22.9
1,3-Dichloropropane ug/L 20 94 60-140107 13 3020ND18.8 21.3
1,4-Dichlorobenzene ug/L 20 92 60-140104 13 3020ND18.4 20.9
2,2-Dichloropropane ug/L R1207860-140109 34 3020ND15.5 21.8
2-Chlorotoluene ug/L 20 98 60-140114 15 3020ND19.6 22.8
4-Chlorotoluene ug/L 20 103 60-140118 14 3020ND20.6 23.6
Benzene ug/L 20 101 60-140114 12 3020ND20.2 22.8
Bromobenzene ug/L 20 93 60-140105 12 3020ND18.6 20.9
Bromochloromethane ug/L 20 97 60-140106 9 3020ND19.3 21.2
Bromodichloromethane ug/L 20 100 60-140111 10 3020ND20.1 22.2
Bromoform ug/L 20 95 60-140104 10 3020ND18.9 20.9
Bromomethane ug/L 20 117 60-140116 1 3020ND23.4 23.2
Carbon tetrachloride ug/L 20 113 60-140123 8 3020ND22.6 24.6
Chlorobenzene ug/L 20 98 60-140109 10 3020ND19.6 21.7
Chloroethane ug/L 20 97 60-140107 10 3020ND19.4 21.5
Chloroform ug/L 20 101 60-140114 12 3020ND20.3 22.9
Chloromethane ug/L 20 76 60-14085 11 3020ND15.3 17.0
cis-1,2-Dichloroethene ug/L 20 94 60-140108 14 3020ND18.8 21.6
cis-1,3-Dichloropropene ug/L R1206660-14098 39 3020ND13.1 19.5
Dibromochloromethane ug/L 20 94 60-140107 13 3020ND18.8 21.4
Dibromomethane ug/L 20 100 60-140110 10 3020ND20.1 22.1
Dichlorodifluoromethane ug/L 20 77 60-14095 21 3020ND15.5 19.1
Diisopropyl ether ug/L 20 82 60-140100 20 3020ND16.5 20.0
Ethylbenzene ug/L 20 103 60-140115 11 3020ND20.6 23.0
Hexachloro-1,3-butadiene ug/L 20 73 60-14098 29 3020ND14.7 19.7
Isopropylbenzene (Cumene)ug/L 20 91 60-140106 15 3020ND18.2 21.2
m&p-Xylene ug/L 40 112 60-140127 12 3040ND44.8 50.6
Methyl-tert-butyl ether ug/L 20 86 60-140102 18 3020ND17.1 20.4
Methylene Chloride ug/L 20 81 60-14093 14 3020ND16.2 18.6
n-Butylbenzene ug/L 20 76 60-14096 22 3020ND15.3 19.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 51 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
607718MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
9294087002
607719
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
n-Propylbenzene ug/L 20 102 60-140118 14 3020ND20.4 23.5
Naphthalene ug/L M0205660-14073 26 3020ND11.2 14.6
o-Xylene ug/L 20 83 60-14097 15 3020ND16.5 19.3
sec-Butylbenzene ug/L 20 88 60-140104 17 3020ND17.6 20.8
Styrene ug/L 20 92 60-140106 14 3020ND18.4 21.3
tert-Butylbenzene ug/L 20 88 60-140103 16 3020ND17.6 20.7
Tetrachloroethene ug/L 20 102 60-140117 14 3020ND20.4 23.4
Toluene ug/L 20 102 60-140112 10 3020ND20.4 22.4
trans-1,2-Dichloroethene ug/L 20 97 60-140110 13 3020ND19.4 22.1
trans-1,3-Dichloropropene ug/L 20 82 60-14098 18 3020ND16.4 19.7
Trichloroethene ug/L 20 106 60-140115 8 3020ND21.3 23.0
Trichlorofluoromethane ug/L 20 103 60-140113 9 3020ND20.6 22.5
Vinyl chloride ug/L 20 76 60-14094 21 3020ND15.1 18.7
1,2-Dichloroethane-d4 (S)%99 70-13098
4-Bromofluorobenzene (S)%103 70-130103
Dibromofluoromethane (S)%100 70-130100
Toluene-d8 (S)%99 70-130101
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 52 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution ofthe sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
Pace Analytical Services - AshevillePASI-A
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0
The lab does not hold NELAC accreditation for this parameter.N2
Results acceptable because non-target analyte peak heights do not exceed the maximum calibrated upper range of thesystem per Section 9.5.8 of the MADEP VPH method.NC
RPD value was outside control limits.R1
Surrogate recovery not evaluated against control limits due to sample dilution.S4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 53 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
9293852
12610 FMR FOUR CORNERS STORE
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
9293852001 OEXT/13598 GCSV/9785MW-1 MADEP EPH MADEP EPH
9293852002 OEXT/13598 GCSV/9785MW-1D MADEP EPH MADEP EPH
9293852003 OEXT/13598 GCSV/9785MW-2 MADEP EPH MADEP EPH
9293852004 OEXT/13598 GCSV/9785MW-4 MADEP EPH MADEP EPH
9293852005 OEXT/13598 GCSV/9785MW-6 MADEP EPH MADEP EPH
9293852006 OEXT/13598 GCSV/9785MW-7 MADEP EPH MADEP EPH
9293852008 OEXT/13598 GCSV/9785MW-5 MADEP EPH MADEP EPH
9293852001 GCV/5017MW-1 MADEP VPH
9293852002 GCV/5008MW-1D MADEP VPH
9293852003 GCV/5008MW-2 MADEP VPH
9293852004 GCV/4996MW-4 MADEP VPH
9293852005 GCV/5008MW-6 MADEP VPH
9293852006 GCV/5008MW-7 MADEP VPH
9293852007 GCV/5008MW-3 MADEP VPH
9293852008 GCV/5008MW-5 MADEP VPH
9293852001 MPRP/8342 ICP/7711MW-1 SM 3030C EPA 200.7
9293852002 MPRP/8342 ICP/7711MW-1D SM 3030C EPA 200.7
9293852003 MPRP/8342 ICP/7711MW-2 SM 3030C EPA 200.7
9293852004 MPRP/8342 ICP/7711MW-4 SM 3030C EPA 200.7
9293852005 MPRP/8342 ICP/7711MW-6 SM 3030C EPA 200.7
9293852006 MPRP/8342 ICP/7711MW-7 SM 3030C EPA 200.7
9293852007 MPRP/8342 ICP/7711MW-3 SM 3030C EPA 200.7
9293852001 OEXT/13607 MSSV/4945MW-1 EPA 625 EPA 625
9293852002 OEXT/13607 MSSV/4945MW-1D EPA 625 EPA 625
9293852003 OEXT/13607 MSSV/4945MW-2 EPA 625 EPA 625
9293852004 OEXT/13607 MSSV/4945MW-4 EPA 625 EPA 625
9293852005 OEXT/13607 MSSV/4945MW-6 EPA 625 EPA 625
9293852006 OEXT/13607 MSSV/4945MW-7 EPA 625 EPA 625
9293852001 MSV/15276MW-1 SM 6200B
9293852002 MSV/15262MW-1D SM 6200B
9293852003 MSV/15262MW-2 SM 6200B
9293852004 MSV/15262MW-4 SM 6200B
9293852005 MSV/15262MW-6 SM 6200B
9293852006 MSV/15262MW-7 SM 6200B
9293852007 MSV/15262MW-3 SM 6200B
9293852008 MSV/15262MW-5 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Date: 05/23/2011 04:04 PM Page 54 of 54
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]