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HomeMy WebLinkAboutRA-2063_12603_CA_LAB_20131217_Shealy Lab ReportSHEALY ENVIRONMENTAL SERVICES,INC. The electronic signature above is the equivalent of a handwritten signature. This report shall not be reproduced,except in its entirety,without the written approval of Shealy Environmental Services,Inc. Shealy Environmental Services,Inc. 106 Vantage Point Drive West Columbia,SC 29172 (803)791-9700 Fax (803)791-9111 www.shealylab.com Report of Analysis SC Electric and Gas Company 220 Operations Way,C221 Cayce,SC 29033--3701 Attention:Aaron Schwartz Project Name:N.West St &W.Johnson St Lot Number:SL12007 Date Completed:12/13/2017 12/13/2017 4:14 PM Approved and released by: Project Manager:Grant Wilton Page 1 of 12 SHEALY ENVIRONMENTAL SERVICES,INC. SC DHEC No:32010001 NELAC No:E87653 NC DENR No:329 NC Field Parameters No:5639 Shealy Environmental Services,Inc. 106 Vantage Point Drive West Columbia,SC 29172 (803)791-9700 Fax (803)791-9111 www.shealylab.com Case Narrative SC Electric and Gas Company Lot Number:SL12007 This Report of Analysis contains the analytical result(s)for the sample(s)listed on the Sample Summary following this Case Narrative.The sample receiving date is documented in the header information associated with each sample. All results listed in this report relate only to the samples that are contained within this report. Sample receipt,sample analysis,and data review have been performed in accordance with the most current approved NELAC standards,the Shealy Environmental Services,Inc.("Shealy")Quality Assurance Management Plan (QAMP),standard operating procedures (SOPs),and Shealy policies.Any exceptions to the NELAC standards,the QAMP,SOPs or policies are qualified on the results page or discussed below. Where applicable,all soil sample analysis are reported on a dry weight basis unless flagged with a "W" qualifier If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page. Volatile Organic Analysis –Method 8260B The surrogate,Toluene-D8,was recovered above the control limit due to matrix interference. Page 2 of 12 SHEALY ENVIRONMENTAL SERVICES, INC. Sample Summary SC Electric and Gas Company Lot Number: SL12007 Project Name: N.West St & W.Johnson St Project Number: Sample Number Sample ID Matrix Date Sampled Date Received 001 12/11/2017 1145Sample #1 Solid 12/12/2017 (1 sample) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Page 3 of 12 SHEALY ENVIRONMENTAL SERVICES, INC. Detection Summary SC Electric and Gas Company Lot Number: SL12007 Project Name: N.West St & W.Johnson St Project Number: Sample Sample ID Matrix Parameter Method Result Q Units Page 001 Sample #1 Solid Acetone 8260B 19 J ug/kg 5 001 Sample #1 Solid Carbon disulfide 8260B 5.1 J ug/kg 5 001 Sample #1 Solid Ethylbenzene 8260B 23 ug/kg 5 001 Sample #1 Solid Isopropylbenzene 8260B 50 ug/kg 5 001 Sample #1 Solid Methylcyclohexane 8260B 220 ug/kg 5 001 Sample #1 Solid Xylenes (total)8260B 5.7 J ug/kg 6 001 Sample #1 Solid Acenaphthene 8270D 160 ug/kg 7 001 Sample #1 Solid Anthracene 8270D 52 ug/kg 7 001 Sample #1 Solid Benzo(a)anthracene 8270D 18 ug/kg 7 001 Sample #1 Solid Benzo(b)fluoranthene 8270D 12 J ug/kg 7 001 Sample #1 Solid Carbazole 8270D 12 J ug/kg 7 001 Sample #1 Solid Chrysene 8270D 11 J ug/kg 7 001 Sample #1 Solid Dibenzofuran 8270D 77 J ug/kg 7 001 Sample #1 Solid Fluoranthene 8270D 60 ug/kg 7 001 Sample #1 Solid Fluorene 8270D 100 ug/kg 7 001 Sample #1 Solid 2-Methylnaphthalene 8270D 1800 ug/kg 8 001 Sample #1 Solid Naphthalene 8270D 590 ug/kg 8 001 Sample #1 Solid Phenanthrene 8270D 190 ug/kg 8 001 Sample #1 Solid Pyrene 8270D 41 ug/kg 8 001 Sample #1 Solid Arsenic 6010D 0.30 J mg/kg 9 001 Sample #1 Solid Barium 6010D 8.5 mg/kg 9 001 Sample #1 Solid Cadmium 6010D 0.13 J mg/kg 9 001 Sample #1 Solid Chromium 6010D 5.1 mg/kg 9 001 Sample #1 Solid Lead 6010D 2.0 mg/kg 9 (24 detections) 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Page 4 of 12 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SC Electric and Gas Company Sample #1 SL12007-001 12/11/2017 1145 12/12/2017 Solid % Solids:80.3 12/12/2017 2152Project Name: N.West St & W.Johnson St Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 2 5035 8260B 1 12/13/2017 1353 JM1 59545 5.74 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acetone 67-64-1 8260B 19 J 2ug/kg4.322 Benzene 71-43-2 8260B ND 2ug/kg2.25.4 Bromodichloromethane 75-27-4 8260B ND 2ug/kg2.25.4 Bromoform 75-25-2 8260B ND 2ug/kg2.25.4 Bromomethane (Methyl bromide)74-83-9 8260B ND 2ug/kg2.25.4 2-Butanone (MEK)78-93-3 8260B ND 2ug/kg4.322 Carbon disulfide 75-15-0 8260B 5.1 J 2ug/kg2.25.4 Carbon tetrachloride 56-23-5 8260B ND 2ug/kg2.25.4 Chlorobenzene 108-90-7 8260B ND 2ug/kg2.25.4 Chloroethane 75-00-3 8260B ND 2ug/kg2.25.4 Chloroform 67-66-3 8260B ND 2ug/kg2.25.4 Chloromethane (Methyl chloride)74-87-3 8260B ND 2ug/kg2.25.4 Cyclohexane 110-82-7 8260B ND 2ug/kg2.25.4 1,2-Dibromo-3-chloropropane (DBCP)96-12-8 8260B ND 2ug/kg2.25.4 Dibromochloromethane 124-48-1 8260B ND 2ug/kg2.25.4 1,2-Dibromoethane (EDB)106-93-4 8260B ND 2ug/kg2.25.4 1,2-Dichlorobenzene 95-50-1 8260B ND 2ug/kg2.25.4 1,3-Dichlorobenzene 541-73-1 8260B ND 2ug/kg2.25.4 1,4-Dichlorobenzene 106-46-7 8260B ND 2ug/kg2.25.4 Dichlorodifluoromethane 75-71-8 8260B ND 2ug/kg2.25.4 1,1-Dichloroethane 75-34-3 8260B ND 2ug/kg2.25.4 1,2-Dichloroethane 107-06-2 8260B ND 2ug/kg2.25.4 1,1-Dichloroethene 75-35-4 8260B ND 2ug/kg2.25.4 cis-1,2-Dichloroethene 156-59-2 8260B ND 2ug/kg2.25.4 trans-1,2-Dichloroethene 156-60-5 8260B ND 2ug/kg2.25.4 1,2-Dichloropropane 78-87-5 8260B ND 2ug/kg2.25.4 cis-1,3-Dichloropropene 10061-01-5 8260B ND 2ug/kg2.25.4 trans-1,3-Dichloropropene 10061-02-6 8260B ND 2ug/kg2.25.4 Ethylbenzene 100-41-4 8260B 23 2ug/kg2.25.4 2-Hexanone 591-78-6 8260B ND 2ug/kg4.311 Isopropylbenzene 98-82-8 8260B 50 2ug/kg2.25.4 Methyl acetate 79-20-9 8260B ND 2ug/kg2.25.4 Methyl tertiary butyl ether (MTBE)1634-04-4 8260B ND 2ug/kg2.25.4 4-Methyl-2-pentanone 108-10-1 8260B ND 2ug/kg4.311 Methylcyclohexane 108-87-2 8260B 220 2ug/kg2.25.4 Methylene chloride 75-09-2 8260B ND 2ug/kg2.25.4 Styrene 100-42-5 8260B ND 2ug/kg2.25.4 1,1,2,2-Tetrachloroethane 79-34-5 8260B ND 2ug/kg2.25.4 Tetrachloroethene 127-18-4 8260B ND 2ug/kg2.25.4 Toluene 108-88-3 8260B ND 2ug/kg2.25.4 1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B ND 2ug/kg2.25.4 1,2,4-Trichlorobenzene 120-82-1 8260B ND 2ug/kg2.25.4 1,1,1-Trichloroethane 71-55-6 8260B ND 2ug/kg2.25.4 1,1,2-Trichloroethane 79-00-5 8260B ND 2ug/kg2.25.4 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Page 5 of 12 Volatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SC Electric and Gas Company Sample #1 SL12007-001 12/11/2017 1145 12/12/2017 Solid % Solids:80.3 12/12/2017 2152Project Name: N.West St & W.Johnson St Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g) 2 5035 8260B 1 12/13/2017 1353 JM1 59545 5.74 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Trichloroethene 79-01-6 8260B ND 2ug/kg2.25.4 Trichlorofluoromethane 75-69-4 8260B ND 2ug/kg2.25.4 Vinyl chloride 75-01-4 8260B ND 2ug/kg2.25.4 Xylenes (total)1330-20-7 8260B 5.7 J 2ug/kg4.311 AcceptanceRun 2 Surrogate Q % Recovery Limits 1,2-Dichloroethane-d4 82 53-142 Bromofluorobenzene 96 47-138 Toluene-d8 N 134 68-124 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Page 6 of 12 Semivolatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SC Electric and Gas Company Sample #1 SL12007-001 12/11/2017 1145 12/12/2017 Solid % Solids:80.3 12/12/2017 2152Project Name: N.West St & W.Johnson St Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270D 1 12/13/2017 1105 CMP2 12/12/2017 2135 59457 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Acenaphthene 83-32-9 8270D 160 1ug/kg6.216 Acenaphthylene 208-96-8 8270D ND 1ug/kg3.916 Acetophenone 98-86-2 8270D ND 1ug/kg8.582 Anthracene 120-12-7 8270D 52 1ug/kg3.216 Atrazine 1912-24-9 8270D ND 1ug/kg6.282 Benzaldehyde 100-52-7 8270D ND 1ug/kg6.182 Benzo(a)anthracene 56-55-3 8270D 18 1ug/kg2.416 Benzo(a)pyrene 50-32-8 8270D ND 1ug/kg2.116 Benzo(b)fluoranthene 205-99-2 8270D 12 J 1ug/kg2.416 Benzo(g,h,i)perylene 191-24-2 8270D ND 1ug/kg4.616 Benzo(k)fluoranthene 207-08-9 8270D ND 1ug/kg2.616 1,1'-Biphenyl 92-52-4 8270D ND 1ug/kg5.882 4-Bromophenyl phenyl ether 101-55-3 8270D ND 1ug/kg5.782 Butyl benzyl phthalate 85-68-7 8270D ND 1ug/kg4.382 Caprolactam 105-60-2 8270D ND 1ug/kg1582 Carbazole 86-74-8 8270D 12 J 1ug/kg5.182 bis (2-Chloro-1-methylethyl) ether 108-60-1 8270D ND 1ug/kg8.282 4-Chloro-3-methyl phenol 59-50-7 8270D ND 1ug/kg6.982 4-Chloroaniline 106-47-8 8270D ND 1ug/kg7.182 bis(2-Chloroethoxy)methane 111-91-1 8270D ND 1ug/kg4.382 bis(2-Chloroethyl)ether 111-44-4 8270D ND 1ug/kg6.782 2-Chloronaphthalene 91-58-7 8270D ND 1ug/kg1582 2-Chlorophenol 95-57-8 8270D ND 1ug/kg1382 4-Chlorophenyl phenyl ether 7005-72-3 8270D ND 1ug/kg4.982 Chrysene 218-01-9 8270D 11 J 1ug/kg3.816 Dibenzo(a,h)anthracene 53-70-3 8270D ND 1ug/kg3.716 Dibenzofuran 132-64-9 8270D 77 J 1ug/kg6.282 3,3'-Dichlorobenzidine 91-94-1 8270D ND 1ug/kg1282 2,4-Dichlorophenol 120-83-2 8270D ND 1ug/kg8.182 Diethylphthalate 84-66-2 8270D ND 1ug/kg4.982 Dimethyl phthalate 131-11-3 8270D ND 1ug/kg4.582 2,4-Dimethylphenol 105-67-9 8270D ND 1ug/kg1382 Di-n-butyl phthalate 84-74-2 8270D ND 1ug/kg1282 4,6-Dinitro-2-methylphenol 534-52-1 8270D ND 1ug/kg12410 2,4-Dinitrophenol 51-28-5 8270D ND 1ug/kg20410 2,4-Dinitrotoluene 121-14-2 8270D ND 1ug/kg15160 2,6-Dinitrotoluene 606-20-2 8270D ND 1ug/kg13160 Di-n-octylphthalate 117-84-0 8270D ND 1ug/kg1.582 bis(2-Ethylhexyl)phthalate 117-81-7 8270D ND 1ug/kg2.882 Fluoranthene 206-44-0 8270D 60 1ug/kg2.616 Fluorene 86-73-7 8270D 100 1ug/kg2.416 Hexachlorobenzene 118-74-1 8270D ND 1ug/kg6.082 Hexachlorobutadiene 87-68-3 8270D ND 1ug/kg1082 Hexachlorocyclopentadiene 77-47-4 8270D ND 1ug/kg7.9410 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Page 7 of 12 Semivolatile Organic Compounds by GC/MS Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SC Electric and Gas Company Sample #1 SL12007-001 12/11/2017 1145 12/12/2017 Solid % Solids:80.3 12/12/2017 2152Project Name: N.West St & W.Johnson St Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3546 8270D 1 12/13/2017 1105 CMP2 12/12/2017 2135 59457 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Hexachloroethane 67-72-1 8270D ND 1ug/kg6.782 Indeno(1,2,3-c,d)pyrene 193-39-5 8270D ND 1ug/kg3.316 Isophorone 78-59-1 8270D ND 1ug/kg7.682 2-Methylnaphthalene 91-57-6 8270D 1800 1ug/kg7.216 2-Methylphenol 95-48-7 8270D ND 1ug/kg2282 3+4-Methylphenol 106-44-5 8270D ND 1ug/kg20160 Naphthalene 91-20-3 8270D 590 1ug/kg5.816 2-Nitroaniline 88-74-4 8270D ND 1ug/kg23160 3-Nitroaniline 99-09-2 8270D ND 1ug/kg23160 4-Nitroaniline 100-01-6 8270D ND 1ug/kg25160 Nitrobenzene 98-95-3 8270D ND 1ug/kg9.682 2-Nitrophenol 88-75-5 8270D ND 1ug/kg9.6160 4-Nitrophenol 100-02-7 8270D ND 1ug/kg130410 N-Nitrosodi-n-propylamine 621-64-7 8270D ND 1ug/kg7.082 N-Nitrosodiphenylamine (Diphenylamine)86-30-6 8270D ND 1ug/kg6.382 Pentachlorophenol 87-86-5 8270D ND 1ug/kg33410 Phenanthrene 85-01-8 8270D 190 1ug/kg2.816 Phenol 108-95-2 8270D ND 1ug/kg7.782 Pyrene 129-00-0 8270D 41 1ug/kg3.516 2,4,5-Trichlorophenol 95-95-4 8270D ND 1ug/kg5.482 2,4,6-Trichlorophenol 88-06-2 8270D ND 1ug/kg5.982 AcceptanceRun 1 Surrogate Q % Recovery Limits 2-Fluorobiphenyl 87 24-137 2-Fluorophenol 81 16-136 Nitrobenzene-d5 80 12-144 Phenol-d5 81 26-148 Terphenyl-d14 89 20-127 2,4,6-Tribromophenol 90 27-128 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Page 8 of 12 RCRA Metals Description:Matrix: Date Received: Client:Laboratory ID: Date Sampled: SC Electric and Gas Company Sample #1 SL12007-001 12/11/2017 1145 12/12/2017 Solid % Solids:80.3 12/12/2017 2152Project Name: N.West St & W.Johnson St Project Number: Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch 1 3050B 6010D 1 12/13/2017 1315 CJZ 12/12/2017 1031 59389 1 7471B 7471B 1 12/13/2017 1040 COH 59476 AnalyticalCAS Parameter Number Method Result Q LOQ Units Run DL Arsenic 7440-38-2 6010D 0.30 J 1mg/kg0.240.71 Barium 7440-39-3 6010D 8.5 1mg/kg0.311.2 Cadmium 7440-43-9 6010D 0.13 J 1mg/kg0.0590.24 Chromium 7440-47-3 6010D 5.1 1mg/kg0.120.47 Lead 7439-92-1 6010D 2.0 1mg/kg0.210.47 Mercury 7439-97-6 7471B ND 1mg/kg0.0220.090 Selenium 7782-49-2 6010D ND 1mg/kg0.380.94 Silver 7440-22-4 6010D ND 1mg/kg0.120.47 J = Estimated result < LOQ and > DL_ LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the DL N = Recovery is out of criteria H = Out of holding time DL = Detection Limit W = Reported on wet weight basis 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Page 9 of 12 Chain of Custody and Miscellaneous Documents 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Page 10 of 12 SHEALY ENVIRONMENTAL SERVICES, INC. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Page 11 of 12 SHEALY ENVIRONMENTAL SERVICES, INC. 106 Vantage Point Drive West Columbia, SC 29172 (803) 791-9700 Fax (803) 791-9111 www.shealylab.com Shealy Environmental Services, Inc. Page 12 of 12