HomeMy WebLinkAboutRA-1913_11680_CA_MRP_20200316_GWMR FINAL
WithersRavenel
Our People. Your Success.
115 MacKenan Drive | Cary, NC 27511
t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C‐0832
Cary | Greensboro | Pittsboro | Raleigh | Wilmington
March 16, 2020
State of North Carolina
Department of Environmental Quality
Federal & State Lead Program
Division of Waste Management‐Underground Storage Tank Section
1646 Mail Service Center
Raleigh, North Carolina 27699‐1646
Attn: Mr. Mark Petermann
RE: SUBSEQUENT MONITORING REPORT
Former Shotwell’s Grocery
8681 US Highway 15 North
Bullock, Granville County, North Carolina
Groundwater Incident Number: 11680
Facility ID No.: 00‐0‐016798
WR Project Number: 02170214.17
Mr. Petermann:
WithersRavenel, Inc. (WR) has completed groundwater and supply well sampling activities and
emplacement of Provectus ORS Sleeves in select wells in association with our proposal
numbered TA‐07 for the above referenced site, approved by the UST Section on January 27,
2020. The enclosed report summarizes the results of these recently completed activities.
WR appreciates the opportunity to be of service to the Federal & State Lead Program. Should
you have any questions regarding the attached, please contact Matthew James at (919) 238‐
0335.
Cordially,
WithersRavenel
Kevin B. Buchanan G. Matthew James, PG
Staff Environmental Scientist II Senior Geologist
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TABLE OF CONTENTS
A.SITE INFORMATION ................................................................................................................................................... 3
B.EXECUTIVE SUMMARY ............................................................................................................................................. 4
C.SITE HISTORY AND CHARACTERIZATION.......................................................................................................... 7
D.PRESENTATION OF CURRENT/COMPARISON TO HISTORICAL ASSESSMENT
INFORMATION ............................................................................................................................................................. 13
E.CONCLUSIONS AND RECOMMENDATIONS ................................................................................................... 16
FIGURES
Figure 1 General Location Map
Figure 2 Site Map
Figure 3A Shallow Groundwater Hydraulic Gradient Map (ft) ‐ February 2020
Figure 3B Deep Groundwater Hydraulic Gradient Map (ft) ‐ February 2020
Figure 4 Analytical Results for Groundwater Samples – February 2020
Figure 5 Groundwater IPE Isoconcentration Map ‐ February 2020
Figure 6 Receptor Map with Supply Well Analytical Results Shown
TABLES
Table B‐1 Site History – UST/AST System and Other Release Information
Table B‐4 Summary of Groundwater Analytical Results
Table B‐5A Public & Private Water Supply Well Information
Table B‐5B Additional Receptor Information
Table B‐7 Monitoring and Remediation Well Construction Information
Table B‐9 Current & Historical Groundwater Elevations and Free Product Thickness’
APPENDICES
Appendix A Laboratory Analytical Report and Chain‐of‐Custody
Appendix B Copy of Field Notes
Appendix C Photographic Documentation
Appendix D General Standard Operating Procedures
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B. EXECUTIVE SUMMARY
1. Summary of Activities Associated with Current TA
WithersRavenel, Inc. (WR) gauged, purged and sampled monitoring wells DW‐1, M4, M6, M13,
M‐14, MW‐17, MW‐18, MW‐20, MW‐21, MW‐22, MW‐23, MW‐24, MW‐25, MW‐26, MW‐
26D, MW‐27 and MW‐27D, purged and sampled supply wells WSW‐8, WSW‐10, WSW‐12,
WSW‐14, WSW‐15 and WSW‐17.
2. Soil, Groundwater and Free Product Assessment Information
Soils
No soil sampling was performed at the facility in association with the current TA. Laboratory
analytical results for soil samples obtained from twelve soil borings located around the former
UST area (WR‐1 through WR‐12, inclusive) during September 2015 indicated the presence of
petroleum compounds at concentrations exceeding their respective Soil‐to‐Water Maximum Soil
Contaminant Concentrations (MSCCs) in five of the twelve samples submitted for analysis.
Although not defined to levels equivalent to the Soil‐to‐Water MSCCs, the analytical results for
these samples and those obtained by Marshal Miller Associates, Inc. (MMA) in August 1998 infer
that soil contamination in this area is limited to on‐site locations encompassing an area of
approximately 413 square feet (ft2), extending to the depth of the water table beneath the site.
Assuming a thickness of five ft, and not accounting for soils beneath the water table in a zone of
“smearing”, this equates to a total of 2,065 cubic ft (ft3) or about 76 cubic yards (yd3) of
contaminated soil. Petroleum‐contaminated soils appear to extend from near the southern end
of the pump island on the site towards the north‐northeast along the eastern side of the area
excavated by MMA in August 1998. It would be expected that petroleum compounds identified
in soils at the site would continue to leach to groundwater, ultimately posing an exposure risk to
receptors located downgradient of the source location.
The estimation of soil impact described above does not include the area in close proximity to the
Shotwell Grocery building from which a single soil sample (SS5A) showed tetrachloroethene
(PCE) at a concentration exceeding the Soil‐to‐Water MSCC for the compound. No assessment
of PCE impact in close proximity or beneath the building on the site has been undertaken, to
date.
Groundwater
Laboratory analytical results for groundwater samples obtained from monitoring wells associated
with the release at the site during February 2020 indicated the presence of one or more
petroleum‐related compounds in samples obtained from wells DW‐1, M‐4, M‐6, M‐14, MW‐18,
MW‐23, MW‐24, MW‐26D, MW‐27 and MW‐27D. One or more of the compounds detected in
samples from wells DW‐1, M‐4, M‐6, MW‐24, MW‐27 and MW‐27D were reported at
concentrations exceeding their respective 2L Standard(s) defined by NCAC Title 15A,
Subchapter 2L, Section .0202 (Water Quality Standards for Class GA Groundwater). None of the
compounds identified in the groundwater samples were reported at concentrations above their
respective Gross Contaminant Levels (GCLs). The greatest concentrations of contaminants were
noted in source area monitoring well MW‐24, consistent with previous data for the well.
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Contaminants in groundwater appear to extend hydraulically down‐gradient of the former UST
area to the north‐northeast. Based on current data, the lateral extent of groundwater
contamination relating to the release on the site extends approximately 375 ft to the northeast
of the source area, and its cross‐gradient extent increases from an initial (on‐site) width of
approximately 70 ft to an ultimate (downgradient) width of approximately 120 ft. In the surficial
aquifer, contaminants extend to as deep as approximately 25 ft at the location of monitoring well
M‐4. As impact was noted in groundwater samples obtained from Type III monitoring well MW‐
27D, transmission of contaminants into the bedrock aquifer from the overlying saprolitic
materials appears to be occurring, although it is not currently possible to quantify the location(s)
at which this transmission occurs. This was first noted at the site by MMA in their March 1998
Comprehensive Site Assessment (CSA).
The current extent of groundwater contamination to the northeast of the site has not been
defined to levels equivalent to the 2L Standards, and contaminants persist at down‐gradient, off‐
site locations. Current data, in comparison to that of samples obtained during September 2018,
have shown general stability of contaminant concentrations, however, contaminants persist at
levels exceeding their respective 2L Standards.
Free Product
Free product has not been measured in any wells relating to the release on the site, to date.
3. Receptor Information
A receptor survey update was conducted by Crawford Environmental Services (CES) as part of
the “Groundwater Monitoring Event Letter/Report” dated August 21, 2012. According to that
report, the subject property and surrounding properties are supplied water by domestic water
supply wells. The survey identified the presence of thirty‐three (33) supply wells within 1,000 ft
of the release area. The nearest surface water feature was identified as a man‐made pond
located on the western adjacent property approximately 150 ft west of the former UST basin
(source area). Land surface topography observed on the USGS map indicates that the
surrounding vicinity slopes to the northeast, in the direction of reported groundwater flow,
towards an unnamed tributary of Bear Pond Creek, located approximately 1,000 northeast of the
subject site.
Laboratory results for samples collected from supply wells showed IPE (WSW‐8 and WSW‐10)
and MTBE (WSW‐8 and WSW‐12) at concentrations beneath their respective 2L Standards.
1,2‐DCA and IPE were each reported in WSW‐12 at levels above their 2L Standards.
4. Remediation Activities
Three 1,000‐gallon gasoline USTs were reportedly closed by removal in January 1990.
Subsequent to closure of the USTs, source area soil excavation was performed in August 1998 in
an effort to remove as much impacted material as possible at the time. Beyond UST closures and
the source area soils excavation, the only (interim) remedial actions undertaken at the site, to
date have been the installation of Provectus® ORS Well sleeves in wells M‐4, MW‐24, MW‐27
and MW‐27D during September 2018, January 2019, May 2019 and August 2019.
5. Recommendations
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Based on the results of assessment and monitoring activities conducted at the site in association
with this TA, WR recommends the following:
Complete a receptor survey update for the site and surrounding properties.
Based on formulation of a timeline for implementation and agreement by NCDEQ, implement
the Corrective Action Plan (CAP) completed by WR in June 2016, including:
a) Completion and submittal of an UIC permit to allow for groundwater remediation at the
site,
b) The remediation of unsaturated and smear zone source area soils through excavation,
augmented by emplacement of Klozur CR® (persulfate and calcium peroxide), and
c) The reduction of source area groundwater concentrations through injection of Klozur®
One™ (sodium persulfate & iron EDTA). Note: based on the results of the clean water
injection test, WR anticipates the “injection “of material to occur as a “gravity drain” into
the affected groundwater, and resulting from design calculations, performance of the
injection of material over nine‐days’ time.
Implementation of the CAP would require the following in terms of monitoring:
Specific groundwater field testing with Klozur® field test kits to determine the viability and
distribution of injectant.
Sampling of groundwater at select locations at three‐month intervals to determine the
effectiveness of groundwater remediation.
Continued groundwater monitoring of the monitoring wells and water supply wells (WSW‐8,
WSW‐9, WSW‐10, WSW‐11, WSW‐12, WSW‐13, WSW‐14, WSW‐15, WSW‐23, and
WSW‐24) downgradient and within 500 ft of the release.
In conjunction with the implementation of the CAP, replacement of Provectus ORS®
Monitoring Well Socks in monitoring wells M‐4, MW‐24, MW‐27 and MW‐27D to enhance
in situ biodegradation.
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C. SITE HISTORY AND CHARACTERIZATION
WR completed groundwater and supply well sampling activities between February 13 and 14,
2020. The following information summarizes the site history and characterization.
UST Information
The locations of the former UST system, onsite improvements, and monitoring well locations are
depicted on Figure 2. The former USTs were located along the eastern edge of the onsite
building in the northeastern portion of the property. According to the “Comprehensive Site
Assessment Report” prepared by MM&A dated March 30, 1998, the three 1,000‐gallon USTs
were closed by removal in January 1990. No other known USTs currently exist at the site. At
present, three 1,000‐gallon aboveground storage tanks (ASTs) are situated along the southern
edge of the onsite building. These ASTs formerly contained gasoline and rest in separate steel
secondary containment structures. At the time of WR’s site activities, the ASTs were not in
operation as the subject site was vacant with no power connected to the building, onsite well, or
onsite gasoline dispensers. Table B‐1 summarizes information regarding the USTs that were
formerly utilized on the property. Site photographs are included in Appendix C.
2. Description of Release/General Assessment History
The following summary of the assessment history is based on WR’s review of historical files for
the subject incident:
In 1994, a complaint concerning a fuel odor in well water at the then “Walton residence”
located on the northern adjacent property at 8683 US Highway 15 N, prompted NCDENR to
sample well water in the vicinity of the subject site. Laboratory results indicated the presence
of 1,2‐dichloroethane and/or isopropyl ether (IPE), common gasoline additives, in water
supply wells located on the subject site property, the northern adjacent property, and the
eastern adjacent property containing the Bullock Post Office.
Field investigation activities were initiated by NCDENR (now NCDEQ) Technical Services
Unit (TSU) to determine the source of the petroleum contamination. In March 1995, the TSU
advanced and installed sixteen groundwater monitoring wells (M‐1 through M‐16) on
properties along US Highway 15 N. Details of the field investigation were summarized in the
May 1997 NCDENR TSU report entitled “Groundwater Pollution Incident #11860, Walton
Residence, Granville County, NC”. The results of the investigation revealed two potential
sources. Petroleum‐impacted soil and groundwater were detected in the area of the removed
USTs on the Shotwell property (subject site) and from a UST system operated at Williamson’s
Grill, a country store located approximately 700 ft north of the subject site at 8695 US
Highway 15 N. The report concluded that the former USTs operated on the Shotwell
property were most likely the source for the release of petroleum since 1,2‐dichloroethane
was not detected in soil or groundwater samples at the Williamson’s Grill site and was
detected in both water supply wells and monitoring wells on and adjacent to the Shotwell
property.
In response to the above TSU report, NCDENR issued a Notice of Violation (NOV) to Oxford
Oil Company on August 29, 1997. The subject site was assigned a high priority ranking due
to the impact of nearby water supply wells.
In January 1998, NCDENR installed point‐of‐entry (POE) systems at the residences located
at 8683, 8685, and 8687 US Highway 15 N to remove petroleum contamination from the
drinking water prior to the water entering the residential structures.
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MM&A prepared a “Comprehensive Site Assessment” report dated March 30, 1998. Field
activities associated with the report included the advancement of 16 soil borings in
December 1997. Results of the soil assessment activities indicated that onsite soil
contamination was limited to the former UST basin. February 1998, MM&M installed 7
“shallow” Type II groundwater monitoring wells (MW‐17 through MW‐23) and one “deep”
Type III groundwater monitoring well (DW‐1). Results of groundwater analysis revealed
concentrations of BTEX, MTBE, IPE, 1,2,4‐trimethylbenzene, and 1,2‐dichloroethane in
source area well M‐15 installed within the former UST basin. Concentrations of MTBE, IPE,
and 1,2‐dichloroethane were detected at concentrations above the 2L standard in offsite
shallow wells and appear to be migrating offsite in a northeasterly direction. Concentrations
of benzene, MTBE, and IPE were detected in the onsite deep well (DW‐1), above 2L
Standards. Concentrations of MTBE, IPE, and 1,2‐dichloroethane were also detected in
several samples collected from nearby water supply wells.
MM&A prepared a “Corrective Action Plan” report dated July 16, 1998. As presented in the
report, MM&A recommended excavating onsite source area soils found within the former
UST basin, the installation of a groundwater pump and treat system, and installing new
shallow bored wells on the surrounding impacted properties to provide safe drinking water
supplies.
MM&A prepared a “Soil Excavation Report” dated May 3, 1999 documenting the removal of
source area soils. MM&A excavated a 22 by 20‐foot area to a depth of 6 ft below land
surface (BLS) for a total of approximately 90 cubic yards. Benzene, ethylbenzene, di‐
isopropyl ether, naphthalene, and tetrachloroethene were detected above UST Soil‐to‐
Groundwater MSCCs in collected sidewall samples; however, the limits of the excavation
could not be extended due to the presence of the existing onsite building and property
boundaries.
The NCDENR issued a Notice of Regulatory Requirements (NORR) letter dated January 13,
2004 requesting the completion of a site reconnaissance receptor survey.
Stratus Environmental Services, LLP (Stratus) completed a “Comprehensive Site Assessment
Addendum” report dated March 12, 2008. WR was not provided this report for review. Upon
receiving the “Comprehensive Site Assessment Addendum” report, the NCDENR issued a
NORR letter dated July 31, 2008 concluding that the petroleum contamination at the subject
site had not been adequately characterized and requested the full extent of groundwater and
soil contamination at the site be defined. The letter also requested the completion of an
additional CAP following full characterization of the contamination.
The NCDENR issued a Notice of Violation (NOV) letter dated November 9, 2009
acknowledging the failure to submit a CAP within 60 days of receipt of the NORR letter
dated July 31, 2008.
Crawford Environmental Services, Inc. (CES) prepared a “Groundwater Monitoring Event
Letter/Report” dated August 21, 2012 documenting groundwater sampling activities and the
results of a receptor survey update. Petroleum compounds were detected above the 2L
Standards in groundwater monitoring wells M‐4, M‐6, and MW‐23. 1,2‐Dichloroethane, IPE,
and MTBE were detected at concentrations exceeding 2L Standards in the sample collected
from water supply well WSW‐12. Concentrations of petroleum‐related compounds were also
detected in water supply wells WSW‐8, WSW‐9, WSW‐10, and WSW‐15; however,
concentrations of chemicals detected in the wells did not exceed 2L Standards.
WR performed a groundwater and supply well sampling event at the site during July 2014.
Groundwater flow direction was shown to be in a northeastern direction towards the
unnamed tributary of Bear Pond Creek. Laboratory analytical results for the groundwater
samples showed the presence of 1,2‐dichloroethane, di‐isopropyl ether, and MTBE in well
M‐4 at concentrations that exceed the 2L standard. Petroleum‐associated compounds were
detected in wells M‐6, MW‐14, MW‐18, MW‐20, MW‐21, MW‐22, MW‐23, and DW‐1 but
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concentrations did not exceed 2L Standards. No free product was observed in the
monitoring wells. Laboratory analytical results showed 1,2‐dichloroethane and di‐isopropyl
ether in water supply well WSW‐12 at concentrations that exceed the 2L standard. No
compounds were detected above laboratory detection limits in samples collected from water
supply wells WSW‐8, WSW‐11, WSW‐14, and WSW‐15. The POE systems installed at the
residences located at 8683 and 8687 US Highway 15 N (water supply wells WSW‐8 and
WSW‐11, respectively) appeared to be functioning properly and maintaining acceptable
water quality conditions.
WR performed assessment activities at the site in September 2015 which included the
advancement and sampling of twelve soil borings (WR‐1 through WR‐12, inclusive),
installation of four Type II monitoring wells (MW‐24, MW‐25, MW‐26, and MW‐27), and the
installation of two Type III monitoring wells (MW‐26D and MW‐27D). WR also gauged,
purged and sampled monitoring wells M‐1, M‐4, M‐6, M‐13, M‐14, MW‐17, MW‐18, MW‐
20, MW‐21, MW‐22, MW‐23, MW‐24, MW‐25, MW‐26, MW‐26D, MW‐27, MW‐27D and
DW‐1, and purged and sampled supply wells WSW‐8, WSW‐9, WSW‐10 (both Pre‐ and
Post‐POE), WSW‐12 and WSW‐14. Analytical results for soil samples obtained from
locations across the subject site in September 2015 indicated the presence of one or more
petroleum‐related compounds in samples from each of the borings, with the exception of the
sample from WR‐12, which did not show any compounds at concentrations above the
laboratory MDL for EPA‐8260. One or more compounds detected in samples from borings
WR‐4, WR‐5, WR‐7, WR‐9 and WR‐10 were reported at concentrations exceeding their
respective Soil‐to‐Water MSCCs. No compounds were reported at levels exceeding their
respective Residential or Industrial/Commercial MSCCs. Analytical results for groundwater
samples obtained from site monitoring wells during September 2015 indicated one or more
targeted compounds in M‐4, M‐6, M‐14, MW‐18, MW‐20, MW‐21, MW‐23, MW‐24,
MW27 and MW‐27D. One or more compounds detected in samples from M‐4, M‐14, MW‐
24, MW‐27 and MW‐27D were reported at concentrations exceeding their respective 2L
Standards. No compounds identified in any samples obtained during September 2015 were
reported at concentrations exceeding their respective GCLs.
In April 2016, WR gauged, purged and sampled monitoring wells DW‐1, M‐1, M‐4, M‐6, M‐
13, M‐14, MW‐17, MW‐18, MW‐20, MW‐21, MW‐22, MW‐23, MW‐24, MW‐25, MW‐26,
MW‐26D, MW‐27 and MW‐27D, and purged and sampled supply wells WSW‐8, WSW‐10
(both pre‐ and post‐POE), WSW‐12, WSW‐14, WSW‐15 and WSW‐37. WR also performed
assessment and calculations associated with the preparation of the June 2016 CAP.
Laboratory analytical results indicated the presence of one or more petroleum‐related
compounds at concentrations exceeding their respective 2L Standard(s) in samples from M‐4,
MW‐20, MW‐23, MW‐24, MW‐27 and MW‐27D. None of the compounds identified in the
groundwater samples were reported at concentrations above their respective GCLs.
Analytical data for samples obtained from water supply wells WSW‐8, WSW‐9, WSW‐10
(both Pre‐ and Post‐POE), WSW‐12, WSW‐14, and WSW‐15 indicated the presence of one
or more targeted compounds at levels above the laboratory MDLfor SM6200B in samples
obtained from WSW‐8, WSW‐10 (both Pre‐ and Post‐POE) and WSW‐12. 1,2‐DCA was
reported in the samples obtained from WSW‐8 and WSW‐12 at concentrations exceeding
the 2L Standard for the compound, but beneath the Maximum Contaminant Level (MCL)
established by the US EPA, Region IV.
WR conducted assessment and monitoring activities at the site during August 2017 including
the installation of five 1‐inch diameter Type II observation wells (OW‐1 through OW‐5,
inclusive), conducted a clean water injection pilot test, and performed a site‐wide
groundwater and supply well sampling event. Performance of the clean water injection pilot
test confirmed the viability of “injection “of remedial materials at the location, albeit implied
influence observed in the performance of the injection test show that a low flow rate or
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“gravity feeding” will be necessary for successful emplacement of material. Laboratory
analytical results for groundwater samples obtained from monitoring wells associated with
the release at the site during August 2017 indicated the presence of one or more petroleum‐
related compounds in samples obtained from wells DW‐1, M‐4, MW‐18, MW‐21, MW‐22,
MW‐23, MW‐24, MW‐27 and MW‐27D. One or more of the compounds detected in
samples from wells M‐4, MW‐23, MW‐24, MW‐27 and MW‐27D were reported at
concentrations exceeding their respective 2L Standard(s). None of the compounds identified
in the groundwater samples were reported at concentrations above their respective GCLs.
The greatest concentrations of contaminants were noted in source area monitoring well
MW‐24, although levels of total contaminants reported in the sample were at the time
shown to have been decreased by 70% over the April 2016 data for the well. Analytical data
for samples obtained from water supply wells WSW‐8, WSW‐10 and WSW‐12 indicated the
presence of one or more targeted compounds at levels above the laboratory MDL for
SM6200B. 1,2‐DCA was reported in the sample obtained from WSW‐12 at a concentration
exceeding the 2L Standard for the compound. Data for samples from remaining supply wells
sampled during August 2017 did not show the presence of targeted compounds at
concentrations exceeding the laboratory MDL.
WR personnel abandoned monitoring well M‐1 (located on the Hayes property, north of the
site source location) on December 13, 2017. This well was abandoned as a result of a
request from the property owner on which the well was situated to either reconstruct the
well in a way which would limit the well exposure (e.g., install as a flush mounted well) or
abandon the well completely. After consulting with he NCDEQ Incident Manager (Mr. Mark
Petermann) it was decided to abandon the well, as historical data for samples from M‐1 had
not shown contaminant impact.
WR performed a groundwater and supply well sampling event during September 2018. One
or more compounds targeted by SM6200B were reported in groundwater samples obtained
from wells DW‐1, M‐4, M‐6 MW‐18, MW‐20, MW‐21, MW‐23, MW‐24, MW‐26D, MW‐27
and MW‐27D. One or more of the compounds detected in samples from wells MW‐24,
MW‐27 and MW‐27D were reported at concentrations exceeding their respective 2L
Standard(s). None of the compounds identified in the groundwater samples were reported
at concentrations above their respective GCLs. The greatest concentrations of contaminants
were noted in source area monitoring well MW‐24, although levels of total contaminants
reported in the sample were decreased by 54% over the August 2017 data for the well.
Based on the September 2018 groundwater sampling event performed at the location, the
extent of groundwater contamination had not been defined to the northeast of the source
area. Analytical data for samples obtained from water supply wells WSW‐10 and WSW‐12
indicated the presence of one or more targeted compounds at levels above the laboratory
MDL for SM6200B. 1,2‐DCA was reported in the sample obtained from WSW‐12 at a
concentration exceeding the 2L Standard for the compound. Data for samples from
remaining supply wells sampled during September 2018 did not show the presence of
targeted compounds at concentrations exceeding the laboratory MDL.
WR performed a limited groundwater sampling event at the location and emplaced
Provectus® ORS™ Sleeves in the wells (M‐4, MW‐24, MW‐27 and MW‐27D) after their
purging and sampling in January 2019. Analytical data for these samples showed one or
more target contaminants in each of the wells sampled. Several compounds were reported in
the samples obtained from wells M‐4, and MW‐24 at concentrations exceeding their
respective 2L Standards. A single compound (1,2‐dichloroethane) was reported in the
sample from MW‐27D at a level above the 2L Standard. No compounds were reported in
any of these samples at levels exceeding their respective GCLs.
WR performed a limited groundwater sampling event at the location and emplaced
Provectus® ORS™ Sleeves in the wells (M‐4, MW‐24, MW‐27 and MW‐27D) after their
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purging and sampling in May 2019. Analytical data for these samples showed one or more
target contaminants in each of the wells sampled. Several compounds were reported in the
samples obtained from wells M‐4 and MW‐24 at concentrations exceeding their respective
2L Standards. No compounds were reported in any of these samples at levels exceeding
their respective GCLs.
WR performed a limited groundwater sampling event at the location and emplaced
Provectus® ORS™ Sleeves in the wells (M‐4, MW‐24, MW‐27 and MW‐27D) after their
purging and sampling in August 2019. Analytical data for these samples showed one or more
target contaminants in each of the wells sampled at concentrations exceeding their
respective 2L Standards. No compounds were reported in any of these samples at levels
exceeding their respective GCLs.
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3. Brief Description of Site Characteristics
The property is located in Bullock, Granville County, North Carolina (Figure 1). The property
address is 8681 US Highway 15 North and includes a single‐story commercial building formerly
used as a convenience store/bait shop (Figure 2) situated on the eastern portion of a ±0.92‐acre
parcel. The Granville County Parcel ID No. for the property is 193901387114. Surface
coverings at the location include asphalt pavement, gravel and areas of grass and vegetative
growth. A concrete pump island, including three pumps associated with the former UST systems
on the site is located between the site structure and US Highway 15. An in‐ground hydraulic
cylinder associated with a former vehicle lift assembly is located along the southern exterior wall
of the building on the site, between the existing ASTs and the pump island. Municipal water
services are not presently available to the site or surrounding properties, and all occupied
properties rely entirely on private water supply wells for potable water.
The site lies at an approximate elevation of 425 ft above mean sea level (AMSL) and is relatively
flat. Overland drainage at the location is expected to move to the north and east, towards
Beaver Pond Creek, ultimately draining to the John H. Kerr Reservoir within the Roanoke River
Drainage Basin. Surface drainage along roadways adjacent to the site is channeled through man‐
made ditch lines and storm water conveyances, also discharging to the northeast of the site.
Buried storm drainage structures are located along the eastern property boundary of the site.
Groundwater flow direction documented through the course of site investigative activities tends
to mimic indications of overland flow, and given the relatively shallow groundwater elevations
measured at the location, groundwater may discharge to the surface to the northeast of the site.
4. Information on Receptors/Potential Receptors
A receptor survey update was conducted by CES as part of the “Groundwater Monitoring Event
Letter/Report” dated August 21, 2012. According to that report, the subject site and
surrounding properties are supplied water by domestic water supply wells. The survey identified
the presence of 33 supply wells within 1,000‐ft of the release area. The nearest surface water
feature was identified as a man‐made pond located on the western adjacent property
approximately 150 ft west of the former UST basin (source area). Land surface topography
observed on the USGS map indicates that the surrounding vicinity slopes to the northeast, in the
direction of reported groundwater flow, towards an unnamed tributary of Bear Pond Creek
located approximately 1,000 ft northeast of the subject site.
The nearest surface water feature was identified as the man‐made pond located on the western
adjacent property approximately 150 ft west of the source area.
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D. PRESENTATION OF CURRENT/COMPARISON TO HISTORICAL
ASSESSMENT INFORMATION
Between February 13 and 14, 2020, WR personnel mobilized to the subject site to perform
assessment and sampling activities in accordance with task authorization TA‐07. Activities
included those more thoroughly described in the following sections:
Groundwater Elevations/Free Product Level Measurements
Prior to the purging and sampling of site monitoring wells, as described below, WR personnel
opened and gauged each well targeted for sampling with an electronic free product/water level
indicator to determine the depth to groundwater within each of the wells. In the performance of
these activities, free product was not measured within any of the wells gauged as a part of site
investigation.
The depth to groundwater measurements in the monitoring wells across the site varied from 0.0
ft (“at”) top of casing (TOC) in monitoring wells M‐4 and MW‐23 to 8.13 ft beneath TOC (BTOC)
in monitoring well M‐13. It should be noted that WR personnel observed evidence that
groundwater was discharging to the surface in the vicinity of wells M‐4 and MW‐23 (e.g.,
saturated or near saturated surface soils).
Based on groundwater elevation measurements from February 2020, groundwater flow through
the site in the “shallow” aquifer appears to trend to the east, with a northerly component on the
northern portion of the area, and southeastern component to the east of the source area (on the
eastern side of US Highway 15). The surficial aquifer is likely influenced by probable surface
discharge to the north of Buckhorn Road. Gradient as determined through groundwater
elevation measurements obtained in February 2020 are generally consistent with past
interpretations of groundwater flow, however, influence of surface discharge in the vicinity of
M‐4 and MW‐23 north of Buckhorn Road impacts groundwater flow. Shallow groundwater
hydraulic gradient as determined based on February 2020 measurements is shown on Figure 3A.
Groundwater flow within the “deep” aquifer is depicted on Figure 3B, and shows flow to trend to
the east. Groundwater elevation measurement data for this event are presented in Table B‐7,
while historical groundwater elevation measurements are included in Table B‐9.
Groundwater Sampling and Analytical Results
Monitoring Well Sampling
WR personnel obtained groundwater samples from monitoring wells M‐4, M‐6, M‐13, M‐14,
MW‐17, MW‐18, MW‐20, MW‐21, MW‐22, MW‐23, MW‐24, MW‐25, MW‐26, MW‐26D,
MW‐27, MW‐27D and DW‐1 between February 13 and 14, 2020, following gauging and
purging. Prior to the purging and sampling of wells M‐4, MW‐24, MW‐27 and MW‐27D, WR
personnel removed the Provectus® ORS sleeves which had been installed in these wells in
August 2019.
Each well was purged and sampled through the use of dedicated disposable bailers as described
in the procedures outlined in Appendix E. Copies of field notes are included in Appendix B.
Following purging, samples were decanted directly from the bailer(s) into laboratory prepared
sample containers holding appropriate preservative(s) as required. Groundwater samples were
submitted to Waypoint Analytical, LLC (Waypoint), formerly Prism Laboratories, Inc. (Prism) for
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analysis by SM6200B (VOCs). The laboratory analytical report and chain‐of‐custody records
associated with these samples are included in Appendix A.
Laboratory Results
Analytical data for groundwater samples obtained from site monitoring wells during February
2020 indicated:
Laboratory analytical results for groundwater samples obtained from monitoring wells associated
with the release at the site during February 2020 indicated the presence of one or more
petroleum‐related compounds in samples obtained from wells DW‐1, M‐4, M‐6, M‐14, MW‐18,
MW‐23, MW‐24, MW‐26D, MW‐27 and MW‐27D. One or more of the compounds detected in
samples from wells DW‐1, M‐4, M‐6, MW‐24, MW‐27 and MW‐27D were reported at
concentrations exceeding their respective 2L Standards. None of the compounds identified in
the groundwater samples were reported at concentrations above their respective GCLs. The
greatest concentrations of contaminants were noted in source area monitoring well MW‐24,
consistent with previous data for the well.
Current data, in comparison to that of samples obtained during previous sampling events showed
increases in contaminants in wells DW‐1, M‐6 and MW‐24. Contaminant increases in these
wells were not, however, substantial. Data for remaining wells showed contaminant
concentrations to be relatively stable.
WR personnel noted the presence of very shallow groundwater and near saturated surface soils
in the vicinity of monitoring wells M‐4 and MW‐23. This is borne out by the implied shallow
groundwater hydraulic gradient (Figure 3A) based on water level elevations as measured during
February 2020.
Changes in total contaminants for select wells between the September 2018 and February 2020
sampling events are shown in the following table:
September 2018 February 2020
DW‐1 5.55 141.51 2450%Increase
M‐4 16.56 280 1591%Increase
M‐6 3.91 4 2%Increase
M‐14 0 0.9 100%Increase
MW‐18 7.1 8.36 18%Increase
MW‐21 5.64 0 -100%Decrease
MW‐22 000%Stable
MW‐23 34.46 21.9 -36%Decrease
MW‐24 3345 8208 145%Increase
MW‐27 82.8 99 20%Increase
MW‐27D 212.11 166.75 -21%Decrease
Total Compounds (ug/L)Difference TrendWell ID
Changes in Total Compounds Reported in Groundwater Samples: September 2018 - February 2020
Although both increases and decreases of total contaminants were shown in several wells, the
changes are not thought to be statistically significant, based on the relatively low levels of
contaminants reported.
Based on the presence of specific contaminants (1,2‐DCA, IPE and MTBE) in samples retained
from Type III well MW‐27D, groundwater within a water‐bearing fracture or fractures within the
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well appears to have been impacted by the release on the site. It is currently unclear whether
fractures correspond to water‐bearing zone(s) within surrounding supply wells. With these
compounds having been detected in three of the water supply wells located in proximity to the
site, there is strong likelihood that there is a connection, at least in these 3 wells.
The groundwater analytical results are summarized in Table B‐4 and shown on Figure 4. An
isoconcentration map showing an estimate of IPE in groundwater is shown on Figure 5.
Supply Well Sampling and Analytical Results
Supply Well Sampling
WR personnel obtained supply well samples from WSW‐8, WSW‐10, WSW‐12, WSW‐14,
WSW‐15 and WSW‐17 on February 14, 2020 following purging. Each well was purged by
allowing the associated well pump to run continuously for a minimum of ten (10) minutes, after
which samples were decanted directly from the sample point(s) into laboratory‐prepared sample
containers holding appropriate preservative(s) as required. Supply well samples were submitted
to Waypoint for analysis by SM6200B.
Laboratory Results
Analytical data for samples obtained from water supply wells WSW‐8, WSW‐10 and WSW‐12
indicated the presence of one or more targeted compounds at levels above the laboratory MDL
for SM6200B. 1,2‐DCA and IPE were reported in the sample obtained from WSW‐12 at
concentrations exceeding the 2L Standards for the compounds. Data for samples from
remaining supply wells sampled during February 2020 did not show the presence of targeted
compounds at concentrations exceeding the laboratory MDL. The laboratory analytical report
and chain‐of‐custody record associated with these samples are included in Appendix A.
Analytical results for those supply wells sampled in association with this TA are also shown on
Figure 6.
Interim Remedial Action
Provectus ORS Sleeve Installations
Following the purging and sampling of monitoring wells M‐4, MW‐24, MW‐27 and MW‐27D,
Provectus ORS Well Sleeves were emplaced within these locations to aid in possible attenuation
of contaminants in groundwater. These sleeves were installed as replacements for Unirem® PRP
Well Booms which had been placed into the wells in August 2019.
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E. CONCLUSIONS AND RECOMMENDATIONS
This report documents the results of field activities conducted at the site during February 2020,
which included the purging and sampling of monitoring wells M‐4, M‐6, M‐13, M‐14, MW‐17,
MW‐18, MW‐20, MW‐21, MW‐22, MW‐23, MW‐24, MW‐25, MW‐26, MW‐26D, MW‐27,
MW‐27D and DW‐1, the purging and sampling of supply wells WSW‐8, WSW‐10, WSW‐12,
WSW‐14, WSW‐15 and WSW‐17. Data obtained during these assessment and sampling
activities combined with historical information show the following:
All occupied properties located within 1,000 ft of the site rely on private water supply wells
for provision of potable water, and several supply wells located within that radius have been
impacted by the release on the site, including WSW‐8, WSW‐10 and WSW‐12.
No wellhead protection areas have been identified within ½ mile of the site, and no
municipally‐operated water utility approaches within several miles of the site.
Data for soil samples retained in association with the installation of twelve soil borings at the
site in locations surrounding the former UST area (WR‐1 through WR‐12, inclusive) during
September 2015 indicated the presence of targeted petroleum compounds at concentrations
exceeding their respective Soil‐to‐Water MSCCs in five of the twelve samples submitted for
analysis. Although not defined to levels equivalent to the Soil‐to‐Water MSCCs, data for
these soil samples, and those obtained by MMA in August 1998, tend to infer that soil
contamination at the location is limited to on‐site areas.
Based on groundwater elevation measurements from February 2020, groundwater flow
through the site in the “shallow” aquifer appears to trend to the east, with a northerly
component on the northern portion of the area, and southeastern component to the east of
the source area (on the eastern side of US Highway 15). The surficial aquifer is likely
influenced by probable surface discharge to the north of Buckhorn Road. Gradient as
determined through groundwater elevation measurements obtained in February 2020 are
generally consistent with past interpretations of groundwater flow, however, influence of
surface discharge in the vicinity of M‐4 and MW‐23 north of Buckhorn Road impacts
groundwater flow.
Data for groundwater samples obtained from monitoring wells associated with the release at
the site during February 2020 indicated the presence of one or more petroleum‐related
compounds in samples obtained from wells DW‐1, M‐4, M‐6, M‐14, MW‐18, MW‐23, MW‐
24, MW‐26D, MW‐27 and MW‐27D. One or more of the compounds detected in samples
from wells DW‐1, M‐4, M‐6, MW‐24, MW‐27 and MW‐27D were reported at
concentrations exceeding their respective 2L Standards. None of the compounds identified
in the groundwater samples were reported at concentrations above their respective GCLs.
The greatest concentrations of contaminants were noted in source area monitoring well
MW‐24, consistent with previous data for the well. Current data, in comparison to that of
samples obtained during previous sampling events showed increases in contaminants in wells
DW‐1, M‐6 and MW‐24. Contaminant increases in these wells were not, however,
substantial. Data for remaining wells showed contaminant concentrations to be relatively
stable.
While data for groundwater samples obtained during February 2020 showed both increases
and decreases of contaminant concentrations in selected wells, the relatively low
concentrations were generally consistent with those from samples obtained during
September 2018. Also owed to the relatively low contaminant concentrations identified in
groundwater samples, the changes are not thought to be statistically significant. This trend
may relate to “contaminant washing” through water‐bearing strata, in combination with the
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installation and periodic replacement of Provectus® ORS sleeves in monitoring wells M‐4,
MW‐24, MW‐27 and MW‐27D.
Although the extent of groundwater contamination has not been defined to the northeast,
the greatest concentrations of contaminants were noted in the vicinity of monitoring well
MW‐24, situated in close proximity to the source area on the site, and MW‐27 to the
northeast. Contaminants appear to extend hydraulically down‐gradient of the former UST
area to the north‐northeast of the source area.
Based on the presence of specific contaminants (1,2‐DCA, IPE and MTBE) in samples
retained from Type III well MW‐27D, groundwater within a water‐bearing fracture or
fractures within the well appears to have been impacted by the release on the site. It is
currently unclear whether the fracture(s) correspond to water‐bearing zone(s) within
surrounding supply wells. With these compounds being detected in three of the water
supply wells tested, there is strong likelihood that there is a connection, at least in these
three wells.
Analytical data for samples obtained from water supply wells WSW‐8, WSW‐10 and WSW‐
12 indicated the presence of one or more targeted compounds at levels above the laboratory
MDL for SM6200B. 1,2‐DCA and IPE were reported in the sample obtained from WSW‐12
at concentrations exceeding the 2L Standards for the compounds. Based on Department
information and a previous interview with the property owner, water from WSW‐12 is not
used for potable use but for flushing toilets and cleaning purposes only.
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Based on the results of assessment and monitoring activities conducted at the site in association
with this TA, WR recommends the following:
Complete a receptor survey update for the site and surrounding properties.
Based on formulation of a timeline for implementation and agreement by NCDEQ, implement
the Corrective Action Plan (CAP) completed by WR in June 2016, including:
d) Completion and submittal of an UIC permit to allow for groundwater remediation at the
site,
e) The remediation of unsaturated and smear zone source area soils through excavation,
augmented by emplacement of Klozur CR® (persulfate and calcium peroxide), and
f) The reduction of source area groundwater concentrations through injection of Klozur®
One™ (sodium persulfate & iron EDTA). Note: based on the results of the clean water
injection test, WR anticipates the “injection “of material to occur as a “gravity drain” into
the affected groundwater, and resulting from design calculations, performance of the
injection of material over nine‐days’ time.
Implementation of the CAP would require the following in terms of monitoring:
Specific groundwater field testing with Klozur® field test kits to determine the viability and
distribution of injectant.
Sampling of groundwater at select locations at three‐month intervals to determine the
effectiveness of groundwater remediation.
Continued groundwater monitoring of the monitoring wells and water supply wells (WSW‐8,
WSW‐9, WSW‐10, WSW‐11, WSW‐12, WSW‐13, WSW‐14, WSW‐15, WSW‐23, and
WSW‐24) downgradient and within 500 ft of the release.
In conjunction with the implementation of the CAP, replacement of Provectus ORS®
Monitoring Well Socks in monitoring wells M‐4, MW‐24, MW‐27 and MW‐27D to enhance
in situ biodegradation.
FIGURES
TABLES
UST IDNumberCurrent/LastContentsPreviousContentsCapacity(in gallons)ConstructionDetailsTankDimensions (diameter x length) (ft)Description ofAssociatedPiping & PumpsDate of TankInstallationStatus ofUSTWas release associated with UST System? (Y/N)1 Gasoline N/A 1,000 Steel ~4.0 x 10.83 N/A UnknownPermanently Closed by Removal (January 1990)Y2 Gasoline N/A 1,000 Steel ~4.0 x 10.83 N/A UnknownPermanently Closed by Removal (January 1990)Y3 Gasoline N/A 1,000 Steel ~4.0 x 10.83 N/A UnknownPermanently Closed by Removal (January 1990)YAST IDNumberCurrent/LastContentsPreviousContentsCapacity(in gallons)ConstructionDetailsTankDimensions (diameter x length) (ft)Description ofAssociatedPiping & PumpsDate of TankInstallationStatus ofASTWas release associated with AST System? (Y/N)1 Gasoline N/A 1,000Steel w/SecondaryContainment~4.0 x 10.0 N/A Unknown Not In Use N2 Gasoline N/A 1,000Steel w/SecondaryContainment~4.0 x 10.0 N/A Unknown Not In Use N3 Gasoline N/A 1,000Steel w/SecondaryContainment~4.0 x 10.0 N/A Unknown Not In Use NIncident NumberMaterialReleasedDateofRelease11680 Gasoline UnknownTable B-1Site History: UST/AST System & Other Release InformationSHOTWELL'S GROCERYUST release was detected as petroleum contamination was identified in soil samples collected during tank closure activities.8681 US Highway 15 NIncident Number: 11680Bullock, Granville County, North CarolinaDescription of ReleasePage 1 of 1
CalculatedAcetone Benzene sec‐Butylbenzene tert‐Butylbenzene Chloroethane Chloroform 1,2‐DichloroethaneEthanol Ethylbenzene Hexachloro‐1,3‐butadiene Diisopropyl ether Isopropylbenzene (Cumene)Isopropyltoluene, 4‐ MBK, Methyl Butyl Ketone (2‐Hexanone) Methylene Chloride Methyl‐tert‐butyl etherMIBK (4‐Methyl‐2‐pentanone) Naphthalene n‐Propylbenzene Styrene Toluene 1,2,4‐Trimethylbenzene 1,3,5‐TrimethylbenzeneTotal Xylene67‐64‐171‐43‐2135‐98‐898‐06‐675‐00‐367‐66‐3 107‐06‐264‐17‐5100‐41‐487‐68‐3108‐20‐398‐82‐899‐87‐6591‐78‐675‐09‐21634‐04‐4108‐10‐191‐20‐3 103‐65‐1100‐42‐5108‐88‐395‐63‐6108‐67‐81330‐20‐77/2/2014NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.01.4<0.50 NR NR <2.07.5NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/30/2015NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.01.6NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/5/2016NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/2/2017NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.02.5<0.50 NR NR <2.02.1NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/25/2018NR <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 NR <1.00 <1.00 NR <1.00 NR NR <5.005.55NR <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <22/13/2020<10 <0.048 <0.076 <0.088 <0.22 <0.076 0.51<27 <0.061 <0.16 82<0.054 <0.089 <0.065 <0.083 59<0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 7/2/2014NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/29/2015NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/6/2016NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/2/2017NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.07/2/2014NR <0.50 <0.50 <0.50 <1.0 <0.501.5NR <0.50 <2.0298<0.50 NR NR <2.044.1NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/29/2015NR <1.0 <1.0 <1.0 <2.0 <1.03.4NR <1.0 <4.0430<1.0 NR NR <4.092.2NR <4.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.04/6/2016NR <1.2 <1.2 <1.2 <2.5 <1.22.4NR <1.2 <5.0358<1.2 NR NR <5.059.5NR <5.0 <1.2 <1.2 <1.2 <1.2 <1.2 <2.58/2/2017NR <1.2 <1.2 <1.2 <2.5 <1.22.5NR <1.2 <5.0452<1.2 NR NR5.6 81.4NR <5.0 <1.2 <1.2 <1.2 <1.2 <1.2 <2.59/28/2018NR <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 NR <1.00 <1.00 NR <1.00 NR NR <5.0012.9NR <5.00 <1.00 <1.003.66<1.00 <1.00 <21/16/2019<10 <0.048 <0.076 <0.088 <0.22 <0.076 1.9 650<27 <0.061 <0.16 <0.065 <0.054 <0.089 <0.083 <0.078 110<0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.126/20/2019 16<0.048 <0.076 <0.088 <0.22 <0.076 1<27 <0.061 <0.16 420<0.054 <0.089 <0.065 <0.083 84<0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 8/29/2019 27<0.048 <0.076 <0.088 <0.22 <0.076 1.5<27 <0.061 <0.16 550<0.054 <0.089 <0.065 <0.083 110<0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 2/14/2020<10 <0.048 <0.076 <0.088 <0.22 <0.076 <0.066 <27 <0.061 <0.16 230<0.054 <0.089 <0.065 <0.083 50<0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 7/2/2014NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.05.8<0.50 NR NR <2.00.92NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/29/2015NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.06.5<0.50 NR NR <2.00.95NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/5/2016NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.01.9<0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/2/2017NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.02.7<0.50 NR NR <2.00.53NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/25/2018NR <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 NR <1.00 <1.00 NR <1.00 NR NR <5.00 <1.00 NR <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <22/14/2020<10 <0.048 <0.076 <0.088 <0.22 <0.076 <0.066 <27 <0.061 <0.16 230<0.054 <0.089 <0.065 <0.083 50<0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 9/29/2015NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/5/2016NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/2/2017NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/25/2018NR <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 NR <1.00 <1.00 NR <1.00 NR NR <5.00 <1.00 NR <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <22/13/2020<10 <0.048 <0.076 <0.088 <0.22 <0.076 <0.066 <27 <0.061 <0.16 <0.050 <0.054 <0.089 <0.065 <0.083 <0.042 <0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 7/2/2014NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.00.71<0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/29/2015NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR11.8<0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/6/2016NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.01.8<0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/2/2017NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/28/2018NR <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 NR <1.00 <1.00 NR <1.00 NR NR <5.00 <1.00 NR <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <22/14/2020<10 <0.048 <0.076 <0.088 <0.22 <0.076 <0.066 <27 <0.061 <0.16 0.9<0.054 <0.089 <0.065 <0.083 <1 <0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 7/2/2014NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/29/2015NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/5/2016NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/2/2017NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/25/2018NR <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 NR <1.00 <1.00 NR <1.00 NR NR <5.00 <1.00 NR <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <22/13/2020<10 <0.048 <0.076 <0.088 <0.22 <0.076 <0.066 <27 <0.061 <0.16 <0.050 <0.054 <0.089 <0.065 <0.083 <0.042 <0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 6000 1 70 70 3000 70 0.4 NL 600 0.4 70 70 NL NL 5 20 NL 6 70 70 600 400 400 500NL 5 NL NL NL NL 5 NL 700 NL NL NL NL NL NL NL NL NL NL 100 1,000 NL NL 10,0006000000 5,000 8,500 15,000 NL 70,000 400 NL 84,500 400 70,000 25,000 117 NL 5,000 20,000 100000 6,000 3,000 70,000 260,000 28,500 25,000 85,500Notes:1)2)3)4)5)6)7)NL= Compound Not ListedResultResultResult= Result Exceeds 2L Standard= Result Exceeds GCLGCLs for Groundwater = NCDENR UST Section Gross Contamination Levels for GroundwaterUS EPA MCL = Maximum Contaminant Level ‐ The highest level of a contaminant that is allowed in drinking water per the National Primary Drinking Water Regulations. For the purposes of this table the MCL applies to supply well samples only.Chemical Abstract (CAS) Number provided beneath compound names. WR personnel mistakenly identified a spigot located at the Bullock Baptist Church as being associated with supply well WSW‐37, which has been abandoned. WR personnel sampled this spigot without knowledge that the sample was actually originating from WSW‐14. = Result Exceeds Laboratory Detection LimitsM‐6M‐13M‐14NC 2L Standard US EPA MCLGCLs for GroundwaterAll results provided in ug/L (micrograms per liter) or parts per billionCompounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of constituents. NC 2L Standard ‐ North Carolina Groundwater Quality Standard as per NC Administrative Code 15A NCAC 02LSampleIDDateCollectedDW‐1M‐1M‐4Analytical MethodSM6200BTABLE B‐4SUMMARY OF GROUNDWATER ANALYTICAL RESULTSSHOTWELL'S GROCERYIncident Number: 116808681 US Highway 15 NBullock, Granville County, North CarolinaMW‐17Page 1 of 4
CalculatedAcetone Benzene sec‐Butylbenzene tert‐Butylbenzene Chloroethane Chloroform 1,2‐DichloroethaneEthanol Ethylbenzene Hexachloro‐1,3‐butadiene Diisopropyl ether Isopropylbenzene (Cumene)Isopropyltoluene, 4‐ MBK, Methyl Butyl Ketone (2‐Hexanone) Methylene Chloride Methyl‐tert‐butyl etherMIBK (4‐Methyl‐2‐pentanone) Naphthalene n‐Propylbenzene Styrene Toluene 1,2,4‐Trimethylbenzene 1,3,5‐TrimethylbenzeneTotal Xylene67‐64‐171‐43‐2135‐98‐898‐06‐675‐00‐367‐66‐3 107‐06‐264‐17‐5100‐41‐487‐68‐3108‐20‐398‐82‐899‐87‐6591‐78‐675‐09‐21634‐04‐4108‐10‐191‐20‐3 103‐65‐1100‐42‐5108‐88‐395‐63‐6108‐67‐81330‐20‐7SampleIDDateCollectedAnalytical MethodSM6200BTABLE B‐4SUMMARY OF GROUNDWATER ANALYTICAL RESULTSSHOTWELL'S GROCERYIncident Number: 116808681 US Highway 15 NBullock, Granville County, North Carolina7/2/2014NR <0.501.2 1.2<1.0 <0.50 <0.50 NR <0.50 <2.017.1<0.50 NR NR <2.05.6NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/29/2015NR <0.501.3 1<1.0 <0.50 <0.50 NR <0.50 <2.012<0.50 NR NR <2.03.9NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/5/2016NR <0.500.8 0.63<1.0 <0.50 <0.50 NR <0.50 <2.03.9<0.50 NR NR <2.01.3NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/1/2017NR <0.500.97 0.8<1.0 <0.50 <0.50 NR <0.50 <2.08.5<0.50 NR NR <2.03.1NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/25/2018NR <1.00 <1.001.03<5.00 <5.00 <1.00 NR <1.00 <1.00 NR <1.00 NR NR <5.001.77NR <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <22/13/2020<10 <0.048 0.59 0.97<0.22 <0.076 <0.066 <27 <0.061 <0.16 5<0.054 <0.089 <0.065 <0.083 1.8<0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 7/2/2014NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.01.8<0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/29/2015NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.03.6<0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/6/2016NR1.4<0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.070<0.50 NR NR <2.06.7NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/2/2017NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/25/2018NR <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 NR <1.00 <1.00 NR <1.00 NR NR <5.00 <1.00 NR <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <22/14/2020<10 <0.048 <0.076 <0.088 <0.22 <0.076 <0.066 <27 <0.061 <0.16 <0.050 <0.054 <0.089 <0.065 <0.083 <0.042 <0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 7/2/2014NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.032.4<0.50 NR NR <2.02NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/29/2015NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.020<0.50 NR NR <2.01.5NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/5/2016NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.08.2<0.50 NR NR <2.00.77NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/2/2017NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.09.4<0.50 NR NR <2.01.1NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/25/2018NR <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 NR <1.00 <1.00 NR <1.00 NR NR <5.00 <1.00 NR <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <22/14/2020<10 <0.048 <0.076 <0.088 <0.22 <0.076 <0.066 <27 <0.061 <0.16 <0.050 <0.054 <0.089 <0.065 <0.083 <0.042 <0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 7/2/2014NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.05.5<0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/29/2015NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/6/2016NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.00.76<0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/2/2017NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.01.5<0.50 NR NR <2.00.75NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/28/2018NR <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 NR <1.00 <1.00 NR <1.00 NR NR <5.00 <1.00 NR <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <22/14/2020<10 <0.048 <0.076 <0.088 <0.22 <0.076 <0.066 <27 <0.061 <0.16 <0.050 <0.054 <0.089 <0.065 <0.083 <0.042 <0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 7/2/2014NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.064<0.50 NR NR <2.05.9NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/29/2015NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.012.9<0.50 NR NR <2.01.7NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/6/2016NR <0.50 <0.50 <0.50 <1.0 <0.501.4NR <0.50 <2.0250<0.50 NR NR <2.037.3NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/2/2017NR <1.0 <1.0 <1.0 <2.0 <1.01.1NR <1.0 <4.0227<1.0 NR NR5.3 38.6NR <4.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.09/25/2018NR <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 NR <1.00 <1.00 NR <1.00 NR NR <5.005.06NR <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <22/14/2020<10 <0.048 <0.076 <0.088 <0.22 <0.076 <0.066 <27 <0.061 <0.16 18<0.054 <0.089 <0.065 <0.083 3.9<0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 9/29/2015NR2220 7.5<0.50<1.0<0.501.9NR2380<2.01780 93.2NR NR <2.0280NR198 212 10.8 9600 973 256 73704/5/2016NR1720<25.0 <25.0 <50.0 <25.0 <25.0 NR2380<1001010 83.6NR NR <100147NR286 202<25.09260 1080 273 81008/1/2017NR690<5.0 <5.0 <10.0 <5.0 <5.0 NR1120<20.0695 41.9NR NR <20.0108NR111<5.0 <5.01330 373 96.4 26489/25/2018NR44.5<1.00 <1.00 <5.00 <5.00 <1.00 NR384<1.00 NR <1.00 NR NR <5.0016.6NR57.9 107<1.00626 363 145 14911/16/2019<0.31 370 4.1<0.088 <0.22 <0.076 <0.066 210<27990<0.16 <0.065 38 2<0.083 3.1 40 87 97<0.047 4400 540 140 42006/20/2019<1001300 15<0.88 <2.2 <0.76 <5.0 <270 870<1.6 1900 24<0.89 <0.65 <0.83 210<1065 54<0.47 6500 300 81 33008/29/2019 140 230 4.6<0.088 <0.22 <0.076 0.54<27 530<0.16 470 24 2 2.8<0.083 74 3.8 48 65 0.63 990 290 85 16002/13/2020<3.1 130 16<0.88 <2.2 <0.76 <0.66 <270 770<1.6 140 61 10<0.65 <0.83 21<0.78 110 200<0.47 1500 1200 350 37006000 1 70 70 3000 70 0.4 NL 600 0.4 70 70 NL NL 5 20 NL 6 70 70 600 400 400 500NL 5 NL NL NL NL 5 NL 700 NL NL NL NL NL NL NL NL NL NL 100 1,000 NL NL 10,0006000000 5,000 8,500 15,000 NL 70,000 400 NL 84,500 400 70,000 25,000 117 NL 5,000 20,000 100000 6,000 3,000 70,000 260,000 28,500 25,000 85,500Notes:1)2)3)4)5)6)7)NL= Compound Not ListedResultResultResultChemical Abstract (CAS) Number provided beneath compound names. WR personnel mistakenly identified a spigot located at the Bullock Baptist Church as being associated with supply well WSW‐37, which has been abandoned. WR personnel sampled this spigot without knowledge that the sample was actually originating from WSW‐14. = Result Exceeds Laboratory Detection Limits= Result Exceeds 2L Standard= Result Exceeds GCLAll results provided in ug/L (micrograms per liter) or parts per billionCompounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of constituents. NC 2L Standard ‐ North Carolina Groundwater Quality Standard as per NC Administrative Code 15A NCAC 02LGCLs for Groundwater = NCDENR UST Section Gross Contamination Levels for GroundwaterUS EPA MCL = Maximum Contaminant Level ‐ The highest level of a contaminant that is allowed in drinking water per the National Primary Drinking Water Regulations. For the purposes of this table the MCL applies to supply well samples only.NC 2L Standard US EPA MCLGCLs for GroundwaterMW‐18MW‐20MW‐21MW‐22MW‐23MW‐24Page 2 of 4
CalculatedAcetone Benzene sec‐Butylbenzene tert‐Butylbenzene Chloroethane Chloroform 1,2‐DichloroethaneEthanol Ethylbenzene Hexachloro‐1,3‐butadiene Diisopropyl ether Isopropylbenzene (Cumene)Isopropyltoluene, 4‐ MBK, Methyl Butyl Ketone (2‐Hexanone) Methylene Chloride Methyl‐tert‐butyl etherMIBK (4‐Methyl‐2‐pentanone) Naphthalene n‐Propylbenzene Styrene Toluene 1,2,4‐Trimethylbenzene 1,3,5‐TrimethylbenzeneTotal Xylene67‐64‐171‐43‐2135‐98‐898‐06‐675‐00‐367‐66‐3 107‐06‐264‐17‐5100‐41‐487‐68‐3108‐20‐398‐82‐899‐87‐6591‐78‐675‐09‐21634‐04‐4108‐10‐191‐20‐3 103‐65‐1100‐42‐5108‐88‐395‐63‐6108‐67‐81330‐20‐7SampleIDDateCollectedAnalytical MethodSM6200BTABLE B‐4SUMMARY OF GROUNDWATER ANALYTICAL RESULTSSHOTWELL'S GROCERYIncident Number: 116808681 US Highway 15 NBullock, Granville County, North Carolina9/29/2015NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/5/2016NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/2/2017NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/25/2018NR <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 NR <1.00 <1.00 NR <1.00 NR NR <5.00 <1.00 NR <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <22/13/2020<10 <0.048 <0.076 <0.088 <0.22 <0.076 <0.066 <27 <0.061 <0.16 <0.050 <0.054 <0.089 <0.065 <0.083 <0.042 <0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 9/29/2015NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/5/2016NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.03.5<0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/2/2017NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/25/2018NR <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 NR <1.00 <1.00 NR <1.00 NR NR <5.00 <1.00 NR <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <22/13/2020<10 <0.048 <0.076 <0.088 <0.22 <0.076 <0.066 <27 <0.061 <0.16 3.5<0.054 <0.089 <0.065 <0.083 <1 <0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 9/29/2015NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/5/2016NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/2/2017NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/25/2018NR <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 NR <1.00 <1.00 NR <1.00 NR NR <5.00 <1.00 NR <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <22/13/2020<10 <0.048 <0.076 <0.088 <0.22 <0.076 <0.066 <27 <0.061 <0.16 <0.050 <0.054 <0.089 <0.065 <0.083 <0.042 <0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 9/29/2015NR <0.50 <0.50 <0.50 <1.0 <0.501.3NR <0.50 <2.0102<0.50 NR NR <2.013.5NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/6/2016NR <0.50 <0.50 <0.50 <1.0 <0.500.71NR <0.50 <2.038<0.50 NR NR <2.04.6NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/2/2017NR <0.50 <0.50 <0.50 <1.0 <0.500.97NR <0.50 <2.060.1<0.50 NR NR <2.08.3NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/25/2018NR <1.00 <1.00 <1.00 <5.00 <5.001.01NR <1.00 <1.00 NR <1.00 NR NR <5.0027.1NR <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <21/16/2019<0.31 <0.048 <0.076 <0.088 <0.22 <0.076 0.71 67<27 <0.061 <0.16 <0.065 <0.054 <0.089 <0.083 <0.078 10<0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.126/20/2019<10 <0.048 <0.076 <0.088 <0.22 <0.076 <0.50 <27 <0.061 <0.16 29<0.054 <0.089 <0.065 <0.083 4.3<0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 8/29/2019<10 <0.048 <0.076 <0.088 <0.22 <0.076 0.77<27 <0.061 <0.16 110<0.054 <0.089 <0.065 <0.083 19<0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 2/14/2020<0.31 <0.048 <0.076 <0.088 <0.22 <0.076 0.75<27 <0.061 <0.16 140<0.054 <0.089 <0.065 <0.083 26<0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 9/29/2015NR <0.50 <0.50 <0.50 <1.0 <0.501.8NR <0.50 <2.0173<0.50 NR NR <2.028.2NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/6/2016NR <0.50 <0.50 <0.50 <1.0 <0.500.54NR <0.50 <2.023.7<0.50 NR NR <2.03.4NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/2/2017NR <0.50 <0.50 <0.50 <1.0 <0.500.53NR <0.50 <2.037.8<0.50 NR NR <2.05.5NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/25/2018NR <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 NR <1.00 <1.00 NR <1.00 NR NR <5.0010.9NR <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <21/16/2019<0.31 <0.048 <0.076 <0.088 <0.22 <0.50 <0.534<27 <0.061 <0.16 <0.065 <0.054 <0.089 <0.083 <0.078 5.5<0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.126/20/2019<0.31 <0.048 <0.076 <0.088 <0.22 <0.076 <0.066 <27 <0.061 <0.16 11<0.054 <0.089 <0.065 <0.083 1.8<0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 8/29/2019 46<0.048 <0.076 <0.088 <0.22 <0.076 0.62<27 <0.061 <0.16 97<0.054 <0.089 <0.065 <0.083 21<0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 2/14/2020<10 <0.048 <0.076 <0.088 <0.22 <0.076 <0.5 <27 <0.061 <0.16 82<0.054 <0.089 <0.065 <0.083 17<0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 6000 1 70 70 3000 70 0.4 NL 600 0.4 70 70 NL NL 5 20 NL 6 70 70 600 400 400 500NL 5 NL NL NL NL 5 NL 700 NL NL NL NL NL NL NL NL NL NL 100 1,000 NL NL 10,0006000000 5,000 8,500 15,000 NL 70,000 400 NL 84,500 400 70,000 25,000 117 NL 5,000 20,000 100000 6,000 3,000 70,000 260,000 28,500 25,000 85,500Notes:1)2)3)4)5)6)7)NL= Compound Not ListedResultResultResult= Result Exceeds Laboratory Detection Limits= Result Exceeds 2L Standard= Result Exceeds GCLNC 2L Standard ‐ North Carolina Groundwater Quality Standard as per NC Administrative Code 15A NCAC 02LGCLs for Groundwater = NCDENR UST Section Gross Contamination Levels for GroundwaterUS EPA MCL = Maximum Contaminant Level ‐ The highest level of a contaminant that is allowed in drinking water per the National Primary Drinking Water Regulations. For the purposes of this table the MCL applies to supply well samples only.Chemical Abstract (CAS) Number provided beneath compound names. WR personnel mistakenly identified a spigot located at the Bullock Baptist Church as being associated with supply well WSW‐37, which has been abandoned. WR personnel sampled this spigot without knowledge that the sample was actually originating from WSW‐14. NC 2L Standard US EPA MCLGCLs for GroundwaterAll results provided in ug/L (micrograms per liter) or parts per billionCompounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of constituents. MW‐27DMW‐27MW‐25MW‐26DMW‐26Page 3 of 4
CalculatedAcetone Benzene sec‐Butylbenzene tert‐Butylbenzene Chloroethane Chloroform 1,2‐DichloroethaneEthanol Ethylbenzene Hexachloro‐1,3‐butadiene Diisopropyl ether Isopropylbenzene (Cumene)Isopropyltoluene, 4‐ MBK, Methyl Butyl Ketone (2‐Hexanone) Methylene Chloride Methyl‐tert‐butyl etherMIBK (4‐Methyl‐2‐pentanone) Naphthalene n‐Propylbenzene Styrene Toluene 1,2,4‐Trimethylbenzene 1,3,5‐TrimethylbenzeneTotal Xylene67‐64‐171‐43‐2135‐98‐898‐06‐675‐00‐367‐66‐3 107‐06‐264‐17‐5100‐41‐487‐68‐3108‐20‐398‐82‐899‐87‐6591‐78‐675‐09‐21634‐04‐4108‐10‐191‐20‐3 103‐65‐1100‐42‐5108‐88‐395‐63‐6108‐67‐81330‐20‐7SampleIDDateCollectedAnalytical MethodSM6200BTABLE B‐4SUMMARY OF GROUNDWATER ANALYTICAL RESULTSSHOTWELL'S GROCERYIncident Number: 116808681 US Highway 15 NBullock, Granville County, North Carolina7/2/2014NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/30/2015NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.06<0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/6/2016NR <0.50 <0.50 <0.50 <1.0 <0.500.77NR <0.50 <2.030.8<0.50 NR NR <2.03.6NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/1/2017NR <0.50 <0.50 <0.501.1<0.50 <0.50 NR <0.50 <2.04.6<0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/28/2018NR <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 NR <1.00 <1.00 NR <1.00 NR NR <5.00 <1.00 NR <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <22/14/2020<10 <0.048 <0.076 <0.088 <0.22 <0.076 <0.5 <27 <0.061 <0.16 11<0.054 <0.089 <0.065 <0.083 1.2<0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 WSW‐9 9/30/2015NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/30/2015NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.01.5<0.50 NR NR <2.00.57NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/5/2016NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.04<0.50 NR NR <2.01.5NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/2/2017NR <0.50 <0.50 <0.50 <1.01.9<0.50 NR <0.50 <2.02.6<0.50 NR NR <2.00.96NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/28/2018NR <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 NR <1.00 <1.00 NR <1.00 NR NR <5.001.08NR <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <22/14/2020<0.31 <0.048 <0.076 <0.088 <0.22 <0.076 <0.066 <27 <0.061 <0.16 2.4<0.054 <0.089 <0.065 <0.083 <1 <0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 9/30/2015NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.01.1<0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/5/2016NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.04.7<0.50 NR NR <2.01.5NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0WSW‐11 7/2/2014NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.07/2/2014NR <0.50 <0.50 <0.50 <1.0 <0.501.9NR <0.50 <2.094.9<0.50 NR NR <2.013.8NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/30/2015NR <0.50 <0.50 <0.50 <1.0 <0.502.3NR <0.50 <2.0140<0.50 NR NR <2.018.9NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/5/2016NR <0.50 <0.50 <0.50 <1.0 <0.500.74NR <0.50 <2.019.6<0.50 NR NR <2.02NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/1/2017NR <0.50 <0.50 <0.50 <1.0 <0.501.2NR <0.50 <2.046.9<0.50 NR NR <2.09NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/28/2018NR <1.00 <1.00 <1.00 <5.00 <5.001.7NR <1.00 <1.00 NR <1.00 NR NR <5.0015.2NR <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <22/13/2020<10 <0.048 <0.076 <0.088 <0.22 <0.076 1.6<27 <0.061 <0.16 80<0.054 <0.089 <0.065 <0.083 18<0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 7/2/2014NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/30/2015NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/5/2016NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/1/2017NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/28/2018NR <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 NR <1.00 <1.00 NR <1.00 NR NR <5.00 <1.00 NR <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <22/14/2020<10 <0.048 <0.076 <0.088 <0.22 <0.076 <0.066 <27 <0.061 <0.16 <0.050 <0.054 <0.089 <0.065 <0.083 <0.042 <0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 7/2/2014NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.04/5/2016NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.08/1/2017NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.02/14/2020<10 <0.048 <0.076 <0.088 <0.22 <0.076 <0.066 <27 <0.061 <0.16 <0.050 <0.054 <0.089 <0.065 <0.083 <0.042 <0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 8/1/2017NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.09/28/2018NR <1.00 <1.00 <1.00 <5.00 <5.00 <1.00 NR <1.00 <1.00 NR <1.00 NR NR <5.00 <1.00 NR <5.00 <1.00 <1.00 <1.00 <1.00 <1.00 <22/14/2020<10 <0.048 <0.076 <0.088 <0.22 <0.076 <0.066 <27 <0.061 <0.16 <0.050 <0.054 <0.089 <0.065 <0.083 <0.042 <0.078 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 WSW‐37 4/6/2016NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.0WSW‐40 8/1/2017NR <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 NR <0.50 <2.0 <0.50 <0.50 NR NR <2.0 <0.50 NR <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.06000 1 70 70 3000 70 0.4 NL 600 0.4 70 70 NL NL 5 20 NL 6 70 70 600 400 400 500NL 5 NL NL NL NL 5 NL 700 NL NL NL NL NL NL NL NL NL NL 100 1,000 NL NL 10,0006000000 5,000 8,500 15,000 NL 70,000 400 NL 84,500 400 70,000 25,000 117 NL 5,000 20,000 100000 6,000 3,000 70,000 260,000 28,500 25,000 85,500Notes:1)2)3)4)5)6)7)NL= Compound Not ListedResultResultResultChemical Abstract (CAS) Number provided beneath compound names. WR personnel mistakenly identified a spigot located at the Bullock Baptist Church as being associated with supply well WSW‐37, which has been abandoned. WR personnel sampled this spigot without knowledge that the sample was actually originating from WSW‐14. = Result Exceeds Laboratory Detection Limits= Result Exceeds GCLGCLs for GroundwaterAll results provided in ug/L (micrograms per liter) or parts per billionCompounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included in the Appendix for a full list of constituents. NC 2L Standard ‐ North Carolina Groundwater Quality Standard as per NC Administrative Code 15A NCAC 02LGCLs for Groundwater = NCDENR UST Section Gross Contamination Levels for GroundwaterUS EPA MCL = Maximum Contaminant Level ‐ The highest level of a contaminant that is allowed in drinking water per the National Primary Drinking Water Regulations. For the purposes of this table the MCL applies to supply well samples only.= Result Exceeds 2L StandardUS EPA MCLWSW‐10 PRENC 2L Standard WSW‐8WSW‐10 POSTWSW‐12WSW‐14WSW‐15WSW‐17Page 4 of 4
Easting Northing
WSW-7 193901483904 8700 US Hwy 15 N
Donald B. & Constance M.
Hanson
8700 US Hwy 15 N
Bullock, NC 27507 Unknown Unknown Unknown 976 Cross-gradient 2134253.55 998948.86
WSW-8 193901388405 8687 US Hwy 15 N
Harold W. & Betty Jean
Duncan
2624 Vaughan Rd
Bullock, NC 27507
Potable/POE
removed by
STF under
18199
Unknown Unknown 331 Cross-gradient 2133863.25 998426.04
WSW-9 193901481443 8688 US Hwy 15 N
Dwight A. & Jackie
Bullock
8688 US Hwy 15 N
Bullock, NC 27507
Potable/POE
System Unknown Unknown 592 Down-gradient 2134240.74 998435.55
WSW-10 193901387387 8685 US Hwy 15 N
Brian M. & Heather W.
Hayes
8685 US Hwy 15 N
Bullock, NC 27507
Potable/POE
System
instaled by
Oxford Oil
Unknown Unknown 274 Cross-gradient 2133828.72 998377.81
WSW-11 193901387245 8683 US Hwy 15 N
Richard A. & Julie A.
Carter
PO Box 297
Bullock, NC 27507
Potable/POE
removed by
STF 5/31/2016
Unknown Unknown 111 Cross-gradient 2133765.59 998225.88
WSW-12 193901389295 8682 US Hwy 15 N
Martin B. & Nancy S. Lee
(Post Office Building)
PO Box 266
Bullock, NC 27507
Toilets &
Cleaning Only Unknown Unknown 190 Down-gradient 2133922.14 998178.32
WSW-13 193901485476 4089 Buckhorn Rd Carolin & F. W. Stovall
4089 Buckhorn Rd
Bullock, NC 27507 Inactive Unknown Unknown 610 Down-gradient 2134351.58 998139.92
WSW-14 193901379990 4078 Buckhorn Rd Bullock Baptist Chruch, Inc.
PO Box 86
Bullock, NC 27507 Potable Unknown Unknown 417 Cross-gradient 2134029.76 997816.23
WSW-15 193901376962 8675 US Hwy 15 N
Bullock Volunteer Fire
Department
PO Box 386
Bullock, NC 27507
Toilets &
Cleaning Only Unknown Unknown 304 Cross-gradient 2133640.17 997831.62
WSW-16 193901387114 8681 US Hwy 15 N
Shotwells Grocery
(Subject Site)
PO Box 38
Bullock, NC 27507 Inactive Unknown Unknown 57 Cross-gradient 2133685.86 998107.01
WSW-17 193901374941 4064 Herbert Faucette Rd Steven A. Keeton
4064 Herbert Faucette Rd
Bullock, NC 27507 Potable Unknown Unknown 283 Up-gradient 2133495.03 997978.87
WSW-18 193901393358 4061 Herbert Faucette Rd W. E. & Ora K. Capps
PO Box 157
Bullock, NC 27507 Unknown Unknown Unknown 871 Up-gradient 2133098.90 998705.33
WSW-19 193901380339 4057 Herbert Faucette Rd Irvin S. & Linda J. Gooch PO Box 212
Bullock, NC 27507 Unknown Unknown Unknown 865 Up-gradient 2132973.03 998513.84
WSW-20 193901388535 8689 US Hwy 15 N Horace Capps
PO Box 92
Bullock, NC 27507 Unknown Unknown Unknown 608 Cross-gradient 2133709.07 998725.22
WSW-21 193900388864 8695 US Hwy 15 N
Michael W. & Elisabeth
Matthews
9083 McDuffey Rd
Oxford, NC 27507 Unknown Unknown Unknown 775 Cross-gradient 2133752.43 998892.95
WSW-22 193901399070 8699 US Hwy 15 N
Francisco & P. Duran
Bautista
8699 US Hwy 15 N
Bullock, NC 27507 Active Potable Unknown Unknown 952 Cross-gradient 2133942.72 999048.33
WSW-23 193901482607 8694B US Hwy 15 N
Dovey B. Cooper
(DBA Dovey's Hair Styling)
PO Box 36
Bullock, NC 27507 Unknown Unknown Unknown 852 Down-gradient 2134342.99 998720.86
WSW-24 193901485476 4089 Buckhorn Rd Carolin & F. W. Stovall
4089 Buckhorn Rd
Bullock, NC 27507 Unknown Unknown Unknown 699 Down-gradient 2134405.82 998336.02
WSW-25 193901383305 4047 Herbert Faucette Rd
William D. & Wanda M.
Capps
PO Box 3
Bullock, NC 27507 Potable Unknown Unknown 654 Up-gradient 2133220.58 998513.84
WSW-26 193901474869 4088 Buckhorn Rd
Linda S. & Kevin W.
Nicholson
PO Box 156
Bullock, NC 27507 Potable Unknown Unknown 748 Down-gradient 2134445.45 997866.02
WSW-27 193901476806 4090 Buckhorn Rd
Daniel M. Faucette Jr. &
Betsy Faucette
4090 Buckhorn Rd
Bullock, NC 27507
Potable/Hand
Dug Unknown Unknown 926 Down-gradient 2134621.68 997829.68
WSW-28 193901476806 4090 Buckhorn Rd
Daniel M. Faucette Jr. &
Betsy Faucette
4090 Buckhorn Rd
Bullock, NC 27507 Potable Unknown Unknown 891 Down-gradient 2134554.54 997752.80
WSW-29 193901476806 4090 Buckhorn Rd
Daniel M. Faucette Jr. &
Betsy Faucette
4090 Buckhorn Rd
Bullock, NC 27507
Toilets &
Bathing (Drink
Distilled)
Unknown Unknown 849 Down-gradient 2134574.13 997949.88
WSW-30 193901477973 4094 Buckhorn Rd Russell E. Jones Jr.
4094 Buckhorn Rd
Bullock, NC 27507 Potable Unknown Unknown 1025 Down-gradient 2134755.95 997969.45
WSW-31 193901488433 4095 Buckhorn Rd Carolyn C. Stovall
4030 Stovall Rd
Oxford, NC 27507 Potable Unknown Unknown 1070 Down-gradient 2134811.93 998134.54
WSW-32 193901375770 8671 US Hwy 15 N
Bullock Bolunteer Fire
Department
PO Box 366
Bullock, NC 27507 Potable Unknown Unknown 393 Cross-gradient 2133626.44 997741.96
WSW-33 193901375516 8667 US Hwy 15 N
William R. & Nancy R.
Frazier
7681 Harts Cross Rd
Oxford, NC 27565 Potable Unknown Unknown 594 Cross-gradient 2133562.20 997551.97
WSW-34 193901374452 8663 US Hwy 15 N
William F. Ott Jr. &
Jean M. Ott
PO Box 246
Bullock, NC 27507 Potable Unknown Unknown 694 Cross-gradient 2133489.50 997471.72
WSW-34A 193901374452 8663 US Hwy 15 N
William F. Ott Jr. &
Jean M. Ott
PO Box 246
Bullock, NC 27507 Unknown Unknown Unknown 796 Cross-gradient 2133443.70 997380.19
WSW-35 193901373247 8661 US Hwy 15 N
Judy H. Williams &
Nancy Hoyle
PO Box 269
Bullock, NC 27507 Potable Unknown Unknown 929 Cross-gradient 2133424.20 997244.61
WSW-35A 193901373247 8661 US Hwy 15 N
Judy H. Williams &
Nancy Hoyle
PO Box 269
Bullock, NC 27507 Unknown Unknown Unknown 971 Cross-gradient 2133267.46 997270.63
WSW-37 193901379990 4078 Buckhorn Rd Bullock Baptist Chruch, Inc.
PO Box 86
Bullock, NC 27507 Abandoned Unknown Unknown 318 Cross-gradient 2134023.65 997971.94
WSW-38 193901378531 8668 US Hwy 15 N
George & Peggy H.
Whitfield
PO Box 278
Bullock, NC 27507 Potable Unknown Unknown 527 Cross-gradient 2133733.21 997591.01
WSW-40 193901376962 8675 US Hwy 15 N
Bullock Volunteer Fire
Department
PO Box 386
Bullock, NC 27507
Reportedly
Non-Existent Unknown Unknown 132 Cross-gradient 2133709.08 997990.06
WSW-41 193901373347 US Hwy 15 N
Judy H. Williams &
Nancy Hoyle
PO Box 269
Bullock, NC 27507 Unknown Unknown Unknown 844 Cross-gradient 2133331.30 997380.19
2.) Information regarding the water supply well's use and location were obtained from the Groundwater Monitoring Report dated April 18, 2013 and produced by Crawford Environmental Services.
3.) WR has not performed a receptor survey in association with the subject property and thus the information provided above has not been verified.
Well
Screen
Interval
(feet)
TABLE B-5A
PUBLIC & PRIVATE WATER SUPPLY WELL INFORMATION
SHOTWELL'S GROCERY
8681 US Highway 15 N
Bullock, Granville County, North Carolina
Well Distance
from Source Area
(feet)
Location
Relative to
Groundwater
Flow
Notes:
1.) Well location addresses and property owner address were obtained from the Granville County GIS Department.
Well Coordinates
(NC State Plane NAD 83 Feet)Property Owner AddressProperty AddressWell ID Property Owner
Parcel
Number Well Use Well Depth
(feet)
Incident Number: 11680
Page 1 of 1
Easting NorthingPondSmall Pond(~1 Acre)West of Subject SiteN/A N/A 160 Up-gradient 2133595.63 998188.20TABLE B-5BADDITIONAL RECEPTOR INFORMATIONSHOTWELL'S GROCERY8681 US Highway 15 NBullock, Granville County, North CarolinaIncident Number: 11680Notes: 1.) WR has not performed a receptor survey in association with the subject property and thus the information provided above has not been verified. Distance from Source Area(feet)Location Relative to Groundwater FlowLocation of Significant Points(NC State Plane NAD 83 Feet)Receptor IDDescription LocationContactInformationUsagePage 1 of 1
Easting NorthingDW-1 2/20/1998 2 100.0 90.0 90 - 100 100.99 2/13/2020 5.75 --- 95.24 2133783.37 998157.85M-4 3/28/1995 2 23.7 17.6 17.6 - 23.7 96.16 2/14/2020 0.00 --- 96.16 2133960.89 998336.82M-6 3/29/1995 2 32.1 26.0 26 - 32.1 99.74 2/14/2020 3.00 --- 96.74 2133909.53 998169.83M-13 4/25/1995 2 14.5 9.5 9.5 - 14.5 104.90 2/13/2020 8.13 --- 96.77 2133968.66 997784.05M-14 4/26/1995 2 25.4 19.5 19.5 - 25.4 98.69 2/14/2020 4.00 --- 94.69 2133860.14 998420.42MW-17 2/18/1998 2 14.0 5.0 5 - 14 100.86 2/13/2020 4.02 --- 96.84 2133728.40 998107.34MW-18 2/18/1998 2 14.2 5.0 5 - 14.2 100.83 2/13/2020 4.06 --- 96.77 2133790.23 998106.56MW-20 2/18/1998 2 15.3 2.5 2.5 - 15.3 98.51 2/14/2020 1.20 --- 97.31 2133807.24 998205.93MW-21 2/19/1998 2 17.4 2.5 2.5 - 17.4 99.55 2/14/2020 2.77 --- 96.78 2133916.80 998182.40MW-22 2/19/1998 2 17.7 2.5 2.5 - 17.7 97.40 2/14/2020 1.98 --- 95.42 2133856.18 998404.96MW-23 2/19/1998 2 17.5 2.5 2.5 - 17.5 95.71 2/14/2020 0.00 --- 95.71 2133952.08 998369.89MW-24 9/23/2015 2 18.0 3.0 3 - 18 101.10 2/14/2020 4.10 --- 97.00 2133779.54 998143.24MW-25 9/22/2015 2 14.0 3.0 3 - 14 101.71 2/13/2020 5.05 --- 96.66 2133856.00 998010.98MW-26 9/22/2015 2 18.0 3.0 3 - 18 99.89 2/13/2020 4.70 --- 95.19 2133886.06 998107.61MW-26D 9/24/2015 2 37.0 32.0 32 - 37 100.02 2/13/2020 3.45 --- 96.57 2133884.26 998100.57MW-27 9/23/2015 2 14.0 4.0 4 - 14 98.29 2/14/2020 1.58 --- 96.71 2134045.86 998315.38MW-27D 9/23/2015 2 34.0 29.0 29 - 34 98.03 2/14/2020 1.47 --- 96.56 2134053.27 998321.321)2)3)4)5)TABLE B-78681 US Highway 15 NMONITORING & REMEDIATION WELL CONSTRUCTION INFORMATIONWell Casing Diameter(in)Free Product Thickness(ft)Total Depth (ft)Date Water Level MeasuredScreened Interval (ft)Well Casing Depth (ft)Incident Number: 11680SHOTWELL'S GROCERYWell Coordinates(NC State Plane NAD 83 Feet)Bullock, Granville County, North CarolinaWell IDGroundwaterElevation (ft)Depth-to-Water from Top-of-Casing(ft)Top-of-Casing Elevation (ft)Date InstalledElevations for monitoring wells M-1, M-2, M-3, M-7, M-9, M-10, M-11, M-12, M-15 and M-19 from survey performed by CES, July 2012.Elevations for monitoring wells M-14, MW-17, MW-18, MW-20, MW-22 and MW-23 from survey performed by WR, July 2014.Elevations for monitoring wells M-4, M-6, M-13, MW-21, MW-24, MW-25, MW-26, MW-26D, MW-27 and MW-27D from survey performed by WR, September 2015.Well coordinates obtained using a Trimble 2005 Series GeoXH GPS Unit.Top of casing (TOC) elevations relative to arbitrary 100.00 ft benchmark established at TOC of monitoring well M-1 by Crawford Environmental Services, Inc. (CES), July 2014.Notes: Page 1 of 1
Well ID
Screened
Interval
(ft)
Top-of-Casing
Elevation
(ft)
Date Water Level
Measured
Depth-to-Product
(ft)
Depth-to-Water
Uncorrected
(ft)
Free Product
Thickness
(ft)
Depth-to-Water
Corrected
(ft)
Groundwater
Surface
Elevation
(ft)
2/24/1998 --- 35.82 --- 35.82 64.95
7/3/2014 --- 6.99 --- 6.99 93.78
9/29/2015 --- 7.30 --- 7.30 93.47
4/5/2016 --- 3.35 --- 3.35 97.42
2/13/2020 --- 5.75 --- 5.75 95.02
10/30/1997 --- 7.46 --- 7.46 92.54
12/18/1997 --- 6.20 --- 6.20 93.80
2/24/1998
10/25/2007 --- 11.08 --- 11.08 88.92
7/24/2012 --- 9.31 --- 9.31 90.69
7/3/2014 --- 4.27 --- 4.27 95.73
9/29/2015 --- 4.38 --- 4.38 95.62
4/6/2016 --- 2.90 --- 2.90 97.10
12/13/2017
10/30/1997 --- 8.60 --- 8.60 91.74
12/18/1997 --- 6.84 --- 6.84 93.50
2/24/1998
10/30/1997 --- 7.51 --- 7.51 92.87
12/18/1997 --- 6.27 --- 6.27 94.11
2/24/1998
10/25/2007 --- 10.52 --- 10.52 89.86
7/24/2012
10/30/1997 --- 6.90 --- 6.90 93.33
12/18/1997 --- 5.38 --- 5.38 94.85
2/24/1998
10/25/2007 --- 11.12 --- 11.12 89.11
7/24/2012 --- 8.88 --- 8.88 91.35
7/3/2014 --- 4.15 --- 4.15 96.08
9/29/2015 --- 2.71 --- 2.71 97.52
4/6/2016 --- 0.65 --- 0.65 99.58
2/14/2020 --- 0.00 --- 0.00 100.23
10/30/1997 --- 5.74 --- 5.74 97.65
12/18/1997 --- 4.97 --- 4.97 98.42
2/24/1998
10/30/1997 --- 10.45 --- 10.45 91.16
12/18/1997 --- 8.63 --- 8.63 92.98
2/24/1998
10/25/2007 --- 14.98 --- 14.98 86.63
7/24/2012 --- 12.27 --- 12.27 89.34
7/3/2014 --- 7.21 --- 7.21 94.40
9/29/2015 --- 6.68 --- 6.68 94.93
4/5/2016 --- 2.74 --- 2.74 98.87
2/14/2020 --- 3.00 --- 3.00 98.61
M-7 12 - 17 100.36 10/30/1997 --- 9.68 --- 9.68 90.68
M-9 24 - 29 111.70 10/30/1997 --- 15.76 --- 15.76 95.94
M-10 14.5 - 19.5 102.48 10/30/1997 --- 14.00 --- 14.00 88.48
M-11 15 - 20 99.16 10/30/1997 --- 8.43 --- 8.43 90.73
10/30/1997 --- 7.25 --- 7.25 91.14
12/18/1997 --- 5.90 --- 5.90 92.49
10/25/2007 --- 11.41 --- 11.41 86.98
M-6
M-4 17.6 - 22.6 100.23
101.6126 - 31
DW-1 90 -100 100.77
M-1 15 - 19 100.00
Abandoned 12/13/2017
M-2
M-3
M-5
12.5 - 17.5 100.34
15.5 - 20.5 100.38
12 - 17 103.39
TABLE B-9
CURRENT & HISTORICAL GROUNDWATER ELEVATIONS & FREE PRODUCT THICKNESS
SHOTWELL'S GROCERY
8681 US Highway 15 N
Bullock, Granville County, North Carolina
Incident Number: 11680
Well Destroyed
Well Destroyed
Well Destroyed
Well Not Located
Well Not Located
Well Not Located
Well Not Located
M-12 12.5 - 19.5 98.39
Page 1 of 3
Well ID
Screened
Interval
(ft)
Top-of-Casing
Elevation
(ft)
Date Water Level
Measured
Depth-to-Product
(ft)
Depth-to-Water
Uncorrected
(ft)
Free Product
Thickness
(ft)
Depth-to-Water
Corrected
(ft)
Groundwater
Surface
Elevation
(ft)
TABLE B-9
CURRENT & HISTORICAL GROUNDWATER ELEVATIONS & FREE PRODUCT THICKNESS
SHOTWELL'S GROCERY
8681 US Highway 15 N
Bullock, Granville County, North Carolina
Incident Number: 11680
10/30/1997 --- 12.23 --- 12.23 94.29
9/29/2015 --- 10.09 --- 10.09 96.43
4/5/2016 --- 5.47 --- 5.47 101.05
2/13/2020 --- 8.13 --- 8.13 98.39
10/30/1997 --- 7.79 --- 7.79 91.42
12/18/1997 --- 6.52 --- 6.52 92.69
10/25/2007 --- 12.61 --- 12.61 86.60
7/24/2012 --- 8.52 --- 8.52 90.69
7/3/2014 --- 5.19 --- 5.19 94.02
9/29/2015 --- 5.57 --- 5.57 93.64
4/6/2016 --- 4.87 --- 4.87 94.34
2/14/2020 --- 4.00 --- 4.00 95.21
10/30/1997 --- 8.16 --- 8.16 92.64
12/18/1997 --- 7.05 --- 7.05 93.75
10/25/2007
M16 2/24/1998
2/20/1998 --- 3.21 --- 3.21 97.44
10/25/2007 --- 10.43 --- 10.43 90.22
7/24/2012 --- 9.55 --- 9.55 91.10
7/3/2014 --- 4.37 --- 4.37 96.28
9/29/2015 5.00 --- 5.00 95.65
4/5/2016 --- 2.33 --- 2.33 98.32
2/13/2020 --- 4.02 --- 4.02 96.63
2/20/1998 --- 5.10 --- 5.10 95.64
10/25/2007 --- 10.22 --- 10.22 90.52
7/24/2012 --- 9.27 --- 9.27 91.47
7/3/2014 --- 4.21 --- 4.21 96.53
9/29/2015 5.20 --- 5.20 95.54
4/5/2016 --- 2.44 --- 2.44 98.30
2/13/2020 --- 4.06 --- 4.06 96.68
MW-19 2.5 - 17.5 98.61 2/20/1998 --- 1.68 --- 1.68 96.93
2/20/1998 --- 1.77 --- 1.77 96.59
10/25/2007 --- 9.15 --- 9.15 89.21
7/24/2012 --- 8.02 --- 8.02 90.34
7/3/2014 --- 3.24 --- 3.24 95.12
9/29/2015 --- 1.99 --- 1.99 96.37
4/6/2016 --- 1.89 --- 1.89 96.47
2/14/2020 --- 1.20 --- 1.20 97.16
2/20/1998 --- 2.08 --- 2.08 97.49
10/25/2007 --- 12.71 --- 12.71 86.86
7/24/2012 --- 10.51 --- 10.51 89.06
7/3/2014 --- 5.61 --- 5.61 93.96
9/29/2015 --- 6.50 --- 6.50 93.07
4/5/2016 --- 3.09 --- 3.09 96.48
2/14/2020 --- 2.77 --- 2.77 96.80
2/20/1998 --- 1.59 --- 1.59 95.61
10/25/2007 --- 10.09 --- 10.09 87.11
7/24/2012 --- 8.21 --- 8.21 88.99
7/3/2014 --- 4.20 --- 4.20 93.00
9/29/2015 --- 3.94 --- 3.94 93.26
4/6/2016 --- 2.70 --- 2.70 94.50
2/14/2020 --- 1.98 --- 1.98 95.22
5 - 15 100.74
2.5 - 17.5 98.36
99.572.5 - 17.5
M-13 9.5 - 14.5 106.52
MW-22
MW-21
MW-20
MW-18
2.5 - 17.5 97.20
10 - 15 100.80
MW-17
M-14 19.5 - 24.5 99.21
5 - 15 100.65
M-15
Well Destroyed
Well Destroyed
Page 2 of 3
Well ID
Screened
Interval
(ft)
Top-of-Casing
Elevation
(ft)
Date Water Level
Measured
Depth-to-Product
(ft)
Depth-to-Water
Uncorrected
(ft)
Free Product
Thickness
(ft)
Depth-to-Water
Corrected
(ft)
Groundwater
Surface
Elevation
(ft)
TABLE B-9
CURRENT & HISTORICAL GROUNDWATER ELEVATIONS & FREE PRODUCT THICKNESS
SHOTWELL'S GROCERY
8681 US Highway 15 N
Bullock, Granville County, North Carolina
Incident Number: 11680
2/20/1998 --- 0.00 --- 0.00 95.71
7/24/2012 --- 6.84 --- 6.84 88.87
7/3/2014 --- 2.65 --- 2.65 93.06
9/29/2015 --- 2.17 --- 2.17 93.54
4/6/2016 --- 0.50 --- 0.50 95.21
2/14/2020 --- 0.00 --- 0.00 95.71
9/29/2015 --- 5.78 --- 5.78 95.32
4/5/2016 --- 3.59 --- 3.59 97.51
2/14/2020 --- 4.10 --- 4.10 97.00
9/29/2015 --- 3.96 --- 3.96 97.75
4/5/2016 --- 1.39 --- 1.39 100.32
2/23/2020 5.05 5.05 96.66
9/29/2015 --- 5.93 --- 5.93 93.96
4/5/2016 --- 1.98 --- 1.98 97.91
2/13/2020 --- 4.70 --- 4.70 95.19
9/29/2015 --- 6.03 --- 6.03 93.99
4/5/2016 --- 1.80 --- 1.80 98.22
2/13/2020 --- 3.45 --- 3.45 96.57
9/29/2015 --- 6.22 --- 6.22 92.07
4/6/2016 --- 2.22 --- 2.22 96.07
2/14/2020 --- 1.58 --- 1.58 96.71
9/29/2015 --- 5.90 --- 5.90 92.13
4/6/2016 --- 2.09 --- 2.09 95.94
2/14/2020 --- 1.47 --- 1.47 96.56
1)
2)
3)
4)
5)
MW-27D 29 - 34 98.03
MW-27
MW-26D
MW-26
MW-25
MW-24
MW-23
Well coordinates obtained using a Trimble 2005 Series GeoXH GPS Unit.
Top of casing (TOC) elevations relative to arbitrary 100.00 ft benchmark established at TOC of monitoring well M-1 by Crawford Environmental
Services, Inc. (CES), July 2014.
Elevations for monitoring wells M-1, M-2, M-3, M-7, M-9, M-10, M-11, M-12, M-15 and M-19 from survey performed by CES, July 2012.
Elevations for monitoring wells M-14, MW-17, MW-18, MW-20, MW-22 and MW-23 from survey performed by WR, July 2014.
Elevations for monitoring wells M-4, M-6, M-13, MW-21, MW-24, MW-25, MW-26, MW-26D, MW-27 and MW-27D from survey performed by
WR, September 2015.
4 - 14 98.29
3 - 18 99.89
100.0232 - 37
3 - 18 101.1
101.713 - 14
95.712.5 - 17.5
Notes:
Page 3 of 3
APPENDIX A
LABORATORY ANALYTICAL REPORT
AND
CHAIN‐OF‐CUSTODY
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
3/2/20 12:07
Withers & Ravenel
Kevin Buchanan
115 Mackenan Dr. BUILDING 117
Cary, NC 27511
Project: Shotwell Grocery
Project No.: 02170214.17
Lab Submittal Date: 02/18/2020
Work Order: 0020258
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOINT ANALYTICAL
Senior Project Manager
Reviewed ByAngela D. Overcash Angela D. Overcash
Senior Project Manager
Data Qualifiers Key Reference:
D RPD value outside of the control limits.
M Matrix spike outside of the control limits.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Sample Receipt Summary
03/02/2020
Work Order: 0020258
Client Sample ID MatrixLab Sample ID Date/Time Sampled Date/Time Received
0020258-01 02/13/20 14:30DW-1 02/18/20 16:05Water
0020258-02 02/14/20 11:25M-4 02/18/20 16:05Water
0020258-03 02/14/20 9:55M-6 02/18/20 16:05Water
0020258-04 02/13/20 15:15M-13 02/18/20 16:05Water
0020258-05 02/14/20 13:00M-14 02/18/20 16:05Water
0020258-06 02/13/20 13:20MW-17 02/18/20 16:05Water
0020258-07 02/13/20 13:40MW-18 02/18/20 16:05Water
0020258-08 02/14/20 10:35MW-20 02/18/20 16:05Water
0020258-09 02/14/20 10:15MW-21 02/18/20 16:05Water
0020258-10 02/14/20 13:25MW-22 02/18/20 16:05Water
0020258-11 02/14/20 11:00MW-23 02/18/20 16:05Water
0020258-12 02/13/20 14:50MW-24 02/18/20 16:05Water
0020258-13 02/13/20 15:50MW-25 02/18/20 16:05Water
0020258-14 02/13/20 16:30MW-26 02/18/20 16:05Water
0020258-15 02/13/20 17:00MW-26D 02/18/20 16:05Water
0020258-16 02/14/20 11:50MW-27 02/18/20 16:05Water
0020258-17 02/14/20 12:30MW-27D 02/18/20 16:05Water
0020258-18 02/14/20 13:40WSW-8 02/18/20 16:05Water
0020258-19 02/14/20 14:40WSW-10 02/18/20 16:05Water
0020258-20 02/13/20 16:10WSW-12 02/18/20 16:05Water
0020258-21 02/14/20 15:20WSW-15 02/18/20 16:05Water
0020258-22 02/14/20 15:03WSW-17 02/18/20 16:05Water
0020258-23 02/14/20 15:03WSW-14 02/18/20 16:05Water
Samples were received in good condition at 3.4 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Client ID ResultParameterMethod UnitsWaypoint ID
Work Order: 0020258
03/02/2020
Summary of Detections
0.51 ug/L0020258-01 DW-1 1,2-Dichloroethane *SM6200 B
82 ug/L0020258-01 DW-1 Isopropyl Ether *SM6200 B
59 ug/L0020258-01 DW-1 Methyl-tert-Butyl Ether *SM6200 B
230 ug/L0020258-02 M-4 Isopropyl Ether *SM6200 B
50 ug/L0020258-02 M-4 Methyl-tert-Butyl Ether *SM6200 B
4.0 ug/L0020258-03 M-6 Isopropyl Ether *SM6200 B
0.90 ug/L0020258-05 M-14 Isopropyl Ether *SM6200 B
5.0 ug/L0020258-07 MW-18 Isopropyl Ether *SM6200 B
1.8 ug/L0020258-07 MW-18 Methyl-tert-Butyl Ether *SM6200 B
0.59 ug/L0020258-07 MW-18 sec-Butylbenzene *SM6200 B
0.97 ug/L0020258-07 MW-18 tert-Butylbenzene *SM6200 B
18 ug/L0020258-11 MW-23 Isopropyl Ether *SM6200 B
3.9 ug/L0020258-11 MW-23 Methyl-tert-Butyl Ether *SM6200 B
1200 ug/L0020258-12 MW-24 1,2,4-Trimethylbenzene *SM6200 B
350 ug/L0020258-12 MW-24 1,3,5-Trimethylbenzene *SM6200 B
10 ug/L0020258-12 MW-24 4-Isopropyltoluene *SM6200 B
130 ug/L0020258-12 MW-24 Benzene *SM6200 B
770 ug/L0020258-12 MW-24 Ethylbenzene *SM6200 B
140 ug/L0020258-12 MW-24 Isopropyl Ether *SM6200 B
61 ug/L0020258-12 MW-24 Isopropylbenzene (Cumene)*SM6200 B
2600 ug/L0020258-12 MW-24 m,p-Xylenes *SM6200 B
21 ug/L0020258-12 MW-24 Methyl-tert-Butyl Ether *SM6200 B
110 ug/L0020258-12 MW-24 Naphthalene *SM6200 B
64 ug/L0020258-12 MW-24 n-Butylbenzene *SM6200 B
200 ug/L0020258-12 MW-24 n-Propylbenzene *SM6200 B
1100 ug/L0020258-12 MW-24 o-Xylene *SM6200 B
16 ug/L0020258-12 MW-24 sec-Butylbenzene *SM6200 B
1500 ug/L0020258-12 MW-24 Toluene *SM6200 B
3700 ug/L0020258-12 MW-24 Xylenes, total *SM6200 B
3.5 ug/L0020258-15 MW-26D Isopropyl Ether *SM6200 B
82 ug/L0020258-16 MW-27 Isopropyl Ether *SM6200 B
17 ug/L0020258-16 MW-27 Methyl-tert-Butyl Ether *SM6200 B
0.75 ug/L0020258-17 MW-27D 1,2-Dichloroethane *SM6200 B
140 ug/L0020258-17 MW-27D Isopropyl Ether *SM6200 B
26 ug/L0020258-17 MW-27D Methyl-tert-Butyl Ether *SM6200 B
11 ug/L0020258-18 WSW-8 Isopropyl Ether *SM6200 B
1.2 ug/L0020258-18 WSW-8 Methyl-tert-Butyl Ether *SM6200 B
2.4 ug/L0020258-19 WSW-10 Isopropyl Ether *SM6200 B
1.6 ug/L0020258-20 WSW-12 1,2-Dichloroethane *SM6200 B
80 ug/L0020258-20 WSW-12 Isopropyl Ether *SM6200 B
18 ug/L0020258-20 WSW-12 Methyl-tert-Butyl Ether *SM6200 B
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: DW-1
Sample ID: 0020258-01
Work Order: 0020258
Time Collected: 02/13/20 14:30
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 20:45 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.0761,2-Dichlorobenzene
0.51 *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B039212.0 2/24/20 20:45 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03921102/24/20 20:45 JLBug/L 0.31Acetone
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.048Benzene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B039211.0 2/24/20 20:45 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B039211.0 2/24/20 20:45 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B039212002/24/20 20:45 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: DW-1
Sample ID: 0020258-01
Work Order: 0020258
Time Collected: 02/13/20 14:30
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 20:45 JLBug/L 0.16Hexachlorobutadiene
82 *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B039211.0 2/24/20 20:45 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B039211.0 2/24/20 20:45 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B039215.0 2/24/20 20:45 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B039211.0 2/24/20 20:45 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B039212.0 2/24/20 20:45 JLBug/L 0.083Methylene Chloride
59 *SM6200 B P0B039211.0 2/24/20 20:45 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B039211.0 2/24/20 20:45 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.047Styrene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.044Toluene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B039215.0 2/24/20 20:45 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B039210.50 2/24/20 20:45 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B039211.5 2/24/20 20:45 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-130101 %Dibromofluoromethane
70-13096 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: M-4
Sample ID: 0020258-02
Work Order: 0020258
Time Collected: 02/14/20 11:25
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B038812.0 2/24/20 20:51 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B038812.0 2/24/20 20:51 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03881102/24/20 20:51 JLBug/L 0.31Acetone
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.048Benzene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B038811.0 2/24/20 20:51 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B038811.0 2/24/20 20:51 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B038812002/24/20 20:51 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: M-4
Sample ID: 0020258-02
Work Order: 0020258
Time Collected: 02/14/20 11:25
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B038812.0 2/24/20 20:51 JLBug/L 0.16Hexachlorobutadiene
230 *SM6200 B P0B0388105.0 2/24/20 21:25 JLBug/L 0.50Isopropyl Ether
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B038811.0 2/24/20 20:51 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B038811.0 2/24/20 20:51 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B038815.0 2/24/20 20:51 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B038811.0 2/24/20 20:51 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B038812.0 2/24/20 20:51 JLBug/L 0.083Methylene Chloride
50 *SM6200 B P0B038811.0 2/24/20 20:51 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B038811.0 2/24/20 20:51 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.047Styrene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.044Toluene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B038815.0 2/24/20 20:51 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B038810.50 2/24/20 20:51 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B038811.5 2/24/20 20:51 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-130107 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: M-6
Sample ID: 0020258-03
Work Order: 0020258
Time Collected: 02/14/20 09:55
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 15:50 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B039212.0 2/24/20 15:50 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03921102/24/20 15:50 JLBug/L 0.31Acetone
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.048Benzene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B039211.0 2/24/20 15:50 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B039211.0 2/24/20 15:50 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B039212002/24/20 15:50 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: M-6
Sample ID: 0020258-03
Work Order: 0020258
Time Collected: 02/14/20 09:55
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 15:50 JLBug/L 0.16Hexachlorobutadiene
4.0 *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B039211.0 2/24/20 15:50 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B039211.0 2/24/20 15:50 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B039215.0 2/24/20 15:50 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B039211.0 2/24/20 15:50 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B039212.0 2/24/20 15:50 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0B039211.0 2/24/20 15:50 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B039211.0 2/24/20 15:50 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.047Styrene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.044Toluene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B039215.0 2/24/20 15:50 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B039210.50 2/24/20 15:50 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B039211.5 2/24/20 15:50 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: M-13
Sample ID: 0020258-04
Work Order: 0020258
Time Collected: 02/13/20 15:15
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 17:04 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B039212.0 2/24/20 17:04 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03921102/24/20 17:04 JLBug/L 0.31Acetone
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.048Benzene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B039211.0 2/24/20 17:04 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B039211.0 2/24/20 17:04 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B039212002/24/20 17:04 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: M-13
Sample ID: 0020258-04
Work Order: 0020258
Time Collected: 02/13/20 15:15
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 17:04 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B039211.0 2/24/20 17:04 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B039211.0 2/24/20 17:04 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B039215.0 2/24/20 17:04 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B039211.0 2/24/20 17:04 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B039212.0 2/24/20 17:04 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0B039211.0 2/24/20 17:04 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B039211.0 2/24/20 17:04 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.047Styrene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.044Toluene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B039215.0 2/24/20 17:04 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B039210.50 2/24/20 17:04 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B039211.5 2/24/20 17:04 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-13096 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: M-14
Sample ID: 0020258-05
Work Order: 0020258
Time Collected: 02/14/20 13:00
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 17:28 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B039212.0 2/24/20 17:28 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03921102/24/20 17:28 JLBug/L 0.31Acetone
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.048Benzene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B039211.0 2/24/20 17:28 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B039211.0 2/24/20 17:28 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B039212002/24/20 17:28 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: M-14
Sample ID: 0020258-05
Work Order: 0020258
Time Collected: 02/14/20 13:00
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 17:28 JLBug/L 0.16Hexachlorobutadiene
0.90 *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B039211.0 2/24/20 17:28 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B039211.0 2/24/20 17:28 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B039215.0 2/24/20 17:28 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B039211.0 2/24/20 17:28 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B039212.0 2/24/20 17:28 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0B039211.0 2/24/20 17:28 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B039211.0 2/24/20 17:28 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.047Styrene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.044Toluene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B039215.0 2/24/20 17:28 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B039210.50 2/24/20 17:28 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B039211.5 2/24/20 17:28 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
70-13099 %Dibromofluoromethane
70-13096 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-17
Sample ID: 0020258-06
Work Order: 0020258
Time Collected: 02/13/20 13:20
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 17:53 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B039212.0 2/24/20 17:53 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03921102/24/20 17:53 JLBug/L 0.31Acetone
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.048Benzene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B039211.0 2/24/20 17:53 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B039211.0 2/24/20 17:53 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B039212002/24/20 17:53 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-17
Sample ID: 0020258-06
Work Order: 0020258
Time Collected: 02/13/20 13:20
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 17:53 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B039211.0 2/24/20 17:53 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B039211.0 2/24/20 17:53 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B039215.0 2/24/20 17:53 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B039211.0 2/24/20 17:53 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B039212.0 2/24/20 17:53 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0B039211.0 2/24/20 17:53 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B039211.0 2/24/20 17:53 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.047Styrene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.044Toluene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B039215.0 2/24/20 17:53 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B039210.50 2/24/20 17:53 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B039211.5 2/24/20 17:53 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13095 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-18
Sample ID: 0020258-07
Work Order: 0020258
Time Collected: 02/13/20 13:40
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 18:17 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B039212.0 2/24/20 18:17 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03921102/24/20 18:17 JLBug/L 0.31Acetone
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.048Benzene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B039211.0 2/24/20 18:17 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B039211.0 2/24/20 18:17 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B039212002/24/20 18:17 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-18
Sample ID: 0020258-07
Work Order: 0020258
Time Collected: 02/13/20 13:40
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 18:17 JLBug/L 0.16Hexachlorobutadiene
5.0 *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B039211.0 2/24/20 18:17 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B039211.0 2/24/20 18:17 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B039215.0 2/24/20 18:17 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B039211.0 2/24/20 18:17 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B039212.0 2/24/20 18:17 JLBug/L 0.083Methylene Chloride
1.8 *SM6200 B P0B039211.0 2/24/20 18:17 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B039211.0 2/24/20 18:17 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.044o-Xylene
0.59 *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.047Styrene
0.97 *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.044Toluene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B039215.0 2/24/20 18:17 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B039210.50 2/24/20 18:17 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B039211.5 2/24/20 18:17 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
70-13098 %Dibromofluoromethane
70-13096 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-20
Sample ID: 0020258-08
Work Order: 0020258
Time Collected: 02/14/20 10:35
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 18:42 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B039212.0 2/24/20 18:42 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03921102/24/20 18:42 JLBug/L 0.31Acetone
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.048Benzene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B039211.0 2/24/20 18:42 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B039211.0 2/24/20 18:42 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B039212002/24/20 18:42 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-20
Sample ID: 0020258-08
Work Order: 0020258
Time Collected: 02/14/20 10:35
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 18:42 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B039211.0 2/24/20 18:42 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B039211.0 2/24/20 18:42 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B039215.0 2/24/20 18:42 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B039211.0 2/24/20 18:42 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B039212.0 2/24/20 18:42 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0B039211.0 2/24/20 18:42 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B039211.0 2/24/20 18:42 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.047Styrene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.044Toluene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B039215.0 2/24/20 18:42 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B039210.50 2/24/20 18:42 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B039211.5 2/24/20 18:42 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13096 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-21
Sample ID: 0020258-09
Work Order: 0020258
Time Collected: 02/14/20 10:15
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 19:07 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B039212.0 2/24/20 19:07 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03921102/24/20 19:07 JLBug/L 0.31Acetone
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.048Benzene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B039211.0 2/24/20 19:07 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B039211.0 2/24/20 19:07 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B039212002/24/20 19:07 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-21
Sample ID: 0020258-09
Work Order: 0020258
Time Collected: 02/14/20 10:15
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 19:07 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B039211.0 2/24/20 19:07 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B039211.0 2/24/20 19:07 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B039215.0 2/24/20 19:07 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B039211.0 2/24/20 19:07 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B039212.0 2/24/20 19:07 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0B039211.0 2/24/20 19:07 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B039211.0 2/24/20 19:07 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.047Styrene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.044Toluene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B039215.0 2/24/20 19:07 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B039210.50 2/24/20 19:07 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B039211.5 2/24/20 19:07 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
70-13099 %Dibromofluoromethane
70-13095 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-22
Sample ID: 0020258-10
Work Order: 0020258
Time Collected: 02/14/20 13:25
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 19:31 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B039212.0 2/24/20 19:31 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03921102/24/20 19:31 JLBug/L 0.31Acetone
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.048Benzene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B039211.0 2/24/20 19:31 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B039211.0 2/24/20 19:31 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B039212002/24/20 19:31 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-22
Sample ID: 0020258-10
Work Order: 0020258
Time Collected: 02/14/20 13:25
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 19:31 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B039211.0 2/24/20 19:31 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B039211.0 2/24/20 19:31 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B039215.0 2/24/20 19:31 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B039211.0 2/24/20 19:31 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B039212.0 2/24/20 19:31 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0B039211.0 2/24/20 19:31 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B039211.0 2/24/20 19:31 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.047Styrene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.044Toluene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B039215.0 2/24/20 19:31 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B039210.50 2/24/20 19:31 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B039211.5 2/24/20 19:31 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-13099 %Dibromofluoromethane
70-13095 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-23
Sample ID: 0020258-11
Work Order: 0020258
Time Collected: 02/14/20 11:00
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 19:56 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B039212.0 2/24/20 19:56 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03921102/24/20 19:56 JLBug/L 0.31Acetone
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.048Benzene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B039211.0 2/24/20 19:56 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B039211.0 2/24/20 19:56 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B039212002/24/20 19:56 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-23
Sample ID: 0020258-11
Work Order: 0020258
Time Collected: 02/14/20 11:00
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 19:56 JLBug/L 0.16Hexachlorobutadiene
18 *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B039211.0 2/24/20 19:56 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B039211.0 2/24/20 19:56 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B039215.0 2/24/20 19:56 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B039211.0 2/24/20 19:56 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B039212.0 2/24/20 19:56 JLBug/L 0.083Methylene Chloride
3.9 *SM6200 B P0B039211.0 2/24/20 19:56 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B039211.0 2/24/20 19:56 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.047Styrene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.044Toluene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B039215.0 2/24/20 19:56 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B039210.50 2/24/20 19:56 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B039211.5 2/24/20 19:56 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13095 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-24
Sample ID: 0020258-12
Work Order: 0020258
Time Collected: 02/13/20 14:50
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 1.11,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.611,1,1-Trichloroethane
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.661,1,2-Trichloroethane
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.831,1-Dichloroethane
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.831,1-Dichloroethylene
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.511,1-Dichloropropylene
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 4.01,2,3-Trichlorobenzene
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 1.41,2,3-Trichloropropane
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 1.31,2,4-Trichlorobenzene
1200 *SM6200 B P0B0388100502/24/20 23:41 JLBug/L 5.41,2,4-Trimethylbenzene
BRL *SM6200 B P0B038810202/24/20 23:07 JLBug/L 1.71,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.511,2-Dibromoethane
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.761,2-Dichlorobenzene
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.661,2-Dichloroethane
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 1.11,2-Dichloropropane
350 *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.761,3,5-Trimethylbenzene
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.541,3-Dichlorobenzene
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.431,3-Dichloropropane
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.501,4-Dichlorobenzene
BRL *SM6200 B P0B038810202/24/20 23:07 JLBug/L 1.12,2-Dichloropropane
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.662-Chlorotoluene
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.504-Chlorotoluene
10 *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.894-Isopropyltoluene
BRL *SM6200 B P0B0388101002/24/20 23:07 JLBug/L 3.1Acetone
130 *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.48Benzene
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.57Bromobenzene
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 1.4Bromochloromethane
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.62Bromodichloromethane
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.40Bromoform
BRL *SM6200 B P0B038810102/24/20 23:07 JLBug/L 1.8Bromomethane
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 1.1Carbon Tetrachloride
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.62Chlorobenzene
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 2.2Chloroethane
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.76Chloroform
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.79Chloromethane
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.56cis-1,2-Dichloroethylene
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.79cis-1,3-Dichloropropylene
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.81Dibromochloromethane
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.65Dibromomethane
BRL *SM6200 B P0B038810102/24/20 23:07 JLBug/L 1.1Dichlorodifluoromethane
BRL *SM6200 B P0B03881020002/24/20 23:07 JLBug/L 270Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-24
Sample ID: 0020258-12
Work Order: 0020258
Time Collected: 02/13/20 14:50
Time Submitted: 02/18/20 16:05
02170214.17
770 *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.61Ethylbenzene
BRL *SM6200 B P0B038810202/24/20 23:07 JLBug/L 1.6Hexachlorobutadiene
140 *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.50Isopropyl Ether
61 *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.54Isopropylbenzene (Cumene)
2600 *SM6200 B P0B03881001002/24/20 23:41 JLBug/L 12m,p-Xylenes
BRL *SM6200 B P0B038810102/24/20 23:07 JLBug/L 0.65Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B038810502/24/20 23:07 JLBug/L 2.4Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B038810102/24/20 23:07 JLBug/L 0.78Methyl Isobutyl Ketone
BRL *SM6200 B P0B038810202/24/20 23:07 JLBug/L 0.83Methylene Chloride
21 *SM6200 B P0B038810102/24/20 23:07 JLBug/L 0.42Methyl-tert-Butyl Ether
110 *SM6200 B P0B038810102/24/20 23:07 JLBug/L 1.9Naphthalene
64 *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.76n-Butylbenzene
200 *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.87n-Propylbenzene
1100 *SM6200 B P0B0388100502/24/20 23:41 JLBug/L 4.4o-Xylene
16 *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.76sec-Butylbenzene
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.47Styrene
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.88tert-Butylbenzene
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.98Tetrachloroethylene
1500 *SM6200 B P0B0388100502/24/20 23:41 JLBug/L 4.4Toluene
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.70trans-1,2-Dichloroethylene
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 1.2trans-1,3-Dichloropropylene
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.78Trichloroethylene
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.62Trichlorofluoromethane
BRL *SM6200 B P0B038810502/24/20 23:07 JLBug/L 0.60Vinyl acetate
BRL *SM6200 B P0B0388105.0 2/24/20 23:07 JLBug/L 0.97Vinyl chloride
3700 *SM6200 B P0B03881001502/24/20 23:41 JLBug/L 15Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-13098 %Dibromofluoromethane
70-13099 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-25
Sample ID: 0020258-13
Work Order: 0020258
Time Collected: 02/13/20 15:50
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 21:10 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B039212.0 2/24/20 21:10 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03921102/24/20 21:10 JLBug/L 0.31Acetone
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.048Benzene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B039211.0 2/24/20 21:10 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B039211.0 2/24/20 21:10 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B039212002/24/20 21:10 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-25
Sample ID: 0020258-13
Work Order: 0020258
Time Collected: 02/13/20 15:50
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 21:10 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B039211.0 2/24/20 21:10 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B039211.0 2/24/20 21:10 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B039215.0 2/24/20 21:10 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B039211.0 2/24/20 21:10 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B039212.0 2/24/20 21:10 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0B039211.0 2/24/20 21:10 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B039211.0 2/24/20 21:10 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.047Styrene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.044Toluene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B039215.0 2/24/20 21:10 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B039210.50 2/24/20 21:10 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B039211.5 2/24/20 21:10 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13096 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-26
Sample ID: 0020258-14
Work Order: 0020258
Time Collected: 02/13/20 16:30
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 20:21 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B039212.0 2/24/20 20:21 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03921102/24/20 20:21 JLBug/L 0.31Acetone
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.048Benzene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B039211.0 2/24/20 20:21 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B039211.0 2/24/20 20:21 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B039212002/24/20 20:21 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-26
Sample ID: 0020258-14
Work Order: 0020258
Time Collected: 02/13/20 16:30
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 20:21 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B039211.0 2/24/20 20:21 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B039211.0 2/24/20 20:21 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B039215.0 2/24/20 20:21 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B039211.0 2/24/20 20:21 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B039212.0 2/24/20 20:21 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0B039211.0 2/24/20 20:21 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B039211.0 2/24/20 20:21 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.047Styrene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.044Toluene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B039215.0 2/24/20 20:21 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B039210.50 2/24/20 20:21 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B039211.5 2/24/20 20:21 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130104 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-26D
Sample ID: 0020258-15
Work Order: 0020258
Time Collected: 02/13/20 17:00
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B039512.0 2/25/20 17:42 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B039512.0 2/25/20 17:42 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03951102/25/20 17:42 JLBug/L 0.31Acetone
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.048Benzene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B039511.0 2/25/20 17:42 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B039511.0 2/25/20 17:42 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B039512002/25/20 17:42 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-26D
Sample ID: 0020258-15
Work Order: 0020258
Time Collected: 02/13/20 17:00
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B039512.0 2/25/20 17:42 JLBug/L 0.16Hexachlorobutadiene
3.5 *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B039511.0 2/25/20 17:42 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B039511.0 2/25/20 17:42 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B039515.0 2/25/20 17:42 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B039511.0 2/25/20 17:42 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B039512.0 2/25/20 17:42 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0B039511.0 2/25/20 17:42 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B039511.0 2/25/20 17:42 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.047Styrene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.044Toluene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B039515.0 2/25/20 17:42 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B039510.50 2/25/20 17:42 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B039511.5 2/25/20 17:42 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13098 %4-Bromofluorobenzene
70-130101 %Dibromofluoromethane
70-13095 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-27
Sample ID: 0020258-16
Work Order: 0020258
Time Collected: 02/14/20 11:50
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 21:34 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B039212.0 2/24/20 21:34 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03921102/24/20 21:34 JLBug/L 0.31Acetone
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.048Benzene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B039211.0 2/24/20 21:34 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B039211.0 2/24/20 21:34 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B039212002/24/20 21:34 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-27
Sample ID: 0020258-16
Work Order: 0020258
Time Collected: 02/14/20 11:50
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B039212.0 2/24/20 21:34 JLBug/L 0.16Hexachlorobutadiene
82 *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B039211.0 2/24/20 21:34 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B039211.0 2/24/20 21:34 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B039215.0 2/24/20 21:34 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B039211.0 2/24/20 21:34 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B039212.0 2/24/20 21:34 JLBug/L 0.083Methylene Chloride
17 *SM6200 B P0B039211.0 2/24/20 21:34 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B039211.0 2/24/20 21:34 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.047Styrene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.044Toluene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B039215.0 2/24/20 21:34 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B039210.50 2/24/20 21:34 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B039211.5 2/24/20 21:34 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13095 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-27D
Sample ID: 0020258-17
Work Order: 0020258
Time Collected: 02/14/20 12:30
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B038812.0 2/24/20 21:59 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.0761,2-Dichlorobenzene
0.75 *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B038812.0 2/24/20 21:59 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03881102/24/20 21:59 JLBug/L 0.31Acetone
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.048Benzene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B038811.0 2/24/20 21:59 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B038811.0 2/24/20 21:59 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B038812002/24/20 21:59 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-27D
Sample ID: 0020258-17
Work Order: 0020258
Time Collected: 02/14/20 12:30
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B038812.0 2/24/20 21:59 JLBug/L 0.16Hexachlorobutadiene
140 *SM6200 B P0B0388105.0 2/24/20 22:33 JLBug/L 0.50Isopropyl Ether
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B038811.0 2/24/20 21:59 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B038811.0 2/24/20 21:59 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B038815.0 2/24/20 21:59 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B038811.0 2/24/20 21:59 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B038812.0 2/24/20 21:59 JLBug/L 0.083Methylene Chloride
26 *SM6200 B P0B038811.0 2/24/20 21:59 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B038811.0 2/24/20 21:59 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.047Styrene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.044Toluene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B038815.0 2/24/20 21:59 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B038810.50 2/24/20 21:59 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B038811.5 2/24/20 21:59 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-130108 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-8
Sample ID: 0020258-18
Work Order: 0020258
Time Collected: 02/14/20 13:40
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B039512.0 2/25/20 18:07 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B039512.0 2/25/20 18:07 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03951102/25/20 18:07 JLBug/L 0.31Acetone
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.048Benzene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B039511.0 2/25/20 18:07 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B039511.0 2/25/20 18:07 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B039512002/25/20 18:07 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-8
Sample ID: 0020258-18
Work Order: 0020258
Time Collected: 02/14/20 13:40
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B039512.0 2/25/20 18:07 JLBug/L 0.16Hexachlorobutadiene
11 *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B039511.0 2/25/20 18:07 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B039511.0 2/25/20 18:07 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B039515.0 2/25/20 18:07 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B039511.0 2/25/20 18:07 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B039512.0 2/25/20 18:07 JLBug/L 0.083Methylene Chloride
1.2 *SM6200 B P0B039511.0 2/25/20 18:07 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B039511.0 2/25/20 18:07 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.047Styrene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.044Toluene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B039515.0 2/25/20 18:07 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B039510.50 2/25/20 18:07 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B039511.5 2/25/20 18:07 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-13099 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-10
Sample ID: 0020258-19
Work Order: 0020258
Time Collected: 02/14/20 14:40
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B038812.0 2/24/20 19:09 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B038812.0 2/24/20 19:09 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03881102/24/20 19:09 JLBug/L 0.31Acetone
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.048Benzene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B038811.0 2/24/20 19:09 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B038811.0 2/24/20 19:09 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B038812002/24/20 19:09 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-10
Sample ID: 0020258-19
Work Order: 0020258
Time Collected: 02/14/20 14:40
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B038812.0 2/24/20 19:09 JLBug/L 0.16Hexachlorobutadiene
2.4 *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B038811.0 2/24/20 19:09 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B038811.0 2/24/20 19:09 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B038815.0 2/24/20 19:09 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B038811.0 2/24/20 19:09 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B038812.0 2/24/20 19:09 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0B038811.0 2/24/20 19:09 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B038811.0 2/24/20 19:09 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.047Styrene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.044Toluene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B038815.0 2/24/20 19:09 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B038810.50 2/24/20 19:09 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B038811.5 2/24/20 19:09 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13098 %4-Bromofluorobenzene
70-130109 %Dibromofluoromethane
70-13099 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-12
Sample ID: 0020258-20
Work Order: 0020258
Time Collected: 02/13/20 16:10
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B039512.0 2/26/20 0:40 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.0761,2-Dichlorobenzene
1.6 *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B039512.0 2/26/20 0:40 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03951102/26/20 0:40 JLBug/L 0.31Acetone
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.048Benzene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B039511.0 2/26/20 0:40 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B039511.0 2/26/20 0:40 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B039512002/26/20 0:40 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-12
Sample ID: 0020258-20
Work Order: 0020258
Time Collected: 02/13/20 16:10
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B039512.0 2/26/20 0:40 JLBug/L 0.16Hexachlorobutadiene
80 *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B039511.0 2/26/20 0:40 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B039511.0 2/26/20 0:40 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B039515.0 2/26/20 0:40 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B039511.0 2/26/20 0:40 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B039512.0 2/26/20 0:40 JLBug/L 0.083Methylene Chloride
18 *SM6200 B P0B039511.0 2/26/20 0:40 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B039511.0 2/26/20 0:40 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.047Styrene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.044Toluene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B039515.0 2/26/20 0:40 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B039510.50 2/26/20 0:40 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B039511.5 2/26/20 0:40 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13094 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-15
Sample ID: 0020258-21
Work Order: 0020258
Time Collected: 02/14/20 15:20
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B039512.0 2/25/20 18:32 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B039512.0 2/25/20 18:32 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03951102/25/20 18:32 JLBug/L 0.31Acetone
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.048Benzene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B039511.0 2/25/20 18:32 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B039511.0 2/25/20 18:32 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B039512002/25/20 18:32 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-15
Sample ID: 0020258-21
Work Order: 0020258
Time Collected: 02/14/20 15:20
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B039512.0 2/25/20 18:32 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B039511.0 2/25/20 18:32 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B039511.0 2/25/20 18:32 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B039515.0 2/25/20 18:32 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B039511.0 2/25/20 18:32 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B039512.0 2/25/20 18:32 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0B039511.0 2/25/20 18:32 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B039511.0 2/25/20 18:32 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.047Styrene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.044Toluene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B039515.0 2/25/20 18:32 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B039510.50 2/25/20 18:32 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B039511.5 2/25/20 18:32 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-13099 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-17
Sample ID: 0020258-22
Work Order: 0020258
Time Collected: 02/14/20 15:03
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B039512.0 2/25/20 18:56 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B039512.0 2/25/20 18:56 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03951102/25/20 18:56 JLBug/L 0.31Acetone
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.048Benzene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B039511.0 2/25/20 18:56 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B039511.0 2/25/20 18:56 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B039512002/25/20 18:56 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-17
Sample ID: 0020258-22
Work Order: 0020258
Time Collected: 02/14/20 15:03
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B039512.0 2/25/20 18:56 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B039511.0 2/25/20 18:56 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B039511.0 2/25/20 18:56 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B039515.0 2/25/20 18:56 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B039511.0 2/25/20 18:56 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B039512.0 2/25/20 18:56 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0B039511.0 2/25/20 18:56 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B039511.0 2/25/20 18:56 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.047Styrene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.044Toluene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B039515.0 2/25/20 18:56 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B039510.50 2/25/20 18:56 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B039511.5 2/25/20 18:56 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-13099 %Dibromofluoromethane
70-13095 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-14
Sample ID: 0020258-23
Work Order: 0020258
Time Collected: 02/14/20 15:03
Time Submitted: 02/18/20 16:05
02170214.17
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0B039512.0 2/25/20 19:21 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0B039512.0 2/25/20 19:21 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0B03951102/25/20 19:21 JLBug/L 0.31Acetone
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.048Benzene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.040Bromoform
BRL *SM6200 B P0B039511.0 2/25/20 19:21 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.076Chloroform
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0B039511.0 2/25/20 19:21 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0B039512002/25/20 19:21 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
Laboratory Report
03/02/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-14
Sample ID: 0020258-23
Work Order: 0020258
Time Collected: 02/14/20 15:03
Time Submitted: 02/18/20 16:05
02170214.17
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0B039512.0 2/25/20 19:21 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0B039511.0 2/25/20 19:21 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0B039511.0 2/25/20 19:21 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0B039515.0 2/25/20 19:21 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0B039511.0 2/25/20 19:21 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0B039512.0 2/25/20 19:21 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0B039511.0 2/25/20 19:21 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0B039511.0 2/25/20 19:21 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.047Styrene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.044Toluene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0B039515.0 2/25/20 19:21 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0B039510.50 2/25/20 19:21 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0B039511.5 2/25/20 19:21 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13095 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
3/2/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.17
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0020258
Time Submitted: 2/18/2020 4:05:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0B0388 - 5030B
Blank (P0B0388-BLK1)Prepared & Analyzed: 02/24/20
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL10
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL1.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethanol ug/LBRL200
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
3/2/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.17
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0020258
Time Submitted: 2/18/2020 4:05:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0B0388 - 5030B
Blank (P0B0388-BLK1)Prepared & Analyzed: 02/24/20
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL1.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL0.50
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL5.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9748.6
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10753.3
ug/L 50.00 70-130Surrogate: Toluene-d8 9748.6
LCS (P0B0388-BS1)Prepared & Analyzed: 02/24/20
1,1,1,2-Tetrachloroethane ug/L22.6 0.50 20.00 70-130113
1,1,1-Trichloroethane ug/L21.7 0.50 20.00 70-130109
1,1,2,2-Tetrachloroethane ug/L21.1 0.50 20.00 70-130106
1,1,2-Trichloroethane ug/L21.5 0.50 20.00 70-130108
1,1-Dichloroethane ug/L22.3 0.50 20.00 70-130111
1,1-Dichloroethylene ug/L21.7 0.50 20.00 70-130109
1,1-Dichloropropylene ug/L21.9 0.50 20.00 70-130110
1,2,3-Trichlorobenzene ug/L22.1 0.50 20.00 70-130110
1,2,3-Trichloropropane ug/L21.0 0.50 20.00 70-130105
1,2,4-Trichlorobenzene ug/L20.7 0.50 20.00 70-130104
1,2,4-Trimethylbenzene ug/L21.7 0.50 20.00 70-130109
1,2-Dibromo-3-chloropropane ug/L20.8 2.0 20.00 70-130104
1,2-Dibromoethane ug/L23.2 0.50 20.00 70-130116
1,2-Dichlorobenzene ug/L20.7 0.50 20.00 70-130104
1,2-Dichloroethane ug/L20.8 0.50 20.00 70-130104
1,2-Dichloropropane ug/L21.2 0.50 20.00 70-130106
1,3,5-Trimethylbenzene ug/L20.9 0.50 20.00 70-130104
1,3-Dichlorobenzene ug/L20.8 0.50 20.00 70-130104
1,3-Dichloropropane ug/L22.2 0.50 20.00 70-130111
1,4-Dichlorobenzene ug/L20.8 0.50 20.00 70-130104
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
3/2/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.17
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0020258
Time Submitted: 2/18/2020 4:05:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0B0388 - 5030B
LCS (P0B0388-BS1)Prepared & Analyzed: 02/24/20
2,2-Dichloropropane ug/L22.1 2.0 20.00 70-130110
2-Chlorotoluene ug/L20.8 0.50 20.00 70-130104
4-Chlorotoluene ug/L21.0 0.50 20.00 70-130105
4-Isopropyltoluene ug/L22.2 0.50 20.00 70-130111
Acetone ug/L33.2 10 40.00 40-16083
Benzene ug/L21.5 0.50 20.00 70-130108
Bromobenzene ug/L21.4 0.50 20.00 70-130107
Bromochloromethane ug/L21.6 0.50 20.00 70-130108
Bromodichloromethane ug/L21.1 0.50 20.00 70-130106
Bromoform ug/L23.1 0.50 20.00 70-130116
Bromomethane ug/L23.6 1.0 20.00 60-140118
Carbon Tetrachloride ug/L21.9 0.50 20.00 70-130110
Chlorobenzene ug/L21.2 0.50 20.00 70-130106
Chloroethane ug/L21.6 0.50 20.00 60-140108
Chloroform ug/L21.5 0.50 20.00 70-130108
Chloromethane ug/L20.6 0.50 20.00 60-140103
cis-1,2-Dichloroethylene ug/L19.7 0.50 20.00 70-13099
cis-1,3-Dichloropropylene ug/L22.1 0.50 20.00 70-130110
Dibromochloromethane ug/L21.3 0.50 20.00 70-130107
Dibromomethane ug/L21.6 0.50 20.00 70-130108
Dichlorodifluoromethane ug/L20.9 1.0 20.00 60-140104
Ethanol ug/L604 200 500.0 60-140121
Ethylbenzene ug/L22.4 0.50 20.00 70-130112
Hexachlorobutadiene ug/L21.1 2.0 20.00 70-130105
Isopropyl Ether ug/L20.8 0.50 20.00 70-130104
Isopropylbenzene (Cumene)ug/L22.2 0.50 20.00 70-130111
m,p-Xylenes ug/L45.4 1.0 40.00 70-130114
Methyl Butyl Ketone (2-Hexanone)ug/L19.9 1.0 20.00 60-140100
Methyl Ethyl Ketone (2-Butanone)ug/L18.4 5.0 20.00 60-14092
Methyl Isobutyl Ketone ug/L23.4 1.0 20.00 60-140117
Methylene Chloride ug/L20.5 2.0 20.00 70-130103
Methyl-tert-Butyl Ether ug/L21.0 1.0 20.00 70-130105
Naphthalene ug/L21.0 1.0 20.00 70-130105
n-Butylbenzene ug/L21.7 0.50 20.00 70-130109
n-Propylbenzene ug/L21.2 0.50 20.00 70-130106
o-Xylene ug/L22.0 0.50 20.00 70-130110
sec-Butylbenzene ug/L22.1 0.50 20.00 70-130110
Styrene ug/L23.0 0.50 20.00 70-130115
tert-Butylbenzene ug/L22.2 0.50 20.00 70-130111
Tetrachloroethylene ug/L21.6 0.50 20.00 70-130108
Toluene ug/L21.8 0.50 20.00 70-130109
trans-1,2-Dichloroethylene ug/L21.2 0.50 20.00 70-130106
trans-1,3-Dichloropropylene ug/L21.7 0.50 20.00 70-130108
Trichloroethylene ug/L20.7 0.50 20.00 70-130104
Trichlorofluoromethane ug/L22.3 0.50 20.00 60-140112
Vinyl acetate ug/L23.9 5.0 20.00 60-140119
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
3/2/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.17
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0020258
Time Submitted: 2/18/2020 4:05:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0B0388 - 5030B
LCS (P0B0388-BS1)Prepared & Analyzed: 02/24/20
Vinyl chloride ug/L24.2 0.50 20.00 60-140121
Xylenes, total ug/L67.5 1.5 60.00 70-130112
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9949.3
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10150.4
ug/L 50.00 70-130Surrogate: Toluene-d8 10050.2
Batch P0B0392 - SM6200 B
Blank (P0B0392-BLK1)Prepared & Analyzed: 02/24/20
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL10
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL1.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
3/2/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.17
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0020258
Time Submitted: 2/18/2020 4:05:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0B0392 - SM6200 B
Blank (P0B0392-BLK1)Prepared & Analyzed: 02/24/20
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethanol ug/LBRL200
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL1.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL0.50
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL5.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.4
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9748.5
ug/L 50.00 70-130Surrogate: Toluene-d8 9647.8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
3/2/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.17
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0020258
Time Submitted: 2/18/2020 4:05:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0B0392 - SM6200 B
LCS (P0B0392-BS1)Prepared & Analyzed: 02/24/20
1,1,1,2-Tetrachloroethane ug/L20.5 0.50 20.00 70-130102
1,1,1-Trichloroethane ug/L21.2 0.50 20.00 70-130106
1,1,2,2-Tetrachloroethane ug/L20.3 0.50 20.00 70-130101
1,1,2-Trichloroethane ug/L21.3 0.50 20.00 70-130107
1,1-Dichloroethane ug/L21.4 0.50 20.00 70-130107
1,1-Dichloroethylene ug/L20.6 0.50 20.00 70-130103
1,1-Dichloropropylene ug/L20.9 0.50 20.00 70-130105
1,2,3-Trichlorobenzene ug/L21.6 0.50 20.00 70-130108
1,2,3-Trichloropropane ug/L19.7 0.50 20.00 70-13098
1,2,4-Trichlorobenzene ug/L20.3 0.50 20.00 70-130102
1,2,4-Trimethylbenzene ug/L19.5 0.50 20.00 70-13098
1,2-Dibromo-3-chloropropane ug/L18.2 2.0 20.00 70-13091
1,2-Dibromoethane ug/L19.8 0.50 20.00 70-13099
1,2-Dichlorobenzene ug/L19.6 0.50 20.00 70-13098
1,2-Dichloroethane ug/L20.4 0.50 20.00 70-130102
1,2-Dichloropropane ug/L21.0 0.50 20.00 70-130105
1,3,5-Trimethylbenzene ug/L19.6 0.50 20.00 70-13098
1,3-Dichlorobenzene ug/L19.7 0.50 20.00 70-13098
1,3-Dichloropropane ug/L20.6 0.50 20.00 70-130103
1,4-Dichlorobenzene ug/L19.1 0.50 20.00 70-13096
2,2-Dichloropropane ug/L21.4 2.0 20.00 70-130107
2-Chlorotoluene ug/L19.8 0.50 20.00 70-13099
4-Chlorotoluene ug/L19.7 0.50 20.00 70-13098
4-Isopropyltoluene ug/L19.3 0.50 20.00 70-13096
Acetone ug/L36.2 10 40.00 40-16090
Benzene ug/L20.7 0.50 20.00 70-130104
Bromobenzene ug/L20.2 0.50 20.00 70-130101
Bromochloromethane ug/L20.9 0.50 20.00 70-130104
Bromodichloromethane ug/L21.2 0.50 20.00 70-130106
Bromoform ug/L19.8 0.50 20.00 70-13099
Bromomethane ug/L17.2 1.0 20.00 60-14086
Carbon Tetrachloride ug/L19.6 0.50 20.00 70-13098
Chlorobenzene ug/L19.8 0.50 20.00 70-13099
Chloroethane ug/L24.7 0.50 20.00 60-140124
Chloroform ug/L21.2 0.50 20.00 70-130106
Chloromethane ug/L19.0 0.50 20.00 60-14095
cis-1,2-Dichloroethylene ug/L20.6 0.50 20.00 70-130103
cis-1,3-Dichloropropylene ug/L20.6 0.50 20.00 70-130103
Dibromochloromethane ug/L20.0 0.50 20.00 70-130100
Dibromomethane ug/L20.6 0.50 20.00 70-130103
Dichlorodifluoromethane ug/L20.7 1.0 20.00 60-140104
Ethanol ug/L567 200 500.0 60-140113
Ethylbenzene ug/L19.9 0.50 20.00 70-130100
Hexachlorobutadiene ug/L20.7 2.0 20.00 70-130104
Isopropyl Ether ug/L20.4 0.50 20.00 70-130102
Isopropylbenzene (Cumene)ug/L20.0 0.50 20.00 70-130100
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
3/2/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.17
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0020258
Time Submitted: 2/18/2020 4:05:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0B0392 - SM6200 B
LCS (P0B0392-BS1)Prepared & Analyzed: 02/24/20
m,p-Xylenes ug/L40.3 1.0 40.00 70-130101
Methyl Butyl Ketone (2-Hexanone)ug/L19.6 1.0 20.00 60-14098
Methyl Ethyl Ketone (2-Butanone)ug/L21.6 5.0 20.00 60-140108
Methyl Isobutyl Ketone ug/L20.4 1.0 20.00 60-140102
Methylene Chloride ug/L19.6 2.0 20.00 70-13098
Methyl-tert-Butyl Ether ug/L20.6 1.0 20.00 70-130103
Naphthalene ug/L19.1 1.0 20.00 70-13096
n-Butylbenzene ug/L19.9 0.50 20.00 70-130100
n-Propylbenzene ug/L19.7 0.50 20.00 70-13098
o-Xylene ug/L19.8 0.50 20.00 70-13099
sec-Butylbenzene ug/L19.4 0.50 20.00 70-13097
Styrene ug/L20.0 0.50 20.00 70-130100
tert-Butylbenzene ug/L19.0 0.50 20.00 70-13095
Tetrachloroethylene ug/L20.1 0.50 20.00 70-130100
Toluene ug/L20.9 0.50 20.00 70-130104
trans-1,2-Dichloroethylene ug/L20.5 0.50 20.00 70-130102
trans-1,3-Dichloropropylene ug/L21.2 0.50 20.00 70-130106
Trichloroethylene ug/L19.6 0.50 20.00 70-13098
Trichlorofluoromethane ug/L21.3 0.50 20.00 60-140106
Vinyl acetate ug/L23.1 5.0 20.00 60-140115
Vinyl chloride ug/L23.0 0.50 20.00 60-140115
Xylenes, total ug/L60.1 1.5 60.00 70-130100
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10050.1
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9648.2
ug/L 50.00 70-130Surrogate: Toluene-d8 9848.8
Matrix Spike (P0B0392-MS1)Prepared & Analyzed: 02/24/20 Source: 0020258-03
1,1,1,2-Tetrachloroethane ug/L2055.0 200.0 BRL 70-130103
1,1,1-Trichloroethane ug/L2225.0 200.0 BRL 70-130111
1,1,2,2-Tetrachloroethane ug/L1965.0 200.0 BRL 70-13098
1,1,2-Trichloroethane ug/L2105.0 200.0 BRL 70-130105
1,1-Dichloroethane ug/L2225.0 200.0 BRL 70-130111
1,1-Dichloroethylene ug/L2235.0 200.0 BRL 70-130111
1,1-Dichloropropylene ug/L2185.0 200.0 BRL 70-130109
1,2,3-Trichlorobenzene ug/L1925.0 200.0 BRL 70-13096
1,2,3-Trichloropropane ug/L1995.0 200.0 BRL 70-130100
1,2,4-Trichlorobenzene ug/L1965.0 200.0 BRL 70-13098
1,2,4-Trimethylbenzene ug/L1985.0 200.0 BRL 70-13099
1,2-Dibromo-3-chloropropane ug/L17820 200.0 BRL 70-13089
1,2-Dibromoethane ug/L2005.0 200.0 BRL 70-130100
1,2-Dichlorobenzene ug/L1965.0 200.0 BRL 70-13098
1,2-Dichloroethane ug/L2145.0 200.0 BRL 70-130107
1,2-Dichloropropane ug/L2125.0 200.0 BRL 70-130106
1,3,5-Trimethylbenzene ug/L1955.0 200.0 BRL 70-13098
1,3-Dichlorobenzene ug/L1985.0 200.0 BRL 70-13099
1,3-Dichloropropane ug/L2045.0 200.0 BRL 70-130102
1,4-Dichlorobenzene ug/L1925.0 200.0 BRL 70-13096
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
3/2/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.17
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0020258
Time Submitted: 2/18/2020 4:05:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0B0392 - SM6200 B
Matrix Spike (P0B0392-MS1)Prepared & Analyzed: 02/24/20 Source: 0020258-03
2,2-Dichloropropane ug/L21920 200.0 BRL 70-130109
2-Chlorotoluene ug/L2005.0 200.0 BRL 70-130100
4-Chlorotoluene ug/L2005.0 200.0 BRL 70-130100
4-Isopropyltoluene ug/L1945.0 200.0 BRL 70-13097
Acetone ug/L313 100 400.0 BRL 40-16078
Benzene ug/L2165.0 200.0 BRL 70-130108
Bromobenzene ug/L2035.0 200.0 BRL 70-130102
Bromochloromethane ug/L2145.0 200.0 BRL 70-130107
Bromodichloromethane ug/L2095.0 200.0 BRL 70-130105
Bromoform ug/L1965.0 200.0 BRL 70-13098
Bromomethane ug/L110 10 200.0 BRL M60-14055
Carbon Tetrachloride ug/L2115.0 200.0 BRL 70-130106
Chlorobenzene ug/L2005.0 200.0 BRL 70-130100
Chloroethane ug/L2525.0 200.0 BRL 60-140126
Chloroform ug/L2225.0 200.0 BRL 70-130111
Chloromethane ug/L1925.0 200.0 BRL 60-14096
cis-1,2-Dichloroethylene ug/L2085.0 200.0 BRL 70-130104
cis-1,3-Dichloropropylene ug/L2065.0 200.0 BRL 70-130103
Dibromochloromethane ug/L2005.0 200.0 BRL 70-130100
Dibromomethane ug/L2095.0 200.0 BRL 70-130105
Dichlorodifluoromethane ug/L22610 200.0 BRL 60-140113
Ethanol ug/L5560 2000 5000 BRL 60-140111
Ethylbenzene ug/L2045.0 200.0 BRL 70-130102
Hexachlorobutadiene ug/L19920 200.0 BRL 70-13099
Isopropyl Ether ug/L2105.0 200.0 4.00 70-130103
Isopropylbenzene (Cumene)ug/L2055.0 200.0 BRL 70-130103
m,p-Xylenes ug/L41210 400.0 BRL 70-130103
Methyl Butyl Ketone (2-Hexanone)ug/L18510 200.0 BRL 60-14092
Methyl Ethyl Ketone (2-Butanone)ug/L20750 200.0 BRL 60-140103
Methyl Isobutyl Ketone ug/L19410 200.0 BRL 60-14097
Methylene Chloride ug/L19420 200.0 BRL 70-13097
Methyl-tert-Butyl Ether ug/L21210 200.0 0.980 70-130106
Naphthalene ug/L17110 200.0 BRL 70-13086
n-Butylbenzene ug/L1925.0 200.0 BRL 70-13096
n-Propylbenzene ug/L2005.0 200.0 BRL 70-130100
o-Xylene ug/L2015.0 200.0 BRL 70-130101
sec-Butylbenzene ug/L1985.0 200.0 BRL 70-13099
Styrene ug/L1995.0 200.0 BRL 70-130100
tert-Butylbenzene ug/L1965.0 200.0 BRL 70-13098
Tetrachloroethylene ug/L2015.0 200.0 BRL 70-130100
Toluene ug/L2165.0 200.0 BRL 70-130108
trans-1,2-Dichloroethylene ug/L2145.0 200.0 BRL 70-130107
trans-1,3-Dichloropropylene ug/L2125.0 200.0 BRL 70-130106
Trichloroethylene ug/L2085.0 200.0 BRL 70-130104
Trichlorofluoromethane ug/L2245.0 200.0 BRL 60-140112
Vinyl acetate ug/L23950 200.0 BRL 60-140120
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
3/2/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.17
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0020258
Time Submitted: 2/18/2020 4:05:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0B0392 - SM6200 B
Matrix Spike (P0B0392-MS1)Prepared & Analyzed: 02/24/20 Source: 0020258-03
Vinyl chloride ug/L2355.0 200.0 BRL 60-140117
Xylenes, total ug/L61315 600.0 BRL 70-130102
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10250.9
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9848.8
ug/L 50.00 70-130Surrogate: Toluene-d8 9748.5
Matrix Spike Dup (P0B0392-MSD1)Prepared & Analyzed: 02/24/20 Source: 0020258-03
1,1,1,2-Tetrachloroethane ug/L2035.0 200.0 BRL 2070-130101 1
1,1,1-Trichloroethane ug/L2155.0 200.0 BRL 2070-130107 3
1,1,2,2-Tetrachloroethane ug/L2045.0 200.0 BRL 2070-130102 4
1,1,2-Trichloroethane ug/L2155.0 200.0 BRL 2070-130107 2
1,1-Dichloroethane ug/L2205.0 200.0 BRL 2070-130110 0.9
1,1-Dichloroethylene ug/L2075.0 200.0 BRL 2070-130104 7
1,1-Dichloropropylene ug/L2135.0 200.0 BRL 2070-130106 2
1,2,3-Trichlorobenzene ug/L2015.0 200.0 BRL 2070-130100 4
1,2,3-Trichloropropane ug/L1995.0 200.0 BRL 2070-130100 0.2
1,2,4-Trichlorobenzene ug/L1985.0 200.0 BRL 2070-13099 1
1,2,4-Trimethylbenzene ug/L1965.0 200.0 BRL 2070-13098 1
1,2-Dibromo-3-chloropropane ug/L19620 200.0 BRL 2070-13098 9
1,2-Dibromoethane ug/L2035.0 200.0 BRL 2070-130101 1
1,2-Dichlorobenzene ug/L1985.0 200.0 BRL 2070-13099 1
1,2-Dichloroethane ug/L2095.0 200.0 BRL 2070-130105 2
1,2-Dichloropropane ug/L2155.0 200.0 BRL 2070-130107 1
1,3,5-Trimethylbenzene ug/L1945.0 200.0 BRL 2070-13097 0.7
1,3-Dichlorobenzene ug/L1975.0 200.0 BRL 2070-13099 0.3
1,3-Dichloropropane ug/L2065.0 200.0 BRL 2070-130103 0.7
1,4-Dichlorobenzene ug/L1915.0 200.0 BRL 2070-13095 0.7
2,2-Dichloropropane ug/L21820 200.0 BRL 2070-130109 0.5
2-Chlorotoluene ug/L1985.0 200.0 BRL 2070-13099 1
4-Chlorotoluene ug/L2005.0 200.0 BRL 2070-130100 0.05
4-Isopropyltoluene ug/L1925.0 200.0 BRL 2070-13096 0.9
Acetone ug/L323 100 400.0 BRL 2040-16081 3
Benzene ug/L2105.0 200.0 BRL 2070-130105 3
Bromobenzene ug/L2025.0 200.0 BRL 2070-130101 0.7
Bromochloromethane ug/L2115.0 200.0 BRL 2070-130106 1
Bromodichloromethane ug/L2135.0 200.0 BRL 2070-130106 2
Bromoform ug/L1955.0 200.0 BRL 2070-13098 0.6
Bromomethane ug/L14010 200.0 BRL 20 D60-14070 24
Carbon Tetrachloride ug/L2025.0 200.0 BRL 2070-130101 5
Chlorobenzene ug/L1965.0 200.0 BRL 2070-13098 2
Chloroethane ug/L2525.0 200.0 BRL 2060-140126 0.2
Chloroform ug/L2195.0 200.0 BRL 2070-130110 1
Chloromethane ug/L1895.0 200.0 BRL 2060-14094 2
cis-1,2-Dichloroethylene ug/L2065.0 200.0 BRL 2070-130103 1
cis-1,3-Dichloropropylene ug/L2065.0 200.0 BRL 2070-130103 0.4
Dibromochloromethane ug/L1975.0 200.0 BRL 2070-13099 2
Dibromomethane ug/L2135.0 200.0 BRL 2070-130107 2
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
3/2/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.17
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0020258
Time Submitted: 2/18/2020 4:05:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0B0392 - SM6200 B
Matrix Spike Dup (P0B0392-MSD1)Prepared & Analyzed: 02/24/20 Source: 0020258-03
Dichlorodifluoromethane ug/L21210 200.0 BRL 2060-140106 7
Ethanol ug/L5800 2000 5000 BRL 2060-140116 4
Ethylbenzene ug/L2005.0 200.0 BRL 2070-130100 2
Hexachlorobutadiene ug/L20220 200.0 BRL 2070-130101 2
Isopropyl Ether ug/L2105.0 200.0 4.00 2070-130103 0.4
Isopropylbenzene (Cumene)ug/L1985.0 200.0 BRL 2070-13099 3
m,p-Xylenes ug/L40410 400.0 BRL 2070-130101 2
Methyl Butyl Ketone (2-Hexanone)ug/L19910 200.0 BRL 2060-14099 7
Methyl Ethyl Ketone (2-Butanone)ug/L21450 200.0 BRL 2060-140107 4
Methyl Isobutyl Ketone ug/L20610 200.0 BRL 2060-140103 6
Methylene Chloride ug/L19820 200.0 BRL 2070-13099 3
Methyl-tert-Butyl Ether ug/L21410 200.0 0.980 2070-130107 0.9
Naphthalene ug/L18710 200.0 BRL 2070-13094 9
n-Butylbenzene ug/L1955.0 200.0 BRL 2170-13098 1
n-Propylbenzene ug/L1945.0 200.0 BRL 1870-13097 3
o-Xylene ug/L1995.0 200.0 BRL 2070-130100 1
sec-Butylbenzene ug/L1935.0 200.0 BRL 2070-13097 3
Styrene ug/L1985.0 200.0 BRL 2070-13099 0.4
tert-Butylbenzene ug/L1925.0 200.0 BRL 2070-13096 2
Tetrachloroethylene ug/L1975.0 200.0 BRL 2070-13098 2
Toluene ug/L2145.0 200.0 BRL 2070-130107 1
trans-1,2-Dichloroethylene ug/L2065.0 200.0 BRL 2070-130103 4
trans-1,3-Dichloropropylene ug/L2135.0 200.0 BRL 2070-130106 0.09
Trichloroethylene ug/L2015.0 200.0 BRL 2070-130100 4
Trichlorofluoromethane ug/L2165.0 200.0 BRL 2060-140108 3
Vinyl acetate ug/L23650 200.0 BRL 2060-140118 1
Vinyl chloride ug/L2245.0 200.0 BRL 2060-140112 5
Xylenes, total ug/L60315 600.0 BRL 2070-130101 2
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.3
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9848.9
ug/L 50.00 70-130Surrogate: Toluene-d8 9748.7
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
3/2/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.17
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0020258
Time Submitted: 2/18/2020 4:05:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0B0395 - SM6200 B
Blank (P0B0395-BLK1)Prepared & Analyzed: 02/25/20
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL10
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL1.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethanol ug/LBRL200
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
3/2/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.17
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0020258
Time Submitted: 2/18/2020 4:05:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0B0395 - SM6200 B
Blank (P0B0395-BLK1)Prepared & Analyzed: 02/25/20
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL1.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL0.50
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL5.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.7
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9848.9
ug/L 50.00 70-130Surrogate: Toluene-d8 9647.8
LCS (P0B0395-BS1)Prepared & Analyzed: 02/25/20
1,1,1,2-Tetrachloroethane ug/L21.0 0.50 20.00 70-130105
1,1,1-Trichloroethane ug/L22.5 0.50 20.00 70-130113
1,1,2,2-Tetrachloroethane ug/L21.6 0.50 20.00 70-130108
1,1,2-Trichloroethane ug/L22.2 0.50 20.00 70-130111
1,1-Dichloroethane ug/L23.2 0.50 20.00 70-130116
1,1-Dichloroethylene ug/L22.2 0.50 20.00 70-130111
1,1-Dichloropropylene ug/L22.3 0.50 20.00 70-130112
1,2,3-Trichlorobenzene ug/L23.0 0.50 20.00 70-130115
1,2,3-Trichloropropane ug/L21.0 0.50 20.00 70-130105
1,2,4-Trichlorobenzene ug/L21.3 0.50 20.00 70-130107
1,2,4-Trimethylbenzene ug/L21.0 0.50 20.00 70-130105
1,2-Dibromo-3-chloropropane ug/L20.4 2.0 20.00 70-130102
1,2-Dibromoethane ug/L20.8 0.50 20.00 70-130104
1,2-Dichlorobenzene ug/L20.7 0.50 20.00 70-130104
1,2-Dichloroethane ug/L21.8 0.50 20.00 70-130109
1,2-Dichloropropane ug/L22.1 0.50 20.00 70-130110
1,3,5-Trimethylbenzene ug/L20.8 0.50 20.00 70-130104
1,3-Dichlorobenzene ug/L20.5 0.50 20.00 70-130102
1,3-Dichloropropane ug/L21.0 0.50 20.00 70-130105
1,4-Dichlorobenzene ug/L20.2 0.50 20.00 70-130101
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
3/2/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.17
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0020258
Time Submitted: 2/18/2020 4:05:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0B0395 - SM6200 B
LCS (P0B0395-BS1)Prepared & Analyzed: 02/25/20
2,2-Dichloropropane ug/L22.7 2.0 20.00 70-130114
2-Chlorotoluene ug/L21.2 0.50 20.00 70-130106
4-Chlorotoluene ug/L21.0 0.50 20.00 70-130105
4-Isopropyltoluene ug/L20.7 0.50 20.00 70-130103
Acetone ug/L34.0 10 40.00 40-16085
Benzene ug/L22.1 0.50 20.00 70-130111
Bromobenzene ug/L21.4 0.50 20.00 70-130107
Bromochloromethane ug/L22.1 0.50 20.00 70-130110
Bromodichloromethane ug/L22.0 0.50 20.00 70-130110
Bromoform ug/L20.2 0.50 20.00 70-130101
Bromomethane ug/L15.7 1.0 20.00 60-14078
Carbon Tetrachloride ug/L21.1 0.50 20.00 70-130106
Chlorobenzene ug/L20.4 0.50 20.00 70-130102
Chloroethane ug/L25.6 0.50 20.00 60-140128
Chloroform ug/L22.8 0.50 20.00 70-130114
Chloromethane ug/L19.8 0.50 20.00 60-14099
cis-1,2-Dichloroethylene ug/L21.7 0.50 20.00 70-130109
cis-1,3-Dichloropropylene ug/L21.5 0.50 20.00 70-130107
Dibromochloromethane ug/L20.7 0.50 20.00 70-130103
Dibromomethane ug/L21.8 0.50 20.00 70-130109
Dichlorodifluoromethane ug/L21.6 1.0 20.00 60-140108
Ethanol ug/L597 200 500.0 60-140119
Ethylbenzene ug/L21.1 0.50 20.00 70-130106
Hexachlorobutadiene ug/L21.8 2.0 20.00 70-130109
Isopropyl Ether ug/L21.6 0.50 20.00 70-130108
Isopropylbenzene (Cumene)ug/L21.8 0.50 20.00 70-130109
m,p-Xylenes ug/L42.4 1.0 40.00 70-130106
Methyl Butyl Ketone (2-Hexanone)ug/L20.0 1.0 20.00 60-140100
Methyl Ethyl Ketone (2-Butanone)ug/L24.4 5.0 20.00 60-140122
Methyl Isobutyl Ketone ug/L21.3 1.0 20.00 60-140106
Methylene Chloride ug/L20.3 2.0 20.00 70-130102
Methyl-tert-Butyl Ether ug/L21.6 1.0 20.00 70-130108
Naphthalene ug/L20.7 1.0 20.00 70-130104
n-Butylbenzene ug/L21.0 0.50 20.00 70-130105
n-Propylbenzene ug/L21.0 0.50 20.00 70-130105
o-Xylene ug/L20.8 0.50 20.00 70-130104
sec-Butylbenzene ug/L21.0 0.50 20.00 70-130105
Styrene ug/L21.2 0.50 20.00 70-130106
tert-Butylbenzene ug/L20.6 0.50 20.00 70-130103
Tetrachloroethylene ug/L20.5 0.50 20.00 70-130102
Toluene ug/L22.5 0.50 20.00 70-130112
trans-1,2-Dichloroethylene ug/L21.6 0.50 20.00 70-130108
trans-1,3-Dichloropropylene ug/L21.9 0.50 20.00 70-130109
Trichloroethylene ug/L21.2 0.50 20.00 70-130106
Trichlorofluoromethane ug/L22.8 0.50 20.00 60-140114
Vinyl acetate ug/L24.3 5.0 20.00 60-140121
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
3/2/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.17
Project: Shotwell GroceryWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0020258
Time Submitted: 2/18/2020 4:05:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0B0395 - SM6200 B
LCS (P0B0395-BS1)Prepared & Analyzed: 02/25/20
Vinyl chloride ug/L23.8 0.50 20.00 60-140119
Xylenes, total ug/L63.2 1.5 60.00 70-130105
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10351.6
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9848.8
ug/L 50.00 70-130Surrogate: Toluene-d8 9949.3
Sample Extraction Data
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P0B03880020258-02 02/24/20 9:1710 10mL mL
P0B03880020258-02 02/24/20 9:1710 10mL mL
P0B03880020258-12 02/24/20 9:1710 10mL mL
P0B03880020258-12 02/24/20 9:1710 10mL mL
P0B03880020258-17 02/24/20 9:1710 10mL mL
P0B03880020258-17 02/24/20 9:1710 10mL mL
P0B03880020258-19 02/24/20 9:1710 10mL mL
Prep Method: SM6200 B
Lab Number Batch Date/TimeInitialFinal
P0B03920020258-01 02/24/20 10:5810 10mL mL
P0B03920020258-03 02/24/20 10:5810 10mL mL
P0B03920020258-04 02/24/20 10:5810 10mL mL
P0B03920020258-05 02/24/20 10:5810 10mL mL
P0B03920020258-06 02/24/20 10:5810 10mL mL
P0B03920020258-07 02/24/20 10:5810 10mL mL
P0B03920020258-08 02/24/20 10:5810 10mL mL
P0B03920020258-09 02/24/20 10:5810 10mL mL
P0B03920020258-10 02/24/20 10:5810 10mL mL
P0B03920020258-11 02/24/20 10:5810 10mL mL
P0B03920020258-13 02/24/20 10:5810 10mL mL
P0B03920020258-14 02/24/20 10:5810 10mL mL
P0B03950020258-15 02/25/20 12:4410 10mL mL
P0B03920020258-16 02/24/20 10:5810 10mL mL
P0B03950020258-18 02/25/20 12:4410 10mL mL
P0B03950020258-20 02/25/20 12:4410 10mL mL
P0B03950020258-21 02/25/20 12:4410 10mL mL
P0B03950020258-22 02/25/20 12:4410 10mL mL
P0B03950020258-23 02/25/20 12:4410 10mL mL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409
APPENDIX B
COPY OF FIELD NOTES
APPENDIX C
PHOTOGRAPHIC DOCUMENTATION
Photo 1 Shotwell Grocery – View to West
Photo 2 View of Shotwell Grocery to North
Photo 3 Monitoring Well M-4
Photo 4 Monitoring Well M-13
Photo 5 Monitoring Well M-14
Photo 6 Monitoring Well MW-17
Photo 7 Monitoring Well MW-18
Photo 8 Monitoring Well MW-20
Photo 9 Monitoring Well MW-21
Photo 10 Monitoring Well MW-22
Photo 11 Monitoring Well MW-23
Photo 12 Monitoring Well MW-24
Photo 13 Monitoring Well MW-25
Photo 14 Monitoring Wells MW-26 & MW-26D
Photo 15 Monitoring Wells MW-27 & MW-27D
Photo 16 Monitoring Well DW-1
Photo 17 WSW-8 Sample Point
Photo 18 WSW-10
Photo 19 WSW-14
Photo 20 WSW-15
APPENDIX D
GENERAL STANDARD OPERATING PROCEDURES
Generalized Standard Operating Procedures (Not All Inclusive)
WithersRavenel
Our People. Your Success.
Soil Sampling, Soil Boring and Monitor Well Installation, Well Development
Soil borings are installed utilizing a stainless-steel hand auger, direct-push hydraulic drill or auger rotary
drill using either a macro core™ sampler, hollow stem augers, or air rotary roller cone bit. Soil borings are
typically sampled at discrete intervals from the bucket of a clean stainless steel hand auger, direct push
stainless steel sampler with acetate sleeve, or a split barrel sampler. When appropriate, soil samples may
be collected from drill cuttings associated with the boring or well installation.
Monitor wells are constructed within select soil borings of one, two, or four-inch inside diameter PVC
casing and machine slotted screen in accordance with NCAC Title 15A, Subchapter 02C (Well
Construction Standards, Criteria and Standards Applicable to Water Supply and Certain Other Wells).
Clean-washed “#2 Torpedo Sand” is typically utilized to fill the boring annulus surrounding the well
screen, extending to a minimum of 1-foot above the well screen. A minimum 1-foot thick bentonite clay
seal is emplaced above the sand pack and hydrated. Neat cement grout is placed in the remaining annulus
space from the upper portion of the bentonite seal to within 1-foot of surface grade. In coastal plain areas
where shallow groundwater is encountered, a variance to construction standards may be employed to
ensure the upper portion of the well screen intersects the upper aquifer surface. Wellheads may be
completed with either concrete-set flush mounted traffic-bearing steel skirted manholes with bolt down
covers or steel above-ground “stick-up” well protectors set in a concrete pad. The monitoring wells are
secured with locking caps. Temporary wells or piezometers may be completed with the PVC riser cut at
or above grade, and are abandoned within 24-hours of their installation.
Wells may be developed using a bailer, electric submersible pump, pneumatic pump, or peristaltic pump,
dependent upon site conditions. When wells are developed by the driller, they may be developed with
any of the methods outlined above, in addition to air or water injection. Soil boring logs and well
construction details are typically prepared for presentation in a report appendix. Borings completed in
bedrock may be drilled using air rotary, coring, or sonic drilling methods.
Groundwater Depth to Water Measurements
Groundwater level measurements are typically obtained using an electronic water level indicator which
registers a tone and/or illuminated light when the probe contacts groundwater. Depth to groundwater
measurements are obtained by lowering the probe attached to a cable usually marked in 0.01 foot
intervals into the well until the probe of the meter intersects the water surface. The measurement from
the top of the riser pipe or top of casing (TOC) to the water level is recorded to the nearest 0.01 foot. The
electronic water level indicator probe and exposed probe cable is decontaminated between measurement
locations.
Generalized Standard Operating Procedures (Not All Inclusive)
WithersRavenel
Our People. Your Success.
Free Product Level Measurements
Light Non-Aqueous Phase Liquid (LNAPL) or “free product” present on the water table is measured using
an electronic oil/water interface probe. The interface probe has both an audible and illuminating light
that indicate when a liquid level is encountered. The oil/water interface probe registers a solid tone and
solidly lit light when LNAPL petroleum product is encountered and a beeping tone flashing light when
groundwater is encountered. Depth to LNAPL measurements are obtained by lowering the probe
attached to a cable marked in 0.01 foot intervals into the well until the probe of the meter intersects the
product or groundwater. The measurements from the top of the riser pipe or TOC to the liquid level are
recorded to the nearest 0.01 foot. The thickness of LNAPL is calculated by subtracting the depth to
LNAPL measurement from the depth to groundwater measurement. The electronic interface probe is
decontaminated between measurement locations.
Soil Sampling and Field Screening
Soil sampling is performed in general accordance with ASTM: 1586-84 where applicable. Sampling
procedures are followed to protect the chemical integrity of the soil samples and minimize the potential
for cross contamination between sample locations, including discarding of the exterior of the sample
which contacts the auger bucket, acetate sleeve, or split barrel sampler, the use of stainless steel sampling
equipment, and the thorough decontamination of sampling apparatus prior to use and between sample
locations.
Soil samples retained as a part of excavation or other intrusive “digging” activities may be collected from
the bucket of excavation equipment or using a hand shovel, if appropriate. Care to collect soil samples
from excavation equipment includes retrieving native soil from material that has not made contact with
the excavating equipment. Samples are collected in sealable bags or by directly filling sample containers
as described above.
Sampling is performed using new, disposable nitrile gloves for each sample location to ensure sample
integrity and minimize the potential for cross contamination or field personnel exposure to contaminants.
Sampling equipment such as hand auger extensions and buckets, direct push samplers, split spoons or
shovels, are decontaminated prior to their use in the collection of samples.
Samples are placed within laboratory grade sample containers provided by the laboratory to which the
samples are submitted, labeled, sealed, and placed in an ice filled cooler. An aliquot of the sample is
typically placed in a clean sealable bag and allowed to reach ambient air temperature for future screening
of volatile vapor content with a photoionization detector (PID), flame-ionization detector (FID) or other
portable screening device.
Screening of samples with a PID, FID or other field screening device is performed in accordance with
device manufacturer specifications for screening, following calibration of the instrument based on
manufacturer recommended procedures.
Generalized Standard Operating Procedures (Not All Inclusive)
WithersRavenel
Our People. Your Success.
Groundwater Sampling
Groundwater samples are generally collected using one of three standard methods – through the use of a
dedicated, disposable bailer, a peristaltic pump or submersible electric pump.
When sampling with a bailer, a minimum of three well volumes of groundwater are extracted from the
well as a means of purging, unless the well is purged to a “dry” state prior to the removal of three volumes
of water. Prior to collection of the groundwater sample with the bailer, the water level is allowed to
recover to within 80% of the original level measured prior to purging.
When sampling with a peristaltic or submersible electric pump, polyethylene (PE) tubing (or equivalent) is
emplaced into the screened section of the monitoring well, and the pump is used to extract water through
the tubing. When using the either of these methods, general water quality measurements including but
not limited to pH, temperature, dissolved oxygen (DO), oxygen reductive potential (ORP), specific
conductivity and turbidity may be used as methods for determining when an adequate purge of the well
has been conducted. When water quality parameters are measured, the resulting data are included in
well purge forms or field notes specific to each site and sampling point.
Following the purging of three well volumes of groundwater (in the case of the bailed well) or stability of
monitored measurements (in the case of the peristaltic or submersible electric pump), the groundwater
sample(s) are introduced directly into sample containers provided by the laboratory to which samples are
ultimately submitted for analysis. Any samples requiring chemical preservation are contained in pre-
preserved container(s) provided by the laboratory.
Sampling is performed using new, disposable nitrile gloves for each sample location to ensure sample
integrity and minimize the potential for cross contamination of samples or field personnel exposure to
contaminants.
Water Supply Well Sampling
Sampling of water supply wells is accomplished through the collection of a representative sample from an
in-line water tap or other point accessible for sampling. Where possible, the sample is collected from a
point prior to any filtration or point of entry (POE) system which might be installed on a well. In some
cases, samples will be collected from both pre and post-POE locations. Prior to the collection of samples
through an in-place sampling point, the tap or sampling port is cleaned with an Alconox® and deionized
water solution, rinsed with deionized water, and again with an isopropyl alcohol (IPA) rinse.
In the case of active supply wells (e.g., a well with a useable well pump with an active power supply), the
well pump is energized and allowed to run for a minimum of ten (10) minutes time, after which a sample is
contained in laboratory grade sample containers as described in the previous section. Water quality
parameters may be (but are not necessarily) measured in association with the well purging.
Supply wells without active power supplies are not generally sampled, as the well seal cannot be
compromised by individuals not certified as a well contractor. However, in the case of a well with no
power supply or pump installed, samples could be obtained through the use of a bailer, peristaltic pump or
electric submersible pump.
Generalized Standard Operating Procedures (Not All Inclusive)
WithersRavenel
Our People. Your Success.
Decontamination Procedures
Decontamination procedures employed in the performance of field activities will vary dependent upon
the method(s) of sampling performed at any site, but will generally include the following:
• Remove excess soil/sludge from any sampling equipment as needed,
• Wash and scrub the equipment with a phosphate-free detergent such as Alconox® or Liquinox® in a
contaminant-free tap water solution. Use a brush to remove particulate matter and surface films as
necessary,
• Rinse thoroughly with tap water,
• Rinse thoroughly with analyte-free water (deionized water),
Rinse thoroughly with isopropyl alcohol,
• Allow the equipment to air dry,
• Prevent inadvertent contamination during storage and transport (accomplished through storage of
equipment in foil or plastic bags/sheeting).
In the case of disposable bailers and tubing utilized for the purging and sampling of wells, these items may
be decontaminated prior to their disposal. In general, no decontamination of these items is necessary
prior to their use in sampling.