RA-1601_12604_CA_MRP_20191217

Groundwater Monitoring Report
Stovall Country Store, Incident No. TF-12604
6195 Highway 96
Oxford, Granville County NC
S&ME Project No. 4305-18-013A
PREPARED FOR:
NCDEQ, DWM, UST Section
1646 Mail Service Center
Raleigh, NC 27699-1646
PREPARED BY:
S&ME, Inc.
3201 Spring Forest Road
Raleigh, NC 27616
December 18, 2019

S&ME, Inc. | 3201 Spring Forest Road | Raleigh, NC 27616 | p 919.872.2660 | www.smeinc.com

December 18, 2019
NCDEQ, DWM, UST Section
1646 Mail Service Center
Raleigh, NC 27699-1646
Attention: Mr. Mark Petermann, L.G. via email: [e-mail]
Reference: Groundwater Monitoring Report
Stovall’s Grocery, Incident #12604, UST No. RA-1601
6195 Highway 96
Oxford, Granville Count, North Carolina
S&ME Project No. 4305-18-013
Dear Mr. Petermann:
S&ME, Inc., (S&ME) presents this report in accordance with the North Carolina Department of Environmental
Quality/S&ME Contract No. N17002 and S&ME Proposal No. 43-1700741-A, dated October 23, 2019, as
authorized by Task Authorization No. 02, dated October 25, 2019.
If you have any questions or comments regarding this report, please contact us at your convenience.
Sincerely,
S&ME, Inc.
Jim Peele Thomas P. Raymond, P.E., P.M.P.
Staff Environmental Professional Senior Engineer
[e-mail] [e-mail]

cc: Michael Pfeifer - Senior Project Manager – S&ME, Inc.

Attachments: Groundwater Monitoring Report

Groundwater Monitoring Report
Stovall’s Grocery, Incident #12604, UST No. RA-1601
6195 Highway 96
Oxford, Granville Count, North Carolina
S&ME Project No. 4305-18-013
December 18, 2019 ii
Table of Contents
1.0 Site Information ................................................................................................................ 1
1.1 Site Identification ............................................................................................................................ 1
1.2 Information about Contacts Associated with the Leaking UST System ................................. 1
1.3 Information about Release ............................................................................................................ 1
1.4 Information about the Monitoring Report .................................................................................. 1
1.5 Certification ..................................................................................................................................... 2
2.0 Executive Summary .......................................................................................................... 3
3.0 Scope of Services ............................................................................................................... 4
3.1 Contract Information ..................................................................................................................... 4
3.2 Approved Scope of Services ......................................................................................................... 4
4.0 Site History and Characterization ................................................................................. 4
4.1 UST Owner and Operator Information ....................................................................................... 4
4.2 UST Information ............................................................................................................................. 4
4.3 Description of the UST Release .................................................................................................... 4
4.4 Site Characteristics ......................................................................................................................... 5
4.5 Owners and Occupants of Adjoining/Nearby Properties and Land Use ............................... 5
4.6 Receptors/Potential Receptor Information .................................................................................. 5
5.0 Current Site Assessment Information .......................................................................... 5
5.1 Current Liquid Levels .................................................................................................................... 5
5.2 Groundwater Monitoring Event .................................................................................................. 6
5.3 Summary of Groundwater Information ...................................................................................... 6
5.4 Regional and Site Geology and Hydrogeology .......................................................................... 6
5.4.1 Soil and Bedrock ................................................................................................................................ 6
5.4.2 Hydrogeology .................................................................................................................................... 7
5.5 Evaluation of Soil, Groundwater, Surface Water, and Free Product Assessment Information .............. 7
5.5.1 Current Extent and Severity of Contamination ............................................................................... 7
5.5.2 Cleanup Levels Achieved ................................................................................................................... 8
6.0 Conclusion and Recommendations ............................................................................... 8

Groundwater Monitoring Report
Stovall’s Grocery, Incident #12604, UST No. RA-1601
6195 Highway 96
Oxford, Granville Count, North Carolina
S&ME Project No. 4305-18-013
December 18, 2019 iii
List of Figures
1. Vicinity Map
2. Site Map
3. Groundwater Elevation Map
4. Groundwater Constituent Map
5. Water Supply Well Constituent Map
List of Tables
1. UST Owner/Operator Information
2. UST Information
3. Monitor Well Construction Data and Groundwater Elevations
4. Summary of Historical and Current Groundwater Analytical Results
5. Summary of Historical and Current Water Supply Analytical Results
Appendices
Appendix I – Figures
Appendix II – Tables
Appendix III – Site Photographs
Appendix IV – Field Data Sheets
Appendix V - Laboratory Analytical Report and Chain of Custody Form

Groundwater Monitoring Report
Stovall’s Grocery, Incident #12604, UST No. RA-1601
6195 Highway 96
Oxford, Granville Count, North Carolina
S&ME Project No. 4305-18-013
December 18, 2019 1
1.0 Site Information
1.1 Site Identification
Date of Report: December 18, 2019
Facility I.D. 00-0-000016801 UST Incident No.: 12604 UST No.: RA-1601
Site Risk: _High Site Rank: H0930D Land Use Category: Commercial
Site Name: Stovall’s Country Store
Site Address: _6195 Highway 96
City/Town: Zip Code: 27565 County: Granville
Description of Geographical Data (e.g., diesel fill port): Former UST pit
Location Method (GPS, Topographical map, other): Google Earth
Latitude (decimal degrees): 36.353461° Longitude (decimal degrees): -78.630580°
1.2 Information about Contacts Associated with the Leaking UST System
Former UST Owner: Michael Stovall (Deceased)
UST Operator: Michael Stovall (Deceased)
Property Occupant: Stovall Country Store (Aiman Botros – owner)_
Consultant/Contractor: S&ME, Inc.
Address: 3201 Spring Forest Road, Raleigh, NC Telephone: [phone]
Analytical Laboratory: Con-Test Analytical Laboratory State Certification No.: 652
Address: 39 Spruce Street, East Longmeadow, MA 01028 Telephone: [phone]
1.3 Information about Release
Date Discovered: 2/8/1994_
Estimated Quantity of Release: Unknown
Cause of Release: Spills/Leaks: Leak in UST System
Source of Release (Dispenser/Piping/UST): UST System
Sizes and contents of UST system(s) from which the release occurred: Two 8,000-gallon gasoline, one 4,000-gallon gasoline,
one 1,000-gallon diesel.
Criteria Used to Classify Risk: Free product, GCL exceedances in several monitor wells, on-site water supply well is impacted.
1.4 Information about the Monitoring Report
Date of Groundwater Monitoring: November 6-7, 2019

Groundwater Monitoring Report
Stovall’s Grocery, Incident #12604, UST No. RA-1601
6195 Highway 96
Oxford, Granville Count, North Carolina
S&ME Project No. 4305-18-013
December 18, 2019 2
1.5 Certification
I, Thomas P. Raymond, a Professional Engineer for S&ME, do certify that the information contained in this report is correct and
accurate to the best of my knowledge. S&ME is licensed to practice geology/engineering in North Carolina. Geology License
Certification #C-145 and Engineering License Certification #F-0176.

________________________________________
Thomas P. Raymond, P.E., P.M.P.
Groundwater Monitoring Report
Stovall’s Grocery, Incident #12604, UST No. RA-1601
6195 Highway 96
Oxford, Granville Count, North Carolina
S&ME Project No. 4305-18-013
December 18, 2019 3
2.0 Executive Summary
On November 6 and 7, 2019, S&ME conducted groundwater and water supply well sampling at the Stovall
Country Store in Oxford, Granville County, North Carolina. A Vicinity Map is included as Figure 1 in Appendix I.
The laboratory analytical results indicated that the following constituents were the highest reported
concentrations above the 15A NCAC 2L.0202 Groundwater Standards (2L Standards) in groundwater samples
collected during the November 2019 sampling event:

Contaminant 2L Standard (µg/L) Concentration
(µg/L) Well ID Date
Tert-amyl methyl ether 128 670 DCW-2 11/6/2019
Benzene 1 10,000* MW-14 11/7/2019
Tert-butyl alcohol 10 13,000* DCW-2 11/6/2019
Toluene 600 32,000 MW-14 11/7/2019
Ethylbenzene 600 3,500 MW-21 11/7/2019
Total Xylenes 500 16,300 MW-21 11/7/2019
Methyl tert-butyl ether 20 8,200 DCW-2 11/6/2019
Di-isopropyl ether 70 1,000 DCW-2 11/6/2019
Naphthalene 6 1,900 MW-20, MW-21 11/7/2019
1,2,4-Trimethylbenzene 400 2,400 MW-5 11/7/2019
1,3,5-Trimethylbenzene 400 680 MW-5 11/7/2019
Isopropylbenzene 70 100 MW-21 11/7/2019
Tetrachloroethylene 0.7 2.2 MW-28 11/7/2019
Styrene 70 190 MW-20 11/7/2019
*Exceeds Gross Contaminant Level (GCL)

• Conducting a receptor survey was outside of the scope for this assessment. However, based on previous
information:
 There are 18 active potable water supply wells located within 1,000 feet of the source area and six of
these wells are located within 500 feet of the site.
 A municipal water source is not currently available to the site and surrounding properties.
 The closest surface water body is a farm pond and an unnamed tributary to Jordan Creek,
approximately 600 feet to the east of the site.
 Analytical results of the WSW-1 influent and effluent samples indicated that several VOCs were
detected in the influent sample to the system at concentrations exceeding their respective 2L
Standards. No targeted constituents were detected above their respective laboratory method
detection limits in the effluent sample from the system.

Groundwater Monitoring Report
Stovall’s Grocery, Incident #12604, UST No. RA-1601
6195 Highway 96
Oxford, Granville Count, North Carolina
S&ME Project No. 4305-18-013
December 18, 2019 4
To achieve incident closure, the following options are presented:
1. Connect water supply wells located within 1,000 feet of the site to a municipal water source and abandon
the water supply wells (municipal water is not available to the site and surrounding properties).
2. Reduce the level of constituents detected at the site to less than GCLs and impose use restrictions.
3.0 Scope of Services
3.1 Contract Information
The scope of services for this report was performed in general accordance with S&ME’s proposal number 43-
1700741-A dated October 23, 2019. The scope of services was authorized by the North Carolina Department of
Environmental Quality (NCDEQ’s) Task Authorization 02, dated October 25, 2019, and within contract number
N17002.
3.2 Approved Scope of Services
S&ME’s approved Scope of Services for this Task Authorization included: gauging and collecting groundwater
samples from up to 24 monitor wells, collecting an influent and effluent sample from the on-site water supply well
(WSW-1), and preparing this report. The scope of services was completed as proposed.
4.0 Site History and Characterization
4.1 UST Owner and Operator Information

According to an Underground Storage Tank Closure Report dated March 29, 1994 by EA, the UST system was
owned by the former site owner, Mr. Michael Stovall (deceased). The owner/operator information is provided in
Table 1.

4.2 UST Information

Two 8,000-gallon gasoline USTs, one 4,000-gallon diesel UST, and one 1,000-gallon diesel UST formerly operated
at the site. Figure 1 presents the Vicinity Map. Information about the USTs are provided in Table 2, and the
location of the former UST is shown in Figure 2.
4.3 Description of the UST Release
The USTs and approximately 116 cubic yards of contaminated soils were removed from the site on February 8 and
9, 1994. On August 15, 1994 an additional 17 cubic yards of contaminated soils were excavated, removed from
the site and transported to Mr. Stovall’s farm for disposal.

Groundwater Monitoring Report
Stovall’s Grocery, Incident #12604, UST No. RA-1601
6195 Highway 96
Oxford, Granville Count, North Carolina
S&ME Project No. 4305-18-013
December 18, 2019 5
4.4 Site Characteristics

 The site is currently occupied by the Stovall Country Store, a single-story block building that is
currently used as a convenience store and grill with retail petroleum sales. Three aboveground
storage tanks (ASTs) supply gasoline and diesel fuel to the dispensing pumps. A map of the site is
provided in Figure 2. Photographs of the site are presented in Appendix III.

 The land use in the area surrounding the Stovall Country Store site is primarily rural residential and
agricultural.

 The site slopes slightly to the east and southeast, with approximately two feet of relief across the site.

 The site consists of asphalt and concrete-paved driveways and parking areas with some gravel areas
and grassy areas behind and to the south of the Stovall Country Store building.

 The nearest identified surface water body is a farm pond and an unnamed tributary to Jordan Creek,
located approximately 600 feet to the east of the source area at the site.
4.5 Owners and Occupants of Adjoining/Nearby Properties and Land Use
The area surrounding the site is primarily rural residential and agricultural. Undeveloped wooded land is present
to the east of the site. Residential properties are located to southeast, southwest and west of the site.
4.6 Receptors/Potential Receptor Information
Water supply well WSW-1 is located at the site and supplies the property with potable water. A POE system
maintained by the site owner has been installed on WSW-1. Conducting a receptor survey was outside of the
scope for this assessment. However, based on previous information:
 There are 18 active potable water supply wells located within 1,000 feet of the source area and six of
these wells are located within 500 feet of the site.
 A municipal water source is not currently available to the site and surrounding properties.
 The closest surface water body is a farm pond and an unnamed tributary to Jordan Creek,
approximately 600 feet to the east of the site.
5.0 Current Site Assessment Information
5.1 Current Liquid Levels
On November 6 and 7, 2019, S&ME personnel measured depth to groundwater in 24 monitoring wells (MW-1,
MW-2, MW-3, MW-5, MW-6, MW-7, MW-9, MW-12, MW-14 through MW-22, MW-24, MW-25, MW-28, DCW-2
through DCW-4, and DCW-7). The depth to groundwater was measured using an electronic water level indicator,
which emits an audible tone when in contact with water. The depth to groundwater measurements at the site
ranged from 19.26 feet below top of casing (ft-btoc) in monitoring well MW-20 to 23.95 ft-btoc in monitoring well
MW-12. Free product was not detected in any of the monitor wells sampled. The depth to water measurements
and monitoring well construction data are provided in Table 3 in Appendix II. Figure 3 in Appendix I presents
the Groundwater Elevation Map.
Groundwater Monitoring Report
Stovall’s Grocery, Incident #12604, UST No. RA-1601
6195 Highway 96
Oxford, Granville Count, North Carolina
S&ME Project No. 4305-18-013
December 18, 2019 6
5.2 Groundwater Monitoring Event
Prior to sampling, monitor wells were purged a minimum of three well casing volumes (or until the well was bailed
dry), and the field parameters temperature, pH, and conductivity were recorded for each casing volume. Copies of
the well sampling forms are provided in Appendix IV. The groundwater samples were placed in laboratory-supplied
containers, placed in a cooler on ice, and shipped under standard chain-of-custody procedure to Con-Test Labs
(Con-Test) of East Longmeadow, Massachusetts, a North Carolina certified laboratory, for analysis of VOCs by EPA
Method 6200B + 10 oxygenates.

In addition to collecting the groundwater samples, S&ME collected a sample from the influent and effluent of the
on-site water supply well (WSW-1). The water supply well was purged for approximately 15 minutes prior to
sampling. The groundwater sample was collected directly into laboratory-supplied containers, stored in a cooler
with ice, and shipped under standard chain-of-custody procedures to Con-Test for laboratory analysis. The water
supply well samples were analyzed for VOCs by EPA Method 6200B + 10 oxygenates. Copies of the sampling sheets
are provided in Appendix IV.

5.3 Summary of Groundwater Information
The laboratory analytical results of the groundwater samples collected on November 6 and 7, 2019 indicated that
several VOCs were detected in concentrations exceeding their respective 2L Standards in multiple monitor wells.
Benzene was detected in a concentration exceeding the gross contamination level (GCL) in monitor wells DCW-3
and MW-14. Tert-butyl alcohol was detected at a concentration exceeding the GCL in DCW-2. A summary of the
groundwater analytical results is presented in Table 4 and shown in Figure 4, and a copy of the laboratory
analytical report is provided in Appendix V.

The laboratory analytical results of the water samples collected from water supply well WSW-1 (influent and
effluent) indicated that benzene, di-isopropyl ether, and methyl tert-butyl ether were detected at concentrations
exceeding their respective 2L Standards in the influent sample to the system. Multiple other targeted constituents
were detected in the influent sample to the system at concentrations above the laboratory minimum detection
limits, but below their respective 2L Standards. No targeted constituents were detected above their respective
laboratory method detection limits in the effluent sample from the system. The current and historical analytical
results for the water samples collected from the water supply wells is presented in Table 5 and presented on
Figure 5. A copy of the laboratory analytical report and chain-of-custody record are provided in Appendix V.
5.4 Regional and Site Geology and Hydrogeology
5.4.1 Soil and Bedrock
According to the US Department of Agriculture Web Soil Survey, soils at the site consist of the Georgeville Silt
Loam, a well-drained soil with slopes of 2% to 6%. According to the boring log for monitor well MW-1, the soils
encountered at the site consisted of red clay and saprolite to a depth of 42 feet below ground surface. The site
lies within the Carolina Slate Belt, in the Piedmont physiographic province. The area is underlain by late
Proterozoic to Cambrian age metamorphosed granitic rocks. Depth to bedrock is reportedly highly variable
across the area.
Groundwater Monitoring Report
Stovall’s Grocery, Incident #12604, UST No. RA-1601
6195 Highway 96
Oxford, Granville Count, North Carolina
S&ME Project No. 4305-18-013
December 18, 2019 7
5.4.2 Hydrogeology
S&ME calculated the groundwater elevations for the monitor wells gauged using the depth-to-water
measurements and the top of casing elevations. Depth to groundwater from top of casing elevations at the site
ranged from 19.26 feet below the top of casing (ft-btoc) in MW-20 to 23.95 ft-btoc in MW-12. The groundwater
elevations were used to prepare a groundwater elevation map (Figure 3), which indicates that groundwater may
generally flow to the east and southeast, however, groundwater may periodically flow radially.
5.5 Evaluation of Soil, Groundwater, Surface Water, and Free Product Assessment
Information
5.5.1 Current Extent and Severity of Contamination
Based upon the laboratory analytical results of the groundwater samples collected on November 6 and 7, 2019,
concentrations of several dissolved phase constituents remain above the 2L Standards in multiple shallow and
deep monitor wells. Benzene was reported in concentrations exceeding the GCL in the groundwater samples
collected from DCW-3 and MW-14. Tert-butyl alcohol was detected at a concentration above the GCL in the
groundwater sample collected from DCW-2. Multiple other targeted constituents were detected at concentrations
above their respective laboratory minimum detection limits, but below the 2L Standards.

Compared to prior sampling events, concentrations of targeted contaminant constituents have generally
decreased in the most contaminated monitoring wells (MW-5, and MW-14 through MW-20), although several
constituents are still reported exceeding their respective 2L Standards and some GCLs in these monitor wells. Free
product was not measured in any monitor wells sampled. Compared to historical water quality (dating back to
January 2013), contaminant concentrations have generally increased in two of the deep groundwater monitor
wells that were sampled (DCW-2 and DCW-3). Two deep groundwater monitor wells (DCW-4 and DCW-7) have
shown a generally decreasing trend in targeted constituent concentrations over this time period.

The groundwater flows generally to the south and southeast across the site, with the most contaminated wells
(both shallow and deep) being located on the southern portion of the site between the fuel dispensing pumps
and the former UST pit on the south side of the structure. Previous reports for the site do not indicate if the
dispensing pumps or product supply lines were removed at the time of UST closure. The dispensing pumps that
are currently operating at the site (supplied by fuel from ASTs) do not appear to be updated. It is likely that there
was release from either the fuel dispensing pumps and/or product dispensing lines associated with the former
UST system. Previous soil sampling conducted in 2006 indicate soil contamination present in the area between
the dispensing pumps and the former UST area.

Deep monitor well DCW-6 (located near WSW-1 and up-gradient from the release area) was not sampled during
this monitoring event, however, historically, there have not been detections of targeted contaminant constituents
in concentrations exceeding 2L Standards. Although water supply well WSW-1 is also located upgradient of the
release area, it is possible that pumping action in this well is drawing contaminants into the well. Concentrations
of several constituents have been historically reported in the influent and effluent of the well. During the
November 2019 sampling event, benzene, di-isopropyl ether, and methyl tert-butyl ether were detected in the
influent sample at concentrations above their respective 2L Standards. Multiple other targeted constituents were
detected at concentrations above their laboratory method detection limit, but below their respective 2L Standards.
Groundwater Monitoring Report
Stovall’s Grocery, Incident #12604, UST No. RA-1601
6195 Highway 96
Oxford, Granville Count, North Carolina
S&ME Project No. 4305-18-013
December 18, 2019 8
No targeted constituents were detected above their laboratory minimum detection limits in the effluent sample
collected from WSW-1.
5.5.2 Cleanup Levels Achieved
 Soil (soil-to-groundwater maximum soil contaminant concentrations) Unknown
 Groundwater (2L standard concentrations) No
 Free Product No
6.0 Conclusion and Recommendations
Based on the current and historical assessment information for the site, the following conclusions are presented:

1. Free product was not detected in monitor wells sampled during the November 2019 sampling event.
2. Petroleum hydrocarbons are present in concentrations exceeding their respective 2L Standards in several
of the monitor wells. Benzene was also detected above its GCL in the sample collected from DCW-3 and
MW-14. Tert-butyl alcohol was detected above the GCL in the sample collected from DCW-2.
3. Based on previous information there are 18 active potable water supply wells located within 1,000 feet of
the source area and six of these wells are located within 500 feet of the site. A municipal water source is
not currently available to the site and surrounding properties. The closest surface water body is a farm
pond and an unnamed tributary to Jordan Creek, approximately 600 feet to the east of the site.
4. Samples collected from WSW-1 (influent and effluent) indicated that several VOCs were detected in the
influent sample to the system. No targeted constituents were detected above their respective laboratory
method detection limits in the sample collected from the effluent side of the system.

Based on the above, the following recommendations are presented:
1. Maintain the current POE system that is installed on the onsite water supply well (WSW-1).
2. Evaluate the potential feasibility with costs to connect water supply wells located within 1,000 feet of the
site to a municipal water source and abandon the water supply wells (municipal water is not available to
the site and surrounding properties).
3. Conduct a soil investigation around the former UST area, former product lines, current product lines, and
current AST area to determine the extent of soil contamination in those areas.
4. Evaluate remediation methods to reduce the level of constituents detected at the site to less than the risk-
based levels.

Appendices
Appendix I – Figures
SITE
Site Parcel
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
11 " = 2,000 '
12-10-19
4305-18-013A
STOVALS COUNTRY STORE TF-126046192 HIGHWAY 96OXFORD, GRANVILLE COUNTY, NORTH CAROLINADrawing Path: Q:\4305\18\013 Stovals\4305-18-013 Stovalls Country Store TF-12604\01_VICINITY.mxd plotted by DHomans 12-10-20190 2,000 4,000(FEET)
VICINITY MAP
³
REFERENCE:GIS BASE LAYERS WERE OBTAINED FROM THE USGS NATIONAL TOPO MAP VIEWER. THISMAP IS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONS DISPLAYED AREAPPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEY INFORMATION, UNLESS STATEDOTHERWISE.
!>
!A$
!A$
!A$
!A$
!A$!A$
!A$!A$
!A$
!A$
!A$
!A$!A$
!A$
!A$
!A$
!A$
!A$
!A$
!A$
!A$
!A$
!A$
!A$
!A$
!A$!A$
!AB
!AB
!AB
!AB
!AB
!AB
!A$
!AB
NC HIGHW AY 86CORNWALL ROAD
PUMP ISLAND
KEROSENE AST & PUMP
FORMER UST LOCATION
Above Ground Storage Tank Location
WSW-1
MW-23
MW-13
MW-3
MW-22
MW-8MW-12
MW-11MW-1
MW-20
MW-19
MW-4
MW-15MW-21
MW-16
MW-14
MW-7
MW-6
MW-28
MW-10
MW-25
MW-24
MW-27
MW-9
MW-26 (NL)
MW-2
MW-18MW-5
DCW-6
DCW-4
DCW-2
DCW-7
DCW-1
DCW-3
MW-17
DCW-5
!A$Monitoring Well
!AB Deep Monitoring Well
!>Approx. Water Supply Well Location
Above Ground Storage Tank Location
Former UST Location
Site Parcel
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.2
1 " = 30 '
12-10-19
4305-18-013ASTOVALS COUNTRY STORE TF-126046192 HIGHWAY 96OXFORD, GRANVILLE COUNTY, NORTH CAROLINADrawing Path: Q:\4305\18\013 Stovals\4305-18-013 Stovalls Country Store TF-12604\02_SITE.mxd plotted by DHomans 12-10-20190 30 60
(FEET)SITE MAP³REFERENCE:GIS BASE LAYERS WERE OBTAINED FROM THE 2017 NCONEMAP AERIAL ORTHOIMAGERYLAYER. THIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONSDISPLAYED ARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEY INFORMATION,UNLESS STATED OTHERWISE.
!>
!A$
!A$
!A$
!A$
!A$!A$
!A$!A$
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!A$
!A$
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!A$
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!A$
!A$
!A$
!A$
!A$!A$
!AB
!AB
!AB
!AB
!AB
!AB
!A$
!AB
NC HIGHW AY 86CORNWALL ROAD
PUMP ISLAND
KEROSENE AST & PUMP
FORMER UST LOCATION
Above Ground Storage Tank Location
WSW-1
MW-23(NM)
MW-13(NM)
MW-3(78.79)
MW-22(78.93)
MW-8(NM)
MW-12(78.81)
MW-11(NM)
MW-1(79.12)
MW-20(80.25)
MW-19(80.16)
MW-4(Destroyed)
MW-15(79.42)MW-21(79.63)
MW-16(Destroyed)
MW-14(79.33)
MW-7(79.13)
MW-6(79.90)
MW-28(80.83)
MW-10(NM)
MW-25(79.62)
MW-24(78.62)
MW-27(NM)
MW-9(81.25)
MW-26 (NL)(NM)
MW-2(77.11)
MW-18(80.69)MW-5(79.23)
DCW-6(NM)
DCW-4(78.87)
DCW-2(78.31)
DCW-7(78.95)
DCW-1(NM)
DCW-3(79.31)
MW-17(78.79)
DCW-5(NM)
81
7 880 79
7980
Groundwater measured November 6&7, 2019.
)16.57(Groundwater Elevation (Feet)
MN Not Measured
!A$Monitoring Well
!AB Deep Monitoring Well (not used for contouring)
Groundwated Flow Direction
Estimated Groundwater Surface Contours (Feet)
!>Approx. Water Supply Well Location
Above Ground Storage Tank Location
Former UST Location
Site Parcel
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.3
1 " = 30 '
12-10-19
4305-18-013ASTOVALS COUNTRY STORE TF-126046192 HIGHWAY 96OXFORD, GRANVILLE COUNTY, NORTH CAROLINADrawing Path: Q:\4305\18\013 Stovals\4305-18-013 Stovalls Country Store TF-12604\03_GW_CONTOURS.mxd plotted by DHomans 12-10-20190 30 60
(FEET)GROUNDWATER ELEVATION MAP³REFERENCE:GIS BASE LAYERS WERE OBTAINED FROM THE 2017 NCONEMAP AERIAL ORTHOIMAGERYLAYER. THIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONSDISPLAYED ARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEY INFORMATION,UNLESS STATED OTHERWISE.
!>
!A$
!A$
!A$
!A$
!A$!A$
!A$!A$
!A$
!A$
!A$
!A$!A$
!A$
!A$
!A$
!A$
!A$
!A$
!A$
!A$
!A$
!A$
!A$
!A$
!A$!A$
!AB
!AB
!AB
!AB
!AB
!AB
!A$
!AB
NC HIGHW AY 86CORNWALL ROAD
DCW-2 (μg/L) Tert-Amyl Methyl Ether= 670Benzene= 2,400Tert-Butyl Alcohol= 13,000Methyl Tert-Butyl Ether= 8,200Di-Isopropyl Ether= 1,000Naphthalene= 880 J
DCW-3 (μg/L) Benzene= 5,900Tert-Butyl Alcohol= 820 JTotal Xylenes= 1,680Methyl Tert-Butyl Ether= 370Di-Isopropyl Ether= 140Naphthalene= 2601,2,4-Trimethylbenzene= 640
DCW-4 (μg/L) Benzene= 2.5 JNaphthalene= 961,2,4-Trimethylbenzene= 930N-Propylbenzene= 94
DCW-7 (μg/L) Benzene= 3.6
MW-1 (μg/L) All < 2L
MW-2 All < 2L
MW-3 All < 2L
MW-5 (μg/L) Benzene= 270Toluene= 12,000Ethylbenzene= 3,000Total Xylenes= 14,800Naphthalene= 1,300 1,2,4-Trimethylbenzene= 2,4001,3,5- Trimethylbenzene= 680Isopropylbenzene= 90 JN-Propylbenzene= 300Styrene= 92 J
MW-6 BDL
MW-7 BDL
MW-9 (μg/L) All < 2L
MW-12 All < 2L
MW-14 Benzene= 10,000Toluene= 32,000Ethylbenzene= 3,000Total Xylenes= 14,300Di-isopropyl ether= 160 J1,2,4-Trimethylbenzene= 1,8001,3,5- Trimethylbenzene= 530Isopropylbenzene= 95 JN-Propylbenzene= 280
MW-15 Benzene= 840Toluene= 29,000Ethylbenzene= 3,000Total Xylenes= 14,5001,2,4-Trimethylbenzene= 1,9001,3,5- Trimethylbenzene= 560Isopropylbenzene= 88 JN-Propylbenzene= 280Styrene= 170
MW-17 (μg/L) Benzene= 61Toluene= 3,500Ethylbenzene= 1,800Total Xylenes= 6,500Naphthalene= 5501,2,4-Trimethylbenzene= 1,000N-Propylbenzene= 140
MW-18 (μg/L) Benzene= 420Toluene= 2,200Ethylbenzene= 2,500Total Xylenes= 3,090Naphthalene= 6901,2,4-Trimethylbenzene= 1,8001,3,5-Trimethylbenzene= 530Isopropylbenzene= 76N-Propylbenzene= 250
MW-19 (μg/L) Toluene= 6,300Ethylbenzene= 2,500Total Xylenes= 8,000Naphthalene= 980 J1,2,4-Trimethylbenzene= 18001,3,5-Trimethylbenzene= 510Isopropylbenzene= 76 JN-Propylbenzene= 260
MW-20 (μg/L) Benzene= 150 JToluene= 23,000Ethylbenzene= 3,300Total Xylenes= 14,200Naphthalene= 1,900 J1,2,4-Trimethylbenzene= 2,3001,3,5-Trimethylbenzene= 650Isopropylbenzene= 92 JN-Propylbenzene= 320Styrene= 190 J
MW-21 (μg/L) Benzene= 3,400Toluene= 28,000Ethylbenzene= 3,500Total Xylenes= 16,300Naphthalene= 1,900 J1,2,4-Trimethylbenzene= 2,3001,3,5-Trimethylbenzene= 670Isopropylbenzene= 100 JN-Propylbenzene= 320Styrene= 160 J
MW-28 (μg/L) Tetrachloroethylene= 2.2
MW-4 Destroyed
MW-8 NS
MW-10 NS
MW-11 NS
MW-16 Destroyed MW-13 NS
MW-22 Benzene= 130Ethylbenzene= 790Total Xylenes= 780Naphthalene= 3401,2,4-Trimethylbenzene= 1,4001,3,5-Trimethylbenzene= 460Isopropylbenzene= 74N-Propylbenzene= 270
MW-23 NS
MW-24 Benzene= 45Total Xylenes= 2,110Naphthalene= 2401,2,4-Trimethylbenzene= 580N-Propylbenzene= 74
MW-25 BDL
MW-26 NSMW-27 NS
DCW-1 NS
DCW-5 NS
DCW-6 NS
WSW-1
!A$Monitoring Well
!AB Deep Monitoring Well
!>Approx. Water Supply Well Location
Above Ground Storage Tank Location
Former UST Location
Site Parcel
Bold indicates concentration exceeds Gross Contamination Levels.
Only Concentrations exceeding 2L Standards are shown.
BDL: Below Detection Limits
NS : Not Sampled
μg/L : Micrograms per Liter
Groundwater sampled November 6 & 7, 2019.
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.4
1 " = 30 '
12-10-19
4305-18-013ASTOVALS COUNTRY STORE TF-126046192 HIGHWAY 96OXFORD, GRANVILLE COUNTY, NORTH CAROLINADrawing Path: Q:\4305\18\013 Stovals\4305-18-013 Stovalls Country Store TF-12604\04_GW_CONSTITUENT.mxd plotted by DHomans 12-10-20190 30 60
(FEET)GROUNDWATER CONSTITUENT MAP³REFERENCE:GIS BASE LAYERS WERE OBTAINED FROM THE 2017 NCONEMAP AERIAL ORTHOIMAGERYLAYER. THIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONSDISPLAYED ARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEY INFORMATION,UNLESS STATED OTHERWISE.
!>NC HIGHW AY 86CORNWALL ROAD
PUMP ISLAND
KEROSENE AST & PUMP
FORMER UST LOCATION
WSW-1 Influent μg/Lbenzene 13* n-butylbenzene 2.8sec-butylbenzene 1.4 Jdi-isopropyl ether 88*isopropylbenzene 3.8methyl tert-butyl ether 460*n-propylbenzene 1.2 Jtert-amyl methyl ether 55tert-butyl alcohol 7001,2,4-trimethylbenzene 6.51,3,5-trimethylbenzene 1.2 Jtotal xylenes 11
WSW-1 Effluent All Below Detection Limits
ABOVE GROUND STORAGE TANK LOCATION
WSW-1
!>Approx. Water Supply Well Location
Above Ground Storage Tank Location
Former UST Location
Site Parcel
County Parcels
* Indicates exceedence of 2L Standardsμg/L: Micrograms per LiterSamples collected November 7, 2019
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
51 " = 50 '
12-13-19
4305-18-013A
STOVALS COUNTRY STORE TF-126046192 HIGHWAY 96OXFORD, GRANVILLE COUNTY, NORTH CAROLINADrawing Path: \\CharNC\CADData\4305\18\013 Stovals\4305-18-013 Stovalls Country Store TF-12604\05_WSW-CONSTITUENT.mxd plotted by mverbanic 12-13-20190 50 100(FEET)
WATER SUPPLY WELL CONSTITUENT MAP ³REFERENCE:GIS BASE LAYERS WERE OBTAINED FROM THE 2017 NCONEMAP AERIAL ORTHOIMAGERYLAYER. THIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONSDISPLAYED ARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEY INFORMATION,UNLESS STATED OTHERWISE.
Appendix II – Tables
TABLE 1
SITE HISTORY - UST/AST SYSTEM INFORMATION
Stovall Country Store (Incident No.: 12604, UST #:RA-1601)
6192 NC Highway 96, Oxford, Granville County, North Carolina
UST
ID Number
Current/Last
Contents
Previous
Contents
Capacity
(gallons)
Construction
Details
Tank
Dimensions
Description of
Associated Piping
and Pumps
Date UST
Installed Status of UST
Was Release
Associated With
UST System?
(Yes/No)
1 None Gasoline 8,000 Steel Not Reported Removed February 1980 Closed - Feb. 1994 Yes
2 None Gasoline 8,000 Steel Not Reported Removed February 1981 Closed - Feb. 1994 Yes
3 None Gasoline 4,000 Steel Not Reported Removed September 1985 Closed - Feb. 1994 Yes
4 None Diesel 1,000 Steel Not Reported Removed September 1985 Closed - Feb. 1994 Yes
Incident
Number
Material
Released
Date of
Release Description of Release
12604 Gasoline Feb. 1994
* : Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non-halogenated or halogenated solvents, etc.
** : Fiberglass (single- or double-walled), steel (single- or double-walled), steel with FRP (single- or double-walled), steel with liner, other, unknown.
*** : Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal (specify date)
Contaminated soils encountered during excavation and removal of four USTs.
S&ME Project # 4305-18-013A
TABLE 2
SITE HISTORY - UST/AST OWNER INFORMATION
Stovall Country Store (Incident No.: 12604, UST #:RA-1601)
6192 NC Highway 96, Oxford, Granville County, North Carolina
S&ME Project # 4305-18-013A
1 Feb. 1981 - Feb. 1994
2 Feb. 1980 - Feb. 1994
3 Sept. 1985 - Feb. 1994
4 Sept. 1985 - Feb. 1994
Address Telephone Number
UST/AST ID
Number(s)
Name of Owner or
Operator
Dates of Ownership /
Operation
Michael Stovall 12604 Both
Incident
Number
Owner or
Operator?
6511 Cornwall Road, Oxford, NC 27565 Not Available
Well ID Date
Installed Well Type Screened
Interval
Total Well
Depth from Top
of Casing
(Ft-BTOC)
Well
Material
Well
Diameter
(inches)
TOC
Elevation
(Ft-Rel)
Date of
Measurement
Depth to
Water
(ft-BTOC)
Groundwater
Elevation
(Ft-Rel)
3/24/2004 9.85 90.15
9/27/2004 15.07 84.93
9/3/2007 21.42 78.58
1/21/2013 25.96 74.04
9/28/2015 20.90 79.10
2/1/2018 23.24 76.76
11/7/2019 20.88 79.12
7/7/1995 13.92 84.09
10/17/1995 NM NA
1/21/2013 NM NA
9/28/2015 21.08 76.93
2/1/2018 23.02 74.99
11/7/2019 20.90 77.11
3/24/2004 10.62 90.02
9/27/2004 16.13 84.51
9/3/2007 21.99 78.65
1/21/2013 27.22 73.42
9/28/2015 21.43 79.21
1/31/2018 24.72 75.92
11/7/2019 21.85 78.79
3/24/2004 14.35 86.52
9/27/2004 19.48 81.39
1/21/2013 26.88 73.99
Free Product 0.80 9/28/2015*20.80 80.13
Free Product 0.10 2/1/2018*24.72 76.24
11/7/2019
3/24/2004 10.59 89.53
9/27/2004 15.90 84.22
9/3/2007 21.14 78.98
1/21/2013 DRY DRY
9/28/2015 20.85 79.27
1/31/2018 24.21 75.9111/7/2019 20.89 79.23
3/24/2004 11.61 90.73
9/27/2004 17.46 84.88
9/3/2007 22.48 79.86
1/21/2013 DRY DRY
9/28/2015 22.47 79.87
2/1/2018 26.50 75.84
11/7/2019 22.44 79.90
3/24/2004 12.84 DRY
9/27/2004 18.60 84.34
9/3/2007 23.90 79.04
1/21/2013 29.63 73.31
9/28/2015 23.70 79.24
1/31/2018 27.42 75.52
11/7/2019 23.81 79.13
3/24/2004 12.65 89.83
9/27/2004 18.37 84.11
9/3/2007 23.98 78.50
1/21/2013 29.55 72.93
9/28/2015 23.69 78.79
1/31/2018 NM NM
11/7/2019 NM NM
9/27/2004 16.05 84.49
9/3/2007 19.30 81.24
1/21/2013 19.30 81.24
9/28/2015 15.65 84.89
2/1/2018 18.82 81.72
11/7/2019 19.29 81.25
9/27/2004 17.57 84.68
9/3/2007 19.32 82.93
1/21/2013 19.50 82.75
9/28/2015 19.27 82.98
2/1/2018 NM NM
11/7/2019 NM NM
9/27/2004 14.52 85.20
9/3/2007 21.01 78.71
1/21/2013 DRY DRY
9/28/2015 20.44 79.28
2/1/2018 NM NM
11/7/2019 NM NM
9/27/2004 18.56 84.20
9/3/2007 24.05 78.71
1/21/2013 24.21 78.55
9/28/2015 23.73 79.03
1/31/2018 24.20 78.56
11/7/2019 23.95 78.81
9/27/2004 16.83 84.12
9/3/2007 22.29 78.66
1/21/2013 DRY DRY
9/28/2015 NM NM
1/31/2018 NM NM
11/7/2019 NM NM
9/27/2004 16.77 84.48
9/3/2007 22.00 79.25
1/21/2013 DRY DRY
9/28/2015 21.74 79.51
1/31/2018 DRY DRY
11/7/2019 21.92 79.33
9/27/2004 16.51 84.74
9/3/2007 21.93 79.32
1/21/2013 DRY DRY
9/28/2015 21.66 79.59
1/31/2018 DRY DRY
11/7/2019 21.83 79.42
9/27/2004 14.52 85.20
9/3/2007 21.01 78.71
1/21/2013 DRY DRY
9/28/2015 20.75 78.97
1/31/2018 DRY DRY
11/7/2019
9/27/2004 14.52 85.20
9/3/2007 21.01 78.71
1/21/2013 DRY DRY
9/28/2015 20.90 78.82
1/31/2018 23.11 76.61
11/7/2019 20.93 78.79
NOTES:
Benchmark established at 100.00 feet rel. at monitor well MW-1
ft-BTOC: feet below top of casing
ft-bgs: feet below ground surface
ft-rel: feet relative
*If Free Product is present in a well, groundwater elevation is calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581]
6192 NC Highway 96, Oxford, Granville County North Carolina
Stovall Country Store (Incident No. 12604, UST No. RA-1601)
WELL CONSTRUCTION AND LIQUID LEVEL DATA
TABLE 3 - PAGE 1
MW-13 7/13/2004 Type II 5.0 - 25.0 25.00 PVC 2.00 100.95
S&ME Project # 4305-18-013A
2.00 100.54
MW-12 7/13/2004 Type II 5.0 - 25.0 25.00 PVC 2.00 102.76
MW-5 6/15/1995 Type II 15.0 - 30.0 30.00 PVC 2.00 100.12
MW-8 9/25/2015 Type II 15.0 - 30.0 30.00 PVC 2.00 102.48
2.00 102.94
MW-1 10/26/1994 Type II 20.0 - 42.0 42.00 PVC 2.00 100.00
2.00 100.87
MW-2 6/14/1995 Type II 20.0 - 35.0 35.00 PVC 2.00 98.01
MW-4* 6/15/1995 Type II 20.0 - 35.0 35.00 PVC
MW-3 6/14/1995 Type II 20.0 - 35.0 35.00 PVC 2.00 100.64
2.00 99.72
MW-6 9/25/1995 Type II 15.0 - 30.0 30.00 PVC 2.00 102.34
MW-7 9/25/2015 Type II 15.0 - 30.0 30.00 PVC
MW-9 7/13/2004 Type II 5.0 - 20.0 20.00 PVC
MW-17 7/13/2004 Type II 5.0 - 25.0 25.00 PVC 2.00 99.72
MW-14 7/16/2004 Type II 5.0 - 25.0 25.00 PVC 2.00 101.25
MW-15 7/16/2004 Type II 5.0 - 25.0 25.00 PVC 2.00 101.25
Well paved over
Well paved over
MW-16 7/13/2004 Type II 5.0 - 25.0 25.00 PVC 2.00 99.72
MW-10 7/13/2004 Type II 5.0 - 20.0 20.00 PVC 2.00 102.25
MW-11 7/13/2004 Type II 5.0 - 25.0 25.00 PVC
Well ID Date
Installed Well Type Screened
Interval
Total Well
Depth from Top
of Casing
(Ft-BTOC)
Well
Material
Well
Diameter
(inches)
TOC
Elevation
(Ft-Rel)
Date of
Measurement
Depth to
Water
(ft-BTOC)
Groundwater
Elevation
(Ft-Rel)
3/27/2004 15.33 85.75
9/3/2007 20.75 80.33
1/21/2013 DRY DRY
9/28/2015 20.29 80.79
1/31/2018 25.23 75.85
11/7/2019 20.39 80.69
3/27/2004 14.09 85.55
9/3/2007 19.86 79.78
1/21/2013 DRY DRY
9/28/2015 19.28 80.36
1/31/2018 22.70 76.94
11/7/2019 19.48 80.16
3/27/2004 13.99 85.52
9/3/2007 19.82 79.69
1/21/2013 DRY DRY
9/28/2015 19.00 80.51
1/31/2018 22.23 77.28
11/7/2019 19.26 80.25
3/27/2004 15.87 85.03
9/3/2007 21.38 79.52
1/21/2013 24.15 76.75
9/28/2015 21.09 79.81
1/31/2018 24.17 76.73
11/7/2019 21.27 79.63
9/27/2004 16.21 84.35
1/21/2013 DRY DRY
9/28/2015 21.36 79.20
1/31/2018 DRY DRY
11/7/2019 21.63 78.93
3/27/2004 17.93 83.89
9/3/2007 23.34 78.48
1/21/2013 DRY DRY
9/28/2015 22.98 78.84
2/1/2018 NM NM
11/7/2019 NM NM
3/27/2004 16.31 DRY
9/3/2007 22.22 78.42
1/21/2013 DRY DRY
9/28/2015 22.19 78.45
2/1/2018 DRY DRY
11/7/2019 22.02 78.62
3/27/2004 16.27 85.30
9/3/2007 22.00 79.57
1/21/2013 DRY DRY
9/28/2015 21.94 79.63
2/1/2018 DRY DRY
11/7/2019 21.95 79.62
9/3/2007 22.00 79.49
1/21/2013 NM NM
9/28/2015 NM NM
2/1/2018 NM NM
11/7/2019 NM NM
9/3/2007 22.35 79.20
1/21/2013 24.36 77.19
9/28/2015 22.50 79.05
2/1/2018 NM NM
11/7/2019 NM NM
9/3/2007 23.95 80.17
1/21/2013 24.20 79.92
9/28/2015 NM NM
2/1/2018 24.23 79.89
11/7/2019 23.29 80.83
3/24/2004 10.07 90.08
9/27/2004 15.25 84.90
9/3/2007 21.32 78.83
1/21/2013 NM NM
9/28/2015 NM NM
2/1/2018 NM NM
11/7/2019 NM NM
3/24/2004 11.15 89.41
9/27/2004 17.28 83.28
1/21/2013 28.39 72.17
9/28/2015 22.41 78.15
1/31/2018 25.87 74.69
11/6/2019 22.25 78.31
9/27/2004 19.63 81.64
9/3/2007 21.71 79.56
1/21/2013 28.00 73.27
9/28/2015 22.18 79.09
1/31/2018 25.56 75.71
11/6/2019 21.96 79.31
9/27/2004 15.50 84.60
9/3/2007 24.59 75.51
1/21/2013 23.88 76.22
9/28/2015 19.86 80.24
2/1/2018 23.82 76.28
11/6/2019 21.23 78.87
9/3/2007 23.79 79.42
1/21/2013 29.24 73.97
9/28/2015 23.48 79.73
2/1/2018 NM NM
11/7/2019 NM NM
9/3/2007 24.02 76.13
1/21/2013 22.92 77.23
9/28/2015 21.60 78.55
2/1/2018 NM NM
11/7/2019 NM NM
9/3/2007 21.62 80.04
1/21/2013 28.55 73.11
9/28/2015 22.92 78.74
2/1/2018 25.75 75.91
11/6/2019 22.71 78.95
NOTES:
Benchmark established at 100.00 feet rel. at monitor well MW-1
ft-BTOC: feet below top of casing
ft-bgs: feet below ground surface
ft-rel: feet relative
*If Free Product is present in a well, groundwater elevation is calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581]
TABLE 3 - PAGE 2
WELL CONSTRUCTION AND LIQUID LEVEL DATA
Stovall Country Store (Incident No. 12604, UST No. RA-1601)
6192 NC Highway 96, Oxford, Granville County North Carolina
S&ME Project # 4305-18-013A
2.00 101.08
MW-19 7/20/2004 Type II 5.0 - 25.0 25.00 PVC 2.00 99.64
MW-18 7/20/2004 Type II 5.0 - 25.0 25.00 PVC
2.00 99.51
MW-21 7/20/2004 Type II 5.0 - 25.0 25.00 PVC 2.00 100.90
MW-20 7/20/2004 Type II 5.0 - 25.0 25.00 PVC
2.00 100.56
MW-23 9/23/2004 Type II 5.0 - 25.0 25.00 PVC 2.00 101.82
MW-22 9/23/2004 Type II 5.0 - 25.0 25.00 PVC
2.00 100.64
MW-25 9/23/2004 Type II 5.0 - 25.0 25.00 PVC 2.00 101.57
MW-24 9/23/2004 Type II 5.0 - 25.0 25.00 PVC
2.00 101.49
MW-27 6/15/2007 Type II 10.0 - 25.0 25.00 PVC 2.00 101.55
MW-26 6/15/2007 Type II 10.0 - 25.0 25.00 PVC
2.00 104.12
DCW-1 9/22/1995 Type III 41.0 - 50.0 50.00 PVC 2.00 100.15
MW-28 6/15/2007 Type II 10.0 - 25.0 25.00 PVC
2.00 100.56
DCW-3 9/14/2004 Type III 55.0 - 60.0 60.00 PVC 2.00 101.27
DCW-2 9/25/1995 Type III 60.0 - 65.0 65.00 PVC
2.00 100.10
DCW-5 6/15/2005 Type III 53.0 - 58.0 58.00 PVC 2.00 103.21
DCW-4 9/14/2004 Type III 55.0 - 60.0 60.00 PVC
2.00 100.15
DCW-7 6/15/2005 Type III 55.0 - 60.0 60.00 PVC 2.00 101.66
DCW-6 6/15/2005 Type III 53.0 - 58.0 58.00 PVC
TABLE 4 - PAGE 1
SUMMARY OF GROUNDWATER SAMPLING RESULTS
Stovall Country Store (Incident No.: 12604, UST #:RA-1601)
6192 NC Highway 96, Oxford, Granville County, North Carolina
S&ME Project # 4305-18-013A
Well
ID
Date
Collected
1/21/2013 NR BDL NR BDL BDL 0.16 J 0.46 J 10.2 3 BDL BDL 5.8 BDL 11 3 17 2.5 BDL 1.1 0.79 3 BDL BDL BDL BDL BDL
9/29/2015 NR BDL NR BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
2/1/2018 2.2 2.6 11 J 0.16 J BDL BDL BDL 0.87 J 23 BDL 2.4 0.73 J BDL 1.5 0.42 J 0.63 0.39 J BDL 0.37 J BDL 0.54 BDL BDL BDL BDL BDL
11/7/2019 BDL 0.28 J BDL BDL 0.19 J BDL BDL 8.5 1 BDL BDL 5.1 BDL 13 4.3 0.75 0.60 BDL 1.20 BDL 2.7 BDL BDL BDL BDL BDL
1/21/2013
9/28/2015 NR BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
2/1/2018 BDL BDL BDL BDL BDL BDL BDL BDL 2.6 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
11/7/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 5.5 J BDL BDL BDL
1/21/2013 NR 0.14 J NR BDL BDL 0.11 J BDL 2.6 8.1 BDL 4.8 BDL 3.2 0.64 0.87 J BDL BDL 0.14 J BDL 0.25 J BDL 120 18 BDL BDL
9/28/2015
1/31/2018 BDL 0.55 BDL BDL BDL BDL 0.36 J 5.3 3.6 BDL 0.35 J 2.4 J BDL 14 2.2 3.2 1.2 BDL 1.4 1.6 2.9 BDL BDL BDL BDL BDL
11/7/2019 BDL BDL BDL BDL BDL BDL BDL 3.2 BDL BDL BDL BDL BDL 6.1 0.63 0.36 J 0.18 J BDL 0.19 J 0.30 J 0.37 J BDL BDL BDL BDL BDL
1/21/2013
9/28/2015
2/1/2018
11/7/2019
1/21/2013
9/28/2015*NR 607 NR BDL BDL 28,000 3,800 19,040 BDL BDL BDL 1,340 BDL 3,240 786 356 BDL BDL 100 BDL BDL BDL BDL BDL BDL 173
1/31/2018*BDL 1,600 BDL BDL BDL 21,000 3,800 17,700 BDL BDL BDL 1,000 J BDL 3,600 870 72 J BDL BDL 120 J BDL 390 BDL BDL BDL BDL 120 J
11/7/2019*BDL 270 BDL BDL BDL 12,000 3,000 14,800 BDL BDL BDL 1,300 BDL 2,400 680 BDL BDL BDL 90 J BDL 300 BDL BDL BDL BDL 92 J
1/21/2013
9/28/2015 NR BDL NR BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.61 BDL BDL 0.87 BDL 0.92 BDL BDL BDL BDL BDL
2/1/2018 NR BDL NR BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
11/7/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
1/21/2013
9/28/2015 NR BDL NR BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
1/31/2018 NR BDL NR BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
11/7/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
1/21/2013 NR BDL NR BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
9/28/2015
1/31/2018
11/7/2019
1/21/2013
9/28/2015 NR BDL NR BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
2/1/2018 BDL BDL BDL BDL BDL BDL BDL BDL 22 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
11/7/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 7.6 J BDL BDL BDL
1/21/2013
9/28/2015
2/1/2018
11/7/2019
1/21/2013
9/28/2015
2/1/2018
11/7/2019
1/21/2013
9/28/2015
1/31/2018 NR BDL NR BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
11/7/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 3.9 J BDL BDL BDL
1/21/2013
9/28/2015
1/31/2018
11/7/2019
1/21/2013
9/28/2015*NR 8,090 NR BDL BDL 22,300 2,650 12,230 89 BDL 128 651 BDL 2,300 540 BDL BDL BDL 77.4 BDL 268 BDL BDL BDL BDL 21.3
1/31/2018
11/7/2019*BDL 10,000 BDL BDL BDL 32,000 3,000 14,300 BDL BDL 160 J BDL BDL 1,800 530 BDL BDL BDL 95 J BDL 280 BDL BDL 1,700 J BDL BDL
1/21/2013
9/28/2015 NR 2,460 NR BDL BDL 39,400 6,590 31,060 BDL BDL BDL 2,080 BDL 10,000 3,040 538 BDL BDL 377 BDL 1,600 BDL BDL BDL BDL 386
1/31/2018
11/7/2019*BDL 840 BDL BDL BDL 29,000 3,000 14,500 BDL BDL BDL BDL BDL 1,900 560 BDL BDL BDL 88 J BDL 280 BDL BDL BDL BDL 170
1/21/2013
9/28/2015*NR 1,870 NR BDL BDL 5,970 946 4,280 55 BDL 26.5 235 BDL 913 244 BDL BDL BDL 38.3 BDL 135 BDL BDL BDL BDL 52.5
1/31/2018
11/7/2019
1/21/2013
9/28/2015*NA 403 NR BDL BDL 9,050 2,140 10,940 BDL BDL BDL 552 BDL 1,970 554 BDL BDL BDL 58.4 BDL 172 BDL BDL BDL BDL 28.7
1/31/2018*BDL 200 BDL BDL BDL 5,600 630 6,800 BDL BDL BDL 82 J BDL 900 310 BDL BDL BDL BDL BDL 20 J BDL BDL BDL BDL 15 J
11/7/2019*BDL 61 BDL BDL BDL 3,500 1,800 6,400 BDL BDL BDL 550 BDL 1,000 270 BDL BDL BDL 47 J BDL 140 BDL BDL BDL BDL 19 J
1/21/2013
9/28/2015*NR 698 NR BDL BDL 6,820 2,820 9,880 BDL BDL BDL 810 BDL 2,140 540 BDL BDL BDL 72.8 BDL 239 BDL BDL BDL BDL 97.1
1/31/2018*BDL 1,100 BDL BDL BDL 6,600 4,200 10,400 BDL BDL BDL 910 BDL 5,100 1,400 220 50 BDL 160 34 640 BDL BDL BDL BDL 26
11/7/2019*BDL 420 BDL BDL BDL 2,200 2,500 3,090 BDL BDL BDL 690 BDL 1,800 530 31 J BDL BDL 76 BDL 250 BDL BDL BDL BDL BDL
1/21/2013
9/28/2015*NR 14.6 NR BDL BDL 6,910 1,420 5,740 BDL BDL BDL 407 BDL 1,410 366 BDL BDL BDL 53 BDL 198 BDL BDL BDL BDL 87.4
1/31/2018*BDL BDL BDL BDL BDL 11,000 2,900 10,700 BDL BDL BDL 1,200 BDL 2,400 530 68 J BDL BDL 74 J BDL 270 BDL BDL BDL BDL 36 J
11/7/2019*BDL BDL BDL BDL BDL 6,300 2,500 8,000 BDL BDL BDL 980 J BDL 1,800 510 50 J BDL BDL 76 J BDL 260 BDL BDL BDL BDL 36 J
1/21/2013
9/28/2015*NR 932 NR BDL BDL 32,800 3,450 16,170 BDL BDL BDL 1,030 BDL 3,120 833 BDL BDL BDL 110 BDL 423 BDL BDL BDL BDL 257
1/31/2018*BDL 420 BDL BDL BDL 29,000 3,200 14,100 BDL BDL BDL 1,200 J BDL 2,600 640 BDL BDL BDL 85 J BDL 310 BDL BDL BDL BDL 220 J
11/7/2019*BDL 150 J BDL BDL BDL 23,000 3,300 14,200 BDL BDL BDL 1,900 J BDL 2,300 650 BDL BDL BDL 92 J BDL 320 BDL BDL BDL BDL 190 J
128 1 10 50 70 600 600 500 20 100 70 6 NE 400 400 70 70 70 70 25 70 200 6,000 4,000 0.7 70
12,800 5,000 10,000 50,000 70,000 260,000 84,500 85,500 20,000 100,000 70,000 6,000 NE 28,500 25,000 6,900 8,500 15,000 25,000 11,700 30,000 61,500 6,000,000 4,000,000 700 70,000
Notes:
Analytes that are not shown for the method were not detected.
Concentrations are reported in micrograms per liter (µg/L).
Concentrations exceeding the laboratory's reporting limits are shown in BOLD fields.
Concentrations exceeding their respective 2L Standard are showin in shaded and BOLD fields.
Concentrations exceeding their respective GCLs are showin in shaded, BOLD, and underlined fields.
2L Standard: North Carolina Groundwater Quality Standards: 15A NCAC 2L.0202
GCL - Gross Contaminantion Level
*: Indicates the sample was run at dilution
J: Detection is below the lowest calibration standard, result is an estimated concentration
NR: Not Reported
BDL: Below laboratory detection limits
2L Standards
GCLs
Dry - Monitor Well Not Sampled
Dry - Monitor Well Not Sampled
Dry - Monitor Well Not Sampled
Not Sampled - Well Has Been Paved Over
MW-18
MW-19
Dry - Monitor Well Not Sampled
MW-20
MW-10
Monitor Well Not Sampled
MW-11
Monitor Well Not Sampled
MW-12 Monitor Well Not Sampled
MW-13
Monitor Well Not Sampled
MW-14
MW-15
MW-16
MW-17
Monitor Well Not Sampled
Insufficient Water Volume - Monitor Well Not Sampled
Monitor Well Not Sampled
Monitor Well Not Sampled
Dry - Monitor Well Not Sampled
Insufficient Water Volume - Monitor Well Not Sampled
Dry - Monitor Well Not Sampled
Dry - Monitor Well Not Sampled
Dry - Monitor Well Not Sampled
Monitor Well Not Sampled
Dry - Monitor Well Not Sampled
Monitor Well Not Sampled
Dry - Monitor Well Not Sampled
Dry - Monitor Well Not Sampled
Monitor Well Not Sampled
Dry - Monitor Well Not Sampled 2-butanone (MEK)acetoneObstructed - Monitor Well Not Sampled
MW-2 chloroform4-methyl-2-pentanonen-PropylbenzeneMW-1 Styrenetert-amyl methyl etherbenzenesec-Butylbenzenenaphthalenedi-isopropyl ethermethyl tert-butyl ether1,2,4-TrimethylbenzeneVolatile Organic Compounds (VOCs) by EPA Method 6200B or Equivalent
tert-butyl alcoholchlorobenzenetetrachloroethyleneAnalytical Method →
Contaminant of Concern →1,3-Dichlorobenzenetert-butylbenzenep-Isopropyltoluene1,3,5- Trimethylbenzenetotal xylenesethylbenzenetolueneisopropylbenzene1,2,3-Trichloropropanen-ButylbenzeneMW-3
MW-4
Not Sampled - Well Has Been Paved Over
MW-5
MW-6
Free Product Present - Monitor Well Not Sampled
Free Product Present - Monitor Well Not Sampled
Dry - Monitor Well Not Sampled
Dry - Monitor Well Not Sampled
Monitor Well Not Sampled
Free Product Present - Monitor Well Not Sampled
MW-7
MW-8
Monitor Well Not Sampled
MW-9
Insufficient Water Volume - Monitor Well Not Sampled
Monitor Well Not Sampled
Monitor Well Not Sampled
Insufficient Water Volume - Monitor Well Not Sampled
TABLE 4 - PAGE 2
SUMMARY OF GROUNDWATER SAMPLING RESULTS
Stovall Country Store (Incident No.: 12604, UST #:RA-1601)
6192 NC Highway 96, Oxford, Granville County, North Carolina
S&ME Project # 4305-18-013A
Well
ID
Date
Collected
1/21/2013
9/28/2015*NR 2,950 NR BDL BDL 25,400 3,050 15,120 BDL BDL BDL 781 BDL 2,340 558 BDL BDL BDL 76.2 BDL 241 BDL BDL BDL BDL 174
1/31/2018*BDL 3,300 BDL BDL BDL 26,000 3,000 13,800 BDL BDL BDL 1,000 J BDL 2,200 490 BDL BDL BDL 72 J BDL 230 BDL BDL BDL BDL 140 J
11/7/2019*BDL 3,400 BDL BDL BDL 28,000 3,500 16,300 BDL BDL BDL 1,900 J BDL 2,300 670 BDL BDL BDL 100 J BDL 320 BDL BDL BDL BDL 160 J
1/21/2013
9/28/2015
1/31/2018
11/7/2019*BDL 130 BDL BDL BDL 82 790 780 BDL BDL BDL 340 BDL 1,400 460 30 14 1.8 J 74 10 270 BDL BDL BDL BDL BDL
1/21/2013
9/28/2015
2/1/2018
11/7/2019
1/21/2013
9/28/2015*NR 226 NR BDL BDL 1,450 340 2,740 BDL BDL BDL 249 BDL 548 129 BDL BDL BDL 22.5 BDL 56.9 BDL BDL BDL BDL BDL
2/1/2018
11/7/2019*BDL 45 BDL BDL BDL 200 380 2,110 BDL 45 J BDL 240 BDL 580 130 15 5.4 BDL 26 4.0 J 74 BDL BDL BDL BDL BDL
1/21/2013
9/28/2015 NR BDL NR BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
2/1/2018
11/7/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
1/21/2013
9/28/2015
2/1/2018
11/7/2019
1/21/2013
9/28/2015
2/1/2018
11/7/2019
1/21/2013 NR BDL NR BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
9/28/2015
2/1/2018 NR BDL NR BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 1.9 BDL
11/7/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 2.2 BDL
1/21/2013
9/28/2015
2/1/2018
11/7/2019
1/21/2013 NR 4,600 NR BDL BDL BDL BDL 480 7,100 BDL 750 BDL BDL 110 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
9/28/2015*NR 5,260 NR BDL BDL 3.1 2.5 143 7,430 BDL 897 73.1 BDL 40.3 8.7 BDL 1.5 BDL 11.1 BDL 8.9 BDL BDL BDL BDL BDL
1/31/2018*1,400 5,800 2,300 BDL BDL BDL BDL 147 J 11,000 BDL 1,200 BDL BDL 47 J BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
11/6/2019*670 2,400 13,000 BDL BDL BDL BDL 260 8,200 BDL 1,000 880 J BDL 230 52 J BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
1/21/2013 NR 7,300 NR BDL BDL BDL 31 J BDL 1,000 BDL 220 480 BDL 390 83 BDL BDL BDL 19 J BDL 190 BDL BDL BDL BDL BDL
9/28/2015*NR 8,240 NR BDL BDL 16.6 34.6 1,034 845 BDL 243 346 BDL 431 96.8 BDL BDL BDL 24.7 BDL 29.1 BDL BDL BDL BDL BDL
1/31/2018*130 3,800 830 BDL BDL 4.5 J 16 341 510 BDL 140 220 BDL 190 29 BDL BDL BDL 8.2 J BDL 7.5 J BDL BDL BDL BDL BDL
11/6/2019*66 5,900 820 J BDL BDL 30 85 1,680 370 BDL 140 260 BDL 640 120 BDL BDL BDL 33 BDL 45 BDL BDL BDL BDL BDL
1/21/2013 NR 6 J NR BDL BDL 220 1,300 6,000 BDL BDL BDL 640 BDL 1,600 390 32 J BDL BDL 61 BDL 190 BDL BDL BDL BDL BDL
9/28/2015 NR BDL NR BDL BDL 70.2 171 2,459 14.7 BDL BDL 594 1.1 1,360 435 BDL BDL BDL 90.2 BDL 173 BDL BDL BDL BDL BDL
2/1/2018*NR 5.8 J NR BDL BDL BDL 24 1,020 30 BDL BDL 230 BDL 1,500 370 12 J 6.8 J BDL 57 BDL 130 BDL BDL BDL BDL BDL
11/6/2019*BDL 2.5 J BDL BDL BDL BDL 11 410 4.7 J BDL BDL 96 BDL 930 290 2.7 J 2.4 J BDL 42 2.6 J 94 BDL BDL BDL BDL BDL
1/21/2013 NR BDL NR BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
9/28/2015
2/1/2018
11/6/2019
1/21/2013 NR BDL NR BDL BDL 0.13J BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 3.4 J BDL BDL BDL
9/28/2015
2/1/2018
11/6/2019
1/21/2013 NR 150 NR BDL BDL 0.22 J BDL 36 BDL BDL 3.2 9.7 BDL 7.9 BDL BDL BDL BDL 0.64 J BDL 0.46 J BDL BDL BDL BDL BDL
9/28/2015 NR 89.5 NR BDL BDL BDL BDL 26.3 BDL BDL 3.9 6.2 BDL 6.1 BDL BDL BDL BDL 0.53 BDL BDL BDL BDL BDL BDL BDL
2/1/2018 BDL 11 BDL BDL BDL BDL BDL 2.9 BDL BDL 0.34 J BDL BDL 0.65 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
11/6/2019 BDL 3.6 BDL BDL BDL BDL BDL 1.19 J BDL BDL BDL BDL BDL 0.22 J BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
128 1 10 50 70 600 600 500 20 100 70 6 NE 400 400 70 70 70 70 25 70 200 6,000 4,000 0.7 70
12,800 5,000 10,000 50,000 70,000 260,000 84,500 85,500 20,000 100,000 70,000 6,000 NE 28,500 25,000 6,900 8,500 15,000 25,000 11,700 30,000 61,500 6,000,000 4,000,000 700 70,000
Notes:
Analytes that are not shown for the method were not detected.
Concentrations are reported in micrograms per liter (µg/L).
Concentrations exceeding the laboratory's reporting limits are shown in BOLD fields.
Concentrations exceeding their respective 2L Standard are showin in shaded and BOLD fields.
Concentrations exceeding their respective GCLs are showin in shaded, BOLD, and underlined fields.
2L Standard: North Carolina Groundwater Quality Standards: 15A NCAC 2L.0202
GCL - Gross Contaminantion Level
*: Indicates the sample was run at dilution
J: Detection is below the lowest calibration standard, result is an estimated concentration
NR: Not Reported
BDL: Below laboratory detection limits
GCLs
Dry - Monitor Well Not Sampled
Monitor Well Not Sampled
Dry - Monitor Well Not Sampled
MW-22
DCW-7
2L Standards
Monitor Well Not Sampled
DCW-2
MW-27
Insufficient Water Volume - Monitor Well Not Sampled
Monitor Well Not Sampled
Monitor Well Not Sampled
Monitor Well Not Sampled
MW-28 Monitor Well Not Sampled
Insufficient Water Volume - Monitor Well Not Sampled
MW-21
DCW-6 Monitor Well Not Sampled
Monitor Well Not Sampled
Monitor Well Not Sampled
DCW-3
DCW-4
DCW-5 Monitor Well Not Sampled
Monitor Well Not Sampled
Monitor Well Not Sampled
DCW-1
Surface Obstruction - Monitor Well Not Sampled
Surface Obstruction - Monitor Well Not Sampled
Monitor Well Not Sampled
MW-25
Dry - Monitor Well Not Sampled
Dry - Monitor Well Not Sampled
MW-26
Insufficient Water Volume - Monitor Well Not Sampled
Not Located - Monitor Well Not Sampled
Monitor Well Not Sampled
Monitor Well Not Sampled
MW-23
Dry - Monitor Well Not Sampled
Monitor Well Not Sampled
Monitor Well Not Sampled
Monitor Well Not Sampled
MW-24
Dry - Monitor Well Not Sampled
Dry - Monitor Well Not Sampled Styrenep-Isopropyltoluenen-Propylbenzene1,3-Dichlorobenzeneacetone2-butanone (MEK)tetrachloroethylene1,2,4-Trimethylbenzene1,3,5- Trimethylbenzenen-Butylbenzenesec-Butylbenzenetert-butylbenzeneisopropylbenzene1,2,3-TrichloropropaneAnalytical Method →Volatile Organic Compounds (VOCs) by EPA Method 6200B or Equivalent
Contaminant of Concern →tert-amyl methyl etherbenzenetert-butyl alcoholchlorobenzenechloroformtolueneethylbenzenetotal xylenesmethyl tert-butyl ether4-methyl-2-pentanonedi-isopropyl ethernaphthalene
Sample ID Date Collected
1/21/2013 130 NR NR BDL BDL 20 BDL 1 160 16 BDL BDL BDL 0.3 J 10 BDL 49 J
2/22/2013 190 NR NR BDL BDL 20 BDL 1.3 170 11 BDL BDL BDL 1.2 13 BDL 77.9
9/18/2015 368 NR NR BDL BDL 54.2 BDL 4.2 289 34.1 BDL BDL BDL 0.57 8.9 BDL 122.2
2/1/2018 13 30 78 BDL 0.13 34 BDL 0.48 190 2.1 BDL BDL BDL BDL 1.1 BDL 6.1
11/7/2019 13 BDL BDL 2.8 1.4 J 88 BDL 3.9 460 BDL 1.2 J 55 700 BDL 6.5 1.2 J 11
1/21/2013 74 NR NR BDL BDL 24 BDL 0.82 J 180 15 BDL BDL BDL BDL 8.4 BDL 33.7
2/22/2013 9 NR NR BDL BDL 20 BDL BDL 170 BDL BDL BDL BDL BDL BDL BDL BDL
9/18/2015 BDL NR NR BDL BDL BDL BDL BDL 160 BDL BDL BDL BDL BDL BDL BDL BDL
2/1/2018 BDL 21 86 BDL BDL 9.7 BDL BDL 330 BDL BDL BDL BDL BDL BDL BDL BDL
11/7/2019 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
1 128 10 70 70 70 600 70 20 6 70 128 10 600 400 400 500
5,000 12,800 10,000 6,900 8,500 70,000 84,500 25,000 20,000 6,000 30,000 128,000 10,000 260,000 28,500 25,000 85,500
Notes:
1. Analytes that are not shown for the method were not detected.
2. µg/L: micrograms per liter
3. VOCs: Volatile Organic Compounds
4. 2L Standard: North Carolina Groundwater Quality Standards: 15A NCAC 2L.0202.
5. BDL: Below Laboratory Detection Limits
6. NR: Analysis Not Requested for Sample
7. Concentrations exceeding the 2L Standards are shown in Shaded and BOLD fields.
8. Concentrations exceeding the laboratory's reporting limits are shown in BOLD fields.
Summary of Water Supply Well Analytical Results
TABLE 5
Analytical Method →methyl tert-butyl etherdi-isopropyl ethernaphthaleneethylbenzeneVolatile Organic Compounds (VOCs) by EPA 6200B(µg/L)
S&ME Project No. 4305-18-013
1,2,4-trimethylbenzeneisopropylbenzenetotal xylenes6192 NC Highway 96, Oxford, Granville County, North Carolina
Stovall Country Store (Incident No.: 12604, UST #:RA-1601)1,3,5-trimethylbenzenen-butylbenzeneGross Contaminant Levels
Contaminant of Concern →benzenetolueneWSW-1 (Eff)
2L Standards tert-amyl methyl ethertert-butyl alocholsec-butylbenzeneWSW-1 (Inf)n-propylbenzenetert-amyl methyl ethertert-butyl alcohol
Appendix III– Photo Log
Groundwater Monitoring Report
Stovall Country Store – Incident No. TF-12604
6195 Highway 96
Oxford, Granville County, North Carolina
S&ME Project No. 4305-18-013A 11/6/2019Photographer: James Waters1 Photo Description General view of the site. 11/6/2019Photographer: James Waters2 Photo Description Area of the monitor well DCW-1 located underneath the
observed structure.
Groundwater Monitoring Report
Stovall Country Store – Incident No. TF-12604
6195 Highway 96
Oxford, Granville County, North Carolina
S&ME Project No. 4305-18-013A 11/6/2019Photographer: James Waters3 Photo Description View of the DCW-2 location. 11/6/2019Photographer: James Waters4 Photo Description View of the DCW-3 location.
Groundwater Monitoring Report
Stovall Country Store – Incident No. TF-12604
6195 Highway 96
Oxford, Granville County, North Carolina
S&ME Project No. 4305-18-013A 11/6/2019Photographer: James Waters5 Photo Description View of the DCW-4 location. 11/6/2019Photographer: James Waters6 Photo Description View of the DCW-5 location.
Groundwater Monitoring Report
Stovall Country Store – Incident No. TF-12604
6195 Highway 96
Oxford, Granville County, North Carolina
S&ME Project No. 4305-18-013A 11/6/2019Photographer: James Waters7 Photo Description View of the DCW-7 location. 11/6/2019Photographer: James Waters8 Photo Description View of the MW-1 location.
Groundwater Monitoring Report
Stovall Country Store – Incident No. TF-12604
6195 Highway 96
Oxford, Granville County, North Carolina
S&ME Project No. 4305-18-013A 11/6/2019Photographer: James Waters9 Photo Description View of the MW-2 location. 11/6/2019Photographer: James Waters10 Photo Description MW-4 and MW-16 location has been paved over.
Groundwater Monitoring Report
Stovall Country Store – Incident No. TF-12604
6195 Highway 96
Oxford, Granville County, North Carolina
S&ME Project No. 4305-18-013A 11/6/2019Photographer: James Waters11 Photo Description View of the MW-5 location. 11/6/2019Photographer: James Waters12 Photo Description View of the MW-6 location.
Groundwater Monitoring Report
Stovall Country Store – Incident No. TF-12604
6195 Highway 96
Oxford, Granville County, North Carolina
S&ME Project No. 4305-18-013A 11/6/2019Photographer: James Waters13 Photo Description View of the MW-7 location. 11/6/2019Photographer: James Waters14 Photo Description View of the MW-8 location.
Groundwater Monitoring Report
Stovall Country Store – Incident No. TF-12604
6195 Highway 96
Oxford, Granville County, North Carolina
S&ME Project No. 4305-18-013A 11/6/2019Photographer: James Waters15 Photo Description View of the MW-9 location. 11/6/2019Photographer: James Waters16 Photo Description View of the MW-12 location.
Groundwater Monitoring Report
Stovall Country Store – Incident No. TF-12604
6195 Highway 96
Oxford, Granville County, North Carolina
S&ME Project No. 4305-18-013A 11/6/2019Photographer: James Waters17 Photo Description View of the MW-13 location. 11/6/2019Photographer: James Waters18 Photo Description View of the MW-14 location.
Groundwater Monitoring Report
Stovall Country Store – Incident No. TF-12604
6195 Highway 96
Oxford, Granville County, North Carolina
S&ME Project No. 4305-18-013A 11/6/2019Photographer: James Waters19 Photo Description View of the MW-15 location. 11/6/2019Photographer: James Waters20 Photo Description View of the MW-17 location.
Groundwater Monitoring Report
Stovall Country Store – Incident No. TF-12604
6195 Highway 96
Oxford, Granville County, North Carolina
S&ME Project No. 4305-18-013A 11/6/2019Photographer: James Waters21 Photo Description View of the MW-17 location. 11/6/2019Photographer: James Waters22 Photo Description View of the MW-18 location.
Groundwater Monitoring Report
Stovall Country Store – Incident No. TF-12604
6195 Highway 96
Oxford, Granville County, North Carolina
S&ME Project No. 4305-18-013A 11/6/2019Photographer: James Waters23 Photo Description View of the MW-19 location. 11/6/2019Photographer: James Waters24 Photo Description View of the MW-20 location.
Groundwater Monitoring Report
Stovall Country Store – Incident No. TF-12604
6195 Highway 96
Oxford, Granville County, North Carolina
S&ME Project No. 4305-18-013A 11/6/2019Photographer: James Waters25 Photo Description View of the MW-21 location. 11/6/2019Photographer: James Waters26 Photo Description View of the MW-22 location.
Groundwater Monitoring Report
Stovall Country Store – Incident No. TF-12604
6195 Highway 96
Oxford, Granville County, North Carolina
S&ME Project No. 4305-18-013A 11/6/2019Photographer: James Waters27 Photo Description View of the MW-23 location. 11/6/2019Photographer: James Waters28 Photo Description View of the MW-24 location.
Groundwater Monitoring Report
Stovall Country Store – Incident No. TF-12604
6195 Highway 96
Oxford, Granville County, North Carolina
S&ME Project No. 4305-18-013A 11/6/2019Photographer: James Waters29 Photo Description View of the MW-25 location. 11/6/2019Photographer: James Waters30 Photo Description View of the MW-28 location.
Groundwater Monitoring Report
Stovall Country Store – Incident No. TF-12604
6195 Highway 96
Oxford, Granville County, North Carolina
S&ME Project No. 4305-18-013A 11/7/2019Photographer: James Waters31 Photo Description View of the WSW-1 location. 11/7/2019Photographer: James Waters32 Photo Description View of the old POE system on WSW-1.
Groundwater Monitoring Report
Stovall Country Store – Incident No. TF-12604
6195 Highway 96
Oxford, Granville County, North Carolina
S&ME Project No. 4305-18-013A 11/7/2019Photographer: James Waters33 Photo Description View of the new POE system at WSW-1 11/7/2019Photographer: James Waters34 Photo Description View of the new POE system cabinet.
Appendix IV – Field Notes and Field Sampling Forms
° F
Date Time
11/6/19 15:05 4.0 10.0
11/6/19 15:05 µS/cm
22.25 ft-TOC inch
65.00 ft-TOC gal
42.75 feet gal
5 ft-GRD gal
-0.05 ft-GRD
15:20 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
15:30 7.4 18.3 408 NM
15:40 6.6 17.4 472 NM
15:50 6.7 17.6 438 NM
15:55
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
James Waters 11/7/2019
9/13/17 8:00 AM
Name Signature Date
(+5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
Sample Method:Bailer Sample Time:
(Gal)
7.0 No Odors
14.0 No Odors
21.0 No Odors
Total Volume Purged:21.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 34.9
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:15:50
Total Well Depth:Well Volume 7.0
Height of Water Column:3 * Well Volume 20.9
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather:Sunny Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:15:55
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:DCW-2 Purge Time (Min.):30
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
° F
Date Time
11/6/19 15:05 4.0 10.0
11/6/19 15:05 µS/cm
21.96 ft-TOC inch
60.00 ft-TOC gal
38.04 feet gal
5 ft-GRD gal
-0.25 ft-GRD
16:00 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
16:10 7.0 18.1 397 NM
16:20 6.8 18 312 NM
16:35
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
James Waters 11/7/2019
DCW-3 was purged dry, allowed to recover, then sampled.
9/13/17 8:00 AM
Name Signature Date
(+5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
Sample Method:Bailer Sample Time:
(Gal)
6.3 Petroleum Odors
11.0 Petroleum Odors
Total Volume Purged:11.0 Well Purged Dry?:Yes
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 31.0
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:16:30
Total Well Depth:Well Volume 6.2
Height of Water Column:3 * Well Volume 18.6
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather:Sunny Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:16:35
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:DCW-3 Purge Time (Min.):30
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
° F
Date Time
11/6/19 15:05 4.0 10.0
11/6/19 15:05 µS/cm
21.23 ft-TOC inch
60.00 ft-TOC gal
38.77 feet gal
5 ft-GRD gal
-0.25 ft-GRD
16:40 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
16:50 6.9 16.4 169 NM
17:00 6.8 16.4 174 NM
17:10 6.1 16.4 157 NM
17:15
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
James Waters 11/7/2019
9/13/17 8:00 AM
Name Signature Date
(+5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
Sample Method:Bailer Sample Time:
(Gal)
6.3 No Odors
12.6 No Odors
19.0 No Odors
Total Volume Purged:19.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 31.6
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:17:10
Total Well Depth:Well Volume 6.3
Height of Water Column:3 * Well Volume 19.0
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather:Sunny Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:17:15
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:DCW-4 Purge Time (Min.):30
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
° F
Date Time
11/6/19 15:05 4.0 10.0
11/6/19 15:05 µS/cm
22.71 ft-TOC inch
60.00 ft-TOC gal
37.29 feet gal
5 ft-GRD gal
-0.2 ft-GRD
17:20 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
17:30 6.4 15.8 87 NM
17:40 6.2 15.8 96 NM
17:50 6.2 15.8 98 NM
17:55
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
James Waters 11/7/2019
Field Blank 11/6/19 is taken at 1800, after sampling DCW-7.
9/13/17 8:00 AM
Name Signature Date
(+5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
Sample Method:Bailer Sample Time:
(Gal)
6.3 No Odors
12.6 No Odors
19.0 No Odors
Total Volume Purged:19.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 30.4
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:17:50
Total Well Depth:Well Volume 6.1
Height of Water Column:3 * Well Volume 18.3
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather:Sunny Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:17:55
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:DCW-7 Purge Time (Min.):30
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
4.00 7.00 10.00
μS/cm μS/cm
°C μS/cm
Qty Pres.Qty Pres.
3 HCl
Date
(1)
(2)
Revision:9/1/17 13:30
Name Signature
James Waters 11/7/2019
Additional Comments (description of location of sample port, water well, filters, etc.)Well / System Photographs
Well house is located to the east, behind the store. The old POE system is no longer in use and a new POE system
has been installed.
Site Sketch
VOCs 6200B (+MTBE, IPE, &
EDB)40mL VOAs
(+ 5 Oxygenates, Ethanol)
WSW-1 Effluent After the Carbon Filters 11/7/2019 16:15
Method Container Method Container
Sample ID Sample Location Sample Date Sample Time
60.00 16:10 6.76 16.9 NM
30.00 16:00 6.43 17.3 NM
45.00 16:05 6.71 16.9 NM
Volume Purged (Gal):60.0 Purge End Time:16:05
Field Parameters and Sampling
Total Volume (Gal)Time pH (s.u.)Temperature Conductivity
Well Purging Information
Purge Rate (GPM): 3.0 Purge Start Time:15:50
pH 11/7/19 08:35 4.00, 7.00, 10.00
Conductivity 11/7/19 08:35 1413 1,413
Equipment Date Time Calibration Solution Calibration Check
POE Present (Y/N): Y Owner Phone No.:
Equipment Calibration Information:
Weather:Partly Cloudy Well Address: 6195 Hwy 96 Oxford, NC
Air Temp (°F):60 Owner Name:The Country Store
Project Number:4305-18-013A Sample Date:Thursday, November 7, 2019
Client Name/Contact:NCDEQ Water Supply Well ID:WSW-1 Effluent
WATER SUPPLY WELL SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy 96 Oxford, NC
4.00 7.00 10.00
μS/cm μS/cm
°C μS/cm
Qty Pres.Qty Pres.
3 HCl
Date
(1)
(2)
Revision:
Project Number:4305-18-013A Sample Date:Thursday, November 7, 2019
Client Name/Contact:NCDEQ Water Supply Well ID:WSW-1 Influent
WATER SUPPLY WELL SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy 96 Oxford, NC
POE Present (Y/N): Y Owner Phone No.:
Equipment Calibration Information:
Weather:Partly Cloudy Well Address: 6195 Hwy 96 Oxford, NC
Air Temp (°F):60 Owner Name:The Country Store
Well Purging Information
Purge Rate (GPM): 3.0 Purge Start Time:15:50
pH 11/7/19 08:35 4.00, 7.00, 10.00
Conductivity 11/7/19 08:35 1413 1,413
Equipment Date Time Calibration Solution Calibration Check
Volume Purged (Gal):60.0 Purge End Time:16:05
Field Parameters and Sampling
Total Volume (Gal)Time pH (s.u.)Temperature Conductivity
30.00 16:00 6.43 17.3 NM
45.00 16:05 6.71 16.9 NM
60.00 16:10 16.9 NM
Sample ID Sample Location Sample Date Sample Time
VOCs 6200B (+MTBE, IPE, &
EDB)40mL VOAs
(+ 5 Oxygenates, Ethanol)
WSW-1 Influent Raw System Influent 11/7/2019 16:20
Method Container Method Container
Additional Comments (description of location of sample port, water well, filters, etc.)Well / System Photographs
Well house is located to the east, behind the store. The old POE system is no longer in use and a new POE
system has been installed.
Site Sketch
9/1/17 13:30
Name Signature
James Waters 11/7/2019
° F
Date Time
11/7/19 08:35 4.0 10.0
11/7/19 08:35 µS/cm
20.88 ft-TOC inch
42.00 ft-TOC gal
21.12 feet gal
22 ft-GRD gal
-0.3 ft-GRD
08:45 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
08:50 7.8 15.8 11 NM
08:55 6.4 16.1 5 NM
09:00 6.1 16.1 NM NM
09:05
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:MW-1 Purge Time (Min.):15
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
Weather:Partly Cloudy Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:09:05
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 3.4
Height of Water Column:3 * Well Volume 10.3
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:11.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 17.2
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:09:00
(Gal)
3.6 No Odors
7.3 No Odors
11.0 No Odors
Sample Method:Bailer Sample Time:
(+ 5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
James Waters 11/7/2019
Multipurpose meter began having problems with conductivity readings. Attempted to recalibrate, but was unable to.
9/13/17 8:00 AM
Name Signature Date
° F
Date Time
11/7/19 08:35 4.0 10.0
11/7/19 08:35 µS/cm
20.90 ft-TOC inch
35.00 ft-TOC gal
14.10 feet gal
15 ft-GRD gal
-0.6 ft-GRD
09:10 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
09:15 6.3 16.3 NM NM
09:30
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:MW-2 Purge Time (Min.):5
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
Weather:Partly Cloudy Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:09:30
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 2.3
Height of Water Column:3 * Well Volume 6.9
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:2.3 Well Purged Dry?:Yes
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 11.5
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:09:15
(Gal)
2.3 No Odors
Sample Method:Bailer Sample Time:
(+ 5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
James Waters 11/7/2019
MW-2 was purged dry, allowed to recover, then sampled.
9/13/17 8:00 AM
Name Signature Date
° F
Date Time
11/7/19 08:35 4.0 10.0
11/7/19 08:35 µS/cm
21.85 ft-TOC inch
35.00 ft-TOC gal
13.15 feet gal
15 ft-GRD gal
-0.65 ft-GRD
09:35 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
09:40 5.9 18 NM NM
09:45 5.4 18 NM NM
09:50 5.3 18 NM NM
09:55
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:MW-3 Purge Time (Min.):15
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
Weather:Partly Cloudy Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:09:55
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 2.1
Height of Water Column:3 * Well Volume 6.4
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:7.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 10.7
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:09:50
(Gal)
2.3 No Odors
4.6 No Odors
7.0 No Odors
Sample Method:Bailer Sample Time:
(+ 5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
James Waters 11/7/2019
9/13/17 8:00 AM
Name Signature Date
° F
Date Time
11/7/19 08:35 4.0 10.0
11/7/19 08:35 µS/cm
20.89 ft-TOC inch
30.00 ft-TOC gal
9.11 feet gal
15 ft-GRD gal
-0.9 ft-GRD
10:00 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
10:05 5.3 17.9 NM NM
10:10 4.9 17.8 NM NM
10:15 4.9 17.7 NM NM
10:20
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:MW-5 Purge Time (Min.):15
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
Weather:Partly Cloudy Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:10:20
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 1.5
Height of Water Column:3 * Well Volume 4.5
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:5.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 7.4
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:10:15
(Gal)
1.6 Petroleum Odors
3.3 Petroleum Odors
5.0 Petroleum Odors
Sample Method:Bailer Sample Time:
(+ 5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
James Waters 11/7/2019
9/13/17 8:00 AM
Name Signature Date
° F
Date Time
11/7/19 08:35 4.0 10.0
11/7/19 08:35 µS/cm
22.44 ft-TOC inch
30.00 ft-TOC gal
7.56 feet gal
15 ft-GRD gal
-0.5 ft-GRD
10:25 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
10:30 5.2 19 NM NM
10:35 5.0 18.8 NM NM
10:40 5.0 18.6 NM NM
10:45
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:MW-6 Purge Time (Min.):15
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
Weather:Partly Cloudy Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:10:45
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 1.2
Height of Water Column:3 * Well Volume 3.7
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:4.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 6.2
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:10:40
(Gal)
1.3 No Odors
2.6 No Odors
4.0 No Odors
Sample Method:Bailer Sample Time:
(+ 5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
James Waters 11/7/2019
9/13/17 8:00 AM
Name Signature Date
° F
Date Time
11/7/19 08:35 4.0 10.0
11/7/19 08:35 µS/cm
23.81 ft-TOC inch
30.00 ft-TOC gal
6.19 feet gal
15 ft-GRD gal
-0.35 ft-GRD
10:50 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
10:55 5.8 19.7 NM NM
11:00 5.7 19.6 NM NM
11:05 5.7 19.5 NM NM
11:10
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:MW-7 Purge Time (Min.):15
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
Weather:Partly Cloudy Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:11:10
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 1.0
Height of Water Column:3 * Well Volume 3.0
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:3.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 5.1
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:11:05
(Gal)
1.0 No Odors
2.0 No Odors
3.0 No Odors
Sample Method:Bailer Sample Time:
(+ 5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
James Waters 11/7/2019
9/13/17 8:00 AM
Name Signature Date
° F
Date Time
11/7/19 08:35 4.0 10.0
11/7/19 08:35 µS/cm
19.29 ft-TOC inch
20.00 ft-TOC gal
0.71 feet gal
15 ft-GRD gal
-0.4 ft-GRD
End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
11:15
Qty Container Pres.Qty Pres.
1 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:MW-9 Purge Time (Min.):
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
Weather:Partly Cloudy Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:11:15
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 0.1
Height of Water Column:3 * Well Volume 0.3
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:Well Purged Dry?:Yes
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 0.6
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:
(Gal)
Sample Method:Bailer Sample Time:
(+ 5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
James Waters 11/7/2019
Not enough water to record parameters. Only able to fill 1 vial.
9/13/17 8:00 AM
Name Signature Date
° F
Date Time
11/7/19 08:35 4.0 10.0
11/7/19 08:35 µS/cm
23.95 ft-TOC inch
25.00 ft-TOC gal
1.05 feet gal
20 ft-GRD gal
-0.5 ft-GRD
End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
11:20
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:MW-12 Purge Time (Min.):
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
Weather:Partly Cloudy Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:11:20
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 0.2
Height of Water Column:3 * Well Volume 0.5
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:Well Purged Dry?:Yes
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 0.9
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:
(Gal)
Sample Method:Bailer Sample Time:
(+ 5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
James Waters 11/7/2019
Not enough water to record parameters.
9/13/17 8:00 AM
Name Signature Date
° F
Date Time
11/7/19 08:35 4.0 10.0
11/7/19 08:35 µS/cm
21.92 ft-TOC inch
25.00 ft-TOC gal
3.08 feet gal
20 ft-GRD gal
-0.4 ft-GRD
11:25 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
11:30 5.1 19.7 NM NM
11:35
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:MW-14 Purge Time (Min.):5
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
Weather:Partly Cloudy Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:11:35
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 0.5
Height of Water Column:3 * Well Volume 1.5
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:0.5 Well Purged Dry?:Yes
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 2.5
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:11:30
(Gal)
0.5 Petroleum Odors
Sample Method:Bailer Sample Time:
(+ 5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
James Waters 11/7/2019
Only enough water to get one set of parameters. Well was purged dry, allowed to recover, then sampled.
9/13/17 8:00 AM
Name Signature Date
° F
Date Time
11/7/19 08:35 4.0 10.0
11/7/19 08:35 µS/cm
21.83 ft-TOC inch
25.00 ft-TOC gal
3.17 feet gal
20 ft-GRD gal
-0.3 ft-GRD
11:40 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
11:45 5.0 20.4 NM NM
11:50 4.8 20.1 NM NM
11:55
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:MW-15 Purge Time (Min.):10
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
Weather:Partly Cloudy Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:11:55
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 0.5
Height of Water Column:3 * Well Volume 1.6
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:1.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 2.6
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:11:50
(Gal)
0.6 No Odors
1.0 No Odors
Sample Method:Bailer Sample Time:
(+ 5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
James Waters 11/7/2019
9/13/17 8:00 AM
Name Signature Date
° F
Date Time
11/7/19 08:35 4.0 10.0
11/7/19 08:35 µS/cm
ft-TOC inch
25.00 ft-TOC gal
25.00 feet gal
20 ft-GRD gal
ft-GRD
End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
Qty Container Pres.Qty Pres.
(1)
Notes:
Form Revision Date:
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:MW-16 Purge Time (Min.):
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
Weather:Partly Cloudy Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 4.1
Height of Water Column:3 * Well Volume 12.2
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:Well Purged Dry?:
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 20.4
Stickup Height:
Well Purging Information
Purge Method:Purge Start Time:
(Gal)
Sample Method:Sample Time:
Analytical Data
Method Method Container
James Waters 11/7/2019
MW-16, along with MW-4, has been covered by a new layer of asphalt in the parking lot. Unable to record water levels or sample MW-16.
9/13/17 8:00 AM
Name Signature Date
° F
Date Time
11/7/19 08:35 4.0 10.0
11/7/19 08:35 µS/cm
20.93 ft-TOC inch
25.00 ft-TOC gal
4.07 feet gal
20 ft-GRD gal
-0.5 ft-GRD
12:10 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
12:15 5.8 18.1 NM NM
12:20 6.1 17.5 NM NM
12:25 6.2 17.4 NM NM
12:30
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:MW-17 Purge Time (Min.):15
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
Weather:Partly Cloudy Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:12:30
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 0.7
Height of Water Column:3 * Well Volume 2.0
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:2.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 3.3
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:12:25
(Gal)
0.6 No Odors
1.3 No Odors
2.0 No Odors
Sample Method:Bailer Sample Time:
(+ 5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
James Waters 11/7/2019
9/13/17 8:00 AM
Name Signature Date
° F
Date Time
11/7/19 08:35 4.0 10.0
11/7/19 08:35 µS/cm
20.39 ft-TOC inch
25.00 ft-TOC gal
4.61 feet gal
20 ft-GRD gal
-0.6 ft-GRD
12:35 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
12:40 6.5 18.4 NM NM
12:45 6.5 18.2 NM NM
12:50 6.5 18 NM NM
12:55
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:MW-18 Purge Time (Min.):15
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
Weather:Partly Cloudy Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:12:55
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 0.8
Height of Water Column:3 * Well Volume 2.3
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:3.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 3.8
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:12:50
(Gal)
1.0 Petroleum Odors
2.0 Petroleum Odors
3.0 Petroleum Odors
Sample Method:Bailer Sample Time:
(+ 5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
James Waters 11/7/2019
9/13/17 8:00 AM
Name Signature Date
° F
Date Time
11/7/19 08:35 4.0 10.0
11/7/19 08:35 µS/cm
19.48 ft-TOC inch
25.00 ft-TOC gal
5.52 feet gal
20 ft-GRD gal
-0.1 ft-GRD
13:00 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
13:05 6.8 18.3 NM NM
13:10 6.6 18.3 NM NM
13:15 6.6 18.2 NM NM
13:20
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:MW-19 Purge Time (Min.):15
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
Weather:Partly Cloudy Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:13:20
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 0.9
Height of Water Column:3 * Well Volume 2.7
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:3.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 4.5
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:13:15
(Gal)
1.0 Petroleum Odors
2.0 Petroleum Odors
3.0 Petroleum Odors
Sample Method:Bailer Sample Time:
(+ 5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
James Waters 11/7/2019
9/13/17 8:00 AM
Name Signature Date
° F
Date Time
11/7/19 08:35 4.0 10.0
11/7/19 08:35 µS/cm
19.26 ft-TOC inch
25.00 ft-TOC gal
5.74 feet gal
20 ft-GRD gal
-0.1 ft-GRD
13:25 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
13:30 6.8 18.1 NM NM
13:35 6.4 17.8 NM NM
13:40 6.4 17.7 NM NM
13:45
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:MW-20 Purge Time (Min.):15
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
Weather:Partly Cloudy Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:13:45
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 0.9
Height of Water Column:3 * Well Volume 2.8
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:3.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 4.7
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:13:40
(Gal)
1.0 Petroleum Odors
2.0 Petroleum Odors
3.0 Petroleum Odors
Sample Method:Bailer Sample Time:
(+ 5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
James Waters 11/7/2019
9/13/17 8:00 AM
Name Signature Date
° F
Date Time
11/7/19 08:35 4.0 10.0
11/7/19 08:35 µS/cm
21.27 ft-TOC inch
25.00 ft-TOC gal
3.73 feet gal
20 ft-GRD gal
-0.5 ft-GRD
13:50 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
13:55 5.5 19.8 NM NM
14:00 4.7 19.7 NM NM
14:05 4.6 19.6 NM NM
14:10
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:MW-21 Purge Time (Min.):15
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
Weather:Partly Cloudy Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:14:10
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 0.6
Height of Water Column:3 * Well Volume 1.8
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:2.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 3.0
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:14:05
(Gal)
0.6 Petroleum Odors
1.3 Petroleum Odors
2.0 Petroleum Odors
Sample Method:Bailer Sample Time:
(+ 5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
James Waters 11/7/2019
9/13/17 8:00 AM
Name Signature Date
° F
Date Time
11/7/19 08:35 4.0 10.0
11/7/19 08:35 µS/cm
21.63 ft-TOC inch
25.00 ft-TOC gal
3.37 feet gal
20 ft-GRD gal
-0.7 ft-GRD
14:15 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
14:20 5.7 19.9 NM NM
14:35
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:MW-22 Purge Time (Min.):5
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
Weather:Partly Cloudy Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:14:35
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 0.5
Height of Water Column:3 * Well Volume 1.6
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:0.6 Well Purged Dry?:Yes
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 2.7
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:14:20
(Gal)
0.6 No Odors
Sample Method:Bailer Sample Time:
(+ 5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
James Waters 11/7/2019
MW-22 was purged dry, allowed to recover, then sampled.
9/13/17 8:00 AM
Name Signature Date
° F
Date Time
11/7/19 08:35 4.0 10.0
11/7/19 08:35 µS/cm
22.02 ft-TOC inch
25.00 ft-TOC gal
2.98 feet gal
20 ft-GRD gal
-0.75 ft-GRD
14:40 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
14:45 7.3 17.5 NM NM
15:00
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:MW-24 Purge Time (Min.):5
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
Weather:Partly Cloudy Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:15:00
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 0.5
Height of Water Column:3 * Well Volume 1.5
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:0.6 Well Purged Dry?:Yes
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 2.4
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:14:45
(Gal)
0.6 No Odors
Sample Method:Bailer Sample Time:
(+ 5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
James Waters 11/7/2019
MW-24 was purged dry, allowed to recover, then sampled.
9/13/17 8:00 AM
Name Signature Date
° F
Date Time
11/7/19 08:35 4.0 10.0
11/7/19 08:35 µS/cm
21.95 ft-TOC inch
25.00 ft-TOC gal
3.05 feet gal
20 ft-GRD gal
6 ft-GRD
15:05 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
15:10 7.3 17.6 NM NM
15:20
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:MW-25 Purge Time (Min.):5
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
Weather:Partly Cloudy Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:15:20
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 0.5
Height of Water Column:3 * Well Volume 1.5
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:0.6 Well Purged Dry?:Yes
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 2.5
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:15:10
(Gal)
0.6 No Odors
Sample Method:Bailer Sample Time:
(+ 5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
James Waters 11/7/2019
MW-25 was purged dry, allowed to recover, then sampled.
9/13/17 8:00 AM
Name Signature Date
° F
Date Time
11/7/19 08:35 4.0 10.0
11/7/19 08:35 µS/cm
23.29 ft-TOC inch
25.00 ft-TOC gal
1.71 feet gal
15 ft-GRD gal
-0.25 ft-GRD
15:25 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
15:30 6.5 17.6 NM NM
15:40
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
Project Number:4305-18-013A Purge Date:November 6, 2019
Source Well:MW-28 Purge Time (Min.):5
GROUNDWATER SAMPLING FORM
Project Name:TF-12604 Stovall’s Grocery
Project Location:6195 Hwy. 96 Oxford, NC
Weather:Partly Cloudy Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:November 6, 2019
Sampled By:James Waters Sample Time:15:40
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Total Well Depth:Well Volume 0.3
Height of Water Column:3 * Well Volume 0.8
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
Total Volume Purged:0.3 Well Purged Dry?:Yes
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 1.4
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:15:30
(Gal)
0.3 No Odors
Sample Method:Bailer Sample Time:
(+ 5 Oxygenates, Ethanol)
Analytical Data
Method Method Container
VOCs 6200B (+MTBE, IPE, & EDB)
James Waters 11/7/2019
MW-25 was purged dry, allowed to recover, then sampled. Field Blank 11/7/19 is taken at 1545, after sampling MW-28.
9/13/17 8:00 AM
Name Signature Date
Appendix V - Laboratory Analytical Report and Chain of Custody
Record
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
November 19, 2019
Michael Pfeifer
S&ME, Inc - Raleigh, NC
3201 Spring Forest Rd.
Raleigh, NC 27616
Project Location: 6195 Hwy 96, Oxford, NC
Client Job Number:
Project Number: 4305-18-013C
Laboratory Work Order Number: 19K0568
Enclosed are results of analyses for samples received by the laboratory on November 8, 2019. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 90
Table of Contents
Table of Contents
Sample Summary 4
Hits Only Report 5
Case Narrative 12
Sample Results 15
19K0568-01 15
19K0568-02 17
19K0568-03 19
19K0568-04 21
19K0568-05 23
19K0568-06 25
19K0568-07 27
19K0568-08 29
19K0568-09 31
19K0568-10 33
19K0568-11 35
19K0568-12 37
19K0568-13 39
19K0568-14 41
19K0568-15 43
19K0568-16 45
19K0568-17 47
19K0568-18 49
19K0568-19 51
19K0568-20 53
19K0568-21 55
Page 2 of 90
Table of Contents
Table of Contents (continued)
19K0568-22 57
19K0568-23 59
19K0568-24 61
19K0568-25 63
19K0568-26 65
19K0568-27 67
Sample Preparation Information 69
QC Data 70
Volatile Organic Compounds by GC/MS 70
B245814 70
B245876 74
B246118 78
Flag/Qualifier Summary 83
Certifications 84
Chain of Custody/Sample Receipt 86
Page 3 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
11/19/2019
S&ME, Inc - Raleigh, NC
3201 Spring Forest Rd.
Raleigh, NC 27616
ATTN: Michael Pfeifer
4305-18-013C
19K0568
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
6195 Hwy 96, Oxford, NC
DCW-2 19K0568-01 Ground Water SM21-22 6200B
DCW-3 19K0568-02 Ground Water SM21-22 6200B
DCW-4 19K0568-03 Ground Water SM21-22 6200B
DCW-7 19K0568-04 Ground Water SM21-22 6200B
Field Blank 11/6/19 19K0568-05 Field Blank SM21-22 6200B
MW-1 19K0568-06 Ground Water SM21-22 6200B
MW-2 19K0568-07 Ground Water SM21-22 6200B
MW-3 19K0568-08 Ground Water SM21-22 6200B
MW-5 19K0568-09 Ground Water SM21-22 6200B
MW-6 19K0568-10 Ground Water SM21-22 6200B
MW-7 19K0568-11 Ground Water SM21-22 6200B
MW-9 19K0568-12 Ground Water SM21-22 6200B
MW-12 19K0568-13 Ground Water SM21-22 6200B
MW-14 19K0568-14 Ground Water SM21-22 6200B
MW-15 19K0568-15 Ground Water SM21-22 6200B
MW-17 19K0568-16 Ground Water SM21-22 6200B
MW-18 19K0568-17 Ground Water SM21-22 6200B
MW-19 19K0568-18 Ground Water SM21-22 6200B
MW-20 19K0568-19 Ground Water SM21-22 6200B
MW-21 19K0568-20 Ground Water SM21-22 6200B
MW-22 19K0568-21 Ground Water SM21-22 6200B
MW-24 19K0568-22 Ground Water SM21-22 6200B
MW-25 19K0568-23 Ground Water SM21-22 6200B
MW-28 19K0568-24 Ground Water SM21-22 6200B
Field Blank 11/7/19 19K0568-25 Field Blank SM21-22 6200B
WSW-1 Effluent 19K0568-26 Water SM21-22 6200B
WSW-1 Influent 19K0568-27 Water SM21-22 6200B
[TOC_1]Sample Summary[TOC]
Page 4 of 90
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:19K0568-05Field Blank 11/6/19
No Results Detected
Client ID:Lab ID:19K0568-10MW-6
No Results Detected
Client ID:Lab ID:19K0568-11MW-7
No Results Detected
Client ID:Lab ID:19K0568-23MW-25
No Results Detected
Client ID:Lab ID:19K0568-25Field Blank 11/7/19
No Results Detected
Client ID:Lab ID:19K0568-26WSW-1 Effluent
No Results Detected
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 5 of 90
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-01DCW-2
DL
1,2,4-Trimethylbenzene 230 100 g/L SM21-22 6200B36
1,3,5-Trimethylbenzene 52 100 g/L SM21-22 6200BJ28
Benzene 2400 100 g/L SM21-22 6200B36
Diisopropyl Ether (DIPE)1000 100 g/L SM21-22 6200B34
m+p Xylene 160 200 g/L SM21-22 6200BJ60
Methyl tert-Butyl Ether (MTBE)8200 100 g/L SM21-22 6200B50
Naphthalene 880 1000 g/L SM21-22 6200BJ62
o-Xylene 100 100 g/L SM21-22 6200B34
tert-Amyl Methyl Ether (TAME)670 200 g/L SM21-22 6200BL-04 28
tert-Butyl Alcohol (TBA)13000 4000 g/L SM21-22 6200B830
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-02DCW-3
DL
1,2,4-Trimethylbenzene 640 25 g/L SM21-22 6200B9.0
1,3,5-Trimethylbenzene 120 25 g/L SM21-22 6200B7.0
Benzene 5900 25 g/L SM21-22 6200B9.0
Diisopropyl Ether (DIPE)140 25 g/L SM21-22 6200B8.5
Ethylbenzene 85 25 g/L SM21-22 6200B6.5
Isopropylbenzene (Cumene)33 25 g/L SM21-22 6200B8.5
m+p Xylene 1400 50 g/L SM21-22 6200B15
Methyl tert-Butyl Ether (MTBE)370 25 g/L SM21-22 6200B12
Naphthalene 260 250 g/L SM21-22 6200B16
n-Propylbenzene 45 25 g/L SM21-22 6200B6.5
o-Xylene 280 25 g/L SM21-22 6200B8.5
tert-Amyl Methyl Ether (TAME)66 50 g/L SM21-22 6200BL-04 7.0
tert-Butyl Alcohol (TBA)820 1000 g/L SM21-22 6200BJ210
Toluene 30 25 g/L SM21-22 6200B7.0
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-03DCW-4
DL
1,2,4-Trimethylbenzene 930 5.0 g/L SM21-22 6200B1.8
1,3,5-Trimethylbenzene 290 5.0 g/L SM21-22 6200B1.4
Benzene 2.5 5.0 g/L SM21-22 6200BJ1.8
Ethylbenzene 11 5.0 g/L SM21-22 6200B1.3
Isopropylbenzene (Cumene)42 5.0 g/L SM21-22 6200B1.7
m+p Xylene 270 10 g/L SM21-22 6200B3.0
Methyl tert-Butyl Ether (MTBE)4.7 5.0 g/L SM21-22 6200BJ2.5
Naphthalene 96 50 g/L SM21-22 6200B3.1
n-Butylbenzene 2.7 5.0 g/L SM21-22 6200BJ2.1
n-Propylbenzene 94 5.0 g/L SM21-22 6200B1.3
o-Xylene 140 5.0 g/L SM21-22 6200B1.7
p-Isopropyltoluene (p-Cymene)2.6 5.0 g/L SM21-22 6200BJ2.0
sec-Butylbenzene 2.4 5.0 g/L SM21-22 6200BJ1.6
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-04DCW-7
DL
1,2,4-Trimethylbenzene 0.22 0.50 g/L SM21-22 6200BJ0.18
Benzene 3.6 0.50 g/L SM21-22 6200B0.18
m+p Xylene 0.67 1.0 g/L SM21-22 6200BJ0.30
o-Xylene 0.52 0.50 g/L SM21-22 6200B0.17
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-06MW-1
DL
1,2,4-Trimethylbenzene 13 0.50 g/L SM21-22 6200B0.18
1,3,5-Trimethylbenzene 4.3 0.50 g/L SM21-22 6200B0.14
Benzene 0.28 0.50 g/L SM21-22 6200BJ0.18
Chloroform 0.19 0.50 g/L SM21-22 6200BJ0.17
Isopropylbenzene (Cumene)1.2 0.50 g/L SM21-22 6200B0.17
m+p Xylene 4.6 1.0 g/L SM21-22 6200B0.30
Methyl tert-Butyl Ether (MTBE)1.0 0.50 g/L SM21-22 6200B0.25
Naphthalene 5.1 5.0 g/L SM21-22 6200B0.31
n-Butylbenzene 0.75 0.50 g/L SM21-22 6200B0.21
n-Propylbenzene 2.7 0.50 g/L SM21-22 6200B0.13
o-Xylene 3.9 0.50 g/L SM21-22 6200B0.17
sec-Butylbenzene 0.60 0.50 g/L SM21-22 6200B0.16
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-07MW-2
DL
Acetone 5.5 50 g/L SM21-22 6200BJ3.8
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-08MW-3
DL
1,2,4-Trimethylbenzene 6.1 0.50 g/L SM21-22 6200B0.18
1,3,5-Trimethylbenzene 0.63 0.50 g/L SM21-22 6200B0.14
Isopropylbenzene (Cumene)0.19 0.50 g/L SM21-22 6200BJ0.17
m+p Xylene 1.3 1.0 g/L SM21-22 6200B0.30
n-Butylbenzene 0.36 0.50 g/L SM21-22 6200BJ0.21
n-Propylbenzene 0.37 0.50 g/L SM21-22 6200BJ0.13
o-Xylene 1.9 0.50 g/L SM21-22 6200B0.17
p-Isopropyltoluene (p-Cymene)0.30 0.50 g/L SM21-22 6200BJ0.20
sec-Butylbenzene 0.18 0.50 g/L SM21-22 6200BJ0.16
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-09MW-5
DL
1,2,4-Trimethylbenzene 2400 120 g/L SM21-22 6200B45
1,3,5-Trimethylbenzene 680 120 g/L SM21-22 6200B35
Benzene 270 120 g/L SM21-22 6200B45
Ethylbenzene 3000 120 g/L SM21-22 6200B32
Isopropylbenzene (Cumene)90 120 g/L SM21-22 6200BJ42
m+p Xylene 10000 250 g/L SM21-22 6200B75
Naphthalene 1300 1200 g/L SM21-22 6200B78
n-Propylbenzene 300 120 g/L SM21-22 6200B32
o-Xylene 4800 120 g/L SM21-22 6200B42
Styrene 92 120 g/L SM21-22 6200BJ28
Toluene 12000 120 g/L SM21-22 6200B35
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-12MW-9
DL
Acetone 7.6 50 g/L SM21-22 6200BJ3.8
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-13MW-12
DL
Acetone 3.9 50 g/L SM21-22 6200BJ3.8
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-14MW-14
DL
1,2,4-Trimethylbenzene 1800 250 g/L SM21-22 6200B90
1,3,5-Trimethylbenzene 530 250 g/L SM21-22 6200B70
2-Butanone (MEK)1700 2500 g/L SM21-22 6200BJ970
Benzene 10000 250 g/L SM21-22 6200B90
Diisopropyl Ether (DIPE)160 250 g/L SM21-22 6200BJ85
Ethylbenzene 3000 250 g/L SM21-22 6200B65
Isopropylbenzene (Cumene)95 250 g/L SM21-22 6200BJ85
m+p Xylene 9600 500 g/L SM21-22 6200B150
n-Propylbenzene 280 250 g/L SM21-22 6200B65
o-Xylene 4700 250 g/L SM21-22 6200B85
Toluene 32000 250 g/L SM21-22 6200B70
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-15MW-15
DL
1,2,4-Trimethylbenzene 1900 200 g/L SM21-22 6200B72
1,3,5-Trimethylbenzene 560 200 g/L SM21-22 6200B56
Benzene 840 200 g/L SM21-22 6200B72
Ethylbenzene 3000 200 g/L SM21-22 6200B52
Isopropylbenzene (Cumene)88 200 g/L SM21-22 6200BJ68
m+p Xylene 9800 400 g/L SM21-22 6200B120
n-Propylbenzene 280 200 g/L SM21-22 6200B52
o-Xylene 4700 200 g/L SM21-22 6200B68
Styrene 170 200 g/L SM21-22 6200BJ44
Toluene 29000 200 g/L SM21-22 6200B56
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-16MW-17
DL
1,2,4-Trimethylbenzene 1000 50 g/L SM21-22 6200B18
1,3,5-Trimethylbenzene 270 50 g/L SM21-22 6200B14
Benzene 61 50 g/L SM21-22 6200B18
Ethylbenzene 1800 50 g/L SM21-22 6200B13
Isopropylbenzene (Cumene)47 50 g/L SM21-22 6200BJ17
m+p Xylene 4500 100 g/L SM21-22 6200B30
Naphthalene 550 500 g/L SM21-22 6200B31
n-Propylbenzene 140 50 g/L SM21-22 6200B13
o-Xylene 1900 50 g/L SM21-22 6200B17
Styrene 19 50 g/L SM21-22 6200BJ11
Toluene 3500 50 g/L SM21-22 6200B14
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-17MW-18
DL
1,2,4-Trimethylbenzene 1800 50 g/L SM21-22 6200B18
1,3,5-Trimethylbenzene 530 50 g/L SM21-22 6200B14
Benzene 420 50 g/L SM21-22 6200B18
Ethylbenzene 2500 50 g/L SM21-22 6200B13
Isopropylbenzene (Cumene)76 50 g/L SM21-22 6200B17
m+p Xylene 2600 100 g/L SM21-22 6200B30
Naphthalene 690 500 g/L SM21-22 6200B31
n-Butylbenzene 31 50 g/L SM21-22 6200BJ21
n-Propylbenzene 250 50 g/L SM21-22 6200B13
o-Xylene 490 50 g/L SM21-22 6200B17
Toluene 2200 50 g/L SM21-22 6200B14
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-18MW-19
DL
1,2,4-Trimethylbenzene 1800 100 g/L SM21-22 6200B36
1,3,5-Trimethylbenzene 510 100 g/L SM21-22 6200B28
Ethylbenzene 2500 100 g/L SM21-22 6200B26
Isopropylbenzene (Cumene)76 100 g/L SM21-22 6200BJ34
m+p Xylene 6500 200 g/L SM21-22 6200B60
Naphthalene 980 1000 g/L SM21-22 6200BJ62
n-Butylbenzene 50 100 g/L SM21-22 6200BJ42
n-Propylbenzene 260 100 g/L SM21-22 6200B26
o-Xylene 1500 100 g/L SM21-22 6200B34
Styrene 36 100 g/L SM21-22 6200BJ22
Toluene 6300 100 g/L SM21-22 6200B28
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-19MW-20
DL
1,2,4-Trimethylbenzene 2300 200 g/L SM21-22 6200B72
1,3,5-Trimethylbenzene 650 200 g/L SM21-22 6200B56
Benzene 150 200 g/L SM21-22 6200BJ72
Ethylbenzene 3300 200 g/L SM21-22 6200B52
Isopropylbenzene (Cumene)92 200 g/L SM21-22 6200BJ68
m+p Xylene 10000 400 g/L SM21-22 6200B120
Naphthalene 1900 2000 g/L SM21-22 6200BJ120
n-Propylbenzene 320 200 g/L SM21-22 6200B52
o-Xylene 4200 200 g/L SM21-22 6200B68
Styrene 190 200 g/L SM21-22 6200BJ44
Toluene 23000 200 g/L SM21-22 6200B56
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-20MW-21
DL
1,2,4-Trimethylbenzene 2300 200 g/L SM21-22 6200B72
1,3,5-Trimethylbenzene 670 200 g/L SM21-22 6200B56
Benzene 3400 200 g/L SM21-22 6200B72
Ethylbenzene 3500 200 g/L SM21-22 6200B52
Isopropylbenzene (Cumene)100 200 g/L SM21-22 6200BJ68
m+p Xylene 11000 400 g/L SM21-22 6200B120
Naphthalene 1900 2000 g/L SM21-22 6200BJ120
n-Propylbenzene 320 200 g/L SM21-22 6200B52
o-Xylene 5300 200 g/L SM21-22 6200B68
Styrene 160 200 g/L SM21-22 6200BJ44
Toluene 28000 200 g/L SM21-22 6200B56
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-21MW-22
DL
1,2,4-Trimethylbenzene 1400 5.0 g/L SM21-22 6200B1.8
1,3,5-Trimethylbenzene 460 5.0 g/L SM21-22 6200B1.4
Benzene 130 5.0 g/L SM21-22 6200B1.8
Ethylbenzene 790 5.0 g/L SM21-22 6200B1.3
Isopropylbenzene (Cumene)74 5.0 g/L SM21-22 6200B1.7
m+p Xylene 630 10 g/L SM21-22 6200B3.0
Naphthalene 340 50 g/L SM21-22 6200B3.1
n-Butylbenzene 30 5.0 g/L SM21-22 6200B2.1
n-Propylbenzene 270 5.0 g/L SM21-22 6200B1.3
o-Xylene 150 5.0 g/L SM21-22 6200B1.7
p-Isopropyltoluene (p-Cymene)10 5.0 g/L SM21-22 6200B2.0
sec-Butylbenzene 14 5.0 g/L SM21-22 6200B1.6
tert-Butylbenzene 1.8 5.0 g/L SM21-22 6200BJ1.7
Toluene 82 5.0 g/L SM21-22 6200B1.4
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-22MW-24
DL
1,2,4-Trimethylbenzene 580 5.0 g/L SM21-22 6200B1.8
1,3,5-Trimethylbenzene 130 5.0 g/L SM21-22 6200B1.4
4-Methyl-2-pentanone (MIBK)45 50 g/L SM21-22 6200BJ17
Benzene 45 5.0 g/L SM21-22 6200B1.8
Ethylbenzene 380 5.0 g/L SM21-22 6200B1.3
Isopropylbenzene (Cumene)26 5.0 g/L SM21-22 6200B1.7
m+p Xylene 1300 10 g/L SM21-22 6200B3.0
Naphthalene 240 50 g/L SM21-22 6200B3.1
n-Butylbenzene 15 5.0 g/L SM21-22 6200B2.1
n-Propylbenzene 74 5.0 g/L SM21-22 6200B1.3
o-Xylene 810 5.0 g/L SM21-22 6200B1.7
p-Isopropyltoluene (p-Cymene)4.0 5.0 g/L SM21-22 6200BJ2.0
sec-Butylbenzene 5.4 5.0 g/L SM21-22 6200B1.6
Toluene 200 5.0 g/L SM21-22 6200B1.4
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-24MW-28
DL
Tetrachloroethylene 2.2 0.50 g/L SM21-22 6200B0.18
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0568-27WSW-1 Influent
DL
1,2,4-Trimethylbenzene 6.5 2.5 g/L SM21-22 6200B0.90
1,3,5-Trimethylbenzene 1.2 2.5 g/L SM21-22 6200BJ0.70
Benzene 13 2.5 g/L SM21-22 6200B0.90
Diisopropyl Ether (DIPE)88 2.5 g/L SM21-22 6200B0.85
Isopropylbenzene (Cumene)3.9 2.5 g/L SM21-22 6200B0.85
Methyl tert-Butyl Ether (MTBE)460 2.5 g/L SM21-22 6200B1.2
n-Butylbenzene 2.8 2.5 g/L SM21-22 6200B1.0
n-Propylbenzene 1.2 2.5 g/L SM21-22 6200BJ0.65
o-Xylene 11 2.5 g/L SM21-22 6200B0.85
sec-Butylbenzene 1.4 2.5 g/L SM21-22 6200BJ0.80
tert-Amyl Methyl Ether (TAME)55 5.0 g/L SM21-22 6200BL-04 0.70
tert-Butyl Alcohol (TBA)700 100 g/L SM21-22 6200B21
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 11 of 90
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method 6200B elevated reporting limits for samples 19K0568-01,02,03,09,14,15,16,17,18,19,20,21,22+27 due to high concentrations of target
compounds.
[TOC_1]Case Narrative[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
SM21-22 6200B
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not
affected since all results are "not detected" for associated samples in this batch and bias is on the high side.
Analyte & Samples(s) Qualified:
L-02
Vinyl Chloride
B245876-BS1, B245876-BSD1, B246118-BS1, B246118-BSD1
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
tert-Amyl Methyl Ether (TAME)
19K0568-01[DCW-2], 19K0568-02[DCW-3], 19K0568-03[DCW-4], 19K0568-04[DCW-7], 19K0568-05[Field Blank 11/6/19], 19K0568-06[MW-1], 19K0568-07[MW-2],
19K0568-08[MW-3], 19K0568-09[MW-5], 19K0568-10[MW-6], 19K0568-11[MW-7], 19K0568-12[MW-9], 19K0568-13[MW-12], 19K0568-14[MW-14],
19K0568-15[MW-15], 19K0568-16[MW-17], 19K0568-17[MW-18], 19K0568-18[MW-19], 19K0568-19[MW-20], 19K0568-20[MW-21], 19K0568-21[MW-22],
19K0568-22[MW-24], 19K0568-23[MW-25], 19K0568-24[MW-28], 19K0568-25[Field Blank 11/7/19], 19K0568-26[WSW-1 Effluent], 19K0568-27[WSW-1 Influent],
B245814-BLK1, B245814-BS1, B245814-BSD1, B245876-BLK1, B245876-BS1, B245876-BSD1, B246118-BLK1, B246118-BS1, B246118-BSD1
tert-Butyl Ethyl Ether (TBEE)
19K0568-01[DCW-2], 19K0568-02[DCW-3], 19K0568-03[DCW-4], 19K0568-04[DCW-7], 19K0568-05[Field Blank 11/6/19], 19K0568-06[MW-1], 19K0568-07[MW-2],
19K0568-08[MW-3], 19K0568-09[MW-5], 19K0568-10[MW-6], 19K0568-11[MW-7], 19K0568-12[MW-9], 19K0568-13[MW-12], 19K0568-14[MW-14],
19K0568-15[MW-15], 19K0568-16[MW-17], 19K0568-17[MW-18], 19K0568-18[MW-19], 19K0568-19[MW-20], 19K0568-20[MW-21], 19K0568-21[MW-22],
19K0568-22[MW-24], 19K0568-23[MW-25], 19K0568-24[MW-28], 19K0568-25[Field Blank 11/7/19], 19K0568-26[WSW-1 Effluent], 19K0568-27[WSW-1 Influent],
B245814-BLK1, B245814-BS1, B245814-BSD1, B245876-BLK1, B245876-BS1, B245876-BSD1, B246118-BLK1, B246118-BS1, B246118-BSD1
Vinyl Acetate
19K0568-14[MW-14], 19K0568-15[MW-15], 19K0568-20[MW-21], 19K0568-21[MW-22], 19K0568-22[MW-24], 19K0568-23[MW-25], 19K0568-24[MW-28],
19K0568-26[WSW-1 Effluent], 19K0568-27[WSW-1 Influent], B245876-BLK1, B245876-BS1, B245876-BSD1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
Naphthalene
B245814-BS1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
outside of control limits. Reduced precision anticipated for any reported result for this compound.
Analyte & Samples(s) Qualified:
L-07A
Ethanol
B246118-BSD1
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.Analyte & Samples(s) Qualified:
R-05
Ethanol
19K0568-05[Field Blank 11/6/19], 19K0568-25[Field Blank 11/7/19], B246118-BLK1, B246118-BS1, B246118-BSD1, S042679-CCV1
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
RL-11
19K0568-01[DCW-2], 19K0568-02[DCW-3], 19K0568-03[DCW-4], 19K0568-09[MW-5], 19K0568-14[MW-14], 19K0568-15[MW-15], 19K0568-16[MW-17],
19K0568-17[MW-18], 19K0568-18[MW-19], 19K0568-19[MW-20], 19K0568-20[MW-21], 19K0568-21[MW-22], 19K0568-22[MW-24], 19K0568-27[WSW-1 Influent]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 14 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-01
Field Sample #: DCW-2
Sample Matrix: Ground Water
Sampled: 11/6/2019 15:55
[TOC_2]19K0568-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 10000 11/16/19 5:04 EEHg/L760 11/12/19SM21-22 6200B200Acetone
670 200 11/16/19 5:04 EEHg/L28 11/12/19SM21-22 6200B200L-04tert-Amyl Methyl Ether (TAME)
2400 100 11/16/19 5:04 EEHg/L36 11/12/19SM21-22 6200B200Benzene
ND 100 11/16/19 5:04 EEHg/L30 11/12/19SM21-22 6200B200Bromobenzene
ND 100 11/16/19 5:04 EEHg/L64 11/12/19SM21-22 6200B200Bromochloromethane
ND 100 11/16/19 5:04 EEHg/L32 11/12/19SM21-22 6200B200Bromodichloromethane
ND 100 11/16/19 5:04 EEHg/L92 11/12/19SM21-22 6200B200Bromoform
ND 200 11/16/19 5:04 EEHg/L160 11/12/19SM21-22 6200B200Bromomethane
ND 1000 11/16/19 5:04 EEHg/L390 11/12/19SM21-22 6200B2002-Butanone (MEK)
13000 4000 11/16/19 5:04 EEHg/L830 11/12/19SM21-22 6200B200tert-Butyl Alcohol (TBA)
ND 100 11/16/19 5:04 EEHg/L42 11/12/19SM21-22 6200B200n-Butylbenzene
ND 100 11/16/19 5:04 EEHg/L32 11/12/19SM21-22 6200B200sec-Butylbenzene
ND 100 11/16/19 5:04 EEHg/L34 11/12/19SM21-22 6200B200tert-Butylbenzene
ND 100 11/16/19 5:04 EEHg/L32 11/12/19SM21-22 6200B200L-04tert-Butyl Ethyl Ether (TBEE)
ND 100 11/16/19 5:04 EEHg/L22 11/12/19SM21-22 6200B200Carbon Tetrachloride
ND 100 11/16/19 5:04 EEHg/L30 11/12/19SM21-22 6200B200Chlorobenzene
ND 10000 11/16/19 5:04 EEHg/L2100 11/12/19SM21-22 6200B200Ethanol
ND 100 11/16/19 5:04 EEHg/L42 11/12/19SM21-22 6200B200Chlorodibromomethane
ND 100 11/16/19 5:04 EEHg/L70 11/12/19SM21-22 6200B200Chloroethane
ND 100 11/16/19 5:04 EEHg/L34 11/12/19SM21-22 6200B200Chloroform
ND 200 11/16/19 5:04 EEHg/L90 11/12/19SM21-22 6200B200Chloromethane
ND 100 11/16/19 5:04 EEHg/L24 11/12/19SM21-22 6200B2002-Chlorotoluene
ND 100 11/16/19 5:04 EEHg/L28 11/12/19SM21-22 6200B2004-Chlorotoluene
ND 100 11/16/19 5:04 EEHg/L38 11/12/19SM21-22 6200B2001,2-Dibromoethane (EDB)
ND 100 11/16/19 5:04 EEHg/L32 11/12/19SM21-22 6200B2001,2-Dichlorobenzene
ND 100 11/16/19 5:04 EEHg/L24 11/12/19SM21-22 6200B2001,3-Dichlorobenzene
ND 100 11/16/19 5:04 EEHg/L26 11/12/19SM21-22 6200B2001,4-Dichlorobenzene
ND 100 11/16/19 5:04 EEHg/L52 11/12/19SM21-22 6200B200Dichlorodifluoromethane (Freon 12)
ND 100 11/16/19 5:04 EEHg/L32 11/12/19SM21-22 6200B2001,1-Dichloroethane
ND 200 11/16/19 5:04 EEHg/L82 11/12/19SM21-22 6200B2001,2-Dichloroethane
ND 100 11/16/19 5:04 EEHg/L64 11/12/19SM21-22 6200B2001,1-Dichloroethylene
ND 100 11/16/19 5:04 EEHg/L26 11/12/19SM21-22 6200B200cis-1,2-Dichloroethylene
ND 100 11/16/19 5:04 EEHg/L62 11/12/19SM21-22 6200B200trans-1,2-Dichloroethylene
ND 100 11/16/19 5:04 EEHg/L40 11/12/19SM21-22 6200B2001,2-Dichloropropane
ND 100 11/16/19 5:04 EEHg/L22 11/12/19SM21-22 6200B2001,3-Dichloropropane
ND 100 11/16/19 5:04 EEHg/L40 11/12/19SM21-22 6200B2002,2-Dichloropropane
ND 100 11/16/19 5:04 EEHg/L32 11/12/19SM21-22 6200B2001,1-Dichloropropene
ND 100 11/16/19 5:04 EEHg/L26 11/12/19SM21-22 6200B200cis-1,3-Dichloropropene
ND 100 11/16/19 5:04 EEHg/L46 11/12/19SM21-22 6200B200trans-1,3-Dichloropropene
1000 100 11/16/19 5:04 EEHg/L34 11/12/19SM21-22 6200B200Diisopropyl Ether (DIPE)
ND 100 11/16/19 5:04 EEHg/L26 11/12/19SM21-22 6200B200Ethylbenzene
ND 1000 11/16/19 5:04 EEHg/L300 11/12/19SM21-22 6200B2002-Hexanone (MBK)
ND 100 11/16/19 5:04 EEHg/L34 11/12/19SM21-22 6200B200Isopropylbenzene (Cumene)
ND 100 11/16/19 5:04 EEHg/L40 11/12/19SM21-22 6200B200p-Isopropyltoluene (p-Cymene)
[TOC_1]Sample Results[TOC]
Page 15 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-01
Field Sample #: DCW-2
Sample Matrix: Ground Water
Sampled: 11/6/2019 15:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
8200 100 11/16/19 5:04 EEHg/L50 11/12/19SM21-22 6200B200Methyl tert-Butyl Ether (MTBE)
ND 1000 11/16/19 5:04 EEHg/L68 11/12/19SM21-22 6200B200Methylene Chloride
ND 1000 11/16/19 5:04 EEHg/L330 11/12/19SM21-22 6200B2004-Methyl-2-pentanone (MIBK)
880 1000 11/16/19 5:04 EEHg/L62 11/12/19SM21-22 6200B200JNaphthalene
ND 100 11/16/19 5:04 EEHg/L26 11/12/19SM21-22 6200B200n-Propylbenzene
ND 100 11/16/19 5:04 EEHg/L22 11/12/19SM21-22 6200B200Styrene
ND 100 11/16/19 5:04 EEHg/L54 11/12/19SM21-22 6200B2001,1,1,2-Tetrachloroethane
ND 100 11/16/19 5:04 EEHg/L44 11/12/19SM21-22 6200B2001,1,2,2-Tetrachloroethane
ND 100 11/16/19 5:04 EEHg/L36 11/12/19SM21-22 6200B200Tetrachloroethylene
ND 100 11/16/19 5:04 EEHg/L28 11/12/19SM21-22 6200B200Toluene
ND 400 11/16/19 5:04 EEHg/L110 11/12/19SM21-22 6200B2001,2,3-Trichlorobenzene
ND 100 11/16/19 5:04 EEHg/L80 11/12/19SM21-22 6200B2001,2,4-Trichlorobenzene
ND 100 11/16/19 5:04 EEHg/L40 11/12/19SM21-22 6200B2001,1,1-Trichloroethane
ND 100 11/16/19 5:04 EEHg/L32 11/12/19SM21-22 6200B2001,1,2-Trichloroethane
ND 100 11/16/19 5:04 EEHg/L48 11/12/19SM21-22 6200B200Trichloroethylene
ND 100 11/16/19 5:04 EEHg/L66 11/12/19SM21-22 6200B200Trichlorofluoromethane (Freon 11)
ND 100 11/16/19 5:04 EEHg/L50 11/12/19SM21-22 6200B2001,2,3-Trichloropropane
230 100 11/16/19 5:04 EEHg/L36 11/12/19SM21-22 6200B2001,2,4-Trimethylbenzene
52 100 11/16/19 5:04 EEHg/L28 11/12/19SM21-22 6200B200J1,3,5-Trimethylbenzene
ND 4000 11/16/19 5:04 EEHg/L2000 11/12/19SM21-22 6200B200Vinyl Acetate
ND 100 11/16/19 5:04 EEHg/L90 11/12/19SM21-22 6200B200Vinyl Chloride
160 200 11/16/19 5:04 EEHg/L60 11/12/19SM21-22 6200B200Jm+p Xylene
100 100 11/16/19 5:04 EEHg/L34 11/12/19SM21-22 6200B200o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 88.6 11/16/19 5:0470-130
Toluene-d8 96.2 11/16/19 5:0470-130
4-Bromofluorobenzene 97.6 11/16/19 5:0470-130
Page 16 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-02
Field Sample #: DCW-3
Sample Matrix: Ground Water
Sampled: 11/6/2019 16:35
[TOC_2]19K0568-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 2500 11/16/19 4:35 EEHg/L190 11/12/19SM21-22 6200B50Acetone
66 50 11/16/19 4:35 EEHg/L7.0 11/12/19SM21-22 6200B50L-04tert-Amyl Methyl Ether (TAME)
5900 25 11/16/19 4:35 EEHg/L9.0 11/12/19SM21-22 6200B50Benzene
ND 25 11/16/19 4:35 EEHg/L7.5 11/12/19SM21-22 6200B50Bromobenzene
ND 25 11/16/19 4:35 EEHg/L16 11/12/19SM21-22 6200B50Bromochloromethane
ND 25 11/16/19 4:35 EEHg/L8.0 11/12/19SM21-22 6200B50Bromodichloromethane
ND 25 11/16/19 4:35 EEHg/L23 11/12/19SM21-22 6200B50Bromoform
ND 50 11/16/19 4:35 EEHg/L39 11/12/19SM21-22 6200B50Bromomethane
ND 250 11/16/19 4:35 EEHg/L97 11/12/19SM21-22 6200B502-Butanone (MEK)
820 1000 11/16/19 4:35 EEHg/L210 11/12/19SM21-22 6200B50Jtert-Butyl Alcohol (TBA)
ND 25 11/16/19 4:35 EEHg/L10 11/12/19SM21-22 6200B50n-Butylbenzene
ND 25 11/16/19 4:35 EEHg/L8.0 11/12/19SM21-22 6200B50sec-Butylbenzene
ND 25 11/16/19 4:35 EEHg/L8.5 11/12/19SM21-22 6200B50tert-Butylbenzene
ND 25 11/16/19 4:35 EEHg/L8.0 11/12/19SM21-22 6200B50L-04tert-Butyl Ethyl Ether (TBEE)
ND 25 11/16/19 4:35 EEHg/L5.5 11/12/19SM21-22 6200B50Carbon Tetrachloride
ND 25 11/16/19 4:35 EEHg/L7.5 11/12/19SM21-22 6200B50Chlorobenzene
ND 2500 11/16/19 4:35 EEHg/L530 11/12/19SM21-22 6200B50Ethanol
ND 25 11/16/19 4:35 EEHg/L10 11/12/19SM21-22 6200B50Chlorodibromomethane
ND 25 11/16/19 4:35 EEHg/L18 11/12/19SM21-22 6200B50Chloroethane
ND 25 11/16/19 4:35 EEHg/L8.5 11/12/19SM21-22 6200B50Chloroform
ND 50 11/16/19 4:35 EEHg/L22 11/12/19SM21-22 6200B50Chloromethane
ND 25 11/16/19 4:35 EEHg/L6.0 11/12/19SM21-22 6200B502-Chlorotoluene
ND 25 11/16/19 4:35 EEHg/L7.0 11/12/19SM21-22 6200B504-Chlorotoluene
ND 25 11/16/19 4:35 EEHg/L9.5 11/12/19SM21-22 6200B501,2-Dibromoethane (EDB)
ND 25 11/16/19 4:35 EEHg/L8.0 11/12/19SM21-22 6200B501,2-Dichlorobenzene
ND 25 11/16/19 4:35 EEHg/L6.0 11/12/19SM21-22 6200B501,3-Dichlorobenzene
ND 25 11/16/19 4:35 EEHg/L6.5 11/12/19SM21-22 6200B501,4-Dichlorobenzene
ND 25 11/16/19 4:35 EEHg/L13 11/12/19SM21-22 6200B50Dichlorodifluoromethane (Freon 12)
ND 25 11/16/19 4:35 EEHg/L8.0 11/12/19SM21-22 6200B501,1-Dichloroethane
ND 50 11/16/19 4:35 EEHg/L20 11/12/19SM21-22 6200B501,2-Dichloroethane
ND 25 11/16/19 4:35 EEHg/L16 11/12/19SM21-22 6200B501,1-Dichloroethylene
ND 25 11/16/19 4:35 EEHg/L6.5 11/12/19SM21-22 6200B50cis-1,2-Dichloroethylene
ND 25 11/16/19 4:35 EEHg/L16 11/12/19SM21-22 6200B50trans-1,2-Dichloroethylene
ND 25 11/16/19 4:35 EEHg/L10 11/12/19SM21-22 6200B501,2-Dichloropropane
ND 25 11/16/19 4:35 EEHg/L5.5 11/12/19SM21-22 6200B501,3-Dichloropropane
ND 25 11/16/19 4:35 EEHg/L10 11/12/19SM21-22 6200B502,2-Dichloropropane
ND 25 11/16/19 4:35 EEHg/L8.0 11/12/19SM21-22 6200B501,1-Dichloropropene
ND 25 11/16/19 4:35 EEHg/L6.5 11/12/19SM21-22 6200B50cis-1,3-Dichloropropene
ND 25 11/16/19 4:35 EEHg/L12 11/12/19SM21-22 6200B50trans-1,3-Dichloropropene
140 25 11/16/19 4:35 EEHg/L8.5 11/12/19SM21-22 6200B50Diisopropyl Ether (DIPE)
85 25 11/16/19 4:35 EEHg/L6.5 11/12/19SM21-22 6200B50Ethylbenzene
ND 250 11/16/19 4:35 EEHg/L76 11/12/19SM21-22 6200B502-Hexanone (MBK)
33 25 11/16/19 4:35 EEHg/L8.5 11/12/19SM21-22 6200B50Isopropylbenzene (Cumene)
ND 25 11/16/19 4:35 EEHg/L10 11/12/19SM21-22 6200B50p-Isopropyltoluene (p-Cymene)
Page 17 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-02
Field Sample #: DCW-3
Sample Matrix: Ground Water
Sampled: 11/6/2019 16:35
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
370 25 11/16/19 4:35 EEHg/L12 11/12/19SM21-22 6200B50Methyl tert-Butyl Ether (MTBE)
ND 250 11/16/19 4:35 EEHg/L17 11/12/19SM21-22 6200B50Methylene Chloride
ND 250 11/16/19 4:35 EEHg/L84 11/12/19SM21-22 6200B504-Methyl-2-pentanone (MIBK)
260 250 11/16/19 4:35 EEHg/L16 11/12/19SM21-22 6200B50Naphthalene
45 25 11/16/19 4:35 EEHg/L6.5 11/12/19SM21-22 6200B50n-Propylbenzene
ND 25 11/16/19 4:35 EEHg/L5.5 11/12/19SM21-22 6200B50Styrene
ND 25 11/16/19 4:35 EEHg/L14 11/12/19SM21-22 6200B501,1,1,2-Tetrachloroethane
ND 25 11/16/19 4:35 EEHg/L11 11/12/19SM21-22 6200B501,1,2,2-Tetrachloroethane
ND 25 11/16/19 4:35 EEHg/L9.0 11/12/19SM21-22 6200B50Tetrachloroethylene
30 25 11/16/19 4:35 EEHg/L7.0 11/12/19SM21-22 6200B50Toluene
ND 100 11/16/19 4:35 EEHg/L28 11/12/19SM21-22 6200B501,2,3-Trichlorobenzene
ND 25 11/16/19 4:35 EEHg/L20 11/12/19SM21-22 6200B501,2,4-Trichlorobenzene
ND 25 11/16/19 4:35 EEHg/L10 11/12/19SM21-22 6200B501,1,1-Trichloroethane
ND 25 11/16/19 4:35 EEHg/L8.0 11/12/19SM21-22 6200B501,1,2-Trichloroethane
ND 25 11/16/19 4:35 EEHg/L12 11/12/19SM21-22 6200B50Trichloroethylene
ND 25 11/16/19 4:35 EEHg/L16 11/12/19SM21-22 6200B50Trichlorofluoromethane (Freon 11)
ND 25 11/16/19 4:35 EEHg/L12 11/12/19SM21-22 6200B501,2,3-Trichloropropane
640 25 11/16/19 4:35 EEHg/L9.0 11/12/19SM21-22 6200B501,2,4-Trimethylbenzene
120 25 11/16/19 4:35 EEHg/L7.0 11/12/19SM21-22 6200B501,3,5-Trimethylbenzene
ND 1000 11/16/19 4:35 EEHg/L510 11/12/19SM21-22 6200B50Vinyl Acetate
ND 25 11/16/19 4:35 EEHg/L22 11/12/19SM21-22 6200B50Vinyl Chloride
1400 50 11/16/19 4:35 EEHg/L15 11/12/19SM21-22 6200B50m+p Xylene
280 25 11/16/19 4:35 EEHg/L8.5 11/12/19SM21-22 6200B50o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 87.6 11/16/19 4:3570-130
Toluene-d8 98.6 11/16/19 4:3570-130
4-Bromofluorobenzene 98.8 11/16/19 4:3570-130
Page 18 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-03
Field Sample #: DCW-4
Sample Matrix: Ground Water
Sampled: 11/6/2019 17:15
[TOC_2]19K0568-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 500 11/16/19 4:07 EEHg/L38 11/12/19SM21-22 6200B10Acetone
ND 10 11/16/19 4:07 EEHg/L1.4 11/12/19SM21-22 6200B10L-04tert-Amyl Methyl Ether (TAME)
2.5 5.0 11/16/19 4:07 EEHg/L1.8 11/12/19SM21-22 6200B10JBenzene
ND 5.0 11/16/19 4:07 EEHg/L1.5 11/12/19SM21-22 6200B10Bromobenzene
ND 5.0 11/16/19 4:07 EEHg/L3.2 11/12/19SM21-22 6200B10Bromochloromethane
ND 5.0 11/16/19 4:07 EEHg/L1.6 11/12/19SM21-22 6200B10Bromodichloromethane
ND 5.0 11/16/19 4:07 EEHg/L4.6 11/12/19SM21-22 6200B10Bromoform
ND 10 11/16/19 4:07 EEHg/L7.8 11/12/19SM21-22 6200B10Bromomethane
ND 50 11/16/19 4:07 EEHg/L19 11/12/19SM21-22 6200B102-Butanone (MEK)
ND 200 11/16/19 4:07 EEHg/L42 11/12/19SM21-22 6200B10tert-Butyl Alcohol (TBA)
2.7 5.0 11/16/19 4:07 EEHg/L2.1 11/12/19SM21-22 6200B10Jn-Butylbenzene
2.4 5.0 11/16/19 4:07 EEHg/L1.6 11/12/19SM21-22 6200B10Jsec-Butylbenzene
ND 5.0 11/16/19 4:07 EEHg/L1.7 11/12/19SM21-22 6200B10tert-Butylbenzene
ND 5.0 11/16/19 4:07 EEHg/L1.6 11/12/19SM21-22 6200B10L-04tert-Butyl Ethyl Ether (TBEE)
ND 5.0 11/16/19 4:07 EEHg/L1.1 11/12/19SM21-22 6200B10Carbon Tetrachloride
ND 5.0 11/16/19 4:07 EEHg/L1.5 11/12/19SM21-22 6200B10Chlorobenzene
ND 500 11/16/19 4:07 EEHg/L110 11/12/19SM21-22 6200B10Ethanol
ND 5.0 11/16/19 4:07 EEHg/L2.1 11/12/19SM21-22 6200B10Chlorodibromomethane
ND 5.0 11/16/19 4:07 EEHg/L3.5 11/12/19SM21-22 6200B10Chloroethane
ND 5.0 11/16/19 4:07 EEHg/L1.7 11/12/19SM21-22 6200B10Chloroform
ND 10 11/16/19 4:07 EEHg/L4.5 11/12/19SM21-22 6200B10Chloromethane
ND 5.0 11/16/19 4:07 EEHg/L1.2 11/12/19SM21-22 6200B102-Chlorotoluene
ND 5.0 11/16/19 4:07 EEHg/L1.4 11/12/19SM21-22 6200B104-Chlorotoluene
ND 5.0 11/16/19 4:07 EEHg/L1.9 11/12/19SM21-22 6200B101,2-Dibromoethane (EDB)
ND 5.0 11/16/19 4:07 EEHg/L1.6 11/12/19SM21-22 6200B101,2-Dichlorobenzene
ND 5.0 11/16/19 4:07 EEHg/L1.2 11/12/19SM21-22 6200B101,3-Dichlorobenzene
ND 5.0 11/16/19 4:07 EEHg/L1.3 11/12/19SM21-22 6200B101,4-Dichlorobenzene
ND 5.0 11/16/19 4:07 EEHg/L2.6 11/12/19SM21-22 6200B10Dichlorodifluoromethane (Freon 12)
ND 5.0 11/16/19 4:07 EEHg/L1.6 11/12/19SM21-22 6200B101,1-Dichloroethane
ND 10 11/16/19 4:07 EEHg/L4.1 11/12/19SM21-22 6200B101,2-Dichloroethane
ND 5.0 11/16/19 4:07 EEHg/L3.2 11/12/19SM21-22 6200B101,1-Dichloroethylene
ND 5.0 11/16/19 4:07 EEHg/L1.3 11/12/19SM21-22 6200B10cis-1,2-Dichloroethylene
ND 5.0 11/16/19 4:07 EEHg/L3.1 11/12/19SM21-22 6200B10trans-1,2-Dichloroethylene
ND 5.0 11/16/19 4:07 EEHg/L2.0 11/12/19SM21-22 6200B101,2-Dichloropropane
ND 5.0 11/16/19 4:07 EEHg/L1.1 11/12/19SM21-22 6200B101,3-Dichloropropane
ND 5.0 11/16/19 4:07 EEHg/L2.0 11/12/19SM21-22 6200B102,2-Dichloropropane
ND 5.0 11/16/19 4:07 EEHg/L1.6 11/12/19SM21-22 6200B101,1-Dichloropropene
ND 5.0 11/16/19 4:07 EEHg/L1.3 11/12/19SM21-22 6200B10cis-1,3-Dichloropropene
ND 5.0 11/16/19 4:07 EEHg/L2.3 11/12/19SM21-22 6200B10trans-1,3-Dichloropropene
ND 5.0 11/16/19 4:07 EEHg/L1.7 11/12/19SM21-22 6200B10Diisopropyl Ether (DIPE)
11 5.0 11/16/19 4:07 EEHg/L1.3 11/12/19SM21-22 6200B10Ethylbenzene
ND 50 11/16/19 4:07 EEHg/L15 11/12/19SM21-22 6200B102-Hexanone (MBK)
42 5.0 11/16/19 4:07 EEHg/L1.7 11/12/19SM21-22 6200B10Isopropylbenzene (Cumene)
2.6 5.0 11/16/19 4:07 EEHg/L2.0 11/12/19SM21-22 6200B10Jp-Isopropyltoluene (p-Cymene)
Page 19 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-03
Field Sample #: DCW-4
Sample Matrix: Ground Water
Sampled: 11/6/2019 17:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
4.7 5.0 11/16/19 4:07 EEHg/L2.5 11/12/19SM21-22 6200B10JMethyl tert-Butyl Ether (MTBE)
ND 50 11/16/19 4:07 EEHg/L3.4 11/12/19SM21-22 6200B10Methylene Chloride
ND 50 11/16/19 4:07 EEHg/L17 11/12/19SM21-22 6200B104-Methyl-2-pentanone (MIBK)
96 50 11/16/19 4:07 EEHg/L3.1 11/12/19SM21-22 6200B10Naphthalene
94 5.0 11/16/19 4:07 EEHg/L1.3 11/12/19SM21-22 6200B10n-Propylbenzene
ND 5.0 11/16/19 4:07 EEHg/L1.1 11/12/19SM21-22 6200B10Styrene
ND 5.0 11/16/19 4:07 EEHg/L2.7 11/12/19SM21-22 6200B101,1,1,2-Tetrachloroethane
ND 5.0 11/16/19 4:07 EEHg/L2.2 11/12/19SM21-22 6200B101,1,2,2-Tetrachloroethane
ND 5.0 11/16/19 4:07 EEHg/L1.8 11/12/19SM21-22 6200B10Tetrachloroethylene
ND 5.0 11/16/19 4:07 EEHg/L1.4 11/12/19SM21-22 6200B10Toluene
ND 20 11/16/19 4:07 EEHg/L5.7 11/12/19SM21-22 6200B101,2,3-Trichlorobenzene
ND 5.0 11/16/19 4:07 EEHg/L4.0 11/12/19SM21-22 6200B101,2,4-Trichlorobenzene
ND 5.0 11/16/19 4:07 EEHg/L2.0 11/12/19SM21-22 6200B101,1,1-Trichloroethane
ND 5.0 11/16/19 4:07 EEHg/L1.6 11/12/19SM21-22 6200B101,1,2-Trichloroethane
ND 5.0 11/16/19 4:07 EEHg/L2.4 11/12/19SM21-22 6200B10Trichloroethylene
ND 5.0 11/16/19 4:07 EEHg/L3.3 11/12/19SM21-22 6200B10Trichlorofluoromethane (Freon 11)
ND 5.0 11/16/19 4:07 EEHg/L2.5 11/12/19SM21-22 6200B101,2,3-Trichloropropane
930 5.0 11/16/19 4:07 EEHg/L1.8 11/12/19SM21-22 6200B101,2,4-Trimethylbenzene
290 5.0 11/16/19 4:07 EEHg/L1.4 11/12/19SM21-22 6200B101,3,5-Trimethylbenzene
ND 200 11/16/19 4:07 EEHg/L100 11/12/19SM21-22 6200B10Vinyl Acetate
ND 5.0 11/16/19 4:07 EEHg/L4.5 11/12/19SM21-22 6200B10Vinyl Chloride
270 10 11/16/19 4:07 EEHg/L3.0 11/12/19SM21-22 6200B10m+p Xylene
140 5.0 11/16/19 4:07 EEHg/L1.7 11/12/19SM21-22 6200B10o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 91.7 11/16/19 4:0770-130
Toluene-d8 99.8 11/16/19 4:0770-130
4-Bromofluorobenzene 106 11/16/19 4:0770-130
Page 20 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-04
Field Sample #: DCW-7
Sample Matrix: Ground Water
Sampled: 11/6/2019 17:55
[TOC_2]19K0568-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/16/19 3:09 EEHg/L3.8 11/12/19SM21-22 6200B1Acetone
ND 1.0 11/16/19 3:09 EEHg/L0.14 11/12/19SM21-22 6200B1L-04tert-Amyl Methyl Ether (TAME)
3.6 0.50 11/16/19 3:09 EEHg/L0.18 11/12/19SM21-22 6200B1Benzene
ND 0.50 11/16/19 3:09 EEHg/L0.15 11/12/19SM21-22 6200B1Bromobenzene
ND 0.50 11/16/19 3:09 EEHg/L0.32 11/12/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/16/19 3:09 EEHg/L0.16 11/12/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/16/19 3:09 EEHg/L0.46 11/12/19SM21-22 6200B1Bromoform
ND 1.0 11/16/19 3:09 EEHg/L0.78 11/12/19SM21-22 6200B1Bromomethane
ND 5.0 11/16/19 3:09 EEHg/L1.9 11/12/19SM21-22 6200B12-Butanone (MEK)
ND 20 11/16/19 3:09 EEHg/L4.2 11/12/19SM21-22 6200B1tert-Butyl Alcohol (TBA)
ND 0.50 11/16/19 3:09 EEHg/L0.21 11/12/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/16/19 3:09 EEHg/L0.16 11/12/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/16/19 3:09 EEHg/L0.17 11/12/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/16/19 3:09 EEHg/L0.16 11/12/19SM21-22 6200B1L-04tert-Butyl Ethyl Ether (TBEE)
ND 0.50 11/16/19 3:09 EEHg/L0.11 11/12/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/16/19 3:09 EEHg/L0.15 11/12/19SM21-22 6200B1Chlorobenzene
ND 50 11/16/19 3:09 EEHg/L11 11/12/19SM21-22 6200B1Ethanol
ND 0.50 11/16/19 3:09 EEHg/L0.21 11/12/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/16/19 3:09 EEHg/L0.35 11/12/19SM21-22 6200B1Chloroethane
ND 0.50 11/16/19 3:09 EEHg/L0.17 11/12/19SM21-22 6200B1Chloroform
ND 1.0 11/16/19 3:09 EEHg/L0.45 11/12/19SM21-22 6200B1Chloromethane
ND 0.50 11/16/19 3:09 EEHg/L0.12 11/12/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/16/19 3:09 EEHg/L0.14 11/12/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/16/19 3:09 EEHg/L0.19 11/12/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/16/19 3:09 EEHg/L0.16 11/12/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/16/19 3:09 EEHg/L0.12 11/12/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/16/19 3:09 EEHg/L0.13 11/12/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/16/19 3:09 EEHg/L0.26 11/12/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/16/19 3:09 EEHg/L0.16 11/12/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/16/19 3:09 EEHg/L0.41 11/12/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/16/19 3:09 EEHg/L0.32 11/12/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/16/19 3:09 EEHg/L0.13 11/12/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/16/19 3:09 EEHg/L0.31 11/12/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/16/19 3:09 EEHg/L0.20 11/12/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/16/19 3:09 EEHg/L0.11 11/12/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/16/19 3:09 EEHg/L0.20 11/12/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/16/19 3:09 EEHg/L0.16 11/12/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/16/19 3:09 EEHg/L0.13 11/12/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/16/19 3:09 EEHg/L0.23 11/12/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/16/19 3:09 EEHg/L0.17 11/12/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/16/19 3:09 EEHg/L0.13 11/12/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/16/19 3:09 EEHg/L1.5 11/12/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/16/19 3:09 EEHg/L0.17 11/12/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/16/19 3:09 EEHg/L0.20 11/12/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
Page 21 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-04
Field Sample #: DCW-7
Sample Matrix: Ground Water
Sampled: 11/6/2019 17:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 11/16/19 3:09 EEHg/L0.25 11/12/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/16/19 3:09 EEHg/L0.34 11/12/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/16/19 3:09 EEHg/L1.7 11/12/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 11/16/19 3:09 EEHg/L0.31 11/12/19SM21-22 6200B1Naphthalene
ND 0.50 11/16/19 3:09 EEHg/L0.13 11/12/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/16/19 3:09 EEHg/L0.11 11/12/19SM21-22 6200B1Styrene
ND 0.50 11/16/19 3:09 EEHg/L0.27 11/12/19SM21-22 6200B11,1,1,2-Tetrachloroethane
ND 0.50 11/16/19 3:09 EEHg/L0.22 11/12/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/16/19 3:09 EEHg/L0.18 11/12/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/16/19 3:09 EEHg/L0.14 11/12/19SM21-22 6200B1Toluene
ND 2.0 11/16/19 3:09 EEHg/L0.57 11/12/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/16/19 3:09 EEHg/L0.40 11/12/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/16/19 3:09 EEHg/L0.20 11/12/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/16/19 3:09 EEHg/L0.16 11/12/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/16/19 3:09 EEHg/L0.24 11/12/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/16/19 3:09 EEHg/L0.33 11/12/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/16/19 3:09 EEHg/L0.25 11/12/19SM21-22 6200B11,2,3-Trichloropropane
0.22 0.50 11/16/19 3:09 EEHg/L0.18 11/12/19SM21-22 6200B1J1,2,4-Trimethylbenzene
ND 0.50 11/16/19 3:09 EEHg/L0.14 11/12/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/16/19 3:09 EEHg/L10 11/12/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/16/19 3:09 EEHg/L0.45 11/12/19SM21-22 6200B1Vinyl Chloride
0.67 1.0 11/16/19 3:09 EEHg/L0.30 11/12/19SM21-22 6200B1Jm+p Xylene
0.52 0.50 11/16/19 3:09 EEHg/L0.17 11/12/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 86.9 11/16/19 3:0970-130
Toluene-d8 97.2 11/16/19 3:0970-130
4-Bromofluorobenzene 99.6 11/16/19 3:0970-130
Page 22 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-05
Field Sample #: Field Blank 11/6/19
Sample Matrix: Field Blank
Sampled: 11/6/2019 18:00
[TOC_2]19K0568-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/15/19 0:57 EEHg/L3.8 11/14/19SM21-22 6200B1Acetone
ND 1.0 11/15/19 0:57 EEHg/L0.14 11/14/19SM21-22 6200B1L-04tert-Amyl Methyl Ether (TAME)
ND 0.50 11/15/19 0:57 EEHg/L0.18 11/14/19SM21-22 6200B1Benzene
ND 0.50 11/15/19 0:57 EEHg/L0.15 11/14/19SM21-22 6200B1Bromobenzene
ND 0.50 11/15/19 0:57 EEHg/L0.32 11/14/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/15/19 0:57 EEHg/L0.16 11/14/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/15/19 0:57 EEHg/L0.46 11/14/19SM21-22 6200B1Bromoform
ND 1.0 11/15/19 0:57 EEHg/L0.78 11/14/19SM21-22 6200B1Bromomethane
ND 5.0 11/15/19 0:57 EEHg/L1.9 11/14/19SM21-22 6200B12-Butanone (MEK)
ND 20 11/15/19 0:57 EEHg/L4.2 11/14/19SM21-22 6200B1tert-Butyl Alcohol (TBA)
ND 0.50 11/15/19 0:57 EEHg/L0.21 11/14/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/15/19 0:57 EEHg/L0.16 11/14/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/15/19 0:57 EEHg/L0.17 11/14/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/15/19 0:57 EEHg/L0.16 11/14/19SM21-22 6200B1L-04tert-Butyl Ethyl Ether (TBEE)
ND 0.50 11/15/19 0:57 EEHg/L0.11 11/14/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/15/19 0:57 EEHg/L0.15 11/14/19SM21-22 6200B1Chlorobenzene
ND 50 11/15/19 0:57 EEHg/L11 11/14/19SM21-22 6200B1R-05Ethanol
ND 0.50 11/15/19 0:57 EEHg/L0.21 11/14/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/15/19 0:57 EEHg/L0.35 11/14/19SM21-22 6200B1Chloroethane
ND 0.50 11/15/19 0:57 EEHg/L0.17 11/14/19SM21-22 6200B1Chloroform
ND 1.0 11/15/19 0:57 EEHg/L0.45 11/14/19SM21-22 6200B1Chloromethane
ND 0.50 11/15/19 0:57 EEHg/L0.12 11/14/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/15/19 0:57 EEHg/L0.14 11/14/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/15/19 0:57 EEHg/L0.19 11/14/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/15/19 0:57 EEHg/L0.16 11/14/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/15/19 0:57 EEHg/L0.12 11/14/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/15/19 0:57 EEHg/L0.13 11/14/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/15/19 0:57 EEHg/L0.26 11/14/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/15/19 0:57 EEHg/L0.16 11/14/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/15/19 0:57 EEHg/L0.41 11/14/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/15/19 0:57 EEHg/L0.32 11/14/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/15/19 0:57 EEHg/L0.13 11/14/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/15/19 0:57 EEHg/L0.31 11/14/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/15/19 0:57 EEHg/L0.20 11/14/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/15/19 0:57 EEHg/L0.11 11/14/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/15/19 0:57 EEHg/L0.20 11/14/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/15/19 0:57 EEHg/L0.16 11/14/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/15/19 0:57 EEHg/L0.13 11/14/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/15/19 0:57 EEHg/L0.23 11/14/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/15/19 0:57 EEHg/L0.17 11/14/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/15/19 0:57 EEHg/L0.13 11/14/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/15/19 0:57 EEHg/L1.5 11/14/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/15/19 0:57 EEHg/L0.17 11/14/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/15/19 0:57 EEHg/L0.20 11/14/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
Page 23 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-05
Field Sample #: Field Blank 11/6/19
Sample Matrix: Field Blank
Sampled: 11/6/2019 18:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 11/15/19 0:57 EEHg/L0.25 11/14/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/15/19 0:57 EEHg/L0.34 11/14/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/15/19 0:57 EEHg/L1.7 11/14/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 11/15/19 0:57 EEHg/L0.31 11/14/19SM21-22 6200B1Naphthalene
ND 0.50 11/15/19 0:57 EEHg/L0.13 11/14/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/15/19 0:57 EEHg/L0.11 11/14/19SM21-22 6200B1Styrene
ND 0.50 11/15/19 0:57 EEHg/L0.27 11/14/19SM21-22 6200B11,1,1,2-Tetrachloroethane
ND 0.50 11/15/19 0:57 EEHg/L0.22 11/14/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/15/19 0:57 EEHg/L0.18 11/14/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/15/19 0:57 EEHg/L0.14 11/14/19SM21-22 6200B1Toluene
ND 2.0 11/15/19 0:57 EEHg/L0.57 11/14/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/15/19 0:57 EEHg/L0.40 11/14/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/15/19 0:57 EEHg/L0.20 11/14/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/15/19 0:57 EEHg/L0.16 11/14/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/15/19 0:57 EEHg/L0.24 11/14/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/15/19 0:57 EEHg/L0.33 11/14/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/15/19 0:57 EEHg/L0.25 11/14/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/15/19 0:57 EEHg/L0.18 11/14/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/15/19 0:57 EEHg/L0.14 11/14/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/15/19 0:57 EEHg/L10 11/14/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/15/19 0:57 EEHg/L0.45 11/14/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/15/19 0:57 EEHg/L0.30 11/14/19SM21-22 6200B1m+p Xylene
ND 0.50 11/15/19 0:57 EEHg/L0.17 11/14/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.7 11/15/19 0:5770-130
Toluene-d8 98.7 11/15/19 0:5770-130
4-Bromofluorobenzene 97.2 11/15/19 0:5770-130
Page 24 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-06
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 11/7/2019 09:05
[TOC_2]19K0568-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/16/19 0:16 EEHg/L3.8 11/12/19SM21-22 6200B1Acetone
ND 1.0 11/16/19 0:16 EEHg/L0.14 11/12/19SM21-22 6200B1L-04tert-Amyl Methyl Ether (TAME)
0.28 0.50 11/16/19 0:16 EEHg/L0.18 11/12/19SM21-22 6200B1JBenzene
ND 0.50 11/16/19 0:16 EEHg/L0.15 11/12/19SM21-22 6200B1Bromobenzene
ND 0.50 11/16/19 0:16 EEHg/L0.32 11/12/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/16/19 0:16 EEHg/L0.16 11/12/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/16/19 0:16 EEHg/L0.46 11/12/19SM21-22 6200B1Bromoform
ND 1.0 11/16/19 0:16 EEHg/L0.78 11/12/19SM21-22 6200B1Bromomethane
ND 5.0 11/16/19 0:16 EEHg/L1.9 11/12/19SM21-22 6200B12-Butanone (MEK)
ND 20 11/16/19 0:16 EEHg/L4.2 11/12/19SM21-22 6200B1tert-Butyl Alcohol (TBA)
0.75 0.50 11/16/19 0:16 EEHg/L0.21 11/12/19SM21-22 6200B1n-Butylbenzene
0.60 0.50 11/16/19 0:16 EEHg/L0.16 11/12/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/16/19 0:16 EEHg/L0.17 11/12/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/16/19 0:16 EEHg/L0.16 11/12/19SM21-22 6200B1L-04tert-Butyl Ethyl Ether (TBEE)
ND 0.50 11/16/19 0:16 EEHg/L0.11 11/12/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/16/19 0:16 EEHg/L0.15 11/12/19SM21-22 6200B1Chlorobenzene
ND 50 11/16/19 0:16 EEHg/L11 11/12/19SM21-22 6200B1Ethanol
ND 0.50 11/16/19 0:16 EEHg/L0.21 11/12/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/16/19 0:16 EEHg/L0.35 11/12/19SM21-22 6200B1Chloroethane
0.19 0.50 11/16/19 0:16 EEHg/L0.17 11/12/19SM21-22 6200B1JChloroform
ND 1.0 11/16/19 0:16 EEHg/L0.45 11/12/19SM21-22 6200B1Chloromethane
ND 0.50 11/16/19 0:16 EEHg/L0.12 11/12/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/16/19 0:16 EEHg/L0.14 11/12/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/16/19 0:16 EEHg/L0.19 11/12/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/16/19 0:16 EEHg/L0.16 11/12/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/16/19 0:16 EEHg/L0.12 11/12/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/16/19 0:16 EEHg/L0.13 11/12/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/16/19 0:16 EEHg/L0.26 11/12/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/16/19 0:16 EEHg/L0.16 11/12/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/16/19 0:16 EEHg/L0.41 11/12/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/16/19 0:16 EEHg/L0.32 11/12/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/16/19 0:16 EEHg/L0.13 11/12/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/16/19 0:16 EEHg/L0.31 11/12/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/16/19 0:16 EEHg/L0.20 11/12/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/16/19 0:16 EEHg/L0.11 11/12/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/16/19 0:16 EEHg/L0.20 11/12/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/16/19 0:16 EEHg/L0.16 11/12/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/16/19 0:16 EEHg/L0.13 11/12/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/16/19 0:16 EEHg/L0.23 11/12/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/16/19 0:16 EEHg/L0.17 11/12/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/16/19 0:16 EEHg/L0.13 11/12/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/16/19 0:16 EEHg/L1.5 11/12/19SM21-22 6200B12-Hexanone (MBK)
1.2 0.50 11/16/19 0:16 EEHg/L0.17 11/12/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/16/19 0:16 EEHg/L0.20 11/12/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
Page 25 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-06
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 11/7/2019 09:05
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
1.0 0.50 11/16/19 0:16 EEHg/L0.25 11/12/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/16/19 0:16 EEHg/L0.34 11/12/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/16/19 0:16 EEHg/L1.7 11/12/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
5.1 5.0 11/16/19 0:16 EEHg/L0.31 11/12/19SM21-22 6200B1Naphthalene
2.7 0.50 11/16/19 0:16 EEHg/L0.13 11/12/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/16/19 0:16 EEHg/L0.11 11/12/19SM21-22 6200B1Styrene
ND 0.50 11/16/19 0:16 EEHg/L0.27 11/12/19SM21-22 6200B11,1,1,2-Tetrachloroethane
ND 0.50 11/16/19 0:16 EEHg/L0.22 11/12/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/16/19 0:16 EEHg/L0.18 11/12/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/16/19 0:16 EEHg/L0.14 11/12/19SM21-22 6200B1Toluene
ND 2.0 11/16/19 0:16 EEHg/L0.57 11/12/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/16/19 0:16 EEHg/L0.40 11/12/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/16/19 0:16 EEHg/L0.20 11/12/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/16/19 0:16 EEHg/L0.16 11/12/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/16/19 0:16 EEHg/L0.24 11/12/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/16/19 0:16 EEHg/L0.33 11/12/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/16/19 0:16 EEHg/L0.25 11/12/19SM21-22 6200B11,2,3-Trichloropropane
13 0.50 11/16/19 0:16 EEHg/L0.18 11/12/19SM21-22 6200B11,2,4-Trimethylbenzene
4.3 0.50 11/16/19 0:16 EEHg/L0.14 11/12/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/16/19 0:16 EEHg/L10 11/12/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/16/19 0:16 EEHg/L0.45 11/12/19SM21-22 6200B1Vinyl Chloride
4.6 1.0 11/16/19 0:16 EEHg/L0.30 11/12/19SM21-22 6200B1m+p Xylene
3.9 0.50 11/16/19 0:16 EEHg/L0.17 11/12/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 86.5 11/16/19 0:1670-130
Toluene-d8 97.6 11/16/19 0:1670-130
4-Bromofluorobenzene 99.8 11/16/19 0:1670-130
Page 26 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-07
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 11/7/2019 09:30
[TOC_2]19K0568-07[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
5.5 50 11/16/19 0:44 EEHg/L3.8 11/12/19SM21-22 6200B1JAcetone
ND 1.0 11/16/19 0:44 EEHg/L0.14 11/12/19SM21-22 6200B1L-04tert-Amyl Methyl Ether (TAME)
ND 0.50 11/16/19 0:44 EEHg/L0.18 11/12/19SM21-22 6200B1Benzene
ND 0.50 11/16/19 0:44 EEHg/L0.15 11/12/19SM21-22 6200B1Bromobenzene
ND 0.50 11/16/19 0:44 EEHg/L0.32 11/12/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/16/19 0:44 EEHg/L0.16 11/12/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/16/19 0:44 EEHg/L0.46 11/12/19SM21-22 6200B1Bromoform
ND 1.0 11/16/19 0:44 EEHg/L0.78 11/12/19SM21-22 6200B1Bromomethane
ND 5.0 11/16/19 0:44 EEHg/L1.9 11/12/19SM21-22 6200B12-Butanone (MEK)
ND 20 11/16/19 0:44 EEHg/L4.2 11/12/19SM21-22 6200B1tert-Butyl Alcohol (TBA)
ND 0.50 11/16/19 0:44 EEHg/L0.21 11/12/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/16/19 0:44 EEHg/L0.16 11/12/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/16/19 0:44 EEHg/L0.17 11/12/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/16/19 0:44 EEHg/L0.16 11/12/19SM21-22 6200B1L-04tert-Butyl Ethyl Ether (TBEE)
ND 0.50 11/16/19 0:44 EEHg/L0.11 11/12/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/16/19 0:44 EEHg/L0.15 11/12/19SM21-22 6200B1Chlorobenzene
ND 50 11/16/19 0:44 EEHg/L11 11/12/19SM21-22 6200B1Ethanol
ND 0.50 11/16/19 0:44 EEHg/L0.21 11/12/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/16/19 0:44 EEHg/L0.35 11/12/19SM21-22 6200B1Chloroethane
ND 0.50 11/16/19 0:44 EEHg/L0.17 11/12/19SM21-22 6200B1Chloroform
ND 1.0 11/16/19 0:44 EEHg/L0.45 11/12/19SM21-22 6200B1Chloromethane
ND 0.50 11/16/19 0:44 EEHg/L0.12 11/12/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/16/19 0:44 EEHg/L0.14 11/12/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/16/19 0:44 EEHg/L0.19 11/12/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/16/19 0:44 EEHg/L0.16 11/12/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/16/19 0:44 EEHg/L0.12 11/12/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/16/19 0:44 EEHg/L0.13 11/12/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/16/19 0:44 EEHg/L0.26 11/12/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/16/19 0:44 EEHg/L0.16 11/12/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/16/19 0:44 EEHg/L0.41 11/12/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/16/19 0:44 EEHg/L0.32 11/12/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/16/19 0:44 EEHg/L0.13 11/12/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/16/19 0:44 EEHg/L0.31 11/12/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/16/19 0:44 EEHg/L0.20 11/12/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/16/19 0:44 EEHg/L0.11 11/12/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/16/19 0:44 EEHg/L0.20 11/12/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/16/19 0:44 EEHg/L0.16 11/12/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/16/19 0:44 EEHg/L0.13 11/12/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/16/19 0:44 EEHg/L0.23 11/12/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/16/19 0:44 EEHg/L0.17 11/12/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/16/19 0:44 EEHg/L0.13 11/12/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/16/19 0:44 EEHg/L1.5 11/12/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/16/19 0:44 EEHg/L0.17 11/12/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/16/19 0:44 EEHg/L0.20 11/12/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
Page 27 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-07
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 11/7/2019 09:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 11/16/19 0:44 EEHg/L0.25 11/12/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/16/19 0:44 EEHg/L0.34 11/12/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/16/19 0:44 EEHg/L1.7 11/12/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 11/16/19 0:44 EEHg/L0.31 11/12/19SM21-22 6200B1Naphthalene
ND 0.50 11/16/19 0:44 EEHg/L0.13 11/12/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/16/19 0:44 EEHg/L0.11 11/12/19SM21-22 6200B1Styrene
ND 0.50 11/16/19 0:44 EEHg/L0.27 11/12/19SM21-22 6200B11,1,1,2-Tetrachloroethane
ND 0.50 11/16/19 0:44 EEHg/L0.22 11/12/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/16/19 0:44 EEHg/L0.18 11/12/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/16/19 0:44 EEHg/L0.14 11/12/19SM21-22 6200B1Toluene
ND 2.0 11/16/19 0:44 EEHg/L0.57 11/12/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/16/19 0:44 EEHg/L0.40 11/12/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/16/19 0:44 EEHg/L0.20 11/12/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/16/19 0:44 EEHg/L0.16 11/12/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/16/19 0:44 EEHg/L0.24 11/12/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/16/19 0:44 EEHg/L0.33 11/12/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/16/19 0:44 EEHg/L0.25 11/12/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/16/19 0:44 EEHg/L0.18 11/12/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/16/19 0:44 EEHg/L0.14 11/12/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/16/19 0:44 EEHg/L10 11/12/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/16/19 0:44 EEHg/L0.45 11/12/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/16/19 0:44 EEHg/L0.30 11/12/19SM21-22 6200B1m+p Xylene
ND 0.50 11/16/19 0:44 EEHg/L0.17 11/12/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 86.9 11/16/19 0:4470-130
Toluene-d8 96.9 11/16/19 0:4470-130
4-Bromofluorobenzene 98.2 11/16/19 0:4470-130
Page 28 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-08
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 11/7/2019 09:55
[TOC_2]19K0568-08[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/16/19 3:38 EEHg/L3.8 11/12/19SM21-22 6200B1Acetone
ND 1.0 11/16/19 3:38 EEHg/L0.14 11/12/19SM21-22 6200B1L-04tert-Amyl Methyl Ether (TAME)
ND 0.50 11/16/19 3:38 EEHg/L0.18 11/12/19SM21-22 6200B1Benzene
ND 0.50 11/16/19 3:38 EEHg/L0.15 11/12/19SM21-22 6200B1Bromobenzene
ND 0.50 11/16/19 3:38 EEHg/L0.32 11/12/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/16/19 3:38 EEHg/L0.16 11/12/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/16/19 3:38 EEHg/L0.46 11/12/19SM21-22 6200B1Bromoform
ND 1.0 11/16/19 3:38 EEHg/L0.78 11/12/19SM21-22 6200B1Bromomethane
ND 5.0 11/16/19 3:38 EEHg/L1.9 11/12/19SM21-22 6200B12-Butanone (MEK)
ND 20 11/16/19 3:38 EEHg/L4.2 11/12/19SM21-22 6200B1tert-Butyl Alcohol (TBA)
0.36 0.50 11/16/19 3:38 EEHg/L0.21 11/12/19SM21-22 6200B1Jn-Butylbenzene
0.18 0.50 11/16/19 3:38 EEHg/L0.16 11/12/19SM21-22 6200B1Jsec-Butylbenzene
ND 0.50 11/16/19 3:38 EEHg/L0.17 11/12/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/16/19 3:38 EEHg/L0.16 11/12/19SM21-22 6200B1L-04tert-Butyl Ethyl Ether (TBEE)
ND 0.50 11/16/19 3:38 EEHg/L0.11 11/12/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/16/19 3:38 EEHg/L0.15 11/12/19SM21-22 6200B1Chlorobenzene
ND 50 11/16/19 3:38 EEHg/L11 11/12/19SM21-22 6200B1Ethanol
ND 0.50 11/16/19 3:38 EEHg/L0.21 11/12/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/16/19 3:38 EEHg/L0.35 11/12/19SM21-22 6200B1Chloroethane
ND 0.50 11/16/19 3:38 EEHg/L0.17 11/12/19SM21-22 6200B1Chloroform
ND 1.0 11/16/19 3:38 EEHg/L0.45 11/12/19SM21-22 6200B1Chloromethane
ND 0.50 11/16/19 3:38 EEHg/L0.12 11/12/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/16/19 3:38 EEHg/L0.14 11/12/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/16/19 3:38 EEHg/L0.19 11/12/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/16/19 3:38 EEHg/L0.16 11/12/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/16/19 3:38 EEHg/L0.12 11/12/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/16/19 3:38 EEHg/L0.13 11/12/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/16/19 3:38 EEHg/L0.26 11/12/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/16/19 3:38 EEHg/L0.16 11/12/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/16/19 3:38 EEHg/L0.41 11/12/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/16/19 3:38 EEHg/L0.32 11/12/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/16/19 3:38 EEHg/L0.13 11/12/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/16/19 3:38 EEHg/L0.31 11/12/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/16/19 3:38 EEHg/L0.20 11/12/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/16/19 3:38 EEHg/L0.11 11/12/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/16/19 3:38 EEHg/L0.20 11/12/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/16/19 3:38 EEHg/L0.16 11/12/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/16/19 3:38 EEHg/L0.13 11/12/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/16/19 3:38 EEHg/L0.23 11/12/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/16/19 3:38 EEHg/L0.17 11/12/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/16/19 3:38 EEHg/L0.13 11/12/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/16/19 3:38 EEHg/L1.5 11/12/19SM21-22 6200B12-Hexanone (MBK)
0.19 0.50 11/16/19 3:38 EEHg/L0.17 11/12/19SM21-22 6200B1JIsopropylbenzene (Cumene)
0.30 0.50 11/16/19 3:38 EEHg/L0.20 11/12/19SM21-22 6200B1Jp-Isopropyltoluene (p-Cymene)
Page 29 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-08
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 11/7/2019 09:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 11/16/19 3:38 EEHg/L0.25 11/12/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/16/19 3:38 EEHg/L0.34 11/12/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/16/19 3:38 EEHg/L1.7 11/12/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 11/16/19 3:38 EEHg/L0.31 11/12/19SM21-22 6200B1Naphthalene
0.37 0.50 11/16/19 3:38 EEHg/L0.13 11/12/19SM21-22 6200B1Jn-Propylbenzene
ND 0.50 11/16/19 3:38 EEHg/L0.11 11/12/19SM21-22 6200B1Styrene
ND 0.50 11/16/19 3:38 EEHg/L0.27 11/12/19SM21-22 6200B11,1,1,2-Tetrachloroethane
ND 0.50 11/16/19 3:38 EEHg/L0.22 11/12/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/16/19 3:38 EEHg/L0.18 11/12/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/16/19 3:38 EEHg/L0.14 11/12/19SM21-22 6200B1Toluene
ND 2.0 11/16/19 3:38 EEHg/L0.57 11/12/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/16/19 3:38 EEHg/L0.40 11/12/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/16/19 3:38 EEHg/L0.20 11/12/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/16/19 3:38 EEHg/L0.16 11/12/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/16/19 3:38 EEHg/L0.24 11/12/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/16/19 3:38 EEHg/L0.33 11/12/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/16/19 3:38 EEHg/L0.25 11/12/19SM21-22 6200B11,2,3-Trichloropropane
6.1 0.50 11/16/19 3:38 EEHg/L0.18 11/12/19SM21-22 6200B11,2,4-Trimethylbenzene
0.63 0.50 11/16/19 3:38 EEHg/L0.14 11/12/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/16/19 3:38 EEHg/L10 11/12/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/16/19 3:38 EEHg/L0.45 11/12/19SM21-22 6200B1Vinyl Chloride
1.3 1.0 11/16/19 3:38 EEHg/L0.30 11/12/19SM21-22 6200B1m+p Xylene
1.9 0.50 11/16/19 3:38 EEHg/L0.17 11/12/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 88.2 11/16/19 3:3870-130
Toluene-d8 97.8 11/16/19 3:3870-130
4-Bromofluorobenzene 102 11/16/19 3:3870-130
Page 30 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-09
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 11/7/2019 10:20
[TOC_2]19K0568-09[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 12000 11/16/19 5:33 EEHg/L950 11/12/19SM21-22 6200B250Acetone
ND 250 11/16/19 5:33 EEHg/L35 11/12/19SM21-22 6200B250L-04tert-Amyl Methyl Ether (TAME)
270 120 11/16/19 5:33 EEHg/L45 11/12/19SM21-22 6200B250Benzene
ND 120 11/16/19 5:33 EEHg/L38 11/12/19SM21-22 6200B250Bromobenzene
ND 120 11/16/19 5:33 EEHg/L80 11/12/19SM21-22 6200B250Bromochloromethane
ND 120 11/16/19 5:33 EEHg/L40 11/12/19SM21-22 6200B250Bromodichloromethane
ND 120 11/16/19 5:33 EEHg/L120 11/12/19SM21-22 6200B250Bromoform
ND 250 11/16/19 5:33 EEHg/L200 11/12/19SM21-22 6200B250Bromomethane
ND 1200 11/16/19 5:33 EEHg/L480 11/12/19SM21-22 6200B2502-Butanone (MEK)
ND 5000 11/16/19 5:33 EEHg/L1000 11/12/19SM21-22 6200B250tert-Butyl Alcohol (TBA)
ND 120 11/16/19 5:33 EEHg/L52 11/12/19SM21-22 6200B250n-Butylbenzene
ND 120 11/16/19 5:33 EEHg/L40 11/12/19SM21-22 6200B250sec-Butylbenzene
ND 120 11/16/19 5:33 EEHg/L42 11/12/19SM21-22 6200B250tert-Butylbenzene
ND 120 11/16/19 5:33 EEHg/L40 11/12/19SM21-22 6200B250L-04tert-Butyl Ethyl Ether (TBEE)
ND 120 11/16/19 5:33 EEHg/L28 11/12/19SM21-22 6200B250Carbon Tetrachloride
ND 120 11/16/19 5:33 EEHg/L38 11/12/19SM21-22 6200B250Chlorobenzene
ND 12000 11/16/19 5:33 EEHg/L2600 11/12/19SM21-22 6200B250Ethanol
ND 120 11/16/19 5:33 EEHg/L52 11/12/19SM21-22 6200B250Chlorodibromomethane
ND 120 11/16/19 5:33 EEHg/L88 11/12/19SM21-22 6200B250Chloroethane
ND 120 11/16/19 5:33 EEHg/L42 11/12/19SM21-22 6200B250Chloroform
ND 250 11/16/19 5:33 EEHg/L110 11/12/19SM21-22 6200B250Chloromethane
ND 120 11/16/19 5:33 EEHg/L30 11/12/19SM21-22 6200B2502-Chlorotoluene
ND 120 11/16/19 5:33 EEHg/L35 11/12/19SM21-22 6200B2504-Chlorotoluene
ND 120 11/16/19 5:33 EEHg/L48 11/12/19SM21-22 6200B2501,2-Dibromoethane (EDB)
ND 120 11/16/19 5:33 EEHg/L40 11/12/19SM21-22 6200B2501,2-Dichlorobenzene
ND 120 11/16/19 5:33 EEHg/L30 11/12/19SM21-22 6200B2501,3-Dichlorobenzene
ND 120 11/16/19 5:33 EEHg/L32 11/12/19SM21-22 6200B2501,4-Dichlorobenzene
ND 120 11/16/19 5:33 EEHg/L65 11/12/19SM21-22 6200B250Dichlorodifluoromethane (Freon 12)
ND 120 11/16/19 5:33 EEHg/L40 11/12/19SM21-22 6200B2501,1-Dichloroethane
ND 250 11/16/19 5:33 EEHg/L100 11/12/19SM21-22 6200B2501,2-Dichloroethane
ND 120 11/16/19 5:33 EEHg/L80 11/12/19SM21-22 6200B2501,1-Dichloroethylene
ND 120 11/16/19 5:33 EEHg/L32 11/12/19SM21-22 6200B250cis-1,2-Dichloroethylene
ND 120 11/16/19 5:33 EEHg/L78 11/12/19SM21-22 6200B250trans-1,2-Dichloroethylene
ND 120 11/16/19 5:33 EEHg/L50 11/12/19SM21-22 6200B2501,2-Dichloropropane
ND 120 11/16/19 5:33 EEHg/L28 11/12/19SM21-22 6200B2501,3-Dichloropropane
ND 120 11/16/19 5:33 EEHg/L50 11/12/19SM21-22 6200B2502,2-Dichloropropane
ND 120 11/16/19 5:33 EEHg/L40 11/12/19SM21-22 6200B2501,1-Dichloropropene
ND 120 11/16/19 5:33 EEHg/L32 11/12/19SM21-22 6200B250cis-1,3-Dichloropropene
ND 120 11/16/19 5:33 EEHg/L58 11/12/19SM21-22 6200B250trans-1,3-Dichloropropene
ND 120 11/16/19 5:33 EEHg/L42 11/12/19SM21-22 6200B250Diisopropyl Ether (DIPE)
3000 120 11/16/19 5:33 EEHg/L32 11/12/19SM21-22 6200B250Ethylbenzene
ND 1200 11/16/19 5:33 EEHg/L380 11/12/19SM21-22 6200B2502-Hexanone (MBK)
90 120 11/16/19 5:33 EEHg/L42 11/12/19SM21-22 6200B250JIsopropylbenzene (Cumene)
ND 120 11/16/19 5:33 EEHg/L50 11/12/19SM21-22 6200B250p-Isopropyltoluene (p-Cymene)
Page 31 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-09
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 11/7/2019 10:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 120 11/16/19 5:33 EEHg/L62 11/12/19SM21-22 6200B250Methyl tert-Butyl Ether (MTBE)
ND 1200 11/16/19 5:33 EEHg/L85 11/12/19SM21-22 6200B250Methylene Chloride
ND 1200 11/16/19 5:33 EEHg/L420 11/12/19SM21-22 6200B2504-Methyl-2-pentanone (MIBK)
1300 1200 11/16/19 5:33 EEHg/L78 11/12/19SM21-22 6200B250Naphthalene
300 120 11/16/19 5:33 EEHg/L32 11/12/19SM21-22 6200B250n-Propylbenzene
92 120 11/16/19 5:33 EEHg/L28 11/12/19SM21-22 6200B250JStyrene
ND 120 11/16/19 5:33 EEHg/L68 11/12/19SM21-22 6200B2501,1,1,2-Tetrachloroethane
ND 120 11/16/19 5:33 EEHg/L55 11/12/19SM21-22 6200B2501,1,2,2-Tetrachloroethane
ND 120 11/16/19 5:33 EEHg/L45 11/12/19SM21-22 6200B250Tetrachloroethylene
12000 120 11/16/19 5:33 EEHg/L35 11/12/19SM21-22 6200B250Toluene
ND 500 11/16/19 5:33 EEHg/L140 11/12/19SM21-22 6200B2501,2,3-Trichlorobenzene
ND 120 11/16/19 5:33 EEHg/L100 11/12/19SM21-22 6200B2501,2,4-Trichlorobenzene
ND 120 11/16/19 5:33 EEHg/L50 11/12/19SM21-22 6200B2501,1,1-Trichloroethane
ND 120 11/16/19 5:33 EEHg/L40 11/12/19SM21-22 6200B2501,1,2-Trichloroethane
ND 120 11/16/19 5:33 EEHg/L60 11/12/19SM21-22 6200B250Trichloroethylene
ND 120 11/16/19 5:33 EEHg/L82 11/12/19SM21-22 6200B250Trichlorofluoromethane (Freon 11)
ND 120 11/16/19 5:33 EEHg/L62 11/12/19SM21-22 6200B2501,2,3-Trichloropropane
2400 120 11/16/19 5:33 EEHg/L45 11/12/19SM21-22 6200B2501,2,4-Trimethylbenzene
680 120 11/16/19 5:33 EEHg/L35 11/12/19SM21-22 6200B2501,3,5-Trimethylbenzene
ND 5000 11/16/19 5:33 EEHg/L2500 11/12/19SM21-22 6200B250Vinyl Acetate
ND 120 11/16/19 5:33 EEHg/L110 11/12/19SM21-22 6200B250Vinyl Chloride
10000 250 11/16/19 5:33 EEHg/L75 11/12/19SM21-22 6200B250m+p Xylene
4800 120 11/16/19 5:33 EEHg/L42 11/12/19SM21-22 6200B250o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 88.8 11/16/19 5:3370-130
Toluene-d8 97.9 11/16/19 5:3370-130
4-Bromofluorobenzene 99.3 11/16/19 5:3370-130
Page 32 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-10
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 11/7/2019 10:45
[TOC_2]19K0568-10[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/16/19 1:13 EEHg/L3.8 11/12/19SM21-22 6200B1Acetone
ND 1.0 11/16/19 1:13 EEHg/L0.14 11/12/19SM21-22 6200B1L-04tert-Amyl Methyl Ether (TAME)
ND 0.50 11/16/19 1:13 EEHg/L0.18 11/12/19SM21-22 6200B1Benzene
ND 0.50 11/16/19 1:13 EEHg/L0.15 11/12/19SM21-22 6200B1Bromobenzene
ND 0.50 11/16/19 1:13 EEHg/L0.32 11/12/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/16/19 1:13 EEHg/L0.16 11/12/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/16/19 1:13 EEHg/L0.46 11/12/19SM21-22 6200B1Bromoform
ND 1.0 11/16/19 1:13 EEHg/L0.78 11/12/19SM21-22 6200B1Bromomethane
ND 5.0 11/16/19 1:13 EEHg/L1.9 11/12/19SM21-22 6200B12-Butanone (MEK)
ND 20 11/16/19 1:13 EEHg/L4.2 11/12/19SM21-22 6200B1tert-Butyl Alcohol (TBA)
ND 0.50 11/16/19 1:13 EEHg/L0.21 11/12/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/16/19 1:13 EEHg/L0.16 11/12/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/16/19 1:13 EEHg/L0.17 11/12/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/16/19 1:13 EEHg/L0.16 11/12/19SM21-22 6200B1L-04tert-Butyl Ethyl Ether (TBEE)
ND 0.50 11/16/19 1:13 EEHg/L0.11 11/12/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/16/19 1:13 EEHg/L0.15 11/12/19SM21-22 6200B1Chlorobenzene
ND 50 11/16/19 1:13 EEHg/L11 11/12/19SM21-22 6200B1Ethanol
ND 0.50 11/16/19 1:13 EEHg/L0.21 11/12/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/16/19 1:13 EEHg/L0.35 11/12/19SM21-22 6200B1Chloroethane
ND 0.50 11/16/19 1:13 EEHg/L0.17 11/12/19SM21-22 6200B1Chloroform
ND 1.0 11/16/19 1:13 EEHg/L0.45 11/12/19SM21-22 6200B1Chloromethane
ND 0.50 11/16/19 1:13 EEHg/L0.12 11/12/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/16/19 1:13 EEHg/L0.14 11/12/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/16/19 1:13 EEHg/L0.19 11/12/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/16/19 1:13 EEHg/L0.16 11/12/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/16/19 1:13 EEHg/L0.12 11/12/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/16/19 1:13 EEHg/L0.13 11/12/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/16/19 1:13 EEHg/L0.26 11/12/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/16/19 1:13 EEHg/L0.16 11/12/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/16/19 1:13 EEHg/L0.41 11/12/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/16/19 1:13 EEHg/L0.32 11/12/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/16/19 1:13 EEHg/L0.13 11/12/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/16/19 1:13 EEHg/L0.31 11/12/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/16/19 1:13 EEHg/L0.20 11/12/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/16/19 1:13 EEHg/L0.11 11/12/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/16/19 1:13 EEHg/L0.20 11/12/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/16/19 1:13 EEHg/L0.16 11/12/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/16/19 1:13 EEHg/L0.13 11/12/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/16/19 1:13 EEHg/L0.23 11/12/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/16/19 1:13 EEHg/L0.17 11/12/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/16/19 1:13 EEHg/L0.13 11/12/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/16/19 1:13 EEHg/L1.5 11/12/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/16/19 1:13 EEHg/L0.17 11/12/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/16/19 1:13 EEHg/L0.20 11/12/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
Page 33 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-10
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 11/7/2019 10:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 11/16/19 1:13 EEHg/L0.25 11/12/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/16/19 1:13 EEHg/L0.34 11/12/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/16/19 1:13 EEHg/L1.7 11/12/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 11/16/19 1:13 EEHg/L0.31 11/12/19SM21-22 6200B1Naphthalene
ND 0.50 11/16/19 1:13 EEHg/L0.13 11/12/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/16/19 1:13 EEHg/L0.11 11/12/19SM21-22 6200B1Styrene
ND 0.50 11/16/19 1:13 EEHg/L0.27 11/12/19SM21-22 6200B11,1,1,2-Tetrachloroethane
ND 0.50 11/16/19 1:13 EEHg/L0.22 11/12/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/16/19 1:13 EEHg/L0.18 11/12/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/16/19 1:13 EEHg/L0.14 11/12/19SM21-22 6200B1Toluene
ND 2.0 11/16/19 1:13 EEHg/L0.57 11/12/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/16/19 1:13 EEHg/L0.40 11/12/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/16/19 1:13 EEHg/L0.20 11/12/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/16/19 1:13 EEHg/L0.16 11/12/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/16/19 1:13 EEHg/L0.24 11/12/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/16/19 1:13 EEHg/L0.33 11/12/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/16/19 1:13 EEHg/L0.25 11/12/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/16/19 1:13 EEHg/L0.18 11/12/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/16/19 1:13 EEHg/L0.14 11/12/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/16/19 1:13 EEHg/L10 11/12/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/16/19 1:13 EEHg/L0.45 11/12/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/16/19 1:13 EEHg/L0.30 11/12/19SM21-22 6200B1m+p Xylene
ND 0.50 11/16/19 1:13 EEHg/L0.17 11/12/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 87.3 11/16/19 1:1370-130
Toluene-d8 96.1 11/16/19 1:1370-130
4-Bromofluorobenzene 98.2 11/16/19 1:1370-130
Page 34 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-11
Field Sample #: MW-7
Sample Matrix: Ground Water
Sampled: 11/7/2019 11:10
[TOC_2]19K0568-11[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/16/19 1:42 EEHg/L3.8 11/12/19SM21-22 6200B1Acetone
ND 1.0 11/16/19 1:42 EEHg/L0.14 11/12/19SM21-22 6200B1L-04tert-Amyl Methyl Ether (TAME)
ND 0.50 11/16/19 1:42 EEHg/L0.18 11/12/19SM21-22 6200B1Benzene
ND 0.50 11/16/19 1:42 EEHg/L0.15 11/12/19SM21-22 6200B1Bromobenzene
ND 0.50 11/16/19 1:42 EEHg/L0.32 11/12/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/16/19 1:42 EEHg/L0.16 11/12/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/16/19 1:42 EEHg/L0.46 11/12/19SM21-22 6200B1Bromoform
ND 1.0 11/16/19 1:42 EEHg/L0.78 11/12/19SM21-22 6200B1Bromomethane
ND 5.0 11/16/19 1:42 EEHg/L1.9 11/12/19SM21-22 6200B12-Butanone (MEK)
ND 20 11/16/19 1:42 EEHg/L4.2 11/12/19SM21-22 6200B1tert-Butyl Alcohol (TBA)
ND 0.50 11/16/19 1:42 EEHg/L0.21 11/12/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/16/19 1:42 EEHg/L0.16 11/12/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/16/19 1:42 EEHg/L0.17 11/12/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/16/19 1:42 EEHg/L0.16 11/12/19SM21-22 6200B1L-04tert-Butyl Ethyl Ether (TBEE)
ND 0.50 11/16/19 1:42 EEHg/L0.11 11/12/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/16/19 1:42 EEHg/L0.15 11/12/19SM21-22 6200B1Chlorobenzene
ND 50 11/16/19 1:42 EEHg/L11 11/12/19SM21-22 6200B1Ethanol
ND 0.50 11/16/19 1:42 EEHg/L0.21 11/12/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/16/19 1:42 EEHg/L0.35 11/12/19SM21-22 6200B1Chloroethane
ND 0.50 11/16/19 1:42 EEHg/L0.17 11/12/19SM21-22 6200B1Chloroform
ND 1.0 11/16/19 1:42 EEHg/L0.45 11/12/19SM21-22 6200B1Chloromethane
ND 0.50 11/16/19 1:42 EEHg/L0.12 11/12/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/16/19 1:42 EEHg/L0.14 11/12/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/16/19 1:42 EEHg/L0.19 11/12/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/16/19 1:42 EEHg/L0.16 11/12/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/16/19 1:42 EEHg/L0.12 11/12/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/16/19 1:42 EEHg/L0.13 11/12/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/16/19 1:42 EEHg/L0.26 11/12/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/16/19 1:42 EEHg/L0.16 11/12/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/16/19 1:42 EEHg/L0.41 11/12/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/16/19 1:42 EEHg/L0.32 11/12/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/16/19 1:42 EEHg/L0.13 11/12/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/16/19 1:42 EEHg/L0.31 11/12/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/16/19 1:42 EEHg/L0.20 11/12/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/16/19 1:42 EEHg/L0.11 11/12/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/16/19 1:42 EEHg/L0.20 11/12/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/16/19 1:42 EEHg/L0.16 11/12/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/16/19 1:42 EEHg/L0.13 11/12/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/16/19 1:42 EEHg/L0.23 11/12/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/16/19 1:42 EEHg/L0.17 11/12/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/16/19 1:42 EEHg/L0.13 11/12/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/16/19 1:42 EEHg/L1.5 11/12/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/16/19 1:42 EEHg/L0.17 11/12/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/16/19 1:42 EEHg/L0.20 11/12/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
Page 35 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-11
Field Sample #: MW-7
Sample Matrix: Ground Water
Sampled: 11/7/2019 11:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 11/16/19 1:42 EEHg/L0.25 11/12/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/16/19 1:42 EEHg/L0.34 11/12/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/16/19 1:42 EEHg/L1.7 11/12/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 11/16/19 1:42 EEHg/L0.31 11/12/19SM21-22 6200B1Naphthalene
ND 0.50 11/16/19 1:42 EEHg/L0.13 11/12/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/16/19 1:42 EEHg/L0.11 11/12/19SM21-22 6200B1Styrene
ND 0.50 11/16/19 1:42 EEHg/L0.27 11/12/19SM21-22 6200B11,1,1,2-Tetrachloroethane
ND 0.50 11/16/19 1:42 EEHg/L0.22 11/12/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/16/19 1:42 EEHg/L0.18 11/12/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/16/19 1:42 EEHg/L0.14 11/12/19SM21-22 6200B1Toluene
ND 2.0 11/16/19 1:42 EEHg/L0.57 11/12/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/16/19 1:42 EEHg/L0.40 11/12/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/16/19 1:42 EEHg/L0.20 11/12/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/16/19 1:42 EEHg/L0.16 11/12/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/16/19 1:42 EEHg/L0.24 11/12/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/16/19 1:42 EEHg/L0.33 11/12/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/16/19 1:42 EEHg/L0.25 11/12/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/16/19 1:42 EEHg/L0.18 11/12/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/16/19 1:42 EEHg/L0.14 11/12/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/16/19 1:42 EEHg/L10 11/12/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/16/19 1:42 EEHg/L0.45 11/12/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/16/19 1:42 EEHg/L0.30 11/12/19SM21-22 6200B1m+p Xylene
ND 0.50 11/16/19 1:42 EEHg/L0.17 11/12/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 89.0 11/16/19 1:4270-130
Toluene-d8 97.4 11/16/19 1:4270-130
4-Bromofluorobenzene 99.2 11/16/19 1:4270-130
Page 36 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-12
Field Sample #: MW-9
Sample Matrix: Ground Water
Sampled: 11/7/2019 11:15
[TOC_2]19K0568-12[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
7.6 50 11/16/19 2:11 EEHg/L3.8 11/12/19SM21-22 6200B1JAcetone
ND 1.0 11/16/19 2:11 EEHg/L0.14 11/12/19SM21-22 6200B1L-04tert-Amyl Methyl Ether (TAME)
ND 0.50 11/16/19 2:11 EEHg/L0.18 11/12/19SM21-22 6200B1Benzene
ND 0.50 11/16/19 2:11 EEHg/L0.15 11/12/19SM21-22 6200B1Bromobenzene
ND 0.50 11/16/19 2:11 EEHg/L0.32 11/12/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/16/19 2:11 EEHg/L0.16 11/12/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/16/19 2:11 EEHg/L0.46 11/12/19SM21-22 6200B1Bromoform
ND 1.0 11/16/19 2:11 EEHg/L0.78 11/12/19SM21-22 6200B1Bromomethane
ND 5.0 11/16/19 2:11 EEHg/L1.9 11/12/19SM21-22 6200B12-Butanone (MEK)
ND 20 11/16/19 2:11 EEHg/L4.2 11/12/19SM21-22 6200B1tert-Butyl Alcohol (TBA)
ND 0.50 11/16/19 2:11 EEHg/L0.21 11/12/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/16/19 2:11 EEHg/L0.16 11/12/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/16/19 2:11 EEHg/L0.17 11/12/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/16/19 2:11 EEHg/L0.16 11/12/19SM21-22 6200B1L-04tert-Butyl Ethyl Ether (TBEE)
ND 0.50 11/16/19 2:11 EEHg/L0.11 11/12/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/16/19 2:11 EEHg/L0.15 11/12/19SM21-22 6200B1Chlorobenzene
ND 50 11/16/19 2:11 EEHg/L11 11/12/19SM21-22 6200B1Ethanol
ND 0.50 11/16/19 2:11 EEHg/L0.21 11/12/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/16/19 2:11 EEHg/L0.35 11/12/19SM21-22 6200B1Chloroethane
ND 0.50 11/16/19 2:11 EEHg/L0.17 11/12/19SM21-22 6200B1Chloroform
ND 1.0 11/16/19 2:11 EEHg/L0.45 11/12/19SM21-22 6200B1Chloromethane
ND 0.50 11/16/19 2:11 EEHg/L0.12 11/12/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/16/19 2:11 EEHg/L0.14 11/12/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/16/19 2:11 EEHg/L0.19 11/12/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/16/19 2:11 EEHg/L0.16 11/12/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/16/19 2:11 EEHg/L0.12 11/12/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/16/19 2:11 EEHg/L0.13 11/12/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/16/19 2:11 EEHg/L0.26 11/12/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/16/19 2:11 EEHg/L0.16 11/12/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/16/19 2:11 EEHg/L0.41 11/12/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/16/19 2:11 EEHg/L0.32 11/12/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/16/19 2:11 EEHg/L0.13 11/12/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/16/19 2:11 EEHg/L0.31 11/12/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/16/19 2:11 EEHg/L0.20 11/12/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/16/19 2:11 EEHg/L0.11 11/12/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/16/19 2:11 EEHg/L0.20 11/12/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/16/19 2:11 EEHg/L0.16 11/12/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/16/19 2:11 EEHg/L0.13 11/12/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/16/19 2:11 EEHg/L0.23 11/12/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/16/19 2:11 EEHg/L0.17 11/12/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/16/19 2:11 EEHg/L0.13 11/12/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/16/19 2:11 EEHg/L1.5 11/12/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/16/19 2:11 EEHg/L0.17 11/12/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/16/19 2:11 EEHg/L0.20 11/12/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
Page 37 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-12
Field Sample #: MW-9
Sample Matrix: Ground Water
Sampled: 11/7/2019 11:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 11/16/19 2:11 EEHg/L0.25 11/12/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/16/19 2:11 EEHg/L0.34 11/12/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/16/19 2:11 EEHg/L1.7 11/12/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 11/16/19 2:11 EEHg/L0.31 11/12/19SM21-22 6200B1Naphthalene
ND 0.50 11/16/19 2:11 EEHg/L0.13 11/12/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/16/19 2:11 EEHg/L0.11 11/12/19SM21-22 6200B1Styrene
ND 0.50 11/16/19 2:11 EEHg/L0.27 11/12/19SM21-22 6200B11,1,1,2-Tetrachloroethane
ND 0.50 11/16/19 2:11 EEHg/L0.22 11/12/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/16/19 2:11 EEHg/L0.18 11/12/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/16/19 2:11 EEHg/L0.14 11/12/19SM21-22 6200B1Toluene
ND 2.0 11/16/19 2:11 EEHg/L0.57 11/12/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/16/19 2:11 EEHg/L0.40 11/12/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/16/19 2:11 EEHg/L0.20 11/12/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/16/19 2:11 EEHg/L0.16 11/12/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/16/19 2:11 EEHg/L0.24 11/12/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/16/19 2:11 EEHg/L0.33 11/12/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/16/19 2:11 EEHg/L0.25 11/12/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/16/19 2:11 EEHg/L0.18 11/12/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/16/19 2:11 EEHg/L0.14 11/12/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/16/19 2:11 EEHg/L10 11/12/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/16/19 2:11 EEHg/L0.45 11/12/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/16/19 2:11 EEHg/L0.30 11/12/19SM21-22 6200B1m+p Xylene
ND 0.50 11/16/19 2:11 EEHg/L0.17 11/12/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 88.1 11/16/19 2:1170-130
Toluene-d8 99.0 11/16/19 2:1170-130
4-Bromofluorobenzene 98.6 11/16/19 2:1170-130
Page 38 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-13
Field Sample #: MW-12
Sample Matrix: Ground Water
Sampled: 11/7/2019 11:20
[TOC_2]19K0568-13[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
3.9 50 11/16/19 2:40 EEHg/L3.8 11/12/19SM21-22 6200B1JAcetone
ND 1.0 11/16/19 2:40 EEHg/L0.14 11/12/19SM21-22 6200B1L-04tert-Amyl Methyl Ether (TAME)
ND 0.50 11/16/19 2:40 EEHg/L0.18 11/12/19SM21-22 6200B1Benzene
ND 0.50 11/16/19 2:40 EEHg/L0.15 11/12/19SM21-22 6200B1Bromobenzene
ND 0.50 11/16/19 2:40 EEHg/L0.32 11/12/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/16/19 2:40 EEHg/L0.16 11/12/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/16/19 2:40 EEHg/L0.46 11/12/19SM21-22 6200B1Bromoform
ND 1.0 11/16/19 2:40 EEHg/L0.78 11/12/19SM21-22 6200B1Bromomethane
ND 5.0 11/16/19 2:40 EEHg/L1.9 11/12/19SM21-22 6200B12-Butanone (MEK)
ND 20 11/16/19 2:40 EEHg/L4.2 11/12/19SM21-22 6200B1tert-Butyl Alcohol (TBA)
ND 0.50 11/16/19 2:40 EEHg/L0.21 11/12/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/16/19 2:40 EEHg/L0.16 11/12/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/16/19 2:40 EEHg/L0.17 11/12/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/16/19 2:40 EEHg/L0.16 11/12/19SM21-22 6200B1L-04tert-Butyl Ethyl Ether (TBEE)
ND 0.50 11/16/19 2:40 EEHg/L0.11 11/12/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/16/19 2:40 EEHg/L0.15 11/12/19SM21-22 6200B1Chlorobenzene
ND 50 11/16/19 2:40 EEHg/L11 11/12/19SM21-22 6200B1Ethanol
ND 0.50 11/16/19 2:40 EEHg/L0.21 11/12/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/16/19 2:40 EEHg/L0.35 11/12/19SM21-22 6200B1Chloroethane
ND 0.50 11/16/19 2:40 EEHg/L0.17 11/12/19SM21-22 6200B1Chloroform
ND 1.0 11/16/19 2:40 EEHg/L0.45 11/12/19SM21-22 6200B1Chloromethane
ND 0.50 11/16/19 2:40 EEHg/L0.12 11/12/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/16/19 2:40 EEHg/L0.14 11/12/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/16/19 2:40 EEHg/L0.19 11/12/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/16/19 2:40 EEHg/L0.16 11/12/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/16/19 2:40 EEHg/L0.12 11/12/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/16/19 2:40 EEHg/L0.13 11/12/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/16/19 2:40 EEHg/L0.26 11/12/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/16/19 2:40 EEHg/L0.16 11/12/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/16/19 2:40 EEHg/L0.41 11/12/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/16/19 2:40 EEHg/L0.32 11/12/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/16/19 2:40 EEHg/L0.13 11/12/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/16/19 2:40 EEHg/L0.31 11/12/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/16/19 2:40 EEHg/L0.20 11/12/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/16/19 2:40 EEHg/L0.11 11/12/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/16/19 2:40 EEHg/L0.20 11/12/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/16/19 2:40 EEHg/L0.16 11/12/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/16/19 2:40 EEHg/L0.13 11/12/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/16/19 2:40 EEHg/L0.23 11/12/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/16/19 2:40 EEHg/L0.17 11/12/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/16/19 2:40 EEHg/L0.13 11/12/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/16/19 2:40 EEHg/L1.5 11/12/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/16/19 2:40 EEHg/L0.17 11/12/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/16/19 2:40 EEHg/L0.20 11/12/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
Page 39 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-13
Field Sample #: MW-12
Sample Matrix: Ground Water
Sampled: 11/7/2019 11:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 11/16/19 2:40 EEHg/L0.25 11/12/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/16/19 2:40 EEHg/L0.34 11/12/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/16/19 2:40 EEHg/L1.7 11/12/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 11/16/19 2:40 EEHg/L0.31 11/12/19SM21-22 6200B1Naphthalene
ND 0.50 11/16/19 2:40 EEHg/L0.13 11/12/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/16/19 2:40 EEHg/L0.11 11/12/19SM21-22 6200B1Styrene
ND 0.50 11/16/19 2:40 EEHg/L0.27 11/12/19SM21-22 6200B11,1,1,2-Tetrachloroethane
ND 0.50 11/16/19 2:40 EEHg/L0.22 11/12/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/16/19 2:40 EEHg/L0.18 11/12/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/16/19 2:40 EEHg/L0.14 11/12/19SM21-22 6200B1Toluene
ND 2.0 11/16/19 2:40 EEHg/L0.57 11/12/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/16/19 2:40 EEHg/L0.40 11/12/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/16/19 2:40 EEHg/L0.20 11/12/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/16/19 2:40 EEHg/L0.16 11/12/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/16/19 2:40 EEHg/L0.24 11/12/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/16/19 2:40 EEHg/L0.33 11/12/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/16/19 2:40 EEHg/L0.25 11/12/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/16/19 2:40 EEHg/L0.18 11/12/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/16/19 2:40 EEHg/L0.14 11/12/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/16/19 2:40 EEHg/L10 11/12/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/16/19 2:40 EEHg/L0.45 11/12/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/16/19 2:40 EEHg/L0.30 11/12/19SM21-22 6200B1m+p Xylene
ND 0.50 11/16/19 2:40 EEHg/L0.17 11/12/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 87.0 11/16/19 2:4070-130
Toluene-d8 97.5 11/16/19 2:4070-130
4-Bromofluorobenzene 97.0 11/16/19 2:4070-130
Page 40 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-14
Field Sample #: MW-14
Sample Matrix: Ground Water
Sampled: 11/7/2019 11:35
[TOC_2]19K0568-14[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 25000 11/14/19 18:43 EEHg/L1900 11/13/19SM21-22 6200B500Acetone
ND 500 11/14/19 18:43 EEHg/L70 11/13/19SM21-22 6200B500L-04tert-Amyl Methyl Ether (TAME)
10000 250 11/14/19 18:43 EEHg/L90 11/13/19SM21-22 6200B500Benzene
ND 250 11/14/19 18:43 EEHg/L75 11/13/19SM21-22 6200B500Bromobenzene
ND 250 11/14/19 18:43 EEHg/L160 11/13/19SM21-22 6200B500Bromochloromethane
ND 250 11/14/19 18:43 EEHg/L80 11/13/19SM21-22 6200B500Bromodichloromethane
ND 250 11/14/19 18:43 EEHg/L230 11/13/19SM21-22 6200B500Bromoform
ND 500 11/14/19 18:43 EEHg/L390 11/13/19SM21-22 6200B500Bromomethane
1700 2500 11/14/19 18:43 EEHg/L970 11/13/19SM21-22 6200B500J2-Butanone (MEK)
ND 10000 11/14/19 18:43 EEHg/L2100 11/13/19SM21-22 6200B500tert-Butyl Alcohol (TBA)
ND 250 11/14/19 18:43 EEHg/L100 11/13/19SM21-22 6200B500n-Butylbenzene
ND 250 11/14/19 18:43 EEHg/L80 11/13/19SM21-22 6200B500sec-Butylbenzene
ND 250 11/14/19 18:43 EEHg/L85 11/13/19SM21-22 6200B500tert-Butylbenzene
ND 250 11/14/19 18:43 EEHg/L80 11/13/19SM21-22 6200B500L-04tert-Butyl Ethyl Ether (TBEE)
ND 250 11/14/19 18:43 EEHg/L55 11/13/19SM21-22 6200B500Carbon Tetrachloride
ND 250 11/14/19 18:43 EEHg/L75 11/13/19SM21-22 6200B500Chlorobenzene
ND 25000 11/14/19 18:43 EEHg/L5300 11/13/19SM21-22 6200B500Ethanol
ND 250 11/14/19 18:43 EEHg/L100 11/13/19SM21-22 6200B500Chlorodibromomethane
ND 250 11/14/19 18:43 EEHg/L180 11/13/19SM21-22 6200B500Chloroethane
ND 250 11/14/19 18:43 EEHg/L85 11/13/19SM21-22 6200B500Chloroform
ND 500 11/14/19 18:43 EEHg/L220 11/13/19SM21-22 6200B500Chloromethane
ND 250 11/14/19 18:43 EEHg/L60 11/13/19SM21-22 6200B5002-Chlorotoluene
ND 250 11/14/19 18:43 EEHg/L70 11/13/19SM21-22 6200B5004-Chlorotoluene
ND 250 11/14/19 18:43 EEHg/L95 11/13/19SM21-22 6200B5001,2-Dibromoethane (EDB)
ND 250 11/14/19 18:43 EEHg/L80 11/13/19SM21-22 6200B5001,2-Dichlorobenzene
ND 250 11/14/19 18:43 EEHg/L60 11/13/19SM21-22 6200B5001,3-Dichlorobenzene
ND 250 11/14/19 18:43 EEHg/L65 11/13/19SM21-22 6200B5001,4-Dichlorobenzene
ND 250 11/14/19 18:43 EEHg/L130 11/13/19SM21-22 6200B500Dichlorodifluoromethane (Freon 12)
ND 250 11/14/19 18:43 EEHg/L80 11/13/19SM21-22 6200B5001,1-Dichloroethane
ND 500 11/14/19 18:43 EEHg/L200 11/13/19SM21-22 6200B5001,2-Dichloroethane
ND 250 11/14/19 18:43 EEHg/L160 11/13/19SM21-22 6200B5001,1-Dichloroethylene
ND 250 11/14/19 18:43 EEHg/L65 11/13/19SM21-22 6200B500cis-1,2-Dichloroethylene
ND 250 11/14/19 18:43 EEHg/L160 11/13/19SM21-22 6200B500trans-1,2-Dichloroethylene
ND 250 11/14/19 18:43 EEHg/L100 11/13/19SM21-22 6200B5001,2-Dichloropropane
ND 250 11/14/19 18:43 EEHg/L55 11/13/19SM21-22 6200B5001,3-Dichloropropane
ND 250 11/14/19 18:43 EEHg/L100 11/13/19SM21-22 6200B5002,2-Dichloropropane
ND 250 11/14/19 18:43 EEHg/L80 11/13/19SM21-22 6200B5001,1-Dichloropropene
ND 250 11/14/19 18:43 EEHg/L65 11/13/19SM21-22 6200B500cis-1,3-Dichloropropene
ND 250 11/14/19 18:43 EEHg/L120 11/13/19SM21-22 6200B500trans-1,3-Dichloropropene
160 250 11/14/19 18:43 EEHg/L85 11/13/19SM21-22 6200B500JDiisopropyl Ether (DIPE)
3000 250 11/14/19 18:43 EEHg/L65 11/13/19SM21-22 6200B500Ethylbenzene
ND 2500 11/14/19 18:43 EEHg/L760 11/13/19SM21-22 6200B5002-Hexanone (MBK)
95 250 11/14/19 18:43 EEHg/L85 11/13/19SM21-22 6200B500JIsopropylbenzene (Cumene)
ND 250 11/14/19 18:43 EEHg/L100 11/13/19SM21-22 6200B500p-Isopropyltoluene (p-Cymene)
Page 41 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-14
Field Sample #: MW-14
Sample Matrix: Ground Water
Sampled: 11/7/2019 11:35
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 250 11/14/19 18:43 EEHg/L120 11/13/19SM21-22 6200B500Methyl tert-Butyl Ether (MTBE)
ND 2500 11/14/19 18:43 EEHg/L170 11/13/19SM21-22 6200B500Methylene Chloride
ND 2500 11/14/19 18:43 EEHg/L840 11/13/19SM21-22 6200B5004-Methyl-2-pentanone (MIBK)
ND 2500 11/14/19 18:43 EEHg/L160 11/13/19SM21-22 6200B500Naphthalene
280 250 11/14/19 18:43 EEHg/L65 11/13/19SM21-22 6200B500n-Propylbenzene
ND 250 11/14/19 18:43 EEHg/L55 11/13/19SM21-22 6200B500Styrene
ND 250 11/14/19 18:43 EEHg/L140 11/13/19SM21-22 6200B5001,1,1,2-Tetrachloroethane
ND 250 11/14/19 18:43 EEHg/L110 11/13/19SM21-22 6200B5001,1,2,2-Tetrachloroethane
ND 250 11/14/19 18:43 EEHg/L90 11/13/19SM21-22 6200B500Tetrachloroethylene
32000 250 11/14/19 18:43 EEHg/L70 11/13/19SM21-22 6200B500Toluene
ND 500 11/14/19 18:43 EEHg/L280 11/13/19SM21-22 6200B5001,2,3-Trichlorobenzene
ND 250 11/14/19 18:43 EEHg/L200 11/13/19SM21-22 6200B5001,2,4-Trichlorobenzene
ND 250 11/14/19 18:43 EEHg/L100 11/13/19SM21-22 6200B5001,1,1-Trichloroethane
ND 250 11/14/19 18:43 EEHg/L80 11/13/19SM21-22 6200B5001,1,2-Trichloroethane
ND 250 11/14/19 18:43 EEHg/L120 11/13/19SM21-22 6200B500Trichloroethylene
ND 250 11/14/19 18:43 EEHg/L160 11/13/19SM21-22 6200B500Trichlorofluoromethane (Freon 11)
ND 250 11/14/19 18:43 EEHg/L120 11/13/19SM21-22 6200B5001,2,3-Trichloropropane
1800 250 11/14/19 18:43 EEHg/L90 11/13/19SM21-22 6200B5001,2,4-Trimethylbenzene
530 250 11/14/19 18:43 EEHg/L70 11/13/19SM21-22 6200B5001,3,5-Trimethylbenzene
ND 10000 11/14/19 18:43 EEHg/L5100 11/13/19SM21-22 6200B500L-04Vinyl Acetate
ND 250 11/14/19 18:43 EEHg/L220 11/13/19SM21-22 6200B500Vinyl Chloride
9600 500 11/14/19 18:43 EEHg/L150 11/13/19SM21-22 6200B500m+p Xylene
4700 250 11/14/19 18:43 EEHg/L85 11/13/19SM21-22 6200B500o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 91.8 11/14/19 18:4370-130
Toluene-d8 97.4 11/14/19 18:4370-130
4-Bromofluorobenzene 101 11/14/19 18:4370-130
Page 42 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-15
Field Sample #: MW-15
Sample Matrix: Ground Water
Sampled: 11/7/2019 11:55
[TOC_2]19K0568-15[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 20000 11/14/19 19:12 EEHg/L1500 11/13/19SM21-22 6200B400Acetone
ND 400 11/14/19 19:12 EEHg/L56 11/13/19SM21-22 6200B400L-04tert-Amyl Methyl Ether (TAME)
840 200 11/14/19 19:12 EEHg/L72 11/13/19SM21-22 6200B400Benzene
ND 200 11/14/19 19:12 EEHg/L60 11/13/19SM21-22 6200B400Bromobenzene
ND 200 11/14/19 19:12 EEHg/L130 11/13/19SM21-22 6200B400Bromochloromethane
ND 200 11/14/19 19:12 EEHg/L64 11/13/19SM21-22 6200B400Bromodichloromethane
ND 200 11/14/19 19:12 EEHg/L180 11/13/19SM21-22 6200B400Bromoform
ND 400 11/14/19 19:12 EEHg/L310 11/13/19SM21-22 6200B400Bromomethane
ND 2000 11/14/19 19:12 EEHg/L780 11/13/19SM21-22 6200B4002-Butanone (MEK)
ND 8000 11/14/19 19:12 EEHg/L1700 11/13/19SM21-22 6200B400tert-Butyl Alcohol (TBA)
ND 200 11/14/19 19:12 EEHg/L84 11/13/19SM21-22 6200B400n-Butylbenzene
ND 200 11/14/19 19:12 EEHg/L64 11/13/19SM21-22 6200B400sec-Butylbenzene
ND 200 11/14/19 19:12 EEHg/L68 11/13/19SM21-22 6200B400tert-Butylbenzene
ND 200 11/14/19 19:12 EEHg/L64 11/13/19SM21-22 6200B400L-04tert-Butyl Ethyl Ether (TBEE)
ND 200 11/14/19 19:12 EEHg/L44 11/13/19SM21-22 6200B400Carbon Tetrachloride
ND 200 11/14/19 19:12 EEHg/L60 11/13/19SM21-22 6200B400Chlorobenzene
ND 20000 11/14/19 19:12 EEHg/L4200 11/13/19SM21-22 6200B400Ethanol
ND 200 11/14/19 19:12 EEHg/L84 11/13/19SM21-22 6200B400Chlorodibromomethane
ND 200 11/14/19 19:12 EEHg/L140 11/13/19SM21-22 6200B400Chloroethane
ND 200 11/14/19 19:12 EEHg/L68 11/13/19SM21-22 6200B400Chloroform
ND 400 11/14/19 19:12 EEHg/L180 11/13/19SM21-22 6200B400Chloromethane
ND 200 11/14/19 19:12 EEHg/L48 11/13/19SM21-22 6200B4002-Chlorotoluene
ND 200 11/14/19 19:12 EEHg/L56 11/13/19SM21-22 6200B4004-Chlorotoluene
ND 200 11/14/19 19:12 EEHg/L76 11/13/19SM21-22 6200B4001,2-Dibromoethane (EDB)
ND 200 11/14/19 19:12 EEHg/L64 11/13/19SM21-22 6200B4001,2-Dichlorobenzene
ND 200 11/14/19 19:12 EEHg/L48 11/13/19SM21-22 6200B4001,3-Dichlorobenzene
ND 200 11/14/19 19:12 EEHg/L52 11/13/19SM21-22 6200B4001,4-Dichlorobenzene
ND 200 11/14/19 19:12 EEHg/L100 11/13/19SM21-22 6200B400Dichlorodifluoromethane (Freon 12)
ND 200 11/14/19 19:12 EEHg/L64 11/13/19SM21-22 6200B4001,1-Dichloroethane
ND 400 11/14/19 19:12 EEHg/L160 11/13/19SM21-22 6200B4001,2-Dichloroethane
ND 200 11/14/19 19:12 EEHg/L130 11/13/19SM21-22 6200B4001,1-Dichloroethylene
ND 200 11/14/19 19:12 EEHg/L52 11/13/19SM21-22 6200B400cis-1,2-Dichloroethylene
ND 200 11/14/19 19:12 EEHg/L120 11/13/19SM21-22 6200B400trans-1,2-Dichloroethylene
ND 200 11/14/19 19:12 EEHg/L80 11/13/19SM21-22 6200B4001,2-Dichloropropane
ND 200 11/14/19 19:12 EEHg/L44 11/13/19SM21-22 6200B4001,3-Dichloropropane
ND 200 11/14/19 19:12 EEHg/L80 11/13/19SM21-22 6200B4002,2-Dichloropropane
ND 200 11/14/19 19:12 EEHg/L64 11/13/19SM21-22 6200B4001,1-Dichloropropene
ND 200 11/14/19 19:12 EEHg/L52 11/13/19SM21-22 6200B400cis-1,3-Dichloropropene
ND 200 11/14/19 19:12 EEHg/L92 11/13/19SM21-22 6200B400trans-1,3-Dichloropropene
ND 200 11/14/19 19:12 EEHg/L68 11/13/19SM21-22 6200B400Diisopropyl Ether (DIPE)
3000 200 11/14/19 19:12 EEHg/L52 11/13/19SM21-22 6200B400Ethylbenzene
ND 2000 11/14/19 19:12 EEHg/L610 11/13/19SM21-22 6200B4002-Hexanone (MBK)
88 200 11/14/19 19:12 EEHg/L68 11/13/19SM21-22 6200B400JIsopropylbenzene (Cumene)
ND 200 11/14/19 19:12 EEHg/L80 11/13/19SM21-22 6200B400p-Isopropyltoluene (p-Cymene)
Page 43 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-15
Field Sample #: MW-15
Sample Matrix: Ground Water
Sampled: 11/7/2019 11:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 200 11/14/19 19:12 EEHg/L100 11/13/19SM21-22 6200B400Methyl tert-Butyl Ether (MTBE)
ND 2000 11/14/19 19:12 EEHg/L140 11/13/19SM21-22 6200B400Methylene Chloride
ND 2000 11/14/19 19:12 EEHg/L670 11/13/19SM21-22 6200B4004-Methyl-2-pentanone (MIBK)
ND 2000 11/14/19 19:12 EEHg/L120 11/13/19SM21-22 6200B400Naphthalene
280 200 11/14/19 19:12 EEHg/L52 11/13/19SM21-22 6200B400n-Propylbenzene
170 200 11/14/19 19:12 EEHg/L44 11/13/19SM21-22 6200B400JStyrene
ND 200 11/14/19 19:12 EEHg/L110 11/13/19SM21-22 6200B4001,1,1,2-Tetrachloroethane
ND 200 11/14/19 19:12 EEHg/L88 11/13/19SM21-22 6200B4001,1,2,2-Tetrachloroethane
ND 200 11/14/19 19:12 EEHg/L72 11/13/19SM21-22 6200B400Tetrachloroethylene
29000 200 11/14/19 19:12 EEHg/L56 11/13/19SM21-22 6200B400Toluene
ND 400 11/14/19 19:12 EEHg/L230 11/13/19SM21-22 6200B4001,2,3-Trichlorobenzene
ND 200 11/14/19 19:12 EEHg/L160 11/13/19SM21-22 6200B4001,2,4-Trichlorobenzene
ND 200 11/14/19 19:12 EEHg/L80 11/13/19SM21-22 6200B4001,1,1-Trichloroethane
ND 200 11/14/19 19:12 EEHg/L64 11/13/19SM21-22 6200B4001,1,2-Trichloroethane
ND 200 11/14/19 19:12 EEHg/L96 11/13/19SM21-22 6200B400Trichloroethylene
ND 200 11/14/19 19:12 EEHg/L130 11/13/19SM21-22 6200B400Trichlorofluoromethane (Freon 11)
ND 200 11/14/19 19:12 EEHg/L100 11/13/19SM21-22 6200B4001,2,3-Trichloropropane
1900 200 11/14/19 19:12 EEHg/L72 11/13/19SM21-22 6200B4001,2,4-Trimethylbenzene
560 200 11/14/19 19:12 EEHg/L56 11/13/19SM21-22 6200B4001,3,5-Trimethylbenzene
ND 8000 11/14/19 19:12 EEHg/L4100 11/13/19SM21-22 6200B400L-04Vinyl Acetate
ND 200 11/14/19 19:12 EEHg/L180 11/13/19SM21-22 6200B400Vinyl Chloride
9800 400 11/14/19 19:12 EEHg/L120 11/13/19SM21-22 6200B400m+p Xylene
4700 200 11/14/19 19:12 EEHg/L68 11/13/19SM21-22 6200B400o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 89.5 11/14/19 19:1270-130
Toluene-d8 96.6 11/14/19 19:1270-130
4-Bromofluorobenzene 99.6 11/14/19 19:1270-130
Page 44 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-16
Field Sample #: MW-17
Sample Matrix: Ground Water
Sampled: 11/7/2019 12:30
[TOC_2]19K0568-16[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 5000 11/16/19 6:30 EEHg/L380 11/12/19SM21-22 6200B100Acetone
ND 100 11/16/19 6:30 EEHg/L14 11/12/19SM21-22 6200B100L-04tert-Amyl Methyl Ether (TAME)
61 50 11/16/19 6:30 EEHg/L18 11/12/19SM21-22 6200B100Benzene
ND 50 11/16/19 6:30 EEHg/L15 11/12/19SM21-22 6200B100Bromobenzene
ND 50 11/16/19 6:30 EEHg/L32 11/12/19SM21-22 6200B100Bromochloromethane
ND 50 11/16/19 6:30 EEHg/L16 11/12/19SM21-22 6200B100Bromodichloromethane
ND 50 11/16/19 6:30 EEHg/L46 11/12/19SM21-22 6200B100Bromoform
ND 100 11/16/19 6:30 EEHg/L78 11/12/19SM21-22 6200B100Bromomethane
ND 500 11/16/19 6:30 EEHg/L190 11/12/19SM21-22 6200B1002-Butanone (MEK)
ND 2000 11/16/19 6:30 EEHg/L420 11/12/19SM21-22 6200B100tert-Butyl Alcohol (TBA)
ND 50 11/16/19 6:30 EEHg/L21 11/12/19SM21-22 6200B100n-Butylbenzene
ND 50 11/16/19 6:30 EEHg/L16 11/12/19SM21-22 6200B100sec-Butylbenzene
ND 50 11/16/19 6:30 EEHg/L17 11/12/19SM21-22 6200B100tert-Butylbenzene
ND 50 11/16/19 6:30 EEHg/L16 11/12/19SM21-22 6200B100L-04tert-Butyl Ethyl Ether (TBEE)
ND 50 11/16/19 6:30 EEHg/L11 11/12/19SM21-22 6200B100Carbon Tetrachloride
ND 50 11/16/19 6:30 EEHg/L15 11/12/19SM21-22 6200B100Chlorobenzene
ND 5000 11/16/19 6:30 EEHg/L1100 11/12/19SM21-22 6200B100Ethanol
ND 50 11/16/19 6:30 EEHg/L21 11/12/19SM21-22 6200B100Chlorodibromomethane
ND 50 11/16/19 6:30 EEHg/L35 11/12/19SM21-22 6200B100Chloroethane
ND 50 11/16/19 6:30 EEHg/L17 11/12/19SM21-22 6200B100Chloroform
ND 100 11/16/19 6:30 EEHg/L45 11/12/19SM21-22 6200B100Chloromethane
ND 50 11/16/19 6:30 EEHg/L12 11/12/19SM21-22 6200B1002-Chlorotoluene
ND 50 11/16/19 6:30 EEHg/L14 11/12/19SM21-22 6200B1004-Chlorotoluene
ND 50 11/16/19 6:30 EEHg/L19 11/12/19SM21-22 6200B1001,2-Dibromoethane (EDB)
ND 50 11/16/19 6:30 EEHg/L16 11/12/19SM21-22 6200B1001,2-Dichlorobenzene
ND 50 11/16/19 6:30 EEHg/L12 11/12/19SM21-22 6200B1001,3-Dichlorobenzene
ND 50 11/16/19 6:30 EEHg/L13 11/12/19SM21-22 6200B1001,4-Dichlorobenzene
ND 50 11/16/19 6:30 EEHg/L26 11/12/19SM21-22 6200B100Dichlorodifluoromethane (Freon 12)
ND 50 11/16/19 6:30 EEHg/L16 11/12/19SM21-22 6200B1001,1-Dichloroethane
ND 100 11/16/19 6:30 EEHg/L41 11/12/19SM21-22 6200B1001,2-Dichloroethane
ND 50 11/16/19 6:30 EEHg/L32 11/12/19SM21-22 6200B1001,1-Dichloroethylene
ND 50 11/16/19 6:30 EEHg/L13 11/12/19SM21-22 6200B100cis-1,2-Dichloroethylene
ND 50 11/16/19 6:30 EEHg/L31 11/12/19SM21-22 6200B100trans-1,2-Dichloroethylene
ND 50 11/16/19 6:30 EEHg/L20 11/12/19SM21-22 6200B1001,2-Dichloropropane
ND 50 11/16/19 6:30 EEHg/L11 11/12/19SM21-22 6200B1001,3-Dichloropropane
ND 50 11/16/19 6:30 EEHg/L20 11/12/19SM21-22 6200B1002,2-Dichloropropane
ND 50 11/16/19 6:30 EEHg/L16 11/12/19SM21-22 6200B1001,1-Dichloropropene
ND 50 11/16/19 6:30 EEHg/L13 11/12/19SM21-22 6200B100cis-1,3-Dichloropropene
ND 50 11/16/19 6:30 EEHg/L23 11/12/19SM21-22 6200B100trans-1,3-Dichloropropene
ND 50 11/16/19 6:30 EEHg/L17 11/12/19SM21-22 6200B100Diisopropyl Ether (DIPE)
1800 50 11/16/19 6:30 EEHg/L13 11/12/19SM21-22 6200B100Ethylbenzene
ND 500 11/16/19 6:30 EEHg/L150 11/12/19SM21-22 6200B1002-Hexanone (MBK)
47 50 11/16/19 6:30 EEHg/L17 11/12/19SM21-22 6200B100JIsopropylbenzene (Cumene)
ND 50 11/16/19 6:30 EEHg/L20 11/12/19SM21-22 6200B100p-Isopropyltoluene (p-Cymene)
Page 45 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-16
Field Sample #: MW-17
Sample Matrix: Ground Water
Sampled: 11/7/2019 12:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 50 11/16/19 6:30 EEHg/L25 11/12/19SM21-22 6200B100Methyl tert-Butyl Ether (MTBE)
ND 500 11/16/19 6:30 EEHg/L34 11/12/19SM21-22 6200B100Methylene Chloride
ND 500 11/16/19 6:30 EEHg/L170 11/12/19SM21-22 6200B1004-Methyl-2-pentanone (MIBK)
550 500 11/16/19 6:30 EEHg/L31 11/12/19SM21-22 6200B100Naphthalene
140 50 11/16/19 6:30 EEHg/L13 11/12/19SM21-22 6200B100n-Propylbenzene
19 50 11/16/19 6:30 EEHg/L11 11/12/19SM21-22 6200B100JStyrene
ND 50 11/16/19 6:30 EEHg/L27 11/12/19SM21-22 6200B1001,1,1,2-Tetrachloroethane
ND 50 11/16/19 6:30 EEHg/L22 11/12/19SM21-22 6200B1001,1,2,2-Tetrachloroethane
ND 50 11/16/19 6:30 EEHg/L18 11/12/19SM21-22 6200B100Tetrachloroethylene
3500 50 11/16/19 6:30 EEHg/L14 11/12/19SM21-22 6200B100Toluene
ND 200 11/16/19 6:30 EEHg/L57 11/12/19SM21-22 6200B1001,2,3-Trichlorobenzene
ND 50 11/16/19 6:30 EEHg/L40 11/12/19SM21-22 6200B1001,2,4-Trichlorobenzene
ND 50 11/16/19 6:30 EEHg/L20 11/12/19SM21-22 6200B1001,1,1-Trichloroethane
ND 50 11/16/19 6:30 EEHg/L16 11/12/19SM21-22 6200B1001,1,2-Trichloroethane
ND 50 11/16/19 6:30 EEHg/L24 11/12/19SM21-22 6200B100Trichloroethylene
ND 50 11/16/19 6:30 EEHg/L33 11/12/19SM21-22 6200B100Trichlorofluoromethane (Freon 11)
ND 50 11/16/19 6:30 EEHg/L25 11/12/19SM21-22 6200B1001,2,3-Trichloropropane
1000 50 11/16/19 6:30 EEHg/L18 11/12/19SM21-22 6200B1001,2,4-Trimethylbenzene
270 50 11/16/19 6:30 EEHg/L14 11/12/19SM21-22 6200B1001,3,5-Trimethylbenzene
ND 2000 11/16/19 6:30 EEHg/L1000 11/12/19SM21-22 6200B100Vinyl Acetate
ND 50 11/16/19 6:30 EEHg/L45 11/12/19SM21-22 6200B100Vinyl Chloride
4500 100 11/16/19 6:30 EEHg/L30 11/12/19SM21-22 6200B100m+p Xylene
1900 50 11/16/19 6:30 EEHg/L17 11/12/19SM21-22 6200B100o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 86.7 11/16/19 6:3070-130
Toluene-d8 98.4 11/16/19 6:3070-130
4-Bromofluorobenzene 102 11/16/19 6:3070-130
Page 46 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-17
Field Sample #: MW-18
Sample Matrix: Ground Water
Sampled: 11/7/2019 12:55
[TOC_2]19K0568-17[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 5000 11/16/19 7:00 EEHg/L380 11/12/19SM21-22 6200B100Acetone
ND 100 11/16/19 7:00 EEHg/L14 11/12/19SM21-22 6200B100L-04tert-Amyl Methyl Ether (TAME)
420 50 11/16/19 7:00 EEHg/L18 11/12/19SM21-22 6200B100Benzene
ND 50 11/16/19 7:00 EEHg/L15 11/12/19SM21-22 6200B100Bromobenzene
ND 50 11/16/19 7:00 EEHg/L32 11/12/19SM21-22 6200B100Bromochloromethane
ND 50 11/16/19 7:00 EEHg/L16 11/12/19SM21-22 6200B100Bromodichloromethane
ND 50 11/16/19 7:00 EEHg/L46 11/12/19SM21-22 6200B100Bromoform
ND 100 11/16/19 7:00 EEHg/L78 11/12/19SM21-22 6200B100Bromomethane
ND 500 11/16/19 7:00 EEHg/L190 11/12/19SM21-22 6200B1002-Butanone (MEK)
ND 2000 11/16/19 7:00 EEHg/L420 11/12/19SM21-22 6200B100tert-Butyl Alcohol (TBA)
31 50 11/16/19 7:00 EEHg/L21 11/12/19SM21-22 6200B100Jn-Butylbenzene
ND 50 11/16/19 7:00 EEHg/L16 11/12/19SM21-22 6200B100sec-Butylbenzene
ND 50 11/16/19 7:00 EEHg/L17 11/12/19SM21-22 6200B100tert-Butylbenzene
ND 50 11/16/19 7:00 EEHg/L16 11/12/19SM21-22 6200B100L-04tert-Butyl Ethyl Ether (TBEE)
ND 50 11/16/19 7:00 EEHg/L11 11/12/19SM21-22 6200B100Carbon Tetrachloride
ND 50 11/16/19 7:00 EEHg/L15 11/12/19SM21-22 6200B100Chlorobenzene
ND 5000 11/16/19 7:00 EEHg/L1100 11/12/19SM21-22 6200B100Ethanol
ND 50 11/16/19 7:00 EEHg/L21 11/12/19SM21-22 6200B100Chlorodibromomethane
ND 50 11/16/19 7:00 EEHg/L35 11/12/19SM21-22 6200B100Chloroethane
ND 50 11/16/19 7:00 EEHg/L17 11/12/19SM21-22 6200B100Chloroform
ND 100 11/16/19 7:00 EEHg/L45 11/12/19SM21-22 6200B100Chloromethane
ND 50 11/16/19 7:00 EEHg/L12 11/12/19SM21-22 6200B1002-Chlorotoluene
ND 50 11/16/19 7:00 EEHg/L14 11/12/19SM21-22 6200B1004-Chlorotoluene
ND 50 11/16/19 7:00 EEHg/L19 11/12/19SM21-22 6200B1001,2-Dibromoethane (EDB)
ND 50 11/16/19 7:00 EEHg/L16 11/12/19SM21-22 6200B1001,2-Dichlorobenzene
ND 50 11/16/19 7:00 EEHg/L12 11/12/19SM21-22 6200B1001,3-Dichlorobenzene
ND 50 11/16/19 7:00 EEHg/L13 11/12/19SM21-22 6200B1001,4-Dichlorobenzene
ND 50 11/16/19 7:00 EEHg/L26 11/12/19SM21-22 6200B100Dichlorodifluoromethane (Freon 12)
ND 50 11/16/19 7:00 EEHg/L16 11/12/19SM21-22 6200B1001,1-Dichloroethane
ND 100 11/16/19 7:00 EEHg/L41 11/12/19SM21-22 6200B1001,2-Dichloroethane
ND 50 11/16/19 7:00 EEHg/L32 11/12/19SM21-22 6200B1001,1-Dichloroethylene
ND 50 11/16/19 7:00 EEHg/L13 11/12/19SM21-22 6200B100cis-1,2-Dichloroethylene
ND 50 11/16/19 7:00 EEHg/L31 11/12/19SM21-22 6200B100trans-1,2-Dichloroethylene
ND 50 11/16/19 7:00 EEHg/L20 11/12/19SM21-22 6200B1001,2-Dichloropropane
ND 50 11/16/19 7:00 EEHg/L11 11/12/19SM21-22 6200B1001,3-Dichloropropane
ND 50 11/16/19 7:00 EEHg/L20 11/12/19SM21-22 6200B1002,2-Dichloropropane
ND 50 11/16/19 7:00 EEHg/L16 11/12/19SM21-22 6200B1001,1-Dichloropropene
ND 50 11/16/19 7:00 EEHg/L13 11/12/19SM21-22 6200B100cis-1,3-Dichloropropene
ND 50 11/16/19 7:00 EEHg/L23 11/12/19SM21-22 6200B100trans-1,3-Dichloropropene
ND 50 11/16/19 7:00 EEHg/L17 11/12/19SM21-22 6200B100Diisopropyl Ether (DIPE)
2500 50 11/16/19 7:00 EEHg/L13 11/12/19SM21-22 6200B100Ethylbenzene
ND 500 11/16/19 7:00 EEHg/L150 11/12/19SM21-22 6200B1002-Hexanone (MBK)
76 50 11/16/19 7:00 EEHg/L17 11/12/19SM21-22 6200B100Isopropylbenzene (Cumene)
ND 50 11/16/19 7:00 EEHg/L20 11/12/19SM21-22 6200B100p-Isopropyltoluene (p-Cymene)
Page 47 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-17
Field Sample #: MW-18
Sample Matrix: Ground Water
Sampled: 11/7/2019 12:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 50 11/16/19 7:00 EEHg/L25 11/12/19SM21-22 6200B100Methyl tert-Butyl Ether (MTBE)
ND 500 11/16/19 7:00 EEHg/L34 11/12/19SM21-22 6200B100Methylene Chloride
ND 500 11/16/19 7:00 EEHg/L170 11/12/19SM21-22 6200B1004-Methyl-2-pentanone (MIBK)
690 500 11/16/19 7:00 EEHg/L31 11/12/19SM21-22 6200B100Naphthalene
250 50 11/16/19 7:00 EEHg/L13 11/12/19SM21-22 6200B100n-Propylbenzene
ND 50 11/16/19 7:00 EEHg/L11 11/12/19SM21-22 6200B100Styrene
ND 50 11/16/19 7:00 EEHg/L27 11/12/19SM21-22 6200B1001,1,1,2-Tetrachloroethane
ND 50 11/16/19 7:00 EEHg/L22 11/12/19SM21-22 6200B1001,1,2,2-Tetrachloroethane
ND 50 11/16/19 7:00 EEHg/L18 11/12/19SM21-22 6200B100Tetrachloroethylene
2200 50 11/16/19 7:00 EEHg/L14 11/12/19SM21-22 6200B100Toluene
ND 200 11/16/19 7:00 EEHg/L57 11/12/19SM21-22 6200B1001,2,3-Trichlorobenzene
ND 50 11/16/19 7:00 EEHg/L40 11/12/19SM21-22 6200B1001,2,4-Trichlorobenzene
ND 50 11/16/19 7:00 EEHg/L20 11/12/19SM21-22 6200B1001,1,1-Trichloroethane
ND 50 11/16/19 7:00 EEHg/L16 11/12/19SM21-22 6200B1001,1,2-Trichloroethane
ND 50 11/16/19 7:00 EEHg/L24 11/12/19SM21-22 6200B100Trichloroethylene
ND 50 11/16/19 7:00 EEHg/L33 11/12/19SM21-22 6200B100Trichlorofluoromethane (Freon 11)
ND 50 11/16/19 7:00 EEHg/L25 11/12/19SM21-22 6200B1001,2,3-Trichloropropane
1800 50 11/16/19 7:00 EEHg/L18 11/12/19SM21-22 6200B1001,2,4-Trimethylbenzene
530 50 11/16/19 7:00 EEHg/L14 11/12/19SM21-22 6200B1001,3,5-Trimethylbenzene
ND 2000 11/16/19 7:00 EEHg/L1000 11/12/19SM21-22 6200B100Vinyl Acetate
ND 50 11/16/19 7:00 EEHg/L45 11/12/19SM21-22 6200B100Vinyl Chloride
2600 100 11/16/19 7:00 EEHg/L30 11/12/19SM21-22 6200B100m+p Xylene
490 50 11/16/19 7:00 EEHg/L17 11/12/19SM21-22 6200B100o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 88.2 11/16/19 7:0070-130
Toluene-d8 100 11/16/19 7:0070-130
4-Bromofluorobenzene 103 11/16/19 7:0070-130
Page 48 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-18
Field Sample #: MW-19
Sample Matrix: Ground Water
Sampled: 11/7/2019 13:20
[TOC_2]19K0568-18[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 10000 11/16/19 7:28 EEHg/L760 11/12/19SM21-22 6200B200Acetone
ND 200 11/16/19 7:28 EEHg/L28 11/12/19SM21-22 6200B200L-04tert-Amyl Methyl Ether (TAME)
ND 100 11/16/19 7:28 EEHg/L36 11/12/19SM21-22 6200B200Benzene
ND 100 11/16/19 7:28 EEHg/L30 11/12/19SM21-22 6200B200Bromobenzene
ND 100 11/16/19 7:28 EEHg/L64 11/12/19SM21-22 6200B200Bromochloromethane
ND 100 11/16/19 7:28 EEHg/L32 11/12/19SM21-22 6200B200Bromodichloromethane
ND 100 11/16/19 7:28 EEHg/L92 11/12/19SM21-22 6200B200Bromoform
ND 200 11/16/19 7:28 EEHg/L160 11/12/19SM21-22 6200B200Bromomethane
ND 1000 11/16/19 7:28 EEHg/L390 11/12/19SM21-22 6200B2002-Butanone (MEK)
ND 4000 11/16/19 7:28 EEHg/L830 11/12/19SM21-22 6200B200tert-Butyl Alcohol (TBA)
50 100 11/16/19 7:28 EEHg/L42 11/12/19SM21-22 6200B200Jn-Butylbenzene
ND 100 11/16/19 7:28 EEHg/L32 11/12/19SM21-22 6200B200sec-Butylbenzene
ND 100 11/16/19 7:28 EEHg/L34 11/12/19SM21-22 6200B200tert-Butylbenzene
ND 100 11/16/19 7:28 EEHg/L32 11/12/19SM21-22 6200B200L-04tert-Butyl Ethyl Ether (TBEE)
ND 100 11/16/19 7:28 EEHg/L22 11/12/19SM21-22 6200B200Carbon Tetrachloride
ND 100 11/16/19 7:28 EEHg/L30 11/12/19SM21-22 6200B200Chlorobenzene
ND 10000 11/16/19 7:28 EEHg/L2100 11/12/19SM21-22 6200B200Ethanol
ND 100 11/16/19 7:28 EEHg/L42 11/12/19SM21-22 6200B200Chlorodibromomethane
ND 100 11/16/19 7:28 EEHg/L70 11/12/19SM21-22 6200B200Chloroethane
ND 100 11/16/19 7:28 EEHg/L34 11/12/19SM21-22 6200B200Chloroform
ND 200 11/16/19 7:28 EEHg/L90 11/12/19SM21-22 6200B200Chloromethane
ND 100 11/16/19 7:28 EEHg/L24 11/12/19SM21-22 6200B2002-Chlorotoluene
ND 100 11/16/19 7:28 EEHg/L28 11/12/19SM21-22 6200B2004-Chlorotoluene
ND 100 11/16/19 7:28 EEHg/L38 11/12/19SM21-22 6200B2001,2-Dibromoethane (EDB)
ND 100 11/16/19 7:28 EEHg/L32 11/12/19SM21-22 6200B2001,2-Dichlorobenzene
ND 100 11/16/19 7:28 EEHg/L24 11/12/19SM21-22 6200B2001,3-Dichlorobenzene
ND 100 11/16/19 7:28 EEHg/L26 11/12/19SM21-22 6200B2001,4-Dichlorobenzene
ND 100 11/16/19 7:28 EEHg/L52 11/12/19SM21-22 6200B200Dichlorodifluoromethane (Freon 12)
ND 100 11/16/19 7:28 EEHg/L32 11/12/19SM21-22 6200B2001,1-Dichloroethane
ND 200 11/16/19 7:28 EEHg/L82 11/12/19SM21-22 6200B2001,2-Dichloroethane
ND 100 11/16/19 7:28 EEHg/L64 11/12/19SM21-22 6200B2001,1-Dichloroethylene
ND 100 11/16/19 7:28 EEHg/L26 11/12/19SM21-22 6200B200cis-1,2-Dichloroethylene
ND 100 11/16/19 7:28 EEHg/L62 11/12/19SM21-22 6200B200trans-1,2-Dichloroethylene
ND 100 11/16/19 7:28 EEHg/L40 11/12/19SM21-22 6200B2001,2-Dichloropropane
ND 100 11/16/19 7:28 EEHg/L22 11/12/19SM21-22 6200B2001,3-Dichloropropane
ND 100 11/16/19 7:28 EEHg/L40 11/12/19SM21-22 6200B2002,2-Dichloropropane
ND 100 11/16/19 7:28 EEHg/L32 11/12/19SM21-22 6200B2001,1-Dichloropropene
ND 100 11/16/19 7:28 EEHg/L26 11/12/19SM21-22 6200B200cis-1,3-Dichloropropene
ND 100 11/16/19 7:28 EEHg/L46 11/12/19SM21-22 6200B200trans-1,3-Dichloropropene
ND 100 11/16/19 7:28 EEHg/L34 11/12/19SM21-22 6200B200Diisopropyl Ether (DIPE)
2500 100 11/16/19 7:28 EEHg/L26 11/12/19SM21-22 6200B200Ethylbenzene
ND 1000 11/16/19 7:28 EEHg/L300 11/12/19SM21-22 6200B2002-Hexanone (MBK)
76 100 11/16/19 7:28 EEHg/L34 11/12/19SM21-22 6200B200JIsopropylbenzene (Cumene)
ND 100 11/16/19 7:28 EEHg/L40 11/12/19SM21-22 6200B200p-Isopropyltoluene (p-Cymene)
Page 49 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-18
Field Sample #: MW-19
Sample Matrix: Ground Water
Sampled: 11/7/2019 13:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 100 11/16/19 7:28 EEHg/L50 11/12/19SM21-22 6200B200Methyl tert-Butyl Ether (MTBE)
ND 1000 11/16/19 7:28 EEHg/L68 11/12/19SM21-22 6200B200Methylene Chloride
ND 1000 11/16/19 7:28 EEHg/L330 11/12/19SM21-22 6200B2004-Methyl-2-pentanone (MIBK)
980 1000 11/16/19 7:28 EEHg/L62 11/12/19SM21-22 6200B200JNaphthalene
260 100 11/16/19 7:28 EEHg/L26 11/12/19SM21-22 6200B200n-Propylbenzene
36 100 11/16/19 7:28 EEHg/L22 11/12/19SM21-22 6200B200JStyrene
ND 100 11/16/19 7:28 EEHg/L54 11/12/19SM21-22 6200B2001,1,1,2-Tetrachloroethane
ND 100 11/16/19 7:28 EEHg/L44 11/12/19SM21-22 6200B2001,1,2,2-Tetrachloroethane
ND 100 11/16/19 7:28 EEHg/L36 11/12/19SM21-22 6200B200Tetrachloroethylene
6300 100 11/16/19 7:28 EEHg/L28 11/12/19SM21-22 6200B200Toluene
ND 400 11/16/19 7:28 EEHg/L110 11/12/19SM21-22 6200B2001,2,3-Trichlorobenzene
ND 100 11/16/19 7:28 EEHg/L80 11/12/19SM21-22 6200B2001,2,4-Trichlorobenzene
ND 100 11/16/19 7:28 EEHg/L40 11/12/19SM21-22 6200B2001,1,1-Trichloroethane
ND 100 11/16/19 7:28 EEHg/L32 11/12/19SM21-22 6200B2001,1,2-Trichloroethane
ND 100 11/16/19 7:28 EEHg/L48 11/12/19SM21-22 6200B200Trichloroethylene
ND 100 11/16/19 7:28 EEHg/L66 11/12/19SM21-22 6200B200Trichlorofluoromethane (Freon 11)
ND 100 11/16/19 7:28 EEHg/L50 11/12/19SM21-22 6200B2001,2,3-Trichloropropane
1800 100 11/16/19 7:28 EEHg/L36 11/12/19SM21-22 6200B2001,2,4-Trimethylbenzene
510 100 11/16/19 7:28 EEHg/L28 11/12/19SM21-22 6200B2001,3,5-Trimethylbenzene
ND 4000 11/16/19 7:28 EEHg/L2000 11/12/19SM21-22 6200B200Vinyl Acetate
ND 100 11/16/19 7:28 EEHg/L90 11/12/19SM21-22 6200B200Vinyl Chloride
6500 200 11/16/19 7:28 EEHg/L60 11/12/19SM21-22 6200B200m+p Xylene
1500 100 11/16/19 7:28 EEHg/L34 11/12/19SM21-22 6200B200o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 91.2 11/16/19 7:2870-130
Toluene-d8 96.8 11/16/19 7:2870-130
4-Bromofluorobenzene 101 11/16/19 7:2870-130
Page 50 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-19
Field Sample #: MW-20
Sample Matrix: Ground Water
Sampled: 11/7/2019 13:45
[TOC_2]19K0568-19[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 20000 11/16/19 7:57 EEHg/L1500 11/12/19SM21-22 6200B400Acetone
ND 400 11/16/19 7:57 EEHg/L56 11/12/19SM21-22 6200B400L-04tert-Amyl Methyl Ether (TAME)
150 200 11/16/19 7:57 EEHg/L72 11/12/19SM21-22 6200B400JBenzene
ND 200 11/16/19 7:57 EEHg/L60 11/12/19SM21-22 6200B400Bromobenzene
ND 200 11/16/19 7:57 EEHg/L130 11/12/19SM21-22 6200B400Bromochloromethane
ND 200 11/16/19 7:57 EEHg/L64 11/12/19SM21-22 6200B400Bromodichloromethane
ND 200 11/16/19 7:57 EEHg/L180 11/12/19SM21-22 6200B400Bromoform
ND 400 11/16/19 7:57 EEHg/L310 11/12/19SM21-22 6200B400Bromomethane
ND 2000 11/16/19 7:57 EEHg/L780 11/12/19SM21-22 6200B4002-Butanone (MEK)
ND 8000 11/16/19 7:57 EEHg/L1700 11/12/19SM21-22 6200B400tert-Butyl Alcohol (TBA)
ND 200 11/16/19 7:57 EEHg/L84 11/12/19SM21-22 6200B400n-Butylbenzene
ND 200 11/16/19 7:57 EEHg/L64 11/12/19SM21-22 6200B400sec-Butylbenzene
ND 200 11/16/19 7:57 EEHg/L68 11/12/19SM21-22 6200B400tert-Butylbenzene
ND 200 11/16/19 7:57 EEHg/L64 11/12/19SM21-22 6200B400L-04tert-Butyl Ethyl Ether (TBEE)
ND 200 11/16/19 7:57 EEHg/L44 11/12/19SM21-22 6200B400Carbon Tetrachloride
ND 200 11/16/19 7:57 EEHg/L60 11/12/19SM21-22 6200B400Chlorobenzene
ND 20000 11/16/19 7:57 EEHg/L4200 11/12/19SM21-22 6200B400Ethanol
ND 200 11/16/19 7:57 EEHg/L84 11/12/19SM21-22 6200B400Chlorodibromomethane
ND 200 11/16/19 7:57 EEHg/L140 11/12/19SM21-22 6200B400Chloroethane
ND 200 11/16/19 7:57 EEHg/L68 11/12/19SM21-22 6200B400Chloroform
ND 400 11/16/19 7:57 EEHg/L180 11/12/19SM21-22 6200B400Chloromethane
ND 200 11/16/19 7:57 EEHg/L48 11/12/19SM21-22 6200B4002-Chlorotoluene
ND 200 11/16/19 7:57 EEHg/L56 11/12/19SM21-22 6200B4004-Chlorotoluene
ND 200 11/16/19 7:57 EEHg/L76 11/12/19SM21-22 6200B4001,2-Dibromoethane (EDB)
ND 200 11/16/19 7:57 EEHg/L64 11/12/19SM21-22 6200B4001,2-Dichlorobenzene
ND 200 11/16/19 7:57 EEHg/L48 11/12/19SM21-22 6200B4001,3-Dichlorobenzene
ND 200 11/16/19 7:57 EEHg/L52 11/12/19SM21-22 6200B4001,4-Dichlorobenzene
ND 200 11/16/19 7:57 EEHg/L100 11/12/19SM21-22 6200B400Dichlorodifluoromethane (Freon 12)
ND 200 11/16/19 7:57 EEHg/L64 11/12/19SM21-22 6200B4001,1-Dichloroethane
ND 400 11/16/19 7:57 EEHg/L160 11/12/19SM21-22 6200B4001,2-Dichloroethane
ND 200 11/16/19 7:57 EEHg/L130 11/12/19SM21-22 6200B4001,1-Dichloroethylene
ND 200 11/16/19 7:57 EEHg/L52 11/12/19SM21-22 6200B400cis-1,2-Dichloroethylene
ND 200 11/16/19 7:57 EEHg/L120 11/12/19SM21-22 6200B400trans-1,2-Dichloroethylene
ND 200 11/16/19 7:57 EEHg/L80 11/12/19SM21-22 6200B4001,2-Dichloropropane
ND 200 11/16/19 7:57 EEHg/L44 11/12/19SM21-22 6200B4001,3-Dichloropropane
ND 200 11/16/19 7:57 EEHg/L80 11/12/19SM21-22 6200B4002,2-Dichloropropane
ND 200 11/16/19 7:57 EEHg/L64 11/12/19SM21-22 6200B4001,1-Dichloropropene
ND 200 11/16/19 7:57 EEHg/L52 11/12/19SM21-22 6200B400cis-1,3-Dichloropropene
ND 200 11/16/19 7:57 EEHg/L92 11/12/19SM21-22 6200B400trans-1,3-Dichloropropene
ND 200 11/16/19 7:57 EEHg/L68 11/12/19SM21-22 6200B400Diisopropyl Ether (DIPE)
3300 200 11/16/19 7:57 EEHg/L52 11/12/19SM21-22 6200B400Ethylbenzene
ND 2000 11/16/19 7:57 EEHg/L610 11/12/19SM21-22 6200B4002-Hexanone (MBK)
92 200 11/16/19 7:57 EEHg/L68 11/12/19SM21-22 6200B400JIsopropylbenzene (Cumene)
ND 200 11/16/19 7:57 EEHg/L80 11/12/19SM21-22 6200B400p-Isopropyltoluene (p-Cymene)
Page 51 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-19
Field Sample #: MW-20
Sample Matrix: Ground Water
Sampled: 11/7/2019 13:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 200 11/16/19 7:57 EEHg/L100 11/12/19SM21-22 6200B400Methyl tert-Butyl Ether (MTBE)
ND 2000 11/16/19 7:57 EEHg/L140 11/12/19SM21-22 6200B400Methylene Chloride
ND 2000 11/16/19 7:57 EEHg/L670 11/12/19SM21-22 6200B4004-Methyl-2-pentanone (MIBK)
1900 2000 11/16/19 7:57 EEHg/L120 11/12/19SM21-22 6200B400JNaphthalene
320 200 11/16/19 7:57 EEHg/L52 11/12/19SM21-22 6200B400n-Propylbenzene
190 200 11/16/19 7:57 EEHg/L44 11/12/19SM21-22 6200B400JStyrene
ND 200 11/16/19 7:57 EEHg/L110 11/12/19SM21-22 6200B4001,1,1,2-Tetrachloroethane
ND 200 11/16/19 7:57 EEHg/L88 11/12/19SM21-22 6200B4001,1,2,2-Tetrachloroethane
ND 200 11/16/19 7:57 EEHg/L72 11/12/19SM21-22 6200B400Tetrachloroethylene
23000 200 11/16/19 7:57 EEHg/L56 11/12/19SM21-22 6200B400Toluene
ND 800 11/16/19 7:57 EEHg/L230 11/12/19SM21-22 6200B4001,2,3-Trichlorobenzene
ND 200 11/16/19 7:57 EEHg/L160 11/12/19SM21-22 6200B4001,2,4-Trichlorobenzene
ND 200 11/16/19 7:57 EEHg/L80 11/12/19SM21-22 6200B4001,1,1-Trichloroethane
ND 200 11/16/19 7:57 EEHg/L64 11/12/19SM21-22 6200B4001,1,2-Trichloroethane
ND 200 11/16/19 7:57 EEHg/L96 11/12/19SM21-22 6200B400Trichloroethylene
ND 200 11/16/19 7:57 EEHg/L130 11/12/19SM21-22 6200B400Trichlorofluoromethane (Freon 11)
ND 200 11/16/19 7:57 EEHg/L100 11/12/19SM21-22 6200B4001,2,3-Trichloropropane
2300 200 11/16/19 7:57 EEHg/L72 11/12/19SM21-22 6200B4001,2,4-Trimethylbenzene
650 200 11/16/19 7:57 EEHg/L56 11/12/19SM21-22 6200B4001,3,5-Trimethylbenzene
ND 8000 11/16/19 7:57 EEHg/L4100 11/12/19SM21-22 6200B400Vinyl Acetate
ND 200 11/16/19 7:57 EEHg/L180 11/12/19SM21-22 6200B400Vinyl Chloride
10000 400 11/16/19 7:57 EEHg/L120 11/12/19SM21-22 6200B400m+p Xylene
4200 200 11/16/19 7:57 EEHg/L68 11/12/19SM21-22 6200B400o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 85.9 11/16/19 7:5770-130
Toluene-d8 96.4 11/16/19 7:5770-130
4-Bromofluorobenzene 98.8 11/16/19 7:5770-130
Page 52 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-20
Field Sample #: MW-21
Sample Matrix: Ground Water
Sampled: 11/7/2019 14:10
[TOC_2]19K0568-20[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 20000 11/14/19 19:40 EEHg/L1500 11/13/19SM21-22 6200B400Acetone
ND 400 11/14/19 19:40 EEHg/L56 11/13/19SM21-22 6200B400L-04tert-Amyl Methyl Ether (TAME)
3400 200 11/14/19 19:40 EEHg/L72 11/13/19SM21-22 6200B400Benzene
ND 200 11/14/19 19:40 EEHg/L60 11/13/19SM21-22 6200B400Bromobenzene
ND 200 11/14/19 19:40 EEHg/L130 11/13/19SM21-22 6200B400Bromochloromethane
ND 200 11/14/19 19:40 EEHg/L64 11/13/19SM21-22 6200B400Bromodichloromethane
ND 200 11/14/19 19:40 EEHg/L180 11/13/19SM21-22 6200B400Bromoform
ND 400 11/14/19 19:40 EEHg/L310 11/13/19SM21-22 6200B400Bromomethane
ND 2000 11/14/19 19:40 EEHg/L780 11/13/19SM21-22 6200B4002-Butanone (MEK)
ND 8000 11/14/19 19:40 EEHg/L1700 11/13/19SM21-22 6200B400tert-Butyl Alcohol (TBA)
ND 200 11/14/19 19:40 EEHg/L84 11/13/19SM21-22 6200B400n-Butylbenzene
ND 200 11/14/19 19:40 EEHg/L64 11/13/19SM21-22 6200B400sec-Butylbenzene
ND 200 11/14/19 19:40 EEHg/L68 11/13/19SM21-22 6200B400tert-Butylbenzene
ND 200 11/14/19 19:40 EEHg/L64 11/13/19SM21-22 6200B400L-04tert-Butyl Ethyl Ether (TBEE)
ND 200 11/14/19 19:40 EEHg/L44 11/13/19SM21-22 6200B400Carbon Tetrachloride
ND 200 11/14/19 19:40 EEHg/L60 11/13/19SM21-22 6200B400Chlorobenzene
ND 20000 11/14/19 19:40 EEHg/L4200 11/13/19SM21-22 6200B400Ethanol
ND 200 11/14/19 19:40 EEHg/L84 11/13/19SM21-22 6200B400Chlorodibromomethane
ND 200 11/14/19 19:40 EEHg/L140 11/13/19SM21-22 6200B400Chloroethane
ND 200 11/14/19 19:40 EEHg/L68 11/13/19SM21-22 6200B400Chloroform
ND 400 11/14/19 19:40 EEHg/L180 11/13/19SM21-22 6200B400Chloromethane
ND 200 11/14/19 19:40 EEHg/L48 11/13/19SM21-22 6200B4002-Chlorotoluene
ND 200 11/14/19 19:40 EEHg/L56 11/13/19SM21-22 6200B4004-Chlorotoluene
ND 200 11/14/19 19:40 EEHg/L76 11/13/19SM21-22 6200B4001,2-Dibromoethane (EDB)
ND 200 11/14/19 19:40 EEHg/L64 11/13/19SM21-22 6200B4001,2-Dichlorobenzene
ND 200 11/14/19 19:40 EEHg/L48 11/13/19SM21-22 6200B4001,3-Dichlorobenzene
ND 200 11/14/19 19:40 EEHg/L52 11/13/19SM21-22 6200B4001,4-Dichlorobenzene
ND 200 11/14/19 19:40 EEHg/L100 11/13/19SM21-22 6200B400Dichlorodifluoromethane (Freon 12)
ND 200 11/14/19 19:40 EEHg/L64 11/13/19SM21-22 6200B4001,1-Dichloroethane
ND 400 11/14/19 19:40 EEHg/L160 11/13/19SM21-22 6200B4001,2-Dichloroethane
ND 200 11/14/19 19:40 EEHg/L130 11/13/19SM21-22 6200B4001,1-Dichloroethylene
ND 200 11/14/19 19:40 EEHg/L52 11/13/19SM21-22 6200B400cis-1,2-Dichloroethylene
ND 200 11/14/19 19:40 EEHg/L120 11/13/19SM21-22 6200B400trans-1,2-Dichloroethylene
ND 200 11/14/19 19:40 EEHg/L80 11/13/19SM21-22 6200B4001,2-Dichloropropane
ND 200 11/14/19 19:40 EEHg/L44 11/13/19SM21-22 6200B4001,3-Dichloropropane
ND 200 11/14/19 19:40 EEHg/L80 11/13/19SM21-22 6200B4002,2-Dichloropropane
ND 200 11/14/19 19:40 EEHg/L64 11/13/19SM21-22 6200B4001,1-Dichloropropene
ND 200 11/14/19 19:40 EEHg/L52 11/13/19SM21-22 6200B400cis-1,3-Dichloropropene
ND 200 11/14/19 19:40 EEHg/L92 11/13/19SM21-22 6200B400trans-1,3-Dichloropropene
ND 200 11/14/19 19:40 EEHg/L68 11/13/19SM21-22 6200B400Diisopropyl Ether (DIPE)
3500 200 11/14/19 19:40 EEHg/L52 11/13/19SM21-22 6200B400Ethylbenzene
ND 2000 11/14/19 19:40 EEHg/L610 11/13/19SM21-22 6200B4002-Hexanone (MBK)
100 200 11/14/19 19:40 EEHg/L68 11/13/19SM21-22 6200B400JIsopropylbenzene (Cumene)
ND 200 11/14/19 19:40 EEHg/L80 11/13/19SM21-22 6200B400p-Isopropyltoluene (p-Cymene)
Page 53 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-20
Field Sample #: MW-21
Sample Matrix: Ground Water
Sampled: 11/7/2019 14:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 200 11/14/19 19:40 EEHg/L100 11/13/19SM21-22 6200B400Methyl tert-Butyl Ether (MTBE)
ND 2000 11/14/19 19:40 EEHg/L140 11/13/19SM21-22 6200B400Methylene Chloride
ND 2000 11/14/19 19:40 EEHg/L670 11/13/19SM21-22 6200B4004-Methyl-2-pentanone (MIBK)
1900 2000 11/14/19 19:40 EEHg/L120 11/13/19SM21-22 6200B400JNaphthalene
320 200 11/14/19 19:40 EEHg/L52 11/13/19SM21-22 6200B400n-Propylbenzene
160 200 11/14/19 19:40 EEHg/L44 11/13/19SM21-22 6200B400JStyrene
ND 200 11/14/19 19:40 EEHg/L110 11/13/19SM21-22 6200B4001,1,1,2-Tetrachloroethane
ND 200 11/14/19 19:40 EEHg/L88 11/13/19SM21-22 6200B4001,1,2,2-Tetrachloroethane
ND 200 11/14/19 19:40 EEHg/L72 11/13/19SM21-22 6200B400Tetrachloroethylene
28000 200 11/14/19 19:40 EEHg/L56 11/13/19SM21-22 6200B400Toluene
ND 400 11/14/19 19:40 EEHg/L230 11/13/19SM21-22 6200B4001,2,3-Trichlorobenzene
ND 200 11/14/19 19:40 EEHg/L160 11/13/19SM21-22 6200B4001,2,4-Trichlorobenzene
ND 200 11/14/19 19:40 EEHg/L80 11/13/19SM21-22 6200B4001,1,1-Trichloroethane
ND 200 11/14/19 19:40 EEHg/L64 11/13/19SM21-22 6200B4001,1,2-Trichloroethane
ND 200 11/14/19 19:40 EEHg/L96 11/13/19SM21-22 6200B400Trichloroethylene
ND 200 11/14/19 19:40 EEHg/L130 11/13/19SM21-22 6200B400Trichlorofluoromethane (Freon 11)
ND 200 11/14/19 19:40 EEHg/L100 11/13/19SM21-22 6200B4001,2,3-Trichloropropane
2300 200 11/14/19 19:40 EEHg/L72 11/13/19SM21-22 6200B4001,2,4-Trimethylbenzene
670 200 11/14/19 19:40 EEHg/L56 11/13/19SM21-22 6200B4001,3,5-Trimethylbenzene
ND 8000 11/14/19 19:40 EEHg/L4100 11/13/19SM21-22 6200B400L-04Vinyl Acetate
ND 200 11/14/19 19:40 EEHg/L180 11/13/19SM21-22 6200B400Vinyl Chloride
11000 400 11/14/19 19:40 EEHg/L120 11/13/19SM21-22 6200B400m+p Xylene
5300 200 11/14/19 19:40 EEHg/L68 11/13/19SM21-22 6200B400o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.0 11/14/19 19:4070-130
Toluene-d8 97.2 11/14/19 19:4070-130
4-Bromofluorobenzene 101 11/14/19 19:4070-130
Page 54 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-21
Field Sample #: MW-22
Sample Matrix: Ground Water
Sampled: 11/7/2019 14:35
[TOC_2]19K0568-21[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 500 11/14/19 20:09 EEHg/L38 11/13/19SM21-22 6200B10Acetone
ND 10 11/14/19 20:09 EEHg/L1.4 11/13/19SM21-22 6200B10L-04tert-Amyl Methyl Ether (TAME)
130 5.0 11/14/19 20:09 EEHg/L1.8 11/13/19SM21-22 6200B10Benzene
ND 5.0 11/14/19 20:09 EEHg/L1.5 11/13/19SM21-22 6200B10Bromobenzene
ND 5.0 11/14/19 20:09 EEHg/L3.2 11/13/19SM21-22 6200B10Bromochloromethane
ND 5.0 11/14/19 20:09 EEHg/L1.6 11/13/19SM21-22 6200B10Bromodichloromethane
ND 5.0 11/14/19 20:09 EEHg/L4.6 11/13/19SM21-22 6200B10Bromoform
ND 10 11/14/19 20:09 EEHg/L7.8 11/13/19SM21-22 6200B10Bromomethane
ND 50 11/14/19 20:09 EEHg/L19 11/13/19SM21-22 6200B102-Butanone (MEK)
ND 200 11/14/19 20:09 EEHg/L42 11/13/19SM21-22 6200B10tert-Butyl Alcohol (TBA)
30 5.0 11/14/19 20:09 EEHg/L2.1 11/13/19SM21-22 6200B10n-Butylbenzene
14 5.0 11/14/19 20:09 EEHg/L1.6 11/13/19SM21-22 6200B10sec-Butylbenzene
1.8 5.0 11/14/19 20:09 EEHg/L1.7 11/13/19SM21-22 6200B10Jtert-Butylbenzene
ND 5.0 11/14/19 20:09 EEHg/L1.6 11/13/19SM21-22 6200B10L-04tert-Butyl Ethyl Ether (TBEE)
ND 5.0 11/14/19 20:09 EEHg/L1.1 11/13/19SM21-22 6200B10Carbon Tetrachloride
ND 5.0 11/14/19 20:09 EEHg/L1.5 11/13/19SM21-22 6200B10Chlorobenzene
ND 500 11/14/19 20:09 EEHg/L110 11/13/19SM21-22 6200B10Ethanol
ND 5.0 11/14/19 20:09 EEHg/L2.1 11/13/19SM21-22 6200B10Chlorodibromomethane
ND 5.0 11/14/19 20:09 EEHg/L3.5 11/13/19SM21-22 6200B10Chloroethane
ND 5.0 11/14/19 20:09 EEHg/L1.7 11/13/19SM21-22 6200B10Chloroform
ND 10 11/14/19 20:09 EEHg/L4.5 11/13/19SM21-22 6200B10Chloromethane
ND 5.0 11/14/19 20:09 EEHg/L1.2 11/13/19SM21-22 6200B102-Chlorotoluene
ND 5.0 11/14/19 20:09 EEHg/L1.4 11/13/19SM21-22 6200B104-Chlorotoluene
ND 5.0 11/14/19 20:09 EEHg/L1.9 11/13/19SM21-22 6200B101,2-Dibromoethane (EDB)
ND 5.0 11/14/19 20:09 EEHg/L1.6 11/13/19SM21-22 6200B101,2-Dichlorobenzene
ND 5.0 11/14/19 20:09 EEHg/L1.2 11/13/19SM21-22 6200B101,3-Dichlorobenzene
ND 5.0 11/14/19 20:09 EEHg/L1.3 11/13/19SM21-22 6200B101,4-Dichlorobenzene
ND 5.0 11/14/19 20:09 EEHg/L2.6 11/13/19SM21-22 6200B10Dichlorodifluoromethane (Freon 12)
ND 5.0 11/14/19 20:09 EEHg/L1.6 11/13/19SM21-22 6200B101,1-Dichloroethane
ND 10 11/14/19 20:09 EEHg/L4.1 11/13/19SM21-22 6200B101,2-Dichloroethane
ND 5.0 11/14/19 20:09 EEHg/L3.2 11/13/19SM21-22 6200B101,1-Dichloroethylene
ND 5.0 11/14/19 20:09 EEHg/L1.3 11/13/19SM21-22 6200B10cis-1,2-Dichloroethylene
ND 5.0 11/14/19 20:09 EEHg/L3.1 11/13/19SM21-22 6200B10trans-1,2-Dichloroethylene
ND 5.0 11/14/19 20:09 EEHg/L2.0 11/13/19SM21-22 6200B101,2-Dichloropropane
ND 5.0 11/14/19 20:09 EEHg/L1.1 11/13/19SM21-22 6200B101,3-Dichloropropane
ND 5.0 11/14/19 20:09 EEHg/L2.0 11/13/19SM21-22 6200B102,2-Dichloropropane
ND 5.0 11/14/19 20:09 EEHg/L1.6 11/13/19SM21-22 6200B101,1-Dichloropropene
ND 5.0 11/14/19 20:09 EEHg/L1.3 11/13/19SM21-22 6200B10cis-1,3-Dichloropropene
ND 5.0 11/14/19 20:09 EEHg/L2.3 11/13/19SM21-22 6200B10trans-1,3-Dichloropropene
ND 5.0 11/14/19 20:09 EEHg/L1.7 11/13/19SM21-22 6200B10Diisopropyl Ether (DIPE)
790 5.0 11/14/19 20:09 EEHg/L1.3 11/13/19SM21-22 6200B10Ethylbenzene
ND 50 11/14/19 20:09 EEHg/L15 11/13/19SM21-22 6200B102-Hexanone (MBK)
74 5.0 11/14/19 20:09 EEHg/L1.7 11/13/19SM21-22 6200B10Isopropylbenzene (Cumene)
10 5.0 11/14/19 20:09 EEHg/L2.0 11/13/19SM21-22 6200B10p-Isopropyltoluene (p-Cymene)
Page 55 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-21
Field Sample #: MW-22
Sample Matrix: Ground Water
Sampled: 11/7/2019 14:35
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 5.0 11/14/19 20:09 EEHg/L2.5 11/13/19SM21-22 6200B10Methyl tert-Butyl Ether (MTBE)
ND 50 11/14/19 20:09 EEHg/L3.4 11/13/19SM21-22 6200B10Methylene Chloride
ND 50 11/14/19 20:09 EEHg/L17 11/13/19SM21-22 6200B104-Methyl-2-pentanone (MIBK)
340 50 11/14/19 20:09 EEHg/L3.1 11/13/19SM21-22 6200B10Naphthalene
270 5.0 11/14/19 20:09 EEHg/L1.3 11/13/19SM21-22 6200B10n-Propylbenzene
ND 5.0 11/14/19 20:09 EEHg/L1.1 11/13/19SM21-22 6200B10Styrene
ND 5.0 11/14/19 20:09 EEHg/L2.7 11/13/19SM21-22 6200B101,1,1,2-Tetrachloroethane
ND 5.0 11/14/19 20:09 EEHg/L2.2 11/13/19SM21-22 6200B101,1,2,2-Tetrachloroethane
ND 5.0 11/14/19 20:09 EEHg/L1.8 11/13/19SM21-22 6200B10Tetrachloroethylene
82 5.0 11/14/19 20:09 EEHg/L1.4 11/13/19SM21-22 6200B10Toluene
ND 10 11/14/19 20:09 EEHg/L5.7 11/13/19SM21-22 6200B101,2,3-Trichlorobenzene
ND 5.0 11/14/19 20:09 EEHg/L4.0 11/13/19SM21-22 6200B101,2,4-Trichlorobenzene
ND 5.0 11/14/19 20:09 EEHg/L2.0 11/13/19SM21-22 6200B101,1,1-Trichloroethane
ND 5.0 11/14/19 20:09 EEHg/L1.6 11/13/19SM21-22 6200B101,1,2-Trichloroethane
ND 5.0 11/14/19 20:09 EEHg/L2.4 11/13/19SM21-22 6200B10Trichloroethylene
ND 5.0 11/14/19 20:09 EEHg/L3.3 11/13/19SM21-22 6200B10Trichlorofluoromethane (Freon 11)
ND 5.0 11/14/19 20:09 EEHg/L2.5 11/13/19SM21-22 6200B101,2,3-Trichloropropane
1400 5.0 11/14/19 20:09 EEHg/L1.8 11/13/19SM21-22 6200B101,2,4-Trimethylbenzene
460 5.0 11/14/19 20:09 EEHg/L1.4 11/13/19SM21-22 6200B101,3,5-Trimethylbenzene
ND 200 11/14/19 20:09 EEHg/L100 11/13/19SM21-22 6200B10L-04Vinyl Acetate
ND 5.0 11/14/19 20:09 EEHg/L4.5 11/13/19SM21-22 6200B10Vinyl Chloride
630 10 11/14/19 20:09 EEHg/L3.0 11/13/19SM21-22 6200B10m+p Xylene
150 5.0 11/14/19 20:09 EEHg/L1.7 11/13/19SM21-22 6200B10o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.7 11/14/19 20:0970-130
Toluene-d8 98.8 11/14/19 20:0970-130
4-Bromofluorobenzene 105 11/14/19 20:0970-130
Page 56 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-22
Field Sample #: MW-24
Sample Matrix: Ground Water
Sampled: 11/7/2019 15:00
[TOC_2]19K0568-22[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 500 11/14/19 20:38 EEHg/L38 11/13/19SM21-22 6200B10Acetone
ND 10 11/14/19 20:38 EEHg/L1.4 11/13/19SM21-22 6200B10L-04tert-Amyl Methyl Ether (TAME)
45 5.0 11/14/19 20:38 EEHg/L1.8 11/13/19SM21-22 6200B10Benzene
ND 5.0 11/14/19 20:38 EEHg/L1.5 11/13/19SM21-22 6200B10Bromobenzene
ND 5.0 11/14/19 20:38 EEHg/L3.2 11/13/19SM21-22 6200B10Bromochloromethane
ND 5.0 11/14/19 20:38 EEHg/L1.6 11/13/19SM21-22 6200B10Bromodichloromethane
ND 5.0 11/14/19 20:38 EEHg/L4.6 11/13/19SM21-22 6200B10Bromoform
ND 10 11/14/19 20:38 EEHg/L7.8 11/13/19SM21-22 6200B10Bromomethane
ND 50 11/14/19 20:38 EEHg/L19 11/13/19SM21-22 6200B102-Butanone (MEK)
ND 200 11/14/19 20:38 EEHg/L42 11/13/19SM21-22 6200B10tert-Butyl Alcohol (TBA)
15 5.0 11/14/19 20:38 EEHg/L2.1 11/13/19SM21-22 6200B10n-Butylbenzene
5.4 5.0 11/14/19 20:38 EEHg/L1.6 11/13/19SM21-22 6200B10sec-Butylbenzene
ND 5.0 11/14/19 20:38 EEHg/L1.7 11/13/19SM21-22 6200B10tert-Butylbenzene
ND 5.0 11/14/19 20:38 EEHg/L1.6 11/13/19SM21-22 6200B10L-04tert-Butyl Ethyl Ether (TBEE)
ND 5.0 11/14/19 20:38 EEHg/L1.1 11/13/19SM21-22 6200B10Carbon Tetrachloride
ND 5.0 11/14/19 20:38 EEHg/L1.5 11/13/19SM21-22 6200B10Chlorobenzene
ND 500 11/14/19 20:38 EEHg/L110 11/13/19SM21-22 6200B10Ethanol
ND 5.0 11/14/19 20:38 EEHg/L2.1 11/13/19SM21-22 6200B10Chlorodibromomethane
ND 5.0 11/14/19 20:38 EEHg/L3.5 11/13/19SM21-22 6200B10Chloroethane
ND 5.0 11/14/19 20:38 EEHg/L1.7 11/13/19SM21-22 6200B10Chloroform
ND 10 11/14/19 20:38 EEHg/L4.5 11/13/19SM21-22 6200B10Chloromethane
ND 5.0 11/14/19 20:38 EEHg/L1.2 11/13/19SM21-22 6200B102-Chlorotoluene
ND 5.0 11/14/19 20:38 EEHg/L1.4 11/13/19SM21-22 6200B104-Chlorotoluene
ND 5.0 11/14/19 20:38 EEHg/L1.9 11/13/19SM21-22 6200B101,2-Dibromoethane (EDB)
ND 5.0 11/14/19 20:38 EEHg/L1.6 11/13/19SM21-22 6200B101,2-Dichlorobenzene
ND 5.0 11/14/19 20:38 EEHg/L1.2 11/13/19SM21-22 6200B101,3-Dichlorobenzene
ND 5.0 11/14/19 20:38 EEHg/L1.3 11/13/19SM21-22 6200B101,4-Dichlorobenzene
ND 5.0 11/14/19 20:38 EEHg/L2.6 11/13/19SM21-22 6200B10Dichlorodifluoromethane (Freon 12)
ND 5.0 11/14/19 20:38 EEHg/L1.6 11/13/19SM21-22 6200B101,1-Dichloroethane
ND 10 11/14/19 20:38 EEHg/L4.1 11/13/19SM21-22 6200B101,2-Dichloroethane
ND 5.0 11/14/19 20:38 EEHg/L3.2 11/13/19SM21-22 6200B101,1-Dichloroethylene
ND 5.0 11/14/19 20:38 EEHg/L1.3 11/13/19SM21-22 6200B10cis-1,2-Dichloroethylene
ND 5.0 11/14/19 20:38 EEHg/L3.1 11/13/19SM21-22 6200B10trans-1,2-Dichloroethylene
ND 5.0 11/14/19 20:38 EEHg/L2.0 11/13/19SM21-22 6200B101,2-Dichloropropane
ND 5.0 11/14/19 20:38 EEHg/L1.1 11/13/19SM21-22 6200B101,3-Dichloropropane
ND 5.0 11/14/19 20:38 EEHg/L2.0 11/13/19SM21-22 6200B102,2-Dichloropropane
ND 5.0 11/14/19 20:38 EEHg/L1.6 11/13/19SM21-22 6200B101,1-Dichloropropene
ND 5.0 11/14/19 20:38 EEHg/L1.3 11/13/19SM21-22 6200B10cis-1,3-Dichloropropene
ND 5.0 11/14/19 20:38 EEHg/L2.3 11/13/19SM21-22 6200B10trans-1,3-Dichloropropene
ND 5.0 11/14/19 20:38 EEHg/L1.7 11/13/19SM21-22 6200B10Diisopropyl Ether (DIPE)
380 5.0 11/14/19 20:38 EEHg/L1.3 11/13/19SM21-22 6200B10Ethylbenzene
ND 50 11/14/19 20:38 EEHg/L15 11/13/19SM21-22 6200B102-Hexanone (MBK)
26 5.0 11/14/19 20:38 EEHg/L1.7 11/13/19SM21-22 6200B10Isopropylbenzene (Cumene)
4.0 5.0 11/14/19 20:38 EEHg/L2.0 11/13/19SM21-22 6200B10Jp-Isopropyltoluene (p-Cymene)
Page 57 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-22
Field Sample #: MW-24
Sample Matrix: Ground Water
Sampled: 11/7/2019 15:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 5.0 11/14/19 20:38 EEHg/L2.5 11/13/19SM21-22 6200B10Methyl tert-Butyl Ether (MTBE)
ND 50 11/14/19 20:38 EEHg/L3.4 11/13/19SM21-22 6200B10Methylene Chloride
45 50 11/14/19 20:38 EEHg/L17 11/13/19SM21-22 6200B10J4-Methyl-2-pentanone (MIBK)
240 50 11/14/19 20:38 EEHg/L3.1 11/13/19SM21-22 6200B10Naphthalene
74 5.0 11/14/19 20:38 EEHg/L1.3 11/13/19SM21-22 6200B10n-Propylbenzene
ND 5.0 11/14/19 20:38 EEHg/L1.1 11/13/19SM21-22 6200B10Styrene
ND 5.0 11/14/19 20:38 EEHg/L2.7 11/13/19SM21-22 6200B101,1,1,2-Tetrachloroethane
ND 5.0 11/14/19 20:38 EEHg/L2.2 11/13/19SM21-22 6200B101,1,2,2-Tetrachloroethane
ND 5.0 11/14/19 20:38 EEHg/L1.8 11/13/19SM21-22 6200B10Tetrachloroethylene
200 5.0 11/14/19 20:38 EEHg/L1.4 11/13/19SM21-22 6200B10Toluene
ND 10 11/14/19 20:38 EEHg/L5.7 11/13/19SM21-22 6200B101,2,3-Trichlorobenzene
ND 5.0 11/14/19 20:38 EEHg/L4.0 11/13/19SM21-22 6200B101,2,4-Trichlorobenzene
ND 5.0 11/14/19 20:38 EEHg/L2.0 11/13/19SM21-22 6200B101,1,1-Trichloroethane
ND 5.0 11/14/19 20:38 EEHg/L1.6 11/13/19SM21-22 6200B101,1,2-Trichloroethane
ND 5.0 11/14/19 20:38 EEHg/L2.4 11/13/19SM21-22 6200B10Trichloroethylene
ND 5.0 11/14/19 20:38 EEHg/L3.3 11/13/19SM21-22 6200B10Trichlorofluoromethane (Freon 11)
ND 5.0 11/14/19 20:38 EEHg/L2.5 11/13/19SM21-22 6200B101,2,3-Trichloropropane
580 5.0 11/14/19 20:38 EEHg/L1.8 11/13/19SM21-22 6200B101,2,4-Trimethylbenzene
130 5.0 11/14/19 20:38 EEHg/L1.4 11/13/19SM21-22 6200B101,3,5-Trimethylbenzene
ND 200 11/14/19 20:38 EEHg/L100 11/13/19SM21-22 6200B10L-04Vinyl Acetate
ND 5.0 11/14/19 20:38 EEHg/L4.5 11/13/19SM21-22 6200B10Vinyl Chloride
1300 10 11/14/19 20:38 EEHg/L3.0 11/13/19SM21-22 6200B10m+p Xylene
810 5.0 11/14/19 20:38 EEHg/L1.7 11/13/19SM21-22 6200B10o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 94.6 11/14/19 20:3870-130
Toluene-d8 99.2 11/14/19 20:3870-130
4-Bromofluorobenzene 101 11/14/19 20:3870-130
Page 58 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-23
Field Sample #: MW-25
Sample Matrix: Ground Water
Sampled: 11/7/2019 15:20
[TOC_2]19K0568-23[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/14/19 16:48 EEHg/L3.8 11/13/19SM21-22 6200B1Acetone
ND 1.0 11/14/19 16:48 EEHg/L0.14 11/13/19SM21-22 6200B1L-04tert-Amyl Methyl Ether (TAME)
ND 0.50 11/14/19 16:48 EEHg/L0.18 11/13/19SM21-22 6200B1Benzene
ND 0.50 11/14/19 16:48 EEHg/L0.15 11/13/19SM21-22 6200B1Bromobenzene
ND 0.50 11/14/19 16:48 EEHg/L0.32 11/13/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/14/19 16:48 EEHg/L0.16 11/13/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/14/19 16:48 EEHg/L0.46 11/13/19SM21-22 6200B1Bromoform
ND 1.0 11/14/19 16:48 EEHg/L0.78 11/13/19SM21-22 6200B1Bromomethane
ND 5.0 11/14/19 16:48 EEHg/L1.9 11/13/19SM21-22 6200B12-Butanone (MEK)
ND 20 11/14/19 16:48 EEHg/L4.2 11/13/19SM21-22 6200B1tert-Butyl Alcohol (TBA)
ND 0.50 11/14/19 16:48 EEHg/L0.21 11/13/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/14/19 16:48 EEHg/L0.16 11/13/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/14/19 16:48 EEHg/L0.17 11/13/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/14/19 16:48 EEHg/L0.16 11/13/19SM21-22 6200B1L-04tert-Butyl Ethyl Ether (TBEE)
ND 0.50 11/14/19 16:48 EEHg/L0.11 11/13/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/14/19 16:48 EEHg/L0.15 11/13/19SM21-22 6200B1Chlorobenzene
ND 50 11/14/19 16:48 EEHg/L11 11/13/19SM21-22 6200B1Ethanol
ND 0.50 11/14/19 16:48 EEHg/L0.21 11/13/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/14/19 16:48 EEHg/L0.35 11/13/19SM21-22 6200B1Chloroethane
ND 0.50 11/14/19 16:48 EEHg/L0.17 11/13/19SM21-22 6200B1Chloroform
ND 1.0 11/14/19 16:48 EEHg/L0.45 11/13/19SM21-22 6200B1Chloromethane
ND 0.50 11/14/19 16:48 EEHg/L0.12 11/13/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/14/19 16:48 EEHg/L0.14 11/13/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/14/19 16:48 EEHg/L0.19 11/13/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/14/19 16:48 EEHg/L0.16 11/13/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/14/19 16:48 EEHg/L0.12 11/13/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/14/19 16:48 EEHg/L0.13 11/13/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/14/19 16:48 EEHg/L0.26 11/13/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/14/19 16:48 EEHg/L0.16 11/13/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/14/19 16:48 EEHg/L0.41 11/13/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/14/19 16:48 EEHg/L0.32 11/13/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/14/19 16:48 EEHg/L0.13 11/13/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/14/19 16:48 EEHg/L0.31 11/13/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/14/19 16:48 EEHg/L0.20 11/13/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/14/19 16:48 EEHg/L0.11 11/13/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/14/19 16:48 EEHg/L0.20 11/13/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/14/19 16:48 EEHg/L0.16 11/13/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/14/19 16:48 EEHg/L0.13 11/13/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/14/19 16:48 EEHg/L0.23 11/13/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/14/19 16:48 EEHg/L0.17 11/13/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/14/19 16:48 EEHg/L0.13 11/13/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/14/19 16:48 EEHg/L1.5 11/13/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/14/19 16:48 EEHg/L0.17 11/13/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/14/19 16:48 EEHg/L0.20 11/13/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
Page 59 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-23
Field Sample #: MW-25
Sample Matrix: Ground Water
Sampled: 11/7/2019 15:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 11/14/19 16:48 EEHg/L0.25 11/13/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/14/19 16:48 EEHg/L0.34 11/13/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/14/19 16:48 EEHg/L1.7 11/13/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 11/14/19 16:48 EEHg/L0.31 11/13/19SM21-22 6200B1Naphthalene
ND 0.50 11/14/19 16:48 EEHg/L0.13 11/13/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/14/19 16:48 EEHg/L0.11 11/13/19SM21-22 6200B1Styrene
ND 0.50 11/14/19 16:48 EEHg/L0.27 11/13/19SM21-22 6200B11,1,1,2-Tetrachloroethane
ND 0.50 11/14/19 16:48 EEHg/L0.22 11/13/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/14/19 16:48 EEHg/L0.18 11/13/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/14/19 16:48 EEHg/L0.14 11/13/19SM21-22 6200B1Toluene
ND 1.0 11/14/19 16:48 EEHg/L0.57 11/13/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/14/19 16:48 EEHg/L0.40 11/13/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/14/19 16:48 EEHg/L0.20 11/13/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/14/19 16:48 EEHg/L0.16 11/13/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/14/19 16:48 EEHg/L0.24 11/13/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/14/19 16:48 EEHg/L0.33 11/13/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/14/19 16:48 EEHg/L0.25 11/13/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/14/19 16:48 EEHg/L0.18 11/13/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/14/19 16:48 EEHg/L0.14 11/13/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/14/19 16:48 EEHg/L10 11/13/19SM21-22 6200B1L-04Vinyl Acetate
ND 0.50 11/14/19 16:48 EEHg/L0.45 11/13/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/14/19 16:48 EEHg/L0.30 11/13/19SM21-22 6200B1m+p Xylene
ND 0.50 11/14/19 16:48 EEHg/L0.17 11/13/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 91.0 11/14/19 16:4870-130
Toluene-d8 97.2 11/14/19 16:4870-130
4-Bromofluorobenzene 101 11/14/19 16:4870-130
Page 60 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-24
Field Sample #: MW-28
Sample Matrix: Ground Water
Sampled: 11/7/2019 15:40
[TOC_2]19K0568-24[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/14/19 17:17 EEHg/L3.8 11/13/19SM21-22 6200B1Acetone
ND 1.0 11/14/19 17:17 EEHg/L0.14 11/13/19SM21-22 6200B1L-04tert-Amyl Methyl Ether (TAME)
ND 0.50 11/14/19 17:17 EEHg/L0.18 11/13/19SM21-22 6200B1Benzene
ND 0.50 11/14/19 17:17 EEHg/L0.15 11/13/19SM21-22 6200B1Bromobenzene
ND 0.50 11/14/19 17:17 EEHg/L0.32 11/13/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/14/19 17:17 EEHg/L0.16 11/13/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/14/19 17:17 EEHg/L0.46 11/13/19SM21-22 6200B1Bromoform
ND 1.0 11/14/19 17:17 EEHg/L0.78 11/13/19SM21-22 6200B1Bromomethane
ND 5.0 11/14/19 17:17 EEHg/L1.9 11/13/19SM21-22 6200B12-Butanone (MEK)
ND 20 11/14/19 17:17 EEHg/L4.2 11/13/19SM21-22 6200B1tert-Butyl Alcohol (TBA)
ND 0.50 11/14/19 17:17 EEHg/L0.21 11/13/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/14/19 17:17 EEHg/L0.16 11/13/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/14/19 17:17 EEHg/L0.17 11/13/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/14/19 17:17 EEHg/L0.16 11/13/19SM21-22 6200B1L-04tert-Butyl Ethyl Ether (TBEE)
ND 0.50 11/14/19 17:17 EEHg/L0.11 11/13/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/14/19 17:17 EEHg/L0.15 11/13/19SM21-22 6200B1Chlorobenzene
ND 50 11/14/19 17:17 EEHg/L11 11/13/19SM21-22 6200B1Ethanol
ND 0.50 11/14/19 17:17 EEHg/L0.21 11/13/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/14/19 17:17 EEHg/L0.35 11/13/19SM21-22 6200B1Chloroethane
ND 0.50 11/14/19 17:17 EEHg/L0.17 11/13/19SM21-22 6200B1Chloroform
ND 1.0 11/14/19 17:17 EEHg/L0.45 11/13/19SM21-22 6200B1Chloromethane
ND 0.50 11/14/19 17:17 EEHg/L0.12 11/13/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/14/19 17:17 EEHg/L0.14 11/13/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/14/19 17:17 EEHg/L0.19 11/13/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/14/19 17:17 EEHg/L0.16 11/13/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/14/19 17:17 EEHg/L0.12 11/13/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/14/19 17:17 EEHg/L0.13 11/13/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/14/19 17:17 EEHg/L0.26 11/13/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/14/19 17:17 EEHg/L0.16 11/13/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/14/19 17:17 EEHg/L0.41 11/13/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/14/19 17:17 EEHg/L0.32 11/13/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/14/19 17:17 EEHg/L0.13 11/13/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/14/19 17:17 EEHg/L0.31 11/13/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/14/19 17:17 EEHg/L0.20 11/13/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/14/19 17:17 EEHg/L0.11 11/13/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/14/19 17:17 EEHg/L0.20 11/13/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/14/19 17:17 EEHg/L0.16 11/13/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/14/19 17:17 EEHg/L0.13 11/13/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/14/19 17:17 EEHg/L0.23 11/13/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/14/19 17:17 EEHg/L0.17 11/13/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/14/19 17:17 EEHg/L0.13 11/13/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/14/19 17:17 EEHg/L1.5 11/13/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/14/19 17:17 EEHg/L0.17 11/13/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/14/19 17:17 EEHg/L0.20 11/13/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
Page 61 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-24
Field Sample #: MW-28
Sample Matrix: Ground Water
Sampled: 11/7/2019 15:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 11/14/19 17:17 EEHg/L0.25 11/13/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/14/19 17:17 EEHg/L0.34 11/13/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/14/19 17:17 EEHg/L1.7 11/13/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 11/14/19 17:17 EEHg/L0.31 11/13/19SM21-22 6200B1Naphthalene
ND 0.50 11/14/19 17:17 EEHg/L0.13 11/13/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/14/19 17:17 EEHg/L0.11 11/13/19SM21-22 6200B1Styrene
ND 0.50 11/14/19 17:17 EEHg/L0.27 11/13/19SM21-22 6200B11,1,1,2-Tetrachloroethane
ND 0.50 11/14/19 17:17 EEHg/L0.22 11/13/19SM21-22 6200B11,1,2,2-Tetrachloroethane
2.2 0.50 11/14/19 17:17 EEHg/L0.18 11/13/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/14/19 17:17 EEHg/L0.14 11/13/19SM21-22 6200B1Toluene
ND 1.0 11/14/19 17:17 EEHg/L0.57 11/13/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/14/19 17:17 EEHg/L0.40 11/13/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/14/19 17:17 EEHg/L0.20 11/13/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/14/19 17:17 EEHg/L0.16 11/13/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/14/19 17:17 EEHg/L0.24 11/13/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/14/19 17:17 EEHg/L0.33 11/13/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/14/19 17:17 EEHg/L0.25 11/13/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/14/19 17:17 EEHg/L0.18 11/13/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/14/19 17:17 EEHg/L0.14 11/13/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/14/19 17:17 EEHg/L10 11/13/19SM21-22 6200B1L-04Vinyl Acetate
ND 0.50 11/14/19 17:17 EEHg/L0.45 11/13/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/14/19 17:17 EEHg/L0.30 11/13/19SM21-22 6200B1m+p Xylene
ND 0.50 11/14/19 17:17 EEHg/L0.17 11/13/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 91.4 11/14/19 17:1770-130
Toluene-d8 97.2 11/14/19 17:1770-130
4-Bromofluorobenzene 98.8 11/14/19 17:1770-130
Page 62 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-25
Field Sample #: Field Blank 11/7/19
Sample Matrix: Field Blank
Sampled: 11/7/2019 15:45
[TOC_2]19K0568-25[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/15/19 0:28 EEHg/L3.8 11/14/19SM21-22 6200B1Acetone
ND 1.0 11/15/19 0:28 EEHg/L0.14 11/14/19SM21-22 6200B1L-04tert-Amyl Methyl Ether (TAME)
ND 0.50 11/15/19 0:28 EEHg/L0.18 11/14/19SM21-22 6200B1Benzene
ND 0.50 11/15/19 0:28 EEHg/L0.15 11/14/19SM21-22 6200B1Bromobenzene
ND 0.50 11/15/19 0:28 EEHg/L0.32 11/14/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/15/19 0:28 EEHg/L0.16 11/14/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/15/19 0:28 EEHg/L0.46 11/14/19SM21-22 6200B1Bromoform
ND 1.0 11/15/19 0:28 EEHg/L0.78 11/14/19SM21-22 6200B1Bromomethane
ND 5.0 11/15/19 0:28 EEHg/L1.9 11/14/19SM21-22 6200B12-Butanone (MEK)
ND 20 11/15/19 0:28 EEHg/L4.2 11/14/19SM21-22 6200B1tert-Butyl Alcohol (TBA)
ND 0.50 11/15/19 0:28 EEHg/L0.21 11/14/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/15/19 0:28 EEHg/L0.16 11/14/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/15/19 0:28 EEHg/L0.17 11/14/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/15/19 0:28 EEHg/L0.16 11/14/19SM21-22 6200B1L-04tert-Butyl Ethyl Ether (TBEE)
ND 0.50 11/15/19 0:28 EEHg/L0.11 11/14/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/15/19 0:28 EEHg/L0.15 11/14/19SM21-22 6200B1Chlorobenzene
ND 50 11/15/19 0:28 EEHg/L11 11/14/19SM21-22 6200B1R-05Ethanol
ND 0.50 11/15/19 0:28 EEHg/L0.21 11/14/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/15/19 0:28 EEHg/L0.35 11/14/19SM21-22 6200B1Chloroethane
ND 0.50 11/15/19 0:28 EEHg/L0.17 11/14/19SM21-22 6200B1Chloroform
ND 1.0 11/15/19 0:28 EEHg/L0.45 11/14/19SM21-22 6200B1Chloromethane
ND 0.50 11/15/19 0:28 EEHg/L0.12 11/14/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/15/19 0:28 EEHg/L0.14 11/14/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/15/19 0:28 EEHg/L0.19 11/14/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/15/19 0:28 EEHg/L0.16 11/14/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/15/19 0:28 EEHg/L0.12 11/14/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/15/19 0:28 EEHg/L0.13 11/14/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/15/19 0:28 EEHg/L0.26 11/14/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/15/19 0:28 EEHg/L0.16 11/14/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/15/19 0:28 EEHg/L0.41 11/14/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/15/19 0:28 EEHg/L0.32 11/14/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/15/19 0:28 EEHg/L0.13 11/14/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/15/19 0:28 EEHg/L0.31 11/14/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/15/19 0:28 EEHg/L0.20 11/14/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/15/19 0:28 EEHg/L0.11 11/14/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/15/19 0:28 EEHg/L0.20 11/14/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/15/19 0:28 EEHg/L0.16 11/14/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/15/19 0:28 EEHg/L0.13 11/14/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/15/19 0:28 EEHg/L0.23 11/14/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/15/19 0:28 EEHg/L0.17 11/14/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/15/19 0:28 EEHg/L0.13 11/14/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/15/19 0:28 EEHg/L1.5 11/14/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/15/19 0:28 EEHg/L0.17 11/14/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/15/19 0:28 EEHg/L0.20 11/14/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
Page 63 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-25
Field Sample #: Field Blank 11/7/19
Sample Matrix: Field Blank
Sampled: 11/7/2019 15:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 11/15/19 0:28 EEHg/L0.25 11/14/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/15/19 0:28 EEHg/L0.34 11/14/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/15/19 0:28 EEHg/L1.7 11/14/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 11/15/19 0:28 EEHg/L0.31 11/14/19SM21-22 6200B1Naphthalene
ND 0.50 11/15/19 0:28 EEHg/L0.13 11/14/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/15/19 0:28 EEHg/L0.11 11/14/19SM21-22 6200B1Styrene
ND 0.50 11/15/19 0:28 EEHg/L0.27 11/14/19SM21-22 6200B11,1,1,2-Tetrachloroethane
ND 0.50 11/15/19 0:28 EEHg/L0.22 11/14/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/15/19 0:28 EEHg/L0.18 11/14/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/15/19 0:28 EEHg/L0.14 11/14/19SM21-22 6200B1Toluene
ND 2.0 11/15/19 0:28 EEHg/L0.57 11/14/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/15/19 0:28 EEHg/L0.40 11/14/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/15/19 0:28 EEHg/L0.20 11/14/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/15/19 0:28 EEHg/L0.16 11/14/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/15/19 0:28 EEHg/L0.24 11/14/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/15/19 0:28 EEHg/L0.33 11/14/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/15/19 0:28 EEHg/L0.25 11/14/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/15/19 0:28 EEHg/L0.18 11/14/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/15/19 0:28 EEHg/L0.14 11/14/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/15/19 0:28 EEHg/L10 11/14/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/15/19 0:28 EEHg/L0.45 11/14/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/15/19 0:28 EEHg/L0.30 11/14/19SM21-22 6200B1m+p Xylene
ND 0.50 11/15/19 0:28 EEHg/L0.17 11/14/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.8 11/15/19 0:2870-130
Toluene-d8 96.6 11/15/19 0:2870-130
4-Bromofluorobenzene 96.6 11/15/19 0:2870-130
Page 64 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-26
Field Sample #: WSW-1 Effluent
Sample Matrix: Water
Sampled: 11/7/2019 16:15
[TOC_2]19K0568-26[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/14/19 12:57 EEHg/L3.8 11/13/19SM21-22 6200B1Acetone
ND 1.0 11/14/19 12:57 EEHg/L0.14 11/13/19SM21-22 6200B1L-04tert-Amyl Methyl Ether (TAME)
ND 0.50 11/14/19 12:57 EEHg/L0.18 11/13/19SM21-22 6200B1Benzene
ND 0.50 11/14/19 12:57 EEHg/L0.15 11/13/19SM21-22 6200B1Bromobenzene
ND 0.50 11/14/19 12:57 EEHg/L0.32 11/13/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/14/19 12:57 EEHg/L0.16 11/13/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/14/19 12:57 EEHg/L0.46 11/13/19SM21-22 6200B1Bromoform
ND 1.0 11/14/19 12:57 EEHg/L0.78 11/13/19SM21-22 6200B1Bromomethane
ND 5.0 11/14/19 12:57 EEHg/L1.9 11/13/19SM21-22 6200B12-Butanone (MEK)
ND 20 11/14/19 12:57 EEHg/L4.2 11/13/19SM21-22 6200B1tert-Butyl Alcohol (TBA)
ND 0.50 11/14/19 12:57 EEHg/L0.21 11/13/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/14/19 12:57 EEHg/L0.16 11/13/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/14/19 12:57 EEHg/L0.17 11/13/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/14/19 12:57 EEHg/L0.16 11/13/19SM21-22 6200B1L-04tert-Butyl Ethyl Ether (TBEE)
ND 0.50 11/14/19 12:57 EEHg/L0.11 11/13/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/14/19 12:57 EEHg/L0.15 11/13/19SM21-22 6200B1Chlorobenzene
ND 50 11/14/19 12:57 EEHg/L11 11/13/19SM21-22 6200B1Ethanol
ND 0.50 11/14/19 12:57 EEHg/L0.21 11/13/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/14/19 12:57 EEHg/L0.35 11/13/19SM21-22 6200B1Chloroethane
ND 0.50 11/14/19 12:57 EEHg/L0.17 11/13/19SM21-22 6200B1Chloroform
ND 1.0 11/14/19 12:57 EEHg/L0.45 11/13/19SM21-22 6200B1Chloromethane
ND 0.50 11/14/19 12:57 EEHg/L0.12 11/13/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/14/19 12:57 EEHg/L0.14 11/13/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/14/19 12:57 EEHg/L0.19 11/13/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/14/19 12:57 EEHg/L0.16 11/13/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/14/19 12:57 EEHg/L0.12 11/13/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/14/19 12:57 EEHg/L0.13 11/13/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/14/19 12:57 EEHg/L0.26 11/13/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/14/19 12:57 EEHg/L0.16 11/13/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/14/19 12:57 EEHg/L0.41 11/13/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/14/19 12:57 EEHg/L0.32 11/13/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/14/19 12:57 EEHg/L0.13 11/13/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/14/19 12:57 EEHg/L0.31 11/13/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/14/19 12:57 EEHg/L0.20 11/13/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/14/19 12:57 EEHg/L0.11 11/13/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/14/19 12:57 EEHg/L0.20 11/13/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/14/19 12:57 EEHg/L0.16 11/13/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/14/19 12:57 EEHg/L0.13 11/13/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/14/19 12:57 EEHg/L0.23 11/13/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/14/19 12:57 EEHg/L0.17 11/13/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/14/19 12:57 EEHg/L0.13 11/13/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/14/19 12:57 EEHg/L1.5 11/13/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/14/19 12:57 EEHg/L0.17 11/13/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/14/19 12:57 EEHg/L0.20 11/13/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
Page 65 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-26
Field Sample #: WSW-1 Effluent
Sample Matrix: Water
Sampled: 11/7/2019 16:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 11/14/19 12:57 EEHg/L0.25 11/13/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/14/19 12:57 EEHg/L0.34 11/13/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/14/19 12:57 EEHg/L1.7 11/13/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 5.0 11/14/19 12:57 EEHg/L0.31 11/13/19SM21-22 6200B1Naphthalene
ND 0.50 11/14/19 12:57 EEHg/L0.13 11/13/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/14/19 12:57 EEHg/L0.11 11/13/19SM21-22 6200B1Styrene
ND 0.50 11/14/19 12:57 EEHg/L0.27 11/13/19SM21-22 6200B11,1,1,2-Tetrachloroethane
ND 0.50 11/14/19 12:57 EEHg/L0.22 11/13/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/14/19 12:57 EEHg/L0.18 11/13/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/14/19 12:57 EEHg/L0.14 11/13/19SM21-22 6200B1Toluene
ND 1.0 11/14/19 12:57 EEHg/L0.57 11/13/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/14/19 12:57 EEHg/L0.40 11/13/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/14/19 12:57 EEHg/L0.20 11/13/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/14/19 12:57 EEHg/L0.16 11/13/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/14/19 12:57 EEHg/L0.24 11/13/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/14/19 12:57 EEHg/L0.33 11/13/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/14/19 12:57 EEHg/L0.25 11/13/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/14/19 12:57 EEHg/L0.18 11/13/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/14/19 12:57 EEHg/L0.14 11/13/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/14/19 12:57 EEHg/L10 11/13/19SM21-22 6200B1L-04Vinyl Acetate
ND 0.50 11/14/19 12:57 EEHg/L0.45 11/13/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/14/19 12:57 EEHg/L0.30 11/13/19SM21-22 6200B1m+p Xylene
ND 0.50 11/14/19 12:57 EEHg/L0.17 11/13/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 88.5 11/14/19 12:5770-130
Toluene-d8 97.7 11/14/19 12:5770-130
4-Bromofluorobenzene 103 11/14/19 12:5770-130
Page 66 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-27
Field Sample #: WSW-1 Influent
Sample Matrix: Water
Sampled: 11/7/2019 16:20
[TOC_2]19K0568-27[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 250 11/14/19 18:14 EEHg/L19 11/13/19SM21-22 6200B5Acetone
55 5.0 11/14/19 18:14 EEHg/L0.70 11/13/19SM21-22 6200B5L-04tert-Amyl Methyl Ether (TAME)
13 2.5 11/14/19 18:14 EEHg/L0.90 11/13/19SM21-22 6200B5Benzene
ND 2.5 11/14/19 18:14 EEHg/L0.75 11/13/19SM21-22 6200B5Bromobenzene
ND 2.5 11/14/19 18:14 EEHg/L1.6 11/13/19SM21-22 6200B5Bromochloromethane
ND 2.5 11/14/19 18:14 EEHg/L0.80 11/13/19SM21-22 6200B5Bromodichloromethane
ND 2.5 11/14/19 18:14 EEHg/L2.3 11/13/19SM21-22 6200B5Bromoform
ND 5.0 11/14/19 18:14 EEHg/L3.9 11/13/19SM21-22 6200B5Bromomethane
ND 25 11/14/19 18:14 EEHg/L9.7 11/13/19SM21-22 6200B52-Butanone (MEK)
700 100 11/14/19 18:14 EEHg/L21 11/13/19SM21-22 6200B5tert-Butyl Alcohol (TBA)
2.8 2.5 11/14/19 18:14 EEHg/L1.0 11/13/19SM21-22 6200B5n-Butylbenzene
1.4 2.5 11/14/19 18:14 EEHg/L0.80 11/13/19SM21-22 6200B5Jsec-Butylbenzene
ND 2.5 11/14/19 18:14 EEHg/L0.85 11/13/19SM21-22 6200B5tert-Butylbenzene
ND 2.5 11/14/19 18:14 EEHg/L0.80 11/13/19SM21-22 6200B5L-04tert-Butyl Ethyl Ether (TBEE)
ND 2.5 11/14/19 18:14 EEHg/L0.55 11/13/19SM21-22 6200B5Carbon Tetrachloride
ND 2.5 11/14/19 18:14 EEHg/L0.75 11/13/19SM21-22 6200B5Chlorobenzene
ND 250 11/14/19 18:14 EEHg/L53 11/13/19SM21-22 6200B5Ethanol
ND 2.5 11/14/19 18:14 EEHg/L1.0 11/13/19SM21-22 6200B5Chlorodibromomethane
ND 2.5 11/14/19 18:14 EEHg/L1.8 11/13/19SM21-22 6200B5Chloroethane
ND 2.5 11/14/19 18:14 EEHg/L0.85 11/13/19SM21-22 6200B5Chloroform
ND 5.0 11/14/19 18:14 EEHg/L2.2 11/13/19SM21-22 6200B5Chloromethane
ND 2.5 11/14/19 18:14 EEHg/L0.60 11/13/19SM21-22 6200B52-Chlorotoluene
ND 2.5 11/14/19 18:14 EEHg/L0.70 11/13/19SM21-22 6200B54-Chlorotoluene
ND 2.5 11/14/19 18:14 EEHg/L0.95 11/13/19SM21-22 6200B51,2-Dibromoethane (EDB)
ND 2.5 11/14/19 18:14 EEHg/L0.80 11/13/19SM21-22 6200B51,2-Dichlorobenzene
ND 2.5 11/14/19 18:14 EEHg/L0.60 11/13/19SM21-22 6200B51,3-Dichlorobenzene
ND 2.5 11/14/19 18:14 EEHg/L0.65 11/13/19SM21-22 6200B51,4-Dichlorobenzene
ND 2.5 11/14/19 18:14 EEHg/L1.3 11/13/19SM21-22 6200B5Dichlorodifluoromethane (Freon 12)
ND 2.5 11/14/19 18:14 EEHg/L0.80 11/13/19SM21-22 6200B51,1-Dichloroethane
ND 5.0 11/14/19 18:14 EEHg/L2.0 11/13/19SM21-22 6200B51,2-Dichloroethane
ND 2.5 11/14/19 18:14 EEHg/L1.6 11/13/19SM21-22 6200B51,1-Dichloroethylene
ND 2.5 11/14/19 18:14 EEHg/L0.65 11/13/19SM21-22 6200B5cis-1,2-Dichloroethylene
ND 2.5 11/14/19 18:14 EEHg/L1.6 11/13/19SM21-22 6200B5trans-1,2-Dichloroethylene
ND 2.5 11/14/19 18:14 EEHg/L1.0 11/13/19SM21-22 6200B51,2-Dichloropropane
ND 2.5 11/14/19 18:14 EEHg/L0.55 11/13/19SM21-22 6200B51,3-Dichloropropane
ND 2.5 11/14/19 18:14 EEHg/L1.0 11/13/19SM21-22 6200B52,2-Dichloropropane
ND 2.5 11/14/19 18:14 EEHg/L0.80 11/13/19SM21-22 6200B51,1-Dichloropropene
ND 2.5 11/14/19 18:14 EEHg/L0.65 11/13/19SM21-22 6200B5cis-1,3-Dichloropropene
ND 2.5 11/14/19 18:14 EEHg/L1.2 11/13/19SM21-22 6200B5trans-1,3-Dichloropropene
88 2.5 11/14/19 18:14 EEHg/L0.85 11/13/19SM21-22 6200B5Diisopropyl Ether (DIPE)
ND 2.5 11/14/19 18:14 EEHg/L0.65 11/13/19SM21-22 6200B5Ethylbenzene
ND 25 11/14/19 18:14 EEHg/L7.6 11/13/19SM21-22 6200B52-Hexanone (MBK)
3.9 2.5 11/14/19 18:14 EEHg/L0.85 11/13/19SM21-22 6200B5Isopropylbenzene (Cumene)
ND 2.5 11/14/19 18:14 EEHg/L1.0 11/13/19SM21-22 6200B5p-Isopropyltoluene (p-Cymene)
Page 67 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/8/2019
Work Order: 19K0568Sample Description:Project Location: 6195 Hwy 96, Oxford, NC
Sample ID: 19K0568-27
Field Sample #: WSW-1 Influent
Sample Matrix: Water
Sampled: 11/7/2019 16:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
460 2.5 11/14/19 18:14 EEHg/L1.2 11/13/19SM21-22 6200B5Methyl tert-Butyl Ether (MTBE)
ND 25 11/14/19 18:14 EEHg/L1.7 11/13/19SM21-22 6200B5Methylene Chloride
ND 25 11/14/19 18:14 EEHg/L8.4 11/13/19SM21-22 6200B54-Methyl-2-pentanone (MIBK)
ND 25 11/14/19 18:14 EEHg/L1.6 11/13/19SM21-22 6200B5Naphthalene
1.2 2.5 11/14/19 18:14 EEHg/L0.65 11/13/19SM21-22 6200B5Jn-Propylbenzene
ND 2.5 11/14/19 18:14 EEHg/L0.55 11/13/19SM21-22 6200B5Styrene
ND 2.5 11/14/19 18:14 EEHg/L1.4 11/13/19SM21-22 6200B51,1,1,2-Tetrachloroethane
ND 2.5 11/14/19 18:14 EEHg/L1.1 11/13/19SM21-22 6200B51,1,2,2-Tetrachloroethane
ND 2.5 11/14/19 18:14 EEHg/L0.90 11/13/19SM21-22 6200B5Tetrachloroethylene
ND 2.5 11/14/19 18:14 EEHg/L0.70 11/13/19SM21-22 6200B5Toluene
ND 5.0 11/14/19 18:14 EEHg/L2.8 11/13/19SM21-22 6200B51,2,3-Trichlorobenzene
ND 2.5 11/14/19 18:14 EEHg/L2.0 11/13/19SM21-22 6200B51,2,4-Trichlorobenzene
ND 2.5 11/14/19 18:14 EEHg/L1.0 11/13/19SM21-22 6200B51,1,1-Trichloroethane
ND 2.5 11/14/19 18:14 EEHg/L0.80 11/13/19SM21-22 6200B51,1,2-Trichloroethane
ND 2.5 11/14/19 18:14 EEHg/L1.2 11/13/19SM21-22 6200B5Trichloroethylene
ND 2.5 11/14/19 18:14 EEHg/L1.6 11/13/19SM21-22 6200B5Trichlorofluoromethane (Freon 11)
ND 2.5 11/14/19 18:14 EEHg/L1.2 11/13/19SM21-22 6200B51,2,3-Trichloropropane
6.5 2.5 11/14/19 18:14 EEHg/L0.90 11/13/19SM21-22 6200B51,2,4-Trimethylbenzene
1.2 2.5 11/14/19 18:14 EEHg/L0.70 11/13/19SM21-22 6200B5J1,3,5-Trimethylbenzene
ND 100 11/14/19 18:14 EEHg/L51 11/13/19SM21-22 6200B5L-04Vinyl Acetate
ND 2.5 11/14/19 18:14 EEHg/L2.2 11/13/19SM21-22 6200B5Vinyl Chloride
ND 5.0 11/14/19 18:14 EEHg/L1.5 11/13/19SM21-22 6200B5m+p Xylene
11 2.5 11/14/19 18:14 EEHg/L0.85 11/13/19SM21-22 6200B5o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 94.8 11/14/19 18:1470-130
Toluene-d8 98.0 11/14/19 18:1470-130
4-Bromofluorobenzene 104 11/14/19 18:1470-130
Page 68 of 90
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B245814 11/12/190.025 5.0019K0568-01 [DCW-2]
B245814 11/12/190.1 5.0019K0568-02 [DCW-3]
B245814 11/12/190.5 5.0019K0568-03 [DCW-4]
B245814 11/12/195 5.0019K0568-04 [DCW-7]
B245814 11/12/195 5.0019K0568-06 [MW-1]
B245814 11/12/195 5.0019K0568-07 [MW-2]
B245814 11/12/195 5.0019K0568-08 [MW-3]
B245814 11/12/190.02 5.0019K0568-09 [MW-5]
B245814 11/12/195 5.0019K0568-10 [MW-6]
B245814 11/12/195 5.0019K0568-11 [MW-7]
B245814 11/12/195 5.0019K0568-12 [MW-9]
B245814 11/12/195 5.0019K0568-13 [MW-12]
B245814 11/12/190.05 5.0019K0568-16 [MW-17]
B245814 11/12/190.05 5.0019K0568-17 [MW-18]
B245814 11/12/190.025 5.0019K0568-18 [MW-19]
B245814 11/12/190.0125 5.0019K0568-19 [MW-20]
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B245876 11/13/190.01 5.0019K0568-14 [MW-14]
B245876 11/13/190.0125 5.0019K0568-15 [MW-15]
B245876 11/13/190.0125 5.0019K0568-20 [MW-21]
B245876 11/13/190.5 5.0019K0568-21 [MW-22]
B245876 11/13/190.5 5.0019K0568-22 [MW-24]
B245876 11/13/195 5.0019K0568-23 [MW-25]
B245876 11/13/195 5.0019K0568-24 [MW-28]
B245876 11/13/195 5.0019K0568-26 [WSW-1 Effluent]
B245876 11/13/191 5.0019K0568-27 [WSW-1 Influent]
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B246118 11/14/195 5.0019K0568-05 [Field Blank 11/6/19]
B246118 11/14/195 5.0019K0568-25 [Field Blank 11/7/19]
[TOC_1]Sample Preparation Information[TOC]
Page 69 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B245814 - SW-846 5030B
[TOC_3]B245814[TOC]
Blank (B245814-BLK1) Prepared: 11/12/19 Analyzed: 11/15/19
Acetone g/L50ND
tert-Amyl Methyl Ether (TAME)g/L0.50 L-04ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
tert-Butyl Alcohol (TBA)g/L20ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
tert-Butyl Ethyl Ether (TBEE)g/L0.50 L-04ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,1,2-Tetrachloroethane g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
[TOC_1]QC Data[TOC]
Page 70 of 90
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245814 - SW-846 5030B
Blank (B245814-BLK1) Prepared: 11/12/19 Analyzed: 11/15/19
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 88.022.0
g/L 25.0 70-130Surrogate: Toluene-d8 97.924.5
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 97.524.4
LCS (B245814-BS1) Prepared: 11/12/19 Analyzed: 11/15/19
Acetone g/L50 100 70-13094.194.1
tert-Amyl Methyl Ether (TAME)g/L0.50 10.0 L-0470-13052.1 *5.21
Benzene g/L0.50 10.0 70-13090.49.04
Bromobenzene g/L0.50 10.0 70-13099.49.94
Bromochloromethane g/L0.50 10.0 70-13085.48.54
Bromodichloromethane g/L0.50 10.0 70-13095.59.55
Bromoform g/L0.50 10.0 70-13010810.8
Bromomethane g/L1.0 10.0 60-14012012.0
2-Butanone (MEK)g/L5.0 100 70-13077.277.2
tert-Butyl Alcohol (TBA)g/L20 100 40-13092.092.0
n-Butylbenzene g/L0.50 10.0 70-13010810.8
sec-Butylbenzene g/L0.50 10.0 70-13011211.2
tert-Butylbenzene g/L0.50 10.0 70-13011211.2
tert-Butyl Ethyl Ether (TBEE)g/L0.50 10.0 L-0470-13059.8 *5.98
Carbon Tetrachloride g/L0.50 10.0 70-13010310.3
Chlorobenzene g/L0.50 10.0 70-13011011.0
Ethanol g/L50 100 70-130108108
Chlorodibromomethane g/L0.50 10.0 70-13099.49.94
Chloroethane g/L0.50 10.0 60-14092.29.22
Chloroform g/L0.50 10.0 70-13091.19.11
Chloromethane g/L0.60 10.0 60-14088.28.82
2-Chlorotoluene g/L0.50 10.0 70-13010210.2
4-Chlorotoluene g/L0.50 10.0 70-13010810.8
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13098.79.87
1,2-Dichlorobenzene g/L0.50 10.0 70-13010510.5
1,3-Dichlorobenzene g/L0.50 10.0 70-13010810.8
1,4-Dichlorobenzene g/L0.50 10.0 70-13010510.5
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14090.49.04
1,1-Dichloroethane g/L0.50 10.0 70-13090.29.02
1,2-Dichloroethane g/L0.50 10.0 70-13096.99.69
1,1-Dichloroethylene g/L0.50 10.0 70-13010210.2
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13091.29.12
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245814 - SW-846 5030B
LCS (B245814-BS1) Prepared: 11/12/19 Analyzed: 11/15/19
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13096.19.61
1,2-Dichloropropane g/L0.50 10.0 70-13091.99.19
1,3-Dichloropropane g/L0.50 10.0 70-13094.39.43
2,2-Dichloropropane g/L0.50 10.0 70-13085.58.55
1,1-Dichloropropene g/L0.50 10.0 70-13010010.0
cis-1,3-Dichloropropene g/L0.50 10.0 70-13095.79.57
trans-1,3-Dichloropropene g/L0.50 10.0 70-13089.18.91
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13082.48.24
Ethylbenzene g/L0.50 10.0 70-13011011.0
2-Hexanone (MBK)g/L5.0 100 70-13088.788.7
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13011311.3
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13010710.7
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13076.87.68
Methylene Chloride g/L5.0 10.0 70-13088.48.84
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-13091.191.1
Naphthalene g/L0.50 10.0 L-0770-130131*13.1
n-Propylbenzene g/L0.50 10.0 70-13010910.9
Styrene g/L0.50 10.0 70-13010110.1
1,1,1,2-Tetrachloroethane g/L0.50 10.0 70-13011611.6
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13010410.4
Tetrachloroethylene g/L0.50 10.0 70-13011211.2
Toluene g/L0.50 10.0 70-13010110.1
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13077.27.72
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13094.59.45
1,1,1-Trichloroethane g/L0.50 10.0 70-13010310.3
1,1,2-Trichloroethane g/L0.50 10.0 70-13097.19.71
Trichloroethylene g/L0.50 10.0 70-13010310.3
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13010910.9
1,2,3-Trichloropropane g/L0.50 10.0 70-13010510.5
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13010410.4
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13011111.1
Vinyl Acetate g/L20 100 70-13071.071.0
Vinyl Chloride g/L0.50 10.0 60-14011511.5
m+p Xylene g/L1.0 20.0 70-13011122.2
o-Xylene g/L0.50 10.0 70-13011111.1
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 94.923.7
g/L 25.0 70-130Surrogate: Toluene-d8 98.224.6
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10025.1
LCS Dup (B245814-BSD1) Prepared: 11/12/19 Analyzed: 11/15/19
Acetone g/L50 100 2570-13094.6 0.43594.6
tert-Amyl Methyl Ether (TAME)g/L0.50 10.0 25 L-0470-13059.3 12.9*5.93
Benzene g/L0.50 10.0 2570-13087.1 3.728.71
Bromobenzene g/L0.50 10.0 2570-130100 1.1010.0
Bromochloromethane g/L0.50 10.0 2570-13082.9 2.978.29
Bromodichloromethane g/L0.50 10.0 2570-13094.9 0.6309.49
Bromoform g/L0.50 10.0 2570-130110 2.0311.0
Bromomethane g/L1.0 10.0 2560-140111 8.0711.1
2-Butanone (MEK)g/L5.0 100 2570-13081.8 5.7981.8
tert-Butyl Alcohol (TBA)g/L20 100 2540-13094.7 2.8794.7
n-Butylbenzene g/L0.50 10.0 2570-130112 3.8111.2
sec-Butylbenzene g/L0.50 10.0 2570-130111 1.4311.1
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245814 - SW-846 5030B
LCS Dup (B245814-BSD1) Prepared: 11/12/19 Analyzed: 11/15/19
tert-Butylbenzene g/L0.50 10.0 2570-130111 0.53711.1
tert-Butyl Ethyl Ether (TBEE)g/L0.50 10.0 25 L-0470-13065.5 9.10*6.55
Carbon Tetrachloride g/L0.50 10.0 2570-13099.8 3.459.98
Chlorobenzene g/L0.50 10.0 2570-130106 3.5210.6
Ethanol g/L50 100 2570-130122 11.8122
Chlorodibromomethane g/L0.50 10.0 2570-13096.1 3.389.61
Chloroethane g/L0.50 10.0 2560-14086.1 6.848.61
Chloroform g/L0.50 10.0 2570-13087.0 4.608.70
Chloromethane g/L0.60 10.0 2560-14087.1 1.258.71
2-Chlorotoluene g/L0.50 10.0 2570-13099.7 2.089.97
4-Chlorotoluene g/L0.50 10.0 2570-130109 1.1010.9
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130100 1.8110.0
1,2-Dichlorobenzene g/L0.50 10.0 2570-130108 2.2510.8
1,3-Dichlorobenzene g/L0.50 10.0 2570-130109 0.91910.9
1,4-Dichlorobenzene g/L0.50 10.0 2570-130107 1.3210.7
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14089.7 0.7778.97
1,1-Dichloroethane g/L0.50 10.0 2570-13086.2 4.548.62
1,2-Dichloroethane g/L0.50 10.0 2570-13095.6 1.359.56
1,1-Dichloroethylene g/L0.50 10.0 2570-13099.4 2.789.94
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13088.5 3.018.85
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13092.1 4.259.21
1,2-Dichloropropane g/L0.50 10.0 2570-13088.1 4.228.81
1,3-Dichloropropane g/L0.50 10.0 2570-13092.4 2.049.24
2,2-Dichloropropane g/L0.50 10.0 2570-13083.5 2.378.35
1,1-Dichloropropene g/L0.50 10.0 2570-13094.5 5.869.45
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13094.7 1.059.47
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13090.5 1.569.05
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-13080.0 2.968.00
Ethylbenzene g/L0.50 10.0 2570-130108 2.2010.8
2-Hexanone (MBK)g/L5.0 100 2570-13091.6 3.2491.6
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130112 0.88711.2
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130106 1.0310.6
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13078.5 2.197.85
Methylene Chloride g/L5.0 10.0 2570-13089.9 1.688.99
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-13095.3 4.5495.3
Naphthalene g/L0.50 10.0 2570-130125 4.7612.5
n-Propylbenzene g/L0.50 10.0 2570-130111 2.0911.1
Styrene g/L0.50 10.0 2570-13097.2 3.649.72
1,1,1,2-Tetrachloroethane g/L0.50 10.0 2570-130110 5.9211.0
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130109 4.1210.9
Tetrachloroethylene g/L0.50 10.0 2570-130109 1.9910.9
Toluene g/L0.50 10.0 2570-13098.5 2.519.85
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-13091.0 16.49.10
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-130102 7.5410.2
1,1,1-Trichloroethane g/L0.50 10.0 2570-13098.9 3.969.89
1,1,2-Trichloroethane g/L0.50 10.0 2570-13096.3 0.8279.63
Trichloroethylene g/L0.50 10.0 2570-13098.8 4.169.88
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-130105 4.0110.5
1,2,3-Trichloropropane g/L0.50 10.0 2570-130107 2.1710.7
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130103 1.8310.3
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130109 1.2710.9
Vinyl Acetate g/L20 100 2570-13073.5 3.4573.5
Page 73 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245814 - SW-846 5030B
LCS Dup (B245814-BSD1) Prepared: 11/12/19 Analyzed: 11/15/19
Vinyl Chloride g/L0.50 10.0 2560-140123 6.3912.3
m+p Xylene g/L1.0 20.0 2570-130110 0.72322.0
o-Xylene g/L0.50 10.0 2570-130111 0.089911.1
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 93.323.3
g/L 25.0 70-130Surrogate: Toluene-d8 96.924.2
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 99.424.9
Batch B245876 - SW-846 5030B [TOC_3]B245876[TOC]
Blank (B245876-BLK1) Prepared: 11/13/19 Analyzed: 11/14/19
Acetone g/L50ND
tert-Amyl Methyl Ether (TAME)g/L0.50 L-04ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
tert-Butyl Alcohol (TBA)g/L20ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
tert-Butyl Ethyl Ether (TBEE)g/L0.50 L-04ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
Page 74 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245876 - SW-846 5030B
Blank (B245876-BLK1) Prepared: 11/13/19 Analyzed: 11/14/19
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,1,2-Tetrachloroethane g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20 L-04ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 85.921.5
g/L 25.0 70-130Surrogate: Toluene-d8 97.524.4
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10125.4
LCS (B245876-BS1) Prepared: 11/13/19 Analyzed: 11/14/19
Acetone g/L50 100 70-130118118
tert-Amyl Methyl Ether (TAME)g/L0.50 10.0 L-0470-13060.9 *6.09
Benzene g/L0.50 10.0 70-13082.08.20
Bromobenzene g/L0.50 10.0 70-13010210.2
Bromochloromethane g/L0.50 10.0 70-13076.47.64
Bromodichloromethane g/L0.50 10.0 70-13096.19.61
Bromoform g/L0.50 10.0 70-13010810.8
Bromomethane g/L1.0 10.0 60-14060.86.08
2-Butanone (MEK)g/L5.0 100 70-13079.979.9
tert-Butyl Alcohol (TBA)g/L20 100 40-13065.165.1
n-Butylbenzene g/L0.50 10.0 70-13011011.0
sec-Butylbenzene g/L0.50 10.0 70-13011111.1
tert-Butylbenzene g/L0.50 10.0 70-13010710.7
tert-Butyl Ethyl Ether (TBEE)g/L0.50 10.0 L-0470-13063.6 *6.36
Carbon Tetrachloride g/L0.50 10.0 70-13010110.1
Chlorobenzene g/L0.50 10.0 70-13010910.9
Ethanol g/L50 100 70-130118118
Chlorodibromomethane g/L0.50 10.0 70-13010210.2
Chloroethane g/L0.50 10.0 60-14084.88.48
Chloroform g/L0.50 10.0 70-13084.48.44
Chloromethane g/L0.60 10.0 60-14060.56.05
2-Chlorotoluene g/L0.50 10.0 70-13010110.1
4-Chlorotoluene g/L0.50 10.0 70-13011011.0
Page 75 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245876 - SW-846 5030B
LCS (B245876-BS1) Prepared: 11/13/19 Analyzed: 11/14/19
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13010310.3
1,2-Dichlorobenzene g/L0.50 10.0 70-13010310.3
1,3-Dichlorobenzene g/L0.50 10.0 70-13010810.8
1,4-Dichlorobenzene g/L0.50 10.0 70-13010410.4
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14067.96.79
1,1-Dichloroethane g/L0.50 10.0 70-13083.88.38
1,2-Dichloroethane g/L0.50 10.0 70-13010110.1
1,1-Dichloroethylene g/L0.50 10.0 70-13010510.5
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13085.78.57
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13086.78.67
1,2-Dichloropropane g/L0.50 10.0 70-13085.58.55
1,3-Dichloropropane g/L0.50 10.0 70-13092.59.25
2,2-Dichloropropane g/L0.50 10.0 70-13099.79.97
1,1-Dichloropropene g/L0.50 10.0 70-13088.38.83
cis-1,3-Dichloropropene g/L0.50 10.0 70-13093.09.30
trans-1,3-Dichloropropene g/L0.50 10.0 70-13094.59.45
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13077.57.75
Ethylbenzene g/L0.50 10.0 70-13011011.0
2-Hexanone (MBK)g/L5.0 100 70-13095.295.2
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13011511.5
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13010610.6
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13083.28.32
Methylene Chloride g/L5.0 10.0 70-13077.67.76
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-13096.596.5
Naphthalene g/L0.50 10.0 70-13010010.0
n-Propylbenzene g/L0.50 10.0 70-13011411.4
Styrene g/L0.50 10.0 70-13098.59.85
1,1,1,2-Tetrachloroethane g/L0.50 10.0 70-13011311.3
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13010610.6
Tetrachloroethylene g/L0.50 10.0 70-13011411.4
Toluene g/L0.50 10.0 70-13010010.0
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13088.98.89
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13010210.2
1,1,1-Trichloroethane g/L0.50 10.0 70-13098.99.89
1,1,2-Trichloroethane g/L0.50 10.0 70-13010110.1
Trichloroethylene g/L0.50 10.0 70-13095.99.59
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13010310.3
1,2,3-Trichloropropane g/L0.50 10.0 70-13010310.3
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13097.69.76
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13011211.2
Vinyl Acetate g/L20 100 L-0470-13062.0 *62.0
Vinyl Chloride g/L0.50 10.0 L-0260-140180*18.0
m+p Xylene g/L1.0 20.0 70-13011122.2
o-Xylene g/L0.50 10.0 70-13011211.2
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 88.822.2
g/L 25.0 70-130Surrogate: Toluene-d8 98.024.5
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10426.0
Page 76 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245876 - SW-846 5030B
LCS Dup (B245876-BSD1) Prepared: 11/13/19 Analyzed: 11/14/19
Acetone g/L50 100 2570-130120 1.73120
tert-Amyl Methyl Ether (TAME)g/L0.50 10.0 25 L-0470-13065.3 6.97*6.53
Benzene g/L0.50 10.0 2570-13079.0 3.737.90
Bromobenzene g/L0.50 10.0 2570-13097.8 4.209.78
Bromochloromethane g/L0.50 10.0 2570-13075.5 1.187.55
Bromodichloromethane g/L0.50 10.0 2570-13096.1 0.009.61
Bromoform g/L0.50 10.0 2570-130109 1.4710.9
Bromomethane g/L1.0 10.0 2560-14070.7 15.17.07
2-Butanone (MEK)g/L5.0 100 2570-13077.0 3.6877.0
tert-Butyl Alcohol (TBA)g/L20 100 2540-13078.1 18.278.1
n-Butylbenzene g/L0.50 10.0 2570-130105 4.6610.5
sec-Butylbenzene g/L0.50 10.0 2570-130101 8.7710.1
tert-Butylbenzene g/L0.50 10.0 2570-13099.6 7.549.96
tert-Butyl Ethyl Ether (TBEE)g/L0.50 10.0 25 L-0470-13066.1 3.86*6.61
Carbon Tetrachloride g/L0.50 10.0 2570-13096.9 4.349.69
Chlorobenzene g/L0.50 10.0 2570-130105 3.5510.5
Ethanol g/L50 100 2570-13096.0 20.996.0
Chlorodibromomethane g/L0.50 10.0 2570-13099.0 2.699.90
Chloroethane g/L0.50 10.0 2560-14086.1 1.528.61
Chloroform g/L0.50 10.0 2570-13081.8 3.138.18
Chloromethane g/L0.60 10.0 2560-14062.7 3.576.27
2-Chlorotoluene g/L0.50 10.0 2570-130102 1.1810.2
4-Chlorotoluene g/L0.50 10.0 2570-130108 1.3810.8
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130101 2.0610.1
1,2-Dichlorobenzene g/L0.50 10.0 2570-130102 1.0710.2
1,3-Dichlorobenzene g/L0.50 10.0 2570-130103 4.7510.3
1,4-Dichlorobenzene g/L0.50 10.0 2570-130101 2.8210.1
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14065.3 3.906.53
1,1-Dichloroethane g/L0.50 10.0 2570-13081.7 2.548.17
1,2-Dichloroethane g/L0.50 10.0 2570-130100 0.89310.0
1,1-Dichloroethylene g/L0.50 10.0 2570-130104 1.0510.4
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13081.6 4.908.16
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13083.9 3.288.39
1,2-Dichloropropane g/L0.50 10.0 2570-13083.6 2.258.36
1,3-Dichloropropane g/L0.50 10.0 2570-13090.3 2.419.03
2,2-Dichloropropane g/L0.50 10.0 2570-13095.9 3.899.59
1,1-Dichloropropene g/L0.50 10.0 2570-13086.3 2.298.63
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13090.7 2.509.07
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13092.1 2.579.21
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-13078.2 0.8997.82
Ethylbenzene g/L0.50 10.0 2570-130104 5.6910.4
2-Hexanone (MBK)g/L5.0 100 2570-13097.8 2.6597.8
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130110 4.5411.0
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-13099.9 5.939.99
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13086.3 3.668.63
Methylene Chloride g/L5.0 10.0 2570-13076.6 1.307.66
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-130100 3.58100
Naphthalene g/L0.50 10.0 2570-130110 9.7911.0
n-Propylbenzene g/L0.50 10.0 2570-130108 5.8710.8
Styrene g/L0.50 10.0 2570-13094.5 4.159.45
1,1,1,2-Tetrachloroethane g/L0.50 10.0 2570-130111 1.8811.1
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130109 2.6910.9
Page 77 of 90
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245876 - SW-846 5030B
LCS Dup (B245876-BSD1) Prepared: 11/13/19 Analyzed: 11/14/19
Tetrachloroethylene g/L0.50 10.0 2570-130110 3.5811.0
Toluene g/L0.50 10.0 2570-13096.3 4.279.63
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-130105 16.210.5
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-130109 7.2010.9
1,1,1-Trichloroethane g/L0.50 10.0 2570-13093.4 5.729.34
1,1,2-Trichloroethane g/L0.50 10.0 2570-13094.6 6.159.46
Trichloroethylene g/L0.50 10.0 2570-13095.8 0.1049.58
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13099.2 3.959.92
1,2,3-Trichloropropane g/L0.50 10.0 2570-130105 2.2110.5
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-13092.9 4.939.29
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130109 3.1710.9
Vinyl Acetate g/L20 100 25 L-0470-13062.5 0.787*62.5
Vinyl Chloride g/L0.50 10.0 25 L-0260-140219 19.6*21.9
m+p Xylene g/L1.0 20.0 2570-130106 4.1021.3
o-Xylene g/L0.50 10.0 2570-130107 4.8510.7
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 89.922.5
g/L 25.0 70-130Surrogate: Toluene-d8 98.024.5
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10526.2
Batch B246118 - SW-846 5030B
[TOC_3]B246118[TOC]
Blank (B246118-BLK1) Prepared & Analyzed: 11/14/19
Acetone g/L50ND
tert-Amyl Methyl Ether (TAME)g/L0.50 L-04ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
tert-Butyl Alcohol (TBA)g/L20ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
tert-Butyl Ethyl Ether (TBEE)g/L0.50 L-04ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50 R-05ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B246118 - SW-846 5030B
Blank (B246118-BLK1) Prepared & Analyzed: 11/14/19
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,1,2-Tetrachloroethane g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 93.223.3
g/L 25.0 70-130Surrogate: Toluene-d8 96.424.1
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 98.824.7
LCS (B246118-BS1) Prepared & Analyzed: 11/14/19
Acetone g/L50 100 70-130107107
tert-Amyl Methyl Ether (TAME)g/L0.50 10.0 L-0470-13068.3 *6.83
Benzene g/L0.50 10.0 70-13085.58.55
Bromobenzene g/L0.50 10.0 70-13010010.0
Bromochloromethane g/L0.50 10.0 70-13081.58.15
Bromodichloromethane g/L0.50 10.0 70-13094.39.43
Bromoform g/L0.50 10.0 70-13011011.0
Bromomethane g/L1.0 10.0 60-14011011.0
2-Butanone (MEK)g/L5.0 100 70-13079.279.2
tert-Butyl Alcohol (TBA)g/L20 100 40-13097.097.0
n-Butylbenzene g/L0.50 10.0 70-13010510.5
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B246118 - SW-846 5030B
LCS (B246118-BS1) Prepared & Analyzed: 11/14/19
sec-Butylbenzene g/L0.50 10.0 70-13010910.9
tert-Butylbenzene g/L0.50 10.0 70-13011011.0
tert-Butyl Ethyl Ether (TBEE)g/L0.50 10.0 L-0470-13073.47.34
Carbon Tetrachloride g/L0.50 10.0 70-13010010.0
Chlorobenzene g/L0.50 10.0 70-13011011.0
Ethanol g/L50 100 R-0570-130113113
Chlorodibromomethane g/L0.50 10.0 70-13098.29.82
Chloroethane g/L0.50 10.0 60-14092.59.25
Chloroform g/L0.50 10.0 70-13088.08.80
Chloromethane g/L0.60 10.0 60-14076.67.66
2-Chlorotoluene g/L0.50 10.0 70-13010410.4
4-Chlorotoluene g/L0.50 10.0 70-13011011.0
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13010110.1
1,2-Dichlorobenzene g/L0.50 10.0 70-13010510.5
1,3-Dichlorobenzene g/L0.50 10.0 70-13010810.8
1,4-Dichlorobenzene g/L0.50 10.0 70-13010610.6
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14090.99.09
1,1-Dichloroethane g/L0.50 10.0 70-13084.18.41
1,2-Dichloroethane g/L0.50 10.0 70-13010210.2
1,1-Dichloroethylene g/L0.50 10.0 70-13010910.9
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13086.48.64
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13089.18.91
1,2-Dichloropropane g/L0.50 10.0 70-13085.38.53
1,3-Dichloropropane g/L0.50 10.0 70-13094.79.47
2,2-Dichloropropane g/L0.50 10.0 70-13083.88.38
1,1-Dichloropropene g/L0.50 10.0 70-13094.79.47
cis-1,3-Dichloropropene g/L0.50 10.0 70-13094.89.48
trans-1,3-Dichloropropene g/L0.50 10.0 70-13089.08.90
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13079.67.96
Ethylbenzene g/L0.50 10.0 70-13011611.6
2-Hexanone (MBK)g/L5.0 100 70-13091.791.7
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13011611.6
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13010610.6
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13083.78.37
Methylene Chloride g/L5.0 10.0 70-13094.99.49
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-13094.294.2
Naphthalene g/L0.50 10.0 70-13010510.5
n-Propylbenzene g/L0.50 10.0 70-13011311.3
Styrene g/L0.50 10.0 70-13010810.8
1,1,1,2-Tetrachloroethane g/L0.50 10.0 70-13011411.4
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13010810.8
Tetrachloroethylene g/L0.50 10.0 70-13010910.9
Toluene g/L0.50 10.0 70-13010310.3
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13079.97.99
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13091.69.16
1,1,1-Trichloroethane g/L0.50 10.0 70-13010110.1
1,1,2-Trichloroethane g/L0.50 10.0 70-13095.59.55
Trichloroethylene g/L0.50 10.0 70-13098.79.87
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13011811.8
1,2,3-Trichloropropane g/L0.50 10.0 70-13010810.8
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13011211.2
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13011211.2
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B246118 - SW-846 5030B
LCS (B246118-BS1) Prepared & Analyzed: 11/14/19
Vinyl Acetate g/L20 100 70-13079.479.4
Vinyl Chloride g/L0.50 10.0 L-0260-140208*20.8
m+p Xylene g/L1.0 20.0 70-13011723.5
o-Xylene g/L0.50 10.0 70-13011811.8
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 96.324.1
g/L 25.0 70-130Surrogate: Toluene-d8 98.124.5
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10225.4
LCS Dup (B246118-BSD1) Prepared & Analyzed: 11/14/19
Acetone g/L50 100 2570-130110 3.49110
tert-Amyl Methyl Ether (TAME)g/L0.50 10.0 25 L-0470-13068.4 0.146*6.84
Benzene g/L0.50 10.0 2570-13086.5 1.168.65
Bromobenzene g/L0.50 10.0 2570-130103 2.2710.3
Bromochloromethane g/L0.50 10.0 2570-13078.6 3.627.86
Bromodichloromethane g/L0.50 10.0 2570-130101 6.6610.1
Bromoform g/L0.50 10.0 2570-130114 3.9411.4
Bromomethane g/L1.0 10.0 2560-140120 8.4512.0
2-Butanone (MEK)g/L5.0 100 2570-13079.7 0.55479.7
tert-Butyl Alcohol (TBA)g/L20 100 2540-130102 5.34102
n-Butylbenzene g/L0.50 10.0 2570-130112 6.6211.2
sec-Butylbenzene g/L0.50 10.0 2570-130116 6.2311.6
tert-Butylbenzene g/L0.50 10.0 2570-130115 4.0911.5
tert-Butyl Ethyl Ether (TBEE)g/L0.50 10.0 25 L-0470-13073.3 0.1367.33
Carbon Tetrachloride g/L0.50 10.0 2570-130100 0.099910.0
Chlorobenzene g/L0.50 10.0 2570-130114 3.4011.4
Ethanol g/L50 100 25 L-07A, R-0570-130149 26.8**149
Chlorodibromomethane g/L0.50 10.0 2570-130102 4.2910.2
Chloroethane g/L0.50 10.0 2560-14091.1 1.539.11
Chloroform g/L0.50 10.0 2570-13087.0 1.148.70
Chloromethane g/L0.60 10.0 2560-14077.5 1.177.75
2-Chlorotoluene g/L0.50 10.0 2570-130108 3.6910.8
4-Chlorotoluene g/L0.50 10.0 2570-130114 4.0211.4
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130102 0.59210.2
1,2-Dichlorobenzene g/L0.50 10.0 2570-130109 3.4610.9
1,3-Dichlorobenzene g/L0.50 10.0 2570-130113 4.3411.3
1,4-Dichlorobenzene g/L0.50 10.0 2570-130110 4.1711.0
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14091.7 0.8769.17
1,1-Dichloroethane g/L0.50 10.0 2570-13083.7 0.4778.37
1,2-Dichloroethane g/L0.50 10.0 2570-130104 1.9410.4
1,1-Dichloroethylene g/L0.50 10.0 2570-130109 0.091510.9
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13086.6 0.2318.66
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13090.6 1.679.06
1,2-Dichloropropane g/L0.50 10.0 2570-13087.7 2.778.77
1,3-Dichloropropane g/L0.50 10.0 2570-13096.9 2.309.69
2,2-Dichloropropane g/L0.50 10.0 2570-13083.0 0.9598.30
1,1-Dichloropropene g/L0.50 10.0 2570-13095.4 0.7369.54
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13096.0 1.269.60
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13093.9 5.369.39
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-13076.6 3.847.66
Ethylbenzene g/L0.50 10.0 2570-130118 2.5611.8
2-Hexanone (MBK)g/L5.0 100 2570-13097.2 5.8197.2
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130121 4.8112.1
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B246118 - SW-846 5030B
LCS Dup (B246118-BSD1) Prepared & Analyzed: 11/14/19
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130111 4.5111.1
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13084.5 0.9518.45
Methylene Chloride g/L5.0 10.0 2570-13096.0 1.159.60
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-130100 6.00100
Naphthalene g/L0.50 10.0 2570-130110 4.2811.0
n-Propylbenzene g/L0.50 10.0 2570-130118 4.0811.8
Styrene g/L0.50 10.0 2570-130107 0.27910.7
1,1,1,2-Tetrachloroethane g/L0.50 10.0 2570-130119 4.1211.9
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130114 5.2311.4
Tetrachloroethylene g/L0.50 10.0 2570-130112 3.4411.2
Toluene g/L0.50 10.0 2570-130105 1.4410.5
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-13093.6 15.89.36
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-130104 12.210.4
1,1,1-Trichloroethane g/L0.50 10.0 2570-130102 1.2810.2
1,1,2-Trichloroethane g/L0.50 10.0 2570-13097.8 2.389.78
Trichloroethylene g/L0.50 10.0 2570-130102 3.3910.2
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-130119 0.92911.9
1,2,3-Trichloropropane g/L0.50 10.0 2570-130113 4.4311.3
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130113 1.3311.3
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130117 4.2711.7
Vinyl Acetate g/L20 100 2570-13081.3 2.3981.3
Vinyl Chloride g/L0.50 10.0 25 L-0260-140232 10.7*23.2
m+p Xylene g/L1.0 20.0 2570-130121 2.9824.2
o-Xylene g/L0.50 10.0 2570-130122 3.1612.2
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 94.623.7
g/L 25.0 70-130Surrogate: Toluene-d8 98.024.5
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10325.7
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*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
FLAG/QUALIFIER SUMMARY
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits.
Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is
on the high side.
L-02
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD outside of control limits. Reduced precision anticipated for any reported result for
this compound.
L-07A
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any
reported value for this compound.
R-05
Elevated reporting limit due to high concentration of target compounds.RL-11
[TOC_1]Flag/Qualifier Summary[TOC]
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
[TOC_1]Certifications[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2020
M-MA100Massachusetts DEPMA 06/30/2020
PH-0567Connecticut Department of Publilc HealthCT 09/30/2021
10899 NELAPNew York State Department of HealthNY 04/1/2020
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2020
LAO00112Rhode Island Department of HealthRI 12/30/2019
652North Carolina Div. of Water QualityNC 12/31/2019
MA007 NELAPNew Jersey DEPNJ 06/30/2020
E871027 NELAPFlorida Department of HealthFL 06/30/2020
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2020
2011028State of MaineME 06/9/2021
460217Commonwealth of VirginiaVA 12/14/2019
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2020
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2020
25703North Carolina Department of HealthNC-DW 07/31/2020
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2020
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