RA-1056_6878_CA_MRP_20200319

Groundwater Monitoring Report
Carter’s Grocery, TF-6878
Raleigh, Wake County, North Carolina
S&ME Project No. 4305-18-132B
PREPARED FOR:
NCDEQ, DWM, UST Section
1646 Mail Service Center
Raleigh, NC 27616-1646
PREPARED BY:
S&ME, Inc.
3201 Spring Forest Road
Raleigh, NC 27616
March 19, 2020

S&ME, Inc. | 3201 Spring Forest Road | Raleigh, NC 27616 | p 919.872.2660 | www.smeinc.com

March 19, 2020
NCDEQ, DWM, UST Section
1637 Mail Service Center
Raleigh, NC 27616-1637
Attention: Ms. Linda Blalock Via email: [e-mail]
Reference: Groundwater Monitoring Report
Carter’s Grocery, TF-6878
101 Rand Road
Raleigh, Wake County, North Carolina
S&ME Project No. 4305-18-132B
Dear: Ms. Linda Blalock
S&ME, Inc., (S&ME) presents this report in accordance with the North Carolina Department of Environmental
Quality/S&ME Contract No. N17002 and S&ME Proposal No. 43-1800450B, dated February 10, 2020, as
authorized by Task Authorization No. 03, dated February 11, 2020.
If you have any questions or comments regarding this report, please contact us at your convenience.
Sincerely,
S&ME, Inc.

Jim Peele Thomas P. Raymond, P.E., P.M.P.
Environmental Staff Professional Senior Engineer
[e-mail] [e-mail]

CC: Michael Pfeifer [e-mail]

Attachment: Groundwater Monitoring Report

Groundwater Monitoring Report
Carter’s Grocery, Incident No. 6878, UST No. RA-1056
101 Rand Road
Raleigh, Wake County, North Carolina
S&ME Project No. 4305-18-132B
March 19, 2020 ii

Table of Contents
1.0 Site Information ................................................................................................................ 1
1.1 Site Identification ............................................................................................................................ 1
1.2 Information about Contacts Associated with the Leaking UST System ................................. 1
1.3 Information about Release ............................................................................................................ 1
1.4 Information about the Monitoring Report .................................................................................. 1
1.5 Certification ..................................................................................................................................... 2
2.0 Executive Summary .......................................................................................................... 3
3.0 Scope of Services ............................................................................................................... 4
3.1 Contract Information ..................................................................................................................... 4
3.2 Approved Scope of Services ......................................................................................................... 4
4.0 Site History and Characterization ................................................................................. 4
4.1 UST Owner and Operator Information ....................................................................................... 4
4.2 UST Information ............................................................................................................................. 4
4.3 Description of the UST Release .................................................................................................... 5
4.4 Site Characteristics ......................................................................................................................... 5
4.5 Owners and Occupants of Adjoining/Nearby Properties and Land Use ............................... 5
4.6 Receptors/Potential Receptor Information .................................................................................. 6
5.0 Current Site Assessment Information .......................................................................... 6
5.1 Current Liquid Levels .................................................................................................................... 6
5.2 Groundwater Monitoring Event .................................................................................................. 6
5.3 Water Supply Well Monitoring Event ......................................................................................... 6
5.4 Summary of Groundwater Information ...................................................................................... 7
5.5 Regional and Site Geology and Hydrogeology .......................................................................... 7
5.5.1 Soil and Bedrock ................................................................................................................................ 7
5.5.2 Hydrogeology .................................................................................................................................... 7
5.6 Evaluation of Soil, Groundwater, Surface Water, and Free Product Assessment
Information ...................................................................................................................................... 8
5.6.1 Current Extent and Severity of Contamination ............................................................................... 8
5.6.2 Cleanup Levels Achieved ................................................................................................................... 8
Groundwater Monitoring Report
Carter’s Grocery, Incident No. 6878, UST No. RA-1056
101 Rand Road
Raleigh, Wake County, North Carolina
S&ME Project No. 4305-18-132B
March 19, 2020 iii
6.0 Conclusion and Recommendations ............................................................................... 9

List of Figures
Figure 1 Vicinity Map
Figure 2 Site Map
Figure 3 Groundwater Contour Map
Figure 4 Groundwater Constituent Map
List of Tables
Table 1 UST Owner/Operator Information
Table 2 UST System Information
Table 3 Well Construction and Liquid Level Information
Table 4 Groundwater Analytical Results
Table 5 Water Supply Well Analytical Results
Appendices
Appendix I –Figures
Appendix II – Tables
Appendix III – Site Photographs
Appendix IV – Field Data Sheets
Appendix V – Laboratory Analytical Reports and Chain of Custody Forms

Groundwater Monitoring Report
Carter’s Grocery, Incident No. 6878, UST No. RA-1056
101 Rand Road
Raleigh, Wake County, North Carolina
S&ME Project No. 4305-18-132B
March 19, 2020 1
1.0 Site Information
1.1 Site Identification
 Date of Report: 3/18/2020
 Facility I.D. 00-0-0000026046 UST Incident No.: 6878 UST No.: RA-1056
 Site Risk: High Site Rank: 160A Land Use Category: Residential
 Site Name: Carter’s Grocery
 Site Address: 101 Rand Road
 City/Town: Raleigh Zip Code: 27603 County: Wake
 Description of Geographical Data (e.g., diesel fill port): Former UST Basin
 Location Method (GPS, Topographical map, other): Google Earth
 Latitude (decimal degrees): 35.649267.° Longitude (decimal degrees): -78.650681.°
1.2 Information about Contacts Associated with the Leaking UST System
 UST Owner: Mr. George Russell Carter (Deceased)
 Address: 7601 Old Baucom Road, Raleigh, NC 27610 Telephone: N/A
 UST Operator: Mr. George Russell Carter
 Address: 7601 Old Baucom Road, Raleigh, NC 27610 Telephone: N/A
 Property Occupant: Mr. George Randy Carter Telephone: [phone]
 Consultant/Contractor: S&ME, Inc.
 Address: 3201 Spring Forest Road, Raleigh, NC 27616 Telephone: [phone]
 Analytical Laboratory: Con-Test Analytical Laboratory State Certification No.: 652
 Address: 39 Spruce Street, East Longmeadow, MA 01028 Telephone: [phone]
1.3 Information about Release
 Date Discovered: 6/8/1991
 Estimated Quantity of Release: Unknown
 Cause of Release: Unknown
 Source of Release (Dispenser/Piping/UST): UST Systems
 Sizes and contents of UST system(s) from which the release occurred: Two 560-gallon gasoline USTs; one
270-gallon kerosene UST; two 6,000-gallon gasoline USTs; one 3,000-gallon gasoline UST.
 Criteria Used to Classify Risk: Free product in monitor well MW-1, several active water supply wells in area.
1.4 Information about the Monitoring Report
 Date of Groundwater Monitoring: March 5 and 6, 2020

Groundwater Monitoring Report
Carter’s Grocery, Incident No. 6878, UST No. RA-1056
101 Rand Road
Raleigh, Wake County, North Carolina
S&ME Project No. 4305-18-132B
March 19, 2020 2
1.5 Certification
I, Thomas P. Raymond, a Licensed Engineer for S&ME, do certify that the information contained in this report is
correct and accurate to the best of my knowledge. S&ME is licensed to practice geology/engineering in North
Carolina. Geology License Certification #C-145 and Engineering License Certification #F-0176.

___________________
Thomas P. Raymond, P.E., P.M.P.

Groundwater Monitoring Report
Carter’s Grocery, Incident No. 6878, UST No. RA-1056
101 Rand Road
Raleigh, Wake County, North Carolina
S&ME Project No. 4305-18-132B
March 19, 2020 3
2.0 Executive Summary
The following presents a summary of the groundwater sampling event conducted by S&ME at the Carter’s Grocery
site in Raleigh, Wake County, North Carolina. On March 5 and 6, 2020 S&ME collected groundwater samples from
monitor wells MW-2 through MW-11 and water supply well WSW-1. S&ME personnel measured 0.39 feet of free
product in MW-1.
The laboratory analytical results indicated that the following constituents were reported in monitor well samples at
concentrations exceeding their respective 15A NCAC 2L.0202 Groundwater Standards (2L Standards):

Contaminant 2L Standard (µg/L) Concentration
(µg/L) Well ID Date
benzene 1 55 MW-11 3/6/2020
methyl tert-butyl ether 20 25 MW-11 3/6/2020

 Approximately 0.39 feet of free product was measured in MW-1.

 The dissolved phase petroleum constituents in monitor wells MW-3, MW-4, MW-9 and MW-11 have
generally decreased in concentration since the previous sampling event in June 2018.

 No contaminants were reported above the laboratory detection limit in monitor wells MW-6, or MW-
10.

 Based on groundwater elevations measured on March 5, 2020 and previously reported elevations,
groundwater flows to the northeast.

 One water supply well (WSW-1), located on the property, was sampled on March 6, 2020. No VOCs
were detected above the laboratory detection limit in this well.

 To achieve incident closure:
1. Evaluate methods to remediate free product in the area of monitor well MW-1.
2. Obtain permission to sample selected water supply wells within 1,000 feet of the site. If
contaminants are found, connect to an alternative water supply (when available) and abandon
wells.

Groundwater Monitoring Report
Carter’s Grocery, Incident No. 6878, UST No. RA-1056
101 Rand Road
Raleigh, Wake County, North Carolina
S&ME Project No. 4305-18-132B
March 19, 2020 4
3.0 Scope of Services
3.1 Contract Information
The scope of services for this report was performed in general accordance with S&ME’s proposal number 43-
1800450B dated February 10, 2020. The scope of services was authorized by the North Carolina Department of
Environmental Quality (NCDEQ’s) Task Authorization 03, dated February 11, 2020, and within contract number
N17002.
3.2 Approved Scope of Services
S&ME’s approved Scope of Services for this Task Authorization included gauging MW-1 for free product,
sampling 10 other monitoring wells (MW-2 through MW-11), collecting a sample from water supply well WSW-1
and preparing this report.

The scope of services was completed as proposed.
4.0 Site History and Characterization
4.1 UST Owner and Operator Information
According to previous reports, prepared by others, the on-site gas station opened in the mid-1940s. At this time
two 560-gallon gasoline underground storage tanks (USTs) were installed. In 1958, Mr. George Carter purchased
the property. Considering the USTs were installed prior to Mr. Carter’s purchase, it should be noted that the NC
Underground Storage Tank Database recorded December 30, 1964 as the installation date for the two 560-gallon
gasoline USTs. Under the ownership of Mr. Carter one 270-gallon kerosene UST (in 1970), two 6,000-gallon, and
one 3,000-gallon gasoline USTs (in 1973) were installed. The property is currently owned by Mr. Carter’s son, Mr.
George Randel Carter, who inherited the property. Figure 1, Appendix I presents the Vicinity Map. The UST
owner/operator information is provided in Table 1, Appendix II.

4.2 UST Information
The previous Groundwater Monitoring Report prepared by Crawford Environmental Services and dated June 3,
2013, indicated that Mr. Carter stated the NC Underground Storage Tank Database has made errors in recording
dates associated with the UST installations. A total of six USTs (two 560-gallon gasoline, one 270-gallon kerosene,
two 6,000-gallon gasoline and one 3,000-gallon gasoline tanks) were a part of the UST system on site. According
to the Underground Storage Tank Closure Report dated June 28, 2004, prepared by Terraquest, the two 560-gallon
gasoline tanks located under the canopy and pump island were closed in place in June 1991. The 270-gallon
kerosene UST was removed in December 1991. The remaining USTs (two 6,000-gallon gasoline and one 3,000-
gallon gasoline tanks) were removed on April 29, 2004. Information about the USTs is provided in Table 2, and
the location of the former USTs are shown in Figure 2.
Groundwater Monitoring Report
Carter’s Grocery, Incident No. 6878, UST No. RA-1056
101 Rand Road
Raleigh, Wake County, North Carolina
S&ME Project No. 4305-18-132B
March 19, 2020 5
4.3 Description of the UST Release
There are two incidents associated with Carter’s Grocery (TF-6878 and TF-26632). Following the abandonment in
place of the two 560-gallon gasoline USTs in 1991, methyl tert-butyl ether was detected in an onsite water supply
well, which confirmed a release from the USTs. Mr. Carter contracted the removal of the 270-gallon kerosene UST
and approximately 10 cubic yards of contaminated soil.
In 1993 the remaining USTs (two 6,000-gallon and one 3,000-gallon gasoline tanks) were inspected and certified
as “tight”. A replacement water supply well was installed at the site on February 17, 1993. The new well (WSW-1)
was installed approximately 30 feet to the northwest of the existing water supply well. Petroleum constituents
were confirmed to be present in the soils during installation of WSW-1. The former supply well was abandoned.
Immediately following the installation of WSW-1, samples were collected from the new wellhead and from an
indoor faucet. The analytical results detected toluene below the Primary Federal Drinking Water Standards and
below the 15 NCAC 2L Standard. No other petroleum constituents were detected above their laboratory detection
limit.
The remaining USTs (two 6,000-gallon and one 3,000-gallon gasoline tanks) were excavated and removed April 29,
2004, during this time soil contamination was discovered. No contaminated soil was removed from the site during
excavation.
According to the previous monitoring event conducted by Crawford Environmental on June 3, 2013, two monitor
wells (MW-1 and MW-2) were reported to have free product. At this time, MW-1 had a free product thickness of
1.3 feet and was not sampled. MW-2 had a free product thickness of 0.3 feet, a groundwater sample was taken
from monitor well MW-2 despite the presence of free product. The laboratory analytical results for monitor well
MW-2 indicated the presence of two VOCs above the 2L Standard: benzene at 1.3 micrograms per liter (µg/L) and
naphthalene at 6.2 µg/L. The sample was not run at dilution according to the laboratory analytical report dated
June 17, 2013. Several other VOCs were detected in monitor well MW-2 but below the 2L Standard.
4.4 Site Characteristics
The site, located at 101 Rand Road, is located in a rural area of Raleigh, Wake County, North Carolina. An active
gas station was operated beginning in the mid-1940s and closed in 2004. The site has one structure that is
currently used as an office with no active petroleum sales. Most of the land on site is a grassy yard with a concrete
parking area adjacent to the front of the building. A photographic log of the site and surroundings is provided as
Appendix III.
4.5 Owners and Occupants of Adjoining/Nearby Properties and Land Use
The site and adjacent properties are classified as residential. Water supply well WSW-2, is located on the Pollard
property located to the southeast across Rand Road from the site. The Pollards formerly operated the site as a
small restaurant, the property is now vacant. An agricultural field is located to the north and west of the property,
with a church to the northeast. A new residential community is located to the south across Ten Ten Road. A site
map is provided as Figure 2.
Groundwater Monitoring Report
Carter’s Grocery, Incident No. 6878, UST No. RA-1056
101 Rand Road
Raleigh, Wake County, North Carolina
S&ME Project No. 4305-18-132B
March 19, 2020 6
4.6 Receptors/Potential Receptor Information
Conducting a receptor survey was outside of the scope for this assessment. However, based on the
Comprehensive Site Assessment Report prepared by Terraquest on January 3, 2008, 48 water supply wells are
located within 1,500 feet of the source area. According to the US Fish and Wildlife Nation Wetlands Inventory
accessed on July 21, 2018, four streams, three wetlands and one pond are located within 1,500 feet of the source
area. Municipal water is not available to this area.

5.0 Current Site Assessment Information
5.1 Current Liquid Levels
The depth to groundwater from the top of casing in 10 monitor wells (MW-2 through MW-11) was measured on
March 5 and 6, 2020 from the top of well casings. Measurements ranged from 7.19 feet below top of casing (ft-
btoc) in MW-11, to 16.10 ft-btoc in MW-2.
S&ME personnel measured approximately 0.39 feet of free product in MW-1 on March 5, 2020. Monitor wells
MW-1 and MW-2 have previously contained free product. However, free product was not detected in MW-2 on
June 14, 2018 and on March 5, 2020. The depth to free product in monitor well MW-1 measured 15.52 feet below
top of casing (ft-btoc). The depth to groundwater in monitor well MW-1 measured 15.91 (ft-btoc) on March 5,
2020. Depth to free product and groundwater was measured using an electronic interface probe, which emits an
audible tone when encountering free product, and a distinctly different tone when encountering groundwater.

The elevations for MW-1 through MW-11 were previously measured and recorded. The groundwater elevations
were calculated using the difference in relative top of casing elevations and depth to water. MW-8 had the highest
groundwater elevation at 84.52 feet-relative (ft-rel). The lowest groundwater elevation was found in MW-11,
measuring 77.25 ft-rel. The depth to groundwater measurements and groundwater elevations are provided in
Figure 3 and Table 3.
5.2 Groundwater Monitoring Event
On March 5 and 6, 2020, groundwater samples were collected from 10 monitor wells (MW-2 through MW-11).
Free product was measured in MW-1 and was not sampled. The monitor wells were purged to three casing
volumes or bailed dry and allowed to recover before sampling. Using a new disposable polyethylene bailer at each
well, groundwater samples were collected directly into laboratory supplied containers, place in a cooler on ice and
shipped under standard chain-of-custody record to Con-Test Analytical Laboratory (ConTest) for analysis. The
groundwater samples were analyzed for VOCs by EPA method 6200B. Copies of the field sample summary records
are provided in Appendix IV.
5.3 Water Supply Well Monitoring Event
On March 6, 2020 S&ME personnel collected a sample from the onsite water supply well (WSW-1). The sample
from WSW-1 was collected from an outside spigot located on the well house. The tap was opened and allowed to
run for approximately 15 minutes prior to sampling. The samples were collected directly into the laboratory-
Groundwater Monitoring Report
Carter’s Grocery, Incident No. 6878, UST No. RA-1056
101 Rand Road
Raleigh, Wake County, North Carolina
S&ME Project No. 4305-18-132B
March 19, 2020 7
supplied containers, placed in a cooler on and shipped under standard chain-of-custody record to ConTest for
analysis. The water supply well samples were analyzed for VOCs by EPA method 6200B. Copies of the field sample
summary records are provided in Appendix IV.
5.4 Summary of Groundwater Information
The laboratory analytical results of the groundwater samples collected from four of the ten monitor wells (MW-3,
MW-4, MW-9 and MW-11) indicated the following constituents were detected above their respective 2L
Standards:
 Benzene: MW-3, MW-4, MW-9 and MW-11
 Methyl tert-butyl ether: MW-11
Approximately, 0.39 feet of free product was measured in MW-1 on March 5, 2020 and was not sampled. MW-4 is
located at the former pump island and is upgradient from source area, MW-3, MW-9 and MW-11 are located
down gradient from the source area. Several additional VOCs were reported at concentrations below their
respective 2L Standards in MW-2, MW-3, MW-4, MW-5, MW-7, MW-9 and MW-11. Monitor well MW-5 is a deep
well, with a depth of 40 feet and is located in the former UST basin, approximately 10 feet to the north of MW-1.
No VOCs were detected above the laboratory detection limit in MW-6 and MW-10.

No VOCs were detected above the laboratory detection limit in the sample collected from WSW-1.

A summary of the groundwater analytical results is presented in Table 4 and a summary of the water supply well
analytical results is found in Table 5. A map of constituent levels is presented in Figure 4, and a copy of the
laboratory analytical report is provided in Appendix V.
5.5 Regional and Site Geology and Hydrogeology
5.5.1 Soil and Bedrock
According to the US Department of Agriculture (USDA), Web Soil Survey soils at the site consist of Fuquay-Urban
land complex, with 0 to 6 percent slopes. Well-drained loamy sands and sandy clay loam formed within the
Coastal plain sediments of the Middendorf formation, according to the 1985 US Geological Survey Geologic Map
of North Carolina. Just north of the site is the boundary of the Raleigh Belt with biotite gneiss and schist
formation. Sedimentary and Metamorphic rock are commonly found in these geologic regions. Silty clayey sand,
Sandy silty clay, and clayey sand were encountered during the installation of the monitor wells. Additionally,
during the construction of WSW-1 Middendorf sediments, saprolite and light gray to white granite bedrock were
encountered.
5.5.2 Hydrogeology
S&ME calculated the groundwater elevations for the monitor wells gauged using the depth-to-water
measurements and the top of casing elevations. The groundwater elevations were used to prepare a groundwater
contour map (Figure 3), which indicates that groundwater flows to the northeast. The gradient at the site is
Groundwater Monitoring Report
Carter’s Grocery, Incident No. 6878, UST No. RA-1056
101 Rand Road
Raleigh, Wake County, North Carolina
S&ME Project No. 4305-18-132B
March 19, 2020 8
relatively flat with a steep slope leading to monitor well MW-11. A fate and transport model has not been created;
therefore, the rate of contaminant migration has not been calculated.
5.6 Evaluation of Soil, Groundwater, Surface Water, and Free Product Assessment
Information
5.6.1 Current Extent and Severity of Contamination
During this sampling event, free product was measured in MW-1. Free product was also previously detected in
MW-1. Concentrations of VOCs has generally decreased in MW-3, MW-4, MW-9, and MW-11 since the previous
monitoring event.

Groundwater is flowing to the northeast. Based on this information, MW-3, MW-9 and MW-11 are downgradient
of the former UST system. However, MW-4, which has also had detections of VOCs above the 2L Standards, is
located upgradient from the former UST system at the former pump island. The detections of VOCs in MW-4 are
likely associated with a release of petroleum products from the former product dispensing pumps and/or the two
560-gallon USTs closed in place under the pump island. The extent of the contaminated groundwater plume has
not yet been delineated. The laboratory analytical results from the onsite water supply well (WSW-1) indicated no
VOCs were detected above the laboratory detection limits.

According to previous reports, approximately 10 cubic yards of soil was removed from the site upon excavation of
the 270-gallon kerosene UST in 1991 and the soil was land-farmed on the northwestern portion of the property.
Contaminated soils were detected during installation of WSW-1 in 1993 and petroleum constituents were
reported in soil samples exceeding the 10 mg/kg action level during the UST removal in 2004. However, the
impacted soil at the site was not completely removed and petroleum contaminated soil may remain in place at the
former UST pit and former dispensing pump area. The extent of soil contamination is unknown.
5.6.2 Cleanup Levels Achieved
Soil (soil-to-groundwater maximum soil contaminant concentrations) No
Groundwater (2L standard concentrations) No
Free Product No

Groundwater Monitoring Report
Carter’s Grocery, Incident No. 6878, UST No. RA-1056
101 Rand Road
Raleigh, Wake County, North Carolina
S&ME Project No. 4305-18-132B
March 19, 2020 9
6.0 Conclusions and Recommendations
Based on the current and historical assessment information for the site, the following conclusions are presented:

1. The depth to groundwater was measured at the site on March 5 and 6, 2020 by S&ME personnel. The
groundwater is flowing to the northeast.
2. Free product is present in monitor well MW-1. During the previous monitoring report, free product was
also detected in monitor well MW-1.
3. The laboratory analytical results of the groundwater samples indicate that several VOCs were reported
above their 2L Standards in four monitor wells (MW-3, MW-4, MW-9 and MW-11). No VOC
concentrations were detected in monitor wells MW-6 and MW-10.
4. One water supply well, located approximately 30-feet to the north of the former UST pit, was sampled. No
VOC concentrations were detected above laboratory detection limits.

Based on the above, the following recommendations are presented:

1. Conduct a free product bail down evaluation to determine mobility and recoverability of the free product.
2. Obtain access agreements from property owners of surrounding properties to sample water supply wells.
If contaminant constituents are found, connect to an alternative water (if available) supply and abandon
wells.

Appendices

Appendix I –Figures

SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
11 " = 2,000 '
3-18-20
4305-18-132B
CARTER'S GROCERY (TF-6878)101 RAND ROADRALEIGH, WAKE COUNTY, NORTH CAROLINADrawing Path: Q:\PROJECTS\2018\4305-18-132B Carter's Grocery\FG1_VICINITY.mxd plotted by mverbanic 03-18-20200 2,000 4,000(FEET)
VICINITY MAP
³
REFERENCE:GIS BASE LAYERS WERE OBTAINED FROM THE 2018 ESRI USGS TOPO BASEMAP. THIS MAPIS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONS DISPLAYED AREAPPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEY INFORMATION, UNLESS STATEDOTHERWISE.
SITE
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A
!<
!<WSW-2
WSW-1
RAND RDTEN TEN RD
MW-8
MW-7
MW-4
MW-5
MW-2
MW-6
MW-3
MW-11
MW-9
MW-10
MW-1
!<WATER SUPPLY WELLS
@A MONITOR WELLSSITE BOUNDARY
WAKE COUNTY PROPERTY LINES
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
21 " = 45 '
3-18-20
4305-18-132B
CARTER'S GROCERY (TF-6878)101 RAND ROADRALEIGH, WAKE COUNTY, NORTH CAROLINADrawing Path: Q:\PROJECTS\2018\4305-18-132B Carter's Grocery\FG2_SITE.mxd plotted by mverbanic 03-18-20200 45 90(FEET)
SITE MAP
³
REFERENCE:GIS BASE LAYERS WERE OBTAINED FROM THE 2017 NCEONEMAP.COM AERIALORTHOIMAGERY LAYER. THIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURELOCATIONS DISPLAYED ARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEYINFORMATION, UNLESS STATED OTHERWISE.
FORMER UST BASIN OFTWO 6,000-GALLON GASOLINE TANKS AND ONE 3,000 GALLON GASOLINE TANK (REMOVED)
FORMER PUMP ISLANDAND BASIN OF TWO 560-GALLON GASOLINE USTs(CLOSED IN PLACE)
SITE
FORMER 270-GALLONKEROSENE TANK BASIN(REMOVED)
!<
!<
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A RAND RDTEN TEN RD
WSW-1
WSW-2
MW-8(84.52')
MW-7(83.84')
MW-4(84.05')
MW-5(83.58')
MW-2(83.16')
MW-6(83.20')
MW-3(83.35')
MW-11(77.25')MW-9(82.83')
MW-10(83.23')
MW-1(83.68')
8
4
.5
77.578
78.57
9
79.5
80848
0.5
8181.58283.58
2
.5
83GROUNDWATER FLOW DIRECTIONGROUNDWATER CONTOURS
@A MONITOR WELL
!<LOCATION OF WATER SUPPLY WELLS
LOCATION OF SITEWAKE COUNTY PROPERTY LINES
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
31 " = 50 '
3-19-20
4305-18-132B
CARTER'S GROCERY (TF-6878)101 RAND ROADRALEIGH, WAKE COUNTY, NORTH CAROLINADrawing Path: C:\Users\mverbanic\Desktop\Remote GIS\4305-18-132B Carters Grocery\FG3_GWELEVATION.mxd plotted by mverbanic 03-19-20200 50 100(FEET)
GROUNDWATER CONTOUR MAP
³
REFERENCE:GIS BASE LAYERS WERE OBTAINED FROM THE 2017 NCEONEMAP.COM AERIALORTHOIMAGERY LAYER. THIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURELOCATIONS DISPLAYED ARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEYINFORMATION, UNLESS STATED OTHERWISE.
GROUNDWATER ELEVATIONS MEASURED ON MARCH 5 AND 6, 2020(72.76) : GROUNDWATER ELEVATIONS MEASURED IN FEET-RELATIVE (FT-REL)
SITE
FORMER UST BASIN OFTWO 6,000-GALLON GASOLINE TANKS AND ONE 3,000 GALLON GASOLINE TANK (REMOVED)
FORMER PUMP ISLANDAND BASIN OF TWO 560-GALLON GASOLINE USTs(CLOSED IN PLACE)
FORMER 270-GALLONKEROSENE TANK BASIN(REMOVED)
!<
!<
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A
@A
WSW-2 NS
MW-5 µg/L NAPHTHALENE 0.39 J
MW-4 µg/L BENZENE 47N-BUTYLBENZENE 8.1SEC-BUTYLBENZENE 1.9TERT-BUTYLBENZENE 0.80 JETHYLBENZENE 18ISOPROPYLBENZENE 4.5P-ISOPROPYLTOLUENE 5.4NAPHTHALENE 4.4N-PROPYLBENZENE 3.4TOLUENE 331,2,4-TRIMETHYLBENZENE 1901,3,5-TRIMETHYLBENZENE 86TOTAL XYLENES 370
MW-1 0.39 FT OF FREE PRODUCT
MW-2 µg/L CHLOROMETHANE 0.67 J
WSW-1 BDL
MW-6 BDL
MW-10 BDL
MW-9 µg/L BENZENE 19CHLOROFORM 0.24ETHYLBENZENE 4.9ISOPROPYLBENZENE 0.56METHYL TERT-BUTYL ETHER 0.78NAPHTHALENE 1.2N-PROPYLBENZENE 0.70TOLUENE 0.941,2,4-TRIMETHYLBENZENE 0.781,3,5-TRIMETHYLBENZENE 0.89TOTAL XYLENES 2.1
MW-11 µg/L ACETONE 4.0 JBENZENE 55N-BUTYLBENZENE 0.52SEC-BUTYLBENZENE 0.37 JCHLOROFORM 1.5DIISOPROPYL ETHER 0.33 JISOPROPYLBENZENE 2.9P-ISOPROPYLTOLUENE 0.20 JMETHYL TERT-BUTYL ETHER 25NAPHTHALENE 3.6TOLUENE 0.521,2,4-TRIMETHYLBENZENE 1.2TOTAL XYLENES 6.8
MW-3 µg/L BENZENE 1.8N-BUTYLBENZENE 1.4SEC-BUTYLBENZENE 0.63CHLOROFORM 0.28 JETHYLBENZENE 15ISOPROPYLBENZENE 2.4P-ISOPROPYLTOLUENE 0.32 JNAPHTHALENE 5.6N-PROPYLBENZENE 4.4TOLUENE 101,2,4-TRIMETHYLBENZENE 161,3,5-TRIMETHYLBENZENE 8.7TOTAL XYLENES 30
FORMER UST BASIN OFTWO 6,000-GALLON GASOLINE TANKS AND ONE 3,000 GALLON GASOLINE TANK (REMOVED)
FORMER PUMP ISLANDAND BASIN OF TWO 560-GALLON GASOLINE USTs(CLOSED IN PLACE)
FORMER 270-GALLONKEROSENE TANK BASIN(REMOVED)
MW-7 µg/L 1,2,4-TRIMETHYLBENZENE 0.20 J
MW-8 µg/L CHLOROMETHANE 0.55 J RAND RDTEN TEN RD
@A MONITOR WELLS
!<WATER SUPPLY WELLS
FORMER UST BASIN
LOCATION OF SITEWAKE COUNTY PROPERTY LINES
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
41 " = 50 '
3-18-20
4305-18-132B
CARTER'S GROCERY (TF-6878)101 RAND ROADRALEIGH, WAKE COUNTY, NORTH CAROLINADrawing Path: C:\Users\mverbanic\Desktop\Remote GIS\4305-18-132B Carters Grocery\FG4_CONSTITUENT.mxd plotted by mverbanic 03-18-20200 50 100(FEET)
GROUNDWATER CONSTITUENT MAP
³
NOTES:GROUNDWATER SAMPLES COLLECTED MARCH 5 AND 6, 2020FREE PRODUCT MEASURED IN MW-1 ON MARCH 5, 2020µg/L: MICROGRAMS PER LITERBDL: BELOW DETECTION LIMITJ: DETECTION IS AN ESTIMATED CONCENTRATIONNS: NOT SAMPLED
REFERENCE:GIS BASE LAYERS WERE OBTAINED FROM THE 2017 NCEONEMAP.COM AERIALORTHOIMAGERY LAYER. THIS MAP IS FOR INFORMATIONAL PURPOSES ONLY. ALLFEATURE LOCATIONS DISPLAYED ARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL

Appendix II –Tables

TABLE 1
SITE HISTORY - UST OWNER INFORMATION
Carter's Grocery, TF-6878 RA-1056
101 Rand Road, Raleigh, Wake County, North Carolina
S&ME Project # 4305-18-132B
1-2 Unknown mid-1940s - 1958 6878 Unknown
1-2 1958 - 1991 6878 Both
3 1970 - 1991 6878 Both
4-6 1973 - 2004 26632 Both
101 Rand Road, Raleigh, North Carolina NA
Incident
Number
Owner or
Operator?
Former Address Telephone Number
UST ID
Numbers
Name of Owner and
Operator Dates of Ownership / Operation
George Russell Carter
TABLE 2
SITE HISTORY - UST SYSTEM INFORMATION
Carter's Grocery, TF-6878 RA-1056
101 Rand Road, Raleigh, Wake County, North Carolina
S&ME Project # 4305-18-132B
UST
ID Number
Current
Contents
Previous
Contents
Capacity
(gallons)
Constructi
on Details
Tank
Dimensions
D/L (ft)
Description of
Associated Piping
and Pumps
Date UST
Installed Status of UST
Was Release
Associated With
UST System?
1 None Gasoline 560 Steel Unknown Abandoned in
Place mid-1940s Abandonded in Place
6/8/1991
2 None Gasoline 560 Steel Unknown Abandoned in
Place mid-1940s Abandonded in Place
6/8/1991
3 None Kerosene 270 Unknown Unknown Removed 1/24/1970 Removed 12/21/1991
4 None Gassoline 6,000 Unknown 8' x 16'Removed 12/31/1973 Removed 4/29/2004
5 None Gasoline 6,000 Unknown 8' x 16'Removed 12/31/1973 Removed 4/29/2004
6 None Gasoline 3,000 Unknown 5.3' x 18'Removed 12/31/1973 Removed 4/29/2004
Incident
Number
Associated
USTs
Material
Released
Date of
Release Description of Release
6878 1-2 Gasoline 6/8/1991
26632 3-6 Gasoline and
Kerosene 4/29/2004
Yes
Detection of methyl tert-butyl ether was found in on site water supply well
Soil contamination discovered at time of UST closures
Well ID Date Installed
Well Casing
Depth
(ft-bgs)
Screened
Interval
(ft-bgs)
Well Diameter
(inches)
Total Well Depth
from Top of
Casing
(ft.)
Top of Casing
Elevation
(ft-rel)
Date of
Measurement
Depth to
Free
Product (ft-
BTOC)
Free
Product
Thickness
(ft.)
Depth to
Water
(ft-BTOC)
Groundwater
Elevation* (ft-
rel)
3/9/2005 18.25 81.01
8/29/2007 22.82 76.44
9/21/2007 24.87 74.39
6/3/2013 18.50 1.30 19.81 80.56
6/28/2018 20.92 1.09 22.01 78.19
3/5/2020 15.52 0.39 15.91 83.68
3/9/2005 18.80 80.85
8/29/2007 23.28 76.37
9/21/2007 23.80 75.85
6/3/2013 19.00 0.30 19.30 80.61
6/14/2018 21.01 78.64
3/5/2020 16.10 83.16
3/9/2005 18.33 80.85
8/29/2007 22.90 76.28
9/21/2007 23.38 75.85
6/3/2013 18.30 80.25
6/14/2018 20.68 78.50
3/5/2020 15.83 83.35
3/9/2005 18.63 81.31
8/29/2007 23.26 76.68
9/21/2007 23.79 76.15
6/3/2013 19.13 80.81
6/14/2018 20.98 78.96
3/5/2020 15.89 84.05
3/9/2005 18.69 80.85
8/29/2007 23.14 76.40
9/21/2007 23.64 75.90
6/3/2013 19.20 80.34
6/14/2018 20.89 78.65
3/5/2020 15.96 83.58
8/29/2007 22.91 76.17
9/21/2007 23.39 75.69
6/3/2013 19.00 80.08
6/14/2018 20.68 78.40
3/5/2020 15.88 83.20
8/29/2007 22.87 76.54
9/21/2007 23.37 76.04
6/3/2013 18.76 80.65
6/14/2018 20.56 78.85
3/5/2020 15.57 83.84
8/29/2007 23.19 76.96
9/21/2007 23.77 76.38
6/3/2013 19.02 81.13
6/14/2018 20.91 79.24
3/5/2020 15.63 84.52
9/21/2007 20.73 75.62
6/3/2013 16.46 79.89
6/14/2018 18.17 78.18
3/6/2020 13.52 82.83
9/21/2007 23.21 75.77
6/3/2013 18.77 80.21
6/14/2018 20.51 78.47
3/6/2020 15.75 83.23
6/3/2013 10.00 74.44
6/14/2018 11.68 72.76
3/6/2020 7.19 77.25
Notes:
ft-bgs: feet below ground surface
ft-rel: feet relative
ft-BTOC: feet below top of casing
NM: None measured
S&ME measured relative top of casing elevation for monitor well MW-11 on June 14, 2018.
* : If Free Product is present in a well, groundwater elevation should be calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581]
NM
NM
NM
28.00 99.26
26.00 99.65
NM
WELL CONSTRUCTION AND LIQUID LEVEL DATA
TABLE 3
S&ME Project # 4305-18-132B
101 Rand Road, Raleigh, Wake County, North Carolina
Carter's Grocery, TF-6878 RA-1056
29.00 99.41 NM
30.00 100.15 NM
26.00 99.18 NM
27.00 99.94 NM
MW-1 1/17/2005 8 8.0-28.0 2
MW-2 3/2/2005 9 9.0-26.0 2
MW-3 3/2/2005 9 9.0-26.0 2
MW-4 3/2/2005 10 10.0-27.0 2
40.00 99.54 NM
MW-6 7/25/2007 15 15.0-30.0 2 30.00 99.08 NM
MW-5 3/8/2005 35 35.0-40.0 2
MW-7 7/25/2007 14 14.0-29.0 2
MW-8 7/25/2007 15 15.0-30.0 2
96.35 NM
MW-10 9 9.0-26.0 2 26.00 98.98 NM
MW-9 9/18/2007 10 10.0-25.0 2 25.00
9/18/2007
27.00 84.44 NMMW-11 5/27/2008 12 12.0-27.0 2
Well ID Date Collected
ChloroformChloromethane2-Hexanone4-Methyl-2-pentanone1/20/2005 BDL 9,300 BDL BDL BDL BDL BDL BDL BDL BDL 2,000 BDL BDL BDL BDL BDL BDL BDL BDL 20,000 BDL BDL 10,2007/27/2007 BDL 18,000 BDL BDL BDL BDL BDL BDL BDL BDL 1,300 BDL BDL BDL 890 BDL BDL BDL BDL 22,000 BDL BDL 6,800
6/3/2013
6/28/2018
3/5/2020
3/9/2005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL7/27/2007 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL6/3/2013 BDL 1.3 2.4 0.31 J BDL BDL BDL BDL BDL BDL 3.1 BDL 0.37 J 0.25 J BDL BDL 6.2 1.8 BDL 10 22 5.1 22.4
6/14/2018 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
3/5/2020 BDL BDL BDL BDL BDL BDL 0.67 J BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
3/9/2005 BDL 29 BDL 1.1 BDL BDL BDL BDL BDL BDL 38 BDL 6.0 BDL BDL BDL 14 BDL BDL 42 BDL BDL 221
7/27/2007 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
6/3/2013 BDL 0.83 0.47 J BDL BDL BDL BDL BDL BDL BDL 2.4 BDL 0.18 J BDL BDL BDL 4.1 0.78 BDL 8.6 8.0 1.8 166/14/2018 BDL 27 2.7 1.4 BDL 0.80 BDL BDL BDL BDL 50 BDL 6.7 0.82 BDL BDL 16 11 0.24 J 16 22 27 142
3/5/2020 BDL 1.8 1.4 0.63 BDL 0.28 J BDL BDL BDL BDL 15 BDL 2.4 0.32 J BDL BDL 5.6 4.4 BDL 10 16 8.7 30
3/9/2005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 130 BDL 27 BDL BDL BDL BDL BDL BDL 110 BDL BDL 720
7/27/2007 BDL 19 3.3 2.2 BDL BDL BDL BDL BDL BDL 36 BDL 9.6 7.2 BDL BDL BDL BDL BDL 45 BDL BDL 229
6/3/2013 270 4.5 8.5 1.1 0.54 0.24 J BDL 2.0 1.6 BDL 22 11 4.4 3.8 14 4.2 25 6 BDL 72 210 96 800
6/14/2018 BDL 86 3.0 1.7 0.81 BDL BDL BDL BDL BDL 19 BDL 4.4 5.3 1.7 BDL 13 3.6 0.30 J 53 260 *97 680*3/6/2020*BDL 47 8.1 1.9 0.80 J BDL BDL BDL BDL BDL 18 BDL 4.5 5.4 BDL BDL 4.4 3.4 BDL 33 190 86 3703/9/20005 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
7/27/2007 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
6/3/2013 BDL 7.5 11 2.7 0.17 J BDL BDL BDL BDL BDL 82 BDL 9.8 1.6 BDL BDL 18 32 BDL 170 170 57 450
6/14/2018 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
3/5/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.39 J BDL BDL BDL BDL BDL BDL
7/27/2007 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
6/3/2013 BDL 0.17 J 0.18 J BDL BDL 0.42 J BDL BDL BDL BDL 0.54 BDL BDL BDL BDL BDL BDL 0.23 J BDL 1.9 2.1 0.51 3.5
6/14/2018 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
3/6/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
7/27/2007 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
6/3/2013 BDL 0.17 J BDL BDL BDL 0.33 J BDL BDL BDL BDL 0.41 J BDL BDL BDL BDL BDL BDL 0.14 J BDL 1.3 1.6 0.51 3.0
6/14/2018 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
3/5/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.20 J BDL BDL
7/27/2007 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
6/3/2013 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.23 J BDL BDL BDL BDL BDL BDL BDL BDL 0.83 0.50 0.14 1.3
6/14/2018 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
3/5/2020 BDL BDL BDL BDL BDL BDL 0.55 J BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
9/21/2007 BDL 30 BDL 2.1 BDL BDL BDL BDL BDL 2.2 190 BDL 13 5 27 BDL BDL BDL BDL 370 BDL BDL 830
6/3/2013 BDL 0.35 J BDL BDL BDL 0.78 BDL BDL BDL BDL 0.49 J BDL BDL BDL 4.7 BDL BDL 0.14 J BDL 1.9 0.99 0.27 J 3.0
6/14/2018 BDL 110 0.65 0.39 J BDL BDL BDL BDL BDL 0.27 J 20 BDL 2.4 0.22 J 12 BDL 5.3 2.6 0.20 J 3.0 0.95 3.9 1.6
3/6/2020 BDL 19 BDL BDL BDL 0.24 BDL BDL BDL BDL 4.9 BDL 0.56 BDL 0.78 BDL 1.2 0.70 BDL 0.94 0.78 0.89 2.1
9/21/2007 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 57 BDL BDL BDL BDL BDL BDL BDL BDL
6/3/2013 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL 0.20 J BDL BDL BDL BDL BDL BDL BDL BDL 0.64 0.43 J 0.10 J 1.1
6/14/2018 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
3/6/2020 BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL BDL
5/27/2008 BDL 390 BDL BDL BDL 6.4 BDL BDL BDL 2.0 2.9 BDL 2.2 BDL 52 BDL 8.4 BDL BDL BDL 25 4.4 110
6/3/2013 BDL 69 0.35 J 0.18 J BDL 4.2 BDL 0.23 J 2.8 1.2 0.37 J BDL 1.2 0.14 J 98 BDL 3.8 0.13 J BDL 0.87 7.6 4.3 42
6/14/2018 BDL 200 1.0 0.68 BDL 1.8 BDL BDL BDL 0.88 0.23 J BDL 4.6 0.41 J 69 BDL 9.0 BDL BDL 1.5 0.80 BDL 4.7
3/6/2020 4.0 J 55 0.52 0.37 J BDL 1.5 BDL BDL BDL 0.33 J BDL BDL 2.9 0.20 J 25 BDL 3.6 BDL BDL 0.52 1.2 BDL 6.8
6,000 1 70 70 70 70 3 0.02 0.4 70 600 280 70 25 20 4,000 6 70 70 600 400 400 500
6,000,000 5,000 6,900 8,500 15,000 70,000 3,000 50 400 70,000 84,500 2,800,000 25,000 11,700 20,000 4,000,000 6,000 30,000 70,000 260,000 28,500 25,000 85,500
Notes:
Analytes that are not shown for the method were not detected.* Indicates sample was run at a dilution.
Concentrations are reported in micrograms per liter (µg/L).GCL: Gross Contaminantion Level
2L Standard: North Carolina Groundwater Quality Standards: 15A NCAC 2L.0202 BDL: Not detected in concentrations exceeding laboratory detection limits
Concentrations exceeding the laboratory's reporting limits are shown in BOLD fields.NE: Regulatory standard not established for analyte
Concentrations exceeding the 2L Standards are shown in Shaded and BOLD fields.J: Detection is an estimated concentration
Concentrations exceeding the Gross Contamination Levels are shown in Underlined, Shaded, and BOLD fields.
MW-3
MW-4
MW-5
MW-6
Free Product - 0.39 feet thickness
SUMMARY OF GROUNDWATER SAMPLING RESULTS
Carter's Grocery, TF-6878 RA-1056
TABLE 4
101 Rand Road, Raleigh, Wake County, North Carolina
S&ME Project # 4305-18-132B
Analytical Method ->1,2-dibromoethanen-PropylbenzeneBenzeneNaphthaleneDi-isopropyl etherContaminant of Concern ->AcetoneVolatile Organic Compounds (VOCs) by EPA Method 6200B (µg/L)p-IsopropyltolueneStyrenetert-butylbenzene2L Standards
GCLs Total xylenes1,2-dichloroethanesec-butylbenzeneIsoproplybenzeneMethyl tert-butyl etherEthylbenzenen-butylbenzene1,3,5-TrimethylbenzeneToluene1,2,4-TrimethylbenzeneFree Product - 1.3 feet thickness
Free Product - 1.09 feet thickness
MW-1
MW-2
MW-7
MW-8
MW-9
MW-10
MW-11
Volatile Organic Compounds (VOCs) by EPA Method
6200B (µg/L)
Well ID Date Collected
6/3/2018 BDL
6/15/2018 BDL
3/6/2020 BDL
6/15/2018 Not Sampled
3/6/2020 Not Sampled
6/3/2013 BDL
6/15/2018 Not Sampled
3/6/2020 Not Sampled
Consituent Specific
Consituent Specific
Notes:
Analytes that are not shown for the method were not detected.
Concentrations are reported in micrograms per liter (µg/L).
2L Standard: North Carolina Groundwater Quality Standards: 15A NCAC 2L.0202
GCL - Gross Contaminantion Level
BDL: Not detected in concentrations exceeding laboratory detection limits
Analytical Method ->
TABLE 5
SUMMARY OF WATER SUPPLY WELL SAMPLING RESULTS
Carter's Grocery, TF-6878 RA-1056
101 Rand Road, Raleigh, Wake County, North Carolina
S&ME Project # 4305-18-132B
2L Standards
GCLs
Contaminant of Concern ->
Consituent Specific
WSW-1
WSW-2
WSW-4

Appendix III – Site Photographs

Groundwater Monitoring Report
Carter’s Grocery, Incident No. 6878, UST No. RA-1056
101 Rand Road
Raleigh, Wake County, North Carolina
S&ME Project No. 4305-18-132B
March 18, 2020 i

Date: 3/5/2020 Photographer: JW Location / Orientation MW-1 / West
Remarks MW-1 location

Date: 3/5/2020 Photographer: JW Location / Orientation MW-2 / South
Remarks MW-2 location
Groundwater Monitoring Report
Carter’s Grocery, Incident No. 6878, UST No. RA-1056
101 Rand Road
Raleigh, Wake County, North Carolina
S&ME Project No. 4305-18-132B
March 18, 2020 ii

Date: 3/5/2020 Photographer: JW Location / Orientation MW-3 / Southeast
Remarks MW-3 location

Date: 3/5/2020 Photographer JW Location / Orientation Parking area adjacent to former Pump Island / East
Remarks MW-4
Groundwater Monitoring Report
Carter’s Grocery, Incident No. 6878, UST No. RA-1056
101 Rand Road
Raleigh, Wake County, North Carolina
S&ME Project No. 4305-18-132B
March 18, 2020 iii

Date: 3/5/2020 Photographer: JW Location / Orientation MW-5 / West
Remarks MW-5 Location

Date: 3/5/2020 Photographer: JW Location / Orientation Intersection of Rand Road and Ten Ten Road / Southwest
Remarks MW-7
Groundwater Monitoring Report
Carter’s Grocery, Incident No. 6878, UST No. RA-1056
101 Rand Road
Raleigh, Wake County, North Carolina
S&ME Project No. 4305-18-132B
March 18, 2020 iv

Date: 3/5/2020 Photographer: JW Location / Orientation Ten Ten Road / East
Remarks MW-8

Date: 3/5/2020 Photographer JW Location / Orientation Rand Road / East
Remarks Property WSW-2 and MW-10
Groundwater Monitoring Report
Carter’s Grocery, Incident No. 6878, UST No. RA-1056
101 Rand Road
Raleigh, Wake County, North Carolina
S&ME Project No. 4305-18-132B
March 18, 2020 v

Date: 3/5/2020 Photographer: JW Location / Orientation MW-9 / Southeast
Remarks MW-9 location

Date: 3/5/2020 Photographer: JW Location / Orientation MW-11 Property / Southeast
Remarks MW-11

Appendix IV – Field Data Sheets
° F
Date Time
3/5/20 11:45 4.0 10.0
3/5/20 11:45 µS/cm
15.91 ft-TOC inch
28.00 ft-TOC gal
12.09 feet gal
20 ft-GRD gal
-0.25 ft-GRD
End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
James Waters 3/5/2020
Product is at 15.52 ft. below top of casing. 0.39 ft. of product. MW-1 is not sampled.
9/13/17 8:00 AM
Name Signature Date
Analytical Data
Method Method Container
6200B (+MTBE, IPE, & EDB)
Sample Method:Bailer Sample Time:
(Gal)
Petroleum Odors
Total Volume Purged:Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 9.9
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:
Total Well Depth:Well Volume 2.0
Height of Water Column:3 * Well Volume 5.9
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather:Overcast Air Temp:55
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:March 5, 2020
Sampled By:James Waters Sample Time:
Project Number:4305-18-132B Purge Date:March 5, 2020
Source Well:MW-1 Purge Time (Min.):
GROUNDWATER SAMPLING FORM
Project Name:TF-6878 Carter’s Grocery
Project Location:101 Rand Road Raleigh, NC
° F
Date Time
3/5/20 11:45 4.0 10.0
3/5/20 11:45 µS/cm
16.10 ft-TOC inch
26.00 ft-TOC gal
9.90 feet gal
17 ft-GRD gal
-0.3 ft-GRD
12:05 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
12:10 5.0 17.7 96 NM
12:15 4.1 16.6 52 NM
12:20 4.1 16.7 46 NM
12:25
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
James Waters 3/5/2020
9/13/17 8:00 AM
Name Signature Date
Analytical Data
Method Method Container
6200B (+MTBE, IPE, & EDB)
Sample Method:Bailer Sample Time:
(Gal)
1.6 No Odors
3.3 No Odors
5.0 No Odors
Total Volume Purged:5.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 8.1
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:12:20
Total Well Depth:Well Volume 1.6
Height of Water Column:3 * Well Volume 4.8
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather:Overcast Air Temp:55
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:March 5, 2020
Sampled By:James Waters Sample Time:12:25
Project Number:4305-18-132B Purge Date:March 5, 2020
Source Well:MW-2 Purge Time (Min.):15
GROUNDWATER SAMPLING FORM
Project Name:TF-6878 Carter’s Grocery
Project Location:101 Rand Road Raleigh, NC
° F
Date Time
3/5/20 11:45 4.0 10.0
3/5/20 11:45 µS/cm
15.83 ft-TOC inch
26.00 ft-TOC gal
10.17 feet gal
17 ft-GRD gal
-0.3 ft-GRD
12:30 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
12:35 4.1 18.2 57 NM
12:40 4.1 18.8 38 NM
12:45 4.1 18.9 37 NM
12:50
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
James Waters 3/5/2020
9/13/17 8:00 AM
Name Signature Date
Analytical Data
Method Method Container
6200B (+MTBE, IPE, & EDB)
Sample Method:Bailer Sample Time:
(Gal)
1.7 No Odors
3.4 No Odors
5.0 No Odors
Total Volume Purged:5.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 8.3
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:12:45
Total Well Depth:Well Volume 1.7
Height of Water Column:3 * Well Volume 5.0
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather:Overcast Air Temp:55
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:March 5, 2020
Sampled By:James Waters Sample Time:12:50
Project Number:4305-18-132B Purge Date:March 5, 2020
Source Well:MW-3 Purge Time (Min.):15
GROUNDWATER SAMPLING FORM
Project Name:TF-6878 Carter’s Grocery
Project Location:101 Rand Road Raleigh, NC
° F
Date Time
3/5/20 11:45 4.0 10.0
3/5/20 11:45 µS/cm
15.89 ft-TOC inch
27.00 ft-TOC gal
11.11 feet gal
17 ft-GRD gal
-0.3 ft-GRD
12:55 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
13:00 3.9 20 42 NM
13:05 3.9 20.2 66 NM
13:10 3.8 20.2 87 NM
13:15
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
James Waters 3/5/2020
9/13/17 8:00 AM
Name Signature Date
Analytical Data
Method Method Container
6200B (+MTBE, IPE, & EDB)
Sample Method:Bailer Sample Time:
(Gal)
2.0 Petroleum Odors
4.0 Petroleum Odors
6.0 Petroleum Odors
Total Volume Purged:6.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 9.1
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:13:10
Total Well Depth:Well Volume 1.8
Height of Water Column:3 * Well Volume 5.4
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather:Overcast Air Temp:55
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:March 5, 2020
Sampled By:James Waters Sample Time:13:15
Project Number:4305-18-132B Purge Date:March 5, 2020
Source Well:MW-4 Purge Time (Min.):15
GROUNDWATER SAMPLING FORM
Project Name:TF-6878 Carter’s Grocery
Project Location:101 Rand Road Raleigh, NC
° F
Date Time
3/5/20 11:45 4.0 10.0
3/5/20 11:45 µS/cm
15.96 ft-TOC inch
40.00 ft-TOC gal
24.04 feet gal
5 ft-GRD gal
-0.025 ft-GRD
13:20 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
13:30 4.2 19.4 81 NM
13:40 4.5 19 107 NM
13:50 4.2 18.9 111 NM
13:55
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
James Waters 3/5/2020
9/13/17 8:00 AM
Name Signature Date
Analytical Data
Method Method Container
6200B (+MTBE, IPE, & EDB)
Sample Method:Bailer Sample Time:
(Gal)
4.0 No Odors
8.0 No Odors
12.0 No Odors
Total Volume Purged:12.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 19.6
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:13:50
Total Well Depth:Well Volume 3.9
Height of Water Column:3 * Well Volume 11.8
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather:Overcast Air Temp:55
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:March 5, 2020
Sampled By:James Waters Sample Time:13:55
Project Number:4305-18-132B Purge Date:March 5, 2020
Source Well:MW-5 Purge Time (Min.):30
GROUNDWATER SAMPLING FORM
Project Name:TF-6878 Carter’s Grocery
Project Location:101 Rand Road Raleigh, NC
° F
Date Time
3/5/20 11:45 4.0 10.0
3/5/20 11:45 µS/cm
15.88 ft-TOC inch
30.00 ft-TOC gal
14.12 feet gal
15 ft-GRD gal
-0.4 ft-GRD
14:00 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
14:05 4.3 17.6 118 NM
14:10 4.0 17.2 133 NM
14:15 3.9 17.3 134 NM
14:20
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
James Waters 3/5/2020
9/13/17 8:00 AM
Name Signature Date
Analytical Data
Method Method Container
6200B (+MTBE, IPE, & EDB)
Sample Method:Bailer Sample Time:
(Gal)
2.3 No Odors
4.6 No Odors
7.0 No Odors
Total Volume Purged:7.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 11.5
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:14:15
Total Well Depth:Well Volume 2.3
Height of Water Column:3 * Well Volume 6.9
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather:Overcast Air Temp:55
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:March 5, 2020
Sampled By:James Waters Sample Time:14:20
Project Number:4305-18-132B Purge Date:March 5, 2020
Source Well:MW-6 Purge Time (Min.):15
GROUNDWATER SAMPLING FORM
Project Name:TF-6878 Carter’s Grocery
Project Location:101 Rand Road Raleigh, NC
° F
Date Time
3/5/20 11:45 4.0 10.0
3/5/20 11:45 µS/cm
15.57 ft-TOC inch
29.00 ft-TOC gal
13.43 feet gal
15 ft-GRD gal
-0.3 ft-GRD
14:25 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
14:30 3.7 18.8 322 NM
14:35 3.6 20.3 411 NM
14:40 3.6 20.3 415 NM
14:45
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
James Waters 3/5/2020
9/13/17 8:00 AM
Name Signature Date
Analytical Data
Method Method Container
6200B (+MTBE, IPE, & EDB)
Sample Method:Bailer Sample Time:
(Gal)
2.3 No Odors
4.6 No Odors
7.0 No Odors
Total Volume Purged:7.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 11.0
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:14:40
Total Well Depth:Well Volume 2.2
Height of Water Column:3 * Well Volume 6.6
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather:Overcast Air Temp:55
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:March 5, 2020
Sampled By:James Waters Sample Time:14:45
Project Number:4305-18-132B Purge Date:March 5, 2020
Source Well:MW-7 Purge Time (Min.):15
GROUNDWATER SAMPLING FORM
Project Name:TF-6878 Carter’s Grocery
Project Location:101 Rand Road Raleigh, NC
° F
Date Time
3/5/20 11:45 4.0 10.0
3/5/20 11:45 µS/cm
15.63 ft-TOC inch
30.00 ft-TOC gal
14.37 feet gal
15 ft-GRD gal
-0.5 ft-GRD
15:00 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
15:05 3.9 19.9 96 NM
15:10 3.7 19.5 94 NM
15:15 3.7 19.3 94 NM
15:20
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
James Waters 3/5/2020
9/13/17 8:00 AM
Name Signature Date
Analytical Data
Method Method Container
6200B (+MTBE, IPE, & EDB)
Sample Method:Bailer Sample Time:
(Gal)
2.3 No Odors
4.6 No Odors
7.0 No Odors
Total Volume Purged:7.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 11.7
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:15:15
Total Well Depth:Well Volume 2.3
Height of Water Column:3 * Well Volume 7.0
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather:Overcast Air Temp:55
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:March 5, 2020
Sampled By:James Waters Sample Time:15:20
Project Number:4305-18-132B Purge Date:March 5, 2020
Source Well:MW-8 Purge Time (Min.):15
GROUNDWATER SAMPLING FORM
Project Name:TF-6878 Carter’s Grocery
Project Location:101 Rand Road Raleigh, NC
° F
Date Time
3/6/20 09:40 4.0 10.0
3/6/20 09:40 µS/cm
13.52 ft-TOC inch
25.00 ft-TOC gal
11.48 feet gal
15 ft-GRD gal
-0.2 ft-GRD
10:00 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
10:05 4.1 17.5 148 NM
10:10 4.2 17.7 130 NM
10:15 4.3 17.8 115 NM
10:20
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
James Waters 3/6/2020
9/13/17 8:00 AM
Name Signature Date
Analytical Data
Method Method Container
6200B (+MTBE, IPE, & EDB)
Sample Method:Bailer Sample Time:
(Gal)
2.0 No Odors
4.0 No Odors
6.0 No Odors
Total Volume Purged:6.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 9.4
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:10:15
Total Well Depth:Well Volume 1.9
Height of Water Column:3 * Well Volume 5.6
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather:Sunny Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:March 6, 2020
Sampled By:James Waters Sample Time:10:20
Project Number:4305-18-132B Purge Date:March 6, 2020
Source Well:MW-9 Purge Time (Min.):15
GROUNDWATER SAMPLING FORM
Project Name:TF-6878 Carter’s Grocery
Project Location:101 Rand Road Raleigh, NC
° F
Date Time
3/6/20 09:40 4.0 10.0
3/6/20 09:40 µS/cm
15.75 ft-TOC inch
26.00 ft-TOC gal
10.25 feet gal
17 ft-GRD gal
-0.5 ft-GRD
10:30 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
10:35 4.1 18.7 216 NM
10:40 4.1 19 213 NM
10:45 4.2 19 210 NM
10:50
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
James Waters 3/6/2020
9/13/17 8:00 AM
Name Signature Date
Analytical Data
Method Method Container
6200B (+MTBE, IPE, & EDB)
Sample Method:Bailer Sample Time:
(Gal)
1.6 No Odors
3.3 No Odors
5.0 No Odors
Total Volume Purged:5.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 8.4
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:10:45
Total Well Depth:Well Volume 1.7
Height of Water Column:3 * Well Volume 5.0
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather:Sunny Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:March 6, 2020
Sampled By:James Waters Sample Time:10:50
Project Number:4305-18-132B Purge Date:March 6, 2020
Source Well:MW-10 Purge Time (Min.):15
GROUNDWATER SAMPLING FORM
Project Name:TF-6878 Carter’s Grocery
Project Location:101 Rand Road Raleigh, NC
° F
Date Time
3/6/20 09:40 4.0 10.0
3/6/20 09:40 µS/cm
7.19 ft-TOC inch
27.00 ft-TOC gal
19.81 feet gal
15 ft-GRD gal
-0.15 ft-GRD
11:15 End Time:
gal
Time pH
Temp
Cond Turbidity

(s.u.)(°C) µS/cm (NTU)
11:20 4.5 17.4 104 NM
11:25 4.6 17.6 105 NM
11:30 4.5 17.8 107 NM
11:35
Qty Container Pres.Qty Pres.
3 40mL VOAs HCl
(1)
Notes:
Form Revision Date:
James Waters 3/6/2020
9/13/17 8:00 AM
Name Signature Date
Analytical Data
Method Method Container
6200B (+MTBE, IPE, & EDB)
Sample Method:Bailer Sample Time:
(Gal)
3.3 No Odors
6.6 No Odors
10.0 No Odors
Total Volume Purged:10.0 Well Purged Dry?:No
Field Parameters
Cumulative Volume Comments
Screen Length:5 * Well Volume 16.2
Stickup Height:
Well Purging Information
Purge Method:Bailer Purge Start Time:11:30
Total Well Depth:Well Volume 3.2
Height of Water Column:3 * Well Volume 9.7
Water Level & Well Data
Measuring Point:Top of Casing Well Volume
Depth to Water:Well Diameter 2
pH 4.00, 7.00, 10.00 7.0
Conductivity 1,413 1,413 µS/cm
Weather:Sunny Air Temp:60
Equipment Calibration Information:
Equipment Calibration Solution Calibration Check
Locked?:Yes Sample Date:March 6, 2020
Sampled By:James Waters Sample Time:11:35
Project Number:4305-18-132B Purge Date:March 6, 2020
Source Well:MW-11 Purge Time (Min.):15
GROUNDWATER SAMPLING FORM
Project Name:TF-6878 Carter’s Grocery
Project Location:101 Rand Road Raleigh, NC
4.00 7.00 10.00
μS/cm μS/cm
°C μS/cm
Qty Pres.Qty Pres.
3 HCl
Date
(1)
(2)
Revision:
Project Number:4305-18-132 B Sample Date:Friday, March 6, 2020
Client Name/Contact:NCDEQ Water Supply Well ID:WSW-1
WATER SUPPLY WELL SAMPLING FORM
Project Name:TF-6867 Carter’s Grocery
Project Location:101 Rand Road Raleigh, NC
POE Present (Y/N): N Owner Phone No.:919-772-4456
Equipment Calibration Information:
Weather:Sunny Well Address: 101 Rand Road
Air Temp (°F):60 Owner Name:Carter Heating and Air
Well Purging Information
Purge Rate (GPM): 5.0 Purge Start Time:11:59
pH 3/6/20 09:40 4.00, 7.00, 10.00
Conductivity 3/6/20 09:40 1413 1,413
Equipment Date Time Calibration Solution Calibration Check
Volume Purged (Gal):75.0 Purge End Time:12:05
Field Parameters and Sampling
Total Volume (Gal)Time pH (s.u.)Temperature Conductivity
25.00 11:55 6.7 17.5 129.3
50.00 12:00 6.85 17.6 129.1
75.00 12:05 6.97 17.7 128..9
Sample ID Sample Location Sample Date Sample Time
6200B (+MTBE, IPE, & EDB)40mL VOAs
WSW-1 Hose Bib at Well Head 3/6/2020 12:10
Method Container Method Container
Additional Comments (description of location of sample port, water well, filters, etc.)Well / System Photographs
Well House is located behind the fence to the NE of the building on the property. The sampling spigot is located
on the side of the Well House
Site Sketch
9/1/17 13:30
Name Signature
James Waters 3/6/2020

Appendix V – Laboratory Analytical Reports and Chain of Custody
Forms

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
March 17, 2020
Michael Pfeifer
S&ME, Inc - Raleigh, NC
3201 Spring Forest Rd.
Raleigh, NC 27616
Project Location: 101 Rand Road., Raleigh, NC
Client Job Number:
Project Number: 4305-18-132B
Laboratory Work Order Number: 20C0345
Enclosed are results of analyses for samples received by the laboratory on March 6, 2020. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 42
Table of Contents
Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 5
20C0345-01 5
20C0345-02 7
20C0345-03 9
20C0345-04 11
20C0345-05 13
20C0345-06 15
20C0345-07 17
20C0345-08 19
20C0345-09 21
20C0345-10 23
20C0345-11 25
Sample Preparation Information 27
QC Data 28
Volatile Organic Compounds by GC/MS 28
B253782 28
B253893 32
Flag/Qualifier Summary 36
Certifications 37
Chain of Custody/Sample Receipt 39
Page 2 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
3/17/2020
S&ME, Inc - Raleigh, NC
3201 Spring Forest Rd.
Raleigh, NC 27616
ATTN: Michael Pfeifer
4305-18-132B
20C0345
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
101 Rand Road., Raleigh, NC
MW-2 20C0345-01 Ground Water SM21-22 6200B
MW-3 20C0345-02 Ground Water SM21-22 6200B
MW-4 20C0345-03 Ground Water SM21-22 6200B
MW-5 20C0345-04 Ground Water SM21-22 6200B
MW-6 20C0345-05 Ground Water SM21-22 6200B
MW-7 20C0345-06 Ground Water SM21-22 6200B
MW-8 20C0345-07 Ground Water SM21-22 6200B
MW-9 20C0345-08 Ground Water SM21-22 6200B
MW-10 20C0345-09 Ground Water SM21-22 6200B
MW-11 20C0345-10 Ground Water SM21-22 6200B
WSW-1 20C0345-11 Water SM21-22 6200B
[TOC_1]Sample Summary[TOC]
Page 3 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method 6200B elevated reporting limit for sample 20C0345-03 due to high concentrations of target compounds.
[TOC_1]Case Narrative[TOC]
SM21-22 6200B
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
1,2,3-Trichlorobenzene
20C0345-03[MW-4], B253893-BLK1, B253893-BS1, B253893-BSD1, S046512-CCV1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
Naphthalene
B253893-BS1
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
RL-11
20C0345-03[MW-4]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 4 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-01
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 3/5/2020 12:25
[TOC_2]20C0345-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/10/20 5:03 LBDg/L3.8 3/9/20SM21-22 6200B1Acetone
ND 0.50 3/10/20 5:03 LBDg/L0.18 3/9/20SM21-22 6200B1Benzene
ND 0.50 3/10/20 5:03 LBDg/L0.15 3/9/20SM21-22 6200B1Bromobenzene
ND 0.50 3/10/20 5:03 LBDg/L0.32 3/9/20SM21-22 6200B1Bromochloromethane
ND 0.50 3/10/20 5:03 LBDg/L0.16 3/9/20SM21-22 6200B1Bromodichloromethane
ND 0.50 3/10/20 5:03 LBDg/L0.46 3/9/20SM21-22 6200B1Bromoform
ND 2.0 3/10/20 5:03 LBDg/L0.78 3/9/20SM21-22 6200B1Bromomethane
ND 5.0 3/10/20 5:03 LBDg/L1.9 3/9/20SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/10/20 5:03 LBDg/L0.21 3/9/20SM21-22 6200B1n-Butylbenzene
ND 0.50 3/10/20 5:03 LBDg/L0.16 3/9/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/10/20 5:03 LBDg/L0.17 3/9/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/10/20 5:03 LBDg/L0.11 3/9/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/10/20 5:03 LBDg/L0.15 3/9/20SM21-22 6200B1Chlorobenzene
ND 50 3/10/20 5:03 LBDg/L11 3/9/20SM21-22 6200B1Ethanol
ND 0.50 3/10/20 5:03 LBDg/L0.21 3/9/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/10/20 5:03 LBDg/L0.35 3/9/20SM21-22 6200B1Chloroethane
ND 0.50 3/10/20 5:03 LBDg/L0.17 3/9/20SM21-22 6200B1Chloroform
0.67 1.0 3/10/20 5:03 LBDg/L0.45 3/9/20SM21-22 6200B1JChloromethane
ND 0.50 3/10/20 5:03 LBDg/L0.12 3/9/20SM21-22 6200B12-Chlorotoluene
ND 0.50 3/10/20 5:03 LBDg/L0.14 3/9/20SM21-22 6200B14-Chlorotoluene
ND 0.50 3/10/20 5:03 LBDg/L0.19 3/9/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/10/20 5:03 LBDg/L0.16 3/9/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/10/20 5:03 LBDg/L0.12 3/9/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/10/20 5:03 LBDg/L0.13 3/9/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/10/20 5:03 LBDg/L0.26 3/9/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/10/20 5:03 LBDg/L0.16 3/9/20SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/10/20 5:03 LBDg/L0.41 3/9/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 3/10/20 5:03 LBDg/L0.32 3/9/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/10/20 5:03 LBDg/L0.13 3/9/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/10/20 5:03 LBDg/L0.31 3/9/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/10/20 5:03 LBDg/L0.20 3/9/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 3/10/20 5:03 LBDg/L0.11 3/9/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/10/20 5:03 LBDg/L0.20 3/9/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 3/10/20 5:03 LBDg/L0.16 3/9/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/10/20 5:03 LBDg/L0.13 3/9/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/10/20 5:03 LBDg/L0.23 3/9/20SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/10/20 5:03 LBDg/L0.17 3/9/20SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/10/20 5:03 LBDg/L0.13 3/9/20SM21-22 6200B1Ethylbenzene
ND 5.0 3/10/20 5:03 LBDg/L1.5 3/9/20SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/10/20 5:03 LBDg/L0.17 3/9/20SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/10/20 5:03 LBDg/L0.20 3/9/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/10/20 5:03 LBDg/L0.25 3/9/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/10/20 5:03 LBDg/L0.34 3/9/20SM21-22 6200B1Methylene Chloride
ND 5.0 3/10/20 5:03 LBDg/L1.7 3/9/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
[TOC_1]Sample Results[TOC]
Page 5 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-01
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 3/5/2020 12:25
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/10/20 5:03 LBDg/L0.31 3/9/20SM21-22 6200B1Naphthalene
ND 0.50 3/10/20 5:03 LBDg/L0.13 3/9/20SM21-22 6200B1n-Propylbenzene
ND 0.50 3/10/20 5:03 LBDg/L0.11 3/9/20SM21-22 6200B1Styrene
ND 0.50 3/10/20 5:03 LBDg/L0.22 3/9/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/10/20 5:03 LBDg/L0.18 3/9/20SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/10/20 5:03 LBDg/L0.14 3/9/20SM21-22 6200B1Toluene
ND 1.0 3/10/20 5:03 LBDg/L0.57 3/9/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/10/20 5:03 LBDg/L0.40 3/9/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/10/20 5:03 LBDg/L0.20 3/9/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/10/20 5:03 LBDg/L0.16 3/9/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 3/10/20 5:03 LBDg/L0.24 3/9/20SM21-22 6200B1Trichloroethylene
ND 0.50 3/10/20 5:03 LBDg/L0.33 3/9/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/10/20 5:03 LBDg/L0.25 3/9/20SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/10/20 5:03 LBDg/L0.18 3/9/20SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/10/20 5:03 LBDg/L0.14 3/9/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 3/10/20 5:03 LBDg/L10 3/9/20SM21-22 6200B1Vinyl Acetate
ND 0.50 3/10/20 5:03 LBDg/L0.45 3/9/20SM21-22 6200B1Vinyl Chloride
ND 1.0 3/10/20 5:03 LBDg/L0.30 3/9/20SM21-22 6200B1m+p Xylene
ND 0.50 3/10/20 5:03 LBDg/L0.17 3/9/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 92.4 3/10/20 5:0370-130
Toluene-d8 99.2 3/10/20 5:0370-130
4-Bromofluorobenzene 97.8 3/10/20 5:0370-130
Page 6 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-02
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 3/5/2020 12:50
[TOC_2]20C0345-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/10/20 5:30 LBDg/L3.8 3/9/20SM21-22 6200B1Acetone
1.8 0.50 3/10/20 5:30 LBDg/L0.18 3/9/20SM21-22 6200B1Benzene
ND 0.50 3/10/20 5:30 LBDg/L0.15 3/9/20SM21-22 6200B1Bromobenzene
ND 0.50 3/10/20 5:30 LBDg/L0.32 3/9/20SM21-22 6200B1Bromochloromethane
ND 0.50 3/10/20 5:30 LBDg/L0.16 3/9/20SM21-22 6200B1Bromodichloromethane
ND 0.50 3/10/20 5:30 LBDg/L0.46 3/9/20SM21-22 6200B1Bromoform
ND 2.0 3/10/20 5:30 LBDg/L0.78 3/9/20SM21-22 6200B1Bromomethane
ND 5.0 3/10/20 5:30 LBDg/L1.9 3/9/20SM21-22 6200B12-Butanone (MEK)
1.4 0.50 3/10/20 5:30 LBDg/L0.21 3/9/20SM21-22 6200B1n-Butylbenzene
0.63 0.50 3/10/20 5:30 LBDg/L0.16 3/9/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/10/20 5:30 LBDg/L0.17 3/9/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/10/20 5:30 LBDg/L0.11 3/9/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/10/20 5:30 LBDg/L0.15 3/9/20SM21-22 6200B1Chlorobenzene
ND 50 3/10/20 5:30 LBDg/L11 3/9/20SM21-22 6200B1Ethanol
ND 0.50 3/10/20 5:30 LBDg/L0.21 3/9/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/10/20 5:30 LBDg/L0.35 3/9/20SM21-22 6200B1Chloroethane
0.28 0.50 3/10/20 5:30 LBDg/L0.17 3/9/20SM21-22 6200B1JChloroform
ND 1.0 3/10/20 5:30 LBDg/L0.45 3/9/20SM21-22 6200B1Chloromethane
ND 0.50 3/10/20 5:30 LBDg/L0.12 3/9/20SM21-22 6200B12-Chlorotoluene
ND 0.50 3/10/20 5:30 LBDg/L0.14 3/9/20SM21-22 6200B14-Chlorotoluene
ND 0.50 3/10/20 5:30 LBDg/L0.19 3/9/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/10/20 5:30 LBDg/L0.16 3/9/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/10/20 5:30 LBDg/L0.12 3/9/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/10/20 5:30 LBDg/L0.13 3/9/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/10/20 5:30 LBDg/L0.26 3/9/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/10/20 5:30 LBDg/L0.16 3/9/20SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/10/20 5:30 LBDg/L0.41 3/9/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 3/10/20 5:30 LBDg/L0.32 3/9/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/10/20 5:30 LBDg/L0.13 3/9/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/10/20 5:30 LBDg/L0.31 3/9/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/10/20 5:30 LBDg/L0.20 3/9/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 3/10/20 5:30 LBDg/L0.11 3/9/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/10/20 5:30 LBDg/L0.20 3/9/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 3/10/20 5:30 LBDg/L0.16 3/9/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/10/20 5:30 LBDg/L0.13 3/9/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/10/20 5:30 LBDg/L0.23 3/9/20SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/10/20 5:30 LBDg/L0.17 3/9/20SM21-22 6200B1Diisopropyl Ether (DIPE)
15 0.50 3/10/20 5:30 LBDg/L0.13 3/9/20SM21-22 6200B1Ethylbenzene
ND 5.0 3/10/20 5:30 LBDg/L1.5 3/9/20SM21-22 6200B12-Hexanone (MBK)
2.4 0.50 3/10/20 5:30 LBDg/L0.17 3/9/20SM21-22 6200B1Isopropylbenzene (Cumene)
0.32 0.50 3/10/20 5:30 LBDg/L0.20 3/9/20SM21-22 6200B1Jp-Isopropyltoluene (p-Cymene)
ND 0.50 3/10/20 5:30 LBDg/L0.25 3/9/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/10/20 5:30 LBDg/L0.34 3/9/20SM21-22 6200B1Methylene Chloride
ND 5.0 3/10/20 5:30 LBDg/L1.7 3/9/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 7 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-02
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 3/5/2020 12:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
5.6 0.50 3/10/20 5:30 LBDg/L0.31 3/9/20SM21-22 6200B1Naphthalene
4.4 0.50 3/10/20 5:30 LBDg/L0.13 3/9/20SM21-22 6200B1n-Propylbenzene
ND 0.50 3/10/20 5:30 LBDg/L0.11 3/9/20SM21-22 6200B1Styrene
ND 0.50 3/10/20 5:30 LBDg/L0.22 3/9/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/10/20 5:30 LBDg/L0.18 3/9/20SM21-22 6200B1Tetrachloroethylene
10 0.50 3/10/20 5:30 LBDg/L0.14 3/9/20SM21-22 6200B1Toluene
ND 1.0 3/10/20 5:30 LBDg/L0.57 3/9/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/10/20 5:30 LBDg/L0.40 3/9/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/10/20 5:30 LBDg/L0.20 3/9/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/10/20 5:30 LBDg/L0.16 3/9/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 3/10/20 5:30 LBDg/L0.24 3/9/20SM21-22 6200B1Trichloroethylene
ND 0.50 3/10/20 5:30 LBDg/L0.33 3/9/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/10/20 5:30 LBDg/L0.25 3/9/20SM21-22 6200B11,2,3-Trichloropropane
16 0.50 3/10/20 5:30 LBDg/L0.18 3/9/20SM21-22 6200B11,2,4-Trimethylbenzene
8.7 0.50 3/10/20 5:30 LBDg/L0.14 3/9/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 3/10/20 5:30 LBDg/L10 3/9/20SM21-22 6200B1Vinyl Acetate
ND 0.50 3/10/20 5:30 LBDg/L0.45 3/9/20SM21-22 6200B1Vinyl Chloride
22 1.0 3/10/20 5:30 LBDg/L0.30 3/9/20SM21-22 6200B1m+p Xylene
7.8 0.50 3/10/20 5:30 LBDg/L0.17 3/9/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 90.7 3/10/20 5:3070-130
Toluene-d8 99.0 3/10/20 5:3070-130
4-Bromofluorobenzene 98.4 3/10/20 5:3070-130
Page 8 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-03
Field Sample #: MW-4
Sample Matrix: Ground Water
Sampled: 3/5/2020 13:15
[TOC_2]20C0345-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 100 3/10/20 19:49 EEHg/L7.6 3/10/20SM21-22 6200B2Acetone
47 1.0 3/10/20 19:49 EEHg/L0.36 3/10/20SM21-22 6200B2Benzene
ND 1.0 3/10/20 19:49 EEHg/L0.30 3/10/20SM21-22 6200B2Bromobenzene
ND 1.0 3/10/20 19:49 EEHg/L0.64 3/10/20SM21-22 6200B2Bromochloromethane
ND 1.0 3/10/20 19:49 EEHg/L0.32 3/10/20SM21-22 6200B2Bromodichloromethane
ND 1.0 3/10/20 19:49 EEHg/L0.92 3/10/20SM21-22 6200B2Bromoform
ND 4.0 3/10/20 19:49 EEHg/L1.6 3/10/20SM21-22 6200B2Bromomethane
ND 10 3/10/20 19:49 EEHg/L3.9 3/10/20SM21-22 6200B22-Butanone (MEK)
8.1 1.0 3/10/20 19:49 EEHg/L0.42 3/10/20SM21-22 6200B2n-Butylbenzene
1.9 1.0 3/10/20 19:49 EEHg/L0.32 3/10/20SM21-22 6200B2sec-Butylbenzene
0.80 1.0 3/10/20 19:49 EEHg/L0.34 3/10/20SM21-22 6200B2Jtert-Butylbenzene
ND 1.0 3/10/20 19:49 EEHg/L0.22 3/10/20SM21-22 6200B2Carbon Tetrachloride
ND 1.0 3/10/20 19:49 EEHg/L0.30 3/10/20SM21-22 6200B2Chlorobenzene
ND 100 3/10/20 19:49 EEHg/L21 3/10/20SM21-22 6200B2Ethanol
ND 1.0 3/10/20 19:49 EEHg/L0.42 3/10/20SM21-22 6200B2Chlorodibromomethane
ND 1.0 3/10/20 19:49 EEHg/L0.70 3/10/20SM21-22 6200B2Chloroethane
ND 1.0 3/10/20 19:49 EEHg/L0.34 3/10/20SM21-22 6200B2Chloroform
ND 2.0 3/10/20 19:49 EEHg/L0.90 3/10/20SM21-22 6200B2Chloromethane
ND 1.0 3/10/20 19:49 EEHg/L0.24 3/10/20SM21-22 6200B22-Chlorotoluene
ND 1.0 3/10/20 19:49 EEHg/L0.28 3/10/20SM21-22 6200B24-Chlorotoluene
ND 1.0 3/10/20 19:49 EEHg/L0.38 3/10/20SM21-22 6200B21,2-Dibromoethane (EDB)
ND 1.0 3/10/20 19:49 EEHg/L0.32 3/10/20SM21-22 6200B21,2-Dichlorobenzene
ND 1.0 3/10/20 19:49 EEHg/L0.24 3/10/20SM21-22 6200B21,3-Dichlorobenzene
ND 1.0 3/10/20 19:49 EEHg/L0.26 3/10/20SM21-22 6200B21,4-Dichlorobenzene
ND 1.0 3/10/20 19:49 EEHg/L0.52 3/10/20SM21-22 6200B2Dichlorodifluoromethane (Freon 12)
ND 1.0 3/10/20 19:49 EEHg/L0.32 3/10/20SM21-22 6200B21,1-Dichloroethane
ND 1.0 3/10/20 19:49 EEHg/L0.82 3/10/20SM21-22 6200B21,2-Dichloroethane
ND 1.0 3/10/20 19:49 EEHg/L0.64 3/10/20SM21-22 6200B21,1-Dichloroethylene
ND 1.0 3/10/20 19:49 EEHg/L0.26 3/10/20SM21-22 6200B2cis-1,2-Dichloroethylene
ND 1.0 3/10/20 19:49 EEHg/L0.62 3/10/20SM21-22 6200B2trans-1,2-Dichloroethylene
ND 1.0 3/10/20 19:49 EEHg/L0.40 3/10/20SM21-22 6200B21,2-Dichloropropane
ND 1.0 3/10/20 19:49 EEHg/L0.22 3/10/20SM21-22 6200B21,3-Dichloropropane
ND 1.0 3/10/20 19:49 EEHg/L0.40 3/10/20SM21-22 6200B22,2-Dichloropropane
ND 1.0 3/10/20 19:49 EEHg/L0.32 3/10/20SM21-22 6200B21,1-Dichloropropene
ND 1.0 3/10/20 19:49 EEHg/L0.26 3/10/20SM21-22 6200B2cis-1,3-Dichloropropene
ND 1.0 3/10/20 19:49 EEHg/L0.46 3/10/20SM21-22 6200B2trans-1,3-Dichloropropene
ND 1.0 3/10/20 19:49 EEHg/L0.34 3/10/20SM21-22 6200B2Diisopropyl Ether (DIPE)
18 1.0 3/10/20 19:49 EEHg/L0.26 3/10/20SM21-22 6200B2Ethylbenzene
ND 10 3/10/20 19:49 EEHg/L3.0 3/10/20SM21-22 6200B22-Hexanone (MBK)
4.5 1.0 3/10/20 19:49 EEHg/L0.34 3/10/20SM21-22 6200B2Isopropylbenzene (Cumene)
5.4 1.0 3/10/20 19:49 EEHg/L0.40 3/10/20SM21-22 6200B2p-Isopropyltoluene (p-Cymene)
ND 1.0 3/10/20 19:49 EEHg/L0.50 3/10/20SM21-22 6200B2Methyl tert-Butyl Ether (MTBE)
ND 10 3/10/20 19:49 EEHg/L0.68 3/10/20SM21-22 6200B2Methylene Chloride
ND 10 3/10/20 19:49 EEHg/L3.3 3/10/20SM21-22 6200B24-Methyl-2-pentanone (MIBK)
Page 9 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-03
Field Sample #: MW-4
Sample Matrix: Ground Water
Sampled: 3/5/2020 13:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
4.4 1.0 3/10/20 19:49 EEHg/L0.62 3/10/20SM21-22 6200B2Naphthalene
3.4 1.0 3/10/20 19:49 EEHg/L0.26 3/10/20SM21-22 6200B2n-Propylbenzene
ND 1.0 3/10/20 19:49 EEHg/L0.22 3/10/20SM21-22 6200B2Styrene
ND 1.0 3/10/20 19:49 EEHg/L0.44 3/10/20SM21-22 6200B21,1,2,2-Tetrachloroethane
ND 1.0 3/10/20 19:49 EEHg/L0.36 3/10/20SM21-22 6200B2Tetrachloroethylene
33 1.0 3/10/20 19:49 EEHg/L0.28 3/10/20SM21-22 6200B2Toluene
ND 2.0 3/10/20 19:49 EEHg/L1.1 3/10/20SM21-22 6200B2L-041,2,3-Trichlorobenzene
ND 1.0 3/10/20 19:49 EEHg/L0.80 3/10/20SM21-22 6200B21,2,4-Trichlorobenzene
ND 1.0 3/10/20 19:49 EEHg/L0.40 3/10/20SM21-22 6200B21,1,1-Trichloroethane
ND 1.0 3/10/20 19:49 EEHg/L0.32 3/10/20SM21-22 6200B21,1,2-Trichloroethane
ND 1.0 3/10/20 19:49 EEHg/L0.48 3/10/20SM21-22 6200B2Trichloroethylene
ND 1.0 3/10/20 19:49 EEHg/L0.66 3/10/20SM21-22 6200B2Trichlorofluoromethane (Freon 11)
ND 1.0 3/10/20 19:49 EEHg/L0.50 3/10/20SM21-22 6200B21,2,3-Trichloropropane
190 1.0 3/10/20 19:49 EEHg/L0.36 3/10/20SM21-22 6200B21,2,4-Trimethylbenzene
86 1.0 3/10/20 19:49 EEHg/L0.28 3/10/20SM21-22 6200B21,3,5-Trimethylbenzene
ND 40 3/10/20 19:49 EEHg/L20 3/10/20SM21-22 6200B2Vinyl Acetate
ND 1.0 3/10/20 19:49 EEHg/L0.90 3/10/20SM21-22 6200B2Vinyl Chloride
230 2.0 3/10/20 19:49 EEHg/L0.60 3/10/20SM21-22 6200B2m+p Xylene
140 1.0 3/10/20 19:49 EEHg/L0.34 3/10/20SM21-22 6200B2o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 92.7 3/10/20 19:4970-130
Toluene-d8 99.5 3/10/20 19:4970-130
4-Bromofluorobenzene 99.4 3/10/20 19:4970-130
Page 10 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-04
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 3/5/2020 13:55
[TOC_2]20C0345-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/10/20 5:56 LBDg/L3.8 3/9/20SM21-22 6200B1Acetone
ND 0.50 3/10/20 5:56 LBDg/L0.18 3/9/20SM21-22 6200B1Benzene
ND 0.50 3/10/20 5:56 LBDg/L0.15 3/9/20SM21-22 6200B1Bromobenzene
ND 0.50 3/10/20 5:56 LBDg/L0.32 3/9/20SM21-22 6200B1Bromochloromethane
ND 0.50 3/10/20 5:56 LBDg/L0.16 3/9/20SM21-22 6200B1Bromodichloromethane
ND 0.50 3/10/20 5:56 LBDg/L0.46 3/9/20SM21-22 6200B1Bromoform
ND 2.0 3/10/20 5:56 LBDg/L0.78 3/9/20SM21-22 6200B1Bromomethane
ND 5.0 3/10/20 5:56 LBDg/L1.9 3/9/20SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/10/20 5:56 LBDg/L0.21 3/9/20SM21-22 6200B1n-Butylbenzene
ND 0.50 3/10/20 5:56 LBDg/L0.16 3/9/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/10/20 5:56 LBDg/L0.17 3/9/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/10/20 5:56 LBDg/L0.11 3/9/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/10/20 5:56 LBDg/L0.15 3/9/20SM21-22 6200B1Chlorobenzene
ND 50 3/10/20 5:56 LBDg/L11 3/9/20SM21-22 6200B1Ethanol
ND 0.50 3/10/20 5:56 LBDg/L0.21 3/9/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/10/20 5:56 LBDg/L0.35 3/9/20SM21-22 6200B1Chloroethane
ND 0.50 3/10/20 5:56 LBDg/L0.17 3/9/20SM21-22 6200B1Chloroform
ND 1.0 3/10/20 5:56 LBDg/L0.45 3/9/20SM21-22 6200B1Chloromethane
ND 0.50 3/10/20 5:56 LBDg/L0.12 3/9/20SM21-22 6200B12-Chlorotoluene
ND 0.50 3/10/20 5:56 LBDg/L0.14 3/9/20SM21-22 6200B14-Chlorotoluene
ND 0.50 3/10/20 5:56 LBDg/L0.19 3/9/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/10/20 5:56 LBDg/L0.16 3/9/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/10/20 5:56 LBDg/L0.12 3/9/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/10/20 5:56 LBDg/L0.13 3/9/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/10/20 5:56 LBDg/L0.26 3/9/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/10/20 5:56 LBDg/L0.16 3/9/20SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/10/20 5:56 LBDg/L0.41 3/9/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 3/10/20 5:56 LBDg/L0.32 3/9/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/10/20 5:56 LBDg/L0.13 3/9/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/10/20 5:56 LBDg/L0.31 3/9/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/10/20 5:56 LBDg/L0.20 3/9/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 3/10/20 5:56 LBDg/L0.11 3/9/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/10/20 5:56 LBDg/L0.20 3/9/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 3/10/20 5:56 LBDg/L0.16 3/9/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/10/20 5:56 LBDg/L0.13 3/9/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/10/20 5:56 LBDg/L0.23 3/9/20SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/10/20 5:56 LBDg/L0.17 3/9/20SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/10/20 5:56 LBDg/L0.13 3/9/20SM21-22 6200B1Ethylbenzene
ND 5.0 3/10/20 5:56 LBDg/L1.5 3/9/20SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/10/20 5:56 LBDg/L0.17 3/9/20SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/10/20 5:56 LBDg/L0.20 3/9/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/10/20 5:56 LBDg/L0.25 3/9/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/10/20 5:56 LBDg/L0.34 3/9/20SM21-22 6200B1Methylene Chloride
ND 5.0 3/10/20 5:56 LBDg/L1.7 3/9/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 11 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-04
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 3/5/2020 13:55
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
0.39 0.50 3/10/20 5:56 LBDg/L0.31 3/9/20SM21-22 6200B1JNaphthalene
ND 0.50 3/10/20 5:56 LBDg/L0.13 3/9/20SM21-22 6200B1n-Propylbenzene
ND 0.50 3/10/20 5:56 LBDg/L0.11 3/9/20SM21-22 6200B1Styrene
ND 0.50 3/10/20 5:56 LBDg/L0.22 3/9/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/10/20 5:56 LBDg/L0.18 3/9/20SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/10/20 5:56 LBDg/L0.14 3/9/20SM21-22 6200B1Toluene
ND 1.0 3/10/20 5:56 LBDg/L0.57 3/9/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/10/20 5:56 LBDg/L0.40 3/9/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/10/20 5:56 LBDg/L0.20 3/9/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/10/20 5:56 LBDg/L0.16 3/9/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 3/10/20 5:56 LBDg/L0.24 3/9/20SM21-22 6200B1Trichloroethylene
ND 0.50 3/10/20 5:56 LBDg/L0.33 3/9/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/10/20 5:56 LBDg/L0.25 3/9/20SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/10/20 5:56 LBDg/L0.18 3/9/20SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/10/20 5:56 LBDg/L0.14 3/9/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 3/10/20 5:56 LBDg/L10 3/9/20SM21-22 6200B1Vinyl Acetate
ND 0.50 3/10/20 5:56 LBDg/L0.45 3/9/20SM21-22 6200B1Vinyl Chloride
ND 1.0 3/10/20 5:56 LBDg/L0.30 3/9/20SM21-22 6200B1m+p Xylene
ND 0.50 3/10/20 5:56 LBDg/L0.17 3/9/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.1 3/10/20 5:5670-130
Toluene-d8 99.7 3/10/20 5:5670-130
4-Bromofluorobenzene 99.9 3/10/20 5:5670-130
Page 12 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-05
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 3/5/2020 14:20
[TOC_2]20C0345-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/10/20 6:22 LBDg/L3.8 3/9/20SM21-22 6200B1Acetone
ND 0.50 3/10/20 6:22 LBDg/L0.18 3/9/20SM21-22 6200B1Benzene
ND 0.50 3/10/20 6:22 LBDg/L0.15 3/9/20SM21-22 6200B1Bromobenzene
ND 0.50 3/10/20 6:22 LBDg/L0.32 3/9/20SM21-22 6200B1Bromochloromethane
ND 0.50 3/10/20 6:22 LBDg/L0.16 3/9/20SM21-22 6200B1Bromodichloromethane
ND 0.50 3/10/20 6:22 LBDg/L0.46 3/9/20SM21-22 6200B1Bromoform
ND 2.0 3/10/20 6:22 LBDg/L0.78 3/9/20SM21-22 6200B1Bromomethane
ND 5.0 3/10/20 6:22 LBDg/L1.9 3/9/20SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/10/20 6:22 LBDg/L0.21 3/9/20SM21-22 6200B1n-Butylbenzene
ND 0.50 3/10/20 6:22 LBDg/L0.16 3/9/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/10/20 6:22 LBDg/L0.17 3/9/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/10/20 6:22 LBDg/L0.11 3/9/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/10/20 6:22 LBDg/L0.15 3/9/20SM21-22 6200B1Chlorobenzene
ND 50 3/10/20 6:22 LBDg/L11 3/9/20SM21-22 6200B1Ethanol
ND 0.50 3/10/20 6:22 LBDg/L0.21 3/9/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/10/20 6:22 LBDg/L0.35 3/9/20SM21-22 6200B1Chloroethane
ND 0.50 3/10/20 6:22 LBDg/L0.17 3/9/20SM21-22 6200B1Chloroform
ND 1.0 3/10/20 6:22 LBDg/L0.45 3/9/20SM21-22 6200B1Chloromethane
ND 0.50 3/10/20 6:22 LBDg/L0.12 3/9/20SM21-22 6200B12-Chlorotoluene
ND 0.50 3/10/20 6:22 LBDg/L0.14 3/9/20SM21-22 6200B14-Chlorotoluene
ND 0.50 3/10/20 6:22 LBDg/L0.19 3/9/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/10/20 6:22 LBDg/L0.16 3/9/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/10/20 6:22 LBDg/L0.12 3/9/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/10/20 6:22 LBDg/L0.13 3/9/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/10/20 6:22 LBDg/L0.26 3/9/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/10/20 6:22 LBDg/L0.16 3/9/20SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/10/20 6:22 LBDg/L0.41 3/9/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 3/10/20 6:22 LBDg/L0.32 3/9/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/10/20 6:22 LBDg/L0.13 3/9/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/10/20 6:22 LBDg/L0.31 3/9/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/10/20 6:22 LBDg/L0.20 3/9/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 3/10/20 6:22 LBDg/L0.11 3/9/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/10/20 6:22 LBDg/L0.20 3/9/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 3/10/20 6:22 LBDg/L0.16 3/9/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/10/20 6:22 LBDg/L0.13 3/9/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/10/20 6:22 LBDg/L0.23 3/9/20SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/10/20 6:22 LBDg/L0.17 3/9/20SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/10/20 6:22 LBDg/L0.13 3/9/20SM21-22 6200B1Ethylbenzene
ND 5.0 3/10/20 6:22 LBDg/L1.5 3/9/20SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/10/20 6:22 LBDg/L0.17 3/9/20SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/10/20 6:22 LBDg/L0.20 3/9/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/10/20 6:22 LBDg/L0.25 3/9/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/10/20 6:22 LBDg/L0.34 3/9/20SM21-22 6200B1Methylene Chloride
ND 5.0 3/10/20 6:22 LBDg/L1.7 3/9/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 13 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-05
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 3/5/2020 14:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/10/20 6:22 LBDg/L0.31 3/9/20SM21-22 6200B1Naphthalene
ND 0.50 3/10/20 6:22 LBDg/L0.13 3/9/20SM21-22 6200B1n-Propylbenzene
ND 0.50 3/10/20 6:22 LBDg/L0.11 3/9/20SM21-22 6200B1Styrene
ND 0.50 3/10/20 6:22 LBDg/L0.22 3/9/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/10/20 6:22 LBDg/L0.18 3/9/20SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/10/20 6:22 LBDg/L0.14 3/9/20SM21-22 6200B1Toluene
ND 1.0 3/10/20 6:22 LBDg/L0.57 3/9/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/10/20 6:22 LBDg/L0.40 3/9/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/10/20 6:22 LBDg/L0.20 3/9/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/10/20 6:22 LBDg/L0.16 3/9/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 3/10/20 6:22 LBDg/L0.24 3/9/20SM21-22 6200B1Trichloroethylene
ND 0.50 3/10/20 6:22 LBDg/L0.33 3/9/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/10/20 6:22 LBDg/L0.25 3/9/20SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/10/20 6:22 LBDg/L0.18 3/9/20SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/10/20 6:22 LBDg/L0.14 3/9/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 3/10/20 6:22 LBDg/L10 3/9/20SM21-22 6200B1Vinyl Acetate
ND 0.50 3/10/20 6:22 LBDg/L0.45 3/9/20SM21-22 6200B1Vinyl Chloride
ND 1.0 3/10/20 6:22 LBDg/L0.30 3/9/20SM21-22 6200B1m+p Xylene
ND 0.50 3/10/20 6:22 LBDg/L0.17 3/9/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.3 3/10/20 6:2270-130
Toluene-d8 99.1 3/10/20 6:2270-130
4-Bromofluorobenzene 94.8 3/10/20 6:2270-130
Page 14 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-06
Field Sample #: MW-7
Sample Matrix: Ground Water
Sampled: 3/5/2020 14:45
[TOC_2]20C0345-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/10/20 6:49 LBDg/L3.8 3/9/20SM21-22 6200B1Acetone
ND 0.50 3/10/20 6:49 LBDg/L0.18 3/9/20SM21-22 6200B1Benzene
ND 0.50 3/10/20 6:49 LBDg/L0.15 3/9/20SM21-22 6200B1Bromobenzene
ND 0.50 3/10/20 6:49 LBDg/L0.32 3/9/20SM21-22 6200B1Bromochloromethane
ND 0.50 3/10/20 6:49 LBDg/L0.16 3/9/20SM21-22 6200B1Bromodichloromethane
ND 0.50 3/10/20 6:49 LBDg/L0.46 3/9/20SM21-22 6200B1Bromoform
ND 2.0 3/10/20 6:49 LBDg/L0.78 3/9/20SM21-22 6200B1Bromomethane
ND 5.0 3/10/20 6:49 LBDg/L1.9 3/9/20SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/10/20 6:49 LBDg/L0.21 3/9/20SM21-22 6200B1n-Butylbenzene
ND 0.50 3/10/20 6:49 LBDg/L0.16 3/9/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/10/20 6:49 LBDg/L0.17 3/9/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/10/20 6:49 LBDg/L0.11 3/9/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/10/20 6:49 LBDg/L0.15 3/9/20SM21-22 6200B1Chlorobenzene
ND 50 3/10/20 6:49 LBDg/L11 3/9/20SM21-22 6200B1Ethanol
ND 0.50 3/10/20 6:49 LBDg/L0.21 3/9/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/10/20 6:49 LBDg/L0.35 3/9/20SM21-22 6200B1Chloroethane
ND 0.50 3/10/20 6:49 LBDg/L0.17 3/9/20SM21-22 6200B1Chloroform
ND 1.0 3/10/20 6:49 LBDg/L0.45 3/9/20SM21-22 6200B1Chloromethane
ND 0.50 3/10/20 6:49 LBDg/L0.12 3/9/20SM21-22 6200B12-Chlorotoluene
ND 0.50 3/10/20 6:49 LBDg/L0.14 3/9/20SM21-22 6200B14-Chlorotoluene
ND 0.50 3/10/20 6:49 LBDg/L0.19 3/9/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/10/20 6:49 LBDg/L0.16 3/9/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/10/20 6:49 LBDg/L0.12 3/9/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/10/20 6:49 LBDg/L0.13 3/9/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/10/20 6:49 LBDg/L0.26 3/9/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/10/20 6:49 LBDg/L0.16 3/9/20SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/10/20 6:49 LBDg/L0.41 3/9/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 3/10/20 6:49 LBDg/L0.32 3/9/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/10/20 6:49 LBDg/L0.13 3/9/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/10/20 6:49 LBDg/L0.31 3/9/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/10/20 6:49 LBDg/L0.20 3/9/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 3/10/20 6:49 LBDg/L0.11 3/9/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/10/20 6:49 LBDg/L0.20 3/9/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 3/10/20 6:49 LBDg/L0.16 3/9/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/10/20 6:49 LBDg/L0.13 3/9/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/10/20 6:49 LBDg/L0.23 3/9/20SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/10/20 6:49 LBDg/L0.17 3/9/20SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/10/20 6:49 LBDg/L0.13 3/9/20SM21-22 6200B1Ethylbenzene
ND 5.0 3/10/20 6:49 LBDg/L1.5 3/9/20SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/10/20 6:49 LBDg/L0.17 3/9/20SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/10/20 6:49 LBDg/L0.20 3/9/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/10/20 6:49 LBDg/L0.25 3/9/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/10/20 6:49 LBDg/L0.34 3/9/20SM21-22 6200B1Methylene Chloride
ND 5.0 3/10/20 6:49 LBDg/L1.7 3/9/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 15 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-06
Field Sample #: MW-7
Sample Matrix: Ground Water
Sampled: 3/5/2020 14:45
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/10/20 6:49 LBDg/L0.31 3/9/20SM21-22 6200B1Naphthalene
ND 0.50 3/10/20 6:49 LBDg/L0.13 3/9/20SM21-22 6200B1n-Propylbenzene
ND 0.50 3/10/20 6:49 LBDg/L0.11 3/9/20SM21-22 6200B1Styrene
ND 0.50 3/10/20 6:49 LBDg/L0.22 3/9/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/10/20 6:49 LBDg/L0.18 3/9/20SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/10/20 6:49 LBDg/L0.14 3/9/20SM21-22 6200B1Toluene
ND 1.0 3/10/20 6:49 LBDg/L0.57 3/9/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/10/20 6:49 LBDg/L0.40 3/9/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/10/20 6:49 LBDg/L0.20 3/9/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/10/20 6:49 LBDg/L0.16 3/9/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 3/10/20 6:49 LBDg/L0.24 3/9/20SM21-22 6200B1Trichloroethylene
ND 0.50 3/10/20 6:49 LBDg/L0.33 3/9/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/10/20 6:49 LBDg/L0.25 3/9/20SM21-22 6200B11,2,3-Trichloropropane
0.20 0.50 3/10/20 6:49 LBDg/L0.18 3/9/20SM21-22 6200B1J1,2,4-Trimethylbenzene
ND 0.50 3/10/20 6:49 LBDg/L0.14 3/9/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 3/10/20 6:49 LBDg/L10 3/9/20SM21-22 6200B1Vinyl Acetate
ND 0.50 3/10/20 6:49 LBDg/L0.45 3/9/20SM21-22 6200B1Vinyl Chloride
ND 1.0 3/10/20 6:49 LBDg/L0.30 3/9/20SM21-22 6200B1m+p Xylene
ND 0.50 3/10/20 6:49 LBDg/L0.17 3/9/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 90.4 3/10/20 6:4970-130
Toluene-d8 97.8 3/10/20 6:4970-130
4-Bromofluorobenzene 92.6 3/10/20 6:4970-130
Page 16 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-07
Field Sample #: MW-8
Sample Matrix: Ground Water
Sampled: 3/5/2020 15:20
[TOC_2]20C0345-07[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/10/20 7:15 LBDg/L3.8 3/9/20SM21-22 6200B1Acetone
ND 0.50 3/10/20 7:15 LBDg/L0.18 3/9/20SM21-22 6200B1Benzene
ND 0.50 3/10/20 7:15 LBDg/L0.15 3/9/20SM21-22 6200B1Bromobenzene
ND 0.50 3/10/20 7:15 LBDg/L0.32 3/9/20SM21-22 6200B1Bromochloromethane
ND 0.50 3/10/20 7:15 LBDg/L0.16 3/9/20SM21-22 6200B1Bromodichloromethane
ND 0.50 3/10/20 7:15 LBDg/L0.46 3/9/20SM21-22 6200B1Bromoform
ND 2.0 3/10/20 7:15 LBDg/L0.78 3/9/20SM21-22 6200B1Bromomethane
ND 5.0 3/10/20 7:15 LBDg/L1.9 3/9/20SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/10/20 7:15 LBDg/L0.21 3/9/20SM21-22 6200B1n-Butylbenzene
ND 0.50 3/10/20 7:15 LBDg/L0.16 3/9/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/10/20 7:15 LBDg/L0.17 3/9/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/10/20 7:15 LBDg/L0.11 3/9/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/10/20 7:15 LBDg/L0.15 3/9/20SM21-22 6200B1Chlorobenzene
ND 50 3/10/20 7:15 LBDg/L11 3/9/20SM21-22 6200B1Ethanol
ND 0.50 3/10/20 7:15 LBDg/L0.21 3/9/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/10/20 7:15 LBDg/L0.35 3/9/20SM21-22 6200B1Chloroethane
ND 0.50 3/10/20 7:15 LBDg/L0.17 3/9/20SM21-22 6200B1Chloroform
0.55 1.0 3/10/20 7:15 LBDg/L0.45 3/9/20SM21-22 6200B1JChloromethane
ND 0.50 3/10/20 7:15 LBDg/L0.12 3/9/20SM21-22 6200B12-Chlorotoluene
ND 0.50 3/10/20 7:15 LBDg/L0.14 3/9/20SM21-22 6200B14-Chlorotoluene
ND 0.50 3/10/20 7:15 LBDg/L0.19 3/9/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/10/20 7:15 LBDg/L0.16 3/9/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/10/20 7:15 LBDg/L0.12 3/9/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/10/20 7:15 LBDg/L0.13 3/9/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/10/20 7:15 LBDg/L0.26 3/9/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/10/20 7:15 LBDg/L0.16 3/9/20SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/10/20 7:15 LBDg/L0.41 3/9/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 3/10/20 7:15 LBDg/L0.32 3/9/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/10/20 7:15 LBDg/L0.13 3/9/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/10/20 7:15 LBDg/L0.31 3/9/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/10/20 7:15 LBDg/L0.20 3/9/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 3/10/20 7:15 LBDg/L0.11 3/9/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/10/20 7:15 LBDg/L0.20 3/9/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 3/10/20 7:15 LBDg/L0.16 3/9/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/10/20 7:15 LBDg/L0.13 3/9/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/10/20 7:15 LBDg/L0.23 3/9/20SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/10/20 7:15 LBDg/L0.17 3/9/20SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/10/20 7:15 LBDg/L0.13 3/9/20SM21-22 6200B1Ethylbenzene
ND 5.0 3/10/20 7:15 LBDg/L1.5 3/9/20SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/10/20 7:15 LBDg/L0.17 3/9/20SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/10/20 7:15 LBDg/L0.20 3/9/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/10/20 7:15 LBDg/L0.25 3/9/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/10/20 7:15 LBDg/L0.34 3/9/20SM21-22 6200B1Methylene Chloride
ND 5.0 3/10/20 7:15 LBDg/L1.7 3/9/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 17 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-07
Field Sample #: MW-8
Sample Matrix: Ground Water
Sampled: 3/5/2020 15:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/10/20 7:15 LBDg/L0.31 3/9/20SM21-22 6200B1Naphthalene
ND 0.50 3/10/20 7:15 LBDg/L0.13 3/9/20SM21-22 6200B1n-Propylbenzene
ND 0.50 3/10/20 7:15 LBDg/L0.11 3/9/20SM21-22 6200B1Styrene
ND 0.50 3/10/20 7:15 LBDg/L0.22 3/9/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/10/20 7:15 LBDg/L0.18 3/9/20SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/10/20 7:15 LBDg/L0.14 3/9/20SM21-22 6200B1Toluene
ND 1.0 3/10/20 7:15 LBDg/L0.57 3/9/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/10/20 7:15 LBDg/L0.40 3/9/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/10/20 7:15 LBDg/L0.20 3/9/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/10/20 7:15 LBDg/L0.16 3/9/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 3/10/20 7:15 LBDg/L0.24 3/9/20SM21-22 6200B1Trichloroethylene
ND 0.50 3/10/20 7:15 LBDg/L0.33 3/9/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/10/20 7:15 LBDg/L0.25 3/9/20SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/10/20 7:15 LBDg/L0.18 3/9/20SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/10/20 7:15 LBDg/L0.14 3/9/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 3/10/20 7:15 LBDg/L10 3/9/20SM21-22 6200B1Vinyl Acetate
ND 0.50 3/10/20 7:15 LBDg/L0.45 3/9/20SM21-22 6200B1Vinyl Chloride
ND 1.0 3/10/20 7:15 LBDg/L0.30 3/9/20SM21-22 6200B1m+p Xylene
ND 0.50 3/10/20 7:15 LBDg/L0.17 3/9/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 90.1 3/10/20 7:1570-130
Toluene-d8 98.9 3/10/20 7:1570-130
4-Bromofluorobenzene 96.8 3/10/20 7:1570-130
Page 18 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-08
Field Sample #: MW-9
Sample Matrix: Ground Water
Sampled: 3/6/2020 10:20
[TOC_2]20C0345-08[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/10/20 7:42 LBDg/L3.8 3/9/20SM21-22 6200B1Acetone
19 0.50 3/10/20 7:42 LBDg/L0.18 3/9/20SM21-22 6200B1Benzene
ND 0.50 3/10/20 7:42 LBDg/L0.15 3/9/20SM21-22 6200B1Bromobenzene
ND 0.50 3/10/20 7:42 LBDg/L0.32 3/9/20SM21-22 6200B1Bromochloromethane
ND 0.50 3/10/20 7:42 LBDg/L0.16 3/9/20SM21-22 6200B1Bromodichloromethane
ND 0.50 3/10/20 7:42 LBDg/L0.46 3/9/20SM21-22 6200B1Bromoform
ND 2.0 3/10/20 7:42 LBDg/L0.78 3/9/20SM21-22 6200B1Bromomethane
ND 5.0 3/10/20 7:42 LBDg/L1.9 3/9/20SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/10/20 7:42 LBDg/L0.21 3/9/20SM21-22 6200B1n-Butylbenzene
ND 0.50 3/10/20 7:42 LBDg/L0.16 3/9/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/10/20 7:42 LBDg/L0.17 3/9/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/10/20 7:42 LBDg/L0.11 3/9/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/10/20 7:42 LBDg/L0.15 3/9/20SM21-22 6200B1Chlorobenzene
ND 50 3/10/20 7:42 LBDg/L11 3/9/20SM21-22 6200B1Ethanol
ND 0.50 3/10/20 7:42 LBDg/L0.21 3/9/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/10/20 7:42 LBDg/L0.35 3/9/20SM21-22 6200B1Chloroethane
0.24 0.50 3/10/20 7:42 LBDg/L0.17 3/9/20SM21-22 6200B1JChloroform
ND 1.0 3/10/20 7:42 LBDg/L0.45 3/9/20SM21-22 6200B1Chloromethane
ND 0.50 3/10/20 7:42 LBDg/L0.12 3/9/20SM21-22 6200B12-Chlorotoluene
ND 0.50 3/10/20 7:42 LBDg/L0.14 3/9/20SM21-22 6200B14-Chlorotoluene
ND 0.50 3/10/20 7:42 LBDg/L0.19 3/9/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/10/20 7:42 LBDg/L0.16 3/9/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/10/20 7:42 LBDg/L0.12 3/9/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/10/20 7:42 LBDg/L0.13 3/9/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/10/20 7:42 LBDg/L0.26 3/9/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/10/20 7:42 LBDg/L0.16 3/9/20SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/10/20 7:42 LBDg/L0.41 3/9/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 3/10/20 7:42 LBDg/L0.32 3/9/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/10/20 7:42 LBDg/L0.13 3/9/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/10/20 7:42 LBDg/L0.31 3/9/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/10/20 7:42 LBDg/L0.20 3/9/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 3/10/20 7:42 LBDg/L0.11 3/9/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/10/20 7:42 LBDg/L0.20 3/9/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 3/10/20 7:42 LBDg/L0.16 3/9/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/10/20 7:42 LBDg/L0.13 3/9/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/10/20 7:42 LBDg/L0.23 3/9/20SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/10/20 7:42 LBDg/L0.17 3/9/20SM21-22 6200B1Diisopropyl Ether (DIPE)
4.9 0.50 3/10/20 7:42 LBDg/L0.13 3/9/20SM21-22 6200B1Ethylbenzene
ND 5.0 3/10/20 7:42 LBDg/L1.5 3/9/20SM21-22 6200B12-Hexanone (MBK)
0.56 0.50 3/10/20 7:42 LBDg/L0.17 3/9/20SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/10/20 7:42 LBDg/L0.20 3/9/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
0.78 0.50 3/10/20 7:42 LBDg/L0.25 3/9/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/10/20 7:42 LBDg/L0.34 3/9/20SM21-22 6200B1Methylene Chloride
ND 5.0 3/10/20 7:42 LBDg/L1.7 3/9/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 19 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-08
Field Sample #: MW-9
Sample Matrix: Ground Water
Sampled: 3/6/2020 10:20
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
1.2 0.50 3/10/20 7:42 LBDg/L0.31 3/9/20SM21-22 6200B1Naphthalene
0.70 0.50 3/10/20 7:42 LBDg/L0.13 3/9/20SM21-22 6200B1n-Propylbenzene
ND 0.50 3/10/20 7:42 LBDg/L0.11 3/9/20SM21-22 6200B1Styrene
ND 0.50 3/10/20 7:42 LBDg/L0.22 3/9/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/10/20 7:42 LBDg/L0.18 3/9/20SM21-22 6200B1Tetrachloroethylene
0.94 0.50 3/10/20 7:42 LBDg/L0.14 3/9/20SM21-22 6200B1Toluene
ND 1.0 3/10/20 7:42 LBDg/L0.57 3/9/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/10/20 7:42 LBDg/L0.40 3/9/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/10/20 7:42 LBDg/L0.20 3/9/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/10/20 7:42 LBDg/L0.16 3/9/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 3/10/20 7:42 LBDg/L0.24 3/9/20SM21-22 6200B1Trichloroethylene
ND 0.50 3/10/20 7:42 LBDg/L0.33 3/9/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/10/20 7:42 LBDg/L0.25 3/9/20SM21-22 6200B11,2,3-Trichloropropane
0.78 0.50 3/10/20 7:42 LBDg/L0.18 3/9/20SM21-22 6200B11,2,4-Trimethylbenzene
0.89 0.50 3/10/20 7:42 LBDg/L0.14 3/9/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 3/10/20 7:42 LBDg/L10 3/9/20SM21-22 6200B1Vinyl Acetate
ND 0.50 3/10/20 7:42 LBDg/L0.45 3/9/20SM21-22 6200B1Vinyl Chloride
1.6 1.0 3/10/20 7:42 LBDg/L0.30 3/9/20SM21-22 6200B1m+p Xylene
0.45 0.50 3/10/20 7:42 LBDg/L0.17 3/9/20SM21-22 6200B1Jo-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 91.4 3/10/20 7:4270-130
Toluene-d8 100 3/10/20 7:4270-130
4-Bromofluorobenzene 94.5 3/10/20 7:4270-130
Page 20 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-09
Field Sample #: MW-10
Sample Matrix: Ground Water
Sampled: 3/6/2020 10:50
[TOC_2]20C0345-09[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/10/20 8:08 LBDg/L3.8 3/9/20SM21-22 6200B1Acetone
ND 0.50 3/10/20 8:08 LBDg/L0.18 3/9/20SM21-22 6200B1Benzene
ND 0.50 3/10/20 8:08 LBDg/L0.15 3/9/20SM21-22 6200B1Bromobenzene
ND 0.50 3/10/20 8:08 LBDg/L0.32 3/9/20SM21-22 6200B1Bromochloromethane
ND 0.50 3/10/20 8:08 LBDg/L0.16 3/9/20SM21-22 6200B1Bromodichloromethane
ND 0.50 3/10/20 8:08 LBDg/L0.46 3/9/20SM21-22 6200B1Bromoform
ND 2.0 3/10/20 8:08 LBDg/L0.78 3/9/20SM21-22 6200B1Bromomethane
ND 5.0 3/10/20 8:08 LBDg/L1.9 3/9/20SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/10/20 8:08 LBDg/L0.21 3/9/20SM21-22 6200B1n-Butylbenzene
ND 0.50 3/10/20 8:08 LBDg/L0.16 3/9/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/10/20 8:08 LBDg/L0.17 3/9/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/10/20 8:08 LBDg/L0.11 3/9/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/10/20 8:08 LBDg/L0.15 3/9/20SM21-22 6200B1Chlorobenzene
ND 50 3/10/20 8:08 LBDg/L11 3/9/20SM21-22 6200B1Ethanol
ND 0.50 3/10/20 8:08 LBDg/L0.21 3/9/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/10/20 8:08 LBDg/L0.35 3/9/20SM21-22 6200B1Chloroethane
ND 0.50 3/10/20 8:08 LBDg/L0.17 3/9/20SM21-22 6200B1Chloroform
ND 1.0 3/10/20 8:08 LBDg/L0.45 3/9/20SM21-22 6200B1Chloromethane
ND 0.50 3/10/20 8:08 LBDg/L0.12 3/9/20SM21-22 6200B12-Chlorotoluene
ND 0.50 3/10/20 8:08 LBDg/L0.14 3/9/20SM21-22 6200B14-Chlorotoluene
ND 0.50 3/10/20 8:08 LBDg/L0.19 3/9/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/10/20 8:08 LBDg/L0.16 3/9/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/10/20 8:08 LBDg/L0.12 3/9/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/10/20 8:08 LBDg/L0.13 3/9/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/10/20 8:08 LBDg/L0.26 3/9/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/10/20 8:08 LBDg/L0.16 3/9/20SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/10/20 8:08 LBDg/L0.41 3/9/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 3/10/20 8:08 LBDg/L0.32 3/9/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/10/20 8:08 LBDg/L0.13 3/9/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/10/20 8:08 LBDg/L0.31 3/9/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/10/20 8:08 LBDg/L0.20 3/9/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 3/10/20 8:08 LBDg/L0.11 3/9/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/10/20 8:08 LBDg/L0.20 3/9/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 3/10/20 8:08 LBDg/L0.16 3/9/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/10/20 8:08 LBDg/L0.13 3/9/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/10/20 8:08 LBDg/L0.23 3/9/20SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/10/20 8:08 LBDg/L0.17 3/9/20SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/10/20 8:08 LBDg/L0.13 3/9/20SM21-22 6200B1Ethylbenzene
ND 5.0 3/10/20 8:08 LBDg/L1.5 3/9/20SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/10/20 8:08 LBDg/L0.17 3/9/20SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/10/20 8:08 LBDg/L0.20 3/9/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/10/20 8:08 LBDg/L0.25 3/9/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/10/20 8:08 LBDg/L0.34 3/9/20SM21-22 6200B1Methylene Chloride
ND 5.0 3/10/20 8:08 LBDg/L1.7 3/9/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 21 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-09
Field Sample #: MW-10
Sample Matrix: Ground Water
Sampled: 3/6/2020 10:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/10/20 8:08 LBDg/L0.31 3/9/20SM21-22 6200B1Naphthalene
ND 0.50 3/10/20 8:08 LBDg/L0.13 3/9/20SM21-22 6200B1n-Propylbenzene
ND 0.50 3/10/20 8:08 LBDg/L0.11 3/9/20SM21-22 6200B1Styrene
ND 0.50 3/10/20 8:08 LBDg/L0.22 3/9/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/10/20 8:08 LBDg/L0.18 3/9/20SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/10/20 8:08 LBDg/L0.14 3/9/20SM21-22 6200B1Toluene
ND 1.0 3/10/20 8:08 LBDg/L0.57 3/9/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/10/20 8:08 LBDg/L0.40 3/9/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/10/20 8:08 LBDg/L0.20 3/9/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/10/20 8:08 LBDg/L0.16 3/9/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 3/10/20 8:08 LBDg/L0.24 3/9/20SM21-22 6200B1Trichloroethylene
ND 0.50 3/10/20 8:08 LBDg/L0.33 3/9/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/10/20 8:08 LBDg/L0.25 3/9/20SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/10/20 8:08 LBDg/L0.18 3/9/20SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/10/20 8:08 LBDg/L0.14 3/9/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 3/10/20 8:08 LBDg/L10 3/9/20SM21-22 6200B1Vinyl Acetate
ND 0.50 3/10/20 8:08 LBDg/L0.45 3/9/20SM21-22 6200B1Vinyl Chloride
ND 1.0 3/10/20 8:08 LBDg/L0.30 3/9/20SM21-22 6200B1m+p Xylene
ND 0.50 3/10/20 8:08 LBDg/L0.17 3/9/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.7 3/10/20 8:0870-130
Toluene-d8 97.8 3/10/20 8:0870-130
4-Bromofluorobenzene 97.4 3/10/20 8:0870-130
Page 22 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-10
Field Sample #: MW-11
Sample Matrix: Ground Water
Sampled: 3/6/2020 11:35
[TOC_2]20C0345-10[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
4.0 50 3/10/20 8:35 LBDg/L3.8 3/9/20SM21-22 6200B1JAcetone
55 0.50 3/10/20 8:35 LBDg/L0.18 3/9/20SM21-22 6200B1Benzene
ND 0.50 3/10/20 8:35 LBDg/L0.15 3/9/20SM21-22 6200B1Bromobenzene
ND 0.50 3/10/20 8:35 LBDg/L0.32 3/9/20SM21-22 6200B1Bromochloromethane
ND 0.50 3/10/20 8:35 LBDg/L0.16 3/9/20SM21-22 6200B1Bromodichloromethane
ND 0.50 3/10/20 8:35 LBDg/L0.46 3/9/20SM21-22 6200B1Bromoform
ND 2.0 3/10/20 8:35 LBDg/L0.78 3/9/20SM21-22 6200B1Bromomethane
ND 5.0 3/10/20 8:35 LBDg/L1.9 3/9/20SM21-22 6200B12-Butanone (MEK)
0.52 0.50 3/10/20 8:35 LBDg/L0.21 3/9/20SM21-22 6200B1n-Butylbenzene
0.37 0.50 3/10/20 8:35 LBDg/L0.16 3/9/20SM21-22 6200B1Jsec-Butylbenzene
ND 0.50 3/10/20 8:35 LBDg/L0.17 3/9/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/10/20 8:35 LBDg/L0.11 3/9/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/10/20 8:35 LBDg/L0.15 3/9/20SM21-22 6200B1Chlorobenzene
ND 50 3/10/20 8:35 LBDg/L11 3/9/20SM21-22 6200B1Ethanol
ND 0.50 3/10/20 8:35 LBDg/L0.21 3/9/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/10/20 8:35 LBDg/L0.35 3/9/20SM21-22 6200B1Chloroethane
1.5 0.50 3/10/20 8:35 LBDg/L0.17 3/9/20SM21-22 6200B1Chloroform
ND 1.0 3/10/20 8:35 LBDg/L0.45 3/9/20SM21-22 6200B1Chloromethane
ND 0.50 3/10/20 8:35 LBDg/L0.12 3/9/20SM21-22 6200B12-Chlorotoluene
ND 0.50 3/10/20 8:35 LBDg/L0.14 3/9/20SM21-22 6200B14-Chlorotoluene
ND 0.50 3/10/20 8:35 LBDg/L0.19 3/9/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/10/20 8:35 LBDg/L0.16 3/9/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/10/20 8:35 LBDg/L0.12 3/9/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/10/20 8:35 LBDg/L0.13 3/9/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/10/20 8:35 LBDg/L0.26 3/9/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/10/20 8:35 LBDg/L0.16 3/9/20SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/10/20 8:35 LBDg/L0.41 3/9/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 3/10/20 8:35 LBDg/L0.32 3/9/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/10/20 8:35 LBDg/L0.13 3/9/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/10/20 8:35 LBDg/L0.31 3/9/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/10/20 8:35 LBDg/L0.20 3/9/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 3/10/20 8:35 LBDg/L0.11 3/9/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/10/20 8:35 LBDg/L0.20 3/9/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 3/10/20 8:35 LBDg/L0.16 3/9/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/10/20 8:35 LBDg/L0.13 3/9/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/10/20 8:35 LBDg/L0.23 3/9/20SM21-22 6200B1trans-1,3-Dichloropropene
0.33 0.50 3/10/20 8:35 LBDg/L0.17 3/9/20SM21-22 6200B1JDiisopropyl Ether (DIPE)
ND 0.50 3/10/20 8:35 LBDg/L0.13 3/9/20SM21-22 6200B1Ethylbenzene
ND 5.0 3/10/20 8:35 LBDg/L1.5 3/9/20SM21-22 6200B12-Hexanone (MBK)
2.9 0.50 3/10/20 8:35 LBDg/L0.17 3/9/20SM21-22 6200B1Isopropylbenzene (Cumene)
0.20 0.50 3/10/20 8:35 LBDg/L0.20 3/9/20SM21-22 6200B1Jp-Isopropyltoluene (p-Cymene)
25 0.50 3/10/20 8:35 LBDg/L0.25 3/9/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/10/20 8:35 LBDg/L0.34 3/9/20SM21-22 6200B1Methylene Chloride
ND 5.0 3/10/20 8:35 LBDg/L1.7 3/9/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 23 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-10
Field Sample #: MW-11
Sample Matrix: Ground Water
Sampled: 3/6/2020 11:35
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
3.6 0.50 3/10/20 8:35 LBDg/L0.31 3/9/20SM21-22 6200B1Naphthalene
ND 0.50 3/10/20 8:35 LBDg/L0.13 3/9/20SM21-22 6200B1n-Propylbenzene
ND 0.50 3/10/20 8:35 LBDg/L0.11 3/9/20SM21-22 6200B1Styrene
ND 0.50 3/10/20 8:35 LBDg/L0.22 3/9/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/10/20 8:35 LBDg/L0.18 3/9/20SM21-22 6200B1Tetrachloroethylene
0.52 0.50 3/10/20 8:35 LBDg/L0.14 3/9/20SM21-22 6200B1Toluene
ND 1.0 3/10/20 8:35 LBDg/L0.57 3/9/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/10/20 8:35 LBDg/L0.40 3/9/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/10/20 8:35 LBDg/L0.20 3/9/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/10/20 8:35 LBDg/L0.16 3/9/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 3/10/20 8:35 LBDg/L0.24 3/9/20SM21-22 6200B1Trichloroethylene
ND 0.50 3/10/20 8:35 LBDg/L0.33 3/9/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/10/20 8:35 LBDg/L0.25 3/9/20SM21-22 6200B11,2,3-Trichloropropane
1.2 0.50 3/10/20 8:35 LBDg/L0.18 3/9/20SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/10/20 8:35 LBDg/L0.14 3/9/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 3/10/20 8:35 LBDg/L10 3/9/20SM21-22 6200B1Vinyl Acetate
ND 0.50 3/10/20 8:35 LBDg/L0.45 3/9/20SM21-22 6200B1Vinyl Chloride
3.4 1.0 3/10/20 8:35 LBDg/L0.30 3/9/20SM21-22 6200B1m+p Xylene
3.4 0.50 3/10/20 8:35 LBDg/L0.17 3/9/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 91.6 3/10/20 8:3570-130
Toluene-d8 98.6 3/10/20 8:3570-130
4-Bromofluorobenzene 95.5 3/10/20 8:3570-130
Page 24 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-11
Field Sample #: WSW-1
Sample Matrix: Water
Sampled: 3/6/2020 12:10
[TOC_2]20C0345-11[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 3/10/20 4:37 LBDg/L3.8 3/9/20SM21-22 6200B1Acetone
ND 0.50 3/10/20 4:37 LBDg/L0.18 3/9/20SM21-22 6200B1Benzene
ND 0.50 3/10/20 4:37 LBDg/L0.15 3/9/20SM21-22 6200B1Bromobenzene
ND 0.50 3/10/20 4:37 LBDg/L0.32 3/9/20SM21-22 6200B1Bromochloromethane
ND 0.50 3/10/20 4:37 LBDg/L0.16 3/9/20SM21-22 6200B1Bromodichloromethane
ND 0.50 3/10/20 4:37 LBDg/L0.46 3/9/20SM21-22 6200B1Bromoform
ND 2.0 3/10/20 4:37 LBDg/L0.78 3/9/20SM21-22 6200B1Bromomethane
ND 5.0 3/10/20 4:37 LBDg/L1.9 3/9/20SM21-22 6200B12-Butanone (MEK)
ND 0.50 3/10/20 4:37 LBDg/L0.21 3/9/20SM21-22 6200B1n-Butylbenzene
ND 0.50 3/10/20 4:37 LBDg/L0.16 3/9/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 3/10/20 4:37 LBDg/L0.17 3/9/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 3/10/20 4:37 LBDg/L0.11 3/9/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 3/10/20 4:37 LBDg/L0.15 3/9/20SM21-22 6200B1Chlorobenzene
ND 50 3/10/20 4:37 LBDg/L11 3/9/20SM21-22 6200B1Ethanol
ND 0.50 3/10/20 4:37 LBDg/L0.21 3/9/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 3/10/20 4:37 LBDg/L0.35 3/9/20SM21-22 6200B1Chloroethane
ND 0.50 3/10/20 4:37 LBDg/L0.17 3/9/20SM21-22 6200B1Chloroform
ND 1.0 3/10/20 4:37 LBDg/L0.45 3/9/20SM21-22 6200B1Chloromethane
ND 0.50 3/10/20 4:37 LBDg/L0.12 3/9/20SM21-22 6200B12-Chlorotoluene
ND 0.50 3/10/20 4:37 LBDg/L0.14 3/9/20SM21-22 6200B14-Chlorotoluene
ND 0.50 3/10/20 4:37 LBDg/L0.19 3/9/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 3/10/20 4:37 LBDg/L0.16 3/9/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 3/10/20 4:37 LBDg/L0.12 3/9/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 3/10/20 4:37 LBDg/L0.13 3/9/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 3/10/20 4:37 LBDg/L0.26 3/9/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 3/10/20 4:37 LBDg/L0.16 3/9/20SM21-22 6200B11,1-Dichloroethane
ND 0.50 3/10/20 4:37 LBDg/L0.41 3/9/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 3/10/20 4:37 LBDg/L0.32 3/9/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 3/10/20 4:37 LBDg/L0.13 3/9/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 3/10/20 4:37 LBDg/L0.31 3/9/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 3/10/20 4:37 LBDg/L0.20 3/9/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 3/10/20 4:37 LBDg/L0.11 3/9/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 3/10/20 4:37 LBDg/L0.20 3/9/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 3/10/20 4:37 LBDg/L0.16 3/9/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 3/10/20 4:37 LBDg/L0.13 3/9/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 3/10/20 4:37 LBDg/L0.23 3/9/20SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 3/10/20 4:37 LBDg/L0.17 3/9/20SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 3/10/20 4:37 LBDg/L0.13 3/9/20SM21-22 6200B1Ethylbenzene
ND 5.0 3/10/20 4:37 LBDg/L1.5 3/9/20SM21-22 6200B12-Hexanone (MBK)
ND 0.50 3/10/20 4:37 LBDg/L0.17 3/9/20SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 3/10/20 4:37 LBDg/L0.20 3/9/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 3/10/20 4:37 LBDg/L0.25 3/9/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 3/10/20 4:37 LBDg/L0.34 3/9/20SM21-22 6200B1Methylene Chloride
ND 5.0 3/10/20 4:37 LBDg/L1.7 3/9/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 25 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 3/6/2020
Work Order: 20C0345Sample Description:Project Location: 101 Rand Road., Raleigh, NC
Sample ID: 20C0345-11
Field Sample #: WSW-1
Sample Matrix: Water
Sampled: 3/6/2020 12:10
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 3/10/20 4:37 LBDg/L0.31 3/9/20SM21-22 6200B1Naphthalene
ND 0.50 3/10/20 4:37 LBDg/L0.13 3/9/20SM21-22 6200B1n-Propylbenzene
ND 0.50 3/10/20 4:37 LBDg/L0.11 3/9/20SM21-22 6200B1Styrene
ND 0.50 3/10/20 4:37 LBDg/L0.22 3/9/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 3/10/20 4:37 LBDg/L0.18 3/9/20SM21-22 6200B1Tetrachloroethylene
ND 0.50 3/10/20 4:37 LBDg/L0.14 3/9/20SM21-22 6200B1Toluene
ND 1.0 3/10/20 4:37 LBDg/L0.57 3/9/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 3/10/20 4:37 LBDg/L0.40 3/9/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 3/10/20 4:37 LBDg/L0.20 3/9/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 3/10/20 4:37 LBDg/L0.16 3/9/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 3/10/20 4:37 LBDg/L0.24 3/9/20SM21-22 6200B1Trichloroethylene
ND 0.50 3/10/20 4:37 LBDg/L0.33 3/9/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 3/10/20 4:37 LBDg/L0.25 3/9/20SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 3/10/20 4:37 LBDg/L0.18 3/9/20SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 3/10/20 4:37 LBDg/L0.14 3/9/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 3/10/20 4:37 LBDg/L10 3/9/20SM21-22 6200B1Vinyl Acetate
ND 0.50 3/10/20 4:37 LBDg/L0.45 3/9/20SM21-22 6200B1Vinyl Chloride
ND 1.0 3/10/20 4:37 LBDg/L0.30 3/9/20SM21-22 6200B1m+p Xylene
ND 0.50 3/10/20 4:37 LBDg/L0.17 3/9/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 90.7 3/10/20 4:3770-130
Toluene-d8 99.5 3/10/20 4:3770-130
4-Bromofluorobenzene 96.6 3/10/20 4:3770-130
Page 26 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5030B Analytical Method: SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B253782 03/09/205 5.0020C0345-01 [MW-2]
B253782 03/09/205 5.0020C0345-02 [MW-3]
B253782 03/09/205 5.0020C0345-04 [MW-5]
B253782 03/09/205 5.0020C0345-05 [MW-6]
B253782 03/09/205 5.0020C0345-06 [MW-7]
B253782 03/09/205 5.0020C0345-07 [MW-8]
B253782 03/09/205 5.0020C0345-08 [MW-9]
B253782 03/09/205 5.0020C0345-09 [MW-10]
B253782 03/09/205 5.0020C0345-10 [MW-11]
B253782 03/09/205 5.0020C0345-11 [WSW-1]
Prep Method: SW-846 5030B Analytical Method: SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B253893 03/10/202.5 5.0020C0345-03 [MW-4]
[TOC_1]Sample Preparation Information[TOC]
Page 27 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B253782 - SW-846 5030B
[TOC_3]B253782[TOC]
Blank (B253782-BLK1) Prepared & Analyzed: 03/09/20
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
[TOC_1]QC Data[TOC]
Page 28 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B253782 - SW-846 5030B
Blank (B253782-BLK1) Prepared & Analyzed: 03/09/20
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 87.421.9
g/L 25.0 70-130Surrogate: Toluene-d8 98.124.5
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 95.223.8
LCS (B253782-BS1) Prepared & Analyzed: 03/09/20
Acetone g/L50 200 70-130101201
Benzene g/L0.50 20.0 70-13010220.4
Bromobenzene g/L0.50 20.0 70-13010621.2
Bromochloromethane g/L0.50 20.0 70-13011022.0
Bromodichloromethane g/L0.50 20.0 70-13010721.4
Bromoform g/L0.50 20.0 70-13011122.1
Bromomethane g/L1.0 20.0 60-14010521.0
2-Butanone (MEK)g/L5.0 200 70-13093.3187
n-Butylbenzene g/L0.50 20.0 70-13095.319.1
sec-Butylbenzene g/L0.50 20.0 70-13010420.9
tert-Butylbenzene g/L0.50 20.0 70-13010420.8
Carbon Tetrachloride g/L0.50 20.0 70-13098.419.7
Chlorobenzene g/L0.50 20.0 70-13011523.0
Ethanol g/L50 200 70-130102205
Chlorodibromomethane g/L0.50 20.0 70-13010921.8
Chloroethane g/L0.50 20.0 60-14010420.7
Chloroform g/L0.50 20.0 70-13010120.1
Chloromethane g/L0.60 20.0 60-14084.817.0
2-Chlorotoluene g/L0.50 20.0 70-13010621.2
4-Chlorotoluene g/L0.50 20.0 70-13010621.3
1,2-Dibromoethane (EDB)g/L0.50 20.0 70-13011122.2
1,2-Dichlorobenzene g/L0.50 20.0 70-13010821.5
1,3-Dichlorobenzene g/L0.50 20.0 70-13011222.3
1,4-Dichlorobenzene g/L0.50 20.0 70-13010621.3
Dichlorodifluoromethane (Freon 12)g/L0.50 20.0 60-14080.116.0
1,1-Dichloroethane g/L0.50 20.0 70-13010220.4
1,2-Dichloroethane g/L0.50 20.0 70-13010220.3
1,1-Dichloroethylene g/L0.50 20.0 70-13010621.3
cis-1,2-Dichloroethylene g/L0.50 20.0 70-13010220.4
trans-1,2-Dichloroethylene g/L0.50 20.0 70-13098.719.7
1,2-Dichloropropane g/L0.50 20.0 70-13010621.3
1,3-Dichloropropane g/L0.50 20.0 70-13010621.1
2,2-Dichloropropane g/L0.50 20.0 70-13082.616.5
1,1-Dichloropropene g/L0.50 20.0 70-13097.819.6
cis-1,3-Dichloropropene g/L0.50 20.0 70-13010721.3
trans-1,3-Dichloropropene g/L0.50 20.0 70-13010220.3
Page 29 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B253782 - SW-846 5030B
LCS (B253782-BS1) Prepared & Analyzed: 03/09/20
Diisopropyl Ether (DIPE)g/L0.50 20.0 70-13010220.4
Ethylbenzene g/L0.50 20.0 70-13010621.1
2-Hexanone (MBK)g/L5.0 200 70-13096.5193
Isopropylbenzene (Cumene)g/L0.50 20.0 70-13010821.5
p-Isopropyltoluene (p-Cymene)g/L0.50 20.0 70-13010020.1
Methyl tert-Butyl Ether (MTBE)g/L0.50 20.0 70-13010320.5
Methylene Chloride g/L5.0 20.0 70-13011122.3
4-Methyl-2-pentanone (MIBK)g/L5.0 200 70-13094.7189
Naphthalene g/L0.50 20.0 70-13072.814.6
n-Propylbenzene g/L0.50 20.0 70-13010320.6
Styrene g/L0.50 20.0 70-13011021.9
1,1,2,2-Tetrachloroethane g/L0.50 20.0 70-13011823.7
Tetrachloroethylene g/L0.50 20.0 70-13010621.2
Toluene g/L0.50 20.0 70-13010621.2
1,2,3-Trichlorobenzene g/L1.0 20.0 70-13071.614.3
1,2,4-Trichlorobenzene g/L0.50 20.0 70-13081.216.2
1,1,1-Trichloroethane g/L0.50 20.0 70-13095.919.2
1,1,2-Trichloroethane g/L0.50 20.0 70-13011222.4
Trichloroethylene g/L0.50 20.0 70-13010621.2
Trichlorofluoromethane (Freon 11)g/L0.50 20.0 70-13093.818.8
1,2,3-Trichloropropane g/L0.50 20.0 70-13098.419.7
1,2,4-Trimethylbenzene g/L0.50 20.0 70-13010220.3
1,3,5-Trimethylbenzene g/L0.50 20.0 70-13010220.5
Vinyl Acetate g/L20 200 70-13074.7149
Vinyl Chloride g/L0.50 20.0 60-14082.416.5
m+p Xylene g/L1.0 40.0 70-13010742.7
o-Xylene g/L0.50 20.0 70-13010921.8
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 90.722.7
g/L 25.0 70-130Surrogate: Toluene-d8 99.324.8
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 98.224.5
LCS Dup (B253782-BSD1) Prepared & Analyzed: 03/09/20
Acetone g/L50 200 2570-130105 3.80209
Benzene g/L0.50 20.0 2570-130101 0.59020.3
Bromobenzene g/L0.50 20.0 2570-130105 1.1421.0
Bromochloromethane g/L0.50 20.0 2570-130111 0.63322.2
Bromodichloromethane g/L0.50 20.0 2570-130107 0.093421.4
Bromoform g/L0.50 20.0 2570-130111 0.49622.2
Bromomethane g/L1.0 20.0 2560-140104 0.85920.9
2-Butanone (MEK)g/L5.0 200 2570-13094.9 1.72190
n-Butylbenzene g/L0.50 20.0 2570-13094.3 1.0518.9
sec-Butylbenzene g/L0.50 20.0 2570-130108 2.9721.5
tert-Butylbenzene g/L0.50 20.0 2570-130110 5.6022.0
Carbon Tetrachloride g/L0.50 20.0 2570-13099.0 0.65819.8
Chlorobenzene g/L0.50 20.0 2570-130114 0.74222.8
Ethanol g/L50 200 2570-130101 1.26202
Chlorodibromomethane g/L0.50 20.0 2570-130110 1.0522.0
Chloroethane g/L0.50 20.0 2560-140104 0.38520.8
Chloroform g/L0.50 20.0 2570-130102 0.89120.3
Chloromethane g/L0.60 20.0 2560-14088.0 3.7117.6
2-Chlorotoluene g/L0.50 20.0 2570-130107 1.1321.4
4-Chlorotoluene g/L0.50 20.0 2570-130107 1.0321.5
Page 30 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B253782 - SW-846 5030B
LCS Dup (B253782-BSD1) Prepared & Analyzed: 03/09/20
1,2-Dibromoethane (EDB)g/L0.50 20.0 2570-130112 1.3922.5
1,2-Dichlorobenzene g/L0.50 20.0 2570-130114 5.6422.8
1,3-Dichlorobenzene g/L0.50 20.0 2570-130114 2.6122.9
1,4-Dichlorobenzene g/L0.50 20.0 2570-130109 2.3721.8
Dichlorodifluoromethane (Freon 12)g/L0.50 20.0 2560-14077.2 3.6215.4
1,1-Dichloroethane g/L0.50 20.0 2570-130102 0.34320.4
1,2-Dichloroethane g/L0.50 20.0 2570-130101 0.14820.3
1,1-Dichloroethylene g/L0.50 20.0 2570-130105 0.85021.1
cis-1,2-Dichloroethylene g/L0.50 20.0 2570-130101 0.78720.2
trans-1,2-Dichloroethylene g/L0.50 20.0 2570-130104 5.4720.8
1,2-Dichloropropane g/L0.50 20.0 2570-130106 0.66021.1
1,3-Dichloropropane g/L0.50 20.0 2570-130107 1.0821.4
2,2-Dichloropropane g/L0.50 20.0 2570-13082.8 0.30216.6
1,1-Dichloropropene g/L0.50 20.0 2570-13097.8 0.051119.6
cis-1,3-Dichloropropene g/L0.50 20.0 2570-130107 0.18721.4
trans-1,3-Dichloropropene g/L0.50 20.0 2570-130102 0.24620.4
Diisopropyl Ether (DIPE)g/L0.50 20.0 2570-130103 0.83120.5
Ethylbenzene g/L0.50 20.0 2570-130106 0.61421.2
2-Hexanone (MBK)g/L5.0 200 2570-13096.4 0.0777193
Isopropylbenzene (Cumene)g/L0.50 20.0 2570-130108 0.41721.6
p-Isopropyltoluene (p-Cymene)g/L0.50 20.0 2570-130104 3.8120.8
Methyl tert-Butyl Ether (MTBE)g/L0.50 20.0 2570-130111 7.7322.2
Methylene Chloride g/L5.0 20.0 2570-130102 8.7120.4
4-Methyl-2-pentanone (MIBK)g/L5.0 200 2570-13094.9 0.163190
Naphthalene g/L0.50 20.0 2570-13074.2 1.8414.8
n-Propylbenzene g/L0.50 20.0 2570-130103 0.0020.6
Styrene g/L0.50 20.0 2570-130109 0.22821.9
1,1,2,2-Tetrachloroethane g/L0.50 20.0 2570-130120 1.0523.9
Tetrachloroethylene g/L0.50 20.0 2570-130106 0.047321.2
Toluene g/L0.50 20.0 2570-130105 0.85221.0
1,2,3-Trichlorobenzene g/L1.0 20.0 2570-13073.6 2.8914.7
1,2,4-Trichlorobenzene g/L0.50 20.0 2570-13079.7 1.9315.9
1,1,1-Trichloroethane g/L0.50 20.0 2570-13095.9 0.0019.2
1,1,2-Trichloroethane g/L0.50 20.0 2570-130114 1.6022.7
Trichloroethylene g/L0.50 20.0 2570-130107 0.80021.3
Trichlorofluoromethane (Freon 11)g/L0.50 20.0 2570-13089.7 4.4717.9
1,2,3-Trichloropropane g/L0.50 20.0 2570-130104 5.3020.7
1,2,4-Trimethylbenzene g/L0.50 20.0 2570-130105 3.3921.0
1,3,5-Trimethylbenzene g/L0.50 20.0 2570-130104 1.2120.7
Vinyl Acetate g/L20 200 2570-13075.5 0.986151
Vinyl Chloride g/L0.50 20.0 2560-14085.8 4.0517.2
m+p Xylene g/L1.0 40.0 2570-130106 0.77642.4
o-Xylene g/L0.50 20.0 2570-130109 0.18321.9
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 90.322.6
g/L 25.0 70-130Surrogate: Toluene-d8 10025.1
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 98.024.5
Page 31 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B253893 - SW-846 5030B
[TOC_3]B253893[TOC]
Blank (B253893-BLK1) Prepared & Analyzed: 03/10/20
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0 L-04ND
1,2,4-Trichlorobenzene g/L0.50ND
Page 32 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B253893 - SW-846 5030B
Blank (B253893-BLK1) Prepared & Analyzed: 03/10/20
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 92.723.2
g/L 25.0 70-130Surrogate: Toluene-d8 98.824.7
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 94.323.6
LCS (B253893-BS1) Prepared & Analyzed: 03/10/20
Acetone g/L50 200 70-13088.9178
Benzene g/L0.50 20.0 70-13097.419.5
Bromobenzene g/L0.50 20.0 70-13010220.4
Bromochloromethane g/L0.50 20.0 70-13010721.3
Bromodichloromethane g/L0.50 20.0 70-13010320.6
Bromoform g/L0.50 20.0 70-13010821.6
Bromomethane g/L1.0 20.0 60-14096.819.4
2-Butanone (MEK)g/L5.0 200 70-13090.0180
n-Butylbenzene g/L0.50 20.0 70-13088.017.6
sec-Butylbenzene g/L0.50 20.0 70-13099.219.8
tert-Butylbenzene g/L0.50 20.0 70-13098.419.7
Carbon Tetrachloride g/L0.50 20.0 70-13094.418.9
Chlorobenzene g/L0.50 20.0 70-13010821.6
Ethanol g/L50 200 70-130102203
Chlorodibromomethane g/L0.50 20.0 70-13010521.0
Chloroethane g/L0.50 20.0 60-14011122.1
Chloroform g/L0.50 20.0 70-13097.319.5
Chloromethane g/L0.60 20.0 60-14081.416.3
2-Chlorotoluene g/L0.50 20.0 70-13010120.2
4-Chlorotoluene g/L0.50 20.0 70-13010120.2
1,2-Dibromoethane (EDB)g/L0.50 20.0 70-13010821.6
1,2-Dichlorobenzene g/L0.50 20.0 70-13010420.8
1,3-Dichlorobenzene g/L0.50 20.0 70-13010821.6
1,4-Dichlorobenzene g/L0.50 20.0 70-13010220.3
Dichlorodifluoromethane (Freon 12)g/L0.50 20.0 60-14072.514.5
1,1-Dichloroethane g/L0.50 20.0 70-13097.219.4
1,2-Dichloroethane g/L0.50 20.0 70-13097.019.4
1,1-Dichloroethylene g/L0.50 20.0 70-13090.618.1
cis-1,2-Dichloroethylene g/L0.50 20.0 70-13098.219.6
trans-1,2-Dichloroethylene g/L0.50 20.0 70-13099.719.9
1,2-Dichloropropane g/L0.50 20.0 70-13010420.8
1,3-Dichloropropane g/L0.50 20.0 70-13010320.7
2,2-Dichloropropane g/L0.50 20.0 70-13092.618.5
1,1-Dichloropropene g/L0.50 20.0 70-13092.218.4
cis-1,3-Dichloropropene g/L0.50 20.0 70-13010420.8
trans-1,3-Dichloropropene g/L0.50 20.0 70-13010320.6
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B253893 - SW-846 5030B
LCS (B253893-BS1) Prepared & Analyzed: 03/10/20
Diisopropyl Ether (DIPE)g/L0.50 20.0 70-13010020.0
Ethylbenzene g/L0.50 20.0 70-13010120.3
2-Hexanone (MBK)g/L5.0 200 70-13090.7181
Isopropylbenzene (Cumene)g/L0.50 20.0 70-13010220.4
p-Isopropyltoluene (p-Cymene)g/L0.50 20.0 70-13095.319.1
Methyl tert-Butyl Ether (MTBE)g/L0.50 20.0 70-13010721.3
Methylene Chloride g/L5.0 20.0 70-13010020.1
4-Methyl-2-pentanone (MIBK)g/L5.0 200 70-13088.9178
Naphthalene g/L0.50 20.0 L-0770-13062.4 *12.5
n-Propylbenzene g/L0.50 20.0 70-13098.219.6
Styrene g/L0.50 20.0 70-13010521.0
1,1,2,2-Tetrachloroethane g/L0.50 20.0 70-13011623.1
Tetrachloroethylene g/L0.50 20.0 70-13010220.4
Toluene g/L0.50 20.0 70-13010120.1
1,2,3-Trichlorobenzene g/L1.0 20.0 L-0470-13063.6 *12.7
1,2,4-Trichlorobenzene g/L0.50 20.0 70-13070.414.1
1,1,1-Trichloroethane g/L0.50 20.0 70-13092.418.5
1,1,2-Trichloroethane g/L0.50 20.0 70-13011022.0
Trichloroethylene g/L0.50 20.0 70-13010220.4
Trichlorofluoromethane (Freon 11)g/L0.50 20.0 70-13086.417.3
1,2,3-Trichloropropane g/L0.50 20.0 70-13010020.0
1,2,4-Trimethylbenzene g/L0.50 20.0 70-13098.619.7
1,3,5-Trimethylbenzene g/L0.50 20.0 70-13098.019.6
Vinyl Acetate g/L20 200 70-13086.5173
Vinyl Chloride g/L0.50 20.0 60-14080.016.0
m+p Xylene g/L1.0 40.0 70-13010140.4
o-Xylene g/L0.50 20.0 70-13010521.0
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 89.822.5
g/L 25.0 70-130Surrogate: Toluene-d8 99.224.8
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 97.424.3
LCS Dup (B253893-BSD1) Prepared & Analyzed: 03/10/20
Acetone g/L50 200 2570-13098.0 9.75196
Benzene g/L0.50 20.0 2570-130100 2.9420.0
Bromobenzene g/L0.50 20.0 2570-130104 1.9920.8
Bromochloromethane g/L0.50 20.0 2570-130108 1.4921.7
Bromodichloromethane g/L0.50 20.0 2570-130107 3.6321.3
Bromoform g/L0.50 20.0 2570-130110 1.3821.9
Bromomethane g/L1.0 20.0 2560-140109 12.221.9
2-Butanone (MEK)g/L5.0 200 2570-13096.4 6.86193
n-Butylbenzene g/L0.50 20.0 2570-13092.3 4.7118.5
sec-Butylbenzene g/L0.50 20.0 2570-130106 6.3021.1
tert-Butylbenzene g/L0.50 20.0 2570-130105 6.5821.0
Carbon Tetrachloride g/L0.50 20.0 2570-13095.0 0.73919.0
Chlorobenzene g/L0.50 20.0 2570-130112 3.8622.4
Ethanol g/L50 200 2570-13098.8 2.91198
Chlorodibromomethane g/L0.50 20.0 2570-130107 1.8421.4
Chloroethane g/L0.50 20.0 2560-140103 6.9320.6
Chloroform g/L0.50 20.0 2570-13099.9 2.6420.0
Chloromethane g/L0.60 20.0 2560-14081.4 0.061416.3
2-Chlorotoluene g/L0.50 20.0 2570-130105 3.4020.9
4-Chlorotoluene g/L0.50 20.0 2570-130105 4.4621.1
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B253893 - SW-846 5030B
LCS Dup (B253893-BSD1) Prepared & Analyzed: 03/10/20
1,2-Dibromoethane (EDB)g/L0.50 20.0 2570-130111 2.9322.2
1,2-Dichlorobenzene g/L0.50 20.0 2570-130108 3.4921.6
1,3-Dichlorobenzene g/L0.50 20.0 2570-130113 4.8322.7
1,4-Dichlorobenzene g/L0.50 20.0 2570-130109 6.5221.7
Dichlorodifluoromethane (Freon 12)g/L0.50 20.0 2560-14074.7 2.9914.9
1,1-Dichloroethane g/L0.50 20.0 2570-130100 3.3420.1
1,2-Dichloroethane g/L0.50 20.0 2570-130101 4.2920.3
1,1-Dichloroethylene g/L0.50 20.0 2570-13096.0 5.7919.2
cis-1,2-Dichloroethylene g/L0.50 20.0 2570-130101 2.5220.1
trans-1,2-Dichloroethylene g/L0.50 20.0 2570-130101 0.94820.1
1,2-Dichloropropane g/L0.50 20.0 2570-130107 2.8421.4
1,3-Dichloropropane g/L0.50 20.0 2570-130105 1.4921.0
2,2-Dichloropropane g/L0.50 20.0 2570-13093.8 1.2318.8
1,1-Dichloropropene g/L0.50 20.0 2570-13095.5 3.5219.1
cis-1,3-Dichloropropene g/L0.50 20.0 2570-130107 3.0821.4
trans-1,3-Dichloropropene g/L0.50 20.0 2570-130106 2.4021.1
Diisopropyl Ether (DIPE)g/L0.50 20.0 2570-130101 1.0920.2
Ethylbenzene g/L0.50 20.0 2570-130105 3.2520.9
2-Hexanone (MBK)g/L5.0 200 2570-13099.6 9.33199
Isopropylbenzene (Cumene)g/L0.50 20.0 2570-130105 3.1821.1
p-Isopropyltoluene (p-Cymene)g/L0.50 20.0 2570-130100 5.1120.1
Methyl tert-Butyl Ether (MTBE)g/L0.50 20.0 2570-130107 0.60821.4
Methylene Chloride g/L5.0 20.0 2570-130111 9.7122.1
4-Methyl-2-pentanone (MIBK)g/L5.0 200 2570-13096.7 8.41193
Naphthalene g/L0.50 20.0 2570-13072.0 14.214.4
n-Propylbenzene g/L0.50 20.0 2570-130101 2.7620.2
Styrene g/L0.50 20.0 2570-130108 2.7821.6
1,1,2,2-Tetrachloroethane g/L0.50 20.0 2570-130119 2.6923.8
Tetrachloroethylene g/L0.50 20.0 2570-130105 2.8021.0
Toluene g/L0.50 20.0 2570-130104 3.4220.8
1,2,3-Trichlorobenzene g/L1.0 20.0 25 L-0470-13069.7 9.07*13.9
1,2,4-Trichlorobenzene g/L0.50 20.0 2570-13076.6 8.5115.3
1,1,1-Trichloroethane g/L0.50 20.0 2570-13095.6 3.3519.1
1,1,2-Trichloroethane g/L0.50 20.0 2570-130113 2.1622.5
Trichloroethylene g/L0.50 20.0 2570-130105 2.9421.0
Trichlorofluoromethane (Freon 11)g/L0.50 20.0 2570-13083.4 3.4216.7
1,2,3-Trichloropropane g/L0.50 20.0 2570-13097.5 2.4819.5
1,2,4-Trimethylbenzene g/L0.50 20.0 2570-130103 4.3720.6
1,3,5-Trimethylbenzene g/L0.50 20.0 2570-130101 2.6220.1
Vinyl Acetate g/L20 200 2570-13087.1 0.714174
Vinyl Chloride g/L0.50 20.0 2560-14084.9 6.0117.0
m+p Xylene g/L1.0 40.0 2570-130104 2.8841.6
o-Xylene g/L0.50 20.0 2570-130108 2.8721.6
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 89.722.4
g/L 25.0 70-130Surrogate: Toluene-d8 99.324.8
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 98.424.6
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Elevated reporting limit due to high concentration of target compounds.RL-11
[TOC_1]Flag/Qualifier Summary[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
[TOC_1]Certifications[TOC]
Page 37 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2022
M-MA100Massachusetts DEPMA 06/30/2020
PH-0567Connecticut Department of Publilc HealthCT 09/30/2021
10899 NELAPNew York State Department of HealthNY 04/1/2020
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2021
LAO00112Rhode Island Department of HealthRI 12/30/2020
652North Carolina Div. of Water QualityNC 12/31/2020
MA007 NELAPNew Jersey DEPNJ 06/30/2020
E871027 NELAPFlorida Department of HealthFL 06/30/2020
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2020
2011028State of MaineME 06/9/2021
460217Commonwealth of VirginiaVA 12/14/2020
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2020
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2020
25703North Carolina Department of HealthNC-DW 07/31/2020
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2020
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