RA-918_6174_CA_LAB_20200228_Contest Labs_Final

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
February 28, 2020
Matt Gillis
ECS Southeast - Raleigh, NC
9001 Glenwood Avenue
Raleigh, NC 27617
Project Location: Middleburg, Vance County, NC
Client Job Number:
Project Number: 49:1638-E
Laboratory Work Order Number: 20B0870
Enclosed are results of analyses for samples received by the laboratory on February 19, 2020. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 45
Table of Contents
Table of Contents
Sample Summary 3
Hits Only Report 4
Case Narrative 7
Sample Results 8
20B0870-01 8
20B0870-02 10
20B0870-03 12
20B0870-04 14
20B0870-05 16
20B0870-06 18
20B0870-07 20
20B0870-08 22
20B0870-09 24
20B0870-10 26
20B0870-11 28
Sample Preparation Information 30
QC Data 31
Volatile Organic Compounds by GC/MS 31
B252791 31
B252860 35
Flag/Qualifier Summary 39
Certifications 40
Chain of Custody/Sample Receipt 42
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
2/28/2020
ECS Southeast - Raleigh, NC
9001 Glenwood Avenue
Raleigh, NC 27617
ATTN: Matt Gillis
49:1638-E
20B0870
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Middleburg, Vance County, NC
field blank 20B0870-01 Field Blank SM21-22 6200B
MW-6 20B0870-02 Ground Water SM21-22 6200B
MW-4R 20B0870-03 Ground Water SM21-22 6200B
MW-2R 20B0870-04 Ground Water SM21-22 6200B
MW-13 20B0870-05 Ground Water SM21-22 6200B
MW-1R 20B0870-06 Ground Water SM21-22 6200B
MW-12 20B0870-07 Ground Water SM21-22 6200B
DW-1 20B0870-08 Ground Water SM21-22 6200B
WSW-1 20B0870-09 Ground Water SM21-22 6200B
WSW-2 20B0870-10 Ground Water SM21-22 6200B
WSW-13 20B0870-11 Ground Water SM21-22 6200B
[TOC_1]Sample Summary[TOC]
Page 3 of 45
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:20B0870-01field blank
No Results Detected
Client ID:Lab ID:20B0870-02MW-6
No Results Detected
Client ID:Lab ID:20B0870-04MW-2R
No Results Detected
Client ID:Lab ID:20B0870-05MW-13
No Results Detected
Client ID:Lab ID:20B0870-08DW-1
No Results Detected
Client ID:Lab ID:20B0870-10WSW-2
No Results Detected
Client ID:Lab ID:20B0870-11WSW-13
No Results Detected
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 4 of 45
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
20B0870-03MW-4R
DL
1,2,4-Trimethylbenzene 4.8 0.50 g/L SM21-22 6200B0.18
1,2-Dichloroethane 0.93 1.0 g/L SM21-22 6200BJ0.41
1,3,5-Trimethylbenzene 5.9 0.50 g/L SM21-22 6200B0.14
Benzene 63 0.50 g/L SM21-22 6200B0.18
Diisopropyl Ether (DIPE)1.2 0.50 g/L SM21-22 6200B0.17
Ethylbenzene 16 0.50 g/L SM21-22 6200B0.13
Isopropylbenzene (Cumene)11 0.50 g/L SM21-22 6200B0.17
m+p Xylene 11 1.0 g/L SM21-22 6200B0.30
Methyl tert-Butyl Ether (MTBE)0.92 0.50 g/L SM21-22 6200B0.25
Naphthalene 47 5.0 g/L SM21-22 6200B0.31
n-Butylbenzene 5.0 0.50 g/L SM21-22 6200B0.21
n-Propylbenzene 12 0.50 g/L SM21-22 6200B0.13
o-Xylene 1.0 0.50 g/L SM21-22 6200B0.17
p-Isopropyltoluene (p-Cymene)1.2 0.50 g/L SM21-22 6200B0.20
sec-Butylbenzene 1.8 0.50 g/L SM21-22 6200B0.16
Styrene 0.42 0.50 g/L SM21-22 6200BJ0.11
Toluene 2.2 0.50 g/L SM21-22 6200B0.14
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
20B0870-06MW-1R
DL
1,2,4-Trimethylbenzene 460 20 g/L SM21-22 6200B7.2
1,2-Dibromoethane (EDB)38 20 g/L SM21-22 6200B7.6
1,3,5-Trimethylbenzene 220 20 g/L SM21-22 6200B5.6
Benzene 970 20 g/L SM21-22 6200B7.2
Diisopropyl Ether (DIPE)28 20 g/L SM21-22 6200B6.8
Ethylbenzene 230 20 g/L SM21-22 6200B5.2
Isopropylbenzene (Cumene)12 20 g/L SM21-22 6200BJ6.8
m+p Xylene 1700 40 g/L SM21-22 6200B12
Methyl tert-Butyl Ether (MTBE)34 20 g/L SM21-22 6200BL-04 10
Naphthalene 360 200 g/L SM21-22 6200B12
n-Butylbenzene 9.2 20 g/L SM21-22 6200BJ8.4
n-Propylbenzene 20 20 g/L SM21-22 6200B5.2
o-Xylene 950 20 g/L SM21-22 6200B6.8
Styrene 6.0 20 g/L SM21-22 6200BJ4.4
Toluene 2500 20 g/L SM21-22 6200B5.6
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
20B0870-07MW-12
DL
1,2,4-Trimethylbenzene 1000 25 g/L SM21-22 6200B9.0
1,2-Dichloroethane 120 50 g/L SM21-22 6200B20
1,3,5-Trimethylbenzene 330 25 g/L SM21-22 6200B7.0
Benzene 1700 25 g/L SM21-22 6200B9.0
Diisopropyl Ether (DIPE)150 25 g/L SM21-22 6200B8.5
Ethylbenzene 1200 25 g/L SM21-22 6200B6.5
Isopropylbenzene (Cumene)35 25 g/L SM21-22 6200B8.5
m+p Xylene 5000 50 g/L SM21-22 6200B15
Methyl tert-Butyl Ether (MTBE)290 25 g/L SM21-22 6200B12
Naphthalene 500 250 g/L SM21-22 6200B16
n-Butylbenzene 16 25 g/L SM21-22 6200BJ10
n-Propylbenzene 86 25 g/L SM21-22 6200B6.5
o-Xylene 2400 25 g/L SM21-22 6200B8.5
Styrene 24 25 g/L SM21-22 6200BJ5.5
Toluene 3400 25 g/L SM21-22 6200B7.0
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
20B0870-09WSW-1
DL
Chloroform 0.38 0.50 g/L SM21-22 6200BJ0.17
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 6 of 45
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method 6200B elevated reporting limit for samples 20B0870-06+07 due to high concentrations of target compounds.
[TOC_1]Case Narrative[TOC]
SM21-22 6200B
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not
affected since all results are "not detected" for associated samples in this batch and bias is on the high side.
Analyte & Samples(s) Qualified:
L-02
Vinyl Chloride
B252791-BS1, B252791-BSD1, B252860-BS1, B252860-BSD1
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
Methyl tert-Butyl Ether (MTBE)
20B0870-06[MW-1R], B252860-BLK1, B252860-BS1, B252860-BSD1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.Analyte & Samples(s) Qualified:
L-07
Ethanol
B252791-BS1
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
RL-11
20B0870-06[MW-1R], 20B0870-07[MW-12]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-01
Field Sample #: field blank
Sample Matrix: Field Blank
Sampled: 2/18/2020 11:17
[TOC_2]20B0870-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 2/22/20 20:43 EEHg/L3.8 2/21/20SM21-22 6200B1Acetone
ND 0.50 2/22/20 20:43 EEHg/L0.18 2/21/20SM21-22 6200B1Benzene
ND 0.50 2/22/20 20:43 EEHg/L0.15 2/21/20SM21-22 6200B1Bromobenzene
ND 0.50 2/22/20 20:43 EEHg/L0.32 2/21/20SM21-22 6200B1Bromochloromethane
ND 0.50 2/22/20 20:43 EEHg/L0.16 2/21/20SM21-22 6200B1Bromodichloromethane
ND 0.50 2/22/20 20:43 EEHg/L0.46 2/21/20SM21-22 6200B1Bromoform
ND 1.0 2/22/20 20:43 EEHg/L0.78 2/21/20SM21-22 6200B1Bromomethane
ND 5.0 2/22/20 20:43 EEHg/L1.9 2/21/20SM21-22 6200B12-Butanone (MEK)
ND 0.50 2/22/20 20:43 EEHg/L0.21 2/21/20SM21-22 6200B1n-Butylbenzene
ND 0.50 2/22/20 20:43 EEHg/L0.16 2/21/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 2/22/20 20:43 EEHg/L0.17 2/21/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 2/22/20 20:43 EEHg/L0.11 2/21/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 2/22/20 20:43 EEHg/L0.15 2/21/20SM21-22 6200B1Chlorobenzene
ND 50 2/22/20 20:43 EEHg/L11 2/21/20SM21-22 6200B1Ethanol
ND 0.50 2/22/20 20:43 EEHg/L0.21 2/21/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 2/22/20 20:43 EEHg/L0.35 2/21/20SM21-22 6200B1Chloroethane
ND 0.50 2/22/20 20:43 EEHg/L0.17 2/21/20SM21-22 6200B1Chloroform
ND 1.0 2/22/20 20:43 EEHg/L0.45 2/21/20SM21-22 6200B1Chloromethane
ND 0.50 2/22/20 20:43 EEHg/L0.12 2/21/20SM21-22 6200B12-Chlorotoluene
ND 0.50 2/22/20 20:43 EEHg/L0.14 2/21/20SM21-22 6200B14-Chlorotoluene
ND 0.50 2/22/20 20:43 EEHg/L0.19 2/21/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 2/22/20 20:43 EEHg/L0.16 2/21/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 2/22/20 20:43 EEHg/L0.12 2/21/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 2/22/20 20:43 EEHg/L0.13 2/21/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 2/22/20 20:43 EEHg/L0.26 2/21/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 2/22/20 20:43 EEHg/L0.16 2/21/20SM21-22 6200B11,1-Dichloroethane
ND 1.0 2/22/20 20:43 EEHg/L0.41 2/21/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 2/22/20 20:43 EEHg/L0.32 2/21/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 2/22/20 20:43 EEHg/L0.13 2/21/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 2/22/20 20:43 EEHg/L0.31 2/21/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 2/22/20 20:43 EEHg/L0.20 2/21/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 2/22/20 20:43 EEHg/L0.11 2/21/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 2/22/20 20:43 EEHg/L0.20 2/21/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 2/22/20 20:43 EEHg/L0.16 2/21/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 2/22/20 20:43 EEHg/L0.13 2/21/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 2/22/20 20:43 EEHg/L0.23 2/21/20SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 2/22/20 20:43 EEHg/L0.17 2/21/20SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 2/22/20 20:43 EEHg/L0.13 2/21/20SM21-22 6200B1Ethylbenzene
ND 5.0 2/22/20 20:43 EEHg/L1.5 2/21/20SM21-22 6200B12-Hexanone (MBK)
ND 0.50 2/22/20 20:43 EEHg/L0.17 2/21/20SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 2/22/20 20:43 EEHg/L0.20 2/21/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 2/22/20 20:43 EEHg/L0.25 2/21/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 2/22/20 20:43 EEHg/L0.34 2/21/20SM21-22 6200B1Methylene Chloride
ND 5.0 2/22/20 20:43 EEHg/L1.7 2/21/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
[TOC_1]Sample Results[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-01
Field Sample #: field blank
Sample Matrix: Field Blank
Sampled: 2/18/2020 11:17
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 2/22/20 20:43 EEHg/L0.31 2/21/20SM21-22 6200B1Naphthalene
ND 0.50 2/22/20 20:43 EEHg/L0.13 2/21/20SM21-22 6200B1n-Propylbenzene
ND 0.50 2/22/20 20:43 EEHg/L0.11 2/21/20SM21-22 6200B1Styrene
ND 0.50 2/22/20 20:43 EEHg/L0.22 2/21/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 2/22/20 20:43 EEHg/L0.18 2/21/20SM21-22 6200B1Tetrachloroethylene
ND 0.50 2/22/20 20:43 EEHg/L0.14 2/21/20SM21-22 6200B1Toluene
ND 2.0 2/22/20 20:43 EEHg/L0.57 2/21/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 2/22/20 20:43 EEHg/L0.40 2/21/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 2/22/20 20:43 EEHg/L0.20 2/21/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 2/22/20 20:43 EEHg/L0.16 2/21/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 2/22/20 20:43 EEHg/L0.24 2/21/20SM21-22 6200B1Trichloroethylene
ND 0.50 2/22/20 20:43 EEHg/L0.33 2/21/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 2/22/20 20:43 EEHg/L0.25 2/21/20SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 2/22/20 20:43 EEHg/L0.18 2/21/20SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 2/22/20 20:43 EEHg/L0.14 2/21/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 2/22/20 20:43 EEHg/L10 2/21/20SM21-22 6200B1Vinyl Acetate
ND 0.50 2/22/20 20:43 EEHg/L0.45 2/21/20SM21-22 6200B1Vinyl Chloride
ND 1.0 2/22/20 20:43 EEHg/L0.30 2/21/20SM21-22 6200B1m+p Xylene
ND 0.50 2/22/20 20:43 EEHg/L0.17 2/21/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 89.4 2/22/20 20:4370-130
Toluene-d8 99.6 2/22/20 20:4370-130
4-Bromofluorobenzene 93.6 2/22/20 20:4370-130
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-02
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 2/18/2020 11:38
[TOC_2]20B0870-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 2/23/20 0:35 EEHg/L3.8 2/21/20SM21-22 6200B1Acetone
ND 0.50 2/23/20 0:35 EEHg/L0.18 2/21/20SM21-22 6200B1Benzene
ND 0.50 2/23/20 0:35 EEHg/L0.15 2/21/20SM21-22 6200B1Bromobenzene
ND 0.50 2/23/20 0:35 EEHg/L0.32 2/21/20SM21-22 6200B1Bromochloromethane
ND 0.50 2/23/20 0:35 EEHg/L0.16 2/21/20SM21-22 6200B1Bromodichloromethane
ND 0.50 2/23/20 0:35 EEHg/L0.46 2/21/20SM21-22 6200B1Bromoform
ND 1.0 2/23/20 0:35 EEHg/L0.78 2/21/20SM21-22 6200B1Bromomethane
ND 5.0 2/23/20 0:35 EEHg/L1.9 2/21/20SM21-22 6200B12-Butanone (MEK)
ND 0.50 2/23/20 0:35 EEHg/L0.21 2/21/20SM21-22 6200B1n-Butylbenzene
ND 0.50 2/23/20 0:35 EEHg/L0.16 2/21/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 2/23/20 0:35 EEHg/L0.17 2/21/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 2/23/20 0:35 EEHg/L0.11 2/21/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 2/23/20 0:35 EEHg/L0.15 2/21/20SM21-22 6200B1Chlorobenzene
ND 50 2/23/20 0:35 EEHg/L11 2/21/20SM21-22 6200B1Ethanol
ND 0.50 2/23/20 0:35 EEHg/L0.21 2/21/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 2/23/20 0:35 EEHg/L0.35 2/21/20SM21-22 6200B1Chloroethane
ND 0.50 2/23/20 0:35 EEHg/L0.17 2/21/20SM21-22 6200B1Chloroform
ND 1.0 2/23/20 0:35 EEHg/L0.45 2/21/20SM21-22 6200B1Chloromethane
ND 0.50 2/23/20 0:35 EEHg/L0.12 2/21/20SM21-22 6200B12-Chlorotoluene
ND 0.50 2/23/20 0:35 EEHg/L0.14 2/21/20SM21-22 6200B14-Chlorotoluene
ND 0.50 2/23/20 0:35 EEHg/L0.19 2/21/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 2/23/20 0:35 EEHg/L0.16 2/21/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 2/23/20 0:35 EEHg/L0.12 2/21/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 2/23/20 0:35 EEHg/L0.13 2/21/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 2/23/20 0:35 EEHg/L0.26 2/21/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 2/23/20 0:35 EEHg/L0.16 2/21/20SM21-22 6200B11,1-Dichloroethane
ND 1.0 2/23/20 0:35 EEHg/L0.41 2/21/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 2/23/20 0:35 EEHg/L0.32 2/21/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 2/23/20 0:35 EEHg/L0.13 2/21/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 2/23/20 0:35 EEHg/L0.31 2/21/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 2/23/20 0:35 EEHg/L0.20 2/21/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 2/23/20 0:35 EEHg/L0.11 2/21/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 2/23/20 0:35 EEHg/L0.20 2/21/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 2/23/20 0:35 EEHg/L0.16 2/21/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 2/23/20 0:35 EEHg/L0.13 2/21/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 2/23/20 0:35 EEHg/L0.23 2/21/20SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 2/23/20 0:35 EEHg/L0.17 2/21/20SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 2/23/20 0:35 EEHg/L0.13 2/21/20SM21-22 6200B1Ethylbenzene
ND 5.0 2/23/20 0:35 EEHg/L1.5 2/21/20SM21-22 6200B12-Hexanone (MBK)
ND 0.50 2/23/20 0:35 EEHg/L0.17 2/21/20SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 2/23/20 0:35 EEHg/L0.20 2/21/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 2/23/20 0:35 EEHg/L0.25 2/21/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 2/23/20 0:35 EEHg/L0.34 2/21/20SM21-22 6200B1Methylene Chloride
ND 5.0 2/23/20 0:35 EEHg/L1.7 2/21/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-02
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 2/18/2020 11:38
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 2/23/20 0:35 EEHg/L0.31 2/21/20SM21-22 6200B1Naphthalene
ND 0.50 2/23/20 0:35 EEHg/L0.13 2/21/20SM21-22 6200B1n-Propylbenzene
ND 0.50 2/23/20 0:35 EEHg/L0.11 2/21/20SM21-22 6200B1Styrene
ND 0.50 2/23/20 0:35 EEHg/L0.22 2/21/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 2/23/20 0:35 EEHg/L0.18 2/21/20SM21-22 6200B1Tetrachloroethylene
ND 0.50 2/23/20 0:35 EEHg/L0.14 2/21/20SM21-22 6200B1Toluene
ND 2.0 2/23/20 0:35 EEHg/L0.57 2/21/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 2/23/20 0:35 EEHg/L0.40 2/21/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 2/23/20 0:35 EEHg/L0.20 2/21/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 2/23/20 0:35 EEHg/L0.16 2/21/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 2/23/20 0:35 EEHg/L0.24 2/21/20SM21-22 6200B1Trichloroethylene
ND 0.50 2/23/20 0:35 EEHg/L0.33 2/21/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 2/23/20 0:35 EEHg/L0.25 2/21/20SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 2/23/20 0:35 EEHg/L0.18 2/21/20SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 2/23/20 0:35 EEHg/L0.14 2/21/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 2/23/20 0:35 EEHg/L10 2/21/20SM21-22 6200B1Vinyl Acetate
ND 0.50 2/23/20 0:35 EEHg/L0.45 2/21/20SM21-22 6200B1Vinyl Chloride
ND 1.0 2/23/20 0:35 EEHg/L0.30 2/21/20SM21-22 6200B1m+p Xylene
ND 0.50 2/23/20 0:35 EEHg/L0.17 2/21/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 89.8 2/23/20 0:3570-130
Toluene-d8 97.5 2/23/20 0:3570-130
4-Bromofluorobenzene 94.4 2/23/20 0:3570-130
Page 11 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-03
Field Sample #: MW-4R
Sample Matrix: Ground Water
Sampled: 2/18/2020 11:56
[TOC_2]20B0870-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 2/23/20 3:28 EEHg/L3.8 2/21/20SM21-22 6200B1Acetone
63 0.50 2/23/20 3:28 EEHg/L0.18 2/21/20SM21-22 6200B1Benzene
ND 0.50 2/23/20 3:28 EEHg/L0.15 2/21/20SM21-22 6200B1Bromobenzene
ND 0.50 2/23/20 3:28 EEHg/L0.32 2/21/20SM21-22 6200B1Bromochloromethane
ND 0.50 2/23/20 3:28 EEHg/L0.16 2/21/20SM21-22 6200B1Bromodichloromethane
ND 0.50 2/23/20 3:28 EEHg/L0.46 2/21/20SM21-22 6200B1Bromoform
ND 1.0 2/23/20 3:28 EEHg/L0.78 2/21/20SM21-22 6200B1Bromomethane
ND 5.0 2/23/20 3:28 EEHg/L1.9 2/21/20SM21-22 6200B12-Butanone (MEK)
5.0 0.50 2/23/20 3:28 EEHg/L0.21 2/21/20SM21-22 6200B1n-Butylbenzene
1.8 0.50 2/23/20 3:28 EEHg/L0.16 2/21/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 2/23/20 3:28 EEHg/L0.17 2/21/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 2/23/20 3:28 EEHg/L0.11 2/21/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 2/23/20 3:28 EEHg/L0.15 2/21/20SM21-22 6200B1Chlorobenzene
ND 50 2/23/20 3:28 EEHg/L11 2/21/20SM21-22 6200B1Ethanol
ND 0.50 2/23/20 3:28 EEHg/L0.21 2/21/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 2/23/20 3:28 EEHg/L0.35 2/21/20SM21-22 6200B1Chloroethane
ND 0.50 2/23/20 3:28 EEHg/L0.17 2/21/20SM21-22 6200B1Chloroform
ND 1.0 2/23/20 3:28 EEHg/L0.45 2/21/20SM21-22 6200B1Chloromethane
ND 0.50 2/23/20 3:28 EEHg/L0.12 2/21/20SM21-22 6200B12-Chlorotoluene
ND 0.50 2/23/20 3:28 EEHg/L0.14 2/21/20SM21-22 6200B14-Chlorotoluene
ND 0.50 2/23/20 3:28 EEHg/L0.19 2/21/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 2/23/20 3:28 EEHg/L0.16 2/21/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 2/23/20 3:28 EEHg/L0.12 2/21/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 2/23/20 3:28 EEHg/L0.13 2/21/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 2/23/20 3:28 EEHg/L0.26 2/21/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 2/23/20 3:28 EEHg/L0.16 2/21/20SM21-22 6200B11,1-Dichloroethane
0.93 1.0 2/23/20 3:28 EEHg/L0.41 2/21/20SM21-22 6200B1J1,2-Dichloroethane
ND 0.50 2/23/20 3:28 EEHg/L0.32 2/21/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 2/23/20 3:28 EEHg/L0.13 2/21/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 2/23/20 3:28 EEHg/L0.31 2/21/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 2/23/20 3:28 EEHg/L0.20 2/21/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 2/23/20 3:28 EEHg/L0.11 2/21/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 2/23/20 3:28 EEHg/L0.20 2/21/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 2/23/20 3:28 EEHg/L0.16 2/21/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 2/23/20 3:28 EEHg/L0.13 2/21/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 2/23/20 3:28 EEHg/L0.23 2/21/20SM21-22 6200B1trans-1,3-Dichloropropene
1.2 0.50 2/23/20 3:28 EEHg/L0.17 2/21/20SM21-22 6200B1Diisopropyl Ether (DIPE)
16 0.50 2/23/20 3:28 EEHg/L0.13 2/21/20SM21-22 6200B1Ethylbenzene
ND 5.0 2/23/20 3:28 EEHg/L1.5 2/21/20SM21-22 6200B12-Hexanone (MBK)
11 0.50 2/23/20 3:28 EEHg/L0.17 2/21/20SM21-22 6200B1Isopropylbenzene (Cumene)
1.2 0.50 2/23/20 3:28 EEHg/L0.20 2/21/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
0.92 0.50 2/23/20 3:28 EEHg/L0.25 2/21/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 2/23/20 3:28 EEHg/L0.34 2/21/20SM21-22 6200B1Methylene Chloride
ND 5.0 2/23/20 3:28 EEHg/L1.7 2/21/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 12 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-03
Field Sample #: MW-4R
Sample Matrix: Ground Water
Sampled: 2/18/2020 11:56
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
47 5.0 2/23/20 3:28 EEHg/L0.31 2/21/20SM21-22 6200B1Naphthalene
12 0.50 2/23/20 3:28 EEHg/L0.13 2/21/20SM21-22 6200B1n-Propylbenzene
0.42 0.50 2/23/20 3:28 EEHg/L0.11 2/21/20SM21-22 6200B1JStyrene
ND 0.50 2/23/20 3:28 EEHg/L0.22 2/21/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 2/23/20 3:28 EEHg/L0.18 2/21/20SM21-22 6200B1Tetrachloroethylene
2.2 0.50 2/23/20 3:28 EEHg/L0.14 2/21/20SM21-22 6200B1Toluene
ND 2.0 2/23/20 3:28 EEHg/L0.57 2/21/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 2/23/20 3:28 EEHg/L0.40 2/21/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 2/23/20 3:28 EEHg/L0.20 2/21/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 2/23/20 3:28 EEHg/L0.16 2/21/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 2/23/20 3:28 EEHg/L0.24 2/21/20SM21-22 6200B1Trichloroethylene
ND 0.50 2/23/20 3:28 EEHg/L0.33 2/21/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 2/23/20 3:28 EEHg/L0.25 2/21/20SM21-22 6200B11,2,3-Trichloropropane
4.8 0.50 2/23/20 3:28 EEHg/L0.18 2/21/20SM21-22 6200B11,2,4-Trimethylbenzene
5.9 0.50 2/23/20 3:28 EEHg/L0.14 2/21/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 2/23/20 3:28 EEHg/L10 2/21/20SM21-22 6200B1Vinyl Acetate
ND 0.50 2/23/20 3:28 EEHg/L0.45 2/21/20SM21-22 6200B1Vinyl Chloride
11 1.0 2/23/20 3:28 EEHg/L0.30 2/21/20SM21-22 6200B1m+p Xylene
1.0 0.50 2/23/20 3:28 EEHg/L0.17 2/21/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 88.5 2/23/20 3:2870-130
Toluene-d8 98.3 2/23/20 3:2870-130
4-Bromofluorobenzene 101 2/23/20 3:2870-130
Page 13 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-04
Field Sample #: MW-2R
Sample Matrix: Ground Water
Sampled: 2/18/2020 12:16
[TOC_2]20B0870-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 2/23/20 1:32 EEHg/L3.8 2/21/20SM21-22 6200B1Acetone
ND 0.50 2/23/20 1:32 EEHg/L0.18 2/21/20SM21-22 6200B1Benzene
ND 0.50 2/23/20 1:32 EEHg/L0.15 2/21/20SM21-22 6200B1Bromobenzene
ND 0.50 2/23/20 1:32 EEHg/L0.32 2/21/20SM21-22 6200B1Bromochloromethane
ND 0.50 2/23/20 1:32 EEHg/L0.16 2/21/20SM21-22 6200B1Bromodichloromethane
ND 0.50 2/23/20 1:32 EEHg/L0.46 2/21/20SM21-22 6200B1Bromoform
ND 1.0 2/23/20 1:32 EEHg/L0.78 2/21/20SM21-22 6200B1Bromomethane
ND 5.0 2/23/20 1:32 EEHg/L1.9 2/21/20SM21-22 6200B12-Butanone (MEK)
ND 0.50 2/23/20 1:32 EEHg/L0.21 2/21/20SM21-22 6200B1n-Butylbenzene
ND 0.50 2/23/20 1:32 EEHg/L0.16 2/21/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 2/23/20 1:32 EEHg/L0.17 2/21/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 2/23/20 1:32 EEHg/L0.11 2/21/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 2/23/20 1:32 EEHg/L0.15 2/21/20SM21-22 6200B1Chlorobenzene
ND 50 2/23/20 1:32 EEHg/L11 2/21/20SM21-22 6200B1Ethanol
ND 0.50 2/23/20 1:32 EEHg/L0.21 2/21/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 2/23/20 1:32 EEHg/L0.35 2/21/20SM21-22 6200B1Chloroethane
ND 0.50 2/23/20 1:32 EEHg/L0.17 2/21/20SM21-22 6200B1Chloroform
ND 1.0 2/23/20 1:32 EEHg/L0.45 2/21/20SM21-22 6200B1Chloromethane
ND 0.50 2/23/20 1:32 EEHg/L0.12 2/21/20SM21-22 6200B12-Chlorotoluene
ND 0.50 2/23/20 1:32 EEHg/L0.14 2/21/20SM21-22 6200B14-Chlorotoluene
ND 0.50 2/23/20 1:32 EEHg/L0.19 2/21/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 2/23/20 1:32 EEHg/L0.16 2/21/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 2/23/20 1:32 EEHg/L0.12 2/21/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 2/23/20 1:32 EEHg/L0.13 2/21/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 2/23/20 1:32 EEHg/L0.26 2/21/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 2/23/20 1:32 EEHg/L0.16 2/21/20SM21-22 6200B11,1-Dichloroethane
ND 1.0 2/23/20 1:32 EEHg/L0.41 2/21/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 2/23/20 1:32 EEHg/L0.32 2/21/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 2/23/20 1:32 EEHg/L0.13 2/21/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 2/23/20 1:32 EEHg/L0.31 2/21/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 2/23/20 1:32 EEHg/L0.20 2/21/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 2/23/20 1:32 EEHg/L0.11 2/21/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 2/23/20 1:32 EEHg/L0.20 2/21/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 2/23/20 1:32 EEHg/L0.16 2/21/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 2/23/20 1:32 EEHg/L0.13 2/21/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 2/23/20 1:32 EEHg/L0.23 2/21/20SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 2/23/20 1:32 EEHg/L0.17 2/21/20SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 2/23/20 1:32 EEHg/L0.13 2/21/20SM21-22 6200B1Ethylbenzene
ND 5.0 2/23/20 1:32 EEHg/L1.5 2/21/20SM21-22 6200B12-Hexanone (MBK)
ND 0.50 2/23/20 1:32 EEHg/L0.17 2/21/20SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 2/23/20 1:32 EEHg/L0.20 2/21/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 2/23/20 1:32 EEHg/L0.25 2/21/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 2/23/20 1:32 EEHg/L0.34 2/21/20SM21-22 6200B1Methylene Chloride
ND 5.0 2/23/20 1:32 EEHg/L1.7 2/21/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 14 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-04
Field Sample #: MW-2R
Sample Matrix: Ground Water
Sampled: 2/18/2020 12:16
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 2/23/20 1:32 EEHg/L0.31 2/21/20SM21-22 6200B1Naphthalene
ND 0.50 2/23/20 1:32 EEHg/L0.13 2/21/20SM21-22 6200B1n-Propylbenzene
ND 0.50 2/23/20 1:32 EEHg/L0.11 2/21/20SM21-22 6200B1Styrene
ND 0.50 2/23/20 1:32 EEHg/L0.22 2/21/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 2/23/20 1:32 EEHg/L0.18 2/21/20SM21-22 6200B1Tetrachloroethylene
ND 0.50 2/23/20 1:32 EEHg/L0.14 2/21/20SM21-22 6200B1Toluene
ND 2.0 2/23/20 1:32 EEHg/L0.57 2/21/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 2/23/20 1:32 EEHg/L0.40 2/21/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 2/23/20 1:32 EEHg/L0.20 2/21/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 2/23/20 1:32 EEHg/L0.16 2/21/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 2/23/20 1:32 EEHg/L0.24 2/21/20SM21-22 6200B1Trichloroethylene
ND 0.50 2/23/20 1:32 EEHg/L0.33 2/21/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 2/23/20 1:32 EEHg/L0.25 2/21/20SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 2/23/20 1:32 EEHg/L0.18 2/21/20SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 2/23/20 1:32 EEHg/L0.14 2/21/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 2/23/20 1:32 EEHg/L10 2/21/20SM21-22 6200B1Vinyl Acetate
ND 0.50 2/23/20 1:32 EEHg/L0.45 2/21/20SM21-22 6200B1Vinyl Chloride
ND 1.0 2/23/20 1:32 EEHg/L0.30 2/21/20SM21-22 6200B1m+p Xylene
ND 0.50 2/23/20 1:32 EEHg/L0.17 2/21/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 89.7 2/23/20 1:3270-130
Toluene-d8 96.6 2/23/20 1:3270-130
4-Bromofluorobenzene 92.4 2/23/20 1:3270-130
Page 15 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-05
Field Sample #: MW-13
Sample Matrix: Ground Water
Sampled: 2/18/2020 12:30
[TOC_2]20B0870-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 2/23/20 2:01 EEHg/L3.8 2/21/20SM21-22 6200B1Acetone
ND 0.50 2/23/20 2:01 EEHg/L0.18 2/21/20SM21-22 6200B1Benzene
ND 0.50 2/23/20 2:01 EEHg/L0.15 2/21/20SM21-22 6200B1Bromobenzene
ND 0.50 2/23/20 2:01 EEHg/L0.32 2/21/20SM21-22 6200B1Bromochloromethane
ND 0.50 2/23/20 2:01 EEHg/L0.16 2/21/20SM21-22 6200B1Bromodichloromethane
ND 0.50 2/23/20 2:01 EEHg/L0.46 2/21/20SM21-22 6200B1Bromoform
ND 1.0 2/23/20 2:01 EEHg/L0.78 2/21/20SM21-22 6200B1Bromomethane
ND 5.0 2/23/20 2:01 EEHg/L1.9 2/21/20SM21-22 6200B12-Butanone (MEK)
ND 0.50 2/23/20 2:01 EEHg/L0.21 2/21/20SM21-22 6200B1n-Butylbenzene
ND 0.50 2/23/20 2:01 EEHg/L0.16 2/21/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 2/23/20 2:01 EEHg/L0.17 2/21/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 2/23/20 2:01 EEHg/L0.11 2/21/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 2/23/20 2:01 EEHg/L0.15 2/21/20SM21-22 6200B1Chlorobenzene
ND 50 2/23/20 2:01 EEHg/L11 2/21/20SM21-22 6200B1Ethanol
ND 0.50 2/23/20 2:01 EEHg/L0.21 2/21/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 2/23/20 2:01 EEHg/L0.35 2/21/20SM21-22 6200B1Chloroethane
ND 0.50 2/23/20 2:01 EEHg/L0.17 2/21/20SM21-22 6200B1Chloroform
ND 1.0 2/23/20 2:01 EEHg/L0.45 2/21/20SM21-22 6200B1Chloromethane
ND 0.50 2/23/20 2:01 EEHg/L0.12 2/21/20SM21-22 6200B12-Chlorotoluene
ND 0.50 2/23/20 2:01 EEHg/L0.14 2/21/20SM21-22 6200B14-Chlorotoluene
ND 0.50 2/23/20 2:01 EEHg/L0.19 2/21/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 2/23/20 2:01 EEHg/L0.16 2/21/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 2/23/20 2:01 EEHg/L0.12 2/21/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 2/23/20 2:01 EEHg/L0.13 2/21/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 2/23/20 2:01 EEHg/L0.26 2/21/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 2/23/20 2:01 EEHg/L0.16 2/21/20SM21-22 6200B11,1-Dichloroethane
ND 1.0 2/23/20 2:01 EEHg/L0.41 2/21/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 2/23/20 2:01 EEHg/L0.32 2/21/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 2/23/20 2:01 EEHg/L0.13 2/21/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 2/23/20 2:01 EEHg/L0.31 2/21/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 2/23/20 2:01 EEHg/L0.20 2/21/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 2/23/20 2:01 EEHg/L0.11 2/21/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 2/23/20 2:01 EEHg/L0.20 2/21/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 2/23/20 2:01 EEHg/L0.16 2/21/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 2/23/20 2:01 EEHg/L0.13 2/21/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 2/23/20 2:01 EEHg/L0.23 2/21/20SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 2/23/20 2:01 EEHg/L0.17 2/21/20SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 2/23/20 2:01 EEHg/L0.13 2/21/20SM21-22 6200B1Ethylbenzene
ND 5.0 2/23/20 2:01 EEHg/L1.5 2/21/20SM21-22 6200B12-Hexanone (MBK)
ND 0.50 2/23/20 2:01 EEHg/L0.17 2/21/20SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 2/23/20 2:01 EEHg/L0.20 2/21/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 2/23/20 2:01 EEHg/L0.25 2/21/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 2/23/20 2:01 EEHg/L0.34 2/21/20SM21-22 6200B1Methylene Chloride
ND 5.0 2/23/20 2:01 EEHg/L1.7 2/21/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 16 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-05
Field Sample #: MW-13
Sample Matrix: Ground Water
Sampled: 2/18/2020 12:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 2/23/20 2:01 EEHg/L0.31 2/21/20SM21-22 6200B1Naphthalene
ND 0.50 2/23/20 2:01 EEHg/L0.13 2/21/20SM21-22 6200B1n-Propylbenzene
ND 0.50 2/23/20 2:01 EEHg/L0.11 2/21/20SM21-22 6200B1Styrene
ND 0.50 2/23/20 2:01 EEHg/L0.22 2/21/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 2/23/20 2:01 EEHg/L0.18 2/21/20SM21-22 6200B1Tetrachloroethylene
ND 0.50 2/23/20 2:01 EEHg/L0.14 2/21/20SM21-22 6200B1Toluene
ND 2.0 2/23/20 2:01 EEHg/L0.57 2/21/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 2/23/20 2:01 EEHg/L0.40 2/21/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 2/23/20 2:01 EEHg/L0.20 2/21/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 2/23/20 2:01 EEHg/L0.16 2/21/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 2/23/20 2:01 EEHg/L0.24 2/21/20SM21-22 6200B1Trichloroethylene
ND 0.50 2/23/20 2:01 EEHg/L0.33 2/21/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 2/23/20 2:01 EEHg/L0.25 2/21/20SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 2/23/20 2:01 EEHg/L0.18 2/21/20SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 2/23/20 2:01 EEHg/L0.14 2/21/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 2/23/20 2:01 EEHg/L10 2/21/20SM21-22 6200B1Vinyl Acetate
ND 0.50 2/23/20 2:01 EEHg/L0.45 2/21/20SM21-22 6200B1Vinyl Chloride
ND 1.0 2/23/20 2:01 EEHg/L0.30 2/21/20SM21-22 6200B1m+p Xylene
ND 0.50 2/23/20 2:01 EEHg/L0.17 2/21/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 88.6 2/23/20 2:0170-130
Toluene-d8 97.8 2/23/20 2:0170-130
4-Bromofluorobenzene 93.8 2/23/20 2:0170-130
Page 17 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-06
Field Sample #: MW-1R
Sample Matrix: Ground Water
Sampled: 2/18/2020 12:52
[TOC_2]20B0870-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 2000 2/25/20 8:49 EEHg/L150 2/24/20SM21-22 6200B40Acetone
970 20 2/25/20 8:49 EEHg/L7.2 2/24/20SM21-22 6200B40Benzene
ND 20 2/25/20 8:49 EEHg/L6.0 2/24/20SM21-22 6200B40Bromobenzene
ND 20 2/25/20 8:49 EEHg/L13 2/24/20SM21-22 6200B40Bromochloromethane
ND 20 2/25/20 8:49 EEHg/L6.4 2/24/20SM21-22 6200B40Bromodichloromethane
ND 20 2/25/20 8:49 EEHg/L18 2/24/20SM21-22 6200B40Bromoform
ND 40 2/25/20 8:49 EEHg/L31 2/24/20SM21-22 6200B40Bromomethane
ND 200 2/25/20 8:49 EEHg/L78 2/24/20SM21-22 6200B402-Butanone (MEK)
9.2 20 2/25/20 8:49 EEHg/L8.4 2/24/20SM21-22 6200B40Jn-Butylbenzene
ND 20 2/25/20 8:49 EEHg/L6.4 2/24/20SM21-22 6200B40sec-Butylbenzene
ND 20 2/25/20 8:49 EEHg/L6.8 2/24/20SM21-22 6200B40tert-Butylbenzene
ND 20 2/25/20 8:49 EEHg/L4.4 2/24/20SM21-22 6200B40Carbon Tetrachloride
ND 20 2/25/20 8:49 EEHg/L6.0 2/24/20SM21-22 6200B40Chlorobenzene
ND 2000 2/25/20 8:49 EEHg/L420 2/24/20SM21-22 6200B40Ethanol
ND 20 2/25/20 8:49 EEHg/L8.4 2/24/20SM21-22 6200B40Chlorodibromomethane
ND 20 2/25/20 8:49 EEHg/L14 2/24/20SM21-22 6200B40Chloroethane
ND 20 2/25/20 8:49 EEHg/L6.8 2/24/20SM21-22 6200B40Chloroform
ND 40 2/25/20 8:49 EEHg/L18 2/24/20SM21-22 6200B40Chloromethane
ND 20 2/25/20 8:49 EEHg/L4.8 2/24/20SM21-22 6200B402-Chlorotoluene
ND 20 2/25/20 8:49 EEHg/L5.6 2/24/20SM21-22 6200B404-Chlorotoluene
38 20 2/25/20 8:49 EEHg/L7.6 2/24/20SM21-22 6200B401,2-Dibromoethane (EDB)
ND 20 2/25/20 8:49 EEHg/L6.4 2/24/20SM21-22 6200B401,2-Dichlorobenzene
ND 20 2/25/20 8:49 EEHg/L4.8 2/24/20SM21-22 6200B401,3-Dichlorobenzene
ND 20 2/25/20 8:49 EEHg/L5.2 2/24/20SM21-22 6200B401,4-Dichlorobenzene
ND 20 2/25/20 8:49 EEHg/L10 2/24/20SM21-22 6200B40Dichlorodifluoromethane (Freon 12)
ND 20 2/25/20 8:49 EEHg/L6.4 2/24/20SM21-22 6200B401,1-Dichloroethane
ND 40 2/25/20 8:49 EEHg/L16 2/24/20SM21-22 6200B401,2-Dichloroethane
ND 20 2/25/20 8:49 EEHg/L13 2/24/20SM21-22 6200B401,1-Dichloroethylene
ND 20 2/25/20 8:49 EEHg/L5.2 2/24/20SM21-22 6200B40cis-1,2-Dichloroethylene
ND 20 2/25/20 8:49 EEHg/L12 2/24/20SM21-22 6200B40trans-1,2-Dichloroethylene
ND 20 2/25/20 8:49 EEHg/L8.0 2/24/20SM21-22 6200B401,2-Dichloropropane
ND 20 2/25/20 8:49 EEHg/L4.4 2/24/20SM21-22 6200B401,3-Dichloropropane
ND 20 2/25/20 8:49 EEHg/L8.0 2/24/20SM21-22 6200B402,2-Dichloropropane
ND 20 2/25/20 8:49 EEHg/L6.4 2/24/20SM21-22 6200B401,1-Dichloropropene
ND 20 2/25/20 8:49 EEHg/L5.2 2/24/20SM21-22 6200B40cis-1,3-Dichloropropene
ND 20 2/25/20 8:49 EEHg/L9.2 2/24/20SM21-22 6200B40trans-1,3-Dichloropropene
28 20 2/25/20 8:49 EEHg/L6.8 2/24/20SM21-22 6200B40Diisopropyl Ether (DIPE)
230 20 2/25/20 8:49 EEHg/L5.2 2/24/20SM21-22 6200B40Ethylbenzene
ND 200 2/25/20 8:49 EEHg/L61 2/24/20SM21-22 6200B402-Hexanone (MBK)
12 20 2/25/20 8:49 EEHg/L6.8 2/24/20SM21-22 6200B40JIsopropylbenzene (Cumene)
ND 20 2/25/20 8:49 EEHg/L8.0 2/24/20SM21-22 6200B40p-Isopropyltoluene (p-Cymene)
34 20 2/25/20 8:49 EEHg/L10 2/24/20SM21-22 6200B40L-04Methyl tert-Butyl Ether (MTBE)
ND 200 2/25/20 8:49 EEHg/L14 2/24/20SM21-22 6200B40Methylene Chloride
ND 200 2/25/20 8:49 EEHg/L67 2/24/20SM21-22 6200B404-Methyl-2-pentanone (MIBK)
Page 18 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-06
Field Sample #: MW-1R
Sample Matrix: Ground Water
Sampled: 2/18/2020 12:52
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
360 200 2/25/20 8:49 EEHg/L12 2/24/20SM21-22 6200B40Naphthalene
20 20 2/25/20 8:49 EEHg/L5.2 2/24/20SM21-22 6200B40n-Propylbenzene
6.0 20 2/25/20 8:49 EEHg/L4.4 2/24/20SM21-22 6200B40JStyrene
ND 20 2/25/20 8:49 EEHg/L8.8 2/24/20SM21-22 6200B401,1,2,2-Tetrachloroethane
ND 20 2/25/20 8:49 EEHg/L7.2 2/24/20SM21-22 6200B40Tetrachloroethylene
2500 20 2/25/20 8:49 EEHg/L5.6 2/24/20SM21-22 6200B40Toluene
ND 80 2/25/20 8:49 EEHg/L23 2/24/20SM21-22 6200B401,2,3-Trichlorobenzene
ND 20 2/25/20 8:49 EEHg/L16 2/24/20SM21-22 6200B401,2,4-Trichlorobenzene
ND 20 2/25/20 8:49 EEHg/L8.0 2/24/20SM21-22 6200B401,1,1-Trichloroethane
ND 20 2/25/20 8:49 EEHg/L6.4 2/24/20SM21-22 6200B401,1,2-Trichloroethane
ND 20 2/25/20 8:49 EEHg/L9.6 2/24/20SM21-22 6200B40Trichloroethylene
ND 20 2/25/20 8:49 EEHg/L13 2/24/20SM21-22 6200B40Trichlorofluoromethane (Freon 11)
ND 20 2/25/20 8:49 EEHg/L10 2/24/20SM21-22 6200B401,2,3-Trichloropropane
460 20 2/25/20 8:49 EEHg/L7.2 2/24/20SM21-22 6200B401,2,4-Trimethylbenzene
220 20 2/25/20 8:49 EEHg/L5.6 2/24/20SM21-22 6200B401,3,5-Trimethylbenzene
ND 800 2/25/20 8:49 EEHg/L410 2/24/20SM21-22 6200B40Vinyl Acetate
ND 20 2/25/20 8:49 EEHg/L18 2/24/20SM21-22 6200B40Vinyl Chloride
1700 40 2/25/20 8:49 EEHg/L12 2/24/20SM21-22 6200B40m+p Xylene
950 20 2/25/20 8:49 EEHg/L6.8 2/24/20SM21-22 6200B40o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 88.5 2/25/20 8:4970-130
Toluene-d8 98.5 2/25/20 8:4970-130
4-Bromofluorobenzene 97.4 2/25/20 8:4970-130
Page 19 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-07
Field Sample #: MW-12
Sample Matrix: Ground Water
Sampled: 2/18/2020 13:00
[TOC_2]20B0870-07[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 2500 2/23/20 4:55 EEHg/L190 2/21/20SM21-22 6200B50Acetone
1700 25 2/23/20 4:55 EEHg/L9.0 2/21/20SM21-22 6200B50Benzene
ND 25 2/23/20 4:55 EEHg/L7.5 2/21/20SM21-22 6200B50Bromobenzene
ND 25 2/23/20 4:55 EEHg/L16 2/21/20SM21-22 6200B50Bromochloromethane
ND 25 2/23/20 4:55 EEHg/L8.0 2/21/20SM21-22 6200B50Bromodichloromethane
ND 25 2/23/20 4:55 EEHg/L23 2/21/20SM21-22 6200B50Bromoform
ND 50 2/23/20 4:55 EEHg/L39 2/21/20SM21-22 6200B50Bromomethane
ND 250 2/23/20 4:55 EEHg/L97 2/21/20SM21-22 6200B502-Butanone (MEK)
16 25 2/23/20 4:55 EEHg/L10 2/21/20SM21-22 6200B50Jn-Butylbenzene
ND 25 2/23/20 4:55 EEHg/L8.0 2/21/20SM21-22 6200B50sec-Butylbenzene
ND 25 2/23/20 4:55 EEHg/L8.5 2/21/20SM21-22 6200B50tert-Butylbenzene
ND 25 2/23/20 4:55 EEHg/L5.5 2/21/20SM21-22 6200B50Carbon Tetrachloride
ND 25 2/23/20 4:55 EEHg/L7.5 2/21/20SM21-22 6200B50Chlorobenzene
ND 2500 2/23/20 4:55 EEHg/L530 2/21/20SM21-22 6200B50Ethanol
ND 25 2/23/20 4:55 EEHg/L10 2/21/20SM21-22 6200B50Chlorodibromomethane
ND 25 2/23/20 4:55 EEHg/L18 2/21/20SM21-22 6200B50Chloroethane
ND 25 2/23/20 4:55 EEHg/L8.5 2/21/20SM21-22 6200B50Chloroform
ND 50 2/23/20 4:55 EEHg/L22 2/21/20SM21-22 6200B50Chloromethane
ND 25 2/23/20 4:55 EEHg/L6.0 2/21/20SM21-22 6200B502-Chlorotoluene
ND 25 2/23/20 4:55 EEHg/L7.0 2/21/20SM21-22 6200B504-Chlorotoluene
ND 25 2/23/20 4:55 EEHg/L9.5 2/21/20SM21-22 6200B501,2-Dibromoethane (EDB)
ND 25 2/23/20 4:55 EEHg/L8.0 2/21/20SM21-22 6200B501,2-Dichlorobenzene
ND 25 2/23/20 4:55 EEHg/L6.0 2/21/20SM21-22 6200B501,3-Dichlorobenzene
ND 25 2/23/20 4:55 EEHg/L6.5 2/21/20SM21-22 6200B501,4-Dichlorobenzene
ND 25 2/23/20 4:55 EEHg/L13 2/21/20SM21-22 6200B50Dichlorodifluoromethane (Freon 12)
ND 25 2/23/20 4:55 EEHg/L8.0 2/21/20SM21-22 6200B501,1-Dichloroethane
120 50 2/23/20 4:55 EEHg/L20 2/21/20SM21-22 6200B501,2-Dichloroethane
ND 25 2/23/20 4:55 EEHg/L16 2/21/20SM21-22 6200B501,1-Dichloroethylene
ND 25 2/23/20 4:55 EEHg/L6.5 2/21/20SM21-22 6200B50cis-1,2-Dichloroethylene
ND 25 2/23/20 4:55 EEHg/L16 2/21/20SM21-22 6200B50trans-1,2-Dichloroethylene
ND 25 2/23/20 4:55 EEHg/L10 2/21/20SM21-22 6200B501,2-Dichloropropane
ND 25 2/23/20 4:55 EEHg/L5.5 2/21/20SM21-22 6200B501,3-Dichloropropane
ND 25 2/23/20 4:55 EEHg/L10 2/21/20SM21-22 6200B502,2-Dichloropropane
ND 25 2/23/20 4:55 EEHg/L8.0 2/21/20SM21-22 6200B501,1-Dichloropropene
ND 25 2/23/20 4:55 EEHg/L6.5 2/21/20SM21-22 6200B50cis-1,3-Dichloropropene
ND 25 2/23/20 4:55 EEHg/L12 2/21/20SM21-22 6200B50trans-1,3-Dichloropropene
150 25 2/23/20 4:55 EEHg/L8.5 2/21/20SM21-22 6200B50Diisopropyl Ether (DIPE)
1200 25 2/23/20 4:55 EEHg/L6.5 2/21/20SM21-22 6200B50Ethylbenzene
ND 250 2/23/20 4:55 EEHg/L76 2/21/20SM21-22 6200B502-Hexanone (MBK)
35 25 2/23/20 4:55 EEHg/L8.5 2/21/20SM21-22 6200B50Isopropylbenzene (Cumene)
ND 25 2/23/20 4:55 EEHg/L10 2/21/20SM21-22 6200B50p-Isopropyltoluene (p-Cymene)
290 25 2/23/20 4:55 EEHg/L12 2/21/20SM21-22 6200B50Methyl tert-Butyl Ether (MTBE)
ND 250 2/23/20 4:55 EEHg/L17 2/21/20SM21-22 6200B50Methylene Chloride
ND 250 2/23/20 4:55 EEHg/L84 2/21/20SM21-22 6200B504-Methyl-2-pentanone (MIBK)
Page 20 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-07
Field Sample #: MW-12
Sample Matrix: Ground Water
Sampled: 2/18/2020 13:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
500 250 2/23/20 4:55 EEHg/L16 2/21/20SM21-22 6200B50Naphthalene
86 25 2/23/20 4:55 EEHg/L6.5 2/21/20SM21-22 6200B50n-Propylbenzene
24 25 2/23/20 4:55 EEHg/L5.5 2/21/20SM21-22 6200B50JStyrene
ND 25 2/23/20 4:55 EEHg/L11 2/21/20SM21-22 6200B501,1,2,2-Tetrachloroethane
ND 25 2/23/20 4:55 EEHg/L9.0 2/21/20SM21-22 6200B50Tetrachloroethylene
3400 25 2/23/20 4:55 EEHg/L7.0 2/21/20SM21-22 6200B50Toluene
ND 100 2/23/20 4:55 EEHg/L28 2/21/20SM21-22 6200B501,2,3-Trichlorobenzene
ND 25 2/23/20 4:55 EEHg/L20 2/21/20SM21-22 6200B501,2,4-Trichlorobenzene
ND 25 2/23/20 4:55 EEHg/L10 2/21/20SM21-22 6200B501,1,1-Trichloroethane
ND 25 2/23/20 4:55 EEHg/L8.0 2/21/20SM21-22 6200B501,1,2-Trichloroethane
ND 25 2/23/20 4:55 EEHg/L12 2/21/20SM21-22 6200B50Trichloroethylene
ND 25 2/23/20 4:55 EEHg/L16 2/21/20SM21-22 6200B50Trichlorofluoromethane (Freon 11)
ND 25 2/23/20 4:55 EEHg/L12 2/21/20SM21-22 6200B501,2,3-Trichloropropane
1000 25 2/23/20 4:55 EEHg/L9.0 2/21/20SM21-22 6200B501,2,4-Trimethylbenzene
330 25 2/23/20 4:55 EEHg/L7.0 2/21/20SM21-22 6200B501,3,5-Trimethylbenzene
ND 1000 2/23/20 4:55 EEHg/L510 2/21/20SM21-22 6200B50Vinyl Acetate
ND 25 2/23/20 4:55 EEHg/L22 2/21/20SM21-22 6200B50Vinyl Chloride
5000 50 2/23/20 4:55 EEHg/L15 2/21/20SM21-22 6200B50m+p Xylene
2400 25 2/23/20 4:55 EEHg/L8.5 2/21/20SM21-22 6200B50o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 91.1 2/23/20 4:5570-130
Toluene-d8 97.7 2/23/20 4:5570-130
4-Bromofluorobenzene 96.8 2/23/20 4:5570-130
Page 21 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-08
Field Sample #: DW-1
Sample Matrix: Ground Water
Sampled: 2/18/2020 13:28
[TOC_2]20B0870-08[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 2/23/20 1:04 EEHg/L3.8 2/21/20SM21-22 6200B1Acetone
ND 0.50 2/23/20 1:04 EEHg/L0.18 2/21/20SM21-22 6200B1Benzene
ND 0.50 2/23/20 1:04 EEHg/L0.15 2/21/20SM21-22 6200B1Bromobenzene
ND 0.50 2/23/20 1:04 EEHg/L0.32 2/21/20SM21-22 6200B1Bromochloromethane
ND 0.50 2/23/20 1:04 EEHg/L0.16 2/21/20SM21-22 6200B1Bromodichloromethane
ND 0.50 2/23/20 1:04 EEHg/L0.46 2/21/20SM21-22 6200B1Bromoform
ND 1.0 2/23/20 1:04 EEHg/L0.78 2/21/20SM21-22 6200B1Bromomethane
ND 5.0 2/23/20 1:04 EEHg/L1.9 2/21/20SM21-22 6200B12-Butanone (MEK)
ND 0.50 2/23/20 1:04 EEHg/L0.21 2/21/20SM21-22 6200B1n-Butylbenzene
ND 0.50 2/23/20 1:04 EEHg/L0.16 2/21/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 2/23/20 1:04 EEHg/L0.17 2/21/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 2/23/20 1:04 EEHg/L0.11 2/21/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 2/23/20 1:04 EEHg/L0.15 2/21/20SM21-22 6200B1Chlorobenzene
ND 50 2/23/20 1:04 EEHg/L11 2/21/20SM21-22 6200B1Ethanol
ND 0.50 2/23/20 1:04 EEHg/L0.21 2/21/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 2/23/20 1:04 EEHg/L0.35 2/21/20SM21-22 6200B1Chloroethane
ND 0.50 2/23/20 1:04 EEHg/L0.17 2/21/20SM21-22 6200B1Chloroform
ND 1.0 2/23/20 1:04 EEHg/L0.45 2/21/20SM21-22 6200B1Chloromethane
ND 0.50 2/23/20 1:04 EEHg/L0.12 2/21/20SM21-22 6200B12-Chlorotoluene
ND 0.50 2/23/20 1:04 EEHg/L0.14 2/21/20SM21-22 6200B14-Chlorotoluene
ND 0.50 2/23/20 1:04 EEHg/L0.19 2/21/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 2/23/20 1:04 EEHg/L0.16 2/21/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 2/23/20 1:04 EEHg/L0.12 2/21/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 2/23/20 1:04 EEHg/L0.13 2/21/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 2/23/20 1:04 EEHg/L0.26 2/21/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 2/23/20 1:04 EEHg/L0.16 2/21/20SM21-22 6200B11,1-Dichloroethane
ND 1.0 2/23/20 1:04 EEHg/L0.41 2/21/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 2/23/20 1:04 EEHg/L0.32 2/21/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 2/23/20 1:04 EEHg/L0.13 2/21/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 2/23/20 1:04 EEHg/L0.31 2/21/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 2/23/20 1:04 EEHg/L0.20 2/21/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 2/23/20 1:04 EEHg/L0.11 2/21/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 2/23/20 1:04 EEHg/L0.20 2/21/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 2/23/20 1:04 EEHg/L0.16 2/21/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 2/23/20 1:04 EEHg/L0.13 2/21/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 2/23/20 1:04 EEHg/L0.23 2/21/20SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 2/23/20 1:04 EEHg/L0.17 2/21/20SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 2/23/20 1:04 EEHg/L0.13 2/21/20SM21-22 6200B1Ethylbenzene
ND 5.0 2/23/20 1:04 EEHg/L1.5 2/21/20SM21-22 6200B12-Hexanone (MBK)
ND 0.50 2/23/20 1:04 EEHg/L0.17 2/21/20SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 2/23/20 1:04 EEHg/L0.20 2/21/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 2/23/20 1:04 EEHg/L0.25 2/21/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 2/23/20 1:04 EEHg/L0.34 2/21/20SM21-22 6200B1Methylene Chloride
ND 5.0 2/23/20 1:04 EEHg/L1.7 2/21/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 22 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-08
Field Sample #: DW-1
Sample Matrix: Ground Water
Sampled: 2/18/2020 13:28
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 2/23/20 1:04 EEHg/L0.31 2/21/20SM21-22 6200B1Naphthalene
ND 0.50 2/23/20 1:04 EEHg/L0.13 2/21/20SM21-22 6200B1n-Propylbenzene
ND 0.50 2/23/20 1:04 EEHg/L0.11 2/21/20SM21-22 6200B1Styrene
ND 0.50 2/23/20 1:04 EEHg/L0.22 2/21/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 2/23/20 1:04 EEHg/L0.18 2/21/20SM21-22 6200B1Tetrachloroethylene
ND 0.50 2/23/20 1:04 EEHg/L0.14 2/21/20SM21-22 6200B1Toluene
ND 2.0 2/23/20 1:04 EEHg/L0.57 2/21/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 2/23/20 1:04 EEHg/L0.40 2/21/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 2/23/20 1:04 EEHg/L0.20 2/21/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 2/23/20 1:04 EEHg/L0.16 2/21/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 2/23/20 1:04 EEHg/L0.24 2/21/20SM21-22 6200B1Trichloroethylene
ND 0.50 2/23/20 1:04 EEHg/L0.33 2/21/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 2/23/20 1:04 EEHg/L0.25 2/21/20SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 2/23/20 1:04 EEHg/L0.18 2/21/20SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 2/23/20 1:04 EEHg/L0.14 2/21/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 2/23/20 1:04 EEHg/L10 2/21/20SM21-22 6200B1Vinyl Acetate
ND 0.50 2/23/20 1:04 EEHg/L0.45 2/21/20SM21-22 6200B1Vinyl Chloride
ND 1.0 2/23/20 1:04 EEHg/L0.30 2/21/20SM21-22 6200B1m+p Xylene
ND 0.50 2/23/20 1:04 EEHg/L0.17 2/21/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 90.8 2/23/20 1:0470-130
Toluene-d8 99.1 2/23/20 1:0470-130
4-Bromofluorobenzene 95.0 2/23/20 1:0470-130
Page 23 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-09
Field Sample #: WSW-1
Sample Matrix: Ground Water
Sampled: 2/18/2020 15:00
[TOC_2]20B0870-09[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 2/22/20 21:12 EEHg/L3.8 2/21/20SM21-22 6200B1Acetone
ND 0.50 2/22/20 21:12 EEHg/L0.18 2/21/20SM21-22 6200B1Benzene
ND 0.50 2/22/20 21:12 EEHg/L0.15 2/21/20SM21-22 6200B1Bromobenzene
ND 0.50 2/22/20 21:12 EEHg/L0.32 2/21/20SM21-22 6200B1Bromochloromethane
ND 0.50 2/22/20 21:12 EEHg/L0.16 2/21/20SM21-22 6200B1Bromodichloromethane
ND 0.50 2/22/20 21:12 EEHg/L0.46 2/21/20SM21-22 6200B1Bromoform
ND 1.0 2/22/20 21:12 EEHg/L0.78 2/21/20SM21-22 6200B1Bromomethane
ND 5.0 2/22/20 21:12 EEHg/L1.9 2/21/20SM21-22 6200B12-Butanone (MEK)
ND 0.50 2/22/20 21:12 EEHg/L0.21 2/21/20SM21-22 6200B1n-Butylbenzene
ND 0.50 2/22/20 21:12 EEHg/L0.16 2/21/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 2/22/20 21:12 EEHg/L0.17 2/21/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 2/22/20 21:12 EEHg/L0.11 2/21/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 2/22/20 21:12 EEHg/L0.15 2/21/20SM21-22 6200B1Chlorobenzene
ND 50 2/22/20 21:12 EEHg/L11 2/21/20SM21-22 6200B1Ethanol
ND 0.50 2/22/20 21:12 EEHg/L0.21 2/21/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 2/22/20 21:12 EEHg/L0.35 2/21/20SM21-22 6200B1Chloroethane
0.38 0.50 2/22/20 21:12 EEHg/L0.17 2/21/20SM21-22 6200B1JChloroform
ND 1.0 2/22/20 21:12 EEHg/L0.45 2/21/20SM21-22 6200B1Chloromethane
ND 0.50 2/22/20 21:12 EEHg/L0.12 2/21/20SM21-22 6200B12-Chlorotoluene
ND 0.50 2/22/20 21:12 EEHg/L0.14 2/21/20SM21-22 6200B14-Chlorotoluene
ND 0.50 2/22/20 21:12 EEHg/L0.19 2/21/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 2/22/20 21:12 EEHg/L0.16 2/21/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 2/22/20 21:12 EEHg/L0.12 2/21/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 2/22/20 21:12 EEHg/L0.13 2/21/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 2/22/20 21:12 EEHg/L0.26 2/21/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 2/22/20 21:12 EEHg/L0.16 2/21/20SM21-22 6200B11,1-Dichloroethane
ND 1.0 2/22/20 21:12 EEHg/L0.41 2/21/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 2/22/20 21:12 EEHg/L0.32 2/21/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 2/22/20 21:12 EEHg/L0.13 2/21/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 2/22/20 21:12 EEHg/L0.31 2/21/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 2/22/20 21:12 EEHg/L0.20 2/21/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 2/22/20 21:12 EEHg/L0.11 2/21/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 2/22/20 21:12 EEHg/L0.20 2/21/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 2/22/20 21:12 EEHg/L0.16 2/21/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 2/22/20 21:12 EEHg/L0.13 2/21/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 2/22/20 21:12 EEHg/L0.23 2/21/20SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 2/22/20 21:12 EEHg/L0.17 2/21/20SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 2/22/20 21:12 EEHg/L0.13 2/21/20SM21-22 6200B1Ethylbenzene
ND 5.0 2/22/20 21:12 EEHg/L1.5 2/21/20SM21-22 6200B12-Hexanone (MBK)
ND 0.50 2/22/20 21:12 EEHg/L0.17 2/21/20SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 2/22/20 21:12 EEHg/L0.20 2/21/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 2/22/20 21:12 EEHg/L0.25 2/21/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 2/22/20 21:12 EEHg/L0.34 2/21/20SM21-22 6200B1Methylene Chloride
ND 5.0 2/22/20 21:12 EEHg/L1.7 2/21/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 24 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-09
Field Sample #: WSW-1
Sample Matrix: Ground Water
Sampled: 2/18/2020 15:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 2/22/20 21:12 EEHg/L0.31 2/21/20SM21-22 6200B1Naphthalene
ND 0.50 2/22/20 21:12 EEHg/L0.13 2/21/20SM21-22 6200B1n-Propylbenzene
ND 0.50 2/22/20 21:12 EEHg/L0.11 2/21/20SM21-22 6200B1Styrene
ND 0.50 2/22/20 21:12 EEHg/L0.22 2/21/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 2/22/20 21:12 EEHg/L0.18 2/21/20SM21-22 6200B1Tetrachloroethylene
ND 0.50 2/22/20 21:12 EEHg/L0.14 2/21/20SM21-22 6200B1Toluene
ND 2.0 2/22/20 21:12 EEHg/L0.57 2/21/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 2/22/20 21:12 EEHg/L0.40 2/21/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 2/22/20 21:12 EEHg/L0.20 2/21/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 2/22/20 21:12 EEHg/L0.16 2/21/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 2/22/20 21:12 EEHg/L0.24 2/21/20SM21-22 6200B1Trichloroethylene
ND 0.50 2/22/20 21:12 EEHg/L0.33 2/21/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 2/22/20 21:12 EEHg/L0.25 2/21/20SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 2/22/20 21:12 EEHg/L0.18 2/21/20SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 2/22/20 21:12 EEHg/L0.14 2/21/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 2/22/20 21:12 EEHg/L10 2/21/20SM21-22 6200B1Vinyl Acetate
ND 0.50 2/22/20 21:12 EEHg/L0.45 2/21/20SM21-22 6200B1Vinyl Chloride
ND 1.0 2/22/20 21:12 EEHg/L0.30 2/21/20SM21-22 6200B1m+p Xylene
ND 0.50 2/22/20 21:12 EEHg/L0.17 2/21/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 91.4 2/22/20 21:1270-130
Toluene-d8 98.7 2/22/20 21:1270-130
4-Bromofluorobenzene 95.2 2/22/20 21:1270-130
Page 25 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-10
Field Sample #: WSW-2
Sample Matrix: Ground Water
Sampled: 2/18/2020 15:19
[TOC_2]20B0870-10[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 2/22/20 22:10 EEHg/L3.8 2/21/20SM21-22 6200B1Acetone
ND 0.50 2/22/20 22:10 EEHg/L0.18 2/21/20SM21-22 6200B1Benzene
ND 0.50 2/22/20 22:10 EEHg/L0.15 2/21/20SM21-22 6200B1Bromobenzene
ND 0.50 2/22/20 22:10 EEHg/L0.32 2/21/20SM21-22 6200B1Bromochloromethane
ND 0.50 2/22/20 22:10 EEHg/L0.16 2/21/20SM21-22 6200B1Bromodichloromethane
ND 0.50 2/22/20 22:10 EEHg/L0.46 2/21/20SM21-22 6200B1Bromoform
ND 1.0 2/22/20 22:10 EEHg/L0.78 2/21/20SM21-22 6200B1Bromomethane
ND 5.0 2/22/20 22:10 EEHg/L1.9 2/21/20SM21-22 6200B12-Butanone (MEK)
ND 0.50 2/22/20 22:10 EEHg/L0.21 2/21/20SM21-22 6200B1n-Butylbenzene
ND 0.50 2/22/20 22:10 EEHg/L0.16 2/21/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 2/22/20 22:10 EEHg/L0.17 2/21/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 2/22/20 22:10 EEHg/L0.11 2/21/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 2/22/20 22:10 EEHg/L0.15 2/21/20SM21-22 6200B1Chlorobenzene
ND 50 2/22/20 22:10 EEHg/L11 2/21/20SM21-22 6200B1Ethanol
ND 0.50 2/22/20 22:10 EEHg/L0.21 2/21/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 2/22/20 22:10 EEHg/L0.35 2/21/20SM21-22 6200B1Chloroethane
ND 0.50 2/22/20 22:10 EEHg/L0.17 2/21/20SM21-22 6200B1Chloroform
ND 1.0 2/22/20 22:10 EEHg/L0.45 2/21/20SM21-22 6200B1Chloromethane
ND 0.50 2/22/20 22:10 EEHg/L0.12 2/21/20SM21-22 6200B12-Chlorotoluene
ND 0.50 2/22/20 22:10 EEHg/L0.14 2/21/20SM21-22 6200B14-Chlorotoluene
ND 0.50 2/22/20 22:10 EEHg/L0.19 2/21/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 2/22/20 22:10 EEHg/L0.16 2/21/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 2/22/20 22:10 EEHg/L0.12 2/21/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 2/22/20 22:10 EEHg/L0.13 2/21/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 2/22/20 22:10 EEHg/L0.26 2/21/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 2/22/20 22:10 EEHg/L0.16 2/21/20SM21-22 6200B11,1-Dichloroethane
ND 1.0 2/22/20 22:10 EEHg/L0.41 2/21/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 2/22/20 22:10 EEHg/L0.32 2/21/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 2/22/20 22:10 EEHg/L0.13 2/21/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 2/22/20 22:10 EEHg/L0.31 2/21/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 2/22/20 22:10 EEHg/L0.20 2/21/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 2/22/20 22:10 EEHg/L0.11 2/21/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 2/22/20 22:10 EEHg/L0.20 2/21/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 2/22/20 22:10 EEHg/L0.16 2/21/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 2/22/20 22:10 EEHg/L0.13 2/21/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 2/22/20 22:10 EEHg/L0.23 2/21/20SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 2/22/20 22:10 EEHg/L0.17 2/21/20SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 2/22/20 22:10 EEHg/L0.13 2/21/20SM21-22 6200B1Ethylbenzene
ND 5.0 2/22/20 22:10 EEHg/L1.5 2/21/20SM21-22 6200B12-Hexanone (MBK)
ND 0.50 2/22/20 22:10 EEHg/L0.17 2/21/20SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 2/22/20 22:10 EEHg/L0.20 2/21/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 2/22/20 22:10 EEHg/L0.25 2/21/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 2/22/20 22:10 EEHg/L0.34 2/21/20SM21-22 6200B1Methylene Chloride
ND 5.0 2/22/20 22:10 EEHg/L1.7 2/21/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 26 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-10
Field Sample #: WSW-2
Sample Matrix: Ground Water
Sampled: 2/18/2020 15:19
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 2/22/20 22:10 EEHg/L0.31 2/21/20SM21-22 6200B1Naphthalene
ND 0.50 2/22/20 22:10 EEHg/L0.13 2/21/20SM21-22 6200B1n-Propylbenzene
ND 0.50 2/22/20 22:10 EEHg/L0.11 2/21/20SM21-22 6200B1Styrene
ND 0.50 2/22/20 22:10 EEHg/L0.22 2/21/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 2/22/20 22:10 EEHg/L0.18 2/21/20SM21-22 6200B1Tetrachloroethylene
ND 0.50 2/22/20 22:10 EEHg/L0.14 2/21/20SM21-22 6200B1Toluene
ND 2.0 2/22/20 22:10 EEHg/L0.57 2/21/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 2/22/20 22:10 EEHg/L0.40 2/21/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 2/22/20 22:10 EEHg/L0.20 2/21/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 2/22/20 22:10 EEHg/L0.16 2/21/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 2/22/20 22:10 EEHg/L0.24 2/21/20SM21-22 6200B1Trichloroethylene
ND 0.50 2/22/20 22:10 EEHg/L0.33 2/21/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 2/22/20 22:10 EEHg/L0.25 2/21/20SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 2/22/20 22:10 EEHg/L0.18 2/21/20SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 2/22/20 22:10 EEHg/L0.14 2/21/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 2/22/20 22:10 EEHg/L10 2/21/20SM21-22 6200B1Vinyl Acetate
ND 0.50 2/22/20 22:10 EEHg/L0.45 2/21/20SM21-22 6200B1Vinyl Chloride
ND 1.0 2/22/20 22:10 EEHg/L0.30 2/21/20SM21-22 6200B1m+p Xylene
ND 0.50 2/22/20 22:10 EEHg/L0.17 2/21/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 89.7 2/22/20 22:1070-130
Toluene-d8 98.1 2/22/20 22:1070-130
4-Bromofluorobenzene 93.6 2/22/20 22:1070-130
Page 27 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-11
Field Sample #: WSW-13
Sample Matrix: Ground Water
Sampled: 2/18/2020 15:30
[TOC_2]20B0870-11[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 2/22/20 21:41 EEHg/L3.8 2/21/20SM21-22 6200B1Acetone
ND 0.50 2/22/20 21:41 EEHg/L0.18 2/21/20SM21-22 6200B1Benzene
ND 0.50 2/22/20 21:41 EEHg/L0.15 2/21/20SM21-22 6200B1Bromobenzene
ND 0.50 2/22/20 21:41 EEHg/L0.32 2/21/20SM21-22 6200B1Bromochloromethane
ND 0.50 2/22/20 21:41 EEHg/L0.16 2/21/20SM21-22 6200B1Bromodichloromethane
ND 0.50 2/22/20 21:41 EEHg/L0.46 2/21/20SM21-22 6200B1Bromoform
ND 1.0 2/22/20 21:41 EEHg/L0.78 2/21/20SM21-22 6200B1Bromomethane
ND 5.0 2/22/20 21:41 EEHg/L1.9 2/21/20SM21-22 6200B12-Butanone (MEK)
ND 0.50 2/22/20 21:41 EEHg/L0.21 2/21/20SM21-22 6200B1n-Butylbenzene
ND 0.50 2/22/20 21:41 EEHg/L0.16 2/21/20SM21-22 6200B1sec-Butylbenzene
ND 0.50 2/22/20 21:41 EEHg/L0.17 2/21/20SM21-22 6200B1tert-Butylbenzene
ND 0.50 2/22/20 21:41 EEHg/L0.11 2/21/20SM21-22 6200B1Carbon Tetrachloride
ND 0.50 2/22/20 21:41 EEHg/L0.15 2/21/20SM21-22 6200B1Chlorobenzene
ND 50 2/22/20 21:41 EEHg/L11 2/21/20SM21-22 6200B1Ethanol
ND 0.50 2/22/20 21:41 EEHg/L0.21 2/21/20SM21-22 6200B1Chlorodibromomethane
ND 0.50 2/22/20 21:41 EEHg/L0.35 2/21/20SM21-22 6200B1Chloroethane
ND 0.50 2/22/20 21:41 EEHg/L0.17 2/21/20SM21-22 6200B1Chloroform
ND 1.0 2/22/20 21:41 EEHg/L0.45 2/21/20SM21-22 6200B1Chloromethane
ND 0.50 2/22/20 21:41 EEHg/L0.12 2/21/20SM21-22 6200B12-Chlorotoluene
ND 0.50 2/22/20 21:41 EEHg/L0.14 2/21/20SM21-22 6200B14-Chlorotoluene
ND 0.50 2/22/20 21:41 EEHg/L0.19 2/21/20SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 2/22/20 21:41 EEHg/L0.16 2/21/20SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 2/22/20 21:41 EEHg/L0.12 2/21/20SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 2/22/20 21:41 EEHg/L0.13 2/21/20SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 2/22/20 21:41 EEHg/L0.26 2/21/20SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 2/22/20 21:41 EEHg/L0.16 2/21/20SM21-22 6200B11,1-Dichloroethane
ND 1.0 2/22/20 21:41 EEHg/L0.41 2/21/20SM21-22 6200B11,2-Dichloroethane
ND 0.50 2/22/20 21:41 EEHg/L0.32 2/21/20SM21-22 6200B11,1-Dichloroethylene
ND 0.50 2/22/20 21:41 EEHg/L0.13 2/21/20SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 2/22/20 21:41 EEHg/L0.31 2/21/20SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 2/22/20 21:41 EEHg/L0.20 2/21/20SM21-22 6200B11,2-Dichloropropane
ND 0.50 2/22/20 21:41 EEHg/L0.11 2/21/20SM21-22 6200B11,3-Dichloropropane
ND 0.50 2/22/20 21:41 EEHg/L0.20 2/21/20SM21-22 6200B12,2-Dichloropropane
ND 0.50 2/22/20 21:41 EEHg/L0.16 2/21/20SM21-22 6200B11,1-Dichloropropene
ND 0.50 2/22/20 21:41 EEHg/L0.13 2/21/20SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 2/22/20 21:41 EEHg/L0.23 2/21/20SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 2/22/20 21:41 EEHg/L0.17 2/21/20SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 2/22/20 21:41 EEHg/L0.13 2/21/20SM21-22 6200B1Ethylbenzene
ND 5.0 2/22/20 21:41 EEHg/L1.5 2/21/20SM21-22 6200B12-Hexanone (MBK)
ND 0.50 2/22/20 21:41 EEHg/L0.17 2/21/20SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 2/22/20 21:41 EEHg/L0.20 2/21/20SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 2/22/20 21:41 EEHg/L0.25 2/21/20SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 2/22/20 21:41 EEHg/L0.34 2/21/20SM21-22 6200B1Methylene Chloride
ND 5.0 2/22/20 21:41 EEHg/L1.7 2/21/20SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 28 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 2/19/2020
Work Order: 20B0870Sample Description:Project Location: Middleburg, Vance County, NC
Sample ID: 20B0870-11
Field Sample #: WSW-13
Sample Matrix: Ground Water
Sampled: 2/18/2020 15:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 2/22/20 21:41 EEHg/L0.31 2/21/20SM21-22 6200B1Naphthalene
ND 0.50 2/22/20 21:41 EEHg/L0.13 2/21/20SM21-22 6200B1n-Propylbenzene
ND 0.50 2/22/20 21:41 EEHg/L0.11 2/21/20SM21-22 6200B1Styrene
ND 0.50 2/22/20 21:41 EEHg/L0.22 2/21/20SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 2/22/20 21:41 EEHg/L0.18 2/21/20SM21-22 6200B1Tetrachloroethylene
ND 0.50 2/22/20 21:41 EEHg/L0.14 2/21/20SM21-22 6200B1Toluene
ND 2.0 2/22/20 21:41 EEHg/L0.57 2/21/20SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 2/22/20 21:41 EEHg/L0.40 2/21/20SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 2/22/20 21:41 EEHg/L0.20 2/21/20SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 2/22/20 21:41 EEHg/L0.16 2/21/20SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 2/22/20 21:41 EEHg/L0.24 2/21/20SM21-22 6200B1Trichloroethylene
ND 0.50 2/22/20 21:41 EEHg/L0.33 2/21/20SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 2/22/20 21:41 EEHg/L0.25 2/21/20SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 2/22/20 21:41 EEHg/L0.18 2/21/20SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 2/22/20 21:41 EEHg/L0.14 2/21/20SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 2/22/20 21:41 EEHg/L10 2/21/20SM21-22 6200B1Vinyl Acetate
ND 0.50 2/22/20 21:41 EEHg/L0.45 2/21/20SM21-22 6200B1Vinyl Chloride
ND 1.0 2/22/20 21:41 EEHg/L0.30 2/21/20SM21-22 6200B1m+p Xylene
ND 0.50 2/22/20 21:41 EEHg/L0.17 2/21/20SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 90.3 2/22/20 21:4170-130
Toluene-d8 97.6 2/22/20 21:4170-130
4-Bromofluorobenzene 94.4 2/22/20 21:4170-130
Page 29 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B252791 02/21/205 5.0020B0870-01 [field blank]
B252791 02/21/205 5.0020B0870-02 [MW-6]
B252791 02/21/205 5.0020B0870-03 [MW-4R]
B252791 02/21/205 5.0020B0870-04 [MW-2R]
B252791 02/21/205 5.0020B0870-05 [MW-13]
B252791 02/21/200.1 5.0020B0870-07 [MW-12]
B252791 02/21/205 5.0020B0870-08 [DW-1]
B252791 02/21/205 5.0020B0870-09 [WSW-1]
B252791 02/21/205 5.0020B0870-10 [WSW-2]
B252791 02/21/205 5.0020B0870-11 [WSW-13]
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B252860 02/24/200.125 5.0020B0870-06 [MW-1R]
[TOC_1]Sample Preparation Information[TOC]
Page 30 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B252791 - SW-846 5030B
[TOC_3]B252791[TOC]
Blank (B252791-BLK1) Prepared: 02/21/20 Analyzed: 02/22/20
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
[TOC_1]QC Data[TOC]
Page 31 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B252791 - SW-846 5030B
Blank (B252791-BLK1) Prepared: 02/21/20 Analyzed: 02/22/20
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 90.422.6
g/L 25.0 70-130Surrogate: Toluene-d8 98.624.6
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 96.024.0
LCS (B252791-BS1) Prepared: 02/21/20 Analyzed: 02/22/20
Acetone g/L50 100 70-13085.585.5
Benzene g/L0.50 10.0 70-13088.38.83
Bromobenzene g/L0.50 10.0 70-13010110.1
Bromochloromethane g/L0.50 10.0 70-13095.79.57
Bromodichloromethane g/L0.50 10.0 70-13099.69.96
Bromoform g/L0.50 10.0 70-13097.89.78
Bromomethane g/L1.0 10.0 60-14010610.6
2-Butanone (MEK)g/L5.0 100 70-13080.180.1
n-Butylbenzene g/L0.50 10.0 70-13010910.9
sec-Butylbenzene g/L0.50 10.0 70-13011011.0
tert-Butylbenzene g/L0.50 10.0 70-13010910.9
Carbon Tetrachloride g/L0.50 10.0 70-13098.69.86
Chlorobenzene g/L0.50 10.0 70-13010510.5
Ethanol g/L50 100 L-0770-130132*132
Chlorodibromomethane g/L0.50 10.0 70-13096.09.60
Chloroethane g/L0.50 10.0 60-14093.69.36
Chloroform g/L0.50 10.0 70-13088.38.83
Chloromethane g/L0.60 10.0 60-14085.38.53
2-Chlorotoluene g/L0.50 10.0 70-13010010.0
4-Chlorotoluene g/L0.50 10.0 70-13010910.9
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13093.29.32
1,2-Dichlorobenzene g/L0.50 10.0 70-13010310.3
1,3-Dichlorobenzene g/L0.50 10.0 70-13010410.4
1,4-Dichlorobenzene g/L0.50 10.0 70-13010410.4
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14075.17.51
1,1-Dichloroethane g/L0.50 10.0 70-13090.49.04
1,2-Dichloroethane g/L0.50 10.0 70-13098.59.85
1,1-Dichloroethylene g/L0.50 10.0 70-13098.49.84
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13094.39.43
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13097.49.74
1,2-Dichloropropane g/L0.50 10.0 70-13097.19.71
1,3-Dichloropropane g/L0.50 10.0 70-13096.19.61
2,2-Dichloropropane g/L0.50 10.0 70-13080.28.02
1,1-Dichloropropene g/L0.50 10.0 70-13094.39.43
cis-1,3-Dichloropropene g/L0.50 10.0 70-13099.39.93
trans-1,3-Dichloropropene g/L0.50 10.0 70-13095.69.56
Page 32 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B252791 - SW-846 5030B
LCS (B252791-BS1) Prepared: 02/21/20 Analyzed: 02/22/20
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13098.69.86
Ethylbenzene g/L0.50 10.0 70-13010610.6
2-Hexanone (MBK)g/L5.0 100 70-13096.996.9
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13011011.0
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13010610.6
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13070.67.06
Methylene Chloride g/L5.0 10.0 70-13097.69.76
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-130102102
Naphthalene g/L0.50 10.0 70-13091.39.13
n-Propylbenzene g/L0.50 10.0 70-13010910.9
Styrene g/L0.50 10.0 70-13010510.5
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13097.79.77
Tetrachloroethylene g/L0.50 10.0 70-13010710.7
Toluene g/L0.50 10.0 70-13010110.1
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13092.49.24
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13098.09.80
1,1,1-Trichloroethane g/L0.50 10.0 70-13097.29.72
1,1,2-Trichloroethane g/L0.50 10.0 70-13094.89.48
Trichloroethylene g/L0.50 10.0 70-13099.89.98
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13097.69.76
1,2,3-Trichloropropane g/L0.50 10.0 70-13093.79.37
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13010410.4
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13010910.9
Vinyl Acetate g/L20 100 70-13083.683.6
Vinyl Chloride g/L0.50 10.0 L-0260-140216*21.6
m+p Xylene g/L1.0 20.0 70-13010821.6
o-Xylene g/L0.50 10.0 70-13010810.8
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 90.522.6
g/L 25.0 70-130Surrogate: Toluene-d8 95.423.8
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 96.224.0
LCS Dup (B252791-BSD1) Prepared: 02/21/20 Analyzed: 02/22/20
Acetone g/L50 100 2570-13092.4 7.8192.4
Benzene g/L0.50 10.0 2570-13089.6 1.468.96
Bromobenzene g/L0.50 10.0 2570-130104 3.2110.4
Bromochloromethane g/L0.50 10.0 2570-13099.0 3.399.90
Bromodichloromethane g/L0.50 10.0 2570-130108 8.0910.8
Bromoform g/L0.50 10.0 2570-130103 4.7910.3
Bromomethane g/L1.0 10.0 2560-140108 2.3410.8
2-Butanone (MEK)g/L5.0 100 2570-13086.2 7.3086.2
n-Butylbenzene g/L0.50 10.0 2570-130111 1.7311.1
sec-Butylbenzene g/L0.50 10.0 2570-130111 0.63111.1
tert-Butylbenzene g/L0.50 10.0 2570-130110 0.54911.0
Carbon Tetrachloride g/L0.50 10.0 2570-13099.0 0.4059.90
Chlorobenzene g/L0.50 10.0 2570-130106 0.76010.6
Ethanol g/L50 100 2570-130127 3.76127
Chlorodibromomethane g/L0.50 10.0 2570-130102 6.5510.2
Chloroethane g/L0.50 10.0 2560-14091.1 2.719.11
Chloroform g/L0.50 10.0 2570-13089.9 1.808.99
Chloromethane g/L0.60 10.0 2560-14087.1 2.098.71
2-Chlorotoluene g/L0.50 10.0 2570-13099.4 0.6029.94
4-Chlorotoluene g/L0.50 10.0 2570-130110 1.2811.0
Page 33 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B252791 - SW-846 5030B
LCS Dup (B252791-BSD1) Prepared: 02/21/20 Analyzed: 02/22/20
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130100 7.5410.0
1,2-Dichlorobenzene g/L0.50 10.0 2570-130106 2.9610.6
1,3-Dichlorobenzene g/L0.50 10.0 2570-130108 3.3910.8
1,4-Dichlorobenzene g/L0.50 10.0 2570-130106 1.8110.6
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14072.4 3.667.24
1,1-Dichloroethane g/L0.50 10.0 2570-13092.3 2.089.23
1,2-Dichloroethane g/L0.50 10.0 2570-130102 3.2010.2
1,1-Dichloroethylene g/L0.50 10.0 2570-13095.8 2.689.58
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13095.7 1.479.57
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13096.2 1.249.62
1,2-Dichloropropane g/L0.50 10.0 2570-13097.4 0.3089.74
1,3-Dichloropropane g/L0.50 10.0 2570-13098.6 2.579.86
2,2-Dichloropropane g/L0.50 10.0 2570-13080.3 0.1258.03
1,1-Dichloropropene g/L0.50 10.0 2570-13095.5 1.269.55
cis-1,3-Dichloropropene g/L0.50 10.0 2570-130101 1.7010.1
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13097.1 1.569.71
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130103 4.2710.3
Ethylbenzene g/L0.50 10.0 2570-130108 2.1510.8
2-Hexanone (MBK)g/L5.0 100 2570-130109 12.0109
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130113 2.6811.3
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130107 1.5010.7
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13076.6 8.157.66
Methylene Chloride g/L5.0 10.0 2570-13097.1 0.5149.71
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-130113 9.69113
Naphthalene g/L0.50 10.0 2570-130104 13.510.4
n-Propylbenzene g/L0.50 10.0 2570-130111 1.7211.1
Styrene g/L0.50 10.0 2570-130108 2.4510.8
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130105 7.1110.5
Tetrachloroethylene g/L0.50 10.0 2570-130110 2.3911.0
Toluene g/L0.50 10.0 2570-130102 1.3810.2
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-130113 20.411.3
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-130113 14.011.3
1,1,1-Trichloroethane g/L0.50 10.0 2570-13097.0 0.2069.70
1,1,2-Trichloroethane g/L0.50 10.0 2570-13098.1 3.429.81
Trichloroethylene g/L0.50 10.0 2570-13099.6 0.2019.96
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13095.0 2.709.50
1,2,3-Trichloropropane g/L0.50 10.0 2570-130103 9.6510.3
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130106 2.5710.6
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130111 1.9111.1
Vinyl Acetate g/L20 100 2570-13089.4 6.7489.4
Vinyl Chloride g/L0.50 10.0 25 L-0260-140213 1.31*21.3
m+p Xylene g/L1.0 20.0 2570-130110 2.0622.0
o-Xylene g/L0.50 10.0 2570-130112 3.0011.2
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 93.623.4
g/L 25.0 70-130Surrogate: Toluene-d8 98.024.5
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 98.324.6
Page 34 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B252860 - SW-846 5030B
[TOC_3]B252860[TOC]
Blank (B252860-BLK1) Prepared: 02/24/20 Analyzed: 02/25/20
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50 L-04ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
Page 35 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B252860 - SW-846 5030B
Blank (B252860-BLK1) Prepared: 02/24/20 Analyzed: 02/25/20
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 88.622.2
g/L 25.0 70-130Surrogate: Toluene-d8 96.624.2
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 90.122.5
LCS (B252860-BS1) Prepared & Analyzed: 02/24/20
Acetone g/L50 100 70-13085.785.7
Benzene g/L0.50 10.0 70-13080.48.04
Bromobenzene g/L0.50 10.0 70-13098.69.86
Bromochloromethane g/L0.50 10.0 70-13089.48.94
Bromodichloromethane g/L0.50 10.0 70-13095.99.59
Bromoform g/L0.50 10.0 70-13096.49.64
Bromomethane g/L1.0 10.0 60-14092.59.25
2-Butanone (MEK)g/L5.0 100 70-13080.480.4
n-Butylbenzene g/L0.50 10.0 70-13010110.1
sec-Butylbenzene g/L0.50 10.0 70-13010410.4
tert-Butylbenzene g/L0.50 10.0 70-13010510.5
Carbon Tetrachloride g/L0.50 10.0 70-13091.79.17
Chlorobenzene g/L0.50 10.0 70-13010110.1
Ethanol g/L50 100 70-130125125
Chlorodibromomethane g/L0.50 10.0 70-13095.49.54
Chloroethane g/L0.50 10.0 60-14081.78.17
Chloroform g/L0.50 10.0 70-13085.28.52
Chloromethane g/L0.60 10.0 60-14072.87.28
2-Chlorotoluene g/L0.50 10.0 70-13094.19.41
4-Chlorotoluene g/L0.50 10.0 70-13010310.3
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13093.99.39
1,2-Dichlorobenzene g/L0.50 10.0 70-13099.79.97
1,3-Dichlorobenzene g/L0.50 10.0 70-13099.89.98
1,4-Dichlorobenzene g/L0.50 10.0 70-13010110.1
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14065.26.52
1,1-Dichloroethane g/L0.50 10.0 70-13085.38.53
1,2-Dichloroethane g/L0.50 10.0 70-13094.29.42
1,1-Dichloroethylene g/L0.50 10.0 70-13087.88.78
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13089.18.91
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13085.78.57
1,2-Dichloropropane g/L0.50 10.0 70-13095.39.53
1,3-Dichloropropane g/L0.50 10.0 70-13095.79.57
2,2-Dichloropropane g/L0.50 10.0 70-13083.28.32
1,1-Dichloropropene g/L0.50 10.0 70-13086.88.68
cis-1,3-Dichloropropene g/L0.50 10.0 70-13096.89.68
trans-1,3-Dichloropropene g/L0.50 10.0 70-13093.19.31
Page 36 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B252860 - SW-846 5030B
LCS (B252860-BS1) Prepared & Analyzed: 02/24/20
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13096.59.65
Ethylbenzene g/L0.50 10.0 70-13010310.3
2-Hexanone (MBK)g/L5.0 100 70-13099.999.9
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13010810.8
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13099.79.97
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 L-0470-13067.2 *6.72
Methylene Chloride g/L5.0 10.0 70-13093.09.30
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-130104104
Naphthalene g/L0.50 10.0 70-13093.09.30
n-Propylbenzene g/L0.50 10.0 70-13010410.4
Styrene g/L0.50 10.0 70-13010110.1
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13098.99.89
Tetrachloroethylene g/L0.50 10.0 70-13010110.1
Toluene g/L0.50 10.0 70-13094.79.47
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13096.59.65
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13095.99.59
1,1,1-Trichloroethane g/L0.50 10.0 70-13093.49.34
1,1,2-Trichloroethane g/L0.50 10.0 70-13092.39.23
Trichloroethylene g/L0.50 10.0 70-13091.79.17
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13088.78.87
1,2,3-Trichloropropane g/L0.50 10.0 70-13093.99.39
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13098.09.80
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13010310.3
Vinyl Acetate g/L20 100 70-13078.178.1
Vinyl Chloride g/L0.50 10.0 L-0260-140168*16.8
m+p Xylene g/L1.0 20.0 70-13010320.6
o-Xylene g/L0.50 10.0 70-13010510.5
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 88.922.2
g/L 25.0 70-130Surrogate: Toluene-d8 97.824.4
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 98.324.6
LCS Dup (B252860-BSD1) Prepared & Analyzed: 02/24/20
Acetone g/L50 100 2570-13082.3 4.1282.3
Benzene g/L0.50 10.0 2570-13079.4 1.257.94
Bromobenzene g/L0.50 10.0 2570-13097.6 1.029.76
Bromochloromethane g/L0.50 10.0 2570-13088.3 1.248.83
Bromodichloromethane g/L0.50 10.0 2570-13094.1 1.899.41
Bromoform g/L0.50 10.0 2570-13095.2 1.259.52
Bromomethane g/L1.0 10.0 2560-14079.0 15.77.90
2-Butanone (MEK)g/L5.0 100 2570-13073.2 9.4373.2
n-Butylbenzene g/L0.50 10.0 2570-130100 1.2910.0
sec-Butylbenzene g/L0.50 10.0 2570-130104 0.48110.4
tert-Butylbenzene g/L0.50 10.0 2570-130104 0.76610.4
Carbon Tetrachloride g/L0.50 10.0 2570-13090.6 1.219.06
Chlorobenzene g/L0.50 10.0 2570-130101 0.0010.1
Ethanol g/L50 100 2570-130127 1.67127
Chlorodibromomethane g/L0.50 10.0 2570-13095.0 0.4209.50
Chloroethane g/L0.50 10.0 2560-14077.0 5.927.70
Chloroform g/L0.50 10.0 2570-13082.9 2.748.29
Chloromethane g/L0.60 10.0 2560-14065.8 10.16.58
2-Chlorotoluene g/L0.50 10.0 2570-13092.0 2.269.20
4-Chlorotoluene g/L0.50 10.0 2570-130102 1.2710.2
Page 37 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B252860 - SW-846 5030B
LCS Dup (B252860-BSD1) Prepared & Analyzed: 02/24/20
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-13088.2 6.268.82
1,2-Dichlorobenzene g/L0.50 10.0 2570-13098.0 1.729.80
1,3-Dichlorobenzene g/L0.50 10.0 2570-13099.4 0.4029.94
1,4-Dichlorobenzene g/L0.50 10.0 2570-13099.8 1.209.98
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14062.7 3.916.27
1,1-Dichloroethane g/L0.50 10.0 2570-13084.6 0.8248.46
1,2-Dichloroethane g/L0.50 10.0 2570-13091.7 2.699.17
1,1-Dichloroethylene g/L0.50 10.0 2570-13085.6 2.548.56
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13086.7 2.738.67
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13083.8 2.248.38
1,2-Dichloropropane g/L0.50 10.0 2570-13092.8 2.669.28
1,3-Dichloropropane g/L0.50 10.0 2570-13090.8 5.259.08
2,2-Dichloropropane g/L0.50 10.0 2570-13082.1 1.338.21
1,1-Dichloropropene g/L0.50 10.0 2570-13084.9 2.218.49
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13093.0 4.009.30
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13087.8 5.868.78
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-13093.0 3.699.30
Ethylbenzene g/L0.50 10.0 2570-130100 3.3410.0
2-Hexanone (MBK)g/L5.0 100 2570-13093.4 6.7293.4
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130104 3.0210.4
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130101 1.2010.1
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 25 L-0470-13059.6 12.0*5.96
Methylene Chloride g/L5.0 10.0 2570-13088.6 4.858.86
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-13095.2 8.8995.2
Naphthalene g/L0.50 10.0 2570-13094.2 1.289.42
n-Propylbenzene g/L0.50 10.0 2570-130104 0.28910.4
Styrene g/L0.50 10.0 2570-130101 0.59510.1
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-13094.7 4.349.47
Tetrachloroethylene g/L0.50 10.0 2570-13097.3 3.839.73
Toluene g/L0.50 10.0 2570-13092.4 2.469.24
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-13098.9 2.469.89
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-130101 4.7810.1
1,1,1-Trichloroethane g/L0.50 10.0 2570-13091.4 2.169.14
1,1,2-Trichloroethane g/L0.50 10.0 2570-13088.2 4.548.82
Trichloroethylene g/L0.50 10.0 2570-13089.1 2.888.91
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13085.3 3.918.53
1,2,3-Trichloropropane g/L0.50 10.0 2570-13093.5 0.4279.35
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-13096.2 1.859.62
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130101 2.0610.1
Vinyl Acetate g/L20 100 2570-13074.8 4.2874.8
Vinyl Chloride g/L0.50 10.0 25 L-0260-140170 1.54*17.0
m+p Xylene g/L1.0 20.0 2570-130101 1.2720.3
o-Xylene g/L0.50 10.0 2570-130104 1.1510.4
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 91.622.9
g/L 25.0 70-130Surrogate: Toluene-d8 97.624.4
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 98.524.6
Page 38 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
FLAG/QUALIFIER SUMMARY
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits.
Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is
on the high side.
L-02
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Elevated reporting limit due to high concentration of target compounds.RL-11
[TOC_1]Flag/Qualifier Summary[TOC]
Page 39 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
[TOC_1]Certifications[TOC]
Page 40 of 45
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2022
M-MA100Massachusetts DEPMA 06/30/2020
PH-0567Connecticut Department of Publilc HealthCT 09/30/2021
10899 NELAPNew York State Department of HealthNY 04/1/2020
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2021
LAO00112Rhode Island Department of HealthRI 12/30/2020
652North Carolina Div. of Water QualityNC 12/31/2020
MA007 NELAPNew Jersey DEPNJ 06/30/2020
E871027 NELAPFlorida Department of HealthFL 06/30/2020
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2020
2011028State of MaineME 06/9/2021
460217Commonwealth of VirginiaVA 12/14/2020
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2020
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2020
25703North Carolina Department of HealthNC-DW 07/31/2020
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2020
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