RA-527_3327_CA_MRP_20200206_GWMR Final

WithersRavenel

Our People. Your Success. 
115 MacKenan Drive | Cary, NC 27511 
t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C‐0832 
Cary | Greensboro | Pittsboro | Raleigh | Wilmington

February 6, 2020 

State of North Carolina 
Department of Environmental Quality 
Federal & State Lead Program  
Division of Waste Management‐Underground Storage Tank Section   
1646 Mail Service Center 
Raleigh, North Carolina 27699‐1646 

Attn: Mr. Mark Petermann 

RE: SUBSEQUENT MONITORING REPORT 
Former Billy's Mini Mart 
3121 NC Highway 86 North 
Hillsborough, Orange County, North Carolina 
Groundwater Incident Number: 3327 
WR Project Number:  02170214.74 

Mr. Petermann: 

WithersRavenel, Inc. (WR) has completed this Subsequent Monitoring Report to document the 
groundwater sampling and site assessment activities described in our proposal number TA‐03 for 
the above referenced site, approved by the Federal & State Lead Program on December 11, 
2019, and change order 03A, approved by NCDEQ on January 30, 2020.  The enclosed report 
summarizes the results of recently completed activities at the facility.  

WR appreciates the opportunity to be of service to the Federal & State Lead Program.  Should 
you have any questions regarding the attached, please contact Matt James at (919) 469‐3340. 

Cordially, 
WithersRavenel
Kevin B. Buchanan G. Matthew James, PG 
Staff Environmental Scientist II Senior Geologist 

Former Billy's Mini Mart Incident # 3327 WR Project # 02140214.74
Subsequent Monitoring Report January 2020

TABLE OF CONTENTS 

A. SITE INFORMATION .................................................................................................. 1 
B. EXECUTIVE SUMMARY ............................................................................................. 2 
C. SITE HISTORY AND CHARACTERIZATION ............................................................... 5 
D. CURRENT ASSESSMENT INFORMATION ............................................................... 10 
E.  CONCLUSIONS AND RECOMMENDATIONS ......................................................... 13 

FIGURES 

Figure 1 General Location Map 
Figure 2 Site Map  
Figure 3 Groundwater Elevations ‐ December 2019 
Figure 4 Groundwater Analytical Results ‐ December 2019 
Figure 5 Groundwater Benzene Isoconcentration Map ‐ December 2019 
Figure 6 Groundwater Naphthalene Isoconcentration Map – December 2019 
Figure 7 Groundwater MTBE Isoconcentration Map – December 2019 
Figure 8 Groundwater Total BTEX Isoconcentration Map – December 2019 
Figure 9 Receptor Map with Supply Well Analytical Results Shown  

TABLES 

Table B‐1 Site History – UST/AST System and Other Release Information  
Table B‐4 Summary of Groundwater Analytical Results 
Table B‐5 Public & Private Water Supply Well Information 
Table B‐7 Monitoring and Remediation Well Construction Information 
Table B‐9 Current & Historical Groundwater Elevations and Free Product Thickness’ 

APPENDICES 

Appendix A Analytical Reports and Chains‐of‐Custody 
Appendix B  Field Notes  
Appendix C Site Photographs  
Appendix D General Standard Operating Procedures 

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B. EXECUTIVE SUMMARY 

1. Summary of Activities Associated with Current TA 

WithersRavenel, Inc. (WR) personnel gauged, purged and sampled monitoring wells MW‐1, MW‐
2R, MW‐3, MW‐4, MW‐5, MW‐6, MW‐7, MW‐8, MW‐9R, MW‐10R, MW‐11, MW‐12, MW‐13, 
MW‐14, MW‐15, MW‐16, MW‐17, DW‐1, DW‐2 and SRW‐1.  WR also gauged well RW‐3 to 
determine whether free product was present, but did not sample the well.  Following gauging 
and/or sampling of wells MW‐11, MW‐14 and RW‐3, Provectus® ORS™ Well Booms were 
emplaced in these wells.  WR personnel also purged and sampled supply wells WSW‐1, WSW‐2, 
WSW‐3, WSW‐4, WSW‐5 and WSW‐6 on December 30, 2019.   Based on the presence of 
targeted compounds in WSW‐1, WSW‐3 and WSW‐4, WR re‐mobilized to the site on January 
20, 2020 for the collection of new samples from these wells at the request of the NCDEQ 
Incident Manager for the site (Mark Petermann).   

2. Soil, Groundwater and Free Product Assessment Information 

Soils 
No soil samples were obtained from locations on the site in connection with this task 
authorization.  To date, assessment of soil impact at the site has not been performed to 
determine the extent of soil contamination exceeding Maximum Soil Contaminant 
Concentrations (MSCCs), however, the 1999 Comprehensive Site Assessment (CSA) completed 
by Stratus Environmental Services, LLP (Stratus) mapped the “approximate lateral extent of 
petroleum hydrocarbons in soil”.     

Groundwater 
Analytical data for groundwater samples collected from site monitoring wells during December 
2019 indicated the presence of one or more targeted compounds in samples from monitoring 
wells MW‐4, MW‐8, MW‐9R, MW‐10R, MW‐11, MW‐12, MW‐13, MW‐14, MW‐17, DW‐2 and 
SRW‐1.  One or more compounds detected in samples from MW‐4, MW‐8, MW‐9R, MW‐10R, 
MW‐11, MW‐12, MW‐13, MW‐14, MW‐17 and SRW‐1 were reported at concentrations 
exceeding their respective 2L Standards defined by NCAC Title 15A, Subchapter 02, Section 
.0202 (Water Quality Standards for Class GA Groundwater).  Benzene was reported at a 
concentration exceeding the Gross Contaminant Levels (GCL) for the compound in the samples 
obtained from MW‐9R and MW‐13.   

Based on measurements obtained on December 2019, groundwater flow could not be 
determined with any great level of certainty.  Flow near the southern portion of the site 
appeared to flow to the south, while flow at the middle and northern portion of the site 
appeared to trend to the west and north.  Previous interpretations of groundwater flow have 
generally trended to the south through the site, with some movement to the north on the 
northern part of the site.  This disparity could be due in part to the potential influence of the 
septic system and associated leach field on the site, located in the vicinity of MW‐2R and MW‐
16, or to fluctuations in general groundwater elevations at the location.   

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Free Product 
Free product has been measured in monitoring wells MW‐8, MW‐11, and SRW‐1 in past 
monitoring events.  No free product was measured in any of the site monitoring wells during the 
December 2019 monitoring event.   

3. Receptor Information 

WR performed a receptor survey at the site in September 2002.  Thirty water supply wells were 
identified within a 1,000‐foot (ft) radius of the release area, one of which (WSW‐1) is located in 
the northeast corner of the site.  Analytical data for past sampling of supply wells located in 
proximity to the release area have shown impact to wells WSW‐1, WSW‐2 and WSW‐4.  In past 
sampling events, chloroform has been reported in one or more samples obtained from WSW‐2 
and WSW‐4 at concentrations exceeding the 2L Standard for the compound.  In addition, MTBE 
was reported on one occasion in WSW‐4 at a level above the 2L Standard for the compound.  
Analytical data for supply well samples obtained from WSW‐1, WSW‐2, WSW‐3 and WSW‐4 in 
April 2017 showed chloroform present at concentrations beneath the 2L Standard for the 
compound.  Results of laboratory testing of samples obtained from supply wells WSW‐1, WSW‐
2, WSW‐3, WSW‐4, WSW‐5 and WSW‐6 in December 2018 showed bromodichloromethane in 
WSW‐1 at a concentration exceeding the 2L Standard for the compound.  Chloroform was 
reported in the samples from WSW‐1, WSW‐2 and WSW‐4, however, the level of the 
compound detected in these samples did not exceed the 2L Standard.     

Laboratory results for samples collected from supply wells WSW‐1, WSW‐2, WSW‐3, WSW‐4, 
WSW‐5 and WSW‐6 in December 2019 showed acetone in WSW‐1 and chloroform in wells 
WSW‐1, WSW‐3 and WSW‐4.  Levels of these compounds detected were beneath the 2L 
Standards for the chemicals.  At the request of NCDEQ, WR re‐sampled WSW‐1, WSW‐3 and 
WSW‐4 on January 20, 2020.  Results of SM6200B analysis of these samples showed 
chloroform present in samples from WSW‐3 and WSW‐4 at levels beneath the 2L Standard.  
Chloromethane was reported in each of the supply wells (WSW‐1, WSW‐3 and WSW‐4) at 
concentrations above the 2L Standard for the compound.   

As acetone is a common chemical associated with the cleaning of laboratory equipment WR 
believes its presence to be a laboratory artifact.  WR believes the presence of both chloroform 
and chloromethane in these wells to be artifacts relating to shock chlorination unrelated to the 
release at the site.    

The nearest surface water feature identified in proximity to the site is an un‐named pond located 
approx. 600 feet to the south/southwest of the site.  Municipal water is not available to the site 
or surrounding properties.  Private water supply well information is included in Table B‐5, and 
supply well locations are depicted on Figure 9.     

4. Remediation Activities 

UST and soil excavation activities were conducted at the site during December 1986.  Following 
assessment activities, a groundwater pump and treatment system was brought online in 1988 
and operated until at least 1999 at the location.  However, sometime after 1999, the system was 
taken offline.  In February 2013 a 96‐hour Mobile Multi‐Phase Extraction (MMPE) event was 
conducted at the site, during which 3,115 gallons (gal) of impacted groundwater were recovered 
and approx. 307.31 gal of volatile product were extracted.  No additional remedial activities have 
been performed at the site, with the exception of the placement of Provectus® ORS™ well 

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sleeves in MW‐11, MW‐14 and RW‐3 in December 2018 and the replacement of these well 
booms in December 2019.   

5. Recommendations 

Based on the assessment results and monitoring activities conducted at the site in association 
with this TA, WR recommends the following: 

 Continue performance of groundwater and supply well sampling to determine contaminant 
trends and ensure supply wells do not show impact. 
 Petition the NCDEQ‐UST Section, Permits and Inspections Branch for records (e.g., tightness 
testing and leak detection) for the USTs currently in use on the property. 
 Install two additional monitoring wells: one approx. 90 feet north‐northwest of MW‐12, and 
one approx. 80 feet east‐northeast of MW‐17, to determine the lateral extent of 2L Standard 
violations and evaluate the possibility for an un‐documented release on the northern portion 
of the site.   
 Complete soil and groundwater assessment through use of Membrane Interface Hydraulic 
Profiling (MiHPt) in conjunction with groundwater assessment focused on collection of data 
for determination of a suitable chemical amendment for remediation at the facility. 
 Should free product be identified during future monitoring at the site, as an interim remedial 
effort, perform a surfactant injection in and around the estimated area of free product 
impact, followed by an MMPE event. 
 Complete a Corrective Action Feasibility Study (CAFS) to address long‐term remediation of 
soil and groundwater at the facility   

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C. SITE HISTORY AND CHARACTERIZATION 

WR completed assessment and sampling activities between December 30, 2019 and January 20, 
2020 at the facility.  The following information summarizes the site history and characterization.   

1. UST Information 

Previous reports indicated a UST system was present at the site in the 1980s and 1990s which 
consisted of one 8,000‐gal and two 4,000‐gal gasoline USTs.  The 8,000‐gal and one of the 
4,000‐gal USTs and the associated dispenser island were located west of the building while the 
second 4,000‐gal UST was located on the north side of the existing building.  A release was 
discovered during November 1986 when Home Oil Company (UST owner) reported to NCDENR 
that 1,000 to 2,000‐gallons of gasoline were unaccounted for from the 4,000‐gal UST located 
west of the building.  As a result, this UST was replaced in December 1986.  A split in one of the 
welded seams of the tank was discovered during its removal.   

In October 2000, the two USTs located west of the building (the 8,000‐gal and the 4,000‐gal 
tanks) were closed by way of removal and replaced with a 10,000‐gal and a 6,000‐gal UST.  The 
replacement tanks were installed north of the building.  During the installation of these new 
USTs, the contractor noted the presence of an additional 4,000‐gal tank, which was left in place 
adjacent to the new UST pit.  NCDENR‐UST Section records indicate that this 4,000‐gal UST 
was closed in 2008.   

The location of the site imposed on the USGS Topographic Map for the vicinity is included as 
Figure 1.  Site improvements, including USTs and monitoring well locations are depicted on 
Figure 2.   

2.  Description of Release/General Assessment History 

The following summary of the assessment history is based on WR’s review of historical files for 
the subject incident: 

 A release of petroleum was discovered in 1986, when at least two of the USTs located on 
the property were removed and soil was excavated to 22 ft below land surface (bls).  A 
groundwater pump and treat system was later installed and began operation in 1988.  It is 
unclear when treatment system operations terminated at the location, but it was estimated 
to have been sometime after 1999.  Two water supply wells sampled in 1988 were found to 
be impacted by MTBE (Penland – 213 parts‐per‐billion or “ppb” and Bledsoe – 28 ppb).  
Supply wells sampled in 2002 indicated an MTBE concentration of 3 ppb in one well sampled 
(Gates).  A Comprehensive Site Assessment (CSA) was completed for the release in June 
1999, which recommended dual‐phase vacuum extraction at the site.  Pilot testing, that 
included SVE, step‐drawdown testing and pump testing for the completion of a Corrective 
Action Plan (CAP) was performed in August 1999.  Based on the 1999 CSA, municipal water 
is not available in the vicinity of the site and soil contamination had not been properly 
assessed.  Only one soil sample was collected from the vadose zone at the location, obtained 
during the installation of DW‐1, 
 WR performed a receptor survey in September of 2002 and determined the following: thirty 
supply wells were identified within 1,000 ft of the site; municipal water is not available to the 
site or surrounding properties; the nearest surface water feature is an un‐named pond 
located approx. 600 feet to the south/southwest of the site; the site and surrounding areas 

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are rural consisting of large lots used primarily for single‐family residential use, or remain 
undeveloped; and the land use at the site is small business retail, 
 WR collected groundwater samples from the existing monitoring/recovery wells at the site 
on June 1, 2004.  Based on the laboratory analytical report, petroleum compounds were 
detected at concentrations above 2L Standards in samples collected from monitoring wells 
MW‐1, MW‐4, MW‐6, MW‐8, MW‐9, MW‐10, RW‐3, DW‐2 and SRW‐1.  No supply wells 
were sampled during this groundwater sampling event.  Reduction of groundwater elevation 
data indicated that groundwater flow direction at the site was to the south/southeast with 
an approx. gradient of 0.04 ft/ft, 
 WR personnel were onsite on September 29, 2005 to collect groundwater samples from the 
existing monitoring/recovery wells at the location (MW‐1 through MW‐10, DMW‐1, DMW‐
2, RW‐3, SRW‐1 and SRW‐2).  Free phase product was detected in monitoring well MW‐8.  
Based on the laboratory analytical report, petroleum compounds were detected at 
concentrations above 2L Standards in samples collected from monitoring wells MW‐4, 
DMW‐1, DMW‐2, SRW‐1, and SRW‐2, 
 WR personnel were onsite on November 2 and 3, 2006 to collect groundwater samples from 
the existing monitoring/recovery wells at the site (MW‐1 through MW‐10, DMW‐1, DMW‐
2, RW‐3, and SRW‐1) and from six water supply wells located in the immediate vicinity of the 
site (Ken’s, Bledsoe, Page, Murray, Huskins, and Gates).  Free phase product was not 
detected in any of the monitoring wells during this sampling event.  Monitoring wells MW‐1, 
MW‐9, and MW‐10 were dry and not able to be sampled.  Based on the laboratory analytical 
report, petroleum compounds were detected at concentrations above 2L Standards in 
samples collected from monitoring wells MW‐4, MW‐8, RW‐3, DMW‐1, and SRW‐1.  No 
targeted compounds were detected above laboratory detection limits in the supply well 
samples,   
 WR personnel were onsite on November 4, 2008 to collect groundwater samples from the 
existing monitoring/recovery wells at the site (MW‐1 through MW‐10, DMW‐1, DMW‐2, 
RW‐3, and SRW‐1).  Free phase product was not detected in MW‐8 or SRW‐1 during this 
sampling event. WR personnel also collected groundwater samples from six water supply 
wells located in the immediate vicinity of the site (Ken’s, Bledsoe, Page, Murray, Huskins, and 
Gates). Groundwater analytical results showed petroleum compounds at concentrations 
above 2L Standards in samples collected from monitoring wells MW‐8, DMW‐1, and SRW‐1. 
The groundwater dissolved contaminant plume was determined to be delineated. No 
targeted compounds were detected in the supply wells that were sampled. Groundwater 
flow direction at the site was determined to be to the southeast, 
 Additional groundwater monitoring events were conducted on August 14, 2009, March 25, 
2010, November 8, 2011 and November 29, 2012. The results of the monitoring events 
indicate free product present in monitoring well MW‐8, at one time, at a thickness of 0.31 
feet.  Petroleum compounds were detected above the 2L standards in monitoring wells MW‐
4, MW‐10R, DMW‐1, SRW‐1, and SRW‐2. Analytical results of the water supply well 
samples indicated the presence of MTBE in samples collected from wells WSW‐1, WSW‐2, 
and WSW‐6 at concentrations below the 2L Standard,   
 An MMPE event was conducted for 96 hours in February 2013. At the conclusion of the 
event, 3,115 ‐gal of contaminated water and 307.31 ‐gal of volatilized product had been 
removed from monitoring well MW‐8,  
 WR completed a groundwater sampling event in November 2014.  Groundwater samples 
were collected from wells MW‐3, MW‐4, MW‐5, MW‐7, MW‐8, MW‐9R, MW‐10R, RW‐3, 
DW‐1, DW‐2, and SRW‐1.  Supply wells WSW‐1, WSW‐6 and WSW‐7 were also sampled.  
Free product was measured in monitoring well MW‐11 at a thickness of 0.01 ft.  Analytical 
results showed the presence of benzene in groundwater monitoring well MW‐9R at a 
concentration that exceeded its GCL.  Analytical results for groundwater samples collected 

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from monitoring wells DW‐1, MW‐4, MW‐8, MW‐9R, MW‐10R, and SRW‐1 showed one or 
more petroleum constituents at concentrations that exceeded their respective 2L standards. 
Analytical results for samples collected from MW‐3, MW‐5 and MW‐7 did not show VOCs at 
concentrations that exceeded their respective laboratory detection limits. Analytical results 
for samples collected from water supply wells WSW‐1, WSW‐6, and WSW‐7 did not show 
VOCs at concentrations that exceeded their respective laboratory detection limits,   
 In May 2015, WR installed monitoring wells MW‐12, MW‐13, MW‐14, MW‐15, MW‐16 and 
MW‐17 and performed a groundwater sampling event at the site.  Data for samples obtained 
in association with the sampling event showed one or more targeted compounds in samples 
from wells MW‐4, MW‐8, MW‐9R, MW‐10R, MW‐11, MW‐12, MW‐13, MW‐14, MW‐15, 
MW‐16, MW‐17, DW‐1, DW‐2, SRW‐1 and RW‐3.  One or more compounds identified in 
samples from MW‐4, MW‐8, MW‐9R, MW‐10R, MW‐11, MW‐12, MW‐13, MW‐14, MW‐
17, DW‐1, DW‐2, SRW‐1 and RW‐3 were reported at concentrations exceeding their 
respective 2L Standards.  Benzene was reported at concentrations exceeding the GCL for the 
compound in samples from MW‐9R and MW‐13, while ethylbenzene, naphthalene, n‐
propylbenzene, 1,2,4‐trimethylbenzene, 1,3,5‐trimethylbenzene and total xylenes were 
reported in the sample from MW‐11 at levels above their respective GCLs.  Dilution of the 
sample from MW‐11 implied that benzene may also have been present in the well at a level 
exceeding the GCL.  Based on measurements obtained during the May 2015 groundwater 
sampling event at the site, groundwater flow appeared to trend to the southeast through the 
site, and   
 In October 2015, WR personnel gauged free product levels within MW‐11 and MW‐14, and 
gauged, purged and sampled monitoring wells MW‐2R, MW‐3, MW‐4, MW‐5, MW‐6, MW‐
7, MW‐8, MW‐9R, MW‐10R, MW‐12, MW‐13, MW‐15, MW‐16, MW‐17, DW‐1, DW‐2 and 
SRW‐1.  WR personnel also purged and sampled supply wells WSW‐1, WSW‐2, WSW‐3, 
WSW‐4, WSW‐5 and WSW‐6 for VOC analysis. Analytical data for groundwater samples 
obtained from monitoring wells at the site indicated the presence of one or more targeted 
compounds in samples obtained from wells MW‐4, MW‐5, MW‐8, MW‐9R, MW‐10R, MW‐
12, MW‐13, MW‐17, DW‐1, DW‐2 and SRW‐1 at concentrations exceeding their respective 
2L Standards.  Benzene was reported at a concentration exceeding the GCL for the 
compound in the sample from MW‐9R.  The presence of free product in wells MW‐11 and 
MW‐14 also represents a GCL violation.   WR also obtained free product samples from 
monitoring well MW‐11 and the two active USTs (UST‐1 and UST‐2) located on the property 
for product identification “fingerprint” analyses.  Not accounting for possible degradation of 
select chemical compounds, initial results of fuels and free product testing showed no direct 
correlation between the UST samples and the free product sample obtained from MW‐11.  
Further laboratory interpretation of these data revealed that the fuels contained in USTs 1 
and 2 do not match the product within monitoring well MW‐11.  
 In April 2017, WR personnel gauged free product levels within MW‐11 and MW‐14, and 
gauged, purged and sampled monitoring wells MW‐1, MW‐2R, MW‐3, MW‐4, MW‐5, MW‐
6, MW‐7, MW‐8, MW‐9R, MW‐10R, MW‐12, MW‐13, MW‐15, MW‐16, MW‐17, DW‐1, 
DW‐2 and SRW‐1.  WR personnel also purged and sampled supply wells WSW‐1, WSW‐2, 
WSW‐3, WSW‐4, WSW‐5 and WSW‐6 for VOC analysis. Analytical data for groundwater 
samples obtained from monitoring wells at the site indicated the presence of one or more 
targeted compounds in samples obtained from wells MW‐4, MW‐5, MW‐8, MW‐9R, MW‐
10R, MW‐12, MW‐13, MW‐17, DW‐1, DW‐2 and SRW‐1 at concentrations exceeding their 
respective 2L Standards.  Benzene was reported at a concentration exceeding the GCL for 
the compound in the sample from MW‐9R.  The presence of free product in wells MW‐11 
and MW‐14 also represents a GCL violation. Analytical data for supply well samples obtained 
from WSW‐1, WSW‐2, WSW‐3 and WSW‐4 indicated the presence of chloroform in the 
samples at levels above the laboratory method detection limit (MDL) for SM6200B but 

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beneath the NC 2L Standard for the compound. There is no standard for chloroform listed by 
the US EPA Region IV Maximum Contaminant Levels (MCL), December 2009. Based on 
measurements obtained during the April 2017 groundwater sampling event at the site, 
groundwater flow appears to trend to the south and southeast through the location.   
 WR personnel completed a groundwater and supply well sampling event between November 
29 and December 18, 2018.  Analytical data for groundwater samples collected from 
monitoring wells in association with this event indicated the presence of one or more 
targeted compounds in samples obtained from wells MW‐8, MW‐9R, MW‐12, MW‐13, MW‐
17, DW‐2 and SRW‐1 at concentrations exceeding their respective 2L Standards.  Benzene 
was reported at a concentration exceeding the GCL for the compound in the sample from 
MW‐13.  Free product was measured in wells MW‐11 (0.02 ft) and MW‐14 (0.01 ft).  
Analytical data for supply well samples showed bromodichloromethane present in the sample 
obtained from WSW‐1 at a concentration exceeding the 2L Standard.  Data for samples 
obtained from WSW‐1, WSW‐2 and WSW‐4 showed the presence of chloroform in the 
samples at levels above the laboratory method detection limit (MDL) for SM6200B but 
beneath the NC 2L Standard for the compound.  Analytical data for supply well samples 
obtained from WSW‐3, WSW‐5 and WSW‐6 did not indicate the presence of target 
compounds at levels above their MDLs for SM6200B.  

3.  Brief Description of Site Characteristics 

The site is located in Hillsborough, Orange County, North Carolina (Figure 1) and includes an 
area of approx. 1.6 acres.  The facility is located at 3121 NC Highway 86 and includes the 
following improvements: A one‐story brick/block building (the former Billy's Mini Mart) currently 
operating as Ken's Quickie Mart.  A wood‐framed addition is located at the rear of the building 
along the eastern wall.  Approximately 30% of the site surface is covered with asphalt or 
concrete.  Active UST systems are contained within a UST area located near the northeastern 
corner of the building on site.  These USTs supply dispensers are located beneath a canopy 
located near the northwestern corner of the building.  Potable water utilized on the site is 
obtained from a supply well located near the northeastern corner of the property (WSW‐1).  An 
additional (out of service) supply well is located southwest of the site building, between 
monitoring wells MW‐6 and MW‐8.  A septic system is located to the east of the site building.  
Site features, improvements and monitoring well locations are shown on Figure 2.  Site 
photographs are included in Appendix C.   

The surrounding area consists mainly of private residences and undeveloped properties.  
Carolane Propane Gas Company maintains a facility located to the north of the site, on the 
northern side of Phelps Road.  Municipal water is not currently available to the site or 
surrounding properties.   

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4.  Information on Receptors/Potential Receptors 

A receptor survey was performed in association with the release at the site by WR in September 
2002 and included the following findings: 

 Thirty water supply wells were identified within 1,000 ft of the site, 
 An un‐named surface water body (pond) is located approx. 600 feet south‐southwest of the 
site, 
 No public water supply was found to be available to the site or surrounding properties. 

Private water supply well information is included in Table B‐5, and well locations are depicted on 
Figure 9.     

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D. CURRENT ASSESSMENT INFORMATION 

On December 30, 2019, WR personnel mobilized to the facility to perform assessment and 
sampling activities in accordance with TA‐03 for the site, and returned to the site on January 20, 
2020 for the purposes of re‐sampling supply wells WSW‐1, WSW‐3 and WSW‐4.  Proposed 
activities included the following, which are described in subsequent sections: 

 Gauging of free product (if present) within select wells, 
 Gauging, purging and sampling of monitoring wells MW‐1, MW‐2R, MW‐3, MW‐4, MW‐5, 
MW‐6, MW‐7, MW‐8, MW‐9R, MW‐10R, MW‐11, MW‐12, MW‐13, MW‐14, MW‐15, 
MW‐16, MW‐17, DW‐1, DW‐2 and SRW‐1.   
 Collection of samples from six supply wells (WSW‐1, WSW‐2, WSW‐3, WSW‐4, WSW‐5 and 
WSW‐6, located in proximity to the site. 

1 Groundwater Elevations/Free Product Level Measurements 

Prior to the purging and sampling of site monitoring wells, as described below, WR personnel 
opened and gauged wells MW‐11, MW‐13 and RW‐2 with an electronic free product/water 
level indicator to determine whether measurable free product was present and determine the 
depth to groundwater within those wells.  Remaining wells were gauged with an electronic water 
level indicator.  In the performance of these activities, free product was not measured in any of 
the monitoring wells during the December 2019 event. Following gauging and/or sampling, 
Provectus® ORS™ well sleeved were left in place within these wells.   

The depth to groundwater measurements in the shallow (Type II) monitoring wells ranged from 
24.47 ft beneath top‐of‐casing (BTOC) in monitoring well MW‐15 to 32.00 ft‐BTOC in 
monitoring well MW‐6.  Based on measurements obtained in December 2019, groundwater flow 
could not be determined with any great level of certainty.  Previous interpretations of 
groundwater flow have generally trended to the south through the site, with some movement to 
the north on the northern part of the site.  This disparity could be due in part to the potential 
influence of the septic system and associated leach field on the site, located in the vicinity of 
MW‐2R and MW‐16, or to general fluctuations in groundwater elevations across the site.  On 
average, groundwater elevations within the surficial aquifer were 4.15 ft shallower than those 
measured in November 2018.  Groundwater elevations as determined based on December 2019 
measurements are shown on Figure 3.  Groundwater elevation measurement data for this event 
are presented in Table B‐7, while historical groundwater elevation measurements are included in 
Table B‐9.  Copies of field notes are included in Appendix B.   

2 Groundwater Sampling and Analytical Results 

Monitoring Well Sampling  

WR personnel obtained groundwater samples from monitoring wells MW‐1, MW‐2R, MW‐3, 
MW‐4, MW‐5, MW‐6, MW‐7, MW‐8, MW‐9R, MW‐10R, MW‐11, MW‐12, MW‐13, MW‐15, 
MW‐16, MW‐17, DW‐1, DW‐2 and SRW‐1 following gauging and purging.  Each well was 
purged utilizing dedicated disposable bailers as described in procedures outlined in Appendix D.   

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Following purging and recharge of each well, groundwater samples were decanted directly from 
the dedicated bailer(s) into laboratory‐prepared sample containers holding appropriate 
preservative(s) as required.  Groundwater samples were submitted to Waypoint Analytical 
Carolinas, Inc. (Waypoint), formerly Prism Laboratories, Inc. for analysis by SM6200B.  The 
laboratory analytical report and chain‐of‐custody record associated with these samples are 
included in Appendix A.  

Laboratory Results 

Analytical data for groundwater samples collected from monitoring wells at the site in December 
2019 indicated the presence of one or more targeted compounds in samples from monitoring 
wells MW‐4, MW‐8, MW‐9R, MW‐10R, MW‐11, MW‐12, MW‐13, MW‐14, MW‐17, DW‐2 and 
SRW‐1.  One or more compounds detected in samples from MW‐4, MW‐8, MW‐9R, MW‐10R, 
MW‐11, MW‐12, MW‐13, MW‐14, MW‐17 and SRW‐1 were reported at concentrations 
exceeding their respective 2L Standards.  Benzene was reported at a concentration exceeding 
the GCL for the compound in the samples obtained from MW‐9R and MW‐13.   

Based solely on total BTEX concentrations for groundwater samples from December 2019 in 
comparison to those from November/December 2019, increases in contaminants were indicated 
in nearly all of the monitoring wells sampled.  Changes in total BTEX concentrations at the 
location, whether increasing or decreasing, may relate to fluctuations in groundwater elevations 
at the site, although continued monitoring assists in mapping these trends.  On average, 
groundwater elevations within the surficial aquifer were 4.15 ft shallower than those measured 
in November 2019.  The changes in total BTEX over the November/December 2018 – 
December 2019 period are shown in the following table: 

Well ID Total BTEX 
November/December 2018 
Total BTEX 
December 2019 
Change Percent Change 
MW‐4 BDL 795 increase ‐100 
MW‐8 29.29 495.2 increase 1,590 
MW‐9R 382 15,300 increase 3,905 
MW‐10R 8.17 217.4 increase 2,560 
MW‐11 (Free Product) 6,465  ‐‐‐  ‐‐‐ 
MW‐12 250.77 190.57 decrease ‐24 
MW‐13 35,600 41,700 increase 17.1 
MW‐14 (Free Product) 45,200  ‐‐‐  ‐‐‐ 
MW‐17 1,030 5,492 increase 433 
SRW‐1 649.2 3,242 increase 399 

Data for groundwater samples analyzed in association with the present and previous TAs, there 
appear to be two separate areas of elevated impact on the property – one centered on the area 
of free product impact, and the second in the vicinity of monitoring well MW‐17, located 
upgradient of the free product source.  Based on current and historical gradient patterns at the 
site, co‐mingling of these plumes likely occurs near the northern portion of the building on the 
site.   

Groundwater analytical results are summarized in Table B‐4 and shown on Figure 4. 
Isoconcentration maps showing benzene, naphthalene, MTBE and total BTEX are included as 
Figures 5, 6, 7 and 8, respectively.   

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3 Water Supply Well Sampling and Analytical Results 

Supply Well Sampling (December 30, 2019)  

WR obtained supply well samples from wells WSW‐1, WSW‐2, WSW‐3, WSW‐4, WSW‐5 and 
WSW‐6 following purging.  The wells were purged for a minimum of ten minutes prior to the 
collection of samples.  After purging, samples were decanted directly from the sample port (e.g., 
spigot) used for purging into laboratory‐prepared sample containers holding appropriate 
preservatives (as required).  These samples were submitted to Waypoint for analysis by 
SM6200B.   

 Laboratory Results (December 30, 2019) 

Analytical data for supply well samples showed acetone present in the sample obtained from 
WSW‐1 at a concentration beneath the 2L Standard, and chloroform in samples from WSW‐1, 
WSW‐3 and WSW‐4, also at concentrations beneath the 2L Standard.  Results for remaining 
supply wells (WSW‐2, WSW‐5 and WSW‐6) did not indicate the presence of compounds 
targeted by SM6200B.  These results are included in Table B‐4.  The laboratory analytical report 
and chain‐of‐custody record associated with these samples are included in Appendix A.  
Locations of supply wells are shown on Figure 9.   

The presence of acetone in WSW‐1 is believed by WR to be a laboratory artifact associated with 
cleaning of laboratory apparatus.  Chloroform detected in the supply wells may be related to the 
shock chlorination of these wells. 

Supply Well Sampling (January 20, 2020)  

Based on data for wells WSW‐1, WSW‐3 and WSW‐4, the NCDEQ Incident Manager for the 
site (Mr. Mark Petermann) requested that WR re‐sample these wells.  WR returned to the site on 
January 20, 2020 and obtained supply well samples from wells WSW‐1, WSW‐3 and WSW‐4 
following purging.  The wells were purged for a minimum of ten minutes prior to the collection of 
samples.  After purging, samples were decanted directly from the sample port (e.g., spigot) used 
for purging into laboratory‐prepared sample containers holding appropriate preservatives (as 
required).  These samples were submitted to Waypoint for analysis by SM6200B.   

 Laboratory Results (January 20, 2020) 

Results of SM6200B analysis of these samples showed chloroform present in samples from 
WSW‐3 and WSW‐4 at levels beneath the 2L Standard.  Chloromethane was reported in each of 
the supply wells (WSW‐1, WSW‐3 and WSW‐4) at concentrations above the 2L Standard for the 
compound.  These results are included in Table B‐4.  The laboratory analytical report and chain‐
of‐custody record associated with these samples are included in Appendix A.  WR believes the 
presence of both chloroform and chloromethane in these wells to be artifacts relating to shock 
chlorination unrelated to the release at the site.    

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E.  CONCLUSIONS AND RECOMMENDATIONS 

This report documents the results of field activities conducted at the site between December 30, 
2019 and January 20, 2020.  Conclusions based on assessment and sampling activities, 
combined with analytical data historical information at the site include the following: 

 No public or private water supply system services the site or surrounding area, 
 As many as 30 water supply wells are located within 1,000 ft of the source area.  
 Analytical data for the supply well sample obtained from WSW‐1 showed acetone at a 
concentration beneath the 2L Standard for the compound.  WR believes the presence of the 
chemical in this sample to be a laboratory artifact.   
 Chloroform was shown present in samples from WSW‐1, WSW‐3 and WSW‐4 at 
concentrations beneath the 2L Standard.  WR attributes the presence of this chemical in the 
samples to shock chlorination of the supply wells. 
 Data for samples from supply wells WSW‐3, WSW‐5 and WSW‐6 did not show 
contaminants at concentrations exceeding the laboratory MDL for SM6200B. 
 Results for testing of samples from WSW‐1, WSW‐3 and WSW‐4 collected in January 2020 
showed chloroform present in samples from WSW‐3 and WSW‐4 at levels beneath the 2L 
Standard.  Chloromethane was reported in each of the supply wells (WSW‐1, WSW‐3 and 
WSW‐4) at concentrations above the 2L Standard for the compound.  WR believes the 
presence of both chloroform and chloromethane in these wells to be artifacts relating to 
shock chlorination unrelated to the release at the site.    
 Numerous wells located on the property contain contaminants at levels in excess of their 
respective 2L Standard(s).  
 Benzene was reported in the samples obtained from MW‐9R and MW‐13 at concentrations 
exceeding the GCL for the compound.  
 No free product was measured in any of the monitoring wells gauged in association with 
sampling in December 2019.   
 Based on current data, it appears that two distinct areas of impact exist on the site ‐ one 
centered on the area of historical free product impact and the other in the vicinity of MW‐
17, upgradient of the historical free product.  Co‐mingling of the plumes is likely occurring 
near the northern corner of the building on site.  The possibility exists that an on‐going and 
uncontrolled release is occurring from one or more of the "new" UST systems on the site.  
 The lateral and vertical extents of groundwater impact at the site have not been determined 
to levels equivalent to the 2L Standards. Elevated groundwater contaminants identified in 
wells MW‐12 and MW‐17 may be indicative of an un‐documented release on the northern 
portion of the site. 
 Fluctuations in contaminants are occurring at the site, and present data for total BTEX 
concentrations in monitoring wells suggest an increasing trend.  Changes in total BTEX 
concentrations at the location, whether increasing or decreasing, may relate to changes in 
groundwater elevations at the site, although continued monitoring assists in mapping trends.   
 Groundwater elevations for monitoring wells measured in December 2019 were, on average, 
4.15 ft shallower than those measured in November 2018.  The increase in total BTEX 
concentrations in site wells may relate to liberation of contaminants from soils which were 
not in direct contact with groundwater in November 2018.   
 Based on data for soil samples collected in association with assessment activities performed 
at the site to date, the extent of soil contamination at the site has not been defined to levels 
equivalent to the Soil‐to‐Water, Residential, or Industrial/Commercial MSCCs.  
 Based on groundwater level measurements conducted at the site during December 2019, 
groundwater flow could not be reliably discerned.  Previous data suggest overall trends to 
the southeast through the location.     

Former Billy's Mini Mart Incident # 3327 WR Project # 02170214.74 
Subsequent Monitoring Report  February 2020 
14

Based on the results of assessment and monitoring activities conducted at the site in association 
with this TA, WR recommends the following: 

 Continue performance of groundwater and supply well sampling to determine contaminant 
trends and ensure supply wells do not show impact. 
 Petition the NCDEQ‐UST Section, Permits and Inspections Branch for records (e.g., tightness 
testing and leak detection) for the USTs currently in use on the property. 
 Install two additional monitoring wells: one approx. 90 feet north‐northwest of MW‐12, and 
one approx. 80 feet east‐northeast of MW‐17, to determine the lateral extent of 2L Standard 
violations and evaluate the possibility for an un‐documented release on the northern portion 
of the site.   
 Complete soil and groundwater assessment through use of Membrane Interface Hydraulic 
Profiling (MiHPt) in conjunction with groundwater assessment focused on collection of data 
for determination of a suitable chemical amendment for remediation at the facility. 
 Should free product be identified during future monitoring at the site, as an interim remedial 
effort, perform a surfactant injection in and around the estimated area of free product 
impact, followed by an MMPE event. 
 Complete a Corrective Action Feasibility Study (CAFS) to address long‐term remediation of 
soil and groundwater at the facility   

FIGURES 

TABLES 
UST IDNumberCurrent/LastContentsPreviousContentsCapacity(in gallons)ConstructionDetailsTankDimensions (diameter x length) (ft)Description ofAssociatedPiping & PumpsDate of TankInstallationStatus ofUSTWas release associated with UST System? (Y/N)1 Gasoline Gasoline 10,000 Unknown Unknown Unknown 2000 Acitve Unknown2 Gasoline Gasoline 6,000 Unknown Unknown Unknown 2000 Active Unknown3 Unknown Unknown 4,000 Steel Unknown Unknown Unknown Closed (12/16/2008)1Unknown4 Gasoline Unknown 4,000 Steel Unknown Unknown UnknownClosed by removal (2000)Unknown5 Gasoline Unknown 8,000 Steel Unknown Unknown UnknownClosed by removal (2000)Unknown6 Unknown Unknown 4,000 Unknown Unknown Unknown UnknownClosed by removal (1986)UnknownAST IDNumberCurrent/LastContentsPreviousContentsCapacity(in gallons)ConstructionDetailsTankDimensions (diameter x length) (ft)Description ofAssociatedPiping & PumpsDate of TankInstallationStatus ofASTWas release associated with AST System? (Y/N)1 Kerosene Unknown Unknown Unknown Unknown Unknown Unknown Unknown Unknown2 Propane Unknown Unknown Unknown Unknown Unknown Unknown Unknown Unknown3 Unknown Unknown Unknown Unknown Unknown Unknown Unknown Unknown UnknownIncidentNumberMaterialReleasedDateofRelease3327 Gasoline 1986Notes:               1. = Per NCDEQ DWM‐UST Section records.  Table B‐1Site History:  UST/AST System & Other Release InformationBilly's Mini MartThe UST owners (Home Oil Company) notified NCDENR that the UST system located at the site lost between 1,000 and 2,000 gallons of gasoline.3121 NC Highway 86 Hillsborough, Orange County, NCIncident Number: 3327Description of ReleasePage 1 of 1
Calculated 504.1AcetoneBenzeneBromodichloromethanen‐Butylbenzenesec‐Butylbenzenetert‐ButylbenzeneChloroformChloromethane1,2‐DichloroethaneDi‐isopropyl etherEthylbenzene2‐HexanoneIsopropylbenzenep‐Isopropyltoluene2‐Butanone (MEK)4‐Methyl‐2‐pentanone (MIBK)Methyl tert‐butyl etherNaphthalenen‐PropylbenzeneStyreneToluene1,2,4‐Trimethylbenzene1,3,5‐TrimethylbenzeneTotal Xylenetert‐Amyl alcohol (TAA)tert‐Amyl Methyl Ether (TAME)*tert‐Butyl alcohol (tert‐butanol, TBA)*Ethylene Dibromide67‐64‐171‐43‐275‐27‐4 104‐51‐8 135‐98‐898‐06‐667‐66‐374‐87‐3 107‐06‐2 108‐20‐3 100‐41‐4 591‐78‐698‐82‐899‐87‐678‐93‐3 108‐10‐1 1634‐04‐491‐20‐3 103‐65‐1 100‐42‐5 108‐88‐395‐63‐6 108‐67‐8NA 75‐85‐4 994‐05‐875‐65‐0 106‐93‐411/8/2011ND900NR ND ND NA ND ND ND11 70NA5.1ND NA NA2300 22 8.3NA18 22 9.8 34.64NA NR NR NA11/29/2012ND140NR0.26 0.28ND0.16NR0.5 7.1 16NA1.3ND ND ND1100ND2.2ND1.6 5.3 0.5 4.2NA NR NR NA11/5/2014<5013<1.0 <1.0 <1.0 <1.0 <5.0 <2.5 <1.04.2<20 NA <1.0 <1.0 <10 <10910<5.0 <1.0 <1.0 <5.0 <20 <20 <40 NA13 210<0.010 5/5/2015<250 <5 <5 <5 <5 <5 <25 <12 <5 <5 <5 <50 <5 <5 <50 <50300<25 <5 <5 <25 <5 <5 <10 <250 <534NA10/13/2015<250 <5 <5 <5 <5 <5 <25 <12.5 <5 <5 <5 <50 <5 <5 <50 <50404<25 <5 <5 <25 <5 <5 <10 <250 <554.5NA4/19/2017<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <101.06<5 <1 <1 <1 <1 <1 <2 <50 <1 <5 NA12/18/2018<0.31 <0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 2.2<0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 <0.72 <0.10 <0.64 NA12/30/2019<0.31 <0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 <0.72 <0.10 <0.64 NA11/8/2011ND ND ND ND ND NA ND ND ND ND ND NA ND ND NA NA1.7ND ND ND ND ND ND ND NA NR NR NA11/29/2012ND ND ND ND ND ND0.18NR ND0.47ND NA ND ND ND ND3.8ND ND ND ND ND ND ND NA NR NR NA11/5/2014<50 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <2.5 <1.0 <1.0 <1.0 NA <1.0 <1.0 <10 <109.8<5.0 <1.0 <1.0 <5.0 <1.0 <1.0 <2.0 NA <1.0 <5.0 <0.010 5/5/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <1078<5 <1 <1 <5 <1 <1 <2 <501.2 10NA10/13/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <1026<5 <1 <1 <5 <1 <1 <2 <50 <1 <5 NA4/18/2017<50 <1 <1 <1 <1 <1 <5 <2.5 <10.384<1 <10 <1 <1 <10 <1045.6<5 <1 <1 <1 <1 <1 <2 <500.623 4.74NA12/18/2018<0.31 <0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 23<0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 <0.72 <10 <0.64 NA12/30/2019<10 <0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 23<0.054 <0.076 <0.15 <0.72 <0.10 <0.64 NA11/8/2011ND ND NR ND ND ND ND ND ND ND ND NA ND ND ND ND ND ND ND ND ND ND ND ND NA NR NR ND11/29/2012 5/06/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 <50 <1 <5 NA10/12/20154/18/201712/18/2018<0.31 <0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 <0.72 <0.10 <0.64 NA12/30/2019<10 <0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 <0.72 <0.10 <0.64 NA3/25/20104ND ND ND ND ND3.8NR ND ND ND NA ND ND ND ND ND ND ND ND ND ND ND ND NA NR NR ND 5/5/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 <50 <1 <5 NA10/12/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 <50 <1 <5 NA4/18/2017<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <1 <1 <1 <2 <50 <1 <5 NA12/18/2018<0.31 <0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 <0.72 <0.10 <0.64 NA12/30/2019<10 <0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 <0.72 <0.10 <0.64 NA11/8/2011ND ND ND ND ND ND ND ND ND ND ND NA ND ND ND ND0.32ND ND ND ND ND ND ND NA NR NR ND11/4/2014<50 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <2.5 <1.0 <1.0 <1.0 NA <1.0 <1.0 <10 <10 <1.0 <5.0 <1.0 <1.0 <5.0 <1.0 <1.0 <2.0 NA <1.0 <5.0 NA 5/5/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 <50 <1 <5 NA10/12/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 <50 <1 <5 NA4/18/2017<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <1 <1 <1 <2 <50 <1 <5 NA12/18/2018<0.31 <0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 <0.72 <0.10 <0.64 NA12/30/2019<0.31 <0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 <0.72 <0.10 <0.64 NA3/25/2010ND230NR6.7 5NA ND NR ND5.8 93NA37 3.3NA NA1100 110 88NA6 280 91 180.93NA NR NR NA11/8/2011ND40NR13 4.4 0.23 2.0NR ND5.1 29NA17 2.6ND ND600 48 43ND2 110 26 44.4NA NR NR NA11/5/2014<12002400<25 <25 <25 <25 <120 <62 <25 <25210NA <25 <25 <250 <2502000 140 25<25 <120470 180 677NA110 940<0.010 5/5/2015<12001000<25 <25 <25 <25 <120 <62 <25 <25200<25033<25 <250 <250950 210 86<25 <120660 260 429 1200<25310NA10/13/2015<501040<12.38 1.99<1 <5 <2.5 <110.7 108<1010.1 1.21<10 <101190 101 19.7<115.9 172 46.8 153.52 1140 21.9 254NA4/18/2017<50824<17.93 6.05<1 <5 <2.5 <113.5 127<1019.2 5.2<10 <101700 157 48.5<19.44 167 20.9 56.62 1640 26.9<250 NA12/18/2018<0.31 <0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 2.9<0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 <0.72 <0.10 <0.64 NA12/30/201935 560<0.062 21 11<0.50 <0.076 <0.079 <0.066 11 170<0.065 39 7.2<0.24 <0.078 980 210 77<0.047 11 79 36 54<0.72 24 310NA1/8/2011ND ND ND ND ND ND ND NR ND ND ND NA ND ND ND ND ND ND ND NA ND ND ND ND NA NR NR ND11/29/2012ND ND ND ND ND ND0.22NR ND ND ND NA ND ND ND ND ND ND ND ND ND ND ND ND NA NR NR ND11/4/2014<50 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <2.5 <1.0 <1.0 <1.0 NA <1.0 <1.0 <10 <10 <1.0 <5.0 <1.0 <1.0 <5.0 <1.0 <1.0 <2.0 NA <1.0 <5.0 NM 5/5/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 <50 <1 <5 NA10/13/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <16.06<1 <1 <5 <1 <1 <2 <50 <1 <5 NA4/19/2017<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <1 <1 <1 <2 <50 <1 <5 NA12/18/2018<0.31 <0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 <0.72 <0.10 <0.64 NA12/30/2019<0.31 <0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 <0.72 <0.10 <0.64 NA6,000 1 0.6 70 70 70 70 3 0.4 70 600 40 70 25 4000 100 20 6 70 70 600 400 400 500 40 128 10 0.026,000,000 5,000 NL 6,900 8,500 15,000 70,000 3,000 400 70,000 84,500 40,000 25,000 11,700 4,000,000 100,000 20,000 6,000 3,000 70,000 260,000 28,50025,000 85,500 40,000 12,800 10,000 50Notes:1)NLResult2)NAResult3)NRResult4)ND= Result Exceeds Laboratory Detec= Result Exceeds GCL ValueAll results provided in ug/L (micrograms per liter) or parts per billionNC 2L Standard ‐ North Carolina Groundwater Quality Standard as per NC Administrative Code 15A NCAC 02L .0202GCLs for Groundwater = NCDEQ UST Section Gross Contamination Levels for GroundwaterDateCollectedWell Not Sampled ‐ DryNC 2L Standard GCLs for GroundwaterSampleIDWell Not Sampled ‐ DryMW‐2Well Not Sampled ‐ DryMW‐4Analytical MethodTABLE B‐4SUMMARY OF GROUNDWATER ANALYTICAL RESULTSBilly's Mini MartIncident Number: 33273121 NC Highway 86 6200B ‐ Volatile Organic CompoundsHillsborough, Orange County, NC= Compound Not Detected.= Compound Not Reported By Previous Consultants= Compound Not Analyzed for by Laboratory.= Not Listed= Result Exceeds 2L StandardCompounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included  in the Appendix for a full list of constituents. DW‐1MW‐5MW‐3MW‐2RMW‐1DW‐2Page 1 of 4
Calculated 504.1AcetoneBenzeneBromodichloromethanen‐Butylbenzenesec‐Butylbenzenetert‐ButylbenzeneChloroformChloromethane1,2‐DichloroethaneDi‐isopropyl etherEthylbenzene2‐HexanoneIsopropylbenzenep‐Isopropyltoluene2‐Butanone (MEK)4‐Methyl‐2‐pentanone (MIBK)Methyl tert‐butyl etherNaphthalenen‐PropylbenzeneStyreneToluene1,2,4‐Trimethylbenzene1,3,5‐TrimethylbenzeneTotal Xylenetert‐Amyl alcohol (TAA)tert‐Amyl Methyl Ether (TAME)*tert‐Butyl alcohol (tert‐butanol, TBA)*Ethylene Dibromide67‐64‐171‐43‐275‐27‐4 104‐51‐8 135‐98‐898‐06‐667‐66‐374‐87‐3 107‐06‐2 108‐20‐3 100‐41‐4 591‐78‐698‐82‐899‐87‐678‐93‐3 108‐10‐1 1634‐04‐491‐20‐3 103‐65‐1 100‐42‐5 108‐88‐395‐63‐6 108‐67‐8NA 75‐85‐4 994‐05‐875‐65‐0 106‐93‐4DateCollectedSampleIDAnalytical MethodTABLE B‐4SUMMARY OF GROUNDWATER ANALYTICAL RESULTSBilly's Mini MartIncident Number: 33273121 NC Highway 86 6200B ‐ Volatile Organic CompoundsHillsborough, Orange County, NC3/25/2010ND ND ND ND ND ND ND ND ND ND ND NA ND ND ND ND ND ND ND NA ND ND ND ND NA NR NR ND1/8/2011ND ND ND ND ND ND ND ND ND ND ND NA ND ND ND ND ND ND ND NA ND ND ND ND NA NR NR ND11/29/2012ND ND ND ND ND ND0.26ND ND ND NA ND ND ND ND0.2 0.8 0.65ND ND4.2 2ND NA NR NR ND 5/06/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 <50 <1 <5 NA10/13/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 <50 <1 <5 NA4/18/2017<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <1 <1 <1 <2 <50 <1 <5 NA12/18/2018<0.31 <0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <1 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 <0.72 <0.10 <0.64 NA12/30/2019<0.31 <0.048 <0.062 <0.076 <0.076 <0.088 <0.50 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 <0.72 <0.10 <0.64 NA3/25/2010ND ND ND ND ND2.5ND ND ND NA ND ND ND ND ND ND ND NA ND ND ND ND NA NR NR ND11/4/2014<50 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <2.5 <1.0 <1.0 <1.0 NA <1.0 <1.0 <10 <10 <1.0 <5.0 <1.0 <1.0 <5.0 <1.0 <1.0 <2.0 NA <1.0 <5.0 NA 5/5/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 <50 <1 <5 NA10/13/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 <50 <1 <5 NA4/19/2017<50 <1 <1 <1 <1 <11.98<2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <1 <1 <1 <2 <50 <1 <5 NA12/18/2018<0.31 <0.048 <0.062 <0.076 <0.076 <0.088 3.3<0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 <0.72 <0.10 <0.64 NA12/30/2019<10 <0.048 <0.062 <0.076 <0.076 <0.088 3<0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <1 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 <0.72 <0.10 <0.64 NA3/25/2010ND700 130 37NA ND ND600NA97 56ND250 98 470 290NA630 2800 860 6800NA NR NR NA1/8/201111/29/201211/5/2014<5055<1.086 57 1.3<5.0 <2.5 <1.0 <1.0140NA170 34<10 <10 <1.0330 250<1.014 1200 560 970NA2<5.0 <0.010 5/06/2015<50340<127 15<1 <5 <2.5 <1 <1150<1067 21<1099<1320 150<172 1000 390 1890<500 <1 <5 NA10/12/2015<5076.6<117.1 7.78<1 <5 <2.5 <1 <152<1044.8 4.24<1010.8<1176 86.1<19.44 493 157 317.7<500 <10 <50 NA4/18/2017<5024.4<121.9 11.9<1 <5 <2.5 <1 <143<1050.8 25<10 <1012.4 133 162<13.03 541 288 213.83 32.9<15.29NA12/18/2018<0.31 2.4<0.062 23 12<0.088 <0.076 <0.079 <0.066 <0.050 15<0.065 31 5.1<0.24 <0.078 <0.042 29 89<0.047 0.89 75 130 11<0.72 <0.10 <0.64 NA12/30/2019<0.31 34<0.062 47 23 0.62<0.076 <0.079 <0.066 <0.050 68<0.065 78 12<0.24 <0.078 <0.042 180 180<0.047 3.2 850 340 390 47<0.10 <0.64 NA3/25/2010ND11000190ND NA ND ND89 3500NA140ND NA NA8400 710 260NA7500 2600 580 16300NA NR NR NA11/5/2014<25006600<50 <50 <50 <50 <250 <120 <5073 2600NA110<50 <500 <5006100 590 360<503500 2700 800 10500NA660 3100 0.091 5/06/2015<50006500<100 <100 <100 <100 <500 <250 <100 <1001800<1000 <100 <100 <1000 <10004400 540 220<1002200 1600 450 7100 6500<1001700NA10/12/2015<50006730<100 <100 <100 <100 <500 <250 <100 <1001380<1000 <100 <100 <1000 <10004080<500173<1001900 1120 312 5100 5320<100843NA4/18/2017<50005090<100 <100 <100 <100 <500 <250 <10054.2 1120<100047.7<100 <1000 <10003550 325 168<100956 869 263 3728 4000 58.4<500 NA12/18/2018<0.31 260<0.062 8.6 4.7<0.088 <0.076 <0.079 <0.066 20 62<0.065 13 5<0.24 <0.078 590 25 23<0.047 11 27 11 49<0.72 12 350NA12/30/2019<3.1 7200<0.62 23 11<0.88 <0.76 <0.79 <0.66 51 1900 25 70 6.8<2.4 93 3600 580 210<0.47 800 1400 370 5400 5500<100 <6.4 NA1/8/2011ND200 210 87NA ND ND ND ND2200NA290 66ND NA ND870 1000 73 1100 2900 1700 9000NA NR NR NA11/29/2012ND190 76 22ND ND ND ND ND1300NA100ND ND ND ND830 360 81 580 2600 700 4800NA NR NR NA11/5/2014<2500300<50 <50 <50 <50 <250 <120 <50 <50660NA77<50 <500 <50069 360 230<50 <2501600 490 2760NA <50 <250 <0.010 5/06/2015<2500430<50 <50 <50 <50 <250 <120 <50 <50640<50076<50 <500 <500390 800 210<50260 1700 590 2520 3100<50 <250 NA10/12/2015<5013.9<19.35 4.74<1 <5 <2.5 <1 <140.9<1012.8 2.39<10 <102.65 35.9 38.6<15.81 114 67.1 95.7 51.5<1 <5 NA4/18/2017<50038.9<16.19 3.87<1 <50 <25 <10 <10196<1023.8 8.42<10024 64.4 115 77.2 0.758 27 291 128 409.7 112<10 <50 NA12/18/2018<0.31 0.97<0.062 1.1 0.58<0.088 <0.076 <0.079 <0.066 <0.050 1.2<0.065 <0.054 <0.5 <0.24 <0.078 1.2<11.2<0.047 <0.044 6 3.8 6<0.72 <0.10 <0.64 NA12/30/201925 8.2<0.062 11 3.9<0.088 <0.076 <0.079 <0.066 <0.050 73<0.065 14 1.7<0.24 12 6.1 50 44<0.047 6.2 130 68 130<0.72 <0.10 <0.64 NA1/8/2011100 130 33ND NA ND ND ND1500NA47ND46NA39 33 140 48 1700 1100 270 8300NA NR NR NA11/29/201211/5/2014 5/06/2015<500000 <10000 <10000 <10000 <10000 <10000 <50000 <25000 <10000 <10000120000<100000 <10000 <10000 <100000 <100000 <1000017000040000<10000 <5000040000099000740000<500000 <10000 <50000 NA10/13/20154/18/201712/18/201812/30/2019<3.1 16<0.62 19 12<0.88 <0.76 <0.79 <0.66 <0.50 800 73 74 10<2.4 350 <0.42 1800 170<549 2900 840 5600<7.2 <1.0 <6.4 NA 5/07/2015<50180<13.6 5.6<1 <5 <2.5 <136 7.8<1010 10<10 <10980 160 5.8<1 <5140 29 156<500016 1800NA10/12/2015<5037.7<11.7 2.76<1 <5 <2.5 <13.5 2.83<105.55 2.31<10 <1094.8 137 3.4<1 <580.6 15 91.7<2501.01 94.7NA4/18/2017<5051<13.88 5.3<11.11<2.5 <15.73 0.51<108.57 14<10 <10135 166 1.26<10.469 118 20.9 106.6 367 2.08 314NA12/18/2018<0.31 120<0.062 3.8 4.9<0.51.4<0.079 <0.066 23<0.5 <0.065 7.4 5<0.24 <0.078 420 230 1.1<0.047 0.77 130 26 130<0.72 <101100NA12/30/2019<0.31 93<0.503.9 6<0.501.2<0.079 <0.066 11<0.50 <0.065 9.5 4.8<0.24 <0.078 250 1200 1.3<0.047 0.57 80 18 97 910<10660NA6,000 1 0.6 70 70 70 70 3 0.4 70 600 40 70 25 4000 100 20 6 70 70 600 400 400 500 40 128 10 0.026,000,000 5,000 NL 6,900 8,500 15,000 70,000 3,000 400 70,000 84,500 40,000 25,000 11,700 4,000,000 100,000 20,000 6,000 3,000 70,000 260,000 28,50025,000 85,500 40,000 12,800 10,000 50Notes:1)NLResult2)NAResult3)NRResult4)NDNot Sampled ‐ Free Product PresentWell Not Sampled ‐ Free Product PresentWell Not Sampled ‐ Free Product PresentWell Not Sampled ‐ Free Product PresentWell Not Sampled ‐ Free Product PresentWell Not Sampled ‐ DryMW‐12MW‐11MW‐10RNot Sampled ‐ Free Product PresentMW‐9RGCLs for GroundwaterAll results provided in ug/L (micrograms per liter) or parts per billion= Not Listed= Result Exceeds Laboratory DetecNC 2L Standard ‐ North Carolina Groundwater Quality Standard as per NC Administrative Code 15A NCAC 02L .0202= Compound Not Reported By Previous Consultants= Result Exceeds GCL ValueGCLs for Groundwater = NCDEQ UST Section Gross Contamination Levels for Groundwater= Compound Not Detected.Compounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included  in the Appendix for a full list of constituents. = Compound Not Analyzed for by Laboratory.= Result Exceeds 2L StandardMW‐8MW‐7MW‐6NC 2L Standard Page 2 of 4
Calculated 504.1AcetoneBenzeneBromodichloromethanen‐Butylbenzenesec‐Butylbenzenetert‐ButylbenzeneChloroformChloromethane1,2‐DichloroethaneDi‐isopropyl etherEthylbenzene2‐HexanoneIsopropylbenzenep‐Isopropyltoluene2‐Butanone (MEK)4‐Methyl‐2‐pentanone (MIBK)Methyl tert‐butyl etherNaphthalenen‐PropylbenzeneStyreneToluene1,2,4‐Trimethylbenzene1,3,5‐TrimethylbenzeneTotal Xylenetert‐Amyl alcohol (TAA)tert‐Amyl Methyl Ether (TAME)*tert‐Butyl alcohol (tert‐butanol, TBA)*Ethylene Dibromide67‐64‐171‐43‐275‐27‐4 104‐51‐8 135‐98‐898‐06‐667‐66‐374‐87‐3 107‐06‐2 108‐20‐3 100‐41‐4 591‐78‐698‐82‐899‐87‐678‐93‐3 108‐10‐1 1634‐04‐491‐20‐3 103‐65‐1 100‐42‐5 108‐88‐395‐63‐6 108‐67‐8NA 75‐85‐4 994‐05‐875‐65‐0 106‐93‐4DateCollectedSampleIDAnalytical MethodTABLE B‐4SUMMARY OF GROUNDWATER ANALYTICAL RESULTSBilly's Mini MartIncident Number: 33273121 NC Highway 86 6200B ‐ Volatile Organic CompoundsHillsborough, Orange County, NC 5/07/20159709200<1011<10 <10 <50 <25 <10 <103500 350 84 18 620 150 3400 660 250 84 29000 1800 460 17200<2500019 1000NA10/12/2015<2500697<50 <50 <50 <50 <250 <125 <50 <50829<500 <50 <50 <500 <500 <50616 76<502820 605 154 4380<2500 <50 <250 NA4/19/2017541 2930<5033.9<50 <50 <250 <125 <50 <504780 655 157 53.5<500252 165 1120 543<506710 3720 941 24270 1070<50599NA12/18/2018<3.1 5500<0.62 390 140<0.88 <0.76 <0.79 <0.66 <0.50 4200 630 380 72<2.4 430 1400 1400 65021 4900 4500 1200 21000<7.2 <0.10 <6.4 NA12/30/2019<10005400<6.2 <50 <50 <8.8 <7.6 <7.9 <6.6 <5.0 5300 1000 180<8.9 <24 430 550 1000 600<504000 4300 1100 27000 2400<10 <64 NA 5/07/2015<100004800<200 <200 <200 <200 <1000 <500 <200 <2002000<2000 <200 <200 <2000 <20004100<1000 <200 <20011000 1100 310 6800<10000210 1800NA10/12/20154/18/201712/18/201812/30/20195701,100 6 54 25<0.88 <0.76 <0.79 <0.66 18 4,100 370 150 11 400 170 230 1,600 470 84 18,000 3,600 920 22,000 1,500<100 <6.4 NA 5/07/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <51.1<14.4<50 <1 <5 NA10/12/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 <50 <1 <5 NA4/18/2017<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <1 <1 <1 <2 <50 <1 <5 NA12/18/2018<0.31 <0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 <0.72 <0.10 <0.64 NA12/30/2019<0.31 <0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 <0.72 <0.10 <0.64 NA 5/07/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <16.3<10 <1 <1 <10 <10 <1 <52.7<1 <512 4.1 31<50 <1 <5 NA10/12/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 <50 <1 <5 NA4/18/2017<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <1 <1 <1 <2 <50 <1 <5 NA12/18/2018<0.31 <0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 <0.72 <0.10 <0.64 NA12/30/2019<10 <0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <1 <0.087 <0.047 <0.044 <0.054 <0.076 <1.5 <0.72 <0.10 <0.64 NA 5/07/2015<2500980<50 <50 <50 <50 <250 <120 <50 <501900<500110<50 <500 <500260 470 350<50480 2500 660 10200<2500 <50 <250 NA10/12/2015<1250940<25 <25 <25 <25 <125 <62.5 <2544.3 570<25042.4<25 <250 <250244 198 127<25132 1050 274 3740 1900<25238NA4/18/2017<1250602<25137 44.8<25 <125 <62.5 <2526.8 597<250150 113<250 <250104 413 524<2572.4 3610 1020 5430 863<25399NA12/18/2018<3.1 31<0.62 120 47<0.88 <0.76 <0.79 <0.66 <0.50 64<0.65 52 24<2.4 <0.78 <0.42 180 180<0.47 5 1600 620 930<7.2 <1.0 <6.4 NA12/30/2019<3.1 550<0.62 130 50<0.88 <0.76 <0.79 <0.66 30 580<0.65 170 21<2.4 <0.78 80 470 570<0.47 62 2500 700 4300 1100<1.0 <6.4 NA3/25/2010ND2400 120ND NA ND ND ND ND1300NA70NA120 1400 410 140ND590 2400 710 9000NA NR NR NA1/8/2011ND3600 51 22NA ND ND ND ND1300NA110 37ND NA3200 590 290ND330 3900 3900 8000NA NR NR NA11/29/2012ND1000 120 22ND ND ND ND ND480NA48 24ND ND1300 850 130 24 120 2700 2700 3970NA NR NR NA11/4/2014<12001800<25 <25 <25 <25 <120 <62 <25 <25380NA <25 <25 <250 <2501600 210 44<25 <120840 380 1180NA31 660<0.010 5/06/2015<25002300<50 <50 <50 <50 <250 <120 <50 <50640<500 <50 <50 <500 <5001600 280 73<50 <2501200 520 2360<2500 <50 <250 NA10/12/2015<12501860<25 <25 <25 <25 <125 <62.5 <25 <25421<250 <25 <25 <250 <2501610 217 39.4<25 <125615 250 1126.4 1430<25363NA4/19/2017<25003060<50 <50 <50 <50 <250 <125 <5022.3 869<50041.7 28.5<500 <5002360 383 102<5098.3 1150 414 1449.3 2620 47 1310NA12/18/2018<0.31 310<0.062 2.3 1.3<0.088 <0.076 <0.079 <0.066 2.1 110<0.065 7.7 1.2<0.24 <0.078 180 62 20<0.047 9.2 190 67 220<0.72 <10 <0.64 NA12/30/2019<3.1 2000<0.62 12 7.9<0.88 <0.76 <0.79 <0.66 18 540<0.65 38 6.2<2.4 <0.78 1400 400 97<0.47 62 680 250 640 1800<100 <6.4 NA3/25/2010ND220ND ND ND ND ND ND11 100NA ND ND NA ND1200ND16ND ND92 31 205NA NR NR NA1/8/2011ND110 2.8 2.6ND ND ND ND14 71NA5.8 1.1ND NA3100 22 16ND1.6 58 13 76.8NA NR NR NA11/29/2012ND9 1.1 1.1ND ND ND ND12 11NA0.91ND ND ND1200 8.6 3.6 0.5 0.39 3.8 0.36 3.23NA NR NR NA12/18/201812/30/20193/25/2010NA0.52ND0.51NA ND ND ND ND43NA ND ND NA NA1400ND ND NA ND ND ND ND NA NR NR NA1/8/2011ND ND ND NA ND ND ND ND47NA ND ND ND NA2700ND ND ND ND ND ND ND NA NR NR NA11/29/201211/5/2014<1000 <20 <20 <20 <20 <20 <20 <2042<20 NA <20 <20 <20 <202200<20 <20 <20 <2027<20 <40 NA150 2100NA 5/06/2015<1000 <20 <20 <20 <20 <20 <100 <50 <2036<20 <200 <20 <20 <200 <2001700<100 <20 <20 <100 <20 <20 <40 <100094 1400NA12/18/201812/30/20196,000 1 0.6 70 70 70 70 3 0.4 70 600 40 70 25 4000 100 20 6 70 70 600 400 400 500 40 128 10 0.026,000,000 5,000 NL 6,900 8,500 15,000 70,000 3,000 400 70,000 84,500 40,000 25,000 11,700 4,000,000 100,000 20,000 6,000 3,000 70,000 260,000 28,50025,000 85,500 40,000 12,800 10,000 50Notes:1)NLResult2)NAResult3)NRResult4)NDMW‐14GCLs for GroundwaterAll results provided in ug/L (micrograms per liter) or parts per billionCompounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included  in the Appendix for a full list of constituents. GCLs for Groundwater = NCDEQ UST Section Gross Contamination Levels for GroundwaterNC 2L Standard ‐ North Carolina Groundwater Quality Standard as per NC Administrative Code 15A NCAC 02L .0202MW‐13Well Not Sampled ‐ Free Product PresentNot Sampled ‐ Free Product PresentWell Not Sampled ‐ DryNot Sampled Not Sampled Not Sampled Not Sampled Not Sampled ‐ Free Product Present= Compound Not Reported By Previous Consultants= Result Exceeds GCL Value= Not Listed= Result Exceeds Laboratory Detec= Compound Not Analyzed for by Laboratory.= Result Exceeds 2L Standard= Compound Not Detected.SRW‐2RW‐3SRW‐1MW‐17MW‐16MW‐15NC 2L Standard Page 3 of 4
Calculated 504.1AcetoneBenzeneBromodichloromethanen‐Butylbenzenesec‐Butylbenzenetert‐ButylbenzeneChloroformChloromethane1,2‐DichloroethaneDi‐isopropyl etherEthylbenzene2‐HexanoneIsopropylbenzenep‐Isopropyltoluene2‐Butanone (MEK)4‐Methyl‐2‐pentanone (MIBK)Methyl tert‐butyl etherNaphthalenen‐PropylbenzeneStyreneToluene1,2,4‐Trimethylbenzene1,3,5‐TrimethylbenzeneTotal Xylenetert‐Amyl alcohol (TAA)tert‐Amyl Methyl Ether (TAME)*tert‐Butyl alcohol (tert‐butanol, TBA)*Ethylene Dibromide67‐64‐171‐43‐275‐27‐4 104‐51‐8 135‐98‐898‐06‐667‐66‐374‐87‐3 107‐06‐2 108‐20‐3 100‐41‐4 591‐78‐698‐82‐899‐87‐678‐93‐3 108‐10‐1 1634‐04‐491‐20‐3 103‐65‐1 100‐42‐5 108‐88‐395‐63‐6 108‐67‐8NA 75‐85‐4 994‐05‐875‐65‐0 106‐93‐4DateCollectedSampleIDAnalytical MethodTABLE B‐4SUMMARY OF GROUNDWATER ANALYTICAL RESULTSBilly's Mini MartIncident Number: 33273121 NC Highway 86 6200B ‐ Volatile Organic CompoundsHillsborough, Orange County, NC1/8/2011ND ND ND ND NA ND1.3ND ND ND NA ND ND ND NA ND ND ND ND ND ND ND ND NA NR NR NA11/29/2012ND ND ND ND ND ND2.5ND ND ND NA ND ND ND ND0.85ND ND ND ND ND ND ND NA NR NR NA11/4/2014<50 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <2.5 <1.0 <1.0 <1.0 NA <1.0 <1.0 <10 <10 <1.0 <5.0 <1.0 <1.0 <5.0 <1.0 <1.0 <2.0 NA <1.0 <5.0 NA 5/5/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 NA <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 NA NA NA NA10/12/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 <50 <1 <5 NA4/19/2017<50 <1 <1 <1 <1 <10.807<2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <1 <1 <1 <2 <50 <1 <5 NA12/18/2018<10 <0.048 2.5<0.076 <0.076 <0.088 8.6<0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 NA NA NA NA12/30/201932<0.048 <0.062 <0.076 <0.076 <0.088 1.3<0.50 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 NA NA NA NA1/20/2020<0.31 <0.048 <0.062 <0.076 <0.076 <0.72 <0.076 17<0.066 <27 <0.061 <0.050 <0.054 <0.089 <0.065 <0.083 <0.042 <0.078 <0.19 <0.087 <0.10 <0.098 <0.062 <0.060 <0.044 <0.12 <0.12 NA1/8/201126ND ND ND NA NA0.81ND ND ND NA ND ND ND NA0.94ND ND ND ND ND ND ND NA NR NR NA11/29/2012ND ND ND ND ND ND97ND ND ND NA ND ND83ND0.77ND ND ND ND ND ND ND NA NR NR NA 5/5/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 NA <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 NA NA NA NA10/12/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 <50 <1 <5 NA4/19/2017<50 <1 <1 <1 <1 <10.64<2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <1 <1 <1 <2 <50 <1 <5 NA12/18/2018<10 <0.048 <0.062 <0.076 <0.076 <0.088 1.1<0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 NA NA NA NA12/30/2019<0.31 <0.048 <0.062 <0.076 <0.076 <0.088 <0.50 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 NA NA NA NA 5/6/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 NA <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 NA NA NA NA10/12/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 <50 <1 <5 NA4/19/2017<50 <1 <1 <1 <1 <10.656<2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <1 <1 <1 <2 <50 <1 <5 NA12/18/2018<10 <0.048 <0.062 <0.076 <0.076 <0.088 <0.5 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 NA NA NA NA12/30/2019<0.31 <0.048 <0.062 <0.076 <0.076 <0.088 1.2<0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 NA NA NA NA1/20/2020<0.31 <0.048 <0.062 <0.076 <0.076 <0.72 0.94 8.2<0.066 <27 <0.061 <0.050 <0.054 <0.089 <0.065 <0.083 <0.042 <0.078 <0.19 <0.087 <0.10 <0.098 <0.062 <0.060 <0.044 <0.12 <0.12 NA1/8/2011ND ND ND ND ND NA97ND26ND NA ND ND ND ND83ND ND ND ND ND ND0.94NA NR NR NA11/29/2012ND ND ND ND ND ND1.1ND ND ND NA ND ND ND ND ND ND ND ND ND ND ND ND NA NR NR NA 5/5/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 NA <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 NA NA NA NA10/12/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 <50 <1 <5 NA4/19/2017<50 <1 <1 <1 <1 <10.628<2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <1 <1 <1 <2 <50 <1 <5 NA12/18/2018<10 <0.048 <0.062 <0.076 <0.076 <0.088 0.87<0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 NA NA NA NA12/30/2019<10 <0.048 <0.062 <0.076 <0.076 <0.088 1.4<0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 NA NA NA NA1/20/2020<0.31 <0.048 <0.062 <0.076 <0.076 <0.72 1.4 7.9<0.066 <27 <0.061 <0.050 <0.054 <0.089 <0.065 <0.083 <0.042 <0.078 <0.19 <0.087 <0.10 <0.098 <0.062 <0.060 <0.044 <0.12 <0.12 NA 5/5/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 NA <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 NA NA NA NA10/12/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 <50 <1 <5 NA4/19/2017<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <1 <1 <1 <2 <50 <1 <5 NA12/18/2018<10 <0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 NA NA NA NA12/30/2019<10 <0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 NA NA NA NA1/8/2011ND ND ND ND NA NA ND ND ND ND NA ND ND ND NA ND ND ND ND ND ND ND ND NA NR NR NA11/29/2012ND ND ND ND ND ND0.37ND ND ND NA ND ND ND ND0.77ND ND ND ND ND ND ND NA NR NR NA11/4/2014<50 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <2.5 <1.0 <1.0 <1.0 NA <1.0 <1.0 <10 <10 <1.0 <5.0 <1.0 <1.0 <5.0 <1.0 <1.0 <2.0 NA <1.0 <5.0 NA 5/5/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 NA <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 NA NA NA NA10/12/2015<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <5 <1 <1 <2 <50 <1 <5 NA4/19/2017<50 <1 <1 <1 <1 <1 <5 <2.5 <1 <1 <1 <10 <1 <1 <10 <10 <1 <5 <1 <1 <1 <1 <1 <2 <50 <1 <5 NA12/18/201825<0.048 <0.062 <0.076 <0.076 <0.088 <0.076 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 NA NA NA NA12/30/2019<10 <0.048 <0.062 <0.076 <0.076 <0.088 <0.50 <0.079 <0.066 <0.050 <0.061 <0.065 <0.054 <0.089 <0.24 <0.078 <0.042 <0.19 <0.087 <0.047 <0.044 <0.054 <0.076 <0.15 NA NA NA NA1/8/2011ND ND ND ND NA NA ND ND ND ND NA ND ND ND ND ND ND ND ND ND ND ND ND NA NR NR NA11/29/2012ND ND ND ND ND ND ND ND ND ND NA ND ND ND ND ND ND ND ND ND ND ND ND NA NR NR NA11/4/2014<50 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <2.5 <1.0 <1.0 <1.0 NA <1.0 <1.0 <10 <10 <1.0 <5.0 <1.0 <1.0 <5.0 <1.0 <1.0 <2.0 NA <1.0 <5.0 NA4/19/201712/18/20186,000 1 0.6 70 70 70 70 3 0.4 70 600 40 70 25 4000 100 20 6 70 70 600 400 400 500 40 128 10 0.026,000,000 5,000 NL 6,900 8,500 15,000 70,000 3,000 400 70,000 84,500 40,000 25,000 11,700 4,000,000 100,000 20,000 6,000 3,000 70,000 260,000 28,50025,000 85,500 40,000 12,800 10,000 50NL 5 NL NL NL 5 NL NL 7 NL NL 5 NL NL NL 100 NL NL 5 1000 5 10000 NL NL NL NL NL NLNotes:1)NLResult2)NAResult3)NRResult4)ND5)US EPA Region IV MCL = Maximum Contaminant Level defined by US EPA Region IV, December 2009.  Standard as shown hereon applies only to supply well samples.GCLs for GroundwaterNC 2L Standard Compounds analyzed for by laboratory but not listed were not detected above laboratory detection limits. See the laboratory report included  in the Appendix for a full list of constituents. = Compound Not Analyzed for by Laboratory.= Result Exceeds 2L StandardUS EPA Region IV MCLGCLs for Groundwater = NCDEQ UST Section Gross Contamination Levels for Groundwater= Compound Not Detected.WSW‐7WSW‐5WSW‐6WSW‐1All results provided in ug/L (micrograms per liter) or parts per billion= Not Listed= Result Exceeds Laboratory DetecNot SampledNot SampledNC 2L Standard ‐ North Carolina Groundwater Quality Standard as per NC Administrative Code 15A NCAC 02L .0202= Compound Not Reported By Previous Consultants= Result Exceeds GCL ValueWSW‐2WSW‐3WSW‐4Page 4 of 4
Easting Northing
WSW-1 9866485561 3121 NC Highway 86 N Kittaney, Inc.
3121 NC Highway 86 North
Hillsborough, NC 27278 Sole source Unknown Unknown 123 Up-gradient 1964673.17 868647.98
WSW-1A 9866485561 3121 NC Highway 86 N Kittaney, Inc.
3121 NC Highway 86 North
Hillsborough, NC 27278 Out of Service Unknown Unknown 50 Down-gradient 1964835.73 868513.02
WSW-2 9866488257 117 Phelps Road Steven D Bledsoe
505 Phelps Road
Hillsborough, NC 27278 Sole source Unknown Unknown 250 Down-gradient 1964575.64 868305.58
WSW-3 9866486069 3105 NC Highway 86 N Laverne W James
288 Atwater Street
Yanceyville, NC 27379 Sole source Unknown Unknown 248 Down-gradient 1964575.64 868305.58
WSW-4 9866482247 103 Kenion Road Norman E Murray
6005 Mt. Herman Church
Durham, NC 27705 Sole source Unknown Unknown 341 Down-gradient 1964250.52 868583.00
WSW-5 9866580465 201 Phelps Road
Artis Eugene Summey
Dianne T Summey
201 Phelps Road
Hillsborough, NC 27278 Sole source Unknown Unknown 453 Cross-gradient 1965040.81 868575.50
WSW-6 9866488975 118 Phelps Road
Robert L. Bates
Alesha R. Bates
118 Phelps Road
Hillsborough, NC 27278 Sole source Unknown Unknown 456 Up-gradient 1964857.04 868921.05
WSW-7 9866480995 3208 NC Highway 86 N Cleo C Huskins
3220 NC Highway 86 N
Hillsborough, NC 27278 Sole source Unknown Unknown 683 Up-gradient 1964157.30 869080.88
WSW-8 9866389233 123 Kenion Road Donald W. Waters
44 Goldthread Ave.
Clayton, NC 27527 Sole source Unknown Unknown 705 Cross-gradient 1963912.90 868353.07
WSW-9 9866384284 219 Kenion Road
Richard A Roberts
Vivian M Roberts
219 Kenion Road
Hillsborough, NC 27278 Sole source Unknown Unknown 898 Cross-gradient 1963717.82 868300.58
WSW-10 9866477809 3019 NC Highway 86 N Anghello C. Turcios
3019 NC Highway 86 N
Hillsborough, NC 27278 Sole source Unknown Unknown 523 Down-gradient 1964638.16 868023.16
WSW-11 9866477735 3015 NC Highway 86 N Cindy Espada 3015 NC Highway 86 N
Hillsborough, NC 27278 Sole source Unknown Unknown 689 Down-gradient 1964833.23 867900.70
WSW-12 9866479597 3005 NC Highway 86 N Vijaya Vaidya
302 W. Hill Ave. S.
Hillsborough, NC 27278 Sole source Unknown Unknown 915 Down-gradient 1964875.75 867665.76
WSW-13 9866580057 205 Phelps Road
Steven E Summey
Allison L Summey
205 Phelps Road
Hillsborough, NC 27278 Sole source Unknown Unknown 797 Down-gradient 1965178.36 867995.67
WSW-14 9866585010 221 Phelps Road
Ethan C. Helgevold
Kelly E. Helgevold
221 Phelps Road
Hillsborough, NC 27278 Sole source Unknown Unknown 929 Down-gradient 1965178.36 867995.67
WSW-15 9866582061 211 Phelps Road Brenda B Summey
207 Phelps Road
Hillsborough, NC 27278 Sole source Unknown Unknown 668 Cross-gradient 1965258.39 868565.51
WSW-16 9866584839 214 Phelps Road
Charles N Helgevold
Mary Beth Helgevold
214 Phelps Road
Hillsborough, NC 27278 Sole source Unknown Unknown 907 Cross-gradient 1965473.46 868777.94
WSW-17 9866591014 112 Phelps Road
Jefferson D Page
Susan B Page
112 Phelps Road
Hillsborough, NC 27278 Sole source Unknown Unknown 778 Up-gradient 1965128.95 869120.84
WSW-18 9866496245 3221 NC Highway 86 N
Joy E Alvis
Christopher M Alvis
3221 NC Highway 86 N
Hillsborough, NC 27278 Sole source Unknown Unknown 728 Up-gradient 1964457.19 869276.69
WSW-19 9866493405 3305 NC Highway 86 N
Melvia H Ward
Willard A Ward
4124 Walnut Grove Chu
Hillsborough, NC 27278 Sole source Unknown Unknown 919 Up-gradient 1964369.22 869452.51
WSW-20 9866490291 3218 NC Highway 86 N
Michael Huskins
Nancy Huskins
712 Lakeview Drive
Cedar Grove, NC 27231 Sole source Unknown Unknown 937 Up-gradient 1964057.33 869340.62
WSW-21 9866497712 3313 NC Highway 86 N Janis I Zink
3313 NC Highway 86 N
Hillsborough, NC 27278 Sole source Unknown Unknown 1083 Up-gradient NA NA
WSW-22 9866378756 3027 Dry Run Drive Gladys Chapman
3116 Hawkins Road
Hurdle Mills, NC 27541 Sole source Unknown Unknown 970 Cross-gradient 1963957.91 867805.72
WSW-23 9866376758 3026 Dry Run Drive Gladys Chapman
3116 Hawkins Road
Hurdle Mills, NC 27541 Sole source Unknown Unknown 1060 Cross-gradient NA NA
WSW-24 9866378530 3013 Dry Run Road Gladys Chapman
3116 Hawkins Road
Hurdle Mills, NC 27541 Sole source Unknown Unknown 1119 Cross-gradient NA NA
WSW-25 9866478321 2921 NC Highway 86 N Amy Dickey
2921 NC Highway 86 N
Hillsborough, NC 27278 Sole source Unknown Unknown 1194 Down-gradient NA NA
WSW-26 9866587158 305 Phelps Road William R Browning
305 Phelps Road
Hillsborough, NC 27278 Sole source Unknown Unknown 1286 Cross-gradient NA NA
WSW-27 9866588812 304 Phelps Road
Charles N Helgevold
Mary Beth Helgevold
214 Phelps Road
Hillsborough, NC 27278 Sole source Unknown Unknown 1252 Cross-gradient NA NA
WSW-28 9866586953 214 Phelps Road
Charles N Helgevold
Mary Beth Helgevold
214 Phelps Road
Hillsborough, NC 27278 Sole source Unknown Unknown 1046 Down-gradient NA NA
1)
2)
3)
Parcel
Number
Location
Relative to
Groundwater
Flow
Well Coordinates
(NC State Plane NAD 83 Feet)Property Address
TABLE B-5
PUBLIC & PRIVATE WATER SUPPLY WELL INFORMATION
Billy's Mini Mart
3121 NC Highway 86
Hillsborough, Orange County, NC
Property Owner Address
Incident Number: 3327
Well ID Well Use Well Depth
(feet)
Well location addresses and property owner information was obtained from the Orange County GIS Department. Property ownership information current as of January 3, 2020.
WR completed a well survey at the site in 2002.
BOLD, Italicized owner names represent "new" owners of properties shown.
Well
Screen
Interval
(feet)
Well Distance
from Source Area
(feet)
Property Owner
Notes:
Page 1 of 1
Easting NorthingMW‐1 Unknown 2 30 15 15 ‐ 30 101.58 12/30/2019 28.88‐‐‐‐72.7 1964476.82 868535.62MW‐2R 3/22/2010 2 35 20 20 ‐ 35 98.36 12/30/2019 27.15‐‐‐‐71.21 1964626.77 868637.60MW‐3 Unknown 2 48 28 28 ‐ 48 98.67 12/30/2019 30.93‐‐‐‐67.74 1964572.47 868536.85MW‐4 Unknown 2 39 24 24 ‐ 39 99.27 12/30/2019 28.37‐‐‐‐70.90 1964540.45 868542.18MW‐5 Unknown 2 39 24 24 ‐ 39 100.82 12/30/2019 29.27‐‐‐‐71.55 1964457.79 868649.55MW‐6 Unknown 2 39 24 24 ‐ 39 99.90 12/30/2019 32.00‐‐‐‐67.90 1964530.60 868483.10MW‐7 Unknown 2 39 24 24 ‐ 39 103.42 12/30/2019 32.17‐‐‐‐71.25 1964392.66 868477.36MW‐8 Unknown 2 39 9 9 ‐ 39 100.04 12/30/2019 28.93‐‐‐‐71.11 1964516.23 868513.05MW‐9R 3/22/2010 2 40 25 25 ‐ 40 100.83 12/30/2019 29.73‐‐‐‐71.10 1964504.32 868547.51MW‐10R 3/22/2010 2 40 25 25 ‐ 40 100.98 12/30/2019 29.93‐‐‐‐71.05 1964503.09 868525.77MW‐11 3/22/2010 2 35 20 20 ‐ 35 100.00 12/30/2019 26.33‐‐‐‐73.67 1964521.26 868579.53MW‐12 5/6/2015 2 39 24 24 ‐ 39 99.02 12/30/2019 27.65‐‐‐‐71.37 1964542.48 868659.90MW‐13 5/6/2015 2 39 24 24 ‐ 39 100.52 12/30/2019 29.14‐‐‐‐71.38 1964496.32 868616.51MW‐14 5/7/2015 2 39 24 24 ‐ 39 99.25 12/30/2019 28.11‐‐‐‐71.14 1964547.71 868596.96MW‐15 5/7/2015 2 39 24 24 ‐ 39 97.96 12/30/2019 24.47‐‐‐‐73.49 1964612.71 868552.54MW‐16 5/6/2015 2 39 24 24 ‐ 39 98.72 12/30/2019 27.63‐‐‐‐71.09 1964600.28 868632.40MW‐17 5/6/2015 2 39 24 24 ‐ 39 98.40 12/30/2019 27.00‐‐‐‐71.40 1964608.36 868674.28DW‐1 Unknown 2 59 54 54 ‐ 59 99.18 12/30/2019 54.50‐‐‐‐44.68 1964536.35 868540.13DW‐2 Unknown 2 80 75 75 ‐ 80 99.29 12/30/2019 20.20‐‐‐‐79.09 1964536.76 868531.92RW‐3 Unknown 2 30.0 Unknown Unknown‐‐‐‐12/30/2019 28.50‐‐‐‐ ‐‐‐‐1964545.62 868560.47SRW‐1 Unknown 6 50 10 10 ‐ 50 99.60 12/30/2019 28.60‐‐‐‐71.00 1964522.39 868536.85SRW‐2 Unknown 6 Unknown Unknown Unknown 100.90 12/30/2019 NM‐‐‐‐ ‐‐‐1964473.12 868556.951)2)3)4) NM = Not MeasuredTotal Depth     (feet)Date Water Level MeasuredScreened Interval     (feet) Well construction information was obtained from previous consultants reports, excepting construction data for MW‐12, MW‐13, MW‐14, MW‐15, MW‐16 and MW‐17. Top‐of‐Casing elevations for all wells excepting MW‐12, MW‐13, MW‐14, MW‐15, MW‐16 and MW‐17 were determined by previous consultants and are relative to an elevation of 100.00 feet established at the TOC for MW‐11.Depth‐to‐Water from Top‐of‐Casing(feet) Groundwater elevation calculated by: (Top‐of‐Casing ‐ Depth‐to‐Water) + (Free Product Thickness x 0.8581)TABLE B‐73121 NC Highway 86 MONITORING & REMEDIATION WELL CONSTRUCTION INFORMATIONWell Casing Diameter(inches)Free Product Thickness(feet)Top‐of‐Casing Elevation      (feet)Well Casing Depth (feet)Billy's Mini MartHillsborough, Orange County, NCNotes: Date InstalledGroundwaterElevation        (feet)Incident Number: 3327Well IDWell Coordinates(NC State Plane NAD 83 Feet)Page 1 of 1
Well ID
Screened 
Interval     
(feet)
Top‐of‐Casing 
Elevation          
(feet)
Date Water Level 
Measured
Depth‐to‐Product
(feet)
Depth‐to‐Water
Uncorrected
(feet)
Free Product 
Thickness
(feet)
Depth‐to‐Water
Corrected
(feet)
Groundwater 
Surface
Elevation          
(feet)
12/30/2019 ‐‐‐28.88 ‐‐‐28.88 72.70
11/29/2018 ‐‐‐26.23 ‐‐‐26.23 75.35
4/18/2017 ‐‐‐29.56 ‐‐‐29.56 72.02
10/12/2015 ‐‐‐Dry ‐‐‐Dry ‐‐‐
5/5/2015 ‐‐‐26.21 ‐‐‐26.21 75.37
11/4/2014 ‐‐‐Dry ‐‐‐Dry ‐‐‐
11/29/2012 ‐‐‐Dry ‐‐‐Dry ‐‐‐
11/8/2011 ‐‐‐28.89 ‐‐‐28.89 72.69
3/25/2010 ‐‐‐27.36 ‐‐‐27.36 74.22
8/14/2009 ‐‐‐28.84 ‐‐‐28.84 72.74
11/4/2008 ‐‐‐Dry ‐‐‐Dry ‐‐‐
12/30/2019 ‐‐‐27.15 ‐‐‐27.15 71.21
11/29/2018 ‐‐‐21.58 ‐‐‐21.58 76.78
4/18/2017 ‐‐‐26.43 ‐‐‐26.43 71.93
10/12/2015 ‐‐‐28.13 ‐‐‐28.13 70.23
5/5/2015 ‐‐‐21.95 ‐‐‐21.95 76.41
11/4/2014 ‐‐‐27.62 ‐‐‐27.62 70.74
11/29/2012 ‐‐‐33.98 ‐‐‐33.98 64.38
11/8/2011 ‐‐‐Dry ‐‐‐Dry ‐‐‐
3/25/2010 ‐‐‐23.95 ‐‐‐23.95 74.41
12/30/2019 ‐‐‐30.93 ‐‐‐30.93 67.74
11/29/2018 ‐‐‐27.64 ‐‐‐27.64 71.03
4/18/2017 ‐‐‐30.78 ‐‐‐30.78 67.89
10/12/2015 ‐‐‐30.05 ‐‐‐30.05 68.62
5/5/2015 ‐‐‐27.39 ‐‐‐27.39 71.28
11/4/2014 ‐‐‐31.33 ‐‐‐31.33 67.34
11/29/2012 ‐‐‐35.50 ‐‐‐35.50 63.17
11/8/2011 ‐‐‐35.82 ‐‐‐35.82 62.85
3/25/2010 ‐‐‐28.07 ‐‐‐28.07 70.60
8/14/2009 ‐‐‐31.84 ‐‐‐31.84 66.83
11/4/2008 ‐‐‐33.58 ‐‐‐33.58 65.09
12/30/2019 ‐‐‐28.37 ‐‐‐28.37 70.90
11/29/2018 ‐‐‐24.16 ‐‐‐24.16 74.51
4/18/2017 ‐‐‐27.71 ‐‐‐27.71 71.56
10/12/2015 ‐‐‐28.20 ‐‐‐28.20 71.07
5/5/2015 ‐‐‐24.13 ‐‐‐24.13 75.14
11/4/2014 ‐‐‐29.23 ‐‐‐29.23 70.04
11/29/2012 ‐‐‐35.34 ‐‐‐35.34 63.93
11/8/2011 ‐‐‐35.22 ‐‐‐35.22 64.05
3/25/2010 ‐‐‐25.32 ‐‐‐25.32 73.95
8/14/2009 ‐‐‐29.36 ‐‐‐29.36 69.91
11/4/2008 ‐‐‐NM ‐‐‐ ‐‐‐NM
12/30/2019 ‐‐‐29.27 ‐‐‐29.27 71.55
11/29/2018 ‐‐‐25.13 ‐‐‐25.13 74.14
4/18/2017 ‐‐‐28.46 ‐‐‐28.46 72.36
10/12/2015 ‐‐‐29.41 ‐‐‐29.41 71.41
5/5/2015 ‐‐‐25.14 ‐‐‐25.14 75.68
11/4/2014 ‐‐‐30.28 ‐‐‐30.28 70.54
11/29/2012 ‐‐‐36.96 ‐‐‐36.96 63.86
11/8/2011 ‐‐‐36.63 ‐‐‐36.63 64.19
3/25/2010 ‐‐‐26.34 ‐‐‐26.34 74.48
8/14/2009 ‐‐‐30.44 ‐‐‐30.44 70.38
11/4/2008 ‐‐‐34.33 ‐‐‐34.33 66.49
12/30/2019 ‐‐‐32.00 ‐‐‐32.00 67.90
11/29/2018 ‐‐‐27.78 ‐‐‐27.78 73.04
4/18/2017 ‐‐‐31.84 ‐‐‐31.84 68.06
10/12/2015 ‐‐‐31.16 ‐‐‐31.16 68.74
5/5/2015 ‐‐‐28.43 ‐‐‐28.43 71.47
11/4/2014 ‐‐‐NM ‐‐‐ ‐‐‐NM
11/29/2012 ‐‐‐36.96 ‐‐‐36.96 62.94
11/8/2011 ‐‐‐36.63 ‐‐‐36.63 63.27
3/25/2010 ‐‐‐26.34 ‐‐‐26.34 73.56
8/14/2009 ‐‐‐30.44 ‐‐‐30.44 69.46
11/4/2008 ‐‐‐34.33 ‐‐‐34.33 65.57
100.8224 ‐ 39
99.2724 ‐ 39
MW‐115 ‐ 30 101.58
MW‐2R
MW‐3
MW‐4
MW‐5
MW‐6
Incident Number: 3327
TABLE B‐9
CURRENT & HISTORICAL GROUNDWATER ELEVATIONS & FREE PRODUCT THICKNESS
Billy's Mini Mart
3121 NC Highway 86 
Hillsborough, Orange County, NC
99.9024 ‐ 39
28 ‐ 48 98.67
98.3620 ‐ 35
Page 1 of 3
Well ID
Screened 
Interval     
(feet)
Top‐of‐Casing 
Elevation          
(feet)
Date Water Level 
Measured
Depth‐to‐Product
(feet)
Depth‐to‐Water
Uncorrected
(feet)
Free Product 
Thickness
(feet)
Depth‐to‐Water
Corrected
(feet)
Groundwater 
Surface
Elevation          
(feet)
Incident Number: 3327
TABLE B‐9
CURRENT & HISTORICAL GROUNDWATER ELEVATIONS & FREE PRODUCT THICKNESS
Billy's Mini Mart
3121 NC Highway 86 
Hillsborough, Orange County, NC
12/30/2019 ‐‐‐32.17 ‐‐‐32.17 71.25
11/29/2018 ‐‐‐NM ‐‐‐ ‐‐‐ ‐‐‐
4/18/2017 ‐‐‐31.44 ‐‐‐31.44 71.98
10/12/2015 ‐‐‐32.18 ‐‐‐32.18 71.24
5/5/2015 ‐‐‐28.03 ‐‐‐28.03 71.11
11/4/2014 ‐‐‐33.12 ‐‐‐33.12 70.30
11/29/2012 ‐‐‐Dry ‐‐‐ ‐‐‐Dry
11/8/2011 ‐‐‐Dry ‐‐‐ ‐‐‐Dry
3/25/2010 ‐‐‐29.16 ‐‐‐29.16 74.26
8/14/2009 ‐‐‐33.28 ‐‐‐33.28 70.14
11/4/2008 ‐‐‐37.01 ‐‐‐37.01 66.41
12/30/2019 ‐‐‐28.93 ‐‐‐28.93 71.11
11/29/2018 ‐‐‐24.77 ‐‐‐24.77 75.27
4/18/2017 ‐‐‐28.26 ‐‐‐28.26 71.78
10/12/2015 ‐‐‐28.98 ‐‐‐28.98 71.06
5/5/2015 ‐‐‐24.85 ‐‐‐24.85 75.19
11/4/2014 ‐‐‐29.93 ‐‐‐29.93 70.11
2/15/2013 ‐‐‐34.17 ‐‐‐34.17 65.87
2/11/2013 ‐‐‐34.23 ‐‐‐34.23 65.81
11/29/2012 ‐‐‐36.52 ‐‐‐36.52 63.52
11/8/2011 ‐‐‐36.06 ‐‐‐36.06 63.98
3/25/2010 ‐‐‐25.98 ‐‐‐25.98 74.06
8/14/2009 ‐‐‐31.20 ‐‐‐31.20 68.84
11/4/2008 ‐‐‐33.65 ‐‐‐33.65 66.39
12/30/2019 ‐‐‐29.73 ‐‐‐29.73 71.10
11/29/2018 ‐‐‐25.61 ‐‐‐25.61 75.22
4/18/2017 ‐‐‐29.06 ‐‐‐29.06 71.77
10/12/2015 ‐‐‐29.75 ‐‐‐29.75 71.08
5/5/2015 ‐‐‐25.64 ‐‐‐25.64 75.19
11/4/2014 ‐‐‐30.75 ‐‐‐30.75 70.08
11/29/2012 ‐‐‐34.80 ‐‐‐34.80 66.03
11/8/2011 ‐‐‐Dry ‐‐‐Dry Dry
3/25/2010 ‐‐‐26.77 ‐‐‐26.77 74.06
12/30/2019 ‐‐‐29.93 ‐‐‐29.93 71.05
11/29/2018 ‐‐‐25.61 ‐‐‐25.61 75.22
4/18/2017 ‐‐‐29.24 ‐‐‐29.24 71.74
10/12/2015 ‐‐‐29.93 ‐‐‐29.93 71.05
5/5/2015 ‐‐‐25.81 ‐‐‐25.81 75.17
11/4/2014 ‐‐‐30.91 ‐‐‐30.91 70.07
11/29/2012 ‐‐‐37.26 ‐‐‐37.26 63.72
11/8/2011 ‐‐‐37.04 ‐‐‐37.04 63.94
3/25/2010 ‐‐‐26.86 ‐‐‐26.86 74.12
12/30/2019 ‐‐‐26.33 ‐‐‐26.33 73.67
11/29/2018 22.73 22.75 0.02 22.75 78.23
4/18/2017 27.92 28.18 0.26 27.96 71.05
10/12/2015 26.91 27.12 0.21 26.94 73.67
5/5/2015 ‐‐‐24.33 ‐‐‐24.33 75.67
11/4/2014 29.51 29.52 0.01 29.51 70.49
11/29/2012 ‐‐‐35.04 ‐‐‐35.04 64.96
11/8/2011 ‐‐‐35.00 ‐‐‐35.00 65.00
3/25/2010 ‐‐‐24.60 ‐‐‐24.60 75.40
12/30/2019 ‐‐‐27.65 ‐‐‐27.65 71.37
11/29/2018 ‐‐‐23.53 ‐‐‐23.53 75.49
4/18/2017 ‐‐‐26.92 ‐‐‐26.92 72.10
10/12/2015 ‐‐‐27.52 ‐‐‐27.52 71.50
5/7/2015 ‐‐‐23.50 ‐‐‐23.50 75.52
12/30/2019 ‐‐‐29.14 ‐‐‐29.14 71.38
11/29/2018 ‐‐‐25.11 ‐‐‐25.11 73.91
4/18/2017 ‐‐‐28.52 ‐‐‐28.52 72.00
10/12/2015 ‐‐‐29.22 ‐‐‐29.22 71.30
5/7/2015 ‐‐‐25.12 ‐‐‐25.12 75.40
12/30/2019 ‐‐‐28.11 ‐‐‐28.11 71.14
11/29/2018 23.90 23.91 0.01 23.91 76.61
4/18/2017 27.44 27.69 0.25 27.48 71.77
10/12/2015 28.12 28.15 0.03 28.12 72.40
5/7/2015 ‐‐‐24.21 ‐‐‐24.21 75.04
25 ‐ 40 100.83
100.04
MW‐10R
MW‐7
MW‐8
MW‐9R
MW‐11
MW‐12
MW‐13
MW‐14 99.2524 ‐ 39
24 ‐ 39 100.52
99.0224 ‐ 39
20 ‐ 35 100.00
100.9825 ‐ 40
9 ‐ 39
24 ‐ 39 103.42
Page 2 of 3
Well ID
Screened 
Interval     
(feet)
Top‐of‐Casing 
Elevation          
(feet)
Date Water Level 
Measured
Depth‐to‐Product
(feet)
Depth‐to‐Water
Uncorrected
(feet)
Free Product 
Thickness
(feet)
Depth‐to‐Water
Corrected
(feet)
Groundwater 
Surface
Elevation          
(feet)
Incident Number: 3327
TABLE B‐9
CURRENT & HISTORICAL GROUNDWATER ELEVATIONS & FREE PRODUCT THICKNESS
Billy's Mini Mart
3121 NC Highway 86 
Hillsborough, Orange County, NC
12/30/2019 ‐‐‐24.47 ‐‐‐24.47 73.49
11/29/2018 ‐‐‐19.92 ‐‐‐19.92 79.33
4/18/2017 ‐‐‐27.12 ‐‐‐27.12 70.84
10/12/2015 ‐‐‐26.24 ‐‐‐26.24 71.72
5/7/2015 ‐‐‐30.55 ‐‐‐30.55 67.41
12/30/2019 ‐‐‐27.63 ‐‐‐27.63 71.09
11/29/2018 ‐‐‐23.38 ‐‐‐23.38 74.58
4/18/2017 ‐‐‐26.90 ‐‐‐26.90 71.82
10/12/2015 ‐‐‐27.43 ‐‐‐27.43 71.29
5/7/2015 ‐‐‐23.47 ‐‐‐23.47 75.25
12/30/2019 ‐‐‐27.00 ‐‐‐27.00 71.40
11/29/2018 ‐‐‐22.10 ‐‐‐22.10 76.62
4/18/2017 ‐‐‐26.36 ‐‐‐26.36 72.04
10/12/2015 ‐‐‐26.78 ‐‐‐26.78 71.62
5/7/2015 ‐‐‐23.90 ‐‐‐23.90 74.50
12/30/2019 ‐‐‐54.50 ‐‐‐54.50 44.68
11/29/2018 ‐‐‐23.93 ‐‐‐23.93 75.25
4/18/2017 ‐‐‐27.36 ‐‐‐27.36 71.82
10/12/2015 ‐‐‐27.18 ‐‐‐27.18 72.00
5/5/2015 ‐‐‐24.10 ‐‐‐24.10 75.08
11/4/2014 ‐‐‐28.24 ‐‐‐28.24 70.94
11/29/2012 ‐‐‐35.20 ‐‐‐36.65 63.98
11/8/2011 ‐‐‐34.45 ‐‐‐37.00 64.73
3/25/2010 ‐‐‐26.26 ‐‐‐29.09 72.92
12/30/2019 ‐‐‐20.20 ‐‐‐20.20 79.09
11/29/2018 ‐‐‐30.40 ‐‐‐30.40 68.78
4/18/2017 ‐‐‐33.29 ‐‐‐33.29 66.00
10/12/2015 ‐‐‐49.88 ‐‐‐49.88 49.41
5/5/2015 ‐‐‐45.31 ‐‐‐45.31 53.98
11/4/2014 ‐‐‐31.94 ‐‐‐31.94 67.35
11/29/2012 ‐‐‐41.89 ‐‐‐36.65 57.40
11/8/2011 ‐‐‐35.95 ‐‐‐37.00 63.34
3/25/2010 ‐‐‐40.81 ‐‐‐29.09 58.48
12/30/2019 ‐‐‐28.50 ‐‐‐28.50 ‐‐‐
11/29/2018 ‐‐‐26.22 ‐‐‐26.22 ‐‐‐
4/18/2017 ‐‐‐DRY ‐‐‐ ‐‐‐ ‐‐‐
10/12/2015 ‐‐‐ ‐‐‐ ‐‐‐ ‐‐‐NM
5/5/2015 ‐‐‐24.00 ‐‐‐24.00 NM
11/4/2014 ‐‐‐28.81 ‐‐‐28.81 NM
11/29/2012 ‐‐‐Dry ‐‐‐36.65 NM
11/8/2011 ‐‐‐35.95 ‐‐‐37.00 NM
3/25/2010 ‐‐‐40.81 ‐‐‐29.09 NM
12/30/2019 ‐‐‐28.60 ‐‐‐28.60 71.00
11/29/2018 ‐‐‐24.50 ‐‐‐24.50 75.10
4/18/2017 ‐‐‐27.81 ‐‐‐27.81 71.79
10/12/2015 ‐‐‐28.60 ‐‐‐28.60 71.00
5/5/2015 ‐‐‐24.52 ‐‐‐24.52 75.08
11/4/2014 ‐‐‐29.57 ‐‐‐29.57 70.03
11/29/2012 ‐‐‐35.96 ‐‐‐36.65 63.64
11/8/2011 ‐‐‐35.72 ‐‐‐37.00 63.88
3/25/2010 ‐‐‐25.65 ‐‐‐29.09 73.95
12/30/2019 ‐‐‐NM ‐‐‐ ‐‐‐ ‐‐‐
11/29/2018 ‐‐‐NM ‐‐‐ ‐‐‐ ‐‐‐
4/18/2017 ‐‐‐NM ‐‐‐ ‐‐‐ ‐‐‐
10/12/2015 ‐‐‐NM ‐‐‐NM NM
5/5/2015 ‐‐‐NM ‐‐‐NM NM
11/4/2014 ‐‐‐NM ‐‐‐NM NM
11/29/2012 ‐‐‐37.14 ‐‐‐36.65 63.76
11/8/2011 ‐‐‐36.88 ‐‐‐37.00 64.02
3/25/2010 ‐‐‐26.78 ‐‐‐29.09 74.12
1)
2)
3)
4)
5)
75 ‐ 80 99.29
99.1854 ‐ 59
98.7224 ‐ 39
24 ‐ 39 97.96
MW‐17
SRW‐2 ‐‐100.90
 Groundwater elevation calculated by: (Top‐of‐Casing ‐ Depth‐to‐Water) + (Free Product Thickness x 0.8581)
‐‐‐ = Not Applicable
NM = Not Measured
Notes: 
 Well construction information was obtained from previous consultants reports, excepting construction data for MW‐12, MW‐13, MW‐14, MW‐15, MW‐
16 and MW‐17.
 Top‐of‐Casing elevations for all wells excepting MW‐12, MW‐13, MW‐14, MW‐15, MW‐16 and MW‐17 were determined by previous consultants and 
are relative to an elevation of 100.00 feet established at the TOC for MW‐11.
MW‐15
MW‐16
DW‐1
DW‐2
RW‐3
SRW‐110 ‐ 50 99.60
‐‐‐‐
24 ‐ 39 98.40
Page 3 of 3

APPENDIX A 

ANALYTICAL REPORTS AND CHAINS OF CUSTODY 

This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
1/15/20 15:42
Withers & Ravenel
Kevin Buchanan
115 Mackenan Dr. BUILDING 117
Cary, NC 27511
Project: Billy’s Mini Mart
Project No.: NCDEQ#3327 02170214.74
Lab Submittal Date: 01/03/2020
Work Order: 0010027
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOINT ANALYTICAL
Project Management Manager
Reviewed ByAngela D. Overcash Terri W. Cole For Angela D. Overcash
Project Manager
Data Qualifiers Key Reference:
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 91
Sample Receipt Summary
01/15/2020
Work Order: 0010027
Client Sample ID MatrixLab Sample ID Date/Time Sampled Date/Time Received
0010027-01 12/30/19 11:10MW-1 01/03/20 14:10Water
0010027-02 12/30/19 13:45MW-2R 01/03/20 14:10Water
0010027-03 12/30/19 10:00MW-3 01/03/20 14:10Water
0010027-04 12/30/19 9:20MW-4 01/03/20 14:10Water
0010027-05 12/30/19 13:20MW-5 01/03/20 14:10Water
0010027-06 12/30/19 10:20MW-6 01/03/20 14:10Water
0010027-07 12/30/19 12:00MW-7 01/03/20 14:10Water
0010027-08 12/30/19 10:45MW-8 01/03/20 14:10Water
0010027-09 12/30/19 11:10MW-9R 01/03/20 14:10Water
0010027-10 12/30/19 11:35MW-10R 01/03/20 14:10Water
0010027-11 12/30/19 12:25MW-11 01/03/20 14:10Water
0010027-12 12/30/19 14:00MW-12 01/03/20 14:10Water
0010027-13 12/30/19 12:55MW-13 01/03/20 14:10Water
0010027-14 12/30/19 12:40MW-14 01/03/20 14:10Water
0010027-15 12/30/19 9:30MW-15 01/03/20 14:10Water
0010027-16 12/30/19 13:30MW-16 01/03/20 14:10Water
0010027-17 12/30/19 14:10MW-17 01/03/20 14:10Water
0010027-18 12/30/19 9:40DW-1 01/03/20 14:10Water
0010027-19 12/30/19 10:15DW-2 01/03/20 14:10Water
0010027-20 12/30/19 10:40SRW-1 01/03/20 14:10Water
0010027-21 12/30/19 14:15WSW-1 01/03/20 14:10Water
0010027-22 12/30/19 14:30WSW-2 01/03/20 14:10Water
0010027-23 12/30/19 14:46WSW-3 01/03/20 14:10Water
0010027-24 12/30/19 14:31WSW-4 01/03/20 14:10Water
0010027-25 12/30/19 14:45WSW-5 01/03/20 14:10Water
0010027-26 12/30/19 15:01WSW-6 01/03/20 14:10Water
Samples were received in good condition at 2.0 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 91
Client ID ResultParameterMethod UnitsWaypoint ID
Work Order: 0010027
01/15/2020
Summary of Detections
79 ug/L0010027-04 MW-4 1,2,4-Trimethylbenzene *SM6200 B
36 ug/L0010027-04 MW-4 1,3,5-Trimethylbenzene *SM6200 B
7.2 ug/L0010027-04 MW-4 4-Isopropyltoluene *SM6200 B
35 ug/L0010027-04 MW-4 Acetone *SM6200 B
560 ug/L0010027-04 MW-4 Benzene *SM6200 B
170 ug/L0010027-04 MW-4 Ethylbenzene *SM6200 B
11 ug/L0010027-04 MW-4 Isopropyl Ether *SM6200 B
39 ug/L0010027-04 MW-4 Isopropylbenzene (Cumene)*SM6200 B
53 ug/L0010027-04 MW-4 m,p-Xylenes *SM6200 B
980 ug/L0010027-04 MW-4 Methyl-tert-Butyl Ether *SM6200 B
210 ug/L0010027-04 MW-4 Naphthalene *SM6200 B
21 ug/L0010027-04 MW-4 n-Butylbenzene *SM6200 B
77 ug/L0010027-04 MW-4 n-Propylbenzene *SM6200 B
1.4 ug/L0010027-04 MW-4 o-Xylene *SM6200 B
11 ug/L0010027-04 MW-4 sec-Butylbenzene *SM6200 B
24 ug/L0010027-04 MW-4 tert-Amyl Methyl Ether *SM6200 B
310 ug/L0010027-04 MW-4 tert-Butyl Alcohol *SM6200 B
11 ug/L0010027-04 MW-4 Toluene *SM6200 B
54 ug/L0010027-04 MW-4 Xylenes, total *SM6200 B
3.0 ug/L0010027-07 MW-7 Chloroform *SM6200 B
850 ug/L0010027-08 MW-8 1,2,4-Trimethylbenzene *SM6200 B
340 ug/L0010027-08 MW-8 1,3,5-Trimethylbenzene *SM6200 B
12 ug/L0010027-08 MW-8 4-Isopropyltoluene *SM6200 B
34 ug/L0010027-08 MW-8 Benzene *SM6200 B
68 ug/L0010027-08 MW-8 Ethylbenzene *SM6200 B
78 ug/L0010027-08 MW-8 Isopropylbenzene (Cumene)*SM6200 B
390 ug/L0010027-08 MW-8 m,p-Xylenes *SM6200 B
180 ug/L0010027-08 MW-8 Naphthalene *SM6200 B
47 ug/L0010027-08 MW-8 n-Butylbenzene *SM6200 B
180 ug/L0010027-08 MW-8 n-Propylbenzene *SM6200 B
2.4 ug/L0010027-08 MW-8 o-Xylene *SM6200 B
23 ug/L0010027-08 MW-8 sec-Butylbenzene *SM6200 B
47 ug/L0010027-08 MW-8 tert-Amyl Alcohol *SM6200 B
0.62 ug/L0010027-08 MW-8 tert-Butylbenzene *SM6200 B
3.2 ug/L0010027-08 MW-8 Toluene *SM6200 B
390 ug/L0010027-08 MW-8 Xylenes, total *SM6200 B
1400 ug/L0010027-09 MW-9R 1,2,4-Trimethylbenzene *SM6200 B
370 ug/L0010027-09 MW-9R 1,3,5-Trimethylbenzene *SM6200 B
6.8 ug/L0010027-09 MW-9R 4-Isopropyltoluene *SM6200 B
7200 ug/L0010027-09 MW-9R Benzene *SM6200 B
1900 ug/L0010027-09 MW-9R Ethylbenzene *SM6200 B
51 ug/L0010027-09 MW-9R Isopropyl Ether *SM6200 B
70 ug/L0010027-09 MW-9R Isopropylbenzene (Cumene)*SM6200 B
4500 ug/L0010027-09 MW-9R m,p-Xylenes *SM6200 B
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 91
Client ID ResultParameterMethod UnitsWaypoint ID
Work Order: 0010027
01/15/2020
Summary of Detections
25 ug/L0010027-09 MW-9R Methyl Butyl Ketone (2-Hexanone)*SM6200 B
93 ug/L0010027-09 MW-9R Methyl Isobutyl Ketone *SM6200 B
3600 ug/L0010027-09 MW-9R Methyl-tert-Butyl Ether *SM6200 B
580 ug/L0010027-09 MW-9R Naphthalene *SM6200 B
23 ug/L0010027-09 MW-9R n-Butylbenzene *SM6200 B
210 ug/L0010027-09 MW-9R n-Propylbenzene *SM6200 B
870 ug/L0010027-09 MW-9R o-Xylene *SM6200 B
11 ug/L0010027-09 MW-9R sec-Butylbenzene *SM6200 B
5500 ug/L0010027-09 MW-9R tert-Amyl Alcohol *SM6200 B
800 ug/L0010027-09 MW-9R Toluene *SM6200 B
5400 ug/L0010027-09 MW-9R Xylenes, total *SM6200 B
130 ug/L0010027-10 MW-10R 1,2,4-Trimethylbenzene *SM6200 B
68 ug/L0010027-10 MW-10R 1,3,5-Trimethylbenzene *SM6200 B
1.7 ug/L0010027-10 MW-10R 4-Isopropyltoluene *SM6200 B
25 ug/L0010027-10 MW-10R Acetone *SM6200 B
8.2 ug/L0010027-10 MW-10R Benzene *SM6200 B
73 ug/L0010027-10 MW-10R Ethylbenzene *SM6200 B
14 ug/L0010027-10 MW-10R Isopropylbenzene (Cumene)*SM6200 B
130 ug/L0010027-10 MW-10R m,p-Xylenes *SM6200 B
12 ug/L0010027-10 MW-10R Methyl Isobutyl Ketone *SM6200 B
6.1 ug/L0010027-10 MW-10R Methyl-tert-Butyl Ether *SM6200 B
50 ug/L0010027-10 MW-10R Naphthalene *SM6200 B
11 ug/L0010027-10 MW-10R n-Butylbenzene *SM6200 B
44 ug/L0010027-10 MW-10R n-Propylbenzene *SM6200 B
6.3 ug/L0010027-10 MW-10R o-Xylene *SM6200 B
3.9 ug/L0010027-10 MW-10R sec-Butylbenzene *SM6200 B
6.2 ug/L0010027-10 MW-10R Toluene *SM6200 B
130 ug/L0010027-10 MW-10R Xylenes, total *SM6200 B
2900 ug/L0010027-11 MW-11 1,2,4-Trimethylbenzene *SM6200 B
840 ug/L0010027-11 MW-11 1,3,5-Trimethylbenzene *SM6200 B
10 ug/L0010027-11 MW-11 4-Isopropyltoluene *SM6200 B
16 ug/L0010027-11 MW-11 Benzene *SM6200 B
800 ug/L0010027-11 MW-11 Ethylbenzene *SM6200 B
74 ug/L0010027-11 MW-11 Isopropylbenzene (Cumene)*SM6200 B
4900 ug/L0010027-11 MW-11 m,p-Xylenes *SM6200 B
73 ug/L0010027-11 MW-11 Methyl Butyl Ketone (2-Hexanone)*SM6200 B
350 ug/L0010027-11 MW-11 Methyl Isobutyl Ketone *SM6200 B
1800 ug/L0010027-11 MW-11 Naphthalene *SM6200 B
19 ug/L0010027-11 MW-11 n-Butylbenzene *SM6200 B
170 ug/L0010027-11 MW-11 n-Propylbenzene *SM6200 B
670 ug/L0010027-11 MW-11 o-Xylene *SM6200 B
12 ug/L0010027-11 MW-11 sec-Butylbenzene *SM6200 B
49 ug/L0010027-11 MW-11 Toluene *SM6200 B
5600 ug/L0010027-11 MW-11 Xylenes, total *SM6200 B
80 ug/L0010027-12 MW-12 1,2,4-Trimethylbenzene *SM6200 B
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 91
Client ID ResultParameterMethod UnitsWaypoint ID
Work Order: 0010027
01/15/2020
Summary of Detections
18 ug/L0010027-12 MW-12 1,3,5-Trimethylbenzene *SM6200 B
4.8 ug/L0010027-12 MW-12 4-Isopropyltoluene *SM6200 B
93 ug/L0010027-12 MW-12 Benzene *SM6200 B
1.2 ug/L0010027-12 MW-12 Chloroform *SM6200 B
11 ug/L0010027-12 MW-12 Isopropyl Ether *SM6200 B
9.5 ug/L0010027-12 MW-12 Isopropylbenzene (Cumene)*SM6200 B
27 ug/L0010027-12 MW-12 m,p-Xylenes *SM6200 B
250 ug/L0010027-12 MW-12 Methyl-tert-Butyl Ether *SM6200 B
1200 ug/L0010027-12 MW-12 Naphthalene *SM6200 B
3.9 ug/L0010027-12 MW-12 n-Butylbenzene *SM6200 B
1.3 ug/L0010027-12 MW-12 n-Propylbenzene *SM6200 B
70 ug/L0010027-12 MW-12 o-Xylene *SM6200 B
6.0 ug/L0010027-12 MW-12 sec-Butylbenzene *SM6200 B
910 ug/L0010027-12 MW-12 tert-Amyl Alcohol *SM6200 B
660 ug/L0010027-12 MW-12 tert-Butyl Alcohol *SM6200 B
0.57 ug/L0010027-12 MW-12 Toluene *SM6200 B
97 ug/L0010027-12 MW-12 Xylenes, total *SM6200 B
4300 ug/L0010027-13 MW-13 1,2,4-Trimethylbenzene *SM6200 B
1100 ug/L0010027-13 MW-13 1,3,5-Trimethylbenzene *SM6200 B
5400 ug/L0010027-13 MW-13 Benzene *SM6200 B
5300 ug/L0010027-13 MW-13 Ethylbenzene *SM6200 B
180 ug/L0010027-13 MW-13 Isopropylbenzene (Cumene)*SM6200 B
19000 ug/L0010027-13 MW-13 m,p-Xylenes *SM6200 B
1000 ug/L0010027-13 MW-13 Methyl Butyl Ketone (2-Hexanone)*SM6200 B
430 ug/L0010027-13 MW-13 Methyl Isobutyl Ketone *SM6200 B
550 ug/L0010027-13 MW-13 Methyl-tert-Butyl Ether *SM6200 B
1000 ug/L0010027-13 MW-13 Naphthalene *SM6200 B
600 ug/L0010027-13 MW-13 n-Propylbenzene *SM6200 B
7800 ug/L0010027-13 MW-13 o-Xylene *SM6200 B
2400 ug/L0010027-13 MW-13 tert-Amyl Alcohol *SM6200 B
4000 ug/L0010027-13 MW-13 Toluene *SM6200 B
27000 ug/L0010027-13 MW-13 Xylenes, total *SM6200 B
3600 ug/L0010027-14 MW-14 1,2,4-Trimethylbenzene *SM6200 B
920 ug/L0010027-14 MW-14 1,3,5-Trimethylbenzene *SM6200 B
11 ug/L0010027-14 MW-14 4-Isopropyltoluene *SM6200 B
570 ug/L0010027-14 MW-14 Acetone *SM6200 B
1100 ug/L0010027-14 MW-14 Benzene *SM6200 B
6.4 ug/L0010027-14 MW-14 Bromodichloromethane *SM6200 B
4100 ug/L0010027-14 MW-14 Ethylbenzene *SM6200 B
18 ug/L0010027-14 MW-14 Isopropyl Ether *SM6200 B
150 ug/L0010027-14 MW-14 Isopropylbenzene (Cumene)*SM6200 B
15000 ug/L0010027-14 MW-14 m,p-Xylenes *SM6200 B
370 ug/L0010027-14 MW-14 Methyl Butyl Ketone (2-Hexanone)*SM6200 B
400 ug/L0010027-14 MW-14 Methyl Ethyl Ketone (2-Butanone)*SM6200 B
170 ug/L0010027-14 MW-14 Methyl Isobutyl Ketone *SM6200 B
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 91
Client ID ResultParameterMethod UnitsWaypoint ID
Work Order: 0010027
01/15/2020
Summary of Detections
230 ug/L0010027-14 MW-14 Methyl-tert-Butyl Ether *SM6200 B
1600 ug/L0010027-14 MW-14 Naphthalene *SM6200 B
54 ug/L0010027-14 MW-14 n-Butylbenzene *SM6200 B
470 ug/L0010027-14 MW-14 n-Propylbenzene *SM6200 B
7100 ug/L0010027-14 MW-14 o-Xylene *SM6200 B
25 ug/L0010027-14 MW-14 sec-Butylbenzene *SM6200 B
84 ug/L0010027-14 MW-14 Styrene *SM6200 B
1500 ug/L0010027-14 MW-14 tert-Amyl Alcohol *SM6200 B
18000 ug/L0010027-14 MW-14 Toluene *SM6200 B
22000 ug/L0010027-14 MW-14 Xylenes, total *SM6200 B
2500 ug/L0010027-17 MW-17 1,2,4-Trimethylbenzene *SM6200 B
700 ug/L0010027-17 MW-17 1,3,5-Trimethylbenzene *SM6200 B
21 ug/L0010027-17 MW-17 4-Isopropyltoluene *SM6200 B
550 ug/L0010027-17 MW-17 Benzene *SM6200 B
580 ug/L0010027-17 MW-17 Ethylbenzene *SM6200 B
30 ug/L0010027-17 MW-17 Isopropyl Ether *SM6200 B
170 ug/L0010027-17 MW-17 Isopropylbenzene (Cumene)*SM6200 B
3200 ug/L0010027-17 MW-17 m,p-Xylenes *SM6200 B
80 ug/L0010027-17 MW-17 Methyl-tert-Butyl Ether *SM6200 B
470 ug/L0010027-17 MW-17 Naphthalene *SM6200 B
130 ug/L0010027-17 MW-17 n-Butylbenzene *SM6200 B
570 ug/L0010027-17 MW-17 n-Propylbenzene *SM6200 B
1100 ug/L0010027-17 MW-17 o-Xylene *SM6200 B
50 ug/L0010027-17 MW-17 sec-Butylbenzene *SM6200 B
1100 ug/L0010027-17 MW-17 tert-Amyl Alcohol *SM6200 B
62 ug/L0010027-17 MW-17 Toluene *SM6200 B
4300 ug/L0010027-17 MW-17 Xylenes, total *SM6200 B
23 ug/L0010027-19 DW-2 Toluene *SM6200 B
680 ug/L0010027-20 SRW-1 1,2,4-Trimethylbenzene *SM6200 B
250 ug/L0010027-20 SRW-1 1,3,5-Trimethylbenzene *SM6200 B
6.2 ug/L0010027-20 SRW-1 4-Isopropyltoluene *SM6200 B
2000 ug/L0010027-20 SRW-1 Benzene *SM6200 B
540 ug/L0010027-20 SRW-1 Ethylbenzene *SM6200 B
18 ug/L0010027-20 SRW-1 Isopropyl Ether *SM6200 B
38 ug/L0010027-20 SRW-1 Isopropylbenzene (Cumene)*SM6200 B
620 ug/L0010027-20 SRW-1 m,p-Xylenes *SM6200 B
1400 ug/L0010027-20 SRW-1 Methyl-tert-Butyl Ether *SM6200 B
400 ug/L0010027-20 SRW-1 Naphthalene *SM6200 B
12 ug/L0010027-20 SRW-1 n-Butylbenzene *SM6200 B
97 ug/L0010027-20 SRW-1 n-Propylbenzene *SM6200 B
17 ug/L0010027-20 SRW-1 o-Xylene *SM6200 B
7.9 ug/L0010027-20 SRW-1 sec-Butylbenzene *SM6200 B
1800 ug/L0010027-20 SRW-1 tert-Amyl Alcohol *SM6200 B
62 ug/L0010027-20 SRW-1 Toluene *SM6200 B
640 ug/L0010027-20 SRW-1 Xylenes, total *SM6200 B
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 91
Client ID ResultParameterMethod UnitsWaypoint ID
Work Order: 0010027
01/15/2020
Summary of Detections
32 ug/L0010027-21 WSW-1 Acetone *SM6200 B
1.3 ug/L0010027-21 WSW-1 Chloroform *SM6200 B
1.2 ug/L0010027-23 WSW-3 Chloroform *SM6200 B
1.4 ug/L0010027-24 WSW-4 Chloroform *SM6200 B
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-1
Sample ID: 0010027-01
Work Order: 0010027
Time Collected: 12/30/19 11:10
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 19:49 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A008712.0 1/6/20 19:49 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A00871101/6/20 19:49 JLBug/L 0.31Acetone
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.048Benzene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.040Bromoform
BRL *SM6200 B P0A008711.0 1/6/20 19:49 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.076Chloroform
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0A008711.0 1/6/20 19:49 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A008712001/6/20 19:49 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-1
Sample ID: 0010027-01
Work Order: 0010027
Time Collected: 12/30/19 11:10
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 19:49 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A008711.0 1/6/20 19:49 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A008711.0 1/6/20 19:49 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A008715.0 1/6/20 19:49 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A008711.0 1/6/20 19:49 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A008712.0 1/6/20 19:49 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0A008711.0 1/6/20 19:49 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A008711.0 1/6/20 19:49 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.047Styrene
BRL *SM6200 B P0A00871101/6/20 19:49 JLBug/L 0.72tert-Amyl Alcohol
BRL *SM6200 B P0A00871101/6/20 19:49 JLBug/L 0.10tert-Amyl Methyl Ether
BRL *SM6200 B P0A00871101/6/20 19:49 JLBug/L 0.64tert-Butyl Alcohol
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A00871101/6/20 19:49 JLBug/L 0.059tert-Butyl Ethyl Ether
BRL *SM6200 B P0A00871101/6/20 19:49 JLBug/L 0.25tert-Butyl Formate
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.044Toluene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A008715.0 1/6/20 19:49 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0A008710.50 1/6/20 19:49 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0A008711.5 1/6/20 19:49 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130104 %4-Bromofluorobenzene
70-130105 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-2R
Sample ID: 0010027-02
Work Order: 0010027
Time Collected: 12/30/19 13:45
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 20:23 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A008712.0 1/6/20 20:23 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A00871101/6/20 20:23 JLBug/L 0.31Acetone
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.048Benzene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.040Bromoform
BRL *SM6200 B P0A008711.0 1/6/20 20:23 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.076Chloroform
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0A008711.0 1/6/20 20:23 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A008712001/6/20 20:23 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-2R
Sample ID: 0010027-02
Work Order: 0010027
Time Collected: 12/30/19 13:45
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 20:23 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A008711.0 1/6/20 20:23 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A008711.0 1/6/20 20:23 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A008715.0 1/6/20 20:23 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A008711.0 1/6/20 20:23 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A008712.0 1/6/20 20:23 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0A008711.0 1/6/20 20:23 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A008711.0 1/6/20 20:23 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.047Styrene
BRL *SM6200 B P0A00871101/6/20 20:23 JLBug/L 0.72tert-Amyl Alcohol
BRL *SM6200 B P0A00871101/6/20 20:23 JLBug/L 0.10tert-Amyl Methyl Ether
BRL *SM6200 B P0A00871101/6/20 20:23 JLBug/L 0.64tert-Butyl Alcohol
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A00871101/6/20 20:23 JLBug/L 0.059tert-Butyl Ethyl Ether
BRL *SM6200 B P0A00871101/6/20 20:23 JLBug/L 0.25tert-Butyl Formate
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.044Toluene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A008715.0 1/6/20 20:23 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0A008710.50 1/6/20 20:23 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0A008711.5 1/6/20 20:23 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130103 %4-Bromofluorobenzene
70-130107 %Dibromofluoromethane
70-13095 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-3
Sample ID: 0010027-03
Work Order: 0010027
Time Collected: 12/30/19 10:00
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 20:57 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A008712.0 1/6/20 20:57 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A00871101/6/20 20:57 JLBug/L 0.31Acetone
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.048Benzene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.040Bromoform
BRL *SM6200 B P0A008711.0 1/6/20 20:57 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.076Chloroform
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0A008711.0 1/6/20 20:57 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A008712001/6/20 20:57 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-3
Sample ID: 0010027-03
Work Order: 0010027
Time Collected: 12/30/19 10:00
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 20:57 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A008711.0 1/6/20 20:57 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A008711.0 1/6/20 20:57 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A008715.0 1/6/20 20:57 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A008711.0 1/6/20 20:57 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A008712.0 1/6/20 20:57 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0A008711.0 1/6/20 20:57 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A008711.0 1/6/20 20:57 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.047Styrene
BRL *SM6200 B P0A00871101/6/20 20:57 JLBug/L 0.72tert-Amyl Alcohol
BRL *SM6200 B P0A00871101/6/20 20:57 JLBug/L 0.10tert-Amyl Methyl Ether
BRL *SM6200 B P0A00871101/6/20 20:57 JLBug/L 0.64tert-Butyl Alcohol
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A00871101/6/20 20:57 JLBug/L 0.059tert-Butyl Ethyl Ether
BRL *SM6200 B P0A00871101/6/20 20:57 JLBug/L 0.25tert-Butyl Formate
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.044Toluene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A008715.0 1/6/20 20:57 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0A008710.50 1/6/20 20:57 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0A008711.5 1/6/20 20:57 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
70-130105 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-4
Sample ID: 0010027-04
Work Order: 0010027
Time Collected: 12/30/19 09:20
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.131,2,4-Trichlorobenzene
79 *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 21:30 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.111,2-Dichloropropane
36 *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A008712.0 1/6/20 21:30 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.0504-Chlorotoluene
7.2 *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.0894-Isopropyltoluene
35 *SM6200 B P0A00871101/6/20 21:30 JLBug/L 0.31Acetone
560 *SM6200 B P0A0087105.0 1/7/20 16:37 ANGug/L 0.48Benzene
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.040Bromoform
BRL *SM6200 B P0A008711.0 1/6/20 21:30 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.076Chloroform
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0A008711.0 1/6/20 21:30 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A008712001/6/20 21:30 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-4
Sample ID: 0010027-04
Work Order: 0010027
Time Collected: 12/30/19 09:20
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
170 *SM6200 B P0A0087105.0 1/7/20 16:37 ANGug/L 0.61Ethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 21:30 JLBug/L 0.16Hexachlorobutadiene
11 *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.050Isopropyl Ether
39 *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.054Isopropylbenzene (Cumene)
53 *SM6200 B P0A008711.0 1/6/20 21:30 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A008711.0 1/6/20 21:30 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A008715.0 1/6/20 21:30 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A008711.0 1/6/20 21:30 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A008712.0 1/6/20 21:30 JLBug/L 0.083Methylene Chloride
980 *SM6200 B P0A008710101/7/20 16:37 ANGug/L 0.42Methyl-tert-Butyl Ether
210 *SM6200 B P0A008710101/7/20 16:37 ANGug/L 1.9Naphthalene
21 *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.076n-Butylbenzene
77 *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.087n-Propylbenzene
1.4 *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.044o-Xylene
11 *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.047Styrene
BRL *SM6200 B P0A00871101/6/20 21:30 JLBug/L 0.72tert-Amyl Alcohol
24 *SM6200 B P0A00871101/6/20 21:30 JLBug/L 0.10tert-Amyl Methyl Ether
310 *SM6200 B P0A0087101001/7/20 16:37 ANGug/L 6.4tert-Butyl Alcohol
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A00871101/6/20 21:30 JLBug/L 0.059tert-Butyl Ethyl Ether
BRL *SM6200 B P0A00871101/6/20 21:30 JLBug/L 0.25tert-Butyl Formate
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.098Tetrachloroethylene
11 *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.044Toluene
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A008715.0 1/6/20 21:30 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0A008710.50 1/6/20 21:30 JLBug/L 0.097Vinyl chloride
54 *SM6200 B P0A008711.5 1/6/20 21:30 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13098 %4-Bromofluorobenzene
70-13092 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-5
Sample ID: 0010027-05
Work Order: 0010027
Time Collected: 12/30/19 13:20
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A011012.0 1/7/20 14:54 ANGug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A011012.0 1/7/20 14:54 ANGug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A01101101/7/20 14:54 ANGug/L 0.31Acetone
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.048Benzene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.057Bromobenzene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.14Bromochloromethane
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.040Bromoform
BRL *SM6200 B P0A011011.0 1/7/20 14:54 ANGug/L 0.18Bromomethane
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.062Chlorobenzene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.22Chloroethane
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.076Chloroform
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.079Chloromethane
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.065Dibromomethane
BRL *SM6200 B P0A011011.0 1/7/20 14:54 ANGug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A011012001/7/20 14:54 ANGug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-5
Sample ID: 0010027-05
Work Order: 0010027
Time Collected: 12/30/19 13:20
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.061Ethylbenzene
BRL *SM6200 B P0A011012.0 1/7/20 14:54 ANGug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A011011.0 1/7/20 14:54 ANGug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A011011.0 1/7/20 14:54 ANGug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A011015.0 1/7/20 14:54 ANGug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A011011.0 1/7/20 14:54 ANGug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A011012.0 1/7/20 14:54 ANGug/L 0.083Methylene Chloride
BRL *SM6200 B P0A011011.0 1/7/20 14:54 ANGug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A011011.0 1/7/20 14:54 ANGug/L 0.19Naphthalene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.044o-Xylene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.047Styrene
BRL *SM6200 B P0A01101101/7/20 14:54 ANGug/L 0.72tert-Amyl Alcohol
BRL *SM6200 B P0A01101101/7/20 14:54 ANGug/L 0.10tert-Amyl Methyl Ether
BRL *SM6200 B P0A01101101/7/20 14:54 ANGug/L 0.64tert-Butyl Alcohol
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A01101101/7/20 14:54 ANGug/L 0.059tert-Butyl Ethyl Ether
BRL *SM6200 B P0A01101101/7/20 14:54 ANGug/L 0.25tert-Butyl Formate
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.044Toluene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.078Trichloroethylene
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A011015.0 1/7/20 14:54 ANGug/L 0.060Vinyl acetate
BRL *SM6200 B P0A011010.50 1/7/20 14:54 ANGug/L 0.097Vinyl chloride
BRL *SM6200 B P0A011011.5 1/7/20 14:54 ANGug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
70-130104 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-6
Sample ID: 0010027-06
Work Order: 0010027
Time Collected: 12/30/19 10:20
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A011012.0 1/7/20 15:28 ANGug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A011012.0 1/7/20 15:28 ANGug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A01101101/7/20 15:28 ANGug/L 0.31Acetone
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.048Benzene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.057Bromobenzene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.14Bromochloromethane
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.040Bromoform
BRL *SM6200 B P0A011011.0 1/7/20 15:28 ANGug/L 0.18Bromomethane
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.062Chlorobenzene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.22Chloroethane
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.076Chloroform
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.079Chloromethane
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.065Dibromomethane
BRL *SM6200 B P0A011011.0 1/7/20 15:28 ANGug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A011012001/7/20 15:28 ANGug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-6
Sample ID: 0010027-06
Work Order: 0010027
Time Collected: 12/30/19 10:20
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.061Ethylbenzene
BRL *SM6200 B P0A011012.0 1/7/20 15:28 ANGug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A011011.0 1/7/20 15:28 ANGug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A011011.0 1/7/20 15:28 ANGug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A011015.0 1/7/20 15:28 ANGug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A011011.0 1/7/20 15:28 ANGug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A011012.0 1/7/20 15:28 ANGug/L 0.083Methylene Chloride
BRL *SM6200 B P0A011011.0 1/7/20 15:28 ANGug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A011011.0 1/7/20 15:28 ANGug/L 0.19Naphthalene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.044o-Xylene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.047Styrene
BRL *SM6200 B P0A01101101/7/20 15:28 ANGug/L 0.72tert-Amyl Alcohol
BRL *SM6200 B P0A01101101/7/20 15:28 ANGug/L 0.10tert-Amyl Methyl Ether
BRL *SM6200 B P0A01101101/7/20 15:28 ANGug/L 0.64tert-Butyl Alcohol
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A01101101/7/20 15:28 ANGug/L 0.059tert-Butyl Ethyl Ether
BRL *SM6200 B P0A01101101/7/20 15:28 ANGug/L 0.25tert-Butyl Formate
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.044Toluene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.078Trichloroethylene
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A011015.0 1/7/20 15:28 ANGug/L 0.060Vinyl acetate
BRL *SM6200 B P0A011010.50 1/7/20 15:28 ANGug/L 0.097Vinyl chloride
BRL *SM6200 B P0A011011.5 1/7/20 15:28 ANGug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130103 %4-Bromofluorobenzene
70-130106 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-7
Sample ID: 0010027-07
Work Order: 0010027
Time Collected: 12/30/19 12:00
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 23:12 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A008712.0 1/6/20 23:12 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A00871101/6/20 23:12 JLBug/L 0.31Acetone
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.048Benzene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.040Bromoform
BRL *SM6200 B P0A008711.0 1/6/20 23:12 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.22Chloroethane
3.0 *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.076Chloroform
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0A008711.0 1/6/20 23:12 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A008712001/6/20 23:12 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-7
Sample ID: 0010027-07
Work Order: 0010027
Time Collected: 12/30/19 12:00
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 23:12 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A008711.0 1/6/20 23:12 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A008711.0 1/6/20 23:12 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A008715.0 1/6/20 23:12 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A008711.0 1/6/20 23:12 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A008712.0 1/6/20 23:12 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0A008711.0 1/6/20 23:12 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A008711.0 1/6/20 23:12 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.047Styrene
BRL *SM6200 B P0A00871101/6/20 23:12 JLBug/L 0.72tert-Amyl Alcohol
BRL *SM6200 B P0A00871101/6/20 23:12 JLBug/L 0.10tert-Amyl Methyl Ether
BRL *SM6200 B P0A00871101/6/20 23:12 JLBug/L 0.64tert-Butyl Alcohol
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A00871101/6/20 23:12 JLBug/L 0.059tert-Butyl Ethyl Ether
BRL *SM6200 B P0A00871101/6/20 23:12 JLBug/L 0.25tert-Butyl Formate
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.044Toluene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A008715.0 1/6/20 23:12 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0A008710.50 1/6/20 23:12 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0A008711.5 1/6/20 23:12 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130103 %4-Bromofluorobenzene
70-130104 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-8
Sample ID: 0010027-08
Work Order: 0010027
Time Collected: 12/30/19 10:45
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.131,2,4-Trichlorobenzene
850 *SM6200 B P0A011620101/9/20 14:11 ANGug/L 1.11,2,4-Trimethylbenzene
BRL *SM6200 B P0A011612.0 1/8/20 16:08 ANGug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.111,2-Dichloropropane
340 *SM6200 B P0A011620101/9/20 14:11 ANGug/L 1.51,3,5-Trimethylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A011612.0 1/8/20 16:08 ANGug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.0504-Chlorotoluene
12 *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A01161101/8/20 16:08 ANGug/L 0.31Acetone
34 *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.048Benzene
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.057Bromobenzene
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.14Bromochloromethane
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.040Bromoform
BRL *SM6200 B P0A011611.0 1/8/20 16:08 ANGug/L 0.18Bromomethane
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.062Chlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.22Chloroethane
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.076Chloroform
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.079Chloromethane
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.065Dibromomethane
BRL *SM6200 B P0A011611.0 1/8/20 16:08 ANGug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A011612001/8/20 16:08 ANGug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-8
Sample ID: 0010027-08
Work Order: 0010027
Time Collected: 12/30/19 10:45
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
68 *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.061Ethylbenzene
BRL *SM6200 B P0A011612.0 1/8/20 16:08 ANGug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.050Isopropyl Ether
78 *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.054Isopropylbenzene (Cumene)
390 *SM6200 B P0A011620201/9/20 14:11 ANGug/L 2.3m,p-Xylenes
BRL *SM6200 B P0A011611.0 1/8/20 16:08 ANGug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A011615.0 1/8/20 16:08 ANGug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A011611.0 1/8/20 16:08 ANGug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A011612.0 1/8/20 16:08 ANGug/L 0.083Methylene Chloride
BRL *SM6200 B P0A011611.0 1/8/20 16:08 ANGug/L 0.042Methyl-tert-Butyl Ether
180 *SM6200 B P0A011620201/9/20 14:11 ANGug/L 3.8Naphthalene
47 *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.076n-Butylbenzene
180 *SM6200 B P0A011620101/9/20 14:11 ANGug/L 1.7n-Propylbenzene
2.4 *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.044o-Xylene
23 *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.047Styrene
47 *SM6200 B P0A01161101/8/20 16:08 ANGug/L 0.72tert-Amyl Alcohol
BRL *SM6200 B P0A01161101/8/20 16:08 ANGug/L 0.10tert-Amyl Methyl Ether
BRL *SM6200 B P0A01161101/8/20 16:08 ANGug/L 0.64tert-Butyl Alcohol
0.62 *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A01161101/8/20 16:08 ANGug/L 0.059tert-Butyl Ethyl Ether
BRL *SM6200 B P0A01161101/8/20 16:08 ANGug/L 0.25tert-Butyl Formate
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.098Tetrachloroethylene
3.2 *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.044Toluene
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.078Trichloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A011615.0 1/8/20 16:08 ANGug/L 0.060Vinyl acetate
BRL *SM6200 B P0A011610.50 1/8/20 16:08 ANGug/L 0.097Vinyl chloride
390 *SM6200 B P0A011620301/9/20 14:11 ANGug/L 3.0Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
70-13098 %Dibromofluoromethane
70-13099 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-9R
Sample ID: 0010027-09
Work Order: 0010027
Time Collected: 12/30/19 11:10
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 1.11,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.611,1,1-Trichloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.661,1,2-Trichloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.831,1-Dichloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.831,1-Dichloroethylene
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.511,1-Dichloropropylene
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 4.01,2,3-Trichlorobenzene
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 1.41,2,3-Trichloropropane
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 1.31,2,4-Trichlorobenzene
1400 *SM6200 B P0A0116100501/9/20 15:54 ANGug/L 5.41,2,4-Trimethylbenzene
BRL *SM6200 B P0A011610201/8/20 17:25 ANGug/L 1.71,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.511,2-Dibromoethane
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.761,2-Dichlorobenzene
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.661,2-Dichloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 1.11,2-Dichloropropane
370 *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.761,3,5-Trimethylbenzene
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.541,3-Dichlorobenzene
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.431,3-Dichloropropane
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.501,4-Dichlorobenzene
BRL *SM6200 B P0A011610201/8/20 17:25 ANGug/L 1.12,2-Dichloropropane
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.662-Chlorotoluene
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.504-Chlorotoluene
6.8 *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.894-Isopropyltoluene
BRL *SM6200 B P0A0116101001/8/20 17:25 ANGug/L 3.1Acetone
7200 *SM6200 B P0A0116100501/9/20 15:54 ANGug/L 4.8Benzene
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.57Bromobenzene
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 1.4Bromochloromethane
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.62Bromodichloromethane
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.40Bromoform
BRL *SM6200 B P0A011610101/8/20 17:25 ANGug/L 1.8Bromomethane
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 1.1Carbon Tetrachloride
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.62Chlorobenzene
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 2.2Chloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.76Chloroform
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.79Chloromethane
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.56cis-1,2-Dichloroethylene
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.79cis-1,3-Dichloropropylene
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.81Dibromochloromethane
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.65Dibromomethane
BRL *SM6200 B P0A011610101/8/20 17:25 ANGug/L 1.1Dichlorodifluoromethane
BRL *SM6200 B P0A01161020001/8/20 17:25 ANGug/L 270Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-9R
Sample ID: 0010027-09
Work Order: 0010027
Time Collected: 12/30/19 11:10
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
1900 *SM6200 B P0A0116100501/9/20 15:54 ANGug/L 6.1Ethylbenzene
BRL *SM6200 B P0A011610201/8/20 17:25 ANGug/L 1.6Hexachlorobutadiene
51 *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.50Isopropyl Ether
70 *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.54Isopropylbenzene (Cumene)
4500 *SM6200 B P0A01161001001/9/20 15:54 ANGug/L 12m,p-Xylenes
25 *SM6200 B P0A011610101/8/20 17:25 ANGug/L 0.65Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A011610501/8/20 17:25 ANGug/L 2.4Methyl Ethyl Ketone (2-Butanone)
93 *SM6200 B P0A011610101/8/20 17:25 ANGug/L 0.78Methyl Isobutyl Ketone
BRL *SM6200 B P0A011610201/8/20 17:25 ANGug/L 0.83Methylene Chloride
3600 *SM6200 B P0A01161001001/9/20 15:54 ANGug/L 4.2Methyl-tert-Butyl Ether
580 *SM6200 B P0A011610101/8/20 17:25 ANGug/L 1.9Naphthalene
23 *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.76n-Butylbenzene
210 *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.87n-Propylbenzene
870 *SM6200 B P0A0116100501/9/20 15:54 ANGug/L 4.4o-Xylene
11 *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.76sec-Butylbenzene
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.47Styrene
5500 *SM6200 B P0A011610010001/9/20 15:54 ANGug/L 72tert-Amyl Alcohol
BRL *SM6200 B P0A0116101001/8/20 17:25 ANGug/L 1.0tert-Amyl Methyl Ether
BRL *SM6200 B P0A0116101001/8/20 17:25 ANGug/L 6.4tert-Butyl Alcohol
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.88tert-Butylbenzene
BRL *SM6200 B P0A0116101001/8/20 17:25 ANGug/L 0.59tert-Butyl Ethyl Ether
BRL *SM6200 B P0A0116101001/8/20 17:25 ANGug/L 2.5tert-Butyl Formate
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.98Tetrachloroethylene
800 *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.44Toluene
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.70trans-1,2-Dichloroethylene
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 1.2trans-1,3-Dichloropropylene
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.78Trichloroethylene
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.62Trichlorofluoromethane
BRL *SM6200 B P0A011610501/8/20 17:25 ANGug/L 0.60Vinyl acetate
BRL *SM6200 B P0A0116105.0 1/8/20 17:25 ANGug/L 0.97Vinyl chloride
5400 *SM6200 B P0A01161001501/9/20 15:54 ANGug/L 15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-13095 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-10R
Sample ID: 0010027-10
Work Order: 0010027
Time Collected: 12/30/19 11:35
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.131,2,4-Trichlorobenzene
130 *SM6200 B P0A0087105.0 1/7/20 16:03 ANGug/L 0.541,2,4-Trimethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 23:46 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.111,2-Dichloropropane
68 *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A008712.0 1/6/20 23:46 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.0504-Chlorotoluene
1.7 *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.0894-Isopropyltoluene
25 *SM6200 B P0A00871101/6/20 23:46 JLBug/L 0.31Acetone
8.2 *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.048Benzene
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.040Bromoform
BRL *SM6200 B P0A008711.0 1/6/20 23:46 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.076Chloroform
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0A008711.0 1/6/20 23:46 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A008712001/6/20 23:46 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-10R
Sample ID: 0010027-10
Work Order: 0010027
Time Collected: 12/30/19 11:35
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
73 *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 23:46 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.050Isopropyl Ether
14 *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.054Isopropylbenzene (Cumene)
130 *SM6200 B P0A008711.0 1/6/20 23:46 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A008711.0 1/6/20 23:46 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A008715.0 1/6/20 23:46 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
12 *SM6200 B P0A008711.0 1/6/20 23:46 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A008712.0 1/6/20 23:46 JLBug/L 0.083Methylene Chloride
6.1 *SM6200 B P0A008711.0 1/6/20 23:46 JLBug/L 0.042Methyl-tert-Butyl Ether
50 *SM6200 B P0A008711.0 1/6/20 23:46 JLBug/L 0.19Naphthalene
11 *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.076n-Butylbenzene
44 *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.087n-Propylbenzene
6.3 *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.044o-Xylene
3.9 *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.047Styrene
BRL *SM6200 B P0A00871101/6/20 23:46 JLBug/L 0.72tert-Amyl Alcohol
BRL *SM6200 B P0A00871101/6/20 23:46 JLBug/L 0.10tert-Amyl Methyl Ether
BRL *SM6200 B P0A00871101/6/20 23:46 JLBug/L 0.64tert-Butyl Alcohol
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A00871101/6/20 23:46 JLBug/L 0.059tert-Butyl Ethyl Ether
BRL *SM6200 B P0A00871101/6/20 23:46 JLBug/L 0.25tert-Butyl Formate
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.098Tetrachloroethylene
6.2 *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.044Toluene
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A008715.0 1/6/20 23:46 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0A008710.50 1/6/20 23:46 JLBug/L 0.097Vinyl chloride
130 *SM6200 B P0A008711.5 1/6/20 23:46 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130104 %4-Bromofluorobenzene
70-13094 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-11
Sample ID: 0010027-11
Work Order: 0010027
Time Collected: 12/30/19 12:25
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 1.11,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.611,1,1-Trichloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.661,1,2-Trichloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.831,1-Dichloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.831,1-Dichloroethylene
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.511,1-Dichloropropylene
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 4.01,2,3-Trichlorobenzene
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 1.41,2,3-Trichloropropane
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 1.31,2,4-Trichlorobenzene
2900 *SM6200 B P0A0116100501/8/20 20:00 ANGug/L 5.41,2,4-Trimethylbenzene
BRL *SM6200 B P0A011610201/8/20 19:34 ANGug/L 1.71,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.511,2-Dibromoethane
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.761,2-Dichlorobenzene
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.661,2-Dichloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 1.11,2-Dichloropropane
840 *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.761,3,5-Trimethylbenzene
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.541,3-Dichlorobenzene
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.431,3-Dichloropropane
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.501,4-Dichlorobenzene
BRL *SM6200 B P0A011610201/8/20 19:34 ANGug/L 1.12,2-Dichloropropane
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.662-Chlorotoluene
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.504-Chlorotoluene
10 *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.894-Isopropyltoluene
BRL *SM6200 B P0A0116101001/8/20 19:34 ANGug/L 3.1Acetone
16 *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.48Benzene
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.57Bromobenzene
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 1.4Bromochloromethane
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.62Bromodichloromethane
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.40Bromoform
BRL *SM6200 B P0A011610101/8/20 19:34 ANGug/L 1.8Bromomethane
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 1.1Carbon Tetrachloride
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.62Chlorobenzene
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 2.2Chloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.76Chloroform
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.79Chloromethane
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.56cis-1,2-Dichloroethylene
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.79cis-1,3-Dichloropropylene
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.81Dibromochloromethane
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.65Dibromomethane
BRL *SM6200 B P0A011610101/8/20 19:34 ANGug/L 1.1Dichlorodifluoromethane
BRL *SM6200 B P0A01161020001/8/20 19:34 ANGug/L 270Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-11
Sample ID: 0010027-11
Work Order: 0010027
Time Collected: 12/30/19 12:25
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
800 *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.61Ethylbenzene
BRL *SM6200 B P0A011610201/8/20 19:34 ANGug/L 1.6Hexachlorobutadiene
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.50Isopropyl Ether
74 *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.54Isopropylbenzene (Cumene)
4900 *SM6200 B P0A01161001001/8/20 20:00 ANGug/L 12m,p-Xylenes
73 *SM6200 B P0A011610101/8/20 19:34 ANGug/L 0.65Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A011610501/8/20 19:34 ANGug/L 2.4Methyl Ethyl Ketone (2-Butanone)
350 *SM6200 B P0A011610101/8/20 19:34 ANGug/L 0.78Methyl Isobutyl Ketone
BRL *SM6200 B P0A011610201/8/20 19:34 ANGug/L 0.83Methylene Chloride
BRL *SM6200 B P0A011610101/8/20 19:34 ANGug/L 0.42Methyl-tert-Butyl Ether
1800 *SM6200 B P0A01161001001/8/20 20:00 ANGug/L 19Naphthalene
19 *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.76n-Butylbenzene
170 *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.87n-Propylbenzene
670 *SM6200 B P0A0116100501/8/20 20:00 ANGug/L 4.4o-Xylene
12 *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.76sec-Butylbenzene
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.47Styrene
BRL *SM6200 B P0A0116101001/8/20 19:34 ANGug/L 7.2tert-Amyl Alcohol
BRL *SM6200 B P0A0116101001/8/20 19:34 ANGug/L 1.0tert-Amyl Methyl Ether
BRL *SM6200 B P0A0116101001/8/20 19:34 ANGug/L 6.4tert-Butyl Alcohol
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.88tert-Butylbenzene
BRL *SM6200 B P0A0116101001/8/20 19:34 ANGug/L 0.59tert-Butyl Ethyl Ether
BRL *SM6200 B P0A0116101001/8/20 19:34 ANGug/L 2.5tert-Butyl Formate
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.98Tetrachloroethylene
49 *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.44Toluene
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.70trans-1,2-Dichloroethylene
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 1.2trans-1,3-Dichloropropylene
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.78Trichloroethylene
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.62Trichlorofluoromethane
BRL *SM6200 B P0A011610501/8/20 19:34 ANGug/L 0.60Vinyl acetate
BRL *SM6200 B P0A0116105.0 1/8/20 19:34 ANGug/L 0.97Vinyl chloride
5600 *SM6200 B P0A01161001501/8/20 20:00 ANGug/L 15Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
70-13096 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-12
Sample ID: 0010027-12
Work Order: 0010027
Time Collected: 12/30/19 14:00
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.131,2,4-Trichlorobenzene
80 *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A009812.0 1/7/20 18:59 ANGug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.111,2-Dichloropropane
18 *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A009812.0 1/7/20 18:59 ANGug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.0504-Chlorotoluene
4.8 *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A00981101/7/20 18:59 ANGug/L 0.31Acetone
93 *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.048Benzene
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.057Bromobenzene
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.14Bromochloromethane
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.040Bromoform
BRL *SM6200 B P0A009811.0 1/7/20 18:59 ANGug/L 0.18Bromomethane
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.062Chlorobenzene
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.22Chloroethane
1.2 *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.076Chloroform
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.079Chloromethane
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.065Dibromomethane
BRL *SM6200 B P0A009811.0 1/7/20 18:59 ANGug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A009812001/7/20 18:59 ANGug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-12
Sample ID: 0010027-12
Work Order: 0010027
Time Collected: 12/30/19 14:00
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.061Ethylbenzene
BRL *SM6200 B P0A009812.0 1/7/20 18:59 ANGug/L 0.16Hexachlorobutadiene
11 *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.050Isopropyl Ether
9.5 *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.054Isopropylbenzene (Cumene)
27 *SM6200 B P0A009811.0 1/7/20 18:59 ANGug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A009811.0 1/7/20 18:59 ANGug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A009815.0 1/7/20 18:59 ANGug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A009811.0 1/7/20 18:59 ANGug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A009812.0 1/7/20 18:59 ANGug/L 0.083Methylene Chloride
250 *SM6200 B P0A009820201/8/20 19:09 ANGug/L 0.85Methyl-tert-Butyl Ether
1200 *SM6200 B P0A009820201/8/20 19:09 ANGug/L 3.8Naphthalene
3.9 *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.076n-Butylbenzene
1.3 *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.087n-Propylbenzene
70 *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.044o-Xylene
6.0 *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.047Styrene
910 *SM6200 B P0A0098202001/8/20 19:09 ANGug/L 14tert-Amyl Alcohol
BRL *SM6200 B P0A00981101/7/20 18:59 ANGug/L 0.10tert-Amyl Methyl Ether
660 *SM6200 B P0A0098202001/8/20 19:09 ANGug/L 13tert-Butyl Alcohol
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A00981101/7/20 18:59 ANGug/L 0.059tert-Butyl Ethyl Ether
BRL *SM6200 B P0A00981101/7/20 18:59 ANGug/L 0.25tert-Butyl Formate
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.098Tetrachloroethylene
0.57 *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.044Toluene
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.078Trichloroethylene
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A009815.0 1/7/20 18:59 ANGug/L 0.060Vinyl acetate
BRL *SM6200 B P0A009810.50 1/7/20 18:59 ANGug/L 0.097Vinyl chloride
97 *SM6200 B P0A009811.5 1/7/20 18:59 ANGug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130104 %4-Bromofluorobenzene
70-130100 %Dibromofluoromethane
70-13099 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-13
Sample ID: 0010027-13
Work Order: 0010027
Time Collected: 12/30/19 12:55
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 6.11,1,1-Trichloroethane
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 3.61,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 6.61,1,2-Trichloroethane
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 8.31,1-Dichloroethane
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 8.31,1-Dichloroethylene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 5.11,1-Dichloropropylene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 401,2,3-Trichlorobenzene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 141,2,3-Trichloropropane
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 131,2,4-Trichlorobenzene
4300 *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 5.41,2,4-Trimethylbenzene
BRL *SM6200 B P0A01161002001/8/20 21:18 ANGug/L 171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 5.11,2-Dibromoethane
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 7.61,2-Dichlorobenzene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 6.61,2-Dichloroethane
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 111,2-Dichloropropane
1100 *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 7.61,3,5-Trimethylbenzene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 5.41,3-Dichlorobenzene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 4.31,3-Dichloropropane
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 5.01,4-Dichlorobenzene
BRL *SM6200 B P0A01161002001/8/20 21:18 ANGug/L 112,2-Dichloropropane
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 6.62-Chlorotoluene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 5.04-Chlorotoluene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 8.94-Isopropyltoluene
BRL *SM6200 B P0A011610010001/8/20 21:18 ANGug/L 31Acetone
5400 *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 4.8Benzene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 5.7Bromobenzene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 14Bromochloromethane
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 6.2Bromodichloromethane
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 4.0Bromoform
BRL *SM6200 B P0A01161001001/8/20 21:18 ANGug/L 18Bromomethane
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 11Carbon Tetrachloride
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 6.2Chlorobenzene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 22Chloroethane
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 7.6Chloroform
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 7.9Chloromethane
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 5.6cis-1,2-Dichloroethylene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 7.9cis-1,3-Dichloropropylene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 8.1Dibromochloromethane
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 6.5Dibromomethane
BRL *SM6200 B P0A01161001001/8/20 21:18 ANGug/L 11Dichlorodifluoromethane
BRL *SM6200 B P0A0116100200001/8/20 21:18 ANGug/L 2700Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-13
Sample ID: 0010027-13
Work Order: 0010027
Time Collected: 12/30/19 12:55
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
5300 *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 6.1Ethylbenzene
BRL *SM6200 B P0A01161002001/8/20 21:18 ANGug/L 16Hexachlorobutadiene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 5.0Isopropyl Ether
180 *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 5.4Isopropylbenzene (Cumene)
19000 *SM6200 B P0A01161001001/8/20 21:18 ANGug/L 12m,p-Xylenes
1000 *SM6200 B P0A01161001001/8/20 21:18 ANGug/L 6.5Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A01161005001/8/20 21:18 ANGug/L 24Methyl Ethyl Ketone (2-Butanone)
430 *SM6200 B P0A01161001001/8/20 21:18 ANGug/L 7.8Methyl Isobutyl Ketone
BRL *SM6200 B P0A01161002001/8/20 21:18 ANGug/L 8.3Methylene Chloride
550 *SM6200 B P0A01161001001/8/20 21:18 ANGug/L 4.2Methyl-tert-Butyl Ether
1000 *SM6200 B P0A01161001001/8/20 21:18 ANGug/L 19Naphthalene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 7.6n-Butylbenzene
600 *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 8.7n-Propylbenzene
7800 *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 4.4o-Xylene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 7.6sec-Butylbenzene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 4.7Styrene
2400 *SM6200 B P0A011610010001/8/20 21:18 ANGug/L 72tert-Amyl Alcohol
BRL *SM6200 B P0A011610010001/8/20 21:18 ANGug/L 10tert-Amyl Methyl Ether
BRL *SM6200 B P0A011610010001/8/20 21:18 ANGug/L 64tert-Butyl Alcohol
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 8.8tert-Butylbenzene
BRL *SM6200 B P0A011610010001/8/20 21:18 ANGug/L 5.9tert-Butyl Ethyl Ether
BRL *SM6200 B P0A011610010001/8/20 21:18 ANGug/L 25tert-Butyl Formate
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 9.8Tetrachloroethylene
4000 *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 4.4Toluene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 7.0trans-1,2-Dichloroethylene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 7.8Trichloroethylene
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 6.2Trichlorofluoromethane
BRL *SM6200 B P0A01161005001/8/20 21:18 ANGug/L 6.0Vinyl acetate
BRL *SM6200 B P0A0116100501/8/20 21:18 ANGug/L 9.7Vinyl chloride
27000 *SM6200 B P0A01161001501/8/20 21:18 ANGug/L 15Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
70-13097 %Dibromofluoromethane
70-13099 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-14
Sample ID: 0010027-14
Work Order: 0010027
Time Collected: 12/30/19 12:40
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 1.11,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.611,1,1-Trichloroethane
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.661,1,2-Trichloroethane
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.831,1-Dichloroethane
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.831,1-Dichloroethylene
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.511,1-Dichloropropylene
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 4.01,2,3-Trichlorobenzene
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 1.41,2,3-Trichloropropane
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 1.31,2,4-Trichlorobenzene
3600 *SM6200 B P0A0130100501/9/20 15:03 ANGug/L 5.41,2,4-Trimethylbenzene
BRL *SM6200 B P0A013010201/9/20 14:37 ANGug/L 1.71,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.511,2-Dibromoethane
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.761,2-Dichlorobenzene
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.661,2-Dichloroethane
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 1.11,2-Dichloropropane
920 *SM6200 B P0A0130100501/9/20 15:03 ANGug/L 7.61,3,5-Trimethylbenzene
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.541,3-Dichlorobenzene
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.431,3-Dichloropropane
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.501,4-Dichlorobenzene
BRL *SM6200 B P0A013010201/9/20 14:37 ANGug/L 1.12,2-Dichloropropane
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.662-Chlorotoluene
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.504-Chlorotoluene
11 *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.894-Isopropyltoluene
570 *SM6200 B P0A0130101001/9/20 14:37 ANGug/L 3.1Acetone
1100 *SM6200 B P0A0130100501/9/20 15:03 ANGug/L 4.8Benzene
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.57Bromobenzene
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 1.4Bromochloromethane
6.4 *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.62Bromodichloromethane
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.40Bromoform
BRL *SM6200 B P0A013010101/9/20 14:37 ANGug/L 1.8Bromomethane
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 1.1Carbon Tetrachloride
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.62Chlorobenzene
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 2.2Chloroethane
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.76Chloroform
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.79Chloromethane
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.56cis-1,2-Dichloroethylene
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.79cis-1,3-Dichloropropylene
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.81Dibromochloromethane
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.65Dibromomethane
BRL *SM6200 B P0A013010101/9/20 14:37 ANGug/L 1.1Dichlorodifluoromethane
BRL *SM6200 B P0A01301020001/9/20 14:37 ANGug/L 270Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-14
Sample ID: 0010027-14
Work Order: 0010027
Time Collected: 12/30/19 12:40
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
4100 *SM6200 B P0A0130100501/9/20 15:03 ANGug/L 6.1Ethylbenzene
BRL *SM6200 B P0A013010201/9/20 14:37 ANGug/L 1.6Hexachlorobutadiene
18 *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.50Isopropyl Ether
150 *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.54Isopropylbenzene (Cumene)
15000 *SM6200 B P0A01301001001/9/20 15:03 ANGug/L 12m,p-Xylenes
370 *SM6200 B P0A013010101/9/20 14:37 ANGug/L 0.65Methyl Butyl Ketone (2-Hexanone)
400 *SM6200 B P0A013010501/9/20 14:37 ANGug/L 2.4Methyl Ethyl Ketone (2-Butanone)
170 *SM6200 B P0A013010101/9/20 14:37 ANGug/L 0.78Methyl Isobutyl Ketone
BRL *SM6200 B P0A013010201/9/20 14:37 ANGug/L 0.83Methylene Chloride
230 *SM6200 B P0A013010101/9/20 14:37 ANGug/L 0.42Methyl-tert-Butyl Ether
1600 *SM6200 B P0A01301001001/9/20 15:03 ANGug/L 19Naphthalene
54 *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.76n-Butylbenzene
470 *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.87n-Propylbenzene
7100 *SM6200 B P0A0130100501/9/20 15:03 ANGug/L 4.4o-Xylene
25 *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.76sec-Butylbenzene
84 *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.47Styrene
1500 *SM6200 B P0A013010010001/9/20 15:03 ANGug/L 72tert-Amyl Alcohol
BRL *SM6200 B P0A0130101001/9/20 14:37 ANGug/L 1.0tert-Amyl Methyl Ether
BRL *SM6200 B P0A0130101001/9/20 14:37 ANGug/L 6.4tert-Butyl Alcohol
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.88tert-Butylbenzene
BRL *SM6200 B P0A0130101001/9/20 14:37 ANGug/L 0.59tert-Butyl Ethyl Ether
BRL *SM6200 B P0A0130101001/9/20 14:37 ANGug/L 2.5tert-Butyl Formate
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.98Tetrachloroethylene
18000 *SM6200 B P0A013010005001/9/20 16:20 ANGug/L 44Toluene
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.70trans-1,2-Dichloroethylene
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 1.2trans-1,3-Dichloropropylene
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.78Trichloroethylene
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.62Trichlorofluoromethane
BRL *SM6200 B P0A013010501/9/20 14:37 ANGug/L 0.60Vinyl acetate
BRL *SM6200 B P0A0130105.0 1/9/20 14:37 ANGug/L 0.97Vinyl chloride
22000 *SM6200 B P0A01301001501/9/20 15:03 ANGug/L 15Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-13095 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-15
Sample ID: 0010027-15
Work Order: 0010027
Time Collected: 12/30/19 09:30
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A011612.0 1/8/20 15:16 ANGug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A011612.0 1/8/20 15:16 ANGug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A01161101/8/20 15:16 ANGug/L 0.31Acetone
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.048Benzene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.057Bromobenzene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.14Bromochloromethane
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.040Bromoform
BRL *SM6200 B P0A011611.0 1/8/20 15:16 ANGug/L 0.18Bromomethane
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.062Chlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.22Chloroethane
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.076Chloroform
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.079Chloromethane
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.065Dibromomethane
BRL *SM6200 B P0A011611.0 1/8/20 15:16 ANGug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A011612001/8/20 15:16 ANGug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-15
Sample ID: 0010027-15
Work Order: 0010027
Time Collected: 12/30/19 09:30
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.061Ethylbenzene
BRL *SM6200 B P0A011612.0 1/8/20 15:16 ANGug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A011611.0 1/8/20 15:16 ANGug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A011611.0 1/8/20 15:16 ANGug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A011615.0 1/8/20 15:16 ANGug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A011611.0 1/8/20 15:16 ANGug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A011612.0 1/8/20 15:16 ANGug/L 0.083Methylene Chloride
BRL *SM6200 B P0A011611.0 1/8/20 15:16 ANGug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A011611.0 1/8/20 15:16 ANGug/L 0.19Naphthalene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.044o-Xylene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.047Styrene
BRL *SM6200 B P0A01161101/8/20 15:16 ANGug/L 0.72tert-Amyl Alcohol
BRL *SM6200 B P0A01161101/8/20 15:16 ANGug/L 0.10tert-Amyl Methyl Ether
BRL *SM6200 B P0A01161101/8/20 15:16 ANGug/L 0.64tert-Butyl Alcohol
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A01161101/8/20 15:16 ANGug/L 0.059tert-Butyl Ethyl Ether
BRL *SM6200 B P0A01161101/8/20 15:16 ANGug/L 0.25tert-Butyl Formate
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.044Toluene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.078Trichloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A011615.0 1/8/20 15:16 ANGug/L 0.060Vinyl acetate
BRL *SM6200 B P0A011610.50 1/8/20 15:16 ANGug/L 0.097Vinyl chloride
BRL *SM6200 B P0A011611.5 1/8/20 15:16 ANGug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-13097 %Dibromofluoromethane
70-13099 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-16
Sample ID: 0010027-16
Work Order: 0010027
Time Collected: 12/30/19 13:30
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A013012.0 1/9/20 13:45 ANGug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A013012.0 1/9/20 13:45 ANGug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A01301101/9/20 13:45 ANGug/L 0.31Acetone
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.048Benzene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.057Bromobenzene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.14Bromochloromethane
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.040Bromoform
BRL *SM6200 B P0A013011.0 1/9/20 13:45 ANGug/L 0.18Bromomethane
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.062Chlorobenzene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.22Chloroethane
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.076Chloroform
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.079Chloromethane
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.065Dibromomethane
BRL *SM6200 B P0A013011.0 1/9/20 13:45 ANGug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A013012001/9/20 13:45 ANGug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-16
Sample ID: 0010027-16
Work Order: 0010027
Time Collected: 12/30/19 13:30
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.061Ethylbenzene
BRL *SM6200 B P0A013012.0 1/9/20 13:45 ANGug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A013011.0 1/9/20 13:45 ANGug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A013011.0 1/9/20 13:45 ANGug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A013015.0 1/9/20 13:45 ANGug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A013011.0 1/9/20 13:45 ANGug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A013012.0 1/9/20 13:45 ANGug/L 0.083Methylene Chloride
BRL *SM6200 B P0A013011.0 1/9/20 13:45 ANGug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A013011.0 1/9/20 13:45 ANGug/L 0.19Naphthalene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.044o-Xylene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.047Styrene
BRL *SM6200 B P0A01301101/9/20 13:45 ANGug/L 0.72tert-Amyl Alcohol
BRL *SM6200 B P0A01301101/9/20 13:45 ANGug/L 0.10tert-Amyl Methyl Ether
BRL *SM6200 B P0A01301101/9/20 13:45 ANGug/L 0.64tert-Butyl Alcohol
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A01301101/9/20 13:45 ANGug/L 0.059tert-Butyl Ethyl Ether
BRL *SM6200 B P0A01301101/9/20 13:45 ANGug/L 0.25tert-Butyl Formate
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.044Toluene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.078Trichloroethylene
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A013015.0 1/9/20 13:45 ANGug/L 0.060Vinyl acetate
BRL *SM6200 B P0A013010.50 1/9/20 13:45 ANGug/L 0.097Vinyl chloride
BRL *SM6200 B P0A013011.5 1/9/20 13:45 ANGug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
70-13095 %Dibromofluoromethane
70-13098 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-17
Sample ID: 0010027-17
Work Order: 0010027
Time Collected: 12/30/19 14:10
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 1.11,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.611,1,1-Trichloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.661,1,2-Trichloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.831,1-Dichloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.831,1-Dichloroethylene
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.511,1-Dichloropropylene
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 4.01,2,3-Trichlorobenzene
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 1.41,2,3-Trichloropropane
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 1.31,2,4-Trichlorobenzene
2500 *SM6200 B P0A0116100501/8/20 20:52 ANGug/L 5.41,2,4-Trimethylbenzene
BRL *SM6200 B P0A011610201/8/20 20:26 ANGug/L 1.71,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.511,2-Dibromoethane
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.761,2-Dichlorobenzene
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.661,2-Dichloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 1.11,2-Dichloropropane
700 *SM6200 B P0A0116100501/8/20 20:52 ANGug/L 7.61,3,5-Trimethylbenzene
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.541,3-Dichlorobenzene
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.431,3-Dichloropropane
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.501,4-Dichlorobenzene
BRL *SM6200 B P0A011610201/8/20 20:26 ANGug/L 1.12,2-Dichloropropane
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.662-Chlorotoluene
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.504-Chlorotoluene
21 *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.894-Isopropyltoluene
BRL *SM6200 B P0A0116101001/8/20 20:26 ANGug/L 3.1Acetone
550 *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.48Benzene
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.57Bromobenzene
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 1.4Bromochloromethane
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.62Bromodichloromethane
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.40Bromoform
BRL *SM6200 B P0A011610101/8/20 20:26 ANGug/L 1.8Bromomethane
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 1.1Carbon Tetrachloride
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.62Chlorobenzene
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 2.2Chloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.76Chloroform
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.79Chloromethane
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.56cis-1,2-Dichloroethylene
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.79cis-1,3-Dichloropropylene
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.81Dibromochloromethane
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.65Dibromomethane
BRL *SM6200 B P0A011610101/8/20 20:26 ANGug/L 1.1Dichlorodifluoromethane
BRL *SM6200 B P0A01161020001/8/20 20:26 ANGug/L 270Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: MW-17
Sample ID: 0010027-17
Work Order: 0010027
Time Collected: 12/30/19 14:10
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
580 *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.61Ethylbenzene
BRL *SM6200 B P0A011610201/8/20 20:26 ANGug/L 1.6Hexachlorobutadiene
30 *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.50Isopropyl Ether
170 *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.54Isopropylbenzene (Cumene)
3200 *SM6200 B P0A01161001001/8/20 20:52 ANGug/L 12m,p-Xylenes
BRL *SM6200 B P0A011610101/8/20 20:26 ANGug/L 0.65Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A011610501/8/20 20:26 ANGug/L 2.4Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A011610101/8/20 20:26 ANGug/L 0.78Methyl Isobutyl Ketone
BRL *SM6200 B P0A011610201/8/20 20:26 ANGug/L 0.83Methylene Chloride
80 *SM6200 B P0A011610101/8/20 20:26 ANGug/L 0.42Methyl-tert-Butyl Ether
470 *SM6200 B P0A011610101/8/20 20:26 ANGug/L 1.9Naphthalene
130 *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.76n-Butylbenzene
570 *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.87n-Propylbenzene
1100 *SM6200 B P0A0116100501/8/20 20:52 ANGug/L 4.4o-Xylene
50 *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.76sec-Butylbenzene
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.47Styrene
1100 *SM6200 B P0A011610010001/8/20 20:52 ANGug/L 72tert-Amyl Alcohol
BRL *SM6200 B P0A0116101001/8/20 20:26 ANGug/L 1.0tert-Amyl Methyl Ether
BRL *SM6200 B P0A0116101001/8/20 20:26 ANGug/L 6.4tert-Butyl Alcohol
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.88tert-Butylbenzene
BRL *SM6200 B P0A0116101001/8/20 20:26 ANGug/L 0.59tert-Butyl Ethyl Ether
BRL *SM6200 B P0A0116101001/8/20 20:26 ANGug/L 2.5tert-Butyl Formate
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.98Tetrachloroethylene
62 *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.44Toluene
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.70trans-1,2-Dichloroethylene
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 1.2trans-1,3-Dichloropropylene
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.78Trichloroethylene
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.62Trichlorofluoromethane
BRL *SM6200 B P0A011610501/8/20 20:26 ANGug/L 0.60Vinyl acetate
BRL *SM6200 B P0A0116105.0 1/8/20 20:26 ANGug/L 0.97Vinyl chloride
4300 *SM6200 B P0A01161001501/8/20 20:52 ANGug/L 15Xylenes, total
Surrogate Recovery Control Limits
70-13099 %4-Bromofluorobenzene
70-13094 %Dibromofluoromethane
70-13099 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: DW-1
Sample ID: 0010027-18
Work Order: 0010027
Time Collected: 12/30/19 09:40
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 17:00 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A008712.0 1/6/20 17:00 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A00871101/6/20 17:00 JLBug/L 0.31Acetone
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.048Benzene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.040Bromoform
BRL *SM6200 B P0A008711.0 1/6/20 17:00 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.076Chloroform
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0A008711.0 1/6/20 17:00 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A008712001/6/20 17:00 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 42 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: DW-1
Sample ID: 0010027-18
Work Order: 0010027
Time Collected: 12/30/19 09:40
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 17:00 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A008711.0 1/6/20 17:00 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A008711.0 1/6/20 17:00 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A008715.0 1/6/20 17:00 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A008711.0 1/6/20 17:00 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A008712.0 1/6/20 17:00 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0A008711.0 1/6/20 17:00 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A008711.0 1/6/20 17:00 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.047Styrene
BRL *SM6200 B P0A00871101/6/20 17:00 JLBug/L 0.72tert-Amyl Alcohol
BRL *SM6200 B P0A00871101/6/20 17:00 JLBug/L 0.10tert-Amyl Methyl Ether
BRL *SM6200 B P0A00871101/6/20 17:00 JLBug/L 0.64tert-Butyl Alcohol
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A00871101/6/20 17:00 JLBug/L 0.059tert-Butyl Ethyl Ether
BRL *SM6200 B P0A00871101/6/20 17:00 JLBug/L 0.25tert-Butyl Formate
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.044Toluene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A008715.0 1/6/20 17:00 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0A008710.50 1/6/20 17:00 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0A008711.5 1/6/20 17:00 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-130104 %Dibromofluoromethane
70-13096 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 43 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: DW-2
Sample ID: 0010027-19
Work Order: 0010027
Time Collected: 12/30/19 10:15
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 17:34 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A008712.0 1/6/20 17:34 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A00871101/6/20 17:34 JLBug/L 0.31Acetone
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.048Benzene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.040Bromoform
BRL *SM6200 B P0A008711.0 1/6/20 17:34 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.076Chloroform
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0A008711.0 1/6/20 17:34 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A008712001/6/20 17:34 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 44 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: DW-2
Sample ID: 0010027-19
Work Order: 0010027
Time Collected: 12/30/19 10:15
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 17:34 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A008711.0 1/6/20 17:34 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A008711.0 1/6/20 17:34 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A008715.0 1/6/20 17:34 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A008711.0 1/6/20 17:34 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A008712.0 1/6/20 17:34 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0A008711.0 1/6/20 17:34 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A008711.0 1/6/20 17:34 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.047Styrene
BRL *SM6200 B P0A00871101/6/20 17:34 JLBug/L 0.72tert-Amyl Alcohol
BRL *SM6200 B P0A00871101/6/20 17:34 JLBug/L 0.10tert-Amyl Methyl Ether
BRL *SM6200 B P0A00871101/6/20 17:34 JLBug/L 0.64tert-Butyl Alcohol
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A00871101/6/20 17:34 JLBug/L 0.059tert-Butyl Ethyl Ether
BRL *SM6200 B P0A00871101/6/20 17:34 JLBug/L 0.25tert-Butyl Formate
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.098Tetrachloroethylene
23 *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.044Toluene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A008715.0 1/6/20 17:34 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0A008710.50 1/6/20 17:34 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0A008711.5 1/6/20 17:34 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
70-130104 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 45 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: SRW-1
Sample ID: 0010027-20
Work Order: 0010027
Time Collected: 12/30/19 10:40
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 1.11,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.611,1,1-Trichloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.661,1,2-Trichloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.831,1-Dichloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.831,1-Dichloroethylene
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.511,1-Dichloropropylene
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 4.01,2,3-Trichlorobenzene
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 1.41,2,3-Trichloropropane
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 1.31,2,4-Trichlorobenzene
680 *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.541,2,4-Trimethylbenzene
BRL *SM6200 B P0A011610201/8/20 18:17 ANGug/L 1.71,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.511,2-Dibromoethane
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.761,2-Dichlorobenzene
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.661,2-Dichloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 1.11,2-Dichloropropane
250 *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.761,3,5-Trimethylbenzene
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.541,3-Dichlorobenzene
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.431,3-Dichloropropane
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.501,4-Dichlorobenzene
BRL *SM6200 B P0A011610201/8/20 18:17 ANGug/L 1.12,2-Dichloropropane
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.662-Chlorotoluene
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.504-Chlorotoluene
6.2 *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.894-Isopropyltoluene
BRL *SM6200 B P0A0116101001/8/20 18:17 ANGug/L 3.1Acetone
2000 *SM6200 B P0A0116100501/9/20 15:28 ANGug/L 4.8Benzene
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.57Bromobenzene
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 1.4Bromochloromethane
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.62Bromodichloromethane
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.40Bromoform
BRL *SM6200 B P0A011610101/8/20 18:17 ANGug/L 1.8Bromomethane
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 1.1Carbon Tetrachloride
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.62Chlorobenzene
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 2.2Chloroethane
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.76Chloroform
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.79Chloromethane
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.56cis-1,2-Dichloroethylene
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.79cis-1,3-Dichloropropylene
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.81Dibromochloromethane
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.65Dibromomethane
BRL *SM6200 B P0A011610101/8/20 18:17 ANGug/L 1.1Dichlorodifluoromethane
BRL *SM6200 B P0A01161020001/8/20 18:17 ANGug/L 270Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 46 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: SRW-1
Sample ID: 0010027-20
Work Order: 0010027
Time Collected: 12/30/19 10:40
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
540 *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.61Ethylbenzene
BRL *SM6200 B P0A011610201/8/20 18:17 ANGug/L 1.6Hexachlorobutadiene
18 *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.50Isopropyl Ether
38 *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.54Isopropylbenzene (Cumene)
620 *SM6200 B P0A011610101/8/20 18:17 ANGug/L 1.2m,p-Xylenes
BRL *SM6200 B P0A011610101/8/20 18:17 ANGug/L 0.65Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A011610501/8/20 18:17 ANGug/L 2.4Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A011610101/8/20 18:17 ANGug/L 0.78Methyl Isobutyl Ketone
BRL *SM6200 B P0A011610201/8/20 18:17 ANGug/L 0.83Methylene Chloride
1400 *SM6200 B P0A01161001001/9/20 15:28 ANGug/L 4.2Methyl-tert-Butyl Ether
400 *SM6200 B P0A011610101/8/20 18:17 ANGug/L 1.9Naphthalene
12 *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.76n-Butylbenzene
97 *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.87n-Propylbenzene
17 *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.44o-Xylene
7.9 *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.76sec-Butylbenzene
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.47Styrene
1800 *SM6200 B P0A011610010001/9/20 15:28 ANGug/L 72tert-Amyl Alcohol
BRL *SM6200 B P0A0116101001/8/20 18:17 ANGug/L 1.0tert-Amyl Methyl Ether
BRL *SM6200 B P0A0116101001/8/20 18:17 ANGug/L 6.4tert-Butyl Alcohol
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.88tert-Butylbenzene
BRL *SM6200 B P0A0116101001/8/20 18:17 ANGug/L 0.59tert-Butyl Ethyl Ether
BRL *SM6200 B P0A0116101001/8/20 18:17 ANGug/L 2.5tert-Butyl Formate
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.98Tetrachloroethylene
62 *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.44Toluene
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.70trans-1,2-Dichloroethylene
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 1.2trans-1,3-Dichloropropylene
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.78Trichloroethylene
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.62Trichlorofluoromethane
BRL *SM6200 B P0A011610501/8/20 18:17 ANGug/L 0.60Vinyl acetate
BRL *SM6200 B P0A0116105.0 1/8/20 18:17 ANGug/L 0.97Vinyl chloride
640 *SM6200 B P0A011610151/8/20 18:17 ANGug/L 1.5Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
70-13095 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 47 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-1
Sample ID: 0010027-21
Work Order: 0010027
Time Collected: 12/30/19 14:15
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 18:07 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A008712.0 1/6/20 18:07 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.0894-Isopropyltoluene
32 *SM6200 B P0A00871101/6/20 18:07 JLBug/L 0.31Acetone
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.048Benzene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.040Bromoform
BRL *SM6200 B P0A008711.0 1/6/20 18:07 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.22Chloroethane
1.3 *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.076Chloroform
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0A008711.0 1/6/20 18:07 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A008712001/6/20 18:07 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 48 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-1
Sample ID: 0010027-21
Work Order: 0010027
Time Collected: 12/30/19 14:15
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 18:07 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A008711.0 1/6/20 18:07 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A008711.0 1/6/20 18:07 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A008715.0 1/6/20 18:07 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A008711.0 1/6/20 18:07 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A008712.0 1/6/20 18:07 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0A008711.0 1/6/20 18:07 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A008711.0 1/6/20 18:07 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.047Styrene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.044Toluene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A008715.0 1/6/20 18:07 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0A008710.50 1/6/20 18:07 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0A008711.5 1/6/20 18:07 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
70-130103 %Dibromofluoromethane
70-13080 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 49 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-2
Sample ID: 0010027-22
Work Order: 0010027
Time Collected: 12/30/19 14:30
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 18:41 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A008712.0 1/6/20 18:41 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A00871101/6/20 18:41 JLBug/L 0.31Acetone
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.048Benzene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.040Bromoform
BRL *SM6200 B P0A008711.0 1/6/20 18:41 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.076Chloroform
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0A008711.0 1/6/20 18:41 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A008712001/6/20 18:41 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 50 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-2
Sample ID: 0010027-22
Work Order: 0010027
Time Collected: 12/30/19 14:30
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 18:41 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A008711.0 1/6/20 18:41 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A008711.0 1/6/20 18:41 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A008715.0 1/6/20 18:41 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A008711.0 1/6/20 18:41 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A008712.0 1/6/20 18:41 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0A008711.0 1/6/20 18:41 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A008711.0 1/6/20 18:41 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.047Styrene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.044Toluene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A008715.0 1/6/20 18:41 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0A008710.50 1/6/20 18:41 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0A008711.5 1/6/20 18:41 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
70-130104 %Dibromofluoromethane
70-13096 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 51 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-3
Sample ID: 0010027-23
Work Order: 0010027
Time Collected: 12/30/19 14:46
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 19:15 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A008712.0 1/6/20 19:15 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A00871101/6/20 19:15 JLBug/L 0.31Acetone
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.048Benzene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.040Bromoform
BRL *SM6200 B P0A008711.0 1/6/20 19:15 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.22Chloroethane
1.2 *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.076Chloroform
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0A008711.0 1/6/20 19:15 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A008712001/6/20 19:15 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 52 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-3
Sample ID: 0010027-23
Work Order: 0010027
Time Collected: 12/30/19 14:46
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0A008712.0 1/6/20 19:15 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A008711.0 1/6/20 19:15 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A008711.0 1/6/20 19:15 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A008715.0 1/6/20 19:15 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A008711.0 1/6/20 19:15 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A008712.0 1/6/20 19:15 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0A008711.0 1/6/20 19:15 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A008711.0 1/6/20 19:15 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.047Styrene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.044Toluene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A008715.0 1/6/20 19:15 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0A008710.50 1/6/20 19:15 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0A008711.5 1/6/20 19:15 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130100 %4-Bromofluorobenzene
70-130106 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 53 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-4
Sample ID: 0010027-24
Work Order: 0010027
Time Collected: 12/30/19 14:31
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A011612.0 1/8/20 13:59 ANGug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A011612.0 1/8/20 13:59 ANGug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A01161101/8/20 13:59 ANGug/L 0.31Acetone
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.048Benzene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.057Bromobenzene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.14Bromochloromethane
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.040Bromoform
BRL *SM6200 B P0A011611.0 1/8/20 13:59 ANGug/L 0.18Bromomethane
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.062Chlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.22Chloroethane
1.4 *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.076Chloroform
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.079Chloromethane
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.065Dibromomethane
BRL *SM6200 B P0A011611.0 1/8/20 13:59 ANGug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A011612001/8/20 13:59 ANGug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 54 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-4
Sample ID: 0010027-24
Work Order: 0010027
Time Collected: 12/30/19 14:31
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.061Ethylbenzene
BRL *SM6200 B P0A011612.0 1/8/20 13:59 ANGug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A011611.0 1/8/20 13:59 ANGug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A011611.0 1/8/20 13:59 ANGug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A011615.0 1/8/20 13:59 ANGug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A011611.0 1/8/20 13:59 ANGug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A011612.0 1/8/20 13:59 ANGug/L 0.083Methylene Chloride
BRL *SM6200 B P0A011611.0 1/8/20 13:59 ANGug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A011611.0 1/8/20 13:59 ANGug/L 0.19Naphthalene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.044o-Xylene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.047Styrene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.044Toluene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.078Trichloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A011615.0 1/8/20 13:59 ANGug/L 0.060Vinyl acetate
BRL *SM6200 B P0A011610.50 1/8/20 13:59 ANGug/L 0.097Vinyl chloride
BRL *SM6200 B P0A011611.5 1/8/20 13:59 ANGug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
70-13097 %Dibromofluoromethane
70-130100 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 55 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-5
Sample ID: 0010027-25
Work Order: 0010027
Time Collected: 12/30/19 14:45
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A011612.0 1/8/20 14:25 ANGug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A011612.0 1/8/20 14:25 ANGug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A01161101/8/20 14:25 ANGug/L 0.31Acetone
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.048Benzene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.057Bromobenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.14Bromochloromethane
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.040Bromoform
BRL *SM6200 B P0A011611.0 1/8/20 14:25 ANGug/L 0.18Bromomethane
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.062Chlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.22Chloroethane
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.076Chloroform
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.079Chloromethane
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.065Dibromomethane
BRL *SM6200 B P0A011611.0 1/8/20 14:25 ANGug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A011612001/8/20 14:25 ANGug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 56 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-5
Sample ID: 0010027-25
Work Order: 0010027
Time Collected: 12/30/19 14:45
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.061Ethylbenzene
BRL *SM6200 B P0A011612.0 1/8/20 14:25 ANGug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A011611.0 1/8/20 14:25 ANGug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A011611.0 1/8/20 14:25 ANGug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A011615.0 1/8/20 14:25 ANGug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A011611.0 1/8/20 14:25 ANGug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A011612.0 1/8/20 14:25 ANGug/L 0.083Methylene Chloride
BRL *SM6200 B P0A011611.0 1/8/20 14:25 ANGug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A011611.0 1/8/20 14:25 ANGug/L 0.19Naphthalene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.044o-Xylene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.047Styrene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.044Toluene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.078Trichloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A011615.0 1/8/20 14:25 ANGug/L 0.060Vinyl acetate
BRL *SM6200 B P0A011610.50 1/8/20 14:25 ANGug/L 0.097Vinyl chloride
BRL *SM6200 B P0A011611.5 1/8/20 14:25 ANGug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130101 %4-Bromofluorobenzene
70-13096 %Dibromofluoromethane
70-130101 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 57 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-6
Sample ID: 0010027-26
Work Order: 0010027
Time Collected: 12/30/19 15:01
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A011612.0 1/8/20 14:50 ANGug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A011612.0 1/8/20 14:50 ANGug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A01161101/8/20 14:50 ANGug/L 0.31Acetone
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.048Benzene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.057Bromobenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.14Bromochloromethane
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.040Bromoform
BRL *SM6200 B P0A011611.0 1/8/20 14:50 ANGug/L 0.18Bromomethane
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.062Chlorobenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.22Chloroethane
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.076Chloroform
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.079Chloromethane
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.065Dibromomethane
BRL *SM6200 B P0A011611.0 1/8/20 14:50 ANGug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A011612001/8/20 14:50 ANGug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 58 of 91
Laboratory Report
01/15/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-6
Sample ID: 0010027-26
Work Order: 0010027
Time Collected: 12/30/19 15:01
Time Submitted: 01/03/20 14:10
NCDEQ#3327 02170214.74
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.061Ethylbenzene
BRL *SM6200 B P0A011612.0 1/8/20 14:50 ANGug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A011611.0 1/8/20 14:50 ANGug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A011611.0 1/8/20 14:50 ANGug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A011615.0 1/8/20 14:50 ANGug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A011611.0 1/8/20 14:50 ANGug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A011612.0 1/8/20 14:50 ANGug/L 0.083Methylene Chloride
BRL *SM6200 B P0A011611.0 1/8/20 14:50 ANGug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A011611.0 1/8/20 14:50 ANGug/L 0.19Naphthalene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.044o-Xylene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.047Styrene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.044Toluene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.078Trichloroethylene
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A011615.0 1/8/20 14:50 ANGug/L 0.060Vinyl acetate
BRL *SM6200 B P0A011610.50 1/8/20 14:50 ANGug/L 0.097Vinyl chloride
BRL *SM6200 B P0A011611.5 1/8/20 14:50 ANGug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-130102 %4-Bromofluorobenzene
70-13099 %Dibromofluoromethane
70-13099 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 59 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0087 - SM6200 B
Blank (P0A0087-BLK1)Prepared & Analyzed: 01/06/20
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL10
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL1.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethanol ug/LBRL200
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 60 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0087 - SM6200 B
Blank (P0A0087-BLK1)Prepared & Analyzed: 01/06/20
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL1.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL0.50
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Amyl Alcohol ug/LBRL10
tert-Amyl Methyl Ether ug/LBRL10
tert-Butyl Alcohol ug/LBRL10
tert-Butylbenzene ug/LBRL0.50
tert-Butyl Ethyl Ether ug/LBRL10
tert-Butyl Formate ug/LBRL10
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL5.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10050.1
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10351.3
ug/L 50.00 70-130Surrogate: Toluene-d8 9648.0
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 61 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0087 - SM6200 B
LCS (P0A0087-BS1)Prepared & Analyzed: 01/06/20
1,1,1,2-Tetrachloroethane ug/L20.8 0.50 20.00 70-130104
1,1,1-Trichloroethane ug/L21.7 0.50 20.00 70-130109
1,1,2,2-Tetrachloroethane ug/L20.6 0.50 20.00 70-130103
1,1,2-Trichloroethane ug/L20.7 0.50 20.00 70-130103
1,1-Dichloroethane ug/L20.9 0.50 20.00 70-130105
1,1-Dichloroethylene ug/L22.1 0.50 20.00 70-130111
1,1-Dichloropropylene ug/L22.6 0.50 20.00 70-130113
1,2,3-Trichlorobenzene ug/L21.2 0.50 20.00 70-130106
1,2,3-Trichloropropane ug/L21.2 0.50 20.00 70-130106
1,2,4-Trichlorobenzene ug/L20.2 0.50 20.00 70-130101
1,2,4-Trimethylbenzene ug/L21.2 0.50 20.00 70-130106
1,2-Dibromo-3-chloropropane ug/L19.5 2.0 20.00 70-13098
1,2-Dibromoethane ug/L21.2 0.50 20.00 70-130106
1,2-Dichlorobenzene ug/L20.6 0.50 20.00 70-130103
1,2-Dichloroethane ug/L20.0 0.50 20.00 70-130100
1,2-Dichloropropane ug/L21.3 0.50 20.00 70-130107
1,3,5-Trimethylbenzene ug/L21.2 0.50 20.00 70-130106
1,3-Dichlorobenzene ug/L20.9 0.50 20.00 70-130104
1,3-Dichloropropane ug/L20.9 0.50 20.00 70-130104
1,4-Dichlorobenzene ug/L19.9 0.50 20.00 70-130100
2,2-Dichloropropane ug/L21.3 2.0 20.00 70-130106
2-Chlorotoluene ug/L20.7 0.50 20.00 70-130103
4-Chlorotoluene ug/L20.8 0.50 20.00 70-130104
4-Isopropyltoluene ug/L21.9 0.50 20.00 70-130109
Acetone ug/L39.0 10 40.00 40-16097
Benzene ug/L21.7 0.50 20.00 70-130108
Bromobenzene ug/L19.9 0.50 20.00 70-130100
Bromochloromethane ug/L19.9 0.50 20.00 70-13099
Bromodichloromethane ug/L20.7 0.50 20.00 70-130104
Bromoform ug/L20.8 0.50 20.00 70-130104
Bromomethane ug/L24.6 1.0 20.00 60-140123
Carbon Tetrachloride ug/L22.3 0.50 20.00 70-130112
Chlorobenzene ug/L20.1 0.50 20.00 70-130100
Chloroethane ug/L21.7 0.50 20.00 60-140108
Chloroform ug/L20.7 0.50 20.00 70-130104
Chloromethane ug/L22.9 0.50 20.00 60-140114
cis-1,2-Dichloroethylene ug/L20.1 0.50 20.00 70-130101
cis-1,3-Dichloropropylene ug/L22.6 0.50 20.00 70-130113
Dibromochloromethane ug/L20.7 0.50 20.00 70-130103
Dibromomethane ug/L21.4 0.50 20.00 70-130107
Dichlorodifluoromethane ug/L26.9 1.0 20.00 60-140135
Ethanol ug/L552 200 500.0 60-140110
Ethylbenzene ug/L21.2 0.50 20.00 70-130106
Hexachlorobutadiene ug/L20.5 2.0 20.00 70-130102
Isopropyl Ether ug/L19.9 0.50 20.00 70-13099
Isopropylbenzene (Cumene)ug/L22.4 0.50 20.00 70-130112
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 62 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0087 - SM6200 B
LCS (P0A0087-BS1)Prepared & Analyzed: 01/06/20
m,p-Xylenes ug/L43.2 1.0 40.00 70-130108
Methyl Butyl Ketone (2-Hexanone)ug/L20.2 1.0 20.00 60-140101
Methyl Ethyl Ketone (2-Butanone)ug/L21.7 5.0 20.00 60-140109
Methyl Isobutyl Ketone ug/L20.5 1.0 20.00 60-140102
Methylene Chloride ug/L20.6 2.0 20.00 70-130103
Methyl-tert-Butyl Ether ug/L21.3 1.0 20.00 70-130106
Naphthalene ug/L20.4 1.0 20.00 70-130102
n-Butylbenzene ug/L21.5 0.50 20.00 70-130108
n-Propylbenzene ug/L21.3 0.50 20.00 70-130106
o-Xylene ug/L21.1 0.50 20.00 70-130106
sec-Butylbenzene ug/L22.3 0.50 20.00 70-130112
Styrene ug/L21.7 0.50 20.00 70-130108
tert-Amyl Alcohol ug/L21.1 10 20.00 70-130106
tert-Amyl Methyl Ether ug/L43.8 10 40.00 70-130109
tert-Butyl Alcohol ug/L42.7 10 40.00 70-130107
tert-Butylbenzene ug/L22.3 0.50 20.00 70-130111
tert-Butyl Ethyl Ether ug/L42.6 10 40.00 70-130107
tert-Butyl Formate ug/L42.6 10 40.00 70-130107
Tetrachloroethylene ug/L21.6 0.50 20.00 70-130108
Toluene ug/L21.3 0.50 20.00 70-130107
trans-1,2-Dichloroethylene ug/L20.8 0.50 20.00 70-130104
trans-1,3-Dichloropropylene ug/L22.2 0.50 20.00 70-130111
Trichloroethylene ug/L21.7 0.50 20.00 70-130109
Trichlorofluoromethane ug/L23.6 0.50 20.00 60-140118
Vinyl acetate ug/L22.4 5.0 20.00 60-140112
Vinyl chloride ug/L26.2 0.50 20.00 60-140131
Xylenes, total ug/L64.3 1.5 60.00 70-130107
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10050.2
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9748.3
ug/L 50.00 70-130Surrogate: Toluene-d8 9748.5
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 63 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0087 - SM6200 B
LCS Dup (P0A0087-BSD1)Prepared & Analyzed: 01/06/20
1,1,1,2-Tetrachloroethane ug/L20.1 0.50 20.00 2070-130101 3
1,1,1-Trichloroethane ug/L20.2 0.50 20.00 2070-130101 7
1,1,2,2-Tetrachloroethane ug/L20.4 0.50 20.00 2070-130102 1
1,1,2-Trichloroethane ug/L20.8 0.50 20.00 2070-130104 0.8
1,1-Dichloroethane ug/L20.0 0.50 20.00 2070-130100 4
1,1-Dichloroethylene ug/L19.9 0.50 20.00 2070-13099 11
1,1-Dichloropropylene ug/L22.0 0.50 20.00 2070-130110 3
1,2,3-Trichlorobenzene ug/L20.9 0.50 20.00 2070-130104 1
1,2,3-Trichloropropane ug/L21.0 0.50 20.00 2070-130105 1
1,2,4-Trichlorobenzene ug/L20.6 0.50 20.00 2070-130103 2
1,2,4-Trimethylbenzene ug/L20.6 0.50 20.00 2070-130103 3
1,2-Dibromo-3-chloropropane ug/L19.9 2.0 20.00 2070-13099 2
1,2-Dibromoethane ug/L20.8 0.50 20.00 2070-130104 2
1,2-Dichlorobenzene ug/L20.2 0.50 20.00 2070-130101 2
1,2-Dichloroethane ug/L19.5 0.50 20.00 2070-13098 2
1,2-Dichloropropane ug/L20.8 0.50 20.00 2070-130104 3
1,3,5-Trimethylbenzene ug/L20.2 0.50 20.00 2070-130101 5
1,3-Dichlorobenzene ug/L20.4 0.50 20.00 2070-130102 2
1,3-Dichloropropane ug/L20.7 0.50 20.00 2070-130104 0.8
1,4-Dichlorobenzene ug/L19.9 0.50 20.00 2070-13099 0.2
2,2-Dichloropropane ug/L20.1 2.0 20.00 2070-130100 6
2-Chlorotoluene ug/L20.0 0.50 20.00 2070-130100 3
4-Chlorotoluene ug/L20.3 0.50 20.00 2070-130102 3
4-Isopropyltoluene ug/L21.2 0.50 20.00 2070-130106 3
Acetone ug/L38.0 10 40.00 2040-16095 2
Benzene ug/L21.0 0.50 20.00 2070-130105 3
Bromobenzene ug/L19.5 0.50 20.00 2070-13097 2
Bromochloromethane ug/L20.6 0.50 20.00 2070-130103 3
Bromodichloromethane ug/L20.2 0.50 20.00 2070-130101 2
Bromoform ug/L20.2 0.50 20.00 2070-130101 3
Bromomethane ug/L22.8 1.0 20.00 2060-140114 7
Carbon Tetrachloride ug/L21.2 0.50 20.00 2070-130106 5
Chlorobenzene ug/L19.9 0.50 20.00 2070-13099 1
Chloroethane ug/L22.0 0.50 20.00 2060-140110 1
Chloroform ug/L20.4 0.50 20.00 2070-130102 2
Chloromethane ug/L21.7 0.50 20.00 2060-140108 5
cis-1,2-Dichloroethylene ug/L19.6 0.50 20.00 2070-13098 3
cis-1,3-Dichloropropylene ug/L22.4 0.50 20.00 2070-130112 1
Dibromochloromethane ug/L20.2 0.50 20.00 2070-130101 2
Dibromomethane ug/L20.6 0.50 20.00 2070-130103 3
Dichlorodifluoromethane ug/L25.6 1.0 20.00 2060-140128 5
Ethanol ug/L544 200 500.0 2060-140109 2
Ethylbenzene ug/L20.6 0.50 20.00 2070-130103 3
Hexachlorobutadiene ug/L19.2 2.0 20.00 2070-13096 6
Isopropyl Ether ug/L19.8 0.50 20.00 2070-13099 0.5
Isopropylbenzene (Cumene)ug/L21.6 0.50 20.00 2070-130108 4
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 64 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0087 - SM6200 B
LCS Dup (P0A0087-BSD1)Prepared & Analyzed: 01/06/20
m,p-Xylenes ug/L42.6 1.0 40.00 2070-130107 1
Methyl Butyl Ketone (2-Hexanone)ug/L19.0 1.0 20.00 2060-14095 6
Methyl Ethyl Ketone (2-Butanone)ug/L20.1 5.0 20.00 2060-140101 8
Methyl Isobutyl Ketone ug/L19.9 1.0 20.00 2060-140100 3
Methylene Chloride ug/L20.2 2.0 20.00 2070-130101 2
Methyl-tert-Butyl Ether ug/L21.0 1.0 20.00 2070-130105 1
Naphthalene ug/L20.0 1.0 20.00 2070-130100 2
n-Butylbenzene ug/L20.2 0.50 20.00 2070-130101 6
n-Propylbenzene ug/L20.5 0.50 20.00 2070-130102 4
o-Xylene ug/L20.5 0.50 20.00 2070-130103 3
sec-Butylbenzene ug/L21.3 0.50 20.00 2070-130107 5
Styrene ug/L21.6 0.50 20.00 2070-130108 0.6
tert-Amyl Alcohol ug/L21.2 10 20.00 2070-130106 0.3
tert-Amyl Methyl Ether ug/L43.6 10 40.00 2070-130109 0.4
tert-Butyl Alcohol ug/L39.0 10 40.00 2070-13097 9
tert-Butylbenzene ug/L21.6 0.50 20.00 2070-130108 3
tert-Butyl Ethyl Ether ug/L42.5 10 40.00 2070-130106 0.4
tert-Butyl Formate ug/L42.5 10 40.00 2070-130106 0.4
Tetrachloroethylene ug/L21.4 0.50 20.00 2070-130107 0.8
Toluene ug/L20.6 0.50 20.00 2070-130103 3
trans-1,2-Dichloroethylene ug/L19.9 0.50 20.00 2070-130100 4
trans-1,3-Dichloropropylene ug/L21.9 0.50 20.00 2070-130109 1
Trichloroethylene ug/L20.2 0.50 20.00 2070-130101 7
Trichlorofluoromethane ug/L23.0 0.50 20.00 2060-140115 3
Vinyl acetate ug/L22.8 5.0 20.00 2060-140114 2
Vinyl chloride ug/L24.9 0.50 20.00 2060-140124 5
Xylenes, total ug/L63.1 1.5 60.00 2070-130105 2
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.3
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9648.0
ug/L 50.00 70-130Surrogate: Toluene-d8 9849.0
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 65 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0098 - SM6200 B
Blank (P0A0098-BLK1)Prepared & Analyzed: 01/07/20
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL10
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL1.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethanol ug/LBRL200
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 66 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0098 - SM6200 B
Blank (P0A0098-BLK1)Prepared & Analyzed: 01/07/20
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL1.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL0.50
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Amyl Alcohol ug/LBRL10
tert-Amyl Methyl Ether ug/LBRL10
tert-Butyl Alcohol ug/LBRL10
tert-Butylbenzene ug/LBRL0.50
tert-Butyl Ethyl Ether ug/LBRL10
tert-Butyl Formate ug/LBRL10
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL5.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.4
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10049.8
ug/L 50.00 70-130Surrogate: Toluene-d8 9949.6
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 67 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0098 - SM6200 B
LCS (P0A0098-BS1)Prepared & Analyzed: 01/07/20
1,1,1,2-Tetrachloroethane ug/L21.6 0.50 20.00 70-130108
1,1,1-Trichloroethane ug/L23.8 0.50 20.00 70-130119
1,1,2,2-Tetrachloroethane ug/L22.2 0.50 20.00 70-130111
1,1,2-Trichloroethane ug/L22.6 0.50 20.00 70-130113
1,1-Dichloroethane ug/L23.5 0.50 20.00 70-130117
1,1-Dichloroethylene ug/L23.6 0.50 20.00 70-130118
1,1-Dichloropropylene ug/L24.4 0.50 20.00 70-130122
1,2,3-Trichlorobenzene ug/L22.0 0.50 20.00 70-130110
1,2,3-Trichloropropane ug/L22.5 0.50 20.00 70-130112
1,2,4-Trichlorobenzene ug/L21.7 0.50 20.00 70-130108
1,2,4-Trimethylbenzene ug/L22.6 0.50 20.00 70-130113
1,2-Dibromo-3-chloropropane ug/L21.8 2.0 20.00 70-130109
1,2-Dibromoethane ug/L22.2 0.50 20.00 70-130111
1,2-Dichlorobenzene ug/L21.6 0.50 20.00 70-130108
1,2-Dichloroethane ug/L21.3 0.50 20.00 70-130106
1,2-Dichloropropane ug/L21.8 0.50 20.00 70-130109
1,3,5-Trimethylbenzene ug/L22.7 0.50 20.00 70-130113
1,3-Dichlorobenzene ug/L21.9 0.50 20.00 70-130110
1,3-Dichloropropane ug/L22.7 0.50 20.00 70-130114
1,4-Dichlorobenzene ug/L21.9 0.50 20.00 70-130109
2,2-Dichloropropane ug/L24.0 2.0 20.00 70-130120
2-Chlorotoluene ug/L21.9 0.50 20.00 70-130110
4-Chlorotoluene ug/L22.3 0.50 20.00 70-130112
4-Isopropyltoluene ug/L23.4 0.50 20.00 70-130117
Acetone ug/L39.6 10 40.00 40-16099
Benzene ug/L22.3 0.50 20.00 70-130111
Bromobenzene ug/L22.8 0.50 20.00 70-130114
Bromochloromethane ug/L22.9 0.50 20.00 70-130114
Bromodichloromethane ug/L22.6 0.50 20.00 70-130113
Bromoform ug/L22.2 0.50 20.00 70-130111
Bromomethane ug/L21.2 1.0 20.00 60-140106
Carbon Tetrachloride ug/L24.1 0.50 20.00 70-130120
Chlorobenzene ug/L22.0 0.50 20.00 70-130110
Chloroethane ug/L24.1 0.50 20.00 60-140120
Chloroform ug/L23.0 0.50 20.00 70-130115
Chloromethane ug/L19.5 0.50 20.00 60-14098
cis-1,2-Dichloroethylene ug/L21.6 0.50 20.00 70-130108
cis-1,3-Dichloropropylene ug/L23.5 0.50 20.00 70-130117
Dibromochloromethane ug/L22.6 0.50 20.00 70-130113
Dibromomethane ug/L22.9 0.50 20.00 70-130115
Dichlorodifluoromethane ug/L19.7 1.0 20.00 60-14098
Ethanol ug/L560 200 500.0 60-140112
Ethylbenzene ug/L22.3 0.50 20.00 70-130112
Hexachlorobutadiene ug/L23.5 2.0 20.00 70-130117
Isopropyl Ether ug/L21.8 0.50 20.00 70-130109
Isopropylbenzene (Cumene)ug/L23.8 0.50 20.00 70-130119
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 68 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0098 - SM6200 B
LCS (P0A0098-BS1)Prepared & Analyzed: 01/07/20
m,p-Xylenes ug/L45.2 1.0 40.00 70-130113
Methyl Butyl Ketone (2-Hexanone)ug/L21.5 1.0 20.00 60-140107
Methyl Ethyl Ketone (2-Butanone)ug/L20.8 5.0 20.00 60-140104
Methyl Isobutyl Ketone ug/L21.7 1.0 20.00 60-140108
Methylene Chloride ug/L22.0 2.0 20.00 70-130110
Methyl-tert-Butyl Ether ug/L23.0 1.0 20.00 70-130115
Naphthalene ug/L20.9 1.0 20.00 70-130105
n-Butylbenzene ug/L23.2 0.50 20.00 70-130116
n-Propylbenzene ug/L22.9 0.50 20.00 70-130114
o-Xylene ug/L21.9 0.50 20.00 70-130110
sec-Butylbenzene ug/L24.0 0.50 20.00 70-130120
Styrene ug/L22.8 0.50 20.00 70-130114
tert-Amyl Alcohol ug/L23.3 10 20.00 70-130117
tert-Amyl Methyl Ether ug/L45.6 10 40.00 70-130114
tert-Butyl Alcohol ug/L44.8 10 40.00 70-130112
tert-Butylbenzene ug/L23.2 0.50 20.00 70-130116
tert-Butyl Ethyl Ether ug/L45.2 10 40.00 70-130113
tert-Butyl Formate ug/L45.8 10 40.00 70-130114
Tetrachloroethylene ug/L23.7 0.50 20.00 70-130118
Toluene ug/L22.8 0.50 20.00 70-130114
trans-1,2-Dichloroethylene ug/L22.8 0.50 20.00 70-130114
trans-1,3-Dichloropropylene ug/L23.4 0.50 20.00 70-130117
Trichloroethylene ug/L22.6 0.50 20.00 70-130113
Trichlorofluoromethane ug/L23.2 0.50 20.00 60-140116
Vinyl acetate ug/L22.0 5.0 20.00 60-140110
Vinyl chloride ug/L23.2 0.50 20.00 60-140116
Xylenes, total ug/L67.1 1.5 60.00 70-130112
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.6
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9949.3
ug/L 50.00 70-130Surrogate: Toluene-d8 9849.0
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 69 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0098 - SM6200 B
Matrix Spike (P0A0098-MS1)Prepared & Analyzed: 01/07/20 Source: 0010027-12
1,1,1,2-Tetrachloroethane ug/L2055.0 200.0 BRL 70-130102
1,1,1-Trichloroethane ug/L2195.0 200.0 BRL 70-130109
1,1,2,2-Tetrachloroethane ug/L2045.0 200.0 BRL 70-130102
1,1,2-Trichloroethane ug/L2065.0 200.0 BRL 70-130103
1,1-Dichloroethane ug/L2165.0 200.0 BRL 70-130108
1,1-Dichloroethylene ug/L2145.0 200.0 BRL 70-130107
1,1-Dichloropropylene ug/L2265.0 200.0 BRL 70-130113
1,2,3-Trichlorobenzene ug/L1865.0 200.0 BRL 70-13093
1,2,3-Trichloropropane ug/L2105.0 200.0 BRL 70-130105
1,2,4-Trichlorobenzene ug/L1965.0 200.0 BRL 70-13098
1,2,4-Trimethylbenzene ug/L2885.0 200.0 80.1 70-130104
1,2-Dibromo-3-chloropropane ug/L19420 200.0 BRL 70-13097
1,2-Dibromoethane ug/L2055.0 200.0 BRL 70-130102
1,2-Dichlorobenzene ug/L2035.0 200.0 BRL 70-130101
1,2-Dichloroethane ug/L1985.0 200.0 BRL 70-13099
1,2-Dichloropropane ug/L2105.0 200.0 BRL 70-130105
1,3,5-Trimethylbenzene ug/L2275.0 200.0 17.6 70-130105
1,3-Dichlorobenzene ug/L2045.0 200.0 BRL 70-130102
1,3-Dichloropropane ug/L2165.0 200.0 BRL 70-130108
1,4-Dichlorobenzene ug/L2025.0 200.0 BRL 70-130101
2,2-Dichloropropane ug/L22020 200.0 BRL 70-130110
2-Chlorotoluene ug/L2065.0 200.0 BRL 70-130103
4-Chlorotoluene ug/L2045.0 200.0 BRL 70-130102
4-Isopropyltoluene ug/L2265.0 200.0 4.77 70-130110
Acetone ug/L303 100 400.0 BRL 40-16076
Benzene ug/L2975.0 200.0 93.3 70-130102
Bromobenzene ug/L2125.0 200.0 BRL 70-130106
Bromochloromethane ug/L2195.0 200.0 BRL 70-130109
Bromodichloromethane ug/L2125.0 200.0 BRL 70-130106
Bromoform ug/L2105.0 200.0 BRL 70-130105
Bromomethane ug/L12610 200.0 BRL 60-14063
Carbon Tetrachloride ug/L2195.0 200.0 BRL 70-130109
Chlorobenzene ug/L2065.0 200.0 BRL 70-130103
Chloroethane ug/L2095.0 200.0 BRL 60-140104
Chloroform ug/L2165.0 200.0 1.16 70-130108
Chloromethane ug/L1815.0 200.0 BRL 60-14091
cis-1,2-Dichloroethylene ug/L2005.0 200.0 BRL 70-130100
cis-1,3-Dichloropropylene ug/L2215.0 200.0 BRL 70-130111
Dibromochloromethane ug/L2115.0 200.0 BRL 70-130106
Dibromomethane ug/L2215.0 200.0 BRL 70-130110
Dichlorodifluoromethane ug/L16210 200.0 BRL 60-14081
Ethanol ug/L4760 2000 5000 BRL 60-14095
Ethylbenzene ug/L2095.0 200.0 BRL 70-130104
Hexachlorobutadiene ug/L20520 200.0 BRL 70-130103
Isopropyl Ether ug/L2105.0 200.0 10.8 70-130100
Isopropylbenzene (Cumene)ug/L2265.0 200.0 9.54 70-130108
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 70 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0098 - SM6200 B
Matrix Spike (P0A0098-MS1)Prepared & Analyzed: 01/07/20 Source: 0010027-12
m,p-Xylenes ug/L46410 400.0 26.9 70-130109
Methyl Butyl Ketone (2-Hexanone)ug/L19710 200.0 BRL 60-14098
Methyl Ethyl Ketone (2-Butanone)ug/L18650 200.0 BRL 60-14093
Methyl Isobutyl Ketone ug/L20110 200.0 BRL 60-140100
Methylene Chloride ug/L19820 200.0 0.980 70-13098
Methyl-tert-Butyl Ether ug/L46610 200.0 255 70-130106
Naphthalene ug/L34010 200.0 1210 70-130NR
n-Butylbenzene ug/L2135.0 200.0 3.94 70-130105
n-Propylbenzene ug/L2115.0 200.0 1.29 70-130105
o-Xylene ug/L2805.0 200.0 69.8 70-130105
sec-Butylbenzene ug/L2225.0 200.0 6.03 70-130108
Styrene ug/L2105.0 200.0 BRL 70-130105
tert-Amyl Alcohol ug/L1.00E10 100 200.0 910 70-130NR
tert-Amyl Methyl Ether ug/L443 100 400.0 3.70 70-130110
tert-Butyl Alcohol ug/L1050100 400.0 655 70-13099
tert-Butylbenzene ug/L2165.0 200.0 BRL 70-130108
tert-Butyl Ethyl Ether ug/L430 100 400.0 BRL 70-130108
tert-Butyl Formate ug/L385 100 400.0 BRL 70-13096
Tetrachloroethylene ug/L2215.0 200.0 BRL 70-130110
Toluene ug/L2145.0 200.0 0.570 70-130107
trans-1,2-Dichloroethylene ug/L2055.0 200.0 BRL 70-130103
trans-1,3-Dichloropropylene ug/L2175.0 200.0 BRL 70-130109
Trichloroethylene ug/L2155.0 200.0 BRL 70-130107
Trichlorofluoromethane ug/L1995.0 200.0 BRL 60-140100
Vinyl acetate ug/L21550 200.0 BRL 60-140107
Vinyl chloride ug/L1965.0 200.0 BRL 60-14098
Xylenes, total ug/L74415 600.0 96.7 70-130108
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10049.9
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9849.0
ug/L 50.00 70-130Surrogate: Toluene-d8 10049.9
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 71 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0098 - SM6200 B
Matrix Spike Dup (P0A0098-MSD1)Prepared & Analyzed: 01/07/20 Source: 0010027-12
1,1,1,2-Tetrachloroethane ug/L1995.0 200.0 BRL 2070-130100 3
1,1,1-Trichloroethane ug/L2115.0 200.0 BRL 2070-130106 3
1,1,2,2-Tetrachloroethane ug/L2095.0 200.0 BRL 2070-130104 3
1,1,2-Trichloroethane ug/L2105.0 200.0 BRL 2070-130105 2
1,1-Dichloroethane ug/L2115.0 200.0 BRL 2070-130105 2
1,1-Dichloroethylene ug/L2035.0 200.0 BRL 2070-130101 6
1,1-Dichloropropylene ug/L2155.0 200.0 BRL 2070-130107 5
1,2,3-Trichlorobenzene ug/L1965.0 200.0 BRL 2070-13098 5
1,2,3-Trichloropropane ug/L2205.0 200.0 BRL 2070-130110 5
1,2,4-Trichlorobenzene ug/L2015.0 200.0 BRL 2070-130100 3
1,2,4-Trimethylbenzene ug/L2815.0 200.0 80.1 2070-130100 2
1,2-Dibromo-3-chloropropane ug/L211 20 200.0 BRL 2070-130106 8
1,2-Dibromoethane ug/L2105.0 200.0 BRL 2070-130105 2
1,2-Dichlorobenzene ug/L2025.0 200.0 BRL 2070-130101 0.1
1,2-Dichloroethane ug/L1985.0 200.0 BRL 2070-13099 0.2
1,2-Dichloropropane ug/L2045.0 200.0 BRL 2070-130102 3
1,3,5-Trimethylbenzene ug/L2215.0 200.0 17.6 2070-130102 3
1,3-Dichlorobenzene ug/L2035.0 200.0 BRL 2070-130102 0.5
1,3-Dichloropropane ug/L2145.0 200.0 BRL 2070-130107 0.7
1,4-Dichlorobenzene ug/L2005.0 200.0 BRL 2070-130100 0.9
2,2-Dichloropropane ug/L21320 200.0 BRL 2070-130107 3
2-Chlorotoluene ug/L2015.0 200.0 BRL 2070-130101 2
4-Chlorotoluene ug/L2025.0 200.0 BRL 2070-130101 1
4-Isopropyltoluene ug/L2225.0 200.0 4.77 2070-130109 1
Acetone ug/L319 100 400.0 BRL 2040-16080 5
Benzene ug/L2885.0 200.0 93.3 2070-13097 3
Bromobenzene ug/L2105.0 200.0 BRL 2070-130105 1
Bromochloromethane ug/L2105.0 200.0 BRL 2070-130105 4
Bromodichloromethane ug/L2065.0 200.0 BRL 2070-130103 3
Bromoform ug/L2145.0 200.0 BRL 2070-130107 2
Bromomethane ug/L14810 200.0 BRL 2060-14074 16
Carbon Tetrachloride ug/L2105.0 200.0 BRL 2070-130105 4
Chlorobenzene ug/L1965.0 200.0 BRL 2070-13098 5
Chloroethane ug/L2005.0 200.0 BRL 2060-140100 5
Chloroform ug/L2095.0 200.0 1.16 2070-130104 3
Chloromethane ug/L1725.0 200.0 BRL 2060-14086 5
cis-1,2-Dichloroethylene ug/L1985.0 200.0 BRL 2070-13099 1
cis-1,3-Dichloropropylene ug/L2185.0 200.0 BRL 2070-130109 1
Dibromochloromethane ug/L2055.0 200.0 BRL 2070-130103 3
Dibromomethane ug/L2165.0 200.0 BRL 2070-130108 2
Dichlorodifluoromethane ug/L15410 200.0 BRL 2060-14077 6
Ethanol ug/L5130 2000 5000 BRL 2060-140103 7
Ethylbenzene ug/L2025.0 200.0 BRL 2070-130101 3
Hexachlorobutadiene ug/L20120 200.0 BRL 2070-130101 2
Isopropyl Ether ug/L2085.0 200.0 10.8 2070-13098 1
Isopropylbenzene (Cumene)ug/L2225.0 200.0 9.54 2070-130106 2
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 72 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0098 - SM6200 B
Matrix Spike Dup (P0A0098-MSD1)Prepared & Analyzed: 01/07/20 Source: 0010027-12
m,p-Xylenes ug/L43810 400.0 26.9 2070-130103 6
Methyl Butyl Ketone (2-Hexanone)ug/L20010 200.0 BRL 2060-140100 2
Methyl Ethyl Ketone (2-Butanone)ug/L17350 200.0 BRL 2060-14086 8
Methyl Isobutyl Ketone ug/L20110 200.0 BRL 2060-140101 0.2
Methylene Chloride ug/L19420 200.0 0.980 2070-13096 2
Methyl-tert-Butyl Ether ug/L46710 200.0 255 2070-130106 0.2
Naphthalene ug/L36610 200.0 1210 2070-130NR 7
n-Butylbenzene ug/L2085.0 200.0 3.94 2170-130102 2
n-Propylbenzene ug/L2065.0 200.0 1.29 1870-130102 3
o-Xylene ug/L2675.0 200.0 69.8 2070-13099 5
sec-Butylbenzene ug/L2145.0 200.0 6.03 2070-130104 3
Styrene ug/L2095.0 200.0 BRL 2070-130105 0.5
tert-Amyl Alcohol ug/L1.00E10 100 200.0 910 2070-130NR 0
tert-Amyl Methyl Ether ug/L442 100 400.0 3.70 2070-130109 0.3
tert-Butyl Alcohol ug/L1070100 400.0 655 2070-130103 2
tert-Butylbenzene ug/L2075.0 200.0 BRL 2070-130103 4
tert-Butyl Ethyl Ether ug/L426 100 400.0 BRL 2070-130107 0.9
tert-Butyl Formate ug/L386 100 400.0 BRL 2070-13097 0.3
Tetrachloroethylene ug/L2085.0 200.0 BRL 2070-130104 6
Toluene ug/L2085.0 200.0 0.570 2070-130103 3
trans-1,2-Dichloroethylene ug/L1995.0 200.0 BRL 2070-130100 3
trans-1,3-Dichloropropylene ug/L2165.0 200.0 BRL 2070-130108 0.6
Trichloroethylene ug/L2055.0 200.0 BRL 2070-130102 5
Trichlorofluoromethane ug/L1875.0 200.0 BRL 2060-14094 6
Vinyl acetate ug/L21650 200.0 BRL 2060-140108 0.7
Vinyl chloride ug/L1845.0 200.0 BRL 2060-14092 6
Xylenes, total ug/L70615 600.0 96.7 2070-130101 5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.3
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9848.8
ug/L 50.00 70-130Surrogate: Toluene-d8 9849.2
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 73 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0110 - SM6200 B
Blank (P0A0110-BLK1)Prepared & Analyzed: 01/07/20
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL10
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL1.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethanol ug/LBRL200
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 74 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0110 - SM6200 B
Blank (P0A0110-BLK1)Prepared & Analyzed: 01/07/20
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL1.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL0.50
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Amyl Alcohol ug/LBRL10
tert-Amyl Methyl Ether ug/LBRL10
tert-Butyl Alcohol ug/LBRL10
tert-Butylbenzene ug/LBRL0.50
tert-Butyl Ethyl Ether ug/LBRL10
tert-Butyl Formate ug/LBRL10
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL5.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10351.6
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10552.3
ug/L 50.00 70-130Surrogate: Toluene-d8 9647.9
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 75 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0110 - SM6200 B
LCS (P0A0110-BS1)Prepared & Analyzed: 01/07/20
1,1,1,2-Tetrachloroethane ug/L20.3 0.50 20.00 70-130101
1,1,1-Trichloroethane ug/L21.3 0.50 20.00 70-130107
1,1,2,2-Tetrachloroethane ug/L19.4 0.50 20.00 70-13097
1,1,2-Trichloroethane ug/L19.7 0.50 20.00 70-13098
1,1-Dichloroethane ug/L20.6 0.50 20.00 70-130103
1,1-Dichloroethylene ug/L21.5 0.50 20.00 70-130107
1,1-Dichloropropylene ug/L22.7 0.50 20.00 70-130114
1,2,3-Trichlorobenzene ug/L19.7 0.50 20.00 70-13099
1,2,3-Trichloropropane ug/L19.6 0.50 20.00 70-13098
1,2,4-Trichlorobenzene ug/L20.0 0.50 20.00 70-130100
1,2,4-Trimethylbenzene ug/L20.9 0.50 20.00 70-130105
1,2-Dibromo-3-chloropropane ug/L18.5 2.0 20.00 70-13093
1,2-Dibromoethane ug/L20.1 0.50 20.00 70-130101
1,2-Dichlorobenzene ug/L19.8 0.50 20.00 70-13099
1,2-Dichloroethane ug/L19.0 0.50 20.00 70-13095
1,2-Dichloropropane ug/L20.8 0.50 20.00 70-130104
1,3,5-Trimethylbenzene ug/L21.0 0.50 20.00 70-130105
1,3-Dichlorobenzene ug/L20.5 0.50 20.00 70-130102
1,3-Dichloropropane ug/L20.1 0.50 20.00 70-130100
1,4-Dichlorobenzene ug/L19.3 0.50 20.00 70-13096
2,2-Dichloropropane ug/L20.8 2.0 20.00 70-130104
2-Chlorotoluene ug/L20.5 0.50 20.00 70-130103
4-Chlorotoluene ug/L20.4 0.50 20.00 70-130102
4-Isopropyltoluene ug/L22.0 0.50 20.00 70-130110
Acetone ug/L37.9 10 40.00 40-16095
Benzene ug/L21.2 0.50 20.00 70-130106
Bromobenzene ug/L19.4 0.50 20.00 70-13097
Bromochloromethane ug/L19.0 0.50 20.00 70-13095
Bromodichloromethane ug/L20.3 0.50 20.00 70-130101
Bromoform ug/L19.6 0.50 20.00 70-13098
Bromomethane ug/L24.4 1.0 20.00 60-140122
Carbon Tetrachloride ug/L22.1 0.50 20.00 70-130110
Chlorobenzene ug/L19.7 0.50 20.00 70-13098
Chloroethane ug/L23.3 0.50 20.00 60-140117
Chloroform ug/L20.2 0.50 20.00 70-130101
Chloromethane ug/L23.0 0.50 20.00 60-140115
cis-1,2-Dichloroethylene ug/L19.9 0.50 20.00 70-130100
cis-1,3-Dichloropropylene ug/L22.1 0.50 20.00 70-130111
Dibromochloromethane ug/L19.6 0.50 20.00 70-13098
Dibromomethane ug/L20.2 0.50 20.00 70-130101
Dichlorodifluoromethane ug/L29.6 1.0 20.00 60-140148
Ethanol ug/L466 200 500.0 60-14093
Ethylbenzene ug/L21.0 0.50 20.00 70-130105
Hexachlorobutadiene ug/L20.4 2.0 20.00 70-130102
Isopropyl Ether ug/L19.6 0.50 20.00 70-13098
Isopropylbenzene (Cumene)ug/L22.5 0.50 20.00 70-130112
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 76 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0110 - SM6200 B
LCS (P0A0110-BS1)Prepared & Analyzed: 01/07/20
m,p-Xylenes ug/L43.1 1.0 40.00 70-130108
Methyl Butyl Ketone (2-Hexanone)ug/L18.5 1.0 20.00 60-14092
Methyl Ethyl Ketone (2-Butanone)ug/L18.6 5.0 20.00 60-14093
Methyl Isobutyl Ketone ug/L18.8 1.0 20.00 60-14094
Methylene Chloride ug/L20.2 2.0 20.00 70-130101
Methyl-tert-Butyl Ether ug/L20.3 1.0 20.00 70-130101
Naphthalene ug/L18.8 1.0 20.00 70-13094
n-Butylbenzene ug/L21.5 0.50 20.00 70-130108
n-Propylbenzene ug/L21.2 0.50 20.00 70-130106
o-Xylene ug/L20.9 0.50 20.00 70-130104
sec-Butylbenzene ug/L22.2 0.50 20.00 70-130111
Styrene ug/L21.8 0.50 20.00 70-130109
tert-Amyl Alcohol ug/L21.0 10 20.00 70-130105
tert-Amyl Methyl Ether ug/L42.1 10 40.00 70-130105
tert-Butyl Alcohol ug/L39.4 10 40.00 70-13099
tert-Butylbenzene ug/L22.5 0.50 20.00 70-130112
tert-Butyl Ethyl Ether ug/L41.2 10 40.00 70-130103
tert-Butyl Formate ug/L41.2 10 40.00 70-130103
Tetrachloroethylene ug/L21.6 0.50 20.00 70-130108
Toluene ug/L21.1 0.50 20.00 70-130105
trans-1,2-Dichloroethylene ug/L20.5 0.50 20.00 70-130102
trans-1,3-Dichloropropylene ug/L20.8 0.50 20.00 70-130104
Trichloroethylene ug/L20.8 0.50 20.00 70-130104
Trichlorofluoromethane ug/L25.2 0.50 20.00 60-140126
Vinyl acetate ug/L20.9 5.0 20.00 60-140105
Vinyl chloride ug/L26.7 0.50 20.00 60-140134
Xylenes, total ug/L64.0 1.5 60.00 70-130107
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10351.3
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9848.8
ug/L 50.00 70-130Surrogate: Toluene-d8 9849.1
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 77 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0110 - SM6200 B
LCS Dup (P0A0110-BSD1)Prepared & Analyzed: 01/07/20
1,1,1,2-Tetrachloroethane ug/L20.0 0.50 20.00 2070-130100 2
1,1,1-Trichloroethane ug/L20.7 0.50 20.00 2070-130104 3
1,1,2,2-Tetrachloroethane ug/L19.7 0.50 20.00 2070-13098 1
1,1,2-Trichloroethane ug/L19.9 0.50 20.00 2070-130100 1
1,1-Dichloroethane ug/L20.1 0.50 20.00 2070-130101 2
1,1-Dichloroethylene ug/L20.3 0.50 20.00 2070-130102 6
1,1-Dichloropropylene ug/L22.0 0.50 20.00 2070-130110 3
1,2,3-Trichlorobenzene ug/L20.3 0.50 20.00 2070-130102 3
1,2,3-Trichloropropane ug/L19.6 0.50 20.00 2070-13098 0.05
1,2,4-Trichlorobenzene ug/L19.9 0.50 20.00 2070-13099 0.8
1,2,4-Trimethylbenzene ug/L21.0 0.50 20.00 2070-130105 0.4
1,2-Dibromo-3-chloropropane ug/L18.1 2.0 20.00 2070-13090 2
1,2-Dibromoethane ug/L20.1 0.50 20.00 2070-130100 0.3
1,2-Dichlorobenzene ug/L19.4 0.50 20.00 2070-13097 2
1,2-Dichloroethane ug/L19.0 0.50 20.00 2070-13095 0
1,2-Dichloropropane ug/L20.8 0.50 20.00 2070-130104 0.4
1,3,5-Trimethylbenzene ug/L20.8 0.50 20.00 2070-130104 0.7
1,3-Dichlorobenzene ug/L20.3 0.50 20.00 2070-130102 0.8
1,3-Dichloropropane ug/L19.5 0.50 20.00 2070-13097 3
1,4-Dichlorobenzene ug/L19.9 0.50 20.00 2070-13099 3
2,2-Dichloropropane ug/L20.3 2.0 20.00 2070-130102 3
2-Chlorotoluene ug/L20.2 0.50 20.00 2070-130101 2
4-Chlorotoluene ug/L20.2 0.50 20.00 2070-130101 1
4-Isopropyltoluene ug/L21.8 0.50 20.00 2070-130109 0.9
Acetone ug/L38.4 10 40.00 2040-16096 1
Benzene ug/L21.0 0.50 20.00 2070-130105 0.9
Bromobenzene ug/L19.4 0.50 20.00 2070-13097 0.4
Bromochloromethane ug/L19.8 0.50 20.00 2070-13099 4
Bromodichloromethane ug/L20.3 0.50 20.00 2070-130102 0.1
Bromoform ug/L19.6 0.50 20.00 2070-13098 0.4
Bromomethane ug/L25.9 1.0 20.00 2060-140130 6
Carbon Tetrachloride ug/L21.8 0.50 20.00 2070-130109 1
Chlorobenzene ug/L20.0 0.50 20.00 2070-130100 1
Chloroethane ug/L22.8 0.50 20.00 2060-140114 2
Chloroform ug/L19.7 0.50 20.00 2070-13099 2
Chloromethane ug/L22.0 0.50 20.00 2060-140110 4
cis-1,2-Dichloroethylene ug/L19.3 0.50 20.00 2070-13096 3
cis-1,3-Dichloropropylene ug/L21.7 0.50 20.00 2070-130108 2
Dibromochloromethane ug/L19.5 0.50 20.00 2070-13098 0.7
Dibromomethane ug/L20.4 0.50 20.00 2070-130102 1
Dichlorodifluoromethane ug/L27.7 1.0 20.00 2060-140139 6
Ethanol ug/L392 200 500.0 2060-14078 17
Ethylbenzene ug/L20.9 0.50 20.00 2070-130105 0.5
Hexachlorobutadiene ug/L20.6 2.0 20.00 2070-130103 0.9
Isopropyl Ether ug/L19.4 0.50 20.00 2070-13097 0.9
Isopropylbenzene (Cumene)ug/L22.0 0.50 20.00 2070-130110 2
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 78 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0110 - SM6200 B
LCS Dup (P0A0110-BSD1)Prepared & Analyzed: 01/07/20
m,p-Xylenes ug/L42.7 1.0 40.00 2070-130107 1
Methyl Butyl Ketone (2-Hexanone)ug/L18.4 1.0 20.00 2060-14092 0.4
Methyl Ethyl Ketone (2-Butanone)ug/L19.1 5.0 20.00 2060-14095 3
Methyl Isobutyl Ketone ug/L19.6 1.0 20.00 2060-14098 4
Methylene Chloride ug/L19.7 2.0 20.00 2070-13098 2
Methyl-tert-Butyl Ether ug/L20.2 1.0 20.00 2070-130101 0.1
Naphthalene ug/L18.9 1.0 20.00 2070-13094 0.5
n-Butylbenzene ug/L20.9 0.50 20.00 2070-130104 3
n-Propylbenzene ug/L20.8 0.50 20.00 2070-130104 2
o-Xylene ug/L20.5 0.50 20.00 2070-130103 2
sec-Butylbenzene ug/L21.8 0.50 20.00 2070-130109 2
Styrene ug/L21.3 0.50 20.00 2070-130107 2
tert-Amyl Alcohol ug/L20.2 10 20.00 2070-130101 4
tert-Amyl Methyl Ether ug/L41.8 10 40.00 2070-130104 0.9
tert-Butyl Alcohol ug/L40.4 10 40.00 2070-130101 2
tert-Butylbenzene ug/L22.1 0.50 20.00 2070-130110 2
tert-Butyl Ethyl Ether ug/L41.0 10 40.00 2070-130103 0.4
tert-Butyl Formate ug/L41.0 10 40.00 2070-130103 0.4
Tetrachloroethylene ug/L21.7 0.50 20.00 2070-130108 0.3
Toluene ug/L20.8 0.50 20.00 2070-130104 1
trans-1,2-Dichloroethylene ug/L20.1 0.50 20.00 2070-130100 2
trans-1,3-Dichloropropylene ug/L21.1 0.50 20.00 2070-130106 2
Trichloroethylene ug/L20.4 0.50 20.00 2070-130102 2
Trichlorofluoromethane ug/L24.3 0.50 20.00 2060-140122 3
Vinyl acetate ug/L22.1 5.0 20.00 2060-140110 5
Vinyl chloride ug/L26.3 0.50 20.00 2060-140132 1
Xylenes, total ug/L63.2 1.5 60.00 2070-130105 1
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10050.2
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9547.7
ug/L 50.00 70-130Surrogate: Toluene-d8 9748.6
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 79 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0116 - SM6200 B
Blank (P0A0116-BLK1)Prepared & Analyzed: 01/08/20
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL10
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL1.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethanol ug/LBRL200
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 80 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0116 - SM6200 B
Blank (P0A0116-BLK1)Prepared & Analyzed: 01/08/20
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL1.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL0.50
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Amyl Alcohol ug/LBRL10
tert-Amyl Methyl Ether ug/LBRL10
tert-Butyl Alcohol ug/LBRL10
tert-Butylbenzene ug/LBRL0.50
tert-Butyl Ethyl Ether ug/LBRL10
tert-Butyl Formate ug/LBRL10
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL5.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10050.2
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9647.9
ug/L 50.00 70-130Surrogate: Toluene-d8 9849.0
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 81 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0116 - SM6200 B
LCS (P0A0116-BS1)Prepared & Analyzed: 01/08/20
1,1,1,2-Tetrachloroethane ug/L20.8 0.50 20.00 70-130104
1,1,1-Trichloroethane ug/L21.7 0.50 20.00 70-130109
1,1,2,2-Tetrachloroethane ug/L21.7 0.50 20.00 70-130108
1,1,2-Trichloroethane ug/L21.1 0.50 20.00 70-130105
1,1-Dichloroethane ug/L22.0 0.50 20.00 70-130110
1,1-Dichloroethylene ug/L21.5 0.50 20.00 70-130107
1,1-Dichloropropylene ug/L23.0 0.50 20.00 70-130115
1,2,3-Trichlorobenzene ug/L21.3 0.50 20.00 70-130107
1,2,3-Trichloropropane ug/L22.7 0.50 20.00 70-130114
1,2,4-Trichlorobenzene ug/L21.9 0.50 20.00 70-130109
1,2,4-Trimethylbenzene ug/L21.8 0.50 20.00 70-130109
1,2-Dibromo-3-chloropropane ug/L22.0 2.0 20.00 70-130110
1,2-Dibromoethane ug/L21.6 0.50 20.00 70-130108
1,2-Dichlorobenzene ug/L21.4 0.50 20.00 70-130107
1,2-Dichloroethane ug/L19.8 0.50 20.00 70-13099
1,2-Dichloropropane ug/L20.8 0.50 20.00 70-130104
1,3,5-Trimethylbenzene ug/L21.8 0.50 20.00 70-130109
1,3-Dichlorobenzene ug/L21.2 0.50 20.00 70-130106
1,3-Dichloropropane ug/L21.8 0.50 20.00 70-130109
1,4-Dichlorobenzene ug/L21.2 0.50 20.00 70-130106
2,2-Dichloropropane ug/L21.8 2.0 20.00 70-130109
2-Chlorotoluene ug/L21.4 0.50 20.00 70-130107
4-Chlorotoluene ug/L21.6 0.50 20.00 70-130108
4-Isopropyltoluene ug/L22.5 0.50 20.00 70-130112
Acetone ug/L37.2 10 40.00 40-16093
Benzene ug/L21.3 0.50 20.00 70-130107
Bromobenzene ug/L22.0 0.50 20.00 70-130110
Bromochloromethane ug/L21.9 0.50 20.00 70-130109
Bromodichloromethane ug/L21.3 0.50 20.00 70-130106
Bromoform ug/L22.0 0.50 20.00 70-130110
Bromomethane ug/L15.9 1.0 20.00 60-14080
Carbon Tetrachloride ug/L22.2 0.50 20.00 70-130111
Chlorobenzene ug/L21.2 0.50 20.00 70-130106
Chloroethane ug/L19.8 0.50 20.00 60-14099
Chloroform ug/L21.2 0.50 20.00 70-130106
Chloromethane ug/L15.4 0.50 20.00 60-14077
cis-1,2-Dichloroethylene ug/L20.4 0.50 20.00 70-130102
cis-1,3-Dichloropropylene ug/L22.6 0.50 20.00 70-130113
Dibromochloromethane ug/L22.0 0.50 20.00 70-130110
Dibromomethane ug/L22.2 0.50 20.00 70-130111
Dichlorodifluoromethane ug/L14.8 1.0 20.00 60-14074
Ethanol ug/L522 200 500.0 60-140104
Ethylbenzene ug/L21.2 0.50 20.00 70-130106
Hexachlorobutadiene ug/L20.8 2.0 20.00 70-130104
Isopropyl Ether ug/L20.4 0.50 20.00 70-130102
Isopropylbenzene (Cumene)ug/L22.9 0.50 20.00 70-130114
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 82 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0116 - SM6200 B
LCS (P0A0116-BS1)Prepared & Analyzed: 01/08/20
m,p-Xylenes ug/L44.1 1.0 40.00 70-130110
Methyl Butyl Ketone (2-Hexanone)ug/L20.7 1.0 20.00 60-140103
Methyl Ethyl Ketone (2-Butanone)ug/L19.1 5.0 20.00 60-14096
Methyl Isobutyl Ketone ug/L20.8 1.0 20.00 60-140104
Methylene Chloride ug/L20.3 2.0 20.00 70-130101
Methyl-tert-Butyl Ether ug/L22.3 1.0 20.00 70-130112
Naphthalene ug/L21.1 1.0 20.00 70-130106
n-Butylbenzene ug/L22.1 0.50 20.00 70-130111
n-Propylbenzene ug/L21.8 0.50 20.00 70-130109
o-Xylene ug/L21.5 0.50 20.00 70-130108
sec-Butylbenzene ug/L22.4 0.50 20.00 70-130112
Styrene ug/L22.2 0.50 20.00 70-130111
tert-Amyl Alcohol ug/L20.6 10 20.00 70-130103
tert-Amyl Methyl Ether ug/L44.5 10 40.00 70-130111
tert-Butyl Alcohol ug/L44.3 10 40.00 70-130111
tert-Butylbenzene ug/L22.3 0.50 20.00 70-130112
tert-Butyl Ethyl Ether ug/L43.7 10 40.00 70-130109
tert-Butyl Formate ug/L45.1 10 40.00 70-130113
Tetrachloroethylene ug/L22.5 0.50 20.00 70-130112
Toluene ug/L21.7 0.50 20.00 70-130108
trans-1,2-Dichloroethylene ug/L21.1 0.50 20.00 70-130105
trans-1,3-Dichloropropylene ug/L22.8 0.50 20.00 70-130114
Trichloroethylene ug/L21.5 0.50 20.00 70-130108
Trichlorofluoromethane ug/L19.1 0.50 20.00 60-14096
Vinyl acetate ug/L21.5 5.0 20.00 60-140107
Vinyl chloride ug/L17.2 0.50 20.00 60-14086
Xylenes, total ug/L65.6 1.5 60.00 70-130109
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10250.8
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9748.4
ug/L 50.00 70-130Surrogate: Toluene-d8 9949.5
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 83 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0130 - SM6200 B
Blank (P0A0130-BLK1)Prepared & Analyzed: 01/09/20
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL10
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL1.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethanol ug/LBRL200
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 84 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0130 - SM6200 B
Blank (P0A0130-BLK1)Prepared & Analyzed: 01/09/20
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL1.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL0.50
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Amyl Alcohol ug/LBRL10
tert-Amyl Methyl Ether ug/LBRL10
tert-Butyl Alcohol ug/LBRL10
tert-Butylbenzene ug/LBRL0.50
tert-Butyl Ethyl Ether ug/LBRL10
tert-Butyl Formate ug/LBRL10
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL5.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10251.1
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9547.7
ug/L 50.00 70-130Surrogate: Toluene-d8 9849.0
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 85 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0130 - SM6200 B
LCS (P0A0130-BS1)Prepared & Analyzed: 01/09/20
1,1,1,2-Tetrachloroethane ug/L20.2 0.50 20.00 70-130101
1,1,1-Trichloroethane ug/L21.2 0.50 20.00 70-130106
1,1,2,2-Tetrachloroethane ug/L20.7 0.50 20.00 70-130103
1,1,2-Trichloroethane ug/L20.9 0.50 20.00 70-130105
1,1-Dichloroethane ug/L21.6 0.50 20.00 70-130108
1,1-Dichloroethylene ug/L20.8 0.50 20.00 70-130104
1,1-Dichloropropylene ug/L21.5 0.50 20.00 70-130108
1,2,3-Trichlorobenzene ug/L20.5 0.50 20.00 70-130102
1,2,3-Trichloropropane ug/L21.8 0.50 20.00 70-130109
1,2,4-Trichlorobenzene ug/L20.3 0.50 20.00 70-130102
1,2,4-Trimethylbenzene ug/L20.8 0.50 20.00 70-130104
1,2-Dibromo-3-chloropropane ug/L19.7 2.0 20.00 70-13098
1,2-Dibromoethane ug/L20.7 0.50 20.00 70-130103
1,2-Dichlorobenzene ug/L20.4 0.50 20.00 70-130102
1,2-Dichloroethane ug/L19.9 0.50 20.00 70-130100
1,2-Dichloropropane ug/L21.0 0.50 20.00 70-130105
1,3,5-Trimethylbenzene ug/L20.7 0.50 20.00 70-130104
1,3-Dichlorobenzene ug/L20.4 0.50 20.00 70-130102
1,3-Dichloropropane ug/L21.4 0.50 20.00 70-130107
1,4-Dichlorobenzene ug/L20.1 0.50 20.00 70-130101
2,2-Dichloropropane ug/L21.0 2.0 20.00 70-130105
2-Chlorotoluene ug/L20.5 0.50 20.00 70-130102
4-Chlorotoluene ug/L20.4 0.50 20.00 70-130102
4-Isopropyltoluene ug/L20.9 0.50 20.00 70-130104
Acetone ug/L39.0 10 40.00 40-16097
Benzene ug/L21.2 0.50 20.00 70-130106
Bromobenzene ug/L21.2 0.50 20.00 70-130106
Bromochloromethane ug/L21.1 0.50 20.00 70-130105
Bromodichloromethane ug/L21.3 0.50 20.00 70-130107
Bromoform ug/L21.3 0.50 20.00 70-130106
Bromomethane ug/L15.5 1.0 20.00 60-14077
Carbon Tetrachloride ug/L20.6 0.50 20.00 70-130103
Chlorobenzene ug/L20.3 0.50 20.00 70-130101
Chloroethane ug/L20.8 0.50 20.00 60-140104
Chloroform ug/L21.0 0.50 20.00 70-130105
Chloromethane ug/L15.3 0.50 20.00 60-14076
cis-1,2-Dichloroethylene ug/L20.1 0.50 20.00 70-130100
cis-1,3-Dichloropropylene ug/L22.6 0.50 20.00 70-130113
Dibromochloromethane ug/L21.4 0.50 20.00 70-130107
Dibromomethane ug/L21.5 0.50 20.00 70-130107
Dichlorodifluoromethane ug/L16.1 1.0 20.00 60-14080
Ethanol ug/L473 200 500.0 60-14095
Ethylbenzene ug/L20.4 0.50 20.00 70-130102
Hexachlorobutadiene ug/L20.7 2.0 20.00 70-130104
Isopropyl Ether ug/L19.8 0.50 20.00 70-13099
Isopropylbenzene (Cumene)ug/L21.5 0.50 20.00 70-130108
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 86 of 91
1/15/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010027
Time Submitted: 1/3/2020 2:10:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0130 - SM6200 B
LCS (P0A0130-BS1)Prepared & Analyzed: 01/09/20
m,p-Xylenes ug/L41.9 1.0 40.00 70-130105
Methyl Butyl Ketone (2-Hexanone)ug/L19.6 1.0 20.00 60-14098
Methyl Ethyl Ketone (2-Butanone)ug/L19.0 5.0 20.00 60-14095
Methyl Isobutyl Ketone ug/L20.1 1.0 20.00 60-140100
Methylene Chloride ug/L19.3 2.0 20.00 70-13096
Methyl-tert-Butyl Ether ug/L22.1 1.0 20.00 70-130111
Naphthalene ug/L20.3 1.0 20.00 70-130101
n-Butylbenzene ug/L20.4 0.50 20.00 70-130102
n-Propylbenzene ug/L20.5 0.50 20.00 70-130103
o-Xylene ug/L20.9 0.50 20.00 70-130104
sec-Butylbenzene ug/L21.3 0.50 20.00 70-130106
Styrene ug/L21.8 0.50 20.00 70-130109
tert-Amyl Alcohol ug/L27.3 10 20.00 70-130137
tert-Amyl Methyl Ether ug/L44.8 10 40.00 70-130112
tert-Butyl Alcohol ug/L42.2 10 40.00 70-130105
tert-Butylbenzene ug/L20.8 0.50 20.00 70-130104
tert-Butyl Ethyl Ether ug/L43.3 10 40.00 70-130108
tert-Butyl Formate ug/L44.8 10 40.00 70-130112
Tetrachloroethylene ug/L20.9 0.50 20.00 70-130105
Toluene ug/L21.3 0.50 20.00 70-130106
trans-1,2-Dichloroethylene ug/L20.6 0.50 20.00 70-130103
trans-1,3-Dichloropropylene ug/L22.3 0.50 20.00 70-130112
Trichloroethylene ug/L20.5 0.50 20.00 70-130103
Trichlorofluoromethane ug/L19.0 0.50 20.00 60-14095
Vinyl acetate ug/L21.8 5.0 20.00 60-140109
Vinyl chloride ug/L19.4 0.50 20.00 60-14097
Xylenes, total ug/L62.8 1.5 60.00 70-130105
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10050.2
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9647.8
ug/L 50.00 70-130Surrogate: Toluene-d8 9849.2
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 87 of 91
Sample Extraction Data
Prep Method: SM6200 B
Lab Number Batch Date/TimeInitialFinal
P0A00870010027-01 01/06/20 11:0010 10mL mL
P0A00870010027-02 01/06/20 11:0010 10mL mL
P0A00870010027-03 01/06/20 11:0010 10mL mL
P0A00870010027-04 01/06/20 11:0010 10mL mL
P0A00870010027-04 01/06/20 11:0010 10mL mL
P0A01100010027-05 01/07/20 8:4210 10mL mL
P0A01100010027-06 01/07/20 8:4210 10mL mL
P0A00870010027-07 01/06/20 11:0010 10mL mL
P0A01160010027-08 01/08/20 9:4710 10mL mL
P0A01160010027-08 01/08/20 9:4710 10mL mL
P0A01160010027-09 01/08/20 9:4710 10mL mL
P0A01160010027-09 01/08/20 9:4710 10mL mL
P0A00870010027-10 01/06/20 11:0010 10mL mL
P0A00870010027-10 01/06/20 11:0010 10mL mL
P0A01160010027-11 01/08/20 9:4710 10mL mL
P0A01160010027-11 01/08/20 9:4710 10mL mL
P0A00980010027-12 01/07/20 10:0010 10mL mL
P0A00980010027-12 01/07/20 10:0010 10mL mL
P0A01160010027-13 01/08/20 9:4710 10mL mL
P0A01300010027-14 01/09/20 10:2110 10mL mL
P0A01300010027-14 01/09/20 10:2110 10mL mL
P0A01300010027-14 01/09/20 10:2110 10mL mL
P0A01160010027-15 01/08/20 9:4710 10mL mL
P0A01300010027-16 01/09/20 10:2110 10mL mL
P0A01160010027-17 01/08/20 9:4710 10mL mL
P0A01160010027-17 01/08/20 9:4710 10mL mL
P0A00870010027-18 01/06/20 11:0010 10mL mL
P0A00870010027-19 01/06/20 11:0010 10mL mL
P0A01160010027-20 01/08/20 9:4710 10mL mL
P0A01160010027-20 01/08/20 9:4710 10mL mL
P0A00870010027-21 01/06/20 11:0010 10mL mL
P0A00870010027-22 01/06/20 11:0010 10mL mL
P0A00870010027-23 01/06/20 11:0010 10mL mL
P0A01160010027-24 01/08/20 9:4710 10mL mL
P0A01160010027-25 01/08/20 9:4710 10mL mL
P0A01160010027-26 01/08/20 9:4710 10mL mL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 88 of 91
Page 89 of 91
Page 90 of 91
Page 91 of 91
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
1/27/20 11:54
Withers & Ravenel
Kevin Buchanan
115 Mackenan Dr. BUILDING 117
Cary, NC 27511
Project: Billy’s Mini Mart
Project No.: NCDEQ#3327 02170214.74
Lab Submittal Date: 01/22/2020
Work Order: 0010313
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOINT ANALYTICAL
Project Management Manager
Reviewed ByAngela D. Overcash Angela D. Overcash
Project Management Manager
Data Qualifiers Key Reference:
M Matrix spike outside of the control limits.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Sample Receipt Summary
01/27/2020
Work Order: 0010313
Client Sample ID MatrixLab Sample ID Date/Time Sampled Date/Time Received
0010313-01 01/20/20 12:30WSW-1 01/22/20 10:00Water
0010313-02 01/20/20 12:50WSW-3 01/22/20 10:00Water
0010313-03 01/20/20 13:25WSW-4 01/22/20 10:00Water
Samples were received in good condition at 2.1 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Client ID ResultParameterMethod UnitsWaypoint ID
Work Order: 0010313
01/27/2020
Summary of Detections
17 ug/L0010313-01 WSW-1 Chloromethane *SM6200 B
0.94 ug/L0010313-02 WSW-3 Chloroform *SM6200 B
8.2 ug/L0010313-02 WSW-3 Chloromethane *SM6200 B
1.4 ug/L0010313-03 WSW-4 Chloroform *SM6200 B
7.9 ug/L0010313-03 WSW-4 Chloromethane *SM6200 B
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/27/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-1
Sample ID: 0010313-01
Work Order: 0010313
Time Collected: 01/20/20 12:30
Time Submitted: 01/22/20 10:00
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A038112.0 1/23/20 17:53 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A038112.0 1/23/20 17:53 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A03811101/23/20 17:53 JLBug/L 0.31Acetone
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.048Benzene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.040Bromoform
BRL *SM6200 B P0A038111.0 1/23/20 17:53 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.076Chloroform
17 *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0A038111.0 1/23/20 17:53 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A038112001/23/20 17:53 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/27/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-1
Sample ID: 0010313-01
Work Order: 0010313
Time Collected: 01/20/20 12:30
Time Submitted: 01/22/20 10:00
NCDEQ#3327 02170214.74
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0A038112.0 1/23/20 17:53 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A038111.0 1/23/20 17:53 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A038111.0 1/23/20 17:53 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A038115.0 1/23/20 17:53 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A038111.0 1/23/20 17:53 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A038112.0 1/23/20 17:53 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0A038111.0 1/23/20 17:53 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A038111.0 1/23/20 17:53 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.047Styrene
BRL *SM6200 B P0A03811101/23/20 17:53 JLBug/L 0.72tert-Amyl Alcohol
BRL *SM6200 B P0A03811101/23/20 17:53 JLBug/L 0.10tert-Amyl Methyl Ether
BRL *SM6200 B P0A03811101/23/20 17:53 JLBug/L 0.64tert-Butyl Alcohol
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A03811101/23/20 17:53 JLBug/L 0.059tert-Butyl Ethyl Ether
BRL *SM6200 B P0A03811101/23/20 17:53 JLBug/L 0.25tert-Butyl Formate
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.044Toluene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A038115.0 1/23/20 17:53 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0A038110.50 1/23/20 17:53 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0A038111.5 1/23/20 17:53 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13094 %4-Bromofluorobenzene
70-13094 %Dibromofluoromethane
70-13096 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/27/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-3
Sample ID: 0010313-02
Work Order: 0010313
Time Collected: 01/20/20 12:50
Time Submitted: 01/22/20 10:00
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A038112.0 1/23/20 18:18 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A038112.0 1/23/20 18:18 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A03811101/23/20 18:18 JLBug/L 0.31Acetone
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.048Benzene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.040Bromoform
BRL *SM6200 B P0A038111.0 1/23/20 18:18 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.22Chloroethane
0.94 *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.076Chloroform
8.2 *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0A038111.0 1/23/20 18:18 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A038112001/23/20 18:18 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/27/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-3
Sample ID: 0010313-02
Work Order: 0010313
Time Collected: 01/20/20 12:50
Time Submitted: 01/22/20 10:00
NCDEQ#3327 02170214.74
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0A038112.0 1/23/20 18:18 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A038111.0 1/23/20 18:18 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A038111.0 1/23/20 18:18 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A038115.0 1/23/20 18:18 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A038111.0 1/23/20 18:18 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A038112.0 1/23/20 18:18 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0A038111.0 1/23/20 18:18 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A038111.0 1/23/20 18:18 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.047Styrene
BRL *SM6200 B P0A03811101/23/20 18:18 JLBug/L 0.72tert-Amyl Alcohol
BRL *SM6200 B P0A03811101/23/20 18:18 JLBug/L 0.10tert-Amyl Methyl Ether
BRL *SM6200 B P0A03811101/23/20 18:18 JLBug/L 0.64tert-Butyl Alcohol
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A03811101/23/20 18:18 JLBug/L 0.059tert-Butyl Ethyl Ether
BRL *SM6200 B P0A03811101/23/20 18:18 JLBug/L 0.25tert-Butyl Formate
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.044Toluene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A038115.0 1/23/20 18:18 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0A038110.50 1/23/20 18:18 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0A038111.5 1/23/20 18:18 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13094 %4-Bromofluorobenzene
70-13095 %Dibromofluoromethane
70-13095 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/27/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-4
Sample ID: 0010313-03
Work Order: 0010313
Time Collected: 01/20/20 13:25
Time Submitted: 01/22/20 10:00
NCDEQ#3327 02170214.74
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A038112.0 1/23/20 18:43 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A038112.0 1/23/20 18:43 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A03811101/23/20 18:43 JLBug/L 0.31Acetone
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.048Benzene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.040Bromoform
BRL *SM6200 B P0A038111.0 1/23/20 18:43 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.22Chloroethane
1.4 *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.076Chloroform
7.9 *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0A038111.0 1/23/20 18:43 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A038112001/23/20 18:43 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/27/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Sample Matrix: Water
Client Sample ID: WSW-4
Sample ID: 0010313-03
Work Order: 0010313
Time Collected: 01/20/20 13:25
Time Submitted: 01/22/20 10:00
NCDEQ#3327 02170214.74
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0A038112.0 1/23/20 18:43 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A038111.0 1/23/20 18:43 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A038111.0 1/23/20 18:43 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A038115.0 1/23/20 18:43 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A038111.0 1/23/20 18:43 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A038112.0 1/23/20 18:43 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0A038111.0 1/23/20 18:43 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A038111.0 1/23/20 18:43 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.047Styrene
BRL *SM6200 B P0A03811101/23/20 18:43 JLBug/L 0.72tert-Amyl Alcohol
BRL *SM6200 B P0A03811101/23/20 18:43 JLBug/L 0.10tert-Amyl Methyl Ether
BRL *SM6200 B P0A03811101/23/20 18:43 JLBug/L 0.64tert-Butyl Alcohol
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A03811101/23/20 18:43 JLBug/L 0.059tert-Butyl Ethyl Ether
BRL *SM6200 B P0A03811101/23/20 18:43 JLBug/L 0.25tert-Butyl Formate
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.044Toluene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A038115.0 1/23/20 18:43 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0A038110.50 1/23/20 18:43 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0A038111.5 1/23/20 18:43 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13094 %4-Bromofluorobenzene
70-13094 %Dibromofluoromethane
70-13096 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/27/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010313
Time Submitted: 1/22/2020 10:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0381 - 5030B
Blank (P0A0381-BLK1)Prepared & Analyzed: 01/23/20
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL10
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL1.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethanol ug/LBRL200
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/27/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010313
Time Submitted: 1/22/2020 10:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0381 - 5030B
Blank (P0A0381-BLK1)Prepared & Analyzed: 01/23/20
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL1.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL0.50
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Amyl Alcohol ug/LBRL10
tert-Amyl Methyl Ether ug/LBRL10
tert-Butyl Alcohol ug/LBRL10
tert-Butylbenzene ug/LBRL0.50
tert-Butyl Ethyl Ether ug/LBRL10
tert-Butyl Formate ug/LBRL10
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL5.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9547.6
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9447.0
ug/L 50.00 70-130Surrogate: Toluene-d8 9547.4
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/27/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010313
Time Submitted: 1/22/2020 10:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0381 - 5030B
Blank (P0A0381-BLK2)Prepared & Analyzed: 01/23/20
1,1,1,2-Tetrachloroethane ug/LBRL5.0
1,1,1-Trichloroethane ug/LBRL5.0
1,1,2,2-Tetrachloroethane ug/LBRL5.0
1,1,2-Trichloroethane ug/LBRL5.0
1,1-Dichloroethane ug/LBRL5.0
1,1-Dichloroethylene ug/LBRL5.0
1,1-Dichloropropylene ug/LBRL5.0
1,2,3-Trichlorobenzene ug/LBRL5.0
1,2,3-Trichloropropane ug/LBRL5.0
1,2,4-Trichlorobenzene ug/LBRL5.0
1,2,4-Trimethylbenzene ug/LBRL5.0
1,2-Dibromo-3-chloropropane ug/LBRL20
1,2-Dibromoethane ug/LBRL5.0
1,2-Dichlorobenzene ug/LBRL5.0
1,2-Dichloroethane ug/LBRL5.0
1,2-Dichloropropane ug/LBRL5.0
1,3,5-Trimethylbenzene ug/LBRL5.0
1,3-Dichlorobenzene ug/LBRL5.0
1,3-Dichloropropane ug/LBRL5.0
1,4-Dichlorobenzene ug/LBRL5.0
2,2-Dichloropropane ug/LBRL20
2-Chlorotoluene ug/LBRL5.0
4-Chlorotoluene ug/LBRL5.0
4-Isopropyltoluene ug/LBRL5.0
Acetone ug/LBRL100
Benzene ug/LBRL5.0
Bromobenzene ug/LBRL5.0
Bromochloromethane ug/LBRL5.0
Bromodichloromethane ug/LBRL5.0
Bromoform ug/LBRL5.0
Bromomethane ug/LBRL10
Carbon Tetrachloride ug/LBRL5.0
Chlorobenzene ug/LBRL5.0
Chloroethane ug/LBRL5.0
Chloroform ug/LBRL5.0
Chloromethane ug/LBRL5.0
cis-1,2-Dichloroethylene ug/LBRL5.0
cis-1,3-Dichloropropylene ug/LBRL5.0
Dibromochloromethane ug/LBRL5.0
Dibromomethane ug/LBRL5.0
Dichlorodifluoromethane ug/LBRL10
Ethanol ug/LBRL2000
Ethylbenzene ug/LBRL5.0
Hexachlorobutadiene ug/LBRL20
Isopropyl Ether ug/LBRL5.0
Isopropylbenzene (Cumene)ug/LBRL5.0
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/27/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010313
Time Submitted: 1/22/2020 10:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0381 - 5030B
Blank (P0A0381-BLK2)Prepared & Analyzed: 01/23/20
m,p-Xylenes ug/LBRL10
Methyl Butyl Ketone (2-Hexanone)ug/LBRL10
Methyl Ethyl Ketone (2-Butanone)ug/LBRL50
Methyl Isobutyl Ketone ug/LBRL10
Methylene Chloride ug/LBRL20
Methyl-tert-Butyl Ether ug/LBRL10
Naphthalene ug/LBRL10
n-Butylbenzene ug/LBRL5.0
n-Propylbenzene ug/LBRL5.0
o-Xylene ug/LBRL5.0
sec-Butylbenzene ug/LBRL5.0
Styrene ug/LBRL5.0
tert-Amyl Alcohol ug/LBRL100
tert-Amyl Methyl Ether ug/LBRL100
tert-Butyl Alcohol ug/LBRL100
tert-Butylbenzene ug/LBRL5.0
tert-Butyl Ethyl Ether ug/LBRL100
tert-Butyl Formate ug/LBRL100
Tetrachloroethylene ug/LBRL5.0
Toluene ug/LBRL5.0
trans-1,2-Dichloroethylene ug/LBRL5.0
trans-1,3-Dichloropropylene ug/LBRL5.0
Trichloroethylene ug/LBRL5.0
Trichlorofluoromethane ug/LBRL5.0
Vinyl acetate ug/LBRL50
Vinyl chloride ug/LBRL5.0
Xylenes, total ug/LBRL15
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9547.4
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9447.0
ug/L 50.00 70-130Surrogate: Toluene-d8 9447.1
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/27/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010313
Time Submitted: 1/22/2020 10:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0381 - 5030B
LCS (P0A0381-BS1)Prepared & Analyzed: 01/23/20
1,1,1,2-Tetrachloroethane ug/L18.2 0.50 20.00 70-13091
1,1,1-Trichloroethane ug/L21.0 0.50 20.00 70-130105
1,1,2,2-Tetrachloroethane ug/L18.0 0.50 20.00 70-13090
1,1,2-Trichloroethane ug/L20.4 0.50 20.00 70-130102
1,1-Dichloroethane ug/L20.6 0.50 20.00 70-130103
1,1-Dichloroethylene ug/L20.8 0.50 20.00 70-130104
1,1-Dichloropropylene ug/L21.9 0.50 20.00 70-130110
1,2,3-Trichlorobenzene ug/L18.3 0.50 20.00 70-13092
1,2,3-Trichloropropane ug/L19.2 0.50 20.00 70-13096
1,2,4-Trichlorobenzene ug/L18.0 0.50 20.00 70-13090
1,2,4-Trimethylbenzene ug/L17.9 0.50 20.00 70-13090
1,2-Dibromo-3-chloropropane ug/L17.9 2.0 20.00 70-13090
1,2-Dibromoethane ug/L19.6 0.50 20.00 70-13098
1,2-Dichlorobenzene ug/L18.7 0.50 20.00 70-13093
1,2-Dichloroethane ug/L18.8 0.50 20.00 70-13094
1,2-Dichloropropane ug/L20.3 0.50 20.00 70-130102
1,3,5-Trimethylbenzene ug/L18.4 0.50 20.00 70-13092
1,3-Dichlorobenzene ug/L18.8 0.50 20.00 70-13094
1,3-Dichloropropane ug/L20.2 0.50 20.00 70-130101
1,4-Dichlorobenzene ug/L18.8 0.50 20.00 70-13094
2,2-Dichloropropane ug/L20.6 2.0 20.00 70-130103
2-Chlorotoluene ug/L17.8 0.50 20.00 70-13089
4-Chlorotoluene ug/L17.9 0.50 20.00 70-13090
4-Isopropyltoluene ug/L19.1 0.50 20.00 70-13096
Acetone ug/L36.7 10 40.00 40-16092
Benzene ug/L20.7 0.50 20.00 70-130104
Bromobenzene ug/L18.3 0.50 20.00 70-13092
Bromochloromethane ug/L21.4 0.50 20.00 70-130107
Bromodichloromethane ug/L19.6 0.50 20.00 70-13098
Bromoform ug/L17.4 0.50 20.00 70-13087
Bromomethane ug/L12.2 1.0 20.00 60-14061
Carbon Tetrachloride ug/L19.2 0.50 20.00 70-13096
Chlorobenzene ug/L20.0 0.50 20.00 70-130100
Chloroethane ug/L15.5 0.50 20.00 60-14078
Chloroform ug/L20.6 0.50 20.00 70-130103
Chloromethane ug/L16.5 0.50 20.00 60-14082
cis-1,2-Dichloroethylene ug/L19.5 0.50 20.00 70-13097
cis-1,3-Dichloropropylene ug/L20.6 0.50 20.00 70-130103
Dibromochloromethane ug/L18.3 0.50 20.00 70-13092
Dibromomethane ug/L20.5 0.50 20.00 70-130102
Dichlorodifluoromethane ug/L17.6 1.0 20.00 60-14088
Ethanol ug/L507 200 500.0 60-140101
Ethylbenzene ug/L19.8 0.50 20.00 70-13099
Hexachlorobutadiene ug/L20.8 2.0 20.00 70-130104
Isopropyl Ether ug/L19.4 0.50 20.00 70-13097
Isopropylbenzene (Cumene)ug/L19.4 0.50 20.00 70-13097
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/27/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010313
Time Submitted: 1/22/2020 10:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0381 - 5030B
LCS (P0A0381-BS1)Prepared & Analyzed: 01/23/20
m,p-Xylenes ug/L40.6 1.0 40.00 70-130102
Methyl Butyl Ketone (2-Hexanone)ug/L18.3 1.0 20.00 60-14092
Methyl Ethyl Ketone (2-Butanone)ug/L20.0 5.0 20.00 60-140100
Methyl Isobutyl Ketone ug/L19.3 1.0 20.00 60-14096
Methylene Chloride ug/L19.8 2.0 20.00 70-13099
Methyl-tert-Butyl Ether ug/L20.8 1.0 20.00 70-130104
Naphthalene ug/L15.5 1.0 20.00 70-13078
n-Butylbenzene ug/L17.7 0.50 20.00 70-13089
n-Propylbenzene ug/L18.5 0.50 20.00 70-13093
o-Xylene ug/L19.5 0.50 20.00 70-13098
sec-Butylbenzene ug/L19.3 0.50 20.00 70-13097
Styrene ug/L19.8 0.50 20.00 70-13099
tert-Amyl Alcohol ug/L20.1 10 20.00 70-130100
tert-Amyl Methyl Ether ug/L41.6 10 40.00 70-130104
tert-Butyl Alcohol ug/L35.1 10 40.00 70-13088
tert-Butylbenzene ug/L19.4 0.50 20.00 70-13097
tert-Butyl Ethyl Ether ug/L40.8 10 40.00 70-130102
tert-Butyl Formate ug/L34.4 10 40.00 70-13086
Tetrachloroethylene ug/L21.6 0.50 20.00 70-130108
Toluene ug/L20.4 0.50 20.00 70-130102
trans-1,2-Dichloroethylene ug/L20.2 0.50 20.00 70-130101
trans-1,3-Dichloropropylene ug/L20.1 0.50 20.00 70-130100
Trichloroethylene ug/L21.4 0.50 20.00 70-130107
Trichlorofluoromethane ug/L21.8 0.50 20.00 60-140109
Vinyl acetate ug/L17.7 5.0 20.00 60-14088
Vinyl chloride ug/L20.2 0.50 20.00 60-140101
Xylenes, total ug/L60.2 1.5 60.00 70-130100
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9346.6
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9446.8
ug/L 50.00 70-130Surrogate: Toluene-d8 9547.3
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/27/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010313
Time Submitted: 1/22/2020 10:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0381 - 5030B
Matrix Spike (P0A0381-MS1)Prepared & Analyzed: 01/23/20 Source: 0010313-01
1,1,1,2-Tetrachloroethane ug/L1805.0 200.0 BRL 70-13090
1,1,1-Trichloroethane ug/L2045.0 200.0 BRL 70-130102
1,1,2,2-Tetrachloroethane ug/L1835.0 200.0 BRL 70-13092
1,1,2-Trichloroethane ug/L2075.0 200.0 BRL 70-130104
1,1-Dichloroethane ug/L2035.0 200.0 BRL 70-130102
1,1-Dichloroethylene ug/L2025.0 200.0 BRL 70-130101
1,1-Dichloropropylene ug/L2165.0 200.0 BRL 70-130108
1,2,3-Trichlorobenzene ug/L1685.0 200.0 BRL 70-13084
1,2,3-Trichloropropane ug/L1975.0 200.0 BRL 70-13099
1,2,4-Trichlorobenzene ug/L1675.0 200.0 BRL 70-13084
1,2,4-Trimethylbenzene ug/L1755.0 200.0 BRL 70-13087
1,2-Dibromo-3-chloropropane ug/L17720 200.0 BRL 70-13088
1,2-Dibromoethane ug/L1985.0 200.0 BRL 70-13099
1,2-Dichlorobenzene ug/L1835.0 200.0 BRL 70-13091
1,2-Dichloroethane ug/L1875.0 200.0 BRL 70-13094
1,2-Dichloropropane ug/L2015.0 200.0 BRL 70-130101
1,3,5-Trimethylbenzene ug/L1785.0 200.0 BRL 70-13089
1,3-Dichlorobenzene ug/L1825.0 200.0 BRL 70-13091
1,3-Dichloropropane ug/L2015.0 200.0 BRL 70-130101
1,4-Dichlorobenzene ug/L1845.0 200.0 BRL 70-13092
2,2-Dichloropropane ug/L19020 200.0 BRL 70-13095
2-Chlorotoluene ug/L1745.0 200.0 BRL 70-13087
4-Chlorotoluene ug/L1745.0 200.0 BRL 70-13087
4-Isopropyltoluene ug/L1835.0 200.0 BRL 70-13091
Acetone ug/L346 100 400.0 BRL 40-16087
Benzene ug/L2035.0 200.0 BRL 70-130101
Bromobenzene ug/L1785.0 200.0 BRL 70-13089
Bromochloromethane ug/L2125.0 200.0 BRL 70-130106
Bromodichloromethane ug/L1925.0 200.0 BRL 70-13096
Bromoform ug/L1735.0 200.0 BRL 70-13086
Bromomethane ug/L10610 200.0 BRL M60-14053
Carbon Tetrachloride ug/L1865.0 200.0 BRL 70-13093
Chlorobenzene ug/L1985.0 200.0 BRL 70-13099
Chloroethane ug/L1495.0 200.0 BRL 60-14075
Chloroform ug/L2035.0 200.0 BRL 70-130102
Chloromethane ug/L1725.0 200.0 17.2 60-14077
cis-1,2-Dichloroethylene ug/L1935.0 200.0 BRL 70-13097
cis-1,3-Dichloropropylene ug/L1985.0 200.0 BRL 70-13099
Dibromochloromethane ug/L1785.0 200.0 BRL 70-13089
Dibromomethane ug/L2035.0 200.0 BRL 70-130101
Dichlorodifluoromethane ug/L16710 200.0 BRL 60-14083
Ethanol ug/L5380 2000 5000 BRL 60-140108
Ethylbenzene ug/L1935.0 200.0 BRL 70-13096
Hexachlorobutadiene ug/L18720 200.0 BRL 70-13093
Isopropyl Ether ug/L1935.0 200.0 BRL 70-13096
Isopropylbenzene (Cumene)ug/L1875.0 200.0 BRL 70-13094
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/27/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010313
Time Submitted: 1/22/2020 10:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0381 - 5030B
Matrix Spike (P0A0381-MS1)Prepared & Analyzed: 01/23/20 Source: 0010313-01
m,p-Xylenes ug/L39810 400.0 BRL 70-13099
Methyl Butyl Ketone (2-Hexanone)ug/L18510 200.0 BRL 60-14092
Methyl Ethyl Ketone (2-Butanone)ug/L19750 200.0 BRL 60-14098
Methyl Isobutyl Ketone ug/L19610 200.0 BRL 60-14098
Methylene Chloride ug/L19520 200.0 BRL 70-13097
Methyl-tert-Butyl Ether ug/L20810 200.0 BRL 70-130104
Naphthalene ug/L14610 200.0 BRL 70-13073
n-Butylbenzene ug/L1685.0 200.0 BRL 70-13084
n-Propylbenzene ug/L1805.0 200.0 BRL 70-13090
o-Xylene ug/L1925.0 200.0 BRL 70-13096
sec-Butylbenzene ug/L1865.0 200.0 BRL 70-13093
Styrene ug/L1965.0 200.0 BRL 70-13098
tert-Amyl Alcohol ug/L198 100 200.0 BRL 70-13099
tert-Amyl Methyl Ether ug/L412 100 400.0 BRL 70-130103
tert-Butyl Alcohol ug/L375 100 400.0 BRL 70-13094
tert-Butylbenzene ug/L1875.0 200.0 BRL 70-13094
tert-Butyl Ethyl Ether ug/L402 100 400.0 BRL 70-130100
tert-Butyl Formate ug/L285 100 400.0 BRL 70-13071
Tetrachloroethylene ug/L2125.0 200.0 BRL 70-130106
Toluene ug/L2005.0 200.0 BRL 70-130100
trans-1,2-Dichloroethylene ug/L1995.0 200.0 BRL 70-130100
trans-1,3-Dichloropropylene ug/L1945.0 200.0 BRL 70-13097
Trichloroethylene ug/L2075.0 200.0 BRL 70-130103
Trichlorofluoromethane ug/L2195.0 200.0 BRL 60-140110
Vinyl acetate ug/L19650 200.0 BRL 60-14098
Vinyl chloride ug/L1975.0 200.0 BRL 60-14098
Xylenes, total ug/L58915 600.0 BRL 70-13098
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9246.2
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9346.4
ug/L 50.00 70-130Surrogate: Toluene-d8 9547.6
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/27/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010313
Time Submitted: 1/22/2020 10:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0381 - 5030B
Matrix Spike Dup (P0A0381-MSD1)Prepared & Analyzed: 01/23/20 Source: 0010313-01
1,1,1,2-Tetrachloroethane ug/L1795.0 200.0 BRL 2070-13089 0.7
1,1,1-Trichloroethane ug/L1995.0 200.0 BRL 2070-130100 2
1,1,2,2-Tetrachloroethane ug/L1735.0 200.0 BRL 2070-13087 6
1,1,2-Trichloroethane ug/L1985.0 200.0 BRL 2070-13099 5
1,1-Dichloroethane ug/L1985.0 200.0 BRL 2070-13099 2
1,1-Dichloroethylene ug/L1945.0 200.0 BRL 2070-13097 4
1,1-Dichloropropylene ug/L2075.0 200.0 BRL 2070-130103 4
1,2,3-Trichlorobenzene ug/L1655.0 200.0 BRL 2070-13082 2
1,2,3-Trichloropropane ug/L1855.0 200.0 BRL 2070-13092 7
1,2,4-Trichlorobenzene ug/L1645.0 200.0 BRL 2070-13082 2
1,2,4-Trimethylbenzene ug/L1715.0 200.0 BRL 2070-13085 2
1,2-Dibromo-3-chloropropane ug/L16020 200.0 BRL 2070-13080 10
1,2-Dibromoethane ug/L1925.0 200.0 BRL 2070-13096 3
1,2-Dichlorobenzene ug/L1795.0 200.0 BRL 2070-13089 2
1,2-Dichloroethane ug/L1835.0 200.0 BRL 2070-13092 2
1,2-Dichloropropane ug/L1975.0 200.0 BRL 2070-13098 2
1,3,5-Trimethylbenzene ug/L1745.0 200.0 BRL 2070-13087 2
1,3-Dichlorobenzene ug/L1795.0 200.0 BRL 2070-13089 2
1,3-Dichloropropane ug/L1945.0 200.0 BRL 2070-13097 4
1,4-Dichlorobenzene ug/L1805.0 200.0 BRL 2070-13090 2
2,2-Dichloropropane ug/L17820 200.0 BRL 2070-13089 6
2-Chlorotoluene ug/L1695.0 200.0 BRL 2070-13085 3
4-Chlorotoluene ug/L1715.0 200.0 BRL 2070-13086 2
4-Isopropyltoluene ug/L1775.0 200.0 BRL 2070-13089 3
Acetone ug/L301 100 400.0 BRL 2040-16075 14
Benzene ug/L1975.0 200.0 BRL 2070-13098 3
Bromobenzene ug/L1755.0 200.0 BRL 2070-13088 2
Bromochloromethane ug/L2085.0 200.0 BRL 2070-130104 2
Bromodichloromethane ug/L1895.0 200.0 BRL 2070-13094 2
Bromoform ug/L1685.0 200.0 BRL 2070-13084 3
Bromomethane ug/L110 10 200.0 BRL 20 M60-14055 4
Carbon Tetrachloride ug/L1805.0 200.0 BRL 2070-13090 3
Chlorobenzene ug/L1935.0 200.0 BRL 2070-13096 3
Chloroethane ug/L1505.0 200.0 BRL 2060-14075 0.7
Chloroform ug/L2005.0 200.0 BRL 2070-130100 1
Chloromethane ug/L1625.0 200.0 17.2 2060-14072 6
cis-1,2-Dichloroethylene ug/L1875.0 200.0 BRL 2070-13094 3
cis-1,3-Dichloropropylene ug/L1945.0 200.0 BRL 2070-13097 2
Dibromochloromethane ug/L1785.0 200.0 BRL 2070-13089 0.2
Dibromomethane ug/L1995.0 200.0 BRL 2070-130100 2
Dichlorodifluoromethane ug/L15910 200.0 BRL 2060-14079 5
Ethanol ug/L4710 2000 5000 BRL 2060-14094 13
Ethylbenzene ug/L1865.0 200.0 BRL 2070-13093 3
Hexachlorobutadiene ug/L18420 200.0 BRL 2070-13092 2
Isopropyl Ether ug/L1895.0 200.0 BRL 2070-13094 2
Isopropylbenzene (Cumene)ug/L1825.0 200.0 BRL 2070-13091 3
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/27/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: NCDEQ#3327
02170214.74
Project: Billy’s Mini MartWithers & Ravenel
Cary, NC 27511
Attn: Kevin Buchanan
Work Order: 0010313
Time Submitted: 1/22/2020 10:00:00AM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0381 - 5030B
Matrix Spike Dup (P0A0381-MSD1)Prepared & Analyzed: 01/23/20 Source: 0010313-01
m,p-Xylenes ug/L38410 400.0 BRL 2070-13096 3
Methyl Butyl Ketone (2-Hexanone)ug/L16410 200.0 BRL 2060-14082 12
Methyl Ethyl Ketone (2-Butanone)ug/L17250 200.0 BRL 2060-14086 14
Methyl Isobutyl Ketone ug/L17510 200.0 BRL 2060-14088 11
Methylene Chloride ug/L18920 200.0 BRL 2070-13095 3
Methyl-tert-Butyl Ether ug/L20310 200.0 BRL 2070-130101 3
Naphthalene ug/L14010 200.0 BRL 2070-13070 4
n-Butylbenzene ug/L1615.0 200.0 BRL 2170-13080 4
n-Propylbenzene ug/L1755.0 200.0 BRL 1870-13087 3
o-Xylene ug/L1875.0 200.0 BRL 2070-13093 3
sec-Butylbenzene ug/L1795.0 200.0 BRL 2070-13090 4
Styrene ug/L1905.0 200.0 BRL 2070-13095 3
tert-Amyl Alcohol ug/L194 100 200.0 BRL 2070-13097 2
tert-Amyl Methyl Ether ug/L404 100 400.0 BRL 2070-130101 2
tert-Butyl Alcohol ug/L329 100 400.0 BRL 2070-13082 13
tert-Butylbenzene ug/L1825.0 200.0 BRL 2070-13091 3
tert-Butyl Ethyl Ether ug/L397 100 400.0 BRL 2070-13099 1
tert-Butyl Formate ug/L272 100 400.0 BRL 2070-13068 5
Tetrachloroethylene ug/L2025.0 200.0 BRL 2070-130101 5
Toluene ug/L1935.0 200.0 BRL 2070-13096 4
trans-1,2-Dichloroethylene ug/L1925.0 200.0 BRL 2070-13096 4
trans-1,3-Dichloropropylene ug/L1915.0 200.0 BRL 2070-13095 2
Trichloroethylene ug/L2015.0 200.0 BRL 2070-130100 3
Trichlorofluoromethane ug/L2105.0 200.0 BRL 2060-140105 4
Vinyl acetate ug/L18950 200.0 BRL 2060-14095 3
Vinyl chloride ug/L1885.0 200.0 BRL 2060-14094 5
Xylenes, total ug/L57115 600.0 BRL 2070-13095 3
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9346.3
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9346.4
ug/L 50.00 70-130Surrogate: Toluene-d8 9547.4
Sample Extraction Data
Prep Method: 5030B
Lab Number Batch Date/TimeInitialFinal
P0A03810010313-01 01/23/20 12:0010 10mL mL
P0A03810010313-02 01/23/20 12:0010 10mL mL
P0A03810010313-03 01/23/20 12:0010 10mL mL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

APPENDIX B 

FIELD NOTES 

APPENDIX C 

SITE PHOTOGRAPHS 

 Photo 1 
Site View to East‐Northeast 

 Photo 2 
Site View to East 

 Photo 3 
MW‐1 

 Photo 4 
MW‐2R 

 Photo 5 
MW‐3 

 Photo 6 
SRW‐1 (Center), DW‐1 (Middle), MW‐4 (Middle, Right), DW‐2 (Left) 

 Photo 7 
MW‐5 

 Photo 8 
MW‐6 

 Photo 9 
MW‐7 

 Photo 10 
MW‐8 

 Photo 11 
MW‐9, MW‐9R 

 Photo 12 
MW‐10, MW‐10R 

 Photo 13 
MW‐11 

Photo 14 
MW‐12 

 Photo 15 
MW‐13 

 Photo 16 
MW‐14 

 Photo 17 
MW‐15 

 Photo 18 
MW‐16 

 Photo 19 
MW‐17 

 Photo 20 
SRW‐1 

 Photo 21 
RW‐3 (Right) 

 Photo 22 
WSW‐1 

 Photo 23 
WSW‐3 Sample Point 

 Photo 24 
WSW‐4 

APPENDIX D 

GENERAL STANDARD OPERATING PROCEDURES