FA-916_17217_CA_MRP_20160302_ECS FINAL Flowers Store GW Sampling Report

March 2, 2016

Mr. Mark Petermann
NCDEQ, Division of Waste Management, UST Section
1637 Mail Service Center
Raleigh, North Carolina 27699-1637

Reference: Report of Environmental Services – Flowers Store Property
4181 NC Highway 42 East
Clayton, Johnston County, North Carolina
NCDEQ Incident: 17217
NCDEQ Contract: N14007i-C
ECS Project: 49:1226

Dear Mr. Petermann:

As authorized by your acceptance of ECS Carolinas, LLP (ECS) Task Authorization Request #4
(TAR #4) dated January 21, 2016, ECS has completed the Report of Environmental Services for
the above-referenced site. Included in this report is a description of the field activities, the results
obtained, and our conclusions and recommendations. Information regarding the owner of former
underground storage tank (UST), current property owner, contacts, consultant, laboratory, release
information, and latitude and longitude are presented below.

ECS appreciates the opportunity to provide our environmental consulting services to you on this
project. If you have any questions concerning this report or this project, please contact us at (919)
861-9910.

Sincerely,

ECS CAROLINAS, LLP

Matthew Gillis
Environmental Project Manager
[e-mail]
919-861-9845

C. Brian Smith, P.G.
Principal Geologist
[e-mail]
919-861-9850
Report of Environmental Services – Flowers Store Property
4181 NC Highway 42 East
Clayton, Johnston County, North Carolina
NCDEQ Incident: 17217
NCDEQ Contract: N14007i-C
March 2, 2016

SITE INFORMATION

Date of Report: March 2, 2016

Facility I.D.: Unknown
UST Incident No.: 12704
Site Rank: High
Land Use Category: Vacant – Two Buildings are located on the property

Site Name and Location: Flowers Store Property
4181 NC Highway 42 East
Clayton, Johnson County, North Carolina

Location Method: Google Earth
Latitude and Longitude: 36.651793° North, -78.360938° West
Contacts

Primary Contact: Ms. Jana Guertler
526 Powell Road
Raleigh, North Carolina 27606
[phone]

Consultant: ECS Carolinas, LLP
9001 Glenwood Avenue
Raleigh, North Carolina 27617
[phone]
Attn: Matthew Gillis

Laboratory: Pace Analytical Services, Inc.
9800 Kincey Ave, Suite 100
Huntersville, North Carolina 28078
[phone]
NC Certification No. 12

Report of Environmental Services – Flowers Store Property
4181 NC Highway 42 East
Clayton, Johnston County, North Carolina
NCDEQ Incident: 17217
NCDEQ Contract: N14007i-C
March 2, 2016

EXECUTIVE SUMMARY

The subject site is known as the Flowers Store Property and is located at 4181 NC Highway 42
East in Clayton, Johnson County, North Carolina. The subject site is further identified by Johnson
County Geographic Information Systems (GIS) Parcel Identification Number (PIN) 168900-92-
5990.

On January 26, 2016, ECS collected groundwater samples from six existing monitoring wells
(MW-3, MW-5, MW-7, MW-8, MW-9, and MW-10). ECS also collected groundwater samples
from three water supply wells (WSW-2, WSW-4, and WSW-5). The properties associated with
the water supply wells (WSW-3 and WSW-6) were unoccupied; therefore groundwater samples
were not collected.

Laboratory analysis reported naphthalene at a concentration above its North Carolina 2L
Groundwater Quality Standards (NC2LGWQS) but below its Gross Contamination Level (GCL) in
the groundwater sample collected from monitoring well MW-9.

Laboratory analysis reported bromodichloromethane and dibromochloromethane at
concentrations above their respective NC2LGWQS but below their respective GCLs in the
groundwater samples collected from water supply wells WSW-2 and WSW-4.

Laboratory analysis reported 1,2-dichloropropane at a concentration above its NC2LGWQS but
below its GCL in the groundwater sample collected from water supply well WSW-5.

Laboratory analysis reported several additional targeted analytes above their respective laboratory
reporting limits but below their NC2LGWQS in the groundwater samples collected from monitoring
wells MW-9 and water supply wells WSW-2 and WSW-4.

Laboratory analysis did not report targeted analytes at concentrations above the laboratory
reporting limits in the groundwater samples collected from monitoring wells MW-3, MW-5, MW-7,
MW-8, and MW-10.

ECS recommends conducting a groundwater sampling event at the site and conduct
contamination transport modeling to assess the potential migration of the contamination plume for
monitoring well MW-9 and its relation to area water supply wells in April 2016. Once the modeling
is complete and assuming area water supply wells will not be impacted, a Notice of Residual
Petroleum (NRP) for groundwater contamination should be submitted for the site and the NCDEQ
should consider issuing a letter of No Further Action (NFA).

Report of Environmental Services – Flowers Store Property
4181 NC Highway 42 East
Clayton, Johnston County, North Carolina
NCDEQ Incident: 17217
NCDEQ Contract: N14007i-C
March 2, 2016

TABLE OF CONTENTS
SITE HISTORY ............................................................................................................... 1
FIELD ACTIVITIES ......................................................................................................... 4
CONCLUSIONS .............................................................................................................. 6
RECOMMENDATIONS ................................................................................................... 6

FIGURES

Figure 1 Site Location Map
Figure 2 Site Aerial Map
Figure 3 Monitoring Well Location Map
Figure 4 Groundwater Elevation Map
Figure 5 Groundwater Concentration Map
Figure 6 Naphthalene Isoconcentration Map
Figure 7 Water Supply Well Location Map
TABLES

Table 1 UST Information
Table 2 Well Construction and Groundwater Elevation Details
Table 3 Summary of Current Groundwater Analytical Results
Table 4 Summary of Historical Groundwater Analytical Results
Table 5 Summary of Current and Historical Water Supply Well Analytical Results
Table 6 Summary of Historical Soil Sample Analytical Results
Table 7 Water Supply Well Survey

APPENDICIES

Appendix A ECS Personnel Field Notes
Appendix B Site Photographs
Appendix C Laboratory Analytical Data Sheets and Chain of Custody Records

Report of Environmental Services – Flowers Store Property
4181 NC Highway 42 East
Clayton, Johnston County, North Carolina
NCDEQ Incident: 17217
NCDEQ Contract: N14007i-C
March 2, 2016

1
SITE HISTORY

The Flowers Store Property is located at 4181 NC Highway 42 East in Clayton, Johnson
County, North Carolina (Figures 1 and 2). According to a 1994 UST Closure Report prepared
by Froehling & Robertson Inc. (F&R), the site was formerly utilized as a gasoline station and auto
repair service facility. On August 29, 1994, one 8,000-gallon gasoline UST (UST-1), one 1,000-
gallon kerosene/diesel UST (UST-2), and one 6,000-gallon diesel UST (UST-3), along with
associated piping/equipment were removed by Action Oil Equipment Company. A summary of
the former UST information for the site is included in Table 1. Based on the analytical results
of the soil samples, releases were reported beneath UST-2 and UST-3. The laboratory
reported Total Petroleum Hydrocarbons – Gasoline Range Organics (TPH-GRO) and TPH-
Diesel Range Organics (TPH-DRO) at concentrations above their respective North Carolina
Department of Environmental Quality (NCDEQ) UST Section’s Action Level of 10 mg/kg. TPH-
GRO was reported at concentrations ranging from 567 mg/kg to 2,900 mg/kg. TPH-DRO
concentrations ranged from 18.6 mg/kg to 11,100 mg/kg. Contaminated soils were not removed
from the site and groundwater samples were not collected during UST closure activities.

On February 17, 2006, Agra Environmental, Inc. (AGRA) conducted an Initial Site Visit and Site
Receptor Survey. Agra identified one building on the subject site that was used as a repair
garage and was being used for storage. A sump was observed, which possibly was used as an
oil/water separator, near the rear of the garage. Metal debris, including appliances, tanks, and
vehicles were scattered throughout the wooded area along the northern boundary of the subject
site. AGRA also documented that an additional UST (UST-4) was discovered near the
southeastern corner of the subject site. AGRA identified four potential water supply wells within
1,500 feet of the subject site and a pond located on the adjacent property to the northeast of the
site.

A 2006 UST Closure Report, prepared by AGRA, indicates AGRA removed one 1,000-gallon UST
from the southeastern corner of the subject site. AGRA did not observe contaminated soil in the
UST excavation. However, two 55-gallon drums of contaminated soil associated with spillage of
residual sludge from the UST were removed from the subject site. The remaining soils and clean
fill were used to backfill the UST excavation. Soil samples were not collected prior to backfill.

AGRA performed a door-to-door survey of the surrounding area on May 22, 2008. A total of six
water supply wells (WSW-1, WSW-2, WSW-3, WSW-4, WSW-5, and WSW-6) were identified
approximately 525 feet (ft), 525 ft, 1,100 ft, 900 ft, 550 ft, and 1,400 ft from the subject site,
respectively. An interview with the owners of water supply wells WSW-1 and WSW-4, indicated
that both water supply wells were used as a primary drinking water source and the residence was
not connected to the public water supply at that time. An interview with the owners of water supply
wells WSW-2 and WSW-3 indicated that both wells were currently disconnected and the
properties were connected to the public water supply. Additionally, two water supply wells (WSW-
5 and WSW-6) were observed at 160 Motorcycle Road and 270 Motorcycle Road, respectively.
The property owners could not be contacted during the site visit or during follow up interviews.
AGRA identified 160 Motorcycle Road as a residential property and 270 Motorcycle Road as
Pineville Chapel Church.

On June 17, 2008, AGRA conducted an Initial Groundwater Site Investigation and collected
groundwater samples from water supply wells WSW-1 and WSW-4. The laboratory reported bis
Report of Environmental Services – Flowers Store Property
4181 NC Highway 42 East
Clayton, Johnston County, North Carolina
NCDEQ Incident: 17217
NCDEQ Contract: N14007i-C
March 2, 2016

2
(2-ethylhexyl) phthalate in water supply well WSW-1 at a concentration above its North Carolina
Department of Environment and Natural Resources 2L Groundwater Quality Standard
(NC2LGWQS) but below its Gross Contamination Level (GCL). However, AGRA stated that bis
(2-ethylhexyl) phthalate is not a petroleum constituent and was believed to be a laboratory
contaminant. Bis (2-ethylhexyl) phthalate was also reported above its laboratory reporting limit but
below its NC2LGWQS in water supply well WSW-4.

On August 28, 2008, Regional Probing Services installed four temporary monitoring wells (TW-1,
TW-2, TW-3 (MW-3), and TW-4) on the subject site using a Geoprobe. The temporary wells were
each installed to a depth of 35 feet below the ground surface (ft. bgs) with a screened interval of
15 linear feet. Soil encountered during the well installations was very tight red clay. Soil samples
were collected during the installation of each temporary monitoring well at depths of 10 ft. and 20
ft. bgs. The laboratory reported methyl chloride in the soil samples collected from temporary wells
TW-3 and TW-4 at concentrations above the Soil-To-Groundwater Maximum Soil Contaminant
Concentration (MSCC) standard of 0.02 milligrams per kilogram (mg/kg). Diethyl phthalate was
reported in the soil samples collected from TW-2 and TW-3. Di-n-butyl phthalate was reported in
soil sample TW-3. Diethyl phthalate and di-n-butyl phthalate do not have an established MSCC
standard.

On September 2, 2008, AGRA personnel collected groundwater samples from temporary wells
TW-1 through TW-4. Temporary well TW-1 was analyzed for volatile organic compounds (VOCs)
using EPA Method 6200B, for semi-volatile organic compounds (SVOCs) using EPA Method 625,
and Massachusetts Department of Environmental Protection Extractable Petroleum Hydrocarbons
(MADEP EPH), MADEP Volatile Petroleum Hydrocarbons (MADEP VPH), and lead using EPA
Method 6010/303C. Groundwater samples were also collected from temporary wells TW-2, TW-3,
and TW 4 to be analyzed for VOCs using EPA Method 6200B and MADEP VPH. The laboratory
reported lead at a concentration of 250 micrograms per liter (µg/L) in the groundwater sample
collected from temporary well TW-1, which exceeds the NC2LGWQS of 15 µg/L. Di-n-butyl
phthalate was detected in temporary well TW-1 at a concentration of 6.68 µg/L; however di-n-butyl
phthalate does not have a NC2LGWQS. The laboratory did not report additional targeted
analytes from the groundwater samples at concentrations exceeding their respective
NC2LGWQS.

On February 5, 19, and 25, 2009, Cohesion, Inc. (Cohesion) collected soil samples from
numerous locations at the subject site in an attempt to confirm that contaminated soils remain at
the subject site. Laboratory analysis reported TPH above the Action Level of 10 mg/kg in soil
samples collected near the rear of the garage, adjacent to an old CITGO petroleum tanker that
had been discarded in the rear of the property, and near two hydraulic pumps located inside the
garage.

On September 30, 2009, AGRA personnel conducted a soil and groundwater sampling event at
the site. Three soil borings were advanced in the former UST locations (UST-1 to 12 ft bgs, UST-2
to 8 ft bgs, and UST-3 to 10 ft bgs). Additionally, soil borings were advanced adjacent to the
previously installed soil borings B-15 and B-8. Soil samples were collected from B-15 and B-8 at
depths of 2 ft bgs and 8 ft bgs. As part of the sampling event, AGRA personnel attempted to
collect groundwater samples from the four on-site temporary monitoring wells TW-1, TW-2, TW-3,
and TW-4. The temporary wells were previously installed with PVC risers, which extended
approximately 1.5 ft above the ground surface. The aboveground risers of temporary wells TW-1
Report of Environmental Services – Flowers Store Property
4181 NC Highway 42 East
Clayton, Johnston County, North Carolina
NCDEQ Incident: 17217
NCDEQ Contract: N14007i-C
March 2, 2016

3
and TW-2 were broken and TW-4 was dry. The laboratory reported targeted analytes at the
subject site in the soil samples collected near the former locations of UST-2 and UST-3, as well as
adjacent to the discarded tanker on the rear of the property. However, the analytes reported were
below their respective MSCC standards or did not have established MSCC standards. The
laboratory reported tetrachloroethene at concentrations of 0.89 µg/L and 0.71 µg/L in the
groundwater samples collected from TW-1 and TW-2, respectively, which were above the
NC2LGWQS of 0.70 µg/L. Temporary well TW-4 was not sampled. However, targeted analytes
were not reported in TW-4 during the sampling event performed on September 2, 2008.
Additionally, 1,2-dichloropropane was reported at a concentration of 0.51 µg/L in water supply well
WSW-5, which is below the NC2LGWQS of 0.60 µg/L.

On October 4, 2012, Crawford Environmental Services (CES) conducted a groundwater
monitoring event at the subject site. Temporary monitoring wells TW-1, TW-2, and TW-4 were
not located and were presumed destroyed. CES observed six water supply wells within 1,500 feet
of the subject site (WSW-1 through WSW-6). Based on discussions with the property owner, the
home associated with water supply well WSW-1 had been connected to municipal water and the
well had been abandoned. The properties utilizing water supply wells WSW-2 and WSW-3 were
also connected to municipal water. Water supply wells WSW-4 through WSW-6 were still actively
used as a water supply source. CES collected a groundwater sample from temporary well TW-3
and the laboratory did not report targeted analytes above the laboratory reporting limit.

Information contained in a March 26, 2013 Groundwater Monitoring Report prepared by CES,
indicates that on February 13 and 14, 2013, CES installed two permanent monitoring wells (MW-5
and MW-7) at the subject site. CES collected groundwater samples from temporary well TW-3
and monitoring wells MW-5, and MW-7. The laboratory reported several targeted analytes at
concentrations above their respective laboratory reporting limits, but below their respective
NC2LGWQS. Additionally, CES collected soil samples at depths of 8 ft bgs, 13 ft bgs, and 23 ft
bgs during the installation of monitoring well MW-5. The laboratory reported C9-C22 Aromatics at
a concentration above the MSCC in the soil sample collected from MW-5 at 23 ft bgs. The
laboratory reported several additional targeted analytes at concentrations above the laboratory
reporting limits, but below their respective MSCCs. The results of this soil sampling are
summarized in Table 6.

On August 13, 2014, ECS collected two groundwater samples from monitoring wells MW-5 and
MW-7. Monitoring well MW-3 was filled with dirt; therefore, a groundwater sample was not
collected. Additionally, ECS collected groundwater samples from water supply wells WSW-4,
WSW-5, and WSW-6. The laboratory reported several analytes at concentrations above their
respective laboratory reporting limit in the groundwater samples collected from the site
monitoring wells. Additionally, the laboratory reported several analytes at concentrations above
the laboratory reporting limit in the groundwater samples collected from water supply wells
WSW-4 and WSW-5.

On June 11 and 12, 2015, ECS installed three monitoring wells (MW-8 through MW-10),
collected groundwater samples from monitoring well MW-3, MW-5, MW-7 and each of the three
new monitoring wells. ECS also collected groundwater samples from water supply wells WSW-
4 and WSW-5. The properties associated with water supply wells WSW-2, WSW-3, and WSW-
6 were unoccupied; therefore groundwater samples were not collected.

Report of Environmental Services – Flowers Store Property
4181 NC Highway 42 East
Clayton, Johnston County, North Carolina
NCDEQ Incident: 17217
NCDEQ Contract: N14007i-C
March 2, 2016

4
On June 25, 2015 ECS contracted with Bateman Civil Survey to survey the monitoring wells.
During surveying activities, ECS identified bulldozing had occurred near the location of monitoring
well MW-3 and had damaged the well.

SITE GEOLOGY AND HYDROGEOLOGY

As determined from the USGS Topographic Map, Flowers, North Carolina Quadrangle dated
1998 (Figure 1), the site is at an approximate elevation of 275 feet above mean sea level.
Surface runoff on the site is generally to the west.

The subject site is situated in the Coastal Plain Physiographic Province. The soils encountered
in this area are the residual product of in-place chemical weathering of rock presently
underlying the site and/or historic depositional events. In general, shallow unconfined
groundwater movement within the overlying soils is controlled largely by topographic gradients.
However, as the groundwater percolates downward, it becomes controlled by the subsurface
geologic conditions. Thus, the direction of groundwater movement in the deeper aquifers may
not be consistent with the reflecting topography.

In general, shallow unconfined groundwater movement within the overlying soils is controlled
largely by topographic gradients. Recharge occurs primarily by infiltration along higher
elevations and typically discharges into streams or other surface water bodies. The elevation of
the shallow water table is transient and can vary with seasonal fluctuations in precipitation.
Movement of shallow groundwater is generally from higher to lower elevations.

Water Supply Wells

Six previously identified water supply wells are located within 1,000 feet of the source area.
According to the 2012 CES groundwater monitoring report, water supply wells WSW-1, WSW-
2, and WSW-3 are connected to municipal water and WSW-1 is abandoned. Additionally, the
residences associated with water supply wells WSW-4 and WSW-5 are actively used as a
potable water source. Water supply wells WSW-3 and WSW-6 are located greater than 1,000
feet from the source area. ECS previously received a completed water supply well
questionnaire from Ms. Sarah Blanchard, the property owner of the residence associated with
water supply well WSW-4. Ms. Blanchard stated that WSW-4 is active and the residence is not
connected to municipal water. However, water supply well WSW-4 is approximately 975 feet
southeast and topographically crossgradient of the site. ECS also received verbal permission
from the resident of the home associated with water supply well WSW-5 to collect a
groundwater sample. ECS has not received completed water supply well questionnaires from
the remaining property owners within 1,000 feet of the site. The names and addresses of the
property owners with water supply wells located within 1,000 feet of the site are included in
Table 7 and shown on Figure 7.

FIELD ACTIVITIES

On January 26, 2015, ECS collected groundwater samples from monitoring wells MW-3, MW-5,
MW-7, MW-8, MW-9, and MW-10. ECS personnel field notes are included in Appendix A. Site
photographs are included in Appendix B.

Report of Environmental Services – Flowers Store Property
4181 NC Highway 42 East
Clayton, Johnston County, North Carolina
NCDEQ Incident: 17217
NCDEQ Contract: N14007i-C
March 2, 2016

5
Prior to the sampling activities, the static groundwater elevation was measured in each monitoring
well. Well construction details and groundwater elevation data is summarized in Table 2 and
shown of Figure 4. Based on these measurements, ECS determined groundwater flows
generally to the west. Purging and sampling were accomplished using a peristaltic pump and
dedicated tubing. Immediately after collection, the groundwater samples were transferred into
sample containers provided by the laboratory.

ECS also collected groundwater samples from water supply wells WSW-2, WSW-4, and WSW-
5. The property associated with water supply well WSW-6 was unoccupied; therefore a
groundwater sample was not collected.

Prior to water supply well sampling activities, ECS opened the spigots attached to the outside of
the residences for three to five minutes allowing the groundwater to purge from the water
supply wells and associated water lines. After allowing the water supply wells to purge, ECS
collected the groundwater samples from the spigots into sample containers provided by the
laboratory.

The sample containers were labeled with ECS project number, sample identification, sample
date and time, and requested analytical analysis. The containers were placed into protective
packaging material and placed into a cooler with ice to maintain the samples at approximately
4° Celsius (°C). The samples were submitted to Pace Analytical Services, Inc. located in
Huntersville, North Carolina for chemical analysis for volatile organic compounds (VOCs) using
EPA Method 6200B. ECS maintained proper chain of custody (COC) procedures throughout the
sample collection and transportation process. Laboratory data sheets and COC records are
included in Appendix C.

LABORATORY ANALYTICAL RESULTS

Laboratory analysis reported naphthalene at a concentration above its NC2LGWQS but below its
GCL in the groundwater sample collected from monitoring well MW-9.

Laboratory analysis reported bromodichloromethane and dibromochloromethane at
concentrations above their respective NC2LGWQS but below their respective GCLs in the
groundwater samples collected from water supply wells WSW-2 and WSW-4.

Laboratory analysis reported 1,2-dichloropropane at a concentration above its NC2LGWQS but
below its GCL in the groundwater sample collected from water supply well WSW-5.

Laboratory analysis reported several additional targeted analytes above their respective laboratory
reporting limits but below their NC2LGWQS in the groundwater samples collected from monitoring
well MW-9 and water supply wells WSW-2 and WSW-4.

Laboratory analysis did not report targeted analytes at concentrations above the laboratory
reporting limits in the groundwater samples collected from monitoring wells MW-3, MW-5, MW-7,
MW-8, and MW-10.

A summary of the laboratory analytical results is included in Table 3 and shown on Figures 5 and
6. Historical groundwater data is summarized in Tables 4 and 5.
Report of Environmental Services – Flowers Store Property
4181 NC Highway 42 East
Clayton, Johnston County, North Carolina
NCDEQ Incident: 17217
NCDEQ Contract: N14007i-C
March 2, 2016

6

The laboratory analytical data sheets and COCs are included in Appendix C.

CONCLUSIONS

Based on the results of this Groundwater Sampling Event, ECS concludes the following:

• Historically, water supply wells WSW-1, WSW-2 and WSW-3 are connected to the
municipal water supply. The presence of these water supply wells is unknown, except for
WSW-1, which has been abandoned.

• Naphthalene was reported at a concentration above its NC2LGWQS in the groundwater
sample from monitoring well MW-9;

• Laboratory analysis did not report targeted analytes at concentrations above the NC2LGWQS
in the remaining groundwater samples collected from site monitoring wells;

• Laboratory analysis reported bromodichloromethane and dibromochloromethane in water
supply wells WSW-2 and WSW-4 at concentrations above their respective NC2LGWQS.
Bromodichloromethane and dibromochloromethane are common laboratory reagents and are
not considered analytes of concern of the site. Additionally, WSW-4 is located approximately
975 feet southeast and topographically cross-gradient of the site and WSW-2 is connected to
municipal water. Therefore, ECS does not consider these detections associated with the
Flowers Store Property; and

• Laboratory analysis reported 1,2-dichloropropane in water supply well WSW-5 at a
concentration above its NC2LGWQS. WSW-5 is located approximately 525 feet northwest
and topographically cross-gradient of the site. Therefore, ECS does not consider this
detection associated with Flowers Store Property.

RECOMMENDATIONS

• ECS recommends conducting a groundwater sampling event at the site in April 2016;

• ECS recommends conducting contamination transport modeling to assess the potential
migration of the contamination plume for monitoring well MW-9 and its relation to area water
supply wells. Once the modeling is complete and assuming area water supply wells will not
be impacted, a NRP for soil and groundwater contamination should be submitted for the site
and the NCDEQ should consider issuing a letter of NFA;

• ECS recommends that once the NRP has been issued, the NCDEQ should issue a NFA
letter for the site and consider the site for closure; and

• ECS recommends that a copy of this report be submitted to the current property owner.

FIGURES
SOURCE:
USGS TOPOGRAPHIC MAP
FLOWERS
NORTH CAROLINA QUADRANGLE
DATED 1998
SCALE: 1 : 24,000
FIGURE 1
SITE LOCATION MAP
FLOWERS STORE PROPERTY
4181 NC HIGHWAY 42 EAST
CLAYTON, JOHNSTON COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: 17217
ECS PROJECT: 49:1226
SITE
FIGURE 2
SITE AERIAL MAP
FLOWERS STORE PROPERTY
4181 NC HIGHWAY 42 EAST
CLAYTON, JOHNSTON COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: 17217
ECS PROJECT: 49:1226
SOURCE:
JOHNSTON COUNTY GIS
DATED 2013
SCALE AS SHOWN
SITE
SINGLE-FAMILY
RESIDENCES
SINGLE-FAMILY
RESIDENCES
SINGLE-FAMILY
RESIDENCES
Scale: 1 inch = 197 feet
SOURCE:
JOHNSTON COUNTY GIS
DATED 2013
SCALE AS SHOWN
FIGURE 3
MONITORING WELL LOCATION MAP
FLOWERS STORE PROPERTY
4181 NC HIGHWAY 42 EAST
CLAYTON, JOHNSTON COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: 17217
ECS PROJECT: 49:1226
LEGEND
Approximate Location of Monitoring Well
Approximate Location of Former UST
MW-3
MW-7
MW-3
MW-5
Scale: 1 inch = 60 feet
MW-8
MW-9
MW-10
SOURCE:
JOHNSTON COUNTY GIS
DATED 2013
SCALE AS SHOWN
FIGURE 4
GROUNDWATER ELEVATION MAP
FLOWERS STORE PROPERTY
4181 NC HIGHWAY 42 EAST
CLAYTON, JOHNSTON COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: 17217
ECS PROJECT: 49:1226
Scale: 1 inch = 60 feet
MW-7
257.80
260
255245250
MW-8
260.38
MW-3
256.81
MW-5
248.70MW-9
247.03
MW-10
251.56
LEGEND
Approximate Location of Monitoring Well
Groundwater Elevation
Groundwater Contour Line
Estimated Groundwater Contour Line
Estimated Direction of Groundwater Flow
* The site vertical datum is based on NAV88 and the horizontal
datum is based on NAD83.
MW-3
256.32
SOURCE:
JOHNSTON COUNTY GIS
DATED 2013
SCALE AS SHOWN
FIGURE 5
GROUNDWATER CONCENTRATION MAP
FLOWERS STORE PROPERTY
4181 NC HIGHWAY 42 EAST
CLAYTON, JOHNSTON COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: 17217
ECS PROJECT: 49:1226
Scale: 1 inch = 60 feet
MW-7
BRL
MW-3
BRL
MW-5
BRL
MW-8
BRL
MW-9
MW-10
BRL
sec-Butylbenzene 1.3
Isopropylbenzene 1.0
Naphthalene 18.4
n-Propylbenzene 2.0
1,4-Dichlorobenzene 0.51
1,2,4-Trimethylbenzene 8.5
1,3,5-Trimethylbenzene 16.3
Total Xylenes 1.2
LEGEND
Approximate Location of Monitoring Well
1.3 Concentrations Above Laboratory Reporting
Limits (µg/L)
18.4 Bold Concentrations Above the NCDENR
GWQS and/or NC2LGWQS (µg/L)
BRL Below Laboratory Reporting Limit
MW-3
SOURCE:
JOHNSTON COUNTY GIS
DATED 2013
SCALE AS SHOWN
FIGURE 6
NAPHTHALENE ISOCONCENTRATION MAP
FLOWERS STORE PROPERTY
4181 NC HIGHWAY 42 EAST
CLAYTON, JOHNSTON COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: 17217
ECS PROJECT: 49:1226
Scale: 1 inch = 60 feet
MW-7
BRL
MW-3
BRL
MW-5
BRL
MW-8
BRL
MW-9
18.4
MW-10
BRL
LEGEND
Approximate Location of Monitoring Well
Naphthalene Isoconcentration Contour
18.4 Bold Concentrations Above NCDENR GWQS
BRL Below Laboratory Reporting Limit
MW-3
6
SOURCE:
JOHNSTON COUNTY GIS
DATED 2013
SCALE AS SHOWN
FIGURE 7
WATER SUPPLY WELL LOCATION MAP
FLOWERS STORE PROPERTY
4181 NC HIGHWAY 42 EAST
CLAYTON, JOHNSTON COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: 17217
ECS PROJECT: 49:1226
LEGEND
Approximate Location
of Water Supply Well
500 ft.
Radius
1,000 ft.
Radius
WSW-5
SITE
0 361
Scale: 1 inch = 361 feet
WSW-6
Vacant
WSW-4
Potable
WSW-5
Potable
WSW-2
Municipal
WSW-1
Abandoned/
Municipal
WSW-3
Municipal

TABLES
UST ID NumberLast ContentsPrevious ContentsCapacity (in Gallons)Construction DetailsTank DimensionsInstallation DateRemoval DateStatus1 Gasoline Gasoline 8,000 Unknown 8' x 22' Unknown August 1994 Removed2 Kerosene/Diesel Kerosene/Diesel 1,000 Unknown 4' x 12'Unknown August 1994 Removed3 Diesel Diesel 6,000 Unknown 8' x 15' Unknown August 1994Removed4 Gasoline Gasoline 1,000 Unknown 4' x 12' Unknown April 2006 RemovedClayton, Johnston County, North CarolinaECS Project 49:1226Table 1UST InformationFlowers Store Property4181 NC Highway 42 EastNCDEQ Incident: 17217
Monitoring Well IDDate MeasuredDepth to Groundwater (ft. btoc)Date InstalledTotal Well Depth (ft. btoc)Screen Interval (ft. btoc)TOC Elevation *Groundwater Elevation MW-3 1/26/2016 18.42 2/13/2013 35 20-35 275.23 256.81MW-5 1/26/2016 27.52 2/13/2013 38 23-38 276.22 248.70MW-7 1/26/2016 13.38 2/13/2013 40 20-40 271.18 257.80MW-8 1/26/2016 16.40 6/10/2015 30 20-30 276.78 260.38MW-9 1/26/2016 27.14 6/10/2015 30 20-30 274.17 247.03MW-10 1/26/2016 27.64 6/10/2015 49 39-49 279.20 251.56ft. btoc = Feet Below Top of Casing Clayton, Johnston County, North CarolinaECS Project 49:1226TOC = Top of Casing* = Survey performed by Bateman Civil Survey on June 25, 2015. The site vertical datum is based on NAV88 and the horizontal datum is based on NAD83.Table 2Well Construction and Groundwater Elevation DetailsFlowers Store Property4181 NC Highway 42 EastNCDEQ Incident: 17217
Sample ID Sample DateBromodichloromethanesec-ButylbenzeneChloroformDibromochloromethaneIsopropylbenzeneNaphthalenen-Propylbenzene1,2-Dichloropropane1,4- Dichlorobenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTotal XylenesMW-3 1/26/2016BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLMW-5 1/26/2016BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLMW-7 1/26/2016BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLMW-8 1/26/2016BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLMW-9 1/26/2016BRL1.3BRL BRL1.018.42.0BRL0.51 8.5 16.3 1.2MW-10 1/26/2016BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLWSW-2 1/26/20165.4BRL11.81.3BRL BRL BRL BRL BRL BRL BRL BRLWSW-4 1/26/20166.0BRL13.31.3BRL BRL BRL BRL BRL BRL BRL BRLWSW-5 1/26/2016BRL BRL BRL BRL BRL BRL BRL1.7BRL BRL BRL BRL0.6 70 70 0.4 70 6 70 0.6 6 400 400 500NE 8,500 70,000 400 25,000 6,000 30,000 600 6,000 28,500 25,000 85,500BRL = Below Laboratory Reporting LimitTable 3Summary of Current Groundwater Analytical ResultsFlowers Store Property4181 NC Highway 42 EastNC2LGWS (µg/L)GCL (µg/L) Clayton, Johnston County, North CarolinaECS Project 49:1226Analytical MethodNCDEQ Incident: 17217NC2LGWQS = North Carolina 2L Groundwater Quality Standard as of April 1, 2013 GCL = NCDEQ's Gross Contamination Levels for Groundwater as of April 16, 2012Bold = Detected above NC2LGWQSµg/L = Micrograms per LiterStandard Method 6200BNE = Not Established
EPA Method 625EPA Method 6010Monitoring Well IDDate9/2/2008BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL6.68 67 91 350 2509/30/2009BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL0.89BRL BRL BRL BRL BRL10/4/20129/2/2008BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL9/30/2009BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL0.71BRL BRL BRL BRL BRL10/4/20129/2/2008BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL9/30/2009BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL1110/4/2012BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLBRL2/19/2013BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL0.15 JBRL BRL BRL BRL7.28/13/20146/11/2015BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS NS NS NS NS1/26/2016BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSNSNSNSNS9/2/2008BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL9/30/200910/4/20122/19/2013 0.27 J 0.46 JBRL5.2 J 1.2 0.29BRL0.49 JBRL BRL BRL BRL BRL110BRL BRL158/13/2014BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL1,746.7BRL64921.56/11/2015BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS NS NS NS NS1/26/2016BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSNSNSNSNS2/19/2013BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL0.538/13/2014BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL6/12/2015BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS NS NS NS NS1/26/2016BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSNSNSNSNS6/12/2015BRL BRL0.61BRL BRL BRL BRL BRL BRL BRL BRL BRL NS NS NS NS NS1/26/2016BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSNSNSNSNS6/12/2015 15.7 27.7BRL BRL BRL2.1 1.6BRL3.317.13.7BRL NS NS NS NS NS1/26/20168.516.30.51BRLBRL1.30.97BRL2.018.41.2BRLNSNSNSNSNS6/12/2015BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL NS NS NS NS NS1/26/2016BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLBRLNSNSNSNSNSMW-8MW-9MW-10210 15NCDEQ Incident: 17217di-n-Butyl phthalateC9-C18 Aliphatics1,2,4-Trimethylbenzenesec-ButylbenzeneTetrachloroetheneECS Project 49:1226Standard Method 6200B (or equivalent)MADEP EPH/VPHDestroyedp-IsopropyltolueneC19-C36AliphaticsNENE 15,000254,2006,000,0001,3,5-Trimethylbenzene1,4-DichlorobenzeneIsopropylbenzeneNaphthaleneTotal XylenesWell Dry42,000NE8,5006 50030,000 6,000Contaminant of Concern (µg/L)TW-1Table 4Summary of Historical Groundwater Analytical ResultsFlowers Store Property4181 NC Highway 42 EastClayton, Johnston County, North CarolinaAcetoneAnalytical MethodDestroyedn-ButylbenzeneMW-3 (TW-3)n-PropylbenzeneNC2LGWQS = North Carolina 2L Groundwater Quality Standard as of April 1, 2013 GCL = NCDEQ's Gross Contamination Levels for Groundwater as of April 16, 201270TW-2DestroyedC9-C22 AromaticsLead TW-4Destroyed85,5006,0007025,00070700400 400MW-5Bold = Detected above the NC2LGWQS µg/L = Micrograms per LiterBRL = Below Laboratory Reporting LimitJ = Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit28,500 25,000706,0006NE70011,700NE = Not EstablishedNS = Not SampledMW-71NC2LGWQS (µg/L)GCL (µg/L)6,900
WSW-1 6/17/2008BRL10.4BRL BRL BRL59 160 160WSW-2 1/26/2016 5.4BRL11.8 1.3BRL NS NS NS6/17/2008BRL1.22BRL BRL BRL56 1301508/13/2014 12.6BRL39.44.3BRL NS NSNS6/11/2015 12.4BRL24.14.6BRL NS NSNS1/26/20166.0BRL13.31.3BRLNSNSNS8/13/2014BRL BRL BRL BRL1.4NS NSNS6/11/2015BRL BRL BRL BRL2.1NS NSNS1/26/2016BRLBRLBRLBRL1.7NSNSNSWSW-68/13/2014BRLBRLBRLBRLBRLNSNSNSNE 3 70 0.4 0.6 700 10,000200NE17070,000400600NENENENC2LGWQS = North Carolina 2L Groundwater Quality Standard as of April 1, 2013 GCL = NCDEQ's Gross Contamination Levels for Groundwater as of April 16, 2012Bold = Detected above the NC2LGWQSµg/L = Micrograms per LiterBRL = Below Laboratory Reporting LimitNS = Not SampledNE = Not EstablishedChloroformDibromochloromethaneContaminant of Concern (ug/L)Water Supply Well IDBis (2-ethylhexyl) PhthalateWSW-4WSW-5C19-C36 AliphaticsTable 5Summary of Current Historical Water Supply Well Analytical ResultsFlowers Store Property4181 NC Highway 42 EastClayton, Johnston County, North CarolinaECS Project 49:1226C11-C22 AromaticsNCDEQ Incident: 17217GCL (µg/L)NC2LGWQSAnalytical Method1,2-DichloropropaneDate CollectedBromodichloromethaneStandard Method 6200B (or equivalent) MADEP EPH/VPHC9-C18 Aliphatics
SB-5 1 2/13/2013BRL BRL BRL BRL BRL BRL BRL BRLSB-5 13 2/13/2013BRL BRL BRL BRL BRL BRL BRL BRLSB-5 18 2/13/2013BRL BRL BRL BRL0.26BRL39BRLSB-5 23 2/13/2013 0.0020 0.0049 0.0011J 0.22 3.7 128 46758.3 4.3 3.3 6.6 120 540 Immobile 31782 626 626 46 62,571 1,500 31,000 46920,440 16,350 16,350 410 1,635,200 40,000 810,000 12,264mg/kg = milligrams per kilogramBRL = Below Laboratory Reporting LimitC19-C36 AliphaticsDate CollectedResidential MSCCContaminant of Concern (mg/kg)Depth Collected (Ft.)Benzoic AcidC9-C18 AliphaticsC9-C22 Aromaticsn-ButylbenzeneIndustrial/Commercial MSCCSample IDsec-ButylbenzeneSoil to Groundwater MSCC1,3,5-TrimethylbenzeneECS Project 49:1226MSCC = Maximum Soil Contaminant Concentration LevelsAnalytical Method EPA Method 8260B EPA Method 8270D MADEP EPH/VPHNCDEQ = North Carolina Department of Environmental Qualitybis(2-Ethylhexyl)phthalateTable 6Summary of Historical Soil Sample Analytical ResultsFlowers Store Property4181 NC Highway 42 EastClayton, Johnston County, North CarolinaNCDEQ Incident: 17217
Water Supply Well Parcel Address Owner Owner Address Water Well StatusConnected to Municipal WaterApproximate Distance from Source AreaWSW-14181 NC Highway 42 Clayton, NC 27527Flowers, Pamela105 Southridge Drive Garner, NC 27527Abandoned Yes 540 feet northeastWSW-24116 NC Highway 42 Clayton, NC 27527Flowers, Jimmy4116 NC Highway 42 Clayton, NC 27527Unknown Yes 350 feet southWSW-3 Not Listed Flowers, Peggy4400 NC Highway 42 Clayton, NC 27527Unknown Yes 1,000+ feet westWSW-44300 NC Highway 42 Clayton, NC 27527Valcourt, Richard J and Blanchard, Sarah4709 Chickpay Dr Raleigh NC, 27610Potable No 975 feet southeastWSW-5160 Motorcycle Rd Clayton, NC 27527Robertson, Drake160 Motorcycle Rd Clayton, NC 27527Potable No 525 feet northwestWSW-6270 Motorcycle Rd Clayton, NC 27527Pineville Chapel Church270 Motorcycle Road Clayton, NC 27527Unknown Unknown 1,000+ feet northwestTable 7Water Supply Well SurveyFlowers Store Property4181 NC Highway 42 EastClayton, Johnson County, North CarolinaECS Project 49:1226NCDEQ Incident: 17217

APPENDIX A

APPENDIX B
SITE PHOTOGRAPHS
FLOWERS STORE PROPERTY
4181 NC HIGHWAY 42 EAST
CLAYTON, JOHNSON COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: 17217
ECS PROJECT NO 49:1226
Photograph 1: View of the subject site. View is to the northeast.
Photograph 2: View of monitoring well MW-8

APPENDIX C

#=CL#
February 02, 2016
LIMS USE: FR - MATTHEW GILLIS
LIMS OBJECT ID: 92284408
92284408
Project:
Pace Project No.:
RE:
Matthew Gillis
ECS
9001 Glenwood Avenue
Raleigh, NC 27617
FLOWERS STORE PROPERTY
Dear Matthew Gillis:
Enclosed are the analytical results for sample(s) received by the laboratory on January 27, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
Enclosures
cc:Brian Smith, ECS Carolinas LLP
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 35
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 35
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92284408005 MW-9
sec-Butylbenzene 1.3 ug/L 02/02/16 03:010.50SM 6200B
1,4-Dichlorobenzene 0.51 ug/L 02/02/16 03:010.50SM 6200B
Isopropylbenzene (Cumene)0.97 ug/L 02/02/16 03:010.50SM 6200B
Naphthalene 18.4 ug/L 02/02/16 03:012.0SM 6200B
n-Propylbenzene 2.0 ug/L 02/02/16 03:010.50SM 6200B
1,2,4-Trimethylbenzene 8.5 ug/L 02/02/16 03:010.50SM 6200B
1,3,5-Trimethylbenzene 16.3 ug/L 02/02/16 03:010.50SM 6200B
o-Xylene 1.2 ug/L 02/02/16 03:010.50SM 6200B
92284408007 WSW-2
Bromodichloromethane 5.4 ug/L 02/02/16 03:350.50SM 6200B
Chloroform 11.8 ug/L 02/02/16 03:350.50SM 6200B
Dibromochloromethane 1.3 ug/L 02/02/16 03:350.50SM 6200B
92284408008 WSW-4
Bromodichloromethane 6.0 ug/L 02/02/16 03:520.50SM 6200B
Chloroform 13.3 ug/L 02/02/16 03:520.50SM 6200B
Dibromochloromethane 1.3 ug/L 02/02/16 03:520.50SM 6200B
92284408009 WSW-5
1,2-Dichloropropane 1.7 ug/L 02/02/16 04:090.50SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-7 Lab ID:92284408001 Collected:01/26/16 11:48 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 02/01/16 17:42 71-43-20.50 1
Bromobenzene ND ug/L 02/01/16 17:42 108-86-10.50 1
Bromochloromethane ND ug/L 02/01/16 17:42 74-97-50.50 1
Bromodichloromethane ND ug/L 02/01/16 17:42 75-27-40.50 1
Bromoform ND ug/L 02/01/16 17:42 75-25-20.50 1
Bromomethane ND ug/L 02/01/16 17:42 74-83-95.0 1
n-Butylbenzene ND ug/L 02/01/16 17:42 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/01/16 17:42 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/01/16 17:42 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/01/16 17:42 56-23-50.50 1
Chlorobenzene ND ug/L 02/01/16 17:42 108-90-70.50 1
Chloroethane ND ug/L 02/01/16 17:42 75-00-31.0 1
Chloroform ND ug/L 02/01/16 17:42 67-66-30.50 1
Chloromethane ND ug/L 02/01/16 17:42 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/01/16 17:42 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/01/16 17:42 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/01/16 17:42 96-12-81.0 1
Dibromochloromethane ND ug/L 02/01/16 17:42 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/01/16 17:42 106-93-40.50 1
Dibromomethane ND ug/L 02/01/16 17:42 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/01/16 17:42 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/01/16 17:42 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/01/16 17:42 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/01/16 17:42 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/01/16 17:42 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/01/16 17:42 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/01/16 17:42 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/01/16 17:42 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/01/16 17:42 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/01/16 17:42 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/01/16 17:42 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/01/16 17:42 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/01/16 17:42 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/01/16 17:42 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/01/16 17:42 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/01/16 17:42 108-20-30.50 1
Ethylbenzene ND ug/L 02/01/16 17:42 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/01/16 17:42 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/01/16 17:42 98-82-80.50 1
Methylene Chloride ND ug/L 02/01/16 17:42 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/01/16 17:42 1634-04-40.50 1
Naphthalene ND ug/L 02/01/16 17:42 91-20-32.0 1
n-Propylbenzene ND ug/L 02/01/16 17:42 103-65-10.50 1
Styrene ND ug/L 02/01/16 17:42 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/01/16 17:42 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/01/16 17:42 79-34-50.50 1
Tetrachloroethene ND ug/L 02/01/16 17:42 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-7 Lab ID:92284408001 Collected:01/26/16 11:48 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 02/01/16 17:42 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/01/16 17:42 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/01/16 17:42 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/01/16 17:42 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/01/16 17:42 79-00-50.50 1
Trichloroethene ND ug/L 02/01/16 17:42 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/01/16 17:42 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/01/16 17:42 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/01/16 17:42 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/01/16 17:42 108-67-80.50 1
Vinyl chloride ND ug/L 02/01/16 17:42 75-01-41.0 1
m&p-Xylene ND ug/L 02/01/16 17:42 179601-23-11.0 1
o-Xylene ND ug/L 02/01/16 17:42 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)105 %02/01/16 17:42 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %02/01/16 17:42 460-00-470-130 1
Toluene-d8 (S)101 %02/01/16 17:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-8 Lab ID:92284408002 Collected:01/26/16 12:15 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 02/01/16 17:59 71-43-20.50 1
Bromobenzene ND ug/L 02/01/16 17:59 108-86-10.50 1
Bromochloromethane ND ug/L 02/01/16 17:59 74-97-50.50 1
Bromodichloromethane ND ug/L 02/01/16 17:59 75-27-40.50 1
Bromoform ND ug/L 02/01/16 17:59 75-25-20.50 1
Bromomethane ND ug/L 02/01/16 17:59 74-83-95.0 1
n-Butylbenzene ND ug/L 02/01/16 17:59 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/01/16 17:59 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/01/16 17:59 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/01/16 17:59 56-23-50.50 1
Chlorobenzene ND ug/L 02/01/16 17:59 108-90-70.50 1
Chloroethane ND ug/L 02/01/16 17:59 75-00-31.0 1
Chloroform ND ug/L 02/01/16 17:59 67-66-30.50 1
Chloromethane ND ug/L 02/01/16 17:59 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/01/16 17:59 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/01/16 17:59 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/01/16 17:59 96-12-81.0 1
Dibromochloromethane ND ug/L 02/01/16 17:59 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/01/16 17:59 106-93-40.50 1
Dibromomethane ND ug/L 02/01/16 17:59 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/01/16 17:59 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/01/16 17:59 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/01/16 17:59 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/01/16 17:59 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/01/16 17:59 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/01/16 17:59 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/01/16 17:59 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/01/16 17:59 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/01/16 17:59 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/01/16 17:59 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/01/16 17:59 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/01/16 17:59 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/01/16 17:59 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/01/16 17:59 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/01/16 17:59 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/01/16 17:59 108-20-30.50 1
Ethylbenzene ND ug/L 02/01/16 17:59 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/01/16 17:59 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/01/16 17:59 98-82-80.50 1
Methylene Chloride ND ug/L 02/01/16 17:59 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/01/16 17:59 1634-04-40.50 1
Naphthalene ND ug/L 02/01/16 17:59 91-20-32.0 1
n-Propylbenzene ND ug/L 02/01/16 17:59 103-65-10.50 1
Styrene ND ug/L 02/01/16 17:59 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/01/16 17:59 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/01/16 17:59 79-34-50.50 1
Tetrachloroethene ND ug/L 02/01/16 17:59 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-8 Lab ID:92284408002 Collected:01/26/16 12:15 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 02/01/16 17:59 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/01/16 17:59 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/01/16 17:59 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/01/16 17:59 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/01/16 17:59 79-00-50.50 1
Trichloroethene ND ug/L 02/01/16 17:59 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/01/16 17:59 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/01/16 17:59 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/01/16 17:59 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/01/16 17:59 108-67-80.50 1
Vinyl chloride ND ug/L 02/01/16 17:59 75-01-41.0 1
m&p-Xylene ND ug/L 02/01/16 17:59 179601-23-11.0 1
o-Xylene ND ug/L 02/01/16 17:59 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)104 %02/01/16 17:59 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %02/01/16 17:59 460-00-470-130 1
Toluene-d8 (S)101 %02/01/16 17:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-3 Lab ID:92284408003 Collected:01/26/16 12:41 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 02/01/16 18:16 71-43-20.50 1
Bromobenzene ND ug/L 02/01/16 18:16 108-86-10.50 1
Bromochloromethane ND ug/L 02/01/16 18:16 74-97-50.50 1
Bromodichloromethane ND ug/L 02/01/16 18:16 75-27-40.50 1
Bromoform ND ug/L 02/01/16 18:16 75-25-20.50 1
Bromomethane ND ug/L 02/01/16 18:16 74-83-95.0 1
n-Butylbenzene ND ug/L 02/01/16 18:16 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/01/16 18:16 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/01/16 18:16 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/01/16 18:16 56-23-50.50 1
Chlorobenzene ND ug/L 02/01/16 18:16 108-90-70.50 1
Chloroethane ND ug/L 02/01/16 18:16 75-00-31.0 1
Chloroform ND ug/L 02/01/16 18:16 67-66-30.50 1
Chloromethane ND ug/L 02/01/16 18:16 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/01/16 18:16 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/01/16 18:16 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/01/16 18:16 96-12-81.0 1
Dibromochloromethane ND ug/L 02/01/16 18:16 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/01/16 18:16 106-93-40.50 1
Dibromomethane ND ug/L 02/01/16 18:16 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/01/16 18:16 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/01/16 18:16 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/01/16 18:16 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/01/16 18:16 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/01/16 18:16 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/01/16 18:16 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/01/16 18:16 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/01/16 18:16 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/01/16 18:16 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/01/16 18:16 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/01/16 18:16 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/01/16 18:16 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/01/16 18:16 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/01/16 18:16 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/01/16 18:16 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/01/16 18:16 108-20-30.50 1
Ethylbenzene ND ug/L 02/01/16 18:16 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/01/16 18:16 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/01/16 18:16 98-82-80.50 1
Methylene Chloride ND ug/L 02/01/16 18:16 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/01/16 18:16 1634-04-40.50 1
Naphthalene ND ug/L 02/01/16 18:16 91-20-32.0 1
n-Propylbenzene ND ug/L 02/01/16 18:16 103-65-10.50 1
Styrene ND ug/L 02/01/16 18:16 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/01/16 18:16 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/01/16 18:16 79-34-50.50 1
Tetrachloroethene ND ug/L 02/01/16 18:16 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-3 Lab ID:92284408003 Collected:01/26/16 12:41 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 02/01/16 18:16 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/01/16 18:16 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/01/16 18:16 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/01/16 18:16 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/01/16 18:16 79-00-50.50 1
Trichloroethene ND ug/L 02/01/16 18:16 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/01/16 18:16 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/01/16 18:16 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/01/16 18:16 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/01/16 18:16 108-67-80.50 1
Vinyl chloride ND ug/L 02/01/16 18:16 75-01-41.0 1
m&p-Xylene ND ug/L 02/01/16 18:16 179601-23-11.0 1
o-Xylene ND ug/L 02/01/16 18:16 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %02/01/16 18:16 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %02/01/16 18:16 460-00-470-130 1
Toluene-d8 (S)100 %02/01/16 18:16 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-5 Lab ID:92284408004 Collected:01/26/16 13:08 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 02/02/16 02:44 71-43-20.50 1
Bromobenzene ND ug/L 02/02/16 02:44 108-86-10.50 1
Bromochloromethane ND ug/L 02/02/16 02:44 74-97-50.50 1
Bromodichloromethane ND ug/L 02/02/16 02:44 75-27-40.50 1
Bromoform ND ug/L 02/02/16 02:44 75-25-20.50 1
Bromomethane ND ug/L 02/02/16 02:44 74-83-95.0 1
n-Butylbenzene ND ug/L 02/02/16 02:44 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/02/16 02:44 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/02/16 02:44 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/02/16 02:44 56-23-50.50 1
Chlorobenzene ND ug/L 02/02/16 02:44 108-90-70.50 1
Chloroethane ND ug/L 02/02/16 02:44 75-00-31.0 1
Chloroform ND ug/L 02/02/16 02:44 67-66-30.50 1
Chloromethane ND ug/L 02/02/16 02:44 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/02/16 02:44 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/02/16 02:44 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/02/16 02:44 96-12-81.0 1
Dibromochloromethane ND ug/L 02/02/16 02:44 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/02/16 02:44 106-93-40.50 1
Dibromomethane ND ug/L 02/02/16 02:44 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/02/16 02:44 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/02/16 02:44 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/02/16 02:44 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/02/16 02:44 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/02/16 02:44 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/02/16 02:44 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/02/16 02:44 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/02/16 02:44 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/02/16 02:44 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/02/16 02:44 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/02/16 02:44 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/02/16 02:44 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/02/16 02:44 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/02/16 02:44 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/02/16 02:44 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/02/16 02:44 108-20-30.50 1
Ethylbenzene ND ug/L 02/02/16 02:44 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/02/16 02:44 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/02/16 02:44 98-82-80.50 1
Methylene Chloride ND ug/L 02/02/16 02:44 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/02/16 02:44 1634-04-40.50 1
Naphthalene ND ug/L 02/02/16 02:44 91-20-32.0 1
n-Propylbenzene ND ug/L 02/02/16 02:44 103-65-10.50 1
Styrene ND ug/L 02/02/16 02:44 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/02/16 02:44 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/02/16 02:44 79-34-50.50 1
Tetrachloroethene ND ug/L 02/02/16 02:44 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-5 Lab ID:92284408004 Collected:01/26/16 13:08 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 02/02/16 02:44 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/02/16 02:44 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/02/16 02:44 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/02/16 02:44 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/02/16 02:44 79-00-50.50 1
Trichloroethene ND ug/L 02/02/16 02:44 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/02/16 02:44 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/02/16 02:44 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/02/16 02:44 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/02/16 02:44 108-67-80.50 1
Vinyl chloride ND ug/L 02/02/16 02:44 75-01-41.0 1
m&p-Xylene ND ug/L 02/02/16 02:44 179601-23-11.0 1
o-Xylene ND ug/L 02/02/16 02:44 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %02/02/16 02:44 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %02/02/16 02:44 460-00-470-130 1
Toluene-d8 (S)99 %02/02/16 02:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-9 Lab ID:92284408005 Collected:01/26/16 13:34 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 02/02/16 03:01 71-43-20.50 1
Bromobenzene ND ug/L 02/02/16 03:01 108-86-10.50 1
Bromochloromethane ND ug/L 02/02/16 03:01 74-97-50.50 1
Bromodichloromethane ND ug/L 02/02/16 03:01 75-27-40.50 1
Bromoform ND ug/L 02/02/16 03:01 75-25-20.50 1
Bromomethane ND ug/L 02/02/16 03:01 74-83-95.0 1
n-Butylbenzene ND ug/L 02/02/16 03:01 104-51-80.50 1
sec-Butylbenzene 1.3 ug/L 02/02/16 03:01 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/02/16 03:01 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/02/16 03:01 56-23-50.50 1
Chlorobenzene ND ug/L 02/02/16 03:01 108-90-70.50 1
Chloroethane ND ug/L 02/02/16 03:01 75-00-31.0 1
Chloroform ND ug/L 02/02/16 03:01 67-66-30.50 1
Chloromethane ND ug/L 02/02/16 03:01 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/02/16 03:01 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/02/16 03:01 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/02/16 03:01 96-12-81.0 1
Dibromochloromethane ND ug/L 02/02/16 03:01 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/02/16 03:01 106-93-40.50 1
Dibromomethane ND ug/L 02/02/16 03:01 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/02/16 03:01 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/02/16 03:01 541-73-10.50 1
1,4-Dichlorobenzene 0.51 ug/L 02/02/16 03:01 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/02/16 03:01 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/02/16 03:01 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/02/16 03:01 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/02/16 03:01 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/02/16 03:01 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/02/16 03:01 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/02/16 03:01 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/02/16 03:01 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/02/16 03:01 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/02/16 03:01 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/02/16 03:01 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/02/16 03:01 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/02/16 03:01 108-20-30.50 1
Ethylbenzene ND ug/L 02/02/16 03:01 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/02/16 03:01 87-68-32.0 1
Isopropylbenzene (Cumene)0.97 ug/L 02/02/16 03:01 98-82-80.50 1
Methylene Chloride ND ug/L 02/02/16 03:01 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/02/16 03:01 1634-04-40.50 1
Naphthalene 18.4 ug/L 02/02/16 03:01 91-20-32.0 1
n-Propylbenzene 2.0 ug/L 02/02/16 03:01 103-65-10.50 1
Styrene ND ug/L 02/02/16 03:01 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/02/16 03:01 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/02/16 03:01 79-34-50.50 1
Tetrachloroethene ND ug/L 02/02/16 03:01 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-9 Lab ID:92284408005 Collected:01/26/16 13:34 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 02/02/16 03:01 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/02/16 03:01 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/02/16 03:01 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/02/16 03:01 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/02/16 03:01 79-00-50.50 1
Trichloroethene ND ug/L 02/02/16 03:01 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/02/16 03:01 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/02/16 03:01 96-18-40.50 1
1,2,4-Trimethylbenzene 8.5 ug/L 02/02/16 03:01 95-63-60.50 1
1,3,5-Trimethylbenzene 16.3 ug/L 02/02/16 03:01 108-67-80.50 1
Vinyl chloride ND ug/L 02/02/16 03:01 75-01-41.0 1
m&p-Xylene ND ug/L 02/02/16 03:01 179601-23-11.0 1
o-Xylene 1.2 ug/L 02/02/16 03:01 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %02/02/16 03:01 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %02/02/16 03:01 460-00-470-130 1
Toluene-d8 (S)101 %02/02/16 03:01 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-10 Lab ID:92284408006 Collected:01/26/16 11:08 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 02/02/16 03:18 71-43-20.50 1
Bromobenzene ND ug/L 02/02/16 03:18 108-86-10.50 1
Bromochloromethane ND ug/L 02/02/16 03:18 74-97-50.50 1
Bromodichloromethane ND ug/L 02/02/16 03:18 75-27-40.50 1
Bromoform ND ug/L 02/02/16 03:18 75-25-20.50 1
Bromomethane ND ug/L 02/02/16 03:18 74-83-95.0 1
n-Butylbenzene ND ug/L 02/02/16 03:18 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/02/16 03:18 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/02/16 03:18 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/02/16 03:18 56-23-50.50 1
Chlorobenzene ND ug/L 02/02/16 03:18 108-90-70.50 1
Chloroethane ND ug/L 02/02/16 03:18 75-00-31.0 1
Chloroform ND ug/L 02/02/16 03:18 67-66-30.50 1
Chloromethane ND ug/L 02/02/16 03:18 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/02/16 03:18 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/02/16 03:18 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/02/16 03:18 96-12-81.0 1
Dibromochloromethane ND ug/L 02/02/16 03:18 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/02/16 03:18 106-93-40.50 1
Dibromomethane ND ug/L 02/02/16 03:18 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/02/16 03:18 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/02/16 03:18 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/02/16 03:18 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/02/16 03:18 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/02/16 03:18 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/02/16 03:18 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/02/16 03:18 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/02/16 03:18 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/02/16 03:18 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/02/16 03:18 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/02/16 03:18 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/02/16 03:18 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/02/16 03:18 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/02/16 03:18 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/02/16 03:18 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/02/16 03:18 108-20-30.50 1
Ethylbenzene ND ug/L 02/02/16 03:18 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/02/16 03:18 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/02/16 03:18 98-82-80.50 1
Methylene Chloride ND ug/L 02/02/16 03:18 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/02/16 03:18 1634-04-40.50 1
Naphthalene ND ug/L 02/02/16 03:18 91-20-32.0 1
n-Propylbenzene ND ug/L 02/02/16 03:18 103-65-10.50 1
Styrene ND ug/L 02/02/16 03:18 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/02/16 03:18 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/02/16 03:18 79-34-50.50 1
Tetrachloroethene ND ug/L 02/02/16 03:18 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-10 Lab ID:92284408006 Collected:01/26/16 11:08 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 02/02/16 03:18 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/02/16 03:18 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/02/16 03:18 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/02/16 03:18 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/02/16 03:18 79-00-50.50 1
Trichloroethene ND ug/L 02/02/16 03:18 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/02/16 03:18 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/02/16 03:18 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/02/16 03:18 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/02/16 03:18 108-67-80.50 1
Vinyl chloride ND ug/L 02/02/16 03:18 75-01-41.0 1
m&p-Xylene ND ug/L 02/02/16 03:18 179601-23-11.0 1
o-Xylene ND ug/L 02/02/16 03:18 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %02/02/16 03:18 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %02/02/16 03:18 460-00-470-130 1
Toluene-d8 (S)100 %02/02/16 03:18 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:WSW-2 Lab ID:92284408007 Collected:01/26/16 14:25 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 02/02/16 03:35 71-43-20.50 1
Bromobenzene ND ug/L 02/02/16 03:35 108-86-10.50 1
Bromochloromethane ND ug/L 02/02/16 03:35 74-97-50.50 1
Bromodichloromethane 5.4 ug/L 02/02/16 03:35 75-27-40.50 1
Bromoform ND ug/L 02/02/16 03:35 75-25-20.50 1
Bromomethane ND ug/L 02/02/16 03:35 74-83-95.0 1
n-Butylbenzene ND ug/L 02/02/16 03:35 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/02/16 03:35 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/02/16 03:35 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/02/16 03:35 56-23-50.50 1
Chlorobenzene ND ug/L 02/02/16 03:35 108-90-70.50 1
Chloroethane ND ug/L 02/02/16 03:35 75-00-31.0 1
Chloroform 11.8 ug/L 02/02/16 03:35 67-66-30.50 1
Chloromethane ND ug/L 02/02/16 03:35 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/02/16 03:35 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/02/16 03:35 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/02/16 03:35 96-12-81.0 1
Dibromochloromethane 1.3 ug/L 02/02/16 03:35 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/02/16 03:35 106-93-40.50 1
Dibromomethane ND ug/L 02/02/16 03:35 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/02/16 03:35 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/02/16 03:35 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/02/16 03:35 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/02/16 03:35 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/02/16 03:35 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/02/16 03:35 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/02/16 03:35 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/02/16 03:35 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/02/16 03:35 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/02/16 03:35 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/02/16 03:35 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/02/16 03:35 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/02/16 03:35 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/02/16 03:35 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/02/16 03:35 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/02/16 03:35 108-20-30.50 1
Ethylbenzene ND ug/L 02/02/16 03:35 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/02/16 03:35 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/02/16 03:35 98-82-80.50 1
Methylene Chloride ND ug/L 02/02/16 03:35 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/02/16 03:35 1634-04-40.50 1
Naphthalene ND ug/L 02/02/16 03:35 91-20-32.0 1
n-Propylbenzene ND ug/L 02/02/16 03:35 103-65-10.50 1
Styrene ND ug/L 02/02/16 03:35 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/02/16 03:35 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/02/16 03:35 79-34-50.50 1
Tetrachloroethene ND ug/L 02/02/16 03:35 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:WSW-2 Lab ID:92284408007 Collected:01/26/16 14:25 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 02/02/16 03:35 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/02/16 03:35 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/02/16 03:35 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/02/16 03:35 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/02/16 03:35 79-00-50.50 1
Trichloroethene ND ug/L 02/02/16 03:35 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/02/16 03:35 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/02/16 03:35 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/02/16 03:35 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/02/16 03:35 108-67-80.50 1
Vinyl chloride ND ug/L 02/02/16 03:35 75-01-41.0 1
m&p-Xylene ND ug/L 02/02/16 03:35 179601-23-11.0 1
o-Xylene ND ug/L 02/02/16 03:35 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %02/02/16 03:35 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %02/02/16 03:35 460-00-470-130 1
Toluene-d8 (S)99 %02/02/16 03:35 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:WSW-4 Lab ID:92284408008 Collected:01/26/16 14:45 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 02/02/16 03:52 71-43-20.50 1
Bromobenzene ND ug/L 02/02/16 03:52 108-86-10.50 1
Bromochloromethane ND ug/L 02/02/16 03:52 74-97-50.50 1
Bromodichloromethane 6.0 ug/L 02/02/16 03:52 75-27-40.50 1
Bromoform ND ug/L 02/02/16 03:52 75-25-20.50 1
Bromomethane ND ug/L 02/02/16 03:52 74-83-95.0 1
n-Butylbenzene ND ug/L 02/02/16 03:52 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/02/16 03:52 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/02/16 03:52 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/02/16 03:52 56-23-50.50 1
Chlorobenzene ND ug/L 02/02/16 03:52 108-90-70.50 1
Chloroethane ND ug/L 02/02/16 03:52 75-00-31.0 1
Chloroform 13.3 ug/L 02/02/16 03:52 67-66-30.50 1
Chloromethane ND ug/L 02/02/16 03:52 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/02/16 03:52 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/02/16 03:52 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/02/16 03:52 96-12-81.0 1
Dibromochloromethane 1.3 ug/L 02/02/16 03:52 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/02/16 03:52 106-93-40.50 1
Dibromomethane ND ug/L 02/02/16 03:52 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/02/16 03:52 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/02/16 03:52 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/02/16 03:52 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/02/16 03:52 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/02/16 03:52 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/02/16 03:52 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/02/16 03:52 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/02/16 03:52 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/02/16 03:52 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/02/16 03:52 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/02/16 03:52 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/02/16 03:52 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/02/16 03:52 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/02/16 03:52 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/02/16 03:52 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/02/16 03:52 108-20-30.50 1
Ethylbenzene ND ug/L 02/02/16 03:52 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/02/16 03:52 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/02/16 03:52 98-82-80.50 1
Methylene Chloride ND ug/L 02/02/16 03:52 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/02/16 03:52 1634-04-40.50 1
Naphthalene ND ug/L 02/02/16 03:52 91-20-32.0 1
n-Propylbenzene ND ug/L 02/02/16 03:52 103-65-10.50 1
Styrene ND ug/L 02/02/16 03:52 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/02/16 03:52 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/02/16 03:52 79-34-50.50 1
Tetrachloroethene ND ug/L 02/02/16 03:52 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:WSW-4 Lab ID:92284408008 Collected:01/26/16 14:45 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 02/02/16 03:52 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/02/16 03:52 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/02/16 03:52 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/02/16 03:52 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/02/16 03:52 79-00-50.50 1
Trichloroethene ND ug/L 02/02/16 03:52 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/02/16 03:52 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/02/16 03:52 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/02/16 03:52 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/02/16 03:52 108-67-80.50 1
Vinyl chloride ND ug/L 02/02/16 03:52 75-01-41.0 1
m&p-Xylene ND ug/L 02/02/16 03:52 179601-23-11.0 1
o-Xylene ND ug/L 02/02/16 03:52 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %02/02/16 03:52 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %02/02/16 03:52 460-00-470-130 1
Toluene-d8 (S)98 %02/02/16 03:52 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:WSW-5 Lab ID:92284408009 Collected:01/26/16 15:10 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 02/02/16 04:09 71-43-20.50 1
Bromobenzene ND ug/L 02/02/16 04:09 108-86-10.50 1
Bromochloromethane ND ug/L 02/02/16 04:09 74-97-50.50 1
Bromodichloromethane ND ug/L 02/02/16 04:09 75-27-40.50 1
Bromoform ND ug/L 02/02/16 04:09 75-25-20.50 1
Bromomethane ND ug/L 02/02/16 04:09 74-83-9 M15.0 1
n-Butylbenzene ND ug/L 02/02/16 04:09 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/02/16 04:09 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/02/16 04:09 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/02/16 04:09 56-23-50.50 1
Chlorobenzene ND ug/L 02/02/16 04:09 108-90-70.50 1
Chloroethane ND ug/L 02/02/16 04:09 75-00-31.0 1
Chloroform ND ug/L 02/02/16 04:09 67-66-30.50 1
Chloromethane ND ug/L 02/02/16 04:09 74-87-3 M11.0 1
2-Chlorotoluene ND ug/L 02/02/16 04:09 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/02/16 04:09 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/02/16 04:09 96-12-81.0 1
Dibromochloromethane ND ug/L 02/02/16 04:09 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/02/16 04:09 106-93-40.50 1
Dibromomethane ND ug/L 02/02/16 04:09 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/02/16 04:09 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/02/16 04:09 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/02/16 04:09 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/02/16 04:09 75-71-8 M10.50 1
1,1-Dichloroethane ND ug/L 02/02/16 04:09 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/02/16 04:09 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/02/16 04:09 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/02/16 04:09 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/02/16 04:09 156-60-50.50 1
1,2-Dichloropropane 1.7 ug/L 02/02/16 04:09 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/02/16 04:09 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/02/16 04:09 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/02/16 04:09 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/02/16 04:09 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/02/16 04:09 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/02/16 04:09 108-20-30.50 1
Ethylbenzene ND ug/L 02/02/16 04:09 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/02/16 04:09 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/02/16 04:09 98-82-80.50 1
Methylene Chloride ND ug/L 02/02/16 04:09 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/02/16 04:09 1634-04-40.50 1
Naphthalene ND ug/L 02/02/16 04:09 91-20-32.0 1
n-Propylbenzene ND ug/L 02/02/16 04:09 103-65-10.50 1
Styrene ND ug/L 02/02/16 04:09 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/02/16 04:09 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/02/16 04:09 79-34-50.50 1
Tetrachloroethene ND ug/L 02/02/16 04:09 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
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Page 20 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:WSW-5 Lab ID:92284408009 Collected:01/26/16 15:10 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 02/02/16 04:09 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/02/16 04:09 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/02/16 04:09 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/02/16 04:09 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/02/16 04:09 79-00-50.50 1
Trichloroethene ND ug/L 02/02/16 04:09 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/02/16 04:09 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/02/16 04:09 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/02/16 04:09 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/02/16 04:09 108-67-80.50 1
Vinyl chloride ND ug/L 02/02/16 04:09 75-01-41.0 1
m&p-Xylene ND ug/L 02/02/16 04:09 179601-23-11.0 1
o-Xylene ND ug/L 02/02/16 04:09 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %02/02/16 04:09 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %02/02/16 04:09 460-00-470-130 1
Toluene-d8 (S)99 %02/02/16 04:09 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 21 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/35395
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92284408001, 92284408002, 92284408003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1657756
Associated Lab Samples:92284408001, 92284408002, 92284408003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 02/01/16 15:10
1,1,1-Trichloroethane ug/L ND 0.50 02/01/16 15:10
1,1,2,2-Tetrachloroethane ug/L ND 0.50 02/01/16 15:10
1,1,2-Trichloroethane ug/L ND 0.50 02/01/16 15:10
1,1-Dichloroethane ug/L ND 0.50 02/01/16 15:10
1,1-Dichloroethene ug/L ND 0.50 02/01/16 15:10
1,1-Dichloropropene ug/L ND 0.50 02/01/16 15:10
1,2,3-Trichlorobenzene ug/L ND 2.0 02/01/16 15:10
1,2,3-Trichloropropane ug/L ND 0.50 02/01/16 15:10
1,2,4-Trichlorobenzene ug/L ND 2.0 02/01/16 15:10
1,2,4-Trimethylbenzene ug/L ND 0.50 02/01/16 15:10
1,2-Dibromo-3-chloropropane ug/L ND 1.0 02/01/16 15:10
1,2-Dibromoethane (EDB)ug/L ND 0.50 02/01/16 15:10
1,2-Dichlorobenzene ug/L ND 0.50 02/01/16 15:10
1,2-Dichloroethane ug/L ND 0.50 02/01/16 15:10
1,2-Dichloropropane ug/L ND 0.50 02/01/16 15:10
1,3,5-Trimethylbenzene ug/L ND 0.50 02/01/16 15:10
1,3-Dichlorobenzene ug/L ND 0.50 02/01/16 15:10
1,3-Dichloropropane ug/L ND 0.50 02/01/16 15:10
1,4-Dichlorobenzene ug/L ND 0.50 02/01/16 15:10
2,2-Dichloropropane ug/L ND 0.50 02/01/16 15:10
2-Chlorotoluene ug/L ND 0.50 02/01/16 15:10
4-Chlorotoluene ug/L ND 0.50 02/01/16 15:10
Benzene ug/L ND 0.50 02/01/16 15:10
Bromobenzene ug/L ND 0.50 02/01/16 15:10
Bromochloromethane ug/L ND 0.50 02/01/16 15:10
Bromodichloromethane ug/L ND 0.50 02/01/16 15:10
Bromoform ug/L ND 0.50 02/01/16 15:10
Bromomethane ug/L ND 5.0 02/01/16 15:10
Carbon tetrachloride ug/L ND 0.50 02/01/16 15:10
Chlorobenzene ug/L ND 0.50 02/01/16 15:10
Chloroethane ug/L ND 1.0 02/01/16 15:10
Chloroform ug/L ND 0.50 02/01/16 15:10
Chloromethane ug/L ND 1.0 02/01/16 15:10
cis-1,2-Dichloroethene ug/L ND 0.50 02/01/16 15:10
cis-1,3-Dichloropropene ug/L ND 0.50 02/01/16 15:10
Dibromochloromethane ug/L ND 0.50 02/01/16 15:10
Dibromomethane ug/L ND 0.50 02/01/16 15:10
Dichlorodifluoromethane ug/L ND 0.50 02/01/16 15:10
Diisopropyl ether ug/L ND 0.50 02/01/16 15:10
Ethylbenzene ug/L ND 0.50 02/01/16 15:10
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
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Page 22 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1657756
Associated Lab Samples:92284408001, 92284408002, 92284408003
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 02/01/16 15:10
Isopropylbenzene (Cumene)ug/L ND 0.50 02/01/16 15:10
m&p-Xylene ug/L ND 1.0 02/01/16 15:10
Methyl-tert-butyl ether ug/L ND 0.50 02/01/16 15:10
Methylene Chloride ug/L ND 2.0 02/01/16 15:10
n-Butylbenzene ug/L ND 0.50 02/01/16 15:10
n-Propylbenzene ug/L ND 0.50 02/01/16 15:10
Naphthalene ug/L ND 2.0 02/01/16 15:10
o-Xylene ug/L ND 0.50 02/01/16 15:10
sec-Butylbenzene ug/L ND 0.50 02/01/16 15:10
Styrene ug/L ND 0.50 02/01/16 15:10
tert-Butylbenzene ug/L ND 0.50 02/01/16 15:10
Tetrachloroethene ug/L ND 0.50 02/01/16 15:10
Toluene ug/L ND 0.50 02/01/16 15:10
trans-1,2-Dichloroethene ug/L ND 0.50 02/01/16 15:10
trans-1,3-Dichloropropene ug/L ND 0.50 02/01/16 15:10
Trichloroethene ug/L ND 0.50 02/01/16 15:10
Trichlorofluoromethane ug/L ND 1.0 02/01/16 15:10
Vinyl chloride ug/L ND 1.0 02/01/16 15:10
1,2-Dichloroethane-d4 (S)%99 70-130 02/01/16 15:10
4-Bromofluorobenzene (S)%100 70-130 02/01/16 15:10
Toluene-d8 (S)%101 70-130 02/01/16 15:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1657757LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.850 102 60-140
1,1,1-Trichloroethane ug/L 46.750 93 60-140
1,1,2,2-Tetrachloroethane ug/L 48.650 97 60-140
1,1,2-Trichloroethane ug/L 47.950 96 60-140
1,1-Dichloroethane ug/L 45.450 91 60-140
1,1-Dichloroethene ug/L 45.250 90 60-140
1,1-Dichloropropene ug/L 47.350 95 60-140
1,2,3-Trichlorobenzene ug/L 53.250 106 60-140
1,2,3-Trichloropropane ug/L 50.650 101 60-140
1,2,4-Trichlorobenzene ug/L 52.550 105 60-140
1,2,4-Trimethylbenzene ug/L 49.650 99 60-140
1,2-Dibromo-3-chloropropane ug/L 54.250 108 60-140
1,2-Dibromoethane (EDB)ug/L 50.950 102 60-140
1,2-Dichlorobenzene ug/L 48.550 97 60-140
1,2-Dichloroethane ug/L 42.250 84 60-140
1,2-Dichloropropane ug/L 46.450 93 60-140
1,3,5-Trimethylbenzene ug/L 47.950 96 60-140
1,3-Dichlorobenzene ug/L 49.350 99 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
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Huntersville, NC 28078
[phone]
Page 23 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1657757LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 48.150 96 60-140
1,4-Dichlorobenzene ug/L 49.050 98 60-140
2,2-Dichloropropane ug/L 48.350 97 60-140
2-Chlorotoluene ug/L 47.250 94 60-140
4-Chlorotoluene ug/L 47.750 95 60-140
Benzene ug/L 48.950 98 60-140
Bromobenzene ug/L 49.050 98 60-140
Bromochloromethane ug/L 46.850 94 60-140
Bromodichloromethane ug/L 49.350 99 60-140
Bromoform ug/L 60.150 120 60-140
Bromomethane ug/L 34.650 69 60-140
Carbon tetrachloride ug/L 49.050 98 60-140
Chlorobenzene ug/L 47.350 95 60-140
Chloroethane ug/L 45.950 92 60-140
Chloroform ug/L 44.950 90 60-140
Chloromethane ug/L 37.350 75 60-140
cis-1,2-Dichloroethene ug/L 44.350 89 60-140
cis-1,3-Dichloropropene ug/L 49.750 99 60-140
Dibromochloromethane ug/L 56.350 113 60-140
Dibromomethane ug/L 49.050 98 60-140
Dichlorodifluoromethane ug/L 30.250 60 60-140
Diisopropyl ether ug/L 47.650 95 60-140
Ethylbenzene ug/L 46.850 94 60-140
Hexachloro-1,3-butadiene ug/L 52.550 105 60-140
Isopropylbenzene (Cumene)ug/L 46.650 93 60-140
m&p-Xylene ug/L 92.6100 93 60-140
Methyl-tert-butyl ether ug/L 49.850 100 60-140
Methylene Chloride ug/L 43.850 88 60-140
n-Butylbenzene ug/L 49.150 98 60-140
n-Propylbenzene ug/L 46.850 94 60-140
Naphthalene ug/L 52.550 105 60-140
o-Xylene ug/L 45.850 92 60-140
sec-Butylbenzene ug/L 46.950 94 60-140
Styrene ug/L 49.650 99 60-140
tert-Butylbenzene ug/L 39.650 79 60-140
Tetrachloroethene ug/L 46.450 93 60-140
Toluene ug/L 45.550 91 60-140
trans-1,2-Dichloroethene ug/L 45.650 91 60-140
trans-1,3-Dichloropropene ug/L 50.050 100 60-140
Trichloroethene ug/L 45.450 91 60-140
Trichlorofluoromethane ug/L 43.350 87 60-140
Vinyl chloride ug/L 41.150 82 60-140
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
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Huntersville, NC 28078
[phone]
Page 24 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1657758MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92284408003
1657759
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 104 60-140108 420ND20.8 21.6
1,1,1-Trichloroethane ug/L 20 111 60-140111 020ND22.1 22.2
1,1,2,2-Tetrachloroethane ug/L 20 101 60-140104 220ND20.3 20.7
1,1,2-Trichloroethane ug/L 20 104 60-140105 120ND20.8 20.9
1,1-Dichloroethane ug/L 20 105 60-140107 120ND21.1 21.4
1,1-Dichloroethene ug/L 20 112 60-140111 120ND22.4 22.2
1,1-Dichloropropene ug/L 20 112 60-140112 020ND22.3 22.4
1,2,3-Trichlorobenzene ug/L 20 106 60-140112 620ND21.1 22.4
1,2,3-Trichloropropane ug/L 20 104 60-140108 420ND20.9 21.7
1,2,4-Trichlorobenzene ug/L 20 105 60-140110 420ND21.0 21.9
1,2,4-Trimethylbenzene ug/L 20 104 60-140109 420ND20.8 21.8
1,2-Dibromo-3-chloropropane ug/L 20 104 60-140109 420ND20.9 21.8
1,2-Dibromoethane (EDB)ug/L 20 106 60-140111 420ND21.2 22.1
1,2-Dichlorobenzene ug/L 20 101 60-140105 520ND20.1 21.1
1,2-Dichloroethane ug/L 20 97 60-14098 120ND19.6 19.8
1,2-Dichloropropane ug/L 20 102 60-140103 220ND20.3 20.7
1,3,5-Trimethylbenzene ug/L 20 102 60-140106 420ND20.4 21.2
1,3-Dichlorobenzene ug/L 20 102 60-140107 520ND20.5 21.5
1,3-Dichloropropane ug/L 20 101 60-140103 220ND20.2 20.6
1,4-Dichlorobenzene ug/L 20 102 60-140107 520ND20.6 21.6
2,2-Dichloropropane ug/L 20 105 60-140106 120ND21.0 21.3
2-Chlorotoluene ug/L 20 98 60-140103 520ND19.7 20.6
4-Chlorotoluene ug/L 20 101 60-140106 520ND20.2 21.2
Benzene ug/L 20 111 60-140111 020ND22.2 22.2
Bromobenzene ug/L 20 107 60-140114 620ND21.5 22.8
Bromochloromethane ug/L 20 105 60-140106 120ND20.9 21.2
Bromodichloromethane ug/L 20 103 60-140105 220ND20.6 21.0
Bromoform ug/L 20 95 60-140103 820ND19.0 20.6
Bromomethane ug/L 20 81 60-14076 620ND16.1 15.2
Carbon tetrachloride ug/L 20 108 60-140111 320ND21.6 22.2
Chlorobenzene ug/L 20 102 60-140106 420ND20.4 21.2
Chloroethane ug/L 20 118 60-140115 220ND23.5 23.0
Chloroform ug/L 20 103 60-140106 320ND20.6 21.1
Chloromethane ug/L 20 98 60-140100 120ND19.7 19.9
cis-1,2-Dichloroethene ug/L 20 105 60-140106 120ND20.9 21.2
cis-1,3-Dichloropropene ug/L 20 101 60-140104 320ND20.2 20.8
Dibromochloromethane ug/L 20 102 60-140110 820ND20.4 22.1
Dibromomethane ug/L 20 108 60-140108 020ND21.6 21.5
Dichlorodifluoromethane ug/L 20 102 60-140104 120ND20.4 20.7
Diisopropyl ether ug/L 20 107 60-140108 120ND21.3 21.6
Ethylbenzene ug/L 20 102 60-140106 320ND20.5 21.2
Hexachloro-1,3-butadiene ug/L 20 101 60-140104 320ND20.1 20.8
Isopropylbenzene (Cumene)ug/L 20 102 60-140105 420ND20.3 21.1
m&p-Xylene ug/L 40 102 60-140106 340ND40.8 42.2
Methyl-tert-butyl ether ug/L 20 111 60-140113 220ND22.1 22.6
Methylene Chloride ug/L 20 99 60-14099 020ND20.1 20.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
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Page 25 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1657758MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92284408003
1657759
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 101 60-140104 320ND20.1 20.8
n-Propylbenzene ug/L 20 100 60-140105 520ND20.1 21.0
Naphthalene ug/L 20 107 60-140112 520ND21.3 22.5
o-Xylene ug/L 20 101 60-140104 320ND20.2 20.8
sec-Butylbenzene ug/L 20 100 60-140105 520ND19.9 20.9
Styrene ug/L 20 103 60-140106 320ND20.7 21.3
tert-Butylbenzene ug/L 20 85 60-14089 420ND17.0 17.8
Tetrachloroethene ug/L 20 102 60-140106 420ND20.4 21.2
Toluene ug/L 20 102 60-140104 220ND20.5 20.9
trans-1,2-Dichloroethene ug/L 20 105 60-140108 320ND21.1 21.7
trans-1,3-Dichloropropene ug/L 20 100 60-140103 320ND20.1 20.6
Trichloroethene ug/L 20 104 60-140105 120ND20.7 20.9
Trichlorofluoromethane ug/L 20 111 60-140113 220ND22.2 22.5
Vinyl chloride ug/L 20 109 60-140111 220ND21.7 22.1
1,2-Dichloroethane-d4 (S)%103 70-130100
4-Bromofluorobenzene (S)%101 70-130102
Toluene-d8 (S)%100 70-13099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
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[phone]
Page 26 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/35397
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92284408004, 92284408005, 92284408006, 92284408007, 92284408008, 92284408009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1657779
Associated Lab Samples:92284408004, 92284408005, 92284408006, 92284408007, 92284408008, 92284408009
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 02/02/16 02:27
1,1,1-Trichloroethane ug/L ND 0.50 02/02/16 02:27
1,1,2,2-Tetrachloroethane ug/L ND 0.50 02/02/16 02:27
1,1,2-Trichloroethane ug/L ND 0.50 02/02/16 02:27
1,1-Dichloroethane ug/L ND 0.50 02/02/16 02:27
1,1-Dichloroethene ug/L ND 0.50 02/02/16 02:27
1,1-Dichloropropene ug/L ND 0.50 02/02/16 02:27
1,2,3-Trichlorobenzene ug/L ND 2.0 02/02/16 02:27
1,2,3-Trichloropropane ug/L ND 0.50 02/02/16 02:27
1,2,4-Trichlorobenzene ug/L ND 2.0 02/02/16 02:27
1,2,4-Trimethylbenzene ug/L ND 0.50 02/02/16 02:27
1,2-Dibromo-3-chloropropane ug/L ND 1.0 02/02/16 02:27
1,2-Dibromoethane (EDB)ug/L ND 0.50 02/02/16 02:27
1,2-Dichlorobenzene ug/L ND 0.50 02/02/16 02:27
1,2-Dichloroethane ug/L ND 0.50 02/02/16 02:27
1,2-Dichloropropane ug/L ND 0.50 02/02/16 02:27
1,3,5-Trimethylbenzene ug/L ND 0.50 02/02/16 02:27
1,3-Dichlorobenzene ug/L ND 0.50 02/02/16 02:27
1,3-Dichloropropane ug/L ND 0.50 02/02/16 02:27
1,4-Dichlorobenzene ug/L ND 0.50 02/02/16 02:27
2,2-Dichloropropane ug/L ND 0.50 02/02/16 02:27
2-Chlorotoluene ug/L ND 0.50 02/02/16 02:27
4-Chlorotoluene ug/L ND 0.50 02/02/16 02:27
Benzene ug/L ND 0.50 02/02/16 02:27
Bromobenzene ug/L ND 0.50 02/02/16 02:27
Bromochloromethane ug/L ND 0.50 02/02/16 02:27
Bromodichloromethane ug/L ND 0.50 02/02/16 02:27
Bromoform ug/L ND 0.50 02/02/16 02:27
Bromomethane ug/L ND 5.0 02/02/16 02:27
Carbon tetrachloride ug/L ND 0.50 02/02/16 02:27
Chlorobenzene ug/L ND 0.50 02/02/16 02:27
Chloroethane ug/L ND 1.0 02/02/16 02:27
Chloroform ug/L ND 0.50 02/02/16 02:27
Chloromethane ug/L ND 1.0 02/02/16 02:27
cis-1,2-Dichloroethene ug/L ND 0.50 02/02/16 02:27
cis-1,3-Dichloropropene ug/L ND 0.50 02/02/16 02:27
Dibromochloromethane ug/L ND 0.50 02/02/16 02:27
Dibromomethane ug/L ND 0.50 02/02/16 02:27
Dichlorodifluoromethane ug/L ND 0.50 02/02/16 02:27
Diisopropyl ether ug/L ND 0.50 02/02/16 02:27
Ethylbenzene ug/L ND 0.50 02/02/16 02:27
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
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Page 27 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1657779
Associated Lab Samples:92284408004, 92284408005, 92284408006, 92284408007, 92284408008, 92284408009
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 02/02/16 02:27
Isopropylbenzene (Cumene)ug/L ND 0.50 02/02/16 02:27
m&p-Xylene ug/L ND 1.0 02/02/16 02:27
Methyl-tert-butyl ether ug/L ND 0.50 02/02/16 02:27
Methylene Chloride ug/L ND 2.0 02/02/16 02:27
n-Butylbenzene ug/L ND 0.50 02/02/16 02:27
n-Propylbenzene ug/L ND 0.50 02/02/16 02:27
Naphthalene ug/L ND 2.0 02/02/16 02:27
o-Xylene ug/L ND 0.50 02/02/16 02:27
sec-Butylbenzene ug/L ND 0.50 02/02/16 02:27
Styrene ug/L ND 0.50 02/02/16 02:27
tert-Butylbenzene ug/L ND 0.50 02/02/16 02:27
Tetrachloroethene ug/L ND 0.50 02/02/16 02:27
Toluene ug/L ND 0.50 02/02/16 02:27
trans-1,2-Dichloroethene ug/L ND 0.50 02/02/16 02:27
trans-1,3-Dichloropropene ug/L ND 0.50 02/02/16 02:27
Trichloroethene ug/L ND 0.50 02/02/16 02:27
Trichlorofluoromethane ug/L ND 1.0 02/02/16 02:27
Vinyl chloride ug/L ND 1.0 02/02/16 02:27
1,2-Dichloroethane-d4 (S)%102 70-130 02/02/16 02:27
4-Bromofluorobenzene (S)%100 70-130 02/02/16 02:27
Toluene-d8 (S)%100 70-130 02/02/16 02:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1657780LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.950 98 60-140
1,1,1-Trichloroethane ug/L 48.350 97 60-140
1,1,2,2-Tetrachloroethane ug/L 46.250 92 60-140
1,1,2-Trichloroethane ug/L 46.950 94 60-140
1,1-Dichloroethane ug/L 45.950 92 60-140
1,1-Dichloroethene ug/L 47.150 94 60-140
1,1-Dichloropropene ug/L 47.850 96 60-140
1,2,3-Trichlorobenzene ug/L 48.450 97 60-140
1,2,3-Trichloropropane ug/L 48.450 97 60-140
1,2,4-Trichlorobenzene ug/L 47.650 95 60-140
1,2,4-Trimethylbenzene ug/L 46.950 94 60-140
1,2-Dibromo-3-chloropropane ug/L 49.650 99 60-140
1,2-Dibromoethane (EDB)ug/L 48.750 97 60-140
1,2-Dichlorobenzene ug/L 46.050 92 60-140
1,2-Dichloroethane ug/L 42.750 85 60-140
1,2-Dichloropropane ug/L 46.450 93 60-140
1,3,5-Trimethylbenzene ug/L 45.950 92 60-140
1,3-Dichlorobenzene ug/L 46.750 93 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1657780LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 46.850 94 60-140
1,4-Dichlorobenzene ug/L 46.750 93 60-140
2,2-Dichloropropane ug/L 43.150 86 60-140
2-Chlorotoluene ug/L 44.250 88 60-140
4-Chlorotoluene ug/L 45.150 90 60-140
Benzene ug/L 49.450 99 60-140
Bromobenzene ug/L 44.650 89 60-140
Bromochloromethane ug/L 47.150 94 60-140
Bromodichloromethane ug/L 47.850 96 60-140
Bromoform ug/L 51.450 103 60-140
Bromomethane ug/L 38.050 76 60-140
Carbon tetrachloride ug/L 49.550 99 60-140
Chlorobenzene ug/L 46.450 93 60-140
Chloroethane ug/L 47.950 96 60-140
Chloroform ug/L 45.550 91 60-140
Chloromethane ug/L 43.950 88 60-140
cis-1,2-Dichloroethene ug/L 45.250 90 60-140
cis-1,3-Dichloropropene ug/L 47.550 95 60-140
Dibromochloromethane ug/L 51.350 103 60-140
Dibromomethane ug/L 48.750 97 60-140
Dichlorodifluoromethane ug/L 42.350 85 60-140
Diisopropyl ether ug/L 47.350 95 60-140
Ethylbenzene ug/L 46.150 92 60-140
Hexachloro-1,3-butadiene ug/L 47.550 95 60-140
Isopropylbenzene (Cumene)ug/L 45.650 91 60-140
m&p-Xylene ug/L 91.2100 91 60-140
Methyl-tert-butyl ether ug/L 49.350 99 60-140
Methylene Chloride ug/L 43.550 87 60-140
n-Butylbenzene ug/L 45.750 91 60-140
n-Propylbenzene ug/L 44.750 89 60-140
Naphthalene ug/L 48.150 96 60-140
o-Xylene ug/L 45.650 91 60-140
sec-Butylbenzene ug/L 45.150 90 60-140
Styrene ug/L 48.050 96 60-140
tert-Butylbenzene ug/L 38.650 77 60-140
Tetrachloroethene ug/L 45.550 91 60-140
Toluene ug/L 46.850 94 60-140
trans-1,2-Dichloroethene ug/L 46.150 92 60-140
trans-1,3-Dichloropropene ug/L 46.450 93 60-140
Trichloroethene ug/L 46.450 93 60-140
Trichlorofluoromethane ug/L 46.350 93 60-140
Vinyl chloride ug/L 46.450 93 60-140
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1657781MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92284408009
1657782
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 108 60-140103 520ND21.7 20.6
1,1,1-Trichloroethane ug/L 20 103 60-140105 220ND20.6 21.0
1,1,2,2-Tetrachloroethane ug/L 20 104 60-140101 220ND20.7 20.3
1,1,2-Trichloroethane ug/L 20 100 60-140101 120ND20.1 20.2
1,1-Dichloroethane ug/L 20 100 60-140100 020ND20.0 20.0
1,1-Dichloroethene ug/L 20 100 60-140101 020ND20.1 20.1
1,1-Dichloropropene ug/L 20 105 60-140106 120ND21.0 21.2
1,2,3-Trichlorobenzene ug/L 20 112 60-140108 320ND22.4 21.7
1,2,3-Trichloropropane ug/L 20 111 60-140108 320ND22.2 21.5
1,2,4-Trichlorobenzene ug/L 20 110 60-140109 120ND21.9 21.7
1,2,4-Trimethylbenzene ug/L 20 109 60-140106 320ND21.9 21.2
1,2-Dibromo-3-chloropropane ug/L 20 107 60-140104 320ND21.5 20.9
1,2-Dibromoethane (EDB)ug/L 20 109 60-140106 320ND21.8 21.3
1,2-Dichlorobenzene ug/L 20 104 60-140103 120ND20.8 20.7
1,2-Dichloroethane ug/L 20 93 60-14094 020ND18.8 18.8
1,2-Dichloropropane ug/L 20 99 60-140100 1201.7 21.5 21.8
1,3,5-Trimethylbenzene ug/L 20 107 60-140105 220ND21.4 21.0
1,3-Dichlorobenzene ug/L 20 107 60-140106 220ND21.5 21.1
1,3-Dichloropropane ug/L 20 101 60-14098 320ND20.3 19.6
1,4-Dichlorobenzene ug/L 20 107 60-140103 420ND21.4 20.6
2,2-Dichloropropane ug/L 20 102 60-140104 220ND20.5 20.9
2-Chlorotoluene ug/L 20 104 60-140101 320ND20.8 20.2
4-Chlorotoluene ug/L 20 105 60-140102 420ND21.1 20.4
Benzene ug/L 20 107 60-140106 120ND21.3 21.2
Bromobenzene ug/L 20 103 60-14099 420ND20.5 19.8
Bromochloromethane ug/L 20 99 60-140102 320ND19.8 20.5
Bromodichloromethane ug/L 20 99 60-140100 120ND19.8 19.9
Bromoform ug/L 20 95 60-14093 220ND18.9 18.6
Bromomethane ug/L M1202760-14034 2420ND5.4 6.9
Carbon tetrachloride ug/L 20 104 60-140104 020ND20.7 20.8
Chlorobenzene ug/L 20 105 60-140101 320ND20.9 20.3
Chloroethane ug/L 20 94 60-14097 320ND18.9 19.4
Chloroform ug/L 20 100 60-140101 120ND20.0 20.2
Chloromethane ug/L M1205960-14060 120ND11.8 11.9
cis-1,2-Dichloroethene ug/L 20 98 60-14099 120ND19.5 19.7
cis-1,3-Dichloropropene ug/L 20 98 60-14099 120ND19.6 19.9
Dibromochloromethane ug/L 20 103 60-140103 020ND20.5 20.5
Dibromomethane ug/L 20 104 60-140102 220ND20.7 20.4
Dichlorodifluoromethane ug/L M1204160-14043 420ND8.2 8.5
Diisopropyl ether ug/L 20 101 60-140101 020ND20.1 20.2
Ethylbenzene ug/L 20 105 60-140102 320ND21.0 20.4
Hexachloro-1,3-butadiene ug/L 20 109 60-140107 220ND21.8 21.4
Isopropylbenzene (Cumene)ug/L 20 105 60-140100 520ND21.0 20.1
m&p-Xylene ug/L 40 104 60-140101 340ND41.5 40.4
Methyl-tert-butyl ether ug/L 20 104 60-140105 220ND20.7 21.1
Methylene Chloride ug/L 20 93 60-14093 020ND18.7 18.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1657781MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92284408009
1657782
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 109 60-140104 520ND21.7 20.8
n-Propylbenzene ug/L 20 106 60-140101 420ND21.1 20.3
Naphthalene ug/L 20 113 60-140110 320ND22.7 22.1
o-Xylene ug/L 20 102 60-14099 320ND20.4 19.8
sec-Butylbenzene ug/L 20 106 60-140104 120ND21.1 20.8
Styrene ug/L 20 107 60-140103 420ND21.4 20.5
tert-Butylbenzene ug/L 20 89 60-14087 320ND17.9 17.3
Tetrachloroethene ug/L 20 106 60-140101 420ND21.2 20.3
Toluene ug/L 20 102 60-140100 220ND20.4 20.0
trans-1,2-Dichloroethene ug/L 20 99 60-140102 220ND19.8 20.3
trans-1,3-Dichloropropene ug/L 20 99 60-14096 320ND19.7 19.1
Trichloroethene ug/L 20 101 60-140101 120ND20.2 20.1
Trichlorofluoromethane ug/L 20 97 60-14097 020ND19.4 19.4
Vinyl chloride ug/L 20 79 60-14080 120ND15.8 16.0
1,2-Dichloroethane-d4 (S)%97 70-130100
4-Bromofluorobenzene (S)%101 70-130101
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
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Huntersville, NC 28078
[phone]
Page 31 of 35
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
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Huntersville, NC 28078
[phone]
Page 32 of 35
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92284408001 MSV/35395MW-7 SM 6200B
92284408002 MSV/35395MW-8 SM 6200B
92284408003 MSV/35395MW-3 SM 6200B
92284408004 MSV/35397MW-5 SM 6200B
92284408005 MSV/35397MW-9 SM 6200B
92284408006 MSV/35397MW-10 SM 6200B
92284408007 MSV/35397WSW-2 SM 6200B
92284408008 MSV/35397WSW-4 SM 6200B
92284408009 MSV/35397WSW-5 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 35
Page 34 of 35
Page 35 of 35