FA-916_17217_CA_LAB_20191016_WSW 5 Robertson

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
October 16, 2019
Matt Gillis
ECS Southeast - Raleigh, NC
9001 Glenwood Avenue
Raleigh, NC 27617
Project Location: Clayton, NC
Client Job Number:
Project Number: 1226-D
Laboratory Work Order Number: 19J0800
Enclosed are results of analyses for samples received by the laboratory on October 10, 2019. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 18
Table of Contents
Table of Contents
Sample Summary 3
Hits Only Report 4
Case Narrative 5
Sample Results 6
19J0800-01 6
Sample Preparation Information 8
QC Data 9
Volatile Organic Compounds by GC/MS 9
B243099 9
Flag/Qualifier Summary 13
Certifications 14
Chain of Custody/Sample Receipt 16
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
10/16/2019
ECS Southeast - Raleigh, NC
9001 Glenwood Avenue
Raleigh, NC 27617
ATTN: Matt Gillis
1226-D
19J0800
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Clayton, NC
WSW-5 19J0800-01 Ground Water SM21-22 6200B
[TOC_1]Sample Summary[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19J0800-01WSW-5
DL
1,2-Dichloropropane 2.0 0.50 g/L SM21-22 6200B0.20
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
[TOC_1]Case Narrative[TOC]
SM21-22 6200B
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
1,2,3-Trichlorobenzene
19J0800-01[WSW-5], B243099-BLK1, B243099-BS1, B243099-BSD1, S041450-CCV1
Dichlorodifluoromethane (Freon 12)
19J0800-01[WSW-5], B243099-BLK1, B243099-BS1, B243099-BSD1, S041450-CCV1
Naphthalene
19J0800-01[WSW-5], B243099-BLK1, B243099-BS1, B243099-BSD1, S041450-CCV1
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/10/2019
Work Order: 19J0800Sample Description:Project Location: Clayton, NC
Sample ID: 19J0800-01
Field Sample #: WSW-5
Sample Matrix: Ground Water
Sampled: 10/10/2019 13:14
[TOC_2]19J0800-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 10/15/19 2:41 EEHg/L3.8 10/14/19SM21-22 6200B1Acetone
ND 0.50 10/15/19 2:41 EEHg/L0.18 10/14/19SM21-22 6200B1Benzene
ND 0.50 10/15/19 2:41 EEHg/L0.15 10/14/19SM21-22 6200B1Bromobenzene
ND 0.50 10/15/19 2:41 EEHg/L0.32 10/14/19SM21-22 6200B1Bromochloromethane
ND 0.50 10/15/19 2:41 EEHg/L0.16 10/14/19SM21-22 6200B1Bromodichloromethane
ND 0.50 10/15/19 2:41 EEHg/L0.46 10/14/19SM21-22 6200B1Bromoform
ND 2.0 10/15/19 2:41 EEHg/L0.78 10/14/19SM21-22 6200B1Bromomethane
ND 5.0 10/15/19 2:41 EEHg/L1.9 10/14/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 10/15/19 2:41 EEHg/L0.21 10/14/19SM21-22 6200B1n-Butylbenzene
ND 0.50 10/15/19 2:41 EEHg/L0.16 10/14/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 10/15/19 2:41 EEHg/L0.17 10/14/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 10/15/19 2:41 EEHg/L0.11 10/14/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 10/15/19 2:41 EEHg/L0.15 10/14/19SM21-22 6200B1Chlorobenzene
ND 0.50 10/15/19 2:41 EEHg/L0.21 10/14/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 10/15/19 2:41 EEHg/L0.35 10/14/19SM21-22 6200B1Chloroethane
ND 0.50 10/15/19 2:41 EEHg/L0.17 10/14/19SM21-22 6200B1Chloroform
ND 1.0 10/15/19 2:41 EEHg/L0.45 10/14/19SM21-22 6200B1Chloromethane
ND 0.50 10/15/19 2:41 EEHg/L0.12 10/14/19SM21-22 6200B12-Chlorotoluene
ND 0.50 10/15/19 2:41 EEHg/L0.14 10/14/19SM21-22 6200B14-Chlorotoluene
ND 0.50 10/15/19 2:41 EEHg/L0.19 10/14/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 10/15/19 2:41 EEHg/L0.16 10/14/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 10/15/19 2:41 EEHg/L0.12 10/14/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 10/15/19 2:41 EEHg/L0.13 10/14/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 10/15/19 2:41 EEHg/L0.26 10/14/19SM21-22 6200B1L-04Dichlorodifluoromethane (Freon 12)
ND 0.50 10/15/19 2:41 EEHg/L0.16 10/14/19SM21-22 6200B11,1-Dichloroethane
ND 0.50 10/15/19 2:41 EEHg/L0.41 10/14/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 10/15/19 2:41 EEHg/L0.32 10/14/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 10/15/19 2:41 EEHg/L0.13 10/14/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 10/15/19 2:41 EEHg/L0.31 10/14/19SM21-22 6200B1trans-1,2-Dichloroethylene
2.0 0.50 10/15/19 2:41 EEHg/L0.20 10/14/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 10/15/19 2:41 EEHg/L0.11 10/14/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 10/15/19 2:41 EEHg/L0.20 10/14/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 10/15/19 2:41 EEHg/L0.16 10/14/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 10/15/19 2:41 EEHg/L0.13 10/14/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 10/15/19 2:41 EEHg/L0.23 10/14/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 10/15/19 2:41 EEHg/L0.17 10/14/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 10/15/19 2:41 EEHg/L0.13 10/14/19SM21-22 6200B1Ethylbenzene
ND 5.0 10/15/19 2:41 EEHg/L1.5 10/14/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 10/15/19 2:41 EEHg/L0.17 10/14/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 10/15/19 2:41 EEHg/L0.20 10/14/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 10/15/19 2:41 EEHg/L0.25 10/14/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 10/15/19 2:41 EEHg/L0.34 10/14/19SM21-22 6200B1Methylene Chloride
ND 5.0 10/15/19 2:41 EEHg/L1.7 10/14/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
ND 0.50 10/15/19 2:41 EEHg/L0.31 10/14/19SM21-22 6200B1L-04Naphthalene
[TOC_1]Sample Results[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 10/10/2019
Work Order: 19J0800Sample Description:Project Location: Clayton, NC
Sample ID: 19J0800-01
Field Sample #: WSW-5
Sample Matrix: Ground Water
Sampled: 10/10/2019 13:14
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 10/15/19 2:41 EEHg/L0.13 10/14/19SM21-22 6200B1n-Propylbenzene
ND 0.50 10/15/19 2:41 EEHg/L0.11 10/14/19SM21-22 6200B1Styrene
ND 0.50 10/15/19 2:41 EEHg/L0.22 10/14/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 10/15/19 2:41 EEHg/L0.18 10/14/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 10/15/19 2:41 EEHg/L0.14 10/14/19SM21-22 6200B1Toluene
ND 1.0 10/15/19 2:41 EEHg/L0.57 10/14/19SM21-22 6200B1L-041,2,3-Trichlorobenzene
ND 0.50 10/15/19 2:41 EEHg/L0.40 10/14/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 10/15/19 2:41 EEHg/L0.20 10/14/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 10/15/19 2:41 EEHg/L0.16 10/14/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 10/15/19 2:41 EEHg/L0.24 10/14/19SM21-22 6200B1Trichloroethylene
ND 0.50 10/15/19 2:41 EEHg/L0.33 10/14/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 10/15/19 2:41 EEHg/L0.25 10/14/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 10/15/19 2:41 EEHg/L0.18 10/14/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 10/15/19 2:41 EEHg/L0.14 10/14/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 10/15/19 2:41 EEHg/L10 10/14/19SM21-22 6200B1Vinyl Acetate
ND 0.50 10/15/19 2:41 EEHg/L0.45 10/14/19SM21-22 6200B1Vinyl Chloride
ND 1.0 10/15/19 2:41 EEHg/L0.30 10/14/19SM21-22 6200B1m+p Xylene
ND 0.50 10/15/19 2:41 EEHg/L0.17 10/14/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 104 10/15/19 2:4170-130
Toluene-d8 98.3 10/15/19 2:4170-130
4-Bromofluorobenzene 95.8 10/15/19 2:4170-130
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B243099 10/14/195 5.0019J0800-01 [WSW-5]
[TOC_1]Sample Preparation Information[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B243099 - SW-846 5030B
[TOC_3]B243099[TOC]
Blank (B243099-BLK1) Prepared & Analyzed: 10/14/19
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50 L-04ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50 L-04ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0 L-04ND
1,2,4-Trichlorobenzene g/L0.50ND
1,1,1-Trichloroethane g/L0.50ND
[TOC_1]QC Data[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B243099 - SW-846 5030B
Blank (B243099-BLK1) Prepared & Analyzed: 10/14/19
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10526.2
g/L 25.0 70-130Surrogate: Toluene-d8 97.424.4
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 94.323.6
LCS (B243099-BS1) Prepared & Analyzed: 10/14/19
Acetone g/L50 100 70-130101101
Benzene g/L0.50 10.0 70-13010310.3
Bromobenzene g/L0.50 10.0 70-13093.39.33
Bromochloromethane g/L0.50 10.0 70-13011011.0
Bromodichloromethane g/L0.50 10.0 70-13010110.1
Bromoform g/L0.50 10.0 70-13091.99.19
Bromomethane g/L1.0 10.0 60-14011811.8
2-Butanone (MEK)g/L5.0 100 70-130101101
n-Butylbenzene g/L0.50 10.0 70-13092.39.23
sec-Butylbenzene g/L0.50 10.0 70-13010210.2
tert-Butylbenzene g/L0.50 10.0 70-13010010.0
Carbon Tetrachloride g/L0.50 10.0 70-13098.59.85
Chlorobenzene g/L0.50 10.0 70-13010310.3
Chlorodibromomethane g/L0.50 10.0 70-13096.89.68
Chloroethane g/L0.50 10.0 60-14089.48.94
Chloroform g/L0.50 10.0 70-13010910.9
Chloromethane g/L0.60 10.0 60-14010310.3
2-Chlorotoluene g/L0.50 10.0 70-13098.49.84
4-Chlorotoluene g/L0.50 10.0 70-13095.89.58
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13098.99.89
1,2-Dichlorobenzene g/L0.50 10.0 70-13010510.5
1,3-Dichlorobenzene g/L0.50 10.0 70-13010610.6
1,4-Dichlorobenzene g/L0.50 10.0 70-13010210.2
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 L-0460-14051.6 *5.16
1,1-Dichloroethane g/L0.50 10.0 70-13010410.4
1,2-Dichloroethane g/L0.50 10.0 70-13099.49.94
1,1-Dichloroethylene g/L0.50 10.0 70-13099.89.98
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13010510.5
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13096.69.66
1,2-Dichloropropane g/L0.50 10.0 70-13010610.6
1,3-Dichloropropane g/L0.50 10.0 70-13010310.3
2,2-Dichloropropane g/L0.50 10.0 70-13086.98.69
1,1-Dichloropropene g/L0.50 10.0 70-13010410.4
cis-1,3-Dichloropropene g/L0.50 10.0 70-13098.19.81
trans-1,3-Dichloropropene g/L0.50 10.0 70-13091.09.10
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13010310.3
Ethylbenzene g/L0.50 10.0 70-13097.39.73
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B243099 - SW-846 5030B
LCS (B243099-BS1) Prepared & Analyzed: 10/14/19
2-Hexanone (MBK)g/L5.0 100 70-13091.191.1
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13095.59.55
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13094.09.40
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13093.59.35
Methylene Chloride g/L5.0 10.0 70-13010910.9
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-13093.993.9
Naphthalene g/L0.50 10.0 L-0470-13069.6 *6.96
n-Propylbenzene g/L0.50 10.0 70-13092.79.27
Styrene g/L0.50 10.0 70-13094.59.45
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13010710.7
Tetrachloroethylene g/L0.50 10.0 70-13097.99.79
Toluene g/L0.50 10.0 70-13099.99.99
1,2,3-Trichlorobenzene g/L1.0 10.0 L-0470-13066.5 *6.65
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13073.67.36
1,1,1-Trichloroethane g/L0.50 10.0 70-13010510.5
1,1,2-Trichloroethane g/L0.50 10.0 70-13010610.6
Trichloroethylene g/L0.50 10.0 70-13098.69.86
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13097.39.73
1,2,3-Trichloropropane g/L0.50 10.0 70-13097.69.76
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13099.79.97
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13088.78.87
Vinyl Acetate g/L20 100 70-13099.999.9
Vinyl Chloride g/L0.50 10.0 60-14083.68.36
m+p Xylene g/L1.0 20.0 70-13096.019.2
o-Xylene g/L0.50 10.0 70-13097.69.76
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10426.0
g/L 25.0 70-130Surrogate: Toluene-d8 10025.0
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 96.824.2
LCS Dup (B243099-BSD1) Prepared & Analyzed: 10/14/19
Acetone g/L50 100 2570-13094.7 6.3494.7
Benzene g/L0.50 10.0 2570-13098.7 4.079.87
Bromobenzene g/L0.50 10.0 2570-13092.7 0.6459.27
Bromochloromethane g/L0.50 10.0 2570-130107 2.7810.7
Bromodichloromethane g/L0.50 10.0 2570-130101 0.39510.1
Bromoform g/L0.50 10.0 2570-13091.5 0.4369.15
Bromomethane g/L1.0 10.0 2560-140113 3.9011.3
2-Butanone (MEK)g/L5.0 100 2570-13096.5 4.7396.5
n-Butylbenzene g/L0.50 10.0 2570-13088.4 4.328.84
sec-Butylbenzene g/L0.50 10.0 2570-13096.8 5.439.68
tert-Butylbenzene g/L0.50 10.0 2570-13096.7 3.659.67
Carbon Tetrachloride g/L0.50 10.0 2570-13093.3 5.429.33
Chlorobenzene g/L0.50 10.0 2570-13099.8 3.169.98
Chlorodibromomethane g/L0.50 10.0 2570-13095.5 1.359.55
Chloroethane g/L0.50 10.0 2560-14092.9 3.849.29
Chloroform g/L0.50 10.0 2570-130104 5.1610.4
Chloromethane g/L0.60 10.0 2560-14092.8 10.19.28
2-Chlorotoluene g/L0.50 10.0 2570-13094.1 4.479.41
4-Chlorotoluene g/L0.50 10.0 2570-13092.2 3.839.22
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130101 2.1010.1
1,2-Dichlorobenzene g/L0.50 10.0 2570-130103 2.3110.3
1,3-Dichlorobenzene g/L0.50 10.0 2570-130103 3.2610.3
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B243099 - SW-846 5030B
LCS Dup (B243099-BSD1) Prepared & Analyzed: 10/14/19
1,4-Dichlorobenzene g/L0.50 10.0 2570-13099.5 2.879.95
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 25 L-0460-14046.7 9.97*4.67
1,1-Dichloroethane g/L0.50 10.0 2570-130100 3.8310.0
1,2-Dichloroethane g/L0.50 10.0 2570-13098.4 1.019.84
1,1-Dichloroethylene g/L0.50 10.0 2570-13094.9 5.039.49
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13098.8 6.469.88
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13090.7 6.309.07
1,2-Dichloropropane g/L0.50 10.0 2570-13099.9 5.939.99
1,3-Dichloropropane g/L0.50 10.0 2570-13098.5 4.179.85
2,2-Dichloropropane g/L0.50 10.0 2570-13080.5 7.658.05
1,1-Dichloropropene g/L0.50 10.0 2570-13098.2 5.549.82
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13095.7 2.489.57
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13090.1 0.9949.01
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-13098.4 4.579.84
Ethylbenzene g/L0.50 10.0 2570-13093.8 3.669.38
2-Hexanone (MBK)g/L5.0 100 2570-13090.0 1.2890.0
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-13093.2 2.449.32
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-13090.6 3.689.06
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13089.8 4.048.98
Methylene Chloride g/L5.0 10.0 2570-130104 4.2210.4
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-13090.9 3.2790.9
Naphthalene g/L0.50 10.0 25 L-0470-13066.3 4.86*6.63
n-Propylbenzene g/L0.50 10.0 2570-13091.3 1.529.13
Styrene g/L0.50 10.0 2570-13092.5 2.149.25
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130106 1.1310.6
Tetrachloroethylene g/L0.50 10.0 2570-13094.1 3.969.41
Toluene g/L0.50 10.0 2570-13095.4 4.619.54
1,2,3-Trichlorobenzene g/L1.0 10.0 25 L-0470-13063.8 4.14*6.38
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-13072.2 1.927.22
1,1,1-Trichloroethane g/L0.50 10.0 2570-13097.4 7.229.74
1,1,2-Trichloroethane g/L0.50 10.0 2570-130104 1.9010.4
Trichloroethylene g/L0.50 10.0 2570-13095.4 3.309.54
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13088.9 9.028.89
1,2,3-Trichloropropane g/L0.50 10.0 2570-13092.3 5.589.23
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-13097.9 1.829.79
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-13086.9 2.058.69
Vinyl Acetate g/L20 100 2570-13096.1 3.8696.1
Vinyl Chloride g/L0.50 10.0 2560-14078.0 6.937.80
m+p Xylene g/L1.0 20.0 2570-13094.0 2.1618.8
o-Xylene g/L0.50 10.0 2570-13094.5 3.239.45
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10225.5
g/L 25.0 70-130Surrogate: Toluene-d8 10025.1
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 93.823.5
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*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
FLAG/QUALIFIER SUMMARY
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
[TOC_1]Flag/Qualifier Summary[TOC]
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
NC1,1,2,2-Tetrachloroethane
[TOC_1]Certifications[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2020
M-MA100Massachusetts DEPMA 06/30/2020
PH-0567Connecticut Department of Publilc HealthCT 09/30/2021
10899 NELAPNew York State Department of HealthNY 04/1/2020
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2020
LAO00112Rhode Island Department of HealthRI 12/30/2019
652North Carolina Div. of Water QualityNC 12/31/2019
MA007 NELAPNew Jersey DEPNJ 06/30/2020
E871027 NELAPFlorida Department of HealthFL 06/30/2020
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2020
2011028State of MaineME 06/9/2021
460217Commonwealth of VirginiaVA 12/14/2019
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2020
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2020
25703North Carolina Department of HealthNC-DW 07/31/2020
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2020
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