FA-916_17217_CA_LAB_20160202_Pace Labs Analytical Report for Sampling Event 1-26-2016

#=CL#
February 02, 2016
LIMS USE: FR - MATTHEW GILLIS
LIMS OBJECT ID: 92284408
92284408
Project:
Pace Project No.:
RE:
Matthew Gillis
ECS
9001 Glenwood Avenue
Raleigh, NC 27617
FLOWERS STORE PROPERTY
Dear Matthew Gillis:
Enclosed are the analytical results for sample(s) received by the laboratory on January 27, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
Enclosures
cc:Brian Smith, ECS Carolinas LLP
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 35
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 35
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92284408005 MW-9
sec-Butylbenzene 1.3 ug/L 02/02/16 03:010.50SM 6200B
1,4-Dichlorobenzene 0.51 ug/L 02/02/16 03:010.50SM 6200B
Isopropylbenzene (Cumene)0.97 ug/L 02/02/16 03:010.50SM 6200B
Naphthalene 18.4 ug/L 02/02/16 03:012.0SM 6200B
n-Propylbenzene 2.0 ug/L 02/02/16 03:010.50SM 6200B
1,2,4-Trimethylbenzene 8.5 ug/L 02/02/16 03:010.50SM 6200B
1,3,5-Trimethylbenzene 16.3 ug/L 02/02/16 03:010.50SM 6200B
o-Xylene 1.2 ug/L 02/02/16 03:010.50SM 6200B
92284408007 WSW-2
Bromodichloromethane 5.4 ug/L 02/02/16 03:350.50SM 6200B
Chloroform 11.8 ug/L 02/02/16 03:350.50SM 6200B
Dibromochloromethane 1.3 ug/L 02/02/16 03:350.50SM 6200B
92284408008 WSW-4
Bromodichloromethane 6.0 ug/L 02/02/16 03:520.50SM 6200B
Chloroform 13.3 ug/L 02/02/16 03:520.50SM 6200B
Dibromochloromethane 1.3 ug/L 02/02/16 03:520.50SM 6200B
92284408009 WSW-5
1,2-Dichloropropane 1.7 ug/L 02/02/16 04:090.50SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-7 Lab ID:92284408001 Collected:01/26/16 11:48 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 02/01/16 17:42 71-43-20.50 1
Bromobenzene ND ug/L 02/01/16 17:42 108-86-10.50 1
Bromochloromethane ND ug/L 02/01/16 17:42 74-97-50.50 1
Bromodichloromethane ND ug/L 02/01/16 17:42 75-27-40.50 1
Bromoform ND ug/L 02/01/16 17:42 75-25-20.50 1
Bromomethane ND ug/L 02/01/16 17:42 74-83-95.0 1
n-Butylbenzene ND ug/L 02/01/16 17:42 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/01/16 17:42 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/01/16 17:42 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/01/16 17:42 56-23-50.50 1
Chlorobenzene ND ug/L 02/01/16 17:42 108-90-70.50 1
Chloroethane ND ug/L 02/01/16 17:42 75-00-31.0 1
Chloroform ND ug/L 02/01/16 17:42 67-66-30.50 1
Chloromethane ND ug/L 02/01/16 17:42 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/01/16 17:42 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/01/16 17:42 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/01/16 17:42 96-12-81.0 1
Dibromochloromethane ND ug/L 02/01/16 17:42 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/01/16 17:42 106-93-40.50 1
Dibromomethane ND ug/L 02/01/16 17:42 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/01/16 17:42 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/01/16 17:42 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/01/16 17:42 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/01/16 17:42 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/01/16 17:42 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/01/16 17:42 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/01/16 17:42 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/01/16 17:42 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/01/16 17:42 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/01/16 17:42 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/01/16 17:42 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/01/16 17:42 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/01/16 17:42 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/01/16 17:42 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/01/16 17:42 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/01/16 17:42 108-20-30.50 1
Ethylbenzene ND ug/L 02/01/16 17:42 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/01/16 17:42 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/01/16 17:42 98-82-80.50 1
Methylene Chloride ND ug/L 02/01/16 17:42 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/01/16 17:42 1634-04-40.50 1
Naphthalene ND ug/L 02/01/16 17:42 91-20-32.0 1
n-Propylbenzene ND ug/L 02/01/16 17:42 103-65-10.50 1
Styrene ND ug/L 02/01/16 17:42 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/01/16 17:42 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/01/16 17:42 79-34-50.50 1
Tetrachloroethene ND ug/L 02/01/16 17:42 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 35
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ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-7 Lab ID:92284408001 Collected:01/26/16 11:48 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 02/01/16 17:42 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/01/16 17:42 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/01/16 17:42 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/01/16 17:42 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/01/16 17:42 79-00-50.50 1
Trichloroethene ND ug/L 02/01/16 17:42 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/01/16 17:42 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/01/16 17:42 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/01/16 17:42 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/01/16 17:42 108-67-80.50 1
Vinyl chloride ND ug/L 02/01/16 17:42 75-01-41.0 1
m&p-Xylene ND ug/L 02/01/16 17:42 179601-23-11.0 1
o-Xylene ND ug/L 02/01/16 17:42 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)105 %02/01/16 17:42 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %02/01/16 17:42 460-00-470-130 1
Toluene-d8 (S)101 %02/01/16 17:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-8 Lab ID:92284408002 Collected:01/26/16 12:15 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 02/01/16 17:59 71-43-20.50 1
Bromobenzene ND ug/L 02/01/16 17:59 108-86-10.50 1
Bromochloromethane ND ug/L 02/01/16 17:59 74-97-50.50 1
Bromodichloromethane ND ug/L 02/01/16 17:59 75-27-40.50 1
Bromoform ND ug/L 02/01/16 17:59 75-25-20.50 1
Bromomethane ND ug/L 02/01/16 17:59 74-83-95.0 1
n-Butylbenzene ND ug/L 02/01/16 17:59 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/01/16 17:59 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/01/16 17:59 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/01/16 17:59 56-23-50.50 1
Chlorobenzene ND ug/L 02/01/16 17:59 108-90-70.50 1
Chloroethane ND ug/L 02/01/16 17:59 75-00-31.0 1
Chloroform ND ug/L 02/01/16 17:59 67-66-30.50 1
Chloromethane ND ug/L 02/01/16 17:59 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/01/16 17:59 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/01/16 17:59 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/01/16 17:59 96-12-81.0 1
Dibromochloromethane ND ug/L 02/01/16 17:59 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/01/16 17:59 106-93-40.50 1
Dibromomethane ND ug/L 02/01/16 17:59 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/01/16 17:59 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/01/16 17:59 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/01/16 17:59 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/01/16 17:59 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/01/16 17:59 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/01/16 17:59 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/01/16 17:59 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/01/16 17:59 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/01/16 17:59 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/01/16 17:59 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/01/16 17:59 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/01/16 17:59 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/01/16 17:59 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/01/16 17:59 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/01/16 17:59 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/01/16 17:59 108-20-30.50 1
Ethylbenzene ND ug/L 02/01/16 17:59 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/01/16 17:59 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/01/16 17:59 98-82-80.50 1
Methylene Chloride ND ug/L 02/01/16 17:59 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/01/16 17:59 1634-04-40.50 1
Naphthalene ND ug/L 02/01/16 17:59 91-20-32.0 1
n-Propylbenzene ND ug/L 02/01/16 17:59 103-65-10.50 1
Styrene ND ug/L 02/01/16 17:59 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/01/16 17:59 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/01/16 17:59 79-34-50.50 1
Tetrachloroethene ND ug/L 02/01/16 17:59 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-8 Lab ID:92284408002 Collected:01/26/16 12:15 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 02/01/16 17:59 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/01/16 17:59 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/01/16 17:59 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/01/16 17:59 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/01/16 17:59 79-00-50.50 1
Trichloroethene ND ug/L 02/01/16 17:59 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/01/16 17:59 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/01/16 17:59 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/01/16 17:59 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/01/16 17:59 108-67-80.50 1
Vinyl chloride ND ug/L 02/01/16 17:59 75-01-41.0 1
m&p-Xylene ND ug/L 02/01/16 17:59 179601-23-11.0 1
o-Xylene ND ug/L 02/01/16 17:59 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)104 %02/01/16 17:59 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %02/01/16 17:59 460-00-470-130 1
Toluene-d8 (S)101 %02/01/16 17:59 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-3 Lab ID:92284408003 Collected:01/26/16 12:41 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 02/01/16 18:16 71-43-20.50 1
Bromobenzene ND ug/L 02/01/16 18:16 108-86-10.50 1
Bromochloromethane ND ug/L 02/01/16 18:16 74-97-50.50 1
Bromodichloromethane ND ug/L 02/01/16 18:16 75-27-40.50 1
Bromoform ND ug/L 02/01/16 18:16 75-25-20.50 1
Bromomethane ND ug/L 02/01/16 18:16 74-83-95.0 1
n-Butylbenzene ND ug/L 02/01/16 18:16 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/01/16 18:16 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/01/16 18:16 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/01/16 18:16 56-23-50.50 1
Chlorobenzene ND ug/L 02/01/16 18:16 108-90-70.50 1
Chloroethane ND ug/L 02/01/16 18:16 75-00-31.0 1
Chloroform ND ug/L 02/01/16 18:16 67-66-30.50 1
Chloromethane ND ug/L 02/01/16 18:16 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/01/16 18:16 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/01/16 18:16 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/01/16 18:16 96-12-81.0 1
Dibromochloromethane ND ug/L 02/01/16 18:16 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/01/16 18:16 106-93-40.50 1
Dibromomethane ND ug/L 02/01/16 18:16 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/01/16 18:16 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/01/16 18:16 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/01/16 18:16 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/01/16 18:16 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/01/16 18:16 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/01/16 18:16 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/01/16 18:16 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/01/16 18:16 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/01/16 18:16 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/01/16 18:16 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/01/16 18:16 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/01/16 18:16 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/01/16 18:16 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/01/16 18:16 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/01/16 18:16 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/01/16 18:16 108-20-30.50 1
Ethylbenzene ND ug/L 02/01/16 18:16 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/01/16 18:16 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/01/16 18:16 98-82-80.50 1
Methylene Chloride ND ug/L 02/01/16 18:16 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/01/16 18:16 1634-04-40.50 1
Naphthalene ND ug/L 02/01/16 18:16 91-20-32.0 1
n-Propylbenzene ND ug/L 02/01/16 18:16 103-65-10.50 1
Styrene ND ug/L 02/01/16 18:16 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/01/16 18:16 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/01/16 18:16 79-34-50.50 1
Tetrachloroethene ND ug/L 02/01/16 18:16 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-3 Lab ID:92284408003 Collected:01/26/16 12:41 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 02/01/16 18:16 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/01/16 18:16 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/01/16 18:16 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/01/16 18:16 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/01/16 18:16 79-00-50.50 1
Trichloroethene ND ug/L 02/01/16 18:16 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/01/16 18:16 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/01/16 18:16 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/01/16 18:16 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/01/16 18:16 108-67-80.50 1
Vinyl chloride ND ug/L 02/01/16 18:16 75-01-41.0 1
m&p-Xylene ND ug/L 02/01/16 18:16 179601-23-11.0 1
o-Xylene ND ug/L 02/01/16 18:16 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %02/01/16 18:16 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %02/01/16 18:16 460-00-470-130 1
Toluene-d8 (S)100 %02/01/16 18:16 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-5 Lab ID:92284408004 Collected:01/26/16 13:08 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 02/02/16 02:44 71-43-20.50 1
Bromobenzene ND ug/L 02/02/16 02:44 108-86-10.50 1
Bromochloromethane ND ug/L 02/02/16 02:44 74-97-50.50 1
Bromodichloromethane ND ug/L 02/02/16 02:44 75-27-40.50 1
Bromoform ND ug/L 02/02/16 02:44 75-25-20.50 1
Bromomethane ND ug/L 02/02/16 02:44 74-83-95.0 1
n-Butylbenzene ND ug/L 02/02/16 02:44 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/02/16 02:44 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/02/16 02:44 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/02/16 02:44 56-23-50.50 1
Chlorobenzene ND ug/L 02/02/16 02:44 108-90-70.50 1
Chloroethane ND ug/L 02/02/16 02:44 75-00-31.0 1
Chloroform ND ug/L 02/02/16 02:44 67-66-30.50 1
Chloromethane ND ug/L 02/02/16 02:44 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/02/16 02:44 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/02/16 02:44 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/02/16 02:44 96-12-81.0 1
Dibromochloromethane ND ug/L 02/02/16 02:44 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/02/16 02:44 106-93-40.50 1
Dibromomethane ND ug/L 02/02/16 02:44 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/02/16 02:44 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/02/16 02:44 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/02/16 02:44 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/02/16 02:44 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/02/16 02:44 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/02/16 02:44 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/02/16 02:44 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/02/16 02:44 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/02/16 02:44 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/02/16 02:44 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/02/16 02:44 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/02/16 02:44 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/02/16 02:44 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/02/16 02:44 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/02/16 02:44 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/02/16 02:44 108-20-30.50 1
Ethylbenzene ND ug/L 02/02/16 02:44 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/02/16 02:44 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/02/16 02:44 98-82-80.50 1
Methylene Chloride ND ug/L 02/02/16 02:44 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/02/16 02:44 1634-04-40.50 1
Naphthalene ND ug/L 02/02/16 02:44 91-20-32.0 1
n-Propylbenzene ND ug/L 02/02/16 02:44 103-65-10.50 1
Styrene ND ug/L 02/02/16 02:44 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/02/16 02:44 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/02/16 02:44 79-34-50.50 1
Tetrachloroethene ND ug/L 02/02/16 02:44 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-5 Lab ID:92284408004 Collected:01/26/16 13:08 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 02/02/16 02:44 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/02/16 02:44 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/02/16 02:44 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/02/16 02:44 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/02/16 02:44 79-00-50.50 1
Trichloroethene ND ug/L 02/02/16 02:44 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/02/16 02:44 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/02/16 02:44 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/02/16 02:44 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/02/16 02:44 108-67-80.50 1
Vinyl chloride ND ug/L 02/02/16 02:44 75-01-41.0 1
m&p-Xylene ND ug/L 02/02/16 02:44 179601-23-11.0 1
o-Xylene ND ug/L 02/02/16 02:44 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %02/02/16 02:44 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %02/02/16 02:44 460-00-470-130 1
Toluene-d8 (S)99 %02/02/16 02:44 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-9 Lab ID:92284408005 Collected:01/26/16 13:34 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 02/02/16 03:01 71-43-20.50 1
Bromobenzene ND ug/L 02/02/16 03:01 108-86-10.50 1
Bromochloromethane ND ug/L 02/02/16 03:01 74-97-50.50 1
Bromodichloromethane ND ug/L 02/02/16 03:01 75-27-40.50 1
Bromoform ND ug/L 02/02/16 03:01 75-25-20.50 1
Bromomethane ND ug/L 02/02/16 03:01 74-83-95.0 1
n-Butylbenzene ND ug/L 02/02/16 03:01 104-51-80.50 1
sec-Butylbenzene 1.3 ug/L 02/02/16 03:01 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/02/16 03:01 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/02/16 03:01 56-23-50.50 1
Chlorobenzene ND ug/L 02/02/16 03:01 108-90-70.50 1
Chloroethane ND ug/L 02/02/16 03:01 75-00-31.0 1
Chloroform ND ug/L 02/02/16 03:01 67-66-30.50 1
Chloromethane ND ug/L 02/02/16 03:01 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/02/16 03:01 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/02/16 03:01 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/02/16 03:01 96-12-81.0 1
Dibromochloromethane ND ug/L 02/02/16 03:01 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/02/16 03:01 106-93-40.50 1
Dibromomethane ND ug/L 02/02/16 03:01 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/02/16 03:01 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/02/16 03:01 541-73-10.50 1
1,4-Dichlorobenzene 0.51 ug/L 02/02/16 03:01 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/02/16 03:01 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/02/16 03:01 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/02/16 03:01 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/02/16 03:01 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/02/16 03:01 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/02/16 03:01 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/02/16 03:01 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/02/16 03:01 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/02/16 03:01 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/02/16 03:01 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/02/16 03:01 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/02/16 03:01 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/02/16 03:01 108-20-30.50 1
Ethylbenzene ND ug/L 02/02/16 03:01 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/02/16 03:01 87-68-32.0 1
Isopropylbenzene (Cumene)0.97 ug/L 02/02/16 03:01 98-82-80.50 1
Methylene Chloride ND ug/L 02/02/16 03:01 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/02/16 03:01 1634-04-40.50 1
Naphthalene 18.4 ug/L 02/02/16 03:01 91-20-32.0 1
n-Propylbenzene 2.0 ug/L 02/02/16 03:01 103-65-10.50 1
Styrene ND ug/L 02/02/16 03:01 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/02/16 03:01 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/02/16 03:01 79-34-50.50 1
Tetrachloroethene ND ug/L 02/02/16 03:01 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-9 Lab ID:92284408005 Collected:01/26/16 13:34 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 02/02/16 03:01 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/02/16 03:01 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/02/16 03:01 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/02/16 03:01 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/02/16 03:01 79-00-50.50 1
Trichloroethene ND ug/L 02/02/16 03:01 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/02/16 03:01 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/02/16 03:01 96-18-40.50 1
1,2,4-Trimethylbenzene 8.5 ug/L 02/02/16 03:01 95-63-60.50 1
1,3,5-Trimethylbenzene 16.3 ug/L 02/02/16 03:01 108-67-80.50 1
Vinyl chloride ND ug/L 02/02/16 03:01 75-01-41.0 1
m&p-Xylene ND ug/L 02/02/16 03:01 179601-23-11.0 1
o-Xylene 1.2 ug/L 02/02/16 03:01 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %02/02/16 03:01 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %02/02/16 03:01 460-00-470-130 1
Toluene-d8 (S)101 %02/02/16 03:01 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-10 Lab ID:92284408006 Collected:01/26/16 11:08 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 02/02/16 03:18 71-43-20.50 1
Bromobenzene ND ug/L 02/02/16 03:18 108-86-10.50 1
Bromochloromethane ND ug/L 02/02/16 03:18 74-97-50.50 1
Bromodichloromethane ND ug/L 02/02/16 03:18 75-27-40.50 1
Bromoform ND ug/L 02/02/16 03:18 75-25-20.50 1
Bromomethane ND ug/L 02/02/16 03:18 74-83-95.0 1
n-Butylbenzene ND ug/L 02/02/16 03:18 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/02/16 03:18 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/02/16 03:18 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/02/16 03:18 56-23-50.50 1
Chlorobenzene ND ug/L 02/02/16 03:18 108-90-70.50 1
Chloroethane ND ug/L 02/02/16 03:18 75-00-31.0 1
Chloroform ND ug/L 02/02/16 03:18 67-66-30.50 1
Chloromethane ND ug/L 02/02/16 03:18 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/02/16 03:18 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/02/16 03:18 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/02/16 03:18 96-12-81.0 1
Dibromochloromethane ND ug/L 02/02/16 03:18 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/02/16 03:18 106-93-40.50 1
Dibromomethane ND ug/L 02/02/16 03:18 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/02/16 03:18 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/02/16 03:18 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/02/16 03:18 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/02/16 03:18 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/02/16 03:18 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/02/16 03:18 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/02/16 03:18 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/02/16 03:18 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/02/16 03:18 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/02/16 03:18 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/02/16 03:18 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/02/16 03:18 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/02/16 03:18 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/02/16 03:18 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/02/16 03:18 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/02/16 03:18 108-20-30.50 1
Ethylbenzene ND ug/L 02/02/16 03:18 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/02/16 03:18 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/02/16 03:18 98-82-80.50 1
Methylene Chloride ND ug/L 02/02/16 03:18 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/02/16 03:18 1634-04-40.50 1
Naphthalene ND ug/L 02/02/16 03:18 91-20-32.0 1
n-Propylbenzene ND ug/L 02/02/16 03:18 103-65-10.50 1
Styrene ND ug/L 02/02/16 03:18 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/02/16 03:18 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/02/16 03:18 79-34-50.50 1
Tetrachloroethene ND ug/L 02/02/16 03:18 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:MW-10 Lab ID:92284408006 Collected:01/26/16 11:08 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 02/02/16 03:18 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/02/16 03:18 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/02/16 03:18 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/02/16 03:18 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/02/16 03:18 79-00-50.50 1
Trichloroethene ND ug/L 02/02/16 03:18 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/02/16 03:18 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/02/16 03:18 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/02/16 03:18 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/02/16 03:18 108-67-80.50 1
Vinyl chloride ND ug/L 02/02/16 03:18 75-01-41.0 1
m&p-Xylene ND ug/L 02/02/16 03:18 179601-23-11.0 1
o-Xylene ND ug/L 02/02/16 03:18 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %02/02/16 03:18 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %02/02/16 03:18 460-00-470-130 1
Toluene-d8 (S)100 %02/02/16 03:18 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:WSW-2 Lab ID:92284408007 Collected:01/26/16 14:25 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 02/02/16 03:35 71-43-20.50 1
Bromobenzene ND ug/L 02/02/16 03:35 108-86-10.50 1
Bromochloromethane ND ug/L 02/02/16 03:35 74-97-50.50 1
Bromodichloromethane 5.4 ug/L 02/02/16 03:35 75-27-40.50 1
Bromoform ND ug/L 02/02/16 03:35 75-25-20.50 1
Bromomethane ND ug/L 02/02/16 03:35 74-83-95.0 1
n-Butylbenzene ND ug/L 02/02/16 03:35 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/02/16 03:35 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/02/16 03:35 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/02/16 03:35 56-23-50.50 1
Chlorobenzene ND ug/L 02/02/16 03:35 108-90-70.50 1
Chloroethane ND ug/L 02/02/16 03:35 75-00-31.0 1
Chloroform 11.8 ug/L 02/02/16 03:35 67-66-30.50 1
Chloromethane ND ug/L 02/02/16 03:35 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/02/16 03:35 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/02/16 03:35 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/02/16 03:35 96-12-81.0 1
Dibromochloromethane 1.3 ug/L 02/02/16 03:35 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/02/16 03:35 106-93-40.50 1
Dibromomethane ND ug/L 02/02/16 03:35 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/02/16 03:35 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/02/16 03:35 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/02/16 03:35 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/02/16 03:35 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/02/16 03:35 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/02/16 03:35 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/02/16 03:35 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/02/16 03:35 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/02/16 03:35 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/02/16 03:35 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/02/16 03:35 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/02/16 03:35 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/02/16 03:35 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/02/16 03:35 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/02/16 03:35 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/02/16 03:35 108-20-30.50 1
Ethylbenzene ND ug/L 02/02/16 03:35 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/02/16 03:35 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/02/16 03:35 98-82-80.50 1
Methylene Chloride ND ug/L 02/02/16 03:35 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/02/16 03:35 1634-04-40.50 1
Naphthalene ND ug/L 02/02/16 03:35 91-20-32.0 1
n-Propylbenzene ND ug/L 02/02/16 03:35 103-65-10.50 1
Styrene ND ug/L 02/02/16 03:35 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/02/16 03:35 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/02/16 03:35 79-34-50.50 1
Tetrachloroethene ND ug/L 02/02/16 03:35 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:WSW-2 Lab ID:92284408007 Collected:01/26/16 14:25 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 02/02/16 03:35 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/02/16 03:35 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/02/16 03:35 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/02/16 03:35 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/02/16 03:35 79-00-50.50 1
Trichloroethene ND ug/L 02/02/16 03:35 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/02/16 03:35 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/02/16 03:35 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/02/16 03:35 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/02/16 03:35 108-67-80.50 1
Vinyl chloride ND ug/L 02/02/16 03:35 75-01-41.0 1
m&p-Xylene ND ug/L 02/02/16 03:35 179601-23-11.0 1
o-Xylene ND ug/L 02/02/16 03:35 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %02/02/16 03:35 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %02/02/16 03:35 460-00-470-130 1
Toluene-d8 (S)99 %02/02/16 03:35 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:WSW-4 Lab ID:92284408008 Collected:01/26/16 14:45 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 02/02/16 03:52 71-43-20.50 1
Bromobenzene ND ug/L 02/02/16 03:52 108-86-10.50 1
Bromochloromethane ND ug/L 02/02/16 03:52 74-97-50.50 1
Bromodichloromethane 6.0 ug/L 02/02/16 03:52 75-27-40.50 1
Bromoform ND ug/L 02/02/16 03:52 75-25-20.50 1
Bromomethane ND ug/L 02/02/16 03:52 74-83-95.0 1
n-Butylbenzene ND ug/L 02/02/16 03:52 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/02/16 03:52 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/02/16 03:52 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/02/16 03:52 56-23-50.50 1
Chlorobenzene ND ug/L 02/02/16 03:52 108-90-70.50 1
Chloroethane ND ug/L 02/02/16 03:52 75-00-31.0 1
Chloroform 13.3 ug/L 02/02/16 03:52 67-66-30.50 1
Chloromethane ND ug/L 02/02/16 03:52 74-87-31.0 1
2-Chlorotoluene ND ug/L 02/02/16 03:52 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/02/16 03:52 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/02/16 03:52 96-12-81.0 1
Dibromochloromethane 1.3 ug/L 02/02/16 03:52 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/02/16 03:52 106-93-40.50 1
Dibromomethane ND ug/L 02/02/16 03:52 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/02/16 03:52 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/02/16 03:52 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/02/16 03:52 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/02/16 03:52 75-71-80.50 1
1,1-Dichloroethane ND ug/L 02/02/16 03:52 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/02/16 03:52 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/02/16 03:52 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/02/16 03:52 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/02/16 03:52 156-60-50.50 1
1,2-Dichloropropane ND ug/L 02/02/16 03:52 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/02/16 03:52 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/02/16 03:52 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/02/16 03:52 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/02/16 03:52 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/02/16 03:52 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/02/16 03:52 108-20-30.50 1
Ethylbenzene ND ug/L 02/02/16 03:52 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/02/16 03:52 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/02/16 03:52 98-82-80.50 1
Methylene Chloride ND ug/L 02/02/16 03:52 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/02/16 03:52 1634-04-40.50 1
Naphthalene ND ug/L 02/02/16 03:52 91-20-32.0 1
n-Propylbenzene ND ug/L 02/02/16 03:52 103-65-10.50 1
Styrene ND ug/L 02/02/16 03:52 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/02/16 03:52 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/02/16 03:52 79-34-50.50 1
Tetrachloroethene ND ug/L 02/02/16 03:52 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:WSW-4 Lab ID:92284408008 Collected:01/26/16 14:45 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 02/02/16 03:52 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/02/16 03:52 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/02/16 03:52 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/02/16 03:52 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/02/16 03:52 79-00-50.50 1
Trichloroethene ND ug/L 02/02/16 03:52 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/02/16 03:52 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/02/16 03:52 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/02/16 03:52 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/02/16 03:52 108-67-80.50 1
Vinyl chloride ND ug/L 02/02/16 03:52 75-01-41.0 1
m&p-Xylene ND ug/L 02/02/16 03:52 179601-23-11.0 1
o-Xylene ND ug/L 02/02/16 03:52 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)101 %02/02/16 03:52 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %02/02/16 03:52 460-00-470-130 1
Toluene-d8 (S)98 %02/02/16 03:52 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:WSW-5 Lab ID:92284408009 Collected:01/26/16 15:10 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 02/02/16 04:09 71-43-20.50 1
Bromobenzene ND ug/L 02/02/16 04:09 108-86-10.50 1
Bromochloromethane ND ug/L 02/02/16 04:09 74-97-50.50 1
Bromodichloromethane ND ug/L 02/02/16 04:09 75-27-40.50 1
Bromoform ND ug/L 02/02/16 04:09 75-25-20.50 1
Bromomethane ND ug/L 02/02/16 04:09 74-83-9 M15.0 1
n-Butylbenzene ND ug/L 02/02/16 04:09 104-51-80.50 1
sec-Butylbenzene ND ug/L 02/02/16 04:09 135-98-80.50 1
tert-Butylbenzene ND ug/L 02/02/16 04:09 98-06-60.50 1
Carbon tetrachloride ND ug/L 02/02/16 04:09 56-23-50.50 1
Chlorobenzene ND ug/L 02/02/16 04:09 108-90-70.50 1
Chloroethane ND ug/L 02/02/16 04:09 75-00-31.0 1
Chloroform ND ug/L 02/02/16 04:09 67-66-30.50 1
Chloromethane ND ug/L 02/02/16 04:09 74-87-3 M11.0 1
2-Chlorotoluene ND ug/L 02/02/16 04:09 95-49-80.50 1
4-Chlorotoluene ND ug/L 02/02/16 04:09 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 02/02/16 04:09 96-12-81.0 1
Dibromochloromethane ND ug/L 02/02/16 04:09 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 02/02/16 04:09 106-93-40.50 1
Dibromomethane ND ug/L 02/02/16 04:09 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 02/02/16 04:09 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 02/02/16 04:09 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 02/02/16 04:09 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 02/02/16 04:09 75-71-8 M10.50 1
1,1-Dichloroethane ND ug/L 02/02/16 04:09 75-34-30.50 1
1,2-Dichloroethane ND ug/L 02/02/16 04:09 107-06-20.50 1
1,1-Dichloroethene ND ug/L 02/02/16 04:09 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 02/02/16 04:09 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 02/02/16 04:09 156-60-50.50 1
1,2-Dichloropropane 1.7 ug/L 02/02/16 04:09 78-87-50.50 1
1,3-Dichloropropane ND ug/L 02/02/16 04:09 142-28-90.50 1
2,2-Dichloropropane ND ug/L 02/02/16 04:09 594-20-70.50 1
1,1-Dichloropropene ND ug/L 02/02/16 04:09 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 02/02/16 04:09 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 02/02/16 04:09 10061-02-60.50 1
Diisopropyl ether ND ug/L 02/02/16 04:09 108-20-30.50 1
Ethylbenzene ND ug/L 02/02/16 04:09 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 02/02/16 04:09 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 02/02/16 04:09 98-82-80.50 1
Methylene Chloride ND ug/L 02/02/16 04:09 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 02/02/16 04:09 1634-04-40.50 1
Naphthalene ND ug/L 02/02/16 04:09 91-20-32.0 1
n-Propylbenzene ND ug/L 02/02/16 04:09 103-65-10.50 1
Styrene ND ug/L 02/02/16 04:09 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 02/02/16 04:09 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 02/02/16 04:09 79-34-50.50 1
Tetrachloroethene ND ug/L 02/02/16 04:09 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 35
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Sample:WSW-5 Lab ID:92284408009 Collected:01/26/16 15:10 Received:01/27/16 09:50 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 02/02/16 04:09 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 02/02/16 04:09 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 02/02/16 04:09 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 02/02/16 04:09 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 02/02/16 04:09 79-00-50.50 1
Trichloroethene ND ug/L 02/02/16 04:09 79-01-60.50 1
Trichlorofluoromethane ND ug/L 02/02/16 04:09 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 02/02/16 04:09 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 02/02/16 04:09 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 02/02/16 04:09 108-67-80.50 1
Vinyl chloride ND ug/L 02/02/16 04:09 75-01-41.0 1
m&p-Xylene ND ug/L 02/02/16 04:09 179601-23-11.0 1
o-Xylene ND ug/L 02/02/16 04:09 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %02/02/16 04:09 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %02/02/16 04:09 460-00-470-130 1
Toluene-d8 (S)99 %02/02/16 04:09 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/35395
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92284408001, 92284408002, 92284408003
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1657756
Associated Lab Samples:92284408001, 92284408002, 92284408003
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 02/01/16 15:10
1,1,1-Trichloroethane ug/L ND 0.50 02/01/16 15:10
1,1,2,2-Tetrachloroethane ug/L ND 0.50 02/01/16 15:10
1,1,2-Trichloroethane ug/L ND 0.50 02/01/16 15:10
1,1-Dichloroethane ug/L ND 0.50 02/01/16 15:10
1,1-Dichloroethene ug/L ND 0.50 02/01/16 15:10
1,1-Dichloropropene ug/L ND 0.50 02/01/16 15:10
1,2,3-Trichlorobenzene ug/L ND 2.0 02/01/16 15:10
1,2,3-Trichloropropane ug/L ND 0.50 02/01/16 15:10
1,2,4-Trichlorobenzene ug/L ND 2.0 02/01/16 15:10
1,2,4-Trimethylbenzene ug/L ND 0.50 02/01/16 15:10
1,2-Dibromo-3-chloropropane ug/L ND 1.0 02/01/16 15:10
1,2-Dibromoethane (EDB)ug/L ND 0.50 02/01/16 15:10
1,2-Dichlorobenzene ug/L ND 0.50 02/01/16 15:10
1,2-Dichloroethane ug/L ND 0.50 02/01/16 15:10
1,2-Dichloropropane ug/L ND 0.50 02/01/16 15:10
1,3,5-Trimethylbenzene ug/L ND 0.50 02/01/16 15:10
1,3-Dichlorobenzene ug/L ND 0.50 02/01/16 15:10
1,3-Dichloropropane ug/L ND 0.50 02/01/16 15:10
1,4-Dichlorobenzene ug/L ND 0.50 02/01/16 15:10
2,2-Dichloropropane ug/L ND 0.50 02/01/16 15:10
2-Chlorotoluene ug/L ND 0.50 02/01/16 15:10
4-Chlorotoluene ug/L ND 0.50 02/01/16 15:10
Benzene ug/L ND 0.50 02/01/16 15:10
Bromobenzene ug/L ND 0.50 02/01/16 15:10
Bromochloromethane ug/L ND 0.50 02/01/16 15:10
Bromodichloromethane ug/L ND 0.50 02/01/16 15:10
Bromoform ug/L ND 0.50 02/01/16 15:10
Bromomethane ug/L ND 5.0 02/01/16 15:10
Carbon tetrachloride ug/L ND 0.50 02/01/16 15:10
Chlorobenzene ug/L ND 0.50 02/01/16 15:10
Chloroethane ug/L ND 1.0 02/01/16 15:10
Chloroform ug/L ND 0.50 02/01/16 15:10
Chloromethane ug/L ND 1.0 02/01/16 15:10
cis-1,2-Dichloroethene ug/L ND 0.50 02/01/16 15:10
cis-1,3-Dichloropropene ug/L ND 0.50 02/01/16 15:10
Dibromochloromethane ug/L ND 0.50 02/01/16 15:10
Dibromomethane ug/L ND 0.50 02/01/16 15:10
Dichlorodifluoromethane ug/L ND 0.50 02/01/16 15:10
Diisopropyl ether ug/L ND 0.50 02/01/16 15:10
Ethylbenzene ug/L ND 0.50 02/01/16 15:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1657756
Associated Lab Samples:92284408001, 92284408002, 92284408003
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 02/01/16 15:10
Isopropylbenzene (Cumene)ug/L ND 0.50 02/01/16 15:10
m&p-Xylene ug/L ND 1.0 02/01/16 15:10
Methyl-tert-butyl ether ug/L ND 0.50 02/01/16 15:10
Methylene Chloride ug/L ND 2.0 02/01/16 15:10
n-Butylbenzene ug/L ND 0.50 02/01/16 15:10
n-Propylbenzene ug/L ND 0.50 02/01/16 15:10
Naphthalene ug/L ND 2.0 02/01/16 15:10
o-Xylene ug/L ND 0.50 02/01/16 15:10
sec-Butylbenzene ug/L ND 0.50 02/01/16 15:10
Styrene ug/L ND 0.50 02/01/16 15:10
tert-Butylbenzene ug/L ND 0.50 02/01/16 15:10
Tetrachloroethene ug/L ND 0.50 02/01/16 15:10
Toluene ug/L ND 0.50 02/01/16 15:10
trans-1,2-Dichloroethene ug/L ND 0.50 02/01/16 15:10
trans-1,3-Dichloropropene ug/L ND 0.50 02/01/16 15:10
Trichloroethene ug/L ND 0.50 02/01/16 15:10
Trichlorofluoromethane ug/L ND 1.0 02/01/16 15:10
Vinyl chloride ug/L ND 1.0 02/01/16 15:10
1,2-Dichloroethane-d4 (S)%99 70-130 02/01/16 15:10
4-Bromofluorobenzene (S)%100 70-130 02/01/16 15:10
Toluene-d8 (S)%101 70-130 02/01/16 15:10
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1657757LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.850 102 60-140
1,1,1-Trichloroethane ug/L 46.750 93 60-140
1,1,2,2-Tetrachloroethane ug/L 48.650 97 60-140
1,1,2-Trichloroethane ug/L 47.950 96 60-140
1,1-Dichloroethane ug/L 45.450 91 60-140
1,1-Dichloroethene ug/L 45.250 90 60-140
1,1-Dichloropropene ug/L 47.350 95 60-140
1,2,3-Trichlorobenzene ug/L 53.250 106 60-140
1,2,3-Trichloropropane ug/L 50.650 101 60-140
1,2,4-Trichlorobenzene ug/L 52.550 105 60-140
1,2,4-Trimethylbenzene ug/L 49.650 99 60-140
1,2-Dibromo-3-chloropropane ug/L 54.250 108 60-140
1,2-Dibromoethane (EDB)ug/L 50.950 102 60-140
1,2-Dichlorobenzene ug/L 48.550 97 60-140
1,2-Dichloroethane ug/L 42.250 84 60-140
1,2-Dichloropropane ug/L 46.450 93 60-140
1,3,5-Trimethylbenzene ug/L 47.950 96 60-140
1,3-Dichlorobenzene ug/L 49.350 99 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1657757LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 48.150 96 60-140
1,4-Dichlorobenzene ug/L 49.050 98 60-140
2,2-Dichloropropane ug/L 48.350 97 60-140
2-Chlorotoluene ug/L 47.250 94 60-140
4-Chlorotoluene ug/L 47.750 95 60-140
Benzene ug/L 48.950 98 60-140
Bromobenzene ug/L 49.050 98 60-140
Bromochloromethane ug/L 46.850 94 60-140
Bromodichloromethane ug/L 49.350 99 60-140
Bromoform ug/L 60.150 120 60-140
Bromomethane ug/L 34.650 69 60-140
Carbon tetrachloride ug/L 49.050 98 60-140
Chlorobenzene ug/L 47.350 95 60-140
Chloroethane ug/L 45.950 92 60-140
Chloroform ug/L 44.950 90 60-140
Chloromethane ug/L 37.350 75 60-140
cis-1,2-Dichloroethene ug/L 44.350 89 60-140
cis-1,3-Dichloropropene ug/L 49.750 99 60-140
Dibromochloromethane ug/L 56.350 113 60-140
Dibromomethane ug/L 49.050 98 60-140
Dichlorodifluoromethane ug/L 30.250 60 60-140
Diisopropyl ether ug/L 47.650 95 60-140
Ethylbenzene ug/L 46.850 94 60-140
Hexachloro-1,3-butadiene ug/L 52.550 105 60-140
Isopropylbenzene (Cumene)ug/L 46.650 93 60-140
m&p-Xylene ug/L 92.6100 93 60-140
Methyl-tert-butyl ether ug/L 49.850 100 60-140
Methylene Chloride ug/L 43.850 88 60-140
n-Butylbenzene ug/L 49.150 98 60-140
n-Propylbenzene ug/L 46.850 94 60-140
Naphthalene ug/L 52.550 105 60-140
o-Xylene ug/L 45.850 92 60-140
sec-Butylbenzene ug/L 46.950 94 60-140
Styrene ug/L 49.650 99 60-140
tert-Butylbenzene ug/L 39.650 79 60-140
Tetrachloroethene ug/L 46.450 93 60-140
Toluene ug/L 45.550 91 60-140
trans-1,2-Dichloroethene ug/L 45.650 91 60-140
trans-1,3-Dichloropropene ug/L 50.050 100 60-140
Trichloroethene ug/L 45.450 91 60-140
Trichlorofluoromethane ug/L 43.350 87 60-140
Vinyl chloride ug/L 41.150 82 60-140
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%103 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1657758MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92284408003
1657759
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 104 60-140108 420ND20.8 21.6
1,1,1-Trichloroethane ug/L 20 111 60-140111 020ND22.1 22.2
1,1,2,2-Tetrachloroethane ug/L 20 101 60-140104 220ND20.3 20.7
1,1,2-Trichloroethane ug/L 20 104 60-140105 120ND20.8 20.9
1,1-Dichloroethane ug/L 20 105 60-140107 120ND21.1 21.4
1,1-Dichloroethene ug/L 20 112 60-140111 120ND22.4 22.2
1,1-Dichloropropene ug/L 20 112 60-140112 020ND22.3 22.4
1,2,3-Trichlorobenzene ug/L 20 106 60-140112 620ND21.1 22.4
1,2,3-Trichloropropane ug/L 20 104 60-140108 420ND20.9 21.7
1,2,4-Trichlorobenzene ug/L 20 105 60-140110 420ND21.0 21.9
1,2,4-Trimethylbenzene ug/L 20 104 60-140109 420ND20.8 21.8
1,2-Dibromo-3-chloropropane ug/L 20 104 60-140109 420ND20.9 21.8
1,2-Dibromoethane (EDB)ug/L 20 106 60-140111 420ND21.2 22.1
1,2-Dichlorobenzene ug/L 20 101 60-140105 520ND20.1 21.1
1,2-Dichloroethane ug/L 20 97 60-14098 120ND19.6 19.8
1,2-Dichloropropane ug/L 20 102 60-140103 220ND20.3 20.7
1,3,5-Trimethylbenzene ug/L 20 102 60-140106 420ND20.4 21.2
1,3-Dichlorobenzene ug/L 20 102 60-140107 520ND20.5 21.5
1,3-Dichloropropane ug/L 20 101 60-140103 220ND20.2 20.6
1,4-Dichlorobenzene ug/L 20 102 60-140107 520ND20.6 21.6
2,2-Dichloropropane ug/L 20 105 60-140106 120ND21.0 21.3
2-Chlorotoluene ug/L 20 98 60-140103 520ND19.7 20.6
4-Chlorotoluene ug/L 20 101 60-140106 520ND20.2 21.2
Benzene ug/L 20 111 60-140111 020ND22.2 22.2
Bromobenzene ug/L 20 107 60-140114 620ND21.5 22.8
Bromochloromethane ug/L 20 105 60-140106 120ND20.9 21.2
Bromodichloromethane ug/L 20 103 60-140105 220ND20.6 21.0
Bromoform ug/L 20 95 60-140103 820ND19.0 20.6
Bromomethane ug/L 20 81 60-14076 620ND16.1 15.2
Carbon tetrachloride ug/L 20 108 60-140111 320ND21.6 22.2
Chlorobenzene ug/L 20 102 60-140106 420ND20.4 21.2
Chloroethane ug/L 20 118 60-140115 220ND23.5 23.0
Chloroform ug/L 20 103 60-140106 320ND20.6 21.1
Chloromethane ug/L 20 98 60-140100 120ND19.7 19.9
cis-1,2-Dichloroethene ug/L 20 105 60-140106 120ND20.9 21.2
cis-1,3-Dichloropropene ug/L 20 101 60-140104 320ND20.2 20.8
Dibromochloromethane ug/L 20 102 60-140110 820ND20.4 22.1
Dibromomethane ug/L 20 108 60-140108 020ND21.6 21.5
Dichlorodifluoromethane ug/L 20 102 60-140104 120ND20.4 20.7
Diisopropyl ether ug/L 20 107 60-140108 120ND21.3 21.6
Ethylbenzene ug/L 20 102 60-140106 320ND20.5 21.2
Hexachloro-1,3-butadiene ug/L 20 101 60-140104 320ND20.1 20.8
Isopropylbenzene (Cumene)ug/L 20 102 60-140105 420ND20.3 21.1
m&p-Xylene ug/L 40 102 60-140106 340ND40.8 42.2
Methyl-tert-butyl ether ug/L 20 111 60-140113 220ND22.1 22.6
Methylene Chloride ug/L 20 99 60-14099 020ND20.1 20.1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1657758MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92284408003
1657759
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 101 60-140104 320ND20.1 20.8
n-Propylbenzene ug/L 20 100 60-140105 520ND20.1 21.0
Naphthalene ug/L 20 107 60-140112 520ND21.3 22.5
o-Xylene ug/L 20 101 60-140104 320ND20.2 20.8
sec-Butylbenzene ug/L 20 100 60-140105 520ND19.9 20.9
Styrene ug/L 20 103 60-140106 320ND20.7 21.3
tert-Butylbenzene ug/L 20 85 60-14089 420ND17.0 17.8
Tetrachloroethene ug/L 20 102 60-140106 420ND20.4 21.2
Toluene ug/L 20 102 60-140104 220ND20.5 20.9
trans-1,2-Dichloroethene ug/L 20 105 60-140108 320ND21.1 21.7
trans-1,3-Dichloropropene ug/L 20 100 60-140103 320ND20.1 20.6
Trichloroethene ug/L 20 104 60-140105 120ND20.7 20.9
Trichlorofluoromethane ug/L 20 111 60-140113 220ND22.2 22.5
Vinyl chloride ug/L 20 109 60-140111 220ND21.7 22.1
1,2-Dichloroethane-d4 (S)%103 70-130100
4-Bromofluorobenzene (S)%101 70-130102
Toluene-d8 (S)%100 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/35397
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92284408004, 92284408005, 92284408006, 92284408007, 92284408008, 92284408009
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1657779
Associated Lab Samples:92284408004, 92284408005, 92284408006, 92284408007, 92284408008, 92284408009
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 02/02/16 02:27
1,1,1-Trichloroethane ug/L ND 0.50 02/02/16 02:27
1,1,2,2-Tetrachloroethane ug/L ND 0.50 02/02/16 02:27
1,1,2-Trichloroethane ug/L ND 0.50 02/02/16 02:27
1,1-Dichloroethane ug/L ND 0.50 02/02/16 02:27
1,1-Dichloroethene ug/L ND 0.50 02/02/16 02:27
1,1-Dichloropropene ug/L ND 0.50 02/02/16 02:27
1,2,3-Trichlorobenzene ug/L ND 2.0 02/02/16 02:27
1,2,3-Trichloropropane ug/L ND 0.50 02/02/16 02:27
1,2,4-Trichlorobenzene ug/L ND 2.0 02/02/16 02:27
1,2,4-Trimethylbenzene ug/L ND 0.50 02/02/16 02:27
1,2-Dibromo-3-chloropropane ug/L ND 1.0 02/02/16 02:27
1,2-Dibromoethane (EDB)ug/L ND 0.50 02/02/16 02:27
1,2-Dichlorobenzene ug/L ND 0.50 02/02/16 02:27
1,2-Dichloroethane ug/L ND 0.50 02/02/16 02:27
1,2-Dichloropropane ug/L ND 0.50 02/02/16 02:27
1,3,5-Trimethylbenzene ug/L ND 0.50 02/02/16 02:27
1,3-Dichlorobenzene ug/L ND 0.50 02/02/16 02:27
1,3-Dichloropropane ug/L ND 0.50 02/02/16 02:27
1,4-Dichlorobenzene ug/L ND 0.50 02/02/16 02:27
2,2-Dichloropropane ug/L ND 0.50 02/02/16 02:27
2-Chlorotoluene ug/L ND 0.50 02/02/16 02:27
4-Chlorotoluene ug/L ND 0.50 02/02/16 02:27
Benzene ug/L ND 0.50 02/02/16 02:27
Bromobenzene ug/L ND 0.50 02/02/16 02:27
Bromochloromethane ug/L ND 0.50 02/02/16 02:27
Bromodichloromethane ug/L ND 0.50 02/02/16 02:27
Bromoform ug/L ND 0.50 02/02/16 02:27
Bromomethane ug/L ND 5.0 02/02/16 02:27
Carbon tetrachloride ug/L ND 0.50 02/02/16 02:27
Chlorobenzene ug/L ND 0.50 02/02/16 02:27
Chloroethane ug/L ND 1.0 02/02/16 02:27
Chloroform ug/L ND 0.50 02/02/16 02:27
Chloromethane ug/L ND 1.0 02/02/16 02:27
cis-1,2-Dichloroethene ug/L ND 0.50 02/02/16 02:27
cis-1,3-Dichloropropene ug/L ND 0.50 02/02/16 02:27
Dibromochloromethane ug/L ND 0.50 02/02/16 02:27
Dibromomethane ug/L ND 0.50 02/02/16 02:27
Dichlorodifluoromethane ug/L ND 0.50 02/02/16 02:27
Diisopropyl ether ug/L ND 0.50 02/02/16 02:27
Ethylbenzene ug/L ND 0.50 02/02/16 02:27
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1657779
Associated Lab Samples:92284408004, 92284408005, 92284408006, 92284408007, 92284408008, 92284408009
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 02/02/16 02:27
Isopropylbenzene (Cumene)ug/L ND 0.50 02/02/16 02:27
m&p-Xylene ug/L ND 1.0 02/02/16 02:27
Methyl-tert-butyl ether ug/L ND 0.50 02/02/16 02:27
Methylene Chloride ug/L ND 2.0 02/02/16 02:27
n-Butylbenzene ug/L ND 0.50 02/02/16 02:27
n-Propylbenzene ug/L ND 0.50 02/02/16 02:27
Naphthalene ug/L ND 2.0 02/02/16 02:27
o-Xylene ug/L ND 0.50 02/02/16 02:27
sec-Butylbenzene ug/L ND 0.50 02/02/16 02:27
Styrene ug/L ND 0.50 02/02/16 02:27
tert-Butylbenzene ug/L ND 0.50 02/02/16 02:27
Tetrachloroethene ug/L ND 0.50 02/02/16 02:27
Toluene ug/L ND 0.50 02/02/16 02:27
trans-1,2-Dichloroethene ug/L ND 0.50 02/02/16 02:27
trans-1,3-Dichloropropene ug/L ND 0.50 02/02/16 02:27
Trichloroethene ug/L ND 0.50 02/02/16 02:27
Trichlorofluoromethane ug/L ND 1.0 02/02/16 02:27
Vinyl chloride ug/L ND 1.0 02/02/16 02:27
1,2-Dichloroethane-d4 (S)%102 70-130 02/02/16 02:27
4-Bromofluorobenzene (S)%100 70-130 02/02/16 02:27
Toluene-d8 (S)%100 70-130 02/02/16 02:27
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1657780LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 48.950 98 60-140
1,1,1-Trichloroethane ug/L 48.350 97 60-140
1,1,2,2-Tetrachloroethane ug/L 46.250 92 60-140
1,1,2-Trichloroethane ug/L 46.950 94 60-140
1,1-Dichloroethane ug/L 45.950 92 60-140
1,1-Dichloroethene ug/L 47.150 94 60-140
1,1-Dichloropropene ug/L 47.850 96 60-140
1,2,3-Trichlorobenzene ug/L 48.450 97 60-140
1,2,3-Trichloropropane ug/L 48.450 97 60-140
1,2,4-Trichlorobenzene ug/L 47.650 95 60-140
1,2,4-Trimethylbenzene ug/L 46.950 94 60-140
1,2-Dibromo-3-chloropropane ug/L 49.650 99 60-140
1,2-Dibromoethane (EDB)ug/L 48.750 97 60-140
1,2-Dichlorobenzene ug/L 46.050 92 60-140
1,2-Dichloroethane ug/L 42.750 85 60-140
1,2-Dichloropropane ug/L 46.450 93 60-140
1,3,5-Trimethylbenzene ug/L 45.950 92 60-140
1,3-Dichlorobenzene ug/L 46.750 93 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1657780LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 46.850 94 60-140
1,4-Dichlorobenzene ug/L 46.750 93 60-140
2,2-Dichloropropane ug/L 43.150 86 60-140
2-Chlorotoluene ug/L 44.250 88 60-140
4-Chlorotoluene ug/L 45.150 90 60-140
Benzene ug/L 49.450 99 60-140
Bromobenzene ug/L 44.650 89 60-140
Bromochloromethane ug/L 47.150 94 60-140
Bromodichloromethane ug/L 47.850 96 60-140
Bromoform ug/L 51.450 103 60-140
Bromomethane ug/L 38.050 76 60-140
Carbon tetrachloride ug/L 49.550 99 60-140
Chlorobenzene ug/L 46.450 93 60-140
Chloroethane ug/L 47.950 96 60-140
Chloroform ug/L 45.550 91 60-140
Chloromethane ug/L 43.950 88 60-140
cis-1,2-Dichloroethene ug/L 45.250 90 60-140
cis-1,3-Dichloropropene ug/L 47.550 95 60-140
Dibromochloromethane ug/L 51.350 103 60-140
Dibromomethane ug/L 48.750 97 60-140
Dichlorodifluoromethane ug/L 42.350 85 60-140
Diisopropyl ether ug/L 47.350 95 60-140
Ethylbenzene ug/L 46.150 92 60-140
Hexachloro-1,3-butadiene ug/L 47.550 95 60-140
Isopropylbenzene (Cumene)ug/L 45.650 91 60-140
m&p-Xylene ug/L 91.2100 91 60-140
Methyl-tert-butyl ether ug/L 49.350 99 60-140
Methylene Chloride ug/L 43.550 87 60-140
n-Butylbenzene ug/L 45.750 91 60-140
n-Propylbenzene ug/L 44.750 89 60-140
Naphthalene ug/L 48.150 96 60-140
o-Xylene ug/L 45.650 91 60-140
sec-Butylbenzene ug/L 45.150 90 60-140
Styrene ug/L 48.050 96 60-140
tert-Butylbenzene ug/L 38.650 77 60-140
Tetrachloroethene ug/L 45.550 91 60-140
Toluene ug/L 46.850 94 60-140
trans-1,2-Dichloroethene ug/L 46.150 92 60-140
trans-1,3-Dichloropropene ug/L 46.450 93 60-140
Trichloroethene ug/L 46.450 93 60-140
Trichlorofluoromethane ug/L 46.350 93 60-140
Vinyl chloride ug/L 46.450 93 60-140
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1657781MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92284408009
1657782
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 108 60-140103 520ND21.7 20.6
1,1,1-Trichloroethane ug/L 20 103 60-140105 220ND20.6 21.0
1,1,2,2-Tetrachloroethane ug/L 20 104 60-140101 220ND20.7 20.3
1,1,2-Trichloroethane ug/L 20 100 60-140101 120ND20.1 20.2
1,1-Dichloroethane ug/L 20 100 60-140100 020ND20.0 20.0
1,1-Dichloroethene ug/L 20 100 60-140101 020ND20.1 20.1
1,1-Dichloropropene ug/L 20 105 60-140106 120ND21.0 21.2
1,2,3-Trichlorobenzene ug/L 20 112 60-140108 320ND22.4 21.7
1,2,3-Trichloropropane ug/L 20 111 60-140108 320ND22.2 21.5
1,2,4-Trichlorobenzene ug/L 20 110 60-140109 120ND21.9 21.7
1,2,4-Trimethylbenzene ug/L 20 109 60-140106 320ND21.9 21.2
1,2-Dibromo-3-chloropropane ug/L 20 107 60-140104 320ND21.5 20.9
1,2-Dibromoethane (EDB)ug/L 20 109 60-140106 320ND21.8 21.3
1,2-Dichlorobenzene ug/L 20 104 60-140103 120ND20.8 20.7
1,2-Dichloroethane ug/L 20 93 60-14094 020ND18.8 18.8
1,2-Dichloropropane ug/L 20 99 60-140100 1201.7 21.5 21.8
1,3,5-Trimethylbenzene ug/L 20 107 60-140105 220ND21.4 21.0
1,3-Dichlorobenzene ug/L 20 107 60-140106 220ND21.5 21.1
1,3-Dichloropropane ug/L 20 101 60-14098 320ND20.3 19.6
1,4-Dichlorobenzene ug/L 20 107 60-140103 420ND21.4 20.6
2,2-Dichloropropane ug/L 20 102 60-140104 220ND20.5 20.9
2-Chlorotoluene ug/L 20 104 60-140101 320ND20.8 20.2
4-Chlorotoluene ug/L 20 105 60-140102 420ND21.1 20.4
Benzene ug/L 20 107 60-140106 120ND21.3 21.2
Bromobenzene ug/L 20 103 60-14099 420ND20.5 19.8
Bromochloromethane ug/L 20 99 60-140102 320ND19.8 20.5
Bromodichloromethane ug/L 20 99 60-140100 120ND19.8 19.9
Bromoform ug/L 20 95 60-14093 220ND18.9 18.6
Bromomethane ug/L M1202760-14034 2420ND5.4 6.9
Carbon tetrachloride ug/L 20 104 60-140104 020ND20.7 20.8
Chlorobenzene ug/L 20 105 60-140101 320ND20.9 20.3
Chloroethane ug/L 20 94 60-14097 320ND18.9 19.4
Chloroform ug/L 20 100 60-140101 120ND20.0 20.2
Chloromethane ug/L M1205960-14060 120ND11.8 11.9
cis-1,2-Dichloroethene ug/L 20 98 60-14099 120ND19.5 19.7
cis-1,3-Dichloropropene ug/L 20 98 60-14099 120ND19.6 19.9
Dibromochloromethane ug/L 20 103 60-140103 020ND20.5 20.5
Dibromomethane ug/L 20 104 60-140102 220ND20.7 20.4
Dichlorodifluoromethane ug/L M1204160-14043 420ND8.2 8.5
Diisopropyl ether ug/L 20 101 60-140101 020ND20.1 20.2
Ethylbenzene ug/L 20 105 60-140102 320ND21.0 20.4
Hexachloro-1,3-butadiene ug/L 20 109 60-140107 220ND21.8 21.4
Isopropylbenzene (Cumene)ug/L 20 105 60-140100 520ND21.0 20.1
m&p-Xylene ug/L 40 104 60-140101 340ND41.5 40.4
Methyl-tert-butyl ether ug/L 20 104 60-140105 220ND20.7 21.1
Methylene Chloride ug/L 20 93 60-14093 020ND18.7 18.8
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
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Page 30 of 35
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1657781MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92284408009
1657782
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 109 60-140104 520ND21.7 20.8
n-Propylbenzene ug/L 20 106 60-140101 420ND21.1 20.3
Naphthalene ug/L 20 113 60-140110 320ND22.7 22.1
o-Xylene ug/L 20 102 60-14099 320ND20.4 19.8
sec-Butylbenzene ug/L 20 106 60-140104 120ND21.1 20.8
Styrene ug/L 20 107 60-140103 420ND21.4 20.5
tert-Butylbenzene ug/L 20 89 60-14087 320ND17.9 17.3
Tetrachloroethene ug/L 20 106 60-140101 420ND21.2 20.3
Toluene ug/L 20 102 60-140100 220ND20.4 20.0
trans-1,2-Dichloroethene ug/L 20 99 60-140102 220ND19.8 20.3
trans-1,3-Dichloropropene ug/L 20 99 60-14096 320ND19.7 19.1
Trichloroethene ug/L 20 101 60-140101 120ND20.2 20.1
Trichlorofluoromethane ug/L 20 97 60-14097 020ND19.4 19.4
Vinyl chloride ug/L 20 79 60-14080 120ND15.8 16.0
1,2-Dichloroethane-d4 (S)%97 70-130100
4-Bromofluorobenzene (S)%101 70-130101
Toluene-d8 (S)%98 70-13099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 35
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
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[phone]
Page 32 of 35
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92284408
FLOWERS STORE PROPERTY
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92284408001 MSV/35395MW-7 SM 6200B
92284408002 MSV/35395MW-8 SM 6200B
92284408003 MSV/35395MW-3 SM 6200B
92284408004 MSV/35397MW-5 SM 6200B
92284408005 MSV/35397MW-9 SM 6200B
92284408006 MSV/35397MW-10 SM 6200B
92284408007 MSV/35397WSW-2 SM 6200B
92284408008 MSV/35397WSW-4 SM 6200B
92284408009 MSV/35397WSW-5 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 02/02/2016 04:35 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 35
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