FA-916_17217_CA_LAB_20150622_Pace Labs Report for ECS Sampling 6-11-15

#=CL#
June 22, 2015
LIMS USE: FR - MATTHEW GILLIS
LIMS OBJECT ID: 92254444
92254444
Project:
Pace Project No.:
RE:
Matthew Gillis
ECS
9001 Glenwood Avenue
Raleigh, NC 27617
FLOWERS STORE 21858-A
Dear Matthew Gillis:
Enclosed are the analytical results for sample(s) received by the laboratory on June 15, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
The laboratory report is being resubmitted on June 22, 2015, to correct the project ID.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
Project Manager
Enclosures
cc:Matthew Gillis, ECS
Brian Smith, ECS Carolinas LLP
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 33
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84
West Virginia Certification #: 357Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 33
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92254444004 MW-8
1,4-Dichlorobenzene 0.61 ug/L 06/19/15 04:120.50SM 6200B
92254444005 MW-9
sec-Butylbenzene 2.1 ug/L 06/19/15 16:380.50SM 6200B
Isopropylbenzene (Cumene)1.6 ug/L 06/19/15 16:380.50SM 6200B
Naphthalene 17.1 ug/L 06/19/15 16:382.0SM 6200B
n-Propylbenzene 3.3 ug/L 06/19/15 16:380.50SM 6200B
1,2,4-Trimethylbenzene 15.7 ug/L 06/19/15 16:380.50SM 6200B
1,3,5-Trimethylbenzene 27.7 ug/L 06/19/15 16:380.50SM 6200B
m&p-Xylene 1.3 ug/L 06/19/15 16:381.0SM 6200B
o-Xylene 2.4 ug/L 06/19/15 16:380.50SM 6200B
92254444007 WSW-5
1,2-Dichloropropane 2.1 ug/L 06/19/15 02:160.50SM 6200B
92254444008 WSW-4
Bromodichloromethane 12.4 ug/L 06/19/15 02:330.50SM 6200B
Chloroform 24.1 ug/L 06/19/15 02:330.50SM 6200B
Dibromochloromethane 4.6 ug/L 06/19/15 02:330.50SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Sample:MW-3 Lab ID:92254444001 Collected:06/11/15 09:42 Received:06/15/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 06/19/15 03:55 71-43-20.50 1
Bromobenzene ND ug/L 06/19/15 03:55 108-86-10.50 1
Bromochloromethane ND ug/L 06/19/15 03:55 74-97-50.50 1
Bromodichloromethane ND ug/L 06/19/15 03:55 75-27-40.50 1
Bromoform ND ug/L 06/19/15 03:55 75-25-20.50 1
Bromomethane ND ug/L 06/19/15 03:55 74-83-95.0 1
n-Butylbenzene ND ug/L 06/19/15 03:55 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/19/15 03:55 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/19/15 03:55 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/19/15 03:55 56-23-50.50 1
Chlorobenzene ND ug/L 06/19/15 03:55 108-90-70.50 1
Chloroethane ND ug/L 06/19/15 03:55 75-00-31.0 1
Chloroform ND ug/L 06/19/15 03:55 67-66-30.50 1
Chloromethane ND ug/L 06/19/15 03:55 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/19/15 03:55 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/19/15 03:55 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/19/15 03:55 96-12-81.0 1
Dibromochloromethane ND ug/L 06/19/15 03:55 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/19/15 03:55 106-93-40.50 1
Dibromomethane ND ug/L 06/19/15 03:55 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/19/15 03:55 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/19/15 03:55 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/19/15 03:55 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/19/15 03:55 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/19/15 03:55 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/19/15 03:55 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/19/15 03:55 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/19/15 03:55 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/19/15 03:55 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/19/15 03:55 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/19/15 03:55 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/19/15 03:55 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/19/15 03:55 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/19/15 03:55 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/19/15 03:55 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/19/15 03:55 108-20-30.50 1
Ethylbenzene ND ug/L 06/19/15 03:55 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/19/15 03:55 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/19/15 03:55 98-82-80.50 1
Methylene Chloride ND ug/L 06/19/15 03:55 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/19/15 03:55 1634-04-40.50 1
Naphthalene ND ug/L 06/19/15 03:55 91-20-32.0 1
n-Propylbenzene ND ug/L 06/19/15 03:55 103-65-10.50 1
Styrene ND ug/L 06/19/15 03:55 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/19/15 03:55 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/19/15 03:55 79-34-50.50 1
Tetrachloroethene ND ug/L 06/19/15 03:55 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 33
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ANALYTICAL RESULTS
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Sample:MW-3 Lab ID:92254444001 Collected:06/11/15 09:42 Received:06/15/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 06/19/15 03:55 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/19/15 03:55 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/19/15 03:55 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/19/15 03:55 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/19/15 03:55 79-00-50.50 1
Trichloroethene ND ug/L 06/19/15 03:55 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/19/15 03:55 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/19/15 03:55 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/19/15 03:55 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/19/15 03:55 108-67-80.50 1
Vinyl chloride ND ug/L 06/19/15 03:55 75-01-41.0 1
m&p-Xylene ND ug/L 06/19/15 03:55 179601-23-11.0 1
o-Xylene ND ug/L 06/19/15 03:55 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %06/19/15 03:55 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %06/19/15 03:55 460-00-470-130 1
Toluene-d8 (S)101 %06/19/15 03:55 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Sample:MW-5 Lab ID:92254444002 Collected:06/11/15 10:32 Received:06/15/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 06/19/15 01:43 71-43-20.50 1
Bromobenzene ND ug/L 06/19/15 01:43 108-86-10.50 1
Bromochloromethane ND ug/L 06/19/15 01:43 74-97-50.50 1
Bromodichloromethane ND ug/L 06/19/15 01:43 75-27-40.50 1
Bromoform ND ug/L 06/19/15 01:43 75-25-20.50 1
Bromomethane ND ug/L 06/19/15 01:43 74-83-95.0 1
n-Butylbenzene ND ug/L 06/19/15 01:43 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/19/15 01:43 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/19/15 01:43 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/19/15 01:43 56-23-50.50 1
Chlorobenzene ND ug/L 06/19/15 01:43 108-90-70.50 1
Chloroethane ND ug/L 06/19/15 01:43 75-00-31.0 1
Chloroform ND ug/L 06/19/15 01:43 67-66-30.50 1
Chloromethane ND ug/L 06/19/15 01:43 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/19/15 01:43 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/19/15 01:43 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/19/15 01:43 96-12-81.0 1
Dibromochloromethane ND ug/L 06/19/15 01:43 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/19/15 01:43 106-93-40.50 1
Dibromomethane ND ug/L 06/19/15 01:43 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/19/15 01:43 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/19/15 01:43 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/19/15 01:43 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/19/15 01:43 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/19/15 01:43 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/19/15 01:43 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/19/15 01:43 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/19/15 01:43 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/19/15 01:43 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/19/15 01:43 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/19/15 01:43 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/19/15 01:43 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/19/15 01:43 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/19/15 01:43 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/19/15 01:43 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/19/15 01:43 108-20-30.50 1
Ethylbenzene ND ug/L 06/19/15 01:43 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/19/15 01:43 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/19/15 01:43 98-82-80.50 1
Methylene Chloride ND ug/L 06/19/15 01:43 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/19/15 01:43 1634-04-40.50 1
Naphthalene ND ug/L 06/19/15 01:43 91-20-32.0 1
n-Propylbenzene ND ug/L 06/19/15 01:43 103-65-10.50 1
Styrene ND ug/L 06/19/15 01:43 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/19/15 01:43 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/19/15 01:43 79-34-50.50 1
Tetrachloroethene ND ug/L 06/19/15 01:43 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Sample:MW-5 Lab ID:92254444002 Collected:06/11/15 10:32 Received:06/15/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 06/19/15 01:43 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/19/15 01:43 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/19/15 01:43 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/19/15 01:43 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/19/15 01:43 79-00-50.50 1
Trichloroethene ND ug/L 06/19/15 01:43 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/19/15 01:43 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/19/15 01:43 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/19/15 01:43 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/19/15 01:43 108-67-80.50 1
Vinyl chloride ND ug/L 06/19/15 01:43 75-01-41.0 1
m&p-Xylene ND ug/L 06/19/15 01:43 179601-23-11.0 1
o-Xylene ND ug/L 06/19/15 01:43 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %06/19/15 01:43 17060-07-070-130 1
4-Bromofluorobenzene (S)102 %06/19/15 01:43 460-00-470-130 1
Toluene-d8 (S)100 %06/19/15 01:43 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Sample:MW-7 Lab ID:92254444003 Collected:06/12/15 10:48 Received:06/15/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 06/19/15 02:00 71-43-20.50 1
Bromobenzene ND ug/L 06/19/15 02:00 108-86-10.50 1
Bromochloromethane ND ug/L 06/19/15 02:00 74-97-50.50 1
Bromodichloromethane ND ug/L 06/19/15 02:00 75-27-40.50 1
Bromoform ND ug/L 06/19/15 02:00 75-25-20.50 1
Bromomethane ND ug/L 06/19/15 02:00 74-83-95.0 1
n-Butylbenzene ND ug/L 06/19/15 02:00 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/19/15 02:00 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/19/15 02:00 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/19/15 02:00 56-23-50.50 1
Chlorobenzene ND ug/L 06/19/15 02:00 108-90-70.50 1
Chloroethane ND ug/L 06/19/15 02:00 75-00-31.0 1
Chloroform ND ug/L 06/19/15 02:00 67-66-30.50 1
Chloromethane ND ug/L 06/19/15 02:00 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/19/15 02:00 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/19/15 02:00 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/19/15 02:00 96-12-81.0 1
Dibromochloromethane ND ug/L 06/19/15 02:00 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/19/15 02:00 106-93-40.50 1
Dibromomethane ND ug/L 06/19/15 02:00 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/19/15 02:00 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/19/15 02:00 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/19/15 02:00 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/19/15 02:00 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/19/15 02:00 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/19/15 02:00 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/19/15 02:00 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/19/15 02:00 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/19/15 02:00 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/19/15 02:00 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/19/15 02:00 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/19/15 02:00 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/19/15 02:00 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/19/15 02:00 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/19/15 02:00 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/19/15 02:00 108-20-30.50 1
Ethylbenzene ND ug/L 06/19/15 02:00 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/19/15 02:00 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/19/15 02:00 98-82-80.50 1
Methylene Chloride ND ug/L 06/19/15 02:00 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/19/15 02:00 1634-04-40.50 1
Naphthalene ND ug/L 06/19/15 02:00 91-20-32.0 1
n-Propylbenzene ND ug/L 06/19/15 02:00 103-65-10.50 1
Styrene ND ug/L 06/19/15 02:00 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/19/15 02:00 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/19/15 02:00 79-34-50.50 1
Tetrachloroethene ND ug/L 06/19/15 02:00 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Sample:MW-7 Lab ID:92254444003 Collected:06/12/15 10:48 Received:06/15/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 06/19/15 02:00 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/19/15 02:00 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/19/15 02:00 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/19/15 02:00 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/19/15 02:00 79-00-50.50 1
Trichloroethene ND ug/L 06/19/15 02:00 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/19/15 02:00 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/19/15 02:00 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/19/15 02:00 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/19/15 02:00 108-67-80.50 1
Vinyl chloride ND ug/L 06/19/15 02:00 75-01-41.0 1
m&p-Xylene ND ug/L 06/19/15 02:00 179601-23-11.0 1
o-Xylene ND ug/L 06/19/15 02:00 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %06/19/15 02:00 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %06/19/15 02:00 460-00-470-130 1
Toluene-d8 (S)100 %06/19/15 02:00 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Sample:MW-8 Lab ID:92254444004 Collected:06/12/15 10:07 Received:06/15/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 06/19/15 04:12 71-43-20.50 1
Bromobenzene ND ug/L 06/19/15 04:12 108-86-10.50 1
Bromochloromethane ND ug/L 06/19/15 04:12 74-97-50.50 1
Bromodichloromethane ND ug/L 06/19/15 04:12 75-27-40.50 1
Bromoform ND ug/L 06/19/15 04:12 75-25-20.50 1
Bromomethane ND ug/L 06/19/15 04:12 74-83-95.0 1
n-Butylbenzene ND ug/L 06/19/15 04:12 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/19/15 04:12 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/19/15 04:12 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/19/15 04:12 56-23-50.50 1
Chlorobenzene ND ug/L 06/19/15 04:12 108-90-70.50 1
Chloroethane ND ug/L 06/19/15 04:12 75-00-31.0 1
Chloroform ND ug/L 06/19/15 04:12 67-66-30.50 1
Chloromethane ND ug/L 06/19/15 04:12 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/19/15 04:12 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/19/15 04:12 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/19/15 04:12 96-12-81.0 1
Dibromochloromethane ND ug/L 06/19/15 04:12 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/19/15 04:12 106-93-40.50 1
Dibromomethane ND ug/L 06/19/15 04:12 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/19/15 04:12 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/19/15 04:12 541-73-10.50 1
1,4-Dichlorobenzene 0.61 ug/L 06/19/15 04:12 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/19/15 04:12 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/19/15 04:12 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/19/15 04:12 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/19/15 04:12 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/19/15 04:12 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/19/15 04:12 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/19/15 04:12 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/19/15 04:12 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/19/15 04:12 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/19/15 04:12 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/19/15 04:12 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/19/15 04:12 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/19/15 04:12 108-20-30.50 1
Ethylbenzene ND ug/L 06/19/15 04:12 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/19/15 04:12 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/19/15 04:12 98-82-80.50 1
Methylene Chloride ND ug/L 06/19/15 04:12 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/19/15 04:12 1634-04-40.50 1
Naphthalene ND ug/L 06/19/15 04:12 91-20-32.0 1
n-Propylbenzene ND ug/L 06/19/15 04:12 103-65-10.50 1
Styrene ND ug/L 06/19/15 04:12 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/19/15 04:12 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/19/15 04:12 79-34-50.50 1
Tetrachloroethene ND ug/L 06/19/15 04:12 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Sample:MW-8 Lab ID:92254444004 Collected:06/12/15 10:07 Received:06/15/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 06/19/15 04:12 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/19/15 04:12 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/19/15 04:12 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/19/15 04:12 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/19/15 04:12 79-00-50.50 1
Trichloroethene ND ug/L 06/19/15 04:12 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/19/15 04:12 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/19/15 04:12 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/19/15 04:12 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/19/15 04:12 108-67-80.50 1
Vinyl chloride ND ug/L 06/19/15 04:12 75-01-41.0 1
m&p-Xylene ND ug/L 06/19/15 04:12 179601-23-11.0 1
o-Xylene ND ug/L 06/19/15 04:12 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %06/19/15 04:12 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %06/19/15 04:12 460-00-470-130 1
Toluene-d8 (S)99 %06/19/15 04:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Sample:MW-9 Lab ID:92254444005 Collected:06/12/15 09:30 Received:06/15/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 06/19/15 16:38 71-43-20.50 1
Bromobenzene ND ug/L 06/19/15 16:38 108-86-10.50 1
Bromochloromethane ND ug/L 06/19/15 16:38 74-97-50.50 1
Bromodichloromethane ND ug/L 06/19/15 16:38 75-27-40.50 1
Bromoform ND ug/L 06/19/15 16:38 75-25-20.50 1
Bromomethane ND ug/L 06/19/15 16:38 74-83-95.0 1
n-Butylbenzene ND ug/L 06/19/15 16:38 104-51-80.50 1
sec-Butylbenzene 2.1 ug/L 06/19/15 16:38 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/19/15 16:38 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/19/15 16:38 56-23-50.50 1
Chlorobenzene ND ug/L 06/19/15 16:38 108-90-70.50 1
Chloroethane ND ug/L 06/19/15 16:38 75-00-31.0 1
Chloroform ND ug/L 06/19/15 16:38 67-66-30.50 1
Chloromethane ND ug/L 06/19/15 16:38 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/19/15 16:38 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/19/15 16:38 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/19/15 16:38 96-12-81.0 1
Dibromochloromethane ND ug/L 06/19/15 16:38 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/19/15 16:38 106-93-40.50 1
Dibromomethane ND ug/L 06/19/15 16:38 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/19/15 16:38 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/19/15 16:38 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/19/15 16:38 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/19/15 16:38 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/19/15 16:38 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/19/15 16:38 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/19/15 16:38 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/19/15 16:38 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/19/15 16:38 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/19/15 16:38 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/19/15 16:38 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/19/15 16:38 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/19/15 16:38 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/19/15 16:38 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/19/15 16:38 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/19/15 16:38 108-20-30.50 1
Ethylbenzene ND ug/L 06/19/15 16:38 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/19/15 16:38 87-68-32.0 1
Isopropylbenzene (Cumene)1.6 ug/L 06/19/15 16:38 98-82-80.50 1
Methylene Chloride ND ug/L 06/19/15 16:38 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/19/15 16:38 1634-04-40.50 1
Naphthalene 17.1 ug/L 06/19/15 16:38 91-20-32.0 1
n-Propylbenzene 3.3 ug/L 06/19/15 16:38 103-65-10.50 1
Styrene ND ug/L 06/19/15 16:38 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/19/15 16:38 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/19/15 16:38 79-34-50.50 1
Tetrachloroethene ND ug/L 06/19/15 16:38 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Sample:MW-9 Lab ID:92254444005 Collected:06/12/15 09:30 Received:06/15/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 06/19/15 16:38 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/19/15 16:38 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/19/15 16:38 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/19/15 16:38 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/19/15 16:38 79-00-50.50 1
Trichloroethene ND ug/L 06/19/15 16:38 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/19/15 16:38 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/19/15 16:38 96-18-40.50 1
1,2,4-Trimethylbenzene 15.7 ug/L 06/19/15 16:38 95-63-60.50 1
1,3,5-Trimethylbenzene 27.7 ug/L 06/19/15 16:38 108-67-80.50 1
Vinyl chloride ND ug/L 06/19/15 16:38 75-01-41.0 1
m&p-Xylene 1.3 ug/L 06/19/15 16:38 179601-23-11.0 1
o-Xylene 2.4 ug/L 06/19/15 16:38 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %06/19/15 16:38 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %06/19/15 16:38 460-00-470-130 1
Toluene-d8 (S)101 %06/19/15 16:38 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Sample:MW-10 Lab ID:92254444006 Collected:06/12/15 08:53 Received:06/15/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 06/19/15 04:29 71-43-20.50 1
Bromobenzene ND ug/L 06/19/15 04:29 108-86-10.50 1
Bromochloromethane ND ug/L 06/19/15 04:29 74-97-50.50 1
Bromodichloromethane ND ug/L 06/19/15 04:29 75-27-40.50 1
Bromoform ND ug/L 06/19/15 04:29 75-25-20.50 1
Bromomethane ND ug/L 06/19/15 04:29 74-83-95.0 1
n-Butylbenzene ND ug/L 06/19/15 04:29 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/19/15 04:29 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/19/15 04:29 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/19/15 04:29 56-23-50.50 1
Chlorobenzene ND ug/L 06/19/15 04:29 108-90-70.50 1
Chloroethane ND ug/L 06/19/15 04:29 75-00-31.0 1
Chloroform ND ug/L 06/19/15 04:29 67-66-30.50 1
Chloromethane ND ug/L 06/19/15 04:29 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/19/15 04:29 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/19/15 04:29 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/19/15 04:29 96-12-81.0 1
Dibromochloromethane ND ug/L 06/19/15 04:29 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/19/15 04:29 106-93-40.50 1
Dibromomethane ND ug/L 06/19/15 04:29 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/19/15 04:29 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/19/15 04:29 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/19/15 04:29 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/19/15 04:29 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/19/15 04:29 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/19/15 04:29 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/19/15 04:29 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/19/15 04:29 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/19/15 04:29 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/19/15 04:29 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/19/15 04:29 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/19/15 04:29 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/19/15 04:29 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/19/15 04:29 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/19/15 04:29 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/19/15 04:29 108-20-30.50 1
Ethylbenzene ND ug/L 06/19/15 04:29 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/19/15 04:29 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/19/15 04:29 98-82-80.50 1
Methylene Chloride ND ug/L 06/19/15 04:29 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/19/15 04:29 1634-04-40.50 1
Naphthalene ND ug/L 06/19/15 04:29 91-20-32.0 1
n-Propylbenzene ND ug/L 06/19/15 04:29 103-65-10.50 1
Styrene ND ug/L 06/19/15 04:29 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/19/15 04:29 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/19/15 04:29 79-34-50.50 1
Tetrachloroethene ND ug/L 06/19/15 04:29 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Sample:MW-10 Lab ID:92254444006 Collected:06/12/15 08:53 Received:06/15/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 06/19/15 04:29 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/19/15 04:29 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/19/15 04:29 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/19/15 04:29 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/19/15 04:29 79-00-50.50 1
Trichloroethene ND ug/L 06/19/15 04:29 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/19/15 04:29 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/19/15 04:29 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/19/15 04:29 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/19/15 04:29 108-67-80.50 1
Vinyl chloride ND ug/L 06/19/15 04:29 75-01-41.0 1
m&p-Xylene ND ug/L 06/19/15 04:29 179601-23-11.0 1
o-Xylene ND ug/L 06/19/15 04:29 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %06/19/15 04:29 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %06/19/15 04:29 460-00-470-130 1
Toluene-d8 (S)100 %06/19/15 04:29 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Sample:WSW-5 Lab ID:92254444007 Collected:06/11/15 14:10 Received:06/15/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 06/19/15 02:16 71-43-20.50 1
Bromobenzene ND ug/L 06/19/15 02:16 108-86-10.50 1
Bromochloromethane ND ug/L 06/19/15 02:16 74-97-50.50 1
Bromodichloromethane ND ug/L 06/19/15 02:16 75-27-40.50 1
Bromoform ND ug/L 06/19/15 02:16 75-25-20.50 1
Bromomethane ND ug/L 06/19/15 02:16 74-83-95.0 1
n-Butylbenzene ND ug/L 06/19/15 02:16 104-51-80.50 1
sec-Butylbenzene ND ug/L 06/19/15 02:16 135-98-80.50 1
tert-Butylbenzene ND ug/L 06/19/15 02:16 98-06-60.50 1
Carbon tetrachloride ND ug/L 06/19/15 02:16 56-23-50.50 1
Chlorobenzene ND ug/L 06/19/15 02:16 108-90-70.50 1
Chloroethane ND ug/L 06/19/15 02:16 75-00-31.0 1
Chloroform ND ug/L 06/19/15 02:16 67-66-30.50 1
Chloromethane ND ug/L 06/19/15 02:16 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/19/15 02:16 95-49-80.50 1
4-Chlorotoluene ND ug/L 06/19/15 02:16 106-43-40.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/19/15 02:16 96-12-81.0 1
Dibromochloromethane ND ug/L 06/19/15 02:16 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/19/15 02:16 106-93-40.50 1
Dibromomethane ND ug/L 06/19/15 02:16 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/19/15 02:16 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/19/15 02:16 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/19/15 02:16 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/19/15 02:16 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/19/15 02:16 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/19/15 02:16 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/19/15 02:16 75-35-40.50 1
cis-1,2-Dichloroethene ND ug/L 06/19/15 02:16 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/19/15 02:16 156-60-50.50 1
1,2-Dichloropropane 2.1 ug/L 06/19/15 02:16 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/19/15 02:16 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/19/15 02:16 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/19/15 02:16 563-58-60.50 1
cis-1,3-Dichloropropene ND ug/L 06/19/15 02:16 10061-01-50.50 1
trans-1,3-Dichloropropene ND ug/L 06/19/15 02:16 10061-02-60.50 1
Diisopropyl ether ND ug/L 06/19/15 02:16 108-20-30.50 1
Ethylbenzene ND ug/L 06/19/15 02:16 100-41-40.50 1
Hexachloro-1,3-butadiene ND ug/L 06/19/15 02:16 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/19/15 02:16 98-82-80.50 1
Methylene Chloride ND ug/L 06/19/15 02:16 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/19/15 02:16 1634-04-40.50 1
Naphthalene ND ug/L 06/19/15 02:16 91-20-32.0 1
n-Propylbenzene ND ug/L 06/19/15 02:16 103-65-10.50 1
Styrene ND ug/L 06/19/15 02:16 100-42-50.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/19/15 02:16 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/19/15 02:16 79-34-50.50 1
Tetrachloroethene ND ug/L 06/19/15 02:16 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
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Page 16 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Sample:WSW-5 Lab ID:92254444007 Collected:06/11/15 14:10 Received:06/15/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 06/19/15 02:16 108-88-30.50 1
1,2,3-Trichlorobenzene ND ug/L 06/19/15 02:16 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/19/15 02:16 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/19/15 02:16 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/19/15 02:16 79-00-50.50 1
Trichloroethene ND ug/L 06/19/15 02:16 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/19/15 02:16 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/19/15 02:16 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/19/15 02:16 95-63-60.50 1
1,3,5-Trimethylbenzene ND ug/L 06/19/15 02:16 108-67-80.50 1
Vinyl chloride ND ug/L 06/19/15 02:16 75-01-41.0 1
m&p-Xylene ND ug/L 06/19/15 02:16 179601-23-11.0 1
o-Xylene ND ug/L 06/19/15 02:16 95-47-60.50 1
Surrogates
1,2-Dichloroethane-d4 (S)100 %06/19/15 02:16 17060-07-070-130 1
4-Bromofluorobenzene (S)101 %06/19/15 02:16 460-00-470-130 1
Toluene-d8 (S)101 %06/19/15 02:16 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
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Page 17 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Sample:WSW-4 Lab ID:92254444008 Collected:06/11/15 15:15 Received:06/15/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 06/19/15 02:33 71-43-20.50 1
Bromobenzene ND ug/L 06/19/15 02:33 108-86-10.50 1
Bromochloromethane ND ug/L 06/19/15 02:33 74-97-50.50 1
Bromodichloromethane 12.4 ug/L 06/19/15 02:33 75-27-40.50 1
Bromoform ND ug/L 06/19/15 02:33 75-25-20.50 1
Bromomethane ND ug/L 06/19/15 02:33 74-83-9 M15.0 1
n-Butylbenzene ND ug/L 06/19/15 02:33 104-51-8 M1,R10.50 1
sec-Butylbenzene ND ug/L 06/19/15 02:33 135-98-8 M1,R10.50 1
tert-Butylbenzene ND ug/L 06/19/15 02:33 98-06-6 M10.50 1
Carbon tetrachloride ND ug/L 06/19/15 02:33 56-23-50.50 1
Chlorobenzene ND ug/L 06/19/15 02:33 108-90-70.50 1
Chloroethane ND ug/L 06/19/15 02:33 75-00-31.0 1
Chloroform 24.1 ug/L 06/19/15 02:33 67-66-30.50 1
Chloromethane ND ug/L 06/19/15 02:33 74-87-31.0 1
2-Chlorotoluene ND ug/L 06/19/15 02:33 95-49-8 M10.50 1
4-Chlorotoluene ND ug/L 06/19/15 02:33 106-43-4 M10.50 1
1,2-Dibromo-3-chloropropane ND ug/L 06/19/15 02:33 96-12-81.0 1
Dibromochloromethane 4.6 ug/L 06/19/15 02:33 124-48-10.50 1
1,2-Dibromoethane (EDB)ND ug/L 06/19/15 02:33 106-93-40.50 1
Dibromomethane ND ug/L 06/19/15 02:33 74-95-30.50 1
1,2-Dichlorobenzene ND ug/L 06/19/15 02:33 95-50-10.50 1
1,3-Dichlorobenzene ND ug/L 06/19/15 02:33 541-73-10.50 1
1,4-Dichlorobenzene ND ug/L 06/19/15 02:33 106-46-70.50 1
Dichlorodifluoromethane ND ug/L 06/19/15 02:33 75-71-80.50 1
1,1-Dichloroethane ND ug/L 06/19/15 02:33 75-34-30.50 1
1,2-Dichloroethane ND ug/L 06/19/15 02:33 107-06-20.50 1
1,1-Dichloroethene ND ug/L 06/19/15 02:33 75-35-4 M10.50 1
cis-1,2-Dichloroethene ND ug/L 06/19/15 02:33 156-59-20.50 1
trans-1,2-Dichloroethene ND ug/L 06/19/15 02:33 156-60-50.50 1
1,2-Dichloropropane ND ug/L 06/19/15 02:33 78-87-50.50 1
1,3-Dichloropropane ND ug/L 06/19/15 02:33 142-28-90.50 1
2,2-Dichloropropane ND ug/L 06/19/15 02:33 594-20-70.50 1
1,1-Dichloropropene ND ug/L 06/19/15 02:33 563-58-6 M10.50 1
cis-1,3-Dichloropropene ND ug/L 06/19/15 02:33 10061-01-5 M10.50 1
trans-1,3-Dichloropropene ND ug/L 06/19/15 02:33 10061-02-6 M10.50 1
Diisopropyl ether ND ug/L 06/19/15 02:33 108-20-30.50 1
Ethylbenzene ND ug/L 06/19/15 02:33 100-41-4 M1,R10.50 1
Hexachloro-1,3-butadiene ND ug/L 06/19/15 02:33 87-68-32.0 1
Isopropylbenzene (Cumene)ND ug/L 06/19/15 02:33 98-82-8 M1,R10.50 1
Methylene Chloride ND ug/L 06/19/15 02:33 75-09-22.0 1
Methyl-tert-butyl ether ND ug/L 06/19/15 02:33 1634-04-40.50 1
Naphthalene ND ug/L 06/19/15 02:33 91-20-3 M12.0 1
n-Propylbenzene ND ug/L 06/19/15 02:33 103-65-1 M1,R10.50 1
Styrene ND ug/L 06/19/15 02:33 100-42-5 M10.50 1
1,1,1,2-Tetrachloroethane ND ug/L 06/19/15 02:33 630-20-60.50 1
1,1,2,2-Tetrachloroethane ND ug/L 06/19/15 02:33 79-34-50.50 1
Tetrachloroethene ND ug/L 06/19/15 02:33 127-18-40.50 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
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Page 18 of 33
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Sample:WSW-4 Lab ID:92254444008 Collected:06/11/15 15:15 Received:06/15/15 15:30 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: SM 6200B6200B MSV
Toluene ND ug/L 06/19/15 02:33 108-88-3 M1,R10.50 1
1,2,3-Trichlorobenzene ND ug/L 06/19/15 02:33 87-61-62.0 1
1,2,4-Trichlorobenzene ND ug/L 06/19/15 02:33 120-82-12.0 1
1,1,1-Trichloroethane ND ug/L 06/19/15 02:33 71-55-60.50 1
1,1,2-Trichloroethane ND ug/L 06/19/15 02:33 79-00-50.50 1
Trichloroethene ND ug/L 06/19/15 02:33 79-01-60.50 1
Trichlorofluoromethane ND ug/L 06/19/15 02:33 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 06/19/15 02:33 96-18-40.50 1
1,2,4-Trimethylbenzene ND ug/L 06/19/15 02:33 95-63-6 M10.50 1
1,3,5-Trimethylbenzene ND ug/L 06/19/15 02:33 108-67-8 M10.50 1
Vinyl chloride ND ug/L 06/19/15 02:33 75-01-4 M11.0 1
m&p-Xylene ND ug/L 06/19/15 02:33 179601-23-1 M11.0 1
o-Xylene ND ug/L 06/19/15 02:33 95-47-6 M10.50 1
Surrogates
1,2-Dichloroethane-d4 (S)99 %06/19/15 02:33 17060-07-070-130 1
4-Bromofluorobenzene (S)100 %06/19/15 02:33 460-00-470-130 1
Toluene-d8 (S)100 %06/19/15 02:33 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/32214
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92254444001, 92254444002, 92254444003, 92254444004, 92254444006, 92254444007, 92254444008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1488780
Associated Lab Samples:92254444001, 92254444002, 92254444003, 92254444004, 92254444006, 92254444007, 92254444008
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 06/18/15 23:14
1,1,1-Trichloroethane ug/L ND 0.50 06/18/15 23:14
1,1,2,2-Tetrachloroethane ug/L ND 0.50 06/18/15 23:14
1,1,2-Trichloroethane ug/L ND 0.50 06/18/15 23:14
1,1-Dichloroethane ug/L ND 0.50 06/18/15 23:14
1,1-Dichloroethene ug/L ND 0.50 06/18/15 23:14
1,1-Dichloropropene ug/L ND 0.50 06/18/15 23:14
1,2,3-Trichlorobenzene ug/L ND 2.0 06/18/15 23:14
1,2,3-Trichloropropane ug/L ND 0.50 06/18/15 23:14
1,2,4-Trichlorobenzene ug/L ND 2.0 06/18/15 23:14
1,2,4-Trimethylbenzene ug/L ND 0.50 06/18/15 23:14
1,2-Dibromo-3-chloropropane ug/L ND 1.0 06/18/15 23:14
1,2-Dibromoethane (EDB)ug/L ND 0.50 06/18/15 23:14
1,2-Dichlorobenzene ug/L ND 0.50 06/18/15 23:14
1,2-Dichloroethane ug/L ND 0.50 06/18/15 23:14
1,2-Dichloropropane ug/L ND 0.50 06/18/15 23:14
1,3,5-Trimethylbenzene ug/L ND 0.50 06/18/15 23:14
1,3-Dichlorobenzene ug/L ND 0.50 06/18/15 23:14
1,3-Dichloropropane ug/L ND 0.50 06/18/15 23:14
1,4-Dichlorobenzene ug/L ND 0.50 06/18/15 23:14
2,2-Dichloropropane ug/L ND 0.50 06/18/15 23:14
2-Chlorotoluene ug/L ND 0.50 06/18/15 23:14
4-Chlorotoluene ug/L ND 0.50 06/18/15 23:14
Benzene ug/L ND 0.50 06/18/15 23:14
Bromobenzene ug/L ND 0.50 06/18/15 23:14
Bromochloromethane ug/L ND 0.50 06/18/15 23:14
Bromodichloromethane ug/L ND 0.50 06/18/15 23:14
Bromoform ug/L ND 0.50 06/18/15 23:14
Bromomethane ug/L ND 5.0 06/18/15 23:14
Carbon tetrachloride ug/L ND 0.50 06/18/15 23:14
Chlorobenzene ug/L ND 0.50 06/18/15 23:14
Chloroethane ug/L ND 1.0 06/18/15 23:14
Chloroform ug/L ND 0.50 06/18/15 23:14
Chloromethane ug/L ND 1.0 06/18/15 23:14
cis-1,2-Dichloroethene ug/L ND 0.50 06/18/15 23:14
cis-1,3-Dichloropropene ug/L ND 0.50 06/18/15 23:14
Dibromochloromethane ug/L ND 0.50 06/18/15 23:14
Dibromomethane ug/L ND 0.50 06/18/15 23:14
Dichlorodifluoromethane ug/L ND 0.50 06/18/15 23:14
Diisopropyl ether ug/L ND 0.50 06/18/15 23:14
Ethylbenzene ug/L ND 0.50 06/18/15 23:14
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1488780
Associated Lab Samples:92254444001, 92254444002, 92254444003, 92254444004, 92254444006, 92254444007, 92254444008
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 06/18/15 23:14
Isopropylbenzene (Cumene)ug/L ND 0.50 06/18/15 23:14
m&p-Xylene ug/L ND 1.0 06/18/15 23:14
Methyl-tert-butyl ether ug/L ND 0.50 06/18/15 23:14
Methylene Chloride ug/L ND 2.0 06/18/15 23:14
n-Butylbenzene ug/L ND 0.50 06/18/15 23:14
n-Propylbenzene ug/L ND 0.50 06/18/15 23:14
Naphthalene ug/L ND 2.0 06/18/15 23:14
o-Xylene ug/L ND 0.50 06/18/15 23:14
sec-Butylbenzene ug/L ND 0.50 06/18/15 23:14
Styrene ug/L ND 0.50 06/18/15 23:14
tert-Butylbenzene ug/L ND 0.50 06/18/15 23:14
Tetrachloroethene ug/L ND 0.50 06/18/15 23:14
Toluene ug/L ND 0.50 06/18/15 23:14
trans-1,2-Dichloroethene ug/L ND 0.50 06/18/15 23:14
trans-1,3-Dichloropropene ug/L ND 0.50 06/18/15 23:14
Trichloroethene ug/L ND 0.50 06/18/15 23:14
Trichlorofluoromethane ug/L ND 1.0 06/18/15 23:14
Vinyl chloride ug/L ND 1.0 06/18/15 23:14
1,2-Dichloroethane-d4 (S)%98 70-130 06/18/15 23:14
4-Bromofluorobenzene (S)%100 70-130 06/18/15 23:14
Toluene-d8 (S)%101 70-130 06/18/15 23:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1488781LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.650 103 60-140
1,1,1-Trichloroethane ug/L 52.850 106 60-140
1,1,2,2-Tetrachloroethane ug/L 53.150 106 60-140
1,1,2-Trichloroethane ug/L 50.750 101 60-140
1,1-Dichloroethane ug/L 52.050 104 60-140
1,1-Dichloroethene ug/L 56.750 113 60-140
1,1-Dichloropropene ug/L 55.250 110 60-140
1,2,3-Trichlorobenzene ug/L 53.250 106 60-140
1,2,3-Trichloropropane ug/L 51.450 103 60-140
1,2,4-Trichlorobenzene ug/L 52.850 106 60-140
1,2,4-Trimethylbenzene ug/L 54.250 108 60-140
1,2-Dibromo-3-chloropropane ug/L 54.050 108 60-140
1,2-Dibromoethane (EDB)ug/L 54.050 108 60-140
1,2-Dichlorobenzene ug/L 54.750 109 60-140
1,2-Dichloroethane ug/L 49.650 99 60-140
1,2-Dichloropropane ug/L 50.850 102 60-140
1,3,5-Trimethylbenzene ug/L 55.350 111 60-140
1,3-Dichlorobenzene ug/L 53.850 108 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1488781LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 52.150 104 60-140
1,4-Dichlorobenzene ug/L 52.850 106 60-140
2,2-Dichloropropane ug/L 45.150 90 60-140
2-Chlorotoluene ug/L 55.350 111 60-140
4-Chlorotoluene ug/L 54.050 108 60-140
Benzene ug/L 53.450 107 60-140
Bromobenzene ug/L 51.150 102 60-140
Bromochloromethane ug/L 56.050 112 60-140
Bromodichloromethane ug/L 52.150 104 60-140
Bromoform ug/L 47.450 95 60-140
Bromomethane ug/L 37.750 75 60-140
Carbon tetrachloride ug/L 53.850 108 60-140
Chlorobenzene ug/L 52.650 105 60-140
Chloroethane ug/L 48.850 98 60-140
Chloroform ug/L 52.850 106 60-140
Chloromethane ug/L 44.750 89 60-140
cis-1,2-Dichloroethene ug/L 52.350 105 60-140
cis-1,3-Dichloropropene ug/L 51.050 102 60-140
Dibromochloromethane ug/L 51.850 104 60-140
Dibromomethane ug/L 52.850 106 60-140
Dichlorodifluoromethane ug/L 51.850 104 60-140
Diisopropyl ether ug/L 52.050 104 60-140
Ethylbenzene ug/L 52.150 104 60-140
Hexachloro-1,3-butadiene ug/L 60.350 121 60-140
Isopropylbenzene (Cumene)ug/L 57.450 115 60-140
m&p-Xylene ug/L 103100 103 60-140
Methyl-tert-butyl ether ug/L 48.750 97 60-140
Methylene Chloride ug/L 51.350 103 60-140
n-Butylbenzene ug/L 54.250 108 60-140
n-Propylbenzene ug/L 54.550 109 60-140
Naphthalene ug/L 56.250 112 60-140
o-Xylene ug/L 52.750 105 60-140
sec-Butylbenzene ug/L 56.750 113 60-140
Styrene ug/L 54.650 109 60-140
tert-Butylbenzene ug/L 45.950 92 60-140
Tetrachloroethene ug/L 50.950 102 60-140
Toluene ug/L 50.550 101 60-140
trans-1,2-Dichloroethene ug/L 52.950 106 60-140
trans-1,3-Dichloropropene ug/L 50.950 102 60-140
Trichloroethene ug/L 50.350 101 60-140
Trichlorofluoromethane ug/L 47.350 95 60-140
Vinyl chloride ug/L 48.850 98 60-140
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1488782MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92254444008
1488783
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 109 60-140111 220ND21.7 22.1
1,1,1-Trichloroethane ug/L 20 118 60-140121 220ND23.6 24.2
1,1,2,2-Tetrachloroethane ug/L 20 113 60-140115 220ND22.5 22.9
1,1,2-Trichloroethane ug/L 20 108 60-140109 220ND21.5 21.9
1,1-Dichloroethane ug/L 20 114 60-140115 120ND22.7 23.0
1,1-Dichloroethene ug/L M1205060-14064 2520ND9.9 12.8
1,1-Dichloropropene ug/L M120060-140220NDND.38J
1,2,3-Trichlorobenzene ug/L 20 108 60-140116 720ND21.6 23.3
1,2,3-Trichloropropane ug/L 20 116 60-140117 120ND23.2 23.4
1,2,4-Trichlorobenzene ug/L 20 106 60-140114 720ND21.3 22.8
1,2,4-Trimethylbenzene ug/L M120060-140020NDNDND
1,2-Dibromo-3-chloropropane ug/L 20 106 60-140109 220ND21.3 21.8
1,2-Dibromoethane (EDB)ug/L 20 116 60-140117 120ND23.2 23.5
1,2-Dichlorobenzene ug/L 20 116 60-140121 420ND23.2 24.2
1,2-Dichloroethane ug/L 20 107 60-140110 320ND21.4 22.0
1,2-Dichloropropane ug/L 20 113 60-140115 220ND22.5 23.0
1,3,5-Trimethylbenzene ug/L M120060-140020NDNDND
1,3-Dichlorobenzene ug/L 20 115 60-140120 420ND23.1 24.1
1,3-Dichloropropane ug/L 20 112 60-140115 320ND22.5 23.1
1,4-Dichlorobenzene ug/L 20 113 60-140120 520ND22.7 23.9
2,2-Dichloropropane ug/L 20 94 60-14095 220ND18.7 19.0
2-Chlorotoluene ug/L M12022060-140226 320ND44.1 45.2
4-Chlorotoluene ug/L M12016060-140165 320ND32.0 33.0
Benzene ug/L 20 118 60-140122 420ND23.6 24.5
Bromobenzene ug/L 20 101 60-140107 520ND20.2 21.3
Bromochloromethane ug/L 20 123 60-140126 220ND24.7 25.3
Bromodichloromethane ug/L 20 119 60-140124 32012.4 36.2 37.2
Bromoform ug/L 20 89 60-14090 220ND17.8 18.1
Bromomethane ug/L M1204260-14052 2120ND8.4 10.4
Carbon tetrachloride ug/L 20 117 60-140121 320ND23.3 24.1
Chlorobenzene ug/L 20 119 60-140122 320ND23.7 24.4
Chloroethane ug/L 20 112 60-140111 120ND22.4 22.2
Chloroform ug/L 20 122 60-140123 12024.1 48.4 48.8
Chloromethane ug/L 20 126 60-140133 520ND25.1 26.5
cis-1,2-Dichloroethene ug/L 20 116 60-140120 420ND23.2 24.0
cis-1,3-Dichloropropene ug/L M1203660-14047 2620ND7.2 9.3
Dibromochloromethane ug/L 20 105 60-140114 6204.6 25.6 27.3
Dibromomethane ug/L 20 115 60-140117 220ND22.9 23.4
Dichlorodifluoromethane ug/L 20 117 60-140120 320ND23.4 24.0
Diisopropyl ether ug/L 20 114 60-140115 120ND22.8 23.0
Ethylbenzene ug/L M1,R1201360-14022 5120ND2.5 4.3
Hexachloro-1,3-butadiene ug/L 20 135 60-140135 020ND26.9 27.0
Isopropylbenzene (Cumene)ug/L M1,R1202660-14038 3620ND5.2 7.6
m&p-Xylene ug/L M140060-140040NDNDND
Methyl-tert-butyl ether ug/L 20 105 60-140107 220ND20.9 21.4
Methylene Chloride ug/L 20 109 60-140120 1020ND21.7 24.1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
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Page 23 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1488782MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92254444008
1488783
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L M1,R1201160-14019 5420ND2.2 3.9
n-Propylbenzene ug/L M1,R1201460-14023 5020ND2.8 4.6
Naphthalene ug/L M120060-140020NDNDND
o-Xylene ug/L M120060-140020NDNDND
sec-Butylbenzene ug/L M1,R1202460-14036 4020ND4.8 7.2
Styrene ug/L M120060-140020NDNDND
tert-Butylbenzene ug/L M1203860-14050 2820ND7.6 10.1
Tetrachloroethene ug/L 20 116 60-140120 320ND23.2 23.9
Toluene ug/L M1,R120860-14014 5920ND1.5 2.8
trans-1,2-Dichloroethene ug/L 20 120 60-140122 220ND24.1 24.5
trans-1,3-Dichloropropene ug/L M1203760-14048 2720ND7.4 9.7
Trichloroethene ug/L 20 118 60-140120 120ND23.6 24.0
Trichlorofluoromethane ug/L 20 109 60-140110 220ND21.7 22.1
Vinyl chloride ug/L M120060-140020NDNDND
1,2-Dichloroethane-d4 (S)%98 70-13097
4-Bromofluorobenzene (S)%101 70-130100
Toluene-d8 (S)%99 70-130101
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
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Page 24 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
MSV/32225
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92254444005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1489896
Associated Lab Samples:92254444005
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 0.50 06/19/15 16:21
1,1,1-Trichloroethane ug/L ND 0.50 06/19/15 16:21
1,1,2,2-Tetrachloroethane ug/L ND 0.50 06/19/15 16:21
1,1,2-Trichloroethane ug/L ND 0.50 06/19/15 16:21
1,1-Dichloroethane ug/L ND 0.50 06/19/15 16:21
1,1-Dichloroethene ug/L ND 0.50 06/19/15 16:21
1,1-Dichloropropene ug/L ND 0.50 06/19/15 16:21
1,2,3-Trichlorobenzene ug/L ND 2.0 06/19/15 16:21
1,2,3-Trichloropropane ug/L ND 0.50 06/19/15 16:21
1,2,4-Trichlorobenzene ug/L ND 2.0 06/19/15 16:21
1,2,4-Trimethylbenzene ug/L ND 0.50 06/19/15 16:21
1,2-Dibromo-3-chloropropane ug/L ND 1.0 06/19/15 16:21
1,2-Dibromoethane (EDB)ug/L ND 0.50 06/19/15 16:21
1,2-Dichlorobenzene ug/L ND 0.50 06/19/15 16:21
1,2-Dichloroethane ug/L ND 0.50 06/19/15 16:21
1,2-Dichloropropane ug/L ND 0.50 06/19/15 16:21
1,3,5-Trimethylbenzene ug/L ND 0.50 06/19/15 16:21
1,3-Dichlorobenzene ug/L ND 0.50 06/19/15 16:21
1,3-Dichloropropane ug/L ND 0.50 06/19/15 16:21
1,4-Dichlorobenzene ug/L ND 0.50 06/19/15 16:21
2,2-Dichloropropane ug/L ND 0.50 06/19/15 16:21
2-Chlorotoluene ug/L ND 0.50 06/19/15 16:21
4-Chlorotoluene ug/L ND 0.50 06/19/15 16:21
Benzene ug/L ND 0.50 06/19/15 16:21
Bromobenzene ug/L ND 0.50 06/19/15 16:21
Bromochloromethane ug/L ND 0.50 06/19/15 16:21
Bromodichloromethane ug/L ND 0.50 06/19/15 16:21
Bromoform ug/L ND 0.50 06/19/15 16:21
Bromomethane ug/L ND 5.0 06/19/15 16:21
Carbon tetrachloride ug/L ND 0.50 06/19/15 16:21
Chlorobenzene ug/L ND 0.50 06/19/15 16:21
Chloroethane ug/L ND 1.0 06/19/15 16:21
Chloroform ug/L ND 0.50 06/19/15 16:21
Chloromethane ug/L ND 1.0 06/19/15 16:21
cis-1,2-Dichloroethene ug/L ND 0.50 06/19/15 16:21
cis-1,3-Dichloropropene ug/L ND 0.50 06/19/15 16:21
Dibromochloromethane ug/L ND 0.50 06/19/15 16:21
Dibromomethane ug/L ND 0.50 06/19/15 16:21
Dichlorodifluoromethane ug/L ND 0.50 06/19/15 16:21
Diisopropyl ether ug/L ND 0.50 06/19/15 16:21
Ethylbenzene ug/L ND 0.50 06/19/15 16:21
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
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Page 25 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:1489896
Associated Lab Samples:92254444005
Matrix:Water
Analyzed
Hexachloro-1,3-butadiene ug/L ND 2.0 06/19/15 16:21
Isopropylbenzene (Cumene)ug/L ND 0.50 06/19/15 16:21
m&p-Xylene ug/L ND 1.0 06/19/15 16:21
Methyl-tert-butyl ether ug/L ND 0.50 06/19/15 16:21
Methylene Chloride ug/L ND 2.0 06/19/15 16:21
n-Butylbenzene ug/L ND 0.50 06/19/15 16:21
n-Propylbenzene ug/L ND 0.50 06/19/15 16:21
Naphthalene ug/L ND 2.0 06/19/15 16:21
o-Xylene ug/L ND 0.50 06/19/15 16:21
sec-Butylbenzene ug/L ND 0.50 06/19/15 16:21
Styrene ug/L ND 0.50 06/19/15 16:21
tert-Butylbenzene ug/L ND 0.50 06/19/15 16:21
Tetrachloroethene ug/L ND 0.50 06/19/15 16:21
Toluene ug/L ND 0.50 06/19/15 16:21
trans-1,2-Dichloroethene ug/L ND 0.50 06/19/15 16:21
trans-1,3-Dichloropropene ug/L ND 0.50 06/19/15 16:21
Trichloroethene ug/L ND 0.50 06/19/15 16:21
Trichlorofluoromethane ug/L ND 1.0 06/19/15 16:21
Vinyl chloride ug/L ND 1.0 06/19/15 16:21
1,2-Dichloroethane-d4 (S)%99 70-130 06/19/15 16:21
4-Bromofluorobenzene (S)%101 70-130 06/19/15 16:21
Toluene-d8 (S)%99 70-130 06/19/15 16:21
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1489897LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.550 103 60-140
1,1,1-Trichloroethane ug/L 54.350 109 60-140
1,1,2,2-Tetrachloroethane ug/L 52.450 105 60-140
1,1,2-Trichloroethane ug/L 50.750 101 60-140
1,1-Dichloroethane ug/L 54.050 108 60-140
1,1-Dichloroethene ug/L 58.050 116 60-140
1,1-Dichloropropene ug/L 57.550 115 60-140
1,2,3-Trichlorobenzene ug/L 52.150 104 60-140
1,2,3-Trichloropropane ug/L 52.350 105 60-140
1,2,4-Trichlorobenzene ug/L 52.150 104 60-140
1,2,4-Trimethylbenzene ug/L 55.350 111 60-140
1,2-Dibromo-3-chloropropane ug/L 52.050 104 60-140
1,2-Dibromoethane (EDB)ug/L 54.250 108 60-140
1,2-Dichlorobenzene ug/L 54.350 109 60-140
1,2-Dichloroethane ug/L 49.950 100 60-140
1,2-Dichloropropane ug/L 52.250 104 60-140
1,3,5-Trimethylbenzene ug/L 55.750 111 60-140
1,3-Dichlorobenzene ug/L 54.150 108 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
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Huntersville, NC 28078
[phone]
Page 26 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
1489897LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 52.250 104 60-140
1,4-Dichlorobenzene ug/L 53.150 106 60-140
2,2-Dichloropropane ug/L 55.250 110 60-140
2-Chlorotoluene ug/L 54.550 109 60-140
4-Chlorotoluene ug/L 55.050 110 60-140
Benzene ug/L 54.750 109 60-140
Bromobenzene ug/L 54.450 109 60-140
Bromochloromethane ug/L 57.550 115 60-140
Bromodichloromethane ug/L 52.950 106 60-140
Bromoform ug/L 47.750 95 60-140
Bromomethane ug/L 39.050 78 60-140
Carbon tetrachloride ug/L 54.950 110 60-140
Chlorobenzene ug/L 53.150 106 60-140
Chloroethane ug/L 47.850 96 60-140
Chloroform ug/L 54.250 108 60-140
Chloromethane ug/L 40.850 82 60-140
cis-1,2-Dichloroethene ug/L 54.550 109 60-140
cis-1,3-Dichloropropene ug/L 51.850 104 60-140
Dibromochloromethane ug/L 51.250 102 60-140
Dibromomethane ug/L 52.750 105 60-140
Dichlorodifluoromethane ug/L 50.150 100 60-140
Diisopropyl ether ug/L 52.750 105 60-140
Ethylbenzene ug/L 52.650 105 60-140
Hexachloro-1,3-butadiene ug/L 58.850 118 60-140
Isopropylbenzene (Cumene)ug/L 58.750 117 60-140
m&p-Xylene ug/L 105100 105 60-140
Methyl-tert-butyl ether ug/L 49.550 99 60-140
Methylene Chloride ug/L 50.550 101 60-140
n-Butylbenzene ug/L 55.350 111 60-140
n-Propylbenzene ug/L 55.650 111 60-140
Naphthalene ug/L 54.350 109 60-140
o-Xylene ug/L 53.650 107 60-140
sec-Butylbenzene ug/L 56.850 114 60-140
Styrene ug/L 55.250 110 60-140
tert-Butylbenzene ug/L 45.650 91 60-140
Tetrachloroethene ug/L 52.550 105 60-140
Toluene ug/L 52.550 105 60-140
trans-1,2-Dichloroethene ug/L 55.650 111 60-140
trans-1,3-Dichloropropene ug/L 52.350 105 60-140
Trichloroethene ug/L 51.850 104 60-140
Trichlorofluoromethane ug/L 48.150 96 60-140
Vinyl chloride ug/L 49.350 99 60-140
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
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Huntersville, NC 28078
[phone]
Page 27 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1489898MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92253831006
1489899
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 106 60-140113 620ND21.3 22.7
1,1,1-Trichloroethane ug/L 20 117 60-140122 420ND23.4 24.3
1,1,2,2-Tetrachloroethane ug/L 20 113 60-140115 220ND22.6 23.1
1,1,2-Trichloroethane ug/L 20 108 60-140110 220ND21.6 22.1
1,1-Dichloroethane ug/L 20 116 60-140122 520ND23.2 24.4
1,1-Dichloroethene ug/L 20 131 60-140134 220ND26.2 26.8
1,1-Dichloropropene ug/L 20 127 60-140129 220ND25.4 25.8
1,2,3-Trichlorobenzene ug/L 20 106 60-140109 320ND21.3 21.8
1,2,3-Trichloropropane ug/L 20 115 60-140115 020ND22.9 22.9
1,2,4-Trichlorobenzene ug/L 20 104 60-140107 320ND20.9 21.5
1,2,4-Trimethylbenzene ug/L 20 119 60-140121 120ND23.8 24.1
1,2-Dibromo-3-chloropropane ug/L 20 100 60-140101 020ND20.0 20.1
1,2-Dibromoethane (EDB)ug/L 20 113 60-140117 420ND22.6 23.4
1,2-Dichlorobenzene ug/L 20 117 60-140120 220ND23.5 23.9
1,2-Dichloroethane ug/L 20 108 60-140113 420ND21.7 22.6
1,2-Dichloropropane ug/L 20 111 60-140115 420ND22.2 23.1
1,3,5-Trimethylbenzene ug/L 20 122 60-140125 220ND24.5 24.9
1,3-Dichlorobenzene ug/L 20 118 60-140120 220ND23.6 24.0
1,3-Dichloropropane ug/L 20 111 60-140117 520ND22.2 23.3
1,4-Dichlorobenzene ug/L 20 115 60-140116 120ND22.9 23.2
2,2-Dichloropropane ug/L 20 110 60-140116 520ND22.1 23.1
2-Chlorotoluene ug/L 20 122 60-140126 320ND24.4 25.1
4-Chlorotoluene ug/L 20 118 60-140121 220ND23.7 24.2
Benzene ug/L 20 119 60-140123 320ND23.9 24.6
Bromobenzene ug/L 20 119 60-140122 220ND23.9 24.5
Bromochloromethane ug/L 20 122 60-140125 220ND24.5 25.0
Bromodichloromethane ug/L 20 106 60-140110 320ND21.3 22.0
Bromoform ug/L 20 88 60-14091 320ND17.6 18.2
Bromomethane ug/L 20 71 60-14082 1420ND14.2 16.4
Carbon tetrachloride ug/L 20 118 60-140123 420ND23.6 24.6
Chlorobenzene ug/L 20 115 60-140120 420ND23.1 23.9
Chloroethane ug/L 20 100 60-140113 1120ND20.1 22.5
Chloroform ug/L 20 116 60-140121 520ND23.1 24.2
Chloromethane ug/L 20 90 60-14097 820ND18.0 19.4
cis-1,2-Dichloroethene ug/L 20 117 60-140123 520ND23.4 24.5
cis-1,3-Dichloropropene ug/L 20 105 60-140110 420ND21.0 21.9
Dibromochloromethane ug/L 20 97 60-140104 620ND19.5 20.7
Dibromomethane ug/L 20 111 60-140115 420ND22.1 23.1
Dichlorodifluoromethane ug/L 20 109 60-140112 320ND21.7 22.3
Diisopropyl ether ug/L 20 112 60-140118 520ND22.4 23.6
Ethylbenzene ug/L 20 116 60-140121 420ND23.3 24.2
Hexachloro-1,3-butadiene ug/L 20 125 60-140134 720ND25.0 26.9
Isopropylbenzene (Cumene)ug/L 20 129 60-140135 420ND25.9 27.0
m&p-Xylene ug/L 40 115 60-140119 340ND45.9 47.6
Methyl-tert-butyl ether ug/L 20 104 60-140108 420ND20.8 21.6
Methylene Chloride ug/L 20 112 60-140123 920ND22.5 24.7
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
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Huntersville, NC 28078
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Page 28 of 33
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
1489898MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92253831006
1489899
MSD
Result
MSD
% Rec RPD
MSDMS
Spike
Conc.
n-Butylbenzene ug/L 20 118 60-140119 020ND23.7 23.8
n-Propylbenzene ug/L 20 123 60-140125 120ND24.7 25.0
Naphthalene ug/L 20 108 60-140112 420ND21.6 22.4
o-Xylene ug/L 20 115 60-140120 520ND22.9 24.0
sec-Butylbenzene ug/L 20 125 60-140127 120ND25.0 25.3
Styrene ug/L 20 116 60-140120 320ND23.2 24.0
tert-Butylbenzene ug/L 20 103 60-140103 020ND20.6 20.5
Tetrachloroethene ug/L 20 114 60-140119 520ND22.8 23.8
Toluene ug/L 20 114 60-140117 320ND22.8 23.5
trans-1,2-Dichloroethene ug/L 20 121 60-140128 620ND24.2 25.6
trans-1,3-Dichloropropene ug/L 20 105 60-140108 320ND21.0 21.5
Trichloroethene ug/L 20 112 60-140118 520ND22.4 23.7
Trichlorofluoromethane ug/L 20 108 60-140113 520ND21.6 22.6
Vinyl chloride ug/L 20 108 60-140116 720ND21.6 23.2
1,2-Dichloroethane-d4 (S)%98 70-130100
4-Bromofluorobenzene (S)%101 70-130103
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
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[phone]
Page 29 of 33
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
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[phone]
Page 30 of 33
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92254444
FLOWERS STORE 21858-A
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92254444001 MSV/32214MW-3 SM 6200B
92254444002 MSV/32214MW-5 SM 6200B
92254444003 MSV/32214MW-7 SM 6200B
92254444004 MSV/32214MW-8 SM 6200B
92254444005 MSV/32225MW-9 SM 6200B
92254444006 MSV/32214MW-10 SM 6200B
92254444007 MSV/32214WSW-5 SM 6200B
92254444008 MSV/32214WSW-4 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..Date: 06/22/2015 05:44 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 33
Page 32 of 33
Page 33 of 33