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HomeMy WebLinkAbout8602_Surry_MtAiry_MSWLF_CDLF_Dec2019GW_FID1405456_20200507NC DENR
Division of Waste Management - Solid Waste
Email CD (data loaded: Yes / No) Doc/Event #:
Environmental Monitoring
Reoortma Form
Notice: This form and any information attached to it are "Public Records" as defined in NC Gene
available for inspection and examination by any person upon request (NC General Statute 132-6).
are
Instructions:
• Prepare one form for each individually monitored unit.
• Please type or print legibly.
• Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
• Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
• Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitaring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Municipal Engineering Services Co., PA
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Jonathan Pfohl
E-mail: jpfohl@mesco.com
Phone: (919)772-5393
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: Facility Permit # (.0500 or. 1600) October 20-24, 2006)
Surry County Closed C&D and 237 Landfill Road December 10-13, 2019
Closed MSW Landfill -Mt. Airy Mt. Airy, NC 27030 86-02 .1600 January 15, 2020
Environmental Status: (Check all that apply)
Initial/Background Monitoring ❑X Detection Monitoring ❑X Assessment Monitoring QX Corrective Action
of data submitted: (Check all that apply)
Groundwater monitoring data from monitoring wells
Groundwater monitoring data from private water supply wellsFX
Leachate monitoring data ❑ Surface water monitorina data
Notification attached?
Methane gas monitoring data
Corrective action data (specify) MNA parameters on 7 wells
Other(specify)
i No. No groundwater or surface water standards were exceeded.
>( Yes, a nocation of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface wafer standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, 1 have attached complete nocation of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment.
Steven R. Gandy, Ph.D., P.E.
P.O. BOX 97, Garner, NC 27529
Facility Representative Address
C-0281
Senior Project Manager
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009
(919) 772-5393
a Code) Telephone Number
Affix NC Licensed/ Professional Geologist Seal
® ®i
® SEAL ••
® 31020 P IN
®®®®®FN ®•� R f111111
Semi -Annual Water Quality Monitoring Report
with Corrective Action Update
December 2019
Prepared for
Surry County Closed C&D and Closed Landfill
Mt. Airy, North Carolina
Permit No. 86-02
Prepared by
Municipal Engineering Services Company, P.A.
P.O. BOX 97
Garner, North Carolina
MESCO Project Number: G19031.0
V_ 4rA� or -
Steven R. Gandy, Ph.D, P.E.
Senior Project Manager
sgandygmesco.com
/ MUNICIPAL ENGINEERING
Ir�/11�'`I SERVICES COMPANY, P.A.
68 SHIPWASH DRIVE, GARNER, NO 27529 - PHONE: 91 9-772-5393
\ P.O. Box 349, BOONE, NO 28607 - PHONE: 826-262-1767
LICENSE NUMBER: C-13281
Jonathan Pfohl
Environmental Specialist
jpfohlAmesco.com
Introduction
On behalf of Surry County, Municipal Engineering Services Company, P.A. (MESCO) is pleased to present this Semi -
Annual Water Quality Report with Corrective Action Update for the Fall 2019 event performed at the Surry
County closed construction and demolition (C&D) and closed municipal solid waste landfill (MSWLF)-Mount Airy.
NCDEQ Solid Waste Rules 15A NCAC 13B.1632 requires that Surry County provide this report to the NC Solid
Waste Section (SWS) on a semi-annual basis. This report documents the quality of the ground and surface waters
during an event performed on December 10-13, 2019 and January 15, 2020.
During this event laboratory analytical results indicate Appendix I constituents continue to persist in concentrations
above groundwater compliance Standards in samples collected from nine monitoring wells. No constituents were
detected in surface water samples above established NC 2B Standards. Corrective action to remediate VOCs in
groundwater is ongoing within all three areas of concern (AOC) as described in the most recent Corrective Action
Evaluation Report (CAER) and improvement has been observed with updated information presented herein.
Background
The Surry County closed C&D and MSWLF, permit #86-02, is located at 237 Landfill Road in Mt. Airy North
Carolina. The site location topographic map is depicted in the attached Sheet 1. Prior to becoming a C&D landfill
the site operated as an unlined sanitary landfill that consisted of two units.
The northern unit was closed prior to October 1991. The southern unit is comprised of two contiguous portions. The
first part stopped receiving waste prior to October 1991 and the second part stopped receiving waste prior to January
1, 1999. Both portions of the southern unit were properly closed with a low permeability cohesive cap per the
Transition Plan. The top portion of the southern unit served as an exclusive C&D landfill until prior to June 1, 2008
at which time it was properly closed with another cohesive cap in accordance with the Closure Plan. For continuity,
both the northern and the southern units are monitored and reported together.
An Alternative Source Demonstration (ASD) which established Site Maximum Allowable Contaminate (SMAC)
regulatory compliance levels for three metals (cadmium, cobalt, vanadium) was approved by the NCDEQ on April 20,
2020 (FID 11395468).
Water quality at this facility has been monitored at least semi-annually since 1989 with historical data available since
1994. This event was performed in accordance with the NC SWS rules/regulations as promulgated in 15A NCAC
13B and as a condition of the post -closure portion of the permit to operate and memorandums this report contains
sampling procedures, field and laboratory results, groundwater and surface water characterization, and findings. This
report also contains a table of detections compared to Standards, field data results table, groundwater flow
directions/rates table, field observations of the monitoring network table, a potentiometric map of the uppermost
aquifer, histograms of historical detections, statistical trend analysis, laboratory analytical reports with chains -of -
custody (C-O-C) and quality assurance/quality control data.
Sampling Procedures
The water quality monitoring program, current as of this event date, includes sampling locations and parameters as
outlined in the Water Quality Sampling and Analysis Plan (SAP) (DIN:1320110 dated April 2019 and approved by the
SWS (DIN: 1320181) on May 1, 2019. Monitoring locations are shown on the enclosed potentiometric map (Sheet
2). MESCO personnel collected water samples from 18 downgradient groundwater monitoring wells (MW-3R,
MW-4, MW-6 through MW-11, MW-125, MW-13 through MW-17 and MW-19 through MW-23), one background
well (MW-1), one newly installed water supply well (WSW-2) and four surface water locations (SW-1, SW-2, SW-3
and SW-4). Data from three surface water points (SWN-1, SWN-2 and SW-C) designated in the Water Quality
Monitoring Plan for the adjacent lined MSWLF are presented because both permitted landfills share discharge areas.
Quality control measures implemented during this event included the quantification of potential artifact contaminants
via equipment (EB) and field (FB) blanks. Samples were not analyzed from the six injection wells (IW-1), (IW-
2/MW-2), (IW-3/MW-3RS), (IW-4/MW-4), (IW-5/MW-5) and (IW-6/MW-8) since they are exempt due to the
presence of injectant residue which would yield unrepresentative water quality results. Additionally a sample was
not analyzed from MW-12S since recharge was limited hence would not be representative.
A summary of the construction of the water monitoring wells is presented on Table 1. The function and integrity of
all monitoring locations were visually evaluated as documented on Table 2. The depth to water in each well was
electronically gaged prior to purging to quantify the static water level elevation. Low -flow pumping methodology or
bailing was utilized to adequately purge the wells to a minimum of three times the volume of standing water in the
well or until dry. Surface water samples were collected from Stoney Creek discharge feature at previously designated
locations. During well purging and surface water sample collection the required field parameters were recorded.
The samples were then placed into laboratory -prepared, pre -preserved containers via a new disposable polyethylene
bailer. Samples were collected, kept on ice, and transported to a NC -certified laboratory under proper C-O-C
protocols within the specified hold times for each analysis.
Field Parameter Data
Stabilized field parameters were recorded during purging which included depth to water, pH, dissolved oxygen (DO),
temperature, oxidation reduction potential (ORP), specific conductance and turbidity. The field parameter data
indicates the monitored groundwater is slightly acidic, reducing conditions, with relatively low specific conductance
which is generally consistent relative to each other and congruent with data historically reported. Field parameter
data recorded at the surface water locations had low specific conductance and neutral pH which is consistent with
uncontaminated water. A summary of the field parameter data is presented in Table 3 and the field sampling data
sheet is enclosed in Appendix B.
Laboratory Results
Pace Analytical Laboratory (PACE) performed the laboratory analysis of groundwater and surface water samples for
the total recoverable constituents listed in 40 CFR Appendix I and 1,4-Dioxane. A sampling and analysis table
summarizing the locations, constituents, and methods is presented on Table 4. Laboratory results and C-O-Cs are
contained in Appendix A.
2
Water samples were analyzed to the laboratory -established Method Detection Limits (MDL) and any value between
the MDL and laboratory -established Reporting Limit (RL) is qualified by the laboratory as an estimated concentration
hence qualified with a "J". Estimated concentrations are considered non -quantifiable and discretion should be made
prior to making decisions based solely on an approximate value. Table 5 summarizes constituents detected in
groundwater and QC samples compared to groundwater compliance standards which include Interim Maximum
Allowable Concentrations (IMAC), North Carolina Groundwater Standards (2L) and Site Maximum Allowable
Concentrations (SMAC). Although not applicable for regulatory compliance purposes detections are also compared
to the Maximum Contaminant Level (MCL) commonly referenced as the Federal "Drinking Water Standard". Table
6 lists the constituents detected in surface water samples compared to the current version of the Division of Water
Quality Surface Water Quality Tables.
Quality Control Samples
Zinc and 1,4-Dichlorobenzene were detected in both of the quality control samples (EB, FB).
Groundwater Samples Detected Above Standards
One or two metals were detected in quantifiable concentrations (> RL) above the NC 2L/IMAC/SMAC Value in
samples collected from 7 wells as shown on Table 5 and summarized below.
Metals Detected Above RL and 2L/IMAC/SMAC Values in Groundwater
Cd
Co
Tl
cadmium
cobalt
thallium
2L/SMAC
8
11
0.28
MW-6
34.2
0.46
MW-7
46
MW-9
180
0.34
MW-11
17.7
MW-16
376
MW-20
47.4
MW-22
8.7
130
Concentrations in ug/L.
VOC(s) were detected in quantifiable concentrations (> RL) above the NC 2L Standard in samples collected from five
wells as shown on Table 5 and summarized below.
VOC(s) Detected Above 2L Standards in Groundwater
1,2-DCA
1,2-DCP
1,4-DCB
Benzene
VC
2L STD.
0.4
0.6
6
1
0.03
MW-9
1.8
16.9
MW-13
1.1
7.7
MW-15
1.7
MW-16
1.4
7.5
1.2
MW-20
2.5
Concentrations in ug/L,
3
The majority of the monitoring locations that were found to contain VOCs included a mixture of dissolved phase
aromatic hydrocarbons and chlorinated aliphatic hydrocarbons. The only constituent which originated from an
anthropogenic source in levels above the EPA established maximum contaminant levels (MCLs) primary "Drinking
Water Standards" was vinyl chloride in samples MW-9 and MW-20. A site map depicting the concentrations and
estimated horizontal extent of VOCs that exceeded the 2L Standard during this event is presented on Sheet 2.
Surface Water Samples
No parameters were detected in concentrations above established 2B Groundwater Standards.
Corrective Action Update
Groundwater remediation continues to be implemented per the approved Corrective Action Plan (CAP) at the three
designated areas of concern (AOC) (Northern, Southern and MW-11). A second Corrective Action Evaluation Report
(CAER) (DIN: 1320112) was submitted on April 30, 2019 which demonstrated that groundwater conditions continue
to improve, except for area near MW-9, which was approved by the SWS on May 1, 2019 (DIN:1320182). A
historical summary of corrective actions performed to date are briefly described in the following sections.
MNAAnalysis (AOCs Northern, Southern and MW-11)
Semi-annual MNA monitoring of a subset of 12 wells for the full suite of SWS recommended parameters was
initiated on May 18, 2010 and performed for four consecutive semi-annual events to establish a baseline. A
revised SAP prescribing 7 wells with various targeted MNA constituents was approved by the SWS and initiated
during an event performed in May 2013. MNA monitoring was limited to field parameters (ORP, DO and turbidity)
during this event in compliance with the SAP. MNA parameters are presented on Table 3.
Enhanced Bioremediation via Substrate Injection (AOC Southern and Northern)
Per the SWS approved Corrective Action Plan enhanced bioremediation via substrate and tracer injection was
initiated in the Southern and Northern AOCs in accordance with requirements outlined in the Injection Well Permit
Application and Well Permit No. WI0400176 (5/6/11) in an effort to reduce low level aliphatic and aromatic
chlorinated hydrocarbons in groundwater to below the 2L Standards. An edible oil substate (EOS)-water emulsion
with sodium bromide tracer was injected into four wells (IW-1, IW-2, IW-3 and IW-5) on November 2-3, 2011.
Similar substrates were injected into monitoring wells MW-4/IW-4 and MW-8/IW-6 on October 24-25, 2012. Details
of the injection events are provided in the Injection Event Record dated November 4, 2011 and January 10, 2013.
As directed in the UIC Injection Well Permit renewed on April 15, 2013 semi-annual post -injection water quality
monitoring of wells located downgradient of viable injection points (MW-3R, MW-7, MW-9, MW-12S, MW-13,
MW-14, MW-15, MW-16, MW-17, MW-18, MW-19, MW-20, MW-21, MW-22, MW-23) and upgradient background
well MW-1 was also performed in conjunction with this semi-annual event. Total aggregate VOC concentrations
reported during this event were lower at all locations and an increasing trend is not evident when compared to the
respective moving averages of the five events preceding injection in the selected wells downgradient of the injection
points (Figure 1).
4
MW-11 AOC Investigations
The CAP designated MW-11 as an area of concern due to detections of VOCs detected in exceedance of 2L
Standards. MW-11 is located within the compliance boundary near the northern property line which is hydraulically
upgradient of the closed northern landfill. The northern landfill closed before October 1991 which was before
adoption of NC Section .1600 rules that address assessment and corrective action. VOCs have historically been
detected in excess of the 2L Standard at MW-11 which include a mixture of aromatics (fuel hydrocarbons) and
chlorinated hydrocarbons (solvents). VOCs were not detected above allowable Standards in samples collected from
MW-11 for the second consecutive event which is an improvement compared to previous events. MNA will continue
at MW-11 and substrate injection is no longer planned nor required as described in the most recent CAER.
Groundwater and Surface Water Characterization
A potentiometric map constructed from water elevations taken from the uppermost aquifer which consists of both
saprolite and the hydraulically connected upper portion of the fractured bedrock system is enclosed as Sheet 2.
Groundwater flow directions and velocity rates were calculated through modified Darcy's equation as shown on Table
7. Consistent with previous events the groundwater apparently flows in a general southeasterly direction towards the
tributaries of the Ararat River. The calculated average linear velocity of groundwater indicates an approximate
average of 2,044 ft/yr in the wells screened in regolith and 365 ft/yr in the wells screened in the bedrock. The
consistent disparity in flow rates between wells is indicative of heterogeneous geologic conditions and/or a product of
the limitations of the linear velocity equation when applied to anisotropic conditions which are characteristic of the
geology of the Piedmont. Streams located within the facility boundaries were observed to be of moderate volume
and flow with low turbidity.
Findings
One or more Appendix I constituent(s) were detected above allowable compliance levels in samples collected from
the uppermost aquifer at nine locations (MW-6, MW-7, MW-9, MW-11, MW-13, MW-15, MW-16, MW-20 and MW-
22). Since the previous event in October 2018 the plume appears to have advanced from the northern AOC to beyond
MW-20. All VOC concentrations remain within their own respective historically identified range.
Qualitative evaluation of VOC concentrations indicates a general decreasing trend over time and distance from the
landfill. During this event total cumulative VOC concentrations decreased compared to their respective five event
averages preceding corrective action at most locations (Figure 2). Results of statistical temporal trend analysis,
using Sen's Slope Estimator at a 95% confidence level indicate that none of the individual well's cumulative VOC
concentrations have increased compared to when corrective action began 8 years ago except for MW-9. The Southern
AOC and site -wide cumulative VOC levels continue to exhibit a decreasing trend.
The area of the uppermost aquifer beyond the compliance boundary containing quantifiable concentrations of VOCs
in exceedance of the 2L Standard during this event is estimated at 0.0 acres in the Northern AOC, 0.0 acres in the
MW-11 AOC and 4 acres in the Southern AOC for a total facility wide area of approximately 4 acres (Sheet 2). The
total area impacted beyond the compliance boundary has retracted an estimated 50% (from 8 acres to 4 acres)
compared to when corrective action was initiated 10 years ago and remains the same as the previous event.
5
Evaluation of the most current water quality data continues to support assertions drawn in previous reports. A few
VOCs persist in the upper portion of the aquifer but concentrations are decreasing over time and distance away from
the landfill. Samples collected from the local discharge features, which are all located within the property boundaries,
continue to lack contaminates above allowable levels. Data continues to indicate that the plumes within each AOC
have stabilized and/or decreasing and there is adequate evidence that groundwater is naturally attenuating. Corrective
action will continue per the approved CAP with amendments described in the latest CAER.
Closing
Water quality monitoring and corrective action will continue with the next event scheduled for the Spring of 2020.
Sheets
Topographic Map with Site Location
Surry County Landfill, Mt. Airy fl
237 Landfill Road
Mount Airy, NC 28621
Lat: 36-26-30.065
Long:-80-34-15.314
Northing:983356.18
Easting:1537885.48
0 Surry Co Property Line
O Closed Unlined C&D Landfill
O Closed Unlined Sanitary Landfill
O Active Lined MSW Landfill
SHEET 1
SWN-1 (-350 FT UPSTREAM)
1100
237 LANDFILL ROAD
r�3p
MW_-11
GWE=1129.45-
�.
•
�_—
r —
SCALEHOUSE
w
/
0
I
I�
M W-9
'moo
Benzene - 1.8
1 Chloride - 16
I''
7p9p 1
1
1
�o0 1
MW-20
o 1
Vinyl Chloride - 2.5
IW--6.71
�CWE=1046.44
r`
-GWE=1061.37
_
MWo 63.18
SW-2 ,
sw
IMW--7
GWE=106110
IF-
NOW OR FORMERLY
OWNED BY
JOHNNY COX
1050 IW-3/ l l l I I
GWE=989.17
MW-3R*
MW-16 ;,'GWE=976.79
GWE=974.18 / ,`
MW-16 '
112-Dichloroethane - 1.4
1050
INACTIVE LINED
PHASE 1
PTO 12/1 /98
MONITORED SEPERATELY
\\\'0000
ACTIVE LFG EXTRACTION
MW-6/,j
GWE=1045.51
1,4-Dichlorobenzene - 7.5 U II
Vinvl Chloride - 1.
SW-3 sw �� 0 i
MW-17
' GWE=956.50
i
J�
�— CLOSED UNLINED MSW (8602-MSWLF-1983)
STOPPED RECEIVING WASTE BEFORE OCTOBER 9,199
ACTIVE LCID (NO PERMIT) <2 ACRES
� I
I WSW-2
MW--1
GWE=1109.14
I TIRES BURIED UNDER SOIL AND GRASS
j
CLOSED UNLINED C&D(8602-CDLF-2001)
STOPPED RECEIVING C&D BEFORE JUNE 30, 20
CLOSURE REQUIREMENTS COMPLETED BEFOR
I CLOSED C&D OVER CLOSED UNLINED MSW (8602-CDLF ON TOP OF MSW)
STOPPED RECEIVING C&D BEFORE MARCH 3, 2006
STOPPED RECEIVING MSW BY JAN. 1, 1999
LFG EXTRACTION SYSTEM
J
' MW-12D*�
IW-2 GWE=1027.05 /
GWE= MW-12S
/,�p50 Op�g iw� GWE=1012.80 /
MW-1800
� /© GWE=974.36 /I /
/
IW-4
GWE=
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GWE=
A O G WE=980.30
M.
/ I
Mw
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W--13 /
' GWE=982.67
sw SW-1
PROPERTY LINE
MW-21
GWE=959.55
^000
g0
MW-22 , 9
GWE=948. ` 950
MW-23
910 / GWE=948.30
960
960
-7
g50 �
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GWE=936.95
o
-
/ o SW-4
LAGOON ! l I
SWN-2 (-1,420') & SW-C (-450')
DOWNSTREAM)
MW-15
Vinyl Chlorid"-1.7
MW-15
GWE=1024.96
ARoAFRTy
<iyF
NOW OR FORMERLY
OWNED BY
SHAWNA SUMMERS
LEGEND
EXISTING TOPOGRAPHIC CONTOURS
EXISITING ROAD/PATH
EXISTING CHAINLINK FENCE
EXISTING STRUCTURE
PERENNIAL CREEK, STREAM, ETC.
INTERMITTANT CREEK, STREAM, ETC.
PROPERTY LINE
- — — — — — — — — - LINED MSWLF PHASE LIMITS
- — — — — — — — — UNLINED WASTE LIMITS (APPROXIMATE)
COMPLIANCE BOUNDARY
1060 POTENTIOMETRIC GROUNDWATER CONTOUR (DEC. 2019)
GWE = 2626.85 GROUNDWATER POTENTIOMETRIC ELEVATION
*MW- ELEVATION NOT USED FOR CONTOURING
ESTIMATED EXTENT OF VOC VIOLATIONS (DEC. 2019)
BEYOND COMPLIANCE BOUNDARY (-4 ACRES)
ASURFACE WATER SAMPLING LOCATION
nn: MONITORING WELL EXISTING
1w INJECTION WELL EXISTING
O WATER SUPPLY WELL EXISTING
(APPROXIMATE LOCATION)
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DATE: 4110120
DRWN. BY: J. PFOHL
CHKD. BY.- S. GANDY
PROJECT NUMBER
DRAWING NO. SHEET NO.
SHEET 2 1 OF 1
Figure
Figure 1
Total Cumulative VOC Concentrations Pre/Post Injection Comparison
October 22, 2009 - December 14, 2019
DOWNGRADIENT OF IW-2 (TOTAL CUMULATIVE VOC CONCENTRATIONS)
s.mkox:
��nv.,s ovxns
DOWNGRADIENT OF IWA (TOTAL CUMULATIVE VOC CONCENTRATIONS)
s.meou.
�uws o�+a nrrvza
DOWNGRADIENT OF IW-7 (TOTAL CUMULATIVE VOC CONCENTRATIONS)
s.meoa.
�M,v.m or�vax
DOWNGRADIENT OF IW-5 (TOTAL CUMULATIVE VOC CONCENTRATIONS)
s�oemx
Baseline
Period (Oct.
2009-Oct.
2011)
Difference
Difference
Average of
Between
Between
first Five
Corrective
Most
Most
Statistical
Oct
May
Oct
May
Oct
Action
Dec.
Recent &
Recent &
Trend* Between
2009
2010
2010
2011
2011
Events
2019
Baseline
Baseline
Oct. 2009-Dec.
Well ID
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(uq/L)
(uq/L)
(D/D)
2019
INJECTION WELL (IW-1) UNSUCCESSFUL INJECTION SO DOWNGRADIENT WELLS NOT SHOWN
INJECTION WELL (IW-2) MONITORED DOWNGRADIENT BY MW-12S & MW-13
MW-12S
0.00
0.00
0.00
0.00
5.40
1.08
0 NS
0.00
0
HNo TrendH
MW-13
61.00
50.60
74.20
87.30
72.50
69.12
39.08
-30.04
-43
�Downward�
INJECTION WELL (IW-3) MONITORED DOWNGRADIENT BY MW-3R & MW-16
MW-3R
0.00
0.00
1 0.00
0.00
0.00
0.00
0.00
0.00
0
HNo TrendH
MW-16
1137.90
113.60
135.70
121.20
116.30
124.94
26.32
-98.62
-79
. Downward
INJECTION WELL (IW-4) MONITORED DOWNGRADIENT BY MW-14, MW-21 & MW-23
MW-14
15.20
15.60
15.60
8.20
17.00
14.32
6.80
-7.52
-53
HNo TrendH
MW-21
52.10
50.70
51.38
39.10
32.41
45.14
16.21
-28.93
-64
Downward.
MW-23
4.30
0.00
0.00
0.00
0.00
0.86
0.55
-0.31
-36
HNo TrendH
INJECTION WELL (IW-5) MONITORED DOWNGRADIENT BY MW-15 & MW-19
MW-15
96.13
63.89
55.00
78.10
64.06
71.44
49.02
-22.42
-31
Downward.
MW-19
0.00
0.00
0.00
0.00
0.00
0.00
3.13
3.13
100
HNo TrendH
INJECTION WELL (IW-6) NOT SHOWN AS NO WELLS DOWNGRADIENT WITHIN ZONE OF INFLUENCE
* = Statistical Trend analysis via Sen's Slope Estimator at a 95% confidence level
Surry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1
Figure 2
Total Cumulative VOC Concentrations Time Series Graphs/Table
October 22, 2009 - December 14, 2019
Total Cumu l_ t=_ VOCs
SOUTHERN AOC (TOTAL CUMULATIVE VOC CONCENTRATIONS) NORTHERN AOC (TOTAL CUMULATIVE VOC CONCENTRATIONS)
sum�o.e
13 oI 18 - A-4 �orm-is 4Ae 1 +rxv.n
AOC
Well ID
Oct
2009
May
2010
Oct
2010
May
2011
Oct
2011
Average of
first Five
Corrective
Action
Events
Dec. 2019
Difference
Difference
Statistical Trend
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(ug/L)
(%)
Oct 2009 -Dec. 2019
Background
MW-1
0.00
0.00
0.00
0.00
0.00
0.00
0
0.00
0
No Trend
IW-2 (MW-2)
105.25
207.00
207.93
159.90
79.10
151.84
79.10 NS
NS
NS
No Trend
IW-3 (MW-3RS)
202.90
127.50
127.50
144.00
127.60
145.90
127.60 NS
NS
NS
No Trend
MW-3R
0.00
0.00
0.00
0.00
0.00
0.00
0
0.00
0
No Trend
IW-4 (MW-4)
27.00
24.20
24.20
27.60
23.50
25.30
18.10 NS
NS
NS
No Trend
IW-5 (MW-5)
35.00
46.50
46.50
47.40
34.80
42.04
34.80 NS
NS
NS
No Trend
MW-12S
0.00
0.00
0.00
0.00
5.40
1.08
0 NS
NS
NS
No Trend
MW-12D
0.00
0.00
0.00
0.00
0.00
0.00
0 "S
0.00
0
No Trend
MW-13
61.00
50.60
74.20
87.30
72.50
69.12
39.08
-30.04
-44
Downward
Southern
MW-14
15.20
15.60
15.60
8.20
17.00
14.32
6.8
-7.52
-53
Downward
MW-15
96.13
55.00
55.00
78.10
64.06
69.66
36.9
-32.76
-47
Downward
MW-16
137.90
113.60
135.70
121.20
116.30
124.94
26.32
-98.62
-79
Downward
MW-17
20.34
8.40
8.85
0.00
5.77
8.67
0
-8.67
-100
No Trend
MW-18
0.00
0.00
0.00
0.00
0.00
0.00
0 NS
0.00
0
No Trend
MW-19
0.00
0.00
0.00
0.00
0.00
0.00
0.47
0.47
100
No Trend
MW-21
52.10
50.70
51.38
39.10
32.41
45.14
16.21
-28.93
-64
Downward
MW-22
28.90
23.80
23.80
11.66
5.20
18.67
11.74
-6.93
-37
Downward
MW-23
4.30
0.00
0.00
0.00
0.00
0.86
0.55
-0.31
-36
No Trend
Combined Total
786.02
722.90
770.66
724.46
583.64
717.54
397.67
-319.87
-45
Downward
MW-6
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
100
No Trend
MW-7
7.40
9.40
11.20
9.70
8.80
9.30
2.71
-6.59
-71
Downward
Northern
IW-6 (MW-8)
22.00
23.90
16.00
12.30
12.60
17.36
10.20 NS
NS
NS
No Trend
MW-9
23.50
20.40
23.20
25.80
22.90
23.16
56.93
33.77
146
Upward
MW-20
0.00
0.00
0.00
0.00
0.00
0.00
18.05
18.05
100
No Trend
Combined Total
52.90
53.70
50.40
47.80
44.30
49.82
87.89
38.07
76
No Trend
MW-11
MW-11
10.10
6.00
6.00
5.44
23.20
10.15
5.00
-5.15
-51
No Trend
SITEWIDE
Combined Total
849.02
782.60
827.06
777.70
651.14
777.50
490.56
-286.94
-37
Downward
N5 = Not sampled this event so most recent concentration shown and used in calculations
" = Statistical trend analysis via Sen's Slope Estimator on original and transformed log -normal at a 95% Confidence Level
Surry County Closed C&D and Closed MSW LF, Mt. Airy Page 1 of 1
Tables
Table 1
Groundwater Monitoring Well Construction Table
December 10-13, 2019
Monitoring Well
Date
Installed
Well
Diameter
Total Well
Depth
Top of Screen
Depth
Screen
Length
Geology of
Screened
Interval
Top of Casing
Elevation
Ground
Elevation
Groundwater
Elevation
Depth to
Water
Latitude
Longitude
(inches)
(ft bgs)
(ft bgs)
(ft)
(ft amsl)
(ft amsl)
(ft amsl)
(ft btoc)
MW-1
11/28/89
2
40
30
10
Clay
1134.35
1133.15
1109.14
25.21
36.439211
-80.568133
0-2 (was MW-2)
11/28/89
2
70
60
10
Clay
1068.86
1068.36
NR
NR
36.435833
-80.568894
MW-3R
9/27/94
2
101
86
15
Rock
1017.50
1015.00
976.79
40.71
36.434725
-80.571989
IW-3 (was MW-3RS)
5/17/01
2
52
37
15
Rock
1020.57
1018.24
989.17
31.40
36.434656
-80.571858
IW-4 (was MW-4)
8/30/94
2
55.4
40.4
15
Rock
1026.26
1025.06
NR
NR
36.434686
-80.569200
0-5 (was MW-5)
8/27/94
2
63
48
15
Rock
1080.18
1077.78
1038.75
41.43
36.434614
-80.570436
MW-6
9/7/94
2
29.7
14.7
15
Rock
1067.67
1065.61
1045.51
22.16
36.437431
-80.571067
MW-7
8/23/94
2
23
8
15
Rock
1073.50
1071.50
1061.10
12.4
36.438439
-80.570722
IW-6 (was MW-8)
8/16/94
2
54
39
15
Rock
1088.45
1086.45
1046.44
42.01
36.439278
-80.570381
MW-9
8/22/94
2
43.8
28.8
15
Rock
1094.07
1092.07
1061.37
32.70
36.439289
-80.571508
MW-11
8/15/94
2
40
25
15
Rock
1151.80
1150.40
1129.45
22.35
36.441589
-80.569558
MW-12S
5/31/01
2
51
11
40
Rock
1025.80
1023.25
1012.80
13.00
36.435942
-80.567972
MW-12D
5/30/01
2
100
90
10
Rock
1027.05
1023.75
1027.05
0.00
36.435964
-80.567994
MW-13
5/30/06
2
35.78
20.78
15
Saprolite
1008.48
1005.75
982.67
25.81
36.435036
-80.568183
MW-14
5/30/06
2
48.03
33.03
15
Rock
1018.80
1016.11
980.30
38.50
36.434267
-80.569239
MW-15
6/22/06
2
57
42
15
Rock
1075.96
1073.23
1024.96
51.00
36.433797
-80.570467
MW-16
6/21/06
2
36.3
21.3
15
Rock
999.54
996.67
974.18
25.36
36.434536
-80.572117
MW-17
6/1/07
2
15.32
5.32
10
Rock
965.43
962.26
956.50
8.93
36.433558
-80.572517
MW-18
6/1/07
2
18.15
8.15
10
Saprolite
983.00
980.00
974.36
8.64
36.435453
-80.567050
MW-19
6/1/07
2
17.1
7.1
10
PWR
946.27
942.97
936.95
9.32
36.432231
-80.570556
MW-20
6/1/07
2
25.64
10.64
15
Rock
1082.19
1079.12
1063.18
19.01
36.439025
-80.571650
MW-21
6/1/07
2
15.41
5.41
10
Saprolite/PWR
965.36
962.22
959.55
5.81
36.434214
-80.568717
MW-22
6/1/07
2
16.04
6.04
10
Saprolite
953.40
950.23
948.95
4.45
36.432928
-80.571678
MW-23
6/1/07
2
17.1
7.1
10
Sandy Silt
955.31
952.09
948.30
7.01
36.432828
-80.569156
NOTE:
bgs = below ground surface
amsl= above mean sea level
btoc = below top of casing (PVC well casing)
Slurry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1
Table 2
Field Observations of Monitoring Locations
December 10-13, 2019
Location
Viable
Monitoring
Location
Lack of Any
Evidence of
Tampering
Locked on
Arrival &
Departure
Hinge/Hasp
Operational
Tagged
or
Labeled
Concrete
Surface Pad
Appears
Effective
Comments
MW-1
Yes
Yes
Yes
Yes
Yes
Yes
IW-1
No
Yes
Yes
Yes
Yes
Yes
Fouled since injection 11/2/11.
IW-2 (was MW-2)
No
Yes
Yes
Yes
Yes
Yes
Fouled since injection 11/2/11. No pad visible
MW-3R
Yes
Yes
Yes
Yes
Yes
Yes
IW-3 (was MW-3RS)
No
Yes
Yes
Yes
Yes
Yes
Fouled since injection 11/2/11.
IW-4 (was MW-4)
No
Yes
Yes
Yes
Yes
Yes
Fouled since injection 10/24/12.
IW-5 (was MW-5)
No
Yes
Yes
Yes
Yes
Yes
Fouled since injection 11/2/11. Bailer would not descend
MW-6
Yes
Yes
Yes
Yes
Yes
Yes
MW-7
Yes
Yes
Yes
Yes
Yes
Yes
IW-6 (was MW-8)
No
Yes
Yes
Yes
Yes
Yes
Fouled since injection 10/24/12.
MW-9
Yes
Yes
Yes
Yes
Yes
Yes
MW-11
Yes
Yes
Yes
Yes
Yes
Yes
Black particles
MW-12S
No
Yes
Yes
Yes
Yes
Yes
Insufficient recharge, not sampled, atypical
MW-12D
Yes
Yes
Yes
Yes
Yes
Yes
Flowing artesian which is typical
MW-13
Yes
Yes
Yes
Yes
Yes
Yes
MW-14
Yes
Yes
Yes
Yes
Yes
Yes
MW-15
Yes
Yes
Yes
Yes
Yes
Yes
MW-16
Yes
Yes
Yes
Yes
Yes
Yes
No red purge water, atypical
MW-17
Yes
Yes
Yes
Yes
Yes
Yes
MW-18
Yes
Yes
Yes
Yes
Yes
Yes
MW-19
Yes
Yes
Yes
Yes
Yes
Yes
MW-20
Yes
Yes
Yes
Yes
Yes
Yes
MW-21
Yes
Yes
Yes
Yes
Yes
Yes
MW-22
Yes
Yes
Yes
Yes
Yes
Yes
Red purge water
MW-23
Yes
Yes
Yes
Yes
Yes
Yes
sW-1
Yes
SW-2
Yes
High gage height & moderate flow
SW-3
Yes
Moderate gage height & flow
SW-4
Yes
High gage height & flow
SW-c
Yes
High gage height & flow
SWN-1
Yes
High gage height & flow
SWN-2
Yes
Moderate gage height & flow
SCALEHOUSE
No
Scalehouse sample not taken
Any unusual field conditions, observations, or events:
Injection wells (IW-1, IW-2, IW-3, IW4, IW-5 and IW-6) exempt from laboratory analysis as approved by NC SWS on May 10, 2013 (DIN:18938)
Visual markers (10 ft PVC pipes) remain secured to each monitoring well case
Slurry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1
Table 3
Field Parameter Data Summary
December 10-13, 2019
January 15, 2020 (WSW-2)
Parameter
Depth to
Water
Water
Elevation
TOC
Elevation
Temp.
ORP
DO
pH
Specific
Conductance
Turbidity
Units
ft (btoc)
ft (amsl)
ft (amsl) C
my
mg/L
SU
umhos/cm
NTU
MW-1
25.21
1109.14
1134.35
15.4
-174
NR
6.48
111
0.49
IW-2
NR
NR
1068.86
NR
NR
NR
NR
NR
>1000
MW-3R
40.71
976.79
1017.50
14.9
55
2.0
6.68
310
3.00
IW-3
31.40
989.17
1020.57
NR
NR
NR
NR
NR
>1000
IW-4
NR
NR
1026.26
NR
NR
NR
NR
NR
>1000
IW-5
41.43
1038.75
1080.18
NR
NR
NR
NR
NR
NR
MW-6
22.16
1045.51
1067.67
14.9
-30
1.5
6.45
312
3.09
MW-7
12.40
1061.10
1073.50
NR
NR
NR
NR
NR
0.29
IW-6
42.01
1046.44
1088.45
NR
NR
NR
NR
NR
NR
MW-9
32.70
1061.37
1094.07
15.8
-141
NR
6.47
343
0.67
MW-11
22.35
1129.45
1151.80
14.8
-150
NR
6.06
206
10.0
MW-12S
13.00
1012.80
1025.80
13.7
-179
NR
7.42
348
NR
MW-12D
0.00
>1027.05
1027.05
NR
NR
NR
NR
NR
NR
MW-13
25.81
982.67
1008.48
14.0
-172
NR
5.99
332
1.95
MW-14
38.50
980.30
1018.80
13.8
-167
NR
5.83
142
2.73
MW-15
51.00
1024.96
1075.96
13.9
2
1.9
5.72
157
2.67
MW-16
25.36
974.18
999.54
14.0
266
1.6
6.14
587
6.96
MW-17
8.93
956.50
965.43
13.8
-151
NR
6.72
250
40.4
MW-18
8.64
974.36
983.00
NR
NR
NR
NR
NR
NR
MW-19
9.32
936.95
946.27
14.8
-24
7.8
5.47
66
24.6
MW-20
19.01
1063.18
1082.19
15.3
-132
NR
5.60
147
2.69
MW-21
5.81
959.55
965.36
13.9
12
4.0
5.50
251
0.25
MW-22
4.45
948.95
953.40
11.3
-149
NR
6.55
457
9.69
MW-23
7.01
948.30
955.31
14.1
-2
7.9
5.88
79
NR
WSW-2
na
na
na
NR
NR
NR
NR
NR
NR
Minimum
0.00
936.95
946.27
11.3
-179
1.5
5.47
66
0.86
Average
22.15
1010.50
1034.58
14.3
-71
3.8
6.19
256
153
Maximum
51.00
1129.45
1151.80
15.8
266
7.9
7.42
587
>1000
SW-1
-
-
-
4.4
-156
NR
7.48
95
4.48
SW-2
-
-
-
4.9
-180
NR
7.53
110
2.13
SW-3
-
-
-
5.3
-98
NR
7.37
98
40.5
SW-4
-
-
-
5.7
-151
NR
7.54
57
22.8
SWN-1
-
-
-
5.6
-150
NR
7.47
70
2.40
SWN-2
-
-
-
5.3
1 -176
NR
8.5
98
3.06
Minimum
-
-
-
4.4
-180
-
7.37
57
2.13
Average
-
-
-
5.2
-152
-
7.65
88
12.6
Maximum
-
-
-
5.7
-98
-
8.50
110
40.5
NOTES:
btoc = Below top of casing
amsl = Above mean sea level
na = Not available
NR = No reading attempted
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1
Table 4
Sampling and Analysis Summary
December 10-13, 2019
January 15, 2020 (WSW-2)
App.
I
10ther
I
Field
Parameter
a
O
m
c
N
O
a°
0
c
_
o
CL
QCY)
N
U
7
^
a
w
c
X
O
Q
a
N
X
N
C
5
U
N
U
m
O Q
�
O
N
a
N
Q
E
c
6
a
O
�
F
m
o
O
F
U
a
F
0
0
0
co
0
0
co
N
OD
N
OD
N
N
N
N
N
N
w
w
w
o
-o
a
-0
-0
-o
m
a m
J
1.92
J
J
u-
LL
LL.
LL
LL
u-
IW-1
Not sampled'
MW-1
X X X I I X I X X X X
IW-2
Not sampled'
MW-3R
X X X I X I X I X X X X
IW-3
Not sampled'
IW-4
Not sampled'
IW-5
Not sampled'
MW-6
X
X
X
X
I
I X
X
X
X
MW-7
X
X
X
X
I X
I X
X
X
X
IW-6
Not sampled'
MW-9
X
X
X
X
X
X
X
X
MW-11
X
X
X
X
X
X
X
X
MW-12S
Not sampled 2
X
X
X
X
MW-12D
Not sampled'
MW-13
X
X
X
X
X
X
X
X
MW-14
X
X
X
X
X
X
X
X
MW-15
X
X
X
X
X
X
X
X
X
MW-16
X
X
X
X
X
X
X
X
X
MW-17
X
X
X
X
X
X
X
X
MW-18
X
X
X
X
X
X
X
MW-19
X
X
X
X
X
X
X
X
X
MW-20
X
X
X
X
X
X
X
X
MW-21
X
X
X
X
X
X
X
X
X
MW-22
X
X
X
X
X
X
X
X
MW-23
X
X
X
X
X
X
X
X
X
WSW-2
X
X
X
SW-1
X
X
X
X
X
X
X
X
SW-2
X
X
X
X
X
X
X
X
SW-3
X
X
X
X
X
X
X
X
SW-4
X
X
X
X
X
X
X
X
SW-c
X
X
X
X
X
X
X
SWN-1
X
X
X
X
X
X
X
X
SWN-2
X
X
X
X
X
X
X
X
EB
X
X
X
FB
X
X
X
NOTES:
App I List = From current 40 CFR 258
' Not sampled since no longer on monitoring plan [DIN:18936]
2 Not sampled since insufficiently recharged
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1
Table 5
Groundwater and QC Sample Detections
December 11-14, 2019, January 15, 2020 (WSW-2)
Parameter Name
MDL
RL
2L / IMAC
MCL
MW-1
MW-3R
MW-6
MW-7
MW-9
MW-11
MW-13
MW-14
MW-15
MW-16
MW-17
MW-19
MW-20
MW-21
MW-22
MW-23
WSW-2
EB
FB
SMAC VALUE*
BG
S
S
S
S
S
S
S
S
S
S
S
S
S
S
S
WSW
QC
QC
Metals Tar eted 40CFR
258 Appendix I
Barium, total
1
5
700
2000
50.5
7.4
70
45.6
43.4
40.1
--
25.3
50.5
99.5
23.9
45.7
43
57.3
117
24.3
11.7 J
3.5 J
3.2 J
Beryllium, total
0.2
1
4
4
0.24 J B
0.28 J B
0.29 J B
--
0.42 J B
0.3 J B
0.42 J B
0.23 J
Cadmium, total
0.4
1
8*
5
0.61
0.69 J
0.57 J
1.3
1.4
--
0.59 J
1.2
1.5
1.3
0.64 J
4.5
8.7 (L)
Cobalt, total
1.1
5
11*
NE
1.1 J
34.2 (L)
46 (L)
180 (L)
17.7 (L)
--
2.5 J
376 (L)
1.5 J
47.4 (L)
4 J
130 (L)
Copper, total
2.1
5
1000
1300
2.8 J
--
4.4 J
2.5 J
2.7 J
2.7 J
3.2 J
Lead, total
1.6
5
15
15
--
2.3 J
3.1 J
Nickel, total
0.9
5
100
NE
1.4J
2.5J
6.9
2.6J
--
1.6J
2.2J
19.4
3.1 J
1.2J
3.9J
1.3J
9.8
1.2J
Selenium, total
4.7
10
20
50
--
12.4
8.3 J
Thallium, total
0.06
0.1
0.28
2
0.46 (L)
0.13
0.34 (L)
0.065 J
--
0.097 J
0.28
0.068 J
0.57
0.15
Vanadium, total
1.3
5
27*
NE
1.7 J
1.4 J
1.9 J
2.1 J
--
3.2 J
2.7 J
2.5 J
2.1 J
3.7 J
Zinc, total
3.9
10
1000
NE
8.9 J
7.9 J
20.6
--
4.7 J
8.5 J
12.1
7.7 J
15
4.7 J
41.8
5.5 J
12.8
8.4 J
Turbidity (Field Measured)
Turbidity (NTU) 0.01 - NE NE 0.49 3.00 3.09 0.29 0.67 10.0 -- 2.73 2.67 6.96 40.4 24.6 2.69 0.25 9.69 -- -- -- --
VOCs (Targeted 40CFR 258 Appendix I and 1,4-Dioxane)
1,1-Dichloroethane
0.27
1
6
NE
1.3
2
2
5.4
0.56 J
0.73 J
2.1
0.62 J
1,2-Dichlorobenzene
0.29
1
20
NE
1.4
0.77 J
0.7 J
0.89 J
0.64 J
1,2-Dichloroethane
0.34
1
0.4
5
1.1 (L)
1.4 (L)
0.44 J
0.49 J
1,2-Dichloropropane
0.19
1
0.6
5
0.73 J
1,4-Dichlorobenzene
0.26
1
6
75
0.45 J
4.7
2.2
7.7 (L)
2.9
7.5 (L)
2.1
5.8
1.5
1.9
Benzene
0.15
1
1
5
1.8 (L)
0.41 J
0.54 J
0.3 J
0.96 J
0.73 J
0.39 J
Chlorobenzene
0.23
1
50
100
0.81 J
1.6
1 J
3.6
2.1
3.5
0.82 J
2.3
Chloroethane
0.49
1
3000
NE
1.9
0.6 J
cis-1,2-Dichloroethene
0.29
1
70
70
39.1
0.66 J
21.9
4.8
22.9
10.5
0.47 J
5.1
13.2
1.5
0.55 J
0.43 J
Toluene
0.24
1
600
1000
0.32 J
Trichloroethene
0.22
1
3
5
0.76 J
1.9
0.47 J
Vinyl chloride
1 0.24
1
1 0.03
1 2
1
1
1
1 16.9 L
0.71 J
1.7 (L)
1 1.2 (L)
2.5 L
Notes:
Units ug/L except for turbidity, Blank cells means not detected above MDL, -- means parameter not analyzed, NE means not established
Bold Above RL and Established 2L//IMAC/SMAC (Regulatory compliance Standard)
Green Highlighted Above Established MCL Drinking Water Std. (No regulatory significance)
BG = Background Well Sample, QC = Quality Control Sample, S = Sentinal Well Sample, WSW = Water Supply Well Sample.
MDL = Adjusted Method Detection Limit established by the laboratory via a statistical calculation.
Since the MDL is below the point of calibration, results reported down to the MDL are not reliable and must be qualified as estimated values and, as such, carry a "J" qualifier designation.
RL = Reporting Limit established by the laboratory. The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix.
2L = NC 2L Groundater Standard 15A NCAC 02L .0202
IMAC = Interim Maximum Allowable Concentration
SMAC = Site Maximum Allowable Concentration. Approved by SWS on 4/7/20 (FID:1395468)
MCL = Maximum Contaminant Level for drinking water established by the USEPA.
J = "J-qualified". Defined by the lab as "Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit".
(N) Preliminary source is believed to be Natural originating from erosion of natural deposits. Source not anthropogenic.
(L) Prelilminary source is believed to be anthropogenic with Landfill Gas Wor leachate as suspected transport mechanism.
A definitive source of the detections was not determined as part of this report.
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1
Table 6
Surface Water Sample Detections
December 12-13, 2019, January 15, 2020 (SWN-1)
Parameter Name
MDL
RL
NC 2113
STD'
EPA
NIR
NC
ISTV3
°
MCL
SWN-1
SWN-2
SW-C
SW-1
SW-2
SW-3
SW-4
SW-C
SWN-2
U
D
D
D
D
D
D
D
D
Metals (Targeted 40CFR 258 Appendix 1)
Barium, total
1
5
NE
NE
200,000
2,000
16.5 J
17.2
26 J
20.7
18.8 J
26.4
27.2
17.2
Beryllium, total
0.2
1
65
NE
NE
4
0.45 J B
0.75 J
0.2 J B
0.31 J B
0.41 J
Cadmium, total
0.4
1
1.23
NE
NE
5
0.67 J
0.81 J
0.56 J
t0.45
Cobalt, total
1.1
5
NE
NE
4
NE
1.5 J
21.3
1.4 J
1.2 J1.5
J
Copper, total
2.1
5
5.67
NE
NE
1,300
3.1 J
Nickel, total
0.9
5
119.99
NE
NE
NE
1 J
Nickel, total
0.9
5
387.68
NE
NE
NE
Vanadium, total
1.3
5
NE
NE
NE
NE
2.5 J
1.8 J
3.5 J
2 J
2.5 J
Zinc, total
3.9
10
96.99
NE
NE
NE
7.5 J
11.7
8.3 J
7.5 J
Zinc, total
3.9
10
29.97
NE
NE
NE
4.3 J
Zinc, total
3.9
10
53.91
NE
NE
NE
4.8 J
Hardness as CaCo3 (Field Measured)
Hardness (mg/L) 20 NE NE NE NE 40 60 80 20 40 40 80 80 60
VOCs (Targeted 40CFR 258 Appendix I & 1,4-Dioxane)
cis-1,2-Dichloroethene 0.15 1 NE NE 720 70 3
Notes:
Units ug/L unless indicated otherwise, Blank cells means Not Detected, NE means Standard Not Established
J = "J-qualified". Defined by the lab as "Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit".
B = "B-qualified" by the lab. Analyte was detected in the associated method blank which may be interpreted as a false positive
Red Bold Above RL and Applicable 213 Std.
Above Established Federal MCL Primary Drinking Water Std.
Receiving surface waters are Stoney Creek (12-72-12) and Ararat River (12-72-(4.5) ) Both Class C. 03040101 (8-Digit HUC).
NC 26 STD = North Carolina 15A NCAC 02B Water Quality Standards for Surface Waters. Presumed NC SWS adopted the numerical Standard for regulatory compliance purposes.
2B Standards from All Waters (C & SC) or Class C. 213 Standard for cadmium, copper, nickel and zinc from calculations for acute exposure based on measured hardness values.
Cadmium 26 Standard calculation:WER*[(1.136672-[In hardness](0.041838))*eA(0.9151 [In hardness]-3.1485)]
Copper 26 Standard calculation:WER*[0.960*eA{0.9422[ln hardness]-1.700)]
Nickel 2B Standard calculation:WER*[0.998*eNO.8460[ln hardness]+2.255)]
Zinc 26 Standard calculation:WER*[0.986*eA(0.8473[ln hardness]+0.884)]
2 EPA NRWQC = EPA Nationally Recommended Water Quality Criteria for Aquatic Life & Human Health.
Nationally Recommended Water Quality Criteria for which NC does not have a Water Quality Standard for one or more uses
s NC ISTV= North Carolina In -Stream Target Value. Established per language in 15A NCAC 02B .0202 & .0208. Contact DWR staff for further information.
NC PV for barium fresh water All waters (Class C), for cobalt and cis-1,2DCE All waters Fresh & Salt (Class C & SC)
° MCL= Maximum Contaminant Level. Federal Primary "Drinking Water Standard". Shown for comparison purposes only. Not applicable for regulatory compliance purposes
Surry County Closed CDLF and Closed MSWLF, Mt. Airy Page 1 of 1
Table 7
Hydrogeolofic Properties at Monitoring Well Locations
December 11-14, 2019
Well
Hydraulic Conductivity
Effective
Porosity
Hydraulic
Gradient
Groundwater Average
Linear Velocity Rate
Flow
Direction
inimum
Distance From
Upgradient
EOW
Ground Water
Depth
Groundwater
Potentiometric
Elevation
Screened Interval
Lithology
(cm/second)
(ft/day)
N
(feet/feet)
(feet/year)
A
(feet btoc)
(feet amsl)
MW-1
4.30E-05
0.12
15
0.086
26
N69W
0
25.21
1109.14
Clay
IW-2
4.30E-05
0.12
15
-
-
-
NR
NR
Clay
MW-7
8.10E-04
2.30
1 15
0.089
1 499
N63W
1 704
12.40
1061.10
PWR / Fractured Rock
IW-6
4.40E-04
1.25
15
0.111
337
S03E
-
42.01
1046.44
PWR/ Fractured Rock
MW-9
1.90E-04
0.54
15
0.089
117
S36E
614
32.70
1061.37
Sandy Silt
MW-13
2.06E-04
0.58
23
0.164
152
S42E
1,850
25.81
982.67
Saprolite
MW-18
2.04E-03
5.78
15
0.133
1,869
0
8.64
974.36
Saprolite
MW-19
1.10E-03
3.12
3
0.095
3,616
S16W
2,663
9.32
936.95
PWR
MW-21
1.28E-03
3.63
3
0.147
6,480
S72E
2,041
5.81
959.55
Saprolite/PWR
MW-22
9.88E-04
2.80
15
1.050
7,156
S29W
2,506
4.45
948.95
Saprolite
MW-23
3.04E-04
0.86
1 15
0.089
188
S30E
2,610
7.01
948.30
Sandy Silt
Minimum
4.30E-05
0.12
3
0.086
26
0
4.45
936.95
Average
6.77E-04
1.92
14
0.205
2,044
1,443
17.34
1002.88
Maximum
2.04E-03
5.78
23
1.050
7,156
2,663
42.01
1109.14
MW-3R
2.40E-04
0.68
5
na
na
NR
1,994
40.71
976.79
Fractured Rock
IW-3
2.40E-05
0.07
5
0.169
84
S41W
-
31.40
989.17
Fractured Rock
IW-4
1.10E-04
0.31
5
-
NR
NR
Fractured Rock
IW-5
1.50E-05
0.04
5
-
-
-
>40.68
<1039.50
Fractured Rock
MW-6
1.90E-05
0.05
5
0.132
52
S80W
963
22.16
1045.51
Fractured Rock
MW-11
3.10E-04
0.88
5
0.069
442
S22W
0
22.35
1129.45
Fractured Rock
MW-12S
na
na
3
0.156
na
S23E
0
13.00
1012.80
Fractured Rock
MW-12D
1.30E-06
0.00
5
--
--
0
0.00
>1027.05
Fractured Rock
MW-14
7.45E-03
21.12
3
0.154
39,529
S77E
2,098
38.50
980.30
Fractured Rock
MW-15
7.21E-05
0.20
3
0.093
230
S07E
2,020
51.00
1024.96
Fractured Rock
MW-16
2.82E-05
0.08
3
0.169
165
S40W
2,089
25.36
974.18
Fractured Rock
MW-17
2.94E-04
0.83
3
0.119
1,207
S67W
2,547
8.93
956.50
Rock
MW-20
1.92E-04
0.54
3
0.056
372
S22E
692
19.01
1063.18
Rock
Minimum
1.30E-06
0.00
3
0.056
52
0
0.00
956.50
Average
7.30E-04
2.07
4
0.124
365
1,240
24.77
1015.28
Maximum
7.45E-03
21.12
5
0.169
1,207
2 547
51.00
1129.45
NOTES: Values for hydraulic conductivity determined via slug test by GAI, MESCO, or Joyce.
Hydrologic gradient from water levels recorded on December 11-14, 2019.
Wells screened entirely in rock were not utilized for flow directions/gradients.
Screens that traverse both rock and regolith assumed flow in regolith dominates.
Hydraulic Conducitivity value and flow rate for MW-14 was considered an outlier; therefore not included in the average or maximum.
na = Not available/applicable
Average Linear Velocity (Q) is defined by modified Darcy's equation:
K A K= hydraulic conductivity
where Q ri dl ne = effective porosity
e
dh=head difference
dl= horizontal distance
Slurry County Closed C&D and Closed MSWLF, Mt. Airy Page 1 of 1
Appendix A
Field Sampling Parameter Data Sheet(s)
Field Sampling Data Sheet
Project:
Surry Co
Closed C&D
and Closed
MSWLF-Mt.
Airy
5 F
- --
G A
-
'.?D
Parameters
Sample
Type
Goes
Dry
During
Purge
Total
Depth
Measured
as
expected
Total
Depth
Expected
Comment
s
Water
DO
(mg/L)
Quality
OR
P
p H
Parameters
Temp
, ©
(Stabilized)
S ecifi
p
c Cond.
( us/cm
TDS
( mg/L)
�
f-
CH4
Gas
Vapors
Monitoring
Point
-%Te
Date
e
Time
Sampling
Depth to
Water
(BTOP)
Static
Depth to
Water
(BTOP)
Collection
Volume
Purged
(Gal)
h1,7
40
MW-1
; -
(0: -/
._,
IW-2
-
-
-
-
-
-
68.08
-
-
-
-
-
-
-
-
-
-
-
100
52
57
-
-
-
-
�-
-
-
-
-
-
-
-
-
3 ^ 2
-�
MW-3R
i t -
L) 6, -7 {
3 , L;
I W-3
-
-
) , �a
-
-
IW-4
-
-
-
-
64
-
-
-
-
IW-5
-
-
oLI 3
-
-
��
,� . �a
✓ i
r , e
�
31
25
t'
MW-6
4n�I
0 7
-L m�
MW-7
i3.)
�
I U
56
46
S.
e,
t'
IW-6
MW-9
MW-11100
�1
?®
40
s
rf
;b�
l''
7
�`
35.78
03
56.98
36.28
15.32.
o,
�';
_
`t
k
5l{ L
D 6
QI79
MW-12S
A/ `)
tl,
MW-13
t f
a r Lf
MW-14
MW-15
�
MW-16II
7�
;,b
MW-17
-
-
-
-
18.15
-
-
-
-
-
MW-18
-
-
I
,r
� �,
t?
17.1
25.64
15.41
16.04
17.1
222
'-
�13
5,
S•
���.0
,%'
rip•
,vI
"
MW-19
_
—
e
M W-20
j b D 1
MW-21
� �� I ��-
=�d � �'�
�� � i
MW-22
l
#�
MW-23
Ji, V
i '
(� t
SS B=Stainless Steel Baler, u B=uisposaulu od-1, r-�Uvv 11-v I U19" .. -
VT=Very Turbid, MT=Moderately Turbid, ST=Slightly Turbid, C=Clear
Field Sampling Data Sheet
hiunicll>ul (J ;_$J 1�= a t•:nFl.. avrluF
Project: Surry Co Closed C&D over Closed MSWLF & Active Subtitle D Lined- Mt. Airy (Shared Surface Waters) Samplers:
Monitoring
Point
Collect
Date
Collect
Time
SamplingParameters Water
Quality
Parameters (Stabilized)
Visual
Flow
Rate
Lab
Parameter
s to be
analyzed
for
Visual
Gua a
Ht.
Sample
Type
Goes
Dry
During
Purge
Total
Depth
Measured
as
expected
Comments
DO
(mg/L)
OR
P
pH
Temp
©
Specifi
c Cond.
(us/cm
Hardness
(mg/L)
�
:o
fl
CH4
Gas
Vapors
(pp )
SW-1
SW-2
SW-3
SWN-1
SWN-2
SW-C
a /
✓, '' U
,
I r
i t s 31,'
Gl ,
°;.
) v `
V
'�:
�„ f.
I
I
I
I
_
—
-
—
-
—
-
—
-
s5 T T fl d `. tlF; '
1�
/K0r Ue1°Vv
el.,.
—15,
-176S,5�
a�
✓ °
7°z:
4
�
-
SS B=Stainless Steel Baler.
D B=Disposable
Baler, P=Low flow Pump, PD=Purged Dry
VT=Very Turbid, MT=Moderately Turbid, ST=Slightly Turbid, C=Clear
NR=No Reading Attempted, NS=No Sample Obtained
Appendix B
Laboratory Analysis Reports
Chains of Custody
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
December 31, 2019
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
RE: Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on December 16, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
ft*OL-'
Angela Baioni
angela.baioni@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Steven R. Gandy, Municipal Engineering Services Co.
Maddie German, Municipal Engineering Services
REPORT OF LABORATORY ANALYSIS
r
e
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
SAMPLE SUMMARY
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92457590001
MW-1
Water
12/13/19 10:27
12/16/19 08:30
92457590002
MW-3R
Water
12/12/19 13:45
12/16/19 08:30
92457590003
MW-6
Water
12/12/19 14:07
12/16/19 08:30
92457590004
MW-7
Water
12/12/19 14:09
12/16/19 08:30
92457590005
MW-9
Water
12/13/19 14:41
12/16/19 08:30
92457590006
MW-11
Water
12/13/19 14:59
12/16/19 08:30
92457590007
MW-13
Water
12/13/19 13:53
12/16/19 08:30
92457590008
MW-14
Water
12/13/19 10:10
12/16/19 08:30
92457590009
MW-15
Water
12/12/19 13:57
12/16/19 08:30
92457590010
MW-16
Water
12/12/19 13:50
12/16/19 08:30
92457590011
MW-17
Water
12/13/19 13:15
12/16/19 08:30
92457590012
MW-19
Water
12/13/19 00:00
12/16/19 08:30
92457590013
MW-20
Water
12/13/19 14:28
12/16/19 08:30
92457590014
MW-21
Water
12/12/19 14:34
12/16/19 08:30
92457590015
MW-22
Water
12/13/19 15:23
12/16/19 08:30
92457590016
MW-23
Water
12/12/19 11:25
12/16/19 08:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 63
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SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Surry Closed -Mt. Airy
92457590
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92457590001
MW-1
EPA 601 OD
KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92457590002
MW-3R
EPA 601 OD
KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92457590003
MW-6
EPA 601 OD
KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92457590004
MW-7
EPA 601 OD
KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92457590005
MW-9
EPA 601 OD
KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92457590006
MW-11
EPA 601 OD
KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92457590007
MW-13
EPA 601 OD
KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92457590008
MW-14
EPA 601 OD
KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92457590009
MW-15
EPA 601 OD
KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92457590010
MW-16
EPA 601 OD
DS, KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92457590011
MW-17
EPA 601 OD
KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92457590012
MW-19
EPA 601 OD
KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92457590013
MW-20
EPA 601 OD
KQ
14
PASI-A
REPORT OF LABORATORY ANALYSIS
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9800 Kincey Ave. Suite 100
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(704)875-9092
SAMPLE ANALYTE COUNT
Project:
Surry Closed -Mt. Airy
Pace Project No.:
92457590
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92457590014
MW-21
EPA 601 OD
KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92457590015
MW-22
EPA 601 OD
KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92457590016
MW-23
EPA 601 OD
KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 5 of 63
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(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MWA Lab ID: 92457590001 Collected: 12/13/19 10:27 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.0
1
12/24/19 01:21
12/24/19 23:15
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:15
7440-38-2
Barium
50.5
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:15
7440-39-3
Beryllium
ND
ug/L
1.0
0.20
1
12/24/19 01:21
12/24/19 23:15
7440-41-7
Cadmium
0.61J
ug/L
1.0
0.40
1
12/24/19 01:21
12/24/19 23:15
7440-43-9
Chromium
ND
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:15
7440-47-3
Cobalt
1.1J
ug/L
5.0
1.1
1
12/24/19 01:21
12/24/19 23:15
7440-48-4
Copper
ND
ug/L
5.0
2.1
1
12/24/19 01:21
12/24/19 23:15
7440-50-8
Lead
ND
ug/L
5.0
1.6
1
12/24/19 01:21
12/24/19 23:15
7439-92-1
Nickel
1.4J
ug/L
5.0
0.90
1
12/24/19 01:21
12/24/19 23:15
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:15
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
12/24/19 01:21
12/24/19 23:15
7440-22-4
Vanadium
ND
ug/L
5.0
1.3
1
12/24/19 01:21
12/24/19 23:15
7440-62-2
Zinc
8.91
ug/L
10.0
3.9
1
12/24/19 01:21
12/24/19 23:15
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
ND
ug/L
0.10
0.060
1
12/24/19 02:04
12/30/19 19:37
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Acetone
ND
ug/L
25.0
6.2
1
12/24/19 02:23
67-64-1
Acrylonitrile
ND
ug/L
10.0
0.90
1
12/24/19 02:23
107-13-1
Benzene
ND
ug/L
1.0
0.15
1
12/24/19 02:23
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.34
1
12/24/19 02:23
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.26
1
12/24/19 02:23
75-27-4
Bromoform
ND
ug/L
1.0
0.62
1
12/24/19 02:23
75-25-2
Bromomethane
ND
ug/L
2.0
0.62
1
12/24/19 02:23
74-83-9 v2
2-Butanone (MEK)
ND
ug/L
5.0
3.3
1
12/24/19 02:23
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.40
1
12/24/19 02:23
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.22
1
12/24/19 02:23
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.23
1
12/24/19 02:23
108-90-7
Chloroethane
ND
ug/L
1.0
0.49
1
12/24/19 02:23
75-00-3 v2
Chloroform
ND
ug/L
5.0
2.3
1
12/24/19 02:23
67-66-3
Chloromethane
ND
ug/L
1.0
0.39
1
12/24/19 02:23
74-87-3 v2
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
0.26
1
12/24/19 02:23
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.41
1
12/24/19 02:23
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.26
1
12/24/19 02:23
106-93-4
Dibromomethane
ND
ug/L
1.0
0.46
1
12/24/19 02:23
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.29
1
12/24/19 02:23
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.26
1
12/24/19 02:23
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.54
1
12/24/19 02:23
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.27
1
12/24/19 02:23
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.34
1
12/24/19 02:23
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.24
1
12/24/19 02:23
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
0.29
1
12/24/19 02:23
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
0.25
1
12/24/19 02:23
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.19
1
12/24/19 02:23
78-87-5
REPORT OF LABORATORY ANALYSIS
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Date: 12/31 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 6 of 63
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MWA
Lab ID:
92457590001
Collected:
12/13/19 10:27
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/24/19 02:23
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/24/19 02:23
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/24/19 02:23
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/24/19 02:23
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/24/19 02:23
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/24/19 02:23
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/24/19 02:23
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/24/19 02:23
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/24/19 02:23
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/24/19 02:23
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/24/19 02:23
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/24/19 02:23
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/24/19 02:23
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/24/19 02:23
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/24/19 02:23
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/24/19 02:23
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/24/19 02:23
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/24/19 02:23
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/24/19 02:23
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
12/24/19 02:23
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/24/19 02:23
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
12/24/19 02:23
460-00-4
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
12/24/19 02:23
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
12/24/19 02:23
2037-26-5
Date: 12/31 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 63
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-3R Lab ID: 92457590002 Collected: 12/12/19 13:45 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.0
1
12/24/19 01:21
12/24/19 23:25
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:25
7440-38-2
Barium
7.4
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:25
7440-39-3
Beryllium
0.24J
ug/L
1.0
0.20
1
12/24/19 01:21
12/24/19 23:25
7440-41-7 B
Cadmium
ND
ug/L
1.0
0.40
1
12/24/19 01:21
12/24/19 23:25
7440-43-9
Chromium
ND
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:25
7440-47-3
Cobalt
ND
ug/L
5.0
1.1
1
12/24/19 01:21
12/24/19 23:25
7440-48-4
Copper
ND
ug/L
5.0
2.1
1
12/24/19 01:21
12/24/19 23:25
7440-50-8
Lead
ND
ug/L
5.0
1.6
1
12/24/19 01:21
12/24/19 23:25
7439-92-1
Nickel
ND
ug/L
5.0
0.90
1
12/24/19 01:21
12/24/19 23:25
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:25
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
12/24/19 01:21
12/24/19 23:25
7440-22-4
Vanadium
ND
ug/L
5.0
1.3
1
12/24/19 01:21
12/24/19 23:25
7440-62-2
Zinc
ND
ug/L
10.0
3.9
1
12/24/19 01:21
12/24/19 23:25
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
ND
ug/L
0.10
0.060
1
12/24/19 02:04
12/30/19 19:45
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Acetone
ND
ug/L
25.0
6.2
1
12/23/19 18:57
67-64-1
Acrylonitrile
ND
ug/L
10.0
0.90
1
12/23/19 18:57
107-13-1
Benzene
ND
ug/L
1.0
0.15
1
12/23/19 18:57
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.34
1
12/23/19 18:57
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.26
1
12/23/19 18:57
75-27-4
Bromoform
ND
ug/L
1.0
0.62
1
12/23/19 18:57
75-25-2
Bromomethane
ND
ug/L
2.0
0.62
1
12/23/19 18:57
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
3.3
1
12/23/19 18:57
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.40
1
12/23/19 18:57
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.22
1
12/23/19 18:57
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.23
1
12/23/19 18:57
108-90-7
Chloroethane
ND
ug/L
1.0
0.49
1
12/23/19 18:57
75-00-3
Chloroform
ND
ug/L
5.0
2.3
1
12/23/19 18:57
67-66-3
Chloromethane
ND
ug/L
1.0
0.39
1
12/23/19 18:57
74-87-3
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
0.26
1
12/23/19 18:57
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.41
1
12/23/19 18:57
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.26
1
12/23/19 18:57
106-93-4
Dibromomethane
ND
ug/L
1.0
0.46
1
12/23/19 18:57
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.29
1
12/23/19 18:57
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.26
1
12/23/19 18:57
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.54
1
12/23/19 18:57
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.27
1
12/23/19 18:57
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.34
1
12/23/19 18:57
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.24
1
12/23/19 18:57
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
0.29
1
12/23/19 18:57
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
0.25
1
12/23/19 18:57
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.19
1
12/23/19 18:57
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 63
lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-3R
Lab ID:
92457590002
Collected:
12/12/19 13:45
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/23/19 18:57
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/23/19 18:57
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/23/19 18:57
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/23/19 18:57
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/23/19 18:57
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/23/19 18:57
74-88-4
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/23/19 18:57
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/23/19 18:57
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/23/19 18:57
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/23/19 18:57
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/23/19 18:57
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/23/19 18:57
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/23/19 18:57
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/23/19 18:57
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/23/19 18:57
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/23/19 18:57
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/23/19 18:57
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/23/19 18:57
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/23/19 18:57
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
12/23/19 18:57
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/23/19 18:57
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
1
12/23/19 18:57
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
12/23/19 18:57
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
12/23/19 18:57
2037-26-5
Date: 12/31 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-6 Lab ID: 92457590003 Collected: 12/12/19 14:07 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 12/31 /2019 11:05 AM
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
ND
ug/L
5.0
3.0
1
12/24/19 01:21
12/24/19 23:28
7440-36-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:28
7440-38-2
70.0
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:28
7440-39-3
ND
ug/L
1.0
0.20
1
12/24/19 01:21
12/24/19 23:28
7440-41-7
0.69J
ug/L
1.0
0.40
1
12/24/19 01:21
12/24/19 23:28
7440-43-9
ND
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:28
7440-47-3
34.2
ug/L
5.0
1.1
1
12/24/19 01:21
12/24/19 23:28
7440-48-4
ND
ug/L
5.0
2.1
1
12/24/19 01:21
12/24/19 23:28
7440-50-8
ND
ug/L
5.0
1.6
1
12/24/19 01:21
12/24/19 23:28
7439-92-1
2.5J
ug/L
5.0
0.90
1
12/24/19 01:21
12/24/19 23:28
7440-02-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:28
7782-49-2
ND
ug/L
5.0
2.5
1
12/24/19 01:21
12/24/19 23:28
7440-22-4
1.7J
ug/L
5.0
1.3
1
12/24/19 01:21
12/24/19 23:28
7440-62-2
ND
ug/L
10.0
3.9
1
12/24/19 01:21
12/24/19 23:28
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
0.46 ug/L 0.10 0.060 1 12/24/19 02:04 12/30/19 19:49 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
12/23/1919:15
67-64-1
ND
ug/L
10.0
0.90
1
12/23/1919:15
107-13-1
ND
ug/L
1.0
0.15
1
12/23/1919:15
71-43-2
ND
ug/L
1.0
0.34
1
12/23/1919:15
74-97-5
ND
ug/L
1.0
0.26
1
12/23/1919:15
75-27-4
ND
ug/L
1.0
0.62
1
12/23/1919:15
75-25-2
ND
ug/L
2.0
0.62
1
12/23/1919:15
74-83-9
ND
ug/L
5.0
3.3
1
12/23/1919:15
78-93-3
ND
ug/L
2.0
0.40
1
12/23/1919:15
75-15-0
ND
ug/L
1.0
0.22
1
12/23/1919:15
56-23-5
ND
ug/L
1.0
0.23
1
12/23/1919:15
108-90-7
ND
ug/L
1.0
0.49
1
12/23/1919:15
75-00-3
ND
ug/L
5.0
2.3
1
12/23/1919:15
67-66-3
ND
ug/L
1.0
0.39
1
12/23/1919:15
74-87-3
ND
ug/L
5.0
0.26
1
12/23/1919:15
96-12-8
ND
ug/L
1.0
0.41
1
12/23/1919:15
124-48-1
ND
ug/L
1.0
0.26
1
12/23/1919:15
106-93-4
ND
ug/L
1.0
0.46
1
12/23/1919:15
74-95-3
ND
ug/L
1.0
0.29
1
12/23/1919:15
95-50-1
ND
ug/L
1.0
0.26
1
12/23/1919:15
106-46-7
ND
ug/L
1.0
0.54
1
12/23/1919:15
110-57-6
ND
ug/L
1.0
0.27
1
12/23/1919:15
75-34-3
ND
ug/L
1.0
0.34
1
12/23/1919:15
107-06-2
ND
ug/L
1.0
0.24
1
12/23/1919:15
75-35-4
ND
ug/L
1.0
0.29
1
12/23/1919:15
156-59-2
ND
ug/L
1.0
0.25
1
12/23/1919:15
156-60-5
ND
ug/L
1.0
0.19
1
12/23/1919:15
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-6
Lab ID:
92457590003
Collected:
12/12/19 14:07
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/23/19 19:15
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/23/19 19:15
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/23/19 19:15
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/23/19 19:15
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/23/19 19:15
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/23/19 19:15
74-88-4
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/23/19 19:15
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/23/19 19:15
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/23/19 19:15
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/23/19 19:15
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/23/19 19:15
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/23/19 19:15
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/23/19 19:15
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/23/19 19:15
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/23/19 19:15
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/23/19 19:15
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/23/19 19:15
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/23/19 19:15
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/23/19 19:15
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
12/23/19 19:15
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/23/19 19:15
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
12/23/19 19:15
460-00-4
1,2-Dichloroethane-d4 (S)
98
%
70-130
1
12/23/19 19:15
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
12/23/19 19:15
2037-26-5
Date: 12/31 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-7 Lab ID: 92457590004 Collected: 12/12/19 14:09 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 12/31 /2019 11:05 AM
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
ND
ug/L
5.0
3.0
1
12/24/19 01:21
12/24/19 23:31
7440-36-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:31
7440-38-2
45.6
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:31
7440-39-3
0.28J
ug/L
1.0
0.20
1
12/24/19 01:21
12/24/19 23:31
7440-41-7 B
0.57J
ug/L
1.0
0.40
1
12/24/19 01:21
12/24/19 23:31
7440-43-9
ND
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:31
7440-47-3
46.0
ug/L
5.0
1.1
1
12/24/19 01:21
12/24/19 23:31
7440-48-4
ND
ug/L
5.0
2.1
1
12/24/19 01:21
12/24/19 23:31
7440-50-8
ND
ug/L
5.0
1.6
1
12/24/19 01:21
12/24/19 23:31
7439-92-1
ND
ug/L
5.0
0.90
1
12/24/19 01:21
12/24/19 23:31
7440-02-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:31
7782-49-2
ND
ug/L
5.0
2.5
1
12/24/19 01:21
12/24/19 23:31
7440-22-4
1.4J
ug/L
5.0
1.3
1
12/24/19 01:21
12/24/19 23:31
7440-62-2
7.9J
ug/L
10.0
3.9
1
12/24/19 01:21
12/24/19 23:31
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
0.13 ug/L 0.10 0.060 1 12/24/19 02:04 12/30/19 19:57 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
12/23/1919:33
67-64-1
ND
ug/L
10.0
0.90
1
12/23/1919:33
107-13-1
ND
ug/L
1.0
0.15
1
12/23/1919:33
71-43-2
ND
ug/L
1.0
0.34
1
12/23/1919:33
74-97-5
ND
ug/L
1.0
0.26
1
12/23/1919:33
75-27-4
ND
ug/L
1.0
0.62
1
12/23/1919:33
75-25-2
ND
ug/L
2.0
0.62
1
12/23/1919:33
74-83-9
ND
ug/L
5.0
3.3
1
12/23/1919:33
78-93-3
ND
ug/L
2.0
0.40
1
12/23/1919:33
75-15-0
ND
ug/L
1.0
0.22
1
12/23/1919:33
56-23-5
0.811
ug/L
1.0
0.23
1
12/23/1919:33
108-90-7
ND
ug/L
1.0
0.49
1
12/23/1919:33
75-00-3
ND
ug/L
5.0
2.3
1
12/23/1919:33
67-66-3
ND
ug/L
1.0
0.39
1
12/23/1919:33
74-87-3
ND
ug/L
5.0
0.26
1
12/23/1919:33
96-12-8
ND
ug/L
1.0
0.41
1
12/23/1919:33
124-48-1
ND
ug/L
1.0
0.26
1
12/23/1919:33
106-93-4
ND
ug/L
1.0
0.46
1
12/23/1919:33
74-95-3
ND
ug/L
1.0
0.29
1
12/23/1919:33
95-50-1
0.45J
ug/L
1.0
0.26
1
12/23/1919:33
106-46-7
ND
ug/L
1.0
0.54
1
12/23/1919:33
110-57-6
ND
ug/L
1.0
0.27
1
12/23/1919:33
75-34-3
ND
ug/L
1.0
0.34
1
12/23/1919:33
107-06-2
ND
ug/L
1.0
0.24
1
12/23/1919:33
75-35-4
ND
ug/L
1.0
0.29
1
12/23/1919:33
156-59-2
ND
ug/L
1.0
0.25
1
12/23/1919:33
156-60-5
ND
ug/L
1.0
0.19
1
12/23/1919:33
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-7
Lab ID:
92457590004
Collected:
12/12/19 14:09
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/23/19 19:33
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/23/19 19:33
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/23/19 19:33
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/23/19 19:33
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/23/19 19:33
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/23/19 19:33
74-88-4
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/23/19 19:33
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/23/19 19:33
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/23/19 19:33
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/23/19 19:33
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/23/19 19:33
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/23/19 19:33
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/23/19 19:33
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/23/19 19:33
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/23/19 19:33
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/23/19 19:33
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/23/19 19:33
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/23/19 19:33
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/23/19 19:33
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
12/23/19 19:33
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/23/19 19:33
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
12/23/19 19:33
460-00-4
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
12/23/19 19:33
17060-07-0
Toluene-d8 (S)
102
%
70-130
1
12/23/19 19:33
2037-26-5
Date: 12/31 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-9 Lab ID: 92457590005 Collected: 12/13/19 14:41 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 12/31 /2019 11:05 AM
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
ND
ug/L
5.0
3.0
1
12/24/19 01:21
12/24/19 23:34
7440-36-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:34
7440-38-2
43.4
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:34
7440-39-3
ND
ug/L
1.0
0.20
1
12/24/19 01:21
12/24/19 23:34
7440-41-7
1.3
ug/L
1.0
0.40
1
12/24/19 01:21
12/24/19 23:34
7440-43-9
ND
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:34
7440-47-3
180
ug/L
5.0
1.1
1
12/24/19 01:21
12/24/19 23:34
7440-48-4
ND
ug/L
5.0
2.1
1
12/24/19 01:21
12/24/19 23:34
7440-50-8
ND
ug/L
5.0
1.6
1
12/24/19 01:21
12/24/19 23:34
7439-92-1
6.9
ug/L
5.0
0.90
1
12/24/19 01:21
12/24/19 23:34
7440-02-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:34
7782-49-2
ND
ug/L
5.0
2.5
1
12/24/19 01:21
12/24/19 23:34
7440-22-4
1.91
ug/L
5.0
1.3
1
12/24/19 01:21
12/24/19 23:34
7440-62-2
ND
ug/L
10.0
3.9
1
12/24/19 01:21
12/24/19 23:34
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
0.34 ug/L 0.10 0.060 1 12/24/19 02:04 12/30/19 20:05 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
12/24/19 02:41
67-64-1
ND
ug/L
10.0
0.90
1
12/24/19 02:41
107-13-1
1.8
ug/L
1.0
0.15
1
12/24/19 02:41
71-43-2
ND
ug/L
1.0
0.34
1
12/24/19 02:41
74-97-5
ND
ug/L
1.0
0.26
1
12/24/19 02:41
75-27-4
ND
ug/L
1.0
0.62
1
12/24/19 02:41
75-25-2
ND
ug/L
2.0
0.62
1
12/24/19 02:41
74-83-9
ND
ug/L
5.0
3.3
1
12/24/19 02:41
78-93-3
ND
ug/L
2.0
0.40
1
12/24/19 02:41
75-15-0
ND
ug/L
1.0
0.22
1
12/24/19 02:41
56-23-5
1.6
ug/L
1.0
0.23
1
12/24/19 02:41
108-90-7
1.9
ug/L
1.0
0.49
1
12/24/19 02:41
75-00-3
ND
ug/L
5.0
2.3
1
12/24/19 02:41
67-66-3
ND
ug/L
1.0
0.39
1
12/24/19 02:41
74-87-3
ND
ug/L
5.0
0.26
1
12/24/19 02:41
96-12-8
ND
ug/L
1.0
0.41
1
12/24/19 02:41
124-48-1
ND
ug/L
1.0
0.26
1
12/24/19 02:41
106-93-4
ND
ug/L
1.0
0.46
1
12/24/19 02:41
74-95-3
1.4
ug/L
1.0
0.29
1
12/24/19 02:41
95-50-1
4.7
ug/L
1.0
0.26
1
12/24/19 02:41
106-46-7
ND
ug/L
1.0
0.54
1
12/24/19 02:41
110-57-6
1.3
ug/L
1.0
0.27
1
12/24/19 02:41
75-34-3
ND
ug/L
1.0
0.34
1
12/24/19 02:41
107-06-2
ND
ug/L
1.0
0.24
1
12/24/19 02:41
75-35-4
39.1
ug/L
1.0
0.29
1
12/24/19 02:41
156-59-2
ND
ug/L
1.0
0.25
1
12/24/19 02:41
156-60-5
ND
ug/L
1.0
0.19
1
12/24/19 02:41
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v2
v2
v2
Page 14 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-9
Lab ID:
92457590005
Collected:
12/13/19 14:41
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/24/19 02:41
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/24/19 02:41
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/24/19 02:41
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/24/19 02:41
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/24/19 02:41
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/24/19 02:41
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/24/19 02:41
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/24/19 02:41
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/24/19 02:41
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/24/19 02:41
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/24/19 02:41
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/24/19 02:41
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/24/19 02:41
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/24/19 02:41
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/24/19 02:41
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/24/19 02:41
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/24/19 02:41
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/24/19 02:41
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/24/19 02:41
108-05-4
Vinyl chloride
16.9
ug/L
1.0
0.24
1
12/24/19 02:41
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/24/19 02:41
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
104
%
70-130
1
12/24/19 02:41
460-00-4
1,2-Dichloroethane-d4 (S)
100
%
70-130
1
12/24/19 02:41
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
12/24/19 02:41
2037-26-5
Date: 12/31 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-11 Lab ID: 92457590006 Collected: 12/13/19 14:59 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 12/31 /2019 11:05 AM
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
ND
ug/L
5.0
3.0
1
12/24/19 01:21
12/24/19 23:37
7440-36-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:37
7440-38-2
40.1
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:37
7440-39-3
0.29J
ug/L
1.0
0.20
1
12/24/19 01:21
12/24/19 23:37
7440-41-7
1.4
ug/L
1.0
0.40
1
12/24/19 01:21
12/24/19 23:37
7440-43-9
ND
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:37
7440-47-3
17.7
ug/L
5.0
1.1
1
12/24/19 01:21
12/24/19 23:37
7440-48-4
2.8J
ug/L
5.0
2.1
1
12/24/19 01:21
12/24/19 23:37
7440-50-8
ND
ug/L
5.0
1.6
1
12/24/19 01:21
12/24/19 23:37
7439-92-1
2.6J
ug/L
5.0
0.90
1
12/24/19 01:21
12/24/19 23:37
7440-02-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:37
7782-49-2
ND
ug/L
5.0
2.5
1
12/24/19 01:21
12/24/19 23:37
7440-22-4
2.1J
ug/L
5.0
1.3
1
12/24/19 01:21
12/24/19 23:37
7440-62-2
20.6
ug/L
10.0
3.9
1
12/24/19 01:21
12/24/19 23:37
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
0.065J ug/L 0.10 0.060 1 12/24/19 02:04 12/30/19 20:20 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
12/24/19 02:59
67-64-1
ND
ug/L
10.0
0.90
1
12/24/19 02:59
107-13-1
0.41J
ug/L
1.0
0.15
1
12/24/19 02:59
71-43-2
ND
ug/L
1.0
0.34
1
12/24/19 02:59
74-97-5
ND
ug/L
1.0
0.26
1
12/24/19 02:59
75-27-4
ND
ug/L
1.0
0.62
1
12/24/19 02:59
75-25-2
ND
ug/L
2.0
0.62
1
12/24/19 02:59
74-83-9
ND
ug/L
5.0
3.3
1
12/24/19 02:59
78-93-3
ND
ug/L
2.0
0.40
1
12/24/19 02:59
75-15-0
ND
ug/L
1.0
0.22
1
12/24/19 02:59
56-23-5
1.0J
ug/L
1.0
0.23
1
12/24/19 02:59
108-90-7
ND
ug/L
1.0
0.49
1
12/24/19 02:59
75-00-3
ND
ug/L
5.0
2.3
1
12/24/19 02:59
67-66-3
ND
ug/L
1.0
0.39
1
12/24/19 02:59
74-87-3
ND
ug/L
5.0
0.26
1
12/24/19 02:59
96-12-8
ND
ug/L
1.0
0.41
1
12/24/19 02:59
124-48-1
ND
ug/L
1.0
0.26
1
12/24/19 02:59
106-93-4
ND
ug/L
1.0
0.46
1
12/24/19 02:59
74-95-3
ND
ug/L
1.0
0.29
1
12/24/19 02:59
95-50-1
2.2
ug/L
1.0
0.26
1
12/24/19 02:59
106-46-7
ND
ug/L
1.0
0.54
1
12/24/19 02:59
110-57-6
ND
ug/L
1.0
0.27
1
12/24/19 02:59
75-34-3
ND
ug/L
1.0
0.34
1
12/24/19 02:59
107-06-2
ND
ug/L
1.0
0.24
1
12/24/19 02:59
75-35-4
0.66J
ug/L
1.0
0.29
1
12/24/19 02:59
156-59-2
ND
ug/L
1.0
0.25
1
12/24/19 02:59
156-60-5
0.73J
ug/L
1.0
0.19
1
12/24/19 02:59
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
B
v2
v2
v2
Page 16 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-11
Lab ID:
92457590006
Collected:
12/13/19 14:59
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/24/19 02:59
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/24/19 02:59
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/24/19 02:59
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/24/19 02:59
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/24/19 02:59
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/24/19 02:59
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/24/19 02:59
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/24/19 02:59
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/24/19 02:59
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/24/19 02:59
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/24/19 02:59
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/24/19 02:59
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/24/19 02:59
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/24/19 02:59
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/24/19 02:59
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/24/19 02:59
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/24/19 02:59
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/24/19 02:59
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/24/19 02:59
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
12/24/19 02:59
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/24/19 02:59
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
12/24/19 02:59
460-00-4
1,2-Dichloroethane-d4 (S)
102
%
70-130
1
12/24/19 02:59
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
12/24/19 02:59
2037-26-5
Date: 12/31 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-13 Lab ID: 92457590007 Collected: 12/13/19 13:53 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 12/31 /2019 11:05 AM
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
ND
ug/L
5.0
3.0
1
12/24/19 01:21
12/24/19 23:40
7440-36-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:40
7440-38-2
20.2
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:40
7440-39-3
0.26J
ug/L
1.0
0.20
1
12/24/19 01:21
12/24/19 23:40
7440-41-7
ND
ug/L
1.0
0.40
1
12/24/19 01:21
12/24/19 23:40
7440-43-9
ND
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:40
7440-47-3
ND
ug/L
5.0
1.1
1
12/24/19 01:21
12/24/19 23:40
7440-48-4
ND
ug/L
5.0
2.1
1
12/24/19 01:21
12/24/19 23:40
7440-50-8
ND
ug/L
5.0
1.6
1
12/24/19 01:21
12/24/19 23:40
7439-92-1
ND
ug/L
5.0
0.90
1
12/24/19 01:21
12/24/19 23:40
7440-02-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:40
7782-49-2
ND
ug/L
5.0
2.5
1
12/24/19 01:21
12/24/19 23:40
7440-22-4
ND
ug/L
5.0
1.3
1
12/24/19 01:21
12/24/19 23:40
7440-62-2
4.6J
ug/L
10.0
3.9
1
12/24/19 01:21
12/24/19 23:40
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 0.10 0.060 1 12/24/19 02:04 12/30/19 20:28 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
12/24/19 03:17
67-64-1
ND
ug/L
10.0
0.90
1
12/24/19 03:17
107-13-1
ND
ug/L
1.0
0.15
1
12/24/19 03:17
71-43-2
ND
ug/L
1.0
0.34
1
12/24/19 03:17
74-97-5
ND
ug/L
1.0
0.26
1
12/24/19 03:17
75-27-4
ND
ug/L
1.0
0.62
1
12/24/19 03:17
75-25-2
ND
ug/L
2.0
0.62
1
12/24/19 03:17
74-83-9
ND
ug/L
5.0
3.3
1
12/24/19 03:17
78-93-3
ND
ug/L
2.0
0.40
1
12/24/19 03:17
75-15-0
ND
ug/L
1.0
0.22
1
12/24/19 03:17
56-23-5
ND
ug/L
1.0
0.23
1
12/24/19 03:17
108-90-7
ND
ug/L
1.0
0.49
1
12/24/19 03:17
75-00-3
ND
ug/L
5.0
2.3
1
12/24/19 03:17
67-66-3
ND
ug/L
1.0
0.39
1
12/24/19 03:17
74-87-3
ND
ug/L
5.0
0.26
1
12/24/19 03:17
96-12-8
ND
ug/L
1.0
0.41
1
12/24/19 03:17
124-48-1
ND
ug/L
1.0
0.26
1
12/24/19 03:17
106-93-4
ND
ug/L
1.0
0.46
1
12/24/19 03:17
74-95-3
ND
ug/L
1.0
0.29
1
12/24/19 03:17
95-50-1
ND
ug/L
1.0
0.26
1
12/24/19 03:17
106-46-7
ND
ug/L
1.0
0.54
1
12/24/19 03:17
110-57-6
ND
ug/L
1.0
0.27
1
12/24/19 03:17
75-34-3
ND
ug/L
1.0
0.34
1
12/24/19 03:17
107-06-2
ND
ug/L
1.0
0.24
1
12/24/19 03:17
75-35-4
ND
ug/L
1.0
0.29
1
12/24/19 03:17
156-59-2
ND
ug/L
1.0
0.25
1
12/24/19 03:17
156-60-5
ND
ug/L
1.0
0.19
1
12/24/19 03:17
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
B
v2
v2
v2
Page 18 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-13
Lab ID:
92457590007
Collected:
12/13/19 13:53
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/24/19 03:17
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/24/19 03:17
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/24/19 03:17
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/24/19 03:17
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/24/19 03:17
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/24/19 03:17
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/24/19 03:17
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/24/19 03:17
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/24/19 03:17
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/24/19 03:17
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/24/19 03:17
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/24/19 03:17
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/24/19 03:17
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/24/19 03:17
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/24/19 03:17
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/24/19 03:17
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/24/19 03:17
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/24/19 03:17
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/24/19 03:17
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
12/24/19 03:17
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/24/19 03:17
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
12/24/19 03:17
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
12/24/19 03:17
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
12/24/19 03:17
2037-26-5
Date: 12/31 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-14 Lab ID: 92457590008 Collected: 12/13/19 10:10 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 12/31 /2019 11:05 AM
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
ND
ug/L
5.0
3.0
1
12/24/19 01:21
12/24/19 23:44
7440-36-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:44
7440-38-2
25.3
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:44
7440-39-3
ND
ug/L
1.0
0.20
1
12/24/19 01:21
12/24/19 23:44
7440-41-7
0.59J
ug/L
1.0
0.40
1
12/24/19 01:21
12/24/19 23:44
7440-43-9
ND
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:44
7440-47-3
ND
ug/L
5.0
1.1
1
12/24/19 01:21
12/24/19 23:44
7440-48-4
ND
ug/L
5.0
2.1
1
12/24/19 01:21
12/24/19 23:44
7440-50-8
ND
ug/L
5.0
1.6
1
12/24/19 01:21
12/24/19 23:44
7439-92-1
1.6J
ug/L
5.0
0.90
1
12/24/19 01:21
12/24/19 23:44
7440-02-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:44
7782-49-2
ND
ug/L
5.0
2.5
1
12/24/19 01:21
12/24/19 23:44
7440-22-4
ND
ug/L
5.0
1.3
1
12/24/19 01:21
12/24/19 23:44
7440-62-2
4.7J
ug/L
10.0
3.9
1
12/24/19 01:21
12/24/19 23:44
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 0.10 0.060 1 12/24/19 02:04 12/30/19 20:32 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
12/24/19 03:35
67-64-1
ND
ug/L
10.0
0.90
1
12/24/19 03:35
107-13-1
ND
ug/L
1.0
0.15
1
12/24/19 03:35
71-43-2
ND
ug/L
1.0
0.34
1
12/24/19 03:35
74-97-5
ND
ug/L
1.0
0.26
1
12/24/19 03:35
75-27-4
ND
ug/L
1.0
0.62
1
12/24/19 03:35
75-25-2
ND
ug/L
2.0
0.62
1
12/24/19 03:35
74-83-9
ND
ug/L
5.0
3.3
1
12/24/19 03:35
78-93-3
ND
ug/L
2.0
0.40
1
12/24/19 03:35
75-15-0
ND
ug/L
1.0
0.22
1
12/24/19 03:35
56-23-5
ND
ug/L
1.0
0.23
1
12/24/19 03:35
108-90-7
ND
ug/L
1.0
0.49
1
12/24/19 03:35
75-00-3
ND
ug/L
5.0
2.3
1
12/24/19 03:35
67-66-3
ND
ug/L
1.0
0.39
1
12/24/19 03:35
74-87-3
ND
ug/L
5.0
0.26
1
12/24/19 03:35
96-12-8
ND
ug/L
1.0
0.41
1
12/24/19 03:35
124-48-1
ND
ug/L
1.0
0.26
1
12/24/19 03:35
106-93-4
ND
ug/L
1.0
0.46
1
12/24/19 03:35
74-95-3
ND
ug/L
1.0
0.29
1
12/24/19 03:35
95-50-1
ND
ug/L
1.0
0.26
1
12/24/19 03:35
106-46-7
ND
ug/L
1.0
0.54
1
12/24/19 03:35
110-57-6
2.0
ug/L
1.0
0.27
1
12/24/19 03:35
75-34-3
ND
ug/L
1.0
0.34
1
12/24/19 03:35
107-06-2
ND
ug/L
1.0
0.24
1
12/24/19 03:35
75-35-4
4.8
ug/L
1.0
0.29
1
12/24/19 03:35
156-59-2
ND
ug/L
1.0
0.25
1
12/24/19 03:35
156-60-5
ND
ug/L
1.0
0.19
1
12/24/19 03:35
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v2
v2
v2
Page 20 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-14
Lab ID:
92457590008
Collected:
12/13/19 10:10
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/24/19 03:35
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/24/19 03:35
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/24/19 03:35
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/24/19 03:35
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/24/19 03:35
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/24/19 03:35
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/24/19 03:35
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/24/19 03:35
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/24/19 03:35
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/24/19 03:35
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/24/19 03:35
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/24/19 03:35
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/24/19 03:35
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/24/19 03:35
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/24/19 03:35
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/24/19 03:35
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/24/19 03:35
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/24/19 03:35
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/24/19 03:35
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
12/24/19 03:35
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/24/19 03:35
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
12/24/19 03:35
460-00-4
1,2-Dichloroethane-d4 (S)
98
%
70-130
1
12/24/19 03:35
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
12/24/19 03:35
2037-26-5
Date: 12/31 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 21 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-15 Lab ID: 92457590009 Collected: 12/12/19 13:57 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 12/31 /2019 11:05 AM
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
ND
ug/L
5.0
3.0
1
12/24/19 01:21
12/24/19 23:47
7440-36-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:47
7440-38-2
50.5
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:47
7440-39-3
0.42J
ug/L
1.0
0.20
1
12/24/19 01:21
12/24/19 23:47
7440-41-7 B
1.2
ug/L
1.0
0.40
1
12/24/19 01:21
12/24/19 23:47
7440-43-9
ND
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:47
7440-47-3
2.5J
ug/L
5.0
1.1
1
12/24/19 01:21
12/24/19 23:47
7440-48-4
ND
ug/L
5.0
2.1
1
12/24/19 01:21
12/24/19 23:47
7440-50-8
ND
ug/L
5.0
1.6
1
12/24/19 01:21
12/24/19 23:47
7439-92-1
2.2J
ug/L
5.0
0.90
1
12/24/19 01:21
12/24/19 23:47
7440-02-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:47
7782-49-2
ND
ug/L
5.0
2.5
1
12/24/19 01:21
12/24/19 23:47
7440-22-4
3.2J
ug/L
5.0
1.3
1
12/24/19 01:21
12/24/19 23:47
7440-62-2
8.5J
ug/L
10.0
3.9
1
12/24/19 01:21
12/24/19 23:47
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
0.097J ug/L 0.10 0.060 1 12/24/19 02:04 12/30/19 20:36 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
12/23/1919:50
67-64-1
ND
ug/L
10.0
0.90
1
12/23/1919:50
107-13-1
0.30J
ug/L
1.0
0.15
1
12/23/1919:50
71-43-2
ND
ug/L
1.0
0.34
1
12/23/1919:50
74-97-5
ND
ug/L
1.0
0.26
1
12/23/1919:50
75-27-4
ND
ug/L
1.0
0.62
1
12/23/1919:50
75-25-2
ND
ug/L
2.0
0.62
1
12/23/1919:50
74-83-9
ND
ug/L
5.0
3.3
1
12/23/1919:50
78-93-3
ND
ug/L
2.0
0.40
1
12/23/1919:50
75-15-0
ND
ug/L
1.0
0.22
1
12/23/1919:50
56-23-5
2.1
ug/L
1.0
0.23
1
12/23/1919:50
108-90-7
ND
ug/L
1.0
0.49
1
12/23/1919:50
75-00-3
ND
ug/L
5.0
2.3
1
12/23/1919:50
67-66-3
ND
ug/L
1.0
0.39
1
12/23/1919:50
74-87-3
ND
ug/L
5.0
0.26
1
12/23/1919:50
96-12-8
ND
ug/L
1.0
0.41
1
12/23/1919:50
124-48-1
ND
ug/L
1.0
0.26
1
12/23/1919:50
106-93-4
ND
ug/L
1.0
0.46
1
12/23/1919:50
74-95-3
ND
ug/L
1.0
0.29
1
12/23/1919:50
95-50-1
2.9
ug/L
1.0
0.26
1
12/23/1919:50
106-46-7
ND
ug/L
1.0
0.54
1
12/23/1919:50
110-57-6
5.4
ug/L
1.0
0.27
1
12/23/1919:50
75-34-3
ND
ug/L
1.0
0.34
1
12/23/1919:50
107-06-2
ND
ug/L
1.0
0.24
1
12/23/1919:50
75-35-4
22.9
ug/L
1.0
0.29
1
12/23/1919:50
156-59-2
ND
ug/L
1.0
0.25
1
12/23/1919:50
156-60-5
ND
ug/L
1.0
0.19
1
12/23/1919:50
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 22 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-15
Lab ID:
92457590009
Collected:
12/12/19 13:57
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/23/19 19:50
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/23/19 19:50
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/23/19 19:50
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/23/19 19:50
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/23/19 19:50
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/23/19 19:50
74-88-4
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/23/19 19:50
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/23/19 19:50
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/23/19 19:50
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/23/19 19:50
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/23/19 19:50
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/23/19 19:50
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/23/19 19:50
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/23/19 19:50
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/23/19 19:50
79-00-5
Trichloroethene
1.9
ug/L
1.0
0.22
1
12/23/19 19:50
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/23/19 19:50
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/23/19 19:50
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/23/19 19:50
108-05-4
Vinyl chloride
1.7
ug/L
1.0
0.24
1
12/23/19 19:50
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/23/19 19:50
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
12/23/19 19:50
460-00-4
1,2-Dichloroethane-d4 (S)
98
%
70-130
1
12/23/19 19:50
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
12/23/19 19:50
2037-26-5
Date: 12/31 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 23 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-16 Lab ID: 92457590010 Collected: 12/12/19 13:50 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 12/31 /2019 11:05 AM
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
ND
ug/L
5.0
3.0
1
12/24/19 01:21
12/24/19 23:50
7440-36-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:50
7440-38-2
99.5
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:50
7440-39-3
ND
ug/L
1.0
0.20
1
12/24/19 01:21
12/24/19 23:50
7440-41-7
1.5
ug/L
1.0
0.40
1
12/24/19 01:21
12/24/19 23:50
7440-43-9
ND
ug/L
25.0
5.0
5
12/24/19 01:21
12/26/19 16:45
7440-47-3 D3
376
ug/L
5.0
1.1
1
12/24/19 01:21
12/24/19 23:50
7440-48-4
4.4J
ug/L
5.0
2.1
1
12/24/19 01:21
12/24/19 23:50
7440-50-8
2.3J
ug/L
5.0
1.6
1
12/24/19 01:21
12/24/19 23:50
7439-92-1
19.4
ug/L
5.0
0.90
1
12/24/19 01:21
12/24/19 23:50
7440-02-0
12.4
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:50
7782-49-2
ND
ug/L
5.0
2.5
1
12/24/19 01:21
12/24/19 23:50
7440-22-4
2.7J
ug/L
5.0
1.3
1
12/24/19 01:21
12/24/19 23:50
7440-62-2
12.1
ug/L
10.0
3.9
1
12/24/19 01:21
12/24/19 23:50
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
0.28 ug/L 0.10 0.060 1 12/24/19 02:04 12/30/19 20:40 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
12/23/19 20:08
67-64-1
ND
ug/L
10.0
0.90
1
12/23/19 20:08
107-13-1
0.96J
ug/L
1.0
0.15
1
12/23/19 20:08
71-43-2
ND
ug/L
1.0
0.34
1
12/23/19 20:08
74-97-5
ND
ug/L
1.0
0.26
1
12/23/19 20:08
75-27-4
ND
ug/L
1.0
0.62
1
12/23/19 20:08
75-25-2
ND
ug/L
2.0
0.62
1
12/23/19 20:08
74-83-9
ND
ug/L
5.0
3.3
1
12/23/19 20:08
78-93-3
ND
ug/L
2.0
0.40
1
12/23/19 20:08
75-15-0
ND
ug/L
1.0
0.22
1
12/23/19 20:08
56-23-5
3.5
ug/L
1.0
0.23
1
12/23/19 20:08
108-90-7
ND
ug/L
1.0
0.49
1
12/23/19 20:08
75-00-3
ND
ug/L
5.0
2.3
1
12/23/19 20:08
67-66-3
ND
ug/L
1.0
0.39
1
12/23/19 20:08
74-87-3
ND
ug/L
5.0
0.26
1
12/23/19 20:08
96-12-8
ND
ug/L
1.0
0.41
1
12/23/19 20:08
124-48-1
ND
ug/L
1.0
0.26
1
12/23/19 20:08
106-93-4
ND
ug/L
1.0
0.46
1
12/23/19 20:08
74-95-3
0.70J
ug/L
1.0
0.29
1
12/23/19 20:08
95-50-1
7.5
ug/L
1.0
0.26
1
12/23/19 20:08
106-46-7
ND
ug/L
1.0
0.54
1
12/23/19 20:08
110-57-6
0.56J
ug/L
1.0
0.27
1
12/23/19 20:08
75-34-3
1.4
ug/L
1.0
0.34
1
12/23/19 20:08
107-06-2
ND
ug/L
1.0
0.24
1
12/23/19 20:08
75-35-4
10.5
ug/L
1.0
0.29
1
12/23/19 20:08
156-59-2
ND
ug/L
1.0
0.25
1
12/23/19 20:08
156-60-5
ND
ug/L
1.0
0.19
1
12/23/19 20:08
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 24 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-16
Lab ID:
92457590010
Collected:
12/12/19 13:50
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/23/19 20:08
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/23/19 20:08
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/23/19 20:08
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/23/19 20:08
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/23/19 20:08
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/23/19 20:08
74-88-4
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/23/19 20:08
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/23/19 20:08
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/23/19 20:08
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/23/19 20:08
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/23/19 20:08
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/23/19 20:08
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/23/19 20:08
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/23/19 20:08
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/23/19 20:08
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/23/19 20:08
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/23/19 20:08
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/23/19 20:08
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/23/19 20:08
108-05-4
Vinyl chloride
1.2
ug/L
1.0
0.24
1
12/23/19 20:08
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/23/19 20:08
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
12/23/19 20:08
460-00-4
1,2-Dichloroethane-d4 (S)
101
%
70-130
1
12/23/19 20:08
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
12/23/19 20:08
2037-26-5
Date: 12/31 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 25 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-17 Lab ID: 92457590011 Collected: 12/13/19 13:15 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 12/31 /2019 11:05 AM
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
ND
ug/L
5.0
3.0
1
12/24/19 01:21
12/24/19 23:53
7440-36-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:53
7440-38-2
23.9
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:53
7440-39-3
ND
ug/L
1.0
0.20
1
12/24/19 01:21
12/24/19 23:53
7440-41-7
1.3
ug/L
1.0
0.40
1
12/24/19 01:21
12/24/19 23:53
7440-43-9
ND
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:53
7440-47-3
1.5J
ug/L
5.0
1.1
1
12/24/19 01:21
12/24/19 23:53
7440-48-4
ND
ug/L
5.0
2.1
1
12/24/19 01:21
12/24/19 23:53
7440-50-8
ND
ug/L
5.0
1.6
1
12/24/19 01:21
12/24/19 23:53
7439-92-1
3.1J
ug/L
5.0
0.90
1
12/24/19 01:21
12/24/19 23:53
7440-02-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:53
7782-49-2
ND
ug/L
5.0
2.5
1
12/24/19 01:21
12/24/19 23:53
7440-22-4
2.5J
ug/L
5.0
1.3
1
12/24/19 01:21
12/24/19 23:53
7440-62-2
ND
ug/L
10.0
3.9
1
12/24/19 01:21
12/24/19 23:53
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
0.068J ug/L 0.10 0.060 1 12/24/19 02:04 12/30/19 20:48 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
12/24/19 03:53
67-64-1
ND
ug/L
10.0
0.90
1
12/24/19 03:53
107-13-1
ND
ug/L
1.0
0.15
1
12/24/19 03:53
71-43-2
ND
ug/L
1.0
0.34
1
12/24/19 03:53
74-97-5
ND
ug/L
1.0
0.26
1
12/24/19 03:53
75-27-4
ND
ug/L
1.0
0.62
1
12/24/19 03:53
75-25-2
ND
ug/L
2.0
0.62
1
12/24/19 03:53
74-83-9
ND
ug/L
5.0
3.3
1
12/24/19 03:53
78-93-3
ND
ug/L
2.0
0.40
1
12/24/19 03:53
75-15-0
ND
ug/L
1.0
0.22
1
12/24/19 03:53
56-23-5
ND
ug/L
1.0
0.23
1
12/24/19 03:53
108-90-7
ND
ug/L
1.0
0.49
1
12/24/19 03:53
75-00-3
ND
ug/L
5.0
2.3
1
12/24/19 03:53
67-66-3
ND
ug/L
1.0
0.39
1
12/24/19 03:53
74-87-3
ND
ug/L
5.0
0.26
1
12/24/19 03:53
96-12-8
ND
ug/L
1.0
0.41
1
12/24/19 03:53
124-48-1
ND
ug/L
1.0
0.26
1
12/24/19 03:53
106-93-4
ND
ug/L
1.0
0.46
1
12/24/19 03:53
74-95-3
ND
ug/L
1.0
0.29
1
12/24/19 03:53
95-50-1
ND
ug/L
1.0
0.26
1
12/24/19 03:53
106-46-7
ND
ug/L
1.0
0.54
1
12/24/19 03:53
110-57-6
ND
ug/L
1.0
0.27
1
12/24/19 03:53
75-34-3
ND
ug/L
1.0
0.34
1
12/24/19 03:53
107-06-2
ND
ug/L
1.0
0.24
1
12/24/19 03:53
75-35-4
ND
ug/L
1.0
0.29
1
12/24/19 03:53
156-59-2
ND
ug/L
1.0
0.25
1
12/24/19 03:53
156-60-5
ND
ug/L
1.0
0.19
1
12/24/19 03:53
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v2
v2
v2
Page 26 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-17
Lab ID:
92457590011
Collected:
12/13/19 13:15
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/24/19 03:53
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/24/19 03:53
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/24/19 03:53
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/24/19 03:53
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/24/19 03:53
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/24/19 03:53
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/24/19 03:53
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/24/19 03:53
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/24/19 03:53
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/24/19 03:53
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/24/19 03:53
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/24/19 03:53
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/24/19 03:53
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/24/19 03:53
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/24/19 03:53
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/24/19 03:53
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/24/19 03:53
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/24/19 03:53
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/24/19 03:53
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
12/24/19 03:53
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/24/19 03:53
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
101
%
70-130
1
12/24/19 03:53
460-00-4
1,2-Dichloroethane-d4 (S)
99
%
70-130
1
12/24/19 03:53
17060-07-0
Toluene-d8 (S)
99
%
70-130
1
12/24/19 03:53
2037-26-5
Date: 12/31 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 27 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-19 Lab ID: 92457590012 Collected: 12/13/19 00:00 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 12/31 /2019 11:05 AM
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
ND
ug/L
5.0
3.0
1
12/24/19 01:21
12/25/19 00:03
7440-36-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/25/19 00:03
7440-38-2
45.7
ug/L
5.0
1.0
1
12/24/19 01:21
12/25/19 00:03
7440-39-3
0.30J
ug/L
1.0
0.20
1
12/24/19 01:21
12/25/19 00:03
7440-41-7
0.64J
ug/L
1.0
0.40
1
12/24/19 01:21
12/25/19 00:03
7440-43-9
ND
ug/L
5.0
1.0
1
12/24/19 01:21
12/25/19 00:03
7440-47-3
ND
ug/L
5.0
1.1
1
12/24/19 01:21
12/25/19 00:03
7440-48-4
2.5J
ug/L
5.0
2.1
1
12/24/19 01:21
12/25/19 00:03
7440-50-8
ND
ug/L
5.0
1.6
1
12/24/19 01:21
12/25/19 00:03
7439-92-1
1.2J
ug/L
5.0
0.90
1
12/24/19 01:21
12/25/19 00:03
7440-02-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/25/19 00:03
7782-49-2
ND
ug/L
5.0
2.5
1
12/24/19 01:21
12/25/19 00:03
7440-22-4
2.1J
ug/L
5.0
1.3
1
12/24/19 01:21
12/25/19 00:03
7440-62-2
7.7J
ug/L
10.0
3.9
1
12/24/19 01:21
12/25/19 00:03
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 0.10 0.060 1 12/24/19 02:04 12/30/19 20:56 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
12/24/19 04:11
67-64-1
ND
ug/L
10.0
0.90
1
12/24/19 04:11
107-13-1
ND
ug/L
1.0
0.15
1
12/24/19 04:11
71-43-2
ND
ug/L
1.0
0.34
1
12/24/19 04:11
74-97-5
ND
ug/L
1.0
0.26
1
12/24/19 04:11
75-27-4
ND
ug/L
1.0
0.62
1
12/24/19 04:11
75-25-2
ND
ug/L
2.0
0.62
1
12/24/19 04:11
74-83-9
ND
ug/L
5.0
3.3
1
12/24/19 04:11
78-93-3
ND
ug/L
2.0
0.40
1
12/24/19 04:11
75-15-0
ND
ug/L
1.0
0.22
1
12/24/19 04:11
56-23-5
ND
ug/L
1.0
0.23
1
12/24/19 04:11
108-90-7
ND
ug/L
1.0
0.49
1
12/24/19 04:11
75-00-3
ND
ug/L
5.0
2.3
1
12/24/19 04:11
67-66-3
ND
ug/L
1.0
0.39
1
12/24/19 04:11
74-87-3
ND
ug/L
5.0
0.26
1
12/24/19 04:11
96-12-8
ND
ug/L
1.0
0.41
1
12/24/19 04:11
124-48-1
ND
ug/L
1.0
0.26
1
12/24/19 04:11
106-93-4
ND
ug/L
1.0
0.46
1
12/24/19 04:11
74-95-3
ND
ug/L
1.0
0.29
1
12/24/19 04:11
95-50-1
ND
ug/L
1.0
0.26
1
12/24/19 04:11
106-46-7
ND
ug/L
1.0
0.54
1
12/24/19 04:11
110-57-6
ND
ug/L
1.0
0.27
1
12/24/19 04:11
75-34-3
ND
ug/L
1.0
0.34
1
12/24/19 04:11
107-06-2
ND
ug/L
1.0
0.24
1
12/24/19 04:11
75-35-4
0.47J
ug/L
1.0
0.29
1
12/24/19 04:11
156-59-2
ND
ug/L
1.0
0.25
1
12/24/19 04:11
156-60-5
ND
ug/L
1.0
0.19
1
12/24/19 04:11
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
B
v2
v2
v2
Page 28 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-19
Lab ID:
92457590012
Collected:
12/13/19 00:00
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/24/19 04:11
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/24/19 04:11
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/24/19 04:11
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/24/19 04:11
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/24/19 04:11
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/24/19 04:11
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/24/19 04:11
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/24/19 04:11
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/24/19 04:11
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/24/19 04:11
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/24/19 04:11
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/24/19 04:11
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/24/19 04:11
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/24/19 04:11
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/24/19 04:11
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/24/19 04:11
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/24/19 04:11
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/24/19 04:11
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/24/19 04:11
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
12/24/19 04:11
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/24/19 04:11
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
103
%
70-130
1
12/24/19 04:11
460-00-4
1,2-Dichloroethane-d4 (S)
96
%
70-130
1
12/24/19 04:11
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
12/24/19 04:11
2037-26-5
Date: 12/31 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 29 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-20 Lab ID: 92457590013 Collected: 12/13/19 14:28 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 12/31 /2019 11:05 AM
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
ND
ug/L
5.0
3.0
1
12/24/19 01:21
12/25/19 00:06
7440-36-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/25/19 00:06
7440-38-2
43.0
ug/L
5.0
1.0
1
12/24/19 01:21
12/25/19 00:06
7440-39-3
0.42J
ug/L
1.0
0.20
1
12/24/19 01:21
12/25/19 00:06
7440-41-7
4.5
ug/L
1.0
0.40
1
12/24/19 01:21
12/25/19 00:06
7440-43-9
ND
ug/L
5.0
1.0
1
12/24/19 01:21
12/25/19 00:06
7440-47-3
47.4
ug/L
5.0
1.1
1
12/24/19 01:21
12/25/19 00:06
7440-48-4
2.7J
ug/L
5.0
2.1
1
12/24/19 01:21
12/25/19 00:06
7440-50-8
ND
ug/L
5.0
1.6
1
12/24/19 01:21
12/25/19 00:06
7439-92-1
3.9J
ug/L
5.0
0.90
1
12/24/19 01:21
12/25/19 00:06
7440-02-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/25/19 00:06
7782-49-2
ND
ug/L
5.0
2.5
1
12/24/19 01:21
12/25/19 00:06
7440-22-4
3.7J
ug/L
5.0
1.3
1
12/24/19 01:21
12/25/19 00:06
7440-62-2
15.0
ug/L
10.0
3.9
1
12/24/19 01:21
12/25/19 00:06
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
0.57 ug/L 0.10 0.060 1 12/24/19 02:04 12/30/19 21:07 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
12/24/19 04:28
67-64-1
ND
ug/L
10.0
0.90
1
12/24/19 04:28
107-13-1
0.73J
ug/L
1.0
0.15
1
12/24/19 04:28
71-43-2
ND
ug/L
1.0
0.34
1
12/24/19 04:28
74-97-5
ND
ug/L
1.0
0.26
1
12/24/19 04:28
75-27-4
ND
ug/L
1.0
0.62
1
12/24/19 04:28
75-25-2
ND
ug/L
2.0
0.62
1
12/24/19 04:28
74-83-9
ND
ug/L
5.0
3.3
1
12/24/19 04:28
78-93-3
ND
ug/L
2.0
0.40
1
12/24/19 04:28
75-15-0
ND
ug/L
1.0
0.22
1
12/24/19 04:28
56-23-5
0.82J
ug/L
1.0
0.23
1
12/24/19 04:28
108-90-7
0.60J
ug/L
1.0
0.49
1
12/24/19 04:28
75-00-3
ND
ug/L
5.0
2.3
1
12/24/19 04:28
67-66-3
ND
ug/L
1.0
0.39
1
12/24/19 04:28
74-87-3
ND
ug/L
5.0
0.26
1
12/24/19 04:28
96-12-8
ND
ug/L
1.0
0.41
1
12/24/19 04:28
124-48-1
ND
ug/L
1.0
0.26
1
12/24/19 04:28
106-93-4
ND
ug/L
1.0
0.46
1
12/24/19 04:28
74-95-3
0.891
ug/L
1.0
0.29
1
12/24/19 04:28
95-50-1
2.1
ug/L
1.0
0.26
1
12/24/19 04:28
106-46-7
ND
ug/L
1.0
0.54
1
12/24/19 04:28
110-57-6
0.73J
ug/L
1.0
0.27
1
12/24/19 04:28
75-34-3
ND
ug/L
1.0
0.34
1
12/24/19 04:28
107-06-2
ND
ug/L
1.0
0.24
1
12/24/19 04:28
75-35-4
5.1
ug/L
1.0
0.29
1
12/24/19 04:28
156-59-2
ND
ug/L
1.0
0.25
1
12/24/19 04:28
156-60-5
ND
ug/L
1.0
0.19
1
12/24/19 04:28
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
B
v2
v2
v2
Page 30 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-20
Lab ID:
92457590013
Collected:
12/13/19 14:28
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/24/19 04:28
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/24/19 04:28
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/24/19 04:28
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/24/19 04:28
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/24/19 04:28
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/24/19 04:28
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/24/19 04:28
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/24/19 04:28
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/24/19 04:28
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/24/19 04:28
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/24/19 04:28
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/24/19 04:28
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/24/19 04:28
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/24/19 04:28
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/24/19 04:28
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/24/19 04:28
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/24/19 04:28
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/24/19 04:28
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/24/19 04:28
108-05-4
Vinyl chloride
2.5
ug/L
1.0
0.24
1
12/24/19 04:28
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/24/19 04:28
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
12/24/19 04:28
460-00-4
1,2-Dichloroethane-d4 (S)
96
%
70-130
1
12/24/19 04:28
17060-07-0
Toluene-d8 (S)
98
%
70-130
1
12/24/19 04:28
2037-26-5
Date: 12/31 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 31 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-21 Lab ID: 92457590014 Collected: 12/12/19 14:34 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 12/31 /2019 11:05 AM
Analytical Method: EPA 601 OD Preparation Method: EPA 301 OA
ND
ug/L
5.0
3.0
1
12/24/19 01:21
12/25/19 00:09
7440-36-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/25/19 00:09
7440-38-2
57.3
ug/L
5.0
1.0
1
12/24/19 01:21
12/25/19 00:09
7440-39-3
ND
ug/L
1.0
0.20
1
12/24/19 01:21
12/25/19 00:09
7440-41-7
ND
ug/L
1.0
0.40
1
12/24/19 01:21
12/25/19 00:09
7440-43-9
ND
ug/L
5.0
1.0
1
12/24/19 01:21
12/25/19 00:09
7440-47-3
4.OJ
ug/L
5.0
1.1
1
12/24/19 01:21
12/25/19 00:09
7440-48-4
ND
ug/L
5.0
2.1
1
12/24/19 01:21
12/25/19 00:09
7440-50-8
ND
ug/L
5.0
1.6
1
12/24/19 01:21
12/25/19 00:09
7439-92-1
1.3J
ug/L
5.0
0.90
1
12/24/19 01:21
12/25/19 00:09
7440-02-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/25/19 00:09
7782-49-2
ND
ug/L
5.0
2.5
1
12/24/19 01:21
12/25/19 00:09
7440-22-4
ND
ug/L
5.0
1.3
1
12/24/19 01:21
12/25/19 00:09
7440-62-2
4.7J
ug/L
10.0
3.9
1
12/24/19 01:21
12/25/19 00:09
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 0.10 0.060 1 12/24/19 02:04 12/30/19 21:15 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
12/23/19 20:26
67-64-1
ND
ug/L
10.0
0.90
1
12/23/19 20:26
107-13-1
ND
ug/L
1.0
0.15
1
12/23/19 20:26
71-43-2
ND
ug/L
1.0
0.34
1
12/23/19 20:26
74-97-5
ND
ug/L
1.0
0.26
1
12/23/19 20:26
75-27-4
ND
ug/L
1.0
0.62
1
12/23/19 20:26
75-25-2
ND
ug/L
2.0
0.62
1
12/23/19 20:26
74-83-9
ND
ug/L
5.0
3.3
1
12/23/19 20:26
78-93-3
ND
ug/L
2.0
0.40
1
12/23/19 20:26
75-15-0
ND
ug/L
1.0
0.22
1
12/23/19 20:26
56-23-5
ND
ug/L
1.0
0.23
1
12/23/19 20:26
108-90-7
ND
ug/L
1.0
0.49
1
12/23/19 20:26
75-00-3
ND
ug/L
5.0
2.3
1
12/23/19 20:26
67-66-3
ND
ug/L
1.0
0.39
1
12/23/19 20:26
74-87-3
ND
ug/L
5.0
0.26
1
12/23/19 20:26
96-12-8
ND
ug/L
1.0
0.41
1
12/23/19 20:26
124-48-1
ND
ug/L
1.0
0.26
1
12/23/19 20:26
106-93-4
ND
ug/L
1.0
0.46
1
12/23/19 20:26
74-95-3
ND
ug/L
1.0
0.29
1
12/23/19 20:26
95-50-1
ND
ug/L
1.0
0.26
1
12/23/19 20:26
106-46-7
ND
ug/L
1.0
0.54
1
12/23/19 20:26
110-57-6
2.1
ug/L
1.0
0.27
1
12/23/19 20:26
75-34-3
0.44J
ug/L
1.0
0.34
1
12/23/19 20:26
107-06-2
ND
ug/L
1.0
0.24
1
12/23/19 20:26
75-35-4
13.2
ug/L
1.0
0.29
1
12/23/19 20:26
156-59-2
ND
ug/L
1.0
0.25
1
12/23/19 20:26
156-60-5
ND
ug/L
1.0
0.19
1
12/23/19 20:26
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 32 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-21
Lab ID:
92457590014
Collected:
12/12/19 14:34
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/23/19 20:26
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/23/19 20:26
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/23/19 20:26
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/23/19 20:26
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/23/19 20:26
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/23/19 20:26
74-88-4
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/23/19 20:26
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/23/19 20:26
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/23/19 20:26
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/23/19 20:26
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/23/19 20:26
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/23/19 20:26
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/23/19 20:26
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/23/19 20:26
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/23/19 20:26
79-00-5
Trichloroethene
0.47J
ug/L
1.0
0.22
1
12/23/19 20:26
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/23/19 20:26
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/23/19 20:26
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/23/19 20:26
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
12/23/19 20:26
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/23/19 20:26
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
12/23/19 20:26
460-00-4
1,2-Dichloroethane-d4 (S)
100
%
70-130
1
12/23/19 20:26
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
12/23/19 20:26
2037-26-5
Date: 12/31 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 33 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-22 Lab ID: 92457590015 Collected: 12/13/19 15:23 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 12/31 /2019 11:05 AM
Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
ND
ug/L
5.0
3.0
1
12/26/1917:06
12/27/1912:12
7440-36-0
ND
ug/L
10.0
4.7
1
12/26/1917:06
12/27/1912:12
7440-38-2
117
ug/L
5.0
1.0
1
12/26/1917:06
12/27/1912:12
7440-39-3
ND
ug/L
1.0
0.20
1
12/26/1917:06
12/27/1912:12
7440-41-7
8.7
ug/L
1.0
0.40
1
12/26/1917:06
12/27/1912:12
7440-43-9
ND
ug/L
5.0
1.0
1
12/26/1917:06
12/27/1912:12
7440-47-3
130
ug/L
5.0
1.1
1
12/26/1917:06
12/27/1912:12
7440-48-4
2.7J
ug/L
5.0
2.1
1
12/26/1917:06
12/27/1912:12
7440-50-8
3.1J
ug/L
5.0
1.6
1
12/26/1917:06
12/27/1912:12
7439-92-1
9.8
ug/L
5.0
0.90
1
12/26/1917:06
12/27/1912:12
7440-02-0
8.3J
ug/L
10.0
4.7
1
12/26/1917:06
12/27/1912:12
7782-49-2
ND
ug/L
5.0
2.5
1
12/26/1917:06
12/27/1912:12
7440-22-4
ND
ug/L
5.0
1.3
1
12/26/1917:06
12/27/1912:12
7440-62-2
41.8
ug/L
10.0
3.9
1
12/26/1917:06
12/27/1912:12
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
0.15 ug/L 0.10 0.060 1 12/26/1917:06 12/30/1919:21 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
12/24/19 04:46
67-64-1
ND
ug/L
10.0
0.90
1
12/24/19 04:46
107-13-1
0.39J
ug/L
1.0
0.15
1
12/24/19 04:46
71-43-2
ND
ug/L
1.0
0.34
1
12/24/19 04:46
74-97-5
ND
ug/L
1.0
0.26
1
12/24/19 04:46
75-27-4
ND
ug/L
1.0
0.62
1
12/24/19 04:46
75-25-2
ND
ug/L
2.0
0.62
1
12/24/19 04:46
74-83-9
ND
ug/L
5.0
3.3
1
12/24/19 04:46
78-93-3
ND
ug/L
2.0
0.40
1
12/24/19 04:46
75-15-0
ND
ug/L
1.0
0.22
1
12/24/19 04:46
56-23-5
2.3
ug/L
1.0
0.23
1
12/24/19 04:46
108-90-7
ND
ug/L
1.0
0.49
1
12/24/19 04:46
75-00-3
ND
ug/L
5.0
2.3
1
12/24/19 04:46
67-66-3
ND
ug/L
1.0
0.39
1
12/24/19 04:46
74-87-3
ND
ug/L
5.0
0.26
1
12/24/19 04:46
96-12-8
ND
ug/L
1.0
0.41
1
12/24/19 04:46
124-48-1
ND
ug/L
1.0
0.26
1
12/24/19 04:46
106-93-4
ND
ug/L
1.0
0.46
1
12/24/19 04:46
74-95-3
0.64J
ug/L
1.0
0.29
1
12/24/19 04:46
95-50-1
5.8
ug/L
1.0
0.26
1
12/24/19 04:46
106-46-7
ND
ug/L
1.0
0.54
1
12/24/19 04:46
110-57-6
0.62J
ug/L
1.0
0.27
1
12/24/19 04:46
75-34-3
0.49J
ug/L
1.0
0.34
1
12/24/19 04:46
107-06-2
ND
ug/L
1.0
0.24
1
12/24/19 04:46
75-35-4
1.5
ug/L
1.0
0.29
1
12/24/19 04:46
156-59-2
ND
ug/L
1.0
0.25
1
12/24/19 04:46
156-60-5
ND
ug/L
1.0
0.19
1
12/24/19 04:46
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
v2
v2
v2
Page 34 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-22
Lab ID:
92457590015
Collected:
12/13/19 15:23
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/24/19 04:46
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/24/19 04:46
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/24/19 04:46
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/24/19 04:46
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/24/19 04:46
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/24/19 04:46
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/24/19 04:46
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/24/19 04:46
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/24/19 04:46
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/24/19 04:46
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/24/19 04:46
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/24/19 04:46
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/24/19 04:46
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/24/19 04:46
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/24/19 04:46
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/24/19 04:46
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/24/19 04:46
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/24/19 04:46
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/24/19 04:46
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
12/24/19 04:46
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/24/19 04:46
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
12/24/19 04:46
460-00-4
1,2-Dichloroethane-d4 (S)
102
%
70-130
1
12/24/19 04:46
17060-07-0
Toluene-d8 (S)
105
%
70-130
1
12/24/19 04:46
2037-26-5
Date: 12/31 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 35 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-23 Lab ID: 92457590016 Collected: 12/12/19 11:25 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 12/31 /2019 11:05 AM
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
ND
ug/L
5.0
3.0
1
12/26/1917:06
12/27/1912:16
7440-36-0
ND
ug/L
10.0
4.7
1
12/26/1917:06
12/27/1912:16
7440-38-2
24.3
ug/L
5.0
1.0
1
12/26/1917:06
12/27/1912:16
7440-39-3
0.23J
ug/L
1.0
0.20
1
12/26/1917:06
12/27/1912:16
7440-41-7
ND
ug/L
1.0
0.40
1
12/26/1917:06
12/27/1912:16
7440-43-9
ND
ug/L
5.0
1.0
1
12/26/1917:06
12/27/1912:16
7440-47-3
ND
ug/L
5.0
1.1
1
12/26/1917:06
12/27/1912:16
7440-48-4
ND
ug/L
5.0
2.1
1
12/26/1917:06
12/27/1912:16
7440-50-8
ND
ug/L
5.0
1.6
1
12/26/1917:06
12/27/1912:16
7439-92-1
ND
ug/L
5.0
0.90
1
12/26/1917:06
12/27/1912:16
7440-02-0
ND
ug/L
10.0
4.7
1
12/26/1917:06
12/27/1912:16
7782-49-2
ND
ug/L
5.0
2.5
1
12/26/1917:06
12/27/1912:16
7440-22-4
ND
ug/L
5.0
1.3
1
12/26/1917:06
12/27/1912:16
7440-62-2
5.5J
ug/L
10.0
3.9
1
12/26/1917:06
12/27/1912:16
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 0.10 0.060 1 12/26/19 17:06 12/30/19 20:07 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
12/23/19 20:44
67-64-1
ND
ug/L
10.0
0.90
1
12/23/19 20:44
107-13-1
ND
ug/L
1.0
0.15
1
12/23/19 20:44
71-43-2
ND
ug/L
1.0
0.34
1
12/23/19 20:44
74-97-5
ND
ug/L
1.0
0.26
1
12/23/19 20:44
75-27-4
ND
ug/L
1.0
0.62
1
12/23/19 20:44
75-25-2
ND
ug/L
2.0
0.62
1
12/23/19 20:44
74-83-9
ND
ug/L
5.0
3.3
1
12/23/19 20:44
78-93-3
ND
ug/L
2.0
0.40
1
12/23/19 20:44
75-15-0
ND
ug/L
1.0
0.22
1
12/23/19 20:44
56-23-5
ND
ug/L
1.0
0.23
1
12/23/19 20:44
108-90-7
ND
ug/L
1.0
0.49
1
12/23/19 20:44
75-00-3
ND
ug/L
5.0
2.3
1
12/23/19 20:44
67-66-3
ND
ug/L
1.0
0.39
1
12/23/19 20:44
74-87-3
ND
ug/L
5.0
0.26
1
12/23/19 20:44
96-12-8
ND
ug/L
1.0
0.41
1
12/23/19 20:44
124-48-1
ND
ug/L
1.0
0.26
1
12/23/19 20:44
106-93-4
ND
ug/L
1.0
0.46
1
12/23/19 20:44
74-95-3
ND
ug/L
1.0
0.29
1
12/23/19 20:44
95-50-1
ND
ug/L
1.0
0.26
1
12/23/19 20:44
106-46-7
ND
ug/L
1.0
0.54
1
12/23/19 20:44
110-57-6
ND
ug/L
1.0
0.27
1
12/23/19 20:44
75-34-3
ND
ug/L
1.0
0.34
1
12/23/19 20:44
107-06-2
ND
ug/L
1.0
0.24
1
12/23/19 20:44
75-35-4
0.55J
ug/L
1.0
0.29
1
12/23/19 20:44
156-59-2
ND
ug/L
1.0
0.25
1
12/23/19 20:44
156-60-5
ND
ug/L
1.0
0.19
1
12/23/19 20:44
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 36 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Sample: MW-23
Lab ID:
92457590016
Collected:
12/12/19 11:25
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/23/19 20:44
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/23/19 20:44
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/23/19 20:44
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/23/19 20:44
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/23/19 20:44
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/23/19 20:44
74-88-4
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/23/19 20:44
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/23/19 20:44
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/23/19 20:44
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/23/19 20:44
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/23/19 20:44
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/23/19 20:44
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/23/19 20:44
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/23/19 20:44
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/23/19 20:44
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/23/19 20:44
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/23/19 20:44
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/23/19 20:44
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/23/19 20:44
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
12/23/19 20:44
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/23/19 20:44
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
103
%
70-130
1
12/23/19 20:44
460-00-4
1,2-Dichloroethane-d4 (S)
101
%
70-130
1
12/23/19 20:44
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
12/23/19 20:44
2037-26-5
Date: 12/31 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 37 of 63
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
QC Batch: 516498 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92457590001, 92457590002, 92457590003, 92457590004, 92457590005, 92457590006, 92457590007,
92457590008,92457590009,92457590010,92457590011,92457590012,92457590013,92457590014
METHOD BLANK: 2767371 Matrix: Water
Associated Lab Samples: 92457590001, 92457590002, 92457590003, 92457590004, 92457590005, 92457590006, 92457590007,
92457590008,92457590009,92457590010,92457590011,92457590012,92457590013,92457590014
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Antimony
ug/L
ND
5.0
3.0
12/24/19 22:28
Arsenic
ug/L
ND
10.0
4.7
12/24/19 22:28
Barium
ug/L
ND
5.0
1.0
12/24/19 22:28
Beryllium
ug/L
0.25J
1.0
0.20
12/24/19 22:28
Cadmium
ug/L
ND
1.0
0.40
12/24/19 22:28
Chromium
ug/L
ND
5.0
1.0
12/24/19 22:28
Cobalt
ug/L
ND
5.0
1.1
12/24/19 22:28
Copper
ug/L
ND
5.0
2.1
12/24/19 22:28
Lead
ug/L
ND
5.0
1.6
12/24/19 22:28
Nickel
ug/L
ND
5.0
0.90
12/24/19 22:28
Selenium
ug/L
ND
10.0
4.7
12/24/19 22:28
Silver
ug/L
ND
5.0
2.5
12/24/19 22:28
Vanadium
ug/L
ND
5.0
1.3
12/24/19 22:28
Zinc
ug/L
ND
10.0
3.9
12/24/19 22:28
LABORATORY CONTROL SAMPLE:
Parameter
2767372
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Antimony
ug/L
500
502
100
80-120
Arsenic
ug/L
500
503
101
80-120
Barium
ug/L
500
480
96
80-120
Beryllium
ug/L
500
479
96
80-120
Cadmium
ug/L
500
488
98
80-120
Chromium
ug/L
500
483
97
80-120
Cobalt
ug/L
500
491
98
80-120
Copper
ug/L
500
491
98
80-120
Lead
ug/L
500
494
99
80-120
Nickel
ug/L
500
487
97
80-120
Selenium
ug/L
500
487
97
80-120
Silver
ug/L
250
244
97
80-120
Vanadium
ug/L
500
483
97
80-120
Zinc
ug/L
500
481
96
80-120
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 38 of 63
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project:
Pace Project No.:
Surry Closed -Mt. Airy
92457590
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2767373
2767374
MS
MSD
92457589002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Antimony
ug/L
ND
500
500
524
519
105
104
75-125
1
20
Arsenic
ug/L
ND
500
500
538
526
107
105
75-125
2
20
Barium
ug/L
18.8
500
500
523
515
101
99
75-125
1
20
Beryllium
ug/L
0.20J
500
500
503
494
101
99
75-125
2
20
Cadmium
ug/L
0.81J
500
500
523
514
104
103
75-125
2
20
Chromium
ug/L
ND
500
500
509
503
102
101
75-125
1
20
Cobalt
ug/L
21.3
500
500
537
528
103
101
75-125
2
20
Copper
ug/L
ND
500
500
515
504
103
101
75-125
2
20
Lead
ug/L
ND
500
500
519
514
104
103
75-125
1
20
Nickel
ug/L
ND
500
500
514
507
103
101
75-125
1
20
Selenium
ug/L
ND
500
500
537
530
107
106
75-125
1
20
Silver
ug/L
ND
250
250
256
254
103
101
75-125
1
20
Vanadium
ug/L
ND
500
500
512
505
102
101
75-125
1
20
Zinc
ug/L
4.8J
500
500
522
515
103
102
75-125
1
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC.
Page 39 of 63
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
QC Batch: 516818 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92457590015, 92457590016
METHOD BLANK: 2768522
Associated Lab Samples: 92457590015, 92457590016
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Antimony
ug/L
ND
5.0
3.0
12/27/1911:47
Arsenic
ug/L
ND
10.0
4.7
12/27/1911:47
Barium
ug/L
ND
5.0
1.0
12/27/1911:47
Beryllium
ug/L
ND
1.0
0.20
12/27/1911:47
Cadmium
ug/L
ND
1.0
0.40
12/27/1911:47
Chromium
ug/L
ND
5.0
1.0
12/27/1911:47
Cobalt
ug/L
ND
5.0
1.1
12/27/1911:47
Copper
ug/L
ND
5.0
2.1
12/27/1911:47
Lead
ug/L
ND
5.0
1.6
12/27/1911:47
Nickel
ug/L
ND
5.0
0.90
12/27/1911:47
Selenium
ug/L
ND
10.0
4.7
12/27/1911:47
Silver
ug/L
ND
5.0
2.5
12/27/1911:47
Vanadium
ug/L
ND
5.0
1.3
12/27/1911:47
Zinc
ug/L
ND
10.0
3.9
12/27/1911:47
LABORATORY CONTROL SAMPLE:
Parameter
2768523
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
487
97
80-120
Arsenic
ug/L
500
486
97
80-120
Barium
ug/L
500
496
99
80-120
Beryllium
ug/L
500
480
96
80-120
Cadmium
ug/L
500
499
100
80-120
Chromium
ug/L
500
492
98
80-120
Cobalt
ug/L
500
489
98
80-120
Copper
ug/L
500
485
97
80-120
Lead
ug/L
500
492
98
80-120
Nickel
ug/L
500
498
100
80-120
Selenium
ug/L
500
478
96
80-120
Silver
ug/L
250
242
97
80-120
Vanadium
ug/L
500
474
95
80-120
Zinc
ug/L
500
474
95
80-120
Qualifiers
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2768524 2768525
MS MSD
92457256007 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Antimony ug/L ND 500 500 516 494 103 99 75-125 4 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC.
Page 40 of 63
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project:
Pace Project No.:
Surry Closed -Mt. Airy
92457590
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2768524
2768525
MS
MSD
92457256007
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Arsenic
ug/L
ND
500
500
515
508
102
101
75-125
1
20
Barium
ug/L
41.3
500
500
556
558
103
103
75-125
0
20
Beryllium
ug/L
ND
500
500
497
494
99
99
75-125
1
20
Cadmium
ug/L
ND
500
500
533
538
106
108
75-125
1
20
Chromium
ug/L
ND
500
500
513
520
103
104
75-125
1
20
Cobalt
ug/L
ND
500
500
508
511
102
102
75-125
1
20
Copper
ug/L
ND
500
500
503
503
100
100
75-125
0
20
Lead
ug/L
ND
500
500
514
516
103
103
75-125
0
20
Nickel
ug/L
0.93J
500
500
520
523
104
104
75-125
0
20
Selenium
ug/L
ND
500
500
530
521
105
104
75-125
2
20
Silver
ug/L
ND
250
250
250
166
100
67
75-125
40
20 M1,R1
Vanadium
ug/L
ND
500
500
496
499
99
100
75-125
1
20
Zinc
ug/L
4.2J
500
500
611
516
121
102
75-125
17
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC.
Page 41 of 63
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
QC Batch: 516501 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Associated Lab Samples: 92457590001, 92457590002, 92457590003, 92457590004, 92457590005, 92457590006, 92457590007,
92457590008,92457590009,92457590010,92457590011,92457590012,92457590013,92457590014
METHOD BLANK: 2767378 Matrix: Water
Associated Lab Samples: 92457590001, 92457590002, 92457590003, 92457590004, 92457590005, 92457590006, 92457590007,
92457590008,92457590009,92457590010,92457590011,92457590012,92457590013,92457590014
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Thallium ug/L ND 0.10 0.060 12/30/1915:28
LABORATORY CONTROL SAMPLE: 2767379
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Thallium ug/L 10 9.9 99 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2767380 2767381
MS MSD
92457589003 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND 10 10 11.0 10.8 110 108 75-125 2 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC.
Page 42 of 63
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
QC Batch: 516819 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Associated Lab Samples: 92457590015, 92457590016
METHOD BLANK: 2768527 Matrix: Water
Associated Lab Samples: 92457590015, 92457590016
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Thallium ug/L ND 0.10 0.060 12/30/1915:34
LABORATORY CONTROL SAMPLE: 2768528
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Thallium ug/L 10 10 100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2768529 2768530
MS MSD
92457590015 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Thallium ug/L 0.15 10 10 10.4 10.2 102 101 75-125 2 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC.
Page 43 of 63
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
QC Batch: 516392 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Associated Lab Samples: 92457590002, 92457590003, 92457590004, 92457590009, 92457590010, 92457590014, 92457590016
METHOD BLANK: 2766751 Matrix: Water
Associated Lab Samples: 92457590002, 92457590003, 92457590004, 92457590009, 92457590010, 92457590014, 92457590016
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.34
12/23/19 12:25
1,1,1-Trichloroethane
ug/L
ND
1.0
0.18
12/23/19 12:25
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
12/23/19 12:25
1,1,2-Trichloroethane
ug/L
ND
1.0
0.24
12/23/19 12:25
1,1-Dichloroethane
ug/L
ND
1.0
0.27
12/23/19 12:25
1,1-Dichloroethene
ug/L
ND
1.0
0.24
12/23/19 12:25
1,2,3-Trichloropropane
ug/L
ND
1.0
0.35
12/23/19 12:25
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
0.26
12/23/19 12:25
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.26
12/23/19 12:25
1,2-Dichlorobenzene
ug/L
ND
1.0
0.29
12/23/19 12:25
1,2-Dichloroethane
ug/L
ND
1.0
0.34
12/23/19 12:25
1,2-Dichloropropane
ug/L
ND
1.0
0.19
12/23/19 12:25
1,4-Dichlorobenzene
ug/L
ND
1.0
0.26
12/23/19 12:25
1,4-Dioxane (p-Dioxane)
ug/L
ND
150
56.2
12/23/19 12:25
2-Butanone (MEK)
ug/L
ND
5.0
3.3
12/23/19 12:25
2-Hexanone
ug/L
ND
5.0
0.57
12/23/19 12:25
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
4.5
12/23/19 12:25
Acetone
ug/L
ND
25.0
6.2
12/23/19 12:25
Acrylonitrile
ug/L
ND
10.0
0.90
12/23/19 12:25
Benzene
ug/L
ND
1.0
0.15
12/23/19 12:25
Bromochloromethane
ug/L
ND
1.0
0.34
12/23/19 12:25
Bromodichloromethane
ug/L
ND
1.0
0.26
12/23/19 12:25
Bromoform
ug/L
ND
1.0
0.62
12/23/19 12:25
Bromomethane
ug/L
ND
2.0
0.62
12/23/19 12:25
Carbon disulfide
ug/L
ND
2.0
0.40
12/23/19 12:25
Carbon tetrachloride
ug/L
ND
1.0
0.22
12/23/19 12:25
Chlorobenzene
ug/L
ND
1.0
0.23
12/23/19 12:25
Chloroethane
ug/L
ND
1.0
0.49
12/23/19 12:25
Chloroform
ug/L
ND
5.0
2.3
12/23/19 12:25
Chloromethane
ug/L
ND
1.0
0.39
12/23/19 12:25
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.29
12/23/19 12:25
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.30
12/23/19 12:25
Dibromochloromethane
ug/L
ND
1.0
0.41
12/23/19 12:25
Dibromomethane
ug/L
ND
1.0
0.46
12/23/19 12:25
Ethylbenzene
ug/L
ND
1.0
0.26
12/23/19 12:25
lodomethane
ug/L
ND
20.0
12.5
12/23/19 12:25
Methylene Chloride
ug/L
ND
5.0
3.7
12/23/19 12:25
Styrene
ug/L
ND
1.0
0.27
12/23/19 12:25
Tetrachloroethene
ug/L
ND
1.0
0.16
12/23/19 12:25
Toluene
ug/L
ND
1.0
0.24
12/23/19 12:25
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.25
12/23/19 12:25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 44 of 63
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
METHOD BLANK: 2766751 Matrix: Water
Associated Lab Samples: 92457590002,92457590003,92457590004,92457590009,92457590010,92457590014,92457590016
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.31
12/23/19 12:25
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.54
12/23/19 12:25
Trichloroethene
ug/L
ND
1.0
0.22
12/23/19 12:25
Trichlorofluoromethane
ug/L
ND
1.0
0.31
12/23/19 12:25
Vinyl acetate
ug/L
ND
2.0
1.4
12/23/19 12:25
Vinyl chloride
ug/L
ND
1.0
0.24
12/23/19 12:25
Xylene (Total)
ug/L
ND
1.0
0.63
12/23/19 12:25
1,2-Dichloroethane-d4 (S)
%
99
70-130
12/23/19 12:25
4-Bromofluorobenzene (S)
%
101
70-130
12/23/19 12:25
Toluene-d8 (S)
%
103
70-130
12/23/19 12:25
LABORATORY CONTROL SAMPLE:
Parameter
2766752
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
49.8
100
70-130
1,1,1-Trichloroethane
ug/L
50
43.9
88
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
49.8
100
70-130
1,1,2-Trichloroethane
ug/L
50
47.8
96
70-130
1,1-Dichloroethane
ug/L
50
44.7
89
70-130
1,1-Dichloroethene
ug/L
50
48.2
96
70-130
1,2,3-Trichloropropane
ug/L
50
50.1
100
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
50.3
101
70-130
1,2-Dibromoethane (EDB)
ug/L
50
50.3
101
70-130
1,2-Dichlorobenzene
ug/L
50
51.7
103
70-130
1,2-Dichloroethane
ug/L
50
43.8
88
70-130
1,2-Dichloropropane
ug/L
50
50.0
100
70-130
1,4-Dichlorobenzene
ug/L
50
50.9
102
70-130
1,4-Dioxane(p-Dioxane)
ug/L
1000
1030
103
59-169
2-Butanone (MEK)
ug/L
100
97.2
97
64-135
2-Hexanone
ug/L
100
98.7
99
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
97.1
97
70-130
Acetone
ug/L
100
108
108
61-157
Acrylonitrile
ug/L
250
232
93
61-143
Benzene
ug/L
50
47.0
94
70-130
Bromochloromethane
ug/L
50
42.8
86
70-130
Bromodichloromethane
ug/L
50
45.5
91
70-130
Bromoform
ug/L
50
44.7
89
70-130
Bromomethane
ug/L
50
41.8
84
38-130
Carbon disulfide
ug/L
50
47.5
95
68-130
Carbon tetrachloride
ug/L
50
44.5
89
70-130
Chlorobenzene
ug/L
50
50.5
101
70-130
Chloroethane
ug/L
50
35.5
71
37-142
Chloroform
ug/L
50
44.3
89
70-130
Chloromethane
ug/L
50
39.6
79
48-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 45 of 63
Pace Analytical Services, LLC
9800
lCtaac,Analyfical ® Kiney Ave. Suite 100
Huntersville, NC 28078
0788
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
LABORATORY CONTROL SAMPLE:
Parameter
2766752
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
cis-1,2-Dichloroethene
ug/L
50
44.4
89
70-130
cis-1,3-Dichloropropene
ug/L
50
50.6
101
70-130
Dibromochloromethane
ug/L
50
46.7
93
70-130
Dibromomethane
ug/L
50
47.4
95
70-130
Ethylbenzene
ug/L
50
47.8
96
70-130
lodomethane
ug/L
100
66.9
67
40-130
Methylene Chloride
ug/L
50
43.5
87
67-132
Styrene
ug/L
50
50.0
100
70-130
Tetrachloroethene
ug/L
50
48.1
96
69-130
Toluene
ug/L
50
45.1
90
70-130
trans-1,2-Dichloroethene
ug/L
50
45.9
92
70-130
trans- 1,3-Dichloropropene
ug/L
50
49.3
99
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
50.8
102
35-189
Trichloroethene
ug/L
50
48.9
98
70-130
Trichlorofluoromethane
ug/L
50
45.4
91
63-130
Vinyl acetate
ug/L
100
103
103
55-143
Vinyl chloride
ug/L
50
49.1
98
70-131
Xylene (Total)
ug/L
150
139
93
70-130
1,2-Dichloroethane-d4 (S)
%
82
70-130
4-Bromofluorobenzene (S)
%
96
70-130
Toluene-d8 (S)
%
98
70-130
MATRIX SPIKE SAMPLE:
Parameter
2766754
Units
92457590003
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
19.6
98
73-134
1,1,1-Trichloroethane
ug/L
ND
20
18.9
95
82-143
1,1,2,2-Tetrachloroethane
ug/L
ND
20
19.3
97
70-136
1,1,2-Trichloroethane
ug/L
ND
20
19.8
99
70-135
1,1-Dichloroethane
ug/L
ND
20
19.7
98
70-139
1,1-Dichloroethene
ug/L
ND
20
19.6
98
70-154
1,2,3-Trichloropropane
ug/L
ND
20
19.7
98
71-137
1,2-Dibromo-3-chloropropane
ug/L
ND
20
17.7
88
65-134
1,2-Dibromoethane (EDB)
ug/L
ND
20
20.4
102
70-137
1,2-Dichlorobenzene
ug/L
ND
20
20.6
103
70-133
1,2-Dichloroethane
ug/L
ND
20
19.2
96
70-137
1,2-Dichloropropane
ug/L
ND
20
21.0
105
70-140
1,4-Dichlorobenzene
ug/L
ND
20
20.6
103
70-133
1,4-Dioxane (p-Dioxane)
ug/L
ND
400
386
97
53-168
2-Butanone (MEK)
ug/L
ND
40
38.8
97
60-139
2-Hexanone
ug/L
ND
40
35.2
88
65-138
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
35.4
89
65-135
Acetone
ug/L
ND
40
39.1
98
60-148
Acrylonitrile
ug/L
ND
100
95.5
96
64-147
Benzene
ug/L
ND
20
19.8
99
70-151
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 46 of 63
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
MATRIX SPIKE SAMPLE: 2766754
92457590003
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Bromochloromethane
ug/L
ND
20
19.8
99
70-141
Bromodichloromethane
ug/L
ND
20
18.4
92
70-138
Bromoform
ug/L
ND
20
15.8
79
63-130
Bromomethane
ug/L
ND
20
17.4
87
15-152
Carbon disulfide
ug/L
ND
20
20.6
103
69-149
Carbon tetrachloride
ug/L
ND
20
19.0
95
70-143
Chlorobenzene
ug/L
ND
20
20.8
104
70-138
Chloroethane
ug/L
ND
20
18.7
94
52-163
Chloroform
ug/L
ND
20
19.2
96
70-139
Chloromethane
ug/L
ND
20
16.8
84
41-139
cis-1,2-Dichloroethene
ug/L
ND
20
19.3
97
70-141
cis-1,3-Dichloropropene
ug/L
ND
20
20.1
101
70-137
Dibromochloromethane
ug/L
ND
20
18.0
90
70-134
Dibromomethane
ug/L
ND
20
20.0
100
70-138
Ethylbenzene
ug/L
ND
20
20.1
100
66-153
lodomethane
ug/L
ND
40
26.6
66
20-138
Methylene Chloride
ug/L
ND
20
19.6
98
42-159
Styrene
ug/L
ND
20
20.8
104
70-135
Tetrachloroethene
ug/L
ND
20
20.0
100
59-143
Toluene
ug/L
ND
20
18.6
93
59-148
trans-1,2-Dichloroethene
ug/L
ND
20
18.9
94
70-146
trans- 1,3-Dichloropropene
ug/L
ND
20
19.3
96
70-135
trans-1,4-Dichloro-2-butene
ug/L
ND
20
19.1
95
47-135
Trichloroethene
ug/L
ND
20
20.5
102
70-147
Trichlorofluoromethane
ug/L
ND
20
19.9
99
70-148
Vinyl acetate
ug/L
ND
40
40.6
102
49-151
Vinyl chloride
ug/L
ND
20
21.5
107
70-156
Xylene (Total)
ug/L
ND
60
59.6
99
63-158
1,2-Dichloroethane-d4 (S)
%
91
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
97
70-130
SAMPLE DUPLICATE: 2766753
Parameter
Units
92457590002
Result
Dup
Result RPD
Max
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,1-Trichloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
ND
ND
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,2,3-Trichloropropane
ug/L
ND
ND
30
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
30
1,2-Dibromoethane (EDB)
ug/L
ND
ND
30
1,2-Dichlorobenzene
ug/L
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 47 of 63
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
SAMPLE DUPLICATE: 2766753
Parameter
Units
92457590002
Result
Dup
Result RPD
Max
RPD
1,2-Dichloroethane
ug/L
ND
ND
30
1,2-Dichloropropane
ug/L
ND
ND
30
1,4-Dichlorobenzene
ug/L
ND
ND
30
1,4-Dioxane (p-Dioxane)
ug/L
ND
ND
30
2-Butanone (MEK)
ug/L
ND
ND
30
2-Hexanone
ug/L
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
30
Acetone
ug/L
ND
ND
30
Acrylonitrile
ug/L
ND
ND
30
Benzene
ug/L
ND
ND
30
Bromochloromethane
ug/L
ND
ND
30
Bromodichloromethane
ug/L
ND
ND
30
Bromoform
ug/L
ND
ND
30
Bromomethane
ug/L
ND
ND
30
Carbon disulfide
ug/L
ND
ND
30
Carbon tetrachloride
ug/L
ND
ND
30
Chlorobenzene
ug/L
ND
ND
30
Chloroethane
ug/L
ND
ND
30
Chloroform
ug/L
ND
ND
30
Chloromethane
ug/L
ND
ND
30
cis-1,2-Dichloroethene
ug/L
ND
ND
30
cis-1,3-Dichloropropene
ug/L
ND
ND
30
Dibromochloromethane
ug/L
ND
ND
30
Dibromomethane
ug/L
ND
ND
30
Ethylbenzene
ug/L
ND
ND
30
lodomethane
ug/L
ND
ND
30
Methylene Chloride
ug/L
ND
ND
30
Styrene
ug/L
ND
ND
30
Tetrachloroethene
ug/L
ND
ND
30
Toluene
ug/L
ND
ND
30
trans-1,2-Dichloroethene
ug/L
ND
ND
30
trans- 1,3-Dichloropropene
ug/L
ND
ND
30
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
30
Trichloroethene
ug/L
ND
ND
30
Trichlorofluoromethane
ug/L
ND
ND
30
Vinyl acetate
ug/L
ND
ND
30
Vinyl chloride
ug/L
ND
ND
30
Xylene (Total)
ug/L
ND
ND
30
1,2-Dichloroethane-d4 (S)
%
99
97
4-Bromofluorobenzene (S)
%
99
100
Toluene-d8 (S)
%
99
101
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC.
Page 48 of 63
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
QC Batch: 516422 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Associated Lab Samples: 92457590001, 92457590005, 92457590006, 92457590007, 92457590008, 92457590011, 92457590012,
92457590013,92457590015
METHOD BLANK: 2766873 Matrix: Water
Associated Lab Samples: 92457590001, 92457590005, 92457590006, 92457590007, 92457590008, 92457590011, 92457590012,
92457590013,92457590015
Parameter
Units
Blank
Result
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.34
12/24/19 00:18
1,1,1-Trichloroethane
ug/L
ND
1.0
0.18
12/24/19 00:18
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
12/24/19 00:18
1,1,2-Trichloroethane
ug/L
ND
1.0
0.24
12/24/19 00:18
1,1-Dichloroethane
ug/L
ND
1.0
0.27
12/24/19 00:18
1,1-Dichloroethene
ug/L
ND
1.0
0.24
12/24/19 00:18
1,2,3-Trichloropropane
ug/L
ND
1.0
0.35
12/24/19 00:18
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
0.26
12/24/19 00:18
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.26
12/24/19 00:18
1,2-Dichlorobenzene
ug/L
ND
1.0
0.29
12/24/19 00:18
1,2-Dichloroethane
ug/L
ND
1.0
0.34
12/24/19 00:18
1,2-Dichloropropane
ug/L
ND
1.0
0.19
12/24/19 00:18
1,4-Dichlorobenzene
ug/L
ND
1.0
0.26
12/24/19 00:18
1,4-Dioxane (p-Dioxane)
ug/L
ND
150
56.2
12/24/19 00:18
2-Butanone (MEK)
ug/L
ND
5.0
3.3
12/24/19 00:18
2-Hexanone
ug/L
ND
5.0
0.57
12/24/19 00:18
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
4.5
12/24/19 00:18
Acetone
ug/L
ND
25.0
6.2
12/24/19 00:18
Acrylonitrile
ug/L
ND
10.0
0.90
12/24/19 00:18
Benzene
ug/L
ND
1.0
0.15
12/24/19 00:18
Bromochloromethane
ug/L
ND
1.0
0.34
12/24/19 00:18
Bromodichloromethane
ug/L
ND
1.0
0.26
12/24/19 00:18
Bromoform
ug/L
ND
1.0
0.62
12/24/19 00:18
Bromomethane
ug/L
ND
2.0
0.62
12/24/19 00:18
Carbon disulfide
ug/L
ND
2.0
0.40
12/24/19 00:18
Carbon tetrachloride
ug/L
ND
1.0
0.22
12/24/19 00:18
Chlorobenzene
ug/L
ND
1.0
0.23
12/24/19 00:18
Chloroethane
ug/L
ND
1.0
0.49
12/24/19 00:18
Chloroform
ug/L
ND
5.0
2.3
12/24/19 00:18
Chloromethane
ug/L
ND
1.0
0.39
12/24/19 00:18
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.29
12/24/19 00:18
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.30
12/24/19 00:18
Dibromochloromethane
ug/L
ND
1.0
0.41
12/24/19 00:18
Dibromomethane
ug/L
ND
1.0
0.46
12/24/19 00:18
Ethylbenzene
ug/L
ND
1.0
0.26
12/24/19 00:18
lodomethane
ug/L
ND
20.0
12.5
12/24/19 00:18
Methylene Chloride
ug/L
ND
5.0
3.7
12/24/19 00:18
Styrene
ug/L
ND
1.0
0.27
12/24/19 00:18
Tetrachloroethene
ug/L
ND
1.0
0.16
12/24/19 00:18
Toluene
ug/L
ND
1.0
0.24
12/24/19 00:18
v2
v2
v2
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 49 of 63
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
METHOD BLANK: 2766873 Matrix: Water
Associated Lab Samples: 92457590001, 92457590005, 92457590006, 92457590007, 92457590008, 92457590011, 92457590012,
92457590013,92457590015
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.25
12/24/19 00:18
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.31
12/24/19 00:18
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.54
12/24/19 00:18
Trichloroethene
ug/L
ND
1.0
0.22
12/24/19 00:18
Trichlorofluoromethane
ug/L
ND
1.0
0.31
12/24/19 00:18
Vinyl acetate
ug/L
ND
2.0
1.4
12/24/19 00:18
Vinyl chloride
ug/L
ND
1.0
0.24
12/24/19 00:18
Xylene (Total)
ug/L
ND
1.0
0.63
12/24/19 00:18
1,2-Dichloroethane-d4 (S)
%
97
70-130
12/24/19 00:18
4-Bromofluorobenzene (S)
%
101
70-130
12/24/19 00:18
Toluene-d8 (S)
%
100
70-130
12/24/19 00:18
LABORATORY CONTROL SAMPLE:
Parameter
2766874
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
47.2
94
70-130
1,1,1-Trichloroethane
ug/L
50
41.9
84
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
47.5
95
70-130
1,1,2-Trichloroethane
ug/L
50
45.5
91
70-130
1,1-Dichloroethane
ug/L
50
44.3
89
70-130
1,1-Dichloroethene
ug/L
50
47.0
94
70-130
1,2,3-Trichloropropane
ug/L
50
48.0
96
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
43.8
88
70-130
1,2-Dibromoethane (EDB)
ug/L
50
48.7
97
70-130
1,2-Dichlorobenzene
ug/L
50
48.9
98
70-130
1,2-Dichloroethane
ug/L
50
44.0
88
70-130
1,2-Dichloropropane
ug/L
50
46.2
92
70-130
1,4-Dichlorobenzene
ug/L
50
47.7
95
70-130
1,4-Dioxane (p-Dioxane)
ug/L
1000
943
94
59-169
2-Butanone (MEK)
ug/L
100
90.9
91
64-135
2-Hexanone
ug/L
100
90.5
91
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
89.8
90
70-130
Acetone
ug/L
100
94.3
94
61-157
Acrylonitrile
ug/L
250
227
91
61-143
Benzene
ug/L
50
44.6
89
70-130
Bromochloromethane
ug/L
50
42.9
86
70-130
Bromodichloromethane
ug/L
50
42.1
84
70-130
Bromoform
ug/L
50
40.8
82
70-130
Bromomethane
ug/L
50
34.7
69
38-130 v2
Carbon disulfide
ug/L
50
45.5
91
68-130
Carbon tetrachloride
ug/L
50
40.6
81
70-130
Chlorobenzene
ug/L
50
48.0
96
70-130
Chloroethane
ug/L
50
35.4
71
37-142 v2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 50 of 63
Pace Analytical Services, LLC
9800
lCtaac,Analyfical ® Kiney Ave. Suite 100
Huntersville, NC 28078
0788
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
LABORATORY CONTROL SAMPLE:
Parameter
2766874
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Chloroform
ug/L
50
43.6
87
70-130
Chloromethane
ug/L
50
36.7
73
48-130 v2
cis-1,2-Dichloroethene
ug/L
50
43.7
87
70-130
cis-1,3-Dichloropropene
ug/L
50
46.7
93
70-130
Dibromochloromethane
ug/L
50
43.6
87
70-130
Dibromomethane
ug/L
50
45.7
91
70-130
Ethylbenzene
ug/L
50
45.5
91
70-130
lodomethane
ug/L
100
73.1
73
40-130 v2
Methylene Chloride
ug/L
50
42.7
85
67-132
Styrene
ug/L
50
47.6
95
70-130
Tetrachloroethene
ug/L
50
45.7
91
69-130
Toluene
ug/L
50
42.1
84
70-130
trans-1,2-Dichloroethene
ug/L
50
44.7
89
70-130
trans- 1,3-Dichloropropene
ug/L
50
44.8
90
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
44.9
90
35-189
Trichloroethene
ug/L
50
45.9
92
70-130
Trichlorofluoromethane
ug/L
50
41.5
83
63-130
Vinyl acetate
ug/L
100
99.9
100
55-143
Vinyl chloride
ug/L
50
46.5
93
70-131
Xylene (Total)
ug/L
150
135
90
70-130
1,2-Dichloroethane-d4 (S)
%
87
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
97
70-130
MATRIX SPIKE SAMPLE:
Parameter
2766876
Units
92457589002
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
19.6
98
73-134
1,1,1-Trichloroethane
ug/L
ND
20
18.8
94
82-143
1,1,2,2-Tetrachloroethane
ug/L
ND
20
19.1
96
70-136
1,1,2-Trichloroethane
ug/L
ND
20
19.5
98
70-135
1,1-Dichloroethane
ug/L
ND
20
20.2
101
70-139
1,1-Dichloroethene
ug/L
ND
20
20.1
100
70-154
1,2,3-Trichloropropane
ug/L
ND
20
19.6
98
71-137
1,2-Dibromo-3-chloropropane
ug/L
ND
20
17.3
87
65-134
1,2-Dibromoethane (EDB)
ug/L
ND
20
20.4
102
70-137
1,2-Dichlorobenzene
ug/L
ND
20
20.8
104
70-133
1,2-Dichloroethane
ug/L
ND
20
18.8
94
70-137
1,2-Dichloropropene
ug/L
ND
20
20.9
104
70-140
1,4-Dichlorobenzene
ug/L
ND
20
21.1
106
70-133
1,4-Dioxane (p-Dioxane)
ug/L
ND
400
376
94
53-168
2-Butanone (MEK)
ug/L
ND
40
37.1
93
60-139
2-Hexanone
ug/L
ND
40
33.9
85
65-138
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
34.4
86
65-135
Acetone
ug/L
ND
40
37.8
95
60-148
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 51 of 63
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
MATRIX SPIKE SAMPLE:
Parameter
2766876
Units
92457589002
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Acrylonitrile
ug/L
ND
100
94.9
95
64-147
Benzene
ug/L
ND
20
19.8
99
70-151
Bromochloromethane
ug/L
ND
20
19.2
96
70-141
Bromodichloromethane
ug/L
ND
20
18.4
92
70-138
Bromoform
ug/L
ND
20
16.3
81
63-130
Bromomethane
ug/L
ND
20
18.9
95
15-152
Carbon disulfide
ug/L
ND
20
20.6
103
69-149
Carbon tetrachloride
ug/L
ND
20
19.3
96
70-143
Chlorobenzene
ug/L
ND
20
21.1
105
70-138
Chloroethane
ug/L
ND
20
20.1
100
52-163
Chloroform
ug/L
ND
20
19.5
98
70-139
Chloromethane
ug/L
ND
20
17.4
87
41-139
cis-1,2-Dichloroethene
ug/L
3.0
20
22.3
96
70-141
cis-1,3-Dichloropropene
ug/L
ND
20
20.2
101
70-137
Dibromochloromethane
ug/L
ND
20
18.3
91
70-134
Dibromomethane
ug/L
ND
20
20.1
101
70-138
Ethylbenzene
ug/L
ND
20
20.1
101
66-153
lodomethane
ug/L
ND
40
28.6
72
20-138
Methylene Chloride
ug/L
ND
20
19.5
97
42-159
Styrene
ug/L
ND
20
20.8
104
70-135
Tetrachloroethene
ug/L
ND
20
20.2
101
59-143
Toluene
ug/L
ND
20
18.8
94
59-148
trans-1,2-Dichloroethene
ug/L
ND
20
20.3
102
70-146
trans- 1,3-Dichloropropene
ug/L
ND
20
19.2
96
70-135
trans-1,4-Dichloro-2-butene
ug/L
ND
20
19.1
96
47-135
Trichloroethene
ug/L
ND
20
21.0
105
70-147
Trichlorofluoromethane
ug/L
ND
20
20.4
102
70-148
Vinyl acetate
ug/L
ND
40
39.3
98
49-151
Vinyl chloride
ug/L
ND
20
22.4
112
70-156
Xylene (Total)
ug/L
ND
60
60.0
100
63-158
1,2-Dichloroethane-d4 (S)
%
88
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
97
70-130
SAMPLE DUPLICATE: 2766875
92457587004
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,1-Trichloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
ND
ND
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,2,3-Trichloropropane
ug/L
ND
ND
30
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 52 of 63
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
SAMPLE DUPLICATE: 2766875
Parameter
Units
92457587004
Result
Dup
Result RPD
Max
RPD
1,2-Dibromoethane (EDB)
ug/L
ND
ND
30
1,2-Dichlorobenzene
ug/L
ND
ND
30
1,2-Dichloroethane
ug/L
ND
ND
30
1,2-Dichloropropane
ug/L
ND
ND
30
1,4-Dichlorobenzene
ug/L
ND
ND
30
1,4-Dioxane (p-Dioxane)
ug/L
ND
ND
30
2-Butanone (MEK)
ug/L
ND
ND
30
2-Hexanone
ug/L
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
30
Acetone
ug/L
ND
ND
30
Acrylonitrile
ug/L
ND
ND
30
Benzene
ug/L
ND
ND
30
Bromochloromethane
ug/L
ND
ND
30
Bromodichloromethane
ug/L
ND
ND
30
Bromoform
ug/L
ND
ND
30
Bromomethane
ug/L
ND
ND
30
Carbon disulfide
ug/L
ND
ND
30
Carbon tetrachloride
ug/L
ND
ND
30
Chlorobenzene
ug/L
ND
ND
30
Chloroethane
ug/L
ND
ND
30
Chloroform
ug/L
ND
ND
30
Chloromethane
ug/L
ND
ND
30
cis-1,2-Dichloroethene
ug/L
ND
ND
30
cis-1,3-Dichloropropene
ug/L
ND
ND
30
Dibromochloromethane
ug/L
ND
ND
30
Dibromomethane
ug/L
ND
ND
30
Ethylbenzene
ug/L
ND
ND
30
lodomethane
ug/L
ND
ND
30
Methylene Chloride
ug/L
ND
ND
30
Styrene
ug/L
ND
ND
30
Tetrachloroethene
ug/L
ND
ND
30
Toluene
ug/L
ND
ND
30
trans-1,2-Dichloroethene
ug/L
ND
ND
30
trans- 1,3-Dichloropropene
ug/L
ND
ND
30
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
30
Trichloroethene
ug/L
ND
ND
30
Trichlorofluoromethane
ug/L
ND
ND
30
Vinyl acetate
ug/L
ND
ND
30
Vinyl chloride
ug/L
ND
ND
30
Xylene (Total)
ug/L
ND
ND
30
1,2-Dichloroethane-d4 (S)
%
95
97
4-Bromofluorobenzene (S)
%
99
99
Toluene-d8 (S)
%
100
101
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC.
Page 53 of 63
Pace Analytical Services, LLC
9800
lCtaac,Analyfical ® Kiney Ave. Suite 100
Huntersville, NC 28078
0788
www.pacelabs.com (704)875-9092
QUALIFIERS
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
B Analyte was detected in the associated method blank.
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/31 /2019 11:05 AM without the written consent of Pace Analytical Services, LLC. Page 54 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Surry Closed -Mt. Airy
92457590
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92457590001
MW-1
EPA 3010A
516498
EPA 6010D
516514
92457590002
MW-3R
EPA 3010A
516498
EPA 6010D
516514
92457590003
MW-6
EPA 3010A
516498
EPA 6010D
516514
92457590004
MW-7
EPA 3010A
516498
EPA 6010D
516514
92457590005
MW-9
EPA 3010A
516498
EPA 6010D
516514
92457590006
MW-11
EPA 3010A
516498
EPA 6010D
516514
92457590007
MW-13
EPA 3010A
516498
EPA 6010D
516514
92457590008
MW-14
EPA 3010A
516498
EPA 6010D
516514
92457590009
MW-15
EPA 3010A
516498
EPA 6010D
516514
92457590010
MW-16
EPA 3010A
516498
EPA 6010D
516514
92457590011
MW-17
EPA 3010A
516498
EPA 6010D
516514
92457590012
MW-19
EPA 3010A
516498
EPA 6010D
516514
92457590013
MW-20
EPA 3010A
516498
EPA 6010D
516514
92457590014
MW-21
EPA 3010A
516498
EPA 6010D
516514
92457590015
MW-22
EPA 3010A
516818
EPA 6010D
516834
92457590016
MW-23
EPA 3010A
516818
EPA 6010D
516834
92457590001
MWA
EPA 3010A
516501
EPA 6020B
516518
92457590002
MW-3R
EPA 3010A
516501
EPA 6020B
516518
92457590003
MW-6
EPA 3010A
516501
EPA 6020B
516518
92457590004
MW-7
EPA 3010A
516501
EPA 6020B
516518
92457590005
MW-9
EPA 3010A
516501
EPA 6020B
516518
92457590006
MW-11
EPA 3010A
516501
EPA 6020B
516518
92457590007
MW-13
EPA 3010A
516501
EPA 6020B
516518
92457590008
MW-14
EPA 3010A
516501
EPA 6020B
516518
92457590009
MW-15
EPA 3010A
516501
EPA 6020B
516518
92457590010
MW-16
EPA 3010A
516501
EPA 6020B
516518
92457590011
MW-17
EPA 3010A
516501
EPA 6020B
516518
92457590012
MW-19
EPA 3010A
516501
EPA 6020B
516518
92457590013
MW-20
EPA 3010A
516501
EPA 6020B
516518
92457590014
MW-21
EPA 3010A
516501
EPA 6020B
516518
92457590015
MW-22
EPA 3010A
516819
EPA 6020B
516838
92457590016
MW-23
EPA 3010A
516819
EPA 6020B
516838
92457590001
MWA
EPA 8260D
516422
92457590002
MW-3R
EPA 8260D
516392
92457590003
MW-6
EPA 8260D
516392
92457590004
MW-7
EPA 8260D
516392
92457590005
MW-9
EPA 8260D
516422
92457590006
MW-11
EPA 8260D
516422
92457590007
MW-13
EPA 8260D
516422
92457590008
MW-14
EPA 8260D
516422
92457590009
MW-15
EPA 8260D
516392
92457590010
MW-16
EPA 8260D
516392
92457590011
MW-17
EPA 8260D
516422
92457590012
MW-19
EPA 8260D
516422
92457590013
MW-20
EPA 8260D
516422
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 12/31 /2019 11:05
AM
without the written consent of Pace Analytical Services, LLC.
Page 55 of 63
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Surry Closed -Mt. Airy
Pace Project No.: 92457590
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92457590014
MW-21
EPA 8260D
516392
92457590015
MW-22
EPA 8260D
516422
92457590016
MW-23
EPA 8260D
516392
Date: 12/31 /2019 11:05 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
Page 56 of 63
Document Name:
Document Revised: February 7, 2018
m
IceAnalyhcal
Sample Condition Upon Recel t(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR•CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples: /
Asheville ❑ Eden❑ Greenwood ❑ Huntersville D Ralelgh❑ Mechanicsville❑
ConditionSample Client Name: WO# : 92457594
Upon Receipt II _Project �.:
TA�Iad '� O� �1 14, r 1(, I r1r`1
Courier: ❑Fed Ex I []UPS V ❑USPS ❑Client II I �I' I�I I I II�IIII I�I
❑ Commercial E ace ❑Other; 192457390 1
Custody Seal Present? ❑Yes Uo Seals Intact? ❑Yes D<0—
Packing Material; ❑Bubble Wrap 2fubble Bags ❑None 0 Other
Thermometer; Type of Ice: 00et ❑Blue
EKG= ID: 9f2TO58
Cooler Temp ('Cl: r Correction Factor: Add/Subtract ('Cl 0.0°C
Cooler Temp Corrected
USCIA Regulated Sall (EYN/A, water sample)
Did samples origins a in a quarantine zone within the United States: CA, NY, or SC (check maps)?
r -Ivey
1
pate/Initials Person Examining Contents:����--/�
Vologlcal sue Frozen?
Dyes No [:]N/A
❑None
Temp should be alcove freezing to VC
❑Samples out of temp criteria. Samples on ice, cooling process
hasbegun
Dld sarplesoriglnate from a foreign source (internationally,
Ineludine Hawaii and PuertoRicol? 171YeS nNo
Comments/Dlscrepangy
of Custody Present?
01y.
❑No
jEA_
1.
_Chain
Samples Arrived within Hold Time?
es
❑No
❑NJA
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes
Na
❑N/A
3.
Rush Turn Around Time Requested?
❑vas
No
❑'�JA
4.
r—offitiFnt Volume?.
`
QNo
❑18/4
S.
Correct Containers Used?
-Pace Containers Used?
E31es
91/.'
[IN,
❑Nr
--ON/A
❑N/A
G.
"
Containers Intact?
2 es
❑Na
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑No
rv!A
8.
Sample Lapels Match COC7
-Includes 0ate/Time/ID/Analysis Matrix:
�<es
❑No
[I N/A
9.
Headspace in VOA Vials (>54n:m)?
❑Yes Q<_
N/A
10.
Trip Blank Present-
Trip Blank Custody Seals Present?
❑Yes
Yes
Elko
[]No
❑N/A
/A
11.
COMMENTS/SAMPLE DISCREPANCY
NI w 2' r � �•�- �
Lot 10 of split containers;
CLIENT NOTIFICATION/RE50LUTZN
Person contacted.
Date/Time; — __
Project Manager SCURF Review: r"1 1 1 lk Project Manager SRF Review: H-M7 -
Fleldl)ataf:equtred? []Yes [:]No
Date: ! J_1 9'1 q
Date: 12 v �4
Page 57 of 63
Document Name:
Document Revised: February7, 2018
�,
Sample Condition Upon Recelpt SCURI
Page 1 of 2
. a .wnalytiof
Document No.:
lssuingAuthority,
F-CAR-CS•033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination Is
verified and within the acceptance range for preservation
Samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"*Bottom half of box is to list number of bottle
Project # WO#
PM: AMB
CLIENT:
:92457590
Due Dale: 12/31/19
92-Municipal
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pH Adjustment Log for Fraserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservatlon adjusted
Time preservation
aejusted
Amount of Preservative
added
Lot H
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will beientto the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 58 of 63
Document Name:
Document Revised: February 7, 2018
1
Sample Condition Upon Recelpt(SCURI
Page 1 of 2
. aceAnalytical
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
*Check stark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, D110/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottle
Project # Wp# : 9245759D
F� Z
PM: AMB Due Date: 12/31/19
CLIENT: 92-Municipal
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added
Lot N
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 59 of 63
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lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
January 30, 2020
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
RE: Project: Surry WSW-2 (DW)
Pace Project No.: 92460944
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on January 16, 2020.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring for
Angela Baioni
angela.baioni@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Steven R. Gandy, Municipal Engineering Services Co.
Maddie German, Municipal Engineering Services
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 13
lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: Surry WSW-2 (DW)
Pace Project No.: 92460944
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 13
lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: Surry WSW-2 (DW)
Pace Project No.: 92460944
Lab ID Sample ID
92460944001 WSW-2
SAMPLE SUMMARY
Matrix Date Collected Date Received
Water 01 /15/20 13:30 01 /16/20 08:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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Page 3 of 13
lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Surry WSW-2 (DW)
92460944
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92460944001
WSW-2
HACH 10206
SOB
1
PASI-E
SM 4500-NO2 B-2011
SOB
1
PASI-E
EPA 200.7 Rev 4.4 1994
SH1
2
PASI-A
EPA 245.1 Rev 3.0 1994
SOO
1
PASI-A
EPA 300.0 Rev 2.1 1993
BRJ
3
PASI-A
REPORT OF LABORATORY ANALYSIS
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lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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(704)875-9092
ANALYTICAL RESULTS
Project: Surry WSW-2 (DW)
Pace Project No.: 92460944
Sample: WSW-2
Lab ID: 92460944001 Collected: 01/15/20 13:30
Received: 01/16/20 08:30 Matrix: Water
Report
Parameters
Results Units Limit MDL
DF
Prepared Analyzed
CAS No. Qual
HACH 10206 Nitrogen, Nitrate
Analytical Method: HACH 10206
Nitrogen, Nitrate
ND mg/L 0.30 0.30
1
01/17/20 11:23
14797-55-8 R1
450ONO2B Nitrite, unpres
Analytical Method: SM 4500-NO2 B-2011
Nitrogen, Nitrite
ND mg/L 0.010 0.0050
1
01/17/20 13:08
14797-65-0 M1
200.7 MET ICP
Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation
Method: EPA 200.7 Rev 4.4 1994
Iron
1150 ug/L 50.0 19.5
1
01/24/20 01:20 01/24/20 21:58
7439-89-6
Manganese
175 ug/L 5.0 0.90
1
01/24/20 01:20 01/24/20 21:58
7439-96-5
245.1 Mercury
Analytical Method: EPA 245.1 Rev 3.0 1994 Preparation
Method: EPA 245.1 Rev 3.0 1994
Mercury
ND ug/L 0.20 0.10
1
01/17/2017:50 01/20/2015:42
7439-97-6
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0 Rev 2.1 1993
Chloride
1.4 mg/L 1.0 0.60
1
01/23/20 23:01
16887-00-6
Fluoride
0.082J mg/L 0.10 0.050
1
01/23/20 23:01
16984-48-8
Sulfate
8.5 mg/L 1.0 0.50
1
01/23/20 23:01
14808-79-8
Date: 01/30/2020 02:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 13
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry WSW-2 (DW)
Pace Project No.: 92460944
QC Batch: 519959
Analysis Method:
HACH 10206
QC Batch Method: HACH 10206
Analysis Description:
10206 Nitrogen, Nitrate
Associated Lab Samples: 92460944001
METHOD BLANK: 2782423
Matrix: Water
Associated Lab Samples: 92460944001
Blank Reporting
Parameter Units
Result Limit
MDL Analyzed Qualifiers
Nitrogen, Nitrate mg/L
ND 0.30 0.30 01/17/20 11:23
LABORATORY CONTROL SAMPLE: 2782424
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Nitrate mg/L
5 5.0
101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2782425 2782426
MS MSD
92460944001
Spike Spike MS
MSD MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Nitrate mg/L ND
5 5 5.1
4.5 101 91 90-110 11 10 R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /30/2020 02:37 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 13
lV11.1 Analytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry WSW-2 (DW)
Pace Project No.: 92460944
QC Batch: 520000
Analysis Method:
SM 4500-NO2 B-2011
QC Batch Method: SM 4500-NO2 B-2011
Analysis Description:
4500NO2B, Nitrite, unpres
Associated Lab Samples: 92460944001
METHOD BLANK: 2782709
Matrix: Water
Associated Lab Samples: 92460944001
Blank Reporting
Parameter Units
Result Limit
MDL Analyzed Qualifiers
Nitrogen, Nitrite mg/L
ND 0.010 0.0050 01/17/20 13:07
LABORATORY CONTROL SAMPLE: 2782710
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Nitrite mg/L
0.1 0.10
102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2782711 2782712
MS MSD
92460944001
Spike Spike MS
MSD MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD RPD Qual
Nitrogen, Nitrite mg/L ND
0.1 0.1 0.11
0.11 110 111 90-110 1 10 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /30/2020 02:37 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 13
lV11.1 Analytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry WSW-2 (DW)
Pace Project No.: 92460944
QC Batch: 520036 Analysis Method: EPA 245.1 Rev 3.0 1994
QC Batch Method: EPA 245.1 Rev 3.0 1994 Analysis Description: 245.1 Mercury
Associated Lab Samples: 92460944001
METHOD BLANK: 2782854 Matrix: Water
Associated Lab Samples: 92460944001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Mercury ug/L ND 0.20 0.10 01/20/2015:26
LABORATORY CONTROL SAMPLE: 2782855
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 2.6 103 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2782856 2782857
MS MSD
92461112001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Mercury ug/L ND 2.5 2.5 3.8 2.4 143 88 70-130 45 20 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /30/2020 02:37 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 13
lV11.1 Analytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry WSW-2 (DW)
Pace Project No.: 92460944
QC Batch: 521152 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Associated Lab Samples: 92460944001
METHOD BLANK: 2788321 Matrix: Water
Associated Lab Samples: 92460944001
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Iron ug/L ND 50.0 19.5 01/24/20 21:34
Manganese ug/L ND 5.0 0.90 01/24/20 21:34
LABORATORY CONTROL SAMPLE: 2788322
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Iron ug/L 5000 4820 96 85-115
Manganese ug/L 500 477 95 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2788323
2788324
MS
MSD
92461738001
Spike
Spike
MS
MSD MS
MSD
% Rec
Max
Parameter Units
Result
Conc.
Conc.
Result
Result % Rec
% Rec
Limits
RPD RPD Qual
Iron ug/L
632
5000
5000
5720
5900 102
105
70-130
3 20
Manganese ug/L
23.5
500
500
503
534 96
102
70-130
6 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /30/2020 02:37 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 13
lV11.1 Analytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry WSW-2 (DW)
Pace Project No.: 92460944
QC Batch: 520630 Analysis Method: EPA 300.0 Rev 2.1 1993
QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92460944001
METHOD BLANK: 2785761
Associated Lab Samples: 92460944001
Parameter Units
Chloride mg/L
Fluoride mg/L
Sulfate mg/L
Matrix: Water
Blank Reporting
Result Limit
ND 1.0
ND 0.10
ND 1.0
MDL Analyzed
0.60 01/23/2017:31
0.050 01/23/2017:31
0.50 01/23/2017:31
Qualifiers
LABORATORY CONTROL SAMPLE: 2785762
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chloride mg/L 50 51.0 102 90-110
Fluoride mg/L 2.5 2.5 101 90-110
Sulfate mg/L 50 52.0 104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2785763
2785764
MS
MSD
92461517023 Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units
Result Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
Chloride mg/L
20.4 50
50
72.1
72.4
103
104
90-110
0 10
Fluoride mg/L
ND 2.5
2.5
2.5
2.6
98
104
90-110
5 10
Sulfate mg/L
115 50
50
162
163
95
95
90-110
0 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2785765
2785766
MS
MSD
2627951037 Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units
Result Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
Chloride mg/L
8.1 50
50
60.6
60.6
105
105
90-110
0 10
Fluoride mg/L
ND 2.5
2.5
2.5
2.6
99
101
90-110
2 10
Sulfate mg/L
2.5 50
50
55.2
55.2
106
106
90-110
0 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01 /30/2020 02:37 PM without the written consent of Pace Analytical Services, LLC.
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QUALIFIERS
Project: Surry WSW-2 (DW)
Pace Project No.: 92460944
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Surry WSW-2 (DW)
Pace Project No.: 92460944
Lab ID
Sample ID
QC Batch Method
QC Batch
92460944001
WSW-2
HACH 10206
519959
92460944001
WSW-2
SM 4500-NO2 B-2011
520000
92460944001
WSW-2
EPA 200.7 Rev 4.4 1994
521152
92460944001
WSW-2
EPA 245.1 Rev 3.0 1994
520036
92460944001
WSW-2
EPA 300.0 Rev 2.1 1993
520630
Date: 01/30/2020 02:37 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical Method
Analytical
Batch
EPA 200.7 Rev 4.4 1994 521175
EPA 245.1 Rev 3.0 1994 520079
Page 12 of 13
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Page 13 of 13
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
February 05, 2020
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
RE: Project: Surry WSW-2 (SWS)
Pace Project No.: 92460998
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on January 16, 2020.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
ft*OL-'
Angela Baioni
angela.baioni@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Steven R. Gandy, Municipal Engineering Services Co.
Maddie German, Municipal Engineering Services
REPORT OF LABORATORY ANALYSIS
r
e
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without the written consent of Pace Analytical Services, LLC.
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(704)875-9092
Project: Surry WSW-2 (SWS)
Pace Project No.: 92460998
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
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Project: Surry WSW-2 (SWS)
Pace Project No.: 92460998
Lab ID Sample ID
92460998001 WSW-2
SAMPLE SUMMARY
Matrix Date Collected Date Received
Water 01 /15/20 13:30 01 /16/20 08:30
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SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Surry WSW-2 (SWS)
92460998
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92460998001
WSW-2
EPA 6010D
KQ
14
PASI-A
EPA 6020E
BG2
1
PASI-A
EPA 8260D
CL
51
PASI-C
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ANALYTICAL RESULTS
Project: Surry WSW-2 (SWS)
Pace Project No.: 92460998
Sample: WSW-2 Lab ID: 92460998001 Collected: 01/15/20 13:30 Received: 01/16/20 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 02/05/2020 10:52 AM
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
ND
ug/L
5.0
3.0
1
01/25/20 01:26
01/27/20 22:24
7440-36-0
ND
ug/L
10.0
4.7
1
01/25/20 01:26
01/27/20 22:24
7440-38-2
11.7
ug/L
5.0
1.0
1
01/25/20 01:26
01/27/20 22:24
7440-39-3
N D
ug/L
1.0
0.20
1
01/25/20 01:26
01/27/20 22:24
7440-41-7
ND
ug/L
1.0
0.40
1
01/25/20 01:26
01/27/20 22:24
7440-43-9
ND
ug/L
5.0
1.0
1
01/25/20 01:26
01/27/20 22:24
7440-47-3
ND
ug/L
5.0
1.1
1
01/25/20 01:26
01/27/20 22:24
7440-48-4
3.2J
ug/L
5.0
2.1
1
01/25/20 01:26
01/27/20 22:24
7440-50-8
ND
ug/L
5.0
1.6
1
01/25/20 01:26
01/27/20 22:24
7439-92-1
1.2J
ug/L
5.0
0.90
1
01/25/20 01:26
01/27/20 22:24
7440-02-0
ND
ug/L
10.0
4.7
1
01/25/20 01:26
01/27/20 22:24
7782-49-2
ND
ug/L
5.0
2.5
1
01/25/20 01:26
01/27/20 22:24
7440-22-4
ND
ug/L
5.0
1.3
1
01/25/20 01:26
01/27/20 22:24
7440-62-2
ND
ug/L
10.0
3.9
1
01/25/20 01:26
01/27/20 22:24
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 0.10 0.060 1 01/24/20 02:35 02/03/20 18:54 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
01/27/2014:54
67-64-1 v1
ND
ug/L
10.0
0.90
1
01/27/2014:54
107-13-1
N D
ug/L
1.0
0.15
1
01/27/20 14:54
71-43-2
ND
ug/L
1.0
0.34
1
01/27/2014:54
74-97-5
ND
ug/L
1.0
0.26
1
01/27/2014:54
75-27-4
ND
ug/L
1.0
0.62
1
01/27/2014:54
75-25-2
ND
ug/L
2.0
0.62
1
01/27/2014:54
74-83-9 IH,IK
ND
ug/L
5.0
3.3
1
01/27/2014:54
78-93-3
ND
ug/L
2.0
0.40
1
01/27/2014:54
75-15-0
ND
ug/L
1.0
0.22
1
01/27/2014:54
56-23-5
ND
ug/L
1.0
0.23
1
01/27/2014:54
108-90-7
ND
ug/L
1.0
0.49
1
01/27/2014:54
75-00-3
ND
ug/L
5.0
2.3
1
01/27/2014:54
67-66-3
ND
ug/L
1.0
0.39
1
01/27/2014:54
74-87-3
ND
ug/L
5.0
0.26
1
01/27/2014:54
96-12-8
ND
ug/L
1.0
0.41
1
01/27/2014:54
124-48-1
ND
ug/L
1.0
0.26
1
01/27/2014:54
106-93-4
ND
ug/L
1.0
0.46
1
01/27/2014:54
74-95-3
ND
ug/L
1.0
0.29
1
01/27/2014:54
95-50-1
ND
ug/L
1.0
0.26
1
01/27/2014:54
106-46-7
ND
ug/L
1.0
0.54
1
01/27/2014:54
110-57-6 v1
ND
ug/L
1.0
0.27
1
01/27/2014:54
75-34-3
ND
ug/L
1.0
0.34
1
01/27/2014:54
107-06-2
ND
ug/L
1.0
0.24
1
01/27/2014:54
75-35-4
0.43J
ug/L
1.0
0.29
1
01/27/2014:54
156-59-2
ND
ug/L
1.0
0.25
1
01/27/2014:54
156-60-5
ND
ug/L
1.0
0.19
1
01/27/2014:54
78-87-5
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ANALYTICAL RESULTS
Project: Surry WSW-2 (SWS)
Pace Project No.: 92460998
Sample: WSW-2
Lab ID:
92460998001
Collected:
01/15/20 13:30
Received: 01/16/20 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
01/27/20 14:54
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
01/27/20 14:54
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
01/27/20 14:54
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
01/27/20 14:54
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
01/27/20 14:54
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
01/27/20 14:54
74-88-4
Methylene Chloride
ND
ug/L
5.0
3.7
1
01/27/20 14:54
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
01/27/20 14:54
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
01/27/20 14:54
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
01/27/20 14:54
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
01/27/20 14:54
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
01/27/20 14:54
127-18-4
Toluene
0.32J
ug/L
1.0
0.24
1
01/27/20 14:54
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
01/27/20 14:54
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
01/27/20 14:54
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
01/27/20 14:54
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
01/27/20 14:54
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
01/27/20 14:54
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
01/27/20 14:54
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
01/27/20 14:54
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
01/27/20 14:54
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
105
%
70-130
1
01/27/20 14:54
460-00-4
1,2-Dichloroethane-d4 (S)
112
%
70-130
1
01/27/20 14:54
17060-07-0
Toluene-d8 (S)
103
%
70-130
1
01/27/20 14:54
2037-26-5
Date: 02/05/2020 10:52 AM
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: Surry WSW-2 (SWS)
Pace Project No.: 92460998
QC Batch: 521394 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92460998001
METHOD BLANK: 2789535
Associated Lab Samples: 92460998001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Antimony
ug/L
ND
5.0
3.0
01/27/20 22:08
Arsenic
ug/L
ND
10.0
4.7
01/27/20 22:08
Barium
ug/L
ND
5.0
1.0
01/27/20 22:08
Beryllium
ug/L
ND
1.0
0.20
01/27/20 22:08
Cadmium
ug/L
ND
1.0
0.40
01/27/20 22:08
Chromium
ug/L
ND
5.0
1.0
01/27/20 22:08
Cobalt
ug/L
ND
5.0
1.1
01/27/20 22:08
Copper
ug/L
ND
5.0
2.1
01/27/20 22:08
Lead
ug/L
ND
5.0
1.6
01/27/20 22:08
Nickel
ug/L
ND
5.0
0.90
01/27/20 22:08
Selenium
ug/L
ND
10.0
4.7
01/27/20 22:08
Silver
ug/L
ND
5.0
2.5
01/27/20 22:08
Vanadium
ug/L
ND
5.0
1.3
01/27/20 22:08
Zinc
ug/L
ND
10.0
3.9
01/27/20 22:08
LABORATORY CONTROL SAMPLE:
Parameter
2789536
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
483
97
80-120
Arsenic
ug/L
500
470
94
80-120
Barium
ug/L
500
488
98
80-120
Beryllium
ug/L
500
485
97
80-120
Cadmium
ug/L
500
478
96
80-120
Chromium
ug/L
500
478
96
80-120
Cobalt
ug/L
500
482
96
80-120
Copper
ug/L
500
491
98
80-120
Lead
ug/L
500
479
96
80-120
Nickel
ug/L
500
484
97
80-120
Selenium
ug/L
500
454
91
80-120
Silver
ug/L
250
240
96
80-120
Vanadium
ug/L
500
480
96
80-120
Zinc
ug/L
500
462
92
80-120
Qualifiers
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2789537 2789538
MS MSD
92460998001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Antimony ug/L ND 500 500 498 498 99 99 75-125 0 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/05/2020 10:52 AM without the written consent of Pace Analytical Services, LLC.
Page 7 of 18
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project:
Pace Project No.:
Surry WSW-2 (SWS)
92460998
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2789537
2789538
MS
MSD
92460998001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Arsenic
ug/L
ND
500
500
482
484
96
96
75-125
0
20
Barium
ug/L
11.7
500
500
512
510
100
100
75-125
0
20
Beryllium
ug/L
ND
500
500
506
502
101
100
75-125
1
20
Cadmium
ug/L
ND
500
500
503
501
101
100
75-125
0
20
Chromium
ug/L
ND
500
500
501
502
100
100
75-125
0
20
Cobalt
ug/L
ND
500
500
489
488
98
97
75-125
0
20
Copper
ug/L
3.2J
500
500
505
510
100
101
75-125
1
20
Lead
ug/L
ND
500
500
496
494
99
99
75-125
0
20
Nickel
ug/L
1.2J
500
500
495
491
99
98
75-125
1
20
Selenium
ug/L
ND
500
500
514
512
103
102
75-125
0
20
Silver
ug/L
ND
250
250
250
251
100
100
75-125
0
20
Vanadium
ug/L
ND
500
500
492
488
98
98
75-125
1
20
Zinc
ug/L
ND
500
500
486
481
97
96
75-125
1
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/05/2020 10:52 AM without the written consent of Pace Analytical Services, LLC.
Page 8 of 18
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry WSW-2 (SWS)
Pace Project No.: 92460998
QC Batch: 521171
Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A
Analysis Description: 6020 MET
Associated Lab Samples: 92460998001
METHOD BLANK: 2788393
Matrix: Water
Associated Lab Samples: 92460998001
Blank Reporting
Parameter Units
Result Limit MDL
Analyzed Qualifiers
Thallium ug/L
ND 0.10 0.060 02/03/2018:32
LABORATORY CONTROL SAMPLE: 2788394
Spike LCS LCS
% Rec
Parameter Units
Conc. Result % Rec
Limits Qualifiers
Thallium ug/L
10 9.4 94
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2788395 2788396
MS MSD
92460998001
Spike Spike MS MSD
MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result Result
% Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND
10 10 9.7 9.9
97 98 75-125 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/05/2020 10:52 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 18
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry WSW-2 (SWS)
Pace Project No.: 92460998
QC Batch: 521561 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Associated Lab Samples: 92460998001
METHOD BLANK: 2790180
Associated Lab Samples: 92460998001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.34
01/27/20 13:28
1,1,1-Trichloroethane
ug/L
ND
1.0
0.18
01/27/20 13:28
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
01/27/20 13:28
1,1,2-Trichloroethane
ug/L
ND
1.0
0.24
01/27/20 13:28
1,1-Dichloroethane
ug/L
ND
1.0
0.27
01/27/20 13:28
1,1-Dichloroethene
ug/L
ND
1.0
0.24
01/27/20 13:28
1,2,3-Trichloropropane
ug/L
ND
1.0
0.35
01/27/20 13:28
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
0.26
01/27/20 13:28
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.26
01/27/20 13:28
1,2-Dichlorobenzene
ug/L
ND
1.0
0.29
01/27/20 13:28
1,2-Dichloroethane
ug/L
ND
1.0
0.34
01/27/20 13:28
1,2-Dichloropropane
ug/L
ND
1.0
0.19
01/27/20 13:28
1,4-Dichlorobenzene
ug/L
ND
1.0
0.26
01/27/20 13:28
1,4-Dioxane (p-Dioxane)
ug/L
ND
150
56.2
01/27/20 13:28
2-Butanone (MEK)
ug/L
ND
5.0
3.3
01/27/20 13:28
2-Hexanone
ug/L
ND
5.0
0.57
01/27/20 13:28
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
4.5
01/27/20 13:28
Acetone
ug/L
ND
25.0
6.2
01/27/20 13:28
Acrylonitrile
ug/L
ND
10.0
0.90
01/27/20 13:28
Benzene
ug/L
ND
1.0
0.15
01/27/20 13:28
Bromochloromethane
ug/L
ND
1.0
0.34
01/27/20 13:28
Bromodichloromethane
ug/L
ND
1.0
0.26
01/27/20 13:28
Bromoform
ug/L
ND
1.0
0.62
01/27/20 13:28
Bromomethane
ug/L
ND
2.0
0.62
01/27/20 13:28
Carbon disulfide
ug/L
ND
2.0
0.40
01/27/20 13:28
Carbon tetrachloride
ug/L
ND
1.0
0.22
01/27/20 13:28
Chlorobenzene
ug/L
ND
1.0
0.23
01/27/20 13:28
Chloroethane
ug/L
ND
1.0
0.49
01/27/20 13:28
Chloroform
ug/L
ND
5.0
2.3
01/27/20 13:28
Chloromethane
ug/L
ND
1.0
0.39
01/27/20 13:28
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.29
01/27/20 13:28
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.30
01/27/20 13:28
Dibromochloromethane
ug/L
ND
1.0
0.41
01/27/20 13:28
Dibromomethane
ug/L
ND
1.0
0.46
01/27/20 13:28
Ethylbenzene
ug/L
ND
1.0
0.26
01/27/20 13:28
lodomethane
ug/L
ND
20.0
12.5
01/27/20 13:28
Methylene Chloride
ug/L
ND
5.0
3.7
01/27/20 13:28
Styrene
ug/L
ND
1.0
0.27
01/27/20 13:28
Tetrachloroethene
ug/L
ND
1.0
0.16
01/27/20 13:28
Toluene
ug/L
ND
1.0
0.24
01/27/20 13:28
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.25
01/27/20 13:28
Qualifiers
v1
IH,IK
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/05/2020 10:52 AM without the written consent of Pace Analytical Services, LLC. Page 10 of 18
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: Surry WSW-2 (SWS)
Pace Project No.: 92460998
METHOD BLANK: 2790180
Associated Lab Samples: 92460998001
Parameter
Units
trans- 1,3-Dichloropropene
ug/L
trans-1,4-Dichloro-2-butene
ug/L
Trichloroethene
ug/L
Trichlorofluoromethane
ug/L
Vinyl acetate
ug/L
Vinyl chloride
ug/L
Xylene (Total)
ug/L
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LABORATORY CONTROL SAMPLE: 2790181
Parameter
QUALITY CONTROL DATA
Matrix: Water
Blank
Result
Reporting
Limit
ND
1.0
ND
1.0
ND
1.0
ND
1.0
ND
2.0
ND
1.0
ND
1.0
112
70-130
104
70-130
103
70-130
MDL Analyzed
0.31
01 /27/20 13:28
0.54
01 /27/20 13:28
0.22
01 /27/20 13:28
0.31
01 /27/20 13:28
1.4
01 /27/20 13:28
0.24
01 /27/20 13:28
0.63
01 /27/20 13:28
01 /27/20 13:28
01 /27/20 13:28
01 /27/20 13:28
v1
Qualifiers
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
52.1
104
70-130
1,1,1-Trichloroethane
ug/L
50
55.3
111
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
49.4
99
70-130
1,1,2-Trichloroethane
ug/L
50
54.5
109
70-130
1,1-Dichloroethane
ug/L
50
52.8
106
70-130
1,1-Dichloroethene
ug/L
50
53.7
107
70-130
1,2,3-Trichloropropane
ug/L
50
47.4
95
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
53.6
107
70-130
1,2-Dibromoethane (EDB)
ug/L
50
52.3
105
70-130
1,2-Dichlorobenzene
ug/L
50
48.6
97
70-130
1,2-Dichloroethane
ug/L
50
52.8
106
70-130
1,2-Dichloropropane
ug/L
50
53.0
106
70-130
1,4-Dichlorobenzene
ug/L
50
47.6
95
70-130
1,4-Dioxane(p-Dioxane)
ug/L
1000
1060
106
59-169
2-Butanone (MEK)
ug/L
100
113
113
64-135
2-Hexanone
ug/L
100
104
104
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
108
108
70-130
Acetone
ug/L
100
120
120
61-157 v1
Acrylonitrile
ug/L
250
272
109
61-143
Benzene
ug/L
50
51.8
104
70-130
Bromochloromethane
ug/L
50
55.6
111
70-130
Bromodichloromethane
ug/L
50
53.1
106
70-130
Bromoform
ug/L
50
51.8
104
70-130
Bromomethane
ug/L
50
54.8
110
38-130lH,IK
Carbon disulfide
ug/L
50
57.8
116
68-130
Carbon tetrachloride
ug/L
50
53.4
107
70-130
Chlorobenzene
ug/L
50
48.7
97
70-130
Chloroethane
ug/L
50
52.2
104
37-142
Chloroform
ug/L
50
54.4
109
70-130
Chloromethane
ug/L
50
47.3
95
48-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/05/2020 10:52 AM without the written consent of Pace Analytical Services, LLC. Page 11 of 18
Pace Analytical Services, LLC
9800
lCtaac,Analyfical ® Kiney Ave. Suite 100
Huntersville, NC 28078
0788
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: Surry WSW-2 (SWS)
Pace Project No.: 92460998
LABORATORY CONTROL SAMPLE:
Parameter
2790181
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
cis-1,2-Dichloroethene
ug/L
50
53.6
107
70-130
cis-1,3-Dichloropropene
ug/L
50
54.7
109
70-130
Dibromochloromethane
ug/L
50
52.5
105
70-130
Dibromomethane
ug/L
50
53.2
106
70-130
Ethylbenzene
ug/L
50
47.6
95
70-130
lodomethane
ug/L
100
105
105
40-130
Methylene Chloride
ug/L
50
54.0
108
67-132
Styrene
ug/L
50
48.8
98
70-130
Tetrachloroethene
ug/L
50
48.6
97
69-130
Toluene
ug/L
50
50.1
100
70-130
trans-1,2-Dichloroethene
ug/L
50
53.3
107
70-130
trans- 1,3-Dichloropropene
ug/L
50
55.2
110
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
81.9
164
35-189 v1
Trichloroethene
ug/L
50
53.3
107
70-130
Trichlorofluoromethane
ug/L
50
51.6
103
63-130
Vinyl acetate
ug/L
100
119
119
55-143
Vinyl chloride
ug/L
50
59.0
118
70-131
Xylene (Total)
ug/L
150
143
95
70-130
1,2-Dichloroethane-d4 (S)
%
104
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8(S)
%
101
70-130
MATRIX SPIKE SAMPLE:
Parameter
2790183
Units
92461000001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
21.7
108
73-134
1,1,1-Trichloroethane
ug/L
ND
20
27.5
137
82-143
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20.2
101
70-136
1,1,2-Trichloroethane
ug/L
ND
20
24.0
120
70-135
1,1-Dichloroethane
ug/L
ND
20
26.8
134
70-139
1,1-Dichloroethene
ug/L
ND
20
28.2
141
70-154
1,2,3-Trichloropropane
ug/L
ND
20
19.8
99
71-137
1,2-Dibromo-3-chloropropane
ug/L
ND
20
21.1
106
65-134
1,2-Dibromoethane (EDB)
ug/L
ND
20
21.0
105
70-137
1,2-Dichlorobenzene
ug/L
ND
20
21.0
105
70-133
1,2-Dichloroethane
ug/L
ND
20
25.7
128
70-137
1,2-Dichloropropane
ug/L
ND
20
24.1
121
70-140
1,4-Dichlorobenzene
ug/L
ND
20
21.0
105
70-133
1,4-Dioxane (p-Dioxane)
ug/L
ND
400
439
110
53-168
2-Butanone (MEK)
ug/L
ND
40
52.7
132
60-139
2-Hexanone
ug/L
ND
40
40.0
100
65-138
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
43.3
108
65-135
Acetone
ug/L
ND
40
54.8
137
60-148 v1
Acrylonitrile
ug/L
ND
100
124
124
64-147
Benzene
ug/L
1.5
20
26.6
125
70-151
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/05/2020 10:52 AM without the written consent of Pace Analytical Services, LLC. Page 12 of 18
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry WSW-2 (SWS)
Pace Project No.: 92460998
MATRIX SPIKE SAMPLE: 2790183
92461000001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Bromochloromethane
ug/L
ND
20
27.0
135
70-141
Bromodichloromethane
ug/L
ND
20
24.2
121
70-138
Bromoform
ug/L
ND
20
19.4
97
63-130
Bromomethane
ug/L
ND
20
23.5
117
15-152 IH,IK
Carbon disulfide
ug/L
ND
20
27.8
139
69-149
Carbon tetrachloride
ug/L
ND
20
26.1
131
70-143
Chlorobenzene
ug/L
ND
20
21.6
108
70-138
Chloroethane
ug/L
ND
20
30.2
151
52-163
Chloroform
ug/L
ND
20
26.7
133
70-139
Chloromethane
ug/L
ND
20
25.3
126
41-139
cis-1,2-Dichloroethene
ug/L
1.9
20
28.9
135
70-141
cis-1,3-Dichloropropene
ug/L
ND
20
23.4
117
70-137
Dibromochloromethane
ug/L
ND
20
21.4
107
70-134
Dibromomethane
ug/L
ND
20
23.8
119
70-138
Ethylbenzene
ug/L
ND
20
21.2
106
66-153
Iodomethane
ug/L
ND
40
43.9
110
20-138
Methylene Chloride
ug/L
ND
20
27.5
138
42-159
Styrene
ug/L
ND
20
21.5
108
70-135
Tetrachloroethene
ug/L
ND
20
21.3
107
59-143
Toluene
ug/L
ND
20
23.1
116
59-148
trans-1,2-Dichloroethene
ug/L
ND
20
27.4
137
70-146
trans- 1,3-Dichloropropene
ug/L
ND
20
23.1
115
70-135
trans-1,4-Dichloro-2-butene
ug/L
ND
20
17.6
88
47-135 v1
Trichloroethene
ug/L
ND
20
25.2
126
70-147
Trichlorofluoromethane
ug/L
ND
20
26.8
134
70-148
Vinyl acetate
ug/L
ND
40
46.6
117
49-151
Vinyl chloride
ug/L
0.65J
20
32.9
161
70-156 M1
Xylene (Total)
ug/L
ND
60
64.6
108
63-158
1,2-Dichloroethane-d4 (S)
%
111
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8(S)
%
101
70-130
SAMPLE DUPLICATE: 2790182
92460999001
Dup
Max
Parameter
Units
Result
Result RPD
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,1-Trichloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
ND
ND
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,2,3-Trichloropropane
ug/L
ND
ND
30
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
30
1,2-Dibromoethane (EDB)
ug/L
ND
ND
30
1,2-Dichlorobenzene
ug/L
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry WSW-2 (SWS)
Pace Project No.: 92460998
SAMPLE DUPLICATE: 2790182
Parameter
Units
92460999001
Result
Dup
Result RPD
Max
RPD Qualifiers
1,2-Dichloroethane
ug/L
ND
ND
30
1,2-Dichloropropane
ug/L
ND
ND
30
1,4-Dichlorobenzene
ug/L
ND
ND
30
1,4-Dioxane (p-Dioxane)
ug/L
ND
ND
30
2-Butanone (MEK)
ug/L
ND
ND
30
2-Hexanone
ug/L
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
30
Acetone
ug/L
ND
ND
30 v1
Acrylonitrile
ug/L
ND
ND
30
Benzene
ug/L
ND
ND
30
Bromochloromethane
ug/L
ND
ND
30
Bromodichloromethane
ug/L
ND
ND
30
Bromoform
ug/L
ND
ND
30
Bromomethane
ug/L
ND
ND
301H,IK
Carbon disulfide
ug/L
ND
ND
30
Carbon tetrachloride
ug/L
ND
ND
30
Chlorobenzene
ug/L
ND
ND
30
Chloroethane
ug/L
ND
ND
30
Chloroform
ug/L
ND
ND
30
Chloromethane
ug/L
ND
ND
30
cis-1,2-Dichloroethene
ug/L
ND
ND
30
cis-1,3-Dichloropropene
ug/L
ND
ND
30
Dibromochloromethane
ug/L
ND
ND
30
Dibromomethane
ug/L
ND
ND
30
Ethylbenzene
ug/L
ND
ND
30
lodomethane
ug/L
ND
ND
30
Methylene Chloride
ug/L
ND
ND
30
Styrene
ug/L
ND
ND
30
Tetrachloroethene
ug/L
ND
ND
30
Toluene
ug/L
ND
ND
30
trans-1,2-Dichloroethene
ug/L
ND
ND
30
trans- 1,3-Dichloropropene
ug/L
ND
ND
30
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
30 v1
Trichloroethene
ug/L
ND
ND
30
Trichlorofluoromethane
ug/L
ND
ND
30
Vinyl acetate
ug/L
ND
ND
30
Vinyl chloride
ug/L
ND
ND
30
Xylene (Total)
ug/L
ND
ND
30
1,2-Dichloroethane-d4 (S)
%
115
113
4-Bromofluorobenzene (S)
%
105
105
Toluene-d8 (S)
%
103
102
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/05/2020 10:52 AM without the written consent of Pace Analytical Services, LLC.
Page 14 of 18
Pace Analytical Services, LLC
9800
lCtaac,Analyfical ® Kiney Ave. Suite 100
Huntersville, NC 28078
0788
www.pacelabs.com (704)875-9092
QUALIFIERS
Project: Surry WSW-2 (SWS)
Pace Project No.: 92460998
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
REPORT OF LABORATORY ANALYSIS
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Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Surry WSW-2 (SWS)
92460998
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92460998001
WSW-2
EPA 3010A
521394 EPA 6010D
521404
92460998001
WSW-2
EPA 3010A
521171 EPA 6020B
521187
92460998001
WSW-2
EPA 8260D
521561
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/05/2020 10:52 AM without the written consent of Pace Analytical Services, LLC. Page 16 of 18
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Page 18 of 18
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
February 07, 2020
Mr. Jonathan Pfohl
Municipal Engineering Services
68 Shipwash Dr.
Garner, NC 27529
RE: Project: Surry MSWLF SWs
Pace Project No.: 92457589
Dear Mr. Pfohl:
Enclosed are the analytical results for sample(s) received by the laboratory on December 16, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
A revised report is being generated on 2/7/2020 to remove results for sample 92457589005, per
client request.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
angela.baioni@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Steven R. Gandy, Municipal Engineering Services Co.
Maddie German, Municipal Engineering Services
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 38
lceAnalyircal
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: Surry MSWLF SWs
Pace Project No.: 92457589
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 2 of 38
lceAnalyircal
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(704)875-9092
SAMPLE SUMMARY
Project: Surry MSWLF SWs
Pace Project No.: 92457589
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92457589001
SW-1
Water
12/12/19 12:10
12/16/19 08:30
92457589002
SW-2
Water
12/13/19 14:28
12/16/19 08:30
92457589003
SW-3
Water
12/13/19 15:08
12/16/19 08:30
92457589004
SW-4
Water
12/13/19 13:30
12/16/19 08:30
92457589006
SWN-2
Water
12/12/19 16:55
12/16/19 08:30
92457589007
SW-C
Water
12/13/19 13:45
12/16/19 08:30
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 38
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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(704)875-9092
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Surry MSWLF SWs
92457589
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92457589001
SW-1
EPA 601 OD
KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92457589002
SW-2
EPA 601 OD
KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92457589003
SW-3
EPA 601 OD
KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92457589004
SW-4
EPA 601 OD
KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92457589006
SWN-2
EPA 601 OD
KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
92457589007
SW-C
EPA 601 OD
KQ
14
PASI-A
EPA 6020E
JOR
1
PASI-A
EPA 8260D
CL
51
PASI-C
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92457589
Sample: SW-1 Lab ID: 92457589001 Collected: 12/12/19 12:10 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 02/07/2020 11:46 AM
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
ND
ug/L
5.0
3.0
1
12/24/19 01:21
12/25/19 00:18
7440-36-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/25/19 00:18
7440-38-2
20.7
ug/L
5.0
1.0
1
12/24/19 01:21
12/25/19 00:18
7440-39-3
0.75J
ug/L
1.0
0.20
1
12/24/19 01:21
12/25/19 00:18
7440-41-7
0.67J
ug/L
1.0
0.40
1
12/24/19 01:21
12/25/19 00:18
7440-43-9
ND
ug/L
5.0
1.0
1
12/24/19 01:21
12/25/19 00:18
7440-47-3
ND
ug/L
5.0
1.1
1
12/24/19 01:21
12/25/19 00:18
7440-48-4
ND
ug/L
5.0
2.1
1
12/24/19 01:21
12/25/19 00:18
7440-50-8
ND
ug/L
5.0
1.6
1
12/24/19 01:21
12/25/19 00:18
7439-92-1
1.0J
ug/L
5.0
0.90
1
12/24/19 01:21
12/25/19 00:18
7440-02-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/25/19 00:18
7782-49-2
ND
ug/L
5.0
2.5
1
12/24/19 01:21
12/25/19 00:18
7440-22-4
1.8J
ug/L
5.0
1.3
1
12/24/19 01:21
12/25/19 00:18
7440-62-2
4.3J
ug/L
10.0
3.9
1
12/24/19 01:21
12/25/19 00:18
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 0.10 0.060 1 12/24/19 02:04 12/30/19 15:54 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
12/23/1918:21
67-64-1
ND
ug/L
10.0
0.90
1
12/23/1918:21
107-13-1
ND
ug/L
1.0
0.15
1
12/23/1918:21
71-43-2
ND
ug/L
1.0
0.34
1
12/23/1918:21
74-97-5
ND
ug/L
1.0
0.26
1
12/23/1918:21
75-27-4
ND
ug/L
1.0
0.62
1
12/23/1918:21
75-25-2
ND
ug/L
2.0
0.62
1
12/23/1918:21
74-83-9
ND
ug/L
5.0
3.3
1
12/23/1918:21
78-93-3
ND
ug/L
2.0
0.40
1
12/23/1918:21
75-15-0
ND
ug/L
1.0
0.22
1
12/23/1918:21
56-23-5
ND
ug/L
1.0
0.23
1
12/23/1918:21
108-90-7
ND
ug/L
1.0
0.49
1
12/23/1918:21
75-00-3
ND
ug/L
5.0
2.3
1
12/23/1918:21
67-66-3
ND
ug/L
1.0
0.39
1
12/23/1918:21
74-87-3
ND
ug/L
5.0
0.26
1
12/23/1918:21
96-12-8
ND
ug/L
1.0
0.41
1
12/23/1918:21
124-48-1
ND
ug/L
1.0
0.26
1
12/23/1918:21
106-93-4
ND
ug/L
1.0
0.46
1
12/23/1918:21
74-95-3
ND
ug/L
1.0
0.29
1
12/23/1918:21
95-50-1
ND
ug/L
1.0
0.26
1
12/23/1918:21
106-46-7
ND
ug/L
1.0
0.54
1
12/23/1918:21
110-57-6
ND
ug/L
1.0
0.27
1
12/23/1918:21
75-34-3
ND
ug/L
1.0
0.34
1
12/23/1918:21
107-06-2
ND
ug/L
1.0
0.24
1
12/23/1918:21
75-35-4
ND
ug/L
1.0
0.29
1
12/23/1918:21
156-59-2
ND
ug/L
1.0
0.25
1
12/23/1918:21
156-60-5
ND
ug/L
1.0
0.19
1
12/23/1918:21
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 38
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92457589
Sample: SW-1
Lab ID:
92457589001
Collected:
12/12/19 12:10
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/23/19 18:21
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/23/19 18:21
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/23/19 18:21
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/23/19 18:21
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/23/19 18:21
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/23/19 18:21
74-88-4
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/23/19 18:21
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/23/19 18:21
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/23/19 18:21
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/23/19 18:21
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/23/19 18:21
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/23/19 18:21
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/23/19 18:21
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/23/19 18:21
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/23/19 18:21
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/23/19 18:21
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/23/19 18:21
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/23/19 18:21
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/23/19 18:21
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
12/23/19 18:21
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/23/19 18:21
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
101
%
70-130
1
12/23/19 18:21
460-00-4
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
12/23/19 18:21
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
12/23/19 18:21
2037-26-5
Date: 02/07/2020 11:46 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 38
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92457589
Sample: SW-2 Lab ID: 92457589002 Collected: 12/13/19 14:28 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 601 OD Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.0
1
12/24/19 01:21
12/24/19 22:47
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 22:47
7440-38-2
Barium
18.8
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 22:47
7440-39-3
Beryllium
0.20J
ug/L
1.0
0.20
1
12/24/19 01:21
12/24/19 22:47
7440-41-7
B
Cadmium
0.811
ug/L
1.0
0.40
1
12/24/19 01:21
12/24/19 22:47
7440-43-9
Chromium
ND
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 22:47
7440-47-3
Cobalt
21.3
ug/L
5.0
1.1
1
12/24/19 01:21
12/24/19 22:47
7440-48-4
Copper
ND
ug/L
5.0
2.1
1
12/24/19 01:21
12/24/19 22:47
7440-50-8
Lead
ND
ug/L
5.0
1.6
1
12/24/19 01:21
12/24/19 22:47
7439-92-1
Nickel
ND
ug/L
5.0
0.90
1
12/24/19 01:21
12/24/19 22:47
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 22:47
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
12/24/19 01:21
12/24/19 22:47
7440-22-4
Vanadium
ND
ug/L
5.0
1.3
1
12/24/19 01:21
12/24/19 22:47
7440-62-2
Zinc
4.8J
ug/L
10.0
3.9
1
12/24/19 01:21
12/24/19 22:47
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
ND
ug/L
0.10
0.060
1
12/24/19 02:04
12/30/19 18:19
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Acetone
ND
ug/L
25.0
6.2
1
12/24/19 00:54
67-64-1
Acrylonitrile
ND
ug/L
10.0
0.90
1
12/24/19 00:54
107-13-1
Benzene
ND
ug/L
1.0
0.15
1
12/24/19 00:54
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.34
1
12/24/19 00:54
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.26
1
12/24/19 00:54
75-27-4
Bromoform
ND
ug/L
1.0
0.62
1
12/24/19 00:54
75-25-2
Bromomethane
ND
ug/L
2.0
0.62
1
12/24/19 00:54
74-83-9
v2
2-Butanone (MEK)
ND
ug/L
5.0
3.3
1
12/24/19 00:54
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.40
1
12/24/19 00:54
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.22
1
12/24/19 00:54
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.23
1
12/24/19 00:54
108-90-7
Chloroethane
ND
ug/L
1.0
0.49
1
12/24/19 00:54
75-00-3
v2
Chloroform
ND
ug/L
5.0
2.3
1
12/24/19 00:54
67-66-3
Chloromethane
ND
ug/L
1.0
0.39
1
12/24/19 00:54
74-87-3
v2
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
0.26
1
12/24/19 00:54
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.41
1
12/24/19 00:54
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.26
1
12/24/19 00:54
106-93-4
Dibromomethane
ND
ug/L
1.0
0.46
1
12/24/19 00:54
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.29
1
12/24/19 00:54
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.26
1
12/24/19 00:54
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.54
1
12/24/19 00:54
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.27
1
12/24/19 00:54
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.34
1
12/24/19 00:54
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.24
1
12/24/19 00:54
75-35-4
cis-1,2-Dichloroethene
3.0
ug/L
1.0
0.29
1
12/24/19 00:54
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
0.25
1
12/24/19 00:54
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.19
1
12/24/19 00:54
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/07/2020 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 7 of 38
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92457589
Sample: SW-2
Lab ID:
92457589002
Collected:
12/13/19 14:28
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/24/19 00:54
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/24/19 00:54
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/24/19 00:54
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/24/19 00:54
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/24/19 00:54
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/24/19 00:54
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/24/19 00:54
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/24/19 00:54
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/24/19 00:54
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/24/19 00:54
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/24/19 00:54
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/24/19 00:54
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/24/19 00:54
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/24/19 00:54
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/24/19 00:54
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/24/19 00:54
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/24/19 00:54
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/24/19 00:54
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/24/19 00:54
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
12/24/19 00:54
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/24/19 00:54
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
12/24/19 00:54
460-00-4
1,2-Dichloroethane-d4 (S)
100
%
70-130
1
12/24/19 00:54
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
12/24/19 00:54
2037-26-5
Date: 02/07/2020 11:46 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 38
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92457589
Sample: SW-3 Lab ID: 92457589003 Collected: 12/13/19 15:08 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Antimony
ND
ug/L
5.0
3.0
1
12/24/19 01:21
12/24/19 22:59
7440-36-0
Arsenic
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 22:59
7440-38-2
Barium
26.4
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 22:59
7440-39-3
Beryllium
0.31J
ug/L
1.0
0.20
1
12/24/19 01:21
12/24/19 22:59
7440-41-7
B
Cadmium
0.56J
ug/L
1.0
0.40
1
12/24/19 01:21
12/24/19 22:59
7440-43-9
Chromium
ND
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 22:59
7440-47-3
Cobalt
1.4J
ug/L
5.0
1.1
1
12/24/19 01:21
12/24/19 22:59
7440-48-4
Copper
3.1J
ug/L
5.0
2.1
1
12/24/19 01:21
12/24/19 22:59
7440-50-8
Lead
ND
ug/L
5.0
1.6
1
12/24/19 01:21
12/24/19 22:59
7439-92-1
Nickel
ND
ug/L
5.0
0.90
1
12/24/19 01:21
12/24/19 22:59
7440-02-0
Selenium
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 22:59
7782-49-2
Silver
ND
ug/L
5.0
2.5
1
12/24/19 01:21
12/24/19 22:59
7440-22-4
Vanadium
3.5J
ug/L
5.0
1.3
1
12/24/19 01:21
12/24/19 22:59
7440-62-2
Zinc
11.7
ug/L
10.0
3.9
1
12/24/19 01:21
12/24/19 22:59
7440-66-6
6020 MET ICPMS
Analytical Method: EPA 6020E Preparation Method:
EPA
3010A
Thallium
ND
ug/L
0.10
0.060
1
12/24/19 02:04
12/30/19 18:27
7440-28-0
8260D MSV Low Level Landfill
Analytical Method: EPA 8260D
Acetone
ND
ug/L
25.0
6.2
1
12/24/19 01:12
67-64-1
Acrylonitrile
ND
ug/L
10.0
0.90
1
12/24/19 01:12
107-13-1
Benzene
ND
ug/L
1.0
0.15
1
12/24/19 01:12
71-43-2
Bromochloromethane
ND
ug/L
1.0
0.34
1
12/24/19 01:12
74-97-5
Bromodichloromethane
ND
ug/L
1.0
0.26
1
12/24/19 01:12
75-27-4
Bromoform
ND
ug/L
1.0
0.62
1
12/24/19 01:12
75-25-2
Bromomethane
ND
ug/L
2.0
0.62
1
12/24/19 01:12
74-83-9
v2
2-Butanone (MEK)
ND
ug/L
5.0
3.3
1
12/24/19 01:12
78-93-3
Carbon disulfide
ND
ug/L
2.0
0.40
1
12/24/19 01:12
75-15-0
Carbon tetrachloride
ND
ug/L
1.0
0.22
1
12/24/19 01:12
56-23-5
Chlorobenzene
ND
ug/L
1.0
0.23
1
12/24/19 01:12
108-90-7
Chloroethane
ND
ug/L
1.0
0.49
1
12/24/19 01:12
75-00-3
v2
Chloroform
ND
ug/L
5.0
2.3
1
12/24/19 01:12
67-66-3
Chloromethane
ND
ug/L
1.0
0.39
1
12/24/19 01:12
74-87-3
v2
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
0.26
1
12/24/19 01:12
96-12-8
Dibromochloromethane
ND
ug/L
1.0
0.41
1
12/24/19 01:12
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
0.26
1
12/24/19 01:12
106-93-4
Dibromomethane
ND
ug/L
1.0
0.46
1
12/24/19 01:12
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
0.29
1
12/24/19 01:12
95-50-1
1,4-Dichlorobenzene
ND
ug/L
1.0
0.26
1
12/24/19 01:12
106-46-7
trans-1,4-Dichloro-2-butene
ND
ug/L
1.0
0.54
1
12/24/19 01:12
110-57-6
1,1-Dichloroethane
ND
ug/L
1.0
0.27
1
12/24/19 01:12
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
0.34
1
12/24/19 01:12
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
0.24
1
12/24/19 01:12
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
0.29
1
12/24/19 01:12
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
0.25
1
12/24/19 01:12
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
0.19
1
12/24/19 01:12
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/07/2020 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 38
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92457589
Sample: SW-3
Lab ID:
92457589003
Collected:
12/13/19 15:08
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/24/19 01:12
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/24/19 01:12
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/24/19 01:12
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/24/19 01:12
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/24/19 01:12
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/24/19 01:12
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/24/19 01:12
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/24/19 01:12
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/24/19 01:12
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/24/19 01:12
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/24/19 01:12
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/24/19 01:12
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/24/19 01:12
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/24/19 01:12
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/24/19 01:12
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/24/19 01:12
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/24/19 01:12
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/24/19 01:12
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/24/19 01:12
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
12/24/19 01:12
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/24/19 01:12
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
12/24/19 01:12
460-00-4
1,2-Dichloroethane-d4 (S)
100
%
70-130
1
12/24/19 01:12
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
12/24/19 01:12
2037-26-5
Date: 02/07/2020 11:46 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 38
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92457589
Sample: SW-4 Lab ID: 92457589004 Collected: 12/13/19 13:30 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 02/07/2020 11:46 AM
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
ND
ug/L
5.0
3.0
1
12/24/19 01:21
12/24/19 23:03
7440-36-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:03
7440-38-2
27.2
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:03
7440-39-3
0.41J
ug/L
1.0
0.20
1
12/24/19 01:21
12/24/19 23:03
7440-41-7
ND
ug/L
1.0
0.40
1
12/24/19 01:21
12/24/19 23:03
7440-43-9
ND
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:03
7440-47-3
1.2J
ug/L
5.0
1.1
1
12/24/19 01:21
12/24/19 23:03
7440-48-4
ND
ug/L
5.0
2.1
1
12/24/19 01:21
12/24/19 23:03
7440-50-8
ND
ug/L
5.0
1.6
1
12/24/19 01:21
12/24/19 23:03
7439-92-1
1.1J
ug/L
5.0
0.90
1
12/24/19 01:21
12/24/19 23:03
7440-02-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:03
7782-49-2
ND
ug/L
5.0
2.5
1
12/24/19 01:21
12/24/19 23:03
7440-22-4
2.OJ
ug/L
5.0
1.3
1
12/24/19 01:21
12/24/19 23:03
7440-62-2
8.3J
ug/L
10.0
3.9
1
12/24/19 01:21
12/24/19 23:03
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 0.10 0.060 1 12/24/19 02:04 12/30/19 18:58 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
12/24/19 01:30
67-64-1
ND
ug/L
10.0
0.90
1
12/24/19 01:30
107-13-1
ND
ug/L
1.0
0.15
1
12/24/19 01:30
71-43-2
ND
ug/L
1.0
0.34
1
12/24/19 01:30
74-97-5
ND
ug/L
1.0
0.26
1
12/24/19 01:30
75-27-4
ND
ug/L
1.0
0.62
1
12/24/19 01:30
75-25-2
ND
ug/L
2.0
0.62
1
12/24/19 01:30
74-83-9
ND
ug/L
5.0
3.3
1
12/24/19 01:30
78-93-3
ND
ug/L
2.0
0.40
1
12/24/19 01:30
75-15-0
ND
ug/L
1.0
0.22
1
12/24/19 01:30
56-23-5
ND
ug/L
1.0
0.23
1
12/24/19 01:30
108-90-7
ND
ug/L
1.0
0.49
1
12/24/19 01:30
75-00-3
ND
ug/L
5.0
2.3
1
12/24/19 01:30
67-66-3
ND
ug/L
1.0
0.39
1
12/24/19 01:30
74-87-3
ND
ug/L
5.0
0.26
1
12/24/19 01:30
96-12-8
ND
ug/L
1.0
0.41
1
12/24/19 01:30
124-48-1
ND
ug/L
1.0
0.26
1
12/24/19 01:30
106-93-4
ND
ug/L
1.0
0.46
1
12/24/19 01:30
74-95-3
ND
ug/L
1.0
0.29
1
12/24/19 01:30
95-50-1
ND
ug/L
1.0
0.26
1
12/24/19 01:30
106-46-7
ND
ug/L
1.0
0.54
1
12/24/19 01:30
110-57-6
ND
ug/L
1.0
0.27
1
12/24/19 01:30
75-34-3
ND
ug/L
1.0
0.34
1
12/24/19 01:30
107-06-2
ND
ug/L
1.0
0.24
1
12/24/19 01:30
75-35-4
ND
ug/L
1.0
0.29
1
12/24/19 01:30
156-59-2
ND
ug/L
1.0
0.25
1
12/24/19 01:30
156-60-5
ND
ug/L
1.0
0.19
1
12/24/19 01:30
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
B
v2
v2
v2
Page 11 of 38
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92457589
Sample: SW-4
Lab ID:
92457589004
Collected:
12/13/19 13:30
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/24/19 01:30
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/24/19 01:30
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/24/19 01:30
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/24/19 01:30
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/24/19 01:30
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/24/19 01:30
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/24/19 01:30
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/24/19 01:30
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/24/19 01:30
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/24/19 01:30
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/24/19 01:30
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/24/19 01:30
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/24/19 01:30
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/24/19 01:30
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/24/19 01:30
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/24/19 01:30
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/24/19 01:30
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/24/19 01:30
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/24/19 01:30
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
12/24/19 01:30
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/24/19 01:30
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
102
%
70-130
1
12/24/19 01:30
460-00-4
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
12/24/19 01:30
17060-07-0
Toluene-d8 (S)
101
%
70-130
1
12/24/19 01:30
2037-26-5
Date: 02/07/2020 11:46 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 38
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92457589
Sample: SWN-2 Lab ID: 92457589006 Collected: 12/12/19 16:55 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 02/07/2020 11:46 AM
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
ND
ug/L
5.0
3.0
1
12/24/19 01:21
12/24/19 23:09
7440-36-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:09
7440-38-2
17.2
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:09
7440-39-3
ND
ug/L
1.0
0.20
1
12/24/19 01:21
12/24/19 23:09
7440-41-7
ND
ug/L
1.0
0.40
1
12/24/19 01:21
12/24/19 23:09
7440-43-9
ND
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:09
7440-47-3
1.5J
ug/L
5.0
1.1
1
12/24/19 01:21
12/24/19 23:09
7440-48-4
ND
ug/L
5.0
2.1
1
12/24/19 01:21
12/24/19 23:09
7440-50-8
ND
ug/L
5.0
1.6
1
12/24/19 01:21
12/24/19 23:09
7439-92-1
ND
ug/L
5.0
0.90
1
12/24/19 01:21
12/24/19 23:09
7440-02-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:09
7782-49-2
ND
ug/L
5.0
2.5
1
12/24/19 01:21
12/24/19 23:09
7440-22-4
ND
ug/L
5.0
1.3
1
12/24/19 01:21
12/24/19 23:09
7440-62-2
ND
ug/L
10.0
3.9
1
12/24/19 01:21
12/24/19 23:09
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 0.10 0.060 1 12/24/19 02:04 12/30/19 19:10 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
12/23/1918:39
67-64-1
ND
ug/L
10.0
0.90
1
12/23/1918:39
107-13-1
ND
ug/L
1.0
0.15
1
12/23/1918:39
71-43-2
ND
ug/L
1.0
0.34
1
12/23/1918:39
74-97-5
ND
ug/L
1.0
0.26
1
12/23/1918:39
75-27-4
ND
ug/L
1.0
0.62
1
12/23/1918:39
75-25-2
ND
ug/L
2.0
0.62
1
12/23/1918:39
74-83-9
ND
ug/L
5.0
3.3
1
12/23/1918:39
78-93-3
ND
ug/L
2.0
0.40
1
12/23/1918:39
75-15-0
ND
ug/L
1.0
0.22
1
12/23/1918:39
56-23-5
ND
ug/L
1.0
0.23
1
12/23/1918:39
108-90-7
ND
ug/L
1.0
0.49
1
12/23/1918:39
75-00-3
ND
ug/L
5.0
2.3
1
12/23/1918:39
67-66-3
ND
ug/L
1.0
0.39
1
12/23/1918:39
74-87-3
ND
ug/L
5.0
0.26
1
12/23/1918:39
96-12-8
ND
ug/L
1.0
0.41
1
12/23/1918:39
124-48-1
ND
ug/L
1.0
0.26
1
12/23/1918:39
106-93-4
ND
ug/L
1.0
0.46
1
12/23/1918:39
74-95-3
ND
ug/L
1.0
0.29
1
12/23/1918:39
95-50-1
ND
ug/L
1.0
0.26
1
12/23/1918:39
106-46-7
ND
ug/L
1.0
0.54
1
12/23/1918:39
110-57-6
ND
ug/L
1.0
0.27
1
12/23/1918:39
75-34-3
ND
ug/L
1.0
0.34
1
12/23/1918:39
107-06-2
ND
ug/L
1.0
0.24
1
12/23/1918:39
75-35-4
ND
ug/L
1.0
0.29
1
12/23/1918:39
156-59-2
ND
ug/L
1.0
0.25
1
12/23/1918:39
156-60-5
ND
ug/L
1.0
0.19
1
12/23/1918:39
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 38
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92457589
Sample: SWN-2
Lab ID:
92457589006
Collected:
12/12/19 16:55
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/23/19 18:39
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/23/19 18:39
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/23/19 18:39
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/23/19 18:39
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/23/19 18:39
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/23/19 18:39
74-88-4
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/23/19 18:39
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/23/19 18:39
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/23/19 18:39
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/23/19 18:39
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/23/19 18:39
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/23/19 18:39
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/23/19 18:39
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/23/19 18:39
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/23/19 18:39
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/23/19 18:39
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/23/19 18:39
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/23/19 18:39
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/23/19 18:39
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
12/23/19 18:39
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/23/19 18:39
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
104
%
70-130
1
12/23/19 18:39
460-00-4
1,2-Dichloroethane-d4 (S)
100
%
70-130
1
12/23/19 18:39
17060-07-0
Toluene-d8 (S)
108
%
70-130
1
12/23/19 18:39
2037-26-5
Date: 02/07/2020 11:46 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 14 of 38
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92457589
Sample: SW-C Lab ID: 92457589007 Collected: 12/13/19 13:45 Received: 12/16/19 08:30 Matrix: Water
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
6010 MET ICP
Antimony
Arsenic
Barium
Beryllium
Cadmium
Chromium
Cobalt
Copper
Lead
Nickel
Selenium
Silver
Vanadium
Zinc
6020 MET ICPMS
Thallium
8260D MSV Low Level Landfill
Acetone
Acrylonitrile
Benzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
1,2-Dibromo-3-chloropropane
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
Date: 02/07/2020 11:46 AM
Analytical Method: EPA 6010D Preparation Method: EPA 3010A
ND
ug/L
5.0
3.0
1
12/24/19 01:21
12/24/19 23:12
7440-36-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:12
7440-38-2
26.0
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:12
7440-39-3
0.45J
ug/L
1.0
0.20
1
12/24/19 01:21
12/24/19 23:12
7440-41-7
ND
ug/L
1.0
0.40
1
12/24/19 01:21
12/24/19 23:12
7440-43-9
ND
ug/L
5.0
1.0
1
12/24/19 01:21
12/24/19 23:12
7440-47-3
ND
ug/L
5.0
1.1
1
12/24/19 01:21
12/24/19 23:12
7440-48-4
ND
ug/L
5.0
2.1
1
12/24/19 01:21
12/24/19 23:12
7440-50-8
ND
ug/L
5.0
1.6
1
12/24/19 01:21
12/24/19 23:12
7439-92-1
ND
ug/L
5.0
0.90
1
12/24/19 01:21
12/24/19 23:12
7440-02-0
ND
ug/L
10.0
4.7
1
12/24/19 01:21
12/24/19 23:12
7782-49-2
ND
ug/L
5.0
2.5
1
12/24/19 01:21
12/24/19 23:12
7440-22-4
2.5J
ug/L
5.0
1.3
1
12/24/19 01:21
12/24/19 23:12
7440-62-2
7.5J
ug/L
10.0
3.9
1
12/24/19 01:21
12/24/19 23:12
7440-66-6
Analytical Method: EPA 6020E Preparation Method: EPA 3010A
ND ug/L 0.10 0.060 1 12/24/19 02:04 12/30/19 19:14 7440-28-0
Analytical Method: EPA 8260D
ND
ug/L
25.0
6.2
1
12/24/19 02:05
67-64-1
ND
ug/L
10.0
0.90
1
12/24/19 02:05
107-13-1
ND
ug/L
1.0
0.15
1
12/24/19 02:05
71-43-2
ND
ug/L
1.0
0.34
1
12/24/19 02:05
74-97-5
ND
ug/L
1.0
0.26
1
12/24/19 02:05
75-27-4
ND
ug/L
1.0
0.62
1
12/24/19 02:05
75-25-2
ND
ug/L
2.0
0.62
1
12/24/19 02:05
74-83-9
ND
ug/L
5.0
3.3
1
12/24/19 02:05
78-93-3
ND
ug/L
2.0
0.40
1
12/24/19 02:05
75-15-0
ND
ug/L
1.0
0.22
1
12/24/19 02:05
56-23-5
ND
ug/L
1.0
0.23
1
12/24/19 02:05
108-90-7
ND
ug/L
1.0
0.49
1
12/24/19 02:05
75-00-3
ND
ug/L
5.0
2.3
1
12/24/19 02:05
67-66-3
ND
ug/L
1.0
0.39
1
12/24/19 02:05
74-87-3
ND
ug/L
5.0
0.26
1
12/24/19 02:05
96-12-8
ND
ug/L
1.0
0.41
1
12/24/19 02:05
124-48-1
ND
ug/L
1.0
0.26
1
12/24/19 02:05
106-93-4
ND
ug/L
1.0
0.46
1
12/24/19 02:05
74-95-3
ND
ug/L
1.0
0.29
1
12/24/19 02:05
95-50-1
ND
ug/L
1.0
0.26
1
12/24/19 02:05
106-46-7
ND
ug/L
1.0
0.54
1
12/24/19 02:05
110-57-6
ND
ug/L
1.0
0.27
1
12/24/19 02:05
75-34-3
ND
ug/L
1.0
0.34
1
12/24/19 02:05
107-06-2
ND
ug/L
1.0
0.24
1
12/24/19 02:05
75-35-4
ND
ug/L
1.0
0.29
1
12/24/19 02:05
156-59-2
ND
ug/L
1.0
0.25
1
12/24/19 02:05
156-60-5
ND
ug/L
1.0
0.19
1
12/24/19 02:05
78-87-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
B
v2
v2
v2
Page 15 of 38
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: Surry MSWLF SWs
Pace Project No.: 92457589
Sample: SW-C
Lab ID:
92457589007
Collected:
12/13/19 13:45
Received: 12/16/19 08:30 Matrix: Water
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared Analyzed
CAS No. Qual
8260D MSV Low Level Landfill
Analytical
Method: EPA 8260D
cis-1,3-Dichloropropene
ND
ug/L
1.0
0.30
1
12/24/19 02:05
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
0.31
1
12/24/19 02:05
10061-02-6
1,4-Dioxane (p-Dioxane)
ND
ug/L
150
56.2
1
12/24/19 02:05
123-91-1
Ethylbenzene
ND
ug/L
1.0
0.26
1
12/24/19 02:05
100-41-4
2-Hexanone
ND
ug/L
5.0
0.57
1
12/24/19 02:05
591-78-6
lodomethane
ND
ug/L
20.0
12.5
1
12/24/19 02:05
74-88-4 v2
Methylene Chloride
ND
ug/L
5.0
3.7
1
12/24/19 02:05
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
5.0
4.5
1
12/24/19 02:05
108-10-1
Styrene
ND
ug/L
1.0
0.27
1
12/24/19 02:05
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
0.34
1
12/24/19 02:05
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
0.22
1
12/24/19 02:05
79-34-5
Tetrachloroethene
ND
ug/L
1.0
0.16
1
12/24/19 02:05
127-18-4
Toluene
ND
ug/L
1.0
0.24
1
12/24/19 02:05
108-88-3
1,1,1-Trichloroethane
ND
ug/L
1.0
0.18
1
12/24/19 02:05
71-55-6
1,1,2-Trichloroethane
ND
ug/L
1.0
0.24
1
12/24/19 02:05
79-00-5
Trichloroethene
ND
ug/L
1.0
0.22
1
12/24/19 02:05
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.31
1
12/24/19 02:05
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
0.35
1
12/24/19 02:05
96-18-4
Vinyl acetate
ND
ug/L
2.0
1.4
1
12/24/19 02:05
108-05-4
Vinyl chloride
ND
ug/L
1.0
0.24
1
12/24/19 02:05
75-01-4
Xylene (Total)
ND
ug/L
1.0
0.63
1
12/24/19 02:05
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
1
12/24/19 02:05
460-00-4
1,2-Dichloroethane-d4 (S)
101
%
70-130
1
12/24/19 02:05
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
12/24/19 02:05
2037-26-5
Date: 02/07/2020 11:46 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 16 of 38
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92457589
QC Batch: 516496 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92457589001
METHOD BLANK: 2767363
Associated Lab Samples: 92457589001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
Antimony
ug/L
ND
5.0
3.0
12/25/19 00:12
Arsenic
ug/L
ND
10.0
4.7
12/25/19 00:12
Barium
ug/L
ND
5.0
1.0
12/25/19 00:12
Beryllium
ug/L
ND
1.0
0.20
12/25/19 00:12
Cadmium
ug/L
ND
1.0
0.40
12/25/19 00:12
Chromium
ug/L
ND
5.0
1.0
12/25/19 00:12
Cobalt
ug/L
ND
5.0
1.1
12/25/19 00:12
Copper
ug/L
ND
5.0
2.1
12/25/19 00:12
Lead
ug/L
ND
5.0
1.6
12/25/19 00:12
Nickel
ug/L
ND
5.0
0.90
12/25/19 00:12
Selenium
ug/L
ND
10.0
4.7
12/25/19 00:12
Silver
ug/L
ND
5.0
2.5
12/25/19 00:12
Vanadium
ug/L
ND
5.0
1.3
12/25/19 00:12
Zinc
ug/L
ND
10.0
3.9
12/25/19 00:12
LABORATORY CONTROL SAMPLE:
Parameter
2767364
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
501
100
80-120
Arsenic
ug/L
500
503
101
80-120
Barium
ug/L
500
498
100
80-120
Beryllium
ug/L
500
497
99
80-120
Cadmium
ug/L
500
498
100
80-120
Chromium
ug/L
500
498
100
80-120
Cobalt
ug/L
500
498
100
80-120
Copper
ug/L
500
504
101
80-120
Lead
ug/L
500
502
100
80-120
Nickel
ug/L
500
498
100
80-120
Selenium
ug/L
500
492
98
80-120
Silver
ug/L
250
250
100
80-120
Vanadium
ug/L
500
495
99
80-120
Zinc
ug/L
500
486
97
80-120
Qualifiers
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2767365 2767366
MS MSD
92457589001 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Antimony ug/L ND 500 500 523 517 105 103 75-125 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/07/2020 11:46 AM without the written consent of Pace Analytical Services, LLC.
Page 17 of 38
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project:
Pace Project No.:
Surry MSWLF SWs
92457589
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
2767365
2767366
MS
MSD
92457589001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Arsenic
ug/L
ND
500
500
530
518
106
103
75-125
2
20
Barium
ug/L
20.7
500
500
532
523
102
101
75-125
2
20
Beryllium
ug/L
0.75J
500
500
510
502
102
100
75-125
2
20
Cadmium
ug/L
0.67J
500
500
524
518
105
104
75-125
1
20
Chromium
ug/L
ND
500
500
518
509
103
102
75-125
2
20
Cobalt
ug/L
ND
500
500
514
508
103
101
75-125
1
20
Copper
ug/L
ND
500
500
515
510
103
102
75-125
1
20
Lead
ug/L
ND
500
500
519
511
104
102
75-125
1
20
Nickel
ug/L
1.01
500
500
514
509
103
102
75-125
1
20
Selenium
ug/L
ND
500
500
540
534
108
107
75-125
1
20
Silver
ug/L
ND
250
250
258
255
103
102
75-125
1
20
Vanadium
ug/L
1.8J
500
500
513
506
102
101
75-125
1
20
Zinc
ug/L
4.3J
500
500
519
512
103
102
75-125
1
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/07/2020 11:46 AM without the written consent of Pace Analytical Services, LLC.
Page 18 of 38
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92457589
QC Batch: 516498 Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92457589002, 92457589003, 92457589004, 92457589006, 92457589007
METHOD BLANK: 2767371
Matrix:
Water
Associated Lab Samples:
92457589002, 92457589003, 92457589004, 92457589006, 92457589007
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed
Antimony
ug/L
ND
5.0
3.0
12/24/19 22:28
Arsenic
ug/L
ND
10.0
4.7
12/24/19 22:28
Barium
ug/L
ND
5.0
1.0
12/24/19 22:28
Beryllium
ug/L
0.25J
1.0
0.20
12/24/19 22:28
Cadmium
ug/L
ND
1.0
0.40
12/24/19 22:28
Chromium
ug/L
ND
5.0
1.0
12/24/19 22:28
Cobalt
ug/L
ND
5.0
1.1
12/24/19 22:28
Copper
ug/L
ND
5.0
2.1
12/24/19 22:28
Lead
ug/L
ND
5.0
1.6
12/24/19 22:28
Nickel
ug/L
ND
5.0
0.90
12/24/19 22:28
Selenium
ug/L
ND
10.0
4.7
12/24/19 22:28
Silver
ug/L
ND
5.0
2.5
12/24/19 22:28
Vanadium
ug/L
ND
5.0
1.3
12/24/19 22:28
Zinc
ug/L
ND
10.0
3.9
12/24/19 22:28
LABORATORY CONTROL SAMPLE:
Parameter
2767372
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Antimony
ug/L
500
502
100
80-120
Arsenic
ug/L
500
503
101
80-120
Barium
ug/L
500
480
96
80-120
Beryllium
ug/L
500
479
96
80-120
Cadmium
ug/L
500
488
98
80-120
Chromium
ug/L
500
483
97
80-120
Cobalt
ug/L
500
491
98
80-120
Copper
ug/L
500
491
98
80-120
Lead
ug/L
500
494
99
80-120
Nickel
ug/L
500
487
97
80-120
Selenium
ug/L
500
487
97
80-120
Silver
ug/L
250
244
97
80-120
Vanadium
ug/L
500
483
97
80-120
Zinc
ug/L
500
481
96
80-120
Qualifiers
Qualifiers
MS MSD
92457589002 Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Antimony ug/L ND 500 500 524 519 105 104 75-125 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/07/2020 11:46 AM without the written consent of Pace Analytical Services, LLC.
Page 19 of 38
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project:
Pace Project No.:
Surry MSWLF SWs
92457589
MATRIX SPIKE &
MATRIX SPIKE DUPLICATE:
2767373
2767374
MS
MSD
92457589002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Arsenic
ug/L
ND
500
500
538
526
107
105
75-125
2
20
Barium
ug/L
18.8
500
500
523
515
101
99
75-125
1
20
Beryllium
ug/L
0.20J
500
500
503
494
101
99
75-125
2
20
Cadmium
ug/L
0.81J
500
500
523
514
104
103
75-125
2
20
Chromium
ug/L
ND
500
500
509
503
102
101
75-125
1
20
Cobalt
ug/L
21.3
500
500
537
528
103
101
75-125
2
20
Copper
ug/L
ND
500
500
515
504
103
101
75-125
2
20
Lead
ug/L
ND
500
500
519
514
104
103
75-125
1
20
Nickel
ug/L
ND
500
500
514
507
103
101
75-125
1
20
Selenium
ug/L
ND
500
500
537
530
107
106
75-125
1
20
Silver
ug/L
ND
250
250
256
254
103
101
75-125
1
20
Vanadium
ug/L
ND
500
500
512
505
102
101
75-125
1
20
Zinc
ug/L
4.8J
500
500
522
515
103
102
75-125
1
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/07/2020 11:46 AM without the written consent of Pace Analytical Services, LLC.
Page 20 of 38
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92457589
QC Batch: 516497
Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A
Analysis Description: 6020 MET
Associated Lab Samples: 92457589001
METHOD BLANK: 2767367
Matrix: Water
Associated Lab Samples: 92457589001
Blank Reporting
Parameter Units
Result Limit MDL
Analyzed Qualifiers
Thallium ug/L
ND 0.10 0.060 12/30/1915:27
LABORATORY CONTROL SAMPLE: 2767368
Spike LCS LCS
% Rec
Parameter Units
Conc. Result % Rec
Limits Qualifiers
Thallium ug/L
10 10.1 101
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2767369 2767370
MS MSD
92458051011
Spike Spike MS MSD
MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result Result
% Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND
10 10 10.5 10.4
105 104 75-125 1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/07/2020 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 21 of 38
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92457589
QC Batch: 516501
Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A
Analysis Description: 6020 MET
Associated Lab Samples: 92457589002, 92457589003,
92457589004, 92457589006, 92457589007
METHOD BLANK: 2767378
Matrix: Water
Associated Lab Samples: 92457589002, 92457589003,
92457589004, 92457589006, 92457589007
Blank Reporting
Parameter Units
Result Limit MDL Analyzed Qualifiers
Thallium ug/L
ND 0.10 0.060 12/30/1915:28
LABORATORY CONTROL SAMPLE: 2767379
Spike LCS LCS % Rec
Parameter Units
Conc. Result % Rec Limits Qualifiers
Thallium ug/L
10 9.9 99 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2767380 2767381
MS MSD
92457589003
Spike Spike MS MSD MS MSD % Rec Max
Parameter Units Result
Conc. Conc. Result Result % Rec % Rec Limits RPD RPD Qual
Thallium ug/L ND
10 10 11.0 10.8 110 108 75-125 2 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/07/2020 11:46 AM without the written consent of Pace Analytical Services, LLC.
Page 22 of 38
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92457589
QC Batch: 516391 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Associated Lab Samples: 92457589001, 92457589006
METHOD BLANK: 2766744
Associated Lab Samples: 92457589001, 92457589006
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.34
12/23/19 12:07
1,1,1-Trichloroethane
ug/L
ND
1.0
0.18
12/23/19 12:07
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
12/23/19 12:07
1,1,2-Trichloroethane
ug/L
ND
1.0
0.24
12/23/19 12:07
1,1-Dichloroethane
ug/L
ND
1.0
0.27
12/23/19 12:07
1,1-Dichloroethene
ug/L
ND
1.0
0.24
12/23/19 12:07
1,2,3-Trichloropropane
ug/L
ND
1.0
0.35
12/23/19 12:07
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
0.26
12/23/19 12:07
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.26
12/23/19 12:07
1,2-Dichlorobenzene
ug/L
ND
1.0
0.29
12/23/19 12:07
1,2-Dichloroethane
ug/L
ND
1.0
0.34
12/23/19 12:07
1,2-Dichloropropane
ug/L
ND
1.0
0.19
12/23/19 12:07
1,4-Dichlorobenzene
ug/L
ND
1.0
0.26
12/23/19 12:07
1,4-Dioxane (p-Dioxane)
ug/L
ND
150
56.2
12/23/19 12:07
2-Butanone (MEK)
ug/L
ND
5.0
3.3
12/23/19 12:07
2-Hexanone
ug/L
ND
5.0
0.57
12/23/19 12:07
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
4.5
12/23/19 12:07
Acetone
ug/L
ND
25.0
6.2
12/23/19 12:07
Acrylonitrile
ug/L
ND
10.0
0.90
12/23/19 12:07
Benzene
ug/L
ND
1.0
0.15
12/23/19 12:07
Bromochloromethane
ug/L
ND
1.0
0.34
12/23/19 12:07
Bromodichloromethane
ug/L
ND
1.0
0.26
12/23/19 12:07
Bromoform
ug/L
ND
1.0
0.62
12/23/19 12:07
Bromomethane
ug/L
ND
2.0
0.62
12/23/19 12:07
Carbon disulfide
ug/L
ND
2.0
0.40
12/23/19 12:07
Carbon tetrachloride
ug/L
ND
1.0
0.22
12/23/19 12:07
Chlorobenzene
ug/L
ND
1.0
0.23
12/23/19 12:07
Chloroethane
ug/L
ND
1.0
0.49
12/23/19 12:07
Chloroform
ug/L
ND
5.0
2.3
12/23/19 12:07
Chloromethane
ug/L
ND
1.0
0.39
12/23/19 12:07
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.29
12/23/19 12:07
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.30
12/23/19 12:07
Dibromochloromethane
ug/L
ND
1.0
0.41
12/23/19 12:07
Dibromomethane
ug/L
ND
1.0
0.46
12/23/19 12:07
Ethylbenzene
ug/L
ND
1.0
0.26
12/23/19 12:07
lodomethane
ug/L
ND
20.0
12.5
12/23/19 12:07
Methylene Chloride
ug/L
ND
5.0
3.7
12/23/19 12:07
Styrene
ug/L
ND
1.0
0.27
12/23/19 12:07
Tetrachloroethene
ug/L
ND
1.0
0.16
12/23/19 12:07
Toluene
ug/L
ND
1.0
0.24
12/23/19 12:07
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.25
12/23/19 12:07
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/07/2020 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 23 of 38
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92457589
METHOD BLANK: 2766744
Associated Lab Samples: 92457589001, 92457589006
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
MDL
Analyzed
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.31
12/23/19 12:07
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.54
12/23/19 12:07
Trichloroethene
ug/L
ND
1.0
0.22
12/23/19 12:07
Trichlorofluoromethane
ug/L
ND
1.0
0.31
12/23/19 12:07
Vinyl acetate
ug/L
ND
2.0
1.4
12/23/19 12:07
Vinyl chloride
ug/L
ND
1.0
0.24
12/23/19 12:07
Xylene (Total)
ug/L
ND
1.0
0.63
12/23/19 12:07
1,2-Dichloroethane-d4 (S)
%
98
70-130
12/23/19 12:07
4-Bromofluorobenzene (S)
%
102
70-130
12/23/19 12:07
Toluene-d8 (S)
%
101
70-130
12/23/19 12:07
LABORATORY CONTROL SAMPLE:
Parameter
2766745
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
51.1
102
70-130
1,1,1-Trichloroethane
ug/L
50
45.2
90
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
49.7
99
70-130
1,1,2-Trichloroethane
ug/L
50
48.3
97
70-130
1,1-Dichloroethane
ug/L
50
47.1
94
70-130
1,1-Dichloroethene
ug/L
50
47.0
94
70-130
1,2,3-Trichloropropane
ug/L
50
50.1
100
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
49.4
99
70-130
1,2-Dibromoethane (EDB)
ug/L
50
51.5
103
70-130
1,2-Dichlorobenzene
ug/L
50
53.3
107
70-130
1,2-Dichloroethane
ug/L
50
45.5
91
70-130
1,2-Dichloropropane
ug/L
50
50.3
101
70-130
1,4-Dichlorobenzene
ug/L
50
53.1
106
70-130
1,4-Dioxane(p-Dioxane)
ug/L
1000
1010
101
59-169
2-Butanone (MEK)
ug/L
100
99.7
100
64-135
2-Hexanone
ug/L
100
96.3
96
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
94.5
95
70-130
Acetone
ug/L
100
107
107
61-157
Acrylonitrile
ug/L
250
235
94
61-143
Benzene
ug/L
50
48.3
97
70-130
Bromochloromethane
ug/L
50
45.4
91
70-130
Bromodichloromethane
ug/L
50
45.9
92
70-130
Bromoform
ug/L
50
46.2
92
70-130
Bromomethane
ug/L
50
35.9
72
38-130
Carbon disulfide
ug/L
50
49.9
100
68-130
Carbon tetrachloride
ug/L
50
45.0
90
70-130
Chlorobenzene
ug/L
50
51.9
104
70-130
Chloroethane
ug/L
50
36.2
72
37-142
Chloroform
ug/L
50
46.1
92
70-130
Chloromethane
ug/L
50
40.4
81
48-130
Qualifiers
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/07/2020 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 24 of 38
Pace Analytical Services, LLC
9800
lCtaac,Analyfical ® Kiney Ave. Suite 100
Huntersville, NC 28078
0788
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92457589
LABORATORY CONTROL SAMPLE:
Parameter
2766745
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
cis-1,2-Dichloroethene
ug/L
50
46.6
93
70-130
cis-1,3-Dichloropropene
ug/L
50
51.7
103
70-130
Dibromochloromethane
ug/L
50
48.6
97
70-130
Dibromomethane
ug/L
50
48.8
98
70-130
Ethylbenzene
ug/L
50
48.8
98
70-130
lodomethane
ug/L
100
73.6
74
40-130
Methylene Chloride
ug/L
50
45.0
90
67-132
Styrene
ug/L
50
51.3
103
70-130
Tetrachloroethene
ug/L
50
49.7
99
69-130
Toluene
ug/L
50
45.1
90
70-130
trans-1,2-Dichloroethene
ug/L
50
47.7
95
70-130
trans- 1,3-Dichloropropene
ug/L
50
49.9
100
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
52.2
104
35-189
Trichloroethene
ug/L
50
49.7
99
70-130
Trichlorofluoromethane
ug/L
50
44.9
90
63-130
Vinyl acetate
ug/L
100
107
107
55-143
Vinyl chloride
ug/L
50
50.6
101
70-131
Xylene (Total)
ug/L
150
144
96
70-130
1,2-Dichloroethane-d4 (S)
%
85
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
98
70-130
MATRIX SPIKE SAMPLE:
Parameter
2766746
Units
92457589001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20.0
100
73-134
1,1,1-Trichloroethane
ug/L
ND
20
19.2
96
82-143
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20.0
100
70-136
1,1,2-Trichloroethane
ug/L
ND
20
19.9
100
70-135
1,1-Dichloroethane
ug/L
ND
20
20.1
101
70-139
1,1-Dichloroethene
ug/L
ND
20
20.3
101
70-154
1,2,3-Trichloropropane
ug/L
ND
20
20.4
102
71-137
1,2-Dibromo-3-chloropropane
ug/L
ND
20
17.1
86
65-134
1,2-Dibromoethane (EDB)
ug/L
ND
20
20.7
103
70-137
1,2-Dichlorobenzene
ug/L
ND
20
20.9
104
70-133
1,2-Dichloroethane
ug/L
ND
20
19.2
96
70-137
1,2-Dichloropropane
ug/L
ND
20
20.8
104
70-140
1,4-Dichlorobenzene
ug/L
ND
20
20.9
105
70-133
1,4-Dioxane (p-Dioxane)
ug/L
ND
400
393
98
53-168
2-Butanone (MEK)
ug/L
ND
40
38.7
97
60-139
2-Hexanone
ug/L
ND
40
35.5
89
65-138
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
35.7
89
65-135
Acetone
ug/L
ND
40
37.2
93
60-148
Acrylonitrile
ug/L
ND
100
96.4
96
64-147
Benzene
ug/L
ND
20
20.3
102
70-151
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/07/2020 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 25 of 38
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92457589
MATRIX SPIKE SAMPLE: 2766746
92457589001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Bromochloromethane
ug/L
ND
20
19.6
98
70-141
Bromodichloromethane
ug/L
ND
20
18.6
93
70-138
Bromoform
ug/L
ND
20
16.4
82
63-130
Bromomethane
ug/L
ND
20
19.2
96
15-152
Carbon disulfide
ug/L
ND
20
20.9
105
69-149
Carbon tetrachloride
ug/L
ND
20
19.5
97
70-143
Chlorobenzene
ug/L
ND
20
21.6
108
70-138
Chloroethane
ug/L
ND
20
19.9
100
52-163
Chloroform
ug/L
ND
20
20.0
100
70-139
Chloromethane
ug/L
ND
20
17.0
85
41-139
cis-1,2-Dichloroethene
ug/L
ND
20
19.6
98
70-141
cis-1,3-Dichloropropene
ug/L
ND
20
20.3
101
70-137
Dibromochloromethane
ug/L
ND
20
18.2
91
70-134
Dibromomethane
ug/L
ND
20
19.9
99
70-138
Ethylbenzene
ug/L
ND
20
20.6
103
66-153
lodomethane
ug/L
ND
40
20.5
51
20-138
Methylene Chloride
ug/L
ND
20
20.2
101
42-159
Styrene
ug/L
ND
20
21.0
105
70-135
Tetrachloroethene
ug/L
ND
20
20.5
102
59-143
Toluene
ug/L
ND
20
18.9
95
59-148
trans-1,2-Dichloroethene
ug/L
ND
20
20.7
103
70-146
trans- 1,3-Dichloropropene
ug/L
ND
20
19.4
97
70-135
trans-1,4-Dichloro-2-butene
ug/L
ND
20
19.8
99
47-135
Trichloroethene
ug/L
ND
20
21.2
106
70-147
Trichlorofluoromethane
ug/L
ND
20
20.4
102
70-148
Vinyl acetate
ug/L
ND
40
40.8
102
49-151
Vinyl chloride
ug/L
ND
20
21.9
109
70-156
Xylene (Total)
ug/L
ND
60
60.3
100
63-158
1,2-Dichloroethane-d4 (S)
%
90
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
97
70-130
SAMPLE DUPLICATE: 2766747
Parameter
Units
92457589006
Result
Dup
Result RPD
Max
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,1-Trichloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
ND
ND
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,2,3-Trichloropropane
ug/L
ND
ND
30
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
30
1,2-Dibromoethane (EDB)
ug/L
ND
ND
30
1,2-Dichlorobenzene
ug/L
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/07/2020 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 26 of 38
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92457589
SAMPLE DUPLICATE: 2766747
Parameter
Units
92457589006
Result
Dup
Result RPD
Max
RPD
1,2-Dichloroethane
ug/L
ND
ND
30
1,2-Dichloropropane
ug/L
ND
ND
30
1,4-Dichlorobenzene
ug/L
ND
ND
30
1,4-Dioxane (p-Dioxane)
ug/L
ND
ND
30
2-Butanone (MEK)
ug/L
ND
ND
30
2-Hexanone
ug/L
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
30
Acetone
ug/L
ND
ND
30
Acrylonitrile
ug/L
ND
ND
30
Benzene
ug/L
ND
ND
30
Bromochloromethane
ug/L
ND
ND
30
Bromodichloromethane
ug/L
ND
ND
30
Bromoform
ug/L
ND
ND
30
Bromomethane
ug/L
ND
ND
30
Carbon disulfide
ug/L
ND
ND
30
Carbon tetrachloride
ug/L
ND
ND
30
Chlorobenzene
ug/L
ND
ND
30
Chloroethane
ug/L
ND
ND
30
Chloroform
ug/L
ND
ND
30
Chloromethane
ug/L
ND
ND
30
cis-1,2-Dichloroethene
ug/L
ND
ND
30
cis-1,3-Dichloropropene
ug/L
ND
ND
30
Dibromochloromethane
ug/L
ND
ND
30
Dibromomethane
ug/L
ND
ND
30
Ethylbenzene
ug/L
ND
ND
30
lodomethane
ug/L
ND
ND
30
Methylene Chloride
ug/L
ND
ND
30
Styrene
ug/L
ND
ND
30
Tetrachloroethene
ug/L
ND
ND
30
Toluene
ug/L
ND
ND
30
trans-1,2-Dichloroethene
ug/L
ND
ND
30
trans- 1,3-Dichloropropene
ug/L
ND
ND
30
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
30
Trichloroethene
ug/L
ND
ND
30
Trichlorofluoromethane
ug/L
ND
ND
30
Vinyl acetate
ug/L
ND
ND
30
Vinyl chloride
ug/L
ND
ND
30
Xylene (Total)
ug/L
ND
ND
30
1,2-Dichloroethane-d4 (S)
%
100
95
4-Bromofluorobenzene (S)
%
104
99
Toluene-d8 (S)
%
108
101
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/07/2020 11:46 AM without the written consent of Pace Analytical Services, LLC.
Page 27 of 38
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92457589
QC Batch: 516422 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Landfill
Associated Lab Samples: 92457589002, 92457589003, 92457589004, 92457589007
METHOD BLANK: 2766873 Matrix: Water
Associated Lab Samples: 92457589002, 92457589003, 92457589004, 92457589007
Blank Reporting
Parameter Units Result Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
0.34
12/24/19 00:18
1,1,1-Trichloroethane
ug/L
ND
1.0
0.18
12/24/19 00:18
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
0.22
12/24/19 00:18
1,1,2-Trichloroethane
ug/L
ND
1.0
0.24
12/24/19 00:18
1,1-Dichloroethane
ug/L
ND
1.0
0.27
12/24/19 00:18
1,1-Dichloroethene
ug/L
ND
1.0
0.24
12/24/19 00:18
1,2,3-Trichloropropane
ug/L
ND
1.0
0.35
12/24/19 00:18
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
0.26
12/24/19 00:18
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
0.26
12/24/19 00:18
1,2-Dichlorobenzene
ug/L
ND
1.0
0.29
12/24/19 00:18
1,2-Dichloroethane
ug/L
ND
1.0
0.34
12/24/19 00:18
1,2-Dichloropropane
ug/L
ND
1.0
0.19
12/24/19 00:18
1,4-Dichlorobenzene
ug/L
ND
1.0
0.26
12/24/19 00:18
1,4-Dioxane (p-Dioxane)
ug/L
ND
150
56.2
12/24/19 00:18
2-Butanone (MEK)
ug/L
ND
5.0
3.3
12/24/19 00:18
2-Hexanone
ug/L
ND
5.0
0.57
12/24/19 00:18
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
4.5
12/24/19 00:18
Acetone
ug/L
ND
25.0
6.2
12/24/19 00:18
Acrylonitrile
ug/L
ND
10.0
0.90
12/24/19 00:18
Benzene
ug/L
ND
1.0
0.15
12/24/19 00:18
Bromochloromethane
ug/L
ND
1.0
0.34
12/24/19 00:18
Bromodichloromethane
ug/L
ND
1.0
0.26
12/24/19 00:18
Bromoform
ug/L
ND
1.0
0.62
12/24/19 00:18
Bromomethane
ug/L
ND
2.0
0.62
12/24/19 00:18
Carbon disulfide
ug/L
ND
2.0
0.40
12/24/19 00:18
Carbon tetrachloride
ug/L
ND
1.0
0.22
12/24/19 00:18
Chlorobenzene
ug/L
ND
1.0
0.23
12/24/19 00:18
Chloroethane
ug/L
ND
1.0
0.49
12/24/19 00:18
Chloroform
ug/L
ND
5.0
2.3
12/24/19 00:18
Chloromethane
ug/L
ND
1.0
0.39
12/24/19 00:18
cis-1,2-Dichloroethene
ug/L
ND
1.0
0.29
12/24/19 00:18
cis-1,3-Dichloropropene
ug/L
ND
1.0
0.30
12/24/19 00:18
Dibromochloromethane
ug/L
ND
1.0
0.41
12/24/19 00:18
Dibromomethane
ug/L
ND
1.0
0.46
12/24/19 00:18
Ethylbenzene
ug/L
ND
1.0
0.26
12/24/19 00:18
lodomethane
ug/L
ND
20.0
12.5
12/24/19 00:18
Methylene Chloride
ug/L
ND
5.0
3.7
12/24/19 00:18
Styrene
ug/L
ND
1.0
0.27
12/24/19 00:18
Tetrachloroethene
ug/L
ND
1.0
0.16
12/24/19 00:18
Toluene
ug/L
ND
1.0
0.24
12/24/19 00:18
trans-1,2-Dichloroethene
ug/L
ND
1.0
0.25
12/24/19 00:18
v2
v2
v2
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/07/2020 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 28 of 38
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92457589
METHOD BLANK: 2766873 Matrix: Water
Associated Lab Samples: 92457589002, 92457589003, 92457589004, 92457589007
Blank Reporting
Parameter Units Result Limit
MDL
Analyzed Qualifiers
trans- 1,3-Dichloropropene
ug/L
ND
1.0
0.31
12/24/19 00:18
trans-1,4-Dichloro-2-butene
ug/L
ND
1.0
0.54
12/24/19 00:18
Trichloroethene
ug/L
ND
1.0
0.22
12/24/19 00:18
Trichlorofluoromethane
ug/L
ND
1.0
0.31
12/24/19 00:18
Vinyl acetate
ug/L
ND
2.0
1.4
12/24/19 00:18
Vinyl chloride
ug/L
ND
1.0
0.24
12/24/19 00:18
Xylene (Total)
ug/L
ND
1.0
0.63
12/24/19 00:18
1,2-Dichloroethane-d4 (S)
%
97
70-130
12/24/19 00:18
4-Bromofluorobenzene (S)
%
101
70-130
12/24/19 00:18
Toluene-d8 (S)
%
100
70-130
12/24/19 00:18
LABORATORY CONTROL SAMPLE:
Parameter
2766874
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
47.2
94
70-130
1,1,1-Trichloroethane
ug/L
50
41.9
84
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
47.5
95
70-130
1,1,2-Trichloroethane
ug/L
50
45.5
91
70-130
1,1-Dichloroethane
ug/L
50
44.3
89
70-130
1,1-Dichloroethene
ug/L
50
47.0
94
70-130
1,2,3-Trichloropropane
ug/L
50
48.0
96
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
43.8
88
70-130
1,2-Dibromoethane (EDB)
ug/L
50
48.7
97
70-130
1,2-Dichlorobenzene
ug/L
50
48.9
98
70-130
1,2-Dichloroethane
ug/L
50
44.0
88
70-130
1,2-Dichloropropane
ug/L
50
46.2
92
70-130
1,4-Dichlorobenzene
ug/L
50
47.7
95
70-130
1,4-Dioxane (p-Dioxane)
ug/L
1000
943
94
59-169
2-Butanone (MEK)
ug/L
100
90.9
91
64-135
2-Hexanone
ug/L
100
90.5
91
66-135
4-Methyl-2-pentanone (MIBK)
ug/L
100
89.8
90
70-130
Acetone
ug/L
100
94.3
94
61-157
Acrylonitrile
ug/L
250
227
91
61-143
Benzene
ug/L
50
44.6
89
70-130
Bromochloromethane
ug/L
50
42.9
86
70-130
Bromodichloromethane
ug/L
50
42.1
84
70-130
Bromoform
ug/L
50
40.8
82
70-130
Bromomethane
ug/L
50
34.7
69
38-130 v2
Carbon disulfide
ug/L
50
45.5
91
68-130
Carbon tetrachloride
ug/L
50
40.6
81
70-130
Chlorobenzene
ug/L
50
48.0
96
70-130
Chloroethane
ug/L
50
35.4
71
37-142 v2
Chloroform
ug/L
50
43.6
87
70-130
Chloromethane
ug/L
50
36.7
73
48-130 v2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/07/2020 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 29 of 38
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92457589
LABORATORY CONTROL SAMPLE:
Parameter
2766874
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
cis-1,2-Dichloroethene
ug/L
50
43.7
87
70-130
cis-1,3-Dichloropropene
ug/L
50
46.7
93
70-130
Dibromochloromethane
ug/L
50
43.6
87
70-130
Dibromomethane
ug/L
50
45.7
91
70-130
Ethylbenzene
ug/L
50
45.5
91
70-130
lodomethane
ug/L
100
73.1
73
40-130 v2
Methylene Chloride
ug/L
50
42.7
85
67-132
Styrene
ug/L
50
47.6
95
70-130
Tetrachloroethene
ug/L
50
45.7
91
69-130
Toluene
ug/L
50
42.1
84
70-130
trans-1,2-Dichloroethene
ug/L
50
44.7
89
70-130
trans- 1,3-Dichloropropene
ug/L
50
44.8
90
70-130
trans-1,4-Dichloro-2-butene
ug/L
50
44.9
90
35-189
Trichloroethene
ug/L
50
45.9
92
70-130
Trichlorofluoromethane
ug/L
50
41.5
83
63-130
Vinyl acetate
ug/L
100
99.9
100
55-143
Vinyl chloride
ug/L
50
46.5
93
70-131
Xylene (Total)
ug/L
150
135
90
70-130
1,2-Dichloroethane-d4 (S)
%
87
70-130
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
97
70-130
MATRIX SPIKE SAMPLE:
Parameter
2766876
Units
92457589002
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
19.6
98
73-134
1,1,1-Trichloroethane
ug/L
ND
20
18.8
94
82-143
1,1,2,2-Tetrachloroethane
ug/L
ND
20
19.1
96
70-136
1,1,2-Trichloroethane
ug/L
ND
20
19.5
98
70-135
1,1-Dichloroethane
ug/L
ND
20
20.2
101
70-139
1,1-Dichloroethene
ug/L
ND
20
20.1
100
70-154
1,2,3-Trichloropropane
ug/L
ND
20
19.6
98
71-137
1,2-Dibromo-3-chloropropane
ug/L
ND
20
17.3
87
65-134
1,2-Dibromoethane (EDB)
ug/L
ND
20
20.4
102
70-137
1,2-Dichlorobenzene
ug/L
ND
20
20.8
104
70-133
1,2-Dichloroethane
ug/L
ND
20
18.8
94
70-137
1,2-Dichloropropane
ug/L
ND
20
20.9
104
70-140
1,4-Dichlorobenzene
ug/L
ND
20
21.1
106
70-133
1,4-Dioxane (p-Dioxane)
ug/L
ND
400
376
94
53-168
2-Butanone (MEK)
ug/L
ND
40
37.1
93
60-139
2-Hexanone
ug/L
ND
40
33.9
85
65-138
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
34.4
86
65-135
Acetone
ug/L
ND
40
37.8
95
60-148
Acrylonitrile
ug/L
ND
100
94.9
95
64-147
Benzene
ug/L
ND
20
19.8
99
70-151
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/07/2020 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 30 of 38
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92457589
MATRIX SPIKE SAMPLE: 2766876
92457589002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Bromochloromethane
ug/L
ND
20
19.2
96
70-141
Bromodichloromethane
ug/L
ND
20
18.4
92
70-138
Bromoform
ug/L
ND
20
16.3
81
63-130
Bromomethane
ug/L
ND
20
18.9
95
15-152
Carbon disulfide
ug/L
ND
20
20.6
103
69-149
Carbon tetrachloride
ug/L
ND
20
19.3
96
70-143
Chlorobenzene
ug/L
ND
20
21.1
105
70-138
Chloroethane
ug/L
ND
20
20.1
100
52-163
Chloroform
ug/L
ND
20
19.5
98
70-139
Chloromethane
ug/L
ND
20
17.4
87
41-139
cis-1,2-Dichloroethene
ug/L
3.0
20
22.3
96
70-141
cis-1,3-Dichloropropene
ug/L
ND
20
20.2
101
70-137
Dibromochloromethane
ug/L
ND
20
18.3
91
70-134
Dibromomethane
ug/L
ND
20
20.1
101
70-138
Ethylbenzene
ug/L
ND
20
20.1
101
66-153
lodomethane
ug/L
ND
40
28.6
72
20-138
Methylene Chloride
ug/L
ND
20
19.5
97
42-159
Styrene
ug/L
ND
20
20.8
104
70-135
Tetrachloroethene
ug/L
ND
20
20.2
101
59-143
Toluene
ug/L
ND
20
18.8
94
59-148
trans-1,2-Dichloroethene
ug/L
ND
20
20.3
102
70-146
trans- 1,3-Dichloropropene
ug/L
ND
20
19.2
96
70-135
trans-1,4-Dichloro-2-butene
ug/L
ND
20
19.1
96
47-135
Trichloroethene
ug/L
ND
20
21.0
105
70-147
Trichlorofluoromethane
ug/L
ND
20
20.4
102
70-148
Vinyl acetate
ug/L
ND
40
39.3
98
49-151
Vinyl chloride
ug/L
ND
20
22.4
112
70-156
Xylene (Total)
ug/L
ND
60
60.0
100
63-158
1,2-Dichloroethane-d4 (S)
%
88
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
97
70-130
SAMPLE DUPLICATE: 2766875
Parameter
Units
92457587004
Result
Dup
Result RPD
Max
RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,1-Trichloroethane
ug/L
ND
ND
30
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
30
1,1,2-Trichloroethane
ug/L
ND
ND
30
1,1-Dichloroethane
ug/L
ND
ND
30
1,1-Dichloroethene
ug/L
ND
ND
30
1,2,3-Trichloropropane
ug/L
ND
ND
30
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
30
1,2-Dibromoethane (EDB)
ug/L
ND
ND
30
1,2-Dichlorobenzene
ug/L
ND
ND
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/07/2020 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 31 of 38
lV11.1 Analytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Surry MSWLF SWs
Pace Project No.: 92457589
SAMPLE DUPLICATE: 2766875
Parameter
Units
92457587004
Result
Dup
Result RPD
Max
RPD
1,2-Dichloroethane
ug/L
ND
ND
30
1,2-Dichloropropane
ug/L
ND
ND
30
1,4-Dichlorobenzene
ug/L
ND
ND
30
1,4-Dioxane (p-Dioxane)
ug/L
ND
ND
30
2-Butanone (MEK)
ug/L
ND
ND
30
2-Hexanone
ug/L
ND
ND
30
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
30
Acetone
ug/L
ND
ND
30
Acrylonitrile
ug/L
ND
ND
30
Benzene
ug/L
ND
ND
30
Bromochloromethane
ug/L
ND
ND
30
Bromodichloromethane
ug/L
ND
ND
30
Bromoform
ug/L
ND
ND
30
Bromomethane
ug/L
ND
ND
30
Carbon disulfide
ug/L
ND
ND
30
Carbon tetrachloride
ug/L
ND
ND
30
Chlorobenzene
ug/L
ND
ND
30
Chloroethane
ug/L
ND
ND
30
Chloroform
ug/L
ND
ND
30
Chloromethane
ug/L
ND
ND
30
cis-1,2-Dichloroethene
ug/L
ND
ND
30
cis-1,3-Dichloropropene
ug/L
ND
ND
30
Dibromochloromethane
ug/L
ND
ND
30
Dibromomethane
ug/L
ND
ND
30
Ethylbenzene
ug/L
ND
ND
30
lodomethane
ug/L
ND
ND
30
Methylene Chloride
ug/L
ND
ND
30
Styrene
ug/L
ND
ND
30
Tetrachloroethene
ug/L
ND
ND
30
Toluene
ug/L
ND
ND
30
trans-1,2-Dichloroethene
ug/L
ND
ND
30
trans- 1,3-Dichloropropene
ug/L
ND
ND
30
trans-1,4-Dichloro-2-butene
ug/L
ND
ND
30
Trichloroethene
ug/L
ND
ND
30
Trichlorofluoromethane
ug/L
ND
ND
30
Vinyl acetate
ug/L
ND
ND
30
Vinyl chloride
ug/L
ND
ND
30
Xylene (Total)
ug/L
ND
ND
30
1,2-Dichloroethane-d4 (S)
%
95
97
4-Bromofluorobenzene (S)
%
99
99
Toluene-d8 (S)
%
100
101
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/07/2020 11:46 AM without the written consent of Pace Analytical Services, LLC.
Page 32 of 38
Pace Analytical Services, LLC
9800
lCtaac,Analyfical ® Kiney Ave. Suite 100
Huntersville, NC 28078
0788
www.pacelabs.com (704)875-9092
QUALIFIERS
Project: Surry MSWLF SWs
Pace Project No.: 92457589
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
B Analyte was detected in the associated method blank.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/07/2020 11:46 AM without the written consent of Pace Analytical Services, LLC. Page 33 of 38
lceAnalyircal
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Surry MSWLF SWs
92457589
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92457589001
SW-1
EPA 3010A
516496
EPA 6010D
516513
92457589002
SW-2
EPA 3010A
516498
EPA 6010D
516514
92457589003
SW-3
EPA 3010A
516498
EPA 6010D
516514
92457589004
SW-4
EPA 3010A
516498
EPA 6010D
516514
92457589006
SWN-2
EPA 3010A
516498
EPA 6010D
516514
92457589007
SW-C
EPA 3010A
516498
EPA 6010D
516514
92457589001
SW-1
EPA 3010A
516497
EPA 6020B
516517
92457589002
SW-2
EPA 3010A
516501
EPA 6020B
516518
92457589003
SW-3
EPA 3010A
516501
EPA 6020B
516518
92457589004
SW-4
EPA 3010A
516501
EPA 6020B
516518
92457589006
SWN-2
EPA 3010A
516501
EPA 6020B
516518
92457589007
SW-C
EPA 3010A
516501
EPA 6020B
516518
92457589001
SW-1
EPA 8260D
516391
92457589002
SW-2
EPA 8260D
516422
92457589003
SW-3
EPA 8260D
516422
92457589004
SW-4
EPA 8260D
516422
92457589006
SWN-2
EPA 8260D
516391
92457589007
SW-C
EPA 8260D
516422
Date: 02/07/2020 11:46 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 34 of 38
Document Name:
Document Revised: February 7, 2018
m
Y aCeAnalyficaf
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
!
F-CAR-CS-033-Rev.05
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville Raleigh❑ Mechanicsville[]
Sample Condition Client Name: Proje wo# : 92457589
upon Receipt ct
mul,n1i V1 I
Courier: ❑Fed Ex I ❑UPS V ❑uSP5 ❑Client
❑ Commercial ace ❑Other; 929 57589
Custody Seal Present? ❑Yes E36 Seals Intact? ❑Yes E390
Packing Material; ❑Bubble Wrap ubbfe Bags ❑None ❑ Other
Thermometer: Type of Ice: Q<et ❑Blue
CWGun ID: 92TO58
Cooler Temp i'C): 1 - 5 Correction Factor: Add/Subtract VC) 0.0°C
Cooler Temp Corrected ('C): .
USDA Regulated Sall (El --N/A, water sample)
Did samples origina a in a quarantine zone. within the United States: CA, NY, or 5C (check maps)?
M
Date/initials Person EKamining Contents:_ j�
Slofaglcaf ue Frozen?
❑Yes No [-]N/A
❑None
Temp should be above freezing to VC
[]samples out of terip criteria. Samples on ice, coolingprocess
hasbegto
Did sanplesoriginate fram aforelgn source tinternationally,
Including Hawaii and Puerto Ricci? nYes ❑No
Comme r:.ts/Discrepancy;
Chain of Custody Present?
Yes
No
❑NIA
1.
`
Samples Arrived within Hold Time?
es
ON.
❑NIA
2.
Short Hold Time Analysis (t72 hr.)?
❑Yes
RrN. _
❑NIA
3,
flush Turn Around Time Requestei7
nYes
No
[]N/A
4.
Sufficient Volume?
Fd<
❑Nn
❑N!A
5.
Correct Containers Used?
0<
ON.
❑N/A
6.
-Pace Containers Used
51es
[-]No
[]N/A
Containers Intact?
2fB
❑ND
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
❑Nv
0<1A
B.
Sample Labels Match COC7
es
❑No
[] N/A
9.
-Includes Date/Time/IDtAnalysis Matrix:
`
Headspace in VOA Vials 1>5-6nimf?
Oyes
0<
❑N/A
10.
Trip Blank Present-
❑Yes
Oka
❑NIA
11.
Trip Blank Custody Seals Present?
[]Yes
❑No
A'
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIRCATIdN/RESOLUTION
Field Data Required? []Yes [:]No
I
Person contacted:
Date/Time:
Project Manager SCURF Review: omb slate: f S ^1 q
Project Manager SRF Review: T J f ►�L _ Date: ! - j 9-
Page 35 of 38
_ � aceAnalytical
Document Name:
Sample Condition Upon Recelpt(SCUR)
Document Revised: February 7, 2018
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR•CS-033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/BUS (water) DOC, LLHg
**Bottom half of box is to —IFS —f—number of battle
Project 1#
WN : 92457589
PM: AMB Due Date: 12/31/19
CLIENT: 92—Municipal
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Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy ofthis form will be sent to the North Carolina DEHNR Cemricanan VTTICe ti.e.
out of hold, incorrect preservative, out of temp, incorrect containers.
Page 36 of 38
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Page 38 of 38