FA-644_11660_CA_MRP_20200103

January 3, 2020

Mr. Mark Petermann
NCDEQ, Division of Waste Management, UST Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Reference: Groundwater Monitoring Report – Four Points Grocery Site
5830 Goldsboro Road
Wade, Cumberland County, North Carolina
NCDEQ Incident: 11660
UST No: FA-664
NCDEQ Contract: N17006
ECS Project: 49:1503-F

Dear Mr. Petermann:

As authorized by your acceptance of ECS Southeast, LLP (ECS) Task Authorization Request No.
5 (TAR No. 5) dated October 8, 2019, ECS has completed the Groundwater Monitoring Report
for the above-referenced site. Included in this report is a description of the field activities, the
results obtained, and our conclusions and recommendations.

ECS appreciates the opportunity to provide our environmental consulting services to you on this
project. If you have any questions concerning this report or this project, please contact us.

Sincerely,

ECS SOUTHEAST, LLP

Samantha M. Szakasits, G.I.T. Matthew Gillis
Assistant Staff Project Manager Sr. Environmental Project Manager
[e-mail] [e-mail]
919-861-9832 919-861-9845

Roger A. Smith, P.G.
Principal Geologist
NC License No. 1724
[e-mail]
704-525-5152
Groundwater Monitoring Report – Four Points Grocery Site
5830 Goldsboro Road
Wade, Cumberland County, North Carolina
NCDEQ Incident: 11660
UST No: FA-644
NCDEQ Contract: N17006

1
SITE INFORMATION

Facility I.D.: Unknown
UST Incident No.: 11660
UST No.: FA-644
Site Rank: H332D
Land Use Category: Residential

Site Name and Location: Four Points Grocery Site
5830 Goldsboro Road
Wade, Cumberland County, North Carolina

Latitude and Longitude: 35.133345 North, -78.695361 West
Contacts

Property Owner: Ms. Carol Lucas
5830 Goldsboro Road
Wade, North Carolina 28395

Consultant: ECS Southeast, LLP
9001 Glenwood Avenue
Raleigh, North Carolina 27617
[phone]
Attn: Matthew Gillis

Laboratory: Con-Test Analytical Laboratory
39 Spruce Street
East Longmeadow, MA 01028
[phone]
NC Certification No. 652

Groundwater Monitoring Report – Four Points Grocery Site
5830 Goldsboro Road
Wade, Cumberland County, North Carolina
NCDEQ Incident: 11660
UST No: FA-644
NCDEQ Contract: N17006

3
EXECUTIVE SUMMARY

The subject site is known as the Four Points Grocery Site and is located at 5830 Goldsboro Road
in Wade, Cumberland County, North Carolina. The subject site is further identified by
Cumberland County Geographic Information Systems (GIS) Parcel Identification Number (PIN)
0590-13-1462 and is owned by Mrs. Carol Lucas. The subject site formerly operated as a
gasoline station and grocery store and was converted into a single-family residence. The
Crossroads Site is located approximately 350 feet northeast and topographically downgradient of
the Four Points Grocery Site. In the past, the two sites were assessed concurrently and shared
the same network of monitoring wells and water supply wells.

INCIDENT RISK EVALUATION SUMMARY
SOURCE INFORMATION
Source, Date, and Nature of Release 2 x 1,000-gallon UST (unknown) and 1 x 500-gallon UST
(unknown)
Each Known Source Removed? Yes – Known 3 USTs removed in 1988
Additional Sources Likely Present? No
Known Sources Assessed (USTs, Piping,
Dispensers)? Yes
FREE PRODUCT
Free Product Present? Yes, prior to AVFR event
SITE SOIL CONDITIONS
TPH Soil Data Available? Maximum concentration at site No
Risk-Based Soil Data Available? No
Maximum Soil Contaminant Concentrations Unknown
Current Extent of Soil Impact Delineated? Unknown
SITE GROUNDWATER CONDITIONS
Average Depth to Groundwater? Approx. 2.5 to 4.5 feet below ground surface
Contaminants Present Above NC2L? Yes (Monitoring wells MW-2, MW-2D, MW-3, and MW-5)
Contaminants Present Above GCLs? No
Groundwater Plume Delineated? No
Groundwater Plume Migrated Off-Site? Unknown
Contaminant Level Trend Stable/Decreasing – migrating west-southwest
RECEPTOR INFORMATION
Date of Most Current Receptor Survey March 2018
Potable Water-Supply Wells within 1,000’? Yes (Water supply wells SW-4, SW-5, and SW-6)
Water Available to Properties within 1,000’? Yes
Non-Potable Wells within 250’? Yes (Water supply well SW-2)
Site within Wellhead Protection Area? No
Surface Water Bodies within 500’? No
REMEDIAL ACTIVITIES
Remedial activities conducted? AFVR and O-Sox Remedial Device Deployment
VAPOR INTRUSION
Dissolved Contaminants exceeding Groundwater Screening
Levels for Vapors present within 5’ of Ground Surface? Yes
Occupied Structures on the Site? Yes

Groundwater Monitoring Report – Four Points Grocery Site
5830 Goldsboro Road
Wade, Cumberland County, North Carolina
NCDEQ Incident: 11660
UST No: FA-644
NCDEQ Contract: N17006

4
On November 5, 2019, ECS removed the O-SOX remedial devices from monitoring wells MW-2,
MW-2D, MW-3, MW-4, and MW-5 prior to sampling activities. ECS then collected a field blank
and groundwater samples from monitoring wells MW-1, MW-2, MW-2D, MW-3 through MW-6,
and water supply wells SW-4, SW-5, SW-6.

Laboratory analysis reported several targeted analytes at concentrations above their respective
North Carolina 2L Groundwater Quality Standards (NC2LGWQS) but below their respective Gross
Contamination Levels (GCLs) in the groundwater sample collected from monitoring wells MW-2,
MW-2D, MW-3, and MW-5. Laboratory analysis reported several additional targeted analytes at
concentrations above their respective laboratory reporting limits but below their respective
NC2LGWQS in the groundwater samples collected from monitoring wells MW-2, MW-2D, MW-3,
MW-4, and MW-5.

Laboratory analysis did not report targeted analytes at concentrations above the laboratory
reporting limits in the groundwater samples collected from monitoring well MW-1 and MW-6, and
water supply wells SW-4, SW-5, and SW-6.

Based on the results of this assessment, ECS concludes the following:

 Laboratory analysis reported several targeted analytes at concentrations above their
respective NC2LGWQS but below their respective GCLs in the groundwater sample collected
from monitoring wells MW-2, MW-2D, MW-3, and MW-5.
 Laboratory analysis did not report targeted analytes at concentrations above the laboratory
reporting limits in the groundwater samples collected from monitoring well MW-1 and MW-6,
and supply wells SW-4, SW-5, and SW-6.
 Ms. Carol Lucas, the property owner of the residence associated with water supply well SW-
5 (subject site) informed ECS during a previous site visit that she is connected to municipal
water but refuses to use municipal water and prefers to use her water supply well.
 Since the previous groundwater sampling event and the 2018 aggressive fluid and vapor
recovery (AFVR) event, concentrations of targeted analytes have decreased significantly in
the groundwater samples collected from monitoring wells MW-2 and MW-3 however,
concentrations have slightly increased in the groundwater sample collected from monitoring
well MW-5. This suggests that the contaminant plume appears to be migrating downgradient
of the source area. The concentrations of targeted analytes in MW-2D have remained
unchanged.
 The O-SOX appear to have significantly reduced the dissolved petroleum-related constituents
subsequent to the Aggressive Fluid Vapor Recovery (AFVR) event conducted in November
2018.
 The extent of the plume has yet to be defined to the west-southwest.

Based on the results and conclusions of this assessment, ECS recommends deploying O-SOX
in monitoring wells MW-2, MW-2D, MW-3, and MW-5 and collecting groundwater samples from
the seven monitoring wells (MW-1 through MW-6) and the three water supply wells (SW-4
through SW-6) 90 days subsequent to the O-SOX deployment. Based on a conversation with
Mr. Mark Petermann of NCDEQ, the NCDEQ recommends reconfirming with Mr. Sealey, owner
of water supply well SW-4, that he continues to agree to be connected to municipal water, if
warranted. Additionally, NCDEQ recommends advising Ms. Lucas, property owner of the
Groundwater Monitoring Report – Four Points Grocery Site
5830 Goldsboro Road
Wade, Cumberland County, North Carolina
NCDEQ Incident: 11660
UST No: FA-644
NCDEQ Contract: N17006

5
subject site, that since she is already connected to municipal water but chooses to use her
water supply well the risk of the site could be alleviated and when possible the NCDEQ will
close the incident and attach a deed restriction to the property.

Groundwater Monitoring Report – Four Points Grocery Site
5830 Goldsboro Road
Wade, Cumberland County, North Carolina
NCDEQ Incident: 11660
UST No: FA-644
NCDEQ Contract: N17006

6
TABLE OF CONTENTS

1.0 SITE HISTORY ......................................................................................................... 7
2.0 SITE GEOLOGY AND HYDROGEOLOGY............................................................... 9
4.0 FIELD ACTIVITIES ................................................................................................. 11
5.0 LABORATORY ANALYTICAL RESULTS ............................................................... 12
6.0 CONCLUSIONS ...................................................................................................... 13
7.0 RECOMMENDATIONS ........................................................................................... 13

FIGURES

Figure 1 Site Location Map
Figure 2 Aerial Site Map
Figure 3 Water Supply Well Location Map
Figure 4 Monitoring Well Location Map
Figure 5 Groundwater Elevation Map
Figure 6 Groundwater Concentration Map
Figure 7 Ethylbenzene Isoconcentration Map
TABLES

Table 1 UST Information
Table 2 Water Supply Well Information
Table 3 Monitoring Well Construction and Groundwater Elevation Details
Table 4 Geochemical Measurements
Table 5 Summary of Current Groundwater Analytical Results
Table 6 Summary of Historical Groundwater Analytical Results

APPENDICIES

Appendix A Site Photographs
Appendix B ECS Personnel Field Notes
Appendix C Laboratory Analytical Data Sheets and Chain of Custody Record

Groundwater Monitoring Report – Four Points Grocery Site
5830 Goldsboro Road
Wade, Cumberland County, North Carolina
NCDEQ Incident: 11660
UST No: FA-644
NCDEQ Contract: N17006

7
1.0 SITE HISTORY

The Four Points Grocery Site is located at 5830 Goldsboro Road in Wade, Cumberland County,
North Carolina (Figures 1 and 2). Information contained in a 2010 Comprehensive Site
Assessment Report, prepared by Agra Environmental, Inc. (Agra), reported that on December 16,
1993, S&ME advanced 13 temporary wells along the DOT right-of-way. Petroleum contamination
was reported in groundwater samples collected from seven of the 13 soil borings. The highest
concentration of contaminants was reported in the temporary well located at the Four Points
Grocery Site. The Four Points Grocery Site previously contained USTs, which were closed in-
place in 1988. Information pertaining to the former USTs is summarized in Table 1. The Four
Points Grocery Site was accepted into the Trust Fund in March 1994. S&ME conducted an
additional site assessment at the Four Points Grocery Site on October 11 and 12, 1995. S&ME
installed three monitoring wells (MW-1, MW-2, and MW-3) at the Four Points Grocery Site. The
laboratory detected several targeted analytes at concentrations above the respective
NC2LGWQS in monitoring wells MW-2 and MW-3.

In July 2009, Agra conducted a water supply well sampling event and sampled the McLamb water
supply well (DW-2), associated with the Crossroads site, subject site water supply well (DW-3)
(IW-10), and Lucas water supply well (DW-5) (SW-5). The laboratory did not detect targeted
analytes at concentrations above the laboratory reporting limits in the groundwater samples
collected. During the sampling event, several property owners indicated a public water line would
be installed along the DOT right-of-way in the near future and that properties would be required to
connect to the municipal water line, although several owners stated that they would continue to
utilize their water supply wells.

In July 2010, Agra installed a Type III monitoring well (MW-2D) at the subject site. During boring
advancement, Agra screened soils from the boring of MW-2D with a photoionized detector (PID).
The PID measured 1,064 parts per million (ppm) from the soils collected from MW-2D.
Additionally, Agra collected groundwater samples from the monitoring wells and water supply
wells. Agra was unable to locate monitoring wells MW-10, MW-12, MW-16, MW-19, and MW-20;
therefore, groundwater samples were not collected from these wells. Monitoring well MW-18 was
dry; therefore, a groundwater sample was not collected. Monitoring wells MW-10, MW-12, MW-
16, MW-18, MW-19, and MW-20 are associated with the Crossroads Site, located south of the
Four Points Grocery site. The laboratory detected several targeted analytes at concentrations
above the NC2LGWQS in monitoring wells MW-2, MW-2D, and MW-3. The laboratory did not
detect targeted analytes at concentrations above the NC2LGWQS in monitoring well MW-1. The
laboratory did not detect targeted analytes at concentrations above the NC2LGWQS in water
supply wells SW-5, SW-6, and IW-7.

Information contained in a 2011 Groundwater Monitoring Report, prepared by Agra, reported
approximately 0.5 feet of free product was observed in monitoring well MW-2. The laboratory did
not detect targeted analytes at concentrations above the respective NC2LGWQS in monitoring
wells MW-1, MW-2D, or MW-3. The laboratory did not detect targeted analytes at concentrations
above the NC2LGWQS in water supply wells SW-5 or SW-6.

Information contained in a 2012 Electromagnetic Survey Report, prepared by Agra, reported a
high-resolution electromagnetic (EM) survey was completed along the northern and southern
sides of the Four Points Grocery building. Agra identified three anomalies consist with USTs. The
Groundwater Monitoring Report – Four Points Grocery Site
5830 Goldsboro Road
Wade, Cumberland County, North Carolina
NCDEQ Incident: 11660
UST No: FA-644
NCDEQ Contract: N17006

8
USTs were believed to be located underneath the house extension (canopy) and oriented
northwest to southeast. Two of the three USTs were determined to have a likely capacity of
approximately 1,000 gallons and the third UST a likely capacity of approximately 550 gallons. The
USTs are located approximately 40 to 50 feet northeast and up-gradient of monitoring well MW-2.
These USTs have not been confirmed by collaborating evidence. Agra attempted to install hand
auger borings in the vicinity of MW-2 and the USTs. Agra encountered asphalt at approximately 6
inches below the ground surface; therefore, soil samples were not collected.

On September 8, 2014, ECS conducted a receptor survey at the subject site. ECS observed four
monitoring wells and one water supply well on the subject site. Additionally, ECS identified nine
water supply wells within 1,500 feet of the subject site. Big Creek was identified approximately
9,500 feet southwest of site. Surface runoff on the site is expected to flow generally to the
southwest towards Big Creek.

On February 18, 2015, ECS collected groundwater samples from monitoring wells MW-1
through MW-3, and MW-2D. ECS also collected groundwater samples from water supply wells
SW-2 and SW-4. Laboratory analysis reported several targeted analytes at concentrations above
the respective NC2LGWQS but below their respective GCLs in the groundwater samples
collected from monitoring wells MW-2 and MW-2D. Laboratory analysis reported several
additional targeted analytes at concentrations above laboratory reporting limits but below the
respective NC2LGWQS in the groundwater samples collected from monitoring wells MW-2, MW-
2D, and MW-3. The laboratory did not report targeted analytes at concentrations above the
respective laboratory reporting limits in the groundwater sample collected from monitoring well
MW-1. Laboratory analysis reported chloroform at a concentration above laboratory reporting
limits but below its NC2LGWQS in the groundwater sample collected from water supply well SW-
2. The laboratory did not report targeted analytes at concentrations above the respective
laboratory reporting limits in the groundwater sample collected from water supply well SW-4.

On March 23, 2016, ECS installed three groundwater monitoring wells (MW-4 through MW-6) at
the subject site. ECS contracted with Bateman Civil Survey to survey the new monitoring wells.
On March 23 and 25, 2016, ECS collected groundwater samples from monitoring wells MW-1,
MW-2, MW-2D, MW-3 through MW-6, and water supply wells SW-4 through SW-6. Laboratory
analysis reported several targeted analytes at concentrations above the respective NC2LGWQS
but below their respective GCLs in the groundwater samples collected from monitoring wells MW-
2, MW-2D, MW-3, and MW-5. Laboratory analysis reported several additional targeted analytes
at concentrations above laboratory reporting limits but below the respective NC2LGWQS in the
groundwater samples collected from monitoring wells MW-2, MW-2D, MW-3 and MW-5.
Laboratory analysis did not report targeted analytes at concentrations above the respective
laboratory reporting limits in the groundwater sample collected from monitoring wells MW-1, MW-
4, and MW-6 and water supply wells SW-4, SW-5, and SW-6.

On December 13, 2016, ECS collected a field blank and groundwater samples from monitoring
wells MW-2, MW-2D, MW-3, and MW-5. Laboratory analysis reported several targeted analytes
above the respective NC2LGWQS but below the respective GCL in the groundwater sample
collected from monitoring well MW-2. Laboratory analysis also reported several additional
targeted analytes above the laboratory reporting limits but below the respective NC2LGWQS in
the groundwater sample collected from monitoring well MW-2, MW-2D, and MW-3. Laboratory
analysis reported naphthalene above its NC2LGWQS but below its GCL in the groundwater
Groundwater Monitoring Report – Four Points Grocery Site
5830 Goldsboro Road
Wade, Cumberland County, North Carolina
NCDEQ Incident: 11660
UST No: FA-644
NCDEQ Contract: N17006

9
samples collected from monitoring wells MW-2D and MW-3. Laboratory analysis reported several
targeted analytes above the respective NC2LGWQS but below the respective GCLs in the
groundwater sample collected from monitoring well MW-5.

On June 13, 2017, ECS collected groundwater samples from monitoring wells MW-2, MW-2D,
MW-3, and MW-5. Laboratory analysis reported several targeted analytes above their respective
NC2LGWQS but below their respective GCL in the groundwater samples collected from
monitoring wells MW-2, MW-2D, MW-3, and MW-5. Laboratory analysis also reported several
additional targeted analytes at concentrations above their respective laboratory reporting limits but
below their respective NC2LGWQS in the groundwater samples collected from monitoring well
MW-2, MW-2D, MW-3, and MW-5. Laboratory analysis reported naphthalene at a concentration
above its NC2LGWQS but below its GCL in the groundwater sample collected from monitoring
well MW-2D.

On March 27 and 28, 2018, ECS collected groundwater samples from monitoring wells MW-1,
MW-2, MW-2D, MW-4, MW-5, and MW-6, and water supply wells SW-4 and SW-5. Free
product was encountered at monitoring well MW-3 at a thickness of 0.02 feet. Laboratory
analysis reported several targeted analytes at concentrations above their respective NC2LGWQS
but below their respective GCLs in the groundwater sample collected from monitoring well MW-2.
Laboratory analysis also reported several additional targeted analytes at concentrations above
their respective laboratory reporting limits but below their respective NC2LGWQS in the
groundwater samples collected from monitoring well MW-2. Laboratory analysis reported several
targeted analytes at concentrations above their respective lab reporting limits but below their
respective NC2LGWQS in the groundwater samples collected from monitoring wells MW-2D,
MW-4, and MW-5. Laboratory analysis did not report targeted analytes at concentrations above
the lab reporting limits in the groundwater samples collected from monitoring wells MW-1 and
MW-6, the field blank, and water supply wells SW-4 and SW-5.

On November 8, 2018, ECS contracted with HERR, Inc. (HERR) to conduct an AFVR event at
the site using monitoring well MW-3 as an extraction point. A total of approximately 2,784
gallons of liquid was removed from the monitoring well. On November 20, 2018, ECS then
collected groundwater samples from monitoring wells MW-1, MW-2, MW-2D, and MW-3
through MW-6. Laboratory analysis reported several targeted analytes at concentrations above
their respective NC2LGWQS but below their respective GCLs in the groundwater sample
collected from monitoring wells MW-2, MW-2D, MW-3, and MW-5. Laboratory analysis reported
several additional targeted analytes at concentrations above their respective laboratory reporting
limits but below their respective NC2LGWQS in the groundwater samples collected from
monitoring wells MW-2, MW-2D, MW-3, and MW-5. Laboratory analysis did not report targeted
analytes at concentrations above the lab reporting limits in the groundwater samples collected
from monitoring well MW-1, MW-4, and MW-6, the field blank, and supply well SW-4.

2.0 SITE GEOLOGY AND HYDROGEOLOGY

As determined from the USGS Topographic Map, Wade, North Carolina Quadrangle dated
2013 (Figure 1), the site is at an approximate elevation of 170 feet above mean sea level.
Surface runoff and groundwater flow at the site is generally to the southwest.

Groundwater Monitoring Report – Four Points Grocery Site
5830 Goldsboro Road
Wade, Cumberland County, North Carolina
NCDEQ Incident: 11660
UST No: FA-644
NCDEQ Contract: N17006

10
The subject site is situated in the Coastal Plain Physiographic Province. The soils encountered
in this area are the residual product of in-place chemical weathering of rock presently
underlying the site and/or historic depositional events. In general, shallow unconfined
groundwater movement within the overlying soils is controlled largely by topographic gradients.
However, as the groundwater percolates downward, it becomes controlled by the subsurface
geologic conditions. Thus, the direction of groundwater movement in the deeper aquifers may
not be consistent with the reflecting topography.

In general, shallow unconfined groundwater movement within the overlying soils is controlled
largely by topographic gradients. Recharge occurs primarily by infiltration along higher
elevations and typically discharges into streams or other surface water bodies. The elevation of
the shallow water table is transient and can vary with seasonal fluctuations in precipitation.
Movement of shallow groundwater is generally from higher to lower elevations.

3.0 WATER SUPPLY WELLS

Historically, eight water supply wells (IW-1, SW-2, SW-4, SW-5, SW-6, IW-7, IW-9, and IW-10)
have been identified within 1,000 feet of the source area. In the 2014 Limited Site Assessment
(Phase II) prepared by Henry Nemargut Engineering Services, it was reported water supply
wells IW-7 and IW-9 were inactive and water supply wells IW-1 and IW-10 were used for
irrigation. Mr. Thomas J. Sealey, the property owner of the residence associated with water
supply well SW-4 located at 5815 Goldsboro Road in Wade, North Carolina has agreed to
connect to the municipal water supply, but would still maintain connection to his water supply
well to use for irrigation. Ms. Carol Lucas, the property owner of the residence associated with
water supply well SW-5 (subject site) informed ECS during a previous site visit that she is
connected to municipal water but refuses to use municipal water and prefers to use her water
supply well. ECS did not receive responses from the property owners associated with water
supply wells SW-2 and IW-9. Previously, ECS spoke with Ms. Melissa Cannon, the tenant
associated with SW-2, and Ms. Cannon stated she does not have the funds to pay for a water
bill at this time. During the June 13, 2017 sampling event, the residence associated with water
supply well SW-2 appeared to be vacant.

ECS conducted an updated receptor survey in March 2018 associated with the Crossroads site.
During the site reconnaissance, ECS determined that the home (addressed as 5816 Goldsboro
Road) associated with water supply well SW-2 has been vacant for at least six months and is
being sold to Christino Antonio Ventura and his wife, who currently reside at 5860 Goldsboro
Road. According to Mr. Christino Ventura’s and Mr. Miguel Ventura, the home will likely be
connected to municipal water once renovations are completed. Mr. Miguel Ventura shared that
water supply well SW-2 is currently broken and inactive.

Additionally, ECS mobilized to the Dawson residence (addressed as 5261 Wade Stedman
Road) and spoke with Mr. Walter Dawson who indicated that he is connected to municipal
water but does not have an active account. ECS spoke via phone with Mr. Thomas Sealey who
indicated he is not interested in abandoning water supply well SW-4 and wishes to continue
using it for irrigation. As per his instructions, ECS left the Access Agreement with pre-paid
postage at his residence on March 26, 2018. At the time of this report issuance, ECS has not
received his written response to the Access Agreement requesting his written permission to
abandon his water supply well and confirming his willingness to connect to municipal water. Ms.
Groundwater Monitoring Report – Four Points Grocery Site
5830 Goldsboro Road
Wade, Cumberland County, North Carolina
NCDEQ Incident: 11660
UST No: FA-644
NCDEQ Contract: N17006

11
Carol Lucas informed ECS that she does not want to activate her municipal water connection or
abandon her water supply well. ECS considers water supply well SW-6 to be active and
potable.

In summary, ECS found that:

 Water Supply Well SW-4 – located approximately 250 feet northwest from the subject site -
owned by Mr. Thomas Sealey, is currently active and potable. Mr. Thomas Sealey has
verbally refused to abandon his water supply well, but agreed to connect to municipal water.
 Water Supply Well SW-5 – located approximately 50 feet south of the source area on the
subject site – owned by Mr. Albert and Mrs. Carol Lucas, is currently active and potable. Ms.
Carol Lucas has verbally refused to abandon her water supply well and refused to reactive
her municipal water account.
 Water Supply Well SW-6 – located approximately 800 feet northwest from the subject site -
owned by Mr. Walter Dawson, is currently active and potable. Mr. Walter has verbally
refused to reactivate his municipal water account.
 Water Supply Well IW-1 – located approximately 700 feet southwest from the subject site –
owned by Ms. Phyllis Faircloth, is currently inactive and the residence associated the
inactive water supply well is connected to municipal water. At the time of the previous
report, ECS has not received information regarding Ms. Phyllis Faircloth’s pending decision
regarding possible inactive water supply well abandonment approval or denial.
 Water Supply Well SW-2 – located approximately 200 feet southwest from the subject site –
presumably owned by Ms. Melissa Cannon, is currently inactive and broken. The residence
associated with the inactive water supply well is vacant and under renovation. The future
property owners would like to connect the property to municipal water and abandon the
inactive water supply well.

The locations of water supply wells are shown on Figure 3. A summary of the water supply well
information is included in Table 2.

4.0 FIELD ACTIVITIES

4.1 Monitoring Well Sampling Activities

On November 5, 2018, ECS collected a field blank and groundwater samples from monitoring
wells MW-1, MW-2, MW-2D, MW-3, MW-4, MW-5, and MW-6. The locations of the monitoring
wells are shown on Figure 4. ECS removed the O-SOX from monitoring wells MW-2, MW-2D,
MW-3, MW-4, and MW-5 prior to sampling activities. Site photographs documenting field
activities are included in Appendix A.

Prior to sampling and allowing the groundwater within the monitoring wells to equilibrate, ECS
collected static groundwater elevation measurements from each monitoring well using a
decontaminated water level meter. ECS collected the field blank by pouring DI water over the
water level meter probe and into the appropriate laboratory prepared sample containers.
Monitoring well construction details and groundwater elevation data is summarized in Table 3
and shown on Figure 5. Based on the groundwater elevation data, groundwater at the site
generally flows to the southwest.
Groundwater Monitoring Report – Four Points Grocery Site
5830 Goldsboro Road
Wade, Cumberland County, North Carolina
NCDEQ Incident: 11660
UST No: FA-644
NCDEQ Contract: N17006

12

Purging and sampling were accomplished using a new disposable bailer for each well. Monitoring
wells MW-1, MW-2, MW-2D, MW-3, MW-4, MW-5, and MW-6 were each purged until the
following geochemical field measurements had stabilized; temperature, pH, conductivity, and
dissolved oxygen. Geochemical measurements are included in Table 4. ECS personnel field
notes completed during field activities are included in the Appendix B. The groundwater samples
were transferred into sample containers provided by the laboratory.

The sample containers were labeled with ECS project number, sample identification, sample
date and time, and requested analytical analysis. The containers were placed into protective
packaging material and placed into a cooler with ice to maintain the samples at approximately
4 Celsius (C). The samples were submitted to Con-Test Analytical Laboratory (Con-Test), a
North Carolina certified laboratory located in East Longmeadow, Massachusetts for chemical
analysis for volatile organic compounds (VOCs) using Standard Method 6200B. ECS
maintained Chain of Custody (COC) procedures throughout the sample collection and
transportation process.

4.2 Water Supply Well Sampling Activities

ECS previously obtained written authorization from property owners to sample water supply wells
SW-4, SW-5, and SW-6. On November 5, 2019, groundwater samples were collected from
these three water supply wells. Each water supply well was allowed to purge by opening the
spigot and running the well approximately 10 to 15 minutes. After purging the wells, the
groundwater samples were transferred into sample containers provided by the laboratory.

The sample containers were labeled with ECS project number, sample identification, sample
date and time, and requested analytical analysis. The containers were placed into protective
packaging material and placed into a cooler with ice to maintain the samples at approximately
4 Celsius (C). The samples were submitted to Con-Test for chemical analysis for VOCs using
Standard Method 6200B. ECS maintained COC procedures throughout the sample collection
and transportation process.

5.0 LABORATORY ANALYTICAL RESULTS

5.1 Monitoring Well Analytical Results

Laboratory analysis reported several targeted analytes at concentrations above their respective
NC2LGWQS but below their respective GCLs in the groundwater sample collected from
monitoring wells MW-2, MW-2D, MW-3, and MW-5. Laboratory analysis reported several
additional targeted analytes at concentrations above their respective laboratory reporting limits but
below their respective NC2LGWQS in the groundwater samples collected from monitoring wells
MW-2, MW-2D, MW-3, and MW-5.

Acetone was detected above its laboratory detection limit in the groundwater sample collected
from monitoring well MW-4; however, the detection was a concentration that was flagged by the
laboratory as J-value, indicating it was detected but below the reporting limit (lowest calibration
standard); therefore, the result is an estimated concentration. It should be noted that acetone is
Groundwater Monitoring Report – Four Points Grocery Site
5830 Goldsboro Road
Wade, Cumberland County, North Carolina
NCDEQ Incident: 11660
UST No: FA-644
NCDEQ Contract: N17006

13
a common laboratory artifact, and the reported estimated detections may not be indicative of
current site conditions.

Laboratory analysis did not report targeted analytes at concentrations above the laboratory
reporting limits in the groundwater samples collected from monitoring wells MW-1 and MW-6.

5.2 Water Supply Well Analytical Results

Laboratory analysis did not report targeted analytes at concentrations above the laboratory
reporting limits in the groundwater samples collected from supply wells SW-4, SW-5, and SW-6.

5.3 Field Blank Analytical Results

Methylene chloride was detected above its laboratory detection limit in the field blank; however,
the detection was a concentration were flagged by the laboratory as J-value indicating it was
detected but below the reporting limit; therefore, the result is an estimated concentration. It
should be noted that methylene chloride is a common laboratory artifact, and the reported
estimated detections may not be indicative of current site conditions.

A summary of the laboratory analytical results is included in Table 5 and shown on Figure 6 and
Figure 7. A summary of historical groundwater analytical results is included in Table 6. The
laboratory analytical data sheets and COCs are included in Appendix C.

6.0 CONCLUSIONS

Based on the results of this assessment, ECS concludes the following:

 Laboratory analysis reported several targeted analytes at concentrations above their
respective NC2LGWQS but below their respective GCLs in the groundwater sample collected
from monitoring wells MW-2, MW-2D, MW-3, and MW-5.

 Laboratory analysis did not report targeted analytes at concentrations above the laboratory
reporting limits in the groundwater samples collected from monitoring well MW-1 and MW-6,
and supply wells SW-4, SW-5, and SW-6.

 Ms. Carol Lucas, the property owner of the residence associated with water supply well SW-
5 (subject site) informed ECS during a previous site visit that she is connected to municipal
water but refuses to use municipal water and prefers to use her water supply well.

 Since the previous groundwater sampling event and the 2018 aggressive fluid and vapor
recovery (AFVR) event, concentrations of targeted analytes have decreased significantly in
the groundwater samples collected from monitoring wells MW-2 and MW-3 however,
concentrations have slightly increased in the groundwater sample collected from monitoring
well MW-5. This suggests that the contaminant plume appears to be migrating downgradient
of the source area. The concentrations of targeted analytes in MW-2D have remained
unchanged.

Groundwater Monitoring Report – Four Points Grocery Site
5830 Goldsboro Road
Wade, Cumberland County, North Carolina
NCDEQ Incident: 11660
UST No: FA-644
NCDEQ Contract: N17006
14
The O-SOX appear to have significantly reduced the dissolved petroleum-related constituents
subsequent to the Aggressive Fluid Vapor Recovery (AFVR) event conducted in November
2018.
The extent of the plume has yet to be defined to the west-southwest.
7.0 RECOMMENDATIONS
Based on the results and conclusions of this assessment, ECS recommends deploying O-SOX
in monitoring wells MW-2, MW-2D, MW-3, and MW-5 and collecting groundwater samples from
the seven monitoring wells (MW-1 through MW-6) and the three water supply wells (SW-4
through SW-6) 90 days subsequent to the O-SOX deployment. Based on a conversation with
Mr. Mark Petermann of NCDEQ, the NCDEQ recommends reconfirming with Mr. Sealey, owner
of water supply well SW-4, that he continues to agree to be connected to municipal water, if
warranted. Additionally, NCDEQ recommends advising Ms. Lucas, property owner of the
subject site, that since she is already connected to municipal water but chooses to use her
water supply well the risk of the site could be alleviated and when possible the NCDEQ will
close the incident and attach a deed restriction to the property.

FIGURES
SOURCE:
USGS TOPOGRAPHIC MAP
WADE NORTH CAROLINA QUADRANGLE
DATED 1913
SCALE: 1 : 24,000
FIGURE 1
SITE LOCATION MAP
FOUR POINTS GROCERY SITE
5830 GOLDSBORO ROAD
WADE, CUMBERLAND COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-11660
NCDEQ UST: FA-644
ECS PROJECT: 49:1503-F
SITE
FIGURE 2
AERIAL SITE MAP
FOUR POINTS GROCERY SITE
5830 GOLDSBORO ROAD
WADE, CUMBERLAND COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-11660
NCDEQ UST: FA-644
ECS PROJECT: 49:1503-F
SOURCE:
GOOGLE EARTH
DATED 2013
SCALE AS SHOWN
1 inch = 155 feet
AGRICULTURAL
SINGLE-FAMILY
RESIDENCES
AGRICULTURAL
CROSSROADS
SITE
SITE
SOURCE:
GOOGLE EARTH
DATED 2013
SCALE AS SHOWN
FIGURE 3
WATER SUPPLY WELL LOCATION MAP
FOUR POINTS GROCERY SITE
5830 GOLDSBORO ROAD
WADE, CUMBERLAND COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-11660
NCDEQ UST: FA-644
ECS PROJECT: 49:1503-F
1 inch = 500 feet
1,000 ft.
Radius
SW-6
Active
SW-5
Active
IW-9
Inactive
SW-4
Active
IW-1
Inactive
IW-7
Inactive
SITE
SW-2
Inactive
IW-7
SW-2
LEGEND
Approximate Location of Active,
Potable Water Supply Well
Approximate Location of Inactive
Water Supply Well
500 ft.
Radius
SOURCE:
GOOGLE EARTH
DATED 2013
SCALE AS SHOWN
FIGURE 4
MONITORING WELL LOCATION MAP
FOUR POINTS GROCERY SITE
5830 GOLDSBORO ROAD
WADE, CUMBERLAND COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-11660
NCDEQ UST: FA-644
ECS PROJECT: 49:1503-F
1 inch = 40 feet
SITE
MW-2
MW-2D
MW-3
MW-1
LEGEND
Approximate Location of Monitoring Well
Approximate Location of Active Water
Supply Well
Approximate Location of USTs Identified in
EM Survey dated 2012
MW-3
SW-5
SW-5
MW-6
MW-5
MW-4
SOURCE:
GOOGLE EARTH
DATED 2013
SCALE AS SHOWN
FIGURE 5
GROUNDWATER ELEVATION MAP
FOUR POINTS GROCERY SITE
5830 GOLDSBORO ROAD
WADE, CUMBERLAND COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-11660
NCDEQ UST: FA-644
ECS PROJECT: 49:1503-F
1 inch = 40 feet
SW-5
MW-6
161.24
MW-1
161.26
LEGEND
Approximate Location of Monitoring Well
Approximate Location of Active Water Supply Well
Groundwater Elevation
Groundwater Contour Line
Estimated Direction of Groundwater Flow
*Datum not used in determining groundwater elevation
MW-3
160.96
SW-5
Survey conducted by Bateman Civil Survey on March 25, 2016. Site vertical datum based on
NAV88. Site horizontal datum based on NAD83
MW-3
160.96
MW-2D *
159.41
161.00 161.25
MW-5
161.24
MW-2
161.00
MW-4
161.04
SOURCE:
GOOGLE EARTH
DATED 2013
SCALE AS SHOWN
FIGURE 6
GROUNDWATER CONCENTRATION MAP
FOUR POINTS GROCERY SITE
5830 GOLDSBORO ROAD
WADE, CUMBERLAND COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-11660
NCDEQ UST: FA-644
ECS PROJECT: 49:1503-F
1 inch = 40 feet
LEGEND
Approximate Location of Monitoring Well
Approximate Location of Active Water Supply Well
60 Concentration Above Laboratory Reporting Limit (µg/L)
4,500 Bold Concentration Above the NC2LGWQS (µg/L)
BRL Below Reporting Limits
J Estimated Concentration
MW-3
MW-1
BRL
SW-5
BRL
SW-5
MW-6
BRL
MW-2
Toluene 440
Ethylbenzene 360
Total Xylenes 1,680
2-Butanone (MEK)60 J
n-Butylbenzene 11
sec-Butlybenzene 6.4 J
Isopropylbenzene 30
Naphthalene 160
n-Propylbenzene 83
1,2,4-Trimethylbenzene 410
1,3,5-Trimethylbenzene 95
MW-2D
Toluene 1.2
Ethylbenzene 100
Total Xylenes 43
n-Butylbenzene 2.1
sec-Butlybenzene 1.6
Isopropylbenzene 9.4
p-Isopropyltoluene 0.60 J
Naphthalene 29
n-Propylbenzene 24
1,2,4-Trimethylbenzene 30
1,3,5-Trimethylbenzene 5.5
MW-3
Toluene 1,000
Ethylbenzene 900
Total Xylenes 4,500
n-Butylbenzene 40 J
sec-Butlybenzene 27 J
Isopropylbenzene 68
Naphthalene 730
n-Propylbenzene 220
1,2,4-Trimethylbenzene 1,400
1,3,5-Trimethylbenzene 370
MW-5
Toluene 440
Ethylbenzene 1,900
Total Xylenes 9,400
2-Butanone (MEK)66 J
n-Butylbenzene 9.6 J
sec-Butlybenzene 7.0 J
Isopropylbenzene 60
Naphthalene 310
n-Propylbenzene 140
Styrene 9.6 J
1,2,4-Trimethylbenzene 1,000
1,3,5-Trimethylbenzene 240
MW-4
Acetone 17 J
SOURCE:
GOOGLE EARTH
DATED 2013
SCALE AS SHOWN
FIGURE 7
ETHYLBENZENE ISOCONCENTRATION MAP
FOUR POINTS GROCERY SITE
5830 GOLDSBORO ROAD
WADE, CUMBERLAND COUNTY,
NORTH CAROLINA
NCDEQ INCIDENT: TF-11660
NCDEQ UST: FA-644
ECS PROJECT: 49:1503-E
1 inch = 40 feet
MW-1
BRL
SW-5
BRL
MW-6
BRL
MW-2
360
MW-4
BRL
LEGEND
Approximate Location of Monitoring Well
Approximate Location of Water Supply Well
Ethylbenzene Isoconcentration Contour (µg/L)
Estimated Ethylbenzene Isoconcentration Contour (µg/L)
41 Concentration Above the Laboratory Reporting Limit
1,900 Bold Concentration Above the NC2LGWQS
BRL Below Recording Limit
NOTES:
1.) *Concentration not used to determine the horizontal extent of ethylbenzene
MW-3
SW-5
MW-3
900
MW-2D*
100
MW-5
1,900
6
600
1,000

TABLES
UST ID
Number Contents Capacity
(in Gallons)
Constructio
n Details
Tank
Dimensions Installation Date Closure Date Status
1 Unknown 1,000 Unknown Unknown Unknown 1988 Closed-In Place
2 Unknown 1,000 Unknown Unknown Unknown 1988 Closed-In Place
3 Unknown 500 Unknown Unknown Unknown 1988 Closed-In Place
Wade, Cumberland County, North Carolina
ECS Project: 49:1503-F
Table 1
UST Information
Four Points Grocery Site
5830 Goldsboro Road
NCDEQ Incident:TF-11660
NCDEQ UST: FA-644
Water Supply
Well ID Well Owner*Well Owner Address*Well Address Well Address
PIN*Well Use Connected to Municipal Water Well Depth (ft
bgs)Type of Well
Approximate
Distance from Source
Area of Release (ft)
IW-1 Phyllis Faircloth 5764 Goldsboro Road Wade, NC 28395 5764 Goldsboro Road Wade, NC 28395 0590-03-6100 Irrigation Yes - Active Account Status Unknown Unknown 700 ft southwest
SW-2 Melissa Cannon 5816 Goldsboro Road Wade, NC 28395 5816 Goldsboro Road Wade, NC 28395 0590-13-0324 Inactive No - Desires to Connect in Future (Vacant Home undergoing Renovations)Unknown Unknown 200 ft southwest
SW-4 Thomas J. Sealey 5815 Goldsboro Road Wade,
NC 28395
5815 Goldsboro Road Wade,
NC 28395 0590-03-8789 Active No - Agreed to Connect Unknown Unknown 250 ft nothwest
SW-5 Albert & Carol Lucas 5830 Goldsboro Road Wade, NC 28395 5830 Goldsboro Road Wade, NC 28395 0590-13-1462 Active Yes - Inactive Account Status Unknown Unknown 50 ft south
SW-6 Walter Dawson 5261 Wade Stedman Road Wade, NC 28395 5261 Wade Stedman Road Wade, NC 28395 0590-03-5997 Active Yes - Inactive Account Status Unknown Unknown 800 ft northwest
IW-7 Jesse E. Dix 5285 Wade Stedman Road Wade, NC 28395 5285 Wade Stedman Road Wade, NC 28395 0590-04-5201 Inactive Yes - Active Account Status NA NA 850 ft northwest
IW-9 Judy M. Price 4513 Woodswallow Drive Fayetteville, NC 28312 5884 Goldsboro Road Wade, NC 28395 0590-13-5745 Inactive Yes - Active Account Status NA NA 550 ft northeast
IW-10 Ali Alsaidi 5786 Goldsboro Road Wade,
NC 28395
5786 Goldsboro Road Wade,
NC 28395 0590-03-6337 Abandoned Yes - Active Account Status NA NA 550 ft southwest
(Crossroads Site)
NOTES:
ft = feet
PIN = Property Identification Number
NCDEQ UST: FA-644
NA = Not Applicable
*Property Owner information confirmed by ECS via Cumberland County GIS on March 23 and April 24, 2018.
ft bgs = feet below the ground surface
ECS Project: 49:1503-F
Table 2
Water Supply Well Information
Four Points Grocery
5830 Goldsboro RoadWade, Cumberland County, North CarolinaNCDEQ Incident: TF-11660
Monitoring Well ID Date Measured
Depth to
Groundwater (ft. btoc)
Casing Inner
Diameter (I.D. in. )Date Installed Total Well Depth (ft. btoc)Screen Interval (ft. btoc)TOC Elevation *Groundwater Elevation (ft)
MW-1 11/5/2019 6.66 2 October 1995 13 3-13 167.92 161.26
MW-2 11/5/2019 6.53 2 October 1995 13 3-13 167.53 161.00
MW-2D 11/5/2019 8.56 2 July 2010 35 30-35 167.97 159.41
MW-3 11/5/2019 7.19 2 October 1995 13 3-13 168.15 160.96
MW-4 11/5/2019 6.73 2 March 24, 2016 12 2-12 167.77 161.04
MW-5 11/5/2019 6.83 2 March 24, 2016 12 2-12 168.07 161.24
MW-6 11/5/2019 6.82 2 March 24, 2016 12 2-12 168.06 161.24
NOTES:
ft. btoc = Feet Below Top of Casing
I.D. in. = Inside Diameter in Inches
NM = Not Measured
TOC = Top of Casing*Survey conducted by Bateman Civil Survey on March 25, 2016. Site vertical datum based on NAV88. Site horizontal datum based on NAD83.
ECS Project: 49:1503-F
NCDEQ Incident: TF-11660NCDEQ UST: FA-644
Table 3Monitoring Well Construction and Groundwater Elevation Details
Four Points Grocery Site
5830 Goldsboro Road
Wade, Cumberland County, North Carolina
SAMPLE ID MW-1 MW-2 MW-2D MW-3 MW-4 MW-5 MW-6
Date Sampled
pH 7.35 7.43 7.40 6.91 6.64 9.90 9.82
Temperature (oC)18.35 16.10 18.70 15.80 18.30 14.35 14.38
Conductivity (mS/cm)0.062 0.202 0.122 0.233 0.060 1.660 1.195
Dissolved O2 (mg/L)3.50 1.85 3.11 2.25 2.05 4.97 4.16Turbidity (Observed)NT ST ST ST T NT NT
NOTES:
mS/cm = milliseimens per centimeter
mg/L= milligrams per Liter
°C = degress Celsius
NT = Not Turbid
ST= Slightly Turbid
T= Turbid
Measured using YSI model 556 Meter
11/5/2019
NCDEQ UST: FA-644
ECS Project: 49:1503-F
Table 4
Geochemical Measurements
Four Points Grocery Site
5830 Goldsboro Road
Wade, Cumberland County, North Carolina
NCDEQ Incident: TF-11660
Sample ID Sample Date
TolueneEthylbenzeneTotal XylenesAcetone2-Butanone (MEK)n-Butylbenzenesec-ButylbenzeneIsopropylbenzene4-IsopropyltolueneMethylene ChlorideNaphthalenen-PropylbenzeneStyrene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneMW-1 11/5/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
MW-2 11/5/2019 440 360 1,680 BRL 60 J 11 6.4 J 30 BRL BRL 160 83 BRL 410 95
MW-2D 11/5/2019 1.2 100 43 BRL BRL 2.1 1.6 9.4 0.60 J BRL 29 24 BRL 30 5.5
MW-3 11/5/2019 1,000 900 4,500 BRL BRL 40 J 27 J 68 BRL BRL 730 220 BRL 1,400 370
MW-4 11/5/2019 BRL BRL BRL 17 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
MW-5 11/5/2019 440 1,900 9,400 BRL 66 J 9.6 J 7.0 J 60 BRL BRL 310 140 9.6 J 1,000 240
MW-6 11/5/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
SW-4 11/5/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
SW-5 11/5/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
SW-6 11/5/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
Field Blank 11/5/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL 0.43 J BRL BRL BRL BRL BRL
600 600 500 6,000 4,000 70 70 70 25 5 6 70 70 400 400
260,000 84,500 85,500 6,000,000 4,000,000 6,900 8,500 25,000 11,700 5,000 6,000 30,000 70,000 28,500 28,500
NOTES:
NC2LGWQS = North Carolina 2L Groundwater Quality Standard as of April 1, 2013
GCL = NCDEQ's Gross Contamination Levels for Groundwater as of April 16, 2012
BRL = Below Reporting Limit
J = Detected but below the Reporting Limit; therefore, result is an estimated concentration
Table 5
Summary of Current Groundwater Analytical Results
Four Points Grocery Site
5830 Goldsboro Road
Wade, Cumberland County, North Carolina
NCDEQ Incident: TF-11660
(µg/L) = Micrograms per L
NC2LGWQS (µg/L)
GCL (µg/L)
NCDEQ UST: FA-644
ECS Project: 49:1503-F
Standard Method 6200B
Contaminant of Concern/Concentration (µg/L)Analytical Method
Bold = Detected above the NC2LGWQS (µg/L)
Sample ID Sample Date
BenzeneTolueneEthylbenzeneTotal XylenesAcetone2-Butanone (MEK)n-Butylbenzenesec-Butylbenzenetert-ButylbenzeneChloroformo-ChlorotolueneIsopropylbenzenep-IsopropyltolueneMethyl chlorideMethyl Isobutyl KetoneMethyl tert-butyl etherNaphthalenen-PropylbenzeneStyrene1,2,3-Tricholopropane1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene5/13/2002 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL2/19/2003 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL3/29/2004 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL5/5/2005 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL1/31/2006 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL2/8/2007 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL5/23/2008 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL7/22/2010 BRL 1.3 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL2/18/2015 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL3/23/2016 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL3/27/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL11/20/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL11/5/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
5/13/2002 1,840 11,500 1,140 5,040 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL2/19/2003 1,400 14,200 1,600 8,850 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL3/29/2004 933 8,070 626 2,648 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL5/5/2005 1,300 19,000 1,700 8,400 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL1/31/2006 BRL 23,000 1,800 9,100 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
2/8/2007 10 4,400 770 3,600 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL5/23/2008 700 28,000 6,400 24,600 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL7/22/2010 140 21,000 2,200 12,100 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL2/18/2015 BRL 12,200 1,660 11,600 BRL BRL BRL BRL BRL BRL BRL 73.5 BRL BRL BRL BRL 368 164 19.4 BRL 1,340 3573/23/2016 BRL 4,500 1,200 6,400 BRL BRL BRL BRL BRL BRL BRL 40 BRL BRL BRL BRL 200 97 7.5 BRL 850 210
12/13/2016 BRL 3,380 1,020 5,710 BRL BRL 7.6 J 6.4 J BRL BRL 27.6 41.4 3.8 J BRL BRL BRL 232 107 8.5 J BRL 931 2456/13/2017 BRL 3,140 1,760 9,410 BRL BRL BRL BRL BRL BRL BRL 65.7 BRL BRL BRL BRL 387 BRL 15.3 BRL 1,260 BRL3/26/2018 BRL 1,700 3,200 15,700 BRL BRL 40 BRL BRL BRL BRL 150 BRL BRL BRL BRL 800 J 350 BRL BRL 2,500 57011/20/2018 BRL 800 1,000 5,600 BRL BRL 5.6 3.4 0.37 J 0.31 J BRL 47 2.0 BRL BRL BRL 150 120 BRL BRL 720 20011/5/2019 BRL 440 360 1,680 BRL 60 J 11 6.4 J BRL BRL BRL 30 BRL BRL BRL BRL 160 83 BRL BRL 410 95
7/22/2010 0.35 220 27 360 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL10/13/2011 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
2/18/2015 BRL 28.9 301 770 BRL BRL BRL BRL BRL BRL BRL 24.7 BRL BRL BRL BRL 89.9 63.4 BRL BRL 379 1103/23/2016 BRL 40 590 1,200 BRL BRL 7.5 6.0 BRL BRL BRL 47 2.5 BRL 1.4 BRL 250 110 BRL BRL 590 20012/13/2016 BRL 13.2 127 439 BRL BRL 1.8 1.5 0.18 J BRL BRL 9.4 1.4 0.21 J BRL BRL 70.4 29.3 BRL BRL 208 65.76/13/2017 BRL 11.6 228 413 BRL BRL BRL BRL BRL BRL BRL 15.8 BRL BRL BRL BRL 80.7 BRL BRL 89.7 254 BRL3/26/2018 BRL 0.95 19.0 28 BRL BRL 0.4 J 0.32 J BRL BRL BRL 2.0 BRL BRL BRL BRL 3.8 J 3.9 BRL BRL 7.5 1.711/20/2018 BRL 4.4 41 157 BRL BRL 1.6 0.55 BRL BRL BRL 4.6 0.20 J BRL BRL BRL 15 7.2 BRL BRL 53 1811/5/2019 BRL 1.2 100 43 BRL BRL 2.1 1.6 BRL BRL BRL 9.4 0.60 J BRL BRL BRL 29 24 BRL BRL 30 5.5
5/13/2002 8.8 8,210 1,020 5,870 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL 15.6 BRL BRL BRL BRL BRL BRL2/19/2003 BRL 11,700 1,760 9,040 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL3/29/2004 19.6 4,150 413 1,741 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
5/5/2005 BRL 8,600 1,000 5,400 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL1/31/2006 BRL 12,000 1,500 7,800 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL2/8/2007 750 21,000 1,400 7,200 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL5/23/2008 5.2 2,400 790 2,900 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL7/22/2010 BRL 21,000 5,100 26,600 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL2/18/2015 BRL 178 26.3 134.7 BRL BRL BRL BRL BRL BRL BRL 0.98 BRL BRL BRL BRL 4.9 2.2 BRL BRL 24.1 6.73/23/2016 BRL 310 68.0 280 BRL BRL BRL BRL BRL BRL BRL 2.5 BRL BRL BRL BRL 10 6.2 0.53 BRL 47.0 12.0
12/13/2016 BRL 330 61.1 424 BRL BRL 0.46 J 0.44 J BRL BRL BRL 3.8 0.25 J 0.96 BRL BRL 22.6 10.8 0.69 BRL 58.9 25.46/13/2017 BRL 6,360 1,200 6,410 BRL BRL BRL BRL BRL BRL BRL 47.0 BRL BRL BRL BRL 269 BRL BRL BRL 1,010 BRL
3/26/201811/20/2018 BRL 8,200 1,900 9,700 BRL BRL 12 J BRL BRL BRL BRL 54 BRL BRL BRL BRL 230 120 BRL BRL 960 240
11/5/2019 BRL 1,000 900 4,500 BRL BRL 40 J 27 J BRL BRL BRL 68 BRL BRL BRL BRL 730 220 BRL BRL 1,400 3703/25/2016 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL3/26/2018 BRL 3.1 1.1 5.0 BRL BRL BRL BRL BRL 0.47 J BRL BRL BRL BRL BRL BRL .32 J .18 J BRL BRL 0.75 BRL11/20/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
11/5/2019 BRL BRL BRL BRL 17 J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL3/25/2016 BRL 7,000 5,600 32,000 BRL BRL 140 39 BRL BRL BRL 250 18 BRL BRL BRL 610 690 31 BRL 4,300 1,10012/13/2016 BRL 3,930 3,690 20,400 BRL BRL 14.8 J 12.4 J BRL BRL BRL 115 6.8 J BRL BRL BRL 612 298 23.7 J BRL 2,230 5446/13/2017 BRL 3,310 3,230 17,350 BRL BRL BRL BRL BRL BRL BRL 113 BRL BRL BRL BRL 485 BRL 26.9 BRL 1,980 BRL3/27/2018 BRL 20 34 172 17 J BRL 0.73 0.26 J BRL 0.25 J BRL 1.6 0.18 J BRL BRL BRL 3.7 3.7 BRL BRL 23 4.611/20/2018 BRL 200 740 3,700 BRL BRL 26 7.5 BRL BRL BRL 41 4.2 J BRL BRL BRL 140 110 BRL BRL 740 21011/5/2019 BRL 440 1,900 9,400 BRL 66 J 9.6 J 7.0 J BRL BRL BRL 60 BRL BRL BRL BRL 310 140 9.6 J BRL 1,000 240
3/25/2016 BRL BRL BRL 0.65J BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL3/27/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL11/20/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL11/5/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRLSW-2 2/19/2015 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL2/19/2015 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL3/25/2016 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL3/26/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL11/20/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
11/5/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL3/25/2016 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL3/26/2018 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL11/5/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL3/25/2016 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL11/5/2019 BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL
1 600 600 500 6,000 4,000 70 70 70 70 NE 70 25 3 100 20 6 70 70 NE 400 400
5,000 260,000 84,500 85,500 6,000,000 4,000,000 6,900 8,500 15,000 70,000 NE 25,000 11,700 3,000 100,000 20,000 6,000 30,000 70,000 NE 28,500 25,000
NOTES:NC2LGWQS = North Carolina 2L Groundwater Quality Standard as of April 1, 2013GCL = NCDEQ's Gross Contamination Levels for Groundwater as of April 16, 2012Bold = Detected above the NC2LGWQS(µg/L) = Micrograms per LiterBRL = Below Reporting LimitJ = Detected but below the Reporting Limit; therefore, result is an estimated concentrationNE = Not Established
MW-6
SW-4
SW-5
MW-1
MW-2
MW-2D
Contaminant of Concern/Concentration (µg/L)
GCL (µg/L)
NC2LGWQS (µg/L)
SW-6
Analytical Method
MW-3
FREE PRODUCT
MW-4
MW-5
ECS Project: 49:1503-FNCDEQ UST: FA-644
Standard Method 6200B (or equivalent)
Table 6Summary of Historical Groundwater Analytical ResultsFour Points Grocery Site5830 Goldsboro Road
Wade, Cumberland County, North Carolina
NCDEQ Incident: TF-11660

APPENDIX A
SITE PHOTOGRAPHS
FOUR POINTS GROCERY SITE
5830 GOLDSBORO ROAD
WADE, CUMBERLAND COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-11660
ECS PROJECT: 49:1503-F
Photograph 1: View of the subject site and location of monitoring well MW-6. View is to the southeast.
Photograph 2: View of the location of water supply well SW-5. View is to the southeast.
Photograph 3: View of the location of monitoring well MW-1. View is to the southwest.
Photograph 4: View of the location of monitoring wells MW-2 and MW-2D. View is to the northeast.
SITE PHOTOGRAPHS
FOUR POINTS GROCERY SITE
5830 GOLDSBORO ROAD
WADE, CUMBERLAND COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-11660
ECS PROJECT: 49:1503-F
SITE PHOTOGRAPHS
FOUR POINTS GROCERY SITE
5830 GOLDSBORO ROAD
WADE, CUMBERLAND COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-11660
ECS PROJECT: 49:1503-F
Photograph 5: View of the location of monitoring well MW-3. View is to the northwest.
Photograph 6: View of the location of monitoring well MW-4. View is to the northeast.
SITE PHOTOGRAPHS
FOUR POINTS GROCERY SITE
5830 GOLDSBORO ROAD
WADE, CUMBERLAND COUNTY, NORTH CAROLINA
NCDEQ INCIDENT: TF-11660
ECS PROJECT: 49:1503-F
Photograph 7: View of the location of monitoring well MW-5. View is to the northeast.
Photograph 8: View of the location of water supply well SW-4. View is to the northwest.

APPENDIX B

APPENDIX C

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
November 12, 2019
Matt Gillis
ECS Southeast - Raleigh, NC
9001 Glenwood Avenue
Raleigh, NC 27617
Project Location: Wade, NC
Client Job Number:
Project Number: 49:1503 f
Laboratory Work Order Number: 19K0437
Enclosed are results of analyses for samples received by the laboratory on November 6, 2019. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 42
Table of Contents
Table of Contents
Sample Summary 3
Hits Only Report 4
Case Narrative 7
Sample Results 8
19K0437-01 8
19K0437-02 10
19K0437-03 12
19K0437-04 14
19K0437-05 16
19K0437-06 18
19K0437-07 20
19K0437-08 22
19K0437-09 24
19K0437-10 26
19K0437-11 28
Sample Preparation Information 30
QC Data 31
Volatile Organic Compounds by GC/MS 31
B245494 31
Flag/Qualifier Summary 36
Certifications 37
Chain of Custody/Sample Receipt 39
Page 2 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
11/12/2019
ECS Southeast - Raleigh, NC
9001 Glenwood Avenue
Raleigh, NC 27617
ATTN: Matt Gillis
49:1503 f
19K0437
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Wade, NC
field blank 19K0437-01 Field Blank SM21-22 6200B
MW-6 19K0437-02 Ground Water SM21-22 6200B
MW-5 19K0437-03 Ground Water SM21-22 6200B
MW-4 19K0437-04 Ground Water SM21-22 6200B
MW-3 19K0437-05 Ground Water SM21-22 6200B
MW-2 19K0437-06 Ground Water SM21-22 6200B
MW-1 19K0437-07 Ground Water SM21-22 6200B
MW-2D 19K0437-08 Ground Water SM21-22 6200B
SW-5 19K0437-09 Ground Water SM21-22 6200B
SW-4 19K0437-10 Ground Water SM21-22 6200B
SW-6 19K0437-11 Ground Water SM21-22 6200B
[TOC_1]Sample Summary[TOC]
Page 3 of 42
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:19K0437-02MW-6
No Results Detected
Client ID:Lab ID:19K0437-07MW-1
No Results Detected
Client ID:Lab ID:19K0437-09SW-5
No Results Detected
Client ID:Lab ID:19K0437-10SW-4
No Results Detected
Client ID:Lab ID:19K0437-11SW-6
No Results Detected
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 4 of 42
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0437-01field blank
DL
Methylene Chloride 0.43 5.0 g/L SM21-22 6200BJ0.34
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0437-03MW-5
DL
1,2,4-Trimethylbenzene 1000 10 g/L SM21-22 6200B3.6
1,3,5-Trimethylbenzene 240 10 g/L SM21-22 6200B2.8
2-Butanone (MEK)66 100 g/L SM21-22 6200BJ39
Ethylbenzene 1900 10 g/L SM21-22 6200B2.6
Isopropylbenzene (Cumene)60 10 g/L SM21-22 6200B3.4
m+p Xylene 6000 20 g/L SM21-22 6200B6.0
Naphthalene 310 100 g/L SM21-22 6200B6.2
n-Butylbenzene 9.6 10 g/L SM21-22 6200BJ4.2
n-Propylbenzene 140 10 g/L SM21-22 6200B2.6
o-Xylene 3400 10 g/L SM21-22 6200B3.4
sec-Butylbenzene 7.0 10 g/L SM21-22 6200BJ3.2
Styrene 9.6 10 g/L SM21-22 6200BJ2.2
Toluene 440 10 g/L SM21-22 6200B2.8
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0437-04MW-4
DL
Acetone 17 50 g/L SM21-22 6200BL-06, J 3.8
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0437-05MW-3
DL
1,2,4-Trimethylbenzene 1400 50 g/L SM21-22 6200B18
1,3,5-Trimethylbenzene 370 50 g/L SM21-22 6200B14
Ethylbenzene 900 50 g/L SM21-22 6200B13
Isopropylbenzene (Cumene)68 50 g/L SM21-22 6200B17
m+p Xylene 3100 100 g/L SM21-22 6200B30
Naphthalene 730 500 g/L SM21-22 6200B31
n-Butylbenzene 40 50 g/L SM21-22 6200BJ21
n-Propylbenzene 220 50 g/L SM21-22 6200B13
o-Xylene 1400 50 g/L SM21-22 6200B17
sec-Butylbenzene 27 50 g/L SM21-22 6200BJ16
Toluene 1000 50 g/L SM21-22 6200B14
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0437-06MW-2
DL
1,2,4-Trimethylbenzene 410 10 g/L SM21-22 6200B3.6
1,3,5-Trimethylbenzene 95 10 g/L SM21-22 6200B2.8
2-Butanone (MEK)60 100 g/L SM21-22 6200BJ39
Ethylbenzene 360 10 g/L SM21-22 6200B2.6
Isopropylbenzene (Cumene)30 10 g/L SM21-22 6200B3.4
m+p Xylene 1100 20 g/L SM21-22 6200B6.0
Naphthalene 160 100 g/L SM21-22 6200B6.2
n-Butylbenzene 11 10 g/L SM21-22 6200B4.2
n-Propylbenzene 83 10 g/L SM21-22 6200B2.6
o-Xylene 580 10 g/L SM21-22 6200B3.4
sec-Butylbenzene 6.4 10 g/L SM21-22 6200BJ3.2
Toluene 440 10 g/L SM21-22 6200B2.8
Page 5 of 42
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0437-08MW-2D
DL
1,2,4-Trimethylbenzene 30 1.0 g/L SM21-22 6200B0.36
1,3,5-Trimethylbenzene 5.5 1.0 g/L SM21-22 6200B0.28
Ethylbenzene 100 1.0 g/L SM21-22 6200B0.26
Isopropylbenzene (Cumene)9.4 1.0 g/L SM21-22 6200B0.34
m+p Xylene 21 2.0 g/L SM21-22 6200B0.60
Naphthalene 29 10 g/L SM21-22 6200B0.62
n-Butylbenzene 2.1 1.0 g/L SM21-22 6200B0.42
n-Propylbenzene 24 1.0 g/L SM21-22 6200B0.26
o-Xylene 22 1.0 g/L SM21-22 6200B0.34
p-Isopropyltoluene (p-Cymene)0.60 1.0 g/L SM21-22 6200BJ0.40
sec-Butylbenzene 1.6 1.0 g/L SM21-22 6200B0.32
Toluene 1.2 1.0 g/L SM21-22 6200B0.28
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 6 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method 6200B elevated reporting limits for samples 19K0437-03,05,06+08 due to high concentrations of target compounds.
[TOC_1]Case Narrative[TOC]
SM21-22 6200B
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not
affected since all results are "not detected" for associated samples in this batch and bias is on the high side.
Analyte & Samples(s) Qualified:
L-02
2-Hexanone (MBK)
B245494-BS1, B245494-BSD1
4-Methyl-2-pentanone (MIBK)
B245494-BS1, B245494-BSD1
Ethanol
B245494-BS1, B245494-BSD1
Vinyl Chloride
B245494-BS1, B245494-BSD1
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the high side.
Analyte & Samples(s) Qualified:
L-06
Acetone
19K0437-04[MW-4], B245494-BS1, B245494-BSD1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
tert-Amyl Methyl Ether (TAME)
B245494-BS1
tert-Butyl Alcohol (TBA)
B245494-BSD1
Elevated reporting limit due to high concentration of target compounds.
Analyte & Samples(s) Qualified:
RL-11
19K0437-03[MW-5], 19K0437-05[MW-3], 19K0437-06[MW-2], 19K0437-08[MW-2D]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 7 of 42
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-01
Field Sample #: field blank
Sample Matrix: Field Blank
Sampled: 11/5/2019 10:32
[TOC_2]19K0437-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/9/19 2:48 EEHg/L3.8 11/8/19SM21-22 6200B1Acetone
ND 0.50 11/9/19 2:48 EEHg/L0.18 11/8/19SM21-22 6200B1Benzene
ND 0.50 11/9/19 2:48 EEHg/L0.15 11/8/19SM21-22 6200B1Bromobenzene
ND 0.50 11/9/19 2:48 EEHg/L0.32 11/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/9/19 2:48 EEHg/L0.16 11/8/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/9/19 2:48 EEHg/L0.46 11/8/19SM21-22 6200B1Bromoform
ND 1.0 11/9/19 2:48 EEHg/L0.78 11/8/19SM21-22 6200B1Bromomethane
ND 5.0 11/9/19 2:48 EEHg/L1.9 11/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/9/19 2:48 EEHg/L0.21 11/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/9/19 2:48 EEHg/L0.16 11/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/9/19 2:48 EEHg/L0.17 11/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/9/19 2:48 EEHg/L0.11 11/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/9/19 2:48 EEHg/L0.15 11/8/19SM21-22 6200B1Chlorobenzene
ND 50 11/9/19 2:48 EEHg/L11 11/8/19SM21-22 6200B1Ethanol
ND 0.50 11/9/19 2:48 EEHg/L0.21 11/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/9/19 2:48 EEHg/L0.35 11/8/19SM21-22 6200B1Chloroethane
ND 0.50 11/9/19 2:48 EEHg/L0.17 11/8/19SM21-22 6200B1Chloroform
ND 1.0 11/9/19 2:48 EEHg/L0.45 11/8/19SM21-22 6200B1Chloromethane
ND 0.50 11/9/19 2:48 EEHg/L0.12 11/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/9/19 2:48 EEHg/L0.14 11/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/9/19 2:48 EEHg/L0.19 11/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/9/19 2:48 EEHg/L0.16 11/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/9/19 2:48 EEHg/L0.12 11/8/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/9/19 2:48 EEHg/L0.13 11/8/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/9/19 2:48 EEHg/L0.26 11/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/9/19 2:48 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/9/19 2:48 EEHg/L0.41 11/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/9/19 2:48 EEHg/L0.32 11/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/9/19 2:48 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/9/19 2:48 EEHg/L0.31 11/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/9/19 2:48 EEHg/L0.20 11/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/9/19 2:48 EEHg/L0.11 11/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/9/19 2:48 EEHg/L0.20 11/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/9/19 2:48 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/9/19 2:48 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/9/19 2:48 EEHg/L0.23 11/8/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/9/19 2:48 EEHg/L0.17 11/8/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/9/19 2:48 EEHg/L0.13 11/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/9/19 2:48 EEHg/L1.5 11/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/9/19 2:48 EEHg/L0.17 11/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/9/19 2:48 EEHg/L0.20 11/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/9/19 2:48 EEHg/L0.25 11/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
0.43 5.0 11/9/19 2:48 EEHg/L0.34 11/8/19SM21-22 6200B1JMethylene Chloride
ND 5.0 11/9/19 2:48 EEHg/L1.7 11/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
[TOC_1]Sample Results[TOC]
Page 8 of 42
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-01
Field Sample #: field blank
Sample Matrix: Field Blank
Sampled: 11/5/2019 10:32
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 11/9/19 2:48 EEHg/L0.31 11/8/19SM21-22 6200B1Naphthalene
ND 0.50 11/9/19 2:48 EEHg/L0.13 11/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/9/19 2:48 EEHg/L0.11 11/8/19SM21-22 6200B1Styrene
ND 0.50 11/9/19 2:48 EEHg/L0.22 11/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/9/19 2:48 EEHg/L0.18 11/8/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/9/19 2:48 EEHg/L0.14 11/8/19SM21-22 6200B1Toluene
ND 2.0 11/9/19 2:48 EEHg/L0.57 11/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/9/19 2:48 EEHg/L0.40 11/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/9/19 2:48 EEHg/L0.20 11/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/9/19 2:48 EEHg/L0.16 11/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/9/19 2:48 EEHg/L0.24 11/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/9/19 2:48 EEHg/L0.33 11/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/9/19 2:48 EEHg/L0.25 11/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/9/19 2:48 EEHg/L0.18 11/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/9/19 2:48 EEHg/L0.14 11/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/9/19 2:48 EEHg/L10 11/8/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/9/19 2:48 EEHg/L0.45 11/8/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/9/19 2:48 EEHg/L0.30 11/8/19SM21-22 6200B1m+p Xylene
ND 0.50 11/9/19 2:48 EEHg/L0.17 11/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 107 11/9/19 2:4870-130
Toluene-d8 101 11/9/19 2:4870-130
4-Bromofluorobenzene 92.8 11/9/19 2:4870-130
Page 9 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-02
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 11/5/2019 10:40
[TOC_2]19K0437-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/9/19 3:45 EEHg/L3.8 11/8/19SM21-22 6200B1Acetone
ND 0.50 11/9/19 3:45 EEHg/L0.18 11/8/19SM21-22 6200B1Benzene
ND 0.50 11/9/19 3:45 EEHg/L0.15 11/8/19SM21-22 6200B1Bromobenzene
ND 0.50 11/9/19 3:45 EEHg/L0.32 11/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/9/19 3:45 EEHg/L0.16 11/8/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/9/19 3:45 EEHg/L0.46 11/8/19SM21-22 6200B1Bromoform
ND 1.0 11/9/19 3:45 EEHg/L0.78 11/8/19SM21-22 6200B1Bromomethane
ND 5.0 11/9/19 3:45 EEHg/L1.9 11/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/9/19 3:45 EEHg/L0.21 11/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/9/19 3:45 EEHg/L0.16 11/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/9/19 3:45 EEHg/L0.17 11/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/9/19 3:45 EEHg/L0.11 11/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/9/19 3:45 EEHg/L0.15 11/8/19SM21-22 6200B1Chlorobenzene
ND 50 11/9/19 3:45 EEHg/L11 11/8/19SM21-22 6200B1Ethanol
ND 0.50 11/9/19 3:45 EEHg/L0.21 11/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/9/19 3:45 EEHg/L0.35 11/8/19SM21-22 6200B1Chloroethane
ND 0.50 11/9/19 3:45 EEHg/L0.17 11/8/19SM21-22 6200B1Chloroform
ND 1.0 11/9/19 3:45 EEHg/L0.45 11/8/19SM21-22 6200B1Chloromethane
ND 0.50 11/9/19 3:45 EEHg/L0.12 11/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/9/19 3:45 EEHg/L0.14 11/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/9/19 3:45 EEHg/L0.19 11/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/9/19 3:45 EEHg/L0.16 11/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/9/19 3:45 EEHg/L0.12 11/8/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/9/19 3:45 EEHg/L0.13 11/8/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/9/19 3:45 EEHg/L0.26 11/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/9/19 3:45 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/9/19 3:45 EEHg/L0.41 11/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/9/19 3:45 EEHg/L0.32 11/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/9/19 3:45 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/9/19 3:45 EEHg/L0.31 11/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/9/19 3:45 EEHg/L0.20 11/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/9/19 3:45 EEHg/L0.11 11/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/9/19 3:45 EEHg/L0.20 11/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/9/19 3:45 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/9/19 3:45 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/9/19 3:45 EEHg/L0.23 11/8/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/9/19 3:45 EEHg/L0.17 11/8/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/9/19 3:45 EEHg/L0.13 11/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/9/19 3:45 EEHg/L1.5 11/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/9/19 3:45 EEHg/L0.17 11/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/9/19 3:45 EEHg/L0.20 11/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/9/19 3:45 EEHg/L0.25 11/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/9/19 3:45 EEHg/L0.34 11/8/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/9/19 3:45 EEHg/L1.7 11/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 10 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-02
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 11/5/2019 10:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 11/9/19 3:45 EEHg/L0.31 11/8/19SM21-22 6200B1Naphthalene
ND 0.50 11/9/19 3:45 EEHg/L0.13 11/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/9/19 3:45 EEHg/L0.11 11/8/19SM21-22 6200B1Styrene
ND 0.50 11/9/19 3:45 EEHg/L0.22 11/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/9/19 3:45 EEHg/L0.18 11/8/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/9/19 3:45 EEHg/L0.14 11/8/19SM21-22 6200B1Toluene
ND 2.0 11/9/19 3:45 EEHg/L0.57 11/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/9/19 3:45 EEHg/L0.40 11/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/9/19 3:45 EEHg/L0.20 11/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/9/19 3:45 EEHg/L0.16 11/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/9/19 3:45 EEHg/L0.24 11/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/9/19 3:45 EEHg/L0.33 11/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/9/19 3:45 EEHg/L0.25 11/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/9/19 3:45 EEHg/L0.18 11/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/9/19 3:45 EEHg/L0.14 11/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/9/19 3:45 EEHg/L10 11/8/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/9/19 3:45 EEHg/L0.45 11/8/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/9/19 3:45 EEHg/L0.30 11/8/19SM21-22 6200B1m+p Xylene
ND 0.50 11/9/19 3:45 EEHg/L0.17 11/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 108 11/9/19 3:4570-130
Toluene-d8 101 11/9/19 3:4570-130
4-Bromofluorobenzene 95.9 11/9/19 3:4570-130
Page 11 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-03
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 11/5/2019 10:52
[TOC_2]19K0437-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 1000 11/9/19 10:00 EEHg/L76 11/8/19SM21-22 6200B20Acetone
ND 10 11/9/19 10:00 EEHg/L3.6 11/8/19SM21-22 6200B20Benzene
ND 10 11/9/19 10:00 EEHg/L3.0 11/8/19SM21-22 6200B20Bromobenzene
ND 10 11/9/19 10:00 EEHg/L6.4 11/8/19SM21-22 6200B20Bromochloromethane
ND 10 11/9/19 10:00 EEHg/L3.2 11/8/19SM21-22 6200B20Bromodichloromethane
ND 10 11/9/19 10:00 EEHg/L9.2 11/8/19SM21-22 6200B20Bromoform
ND 20 11/9/19 10:00 EEHg/L16 11/8/19SM21-22 6200B20Bromomethane
66 100 11/9/19 10:00 EEHg/L39 11/8/19SM21-22 6200B20J2-Butanone (MEK)
9.6 10 11/9/19 10:00 EEHg/L4.2 11/8/19SM21-22 6200B20Jn-Butylbenzene
7.0 10 11/9/19 10:00 EEHg/L3.2 11/8/19SM21-22 6200B20Jsec-Butylbenzene
ND 10 11/9/19 10:00 EEHg/L3.4 11/8/19SM21-22 6200B20tert-Butylbenzene
ND 10 11/9/19 10:00 EEHg/L2.2 11/8/19SM21-22 6200B20Carbon Tetrachloride
ND 10 11/9/19 10:00 EEHg/L3.0 11/8/19SM21-22 6200B20Chlorobenzene
ND 1000 11/9/19 10:00 EEHg/L210 11/8/19SM21-22 6200B20Ethanol
ND 10 11/9/19 10:00 EEHg/L4.2 11/8/19SM21-22 6200B20Chlorodibromomethane
ND 10 11/9/19 10:00 EEHg/L7.0 11/8/19SM21-22 6200B20Chloroethane
ND 10 11/9/19 10:00 EEHg/L3.4 11/8/19SM21-22 6200B20Chloroform
ND 20 11/9/19 10:00 EEHg/L9.0 11/8/19SM21-22 6200B20Chloromethane
ND 10 11/9/19 10:00 EEHg/L2.4 11/8/19SM21-22 6200B202-Chlorotoluene
ND 10 11/9/19 10:00 EEHg/L2.8 11/8/19SM21-22 6200B204-Chlorotoluene
ND 10 11/9/19 10:00 EEHg/L3.8 11/8/19SM21-22 6200B201,2-Dibromoethane (EDB)
ND 10 11/9/19 10:00 EEHg/L3.2 11/8/19SM21-22 6200B201,2-Dichlorobenzene
ND 10 11/9/19 10:00 EEHg/L2.4 11/8/19SM21-22 6200B201,3-Dichlorobenzene
ND 10 11/9/19 10:00 EEHg/L2.6 11/8/19SM21-22 6200B201,4-Dichlorobenzene
ND 10 11/9/19 10:00 EEHg/L5.2 11/8/19SM21-22 6200B20Dichlorodifluoromethane (Freon 12)
ND 10 11/9/19 10:00 EEHg/L3.2 11/8/19SM21-22 6200B201,1-Dichloroethane
ND 20 11/9/19 10:00 EEHg/L8.2 11/8/19SM21-22 6200B201,2-Dichloroethane
ND 10 11/9/19 10:00 EEHg/L6.4 11/8/19SM21-22 6200B201,1-Dichloroethylene
ND 10 11/9/19 10:00 EEHg/L2.6 11/8/19SM21-22 6200B20cis-1,2-Dichloroethylene
ND 10 11/9/19 10:00 EEHg/L6.2 11/8/19SM21-22 6200B20trans-1,2-Dichloroethylene
ND 10 11/9/19 10:00 EEHg/L4.0 11/8/19SM21-22 6200B201,2-Dichloropropane
ND 10 11/9/19 10:00 EEHg/L2.2 11/8/19SM21-22 6200B201,3-Dichloropropane
ND 10 11/9/19 10:00 EEHg/L4.0 11/8/19SM21-22 6200B202,2-Dichloropropane
ND 10 11/9/19 10:00 EEHg/L3.2 11/8/19SM21-22 6200B201,1-Dichloropropene
ND 10 11/9/19 10:00 EEHg/L2.6 11/8/19SM21-22 6200B20cis-1,3-Dichloropropene
ND 10 11/9/19 10:00 EEHg/L4.6 11/8/19SM21-22 6200B20trans-1,3-Dichloropropene
ND 10 11/9/19 10:00 EEHg/L3.4 11/8/19SM21-22 6200B20Diisopropyl Ether (DIPE)
1900 10 11/9/19 10:00 EEHg/L2.6 11/8/19SM21-22 6200B20Ethylbenzene
ND 100 11/9/19 10:00 EEHg/L30 11/8/19SM21-22 6200B202-Hexanone (MBK)
60 10 11/9/19 10:00 EEHg/L3.4 11/8/19SM21-22 6200B20Isopropylbenzene (Cumene)
ND 10 11/9/19 10:00 EEHg/L4.0 11/8/19SM21-22 6200B20p-Isopropyltoluene (p-Cymene)
ND 10 11/9/19 10:00 EEHg/L5.0 11/8/19SM21-22 6200B20Methyl tert-Butyl Ether (MTBE)
ND 100 11/9/19 10:00 EEHg/L6.8 11/8/19SM21-22 6200B20Methylene Chloride
ND 100 11/9/19 10:00 EEHg/L33 11/8/19SM21-22 6200B204-Methyl-2-pentanone (MIBK)
Page 12 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-03
Field Sample #: MW-5
Sample Matrix: Ground Water
Sampled: 11/5/2019 10:52
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
310 100 11/9/19 10:00 EEHg/L6.2 11/8/19SM21-22 6200B20Naphthalene
140 10 11/9/19 10:00 EEHg/L2.6 11/8/19SM21-22 6200B20n-Propylbenzene
9.6 10 11/9/19 10:00 EEHg/L2.2 11/8/19SM21-22 6200B20JStyrene
ND 10 11/9/19 10:00 EEHg/L4.4 11/8/19SM21-22 6200B201,1,2,2-Tetrachloroethane
ND 10 11/9/19 10:00 EEHg/L3.6 11/8/19SM21-22 6200B20Tetrachloroethylene
440 10 11/9/19 10:00 EEHg/L2.8 11/8/19SM21-22 6200B20Toluene
ND 40 11/9/19 10:00 EEHg/L11 11/8/19SM21-22 6200B201,2,3-Trichlorobenzene
ND 10 11/9/19 10:00 EEHg/L8.0 11/8/19SM21-22 6200B201,2,4-Trichlorobenzene
ND 10 11/9/19 10:00 EEHg/L4.0 11/8/19SM21-22 6200B201,1,1-Trichloroethane
ND 10 11/9/19 10:00 EEHg/L3.2 11/8/19SM21-22 6200B201,1,2-Trichloroethane
ND 10 11/9/19 10:00 EEHg/L4.8 11/8/19SM21-22 6200B20Trichloroethylene
ND 10 11/9/19 10:00 EEHg/L6.6 11/8/19SM21-22 6200B20Trichlorofluoromethane (Freon 11)
ND 10 11/9/19 10:00 EEHg/L5.0 11/8/19SM21-22 6200B201,2,3-Trichloropropane
1000 10 11/9/19 10:00 EEHg/L3.6 11/8/19SM21-22 6200B201,2,4-Trimethylbenzene
240 10 11/9/19 10:00 EEHg/L2.8 11/8/19SM21-22 6200B201,3,5-Trimethylbenzene
ND 400 11/9/19 10:00 EEHg/L200 11/8/19SM21-22 6200B20Vinyl Acetate
ND 10 11/9/19 10:00 EEHg/L9.0 11/8/19SM21-22 6200B20Vinyl Chloride
6000 20 11/9/19 10:00 EEHg/L6.0 11/8/19SM21-22 6200B20m+p Xylene
3400 10 11/9/19 10:00 EEHg/L3.4 11/8/19SM21-22 6200B20o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 111 11/9/19 10:0070-130
Toluene-d8 102 11/9/19 10:0070-130
4-Bromofluorobenzene 95.1 11/9/19 10:0070-130
Page 13 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-04
Field Sample #: MW-4
Sample Matrix: Ground Water
Sampled: 11/5/2019 11:02
[TOC_2]19K0437-04[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
17 50 11/9/19 4:14 EEHg/L3.8 11/8/19SM21-22 6200B1L-06, JAcetone
ND 0.50 11/9/19 4:14 EEHg/L0.18 11/8/19SM21-22 6200B1Benzene
ND 0.50 11/9/19 4:14 EEHg/L0.15 11/8/19SM21-22 6200B1Bromobenzene
ND 0.50 11/9/19 4:14 EEHg/L0.32 11/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/9/19 4:14 EEHg/L0.16 11/8/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/9/19 4:14 EEHg/L0.46 11/8/19SM21-22 6200B1Bromoform
ND 1.0 11/9/19 4:14 EEHg/L0.78 11/8/19SM21-22 6200B1Bromomethane
ND 5.0 11/9/19 4:14 EEHg/L1.9 11/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/9/19 4:14 EEHg/L0.21 11/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/9/19 4:14 EEHg/L0.16 11/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/9/19 4:14 EEHg/L0.17 11/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/9/19 4:14 EEHg/L0.11 11/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/9/19 4:14 EEHg/L0.15 11/8/19SM21-22 6200B1Chlorobenzene
ND 50 11/9/19 4:14 EEHg/L11 11/8/19SM21-22 6200B1Ethanol
ND 0.50 11/9/19 4:14 EEHg/L0.21 11/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/9/19 4:14 EEHg/L0.35 11/8/19SM21-22 6200B1Chloroethane
ND 0.50 11/9/19 4:14 EEHg/L0.17 11/8/19SM21-22 6200B1Chloroform
ND 1.0 11/9/19 4:14 EEHg/L0.45 11/8/19SM21-22 6200B1Chloromethane
ND 0.50 11/9/19 4:14 EEHg/L0.12 11/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/9/19 4:14 EEHg/L0.14 11/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/9/19 4:14 EEHg/L0.19 11/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/9/19 4:14 EEHg/L0.16 11/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/9/19 4:14 EEHg/L0.12 11/8/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/9/19 4:14 EEHg/L0.13 11/8/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/9/19 4:14 EEHg/L0.26 11/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/9/19 4:14 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/9/19 4:14 EEHg/L0.41 11/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/9/19 4:14 EEHg/L0.32 11/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/9/19 4:14 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/9/19 4:14 EEHg/L0.31 11/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/9/19 4:14 EEHg/L0.20 11/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/9/19 4:14 EEHg/L0.11 11/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/9/19 4:14 EEHg/L0.20 11/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/9/19 4:14 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/9/19 4:14 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/9/19 4:14 EEHg/L0.23 11/8/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/9/19 4:14 EEHg/L0.17 11/8/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/9/19 4:14 EEHg/L0.13 11/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/9/19 4:14 EEHg/L1.5 11/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/9/19 4:14 EEHg/L0.17 11/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/9/19 4:14 EEHg/L0.20 11/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/9/19 4:14 EEHg/L0.25 11/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/9/19 4:14 EEHg/L0.34 11/8/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/9/19 4:14 EEHg/L1.7 11/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 14 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-04
Field Sample #: MW-4
Sample Matrix: Ground Water
Sampled: 11/5/2019 11:02
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 11/9/19 4:14 EEHg/L0.31 11/8/19SM21-22 6200B1Naphthalene
ND 0.50 11/9/19 4:14 EEHg/L0.13 11/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/9/19 4:14 EEHg/L0.11 11/8/19SM21-22 6200B1Styrene
ND 0.50 11/9/19 4:14 EEHg/L0.22 11/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/9/19 4:14 EEHg/L0.18 11/8/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/9/19 4:14 EEHg/L0.14 11/8/19SM21-22 6200B1Toluene
ND 2.0 11/9/19 4:14 EEHg/L0.57 11/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/9/19 4:14 EEHg/L0.40 11/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/9/19 4:14 EEHg/L0.20 11/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/9/19 4:14 EEHg/L0.16 11/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/9/19 4:14 EEHg/L0.24 11/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/9/19 4:14 EEHg/L0.33 11/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/9/19 4:14 EEHg/L0.25 11/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/9/19 4:14 EEHg/L0.18 11/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/9/19 4:14 EEHg/L0.14 11/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/9/19 4:14 EEHg/L10 11/8/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/9/19 4:14 EEHg/L0.45 11/8/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/9/19 4:14 EEHg/L0.30 11/8/19SM21-22 6200B1m+p Xylene
ND 0.50 11/9/19 4:14 EEHg/L0.17 11/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 106 11/9/19 4:1470-130
Toluene-d8 100 11/9/19 4:1470-130
4-Bromofluorobenzene 94.6 11/9/19 4:1470-130
Page 15 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-05
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 11/5/2019 11:13
[TOC_2]19K0437-05[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 5000 11/9/19 10:28 EEHg/L380 11/8/19SM21-22 6200B100Acetone
ND 50 11/9/19 10:28 EEHg/L18 11/8/19SM21-22 6200B100Benzene
ND 50 11/9/19 10:28 EEHg/L15 11/8/19SM21-22 6200B100Bromobenzene
ND 50 11/9/19 10:28 EEHg/L32 11/8/19SM21-22 6200B100Bromochloromethane
ND 50 11/9/19 10:28 EEHg/L16 11/8/19SM21-22 6200B100Bromodichloromethane
ND 50 11/9/19 10:28 EEHg/L46 11/8/19SM21-22 6200B100Bromoform
ND 100 11/9/19 10:28 EEHg/L78 11/8/19SM21-22 6200B100Bromomethane
ND 500 11/9/19 10:28 EEHg/L190 11/8/19SM21-22 6200B1002-Butanone (MEK)
40 50 11/9/19 10:28 EEHg/L21 11/8/19SM21-22 6200B100Jn-Butylbenzene
27 50 11/9/19 10:28 EEHg/L16 11/8/19SM21-22 6200B100Jsec-Butylbenzene
ND 50 11/9/19 10:28 EEHg/L17 11/8/19SM21-22 6200B100tert-Butylbenzene
ND 50 11/9/19 10:28 EEHg/L11 11/8/19SM21-22 6200B100Carbon Tetrachloride
ND 50 11/9/19 10:28 EEHg/L15 11/8/19SM21-22 6200B100Chlorobenzene
ND 5000 11/9/19 10:28 EEHg/L1100 11/8/19SM21-22 6200B100Ethanol
ND 50 11/9/19 10:28 EEHg/L21 11/8/19SM21-22 6200B100Chlorodibromomethane
ND 50 11/9/19 10:28 EEHg/L35 11/8/19SM21-22 6200B100Chloroethane
ND 50 11/9/19 10:28 EEHg/L17 11/8/19SM21-22 6200B100Chloroform
ND 100 11/9/19 10:28 EEHg/L45 11/8/19SM21-22 6200B100Chloromethane
ND 50 11/9/19 10:28 EEHg/L12 11/8/19SM21-22 6200B1002-Chlorotoluene
ND 50 11/9/19 10:28 EEHg/L14 11/8/19SM21-22 6200B1004-Chlorotoluene
ND 50 11/9/19 10:28 EEHg/L19 11/8/19SM21-22 6200B1001,2-Dibromoethane (EDB)
ND 50 11/9/19 10:28 EEHg/L16 11/8/19SM21-22 6200B1001,2-Dichlorobenzene
ND 50 11/9/19 10:28 EEHg/L12 11/8/19SM21-22 6200B1001,3-Dichlorobenzene
ND 50 11/9/19 10:28 EEHg/L13 11/8/19SM21-22 6200B1001,4-Dichlorobenzene
ND 50 11/9/19 10:28 EEHg/L26 11/8/19SM21-22 6200B100Dichlorodifluoromethane (Freon 12)
ND 50 11/9/19 10:28 EEHg/L16 11/8/19SM21-22 6200B1001,1-Dichloroethane
ND 100 11/9/19 10:28 EEHg/L41 11/8/19SM21-22 6200B1001,2-Dichloroethane
ND 50 11/9/19 10:28 EEHg/L32 11/8/19SM21-22 6200B1001,1-Dichloroethylene
ND 50 11/9/19 10:28 EEHg/L13 11/8/19SM21-22 6200B100cis-1,2-Dichloroethylene
ND 50 11/9/19 10:28 EEHg/L31 11/8/19SM21-22 6200B100trans-1,2-Dichloroethylene
ND 50 11/9/19 10:28 EEHg/L20 11/8/19SM21-22 6200B1001,2-Dichloropropane
ND 50 11/9/19 10:28 EEHg/L11 11/8/19SM21-22 6200B1001,3-Dichloropropane
ND 50 11/9/19 10:28 EEHg/L20 11/8/19SM21-22 6200B1002,2-Dichloropropane
ND 50 11/9/19 10:28 EEHg/L16 11/8/19SM21-22 6200B1001,1-Dichloropropene
ND 50 11/9/19 10:28 EEHg/L13 11/8/19SM21-22 6200B100cis-1,3-Dichloropropene
ND 50 11/9/19 10:28 EEHg/L23 11/8/19SM21-22 6200B100trans-1,3-Dichloropropene
ND 50 11/9/19 10:28 EEHg/L17 11/8/19SM21-22 6200B100Diisopropyl Ether (DIPE)
900 50 11/9/19 10:28 EEHg/L13 11/8/19SM21-22 6200B100Ethylbenzene
ND 500 11/9/19 10:28 EEHg/L150 11/8/19SM21-22 6200B1002-Hexanone (MBK)
68 50 11/9/19 10:28 EEHg/L17 11/8/19SM21-22 6200B100Isopropylbenzene (Cumene)
ND 50 11/9/19 10:28 EEHg/L20 11/8/19SM21-22 6200B100p-Isopropyltoluene (p-Cymene)
ND 50 11/9/19 10:28 EEHg/L25 11/8/19SM21-22 6200B100Methyl tert-Butyl Ether (MTBE)
ND 500 11/9/19 10:28 EEHg/L34 11/8/19SM21-22 6200B100Methylene Chloride
ND 500 11/9/19 10:28 EEHg/L170 11/8/19SM21-22 6200B1004-Methyl-2-pentanone (MIBK)
Page 16 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-05
Field Sample #: MW-3
Sample Matrix: Ground Water
Sampled: 11/5/2019 11:13
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
730 500 11/9/19 10:28 EEHg/L31 11/8/19SM21-22 6200B100Naphthalene
220 50 11/9/19 10:28 EEHg/L13 11/8/19SM21-22 6200B100n-Propylbenzene
ND 50 11/9/19 10:28 EEHg/L11 11/8/19SM21-22 6200B100Styrene
ND 50 11/9/19 10:28 EEHg/L22 11/8/19SM21-22 6200B1001,1,2,2-Tetrachloroethane
ND 50 11/9/19 10:28 EEHg/L18 11/8/19SM21-22 6200B100Tetrachloroethylene
1000 50 11/9/19 10:28 EEHg/L14 11/8/19SM21-22 6200B100Toluene
ND 200 11/9/19 10:28 EEHg/L57 11/8/19SM21-22 6200B1001,2,3-Trichlorobenzene
ND 50 11/9/19 10:28 EEHg/L40 11/8/19SM21-22 6200B1001,2,4-Trichlorobenzene
ND 50 11/9/19 10:28 EEHg/L20 11/8/19SM21-22 6200B1001,1,1-Trichloroethane
ND 50 11/9/19 10:28 EEHg/L16 11/8/19SM21-22 6200B1001,1,2-Trichloroethane
ND 50 11/9/19 10:28 EEHg/L24 11/8/19SM21-22 6200B100Trichloroethylene
ND 50 11/9/19 10:28 EEHg/L33 11/8/19SM21-22 6200B100Trichlorofluoromethane (Freon 11)
ND 50 11/9/19 10:28 EEHg/L25 11/8/19SM21-22 6200B1001,2,3-Trichloropropane
1400 50 11/9/19 10:28 EEHg/L18 11/8/19SM21-22 6200B1001,2,4-Trimethylbenzene
370 50 11/9/19 10:28 EEHg/L14 11/8/19SM21-22 6200B1001,3,5-Trimethylbenzene
ND 2000 11/9/19 10:28 EEHg/L1000 11/8/19SM21-22 6200B100Vinyl Acetate
ND 50 11/9/19 10:28 EEHg/L45 11/8/19SM21-22 6200B100Vinyl Chloride
3100 100 11/9/19 10:28 EEHg/L30 11/8/19SM21-22 6200B100m+p Xylene
1400 50 11/9/19 10:28 EEHg/L17 11/8/19SM21-22 6200B100o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 109 11/9/19 10:2870-130
Toluene-d8 99.5 11/9/19 10:2870-130
4-Bromofluorobenzene 93.3 11/9/19 10:2870-130
Page 17 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-06
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 11/5/2019 11:23
[TOC_2]19K0437-06[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 1000 11/9/19 10:57 EEHg/L76 11/8/19SM21-22 6200B20Acetone
ND 10 11/9/19 10:57 EEHg/L3.6 11/8/19SM21-22 6200B20Benzene
ND 10 11/9/19 10:57 EEHg/L3.0 11/8/19SM21-22 6200B20Bromobenzene
ND 10 11/9/19 10:57 EEHg/L6.4 11/8/19SM21-22 6200B20Bromochloromethane
ND 10 11/9/19 10:57 EEHg/L3.2 11/8/19SM21-22 6200B20Bromodichloromethane
ND 10 11/9/19 10:57 EEHg/L9.2 11/8/19SM21-22 6200B20Bromoform
ND 20 11/9/19 10:57 EEHg/L16 11/8/19SM21-22 6200B20Bromomethane
60 100 11/9/19 10:57 EEHg/L39 11/8/19SM21-22 6200B20J2-Butanone (MEK)
11 10 11/9/19 10:57 EEHg/L4.2 11/8/19SM21-22 6200B20n-Butylbenzene
6.4 10 11/9/19 10:57 EEHg/L3.2 11/8/19SM21-22 6200B20Jsec-Butylbenzene
ND 10 11/9/19 10:57 EEHg/L3.4 11/8/19SM21-22 6200B20tert-Butylbenzene
ND 10 11/9/19 10:57 EEHg/L2.2 11/8/19SM21-22 6200B20Carbon Tetrachloride
ND 10 11/9/19 10:57 EEHg/L3.0 11/8/19SM21-22 6200B20Chlorobenzene
ND 1000 11/9/19 10:57 EEHg/L210 11/8/19SM21-22 6200B20Ethanol
ND 10 11/9/19 10:57 EEHg/L4.2 11/8/19SM21-22 6200B20Chlorodibromomethane
ND 10 11/9/19 10:57 EEHg/L7.0 11/8/19SM21-22 6200B20Chloroethane
ND 10 11/9/19 10:57 EEHg/L3.4 11/8/19SM21-22 6200B20Chloroform
ND 20 11/9/19 10:57 EEHg/L9.0 11/8/19SM21-22 6200B20Chloromethane
ND 10 11/9/19 10:57 EEHg/L2.4 11/8/19SM21-22 6200B202-Chlorotoluene
ND 10 11/9/19 10:57 EEHg/L2.8 11/8/19SM21-22 6200B204-Chlorotoluene
ND 10 11/9/19 10:57 EEHg/L3.8 11/8/19SM21-22 6200B201,2-Dibromoethane (EDB)
ND 10 11/9/19 10:57 EEHg/L3.2 11/8/19SM21-22 6200B201,2-Dichlorobenzene
ND 10 11/9/19 10:57 EEHg/L2.4 11/8/19SM21-22 6200B201,3-Dichlorobenzene
ND 10 11/9/19 10:57 EEHg/L2.6 11/8/19SM21-22 6200B201,4-Dichlorobenzene
ND 10 11/9/19 10:57 EEHg/L5.2 11/8/19SM21-22 6200B20Dichlorodifluoromethane (Freon 12)
ND 10 11/9/19 10:57 EEHg/L3.2 11/8/19SM21-22 6200B201,1-Dichloroethane
ND 20 11/9/19 10:57 EEHg/L8.2 11/8/19SM21-22 6200B201,2-Dichloroethane
ND 10 11/9/19 10:57 EEHg/L6.4 11/8/19SM21-22 6200B201,1-Dichloroethylene
ND 10 11/9/19 10:57 EEHg/L2.6 11/8/19SM21-22 6200B20cis-1,2-Dichloroethylene
ND 10 11/9/19 10:57 EEHg/L6.2 11/8/19SM21-22 6200B20trans-1,2-Dichloroethylene
ND 10 11/9/19 10:57 EEHg/L4.0 11/8/19SM21-22 6200B201,2-Dichloropropane
ND 10 11/9/19 10:57 EEHg/L2.2 11/8/19SM21-22 6200B201,3-Dichloropropane
ND 10 11/9/19 10:57 EEHg/L4.0 11/8/19SM21-22 6200B202,2-Dichloropropane
ND 10 11/9/19 10:57 EEHg/L3.2 11/8/19SM21-22 6200B201,1-Dichloropropene
ND 10 11/9/19 10:57 EEHg/L2.6 11/8/19SM21-22 6200B20cis-1,3-Dichloropropene
ND 10 11/9/19 10:57 EEHg/L4.6 11/8/19SM21-22 6200B20trans-1,3-Dichloropropene
ND 10 11/9/19 10:57 EEHg/L3.4 11/8/19SM21-22 6200B20Diisopropyl Ether (DIPE)
360 10 11/9/19 10:57 EEHg/L2.6 11/8/19SM21-22 6200B20Ethylbenzene
ND 100 11/9/19 10:57 EEHg/L30 11/8/19SM21-22 6200B202-Hexanone (MBK)
30 10 11/9/19 10:57 EEHg/L3.4 11/8/19SM21-22 6200B20Isopropylbenzene (Cumene)
ND 10 11/9/19 10:57 EEHg/L4.0 11/8/19SM21-22 6200B20p-Isopropyltoluene (p-Cymene)
ND 10 11/9/19 10:57 EEHg/L5.0 11/8/19SM21-22 6200B20Methyl tert-Butyl Ether (MTBE)
ND 100 11/9/19 10:57 EEHg/L6.8 11/8/19SM21-22 6200B20Methylene Chloride
ND 100 11/9/19 10:57 EEHg/L33 11/8/19SM21-22 6200B204-Methyl-2-pentanone (MIBK)
Page 18 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-06
Field Sample #: MW-2
Sample Matrix: Ground Water
Sampled: 11/5/2019 11:23
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
160 100 11/9/19 10:57 EEHg/L6.2 11/8/19SM21-22 6200B20Naphthalene
83 10 11/9/19 10:57 EEHg/L2.6 11/8/19SM21-22 6200B20n-Propylbenzene
ND 10 11/9/19 10:57 EEHg/L2.2 11/8/19SM21-22 6200B20Styrene
ND 10 11/9/19 10:57 EEHg/L4.4 11/8/19SM21-22 6200B201,1,2,2-Tetrachloroethane
ND 10 11/9/19 10:57 EEHg/L3.6 11/8/19SM21-22 6200B20Tetrachloroethylene
440 10 11/9/19 10:57 EEHg/L2.8 11/8/19SM21-22 6200B20Toluene
ND 40 11/9/19 10:57 EEHg/L11 11/8/19SM21-22 6200B201,2,3-Trichlorobenzene
ND 10 11/9/19 10:57 EEHg/L8.0 11/8/19SM21-22 6200B201,2,4-Trichlorobenzene
ND 10 11/9/19 10:57 EEHg/L4.0 11/8/19SM21-22 6200B201,1,1-Trichloroethane
ND 10 11/9/19 10:57 EEHg/L3.2 11/8/19SM21-22 6200B201,1,2-Trichloroethane
ND 10 11/9/19 10:57 EEHg/L4.8 11/8/19SM21-22 6200B20Trichloroethylene
ND 10 11/9/19 10:57 EEHg/L6.6 11/8/19SM21-22 6200B20Trichlorofluoromethane (Freon 11)
ND 10 11/9/19 10:57 EEHg/L5.0 11/8/19SM21-22 6200B201,2,3-Trichloropropane
410 10 11/9/19 10:57 EEHg/L3.6 11/8/19SM21-22 6200B201,2,4-Trimethylbenzene
95 10 11/9/19 10:57 EEHg/L2.8 11/8/19SM21-22 6200B201,3,5-Trimethylbenzene
ND 400 11/9/19 10:57 EEHg/L200 11/8/19SM21-22 6200B20Vinyl Acetate
ND 10 11/9/19 10:57 EEHg/L9.0 11/8/19SM21-22 6200B20Vinyl Chloride
1100 20 11/9/19 10:57 EEHg/L6.0 11/8/19SM21-22 6200B20m+p Xylene
580 10 11/9/19 10:57 EEHg/L3.4 11/8/19SM21-22 6200B20o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 113 11/9/19 10:5770-130
Toluene-d8 100 11/9/19 10:5770-130
4-Bromofluorobenzene 96.8 11/9/19 10:5770-130
Page 19 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-07
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 11/5/2019 11:32
[TOC_2]19K0437-07[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/9/19 4:43 EEHg/L3.8 11/8/19SM21-22 6200B1Acetone
ND 0.50 11/9/19 4:43 EEHg/L0.18 11/8/19SM21-22 6200B1Benzene
ND 0.50 11/9/19 4:43 EEHg/L0.15 11/8/19SM21-22 6200B1Bromobenzene
ND 0.50 11/9/19 4:43 EEHg/L0.32 11/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/9/19 4:43 EEHg/L0.16 11/8/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/9/19 4:43 EEHg/L0.46 11/8/19SM21-22 6200B1Bromoform
ND 1.0 11/9/19 4:43 EEHg/L0.78 11/8/19SM21-22 6200B1Bromomethane
ND 5.0 11/9/19 4:43 EEHg/L1.9 11/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/9/19 4:43 EEHg/L0.21 11/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/9/19 4:43 EEHg/L0.16 11/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/9/19 4:43 EEHg/L0.17 11/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/9/19 4:43 EEHg/L0.11 11/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/9/19 4:43 EEHg/L0.15 11/8/19SM21-22 6200B1Chlorobenzene
ND 50 11/9/19 4:43 EEHg/L11 11/8/19SM21-22 6200B1Ethanol
ND 0.50 11/9/19 4:43 EEHg/L0.21 11/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/9/19 4:43 EEHg/L0.35 11/8/19SM21-22 6200B1Chloroethane
ND 0.50 11/9/19 4:43 EEHg/L0.17 11/8/19SM21-22 6200B1Chloroform
ND 1.0 11/9/19 4:43 EEHg/L0.45 11/8/19SM21-22 6200B1Chloromethane
ND 0.50 11/9/19 4:43 EEHg/L0.12 11/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/9/19 4:43 EEHg/L0.14 11/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/9/19 4:43 EEHg/L0.19 11/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/9/19 4:43 EEHg/L0.16 11/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/9/19 4:43 EEHg/L0.12 11/8/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/9/19 4:43 EEHg/L0.13 11/8/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/9/19 4:43 EEHg/L0.26 11/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/9/19 4:43 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/9/19 4:43 EEHg/L0.41 11/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/9/19 4:43 EEHg/L0.32 11/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/9/19 4:43 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/9/19 4:43 EEHg/L0.31 11/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/9/19 4:43 EEHg/L0.20 11/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/9/19 4:43 EEHg/L0.11 11/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/9/19 4:43 EEHg/L0.20 11/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/9/19 4:43 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/9/19 4:43 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/9/19 4:43 EEHg/L0.23 11/8/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/9/19 4:43 EEHg/L0.17 11/8/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/9/19 4:43 EEHg/L0.13 11/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/9/19 4:43 EEHg/L1.5 11/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/9/19 4:43 EEHg/L0.17 11/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/9/19 4:43 EEHg/L0.20 11/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/9/19 4:43 EEHg/L0.25 11/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/9/19 4:43 EEHg/L0.34 11/8/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/9/19 4:43 EEHg/L1.7 11/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 20 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-07
Field Sample #: MW-1
Sample Matrix: Ground Water
Sampled: 11/5/2019 11:32
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 11/9/19 4:43 EEHg/L0.31 11/8/19SM21-22 6200B1Naphthalene
ND 0.50 11/9/19 4:43 EEHg/L0.13 11/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/9/19 4:43 EEHg/L0.11 11/8/19SM21-22 6200B1Styrene
ND 0.50 11/9/19 4:43 EEHg/L0.22 11/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/9/19 4:43 EEHg/L0.18 11/8/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/9/19 4:43 EEHg/L0.14 11/8/19SM21-22 6200B1Toluene
ND 2.0 11/9/19 4:43 EEHg/L0.57 11/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/9/19 4:43 EEHg/L0.40 11/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/9/19 4:43 EEHg/L0.20 11/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/9/19 4:43 EEHg/L0.16 11/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/9/19 4:43 EEHg/L0.24 11/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/9/19 4:43 EEHg/L0.33 11/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/9/19 4:43 EEHg/L0.25 11/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/9/19 4:43 EEHg/L0.18 11/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/9/19 4:43 EEHg/L0.14 11/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/9/19 4:43 EEHg/L10 11/8/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/9/19 4:43 EEHg/L0.45 11/8/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/9/19 4:43 EEHg/L0.30 11/8/19SM21-22 6200B1m+p Xylene
ND 0.50 11/9/19 4:43 EEHg/L0.17 11/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 106 11/9/19 4:4370-130
Toluene-d8 101 11/9/19 4:4370-130
4-Bromofluorobenzene 93.2 11/9/19 4:4370-130
Page 21 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-08
Field Sample #: MW-2D
Sample Matrix: Ground Water
Sampled: 11/5/2019 11:47
[TOC_2]19K0437-08[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
ND 100 11/9/19 9:31 EEHg/L7.6 11/8/19SM21-22 6200B2Acetone
ND 1.0 11/9/19 9:31 EEHg/L0.36 11/8/19SM21-22 6200B2Benzene
ND 1.0 11/9/19 9:31 EEHg/L0.30 11/8/19SM21-22 6200B2Bromobenzene
ND 1.0 11/9/19 9:31 EEHg/L0.64 11/8/19SM21-22 6200B2Bromochloromethane
ND 1.0 11/9/19 9:31 EEHg/L0.32 11/8/19SM21-22 6200B2Bromodichloromethane
ND 1.0 11/9/19 9:31 EEHg/L0.92 11/8/19SM21-22 6200B2Bromoform
ND 2.0 11/9/19 9:31 EEHg/L1.6 11/8/19SM21-22 6200B2Bromomethane
ND 10 11/9/19 9:31 EEHg/L3.9 11/8/19SM21-22 6200B22-Butanone (MEK)
2.1 1.0 11/9/19 9:31 EEHg/L0.42 11/8/19SM21-22 6200B2n-Butylbenzene
1.6 1.0 11/9/19 9:31 EEHg/L0.32 11/8/19SM21-22 6200B2sec-Butylbenzene
ND 1.0 11/9/19 9:31 EEHg/L0.34 11/8/19SM21-22 6200B2tert-Butylbenzene
ND 1.0 11/9/19 9:31 EEHg/L0.22 11/8/19SM21-22 6200B2Carbon Tetrachloride
ND 1.0 11/9/19 9:31 EEHg/L0.30 11/8/19SM21-22 6200B2Chlorobenzene
ND 100 11/9/19 9:31 EEHg/L21 11/8/19SM21-22 6200B2Ethanol
ND 1.0 11/9/19 9:31 EEHg/L0.42 11/8/19SM21-22 6200B2Chlorodibromomethane
ND 1.0 11/9/19 9:31 EEHg/L0.70 11/8/19SM21-22 6200B2Chloroethane
ND 1.0 11/9/19 9:31 EEHg/L0.34 11/8/19SM21-22 6200B2Chloroform
ND 2.0 11/9/19 9:31 EEHg/L0.90 11/8/19SM21-22 6200B2Chloromethane
ND 1.0 11/9/19 9:31 EEHg/L0.24 11/8/19SM21-22 6200B22-Chlorotoluene
ND 1.0 11/9/19 9:31 EEHg/L0.28 11/8/19SM21-22 6200B24-Chlorotoluene
ND 1.0 11/9/19 9:31 EEHg/L0.38 11/8/19SM21-22 6200B21,2-Dibromoethane (EDB)
ND 1.0 11/9/19 9:31 EEHg/L0.32 11/8/19SM21-22 6200B21,2-Dichlorobenzene
ND 1.0 11/9/19 9:31 EEHg/L0.24 11/8/19SM21-22 6200B21,3-Dichlorobenzene
ND 1.0 11/9/19 9:31 EEHg/L0.26 11/8/19SM21-22 6200B21,4-Dichlorobenzene
ND 1.0 11/9/19 9:31 EEHg/L0.52 11/8/19SM21-22 6200B2Dichlorodifluoromethane (Freon 12)
ND 1.0 11/9/19 9:31 EEHg/L0.32 11/8/19SM21-22 6200B21,1-Dichloroethane
ND 2.0 11/9/19 9:31 EEHg/L0.82 11/8/19SM21-22 6200B21,2-Dichloroethane
ND 1.0 11/9/19 9:31 EEHg/L0.64 11/8/19SM21-22 6200B21,1-Dichloroethylene
ND 1.0 11/9/19 9:31 EEHg/L0.26 11/8/19SM21-22 6200B2cis-1,2-Dichloroethylene
ND 1.0 11/9/19 9:31 EEHg/L0.62 11/8/19SM21-22 6200B2trans-1,2-Dichloroethylene
ND 1.0 11/9/19 9:31 EEHg/L0.40 11/8/19SM21-22 6200B21,2-Dichloropropane
ND 1.0 11/9/19 9:31 EEHg/L0.22 11/8/19SM21-22 6200B21,3-Dichloropropane
ND 1.0 11/9/19 9:31 EEHg/L0.40 11/8/19SM21-22 6200B22,2-Dichloropropane
ND 1.0 11/9/19 9:31 EEHg/L0.32 11/8/19SM21-22 6200B21,1-Dichloropropene
ND 1.0 11/9/19 9:31 EEHg/L0.26 11/8/19SM21-22 6200B2cis-1,3-Dichloropropene
ND 1.0 11/9/19 9:31 EEHg/L0.46 11/8/19SM21-22 6200B2trans-1,3-Dichloropropene
ND 1.0 11/9/19 9:31 EEHg/L0.34 11/8/19SM21-22 6200B2Diisopropyl Ether (DIPE)
100 1.0 11/9/19 9:31 EEHg/L0.26 11/8/19SM21-22 6200B2Ethylbenzene
ND 10 11/9/19 9:31 EEHg/L3.0 11/8/19SM21-22 6200B22-Hexanone (MBK)
9.4 1.0 11/9/19 9:31 EEHg/L0.34 11/8/19SM21-22 6200B2Isopropylbenzene (Cumene)
0.60 1.0 11/9/19 9:31 EEHg/L0.40 11/8/19SM21-22 6200B2Jp-Isopropyltoluene (p-Cymene)
ND 1.0 11/9/19 9:31 EEHg/L0.50 11/8/19SM21-22 6200B2Methyl tert-Butyl Ether (MTBE)
ND 10 11/9/19 9:31 EEHg/L0.68 11/8/19SM21-22 6200B2Methylene Chloride
ND 10 11/9/19 9:31 EEHg/L3.3 11/8/19SM21-22 6200B24-Methyl-2-pentanone (MIBK)
Page 22 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-08
Field Sample #: MW-2D
Sample Matrix: Ground Water
Sampled: 11/5/2019 11:47
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Sample Flags: RL-11 Volatile Organic Compounds by GC/MS
29 10 11/9/19 9:31 EEHg/L0.62 11/8/19SM21-22 6200B2Naphthalene
24 1.0 11/9/19 9:31 EEHg/L0.26 11/8/19SM21-22 6200B2n-Propylbenzene
ND 1.0 11/9/19 9:31 EEHg/L0.22 11/8/19SM21-22 6200B2Styrene
ND 1.0 11/9/19 9:31 EEHg/L0.44 11/8/19SM21-22 6200B21,1,2,2-Tetrachloroethane
ND 1.0 11/9/19 9:31 EEHg/L0.36 11/8/19SM21-22 6200B2Tetrachloroethylene
1.2 1.0 11/9/19 9:31 EEHg/L0.28 11/8/19SM21-22 6200B2Toluene
ND 4.0 11/9/19 9:31 EEHg/L1.1 11/8/19SM21-22 6200B21,2,3-Trichlorobenzene
ND 1.0 11/9/19 9:31 EEHg/L0.80 11/8/19SM21-22 6200B21,2,4-Trichlorobenzene
ND 1.0 11/9/19 9:31 EEHg/L0.40 11/8/19SM21-22 6200B21,1,1-Trichloroethane
ND 1.0 11/9/19 9:31 EEHg/L0.32 11/8/19SM21-22 6200B21,1,2-Trichloroethane
ND 1.0 11/9/19 9:31 EEHg/L0.48 11/8/19SM21-22 6200B2Trichloroethylene
ND 1.0 11/9/19 9:31 EEHg/L0.66 11/8/19SM21-22 6200B2Trichlorofluoromethane (Freon 11)
ND 1.0 11/9/19 9:31 EEHg/L0.50 11/8/19SM21-22 6200B21,2,3-Trichloropropane
30 1.0 11/9/19 9:31 EEHg/L0.36 11/8/19SM21-22 6200B21,2,4-Trimethylbenzene
5.5 1.0 11/9/19 9:31 EEHg/L0.28 11/8/19SM21-22 6200B21,3,5-Trimethylbenzene
ND 40 11/9/19 9:31 EEHg/L20 11/8/19SM21-22 6200B2Vinyl Acetate
ND 1.0 11/9/19 9:31 EEHg/L0.90 11/8/19SM21-22 6200B2Vinyl Chloride
21 2.0 11/9/19 9:31 EEHg/L0.60 11/8/19SM21-22 6200B2m+p Xylene
22 1.0 11/9/19 9:31 EEHg/L0.34 11/8/19SM21-22 6200B2o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 108 11/9/19 9:3170-130
Toluene-d8 101 11/9/19 9:3170-130
4-Bromofluorobenzene 98.6 11/9/19 9:3170-130
Page 23 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-09
Field Sample #: SW-5
Sample Matrix: Ground Water
Sampled: 11/5/2019 12:09
[TOC_2]19K0437-09[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/9/19 5:12 EEHg/L3.8 11/8/19SM21-22 6200B1Acetone
ND 0.50 11/9/19 5:12 EEHg/L0.18 11/8/19SM21-22 6200B1Benzene
ND 0.50 11/9/19 5:12 EEHg/L0.15 11/8/19SM21-22 6200B1Bromobenzene
ND 0.50 11/9/19 5:12 EEHg/L0.32 11/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/9/19 5:12 EEHg/L0.16 11/8/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/9/19 5:12 EEHg/L0.46 11/8/19SM21-22 6200B1Bromoform
ND 1.0 11/9/19 5:12 EEHg/L0.78 11/8/19SM21-22 6200B1Bromomethane
ND 5.0 11/9/19 5:12 EEHg/L1.9 11/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/9/19 5:12 EEHg/L0.21 11/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/9/19 5:12 EEHg/L0.16 11/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/9/19 5:12 EEHg/L0.17 11/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/9/19 5:12 EEHg/L0.11 11/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/9/19 5:12 EEHg/L0.15 11/8/19SM21-22 6200B1Chlorobenzene
ND 50 11/9/19 5:12 EEHg/L11 11/8/19SM21-22 6200B1Ethanol
ND 0.50 11/9/19 5:12 EEHg/L0.21 11/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/9/19 5:12 EEHg/L0.35 11/8/19SM21-22 6200B1Chloroethane
ND 0.50 11/9/19 5:12 EEHg/L0.17 11/8/19SM21-22 6200B1Chloroform
ND 1.0 11/9/19 5:12 EEHg/L0.45 11/8/19SM21-22 6200B1Chloromethane
ND 0.50 11/9/19 5:12 EEHg/L0.12 11/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/9/19 5:12 EEHg/L0.14 11/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/9/19 5:12 EEHg/L0.19 11/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/9/19 5:12 EEHg/L0.16 11/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/9/19 5:12 EEHg/L0.12 11/8/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/9/19 5:12 EEHg/L0.13 11/8/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/9/19 5:12 EEHg/L0.26 11/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/9/19 5:12 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/9/19 5:12 EEHg/L0.41 11/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/9/19 5:12 EEHg/L0.32 11/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/9/19 5:12 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/9/19 5:12 EEHg/L0.31 11/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/9/19 5:12 EEHg/L0.20 11/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/9/19 5:12 EEHg/L0.11 11/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/9/19 5:12 EEHg/L0.20 11/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/9/19 5:12 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/9/19 5:12 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/9/19 5:12 EEHg/L0.23 11/8/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/9/19 5:12 EEHg/L0.17 11/8/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/9/19 5:12 EEHg/L0.13 11/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/9/19 5:12 EEHg/L1.5 11/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/9/19 5:12 EEHg/L0.17 11/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/9/19 5:12 EEHg/L0.20 11/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/9/19 5:12 EEHg/L0.25 11/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/9/19 5:12 EEHg/L0.34 11/8/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/9/19 5:12 EEHg/L1.7 11/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 24 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-09
Field Sample #: SW-5
Sample Matrix: Ground Water
Sampled: 11/5/2019 12:09
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 11/9/19 5:12 EEHg/L0.31 11/8/19SM21-22 6200B1Naphthalene
ND 0.50 11/9/19 5:12 EEHg/L0.13 11/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/9/19 5:12 EEHg/L0.11 11/8/19SM21-22 6200B1Styrene
ND 0.50 11/9/19 5:12 EEHg/L0.22 11/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/9/19 5:12 EEHg/L0.18 11/8/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/9/19 5:12 EEHg/L0.14 11/8/19SM21-22 6200B1Toluene
ND 2.0 11/9/19 5:12 EEHg/L0.57 11/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/9/19 5:12 EEHg/L0.40 11/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/9/19 5:12 EEHg/L0.20 11/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/9/19 5:12 EEHg/L0.16 11/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/9/19 5:12 EEHg/L0.24 11/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/9/19 5:12 EEHg/L0.33 11/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/9/19 5:12 EEHg/L0.25 11/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/9/19 5:12 EEHg/L0.18 11/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/9/19 5:12 EEHg/L0.14 11/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/9/19 5:12 EEHg/L10 11/8/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/9/19 5:12 EEHg/L0.45 11/8/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/9/19 5:12 EEHg/L0.30 11/8/19SM21-22 6200B1m+p Xylene
ND 0.50 11/9/19 5:12 EEHg/L0.17 11/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 108 11/9/19 5:1270-130
Toluene-d8 99.8 11/9/19 5:1270-130
4-Bromofluorobenzene 94.6 11/9/19 5:1270-130
Page 25 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-10
Field Sample #: SW-4
Sample Matrix: Ground Water
Sampled: 11/5/2019 12:30
[TOC_2]19K0437-10[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/9/19 5:41 EEHg/L3.8 11/8/19SM21-22 6200B1Acetone
ND 0.50 11/9/19 5:41 EEHg/L0.18 11/8/19SM21-22 6200B1Benzene
ND 0.50 11/9/19 5:41 EEHg/L0.15 11/8/19SM21-22 6200B1Bromobenzene
ND 0.50 11/9/19 5:41 EEHg/L0.32 11/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/9/19 5:41 EEHg/L0.16 11/8/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/9/19 5:41 EEHg/L0.46 11/8/19SM21-22 6200B1Bromoform
ND 1.0 11/9/19 5:41 EEHg/L0.78 11/8/19SM21-22 6200B1Bromomethane
ND 5.0 11/9/19 5:41 EEHg/L1.9 11/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/9/19 5:41 EEHg/L0.21 11/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/9/19 5:41 EEHg/L0.16 11/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/9/19 5:41 EEHg/L0.17 11/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/9/19 5:41 EEHg/L0.11 11/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/9/19 5:41 EEHg/L0.15 11/8/19SM21-22 6200B1Chlorobenzene
ND 50 11/9/19 5:41 EEHg/L11 11/8/19SM21-22 6200B1Ethanol
ND 0.50 11/9/19 5:41 EEHg/L0.21 11/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/9/19 5:41 EEHg/L0.35 11/8/19SM21-22 6200B1Chloroethane
ND 0.50 11/9/19 5:41 EEHg/L0.17 11/8/19SM21-22 6200B1Chloroform
ND 1.0 11/9/19 5:41 EEHg/L0.45 11/8/19SM21-22 6200B1Chloromethane
ND 0.50 11/9/19 5:41 EEHg/L0.12 11/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/9/19 5:41 EEHg/L0.14 11/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/9/19 5:41 EEHg/L0.19 11/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/9/19 5:41 EEHg/L0.16 11/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/9/19 5:41 EEHg/L0.12 11/8/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/9/19 5:41 EEHg/L0.13 11/8/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/9/19 5:41 EEHg/L0.26 11/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/9/19 5:41 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/9/19 5:41 EEHg/L0.41 11/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/9/19 5:41 EEHg/L0.32 11/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/9/19 5:41 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/9/19 5:41 EEHg/L0.31 11/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/9/19 5:41 EEHg/L0.20 11/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/9/19 5:41 EEHg/L0.11 11/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/9/19 5:41 EEHg/L0.20 11/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/9/19 5:41 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/9/19 5:41 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/9/19 5:41 EEHg/L0.23 11/8/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/9/19 5:41 EEHg/L0.17 11/8/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/9/19 5:41 EEHg/L0.13 11/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/9/19 5:41 EEHg/L1.5 11/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/9/19 5:41 EEHg/L0.17 11/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/9/19 5:41 EEHg/L0.20 11/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/9/19 5:41 EEHg/L0.25 11/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/9/19 5:41 EEHg/L0.34 11/8/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/9/19 5:41 EEHg/L1.7 11/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 26 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-10
Field Sample #: SW-4
Sample Matrix: Ground Water
Sampled: 11/5/2019 12:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 11/9/19 5:41 EEHg/L0.31 11/8/19SM21-22 6200B1Naphthalene
ND 0.50 11/9/19 5:41 EEHg/L0.13 11/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/9/19 5:41 EEHg/L0.11 11/8/19SM21-22 6200B1Styrene
ND 0.50 11/9/19 5:41 EEHg/L0.22 11/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/9/19 5:41 EEHg/L0.18 11/8/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/9/19 5:41 EEHg/L0.14 11/8/19SM21-22 6200B1Toluene
ND 2.0 11/9/19 5:41 EEHg/L0.57 11/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/9/19 5:41 EEHg/L0.40 11/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/9/19 5:41 EEHg/L0.20 11/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/9/19 5:41 EEHg/L0.16 11/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/9/19 5:41 EEHg/L0.24 11/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/9/19 5:41 EEHg/L0.33 11/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/9/19 5:41 EEHg/L0.25 11/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/9/19 5:41 EEHg/L0.18 11/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/9/19 5:41 EEHg/L0.14 11/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/9/19 5:41 EEHg/L10 11/8/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/9/19 5:41 EEHg/L0.45 11/8/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/9/19 5:41 EEHg/L0.30 11/8/19SM21-22 6200B1m+p Xylene
ND 0.50 11/9/19 5:41 EEHg/L0.17 11/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 109 11/9/19 5:4170-130
Toluene-d8 101 11/9/19 5:4170-130
4-Bromofluorobenzene 93.0 11/9/19 5:4170-130
Page 27 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-11
Field Sample #: SW-6
Sample Matrix: Ground Water
Sampled: 11/5/2019 12:50
[TOC_2]19K0437-11[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 11/9/19 6:09 EEHg/L3.8 11/8/19SM21-22 6200B1Acetone
ND 0.50 11/9/19 6:09 EEHg/L0.18 11/8/19SM21-22 6200B1Benzene
ND 0.50 11/9/19 6:09 EEHg/L0.15 11/8/19SM21-22 6200B1Bromobenzene
ND 0.50 11/9/19 6:09 EEHg/L0.32 11/8/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/9/19 6:09 EEHg/L0.16 11/8/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/9/19 6:09 EEHg/L0.46 11/8/19SM21-22 6200B1Bromoform
ND 1.0 11/9/19 6:09 EEHg/L0.78 11/8/19SM21-22 6200B1Bromomethane
ND 5.0 11/9/19 6:09 EEHg/L1.9 11/8/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/9/19 6:09 EEHg/L0.21 11/8/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/9/19 6:09 EEHg/L0.16 11/8/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/9/19 6:09 EEHg/L0.17 11/8/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/9/19 6:09 EEHg/L0.11 11/8/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/9/19 6:09 EEHg/L0.15 11/8/19SM21-22 6200B1Chlorobenzene
ND 50 11/9/19 6:09 EEHg/L11 11/8/19SM21-22 6200B1Ethanol
ND 0.50 11/9/19 6:09 EEHg/L0.21 11/8/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/9/19 6:09 EEHg/L0.35 11/8/19SM21-22 6200B1Chloroethane
ND 0.50 11/9/19 6:09 EEHg/L0.17 11/8/19SM21-22 6200B1Chloroform
ND 1.0 11/9/19 6:09 EEHg/L0.45 11/8/19SM21-22 6200B1Chloromethane
ND 0.50 11/9/19 6:09 EEHg/L0.12 11/8/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/9/19 6:09 EEHg/L0.14 11/8/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/9/19 6:09 EEHg/L0.19 11/8/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/9/19 6:09 EEHg/L0.16 11/8/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/9/19 6:09 EEHg/L0.12 11/8/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/9/19 6:09 EEHg/L0.13 11/8/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/9/19 6:09 EEHg/L0.26 11/8/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/9/19 6:09 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/9/19 6:09 EEHg/L0.41 11/8/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/9/19 6:09 EEHg/L0.32 11/8/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/9/19 6:09 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/9/19 6:09 EEHg/L0.31 11/8/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/9/19 6:09 EEHg/L0.20 11/8/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/9/19 6:09 EEHg/L0.11 11/8/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/9/19 6:09 EEHg/L0.20 11/8/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/9/19 6:09 EEHg/L0.16 11/8/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/9/19 6:09 EEHg/L0.13 11/8/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/9/19 6:09 EEHg/L0.23 11/8/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/9/19 6:09 EEHg/L0.17 11/8/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/9/19 6:09 EEHg/L0.13 11/8/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/9/19 6:09 EEHg/L1.5 11/8/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/9/19 6:09 EEHg/L0.17 11/8/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/9/19 6:09 EEHg/L0.20 11/8/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/9/19 6:09 EEHg/L0.25 11/8/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/9/19 6:09 EEHg/L0.34 11/8/19SM21-22 6200B1Methylene Chloride
ND 5.0 11/9/19 6:09 EEHg/L1.7 11/8/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
Page 28 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 11/6/2019
Work Order: 19K0437Sample Description:Project Location: Wade, NC
Sample ID: 19K0437-11
Field Sample #: SW-6
Sample Matrix: Ground Water
Sampled: 11/5/2019 12:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 11/9/19 6:09 EEHg/L0.31 11/8/19SM21-22 6200B1Naphthalene
ND 0.50 11/9/19 6:09 EEHg/L0.13 11/8/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/9/19 6:09 EEHg/L0.11 11/8/19SM21-22 6200B1Styrene
ND 0.50 11/9/19 6:09 EEHg/L0.22 11/8/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/9/19 6:09 EEHg/L0.18 11/8/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/9/19 6:09 EEHg/L0.14 11/8/19SM21-22 6200B1Toluene
ND 2.0 11/9/19 6:09 EEHg/L0.57 11/8/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/9/19 6:09 EEHg/L0.40 11/8/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/9/19 6:09 EEHg/L0.20 11/8/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/9/19 6:09 EEHg/L0.16 11/8/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/9/19 6:09 EEHg/L0.24 11/8/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/9/19 6:09 EEHg/L0.33 11/8/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/9/19 6:09 EEHg/L0.25 11/8/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/9/19 6:09 EEHg/L0.18 11/8/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/9/19 6:09 EEHg/L0.14 11/8/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/9/19 6:09 EEHg/L10 11/8/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/9/19 6:09 EEHg/L0.45 11/8/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/9/19 6:09 EEHg/L0.30 11/8/19SM21-22 6200B1m+p Xylene
ND 0.50 11/9/19 6:09 EEHg/L0.17 11/8/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 104 11/9/19 6:0970-130
Toluene-d8 99.8 11/9/19 6:0970-130
4-Bromofluorobenzene 92.4 11/9/19 6:0970-130
Page 29 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B245494 11/08/1955.0019K0437-01 [field blank]
B245494 11/08/1955.0019K0437-02 [MW-6]
B245494 11/08/190.25 5.0019K0437-03 [MW-5]
B245494 11/08/1955.0019K0437-04 [MW-4]
B245494 11/08/190.05 5.0019K0437-05 [MW-3]
B245494 11/08/190.25 5.0019K0437-06 [MW-2]
B245494 11/08/1955.0019K0437-07 [MW-1]
B245494 11/08/192.5 5.0019K0437-08 [MW-2D]
B245494 11/08/1955.0019K0437-09 [SW-5]
B245494 11/08/1955.0019K0437-10 [SW-4]
B245494 11/08/1955.0019K0437-11 [SW-6]
[TOC_1]Sample Preparation Information[TOC]
Page 30 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B245494 - SW-846 5030B
[TOC_3]B245494[TOC]
Blank (B245494-BLK1) Prepared: 11/08/19 Analyzed: 11/09/19
Acetone g/L50ND
tert-Amyl Methyl Ether (TAME)g/L0.50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
tert-Butyl Alcohol (TBA)g/L20ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
tert-Butyl Ethyl Ether (TBEE)g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
[TOC_1]QC Data[TOC]
Page 31 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245494 - SW-846 5030B
Blank (B245494-BLK1) Prepared: 11/08/19 Analyzed: 11/09/19
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10927.2
g/L 25.0 70-130Surrogate: Toluene-d8 10125.3
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 96.224.1
LCS (B245494-BS1) Prepared & Analyzed: 11/08/19
Acetone g/L50 100 L-0670-130138*138
tert-Amyl Methyl Ether (TAME)g/L0.50 10.0 L-0770-13066.4 *6.64
Benzene g/L0.50 10.0 70-13095.49.54
Bromobenzene g/L0.50 10.0 70-13010510.5
Bromochloromethane g/L0.50 10.0 70-13011011.0
Bromodichloromethane g/L0.50 10.0 70-13011011.0
Bromoform g/L0.50 10.0 70-13095.39.53
Bromomethane g/L1.0 10.0 60-14011011.0
2-Butanone (MEK)g/L5.0 100 70-130112112
tert-Butyl Alcohol (TBA)g/L20 100 40-130121121
n-Butylbenzene g/L0.50 10.0 70-13011911.9
sec-Butylbenzene g/L0.50 10.0 70-13011711.7
tert-Butylbenzene g/L0.50 10.0 70-13011611.6
tert-Butyl Ethyl Ether (TBEE)g/L0.50 10.0 70-13078.97.89
Carbon Tetrachloride g/L0.50 10.0 70-13010610.6
Chlorobenzene g/L0.50 10.0 70-13010410.4
Ethanol g/L50 100 L-0270-130199*199
Chlorodibromomethane g/L0.50 10.0 70-13010510.5
Chloroethane g/L0.50 10.0 60-14096.69.66
Chloroform g/L0.50 10.0 70-13096.99.69
Chloromethane g/L0.60 10.0 60-14010410.4
2-Chlorotoluene g/L0.50 10.0 70-13010110.1
4-Chlorotoluene g/L0.50 10.0 70-13010610.6
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13010310.3
1,2-Dichlorobenzene g/L0.50 10.0 70-13010810.8
1,3-Dichlorobenzene g/L0.50 10.0 70-13010910.9
1,4-Dichlorobenzene g/L0.50 10.0 70-13010710.7
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14081.58.15
1,1-Dichloroethane g/L0.50 10.0 70-13010310.3
1,2-Dichloroethane g/L0.50 10.0 70-13011711.7
1,1-Dichloroethylene g/L0.50 10.0 70-13011411.4
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13010810.8
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13010710.7
Page 32 of 42
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245494 - SW-846 5030B
LCS (B245494-BS1) Prepared & Analyzed: 11/08/19
1,2-Dichloropropane g/L0.50 10.0 70-13010910.9
1,3-Dichloropropane g/L0.50 10.0 70-13010910.9
2,2-Dichloropropane g/L0.50 10.0 70-13093.99.39
1,1-Dichloropropene g/L0.50 10.0 70-13010410.4
cis-1,3-Dichloropropene g/L0.50 10.0 70-13010810.8
trans-1,3-Dichloropropene g/L0.50 10.0 70-13010310.3
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13011711.7
Ethylbenzene g/L0.50 10.0 70-13010810.8
2-Hexanone (MBK)g/L5.0 100 L-0270-130132*132
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13011011.0
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13011011.0
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13089.78.97
Methylene Chloride g/L5.0 10.0 70-13011711.7
4-Methyl-2-pentanone (MIBK)g/L5.0 100 L-0270-130138*138
Naphthalene g/L0.50 10.0 70-13010810.8
n-Propylbenzene g/L0.50 10.0 70-13011011.0
Styrene g/L0.50 10.0 70-13098.69.86
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13010910.9
Tetrachloroethylene g/L0.50 10.0 70-13010810.8
Toluene g/L0.50 10.0 70-13010510.5
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13087.38.73
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13097.79.77
1,1,1-Trichloroethane g/L0.50 10.0 70-13011111.1
1,1,2-Trichloroethane g/L0.50 10.0 70-13010210.2
Trichloroethylene g/L0.50 10.0 70-13011011.0
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13011011.0
1,2,3-Trichloropropane g/L0.50 10.0 70-13011511.5
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13011011.0
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13010610.6
Vinyl Acetate g/L20 100 70-130104104
Vinyl Chloride g/L0.50 10.0 L-0260-140302*30.2
m+p Xylene g/L1.0 20.0 70-13010721.4
o-Xylene g/L0.50 10.0 70-13010910.9
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10927.3
g/L 25.0 70-130Surrogate: Toluene-d8 10225.4
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 97.224.3
LCS Dup (B245494-BSD1) Prepared: 11/08/19 Analyzed: 11/09/19
Acetone g/L50 100 25 L-0670-130154 10.7*154
tert-Amyl Methyl Ether (TAME)g/L0.50 10.0 2570-13072.6 8.927.26
Benzene g/L0.50 10.0 2570-13096.6 1.259.66
Bromobenzene g/L0.50 10.0 2570-130107 1.4110.7
Bromochloromethane g/L0.50 10.0 2570-130112 1.5311.2
Bromodichloromethane g/L0.50 10.0 2570-130108 1.1910.8
Bromoform g/L0.50 10.0 2570-130104 9.2110.4
Bromomethane g/L1.0 10.0 2560-140105 4.9410.5
2-Butanone (MEK)g/L5.0 100 2570-130124 9.73124
tert-Butyl Alcohol (TBA)g/L20 100 25 L-0740-130136 11.4*136
n-Butylbenzene g/L0.50 10.0 2570-130114 4.0311.4
sec-Butylbenzene g/L0.50 10.0 2570-130112 4.5511.2
tert-Butylbenzene g/L0.50 10.0 2570-130110 5.3311.0
tert-Butyl Ethyl Ether (TBEE)g/L0.50 10.0 2570-13084.6 6.978.46
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245494 - SW-846 5030B
LCS Dup (B245494-BSD1) Prepared: 11/08/19 Analyzed: 11/09/19
Carbon Tetrachloride g/L0.50 10.0 2570-130106 0.28310.6
Chlorobenzene g/L0.50 10.0 2570-130102 2.8110.2
Ethanol g/L50 100 25 L-0270-130203 1.70*203
Chlorodibromomethane g/L0.50 10.0 2570-130104 1.0510.4
Chloroethane g/L0.50 10.0 2560-14098.2 1.649.82
Chloroform g/L0.50 10.0 2570-13098.7 1.849.87
Chloromethane g/L0.60 10.0 2560-14097.3 7.049.73
2-Chlorotoluene g/L0.50 10.0 2570-130102 0.59310.2
4-Chlorotoluene g/L0.50 10.0 2570-130110 3.0511.0
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130104 0.96710.4
1,2-Dichlorobenzene g/L0.50 10.0 2570-130107 0.93010.7
1,3-Dichlorobenzene g/L0.50 10.0 2570-130110 0.45711.0
1,4-Dichlorobenzene g/L0.50 10.0 2570-130106 1.3110.6
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14078.4 3.887.84
1,1-Dichloroethane g/L0.50 10.0 2570-130104 1.2610.4
1,2-Dichloroethane g/L0.50 10.0 2570-130118 0.25511.8
1,1-Dichloroethylene g/L0.50 10.0 2570-130114 0.43911.4
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-130107 0.74610.7
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-130108 0.46510.8
1,2-Dichloropropane g/L0.50 10.0 2570-130106 2.5110.6
1,3-Dichloropropane g/L0.50 10.0 2570-130109 0.55010.9
2,2-Dichloropropane g/L0.50 10.0 2570-13092.0 2.049.20
1,1-Dichloropropene g/L0.50 10.0 2570-130106 1.3310.6
cis-1,3-Dichloropropene g/L0.50 10.0 2570-130106 2.7110.6
trans-1,3-Dichloropropene g/L0.50 10.0 2570-130107 3.1410.7
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130116 0.86111.6
Ethylbenzene g/L0.50 10.0 2570-130106 2.0610.6
2-Hexanone (MBK)g/L5.0 100 25 L-0270-130152 13.9*152
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130110 0.54611.0
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130107 2.4910.7
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13098.6 9.459.86
Methylene Chloride g/L5.0 10.0 2570-130122 4.1912.2
4-Methyl-2-pentanone (MIBK)g/L5.0 100 25 L-0270-130150 8.49*150
Naphthalene g/L0.50 10.0 2570-130116 7.2511.6
n-Propylbenzene g/L0.50 10.0 2570-130108 1.4710.8
Styrene g/L0.50 10.0 2570-13095.4 3.309.54
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130118 8.2011.8
Tetrachloroethylene g/L0.50 10.0 2570-130104 3.5010.4
Toluene g/L0.50 10.0 2570-130104 1.4310.4
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-130107 20.210.7
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-130109 10.610.9
1,1,1-Trichloroethane g/L0.50 10.0 2570-130107 3.4910.7
1,1,2-Trichloroethane g/L0.50 10.0 2570-130105 2.8010.5
Trichloroethylene g/L0.50 10.0 2570-130104 5.5910.4
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-130109 0.54710.9
1,2,3-Trichloropropane g/L0.50 10.0 2570-130123 6.4612.3
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-130104 6.1610.4
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130106 0.18810.6
Vinyl Acetate g/L20 100 2570-130117 11.9117
Vinyl Chloride g/L0.50 10.0 25 L-0260-140269 11.4*26.9
m+p Xylene g/L1.0 20.0 2570-130107 0.23321.4
o-Xylene g/L0.50 10.0 2570-130110 0.91211.0
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245494 - SW-846 5030B
LCS Dup (B245494-BSD1) Prepared: 11/08/19 Analyzed: 11/09/19
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 11127.8
g/L 25.0 70-130Surrogate: Toluene-d8 10125.2
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 98.324.6
Page 35 of 42
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
FLAG/QUALIFIER SUMMARY
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits.
Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is
on the high side.
L-02
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the high side.
L-06
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Elevated reporting limit due to high concentration of target compounds.RL-11
[TOC_1]Flag/Qualifier Summary[TOC]
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
[TOC_1]Certifications[TOC]
Page 37 of 42
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2020
M-MA100Massachusetts DEPMA 06/30/2020
PH-0567Connecticut Department of Publilc HealthCT 09/30/2021
10899 NELAPNew York State Department of HealthNY 04/1/2020
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2020
LAO00112Rhode Island Department of HealthRI 12/30/2019
652North Carolina Div. of Water QualityNC 12/31/2019
MA007 NELAPNew Jersey DEPNJ 06/30/2020
E871027 NELAPFlorida Department of HealthFL 06/30/2020
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2020
2011028State of MaineME 06/9/2021
460217Commonwealth of VirginiaVA 12/14/2019
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2020
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2020
25703North Carolina Department of HealthNC-DW 07/31/2020
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2020
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