MO-6196_23514_CA_MRP_20200116

Groundwater Monitoring Report
Exxon Service Station

226 South Main Avenue
Newton, Catawba County, North Carolina 28658
NCDEQ Incident #23514
ATC Project #SLP2351403

January 16, 2020

TABLE OF CONTENTS

1.0 SITE IDENTIFICATION .......................................................................................1
2.0 EXECUTIVE SUMMARY .....................................................................................2
3.0 SITE DESCRIPTION .............................................................................................3
3.1 Site Characterization ................................................................................3
3.2 Site Background .......................................................................................3
3.3 Site and Regional Geology ......................................................................4
3.4 Site and Regional Hydrogeology .............................................................4
4.0 GROUNDWATER CHARACTERIZATION.......................................................5
4.1 Groundwater Levels .................................................................................5
4.2 Groundwater Quality ...............................................................................5
5.0 CONCLUSIONS AND RECOMMENDATIONS .................................................6

TABLES

Table 1 Monitoring Well Construction Details
Table 2 Groundwater Elevation Data
Table 3 Recent Groundwater Analytical Results
Table 4 Historical Groundwater Analytical Results

FIGURES

Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Groundwater Elevation Contour Map
Figure 4 Benzene Isoconcentration Contour Map
Figure 5 Groundwater Analytical Results

APPENDICES

Appendix A Field Notes
Appendix B Laboratory Analytical Report

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2.0 EXECUTIVE SUMMARY
ATC Associates of North Carolina, P.C. (ATC) has completed a Groundwater Monitoring Report
(GMR), which included groundwater monitoring well sampling at the Exxon Service Station. The
site is located at 226 South Main Avenue, Newton, Catawba County, North Carolina. This report
was completed based on the approval of Task Authorization, TA-03 on October 22, 2019, by the
Trust Fund Branch of the Underground Storage Tank (UST) Section, Division of Waste
Management, North Carolina Department of Environmental Quality (NCDEQ). The work is being
performed as part of State Lead Contract, #N17004 between NCDEQ and ATC.

A petroleum release, identified during the June 2001 removal of four on-site USTs, was reported to
the NCDEQ in August 2001. The site is currently occupied by Redline Automotive and Napa
Autocare Center with no retail fuel operations. Thus, this GMR documents impact conditions
associated with assessment and monitoring of former site operations and the historical UST system.

In accordance with activities approved under TA-03, ATC gauged and sampled six groundwater
monitoring wells (MW-1SR, MW-3, MW-4, MW-6, MW-8, and MW-11) on October 29, 2019.
Monitoring well MW-5 could not be located, and was not sampled. Groundwater samples were
submitted to Pace Analytical (Pace) of Huntersville, North Carolina and analyzed for volatile
organic compounds (VOCs) by Standard Method 6200B.

The findings from the recent and previous assessment activities indicate the following:

 Municipal water is available to the site and surrounding area, and potential water supply
wells have not been identified within 1,500 feet of the site;
 One surface water body, a tributary to Hildebran Creek, is located approximately 400 feet
southwest of the site;
 Light non-aqueous phase liquid (LNAPL) was not measured in the sampled monitoring
wells;
 Groundwater from monitoring wells MW-3, MW-4, MW-8, and MW-11 contained
concentrations of at least one constituent above the 15A NCAC 02L .0202 Groundwater
Quality Standards (2L Standards);
 Concentrations of one or more constituents exceeded the 15A NCAC 2B Surface Water
Quality Standards (2B Standards) by more than 10 times, in wells MW-3, MW-4, MW-8,
and MW-11;
 None of the detected concentrations in the monitoring well samples exceeded the Gross
Contamination Levels (GCLs);
 Tetrachloroethylene (TCE) was detected (and has been detected) at concentrations
exceeding the 2L Standards, in the sidegradient well MW-8, located south of Kelly’s Village
Cleaners (232 South Main Avenue) just east of the site; and
 Groundwater flow is to the southwest.

Contaminant concentrations appear to be stable or decreasing. ATC recommends continued
monitored natural attenuation. However, ATC also recommends that the NCDEQ consider closing
the incident with a Notice of Residual Petroleum.

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3.0 SITE DESCRIPTION
3.1 Site Characterization
The NCDEQ retained ATC to provide environmental consulting services for the Exxon Service
Station, located at 226 South Main Avenue, Newton, Catawba County, North Carolina. Figure 1
depicts the site location on a topographic map. The site currently operates as Redline Automotive
and Napa Autocare Center, an automotive repair and parts retail businesses. Municipal water is
available to the site and vicinity.

3.2 Site Background
The site formerly operated as Exxon Service Station, a petroleum retail facility and automotive
service station. Four USTs were located at the site, including three 8,000-gallon gasoline USTs
and one 1,000-gallon waste oil UST. The tanks were installed in January 1987. Two fuel oil
aboveground storage tanks (ASTs) were also located at the site. In 2001, the USTs and ASTs
were removed. Soil samples collected beneath the USTs and product lines indicated elevated
concentrations of diesel and gasoline range total petroleum hydrocarbons (TPH). The UST
Closure Report completed by Enviro-Pro, P.C. (Enviro-Pro) on August 10, 2001, indicated older
USTs located in the same tank basin were replaced with the three 8,000-gallon gasoline USTs
and that the older USTs were the likely cause of the identified impacted soil. Details regarding
potential additional former USTs at the site is not available.

A Phase I Limited Site Assessment (LSA) was conducted at the site by BPA Environmental &
Engineering, Inc. (BPA) in October 2001. One groundwater monitoring well, MW-1S, was
installed in the former gasoline UST basin and sampled. Benzene concentration exceeded the 2L
Standard. A Phase II LSA was completed in December 2001, including the installation of four
additional monitoring wells, MW-1D, MW-2, MW-3, and MW-4. The Phase I/II LSA Report
indicated public water was available to the site and surrounding area; no water supply wells used
for drinking purposes were located within 1,500 feet of the site; and no water supply wells used
for any purpose were located within 500 feet of the site. A tributary to Hildebran Creek was
identified approximately 500 feet southwest of the site. Soil samples collected during well
installation activities indicated contaminant concentrations above Soil-to-Groundwater
Maximum Soil Contaminant Concentrations (MSCCs) and a concentration of p-isopropyltoluene
above the Residential MSCC. Groundwater samples collected during LSA activities indicated
concentrations exceeding GCLs in well MW-3 and concentrations exceeding 2L Standards in
wells MW-1S, MW-2, MW-3, and MW-4.

Comprehensive Site Assessment (CSA) and CSA Addendum activities were conducted by
Enviro-Pro in 2002, to delineate soil and groundwater impact at the site. Five soil borings were
advanced at the site. Sampled soils indicated contaminant concentrations exceeding Soil-to-
Groundwater MSCCs. Four Type II monitoring wells (MW-5 through MW-8) were installed in
May 2002, and two Type II monitoring wells (MW-9 and MW-10) were installed in August 2002
at off-site properties. Petroleum hydrocarbons were reported above 2L Standards in wells MW-5,
MW-6, MW-7, and MW-8. Slug tests conducted in wells MW-2, MW-6, and MW-8 indicated a
hydraulic conductivity in the area of the former gasoline UST basin of 0.034 feet/day.

Two additional soil samples were collected in October 2002 in the area of the former gasoline
product lines. Gasoline range TPH concentrations did not exceed laboratory reporting limits.

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In June 2003, Enviro-Pro completed soil excavation activities for the site. A total of 655 tons of
contaminated soil was removed from the former gasoline UST basin area. Excavation ceased
vertically at a depth of 25 feet below grade due to the depth of the shallow water table.
Excavation ceased laterally to the south due to the proximity of Highway 10. Six confirmation
soil samples were collected following excavation activities. Soil samples S-1 and S-2 were
collected from the excavation bottom and sidewall, respectively, and analyzed by the
Massachusetts Department of Environmental Protection Volatile Petroleum Hydrocarbon
(MADEP VPH) method. Both samples exceeded the Residential MSCCs.

Since 2016, ATC has conducted several groundwater sampling events and installed additional
groundwater monitoring wells for additional contaminant delineation.

On November 9, 2017, ATC performed an updated sensitive receptor survey by conducting a
visual reconnaissance of the surrounding area within 1,500 feet of the source area. ATC
reviewed the Catawba County GIS website and confirmed city water was available to properties
in the area. An unnamed tributary of Hildebran Creek was observed approximately 500 feet to
the southwest of the subject site. The site is not located in a wellhead protection program area or
in the Coastal Plain Physiographic region.

In March 2019, monitoring well MW-11 was installed and sampled to help delineate the area of
on-site contamination. Heavy petroleum odors were observed during well installation in soils from
approximately 20-35 feet bgs, and a visible sheen was observed on the groundwater during well
development. Six monitoring wells were located and sampled. Multiple monitoring wells
contained petroleum constituents exceeding 2L Standards, and newly installed well MW-11
contained concentrations of several constituents close to GCLs. ATC recommended a limited
confirmation sampling event approximately six months later.

3.3 Site and Regional Geology

According to the Geologic Map of North Carolina, produced by the State of North Carolina in
1985, the site is located in the Inner Piedmont Belt of the Piedmont Physiographic Province of
North Carolina. The rock types at the site have been identified as biotite gneiss and schist. The
shallow subsurface in most areas of the Piedmont contains residual soil overburden, including
structure-free residuum, saprolite, and partially weathered rock (PWR) that derive from in-place
weathering of the crystalline bedrock. Occasional areas containing recent deposits of alluvium in
the uppermost subsurface are found near streams and rivers. Saprolite and PWR typically contain
some relict structures from the original rock material. Depth to rock ranges from ground surface
at occasional outcrops to depths of greater than 100 feet in areas of easily weathered rock.

According to monitoring well installation records from the 2001 Phase I LSA, the primary soil
types encountered consisted of a surface layer of fill, followed by micaceous silt and clay with
little to some fine sand. Bedrock has been encountered on-site at a depth of 54.5 feet below
ground surface (ft bgs).

3.4 Site and Regional Hydrogeology

The shallow aquifer occurrence varies in depth from ground surface at springs, creeks, and rivers
to as deep as 50 feet or more beneath upland surfaces in some parts of the Piedmont. Water in the
alluvium or unconsolidated residual material, including saprolite and PWR, usually behaves as
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an unconfined aquifer, or water table, and will yield water with head elevation equivalent to the
first elevation where water was encountered. Permeability varies with lithology and is typically
relatively low in residual soils, with higher permeability in saprolite or PWR due to relict rock
texture and variable susceptibility to weathering exhibited by different minerals in the rock.
Groundwater flow in residual soils or alluvium is usually in rough concurrence with local
topographic conditions and is toward local drainage features. Based on the data from the
monitoring well network, shallow groundwater flows generally to the southwest. Depth to water
at the site ranges from approximately 9-22 ft bgs, based on recent field data.

The bedrock fractures or other planar features of the Inner Piedmont Belt Physiographic
Province generally constitute the bedrock aquifer, with the surrounding rock material being
effectively impermeable. Along with fractures, contacts between rock bodies probably constitute
zones of significant groundwater occurrence in the bedrock. The surrounding material and
overlying residuum tend to make the bedrock aquifer a semi-confined aquifer. That is, the
overlying water and soil weight normally results in pressure that causes water in a borehole,
which intersects a fracture or other feature, to rise above the elevation of the fracture or feature.
Modern water supply wells in the Piedmont are typically installed with a surface casing through
the unconsolidated material, and an open borehole into the bedrock where water-bearing
fractures are encountered.

4.0 GROUNDWATER CHARACTERIZATION

4.1 Groundwater Levels
On October 29, 2019, monitoring wells MW-1SR, MW-3, MW-4, MW-6, MW-8, and MW-11
were gauged for depth to groundwater. A site map is presented as Figure 2. Table 1 summarizes
monitoring well construction details. An oil/water interface probe was used to measure the depth
to groundwater from the top of well casing (TOC). LNAPL was not measured in the wells
gauged. ATC staff attempted to locate sidegradient well MW-5 with a metal detector and spud
bar, but was unsuccessful. Current and historical groundwater elevation data can be found in
Table 2 and a groundwater elevation contours are depicted in Figure 3. Field notes are included
in Appendix A.

4.2 Groundwater Quality
On October 29, 2019 monitoring wells MW-1SR, MW-3, MW-4, MW-6, MW-8, and MW-11 were
gauged, purged of approximately three standing well volumes or until purged dry and allowed to
recharge, and sampled. Groundwater samples were collected in preserved laboratory-supplied
containers; entered into chain of custody control; placed on ice; and delivered to North Carolina-
accredited Pace in Huntersville, North Carolina. A field blank was also collected during the
sampling event and included with the groundwater samples. The groundwater samples were
analyzed for petroleum constituents, including VOCs by Standard Method 6200B. The analytical
report for groundwater is included in Appendix B.

Recent groundwater analytical results are summarized in Table 3. Historical groundwater quality
data is represented in Table 4. The groundwater analytical results were compared to the NCDEQ 2L
Standards for groundwater quality, and the NCDEQ 2B Standards for surface water quality. Results
are summarized as follows:
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 LNAPL was not measured in the sampled monitoring wells;
 None of the detected concentrations in the monitoring well samples exceeded the GCLs;
 Monitoring wells MW-3, MW-4, MW-8, and MW-11 contained concentrations of at least
one petroleum constituent above the 2L Standard;
 Groundwater from monitoring wells MW-3, MW-4, MW-8, and MW-11 also contained one
or more petroleum constituent at concentrations more than 10 times 2B Standards; and
 TCE was detected at concentrations exceeding the 2L Standards in the sidegradient well,
MW-8, located south of Kelly’s Village Cleaners (232 South Main Avenue) which is an
active dry-cleaning facility located just east of the Exxon Service Station site. ATC has
previously recommended the incident manager contact DSCA for the possibility of a solvent
release associated with Kelly’s Village Cleaners. If no record, an investigation into the
likelyhood of a solvent release from KVC should be considered/reported to DSCA.

A benzene isoconcentration contour map is displayed as Figure 4. Other constituent concentrations
exceeding 2L standards are shown on a map as additional groundwater analytical results in Figure
5.

As part of ATC’s quality assurance and quality control (QA and QC) measures, a data review of the
laboratory reports was conducted. A field blank sample was collected for QA/QC purposes. During
the review, it was found that the samples were received from the laboratory in acceptable condition
and properly preserved. The samples were analyzed within correct holding times and reported
within the lab report, and the chain of custody was properly completed by all parties. The laboratory
QC report shows that an internal blank was analyzed for each method that was used for the original
samples. The laboratory fortified blank (LFB), laboratory control sample (LCS), and field blank
results were also provided for each analytical method. Refer to the laboratory report in Appendix
B for details regarding QA results for the laboratory samples and any noted exceptions. Overall,
ATC concludes that the laboratory results are usable and any exceptions do not significantly impact
the conclusions presented in this report.

5.0 CONCLUSIONS AND RECOMMENDATIONS

On behalf of the Trust Fund Branch of the UST Section, ATC has completed a Groundwater
Monitoring Report, and sampled six groundwater monitoring wells (MW-1SR, MW-3, MW-4,
MW-6, MW-8, and MW-11). The finding from the recent and previous assessment activities
indicate the following:

 Municipal water is available to the site and surrounding area, and potential water supply
wells have not been identified within 1,500 feet of the site;
 One surface water body, a tributary to Hildebran Creek, is located approximately 400 feet
southwest of the site;
 LNAPL was not measured in the sampled monitoring wells;
 Groundwater from monitoring wells MW-3, MW-4, MW-8, and MW-11 contained
concentrations of at least one constituent above the 2L Standards;
 Concentrations of one or more constituents exceeded to 2B Standards by more than 10 times
in wells MW-3, MW-4, MW-8, and MW-11;
 None of the detected concentrations in the monitoring well samples exceeded the GCLs;
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 TCE was, and has been, detected at concentrations exceeding to 2L Standards in the
sidegradient well, MW-8, located south of Kelly’s Village Cleaners (232 South Main
Avenue), just east of the site; and
 Groundwater flow is to the southwest.

Contaminant concentrations appear to be stable or decreasing. ATC recommends continued
monitored natural attenuation. However, ATC also recommends that the NCDEQ consider closing
the incident with a Notice of Residual Petroleum.

TABLES
TABLE 1
MONITORING WELL CONSTRUCTION DETAILS
EXXON SERVICE STATION
226 South Main Avenue
Newton, Catawba County, North Carolina 28658
NCDEQ Incident #23514
MW-1S 10/22/01 18.42-33.42 33.42 95.45
MW-1SR 10/05/17 20.40-35.40 35.40 97.23
MW-1D 12/13/01 55.19-65.19 65.19 95.82
MW-2 12/12/01 19.65-34.65 34.65 101.48
MW-3 12/12/01 17.19-32.19 32.19 92.66
MW-4 12/13/01 16.07-31.07 31.07 89.17
MW-5 05/16/02 16-31 31 81.45
MW-6 05/16/02 9-24 24 69.27
MW-7 05/16/02 11-26 26 74.70
MW-8 05/16/02 16-31 31 88.22
MW-9 08/07/02 10-25 25 81.61
MW-10 08/07/02 5-20 20 72.67
MW-11 03/04/19 17-32 32 95.73
Notes:
ft = feet
Elevations referenced to an arbitrary datum of 100 feet.
Top of Casing
Elevation
(ft)
Well
ID
Date
Installed
Screen
Interval
(ft)
Total
Depth
(ft)
TABLE 2
GROUNDWATER ELEVATION DATA
EXXON SERVICE STATION
226 South Main Avenue
Newton, Catawba County, North Carolina 28658
NCDEQ Incident #23514
12/14/01 25.21 70.24
06/08/16 NM - CNF NM - CNF
10/05/17 NM - CNF NM - CNF
10/05/17 24.08 73.15
03/04/19 20.15 77.08
10/29/19 21.28 75.95
12/14/01 25.06 70.76
06/08/16 NM - CNF NM - CNF
10/05/17 NM - CNF NM - CNF
03/04/19 NM - CNF NM - CNF
12/14/01 28.01 73.47
06/08/16 23.11 78.37
10/05/17 25.20 76.28
12/14/01 25.19 67.47
06/08/16 20.08 72.58
10/05/17 22.72 69.94
03/04/19 17.50 75.16
10/29/19 21.20 71.46
12/14/01 23.75 65.42
06/08/16 18.68 70.49
10/05/17 21.38 67.79
03/04/19 15.16 74.01
10/29/19 19.09 70.08
05/28/02 18.08 63.37
06/08/16 NM - CNF NM - CNF
10/05/17 NM - CNF NM - CNF
10/29/19 NM - CNF NM - CNF
05/28/02 8.84 60.43
06/08/16 5.69 63.58
10/05/17 7.48 61.79
03/04/19 3.72 65.55
10/29/19 8.61 60.66
05/28/02 13.17 61.53
06/08/16 9.71 64.99
10/05/17 NM NM
05/28/02 17.77 70.45
06/08/16 13.05 75.17
10/05/17 15.83 72.39
03/04/19 10.19 78.03
10/29/19 13.01 75.21
08/08/02 23.39 58.22
06/08/16 21.07 60.54
10/05/17 22.07 59.54
08/08/02 15.60 57.07
06/08/16 17.71 54.96
10/05/17 NM NM
03/05/19 18.65 77.08
10/29/19 20.26 75.47
Notes:
ft = feet NM = Not Measured
TOC = Top of Casing CNF = Could Not Find
Top of casing elevations referenced to an arbitrary datum of 100 feet.
Groundwater elevation calculated by [Top of Casing Elevation - Depth to Water] + [Free Product Thickness*0.8581]
MW-9 25
MW-8 31 88.22
MW-4 31.07 89.17
31
81.61
MW-11 32 95.73
81.45
MW-6 24 69.27
72.6720MW-10
MW-1S
MW-7 26
MW-2
MW-1SR
MW-1D
MW-5
35.40
MW-3 32.19
Groundwater
Elevation
(ft)
Well
ID
TOC
Elevation
(ft)
Depth to
Groundwater
(ft-TOC)
Total Well
Depth
(ft)
Gauging
Date
33.42 95.45
34.65 101.48
74.70
65.19 95.82
97.23
92.66
TABLE 3
RECENT GROUNDWATER ANALYTICAL RESULTS
EXXON SERVICE STATION
226 South Main Avenue
Newton, Catawba County, North Carolina 28658
NCDEQ Incident #23514
BenzeneTolueneEthylbenzeneXylene (Total)Methyl-tert-butyl etherNaphthaleneIsopropyl ether (IPE)1,2-DichloroethaneChloroformTetrachloroethenesec-ButylbenzeneIsopropylbenzene (Cumene)n-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneStyreneTrichloroethenecis-1,2-Dichloroethene2-HexanoneConcentrations in µg/L
SM 6200B
MW-1SR 10/29/19 <0.24 <0.23 <0.24 <0.50 0.53 <0.66 <0.33 <0.26 2.3 <0.23 <0.25 <0.24 <0.24 <0.19 <0.23 <0.26 <0.23 <0.21 5.3
MW-3 10/29/19 53.9 2,400 *288 1,290 <11.1 59.3 <8.4 <6.6 19.8 <5.8 <6.2 12.9 25.9 145 48.4 19.8 <5.8 <5.2 <15.1
MW-4 10/29/19 605 *185 190 152 14.1 102 87.5 <1.3 <1.8 2.6 <1.2 15.4 20.0 40.6 15.7 <1.3 <1.2 <1.0 <3.0
MW-5 10/29/19
MW-6 10/29/19 <0.24 <0.23 <0.24 <0.50 2.5 <0.66 9.1 <0.26 <0.35 <0.23 0.57 <0.24 <0.24 <0.19 <0.23 <0.26 <0.23 <0.21 <0.60
MW-8 10/29/19 <0.24 <0.23 <0.24 <0.50 <0.44 <0.66 <0.33 <0.26 16.6 56.7 *<0.25 <0.24 <0.24 <0.19 <0.23 <0.26 2.4 4.6 <0.60
MW-11 10/29/19 2,770 *46,800 *3,820 *20,500 *<222 734J *<167 <132 <176 <116 <123 <119 <120 2,550 <114 316 <116 <104 <302
1 600 600 500 20 6 70 0.4 70 0.7 70 70 70 400 400 70 3 70 40
51 11 68 670 1,500 12 20,000 650 2,000 4.0 NE 250 80 390 130 NE 30 720 NE
5,000 260,000 84,500 85,500 20,000 6,000 70,000 400 70,000 700 8,500 25,000 30,000 28,500 25,000 70,000 3,000 70,000 40,000
Notes:
Concentrations are reported in micrograms per liter (µg/L)
2L Standard = 15A NCAC 02L .0202 Groundwater Quality Standard
2B Standard = 15A NCAC 02B Surface Water Quality Standard (lower of Class C Freshwater, Aquatic Life, Fish Consumption)
GCL = Gross Contamination Level
J = Estimated value below laboratory reporting limit
Values in BOLD print exceed the 2L Standard; Values in BOLD-underlined print exceed the GCL; Value* exceed the 2B Standards by more than 10 times.
Not Sampled - Could Not Find
Well ID Sample
Date
Analytical Method
2L Standard
GCL Standard
2B Standard
TABLE 4
HISTORICAL GROUNDWATER ANALYTICAL RESULTS
EXXON SERVICE STATION
226 South Main Avenue
Newton, Catawba County, North Carolina 28658
NCDEQ Incident #23514
Well ID Sample
Date
BenzeneTolueneEthylbenzeneTotal XylenesMethyl Tertiary Butyl EtherNaphthaleneIsopropyl Ether (IPE)1,2-DichloroethaneChloroformTetrachloroethylenen-Butylbenzenesec-ButylbenzeneIsopropylbenzenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneStyreneTrichloroethenecis-1,2-DichloroetheneMethylene Chloridetert-Amyl Methyl EtherChlorobenzenep-Isopropyltoluene1 600 600 500 20 6 70 0.4 70 0.7 70 70 70 70 400 400 70 3 70 5 128 50 25
51 11 68 670 1,500 12 20,000 650 2,000 4 3.9 NE 250 80 390 130 NE 30 720 96 NE 140 320
5,000 260,000 84,500 85,500 20,000 6,000 70,000 400 70,000 700 6,900 8,500 25,000 30,000 28,500 25,000 70000 3000 70000 5000 12,800 50,000 11,700
10/23/01 98 900*160 920 290 31 70 NA <5.0 5 <1.0 <1.0 5.2 15 130 43 NA NA NA NA NA 1.2 NA
06/08/16
10/05/17
10/05/17 <0.12 <0.17 <0.13 <0.39 0.45 J <0.12 <0.18 NA 5 <0.27 <0.15 <0.13 <0.12 <0.13 <0.18 <0.13 NA NA NA NA NA <0.16 <0.15
03/05/19 ND ND ND ND 0.40J ND ND ND 3.4 ND ND ND ND ND ND ND ND ND ND ND NA NA NA
10/29/19 <0.24 <0.23 <0.24 <0.50 0.53 <0.66 <0.33 <0.26 2.3 <0.23 <0.35 <0.25 <0.24 <0.24 <0.19 <0.23 <0.26 <0.23 <0.21 <1.5 NA <0.22 NA
12/14/01 <1.0 BQL BQL BQL BQL BQL BQL NA <5.0 BQL <1.0 <1.0 BQL BQL BQL BQL NA NA NA NA N/A <1.0 N/A
06/08/16
10/05/17
03/04/19
12/14/01 <1.0 BQL BQL BQL BQL BQL BQL NA <5.0 BQL <1.0 <1.0 BQL BQL BQL BQL NA NA NA NA N/A <1.0 N/A
06/08/16 <0.12 <0.17 <0.13 <0.38 <0.090 <0.12 <0.18 NA <0.22 <0.17 <0.15 <0.13 <0.12 <0.13 <0.18 <0.13 NA NA NA NA <0.091 <0.16 <0.15
10/05/17 <0.12 <0.17 <0.13 <0.39 <0.090 <0.12 <0.18 NA <0.22 <0.17 <0.15 <0.13 <0.12 <0.13 <0.18 <0.13 NA NA NA NA NA <0.16 <0.15
12/14/01 13,000 130,000 *23,000 *128,000 3,000 8,200 2,600 NA N/A BQL N/A N/A 4,900 *5,700 *31,000 9,300 *NA NA NA NA N/A BQL N/A
06/08/16 180 3,600 520 2,020 <4.5 100 <9.0 NA <11 <8.5 64 18 J 27 J 74 440 270 NA NA NA NA <4.6 <8.0 12 J
10/05/17 96 4,000 830 3,900 <2.2 130 <4.5 NA <5.5 <6.8 16 6.2 J 37 89 580 190 NA NA NA NA NA <4.0 3.8 J
03/05/19 52.2 1,780 249 1088 ND 52.2 ND ND ND 4.1J ND ND 10.3 25.4 197 120 16.1 ND ND ND NA NA NA
10/29/19 53.9 2,400 *288 1,290 <11.1 59.3 <8.4 <6.6 19.8 <5.8 <8.8 <6.2 12.9 25.9 145 48.4 19.8 <5.8 <5.2 <37.5 NA <5.6 NA
12/14/01 3,100 BQL 410 BQL 19,000 BQL 4,500 NA <1,200 BQL <250 <250 BQL BQL BQL BQL NA NA NA NA N/A <250 N/A
06/08/16 1,600 180 490 230 48 190 320 NA <4.4 <3.4 <3.0 7.2 J 37 49 41 24 NA NA NA NA 55 <3.2 <3.0
10/05/17 1,100 210 300 196 40 200 180 NA <1.1 <1.4 8 5 32 31 17 19 NA NA NA NA NA <0.80 1.0 J
03/04/19 267 27.5 38.4 14.6 20.1 51.8 96.6 0.91J ND 1.8 ND 3.0 7.9 3.5 ND 3.0 ND ND ND ND NA NA NA
10/29/19 605 *185 190 152 14.1 102 87.5 <1.3 <1.8 2.6 <1.8 <1.2 15.4 20.0 40.6 15.7 <1.3 <1.2 <1.0 <7.5 NA <1.1 NA
Concentrations in µg/L
Analytical Method SM 6200B 1
2L Standard
2B Standard
GCL Standard
MW-1S Could Not Find - Well Not Sampled
Could Not Find - Well Not Sampled
MW-1SR
MW-1D Could Not Find - Well Not Sampled
Could Not Find - Well Not Sampled
Could Not Find - Well Not Sampled
MW-2
MW-3
MW-4
Page 1 of 3
TABLE 4
HISTORICAL GROUNDWATER ANALYTICAL RESULTS
EXXON SERVICE STATION
226 South Main Avenue
Newton, Catawba County, North Carolina 28658
NCDEQ Incident #23514
Well ID Sample
Date
BenzeneTolueneEthylbenzeneTotal XylenesMethyl Tertiary Butyl EtherNaphthaleneIsopropyl Ether (IPE)1,2-DichloroethaneChloroformTetrachloroethylenen-Butylbenzenesec-ButylbenzeneIsopropylbenzenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneStyreneTrichloroethenecis-1,2-DichloroetheneMethylene Chloridetert-Amyl Methyl EtherChlorobenzenep-Isopropyltoluene1 600 600 500 20 6 70 0.4 70 0.7 70 70 70 70 400 400 70 3 70 5 128 50 25
51 11 68 670 1,500 12 20,000 650 2,000 4 3.9 NE 250 80 390 130 NE 30 720 96 NE 140 320
5,000 260,000 84,500 85,500 20,000 6,000 70,000 400 70,000 700 6,900 8,500 25,000 30,000 28,500 25,000 70000 3000 70000 5000 12,800 50,000 11,700
Concentrations in µg/L
Analytical Method SM 6200B 1
2L Standard
2B Standard
GCL Standard
05/28/02 1.7 <1.0 <1.0 <1.0 13 NA <1.0 NA <1.0 1.8 NA NA NA NA NA NA NA NA NA NA NA <1.0 NA
06/08/16
10/05/17
10/29/19
05/28/02 130 1.6 <1.0 1.6 1,100 NA 610 NA <1.0 1.3 NA NA NA NA NA NA NA NA NA NA NA <1.0 NA
06/08/16 2.7 <0.17 <0.13 <0.38 9.2 <0.12 21 NA <0.22 <0.17 <0.15 1.0 1.1 <0.13 <0.18 <0.13 NA NA NA NA 2.9 <0.16 <0.15
10/05/17 <0.12 <0.17 <0.13 <0.39 10.0 <0.12 29 NA <0.22 <0.27 <0.15 <0.13 <0.12 <0.13 <0.18 <0.13 NA NA NA NA NA <0.16 <0.15
03/04/19 ND ND ND ND 6.6 ND 30.0 ND ND ND ND ND ND ND ND ND ND ND ND ND NA NA NA
10/29/19 <0.24 <0.23 <0.24 <0.50 2.5 <0.66 9.1 <0.26 <0.35 <0.23 <0.35 0.57 <0.24 <0.24 <0.19 <0.23 <0.26 <0.23 <0.21 <1.5 NA <0.22 NA
05/28/02 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 NA <1.0 <1.0 NA NA NA NA NA NA NA NA NA NA NA <1.0 NA
06/08/16 <0.12 <0.17 <0.13 <0.38 <0.090 <0.12 <0.18 NA <0.22 <0.17 <0.15 <0.13 <0.12 <0.13 <0.18 <0.13 NA NA NA NA <0.091 <0.16 <0.15
10/05/17
05/28/02 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 NA 4.9 36 NA NA NA NA NA NA NA NA NA NA NA <1.0 NA
06/08/16 <0.12 <0.17 <0.13 <0.38 <0.090 <0.12 <0.18 NA 29 11 <0.15 <0.13 <0.12 <0.13 <0.18 <0.13 NA NA NA NA <0.091 <0.16 <0.15
10/05/17 <0.12 <0.17 <0.13 <0.39 <0.090 <0.12 <0.18 NA 26 28 <0.15 <0.13 <0.12 <0.13 <0.18 <0.13 NA NA NA NA NA NA <0.15
03/05/19 ND ND ND ND ND ND ND ND 15.9 41.4 *ND ND ND ND ND ND ND 1.8 3.7 ND NA NA NA
10/29/19 <0.24 <0.23 <0.24 <0.50 <0.44 <0.66 <0.33 <0.26 16.6 56.7 *<0.35 <0.25 <0.24 <0.24 <0.19 <0.23 <0.26 2.4 4.6 <1.5 NA <0.22 NA
08/08/02 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 NA 3.5 <1.0 NA NA NA NA NA NA NA NA NA NA NA <1.0 NA
06/08/16 <0.12 <0.17 <0.13 <0.38 <0.090 <0.12 <0.18 NA 3.6 <0.17 <0.15 <0.13 <0.12 <0.13 <0.18 <0.13 NA NA NA NA <0.091 <0.16 <0.15
10/05/17 <0.12 <0.17 <0.13 <0.39 <0.090 <0.12 <0.18 NA 6.9 0.29 J <0.15 <0.13 <0.12 <0.13 <0.18 <0.13 NA NA NA NA NA <0.16 <0.15
08/08/02 <1.0 <1.0 <1.0 <1.0 <1.0 NA <1.0 NA 13 <1.0 NA NA NA NA NA NA NA NA NA NA NA <1.0 NA
06/08/16 <0.12 <0.17 <0.13 <0.38 <0.090 <0.12 <0.18 NA <0.22 <0.17 <0.15 <0.13 <0.12 <0.13 <0.18 <0.13 NA NA NA NA <0.091 <0.16 <0.15
10/05/17
MW-5 Could Not Find - Well Not Sampled
Could Not Find - Well Not Sampled
Could Not Find - Well Not Sampled
MW-6
MW-7
Well Not Sampled
MW-8
MW-9
MW-10
Well Not Sampled
Page 2 of 3
TABLE 4
HISTORICAL GROUNDWATER ANALYTICAL RESULTS
EXXON SERVICE STATION
226 South Main Avenue
Newton, Catawba County, North Carolina 28658
NCDEQ Incident #23514
Well ID Sample
Date
BenzeneTolueneEthylbenzeneTotal XylenesMethyl Tertiary Butyl EtherNaphthaleneIsopropyl Ether (IPE)1,2-DichloroethaneChloroformTetrachloroethylenen-Butylbenzenesec-ButylbenzeneIsopropylbenzenen-Propylbenzene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneStyreneTrichloroethenecis-1,2-DichloroetheneMethylene Chloridetert-Amyl Methyl EtherChlorobenzenep-Isopropyltoluene1 600 600 500 20 6 70 0.4 70 0.7 70 70 70 70 400 400 70 3 70 5 128 50 25
51 11 68 670 1,500 12 20,000 650 2,000 4 3.9 NE 250 80 390 130 NE 30 720 96 NE 140 320
5,000 260,000 84,500 85,500 20,000 6,000 70,000 400 70,000 700 6,900 8,500 25,000 30,000 28,500 25,000 70000 3000 70000 5000 12,800 50,000 11,700
Concentrations in µg/L
Analytical Method SM 6200B 1
2L Standard
2B Standard
GCL Standard
03/05/19 4,530 *74,500 *5,380 *28,100 *ND 601J *ND ND ND ND ND ND 164J ND 2,690 ND 470 ND ND ND NA NA NA
10/29/19 2,770 *46,800 *3,820 *20,500 *<222 734J *<167 <132 <176 <116 <176 <123 <119 <120 2,550 <114 316 <116 <104 <750 NA <112 NA
Notes:
Concentrations are reported in micrograms per liter (µg/l) or parts per billion equivalents NE = Not Established
2L Standard = 15A NCAC 02L .0202 Groundwater Quality Standard NA = Not Analyzed for specified parameter
GCL = Gross Contamination Level J = Estimated value below method detection limit
Values in BOLD print exceed the 2L Standard; Values in BOLD-underlined print exceed the GCL BQL = Below Quantitation Limit (laboratory report not available for method detection limits)
Value* exceed the 2B Standards by more than 10 times.
1 Samples from 12/14/2001 and earlier were analyzed for volatiles by EPA Method 6210D. Samples collected in 2002 were analyzed for volatiles by EPA Method 8260B.
MW-11
Page 3 of 3

FIGURES

SITE
CAD FILE PREP. BYTYPE CODE REV. BY SCALE PROJECT NO.
TITLE
DATE
REFERENCE: USGS 7.5-MINUTE MAP, NEWTON, NORTH CAROLINA.
DATED 2016
LATITUDE:ƒ1257+
LONGITUDE:ƒ:(67
LB 12/10/19 3
EXXON SERVICE STATION - NCDEQ INCIDENT #23514
MW-1S
MW-1D
MW-2
MW-3
MW-4
MW-5
MW-6
MW-7
MW-8
MW-9
MW-10
East D

S
t
r
e
e
t
South Main AvenueSouth Ashe AvenueSouth Bost AvenueFORMER WASTE OIL UST
SITE
FORMER UST BASIN
FORMER
DISPENSER ISLAND
FORMER
DISPENSER ISLAND
MW-11
CAD FILE PREP. BYTYPE CODE REV. BY SCALE PROJECT NO.
TITLE
DATE
EXPLANATION
MONITORING WELL LOCATION
IMAGE SOURCE: NC GEOSPATIAL DATABASE
LB 12/10/19 3
EXXON SERVICE STATION - NCDEQ INCIDENT #23514
MW-6
MW-7
MW-9
East D

S
t
r
e
e
tSouth Bost AvenueFORMER WASTE OIL UST
FORMER
DISPENSER ISLAND
MW-1SR
FORMER
DISPENSER ISLAND
MW-1D
MW-2
MW-3
MW-4
MW-5
MW-8
MW-10 South Main AvenueSouth Ashe AvenueFORMER UST BASIN
MW-11
SITE
75.95
CAD FILE PREP. BYTYPE CODE REV. BY SCALE PROJECT NO.
TITLE
DATE
ASSOCIATES OF NORTH CAROLINA, P.C.
C:\Users\robert.deppensmith\Desktop\CAD REFERENCES\ATC Logo_Full Color_CMYK.jpg
EXPLANATION
MONITORING WELL LOCATION
GROUNDWATER ELEVATION (AT WELL)
GROUNDWATER CONTOUR LINE
GROUNDWATER FLOW DIRECTION
77.08
NOTES:
1.GROUNDWATER LEVELS MEASURED ON
10/29/19.
2. DASHED LINES INDICATE AREAS OF LESS
CERTAINTY.
75.47
71.46
70.08
NL
75.21
NM
60.66
NM
NM
NM
NM
NOT LOCATED
NL NOT MEASUREDNM
75.070.065
.
0
EXXON SERVICE STATION - NCDEQ INCIDENT #23514
MW-6
MW-7
MW-9
East D

S
t
r
e
e
tSouth Bost AvenueFORMER WASTE OIL UST
FORMER
DISPENSER ISLAND
MW-1SR
FORMER
DISPENSER ISLAND
MW-1D
MW-2
MW-3
MW-4
MW-5
MW-8
MW-10 South Main AvenueSouth Ashe AvenueFORMER UST BASIN
MW-11
SITE
CAD FILE PREP. BYTYPE CODE REV. BY SCALE PROJECT NO.
TITLE
DATE
ASSOCIATES OF NORTH CAROLINA, P.C.
C:\Users\robert.deppensmith\Desktop\CAD REFERENCES\ATC Logo_Full Color_CMYK.jpg
EXPLANATION
MONITORING WELL LOCATION
NOTES:
1.GROUNDWATER SAMPLES TAKEN ON
10/29/19.
2. DASHED LINES INDICATE AREAS OF LESS
CERTAINTY.
<0.24
2,770
53.9
605
NL
NS
BENZENE CONCENTRATION (ug/L)
BENZENE ISOCONCENTRATIONCONTOUR LINE1,780
NS
NS
NS
NS
<0.24
<0.24
2,000
u
g/
L
1 ug/LNOT LOCATED
NL NOT SAMPLEDNS
EXXON SERVICE STATION - NCDEQ INCIDENT #23514
MW-6
MW-7
MW-9
East D

S
t
r
e
e
tSouth Bost AvenueFORMER WASTE OIL UST
FORMER
DISPENSER ISLAND
MW-1SR
FORMER
DISPENSER ISLAND
MW-1D
MW-2
MW-3
MW-4
MW-5
MW-8
MW-10 South Main AvenueSouth Ashe AvenueFORMER UST BASIN
MW-11
SITE
CAD FILE PREP. BYTYPE CODE REV. BY SCALE PROJECT NO.
TITLE
DATE
ASSOCIATES OF NORTH CAROLINA, P.C.
C:\Users\robert.deppensmith\Desktop\CAD REFERENCES\ATC Logo_Full Color_CMYK.jpg
EXPLANATION
MONITORING WELL LOCATION
NOTES:
1.GROUNDWATER SAMPLES TAKEN ON
10/29/19.
NL
NS
NS
NS
NS
NS
NOT LOCATEDNLNOT SAMPLEDNS
EXXON SERVICE STATION - NCDEQ INCIDENT #23514

APPENDIX A

FIELD NOTES

APPENDIX B

LABORATORY ANALYTICAL REPORT

#=CL#
November 05, 2019
LIMS USE: FR - ERIN GREENE
LIMS OBJECT ID: 92451624
92451624
Project:
Pace Project No.:
RE:
Erin Greene
ATC Group
7606 Whitehall Executive Cente
Suite 800
Charlotte, NC 28273
Former Newton
Dear Erin Greene:
Enclosed are the analytical results for sample(s) received by the laboratory on October 30, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 31
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92451624
Former Newton
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 31
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92451624
Former Newton
Lab ID Sample ID Matrix Date Collected Date Received
92451624001 FB-1 Water 10/29/19 11:29 10/30/19 10:11
92451624002 MW-1SR Water 10/29/19 12:19 10/30/19 10:11
92451624003 MW-3 Water 10/29/19 15:32 10/30/19 10:11
92451624004 MW-4 Water 10/29/19 14:58 10/30/19 10:11
92451624005 MW-6 Water 10/29/19 14:21 10/30/19 10:11
92451624006 MW-8 Water 10/29/19 13:39 10/30/19 10:11
92451624007 MW-11 Water 10/29/19 12:58 10/30/19 10:11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 31
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92451624
Former Newton
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92451624001 FB-1 SM 6200B 66 PASI-CSAS
92451624002 MW-1SR SM 6200B 66 PASI-CSAS
92451624003 MW-3 SM 6200B 66 PASI-CCL
92451624004 MW-4 SM 6200B 66 PASI-CCL
92451624005 MW-6 SM 6200B 66 PASI-CSAS
92451624006 MW-8 SM 6200B 66 PASI-CSAS
92451624007 MW-11 SM 6200B 66 PASI-CSAS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451624
Former Newton
Sample:FB-1 Lab ID:92451624001 Collected:10/29/19 11:29 Received:10/30/19 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Benzene <0.24 ug/L 11/01/19 14:13 71-43-20.50 0.24 1
Bromobenzene <0.22 ug/L 11/01/19 14:13 108-86-10.50 0.22 1
Bromochloromethane <0.26 ug/L 11/01/19 14:13 74-97-50.50 0.26 1
Bromodichloromethane <0.18 ug/L 11/01/19 14:13 75-27-40.50 0.18 1
Bromoform <0.40 ug/L 11/01/19 14:13 75-25-20.50 0.40 1
Bromomethane <1.7 ug/L 11/01/19 14:13 74-83-95.0 1.7 1
2-Butanone (MEK)<3.6 ug/L 11/01/19 14:13 78-93-35.0 3.6 1
n-Butylbenzene <0.35 ug/L 11/01/19 14:13 104-51-80.50 0.35 1
sec-Butylbenzene <0.25 ug/L 11/01/19 14:13 135-98-80.50 0.25 1
tert-Butylbenzene <0.25 ug/L 11/01/19 14:13 98-06-60.50 0.25 1
Carbon tetrachloride <0.23 ug/L 11/01/19 14:13 56-23-50.50 0.23 1
Chlorobenzene <0.22 ug/L 11/01/19 14:13 108-90-70.50 0.22 1
Chloroethane <0.58 ug/L 11/01/19 14:13 75-00-31.0 0.58 1
Chloroform <0.35 ug/L 11/01/19 14:13 67-66-30.50 0.35 1
Chloromethane <0.42 ug/L 11/01/19 14:13 74-87-31.0 0.42 1
2-Chlorotoluene <0.21 ug/L 11/01/19 14:13 95-49-80.50 0.21 1
4-Chlorotoluene <0.21 ug/L 11/01/19 14:13 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane <0.38 ug/L 11/01/19 14:13 96-12-81.0 0.38 1
Dibromochloromethane <0.40 ug/L 11/01/19 14:13 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)<0.23 ug/L 11/01/19 14:13 106-93-40.50 0.23 1
Dibromomethane <0.31 ug/L 11/01/19 14:13 74-95-30.50 0.31 1
1,2-Dichlorobenzene <0.24 ug/L 11/01/19 14:13 95-50-10.50 0.24 1
1,3-Dichlorobenzene <0.25 ug/L 11/01/19 14:13 541-73-10.50 0.25 1
1,4-Dichlorobenzene <0.25 ug/L 11/01/19 14:13 106-46-70.50 0.25 1
Dichlorodifluoromethane <0.28 ug/L 11/01/19 14:13 75-71-80.50 0.28 1
1,1-Dichloroethane <0.24 ug/L 11/01/19 14:13 75-34-30.50 0.24 1
1,2-Dichloroethane <0.26 ug/L 11/01/19 14:13 107-06-20.50 0.26 1
1,1-Dichloroethene <0.22 ug/L 11/01/19 14:13 75-35-40.50 0.22 1
cis-1,2-Dichloroethene <0.21 ug/L 11/01/19 14:13 156-59-20.50 0.21 1
trans-1,2-Dichloroethene <0.26 ug/L 11/01/19 14:13 156-60-50.50 0.26 1
1,2-Dichloropropane <0.18 ug/L 11/01/19 14:13 78-87-50.50 0.18 1
1,3-Dichloropropane <0.34 ug/L 11/01/19 14:13 142-28-90.50 0.34 1
2,2-Dichloropropane <0.28 ug/L 11/01/19 14:13 594-20-70.50 0.28 1
1,1-Dichloropropene <0.35 ug/L 11/01/19 14:13 563-58-60.50 0.35 1
cis-1,3-Dichloropropene <0.36 ug/L 11/01/19 14:13 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.39 ug/L 11/01/19 14:13 10061-02-60.50 0.39 1
Diisopropyl ether <0.33 ug/L 11/01/19 14:13 108-20-30.50 0.33 1
Ethylbenzene <0.24 ug/L 11/01/19 14:13 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene <1.2 ug/L 11/01/19 14:13 87-68-32.0 1.2 1
2-Hexanone <0.60 ug/L 11/01/19 14:13 591-78-65.0 0.60 1
Isopropylbenzene (Cumene)<0.24 ug/L 11/01/19 14:13 98-82-80.50 0.24 1
Methylene Chloride <1.5 ug/L 11/01/19 14:13 75-09-22.0 1.5 1
Methyl-tert-butyl ether <0.44 ug/L 11/01/19 14:13 1634-04-40.50 0.44 1
Naphthalene <0.66 ug/L 11/01/19 14:13 91-20-32.0 0.66 1
n-Propylbenzene <0.24 ug/L 11/01/19 14:13 103-65-10.50 0.24 1
Styrene <0.26 ug/L 11/01/19 14:13 100-42-50.50 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451624
Former Newton
Sample:FB-1 Lab ID:92451624001 Collected:10/29/19 11:29 Received:10/30/19 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
1,1,1,2-Tetrachloroethane <0.42 ug/L 11/01/19 14:13 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane <0.19 ug/L 11/01/19 14:13 79-34-50.50 0.19 1
Tetrachloroethene <0.23 ug/L 11/01/19 14:13 127-18-40.50 0.23 1
Toluene <0.23 ug/L 11/01/19 14:13 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene <0.78 ug/L 11/01/19 14:13 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene <0.44 ug/L 11/01/19 14:13 120-82-12.0 0.44 1
1,1,1-Trichloroethane <0.28 ug/L 11/01/19 14:13 71-55-60.50 0.28 1
1,1,2-Trichloroethane <0.23 ug/L 11/01/19 14:13 79-00-50.50 0.23 1
Trichloroethene <0.23 ug/L 11/01/19 14:13 79-01-60.50 0.23 1
Trichlorofluoromethane <0.34 ug/L 11/01/19 14:13 75-69-41.0 0.34 1
1,2,3-Trichloropropane <0.27 ug/L 11/01/19 14:13 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene <0.19 ug/L 11/01/19 14:13 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene <0.23 ug/L 11/01/19 14:13 108-67-80.50 0.23 1
Vinyl chloride <0.41 ug/L 11/01/19 14:13 75-01-41.0 0.41 1
Xylene (Total)<0.50 ug/L 11/01/19 14:13 1330-20-71.0 0.50 1
m&p-Xylene <0.44 ug/L 11/01/19 14:13 179601-23-11.0 0.44 1
o-Xylene <0.24 ug/L 11/01/19 14:13 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %11/01/19 14:13 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %11/01/19 14:13 460-00-470-130 1
Toluene-d8 (S)105 %11/01/19 14:13 2037-26-570-130 1
Sample:MW-1SR Lab ID:92451624002 Collected:10/29/19 12:19 Received:10/30/19 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Benzene <0.24 ug/L 11/01/19 15:07 71-43-20.50 0.24 1
Bromobenzene <0.22 ug/L 11/01/19 15:07 108-86-10.50 0.22 1
Bromochloromethane <0.26 ug/L 11/01/19 15:07 74-97-50.50 0.26 1
Bromodichloromethane <0.18 ug/L 11/01/19 15:07 75-27-40.50 0.18 1
Bromoform <0.40 ug/L 11/01/19 15:07 75-25-20.50 0.40 1
Bromomethane <1.7 ug/L 11/01/19 15:07 74-83-95.0 1.7 1
2-Butanone (MEK)<3.6 ug/L 11/01/19 15:07 78-93-35.0 3.6 1
n-Butylbenzene <0.35 ug/L 11/01/19 15:07 104-51-80.50 0.35 1
sec-Butylbenzene <0.25 ug/L 11/01/19 15:07 135-98-80.50 0.25 1
tert-Butylbenzene <0.25 ug/L 11/01/19 15:07 98-06-60.50 0.25 1
Carbon tetrachloride <0.23 ug/L 11/01/19 15:07 56-23-50.50 0.23 1
Chlorobenzene <0.22 ug/L 11/01/19 15:07 108-90-70.50 0.22 1
Chloroethane <0.58 ug/L 11/01/19 15:07 75-00-31.0 0.58 1
Chloroform 2.3 ug/L 11/01/19 15:07 67-66-30.50 0.35 1
Chloromethane <0.42 ug/L 11/01/19 15:07 74-87-31.0 0.42 1
2-Chlorotoluene <0.21 ug/L 11/01/19 15:07 95-49-80.50 0.21 1
4-Chlorotoluene <0.21 ug/L 11/01/19 15:07 106-43-40.50 0.21 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451624
Former Newton
Sample:MW-1SR Lab ID:92451624002 Collected:10/29/19 12:19 Received:10/30/19 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
1,2-Dibromo-3-chloropropane <0.38 ug/L 11/01/19 15:07 96-12-81.0 0.38 1
Dibromochloromethane <0.40 ug/L 11/01/19 15:07 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)<0.23 ug/L 11/01/19 15:07 106-93-40.50 0.23 1
Dibromomethane <0.31 ug/L 11/01/19 15:07 74-95-30.50 0.31 1
1,2-Dichlorobenzene <0.24 ug/L 11/01/19 15:07 95-50-10.50 0.24 1
1,3-Dichlorobenzene <0.25 ug/L 11/01/19 15:07 541-73-10.50 0.25 1
1,4-Dichlorobenzene <0.25 ug/L 11/01/19 15:07 106-46-70.50 0.25 1
Dichlorodifluoromethane <0.28 ug/L 11/01/19 15:07 75-71-80.50 0.28 1
1,1-Dichloroethane <0.24 ug/L 11/01/19 15:07 75-34-30.50 0.24 1
1,2-Dichloroethane <0.26 ug/L 11/01/19 15:07 107-06-20.50 0.26 1
1,1-Dichloroethene <0.22 ug/L 11/01/19 15:07 75-35-40.50 0.22 1
cis-1,2-Dichloroethene <0.21 ug/L 11/01/19 15:07 156-59-20.50 0.21 1
trans-1,2-Dichloroethene <0.26 ug/L 11/01/19 15:07 156-60-50.50 0.26 1
1,2-Dichloropropane <0.18 ug/L 11/01/19 15:07 78-87-50.50 0.18 1
1,3-Dichloropropane <0.34 ug/L 11/01/19 15:07 142-28-90.50 0.34 1
2,2-Dichloropropane <0.28 ug/L 11/01/19 15:07 594-20-70.50 0.28 1
1,1-Dichloropropene <0.35 ug/L 11/01/19 15:07 563-58-60.50 0.35 1
cis-1,3-Dichloropropene <0.36 ug/L 11/01/19 15:07 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.39 ug/L 11/01/19 15:07 10061-02-60.50 0.39 1
Diisopropyl ether <0.33 ug/L 11/01/19 15:07 108-20-30.50 0.33 1
Ethylbenzene <0.24 ug/L 11/01/19 15:07 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene <1.2 ug/L 11/01/19 15:07 87-68-32.0 1.2 1
2-Hexanone 5.3 ug/L 11/01/19 15:07 591-78-65.0 0.60 1
Isopropylbenzene (Cumene)<0.24 ug/L 11/01/19 15:07 98-82-80.50 0.24 1
Methylene Chloride <1.5 ug/L 11/01/19 15:07 75-09-22.0 1.5 1
Methyl-tert-butyl ether 0.53 ug/L 11/01/19 15:07 1634-04-40.50 0.44 1
Naphthalene <0.66 ug/L 11/01/19 15:07 91-20-32.0 0.66 1
n-Propylbenzene <0.24 ug/L 11/01/19 15:07 103-65-10.50 0.24 1
Styrene <0.26 ug/L 11/01/19 15:07 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane <0.42 ug/L 11/01/19 15:07 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane <0.19 ug/L 11/01/19 15:07 79-34-50.50 0.19 1
Tetrachloroethene <0.23 ug/L 11/01/19 15:07 127-18-40.50 0.23 1
Toluene <0.23 ug/L 11/01/19 15:07 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene <0.78 ug/L 11/01/19 15:07 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene <0.44 ug/L 11/01/19 15:07 120-82-12.0 0.44 1
1,1,1-Trichloroethane <0.28 ug/L 11/01/19 15:07 71-55-60.50 0.28 1
1,1,2-Trichloroethane <0.23 ug/L 11/01/19 15:07 79-00-50.50 0.23 1
Trichloroethene <0.23 ug/L 11/01/19 15:07 79-01-60.50 0.23 1
Trichlorofluoromethane <0.34 ug/L 11/01/19 15:07 75-69-41.0 0.34 1
1,2,3-Trichloropropane <0.27 ug/L 11/01/19 15:07 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene <0.19 ug/L 11/01/19 15:07 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene <0.23 ug/L 11/01/19 15:07 108-67-80.50 0.23 1
Vinyl chloride <0.41 ug/L 11/01/19 15:07 75-01-41.0 0.41 1
Xylene (Total)<0.50 ug/L 11/01/19 15:07 1330-20-71.0 0.50 1
m&p-Xylene <0.44 ug/L 11/01/19 15:07 179601-23-11.0 0.44 1
o-Xylene <0.24 ug/L 11/01/19 15:07 95-47-60.50 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451624
Former Newton
Sample:MW-1SR Lab ID:92451624002 Collected:10/29/19 12:19 Received:10/30/19 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Surrogates
1,2-Dichloroethane-d4 (S)99 %11/01/19 15:07 17060-07-070-130 1
4-Bromofluorobenzene (S)95 %11/01/19 15:07 460-00-470-130 1
Toluene-d8 (S)101 %11/01/19 15:07 2037-26-570-130 1
Sample:MW-3 Lab ID:92451624003 Collected:10/29/19 15:32 Received:10/30/19 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Benzene 53.9 ug/L 11/04/19 18:09 71-43-212.5 6.0 25
Bromobenzene <5.4 ug/L 11/04/19 18:09 108-86-112.5 5.4 25
Bromochloromethane <6.4 ug/L 11/04/19 18:09 74-97-512.5 6.4 25
Bromodichloromethane <4.6 ug/L 11/04/19 18:09 75-27-412.5 4.6 25
Bromoform <10.1 ug/L 11/04/19 18:09 75-25-212.5 10.1 25
Bromomethane <43.0 ug/L 11/04/19 18:09 74-83-9 M112543.0 25
2-Butanone (MEK)<89.8 ug/L 11/04/19 18:09 78-93-312589.8 25
n-Butylbenzene <8.8 ug/L 11/04/19 18:09 104-51-812.5 8.8 25
sec-Butylbenzene <6.2 ug/L 11/04/19 18:09 135-98-812.5 6.2 25
tert-Butylbenzene <6.2 ug/L 11/04/19 18:09 98-06-612.5 6.2 25
Carbon tetrachloride <5.8 ug/L 11/04/19 18:09 56-23-512.5 5.8 25
Chlorobenzene <5.6 ug/L 11/04/19 18:09 108-90-712.5 5.6 25
Chloroethane <14.6 ug/L 11/04/19 18:09 75-00-325.0 14.6 25
Chloroform 19.8 ug/L 11/04/19 18:09 67-66-312.5 8.8 25
Chloromethane <10.4 ug/L 11/04/19 18:09 74-87-325.0 10.4 25
2-Chlorotoluene <5.2 ug/L 11/04/19 18:09 95-49-812.5 5.2 25
4-Chlorotoluene <5.2 ug/L 11/04/19 18:09 106-43-412.5 5.2 25
1,2-Dibromo-3-chloropropane <9.6 ug/L 11/04/19 18:09 96-12-825.0 9.6 25
Dibromochloromethane <10.0 ug/L 11/04/19 18:09 124-48-112.5 10.0 25
1,2-Dibromoethane (EDB)<5.8 ug/L 11/04/19 18:09 106-93-412.5 5.8 25
Dibromomethane <7.8 ug/L 11/04/19 18:09 74-95-312.5 7.8 25
1,2-Dichlorobenzene <6.0 ug/L 11/04/19 18:09 95-50-112.5 6.0 25
1,3-Dichlorobenzene <6.2 ug/L 11/04/19 18:09 541-73-112.5 6.2 25
1,4-Dichlorobenzene <6.2 ug/L 11/04/19 18:09 106-46-712.5 6.2 25
Dichlorodifluoromethane <7.1 ug/L 11/04/19 18:09 75-71-812.5 7.1 25
1,1-Dichloroethane <6.1 ug/L 11/04/19 18:09 75-34-312.5 6.1 25
1,2-Dichloroethane <6.6 ug/L 11/04/19 18:09 107-06-212.5 6.6 25
1,1-Dichloroethene <5.4 ug/L 11/04/19 18:09 75-35-412.5 5.4 25
cis-1,2-Dichloroethene <5.2 ug/L 11/04/19 18:09 156-59-212.5 5.2 25
trans-1,2-Dichloroethene <6.4 ug/L 11/04/19 18:09 156-60-512.5 6.4 25
1,2-Dichloropropane <4.6 ug/L 11/04/19 18:09 78-87-512.5 4.6 25
1,3-Dichloropropane <8.5 ug/L 11/04/19 18:09 142-28-912.5 8.5 25
2,2-Dichloropropane <7.0 ug/L 11/04/19 18:09 594-20-712.5 7.0 25
1,1-Dichloropropene <8.7 ug/L 11/04/19 18:09 563-58-612.5 8.7 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451624
Former Newton
Sample:MW-3 Lab ID:92451624003 Collected:10/29/19 15:32 Received:10/30/19 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
cis-1,3-Dichloropropene <8.9 ug/L 11/04/19 18:09 10061-01-512.5 8.9 25
trans-1,3-Dichloropropene <9.8 ug/L 11/04/19 18:09 10061-02-612.5 9.8 25
Diisopropyl ether <8.4 ug/L 11/04/19 18:09 108-20-312.5 8.4 25
Ethylbenzene 288 ug/L 11/04/19 18:09 100-41-412.5 6.0 25
Hexachloro-1,3-butadiene <30.0 ug/L 11/04/19 18:09 87-68-350.0 30.0 25
2-Hexanone <15.1 ug/L 11/04/19 18:09 591-78-612515.1 25
Isopropylbenzene (Cumene)12.9 ug/L 11/04/19 18:09 98-82-812.5 6.0 25
Methylene Chloride <37.5 ug/L 11/04/19 18:09 75-09-250.0 37.5 25
Methyl-tert-butyl ether <11.1 ug/L 11/04/19 18:09 1634-04-412.5 11.1 25
Naphthalene 59.3 ug/L 11/04/19 18:09 91-20-350.0 16.5 25
n-Propylbenzene 25.9 ug/L 11/04/19 18:09 103-65-112.5 6.0 25
Styrene 19.8 ug/L 11/04/19 18:09 100-42-512.5 6.4 25
1,1,1,2-Tetrachloroethane <10.6 ug/L 11/04/19 18:09 630-20-612.5 10.6 25
1,1,2,2-Tetrachloroethane <4.8 ug/L 11/04/19 18:09 79-34-512.5 4.8 25
Tetrachloroethene <5.8 ug/L 11/04/19 18:09 127-18-412.5 5.8 25
Toluene 2400 ug/L 11/04/19 18:09 108-88-3 M112.5 5.7 25
1,2,3-Trichlorobenzene <19.5 ug/L 11/04/19 18:09 87-61-650.0 19.5 25
1,2,4-Trichlorobenzene <10.9 ug/L 11/04/19 18:09 120-82-150.0 10.9 25
1,1,1-Trichloroethane <7.0 ug/L 11/04/19 18:09 71-55-612.5 7.0 25
1,1,2-Trichloroethane <5.8 ug/L 11/04/19 18:09 79-00-512.5 5.8 25
Trichloroethene <5.8 ug/L 11/04/19 18:09 79-01-612.5 5.8 25
Trichlorofluoromethane <8.4 ug/L 11/04/19 18:09 75-69-425.0 8.4 25
1,2,3-Trichloropropane <6.8 ug/L 11/04/19 18:09 96-18-412.5 6.8 25
1,2,4-Trimethylbenzene 145 ug/L 11/04/19 18:09 95-63-612.5 4.8 25
1,3,5-Trimethylbenzene 48.4 ug/L 11/04/19 18:09 108-67-812.5 5.7 25
Vinyl chloride <10.2 ug/L 11/04/19 18:09 75-01-425.0 10.2 25
Xylene (Total)1290 ug/L 11/04/19 18:09 1330-20-725.0 12.5 25
m&p-Xylene 824 ug/L 11/04/19 18:09 179601-23-125.0 11.0 25
o-Xylene 469 ug/L 11/04/19 18:09 95-47-612.5 5.9 25
Surrogates
1,2-Dichloroethane-d4 (S)97 %11/04/19 18:09 17060-07-070-130 25
4-Bromofluorobenzene (S)96 %11/04/19 18:09 460-00-470-130 25
Toluene-d8 (S)95 %11/04/19 18:09 2037-26-570-130 25
Sample:MW-4 Lab ID:92451624004 Collected:10/29/19 14:58 Received:10/30/19 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Benzene 605 ug/L 11/04/19 16:57 71-43-22.5 1.2 5
Bromobenzene <1.1 ug/L 11/04/19 16:57 108-86-12.5 1.1 5
Bromochloromethane <1.3 ug/L 11/04/19 16:57 74-97-52.5 1.3 5
Bromodichloromethane <0.92 ug/L 11/04/19 16:57 75-27-42.5 0.92 5
Bromoform <2.0 ug/L 11/04/19 16:57 75-25-22.5 2.0 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451624
Former Newton
Sample:MW-4 Lab ID:92451624004 Collected:10/29/19 14:58 Received:10/30/19 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Bromomethane <8.6 ug/L 11/04/19 16:57 74-83-925.0 8.6 5
2-Butanone (MEK)<18.0 ug/L 11/04/19 16:57 78-93-325.0 18.0 5
n-Butylbenzene <1.8 ug/L 11/04/19 16:57 104-51-82.5 1.8 5
sec-Butylbenzene <1.2 ug/L 11/04/19 16:57 135-98-82.5 1.2 5
tert-Butylbenzene <1.2 ug/L 11/04/19 16:57 98-06-62.5 1.2 5
Carbon tetrachloride <1.2 ug/L 11/04/19 16:57 56-23-52.5 1.2 5
Chlorobenzene <1.1 ug/L 11/04/19 16:57 108-90-72.5 1.1 5
Chloroethane <2.9 ug/L 11/04/19 16:57 75-00-35.0 2.9 5
Chloroform <1.8 ug/L 11/04/19 16:57 67-66-32.5 1.8 5
Chloromethane <2.1 ug/L 11/04/19 16:57 74-87-35.0 2.1 5
2-Chlorotoluene <1.0 ug/L 11/04/19 16:57 95-49-82.5 1.0 5
4-Chlorotoluene <1.0 ug/L 11/04/19 16:57 106-43-42.5 1.0 5
1,2-Dibromo-3-chloropropane <1.9 ug/L 11/04/19 16:57 96-12-85.0 1.9 5
Dibromochloromethane <2.0 ug/L 11/04/19 16:57 124-48-12.5 2.0 5
1,2-Dibromoethane (EDB)<1.2 ug/L 11/04/19 16:57 106-93-42.5 1.2 5
Dibromomethane <1.6 ug/L 11/04/19 16:57 74-95-32.5 1.6 5
1,2-Dichlorobenzene <1.2 ug/L 11/04/19 16:57 95-50-12.5 1.2 5
1,3-Dichlorobenzene <1.2 ug/L 11/04/19 16:57 541-73-12.5 1.2 5
1,4-Dichlorobenzene <1.2 ug/L 11/04/19 16:57 106-46-72.5 1.2 5
Dichlorodifluoromethane <1.4 ug/L 11/04/19 16:57 75-71-82.5 1.4 5
1,1-Dichloroethane <1.2 ug/L 11/04/19 16:57 75-34-32.5 1.2 5
1,2-Dichloroethane <1.3 ug/L 11/04/19 16:57 107-06-22.5 1.3 5
1,1-Dichloroethene <1.1 ug/L 11/04/19 16:57 75-35-42.5 1.1 5
cis-1,2-Dichloroethene <1.0 ug/L 11/04/19 16:57 156-59-22.5 1.0 5
trans-1,2-Dichloroethene <1.3 ug/L 11/04/19 16:57 156-60-52.5 1.3 5
1,2-Dichloropropane <0.92 ug/L 11/04/19 16:57 78-87-52.5 0.92 5
1,3-Dichloropropane <1.7 ug/L 11/04/19 16:57 142-28-92.5 1.7 5
2,2-Dichloropropane <1.4 ug/L 11/04/19 16:57 594-20-72.5 1.4 5
1,1-Dichloropropene <1.7 ug/L 11/04/19 16:57 563-58-62.5 1.7 5
cis-1,3-Dichloropropene <1.8 ug/L 11/04/19 16:57 10061-01-52.5 1.8 5
trans-1,3-Dichloropropene <2.0 ug/L 11/04/19 16:57 10061-02-62.5 2.0 5
Diisopropyl ether 87.5 ug/L 11/04/19 16:57 108-20-32.5 1.7 5
Ethylbenzene 190 ug/L 11/04/19 16:57 100-41-42.5 1.2 5
Hexachloro-1,3-butadiene <6.0 ug/L 11/04/19 16:57 87-68-310.0 6.0 5
2-Hexanone <3.0 ug/L 11/04/19 16:57 591-78-625.0 3.0 5
Isopropylbenzene (Cumene)15.4 ug/L 11/04/19 16:57 98-82-82.5 1.2 5
Methylene Chloride <7.5 ug/L 11/04/19 16:57 75-09-210.0 7.5 5
Methyl-tert-butyl ether 14.1 ug/L 11/04/19 16:57 1634-04-42.5 2.2 5
Naphthalene 102 ug/L 11/04/19 16:57 91-20-310.0 3.3 5
n-Propylbenzene 20.0 ug/L 11/04/19 16:57 103-65-12.5 1.2 5
Styrene <1.3 ug/L 11/04/19 16:57 100-42-52.5 1.3 5
1,1,1,2-Tetrachloroethane <2.1 ug/L 11/04/19 16:57 630-20-62.5 2.1 5
1,1,2,2-Tetrachloroethane <0.96 ug/L 11/04/19 16:57 79-34-52.5 0.96 5
Tetrachloroethene 2.6 ug/L 11/04/19 16:57 127-18-42.5 1.2 5
Toluene 185 ug/L 11/04/19 16:57 108-88-32.5 1.1 5
1,2,3-Trichlorobenzene <3.9 ug/L 11/04/19 16:57 87-61-610.0 3.9 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451624
Former Newton
Sample:MW-4 Lab ID:92451624004 Collected:10/29/19 14:58 Received:10/30/19 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
1,2,4-Trichlorobenzene <2.2 ug/L 11/04/19 16:57 120-82-110.0 2.2 5
1,1,1-Trichloroethane <1.4 ug/L 11/04/19 16:57 71-55-62.5 1.4 5
1,1,2-Trichloroethane <1.2 ug/L 11/04/19 16:57 79-00-52.5 1.2 5
Trichloroethene <1.2 ug/L 11/04/19 16:57 79-01-62.5 1.2 5
Trichlorofluoromethane <1.7 ug/L 11/04/19 16:57 75-69-45.0 1.7 5
1,2,3-Trichloropropane <1.4 ug/L 11/04/19 16:57 96-18-42.5 1.4 5
1,2,4-Trimethylbenzene 40.6 ug/L 11/04/19 16:57 95-63-62.5 0.96 5
1,3,5-Trimethylbenzene 15.7 ug/L 11/04/19 16:57 108-67-82.5 1.1 5
Vinyl chloride <2.0 ug/L 11/04/19 16:57 75-01-45.0 2.0 5
Xylene (Total)152 ug/L 11/04/19 16:57 1330-20-75.0 2.5 5
m&p-Xylene 114 ug/L 11/04/19 16:57 179601-23-15.0 2.2 5
o-Xylene 37.5 ug/L 11/04/19 16:57 95-47-62.5 1.2 5
Surrogates
1,2-Dichloroethane-d4 (S)101 %11/04/19 16:57 17060-07-070-130 5
4-Bromofluorobenzene (S)95 %11/04/19 16:57 460-00-470-130 5
Toluene-d8 (S)97 %11/04/19 16:57 2037-26-570-130 5
Sample:MW-6 Lab ID:92451624005 Collected:10/29/19 14:21 Received:10/30/19 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Benzene <0.24 ug/L 11/01/19 15:42 71-43-20.50 0.24 1
Bromobenzene <0.22 ug/L 11/01/19 15:42 108-86-10.50 0.22 1
Bromochloromethane <0.26 ug/L 11/01/19 15:42 74-97-50.50 0.26 1
Bromodichloromethane <0.18 ug/L 11/01/19 15:42 75-27-40.50 0.18 1
Bromoform <0.40 ug/L 11/01/19 15:42 75-25-20.50 0.40 1
Bromomethane <1.7 ug/L 11/01/19 15:42 74-83-95.0 1.7 1
2-Butanone (MEK)<3.6 ug/L 11/01/19 15:42 78-93-35.0 3.6 1
n-Butylbenzene <0.35 ug/L 11/01/19 15:42 104-51-80.50 0.35 1
sec-Butylbenzene 0.57 ug/L 11/01/19 15:42 135-98-80.50 0.25 1
tert-Butylbenzene <0.25 ug/L 11/01/19 15:42 98-06-60.50 0.25 1
Carbon tetrachloride <0.23 ug/L 11/01/19 15:42 56-23-50.50 0.23 1
Chlorobenzene <0.22 ug/L 11/01/19 15:42 108-90-70.50 0.22 1
Chloroethane <0.58 ug/L 11/01/19 15:42 75-00-31.0 0.58 1
Chloroform <0.35 ug/L 11/01/19 15:42 67-66-30.50 0.35 1
Chloromethane <0.42 ug/L 11/01/19 15:42 74-87-31.0 0.42 1
2-Chlorotoluene <0.21 ug/L 11/01/19 15:42 95-49-80.50 0.21 1
4-Chlorotoluene <0.21 ug/L 11/01/19 15:42 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane <0.38 ug/L 11/01/19 15:42 96-12-81.0 0.38 1
Dibromochloromethane <0.40 ug/L 11/01/19 15:42 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)<0.23 ug/L 11/01/19 15:42 106-93-40.50 0.23 1
Dibromomethane <0.31 ug/L 11/01/19 15:42 74-95-30.50 0.31 1
1,2-Dichlorobenzene <0.24 ug/L 11/01/19 15:42 95-50-10.50 0.24 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
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Page 11 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451624
Former Newton
Sample:MW-6 Lab ID:92451624005 Collected:10/29/19 14:21 Received:10/30/19 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
1,3-Dichlorobenzene <0.25 ug/L 11/01/19 15:42 541-73-10.50 0.25 1
1,4-Dichlorobenzene <0.25 ug/L 11/01/19 15:42 106-46-70.50 0.25 1
Dichlorodifluoromethane <0.28 ug/L 11/01/19 15:42 75-71-80.50 0.28 1
1,1-Dichloroethane <0.24 ug/L 11/01/19 15:42 75-34-30.50 0.24 1
1,2-Dichloroethane <0.26 ug/L 11/01/19 15:42 107-06-20.50 0.26 1
1,1-Dichloroethene <0.22 ug/L 11/01/19 15:42 75-35-40.50 0.22 1
cis-1,2-Dichloroethene <0.21 ug/L 11/01/19 15:42 156-59-20.50 0.21 1
trans-1,2-Dichloroethene <0.26 ug/L 11/01/19 15:42 156-60-50.50 0.26 1
1,2-Dichloropropane <0.18 ug/L 11/01/19 15:42 78-87-50.50 0.18 1
1,3-Dichloropropane <0.34 ug/L 11/01/19 15:42 142-28-90.50 0.34 1
2,2-Dichloropropane <0.28 ug/L 11/01/19 15:42 594-20-70.50 0.28 1
1,1-Dichloropropene <0.35 ug/L 11/01/19 15:42 563-58-60.50 0.35 1
cis-1,3-Dichloropropene <0.36 ug/L 11/01/19 15:42 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.39 ug/L 11/01/19 15:42 10061-02-60.50 0.39 1
Diisopropyl ether 9.1 ug/L 11/01/19 15:42 108-20-30.50 0.33 1
Ethylbenzene <0.24 ug/L 11/01/19 15:42 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene <1.2 ug/L 11/01/19 15:42 87-68-32.0 1.2 1
2-Hexanone <0.60 ug/L 11/01/19 15:42 591-78-65.0 0.60 1
Isopropylbenzene (Cumene)<0.24 ug/L 11/01/19 15:42 98-82-80.50 0.24 1
Methylene Chloride <1.5 ug/L 11/01/19 15:42 75-09-22.0 1.5 1
Methyl-tert-butyl ether 2.5 ug/L 11/01/19 15:42 1634-04-40.50 0.44 1
Naphthalene <0.66 ug/L 11/01/19 15:42 91-20-32.0 0.66 1
n-Propylbenzene <0.24 ug/L 11/01/19 15:42 103-65-10.50 0.24 1
Styrene <0.26 ug/L 11/01/19 15:42 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane <0.42 ug/L 11/01/19 15:42 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane <0.19 ug/L 11/01/19 15:42 79-34-50.50 0.19 1
Tetrachloroethene <0.23 ug/L 11/01/19 15:42 127-18-40.50 0.23 1
Toluene <0.23 ug/L 11/01/19 15:42 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene <0.78 ug/L 11/01/19 15:42 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene <0.44 ug/L 11/01/19 15:42 120-82-12.0 0.44 1
1,1,1-Trichloroethane <0.28 ug/L 11/01/19 15:42 71-55-60.50 0.28 1
1,1,2-Trichloroethane <0.23 ug/L 11/01/19 15:42 79-00-50.50 0.23 1
Trichloroethene <0.23 ug/L 11/01/19 15:42 79-01-60.50 0.23 1
Trichlorofluoromethane <0.34 ug/L 11/01/19 15:42 75-69-41.0 0.34 1
1,2,3-Trichloropropane <0.27 ug/L 11/01/19 15:42 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene <0.19 ug/L 11/01/19 15:42 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene <0.23 ug/L 11/01/19 15:42 108-67-80.50 0.23 1
Vinyl chloride <0.41 ug/L 11/01/19 15:42 75-01-41.0 0.41 1
Xylene (Total)<0.50 ug/L 11/01/19 15:42 1330-20-71.0 0.50 1
m&p-Xylene <0.44 ug/L 11/01/19 15:42 179601-23-11.0 0.44 1
o-Xylene <0.24 ug/L 11/01/19 15:42 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %11/01/19 15:42 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %11/01/19 15:42 460-00-470-130 1
Toluene-d8 (S)100 %11/01/19 15:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
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Page 12 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451624
Former Newton
Sample:MW-8 Lab ID:92451624006 Collected:10/29/19 13:39 Received:10/30/19 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Benzene <0.24 ug/L 11/01/19 16:00 71-43-20.50 0.24 1
Bromobenzene <0.22 ug/L 11/01/19 16:00 108-86-10.50 0.22 1
Bromochloromethane <0.26 ug/L 11/01/19 16:00 74-97-50.50 0.26 1
Bromodichloromethane <0.18 ug/L 11/01/19 16:00 75-27-40.50 0.18 1
Bromoform <0.40 ug/L 11/01/19 16:00 75-25-20.50 0.40 1
Bromomethane <1.7 ug/L 11/01/19 16:00 74-83-95.0 1.7 1
2-Butanone (MEK)<3.6 ug/L 11/01/19 16:00 78-93-35.0 3.6 1
n-Butylbenzene <0.35 ug/L 11/01/19 16:00 104-51-80.50 0.35 1
sec-Butylbenzene <0.25 ug/L 11/01/19 16:00 135-98-80.50 0.25 1
tert-Butylbenzene <0.25 ug/L 11/01/19 16:00 98-06-60.50 0.25 1
Carbon tetrachloride <0.23 ug/L 11/01/19 16:00 56-23-50.50 0.23 1
Chlorobenzene <0.22 ug/L 11/01/19 16:00 108-90-70.50 0.22 1
Chloroethane <0.58 ug/L 11/01/19 16:00 75-00-31.0 0.58 1
Chloroform 16.6 ug/L 11/01/19 16:00 67-66-30.50 0.35 1
Chloromethane <0.42 ug/L 11/01/19 16:00 74-87-31.0 0.42 1
2-Chlorotoluene <0.21 ug/L 11/01/19 16:00 95-49-80.50 0.21 1
4-Chlorotoluene <0.21 ug/L 11/01/19 16:00 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane <0.38 ug/L 11/01/19 16:00 96-12-81.0 0.38 1
Dibromochloromethane <0.40 ug/L 11/01/19 16:00 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)<0.23 ug/L 11/01/19 16:00 106-93-40.50 0.23 1
Dibromomethane <0.31 ug/L 11/01/19 16:00 74-95-30.50 0.31 1
1,2-Dichlorobenzene <0.24 ug/L 11/01/19 16:00 95-50-10.50 0.24 1
1,3-Dichlorobenzene <0.25 ug/L 11/01/19 16:00 541-73-10.50 0.25 1
1,4-Dichlorobenzene <0.25 ug/L 11/01/19 16:00 106-46-70.50 0.25 1
Dichlorodifluoromethane <0.28 ug/L 11/01/19 16:00 75-71-80.50 0.28 1
1,1-Dichloroethane <0.24 ug/L 11/01/19 16:00 75-34-30.50 0.24 1
1,2-Dichloroethane <0.26 ug/L 11/01/19 16:00 107-06-20.50 0.26 1
1,1-Dichloroethene <0.22 ug/L 11/01/19 16:00 75-35-40.50 0.22 1
cis-1,2-Dichloroethene 4.6 ug/L 11/01/19 16:00 156-59-20.50 0.21 1
trans-1,2-Dichloroethene <0.26 ug/L 11/01/19 16:00 156-60-50.50 0.26 1
1,2-Dichloropropane <0.18 ug/L 11/01/19 16:00 78-87-50.50 0.18 1
1,3-Dichloropropane <0.34 ug/L 11/01/19 16:00 142-28-90.50 0.34 1
2,2-Dichloropropane <0.28 ug/L 11/01/19 16:00 594-20-70.50 0.28 1
1,1-Dichloropropene <0.35 ug/L 11/01/19 16:00 563-58-60.50 0.35 1
cis-1,3-Dichloropropene <0.36 ug/L 11/01/19 16:00 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.39 ug/L 11/01/19 16:00 10061-02-60.50 0.39 1
Diisopropyl ether <0.33 ug/L 11/01/19 16:00 108-20-30.50 0.33 1
Ethylbenzene <0.24 ug/L 11/01/19 16:00 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene <1.2 ug/L 11/01/19 16:00 87-68-32.0 1.2 1
2-Hexanone <0.60 ug/L 11/01/19 16:00 591-78-65.0 0.60 1
Isopropylbenzene (Cumene)<0.24 ug/L 11/01/19 16:00 98-82-80.50 0.24 1
Methylene Chloride <1.5 ug/L 11/01/19 16:00 75-09-22.0 1.5 1
Methyl-tert-butyl ether <0.44 ug/L 11/01/19 16:00 1634-04-40.50 0.44 1
Naphthalene <0.66 ug/L 11/01/19 16:00 91-20-32.0 0.66 1
n-Propylbenzene <0.24 ug/L 11/01/19 16:00 103-65-10.50 0.24 1
Styrene <0.26 ug/L 11/01/19 16:00 100-42-50.50 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
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Page 13 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451624
Former Newton
Sample:MW-8 Lab ID:92451624006 Collected:10/29/19 13:39 Received:10/30/19 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
1,1,1,2-Tetrachloroethane <0.42 ug/L 11/01/19 16:00 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane <0.19 ug/L 11/01/19 16:00 79-34-50.50 0.19 1
Tetrachloroethene 56.7 ug/L 11/01/19 16:00 127-18-40.50 0.23 1
Toluene <0.23 ug/L 11/01/19 16:00 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene <0.78 ug/L 11/01/19 16:00 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene <0.44 ug/L 11/01/19 16:00 120-82-12.0 0.44 1
1,1,1-Trichloroethane <0.28 ug/L 11/01/19 16:00 71-55-60.50 0.28 1
1,1,2-Trichloroethane <0.23 ug/L 11/01/19 16:00 79-00-50.50 0.23 1
Trichloroethene 2.4 ug/L 11/01/19 16:00 79-01-60.50 0.23 1
Trichlorofluoromethane <0.34 ug/L 11/01/19 16:00 75-69-41.0 0.34 1
1,2,3-Trichloropropane <0.27 ug/L 11/01/19 16:00 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene <0.19 ug/L 11/01/19 16:00 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene <0.23 ug/L 11/01/19 16:00 108-67-80.50 0.23 1
Vinyl chloride <0.41 ug/L 11/01/19 16:00 75-01-41.0 0.41 1
Xylene (Total)<0.50 ug/L 11/01/19 16:00 1330-20-71.0 0.50 1
m&p-Xylene <0.44 ug/L 11/01/19 16:00 179601-23-11.0 0.44 1
o-Xylene <0.24 ug/L 11/01/19 16:00 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %11/01/19 16:00 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %11/01/19 16:00 460-00-470-130 1
Toluene-d8 (S)101 %11/01/19 16:00 2037-26-570-130 1
Sample:MW-11 Lab ID:92451624007 Collected:10/29/19 12:58 Received:10/30/19 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Benzene 2770 ug/L 11/01/19 19:53 71-43-2250120500
Bromobenzene <108 ug/L 11/01/19 19:53 108-86-1250108500
Bromochloromethane <129 ug/L 11/01/19 19:53 74-97-5250129500
Bromodichloromethane <92.5 ug/L 11/01/19 19:53 75-27-425092.5 500
Bromoform <202 ug/L 11/01/19 19:53 75-25-2250202500
Bromomethane <860 ug/L 11/01/19 19:53 74-83-92500860500
2-Butanone (MEK)<1800 ug/L 11/01/19 19:53 78-93-325001800500
n-Butylbenzene <176 ug/L 11/01/19 19:53 104-51-8250176500
sec-Butylbenzene <123 ug/L 11/01/19 19:53 135-98-8250123500
tert-Butylbenzene <125 ug/L 11/01/19 19:53 98-06-6250125500
Carbon tetrachloride <116 ug/L 11/01/19 19:53 56-23-5250116500
Chlorobenzene <112 ug/L 11/01/19 19:53 108-90-7250112500
Chloroethane <292 ug/L 11/01/19 19:53 75-00-3500292500
Chloroform <176 ug/L 11/01/19 19:53 67-66-3250176500
Chloromethane <208 ug/L 11/01/19 19:53 74-87-3500208500
2-Chlorotoluene <104 ug/L 11/01/19 19:53 95-49-8250104500
4-Chlorotoluene <103 ug/L 11/01/19 19:53 106-43-4250103500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
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Page 14 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451624
Former Newton
Sample:MW-11 Lab ID:92451624007 Collected:10/29/19 12:58 Received:10/30/19 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
1,2-Dibromo-3-chloropropane <192 ug/L 11/01/19 19:53 96-12-8500192500
Dibromochloromethane <201 ug/L 11/01/19 19:53 124-48-1250201500
1,2-Dibromoethane (EDB)<116 ug/L 11/01/19 19:53 106-93-4250116500
Dibromomethane <155 ug/L 11/01/19 19:53 74-95-3250155500
1,2-Dichlorobenzene <120 ug/L 11/01/19 19:53 95-50-1250120500
1,3-Dichlorobenzene <125 ug/L 11/01/19 19:53 541-73-1250125500
1,4-Dichlorobenzene <124 ug/L 11/01/19 19:53 106-46-7250124500
Dichlorodifluoromethane <142 ug/L 11/01/19 19:53 75-71-8250142500
1,1-Dichloroethane <122 ug/L 11/01/19 19:53 75-34-3250122500
1,2-Dichloroethane <132 ug/L 11/01/19 19:53 107-06-2250132500
1,1-Dichloroethene <109 ug/L 11/01/19 19:53 75-35-4250109500
cis-1,2-Dichloroethene <104 ug/L 11/01/19 19:53 156-59-2250104500
trans-1,2-Dichloroethene <128 ug/L 11/01/19 19:53 156-60-5250128500
1,2-Dichloropropane <91.5 ug/L 11/01/19 19:53 78-87-525091.5 500
1,3-Dichloropropane <170 ug/L 11/01/19 19:53 142-28-9250170500
2,2-Dichloropropane <140 ug/L 11/01/19 19:53 594-20-7250140500
1,1-Dichloropropene <174 ug/L 11/01/19 19:53 563-58-6250174500
cis-1,3-Dichloropropene <178 ug/L 11/01/19 19:53 10061-01-5250178500
trans-1,3-Dichloropropene <197 ug/L 11/01/19 19:53 10061-02-6250197500
Diisopropyl ether <167 ug/L 11/01/19 19:53 108-20-3250167500
Ethylbenzene 3820 ug/L 11/01/19 19:53 100-41-4250120500
Hexachloro-1,3-butadiene <600 ug/L 11/01/19 19:53 87-68-31000600500
2-Hexanone <302 ug/L 11/01/19 19:53 591-78-62500302500
Isopropylbenzene (Cumene)<119 ug/L 11/01/19 19:53 98-82-8250119500
Methylene Chloride <750 ug/L 11/01/19 19:53 75-09-21000750500
Methyl-tert-butyl ether <222 ug/L 11/01/19 19:53 1634-04-4250222500
Naphthalene 734J ug/L 11/01/19 19:53 91-20-31000330500
n-Propylbenzene <120 ug/L 11/01/19 19:53 103-65-1250120500
Styrene 316 ug/L 11/01/19 19:53 100-42-5250128500
1,1,1,2-Tetrachloroethane <211 ug/L 11/01/19 19:53 630-20-6250211500
1,1,2,2-Tetrachloroethane <96.5 ug/L 11/01/19 19:53 79-34-525096.5 500
Tetrachloroethene <116 ug/L 11/01/19 19:53 127-18-4250116500
Toluene 46800 ug/L 11/01/19 19:53 108-88-3250114500
1,2,3-Trichlorobenzene <390 ug/L 11/01/19 19:53 87-61-61000390500
1,2,4-Trichlorobenzene <218 ug/L 11/01/19 19:53 120-82-11000218500
1,1,1-Trichloroethane <139 ug/L 11/01/19 19:53 71-55-6250139500
1,1,2-Trichloroethane <116 ug/L 11/01/19 19:53 79-00-5250116500
Trichloroethene <116 ug/L 11/01/19 19:53 79-01-6250116500
Trichlorofluoromethane <168 ug/L 11/01/19 19:53 75-69-4500168500
1,2,3-Trichloropropane <136 ug/L 11/01/19 19:53 96-18-4250136500
1,2,4-Trimethylbenzene 2550 ug/L 11/01/19 19:53 95-63-625096.5 500
1,3,5-Trimethylbenzene <114 ug/L 11/01/19 19:53 108-67-8250114500
Vinyl chloride <204 ug/L 11/01/19 19:53 75-01-4500204500
Xylene (Total)20500 ug/L 11/01/19 19:53 1330-20-7500250500
m&p-Xylene 14200 ug/L 11/01/19 19:53 179601-23-1500220500
o-Xylene 6360 ug/L 11/01/19 19:53 95-47-6250118500
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
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Page 15 of 31
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92451624
Former Newton
Sample:MW-11 Lab ID:92451624007 Collected:10/29/19 12:58 Received:10/30/19 10:11 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Surrogates
1,2-Dichloroethane-d4 (S)95 %11/01/19 19:53 17060-07-070-130 500
4-Bromofluorobenzene (S)99 %11/01/19 19:53 460-00-470-130 500
Toluene-d8 (S)100 %11/01/19 19:53 2037-26-570-130 500
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 16 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451624
Former Newton
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
507132
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92451624001, 92451624002, 92451624005, 92451624006, 92451624007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2722835
Associated Lab Samples:92451624001, 92451624002, 92451624005, 92451624006, 92451624007
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.42 0.50 11/01/19 11:320.42
1,1,1-Trichloroethane ug/L <0.28 0.50 11/01/19 11:320.28
1,1,2,2-Tetrachloroethane ug/L <0.19 0.50 11/01/19 11:320.19
1,1,2-Trichloroethane ug/L <0.23 0.50 11/01/19 11:320.23
1,1-Dichloroethane ug/L <0.24 0.50 11/01/19 11:320.24
1,1-Dichloroethene ug/L <0.22 0.50 11/01/19 11:320.22
1,1-Dichloropropene ug/L <0.35 0.50 11/01/19 11:320.35
1,2,3-Trichlorobenzene ug/L <0.78 2.0 11/01/19 11:320.78
1,2,3-Trichloropropane ug/L <0.27 0.50 11/01/19 11:320.27
1,2,4-Trichlorobenzene ug/L <0.44 2.0 11/01/19 11:320.44
1,2,4-Trimethylbenzene ug/L <0.19 0.50 11/01/19 11:320.19
1,2-Dibromo-3-chloropropane ug/L <0.38 1.0 11/01/19 11:320.38
1,2-Dibromoethane (EDB)ug/L <0.23 0.50 11/01/19 11:320.23
1,2-Dichlorobenzene ug/L <0.24 0.50 11/01/19 11:320.24
1,2-Dichloroethane ug/L <0.26 0.50 11/01/19 11:320.26
1,2-Dichloropropane ug/L <0.18 0.50 11/01/19 11:320.18
1,3,5-Trimethylbenzene ug/L <0.23 0.50 11/01/19 11:320.23
1,3-Dichlorobenzene ug/L <0.25 0.50 11/01/19 11:320.25
1,3-Dichloropropane ug/L <0.34 0.50 11/01/19 11:320.34
1,4-Dichlorobenzene ug/L <0.25 0.50 11/01/19 11:320.25
2,2-Dichloropropane ug/L <0.28 0.50 11/01/19 11:320.28
2-Butanone (MEK)ug/L <3.6 5.0 11/01/19 11:323.6
2-Chlorotoluene ug/L <0.21 0.50 11/01/19 11:320.21
2-Hexanone ug/L <0.60 5.0 11/01/19 11:320.60
4-Chlorotoluene ug/L <0.21 0.50 11/01/19 11:320.21
Benzene ug/L <0.24 0.50 11/01/19 11:320.24
Bromobenzene ug/L <0.22 0.50 11/01/19 11:320.22
Bromochloromethane ug/L <0.26 0.50 11/01/19 11:320.26
Bromodichloromethane ug/L <0.18 0.50 11/01/19 11:320.18
Bromoform ug/L <0.40 0.50 11/01/19 11:320.40
Bromomethane ug/L <1.7 5.0 11/01/19 11:321.7
Carbon tetrachloride ug/L <0.23 0.50 11/01/19 11:320.23
Chlorobenzene ug/L <0.22 0.50 11/01/19 11:320.22
Chloroethane ug/L <0.58 1.0 11/01/19 11:320.58
Chloroform ug/L <0.35 0.50 11/01/19 11:320.35
Chloromethane ug/L <0.42 1.0 11/01/19 11:320.42
cis-1,2-Dichloroethene ug/L <0.21 0.50 11/01/19 11:320.21
cis-1,3-Dichloropropene ug/L <0.36 0.50 11/01/19 11:320.36
Dibromochloromethane ug/L <0.40 0.50 11/01/19 11:320.40
Dibromomethane ug/L <0.31 0.50 11/01/19 11:320.31
Dichlorodifluoromethane ug/L <0.28 0.50 11/01/19 11:320.28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451624
Former Newton
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2722835
Associated Lab Samples:92451624001, 92451624002, 92451624005, 92451624006, 92451624007
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L <0.33 0.50 11/01/19 11:320.33
Ethylbenzene ug/L <0.24 0.50 11/01/19 11:320.24
Hexachloro-1,3-butadiene ug/L <1.2 2.0 11/01/19 11:321.2
Isopropylbenzene (Cumene)ug/L <0.24 0.50 11/01/19 11:320.24
m&p-Xylene ug/L <0.44 1.0 11/01/19 11:320.44
Methyl-tert-butyl ether ug/L <0.44 0.50 11/01/19 11:320.44
Methylene Chloride ug/L <1.5 2.0 11/01/19 11:321.5
n-Butylbenzene ug/L <0.35 0.50 11/01/19 11:320.35
n-Propylbenzene ug/L <0.24 0.50 11/01/19 11:320.24
Naphthalene ug/L <0.66 2.0 11/01/19 11:320.66
o-Xylene ug/L <0.24 0.50 11/01/19 11:320.24
sec-Butylbenzene ug/L <0.25 0.50 11/01/19 11:320.25
Styrene ug/L <0.26 0.50 11/01/19 11:320.26
tert-Butylbenzene ug/L <0.25 0.50 11/01/19 11:320.25
Tetrachloroethene ug/L <0.23 0.50 11/01/19 11:320.23
Toluene ug/L <0.23 0.50 11/01/19 11:320.23
trans-1,2-Dichloroethene ug/L <0.26 0.50 11/01/19 11:320.26
trans-1,3-Dichloropropene ug/L <0.39 0.50 11/01/19 11:320.39
Trichloroethene ug/L <0.23 0.50 11/01/19 11:320.23
Trichlorofluoromethane ug/L <0.34 1.0 11/01/19 11:320.34
Vinyl chloride ug/L <0.41 1.0 11/01/19 11:320.41
Xylene (Total)ug/L <0.50 1.0 11/01/19 11:320.50
1,2-Dichloroethane-d4 (S)%98 70-130 11/01/19 11:32
4-Bromofluorobenzene (S)%99 70-130 11/01/19 11:32
Toluene-d8 (S)%102 70-130 11/01/19 11:32
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2722836LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 53.250 106 60-140
1,1,1-Trichloroethane ug/L 53.750 107 60-140
1,1,2,2-Tetrachloroethane ug/L 51.450 103 60-140
1,1,2-Trichloroethane ug/L 52.950 106 60-140
1,1-Dichloroethane ug/L 52.650 105 60-140
1,1-Dichloroethene ug/L 54.450 109 60-140
1,1-Dichloropropene ug/L 53.350 107 60-140
1,2,3-Trichlorobenzene ug/L 57.250 114 60-140
1,2,3-Trichloropropane ug/L 50.850 102 60-140
1,2,4-Trichlorobenzene ug/L 54.850 110 60-140
1,2,4-Trimethylbenzene ug/L 50.850 102 60-140
1,2-Dibromo-3-chloropropane ug/L 55.250 110 60-140
1,2-Dibromoethane (EDB)ug/L 53.550 107 60-140
1,2-Dichlorobenzene ug/L 50.950 102 60-140
1,2-Dichloroethane ug/L 47.050 94 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451624
Former Newton
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2722836LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloropropane ug/L 54.750 109 60-140
1,3,5-Trimethylbenzene ug/L 52.450 105 60-140
1,3-Dichlorobenzene ug/L 50.150 100 60-140
1,3-Dichloropropane ug/L 54.550 109 60-140
1,4-Dichlorobenzene ug/L 50.150 100 60-140
2,2-Dichloropropane ug/L 55.450 111 60-140
2-Butanone (MEK)ug/L 110100 110 60-140
2-Chlorotoluene ug/L 50.850 102 60-140
2-Hexanone ug/L 111100 111 60-140
4-Chlorotoluene ug/L 50.850 102 60-140
Benzene ug/L 53.450 107 60-140
Bromobenzene ug/L 52.250 104 60-140
Bromochloromethane ug/L 50.750 101 60-140
Bromodichloromethane ug/L 55.850 112 60-140
Bromoform ug/L 53.950 108 60-140
Bromomethane ug/L 44.350 89 60-140
Carbon tetrachloride ug/L 51.650 103 60-140
Chlorobenzene ug/L 49.950 100 60-140
Chloroethane ug/L 47.150 94 60-140
Chloroform ug/L 51.450 103 60-140
Chloromethane ug/L 54.850 110 60-140
cis-1,2-Dichloroethene ug/L 52.750 105 60-140
cis-1,3-Dichloropropene ug/L 58.050 116 60-140
Dibromochloromethane ug/L 53.550 107 60-140
Dibromomethane ug/L 50.150 100 60-140
Dichlorodifluoromethane ug/L 61.650 123 60-140
Diisopropyl ether ug/L 55.550 111 60-140
Ethylbenzene ug/L 51.150 102 60-140
Hexachloro-1,3-butadiene ug/L 57.050 114 60-140
Isopropylbenzene (Cumene)ug/L 53.650 107 60-140
m&p-Xylene ug/L 104100 104 60-140
Methyl-tert-butyl ether ug/L 55.250 110 60-140
Methylene Chloride ug/L 51.250 102 60-140
n-Butylbenzene ug/L 55.250 110 60-140
n-Propylbenzene ug/L 52.650 105 60-140
Naphthalene ug/L 56.850 114 60-140
o-Xylene ug/L 53.250 106 60-140
sec-Butylbenzene ug/L 53.750 107 60-140
Styrene ug/L 53.250 106 60-140
tert-Butylbenzene ug/L 44.450 89 60-140
Tetrachloroethene ug/L 54.550 109 60-140
Toluene ug/L 51.850 104 60-140
trans-1,2-Dichloroethene ug/L 52.950 106 60-140
trans-1,3-Dichloropropene ug/L 56.050 112 60-140
Trichloroethene ug/L 53.550 107 60-140
Trichlorofluoromethane ug/L 54.350 109 60-140
Vinyl chloride ug/L 53.850 108 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451624
Former Newton
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2722836LABORATORY CONTROL SAMPLE:
LCSSpike
Xylene (Total)ug/L 157150 105 60-140
1,2-Dichloroethane-d4 (S)%100 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%99 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2722837MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92451287001
2722838
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 5000 109 60-140112 3 305000ND54605620
1,1,1-Trichloroethane ug/L 5000 111 60-140114 3 305000ND55505720
1,1,2,2-Tetrachloroethane ug/L 5000 105 60-140102 3 305000ND52605080
1,1,2-Trichloroethane ug/L 5000 114 60-140113 1 305000ND57105630
1,1-Dichloroethane ug/L 5000 110 60-140112 1 305000ND55005580
1,1-Dichloroethene ug/L 5000 115 60-140115 0 305000ND57405750
1,1-Dichloropropene ug/L 5000 113 60-140114 1 305000ND56505720
1,2,3-Trichlorobenzene ug/L 5000 99 60-140101 2 305000ND49605040
1,2,3-Trichloropropane ug/L 5000 108 60-140102 6 305000ND54005110
1,2,4-Trichlorobenzene ug/L 5000 102 60-140103 1 305000ND51105160
1,2,4-Trimethylbenzene ug/L 5000 102 60-140104 1 305000275078607980
1,2-Dibromo-3-
chloropropane ug/L 5000 107 60-140102 5 305000ND53705090
1,2-Dibromoethane (EDB)ug/L 5000 110 60-140112 1 305000ND55105580
1,2-Dichlorobenzene ug/L 5000 104 60-140104 1 305000ND51805210
1,2-Dichloroethane ug/L 5000 99 60-14097 1 305000ND49304860
1,2-Dichloropropane ug/L 5000 115 60-140116 1 305000ND57405790
1,3,5-Trimethylbenzene ug/L 5000 120 60-140123 2 305000ND60206140
1,3-Dichlorobenzene ug/L 5000 103 60-140102 0 305000ND51505120
1,3-Dichloropropane ug/L 5000 112 60-140114 2 305000ND55805710
1,4-Dichlorobenzene ug/L 5000 103 60-140104 1 305000ND51605210
2,2-Dichloropropane ug/L 5000 105 60-140106 1 305000ND52505310
2-Butanone (MEK)ug/L 10000 106 60-140100 6 3010000ND106009980
2-Chlorotoluene ug/L 5000 106 60-140108 2 305000ND53105390
2-Hexanone ug/L 10000 103 60-140100 3 3010000ND1030010000
4-Chlorotoluene ug/L 5000 105 60-140105 0 305000ND52605250
Benzene ug/L 5000 119 60-140127 2 305000174002330023800
Bromobenzene ug/L 5000 110 60-140111 1 305000ND54905550
Bromochloromethane ug/L 5000 106 60-140104 1 305000ND52905220
Bromodichloromethane ug/L 5000 115 60-140117 1 305000ND57705830
Bromoform ug/L 5000 108 60-140107 0 305000ND53805370
Bromomethane ug/L M150005560-14074 28 305000ND27703680
Carbon tetrachloride ug/L 5000 113 60-140115 1 305000ND56705740
Chlorobenzene ug/L 5000 107 60-140108 0 305000ND53705390
Chloroethane ug/L 5000 106 60-140107 1 305000ND52905350
Chloroform ug/L 5000 109 60-140112 2 305000ND55105640
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451624
Former Newton
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2722837MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92451287001
2722838
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloromethane ug/L 5000 95 60-14097 2 305000ND47304830
cis-1,2-Dichloroethene ug/L 5000 111 60-140110 1 305000ND55405480
cis-1,3-Dichloropropene ug/L 5000 119 60-140120 1 305000ND59406010
Dibromochloromethane ug/L 5000 109 60-140111 1 305000ND54705530
Dibromomethane ug/L 5000 107 60-140102 5 305000ND53605100
Dichlorodifluoromethane ug/L 5000 105 60-140106 1 305000ND52405280
Diisopropyl ether ug/L 5000 111 60-140112 1 30500017857105770
Ethylbenzene ug/L 5000 106 60-140111 3 305000306083608630
Hexachloro-1,3-butadiene ug/L 5000 100 60-140109 9 305000ND50005450
Isopropylbenzene
(Cumene)
ug/L 5000 112 60-140115 2 305000ND57205840
m&p-Xylene ug/L 10000 106 60-140113 3 3010000109002150022200
Methyl-tert-butyl ether ug/L 5000 111 60-140113 1 30500077363406400
Methylene Chloride ug/L 5000 107 60-140107 0 305000ND53405340
n-Butylbenzene ug/L 5000 107 60-140110 3 305000ND53405510
n-Propylbenzene ug/L 5000 113 60-140116 2 305000ND56705810
Naphthalene ug/L 5000 97 60-14097 0 305000118060406020
o-Xylene ug/L 5000 108 60-140117 4 30500052701070011100
sec-Butylbenzene ug/L 5000 109 60-140113 4 305000ND54505650
Styrene ug/L 5000 111 60-140112 1 305000ND56205680
tert-Butylbenzene ug/L 5000 91 60-14093 3 305000ND45504670
Tetrachloroethene ug/L 5000 113 60-140114 1 305000ND56305700
Toluene ug/L 5000 87 60-140125 5 305000341003850040400
trans-1,2-Dichloroethene ug/L 5000 112 60-140111 0 305000ND55905560
trans-1,3-Dichloropropene ug/L 5000 106 60-140113 6 305000ND53105640
Trichloroethene ug/L 5000 113 60-140116 2 305000ND56605780
Trichlorofluoromethane ug/L 5000 114 60-140114 0 305000ND57105700
Vinyl chloride ug/L 5000 107 60-140108 1 305000ND53705400
Xylene (Total)ug/L 15000 107 60-140114 3 3015000161003210033300
1,2-Dichloroethane-d4 (S)%96 70-13097
4-Bromofluorobenzene (S)%100 70-130101
Toluene-d8 (S)%99 70-13099
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451624
Former Newton
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
507397
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92451624003, 92451624004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2724186
Associated Lab Samples:92451624003, 92451624004
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.42 0.50 11/04/19 11:350.42
1,1,1-Trichloroethane ug/L <0.28 0.50 11/04/19 11:350.28
1,1,2,2-Tetrachloroethane ug/L <0.19 0.50 11/04/19 11:350.19
1,1,2-Trichloroethane ug/L <0.23 0.50 11/04/19 11:350.23
1,1-Dichloroethane ug/L <0.24 0.50 11/04/19 11:350.24
1,1-Dichloroethene ug/L <0.22 0.50 11/04/19 11:350.22
1,1-Dichloropropene ug/L <0.35 0.50 11/04/19 11:350.35
1,2,3-Trichlorobenzene ug/L <0.78 2.0 11/04/19 11:350.78
1,2,3-Trichloropropane ug/L <0.27 0.50 11/04/19 11:350.27
1,2,4-Trichlorobenzene ug/L <0.44 2.0 11/04/19 11:350.44
1,2,4-Trimethylbenzene ug/L <0.19 0.50 11/04/19 11:350.19
1,2-Dibromo-3-chloropropane ug/L <0.38 1.0 11/04/19 11:350.38
1,2-Dibromoethane (EDB)ug/L <0.23 0.50 11/04/19 11:350.23
1,2-Dichlorobenzene ug/L <0.24 0.50 11/04/19 11:350.24
1,2-Dichloroethane ug/L <0.26 0.50 11/04/19 11:350.26
1,2-Dichloropropane ug/L <0.18 0.50 11/04/19 11:350.18
1,3,5-Trimethylbenzene ug/L <0.23 0.50 11/04/19 11:350.23
1,3-Dichlorobenzene ug/L <0.25 0.50 11/04/19 11:350.25
1,3-Dichloropropane ug/L <0.34 0.50 11/04/19 11:350.34
1,4-Dichlorobenzene ug/L <0.25 0.50 11/04/19 11:350.25
2,2-Dichloropropane ug/L <0.28 0.50 11/04/19 11:350.28
2-Butanone (MEK)ug/L <3.6 5.0 11/04/19 11:353.6
2-Chlorotoluene ug/L <0.21 0.50 11/04/19 11:350.21
2-Hexanone ug/L <0.60 5.0 11/04/19 11:350.60
4-Chlorotoluene ug/L <0.21 0.50 11/04/19 11:350.21
Benzene ug/L <0.24 0.50 11/04/19 11:350.24
Bromobenzene ug/L <0.22 0.50 11/04/19 11:350.22
Bromochloromethane ug/L <0.26 0.50 11/04/19 11:350.26
Bromodichloromethane ug/L <0.18 0.50 11/04/19 11:350.18
Bromoform ug/L <0.40 0.50 11/04/19 11:350.40
Bromomethane ug/L <1.7 5.0 11/04/19 11:351.7
Carbon tetrachloride ug/L <0.23 0.50 11/04/19 11:350.23
Chlorobenzene ug/L <0.22 0.50 11/04/19 11:350.22
Chloroethane ug/L <0.58 1.0 11/04/19 11:350.58
Chloroform ug/L <0.35 0.50 11/04/19 11:350.35
Chloromethane ug/L <0.42 1.0 11/04/19 11:350.42
cis-1,2-Dichloroethene ug/L <0.21 0.50 11/04/19 11:350.21
cis-1,3-Dichloropropene ug/L <0.36 0.50 11/04/19 11:350.36
Dibromochloromethane ug/L <0.40 0.50 11/04/19 11:350.40
Dibromomethane ug/L <0.31 0.50 11/04/19 11:350.31
Dichlorodifluoromethane ug/L <0.28 0.50 11/04/19 11:350.28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451624
Former Newton
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2724186
Associated Lab Samples:92451624003, 92451624004
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L <0.33 0.50 11/04/19 11:350.33
Ethylbenzene ug/L <0.24 0.50 11/04/19 11:350.24
Hexachloro-1,3-butadiene ug/L <1.2 2.0 11/04/19 11:351.2
Isopropylbenzene (Cumene)ug/L <0.24 0.50 11/04/19 11:350.24
m&p-Xylene ug/L <0.44 1.0 11/04/19 11:350.44
Methyl-tert-butyl ether ug/L <0.44 0.50 11/04/19 11:350.44
Methylene Chloride ug/L <1.5 2.0 11/04/19 11:351.5
n-Butylbenzene ug/L <0.35 0.50 11/04/19 11:350.35
n-Propylbenzene ug/L <0.24 0.50 11/04/19 11:350.24
Naphthalene ug/L <0.66 2.0 11/04/19 11:350.66
o-Xylene ug/L <0.24 0.50 11/04/19 11:350.24
sec-Butylbenzene ug/L <0.25 0.50 11/04/19 11:350.25
Styrene ug/L <0.26 0.50 11/04/19 11:350.26
tert-Butylbenzene ug/L <0.25 0.50 11/04/19 11:350.25
Tetrachloroethene ug/L <0.23 0.50 11/04/19 11:350.23
Toluene ug/L <0.23 0.50 11/04/19 11:350.23
trans-1,2-Dichloroethene ug/L <0.26 0.50 11/04/19 11:350.26
trans-1,3-Dichloropropene ug/L <0.39 0.50 11/04/19 11:350.39
Trichloroethene ug/L <0.23 0.50 11/04/19 11:350.23
Trichlorofluoromethane ug/L <0.34 1.0 11/04/19 11:350.34
Vinyl chloride ug/L <0.41 1.0 11/04/19 11:350.41
Xylene (Total)ug/L <0.50 1.0 11/04/19 11:350.50
1,2-Dichloroethane-d4 (S)%102 70-130 11/04/19 11:35
4-Bromofluorobenzene (S)%92 70-130 11/04/19 11:35
Toluene-d8 (S)%98 70-130 11/04/19 11:35
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2724187LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.250 102 60-140
1,1,1-Trichloroethane ug/L 52.450 105 60-140
1,1,2,2-Tetrachloroethane ug/L 51.150 102 60-140
1,1,2-Trichloroethane ug/L 48.850 98 60-140
1,1-Dichloroethane ug/L 49.950 100 60-140
1,1-Dichloroethene ug/L 57.650 115 60-140
1,1-Dichloropropene ug/L 52.050 104 60-140
1,2,3-Trichlorobenzene ug/L 53.950 108 60-140
1,2,3-Trichloropropane ug/L 50.550 101 60-140
1,2,4-Trichlorobenzene ug/L 52.750 105 60-140
1,2,4-Trimethylbenzene ug/L 47.550 95 60-140
1,2-Dibromo-3-chloropropane ug/L 51.550 103 60-140
1,2-Dibromoethane (EDB)ug/L 54.750 109 60-140
1,2-Dichlorobenzene ug/L 48.350 97 60-140
1,2-Dichloroethane ug/L 46.950 94 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
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Huntersville, NC 28078
[phone]
Page 23 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451624
Former Newton
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2724187LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloropropane ug/L 51.550 103 60-140
1,3,5-Trimethylbenzene ug/L 49.050 98 60-140
1,3-Dichlorobenzene ug/L 47.250 94 60-140
1,3-Dichloropropane ug/L 55.550 111 60-140
1,4-Dichlorobenzene ug/L 48.150 96 60-140
2,2-Dichloropropane ug/L 52.850 106 60-140
2-Butanone (MEK)ug/L 109100 109 60-140
2-Chlorotoluene ug/L 49.550 99 60-140
2-Hexanone ug/L 106100 106 60-140
4-Chlorotoluene ug/L 47.850 96 60-140
Benzene ug/L 48.250 96 60-140
Bromobenzene ug/L 51.450 103 60-140
Bromochloromethane ug/L 49.250 98 60-140
Bromodichloromethane ug/L 50.150 100 60-140
Bromoform ug/L 53.650 107 60-140
Bromomethane ug/L 39.850 80 60-140
Carbon tetrachloride ug/L 47.050 94 60-140
Chlorobenzene ug/L 48.650 97 60-140
Chloroethane ug/L 48.750 97 60-140
Chloroform ug/L 52.450 105 60-140
Chloromethane ug/L 43.150 86 60-140
cis-1,2-Dichloroethene ug/L 52.150 104 60-140
cis-1,3-Dichloropropene ug/L 52.450 105 60-140
Dibromochloromethane ug/L 52.750 105 60-140
Dibromomethane ug/L 49.450 99 60-140
Dichlorodifluoromethane ug/L 48.550 97 60-140
Diisopropyl ether ug/L 53.150 106 60-140
Ethylbenzene ug/L 49.350 99 60-140
Hexachloro-1,3-butadiene ug/L 54.150 108 60-140
Isopropylbenzene (Cumene)ug/L 51.150 102 60-140
m&p-Xylene ug/L 98.8100 99 60-140
Methyl-tert-butyl ether ug/L 54.050 108 60-140
Methylene Chloride ug/L 53.250 106 60-140
n-Butylbenzene ug/L 52.850 106 60-140
n-Propylbenzene ug/L 49.350 99 60-140
Naphthalene ug/L 53.750 107 60-140
o-Xylene ug/L 51.250 102 60-140
sec-Butylbenzene ug/L 49.450 99 60-140
Styrene ug/L 52.050 104 60-140
tert-Butylbenzene ug/L 41.550 83 60-140
Tetrachloroethene ug/L 52.750 105 60-140
Toluene ug/L 45.850 92 60-140
trans-1,2-Dichloroethene ug/L 51.350 103 60-140
trans-1,3-Dichloropropene ug/L 48.950 98 60-140
Trichloroethene ug/L 51.950 104 60-140
Trichlorofluoromethane ug/L 54.050 108 60-140
Vinyl chloride ug/L 48.250 96 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451624
Former Newton
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2724187LABORATORY CONTROL SAMPLE:
LCSSpike
Xylene (Total)ug/L 150150 100 60-140
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%93 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2724188MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92451624003
2724189
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 500 114 60-140110 3 30500<10.6 570 552
1,1,1-Trichloroethane ug/L 500 109 60-140113 3 30500<7.0 546 563
1,1,2,2-Tetrachloroethane ug/L 500 108 60-140112 4 30500<4.8 539 559
1,1,2-Trichloroethane ug/L 500 121 60-140114 6 30500<5.8 605 569
1,1-Dichloroethane ug/L 500 122 60-140123 1 30500<6.1 610 615
1,1-Dichloroethene ug/L 500 120 60-140122 2 30500<5.4 598 609
1,1-Dichloropropene ug/L 500 109 60-140113 3 30500<8.7 546 564
1,2,3-Trichlorobenzene ug/L 500 100 60-140105 5 30500<19.5 499 525
1,2,3-Trichloropropane ug/L 500 106 60-140112 5 30500<6.8 529 558
1,2,4-Trichlorobenzene ug/L 500 101 60-140105 4 30500<10.9 504 524
1,2,4-Trimethylbenzene ug/L 500 108 60-140116 5 30500145687724
1,2-Dibromo-3-
chloropropane ug/L 500 107 60-140114 7 30500<9.6 533 569
1,2-Dibromoethane (EDB)ug/L 500 111 60-140114 3 30500<5.8 556 572
1,2-Dichlorobenzene ug/L 500 106 60-140105 1 30500<6.0 528 525
1,2-Dichloroethane ug/L 500 97 60-14099 2 30500<6.6 483 495
1,2-Dichloropropane ug/L 500 113 60-140110 3 30500<4.6 566 551
1,3,5-Trimethylbenzene ug/L 500 109 60-140112 3 3050048.4 592 610
1,3-Dichlorobenzene ug/L 500 105 60-140105 0 30500<6.2 526 526
1,3-Dichloropropane ug/L 500 115 60-140114 1 30500<8.5 577 571
1,4-Dichlorobenzene ug/L 500 102 60-140105 3 30500<6.2 511 526
2,2-Dichloropropane ug/L 500 98 60-140105 7 30500<7.0 489 525
2-Butanone (MEK)ug/L 1000 100 60-14099 1 301000<89.8 997 987
2-Chlorotoluene ug/L 500 104 60-140109 5 30500<5.2 520 547
2-Hexanone ug/L 1000 104 60-140107 2 301000<15.1 1040 1070
4-Chlorotoluene ug/L 500 105 60-140107 2 30500<5.2 525 534
Benzene ug/L 500 113 60-140112 1 3050053.9 621 616
Bromobenzene ug/L 500 111 60-140112 1 30500<5.4 555 559
Bromochloromethane ug/L 500 104 60-140108 3 30500<6.4 522 540
Bromodichloromethane ug/L 500 115 60-140118 3 30500<4.6 574 589
Bromoform ug/L 500 113 60-140115 2 30500<10.1 563 576
Bromomethane ug/L M15005460-14065 18 30500<43.0 271 326
Carbon tetrachloride ug/L 500 111 60-140110 1 30500<5.8 555 549
Chlorobenzene ug/L 500 108 60-140107 2 30500<5.6 541 533
Chloroethane ug/L 500 108 60-140108 0 30500<14.6 540 538
Chloroform ug/L 500 111 60-140111 0 3050019.8 573 575
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 31
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92451624
Former Newton
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2724188MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92451624003
2724189
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloromethane ug/L 500 75 60-14074 1 30500<10.4 377 372
cis-1,2-Dichloroethene ug/L 500 111 60-140117 5 30500<5.2 554 584
cis-1,3-Dichloropropene ug/L 500 113 60-140120 6 30500<8.9 565 599
Dibromochloromethane ug/L 500 113 60-140113 0 30500<10.0 565 564
Dibromomethane ug/L 500 107 60-140107 0 30500<7.8 535 535
Dichlorodifluoromethane ug/L 500 83 60-14084 1 30500<7.1 415 418
Diisopropyl ether ug/L 500 125 60-140128 2 30500<8.4 624 640
Ethylbenzene ug/L 500 115 60-140109 3 30500288864835
Hexachloro-1,3-butadiene ug/L 500 104 60-140106 2 30500<30.0 518 529
Isopropylbenzene
(Cumene)
ug/L 500 114 60-140118 3 3050012.9 585 604
m&p-Xylene ug/L 1000 117 60-140114 2 30100082419901960
Methyl-tert-butyl ether ug/L 500 122 60-140125 2 30500<11.1 610 624
Methylene Chloride ug/L 500 119 60-140124 4 30500<37.5 596 618
n-Butylbenzene ug/L 500 104 60-140111 7 30500<8.8 520 557
n-Propylbenzene ug/L 500 111 60-140111 1 3050025.9 579 582
Naphthalene ug/L 500 98 60-140106 7 3050059.3 550 588
o-Xylene ug/L 500 114 60-140111 1 3050046910401030
sec-Butylbenzene ug/L 500 113 60-140115 1 30500<6.2 566 574
Styrene ug/L 500 112 60-140114 2 3050019.8 580 591
tert-Butylbenzene ug/L 500 93 60-14095 2 30500<6.2 464 474
Tetrachloroethene ug/L 500 120 60-140115 4 30500<5.8 598 574
Toluene ug/L M150014360-140138 1 30500240031203090
trans-1,2-Dichloroethene ug/L 500 122 60-140123 0 30500<6.4 610 613
trans-1,3-Dichloropropene ug/L 500 119 60-140112 6 30500<9.8 596 562
Trichloroethene ug/L 500 113 60-140111 2 30500<5.8 567 557
Trichlorofluoromethane ug/L 500 113 60-140112 1 30500<8.4 565 561
Vinyl chloride ug/L 500 99 60-14098 1 30500<10.2 493 490
Xylene (Total)ug/L 1500 116 60-140113 1 301500129030302990
1,2-Dichloroethane-d4 (S)%94 70-13097
4-Bromofluorobenzene (S)%104 70-130102
Toluene-d8 (S)%101 70-130101
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 31
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92451624
Former Newton
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 31
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92451624
Former Newton
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92451624001 507132FB-1 SM 6200B
92451624002 507132MW-1SR SM 6200B
92451624003 507397MW-3 SM 6200B
92451624004 507397MW-4 SM 6200B
92451624005 507132MW-6 SM 6200B
92451624006 507132MW-8 SM 6200B
92451624007 507132MW-11 SM 6200B
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 11/05/2019 04:39 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 31
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