MO-4964_16910_CA_MRP_20200318

Groundwater Monitoring Report

Southland Oil Company and Oakdale Hardware
1832 and 1836 Oakdale Road
Charlotte, Mecklenburg County, North Carolina 28216
NCDENR Incident #16910 and #19678
ATC Project No. SLP1691005

March 18, 2020

Groundwater Monitoring Report March 18, 2020
Southland Oil Company and Oakdale Hardware Incident # 16910/19678 ATC Project No. SLP1691005

TABLE OF CONTENTS

1.0 SITE IDENTIFICATION .......................................................................................1
2.0 EXECUTIVE SUMMARY .....................................................................................3
3.0 SITE DESCRIPTION ..............................................................................................4
3.1 Site Characterization ................................................................................4
3.2 Site Background .......................................................................................4
3.3 Site and Regional Geology ......................................................................5
3.4 Site and Regional Hydrogeology .............................................................5
4.0 GROUNDWATER CHARACTERIZATION.......................................................6
4.1 Groundwater Levels .................................................................................6
4.2 Groundwater Quality ...............................................................................6
5.0 CONCLUSIONS AND RECOMMENDATIONS .................................................8

TABLES
Table 1 Water Supply Well Information
Table 2 Monitoring Well Construction Details
Table 3 Groundwater Elevation Data
Table 4 Groundwater Field Parameters
Table 5 Current Groundwater Analytical Results
Table 6 Historical Groundwater Analytical Results

FIGURES
Figure 1 Site Location Map
Figure 2 Water Supply Well Location Map
Figure 3 Site Map
Figure 4 Groundwater Elevation Contour Map
Figure 5 Contaminants of Concern

APPENDICES
Appendix A Field Notes
Appendix B Laboratory Analytical Report

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3. Information about Release

Date Discovered: Southland Oil Company: February 3, 1997
Estimated Quantity of Release: Unknown
Cause of Release: Former UST Systems
Source of Release (Dispenser/Piping/UST): Unknown
Sizes and contents of UST system(s) from which the release occurred: Unknown
Criteria Used to Classify Risk: Exceedance of 2L Standards and at least one potable water
supply well in use within 250 feet of the source area.

Date Discovered: Oakdale Hardware: March 22, 1999
Estimated Quantity of Release: Unknown
Cause of Release: Former UST Systems
Source of Release (Dispenser/Piping/UST): Unknown
Sizes and contents of UST system(s) from which the release occurred: Unknown
Criteria Used to Classify Risk: Exceedance of 2L Standards and potable water supply wells
within 1,000 feet of the source area.

4. Information about the Monitoring Report

Date of Groundwater Monitoring Events: December 19, 2019

5. Certification
I, Al Quarles, a Licensed Geologist for ATC Associates of North
Carolina, P.C., do certify that the information contained in this
report is correct and accurate to the best of my knowledge.

ATC Associates of North Carolina, P.C. is licensed to practice
engineering and geology in North Carolina. The certification
number of the company or corporation is C-1598 for engineering
and C-294 for geology.
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2.0 EXECUTIVE SUMMARY
ATC Associates of North Carolina, P.C. (ATC) has completed a Groundwater Monitoring Report
(GMR) documenting a December 19, 2019, monitoring event the Southland Oil Company and
Oakdale Hardware properties, located at 1832 and 1836 Oakdale Road, in Charlotte, Mecklenburg
County, North Carolina. The GMR is being performed based on a December 16, 2019, Task
Authorizations (TA-05) by the Trust Fund Branch of the Underground Storage Tank (UST) Section,
Division of Waste Management, North Carolina Department of Environment and Natural Resources
(NCDENR). The work is being performed as part of the State Lead Contract #N17004 between
NCDEQ and ATC.

Two adjoining properties (Southland Oil Company and Oakdale Hardware) utilized UST systems
installed in 1971 and 1976, respectively, which have been permanently closed by removal according
to the NCDEQ Registered UST Database. This GMR documents groundwater quality sampling for
volatile organic compounds (VOCs), including petroleum constituents, related to the former
petroleum release from the UST systems. The approved scope includes the sampling of sixteen
monitoring wells (MW-1, 2, 2R, 3, 4, 5, 5R, 6, 6R, 7, 7R, 8, 9, 10, and 11, and DW-1).

The findings from the monitoring event indicate the following:

 One active water supply well (WSW-100, located at 100 Radio Road) is located within 250
feet of the source area, and two community water supply wells (WSW-1918 and C-WSW,
located at 1120 James Street) are located within 1,000 feet of the source area.
 Monitoring wells MW-1, MW-3, MW-4, MW-11 and DW-1 could not be located.
Monitoring wells MW-2, MW-5, MW-6, MW-9 and MW-10 were dry or had insufficient
water to sample. Monitoring wells MW-2R, MW-5R, MW-6R, MW-7R and MW-8 were
sampled.
 Petroleum constituents were not detected above the laboratory detection limits in monitoring
wells MW-2R, MW-6R, or MW-8.
 Monitoring wells MW-5R and MW-7R contained multiple petroleum constituents at
concentrations above the 2L Standards. For the VOCs exceeding 2L Standards,
concentrations decreased for all VOCs in well MW-5R, while concentrations increased for
several VOCs and decreased for several VOCs in well MW-7R, compared to the February
7, 2019. The highest concentrations were detected in MW-7R.
 PCE was detected in MW-5R and MW-7R at concentrations exceeding the 2L Standard, and
TCE was detected in monitoring well MW-5R at a concentration exceeding the 2L
Standard. The source of the chlorinated solvents is not known. These chlorinated VOCs
were not detected previously in these two well, but was detected previously in monitoring
well MW-3 at concentrations less than the 2L Standard.
 None of the sampled monitoring wells contained VOCs at concentrations above GCLs.
 Groundwater flows to the west.

Based on these findings, ATC recommends the following, depending on available funding through
the Trust Fund Program:

 Continue to use ORS in wells MW-5R and MW-7R in an effort to reduced dissolved VOC
concentrations.
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 Conduct semi-annual groundwater sampling events of select monitoring wells and water
supply well WSW-100.
 Depending on the results of the above, consider pursuit of a municipal water connection
with the owner of the 100 Radio Road property.

3.0 SITE DESCRIPTION
3.1 Site Characterization
The NCDEQ retained ATC to provide environmental consulting services for the combined
Southland Oil Company and Oakdale Hardware sites, located at 1832 and 1836 Oakdale Road, in
Charlotte, Mecklenburg County, North Carolina. Figure 1 depicts the sites on a topographic map.
The former Southland Oil Company site currently operates as a refreshment/snack stand, and the
former Oakdale Hardware site operates as a dog grooming and boarding service.

Based on an updated receptor survey conducted in 2015, two inactive water supply wells and one
active drinking water supply well are located within 250 feet of the source areas, and one presumed
active drinking water supply well and two active community water supply wells are located between
250 and 1,000 feet of the source areas. Municipal water is available and in use at the site and most
surrounding properties. Information about the water supply wells is included in Table 1, and a map
depicting their locations is included as Figure 2.

3.2 Site Background
The former Southland Oil Company property (1832 Oakdale Road) previously operated one
6,000-gallon UST and one 4,000-gallon UST, both containing gasoline. The 4,000-gallon UST
was reported as removed on December 1, 1996, and the 6,000-gallon UST was reported as
removed on November 10, 1998.

The former Oakdale Hardware property (1836 Oakdale Road) previously operated one 2,000-
gallon gasoline UST, installed on March 6, 1976. The UST was reported as removed on
December 29, 1993.

In 1998, Carolina Environmental Associates and Nightingale Geologic Consultants, P.C.
prepared a Comprehensive Site Assessment (CSA) for the Southland Oil Company property,
which identified soil and groundwater contamination originating from a release from the UST
system. The CSA also identified 65 supply wells within 1,500 feet of the site.

In September, 1999, ATC performed groundwater monitoring at the site which identified impact
by petroleum constituents above 2L Standards in the monitoring well network associated with
the Southland Oil Company and Oakdale Hardware releases. Subsequent groundwater
monitoring events were performed by Force Environmental Service Company, LLC between
2008 and 2012. The groundwater monitoring reports indicated that many of the site’s monitoring
wells have been historically dry during groundwater monitoring events. Prior groundwater
monitoring indicates remaining impact by petroleum constituents.

In August 2014, ATC performed a groundwater monitoring event at the site with impact identified
in MW-1 and DW-1 above 2L Standards. Three water supply wells were also sampled in August
2014. The on-site water supply well WSW-Site (located at 1828 Oakdale Road) contained
Groundwater Monitoring Report March 18, 2020
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bromoform above the 2L Standard, and detectable concentrations of bromodichloromethane,
chlorodibromomethane, and chloroform below 2L Standards. Nearby water supply well WSW-100
(located at 100 Radio Road) contained MTBE and chloroform below 2L Standards, and community
water supply well WSW-1918 (located at 1120 James Street) contained bromodichloromethane,
chloroform, and tetrachloroethylene (PCE) below 2L Standards.

In December 2014, ATC installed groundwater monitoring wells MW-2R, MW-5R, MW-6R, and
MW-7R to replace historically dry wells. Monitoring wells MW-5R and MW-6R both contained
multiple petroleum constituents above 2L Standards.

ATC conducted an updated receptor survey in October 2015 and identified 11 properties with
water supply wells within 1,500 feet of the sites. Six of the properties with water supply wells
did not have an account with Charlotte-Mecklenburg Utilities Department. One of the identified
properties (located at 1120 James Street) reported the presence of two water supply wells, which
provides drinking water to a total of 46 residences. On behalf of the NCDEQ, ATC sent letters to
property owners at 100 Radio Road (WSW-100) and 1120 James Street (WSW-1918 and C-
WSW), offering to connect them to the municipal water system. The property representative
from 100 Radio Road declined, and a response was not received from the James Street property.
In August 2018, Mr. George Malone purchased the 100 Radio Road property, and the property is
used as a plant nursery (Malone’s Nursery).

From 2016 to present, ATC has conducted semi-annual groundwater sampling activities of select
monitoring wells, in rotation with installing and maintaining oxygen-releasing socks (ORS).
Concentrations of petroleum constituents have decreased with time but remain above 2L
Standards.

3.3 Site and Regional Geology

According to the Geologic Map of North Carolina, produced by the State of North Carolina in
1985, the site lies in the Charlotte Belt of the Piedmont Physiographic Province of North
Carolina. The rock type at the site has been identified as granite. The shallow subsurface in most
areas of the Piedmont contains residual soil overburden, including structure-free residuum, saprolite,
and partially weathered rock (PWR) that derive from in-place weathering of the crystalline bedrock.
Occasional areas containing recent deposits of alluvium in the uppermost subsurface are found near
streams and rivers. Saprolite and PWR typically contain some relict structures from the original
rock material. Depth to rock ranges from ground surface at occasional outcrops to depths of greater
than 100 feet in areas of easily weathered rock. No site specific geological conditions were available
at the time of reporting.

3.4 Site and Regional Hydrogeology
The shallow aquifer occurrence varies in depth from ground surface at springs, creeks, and rivers
to as deep as 50 feet or more beneath upland surfaces in some parts of the Piedmont. Water in the
alluvium or unconsolidated residual material, including saprolite and PWR, usually behaves as
an unconfined aquifer, or water table, and will yield water with head elevation equivalent to the
first elevation where water was encountered. Permeability varies with lithology and is typically
relatively low in residual soils, with higher permeability in saprolite or PWR due to relict rock
texture and variable susceptibility to weathering exhibited by different minerals in the rock.
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Groundwater flow in residual soils or alluvium is usually in rough concurrence with local
topographic conditions. Based on the data from the monitoring well network, shallow
groundwater flows generally to the west. Depth to water at the site ranges from approximately 29
to 31 feet below ground surface (ft bgs), based on the current GMR field data.

The bedrock fractures or other planar features of the Blue Ridge Physiographic Province
generally constitute the bedrock aquifer, with the surrounding rock material being effectively
impermeable. Along with fractures, contacts between rock bodies probably constitute zones of
significant groundwater occurrence in the bedrock. The surrounding material and overlying
residuum tend to make the bedrock aquifer a semi-confined aquifer. That is, the overlying water
and soil weight normally results in pressure that causes water in a borehole, which intersects a
fracture or other feature, to rise above the elevation of the fracture or feature. Modern water
supply wells in the Piedmont, likely including those in the site vicinity, are typically installed
with a surface casing through the unconsolidated material, and an open borehole into the bedrock
where water-bearing fractures are encountered.

4.0 GROUNDWATER CHARACTERIZATION
4.1 Groundwater Levels
On December 19, 2019, ATC conducted a comprehensive groundwater monitoring event. Of the
sixteen wells proposed for sampling, monitoring wells MW-2, MW-2R, MW-5, MW-5R, MW-6,
MW-6R, MW-7, MW-7R, MW-8, MW-9, and MW-10 were located and gauged for depth to
groundwater. Monitoring wells MW-1, MW-3, MW-4, MW-11, and DW-1 were not located.
Figure 3 depicts current site conditions and pertinent features. Table 2 includes monitoring well
construction details.

An electronic water level indicator was used to measure the depth to groundwater and total well
depth from the top of well casing (TOC). Groundwater elevation is then calculated based on
TOC elevations. Depth to groundwater and groundwater elevation data are summarized in Table
3. A groundwater contour map depicting groundwater flow is presented in Figure 4. Based on
the data obtained during the December 19, 2019, field activities, groundwater flows to the west.
Field notes from the December 19, 2019, groundwater monitoring event are presented in
Appendix A.

4.2 Groundwater Quality
On December 19, 2019, ATC collected groundwater samples from monitoring wells MW-2R, MW-
5R, MW-6R, MW-7R, and MW-8 for laboratory analysis. Monitoring wells MW-2, MW-5, MW-6,
MW-7, MW-9, and MW-10 were dry, or did not contain sufficient water for sample collection.

During sampling activities, the wells were purged of three standing well volumes, or purged dry and
allowed to recharge, prior to sample collection to ensure a representative groundwater sample. Prior
to purging wells MW-5R and MW-7R, ORS that were installed in June 2019 were removed.
Groundwater field parameters, including temperature, pH, conductivity, and dissolved oxygen
were measured at the time of sampling. Field parameters for each well are tabulated in Table 4.
Note that the elevated dissolved oxygen, specific conductance, and pH readings in wells MW-5R
and MW-7R are likely due to the prior ORS. Field notes are presented in Appendix A.

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The groundwater samples were collected in laboratory-supplied preserved containers; placed on ice;
entered into chain of custody control; and shipped to North Carolina accredited Pace Analytical
laboratory in Huntersville, North Carolina. The groundwater samples were analyzed by Standard
Method 6200B for VOCs including petroleum constituents. The groundwater analytical results were
compared to the 2L Standards and GCLs. Groundwater analytical results indicate the following:
 None of the sampled wells contained concentrations of VOCs above GCLs.
 Monitoring well MW-5R contained benzene, MTBE, naphthalene, and PCE at
concentrations above 2L Standards. Concentrations decreased compared to the February
2019 results.
 Monitoring well MW-7R contained benzene, toluene, total xylenes, MTBE, naphthalene,
PCE, and TCE at concentrations above 2L Standards. Several of the VOC concentrations
increased and several decreased compared to the February 2019 results.
 PCE was detected in monitoring well MW-5R and MW-7R at concentrations above the 2L
Standard, and TCE was detected in monitoring well MW-5R at a concentration above the
2L Standard. The source of the chlorinated solvents is not known. These chlorinated VOCs
were not detected previously in these two well, but was detected previously in monitoring
well MW-3 at concentrations less than the 2L Standard.
 Petroleum constituents were not detected above the laboratory detection limits in monitoring
wells MW-2R, MW-6R, or MW-8.
 Well MW-9 has been dry since March 2007. Well MW-10 was sampled in May 2011 and
August 2014, with no exceedances of the 2L Standards. When sampled, upgradient wells
MW-3 and MW-4 located between the site and the active drinking water supply wells
(WSW-100, WSW-1918, and C-WSW) did not contain VOCs exceeding laboratory
reporting limits (two VOCs reported at estimated concentrations).

Figure 5 depicts the groundwater quality for VOCs detected above the 2L Standards. Current
groundwater analytical results are summarized in Table 5. Historical groundwater analytical results
are shown in Table 6. The laboratory analytical report is included in Appendix B.

As compared to analytical data from February 2019, petroleum VOC concentrations appear to have
generally decreased in well MW-5R, while VOC concentrations increased and decreased in well
MW-7R. ORS were installed in both wells in June 2019, and the effectiveness does not appear
conclusive.

As part of ATC’s quality assurance and quality control (QA and QC) measures, a data review of the
laboratory reports was conducted. During the review, it was found that the samples were received
from the laboratory in acceptable condition and properly preserved. The samples were analyzed
within correct holding times and reported within the lab report, and the chain of custody was
properly completed by all parties. The laboratory QC report shows that an internal blank was
analyzed for each method that was used for the original samples. The laboratory fortified blank
(LFB) and laboratory control sample (LCS) data results were also provided for each analytical
method. Refer to the laboratory report in Appendix B for details regarding QA results for the
laboratory samples and any noted exceptions. Overall, ATC concludes that the laboratory results
provide reasonably valid and usable information.

Groundwater Monitoring Report March 18, 2020
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5.0 CONCLUSIONS AND RECOMMENDATIONS
On behalf of the Trust Fund Branch of the UST Section, ATC has completed a GMR
documenting a December 19, 2019, monitoring event for the Southland Oil Company and
Oakdale Hardware sites, located at 1832 and 1836 Oakdale Road, in Charlotte, Mecklenburg
County, North Carolina.

The findings from the monitoring event indicate the following:

 One active water supply well (WSW-100, located at 100 Radio Road) is located within 250
feet of the source area, and two community water supply wells (WSW-1918 and C-WSW,
located at 1120 James Street) are located within 1,000 feet of the source area.
 Monitoring wells MW-1, MW-3, MW-4, MW-11 and DW-1 could not be located.
Monitoring wells MW-2, MW-5, MW-6, MW-9 and MW-10 were dry or had insufficient
water to sample. Monitoring wells MW-2R, MW-5R, MW-6R, MW-7R and MW-8 were
sampled.
 Petroleum constituents were not detected above the laboratory detection limits in monitoring
wells MW-2R, MW-6R, or MW-8.
 Monitoring wells MW-5R and MW-7R contained multiple petroleum constituents at
concentrations above the 2L Standards. For the VOCs exceeding 2L Standards,
concentrations decreased for all VOCs in well MW-5R, while concentrations increased for
several VOCs and decreased for several VOCs in well MW-7R, compared to the February
7, 2019. The highest concentrations were detected in MW-7R.
 PCE was detected in MW-5R and MW-7R at concentrations exceeding the 2L Standard, and
TCE was detected in monitoring well MW-5R at a concentration exceeding the 2L
Standard. The source of the chlorinated solvents is not known. These chlorinated VOCs
were not detected previously in these two well, but was detected previously in monitoring
well MW-3 at concentrations less than the 2L Standard.
 None of the sampled monitoring wells contained VOCs at concentrations above GCLs.
 Groundwater flows to the west.

Based on these findings, ATC recommends the following, depending on available funding through
the Trust Fund Program:

 Continue to use ORS in wells MW-5R and MW-7R in an effort to reduced dissolved VOC
concentrations.
 Conduct semi-annual groundwater sampling events of select monitoring wells and water
supply well WSW-100.
 Depending on the results of the above, consider pursuit of a municipal water connection
with the owner of the 100 Radio Road property.

TABLES
TABLE 1
WATER SUPPLY WELL INFORMATION
SOUTHLAND OIL COMPANY and OAKDALE HARDWARE
1832 and 1836 Oakdale Road
Charlotte, North Carolina 26216
NCDENR Incident #16910 and #19678
Well Parcel ID Well Owners / Well Users Property Address Owner Address Distance from
Site (ft)
Well Use
(P/I/N)
Municipal Water
Connection (Y/N)
WSW-Site 3701302 Southland Oil Company 1828 Oakdale Road,
Charlotte, NC 28216
P.O. Box 11048,
Charlotte, NC 28220 Onsite N Y
WSW-100 3701311 Betty Zimmerman 100 Radio Road, Charlotte,
NC 28216
120 Shady Circle,
Charlotte, NC 28216 160 P N
WSW-1825 3516205 Board of Education, Charlotte
Mecklenburg
1825 Oakdale Road,
Charlotte, NC 28216
701 East 2nd Street,
Charlotte, NC 28202 200 N Y
WSW-1918 3702702 Carolina Water Service Inc. of North
Carolina
1120 James Street,
Charlotte, NC 28216
2335 Sanders Road,
Northbrook, IL 60062 820 P N
C-WSW 3702702 Carolina Water Service Inc. of North
Carolina
1120 James Street,
Charlotte, NC 28216
2335 Sanders Road,
Northbrook, IL 60062 820 P N
WSW-1618 3513512 Wade & Pansy Bennett 1618 Ronald Street,
Charlotte, NC 28216
1618 Ronald Street,
Charlotte, NC 28216 900 Unknown Y
WSW-20111 3316120 Pleasant Grove United Methodist
Church
2011 Oakdale Road,
Charlotte, NC 28216
1915 Oakdale Road,
Charlotte, NC 28216 928 N N
WSW-1604 3701406 Valencia Ross 1604 Oakdale Road,
Charlotte, NC 28216
1604 Oakdale Road,
Charlotte, NC 28216 1,100 I Y
WSW-1710 3513615 Ronald & Patti McGowan 1710 Ford Street, Charlotte,
NC 28216
1710 Ford Street,
Charlotte, NC 28216 1,150 P N
WSW- 1610 3513534 Foy & Kathleen Phillips 1610 Byrum Street,
Charlotte, NC 28216
1610 Byrum Street,
Charlotte, NC 28216 1,150 Unknown N
WSW-6210 3516203 Miguel A. Estrada & Lourdes
Arellano-Suarez
6210 Cora Street, Charlotte,
NC 28216
6210 Cora Street,
Charlotte, NC 29216 1,280 P N
WSW-1603 3513617 Nancy Lawson 1603 Byrum Street,
Charlotte, NC 28216
1603 Byrum Street,
Charlotte, NC 28216 1,450 N Y
WSW-6322 3516202 Jimmy Darryl & Jacqueline Benfield
Stogner
6322 Cora Street, Charlotte
NC 28216
6322 Cora Street,
Charlotte, NC 28216 1,500 P N
Notes:
Two water supply wells are located at C-WSW, which provide water to 46 residences (community wells).
P / I / N = Potable water supply / Irrigation / Not in use
Municipal water connections verified with Charlotte Mecklenburg Utilities
There are two wells associated with WSW-1918, are are community water supply wells that serve approximately 46 residences
1 - Identified by previous consultants, the property was observed as vacant and the water supply well was not identified
TABLE 2
MONITORING WELL CONSTRUCTION DETAILS
SOUTHLAND OIL COMPANY and OAKDALE HARDWARE
1832 and 1836 Oakdale Road
Charlotte, North Carolina 26216
NCDEQ Incident #16910
MW-1 5/10/1997 10-25 2 30 97.83
MW-2 9/19/1997 10-25 2 25 96.81
MW-2R 12/17/2014 25-35 2 35 95.11
MW-3 9/19/1997 10-25 2 25 98.33
MW-4 9/19/1997 10-25 2 25 96.1
MW-5 2/27/1998 10-25 2 25 98.91
MW-5R 12/17/2014 25-35 2 35 98.84
MW-6 2/27/1998 10-25 2 25 95.92
MW-6R 12/17/2014 25-35 2 35 93.53
MW-7 2/27/1998 10-25 2 25 98.15
MW-7R 12/17/2014 25-35 2 35 97.51
MW-8 7/6/1998 10-25 2 25 94.38
MW-9 7/6/1998 8.5-28.5 2 28.5 101.37
MW-10 7/6/1998 10-30 2 30 101.32
MW-11 Unknown Unknown 2 31 NA
DW-1 2/27/1998 53.5-58.5 2 58.5 97.89
Top of Casing
ElevationWell ID Date Installed Screen Interval (feet)Well Diameter
(inches)Total Depth (feet)
TABLE 3
GROUNDWATER ELEVATION DATA
SOUTHLAND OIL COMPANY and OAKDALE HARDWARE
1832 and 1836 Oakdale Road
Charlotte, North Carolina 26216
NCDEQ Incident #16910

2/27/1998 15.81 82.02
7/21/1998 20.38 77.45
7/28/1999 24.61 73.22
10/6/2008 28.54 69.29
5/20/2009 25.89 71.94
10/21/2009 DRY NA
3/18/2010 26.91 70.92
5/10/2011 26.94 70.89
3/7/2012 DRY NA
8/4/2014 25.75 72.08
12/19/2019 NF NA
2/27/1998 15.48 81.33
7/21/1998 20.08 76.73
7/28/1999 23.77 73.04
10/6/2008 DRY NA
5/20/2009 DRY NA
10/21/2009 DRY NA
3/18/2010 DRY NA
5/10/2011 24.76 72.05
3/7/2012 25.09 71.72
8/4/2014 24.71 72.10
12/19/2019 24.75 72.06
12/18/2014 29.05 66.06
10/5/2016 27.61 67.50
12/28/2017 31.84 63.27
2/7/2019 25.62 69.49
12/19/2019 26.75 68.36
2/27/1998 17.22 81.11
7/21/1998 21.05 77.28
7/28/1999 24.91 73.42
10/6/2008 DRY NA
5/20/2009 DRY NA
10/21/2009 DRY NA
3/18/2010 DRY NA
5/10/2011 24.91 73.42
3/7/2012 25.19 73.14
8/4/2014 24.89 73.44
12/19/2019 NF NA
MW-2R
MW-1 29.5 97.83
MW-2 25.15 96.81
Gauging Date Groundwater
Elevation Well ID TOC Elevation Depth to
GroundwaterTotal Well Depth
35 95.11
MW-3 25.5 98.33
Page 1 of 4
TABLE 3
GROUNDWATER ELEVATION DATA
SOUTHLAND OIL COMPANY and OAKDALE HARDWARE
1832 and 1836 Oakdale Road
Charlotte, North Carolina 26216
NCDEQ Incident #16910

Gauging Date Groundwater
Elevation Well ID TOC Elevation Depth to
GroundwaterTotal Well Depth
2/27/1998 13.06 83.04
7/21/1998 18.59 77.51
7/28/1999 22.57 73.53
10/6/2008 DRY NA
5/20/2009 DRY NA
10/21/2009 DRY NA
3/18/2010 DRY NA
5/10/2011 DRY NA
3/7/2012 DRY NA
8/4/2014 DRY NA
12/19/2019 NF NA
2/27/1998 18.20 80.71
7/21/1998 21.98 76.93
7/28/1999 23.71 75.20
10/6/2008 DRY NA
5/20/2009 DRY NA
10/21/2009 DRY NA
3/18/2010 DRY NA
5/10/2011 DRY NA
3/7/2012 24.25 74.66
8/4/2014 DRY NA
12/19/2019 23.80 75.11
12/18/2014 31.40 67.41
10/5/2016 34.54 64.27
12/28/2017 33.78 65.03
2/7/2019 29.01 69.80
12/19/2019 31.60 67.21
2/27/1998 14.93 80.99
7/21/1998 19.73 76.19
7/28/1999 23.27 72.65
10/6/2008 NM NA
5/20/2009 NM NA
10/21/2009 NM NA
3/18/2010 NM NA
5/10/2011 NM NA
3/7/2012 NM NA
8/4/2014 24.93 70.99
12/19/2019 24.68 71.24
12/18/2014 31.09 62.44
10/5/2016 26.99 66.54
12/28/2017 32.04 61.49
2/7/2019 24.70 68.83
12/19/2019 27.80 65.73
MW-6R
MW-5R
35 93.53
MW-4 25 96.10
MW-5 24.35 98.91
MW-6 25 95.92
35 98.81
Page 2 of 4
TABLE 3
GROUNDWATER ELEVATION DATA
SOUTHLAND OIL COMPANY and OAKDALE HARDWARE
1832 and 1836 Oakdale Road
Charlotte, North Carolina 26216
NCDEQ Incident #16910

Gauging Date Groundwater
Elevation Well ID TOC Elevation Depth to
GroundwaterTotal Well Depth
2/27/1998 17.30 80.85
7/21/1998 21.61 76.54
7/28/1999 24.28 73.87
10/6/2008 DRY NA
5/20/2009 DRY NA
10/21/2009 DRY NA
3/18/2010 DRY NA
5/10/2011 24.90 73.25
3/7/2012 DRY NA
8/4/2014 DRY NA
12/19/2019 24.90 73.25
12/18/2014 29.42 68.09
10/5/2016 27.61 69.90
12/28/2017 32.83 64.68
2/7/2019 30.91 66.60
12/19/2019 32.15 65.36
7/21/1998 17.72 76.66
7/28/1999 21.28 73.10
10/6/2008 DRY NA
5/20/2009 23.60 70.78
10/21/2009 24.77 69.61
3/18/2010 23.98 70.40
5/10/2011 23.87 70.51
3/7/2012 DRY NA
8/4/2014 22.53 71.85
12/19/2019 23.64 70.74
7/21/1998 25.27 76.10
7/28/1999 DRY NA
10/6/2008 DRY NA
5/20/2009 DRY NA
10/21/2009 DRY NA
3/18/2010 DRY NA
5/10/2011 DRY NA
3/7/2012 DRY NA
8/4/2014 DRY NA
12/19/2019 DRY NA
7/21/1998 25.18 76.14
7/28/1999 28.71 72.61
10/6/2008 DRY NA
5/20/2009 DRY NA
10/21/2009 DRY NA
3/18/2010 DRY NA
5/10/2011 29.81 71.51
3/7/2012 30.23 71.09
8/4/2014 29.72 71.60
12/19/2019 30.04 71.28
MW-7R 35
MW-7 25 98.15
MW-8 25 94.38
97.51
MW-9 28.5 101.37
MW-10 30.35 101.32
Page 3 of 4
TABLE 3
GROUNDWATER ELEVATION DATA
SOUTHLAND OIL COMPANY and OAKDALE HARDWARE
1832 and 1836 Oakdale Road
Charlotte, North Carolina 26216
NCDEQ Incident #16910

Gauging Date Groundwater
Elevation Well ID TOC Elevation Depth to
GroundwaterTotal Well Depth
7/28/1999 24.71 NA
10/6/2008 29.61 NA
5/20/2009 26.93 NA
10/21/2009 29.49 NA
3/18/2010 28.52 NA
5/10/2011 28.14 NA
3/7/2012 DRY NA
8/4/2014 NM NA
12/19/2019 NF NA
2/27/1998 16.04 81.85
7/21/1998 20.79 77.10
7/28/1999 24.71 73.18
10/6/2008 28.87 69.02
5/20/2009 28.42 69.47
10/21/2009 28.69 69.20
3/18/2010 30.55 67.34
5/10/2011 28.40 69.49
3/7/2012 28.50 69.39
8/4/2014 26.38 71.51
12/19/2019 NF NA
Notes:
TOC = Top of Casing
NM = Not Measured
NA = Not Available
NF = Not Found
All measurements expressed in feet
MW-11 31 NA
DW-1 58.5 97.89
Page 4 of 4
TABLE 4
GROUNDWATER FIELD PARAMETERS
SOUTHLAND OIL COMPANY and OAKDALE HARDWARE
1832 and 1836 Oakdale Road
Charlotte, North Carolina 26216
NCDENR Incident #16910 and #19678

Well ID Sample Date Time Temperature (C°)Specific Conductivity
(µS/cm)
Dissolved Oxygen
(mg/L)pH Oxidation Reduction
Potential (mV)
MW-2R 12/19/2019 12:40 18.43 0.133 4.14 9.16 76.0
MW-5R 12/19/2019 12:05 18.66 4.392 24.09 12.03 -13.9
MW-6R 12/19/2019 13:10 18.73 0.186 1.77 7.91 -97.3
MW-7R 12/19/2019 12:20 19.14 6.035 31.32 12.32 -4.0
MW-8 12/19/2019 13:25 18.77 0.19 3.72 6.54 75.0
Notes:
C° = Degrees Celcius
µS/cm = micro-Siemens per centimenter
mg/L = milligrams per Liter
mV = millivolts
TABLE 5
CURRENT GROUNDWATER ANALYTICAL RESULTS
SOUTHLAND OIL COMPANY and OAKDALE HARDWARE
1832 and 1836 Oakdale Road
Charlotte, North Carolina 26216
NCDEQ Incident #16910

Well ID Sample Date
BenzeneTolueneEthylbenzeneTotal XylenesMethyl Tertiary Butyl EtherNaphthaleneIsopropyl EtherIsopropylbenzenen-PropylbenzeneTetrachloroethyleneTrichloroethylene1,2,4-Trimethylbenzene1,3,5-Trimethylbenzene2-Butanone (MEK)cis-1,2-Dichloroethene2-HexanoneMW-1 12/19/2019
MW-2 12/19/2019 Dry
MW-2R 12/19/2019 <0.24 <0.23 <0.24 <0.50 <0.44 <0.66 <0.33 <0.24 <0.24 <0.23 <0.23 <0.19 <0.23 <3.6 <0.21 <0.60
MW-3 12/19/2019
MW-4 12/19/2019
MW-5 12/19/2019
MW-5R 12/19/2019 118 <1.1 16.8 80.1 761 15.7 10.1 <1.2 <1.2 3.0 <1.2 25.8 <1.1 54.4 <1.0 <3.0
MW-6 12/19/2019
MW-6R 12/19/2019 <0.24 <0.23 <0.24 <0.50 <0.44 <0.66 <0.33 <0.24 <0.24 <0.23 <0.23 <0.19 <0.23 <3.6 <0.21 <0.60
MW-7 12/19/2019
MW-7R 12/19/2019 463 961 273 1710 510 125 4.0 15.7 31.8 15.9 3.2 314 51.5 182 3.2 311
MW-8 12/19/2019 <0.24 <0.23 <0.24 <0.50 <0.44 <0.66 <0.33 <0.24 <0.24 <0.23 <0.23 <0.19 <0.23 <3.6 <0.21 <0.60
MW-9 12/19/2019
MW-10 12/19/2019
MW-11 12/19/2019
DW-1 12/19/2019
1 600 600 500 20 6 70 70 70 0.7 3 400 400 4,000 70 40
5,000 260,000 84,500 85,500 20,000 6,000 7,000 25,000 30,000 700 3,000 28,500 25,000 4,000,000 70,000 40,000
Notes:
Concentrations are reported in micrograms per liter (µg/l).J = Estimated value above or equal to Method Detection Limit and less than Quantification Limit.
< = Not detected at or above the laboratory detection limit Values in BOLD print indicate levels above 2L Standards
GCL = Gross Contamination Level
Not Located
Not Located
Not Located
Dry
Dry
Dry
2L Standard (ug/l)
GCL (ug/l)
Dry
Not Located
Not Located
Dry
TABLE 6
HISTORICAL GROUNDWATER ANALYTICAL RESULTS
SOUTHLAND OIL COMPANY and OAKDALE HARDWARE
1832 and 1836 Oakdale Road
Charlotte, North Carolina 26216
NCDEQ Incident #16910
BenzeneTolueneEthylbenzeneTotal XylenesMethyl Tertiary Butyl EtherIsopropyl EtherChloromethaneNaphthaleneChloroformp-IsopropyltolueneMethylene ChlorideTetrachloroethene (PCE)1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzenen-Propylbenzenen-Butylbenzenesec-Butylbenzenetert-Butylbenzene2-Butanone (MEK)4-Methyl-2-pentanone (MIBK)Acetone1 600 600 500 20 70 3 6 70 25.0 5 0.7 400 400 70 70 70 70 70 4,000 100 6,000
5,000 260,000 84,500 85,500 20,000 70,000 3,000 6,000 70,000 11,700 5,000 700 28,500 25,000 25,000 30,000 6,900 8,500 15,000 4,000,000 100,000 6,000,000
3/29/2005 6,500 27,000 2,800 15,200 2,400 <500 ND <2000 ND --ND ND 2,800 <500 <500 <500 <500 <500 --------
11/29/2005 6,500 24,000 2,500 14,600 930 <500 ND <2000 ND --ND ND 3,300 1,000 <500 <500 <500 <500 --------
3/8/2007 84 7,900 2,600 14,200 37 J ND ND 640 ND --ND ND 2,800 850 110 320 ND ND --------
3/13/2007 73.1 450 916 5,290 ND ND ND 692 ND --ND ND 2,650 904 124 297 ND ND --------
4/29/2008 25 403 1,140 4,260 5.5 ND ND 302 <5.0 --ND <5.0 1,140 397 52 130 ND ND --------
10/6/2008 1.7 1.0 11.1 15.9 <0.5 <0.5 <0.5 5.9 <0.5 --<2.0 <0.5 24.7 8.7 <0.5 3.1 <0.5 <0.5 --------
5/20/2009 3.2 213 1270 6,780 <0.5 <0.5 <1.0 718 <0.5 --<2.0 <0.5 1,580 406 113 164 <0.5 <0.5 --------
10/21/2009 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry ------
3/18/2010 42 140 180 360 <0.5 <0.5 0.59 J 56 <0.5 --<2.0 <0.5 230 95 19 46 <0.5 <0.5 --------
8/26/2010 6.4 8.0 160 300 <0.50 <0.50 <0.50 89 <0.50 3.1 <0.50 <0.50 210 5.0 15 25 3.9 <0.50 --------
5/10/2011 1.4 0.77 2.4 5.9 <0.5 <0.5 <0.5 1.6 <0.5 <0.5 <0.5 <0.5 2.5 2.1 <0.5 <0.5 <0.5 <0.5 <0.5 ------
8/4/2014 <7.9 25 J 150 840 <9.0 <18 <32 <12 <14 <12 <320 <8.0 1,400 370 57 130 25 J <8.4 <9.6 ------
12/19/2019 CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL
3/29/2005 95 25 12 113 530 ND ND 49 ND --ND ND 83 ND 3.8 9.0 51 6.0 --------
3/8/2007 1 0.32 J 0.36 J 4.4 360 7.1 ND ND ND --ND ND 2.2 17 ND ND ND ND --------
9/13/2007 ND 3.2 0.8 4.03 96.9 1.5 ND ND ND --ND ND 2.9 3.9 ND ND ND ND --------
4/29/2008 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
9/12/2008 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
5/20/2009 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
10/21/2009 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
3/18/2010 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
8/26/2010 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
5/10/2011 <0.5 0.48 J <0.5 0.55 4.9 <0.5 <0.5 1.2 <0.5 <0.5 <0.5 <0.5 1.1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ------
8/4/2014 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
12/19/2019 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
12/18/2014 0.82 0.40 J <0.092 1 1 <0.18 <0.32 <0.12 <0.14 <0.12 <3.2 <0.080 1 <0.10 <0.11 <0.094 <0.054 <0.084 1 --<1.9 6.2 J
10/5/2016 <0.12 <0.17 <0.13 <0.39 <0.090 <0.18 <0.55 <0.12 0.38 J <0.15 <3.2 <0.27 <0.18 <0.13 <0.12 <0.13 <0.15 <0.13 <0.12 --<1.5 <4.9
12/28/2017 <0.13 0.33 J 0.25 J 1.5 <0.13 <0.13 <0.20 0.23 J 0.32 J <0.13 <1.0 <0.13 0.67 0.33 J <0.13 <0.13 <0.13 <0.13 <0.13 --<1.3 <2.0
02/07/2019 ND ND ND ND ND ND ND ND ND --ND ND ND ND ND ND ND ND ND ------
12/19/2019 <0.24 <0.23 <0.24 <0.50 <0.44 <0.33 <0.42 <0.66 <0.35 --<1.5 <0.23 <0.19 <0.23 <0.24 <0.24 <0.35 <0.25 <0.25 <3.6 ----
2L Standard
GCL Standard
Concentrations in ug/L
MW-2R
MW-2
Well ID Sample
Date
MW-1
Page 1 of 5
TABLE 6
HISTORICAL GROUNDWATER ANALYTICAL RESULTS
SOUTHLAND OIL COMPANY and OAKDALE HARDWARE
1832 and 1836 Oakdale Road
Charlotte, North Carolina 26216
NCDEQ Incident #16910
BenzeneTolueneEthylbenzeneTotal XylenesMethyl Tertiary Butyl EtherIsopropyl EtherChloromethaneNaphthaleneChloroformp-IsopropyltolueneMethylene ChlorideTetrachloroethene (PCE)1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzenen-Propylbenzenen-Butylbenzenesec-Butylbenzenetert-Butylbenzene2-Butanone (MEK)4-Methyl-2-pentanone (MIBK)Acetone1 600 600 500 20 70 3 6 70 25.0 5 0.7 400 400 70 70 70 70 70 4,000 100 6,000
5,000 260,000 84,500 85,500 20,000 70,000 3,000 6,000 70,000 11,700 5,000 700 28,500 25,000 25,000 30,000 6,900 8,500 15,000 4,000,000 100,000 6,000,000
2L Standard
GCL Standard
Concentrations in ug/L
Well ID Sample
Date
3/29/2005 ND ND ND ND ND ND ND ND ND --ND ND ND ND ND ND ND ND --------
3/8/2007 ND ND ND ND ND ND ND ND ND --ND 0.57 ND ND ND ND ND ND --------
9/13/2007 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
4/29/2008 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
9/12/2008 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
5/20/2009 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
10/21/2009 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
3/18/2010 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
8/26/2010 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
5/10/2011 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.33 J <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ------
8/4/2014 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
12/19/2019 CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL
3/8/2007 ND ND ND ND 0.29 J ND ND ND ND --ND ND ND ND ND ND ND ND --------
9/13/2007 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
4/29/2008 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
9/12/2008 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
5/20/2009 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
10/21/2009 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
3/18/2010 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
8/26/2010 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
5/10/2011 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
8/4/2014 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
12/19/2019 CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL
3/8/2007 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
9/13/2007 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
4/29/2008 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
9/12/2008 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
5/20/2009 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
10/21/2009 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
3/18/2010 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
8/26/2010 31 28 3.3 42 130 1.7 0.49 J 1.8 <0.50 --<0.50 <0.50 17 34 0.50 0.78 <0.50 <0.50 --------
8/10/2011 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
8/4/2014 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
12/19/2019 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
MW-5
MW-3
MW-4
Page 2 of 5
TABLE 6
HISTORICAL GROUNDWATER ANALYTICAL RESULTS
SOUTHLAND OIL COMPANY and OAKDALE HARDWARE
1832 and 1836 Oakdale Road
Charlotte, North Carolina 26216
NCDEQ Incident #16910
BenzeneTolueneEthylbenzeneTotal XylenesMethyl Tertiary Butyl EtherIsopropyl EtherChloromethaneNaphthaleneChloroformp-IsopropyltolueneMethylene ChlorideTetrachloroethene (PCE)1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzenen-Propylbenzenen-Butylbenzenesec-Butylbenzenetert-Butylbenzene2-Butanone (MEK)4-Methyl-2-pentanone (MIBK)Acetone1 600 600 500 20 70 3 6 70 25.0 5 0.7 400 400 70 70 70 70 70 4,000 100 6,000
5,000 260,000 84,500 85,500 20,000 70,000 3,000 6,000 70,000 11,700 5,000 700 28,500 25,000 25,000 30,000 6,900 8,500 15,000 4,000,000 100,000 6,000,000
2L Standard
GCL Standard
Concentrations in ug/L
Well ID Sample
Date
12/18/2014 2,300 140 580 2,840 3,200 36 <16 <6.0 <7.2 <6.2 <160 <4.0 820 38 <5.6 64 <2.7 <4.2 <4.8 ----<230
10/5/2016
12/28/2017 270 <6.3 46.2 163 1,830 21.3 J <6.3 24.1 J <0.13 <0.13 <1.0 <0.13 50.2 11.4 J <6.3 <6.3 <6.3 <6.3 <6.3 --<63 <100
02/07/2019 213 ND 51.9 200 1100 16.3 ND 40.8 ND --ND ND 103 ND ND ND ND ND ND ------
12/19/2019 118 <1.1 16.8 80.1 761 10.1 <2.1 15.7 <1.8 --<7.5 3.0 25.8 <1.1 <1.2 <1.2 <1.8 <1.2 <1.2 54.4 ----
3/8/2007 1,900 880 220 1,320 2,500 7.1 J ND 150 ND --ND ND 570 390 40 100 ND ND --------
9/13/2007 CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL
4/29/2008 CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL
9/12/2008 CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL
5/20/2009 CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL
10/21/2009 CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL
3/18/2010 CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL
8/26/2010 CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL
5/10/2011 CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL
8/4/2014 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
12/19/2019 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
12/18/2014 1,800 3,400 1,200 6,800 900 <9.0 <16 730 <7.2 <6.2 <160 <4.0 1,700 260 45 190 92 <4.2 <4.8 ----780 J
10/5/2016 <0.60 <0.85 <0.65 <1.96 0.60 J <0.90 <2.8 <0.60 <1.1 <0.75 <16 <1.4 <0.90 <0.65 <0.60 <0.65 <0.75 <0.65 <0.60 --<7.3 <24
11/18/2016 <0.60 <0.85 10 <1.96 <0.45 <0.90 <2.8 <0.60 <1.1 <0.75 <16 <1.4 <0.90 <0.65 <0.75 <0.65 <0.75 <0.65 <0.60 --<7.3 860
12/28/2017 <0.13 0.28 J 0.35 J 0.31 J <0.13 <0.13 <0.20 <0.13 <0.13 <0.13 <1.0 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 <0.13 --<1.3 3.9 J
02/07/2019 0.35J ND ND ND ND ND ND ND ND --ND ND ND ND ND ND ND ND ND ------
12/19/2019 <0.24 <0.23 <0.24 <0.50 <0.44 <0.33 <0.42 <0.66 <0.35 --<1.5 <0.23 <0.19 <0.23 <0.24 <0.24 <0.35 <0.25 <0.25 ------
11/29/2005 65 110 52 130 130 ND ND 100 ND --ND ND 540 130 15 32 ND ND --------
3/8/2007 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
9/13/2007 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
4/29/2008 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
9/12/2008 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
5/20/2009 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
10/21/2009 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
3/18/2010 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
8/26/2010 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
5/10/2011 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
8/4/2014 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
12/19/2019 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
MW-6R
MW-6
Insufficient Water for Sample Collection
MW-5R
MW-7
Page 3 of 5
TABLE 6
HISTORICAL GROUNDWATER ANALYTICAL RESULTS
SOUTHLAND OIL COMPANY and OAKDALE HARDWARE
1832 and 1836 Oakdale Road
Charlotte, North Carolina 26216
NCDEQ Incident #16910
BenzeneTolueneEthylbenzeneTotal XylenesMethyl Tertiary Butyl EtherIsopropyl EtherChloromethaneNaphthaleneChloroformp-IsopropyltolueneMethylene ChlorideTetrachloroethene (PCE)1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzenen-Propylbenzenen-Butylbenzenesec-Butylbenzenetert-Butylbenzene2-Butanone (MEK)4-Methyl-2-pentanone (MIBK)Acetone1 600 600 500 20 70 3 6 70 25.0 5 0.7 400 400 70 70 70 70 70 4,000 100 6,000
5,000 260,000 84,500 85,500 20,000 70,000 3,000 6,000 70,000 11,700 5,000 700 28,500 25,000 25,000 30,000 6,900 8,500 15,000 4,000,000 100,000 6,000,000
2L Standard
GCL Standard
Concentrations in ug/L
Well ID Sample
Date
12/18/2014 0.68 2.9 1.2 8.6 <0.090 <0.18 <0.32 <0.12 <0.14 <0.12 <3.2 <0.080 4.4 0.46 J <0.11 0.30 J 1.5 <0.084 <0.096 ----<4.7
10/5/2016 1300 3,100 860 6,100 860 <9.0 <28 390 <11 24 J <160 <14 1,600 490 170 170 58 8.5 <6.0 --<73 <240
11/18/2016 1,000 1,900 470 3,300 1100 9.5 <14 340 <5.5 69 <80 <6.8 900 360 94 120 91 60 <3.0 --<37 510
12/28/2017 960 2260 938 4800 <6.3 <6.3 <10 435 <6.3 <6.3 <50 <6.3 1470 294 54.8 184 14.5 J 9.4 J <6.3 --135 <100
02/07/2019 393 902 318 1668 524 3.8 ND 185 ND --ND ND 407 55.5 19.3 54.5 ND ND ND ------
12/19/2019 463 961 273 1710 510 4.0 <2.1 125 <1.8 --<7.5 15.9 314 51.5 15.7 31.8 <1.8 <1.2 <1.2 182 ----
3/8/2007 11 ND ND 6.8 1.9 0.60 ND 5.9 ND --ND ND 4.8 ND 3.3 ND ND ND --------
9/13/2007 4 ND 25.3 ND ND ND ND 10.4 ND --ND ND 18.4 ND ND 8.5 ND ND --------
4/29/2008 Dry Dry Dry Dry Dry Dry Dry Dry Dry --Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
9/12/2008 Dry Dry Dry Dry Dry Dry Dry Dry Dry --Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
5/20/2009 1 0.52 2.3 2.2 <0.5 <0.5 <1.0 10.6 <0.5 --<2.0 <0.5 11.8 2.5 2.0 1.8 <0.5 <0.5 --------
10/21/2009 2 0.61 1.7 0.69 <0.5 <0.5 <1 <2.0 <0.5 --<2.0 <0.5 0.95 <0.5 <0.5 0.83 <0.5 0.99 --------
3/15/2010 44 120 22 73 1.0 <0.5 <1.0 16 0.17 J --<2.0 <0.5 39 12 1.6 6.1 2.8 1.3 --------
8/26/2010 0.15 J 0.59 2.2 1.06 <0.50 <0.50 <0.50 8.0 <0.50 3 <0.50 <0.50 3.3 0.82 1.0 0.91 <0.50 2.8 --------
5/10/2011 <0.5 0.51 1.1 1.01 J <0.5 <0.5 <0.5 2.6 <0.5 <0.5 <0.5 <0.5 2.7 1.1 0.59 <0.5 2.7 1.6 <0.5 ------
8/4/2014 0.16 J 0.22 J 0.44 J 0.99 J <0.090 <0.18 <0.32 7.2 <0.14 3.7 <3.2 <0.080 2.0 0.53 0.56 0.25 J 3.9 1.2 0.38 J ------
12/19/2019 <0.24 <0.23 <0.24 <0.50 <0.44 <0.33 <0.42 <0.66 <0.35 --<1.5 <0.23 <0.19 <0.23 <0.24 <0.24 <0.35 <0.25 <0.25 <3.6 ----
3/8/2007 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
9/13/2007 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
4/29/2008 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
9/12/2008 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
5/20/2009 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
10/21/2009 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
3/18/2010 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
8/26/2010 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
5/10/2011 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
8/4/2014 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
12/19/2019 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
3/8/2007 ND ND ND ND 1.5 ND ND ND 0.33 J --ND ND ND ND ND ND ND ND --------
9/13/2007 ND ND ND ND 1.3 ND ND ND ND --ND ND 0.59 ND ND ND ND ND --------
4/29/2008 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
9/12/2008 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
5/20/2009 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
10/21/2009 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
3/18/2010 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
8/26/2010 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
5/10/2011 <0.5 0.26 J <0.5 <0.5 0.92 <0.5 <0.5 <0.5 0.7 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ------
8/4/2014 <0.079 <0.090 <0.092 <0.29 0.69 <0.18 <0.32 <0.12 0.44 J <0.12 <3.2 <0.080 <0.18 <0.10 <0.11 <0.094 <0.054 <0.084 <0.096 ------
12/19/2019 Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry Dry
MW-10
MW-9
MW-7R
MW-8
Page 4 of 5
TABLE 6
HISTORICAL GROUNDWATER ANALYTICAL RESULTS
SOUTHLAND OIL COMPANY and OAKDALE HARDWARE
1832 and 1836 Oakdale Road
Charlotte, North Carolina 26216
NCDEQ Incident #16910
BenzeneTolueneEthylbenzeneTotal XylenesMethyl Tertiary Butyl EtherIsopropyl EtherChloromethaneNaphthaleneChloroformp-IsopropyltolueneMethylene ChlorideTetrachloroethene (PCE)1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneIsopropylbenzenen-Propylbenzenen-Butylbenzenesec-Butylbenzenetert-Butylbenzene2-Butanone (MEK)4-Methyl-2-pentanone (MIBK)Acetone1 600 600 500 20 70 3 6 70 25.0 5 0.7 400 400 70 70 70 70 70 4,000 100 6,000
5,000 260,000 84,500 85,500 20,000 70,000 3,000 6,000 70,000 11,700 5,000 700 28,500 25,000 25,000 30,000 6,900 8,500 15,000 4,000,000 100,000 6,000,000
2L Standard
GCL Standard
Concentrations in ug/L
Well ID Sample
Date
3/29/2005 3,600 12,000 2,400 11,200 4,900 52 ND 600 ND --ND ND 2,400 ND 650 290 210 ND ND ------
11/29/2005 6,700 21,000 2,900 14,400 1,100 <250 ND <1000 ND --ND ND 4,000 1,200 <250 <250 <250 <250 ND ------
3/8/2007 370 1,400 960 3,700 480 6.1 ND 330 ND --ND ND 2,700 880 110 370 ND ND ND ------
9/13/2007 1,100 4,020 864 4,330 649 ND ND 286 ND --ND ND 1,420 457 ND 148 ND ND ND ------
4/29/2008 805 1,300 733 2,100 697 20 <5.0 251 <2.5 --ND <2.5 851 400 61.1 144 ND ND ND ------
10/6/2008 2.5 9.1 5.3 22.2 <0.5 <0.5 <1.0 4.5 <0.5 --<2.0 <0.5 20.9 6.1 <0.5 3.0 <0.5 <0.5 3.1 ------
5/20/2009 0.99 <0.5 1.3 4.2 <0.5 <0.5 <1.0 5.0 <0.5 --<2.0 <0.5 3.2 0.62 <0.5 <0.5 <0.5 <0.5 <0.5 ------
10/21/2009 3.5 1.8 5.4 14.6 <0.5 <0.5 <1 <2.0 <0.5 --<2.0 <0.5 7.1 1.4 <0.5 1.1 <0.5 <0.5 <0.5 ------
3/18/2010 1.2 3.1 0.79 2.1 <0.5 <0.5 <1.0 1.4 <0.5 --<2.0 <0.5 2.0 0.48 J <0.5 0.38 J <0.5 <0.5 <0.5 ------
8/26/2010 2.5 3.4 2.0 4.9 1.3 <0.50 <0.50 2.9 <0.50 0.12 J <0.50 <0.50 70 1.2 0.59 2.4 <0.50 <0.50 <0.50 ------
5/10/2011 4.2 2.6 4.3 4.9 9 <0.5 <0.5 9.8 <0.5 <0.5 <0.5 <0.5 4.2 <0.5 1.6 4.2 <0.5 <0.5 <0.5 ------
8/4/2014 CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL
12/19/2019 CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL
3/29/2005 2.0 6.2 ND 3.2 36 0.5 ND ND ND --ND ND ND ND ND ND ND ND --------
11/29/2005 1.9 ND ND ND 42 ND ND ND ND --ND ND ND ND ND ND ND ND --------
3/8/2007 7.8 0.92 ND 8.7 26 ND ND 1.4 J ND --ND ND 7.9 ND 0.53 ND ND ND --------
9/13/2007 9.8 ND ND 9.9 26.3 ND ND 3.4 ND --ND ND 12.1 ND 0.93 ND ND ND --------
4/29/2008 35.6 ND ND 14.1 40.2 0.61 ND 7.7 ND --ND <0.50 22.0 ND 3.3 1.8 0.97 ND --------
10/6/2008 43.9 <0.5 <0.5 10.2 42.2 0.91 <1.0 4.1 <0.5 --<2.0 <0.5 6.1 <0.5 <0.5 <0.5 <0.5 <0.5 --------
5/20/2009 55.0 <0.5 0.53 16.5 54.4 1.5 <1.0 10.1 <0.5 --<2.0 <0.5 16.9 <0.5 1.4 0.73 <0.5 <0.5 --------
10/21/2009 74.6 <0.5 <0.5 14.2 46.9 1.7 <1.0 10.4 <0.5 --<2.0 <0.5 18.1 3.1 1.1 0.63 <0.5 <0.5 --------
3/18/2010 190.0 340 55 180 34 1.9 1 27.0 <5.0 --<0.5 <0.5 81 20 6.1 12 3.5 <0.5 --------
8/26/2010 92 0.24 J <0.50 14.8 37 2.1 <0.50 8.4 <0.50 --<0.50 <0.50 22 1.9 3.6 2.3 1.1 0.61 --------
5/10/2011 71 <0.5 <0.5 16.9 27 1.8 <0.5 8 <0.5 <0.5 <0.5 <0.5 19 <0.5 2.9 2.3 1.1 0.53 --------
8/4/2014 4.9 0.5 0.18 J 3.74 J 6.6 0.28 J <0.32 <0.12 <0.14 <0.12 <3.2 <0.080 3.6 0.16 J 0.34 J 0.21 J 0.13 J 0.11 J <0.096 ------
12/19/2019 CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL CNL
Notes:
ND = Not detected at or above the laboratory detection limit J = Estimated value below method reporting limit
CNL = Could Not Locate Values in BOLD print indicate levels above 2L Standards
GCL = Gross Contamination Level -- = Constituent not analyzed
Underlined values indicate detection limit is above 2L Standard due to dilution.
MW-11
DW-1
Page 5 of 5

FIGURES
1,500'1,000'500'LEGENDWATER SUPPLYWELL LOCATIONPROJECT NO.
NOTES:
DATE
TITLE
SCALEREV. BYPREP. BYCAD FILE WSW-1918*1120 James StreetSource: NC GeospatialDatabaseOakdale RoadWSW-100100 Radio RoadWSW-Site1828 Oakdale RoadWSW-16041604 Oakdale RoadRadio RoadPleasant Grove Road1. * WSW-1918 refers to the community water
supply well located at 1120 James Street. The
water supply well sample was collected at 1918
Oakdale Road, which is provided water from the
community well.SITEWSW-20112011 Oakdale Road2. Previously identified water supply well
WSW-2011 was observed as a vacant lot and no
water supply well was identified at the property.WSW-18251825 Oakdale RoadWSW-62106210 Cora StreetWSW-63226322 Cora Street
Former
Oakdale HardwareFormerSouthland OilCompanyOakdaleElementary SchoolMW-10MW-9MW-7MW-6MW-8MW-4MW-2MW-5MW-11DW-1MW-1MW-3OAKDALEROADMW-6RMW-2RMW-7RMW-5RASSOCIATES OF NORTH CAROLINA, P.C.
[phone] FAX [phone]
PROJECT NO.
Charlotte, North Carolina 28273
NOTES:
DATE
TITLE
SCALEREV. BYPREP. BYCAD FILE
1. Groundwater samples collected
December 19, 2019.
2. Deep aquifer well not used in
contour.
3. Dashed areas indicate areas of
less certainty.70.7465.7368.3665.36NMNMNMNMNMNMNMNMNMNM67.2170.068.066.064.067.21NMLEGENDTYPE II MONITORING WELLTYPE III MONITORING WELLGROUNDWATER ELEVATIONIN FEET
NOT MEASUREDGROUNDWATER ELEVATIONCONTOUR (DASHED WHEREINFERRED)GROUNDWATER FLOWDIRECTION
NM4
Former
Oakdale HardwareFormerSouthland OilCompanyOakdaleElementary SchoolMW-10MW-9MW-7MW-6MW-8MW-4MW-2MW-5MW-11DW-1MW-1MW-3OAKDALEROADMW-6RMW-2RMW-7RMW-5RASSOCIATES OF NORTH CAROLINA, P.C.
[phone] FAX [phone]
PROJECT NO.
Charlotte, North Carolina 28273
NOTES:
DATE
TITLE
SCALEREV. BYPREP. BYCAD FILE
1. Groundwater samples collected on
December 19, 2019.
2. Concentrations shown exceed 2L
Standards.CNLLEGENDTYPE II MONITORING WELLTYPE III MONITORING WELLCOULD NOT LOCATENS

APPENDIX A

FIELD NOTES

APPENDIX B

LABORATORY ANALYTICAL REPORT
#=CL#
December 31, 2019
LIMS USE: FR - ERIN GREENE
LIMS OBJECT ID: 92458367
92458367
Project:
Pace Project No.:
RE:
Erin Greene
ATC Group
7606 Whitehall Executive Cente
Suite 800
Charlotte, NC 28273
Southland Oil
Dear Erin Greene:
Enclosed are the analytical results for sample(s) received by the laboratory on December 20, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni for
[e-mail]
Project Manager
Taylor Ezell
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 30
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92458367
Southland Oil
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 30
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92458367
Southland Oil
Lab ID Sample ID Matrix Date Collected Date Received
92458367001 MW-2R Water 12/19/19 12:40 12/20/19 12:10
92458367002 MW-5R Water 12/19/19 12:05 12/20/19 12:10
92458367003 MW-6R Water 12/19/19 13:10 12/20/19 12:10
92458367004 MW-7R Water 12/19/19 12:20 12/20/19 12:10
92458367005 Field Blank Water 12/19/19 13:30 12/20/19 12:10
92458367006 MW-8 Water 12/19/19 13:25 12/20/19 12:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 30
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92458367
Southland Oil
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92458367001 MW-2R SM 6200B 66 PASI-CCL
92458367002 MW-5R SM 6200B 66 PASI-CCL
92458367003 MW-6R SM 6200B 66 PASI-CCL
92458367004 MW-7R SM 6200B 66 PASI-CCL
92458367005 Field Blank SM 6200B 66 PASI-CCL
92458367006 MW-8 SM 6200B 66 PASI-CCL
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92458367
Southland Oil
Sample:MW-2R Lab ID:92458367001 Collected:12/19/19 12:40 Received:12/20/19 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Benzene <0.24 ug/L 12/29/19 17:04 71-43-20.50 0.24 1
Bromobenzene <0.22 ug/L 12/29/19 17:04 108-86-10.50 0.22 1
Bromochloromethane <0.26 ug/L 12/29/19 17:04 74-97-50.50 0.26 1
Bromodichloromethane <0.18 ug/L 12/29/19 17:04 75-27-40.50 0.18 1
Bromoform <0.40 ug/L 12/29/19 17:04 75-25-20.50 0.40 1
Bromomethane <1.7 ug/L 12/29/19 17:04 74-83-95.0 1.7 1
2-Butanone (MEK)<3.6 ug/L 12/29/19 17:04 78-93-35.0 3.6 1
n-Butylbenzene <0.35 ug/L 12/29/19 17:04 104-51-80.50 0.35 1
sec-Butylbenzene <0.25 ug/L 12/29/19 17:04 135-98-80.50 0.25 1
tert-Butylbenzene <0.25 ug/L 12/29/19 17:04 98-06-60.50 0.25 1
Carbon tetrachloride <0.23 ug/L 12/29/19 17:04 56-23-50.50 0.23 1
Chlorobenzene <0.22 ug/L 12/29/19 17:04 108-90-70.50 0.22 1
Chloroethane <0.58 ug/L 12/29/19 17:04 75-00-31.0 0.58 1
Chloroform <0.35 ug/L 12/29/19 17:04 67-66-30.50 0.35 1
Chloromethane <0.42 ug/L 12/29/19 17:04 74-87-31.0 0.42 1
2-Chlorotoluene <0.21 ug/L 12/29/19 17:04 95-49-80.50 0.21 1
4-Chlorotoluene <0.21 ug/L 12/29/19 17:04 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane <0.38 ug/L 12/29/19 17:04 96-12-81.0 0.38 1
Dibromochloromethane <0.40 ug/L 12/29/19 17:04 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)<0.23 ug/L 12/29/19 17:04 106-93-40.50 0.23 1
Dibromomethane <0.31 ug/L 12/29/19 17:04 74-95-30.50 0.31 1
1,2-Dichlorobenzene <0.24 ug/L 12/29/19 17:04 95-50-10.50 0.24 1
1,3-Dichlorobenzene <0.25 ug/L 12/29/19 17:04 541-73-10.50 0.25 1
1,4-Dichlorobenzene <0.25 ug/L 12/29/19 17:04 106-46-70.50 0.25 1
Dichlorodifluoromethane <0.28 ug/L 12/29/19 17:04 75-71-80.50 0.28 1
1,1-Dichloroethane <0.24 ug/L 12/29/19 17:04 75-34-30.50 0.24 1
1,2-Dichloroethane <0.26 ug/L 12/29/19 17:04 107-06-20.50 0.26 1
1,1-Dichloroethene <0.22 ug/L 12/29/19 17:04 75-35-40.50 0.22 1
cis-1,2-Dichloroethene <0.21 ug/L 12/29/19 17:04 156-59-20.50 0.21 1
trans-1,2-Dichloroethene <0.26 ug/L 12/29/19 17:04 156-60-50.50 0.26 1
1,2-Dichloropropane <0.18 ug/L 12/29/19 17:04 78-87-50.50 0.18 1
1,3-Dichloropropane <0.34 ug/L 12/29/19 17:04 142-28-90.50 0.34 1
2,2-Dichloropropane <0.28 ug/L 12/29/19 17:04 594-20-70.50 0.28 1
1,1-Dichloropropene <0.35 ug/L 12/29/19 17:04 563-58-60.50 0.35 1
cis-1,3-Dichloropropene <0.36 ug/L 12/29/19 17:04 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.39 ug/L 12/29/19 17:04 10061-02-60.50 0.39 1
Diisopropyl ether <0.33 ug/L 12/29/19 17:04 108-20-30.50 0.33 1
Ethylbenzene <0.24 ug/L 12/29/19 17:04 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene <1.2 ug/L 12/29/19 17:04 87-68-32.0 1.2 1
2-Hexanone <0.60 ug/L 12/29/19 17:04 591-78-65.0 0.60 1
Isopropylbenzene (Cumene)<0.24 ug/L 12/29/19 17:04 98-82-80.50 0.24 1
Methylene Chloride <1.5 ug/L 12/29/19 17:04 75-09-22.0 1.5 1
Methyl-tert-butyl ether <0.44 ug/L 12/29/19 17:04 1634-04-40.50 0.44 1
Naphthalene <0.66 ug/L 12/29/19 17:04 91-20-32.0 0.66 1
n-Propylbenzene <0.24 ug/L 12/29/19 17:04 103-65-10.50 0.24 1
Styrene <0.26 ug/L 12/29/19 17:04 100-42-50.50 0.26 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92458367
Southland Oil
Sample:MW-2R Lab ID:92458367001 Collected:12/19/19 12:40 Received:12/20/19 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
1,1,1,2-Tetrachloroethane <0.42 ug/L 12/29/19 17:04 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane <0.19 ug/L 12/29/19 17:04 79-34-50.50 0.19 1
Tetrachloroethene <0.23 ug/L 12/29/19 17:04 127-18-40.50 0.23 1
Toluene <0.23 ug/L 12/29/19 17:04 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene <0.78 ug/L 12/29/19 17:04 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene <0.44 ug/L 12/29/19 17:04 120-82-12.0 0.44 1
1,1,1-Trichloroethane <0.28 ug/L 12/29/19 17:04 71-55-60.50 0.28 1
1,1,2-Trichloroethane <0.23 ug/L 12/29/19 17:04 79-00-50.50 0.23 1
Trichloroethene <0.23 ug/L 12/29/19 17:04 79-01-60.50 0.23 1
Trichlorofluoromethane <0.34 ug/L 12/29/19 17:04 75-69-41.0 0.34 1
1,2,3-Trichloropropane <0.27 ug/L 12/29/19 17:04 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene <0.19 ug/L 12/29/19 17:04 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene <0.23 ug/L 12/29/19 17:04 108-67-80.50 0.23 1
Vinyl chloride <0.41 ug/L 12/29/19 17:04 75-01-41.0 0.41 1
Xylene (Total)<0.50 ug/L 12/29/19 17:04 1330-20-71.0 0.50 1
m&p-Xylene <0.44 ug/L 12/29/19 17:04 179601-23-11.0 0.44 1
o-Xylene <0.24 ug/L 12/29/19 17:04 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)97 %12/29/19 17:04 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %12/29/19 17:04 460-00-470-130 1
Toluene-d8 (S)102 %12/29/19 17:04 2037-26-570-130 1
Sample:MW-5R Lab ID:92458367002 Collected:12/19/19 12:05 Received:12/20/19 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Benzene 118 ug/L 12/30/19 02:37 71-43-22.5 1.2 5
Bromobenzene <1.1 ug/L 12/30/19 02:37 108-86-12.5 1.1 5
Bromochloromethane <1.3 ug/L 12/30/19 02:37 74-97-52.5 1.3 5
Bromodichloromethane <0.92 ug/L 12/30/19 02:37 75-27-42.5 0.92 5
Bromoform <2.0 ug/L 12/30/19 02:37 75-25-22.5 2.0 5
Bromomethane <8.6 ug/L 12/30/19 02:37 74-83-925.0 8.6 5
2-Butanone (MEK)54.4 ug/L 12/30/19 02:37 78-93-325.0 18.0 5
n-Butylbenzene <1.8 ug/L 12/30/19 02:37 104-51-82.5 1.8 5
sec-Butylbenzene <1.2 ug/L 12/30/19 02:37 135-98-82.5 1.2 5
tert-Butylbenzene <1.2 ug/L 12/30/19 02:37 98-06-62.5 1.2 5
Carbon tetrachloride <1.2 ug/L 12/30/19 02:37 56-23-52.5 1.2 5
Chlorobenzene <1.1 ug/L 12/30/19 02:37 108-90-72.5 1.1 5
Chloroethane <2.9 ug/L 12/30/19 02:37 75-00-35.0 2.9 5
Chloroform <1.8 ug/L 12/30/19 02:37 67-66-32.5 1.8 5
Chloromethane <2.1 ug/L 12/30/19 02:37 74-87-35.0 2.1 5
2-Chlorotoluene <1.0 ug/L 12/30/19 02:37 95-49-82.5 1.0 5
4-Chlorotoluene <1.0 ug/L 12/30/19 02:37 106-43-42.5 1.0 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92458367
Southland Oil
Sample:MW-5R Lab ID:92458367002 Collected:12/19/19 12:05 Received:12/20/19 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
1,2-Dibromo-3-chloropropane <1.9 ug/L 12/30/19 02:37 96-12-85.0 1.9 5
Dibromochloromethane <2.0 ug/L 12/30/19 02:37 124-48-12.5 2.0 5
1,2-Dibromoethane (EDB)<1.2 ug/L 12/30/19 02:37 106-93-42.5 1.2 5
Dibromomethane <1.6 ug/L 12/30/19 02:37 74-95-32.5 1.6 5
1,2-Dichlorobenzene <1.2 ug/L 12/30/19 02:37 95-50-12.5 1.2 5
1,3-Dichlorobenzene <1.2 ug/L 12/30/19 02:37 541-73-12.5 1.2 5
1,4-Dichlorobenzene <1.2 ug/L 12/30/19 02:37 106-46-72.5 1.2 5
Dichlorodifluoromethane <1.4 ug/L 12/30/19 02:37 75-71-82.5 1.4 5
1,1-Dichloroethane <1.2 ug/L 12/30/19 02:37 75-34-32.5 1.2 5
1,2-Dichloroethane <1.3 ug/L 12/30/19 02:37 107-06-22.5 1.3 5
1,1-Dichloroethene <1.1 ug/L 12/30/19 02:37 75-35-42.5 1.1 5
cis-1,2-Dichloroethene <1.0 ug/L 12/30/19 02:37 156-59-22.5 1.0 5
trans-1,2-Dichloroethene <1.3 ug/L 12/30/19 02:37 156-60-52.5 1.3 5
1,2-Dichloropropane <0.92 ug/L 12/30/19 02:37 78-87-52.5 0.92 5
1,3-Dichloropropane <1.7 ug/L 12/30/19 02:37 142-28-92.5 1.7 5
2,2-Dichloropropane <1.4 ug/L 12/30/19 02:37 594-20-72.5 1.4 5
1,1-Dichloropropene <1.7 ug/L 12/30/19 02:37 563-58-62.5 1.7 5
cis-1,3-Dichloropropene <1.8 ug/L 12/30/19 02:37 10061-01-52.5 1.8 5
trans-1,3-Dichloropropene <2.0 ug/L 12/30/19 02:37 10061-02-62.5 2.0 5
Diisopropyl ether 10.1 ug/L 12/30/19 02:37 108-20-32.5 1.7 5
Ethylbenzene 16.8 ug/L 12/30/19 02:37 100-41-42.5 1.2 5
Hexachloro-1,3-butadiene <6.0 ug/L 12/30/19 02:37 87-68-310.0 6.0 5
2-Hexanone <3.0 ug/L 12/30/19 02:37 591-78-625.0 3.0 5
Isopropylbenzene (Cumene)<1.2 ug/L 12/30/19 02:37 98-82-82.5 1.2 5
Methylene Chloride <7.5 ug/L 12/30/19 02:37 75-09-210.0 7.5 5
Methyl-tert-butyl ether 761 ug/L 12/30/19 02:37 1634-04-42.5 2.2 5
Naphthalene 15.7 ug/L 12/30/19 02:37 91-20-310.0 3.3 5
n-Propylbenzene <1.2 ug/L 12/30/19 02:37 103-65-12.5 1.2 5
Styrene <1.3 ug/L 12/30/19 02:37 100-42-52.5 1.3 5
1,1,1,2-Tetrachloroethane <2.1 ug/L 12/30/19 02:37 630-20-62.5 2.1 5
1,1,2,2-Tetrachloroethane <0.96 ug/L 12/30/19 02:37 79-34-52.5 0.96 5
Tetrachloroethene 3.0 ug/L 12/30/19 02:37 127-18-42.5 1.2 5
Toluene <1.1 ug/L 12/30/19 02:37 108-88-32.5 1.1 5
1,2,3-Trichlorobenzene <3.9 ug/L 12/30/19 02:37 87-61-610.0 3.9 5
1,2,4-Trichlorobenzene <2.2 ug/L 12/30/19 02:37 120-82-110.0 2.2 5
1,1,1-Trichloroethane <1.4 ug/L 12/30/19 02:37 71-55-62.5 1.4 5
1,1,2-Trichloroethane <1.2 ug/L 12/30/19 02:37 79-00-52.5 1.2 5
Trichloroethene <1.2 ug/L 12/30/19 02:37 79-01-62.5 1.2 5
Trichlorofluoromethane <1.7 ug/L 12/30/19 02:37 75-69-45.0 1.7 5
1,2,3-Trichloropropane <1.4 ug/L 12/30/19 02:37 96-18-42.5 1.4 5
1,2,4-Trimethylbenzene 25.8 ug/L 12/30/19 02:37 95-63-62.5 0.96 5
1,3,5-Trimethylbenzene <1.1 ug/L 12/30/19 02:37 108-67-82.5 1.1 5
Vinyl chloride <2.0 ug/L 12/30/19 02:37 75-01-45.0 2.0 5
Xylene (Total)80.1 ug/L 12/30/19 02:37 1330-20-75.0 2.5 5
m&p-Xylene 40.4 ug/L 12/30/19 02:37 179601-23-15.0 2.2 5
o-Xylene 39.8 ug/L 12/30/19 02:37 95-47-62.5 1.2 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92458367
Southland Oil
Sample:MW-5R Lab ID:92458367002 Collected:12/19/19 12:05 Received:12/20/19 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Surrogates
1,2-Dichloroethane-d4 (S)96 %12/30/19 02:37 17060-07-070-130 5
4-Bromofluorobenzene (S)107 %12/30/19 02:37 460-00-470-130 5
Toluene-d8 (S)100 %12/30/19 02:37 2037-26-570-130 5
Sample:MW-6R Lab ID:92458367003 Collected:12/19/19 13:10 Received:12/20/19 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Benzene <0.24 ug/L 12/29/19 17:22 71-43-20.50 0.24 1
Bromobenzene <0.22 ug/L 12/29/19 17:22 108-86-10.50 0.22 1
Bromochloromethane <0.26 ug/L 12/29/19 17:22 74-97-50.50 0.26 1
Bromodichloromethane <0.18 ug/L 12/29/19 17:22 75-27-40.50 0.18 1
Bromoform <0.40 ug/L 12/29/19 17:22 75-25-20.50 0.40 1
Bromomethane <1.7 ug/L 12/29/19 17:22 74-83-95.0 1.7 1
2-Butanone (MEK)<3.6 ug/L 12/29/19 17:22 78-93-35.0 3.6 1
n-Butylbenzene <0.35 ug/L 12/29/19 17:22 104-51-80.50 0.35 1
sec-Butylbenzene <0.25 ug/L 12/29/19 17:22 135-98-80.50 0.25 1
tert-Butylbenzene <0.25 ug/L 12/29/19 17:22 98-06-60.50 0.25 1
Carbon tetrachloride <0.23 ug/L 12/29/19 17:22 56-23-50.50 0.23 1
Chlorobenzene <0.22 ug/L 12/29/19 17:22 108-90-70.50 0.22 1
Chloroethane <0.58 ug/L 12/29/19 17:22 75-00-31.0 0.58 1
Chloroform <0.35 ug/L 12/29/19 17:22 67-66-30.50 0.35 1
Chloromethane <0.42 ug/L 12/29/19 17:22 74-87-31.0 0.42 1
2-Chlorotoluene <0.21 ug/L 12/29/19 17:22 95-49-80.50 0.21 1
4-Chlorotoluene <0.21 ug/L 12/29/19 17:22 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane <0.38 ug/L 12/29/19 17:22 96-12-81.0 0.38 1
Dibromochloromethane <0.40 ug/L 12/29/19 17:22 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)<0.23 ug/L 12/29/19 17:22 106-93-40.50 0.23 1
Dibromomethane <0.31 ug/L 12/29/19 17:22 74-95-30.50 0.31 1
1,2-Dichlorobenzene <0.24 ug/L 12/29/19 17:22 95-50-10.50 0.24 1
1,3-Dichlorobenzene <0.25 ug/L 12/29/19 17:22 541-73-10.50 0.25 1
1,4-Dichlorobenzene <0.25 ug/L 12/29/19 17:22 106-46-70.50 0.25 1
Dichlorodifluoromethane <0.28 ug/L 12/29/19 17:22 75-71-80.50 0.28 1
1,1-Dichloroethane <0.24 ug/L 12/29/19 17:22 75-34-30.50 0.24 1
1,2-Dichloroethane <0.26 ug/L 12/29/19 17:22 107-06-20.50 0.26 1
1,1-Dichloroethene <0.22 ug/L 12/29/19 17:22 75-35-40.50 0.22 1
cis-1,2-Dichloroethene <0.21 ug/L 12/29/19 17:22 156-59-20.50 0.21 1
trans-1,2-Dichloroethene <0.26 ug/L 12/29/19 17:22 156-60-50.50 0.26 1
1,2-Dichloropropane <0.18 ug/L 12/29/19 17:22 78-87-50.50 0.18 1
1,3-Dichloropropane <0.34 ug/L 12/29/19 17:22 142-28-90.50 0.34 1
2,2-Dichloropropane <0.28 ug/L 12/29/19 17:22 594-20-70.50 0.28 1
1,1-Dichloropropene <0.35 ug/L 12/29/19 17:22 563-58-60.50 0.35 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92458367
Southland Oil
Sample:MW-6R Lab ID:92458367003 Collected:12/19/19 13:10 Received:12/20/19 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
cis-1,3-Dichloropropene <0.36 ug/L 12/29/19 17:22 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.39 ug/L 12/29/19 17:22 10061-02-60.50 0.39 1
Diisopropyl ether <0.33 ug/L 12/29/19 17:22 108-20-30.50 0.33 1
Ethylbenzene <0.24 ug/L 12/29/19 17:22 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene <1.2 ug/L 12/29/19 17:22 87-68-32.0 1.2 1
2-Hexanone <0.60 ug/L 12/29/19 17:22 591-78-65.0 0.60 1
Isopropylbenzene (Cumene)<0.24 ug/L 12/29/19 17:22 98-82-80.50 0.24 1
Methylene Chloride <1.5 ug/L 12/29/19 17:22 75-09-22.0 1.5 1
Methyl-tert-butyl ether <0.44 ug/L 12/29/19 17:22 1634-04-40.50 0.44 1
Naphthalene <0.66 ug/L 12/29/19 17:22 91-20-32.0 0.66 1
n-Propylbenzene <0.24 ug/L 12/29/19 17:22 103-65-10.50 0.24 1
Styrene <0.26 ug/L 12/29/19 17:22 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane <0.42 ug/L 12/29/19 17:22 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane <0.19 ug/L 12/29/19 17:22 79-34-50.50 0.19 1
Tetrachloroethene <0.23 ug/L 12/29/19 17:22 127-18-40.50 0.23 1
Toluene <0.23 ug/L 12/29/19 17:22 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene <0.78 ug/L 12/29/19 17:22 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene <0.44 ug/L 12/29/19 17:22 120-82-12.0 0.44 1
1,1,1-Trichloroethane <0.28 ug/L 12/29/19 17:22 71-55-60.50 0.28 1
1,1,2-Trichloroethane <0.23 ug/L 12/29/19 17:22 79-00-50.50 0.23 1
Trichloroethene <0.23 ug/L 12/29/19 17:22 79-01-60.50 0.23 1
Trichlorofluoromethane <0.34 ug/L 12/29/19 17:22 75-69-41.0 0.34 1
1,2,3-Trichloropropane <0.27 ug/L 12/29/19 17:22 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene <0.19 ug/L 12/29/19 17:22 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene <0.23 ug/L 12/29/19 17:22 108-67-80.50 0.23 1
Vinyl chloride <0.41 ug/L 12/29/19 17:22 75-01-41.0 0.41 1
Xylene (Total)<0.50 ug/L 12/29/19 17:22 1330-20-71.0 0.50 1
m&p-Xylene <0.44 ug/L 12/29/19 17:22 179601-23-11.0 0.44 1
o-Xylene <0.24 ug/L 12/29/19 17:22 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %12/29/19 17:22 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %12/29/19 17:22 460-00-470-130 1
Toluene-d8 (S)101 %12/29/19 17:22 2037-26-570-130 1
Sample:MW-7R Lab ID:92458367004 Collected:12/19/19 12:20 Received:12/20/19 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Benzene 463 ug/L 12/30/19 02:55 71-43-22.5 1.2 5
Bromobenzene <1.1 ug/L 12/30/19 02:55 108-86-12.5 1.1 5
Bromochloromethane <1.3 ug/L 12/30/19 02:55 74-97-52.5 1.3 5
Bromodichloromethane <0.92 ug/L 12/30/19 02:55 75-27-42.5 0.92 5
Bromoform <2.0 ug/L 12/30/19 02:55 75-25-22.5 2.0 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92458367
Southland Oil
Sample:MW-7R Lab ID:92458367004 Collected:12/19/19 12:20 Received:12/20/19 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Bromomethane <8.6 ug/L 12/30/19 02:55 74-83-925.0 8.6 5
2-Butanone (MEK)182 ug/L 12/30/19 02:55 78-93-325.0 18.0 5
n-Butylbenzene <1.8 ug/L 12/30/19 02:55 104-51-82.5 1.8 5
sec-Butylbenzene <1.2 ug/L 12/30/19 02:55 135-98-82.5 1.2 5
tert-Butylbenzene <1.2 ug/L 12/30/19 02:55 98-06-62.5 1.2 5
Carbon tetrachloride <1.2 ug/L 12/30/19 02:55 56-23-52.5 1.2 5
Chlorobenzene <1.1 ug/L 12/30/19 02:55 108-90-72.5 1.1 5
Chloroethane <2.9 ug/L 12/30/19 02:55 75-00-35.0 2.9 5
Chloroform <1.8 ug/L 12/30/19 02:55 67-66-32.5 1.8 5
Chloromethane <2.1 ug/L 12/30/19 02:55 74-87-35.0 2.1 5
2-Chlorotoluene <1.0 ug/L 12/30/19 02:55 95-49-82.5 1.0 5
4-Chlorotoluene <1.0 ug/L 12/30/19 02:55 106-43-42.5 1.0 5
1,2-Dibromo-3-chloropropane <1.9 ug/L 12/30/19 02:55 96-12-85.0 1.9 5
Dibromochloromethane <2.0 ug/L 12/30/19 02:55 124-48-12.5 2.0 5
1,2-Dibromoethane (EDB)<1.2 ug/L 12/30/19 02:55 106-93-42.5 1.2 5
Dibromomethane <1.6 ug/L 12/30/19 02:55 74-95-32.5 1.6 5
1,2-Dichlorobenzene <1.2 ug/L 12/30/19 02:55 95-50-12.5 1.2 5
1,3-Dichlorobenzene <1.2 ug/L 12/30/19 02:55 541-73-12.5 1.2 5
1,4-Dichlorobenzene <1.2 ug/L 12/30/19 02:55 106-46-72.5 1.2 5
Dichlorodifluoromethane <1.4 ug/L 12/30/19 02:55 75-71-82.5 1.4 5
1,1-Dichloroethane <1.2 ug/L 12/30/19 02:55 75-34-32.5 1.2 5
1,2-Dichloroethane <1.3 ug/L 12/30/19 02:55 107-06-22.5 1.3 5
1,1-Dichloroethene <1.1 ug/L 12/30/19 02:55 75-35-42.5 1.1 5
cis-1,2-Dichloroethene 3.2 ug/L 12/30/19 02:55 156-59-22.5 1.0 5
trans-1,2-Dichloroethene <1.3 ug/L 12/30/19 02:55 156-60-52.5 1.3 5
1,2-Dichloropropane <0.92 ug/L 12/30/19 02:55 78-87-52.5 0.92 5
1,3-Dichloropropane <1.7 ug/L 12/30/19 02:55 142-28-92.5 1.7 5
2,2-Dichloropropane <1.4 ug/L 12/30/19 02:55 594-20-72.5 1.4 5
1,1-Dichloropropene <1.7 ug/L 12/30/19 02:55 563-58-62.5 1.7 5
cis-1,3-Dichloropropene <1.8 ug/L 12/30/19 02:55 10061-01-52.5 1.8 5
trans-1,3-Dichloropropene <2.0 ug/L 12/30/19 02:55 10061-02-62.5 2.0 5
Diisopropyl ether 4.0 ug/L 12/30/19 02:55 108-20-32.5 1.7 5
Ethylbenzene 273 ug/L 12/30/19 02:55 100-41-42.5 1.2 5
Hexachloro-1,3-butadiene <6.0 ug/L 12/30/19 02:55 87-68-310.0 6.0 5
2-Hexanone 311 ug/L 12/30/19 02:55 591-78-625.0 3.0 5
Isopropylbenzene (Cumene)15.7 ug/L 12/30/19 02:55 98-82-82.5 1.2 5
Methylene Chloride <7.5 ug/L 12/30/19 02:55 75-09-210.0 7.5 5
Methyl-tert-butyl ether 510 ug/L 12/30/19 02:55 1634-04-42.5 2.2 5
Naphthalene 125 ug/L 12/30/19 02:55 91-20-310.0 3.3 5
n-Propylbenzene 31.8 ug/L 12/30/19 02:55 103-65-12.5 1.2 5
Styrene <1.3 ug/L 12/30/19 02:55 100-42-52.5 1.3 5
1,1,1,2-Tetrachloroethane <2.1 ug/L 12/30/19 02:55 630-20-62.5 2.1 5
1,1,2,2-Tetrachloroethane <0.96 ug/L 12/30/19 02:55 79-34-52.5 0.96 5
Tetrachloroethene 15.9 ug/L 12/30/19 02:55 127-18-42.5 1.2 5
Toluene 961 ug/L 12/30/19 02:55 108-88-32.5 1.1 5
1,2,3-Trichlorobenzene <3.9 ug/L 12/30/19 02:55 87-61-610.0 3.9 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92458367
Southland Oil
Sample:MW-7R Lab ID:92458367004 Collected:12/19/19 12:20 Received:12/20/19 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
1,2,4-Trichlorobenzene <2.2 ug/L 12/30/19 02:55 120-82-110.0 2.2 5
1,1,1-Trichloroethane <1.4 ug/L 12/30/19 02:55 71-55-62.5 1.4 5
1,1,2-Trichloroethane <1.2 ug/L 12/30/19 02:55 79-00-52.5 1.2 5
Trichloroethene 3.2 ug/L 12/30/19 02:55 79-01-62.5 1.2 5
Trichlorofluoromethane <1.7 ug/L 12/30/19 02:55 75-69-45.0 1.7 5
1,2,3-Trichloropropane <1.4 ug/L 12/30/19 02:55 96-18-42.5 1.4 5
1,2,4-Trimethylbenzene 314 ug/L 12/30/19 02:55 95-63-62.5 0.96 5
1,3,5-Trimethylbenzene 51.5 ug/L 12/30/19 02:55 108-67-82.5 1.1 5
Vinyl chloride <2.0 ug/L 12/30/19 02:55 75-01-45.0 2.0 5
Xylene (Total)1710 ug/L 12/30/19 02:55 1330-20-75.0 2.5 5
m&p-Xylene 951 ug/L 12/30/19 02:55 179601-23-15.0 2.2 5
o-Xylene 757 ug/L 12/30/19 02:55 95-47-62.5 1.2 5
Surrogates
1,2-Dichloroethane-d4 (S)105 %12/30/19 02:55 17060-07-070-130 5
4-Bromofluorobenzene (S)115 %12/30/19 02:55 460-00-470-130 5
Toluene-d8 (S)99 %12/30/19 02:55 2037-26-570-130 5
Sample:Field Blank Lab ID:92458367005 Collected:12/19/19 13:30 Received:12/20/19 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Benzene <0.24 ug/L 12/29/19 16:47 71-43-20.50 0.24 1
Bromobenzene <0.22 ug/L 12/29/19 16:47 108-86-10.50 0.22 1
Bromochloromethane <0.26 ug/L 12/29/19 16:47 74-97-50.50 0.26 1
Bromodichloromethane <0.18 ug/L 12/29/19 16:47 75-27-40.50 0.18 1
Bromoform <0.40 ug/L 12/29/19 16:47 75-25-20.50 0.40 1
Bromomethane <1.7 ug/L 12/29/19 16:47 74-83-95.0 1.7 1
2-Butanone (MEK)<3.6 ug/L 12/29/19 16:47 78-93-35.0 3.6 1
n-Butylbenzene <0.35 ug/L 12/29/19 16:47 104-51-80.50 0.35 1
sec-Butylbenzene <0.25 ug/L 12/29/19 16:47 135-98-80.50 0.25 1
tert-Butylbenzene <0.25 ug/L 12/29/19 16:47 98-06-60.50 0.25 1
Carbon tetrachloride <0.23 ug/L 12/29/19 16:47 56-23-50.50 0.23 1
Chlorobenzene <0.22 ug/L 12/29/19 16:47 108-90-70.50 0.22 1
Chloroethane <0.58 ug/L 12/29/19 16:47 75-00-31.0 0.58 1
Chloroform <0.35 ug/L 12/29/19 16:47 67-66-30.50 0.35 1
Chloromethane <0.42 ug/L 12/29/19 16:47 74-87-31.0 0.42 1
2-Chlorotoluene <0.21 ug/L 12/29/19 16:47 95-49-80.50 0.21 1
4-Chlorotoluene <0.21 ug/L 12/29/19 16:47 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane <0.38 ug/L 12/29/19 16:47 96-12-81.0 0.38 1
Dibromochloromethane <0.40 ug/L 12/29/19 16:47 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)<0.23 ug/L 12/29/19 16:47 106-93-40.50 0.23 1
Dibromomethane <0.31 ug/L 12/29/19 16:47 74-95-30.50 0.31 1
1,2-Dichlorobenzene <0.24 ug/L 12/29/19 16:47 95-50-10.50 0.24 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
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Page 11 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92458367
Southland Oil
Sample:Field Blank Lab ID:92458367005 Collected:12/19/19 13:30 Received:12/20/19 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
1,3-Dichlorobenzene <0.25 ug/L 12/29/19 16:47 541-73-10.50 0.25 1
1,4-Dichlorobenzene <0.25 ug/L 12/29/19 16:47 106-46-70.50 0.25 1
Dichlorodifluoromethane <0.28 ug/L 12/29/19 16:47 75-71-80.50 0.28 1
1,1-Dichloroethane <0.24 ug/L 12/29/19 16:47 75-34-30.50 0.24 1
1,2-Dichloroethane <0.26 ug/L 12/29/19 16:47 107-06-20.50 0.26 1
1,1-Dichloroethene <0.22 ug/L 12/29/19 16:47 75-35-40.50 0.22 1
cis-1,2-Dichloroethene <0.21 ug/L 12/29/19 16:47 156-59-20.50 0.21 1
trans-1,2-Dichloroethene <0.26 ug/L 12/29/19 16:47 156-60-50.50 0.26 1
1,2-Dichloropropane <0.18 ug/L 12/29/19 16:47 78-87-50.50 0.18 1
1,3-Dichloropropane <0.34 ug/L 12/29/19 16:47 142-28-90.50 0.34 1
2,2-Dichloropropane <0.28 ug/L 12/29/19 16:47 594-20-70.50 0.28 1
1,1-Dichloropropene <0.35 ug/L 12/29/19 16:47 563-58-60.50 0.35 1
cis-1,3-Dichloropropene <0.36 ug/L 12/29/19 16:47 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.39 ug/L 12/29/19 16:47 10061-02-60.50 0.39 1
Diisopropyl ether <0.33 ug/L 12/29/19 16:47 108-20-30.50 0.33 1
Ethylbenzene <0.24 ug/L 12/29/19 16:47 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene <1.2 ug/L 12/29/19 16:47 87-68-32.0 1.2 1
2-Hexanone <0.60 ug/L 12/29/19 16:47 591-78-65.0 0.60 1
Isopropylbenzene (Cumene)<0.24 ug/L 12/29/19 16:47 98-82-80.50 0.24 1
Methylene Chloride <1.5 ug/L 12/29/19 16:47 75-09-22.0 1.5 1
Methyl-tert-butyl ether <0.44 ug/L 12/29/19 16:47 1634-04-40.50 0.44 1
Naphthalene <0.66 ug/L 12/29/19 16:47 91-20-32.0 0.66 1
n-Propylbenzene <0.24 ug/L 12/29/19 16:47 103-65-10.50 0.24 1
Styrene <0.26 ug/L 12/29/19 16:47 100-42-50.50 0.26 1
1,1,1,2-Tetrachloroethane <0.42 ug/L 12/29/19 16:47 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane <0.19 ug/L 12/29/19 16:47 79-34-50.50 0.19 1
Tetrachloroethene <0.23 ug/L 12/29/19 16:47 127-18-40.50 0.23 1
Toluene <0.23 ug/L 12/29/19 16:47 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene <0.78 ug/L 12/29/19 16:47 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene <0.44 ug/L 12/29/19 16:47 120-82-12.0 0.44 1
1,1,1-Trichloroethane <0.28 ug/L 12/29/19 16:47 71-55-60.50 0.28 1
1,1,2-Trichloroethane <0.23 ug/L 12/29/19 16:47 79-00-50.50 0.23 1
Trichloroethene <0.23 ug/L 12/29/19 16:47 79-01-60.50 0.23 1
Trichlorofluoromethane <0.34 ug/L 12/29/19 16:47 75-69-41.0 0.34 1
1,2,3-Trichloropropane <0.27 ug/L 12/29/19 16:47 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene <0.19 ug/L 12/29/19 16:47 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene <0.23 ug/L 12/29/19 16:47 108-67-80.50 0.23 1
Vinyl chloride <0.41 ug/L 12/29/19 16:47 75-01-41.0 0.41 1
Xylene (Total)<0.50 ug/L 12/29/19 16:47 1330-20-71.0 0.50 1
m&p-Xylene <0.44 ug/L 12/29/19 16:47 179601-23-11.0 0.44 1
o-Xylene <0.24 ug/L 12/29/19 16:47 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)92 %12/29/19 16:47 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %12/29/19 16:47 460-00-470-130 1
Toluene-d8 (S)101 %12/29/19 16:47 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
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Page 12 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92458367
Southland Oil
Sample:MW-8 Lab ID:92458367006 Collected:12/19/19 13:25 Received:12/20/19 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
Benzene <0.24 ug/L 12/29/19 17:40 71-43-20.50 0.24 1
Bromobenzene <0.22 ug/L 12/29/19 17:40 108-86-10.50 0.22 1
Bromochloromethane <0.26 ug/L 12/29/19 17:40 74-97-50.50 0.26 1
Bromodichloromethane <0.18 ug/L 12/29/19 17:40 75-27-40.50 0.18 1
Bromoform <0.40 ug/L 12/29/19 17:40 75-25-20.50 0.40 1
Bromomethane <1.7 ug/L 12/29/19 17:40 74-83-95.0 1.7 1
2-Butanone (MEK)<3.6 ug/L 12/29/19 17:40 78-93-35.0 3.6 1
n-Butylbenzene <0.35 ug/L 12/29/19 17:40 104-51-80.50 0.35 1
sec-Butylbenzene <0.25 ug/L 12/29/19 17:40 135-98-80.50 0.25 1
tert-Butylbenzene <0.25 ug/L 12/29/19 17:40 98-06-60.50 0.25 1
Carbon tetrachloride <0.23 ug/L 12/29/19 17:40 56-23-50.50 0.23 1
Chlorobenzene <0.22 ug/L 12/29/19 17:40 108-90-70.50 0.22 1
Chloroethane <0.58 ug/L 12/29/19 17:40 75-00-31.0 0.58 1
Chloroform <0.35 ug/L 12/29/19 17:40 67-66-30.50 0.35 1
Chloromethane <0.42 ug/L 12/29/19 17:40 74-87-31.0 0.42 1
2-Chlorotoluene <0.21 ug/L 12/29/19 17:40 95-49-80.50 0.21 1
4-Chlorotoluene <0.21 ug/L 12/29/19 17:40 106-43-40.50 0.21 1
1,2-Dibromo-3-chloropropane <0.38 ug/L 12/29/19 17:40 96-12-81.0 0.38 1
Dibromochloromethane <0.40 ug/L 12/29/19 17:40 124-48-10.50 0.40 1
1,2-Dibromoethane (EDB)<0.23 ug/L 12/29/19 17:40 106-93-40.50 0.23 1
Dibromomethane <0.31 ug/L 12/29/19 17:40 74-95-30.50 0.31 1
1,2-Dichlorobenzene <0.24 ug/L 12/29/19 17:40 95-50-10.50 0.24 1
1,3-Dichlorobenzene <0.25 ug/L 12/29/19 17:40 541-73-10.50 0.25 1
1,4-Dichlorobenzene <0.25 ug/L 12/29/19 17:40 106-46-70.50 0.25 1
Dichlorodifluoromethane <0.28 ug/L 12/29/19 17:40 75-71-80.50 0.28 1
1,1-Dichloroethane <0.24 ug/L 12/29/19 17:40 75-34-30.50 0.24 1
1,2-Dichloroethane <0.26 ug/L 12/29/19 17:40 107-06-20.50 0.26 1
1,1-Dichloroethene <0.22 ug/L 12/29/19 17:40 75-35-40.50 0.22 1
cis-1,2-Dichloroethene <0.21 ug/L 12/29/19 17:40 156-59-20.50 0.21 1
trans-1,2-Dichloroethene <0.26 ug/L 12/29/19 17:40 156-60-50.50 0.26 1
1,2-Dichloropropane <0.18 ug/L 12/29/19 17:40 78-87-50.50 0.18 1
1,3-Dichloropropane <0.34 ug/L 12/29/19 17:40 142-28-90.50 0.34 1
2,2-Dichloropropane <0.28 ug/L 12/29/19 17:40 594-20-70.50 0.28 1
1,1-Dichloropropene <0.35 ug/L 12/29/19 17:40 563-58-60.50 0.35 1
cis-1,3-Dichloropropene <0.36 ug/L 12/29/19 17:40 10061-01-50.50 0.36 1
trans-1,3-Dichloropropene <0.39 ug/L 12/29/19 17:40 10061-02-60.50 0.39 1
Diisopropyl ether <0.33 ug/L 12/29/19 17:40 108-20-30.50 0.33 1
Ethylbenzene <0.24 ug/L 12/29/19 17:40 100-41-40.50 0.24 1
Hexachloro-1,3-butadiene <1.2 ug/L 12/29/19 17:40 87-68-32.0 1.2 1
2-Hexanone <0.60 ug/L 12/29/19 17:40 591-78-65.0 0.60 1
Isopropylbenzene (Cumene)<0.24 ug/L 12/29/19 17:40 98-82-80.50 0.24 1
Methylene Chloride <1.5 ug/L 12/29/19 17:40 75-09-22.0 1.5 1
Methyl-tert-butyl ether <0.44 ug/L 12/29/19 17:40 1634-04-40.50 0.44 1
Naphthalene <0.66 ug/L 12/29/19 17:40 91-20-32.0 0.66 1
n-Propylbenzene <0.24 ug/L 12/29/19 17:40 103-65-10.50 0.24 1
Styrene <0.26 ug/L 12/29/19 17:40 100-42-50.50 0.26 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
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Huntersville, NC 28078
[phone]
Page 13 of 30
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92458367
Southland Oil
Sample:MW-8 Lab ID:92458367006 Collected:12/19/19 13:25 Received:12/20/19 12:10 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLPQL
Analytical Method: SM 6200B6200B MSV
1,1,1,2-Tetrachloroethane <0.42 ug/L 12/29/19 17:40 630-20-60.50 0.42 1
1,1,2,2-Tetrachloroethane <0.19 ug/L 12/29/19 17:40 79-34-50.50 0.19 1
Tetrachloroethene <0.23 ug/L 12/29/19 17:40 127-18-40.50 0.23 1
Toluene <0.23 ug/L 12/29/19 17:40 108-88-30.50 0.23 1
1,2,3-Trichlorobenzene <0.78 ug/L 12/29/19 17:40 87-61-62.0 0.78 1
1,2,4-Trichlorobenzene <0.44 ug/L 12/29/19 17:40 120-82-12.0 0.44 1
1,1,1-Trichloroethane <0.28 ug/L 12/29/19 17:40 71-55-60.50 0.28 1
1,1,2-Trichloroethane <0.23 ug/L 12/29/19 17:40 79-00-50.50 0.23 1
Trichloroethene <0.23 ug/L 12/29/19 17:40 79-01-60.50 0.23 1
Trichlorofluoromethane <0.34 ug/L 12/29/19 17:40 75-69-41.0 0.34 1
1,2,3-Trichloropropane <0.27 ug/L 12/29/19 17:40 96-18-40.50 0.27 1
1,2,4-Trimethylbenzene <0.19 ug/L 12/29/19 17:40 95-63-60.50 0.19 1
1,3,5-Trimethylbenzene <0.23 ug/L 12/29/19 17:40 108-67-80.50 0.23 1
Vinyl chloride <0.41 ug/L 12/29/19 17:40 75-01-41.0 0.41 1
Xylene (Total)<0.50 ug/L 12/29/19 17:40 1330-20-71.0 0.50 1
m&p-Xylene <0.44 ug/L 12/29/19 17:40 179601-23-11.0 0.44 1
o-Xylene <0.24 ug/L 12/29/19 17:40 95-47-60.50 0.24 1
Surrogates
1,2-Dichloroethane-d4 (S)95 %12/29/19 17:40 17060-07-070-130 1
4-Bromofluorobenzene (S)99 %12/29/19 17:40 460-00-470-130 1
Toluene-d8 (S)102 %12/29/19 17:40 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
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Page 14 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92458367
Southland Oil
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
517123
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92458367001, 92458367003, 92458367005, 92458367006
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2769513
Associated Lab Samples:92458367001, 92458367003, 92458367005, 92458367006
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.42 0.50 12/29/19 15:530.42
1,1,1-Trichloroethane ug/L <0.28 0.50 12/29/19 15:530.28
1,1,2,2-Tetrachloroethane ug/L <0.19 0.50 12/29/19 15:530.19
1,1,2-Trichloroethane ug/L <0.23 0.50 12/29/19 15:530.23
1,1-Dichloroethane ug/L <0.24 0.50 12/29/19 15:530.24
1,1-Dichloroethene ug/L <0.22 0.50 12/29/19 15:530.22
1,1-Dichloropropene ug/L <0.35 0.50 12/29/19 15:530.35
1,2,3-Trichlorobenzene ug/L <0.78 2.0 12/29/19 15:530.78
1,2,3-Trichloropropane ug/L <0.27 0.50 12/29/19 15:530.27
1,2,4-Trichlorobenzene ug/L <0.44 2.0 12/29/19 15:530.44
1,2,4-Trimethylbenzene ug/L <0.19 0.50 12/29/19 15:530.19
1,2-Dibromo-3-chloropropane ug/L <0.38 1.0 12/29/19 15:530.38
1,2-Dibromoethane (EDB)ug/L <0.23 0.50 12/29/19 15:530.23
1,2-Dichlorobenzene ug/L <0.24 0.50 12/29/19 15:530.24
1,2-Dichloroethane ug/L <0.26 0.50 12/29/19 15:530.26
1,2-Dichloropropane ug/L <0.18 0.50 12/29/19 15:530.18
1,3,5-Trimethylbenzene ug/L <0.23 0.50 12/29/19 15:530.23
1,3-Dichlorobenzene ug/L <0.25 0.50 12/29/19 15:530.25
1,3-Dichloropropane ug/L <0.34 0.50 12/29/19 15:530.34
1,4-Dichlorobenzene ug/L <0.25 0.50 12/29/19 15:530.25
2,2-Dichloropropane ug/L <0.28 0.50 12/29/19 15:530.28
2-Butanone (MEK)ug/L <3.6 5.0 12/29/19 15:533.6
2-Chlorotoluene ug/L <0.21 0.50 12/29/19 15:530.21
2-Hexanone ug/L <0.60 5.0 12/29/19 15:530.60
4-Chlorotoluene ug/L <0.21 0.50 12/29/19 15:530.21
Benzene ug/L <0.24 0.50 12/29/19 15:530.24
Bromobenzene ug/L <0.22 0.50 12/29/19 15:530.22
Bromochloromethane ug/L <0.26 0.50 12/29/19 15:530.26
Bromodichloromethane ug/L <0.18 0.50 12/29/19 15:530.18
Bromoform ug/L <0.40 0.50 12/29/19 15:530.40
Bromomethane ug/L <1.7 5.0 12/29/19 15:531.7
Carbon tetrachloride ug/L <0.23 0.50 12/29/19 15:530.23
Chlorobenzene ug/L <0.22 0.50 12/29/19 15:530.22
Chloroethane ug/L <0.58 1.0 12/29/19 15:530.58
Chloroform ug/L <0.35 0.50 12/29/19 15:530.35
Chloromethane ug/L <0.42 1.0 12/29/19 15:530.42
cis-1,2-Dichloroethene ug/L <0.21 0.50 12/29/19 15:530.21
cis-1,3-Dichloropropene ug/L <0.36 0.50 12/29/19 15:530.36
Dibromochloromethane ug/L <0.40 0.50 12/29/19 15:530.40
Dibromomethane ug/L <0.31 0.50 12/29/19 15:530.31
Dichlorodifluoromethane ug/L <0.28 0.50 12/29/19 15:530.28
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
Pace Analytical Services, LLC
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Page 15 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92458367
Southland Oil
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2769513
Associated Lab Samples:92458367001, 92458367003, 92458367005, 92458367006
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L <0.33 0.50 12/29/19 15:530.33
Ethylbenzene ug/L <0.24 0.50 12/29/19 15:530.24
Hexachloro-1,3-butadiene ug/L <1.2 2.0 12/29/19 15:531.2
Isopropylbenzene (Cumene)ug/L <0.24 0.50 12/29/19 15:530.24
m&p-Xylene ug/L <0.44 1.0 12/29/19 15:530.44
Methyl-tert-butyl ether ug/L <0.44 0.50 12/29/19 15:530.44
Methylene Chloride ug/L <1.5 2.0 12/29/19 15:531.5
n-Butylbenzene ug/L <0.35 0.50 12/29/19 15:530.35
n-Propylbenzene ug/L <0.24 0.50 12/29/19 15:530.24
Naphthalene ug/L <0.66 2.0 12/29/19 15:530.66
o-Xylene ug/L <0.24 0.50 12/29/19 15:530.24
sec-Butylbenzene ug/L <0.25 0.50 12/29/19 15:530.25
Styrene ug/L <0.26 0.50 12/29/19 15:530.26
tert-Butylbenzene ug/L <0.25 0.50 12/29/19 15:530.25
Tetrachloroethene ug/L <0.23 0.50 12/29/19 15:530.23
Toluene ug/L <0.23 0.50 12/29/19 15:530.23
trans-1,2-Dichloroethene ug/L <0.26 0.50 12/29/19 15:530.26
trans-1,3-Dichloropropene ug/L <0.39 0.50 12/29/19 15:530.39
Trichloroethene ug/L <0.23 0.50 12/29/19 15:530.23
Trichlorofluoromethane ug/L <0.34 1.0 12/29/19 15:530.34
Vinyl chloride ug/L <0.41 1.0 12/29/19 15:530.41
Xylene (Total)ug/L <0.50 1.0 12/29/19 15:530.50
1,2-Dichloroethane-d4 (S)%97 70-130 12/29/19 15:53
4-Bromofluorobenzene (S)%97 70-130 12/29/19 15:53
Toluene-d8 (S)%103 70-130 12/29/19 15:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2769514LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 50.850 102 60-140
1,1,1-Trichloroethane ug/L 50.250 100 60-140
1,1,2,2-Tetrachloroethane ug/L 48.750 97 60-140
1,1,2-Trichloroethane ug/L 49.550 99 60-140
1,1-Dichloroethane ug/L 47.250 94 60-140
1,1-Dichloroethene ug/L 48.750 97 60-140
1,1-Dichloropropene ug/L 52.950 106 60-140
1,2,3-Trichlorobenzene ug/L 50.250 100 60-140
1,2,3-Trichloropropane ug/L 48.250 96 60-140
1,2,4-Trichlorobenzene ug/L 49.950 100 60-140
1,2,4-Trimethylbenzene ug/L 49.350 99 60-140
1,2-Dibromo-3-chloropropane ug/L 51.050 102 60-140
1,2-Dibromoethane (EDB)ug/L 50.850 102 60-140
1,2-Dichlorobenzene ug/L 49.550 99 60-140
1,2-Dichloroethane ug/L 45.450 91 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
Pace Analytical Services, LLC
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[phone]
Page 16 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92458367
Southland Oil
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2769514LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloropropane ug/L 49.350 99 60-140
1,3,5-Trimethylbenzene ug/L 48.950 98 60-140
1,3-Dichlorobenzene ug/L 49.050 98 60-140
1,3-Dichloropropane ug/L 50.650 101 60-140
1,4-Dichlorobenzene ug/L 49.350 99 60-140
2,2-Dichloropropane ug/L 55.350 111 60-140
2-Butanone (MEK)ug/L 98.6100 99 60-140
2-Chlorotoluene ug/L 47.950 96 60-140
2-Hexanone ug/L 102100 102 60-140
4-Chlorotoluene ug/L 48.750 97 60-140
Benzene ug/L 49.250 98 60-140
Bromobenzene ug/L 49.350 99 60-140
Bromochloromethane ug/L 48.750 97 60-140
Bromodichloromethane ug/L 50.950 102 60-140
Bromoform ug/L 52.350 105 60-140
Bromomethane ug/L 61.250 122 60-140
Carbon tetrachloride ug/L 51.450 103 60-140
Chlorobenzene ug/L 49.050 98 60-140
Chloroethane ug/L 35.150 70 60-140
Chloroform ug/L 46.750 93 60-140
Chloromethane ug/L 33.550 67 60-140
cis-1,2-Dichloroethene ug/L 47.050 94 60-140
cis-1,3-Dichloropropene ug/L 53.450 107 60-140
Dibromochloromethane ug/L 51.850 104 60-140
Dibromomethane ug/L 47.750 95 60-140
Dichlorodifluoromethane ug/L 41.650 83 60-140
Diisopropyl ether ug/L 47.550 95 60-140
Ethylbenzene ug/L 48.150 96 60-140
Hexachloro-1,3-butadiene ug/L 50.250 100 60-140
Isopropylbenzene (Cumene)ug/L 49.250 98 60-140
m&p-Xylene ug/L 97.4100 97 60-140
Methyl-tert-butyl ether ug/L 50.150 100 60-140
Methylene Chloride ug/L 44.550 89 60-140
n-Butylbenzene ug/L 50.550 101 60-140
n-Propylbenzene ug/L 47.150 94 60-140
Naphthalene ug/L 48.750 97 60-140
o-Xylene ug/L 48.850 98 60-140
sec-Butylbenzene ug/L 48.950 98 60-140
Styrene ug/L 50.150 100 60-140
tert-Butylbenzene ug/L 41.850 84 60-140
Tetrachloroethene ug/L 48.650 97 60-140
Toluene ug/L 47.350 95 60-140
trans-1,2-Dichloroethene ug/L 47.250 94 60-140
trans-1,3-Dichloropropene ug/L 53.250 106 60-140
Trichloroethene ug/L 48.750 97 60-140
Trichlorofluoromethane ug/L 42.350 85 60-140
Vinyl chloride ug/L 43.450 87 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92458367
Southland Oil
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2769514LABORATORY CONTROL SAMPLE:
LCSSpike
Xylene (Total)ug/L 146150 97 60-140
1,2-Dichloroethane-d4 (S)%99 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%97 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2769515MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92457678010
2769516
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 8000 107 60-140116 8 308000ND85309250
1,1,1-Trichloroethane ug/L 8000 109 60-140117 7 308000ND87409390
1,1,2,2-Tetrachloroethane ug/L 8000 108 60-140115 6 308000ND86709180
1,1,2-Trichloroethane ug/L 8000 110 60-140115 4 308000ND87909160
1,1-Dichloroethane ug/L 8000 104 60-140109 4 308000ND83408690
1,1-Dichloroethene ug/L 8000 124 60-140130 5 308000ND989010400
1,1-Dichloropropene ug/L 8000 116 60-140124 6 308000ND93109900
1,2,3-Trichlorobenzene ug/L 8000 109 60-140117 7 308000ND87009330
1,2,3-Trichloropropane ug/L 8000 108 60-140113 5 308000ND86109010
1,2,4-Trichlorobenzene ug/L 8000 105 60-140117 11 308000ND83909380
1,2,4-Trimethylbenzene ug/L 8000 111 60-140116 3 30800032201210012500
1,2-Dibromo-3-
chloropropane ug/L 8000 105 60-140115 9 308000ND83809190
1,2-Dibromoethane (EDB)ug/L 8000 107 60-140113 5 308000ND85909050
1,2-Dichlorobenzene ug/L 8000 108 60-140112 4 308000ND86308970
1,2-Dichloroethane ug/L 8000 105 60-140103 1 308000ND83608250
1,2-Dichloropropane ug/L 8000 113 60-140115 2 308000ND90309180
1,3,5-Trimethylbenzene ug/L 8000 123 60-140127 4 308000ND981010200
1,3-Dichlorobenzene ug/L 8000 106 60-140113 7 308000ND84909060
1,3-Dichloropropane ug/L 8000 116 60-140119 3 308000ND92509530
1,4-Dichlorobenzene ug/L 8000 106 60-140113 7 308000ND84709040
2,2-Dichloropropane ug/L 8000 109 60-140116 7 308000ND86909320
2-Butanone (MEK)ug/L 16000 94 60-140103 7 301600048501990021400
2-Chlorotoluene ug/L 8000 113 60-140114 0 308000ND90609090
2-Hexanone ug/L 16000 113 60-140114 0 3016000ND1840018400
4-Chlorotoluene ug/L 8000 108 60-140117 9 308000ND86209390
Benzene ug/L 8000 114 60-140104 3 308000156002470023900
Bromobenzene ug/L 8000 109 60-140117 7 308000ND87109370
Bromochloromethane ug/L 8000 103 60-140112 9 308000ND82208960
Bromodichloromethane ug/L 8000 111 60-140114 2 308000ND89009130
Bromoform ug/L 8000 104 60-140112 8 308000ND82908970
Bromomethane ug/L R180006960-140112 48 308000ND54908970
Carbon tetrachloride ug/L 8000 113 60-140117 3 308000ND90709370
Chlorobenzene ug/L 8000 106 60-140114 7 308000ND85009130
Chloroethane ug/L 8000 104 60-140102 3 308000ND83608120
Chloroform ug/L 8000 107 60-140111 3 30800072393209620
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92458367
Southland Oil
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2769515MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92457678010
2769516
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloromethane ug/L 8000 72 60-14083 14 308000ND57406630
cis-1,2-Dichloroethene ug/L 8000 105 60-140111 5 308000ND84308910
cis-1,3-Dichloropropene ug/L 8000 110 60-140120 8 308000ND88309560
Dibromochloromethane ug/L 8000 110 60-140116 5 308000ND88109270
Dibromomethane ug/L 8000 101 60-140110 8 308000ND81008780
Dichlorodifluoromethane ug/L 8000 83 60-14091 9 308000ND66607270
Diisopropyl ether ug/L 8000 105 60-140109 3 30800028001120011500
Ethylbenzene ug/L 8000 104 60-140113 6 30800041501240013200
Hexachloro-1,3-butadiene ug/L 8000 108 60-140118 8 308000ND86409400
Isopropylbenzene(Cumene)ug/L 8000 114 60-140118 4 308000ND90809430
m&p-Xylene ug/L 16000 113 60-140119 3 3016000131003120032300
Methyl-tert-butyl ether ug/L 8000 110 60-140107 3 30800046492309000
Methylene Chloride ug/L 8000 103 60-14088 15 308000ND82107070
n-Butylbenzene ug/L 8000 112 60-140120 7 308000ND89609560
n-Propylbenzene ug/L 8000 111 60-140116 4 308000ND89109250
Naphthalene ug/L 8000 98 60-140110 10 3080001300912010100
o-Xylene ug/L 8000 113 60-140117 2 30800061801520015500
sec-Butylbenzene ug/L 8000 110 60-140120 8 308000ND88409600
Styrene ug/L 8000 108 60-140113 4 308000ND86809050
tert-Butylbenzene ug/L 8000 96 60-140102 6 308000ND76908150
Tetrachloroethene ug/L 8000 106 60-140113 7 308000ND84609060
Toluene ug/L M180005660-14085 4 308000496005400056400
trans-1,2-Dichloroethene ug/L 8000 115 60-140106 9 308000ND92108460
trans-1,3-Dichloropropene ug/L 8000 108 60-140113 4 308000ND86709060
Trichloroethene ug/L 8000 109 60-140115 5 308000ND87109170
Trichlorofluoromethane ug/L 8000 107 60-140114 7 308000ND85309120
Vinyl chloride ug/L 8000 102 60-140108 6 308000ND81308640
Xylene (Total)ug/L 24000 113 60-140119 3 3024000193004640047800
1,2-Dichloroethane-d4 (S)%103 70-13094
4-Bromofluorobenzene (S)%104 70-130104
Toluene-d8 (S)%96 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92458367
Southland Oil
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
517125
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples:92458367002, 92458367004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2769523
Associated Lab Samples:92458367002, 92458367004
Matrix:Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L <0.42 0.50 12/30/19 01:430.42
1,1,1-Trichloroethane ug/L <0.28 0.50 12/30/19 01:430.28
1,1,2,2-Tetrachloroethane ug/L <0.19 0.50 12/30/19 01:430.19
1,1,2-Trichloroethane ug/L <0.23 0.50 12/30/19 01:430.23
1,1-Dichloroethane ug/L <0.24 0.50 12/30/19 01:430.24
1,1-Dichloroethene ug/L <0.22 0.50 12/30/19 01:430.22
1,1-Dichloropropene ug/L <0.35 0.50 12/30/19 01:430.35
1,2,3-Trichlorobenzene ug/L <0.78 2.0 12/30/19 01:430.78
1,2,3-Trichloropropane ug/L <0.27 0.50 12/30/19 01:430.27
1,2,4-Trichlorobenzene ug/L <0.44 2.0 12/30/19 01:430.44
1,2,4-Trimethylbenzene ug/L <0.19 0.50 12/30/19 01:430.19
1,2-Dibromo-3-chloropropane ug/L <0.38 1.0 12/30/19 01:430.38
1,2-Dibromoethane (EDB)ug/L <0.23 0.50 12/30/19 01:430.23
1,2-Dichlorobenzene ug/L <0.24 0.50 12/30/19 01:430.24
1,2-Dichloroethane ug/L <0.26 0.50 12/30/19 01:430.26
1,2-Dichloropropane ug/L <0.18 0.50 12/30/19 01:430.18
1,3,5-Trimethylbenzene ug/L <0.23 0.50 12/30/19 01:430.23
1,3-Dichlorobenzene ug/L <0.25 0.50 12/30/19 01:430.25
1,3-Dichloropropane ug/L <0.34 0.50 12/30/19 01:430.34
1,4-Dichlorobenzene ug/L <0.25 0.50 12/30/19 01:430.25
2,2-Dichloropropane ug/L <0.28 0.50 12/30/19 01:430.28
2-Butanone (MEK)ug/L <3.6 5.0 12/30/19 01:433.6
2-Chlorotoluene ug/L <0.21 0.50 12/30/19 01:430.21
2-Hexanone ug/L <0.60 5.0 12/30/19 01:430.60
4-Chlorotoluene ug/L <0.21 0.50 12/30/19 01:430.21
Benzene ug/L <0.24 0.50 12/30/19 01:430.24
Bromobenzene ug/L <0.22 0.50 12/30/19 01:430.22
Bromochloromethane ug/L <0.26 0.50 12/30/19 01:430.26
Bromodichloromethane ug/L <0.18 0.50 12/30/19 01:430.18
Bromoform ug/L <0.40 0.50 12/30/19 01:430.40
Bromomethane ug/L <1.7 5.0 12/30/19 01:431.7
Carbon tetrachloride ug/L <0.23 0.50 12/30/19 01:430.23
Chlorobenzene ug/L <0.22 0.50 12/30/19 01:430.22
Chloroethane ug/L <0.58 1.0 12/30/19 01:430.58
Chloroform ug/L <0.35 0.50 12/30/19 01:430.35
Chloromethane ug/L <0.42 1.0 12/30/19 01:430.42
cis-1,2-Dichloroethene ug/L <0.21 0.50 12/30/19 01:430.21
cis-1,3-Dichloropropene ug/L <0.36 0.50 12/30/19 01:430.36
Dibromochloromethane ug/L <0.40 0.50 12/30/19 01:430.40
Dibromomethane ug/L <0.31 0.50 12/30/19 01:430.31
Dichlorodifluoromethane ug/L <0.28 0.50 12/30/19 01:430.28
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92458367
Southland Oil
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2769523
Associated Lab Samples:92458367002, 92458367004
Matrix:Water
AnalyzedMDL
Diisopropyl ether ug/L <0.33 0.50 12/30/19 01:430.33
Ethylbenzene ug/L <0.24 0.50 12/30/19 01:430.24
Hexachloro-1,3-butadiene ug/L <1.2 2.0 12/30/19 01:431.2
Isopropylbenzene (Cumene)ug/L <0.24 0.50 12/30/19 01:430.24
m&p-Xylene ug/L <0.44 1.0 12/30/19 01:430.44
Methyl-tert-butyl ether ug/L <0.44 0.50 12/30/19 01:430.44
Methylene Chloride ug/L <1.5 2.0 12/30/19 01:431.5
n-Butylbenzene ug/L <0.35 0.50 12/30/19 01:430.35
n-Propylbenzene ug/L <0.24 0.50 12/30/19 01:430.24
Naphthalene ug/L <0.66 2.0 12/30/19 01:430.66
o-Xylene ug/L <0.24 0.50 12/30/19 01:430.24
sec-Butylbenzene ug/L <0.25 0.50 12/30/19 01:430.25
Styrene ug/L <0.26 0.50 12/30/19 01:430.26
tert-Butylbenzene ug/L <0.25 0.50 12/30/19 01:430.25
Tetrachloroethene ug/L <0.23 0.50 12/30/19 01:430.23
Toluene ug/L <0.23 0.50 12/30/19 01:430.23
trans-1,2-Dichloroethene ug/L <0.26 0.50 12/30/19 01:430.26
trans-1,3-Dichloropropene ug/L <0.39 0.50 12/30/19 01:430.39
Trichloroethene ug/L <0.23 0.50 12/30/19 01:430.23
Trichlorofluoromethane ug/L <0.34 1.0 12/30/19 01:430.34
Vinyl chloride ug/L <0.41 1.0 12/30/19 01:430.41
Xylene (Total)ug/L <0.50 1.0 12/30/19 01:430.50
1,2-Dichloroethane-d4 (S)%97 70-130 12/30/19 01:43
4-Bromofluorobenzene (S)%100 70-130 12/30/19 01:43
Toluene-d8 (S)%92 70-130 12/30/19 01:43
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2769524LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 51.050 102 60-140
1,1,1-Trichloroethane ug/L 49.050 98 60-140
1,1,2,2-Tetrachloroethane ug/L 50.850 102 60-140
1,1,2-Trichloroethane ug/L 47.550 95 60-140
1,1-Dichloroethane ug/L 43.550 87 60-140
1,1-Dichloroethene ug/L 49.650 99 60-140
1,1-Dichloropropene ug/L 54.750 109 60-140
1,2,3-Trichlorobenzene ug/L 51.750 103 60-140
1,2,3-Trichloropropane ug/L 50.450 101 60-140
1,2,4-Trichlorobenzene ug/L 49.950 100 60-140
1,2,4-Trimethylbenzene ug/L 49.550 99 60-140
1,2-Dibromo-3-chloropropane ug/L 52.250 104 60-140
1,2-Dibromoethane (EDB)ug/L 51.850 104 60-140
1,2-Dichlorobenzene ug/L 50.250 100 60-140
1,2-Dichloroethane ug/L 46.350 93 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92458367
Southland Oil
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2769524LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dichloropropane ug/L 49.450 99 60-140
1,3,5-Trimethylbenzene ug/L 48.350 97 60-140
1,3-Dichlorobenzene ug/L 47.950 96 60-140
1,3-Dichloropropane ug/L 51.050 102 60-140
1,4-Dichlorobenzene ug/L 48.550 97 60-140
2,2-Dichloropropane ug/L 49.750 99 60-140
2-Butanone (MEK)ug/L 101100 101 60-140
2-Chlorotoluene ug/L 47.250 94 60-140
2-Hexanone ug/L 106100 106 60-140
4-Chlorotoluene ug/L 48.350 97 60-140
Benzene ug/L 50.450 101 60-140
Bromobenzene ug/L 49.050 98 60-140
Bromochloromethane ug/L 46.850 94 60-140
Bromodichloromethane ug/L 49.350 99 60-140
Bromoform ug/L 50.950 102 60-140
Bromomethane ug/L 58.250 116 60-140
Carbon tetrachloride ug/L 50.750 101 60-140
Chlorobenzene ug/L 49.150 98 60-140
Chloroethane ug/L 36.150 72 60-140
Chloroform ug/L 45.250 90 60-140
Chloromethane ug/L 33.350 67 60-140
cis-1,2-Dichloroethene ug/L 43.450 87 60-140
cis-1,3-Dichloropropene ug/L 51.950 104 60-140
Dibromochloromethane ug/L 51.250 102 60-140
Dibromomethane ug/L 45.850 92 60-140
Dichlorodifluoromethane ug/L 36.850 74 60-140
Diisopropyl ether ug/L 43.250 86 60-140
Ethylbenzene ug/L 48.550 97 60-140
Hexachloro-1,3-butadiene ug/L 48.450 97 60-140
Isopropylbenzene (Cumene)ug/L 49.350 99 60-140
m&p-Xylene ug/L 98.1100 98 60-140
Methyl-tert-butyl ether ug/L 45.050 90 60-140
Methylene Chloride ug/L 39.150 78 60-140
n-Butylbenzene ug/L 50.450 101 60-140
n-Propylbenzene ug/L 46.850 94 60-140
Naphthalene ug/L 51.150 102 60-140
o-Xylene ug/L 49.550 99 60-140
sec-Butylbenzene ug/L 48.350 97 60-140
Styrene ug/L 49.950 100 60-140
tert-Butylbenzene ug/L 41.650 83 60-140
Tetrachloroethene ug/L 48.250 96 60-140
Toluene ug/L 45.050 90 60-140
trans-1,2-Dichloroethene ug/L 43.050 86 60-140
trans-1,3-Dichloropropene ug/L 50.250 100 60-140
Trichloroethene ug/L 48.950 98 60-140
Trichlorofluoromethane ug/L 44.850 90 60-140
Vinyl chloride ug/L 46.150 92 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92458367
Southland Oil
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2769524LABORATORY CONTROL SAMPLE:
LCSSpike
Xylene (Total)ug/L 148150 98 60-140
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%93 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2769525MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92457678014
2769526
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 5000 105 60-140103 1 305000ND52505170
1,1,1-Trichloroethane ug/L 5000 108 60-140111 2 305000ND54105540
1,1,2,2-Tetrachloroethane ug/L 5000 103 60-14098 4 305000ND51404920
1,1,2-Trichloroethane ug/L 5000 103 60-140109 6 305000ND51505470
1,1-Dichloroethane ug/L 5000 109 60-140101 7 305000ND54305070
1,1-Dichloroethene ug/L 5000 127 60-140126 1 305000ND63306280
1,1-Dichloropropene ug/L 5000 120 60-140113 6 305000ND60105630
1,2,3-Trichlorobenzene ug/L 5000 96 60-140106 11 305000ND47805310
1,2,3-Trichloropropane ug/L 5000 100 60-14098 2 305000ND50204920
1,2,4-Trichlorobenzene ug/L 5000 95 60-140100 5 305000ND47304980
1,2,4-Trimethylbenzene ug/L 5000 95 60-140111 10 305000312078508690
1,2-Dibromo-3-
chloropropane ug/L 5000 96 60-14096 0 305000ND47904780
1,2-Dibromoethane (EDB)ug/L 5000 107 60-140103 4 305000ND53605130
1,2-Dichlorobenzene ug/L 5000 99 60-140100 2 305000ND49305010
1,2-Dichloroethane ug/L 5000 98 60-140102 4 305000ND48905100
1,2-Dichloropropane ug/L 5000 113 60-140110 3 305000ND56605480
1,3,5-Trimethylbenzene ug/L 5000 96 60-140106 8 30500069455005980
1,3-Dichlorobenzene ug/L 5000 94 60-140101 8 305000ND46805060
1,3-Dichloropropane ug/L 5000 107 60-140107 1 305000ND53705330
1,4-Dichlorobenzene ug/L 5000 101 60-140102 0 305000ND50605080
2,2-Dichloropropane ug/L 5000 96 60-14094 2 305000ND48104700
2-Butanone (MEK)ug/L 10000 95 60-14094 1 301000029201240012400
2-Chlorotoluene ug/L 5000 96 60-140100 4 305000ND48004980
2-Hexanone ug/L 10000 98 60-140102 4 3010000ND994010300
4-Chlorotoluene ug/L 5000 91 60-140101 10 305000ND45605070
Benzene ug/L 5000 94 60-14094 0 30500095301420014200
Bromobenzene ug/L 5000 97 60-140103 5 305000ND48705130
Bromochloromethane ug/L 5000 104 60-140104 0 305000ND52005210
Bromodichloromethane ug/L 5000 107 60-140109 2 305000ND53305460
Bromoform ug/L 5000 99 60-14098 1 305000ND49404910
Bromomethane ug/L 5000 78 60-140105 30 305000ND38805230
Carbon tetrachloride ug/L 5000 115 60-140111 4 305000ND57605540
Chlorobenzene ug/L 5000 104 60-140101 2 305000ND51905070
Chloroethane ug/L 5000 110 60-14098 11 305000ND55004920
Chloroform ug/L 5000 105 60-140111 6 305000ND52305570
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 30
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92458367
Southland Oil
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2769525MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92457678014
2769526
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chloromethane ug/L 5000 79 60-14081 2 305000ND39704060
cis-1,2-Dichloroethene ug/L 5000 110 60-140103 6 305000ND54805150
cis-1,3-Dichloropropene ug/L 5000 105 60-140112 7 305000ND52505620
Dibromochloromethane ug/L 5000 108 60-140104 3 305000ND53905220
Dibromomethane ug/L 5000 98 60-140101 3 305000ND48805050
Dichlorodifluoromethane ug/L 5000 90 60-14087 3 305000ND44804370
Diisopropyl ether ug/L 5000 102 60-14095 5 305000188069606650
Ethylbenzene ug/L 5000 108 60-140101 4 305000341088108480
Hexachloro-1,3-butadiene ug/L 5000 97 60-14097 0 305000ND48504850
Isopropylbenzene(Cumene)ug/L 5000 106 60-140103 3 30500013054405270
m&p-Xylene ug/L 10000 109 60-140104 2 3010000119002280022400
Methyl-tert-butyl ether ug/L 5000 107 60-140102 5 30500030856705410
Methylene Chloride ug/L 5000 101 60-14097 3 305000ND50404870
n-Butylbenzene ug/L 5000 105 60-140105 0 305000ND52405240
n-Propylbenzene ug/L 5000 91 60-14097 7 30500040549405280
Naphthalene ug/L 5000 106 60-140109 3 30500082561006290
o-Xylene ug/L 5000 107 60-140102 2 30500057101110010800
sec-Butylbenzene ug/L 5000 96 60-140109 13 305000ND48205470
Styrene ug/L 5000 104 60-140102 2 305000ND51905100
tert-Butylbenzene ug/L 5000 82 60-14092 11 305000ND41204580
Tetrachloroethene ug/L 5000 113 60-14099 14 305000ND56604930
Toluene ug/L M1500018760-140220 4 305000296003900040600
trans-1,2-Dichloroethene ug/L 5000 114 60-140107 7 305000ND57205340
trans-1,3-Dichloropropene ug/L 5000 106 60-140108 2 305000ND52905380
Trichloroethene ug/L 5000 111 60-140108 3 30500038759505790
Trichlorofluoromethane ug/L 5000 110 60-140108 2 305000ND55105400
Vinyl chloride ug/L 5000 105 60-140104 1 305000ND52305180
Xylene (Total)ug/L 15000 109 60-140104 2 3015000176003390033200
1,2-Dichloroethane-d4 (S)%101 70-13095
4-Bromofluorobenzene (S)%100 70-13099
Toluene-d8 (S)%94 70-130105
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 30
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92458367
Southland Oil
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
RPD value was outside control limits.R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 30
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92458367
Southland Oil
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92458367001 517123MW-2R SM 6200B
92458367002 517125MW-5R SM 6200B
92458367003 517123MW-6R SM 6200B
92458367004 517125MW-7R SM 6200B
92458367005 517123Field Blank SM 6200B
92458367006 517123MW-8 SM 6200B
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 12/31/2019 09:03 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 30
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