HomeMy WebLinkAboutMO-4567_15286_CA_MRP_20200103
Groundwater Monitoring Report
Former Evan’s Grocery, No.15286
7022 Landsford Road
Monroe, North Carolina 28112
S&ME Project No. 4305-17-152C
PREPARED FOR:
NCDEQ, DWM, UST Section
1646 Mail Service Center
Raleigh, NC 27699-1646
PREPARED BY:
S&ME, Inc.
9751 Southern Pine Boulevard
Charlotte, NC 28273
January 3, 2020
S&ME, Inc. | 3201 Spring Forest Road | Raleigh, NC 27616 | p 919.872.2660 | www.smeinc.com
January 3, 2020
NCDEQ, DWM, UST Section
1646 Mail Service Center
Raleigh, NC 27699-1646
Attention: Mr. Scott Ryals
Reference: Groundwater Monitoring Report
Former Evan’s Grocery, Incident #15286, UST No. MO-4567
7022 Lansford Road
Monroe, Union County, North Carolina
S&ME Project No. 4305-17-152C
Dear Mr. Ryals:
S&ME, Inc., (S&ME) presents this report in accordance with the North Carolina Department of Environmental
Quality/S&ME Contract No. N17002 and S&ME Proposal No. 43-1400424A, dated August 10, 2018, as authorized
by Task Authorization No. 04, dated August 23, 2019.
If you have any questions or comments regarding this report, please contact us at your convenience.
Sincerely,
S&ME, Inc.
Laura Beth Slagle James E. Wellons III, P.G.
Staff Professional Senior Geologist
SR: WHW
Monitoring Report
Former Former Evan’s Grocery, Incident #15286, UST No. MO-4567
7022 Lansford Road
Monroe, Union County, North Carolina
S&ME Project No. 4305-17-152C
January 3, 2020 ii
Table of Contents
1.0 Site Information ................................................................................................................ 1
1.1 Site Identification ............................................................................................................................ 1
Information about Contacts Associated with the Leaking UST System .............................................................. 1
1.2 Information about Release ............................................................................................................ 1
1.3 Information about the Monitoring Report .................................................................................. 1
1.4 Certification ..................................................................................................................................... 2
2.0 Executive Summary .......................................................................................................... 3
3.0 Scope of Services ............................................................................................................... 4
3.1 Contract Information ..................................................................................................................... 4
3.2 Approved Scope of Services ......................................................................................................... 4
4.0 Site History and Characterization ................................................................................. 5
4.1 UST Owner and Operator Information ....................................................................................... 5
4.2 UST Information ............................................................................................................................. 5
4.3 Description of the UST Release .................................................................................................... 5
4.4 Owners and Occupants of Adjoining/Nearby Properties and Land Use ............................... 5
4.5 Receptors/Potential Receptor Information .................................................................................. 6
5.0 Current Site Assessment Information .......................................................................... 7
5.1 Monitoring Well Installation ......................................................................................................... 7
5.2 Groundwater Monitoring Event .................................................................................................. 7
5.2.1 Soil and Bedrock ................................................................................................................................ 7
5.2.2 Hydrogeology .................................................................................................................................... 7
5.2.3 Current Extent and Severity of Contamination ............................................................................... 8
5.2.4 Cleanup Levels Achieved ................................................................................................................... 8
6.0 Conclusion and Recommendations ............................................................................... 9
Monitoring Report
Former Former Evan’s Grocery, Incident #15286, UST No. MO-4567
7022 Lansford Road
Monroe, Union County, North Carolina
S&ME Project No. 4305-17-152C
January 3, 2020 iii
List of Figures
1. USGS Topographic Map
2. Site Map
3. Groundwater Elevation Map
4. Potential Receptor Map
5. Groundwater Quality Map
List of Tables
1. Site History - UST/AST System Information
2. Site History - UST/AST Owner Information
3. Well Construction and Liquid Level Date
4. Summary of Groundwater Sampling Results
Appendices
Appendix I – Figures
Appendix II – Tables
Appendix III – Site Photographs
Appendix IV – Boring Log, Field Notes and Field Sampling Forms
Appendix V – Laboratory Analytical Reports and Chain of Custody Forms
Monitoring Report
Former Former Evan’s Grocery, Incident #15286, UST No. MO-4567
7022 Lansford Road
Monroe, Union County, North Carolina
S&ME Project No. 4305-17-152C
January 3, 2020 1
1.0 Site Information
1.1 Site Identification
Date of Report: January 3, 2020
Facility I.D. 00-0-0000008708 UST Incident No.: 15286 UST No.: MO-4567
Site Risk: High Site Rank: H0150D Land Use Category: Commercial
Site Name: Former Evans Grocery, Inc. 15286
Site Address: 7022 Landsford Road_
City/Town: Monroe Code: 28112 County: Union
Description of Geographical Data (e.g., diesel fill port): Approximate MW-1 Location
Location Method (GPS, Topographical map, other): Google Earth
Latitude (decimal degrees): 34.842851º N Longitude (decimal degrees): 80.414178º W
Information about Contacts Associated with the Leaking UST System
Former UST Owner/Operator: Laney Oil Company
UST Operator: Laney Oil Company
Property Occupant: Vacant
Consultant/Contractor: S&ME, Inc.
Address: 9751 Southern Pine Boulevard, Raleigh, NC Telephone: 919-872-2660
Analytical Laboratory: Con-Test Analytical Laboratory North Carolina Certification No.: 652
Address: 39 Spruce Street, East Longmeadow, MA 01028 Telephone: 413-525-2332
1.2 Information about Release
Date Reported: 4/1/1996
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release (Dispenser/Piping/UST): UST System
Sizes and contents of UST system(s) from which the release occurred: (2) 2,000-gallon gasoline UST, (1)
1,000-gallon gasoline UST, and (1) 550-gallon diesel UST
1.3 Information about the Monitoring Report
Date of Groundwater Monitoring: November 6, 2019
Monitoring Report
Former Former Evan’s Grocery, Incident #15286, UST No. MO-4567
7022 Lansford Road
Monroe, Union County, North Carolina
S&ME Project No. 4305-17-152C
January 3, 2020 2
1.4 Certification
I, James E. Wellons III, a Professional Geologist for S&ME, do certify that the information contained in this report is
correct and accurate to the best of my knowledge. S&ME is licensed to practice geology/engineering in North
Carolina. Geology License Certification #C-145 and Engineering License Certification #F-0176.
James E. Wellons III, P.E.
Monitoring Report
Former Former Evan’s Grocery, Incident #15286, UST No. MO-4567
7022 Lansford Road
Monroe, Union County, North Carolina
S&ME Project No. 4305-17-152C
January 3, 2020 3
2.0 Executive Summary
On October 10, 2019 S&ME was on site to observe the installation of monitoring well MW-6 by Environmental
Drilling & Probing Services (EDPS), LLC at the Former Evan’s Grocery site. On November 6, 2019 S&ME Personnel
mobilized to the site and collected a groundwater sample from MW-6 and collected water levels and field
measurements from monitoring wells MW-1, MW-2, MW-3, MW-4 and MW-5. The laboratory analytical results
reported multiple constituents present in monitoring well MW-6 at concentrations greater than the 2L Standard:
North Carolina Groundwater Quality Standards: 15A NCAC 2L.0202 and are summarized in the table below.
Contaminant 2L Standard (µg/L) Concentration
(µg/L) Well ID
Benzene 1 190 MW-6
Isopropylbenzene 70 89 MW-6
Methyl tert-butyl ether 20 84 MW-6
Naphthalene 6 320 MW-6
n-Propylbenzene 70 150 MW-6
Xylenes, total 500 1,600 MW-6
1,2,4-Trimethylbenzene 400 1,000 MW-6
S&ME did not measure free product in any of the monitoring wells (MW-1 through MW-6) on November
6, 2019. Free product has not previously been reported in these monitoring wells.
A receptor survey was not completed during this sampling event. Based on the historical data, there are
six active drinking water supply wells (WSW-1, WSW-2, WSW-5, WSW-7, WSW-8 and WSW-10) located
within 1,000 feet of the source area. There are no inactive water supply wells, no irrigation wells, and one
active water supply well located between 0 and 500 feet of the source area; there are five active water
supply wells between 500 and 1,000 feet of the source area. Based on the most recent groundwater flow
at the site water supply well WSW-1 is located downgradient of the site and has the potential to be
impacted by the petroleum release. However, we have been unable to gain access from the property
owner to sample the well. We have made multiple attempts since 2011 to gain access to the water supply
well.
To achieve incident closure, two options are presented:
1. Connect water supply wells located within 1,000 feet of the site to a municipal water source
(municipal water is not available to the site and surrounding properties) – abandoning the water
supply wells located within 250 feet of the source area, or
2. Reduce the level of petroleum constituents to less than the 2L Standard.
Monitoring Report
Former Former Evan’s Grocery, Incident #15286, UST No. MO-4567
7022 Lansford Road
Monroe, Union County, North Carolina
S&ME Project No. 4305-17-152C
January 3, 2020 4
3.0 Scope of Services
3.1 Contract Information
The scope of services for this report was performed in general accordance with S&ME’s proposal number 43-
1400424A dated August 10, 2018 scope of services was authorized by the North Carolina Department of
Environmental Quality (NCDEQ’s)Task Authorization 04, dated August 23, 2019, and within contract number
N17002.
3.2 Approved Scope of Services
S&ME’s approved Scope of Services for this Task Authorization included installing a monitoring well (labeled as
MW-6) to the west of MW-1 and in line with MW-2 and MW-3, sampling monitoring well MW-6 for analysis of
volatile organic compounds (VOCs) by Method 6200B and preparing this report. The scope of services was
completed as proposed.
Monitoring Report
Former Former Evan’s Grocery, Incident #15286, UST No. MO-4567
7022 Lansford Road
Monroe, Union County, North Carolina
S&ME Project No. 4305-17-152C
January 3, 2020 5
4.0 Site History and Characterization
4.1 UST Owner and Operator Information
The UST owner/operator information is provided in Table 1, Appendix II.
4.2 UST Information
Information about the USTs are provided in Table 2.
4.3 Description of the UST Release
Date discovered: March 12, 1996.
Cause and Source (including tank identification number and contents): USTs 1 and 2, (2,000-gallon
gasoline USTs), UST 3 (1,000-gallon gasoline UST), and UST 4 (550-gallon diesel UST)
A photographic log of the site and surroundings is provided as Appendix III.
Based upon the groundwater elevation map (Figure 3), which indicates that the site is located on a
topographic high (between MW-3 and MW-4) and the groundwater is estimated to flow to the east.
4.4 Owners and Occupants of Adjoining/Nearby Properties and Land Use
The site is currently vacant. Historically the site was utilized as a retail automotive fueling station.
The land use of the surrounding area is predominantly residential, with areas of agricultural use and
vacant land.
The site is approximately 550 feet above the Nation Geodetic Vertical Datum of 1929. Based upon the
topographic map reviewed, the area of the subject property is situated on a southwest-northeast
trending ridge, with the predominant slope to the southeast. Refer to Figure 1 for a USGS
Topographic Map.
From the edge of the intersection of Landsford Road and Old Pageland Marshville Highway to the site
structure, the site is covered by gravel. The remainder of the site is covered by grass.
Carolina Creek is located approximately 300 feet east of the source area, and the stream flow is to the
north.
One water supply well (WSW-1) used for drinking water is located approximately 250 feet southeast
of the source area, and five additional wells water supply wells (WSW-2 to the northwest, and WSW-5,
WSW-7, WSW-8, and WSW-10 to the south-southeast) used for drinking water are located between
250 and 1,000 feet of source area.
The site contains an approximately 1,000 square foot structure, which is currently vacant.
Soils underlying the site are the Tarrus gravelly silt loam, which are characterized as having two to
eight percent slopes.
Monitoring Report
Former Former Evan’s Grocery, Incident #15286, UST No. MO-4567
7022 Lansford Road
Monroe, Union County, North Carolina
S&ME Project No. 4305-17-152C
January 3, 2020 6
According to the 1985 USGS Geologic Map of the North Carolina, the site is underlain by the Carolina
Slate Belt of the Piedmont Physiographic Province. Bedrock in this area is metamudstone and meta-
argillite, which is characterized as part of the Cid Formation, which is thin to thick bedded and having
bedding plane and axial-planar cleavage common. It is also interbedded with metasandstone,
metaconglomerate, and metavolcanic rock.
Based upon data collected on November 6, 2019, depth to groundwater measurements at the onsite
monitoring wells ranged from 24.50 feet below top of casing (ft-BTOC) in monitoring well MW-4 to
31.61 ft-BTOC in monitoring well MW-6. Based upon data collected from the previous monitoring
event in July of 2019 groundwater levels were approximately 16.05 to 15.2 feet lower in MW-4 and
MW-1 respectively.
Based upon measurements collected on November 6, 2019, groundwater flow is to the northeast, and west. A site
map is provided as Figure 2 and the locations of water supply wells are provided as Figure 4.
4.5 Receptors/Potential Receptor Information
There are six active potable water supply wells located within 1,000 feet of the source area. Eight
other active potable supply wells are located within 1,000 and 1,500 feet of the source area. One
surface water body (Carolina Creek) is located approximately 300 feet from the source area.
A municipal water source is not currently available to the site and surrounding properties.
Monitoring Report
Former Former Evan’s Grocery, Incident #15286, UST No. MO-4567
7022 Lansford Road
Monroe, Union County, North Carolina
S&ME Project No. 4305-17-152C
January 3, 2020 7
5.0 Current Site Assessment Information
5.1 Monitoring Well Installation
On October 10, 2019 S&ME personnel mobilized to the site to oversee installation of monitoring well MW-6 by
Environmental Drilling & Probing Services (EDPS), LLC. The locations of the existing monitor wells and monitoring
well MW-6 is shown in Figure 2. The signed well construction record by EDPS is included in Appendix IV along
with the boring log completed by S&ME personnel.
5.2 Groundwater Monitoring Event
On November 6, 2019 S&ME personnel mobilized to the site and collected a groundwater sample from
monitoring well MW-6 and collected water levels and field measurements from monitoring wells MW-1, MW-2,
MW-3, MW-4 and MW-5. After measuring the depth-to-water of monitoring well MW-6, S&ME personnel purged
monitoring well MW-6 with a disposable polyethylene bailer by evacuating at least three well volumes. The field
parameters (pH, specific conductivity, and temperature) were collected at the well casing volume and recorded on
groundwater sampling field forms, which are located in Appendix IV. Site photographs are included in Appendix
III.
After completing the well purging, S&ME personnel collected a groundwater sample from monitoring well MW-6
and a field blank. Upon review of the data (see below), it was discovered that the groundwater sample collected
from monitoring well MW-6 was mislabeled in the field as the field blank (FB) and the field blank was labeled as
the sample collected from monitoring well MW-6. The groundwater samples were placed in laboratory-supplied
containers, stored in a cooler with ice, and shipped under chain-of-custody procedures to Con-Test Analytical
Laboratory (Con-Test), a North Carolina certified laboratory for laboratory analysis. The groundwater samples
were analyzed for volatile organic compounds (VOCs) by Standard Method 6200B. The laboratory analytical
results reported multiple constituents present in monitoring well MW-6 at concentrations greater than the 2L
Standard: North Carolina Groundwater Quality Standards: 15A NCAC 2L.0202. Results are shown in Table 4 and
pictured in Figure 5.
The depth-to-water for the monitoring wells ranged from 31.61 feet below top of casing (ft.-BTOC) in monitoring
well MW-6 to 24.50 ft.-BTOC in monitoring well MW-4. The depth to groundwater measurements and
groundwater elevations are provided in Table 3.
5.2.1 Soil and Bedrock
Soils underlying the site are the Tarrus gravelly silt loam, which are characterized as having two to eight percent
slopes. According to the 1985 USGS Geologic Map of the North Carolina, the site is underlain by the Carolina
Slate Belt of the Piedmont Physiographic Province. Bedrock in this area is metamudstone and meta-argillite,
which is characterized as part of the Cid Formation, which is thin to thick bedded and having bedding plane and
axial-planar cleavage common. It is also interbedded with metasandstone, metaconglomerate, and metavolcanic
rock.
5.2.2 Hydrogeology
S&ME calculated the groundwater elevations for the monitor wells gauged using the depth-to-water
measurements collected on November 6, 2019 and the relative top of casing elevations. The groundwater
Monitoring Report
Former Former Evan’s Grocery, Incident #15286, UST No. MO-4567
7022 Lansford Road
Monroe, Union County, North Carolina
S&ME Project No. 4305-17-152C
January 3, 2020 8
elevations were used to prepare a groundwater elevation map (Figure 3), which indicates that the groundwater
flows to the northeast and to the west from monitoring well MW-1. However, in July 2019, groundwater at the
site was calculated to flow to the east, away from a ridge in the vicinity of MW-3. S&ME calculated the average
gradient as approximately 0.098 feet per foot. The change in gradient and groundwater flow since July 2019 may
be attributable to the addition of monitoring well MW-6 and its low groundwater elevation measured during this
monitoring event, in addition to normal fluctuating water levels that occur seasonally.
5.2.3 Current Extent and Severity of Contamination
No free product has been detected in the monitoring wells at the site. Multiple dissolved phase petroleum
constituents in monitor well MW-6 exceed the 2L Standard. No groundwater samples were collected from
monitoring wells MW-1, MW-2, MW-3, MW-4 or MW-5 so the severity of contamination in the vicinity cannot be
spoken to for the current monitoring event. However, historical dissolved contaminant levels indicate
contamination exists at its highest levels near monitoring well MW-1. With the addition of monitoring well MW-6
and the lab results provided during this monitoring event it can be assumed that contamination is likely traveling
west from the vicinity of monitoring well MW-1 with the direction of groundwater flow towards monitoring well
MW-6. Additionally, a groundwater contaminant plume has not been delineated for this monitoring event due to
the lack of data.
5.2.4 Cleanup Levels Achieved
Soil (soil-to-groundwater maximum soil contaminant concentrations) Unknown
Groundwater (2L standard concentrations) No
Free Product - Free product has not been measured at the site. Yes
Monitoring Report
Former Former Evan’s Grocery, Incident #15286, UST No. MO-4567
7022 Lansford Road
Monroe, Union County, North Carolina
S&ME Project No. 4305-17-152C
January 3, 2020 9
6.0 Conclusion and Recommendations
Based on the current and historical assessment information for the site, the following conclusions are presented:
1. The UST Incident meets the following conditions for a High Risk classification:
A. There is one active drinking water supply well within 250 feet of the source area, and four additional
active water supply wells located between 250 and 1,000 feet of the source area. Municipal water is
not available to the area surrounding the site. Based on the most recent groundwater flow at the site
water supply well WSW-1 is located downgradient of the site and has the potential to be impacted by
the petroleum release. However, we have been unable to gain access from the property owner to
sample the well. We have made multiple attempts since 2011 to gain access to the water supply well.
B. Historically contaminant levels in the groundwater exceed the 2L Standards in the previous sampling
event conducted on June 11, 2019.
2. The extent of groundwater contamination at the site is not defined to the south and west.
Based on the above, the following recommendations are presented:
1. Consider collecting natural attenuation data during the next scheduled groundwater sampling event to
further evaluate the site for evidence of natural attenuation.
2. Due to lower water levels in the late summer/fall months, S&ME suggests sampling the wells again in
April 2020 when the water levels should be higher.
3. Attempt to gain access to the adjoining property to the south to collect a groundwater sample from water
supply well WSW-1.
Appendices
Appendix I – Figures
^_
^_Project Location
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
11 " = 2,000 '
12-10-19Drawing Path: Q:\4305\17\152C Evans Grocery 2019 November\1_USGS MAP.mxd plotted by DHomans 12-10-20190 2,000 4,000(FEET)
USGS TOPOGRAPHIC MAP
³
REFERENCE: USGS USA TOPO STREAMING DATASETGIS BASE LAYERS WERE OBTAINED FROM USGS NATIONAL MAP. THIS MAP IS FORINFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONS DISPLAYED ARE APPROXIMATED.THEY ARE NOT BASED ON CIVIL SURVEY INFORMATION, UNLESS STATED OTHERWISE.
4305-17-152C
FORMER EVANS GROCERY TF-15286, UST# MO-45677022 LANDSFORD ROADMONROE, UNION COUNTY, NORTH CAROLINA
!A$
!A$
!A$
!A$
!A$
!A$
¦
Former USTLocations
¦Former DispenserIsland
OLDPAGELANDMARSHVILLERDOLD PAGELAND MARSHVILLE RDLA N DSFO RD RDLAND SFO RD RD
MW-4
MW-1
MW-2
MW-3
MW-5
MW-6
!A$Monitoring Well
Project Parcel
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
21 " = 40 '
12-10-19Drawing Path: Q:\4305\17\152C Evans Grocery 2019 November\2_sitemap.mxd plotted by DHomans 12-10-20190 40 80(FEET)
SITE MAP
³
REFERENCE: 2019 AERIAL PHOTOGRAPHGIS BASE LAYERS WERE OBTAINED FROM UNION COUNTY AND NC ONEMAP. THIS MAP IS FORINFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONS DISPLAYED ARE APPROXIMATED.THEY ARE NOT BASED ON CIVIL SURVEY INFORMATION, UNLESS STATED OTHERWISE.
4305-17-152C
FORMER EVANS GROCERY TF-15286, UST# MO-45677022 LANDSFORD ROADMONROE, UNION COUNTY, NORTH CAROLINA
!A$
!A$
!A$
!A$
!A$
!A$OLDPAGELANDMARSHVILLERDOLD PAGELAND MARSHVILLE RDLA N DSFO RD RDLAN DSFO RD RD
MW-4(74.73)
MW-1(72.41)
MW-2(75.36)
MW-3(74.69)
MW-5(70.44)
MW-6(69.39)
71
7072
7173
7574
727 3
7471
70
72
71
73
75
74
72
73
74
)14.27(Relative Groundwater Elevation (feet) on 11/6/2019
Relative Groundwater Contours (feet)
Groundwater Flow Direction
!A$Monitoring Well
Project Parcel
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
31 " = 30 '
12-10-19Drawing Path: Q:\4305\17\152C Evans Grocery 2019 November\3_gw elevation.mxd plotted by DHomans 12-10-20190 30 60(FEET)
GROUNDWATER ELEVATION MAP
³
REFERENCE: 2019 AERIAL PHOTOGRAPHGIS BASE LAYERS WERE OBTAINED FROM UNION COUNTY AND NC ONEMAP. THISMAP IS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONS DISPLAYEDARE APPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEY INFORMATION, UNLESSSTATED OTHERWISE.
FORMER EVANS GROCERY TF-15286, UST# MO-45677022 LANDSFORD ROADMONROE, UNION COUNTY, NORTH CAROLINA 4305-17-152C
Ð!G
Ð!G
Ð!G
Ð!G
Ð!GÐ!G
●○1
●○1
●○1
●○1
●○1
●○
●○
●○
●○●○E STURDIVANTLANDINGDRLAN DSFO RD RDLANDSFORD RDOLDPAGELANDMARSHVILLERDOLD PAGELAND MARSHVILLE RDWSW-1
WSW-2
WSW-5
WSW-7
WSW-8WSW-10
1
2
3
4
5 1000'500'E Approximate Source Location●○1 Adjacent Properties (See Table 6)
Ð!G Water Supply Wells
Project Parcel
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
41 " = 300 '
12-10-19Drawing Path: Q:\4305\17\152C Evans Grocery 2019 November\4_receptormap.mxd plotted by DHomans 12-10-20190 400 800(FEET)
POTENTIAL RECEPTOR MAP
³
REFERENCE: 2019 AERIAL PHOTOGRAPHGIS BASE LAYERS WERE OBTAINED FROM UNION COUNTY AND NC ONEMAP. THIS MAP IS FORINFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONS DISPLAYED ARE APPROXIMATED.THEY ARE NOT BASED ON CIVIL SURVEY INFORMATION, UNLESS STATED OTHERWISE.
4305-17-152C
FORMER EVANS GROCERY TF-15286, UST# MO-45677022 LANDSFORD ROADMONROE, UNION COUNTY, NORTH CAROLINA
!A$
!A$
!A$
!A$
!A$
!A$
MW-6Benzene= 190Isopropylbenzene= 89Methyl tert-butyl ether= 84Naphthalene= 320n-Propylbenzene= 1501,2,4-Trimethylbenzene= 1,000Total Xylenes= 1,600
MW-4(Not Sampled)
MW-1(Not Sampled)
MW-2(Not Sampled)
MW-3(Not Sampled)
MW-5(Not Sampled)
Concentrations identified by Method6200B exceeding the 2L Standardsare shown in µg/L
Project Parcel
!A$Monitoring Well
SCALE:
DATE:
PROJECT NUMBER
FIGURE NO.
51 " = 30 '
12-18-19Drawing Path: Q:\4305\17\152C Evans Grocery 2019 November\5_gwquality.mxd plotted by DHomans 12-18-20190 30 60(FEET)
GROUNDWATER QUALITY MAPNovember 6, 2019
³
REFERENCE: 2019 AERIAL PHOTOGRAPHGIS BASE LAYERS WERE OBTAINED FROM UNION COUNTY AND NC ONEMAP. THIS MAPIS FOR INFORMATIONAL PURPOSES ONLY. ALL FEATURE LOCATIONS DISPLAYED AREAPPROXIMATED. THEY ARE NOT BASED ON CIVIL SURVEY INFORMATION, UNLESSSTATED OTHERWISE.
4305-17-152C
FORMER EVANS GROCERY TF-15286, UST# MO-45677022 LANDSFORD ROADMONROE, UNION COUNTY, NORTH CAROLINA
Appendix II – Tables
TABLE 1
SITE HISTORY - UST/AST SYSTEM INFORMATION
Former Evans Grocery (Incident No.: 15286, UST #: MO-4567)
7022 Landsford Road, Monroe, North Carolina
S&ME Project # 4305-17-152B
UST
ID Number
Current/Last
Contents
Previous
Contents
Capacity
(gallons)
Construction
Details
Tank
Dimensions
D/L (ft)
Description of
Associated Piping
and Pumps
Date UST
Installed Status of UST
Was Release
Associated With
UST System?
(Yes/No)
1 Gasoline Unknown 2,000 Unkown Unkown Unkown 03/19/83 Closed
(03/05/1996)Yes
2 Gasoline Unknown 2,000 Unkown Unkown Unkown 03/19/83 Closed
(03/05/1996)Yes
3 Gasoline Unknown 1,000 Unkown Unkown Unkown Unknown Closed
(11/23/1998)Yes
4 Diesel Unknown 550 Unkown Unkown Unkown Unknown Closed
(11/23/1998)Yes
Incident
Number
Material
Released
Date of
Release Description of Release
15286 Petroleum 4/1/1996
USTs were removed from the site in March 1996. Indications of contaminated soil were reportedly observed near the
former dispenser island. Analytical results for soil samples collected during closure of the UST system identified
petroleum hydrocarbon concentrations greater than the NCDENR action levels in 1998.
TABLE 2
SITE HISTORY - UST/AST OWNER INFORMATION
Former Evans Grocery (Incident No.: 15286, UST #: MO-4567)
7022 Landsford Road, Monroe, North Carolina
S&ME Project # 4305-17-152B
1 Laney Oil Company Unknown 15286 Unknown
600 N. Johnson Street, Monroe, NC 28110 Unknown
Incident
Number
Owner or
Operator?
Address Telephone Number
UST/AST ID
Number(s)
Name of Owner or
Operator
Dates of Ownership /
Operation
TABLE 3
WELL CONSTRUCTION AND LIQUID LEVEL DATA
7022 Landsford Road, Monroe, North Carolina
S&ME Project # 4305-17-152B
Well
ID
Date
Installed
Date
Water Level
Measured
Well
Casing
Depth
(ft BGS)
Well
Casing
Diameter
(in)
Depth
of Well
(ft-BGS)
Top of
Casing
Elevation*
(ft)
Depth to
Water
from Top
of Casing
(ft)
Free
Product
Thickness
** (ft)
Groundwater
Elevation*
(ft)
05/17/11 13.89 ND 86.11
11/30/11 17.93 ND 82.07
12/05/12 23.45 ND 76.55
12/15/14 19.51 ND 80.49
03/08/16 11.45 ND 88.55
08/07/17 22.56 ND 77.44
09/05/18 26.92 ND 73.08
07/09/19 12.39 ND 87.61
11/06/19 27.59 ND 72.41
05/17/11 18.27 ND 83.26
11/30/11 Dry ND NA
12/05/12 25.90 ND 75.63
12/15/14 22.05 ND 79.48
03/08/16 12.20 ND 89.33
08/07/17 25.22 ND 76.31
09/05/18 Dry ND NA
07/09/19 13.90 ND 87.63
11/06/19 26.17 ND 75.36
05/17/11 14.69 ND 85.50
11/30/11 19.52 ND 80.67
12/05/12 21.50 ND 78.69
12/15/14 17.71 ND 82.48
03/08/16 9.94 ND 90.25
08/07/17 21.02 ND 79.17
09/05/18 23.75 ND 76.44
07/09/19 12.19 ND 88.00
11/06/19 25.50 ND 74.69
05/17/11 9.41 ND 89.82
11/30/11 11.92 ND 87.31
12/05/12 21.65 ND 77.58
12/15/14 16.11 ND 83.12
03/08/16 7.17 ND 92.06
08/07/17 22.44 ND 76.79
09/05/18 Dry ND NA
07/09/19 8.45 ND 90.78
11/06/19 24.50 ND 74.73
05/17/11 13.91 ND 82.33
11/30/11 20.10 ND 76.14
12/05/12 Not Located NA NA
12/15/14 16.95 ND 79.29
03/08/16 7.26 ND 88.98
08/07/17 20.97 ND 75.27
09/05/18 25.60 ND 70.64
07/09/19 8.96 ND 87.28
11/06/19 25.80 ND 70.44
MW-6 10/10/19 11/06/19 2.0 20.0 to 40.0 40.0 101.00 31.61 ND 69.39
NOTES:
* : Reference Point for Elevation Measurements:Benchmark Datum:MW-1 top of casing Benchmark Elevation: 100.00 ft
Assumed or Measured:
ft-BGS = feet below ground surface NM = Not Measured NA = Not Applicable
ND = Not Detected NG = Not Gauged
34.0 96.24
Measured
Former Evans Grocery (Incident No.: 15286, UST #: MO-4567)
Screen
Interval
(ft-BGS)
MW-1
17.0 to 27.0
17.0 to 27.0
17.0 to 27.0
to 30.0 30.0 100.00
MW-2 09/06/01 Unknown 2.0 27.0 101.53
04/01/96 01/30/00 2.0 20.0
27.0 100.19
MW-4 09/06/01 Unknown 2.0 27.0 99.23
MW-3 09/06/01 Unknown 2.0
MW-5 03/06/03 Unknown 2.0 Unknown
Well
ID
Date
Collected
tert-Butylbenzene2L Standard (µg/L) NaphthaleneChloroethaneChloroform1,2-DichloroethaneDiisopropyl ether(Isopropyl ether)p-Isopropyltoluene1,2,4-TrimethylbenzeneStyreneTotal Xylenes1,3,5-TrimethylbenzeneMethyl tert-butyl etherTolueneTABLE 4
Former Evan's Grocery (Incident No.: 15286, UST #: MO-4567)
S&ME Project # 4305-17-152B
SUMMARY OF GROUNDWATER SAMPLING RESULTS
7022 Landsford Road, Monroe, North Carolina
Analytical Method →
Contaminant of Concern →n-PropylbenzeneBenzeneIsopropylbenzeneEthylbenzeneMethyl Ethyl Ketone(2-Butanone)n-Butylbenzenesec-Butylbenzene1,4-DichlorobenzeneVolatile Organic Compounds by Standard Method 6200B or equivalent
05/17/11 250 ---98 18 190 0.78 1.0 ---6.9 ---360 51 ---72 370 160 ---56 1,500 470 1,100
11/30/11 320 ---85 15 ---0.58 2.3 ---9.7 ---315 44 ---81 280 120 10 77 750 350 1,160
12/05/12 147 ---------------------------242 41.4 ---65.4 362 141 ---31 1,340 421 715
12/15/14 158 ---< 2.5 < 2.5 < 2.5 < 5.0 < 2.5 ---< 2.5 < 2.5 328 63.0 ---43.3 377 186 < 2.5 29.4 1,340 475 745
03/08/16 120 ---160 19 <10 <10 <20 ---<10 <10 270 39 15 25 350 130 <10 51 1,200 370 930
8/7/2017 130 <100 520 69 <10 <10 5.0 J ---<10 <10 410 90 44 50 540 340 <10 54 2,400 770 1,200
9/5/2018 180 <120 910 200 5.0 J <12 <12 ---<25 <12 630 210 130 72 690 920 <12 28 5,300 2,000 1,530
6/11/2019 39 <200 88 <20 <20 <20 <20 <20 <40 <20 170 45 <20 28 350 150 <20 11 J 1,100 380 324
11/6/2019
05/17/11 100 ---1.9 1.5 ------------2.8 2.1 1.9 16 ---87 120 3.8 ---3.0 6.2 ---6.4
11/30/11
12/05/12 29.4 6.3 4.8 ---------------3.6 3.3 47.5 ---115 529 11.5 ---29 2.9 2.8 3.7
12/15/14 9.7 3.4 3.3 < 0.50 < 1.0 < 0.50 ---0.80 2.7 2.3 31.7 ---98.5 322 4.0 < 0.50 1.2 5.5 1.4 3.5
03/08/16 74 ---6.2 4.9 <0.50 <0.50 <1 ---<0.50 <0.50 5.4 42 <0.50 68 530 12 <0.50 <0.50 9.9 1.6 J 5.6 J
8/7/2017
9/5/2018
6/11/2019 2.5 <5.0 1.8 1.6 <0.50 <0.50 <0.50 <0.50 <1.0 0.84 0.99 11 <0.50 33 52 1.8 <0.50 <0.50 <0.50 <0.50 <1.5
11/6/2019
05/17/11 0.74 ------------------------1.4 ---0.64 ---97 8.3 ------------------
11/30/11 0.34J ---0.48 J ---------------0.59 0.64 ---------120 ---------140 3.0 0.95 0.42J
12/05/12 5.2 ------------------------2.9 0.52 2.9 ---73.9 ---------1.7 ---------
12/15/14 1.4 ---< 0.50 < 0.50 < 0.50 < 1.0 < 0.50 ---< 0.50 1.4 < 0.50 0.68 ---44.2 < 2.0 < 0.50 < 0.50 0.39 J < 0.50 < 0.50 < 1.5
03/08/16 <0.50 ---<0.50 <0.50 <0.50 <0.50 <1 ---<0.50 <0.50 <0.50 <0.50 <0.50 18 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5
8/7/2017 <0.50 4.9 J <0.50 <0.50 <0.50 <5.0 < 0.50 ---<0.50 0.29 J <0.50 <0.50 <0.50 12 < 2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5
9/5/2018 <0.50 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 ---<0.50 0.43 J <0.50 <0.50 <0.50 32 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5
6/11/2019 <0.50 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 12 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5
11/6/2019
05/17/11 ------0.50 ------------------------------0.59 2.9 0.26 J ------1.7 0.60 0.22 J
11/30/11 ---------------------------------------0.63 ---------------------
12/05/12 ---------------------------------------------------------------
12/15/14 0.33 J ---0.49 J < 0.50 < 0.50 < 1.0 < 0.50 ---< 0.50 < 0.50 1.5 < 0.50 ---0.40 J 1.1 J 0.62 < 0.50 < 0.50 4.9 1.6 3.6
03/08/16 <0.50 ---<0.50 <0.50 <0.50 <0.50 <1 ---<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5
8/7/2017 <0.50 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 ---<0.50 <0.50 <0.50 <0.50 <0.50 <0.50 < 2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5
9/5/2018
6/11/2019 <0.50 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 0.21 J <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5
11/6/2019
05/17/11 ------0.12 J ------------------------------1.7 0.37 J ---------0.31 J ------
11/30/11 ---------------------------------------2.0 0.19 J ------------------
12/05/12
12/15/14 < 0.50 ---< 0.50 < 0.50 < 0.50 < 1.0 < 0.50 ---< 0.50 < 0.50 < 0.50 < 0.50 ---2.5 < 2.0 < 0.50 < 0.50 < 0.50 < 0.50 < 0.50 < 1.5
03/08/16 <0.50 ---<0.50 <0.50 <0.50 <0.50 <1 ---<0.50 <0.50 <0.50 <0.50 <0.50 1.4 <0.50 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5
8/7/2017 <0.50 <5.0 <0.50 <0.50 <0.50 <5.0 <0.50 ---<0.50 <0.50 <0.50 <0.50 <0.50 1.1 <2.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5
9/5/2018 <0.50 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 ---<0.50 <0.50 <0.50 <0.50 <0.50 1.6 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5
6/11/2019 <0.50 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 0.20 J <0.50 <0.50 <0.50 <0.50 <0.50 2.6 <5.0 <0.50 <0.50 <0.50 <0.50 <0.50 <1.5
11/6/2019
MW-6 11/6/2019 190 3.9 J 37 9.8 0.47 J <0.50 0.40 J <0.50 <1.0 1.5 500 89 6.4 84 320 150 <0.50 150 1,000 310 1,600
Notes:
Analytes that are not shown for the method were not detected.Concentrations exceeding the 2L Standards are shown in Shaded and BOLD fields.
Concentrations are reported in micrograms per liter (µg/L).Concentrations exceeding the laboratory's reporting limits are shown in BOLD fields.
2L Standard: North Carolina Groundwater Quality Standards: 15A NCAC 2L.0202
GCL - Gross Contamination Level
--- : Not detected above laboratory reporting limits.
J: Estimated concentration greater than the laboratory method detection, but below the laboratory reporting limit
No Sample Collected- Insufficient Volume In Well
No Sample Collected- Insufficient Volume In Well
No Sample Collected for TA-04
No Sample Collected for TA-04
No Sample Collected for TA-04
No Sample Collected for TA-04
No Sample Collected- Insufficient Volume In Well
No Sample Collected - Insufficient Volume In Well
No Sample Collected- Well Not Located
MW-4
MW-3
MW-1
MW-2
MW-5
No Sample Collected for TA-04
Appendix III – Site Photographs
Groundwater Monitoring Report
Former Evan’s Grocery, Incident #15286, UST No. MO-4567
7022 Lansford Road
Monroe, Union County, North Carolina
S&ME Project No. 4305-17-152C
December 13, 2019 i
Date: 10/10/2019 Photographer: Kelsey Murphy Location / Orientation Drilling
Remarks For installation of monitoring well MW-6.
Date: 10/10/2019 Photographer: Kelsey Murphy Location / Orientation Monitoring Well MW-6
Remarks Click here.
Appendix IV – Boring Log, Field Notes and Field Sampling Forms
LOG OF SOIL BORING
WITH MONITOR WELL CONSTRUCTION NOTES
PROJECT NAME:
DATE DRILLED:
DRILLING METHOD:
DEPTH TO WATER:TOC ELEVATION:
LOGGED BY:
DRILLER:
LATITUDE:LONGITUDE:
ELEVATION
(ft.)
DEPTH (ft.)
LITHOLOGY Description WellConstruction WellDescription
NOTES:
0
-5
-10
-15
-20
-25
-30
-35
-40
0
-5
-10
-15
-20
-25
-30
-35
-40
MW-6
TF-15286 Evan's Grocery
10/10/19
Geo Probe
33.88
N/M
K. Murphy
EDPS
N/A
N/A
Gravel
Clayey SAND: Tan; with some gravel, slightly moist
Silty SAND: Tannish Brown; slightly moist
SILT: Reddish Brown; slightly moist
SILT: Light Brown; slightly moist, strong gasoline odor
SILT: Tan; slighly moist, strong gasoline odor
SILT: Tan; dry, strong gasoline odor
SILT: Tan; with some PWR, dry, no odor detected
Partially Weathered Rock: Whitish Tan; with some medium to fine grained sand
and rock fragments, dry
Partially Weathered Rock: Tan; with some medium to fine grained sand and rockfragments, dry
Rock: Greyish White dust; no recovery
Portland Grout
Sch. 40 PVC Casing
Bentonite
#2 Filter Sand
Sch. 40 0.010" Sl. PVC
Screen
Static Water Level
Initial Water Level
Hours Mileage Signature of S&ME Personnel
8.5 90
S&ME, Inc. | www.smeinc.com
Environmental Field Report
Date:
10/10/19
Job Number:
4305-17-152C
Project Name:
TF-15286 Evan’s Grocery
Weather/Temperature:
Rain
Project Location:
7022 Landsford Road, Monroe, NC
Notes By:
☒
Present at the Site:
Kelsey Murphy
☐
0800 – K. Murphy AOS, began opening MW-1 and MW-3 to measure liquid levels. MW-1 WL: 28.21’,
MW-3 WL: 25.00’
0830 – Chris was Priority Underground AOS, began marking out utilities around proposed MW-6 location.
0900 – EDPS AOS, began unloading equipment0
0926 – Mob to MW-6 location
0930 – S&ME held H&S meeting, drillers don’t have enough 4-1/4 augers to go past 20’, began using air
rotary from the beginning.
1030 – at 25’ and soils are still dry. Waited 40 minutes to see if water would come in, still no water.
Began drilling to 30’
1120 – At 30’ slight moisture in soils. Waited another 30 minutes to see if water would come in. After 30
minutes, still no water.
1150 – began drilling to 40’. Well set at 40’
1550 – EDPS & S&ME offsite for the day
0’-5’ (Hand Auger)
0’-0.25’ – Gravel
0.25’-1’ – Tan clayey sand with some gravel, slightly moist
1’-5’ – Tannish Brown silty sand slightly moist
5’-10’ (AIR)
Reddish brown silt, slightly moist
10’-15’
~10’-12’ – See above description for 5’-10’
12’-14’ – Light brown, silt, slightly moist strong gasoline odor
14’-15’ – Tan silt, slightly moist, strong gasoline odor
15’-20’
Tan silt, dry, strong odor
Equipment Used
GeoProbe 7022DT
Atlas Campo Compressor
TF-15286 Evan’s Grocery
7022 Landsford Road, Monroe, NC
S&ME Project No. 4305-17-152C
10/10/19 2
20’-25’
Tan silt, dry with some PWR
25’-30’
Whitish tan PWR, rock frags with some medium to fine grained sand
30’-35’
30’-33’ – Tan PWR, rock frags, sand, strong odor, on top of rock at 33’
33’-35’ – in rock, grey/white dust
35’-40’
In rock – grey/white dust
Well set at 40’ with 20’ of screen
WELL CONSTRUCTION INFORMATION:
Well Depth: 40’
Screen: 40’-20’
Sand: 40’-18’
Bentonite: 18’-16’
Grout: 16’-0’
Initial Water Level: 33.88
Attachments:
Field forms
Hours Mileage Signature of S&ME Personnel
S&ME, Inc. | www.smeinc.com
Environmental Field Report
Date:
11-06-19
Job Number:
4305-17-152B
Project Name:
TF-15286 Former Evans Grocery
Weather/Temperature:
Sunny, 65 °F
Project Location: 7022 Landsford Rd. Monroe, , North
Carolina
Notes By:
☒
Present at the Site:
Matthew Brundage
☐
Well ID DTW PH Temp conduct. Elevation
MW-1 27.59 5.74 19.4 111 TOC- 7’.0” Ground- 5’ 7/8”
MW-2 26.17 6.32 19.4 417 TOC- 5’ 4” 7/8” Ground- 4’ 9” 1/8”
MW-3 25.50 6.67 19.2 512 TOC- 6’ 1/8” Ground- 6’ 4”’7/8”
MW-4 24.50 5.54 18.7 109 TOC- 7’ 8 1/4” Ground- 7’ 3 “7/8”
MW-5 25.80 6.64 18.2 528 N/M
MW-6 31.61 5.72 19.0 189 TOC- 6’.0 Ground 5’ 7”
Attachments: Field Photos
Equipment Used
Metal detector
Tablet
Water level meter
Survey Equipment
Appendix V – Laboratory Analytical Reports and Chain of Custody
Forms
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332
November 18, 2019
James Wellons
S&ME Inc. Charlotte, NC
9751 Southern Pine Blvd.
Charlotte, NC 28273
Project Location: 7022 Landsford Road, Monroe, NC
Client Job Number:
Project Number: 4305-17-152B
Laboratory Work Order Number: 19K0454
Enclosed are results of analyses for samples received by the laboratory on November 7, 2019. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 24
Table of Contents
Table of Contents
Sample Summary 3
Hits Only Report 4
Case Narrative 5
Sample Results 6
19K0454-01 6
19K0454-02 8
Sample Preparation Information 10
QC Data 11
Volatile Organic Compounds by GC/MS 11
B245799 11
B245890 15
Flag/Qualifier Summary 19
Certifications 20
Chain of Custody/Sample Receipt 22
Page 2 of 24
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332
ANALYTICAL SUMMARY
11/18/2019
S&ME Inc. Charlotte, NC
9751 Southern Pine Blvd.
Charlotte, NC 28273
ATTN: James Wellons
4305-17-152B
19K0454
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
7022 Landsford Road, Monroe, NC
MW-6 19K0454-01 Ground Water SM21-22 6200B
FB 19K0454-02 Field Blank SM21-22 6200B
[TOC_1]Sample Summary[TOC]
Page 3 of 24
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332
[TOC_1]Hits Only Report[TOC]EXECUTIVE SUMMARY
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0454-01MW-6
DL
Acetone 4.2 50 g/L SM21-22 6200BJ3.8
Methylene Chloride 0.79 5.0 g/L SM21-22 6200BJ0.34
Client ID:Lab ID:
Analyte Results/Qual RL Units Method
19K0454-02FB
DL
1,2,4-Trimethylbenzene 1000 20 g/L SM21-22 6200B7.2
1,3,5-Trimethylbenzene 310 20 g/L SM21-22 6200B5.6
2-Butanone (MEK)3.9 5.0 g/L SM21-22 6200BL-06, J 1.9
2-Hexanone (MBK)11 5.0 g/L SM21-22 6200BL-06 1.5
4-Methyl-2-pentanone (MIBK)3.7 5.0 g/L SM21-22 6200BL-06, J 1.7
Acetone 8.4 50 g/L SM21-22 6200BJ3.8
Benzene 190 20 g/L SM21-22 6200B7.2
Chloroform 0.40 0.50 g/L SM21-22 6200BJ0.17
Diisopropyl Ether (DIPE)1.5 0.50 g/L SM21-22 6200BL-06 0.17
Ethylbenzene 500 20 g/L SM21-22 6200B5.2
Isopropylbenzene (Cumene)89 0.50 g/L SM21-22 6200B0.17
m+p Xylene 1100 40 g/L SM21-22 6200B12
Methyl tert-Butyl Ether (MTBE)84 0.50 g/L SM21-22 6200B0.25
Naphthalene 320 200 g/L SM21-22 6200B12
n-Butylbenzene 37 0.50 g/L SM21-22 6200B0.21
n-Propylbenzene 150 20 g/L SM21-22 6200B5.2
o-Xylene 500 20 g/L SM21-22 6200B6.8
p-Isopropyltoluene (p-Cymene)6.4 0.50 g/L SM21-22 6200B0.20
sec-Butylbenzene 9.8 0.50 g/L SM21-22 6200B0.16
tert-Butylbenzene 0.47 0.50 g/L SM21-22 6200BJ0.17
Toluene 150 0.50 g/L SM21-22 6200B0.14
Con-Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 4 of 24
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method 6200B, sample(s) 19K0454-02 ran at a dilution due to the concentration of target compounds exceeding the calibration curve limits.
[TOC_1]Case Narrative[TOC]
SM21-22 6200B
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not
affected since all results are "not detected" for associated samples in this batch and bias is on the high side.
Analyte & Samples(s) Qualified:
L-02
Ethanol
B245799-BS1, B245799-BSD1
Vinyl Acetate
B245799-BS1, B245799-BSD1
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the high side.
Analyte & Samples(s) Qualified:
L-06
2-Butanone (MEK)
19K0454-02[FB], B245799-BS1, B245799-BSD1
2-Hexanone (MBK)
19K0454-02[FB], B245799-BS1, B245799-BSD1
4-Methyl-2-pentanone (MIBK)
19K0454-02[FB], B245799-BS1, B245799-BSD1
Diisopropyl Ether (DIPE)
19K0454-02[FB], B245799-BS1, B245799-BSD1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
Ethanol
B245890-BSD1
Methylene Chloride
B245799-BSD1
Vinyl Acetate
B245890-BS1
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 5 of 24
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332
Date Received: 11/7/2019
Work Order: 19K0454Sample Description:Project Location: 7022 Landsford Road, Monroe, N
Sample ID: 19K0454-01
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 11/6/2019 09:15
[TOC_2]19K0454-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
4.2 50 11/13/19 21:50 EEHg/L3.8 11/13/19SM21-22 6200B1JAcetone
ND 0.50 11/13/19 21:50 EEHg/L0.18 11/13/19SM21-22 6200B1Benzene
ND 0.50 11/13/19 21:50 EEHg/L0.15 11/13/19SM21-22 6200B1Bromobenzene
ND 0.50 11/13/19 21:50 EEHg/L0.32 11/13/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/13/19 21:50 EEHg/L0.16 11/13/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/13/19 21:50 EEHg/L0.46 11/13/19SM21-22 6200B1Bromoform
ND 1.0 11/13/19 21:50 EEHg/L0.78 11/13/19SM21-22 6200B1Bromomethane
ND 5.0 11/13/19 21:50 EEHg/L1.9 11/13/19SM21-22 6200B12-Butanone (MEK)
ND 0.50 11/13/19 21:50 EEHg/L0.21 11/13/19SM21-22 6200B1n-Butylbenzene
ND 0.50 11/13/19 21:50 EEHg/L0.16 11/13/19SM21-22 6200B1sec-Butylbenzene
ND 0.50 11/13/19 21:50 EEHg/L0.17 11/13/19SM21-22 6200B1tert-Butylbenzene
ND 0.50 11/13/19 21:50 EEHg/L0.11 11/13/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/13/19 21:50 EEHg/L0.15 11/13/19SM21-22 6200B1Chlorobenzene
ND 50 11/13/19 21:50 EEHg/L11 11/13/19SM21-22 6200B1Ethanol
ND 0.50 11/13/19 21:50 EEHg/L0.21 11/13/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/13/19 21:50 EEHg/L0.35 11/13/19SM21-22 6200B1Chloroethane
ND 0.50 11/13/19 21:50 EEHg/L0.17 11/13/19SM21-22 6200B1Chloroform
ND 1.0 11/13/19 21:50 EEHg/L0.45 11/13/19SM21-22 6200B1Chloromethane
ND 0.50 11/13/19 21:50 EEHg/L0.12 11/13/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/13/19 21:50 EEHg/L0.14 11/13/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/13/19 21:50 EEHg/L0.19 11/13/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/13/19 21:50 EEHg/L0.16 11/13/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/13/19 21:50 EEHg/L0.12 11/13/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/13/19 21:50 EEHg/L0.13 11/13/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/13/19 21:50 EEHg/L0.26 11/13/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/13/19 21:50 EEHg/L0.16 11/13/19SM21-22 6200B11,1-Dichloroethane
ND 1.0 11/13/19 21:50 EEHg/L0.41 11/13/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/13/19 21:50 EEHg/L0.32 11/13/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/13/19 21:50 EEHg/L0.13 11/13/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/13/19 21:50 EEHg/L0.31 11/13/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/13/19 21:50 EEHg/L0.20 11/13/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/13/19 21:50 EEHg/L0.11 11/13/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/13/19 21:50 EEHg/L0.20 11/13/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/13/19 21:50 EEHg/L0.16 11/13/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/13/19 21:50 EEHg/L0.13 11/13/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/13/19 21:50 EEHg/L0.23 11/13/19SM21-22 6200B1trans-1,3-Dichloropropene
ND 0.50 11/13/19 21:50 EEHg/L0.17 11/13/19SM21-22 6200B1Diisopropyl Ether (DIPE)
ND 0.50 11/13/19 21:50 EEHg/L0.13 11/13/19SM21-22 6200B1Ethylbenzene
ND 5.0 11/13/19 21:50 EEHg/L1.5 11/13/19SM21-22 6200B12-Hexanone (MBK)
ND 0.50 11/13/19 21:50 EEHg/L0.17 11/13/19SM21-22 6200B1Isopropylbenzene (Cumene)
ND 0.50 11/13/19 21:50 EEHg/L0.20 11/13/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
ND 0.50 11/13/19 21:50 EEHg/L0.25 11/13/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
0.79 5.0 11/13/19 21:50 EEHg/L0.34 11/13/19SM21-22 6200B1JMethylene Chloride
ND 5.0 11/13/19 21:50 EEHg/L1.7 11/13/19SM21-22 6200B14-Methyl-2-pentanone (MIBK)
[TOC_1]Sample Results[TOC]
Page 6 of 24
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332
Date Received: 11/7/2019
Work Order: 19K0454Sample Description:Project Location: 7022 Landsford Road, Monroe, N
Sample ID: 19K0454-01
Field Sample #: MW-6
Sample Matrix: Ground Water
Sampled: 11/6/2019 09:15
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 5.0 11/13/19 21:50 EEHg/L0.31 11/13/19SM21-22 6200B1Naphthalene
ND 0.50 11/13/19 21:50 EEHg/L0.13 11/13/19SM21-22 6200B1n-Propylbenzene
ND 0.50 11/13/19 21:50 EEHg/L0.11 11/13/19SM21-22 6200B1Styrene
ND 0.50 11/13/19 21:50 EEHg/L0.22 11/13/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/13/19 21:50 EEHg/L0.18 11/13/19SM21-22 6200B1Tetrachloroethylene
ND 0.50 11/13/19 21:50 EEHg/L0.14 11/13/19SM21-22 6200B1Toluene
ND 2.0 11/13/19 21:50 EEHg/L0.57 11/13/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/13/19 21:50 EEHg/L0.40 11/13/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/13/19 21:50 EEHg/L0.20 11/13/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/13/19 21:50 EEHg/L0.16 11/13/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/13/19 21:50 EEHg/L0.24 11/13/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/13/19 21:50 EEHg/L0.33 11/13/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/13/19 21:50 EEHg/L0.25 11/13/19SM21-22 6200B11,2,3-Trichloropropane
ND 0.50 11/13/19 21:50 EEHg/L0.18 11/13/19SM21-22 6200B11,2,4-Trimethylbenzene
ND 0.50 11/13/19 21:50 EEHg/L0.14 11/13/19SM21-22 6200B11,3,5-Trimethylbenzene
ND 20 11/13/19 21:50 EEHg/L10 11/13/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/13/19 21:50 EEHg/L0.45 11/13/19SM21-22 6200B1Vinyl Chloride
ND 1.0 11/13/19 21:50 EEHg/L0.30 11/13/19SM21-22 6200B1m+p Xylene
ND 0.50 11/13/19 21:50 EEHg/L0.17 11/13/19SM21-22 6200B1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 89.9 11/13/19 21:5070-130
Toluene-d8 98.2 11/13/19 21:5070-130
4-Bromofluorobenzene 99.6 11/13/19 21:5070-130
Page 7 of 24
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332
Date Received: 11/7/2019
Work Order: 19K0454Sample Description:Project Location: 7022 Landsford Road, Monroe, N
Sample ID: 19K0454-02
Field Sample #: FB
Sample Matrix: Field Blank
Sampled: 11/6/2019 08:50
[TOC_2]19K0454-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
8.4 50 11/12/19 16:29 LBDg/L3.8 11/12/19SM21-22 6200B1JAcetone
190 20 11/14/19 0:14 EEHg/L7.2 11/13/19SM21-22 6200B40Benzene
ND 0.50 11/12/19 16:29 LBDg/L0.15 11/12/19SM21-22 6200B1Bromobenzene
ND 1.0 11/12/19 16:29 LBDg/L0.32 11/12/19SM21-22 6200B1Bromochloromethane
ND 0.50 11/12/19 16:29 LBDg/L0.16 11/12/19SM21-22 6200B1Bromodichloromethane
ND 0.50 11/12/19 16:29 LBDg/L0.46 11/12/19SM21-22 6200B1Bromoform
ND 5.0 11/12/19 16:29 LBDg/L0.78 11/12/19SM21-22 6200B1Bromomethane
3.9 5.0 11/12/19 16:29 LBDg/L1.9 11/12/19SM21-22 6200B1L-06, J2-Butanone (MEK)
37 0.50 11/12/19 16:29 LBDg/L0.21 11/12/19SM21-22 6200B1n-Butylbenzene
9.8 0.50 11/12/19 16:29 LBDg/L0.16 11/12/19SM21-22 6200B1sec-Butylbenzene
0.47 0.50 11/12/19 16:29 LBDg/L0.17 11/12/19SM21-22 6200B1Jtert-Butylbenzene
ND 0.50 11/12/19 16:29 LBDg/L0.11 11/12/19SM21-22 6200B1Carbon Tetrachloride
ND 0.50 11/12/19 16:29 LBDg/L0.15 11/12/19SM21-22 6200B1Chlorobenzene
ND 100 11/12/19 16:29 LBDg/L11 11/12/19SM21-22 6200B1Ethanol
ND 0.50 11/12/19 16:29 LBDg/L0.21 11/12/19SM21-22 6200B1Chlorodibromomethane
ND 0.50 11/12/19 16:29 LBDg/L0.35 11/12/19SM21-22 6200B1Chloroethane
0.40 0.50 11/12/19 16:29 LBDg/L0.17 11/12/19SM21-22 6200B1JChloroform
ND 0.60 11/12/19 16:29 LBDg/L0.45 11/12/19SM21-22 6200B1Chloromethane
ND 0.50 11/12/19 16:29 LBDg/L0.12 11/12/19SM21-22 6200B12-Chlorotoluene
ND 0.50 11/12/19 16:29 LBDg/L0.14 11/12/19SM21-22 6200B14-Chlorotoluene
ND 0.50 11/12/19 16:29 LBDg/L0.19 11/12/19SM21-22 6200B11,2-Dibromoethane (EDB)
ND 0.50 11/12/19 16:29 LBDg/L0.16 11/12/19SM21-22 6200B11,2-Dichlorobenzene
ND 0.50 11/12/19 16:29 LBDg/L0.12 11/12/19SM21-22 6200B11,3-Dichlorobenzene
ND 0.50 11/12/19 16:29 LBDg/L0.13 11/12/19SM21-22 6200B11,4-Dichlorobenzene
ND 0.50 11/12/19 16:29 LBDg/L0.26 11/12/19SM21-22 6200B1Dichlorodifluoromethane (Freon 12)
ND 0.50 11/12/19 16:29 LBDg/L0.16 11/12/19SM21-22 6200B11,1-Dichloroethane
ND 0.50 11/12/19 16:29 LBDg/L0.41 11/12/19SM21-22 6200B11,2-Dichloroethane
ND 0.50 11/12/19 16:29 LBDg/L0.32 11/12/19SM21-22 6200B11,1-Dichloroethylene
ND 0.50 11/12/19 16:29 LBDg/L0.13 11/12/19SM21-22 6200B1cis-1,2-Dichloroethylene
ND 0.50 11/12/19 16:29 LBDg/L0.31 11/12/19SM21-22 6200B1trans-1,2-Dichloroethylene
ND 0.50 11/12/19 16:29 LBDg/L0.20 11/12/19SM21-22 6200B11,2-Dichloropropane
ND 0.50 11/12/19 16:29 LBDg/L0.11 11/12/19SM21-22 6200B11,3-Dichloropropane
ND 0.50 11/12/19 16:29 LBDg/L0.20 11/12/19SM21-22 6200B12,2-Dichloropropane
ND 0.50 11/12/19 16:29 LBDg/L0.16 11/12/19SM21-22 6200B11,1-Dichloropropene
ND 0.50 11/12/19 16:29 LBDg/L0.13 11/12/19SM21-22 6200B1cis-1,3-Dichloropropene
ND 0.50 11/12/19 16:29 LBDg/L0.23 11/12/19SM21-22 6200B1trans-1,3-Dichloropropene
1.5 0.50 11/12/19 16:29 LBDg/L0.17 11/12/19SM21-22 6200B1L-06Diisopropyl Ether (DIPE)
500 20 11/14/19 0:14 EEHg/L5.2 11/13/19SM21-22 6200B40Ethylbenzene
11 5.0 11/12/19 16:29 LBDg/L1.5 11/12/19SM21-22 6200B1L-062-Hexanone (MBK)
89 0.50 11/12/19 16:29 LBDg/L0.17 11/12/19SM21-22 6200B1Isopropylbenzene (Cumene)
6.4 0.50 11/12/19 16:29 LBDg/L0.20 11/12/19SM21-22 6200B1p-Isopropyltoluene (p-Cymene)
84 0.50 11/12/19 16:29 LBDg/L0.25 11/12/19SM21-22 6200B1Methyl tert-Butyl Ether (MTBE)
ND 5.0 11/12/19 16:29 LBDg/L0.34 11/12/19SM21-22 6200B1Methylene Chloride
3.7 5.0 11/12/19 16:29 LBDg/L1.7 11/12/19SM21-22 6200B1L-06, J4-Methyl-2-pentanone (MIBK)
Page 8 of 24
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332
Date Received: 11/7/2019
Work Order: 19K0454Sample Description:Project Location: 7022 Landsford Road, Monroe, N
Sample ID: 19K0454-02
Field Sample #: FB
Sample Matrix: Field Blank
Sampled: 11/6/2019 08:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
320 200 11/14/19 0:14 EEHg/L12 11/13/19SM21-22 6200B40Naphthalene
150 20 11/14/19 0:14 EEHg/L5.2 11/13/19SM21-22 6200B40n-Propylbenzene
ND 0.50 11/12/19 16:29 LBDg/L0.11 11/12/19SM21-22 6200B1Styrene
ND 0.50 11/12/19 16:29 LBDg/L0.22 11/12/19SM21-22 6200B11,1,2,2-Tetrachloroethane
ND 0.50 11/12/19 16:29 LBDg/L0.18 11/12/19SM21-22 6200B1Tetrachloroethylene
150 0.50 11/12/19 16:29 LBDg/L0.14 11/12/19SM21-22 6200B1Toluene
ND 1.0 11/12/19 16:29 LBDg/L0.57 11/12/19SM21-22 6200B11,2,3-Trichlorobenzene
ND 0.50 11/12/19 16:29 LBDg/L0.40 11/12/19SM21-22 6200B11,2,4-Trichlorobenzene
ND 0.50 11/12/19 16:29 LBDg/L0.20 11/12/19SM21-22 6200B11,1,1-Trichloroethane
ND 0.50 11/12/19 16:29 LBDg/L0.16 11/12/19SM21-22 6200B11,1,2-Trichloroethane
ND 0.50 11/12/19 16:29 LBDg/L0.24 11/12/19SM21-22 6200B1Trichloroethylene
ND 0.50 11/12/19 16:29 LBDg/L0.33 11/12/19SM21-22 6200B1Trichlorofluoromethane (Freon 11)
ND 0.50 11/12/19 16:29 LBDg/L0.25 11/12/19SM21-22 6200B11,2,3-Trichloropropane
1000 20 11/14/19 0:14 EEHg/L7.2 11/13/19SM21-22 6200B401,2,4-Trimethylbenzene
310 20 11/14/19 0:14 EEHg/L5.6 11/13/19SM21-22 6200B401,3,5-Trimethylbenzene
ND 20 11/12/19 16:29 LBDg/L10 11/12/19SM21-22 6200B1Vinyl Acetate
ND 0.50 11/12/19 16:29 LBDg/L0.45 11/12/19SM21-22 6200B1Vinyl Chloride
1100 40 11/14/19 0:14 EEHg/L12 11/13/19SM21-22 6200B40m+p Xylene
500 20 11/14/19 0:14 EEHg/L6.8 11/13/19SM21-22 6200B40o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 85.8 11/12/19 16:2970-130
1,2-Dichloroethane-d4 91.3 11/14/19 0:1470-130
Toluene-d8 97.7 11/14/19 0:1470-130
Toluene-d8 102 11/12/19 16:2970-130
4-Bromofluorobenzene 107 11/12/19 16:2970-130
4-Bromofluorobenzene 99.6 11/14/19 0:1470-130
Page 9 of 24
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332
Sample Extraction Data
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B245799 11/12/195 5.0019K0454-02 [FB]
Prep Method: SW-846 5030B-SM21-22 6200B
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B245890 11/13/195 5.0019K0454-01 [MW-6]
B245890 11/13/190.125 5.0019K0454-02RE1 [FB]
[TOC_1]Sample Preparation Information[TOC]
Page 10 of 24
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B245799 - SW-846 5030B
[TOC_3]B245799[TOC]
Blank (B245799-BLK1) Prepared & Analyzed: 11/12/19
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50 J0.31
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
[TOC_1]QC Data[TOC]
Page 11 of 24
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245799 - SW-846 5030B
Blank (B245799-BLK1) Prepared & Analyzed: 11/12/19
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 84.921.2
g/L 25.0 70-130Surrogate: Toluene-d8 10025.1
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10225.4
LCS (B245799-BS1) Prepared & Analyzed: 11/12/19
Acetone g/L50 100 70-130112112
Benzene g/L0.50 10.0 70-13098.69.86
Bromobenzene g/L0.50 10.0 70-13098.69.86
Bromochloromethane g/L0.50 10.0 70-13010910.9
Bromodichloromethane g/L0.50 10.0 70-13095.29.52
Bromoform g/L0.50 10.0 70-13010410.4
Bromomethane g/L1.0 10.0 60-14074.37.43
2-Butanone (MEK)g/L5.0 100 L-0670-130131*131
n-Butylbenzene g/L0.50 10.0 70-13083.48.34
sec-Butylbenzene g/L0.50 10.0 70-13086.68.66
tert-Butylbenzene g/L0.50 10.0 70-13088.88.88
Carbon Tetrachloride g/L0.50 10.0 70-13090.89.08
Chlorobenzene g/L0.50 10.0 70-13011311.3
Ethanol g/L50 100 L-0270-130190*190
Chlorodibromomethane g/L0.50 10.0 70-13011011.0
Chloroethane g/L0.50 10.0 60-14099.99.99
Chloroform g/L0.50 10.0 70-13090.29.02
Chloromethane g/L0.60 10.0 60-14085.48.54
2-Chlorotoluene g/L0.50 10.0 70-13010210.2
4-Chlorotoluene g/L0.50 10.0 70-13097.99.79
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13010810.8
1,2-Dichlorobenzene g/L0.50 10.0 70-13096.09.60
1,3-Dichlorobenzene g/L0.50 10.0 70-13093.39.33
1,4-Dichlorobenzene g/L0.50 10.0 70-13095.49.54
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14083.08.30
1,1-Dichloroethane g/L0.50 10.0 70-13010710.7
1,2-Dichloroethane g/L0.50 10.0 70-13097.39.73
1,1-Dichloroethylene g/L0.50 10.0 70-13010410.4
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13010610.6
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13011411.4
1,2-Dichloropropane g/L0.50 10.0 70-13012212.2
1,3-Dichloropropane g/L0.50 10.0 70-13010510.5
2,2-Dichloropropane g/L0.50 10.0 70-13081.78.17
1,1-Dichloropropene g/L0.50 10.0 70-13095.89.58
cis-1,3-Dichloropropene g/L0.50 10.0 70-13010310.3
trans-1,3-Dichloropropene g/L0.50 10.0 70-13093.79.37
Page 12 of 24
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245799 - SW-846 5030B
LCS (B245799-BS1) Prepared & Analyzed: 11/12/19
Diisopropyl Ether (DIPE)g/L0.50 10.0 L-0670-130134*13.4
Ethylbenzene g/L0.50 10.0 70-13010410.4
2-Hexanone (MBK)g/L5.0 100 L-0670-130146*146
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13010210.2
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13086.58.65
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13085.98.59
Methylene Chloride g/L5.0 10.0 70-13012612.6
4-Methyl-2-pentanone (MIBK)g/L5.0 100 L-0670-130150*150
Naphthalene g/L0.50 10.0 70-13010410.4
n-Propylbenzene g/L0.50 10.0 70-13010210.2
Styrene g/L0.50 10.0 70-13010510.5
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13012112.1
Tetrachloroethylene g/L0.50 10.0 70-13011111.1
Toluene g/L0.50 10.0 70-13010510.5
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13010210.2
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13099.09.90
1,1,1-Trichloroethane g/L0.50 10.0 70-13087.78.77
1,1,2-Trichloroethane g/L0.50 10.0 70-13010910.9
Trichloroethylene g/L0.50 10.0 70-13010210.2
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13089.88.98
1,2,3-Trichloropropane g/L0.50 10.0 70-13011311.3
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13092.49.24
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13096.29.62
Vinyl Acetate g/L20 100 L-0270-130147*147
Vinyl Chloride g/L0.50 10.0 60-14010810.8
m+p Xylene g/L1.0 20.0 70-13010320.5
o-Xylene g/L0.50 10.0 70-13010310.3
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 83.921.0
g/L 25.0 70-130Surrogate: Toluene-d8 10325.7
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10225.6
LCS Dup (B245799-BSD1) Prepared & Analyzed: 11/12/19
Acetone g/L50 100 2570-130113 0.790113
Benzene g/L0.50 10.0 2570-13098.3 0.3059.83
Bromobenzene g/L0.50 10.0 2570-130102 3.2910.2
Bromochloromethane g/L0.50 10.0 2570-130105 4.0110.5
Bromodichloromethane g/L0.50 10.0 2570-13094.7 0.5279.47
Bromoform g/L0.50 10.0 2570-130112 7.5311.2
Bromomethane g/L1.0 10.0 2560-14077.1 3.707.71
2-Butanone (MEK)g/L5.0 100 25 L-0670-130137 3.94*137
n-Butylbenzene g/L0.50 10.0 2570-13085.0 1.908.50
sec-Butylbenzene g/L0.50 10.0 2570-13088.1 1.728.81
tert-Butylbenzene g/L0.50 10.0 2570-13088.9 0.1138.89
Carbon Tetrachloride g/L0.50 10.0 2570-13089.1 1.898.91
Chlorobenzene g/L0.50 10.0 2570-130116 3.0611.6
Ethanol g/L50 100 25 L-0270-130207 8.85*207
Chlorodibromomethane g/L0.50 10.0 2570-130106 4.1710.6
Chloroethane g/L0.50 10.0 2560-140104 4.5010.4
Chloroform g/L0.50 10.0 2570-13092.1 2.089.21
Chloromethane g/L0.60 10.0 2560-14085.6 0.2348.56
2-Chlorotoluene g/L0.50 10.0 2570-130102 0.68710.2
4-Chlorotoluene g/L0.50 10.0 2570-130102 4.2010.2
Page 13 of 24
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245799 - SW-846 5030B
LCS Dup (B245799-BSD1) Prepared & Analyzed: 11/12/19
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130108 0.83310.8
1,2-Dichlorobenzene g/L0.50 10.0 2570-13096.3 0.3129.63
1,3-Dichlorobenzene g/L0.50 10.0 2570-13095.4 2.239.54
1,4-Dichlorobenzene g/L0.50 10.0 2570-13093.9 1.589.39
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14084.1 1.328.41
1,1-Dichloroethane g/L0.50 10.0 2570-130108 1.0210.8
1,2-Dichloroethane g/L0.50 10.0 2570-13099.3 2.039.93
1,1-Dichloroethylene g/L0.50 10.0 2570-130104 0.57810.4
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-130110 2.7811.0
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-130114 0.35111.4
1,2-Dichloropropane g/L0.50 10.0 2570-130123 0.48912.3
1,3-Dichloropropane g/L0.50 10.0 2570-130108 2.3510.8
2,2-Dichloropropane g/L0.50 10.0 2570-13089.4 9.008.94
1,1-Dichloropropene g/L0.50 10.0 2570-13098.4 2.689.84
cis-1,3-Dichloropropene g/L0.50 10.0 2570-130105 1.8210.5
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13094.5 0.8509.45
Diisopropyl Ether (DIPE)g/L0.50 10.0 25 L-0670-130135 1.34*13.5
Ethylbenzene g/L0.50 10.0 2570-130106 1.0510.6
2-Hexanone (MBK)g/L5.0 100 25 L-0670-130146 0.0273*146
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130106 3.9310.6
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-13087.3 0.9218.73
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13087.6 1.968.76
Methylene Chloride g/L5.0 10.0 25 L-0770-130132 4.26*13.2
4-Methyl-2-pentanone (MIBK)g/L5.0 100 25 L-0670-130149 0.494*149
Naphthalene g/L0.50 10.0 2570-130110 5.0411.0
n-Propylbenzene g/L0.50 10.0 2570-130108 5.3510.8
Styrene g/L0.50 10.0 2570-130108 3.1910.8
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130128 5.7112.8
Tetrachloroethylene g/L0.50 10.0 2570-130114 2.4911.4
Toluene g/L0.50 10.0 2570-130106 0.47310.6
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-130106 3.8610.6
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-130100 1.4010.0
1,1,1-Trichloroethane g/L0.50 10.0 2570-13089.1 1.588.91
1,1,2-Trichloroethane g/L0.50 10.0 2570-130106 2.1410.6
Trichloroethylene g/L0.50 10.0 2570-130101 1.0910.1
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13093.5 4.049.35
1,2,3-Trichloropropane g/L0.50 10.0 2570-130113 0.088611.3
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-13093.3 0.9699.33
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-13099.4 3.279.94
Vinyl Acetate g/L20 100 25 L-0270-130150 2.05*150
Vinyl Chloride g/L0.50 10.0 2560-140109 1.3810.9
m+p Xylene g/L1.0 20.0 2570-130105 2.0320.9
o-Xylene g/L0.50 10.0 2570-130105 2.2110.5
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 83.720.9
g/L 25.0 70-130Surrogate: Toluene-d8 10025.1
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10425.9
Page 14 of 24
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245890 - SW-846 5030B
[TOC_3]B245890[TOC]
Blank (B245890-BLK1) Prepared & Analyzed: 11/13/19
Acetone g/L50ND
Benzene g/L0.50ND
Bromobenzene g/L0.50ND
Bromochloromethane g/L0.50ND
Bromodichloromethane g/L0.50ND
Bromoform g/L0.50ND
Bromomethane g/L1.0ND
2-Butanone (MEK)g/L5.0ND
n-Butylbenzene g/L0.50ND
sec-Butylbenzene g/L0.50ND
tert-Butylbenzene g/L0.50ND
Carbon Tetrachloride g/L0.50ND
Chlorobenzene g/L0.50ND
Ethanol g/L50ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L0.50ND
Chloroform g/L0.50ND
Chloromethane g/L0.60ND
2-Chlorotoluene g/L0.50ND
4-Chlorotoluene g/L0.50ND
1,2-Dibromoethane (EDB)g/L0.50ND
1,2-Dichlorobenzene g/L0.50ND
1,3-Dichlorobenzene g/L0.50ND
1,4-Dichlorobenzene g/L0.50ND
Dichlorodifluoromethane (Freon 12)g/L0.50ND
1,1-Dichloroethane g/L0.50ND
1,2-Dichloroethane g/L0.50ND
1,1-Dichloroethylene g/L0.50ND
cis-1,2-Dichloroethylene g/L0.50ND
trans-1,2-Dichloroethylene g/L0.50ND
1,2-Dichloropropane g/L0.50ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L0.50ND
1,1-Dichloropropene g/L0.50ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diisopropyl Ether (DIPE)g/L0.50ND
Ethylbenzene g/L0.50ND
2-Hexanone (MBK)g/L5.0ND
Isopropylbenzene (Cumene)g/L0.50ND
p-Isopropyltoluene (p-Cymene)g/L0.50ND
Methyl tert-Butyl Ether (MTBE)g/L0.50ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L5.0ND
Naphthalene g/L0.50ND
n-Propylbenzene g/L0.50ND
Styrene g/L0.50ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L0.50ND
Toluene g/L0.50ND
1,2,3-Trichlorobenzene g/L1.0ND
1,2,4-Trichlorobenzene g/L0.50ND
Page 15 of 24
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245890 - SW-846 5030B
Blank (B245890-BLK1) Prepared & Analyzed: 11/13/19
1,1,1-Trichloroethane g/L0.50ND
1,1,2-Trichloroethane g/L0.50ND
Trichloroethylene g/L0.50ND
Trichlorofluoromethane (Freon 11)g/L0.50ND
1,2,3-Trichloropropane g/L0.50ND
1,2,4-Trimethylbenzene g/L0.50ND
1,3,5-Trimethylbenzene g/L0.50ND
Vinyl Acetate g/L20ND
Vinyl Chloride g/L0.50ND
m+p Xylene g/L1.0ND
o-Xylene g/L0.50ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 90.022.5
g/L 25.0 70-130Surrogate: Toluene-d8 98.824.7
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10025.0
LCS (B245890-BS1) Prepared & Analyzed: 11/13/19
Acetone g/L50 100 70-130104104
Benzene g/L0.50 10.0 70-13088.18.81
Bromobenzene g/L0.50 10.0 70-13010110.1
Bromochloromethane g/L0.50 10.0 70-13087.08.70
Bromodichloromethane g/L0.50 10.0 70-13010210.2
Bromoform g/L0.50 10.0 70-13010310.3
Bromomethane g/L1.0 10.0 60-14060.16.01
2-Butanone (MEK)g/L5.0 100 70-13085.685.6
n-Butylbenzene g/L0.50 10.0 70-13010910.9
sec-Butylbenzene g/L0.50 10.0 70-13011111.1
tert-Butylbenzene g/L0.50 10.0 70-13010810.8
Carbon Tetrachloride g/L0.50 10.0 70-13010010.0
Chlorobenzene g/L0.50 10.0 70-13010310.3
Ethanol g/L50 100 70-130116116
Chlorodibromomethane g/L0.50 10.0 70-13097.29.72
Chloroethane g/L0.50 10.0 60-14086.28.62
Chloroform g/L0.50 10.0 70-13088.58.85
Chloromethane g/L0.60 10.0 60-14070.17.01
2-Chlorotoluene g/L0.50 10.0 70-13097.99.79
4-Chlorotoluene g/L0.50 10.0 70-13010610.6
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13098.79.87
1,2-Dichlorobenzene g/L0.50 10.0 70-13010510.5
1,3-Dichlorobenzene g/L0.50 10.0 70-13010710.7
1,4-Dichlorobenzene g/L0.50 10.0 70-13010610.6
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 60-14073.97.39
1,1-Dichloroethane g/L0.50 10.0 70-13092.39.23
1,2-Dichloroethane g/L0.50 10.0 70-13010010.0
1,1-Dichloroethylene g/L0.50 10.0 70-13010010.0
cis-1,2-Dichloroethylene g/L0.50 10.0 70-13091.79.17
trans-1,2-Dichloroethylene g/L0.50 10.0 70-13098.29.82
1,2-Dichloropropane g/L0.50 10.0 70-13091.29.12
1,3-Dichloropropane g/L0.50 10.0 70-13092.69.26
2,2-Dichloropropane g/L0.50 10.0 70-13092.79.27
1,1-Dichloropropene g/L0.50 10.0 70-13092.69.26
cis-1,3-Dichloropropene g/L0.50 10.0 70-13093.49.34
trans-1,3-Dichloropropene g/L0.50 10.0 70-13091.39.13
Page 16 of 24
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245890 - SW-846 5030B
LCS (B245890-BS1) Prepared & Analyzed: 11/13/19
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13087.78.77
Ethylbenzene g/L0.50 10.0 70-13010610.6
2-Hexanone (MBK)g/L5.0 100 70-13095.795.7
Isopropylbenzene (Cumene)g/L0.50 10.0 70-13010710.7
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 70-13010410.4
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 70-13080.68.06
Methylene Chloride g/L5.0 10.0 70-13092.09.20
4-Methyl-2-pentanone (MIBK)g/L5.0 100 70-130102102
Naphthalene g/L0.50 10.0 70-13010210.2
n-Propylbenzene g/L0.50 10.0 70-13010610.6
Styrene g/L0.50 10.0 70-13091.39.13
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13010510.5
Tetrachloroethylene g/L0.50 10.0 70-13010910.9
Toluene g/L0.50 10.0 70-13010110.1
1,2,3-Trichlorobenzene g/L1.0 10.0 70-13094.39.43
1,2,4-Trichlorobenzene g/L0.50 10.0 70-13010810.8
1,1,1-Trichloroethane g/L0.50 10.0 70-13010010.0
1,1,2-Trichloroethane g/L0.50 10.0 70-13098.69.86
Trichloroethylene g/L0.50 10.0 70-13010110.1
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 70-13096.09.60
1,2,3-Trichloropropane g/L0.50 10.0 70-13010310.3
1,2,4-Trimethylbenzene g/L0.50 10.0 70-13094.49.44
1,3,5-Trimethylbenzene g/L0.50 10.0 70-13010410.4
Vinyl Acetate g/L20 100 L-0770-13069.6 *69.6
Vinyl Chloride g/L0.50 10.0 60-14010710.7
m+p Xylene g/L1.0 20.0 70-13010621.1
o-Xylene g/L0.50 10.0 70-13010510.5
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 93.723.4
g/L 25.0 70-130Surrogate: Toluene-d8 98.824.7
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10125.3
LCS Dup (B245890-BSD1) Prepared & Analyzed: 11/13/19
Acetone g/L50 100 2570-130106 1.97106
Benzene g/L0.50 10.0 2570-13086.8 1.498.68
Bromobenzene g/L0.50 10.0 2570-130101 0.29810.1
Bromochloromethane g/L0.50 10.0 2570-13089.1 2.398.91
Bromodichloromethane g/L0.50 10.0 2570-130103 0.58710.3
Bromoform g/L0.50 10.0 2570-13098.5 4.089.85
Bromomethane g/L1.0 10.0 2560-14067.9 12.26.79
2-Butanone (MEK)g/L5.0 100 2570-13087.1 1.7187.1
n-Butylbenzene g/L0.50 10.0 2570-130108 0.91810.8
sec-Butylbenzene g/L0.50 10.0 2570-130109 1.9110.9
tert-Butylbenzene g/L0.50 10.0 2570-130106 2.1510.6
Carbon Tetrachloride g/L0.50 10.0 2570-13099.3 0.9029.93
Chlorobenzene g/L0.50 10.0 2570-130102 1.3710.2
Ethanol g/L50 100 25 L-0770-130131 11.6*131
Chlorodibromomethane g/L0.50 10.0 2570-130101 4.2310.1
Chloroethane g/L0.50 10.0 2560-14087.5 1.508.75
Chloroform g/L0.50 10.0 2570-13088.2 0.3408.82
Chloromethane g/L0.60 10.0 2560-14070.4 0.4277.04
2-Chlorotoluene g/L0.50 10.0 2570-13098.6 0.7129.86
4-Chlorotoluene g/L0.50 10.0 2570-130105 0.56810.5
Page 17 of 24
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B245890 - SW-846 5030B
LCS Dup (B245890-BSD1) Prepared & Analyzed: 11/13/19
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-130104 5.6110.4
1,2-Dichlorobenzene g/L0.50 10.0 2570-130106 0.094810.6
1,3-Dichlorobenzene g/L0.50 10.0 2570-130108 0.46510.8
1,4-Dichlorobenzene g/L0.50 10.0 2570-130106 0.094710.6
Dichlorodifluoromethane (Freon 12)g/L0.50 10.0 2560-14072.7 1.647.27
1,1-Dichloroethane g/L0.50 10.0 2570-13092.3 0.009.23
1,2-Dichloroethane g/L0.50 10.0 2570-130105 4.3910.5
1,1-Dichloroethylene g/L0.50 10.0 2570-130101 0.69510.1
cis-1,2-Dichloroethylene g/L0.50 10.0 2570-13092.2 0.5449.22
trans-1,2-Dichloroethylene g/L0.50 10.0 2570-13096.8 1.449.68
1,2-Dichloropropane g/L0.50 10.0 2570-13095.1 4.199.51
1,3-Dichloropropane g/L0.50 10.0 2570-13097.7 5.369.77
2,2-Dichloropropane g/L0.50 10.0 2570-13089.4 3.628.94
1,1-Dichloropropene g/L0.50 10.0 2570-13092.9 0.3239.29
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13095.9 2.649.59
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13097.6 6.679.76
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-13091.5 4.249.15
Ethylbenzene g/L0.50 10.0 2570-130104 1.7210.4
2-Hexanone (MBK)g/L5.0 100 2570-130100 4.50100
Isopropylbenzene (Cumene)g/L0.50 10.0 2570-130106 0.28210.6
p-Isopropyltoluene (p-Cymene)g/L0.50 10.0 2570-130103 0.67710.3
Methyl tert-Butyl Ether (MTBE)g/L0.50 10.0 2570-13082.1 1.848.21
Methylene Chloride g/L5.0 10.0 2570-13094.8 3.009.48
4-Methyl-2-pentanone (MIBK)g/L5.0 100 2570-130104 1.86104
Naphthalene g/L0.50 10.0 2570-13099.5 2.389.95
n-Propylbenzene g/L0.50 10.0 2570-130104 1.9910.4
Styrene g/L0.50 10.0 2570-13090.7 0.6599.07
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130107 2.0810.7
Tetrachloroethylene g/L0.50 10.0 2570-130107 1.5810.7
Toluene g/L0.50 10.0 2570-130102 0.69110.2
1,2,3-Trichlorobenzene g/L1.0 10.0 2570-13091.5 3.019.15
1,2,4-Trichlorobenzene g/L0.50 10.0 2570-130105 2.4410.5
1,1,1-Trichloroethane g/L0.50 10.0 2570-13099.7 0.7999.97
1,1,2-Trichloroethane g/L0.50 10.0 2570-130100 1.9110.0
Trichloroethylene g/L0.50 10.0 2570-13098.4 2.219.84
Trichlorofluoromethane (Freon 11)g/L0.50 10.0 2570-13093.8 2.329.38
1,2,3-Trichloropropane g/L0.50 10.0 2570-130105 1.6310.5
1,2,4-Trimethylbenzene g/L0.50 10.0 2570-13095.4 1.059.54
1,3,5-Trimethylbenzene g/L0.50 10.0 2570-130104 0.48110.4
Vinyl Acetate g/L20 100 2570-13071.6 2.8071.6
Vinyl Chloride g/L0.50 10.0 2560-140113 4.9911.3
m+p Xylene g/L1.0 20.0 2570-130106 0.23621.2
o-Xylene g/L0.50 10.0 2570-130108 2.5310.8
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 96.324.1
g/L 25.0 70-130Surrogate: Toluene-d8 10025.1
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 10325.7
Page 18 of 24
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
FLAG/QUALIFIER SUMMARY
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits.
Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is
on the high side.
L-02
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the high side.
L-06
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
[TOC_1]Flag/Qualifier Summary[TOC]
Page 19 of 24
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NCAcetone
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCCarbon Tetrachloride
NCChlorobenzene
NCEthanol
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromoethane (EDB)
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiisopropyl Ether (DIPE)
NCEthylbenzene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
[TOC_1]Certifications[TOC]
Page 20 of 24
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX 413/525-6405 * TEL. 413/525-2332
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SM21-22 6200B in Water
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Acetate
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2020
M-MA100Massachusetts DEPMA 06/30/2020
PH-0567Connecticut Department of Publilc HealthCT 09/30/2021
10899 NELAPNew York State Department of HealthNY 04/1/2020
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2020
LAO00112Rhode Island Department of HealthRI 12/30/2019
652North Carolina Div. of Water QualityNC 12/31/2019
MA007 NELAPNew Jersey DEPNJ 06/30/2020
E871027 NELAPFlorida Department of HealthFL 06/30/2020
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2020
2011028State of MaineME 06/9/2021
460217Commonwealth of VirginiaVA 12/14/2019
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2020
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2020
25703North Carolina Department of HealthNC-DW 07/31/2020
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2020
Page 21 of 24
Table of Contents
Page 22 of 24
Table of Contents
Page 23 of 24
Table of Contents
Page 24 of 24
Table of Contents