5504_LakeNorman_DIN25734_20160212

 
10 Quiet Brook Court 314-496-4654
St. Charles, MO 63303 www.jettenviro.com

February 12, 2016 Submitted via Electronic Mail

Ms. Jackie Drummond
North Carolina Department of Environmental Quality
Division of Waste Management - Solid Waste Section
Asheville Regional Office
2090 US Highway 70
Swannanoa, NC 28778

Dear Ms. Drummond:

Re: Submittal of Groundwater and Surface Water Monitoring Results
Second Semi-Annual 2015 Event
Lake Norman Construction & Demolition Landfill
North Carolina, Permit # 55-04

On behalf of BFI Lake Norman Landfill, Inc., Jett Environmental Consulting is providing a water quality summary
for the Second Semi-Annual 2015 (November 2015) sampling event for the Lake Norman Construction &
Demolition Landfill. Groundwater and surface water sampling was performed by Analytical Services, Inc. (ASI)
and analytical testing was performed by ASI. The groundwater and surface water samples were analyzed for
the Detection Monitoring parameters listed in 15A North Carolina Administrative Code (NCAC) 13B
.0544(b)(1)(D), which included the constituents listed in Appendix I of 40 CFR Part 258 (15 heavy metals and
47 organics), mercury, chloride, manganese, sulfate, iron, specific conductance, pH, temperature, alkalinity,
and total dissolved solids. In accordance with a North Carolina Department of Environmental Quality (NCDEQ)
memorandum for C&D landfills dated June 25, 2010, tetrahydrofuran was also monitored for each of the
samples collected. Included in Attachment A is a copy of the laboratory analytical report and field information
forms.

Assessment Monitoring Program

A Groundwater Assessment Monitoring Work Plan was compiled in accordance with 15A NCAC 13B .0545, due to
confirmed methylene chloride detections at MW-4 above the North Carolina 15A NCAC 2L Water Quality Standard
during the Second Semi-Annual 2014 event. The Groundwater Monitoring Assessment Work Plan was submitted on
March 9, 2015 by Jett Environmental Consulting and approved by NCDEQ in correspondence dated March 16, 2015.
Well MW-5 was installed downgradient of MW-4 on March 25, 2015. The sampling activities associated with the Work
Plan were completed during the May 2015 event. During the May 2015 event, the list of constituents in Appendix II
of 40 CFR Part 258 were monitored at well MW-4 and new well MW-5. A summary of the May 2015 event data was
provided to NCDEQ in correspondence dated July 27, 2015.

Per an August 20, 2015 NCDEQ letter, MW-4 was monitored again during the November 2015 event for the Appendix
II assessment monitoring list.

Groundwater Flow Rate & Direction

The attached Figure 1 provides a potentiometric surface map utilizing water level data from the Second Semi-
Annual 2015 event. Groundwater flow direction for the Second Semi-Annual 2015 event was generally to the
northwest, consistent with past reports.

To calculate the average linear groundwater velocity, the hydraulic gradients were measured from the
potentiometric surface map. The groundwater velocities are then calculated from the following equation:
2 

v = [ Ki/n ] * 365

where:
v = groundwater flow velocity (ft/year)
K = hydraulic conductivity (ft/day)
i = hydraulic gradient (ft/ft)
n = effective porosity (dimensionless)

Based on information provided in the “Construction Plan Application” by S&ME, Inc. dated February 20, 1998,
hydraulic conductivity measurements average 1.13 ft/day and the effective porosity measurements average
33%.

During the Second Semi-Annual 2015 event, the hydraulic gradient from the southeast to northwest portion of
the site was estimated at 0.0238 ft/ft.

Using the hydraulic conductivity of 1.13 ft/day, the effective porosity of 0.33, and a hydraulic gradient of 0.0238
ft/ft, the calculated groundwater velocity was 0.081 ft/day (30 ft/yr) for the Second Semi-Annual 2015 event.

Effectiveness of the Monitoring Systems

The groundwater monitoring well network is designed to detect potential effects on groundwater from the facility.
The designated upgradient monitoring well, MW-1, is positioned to monitor background groundwater quality for
the facility. The remaining three wells (MW-2, MW-3, and MW-4) are positioned in the downgradient position
around the base of the landfill footprint. As stated above, delineation well MW-5 was installed downgradient of
MW-4 in March 2015. Each of the wells was sampled during the Second Semi-Annual 2015 event.

The surface water monitoring network is designed to detect potential effects on surface water from the facility.
The designated upgradient point, SW-1, is positioned to monitor background surface water quality for the facility.
The designated downgradient point, SW-2, is positioned to monitor surface water quality downgradient from
the landfill. Both surface water monitoring points were sampled during the Second Semi-Annual 2015 event.

Based on a review of well and surface water locations, groundwater flow directions, flow gradients, flow rates,
and sampling availability, the present monitoring program is considered sufficient to monitor groundwater and
surface water quality surrounding the facility.

Monitoring Summary

A summary of the inorganic results and organic detections for the Second Semi-Annual 2015 event is available
on Table 1. The following is a brief summary of the monitoring data from the Second Semi-Annual 2015 event:

Groundwater

 The NC Solid Waste Section Limit (SWSL) is the lowest amount of analyte in a sample that can be
quantitatively determined with suitable precision and accuracy. The SWSL is the concentration below
which reported analytical results must be qualified as estimated. Four volatile organic compounds
(VOCs) were detected above an SWSL: dichlorodifluoromethane, methylene chloride, tetrahydrofuran,
and trichlorofluoromethane at MW-4. During the Second Semi-Annual 2015 event, only methylene
chloride at MW-4 was above a North Carolina 15A NCAC 2L Water Quality Standard (see Table 1).
The Second Semi-Annual 2015 concentration of methylene chloride at MW-4 (6.2 ug/L) exceeded the
NC 2L Standard (5 ug/L). No VOCs were detected above the SWSLs at MW-5 during the Second
Semi-Annual 2015 event.

3 

 Two inorganic constituents were reported above the NC 2L Standards: total iron at MW-3, MW-4, and
MW-5; and total manganese at MW-3, MW-4, and MW-5.

Surface Water

 No VOCs were detected above an SWSL in surface water samples.

 Two inorganic constituents were reported above the NC 2B Standards: total iron and total manganese
at SW-1 and SW-2.

Total Iron

SW-1 is located upgradient to the facility. The Second Semi-Annual 2015 concentration of total iron at SW-1 (1,730
ug/L) and SW-2 (4,480 ug/L) are consistent with historical total iron concentrations at upgradient surface water point
SW-1 (474 to 2,920 ug/L) and SW-2 (608 to 4,960 ug/L), respectively.

The Second Semi-Annual 2015 total iron concentrations at MW-3 (1,540 ug/L), MW-4 (3,270 ug/L), and MW-5 (624
ug/L) are consistent with the historical total iron concentrations at MW-3 (84.2 to 10,500 ug/L) and MW-4 (149 to 5,100
ug/L), respectively.

Total Manganese

SW-1 is located upgradient to the facility. The Second Semi-Annual 2015 concentrations of total manganese at SW-
1 (310 ug/L) and downgradient SW-2 (260 ug/L) are consistent with historical total manganese concentrations at
upgradient surface water point SW-1 (97.3 to 674 ug/L) and SW-2 1(28 to 329 ug/L), respectively.

The Second Semi-Annual 2015 total manganese concentrations at MW-3 (68.7 ug/L), MW-4 (163 ug/L), and MW-5
(940 ug/L) are consistent with the historical total manganese concentrations at MW-3 (17.3 to 989 ug/L) and MW-4
(14.3 to 123 ug/L), respectively.

The total iron and total manganese concentrations in groundwater and surface water appear to be attributable to
naturally occurring conditions at the site and not related to the landfill. The total metal concentrations at new well MW-
5 appear to be elevated due to sediment in the sample and should continue to decrease upon further well development
each event.

Assessment Activities Summary

In order to delineate the extent of methylene chloride in the vicinity of MW-4, one additional well (MW-5) was
installed downgradient of MW-4 in March 2015 (see Figure 1). Delineation well MW-5 allowed collection of a
groundwater sample in the direction of any potential migration. The distance from MW-4 to the facility property
boundary (Forney Creek) is approximately 185 feet. Very saturated surface conditions exist between MW-4
and Forney Creek. Well MW-5 was installed approximately 70 feet North of MW-4.

The only organic compounds that have been confirmed detected above SWSLs at MW-4 are methylene
chloride, tetrahydrofuran, and trichlorofluoromethane. Dichlorodifluoromethane was detected for the first time
at MW-4 during the Second Semi-Annual 2015 event. The next semi-annual event (May 2016) will be utilized
to confirm the initial detection of dichlorodifluoromethane at MW-4. Methylene chloride and
trichlorofluoromethane are commonly found in landfill gas (LFG). C&D landfills are not required to have a
leachate collection system. Therefore, a representative leachate sample cannot be collected for comparison
of the groundwater to leachate quality. However, constituents that are typically elevated in landfill leachate (i.e.
heavy metals, BTEX, acetone, ketones) are not detected above the SWSLs at well MW-4.

4 

As proposed in the Work Plan, since new downgradient well MW-5 has indicated no confirmed VOCs above
applicable NC 2L Standards (May and November 2015 events), then the extent of VOC impact has been
considered defined on the landfill property by MW-5.

Recommendations

According to the site’s Water Quality Monitoring Plan and review of sampling field forms, well MW-4 has a total
depth of approximately 22 feet below ground surface (fbgs), indicating a screened interval from 4 to 22 fbgs
(total depth). Review of the historical water level data for MW-4 indicates water levels ranging from
approximately 11.5 to 16.5 fbgs. This shallow well, with a long screen exhibiting a partially unsaturated interval
(ranging from 7.5 to 12.5 feet), could be providing a conduit for landfill gas (gaseous phase) VOCs to partition
into the dissolved phase in groundwater. Therefore, the well construction for MW-4 may be not functioning
optimally, which may be contributing to impacts to groundwater.

The site originally requested abandoning MW-4 and replacing with well MW-5 within the First Semi-Annual 2015
Event Report (dated July 27, 2015). In response to the First Semi-Annual 2015 Event Report, NCDEQ issued
a letter dated August 20, 2015, which requested Appendix II monitoring at MW-4 during the Second Semi-
Annual 2015 event, and based on the results, the abandonment of MW-4 and the status/requirements of the
Assessment Monitoring Program would be evaluated again. During the First Semi-Annual 2015 event, no
Appendix II constituents were detected at MW-4 which are not also on the Appendix I list of constituents. During
the Second Semi-Annual 2015 event, no Appendix II constituents were detected at MW-4 which are not also
on the Appendix I list of constituents, with the exception of dichlorodifluoromethane (a common LFG
constituent). Due to the continued NC 2L Standard Appendix I organic detections and lack of confirmed
Appendix II detections at MW-4, the site again requests approval to abandon MW-4 which may be contributing
to impacts to groundwater based on the unsaturated screen interval.

The next semi-annual groundwater sampling event is tentatively scheduled for May 2016.

Should you have any questions or concerns, please contact Mr. Mike Gurley at [phone] or Steve Jett at
[phone].

Sincerely,

Steve Jett, LG #1825
Owner
Jett Environmental Consulting, PLLC (C-517)

Attachment: Figure 1 – Potentiometric Surface Map
Table 1 – Data Compared to NC Standards, Second Semi-Annual 2015 Event
Attachment A - Laboratory Analytical Report & Field Information Forms

cc: Mike Gurley, Republic Services, Inc. (PDF via Email)
Lake Norman Landfill (1 Hardcopy)
Figure
Well Gradient Status
Top of PVC
Casing
Elevation
(fmsl)1
Depth to
Water (ft)2
Groundwater
Elevation (fmsl)
MW-1 Upgradient 745.77 38.54 707.23
MW-2 Downgradient 680.37 12.06 668.31
MW-3 Downgradient 679.60 12.08 667.52
MW-4 Downgradient 680.29 14.42 665.87
MW-5 Downgradient 680.24 13.78 666.46
Note 1: Top of PVC Casing Elevations from correspondence dated 5/10/02 by S&ME, Inc.
with the exception of MW-5, which was provided by Lawrence Associates on 6/22/15.
Note 2: Depth to water measured by Analytical Services, Inc. on 11/18/15.
Groundwater Elevation Summary Table
Lake Norman Landfill
Table

Constituent Units MDL SWSL NC 2L Std MW-1 MW-2 MW-3 MW-4 MW-5
Alkalinity as CaCO3 ug/L 1000 1000 NE 95000 26000 33000 61000 141000
Antimony, Total ug/L 0.25 6 NE J 0.87 J 0.29 <6.00 <6.00 <6.00
Arsenic, Total ug/L 0.75 10 10 J 0.88 J 0.79 J 0.84 J 0.83 J 0.78
Barium, Total ug/L 0.3 100 700 J 72.6 J 91.2 J 33.4 J 19.2 J 20.8
Beryllium, Total ug/L 0.09 1 NE <1.00 <1.00 <1.00 <1.00 <1.00
Cadmium, Total ug/L 0.1 1 2 <1.00 <1.00 <1.00 <1.00 <1.00
Chloride ug/L 1000 1000 250,000 2800 7400 8000 3100 6600
Chromium, Total ug/L 0.43 10 10 <10.0 <10.0 J 1.31 <10.0 <10.0
Cobalt, Total ug/L 0.29 10 NE <10.0 J 1.72 J 4.99 J 1.13 J 0.9
Copper, Total ug/L 0.41 10 1,000 J 1.31 J 0.69 J 4.62 J 1.39 J 1.67
Cyanide, Total ug/L 10 10 70 NR NR NR <10.0 NR
Iron, Total ug/L 5.72 40 300 J 5.9 300 1540 3270 624
Lead, Total ug/L 0.08 10 15 <10.0 J 0.12 J 0.4 J 0.15 J 0.12
Manganese, Total ug/L 1.04 10 50 J 3.74 20.3 68.7 163 940
Mercury, Total ug/L 0.07 0.2 1 <0.200 <0.200 <0.200 <0.200 <0.200
Nickel, Total ug/L 0.48 50 100 <50.0 <50.0 J 1.72 <50.0 <50.0
pH (Field)su NE NE NE 6.08 5.27 5.45 5.97 6.87
Selenium, Total ug/L 0.85 10 20 <10.0 <10.0 J 0.93 <10.0 <10.0
Silver, Total ug/L 0.22 10 20 <10.0 <10.0 <10.0 <10.0 <10.0
Specific Conductance (Field)umhos/cm 1 1 NE 272 132 131 177 314
Sulfate as SO4 ug/L 5000 5000 250,000 7400 30000 <5000 <5000 <5000
Sulfide as S ug/L 200 200 NE NR NR NR <200 NR
Temperature (Field)Deg-C NE NE NE 15.4 17 15.7 16.5 16.5
Thallium, Total ug/L 0.06 5.5 NE J 0.14 <5.50 <5.50 <5.50 <5.50
Total Dissolved Solids (TDS)ug/L 10000 10000 500,000 198000 127000 102000 117000 236000
Turbidity (Field)NTU NE NE NE 1.68 2.5 7.9 4.05 4.95
Vanadium, Total ug/L 1.57 25 NE J 4.92 J 3.2 J 7.13 J 7.32 J 4.83
Zinc, Total ug/L 1.3 10 1,000 <10.0 J 1.94 J 2.38 J 1.81 J 3.63
Constituent (ug/L) Units MDL SWSL NC 2L Std MW-1 MW-2 MW-3 MW-4 MW-5
Dichlorodifluoromethane ug/L 0.5 5 1,000 NR NR NR 5.1 NR
Methylene chloride ug/L 0.6 1 5 <1.0 <1.0 <1.0 6.2 <1.0
Tetrahydrofuran ug/L 1.5 10 NE <10 <10 <10 21 <10
Trichlorofluoromethane ug/L 0.3 1 2,000 <1.0 <1.0 J 0.4 5.7 <1.0
Constituent (ug/L) Units MDL SWSL NC 2B Std SW-1 SW-2
Alkalinity as CaCO3 ug/L 1000 1000 NE 36000 18000
Antimony, Total ug/L 0.25 6 NE <6.00 <6.00
Arsenic, Total ug/L 0.75 10 10 J 0.92 J 1.11
Barium, Total ug/L 0.3 100 1,000 J 46.8 J 68.9
Beryllium, Total ug/L 0.09 1 6.5 <1.00 J 0.14
Cadmium, Total ug/L 0.1 1 2 <1.00 <1.00
Chloride ug/L 1000 1000 230,000 5100 2600
Chromium, Total ug/L 0.43 10 20 <10.0 J 2.15
Cobalt, Total ug/L 0.29 10 NE J 1.32 J 1.74
Copper, Total ug/L 0.41 10 3 J 0.63 J 5.48
Dissolved Oxygen (Field)ug/L NE NE NE 5900 4600
Iron, Total ug/L 5.72 40 1,000 1730 4480
Lead, Total ug/L 0.08 10 25 J 0.11 J 1.65
Manganese, Total ug/L 1.04 10 200 310 260
Mercury, Total ug/L 0.07 0.2 0.012 J 0.105 <0.200
Nickel, Total ug/L 0.48 50 8.3 <50.0 J 1.44
pH (Field)su NE NE NE 6.58 6.58
Selenium, Total ug/L 0.85 10 5 <10.0 <10.0
Silver, Total ug/L 0.22 10 0.06 <10.0 <10.0
Specific Conductance (Field)umhos/cm 1 1 NE 156 109
Sulfate as SO4 ug/L 5000 5000 NE 5600 10000
Temperature (Field)Deg-C NE NE NE 16.6 14.9
Thallium, Total ug/L 0.06 5.5 NE <5.50 <5.50
Total Dissolved Solids (TDS)ug/L 10000 10000 NE 123000 153000
Turbidity (Field)NTU NE NE NE 6.95 27
Vanadium, Total ug/L 1.57 25 NE J 3.72 J 15.8
Zinc, Total ug/L 1.3 10 50 J 5.2 14.7
NR: Denotes this Appendix II parameter Not Required to be sampled at this well during this event.
NE: Denotes a NC 2L or 2B Standard is not established.
Only the VOCs detected during this event are displayed on the table.
J: Denotes Sample result above the MDL but below the SWSL; estimated value; value may not be accurate.
Denotes result above an SWSL is also above the NC 2L or 2B Standard:
For NC 2B Standard, lowest value utilized from the classifications from the 2B Table published May 15, 2013.
TABLE 1
SECOND SEMI-ANNUAL 2015 EVENT DATA COMPARED TO NC STANDARDS
LAKE NORMAN C&D LANDFILL
GROUNDWATER SAMPLES
SURFACE WATER SAMPLES
Attachment A
Laboratory Analytical Report
&
Field Information Forms

ASI ANALYTICAL SERVICES, INC.
Environmental Monitoring & Laboratory Analysis
110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
BFI Waste Systems of North America, LLC
Project: Lake Norman C&D Landfill
Concord, NC 28027
5105 Morehead Rd.
Mr. Mike Gurley
We appreciate the opportunity to provide the analytical support for your project. The analytical results in this report are based upon information supplied by you, the
client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Analytical Services, Inc. certifies that the
following analytical results meet all requirements of the National Environmental Laboratory Accreditation Conference(NELAC).All test results relate only to the samples
analyzed.
Laboratory Report
Project #:[none]
Prepared For:
Attention:
December 08, 2015
Report Number:AYK0618
Approved:
This report may not be reproduced, except in full, without written approval from Analytical Services, Inc.Page 1 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Sample ID Laboratory ID Matrix Date Sampled
ANALYTICAL REPORT FOR SAMPLES
Date Received
5504-MW1 AYK0618-01 11/18/15 13:35 11/19/15 15:09Ground Water
5504-MW2 AYK0618-02 11/18/15 14:05 11/19/15 15:09Ground Water
5504-MW3 AYK0618-03 11/18/15 14:34 11/19/15 15:09Ground Water
5504-MW4 AYK0618-04 11/18/15 15:04 11/19/15 15:09Ground Water
5504-MW5 AYK0618-05 11/18/15 16:00 11/19/15 15:09Ground Water
5504-MW5 AYK0618-06 11/19/15 09:20 11/19/15 15:09Ground Water
5504-Duplicate AYK0618-07 11/18/15 00:00 11/19/15 15:09Ground Water
5504-Duplicate AYK0618-08 11/19/15 00:00 11/19/15 15:09Ground Water
5504-Field Blank AYK0618-09 11/18/15 14:07 11/19/15 15:09Water
5504-Equipment Blank AYK0618-10 11/18/15 15:20 11/19/15 15:09Water
5504-Trip Blank AYK0618-11 11/18/15 00:00 11/19/15 15:09Water
5504-SW1 AYK0618-12 11/18/15 15:46 11/19/15 15:09Surface Water
5504-SW2 AYK0618-13 11/19/15 08:50 11/19/15 15:09Surface Water
Page 2 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte
SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW1
Ground Water
AYK0618-01 AYK061811/18/15 13:35
Project:Lake Norman C&D Landfill
11/19/15 15:09
On Site
EPA 9050A 272 umhos/cm1Field - Specific Conductance 1 5110542NA1COND11/18/15 13:3511/18/15 13:35
EPA 9040C 6.08 pH Units1Field - pH 5110542NAPH11/18/15 13:3511/18/15 13:35
SM 2550 B 15.4 °C1Field - Temperature 5110542NATEMP11/18/15 13:3511/18/15 13:35
EPA 180.1 1.68 NTU1Field - Turbidity 5110542NATURB11/18/15 13:3511/18/15 13:35
NA 38.54 feet1Field - Water Level 5110542NAWL11/18/15 13:3511/18/15 13:35
General Chemistry
SM 2320 B 95000 ug/L1Alkalinity as CaCO3 1000 5110597SM 2320 B 1000 ALK 11/30/15 10:4511/30/15 10:45
SM 2540 C 198000 ug/L1Total Dissolved Solids 10000 5110550SM 2540 C 10000 E-10173 11/25/15 12:3011/25/15 12:30
Inorganic Anions
EPA 9056A 2800 ug/L1Chloride1000 5110537EPA 9056A 1000 16887-00-6 11/24/15 16:1711/24/15 16:17
EPA 9056A 7400 ug/L1Sulfate5000 5110537EPA 9056A 5000 14808-79-8 11/24/15 16:1711/24/15 16:17
Metals, Total
EPA 6020A 0.87 ug/L1Antimony6.00 J 5120028EPA 3005A 0.25 7440-36-0 12/02/15 17:4612/02/15 09:15
EPA 6020A 0.88 ug/L1Arsenic10.0 J 5120028EPA 3005A 0.75 7440-38-2 12/02/15 17:4612/02/15 09:15
EPA 6020A 72.6 ug/L1Barium100 J 5120028EPA 3005A 0.30 7440-39-3 12/02/15 17:4612/02/15 09:15
NDEPA 6020A ug/L1Beryllium1.00 5120028EPA 3005A 0.09 7440-41-7 12/02/15 17:4612/02/15 09:15
NDEPA 6020A ug/L1Cadmium1.00 5120028EPA 3005A 0.10 7440-43-9 12/02/15 17:4612/02/15 09:15
NDEPA 6020A ug/L1Chromium10.0 5120028EPA 3005A 0.43 7440-47-3 12/02/15 17:4612/02/15 09:15
NDEPA 6020A ug/L1Cobalt10.0 5120028EPA 3005A 0.29 7440-48-4 12/02/15 17:4612/02/15 09:15
Page 3 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW1
Ground Water
AYK0618-01 AYK061811/18/15 13:35
Project:Lake Norman C&D Landfill
11/19/15 15:09
Metals, Total
EPA 6020A 1.31 ug/L1Copper10.0 J 5120028EPA 3005A 0.41 7440-50-8 12/02/15 17:4612/02/15 09:15
NDEPA 6020A ug/L1Lead10.0 5120028EPA 3005A 0.08 7439-92-1 12/02/15 17:4612/02/15 09:15
NDEPA 6020A ug/L1Nickel50.0 5120028EPA 3005A 0.48 7440-02-0 12/02/15 17:4612/02/15 09:15
NDEPA 6020A ug/L1Selenium10.0 5120028EPA 3005A 0.85 7782-49-2 12/02/15 17:4612/02/15 09:15
NDEPA 6020A ug/L1Silver10.0 5120028EPA 3005A 0.22 7440-22-4 12/02/15 17:4612/02/15 09:15
EPA 6020A 0.14 ug/L1Thallium5.50 J 5120028EPA 3005A 0.06 7440-28-0 12/02/15 17:4612/02/15 09:15
EPA 6020A 4.92 ug/L1Vanadium25.0 J 5120028EPA 3005A 1.57 7440-62-2 12/02/15 17:4612/02/15 09:15
NDEPA 6020A ug/L1Zinc10.0 5120028EPA 3005A 1.30 7440-66-6 12/02/15 17:4612/02/15 09:15
EPA 6020A 5.90 ug/L1Iron40.0 J 5120028EPA 3005A 5.72 7439-89-6 12/02/15 17:4612/02/15 09:15
EPA 6020A 3.74 ug/L1Manganese10.0 J 5120028EPA 3005A 1.04 7439-96-5 12/02/15 17:4612/02/15 09:15
NDEPA 7470A ug/L1Mercury0.200 5110582EPA 7470A 0.070 7439-97-6 11/30/15 13:3811/30/15 08:20
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 5110457EPA 5030B 3.1 67-64-1 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Acrylonitrile200 5110457EPA 5030B 2.0 107-13-1 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Benzene1.0 5110457EPA 5030B 0.2 71-43-2 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Bromochloromethane3.0 5110457EPA 5030B 0.5 74-97-5 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 5110457EPA 5030B 0.5 75-27-4 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Bromoform3.0 5110457EPA 5030B 0.5 75-25-2 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Bromomethane10 5110457EPA 5030B 0.8 74-83-9 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Carbon Disulfide 100 5110457EPA 5030B 0.5 75-15-0 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 5110457EPA 5030B 0.4 56-23-5 11/20/15 10:1211/20/15 10:00
Page 4 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW1
Ground Water
AYK0618-01 AYK061811/18/15 13:35
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Chlorobenzene3.0 5110457EPA 5030B 0.5 108-90-7 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Chloroethane10 5110457EPA 5030B 0.6 75-00-3 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Chloroform5.0 5110457EPA 5030B 0.4 67-66-3 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Chloromethane1.0 5110457EPA 5030B 0.6 74-87-3 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Dibromochloromethane1.0 5110457EPA 5030B 0.3 124-48-1 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 5110457EPA 5030B 1.0 96-12-8 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 5110457EPA 5030B 0.4 106-93-4 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Dibromomethane10 5110457EPA 5030B 0.4 74-95-3 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 5110457EPA 5030B 0.2 95-50-1 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 5110457EPA 5030B 0.4 106-46-7 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 5110457EPA 5030B 1.1 110-57-6 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 5110457EPA 5030B 0.3 75-34-3 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 5110457EPA 5030B 0.3 107-06-2 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 5110457EPA 5030B 0.6 75-35-4 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.3 156-59-2 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.4 156-60-5 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 5110457EPA 5030B 0.4 78-87-5 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-01-5 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-02-6 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Ethylbenzene1.0 5110457EPA 5030B 0.2 100-41-4 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Iodomethane10 5110457EPA 5030B 1.7 74-88-4 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 5110457EPA 5030B 0.7 591-78-6 11/20/15 10:1211/20/15 10:00
Page 5 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW1
Ground Water
AYK0618-01 AYK061811/18/15 13:35
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Methylene Chloride 1.0 5110457EPA 5030B 0.6 75-09-2 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 5110457EPA 5030B 0.9 78-93-3 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)50 5110457EPA 5030B 1.0 108-10-1 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Styrene1.0 5110457EPA 5030B 0.3 100-42-5 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 5110457EPA 5030B 0.4 630-20-6 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 5110457EPA 5030B 0.5 79-34-5 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 5110457EPA 5030B 0.4 127-18-4 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Toluene1.0 5110457EPA 5030B 0.2 108-88-3 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 5110457EPA 5030B 0.3 71-55-6 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 5110457EPA 5030B 0.4 79-00-5 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Trichloroethene1.0 5110457EPA 5030B 0.4 79-01-6 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 5110457EPA 5030B 0.3 75-69-4 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 5110457EPA 5030B 0.3 96-18-4 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Vinyl Acetate 50 5110457EPA 5030B 0.6 108-05-4 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 5110457EPA 5030B 0.4 75-01-4 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Xylenes, total 4.0 5110457EPA 5030B 0.6 1330-20-7 11/20/15 10:1211/20/15 10:00
NDEPA 8260B ug/L1Tetrahydrofuran10 5110457EPA 5030B 1.5 109-99-9 11/20/15 10:1211/20/15 10:00
EPA 8260B 101 %Surr: Dibromofluoromethane 5110457EPA 5030B 1868-53-7 11/20/15 10:1211/20/15 10:0080-120
EPA 8260B 116 %Surr: 1,2-Dichloroethane-d4 5110457EPA 5030B 17060-07-0 11/20/15 10:1211/20/15 10:0078-120
EPA 8260B 98 %Surr: Toluene-d8 5110457EPA 5030B 2037-26-5 11/20/15 10:1211/20/15 10:0080-120
EPA 8260B 101 %Surr: 4-Bromofluorobenzene 5110457EPA 5030B 460-00-4 11/20/15 10:1211/20/15 10:0080-120
Page 6 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW2
Ground Water
AYK0618-02 AYK061811/18/15 14:05
Project:Lake Norman C&D Landfill
11/19/15 15:09
On Site
EPA 9050A 132 umhos/cm1Field - Specific Conductance 1 5110542NA1COND11/18/15 14:0511/18/15 14:05
EPA 9040C 5.27 pH Units1Field - pH 5110542NAPH11/18/15 14:0511/18/15 14:05
SM 2550 B 17.0 °C1Field - Temperature 5110542NATEMP11/18/15 14:0511/18/15 14:05
EPA 180.1 2.50 NTU1Field - Turbidity 5110542NATURB11/18/15 14:0511/18/15 14:05
NA 12.06 feet1Field - Water Level 5110542NAWL11/18/15 14:0511/18/15 14:05
General Chemistry
SM 2320 B 26000 ug/L1Alkalinity as CaCO3 1000 5110597SM 2320 B 1000 ALK 11/30/15 10:4511/30/15 10:45
SM 2540 C 127000 ug/L1Total Dissolved Solids 10000 5110550SM 2540 C 10000 E-10173 11/25/15 12:3011/25/15 12:30
Inorganic Anions
EPA 9056A 7400 ug/L1Chloride1000 5110537EPA 9056A 1000 16887-00-6 11/24/15 16:3811/24/15 16:38
EPA 9056A 30000 ug/L1Sulfate5000 5110537EPA 9056A 5000 14808-79-8 11/24/15 16:3811/24/15 16:38
Metals, Total
EPA 6020A 0.29 ug/L1Antimony6.00 J 5120028EPA 3005A 0.25 7440-36-0 12/02/15 17:5112/02/15 09:15
EPA 6020A 0.79 ug/L1Arsenic10.0 J 5120028EPA 3005A 0.75 7440-38-2 12/02/15 17:5112/02/15 09:15
EPA 6020A 91.2 ug/L1Barium100 J 5120028EPA 3005A 0.30 7440-39-3 12/02/15 17:5112/02/15 09:15
NDEPA 6020A ug/L1Beryllium1.00 5120028EPA 3005A 0.09 7440-41-7 12/02/15 17:5112/02/15 09:15
NDEPA 6020A ug/L1Cadmium1.00 5120028EPA 3005A 0.10 7440-43-9 12/02/15 17:5112/02/15 09:15
NDEPA 6020A ug/L1Chromium10.0 5120028EPA 3005A 0.43 7440-47-3 12/02/15 17:5112/02/15 09:15
EPA 6020A 1.72 ug/L1Cobalt10.0 J 5120028EPA 3005A 0.29 7440-48-4 12/02/15 17:5112/02/15 09:15
Page 7 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW2
Ground Water
AYK0618-02 AYK061811/18/15 14:05
Project:Lake Norman C&D Landfill
11/19/15 15:09
Metals, Total
EPA 6020A 0.69 ug/L1Copper10.0 J 5120028EPA 3005A 0.41 7440-50-8 12/02/15 17:5112/02/15 09:15
EPA 6020A 0.12 ug/L1Lead10.0 J 5120028EPA 3005A 0.08 7439-92-1 12/02/15 17:5112/02/15 09:15
NDEPA 6020A ug/L1Nickel50.0 5120028EPA 3005A 0.48 7440-02-0 12/02/15 17:5112/02/15 09:15
NDEPA 6020A ug/L1Selenium10.0 5120028EPA 3005A 0.85 7782-49-2 12/02/15 17:5112/02/15 09:15
NDEPA 6020A ug/L1Silver10.0 5120028EPA 3005A 0.22 7440-22-4 12/02/15 17:5112/02/15 09:15
NDEPA 6020A ug/L1Thallium5.50 5120028EPA 3005A 0.06 7440-28-0 12/02/15 17:5112/02/15 09:15
EPA 6020A 3.20 ug/L1Vanadium25.0 J 5120028EPA 3005A 1.57 7440-62-2 12/02/15 17:5112/02/15 09:15
EPA 6020A 1.94 ug/L1Zinc10.0 J 5120028EPA 3005A 1.30 7440-66-6 12/02/15 17:5112/02/15 09:15
EPA 6020A 300 ug/L1Iron40.0 5120028EPA 3005A 5.72 7439-89-6 12/02/15 17:5112/02/15 09:15
EPA 6020A 20.3 ug/L1Manganese10.0 5120028EPA 3005A 1.04 7439-96-5 12/02/15 17:5112/02/15 09:15
NDEPA 7470A ug/L1Mercury0.200 5110582EPA 7470A 0.070 7439-97-6 11/30/15 13:4011/30/15 08:20
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 5110457EPA 5030B 3.1 67-64-1 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Acrylonitrile200 5110457EPA 5030B 2.0 107-13-1 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Benzene1.0 5110457EPA 5030B 0.2 71-43-2 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Bromochloromethane3.0 5110457EPA 5030B 0.5 74-97-5 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 5110457EPA 5030B 0.5 75-27-4 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Bromoform3.0 5110457EPA 5030B 0.5 75-25-2 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Bromomethane10 5110457EPA 5030B 0.8 74-83-9 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Carbon Disulfide 100 5110457EPA 5030B 0.5 75-15-0 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 5110457EPA 5030B 0.4 56-23-5 11/20/15 10:3811/20/15 10:00
Page 8 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW2
Ground Water
AYK0618-02 AYK061811/18/15 14:05
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Chlorobenzene3.0 5110457EPA 5030B 0.5 108-90-7 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Chloroethane10 5110457EPA 5030B 0.6 75-00-3 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Chloroform5.0 5110457EPA 5030B 0.4 67-66-3 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Chloromethane1.0 5110457EPA 5030B 0.6 74-87-3 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Dibromochloromethane1.0 5110457EPA 5030B 0.3 124-48-1 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 5110457EPA 5030B 1.0 96-12-8 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 5110457EPA 5030B 0.4 106-93-4 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Dibromomethane10 5110457EPA 5030B 0.4 74-95-3 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 5110457EPA 5030B 0.2 95-50-1 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 5110457EPA 5030B 0.4 106-46-7 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 5110457EPA 5030B 1.1 110-57-6 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 5110457EPA 5030B 0.3 75-34-3 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 5110457EPA 5030B 0.3 107-06-2 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 5110457EPA 5030B 0.6 75-35-4 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.3 156-59-2 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.4 156-60-5 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 5110457EPA 5030B 0.4 78-87-5 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-01-5 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-02-6 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Ethylbenzene1.0 5110457EPA 5030B 0.2 100-41-4 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Iodomethane10 5110457EPA 5030B 1.7 74-88-4 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 5110457EPA 5030B 0.7 591-78-6 11/20/15 10:3811/20/15 10:00
Page 9 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW2
Ground Water
AYK0618-02 AYK061811/18/15 14:05
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Methylene Chloride 1.0 5110457EPA 5030B 0.6 75-09-2 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 5110457EPA 5030B 0.9 78-93-3 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)50 5110457EPA 5030B 1.0 108-10-1 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Styrene1.0 5110457EPA 5030B 0.3 100-42-5 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 5110457EPA 5030B 0.4 630-20-6 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 5110457EPA 5030B 0.5 79-34-5 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 5110457EPA 5030B 0.4 127-18-4 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Toluene1.0 5110457EPA 5030B 0.2 108-88-3 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 5110457EPA 5030B 0.3 71-55-6 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 5110457EPA 5030B 0.4 79-00-5 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Trichloroethene1.0 5110457EPA 5030B 0.4 79-01-6 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 5110457EPA 5030B 0.3 75-69-4 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 5110457EPA 5030B 0.3 96-18-4 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Vinyl Acetate 50 5110457EPA 5030B 0.6 108-05-4 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 5110457EPA 5030B 0.4 75-01-4 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Xylenes, total 4.0 5110457EPA 5030B 0.6 1330-20-7 11/20/15 10:3811/20/15 10:00
NDEPA 8260B ug/L1Tetrahydrofuran10 5110457EPA 5030B 1.5 109-99-9 11/20/15 10:3811/20/15 10:00
EPA 8260B 103 %Surr: Dibromofluoromethane 5110457EPA 5030B 1868-53-7 11/20/15 10:3811/20/15 10:0080-120
EPA 8260B 115 %Surr: 1,2-Dichloroethane-d4 5110457EPA 5030B 17060-07-0 11/20/15 10:3811/20/15 10:0078-120
EPA 8260B 98 %Surr: Toluene-d8 5110457EPA 5030B 2037-26-5 11/20/15 10:3811/20/15 10:0080-120
EPA 8260B 103 %Surr: 4-Bromofluorobenzene 5110457EPA 5030B 460-00-4 11/20/15 10:3811/20/15 10:0080-120
Page 10 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW3
Ground Water
AYK0618-03 AYK061811/18/15 14:34
Project:Lake Norman C&D Landfill
11/19/15 15:09
On Site
EPA 9050A 131 umhos/cm1Field - Specific Conductance 1 5110542NA1COND11/18/15 14:3411/18/15 14:34
EPA 9040C 5.45 pH Units1Field - pH 5110542NAPH11/18/15 14:3411/18/15 14:34
SM 2550 B 15.7 °C1Field - Temperature 5110542NATEMP11/18/15 14:3411/18/15 14:34
EPA 180.1 7.90 NTU1Field - Turbidity 5110542NATURB11/18/15 14:3411/18/15 14:34
NA 12.08 feet1Field - Water Level 5110542NAWL11/18/15 14:3411/18/15 14:34
General Chemistry
SM 2320 B 33000 ug/L1Alkalinity as CaCO3 1000 5110597SM 2320 B 1000 ALK 11/30/15 10:4511/30/15 10:45
SM 2540 C 102000 ug/L1Total Dissolved Solids 10000 5110550SM 2540 C 10000 E-10173 11/25/15 12:3011/25/15 12:30
Inorganic Anions
EPA 9056A 8000 ug/L1Chloride1000 5110537EPA 9056A 1000 16887-00-6 11/24/15 16:5811/24/15 16:58
NDEPA 9056A ug/L1Sulfate5000 5110537EPA 9056A 5000 14808-79-8 11/24/15 16:5811/24/15 16:58
Metals, Total
NDEPA 6020A ug/L1Antimony6.00 5120028EPA 3005A 0.25 7440-36-0 12/02/15 17:5612/02/15 09:15
EPA 6020A 0.84 ug/L1Arsenic10.0 J 5120028EPA 3005A 0.75 7440-38-2 12/02/15 17:5612/02/15 09:15
EPA 6020A 33.4 ug/L1Barium100 J 5120028EPA 3005A 0.30 7440-39-3 12/02/15 17:5612/02/15 09:15
NDEPA 6020A ug/L1Beryllium1.00 5120028EPA 3005A 0.09 7440-41-7 12/02/15 17:5612/02/15 09:15
NDEPA 6020A ug/L1Cadmium1.00 5120028EPA 3005A 0.10 7440-43-9 12/02/15 17:5612/02/15 09:15
EPA 6020A 1.31 ug/L1Chromium10.0 J 5120028EPA 3005A 0.43 7440-47-3 12/02/15 17:5612/02/15 09:15
EPA 6020A 4.99 ug/L1Cobalt10.0 J 5120028EPA 3005A 0.29 7440-48-4 12/02/15 17:5612/02/15 09:15
Page 11 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW3
Ground Water
AYK0618-03 AYK061811/18/15 14:34
Project:Lake Norman C&D Landfill
11/19/15 15:09
Metals, Total
EPA 6020A 4.62 ug/L1Copper10.0 J 5120028EPA 3005A 0.41 7440-50-8 12/02/15 17:5612/02/15 09:15
EPA 6020A 0.40 ug/L1Lead10.0 J 5120028EPA 3005A 0.08 7439-92-1 12/02/15 17:5612/02/15 09:15
EPA 6020A 1.72 ug/L1Nickel50.0 J 5120028EPA 3005A 0.48 7440-02-0 12/02/15 17:5612/02/15 09:15
EPA 6020A 0.93 ug/L1Selenium10.0 J 5120028EPA 3005A 0.85 7782-49-2 12/02/15 17:5612/02/15 09:15
NDEPA 6020A ug/L1Silver10.0 5120028EPA 3005A 0.22 7440-22-4 12/02/15 17:5612/02/15 09:15
NDEPA 6020A ug/L1Thallium5.50 5120028EPA 3005A 0.06 7440-28-0 12/02/15 17:5612/02/15 09:15
EPA 6020A 7.13 ug/L1Vanadium25.0 J 5120028EPA 3005A 1.57 7440-62-2 12/02/15 17:5612/02/15 09:15
EPA 6020A 2.38 ug/L1Zinc10.0 J 5120028EPA 3005A 1.30 7440-66-6 12/02/15 17:5612/02/15 09:15
EPA 6020A 1540 ug/L1Iron40.0 5120028EPA 3005A 5.72 7439-89-6 12/02/15 17:5612/02/15 09:15
EPA 6020A 68.7 ug/L1Manganese10.0 5120028EPA 3005A 1.04 7439-96-5 12/02/15 17:5612/02/15 09:15
NDEPA 7470A ug/L1Mercury0.200 5110582EPA 7470A 0.070 7439-97-6 11/30/15 13:4711/30/15 08:20
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 5110457EPA 5030B 3.1 67-64-1 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Acrylonitrile200 5110457EPA 5030B 2.0 107-13-1 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Benzene1.0 5110457EPA 5030B 0.2 71-43-2 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Bromochloromethane3.0 5110457EPA 5030B 0.5 74-97-5 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 5110457EPA 5030B 0.5 75-27-4 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Bromoform3.0 5110457EPA 5030B 0.5 75-25-2 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Bromomethane10 5110457EPA 5030B 0.8 74-83-9 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Carbon Disulfide 100 5110457EPA 5030B 0.5 75-15-0 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 5110457EPA 5030B 0.4 56-23-5 11/20/15 11:0411/20/15 10:00
Page 12 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW3
Ground Water
AYK0618-03 AYK061811/18/15 14:34
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Chlorobenzene3.0 5110457EPA 5030B 0.5 108-90-7 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Chloroethane10 5110457EPA 5030B 0.6 75-00-3 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Chloroform5.0 5110457EPA 5030B 0.4 67-66-3 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Chloromethane1.0 5110457EPA 5030B 0.6 74-87-3 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Dibromochloromethane1.0 5110457EPA 5030B 0.3 124-48-1 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 5110457EPA 5030B 1.0 96-12-8 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 5110457EPA 5030B 0.4 106-93-4 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Dibromomethane10 5110457EPA 5030B 0.4 74-95-3 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 5110457EPA 5030B 0.2 95-50-1 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 5110457EPA 5030B 0.4 106-46-7 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 5110457EPA 5030B 1.1 110-57-6 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 5110457EPA 5030B 0.3 75-34-3 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 5110457EPA 5030B 0.3 107-06-2 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 5110457EPA 5030B 0.6 75-35-4 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.3 156-59-2 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.4 156-60-5 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 5110457EPA 5030B 0.4 78-87-5 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-01-5 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-02-6 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Ethylbenzene1.0 5110457EPA 5030B 0.2 100-41-4 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Iodomethane10 5110457EPA 5030B 1.7 74-88-4 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 5110457EPA 5030B 0.7 591-78-6 11/20/15 11:0411/20/15 10:00
Page 13 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW3
Ground Water
AYK0618-03 AYK061811/18/15 14:34
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Methylene Chloride 1.0 5110457EPA 5030B 0.6 75-09-2 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 5110457EPA 5030B 0.9 78-93-3 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)50 5110457EPA 5030B 1.0 108-10-1 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Styrene1.0 5110457EPA 5030B 0.3 100-42-5 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 5110457EPA 5030B 0.4 630-20-6 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 5110457EPA 5030B 0.5 79-34-5 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 5110457EPA 5030B 0.4 127-18-4 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Toluene1.0 5110457EPA 5030B 0.2 108-88-3 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 5110457EPA 5030B 0.3 71-55-6 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 5110457EPA 5030B 0.4 79-00-5 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Trichloroethene1.0 5110457EPA 5030B 0.4 79-01-6 11/20/15 11:0411/20/15 10:00
EPA 8260B 0.4 ug/L1Trichlorofluoromethane1.0 J 5110457EPA 5030B 0.3 75-69-4 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 5110457EPA 5030B 0.3 96-18-4 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Vinyl Acetate 50 5110457EPA 5030B 0.6 108-05-4 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 5110457EPA 5030B 0.4 75-01-4 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Xylenes, total 4.0 5110457EPA 5030B 0.6 1330-20-7 11/20/15 11:0411/20/15 10:00
NDEPA 8260B ug/L1Tetrahydrofuran10 5110457EPA 5030B 1.5 109-99-9 11/20/15 11:0411/20/15 10:00
EPA 8260B 103 %Surr: Dibromofluoromethane 5110457EPA 5030B 1868-53-7 11/20/15 11:0411/20/15 10:0080-120
EPA 8260B 120 %Surr: 1,2-Dichloroethane-d4 5110457EPA 5030B 17060-07-0 11/20/15 11:0411/20/15 10:0078-120
EPA 8260B 97 %Surr: Toluene-d8 5110457EPA 5030B 2037-26-5 11/20/15 11:0411/20/15 10:0080-120
EPA 8260B 104 %Surr: 4-Bromofluorobenzene 5110457EPA 5030B 460-00-4 11/20/15 11:0411/20/15 10:0080-120
Page 14 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW4
Ground Water
AYK0618-04 AYK061811/18/15 15:04
Project:Lake Norman C&D Landfill
11/19/15 15:09
On Site
EPA 9050A 177 umhos/cm1Field - Specific Conductance 1 5110542NA1COND11/18/15 15:0411/18/15 15:04
EPA 9040C 5.97 pH Units1Field - pH 5110542NAPH11/18/15 15:0411/18/15 15:04
SM 2550 B 16.5 °C1Field - Temperature 5110542NATEMP11/18/15 15:0411/18/15 15:04
EPA 180.1 4.05 NTU1Field - Turbidity 5110542NATURB11/18/15 15:0411/18/15 15:04
NA 14.42 feet1Field - Water Level 5110542NAWL11/18/15 15:0411/18/15 15:04
General Chemistry
SM 2320 B 61000 ug/L1Alkalinity as CaCO3 1000 5110597SM 2320 B 1000 ALK 11/30/15 10:4511/30/15 10:45
NDEPA 9010/9014 ug/L1Cyanide, Total 10.0 5110601EPA 9010 10.0 57-12-5 11/30/15 16:0511/30/15 13:00
NDSM 4500-S D ug/L1Total Sulfide 200 5110534SM 4500-S D 200 18496-25-8 11/24/15 13:3011/24/15 13:30
SM 2540 C 117000 ug/L1Total Dissolved Solids 10000 5110550SM 2540 C 10000 E-10173 11/25/15 12:3011/25/15 12:30
Inorganic Anions
EPA 9056A 3100 ug/L1Chloride1000 5110537EPA 9056A 1000 16887-00-6 11/24/15 17:1911/24/15 17:19
NDEPA 9056A ug/L1Sulfate5000 5110537EPA 9056A 5000 14808-79-8 11/24/15 17:1911/24/15 17:19
Metals, Total
NDEPA 6020A ug/L1Antimony6.00 5120028EPA 3005A 0.25 7440-36-0 12/02/15 18:0112/02/15 09:15
EPA 6020A 0.83 ug/L1Arsenic10.0 J 5120028EPA 3005A 0.75 7440-38-2 12/02/15 18:0112/02/15 09:15
EPA 6020A 19.2 ug/L1Barium100 J 5120028EPA 3005A 0.30 7440-39-3 12/02/15 18:0112/02/15 09:15
NDEPA 6020A ug/L1Beryllium1.00 5120028EPA 3005A 0.09 7440-41-7 12/02/15 18:0112/02/15 09:15
NDEPA 6020A ug/L1Cadmium1.00 5120028EPA 3005A 0.10 7440-43-9 12/02/15 18:0112/02/15 09:15
Page 15 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW4
Ground Water
AYK0618-04 AYK061811/18/15 15:04
Project:Lake Norman C&D Landfill
11/19/15 15:09
Metals, Total
NDEPA 6020A ug/L1Chromium10.0 5120028EPA 3005A 0.43 7440-47-3 12/02/15 18:0112/02/15 09:15
EPA 6020A 1.13 ug/L1Cobalt10.0 J 5120028EPA 3005A 0.29 7440-48-4 12/02/15 18:0112/02/15 09:15
EPA 6020A 1.39 ug/L1Copper10.0 J 5120028EPA 3005A 0.41 7440-50-8 12/02/15 18:0112/02/15 09:15
EPA 6020A 0.15 ug/L1Lead10.0 J 5120028EPA 3005A 0.08 7439-92-1 12/02/15 18:0112/02/15 09:15
NDEPA 6020A ug/L1Nickel50.0 5120028EPA 3005A 0.48 7440-02-0 12/02/15 18:0112/02/15 09:15
NDEPA 6020A ug/L1Selenium10.0 5120028EPA 3005A 0.85 7782-49-2 12/02/15 18:0112/02/15 09:15
NDEPA 6020A ug/L1Silver10.0 5120028EPA 3005A 0.22 7440-22-4 12/02/15 18:0112/02/15 09:15
NDEPA 6020A ug/L1Thallium5.50 5120028EPA 3005A 0.06 7440-28-0 12/02/15 18:0112/02/15 09:15
EPA 6020A 7.32 ug/L1Vanadium25.0 J 5120028EPA 3005A 1.57 7440-62-2 12/02/15 18:0112/02/15 09:15
EPA 6020A 1.81 ug/L1Zinc10.0 J 5120028EPA 3005A 1.30 7440-66-6 12/02/15 18:0112/02/15 09:15
EPA 6020A 3270 ug/L1Iron40.0 5120028EPA 3005A 5.72 7439-89-6 12/02/15 18:0112/02/15 09:15
EPA 6020A 163 ug/L1Manganese10.0 5120028EPA 3005A 1.04 7439-96-5 12/02/15 18:0112/02/15 09:15
NDEPA 7470A ug/L1Mercury0.200 5110582EPA 7470A 0.070 7439-97-6 11/30/15 13:4911/30/15 08:20
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 5110457EPA 5030B 3.1 67-64-1 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Acetonitrile55 5110457EPA 5030B 1.9 75-05-8 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Acrolein53 5110457EPA 5030B 1.8 107-02-8 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Acrylonitrile200 5110457EPA 5030B 2.0 107-13-1 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Benzene1.0 5110457EPA 5030B 0.2 71-43-2 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Bromochloromethane3.0 5110457EPA 5030B 0.5 74-97-5 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 5110457EPA 5030B 0.5 75-27-4 11/20/15 11:3011/20/15 10:00
Page 16 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW4
Ground Water
AYK0618-04 AYK061811/18/15 15:04
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Bromoform3.0 5110457EPA 5030B 0.5 75-25-2 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Bromomethane10 5110457EPA 5030B 0.8 74-83-9 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Carbon Disulfide 100 5110457EPA 5030B 0.5 75-15-0 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 5110457EPA 5030B 0.4 56-23-5 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Chlorobenzene3.0 5110457EPA 5030B 0.5 108-90-7 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Chloroprene
(2-Chloro-1,3-butadiene)20 5110457EPA 5030B 0.5 126-99-8 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Chloroethane10 5110457EPA 5030B 0.6 75-00-3 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Chloroform5.0 5110457EPA 5030B 0.4 67-66-3 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Chloromethane1.0 5110457EPA 5030B 0.6 74-87-3 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Allyl Chloride
(3-Chloropropylene)10 5110457EPA 5030B 1.0 107-05-1 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Dibromochloromethane3.0 5110457EPA 5030B 0.3 124-48-1 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 5110457EPA 5030B 1.0 96-12-8 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 5110457EPA 5030B 0.4 106-93-4 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Dibromomethane10 5110457EPA 5030B 0.4 74-95-3 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 5110457EPA 5030B 0.2 95-50-1 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L11,3-Dichlorobenzene 5.0 5110457EPA 5030B 0.3 541-73-1 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 5110457EPA 5030B 0.4 106-46-7 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 5110457EPA 5030B 1.1 110-57-6 11/20/15 11:3011/20/15 10:00
EPA 8260B 5.1 ug/L1Dichlorodifluoromethane5.0 5110457EPA 5030B 0.5 75-71-8 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 5110457EPA 5030B 0.3 75-34-3 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 5110457EPA 5030B 0.3 107-06-2 11/20/15 11:3011/20/15 10:00
Page 17 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW4
Ground Water
AYK0618-04 AYK061811/18/15 15:04
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 5110457EPA 5030B 0.6 75-35-4 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.3 156-59-2 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.4 156-60-5 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 5110457EPA 5030B 0.4 78-87-5 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L11,3-Dichloropropane 1.0 5110457EPA 5030B 0.4 142-28-9 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L12,2-Dichloropropane 15 5110457EPA 5030B 0.5 594-20-7 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloropropene 5.0 5110457EPA 5030B 0.3 563-58-6 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-01-5 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-02-6 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Ethylbenzene1.0 5110457EPA 5030B 0.2 100-41-4 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Propionitrile (Ethyl Cyanide)150 5110457EPA 5030B 1.4 107-12-0 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Ethyl Methacrylate 10 5110457EPA 5030B 0.5 97-63-2 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Iodomethane10 5110457EPA 5030B 1.7 74-88-4 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Isobutyl Alcohol 100 5110457EPA 5030B 18 78-83-1 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Methacrylonitrile100 5110457EPA 5030B 1.6 126-98-7 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 5110457EPA 5030B 0.7 591-78-6 11/20/15 11:3011/20/15 10:00
EPA 8260B 6.2 ug/L1Methylene Chloride 1.0 5110457EPA 5030B 0.6 75-09-2 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 5110457EPA 5030B 0.9 78-93-3 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Methyl Methacrylate 30 5110457EPA 5030B 0.4 80-62-6 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)100 5110457EPA 5030B 1.0 108-10-1 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Styrene1.0 5110457EPA 5030B 0.3 100-42-5 11/20/15 11:3011/20/15 10:00
Page 18 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW4
Ground Water
AYK0618-04 AYK061811/18/15 15:04
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 5110457EPA 5030B 0.4 630-20-6 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 3.0 5110457EPA 5030B 0.5 79-34-5 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 5110457EPA 5030B 0.4 127-18-4 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Toluene1.0 5110457EPA 5030B 0.2 108-88-3 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 5110457EPA 5030B 0.3 71-55-6 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 5110457EPA 5030B 0.4 79-00-5 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Trichloroethene1.0 5110457EPA 5030B 0.4 79-01-6 11/20/15 11:3011/20/15 10:00
EPA 8260B 5.7 ug/L1Trichlorofluoromethane1.0 5110457EPA 5030B 0.3 75-69-4 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 5110457EPA 5030B 0.3 96-18-4 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Vinyl Acetate 50 5110457EPA 5030B 0.6 108-05-4 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 5110457EPA 5030B 0.4 75-01-4 11/20/15 11:3011/20/15 10:00
NDEPA 8260B ug/L1Xylenes, total 5.0 5110457EPA 5030B 0.6 1330-20-7 11/20/15 11:3011/20/15 10:00
EPA 8260B 21 ug/L1Tetrahydrofuran10 5110457EPA 5030B 1.5 109-99-9 11/20/15 11:3011/20/15 10:00
EPA 8260B 104 %Surr: Dibromofluoromethane 5110457EPA 5030B 1868-53-7 11/20/15 11:3011/20/15 10:0080-120
EPA 8260B 117 %Surr: 1,2-Dichloroethane-d4 5110457EPA 5030B 17060-07-0 11/20/15 11:3011/20/15 10:0078-120
EPA 8260B 97 %Surr: Toluene-d8 5110457EPA 5030B 2037-26-5 11/20/15 11:3011/20/15 10:0080-120
EPA 8260B 104 %Surr: 4-Bromofluorobenzene 5110457EPA 5030B 460-00-4 11/20/15 11:3011/20/15 10:0080-120
Semivolatile Organic Compounds by EPA 8270
NDEPA 8270D ug/L1Acenaphthene10 5110519EPA 3510C 2.2 83-32-9 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Acenaphthylene10 5110519EPA 3510C 2.1 208-96-8 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Acetophenone10 5110519EPA 3510C 3.3 98-86-2 11/24/15 22:2911/24/15 10:00
Page 19 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW4
Ground Water
AYK0618-04 AYK061811/18/15 15:04
Project:Lake Norman C&D Landfill
11/19/15 15:09
Semivolatile Organic Compounds by EPA 8270
NDEPA 8270D ug/L12-Acetylaminofluorene 20 5110519EPA 3510C 6.1 53-96-3 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L14-Aminobiphenyl 20 5110519EPA 3510C 3.0 92-67-1 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Anthracene10 5110519EPA 3510C 1.8 120-12-7 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Benzo(a)anthracene 10 5110519EPA 3510C 2.2 56-55-3 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Benzo(b)fluoranthene 10 5110519EPA 3510C 3.1 205-99-2 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Benzo(k)fluoranthene 10 5110519EPA 3510C 3.4 207-08-9 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Benzo(ghi)perylene 10 5110519EPA 3510C 2.9 191-24-2 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Benzo(a)pyrene 10 5110519EPA 3510C 2.3 50-32-8 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Benzyl alcohol 20 5110519EPA 3510C 3.0 100-51-6 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L14-Bromophenyl phenyl ether 10 5110519EPA 3510C 1.4 101-55-3 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Benzyl butyl phthalate 10 5110519EPA 3510C 3.2 85-68-7 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L14-Chloro-3-methylphenol 20 5110519EPA 3510C 2.3 59-50-7 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L14-Chloroaniline 20 5110519EPA 3510C 3.1 106-47-8 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Chlorobenzilate10 5110519EPA 3510C 4.9 510-15-6 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Bis(2-chloroethoxy)methane 10 5110519EPA 3510C 3.7 111-91-1 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Bis(2-chloroisopropyl)ether 10 5110519EPA 3510C 3.7 108-60-1 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Bis(2-chloroethyl)ether 10 5110519EPA 3510C 4.9 111-44-4 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L12-Chloronaphthalene 10 5110519EPA 3510C 2.9 91-58-7 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L12-Chlorophenol 10 5110519EPA 3510C 3.5 95-57-8 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L14-Chlorophenyl phenyl ether 10 5110519EPA 3510C 1.8 7005-72-3 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Chrysene10 5110519EPA 3510C 2.1 218-01-9 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Diallate10 5110519EPA 3510C 2.9 2303-16-4 11/24/15 22:2911/24/15 10:00
Page 20 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW4
Ground Water
AYK0618-04 AYK061811/18/15 15:04
Project:Lake Norman C&D Landfill
11/19/15 15:09
Semivolatile Organic Compounds by EPA 8270
NDEPA 8270D ug/L1Dibenzo(a,h)anthracene 10 5110519EPA 3510C 2.4 53-70-3 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Dibenzofuran10 5110519EPA 3510C 1.9 132-64-9 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L13,3´-Dichlorobenzidine 20 5110519EPA 3510C 2.4 91-94-1 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Di-n-butyl phthalate 10 5110519EPA 3510C 2.4 84-74-2 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L11,3-Dinitrobenzene 20 5110519EPA 3510C 4.1 99-65-0 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L12,4-Dichlorophenol 10 5110519EPA 3510C 2.8 120-83-2 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L12,6-Dichlorophenol 10 5110519EPA 3510C 6.1 87-65-0 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Diethyl phthalate 10 5110519EPA 3510C 2.0 84-66-2 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Dimethoate20 5110519EPA 3510C 5.4 60-51-5 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L13,3'-Dimethylbenzidine 10 5110519EPA 3510C 7.1 119-93-7 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L17,12-Dimethylbenz(a)anthracene 10 5110519EPA 3510C 5.4 57-97-6 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L14-Dimethylaminoazobenzene 10 5110519EPA 3510C 7.1 60-11-7 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L12,4-Dimethylphenol 10 5110519EPA 3510C 2.4 105-67-9 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Dimethyl phthalate 10 5110519EPA 3510C 1.7 131-11-3 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L14,6-Dinitro-2-methylphenol 50 5110519EPA 3510C 3.0 534-52-1 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L12,4-Dinitrophenol 50 5110519EPA 3510C 2.8 51-28-5 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L12,4-Dinitrotoluene 10 5110519EPA 3510C 2.9 121-14-2 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L12,6-Dinitrotoluene 10 5110519EPA 3510C 1.9 606-20-2 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Di-n-octyl phthalate 10 5110519EPA 3510C 4.0 117-84-0 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Disulfoton10 5110519EPA 3510C 3.3 298-04-4 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Bis(2-ethylhexyl)phthalate 15 5110519EPA 3510C 3.0 117-81-7 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Ethyl Methanesulfonate 20 5110519EPA 3510C 3.5 62-50-0 11/24/15 22:2911/24/15 10:00
Page 21 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW4
Ground Water
AYK0618-04 AYK061811/18/15 15:04
Project:Lake Norman C&D Landfill
11/19/15 15:09
Semivolatile Organic Compounds by EPA 8270
NDEPA 8270D ug/L1Famphur20 5110519EPA 3510C 5.0 52-85-7 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Fluoranthene10 5110519EPA 3510C 2.2 206-44-0 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Fluorene10 5110519EPA 3510C 1.7 86-73-7 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Hexachlorobenzene10 5110519EPA 3510C 1.3 118-74-1 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Hexachlorobutadiene10 5110519EPA 3510C 2.7 87-68-3 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Hexachlorocyclopentadiene10 5110519EPA 3510C 3.3 77-47-4 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Hexachloroethane10 5110519EPA 3510C 3.1 67-72-1 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Hexachloropropene10 5110519EPA 3510C 2.5 1888-71-7 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Indeno(1,2,3-cd)pyrene 10 5110519EPA 3510C 2.7 193-39-5 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Isophorone10 5110519EPA 3510C 3.0 78-59-1 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Isosafrole10 5110519EPA 3510C 3.3 120-58-1 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Kepone20 5110519EPA 3510C 11 143-50-0 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Methapyrilene100 5110519EPA 3510C 9.5 91-80-5 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L13-Methylcholanthrene 10 5110519EPA 3510C 5.4 56-49-5 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Methyl Methanesulfonate 10 5110519EPA 3510C 2.9 66-27-3 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L12-Methylnaphthalene 10 5110519EPA 3510C 2.5 91-57-6 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Methyl Parathion 10 5110519EPA 3510C 4.8 298-00-0 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L12-Methylphenol (o-cresol)10 5110519EPA 3510C 6.0 95-48-7 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L13+4-Methylphenol (m+p-cresol)10 5110519EPA 3510C 5.0 65794-96-9 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Naphthalene10 5110519EPA 3510C 2.6 91-20-3 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L11,4-Naphthoquinone 10 5110519EPA 3510C 5.8 130-15-4 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L11-Naphthylamine 10 5110519EPA 3510C 4.5 134-32-7 11/24/15 22:2911/24/15 10:00
Page 22 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW4
Ground Water
AYK0618-04 AYK061811/18/15 15:04
Project:Lake Norman C&D Landfill
11/19/15 15:09
Semivolatile Organic Compounds by EPA 8270
NDEPA 8270D ug/L12-Naphthylamine 10 5110519EPA 3510C 4.0 91-59-8 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L12-Nitroaniline 50 5110519EPA 3510C 2.5 88-74-4 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L13-Nitroaniline 50 5110519EPA 3510C 2.9 99-09-2 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L14-Nitroaniline 20 5110519EPA 3510C 3.4 100-01-6 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Nitrobenzene10 5110519EPA 3510C 3.6 98-95-3 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L12-Nitrophenol 10 5110519EPA 3510C 3.1 88-75-5 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L14-Nitrophenol 50 5110519EPA 3510C 1.9 100-02-7 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1N-Nitrosodi-n-butylamine 10 5110519EPA 3510C 4.0 924-16-3 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1N-Nitrosodiethylamine 20 5110519EPA 3510C 4.0 55-18-5 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1N-Nitrosodimethylamine 10 5110519EPA 3510C 3.0 62-75-9 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1N-Nitrosodi-n-propylamine 10 5110519EPA 3510C 3.6 621-64-7 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1N-Nitrosodiphenylamine/Diphenyl
amine 10 5110519EPA 3510C 1.9 86-30-6 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1N-Nitrosomethylethylamine 10 5110519EPA 3510C 3.0 10595-95-6 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1N-Nitrosopiperidine 20 5110519EPA 3510C 3.7 100-75-4 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1N-Nitrosopyrrolidine 10 5110519EPA 3510C 4.0 930-55-2 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L15-Nitro-o-toluidine 10 5110519EPA 3510C 4.4 99-55-8 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Parathion10 5110519EPA 3510C 5.0 56-38-2 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Pentachlorobenzene10 5110519EPA 3510C 3.3 608-93-5 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Pentachloronitrobenzene20 5110519EPA 3510C 4.4 82-68-8 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Pentachlorophenol25 5110519EPA 3510C 2.8 87-86-5 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Phenacetin20 5110519EPA 3510C 6.0 62-44-2 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Phenanthrene10 5110519EPA 3510C 1.4 85-01-8 11/24/15 22:2911/24/15 10:00
Page 23 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW4
Ground Water
AYK0618-04 AYK061811/18/15 15:04
Project:Lake Norman C&D Landfill
11/19/15 15:09
Semivolatile Organic Compounds by EPA 8270
NDEPA 8270D ug/L1Phenol10 5110519EPA 3510C 1.4 108-95-2 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1p-Phenylenediamine 10 5110519EPA 3510C 1.5 106-50-3 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Phorate10 5110519EPA 3510C 3.8 298-02-2 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Pronamide10 5110519EPA 3510C 4.3 23950-58-5 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Pyrene10 5110519EPA 3510C 2.6 129-00-0 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Safrole10 5110519EPA 3510C 4.6 94-59-7 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L12,3,4,6+2,3,4,5-Tetrachlorophen
ol 10 5110519EPA 3510C 2.9 58-90-2 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L11,2,4,5-Tetrachlorobenzene 10 5110519EPA 3510C 3.4 95-94-3 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1Thionazin20 5110519EPA 3510C 4.6 297-97-2 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L11,2,4-Trichlorobenzene 10 5110519EPA 3510C 2.4 120-82-1 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1o-Toluidine 10 5110519EPA 3510C 3.8 95-53-4 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L1O,O,O-Triethyl phosphorothioate 10 5110519EPA 3510C 3.9 126-68-1 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L12,4,5-Trichlorophenol 10 5110519EPA 3510C 2.3 95-95-4 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L12,4,6-Trichlorophenol 10 5110519EPA 3510C 3.4 88-06-2 11/24/15 22:2911/24/15 10:00
NDEPA 8270D ug/L11,3,5-Trinitrobenzene 10 5110519EPA 3510C 4.8 99-35-4 11/24/15 22:2911/24/15 10:00
EPA 8270D 36 %Surr: 2-Fluorophenol 5110519EPA 3510C 367-12-4 11/24/15 22:2911/24/15 10:0011-120
EPA 8270D 22 %Surr: Phenol-d6 5110519EPA 3510C 13127-88-3 11/24/15 22:2911/24/15 10:0010-120
EPA 8270D 73 %Surr: 2,4,6-Tribromophenol 5110519EPA 3510C 118-79-6 11/24/15 22:2911/24/15 10:0036-120
EPA 8270D 66 %Surr: 2-Fluorobiphenyl 5110519EPA 3510C 321-60-8 11/24/15 22:2911/24/15 10:0023-120
EPA 8270D 64 %Surr: Nitrobenzene-d5 5110519EPA 3510C 4165-60-0 11/24/15 22:2911/24/15 10:0015-120
EPA 8270D 84 %Surr: p-Terphenyl-dl4 5110519EPA 3510C 1718-51-0 11/24/15 22:2911/24/15 10:0053-121
Page 24 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW4
Ground Water
AYK0618-04 AYK061811/18/15 15:04
Project:Lake Norman C&D Landfill
11/19/15 15:09
Organochlorine Pesticides by EPA 8081
NDEPA 8081B ug/L1Aldrin0.05 5110522EPA 3510C 0.02 309-00-2 11/24/15 16:5611/24/15 08:55
NDEPA 8081B ug/L1BHC-alpha 0.05 5110522EPA 3510C 0.03 319-84-6 11/24/15 16:5611/24/15 08:55
NDEPA 8081B ug/L1BHC-beta 0.05 5110522EPA 3510C 0.03 319-85-7 11/24/15 16:5611/24/15 08:55
NDEPA 8081B ug/L1BHC-delta 0.05 5110522EPA 3510C 0.01 319-86-8 11/24/15 16:5611/24/15 08:55
NDEPA 8081B ug/L1BHC-gamma (Lindane)0.05 5110522EPA 3510C 0.03 58-89-9 11/24/15 16:5611/24/15 08:55
NDEPA 8081B ug/L1Chlordane0.5 5110522EPA 3510C 0.1 57-74-9 11/24/15 16:5611/24/15 08:55
NDEPA 8081B ug/L14,4'-DDD 0.1 5110522EPA 3510C 0.02 72-54-8 11/24/15 16:5611/24/15 08:55
NDEPA 8081B ug/L14,4'-DDE 0.1 5110522EPA 3510C 0.02 72-55-9 11/24/15 16:5611/24/15 08:55
NDEPA 8081B ug/L14,4'-DDT 0.1 5110522EPA 3510C 0.02 50-29-3 11/24/15 16:5611/24/15 08:55
NDEPA 8081B ug/L1Dieldrin0.08 5110522EPA 3510C 0.02 60-57-1 11/24/15 16:5611/24/15 08:55
NDEPA 8081B ug/L1Endosulfan I 0.1 5110522EPA 3510C 0.02 959-98-8 11/24/15 16:5611/24/15 08:55
NDEPA 8081B ug/L1Endosulfan II 0.1 5110522EPA 3510C 0.02 33213-65-9 11/24/15 16:5611/24/15 08:55
NDEPA 8081B ug/L1Endosulfan sulfate 0.1 5110522EPA 3510C 0.02 1031-07-8 11/24/15 16:5611/24/15 08:55
NDEPA 8081B ug/L1Endrin0.1 5110522EPA 3510C 0.01 72-20-8 11/24/15 16:5611/24/15 08:55
NDEPA 8081B ug/L1Endrin aldehyde 0.1 5110522EPA 3510C 0.03 7421-93-4 11/24/15 16:5611/24/15 08:55
NDEPA 8081B ug/L1Heptachlor0.05 5110522EPA 3510C 0.02 76-44-8 11/24/15 16:5611/24/15 08:55
NDEPA 8081B ug/L1Heptachlor epoxide 0.08 5110522EPA 3510C 0.02 1024-57-3 11/24/15 16:5611/24/15 08:55
NDEPA 8081B ug/L1Isodrin20 5110522EPA 3510C 0.03 465-73-6 11/24/15 16:5611/24/15 08:55
NDEPA 8081B ug/L1Methoxychlor1.0 5110522EPA 3510C 0.03 72-43-5 11/24/15 16:5611/24/15 08:55
NDEPA 8081B ug/L1Toxaphene1.5 5110522EPA 3510C 0.5 8001-35-2 11/24/15 16:5611/24/15 08:55
EPA 8081B 97 %Surr: Tetrachloro-m-xylene 5110522EPA 3510C 877-09-8 11/24/15 16:5611/24/15 08:5527-148
EPA 8081B 74 %Surr: Decachlorobiphenyl 5110522EPA 3510C 2051-24-3 11/24/15 16:5611/24/15 08:5510-155
Page 25 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW4
Ground Water
AYK0618-04 AYK061811/18/15 15:04
Project:Lake Norman C&D Landfill
11/19/15 15:09
PCBs by EPA 8082
NDEPA 8082A ug/L1PCB 1016 2.0 5110524EPA 3510C 0.3 12674-11-2 11/24/15 15:5711/24/15 09:02
NDEPA 8082A ug/L1PCB 1221 2.0 5110524EPA 3510C 2.0 11104-28-2 11/24/15 15:5711/24/15 09:02
NDEPA 8082A ug/L1PCB 1232 2.0 5110524EPA 3510C 2.0 11141-16-5 11/24/15 15:5711/24/15 09:02
NDEPA 8082A ug/L1PCB 1242 2.0 5110524EPA 3510C 2.0 53469-21-9 11/24/15 15:5711/24/15 09:02
NDEPA 8082A ug/L1PCB 1248 2.0 5110524EPA 3510C 2.0 12672-29-6 11/24/15 15:5711/24/15 09:02
NDEPA 8082A ug/L1PCB 1254 2.0 5110524EPA 3510C 2.0 11097-69-1 11/24/15 15:5711/24/15 09:02
NDEPA 8082A ug/L1PCB 1260 2.0 5110524EPA 3510C 0.1 11096-82-5 11/24/15 15:5711/24/15 09:02
EPA 8082A 48 %Surr: Decachlorobiphenyl 5110524EPA 3510C 2051-24-3 11/24/15 15:5711/24/15 09:0217-144
Chlorinated Herbicides by EPA 8151
NDEPA 8151A ug/L12,4-D 2.0 5110487EPA 8151A 0.60 94-75-7 11/24/15 15:0511/23/15 08:45
NDEPA 8151A ug/L12,4,5-T 2.0 5110487EPA 8151A 1.2 93-76-5 11/24/15 15:0511/23/15 08:45
NDEPA 8151A ug/L12,4,5-TP (Silvex)2.0 5110487EPA 8151A 0.80 93-72-1 11/24/15 15:0511/23/15 08:45
NDEPA 8151A ug/L1Dinoseb1.0 5110487EPA 8151A 0.72 88-85-7 11/24/15 15:0511/23/15 08:45
EPA 8151A 125 %Surr: DCAA 5110487EPA 8151A 19719-28-9 11/24/15 15:0511/23/15 08:4510-155
Page 26 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW5
Ground Water
AYK0618-05 AYK061811/18/15 16:00
Project:Lake Norman C&D Landfill
11/19/15 15:09
On Site
EPA 9050A 314 umhos/cm1Field - Specific Conductance 1 5110542NA1COND11/18/15 16:0011/18/15 16:00
EPA 9040C 6.87 pH Units1Field - pH 5110542NAPH11/18/15 16:0011/18/15 16:00
SM 2550 B 16.5 °C1Field - Temperature 5110542NATEMP11/18/15 16:0011/18/15 16:00
EPA 180.1 45.0 NTU1Field - Turbidity 5110542NATURB11/18/15 16:0011/18/15 16:00
NA 13.78 feet1Field - Water Level 5110542NAWL11/18/15 16:0011/18/15 16:00
General Chemistry
SM 2320 B 141000 ug/L1Alkalinity as CaCO3 1000 5110597SM 2320 B 1000 ALK 11/30/15 10:4511/30/15 10:45
SM 2540 C 236000 ug/L1Total Dissolved Solids 10000 5110550SM 2540 C 10000 E-10173 11/25/15 12:3011/25/15 12:30
Inorganic Anions
EPA 9056A 6600 ug/L1Chloride1000 5110537EPA 9056A 1000 16887-00-6 11/24/15 19:0211/24/15 19:02
NDEPA 9056A ug/L1Sulfate5000 5110537EPA 9056A 5000 14808-79-8 11/24/15 19:0211/24/15 19:02
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 5110457EPA 5030B 3.1 67-64-1 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Acrylonitrile200 5110457EPA 5030B 2.0 107-13-1 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Benzene1.0 5110457EPA 5030B 0.2 71-43-2 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Bromochloromethane3.0 5110457EPA 5030B 0.5 74-97-5 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 5110457EPA 5030B 0.5 75-27-4 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Bromoform3.0 5110457EPA 5030B 0.5 75-25-2 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Bromomethane10 5110457EPA 5030B 0.8 74-83-9 11/20/15 11:5711/20/15 10:00
Page 27 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW5
Ground Water
AYK0618-05 AYK061811/18/15 16:00
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Carbon Disulfide 100 5110457EPA 5030B 0.5 75-15-0 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 5110457EPA 5030B 0.4 56-23-5 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Chlorobenzene3.0 5110457EPA 5030B 0.5 108-90-7 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Chloroethane10 5110457EPA 5030B 0.6 75-00-3 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Chloroform5.0 5110457EPA 5030B 0.4 67-66-3 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Chloromethane1.0 5110457EPA 5030B 0.6 74-87-3 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Dibromochloromethane1.0 5110457EPA 5030B 0.3 124-48-1 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 5110457EPA 5030B 1.0 96-12-8 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 5110457EPA 5030B 0.4 106-93-4 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Dibromomethane10 5110457EPA 5030B 0.4 74-95-3 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 5110457EPA 5030B 0.2 95-50-1 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 5110457EPA 5030B 0.4 106-46-7 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 5110457EPA 5030B 1.1 110-57-6 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 5110457EPA 5030B 0.3 75-34-3 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 5110457EPA 5030B 0.3 107-06-2 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 5110457EPA 5030B 0.6 75-35-4 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.3 156-59-2 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.4 156-60-5 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 5110457EPA 5030B 0.4 78-87-5 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-01-5 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-02-6 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Ethylbenzene1.0 5110457EPA 5030B 0.2 100-41-4 11/20/15 11:5711/20/15 10:00
Page 28 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW5
Ground Water
AYK0618-05 AYK061811/18/15 16:00
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Iodomethane10 5110457EPA 5030B 1.7 74-88-4 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 5110457EPA 5030B 0.7 591-78-6 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 5110457EPA 5030B 0.6 75-09-2 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 5110457EPA 5030B 0.9 78-93-3 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)50 5110457EPA 5030B 1.0 108-10-1 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Styrene1.0 5110457EPA 5030B 0.3 100-42-5 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 5110457EPA 5030B 0.4 630-20-6 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 5110457EPA 5030B 0.5 79-34-5 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 5110457EPA 5030B 0.4 127-18-4 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Toluene1.0 5110457EPA 5030B 0.2 108-88-3 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 5110457EPA 5030B 0.3 71-55-6 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 5110457EPA 5030B 0.4 79-00-5 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Trichloroethene1.0 5110457EPA 5030B 0.4 79-01-6 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 5110457EPA 5030B 0.3 75-69-4 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 5110457EPA 5030B 0.3 96-18-4 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Vinyl Acetate 50 5110457EPA 5030B 0.6 108-05-4 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 5110457EPA 5030B 0.4 75-01-4 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Xylenes, total 4.0 5110457EPA 5030B 0.6 1330-20-7 11/20/15 11:5711/20/15 10:00
NDEPA 8260B ug/L1Tetrahydrofuran10 5110457EPA 5030B 1.5 109-99-9 11/20/15 11:5711/20/15 10:00
EPA 8260B 103 %Surr: Dibromofluoromethane 5110457EPA 5030B 1868-53-7 11/20/15 11:5711/20/15 10:0080-120
EPA 8260B S-09122 %Surr: 1,2-Dichloroethane-d4 5110457EPA 5030B 17060-07-0 11/20/15 11:5711/20/15 10:0078-120
Page 29 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW5
Ground Water
AYK0618-05 AYK061811/18/15 16:00
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
EPA 8260B 97 %Surr: Toluene-d8 5110457EPA 5030B 2037-26-5 11/20/15 11:5711/20/15 10:0080-120
EPA 8260B 105 %Surr: 4-Bromofluorobenzene 5110457EPA 5030B 460-00-4 11/20/15 11:5711/20/15 10:0080-120
Page 30 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-MW5
Ground Water
AYK0618-06 AYK061811/19/15 09:20
Project:Lake Norman C&D Landfill
11/19/15 15:09
On Site
EPA 180.1 4.95 NTU1Field - Turbidity 5110542NATURB11/19/15 09:2011/19/15 09:20
Metals, Total
NDEPA 6020A ug/L1Antimony6.00 5120028EPA 3005A 0.25 7440-36-0 12/02/15 18:0612/02/15 09:15
EPA 6020A 0.78 ug/L1Arsenic10.0 J 5120028EPA 3005A 0.75 7440-38-2 12/02/15 18:0612/02/15 09:15
EPA 6020A 20.8 ug/L1Barium100 J 5120028EPA 3005A 0.30 7440-39-3 12/02/15 18:0612/02/15 09:15
NDEPA 6020A ug/L1Beryllium1.00 5120028EPA 3005A 0.09 7440-41-7 12/02/15 18:0612/02/15 09:15
NDEPA 6020A ug/L1Cadmium1.00 5120028EPA 3005A 0.10 7440-43-9 12/02/15 18:0612/02/15 09:15
NDEPA 6020A ug/L1Chromium10.0 5120028EPA 3005A 0.43 7440-47-3 12/02/15 18:0612/02/15 09:15
EPA 6020A 0.90 ug/L1Cobalt10.0 J 5120028EPA 3005A 0.29 7440-48-4 12/02/15 18:0612/02/15 09:15
EPA 6020A 1.67 ug/L1Copper10.0 J 5120028EPA 3005A 0.41 7440-50-8 12/02/15 18:0612/02/15 09:15
EPA 6020A 0.12 ug/L1Lead10.0 J 5120028EPA 3005A 0.08 7439-92-1 12/02/15 18:0612/02/15 09:15
NDEPA 6020A ug/L1Nickel50.0 5120028EPA 3005A 0.48 7440-02-0 12/02/15 18:0612/02/15 09:15
NDEPA 6020A ug/L1Selenium10.0 5120028EPA 3005A 0.85 7782-49-2 12/02/15 18:0612/02/15 09:15
NDEPA 6020A ug/L1Silver10.0 5120028EPA 3005A 0.22 7440-22-4 12/02/15 18:0612/02/15 09:15
NDEPA 6020A ug/L1Thallium5.50 5120028EPA 3005A 0.06 7440-28-0 12/02/15 18:0612/02/15 09:15
EPA 6020A 4.83 ug/L1Vanadium25.0 J 5120028EPA 3005A 1.57 7440-62-2 12/02/15 18:0612/02/15 09:15
EPA 6020A 3.63 ug/L1Zinc10.0 J 5120028EPA 3005A 1.30 7440-66-6 12/02/15 18:0612/02/15 09:15
EPA 6020A 624 ug/L1Iron40.0 5120028EPA 3005A 5.72 7439-89-6 12/02/15 18:0612/02/15 09:15
EPA 6020A 940 ug/L1Manganese10.0 5120028EPA 3005A 1.04 7439-96-5 12/02/15 18:0612/02/15 09:15
NDEPA 7470A ug/L1Mercury0.200 5110582EPA 7470A 0.070 7439-97-6 11/30/15 13:5211/30/15 08:20
Page 31 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Duplicate
Ground Water
AYK0618-07 AYK061811/18/15 00:00
Project:Lake Norman C&D Landfill
11/19/15 15:09
General Chemistry
SM 2320 B 130000 ug/L1Alkalinity as CaCO3 1000 5110597SM 2320 B 1000 ALK 11/30/15 10:4511/30/15 10:45
SM 2540 C 208000 ug/L1Total Dissolved Solids 10000 5110550SM 2540 C 10000 E-10173 11/25/15 12:3011/25/15 12:30
Inorganic Anions
EPA 9056A 6100 ug/L1Chloride1000 5110537EPA 9056A 1000 16887-00-6 11/24/15 19:2311/24/15 19:23
NDEPA 9056A ug/L1Sulfate5000 5110537EPA 9056A 5000 14808-79-8 11/24/15 19:2311/24/15 19:23
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 5110457EPA 5030B 3.1 67-64-1 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Acrylonitrile200 5110457EPA 5030B 2.0 107-13-1 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Benzene1.0 5110457EPA 5030B 0.2 71-43-2 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Bromochloromethane3.0 5110457EPA 5030B 0.5 74-97-5 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 5110457EPA 5030B 0.5 75-27-4 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Bromoform3.0 5110457EPA 5030B 0.5 75-25-2 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Bromomethane10 5110457EPA 5030B 0.8 74-83-9 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Carbon Disulfide 100 5110457EPA 5030B 0.5 75-15-0 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 5110457EPA 5030B 0.4 56-23-5 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Chlorobenzene3.0 5110457EPA 5030B 0.5 108-90-7 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Chloroethane10 5110457EPA 5030B 0.6 75-00-3 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Chloroform5.0 5110457EPA 5030B 0.4 67-66-3 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Chloromethane1.0 5110457EPA 5030B 0.6 74-87-3 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Dibromochloromethane1.0 5110457EPA 5030B 0.3 124-48-1 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 5110457EPA 5030B 1.0 96-12-8 11/20/15 12:2311/20/15 10:00
Page 32 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Duplicate
Ground Water
AYK0618-07 AYK061811/18/15 00:00
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 5110457EPA 5030B 0.4 106-93-4 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Dibromomethane10 5110457EPA 5030B 0.4 74-95-3 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 5110457EPA 5030B 0.2 95-50-1 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 5110457EPA 5030B 0.4 106-46-7 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 5110457EPA 5030B 1.1 110-57-6 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 5110457EPA 5030B 0.3 75-34-3 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 5110457EPA 5030B 0.3 107-06-2 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 5110457EPA 5030B 0.6 75-35-4 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.3 156-59-2 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.4 156-60-5 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 5110457EPA 5030B 0.4 78-87-5 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-01-5 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-02-6 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Ethylbenzene1.0 5110457EPA 5030B 0.2 100-41-4 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Iodomethane10 5110457EPA 5030B 1.7 74-88-4 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 5110457EPA 5030B 0.7 591-78-6 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 5110457EPA 5030B 0.6 75-09-2 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 5110457EPA 5030B 0.9 78-93-3 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)50 5110457EPA 5030B 1.0 108-10-1 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Styrene1.0 5110457EPA 5030B 0.3 100-42-5 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 5110457EPA 5030B 0.4 630-20-6 11/20/15 12:2311/20/15 10:00
Page 33 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Duplicate
Ground Water
AYK0618-07 AYK061811/18/15 00:00
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 5110457EPA 5030B 0.5 79-34-5 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 5110457EPA 5030B 0.4 127-18-4 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Toluene1.0 5110457EPA 5030B 0.2 108-88-3 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 5110457EPA 5030B 0.3 71-55-6 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 5110457EPA 5030B 0.4 79-00-5 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Trichloroethene1.0 5110457EPA 5030B 0.4 79-01-6 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 5110457EPA 5030B 0.3 75-69-4 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 5110457EPA 5030B 0.3 96-18-4 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Vinyl Acetate 50 5110457EPA 5030B 0.6 108-05-4 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 5110457EPA 5030B 0.4 75-01-4 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Xylenes, total 4.0 5110457EPA 5030B 0.6 1330-20-7 11/20/15 12:2311/20/15 10:00
NDEPA 8260B ug/L1Tetrahydrofuran10 5110457EPA 5030B 1.5 109-99-9 11/20/15 12:2311/20/15 10:00
EPA 8260B 103 %Surr: Dibromofluoromethane 5110457EPA 5030B 1868-53-7 11/20/15 12:2311/20/15 10:0080-120
EPA 8260B 119 %Surr: 1,2-Dichloroethane-d4 5110457EPA 5030B 17060-07-0 11/20/15 12:2311/20/15 10:0078-120
EPA 8260B 97 %Surr: Toluene-d8 5110457EPA 5030B 2037-26-5 11/20/15 12:2311/20/15 10:0080-120
EPA 8260B 105 %Surr: 4-Bromofluorobenzene 5110457EPA 5030B 460-00-4 11/20/15 12:2311/20/15 10:0080-120
Page 34 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Duplicate
Ground Water
AYK0618-08 AYK061811/19/15 00:00
Project:Lake Norman C&D Landfill
11/19/15 15:09
Metals, Total
NDEPA 6020A ug/L1Antimony6.00 5120028EPA 3005A 0.25 7440-36-0 12/02/15 18:2112/02/15 09:15
NDEPA 6020A ug/L1Arsenic10.0 5120028EPA 3005A 0.75 7440-38-2 12/02/15 18:2112/02/15 09:15
EPA 6020A 20.3 ug/L1Barium100 J 5120028EPA 3005A 0.30 7440-39-3 12/02/15 18:2112/02/15 09:15
NDEPA 6020A ug/L1Beryllium1.00 5120028EPA 3005A 0.09 7440-41-7 12/02/15 18:2112/02/15 09:15
NDEPA 6020A ug/L1Cadmium1.00 5120028EPA 3005A 0.10 7440-43-9 12/02/15 18:2112/02/15 09:15
NDEPA 6020A ug/L1Chromium10.0 5120028EPA 3005A 0.43 7440-47-3 12/02/15 18:2112/02/15 09:15
EPA 6020A 0.88 ug/L1Cobalt10.0 J 5120028EPA 3005A 0.29 7440-48-4 12/02/15 18:2112/02/15 09:15
EPA 6020A 1.36 ug/L1Copper10.0 J 5120028EPA 3005A 0.41 7440-50-8 12/02/15 18:2112/02/15 09:15
EPA 6020A 0.12 ug/L1Lead10.0 J 5120028EPA 3005A 0.08 7439-92-1 12/02/15 18:2112/02/15 09:15
NDEPA 6020A ug/L1Nickel50.0 5120028EPA 3005A 0.48 7440-02-0 12/02/15 18:2112/02/15 09:15
NDEPA 6020A ug/L1Selenium10.0 5120028EPA 3005A 0.85 7782-49-2 12/02/15 18:2112/02/15 09:15
NDEPA 6020A ug/L1Silver10.0 5120028EPA 3005A 0.22 7440-22-4 12/02/15 18:2112/02/15 09:15
NDEPA 6020A ug/L1Thallium5.50 5120028EPA 3005A 0.06 7440-28-0 12/02/15 18:2112/02/15 09:15
EPA 6020A 4.77 ug/L1Vanadium25.0 J 5120028EPA 3005A 1.57 7440-62-2 12/02/15 18:2112/02/15 09:15
EPA 6020A 3.43 ug/L1Zinc10.0 J 5120028EPA 3005A 1.30 7440-66-6 12/02/15 18:2112/02/15 09:15
EPA 6020A 551 ug/L1Iron40.0 5120028EPA 3005A 5.72 7439-89-6 12/02/15 18:2112/02/15 09:15
EPA 6020A 964 ug/L1Manganese10.0 5120028EPA 3005A 1.04 7439-96-5 12/02/15 18:2112/02/15 09:15
NDEPA 7470A ug/L1Mercury0.200 5110582EPA 7470A 0.070 7439-97-6 11/30/15 13:5411/30/15 08:20
Page 35 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Field Blank
Water
AYK0618-09 AYK061811/18/15 14:07
Project:Lake Norman C&D Landfill
11/19/15 15:09
General Chemistry
NDSM 2320 B ug/L1Alkalinity as CaCO3 1000 5110597SM 2320 B 1000 ALK 11/30/15 10:4511/30/15 10:45
SM 2540 C 33000 ug/L1Total Dissolved Solids 10000 5110550SM 2540 C 10000 E-10173 11/25/15 12:3011/25/15 12:30
Inorganic Anions
NDEPA 9056A ug/L1Chloride1000 5110537EPA 9056A 1000 16887-00-6 11/24/15 19:4411/24/15 19:44
NDEPA 9056A ug/L1Sulfate5000 5110537EPA 9056A 5000 14808-79-8 11/24/15 19:4411/24/15 19:44
Metals, Total
NDEPA 6020A ug/L1Antimony6.00 5120028EPA 3005A 0.25 7440-36-0 12/02/15 18:2612/02/15 09:15
EPA 6020A 0.78 ug/L1Arsenic10.0 J 5120028EPA 3005A 0.75 7440-38-2 12/02/15 18:2612/02/15 09:15
EPA 6020A 0.55 ug/L1Barium100 J 5120028EPA 3005A 0.30 7440-39-3 12/02/15 18:2612/02/15 09:15
NDEPA 6020A ug/L1Beryllium1.00 5120028EPA 3005A 0.09 7440-41-7 12/02/15 18:2612/02/15 09:15
NDEPA 6020A ug/L1Cadmium1.00 5120028EPA 3005A 0.10 7440-43-9 12/02/15 18:2612/02/15 09:15
NDEPA 6020A ug/L1Chromium10.0 5120028EPA 3005A 0.43 7440-47-3 12/02/15 18:2612/02/15 09:15
NDEPA 6020A ug/L1Cobalt10.0 5120028EPA 3005A 0.29 7440-48-4 12/02/15 18:2612/02/15 09:15
NDEPA 6020A ug/L1Copper10.0 5120028EPA 3005A 0.41 7440-50-8 12/02/15 18:2612/02/15 09:15
NDEPA 6020A ug/L1Lead10.0 5120028EPA 3005A 0.08 7439-92-1 12/02/15 18:2612/02/15 09:15
NDEPA 6020A ug/L1Nickel50.0 5120028EPA 3005A 0.48 7440-02-0 12/02/15 18:2612/02/15 09:15
NDEPA 6020A ug/L1Selenium10.0 5120028EPA 3005A 0.85 7782-49-2 12/02/15 18:2612/02/15 09:15
NDEPA 6020A ug/L1Silver10.0 5120028EPA 3005A 0.22 7440-22-4 12/02/15 18:2612/02/15 09:15
NDEPA 6020A ug/L1Thallium5.50 5120028EPA 3005A 0.06 7440-28-0 12/02/15 18:2612/02/15 09:15
EPA 6020A 2.52 ug/L1Vanadium25.0 J 5120028EPA 3005A 1.57 7440-62-2 12/02/15 18:2612/02/15 09:15
Page 36 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Field Blank
Water
AYK0618-09 AYK061811/18/15 14:07
Project:Lake Norman C&D Landfill
11/19/15 15:09
Metals, Total
NDEPA 6020A ug/L1Zinc10.0 5120028EPA 3005A 1.30 7440-66-6 12/02/15 18:2612/02/15 09:15
NDEPA 6020A ug/L1Iron40.0 5120028EPA 3005A 5.72 7439-89-6 12/02/15 18:2612/02/15 09:15
NDEPA 6020A ug/L1Manganese10.0 5120028EPA 3005A 1.04 7439-96-5 12/02/15 18:2612/02/15 09:15
NDEPA 7470A ug/L1Mercury0.200 5110582EPA 7470A 0.070 7439-97-6 11/30/15 13:5611/30/15 08:20
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 5110457EPA 5030B 3.1 67-64-1 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Acrylonitrile200 5110457EPA 5030B 2.0 107-13-1 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Benzene1.0 5110457EPA 5030B 0.2 71-43-2 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Bromochloromethane3.0 5110457EPA 5030B 0.5 74-97-5 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 5110457EPA 5030B 0.5 75-27-4 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Bromoform3.0 5110457EPA 5030B 0.5 75-25-2 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Bromomethane10 5110457EPA 5030B 0.8 74-83-9 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Carbon Disulfide 100 5110457EPA 5030B 0.5 75-15-0 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 5110457EPA 5030B 0.4 56-23-5 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Chlorobenzene3.0 5110457EPA 5030B 0.5 108-90-7 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Chloroethane10 5110457EPA 5030B 0.6 75-00-3 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Chloroform5.0 5110457EPA 5030B 0.4 67-66-3 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Chloromethane1.0 5110457EPA 5030B 0.6 74-87-3 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Dibromochloromethane1.0 5110457EPA 5030B 0.3 124-48-1 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 5110457EPA 5030B 1.0 96-12-8 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 5110457EPA 5030B 0.4 106-93-4 11/20/15 12:5011/20/15 10:00
Page 37 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Field Blank
Water
AYK0618-09 AYK061811/18/15 14:07
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Dibromomethane10 5110457EPA 5030B 0.4 74-95-3 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 5110457EPA 5030B 0.2 95-50-1 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 5110457EPA 5030B 0.4 106-46-7 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 5110457EPA 5030B 1.1 110-57-6 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 5110457EPA 5030B 0.3 75-34-3 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 5110457EPA 5030B 0.3 107-06-2 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 5110457EPA 5030B 0.6 75-35-4 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.3 156-59-2 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.4 156-60-5 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 5110457EPA 5030B 0.4 78-87-5 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-01-5 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-02-6 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Ethylbenzene1.0 5110457EPA 5030B 0.2 100-41-4 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Iodomethane10 5110457EPA 5030B 1.7 74-88-4 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 5110457EPA 5030B 0.7 591-78-6 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 5110457EPA 5030B 0.6 75-09-2 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 5110457EPA 5030B 0.9 78-93-3 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)50 5110457EPA 5030B 1.0 108-10-1 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Styrene1.0 5110457EPA 5030B 0.3 100-42-5 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 5110457EPA 5030B 0.4 630-20-6 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 5110457EPA 5030B 0.5 79-34-5 11/20/15 12:5011/20/15 10:00
Page 38 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Field Blank
Water
AYK0618-09 AYK061811/18/15 14:07
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Tetrachloroethene1.0 5110457EPA 5030B 0.4 127-18-4 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Toluene1.0 5110457EPA 5030B 0.2 108-88-3 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 5110457EPA 5030B 0.3 71-55-6 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 5110457EPA 5030B 0.4 79-00-5 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Trichloroethene1.0 5110457EPA 5030B 0.4 79-01-6 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 5110457EPA 5030B 0.3 75-69-4 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 5110457EPA 5030B 0.3 96-18-4 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Vinyl Acetate 50 5110457EPA 5030B 0.6 108-05-4 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 5110457EPA 5030B 0.4 75-01-4 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Xylenes, total 4.0 5110457EPA 5030B 0.6 1330-20-7 11/20/15 12:5011/20/15 10:00
NDEPA 8260B ug/L1Tetrahydrofuran10 5110457EPA 5030B 1.5 109-99-9 11/20/15 12:5011/20/15 10:00
EPA 8260B 104 %Surr: Dibromofluoromethane 5110457EPA 5030B 1868-53-7 11/20/15 12:5011/20/15 10:0080-120
EPA 8260B 118 %Surr: 1,2-Dichloroethane-d4 5110457EPA 5030B 17060-07-0 11/20/15 12:5011/20/15 10:0078-120
EPA 8260B 99 %Surr: Toluene-d8 5110457EPA 5030B 2037-26-5 11/20/15 12:5011/20/15 10:0080-120
EPA 8260B 101 %Surr: 4-Bromofluorobenzene 5110457EPA 5030B 460-00-4 11/20/15 12:5011/20/15 10:0080-120
Page 39 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Equipment Blank
Water
AYK0618-10 AYK061811/18/15 15:20
Project:Lake Norman C&D Landfill
11/19/15 15:09
General Chemistry
SM 2320 B 1000 ug/L1Alkalinity as CaCO3 1000 5110597SM 2320 B 1000 ALK 11/30/15 10:4511/30/15 10:45
SM 2540 C 53000 ug/L1Total Dissolved Solids 10000 5110550SM 2540 C 10000 E-10173 11/25/15 12:3011/25/15 12:30
Inorganic Anions
NDEPA 9056A ug/L1Chloride1000 5110537EPA 9056A 1000 16887-00-6 11/24/15 20:0411/24/15 20:04
NDEPA 9056A ug/L1Sulfate5000 5110537EPA 9056A 5000 14808-79-8 11/24/15 20:0411/24/15 20:04
Metals, Total
NDEPA 6020A ug/L1Antimony6.00 5120028EPA 3005A 0.25 7440-36-0 12/02/15 18:3112/02/15 09:15
NDEPA 6020A ug/L1Arsenic10.0 5120028EPA 3005A 0.75 7440-38-2 12/02/15 18:3112/02/15 09:15
EPA 6020A 0.47 ug/L1Barium100 J 5120028EPA 3005A 0.30 7440-39-3 12/02/15 18:3112/02/15 09:15
NDEPA 6020A ug/L1Beryllium1.00 5120028EPA 3005A 0.09 7440-41-7 12/02/15 18:3112/02/15 09:15
NDEPA 6020A ug/L1Cadmium1.00 5120028EPA 3005A 0.10 7440-43-9 12/02/15 18:3112/02/15 09:15
NDEPA 6020A ug/L1Chromium10.0 5120028EPA 3005A 0.43 7440-47-3 12/02/15 18:3112/02/15 09:15
NDEPA 6020A ug/L1Cobalt10.0 5120028EPA 3005A 0.29 7440-48-4 12/02/15 18:3112/02/15 09:15
NDEPA 6020A ug/L1Copper10.0 5120028EPA 3005A 0.41 7440-50-8 12/02/15 18:3112/02/15 09:15
NDEPA 6020A ug/L1Lead10.0 5120028EPA 3005A 0.08 7439-92-1 12/02/15 18:3112/02/15 09:15
NDEPA 6020A ug/L1Nickel50.0 5120028EPA 3005A 0.48 7440-02-0 12/02/15 18:3112/02/15 09:15
NDEPA 6020A ug/L1Selenium10.0 5120028EPA 3005A 0.85 7782-49-2 12/02/15 18:3112/02/15 09:15
NDEPA 6020A ug/L1Silver10.0 5120028EPA 3005A 0.22 7440-22-4 12/02/15 18:3112/02/15 09:15
NDEPA 6020A ug/L1Thallium5.50 5120028EPA 3005A 0.06 7440-28-0 12/02/15 18:3112/02/15 09:15
EPA 6020A 2.70 ug/L1Vanadium25.0 J 5120028EPA 3005A 1.57 7440-62-2 12/02/15 18:3112/02/15 09:15
Page 40 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Equipment Blank
Water
AYK0618-10 AYK061811/18/15 15:20
Project:Lake Norman C&D Landfill
11/19/15 15:09
Metals, Total
NDEPA 6020A ug/L1Zinc10.0 5120028EPA 3005A 1.30 7440-66-6 12/02/15 18:3112/02/15 09:15
NDEPA 6020A ug/L1Iron40.0 5120028EPA 3005A 5.72 7439-89-6 12/02/15 18:3112/02/15 09:15
NDEPA 6020A ug/L1Manganese10.0 5120028EPA 3005A 1.04 7439-96-5 12/02/15 18:3112/02/15 09:15
NDEPA 7470A ug/L1Mercury0.200 5110582EPA 7470A 0.070 7439-97-6 11/30/15 13:5911/30/15 08:20
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 5110457EPA 5030B 3.1 67-64-1 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Acrylonitrile200 5110457EPA 5030B 2.0 107-13-1 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Benzene1.0 5110457EPA 5030B 0.2 71-43-2 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Bromochloromethane3.0 5110457EPA 5030B 0.5 74-97-5 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 5110457EPA 5030B 0.5 75-27-4 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Bromoform3.0 5110457EPA 5030B 0.5 75-25-2 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Bromomethane10 5110457EPA 5030B 0.8 74-83-9 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Carbon Disulfide 100 5110457EPA 5030B 0.5 75-15-0 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 5110457EPA 5030B 0.4 56-23-5 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Chlorobenzene3.0 5110457EPA 5030B 0.5 108-90-7 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Chloroethane10 5110457EPA 5030B 0.6 75-00-3 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Chloroform5.0 5110457EPA 5030B 0.4 67-66-3 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Chloromethane1.0 5110457EPA 5030B 0.6 74-87-3 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Dibromochloromethane1.0 5110457EPA 5030B 0.3 124-48-1 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 5110457EPA 5030B 1.0 96-12-8 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 5110457EPA 5030B 0.4 106-93-4 11/20/15 14:0811/20/15 10:00
Page 41 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Equipment Blank
Water
AYK0618-10 AYK061811/18/15 15:20
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Dibromomethane10 5110457EPA 5030B 0.4 74-95-3 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 5110457EPA 5030B 0.2 95-50-1 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 5110457EPA 5030B 0.4 106-46-7 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 5110457EPA 5030B 1.1 110-57-6 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 5110457EPA 5030B 0.3 75-34-3 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 5110457EPA 5030B 0.3 107-06-2 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 5110457EPA 5030B 0.6 75-35-4 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.3 156-59-2 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.4 156-60-5 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 5110457EPA 5030B 0.4 78-87-5 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-01-5 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-02-6 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Ethylbenzene1.0 5110457EPA 5030B 0.2 100-41-4 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Iodomethane10 5110457EPA 5030B 1.7 74-88-4 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 5110457EPA 5030B 0.7 591-78-6 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 5110457EPA 5030B 0.6 75-09-2 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 5110457EPA 5030B 0.9 78-93-3 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)50 5110457EPA 5030B 1.0 108-10-1 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Styrene1.0 5110457EPA 5030B 0.3 100-42-5 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 5110457EPA 5030B 0.4 630-20-6 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 5110457EPA 5030B 0.5 79-34-5 11/20/15 14:0811/20/15 10:00
Page 42 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Equipment Blank
Water
AYK0618-10 AYK061811/18/15 15:20
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Tetrachloroethene1.0 5110457EPA 5030B 0.4 127-18-4 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Toluene1.0 5110457EPA 5030B 0.2 108-88-3 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 5110457EPA 5030B 0.3 71-55-6 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 5110457EPA 5030B 0.4 79-00-5 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Trichloroethene1.0 5110457EPA 5030B 0.4 79-01-6 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 5110457EPA 5030B 0.3 75-69-4 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 5110457EPA 5030B 0.3 96-18-4 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Vinyl Acetate 50 5110457EPA 5030B 0.6 108-05-4 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 5110457EPA 5030B 0.4 75-01-4 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Xylenes, total 4.0 5110457EPA 5030B 0.6 1330-20-7 11/20/15 14:0811/20/15 10:00
NDEPA 8260B ug/L1Tetrahydrofuran10 5110457EPA 5030B 1.5 109-99-9 11/20/15 14:0811/20/15 10:00
EPA 8260B 106 %Surr: Dibromofluoromethane 5110457EPA 5030B 1868-53-7 11/20/15 14:0811/20/15 10:0080-120
EPA 8260B S-09121 %Surr: 1,2-Dichloroethane-d4 5110457EPA 5030B 17060-07-0 11/20/15 14:0811/20/15 10:0078-120
EPA 8260B 99 %Surr: Toluene-d8 5110457EPA 5030B 2037-26-5 11/20/15 14:0811/20/15 10:0080-120
EPA 8260B 102 %Surr: 4-Bromofluorobenzene 5110457EPA 5030B 460-00-4 11/20/15 14:0811/20/15 10:0080-120
Page 43 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Trip Blank
Water
AYK0618-11 AYK061811/18/15 00:00
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 5110457EPA 5030B 3.1 67-64-1 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Acrylonitrile200 5110457EPA 5030B 2.0 107-13-1 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Benzene1.0 5110457EPA 5030B 0.2 71-43-2 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Bromochloromethane3.0 5110457EPA 5030B 0.5 74-97-5 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 5110457EPA 5030B 0.5 75-27-4 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Bromoform3.0 5110457EPA 5030B 0.5 75-25-2 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Bromomethane10 5110457EPA 5030B 0.8 74-83-9 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Carbon Disulfide 100 5110457EPA 5030B 0.5 75-15-0 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 5110457EPA 5030B 0.4 56-23-5 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Chlorobenzene3.0 5110457EPA 5030B 0.5 108-90-7 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Chloroethane10 5110457EPA 5030B 0.6 75-00-3 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Chloroform5.0 5110457EPA 5030B 0.4 67-66-3 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Chloromethane1.0 5110457EPA 5030B 0.6 74-87-3 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Dibromochloromethane1.0 5110457EPA 5030B 0.3 124-48-1 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 5110457EPA 5030B 1.0 96-12-8 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 5110457EPA 5030B 0.4 106-93-4 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Dibromomethane10 5110457EPA 5030B 0.4 74-95-3 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 5110457EPA 5030B 0.2 95-50-1 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 5110457EPA 5030B 0.4 106-46-7 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 5110457EPA 5030B 1.1 110-57-6 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 5110457EPA 5030B 0.3 75-34-3 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 5110457EPA 5030B 0.3 107-06-2 11/20/15 14:3511/20/15 10:00
Page 44 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Trip Blank
Water
AYK0618-11 AYK061811/18/15 00:00
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 5110457EPA 5030B 0.6 75-35-4 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.3 156-59-2 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.4 156-60-5 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 5110457EPA 5030B 0.4 78-87-5 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-01-5 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-02-6 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Ethylbenzene1.0 5110457EPA 5030B 0.2 100-41-4 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Iodomethane10 5110457EPA 5030B 1.7 74-88-4 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 5110457EPA 5030B 0.7 591-78-6 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Methylene Chloride 1.0 5110457EPA 5030B 0.6 75-09-2 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 5110457EPA 5030B 0.9 78-93-3 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)50 5110457EPA 5030B 1.0 108-10-1 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Styrene1.0 5110457EPA 5030B 0.3 100-42-5 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 5110457EPA 5030B 0.4 630-20-6 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 5110457EPA 5030B 0.5 79-34-5 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 5110457EPA 5030B 0.4 127-18-4 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Toluene1.0 5110457EPA 5030B 0.2 108-88-3 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 5110457EPA 5030B 0.3 71-55-6 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 5110457EPA 5030B 0.4 79-00-5 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Trichloroethene1.0 5110457EPA 5030B 0.4 79-01-6 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 5110457EPA 5030B 0.3 75-69-4 11/20/15 14:3511/20/15 10:00
Page 45 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-Trip Blank
Water
AYK0618-11 AYK061811/18/15 00:00
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 5110457EPA 5030B 0.3 96-18-4 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Vinyl Acetate 50 5110457EPA 5030B 0.6 108-05-4 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 5110457EPA 5030B 0.4 75-01-4 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Xylenes, total 4.0 5110457EPA 5030B 0.6 1330-20-7 11/20/15 14:3511/20/15 10:00
NDEPA 8260B ug/L1Tetrahydrofuran10 5110457EPA 5030B 1.5 109-99-9 11/20/15 14:3511/20/15 10:00
EPA 8260B 105 %Surr: Dibromofluoromethane 5110457EPA 5030B 1868-53-7 11/20/15 14:3511/20/15 10:0080-120
EPA 8260B S-09123 %Surr: 1,2-Dichloroethane-d4 5110457EPA 5030B 17060-07-0 11/20/15 14:3511/20/15 10:0078-120
EPA 8260B 100 %Surr: Toluene-d8 5110457EPA 5030B 2037-26-5 11/20/15 14:3511/20/15 10:0080-120
EPA 8260B 104 %Surr: 4-Bromofluorobenzene 5110457EPA 5030B 460-00-4 11/20/15 14:3511/20/15 10:0080-120
Page 46 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-SW1
Surface Water
AYK0618-12 AYK061811/18/15 15:46
Project:Lake Norman C&D Landfill
11/19/15 15:09
On Site
EPA 9050A 156 umhos/cm1Field - Specific Conductance 1 5110542NA1COND11/18/15 15:4611/18/15 15:46
SM 4500-O G 5900 ug/L1Dissolved Oxygen 0.0 5110542NA0.0 NA 11/18/15 15:4611/18/15 15:46
EPA 9040C 6.58 pH Units1Field - pH 5110542NAPH11/18/15 15:4611/18/15 15:46
SM 2550 B 16.6 °C1Field - Temperature 5110542NATEMP11/18/15 15:4611/18/15 15:46
EPA 180.1 6.95 NTU1Field - Turbidity 5110542NATURB11/18/15 15:4611/18/15 15:46
General Chemistry
SM 2320 B 36000 ug/L1Alkalinity as CaCO3 1000 5110597SM 2320 B 1000 ALK 11/30/15 10:4511/30/15 10:45
SM 2540 C 123000 ug/L1Total Dissolved Solids 10000 5110550SM 2540 C 10000 E-10173 11/25/15 12:3011/25/15 12:30
Inorganic Anions
EPA 9056A 5100 ug/L1Chloride1000 5110537EPA 9056A 1000 16887-00-6 11/24/15 20:2511/24/15 20:25
EPA 9056A 5600 ug/L1Sulfate5000 5110537EPA 9056A 5000 14808-79-8 11/24/15 20:2511/24/15 20:25
Metals, Total
NDEPA 6020A ug/L1Antimony6.00 5120028EPA 3005A 0.25 7440-36-0 12/02/15 18:3612/02/15 09:15
EPA 6020A 0.92 ug/L1Arsenic10.0 J 5120028EPA 3005A 0.75 7440-38-2 12/02/15 18:3612/02/15 09:15
EPA 6020A 46.8 ug/L1Barium100 J 5120028EPA 3005A 0.30 7440-39-3 12/02/15 18:3612/02/15 09:15
NDEPA 6020A ug/L1Beryllium1.00 5120028EPA 3005A 0.09 7440-41-7 12/02/15 18:3612/02/15 09:15
NDEPA 6020A ug/L1Cadmium1.00 5120028EPA 3005A 0.10 7440-43-9 12/02/15 18:3612/02/15 09:15
NDEPA 6020A ug/L1Chromium10.0 5120028EPA 3005A 0.43 7440-47-3 12/02/15 18:3612/02/15 09:15
EPA 6020A 1.32 ug/L1Cobalt10.0 J 5120028EPA 3005A 0.29 7440-48-4 12/02/15 18:3612/02/15 09:15
Page 47 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-SW1
Surface Water
AYK0618-12 AYK061811/18/15 15:46
Project:Lake Norman C&D Landfill
11/19/15 15:09
Metals, Total
EPA 6020A 0.63 ug/L1Copper10.0 J 5120028EPA 3005A 0.41 7440-50-8 12/02/15 18:3612/02/15 09:15
EPA 6020A 0.11 ug/L1Lead10.0 J 5120028EPA 3005A 0.08 7439-92-1 12/02/15 18:3612/02/15 09:15
NDEPA 6020A ug/L1Nickel50.0 5120028EPA 3005A 0.48 7440-02-0 12/02/15 18:3612/02/15 09:15
NDEPA 6020A ug/L1Selenium10.0 5120028EPA 3005A 0.85 7782-49-2 12/02/15 18:3612/02/15 09:15
NDEPA 6020A ug/L1Silver10.0 5120028EPA 3005A 0.22 7440-22-4 12/02/15 18:3612/02/15 09:15
NDEPA 6020A ug/L1Thallium5.50 5120028EPA 3005A 0.06 7440-28-0 12/02/15 18:3612/02/15 09:15
EPA 6020A 3.72 ug/L1Vanadium25.0 J 5120028EPA 3005A 1.57 7440-62-2 12/02/15 18:3612/02/15 09:15
EPA 6020A 5.20 ug/L1Zinc10.0 J 5120028EPA 3005A 1.30 7440-66-6 12/02/15 18:3612/02/15 09:15
EPA 6020A 1730 ug/L1Iron40.0 5120028EPA 3005A 5.72 7439-89-6 12/02/15 18:3612/02/15 09:15
EPA 6020A 310 ug/L1Manganese10.0 5120028EPA 3005A 1.04 7439-96-5 12/02/15 18:3612/02/15 09:15
EPA 7470A 0.105 ug/L1Mercury0.200 J 5110582EPA 7470A 0.070 7439-97-6 11/30/15 14:0111/30/15 08:20
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 5110457EPA 5030B 3.1 67-64-1 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Acrylonitrile200 5110457EPA 5030B 2.0 107-13-1 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Benzene1.0 5110457EPA 5030B 0.2 71-43-2 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Bromochloromethane3.0 5110457EPA 5030B 0.5 74-97-5 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 5110457EPA 5030B 0.5 75-27-4 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Bromoform3.0 5110457EPA 5030B 0.5 75-25-2 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Bromomethane10 5110457EPA 5030B 0.8 74-83-9 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Carbon Disulfide 100 5110457EPA 5030B 0.5 75-15-0 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 5110457EPA 5030B 0.4 56-23-5 11/20/15 15:0111/20/15 10:00
Page 48 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-SW1
Surface Water
AYK0618-12 AYK061811/18/15 15:46
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Chlorobenzene3.0 5110457EPA 5030B 0.5 108-90-7 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Chloroethane10 5110457EPA 5030B 0.6 75-00-3 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Chloroform5.0 5110457EPA 5030B 0.4 67-66-3 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Chloromethane1.0 5110457EPA 5030B 0.6 74-87-3 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Dibromochloromethane1.0 5110457EPA 5030B 0.3 124-48-1 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 5110457EPA 5030B 1.0 96-12-8 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 5110457EPA 5030B 0.4 106-93-4 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Dibromomethane10 5110457EPA 5030B 0.4 74-95-3 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 5110457EPA 5030B 0.2 95-50-1 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 5110457EPA 5030B 0.4 106-46-7 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 5110457EPA 5030B 1.1 110-57-6 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 5110457EPA 5030B 0.3 75-34-3 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 5110457EPA 5030B 0.3 107-06-2 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 5110457EPA 5030B 0.6 75-35-4 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.3 156-59-2 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.4 156-60-5 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 5110457EPA 5030B 0.4 78-87-5 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-01-5 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-02-6 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Ethylbenzene1.0 5110457EPA 5030B 0.2 100-41-4 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Iodomethane10 5110457EPA 5030B 1.7 74-88-4 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 5110457EPA 5030B 0.7 591-78-6 11/20/15 15:0111/20/15 10:00
Page 49 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-SW1
Surface Water
AYK0618-12 AYK061811/18/15 15:46
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Methylene Chloride 1.0 5110457EPA 5030B 0.6 75-09-2 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 5110457EPA 5030B 0.9 78-93-3 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)50 5110457EPA 5030B 1.0 108-10-1 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Styrene1.0 5110457EPA 5030B 0.3 100-42-5 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 5110457EPA 5030B 0.4 630-20-6 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 5110457EPA 5030B 0.5 79-34-5 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 5110457EPA 5030B 0.4 127-18-4 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Toluene1.0 5110457EPA 5030B 0.2 108-88-3 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 5110457EPA 5030B 0.3 71-55-6 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 5110457EPA 5030B 0.4 79-00-5 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Trichloroethene1.0 5110457EPA 5030B 0.4 79-01-6 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 5110457EPA 5030B 0.3 75-69-4 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 5110457EPA 5030B 0.3 96-18-4 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Vinyl Acetate 50 5110457EPA 5030B 0.6 108-05-4 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 5110457EPA 5030B 0.4 75-01-4 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Xylenes, total 4.0 5110457EPA 5030B 0.6 1330-20-7 11/20/15 15:0111/20/15 10:00
NDEPA 8260B ug/L1Tetrahydrofuran10 5110457EPA 5030B 1.5 109-99-9 11/20/15 15:0111/20/15 10:00
EPA 8260B 105 %Surr: Dibromofluoromethane 5110457EPA 5030B 1868-53-7 11/20/15 15:0111/20/15 10:0080-120
EPA 8260B S-09122 %Surr: 1,2-Dichloroethane-d4 5110457EPA 5030B 17060-07-0 11/20/15 15:0111/20/15 10:0078-120
EPA 8260B 97 %Surr: Toluene-d8 5110457EPA 5030B 2037-26-5 11/20/15 15:0111/20/15 10:0080-120
EPA 8260B 104 %Surr: 4-Bromofluorobenzene 5110457EPA 5030B 460-00-4 11/20/15 15:0111/20/15 10:0080-120
Page 50 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-SW2
Surface Water
AYK0618-13 AYK061811/19/15 08:50
Project:Lake Norman C&D Landfill
11/19/15 15:09
On Site
EPA 9050A 109 umhos/cm1Field - Specific Conductance 1 5110542NA1COND11/19/15 08:5011/19/15 08:50
SM 4500-O G 4600 ug/L1Dissolved Oxygen 0.0 5110542NA0.0 NA 11/19/15 08:5011/19/15 08:50
EPA 9040C 6.58 pH Units1Field - pH 5110542NAPH11/19/15 08:5011/19/15 08:50
SM 2550 B 14.9 °C1Field - Temperature 5110542NATEMP11/19/15 08:5011/19/15 08:50
EPA 180.1 27.0 NTU1Field - Turbidity 5110542NATURB11/19/15 08:5011/19/15 08:50
General Chemistry
SM 2320 B 18000 ug/L1Alkalinity as CaCO3 1000 5110597SM 2320 B 1000 ALK 11/30/15 10:4511/30/15 10:45
SM 2540 C 153000 ug/L1Total Dissolved Solids 10000 5110550SM 2540 C 10000 E-10173 11/25/15 12:3011/25/15 12:30
Inorganic Anions
EPA 9056A 2600 ug/L1Chloride1000 5110537EPA 9056A 1000 16887-00-6 11/24/15 21:2711/24/15 21:27
EPA 9056A 10000 ug/L1Sulfate5000 5110537EPA 9056A 5000 14808-79-8 11/24/15 21:2711/24/15 21:27
Metals, Total
NDEPA 6020A ug/L1Antimony6.00 5120028EPA 3005A 0.25 7440-36-0 12/02/15 18:4012/02/15 09:15
EPA 6020A 1.11 ug/L1Arsenic10.0 J 5120028EPA 3005A 0.75 7440-38-2 12/02/15 18:4012/02/15 09:15
EPA 6020A 68.9 ug/L1Barium100 J 5120028EPA 3005A 0.30 7440-39-3 12/02/15 18:4012/02/15 09:15
EPA 6020A 0.14 ug/L1Beryllium1.00 J 5120028EPA 3005A 0.09 7440-41-7 12/02/15 18:4012/02/15 09:15
NDEPA 6020A ug/L1Cadmium1.00 5120028EPA 3005A 0.10 7440-43-9 12/02/15 18:4012/02/15 09:15
EPA 6020A 2.15 ug/L1Chromium10.0 J 5120028EPA 3005A 0.43 7440-47-3 12/02/15 18:4012/02/15 09:15
EPA 6020A 1.74 ug/L1Cobalt10.0 J 5120028EPA 3005A 0.29 7440-48-4 12/02/15 18:4012/02/15 09:15
Page 51 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-SW2
Surface Water
AYK0618-13 AYK061811/19/15 08:50
Project:Lake Norman C&D Landfill
11/19/15 15:09
Metals, Total
EPA 6020A 5.48 ug/L1Copper10.0 J 5120028EPA 3005A 0.41 7440-50-8 12/02/15 18:4012/02/15 09:15
EPA 6020A 1.65 ug/L1Lead10.0 J 5120028EPA 3005A 0.08 7439-92-1 12/02/15 18:4012/02/15 09:15
EPA 6020A 1.44 ug/L1Nickel50.0 J 5120028EPA 3005A 0.48 7440-02-0 12/02/15 18:4012/02/15 09:15
NDEPA 6020A ug/L1Selenium10.0 5120028EPA 3005A 0.85 7782-49-2 12/02/15 18:4012/02/15 09:15
NDEPA 6020A ug/L1Silver10.0 5120028EPA 3005A 0.22 7440-22-4 12/02/15 18:4012/02/15 09:15
NDEPA 6020A ug/L1Thallium5.50 5120028EPA 3005A 0.06 7440-28-0 12/02/15 18:4012/02/15 09:15
EPA 6020A 15.8 ug/L1Vanadium25.0 J 5120028EPA 3005A 1.57 7440-62-2 12/02/15 18:4012/02/15 09:15
EPA 6020A 14.7 ug/L1Zinc10.0 5120028EPA 3005A 1.30 7440-66-6 12/02/15 18:4012/02/15 09:15
EPA 6020A 4480 ug/L1Iron40.0 5120028EPA 3005A 5.72 7439-89-6 12/02/15 18:4012/02/15 09:15
EPA 6020A 260 ug/L1Manganese10.0 5120028EPA 3005A 1.04 7439-96-5 12/02/15 18:4012/02/15 09:15
NDEPA 7470A ug/L1Mercury0.200 5110582EPA 7470A 0.070 7439-97-6 11/30/15 14:0311/30/15 08:20
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Acetone100 5110457EPA 5030B 3.1 67-64-1 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Acrylonitrile200 5110457EPA 5030B 2.0 107-13-1 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Benzene1.0 5110457EPA 5030B 0.2 71-43-2 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Bromochloromethane3.0 5110457EPA 5030B 0.5 74-97-5 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Bromodichloromethane1.0 5110457EPA 5030B 0.5 75-27-4 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Bromoform3.0 5110457EPA 5030B 0.5 75-25-2 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Bromomethane10 5110457EPA 5030B 0.8 74-83-9 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Carbon Disulfide 100 5110457EPA 5030B 0.5 75-15-0 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Carbon Tetrachloride 1.0 5110457EPA 5030B 0.4 56-23-5 11/20/15 15:2711/20/15 10:00
Page 52 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-SW2
Surface Water
AYK0618-13 AYK061811/19/15 08:50
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Chlorobenzene3.0 5110457EPA 5030B 0.5 108-90-7 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Chloroethane10 5110457EPA 5030B 0.6 75-00-3 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Chloroform5.0 5110457EPA 5030B 0.4 67-66-3 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Chloromethane1.0 5110457EPA 5030B 0.6 74-87-3 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Dibromochloromethane1.0 5110457EPA 5030B 0.3 124-48-1 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromo-3-chloropropane 13 5110457EPA 5030B 1.0 96-12-8 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L11,2-Dibromoethane 1.0 5110457EPA 5030B 0.4 106-93-4 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Dibromomethane10 5110457EPA 5030B 0.4 74-95-3 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L11,2-Dichlorobenzene 5.0 5110457EPA 5030B 0.2 95-50-1 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L11,4-Dichlorobenzene 1.0 5110457EPA 5030B 0.4 106-46-7 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1trans-1,4-Dichloro-2-butene 100 5110457EPA 5030B 1.1 110-57-6 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloroethane 5.0 5110457EPA 5030B 0.3 75-34-3 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloroethane 1.0 5110457EPA 5030B 0.3 107-06-2 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L11,1-Dichloroethene 5.0 5110457EPA 5030B 0.6 75-35-4 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1cis-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.3 156-59-2 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1trans-1,2-Dichloroethene 5.0 5110457EPA 5030B 0.4 156-60-5 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L11,2-Dichloropropane 1.0 5110457EPA 5030B 0.4 78-87-5 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1cis-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-01-5 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1trans-1,3-Dichloropropene 1.0 5110457EPA 5030B 0.3 10061-02-6 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Ethylbenzene1.0 5110457EPA 5030B 0.2 100-41-4 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Iodomethane10 5110457EPA 5030B 1.7 74-88-4 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Methyl Butyl Ketone
(2-Hexanone)50 5110457EPA 5030B 0.7 591-78-6 11/20/15 15:2711/20/15 10:00
Page 53 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
ResultAnalyte SWSL/
RL
Prep
Method Qual DF Units Batch
Analytical
Method MDL CAS #Prep Date/Time Analysis
Date/Time
Client ID:
Date/Time Sampled:
Matrix:
Report No.:
Lab No:
Date/Time Received:
5504-SW2
Surface Water
AYK0618-13 AYK061811/19/15 08:50
Project:Lake Norman C&D Landfill
11/19/15 15:09
Volatile Organic Compounds by EPA 8260
NDEPA 8260B ug/L1Methylene Chloride 1.0 5110457EPA 5030B 0.6 75-09-2 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Methyl Ethyl Ketone
(2-Butanone)100 5110457EPA 5030B 0.9 78-93-3 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L14-Methyl-2-pentanone (MIBK)50 5110457EPA 5030B 1.0 108-10-1 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Styrene1.0 5110457EPA 5030B 0.3 100-42-5 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L11,1,1,2-Tetrachloroethane 5.0 5110457EPA 5030B 0.4 630-20-6 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L11,1,2,2-Tetrachloroethane 1.0 5110457EPA 5030B 0.5 79-34-5 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Tetrachloroethene1.0 5110457EPA 5030B 0.4 127-18-4 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Toluene1.0 5110457EPA 5030B 0.2 108-88-3 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L11,1,1-Trichloroethane 1.0 5110457EPA 5030B 0.3 71-55-6 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L11,1,2-Trichloroethane 1.0 5110457EPA 5030B 0.4 79-00-5 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Trichloroethene1.0 5110457EPA 5030B 0.4 79-01-6 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Trichlorofluoromethane1.0 5110457EPA 5030B 0.3 75-69-4 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L11,2,3-Trichloropropane 1.0 5110457EPA 5030B 0.3 96-18-4 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Vinyl Acetate 50 5110457EPA 5030B 0.6 108-05-4 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Vinyl Chloride 1.0 5110457EPA 5030B 0.4 75-01-4 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Xylenes, total 4.0 5110457EPA 5030B 0.6 1330-20-7 11/20/15 15:2711/20/15 10:00
NDEPA 8260B ug/L1Tetrahydrofuran10 5110457EPA 5030B 1.5 109-99-9 11/20/15 15:2711/20/15 10:00
EPA 8260B 106 %Surr: Dibromofluoromethane 5110457EPA 5030B 1868-53-7 11/20/15 15:2711/20/15 10:0080-120
EPA 8260B S-09121 %Surr: 1,2-Dichloroethane-d4 5110457EPA 5030B 17060-07-0 11/20/15 15:2711/20/15 10:0078-120
EPA 8260B 98 %Surr: Toluene-d8 5110457EPA 5030B 2037-26-5 11/20/15 15:2711/20/15 10:0080-120
EPA 8260B 106 %Surr: 4-Bromofluorobenzene 5110457EPA 5030B 460-00-4 11/20/15 15:2711/20/15 10:0080-120
Page 54 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
General Chemistry - Quality Control
Batch 5110534 - SM 4500-S D
Blank (5110534-BLK1)Prepared & Analyzed: 11/24/15
Total Sulfide ug/LND200
LCS (5110534-BS1)Prepared & Analyzed: 11/24/15
Total Sulfide ug/L511200 476.00 80-120107
Matrix Spike (5110534-MS1)Prepared & Analyzed: 11/24/15 Source: AYK0638-01
Total Sulfide ug/L1190200 476.00 ND QM-0530-129250
Matrix Spike Dup (5110534-MSD1)Prepared & Analyzed: 11/24/15 Source: AYK0638-01
Total Sulfide ug/L989200 476.00 ND 10 QM-0530-129208 18.4
Batch 5110550 - SM 2540 C
Blank (5110550-BLK1)Prepared & Analyzed: 11/25/15
Total Dissolved Solids ug/LND10000
LCS (5110550-BS1)Prepared & Analyzed: 11/25/15
Total Dissolved Solids ug/L41100010000 400000 84-108103
Duplicate (5110550-DUP1)Prepared & Analyzed: 11/25/15 Source: AYK0620-02
Total Dissolved Solids ug/L65200010000 646000 100.9
Duplicate (5110550-DUP2)Prepared & Analyzed: 11/25/15 Source: AYK0648-05
Total Dissolved Solids ug/L11200010000 154000 10 QR-0332
Batch 5110597 - SM 2320 B
Blank (5110597-BLK1)Prepared & Analyzed: 11/30/15
Alkalinity as CaCO3 ug/LND1000
Page 55 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
General Chemistry - Quality Control
Batch 5110597 - SM 2320 B
LCS (5110597-BS1)Prepared & Analyzed: 11/30/15
Alkalinity as CaCO3 ug/L910001000 100000 85-11591
Duplicate (5110597-DUP1)Prepared & Analyzed: 11/30/15 Source: AYK0620-01
Alkalinity as CaCO3 ug/L1520001000 147000 103
Batch 5110601 - EPA 9010
Blank (5110601-BLK1)Prepared & Analyzed: 11/30/15
Cyanide, Total ug/LND10.0
LCS (5110601-BS1)Prepared & Analyzed: 11/30/15
Cyanide, Total ug/L74.0 10.0 80.000 85-11592
Duplicate (5110601-DUP1)Prepared & Analyzed: 11/30/15 Source: AYK0497-02RE1
Cyanide, Total ug/L12610.0 123 202
Matrix Spike (5110601-MS1)Prepared & Analyzed: 11/30/15 Source: AYK0676-02
Cyanide, Total ug/L71.0 10.0 80.000 ND 85-11989
Matrix Spike Dup (5110601-MSD1)Prepared & Analyzed: 11/30/15 Source: AYK0676-02
Cyanide, Total ug/L69.0 10.0 80.000 ND 1385-11986 3
Page 56 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Inorganic Anions - Quality Control
Batch 5110537 - EPA 9056A
Blank (5110537-BLK1)Prepared & Analyzed: 11/24/15
Chloride ug/LND1000
Sulfate ug/LND5000
LCS (5110537-BS1)Prepared & Analyzed: 11/24/15
Chloride ug/L99801000 10000 90-110100
Sulfate ug/L101005000 10000 90-110101
Matrix Spike (5110537-MS1)Prepared & Analyzed: 11/24/15 Source: AYK0618-12
Chloride ug/L144001000 10000 5050 90-11093
Sulfate ug/L147005000 10000 5590 90-11091
Matrix Spike (5110537-MS2)Prepared & Analyzed: 11/24/15 Source: AYK0618-13
Chloride ug/L117001000 10000 2560 90-11092
Sulfate ug/L185005000 10000 9970 90-11085
Matrix Spike Dup (5110537-MSD1)Prepared & Analyzed: 11/24/15 Source: AYK0618-12
Chloride ug/L143001000 10000 5050 1590-11092 0.6
Sulfate ug/L146005000 10000 5590 1590-11090 0.3
Page 57 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 5110582 - EPA 7470A
Blank (5110582-BLK1)Prepared & Analyzed: 11/30/15
Mercury ug/LND0.200
LCS (5110582-BS1)Prepared & Analyzed: 11/30/15
Mercury ug/L2.38 0.200 2.5000 80-12095
Duplicate (5110582-DUP1)Prepared & Analyzed: 11/30/15 Source: AYK0737-02
Mercury ug/LND0.200 0.073 20
Matrix Spike (5110582-MS1)Prepared & Analyzed: 11/30/15 Source: AYK0618-02
Mercury ug/L2.41 0.200 2.5000 ND 75-12597
Matrix Spike Dup (5110582-MSD1)Prepared & Analyzed: 11/30/15 Source: AYK0618-02
Mercury ug/L2.30 0.200 2.5000 ND 2075-12592 5
Post Spike (5110582-PS1)Prepared & Analyzed: 11/30/15 Source: AYK0618-02
Mercury ug/L1.54 1.6667 0.026 80-12091
Batch 5120028 - EPA 3005A
Blank (5120028-BLK1)Prepared & Analyzed: 12/02/15
Antimony ug/LND6.00
Arsenic ug/LND10.0
Barium ug/LND100
Beryllium ug/LND1.00
Cadmium ug/LND1.00
Chromium ug/LND10.0
Cobalt ug/LND10.0
Copper ug/LND10.0
Page 58 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 5120028 - EPA 3005A
Blank (5120028-BLK1)Prepared & Analyzed: 12/02/15
Iron ug/LND40.0
Lead ug/LND10.0
Manganese ug/LND10.0
Nickel ug/LND50.0
Selenium ug/LND10.0
Silver ug/LND10.0
Thallium ug/LND5.50
Vanadium ug/LND25.0
Zinc ug/LND10.0
LCS (5120028-BS1)Prepared & Analyzed: 12/02/15
Antimony ug/L1006.00 100.00 80-120100
Arsenic ug/L97.3 10.0 100.00 80-12097
Barium ug/L98.3 100 100.00 J80-12098
Beryllium ug/L1061.00 100.00 80-120106
Cadmium ug/L1031.00 100.00 80-120103
Chromium ug/L98.2 10.0 100.00 80-12098
Cobalt ug/L99.3 10.0 100.00 80-12099
Copper ug/L97.9 10.0 100.00 80-12098
Iron ug/L98540.0 1000.0 80-12099
Lead ug/L97.9 10.0 100.00 80-12098
Manganese ug/L99.2 10.0 100.00 80-12099
Nickel ug/L98.2 50.0 100.00 80-12098
Selenium ug/L10510.0 100.00 80-120105
Silver ug/L10110.0 100.00 80-120101
Thallium ug/L97.2 5.50 100.00 80-12097
Vanadium ug/L10225.0 100.00 80-120102
Page 59 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 5120028 - EPA 3005A
LCS (5120028-BS1)Prepared & Analyzed: 12/02/15
Zinc ug/L10410.0 100.00 80-120104
Matrix Spike (5120028-MS1)Prepared & Analyzed: 12/02/15 Source: AYK0618-01
Antimony ug/L1006.00 100.00 0.87 75-125100
Arsenic ug/L97.1 10.0 100.00 0.88 75-12596
Barium ug/L166100 100.00 72.6 75-12594
Beryllium ug/L1161.00 100.00 ND 75-125116
Cadmium ug/L99.5 1.00 100.00 ND 75-125100
Chromium ug/L10310.0 100.00 ND 75-125103
Cobalt ug/L10010.0 100.00 ND 75-125100
Copper ug/L10110.0 100.00 1.31 75-12599
Iron ug/L98840.0 1000.0 5.90 75-12598
Lead ug/L10210.0 100.00 ND 75-125102
Manganese ug/L10210.0 100.00 3.74 75-12598
Nickel ug/L10050.0 100.00 ND 75-125100
Selenium ug/L10110.0 100.00 ND 75-125101
Silver ug/L97.7 10.0 100.00 ND 75-12598
Thallium ug/L1015.50 100.00 0.14 75-125101
Vanadium ug/L11025.0 100.00 4.92 75-125105
Zinc ug/L10110.0 100.00 ND 75-125101
Matrix Spike Dup (5120028-MSD1)Prepared & Analyzed: 12/02/15 Source: AYK0618-01
Antimony ug/L1026.00 100.00 0.87 2075-125101 1
Arsenic ug/L94.1 10.0 100.00 0.88 2075-12593 3
Barium ug/L170100 100.00 72.6 2075-12598 2
Beryllium ug/L1121.00 100.00 ND 2075-125112 3
Cadmium ug/L97.1 1.00 100.00 ND 2075-12597 2
Page 60 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 5120028 - EPA 3005A
Matrix Spike Dup (5120028-MSD1)Prepared & Analyzed: 12/02/15 Source: AYK0618-01
Chromium ug/L10310.0 100.00 ND 2075-125103 0.5
Cobalt ug/L10110.0 100.00 ND 2075-125101 0.9
Copper ug/L98.8 10.0 100.00 1.31 2075-12598 2
Iron ug/L101040.0 1000.0 5.90 2075-125100 2
Lead ug/L96.1 10.0 100.00 ND 2075-12596 6
Manganese ug/L10410.0 100.00 3.74 2075-125101 3
Nickel ug/L99.2 50.0 100.00 ND 2075-12599 1
Selenium ug/L10410.0 100.00 ND 2075-125104 3
Silver ug/L10210.0 100.00 ND 2075-125102 4
Thallium ug/L97.2 5.50 100.00 0.14 2075-12597 4
Vanadium ug/L11325.0 100.00 4.92 2075-125108 2
Zinc ug/L10210.0 100.00 ND 2075-125102 1
Post Spike (5120028-PS1)Prepared & Analyzed: 12/02/15 Source: AYK0618-01
Antimony ug/L94.0 100.00 0.87 80-12093
Arsenic ug/L94.5 100.00 0.88 80-12094
Barium ug/L166 100.00 72.6 80-12094
Beryllium ug/L112 100.00 0.0006 80-120112
Cadmium ug/L98.9 100.00 0.008 80-12099
Chromium ug/L104 100.00 0.004 80-120104
Cobalt ug/L106 100.00 0.19 80-120106
Copper ug/L99.3 100.00 1.31 80-12098
Iron ug/L1050 1000.0 5.90 80-120104
Lead ug/L99.8 100.00 -0.003 80-120100
Manganese ug/L106 100.00 3.74 80-120102
Nickel ug/L102 100.00 0.13 80-120101
Selenium ug/L103 100.00 -0.11 80-120103
Page 61 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Metals, Total - Quality Control
Batch 5120028 - EPA 3005A
Post Spike (5120028-PS1)Prepared & Analyzed: 12/02/15 Source: AYK0618-01
Silver ug/L104 100.00 0.02 80-120104
Thallium ug/L98.3 100.00 0.14 80-12098
Vanadium ug/L113 100.00 4.92 80-120108
Zinc ug/L105 100.00 1.09 80-120104
Page 62 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 5110457 - EPA 5030B
Blank (5110457-BLK1)Prepared & Analyzed: 11/20/15
Acetone ug/LND100
Acetone ug/LND100
Acetonitrile ug/LND55
Acrolein ug/LND53
Acrylonitrile ug/LND200
Acrylonitrile ug/LND200
Benzene ug/LND1.0
Benzene ug/LND1.0
Bromochloromethane ug/LND3.0
Bromochloromethane ug/LND3.0
Bromodichloromethane ug/LND1.0
Bromodichloromethane ug/LND1.0
Bromoform ug/LND3.0
Bromoform ug/LND3.0
Bromomethane ug/LND10
Bromomethane ug/LND10
Carbon Disulfide ug/LND100
Carbon Disulfide ug/LND100
Carbon Tetrachloride ug/LND1.0
Carbon Tetrachloride ug/LND1.0
Chlorobenzene ug/LND3.0
Chlorobenzene ug/LND3.0
Chloroprene
(2-Chloro-1,3-butadiene)
ug/LND20
Chloroethane ug/LND10
Chloroethane ug/LND10
Chloroform ug/LND5.0
Page 63 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 5110457 - EPA 5030B
Blank (5110457-BLK1)Prepared & Analyzed: 11/20/15
Chloroform ug/LND5.0
Chloromethane ug/LND1.0
Chloromethane ug/LND1.0
Allyl Chloride (3-Chloropropylene)ug/LND10
Dibromochloromethane ug/LND3.0
Dibromochloromethane ug/LND1.0
1,2-Dibromo-3-chloropropane ug/LND13
1,2-Dibromo-3-chloropropane ug/LND13
1,2-Dibromoethane ug/LND1.0
1,2-Dibromoethane ug/LND1.0
Dibromomethane ug/LND10
Dibromomethane ug/LND10
1,2-Dichlorobenzene ug/LND5.0
1,2-Dichlorobenzene ug/LND5.0
1,3-Dichlorobenzene ug/LND5.0
1,4-Dichlorobenzene ug/LND1.0
1,4-Dichlorobenzene ug/LND1.0
trans-1,4-Dichloro-2-butene ug/LND100
trans-1,4-Dichloro-2-butene ug/LND100
Dichlorodifluoromethane ug/LND5.0
1,1-Dichloroethane ug/LND5.0
1,1-Dichloroethane ug/LND5.0
1,2-Dichloroethane ug/LND1.0
1,2-Dichloroethane ug/LND1.0
1,1-Dichloroethene ug/LND5.0
1,1-Dichloroethene ug/LND5.0
cis-1,2-Dichloroethene ug/LND5.0
Page 64 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 5110457 - EPA 5030B
Blank (5110457-BLK1)Prepared & Analyzed: 11/20/15
cis-1,2-Dichloroethene ug/LND5.0
trans-1,2-Dichloroethene ug/LND5.0
trans-1,2-Dichloroethene ug/LND5.0
1,2-Dichloropropane ug/LND1.0
1,2-Dichloropropane ug/LND1.0
1,3-Dichloropropane ug/LND1.0
2,2-Dichloropropane ug/LND15
1,1-Dichloropropene ug/LND5.0
cis-1,3-Dichloropropene ug/LND1.0
cis-1,3-Dichloropropene ug/LND1.0
trans-1,3-Dichloropropene ug/LND1.0
trans-1,3-Dichloropropene ug/LND1.0
Ethylbenzene ug/LND1.0
Ethylbenzene ug/LND1.0
Propionitrile (Ethyl Cyanide)ug/LND150
Ethyl Methacrylate ug/LND10
Iodomethane ug/LND10
Iodomethane ug/LND10
Isobutyl Alcohol ug/LND100
Methacrylonitrile ug/LND100
Methyl Butyl Ketone (2-Hexanone)ug/LND50
Methyl Butyl Ketone (2-Hexanone)ug/LND50
Methylene Chloride ug/LND1.0
Methylene Chloride ug/LND1.0
Methyl Ethyl Ketone (2-Butanone)ug/LND100
Methyl Ethyl Ketone (2-Butanone)ug/LND100
Methyl Methacrylate ug/LND30
Page 65 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 5110457 - EPA 5030B
Blank (5110457-BLK1)Prepared & Analyzed: 11/20/15
4-Methyl-2-pentanone (MIBK)ug/LND100
4-Methyl-2-pentanone (MIBK)ug/LND50
Styrene ug/LND1.0
Styrene ug/LND1.0
1,1,1,2-Tetrachloroethane ug/LND5.0
1,1,1,2-Tetrachloroethane ug/LND5.0
1,1,2,2-Tetrachloroethane ug/LND1.0
1,1,2,2-Tetrachloroethane ug/LND3.0
Tetrachloroethene ug/LND1.0
Tetrachloroethene ug/LND1.0
Toluene ug/LND1.0
Toluene ug/LND1.0
1,1,1-Trichloroethane ug/LND1.0
1,1,1-Trichloroethane ug/LND1.0
1,1,2-Trichloroethane ug/LND1.0
1,1,2-Trichloroethane ug/LND1.0
Trichloroethene ug/LND1.0
Trichloroethene ug/LND1.0
Trichlorofluoromethane ug/LND1.0
Trichlorofluoromethane ug/LND1.0
1,2,3-Trichloropropane ug/LND1.0
1,2,3-Trichloropropane ug/LND1.0
Vinyl Acetate ug/LND50
Vinyl Acetate ug/LND50
Vinyl Chloride ug/LND1.0
Vinyl Chloride ug/LND1.0
Xylenes, total ug/LND5.0
Page 66 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 5110457 - EPA 5030B
Blank (5110457-BLK1)Prepared & Analyzed: 11/20/15
Xylenes, total ug/LND4.0
Tetrahydrofuran ug/LND10
Tetrahydrofuran ug/LND10
ug/L 50.000 80-120Surr: Dibromofluoromethane 10251
ug/L 50.000 80-120Surr: Dibromofluoromethane 10251
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 11457
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 11457
ug/L 50.000 80-120Surr: Toluene-d8 9949
ug/L 50.000 80-120Surr: Toluene-d8 9949
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10452
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10452
LCS (5110457-BS1)Prepared & Analyzed: 11/20/15
Benzene ug/L47 50.000 67-13494
Benzene ug/L47 50.000 67-13494
Chlorobenzene ug/L45 50.000 69-12291
Chlorobenzene ug/L45 50.000 69-12291
1,1-Dichloroethene ug/L40 50.000 58-14281
1,1-Dichloroethene ug/L40 50.000 58-14281
Toluene ug/L47 50.000 68-12795
Toluene ug/L47 50.000 68-12795
Trichloroethene ug/L48 50.000 72-13295
Trichloroethene ug/L48 50.000 72-13295
Tetrahydrofuran ug/LND10 62-144
ug/L 50.000 80-120Surr: Dibromofluoromethane 10352
Page 67 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 5110457 - EPA 5030B
LCS (5110457-BS1)Prepared & Analyzed: 11/20/15
ug/L 50.000 80-120Surr: Dibromofluoromethane 10352
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 11457
ug/L 50.000 78-120Surr: 1,2-Dichloroethane-d4 11457
ug/L 50.000 80-120Surr: Toluene-d8 9849
ug/L 50.000 80-120Surr: Toluene-d8 9849
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10352
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10352
Matrix Spike (5110457-MS1)Prepared & Analyzed: 11/20/15 Source: AYK0618-01
Benzene ug/L49 50.000 ND 67-13497
Benzene ug/L49 50.000 ND 67-13497
Chlorobenzene ug/L46 50.000 ND 69-12292
Chlorobenzene ug/L46 50.000 ND 69-12292
1,1-Dichloroethene ug/L47 50.000 ND 58-14294
1,1-Dichloroethene ug/L47 50.000 ND 58-14294
Toluene ug/L49 50.000 ND 68-12798
Toluene ug/L49 50.000 ND 68-12798
Trichloroethene ug/L49 50.000 ND 72-13299
Trichloroethene ug/L49 50.000 ND 72-13299
Tetrahydrofuran ug/LND10 ND 62-144
Tetrahydrofuran ug/LND10 ND 62-144
ug/L 50.000 80-120Surr: Dibromofluoromethane 10251
ug/L 50.000 80-120Surr: Dibromofluoromethane 10251
ug/L 50.000 S-0978-120Surr: 1,2-Dichloroethane-d4 12160
ug/L 50.000 S-0978-120Surr: 1,2-Dichloroethane-d4 12160
Page 68 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 5110457 - EPA 5030B
Matrix Spike (5110457-MS1)Prepared & Analyzed: 11/20/15 Source: AYK0618-01
ug/L 50.000 80-120Surr: Toluene-d8 9547
ug/L 50.000 80-120Surr: Toluene-d8 9547
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10653
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10653
Matrix Spike Dup (5110457-MSD1)Prepared & Analyzed: 11/20/15 Source: AYK0618-01
Benzene ug/L49 50.000 ND 967-13497 0.1
Benzene ug/L49 50.000 ND 967-13497 0.1
Chlorobenzene ug/L46 50.000 ND 1369-12291 1
Chlorobenzene ug/L46 50.000 ND 1369-12291 1
1,1-Dichloroethene ug/L46 50.000 ND 958-14292 2
1,1-Dichloroethene ug/L46 50.000 ND 958-14292 2
Toluene ug/L49 50.000 ND 968-12798 0.3
Toluene ug/L49 50.000 ND 968-12798 0.3
Trichloroethene ug/L47 50.000 ND 1172-13294 5
Trichloroethene ug/L47 50.000 ND 1172-13294 5
Tetrahydrofuran ug/LND10 ND 5362-144
Tetrahydrofuran ug/LND10 ND 5362-144
ug/L 50.000 80-120Surr: Dibromofluoromethane 10352
ug/L 50.000 80-120Surr: Dibromofluoromethane 10352
ug/L 50.000 S-0978-120Surr: 1,2-Dichloroethane-d4 12161
ug/L 50.000 S-0978-120Surr: 1,2-Dichloroethane-d4 12161
ug/L 50.000 80-120Surr: Toluene-d8 9849
ug/L 50.000 80-120Surr: Toluene-d8 9849
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10251
Page 69 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Volatile Organic Compounds by EPA 8260 - Quality Control
Batch 5110457 - EPA 5030B
Matrix Spike Dup (5110457-MSD1)Prepared & Analyzed: 11/20/15 Source: AYK0618-01
ug/L 50.000 80-120Surr: 4-Bromofluorobenzene 10251
Page 70 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by EPA 8270 - Quality Control
Batch 5110519 - EPA 3510C
Blank (5110519-BLK1)Prepared & Analyzed: 11/24/15
Acenaphthene ug/LND10
Acenaphthylene ug/LND10
Acetophenone ug/LND10
2-Acetylaminofluorene ug/LND20
4-Aminobiphenyl ug/LND20
Anthracene ug/LND10
Benzo(a)anthracene ug/LND10
Benzo(b)fluoranthene ug/LND10
Benzo(k)fluoranthene ug/LND10
Benzo(ghi)perylene ug/LND10
Benzo(a)pyrene ug/LND10
Benzyl alcohol ug/LND20
4-Bromophenyl phenyl ether ug/LND10
Benzyl butyl phthalate ug/LND10
4-Chloro-3-methylphenol ug/LND20
4-Chloroaniline ug/LND20
Chlorobenzilate ug/LND10
Bis(2-chloroethoxy)methane ug/LND10
Bis(2-chloroisopropyl)ether ug/LND10
Bis(2-chloroethyl)ether ug/LND10
2-Chloronaphthalene ug/LND10
2-Chlorophenol ug/LND10
4-Chlorophenyl phenyl ether ug/LND10
Chrysene ug/LND10
Diallate ug/LND10
Dibenzo(a,h)anthracene ug/LND10
Dibenzofuran ug/LND10
Page 71 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by EPA 8270 - Quality Control
Batch 5110519 - EPA 3510C
Blank (5110519-BLK1)Prepared & Analyzed: 11/24/15
3,3´-Dichlorobenzidine ug/LND20
Di-n-butyl phthalate ug/LND10
1,3-Dinitrobenzene ug/LND20
2,4-Dichlorophenol ug/LND10
2,6-Dichlorophenol ug/LND10
Diethyl phthalate ug/LND10
Dimethoate ug/LND20
3,3'-Dimethylbenzidine ug/LND10
7,12-Dimethylbenz(a)anthracene ug/LND10
4-Dimethylaminoazobenzene ug/LND10
2,4-Dimethylphenol ug/LND10
Dimethyl phthalate ug/LND10
4,6-Dinitro-2-methylphenol ug/LND50
2,4-Dinitrophenol ug/LND50
2,4-Dinitrotoluene ug/LND10
2,6-Dinitrotoluene ug/LND10
Di-n-octyl phthalate ug/LND10
Disulfoton ug/LND10
Bis(2-ethylhexyl)phthalate ug/LND15
Ethyl Methanesulfonate ug/LND20
Famphur ug/LND20
Fluoranthene ug/LND10
Fluorene ug/LND10
Hexachlorobenzene ug/LND10
Hexachlorobutadiene ug/LND10
Hexachlorocyclopentadiene ug/LND10
Hexachloroethane ug/LND10
Page 72 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by EPA 8270 - Quality Control
Batch 5110519 - EPA 3510C
Blank (5110519-BLK1)Prepared & Analyzed: 11/24/15
Hexachloropropene ug/LND10
Indeno(1,2,3-cd)pyrene ug/LND10
Isophorone ug/LND10
Isosafrole ug/LND10
Kepone ug/LND20
Methapyrilene ug/LND100
3-Methylcholanthrene ug/LND10
Methyl Methanesulfonate ug/LND10
2-Methylnaphthalene ug/LND10
Methyl Parathion ug/LND10
2-Methylphenol (o-cresol)ug/LND10
3+4-Methylphenol (m+p-cresol)ug/LND10
Naphthalene ug/LND10
1,4-Naphthoquinone ug/LND10
1-Naphthylamine ug/LND10
2-Naphthylamine ug/LND10
2-Nitroaniline ug/LND50
3-Nitroaniline ug/LND50
Nitrobenzene ug/LND10
4-Nitroaniline ug/LND20
2-Nitrophenol ug/LND10
4-Nitrophenol ug/LND50
N-Nitrosodi-n-butylamine ug/LND10
N-Nitrosodiethylamine ug/LND20
N-Nitrosodimethylamine ug/LND10
N-Nitrosodi-n-propylamine ug/LND10
Page 73 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by EPA 8270 - Quality Control
Batch 5110519 - EPA 3510C
Blank (5110519-BLK1)Prepared & Analyzed: 11/24/15
N-Nitrosodiphenylamine/Diphenyla
mine
ug/LND10
N-Nitrosomethylethylamine ug/LND10
N-Nitrosopiperidine ug/LND20
N-Nitrosopyrrolidine ug/LND10
5-Nitro-o-toluidine ug/LND10
Parathion ug/LND10
Pentachlorobenzene ug/LND10
Pentachloronitrobenzene ug/LND20
Pentachlorophenol ug/LND25
Phenacetin ug/LND20
Phenanthrene ug/LND10
Phenol ug/LND10
p-Phenylenediamine ug/LND10
Phorate ug/LND10
Pronamide ug/LND10
Pyrene ug/LND10
Safrole ug/LND10
1,2,4,5-Tetrachlorobenzene ug/LND10
2,3,4,6+2,3,4,5-Tetrachlorophenol ug/LND10
Thionazin ug/LND20
o-Toluidine ug/LND10
1,2,4-Trichlorobenzene ug/LND10
O,O,O-Triethyl phosphorothioate ug/LND10
2,4,5-Trichlorophenol ug/LND10
2,4,6-Trichlorophenol ug/LND10
1,3,5-Trinitrobenzene ug/LND10
Page 74 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by EPA 8270 - Quality Control
Batch 5110519 - EPA 3510C
Blank (5110519-BLK1)Prepared & Analyzed: 11/24/15
ug/L 100.00 11-120Surr: 2-Fluorophenol 3535
ug/L 100.00 10-120Surr: Phenol-d6 2222
ug/L 50.000 15-120Surr: Nitrobenzene-d5 5929
ug/L 50.000 23-120Surr: 2-Fluorobiphenyl 6131
ug/L 100.00 36-120Surr: 2,4,6-Tribromophenol 6666
ug/L 50.000 53-121Surr: p-Terphenyl-dl4 7940
LCS (5110519-BS1)Prepared & Analyzed: 11/24/15
Acenaphthene ug/L4210 50.000 47-12084
4-Chloro-3-methylphenol ug/L8020 100.00 43-12080
2-Chlorophenol ug/L6810 100.00 30-12068
2,4-Dinitrotoluene ug/L4710 50.000 55-12094
4-Nitrophenol ug/L2350 100.00 14-12023
N-Nitrosodi-n-propylamine ug/L4810 50.000 38-12096
Pentachlorophenol ug/L8525 100.00 47-12085
Phenol ug/L2910 100.00 12-12029
Pyrene ug/L4910 50.000 53-12097
1,2,4-Trichlorobenzene ug/L2910 50.000 29-12058
ug/L 100.00 11-120Surr: 2-Fluorophenol 3434
ug/L 100.00 10-120Surr: Phenol-d6 2424
ug/L 50.000 23-120Surr: 2-Fluorobiphenyl 6834
ug/L 100.00 36-120Surr: 2,4,6-Tribromophenol 8383
ug/L 50.000 15-120Surr: Nitrobenzene-d5 6532
ug/L 50.000 53-121Surr: p-Terphenyl-dl4 8643
Page 75 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by EPA 8270 - Quality Control
Batch 5110519 - EPA 3510C
Matrix Spike (5110519-MS1)Prepared & Analyzed: 11/24/15 Source: AYK0618-04
Acenaphthene ug/L3410 50.000 ND 40-12068
4-Chloro-3-methylphenol ug/L6420 100.00 ND 45-12064
2-Chlorophenol ug/L5610 100.00 ND 33-12056
2,4-Dinitrotoluene ug/L3510 50.000 ND 46-12271
4-Nitrophenol ug/L1650 100.00 ND 15-12016
N-Nitrosodi-n-propylamine ug/L3910 50.000 ND 35-12077
Pentachlorophenol ug/L6125 100.00 ND 40-12061
Phenol ug/L2910 100.00 ND 12-12029
Pyrene ug/L4210 50.000 ND 54-12084
1,2,4-Trichlorobenzene ug/L2210 50.000 ND 12-12045
ug/L 100.00 11-120Surr: 2-Fluorophenol 3333
ug/L 100.00 10-120Surr: Phenol-d6 2424
ug/L 50.000 23-120Surr: 2-Fluorobiphenyl 5527
ug/L 50.000 15-120Surr: Nitrobenzene-d5 5025
ug/L 100.00 36-120Surr: 2,4,6-Tribromophenol 6565
ug/L 50.000 53-121Surr: p-Terphenyl-dl4 7537
Matrix Spike Dup (5110519-MSD1)Prepared & Analyzed: 11/24/15 Source: AYK0618-04
Acenaphthene ug/L3810 50.000 ND 2940-12077 12
4-Chloro-3-methylphenol ug/L6920 100.00 ND 2945-12069 8
2-Chlorophenol ug/L6310 100.00 ND 3233-12063 12
2,4-Dinitrotoluene ug/L3910 50.000 ND 2646-12277 9
4-Nitrophenol ug/L1850 100.00 ND 3515-12018 13
N-Nitrosodi-n-propylamine ug/L4010 50.000 ND 2835-12080 3
Pentachlorophenol ug/L6625 100.00 ND 2740-12066 8
Phenol ug/L3310 100.00 ND 3012-12033 13
Page 76 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Semivolatile Organic Compounds by EPA 8270 - Quality Control
Batch 5110519 - EPA 3510C
Matrix Spike Dup (5110519-MSD1)Prepared & Analyzed: 11/24/15 Source: AYK0618-04
Pyrene ug/L4410 50.000 ND 2154-12088 5
1,2,4-Trichlorobenzene ug/L2510 50.000 ND 3212-12051 13
ug/L 100.00 11-120Surr: 2-Fluorophenol 3939
ug/L 100.00 10-120Surr: Phenol-d6 2828
ug/L 50.000 15-120Surr: Nitrobenzene-d5 5628
ug/L 50.000 23-120Surr: 2-Fluorobiphenyl 6030
ug/L 100.00 36-120Surr: 2,4,6-Tribromophenol 7171
ug/L 50.000 53-121Surr: p-Terphenyl-dl4 7839
Page 77 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Organochlorine Pesticides by EPA 8081 - Quality Control
Batch 5110522 - EPA 3510C
Blank (5110522-BLK1)Prepared & Analyzed: 11/24/15
Aldrin ug/LND0.05
BHC-alpha ug/LND0.05
BHC-beta ug/LND0.05
BHC-delta ug/LND0.05
BHC-gamma (Lindane)ug/LND0.05
Chlordane ug/LND0.5
4,4'-DDD ug/LND0.1
4,4'-DDE ug/LND0.1
4,4'-DDT ug/LND0.1
Dieldrin ug/LND0.08
Endosulfan I ug/LND0.1
Endosulfan II ug/LND0.1
Endosulfan sulfate ug/LND0.1
Endrin ug/LND0.1
Endrin aldehyde ug/LND0.1
Heptachlor ug/LND0.05
Heptachlor epoxide ug/LND0.08
Isodrin ug/LND20
Methoxychlor ug/LND1.0
Toxaphene ug/LND1.5
ug/L 1.0000 27-148Surr: Tetrachloro-m-xylene 850.855
ug/L 1.0000 10-155Surr: Decachlorobiphenyl 490.492
LCS (5110522-BS1)Prepared & Analyzed: 11/24/15
Aldrin ug/L2.4 0.05 2.5000 42-15395
BHC-alpha ug/L2.3 0.05 2.5000 54-14393
Page 78 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Organochlorine Pesticides by EPA 8081 - Quality Control
Batch 5110522 - EPA 3510C
LCS (5110522-BS1)Prepared & Analyzed: 11/24/15
BHC-beta ug/L2.7 0.05 2.5000 60-153107
BHC-delta ug/L2.1 0.05 2.5000 55-13683
BHC-gamma (Lindane)ug/L2.3 0.05 2.5000 53-14691
4,4'-DDD ug/L2.4 0.1 2.5000 61-16795
4,4'-DDE ug/L2.3 0.1 2.5000 57-16894
4,4'-DDT ug/L2.2 0.1 2.5000 38-19188
Dieldrin ug/L2.3 0.08 2.5000 61-15192
Endosulfan I ug/L2.4 0.1 2.5000 57-15497
Endosulfan II ug/L2.3 0.1 2.5000 58-16493
Endosulfan sulfate ug/L2.1 0.1 2.5000 59-16783
Endrin ug/L2.4 0.1 2.5000 43-16595
Endrin aldehyde ug/L2.0 0.1 2.5000 44-15380
Heptachlor ug/L2.4 0.05 2.5000 51-16196
Heptachlor epoxide ug/L2.4 0.08 2.5000 62-15695
Isodrin ug/L2.6 20 2.5000 57-151105
ug/L 1.0000 27-148Surr: Tetrachloro-m-xylene 960.963
ug/L 1.0000 10-155Surr: Decachlorobiphenyl 460.460
Matrix Spike (5110522-MS1)Prepared & Analyzed: 11/24/15 Source: AYK0618-04
Aldrin ug/L2.4 0.05 2.5000 ND 18-14896
BHC-alpha ug/L2.2 0.05 2.5000 ND 15-16788
BHC-beta ug/L2.6 0.05 2.5000 ND 10-174102
BHC-delta ug/L1.9 0.05 2.5000 ND 27-14275
BHC-gamma (Lindane)ug/L2.1 0.05 2.5000 ND 27-14385
4,4'-DDD ug/L2.2 0.1 2.5000 ND 36-16188
4,4'-DDE ug/L2.2 0.1 2.5000 ND 10-18986
Page 79 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Organochlorine Pesticides by EPA 8081 - Quality Control
Batch 5110522 - EPA 3510C
Matrix Spike (5110522-MS1)Prepared & Analyzed: 11/24/15 Source: AYK0618-04
4,4'-DDT ug/L2.0 0.1 2.5000 ND 10-18679
Dieldrin ug/L2.2 0.08 2.5000 ND 31-15387
Endosulfan I ug/L2.5 0.1 2.5000 ND 20-16299
Endosulfan II ug/L2.1 0.1 2.5000 ND 36-15786
Endosulfan sulfate ug/L1.9 0.1 2.5000 ND 15-18475
Endrin ug/L2.3 0.1 2.5000 ND 28-17790
Endrin aldehyde ug/L1.9 0.1 2.5000 ND 10-15277
Heptachlor ug/L2.4 0.05 2.5000 ND 25-16096
Heptachlor epoxide ug/L2.3 0.08 2.5000 ND 35-15292
Isodrin ug/L2.6 20 2.5000 ND 10-164104
ug/L 1.0000 27-148Surr: Tetrachloro-m-xylene 1031.03
ug/L 1.0000 10-155Surr: Decachlorobiphenyl 610.610
Matrix Spike Dup (5110522-MSD1)Prepared & Analyzed: 11/24/15 Source: AYK0618-04
Aldrin ug/L2.4 0.05 2.5000 ND 3918-14897 0.7
BHC-alpha ug/L2.3 0.05 2.5000 ND 4015-16793 5
BHC-beta ug/L2.6 0.05 2.5000 ND 4710-174106 3
BHC-delta ug/L2.2 0.05 2.5000 ND 4227-14289 17
BHC-gamma (Lindane)ug/L2.4 0.05 2.5000 ND 3227-14395 11
4,4'-DDD ug/L2.6 0.1 2.5000 ND 3236-161104 17
4,4'-DDE ug/L2.5 0.1 2.5000 ND 4310-189102 17
4,4'-DDT ug/L2.5 0.1 2.5000 ND 4210-18699 22
Dieldrin ug/L2.5 0.08 2.5000 ND 4431-15399 13
Endosulfan I ug/L2.6 0.1 2.5000 ND 3320-162106 7
Endosulfan II ug/L2.6 0.1 2.5000 ND 3136-157102 18
Endosulfan sulfate ug/L2.3 0.1 2.5000 ND 3715-18493 21
Page 80 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Organochlorine Pesticides by EPA 8081 - Quality Control
Batch 5110522 - EPA 3510C
Matrix Spike Dup (5110522-MSD1)Prepared & Analyzed: 11/24/15 Source: AYK0618-04
Endrin ug/L2.6 0.1 2.5000 ND 3028-177105 15
Endrin aldehyde ug/L2.4 0.1 2.5000 ND 3710-15295 21
Heptachlor ug/L2.4 0.05 2.5000 ND 4225-16097 1
Heptachlor epoxide ug/L2.6 0.08 2.5000 ND 3435-152102 11
Isodrin ug/L2.7 20 2.5000 ND 3310-164107 3
ug/L 1.0000 27-148Surr: Tetrachloro-m-xylene 990.994
ug/L 1.0000 10-155Surr: Decachlorobiphenyl 730.727
Page 81 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
PCBs by EPA 8082 - Quality Control
Batch 5110524 - EPA 3510C
Blank (5110524-BLK1)Prepared & Analyzed: 11/24/15
PCB 1016 ug/LND2.0
PCB 1221 ug/LND2.0
PCB 1232 ug/LND2.0
PCB 1242 ug/LND2.0
PCB 1248 ug/LND2.0
PCB 1254 ug/LND2.0
PCB 1260 ug/LND2.0
ug/L 1.0000 17-144Surr: Decachlorobiphenyl 400.399
LCS (5110524-BS1)Prepared & Analyzed: 11/24/15
PCB 1016 ug/L4.9 2.0 5.0000 47-12099
PCB 1260 ug/L4.8 2.0 5.0000 51-12696
ug/L 1.0000 17-144Surr: Decachlorobiphenyl 480.482
Matrix Spike (5110524-MS1)Prepared & Analyzed: 11/24/15 Source: AYK0618-04
PCB 1016 ug/L5.1 2.0 5.0000 ND 10-183102
PCB 1260 ug/L4.8 2.0 5.0000 ND 19-14195
ug/L 1.0000 17-144Surr: Decachlorobiphenyl 540.539
Matrix Spike Dup (5110524-MSD1)Prepared & Analyzed: 11/24/15 Source: AYK0618-04
PCB 1016 ug/L5.1 2.0 5.0000 ND 1810-183102 0.8
PCB 1260 ug/L5.0 2.0 5.0000 ND 2719-14199 4
ug/L 1.0000 17-144Surr: Decachlorobiphenyl 550.546
Page 82 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Chlorinated Herbicides by EPA 8151 - Quality Control
Batch 5110487 - EPA 8151A
Blank (5110487-BLK1)Prepared: 11/23/15 Analyzed: 11/24/15
2,4-D ug/LND2.0
2,4,5-T ug/LND2.0
2,4,5-TP (Silvex)ug/LND2.0
Dinoseb ug/LND1.0
ug/L 10.000 10-155Surr: DCAA 848.395
LCS (5110487-BS1)Prepared: 11/23/15 Analyzed: 11/24/15
2,4-D ug/L14.71 2.0 10.000 QL-0329-145147
2,4,5-T ug/L9.33 2.0 10.000 31-15093
2,4,5-TP (Silvex)ug/L8.64 2.0 10.000 35-13886
Dinoseb ug/L6.71 1.0 10.000 10-18267
ug/L 10.000 10-155Surr: DCAA 12612.65
Matrix Spike (5110487-MS1)Prepared: 11/23/15 Analyzed: 11/24/15 Source: AYK0618-04
2,4-D ug/L12.07 2.0 10.000 ND 10-156121
2,4,5-T ug/L7.41 2.0 10.000 ND 10-15874
2,4,5-TP (Silvex)ug/L7.35 2.0 10.000 ND 10-15673
Dinoseb ug/L7.39 1.0 10.000 ND 10-17474
ug/L 10.000 10-155Surr: DCAA 12712.66
Matrix Spike Dup (5110487-MSD1)Prepared: 11/23/15 Analyzed: 11/24/15 Source: AYK0618-04
2,4-D ug/L11.85 2.0 10.000 ND 4910-156118 2
2,4,5-T ug/L7.12 2.0 10.000 ND 4810-15871 4
2,4,5-TP (Silvex)ug/L7.15 2.0 10.000 ND 4610-15672 3
Page 83 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Qual Analyte
Chlorinated Herbicides by EPA 8151 - Quality Control
Batch 5110487 - EPA 8151A
Matrix Spike Dup (5110487-MSD1)Prepared: 11/23/15 Analyzed: 11/24/15 Source: AYK0618-04
Dinoseb ug/L7.17 1.0 10.000 ND 5610-17472 3
ug/L 10.000 10-155Surr: DCAA 12512.48
Page 84 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Laboratory Certifications
Code Description Number Expires
02069Louisiana 06/30/2016LA
381North Carolina 12/31/2015NC
E87315FL DOH (Non-Pot. Water, Solids) Eff:: 07/01/2015 06/30/2016NELAC
E87315FL DOH NELAC (Drinking Water) Eff: 07/01/2015 06/30/2016NELDW
98011001South Carolina 06/30/2016SC
T104704397-08-TXTexas 03/31/2016TX
1340Virginia 12/14/2015VA
Page 85 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
Legend
Defination of Laboratory Terms
- Not Detected at levels greater than or equal to SWSL/RLND
SWSL/RL
MDL
- NC DENR Solid Waste Section LImit/Reporting Limit (Adjusted for DF/Prep Factor)
- Method Detection Limit
Qualifiers
- Dilution FactorDF
S-09 Surrogate recovery was outside control limits biased high. Associated target analytes were not detected at levels at or above the Method Detection Limit and
the data was not affected.
QR-03 The RPD value for the sample duplicate or MS/MSD was outside of QC acceptance limits due to suspected matrix interference and/or non-homogeneous
sample matrix.
QM-05 The spike recovery was outside acceptance limits for the MS and/or MSD and/or PDS due to suspected matrix interference. Sample results for the QC batch
were accepted based on acceptable LCS recoveries.
QL-03 Lab Control recoveries were outside of control limits biased high. Target analyte was not detected at levels at or above reporting limit and data was not
affected.
J Estimated value less than Reporting Limit (RL) but greater than Method Detection Limit(MDL) (CLP J-Flag).
Note: Unless otherwise noted, all results are reported on an as received basis.
Page 86 of 87
ASI Environmental Monitoring & Laboratory Analysis110 Technology Parkway, Norcross, GA 30092
[phone] FAX [phone]
ANALYTICAL SERVICES, INC.
BFI Waste Systems of North America, LLC
5105 Morehead Rd.
Concord NC, 28027
Attention: Mr. Mike Gurley December 08, 2015
COC Goes Here
Page 87 of 87
LOG-IN CHECKLIST
BFI Waste Systems of North America, LLC
Lake Norman C&D LandfillProject:
Client:
Printed: 12/8/2015 1:09:30PM
Environmental Monitoring & Laboratory Analysis
[phone] FAX [phone]
110 Technology Parkway, Norcross, GA 30092
ANALYTICAL SERVICES, INC.ASI
Date Received:11/19/15 15:09 Logged In By:Mohammad M. Rahman
Work Order:AYK0618
OBSERVATIONS
Attn: Mr. Mike Gurley
#Samples: 13 #Containers: 60
4.0 4.0
YES
Minimum Temp(C):Maximum Temp(C):
CHECKLIST ITEMS
COC included with Samples
Sample Container(s) Intact
Chain of Custody Complete
Sample Container(s) Match COC
Custody seal Intact
Temperature in Compliance
Sufficient Sample Volume for Analysis
Zero Headspace Maintained for VOA Analyses
Samples labeled preserved (If Applicable)
Samples received within Allowable Hold Times
Samples Received on Ice
Preservation Confirmed
YES
YES
YES
NO
YES
YES
YES
YES
YES
YES
YES
Custody Seal(s) Used:No
Comments:
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