MO-9558_40989_CA_IAR_20200326_Initital Abatement Report

Initial Abatement Action Report Appendix A
Report Formats
Initial Abatement Action Report
In addition to reporting initial response and abatement actions and assessment actions and presenting initial site
characterization, this newly -created Initial Abatement Action Report must fulfill the requirements, when a release
has been discovered, for the following individual reports:
a Site Check Report (Section C)
❑ UST Closure Report (UST-12) with UST-2 Form (Section D)
❑ Post -Excavation Soil Contamination Assessment Report (Section H)
❑ Product Recovery Report (Section E)
Check the applicable report(s). Complete Sections A-L, as required, including the sections specifically designated
for the reports you have indicated. The Initial Abatement Action Report must be submitted to the appropriate
regional office within 90 days following discovery of release.
A. Site Information
1. Site Identification
"-'Date of Report: March 26 2020
`''Facility I.D.: Not Applicable UST Incident Number (if known): 40989
,°'Site Name: Schulte Residence
"='Site Street Address: 4043 Arborway
City/Town: Charlotte Zip Code: 28211 County: Mecklenburg
Description of Geographical Data Point (e.g., diesel fill port): Former UST location
`' Location Method (GPS; topographical map, other): GPS
''Latitude (decimal degrees): 35.1565549 Longitude (decimal degrees):-80.809683
2. Information about Contacts Associated with the Leaking UST System (Addresses must include street, city,
state, zip code and mailing address, if different).
�` UST Owner: Unknown
Address: Tel.:
'-'UST Operator: Unknown
Address: Tel:
Property Owner: Michael Schulte
Address: 4043 Arborway, Charlotte, North Carolina 28211 Tel.: [phone]
'Property Occupant: Michael Schulte
Address: 4043 Arborway, Charlotte, North Carolina 28211 Tel.: [phone]
-Consultant/Contractor: Harmon Environmental PA
Address: 615 Bruce Thomas Road Monroe NC 28112 Tel: [phone]
'Analytical Laboratory: Pace Analytical Services, LLC State Certification No.: 12
Address: 9800 Kincev Avenue, Suite 100, Huntersville,_NC 28078 Tel: [phone]
3. Information about Release
'�aDate Discovered: February 9, 2020
Estimated Quantity of Release: Unknown
'Cause of Release: stormwater flooded an undiscovered historic heating oil UST and transported
petroleum off -site
Source of Release (Dispenser/Piping/UST): UST-1
=-'Sizes and contents of UST system(s) from which the release occurred): 550-gallon heating oil tank
4. Certification (The title page must display the seal and signature of the certifying P.E. or L.C. and the
name and certification number of the company or corporation, if applicable [See 1 SA NCAC 2L
.0103(e)I)---
I, Richard L. Harmon, a Professional En ip /Licensed Geologist (crr cle one) for (firm or company of employment), do
certify that the information containe,ffls curate to the best of my knowledge.
(Please Affix Seal and Signature)° ►o r t
certification number of the coilyip or
Initial Abatement Report
Schulte Residential Property
4043 Arborway
Charlotte, North Carolina 28211
(circle one or both) in North Carolina. The
Harmon Environmental, PA
615 Bruce Thomas Road
Monroe, North Carolina 28112
harmonenvironmental, com

Initial Abatement Action Report Appendix A
B. Site History and Characterization Report Formats
1. Provide UST owner and operator information.
List the names, addresses, telephone numbers, and dates of ownership/operation of all previous UST
owners and operators of the UST system(s). Present in table form (Use Reporting Table B-2, Site
History, UST Owner/Operator Information, from the Guidelines, Appendix B.).
See attached Table B-2.
2. Provide UST information (inclusive of all USTs, currently and historically in place at facility). For each
UST, provide the following information in table form (Use Reporting Table B-1, Site History, UST/AST
System Information, from the Guidelines, Appendix B.):
Tank identification number (keyed to a site map showing the locations of all UST systems);
Last contents of tank;
Previous contents of tank (if any);
Capacity of tank in gallons;
Construction (material and structure);
Tank dimensions;
Installation date;
Description of piping and pump(s) associated with each UST;
Status of UST (in use or not in use, closed in place, closed by removal; date of last use, date of
closure); and
G Indication that a release was or was not associated with the tank or associated piping or pump(s).
Provide discussion to supplement Table 13-1 and the UST location map in order to clarify the spatial and
historical relationships among tanks and between tanks and piping and dispensers. Provide information
about any historical compliance issues.
See attached Table B-1. Following discovery of the release. DeBruhl Environmental Excavating
Inc. was retained by Mr. Schulte to remove the previously _undiscovered 550 gallon. non-
commercial heating oil tank from the residential pro,erty. This tank was located under a
retaining wall and patio area in the back vard between a masonry kas grill and the residential
structure. Due to site constraints, no soil excavation was feasible. Following removal ofthe tank,
DeBruhl Environmental Excavating. Inc. back killed the former tank basin with soil imported from
off -site. Following removal of the tank Harmon Environmental. PA and DeBruhl Environmental
Excavating, Inc. retained to remediate petroleum -impacted soil in the swale on 4033 Arborway
and 4040 Abington Road, apparently resulting from the overflow of the former UST. The tank was
removed on February 10, 2020 and the swale remediation activities were conducted on March I
and March 13, 2020. Incident Number 40989 has been assigned to this project.
3. Provide non -UST information:
r= List, describe, and indicate location of ASTs and associated piping and pump(s) currently and
historically in place at facility) and describe historical releases. For each AST, present the information
in table form (Use Reporting Table B-1, Site History, UST/AST System Information, from the
Guidelines, Appendix B.); and
List, describe, and indicate location and date of spills which have occurred at facility.
See attached Table B-1. This table summarizes the Incidences at this site prior to February 9,
2020 With the exception of UST-J, no releases have been documented at this site.
4. Provide a comprehensive description of the release, including date discovered, cause and source (including
tank identification number and contents), and the relationship of historical UST releases, non -UST releases,
and off -site releases (indicate incident number) to contamination from current release.
Incident Number 40989 has been assjg_ned to the release associated with UST-1. With the
exception ofthis UST no other releases have been documented at this site.
Initial Abatement Report 2 Harmon Environmental, PA
Schulte Residential Property 615 Bruce Thomas Road
4043 Arborway Monroe, North Carolina 28112
Charlotte, North Carolina 28211 harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
5 Provide a brief description of site characteristics (including status of facility (active or inactive), land use of
site and surrounding area, water supply, topography, vegetation, surface water, wells, buildings, surface
cover, soil type, depth to and nature of bedrock, depth to groundwater, direction of groundwater flow, etc.)
The site is located in an established rural portion of Charlotte North Carolina The topography
of this site slopes toward the east draining toward McMullen Creek. The vegetation on site
consists primarily o(grass and ornamental shrubbery. Based on the Soil Survey of Mecklenburg
County published by the United States Department of Agriculture, Natural Resources
Conservation Service (USDA NRCS} in 2019, the soil type associated with this region of
Mecklenburg County as the Cecil -Urban land complex (CuB). The depth to bedrock, the depth to
groundwater and the groundwater flow direction at the site have not been determined.
6. Summarize initial abatement actions, assessment activities; and corrective actions performed to date and list
all reports previously submitted.
DeBruhl Environmental Excavating. Inc. under the oversight of Harmon Environmental: PA
personnel excavated approximately 2.76-tons of petroleum -impacted soil from the swale on 4033
Arborway and 4040 Abington Road. This excavated soil was transported to the Environmental
Soil, Inc. permitted land application site in Lattimore, North Carolina for appropriate disposal.
Harmon Environmental. PA understands a 24-Hour Report was submitted to the Mooresville
Regional Office ofthe North Carolina Department of Environmental Quality(DEO) by others.
C. Site Check Report (if applicable)
Incorporate the minimum requirements of a Site Check Report, as outlined in the Guidelines, Appendix A, p.
43, if a site check revealed a release and initiated the initial response and abatement action.
I. Present and summarize the results of tank and line tightness testing (Refer to Section L, Appendix A,
Tightness testing results and supporting documentation). If theses tightness testing results did not indicate
a release, and if, instead, environmental contamination was the basis for suspecting a release, describe the
environmental contamination.
2.. Describe the site check procedure. (For guidance refer to the Guidelines, Section 4.3, Site Check
Requirements). Reference site and sample location maps provided in Section J, Figures, and summaries of
soil and groundwater analytical results provided in Section K, Tables. Explain how the selection of sample
types and locations was influenced by the nature of the stored substance, the type of initial alarm or cause
for suspicion, the type ofbackfill, the depth to groundwater, and other factors appropriate for identifying
the presence and source of a release. Describe the condition of the UST system (i.e., pitting, holes, etc.)
where it can be observed.
3. If a release is determined, document initial response actions (submittal of 24-Hour Release and Report
Form; repair, replacement, or upgrading of system to prevent further release; mitigation of hazards) and
initial abatement actions (free product removal; submittal of 20-Day Report) performed in Section G, Initial
Response and Abatement Actions;
4. Document any soil excavation activities in Section H, Excavation of Contaminated Soil.
5. Document site investigation.
' Describe field screening, including:
Physical characteristics of the soil samples, as observed during collection;
M Field instrumentation used to screen soils;
Field instrument calibration procedures; and
e _3 Screening results (Refer to table provided in Section K.).
Document soil sampling information (Refer to figures, tables, and appendices provided in Sections J,
K, and L.), including:
Lithological descriptions from logs for borings, excavations;
ter, Type of samples (from excavation, borehole, geoprobe boring, stockpiled soil, etc.);
k_ Sample collection procedures (grab, split spoon, hand auger, etc.);
Location of soil samples;
Depth of soil samples ( feet below land surface);
Time/date collected;
Sample identification; and
Method(s) of soil sample analysis.
Initial Abatement Report 3 Harmon Environmental, PA
Schulte Residential Property 615 Bruce Thomas Road
4043 Arborway Monroe, North Carolina 28112
Charlotte, North Carolina 28211 harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
Document groundwater and surface water sampling information (Refer to figures, tables, and
appendices provided in Sections J, K, and L.), including:
Location of water samples (e.g., of monitoring well, water supply well, stream sampling point);
Field measurements (e.g., pH, dissolved oxygen, specific conductivity, temperature)
,_� Sample collection procedures (grab, bailer, etc.);
_ Time/date collected.
Sample identification; and
m Method(s) of water sample analysis.
Document quality -control measures information (Refer to tables and appendices provided in Sections
K and L.), including:
Sample handling procedures including sample preservation techniques and sample transport
procedures;
u='' Decontamination procedures;
Time and date samples were submitted to lab; and
L-. Collection of samples for quality control purposes (e.g., duplicates, field blanks, trip blanks).
Describe soil and groundwater investigation results, including:
Presentation of analytical results for soil and groundwater samples (Refer to table(s) provided in
Section K. and to appendix with laboratory analytical results provided in Section L.) and discussion of
the results in relation to the cleanup levels or action levels, as appropriate; and
rx Discussion pertaining to the effect of quality control sample results on the interpretation of soil,
groundwater, or surface water analytical results.
6. Present conclusions and recommendations, referencing maps and cross -sections in Section J, as follows:
ra, Describe source and estimated extent of soil contamination (If there are multiple sources of release,
then describe the extent of contamination from each source);
r_<r Indicate if groundwater or bedrock was encountered during investigation and at what depth below land
surface;
Indicate if groundwater assessment was necessary due to the proximity of the UST system to
groundwater or bedrock (or to the presence of a slab or tank for which removal was determined to be
economically or technologically unfeasible), thereby preventing the reliable determination of a release
by soil assessment alone;
Describe source(s) and estimated extent of any groundwater or surface water contamination;
ua Describe source(s) and estimated thickness and extent of any free product;
Indicate what initial response and abatement actions are required; and
cm Discuss the need for further investigation or remediation.
This section is not applicable. UST -I was a non-commercial, non -regulated heating oil tank.
D. UST Closure Report following UST-12 Format) and Site Investigation Report for Permanent Closure or
Change -in -Service of UST (UST-2 Form) (if applicable).
Incorporate the minimum requirements of a UST Closure Report, as outlined in Appendix A, p.55, and
complete the UST-2 Form, found in Appendix A, p. 60 of the Guidelines), if UST closure indicated a release
and initiated the initial response and abatement action.
I. Describe preparations for closure including steps taken to notify authorities, permits obtained, and steps
taken to clean and purge the tanks.
2. Describe the closure procedure (For guidance, refer to the Guidelines, Section 5.), referencing site and
sampling location maps and cross -sections presented in Section J of this report. Clearly state how the
selection of sample types and locations was influenced by the nature of the stored substance, the type of
initial alarm or cause for suspicion, the type of backfill, the depth to groundwater, and other factors
appropriate for identifying the presence and source of a release. If presence of groundwater or bedrock
require the installation and sampling of monitoring well(s), describe the process.
3. Note the amount of residual material pumped from the tank and describe the storage, sampling and disposal
of the residual material and the disposal of the tank, pumps and piping (Refer to appendices with disposal
manifests and certificate of tank disposal in Section L.).
4. If a release is determined, document initial response actions (submittal of 24-Hour Release and Report
Form; repair, replacement, or upgrading of system to prevent further release; mitigation of hazards) and
Initial Abatement Report 4 Harmon Environmental, PA
Schulte Residential Property 615 Bruce Thomas Road
4043 Arborway Monroe, North Carolina 28112
Charlotte; North Carolina 28211 harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
initial abatement actions (free product removal; submittal of 20-Day Report) performed in Section G, Initial
Response and Abatement Actions.
5. Document any soil excavation activities in Section H, Excavation of Contaminated Soil.
6. Document site investigation.
Describe field screening, including:
Physical characteristics of the soil samples, as observed during collection;
G Field instrumentation used to screen soils;
Field instrument calibration procedures; and
c, Screening results (Refer to table provided in Section J.).
' Document soil sampling information (Refer to figures, tables, and appendices provided in Sections 1,
K and L.), including:
Lithological descriptions from logs for borings, excavations;
4 Type of samples (from excavation, borehole, geoprobe boring, stockpiled soil, etc.);
Sample collection procedures (grab, split spoon, hand auger, etc.);
Location of soil samples;
Depth of soil samples (feet below land surface);
Time/date collected;
Sample identification; and
r1 Method(s) of soil sample analysis.
Document groundwater and surface water sampling information (Refer to figures, tables, and
appendices provided in Sections J, K, and L.), including:
Location of water samples (e.g., of monitoring well, water supply well, stream sampling point);
Field measurements (e.g., pH, dissolved oxygen, specific conductivity, ,temperature)
Sample collection procedures (grab, bailer, etc.);
Time/date collected.
Sample identification; and
Method(s) of water sample analysis.
a Document quality -control measures information (Refer to tables and appendices provided in Sections
K and L, including:
r Sample handling procedures including sample preservation techniques and sample transport
procedures;
Decontamination procedures;
z Time and date samples were submitted to lab; and
j Collection of samples for quality control purposes (e.g., duplicates, field blanks, trip blanks).
Describe soil and groundwater investigation results, including:
Presentation of analytical results for soil and groundwater samples (Refer to table(s) provided in
Section K and to appendix with laboratory analytical results provided in Section L.) and discussion of
the results in relation to the cleanup levels or action levels, as appropriate; and
Discussion pertaining to the effect of quality control sample results on the interpretation of soil,
groundwater, or surface water analytical results.
7. Present conclusions and recommendations, referencing maps and cross -sections in Section J as follows:
PER Describe source and estimated extent of soil contamination, referencing maps and cross -sections in
Section J (If there are multiple sources of release, then describe the extent of contamination from each
source.);
r Indicate if groundwater or bedrock was encountered during investigation and at what depth below land
surface;
Indicate if groundwater assessment was necessary due to the proximity of the UST system to
groundwater or bedrock (or to the presence of a slab or tank for which removal was determined to be
economically or technologically unfeasible), thereby preventing the reliable determination of a release
by soil assessment alone;
Describe source(s) and estimated extent of any groundwater or surface water contamination;
Describe source(s) and estimated thickness and extent of any free product;
Indicate what initial response and abatement actions are required; and
Discuss the need for further investigation or remediation.
This section is not applicable. UST-1 was a non-commercial, non -regulated heating oil tank
Initial Abatement Report 5 Harmon Environmental, PA
Schulte Residential Property 615 Bruce Thomas Road
4043 Arborway Monroe, North Carolina 28112
Charlotte, North Carolina 28211 harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
E. Free Product Investigation and Recovery Report (if applicable)
Discuss the status of free product at the site, as follows:
1. If free product is, or has been, present at the site, describe its current and historical status (product distribution,
thickness, recovery activities). Refer to tables in Section K: Table B-7, Monitoring, and Remediation Well
Construction Information; and Table 13-8A, Free Product Recovery Information; Table 13-813, Cumulative Volume
of Free Product Recovered from Site; and Table B-9, Current and Historical Groundwater Elevations and Free
Product Thickness. Also refer to map(s) showing extent of free product in Section J;
2. Identify any on -site or off -site effluent discharges, treatment used, effluent quality, permitting actions taken, and
location of such discharges and identify the disposition of recovered free product ( refer to attached product
disposal manifests);
3. Document the performance; total cost, and cost per gallon to date of each method of free product recovery used at
site. Justify why the technology is or was used; and
4. Provide conclusions and recommendations concerning historical, current, and future recovery activities,
including:
r' Any proposal to change the current method of free product recovery to a better or more cost-effective
technology;
A justification for continued product recovery, if planned; and
Any determination that free product has been eliminated from the site with a recommendation to reclassify
the risk posed by the release, if applicable.
This section is not applicable. No free product was observed during, the initial abatement process
F. Groundwater and Surface Water Investigation (if applicable)
1. If groundwater or bedrock was encountered in pits, trenches or shallow boring during site check, UST
system closure, or initial abatement investigation, if monitoring or water supply wells were found to be
contaminated, or if surface water is present nearby, then indicate actions taken to investigate suspected
contamination from a release (e.g., installation of monitoring wells, groundwater or surface sampling and
analysis).
2. Document groundwater investigation (or, if applicable, refer to groundwater investigations under Section
C, Site Check Report, or Section D, UST Closure Report), as follows:
' Present groundwater and surface water sampling information (Refer to tables and appendices provided
in Sections K and L.), including:
r-s Location of water samples (e.g., of monitoring well, water supply well, stream sampling point);
a= Field measurements (e.g., pH, dissolved oxygen, specific conductivity, temperature)
Sample collection procedures (grab, bailer, etc.);
a Time/date collected.
Sample identification; and
a Method(s) of water sample analysis.
Document quality -control measure information (Refer to tables and appendices provided in Sections K
and L), including:
Sample handling procedures including sample preservation techniques and sample transport
procedures;
Decontamination procedures;
_- Time and date samples were submitted to lab; and
Collection of samples for quality control purposes (e.g., duplicates, field blanks, trip blanks).
Describe groundwater or surface water investigation results, including:
>> Presentation of analytical results (Refer to table(s) provided in Section K and to appendix with
laboratory analytical results provided in Section L.) and discussion of the results in relation to the
cleanup levels (groundwater quality or surface water quality standards); and
Discussion of the effect of quality control sample results on the interpretation of groundwater or
surface water analytical results.
This section is not applicable. Groundwater was not encountered during the initial abatement
process.
G. Initial Response and Abatement Action
Initial Abatement Report 6 Harmon Environmental, PA
Schulte Residential Property 615 Bruce Thomas Road
4043 Arborway Monroe, North Carolina 28112
Charlotte, North Carolina 28211 harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
Describe initial response actions performed within 24 hours of discovery of the release, including:
r Submittal of 24-Hour Release Report and UST Leak Reporting Form (UST-6I);
r:w Action to prevent further release and to determine source of the release;
Identification and mitigation of hazards due to exposure to pollutants (e.g. Responsible party must
identify and sample water supply wells at risk of impact by the release and provide supply of alternate
water, if wells are impacted.); and
Identification and mitigation of hazards due to fire, explosion, and vapor hazards.
DeBruhl Environmental Excavating Inc. under the oversight of Harmon Environmental PA
personnel, excavated approximately 2.76 tons of petroleum -impacted soil from the swale located
on 4033 Arborwav and 4040 Abington Road This excavated soil was transported to the
Environmental Soil Inc permitted land application site for appropriate disposal A 24 Hour
Report was reportedly submitted to the Mooresville Regional Office of the DEO by others prior to
initiation of this project. Pollution hazards associated with former UST-1 was mitigated by
removjne the tank from 4043 Arborway.
2. Describe initial abatement actions performed, including:
a Completion of investigation to confirm presence and determine source of the release;
k_ Investigation and recovery of free product;
e, Continued mitigation and monitoring of fire, explosion, and vapor hazards;
c Remediation of hazards posed by exposed contaminated soil;
Submittal of 20-Day Report summarizing the progress of the initial actions performed within the 20-
day period following discovery of the release; and
Soil excavation activities (Document in Section H, Excavation of Contaminated soil.),
DeBruhl Environmental Excavating. Inc. under the oversight of Harmon Environmental PA
personnel excavated approximately 2.76-tons of petroleum -impacted soil from the swale located
on 4033 Arborway and 4040 Abington Road This soil was transported to the Environmental S'
Inc. permitted land application site in Lattimore, North Carolina for appropriate disposal.
H. Excavation of Contaminated Soil
1. Describe source and estimated extent of soil contamination determined in initial investigations (e.g., site
check, UST system closure), referencing maps and cross -sections in Section J and tables presenting soil
sampling information and results in Section K (If there are multiple sources of release, then describe the
extent of contamination from each source.), including:
.• Sampling location and depths; locations of tanks, piping dispensers, sumps, areas of staining (indicate
if above or below tank); utility lines; potential receptors; buildings; relationship of area(s) of
contaminated soil to groundwater and bedrock; and
If part or all of UST system was removed, indicate dimensions of resulting pits and trenches.
This section is not applicable. UST-1 was a non-commercial, non -regulated heating oil tanks.
Describe excavation process, referencing maps and cross -sections in Section J, tables presenting soil
sampling information and results in section K and disposal manifests and geological logs in Section J; as
follows:
Describe type of equipment used (e.g,, backhoe, track hoe, dump truck);
Describe field screening, if used to determine limits of excavation, including:
Physical characteristics of the soil samples, as observed during collection;
s Field instrumentation used to screen soils;
Field instrument calibration procedures;
Screening results (Refer to table provided in Section K.);
Indicate the final dimensions of the excavation(s);
Indicate the volume (in cubic yards) and weight (in tons) of soil excavated from each excavation (show
calculations);
r Describe relationship of final excavation pit to former UST system; to groundwater, to bedrock, and to
structures; and
Initial Abatement Report 7 Harmon Environmental, PA
.Schulte Residential Property 615 Bruce Thomas Road
4043 Arborway Monroe, North Carolina 28112
Charlotte, North Carolina 28211 harmonenvironmental com

Initial Abatement Action Report Appendix A
Report Formats
;- Indicate if the excavation operation ceased on encountering clean soil, groundwater, or bedrock OR if
excavation ceased 5 feet from tank(s), dispenser(s), and/or piping and at a depth of 17 feet below land
surface.
The petroleum -impacted soil was excavated by hand and using a CaterpillarO 426B backhoe
operated by DeBruhl of DeBruhl Environmental Excavating Inc personnel and loaded into a
dump truck for transport to the Environmental Soils Inc. -permitted land application site in
Lattimore North Carolina for appropriate disposal As excavated soil samples were screened in
the field with a Multi-RaeO photoioni>iLig organic vapor detector calibrated to an isobutylene
standard. The excavation was terminated when field screening results indicated the petroleum -
impacted soil had been removed The total volume of petroleum -impacted soil removed from the
swale on 4033 Arborway and 4040 Abington Road in conjunction with this Initial Abatement
project was approximately 2.76 tons: Based on the Soil Survey of Mecklenburg Count published
_b_y the USDA NRCS in 2019, the soil type associated with this re ig on of Cecil -Urban land complex
(CuB). The depth to bedrock the nth to groundwater and the groundwater flow direction at the
site have not been determined.
3. Describe post -excavation confirmation soil sampling, referencing maps and cross -sections in Section J,
tables presenting soil sampling information and results in Section K, and geological logs in Section L as
follows:
Describe sample location and depth, and methods of collection and analysis for each excavation;
Note if multiple excavations were performed sequentially in an area of contaminated soil, i.e., if
confirmatory sampling following primary excavation indicated that contaminated soil remained, so that
further excavation was performed and a second set of confirmatory samples was collected and
analyzed; and
-7 If contaminated soil was allowed to remain after final excavation, indicate precisely the location and
depth of the residual contamination and explain why it was not removed, i.e., why it was not
economically and/or technologically feasible to excavate it
4. Document Soil Investigation.
Provide soil sampling information for all samples collected following excavation and during previous
investigations. Refer to table provided in Section K: Table B-3, Summary of Soil Sampling Results; to
figures, in Section J; and to appendices, in Section L. Information should include
Lithological descriptions from logs for borings, excavations;
Type of samples (from excavation, borehole, geoprobe boring, stockpiled soil, etc.);
�. Sample collection procedures (grab, split spoon, hand auger, etc.);
Location of soil samples;
:Frya Depth of soil samples ( feet below land surface);
Time/date collected;
Sample identification;
:a Indication of phase of sampling: , site check; closure, IAA, etc.; and
Method(s) of soil sample analysis.
5=1 Document quality -control measures information (Refer to tables and appendices provided in Sections
K and L.), including:
Sample handling procedures including sample preservation techniques and sample transport
procedures;
r Decontamination procedures;
Time and date samples were submitted to lab; and
Collection of samples for quality control purposes (e.g., duplicates, field blanks, trip blanks).
tiW Describe soil investigation results, including:
a Presentation of analytical results for soil samples (Refer to table provided in Section K and to appendix
with laboratory analytical results provided in Section L.);
Discussion of the results in relation to the appropriate cleanup levels, identifying the samples that
exceed the lower of:
(a) the residential MSCCs or
(b) the soil -to -groundwater MSCCs.
Discussion of effect of quality control sample results on the interpretation of soil analytical results.
Initial Abatement Report 8 Harmon Environmental, PA
Schulte Residential Property 615 Bruce Thomas Road
4043 Arborway Monroe, North Carolina 28112
Charlotte, North Carolina 28211 harmonenvironmental.com

Initial Abatement Action Report Appendix A
_ _ _ Report Formats
I.
site constraints. no excavation in the vicinity of the former UST was feasible On March 11 and
March 13, 2020, DeBruhl Environmental Excavating Inc personnel excavated proximately
2.76 tons ofpetroleum-impacted soil from the Swale on 4033 Arborway and 4040 Abington Road
As remediation activities were conducted Harmon Environmental PA personnel collected soil
samples SB-108'-24 "). SB-2(6"-I ') SB-3(0-6"), SB-4(1 ') and SB-SL') from the base of the
swale following removal of the impacted soil These soil samples were collected rom de the
ranging from the ground surface to 24-inches below grade Each of -these samples was place in
glassware provided by the laboratory and shipped on ice to Pace Analytical Services,..LLC in
Huntersville North Carolina......Upon receipt these five samples were analyzed for volatile organic
compounds by SW-846 Method 8260B semi -volatile organic compounds by SW-846 Method
8270E and volatile petroleum hydrocarbon compounds and extractable petroleum hydrocarbon
compounds by Massachusetts Methods. Further, one soil sample (SB-6(S')) was collected in the
vicinity ofthe former UST basin for diesel range total petroleum hydrocarbon compounds analysis
indicate the presence of targeted constituents at concentrations exceeding the Residential
Maximum Soil Contaminant Concentration Standards (version 1-2016-11-03)
5, Describe disposal of contaminated soil, referencing tables presenting soil sampling information and results
in Section K and disposal manifests in Section L as follows:
Indicate volume and weight of contaminated soil removed from each excavation at site;
Describe construction of any stockpile of contaminated soil, describe collection and analysis of
stockpile samples;
:a Indicate if soil was treated onsite (Reference permit in Section L.);
3 Indicate if soil was transported offsite for disposal and, if so, by whom and to what destination; and
sV Confirm that excavation was back -filled with clean soil.
On March 17 and March 13, 2020, DeBruhl Environmental Excavating Inc. excavated
approximately 2.76 tons of petroleum impacted soil from the swale on 4033 Arborway and 4040
Abington Road. As excavated, the soil was transported by wheelbarrow to 4040 Abington Road
and loaded into a dump truck. As the remediation was conducted, Harmon Environmental. PA
personnel collected confirmatory soil samples SB-1(18"-24"), SB-26"-1' . SB-3(0-6") SB-4(I)
and SB-5(1) from the base of the Swale. These samples were delivered by courier Pace Anal tical
Services, LLC in Huntersville, North Carolina for volatile organic compounds by SW-846 Method
8260B, semi -volatile organic compounds by SW--.846 Method 8270E and volatile petroleum
hydrocarbon compounds and extractable petroleum hydrocarbon compounds by Massachusetts
Methods. On March 13, 2020, approximately 2.76 tons of petroleum -impacted soil was removed
From the vicinity of the surface release. The excavated soil was loaded into a dump truck and
transported to the Environmental Soils. Inc. permitted land application site in Lattimore, North
Carolina for appropriate disposal, A copy of the manifest is presented in Appendix H. Following
collection of these samples, portions of the Swale were backlled to grade with topsoil imported
from off site.
6. Present conclusions, as follows;
Briefly summarize excavation process;
:«n Describe extent of final excavation(s) and collection of confirmatory samples;
Indicate if excavation ceased on encountering groundwater or bedrock; and
Indicate whether soil contaminant levels in exceedance of the lowest MSCCs remain in the
excavation(s), further excavation being determined infeasible by the UST Section, or soil contaminant
levels in final excavation confirmatory soil samples were equal to below the lowest MSCCs
Conclusions
1. If soil contaminant levels in exceedance of the lowest MSCCs remain in the excavation(s) (further
excavation being determined infeasible by the UST Section), if groundwater or bedrock has been
encountered in proximity to contamination, or if free product is present, it should be concluded that a
Limited Site Assessment must be performed and a report submitted within 120 days of discovery of the
release, but
Initial Abatement Report 9 Harmon Environmental, PA
Schulte Residential Property 615 Bruce Thomas Road
4043 Arborway Monroe, North Carolina 28112
Charlotte, North Carolina 28211 harmonenvironmental. com

Initial Abatement Action Report Appendix A
Report Formats
2. If soil contaminant levels in final excavation confirmatory soil samples were equal to or below the lowest
MSCCs and if groundwater, bedrock, and free product were not encountered in the excavation(s), then no
further action should be requested.
On February 10, 2020, DeBruhl Environmental Excavating, Inc. removed a formerly
undiscovered, historic, non-commercial 550-gallon heating oil UST from 4043 Arborway. Due to
site constraints, no excavation in the vicinity of the former UST was feasible. On March II and
March 13, 2020, DeBruhl Environmental Excavating Inc. personnel excavated approximately
2.76 tons of petroleum -impacted soil from the swale on 4033 Arborwav and 4040 Abington Road.
As remediation activities were conducted. Harmon Environmental, PA personnel collected soil
samples SB-1(18'-24"), SB-2(6"-1'), SB-3(0-6"), SB-4(1) and SB-5(1') from the base of the
swale following removal of the impacted soil. These soil samples were collected from depths
ranging from the ground surface to 24-inches below grade. Each of these samples was place in
glassware provided by the laboratory and shipped on ice to Pace Analytical Services, LLC in
Huntersville, North Carolina. Upon receipt these rye samples were analyzed for volatile organic
compounds by SW-846 Method 8260B, semi -volatile organic compounds by SW-846 Method
8270E and volatile petroleum hydrocarbon compounds and extractable petroleum hydrocarbon
compounds by Massachusetts Methods. Further, one soil sample jSB-6(5'2) was collected in the
vicinity of the former UST basin for diesel range total petroleum hydrocarbon compounds analysis
by SW--846 Method 8015. A copy of the laboratory report is presented in Appendix J and a copy
of the Chain -of -Custody Record is presented in Appendix L The results of these analyses did not
indicate the presence of targeted constituents at concentrations exceeding; the Residential
Maximum Soil Contaminant Concentration Standards (version 1-2016-11-03). Based on site
constraints no further remediation is feasible in the vicinity of the former UST. As a result,
Harmon Environmental PA recommends this incident be closed with a Notice of Residual
Petroleum linked to the former UST basin at 4040 Arborway_
J. Figures
Provide the following:
1. A topographic map illustrating the area within 1500-foot radius of the source of the release, showing:
Topographic contours;
Site location;
u Buildings;
Adjacent streets; roads, highways (identified by street names and numbers);
Surface water bodies,
r� Groundwater flow direction (if determined); and
�7 North arrow and scale.
See Figyre 1.
2. A site map* and cross -sections illustrating the UST systems)/excavation area(s), drawn to scale, showing:
Buildings and property boundaries;
Underground utilities, such as sewer lines and other conduits; basements; and vaults;
Water supply wells, surface water bodies
Location and orientation of current and former UST(s), pumps; product lines, sumps, etc.;
Length, diameter and volume of current and former UST(s);
Type of material(s) stored in UST(s) (currently and formerly); and
Names or descriptions of properties adjacent to the site; and
North arrow and scale.
Fire 2 presents a scaled drawing_of the residence and property boundaries. Soil sample locations,
sample designations sample depths are depicted on Figure 3 No groundwater sampling activities
were conducted in conjunction with this project As a result this fr re does not present groundwater
monitoring locations or oundwater flow direction - --
3. Map(s)* and geological cross -sections, drawn to scale, depicting all soil analytical results obtained to date
and final confirmatory sample results, to include:
Initial Abatement Report 10 Harmon Environmental, PA
Schulte Residential Property 615 Bruce Thomas Road
4043 Arborway Monroe, North Carolina 28112
Charlotte, North Carolina 28211 harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
r Description of soil and bedrock lithology (as determined by investigation to date);
Location and orientation of UST(s), pumps, piping, sumps, etc.(current and former);
Soil sample identification (unique letter and/or numerical code), location, and depth;
=' Soil sample analytical results;
r s Final limits of each stage of excavation for each excavation on site**; and
4 Two geological cross -sections, drawn across the contaminated area and intersecting at right angles,
showing the vertical distribution of the contaminants in the unsaturated zone. (Indicate vertical and
horizontal scale, orientation of each section, location of water table, soil types and lithology, all
borings and sample locations represented by the sections, and soil analytical results for each
represented sample, and show sections as labeled lines on the map.)
Figure 3 presents ascaled drawing of the area immediately surrounding the surface water ditch.
This figure presents the locations, sample designations, depths and analytical results associated
with the soil samples collected during this excavation project. A north arrow and an approximate
scale are presented on this figure. No geologic cross -sections or excavation log have been
prepared in coniunction with this project. A description of the soil types encountered during this
excavation is discussed in response to Question B.S. ofthis form.
4. Map(s)* and geological cross -sections, drawn to scale, depicting the groundwater and surface water
analytical results,** to include;
i::o Location and orientation of UST(s), pumps, piping, sumps, etc.(current and former);
eE,-:3 Groundwater sample identification (unique letter and/or numerical code referencing monitoring or
water supply well)and location;
Surface water sample identification (unique letter and/or numerical code) and location; and
c Groundwater and surface water sample analytical results.
No groundwater or surface water samples were collected in conjunction with this initial
abatement proiect
5. A free product map* showing thickness (in feet) and extent of free product** using contour lines; and
No free -product was observed during this initial abatement project.
6. A potential receptor map that clearly identifies water supply wells (municipal or public/private wells, etc.) and
other potential receptors (surface water bodies, basements, utilities, etc.) which are at risk.
*Note: If possible, use a single base map to prepare site plans using a map scale of 1 inch = 40 feet (or a
smaller scale for large sites, if necessary). Maps and figures should include conventional symbols, notations,
labeling, legends, scales, and north arrows and should conform to generally accepted practices of map
presentation such as those enumerated in the USGS Geological Survey pamphlet, "Topographic Maps."
** If applicable
A receptor survey was not conducted in conjunction with this initial abatement proiect.
K. Tables
Provide the following:
1. Site History (Complete Tables B-1 and B-2 from Guidelines, Appendix B);
Tables B-I and B-2 are attached
2. Public and Private Water Supply Well and Other Receptor Information (Complete Table B-5 from
Guidelines, Appendix B);
A receptor survey was not conducted in conjunction with this initial abatement project....
Initial Abatement Report 11 Harmon Environmental, PA
Schulte Residential Property 615 Bruce Thomas Road
4043 Arborway Monroe, North Carolina 28112
Charlotte, North Carolina 28211 harmonenvironmental.com

Initial Abatement Action Report Appendix A
Report Formats
3. Field Screening Results;
This table was not used in this project.
4. Summary of Soil Sampling Results (Complete Table B-3 from Guidelines, Appendix 13);
See Table B-3 attached.
5. Summary of Groundwater and Surface Water Sampling Results* (Complete Table B-4 from Guidelines,
Appendix B)*;
This table is not applicable to this project.
6. Monitoring and Remediation Well Construction Information (Complete Table B-7 from Guidelines, Appendix
B)*;
This table is not applicable to this proiect.
7. Free Product Recovery Information (Complete Table 13-8A from Guidelines, Appendix B)*;
This table is not applicable to this project.
8. Cumulative Volume of Free Product Recovered from Site (Complete Table 13-813 from Guidelines, Appendix
B)*;
This table is not applicable to this project.
9. Current and Historical Groundwater Elevations and Free Product Thickness (Complete Table B-9 from
Guidelines, Appendix B)*.
* If applicable
This table is not applicable to this project.
L. Appendices
Provide the following:*
Appendix A
Tightness testing results and supporting documentation*
Appendix B
Notification of Intent: UST Permanent Closure or Change -in -Service (UST-3 Farm)
Appendix C
Site Investigation Report for Permanent Closure or Change -in -Service of UST (UST-2
Form)*
Appendix D
Site Specific Health and Safety Plan (HASP)
Appendix E
Certificate of UST disposal*
Appendix F
Groundwater field measurements (pH, dissolved oxygen, specific conductivity, temperature)*
Appendix G
Standard procedures (sampling, field equipment decontamination, field screening, etc.)
Appendix H
Soil, water, free product, and sludge disposal manifests and soil treatment permits*
Appendix I
Complete chain -of -custody records
Appendix J
Copy of all laboratory analytical records
Appendix K
Photographs of site check, closure, and excavation activities (optional)
Appendix L
Geologic logs for excavation(s)Iborings (related to IAA investigation only)
Appendix M
Monitoring Well Construction Forms (for all wells constructed to date)
* lfapplicable
Initial Abatement Report 12 Harmon Environmental, PA
Schulte Residential Property 615 Bruce Thomas Road
4043 Arborway Monroe, North Carolina 28112
Charlotte, North Carolina 28211 harmonenvironmental. com

Figures

Q .�s4r� is •.i • ♦ . , � �' � ., ' ^� _ '.
v rc
.-., ` r -� _ i� • Pam`
Jr
APPROXIMATE SCALE IN FEET
0 2000 4000
SOURCE: TOPO! 2003 NATIONAL GEOGRAPHIC
HARMON ENVIRONMENTAL, PA FIGURE 1
615 BRUCE THOMAS ROAD SITE LOCATION MAP
MONROE, NORTH CAROLINA SCHULTE RESIDENCE
704-292-4527 4043 ARBORWAY
HARMONENVIRONMENTAL,COM CHARLOTTE, NORTH CAROLINA

i
N
�o
i
�c POOL
mn & DECK
%S CATCH BASIN
m '' moo'
.041 Iwo
o
.00
GQO
LEGEND
APPROXIMATE LOCATION OF
PROPERTY BOUNDARIES
APPROXIMATE LOCATION OF
RESIDENCES
APPROXIMATE LOCATION OF
PAVED AND GRAVEL SURFACES
0 0 ❑ APPROXIMATE LOCATION OF
FENCE
APPROXIMATE LOCATION OF
�- -' FORMER UNDERGROUND
STORAGE TANK
APPROXIMATE SCALE IN FEET
APPROXIMATE LOCATION OF SWALE 0 100 200
SOURCE: MECKLENBURG COUNTY POLARIS AND FIELD MEASUREMENTS
HARMON ENVIRONMENTAL, PA FIGURE 2
615 BRUCE THOMAS ROAD SITE LAYOUT MAP
MONROE, NORTH CAROLINA 28112 SCHULTE RESIDENCE
704-292-4527 4043 ARBORWAY
HARMONENVIRONMENTAL. COM CHARLOTTE, NORTH CAROLINA

SB-1 (18%24")
P-ISOPROPYLTOLUENE 0.0106 MG/KG
NAPHTHALENE 0.0181 MG/KG
1,2,4-TRIMETHYLBENZENE 0.0087 MG/KG
1,3.5-TRIMETHYLBENZENE 0.0083 MG/KG
C9-C12 ALIPHATICS 84.9 MG/KG
C9-C22 AROMATICS 59.2 MG/KG
SB-6(5FT) P'
DRO <&l MG/KG
LEGEND
SB-2 (6"-1')
ACETONE 0.226 MG/KG
BENZO(G,H,I)PERYLENE 1.130 MG/KG
INDENO(1,2,3-CD)PYRENE 0.594 MG/KG
SB-3(6") ,,
ACETONE 0.166 MG/KG ■
)
1,2,4-TRIMETHYLBENZEENZENE 0.0143 MG/KG
POOL _
& DECK
AT BASIN
�Vel
/
Q- /
i Opo
O
APPROXIMATE LOCATION OF
®
SOIL SAMPLE
(1')
APPROXIMATE DEPTH OF SOIL
SAMPLE
MG/KG
MILLIGRAMS PER KILOGRAM
APPROXIMATE LOCATION OF
PROPERTY BOUNDARIES
APPROXIMATE LOCATION OF
RESIDENCES
APPROXIMATE LOCATION OF
PAVED AND GRAVEL SURFACES
-- _;
APPROXIMATE LOCATION OF
`"-
FORMER UNDERGROUND
STORAGETANK
APPROXIMATE LOCATION OF
SWALE
ACETONE s6 5(1)
0.124 MG/KG
NOTES:
SOIL SAMPLES SB-1 (18"-24"). SB-2(6"-l'), SB-3(0-6"), SB-4(1') AND SB-5(1')
PRESENTED IN THIS FIGURE WERE COLLECTED BY HARMON
ENVIRONMENTAL, PA PERSONNEL ON MARCH 11 AND MARCH 13, 2020
FROM THE APPROXIMATE LOCATIONS AND DEPTHS INDICATED. THESE
SAMPLES WERE ANALYZED BY PACE ANALYTICAL SERVICES, LLC FOR
VOLATILE ORGANIC COMPOUNDS BY SW-846 METHOD 8260B,
SEMI -VOLATILE ORGANIC COMPOUNDS BY SW-846 METHOD 8270E
AND VOLATILE AND PETROLEUM HYDROCARBON COMPOUNDS BY
MASSACHUSETTS METHODS. SOIL SAMPLE SB-6(5') WAS COLLECTED BY
HARMON ENVIRONMENTAL, PA PERSONNEL AND ANALYZED BY PACE
ANALYTICAL SERVICES, LLC FOR DIESEL RANGE PETROLEUM
HYDROCARBON COMPOUNDS BY SW-846 METHOD 8015C.
APPROXIMATE SCALE IN FEET
0 100 200
SOURCE: MECKLENBURG COUNTY POLARIS AND FIELD MEASUREMENTS
HARMON ENVIRONMENTAL, PA FIGURE 3
615 BRUCE THOMAS ROAD SITE LAYOUT MAP WITH ANALYTICAL RESULTS
MONROE, NORTH CAROLINA 28112 SCHULTE RESIDENCE
704-292-4527 4043 ARBORWAY
HARMON ENVIRONMENTAL.COM CHARLOTTE, NORTH CAROLINA

Tables

Appendix B
Reporting Tables
Table B-1: Site History — UST/AST System Information
Revision Date: 3/26/20 Incident Number and Name: 40989/Schulte Residence
Description
Was release
UST ID
Current/Last
Previous
Capacity (in
Construction
Tank
of Associated
Date Tank
Status of
associated
Number
Contents *
Contents *
gallons)
Details **
Dimensions
Piping and
Installed
UST ***
with the UST
Pumps
S stem?
UST-1
Heating Oil
Heating
550
Single
46 inches
Copper
Unknown
Removed
Yes
Oil
Wall Steel
by
Feed and
2/10/20
74 inches
Return
Add additional records as necessary
Description
Was release
AST ID
Current/Last
Previous
Capacity (in
Construction
Tank
of Associated
Date Tank
Status of
associated
Number
Contents *
Contents *
gallons)
Details **
Dimensions
Piping and
Installed
AST ***
with the AST
Pumps
S stem?
Add additional records as necessary
* Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non -halogenated or halogenated solvents, etc.
* * Fiberglass (single- or double -walled), steel (single- or double -walled), steel with FRP (single- or double -walled), steel with liner, other, unknown.
*** Currently operational, not in use or temporarily closed (specify date), penmanently closed in place (specify date), permanently closed by removal (specify
date)

Table B-2: Site History - UST Owner and Operator Information
Revision Date: 3/26/20 Incident Number and Name: 40988/Schulte Residence
UST ID Number
Facility ID Number-
UST-1
N/A
Name of Owner
Dates of Ownership'
mm/ddl to mm/dd/
Unknown
Street Address
city
State
Zip
Tele hone Number
Name of Operator
Dates'of Operation
mm/dd! to mm/d'd/
Unknown
Street Address
11 City
State
Zip,
Tele hone Number
UST ID Number
Facility ID Number
Name of Owner
Dates of Operation
mm/dd/ to mm/dd/
Street Address
city
State
Zip-
Telephone Number
Name' of Operator `
Dates of Operation
mm/dd/ to mrn/dd/
Street i Address
city
I'State
I zip
Telephone-,Nu-mber
Add additional records as necessary

Table B-3: Summary of Soil Sampling Results
Revision Date: 3/26/20 Incident Number and Name: 40989/Schulte Residence
Analytical Method
8015
8260B
8260B
8260E
8260E
8260E
8260E
8270E
8270E
VPH&EPH
VPH&EPH
Contaminant of Concern
c
c
N
c
c
N
c
c
v
v
c
L
a
'2
a
E
Sample
Date
Source
Sample
Incident
a
a,
E
w
w
=
a
o
ID
Collected
Area
Depth
Phase
o
0c
X
c
=-°
o
m
N
SB-1 18"24"
3/11/2020
UST
1.5-2 ft
Initial Abatement
.
0.0106
0.0181
0=87
0.0083
<10.1
<0.101
<0.448
<0.448
84.9
59.2
SB-2 6"-1'
3/11/2020
UST
0.5-1 ft
Initial Abatement
<0.0085
<0.0085
<0.0085
<0.0085
<0.169
0.226
1.130
0.594
<16.5
<16.5
SB-3 0-6"
3/11/2020
UST
0-0.5 ft
Initial Abatement
<0.0062
<0.0062
<0.0062
<0.0062
<0.125
0.166
<0.518
<0.518
<15.8
<15.8
SB-4 1'
3/13/2020
UST
1 ft
Initial Abatement
<0.0065
<0.0065
0.0143
<0.0065
<0.130
<0130
<0.431
<0.431
<13.0
<13.0
SB-5 1'
3/13/2020
UST
1 ft
Initial Abatement
<0.0045
<0.0045
<0.0045
<0.0045
<9.0
0.124
<0385
<0.385
<11.7
<11.7
SB-6 5'
3/13/2020
UST
5 ft
Initial Abatement
<6.1
Soil to Groundwater MSCC m k
NA
0.12
0.16
8.5
83
4.6
24
6,400
3.4
540
31
Residential MSCC k
NA 1
100
313
1 782
782
3,129
14,000
469
0.88
1,500
469
Industrial/Commerical MSCC (mg/kg) I
NA 1
40,000 1
8,176
1 20,440 1
20,440 1
81,760 1
360,00n..1
12,264
8
- nnn
1 12,264
Notes: MSCC = Maximum Soil Contaminant Concentration (Version 1-2016-11-03)
Sample Depth presented in feet below ground surface
Results presented in milligrams per kilogram (mg/kg)
DRO = Diesel Range Organic Compounds

Appendix A
Tightness Testing results and Supporting Documentation
(This Appendix is not applicable to this project)

Appendix B
Notification of Intent: UST Permanent Closure or
Change -in -Service (UST-3 Form)
(This Appendix is not applicable to this project)

Appendix
Investigation
Change -in -Services
(This Appendix is not al
Permanent

Appendix

Site Specific Health and Safety Plan
for
Site Assessment Activities
at
4043 Arborway, Charlotte, North Carolina
March 10, 2020
Prepared By:
Harmon Environmental, PA
615 Bruce Thomas Road
Monroe, North Carolina 28112
704-292-4527
harmonenvironmental.com
This document is confidential and is to be used by designated project personnel. Reproduction of
this document is strictly prohibited unless approved in writing by Harmon Environmental, PA.

Signatures of Approval
Project Manager ' Date
2
Corporate Health a afety Coordinator Date
X"'-r ZJ 'r,Zs
Site Health and Safety Manager Date

Plan Acceptance
I have been permitted the opportunity to read this Health and Safety Plan for Site Assessment
Activities at 4043 Arborway in Charlotte, North Carolina, and have been briefed by the Site Safety
Manager or an appropriately designated alternate on its content. All questions and comments I have
asked or stated regarding this Plan have been satisfactorily addressed. I understand the contents of
this Plan and agree to abide by its requirements.
Each person entering exclusion zones defined in Section 5.4 of this Plan shall sign below.
Signature / Printed Name Company Date

Table of Contents
Section
Title
Page No.
1.0
General Information
1
2.0
Project Organization
2
3.0
Site Description
2
4.0
Site Safety Control
2
5.0
Hazard Assessment/Personnel Protection
3
6.0
Decontaminating Procedures
4
7.0
Emergency Procedures
4
Figure Site Layout Map
Appendix A Exposure Limits of Chemical Hazardous
Appendix B Route to Hospital

1.0 General Information
1.1 Site Safety Plan Preparation:
Plan Prepared By: R. Harmon
Date Plan. Approved: March 10, 2020
1.2 Site Information:
Site Name: Schulte residence and surrounding properties
Site Location: 4043 Arborway, Charlotte, NC
Site Contact: None
Site Status: Open (X) Closed ( )
Limited Access O Fenced( )
Existing Site Information:
Detailed O Sketch ( )
Preliminary (X) None( )
Facility EPA I.D. No.:N/A
1.3 Hazardous Materials Information:
State/Form of Hazardous Materials:
Gas ( ) Liquid O Soil (X)
Groundwater (X) Sludge O Solid( )
Material Hazards:
Corrosive O Volatile (X) Ignitable ( )
Toxic ( ) Reactive ( ) Explosive ( )
Radioactive O Unknown O Flammable ( )
1.4 Scope of Work:
Excavate petroleum -impacted soil originating from a former heating oil underground
storage tank. The excavated soil will be loaded directly onto trucks for transport to a
licensed disposal facility. Following completion of the excavation, soil samples will
be collected, and the excavation will be backfilled with clean soil imported from off -
site.
Health and Safety Plan 1 Harmon Environmental, PA
4043 Arhorway, 615 Bruce Thomas Road
Charlotte, NC Monroe, NC 28112
March 10, 2020 [phone]

2.0 Project Organization
Project Manager:
Corporate Health and Safety Coordinator:
Site Health and Safety Manager:
Technical Support:
Harmon Environmental Project No. 842-01
3.0 Site Description
Richard Harmon
Richard Harmon
Richard Harmon
DeBruhl Environmental Excavating, Inc.
The site consists of a commercial property with a former heating oil underground storage tank.
4.0 ,Site Safety Controls
4.1 Site Map:
See attached figure
4.2 Perimeter Control:
No perimeter control is in place at the site,
4.3 Command Post Area:
The command post will be established outside of the exclusion zone at the subject
site. A telephone will be available at the command post area.
4.4 Exclusion Zones:
During the excavation activities, the exclusion zone shall be defined as a 15-foot
radius around the open excavation.
4.5 Decontamination Area:
Decontamination of the excavation equipment will be performed on -site.
5.0 Hazard Assessment/Personnel Protection
5.1 General
Primary routes of potential exposure are through inhalation of dust, ingestion, and
skin contact with impacted soil and/or groundwater. Hazards include the physical
hazard associated with excavation, drilling and well advancement activities. Due to
the outdoor location of the project and expected hazards, moderate health risks are
anticipated.
Health andSafety Plan 2 Harmon Environmental, PA
4043 Arhorway> 615 Bruce Thomas Road
Charlotte, NC Monroe, NC 28112
March 10, 2020 [phone]

5.2 Health and Safety Training Requirements
All field personnel (including Subcontractors) must have appropriate hazardous
waste site health and safety training in accordance with OSHA 1910.120 regulations
prior to initiating on -site activities. The Site Safety Manager must have an additional
8 hours of specific site management training.
5.3 Personnel Protection
General Level of Protection:
A ( ) B ( ) C ( ) D modified ( ) D (X)
Level D:
For all personnel participating in the excavation and sampling activities, the
following equipment is required as a minimum:
• Chemical resistant outer gloves
• Steel toe and shank boots
• Standard work clothing (long -sleeve shirt and long pants)
• Hard hat and safety glasses.
• Ear protection (when noise levels preclude normal conversation)
5.4 Upgrading and Downgrading of Personnel Protection:
Upgrading and downgrading of personnel protection levels will be implemented if
deemed necessary by the Site Safety Manager. Any upgrades will be based on
observed site conditions. Under no circumstances will downgrading be permitted by
any field personnel without the consent of the Site Safety Manager.
6.0 Decontamination Procedures
• Boots, boot covers, and gloves will be cleaned with phosphate -free soap and tap
water.
• Disposable coverings and equipment will be cleaned with phosphate -tree soap and
tap water, then disposed of as normal trash.
• Sampling equipment will be cleaned with phosphate -free soap, and tap water,
followed by a distilled water rinse.
Health andSafely Plan 3 Harmon Environmental, PA
4043 Arborway. 615 Bruce Thomas Road
Charlotte, NC Monroe, NC 28112
March 10, 2020 [phone]

7.0 Emergency Procedure
7.1 Field Communications: Hand signals when distressed; working in noisy
environment; or wearing respirators.
Thumbs up OK
Thumbs Down Not OK
Hands on wrist Exit Exclusion Zone
Hands on Throat Cannot Breath
7.2 In the Event of Personnel Exposure:
Skin Contact: Flush with water, remove impacted clothing. Secure Medical
Attention
Inhalation: Move person away from exclusion zone, administer first aid and CPR
as necessary. Secure medical attention.
Ingestion: Secure medical attention.
Eye Contact: Irrigate with water. Secure medical attention.
7.3 Personnel Injury:
In the event a personnel injury occurs, decontaminate individual if injury is not life
threatening. If decontamination is not feasible, wrap the victim in a blanket,
administer first aid or CPR as necessary, contact the local rescue squad, and hospital.
All injuries, exposures, or spills are to be documented by the Site Safety Manager
and reported to the Project Manager within 24 hours. Such documentation is to be
kept on file at Harmon Environmental, PA for future reference.
7.4 Heat Stress:
In the event of heat stress, move the victim out of the heat to a cool area on site.
Place the victim in shock position with their feet elevated. Cool the victim by
spraying with water or using wet towels and fanning. Secure medical attention.
7.5 First Aid Equipment:
Health and .Safety Plan 4 Harmon Environmental, PA
4043 Arhorway. 615 Bruce Thomas Road
Charlotte, NC Monroe, NC 28112
March 10, 2020 [phone]

A first aid kit is located within the support vehicles on -site. Potable water is
available on -site.
7.6 Route to Hospital
See Appendix B
7.7 Emergency Information:
Service Phone
Ambulance
911
Fire Department
911
Police
911
Hospital (Atrium Health Mercy)
[phone]
Charlotte Poison Control
[phone]
North Carolina Department of Environment,
[phone]
Health and Natural Resources
Region IV EPA
[phone]
DeBruhl Environmental Excavating, Inc.
[phone]
Harmon Environmental, PA
[phone]
842-01,11&S
Health and Safety Plan 5 Harmon Environmental, PA
4043 Arborway, 615 Bruce Thomas Road
Charlotte, NC Monroe, NC 28112
March 10, 2020 [phone]

Figures

Pokru's 3C M2p — MecMenhCg County, NoTft CC2j°CfflI%
4r
Date Printed: 3/10/2020 4:39:43 PM
AW
.✓ 111
a � K� ,
_.._� _ i
,.
This map or report is prepared for the inventory of real property within Mecklenburg County and is compiled from recorded deeds, plats, tax maps, surveys, planimetric maps, and other public records and data.
Users of this map or report are hereby notified that the aforementioned public primary information sources should be consulted for verification. Mecklenburg County and its mapping contractors assume no legal
responsibility for the information contained herein.

Appendix A
Exposure Limits of Chemical Hazards

CONOCO -- DIESEL FUEL NO.2 - DIESEL FUEL Page I-of3
CONOCO - DIESEL FUEL NO. 2 - DIESEL FUEL
MATERIAL SAFETY DATA SHEET
NSN: 9140002865296
Manufacturer's CAGE: 15445
Part,No. Indicator: A
Part Number/Trade Name: DIESEL FUEL NO. 2
General Information
Item Name: DIESEL FUEL
Company's Name: CONOCO INC
Company's Street: 600 N DAIRY ASHFORD RD RM 3012
Company's P. 0. Box: 4784
Company's City: HOUSTON
Company's State: TX
Company's Country: US
Company's Zip Code: 77210-4784
Company's Emerg Ph #: 713-293-5550/800-424-9300
Company's Info Ph #: 713-293-5550
Record No. For Safety Entry 029
Tot Safety Entries This Stk#: 093
Status: SMU
Date MSDS Prepared: 14AUG91
Safety Data Review Date: 24JUN92
Supply Item Manager: KY
MSDS Serial Number: BMZTT
Specification Number: W-F-800
Spec Type, Grade, Class: GRADE DF-2
Hazard Characteristic Code: F4
Ingredients/Identity Information
Proprietary: NO
Ingredient: PETROLEUM MID -DISTILLATE (DIESEL MARINE FUEL)
Ingredient Sequence Number: 01
Percent: 100 %
NIOSH (RTECS) Number: 1004302PE
CAS Number: 68476-34-6
OSHA PEL: 5 MG/M3 AS OIL MIST
ACGIH TLV: 5 MG/M3 AS OIL MIST
Other Recommended Limit: NONE SPECIFIED
Physical/Chemical Characteristics
Appearance And Odor: CLEAR OR LIGHT YELLOW LIQUID, AROMATIC ODOR
Boiling Point: 350 - 680F
Melting Point: NOT GIVEN
Vapor Pressure (MM Hg/70 F): 1 MMHG
Vapor Density (Air=1): > 1
Specific Gravity: 0.85 - 0.93
Decomposition Temperature: NOT GIVEN
Evaporation Rate And Ref: NIL
Solubility In Water: INSOLUBLE
Percent Volatiles By Volume: NIL
Corrosion Rate (IPY): UNKNOWN
Fire and Explosion Hazard Data
Flash Point: 130F,54C
Flash Point Method: TCC
http://msds.pdc.comeH.edu/msds/siri/msds/h/ql94/q436.html 10/14/2001

CONOCO -- DIESEL FUEL NO.2 DIESEL FUEL
Page 2 of 3
Lower Explosive Limit: 0.4 %
Upper Explosive Limit: 6 %
Extinguishing Media: WATER SPRAY, FOAM, DRY CHEMICAL CAARBON DIOXIDE
Special Fire Fighting Proc: USE WATER TO KEEP FIRE -EXPOSED CONTAINERS
COOL. IF LEAK OR SPILL HAS NOT IGNITIED, USE WATER SPRAY TO DISPERSE THE
VAPORS AND TO PROVIDE PROTECTION.
Unusual Fire And Expl Hazrds: PRODUCTS OF COMBUSTION MAY CONTAIN CARBON
MONOXIDE, CARBON DIOXIDE AND OTHER TOXIC MATERILS. DO NOT ENTER ENCLOSED OR
CONFINED SPACE WITHOUT PROPER PPE.
Reactivity Data
Stability: YES
Cond To Avoid (Stability): AVOID HEAT AND FLAME
Materials To Avoid: INCOMATI'BLE WITH OXIDIZING MATERIALS.
Health Hazard Data
Precautions for Safe Handling and Use
Control Measures
Transportation Data
Disposal Data
Label Data
Label Required: YES
Technical Review Date: 24JUN92
MFR Label Number: NONE
Label Status: G
Common Name: DIESEL FUEL NO. 2
Chronic Hazard: NO
Signal Word: CAUTION?
Acute Health Hazard -Slight: X
Contact Hazard -Slight: X
Fire Hazard -Slight: X
Reactivity Hazard -None: X
Special Hazard Precautions: STORE IN WELL VENTILATED AREEA. KEEP CONTAINER
TIGHTLY CLOSED. STORE IN ACCORDANCE WITH NATIONAL FIRE PROTECTION ASSN
REGULATIONS. FIRST AID: INHALATION: REMOVE TO FRESH AIR. IF NOT BREATHING,
GIVE ARTIFICIAL RESPIRATION. IF BREATHING IS DIFFICULT, GIVE OXYGEN. CALL A
PHYSICIAN. SKIN: FLUSH SKIN WITH WATER AFTER CONTACT. REMOVE CONTAMINATED
CLOTHING. EYES: IMMEDIATELY FLUSH WITH WATER FOR 15 MINUTES. CALL A
PHYSICIAN. INGESTION: DO NOT INDUCE VOMITING. IMMEDIATELY GIVE TWO GLASSES
OF WATER. NEVER GIVE ANYTHING TO IF UNCONCIOUS. CALL MD
Protect Eye: Y
Protect Skin: Y
Label Name: CONOCO INC
Label Street: 600 N DAIRY ASHFORD RD RM 3012
Label P.O. Box: 4784
Label City: HOUSTON
Label State: TX
Label Zip Code: 77210-4784
http://msds.pdc.comell.edu/msds/siri/msds/h/gl94/g436.html 10/14/2001

CONOCO -- DIESEL FUEL NO.2 - DIESEL FUEL
Page 3 of 3
Label Country: US
Label. Emergency Number: 713-293-5550/800-424-9300
http://msds.pdc.comell.eduhnsds/siri/msds/h/q l94/g436.hbnl 10/14/2001

Appendix B
Route to Hospital

3/10/2020 4043 Arbor Way, Charlotte, NC to Atrium Health Mercy - Google Maps
GO gle Map-, 4043 Arbor Way, Charlotte, NC to Atrium Health Drive 4.6 miles, 14 min
Mercy
n +-n �4'rium Melt. Mnry
♦»,.. ..N .ma M
n "
p
C
Go gle
PnA Ni.M
Map data ©2020 Google 2000 fir,
a
4043 Arbor Way
t 1. Head north on Arbor Way toward Warburton Rd
2 min (0.7 mi)
Take Providence Rd to S Caswell Rd
8 min (3 6 mi)
r 2. Turn right onto Sharon Ln
♦1 3. Use the left 2 lanes to turn left onto Providence Rd
0 Pass by S State Bank (or, the rigl_! m )
2 1 mi
r 4. Turn right to stay on Providence Rd
0 ss by Wells Fargo Bank (on the ngh)
1.0 mi
Continue on S Caswell Rd. Take Vail Ave to N Colonial Ave
3 min (0 4 mi)
r 5. Turn right onto S Caswell Rd
0.2 mi
r 6. Turn right onto Vail Ave
0.1 mi
https://www.google.com/maps/dir/4043+Arbor+Way,+Charlotte,+NC/Atrium+Health+Mercy,+2001 +Vail+Ave,+Charlotte,+NC+28207/@35.1838115,-80.... 1 /2

Appendix E
Certification of UST Disposal

UST Disposal Company
4921 Hoover Drive
Charlotte, NC 28269
704-599-0770
CERTIFICATE OF TANK DISPOSAL
Certificate Number: 20200316
Contractor:
DeBruhl Environmental Excavating, Inc.
4921 Hoover Drive
Charlotte, NC 28269
TYPE OF TANK SIZE
UST 46" x 74"
Date: 3/16/2020
Address:
4043 Arbor Way
Charlotte, NC 28211
GALLONS
550
UST Disposal Company certifies that the above mentioned tank has been properly
disposed of and the contents and sludge processed in full compliance with local, state and
federal regulations.
rkic iveliBr"fif
UST Disposal Company
4921 Hoover Drive
Charlotte, NC 28269

Appendix F
Groundwater Field Measurements
(This Appendix is not applicable to this project)

Appendix G
Standard Procedures

Standard Procedures
Soil Sampling in Conjunction with UST Spill Response
Soil samples collected during this project were collected using by Harmon
Environmental, PA personnel a hand auger following removal of the impacted media
from the ditch by the excavation contractor.
Typically as the remediation activities are conducted, a sample aliquot is collected from
the hand auger bucket at designated locations and placed directly into a zipper seal bag
for field screening with a Multi-Raeg photoionizing organic vapor detector (PID), or
equivalent, calibrated to an isobutylene standard. New latex gloves, or equivalent, are
worn throughout the collection of the screening sample. Each zipper seal bag is labeled
with a sample designation, time, date, approximate depth and sampler's initials at the
time of collected.
Based on the results of the field screening activities, Harmon Environmental, PA field
personnel may opt to collect an additional sample aliquot for laboratory analysis. Prior to
collecting a sample, new latex gloves, or equivalent, are donned, and the laboratory
supplied sample bottles are labeled. Each soil sample is then collected directly from the
excavator bucket and placed directly into the pre -labeled glassware provided by the
laboratory. These samples are then placed in a cooler on ice pending delivery under
chain -of -custody protocol to the analyzing laboratory.
The depth of each sample, the location of each sample, the time of sample collection, the
field screening results and any deviations from these standard protocols are documented
in the field notes prepared in conjunction with each project.

Appendix H
Soil, Water, Free -Product and Sludge Disposal Manifests
And Soil Treatment Permits

DEBRUHL ENVIRONMENTAL EXCAVATING, INC.
4921 HOOVER DRIVE
CHARLOTTE, NC 28269
704-598-2681- OFFICE
704-598-2988 — FAX
NON -HAZARDOUS WASTE MANIFEST
DATE_ �, % t 3 / 7 LOAD NUMBER J
ENVIRONMENTAL CONSULTANT: Harmon Environmental
Contact: Rick Harmon Phone: [phone]
GENERATOR: hti �'h� L k 1+,e-
Address: 3 A ► ,p it1 �s C.i, ^ rL ,t - , ,_�. �_, 972
_ 1 )
Contact: m K.- a,,oc_ Phone: 2 3i; -- 144 - 4e31�- �
TRANSPORTER: DeBruhl Environmental Excavating, Inc.
Contact: Randy DeBruhl Phone: [phone]
DESTINATION: Environmental Soils, Inc., Dedicated Land Application Site
CLASS & TYPE OF CONTAMINATE IN SOIL: Class Il- petroleum
WASTE ORIGINATION POINT:
COUNTY: Mecklenburg SOURCE OF CONTAMINATION: UST
TRUCK#: VOLUME:_4��t''
DRIVER SIGNATURE: ( DATE:
GENERATORS CERTIFICATION OF WASTE CONSTITUENTS:
In lieu of submitting analytical data (methods 8240 and 8270) verifying that the waste in
question does not contain organic constituents other than those which would normally
appear in analysis of virgin petroleum product residue, I am submitting this Certificate of
Waste Constituents. I certify that I am familiar with the source of contamination of the
soil and further certify the source, to the best of my knowledge, contains no contaminants
other than that listed above.
Signature Date : // 3
Company Name Title,
3 -13 •-2 b

ENVIRONMENTAL SOILS, INC. {
P.O. BOX 295
LATTIMORE, N.C. 28089-0489
704/434-0075
Job Name:
Truck#
Gross Wgt.:
Tare Wgt:
Net Wgt:
Tons:
Weighed by

Appendix I
Completed Chain -of -Custody Records

FaceAnalytjcql
CHAIN -OF -CUSTODY I Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section A Section IS Section C
Of
Required Client Information; Required Project Information: Invoice Information;
Attention;'3
Companyl ReportTo:
A
Addr! -1 * Copy
To: I
1,,p,,y NanjS_,,
REGULATORY AGENCY
Add E,
NPDES GROUNDWATER DRINKING WATER
LIST RCRA OTHER
Email To Purchase
inReferencot
Order No.:
Phone;Project
Name:
Pace prefect
1 thirm9cr.
Site Location
STATE:
rg—`--sted Duo Date/TAT: JProject
Number:
Paw. Profile V.
Requested
Analysis
Filtered
(YIN)
Section D Matrix Codes
Required Client Information MATRIX t CODE
COLLECTED
Preservatives
5z
Dr7nkingW2ter OW
v
O
0
1,
z
2
Water WT
Waste WW
Water
Product P
in
compositc
START
compost-ir
ENIXGRAB
ul
Soil/solid SL
0
O
SAMPLE ID ape
0
1--
V,TJWLP
(A-Z, 0-9 Air AR
Simple IDS MUST BE UNIOUE Tissue Ts
Other OT
0
0
to
<
Q.
ul
z
F-
in
Ito
'a
X
to
Lu
0
In
>,
�z
� b
a.
8
u-
2
Ci
C5
0
rot
72
<
DATE
TIME
DATE
TIME
<
0
X
z
=
I z
z
2
Pace Project No./ Lab I.D.
2-
3hi4pl
,,, I
f
k
L,
C,
A
3
—s F�;, V i I- -z- I-1 I,)
in 4 6
4
1
N1
q
14
14
4
fl13
X
7
8
9
11
121
ADDITIONAL COMMENTS
RELINQU)PHED BY I AFFILIATION
DATE
TIME
ACCEPTED BY I AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
2
-a
SAMPLER NAME AND SIGNAT!
U
C
PRINT Name of SAMPLER;
`
SIGNATURE of SAMP L
DATE Signed
co
0
(MWDDIYY):
(J)
Note: 5y sirpung tic form you are acmpling Pace'r. NET 30 day payment lermt,and agreeing to late charges of 1,5% per month for any invoices not paid within 30 days. F-ALL-0-020rev,07,1540ay-2007

Appendix J
Analytical Results
(Excluded from DENR File Copy per February 20, 2014 Memorandum)

aceAnalytical e
www.pacelabs.com
March 26, 2020
Mr, Rick Harmon
Harmon Environmental
615 Bruce Thomas Road
Monroe, NC 28112
RE: Project: 842 UST
Pace Project No.: 92469653
Dear Mr. Harmon:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results forsample(s) received by the laboratory on March 16, 2020. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
1(704)875-9092
HORIZON Database Administrator
Enclosures
pGG$F�♦
4.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of59

9411
,ac,Analyfical'
www.pacelabs.com
Project: 842 UST
Pace Project No.: 92469653
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #:'37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification # 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 59

Pace Analytical Services, LLC
aceAnalytical 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
SAMPLE ANALYTE COUNT
Project: 842 UST
Pace Project No.: 92469653
Lab ID
Sample ID
Method
Analysts
Analytes
Reported
Laboratory
92469653001
SB-2 (6"-1')
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
JAH
6
PASI-C
EPA 8270E
PKS
75
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
SM 254OG
KDW
1
PASI-A
92469653002
SB-3 (0-6")
MADEP EPH
BAJ
7
PASI-C
MADEPVPH
JAH
6
PASI-C
EPA 8270E
PKS
75
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
SM 254OG
KDW
1
PASI-A
92469653003
SB-1 (18"-24")
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
JAH
6
PASI-C
EPA 8270E
PKS
75
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
SM 2540G
KDW
1
PASI-A
92469653004
SB-4 (1')
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
JAH
6
PASI-C
EPA 8270E
PKS
75
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
SM 2540G
KDW
1
PASI-A
92469653005
SB-5 (1')
MADEP EPH
BAJ
7
PASI-C
MADEP VPH
JAH
6
PASI-C
EPA 8270E
PKS
75
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
SM 254OG
KDW
1
PASI-A
92469653006
SB-6 (5')
EPA 8015C Modified
BAJ
2
PASI-C
ASTM D2974-87
KDF
1
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 59

m
aceAnalytical
www.pacelabs.com
Project: 842 UST
Pace Project No.: 92469653
Lab Sample ID
Method
92469653001
EPA 8270E
EPA 8270E
EPA 8260D
ASTM D2974-87
SM 2540G
92469653002
EPA 8260D
ASTM D2974-87
SM 2540G
92469653003
MADEP EPH
MADEP EPH
MADEP VPH
MADEP VPH
MADEP VPH
EPA 8260D
EPA 8260D
EPA 8260D
EPA 8260D
EPA 8260D
ASTM D2974-87
SM 254OG
92469653004
EPA 8260D
ASTM D2974-87
SM 254OG
92469653005
EPA 8260D
ASTM D2974-87
SM 254OG
92469653006
ASTM D2974-87
SUMMARY OF DETECTION
Client Sample ID
Parameters
SB-2 (6"-1')
Benzo(g,h,i)perylene
Indeno(1,2,3-cd)pyrene
Acetone
Percent Moisture
Total Solids
SB-3 (0-6")
Acetone
Percent Moisture
Total Solids
SB-1 (18"-24")
Aliphatic (C09-C18)
Aromatic (Cl 1-C22)
Aliphatic (C09-C12)
Aromatic (C09-C10),Unadjusted
Total VPH
p-Isopropyltoluene
Naphthalene
1,2,4-Trimethyl benzene
1,3, 5-Trimethyl benzene
o-Xylene
Percent Moisture
Total Solids
SB-4 (1)
1,2,4-Trimethylbenzene
Percent Moisture
Total Solids
SB-5 (V)
Acetone
Percent Moisture
Total Solids
SB-6 (5')
Percent Moisture
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersvilie, NC 28078
[phone]
Result Units Report Limit Analyzed
1130
ug/kg
529
03/20/2014:18
594
ug/kg
529
03/20/2014:18
226
ug/kg
169
03/18/2016:51
38.6
%
0.10
03/16/2016:40
60.7
%
03/24/20 23:03
166
ug/kg
125
03/18/2017:16
36.1
%
0.10
03/16/2016:40
65.4
%
03/24/20 23:03
64.0
mg/kg
27.8
03/23/2012:28 N2
42.7
mg/kg
13.9
03/23/2011:02 N2
20.9
mg/kg
8.67
03/25/20 23:25
16.5
mg/kg
8.67
03/25/20 23:25
37.4
mg/kg
8.67
03/25/20 23:25
10.6
ug/kg
5.0
03/18/2017:41
18.1
ug/kg
5.0
03/18/2017:41
8.7
ug/kg
5.0
03/18/2017:41
8.3
ug/kg
5.0
03/18/2017:41
7.9
ug/kg
5.0
03/18/2017:41
26.9
%
0A0
03/16/2016:40
73.8
%
03/24/20 23:03
14.3
ug/kg
6.5
03/19/2014:15
23.1
%
0.10
03/16/2016:40
77.4
%
03/24/20 23:03
124
ug/kg
90.5
03/18/2018.31
13.5
%
0.10
03/16/2016:40
81.2
%
03/24/20 23:03
18.8
%
0.10
03/1612016:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
r)lmlifi.m
Page 4 of 59

aceAnalXical s
www.pacelabs.com
l
PROJECT NARRATIVE
Project: 842 UST
Pace Project No.: 92469653
Method: EPA 8015C Modified
Description: 8015 GCS THC-Diesel
Client: Harmon Environmental
Date: March 26, 2020
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
General Information:
1 sample was analyzed for EPA 8015C Modified. All samples were received in acceptable condition with any exceptions noted below or
on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3546 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below,
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 531340
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92469870001
R1: RPD value was outside control limits.
• MSD (Lab ID: 2836950)
• Diesel Range Organics(C10-C28)
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 59

Pace Analytical Services, LLC
aceAnalXicalq
9800 neyAve, Suite100
078
Huntersvilie, NC 28078
www.pacelabs.com
[phone]
PROJECT NARRATIVE
Project: 842 UST
Pace Project No.: 92469653
Method: MADEP EPH
Description: MADEP EPH NC Soil
Client: Harmon Environmental
Date: March 26, 2020
General Information:
5 samples were analyzed for MADEP EPH. All samples were received in acceptable condition with any exceptions noted below or on
the chain -of custody and/or the sample condition upon receipt form (SOUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with MADEP EPH with any exceptions noted below,
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 531181
S5: Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
• SB-1 (18"-24") (Lab ID: 92469653003)
• 2-Bromonaphthalene (S)
SB-4 (1') (Lab ID: 92469653004)
• 2-Bromonaphthalene (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike;
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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PROJECT NARRATIVE
Project: 842 UST
Pace Project No.: 92469653
Method: MADEP VPH
Description: MADEPV
Client: Harmon Environmental
Date: March 26, 2020
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
5 samples were analyzed for MADEP VPH. All samples were received in acceptable condition with any exceptions noted below or on
the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Pagel of 59

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PROJECT NARRATIVE
Project: 842 UST
Pace Project No.: 92469653
Method: EPA 8270E
Description: 8270E MSSV Microwave
Client: Harmon Environmental
Date: March 26, 2020
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
5 samples were analyzed for EPA 8270E. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 3546 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
QC Batch: 531416
SO: Surrogate recovery outside laboratory control limits.
• MSD (Lab ID: 2837287)
• Terphenyl-d14 (S)
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: 531416
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92469360001
R1: RPD value was outside control limits.
MSD (Lab ID: 2837287)
• Pyridine
Additional Comments:
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
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PROJECT NARRATIVE
Project: 842 UST
Pace Project No.: 92469653
Method: EPA 8260D
Description: 8260D/5035A Volatile Organics
Client: Harmon Environmental
Date: March 26, 2020
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
5 samples were analyzed for EPA 8260D. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 5035A with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
QC Batch: 531178
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• BLANK (Lab ID: 2836092)
• Bromomethane
• Chloroethane
• Dichlorodifluoromethane
LCS (Lab ID: 2836093)
• Bromomethane
• Chloroethane
• Dichlorodifluoromethane
• LCSD (Lab ID: 2836094)
• Bromomethane
• Chloroethane
• Dichlorodifluoromethane
• SB-1 (18"-24") (Lab ID: 92469653003)
Bromomethane
• Chloroethane
• Dichlorodifluoromethane
• SB-2 (6"-1') (Lab ID:92469653001)
Bromomethane
Chloroethane
• Dichlorodifluoromethane
• SB-3 (0-6") (Lab ID: 92469653002)
• Bromomethane
• Chloroethane
• Dichlorodifluoromethane
• SB-5 (1') (Lab ID: 92469653005)
• Bromomethane
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC, Page 9 of 59

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c
PROJECT NARRATIVE
Project: 842 UST
Pace Project No.: 92469653
Method: EPA 8260D
Description: 8260D/5035AVolatile Organics
Client: Harmon Environmental
Date: March 26, 2020
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 531178
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• Chloroethane
• Dichlorodifluoromethane
QC Batch: 531399
v1: The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated
samples may have a high bias.
• BLANK (Lab ID: 2837162)
• Bromomethane
• LCS (Lab ID: 2837163)
• Bromomethane
MS (Lab ID: 2837957)
Bromomethane
• MSD (Lab ID: 2837958)
• Bromomethane
• SB-4 (1") (Lab ID: 92469653004)
• Bromomethane
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
QC Batch: 531178
L1: Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated samples
may be biased high.
• LCS (Lab ID: 2836093)
• Bromomethane
• LCSD (Lab ID: 2836094)
• Bromomethane
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 59

Pace Analytical Services, LLC
® 9800 Kincey Ave. Suite 100
aceAnalXical Huntersvilie, NC 28078
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[phone]
PROJECT NARRATIVE
Project: 842 UST
Pace Project No.: 92469653
Method: EPA 8260D
Description: 8260D15035A Volatile Organics
Client: Harmon Environmental
Date: March 26, 2020
QC Batch: 531399
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92470071002
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MSD (Lab ID: 2837958)
• 1,2,4-Trimethylbenzene
Additional Comments
Analyte Comments:
QC Batch: 531399
E: Analyte concentration exceeded the calibration range.. The reported result is estimated.
• MS (Lab ID: 2837957)
• Toluene
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 11 of 59

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PROJECT NARRATIVE
Project: 842 UST
Pace Project No.: 92469653
Method: SM 2540G
Description: Total Solids 2540 G-2011
Client: Harmon Environmental
Date: March 26, 2020
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
General Information:
5 samples were analyzed for SM 2540G. All samples were received in acceptable condition with any exceptions noted below or on the
chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments.
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 59

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i
ANALYTICAL RESULTS
Project: 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-2 (6"-l') Lab ID: 92469653001 Collected 03/11/20 10:21 Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)
ND
mg/kg
16.5
1
03/19/20 17:33
03/23/20 10:07
N2
Aliphatic(C19-C36)
ND
mg/kg
16.5
1
03/1912017:33
03/23/20 10:07
N2
Aromatic (Cl 1-C22)
ND
mg/kg
16.5
1
03/19/20 17:33
03/23/20 10:07
N2
Surrogates
Nonatriacontane (S)
54
%
40-140
1
03/19/20 17:33
03/23/20 10:07
7194-86-7
o-Terphenyl (S)
83
%
40-140
1
03/19/20 17:33
03/23120 10:07
84-15-1
2-Fluorobiphenyl (S)
117
%
40-140
1
03/19/20 17:33
03/23/20 10:07
321-60-8
2-Bromonaphthalene (S)
117
%
40-140
1
03/19/20 17:33
03/23/20 10:07
580-13-2
MADEPV Analytical Method: MADEP VPH Preparation Method: MADEPV
Aliphatic (C05-CO8)
ND
mg/kg
8,24
1
03/11/20 10:21
03/25/20 22:19
Aliphatic (C09-C12)
ND
mg/kg
8.24
1
03/11/20 10:21
03/25/20 22:19
Aromatic (C09-C10),Unadjusted
ND
mg/kg
8.24
1
03/11/20 10:21
03/25/20 22:19
Total VPH
ND
mg/kg
8.24
1
03/11/20 10:21
03/25/20 22:19
Surrogates
2,5-Dibromotoluene (FID)
84.6
%
70-130
1
03/11/20 10:21
03/25/20 22:19
2,5-Dibromotoluene (PID)
81.2
%
70-130
1
03/11/20 10:21
03/25/20 22:19
8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA3546
Acenaphthene
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
83-32-9
Acenaphthylene
ND
ug/kg
529
1
03/19/20 12:55
03/2012014:18
208-96-8
Aniline
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
62-53-3
Anthracene
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
120-12-7
Benzo(a)anthracene
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
56-55-3
Benzo(a)pyrene
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
529
1
03/19/20 12:55
03/20/201418
205-99-2
Benzo(g,h,i)perylene
1130
ug/kg
529
1
03/1912012:55
03/20/20 14:18
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
207-08-9
Benzoic Acid
ND
ug/kg
2640
1
03/19/20 12:55
03/20/20 14:18
65-85-0
Benzyl alcohol
ND
ug/kg
1060
1
03/19/20 12:55
03/20/20 14:18
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
101-55-3
Butylbenzylphthalate
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
85-68-7
4-Chloro-3-methylphenol
ND
ug/kg
1060
1
03/1912012:55
03/20/20 14:18
59-50-7
4-Chioroaniline
ND
ug/kg
1060
1
03/19/20 12:55
03/20/20 14:18
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
111-44-4
2-Chloronaphthalene
ND
ug/kg
529
1
03/19/20 12:55
03/20/2014:18
91-58-7
2-Chlorophenol
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
7005-72-3
Chrysene
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
529
1
03119/2012:55
03/20/20 14:18
53-70-3
Dibenzofuran
ND
ug/kg
529
1
03/19/20 12:55
03120/2014:18
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
529
1
03119/2012:55
03/20/20 14:18
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
1060
1
03119/2012:55
03/2012014:18
91-94-1
REPORT
OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 03/26/2020 01:45 PM
without the written consent
of Pace Analytical Services, L.L.C.
Page 13 of 59

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ANALYTICAL RESULTS
Project: 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-2 (6"-1') Lab ID: 92469653001 Collected: 03/11/20 10:21 Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546
2,4-Dichlorophenol
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
120-83-2
Diethylphthalate
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
84-66-2
2,4-Dimethylphenol
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
105-67-9
Dimethylphthalate
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
131-11-3
Di-n-butylphthalate
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/kg
1060
1
03/19/20 12:55
03/20/20 14:18
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2640
1
03/19/20 12:55
03/20/20 14:18
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
606-20-2
Di-n-octylphthalate
ND
ug/kg
529
1
03/19/20 12:55
03/2012014:18
117-84-0
bis(2-Ethylhexyl)phthalate
ND
ug/kg
529
1
03119/2012:55
03/20/20 14:18
117-81-7
Fluoranthene
ND
uglkg
529
1
03/19/20 12:55
03/20/20 14:18
206-44-0
Fluorene
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
529
1
03/19/20 12:55
03/2012014:18
87-68-3
Hexachlorobenzene
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
77-47-4
Hexachloroethane
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
67-72-1
Indeno(1,2,3-cd)pyrene
594
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
193-39-5
Isophorone
ND
uglkg
529
1
03/19/20 12:55
03/20/20 14:18
78-59-1
1-Methylnaphthalene
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
90-12-0
2-Methylnaphthalene
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
91-57-6
2-Methytphenol(o-Cresol)
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
95-48-7
3&4-Methylphenol(m&p Cresol)
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
15831-10-4
Naphthalene
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
91-20-3
2-Nitroaniline
ND
ug/kg
2640
1
03/19/20 12:55
03/20/20 14:18
88-74-4
3-Nitroaniline
ND
ug/kg
2640
1
03/19/20 12:55
03/20/20 14:18
99-09-2
4-Nitroaniline
ND
ug/kg
1060
1
03/19/20 12:55
03/20/20 14:18
100-01-6
Nitrobenzene
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
98-95-3
2-Nitrophenol
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
88-75-5
4-Nitrophenol
ND
ug/kg
2640
1
03/19/20 12:55
03/20/20 14:18
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
529
1
03/1912012:55
03/20/20 14:18
86-30-6
2,2'-0xybis(1-chloropropane)
ND
ug/kg
529
1
03/19/20 12:55
03120/2014:18
108-60-1
Pentachlorophenol
ND
ug/kg
1060
1
03/19/20 12:55
03/20/20 14:18
87-86-5
Phenanthrene
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
85-01-8
Phenol
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
108-95-2
Pyrene
ND
uglkg
529
1
03119/2012:55
03/20/20 14:18
129-00-0
Pyridine
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
529
1
03/19/20 12:55
03/20/20 14:18
88-06-2
Surrogates
Nitrobenzene-d5 (S)
62
%
23-110
1
03/19/20 12:55
03/20/20 14:18
4165-60-0
2-Fluorobiphenyl (S)
47
%
30-110
1
03/19/20 12:55
03/20/20 14:18
321-60-8
Terphenyl-d14 (S)
52
%
28-110
1
03/19/20 12:55
03/20/20 14:18
1718-51-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, I.I.C.
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aceAnalXical
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Project: 842 UST
Pace Project No.: 92469653
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 KinceyAve: Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-2 (6"-1')
Lab ID: 92469653001
Collected: 03/11/20 10:21
Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Surrogates
Phenol-d6 (S)
24
%
22-110
1
03/19/20 12:55
03/20/20 14:18
13127-88-3
2-Fluorophenol (S)
16
%
13-110
1
03/19/20 12:55
03/20/20 14:18
367-12-4
2,4,6-Tribromophenol (S)
46
%
27-110
1
03/19/20 12:55
03/20/20 14:18
118-79-6
8260D/5035A Volatile Organics
Analytical Method: EPA 8260D Preparation Method:
EPA 5035A
Acetone
226
ug/kg
169
1
03/18/20 13:32
03/18/20 16:51
67-64-1
Benzene
ND
ug/kg
8.5
1
03/18/20 13:32
03/18/20 16:51
71-43-2
Bromobenzene
ND
ug/kg
8.5
1
03/18/20 13:32
03/18/20 16:51
108-86-1
Bromochloromethane
ND
ug/kg
8.5
1
03/18/20 13:32
03/18/20 16:51
74-97-5
Bromodichloromethane
ND
ug/kg
8.5
1
03/18/20 13:32
03/18/20 16:51
75-27-4
Bromoform
ND
ug/kg
8.5
1
03/18/20 13:32
03/18/20 16:51
75-25-2
Bromomethane
ND
ug/kg
16:9
1
03/18/20 13:32
03/18/20 16:51
74-83-9 IH,v1
2-Butanone (MEK)
ND
ug/kg
169
1
03/18/20 13:32
03/18/20 16:51
78-93-3
n-Butylbenzene
ND
ug/kg
8.5
1
03/18/20 13:32
03/18/20 16:51
104-51-8
sec-Butylbenzene
ND
ug/kg
8.5
1
03/18/20 13:32
03/18/20 16:51
135-98-8
tert-Butylbenzene
ND
ug/kg
8.5
1
03/18/20 13:32
03/18/20 16:51
98-06-6
Carbon tetrachloride
ND
ug/kg
8.5
1
03/18/20 13:32
03/18/20 16:51
56-23-5
Chiorobenzene
ND
ug/kg
8.5
1
03/18/20 13:32
03/18/20 16:51
108-90-7
Chloroethane
ND
ug/kg
16.9
1
03/18/20 13:32
03/18/2016:51
75-00-3 v1
Chloroform
ND
ug/kg
8.5
1
03/18/20 13:32
03/18/20 16:51
67-66-3
Chloromethane
ND
ug/kg
16.9
1
03/18/20 13:32
03/18/20 16:51
74-87-3
2-Chlorotoluene
ND
ug/kg
8:5
1
03/18/20 13:32
03/18/20 16:51
95-49-8
4-Chlorotoluene
ND
ug/kg
8:5
1
03/18/20 13:32
03/18/20 16:51
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
8,5
1
03/18/20 13:32
03/18/20 16:51
96-12-8
Dibromochloromethane
ND
ug/kg
8.5
1
03/1812013:32
03/18/20 16:51
124-48-1
1,2-Dibromoethane (EDB)
ND
uglkg
8.5
1
03/18/20 13:32
03/18/20 16:51
106-93-4
Dibromomethane
ND
ug/kg
8.5
1
03/18/20 13:32
03/18/20 16:51
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
8.5
1
03/18/20 13:32
03/18/20 16:51
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
8.5
1
03/18/20 13:32
03118/2016:51
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
8.5
1
03/18/20 13:32
03/18/20 16:51
106-46-7
Dichlorodifluoromethane
ND
ug/kg
16.9
1
03/18/20 13:32
03/1812016:51
75-71-8 v1
1,1-Dichloroethane
ND
ug/kg
8.5
1
03/18/20 13:32
03118/2016:51
75-34-3
1,2-Dichloroethane
ND
ug/kg
8.5
1
03/18/20 13:32
03/18/20 16:51
107-06-2
1,1-Dichloroethene
ND
uglkg
8.5
1
03/18/20 13:32
03/18/20 16:51
75-35-4
cis-1;2-Dichloroethene
ND
ug/kg
8.5
1
03/18/20 13:32
03/18/20 16:51
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
8.5
1
03/18/20 13:32
03/1812016:51
156-60-5
1,2-Dichloropropane
ND
ug/kg
8.5
1
03/18/20 13:32
03/18/20 16:51
78-87-5
1,3-Dichloropropane
ND
ug/kg
8.5
1
03/18/20 13:32
03/18/20 16:51
142-28-9
2,2-Dichloropropane
ND
uglkg
8.5
1
03/18/20 13:32
03118/2016:51
594-20-7
1,1-Dichloropropene
ND
ug/kg
8.5
1
03/18/20 13:32
03/1812016:51
563-58-6
cis- 1,3-Dichloropropene.
ND
uglkg
8.5
1
03/18/20 13:32
03/18/20 16:51
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
8.5
1
03/18/20 13:32
03/18/20 16:51
10061-02-6
Diisopropyl ether
ND
ug/kg
8.5
1
03/18/20 13:32
03/18/20 16:51
108-20-3
Ethylbenzene
ND
uglkg
8.5
1
03/18/20 13:32
03/18/2016:51
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
8.5
1
03/18/20 13:32
03118/2016:51
87-68-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC, Page 15 of 59

aceAnalytical
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t
{
ANALYTICAL RESULTS
Project: 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 KinceyAve, Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-2 (6"-fl Lab ID: 92469653001 Collected: 03/11/20 10:21 Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No, Qual
8260D15035A Volatile Organics
2-Hexanone
Isopropylbenzene (Cumene)
p-lsopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1 Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uoromethane
1,2,3-Trichioropropane
1,2,4-Trimethylbenzene
1 3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichioroethane-d4 (S)
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
84.7
1
03/18/2013:32
03/18/2016:51
591-78-6
ND
ug/kg
8.5
1
03/18/2013:32
03/18/2016:51
98-82-8
ND
ug/kg
8.5
1
03/18/2013:32
03/18/2016:51
99-87-6
ND
ug/kg
33.9
1
03/18/2013:32
03/18/2016:51
75-09-2
ND
ug/kg
84.7
1
03118/2013:32
03/18/2016:51
108-10-1
ND
ug/kg
8.5
1
03/18/2013:32
03/18/2016:51
1634-04-4
ND
ug/kg
8.5
1
03/18/2013:32
03/18/2016:51
91-20-3
ND
ug/kg
8.5
1
03/18/2013:32
03/18/2016:51
103-65-1
ND
ug/kg
8.5
1
03/18/2013:32
03/18/2016:51
100-42-5
ND
ug/kg
8.5
1
03/18/2013:32
03/1812016:51
630-20-6
ND
ug/kg
8.5
1
03/18/2013:32
03/18/2016:51
79-34-5
ND
ug/kg
8.5
1
03/1812013:32
03/18/2016:51
127-18-4
ND
ug/kg
8.5
1
03/18/2013:32
03/18/2016:51
108-88-3
ND
ug/kg
8.5
1
03/18/2013:32
03/18/2016:51
87-61-6
ND
ug/kg
8.5
1
03/18/2013:32
03/18/2016:51
120-82-1
ND
ug/kg
8.5
1
03/18/2013:32
03/18/2016:51
71-55-6
ND
ug/kg
8.5
1
03/18/2013:32
03/18/2016:51
79-00-5
ND
ug/kg
8.5
1
03/18/2013:32
03/18/2016:51
79-01-6
ND
ug/kg
8.5
1
03/18/2013:32
03118/2016:51
75-69-4
ND
ug/kg
8.5
1
03/18/2013:32
03/1812016:51
96-18-4
ND
ug/kg
8.5
1
03/18/2013:32
03/1812016:51
95-63-6
ND
ug/kg
8.5
1
03/18/2013:32
03/18/2016:51
108-67-8
ND
ug/kg
84.7
1
03118/2013:32
03/18/2016:51
108-05-4
ND
ug/kg
16.9
1
03/18/2013:32
03/18/2016:51
75-01-4
ND
ug/kg
16.9
1
03/18/2013:32
03/18/2016:51
1330-20-7
ND
ug/kg
16.9
1
03/18/2013:32
03/18/2016:51
179601-23-1
ND
ug/kg
8.5
1
03/18/2013:32
03/18/2016:51
95-47-6
99
%
70-130
1
03/18/2013:32
03118/2016:51
2037-26-5
96
%
70-130
1
03118/2013:32
03118/2016:51
460-00-4
104
%
70-132
1
03/18/2013:32
03/18/2016:51
17060-07-0
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 38.6 % 0.10 1 03/16/20 16:40
Total Solids 2540 G-2011 Analytical Method: SM 2540G Preparation Method: SM 2540 G
Total Solids 60.7 % 1 03/24/20 22:51 03/24/20 23:03
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 59

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ANALYTICAL RESULTS
Project: 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-3 (0-6") Lab ID: 92469653002 Collected: 03/11/20 10:50 Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)
ND
mg/kg
15,8
1
03/19/20 17:33
03/23/20 10:34
N2
Aliphatic (C19-C36)
ND
mg/kg
15.8
1
03/19/20 17:33
03/23/20 10:34
N2
Aromatic (Cl 1-C22)
ND
mg/kg
15.8
1
03/19/20 17:33
03/23/20 10:34
N2
Surrogates
Nonatriacontane (S)
52
%
40-140
1
03/19/20 17:33
03/23/20 10:34
7194-86-7
o-Terphenyl (S)
74
%
40-140
1
03/19/20 17:33
03/23/20 10:34
84-15-1
2-Fluorobiphenyl (S)
109
%
40-140
1
03/19/20 17:33
03/23/20 10:34
321-60-8
2-Bromonaphthalene (S)
108
%
40-140
1
03/19/20 17:33
03/23/20 10:34
580-13-2
MADEPV
Analytical Method:
MADEP VPH Preparation Method:
MADEPV
Aliphatic (C05-CO8)
ND
mg/kg
7.65
1
03/11/20 10:50
03/25/20 22:52
Aliphatic (C09-C12)
ND
mg/kg
7,65
1
03/11/20 10:50
03/25/20 22:52
Aromatic (C09-C10),Unadjusted
ND
mg/kg
7.65
1
03/11/20 10:50
03/25/20 22:52
Total VPH
ND
mg/kg
7.65
1
03/11/20 10:50
03/25/20 22:52
Surrogates
2,5-Dibromotoluene (FID)
85.5
%
70-130
1
03/11120 10:50
03/25/20 22:52
2,5-Dibromotoluene (PID)
82.1
%
70-130
1
03/11/20 10:50
03/25/20 22:52
8270E MSSV Microwave
Analytical Method: EPA 8270E
Preparation Methods EPA 3546
Acenaphthene
ND
ug/kg
518
1
03/1912012:55
03/20/20 14:45
83-32-9
Acenaphthylene
ND
ug/kg
518
1
03/1912012:55
03/20/20 14:45
208-96-8
Aniline
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
62-53-3
Anthracene
ND
ug/kg
518
1
03119/2012:55
03/20/20 14:45
120-12-7
Benzo(a)anthracene
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
56-55-3
Benzo(a)pyrene
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
207-08-9
Benzoic Acid
ND
ug/kg
2590
1
03/1912012:55
03/2012014:45
65-85-0
Benzyl alcohol
ND
ug/kg
1040
1
03/19/20 12:55
03/20/20 14:45
100-51-6
4-Bromophenylphenylether
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
101-55-3
Butylbenzylphthalate
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
85-68-7
4-Chloro-3-methylphenol
ND
ug/kg
1040
1
03/19/20 12:55
03/2012014:45
59-50-7
4-Chloroaniline
ND
ug/kg
1040
1
03/19/20 12:55
03/20/20 14:45
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
111-444
2-Chloronaphthalene
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
91-58-7
2-Chlorophenol
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
7005-72-3
Chrysene
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
53-70-3
Dibenzofuran
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
518
1
03/1912012:55
03/20/20 14:45
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
1040
1
03/19/20 12:55
03/20/20 14:45
91-94-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 59

laceAnalj4icalo
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1
ANALYTICAL RESULTS
Project: 842 UST
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Project No.: 92469653
Sample: SB-3 (0-6") Lab ID: 92469653002 Collected: 03/11/20 10:50 Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
2,4-Dichlorophenol
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
120-83-2
Diethylphthalate
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
84-66-2
2,4-Dimethylphenol
ND
ug/kg
518
1
03/1912012:55
03/20/20 14:45
105-67-9
Dimethylphthalate
ND
ug/kg
518
1
03/19/2012:55
03/20/20 14:45
131-11-3
Di-n-butylphthalate
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/kg
1040
1
03/19/20 12:55
03/20/20 14:45
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2590
1
03/1912012:55
03/20/20 14:45
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
606-20-2
Di-n-octylphthalate
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
117-84-0
bis(2-Ethylhexyi)phthalate
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
117-81-7
Fluoranthene
ND
ug/kg
518
1
03/19/20 12:55
03120/2014:45
206-44-0
Fluorene
ND
ug/kg
518
1
03/19/20 12:55
03120/2014:45
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
87-68-3
Hexachlorobenzene
ND
ug/kg
518
1
03/19/20 12:55
03/2012014:45
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
518
1
03/19/20 12:55
03/2012014:45
77-47-4
Hexachloroethane
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
518
1
03/19/20 12:55
03/20/2014A5
193-39-5
Isophorone
ND
ug/kg
518
1
03/19/20 12:55
03120/2014:45
78-59-1
1-Methylnaphthalene
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
90-12-0
2-Methylnaphthalene
ND
ug/kg
518
1
03/19/20 12:55
03120/2014:45
91-57-6
2-Methylphenol(o-Cresol)
ND
uglkg
518
1
03/19/20 12:55
03/2012014:45
95-48-7
3&4-Methylphenol(m&p Cresol)
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
15831-10-4
Naphthalene
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
91-20-3
2-Nitroaniline
ND
ug/kg
2590
1
03/1912012:55
03/20/20 14:45
88-74-4
3-Nitroaniline
ND
ug/kg
2590
1
03/19/20 12:55
03/20/20 14:45
99-09-2
4-Nitroaniline
ND
ug/kg
1040
1
03/19/20 12:55
03/20/20 14:45
100-01-6
Nitrobenzene
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
98-95-3
2-Nitrophenol
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
88-75-5
4-Nitrophenol
ND
ug/kg
2590
1
03/19/20 12:55
03/20/20 14:45
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
518
1
03/1912012:55
03/20/20 14:45
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
518
1
03/1912012:55
03/20/20 14:45
108-60-1
Pentachlorophenol
ND
ug/kg
1040
1
03/1912012:55
03/20/20 14:45
87-86-5
Phenanthrene
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
85-01-8
Phenol
ND
ug/kg
518
1
03/1912012:55
03/20/20 14:45
108-95-2
Pyrene
ND
ug/kg
518
1
03/19/20 12:55
03120/2014:45
129-00-0
Pyridine
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
518
1
03/19/20 12:55
03/20/20 14:45
88-06-2
Surrogates
Nitrobenzene-d5 (S)
75
%
23-110
1
03/19/20 12:55
03/20/20 14:45
4165-60-0
2-Fluorobiphenyl (S)
54
%
30-110
1
03/19/20 12:55
03/20/20 14:45
321-60-8
Terphenyl-d14 (S)
54
%
28-110
1
03/19/20 12:55
03/20/20 14:45
1718-51-0
REPORT OF LABORATORY ANALYSIS
Qual
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Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 59

Pace Analytical Services, LLC
aceAnalytical 9800 Kincey Ave, Suite 100
www.pacelabs.com Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 842 UST
Pace Project No.: 92469653
Sample: SB-3 (0-6") Lab ID: 92469653002 Collected: 03/11/20 10:50 Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted forpercent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546
Surrogates
Phenol-d6 (S)
45
%
22-110
1
03/19/20 12:55
03/20/20 14:45
13127-88-3
2-Fluorophenol (S)
38
%
13-110
1
03119/20 12:55
03/20/20 14:45
367-12-4
2,4,6-Tribromophenol (S)
62
%
27-110
1
03/19/20 12:55
03/20/20 14:45
118-79-6
8260D15035A Volatile Organics
Analytical Method: EPA 8260D
Preparation Method:
EPA 5035A
Acetone
166
ug/kg
125
1
03/18/20 13:32
03/18/20 17:16
67-64-1
Benzene
ND
ug/kg
6.2
1
03/18/20 13:32
03/18/20 17:16
71-43-2
Bromobenzene
ND
ug/kg
61
1
03/18/20 13:32
03/1812017:16
108-86-1
Bromochloromethane
ND
ug/kg
6.2
1
03/18/20 13:32
03/18/20 17:16
74-97-5
Bromodichloromethane
ND
ug/kg
6.2
1
03/18/20 13:32
03118/2017:16
75-27-4
Bromoform
ND
ug/kg
6.2
1
03/18/20 13:32
03/18/20 17:16
75-25-2
Bromomethane
ND
ug/kg
12.5
1
0311812013:32
03118/2017:16
74-83-9
2-Butanone (MEK)
ND
ug/kg
125
1
03/18/20 13:32
03/18/20 17:16
78-93-3
n-Butylbenzene
ND
ug/kg
6.2
1
03/18/20 13:32
03/18/20 17:16
104-51-8
sec-Butylbenzene
ND
ug/kg
6:2
1
03/18/20 13:32
03/18/20 17:16
135-98-8
tert-Butylbenzene
ND
ug/kg
6.2
1
03/18/20 13:32
03/18/20 17:16
98-06-6
Carbon tetrachloride
ND
uglkg
6.2
1
03/18/20 13:32
03/18/20 17:16
56-23-5
Chlorobenzene
ND
ug/kg
6.2
1
03/18/20 13:32
03/1812017:16
108-90-7
Chloroethane
ND
ug/kg
12.5
1
03/18/20 13:32
03118/2017:16
75-00-3
Chloroform
ND
ug/kg
6.2
1
03/18/20 13:32
03/18/20 17:16
67-66-3
Chloromethane
ND
ug/kg
12.5
1
03/18/20 13:32
03/18/20 17:16
74-87-3
2-Chlorotoluene
ND
ug/kg
6.2
1
03118/2013:32
03/18/20 17:16
95-49-8
4-Chlorotoluene
ND
ug/kg
6.2
1
03118/2013:32
03/18/20 17:16
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
62
1
03/18/20 13:32
03/18/20 17:16
96-12-8
Dibromochioromethane
ND
ug/kg
6.2
1
03/18/20 13:32
03/18/20 17:16
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
6.2
1
03/18/20 13:32
03/18/20 17:16
106-93-4
Dibromomethane
ND
ug/kg
6.2
1
03/18/20 13:32
03/18/20 17:16
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
6.2
1
03/18/20 13:32
03118/2017:16
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
6.2
1
0311812013:32
03/1812017:16
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
6.2
1
03/18/20 13:32
03118/2017:16
106-46-7
Dichlorodifluoromethane
ND
ug/kg
12.5
1
03/18/20 13:32
03/18/20 17:16
75-71-8
1,1-Dichloroethane
ND
ug/kg
6.2
1
03/18/20 13:32
03/18/20 17:16
75-34-3
1,2-Dichloroethane
ND
uglkg
6.2
1
03/18/20 13:32
03/18/20 17:16
107-06-2
1,1-Dichloroethene
ND
ug/kg
6.2
1
03/18/20 13:32
03/18/20 17:16
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
62
1
03/18/20 13:32
03/18/20 17:16
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
6.2
1
03/18/20 13:32
03/18/20 17:16
156-60-5
1,2-Dichloropropane
ND
ug/kg
6.2
1
03118/2013:32
03/18/20 17:16
78-87-5
1,3-Dichloropropane
ND
ug/kg
6.2
1
03/18/20 13:32
03/18/20 17:16
142-28-9
2,2-Dichloropropane
ND
ug/kg
6.2
1
03/18/20 13:32
03/18/20 17:16
594-20-7
1,1-Dichloropropene
ND
ug/kg
6.2
1
03/18/20 13:32
03/18/20 17:16
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
6.2
1
03/18/20 13:32
03/18/20 17:16
10061-01-5
trans-1,3-Dichloropropene
ND
ug/kg
6.2
1
03/18/20 13:32
03/18/20 17:16
10061-02-6
Diisopropyl ether
ND
ug/kg
6.2
1
03/18/20 13:32
03/18/20 17:16
108-20-3
Ethylbenzene
ND
ug/kg
6.2
1
03/18/20 13:32
03/18/20 17:16
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
6.2
1
03/18/20 13:32
03/1812017:16
87-68-3
REPORT OF LABORATORY ANALYSIS
IH,vl
vi
v1
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 59

1�?ceAnalyticala
www.pacolabs.com
ANALYTICAL RESULTS
Project: 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-3 (0-6") Lab ID: 92469653002 Collected: 03/11/20 10:50 Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D/5035A Volatile Organics
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2, 3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Tri c h l o rofl u o ro m ethane
1,2,3-Trichloropropane
1,2,4-Tri methyl benzene
1,3,5-Tri methyl benzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Total Solids 2540 G-2011
Total Solids
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
62.5
1
03/18/2013:32
03/18/2017:16
591-78-6
ND
ug/kg
6.2
1
03/18/2013:32
03/18/2017:16
98-82-8
ND
ug/kg
6.2
1
03/18/2013:32
03/18/2017:16
99-87-6
ND
ug/kg
25.0
1
03/18/2013:32
03/18/2017:16
75-09-2
ND
ug/kg
62.5
1
03/18/2013:32
03/18/2017:16
108-10-1
ND
ug/kg
6.2
1
03/18/2013:32
03/18/2017:16
1634-04-4
ND
ug/kg
6.2
1
03/18/2013:32
03/18/2017:16
91-20-3
ND
ug/kg
6.2
1
03/18/2013:32
03/18/2017:16
103-65-1
ND
ug/kg
6.2
1
03/18/2013:32
03/18/2017:16
100-42-5
ND
ug/kg
6.2
1
03/18/2013:32
03/18/2017:16
630-20-6
ND
ug/kg
6.2
1
03/18/2013:32
03/18/2017:16
79-34-5
ND
ug/kg
6.2
1
03/18/2013:32
03/18/2017:16
127-18-4
ND
ug/kg
6.2
1
03/18/2013:32
03/18/2017:16
108-88-3
ND
ug/kg
6.2
1
03/18/2013:32
03/18/2017:16
87-61-6
ND
ug/kg
6.2
1
03/18/2013:32
03/18/2017:16
120-82-1
ND
ug/kg
6.2
1
03/18/2013:32
03/18/2017:16
71-55-6
ND
ug/kg
6.2
1
03/18/2013:32
03/18/2017:16
79-00-5
ND
ug/kg
6.2
1
03/18/2013:32
03/18/2017:16
79-01-6
ND
ug/kg
6.2
1
03/18/2013:32
03/18/2017:16
75-69-4
ND
ug/kg
6.2
1
03/18/2013:32
03/18/2017:16
96-18-4
ND
ug/kg
6.2
1
03/18/2013:32
03/18/2017:16
95-63-6
ND
ug/kg
6.2
1
03/18/2013:32
03/18/2017:16
108-67-8
ND
ug/kg
62.5
1
03/18/2013:32
03/18/2017:16
108-05-4
ND
ug/kg
12.5
1
03/18/2013:32
03/18/2017:16
75-01-4
ND
ug/kg
12.5
1
03/18/2013:32
03/18/2017:16
1330-20-7
ND
ug/kg
12.5
1
03/18/2013:32
03/18/2017:16
179601-23-1
ND
ug/kg
6.2
1
03/18/2013:32
03/18/2017:16
95-47-6
100
%
70-130
1
03/18/2013:32
03/18/2017:16
2037-26-5
97
%
70-130
1
03/18/2013:32
03/18/2017:16
460-00-4
106
%
70-132
1
03/18/2013:32
03/18/2017:16
17060-07-0
Analytical Method: ASTM D2974-87
36,1 % 0.10 1 03/16/2016:40
Analytical Method: SM 2540G Preparation Method: SM 2540 G
65.4 %
1 03/24/20 22:51 03/24/20 23:03
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 59

Vacie Analytical
www.pacelabs.com
ANALYTICAL RESULTS
Project: 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvilie, NC 28078
[phone]
Sample: SB-1 (18"-24") Lab ID: 92469653003 Collected: 03/11/20 13:40 Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)
64.0
mg/kg
27.8
2
03/19/20 17:33
03/23/20 12:28
N2
Aliphatic (C19-C36)
ND
mg/kg
27.8
2
03/19/20 17:33
03/23/20 12:28
N2
Aromatic (C11-C22)
42.7
mg/kg
13.9
1
03/19/20 17:33
03/23/20 11:02
N2
Surrogates
Nonatriacontane (S)
57
%
40-140
2
03/19/20 17:33
03/23/20 12:28
7194-86-7
o-Terphenyl (S)
89
%
40-140
1
03/19/20 17:33
03/23/20 11:02
84-15-1
2-Fluorobiphenyl (S)
107
%
40-140
1
03/19/20 17:33
03/23/20 11:02
321-60-8
2-Bromonaphthalene (S)
144
%
40-140
1
03/19/20 17:33
03/23/20 11:02
580-13-2
S5
MADEPV Analytical Method: MADEP VPH Preparation Method: MADEPV
Aliphatic(C05-CO8)
ND
mg/kg
8,67
1.28
03/11/20 13:40
03/25/20 23:25
Aliphatic (C09-C12)
20.9
mg/kg
8.67
1.28
03/11/20 13:40
03/25/20 23:25
Aromatic (C09-C10),Unadjusted
16.5
mg/kg
8.67
1.28
03/11/20 13:40
03/25/20 23:25
Total VPH
37.4
mg/kg
8.67
1.28
0311112013:40
03/25/20 23:25
Surrogates
2,5-Dibromotoluene (FID)
92.9
%
70-130
1.28
03/11/20 1340
03/25/20 23:25
2,5-Dibromotoluene (PID)
84.2
%
70-130
1.28
03/11120 13:40
03/25/20 23:25
8270E MSSV Microwave
Analytical Method: EPA 8270E
Preparation Method:
EPA 3546
Acenaphthene
ND
ug/kg
448
1
03119/2012:55
03/20/20 15:12
83-32-9
Acenaphthylene
ND
ug/kg
448
1
03119/2012:55
03/20/20 15:12
208-96-8
Aniline
ND
ug/kg
448
1
03119/2012:55
03/20/20 15:12
62-53-3
Anthracene
ND
ug/kg
448
1
03/19/20 12:55
03/20/20 15:12
120-12-7
Benzo(a)anthracene
ND
ug/kg
448
1
03/19/20 12:55
03/20/20 15:12
56-55-3
Benzo(a)pyrene
ND
ug/kg
448
1
03/19/20 12:55
03/20/20 15:12
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
448
1
03/19/20 12:55
03/20/20 15:12
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
448
1
03/19/20 12:55
03/20/20 15:12
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
448
1
03/19/20 12:55
03/20/20 15:12
207-08-9
Benzoic Acid
ND
ug/kg
2240
1
03/19/20 12:55
03/20/20 15:12
65-85-0
Benzyl alcohol
ND
ug/kg
897
1
03/19/20 12:55
03/20/20 15:12
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
448
1
03/19/20 12:55
03/20/20 15:12
101-55-3
Butylbenzylphthalate
ND
ug/kg
448
1
03/19/20 12:55
03/20/20 15:12
85-68-7
4-Chloro-3-methylphenol
ND
ug/kg
897
1
03/19/20 12:55
03/20/20 15:12
59-50-7
4-Chloroaniline
ND
uglkg
897
1
03/19/20 12:55
03/2012015:12
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
448
1
03/19/20 12:55
03/20/20 15:12
111-91-1
bis(2-Chloroethyi) ether
ND
ug/kg
448
1
03/19/20 12:55
03/20/20 15:12
111-44-4
2-Chloronaphthalene
ND
ug/kg
448
1
03/1912012:55
03/2012015:12
91-58-7
2-Chlorophenol
ND
uglkg
448
1
03/19/20 12:55
03/20/20 15:12
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
448
1
03/19/20 12:55
03/20/20 15:12
7005-72-3
Chrysene
ND
ug/kg
448
1
03/19/20 12:55
03/20/20 15:12
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
448
1
03119/2012:55
03/20/20 15:12
53-70-3
Dibenzofuran
ND
ug/kg
448
1
03/19/20 12:55
03/20/20 15:12
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
448
1
03/19/20 12:55
03/20/20 15:12
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
448
1
03/19/20 12:55
03/20/20 15:12
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
448
1
03/19/20 12:55
03/20/20 15:12
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
897
1
03/19/20 12:55
03/20/20 15:12
91-94-1
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced,
except
in full,
Date: 03/26/2020 01:45 PM
without the written consent of Pace Analytical Services, LLC.
Page 21 of 59

aceAnalXical
www.pacelab$.com
ANALYTICAL RESULTS'
Project: 842 UST
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Project No.: 92469653
Sample: SB-1 (18"-24") Lab ID: 92469653003 Collected: 03/11/20 13:40 Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546
2,4-Dichlorophenol
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
120-83-2
Diethylphthalate
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
84-66-2
2,4-Dimethylphenol
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
105-67-9
Dimethylphthalate
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
131-11-3
Di-n-butylphthalate
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
84-74-2
4,6-Dinitro-2-methyiphenol
ND
ug/kg
897
1
03/19/20 12:55
03/2012015:12
534-52-1
2,4-Dinitrophenoi
ND
ug/kg
2240
1
03/19/20 12:55
03/20/2015:12
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
448
1
03119/2012:55
03/2012015:12
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
606-20-2
Di-n-octylphthalate
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
117-84-0
bis(2-Ethylhexyl)phthalate
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
117-81-7
Fluoranthene
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
206-44-0
Fluorene
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
448
1
03/19/2012.55
03/20/2015:12
87-68-3
Hexachlorobenzene
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
77-47-4
Hexachloroethane
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
193-39-5
Isophorone
ND
ug/kg
448
1
03119/2012:55
03/20/2015:12
78-59-1
1-Methylnaphthalene
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
90-12-0
2-Methylnaphthalene
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
95-48-7
3&4-Methylphenol(m&p Cresol)
ND
ug/kg
448
1
03/19/20 12:55
03/20/20 15:12
15831-10-4
Naphthalene
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
91-20-3
2-Nitroaniline
ND
ug/kg
2240
1
03/19/20 12:55
03/20/2015:12
88-74-4
3-Nitroaniline
ND
ug/kg
2240
1
03/1912012:55
03/20/2015:12
99-09-2
4-Nitroaniline
ND
ug/kg
897
1
03/19/20 12:55
03/20/2015:12
100-01-6
Nitrobenzene
ND
ug/kg
448
1
03/19/20 12:55
0312012015:12
98-95-3
2-Nitrophenol
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
88-75-5
4-Nitrophenol
ND
ug/kg
2240
1
03/19/20 12:55
03/20/2015:12
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
448
1
03/19/20 12:55
03/2012015:12
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
108-60-1
Pentachlorophenol
ND
ug/kg
897
1
03/1912012:55
03/20/2015:12
87-86-5'
Phenanthrene
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
85-01-8
Phenol
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
108-95-2
Pyrene
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
129-00-0
Pyridine
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
120-82-1
2,4,5-Tdchlorophenol
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
448
1
03/19/20 12:55
03/20/2015:12
88-06-2
Surrogates
Nitrobenzene-d5 (S)
64
%
23-110
1
03/19/20 12:55
03/20/20 15:12
4165-60-0
2-Fiuorobiphenyl (S)
57
%
30-110
1
03/19/20 12:55
03/20/20 15:12
321-60-8
Terphenyl-d14 (S)
66
%
28-110
1
03/19/20 12:55
03/20/20 15:12
1718-51-0
REPORT OF LABORATORY ANALYSIS
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Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC, Page 22 of 59

aceAnalyflcal
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ANALYTICAL RESULTS
Project: 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersviile; NC 28078
[phone]
Sample: SB-1 (18"-24") Lab ID: 92469653003 Collected: 03/11/20 13:40 Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Surrogates
Phenol-d6 (S)
53
%
22-110
1
03/19/20 12:55
03/20/20 15:12
13127-88-3
2-Fluorophenol (S)
56
%
13-110
1
03/19/20 12:55
03/20/20 15:12
367-12-4
2,4,6-Tribromophenoi (S)
80
%
27-110
1
03/19/20 12:55
03/20/20 15:12
118-79-6
8260D/5035A Volatile Organics
Analytical Method:
EPA 8260D
Preparation Method:
EPA 5035A
Acetone
ND
ug/kg
101
1
03/18/20 13:32
03/18/20 17:41
67-64-1
Benzene
ND
ug/kg
5.0
1
03/18/20 13:32
03/18/20 17:41
71-43-2
Bromobenzene
ND
ug/kg
5.0
1
03/1812013:32
03/18/20 17:41
108-86-1
Bromochloromethane
ND
ug/kg
5.0
1
03/18/20 13:32
03/18/20 17:41
74-97-5
Bromodichloromethane
ND
ug/kg
5.0
1
03/18/20 13:32
03118/2017:41
75-27-4
Bromoform
ND
ug/kg
&0
1
03/18/20 13:32
03/18/20 17:41
75-25-2
Bromomethane
ND
ug/kg
10.1
1
03/18/20 13:32
03/18/20 17:41
74-83-9 IH,v1
2-Butanone (MEK)
ND
ug/kg
101
1
03/18/20 13:32
03/18/20 17:41
78-93-3
n-Butylbenzene
ND
ug/kg
5.0
1
03/1812013:32
03/18/20 17:41
104-51-8
sec-Butylbenzene
ND
ug/kg
5.0
1
03/18/20 13:32
03/18/20 17:41
135-98-8
tert-Butylbenzene
ND
ug/kg
5.0
1
03/1812013:32
03/18/20 17:41
98-06-6
Carbon tetrachloride
ND
ug/kg
5.0
1
03/18/20 13:32
03/18/20 17:41
56-23-5
Chlorobenzene
ND
ug/kg
5.0
1
03/1812013:32
03/18/20 17:41
108-90-7
Chloroethane
ND
ug/kg
10.1
1
03/18/20 13:32
03/18/20 17:41
75-00-3 v1
Chloroform
ND
ug/kg
5.0
1
03/1812013:32
03/18/20 17:41
67-66-3
Chloromethane
ND
ug/kg
10A
1
03/18/20 13:32
03/18/20 17:41
74-87-3
2-Chlorotoluene
ND
ug/kg
5.0
1
03/18/20 13:32
03/18/20 17:41
95-49-8
4-Chlorotoluene
ND
ug/kg
5.0
1
03/18/20 13:32
03/18/20 17:41
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
5.0
1
03/18/20 13:32
03/18/20 17:41
96-12-8
Dibromochloromethane
ND
ug/kg
5.0
1
03/18/20 13:32
03/18/20 17:41
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
5.0
1
03/18/20 13:32
03/18/20 17:41
106-93-4
Dibromomethane
ND
ug/kg
5.0
1
03/18/20 13:32
03/18/2017A1
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
5.0
1
03/18/20 13:32
03/18/20 17:41
95-50-1
1,3-Dichlorobenzene
ND
uglkg
5.0
1
03/18/20 13:32
03/1812017:41
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
5.0
1
03/18/20 13:32
03/18/20 17:41
106.46-7
Dichlorodifluoromethane
ND
ug/kg
10.1
1
03/18/20 13:32
03/18/20 17:41
75-71-8 v1
1„1-Dichloroethane
ND
ug/kg
5.0
1
03/18/20 13:32
03/18/20 17:41
75-34-3
1,2-Dichloroethane
ND
ug/kg
5.0
1
03/18/20 13:32
03/1812017:41
107-06-2
1,1-Dichloroethene
ND
uglkg
5.0
1
03/18/20 13:32
03/18/20 17:41
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
5.0
1
03/18/20 13:32
03/18/20 17:41
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
5.0
1
03/18/20 13:32
03/18/20 17:41
156-60-5
1,2-Dichloropropane
ND
ug/kg
&0
1
03/18/20 13:32
03/18/20 17:41
78-87-5
1,3-Dichloropropane
ND
ug/kg
5.0
1
03/18/20 13:32
03118/2017:41
142-28-9
2,2-Dichloropropane
ND
ug/kg
5.0
1
03/18/20 13:32
03/18/20 17:41
594-20-7
1,1-Dichloropropene
ND
ug/kg
5.0
1
03/18/20 13:32
03/1812017:41
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
5.0
1
03118/2013:32
03/18/20 17:41
10061-01-5
trans-1,3-Dichloropropene
ND
ug/kg
5.0
1
03/18/20 13:32
03/18/20 17:41
10061-02-6
Diisopropyl ether
ND
ug/kg
5.0
1
03118/20 13:32
03/18/20 17:41
108-20-3
Ethylbenzene
ND
ug/kg
5.0
1
03/18/20 13:32
03/18/20 17:41
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
5.0
1
03/1812013:32
03/18/20 17:41
87-68-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, I.I.C. Page 23 of 59

_per aceAnalytical
www.pacelabs.com
ANALYTICAL RESULTS
Project, 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-1 (18"-24") Lab ID: 92469653003 Collected: 03/11/20 13:40 Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D/5035A Volatile Organics
2-Hexanone
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroetha ne
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofl uorometha ne
1,2,3-Trichloropropane
1,2,4-Tdmethylbenzene
1,3, 5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Total Solids 2540 G-2011
Total Solids
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
50.4
1
03/18/2013:32
03/18/2017:41
591-78-6
ND
ug/kg
5.0
1
03/18/2013:32
03/18/2017:41
98-82-8
10.6
ug/kg
5.0
1
03/18/2013:32
03/18/2017:41
99-87-6
ND
ug/kg
20.2
1
03/1812013:32
03/18/2017t41
75-09-2
ND
ug/kg
50.4
1
03/18/2013:32
03/18/2017:41
108-10-1
ND
ug/kg
5.0
1
03/18/2013:32
03/18/2017:41
1634-04-4
18.1
ug/kg
5.0
1
03/18/2013:32
03/18/2017:41
91-20-3
ND
ug/kg
5.0
1
03/18/2013:32
03/18/2017:41
103-65-1
ND
ug/kg
5.0
1
03/18/2013:32
03/18/2017:41
100-42-5
ND
ug/kg
5.0
1
03/18/2013:32
03/18/2017:41
630-20-6
ND
ug/kg
5.0
1
03/18/2013:32
03/18/2017:41
79-34-5
ND
ug/kg
5.0
1
03/1812013:32
03/18/2017:41
127-18-4
ND
ug/kg
5,0
1
03/18/2013:32
03/18/2017:41
108-88-3
ND
ug/kg
5.0
1
03/18/2013:32
03/18/2017:41
87-61-6
ND
ug/kg
5.0
1
03/18/2013:32
03/18/2017:41
120-82-1
ND
ug/kg
5.0
1
03/18/2013:32
03/18/2017:41
71-55-6
ND
ug/kg
5.0
1
03/18/2013:32
03/1812017:41
79-00-5
ND
ug/kg
5.0
1
03/18/2013:32
03/18/2017:41
79-01-6
ND
ug/kg
5.0
1
03/1812013:32
03/18/2017:41
75-694
ND
ug/kg
5.0
1
03118/2013:32
03/18/2017:41
96-18-4
8.7
ug/kg
5.0
1
03/18/2013:32
03/18/2017:41
95-63-6
8.3
ug/kg
5.0
1
03/18/2013:32
03118/2017:41
108-67-8
ND
ug/kg
50A
1
03/18/2013:32
03/18/2017:41
108.05-4
ND
ug/kg
10.1
1
03/18/2013:32
03/18/2017:41
75-01-4
ND
ug/kg
10.1
1
03/18/2013:32
03/18/2017:41
1330-20.7
ND
ug/kg
10.1
1
03/18/2013:32
03/18/2017:41
179601-23-1
7.9
ug/kg
5.0
1
03/18/2013:32
03/18/2017:41
95-47-6
101
%
70-130
1
03/18/2013:32
03/1812017:41
2037-26-5
99
%
70-130
1
03118/2013:32
03/18/2017:41
460-00-4
104
%
70-132
1
03/18/2013:32
03/18/2017:41
17060-07-0
Analytical Method: ASTM D2974-87
26.9 % 0.10 1 03/16/2016:40
Analytical Method: SM 2540G Preparation Method: SM 2540 G
73.8 %
1 03/24/20 22:51 03/24/20 23:03
REPORT OF LABORATORY ANALYSIS
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Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 59

aceAnalyfiical o
www.pacelabs.com
ANALYTICAL RESULTS
Project: 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-4 (T) Lab ID: 92469653004 Collected: 03/13/20 10:00 Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)
ND
mg/kg
13.0
1
03/19/20 17:33
03/23/20 11:29
N2
Aliphatic (C19-C36)
ND
mg/kg
13.0
1
03/19/20 1733
03/23/20 11:29
N2
Aromatic (C11-C22)
ND
mg/kg
13.0
1
03/19/20 17:33
03/23/20 11:29
N2
Surrogates
Nonatriacontane (S)
68
%
40-140
1
03/19/20 17:33
03/23/20 11:29
7194-86-7
o-Terphenyl (S)
80
%
40-140
1
03/19/20 17:33
03/23/20 11:29
84-15-1
2-Fluorobiphenyl (S)
101
%
40-140
1
03/19/20 17:33
03/23/20 11:29
321-60-8
2-Bromonaphthalene (S)
144
%
40-140
1
03/19/20 17:33
03/23/20 11:29
580-13-2
S5
MADEPV Analytical Method: MADEP VPH Preparation Method: MADEPV
Aliphatic (C05-008)
ND
mg/kg
6.46
1
03/13/20 10:00
03/25/20 23:58
Aliphatic (C09-C12)
ND
mg/kg
6.46
1
03/13/20 10:00
03/25/20 23:58
Aromatic (C09-C10),Unadjusted
ND
mg/kg
6.46
1
03/13/20 10:00
03/25/20 23:58
Total VPH
ND
mg/kg
6.46
1
03/13/20 10:00
03/25/20 23:58
Surrogates
2,5-Dibromotoluene (FID)
83.1
%
70-130
1
03/13/20 10:00
03/25/20 23:58
2,5-Dibromotoluene (PID)
80.1
%
70-130
1
03/13/20 10:00
03/25/20 23:58
8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546
Acenaphthene
ND
ug/kg
431
1
03119/2012:55
03/20/20 15:40
83-32-9
Acenaphthylene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
208-96-8
Aniline
ND
ug/kg
431
1
03/19/20 12:55
03/2012015:40
62-53-3
Anthracene
ND
ug/kg
431
1
03/19/20 12:55
03/2012015:40
120-12-7
Benzo(a)anthracene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
56-55-3
Benzo(a)pyrene
ND
ug/kg
431
1
03119/2012:55
03/20/20 15:40
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
431
1
03119/2012:55
03/2012015:40
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
207-08-9
Benzoic Acid
ND
ug/kg
2150
1
03/19/20 12:55
03/20/20 15:40
65-85-0
Benzyl alcohol
ND
ug/kg
861
1
03/19/20 12:55
03/20/20 15:40
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
101-55-3
Butylbenzyiphthalate
ND
ug/kg
431
1
03119/2012:55
03/20/20 15:40
85-68-7
4-Chloro-3-methylphenol
ND
ug/kg
861
1
03/19/20 12:55
03/20/20 15:40
59-50-7
4-Chloroaniline
ND
ug/kg
861
1
03/19/20 12:55
03/20/20 15:40
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
111-44-4
2-Chloronaphthalene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
91-58-7
2-Chlorophenol
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
7005-72-3
Chrysene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
53-70-3
Dibenzofuran
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
431
1
03/19/20 12:55
03/2012015:40
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
861
1
03/19/20 12:55
03/20/20 15:40
91-94-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 59

aceAnalytical
www.pacelab3.com
ANALYTICAL RESULTS
Project: 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersviile; NC 28078
[phone]
Sample: SB-4 (1) Lab ID: 92469653004 Collected: 03113/20 10:00 Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546
2,4-Dichloropheno►
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
120-83-2
Diethylphthalate
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
84-66-2
2,4-Dimethylphenol
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
105-67-9
Dimethylphthalate
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
131-11-3
Di-n-butylphthalate
ND
ug/kg
431
1
03119/2012:55
03/20/20 15:40
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/kg
861
1
03/19/20 12:55
03/20/20 15:40
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2150
1
03/19/20 12:55
03/20/20 15:40
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
606-20-2
Di-n-octylphthalate
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
117-84-0
bis(2-Ethylhexyi)phthalate
ND
ug/kg
431
1
03/19/20 12:55
03120/2015:40
117-81-7
Fluoranthene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
206-44-0
Fluorene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
87-68-3
Hexachlorobenzene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
118-74-1
Hexachiorocyclopentadiene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
77-47-4
Hexachloroethane
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
193-39-5
Isophorone
ND
ug/kg
431
1
03119/2012:55
03/20/20 15:40
78-59-1
1-Methylnaphthalene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
90-12-0
2-Methy1naphthalene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
95-48-7
3&4-Methylphenol(m&p Cresol)
ND
ug/kg
431
1
03119/20 12:55
03/20/20 15:40
15831-10-4
Naphthalene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
91-20.3
2-Nitroaniilne
ND
ug/kg
2150
1
03/19/20 12:55
03/20/20 15:40
88-74-4
3-Nitroaniline
ND
ug/kg
2150
1
03119/2012:55
03120/2015:40
99-09-2
4-Nitroaniline
ND
ug/kg
861
1
03119/2012:55
03/2012015:40
100-01-6
Nitrobenzene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
98-95-3
2-Nitrophenol
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
88-75-5
4-Nitrophenol
ND
ug/kg
2150
1
03119/2012:55
03/20/20 15:40
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
431
1
03/19/20 12:55
03120/2015:40
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
108-60-1
Pentachlorophenol
ND
ug/kg
861
1
03/19/20 12:55
03120/2015:40
87-86-5
Phenanthrene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
85-01-8
Phenol
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
108-95-2
Pyrene
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
129-00-0
Pyridine
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
110-86-1
1,2,4-Trichiorobenzene
ND
ug/kg
431
1
03/19/20 12:55
03120/2015:40
120-82-1
2,4,5-Tdchlorophenol
ND
ug/kg
431
1
03119/2012:55
03/20/20 15:40
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
431
1
03/19/20 12:55
03/20/20 15:40
88-06-2
Surrogates
Nitrobenzene-d5 (S)
68
%
23-110
1
03/19/20 12:55
03/20/20 15:40
4165-60-0
2-Fluorobiphenyl (S)
54
%
30-110
1
03/19/20 12:55
03/20/20 15:40
321-60-8
Terphenyl-d14 (S)
63
%
28-110
1
03/19/20 12:55
03/20/20 15:40
1718-51-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 59

aeeAnalXieal
www.pacelabs.com
ANALYTICAL RESULTS
Project: 842 UST
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Project No.: 92469653
Sample: SB-4 (1') Lab ID: 92469653004 Collected: 03/13/20 10:00 Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No.
8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546
Surrogates
Phenol-d6 (S)
42
%
22-110
1
03/19/20 12:55
03/20/20 15:40
13127-88-3
2-Fluorophenol (S)
36
%
13-110
1
03/19/20 12:55
03/20/20 15:40
367-12-4
2,4,6-Tribromophenol (S)
48
%
27-110
1
03/19/20 12:55
,03/20/20 15:40
118-79-6
8260D/5035A Volatile Organics
Analytical Method: EPA 8260D
Preparation Method: EPA 5035A
Acetone
ND
ug/kg
130
1
03/1912011:32
03/19/20 14:15
67-64-1
Benzene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
71-43-2
Bromobenzene
ND
ug/kg
6.5
1
03/19/20 11:32
03119/2014:15
108-86-1
Bromochloromethane
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
74-97-5
Bromodichloromethane
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
75-27-4
Bromoform
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
75-25-2
Bromomethane
ND
ug/kg
13.0
1
03/19/20 11:32
03/19/20 14:15
74-83-9
2-Butanone (MEK)
ND
ug/kg
130
1
03/19/20 11:32
03/19/20 14:15
78-93-3
n-Butylbenzene
ND
ug/kg
6.5
1
03/1912011:32
03/19/20 14:15
104-51-8
sec-Butylbenzene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
135-98-8
tert-Butylbenzene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
98-06-6
Carbon tetrachloride
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
56-23-5
Chlorobenzene
ND
ug/kg
6.5
1
03/19/20 11:32
03/1912014:15
108-90-7
Chloroethane
ND
ug/kg
13.0
1
0311912011:32
03/19/20 14:15
75-00-3
Chloroform
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
67-66-3
Chloromethane
ND
ug/kg
13.0
1
03/19/20 11:32
03/19/20 14:15
74-87-3
2-Chlorotoluene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
95-49-8
4-Chlorotoluene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
6.5
1
03119/2011:32
03/19/20 14:15
96-12-8
Dibromochloromethane
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
106-93-4
Dibromomethane
ND
ug/kg
6„5
1
03/1912011:32
03119/2014:15
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
6.5
1
03/19/20 11:32
03119/2014:15
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
6„5
1
03/19/20 11:32
03/19/20 14:15
106-46-7
Dichlorodifluoromethane
ND
ug/kg
13.0
1
03/19/20 11:32
03/19/20 14:15
75-71-8
1,1-Dichloroethane
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
75-34-3
1,2-Dichloroethane
ND
ug/kg
6.5
1
03119/2011:32
03/19/20 14:15
107-06-2
1,1-Dichloroethene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
156-60-5
1,2-Dichloropropane
ND
ug/kg
6.5
1
03119/2011:32
03/19/20 14:15
78-87-5
1,3-Dichloropropane
ND
ug/kg
6„5
1
03/19/20 11:32
03/19/20 14:15
142-28-9
2,2-Dichloropropane
ND
ug/kg
6.5
1
03/19/20 11:32
03/1912014:15
594-20-7
1,1-Dichloropropene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
10061-01-5
trans-1,3-Dichloropropene
ND
ug/kg
6,5
1
03/19/20 11:32
03119/2014:15
10061-02-6
Diisopropyl ether
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
108-20-3
Ethylbenzene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
87-68-3
REPORT OF LABORATORY ANALYSIS
Qual
IH,v1
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 59

Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
I�AceAnalytical' Huntersville, NC 28078
www.pacelabs.com
[phone]
ANALYTICAL RESULTS
Project: 842 UST
Pace Project No.: 92469653
Sample: SB-4 (1') LAID: 92469653004 Collected: 03/13/20 10:00 Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D/5035A Volatile Organics
Analytical Method: EPA8260D Preparation Method: EPA5035A
2-Hexanone
ND
ug/kg
65.0
1
03/191201132
03/19/2014:15
591-78-6
Isopropyl benzene (Cumene)
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
98-82-8
p-Isopropyltoluene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
99-87-6
Methylene Chloride
ND
ug/kg
26.0
1
03/19/20 11:32
03/19/20 14:15
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
65.0
1
03/19/20 11:32
03/19/20 14:15
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
1634-04-4
Naphthalene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
91-20-3
n-Propylbenzene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
103-65-1
Styrene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/2014:15
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
6.5
1
03119/2011:32
03/19/20 14:15
79-34-5
Tetrachloroethene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
127-18-4
Toluene
ND
ug/kg
6:5
1
03/19120 11 :32
03/19/20 14:15
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
79-00-5
Trichloroethene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
79-01-6
Trichlorofluoromethane
ND
ug/kg
6.5
1
03119/2011:32
03/19/2014:16
75-69-4
1,2,3-Trichloropropane
ND
ug/kg
6,5
1
03/19/20 11:32
03/19/20 14:15
96-18-4
1,2,4-Trimethylbenzene
14.3
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
6.5
1
03/19/20 11:32
03/1912014:15
108-67-8
Vinyl acetate
ND
ug/kg
65.0
1
03/19/20 11:32
03/19/20 14:15
108-05-4
Vinyl chloride
ND
ug/kg
13.0
1
03/19/20 11:32
03/19/20 14:15
75-01-4
Xylene (Total)
ND
ug/kg
13.0
1
03/19/20 11:32
03/19/20 14:15
1330-20-7
m&p-Xylene
ND
ug/kg
13.0
1
03/19/20 11:32
03/19/20 14:15
179601-23-1
o-Xylene
ND
ug/kg
6.5
1
03/19/20 11:32
03/19/20 14:15
95-47-6
Surrogates
Toluene-d8 (S)
102
%
70-130
1
03/19/20 11:32
03/19/20 14:15
2037-26-5 u8
4-Bromofluorobenzene (S)
95
%
70-130
1
03/19/20 11:32
03/19/20 14:15
460-00-4
1,2-Dichloroethane-d4 (S)
88
%
70-132
1
03/19/20 11:32
03/19/20 14:15
17060-07-0
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
23.1
%
0A0
1
03/16/20 16:40
Total Solids 2540 G-2011
Analytical Method: SM 254OG Preparation Method: SM 2540 G
Total Solids
77.4
%
1
03/24/20 22:51
03/24/20 23:03
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,
except in full,
Date: 03/26/2020 01:45 PM
without the written consent of Pace Analytical Services, LLC.
Page 28 of 59

aceAnalyfical
t www.pacelabs.com
1
ANALYTICAL RESULTS
Project'. 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-5 (V) Lab lD: 92469653005 Collected: 03/13/20 10:10 Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Soil Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)
ND
mg/kg
11.7
1
03/19/20 17:33
03/23/20 11:56
N2
Aliphatic (C19-C36)
ND
mg/kg
11.7
1
03/19/20 17:33
03/23/20 11:56
N2
Aromatic (C11-C22)
ND
mg/kg
11.7
1
03/19/20 17:33
03/23/20 11:56
N2
Surrogates
Nonatriacontane (S)
71
%
40-140
1
03/19/20 17:33
03/23/20 11:56
7194-86-7
o-Terphenyl (S)
90
%
40-140
1
03/19/20 17:33
03/23/20 11:56
84-15-1
2-Fluorobiphenyl (S)
121
%
40-140
1
03/19/20 17:33
03/23/20 11:56
321-60-8
2-Bromonaphthalene (S)
121
%
40-140
1
03/19/20 17:33
03/23/20 11:56
580-13-2
MADEPV Analytical Method: MADEP VPH Preparation Method: MADEPV
Aliphatic (C05-008)
ND
mg/kg
6.16
1
03/13/20 10:10
03126/20 00:31
Aliphatic (C09-C12)
ND
mg/kg
6.16
1
03/13/20 10:10
03/26/20 00:31
Aromatic(C09-C10),Unadjusted
ND
mg/kg
6.16
1
03/13/20 10:10
03/2612000:31
Total VPH
ND
mg/kg
6.16
1
03/13/20 10:10
03/26/20 00:31
Surrogates
2,5-Dibromotoluene (FID)
83.2
%
70-130
1
03/13/20 10:10
03/26/20 00:31
2,5-Dibromotoluene (PID)
80.9
%
70-130
1
03/13/20 10:10
03/26/20 00:31
8270E MSSV Microwave
Analytical Method: EPA 8270E
Preparation Method: EPA 3546
Acenaphthene
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
83-32-9
Acenaphthylene
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
208-96-8
Aniline
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
62-53-3
Anthracene
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
120-12-7
Benzo(a)anthracene
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
56-55-3
Benzo(a)pyrene
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
385
1
03/19/20 12:55
03/2012016:07
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
385
1
03/1912012:55
03/2012016:07
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
207-08-9
Benzoic Acid
ND
ug/kg
1930
1
03/1912012:55
03/20/20 16:07
65-85-0
Benzyl alcohol
ND
ug/kg
771
1
03/19/20 12:55
03/20/20 16:07
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
101-55-3
Butylbenzylphthalate
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
85-68-7
4-Chloro-3-methylphenol
ND
ug/kg
771
1
03/19/20 12:55
03/20/20 16:07
59-50-7
4-Chloroaniline
ND
ug/kg
771
1
03/19/20 12:55
03/20/20 16:07
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
111-44-4
2-Chloronaphthalene
ND
ug/kg
385
1
03/1912012:55
03/20/20 16:07
91-58-7
2-Chlorophenol
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
385
1
03119/20 12:55
03/20/20 16:07
7005-72-3
Chrysene
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
53-70-3
Dibenzofuran
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
385
1
03/19/20 12:55
03120/2016:07
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
385
1
03/19/20 12:55
03120/2016:07
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
771
1
03119/2012:55
03/20/20 16:07
91-94-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 59

aceAnalytical
www.pacelab3.com
ANALYTICAL RESULTS
Project: 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-5 (1') Lab ID: 92469653005 Collected: 03/13/20 10:10 Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E
Preparation Method: EPA 3546
2,4-Dichlorophenol
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
120-83-2
Diethylphthalate
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
84-66-2
2,4-Dimethylphenol
ND
ug/kg
385
1
03/1912012:55
03/20/20 16:07
105-67-9
Dimethylphthalate
ND
ug/kg
385
1
03/1912012.55
03/20/20 16:07
131-11-3
Di-n-butylphthalate
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/kg
771
1
03/19/20 12:55
03/20/20 16:07
534-52-1
2,4-Dinitrophenol
ND
ug/kg
1930
1
03/19/20 12:55
03/20/20 16:07
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
385
1
03/19/20 12:55
03120/2016:07
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
606-20-2
Di-n-octylphthalate
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
117-84-0
bis(2-Ethylhexyl)phthalate
ND
ug/kg
385
1
03/19/20 12:55
03/2012016:07
117-81-7
Fluoranthene
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
206-44-0
Fluorene
ND
ug/kg
385
1
03/19/20 12:55
03/2012016:07
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
87-68-3
Hexachlorobenzene
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
77-47-4
Hexachloroethane
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
193-39-5
Isophorone
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
78-59-1
1-Methyinaphthalene
ND
ug/kg
385
1
03/19/20 12:55
03120/2016:07
90-12-0
2-Methylnaphthalene
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
91-57-6
2-Methylphenoi(o-Cresol)
ND
ug/kg
385
1
03/19/20 12:55
03120/2016:07
95-48-7
3&4-Methylphenol(m&p Cresol)
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
15831-10-4
Naphthalene
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
91-20-3
2-Nitroaniline
ND
ug/kg
1930
1
03/1912012:55
03/20/20 16:07
88-74-4
3-Nitroaniline
ND
ug/kg
1930
1
03/19/20 12:55
03/20/20 16:07
99-09-2
4-Nitroaniline
ND
ug/kg
771
1
03/19/20 12:55
03120/2016:07
100-01-6
Nitrobenzene
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
98-95-3
2-Nitrophenol
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
88-75-5
4-Nitrophenol
ND
ug/kg
1930
1
03/19/20 12:55
03/20/20 16:07
100-02-7
N-Nitrosodimethylamine
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
621-64-7
N-Nitrosodiphenylamine
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
108-60-1
Pentachlorophenol
ND
ug/kg
771
1
03/19/20 12:55
03/20/20 16:07
87-86-5
Phenanthrene
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
85-01-8
Phenol
ND
ug/kg
385
1
03/19/20 12:55
03/2012016:07
108-95-2
Pyrene
ND
ug/kg
385
1
03/19/20 12:55
'03/20/20 16:07
129-00-0
Pyridine
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
110-86-1
1,2,4-Trichlorobenzene
ND
ug/kg
385
1
03119/2012:55
03/20/20 16:07
120-82-1
2,4,5-Trichlorophenol
ND
ug/kg
385
1
03/1912012:55
03/20/20 16:07
95-95-4
2,4,6-Trichlorophenol
ND
ug/kg
385
1
03/19/20 12:55
03/20/20 16:07
88-06-2
Surrogates
Nitrobenzene-d5 (S)
79
%
23-110
1
03/19/20 12:55
03/20/20 16:07
4165-60-0
2-Fluorobiphenyl (S)
69
%
30-110
1
03/19/20 12:55
03/20/20 16:07
321-60-8
Terphenyl-d14 (S)
65
%
28-110
1
03/19/20 12:55
03/20/20 16:07
1718-51-0
REPORT
OF LABORATORY ANALYSIS
This report shall not be reproduced, except in
full,
Date: 03/26/2020 01:45 PM
without the written
consent of Pace Analytical Services, LLC.
Page 30 of 59

,�aceAnalyticalo
www.pacelabs.com
r
ANALYTICAL RESULTS
Project: 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SB-5 (1') Lab ID: 92469653005 Collected. 03/13/20 10:10 Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Surrogates
Phenol-d6 (S)
50
%
22-110
1
03/19/20 12:55
03/20/20 16:07
13127-88-3
2-Fluorophenol (S)
46
%
13-110
1
03/19/20 12:55
03/20/20 16:07
367-12-4
2,4,6-Tribromophenol (S)
49
%
27-110
1
03/19/20 12:55
03/20/20 16:07
118-79-6
8260D15035AVolatile Organics
Analytical Method: EPA 8260D Preparation Method: EPA5035A
Acetone
124
ug/kg
90.5
1
03/18/20 13:32
03118/2018:31
67-64-1
Benzene
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
71-43-2
Bromobenzene
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
108-86-1
Bromochloromethane
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
74-97-5
Bromodichloromethane
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
75-27-4
Bromoform
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
75-25-2
Bromomethane
ND
ug/kg
9.0
1
03/18/20 13:32
03/18/2018:31
74-83-9 IH,vl
2-Butanone (MEK)
ND
ug/kg
90.5
1
03/18/20 13:32
03/18/20 18:31
78-93-3
n-Butylbenzene
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
104-51-8
sec-Butylbenzene
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
135-98-8
tert-Butylbenzene
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
98-06-6
Carbon tetrachloride
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/20 18:31
56-23-5
Chlorobenzene
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
108-90-7
Chloroethane
ND
ug/kg
9.0
1
03/18/20 13:32
03/18/2018:31
75-00-3 v1
Chloroform
ND
ug/kg
4.5
1
03/1812013:32
03/18/2018:31
67-66-3
Chloromethane
ND
ug/kg
9.0
1
03/18/20 13:32
03/18/2018:31
74-87-3
2-Chlorotoluene
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
95-49-8
4-Chlorotoluene
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
4.5
1
03/18/20 13:32
03118/2018:31
96-12-8
Dibromochioromethane
ND
ug/kg
4;5
1
03/18/20 13:32
03/18/2018:31
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/20 18:31
106-93-4
Dibromomethane
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
74-95-3
1,2-Dichlorobenzene
ND
ug/kg
4.5
1
03/18/20 13:32
03118/2018:31
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
106-46-7
Dichlorodifluoromethane
ND
ug/kg
9.0
1
03/18/20 13:32
03/18/2018:31
75-71-8 v1
1,1-Dichloroethane
ND
ug/kg
4.5
1
03/18/20 13:32
03118/2018:31
75-34-3
1,2-Dichloroethane
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
107-06-2
1,1-Dichloroethane
ND
ug/kg
4,5
1
03/1812013:32
03/18/2018:31
75-35-4
cis- 1,2-Dichloroethene
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
4.5
1
03/18/20 13:32
03118/2018:31
156-60-5
1,2-Dichloropropane
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
78-87-5
1,3-Dichloropropane
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
142-28-9
2,2-Dichloropropane
ND
ug/kg
4.5
1
03/1812013:32
03/18/2018:31
594-20-7
1,1-Dichloropropene
ND
uglkg
4.5
1
03/18/20 13:32
03/18/2018:31
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
4.5
1
03118/2013:32
03/18/2018:31
10061-01-5
trans-1,3-Dichloropropene
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
10061-02-6
Diisopropyl ether
NO
ug/kg
4.5
1
03/18/20 13:32
03/18/20 18:31
108-20-3
Ethylbenzene
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
4.5
1
03/18/20 13:32
03/18/2018:31
87-68-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, I.L.C. Page 31 of 59

aceAnalyfcal
www.pacelabs.com
ANALYTICAL RESULTS
Project: 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
Sample: SB-5 (V) Lab ID: 92469653005 Collected: 03/13/20 10:10 Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D/5035A Volatile Organics
2-Hexanone
Isopropyibenzene (Cumene)
p-isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,11-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3 Trichioropropane
1, 2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Total Solids 2540 G-2011
Total Solids
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
ND
ug/kg
45.2
1
03/18/2013:32
03/18/2018:31
591-78-6
ND
ug/kg
4.5
1
03/18/2013:32
03/18/2018:31
98-82-8
ND
ug/kg
4.5
1
03/18/2013:32
03/18/2018:31
99-87-6
ND
ug/kg
18.1
1
03/18/201332
03118/2018:31
75-09-2
ND
ug/kg
45.2
1
03/18/2013:32
03/18/2018:31
108-10-1
ND
ug/kg
4.5
1
03/18/2013:32
03/18/2018:31
1634-04-4
ND
ug/kg
4.5
1
03/1812013:32
03/18/2018:31
91-20-3
ND
ug/kg
4.5
1
03/18/2013:32
03/18/2018:31
103-65-1
ND
ug/kg
4.5
1
03/18/2013:32
03/18/2018:31
100-42-5
ND
ug/kg
4.5
1
03/18/2013:32
03/1812018:31
630-20-6
ND
ug/kg
4.5
1
03/18/2013:32
03/18/2018:31
79-34-5
ND
ug/kg
4.5
1
03/18/201332
03/18/2018:31
127-18-4
ND
ug/kg
4.5
1
03/18/2013:32
03/18/2018:31
108-88-3
ND
ug/kg
4.5
1
03/18/2013:32
03/18/2018:31
87-61-6
ND
ug/kg
4.5
1
03/18/2013:32
03/18/2018:31
120-82-1
ND
ug/kg
4,5
1
03118/201332
03/18/2018:31
71-55-6
ND
ug/kg
4.5
1
03/18/2013:32
03/18/2018:31
79-00-5
ND
ug/kg
4.5
1
03118/2013:32
03/18/2018:31
79-01-6
ND
ug/kg
4.5
1
03/18/2013:32
03118/2018:31
75-69-4
ND
ug/kg
4.5
1
03/18/2013:32
03/18/2018:31
96-18-4
ND
ug/kg
4.5
1
03/18/2013:32
03118/2018:31
95-63-6
ND
ug/kg
4.5
1
03/18/2013:32
03/18/2018:31
108-67-8
ND
ug/kg
45.2
1
03/18/2013:32
03/18/2018:31
108-05-4
ND
ug/kg
9.0
1
03/18/2013:32
03/18/2018:31
75-01-4
ND
ug/kg
9.0
1
03/18/20 13.32
03/18/20 18 31
1330-20-7
ND
ug/kg
9.0
1
03/18/20 13 32
03/18/20 18:31
179601-23-1
ND
ug/kg
4.5
1
03/18/2013:32
03118/2018:31
95-47-6
101
%
70-130
1
03/18/2013:32
03/18/2018:31
2037-26-5
100
%
70-130
1
03/18/2013:32
03/18/2018:31
460-00-4
103
%
70-132
1
03/18/2013:32
03118/2018:31
17060-07-0
Analytical Method:. ASTM D2974-87
13.5 % 0,10 1 03116/2016:40
Analytical Method: SM 254OG Preparation Method: SM 2540 G
81.2 %
1 03/24/20 22:51 03/24/20 23:03
REPORT OF LABORATORY ANALYSIS
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Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, I.I.C. Page 32 of 59

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ANALYTICAL RESULTS
Project: 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Sample: SB-6 (5') Lab ID: 92469653006 Collected: 03/13/20 11:00 Received: 03/16/20 09:01 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
8015 GCS THC-Diesel Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Diesel Range Organics(C10-C28) ND mg/kg 6.1 1 03/19/20 08:13 03/20/20 00:47
Surrogates
n-Pentacosane (S) 72 % 33-129 1 03/19/20 08:13 03/20/20 00:47 629-99-2
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 18.8 % 0.10 1 03/16/20 16:40
REPORT OF LABORATORY ANALYSIS
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Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: 842 UST
Pace Project No.: 92469653
QC Batch: 1449842 Analysis Method: MADEP VPH
QC Batch Method: MADEPV Analysis Description: MADEPV
Associated Lab Samples: 92469653001, 92469653002; 92469653003, 92469653004, 92469653005
METHOD BLANK: R3512680-2
Matrix: Solid
Associated Lab Samples: 92469653001, 92469653002, 92469653003, 92469653004, 92469653005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aliphatic (C05-008)
mg/kg
ND
5.00
03/25/20 12:51
Aliphatic (C09-C12)
mglkg
ND
5.00
03/25/20 12:51
Aromatic (C09-C1 0), Unadjusted
mg/kg
ND
5.00
03/2512012:51
Total VPH
mg/kg
ND
5.00
03/25/20 12:51
2,5-Dibromotoluene (FID)
%
98.4
70-130
03/25/20 12:51
2,5-Dibromotoluene (PID)
%
96.2
70-130
03/25/20 12:51
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
LABORATORY CONTROL SAMPLE & LCSD: R3512680-1
R3512680-5
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
Aliphatic (C05-008)
mg/kg 60
70.3
69.9
117
117
70-130
0.571
25
Aliphatic (C09-C12)
mg/kg 70
76.2
76.8
109
110
70-130
0.784
25
Aromatic (C09-C10),Unadjusted
mg/kg 10
10.5
10.4
105
104
70-130
0,957
25
Total VPH
mg/kg 140
157
157
112
112
70-130
0
25
2,5-Dibromotoluene (FID)
%
103
85.6
70-130
25-Dibromotoluene (PID)
%
103
84.2
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
R3512680-3
R3512680-4
MS
MSD
92469653005
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc,
Result
Result
% Rec
% Rec
Limits
RPD Qual
Aliphatic (C05-008)
mg/kg
ND
66.5
66.5
78.6
77.6
118
117
70-130
1.26
Aliphatic (C09-C12)
mg/kg
ND
77.6
77.6
84.4
88.9
109
115
70-130
5.26
Aromatic (C09-
mg/kg
2.29
11.1
11.1
11.8
12.3
85.7
90.4
70-130
4.39
C10),Unadjusted
Total VPH
mg/kg
2.29
155
155
175
179
111
114
70-130
2.09
2;5-Dibromotoluene (FID)
%
0.0832
86.8
90.2
70-130
2,5-Dibromotoluene (PID)
%
0.0809
85.9
88.6
70-130
Results presented on this page are in the units Indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC.
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Project: 842 UST
Pace Project No 92469653
QC Batch: 531178
QC Batch Method: EPA 5035A
QUALITY CONTROL DATA
Analysis Method: EPA 8260D
Analysis Description: 8260D MSV 5035AVolatile Organics
Associated Lab Samples: 92469653001, 92469653002, 92469653003, 92469653005
METHOD BLANK: 2836092
Associated Lab Samples:
Parameter
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2, 3-Trichooropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Di bromo-3-chloropropan
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-BUtanone;(MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIB
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1;2-Dichloroethene
cis-1, 3-Dichloropropene
Dibromochloromethane
Matrix: Solid
92469653001,92469653002,92469653003,92469653005
Blank
Reporting
Units
Result
Limit
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
e ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
100
ug/kg
ND
5.0
ug/kg
ND
50.0
ug/kg
ND
5.0
K) ug/kg
ND
50.0
ug/kg
ND
100
ug/kg
ND
5.0
ug/kg
NO
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
10.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
10.0
ug/kg
ND
5.0
ug/kg
ND
10.0
ug/kg
ND
5.0
ug/kg
ND
5.0
ug/kg
ND
5.0
Analyzed
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
03/18/20 13:51
Qualifiers
IH,v1
v1
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC28078
[phone]
Resultspresented on this page arein the units Indicated. by the "Units" column exceptwhere an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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1
QUALITY CONTROL DATA
Project: 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersviile, NC 28078
[phone]
METHOD BLANK: 2836092
Matrix: Solid
Associated Lab Samples: 92469653001, 92469653002, 92469653003, 92469653005
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Dibromomethane
ug/kg
ND
5.0
03/18/20 13:51
Dichlorodifluoromethane
ug/kg
ND
10.0
03/18/20 13:51
v1
Diisopropyl ether
ug/kg
ND
5.0
03/18/20 13:51
Ethyibenzene
ug/kg
ND
5.0
03/18/20 13:51
Hexachioro-1,3-butadiene
ug/kg
ND
5.0
03/18/20 13:51
Isopropyl benzene (Cumene)
ug/kg
ND
5.0
03/18/20 13:51
m&p-Xylene
ug/kg
ND
10.0
03/18/20 13:51
Methyl-tert-butyl ether
ug/kg
ND
5.0
03/18/20 13:51
Methylene Chloride
ug/kg
ND
20.0
03/18/20 13:51
n-Butylbenzene
ug/kg
ND
5,0
03/18/20 13:51
n-Propylbenzene
Ug/kg
ND
5.0
03/18/20 13:51
Naphthalene
ug/kg
ND
5.0
03/18/20 13:51
o-Xylene
ug/kg
ND
5.0
03/1812013:51
p-Isopropyltoluene
ug/kg
ND
5.0
03/18/20 13:51
sec-Butylbenzene
ug/kg
ND
5.0
03/18/20 13:51
Styrene
ug/kg
ND
5.0
03/18/20 13:51
tert-Butylbenzene
ug/kg
ND
5.0
03/18/20 13:51
Tetrachloroethene
ug/kg
ND
5.0
03/18/20 13:51
Toluene
ug/kg
ND
5.0
03/18/20 13:51
trans-1,2-Dichloroethene
ug/kg
ND
5.0
03/18/20 13:51
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
03/18/20 13:51
Trichloroethene
ug/kg
ND
5.0
03/18/20 13:51
Trichlorofluoromethane
ug/kg
ND
5.0
03/18/20 13:51
Vinyl acetate
ug/kg
ND
50.0
03/18/20 13:51
Vinyl chloride
ug/kg
ND
10.0
03/18/20 13:51
Xylene (Total)
ug/kg
ND
10.0
03/18/20 13:51
1,2-Dichloroethane-d4 (S)
%
103
70-132
03/18/20 13:51
4-Bromofluorobenzene (S)
%
100
70-130
03/18/20 13:51
Toluene-d8 (S)
%
104
70-130
03/18/20 13:51
LABORATORY CONTROL SAMPLE & LCSD: 2836093
2836094
Spike
LCS
LCSD
LCS LCSD
% Rec
Parameter
Units
Conc.
Result
Result
% Rec % Rec
Limits RPD
1,1,1,2-Tetrachloroethane
ug/kg
50
52A
51.4
104 103
70-130
1,1,1-Trichloroethane
ug/kg
50
52.1
52.2
104 104
70-130
1,1,2,2-Tetrachloroethane
ug/kg
50
49A
49.0
99 98
55-130
1,1,2-Trichloroethane
ug/kg
50
50.6
50.3
101 101
70-130
1,1-Dichloroethane
ug/kg
50
52.8
53.6
1.06 107
68-130
1,1-Dichloroethene
ug/kg
50
571
57,0
114 114
70-130
1,1-Dichloropropene
ug/kg
50
56.6
55,6
113 111
70-130
1,2,3-Trichlorobenzene
ug/kg
50
49.8
49.4
100 99
70-130
1,2,3-Trichloropropane
ug/kg
50
48.4
49.8
97 100
70-130
1,2,4-Trichlorobenzene
ug/kg
50
51.6
50.3
103 101
70-130
1,2,4-Trimethylbenzene
ug/kg
50
51,5
50.5
103 101
69-130
Max
RPD
1 30
0 30
1 30
1 30
2 30
0 30
2 30
1 30
3 30
3 30
2 30
Results presented on thispage. are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC,
Qualifiers
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QUALITY CONTROL DATA
Project: 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 KlnceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
2836093
Units
Spike
Conc,
2836094
LCS LCSD
Result Result
LCS
% Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD Qualifiers
1,2-Dibromo-3-chloropropane
ug/kg
50
50.5
52.5
101
105
57-141
4
30
1,2-Dibromoethane (EDB)
ug/kg
50
53.9
53.2
108
106
70-130
1
30
1,2-Dichlorobenzene
ug/kg
50
50.4
50.6
101
101
70-130
1
30
1,2-Dichloroethane
ug/kg
50
51.0
51.9
102
104
70-130
2
30
1,2-Dichloropropane
ug/kg
50
52.3
51.6
105
103
70-130
1
30
1,3,5-Trimethylbenzene
ug/kg
50
51.8
51.6
104
103
70-130
0
30
1,3-Dichlorobenzene
ug/kg
50
51.0
51A
102
102
70-130
0
30
1,3-Dichloropropane
ug/kg
50
52.2
51.3
104
103
70-130
2
30
1,4-Dichlorobenzene
ug/kg
50
49.5
49A
99
99
70-130
0
30
2,2-Dichloropropane
ug/kg
50
55.2
53.8
110
108
70-130
3
30
2-Butanone (MEK)
ug/kg
100
97J
96.9J
97
97
60-130
30
2-Chlorotoluene
ug/kg
50
50.3
50.8
101
102
70-130
1
30
2-Hexanone
ug/kg
100
99.0
96.8
99
97
70-132
2
30
4-Chlorotoluene
ug/kg
50
51.3
50.5
103
101
70-130
2
30
4-Methyl-2-pentanone (MIBK)
ug/kg
100
95.0
95.4
95
95
69-130
0
30
Acetone
ug/kg
100
103
106
103
106
49-148
3
30
Benzene
ug/kg
50
55.9
54.8
112
110
70-130
2
30
Bromobenzene
ug/kg
50
50.0
51.1
100
102
70-130
2
30
Bromochloromethane
ug/kg
50
53.1
52.4
106
105
70-130
1
30
Bromodichloromethane
ug/kg
50
52.6
51,9
105
104
70-130
1
30
Bromoform
ug/kg
50
51.0
51.4
102
103
68-136
1
30
Bromomethane
ug/kg
50
72.9
75.5
146
151
60-140
3
301H,L1,vl
Carbon tetrachloride
ug/kg
50
56.4
54.7
113
109
70-130
3
30
Chlorobenzene
ug/kg
50
51.6
50.7
103
101
70-130
2
30
Chloroethane
ug/kg
50
56:9
58.2
114
116
51-147
2
30 v1
Chloroform
ug/kg
50
51.6
50.5
103
101
70-130
2
30
Chloromethane
ug/kg
50
47.4
47.1
95
94
48-130
1
30
cis-1,2-Dichloroethene
ug/kg
50
53.3
52.8
107
106
70-130
1
30
cis-1,3-Dichloropropene
ug/kg
50
52.1
51.6
104
103
70-130
1
30
Dibromochloromethane
ug/kg
50
52.7
51.1
105
102
70.130
3
30
Dibromomethane
ug/kg
50
52.5
52A
105
105
70-130
0
30
Dichlorodifluoromethane
ug/kg
50
56.7
55.5
113
111
49-130
2
30 v1
Diisopropyl ether
ug/kg
50
53.5
53.5
107
107
66-130
0
30
Ethylbenzene
ug/kg
50
50.0
48.4
100
97
70-130
3
30
Hexachloro-1,3-butadiene
ug/kg
50
52.4
51.7
105
103
70-130
1
30
Isopropyl benzene (Cumene)
ug/kg
50
52.0
50.0
104
100
70-130
4
30
m&p-Xylene
ug/kg
100
101
97.2
101
97
70-130
4
30
Methyl-tert-butyl ether
ug/kg
50
53.7
55.9
107
112
70-130
4
30
Methylene Chloride
uglkg
50
53.8
54.1
108
108
50-137
0
30
n-Butylbenzene
ug/kg
50
52.0
50A
104
101
70-130
3
30
n-Propylbenzene
ug/kg
50
49.4
48.2
99
96
70-130
3
30
Naphthalene
ug/kg
50
50.6
50.6
101
101
70-131
0
30
o-Xylene
ug/kg
50
51.2
49.5
102
99
70-130
3
30
p-lsopropyltoluene
ug/kg
50
52.1
50.5
104
101
70-130
3
30
sec-Butylbenzene
ug/kg
50
50A
48.8
100
98
70-130
3
30
Styrene
ug/kg
50
53.0
51.7
106
103
70-130
2
30
tert-Butylbenzene
ug/kg
50
43.5
43.6
87
87
69-130
0
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 59

,1��aceAnalXical
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I
QUALITY CONTROL DATA
Project: 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE & LCSD: 2836093
Parameter Units
Spike
Conc.
2836094
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec
Limits
RPD
Max
RPD Qualifiers
Tetrachloroethene
ug/kg
50
54.5
51.8
109
104
56-130
5
30
Toluene
ug/kg
50
50.0
49.9
100
100
70-130
0
30
trans-1,2-Dichloroethene
ug/kg
50
57.5
57.8
115
116
70-130
1
30
trans-1,3-Dichloropropene
ug/kg
50
51.4
51.7
103
103
70-130
1
30
Trichloroethene
ug/kg
50
55.3
53.9
111
108
70-141
3
30
Trichlorofluoromethane
ug/kg
50
53.0
52.8
106
106
67-130
0
30
Vinyl acetate
ug/kg
100
116
112
116
112
10-136
4
30
Vinyl chloride
ug/kg
50
59.3
60.7
119
121
67-130
2
30
Xylene (Total)
ug/kg
150
153
147
102
98
70-130
4
30
1,2-Dichloroethane-d4 (S)
%
96
96
70-132
4-Bromofluorobenzene (S)
%
103
100
70-130
Toluene-d8 (S)
%
99
99
70-130
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC.
Page 38 of 59

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QUALITY CONTROL DATA
Project: 842 UST
Pace Project No.: 92469653
QC Batch: 531399
QC Batch Method: EPA5035A
Associated Lab Samples: 92469653004
Analysis Method:
Analysis Description:
EPA 8260D
8260D MSV 5035AVolatile Organics
METHOD BLANK: 2837162
Matrix: Solid
Associated Lab Samples: 92469653004
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
03/19/20 10:38
1,1,1-Trichloroethane
ug/kg
ND
5.0
03/19/20 10:38
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
03/19/20 10:38
1,1,2-Trichloroethane
ug/kg
NO
5.0
03/19/20 10:38
1,1-Dichloroethane
ug/kg
ND
5.0
03/19/20 10:38
1,1-Dichloroethene
ug/kg
ND
5.0
03/19/20 10:38
1,1-Dichloropropene
ug/kg
ND
5.0
03/19/20 10:38
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
03119/2010:38
1,2,3-Ticchloropropane
ug/kg
ND
5.0
03/19/20 10:38
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
03/19/20 10:38
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
03/19/20 10:38
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
03/19/20 10:38
1,2-Dibromoethane (EDB)
ug/kg
NO
5.0
03/19/20 10:38
1,2-Dichlorobenzene
ug/kg
ND
5.0
03/19/20 10:38
1,2-Dichloroethane
ug/kg
ND
5.0
03/19/20 10:38
1,2-Dichloropropane
ug/kg
ND
5.0
03/19/20 10:38
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
03/19/20 10:38
1,3-Dichlorobenzene
ug/kg
ND
5.0
03/19/20 10:38
1,3-Dichloropropane
ug/kg
ND
5.0
03/19/20 10:38
1,4-Dichlorobenzene
ug/kg
ND
5.0
03/19/20 10:38
2,2-Dichloropropane
ug/kg
ND
5.0
03119/2010:38
2-Butanone (MEK)
uglkg
ND
100
03/19/20 10:38
2-Chlorotoluene
ug/kg
ND
5.0
03/19/20 10:38
2-Hexanone
ug/kg
ND
50.0
03/19/20 10:38
4-Chlorotoluene
ug/kg
ND
5.0
03119/2010:38
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
03/19/20 10:38
Acetone
ug/kg
ND
100
03/19/20 10:38
Benzene
ug/kg
ND
5.0
03/19/20 10:38
Bromobenzene
ug/kg
ND
5.0
03/19/20 10:38
Bromochloromethane
ug/kg
ND
5.0
03/19/20 10:38
Bromodichloromethane
ug/kg
ND
5.0
03/19/20 10:38
Bromoform
ug/kg
ND
5.0
03/19/20 10:38
Bromomethane
ug/kg
NO
10.0
03/19/20 10:38 IH,v1
Carbon tetrachloride
ug/kg
ND
5.0
03119/2010:38
Chlorobenzene
ug/kg
ND
5.0
03/19/20 10:38
Chloroethane
ug/kg
ND
10.0
03/19/20 10:38
Chloroform
ug/kg
ND
5.0
03/19/20 10:38
Chloromethane
ug/kg
ND
10.0
03/1912010:38
cis-1,2-Dichloroethene
ug/kg
ND
5.0
03/1912010:38
cis-1,3-Dichloropropene
ug/kg
ND
5.0
03/19/20 10:38
Dibromochloromethane
ug/kg
ND
5.0
03/19/20 10:38
Pace, Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 59

acmnalytical
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QUALITY CONTROL DATA
Project: 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 2837162
Matrix: Solid
Associated Lab Samples: 92469653004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Dibromomethane
ug/kg
ND
5:0
03/19/20 10:38
Dichlorodifluoromethane
ug/kg
ND
10.0
03/19/20 10:38
Diisopropyl ether
ug/kg
ND
5.0
03/19/20 10:38
Ethylbenzene
ug/kg
ND
5.0
03119/2010:38
Hexachloro-1,3-butadiene
ug/kg
ND
5.0
03/19/20 10:38
isopropylbenzene (Cumene)
ug/kg
ND
5.0
03/19/20 10:38
m&p-Xylene
ug/kg
ND
10.0
03/19/20 10:38
Methyl-tert-butyl ether
ug/kg
ND
5.0
03/19/20 10:38
Methylene Chloride
ug/kg
ND
20.0
03/19/20 10:38
n-Butylbenzene
ug/kg
ND
5,0
03/19/20 10:38
n-Propylbenzene
ug/kg
ND
5.0
03/19/20 10:38
Naphthalene
ug/kg
ND
5.0
03/19/20 10:38
o-Xylene
ug/kg
ND
5.0
03/19/20 10:38
p-Isopropyltoluene
ug/kg
ND
5.0
03/19/20 10:38
sec -Butyl benzene
uglkg
ND
5.0
03/19/20 10:38
Styrene
ug/kg
ND
5.0
03119/2010:38
tert-Butyl benzene
ug/kg
NO
5.0
03/19/20 10:38
Tetrachloroethene
ug/kg
ND
5.0
03/1912010:38
Toluene
ug/kg
ND
5.0
03/19/20 10:38
trans- 1,2-Dichloroethene
ug/kg
ND
5.0
03/19/20 10:38
trans-1,3-Dichloropropene
ug/kg
ND
5.0
03/19/2010.38
Trichloroethene
ug/kg
NO
5.0
03/19/20 10:38
Trichlorofluoromethane
ug/kg
ND
5.0
03/19/20 10:38
Vinyl acetate
ug/kg
ND
50.0
03/19/20 10:38
Vinyl chloride
ug/kg
ND
10.0
03/19/20 10:38
Xylene (Total)
ug/kg
ND
10.0
03/19/20 10:38
1,2-Dichloroethane-d4 (S)
%
85
70-132
03/19/20 10:38
4-Bromofluorobenzene (S)
%
94
70-130
03/19/20 10:38
Toluene-d8 (S)
%
102
70-130
03/19/20 10:38
LABORATORY CONTROL SAMPLE; 2837163
Spike
LCS
LCS %
Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
50
51A
103
70-130
1,1,1-Trichloroethane
ug/kg
50
417
87
70-130
1,1,2,2-Tetrachloroethane
ug/kg
50
46.9
94
55-130
1,1,2-Trichloroethane
ug/kg
50
45.5
91
70-130
1,1-Dichloroethane
ug/kg
50
44.6
89
68-130
1,1-Dichloroethene
ug/kg
50
46.6
93
70-130
1,1-Dichloropropene
ug/kg
50
48.7
97
70-130
1,2,3-Trichlorobenzene
ug/kg
50
55.8
112
70-130
1,2,3-Trichloropropane
ug/kg
50
47.6
95
70-130
1,2,4-Trichlorobenzene
ug/kg
50
55.6
ill
70-130
1,2,4-Trimethylbenzene
ug/kg
50
54.3
109
69-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03126/2020 01:45 PM without the written consent of Pace Analytical Services, LLC.
Page 40 of 59

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Project: 842 UST
Pace Project No.: 92469653
LABORATORY CONTROL SAMPLE: 2837163
Parameter
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
1,2-Dibromo-3-chloropropane
ug/kg
50
51.8
104
57-141
1,2-Dibromoethane (EDB)
ug/kg
50
50.4
101
70-130
1,2-Dichlorobenzene
ug/kg
50
53.3
107
70-130
1,2-Dichloroethane
ug/kg
50
41.1
82
70-130
1,2-Dichloropropane
ug/kg
50
49.3
99
70-130
1,3,5-Trimethylbenzene
ug/kg
50
55.0
110
70-130
1,3-Dichlorobenzene
ug/kg
50
54.5
109
70-130
1,3-Dichloropropane
ug/kg
50
49.3
99
70-130
1,4-Dichlorobenzene
ug/kg
50
53.2
106
70-130
2,2-Dichloropropane
ug/kg
50
45.1
90
70-130
2-Butanone (MEK)
ug/kg
100
110
110
60-130
2-Chlorotoluene
ug/kg
50
54.3
109
70-130
2-Hexanone
ug/kg
100
105
105
70-132
4-Chlorotoluene
ug/kg
50
53.6
107
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
100
89.8
90
69-130
Acetone
ug/kg
100
111
111
49-148
Benzene
ug/kg
50
49.1
98
70-130
Bromobenzene
ug/kg
50
52.8
106
70-130
Bromochloromethane
ug/kg
50
43.9
88
70-130
Bromodichloromethane
ug/kg
50
46.9
94
70-130
Bromoform
ug/kg
50
48.8
98
68-136
Bromomethane
ug/kg
50
63.0
126
60-1401H,vl
Carbon tetrachloride
ug/kg
50
46.8
94
70-130
Chlorobenzene
ug/kg
50
52.1
104
70-130
Chloroethane
ug/kg
50
49.1
98
51-147
Chloroform
ug/kg
50
46.1
92
70-130
Chloromethane
ug/kg
50
40.5
81
48-130
cis-1,2-Dichloroethene
ug/kg
50
45.0
90
70-130
cis-1,3-Dichloropropene
ug/kg
50
46.1
92
70-130
Dibromochloromethane
ug/kg
50
50.2
100
70-130
Dibromomethane
ug/kg
50
45.3
91
70-130
Dichlorodifluoromethane
ug/kg
50
45.5
91
49-130
Diisopropyl ether
ug/kg
50
45.2
90
66-130
Ethylbenzene
ug/kg
50
50.6
101
70-130
Hexachloro-1,3-butadiene
ug/kg
50
58.2
116
70-130
Isopropylbenzene (Cumene)
ug/kg
50
52.3
105
70-130
m&p-Xylene
uglkg
100
101
101
70-130
Methyl-tert-butyl ether
ug/kg
50
42.8
86
70-130
Methylene Chloride
ug/kg
50
44.8
90
50-137
n-Butylbenzene
ug/kg
50
56.5
113
70-130
n-Propylbenzene
ug/kg
50
53.3
107
70-130
Naphthalene
ug/kg
50
54.0
108
70-131
o-Xytene
ug/kg
50
50.7
101
70-130
p-Isopropyltoluene
ug/kg
50
56.2
112
70-130
sec-Butylbenzene
ug/kg
50
54.8
110
70-130
Styrene
ug/kg
50
52.9
106
70-130
tert-Butyl benzene
ug/kg
50
47.3
95
69-130
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC.
Page 41 of 59

acmnalytical o
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r
t
QUALITY CONTROL DATA
Project: 842 LIST
Pace Project No.: 92469653
LABORATORY CONTROL SAMPLE: 2837163
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Tetrachloroethene
ug/kg
50
51.3
103
56-130
Toluene
ug/kg
50
45.8
92
70-130
trans-1,2-Dichloroethene
ug/kg
50
46.7
93
70-130
trans-1,3-Dichloropropene
ug/kg
50
44.7
89
70-130
Trichloroethene
ug/kg
50
50.6
101
70-141
Trichlorofluoromethane
ug/kg
50
46.1
92
67-130
Vinyl acetate
ug/kg
100
94.3
94
10-136
Vinyl chloride
ug/kg
50
501
100
67-130
Xylene (Total)
ug/kg
150
152
101
70-130
1,2-Dichloroethane-d4 (S)
%
93
70-132
4-Bromofluorobenzene (S)
%
95
70-130
Toluene-d8 (S)
%
98
70-130
MATRIX SPIKE &MATRIX SPIKE DUPLICATE: 2837957
2837958
MS
MSD
92470071002
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD Qual
1,1,1,2-Tetrachloroethane
ug/kg
ND
60800
60800
56100
57900
92
95
52-133
3
1,1,1-Trichloroethane
ug/kg
ND
60800
60800
47800
49000
78
80
49-137
3
1,1,2,2-Tetrachloroethane
ug/kg
ND
60800
60800
53900
56100
89
92
39-150
4
1,1,2-Trichloroethane
ug/kg
ND
60800
60800
52700
54500
87
89
48-140
3
1,1-Dichloroethane
ug/kg
ND
60800
60800
49300
51000
81
84
46-135
3
1,1-Dichloroethene
ug/kg
ND
60800
60800
50300
52500
83
86
38-149
4
1,1-Dichloropropene
ug/kg
ND
60800
60800
52300
53500
86
88
41-140
2
1,2,3-Trichlorobenzene
ug/kg
ND
60800
60800
62400
61800
103
101
10-158
1
1,2,3-Trichloropropane
ug/kg
ND
60800
60800
49100
53500
81
88
33-157
8
1,2,4-Trichlorobenzene
ug/kg
ND
60800
60800
60600
61200
100
100
10-155
1
1,2,4-Trimethylbenzene
ug/kg
506
60800
60800
551000
515000
74
15
24-154
7 M1
mglkg
1,2-Dibromo-3-chloropropane
ug/kg
ND
60800
60800
53900
59600
88
98
33-158
10
1,2-Dibromoethane (EDB)
ug/kg
ND
60800
60800
56300
57800
92
95
40-136
3
1,2-Dichlorobenzene
ug/kg
ND
60800
60800
59500
59700
98
98
27-146
0
1,2-Dichloroethane
ug/kg
ND
60800
60800
45900
48500
75
80
49-140
6
1,2-Dichloropropane
ug/kg
ND
60800
60800
54000
56000
89
92
44.143
4
1,3,5-Trimethylbenzene
ug/kg
151
60800
60800
211000
198000
97
76
40-144
6
mg/kg
1,3-Dichlorobenzene
ug/kg
ND
60800
60800
59900
59800
98
98
33-140
0
1,3-Dichloropropane
ug/kg
ND
60800
60800
55400
57000
91
94
47-147
3
1,4-Dichlorobenzene
ug/kg
ND
60800
60800
60300
60500
99
99
35-139
0
2,2-Dichloropropane
ug/kg
ND
60800
60800
49600
50600
81
83
41-140
2
2-Butanone(MEK)
ug/kg
ND
122000
122000
169000J
174000J
139
143
10-181
2-Chlorotoluene
ug/kg
ND
60800
60800
64500
70000
106
115
38-147
8
2-Hexanone
ug/kg
ND
122000
122000
117000J
116000J
96
95
18-169
4-Chlorotoluene
ug/kg
ND
60800
60800
61600
58600
101
96
36-145
5
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
122000
122000
136000J
141000J
82
86
16-175
Acetone
ug/kg
ND
122000
122000
146000J
150000J
120
123
10-200
Results presented on this page are In the. units. indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC, Page 42 of 59

�Xcmnalytical'
www.pacelabs.com
QUALITY CONTROL DATA
Project: 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE
Parameter
DUPLICATE: 2837957
MS
92470071002 Spike
Units Result Conc.
MSD
Spike
Conc.
2837958
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Benzene
ug/kg
34.2
60800
60800
89300
89200
91
90
46-136
0
mg/kg
Bromobenzene
ug/kg
ND
60800
60800
59000
59100
97
97
38-149
0
Bromochloromethane
ug/kg
ND
60800
60800
50800
53400
83
88
44-142
5
Bromodichloromethane
ug/kg
ND
60800
60800
52400
54700
86
90
41-140
4
Bromoform
ug/kg
ND
60800
60800
53700
54900
88
90
34-145
2
Bromomethane
ug/kg
ND
60800
60800
72600
64400
119
106
14-162
121H,v1
Carbon tetrachloride
ug/kg
ND
60800
60800
49400
52300
81
86
44-141
6
Chlorobenzene
ug/kg
ND
60800
60800
57700
58800
95
97
39-141
2
Chloroethane
ug/kg
ND
60800
60800
58000
59500
95
98
10-182
3
Chloroform
ug/kg
ND
60800
60800
52200
52900
86
87
45-140
1
Chloromethane
ug/kg
ND
60800
60800
44700
46300
73
76
19-149
3
cis-1,2-Dichioroethene
ug/kg
ND
60800
60800
49200
50500
81
83
38-150
3
cis-1,3-Dichloropropene
ug/kg
ND
60800
60800
51700
52700
85
87
30-144
2
Dibromochloromethane
ug/kg
ND
60800
60800
53200
55300
87
91
36-145
4
Dibromomethane
ug/kg
ND
60800
60800
50700
51600
83
85
41-145
2
Dichlorodifluoromethane
ug/kg
ND
60800
60800
46600
48200
76
79
16-146
4
Diisopropyl ether
ug/kg
ND
60800
60800
51700
53200
85
87
41-143
3
Ethylbenzene
ug/kg
193
60800
60800
250000
239000
94
76
35-144
4
mg/kg
Hexachloro-1,3-butadiene
ug/kg
ND
60800
60800
62300
61700
102
101
10-160
1
Isopropylbenzene (Cumene)
ug/kg
19.8
60800
60800
76600
76600
93
93
30-152
0
mg/kg
m&p-Xylene
ug/kg
728
122000
122000
842000
806000
93
64
33-145
4
mg/kg
Methyl-tert-butyl ether
ug/kg
ND
60800
60800
48000
49900
79
82
49-140
4
Methylene Chloride
ug/kg
ND
60800
60800
78100
80400
128
132
10-174
3
n-Butylbenzene
ug/kg
25.6
60800
60800
87100
84000
101
96
10-160
4
mg/kg
n-Propylbenzene
ug/kg
82.9
60800
60800
139000
134000
93
83
24-159
4
mg/kg
Naphthalene
ug/kg
72.6
60800
60800
123000
123000
83
83
10-171
0
mg/kg
o-Xylene
ug/kg
315
60800
60800
378000
360000
103
74
31-150
5
mg/kg
p-Isopropyltoluene
ug/kg
ND
60800
60800
83300
81200
137
133
21-154
3
sec -Butyl benzene
ug/kg
ND
60800
60800
66500
67100
109
110
19-159
1
Styrene
ug/kg
ND
60800
60800
60800
60400
100
99
15-152
1
tert-Butylbenzene
ug/kg
ND
60800
60800
51500
51800
85
85
31-141
1
Tetrachloroethene
ug/kg
ND
60800
60800
54800
55100
90
91
19-141
1
Toluene
ug/kg
556
60800
60800
614000
591000
94
58
31-146
4 E
mg/kg
trans-1,2-Dichloroethene
ug/kg
ND
60800
60800
50000
49800
82
82
28-157
0
trans-1,3-Dichloropropene
ug/kg
ND
60800
60800
49900
50700
82
83
25-146
2
Trichloroethene
ug/kg
ND
60800
60800
54900
56100
90
92
34-149
2
Trichiorofluoromethane
ug/kg
ND
60800
60800
51100
51000
84
84
10-167
0
Vinyl acetate
ug/kg
ND
122000
122000
103000J
108000J
84
88
10-200
Vinyl chloride
ug/kg
ND
60800
60800
52900
56300
87
92
36-155
6
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC,
Page 43 of 59

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f
QUALITY CONTROL DATA
Project: 842 UST
Pace Project No.: 92469653
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2837957
2837958
MS
MSD
92470071002 Spike
Spike
MS MSD
Parameter
Units
Result Conc,
Conc.
Result Result
Xylene (Total)
ug/kg
1040 182000
182000
1220000 1170000
mg/kg
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MS MSD % Rec
% Rec % Rec Limits RPD
97 67 29-148 4
86 93 70-132
95 95 70-130
97 97 70-130
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, L-C,
Qual
Page 44 of 59

aceAnalXical
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QUALITY CONTROL DATA
Project: 842 UST
Pace Project No.: 92469653
QC Batch: 531340 Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 3546 Analysis Description: 8015 Solid GCSV
Associated Lab Samples: 92469653006
METHOD BLANK: 2836947 Matrix: Solid
Associated Lab Samples: 92469653006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Diesel Range Organics(C10-C28) mg/kg ND 4.9 03/20/20 00:23
n-Pentacosane (S) % 83 33-129 03/20/20 00:23
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersviile, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2836948
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Diesel Range Organics(C10-C28) mg/kg 65.6 53.1 81 43-130
n-Pentacosane(S) % 85 33-129
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2836949
2836950
MS
MSD
92469870001 Spike
Spike
MS
MSD MS MSD % Rec
Parameter Units Result Conc,
Conc.
Result
Result % Rec % Rec Limits RPD Qual
Diesel Range Organics(C10- mg/kg ND 72.3
73.8
32.7
45.5 44 60 10-130 33 R1
C28)
n-Pentacosane(S) %
60 65 33-129
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC.
Page 45 of 59

aceAnalytical
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QUALITY CONTROL DATA
Project,. 842 UST
Pace Project No.: 92469653
QC Batch: 531416 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave
Associated Lab Samples: 92469653001,92469653002,92469653003,92469653004,92469653005
METHOD BLANK: 2837284 Matrix: Solid
Associated Lab Samples: 92469653001, 92469653002, 92469653003, 92469653004, 92469653005
Blank
Reporting
Parameter
Units
Result,
Limit
Analyzed Qualifiers
1,2,4 Trichlorobenzene
ug/kg
ND
325
03/20/20 13;24
1,2-Dichiorobenzene
ug/kg
ND
325
03/20/20 13:24
1,3-Dichlorobenzene
ug/kg
ND
325
03/20/20 13:24
1,4-Dichlorobenzene
ug/kg
NO
325
03/20/20 13:24
1-Methylnaphthalene
ug/kg
ND
325
03/20/20 13:24
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
325
03/2012013:24
2,4,5-Trichlorophenol
ug/kg
ND
325
03/20/20 13:24
2,4,6-Trichlorophenol
ug/kg
ND
325
03/20/20 13:24
2,4-Dichlorophenol
ug/kg
ND
325
03/20/20 13:24
2,4-Dimethylphenol
ug/kg
ND
325
03/20/20 13:24
2,4-Dinitrophenol
ug/kg
ND
1620
03/20/20 13:24
2,4-Dinitrotoluene
ug/kg
ND
325
03/20/20 13:24
2,6-Dinitrotoluene
ug/kg
ND
325
03/20/20 13:24
2-Chloronaphthalene
ug/kg
ND
325
03/20/20 13:24
2-Chlorophenol
ug/kg
NO
325
03/20/20 13:24
2-Methylnaphthalene
ug/kg
ND
325
03/2012013:24
2-Methylphenol(o-Cresol)
ug/kg
ND
325
03/20/20 13:24
2-Nitroaniline
ug/kg
ND
1620
03/20/20 13:24
2-Nitrophenol
ug/kg
NO
325
03/20/20 13:24
3&4-Methylphenol(m&p Cresol)
ug/kg
ND
325
03/20/20 13:24
3,3'-Dichiorobenzidine
ug/kg
ND
649
03/20/20 13:24
3-Nitroaniline
ug/kg
ND
1620
03/2012013:24
4,6-Dinitro-2-methyiphenol
ug/kg
NO
649
03/20/20 13:24
4-Bromophenylphenyl ether
ug/kg
ND
325
03/20/20 13:24
4-Chloro-3-methylphenol
ug/kg
ND
649
03/20/20 13:24
4-Chloroaniline
ug/kg
ND
649
03/20/20 13:24
4-Chlorophenyiphenyl ether
ug/kg
ND
325
03/20/20 13:24
4-Nitroaniline
ug/kg
ND
649
03/20/20 13:24
4-Nitrophenol
ug/kg
ND
1620
03/20/20 13:24
Acenaphthene
ug/kg
NO
325
03/20/20 13:24
Acenaphthylene
ug/kg
ND
325
03/20/20 13:24
Aniline
ug/kg
ND
325
03/20/20 13:24
Anthracene
ug/kg
NO
325
03/20/20 13:24
Benzo(a)anthracene
ug/kg
ND
325
03/20/20 13:24
Benzo(a)pyrene
uglkg
ND
325
03120/2013:24
Benzo(b)fluoranthene
ug/kg
ND
325
03/20/20 13:24
Benzo(g,h,i)perylene
ug/kg
ND
325
03/20/20 13:24
Benzo(k)fluoranthene
ug/kg
ND
325
03/20/20 13:24
Benzoic Acid
ug/kg
ND
1620
03/2012013:24
Benzyl alcohol
ug/kg
ND
649
03/20/20 13:24
bis(2-Chioroethoxy)methane
ug/kg
ND
325
03/20/20 13:24
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 59

aceAnalytical
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QUALITY CONTROL DATA
Project: 842 UST
Pace Project No.: 92469653
METHOD BLANK: 2837284 Matrix: Solid
Associated Lab Samples: 92469653001, 92469653002, 92469653003, 92469653004, 92469653005
Parameter
Units
Blank
Result
Reporting
Limit
Analyzed
bis(2-Chloroethyl) ether
ug/kg
ND
325
03/20/20 13:24
bis(2-Ethylhexyl)phthalate
ug/kg
ND
325
03/20/20 13:24
Butylbenzylphthalate
ug/kg
ND
325
03/20/20 13:24
Chrysene
ug/kg
ND
325
03/20/20 13:24
Di-n-butylphthalate
ug/kg
ND
325
03/20/20 13:24
Di-n-octylphthalate
ug/kg
ND
325
03/20/20 13:24
Dibenz(a,h)anthracene
ug/kg
ND
325
03/20/20 13:24
Dibenzofuran
ug/kg
ND
325
03120/2013:24
Diethylphthalate
ug/kg
ND
325
03120/2013:24
Dimethylphthalate
ug/kg
ND
325
03120/2013:24
Fluoranthene
ug/kg
ND
325
03/20/20 13:24
Fluorene
ug/kg
ND
325
03/20/20 13:24
Hexachloro-1,3-butadiene
ug/kg
ND
325
03/20/20 13:24
Hexachlorobenzene
ug/kg
ND
325
03/20/20 13:24
Hexachlorocyclopentadiene
ug/kg
ND
325
03/20/20 13:24
Hexachloroethane
ug/kg
ND
325
03120/2013:24
Indeno(1,2,3-cd)pyrene
ug/kg
ND
325
03/20/20 13:24
Isophorone
ug/kg
ND
325
03120/2013:24
N-Nitroso-di-n-propylamine
ug/kg
ND
325
03/20/20 13:24
N-Nitrosodimethylamine
ug/kg
ND
325
03/20/20 13:24
N-Nitrosodiphenylamine
ug/kg
ND
325
03/20/20 13:24
Naphthalene
ug/kg
ND
325
03120/2013:24
Nitrobenzene
ug/kg
ND
325
03/20/20 13:24
Pentachlorophenol
ug/kg
ND
649
03/20/20 13:24
Phenanthrene
ug/kg
NO
325
03/20/20 13:24
Phenol
ug/kg
ND
325
03/20/20 13:24
Pyrene
ug/kg
ND
325
03/20/20 13:24
Pyridine
ug/kg
ND
325
03/2012013:24
2,4,6-Tribromophenol (S)
%
87
27-110
03/20/20 13:24
2-Fluorobiphenyl (S)
%
85
30-110
03/20/20 13:24
2-Fluorophenol (S)
%
87
13-110
03/20/20 13:24
Nitrobenzene-d5 (S)
%
89
23-110
03/20/20 13:24
Phenol-d6 (S)
%
82
22-110
03/20/20 13:24
Terphenyl-d14 (S)
%
78
28-110
03/20/20 13:24
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2837285
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichoorobenzene
ug/kg
1660
1650
99
52-130
1,2-Dichlorobenzene
ug/kg
1660
1600
97
51-130
1,3-Dichlorobenzene
ug/kg
1660
1570
95
50-130
1,4-Dichlorobenzene
ug/kg
1660
1640
99
49-130
1-Methylnaphthalene
ug/kg
1660
1720
104
55-130
2,2'-Oxybis(1-chloropropane)
ug/kg
1660
1530
92
30-130
Results presented on this page are In the units Indicated by the"Units" column except where an alternate unit is presented to the right of the result,
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 59

aceAnalytical
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QUALITY CONTROL DATA
Project: 842 UST
Pace Project No.: 92469653
LABORATORY CONTROL SAMPLE: 2837285
Parameter
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,4,5-Trichlorophenol
ug/kg
1660
1770
107
55-130
2,4,6-Trichlorophenol
ug/kg
1660
1790
108
57-130
2,4-Dichlorophenol
ug/kg
1660
1780
107
56-130
2,4-Dimethylphenol
ug/kg
1660
1740
105
51-130
2,4-Dinitrophenol
ug/kg
8280
8200
99
27-133
2,4-Dinitrotoluene
ug/kg
1660
1960
118
61-130
2,6-Dinitrotoluene
ug/kg
1660
1860
113
60-130
2-Chloronaphthalene
ug/kg
1660
1760
106
52-130
2-Chlorophenol
ug/kg
1660
1590
96
54-130
2-Methylnaphthalene
ug/kg
1660
1730
104
54-130
2-Methylphenol(o-Cresol)
ug/kg
1660
1650
100
51-130
2-Nitroaniline
ug/kg
3310
3760
114
51-130
2-Nitrophenol
ug/kg
1660
1680
101
49-130
3&4-Methylphenol(m&p Cresol)
ug/kg
1660
1650
100
11-163
3,3'-Dichlorobenzidine
ug/kg
3310
3120
94
10-132
3-Nitroaniline
ug/kg
3310
3270
99
55-130
4,6-Dinitro-2-methylphenol
ug/kg
3310
3370
102
47-142
4-Bromophenylphenyl ether
ug/kg
1660
1720
104
59-130
4-Chloro-3-methylphenol
ug/kg
3310
3560
108
55-130
4-Chloroaniline
ug/kg
3310
3340
101
54-130
4-Chlorophenylphenyl ether
ug/kg
1660
1770
107
58-130
4-Nitroaniline
ug/kg
3310
3590
109
54-130
4-Nitrophenol
ug/kg
8280
9100
110
48-130
Acenaphthene
ug/kg
1660
1770
107
60-130
Acenaphthylene
ug/kg
1660
1790
108
60-130
Aniline
ug/kg
1660
1470
89
43-130
Anthracene
ug/kg
1660
1790
108
63-130
Benzo(a)anthracene
ug/kg
1660
1760
106
59-130
Benzo(a)pyrene
ug/kg
1660
1820
110
57-130
Benzo(b)fluoranthene
ug/kg
1660
1780
107
54-130
Benzo(g,h,i)perylene
ug/kg
1660
1910
116
59-130
Benzo(k)fluoranthene
ug/kg
1660
1800
109
54-130
Benzoic Acid
ug/kg
8280
5060
61
19-130
Benzy alcohol
ug/kg
3310
3340
101
50-130
bis(2-Chloroethoxy)methane
ug/kg
1660
1650
99
54-130
bis(2-Chloroethyl) ether
ug/kg
1660
1510
91
48-130
bis(2-Ethylhexyl)phthalate
ug/kg
1660
1780
108
45-134
Butylbenzylphthalate
ug/kg
1660
1780
108
46-138
Chrysene
ug/kg
1660
1810
109
58-130
Di-n-butylphthalate
ug/kg
1660
1830
Ill
60-130
Di-n-octyiphthalate
ug/kg
1660
1880
114
53-130
Dibenz(a,h)anthracene
ug/kg
1660
1890
114
59-130
Dibenzofuran
ug/kg
1660
1840
111
60-130
Diethylphthalate
ug/kg
1660
1820
110
60-130
Dimethylphthalate
ug/kg
1660
1830
Ill
60-130
Fluoranthene
ug/kg
1660
1820
110
65-130
Fiuorene
ug/kg
1660
1810
109
63-130
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC28078
[phone]
Qualifiers
Results presented on this. page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 59

aceAnalXical
www.pacelab3.COM
(
QUALITY CONTROL DATA
Project: 842 UST
Pace Project No.: 92469653
LABORATORY CONTROL SAMPLE: 2837285
Pace, Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Hexachloro-1,3-butadiene
ug/kg
1660
1680
101
46-130
Hexachlorobenzene
ug/kg
1660
1790
108
58-130
Hexachlorocyclopentadiene
ug/kg
1660
1500
91
23-130
Hexachloroethane
ug/kg
1660
1600
97
47-130
Indeno(1,2,3-cd)pyrene
ug/kg
1660
1890
114
60-130
Isophorone
ug/kg
1660
1780
108
49-130
N-Nitroso-di-n-propylamine
ug/kg
1660
1670
101
47-130
N-Nitrosodimethylamine
ug/kg
1660
1600
97
45-130
N-Nitrosodiphenylamine
ug/kg
1660
1820
110
59-130
Naphthalene
ug/kg
1660
1660
100
55-130
Nitrobenzene
ug/kg
1660
1720
104
49-130
Pentachlorophenol
ug/kg
3310
3210
97
10-132
Phenanthrene
ug/kg
1660
1820
110
62-130
Phenol
ug/kg
1660
1650
99
46-130
Pyrene
ug/kg
1660
1720
104
53-130
Pyridine
ug/kg
1660
1280
78
37-130
2,4,6-Tribromophenol (S)
%
105
27-110
2-Fluorobiphenyl (S)
%
91
30-110
2-Fluorophenol (S)
%
90
13-110
Nitrobenzene-d5 (S)
%
91
23-110
Phenol-d6 (S)
%
86
22-110
Terphenyl-d14 (S)
%
71
28-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2837286
2837287
MS
MSD
92469360001
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD Qual
1,2,4-Trichlorobenzene
ug/kg
ND
1970
2020
1540
1440
78
71
18-130
7
1,2-Dichlorobenzene
ug/kg
NO
1970
2020
1530
1410
78
70
14-130
9
1,3-Dichlorobenzene
ug/kg
ND
1970
2020
1490
1370
76
68
12-130
8
1,4-Dichlorobenzene
ug/kg
ND
1970
2020
1590
1440
81
71
10-130
10
1-Methylnaphthalene
ug/kg
ND
1970
2020
1490
1370
76
68
12-130
8
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
1970
2020
1500
1430
76
71
10-130
5
2,4,5-Trichlorophenol
ug/kg
ND
1970
2020
1960
1870
100
93
13-130
5
2,4,6-Trichlorophenol
ug/kg
ND
1970
2020
1950
1850
99
92
17-130
5
2,4-Dichlorophenol
ug/kg
ND
1970
2020
2040
1880
104
93
10-130
8
2,4-Dimethylphenol
ug/kg
ND
1970
2020
1960
1800
100
89
10-130
9
2,4-Dinitrophenol
ug/kg
ND
9850
10100
7830
10100
80
100
10-130
26
2,4-Dinitrotoluene
ug/kg
ND
1970
2020
1970
1950
100
97
24-130
1
2,6-Dinitrotoluene
ug/kg
ND
1970
2020
1890
1920
96
95
23-130
2
2-Chloronaphthalene
ug/kg
ND
1970
2020
1530
1410
78
70
19-130
8
2-Chlorophenol
ug/kg
ND
1970
2020
1860
1740
95
86
10-130
7
2-Methylnaphthalene
ug/kg
ND
1970
2020
1490
1370
76
68
18-130
9
2-Methylphenol(o-Cresol)
ug/kg
ND
1970
2020
1880
1750
96
86
10-130
8
2-Nitroaniline
ug/kg
ND
3940
4050
4130
4020
105
99
17-130
3
Results presented on this page are In the units Indicated by the "Units" column except where an. alternate unit is presented to the right. of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date:. 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC, Page 49 of 59

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QUALITY CONTROL DATA
Project: 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2837286
MS
92469360001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2837287
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
2-Nitrophenol
ug/kg
ND
1970
2020
1860
1780
94
88
10-130
4
3&4-Methylphenol(m&p
ug/kg
ND
1970
2020
1890
1730
96
86
10-130
9
Cresol)
3,3'-Dichlorobenzidine
ug/kg
ND
3940
4050
2830
3030
72
75
10-130
7
3-Nitroaniline
ug/kg
ND
3940
4050
3810
3620
97
89
24-130
5
4,6-Dinitro-2-methyl phenol
ug/kg
ND
3940
4050
3320
3870
84
96
10-152
15
4-Bromophenylphenyl ether
ug/kg
ND
1970
2020
1520
1470
77
73
29-130
3
4-Chloro-3-methylphenol
ug/kg
ND
3940
4050
4010
3760
102
93
17-130
6
4-Chloroaniline
ug/kg
ND
3940
4050
3710
3380
94
83
14-130
9
4-Chlorophenyiphenyl ether
ug/kg
ND
1970
2020
1480
1380
75
68
25-130
7
4-Nitroaniline
ug/kg
ND
3940
4050
4080
3870
104
96
22-130
5
4-Nitrophenol
ug/kg
ND
9850
10100
10100
9790
102
97
10-130
3
Acenaphthene
ug/kg
ND
1970
2020
1500
1410
76
70
20-130
6
Acenaphthylene
ug/kg
ND
1970
2020
1550
1460
78
72
25-130
6
Aniline
ug/kg
ND
1970
2020
1670
1510
85
75
10-130
10
Anthracene
ug/kg
ND
1970
2020
1570
1450
80
71
29-130
8
Benzo(a)anthracene
ug/kg
ND
1970
2020
1550
1430
79
71
19-130
8
Benzo(a)pyrene
ug/kg
ND
1970
2020
1570
1410
80
70
12-130
10
Benzo(b)fluoranthene
ug/kg
ND
1970
2020
1510
1330
77
66
14-130
13
Benzo(g,h,i)perylene
ug/kg
ND
1970
2020
1760
1610
89
80
10-130
9
Benzo(k)fluoranthene
ug/kg
ND
1970
2020
1520
1360
77
67
14-130
12
Benzoic Acid
ug/kg
ND
9850
10100
9850
8360
100
83
10-130
16
Benzyl alcohol
ug/kg
ND
3940
4050
3760
3490
95
86
13-130
7
bis(2-Chloroethoxy)methane
ug/kg
ND
1970
2020
1780
1670
91
83
16-130
6
bis(2-Chloroethyl) ether
ug/kg
ND
1970
2020
1710
1600
87
79
11-130
7
bis(2-Ethylhexyl)phthalate
ug/kg
ND
1970
2020
1550
1510
78
74
21-130
3
Butylbenzyiphthalate
ug/kg
ND
1970
2020
1530
1470
78
73
23-130
4
Chrysene
ug/kg
ND
1970
2020
1590
1500
81
74
22-130
5
Di-n-butylphthalate
ug/kg
ND
1970
2020
1550
1410
79
70
30-130
10
Di-n-octylphthalate
ug/kg
ND
1970
2020
1640
1590
83
78
23-142
3
Dibenz(a,h)anthracene
ug/kg
ND
1970
2020
1740
1620
88
80
10-130
7
Dibenzofuran
ug/kg
ND
1970
2020
1570
1470
80
73
24-130
7
D iethylphtha late
ug/kg
ND
1970
2020
1700
1650
86
82
26-130
3
Dimethylphthalate
ug/kg
ND
1970
2020
1990
1940
101
96
22-130
2
Fluoranthene
ug/kg
ND
1970
2020
1520
1350
77
67
33-130
12
Fiuorene
ug/kg
ND
1970
2020
1540
1430
78
71
22-130
7
Hexachloro-1,3-butadiene
ug/kg
ND
1970
2020
1380
1280
70
63
13-130
8
Hexachiorobenzene
ug/kg
ND
1970
2020
1570
1510
80
75
29-130
3
Hexachlorocyclopentadiene
ug/kg
ND
1970
2020
1030
1050
52
52
10-130
2
Hexachloroethane
ug/kg
ND
1970
2020
1390
1260
71
62
10-130
10
Indeno(1,2,3-cd)pyrene
ug/kg
ND
1970
2020
1750
1590
89
79
10-130
10
Isophorone
ug/kg
ND
1970
2020
1920
1780
97
88
13-130
7
N-Nitroso-di-n-propylamine
ug/kg
ND
1970
2020
1810
1690
92
84
12-130
7
N-Nitrosodimethylamine
ug/kg
ND
1970
2020
1750
1540
89
76
11-130
13
N-Nitrosodiphenylamine
ug/kg
ND
1970
2020
1720
1710
87
85
15-130
0
Naphthalene
ug/kg
ND
1970
2020
1540
1410
78
70
15-130
9
Results presented on this page are In the units Indicated by the "Units" column. except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full;
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC. Page 50 of 59

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QUALITY CONTROL DATA
Project 842 UST
Pace Project No.: 92469653
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2837286
2837287
MS
MSD
92469360001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Nitrobenzene
ug/kg
ND
1970
2020
1810
1720
92
85
12-130
5
Pentachlorophenol
ug/kg
ND
3940
4050
3540
3460
90
86
10-130
2
Phenanthrene
ug/kg
ND
1970
2020
1600
1480
81
73
27-130
8
Phenol
ug/kg
ND
1970
2020
1860
1720
94
85
10-130
8
Pyrene
ug/kg
ND
1970
2020
1490
1460
76
72
19-130
2
Pyridine
ug/kg.
ND
1970
2020
1300
875
66
43
10-130
39 R1
2,4,6-Tribromophenoi (S)
%
86
57
27-110
2-Fluorobiphenyl (S)
%p
51
34
30-110
2-Fluorophenol (S)
%
84
66
13-110
Nitrobenzene-d5 (S)
%
79
59
23-110
Phenol-d6 (S)
%
80
62
22-110
Terphenyl-d14 (S)
%
32
17
28-110
SO
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC.
Page 51 of 59

,��alcie Analytical
www.pacelabs.com
t
QUALITY CONTROL DATA
Project: 842 UST
Pace Project No.: 92469653
QC Batch: 531181 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Soil
Associated Lab Samples: 92469653001, 92469653002, 92469653003, 92469653004, 92469653005
METHOD BLANK: 2836119
Matrix: Solid
Associated Lab Samples: 92469653001, 92469653002, 92469653003, 92469653004, 92469653005
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Aliphatic (C09-C 18)
mg/kg
ND 10.2 03/19/20 11:32 N2
Aliphatic (C19-C36)
mg/kg
ND 10.2 03/19/20 11:32 N2
Aromatic (C11-C22)
mg/kg
ND 10.2 03/19/20 11:32 N2
2-Bromonaphthalene (S)
%
117 40-140 03/19/20 11:32
2-Fluorobiphenyl (S)
%
116 40-140 03/19/20 11:32
Nonatriacontane (S)
%
81 40-140 03/19/20 11:32
o-Terphenyl (S)
%
91 40-140 03/19/20 11:32
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE & LCSD: 2836120
Parameter Units
Spike
Conc.
2836121
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec
Limits
Max
RPD RPD Qualifiers
Aliphatic (C09-C18)
mg/kg
10.2
ND ND
65
62
40-140
50 N2
Aliphatic (C19-C36)
mg/kg
13.6
11.4 10.9
84
81
40-140
5 50 N2
Aromatic (Cl 1-C22)
mg/kg
28.8
25.5 21.5
89
75
40-140
17 50 N2
2-Bromonaphthalene (S)
%
116
100
40-140
2-Fluorobiphenyl (S)
%
116
97
40-140
Nonatriacontane (S)
%
78
71
40-140
o-Terphenyl(S)
%
99
85
40-140
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, I.I.C.
Page 52 of 59

11�AoAnalXical'
www.pacelabs.com
i
QUALITY CONTROL DATA
Project: 842 UST
Pace Project No.: 92469653
QC Batch: 530773 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92469653001, 92469653002, 92469653003, 92469653004, 92469653005, 92469653006
SAMPLE DUPLICATE: 2834251
92469645003 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 20.1 19.7 2
SAMPLE DUPLICATE: 2834252
92469666001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 79.9 79.9 0
Pace Analytical Services, LLC
9800 Kincey Ave. Suite100
Huntersville, NC 28078
[phone]
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC,
Page 53 of 59

aceAnalytical
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QUALITY CONTROL DATA
Project: 842 UST
Pace Project No.: 92469653
QC Batch: 1449507 Analysis Method: SM 254OG
QC Batch Method: SM 2540 G Analysis Description: Total Solids 2540 G-2011
Associated Lab Samples: 92469653001, 92469653002, 92469653003, 92469653004, 92469653005
METHOD BLANK: R3512327-1 Matrix: Solid
Associated Lab Samples: 92469653001, 92469653002, 92469653003, 92469653004, 92469653005
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Solids % NO 03/24/20 23:03
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: R3512327-2
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Solids % 50 50.0 100 85-115
SAMPLE DUPLICATE: R3512327-3
92469653002 Dup
Parameter Units Result Result RPD Qualifiers
Total Solids % 65.4 63.9 2.33
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, LLC.
Page 54 of 59

aceAnalytical
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QUALIFIERS
Project; 842 UST
Pace Project No.: 92469653
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC28078
[phone]
PQL- Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix,
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270, The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
E Analyte concentration exceeded the calibration range. The reported result is estimated.
IH This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value,
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples maybe biased high.
M1 Matrix spike recovery exceeded QC limits, Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
S0 Surrogate recovery outside laboratory control limits.
S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
u8 Data does not meet all conditions for compliance monitoring due to use of soil jars.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
REPORT OF LABORATORY ANALYSIS
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Date: 03/26/2020 01:45 PM without the written consent of Pace Analytical Services, I.L.C.
Page 55 of 59

aceAnalytical
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: 842 UST
Pace Project No,: 92469653
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC`28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Analytical
Batch
92469653006
SB-6 (5')
EPA 3546
531340
EPA 8015C Modified
531589
92469653001
SB-2 (6"-1')
MADEP EPH
531181
MADEP EPH
531449
92469653002
SB-3 (0-6")
MADEP EPH
531181
MADEP EPH
531449
92469653003
SB-1 (18"-24")
MADEP EPH
531181
MADEP EPH
531449
92469653004
SB-4 (1')
MADEP EPH
531181
MADEP EPH
531449
92469653005
SB-5 (1')
MADEP EPH
531181
MADEP EPH
531449
92469653001
SB-2 (6"-1')
MADEPV
1449842
MADEP VPH
1449842
92469653002
SB-3 (0-6")
MADEPV
1449842
MADEP VPH
1449842
92469653003
SB-1 (18"-24")
MADEPV
1449842
MADEP VPH
1449842
92469653004
SB-4 (I-)
MADEPV
1449842
MADEP VPH
1449842
92469653005
SB-5 (1')
MADEPV
1449842
MADEP VPH
1449842
92469653001
SB-2 (6"-1')
EPA 3546
531416
EPA 8270E
531685
92469653002
SB-3 (0-6")
EPA 3546
531416
EPA 8270E
531685
92469653003
SB-1 (18"-24")
EPA 3546
531416
EPA 8270E
531685
92469653004
SB-4 (1')
EPA 3546
531416
EPA 8270E
531685
92469653005
SB-5 (1')
EPA 3546
531416
EPA 8270E
531685
92469653001
SB-2 (6"-1')
EPA 5035A
531178
EPA 8260D
531182
92469653002
SB-3 (0-6")
EPA 5035A
531178
EPA 8260D
531182
92469653003
SB-1 (18"-24")
EPA 5035A
531178
EPA 8260D
531182
92469653004
SB-4 (1')
EPA 5035A
531399
EPA 8260D
531410
92469653005
SB-5 (1')
EPA 5035A
531178
EPA 8260D
531182
92469653001
SB-2 (6"-1')
ASTM D2974-87
530773
92469653002
SB-3 (0-6")
ASTM D2974-87
530773
92469653003
SBA (18"-24")
ASTM D2974-87
530773
92469653004
SB-4 (1')
ASTM D2974-87
530773
92469653005
SB-5 (1')
ASTM D2974-87
530773
92469653006
SB-6 (5)
ASTM D2974-87
530773
92469653001
SB-2 (6"-1')
SM 2540 G
1449507
SM 254OG
1449507
92469653002
SB-3 (0-6")
SM 2540 G
1449507
SM 254OG
1449507
92469653003
SB-1 (18"-24")
SM 2540 G
1449507
SM 254OG
1449507
92469653004
SB-4 (1')
SM 2540 G
1449507
SM 2540G
1449507
92469653005
SB-5 (1')
SM 2540 G
1449507
SM 2540G
1449507
Date: 03/26/2020 01 A5 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 56 of 59

65 iO L9 96ed
Document Name:
Document Revised: February 7, 2018
aeeAnalytiea!
Sample Condition Upon Recelpt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F•CAR•CS•033•Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Ralelgh❑ Mechanicsville❑
rj ,, Client Name: ® 3
��i I a Project #:
Courier: ❑Fed Ex ❑UPS ❑USPSI ❑Client II Il + II II I (If I�
❑ Commercial OPace []Other: 924696°S3
Custody Seal Present? ❑Yes ❑No' Seals Intact? ❑Yes ❑No
Date/initials Person Examining Contents,.,'I" P
Packing Material: ❑Bubble Wrap [:Bubble Bags ❑None ❑ Other Biological Tissue F oxen?
Thermometer: []Yes FIND ' N/A
❑IR Gun ID:- 92TO60 Type of Ice: ❑yVet ❑Blue QNone
Cooler Temp ('C): Correction Factor; Add/Subtract ('C) 0.0
( Temp should be above freezing to 6°C
Cooler letup Corrected ('C):
❑Samples out of temp criteria. Samples orrice, cooling process
hasbegun
USDA Regulated Sall (❑ N/A, water sample)
Did samples oilpPate in a quarantine`zone within the United States: CA, NY, or SC {check maps)? Did samples originate from a foreign source (intern tionilly,
rlYes INo Includlne Hawaii and Puerto Ricni? rlYes 177INo
Comments/Discrepancy,
'chain of Cus(oily Present? � ' '
[:]No❑N/A
1.
Samples Arrived within Hold Time?
,Yews
13Ves
No _
❑N/A
2.
Short Hold Time Analysis j0Zlin)?
❑Yes
QNo ...
WA
3.
Rush Turn Around TimtRequested?
OYes
❑No
❑N/A
4.
Sufficient Volume? l
[]Yes.
No
N/A
5.
Correct Containers Used?
-Pace Containers Used?
❑Yes:
[]Yes
❑Na
❑No
[]N/A
❑N/A
6.
Containers Intact?
❑Yes
EIN.
EIN�/A
7.
Dissolved analysis: Samples Field filtered?
❑Yes
[]No
IJN/A
8,
Sample Labels Match COC?
❑Yes
❑No
❑N/A
9.
-includes Date/Time/ID/Analysis Matrix:
Headspace In VOA Vials (>5-6mm)?
❑Yes
❑No.,..
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
Yes
(--]No
No
❑N/A
N%A
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
' CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time.
Date:
Date:
Field Data Required? ❑Yes []No

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BP4U-125 mL Plastic Unpreserved (N/A) (CI-)
BP311.1-250mi. Plastic Unpreserved (N/A)
BP210-500 mL Plastic Unpreserved (N/A)
BP1U-1 liter Plastic Unpreserved (N/A)
OP45-125 mL Plastic H2SO4 (pH < 2) (Cl-)
BP3N•250 mL plastic HNO3 (pH < 2)
BP42-125 mL Plastic ZN Acetate & NaOH M)
BP4C-125 mL Plastic NaOH (pH > 12) (CI-)
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WGFU-Wide-mouthed Glass jar Unpreserved
AGIU-1 liter Amber Unpreserved (N/A) (CI-)
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AG1H-1 Titer Amber HCI (pH <2)
AG3U-2S0 mL Amber Unpreserved (N/A) (Ci-)
1ZZAG35-1
liter Amber H2SO4 (pH < 2)
AG3S-250ml. Amber HZSO4 (pH <2)
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AG3A(DG3A)-250 mL Amber NH4CI (N/A)(CI-)
OG9H-00 mL VOA HCI (N/A)
VG9T-40 mL VOA Na2S203 (N/A)
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DG9P-40 mL VOA H3PD4 (N/A)
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V/GK (3 vials per kit)•VPHJGas kit (N/A)
SPSi-125 mL Sterile Plastic (N/A— lab)
SPIT-250 ml. Sterile Plastic (N/A —lab)
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BP3A-2S0 ml. Plastic (NH2)2SO4 (9.3-9.7)
IAGOU-100
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VSGU-20 mL Scintillation vials (N/A)
DG9U-40 mL Amber Unpreserved vials (N/A)
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Appendix K
Photographs of Site Check, Closure and Excavation
(This Appendix was not used)

Appendix L
Geologic Log of the Excavation
(This Appendix is not applicable to this project)

Appendix M
Monitor Well Construction Forms
(This Appendix is not applicable to this project)

Beverly, Trudy
From: Beverly, Trudy
Sent: Monday, April 13, 2020 12:16 PM
To: Rick Harmon
Subject: RE: [External] Initial Abatement Action Report for Schulte Residence 4043 Arborway,
Charlotte, NC Incident 40898
Thanks Rick!
From: Rick Harmon [maiIto: [e-mail]]
Sent: Monday, April 13, 2020 11:36 AM
To: Beverly, Trudy <[e-mail]>
Subject: Re: [External] Initial Abatement Action Report for Schulte Residence 4043 Arborway, Charlotte, NC Incident
40898
External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
[e-mail]
See Attached. Call me if you need anything else.
Richard Harmon, P.G.
Harmon Environmental, PA
615 Bruce Thomas Road
Monroe, NC 28112
704-292-4527
harmonenvironmental. com
On Monday, April 13, 2020, 09:48:27 AM EDT, Beverly, Trudy <trudy.beverly(c�ncdenr.gov> wrote:
Rick,
The IAR report needs to be resubmitted to comply with the UST document submittal policy (see the March 20,
2020 memo). Files should have Optical Character Recognition (OCR) applied. Any scanned document should
have a minimum resolution of 300dpi. Portfolio formats, password protections and/or encryptions should not
be included in the electronic file.
UST website https:Hdeg.nc.gov/about/divisions/waste-management/ust/whats-new
Thanks,
Trudy
Trudy Beverly, L.G.
�� Hydrogeologist, Division of Waste Management
D, E North Carolina Department of Environmental Quality
ue"�um�tol i�;�me nL3 UST Section, Mooresville Regional Office

704.235.2182 (Office)
Trudy.BeverlyC&ncdenr. gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https:Hdeq.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: htWs://deq.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https:Hdeq.nc.gov/about/divisions/waste-management/waste-management-rules-datalwaste-mana ee ment- ig s-mates
File Review Procedures:
https:Hdeq.nc. gov/about/divisions/waste-managementlust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
https:Hdeq.nc.,gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
https://files.nc.2ov/ncdea/Waste%20Mana2ement/D W M/UST/WhatsNew/Final-Electronic-Document-Submittal-Poliev.pdf
https:Hfiles.nc. gov/ncdeq/Waste%2OManagementIDWM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: Beverly, Trudy
Sent: Tuesday, April 7, 2020 11:11 AM
To: Rick Harmon <harmonenv(a�yahoo.com>
Subject: RE: [External] Initial Abatement Action Report for Schulte Residence 4043 Arborway, Charlotte, NC
Incident 40898
Received. No need to post this one to FileZilla. You may find the info below useful. I'll also forward the new
policy to you.

The UST Section has had a change in document submittals as of Friday, March 23rd. I will forward you the
notice in a separate email. They may have missed some consultants. It is my current understanding that the
UST Section no longer requires a paper copy as of March 23rd. Electronic copies can be posted to
FileZilla. The project manager should also be notified via email that a file is on FileZilla for review. The file can
also be attached to the email to the project manager notifying them that a file has been posted to FileZilla. Our
mailing system can handle most file sizes. It is rare to have a file that we cannot receive via email due to its
size. The file can also be placed on a cd and mailed with a cover letter the appropriate regional office if you
don't want to use FileZilla. I suggest that you also email an electronic copy of the file whether you choose to
post to FileZilla or mail a copy on cd with cover letter. Make sure that the electronic reports are signed/sealed
and contain all tables, figures, and lab reports.
Trudy
j-� "c-��D
._:4 �EQ
Lot" rum nI of 6� L314wvty!
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy.Beverlykncdenr. og_v
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: htips:Hdeg.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
https:Hdeg.nc.,aovlabout/divisions/waste-managementlwaste-management-rules-datalwaste-mana eg ment ig s=maps
File Review Procedures:
hfps:Hdeq.nc. gov/about/divisions/waste-managementlustlfile-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
hfps:Hdeq.nc. gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
https://files.nc.govincdeg/Waste%2OManallement/D W MIUSTIWhatsNew/Fin al -Electronic -Document -Sub mittal-Poliev.pdf

https:Hfiles.nc. aovincdeglW aste%20ManagementIDWMIUST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: Rick Harmon [mailto:harmonenv(@yahoo.coml
Sent: Tuesday, April 7, 2020 10:31 AM
To: Beverly, Trudy <trudy.beverly(@ncdenr.gov>
Subject: [External] Initial Abatement Action Report for Schulte Residence 4043 Arborway, Charlotte, NC
Incident 40898
rnal email. Do not click links or open attachments unless you verify. Send all suspicious email as an
attachment to report. [e-mail]
Trudy
I sent this report to via priority mail on March 31, 2020. Due to the current shut -down, I was not certain if you would
receive it. Attached please find a digital copy for your use in the interim. We will proceed with the NORP for the former
UST basin and forward it to you in the near future.
Call or email if you have questions.
Richard Harmon, P.G.
Harmon Environmental, PA
615 Bruce Thomas Road
Monroe, NC 28112
704-292-4527
harmonenvironmental.com