WS-4595_14913_CA_MRP_20200318

GROUNDWATER MONITORING REPORT
KUNTRY KORNER
1075 BALD HILL LOOP
MADISON, ROCKINGHAM COUNTY, NORTH CAROLINA

NCDEQ INCIDENT NUMBER: TF-14913
NCDEQ CONTRACT NUMBER: N17006

ECS PROJECT 49-6390-A

PREPARED FOR:

NCDEQ, UST SECTION
RALEIGH, NORTH CAROLINA

March 18, 2020

March 18, 2020

Ms. Linda Blalock
NCDEQ, Division of Waste Management, UST Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Reference: Groundwater Monitoring Report
Kuntry Korner
1075 Bald Hill Loop
Madison, Rockingham County, North Carolina
NCDEQ Incident No.: TF-14913
NCDEQ Contract No. N17006
ECS Project 49:6390-A

Dear Ms. Blalock:

As authorized by your acceptance of ECS Southeast, LLP’s (ECS) Task Authorization Request No.
2 dated June 13, 2019; and ECS’ emailed change order dated November 21, 2019, ECS has
prepared a Groundwater Monitoring Report for the above referenced site. This report includes a
description of the work performed, the results obtained, and our conclusions and
recommendations.

ECS appreciates the opportunity to provide our environmental consulting services to you on this
project. If you have any questions concerning this report or this project, please contact us.

Sincerely,

ECS SOUTHEAST, LLP

Scott Young, P.G. Roger A. Smith, P.G.
Environmental Project Manager Principal Geologist
[e-mail] [e-mail]
704-525-5152 704-525-5152

Groundwater Monitoring Report
Kuntry Korner
Madison, Rockingham County, North Carolina
NCDEQ Incident No.: TF-14913
ECS Project 49:6390-A
March 18, 2020

1

SITE INFORMATION

Site Name: Kuntry Korner

Site Address: 1075 Bald Hill Loop
State Road, North Carolina 28676

Facility ID Number: Unknown

UST ID Number: WS-4595

NCDEQ Incident Number: TF-14913

Site Risk Ranking: High (Assigned)

Land Use Category: Residential (Assigned)

Latitude/Longitude: 36.3557755 N /79.922142 W

Responsible Party: Melvin L Ashburn, Sr. (deceased)
115 Turner Drive
Mayodan, North Carolina 27027

Current Property Owner: Augusta C. Ashburn
115 Turner Road
Mayodan, NC 27027

Primary Contact: Ms. Linda Blalock
NCDEQ, Division of Waste Management, UST Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646

Primary Consultant: ECS Southeast, LLP
4811 Koger Boulevard
Greensboro, North Carolina 27407
[phone]

Laboratory: Prism Laboratories, Inc.
449 Springbrook Road
Charlotte, North Carolina 28224
[phone]
Laboratory Certification No. 402

1

TABLE OF CONTENTS

1.0 EXECUTIVE SUMMARY ................................................................................................. 2
2.0 PROJECT INFORMATION .............................................................................................. 3
3.0 FIELD ACTIVITIES .......................................................................................................... 5
3.1 Geophysical Survey ................................................................................................... 5
3.2 Monitoring Well Sampling .......................................................................................... 5
3.3 Water-supply Well Sampling ...................................................................................... 6
3.4 Groundwater Chemistry ............................................................................................. 6
4.0 RESULTS ........................................................................................................................ 6
4.1 Monitoring Well Sampling Results ............................................................................. 6
4.2 Water-Supply Well Sampling Results ........................................................................ 7
4.3 Groundwater Flow Direction ...................................................................................... 7
5.0 CONCLUSIONS AND RECOMMENDATIONS ................................................................ 7

FIGURES

Figure 1 USGS Topographic Map
Figure 2 Site Map
Figure 3 Water Supply Well Location Map
Figure 4 Groundwater Analytical Map
Figure 5 Groundwater Contour Map

TABLES

Table 1 UST System Information
Table 1 Water Supply Well Information
Table 2 Monitoring Well Construction and Groundwater Elevation Data
Table 3 Geochemical Measurements
Table 4 Summary of Groundwater Analytical Results
Table 5 Summary of Water Supply Well Analytical Results

APPENDIX

Appendix A Site Photographs
Appendix B Geophysical Survey Map
Appendix C Laboratory Analytical Report and Chain-of-Custody Form
Appendix D Groundwater Sampling Data Forms

Groundwater Monitoring Report
Kuntry Korner
Madison, Rockingham County, North Carolina
NCDEQ Incident No.: TF-14913
ECS Project 49:6390-A
March 18, 2020

2
1.0 EXECUTIVE SUMMARY

As part of Task Authorization No. 2, NCDEQ Contract No. N17006, ECS was contracted to sample
or gauge free product in monitoring wells MW-1 through MW-8, collect samples from water supply
wells WSW-1 through WSW-8, conduct a geophysical survey of the site, and prepare a monitoring
report in regard to NCDEQ Incident No. 14913.

INCIDENT RISK EVALUATION SUMMARY
SOURCE INFORMATION
Source, Date and Nature of Release December 1992 - Unknown
Each Known Source Removed? Yes – USTs were removed
Additional Sources Likely Present? Two suspected USTs
Each Known Source Assessed
(USTs, Piping, Dispensers)? Yes
LNAPL
LNAPL Present? Yes
If yes, depth below ground surface? ~35-38 feet below ground surface
If yes, maximum thickness? 0.09 feet
If yes, extent delineated? No
SITE SOIL CONDITIONS
TPH Soil Data Available? Maximum concentration at site TPH-GRO – 133,000 mg/kg-KK T5-
03/11/96
Risk-Based Soil Data Available? No
Maximum Soil Contaminant Concentrations NA
Extent of Soil Impact Delineated? Unknown
SITE GROUNDWATER CONDITIONS
Average Depth to Groundwater? ~36 feet
Contaminants Present Above NCAC 2L Standards? Yes
Contaminants Present Above Risk-Based GCLs? No; however LNAPL present
Groundwater Plume Delineated? No
Groundwater Plume Migrated Off-Site? Unknown
Contaminant Level Trend Decreasing in samples collected
RECEPTOR INFORMATION
Date of Most Current Receptor Survey February 2010
Potable Water-Supply Wells within 1,000’? Yes
Municipal Water Available to Each Property within 1,000’? No
Non-Potable Wells within 250’? Yes
Site within Wellhead Protection Area? No
Surface Water Bodies within 500’? No
REMEDIAL ACTIVITIES
What active remedial activities, if any, have been conducted to date? UST removal, AFVRs and MMPE events
Are active remedial activities working? Yes
VAPOR INTRUSION
LNAPL or Dissolved Phase Contaminants exceeding Groundwater
Screening Levels for Vapors present within 5’ of Ground Surface?
No
Occupied Structures on the Site? Yes – vacant building

In July 2019, ECS personnel performed gauging and/or sampling of six monitoring wells. Samples
were also collected from five water supply wells. A geophysical survey of the subject property was
also conducted.

Groundwater Monitoring Report
Kuntry Korner
Madison, Rockingham County, North Carolina
NCDEQ Incident No.: TF-14913
ECS Project 49:6390-A
March 18, 2020

3
Based on the results of this sampling event, groundwater concentrations in the samples collected
from monitoring wells MW-2, MW-4, and MW-8 have decreased since the previous sampling events
conducted in August 2014 and May 2018. In addition, free product thickness measured in monitoring
wells MW-3, MW-6, and MW-7 have decreased as compared to the previous gauging event
conducted in May 2018. Groundwater Contamination Levels (GCLs) exceedances have previously
been reported in samples collected from monitoring wells MW-1, MW-3, and MW-5. Monitoring wells
MW-1 and MW-5 have not been located since August 2014 and monitoring well MW-3 has contained
measurable free product since May 2010.

Compound concentrations in excess of the North Carolina 2L Groundwater Quality Standards
(NC2LGWQS) were detected in the sample collected from water supply well WSW-8 on July 31,
2019. Compound concentrations had not been detected in any sample collected from water supply
well WSW-8 greater than the laboratory method reporting limits in any previous sample collected.
ECS returned to the site on November 21, 2019 and collected an additional sample from water supply
well WSW-8. The analytical results of the sample collected in November 2019 did not indicate any
compounds at concentrations greater than the laboratory method reporting limits.

Results of the geophysical survey conducted by KCI indicated two potential previously unknown
USTs located to the north of the site structure.

Based on the conclusions above, ECS recommends installing free product adsorbent socks in
monitoring wells MW-3, MW-6, and MW-7 in order to further reduce the free product thicknesses in
these wells. The free product adsorbent socks would need to be removed and replaced on a bi-
monthly basis. During the installation of the initial free product adsorbent socks, ECS recommends
advancing soil borings via hand auger in the vicinity of the anomalies identified by KCI in order to
confirm the possible presence of previously unknown USTs. Due to the presence of overgrown
brush thickets, ECS recommends conducting clearing activities in order to potentially locate
monitoring wells MW-1 and MW-5 which previously contained the highest compound concentrations
at the site. In addition, ECS recommends collecting a sample from water supply well WSW-8 in
approximately three to four months (February to March 2020) to confirm the recent sampling results.

2.0 PROJECT INFORMATION

The subject site is Kuntry Korner located at 1075 Bald Hill Loop in Madison, Rockingham County,
North Carolina (Figure 1). Photographs of the site are included in Appendix A. Based on
information provided to ECS, sampling conducted by NCDEQ personnel indicated the presence
of methyl tert-butyl ether (MTBE) in an off-site water-supply well in 1995. The incident was
accepted into the Federal Trust Fund in December of 1995.

A geophysical survey conducted in 1996 identified five USTs. In March 1997, Geophex Ltd.
(Geophex) removed two 1,000-gallon USTs, one 550-gallon UST, and two 560-gallon USTs from
the site. UST closure samples collected by Geophex indicated Total Petroleum Hydrocarbons
(TPH) Gasoline Range Organics at concentrations as high as 133,000 milligrams per kilogram.
No concentrations of TPH Diesel Range Organics were detected greater than the laboratory
method reporting limits. Based on the results of UST closure samples collected, Geophex
assumed the previous contents of the USTs were gasoline. The locations of the former USTs are
shown on Figure 2.
Groundwater Monitoring Report
Kuntry Korner
Madison, Rockingham County, North Carolina
NCDEQ Incident No.: TF-14913
ECS Project 49:6390-A
March 18, 2020

4

In 1999, 12 soil borings were advanced on the subject site and four water-supply wells were
sampled by Geophex. Laboratory analysis of the soil samples collected from the soil borings
confirmed the presence of petroleum contamination extending behind the store and toward the
rear (northeast) of the property. MTBE was also detected in water-supply wells WSW-2 and
WSW-3 at concentrations greater than its NC2LGWQS, but less than its GCL. Information
regarding the water supply wells is provided in Table 2. Five monitoring wells (MW-1 through
MW-5) were installed in March 2000. The location of the monitoring wells are shown on Figure
2. Samples were only collected from monitoring wells MW-4 and MW-5 in March 2000, as
monitoring wells MW-1, MW-2, and MW-3 contained measurable amounts of free product.
Laboratory analysis of the groundwater samples indicated several petroleum constituents at
concentrations greater than their respective NC2LGWQS, but less than their respective GCLs, in
the samples collected from monitoring wells MW-4 and MW-5.

An aggressive fluid vapor recovery (AFVR) event was conducted in 2003. Approximately 149
gallons of free product was recovered during the eight-hour AFVR event. After the AFVR event,
the monitoring wells were gauged for free product thickness. Only monitoring well MW-1 showed
measurable free product. Measurable free product was observed in monitoring wells MW-1, MW-
2, and MW-3 in a second post-AFVR gauging event, performed in April 2003.

In 2005, a mobile multi-phase extraction event (MMPE) was conducted. Approximately 55.95
total gallons of free product was recovered during the event. The monitoring wells were gauged
immediately following the event. Monitoring wells MW-1, MW-2, and MW-3 reportedly exhibited
a sheen and were subsequently gauged with no free product detected.

Gauging of monitoring wells MW-1, MW-2, and MW-3 in 2006 indicated free product at
thicknesses of 0.34 feet, 0.56 feet, and 0.95 feet, respectively. Despite increased levels of free
product from 2005, the overall level of free product had decreased since 2003. Analysis of
groundwater samples collected from monitoring wells MW-1, MW-3, and MW-4 detected
petroleum constituents above their respective GCLs. Monitoring well MW-5 could not be located.

Several 96-hour MMPE events were conducted at the site in May, June, July, and September of
2011. Monitoring wells MW-6, MW-7, and MW-8 were installed during the MMPE event in
September of 2011. Samples obtained from monitoring wells MW-1, MW-2, MW-4, MW-5, and
MW-8 indicated concentrations of compounds exceeding their respective NC2LGWQS and
GCLs.

Following the completion of the most recent 96-hour MMPE event (July 2012), free product was
observed in monitoring wells MW-3, MW-6, and MW-7 at thicknesses of 0.13 feet, 0.21 feet, and
2.55 feet, respectively. Monitoring wells MW-1, MW-2, MW-4, MW-5, and MW-6 were sampled
after the completion of the MMPE event. Laboratory analysis of the groundwater collected from
the monitoring wells detected targeted compounds above their respective NC2LGWQSs.
Laboratory analysis of groundwater collected from monitoring well MW-1 detected benzene and
MTBE above their respective GCLs. The report indicated that concentrations of dissolved phase
contaminants have generally decreased in groundwater collected from monitoring wells MW-2
and MW-5 since the implementation of the MMPE events. The relative persistence of the
Groundwater Monitoring Report
Kuntry Korner
Madison, Rockingham County, North Carolina
NCDEQ Incident No.: TF-14913
ECS Project 49:6390-A
March 18, 2020

5
dissolved phase contaminants in groundwater samples collected from monitoring well MW-1 was
attributed to its downgradient location relative to the source area.

On August 15, 2014, ECS personnel collected samples from five monitoring wells (MW-1, MW-2,
MW-4, MW-5, and MW-8). Laboratory analysis of groundwater samples collected from monitoring
wells MW-1, MW-2, MW-4, MW-5, and MW-8 detected targeted compounds that exceed their
respective NC2LGWQS with the concentrations of benzene in monitoring wells MW-1 and MW-5
and the concentration of MTBE in monitoring well MW-8 exceeding their respective GCLs.
Measurable free product was observed in monitoring wells MW-3 (0.44 feet), MW-6 (1.37 feet)
and MW-7 (2.7 feet), and therefore, these monitoring wells were not sampled.

Between August 15, 2014 and August 22, 2014, ECS collected samples from six water-supply wells
(WSW-2 through WSW-5, WSW-7 and WSW-8) located in the vicinity of the site. Laboratory
analysis of the groundwater samples collected from the area water-supply wells did not detect
targeted compounds above laboratory quantitation limits. Water-supply well WSW-1 was not
sampled due to the property being vacant and there was no power to the residence. ECS did not
receive permission to sample water supply well WSW-6, therefore it was not sampled during site
visits.

ECS collected samples from monitoring wells MW-4 and MW-8 and water supply wells WSW-2
through WSW-5, WSW-7, and WSW-8 on May 1, 2018. Free product was measured in monitoring
wells MW-3, MW-6, and MW-7 ranging from 0.08 feet (MW-3) to 3.57 feet (MW-7). Monitoring
wells MW-1, MW-2, and MW-5 could not be located due to overgrown brush thickets. Review of the
laboratory analytical results indicated compound concentrations greater than their respective
NC2LGWQS, but less than their respective GCLs. No compounds were detected at concentrations
greater than the laboratory method reporting limits in the water supply well samples collected.

3.0 FIELD ACTIVITIES

3.1 Geophysical Survey

On July 31, 2019, ECS observed KCI Technologies, Inc. (KCI) perform a geophysical survey of
the site in order to potentially identify any previously unknown USTs at the site. KCI personnel
identified two anomalies located on the north side of the site structure. The signal on the ground
penetrating radar display indicated potential USTs. KCI personnel also detected metallic objects
in the vicinity of the anomalies with a metal detector which would seem to confirm the presence
of two previously unknown USTs. A figure provided by KCI showing the locations of the anomalies
is included in Appendix B.

3.2 Monitoring Well Sampling

On July 31, 2019, ECS personnel gauged and sampled monitoring wells MW-2, MW-4, and MW-8.
Free product was measured in monitoring wells MW-3 (0.02 feet), MW-6 (0.05 feet), and MW-7
(0.09 feet); therefore, these monitoring wells were not sampled. Monitoring wells MW-1 and MW-5
could not be located even with the use of a metal detector due to overgrown brush thickets. The
locations of the wells are shown on Figure 2. Monitoring well construction details and water level
elevation data are summarized in Table 2. Prior to sampling, the wells were purged using a new
Groundwater Monitoring Report
Kuntry Korner
Madison, Rockingham County, North Carolina
NCDEQ Incident No.: TF-14913
ECS Project 49:6390-A
March 18, 2020

6
disposable polyethylene bailer and new length of nylon cord. The wells were developed/purged
by evacuating a minimum of three well volumes. After purging was completed, the groundwater
samples were collected into laboratory prepared containers. Each container was labeled and
placed in a cooler containing ice to maintain the samples at approximately four degrees Celsius
(ºC). The sample containers were then submitted to Pace Analytical Services, LLC (Pace), a
North Carolina certified laboratory located in Huntersville, North Carolina to be analyzed for
volatile organic compounds (VOCs) using Standard Method 6200B. A Chain of Custody Record
(COC) was maintained and is included in the Appendix C.

3.3 Water-supply Well Sampling

On July 31, 2019, ECS collected samples from water-supply wells WSW-2, WSW-3, WSW-4,
WSW-7 and WSW-8. Water supply well WSW-1 was unable to be sampled as the property is
vacant and there is no power supply to the property. Water supply wells WSW-5 and WSW-6 were
unable to be sampled as permission was not obtained. The locations of the water-supply wells are
shown on Figure 3. Water-supply well ownership can be found on Table 1. Prior to sampling, the
water-supply wells and household plumbing were purged by allowing the water to run for
approximately 20 minutes. After purging was completed, the sample was collected into laboratory
prepared containers. Each container was labeled and placed in a cooler containing ice to maintain
the samples at approximately 4 ºC. The sample containers were then submitted to Pace to be
analyzed for VOCs using Standard Method 6200B.

Based upon the laboratory analytical results of the sample collected from water supply well WSW-
8 on July 31, 2019, ECS returned to the site on November 21, 2019, to collect an additional
sample from WSW-8. Prior to sampling, the water-supply well were purged by allowing the water
to run for approximately 20 minutes. After purging was completed, the sample was collected into
laboratory prepared containers. Each container was labeled and placed in a cooler containing
ice to maintain the samples at approximately 4 ºC. The sample containers were then submitted
to Pace to be analyzed for VOCs using Standard Method 6200B.

3.4 Groundwater Chemistry

Prior to collecting the groundwater samples from monitoring wells MW-2, MW-4, and MW-8,
geochemical parameters (temperature, pH, dissolved oxygen, and conductivity) were measured.
The turbidity was observed during the sampling and recorded on the Groundwater Sampling Data
Sheets (Appendix D). Based on the geochemical data, the average groundwater temperature
was 16.52 °C and the average conductivity was 0.104 millisiemens per centimeter. The pH
ranged between 4.42 and 7.05, and the dissolved oxygen (DO) ranged between 4.80 milligrams
per liter (mg/l) to 6.02 mg/l. The geochemical measurements are shown on Table 3.

4.0 RESULTS

4.1 Monitoring Well Sampling Results

Review of the laboratory analytical results indicated benzene, MTBE, and naphthalene in the
samples collected from monitoring wells MW-1 and MW-4, and 1,2-dichloroethane (1,2-DCA) and
1,2-dibromoethane in the sample collected from monitoring well MW-4, were detected at
Groundwater Monitoring Report
Kuntry Korner
Madison, Rockingham County, North Carolina
NCDEQ Incident No.: TF-14913
ECS Project 49:6390-A
March 18, 2020

7
concentrations greater than their respective NC2LGWQS, but less than their respective GCLs. No
compounds were detected in the groundwater sample collected from monitoring well MW-8 at
concentrations greater than the laboratory method reporting limits. The groundwater analytical
results are summarized in Table 4 and graphically depicted on Figure 4.

4.2 Water-Supply Well Sampling Results

Review of the laboratory analytical results indicated benzene, 1,2-DCA, and MTBE were detected in
the sample collected from water supply well WSW-8 on July 31, 2019, at concentrations greater than
their respective NC2LGWQS, but less than their respective GCLs. No compounds were detected in
the samples collected from the remaining water supply wells at concentrations greater than the
laboratory method reporting limits. The results of the second sample collected from water supply
well WSW-8 on November 21, 2019, did not indicate any compounds present at concentrations
greater than the laboratory method reporting limits.

The water supply well sample analytical results are summarized on Table 5.

4.3 Groundwater Flow Direction

Based on the groundwater elevation data collected on July 31, 2019, the groundwater flow
direction is generally to the northeast beneath the site, as depicted on Figure 5.

5.0 CONCLUSIONS AND RECOMMENDATIONS

Based on the results of this sampling event, groundwater concentrations in the samples collected
from monitoring wells MW-2, MW-4, and MW-8 have decreased since the previous sampling events
conducted in August 2014 and May 2018. In addition, free product thickness measured in monitoring
wells MW-3, MW-6, and MW-7 have decreased as compared to the previous gauging event
conducted in May 2018. GCLs exceedances have previously been reported in samples collected
from monitoring wells MW-1, MW-3, and MW-5. Monitoring wells MW-1 and MW-5 have not been
located since August 2014 and monitoring well MW-3 has contained measurable free product since
May 2010.

Compound concentrations in excess of the NC2LGWQS were detected in the sample collected from
water supply well WSW-8 on July 31, 2019. Compound concentrations had not been detected in
any sample collected from water supply well WSW-8 greater than the laboratory method reporting
limits in any previous sample collected. ECS returned to the site on November 21, 2019 and
collected an additional sample from water supply well WSW-8. The analytical results of the sample
collected in November 2019 did not indicate any compounds at concentrations greater than the
laboratory method reporting limits.

Results of the geophysical survey conducted by KCI indicated two potential previously unknown
USTs located to the north of the site structure.

Based on the conclusions above, ECS recommends installing free product adsorbent socks in
monitoring wells MW-3, MW-6, and MW-7 in order to further reduce the free product thicknesses in
these wells. The free product adsorbent socks would need to be removed and replaced on a bi-
Groundwater Monitoring Report
Kuntry Korner
Madison, Rockingham County, North Carolina
NCDEQ Incident No.: TF-14913
ECS Project 49:6390-A
March 18, 2020
8
monthly basis. During the installation of the initial free product adsorbent socks, ECS recommends
advancing soil borings via hand auger in the vicinity of the anomalies identified by KCI in order to
confirm the possible presence of previously unknown USTs. Due to the presence of overgrown
brush thickets, ECS recommends conducting clearing activities in order to potentially locate
monitoring wells MW-1 and MW-5 which previously contained the highest compound concentrations
at the site. In addition, ECS recommends collecting a sample from water supply well WSW-8 in
approximately three to four months (February to March 2020) to confirm the recent sampling results.

FIGURES

SOURCE:
USGS TOPOGRAPHIC MAP
ELLISBORO, NC QUADRANGLE
DATED 1971
’
FIGURE 1
USGS TOPOGRAPHIC MAP
KUNTRY KORNER
1075 BALD HILL LOOP
MADISON, NORTH CAROLINA
INCIDENT #14913
ECS PROJECT NO. 49:6390-A
SITE
APPROXIMATE SITE BOUNDARY
2,000 1,000 0
SOURCE:
ECS SKETCH AND FIELD NOTES
FIGURE 2
SITE MAP
KUNTRY KORNER
1075 BALD HILL LOOP
MADISON, NORTH CAROLINA
INCIDENT # 14913
ECS PROJECT NO. 49:6390-A
88 44 0
MW-1
MW-2
MW-3
MW-4
MW-5
MW-6
MW-7
MW-8
Existing
Building
Shed
Former UST
Locations
SOURCE:
ROCKINGHAM COUNTY GIS DEPARTMENT
AERIAL PHOTOGRAPH, DATED 2010 &
ECS FIELD OBSERVATIONS
FIGURE 3
WATER SUPPLY WELL LOCATION MAP
KUNTRY KORNER
1075 BALD HILL LOOP
MADISON, NORTH CAROLINA
INCIDENT # 14913
ECS PROJECT NO. 49:6390-A
APPROXIMATE SITE BOUNDARY
WSW-1
WSW-2
WSW-3
WSW-4
WSW-5
WSW-6
WSW-8
140 70 0
500’ Radius
WSW-7
SOURCE:
ECS SKETCH AND FIELD NOTES
FIGURE 4
GROUNDWATER ANALYTICAL MAP
KUNTRY KORNER
1075 BALD HILL LOOP
MADISON, NORTH CAROLINA
INCIDENT # 14913
ECS PROJECT NO. 49:6390-A
88 44 0
MW-1
(CNL)
MW-3
(FP)
MW-5
(CNL)
MW-6
(FP)
MW-7
(FP)
Existing
Building
Shed
MW-2
Benzene 34.3
n-Butylbenzene 13.6
Ethylbenzene 17.5
Isopropylbezene 2.1
Isopropyl Ether 2.9
Methyl tert butyl ether 122
Naphthalene 6.8
n-Propylbenzene 11.7
Styrene 0.55
Toluene 20
1,2,4-Trimethylbenzene 34.8
1,3,5-Trimethylbenzene 17
Total Xylenes 13.4
MW-4
Benzene 213
1,2-Dibromoethane 1.5J
1,2-Dichloroethane 3
Ethylbenzene 16.1
Isopropylbezene 1.6J
Isopropyl Ether 54.7
Methyl tert butyl ether 924
Naphthalene 19.4
n-Propylbenzene 2.8
Toluene 246
1,2,4-Trimethylbenzene 62.7
1,3,5-Trimethylbenzene 28.5
Total Xylenes 244
MW-8
All BRL
LEGEND
All results presented in micrograms per liter (mg/L)
Only compounds detected are shown
J = estimated concentration between reporting limit
and detection limit
Bold = Exceeds NC2LGWQS
= Approximate Geophysical Survey Anomalies
SOURCE:
ECS SKETCH AND FIELD NOTES
FIGURE 5
GROUNDWATER CONTOUR MAP
KUNTRY KORNER
1075 BALD HILL LOOP
MADISON, NORTH CAROLINA
INCIDENT # 14913
ECS PROJECT NO. 49:6390-A
88 44 0
MW-1
(CNL)
MW-2
(58.34)
MW-3
(59.67)
MW-4
(60.59)
MW-5
(CNL)
MW-6
(NA)
MW-7
(NA)
MW-8
(NA)
Existing
Building
Shed
60.5 60.0 59.5 59.0 58.5
LEGEND
Monitoring Well Location
Groundwater Contour Line
Groundwater Flow Direction

TABLES

TABLE 1
UST SYSTEM INFORMATION
Kuntry Korner
1075 Bald Hill Loop
Madison, Rockingham County, North Carolina
NCDEQ Incident No.: 14913
ECS Project No.: 49:6390-A
UST ID Contents*Volume Tank Dimensions Installation
Date Removal Date Release?
1 Gasoline 1,000 3.8' x 11.5'Unknown 03/11/96 Yes
2 Gasoline 1,000 3.8' x 11.5'Unknown 03/11/96 Yes
3 Gasoline 550 3.5' x 7.5'Unknown 03/11/96 Yes
4 Gasoline 560 4.0' x 6.0'Unknown 03/11/96 Yes
5 Gasoline 560 4.0' x 6.0'Unknown 03/11/96 Yes
Notes:
UST Information obtained from Tank Closure Assessment and Soil Boring Investiation, submitted by Geophex, Ltd. dated April 1997
* Previous contents assumed by Geophex, Ltd. Based on TPH analytical results
TABLE 2
WATER SUPPLY WELL INFORMATION
Kuntry Korner1075 Bald Hill LoopMadison, Rockingham County, North CarolinaNCDEQ Incident No.: 14913ECS Project No.: 49:6390-A
Well ID Owner Property Adress Owner’s Address Well Usage Distance from
Source Area (ft.)
WSW-1 Gerry Ashby 1061 Balld Hill Loop 7651 NC Highway 704 Inactive (Not
Sampled)119
WSW-2 Kay Collins 1051 Bald Hill Loop Road 1051 Bald Hill Loop Road Active, Sole Source 237
WSW-3 Walter Moore 1041 Bald Hill Loop Road 1041 Bald Hill Loop Road Active, Sole Source 357
WSW-4 Johnny Sparks 1056 Bald Hill Loop Road 1056 Bald Hill Loop Road Active, Sole Source 297
WSW-5 Ricky Knight 1042 Bald Hill Loop Road 1042 Bald Hill Loop Road Active, Sole Source 416
WSW-6 Melia Ann Bowman 1032 Bald Hill Loop Road 1032 Bald Hill Loop Road Active, Sole Source (Not Sampled)479
WSW-7 Ted Griffin 1022 Bald Hill Loop Road 1022 Bald Hill Loop Road Active, Sole Source 594
WSW-8 Bobby Norris 933 Baggage Road 933 Baggage Road Active, Sole Source 416
Notes:
Property information obtained from Rockingham County GIS in June 2018
All addresses are Madison, NC 27025
Municipal Water is not available
TABLE 3
MONITORING WELL CONSTRUCTION AND GROUNDWATER ELEVATION DATA
Kuntry Korner1075 Bald Hill LoopMadison, Rockingham County, North CarolinaNCDEQ Incident No.: 14913ECS Project No.: 49:6390-A
WELL ID WELL DEPTH
(ft)
TOP OF
CASING
ELEVATION (ft)
DATE
WATER
LEVEL MEASURED
DEPTH TO
WATER
(ft BTOC)
DEPTH TO
FREE PRODUCT (ft)
FREE
PRODUCT
THICKNESS (ft)
GROUNDWATER
ELEVATION (ft)
05/04/06 33.05 32.71 0.34 55.4403/09/10 45.74 ND ND 42.4610/21/11 35.26 ND ND 52.94
08/27/12 33.87 ND ND 54.3308/15/14 32.85 ND ND 55.3505/01/18 NM NM NM NM
05/04/06 34.70 34.14 0.56 56.2403/09/10 36.57 ND ND 53.89
10/21/11 37.05 ND ND 53.41
08/27/12 35.74 ND ND 54.7208/15/14 34.38 ND ND 56.08
05/01/18 NM NM NM NM
07/31/19 32.12 NM NM 58.3405/04/06 41.95 41.00 0.95 56.46
03/09/10 43.55 42.70 0.85 54.7710/21/11 NM NM ND ND08/27/12 NM NM ND ND
08/15/14 40.95 40.51 0.44 57.0205/01/18 42.07 42.06 0.08 55.5907/31/19 37.94 37.96 0.02 59.67
05/04/06 43.02 43.02 ND 56.9803/09/10 45.74 45.74 ND 54.26
10/21/11 44.65 ND ND 55.35
08/27/12 43.29 ND ND 56.7108/15/14 42.16 ND ND 57.84
05/01/18 43.08 ND ND 56.92
07/31/19 39.41 ND ND 60.5910/21/11 44.16 ND ND NM
08/27/12 43.69 ND ND NM08/15/15 42.75 ND ND NM05/01/18 NM NM NM NM
08/15/14 38.21 36.84 1.37 NM05/01/18 38.94 37.00 1.04 NM
07/31/19 34.97 35.02 0.05 NA
08/15/14 37.80 35.10 2.70 NM05/01/18 39.89 36.32 3.57 NM
07/31/19 35.62 35.71 0.09 NA
10/21/11 40.87 ND ND NM08/27/12 39.48 ND ND NM
08/15/14 38.45 ND ND NM05/01/18 39.27 ND ND NM
07/31/19 35.82 ND ND NA
Notes:
Top-of-casing elevations measured to arbitrary benchmark established at 100 feet as top-of-casing of monitoring well MW-4
ft = feet
ft BTOC = feet below top-of-casing
NM = Not Measured
ND = Not Detected
NA = Not Applicable
If free product is present, groundwater elevation calcluated as [Top-of-casing elevation - Depth to Groundwater] + [Product Thickness*0.8581]
NM50.0MW-5
NM50.0MW-7
MW-6 50.0 NM
56.0MW-1 88.20
60.0 90.46MW-2
NMNM50.0
62.0MW-3
100.0050.0MW-4
97.59
MW-8
TABLE 4
GEOCHEMICAL MEASUREMENTS
Kuntry Korner
1075 Bald Hill Loop
Madison, Rockingham County, North Carolina
NCDEQ Incident No.: 14913
ECS Project No.: 49:6390-A
Sample ID MW-1 MW-2 MW-3 MW-4 MW-5 MW-6 MW-7 MW-8
Date Sampled 07/31/19 07/31/19 07/31/19 07/31/19 07/31/19 07/31/19 07/31/19 07/31/19
pH CNL 7.05 NS-FP 4.42 CNL NS-FP NS-FP 5.72
Temperature (oC)CNL 16.31 NS-FP 17.11 CNL NS-FP NS-FP 16.13
Conductivity (mS/cm)CNL 0.102 NS-FP 0.086 CNL NS-FP NS-FP 0.124
Dissolved O2 (mg/l)CNL 4.80 NS-FP 5.03 CNL NS-FP NS-FP 6.02
Turbidity (Observed)CNL ST NS-FP T CNL NS-FP NS-FP T
Notes:
°C = degress Celsius
mS/cm = milliseimens per centimeter
mg/l = milligrams per liter
CNL = Could Not Locate
NS-FP= Not Sampled (free product)
ST= Slightly Turbid
T= Turbid
Page 1 of 3
TABLE 5SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
Kuntry Korner
1075 Bald Hill LoopMadison, Rockingham County, North CarolinaNCDEQ Incident No.: 14913ECS Project No.: 49:6390-A
Volatile Organic Compounds by Standard Method 6200B or equivalent
Benzenen-Butylbenzenesec-Butylbenzene1,2-Dibromoethane1,2-DichloroethaneEthylbenzeneIsopropylbezeneIsopropyl Etherp-IsopropyltoluneneMethyl butyl ketoneMethyl isobutyl ketoneMethyl tert butyl etherNaphthalenen-PropylbenzeneStyreneTolueneTrichloroethene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTotal XylenesNC2LGWQS 1 70 70 0.02 0.4 600 70 70 25 40 100 20 6 70 70 600 3 400 400 500
GCL 5,000 6,900 8,500 50 400 84,500 25,000 70,000 11,700 40,000 100,000 20,000 6,000 30,000 70,000 260,000 2,800 28,500 25,500 85,500
Sample
Date
Sample
ID
05/04/06 13,100 229 43.6 76 <20 <5,000 182 <5,000 NA <0.5 NA 139,000 1,800 567 <0.5 30,800 <0.5 6,600 1,120 18,600
03/09/10 20,500 <0.5 <0.5 84.1 213 1,920 68.6 1,940 NA <0.5 NA 62,600 592 204 <0.5 36,900 <0.5 1,510 384 9,100
05/02/11 23,100 <0.5 <0.5 99.9 219 2,620 82.6 1,890 <0.5 300 <0.5 55,600 451 248 <0.5 40,600 <0.5 1,960 420 13,720
07/14/11 11,800 <0.5 <0.5 <0.5 159 1,360 <0.5 864 <0.5 <0.5 <0.5 20,900 613 176 <0.5 20,300 <0.5 1,130 256 7,290
08/04/11 21,300 <0.5 <0.5 <0.5 214 2,540 <0.5 1,560 <0.5 <0.5 <0.5 42,500 847 212 <0.5 42,200 <0.5 1,510 1,210 14,490
10/21/11 24,000 <0.5 <0.5 <0.5 206 2,740 <0.5 1,540 <0.5 <0.5 15 48,800 20.4 7.4 <0.5 48,300 <0.5 1,210 469 13,410
08/27/12 19,400 <0.5 <0.5 <0.5 202 2,410 <0.5 1,100 <0.5 <0.5 <0.5 27,000 538 255 <0.5 38,800 <0.5 2,010 429 13,100
08/15/14 17,500 <0.5 <0.5 <0.5 <0.5 2,210 <0.5 850 <0.5 <5 NA 16,500 395 <0.5 <0.5 36,200 <0.5 1,640 390 10,400
05/01/18 NO SAMPLE COLLECTED - WELL NOT LOCATED
07/31/19 NO SAMPLE COLLECTED - WELL NOT LOCATED
05/04/06 80 7.48 34.4 <0.5 <0.5 122 19.7 11.6 NA <0.5 NA 186 196 38.4 <0.5 572 <0.5 348 90 726
03/09/10 20.3 1.9 <0.5 <0.5 <0.5 5.2 0.71 1.3 NA <0.5 NA 33.7 <0.5 2.1 <0.5 34.6 <0.5 18 7.2 16.2
05/02/11 NP SAMPLE COLLECTED
07/14/11 1,000 <0.5 <0.5 0.57 3.1 182 5.8 88.9 <0.5 8.6 8.4 5,300 44.8 16.9 <0.5 1,620 <0.5 122 20 557
08/04/11 128 <0.5 <0.5 <0.5 <0.5 33.3 <0.5 5.4 1.9 <0.5 <0.5 276 13.3 3.4 <0.5 210 <0.5 19.9 3.8 66.7
10/21/11 304 5.5 2 <0.5 1.2 117 5 18 <0.5 <0.5 15 862 20.4 7.4 <0.5 546 <0.5 57.7 8.6 224.9
08/27/12 534 <0.5 <0.5 <0.5 <0.5 150 5.4 15.9 <0.5 <0.5 <0.5 1,510 53.7 14.6 <0.5 706 <0.5 79.3 5.1 178
08/15/14 312 1.19 0.55 <0.5 1.21 71.5 4 20.9 <0.5 <5 NA 1,660 41.8 10.4 <0.5 189 <0.5 10.5 1.79 61.8
05/01/18 NO SAMPLE COLLECTED - WELL NOT LOCATED
07/31/19 34.3 13.6 <0.5 <0.5 <0.5 17.5 2.1 2.9 <0.5 <0.5 <0.5 122 6.8 11.7 0.55 20 <0.5 34.8 17 13.4
05/04/06 13,600 883 142 240 <50 3,240 242 1,630 NA <0.5 NA 12,400 <2,000 1,110 <0.5 39,600 <0.5 2,080 <2,000 17,580
03/09/10 NO SAMPLE COLLECTED - FREE PRODUCT PRESENT
05/02/11 NO SAMPLE COLLECTED - FREE PRODUCT PRESENT
07/14/11 NO SAMPLE COLLECTED - FREE PRODUCT PRESENT
08/04/11 NO SAMPLE COLLECTED - FREE PRODUCT PRESENT
10/21/11 NO SAMPLE COLLECTED - FREE PRODUCT PRESENT
08/27/12 NO SAMPLE COLLECTED - FREE PRODUCT PRESENT
08/15/14 NO SAMPLE COLLECTED - FREE PRODUCT PRESENT
05/01/18 NO SAMPLE COLLECTED - FREE PRODUCT PRESENT
07/31/19 NO SAMPLE COLLECTED - FREE PRODUCT PRESENT
MW-1
MW-2
MW-3
Page 2 of 3
TABLE 5SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
Kuntry Korner
1075 Bald Hill LoopMadison, Rockingham County, North CarolinaNCDEQ Incident No.: 14913ECS Project No.: 49:6390-A
Volatile Organic Compounds by Standard Method 6200B or equivalent
Benzenen-Butylbenzenesec-Butylbenzene1,2-Dibromoethane1,2-DichloroethaneEthylbenzeneIsopropylbezeneIsopropyl Etherp-IsopropyltoluneneMethyl butyl ketoneMethyl isobutyl ketoneMethyl tert butyl etherNaphthalenen-PropylbenzeneStyreneTolueneTrichloroethene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTotal XylenesNC2LGWQS 1 70 70 0.02 0.4 600 70 70 25 40 100 20 6 70 70 600 3 400 400 500
GCL 5,000 6,900 8,500 50 400 84,500 25,000 70,000 11,700 40,000 100,000 20,000 6,000 30,000 70,000 260,000 2,800 28,500 25,500 85,500
Sample
Date
Sample
ID
05/04/06 2,240 <32 <32 <32 <32 85 <32 544 NA <0.5 NA 11,100 381 <32 <0.5 1,380 <0.5 209 111 1,412
03/09/10 1,580 4.2 1.1 6.6 16.1 72 4.5 140 NA <0.5 NA 2,930 8.2 7.5 <0.5 1,460 <0.5 118 74.8 883
05/02/11 493 <0.5 <0.5 3.5 9.2 28.1 2.1 58.2 <0.5 <0.5 9 1,330 23.9 5.3 <0.5 293 <0.5 83.2 50 374
07/14/11 365 <0.5 <0.5 <0.5 7.7 13.8 <0.5 45.2 <0.5 <0.5 <0.5 1,090 34.8 <0.5 <0.5 202 <0.5 38.1 22.2 203.9
08/04/11 276 <0.5 <0.5 1.7 5.1 3.7 <0.5 39.9 <0.5 <0.5 <0.5 812 10.8 <0.5 <0.5 89.1 <0.5 28.1 23.5 181.2
10/21/11 1,020 <0.5 2.2 5.1 22.7 25.7 6.1 162 4.4 <0.5 21.4 3,270 28.4 4.5 <0.5 282 <0.5 118 73.1 486
08/27/12 733 <0.5 <0.5 <0.5 <0.5 28.2 <0.5 126 <0.5 <0.5 <0.5 2,650 37.5 6.1 <0.5 318 <0.5 103 55.3 424
08/15/14 911 <0.5 0.75 1.98 7.89 26.3 2.77 106 0.98 <5 NA 2,040 22.5 2.7 <0.5 606 <0.5 88.5 47.2 <0.5
05/01/18 2,600 <0.5 <0.5 <0.5 32 250 11 310 <0.5 <5 <0.5 6,500 89 27 <0.5 3,800 <0.5 270 130 1,400
07/31/19 213 <0.5 <0.5 1.5J 3 16.1 1.6J 54.7 <0.5 <0.5 <0.5 924 19.4 2.8 <0.5 246 <0.5 62.7 28.5 244
07/14/11 4,220 <0.5 <0.5 7.2 36.4 578 18.4 335 <0.5 108 <0.5 6,980 164 60.9 <0.5 6,960 <0.5 524 128 3,040
08/04/11 1,450 <0.5 <0.5 <0.5 15.3 196 <0.5 112 16.9 <0.5 <0.5 2,370 91.9 18.2 <0.5 2,440 11.6 136 43.7 1,188
10/21/11 230 2.9 0.94 <0.5 2.7 18.2 2.4 36.8 2.2 <0.5 <0.5 707 7.9 1.6 <0.5 204 <0.5 13.2 5.2 102.7
08/27/12 698 <0.5 <0.5 <0.5 9.5 121 5.6 88.4 <0.5 <0.5 <0.5 1,260 36.7 12.7 <0.5 774 <0.5 106 27.1 713
08/15/14 6,720 <0.5 <0.5 <0.5 188 842 <0.5 682 <0.5 <5 NA 24,400 192 <0.5 <0.5 8,500 <0.5 630 180 4,130
05/01/18 NO SAMPLE COLLECTED - WELL NOT LOCATED
07/31/19 NO SAMPLE COLLECTED - WELL NOT LOCATED
10/21/11 NO SAMPLE COLLECTED - FREE PRODUCT PRESENT
08/27/12 NO SAMPLE COLLECTED - FREE PRODUCT PRESENT
08/15/14 NO SAMPLE COLLECTED - FREE PRODUCT PRESENT
05/01/18 NO SAMPLE COLLECTED - FREE PRODUCT PRESENT
07/31/19 NO SAMPLE COLLECTED - FREE PRODUCT PRESENT
10/21/11 NO SAMPLE COLLECTED - FREE PRODUCT PRESENT
08/27/12 NO SAMPLE COLLECTED - FREE PRODUCT PRESENT
08/15/14 NO SAMPLE COLLECTED - FREE PRODUCT PRESENT
05/01/18 NO SAMPLE COLLECTED - FREE PRODUCT PRESENT
07/31/19 NO SAMPLE COLLECTED - FREE PRODUCT PRESENT
MW-5
MW-6
MW-7
MW-4
Page 3 of 3
TABLE 5SUMMARY OF GROUNDWATER ANALYTICAL RESULTS
Kuntry Korner
1075 Bald Hill LoopMadison, Rockingham County, North CarolinaNCDEQ Incident No.: 14913ECS Project No.: 49:6390-A
Volatile Organic Compounds by Standard Method 6200B or equivalent
Benzenen-Butylbenzenesec-Butylbenzene1,2-Dibromoethane1,2-DichloroethaneEthylbenzeneIsopropylbezeneIsopropyl Etherp-IsopropyltoluneneMethyl butyl ketoneMethyl isobutyl ketoneMethyl tert butyl etherNaphthalenen-PropylbenzeneStyreneTolueneTrichloroethene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTotal XylenesNC2LGWQS 1 70 70 0.02 0.4 600 70 70 25 40 100 20 6 70 70 600 3 400 400 500
GCL 5,000 6,900 8,500 50 400 84,500 25,000 70,000 11,700 40,000 100,000 20,000 6,000 30,000 70,000 260,000 2,800 28,500 25,500 85,500
Sample
Date
Sample
ID
10/21/11 1,740 <0.5 9.9 <0.5 54.5 12.1 25.3 156 <0.5 <0.5 <0.5 1,580 80.9 7.9 <0.5 39.2 <0.5 49.5 12.1 165.5
08/27/12 770 <0.5 <0.5 <0.5 33 6.2 8.2 110 <0.5 <0.5 <0.5 1,030 51.7 <0.5 <0.5 17.5 <0.5 32.2 <0.5 60.1
08/15/14 220 <0.5 <0.5 <0.5 10.4 18.8 4.75 62 <0.5 <5 NA 555 19 4.5 <0.5 62.4 <0.5 25.1 9.05 84.6
05/01/18 16 <0.5 0.62 <0.5 <0.5 <0.5 1.2 34 <0.5 <0.5 <0.5 340 1.8 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5
07/31/19 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <2.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.5
Notes:
Results presented in micrograms per liter (µg/l)
Only compounds detected are shown
NC2LGWQS = North Carolina 2L Groundwater Quality Standards
GCL = Gross Contamination Levels
J = Estimated concentration detected between method reporting limit and detection limit
NA = Not analyzed for compound
VALUE = compound exceeds laboratory method reporting limits
VALUE = compound exceeds NC2LGWQS
VALUE = compound exceeds GCL
MW-8
Page 1 of 2
TABLE 6
SUMMARY OF WATER SUPPLY WELL ANALYTICAL RESULTS
Kuntry Korner
1075 Bald Hill Loop
Madison, Rockingham County, North CarolinaNCDEQ Incident No.: 14913ECS Project No.: 49:6390-A
Volatile Organic Compounds by Standard Method 6200B or equivalent
Benzene1,2-DichloroethaneEthylbenzeneIsopropylbenzeneIsopropyl EtherMethyl tert butyl ethern-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTotal XylenesNC2LGWQS 1 0.4 600 70 70 20 70 600 400 400 500
GCL 5,000 400 84,500 25,000 70,000 20,000 30,000 260,000 28,500 25,500 85,500
Sample ID Sample Date
12/13/01 <1 ---<1 ---<1 <1 ---<1 ------<1
04/04/03 <1 ---<1 ---8 59.7 ---<1 ------<1
10/08/03 <1 ---<1 ---<5 <5 ---<1 ------<3
05/05/04 <1 ---<1 ---<5 <5 ---<1 ------<3
05/04/06 <1 ---<1 ---<1 <2 ---<1 ------<4
03/21/95 <1 ---<1 ---NA 41 ---<1 ------<1
07/08/99 <1 ---<1 ---NA 17.3 ---<1 ------<1
02/08/00 <1 ---<1 ---NA 24.3 ---<1 ------<1
03/29/00 <1 ---<1 ---NA <1 ---<1 ------<1
09/12/01 <1 ---<1 ---1.3 6.3 ---<1 ------<1
10/08/03 <1 ---<1 ---1.6 5 ---<1 ------<1
05/05/04 <1 ---<1 ---<5 5.2 ---<1 ------<1
05/04/06 <1 ---<1 ---5.76 3.54 ---<1 ------<1
03/09/10 <1 ---<1 ---1.9 3.4 ---<1 ------<1
08/04/11 ND ---ND ---ND 0.96 ---ND ------ND
08/27/12 <0.5 ---<0.5 ---ND ND ---<0.5 ------<1.5
08/18/14 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1
05/01/18 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1
07/31/19 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.5
07/08/99 <1 ---<1 ---NA <1 ---<1 ------<1
02/08/00 <1 ---<1 ---NA 42.7 ---<1 ------<1
03/29/00 <1 ---<1 ---NA 43.5 ---<1 ------<1
09/12/01 <1 ---<1 ---3.3 29.9 ---<1 ------<1
04/04/03 <1 ---<1 ---<1 <1 ---<1 ------<1
10/08/03 <1 ---<1 ---21 100 ---<1 ------<3
05/05/04 <1 ---<1 ---3.4J 43 ---<1 ------<3
05/04/06 <1 ---<1 ---<1 <2 ---<1 ------<4
03/09/10 <0.5 ---<0.5 ---<0.5 <0.5 ---<0.5 ------<1.6
08/18/14 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1
05/01/18 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1
07/31/19 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.5
07/08/99 <1 ---<1 ---NS <1 ---<1 ------<1
03/29/00 <1 ---<1 ---NS <1 ---<1 ------<1
09/12/01 <1 ---<1 ---<1 <1 ---<1 ------<1
08/22/14 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1
05/01/18 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1
07/31/19 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.5
03/29/00 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1
09/12/01 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1
08/22/14 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1
05/01/18 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1
WSW-1
WSW-5
WSW-2
WSW-3
WSW-4
Page 2 of 2
TABLE 6
SUMMARY OF WATER SUPPLY WELL ANALYTICAL RESULTS
Kuntry Korner
1075 Bald Hill Loop
Madison, Rockingham County, North CarolinaNCDEQ Incident No.: 14913ECS Project No.: 49:6390-A
Volatile Organic Compounds by Standard Method 6200B or equivalent
Benzene1,2-DichloroethaneEthylbenzeneIsopropylbenzeneIsopropyl EtherMethyl tert butyl ethern-PropylbenzeneToluene1,2,4-Trimethylbenzene1,3,5-TrimethylbenzeneTotal XylenesNC2LGWQS 1 0.4 600 70 70 20 70 600 400 400 500
GCL 5,000 400 84,500 25,000 70,000 20,000 30,000 260,000 28,500 25,500 85,500
Sample ID Sample Date
08/15/14 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1
05/01/18 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1
07/31/19 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.5
08/15/14 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1
05/01/18 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1
07/31/19 10.9 3.0 6.4 1.6 25.5 320 2.5 5.3 8.1 4.5 18.9
11/21/19 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1.5
Notes:
Results presented in micrograms per liter (µg/l)
Only compounds detected are shown
NC2LGWQS = North Carolina 2L Groundwater Quality Standards
GCL = Gross Contamination Levels
NA = Not analyzed for compound
--- = Not previously reported
VALUE = compound exceeds laboratory method reporting limits
VALUE = compound exceeds NC2LGWQS
VALUE = compound exceeds GCL
WSW-8
WSW-7

APPENDIX A

PHOTOGRAPH LOG
KUNTRY KORNER
1075 BALD HILL LOOP
MADISON, ROCKINGHAM COUNTY, NORTH CAROLINA
ECS PROJECT NO. 49-6390
Photograph 1: View of the Site
Photograph 2: View of monitoring well MW-4
PHOTOGRAPH LOG
KUNTRY KORNER
1075 BALD HILL LOOP
MADISON, ROCKINGHAM COUNTY, NORTH CAROLINA
ECS PROJECT NO. 49-6390
Photograph 3: View of monitoring well MW-3
Photograph 4: View of monitoring well MW-6
PHOTOGRAPH LOG
KUNTRY KORNER
1075 BALD HILL LOOP
MADISON, ROCKINGHAM COUNTY, NORTH CAROLINA
ECS PROJECT NO. 49-6390
Photograph 5: View of monitoring well MW-7
Photograph 6: View of monitoring well MW-8
PHOTOGRAPH LOG
KUNTRY KORNER
1075 BALD HILL LOOP
MADISON, ROCKINGHAM COUNTY, NORTH CAROLINA
ECS PROJECT NO. 49-6390
Photograph 7: View of where MW-5 is supposed to be located

APPENDIX B

SUE Printable Web Map
Esri, HERE, Garmin, (c) OpenStreetMap contributors, Esri, HERE,
Garmin, (c) OpenStreetMap contributors, and the GIS user
community, Source: Esri, DigitalGlobe, GeoEye, Earthstar
Geographics, CNES/Airbus DS, USDA, USGS, AeroGRID, IGN, and
SUE_Layers_New - Structures_Point
Hand Hole
Utility Pole
SUE_Layers_New - Utilities
Unknown
Telephone
Cable Television
Gas
10/30/2019 10:25:50 AM
0 0.01 0.020.01 mi
0 0.01 0.030.01 km
1:564
Web AppBuilder for ArcGIS
KCI Associates of NC

APPENDIX C

#=CL#
August 08, 2019
LIMS USE: FR - ASHLEY BARHAM
LIMS OBJECT ID: 92439770
92439770
Project:
Pace Project No.:
RE:
Ashley Barham
ECS Southeast, LLP
4811 Koger Boulevard
Greensboro, NC 27407
NCDEQ KUNTRY KORNER
Dear Ashley Barham:
Enclosed are the analytical results for sample(s) received by the laboratory on August 02, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Taylor Ezell
[e-mail]
Project Manager
[phone]
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
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Page 1 of 41
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 2 of 41
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Lab ID Sample ID Matrix Date Collected Date Received
92439770001 MW-2 Water 07/31/19 17:10 08/02/19 10:51
92439770002 MW-4 Water 07/31/19 13:40 08/02/19 10:51
92439770003 MW-8 Water 07/31/19 14:40 08/02/19 10:51
92439770004 WSW-2 Water 07/31/19 15:50 08/02/19 10:51
92439770005 WSW-3 Water 07/31/19 15:55 08/02/19 10:51
92439770006 WSW-4 Water 07/31/19 16:05 08/02/19 10:51
92439770007 WSW-7 Water 07/31/19 16:20 08/02/19 10:51
92439770008 WSW-8 Water 07/31/19 15:35 08/02/19 10:51
REPORT OF LABORATORY ANALYSIS
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Page 3 of 41
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92439770001 MW-2 SM 6200B 63 PASI-CGAW
92439770002 MW-4 SM 6200B 63 PASI-CGAW
92439770003 MW-8 SM 6200B 63 PASI-CGAW
92439770004 WSW-2 SM 6200B 63 PASI-CCL
92439770005 WSW-3 SM 6200B 63 PASI-CCL
92439770006 WSW-4 SM 6200B 63 PASI-CCL
92439770007 WSW-7 SM 6200B 63 PASI-CCL
92439770008 WSW-8 SM 6200B 63 PASI-CGAW
REPORT OF LABORATORY ANALYSIS
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Page 4 of 41
#=HO#
SUMMARY OF DETECTION
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Parameters AnalyzedResult
Lab Sample ID
Report Limit QualifiersUnitsMethod
Client Sample ID
92439770001 MW-2
Benzene 34.3 ug/L 08/06/19 19:120.50SM 6200B
n-Butylbenzene 13.6 ug/L 08/06/19 19:120.50SM 6200B
Diisopropyl ether 2.9 ug/L 08/06/19 19:120.50SM 6200B
Ethylbenzene 17.5 ug/L 08/06/19 19:120.50SM 6200B
Isopropylbenzene (Cumene)2.1 ug/L 08/06/19 19:120.50SM 6200B
Methyl-tert-butyl ether 122 ug/L 08/06/19 19:120.50SM 6200B
Naphthalene 6.8 ug/L 08/06/19 19:122.0SM 6200B
n-Propylbenzene 11.7 ug/L 08/06/19 19:120.50SM 6200B
Styrene 0.55 ug/L 08/06/19 19:120.50SM 6200B
Toluene 20.0 ug/L 08/06/19 19:120.50SM 6200B
1,2,4-Trimethylbenzene 34.8 ug/L 08/06/19 19:120.50SM 6200B
1,3,5-Trimethylbenzene 17.0 ug/L 08/06/19 19:120.50SM 6200B
m&p-Xylene 9.3 ug/L 08/06/19 19:121.0SM 6200B
o-Xylene 4.1 ug/L 08/06/19 19:120.50SM 6200B
92439770002 MW-4
Benzene 213 ug/L 08/07/19 10:222.5SM 6200B
1,2-Dibromoethane (EDB)1.5J ug/L 08/07/19 10:222.5SM 6200B
1,2-Dichloroethane 3.0 ug/L 08/07/19 10:222.5SM 6200B
Diisopropyl ether 54.7 ug/L 08/07/19 10:222.5SM 6200B
Ethylbenzene 16.1 ug/L 08/07/19 10:222.5SM 6200B
Isopropylbenzene (Cumene)1.6J ug/L 08/07/19 10:222.5SM 6200B
Methyl-tert-butyl ether 924 ug/L 08/07/19 10:222.5SM 6200B
Naphthalene 19.4 ug/L 08/07/19 10:2210.0SM 6200B
n-Propylbenzene 2.8 ug/L 08/07/19 10:222.5SM 6200B
Toluene 246 ug/L 08/07/19 10:222.5SM 6200B
1,2,4-Trimethylbenzene 62.7 ug/L 08/07/19 10:222.5SM 6200B
1,3,5-Trimethylbenzene 28.5 ug/L 08/07/19 10:222.5SM 6200B
m&p-Xylene 159 ug/L 08/07/19 10:225.0SM 6200B
o-Xylene 85.0 ug/L 08/07/19 10:222.5SM 6200B
92439770008 WSW-8
Benzene 10.9 ug/L 08/07/19 06:411.2SM 6200B
1,2-Dichloroethane 3.0 ug/L 08/07/19 06:411.2SM 6200B
Diisopropyl ether 25.5 ug/L 08/07/19 06:411.2SM 6200B
Ethylbenzene 6.4 ug/L 08/07/19 06:411.2SM 6200B
Isopropylbenzene (Cumene)1.6 ug/L 08/07/19 06:411.2SM 6200B
Methyl-tert-butyl ether 320 ug/L 08/07/19 06:411.2SM 6200B
n-Propylbenzene 2.5 ug/L 08/07/19 06:411.2SM 6200B
Toluene 5.3 ug/L 08/07/19 06:411.2SM 6200B
1,2,4-Trimethylbenzene 8.1 ug/L 08/07/19 06:411.2SM 6200B
1,3,5-Trimethylbenzene 4.5 ug/L 08/07/19 06:411.2SM 6200B
m&p-Xylene 13.0 ug/L 08/07/19 06:412.5SM 6200B
o-Xylene 5.9 ug/L 08/07/19 06:411.2SM 6200B
REPORT OF LABORATORY ANALYSIS
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Page 5 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Sample: MW-2 Lab ID: 92439770001 Collected: 07/31/19 17:10 Received: 08/02/19 10:51 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene 34.3 ug/L 08/06/19 19:12 71-43-20.50 0.25 1
Bromobenzene ND ug/L 08/06/19 19:12 108-86-10.50 0.25 1
Bromochloromethane ND ug/L 08/06/19 19:12 74-97-50.50 0.25 1
Bromodichloromethane ND ug/L 08/06/19 19:12 75-27-40.50 0.25 1
Bromoform ND ug/L 08/06/19 19:12 75-25-20.50 0.25 1
Bromomethane ND ug/L 08/06/19 19:12 74-83-95.0 2.5 1
n-Butylbenzene 13.6 ug/L 08/06/19 19:12 104-51-80.50 0.25 1
sec-Butylbenzene ND ug/L 08/06/19 19:12 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 08/06/19 19:12 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 08/06/19 19:12 56-23-50.50 0.25 1
Chlorobenzene ND ug/L 08/06/19 19:12 108-90-70.50 0.25 1
Chloroethane ND ug/L 08/06/19 19:12 75-00-31.0 0.50 1
Chloroform ND ug/L 08/06/19 19:12 67-66-35.0 2.5 1
Chloromethane ND ug/L 08/06/19 19:12 74-87-31.0 0.50 1
2-Chlorotoluene ND ug/L 08/06/19 19:12 95-49-80.50 0.25 1
4-Chlorotoluene ND ug/L 08/06/19 19:12 106-43-40.50 0.25 1
1,2-Dibromo-3-chloropropane ND ug/L 08/06/19 19:12 96-12-81.0 0.50 1
Dibromochloromethane ND ug/L 08/06/19 19:12 124-48-10.50 0.25 1
1,2-Dibromoethane (EDB)ND ug/L 08/06/19 19:12 106-93-40.50 0.25 1
Dibromomethane ND ug/L 08/06/19 19:12 74-95-30.50 0.25 1
1,2-Dichlorobenzene ND ug/L 08/06/19 19:12 95-50-10.50 0.25 1
1,3-Dichlorobenzene ND ug/L 08/06/19 19:12 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 08/06/19 19:12 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 08/06/19 19:12 75-71-80.50 0.25 1
1,1-Dichloroethane ND ug/L 08/06/19 19:12 75-34-30.50 0.25 1
1,2-Dichloroethane ND ug/L 08/06/19 19:12 107-06-20.50 0.25 1
1,1-Dichloroethene ND ug/L 08/06/19 19:12 75-35-40.50 0.25 1
cis-1,2-Dichloroethene ND ug/L 08/06/19 19:12 156-59-20.50 0.25 1
trans-1,2-Dichloroethene ND ug/L 08/06/19 19:12 156-60-50.50 0.25 1
1,2-Dichloropropane ND ug/L 08/06/19 19:12 78-87-50.50 0.25 1
1,3-Dichloropropane ND ug/L 08/06/19 19:12 142-28-90.50 0.25 1
2,2-Dichloropropane ND ug/L 08/06/19 19:12 594-20-70.50 0.25 1
1,1-Dichloropropene ND ug/L 08/06/19 19:12 563-58-60.50 0.25 1
cis-1,3-Dichloropropene ND ug/L 08/06/19 19:12 10061-01-50.50 0.25 1
trans-1,3-Dichloropropene ND ug/L 08/06/19 19:12 10061-02-60.50 0.25 1
Diisopropyl ether 2.9 ug/L 08/06/19 19:12 108-20-30.50 0.25 1
Ethylbenzene 17.5 ug/L 08/06/19 19:12 100-41-40.50 0.25 1
Hexachloro-1,3-butadiene ND ug/L 08/06/19 19:12 87-68-32.0 1.0 1
Isopropylbenzene (Cumene)2.1 ug/L 08/06/19 19:12 98-82-80.50 0.25 1
Methylene Chloride ND ug/L 08/06/19 19:12 75-09-22.0 1.0 1
Methyl-tert-butyl ether 122 ug/L 08/06/19 19:12 1634-04-40.50 0.25 1
Naphthalene 6.8 ug/L 08/06/19 19:12 91-20-32.0 1.0 1
n-Propylbenzene 11.7 ug/L 08/06/19 19:12 103-65-10.50 0.25 1
Styrene 0.55 ug/L 08/06/19 19:12 100-42-50.50 0.25 1
1,1,1,2-Tetrachloroethane ND ug/L 08/06/19 19:12 630-20-60.50 0.25 1
1,1,2,2-Tetrachloroethane ND ug/L 08/06/19 19:12 79-34-50.50 0.25 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
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Page 6 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Sample: MW-2 Lab ID: 92439770001 Collected: 07/31/19 17:10 Received: 08/02/19 10:51 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 08/06/19 19:12 127-18-40.50 0.25 1
Toluene 20.0 ug/L 08/06/19 19:12 108-88-30.50 0.25 1
1,2,3-Trichlorobenzene ND ug/L 08/06/19 19:12 87-61-62.0 1.0 1
1,2,4-Trichlorobenzene ND ug/L 08/06/19 19:12 120-82-12.0 1.0 1
1,1,1-Trichloroethane ND ug/L 08/06/19 19:12 71-55-60.50 0.25 1
1,1,2-Trichloroethane ND ug/L 08/06/19 19:12 79-00-50.50 0.25 1
Trichloroethene ND ug/L 08/06/19 19:12 79-01-60.50 0.25 1
Trichlorofluoromethane ND ug/L 08/06/19 19:12 75-69-41.0 0.50 1
1,2,3-Trichloropropane ND ug/L 08/06/19 19:12 96-18-40.50 0.25 1
1,2,4-Trimethylbenzene 34.8 ug/L 08/06/19 19:12 95-63-60.50 0.25 1
1,3,5-Trimethylbenzene 17.0 ug/L 08/06/19 19:12 108-67-80.50 0.25 1
Vinyl chloride ND ug/L 08/06/19 19:12 75-01-41.0 0.50 1
m&p-Xylene 9.3 ug/L 08/06/19 19:12 179601-23-11.0 0.50 1
o-Xylene 4.1 ug/L 08/06/19 19:12 95-47-60.50 0.25 1
Surrogates
1,2-Dichloroethane-d4 (S)93 %08/06/19 19:12 17060-07-070-130 1
4-Bromofluorobenzene (S)95 %08/06/19 19:12 460-00-470-130 1
Toluene-d8 (S)96 %08/06/19 19:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
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Page 7 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Sample: MW-4 Lab ID: 92439770002 Collected: 07/31/19 13:40 Received: 08/02/19 10:51 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene 213 ug/L 08/07/19 10:22 71-43-22.5 1.2 5
Bromobenzene ND ug/L 08/07/19 10:22 108-86-12.5 1.2 5
Bromochloromethane ND ug/L 08/07/19 10:22 74-97-52.5 1.2 5
Bromodichloromethane ND ug/L 08/07/19 10:22 75-27-42.5 1.2 5
Bromoform ND ug/L 08/07/19 10:22 75-25-22.5 1.2 5
Bromomethane ND ug/L 08/07/19 10:22 74-83-925.0 12.5 5
n-Butylbenzene ND ug/L 08/07/19 10:22 104-51-82.5 1.2 5
sec-Butylbenzene ND ug/L 08/07/19 10:22 135-98-82.5 1.2 5
tert-Butylbenzene ND ug/L 08/07/19 10:22 98-06-62.5 1.2 5
Carbon tetrachloride ND ug/L 08/07/19 10:22 56-23-52.5 1.2 5
Chlorobenzene ND ug/L 08/07/19 10:22 108-90-72.5 1.2 5
Chloroethane ND ug/L 08/07/19 10:22 75-00-35.0 2.5 5
Chloroform ND ug/L 08/07/19 10:22 67-66-325.0 12.5 5
Chloromethane ND ug/L 08/07/19 10:22 74-87-35.0 2.5 5
2-Chlorotoluene ND ug/L 08/07/19 10:22 95-49-82.5 1.2 5
4-Chlorotoluene ND ug/L 08/07/19 10:22 106-43-42.5 1.2 5
1,2-Dibromo-3-chloropropane ND ug/L 08/07/19 10:22 96-12-85.0 2.5 5
Dibromochloromethane ND ug/L 08/07/19 10:22 124-48-12.5 1.2 5
1,2-Dibromoethane (EDB)1.5J ug/L 08/07/19 10:22 106-93-42.5 1.2 5
Dibromomethane ND ug/L 08/07/19 10:22 74-95-32.5 1.2 5
1,2-Dichlorobenzene ND ug/L 08/07/19 10:22 95-50-12.5 1.2 5
1,3-Dichlorobenzene ND ug/L 08/07/19 10:22 541-73-12.5 1.2 5
1,4-Dichlorobenzene ND ug/L 08/07/19 10:22 106-46-72.5 1.2 5
Dichlorodifluoromethane ND ug/L 08/07/19 10:22 75-71-82.5 1.2 5
1,1-Dichloroethane ND ug/L 08/07/19 10:22 75-34-32.5 1.2 5
1,2-Dichloroethane 3.0 ug/L 08/07/19 10:22 107-06-22.5 1.2 5
1,1-Dichloroethene ND ug/L 08/07/19 10:22 75-35-42.5 1.2 5
cis-1,2-Dichloroethene ND ug/L 08/07/19 10:22 156-59-22.5 1.2 5
trans-1,2-Dichloroethene ND ug/L 08/07/19 10:22 156-60-52.5 1.2 5
1,2-Dichloropropane ND ug/L 08/07/19 10:22 78-87-52.5 1.2 5
1,3-Dichloropropane ND ug/L 08/07/19 10:22 142-28-92.5 1.2 5
2,2-Dichloropropane ND ug/L 08/07/19 10:22 594-20-72.5 1.2 5
1,1-Dichloropropene ND ug/L 08/07/19 10:22 563-58-62.5 1.2 5
cis-1,3-Dichloropropene ND ug/L 08/07/19 10:22 10061-01-52.5 1.2 5
trans-1,3-Dichloropropene ND ug/L 08/07/19 10:22 10061-02-62.5 1.2 5
Diisopropyl ether 54.7 ug/L 08/07/19 10:22 108-20-32.5 1.2 5
Ethylbenzene 16.1 ug/L 08/07/19 10:22 100-41-42.5 1.2 5
Hexachloro-1,3-butadiene ND ug/L 08/07/19 10:22 87-68-310.0 5.0 5
Isopropylbenzene (Cumene)1.6J ug/L 08/07/19 10:22 98-82-82.5 1.2 5
Methylene Chloride ND ug/L 08/07/19 10:22 75-09-210.0 5.0 5
Methyl-tert-butyl ether 924 ug/L 08/07/19 10:22 1634-04-42.5 1.2 5
Naphthalene 19.4 ug/L 08/07/19 10:22 91-20-310.0 5.0 5
n-Propylbenzene 2.8 ug/L 08/07/19 10:22 103-65-12.5 1.2 5
Styrene ND ug/L 08/07/19 10:22 100-42-52.5 1.2 5
1,1,1,2-Tetrachloroethane ND ug/L 08/07/19 10:22 630-20-62.5 1.2 5
1,1,2,2-Tetrachloroethane ND ug/L 08/07/19 10:22 79-34-52.5 1.2 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
Pace Analytical Services, LLC
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Page 8 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Sample: MW-4 Lab ID: 92439770002 Collected: 07/31/19 13:40 Received: 08/02/19 10:51 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 08/07/19 10:22 127-18-42.5 1.2 5
Toluene 246 ug/L 08/07/19 10:22 108-88-32.5 1.2 5
1,2,3-Trichlorobenzene ND ug/L 08/07/19 10:22 87-61-610.0 5.0 5
1,2,4-Trichlorobenzene ND ug/L 08/07/19 10:22 120-82-110.0 5.0 5
1,1,1-Trichloroethane ND ug/L 08/07/19 10:22 71-55-62.5 1.2 5
1,1,2-Trichloroethane ND ug/L 08/07/19 10:22 79-00-52.5 1.2 5
Trichloroethene ND ug/L 08/07/19 10:22 79-01-62.5 1.2 5
Trichlorofluoromethane ND ug/L 08/07/19 10:22 75-69-45.0 2.5 5
1,2,3-Trichloropropane ND ug/L 08/07/19 10:22 96-18-42.5 1.2 5
1,2,4-Trimethylbenzene 62.7 ug/L 08/07/19 10:22 95-63-62.5 1.2 5
1,3,5-Trimethylbenzene 28.5 ug/L 08/07/19 10:22 108-67-82.5 1.2 5
Vinyl chloride ND ug/L 08/07/19 10:22 75-01-45.0 2.5 5
m&p-Xylene 159 ug/L 08/07/19 10:22 179601-23-15.0 2.5 5
o-Xylene 85.0 ug/L 08/07/19 10:22 95-47-62.5 1.2 5
Surrogates
1,2-Dichloroethane-d4 (S)96 %08/07/19 10:22 17060-07-070-130 5
4-Bromofluorobenzene (S)96 %08/07/19 10:22 460-00-470-130 5
Toluene-d8 (S)103 %08/07/19 10:22 2037-26-570-130 5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Sample: MW-8 Lab ID: 92439770003 Collected: 07/31/19 14:40 Received: 08/02/19 10:51 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 08/07/19 10:04 71-43-20.50 0.25 1
Bromobenzene ND ug/L 08/07/19 10:04 108-86-10.50 0.25 1
Bromochloromethane ND ug/L 08/07/19 10:04 74-97-50.50 0.25 1
Bromodichloromethane ND ug/L 08/07/19 10:04 75-27-40.50 0.25 1
Bromoform ND ug/L 08/07/19 10:04 75-25-20.50 0.25 1
Bromomethane ND ug/L 08/07/19 10:04 74-83-95.0 2.5 1
n-Butylbenzene ND ug/L 08/07/19 10:04 104-51-80.50 0.25 1
sec-Butylbenzene ND ug/L 08/07/19 10:04 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 08/07/19 10:04 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 08/07/19 10:04 56-23-50.50 0.25 1
Chlorobenzene ND ug/L 08/07/19 10:04 108-90-70.50 0.25 1
Chloroethane ND ug/L 08/07/19 10:04 75-00-31.0 0.50 1
Chloroform ND ug/L 08/07/19 10:04 67-66-35.0 2.5 1
Chloromethane ND ug/L 08/07/19 10:04 74-87-31.0 0.50 1
2-Chlorotoluene ND ug/L 08/07/19 10:04 95-49-80.50 0.25 1
4-Chlorotoluene ND ug/L 08/07/19 10:04 106-43-40.50 0.25 1
1,2-Dibromo-3-chloropropane ND ug/L 08/07/19 10:04 96-12-81.0 0.50 1
Dibromochloromethane ND ug/L 08/07/19 10:04 124-48-10.50 0.25 1
1,2-Dibromoethane (EDB)ND ug/L 08/07/19 10:04 106-93-40.50 0.25 1
Dibromomethane ND ug/L 08/07/19 10:04 74-95-30.50 0.25 1
1,2-Dichlorobenzene ND ug/L 08/07/19 10:04 95-50-10.50 0.25 1
1,3-Dichlorobenzene ND ug/L 08/07/19 10:04 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 08/07/19 10:04 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 08/07/19 10:04 75-71-80.50 0.25 1
1,1-Dichloroethane ND ug/L 08/07/19 10:04 75-34-30.50 0.25 1
1,2-Dichloroethane ND ug/L 08/07/19 10:04 107-06-20.50 0.25 1
1,1-Dichloroethene ND ug/L 08/07/19 10:04 75-35-40.50 0.25 1
cis-1,2-Dichloroethene ND ug/L 08/07/19 10:04 156-59-20.50 0.25 1
trans-1,2-Dichloroethene ND ug/L 08/07/19 10:04 156-60-50.50 0.25 1
1,2-Dichloropropane ND ug/L 08/07/19 10:04 78-87-50.50 0.25 1
1,3-Dichloropropane ND ug/L 08/07/19 10:04 142-28-90.50 0.25 1
2,2-Dichloropropane ND ug/L 08/07/19 10:04 594-20-70.50 0.25 1
1,1-Dichloropropene ND ug/L 08/07/19 10:04 563-58-60.50 0.25 1
cis-1,3-Dichloropropene ND ug/L 08/07/19 10:04 10061-01-50.50 0.25 1
trans-1,3-Dichloropropene ND ug/L 08/07/19 10:04 10061-02-60.50 0.25 1
Diisopropyl ether ND ug/L 08/07/19 10:04 108-20-30.50 0.25 1
Ethylbenzene ND ug/L 08/07/19 10:04 100-41-40.50 0.25 1
Hexachloro-1,3-butadiene ND ug/L 08/07/19 10:04 87-68-32.0 1.0 1
Isopropylbenzene (Cumene)ND ug/L 08/07/19 10:04 98-82-80.50 0.25 1
Methylene Chloride ND ug/L 08/07/19 10:04 75-09-22.0 1.0 1
Methyl-tert-butyl ether ND ug/L 08/07/19 10:04 1634-04-40.50 0.25 1
Naphthalene ND ug/L 08/07/19 10:04 91-20-32.0 1.0 1
n-Propylbenzene ND ug/L 08/07/19 10:04 103-65-10.50 0.25 1
Styrene ND ug/L 08/07/19 10:04 100-42-50.50 0.25 1
1,1,1,2-Tetrachloroethane ND ug/L 08/07/19 10:04 630-20-60.50 0.25 1
1,1,2,2-Tetrachloroethane ND ug/L 08/07/19 10:04 79-34-50.50 0.25 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 10 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Sample: MW-8 Lab ID: 92439770003 Collected: 07/31/19 14:40 Received: 08/02/19 10:51 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 08/07/19 10:04 127-18-40.50 0.25 1
Toluene ND ug/L 08/07/19 10:04 108-88-30.50 0.25 1
1,2,3-Trichlorobenzene ND ug/L 08/07/19 10:04 87-61-62.0 1.0 1
1,2,4-Trichlorobenzene ND ug/L 08/07/19 10:04 120-82-12.0 1.0 1
1,1,1-Trichloroethane ND ug/L 08/07/19 10:04 71-55-60.50 0.25 1
1,1,2-Trichloroethane ND ug/L 08/07/19 10:04 79-00-50.50 0.25 1
Trichloroethene ND ug/L 08/07/19 10:04 79-01-60.50 0.25 1
Trichlorofluoromethane ND ug/L 08/07/19 10:04 75-69-41.0 0.50 1
1,2,3-Trichloropropane ND ug/L 08/07/19 10:04 96-18-40.50 0.25 1
1,2,4-Trimethylbenzene ND ug/L 08/07/19 10:04 95-63-60.50 0.25 1
1,3,5-Trimethylbenzene ND ug/L 08/07/19 10:04 108-67-80.50 0.25 1
Vinyl chloride ND ug/L 08/07/19 10:04 75-01-41.0 0.50 1
m&p-Xylene ND ug/L 08/07/19 10:04 179601-23-11.0 0.50 1
o-Xylene ND ug/L 08/07/19 10:04 95-47-60.50 0.25 1
Surrogates
1,2-Dichloroethane-d4 (S)92 %08/07/19 10:04 17060-07-070-130 1
4-Bromofluorobenzene (S)94 %08/07/19 10:04 460-00-470-130 1
Toluene-d8 (S)98 %08/07/19 10:04 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Sample: WSW-2 Lab ID: 92439770004 Collected: 07/31/19 15:50 Received: 08/02/19 10:51 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 08/06/19 09:12 71-43-20.50 0.25 1
Bromobenzene ND ug/L 08/06/19 09:12 108-86-10.50 0.25 1
Bromochloromethane ND ug/L 08/06/19 09:12 74-97-50.50 0.25 1
Bromodichloromethane ND ug/L 08/06/19 09:12 75-27-40.50 0.25 1
Bromoform ND ug/L 08/06/19 09:12 75-25-20.50 0.25 1
Bromomethane ND ug/L 08/06/19 09:12 74-83-95.0 2.5 1
n-Butylbenzene ND ug/L 08/06/19 09:12 104-51-80.50 0.25 1
sec-Butylbenzene ND ug/L 08/06/19 09:12 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 08/06/19 09:12 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 08/06/19 09:12 56-23-50.50 0.25 1
Chlorobenzene ND ug/L 08/06/19 09:12 108-90-70.50 0.25 1
Chloroethane ND ug/L 08/06/19 09:12 75-00-31.0 0.50 1
Chloroform ND ug/L 08/06/19 09:12 67-66-35.0 2.5 1
Chloromethane ND ug/L 08/06/19 09:12 74-87-31.0 0.50 1
2-Chlorotoluene ND ug/L 08/06/19 09:12 95-49-80.50 0.25 1
4-Chlorotoluene ND ug/L 08/06/19 09:12 106-43-40.50 0.25 1
1,2-Dibromo-3-chloropropane ND ug/L 08/06/19 09:12 96-12-81.0 0.50 1
Dibromochloromethane ND ug/L 08/06/19 09:12 124-48-10.50 0.25 1
1,2-Dibromoethane (EDB)ND ug/L 08/06/19 09:12 106-93-40.50 0.25 1
Dibromomethane ND ug/L 08/06/19 09:12 74-95-30.50 0.25 1
1,2-Dichlorobenzene ND ug/L 08/06/19 09:12 95-50-10.50 0.25 1
1,3-Dichlorobenzene ND ug/L 08/06/19 09:12 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 08/06/19 09:12 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 08/06/19 09:12 75-71-80.50 0.25 1
1,1-Dichloroethane ND ug/L 08/06/19 09:12 75-34-30.50 0.25 1
1,2-Dichloroethane ND ug/L 08/06/19 09:12 107-06-20.50 0.25 1
1,1-Dichloroethene ND ug/L 08/06/19 09:12 75-35-40.50 0.25 1
cis-1,2-Dichloroethene ND ug/L 08/06/19 09:12 156-59-20.50 0.25 1
trans-1,2-Dichloroethene ND ug/L 08/06/19 09:12 156-60-50.50 0.25 1
1,2-Dichloropropane ND ug/L 08/06/19 09:12 78-87-50.50 0.25 1
1,3-Dichloropropane ND ug/L 08/06/19 09:12 142-28-90.50 0.25 1
2,2-Dichloropropane ND ug/L 08/06/19 09:12 594-20-70.50 0.25 1
1,1-Dichloropropene ND ug/L 08/06/19 09:12 563-58-60.50 0.25 1
cis-1,3-Dichloropropene ND ug/L 08/06/19 09:12 10061-01-50.50 0.25 1
trans-1,3-Dichloropropene ND ug/L 08/06/19 09:12 10061-02-60.50 0.25 1
Diisopropyl ether ND ug/L 08/06/19 09:12 108-20-30.50 0.25 1
Ethylbenzene ND ug/L 08/06/19 09:12 100-41-40.50 0.25 1
Hexachloro-1,3-butadiene ND ug/L 08/06/19 09:12 87-68-32.0 1.0 1
Isopropylbenzene (Cumene)ND ug/L 08/06/19 09:12 98-82-80.50 0.25 1
Methylene Chloride ND ug/L 08/06/19 09:12 75-09-22.0 1.0 1
Methyl-tert-butyl ether ND ug/L 08/06/19 09:12 1634-04-40.50 0.25 1
Naphthalene ND ug/L 08/06/19 09:12 91-20-32.0 1.0 1
n-Propylbenzene ND ug/L 08/06/19 09:12 103-65-10.50 0.25 1
Styrene ND ug/L 08/06/19 09:12 100-42-50.50 0.25 1
1,1,1,2-Tetrachloroethane ND ug/L 08/06/19 09:12 630-20-60.50 0.25 1
1,1,2,2-Tetrachloroethane ND ug/L 08/06/19 09:12 79-34-50.50 0.25 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Sample: WSW-2 Lab ID: 92439770004 Collected: 07/31/19 15:50 Received: 08/02/19 10:51 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 08/06/19 09:12 127-18-40.50 0.25 1
Toluene ND ug/L 08/06/19 09:12 108-88-30.50 0.25 1
1,2,3-Trichlorobenzene ND ug/L 08/06/19 09:12 87-61-62.0 1.0 1
1,2,4-Trichlorobenzene ND ug/L 08/06/19 09:12 120-82-12.0 1.0 1
1,1,1-Trichloroethane ND ug/L 08/06/19 09:12 71-55-60.50 0.25 1
1,1,2-Trichloroethane ND ug/L 08/06/19 09:12 79-00-50.50 0.25 1
Trichloroethene ND ug/L 08/06/19 09:12 79-01-60.50 0.25 1
Trichlorofluoromethane ND ug/L 08/06/19 09:12 75-69-41.0 0.50 1
1,2,3-Trichloropropane ND ug/L 08/06/19 09:12 96-18-40.50 0.25 1
1,2,4-Trimethylbenzene ND ug/L 08/06/19 09:12 95-63-60.50 0.25 1
1,3,5-Trimethylbenzene ND ug/L 08/06/19 09:12 108-67-80.50 0.25 1
Vinyl chloride ND ug/L 08/06/19 09:12 75-01-41.0 0.50 1
m&p-Xylene ND ug/L 08/06/19 09:12 179601-23-11.0 0.50 1
o-Xylene ND ug/L 08/06/19 09:12 95-47-60.50 0.25 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %08/06/19 09:12 17060-07-070-130 1
4-Bromofluorobenzene (S)98 %08/06/19 09:12 460-00-470-130 1
Toluene-d8 (S)101 %08/06/19 09:12 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Sample: WSW-3 Lab ID: 92439770005 Collected: 07/31/19 15:55 Received: 08/02/19 10:51 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 08/06/19 09:31 71-43-20.50 0.25 1
Bromobenzene ND ug/L 08/06/19 09:31 108-86-10.50 0.25 1
Bromochloromethane ND ug/L 08/06/19 09:31 74-97-50.50 0.25 1
Bromodichloromethane ND ug/L 08/06/19 09:31 75-27-40.50 0.25 1
Bromoform ND ug/L 08/06/19 09:31 75-25-20.50 0.25 1
Bromomethane ND ug/L 08/06/19 09:31 74-83-95.0 2.5 1
n-Butylbenzene ND ug/L 08/06/19 09:31 104-51-80.50 0.25 1
sec-Butylbenzene ND ug/L 08/06/19 09:31 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 08/06/19 09:31 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 08/06/19 09:31 56-23-50.50 0.25 1
Chlorobenzene ND ug/L 08/06/19 09:31 108-90-70.50 0.25 1
Chloroethane ND ug/L 08/06/19 09:31 75-00-31.0 0.50 1
Chloroform ND ug/L 08/06/19 09:31 67-66-35.0 2.5 1
Chloromethane ND ug/L 08/06/19 09:31 74-87-31.0 0.50 1
2-Chlorotoluene ND ug/L 08/06/19 09:31 95-49-80.50 0.25 1
4-Chlorotoluene ND ug/L 08/06/19 09:31 106-43-40.50 0.25 1
1,2-Dibromo-3-chloropropane ND ug/L 08/06/19 09:31 96-12-81.0 0.50 1
Dibromochloromethane ND ug/L 08/06/19 09:31 124-48-10.50 0.25 1
1,2-Dibromoethane (EDB)ND ug/L 08/06/19 09:31 106-93-40.50 0.25 1
Dibromomethane ND ug/L 08/06/19 09:31 74-95-30.50 0.25 1
1,2-Dichlorobenzene ND ug/L 08/06/19 09:31 95-50-10.50 0.25 1
1,3-Dichlorobenzene ND ug/L 08/06/19 09:31 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 08/06/19 09:31 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 08/06/19 09:31 75-71-80.50 0.25 1
1,1-Dichloroethane ND ug/L 08/06/19 09:31 75-34-30.50 0.25 1
1,2-Dichloroethane ND ug/L 08/06/19 09:31 107-06-20.50 0.25 1
1,1-Dichloroethene ND ug/L 08/06/19 09:31 75-35-40.50 0.25 1
cis-1,2-Dichloroethene ND ug/L 08/06/19 09:31 156-59-20.50 0.25 1
trans-1,2-Dichloroethene ND ug/L 08/06/19 09:31 156-60-50.50 0.25 1
1,2-Dichloropropane ND ug/L 08/06/19 09:31 78-87-50.50 0.25 1
1,3-Dichloropropane ND ug/L 08/06/19 09:31 142-28-90.50 0.25 1
2,2-Dichloropropane ND ug/L 08/06/19 09:31 594-20-70.50 0.25 1
1,1-Dichloropropene ND ug/L 08/06/19 09:31 563-58-60.50 0.25 1
cis-1,3-Dichloropropene ND ug/L 08/06/19 09:31 10061-01-50.50 0.25 1
trans-1,3-Dichloropropene ND ug/L 08/06/19 09:31 10061-02-60.50 0.25 1
Diisopropyl ether ND ug/L 08/06/19 09:31 108-20-30.50 0.25 1
Ethylbenzene ND ug/L 08/06/19 09:31 100-41-40.50 0.25 1
Hexachloro-1,3-butadiene ND ug/L 08/06/19 09:31 87-68-32.0 1.0 1
Isopropylbenzene (Cumene)ND ug/L 08/06/19 09:31 98-82-80.50 0.25 1
Methylene Chloride ND ug/L 08/06/19 09:31 75-09-22.0 1.0 1
Methyl-tert-butyl ether ND ug/L 08/06/19 09:31 1634-04-40.50 0.25 1
Naphthalene ND ug/L 08/06/19 09:31 91-20-32.0 1.0 1
n-Propylbenzene ND ug/L 08/06/19 09:31 103-65-10.50 0.25 1
Styrene ND ug/L 08/06/19 09:31 100-42-50.50 0.25 1
1,1,1,2-Tetrachloroethane ND ug/L 08/06/19 09:31 630-20-60.50 0.25 1
1,1,2,2-Tetrachloroethane ND ug/L 08/06/19 09:31 79-34-50.50 0.25 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Sample: WSW-3 Lab ID: 92439770005 Collected: 07/31/19 15:55 Received: 08/02/19 10:51 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 08/06/19 09:31 127-18-40.50 0.25 1
Toluene ND ug/L 08/06/19 09:31 108-88-30.50 0.25 1
1,2,3-Trichlorobenzene ND ug/L 08/06/19 09:31 87-61-62.0 1.0 1
1,2,4-Trichlorobenzene ND ug/L 08/06/19 09:31 120-82-12.0 1.0 1
1,1,1-Trichloroethane ND ug/L 08/06/19 09:31 71-55-60.50 0.25 1
1,1,2-Trichloroethane ND ug/L 08/06/19 09:31 79-00-50.50 0.25 1
Trichloroethene ND ug/L 08/06/19 09:31 79-01-60.50 0.25 1
Trichlorofluoromethane ND ug/L 08/06/19 09:31 75-69-41.0 0.50 1
1,2,3-Trichloropropane ND ug/L 08/06/19 09:31 96-18-40.50 0.25 1
1,2,4-Trimethylbenzene ND ug/L 08/06/19 09:31 95-63-60.50 0.25 1
1,3,5-Trimethylbenzene ND ug/L 08/06/19 09:31 108-67-80.50 0.25 1
Vinyl chloride ND ug/L 08/06/19 09:31 75-01-41.0 0.50 1
m&p-Xylene ND ug/L 08/06/19 09:31 179601-23-11.0 0.50 1
o-Xylene ND ug/L 08/06/19 09:31 95-47-60.50 0.25 1
Surrogates
1,2-Dichloroethane-d4 (S)94 %08/06/19 09:31 17060-07-070-130 1
4-Bromofluorobenzene (S)96 %08/06/19 09:31 460-00-470-130 1
Toluene-d8 (S)102 %08/06/19 09:31 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Sample: WSW-4 Lab ID: 92439770006 Collected: 07/31/19 16:05 Received: 08/02/19 10:51 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 08/06/19 09:49 71-43-20.50 0.25 1
Bromobenzene ND ug/L 08/06/19 09:49 108-86-10.50 0.25 1
Bromochloromethane ND ug/L 08/06/19 09:49 74-97-50.50 0.25 1
Bromodichloromethane ND ug/L 08/06/19 09:49 75-27-40.50 0.25 1
Bromoform ND ug/L 08/06/19 09:49 75-25-20.50 0.25 1
Bromomethane ND ug/L 08/06/19 09:49 74-83-95.0 2.5 1
n-Butylbenzene ND ug/L 08/06/19 09:49 104-51-80.50 0.25 1
sec-Butylbenzene ND ug/L 08/06/19 09:49 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 08/06/19 09:49 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 08/06/19 09:49 56-23-50.50 0.25 1
Chlorobenzene ND ug/L 08/06/19 09:49 108-90-70.50 0.25 1
Chloroethane ND ug/L 08/06/19 09:49 75-00-31.0 0.50 1
Chloroform ND ug/L 08/06/19 09:49 67-66-35.0 2.5 1
Chloromethane ND ug/L 08/06/19 09:49 74-87-31.0 0.50 1
2-Chlorotoluene ND ug/L 08/06/19 09:49 95-49-80.50 0.25 1
4-Chlorotoluene ND ug/L 08/06/19 09:49 106-43-40.50 0.25 1
1,2-Dibromo-3-chloropropane ND ug/L 08/06/19 09:49 96-12-81.0 0.50 1
Dibromochloromethane ND ug/L 08/06/19 09:49 124-48-10.50 0.25 1
1,2-Dibromoethane (EDB)ND ug/L 08/06/19 09:49 106-93-40.50 0.25 1
Dibromomethane ND ug/L 08/06/19 09:49 74-95-30.50 0.25 1
1,2-Dichlorobenzene ND ug/L 08/06/19 09:49 95-50-10.50 0.25 1
1,3-Dichlorobenzene ND ug/L 08/06/19 09:49 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 08/06/19 09:49 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 08/06/19 09:49 75-71-80.50 0.25 1
1,1-Dichloroethane ND ug/L 08/06/19 09:49 75-34-30.50 0.25 1
1,2-Dichloroethane ND ug/L 08/06/19 09:49 107-06-20.50 0.25 1
1,1-Dichloroethene ND ug/L 08/06/19 09:49 75-35-40.50 0.25 1
cis-1,2-Dichloroethene ND ug/L 08/06/19 09:49 156-59-20.50 0.25 1
trans-1,2-Dichloroethene ND ug/L 08/06/19 09:49 156-60-50.50 0.25 1
1,2-Dichloropropane ND ug/L 08/06/19 09:49 78-87-50.50 0.25 1
1,3-Dichloropropane ND ug/L 08/06/19 09:49 142-28-90.50 0.25 1
2,2-Dichloropropane ND ug/L 08/06/19 09:49 594-20-70.50 0.25 1
1,1-Dichloropropene ND ug/L 08/06/19 09:49 563-58-60.50 0.25 1
cis-1,3-Dichloropropene ND ug/L 08/06/19 09:49 10061-01-50.50 0.25 1
trans-1,3-Dichloropropene ND ug/L 08/06/19 09:49 10061-02-60.50 0.25 1
Diisopropyl ether ND ug/L 08/06/19 09:49 108-20-30.50 0.25 1
Ethylbenzene ND ug/L 08/06/19 09:49 100-41-40.50 0.25 1
Hexachloro-1,3-butadiene ND ug/L 08/06/19 09:49 87-68-32.0 1.0 1
Isopropylbenzene (Cumene)ND ug/L 08/06/19 09:49 98-82-80.50 0.25 1
Methylene Chloride ND ug/L 08/06/19 09:49 75-09-22.0 1.0 1
Methyl-tert-butyl ether ND ug/L 08/06/19 09:49 1634-04-40.50 0.25 1
Naphthalene ND ug/L 08/06/19 09:49 91-20-32.0 1.0 1
n-Propylbenzene ND ug/L 08/06/19 09:49 103-65-10.50 0.25 1
Styrene ND ug/L 08/06/19 09:49 100-42-50.50 0.25 1
1,1,1,2-Tetrachloroethane ND ug/L 08/06/19 09:49 630-20-60.50 0.25 1
1,1,2,2-Tetrachloroethane ND ug/L 08/06/19 09:49 79-34-50.50 0.25 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
Pace Analytical Services, LLC
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Page 16 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Sample: WSW-4 Lab ID: 92439770006 Collected: 07/31/19 16:05 Received: 08/02/19 10:51 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 08/06/19 09:49 127-18-40.50 0.25 1
Toluene ND ug/L 08/06/19 09:49 108-88-30.50 0.25 1
1,2,3-Trichlorobenzene ND ug/L 08/06/19 09:49 87-61-62.0 1.0 1
1,2,4-Trichlorobenzene ND ug/L 08/06/19 09:49 120-82-12.0 1.0 1
1,1,1-Trichloroethane ND ug/L 08/06/19 09:49 71-55-60.50 0.25 1
1,1,2-Trichloroethane ND ug/L 08/06/19 09:49 79-00-50.50 0.25 1
Trichloroethene ND ug/L 08/06/19 09:49 79-01-60.50 0.25 1
Trichlorofluoromethane ND ug/L 08/06/19 09:49 75-69-41.0 0.50 1
1,2,3-Trichloropropane ND ug/L 08/06/19 09:49 96-18-40.50 0.25 1
1,2,4-Trimethylbenzene ND ug/L 08/06/19 09:49 95-63-60.50 0.25 1
1,3,5-Trimethylbenzene ND ug/L 08/06/19 09:49 108-67-80.50 0.25 1
Vinyl chloride ND ug/L 08/06/19 09:49 75-01-41.0 0.50 1
m&p-Xylene ND ug/L 08/06/19 09:49 179601-23-11.0 0.50 1
o-Xylene ND ug/L 08/06/19 09:49 95-47-60.50 0.25 1
Surrogates
1,2-Dichloroethane-d4 (S)98 %08/06/19 09:49 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %08/06/19 09:49 460-00-470-130 1
Toluene-d8 (S)100 %08/06/19 09:49 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
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9800 Kincey Ave. Suite 100
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Page 17 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Sample: WSW-7 Lab ID: 92439770007 Collected: 07/31/19 16:20 Received: 08/02/19 10:51 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene ND ug/L 08/06/19 10:07 71-43-20.50 0.25 1
Bromobenzene ND ug/L 08/06/19 10:07 108-86-10.50 0.25 1
Bromochloromethane ND ug/L 08/06/19 10:07 74-97-50.50 0.25 1
Bromodichloromethane ND ug/L 08/06/19 10:07 75-27-40.50 0.25 1
Bromoform ND ug/L 08/06/19 10:07 75-25-20.50 0.25 1
Bromomethane ND ug/L 08/06/19 10:07 74-83-95.0 2.5 1
n-Butylbenzene ND ug/L 08/06/19 10:07 104-51-80.50 0.25 1
sec-Butylbenzene ND ug/L 08/06/19 10:07 135-98-80.50 0.25 1
tert-Butylbenzene ND ug/L 08/06/19 10:07 98-06-60.50 0.25 1
Carbon tetrachloride ND ug/L 08/06/19 10:07 56-23-50.50 0.25 1
Chlorobenzene ND ug/L 08/06/19 10:07 108-90-70.50 0.25 1
Chloroethane ND ug/L 08/06/19 10:07 75-00-31.0 0.50 1
Chloroform ND ug/L 08/06/19 10:07 67-66-35.0 2.5 1
Chloromethane ND ug/L 08/06/19 10:07 74-87-31.0 0.50 1
2-Chlorotoluene ND ug/L 08/06/19 10:07 95-49-80.50 0.25 1
4-Chlorotoluene ND ug/L 08/06/19 10:07 106-43-40.50 0.25 1
1,2-Dibromo-3-chloropropane ND ug/L 08/06/19 10:07 96-12-81.0 0.50 1
Dibromochloromethane ND ug/L 08/06/19 10:07 124-48-10.50 0.25 1
1,2-Dibromoethane (EDB)ND ug/L 08/06/19 10:07 106-93-40.50 0.25 1
Dibromomethane ND ug/L 08/06/19 10:07 74-95-30.50 0.25 1
1,2-Dichlorobenzene ND ug/L 08/06/19 10:07 95-50-10.50 0.25 1
1,3-Dichlorobenzene ND ug/L 08/06/19 10:07 541-73-10.50 0.25 1
1,4-Dichlorobenzene ND ug/L 08/06/19 10:07 106-46-70.50 0.25 1
Dichlorodifluoromethane ND ug/L 08/06/19 10:07 75-71-80.50 0.25 1
1,1-Dichloroethane ND ug/L 08/06/19 10:07 75-34-30.50 0.25 1
1,2-Dichloroethane ND ug/L 08/06/19 10:07 107-06-20.50 0.25 1
1,1-Dichloroethene ND ug/L 08/06/19 10:07 75-35-40.50 0.25 1
cis-1,2-Dichloroethene ND ug/L 08/06/19 10:07 156-59-20.50 0.25 1
trans-1,2-Dichloroethene ND ug/L 08/06/19 10:07 156-60-50.50 0.25 1
1,2-Dichloropropane ND ug/L 08/06/19 10:07 78-87-50.50 0.25 1
1,3-Dichloropropane ND ug/L 08/06/19 10:07 142-28-90.50 0.25 1
2,2-Dichloropropane ND ug/L 08/06/19 10:07 594-20-70.50 0.25 1
1,1-Dichloropropene ND ug/L 08/06/19 10:07 563-58-60.50 0.25 1
cis-1,3-Dichloropropene ND ug/L 08/06/19 10:07 10061-01-50.50 0.25 1
trans-1,3-Dichloropropene ND ug/L 08/06/19 10:07 10061-02-60.50 0.25 1
Diisopropyl ether ND ug/L 08/06/19 10:07 108-20-30.50 0.25 1
Ethylbenzene ND ug/L 08/06/19 10:07 100-41-40.50 0.25 1
Hexachloro-1,3-butadiene ND ug/L 08/06/19 10:07 87-68-32.0 1.0 1
Isopropylbenzene (Cumene)ND ug/L 08/06/19 10:07 98-82-80.50 0.25 1
Methylene Chloride ND ug/L 08/06/19 10:07 75-09-22.0 1.0 1
Methyl-tert-butyl ether ND ug/L 08/06/19 10:07 1634-04-40.50 0.25 1
Naphthalene ND ug/L 08/06/19 10:07 91-20-32.0 1.0 1
n-Propylbenzene ND ug/L 08/06/19 10:07 103-65-10.50 0.25 1
Styrene ND ug/L 08/06/19 10:07 100-42-50.50 0.25 1
1,1,1,2-Tetrachloroethane ND ug/L 08/06/19 10:07 630-20-60.50 0.25 1
1,1,2,2-Tetrachloroethane ND ug/L 08/06/19 10:07 79-34-50.50 0.25 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
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Huntersville, NC 28078
[phone]
Page 18 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Sample: WSW-7 Lab ID: 92439770007 Collected: 07/31/19 16:20 Received: 08/02/19 10:51 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 08/06/19 10:07 127-18-40.50 0.25 1
Toluene ND ug/L 08/06/19 10:07 108-88-30.50 0.25 1
1,2,3-Trichlorobenzene ND ug/L 08/06/19 10:07 87-61-6 M12.0 1.0 1
1,2,4-Trichlorobenzene ND ug/L 08/06/19 10:07 120-82-12.0 1.0 1
1,1,1-Trichloroethane ND ug/L 08/06/19 10:07 71-55-60.50 0.25 1
1,1,2-Trichloroethane ND ug/L 08/06/19 10:07 79-00-50.50 0.25 1
Trichloroethene ND ug/L 08/06/19 10:07 79-01-60.50 0.25 1
Trichlorofluoromethane ND ug/L 08/06/19 10:07 75-69-41.0 0.50 1
1,2,3-Trichloropropane ND ug/L 08/06/19 10:07 96-18-40.50 0.25 1
1,2,4-Trimethylbenzene ND ug/L 08/06/19 10:07 95-63-60.50 0.25 1
1,3,5-Trimethylbenzene ND ug/L 08/06/19 10:07 108-67-80.50 0.25 1
Vinyl chloride ND ug/L 08/06/19 10:07 75-01-41.0 0.50 1
m&p-Xylene ND ug/L 08/06/19 10:07 179601-23-11.0 0.50 1
o-Xylene ND ug/L 08/06/19 10:07 95-47-60.50 0.25 1
Surrogates
1,2-Dichloroethane-d4 (S)96 %08/06/19 10:07 17060-07-070-130 1
4-Bromofluorobenzene (S)97 %08/06/19 10:07 460-00-470-130 1
Toluene-d8 (S)105 %08/06/19 10:07 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Sample: WSW-8 Lab ID: 92439770008 Collected: 07/31/19 15:35 Received: 08/02/19 10:51 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Benzene 10.9 ug/L 08/07/19 06:41 71-43-21.2 0.62 2.5
Bromobenzene ND ug/L 08/07/19 06:41 108-86-11.2 0.62 2.5
Bromochloromethane ND ug/L 08/07/19 06:41 74-97-51.2 0.62 2.5
Bromodichloromethane ND ug/L 08/07/19 06:41 75-27-41.2 0.62 2.5
Bromoform ND ug/L 08/07/19 06:41 75-25-21.2 0.62 2.5
Bromomethane ND ug/L 08/07/19 06:41 74-83-912.5 6.2 2.5
n-Butylbenzene ND ug/L 08/07/19 06:41 104-51-81.2 0.62 2.5
sec-Butylbenzene ND ug/L 08/07/19 06:41 135-98-81.2 0.62 2.5
tert-Butylbenzene ND ug/L 08/07/19 06:41 98-06-61.2 0.62 2.5
Carbon tetrachloride ND ug/L 08/07/19 06:41 56-23-51.2 0.62 2.5
Chlorobenzene ND ug/L 08/07/19 06:41 108-90-71.2 0.62 2.5
Chloroethane ND ug/L 08/07/19 06:41 75-00-32.5 1.2 2.5
Chloroform ND ug/L 08/07/19 06:41 67-66-312.5 6.2 2.5
Chloromethane ND ug/L 08/07/19 06:41 74-87-32.5 1.2 2.5
2-Chlorotoluene ND ug/L 08/07/19 06:41 95-49-81.2 0.62 2.5
4-Chlorotoluene ND ug/L 08/07/19 06:41 106-43-41.2 0.62 2.5
1,2-Dibromo-3-chloropropane ND ug/L 08/07/19 06:41 96-12-82.5 1.2 2.5
Dibromochloromethane ND ug/L 08/07/19 06:41 124-48-11.2 0.62 2.5
1,2-Dibromoethane (EDB)ND ug/L 08/07/19 06:41 106-93-41.2 0.62 2.5
Dibromomethane ND ug/L 08/07/19 06:41 74-95-31.2 0.62 2.5
1,2-Dichlorobenzene ND ug/L 08/07/19 06:41 95-50-11.2 0.62 2.5
1,3-Dichlorobenzene ND ug/L 08/07/19 06:41 541-73-11.2 0.62 2.5
1,4-Dichlorobenzene ND ug/L 08/07/19 06:41 106-46-71.2 0.62 2.5
Dichlorodifluoromethane ND ug/L 08/07/19 06:41 75-71-81.2 0.62 2.5
1,1-Dichloroethane ND ug/L 08/07/19 06:41 75-34-31.2 0.62 2.5
1,2-Dichloroethane 3.0 ug/L 08/07/19 06:41 107-06-21.2 0.62 2.5
1,1-Dichloroethene ND ug/L 08/07/19 06:41 75-35-41.2 0.62 2.5
cis-1,2-Dichloroethene ND ug/L 08/07/19 06:41 156-59-21.2 0.62 2.5
trans-1,2-Dichloroethene ND ug/L 08/07/19 06:41 156-60-51.2 0.62 2.5
1,2-Dichloropropane ND ug/L 08/07/19 06:41 78-87-51.2 0.62 2.5
1,3-Dichloropropane ND ug/L 08/07/19 06:41 142-28-91.2 0.62 2.5
2,2-Dichloropropane ND ug/L 08/07/19 06:41 594-20-71.2 0.62 2.5
1,1-Dichloropropene ND ug/L 08/07/19 06:41 563-58-61.2 0.62 2.5
cis-1,3-Dichloropropene ND ug/L 08/07/19 06:41 10061-01-51.2 0.62 2.5
trans-1,3-Dichloropropene ND ug/L 08/07/19 06:41 10061-02-61.2 0.62 2.5
Diisopropyl ether 25.5 ug/L 08/07/19 06:41 108-20-31.2 0.62 2.5
Ethylbenzene 6.4 ug/L 08/07/19 06:41 100-41-41.2 0.62 2.5
Hexachloro-1,3-butadiene ND ug/L 08/07/19 06:41 87-68-35.0 2.5 2.5
Isopropylbenzene (Cumene)1.6 ug/L 08/07/19 06:41 98-82-81.2 0.62 2.5
Methylene Chloride ND ug/L 08/07/19 06:41 75-09-25.0 2.5 2.5
Methyl-tert-butyl ether 320 ug/L 08/07/19 06:41 1634-04-41.2 0.62 2.5
Naphthalene ND ug/L 08/07/19 06:41 91-20-35.0 2.5 2.5
n-Propylbenzene 2.5 ug/L 08/07/19 06:41 103-65-11.2 0.62 2.5
Styrene ND ug/L 08/07/19 06:41 100-42-51.2 0.62 2.5
1,1,1,2-Tetrachloroethane ND ug/L 08/07/19 06:41 630-20-61.2 0.62 2.5
1,1,2,2-Tetrachloroethane ND ug/L 08/07/19 06:41 79-34-51.2 0.62 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 41
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Sample: WSW-8 Lab ID: 92439770008 Collected: 07/31/19 15:35 Received: 08/02/19 10:51 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: SM 6200B6200B MSV
Tetrachloroethene ND ug/L 08/07/19 06:41 127-18-41.2 0.62 2.5
Toluene 5.3 ug/L 08/07/19 06:41 108-88-31.2 0.62 2.5
1,2,3-Trichlorobenzene ND ug/L 08/07/19 06:41 87-61-65.0 2.5 2.5
1,2,4-Trichlorobenzene ND ug/L 08/07/19 06:41 120-82-15.0 2.5 2.5
1,1,1-Trichloroethane ND ug/L 08/07/19 06:41 71-55-61.2 0.62 2.5
1,1,2-Trichloroethane ND ug/L 08/07/19 06:41 79-00-51.2 0.62 2.5
Trichloroethene ND ug/L 08/07/19 06:41 79-01-61.2 0.62 2.5
Trichlorofluoromethane ND ug/L 08/07/19 06:41 75-69-42.5 1.2 2.5
1,2,3-Trichloropropane ND ug/L 08/07/19 06:41 96-18-41.2 0.62 2.5
1,2,4-Trimethylbenzene 8.1 ug/L 08/07/19 06:41 95-63-61.2 0.62 2.5
1,3,5-Trimethylbenzene 4.5 ug/L 08/07/19 06:41 108-67-81.2 0.62 2.5
Vinyl chloride ND ug/L 08/07/19 06:41 75-01-42.5 1.2 2.5
m&p-Xylene 13.0 ug/L 08/07/19 06:41 179601-23-12.5 1.2 2.5
o-Xylene 5.9 ug/L 08/07/19 06:41 95-47-61.2 0.62 2.5
Surrogates
1,2-Dichloroethane-d4 (S)92 %08/07/19 06:41 17060-07-070-130 2.5
4-Bromofluorobenzene (S)96 %08/07/19 06:41 460-00-470-130 2.5
Toluene-d8 (S)100 %08/07/19 06:41 2037-26-570-130 2.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 21 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
490429
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92439770004, 92439770005, 92439770006, 92439770007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2645817
Associated Lab Samples:92439770004, 92439770005, 92439770006, 92439770007
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 08/06/19 04:220.25
1,1,1-Trichloroethane ug/L ND 0.50 08/06/19 04:220.25
1,1,2,2-Tetrachloroethane ug/L ND 0.50 08/06/19 04:220.25
1,1,2-Trichloroethane ug/L ND 0.50 08/06/19 04:220.25
1,1-Dichloroethane ug/L ND 0.50 08/06/19 04:220.25
1,1-Dichloroethene ug/L ND 0.50 08/06/19 04:220.25
1,1-Dichloropropene ug/L ND 0.50 08/06/19 04:220.25
1,2,3-Trichlorobenzene ug/L ND 2.0 08/06/19 04:221.0
1,2,3-Trichloropropane ug/L ND 0.50 08/06/19 04:220.25
1,2,4-Trichlorobenzene ug/L ND 2.0 08/06/19 04:221.0
1,2,4-Trimethylbenzene ug/L ND 0.50 08/06/19 04:220.25
1,2-Dibromo-3-chloropropane ug/L ND 1.0 08/06/19 04:220.50
1,2-Dibromoethane (EDB)ug/L ND 0.50 08/06/19 04:220.25
1,2-Dichlorobenzene ug/L ND 0.50 08/06/19 04:220.25
1,2-Dichloroethane ug/L ND 0.50 08/06/19 04:220.25
1,2-Dichloropropane ug/L ND 0.50 08/06/19 04:220.25
1,3,5-Trimethylbenzene ug/L ND 0.50 08/06/19 04:220.25
1,3-Dichlorobenzene ug/L ND 0.50 08/06/19 04:220.25
1,3-Dichloropropane ug/L ND 0.50 08/06/19 04:220.25
1,4-Dichlorobenzene ug/L ND 0.50 08/06/19 04:220.25
2,2-Dichloropropane ug/L ND 0.50 08/06/19 04:220.25
2-Chlorotoluene ug/L ND 0.50 08/06/19 04:220.25
4-Chlorotoluene ug/L ND 0.50 08/06/19 04:220.25
Benzene ug/L ND 0.50 08/06/19 04:220.25
Bromobenzene ug/L ND 0.50 08/06/19 04:220.25
Bromochloromethane ug/L ND 0.50 08/06/19 04:220.25
Bromodichloromethane ug/L ND 0.50 08/06/19 04:220.25
Bromoform ug/L ND 0.50 08/06/19 04:220.25
Bromomethane ug/L ND 5.0 08/06/19 04:222.5
Carbon tetrachloride ug/L ND 0.50 08/06/19 04:220.25
Chlorobenzene ug/L ND 0.50 08/06/19 04:220.25
Chloroethane ug/L ND 1.0 08/06/19 04:220.50
Chloroform ug/L ND 5.0 08/06/19 04:222.5
Chloromethane ug/L ND 1.0 08/06/19 04:220.50
cis-1,2-Dichloroethene ug/L ND 0.50 08/06/19 04:220.25
cis-1,3-Dichloropropene ug/L ND 0.50 08/06/19 04:220.25
Dibromochloromethane ug/L ND 0.50 08/06/19 04:220.25
Dibromomethane ug/L ND 0.50 08/06/19 04:220.25
Dichlorodifluoromethane ug/L ND 0.50 08/06/19 04:220.25
Diisopropyl ether ug/L ND 0.50 08/06/19 04:220.25
Ethylbenzene ug/L ND 0.50 08/06/19 04:220.25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2645817
Associated Lab Samples:92439770004, 92439770005, 92439770006, 92439770007
Matrix: Water
AnalyzedMDL
Hexachloro-1,3-butadiene ug/L ND 2.0 08/06/19 04:221.0
Isopropylbenzene (Cumene)ug/L ND 0.50 08/06/19 04:220.25
m&p-Xylene ug/L ND 1.0 08/06/19 04:220.50
Methyl-tert-butyl ether ug/L ND 0.50 08/06/19 04:220.25
Methylene Chloride ug/L ND 2.0 08/06/19 04:221.0
n-Butylbenzene ug/L ND 0.50 08/06/19 04:220.25
n-Propylbenzene ug/L ND 0.50 08/06/19 04:220.25
Naphthalene ug/L ND 2.0 08/06/19 04:221.0
o-Xylene ug/L ND 0.50 08/06/19 04:220.25
sec-Butylbenzene ug/L ND 0.50 08/06/19 04:220.25
Styrene ug/L ND 0.50 08/06/19 04:220.25
tert-Butylbenzene ug/L ND 0.50 08/06/19 04:220.25
Tetrachloroethene ug/L ND 0.50 08/06/19 04:220.25
Toluene ug/L ND 0.50 08/06/19 04:220.25
trans-1,2-Dichloroethene ug/L ND 0.50 08/06/19 04:220.25
trans-1,3-Dichloropropene ug/L ND 0.50 08/06/19 04:220.25
Trichloroethene ug/L ND 0.50 08/06/19 04:220.25
Trichlorofluoromethane ug/L ND 1.0 08/06/19 04:220.50
Vinyl chloride ug/L ND 1.0 08/06/19 04:220.50
1,2-Dichloroethane-d4 (S)%97 70-130 08/06/19 04:22
4-Bromofluorobenzene (S)%97 70-130 08/06/19 04:22
Toluene-d8 (S)%102 70-130 08/06/19 04:22
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2645818LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.750 99 60-140
1,1,1-Trichloroethane ug/L 52.550 105 60-140
1,1,2,2-Tetrachloroethane ug/L 49.150 98 60-140
1,1,2-Trichloroethane ug/L 51.950 104 60-140
1,1-Dichloroethane ug/L 50.350 101 60-140
1,1-Dichloroethene ug/L 51.550 103 60-140
1,1-Dichloropropene ug/L 52.850 106 60-140
1,2,3-Trichlorobenzene ug/L 49.550 99 60-140
1,2,3-Trichloropropane ug/L 49.350 99 60-140
1,2,4-Trichlorobenzene ug/L 48.550 97 60-140
1,2,4-Trimethylbenzene ug/L 45.550 91 60-140
1,2-Dibromo-3-chloropropane ug/L 52.150 104 60-140
1,2-Dibromoethane (EDB)ug/L 49.450 99 60-140
1,2-Dichlorobenzene ug/L 47.550 95 60-140
1,2-Dichloroethane ug/L 53.350 107 60-140
1,2-Dichloropropane ug/L 51.950 104 60-140
1,3,5-Trimethylbenzene ug/L 45.750 91 60-140
1,3-Dichlorobenzene ug/L 46.550 93 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2645818LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 49.950 100 60-140
1,4-Dichlorobenzene ug/L 45.350 91 60-140
2,2-Dichloropropane ug/L 48.250 96 60-140
2-Chlorotoluene ug/L 45.150 90 60-140
4-Chlorotoluene ug/L 45.450 91 60-140
Benzene ug/L 50.650 101 60-140
Bromobenzene ug/L 46.750 93 60-140
Bromochloromethane ug/L 52.350 105 60-140
Bromodichloromethane ug/L 55.350 111 60-140
Bromoform ug/L 53.750 107 60-140
Bromomethane ug/L 51.350 103 60-140
Carbon tetrachloride ug/L 49.950 100 60-140
Chlorobenzene ug/L 46.750 93 60-140
Chloroethane ug/L 54.950 110 60-140
Chloroform ug/L 49.250 98 60-140
Chloromethane ug/L 55.150 110 60-140
cis-1,2-Dichloroethene ug/L 49.850 100 60-140
cis-1,3-Dichloropropene ug/L 54.150 108 60-140
Dibromochloromethane ug/L 52.350 105 60-140
Dibromomethane ug/L 57.050 114 60-140
Dichlorodifluoromethane ug/L 55.550 111 60-140
Diisopropyl ether ug/L 51.650 103 60-140
Ethylbenzene ug/L 47.250 94 60-140
Hexachloro-1,3-butadiene ug/L 46.650 93 60-140
Isopropylbenzene (Cumene)ug/L 47.550 95 60-140
m&p-Xylene ug/L 95.0100 95 60-140
Methyl-tert-butyl ether ug/L 52.650 105 60-140
Methylene Chloride ug/L 48.650 97 60-140
n-Butylbenzene ug/L 44.350 89 60-140
n-Propylbenzene ug/L 45.450 91 60-140
Naphthalene ug/L 49.850 100 60-140
o-Xylene ug/L 48.350 97 60-140
sec-Butylbenzene ug/L 47.350 95 60-140
Styrene ug/L 48.650 97 60-140
tert-Butylbenzene ug/L 40.550 81 60-140
Tetrachloroethene ug/L 47.950 96 60-140
Toluene ug/L 48.450 97 60-140
trans-1,2-Dichloroethene ug/L 50.550 101 60-140
trans-1,3-Dichloropropene ug/L 54.250 108 60-140
Trichloroethene ug/L 49.750 99 60-140
Trichlorofluoromethane ug/L 56.150 112 60-140
Vinyl chloride ug/L 59.550 119 60-140
1,2-Dichloroethane-d4 (S)%96 70-130
4-Bromofluorobenzene (S)%102 70-130
Toluene-d8 (S)%100 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2645819MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92439770007
2645820
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 20 95 60-14097 3 3020ND19.0 19.5
1,1,1-Trichloroethane ug/L 20 91 60-14090 2 3020ND18.3 18.0
1,1,2,2-Tetrachloroethane ug/L 20 94 60-14093 1 3020ND18.7 18.6
1,1,2-Trichloroethane ug/L 20 90 60-14094 4 3020ND18.0 18.7
1,1-Dichloroethane ug/L 20 88 60-14088 1 3020ND17.6 17.5
1,1-Dichloroethene ug/L 20 94 60-14092 2 3020ND18.9 18.5
1,1-Dichloropropene ug/L 20 95 60-14092 3 3020ND19.0 18.4
1,2,3-Trichlorobenzene ug/L M12014860-140120 21 3020ND29.6 24.0
1,2,3-Trichloropropane ug/L 20 94 60-14093 1 3020ND18.8 18.6
1,2,4-Trichlorobenzene ug/L 20 119 60-140109 9 3020ND23.8 21.8
1,2,4-Trimethylbenzene ug/L 20 92 60-14090 3 3020ND18.4 17.9
1,2-Dibromo-3-
chloropropane ug/L 20 113 60-140100 12 3020ND22.7 20.1
1,2-Dibromoethane (EDB) ug/L 20 94 60-14098 5 3020ND18.7 19.7
1,2-Dichlorobenzene ug/L 20 94 60-14092 3 3020ND18.9 18.4
1,2-Dichloroethane ug/L 20 91 60-14087 4 3020ND18.1 17.4
1,2-Dichloropropane ug/L 20 90 60-14089 0 3020ND17.9 17.9
1,3,5-Trimethylbenzene ug/L 20 92 60-14092 0 3020ND18.5 18.5
1,3-Dichlorobenzene ug/L 20 95 60-14093 2 3020ND19.0 18.6
1,3-Dichloropropane ug/L 20 96 60-14098 1 3020ND19.3 19.6
1,4-Dichlorobenzene ug/L 20 93 60-14090 3 3020ND18.6 18.1
2,2-Dichloropropane ug/L 20 92 60-14092 0 3020ND18.4 18.4
2-Chlorotoluene ug/L 20 91 60-14091 0 3020ND18.3 18.3
4-Chlorotoluene ug/L 20 92 60-14091 1 3020ND18.3 18.2
Benzene ug/L 20 91 60-14091 0 3020ND18.3 18.2
Bromobenzene ug/L 20 95 60-14094 1 3020ND19.0 18.8
Bromochloromethane ug/L 20 87 60-14088 2 3020ND17.4 17.7
Bromodichloromethane ug/L 20 99 60-14098 1 3020ND19.8 19.7
Bromoform ug/L 20 96 60-14097 1 3020ND19.2 19.5
Bromomethane ug/L 20 112 60-140112 0 3020ND22.4 22.4
Carbon tetrachloride ug/L 20 94 60-14095 1 3020ND18.9 19.1
Chlorobenzene ug/L 20 92 60-14095 3 3020ND18.4 18.9
Chloroethane ug/L 20 107 60-140108 0 3020ND21.5 21.5
Chloroform ug/L 20 85 60-14085 1 3020ND16.9 17.0
Chloromethane ug/L 20 110 60-140114 3 3020ND22.1 22.8
cis-1,2-Dichloroethene ug/L 20 86 60-14087 1 3020ND17.2 17.3
cis-1,3-Dichloropropene ug/L 20 98 60-14098 0 3020ND19.6 19.6
Dibromochloromethane ug/L 20 94 60-14097 3 3020ND18.9 19.4
Dibromomethane ug/L 20 101 60-14099 3 3020ND20.3 19.7
Dichlorodifluoromethane ug/L 20 105 60-140104 1 3020ND21.1 20.8
Diisopropyl ether ug/L 20 87 60-14085 2 3020ND17.4 17.1
Ethylbenzene ug/L 20 94 60-14096 1 3020ND18.9 19.1
Hexachloro-1,3-butadiene ug/L 20 109 60-140101 8 3020ND21.9 20.2
Isopropylbenzene(Cumene)ug/L 20 94 60-14097 3 3020ND18.8 19.4
m&p-Xylene ug/L 40 94 60-14096 2 3040ND37.4 38.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2645819MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92439770007
2645820
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 20 87 60-14088 1 3020ND17.5 17.5
Methylene Chloride ug/L 20 84 60-14084 0 3020ND16.8 16.9
n-Butylbenzene ug/L 20 94 60-14089 5 3020ND18.8 17.9
n-Propylbenzene ug/L 20 94 60-14094 0 3020ND18.8 18.7
Naphthalene ug/L 20 135 60-140113 18 3020ND27.0 22.6
o-Xylene ug/L 20 92 60-14097 5 3020ND18.3 19.3
sec-Butylbenzene ug/L 20 98 60-14097 2 3020ND19.6 19.3
Styrene ug/L 20 92 60-14095 3 3020ND18.5 19.1
tert-Butylbenzene ug/L 20 82 60-14080 3 3020ND16.5 16.0
Tetrachloroethene ug/L 20 96 60-140102 6 3020ND19.2 20.3
Toluene ug/L 20 87 60-14088 1 3020ND17.5 17.7
trans-1,2-Dichloroethene ug/L 20 88 60-14091 2 3020ND17.7 18.1
trans-1,3-Dichloropropene ug/L 20 97 60-14098 1 3020ND19.5 19.6
Trichloroethene ug/L 20 93 60-14093 1 3020ND18.5 18.6
Trichlorofluoromethane ug/L 20 104 60-140104 0 3020ND20.7 20.8
Vinyl chloride ug/L 20 107 60-140108 1 3020ND21.5 21.6
1,2-Dichloroethane-d4 (S) %90 70-13090
4-Bromofluorobenzene (S) %96 70-13098
Toluene-d8 (S)%99 70-13097
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
490612
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92439770001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2646519
Associated Lab Samples:92439770001
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 08/06/19 15:340.25
1,1,1-Trichloroethane ug/L ND 0.50 08/06/19 15:340.25
1,1,2,2-Tetrachloroethane ug/L ND 0.50 08/06/19 15:340.25
1,1,2-Trichloroethane ug/L ND 0.50 08/06/19 15:340.25
1,1-Dichloroethane ug/L ND 0.50 08/06/19 15:340.25
1,1-Dichloroethene ug/L ND 0.50 08/06/19 15:340.25
1,1-Dichloropropene ug/L ND 0.50 08/06/19 15:340.25
1,2,3-Trichlorobenzene ug/L ND 2.0 08/06/19 15:341.0
1,2,3-Trichloropropane ug/L ND 0.50 08/06/19 15:340.25
1,2,4-Trichlorobenzene ug/L ND 2.0 08/06/19 15:341.0
1,2,4-Trimethylbenzene ug/L ND 0.50 08/06/19 15:340.25
1,2-Dibromo-3-chloropropane ug/L ND 1.0 08/06/19 15:340.50
1,2-Dibromoethane (EDB)ug/L ND 0.50 08/06/19 15:340.25
1,2-Dichlorobenzene ug/L ND 0.50 08/06/19 15:340.25
1,2-Dichloroethane ug/L ND 0.50 08/06/19 15:340.25
1,2-Dichloropropane ug/L ND 0.50 08/06/19 15:340.25
1,3,5-Trimethylbenzene ug/L ND 0.50 08/06/19 15:340.25
1,3-Dichlorobenzene ug/L ND 0.50 08/06/19 15:340.25
1,3-Dichloropropane ug/L ND 0.50 08/06/19 15:340.25
1,4-Dichlorobenzene ug/L ND 0.50 08/06/19 15:340.25
2,2-Dichloropropane ug/L ND 0.50 08/06/19 15:340.25
2-Chlorotoluene ug/L ND 0.50 08/06/19 15:340.25
4-Chlorotoluene ug/L ND 0.50 08/06/19 15:340.25
Benzene ug/L ND 0.50 08/06/19 15:340.25
Bromobenzene ug/L ND 0.50 08/06/19 15:340.25
Bromochloromethane ug/L ND 0.50 08/06/19 15:340.25
Bromodichloromethane ug/L ND 0.50 08/06/19 15:340.25
Bromoform ug/L ND 0.50 08/06/19 15:340.25
Bromomethane ug/L ND 5.0 08/06/19 15:342.5
Carbon tetrachloride ug/L ND 0.50 08/06/19 15:340.25
Chlorobenzene ug/L ND 0.50 08/06/19 15:340.25
Chloroethane ug/L ND 1.0 08/06/19 15:340.50
Chloroform ug/L ND 5.0 08/06/19 15:342.5
Chloromethane ug/L ND 1.0 08/06/19 15:340.50
cis-1,2-Dichloroethene ug/L ND 0.50 08/06/19 15:340.25
cis-1,3-Dichloropropene ug/L ND 0.50 08/06/19 15:340.25
Dibromochloromethane ug/L ND 0.50 08/06/19 15:340.25
Dibromomethane ug/L ND 0.50 08/06/19 15:340.25
Dichlorodifluoromethane ug/L ND 0.50 08/06/19 15:340.25
Diisopropyl ether ug/L ND 0.50 08/06/19 15:340.25
Ethylbenzene ug/L ND 0.50 08/06/19 15:340.25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2646519
Associated Lab Samples:92439770001
Matrix: Water
AnalyzedMDL
Hexachloro-1,3-butadiene ug/L ND 2.0 08/06/19 15:341.0
Isopropylbenzene (Cumene)ug/L ND 0.50 08/06/19 15:340.25
m&p-Xylene ug/L ND 1.0 08/06/19 15:340.50
Methyl-tert-butyl ether ug/L ND 0.50 08/06/19 15:340.25
Methylene Chloride ug/L ND 2.0 08/06/19 15:341.0
n-Butylbenzene ug/L ND 0.50 08/06/19 15:340.25
n-Propylbenzene ug/L ND 0.50 08/06/19 15:340.25
Naphthalene ug/L ND 2.0 08/06/19 15:341.0
o-Xylene ug/L ND 0.50 08/06/19 15:340.25
sec-Butylbenzene ug/L ND 0.50 08/06/19 15:340.25
Styrene ug/L ND 0.50 08/06/19 15:340.25
tert-Butylbenzene ug/L ND 0.50 08/06/19 15:340.25
Tetrachloroethene ug/L ND 0.50 08/06/19 15:340.25
Toluene ug/L ND 0.50 08/06/19 15:340.25
trans-1,2-Dichloroethene ug/L ND 0.50 08/06/19 15:340.25
trans-1,3-Dichloropropene ug/L ND 0.50 08/06/19 15:340.25
Trichloroethene ug/L ND 0.50 08/06/19 15:340.25
Trichlorofluoromethane ug/L ND 1.0 08/06/19 15:340.50
Vinyl chloride ug/L ND 1.0 08/06/19 15:340.50
1,2-Dichloroethane-d4 (S)%95 70-130 08/06/19 15:34
4-Bromofluorobenzene (S)%95 70-130 08/06/19 15:34
Toluene-d8 (S)%101 70-130 08/06/19 15:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2646520LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.050 98 60-140
1,1,1-Trichloroethane ug/L 45.650 91 60-140
1,1,2,2-Tetrachloroethane ug/L 47.850 96 60-140
1,1,2-Trichloroethane ug/L 46.150 92 60-140
1,1-Dichloroethane ug/L 43.250 86 60-140
1,1-Dichloroethene ug/L 45.650 91 60-140
1,1-Dichloropropene ug/L 46.550 93 60-140
1,2,3-Trichlorobenzene ug/L 60.450 121 60-140
1,2,3-Trichloropropane ug/L 47.950 96 60-140
1,2,4-Trichlorobenzene ug/L 54.250 108 60-140
1,2,4-Trimethylbenzene ug/L 45.650 91 60-140
1,2-Dibromo-3-chloropropane ug/L 53.750 107 60-140
1,2-Dibromoethane (EDB)ug/L 49.850 100 60-140
1,2-Dichlorobenzene ug/L 47.550 95 60-140
1,2-Dichloroethane ug/L 46.250 92 60-140
1,2-Dichloropropane ug/L 45.350 91 60-140
1,3,5-Trimethylbenzene ug/L 46.050 92 60-140
1,3-Dichlorobenzene ug/L 46.850 94 60-140
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 28 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2646520LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 48.650 97 60-140
1,4-Dichlorobenzene ug/L 45.950 92 60-140
2,2-Dichloropropane ug/L 46.150 92 60-140
2-Chlorotoluene ug/L 45.350 91 60-140
4-Chlorotoluene ug/L 45.550 91 60-140
Benzene ug/L 45.950 92 60-140
Bromobenzene ug/L 46.250 92 60-140
Bromochloromethane ug/L 45.950 92 60-140
Bromodichloromethane ug/L 50.350 101 60-140
Bromoform ug/L 52.550 105 60-140
Bromomethane ug/L 38.650 77 60-140
Carbon tetrachloride ug/L 46.350 93 60-140
Chlorobenzene ug/L 45.850 92 60-140
Chloroethane ug/L 43.650 87 60-140
Chloroform ug/L 42.850 86 60-140
Chloromethane ug/L 48.150 96 60-140
cis-1,2-Dichloroethene ug/L 43.150 86 60-140
cis-1,3-Dichloropropene ug/L 50.250 100 60-140
Dibromochloromethane ug/L 49.250 98 60-140
Dibromomethane ug/L 51.950 104 60-140
Dichlorodifluoromethane ug/L 49.350 99 60-140
Diisopropyl ether ug/L 44.050 88 60-140
Ethylbenzene ug/L 46.650 93 60-140
Hexachloro-1,3-butadiene ug/L 51.150 102 60-140
Isopropylbenzene (Cumene)ug/L 46.950 94 60-140
m&p-Xylene ug/L 94.6100 95 60-140
Methyl-tert-butyl ether ug/L 45.150 90 60-140
Methylene Chloride ug/L 41.750 83 60-140
n-Butylbenzene ug/L 45.550 91 60-140
n-Propylbenzene ug/L 45.850 92 60-140
Naphthalene ug/L 57.250 114 60-140
o-Xylene ug/L 47.950 96 60-140
sec-Butylbenzene ug/L 47.650 95 60-140
Styrene ug/L 47.550 95 60-140
tert-Butylbenzene ug/L 40.450 81 60-140
Tetrachloroethene ug/L 49.050 98 60-140
Toluene ug/L 44.550 89 60-140
trans-1,2-Dichloroethene ug/L 44.350 89 60-140
trans-1,3-Dichloropropene ug/L 50.350 101 60-140
Trichloroethene ug/L 46.650 93 60-140
Trichlorofluoromethane ug/L 48.050 96 60-140
Vinyl chloride ug/L 51.250 102 60-140
1,2-Dichloroethane-d4 (S)%91 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%96 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2646521MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92439321003
2646522
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 200 96 60-14089 7 30200ND191 178
1,1,1-Trichloroethane ug/L 200 93 60-14085 9 30200ND187 170
1,1,2,2-Tetrachloroethane ug/L 200 92 60-14088 5 30200ND185 177
1,1,2-Trichloroethane ug/L 200 94 60-14085 10 30200ND188 170
1,1-Dichloroethane ug/L 200 92 60-14084 9 30200ND184 168
1,1-Dichloroethene ug/L 200 98 60-14089 10 30200ND196 177
1,1-Dichloropropene ug/L 200 96 60-14088 8 30200ND192 177
1,2,3-Trichlorobenzene ug/L 200 94 60-140101 6 30200ND189 201
1,2,3-Trichloropropane ug/L 200 96 60-14093 4 30200ND193 185
1,2,4-Trichlorobenzene ug/L 200 93 60-14093 0 30200ND186 186
1,2,4-Trimethylbenzene ug/L 200 111 60-14080 5 3020010301260 1190
1,2-Dibromo-3-
chloropropane ug/L 200 98 60-14095 3 30200ND197 190
1,2-Dibromoethane (EDB) ug/L 200 99 60-14090 9 302008.5 206 188
1,2-Dichlorobenzene ug/L 200 91 60-14083 9 30200ND182 165
1,2-Dichloroethane ug/L 200 92 60-14085 8 302006.9 191 176
1,2-Dichloropropane ug/L 200 93 60-14086 8 30200ND187 172
1,3,5-Trimethylbenzene ug/L 200 99 60-14082 8 30200269468 433
1,3-Dichlorobenzene ug/L 200 92 60-14082 11 30200ND183 165
1,3-Dichloropropane ug/L 200 96 60-14089 8 30200ND192 178
1,4-Dichlorobenzene ug/L 200 91 60-14080 13 30200ND181 159
2,2-Dichloropropane ug/L 200 81 60-14074 10 30200ND163 148
2-Chlorotoluene ug/L 200 96 60-14088 8 30200ND192 177
4-Chlorotoluene ug/L 200 91 60-14081 11 30200ND181 163
Benzene ug/L 200 101 60-14086 5 30200464667 636
Bromobenzene ug/L 200 93 60-14085 9 30200ND186 169
Bromochloromethane ug/L 200 92 60-14085 7 30200ND184 170
Bromodichloromethane ug/L 200 98 60-14088 10 30200ND195 176
Bromoform ug/L 200 96 60-14090 7 30200ND193 179
Bromomethane ug/L M12005560-14057 4 30200ND109 113
Carbon tetrachloride ug/L 200 92 60-14085 8 30200ND184 170
Chlorobenzene ug/L 200 94 60-14086 9 30200ND188 171
Chloroethane ug/L 200 110 60-140107 3 30200ND221 213
Chloroform ug/L 200 88 60-14084 5 30200ND177 167
Chloromethane ug/L 200 101 60-14092 9 30200ND201 183
cis-1,2-Dichloroethene ug/L 200 89 60-14081 9 30200ND177 162
cis-1,3-Dichloropropene ug/L 200 95 60-14087 9 30200ND190 174
Dibromochloromethane ug/L 200 95 60-14087 9 30200ND189 174
Dibromomethane ug/L 200 100 60-14096 5 30200ND201 191
Dichlorodifluoromethane ug/L 200 107 60-14095 12 30200ND214 190
Diisopropyl ether ug/L 200 89 60-14081 9 302007.8 186 170
Ethylbenzene ug/L 200 104 60-14093 4 30200335543 521
Hexachloro-1,3-butadiene ug/L 200 92 60-14083 10 30200ND184 166
Isopropylbenzene(Cumene)ug/L 200 95 60-14087 7 3020041.8 232 215
m&p-Xylene ug/L 400 100 60-14090 6 30400288688 649
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
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Page 30 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2646521MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92439321003
2646522
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 200 92 60-14083 4 30200217401 384
Methylene Chloride ug/L 200 91 60-14083 9 30200ND181 165
n-Butylbenzene ug/L 200 100 60-14090 10 30200ND199 180
n-Propylbenzene ug/L 200 93 60-14081 8 30200107293 269
Naphthalene ug/L 200 88 60-140110 10 30200226402 446
o-Xylene ug/L 200 98 60-14088 5 30200211407 387
sec-Butylbenzene ug/L 200 99 60-14089 10 30200ND198 178
Styrene ug/L 200 94 60-14088 7 30200ND188 176
tert-Butylbenzene ug/L 200 82 60-14073 12 30200ND164 146
Tetrachloroethene ug/L 200 95 60-14089 7 30200ND191 178
Toluene ug/L 200 93 60-14084 5 30200135321 304
trans-1,2-Dichloroethene ug/L 200 94 60-14085 9 30200ND187 170
trans-1,3-Dichloropropene ug/L 200 93 60-14084 10 30200ND187 168
Trichloroethene ug/L 200 92 60-14086 6 30200ND183 172
Trichlorofluoromethane ug/L 200 109 60-14098 10 30200ND217 196
Vinyl chloride ug/L 200 109 60-140103 6 30200ND218 206
1,2-Dichloroethane-d4 (S) %98 70-13096
4-Bromofluorobenzene (S) %97 70-13099
Toluene-d8 (S)%98 70-13095
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
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Page 31 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
490614
SM 6200B
SM 6200B
6200B MSV
Associated Lab Samples: 92439770002, 92439770003, 92439770008
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2646532
Associated Lab Samples:92439770002, 92439770003, 92439770008
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 0.50 08/07/19 02:260.25
1,1,1-Trichloroethane ug/L ND 0.50 08/07/19 02:260.25
1,1,2,2-Tetrachloroethane ug/L ND 0.50 08/07/19 02:260.25
1,1,2-Trichloroethane ug/L ND 0.50 08/07/19 02:260.25
1,1-Dichloroethane ug/L ND 0.50 08/07/19 02:260.25
1,1-Dichloroethene ug/L ND 0.50 08/07/19 02:260.25
1,1-Dichloropropene ug/L ND 0.50 08/07/19 02:260.25
1,2,3-Trichlorobenzene ug/L ND 2.0 08/07/19 02:261.0
1,2,3-Trichloropropane ug/L ND 0.50 08/07/19 02:260.25
1,2,4-Trichlorobenzene ug/L ND 2.0 08/07/19 02:261.0
1,2,4-Trimethylbenzene ug/L ND 0.50 08/07/19 02:260.25
1,2-Dibromo-3-chloropropane ug/L ND 1.0 08/07/19 02:260.50
1,2-Dibromoethane (EDB)ug/L ND 0.50 08/07/19 02:260.25
1,2-Dichlorobenzene ug/L ND 0.50 08/07/19 02:260.25
1,2-Dichloroethane ug/L ND 0.50 08/07/19 02:260.25
1,2-Dichloropropane ug/L ND 0.50 08/07/19 02:260.25
1,3,5-Trimethylbenzene ug/L ND 0.50 08/07/19 02:260.25
1,3-Dichlorobenzene ug/L ND 0.50 08/07/19 02:260.25
1,3-Dichloropropane ug/L ND 0.50 08/07/19 02:260.25
1,4-Dichlorobenzene ug/L ND 0.50 08/07/19 02:260.25
2,2-Dichloropropane ug/L ND 0.50 08/07/19 02:260.25
2-Chlorotoluene ug/L ND 0.50 08/07/19 02:260.25
4-Chlorotoluene ug/L ND 0.50 08/07/19 02:260.25
Benzene ug/L ND 0.50 08/07/19 02:260.25
Bromobenzene ug/L ND 0.50 08/07/19 02:260.25
Bromochloromethane ug/L ND 0.50 08/07/19 02:260.25
Bromodichloromethane ug/L ND 0.50 08/07/19 02:260.25
Bromoform ug/L ND 0.50 08/07/19 02:260.25
Bromomethane ug/L ND 5.0 08/07/19 02:262.5
Carbon tetrachloride ug/L ND 0.50 08/07/19 02:260.25
Chlorobenzene ug/L ND 0.50 08/07/19 02:260.25
Chloroethane ug/L ND 1.0 08/07/19 02:260.50
Chloroform ug/L ND 5.0 08/07/19 02:262.5
Chloromethane ug/L ND 1.0 08/07/19 02:260.50
cis-1,2-Dichloroethene ug/L ND 0.50 08/07/19 02:260.25
cis-1,3-Dichloropropene ug/L ND 0.50 08/07/19 02:260.25
Dibromochloromethane ug/L ND 0.50 08/07/19 02:260.25
Dibromomethane ug/L ND 0.50 08/07/19 02:260.25
Dichlorodifluoromethane ug/L ND 0.50 08/07/19 02:260.25
Diisopropyl ether ug/L ND 0.50 08/07/19 02:260.25
Ethylbenzene ug/L ND 0.50 08/07/19 02:260.25
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
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Huntersville, NC 28078
[phone]
Page 32 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2646532
Associated Lab Samples:92439770002, 92439770003, 92439770008
Matrix: Water
AnalyzedMDL
Hexachloro-1,3-butadiene ug/L ND 2.0 08/07/19 02:261.0
Isopropylbenzene (Cumene)ug/L ND 0.50 08/07/19 02:260.25
m&p-Xylene ug/L ND 1.0 08/07/19 02:260.50
Methyl-tert-butyl ether ug/L ND 0.50 08/07/19 02:260.25
Methylene Chloride ug/L ND 2.0 08/07/19 02:261.0
n-Butylbenzene ug/L ND 0.50 08/07/19 02:260.25
n-Propylbenzene ug/L ND 0.50 08/07/19 02:260.25
Naphthalene ug/L ND 2.0 08/07/19 02:261.0
o-Xylene ug/L ND 0.50 08/07/19 02:260.25
sec-Butylbenzene ug/L ND 0.50 08/07/19 02:260.25
Styrene ug/L ND 0.50 08/07/19 02:260.25
tert-Butylbenzene ug/L ND 0.50 08/07/19 02:260.25
Tetrachloroethene ug/L ND 0.50 08/07/19 02:260.25
Toluene ug/L ND 0.50 08/07/19 02:260.25
trans-1,2-Dichloroethene ug/L ND 0.50 08/07/19 02:260.25
trans-1,3-Dichloropropene ug/L ND 0.50 08/07/19 02:260.25
Trichloroethene ug/L ND 0.50 08/07/19 02:260.25
Trichlorofluoromethane ug/L ND 1.0 08/07/19 02:260.50
Vinyl chloride ug/L ND 1.0 08/07/19 02:260.50
1,2-Dichloroethane-d4 (S)%94 70-130 08/07/19 02:26
4-Bromofluorobenzene (S)%97 70-130 08/07/19 02:26
Toluene-d8 (S)%96 70-130 08/07/19 02:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2646533LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 49.050 98 60-140
1,1,1-Trichloroethane ug/L 43.250 86 60-140
1,1,2,2-Tetrachloroethane ug/L 47.750 95 60-140
1,1,2-Trichloroethane ug/L 48.450 97 60-140
1,1-Dichloroethane ug/L 42.150 84 60-140
1,1-Dichloroethene ug/L 43.150 86 60-140
1,1-Dichloropropene ug/L 45.150 90 60-140
1,2,3-Trichlorobenzene ug/L 60.250 120 60-140
1,2,3-Trichloropropane ug/L 48.550 97 60-140
1,2,4-Trichlorobenzene ug/L 53.150 106 60-140
1,2,4-Trimethylbenzene ug/L 44.450 89 60-140
1,2-Dibromo-3-chloropropane ug/L 55.450 111 60-140
1,2-Dibromoethane (EDB)ug/L 50.350 101 60-140
1,2-Dichlorobenzene ug/L 47.050 94 60-140
1,2-Dichloroethane ug/L 46.150 92 60-140
1,2-Dichloropropane ug/L 45.150 90 60-140
1,3,5-Trimethylbenzene ug/L 44.650 89 60-140
1,3-Dichlorobenzene ug/L 46.350 93 60-140
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
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Huntersville, NC 28078
[phone]
Page 33 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2646533LABORATORY CONTROL SAMPLE:
LCSSpike
1,3-Dichloropropane ug/L 48.750 97 60-140
1,4-Dichlorobenzene ug/L 45.750 91 60-140
2,2-Dichloropropane ug/L 38.250 76 60-140
2-Chlorotoluene ug/L 43.950 88 60-140
4-Chlorotoluene ug/L 44.450 89 60-140
Benzene ug/L 45.050 90 60-140
Bromobenzene ug/L 45.950 92 60-140
Bromochloromethane ug/L 44.650 89 60-140
Bromodichloromethane ug/L 49.250 98 60-140
Bromoform ug/L 53.650 107 60-140
Bromomethane ug/L 42.050 84 60-140
Carbon tetrachloride ug/L 44.850 90 60-140
Chlorobenzene ug/L 45.250 90 60-140
Chloroethane ug/L 41.750 83 60-140
Chloroform ug/L 42.250 84 60-140
Chloromethane ug/L 45.050 90 60-140
cis-1,2-Dichloroethene ug/L 42.150 84 60-140
cis-1,3-Dichloropropene ug/L 48.950 98 60-140
Dibromochloromethane ug/L 50.750 101 60-140
Dibromomethane ug/L 52.150 104 60-140
Dichlorodifluoromethane ug/L 46.450 93 60-140
Diisopropyl ether ug/L 43.350 87 60-140
Ethylbenzene ug/L 45.750 91 60-140
Hexachloro-1,3-butadiene ug/L 47.450 95 60-140
Isopropylbenzene (Cumene)ug/L 46.150 92 60-140
m&p-Xylene ug/L 92.0100 92 60-140
Methyl-tert-butyl ether ug/L 44.950 90 60-140
Methylene Chloride ug/L 41.450 83 60-140
n-Butylbenzene ug/L 43.350 87 60-140
n-Propylbenzene ug/L 44.750 89 60-140
Naphthalene ug/L 57.350 115 60-140
o-Xylene ug/L 46.550 93 60-140
sec-Butylbenzene ug/L 46.050 92 60-140
Styrene ug/L 47.550 95 60-140
tert-Butylbenzene ug/L 39.450 79 60-140
Tetrachloroethene ug/L 45.750 91 60-140
Toluene ug/L 44.750 89 60-140
trans-1,2-Dichloroethene ug/L 42.850 86 60-140
trans-1,3-Dichloropropene ug/L 49.350 99 60-140
Trichloroethene ug/L 45.150 90 60-140
Trichlorofluoromethane ug/L 45.750 91 60-140
Vinyl chloride ug/L 48.750 97 60-140
1,2-Dichloroethane-d4 (S)%92 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
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Huntersville, NC 28078
[phone]
Page 34 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2646534MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92439316001
2646535
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/L 2000 99 60-14097 2 302000ND1980 1930
1,1,1-Trichloroethane ug/L 2000 99 60-14098 1 302000ND1980 1960
1,1,2,2-Tetrachloroethane ug/L 2000 95 60-14091 4 302000ND1900 1820
1,1,2-Trichloroethane ug/L 2000 96 60-14094 2 302000ND1920 1890
1,1-Dichloroethane ug/L 2000 96 60-14093 3 302000ND1920 1860
1,1-Dichloroethene ug/L 2000 104 60-140100 4 302000ND2090 2000
1,1-Dichloropropene ug/L 2000 103 60-140100 2 302000ND2060 2010
1,2,3-Trichlorobenzene ug/L 2000 114 60-140108 6 302000ND2280 2150
1,2,3-Trichloropropane ug/L 2000 95 60-14094 1 302000ND1900 1880
1,2,4-Trichlorobenzene ug/L 2000 104 60-14099 5 302000ND2070 1970
1,2,4-Trimethylbenzene ug/L M1200010160-1400 302000ND2010 ND
1,2-Dibromo-3-
chloropropane ug/L 2000 100 60-14099 1 302000ND2010 1990
1,2-Dibromoethane (EDB) ug/L 2000 102 60-14096 6 302000ND2030 1910
1,2-Dichlorobenzene ug/L 2000 94 60-14093 1 302000ND1890 1860
1,2-Dichloroethane ug/L 2000 99 60-14091 8 302000ND1980 1820
1,2-Dichloropropane ug/L 2000 93 60-14091 3 302000ND1870 1820
1,3,5-Trimethylbenzene ug/L 2000 96 60-14094 2 302000ND1920 1880
1,3-Dichlorobenzene ug/L 2000 94 60-14094 1 302000ND1890 1870
1,3-Dichloropropane ug/L 2000 98 60-14097 1 302000ND1970 1940
1,4-Dichlorobenzene ug/L 2000 94 60-14093 1 302000ND1870 1860
2,2-Dichloropropane ug/L 2000 77 60-14078 0 302000ND1550 1550
2-Chlorotoluene ug/L 2000 95 60-14094 1 302000ND1900 1880
4-Chlorotoluene ug/L 2000 95 60-14093 2 302000ND1900 1860
Benzene ug/L 2000 98 60-14096 2 302000ND1960 1920
Bromobenzene ug/L 2000 97 60-14096 0 302000ND1930 1920
Bromochloromethane ug/L 2000 95 60-14094 1 302000ND1900 1880
Bromodichloromethane ug/L 2000 99 60-140102 4 302000ND1970 2050
Bromoform ug/L 2000 96 60-14095 1 302000ND1930 1910
Bromomethane ug/L M120004660-14046 0 302000ND1280 1280
Carbon tetrachloride ug/L 2000 99 60-14097 2 302000ND1980 1940
Chlorobenzene ug/L 2000 97 60-14094 3 302000ND1940 1890
Chloroethane ug/L 2000 119 60-140109 9 302000ND2380 2180
Chloroform ug/L 2000 92 60-14093 2 302000ND1840 1870
Chloromethane ug/L 2000 107 60-140101 6 302000ND2150 2030
cis-1,2-Dichloroethene ug/L 2000 94 60-14091 3 302000ND1880 1820
cis-1,3-Dichloropropene ug/L 2000 98 60-14096 1 302000ND1950 1920
Dibromochloromethane ug/L 2000 96 60-14095 1 302000ND1920 1910
Dibromomethane ug/L 2000 109 60-140102 6 302000ND2180 2050
Dichlorodifluoromethane ug/L 2000 110 60-140110 1 302000ND2190 2210
Diisopropyl ether ug/L 2000 92 60-14090 2 302000ND1830 1800
Ethylbenzene ug/L 2000 99 60-14096 3 302000ND1970 1920
Hexachloro-1,3-butadiene ug/L 2000 95 60-14092 3 302000ND1900 1850
Isopropylbenzene(Cumene)ug/L 2000 99 60-14097 2 302000ND1980 1940
m&p-Xylene ug/L 4000 100 60-14096 4 304000ND3980 3840
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
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[phone]
Page 35 of 41
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2646534MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92439316001
2646535
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Methyl-tert-butyl ether ug/L 2000 94 60-14092 2 302000ND1890 1850
Methylene Chloride ug/L 2000 93 60-14090 3 302000ND1860 1800
n-Butylbenzene ug/L 2000 90 60-14090 0 302000ND1800 1800
n-Propylbenzene ug/L 2000 97 60-14097 1 302000ND1950 1930
Naphthalene ug/L 2000 131 60-140111 17 302000ND2630 2210
o-Xylene ug/L 2000 100 60-14096 4 302000ND1990 1910
sec-Butylbenzene ug/L 2000 100 60-14099 1 302000ND2010 1980
Styrene ug/L 2000 97 60-14095 2 302000ND1940 1900
tert-Butylbenzene ug/L 2000 86 60-14084 2 302000ND1710 1670
Tetrachloroethene ug/L 2000 102 60-14098 4 302000ND2040 1950
Toluene ug/L 2000 81 60-14074 1 302000851010100 9990
trans-1,2-Dichloroethene ug/L 2000 98 60-14096 1 302000ND1950 1930
trans-1,3-Dichloropropene ug/L 2000 97 60-14094 4 302000ND1940 1870
Trichloroethene ug/L 2000 99 60-14098 1 302000ND1980 1960
Trichlorofluoromethane ug/L 2000 116 60-140111 4 302000ND2330 2230
Vinyl chloride ug/L 2000 115 60-140113 2 302000ND2310 2260
1,2-Dichloroethane-d4 (S) %94 70-13097
4-Bromofluorobenzene (S) %100 70-13097
Toluene-d8 (S)%101 70-13098
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
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Huntersville, NC 28078
[phone]
Page 36 of 41
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 08/08/2019 01:06 PM
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[phone]
Page 37 of 41
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92439770
NCDEQ KUNTRY KORNER
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92439770001 490612MW-2 SM 6200B
92439770002 490614MW-4 SM 6200B
92439770003 490614MW-8 SM 6200B
92439770004 490429WSW-2 SM 6200B
92439770005 490429WSW-3 SM 6200B
92439770006 490429WSW-4 SM 6200B
92439770007 490429WSW-7 SM 6200B
92439770008 490614WSW-8 SM 6200B
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 38 of 41
Page 39 of 41
Page 40 of 41
Page 41 of 41

APPENDIX D