WI-835_5675_CA_RPTS_20200204_GWM Letter Report

WithersRavenel
Our People. Your Success. 
  115 MacKenan Drive | Cary, NC 27511 
t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C‐0832 
Asheville | Cary | Greensboro | Pittsboro | Raleigh | Wilmington 

February 4, 2020 

State of North Carolina 
Department of Environmental Quality 
Federal & State Lead Program 
Division of Waste Management‐Underground Storage Tank Section 
1646 Mail Service Center 
Raleigh, North Carolina 27699‐1646 

Attn: Mr. Scott Ryals, PE 

Reference:   Groundwater Monitoring Letter Report 
Glenn Parker Property 
7102 Ocean Highway 
Sunset Beach, Brunswick County, North Carolina 
UST # WI‐835 
Groundwater Incident #5675 
WR Project Number: 02170214.48 

Dear Mr. Ryals: 

WithersRavenel, Inc. (WR) has prepared this letter report for groundwater and supply well 
sampling conducted at the Glenn Parker Property site located at 7102 Ocean Highway in Sunset 
Beach, Brunswick County, North Carolina. These activities were completed under task 
authorization (TA) 03 in association with NCDEQ Contract # N17005, and included the purging 
and sampling of monitoring wells MW‐13 and MW‐15, as well as the purging and sampling of 
supply well WSW‐1. WR personnel mobilized to the subject site on January 9, 2020 and 
completed these sampling activities as outlined below. 

Groundwater Sampling  

Groundwater monitoring wells MW‐13 and MW‐15 were gauged using a decontaminated 
electronic water level probe. The depths to water within these wells were measured from the 
wells’ top of casing (TOC) to the upper surface of groundwater. Depths to groundwater within 
the wells ranged from 2.64 ft beneath TOC (MW‐13) to 2.74 ft beneath TOC (MW‐15). No free 
product or petroleum sheens were noted in either of the wells.    

WithersRavenel
Our People. Your Success. 

Glenn Parker Property Incident Number: 5675  WR Project # 02170214.48 
Letter Report ‐ Groundwater Monitoring  February 4, 2020 

Following gauging, wells MW‐13 and MW‐15 were purged a minimum of three volumes of water 
in preparation for sampling. The wells were purged and ultimately sampled using separate, new 
polyethylene (PE) bailers. Following purging and adequate recharge of groundwater within the 
wells, samples were decanted from the dedicated bailers directly into laboratory‐prepared 
sample containers holding appropriate preservative as required.   

The samples were placed immediately into a chilled cooler, transported under proper chain‐of‐
custody (COC) protocol, and ultimately submitted to Waypoint Analytical, LLC (Waypoint), 
formerly Prism Laboratories, Inc. (Prism) for analysis of volatile organic compounds (VOCs) by 
Standard Method (SM) 6200B.  

Supply Well Sampling  

Also, under the current TA, WR purged and sampled on‐site supply well WSW‐1. The well was 
purged by allowing the associated well pump to run continuously for a minimum of ten (10) 
minutes, after which the sample was decanted directly from the sample point into laboratory‐
prepared sample containers holding appropriate preservative as required.   

This sample was also relinquished to Waypoint for testing by Standard Method (SM) 6200B.   

Laboratory Results 

Analytical results for groundwater samples collected from monitoring wells MW‐13 and MW‐15 
showed the presence of isopropylbenzene (cumene) in MW‐15 at a concentration above its 
laboratory method detection limit (MDL) for SM6200B. All other target compounds were below 
their respective MDLs. This is an increase from prior sampling events.   

Results for supply well sample WSW‐1 showed the presence of several targeted compounds at 
levels above their respective laboratory MDLs. Benzene and 1,2‐dichloroethane were both 
reported in the sample at levels above their respective NC 2L Standards. The concentration of 
benzene in the sample was also in excess of the US EPA Region IV Maximum Contaminant Level 
(MCL).   

Data for samples obtained from site monitoring wells and WSW‐1 on January 9, 2020 are shown 
below: 

WithersRavenel
Our People. Your Success. 

Glenn Parker Property Incident Number: 5675  WR Project # 02170214.48 
Letter Report ‐ Groundwater Monitoring  February 4, 2020 

Current data for WSW‐1 shows a 25% decrease in total VOC concentrations in comparison to 
those of December 2018. The water supply well is reportedly only used to operate the 
bathrooms and wash golf carts. 

Field notes and site photos for the January 2020 sampling event are included in Attachment A.  
The laboratory analytical report is provided in Attachment B. 
 Compound Name1,2‐Dichloroethane Benzene Ethylbenzene Isopropylbenzene (Cumene) Toluene Xylenes, total Collected
MW‐13 01/09/20 <0.066  <0.048  <0.061  <0.054  <0.044  <0.15 
MW‐15 01/09/20 <0.066  <0.5  <0.5 0.98 <0.044  <1.5 
WSW‐1 01/09/20 1.3 170 8 <0.054 26 32
0.4 1 600 70 600 500
400 5000 84500 25000 260000 85500
5 5 700 NL 1000 NL
Notes:
1)
2)
3)
4)
5)
6)
Result = Result Exceeds Laboratory Detection Limits
Result = Result Exceeds 2L Standard
Result = Result Exceeds 2L & MCL Values
NC GCL
US EPA MCL = Maximum Contaminant Level established by US EPA, Region IV 
(Applies only to supply well sample)
Summary of Analytical Results
Analytical Method
Sample ID
ug/L
NC 2L Standard
US EPA MCL
SM6200B
NL = "No regulatory level established"
All results provided in ug/L (micrograms per liter) or parts per billion
Compounds analyzed for by laboratory but not listed were not detected above 
laboratory detection limits. See the laboratory report included in the Appendix for a 
full list of constituents. 
NC 2L Standard ‐ North Carolina Groundwater Quality Standard as per NC 
Administrative Code 15A NCAC 02L (Table includes "interim" standards)
GCLs for Groundwater = NCDEQ UST Section Gross Contamination Levels for 
Groundwater
WithersRavenel
Our People. Your Success. 

Glenn Parker Property Incident Number: 5675  WR Project # 02170214.48 
Letter Report ‐ Groundwater Monitoring  February 4, 2020 

WithersRavenel appreciates the opportunity to be of service to the Federal & State Lead 
Program. Should you have any questions regarding the attached, please do not hesitate to 
contact Matthew James at (919) 469‐3340. 
Cordially, 
WithersRavenel

  Sandra Miller G. Matthew James, P.G. 
Project Environmental Scientist III Senior Geologist 

Attachments: Field Notes, Site Photographs, and Laboratory Analytical Results    

ATTACHMENT A 

FIELD NOTES & SITE PHOTOGRAPHS 

Frame No. 1 

Description:  View of front of building, facing northeast. 

Frame No. 2 

Description:  View of the eastern side of the building. 
Frame No. 3 

Description:  View of MW‐13.  

Frame No. 4 

Description:  View of MW‐15. 
Frame No. 5 

Description:  View of WSW‐1 spigot. 

ATTACHMENT B 

LABORATORY ANALYTICAL REPORT & CHAIN‐OF‐CUSTODY 

This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Case Narrative
1/24/20 10:24
Withers & Ravenel
Matt James
115 Mackenan Dr. BUILDING 117
Cary, NC 27511
Project: Glenn Parker Property
Project No.: 02170214.48
Lab Submittal Date: 01/14/2020
Work Order: 0010187
Please call if you have any questions relating to this analytical report.
Respectfully,
WAYPOINT ANALYTICAL
Project Management Manager
Reviewed ByAngela D. Overcash Angela D. Overcash
Project Management Manager
Data Qualifiers Key Reference:
M Matrix spike outside of the control limits.
Method Detection LimitMDL
Below Reporting LimitBRL
Relative Percent DifferenceRPD
*Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Sample Receipt Summary
01/24/2020
Work Order: 0010187
Client Sample ID MatrixLab Sample ID Date/Time Sampled Date/Time Received
0010187-01 01/09/20 13:45MW-13 01/14/20 14:25Water
0010187-02 01/09/20 14:10MW-15 01/14/20 14:25Water
0010187-03 01/09/20 14:30WSW-1 01/14/20 14:25Water
Samples were received in good condition at 2.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Client ID ResultParameterMethod UnitsWaypoint ID
Work Order: 0010187
01/24/2020
Summary of Detections
0.98 ug/L0010187-02 MW-15 Isopropylbenzene (Cumene)*SM6200 B
1.3 ug/L0010187-03 WSW-1 1,2-Dichloroethane *SM6200 B
170 ug/L0010187-03 WSW-1 Benzene *SM6200 B
8.0 ug/L0010187-03 WSW-1 Ethylbenzene *SM6200 B
18 ug/L0010187-03 WSW-1 m,p-Xylenes *SM6200 B
14 ug/L0010187-03 WSW-1 o-Xylene *SM6200 B
26 ug/L0010187-03 WSW-1 Toluene *SM6200 B
32 ug/L0010187-03 WSW-1 Xylenes, total *SM6200 B
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/24/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Glenn Parker PropertyWithers & Ravenel
Cary, NC 27511
Attn: Matt James
Sample Matrix: Water
Client Sample ID: MW-13
Sample ID: 0010187-01
Work Order: 0010187
Time Collected: 01/09/20 13:45
Time Submitted: 01/14/20 14:25
02170214.48
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A027812.0 1/17/20 14:45 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A027812.0 1/17/20 14:45 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A02781101/17/20 14:45 JLBug/L 0.31Acetone
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.048Benzene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.040Bromoform
BRL *SM6200 B P0A027811.0 1/17/20 14:45 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.076Chloroform
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0A027811.0 1/17/20 14:45 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A027812001/17/20 14:45 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/24/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Glenn Parker PropertyWithers & Ravenel
Cary, NC 27511
Attn: Matt James
Sample Matrix: Water
Client Sample ID: MW-13
Sample ID: 0010187-01
Work Order: 0010187
Time Collected: 01/09/20 13:45
Time Submitted: 01/14/20 14:25
02170214.48
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0A027812.0 1/17/20 14:45 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A027811.0 1/17/20 14:45 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A027811.0 1/17/20 14:45 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A027815.0 1/17/20 14:45 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A027811.0 1/17/20 14:45 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A027812.0 1/17/20 14:45 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0A027811.0 1/17/20 14:45 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A027811.0 1/17/20 14:45 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.047Styrene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.044Toluene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A027815.0 1/17/20 14:45 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0A027810.50 1/17/20 14:45 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0A027811.5 1/17/20 14:45 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13097 %4-Bromofluorobenzene
70-13094 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/24/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Glenn Parker PropertyWithers & Ravenel
Cary, NC 27511
Attn: Matt James
Sample Matrix: Water
Client Sample ID: MW-15
Sample ID: 0010187-02
Work Order: 0010187
Time Collected: 01/09/20 14:10
Time Submitted: 01/14/20 14:25
02170214.48
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A027812.0 1/17/20 15:10 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.0761,2-Dichlorobenzene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A027812.0 1/17/20 15:10 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A02781101/17/20 15:10 JLBug/L 0.31Acetone
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.048Benzene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.040Bromoform
BRL *SM6200 B P0A027811.0 1/17/20 15:10 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.076Chloroform
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0A027811.0 1/17/20 15:10 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A027812001/17/20 15:10 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/24/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Glenn Parker PropertyWithers & Ravenel
Cary, NC 27511
Attn: Matt James
Sample Matrix: Water
Client Sample ID: MW-15
Sample ID: 0010187-02
Work Order: 0010187
Time Collected: 01/09/20 14:10
Time Submitted: 01/14/20 14:25
02170214.48
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0A027812.0 1/17/20 15:10 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.050Isopropyl Ether
0.98 *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.054Isopropylbenzene (Cumene)
BRL *SM6200 B P0A027811.0 1/17/20 15:10 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A027811.0 1/17/20 15:10 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A027815.0 1/17/20 15:10 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A027811.0 1/17/20 15:10 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A027812.0 1/17/20 15:10 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0A027811.0 1/17/20 15:10 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A027811.0 1/17/20 15:10 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.087n-Propylbenzene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.047Styrene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.098Tetrachloroethylene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.044Toluene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A027815.0 1/17/20 15:10 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0A027810.50 1/17/20 15:10 JLBug/L 0.097Vinyl chloride
BRL *SM6200 B P0A027811.5 1/17/20 15:10 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13097 %4-Bromofluorobenzene
70-13093 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/24/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Glenn Parker PropertyWithers & Ravenel
Cary, NC 27511
Attn: Matt James
Sample Matrix: Water
Client Sample ID: WSW-1
Sample ID: 0010187-03
Work Order: 0010187
Time Collected: 01/09/20 14:30
Time Submitted: 01/14/20 14:25
02170214.48
Volatile Organic Compounds by GC/MS
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.111,1,1,2-Tetrachloroethane
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.0611,1,1-Trichloroethane
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.0361,1,2,2-Tetrachloroethane
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.0661,1,2-Trichloroethane
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.0831,1-Dichloroethane
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.0831,1-Dichloroethylene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.0511,1-Dichloropropylene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.401,2,3-Trichlorobenzene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.141,2,3-Trichloropropane
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.131,2,4-Trichlorobenzene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.0541,2,4-Trimethylbenzene
BRL *SM6200 B P0A027812.0 1/17/20 16:49 JLBug/L 0.171,2-Dibromo-3-chloropropane
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.0511,2-Dibromoethane
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.0761,2-Dichlorobenzene
1.3 *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.0661,2-Dichloroethane
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.111,2-Dichloropropane
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.0761,3,5-Trimethylbenzene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.0541,3-Dichlorobenzene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.0431,3-Dichloropropane
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.0501,4-Dichlorobenzene
BRL *SM6200 B P0A027812.0 1/17/20 16:49 JLBug/L 0.112,2-Dichloropropane
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.0662-Chlorotoluene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.0504-Chlorotoluene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.0894-Isopropyltoluene
BRL *SM6200 B P0A02781101/17/20 16:49 JLBug/L 0.31Acetone
170 *SM6200 B P0A0278105.0 1/17/20 17:14 JLBug/L 0.48Benzene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.057Bromobenzene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.14Bromochloromethane
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.062Bromodichloromethane
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.040Bromoform
BRL *SM6200 B P0A027811.0 1/17/20 16:49 JLBug/L 0.18Bromomethane
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.11Carbon Tetrachloride
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.062Chlorobenzene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.22Chloroethane
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.076Chloroform
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.079Chloromethane
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.056cis-1,2-Dichloroethylene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.079cis-1,3-Dichloropropylene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.081Dibromochloromethane
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.065Dibromomethane
BRL *SM6200 B P0A027811.0 1/17/20 16:49 JLBug/L 0.11Dichlorodifluoromethane
BRL *SM6200 B P0A027812001/17/20 16:49 JLBug/L 27Ethanol
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Laboratory Report
01/24/2020
ResultParameter Batch
ID
Report
Limit
Analysis
Date/Time
MethodDilution
Factor
Units MDL Analyst
115 Mackenan Dr. BUILDING 117 Project No.:
Project: Glenn Parker PropertyWithers & Ravenel
Cary, NC 27511
Attn: Matt James
Sample Matrix: Water
Client Sample ID: WSW-1
Sample ID: 0010187-03
Work Order: 0010187
Time Collected: 01/09/20 14:30
Time Submitted: 01/14/20 14:25
02170214.48
8.0 *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.061Ethylbenzene
BRL *SM6200 B P0A027812.0 1/17/20 16:49 JLBug/L 0.16Hexachlorobutadiene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.050Isopropyl Ether
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.054Isopropylbenzene (Cumene)
18 *SM6200 B P0A027811.0 1/17/20 16:49 JLBug/L 0.12m,p-Xylenes
BRL *SM6200 B P0A027811.0 1/17/20 16:49 JLBug/L 0.065Methyl Butyl Ketone (2-Hexanone)
BRL *SM6200 B P0A027815.0 1/17/20 16:49 JLBug/L 0.24Methyl Ethyl Ketone (2-Butanone)
BRL *SM6200 B P0A027811.0 1/17/20 16:49 JLBug/L 0.078Methyl Isobutyl Ketone
BRL *SM6200 B P0A027812.0 1/17/20 16:49 JLBug/L 0.083Methylene Chloride
BRL *SM6200 B P0A027811.0 1/17/20 16:49 JLBug/L 0.042Methyl-tert-Butyl Ether
BRL *SM6200 B P0A027811.0 1/17/20 16:49 JLBug/L 0.19Naphthalene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.076n-Butylbenzene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.087n-Propylbenzene
14 *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.044o-Xylene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.076sec-Butylbenzene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.047Styrene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.088tert-Butylbenzene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.098Tetrachloroethylene
26 *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.044Toluene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.070trans-1,2-Dichloroethylene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.12trans-1,3-Dichloropropylene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.078Trichloroethylene
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.062Trichlorofluoromethane
BRL *SM6200 B P0A027815.0 1/17/20 16:49 JLBug/L 0.060Vinyl acetate
BRL *SM6200 B P0A027810.50 1/17/20 16:49 JLBug/L 0.097Vinyl chloride
32 *SM6200 B P0A027811.5 1/17/20 16:49 JLBug/L 0.15Xylenes, total
Surrogate Recovery Control Limits
70-13096 %4-Bromofluorobenzene
70-13093 %Dibromofluoromethane
70-13097 %Toluene-d8
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/24/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.48
Project: Glenn Parker PropertyWithers & Ravenel
Cary, NC 27511
Attn: Matt James
Work Order: 0010187
Time Submitted: 1/14/2020 2:25:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0278 - SM6200 B
Blank (P0A0278-BLK1)Prepared & Analyzed: 01/17/20
1,1,1,2-Tetrachloroethane ug/LBRL0.50
1,1,1-Trichloroethane ug/LBRL0.50
1,1,2,2-Tetrachloroethane ug/LBRL0.50
1,1,2-Trichloroethane ug/LBRL0.50
1,1-Dichloroethane ug/LBRL0.50
1,1-Dichloroethylene ug/LBRL0.50
1,1-Dichloropropylene ug/LBRL0.50
1,2,3-Trichlorobenzene ug/LBRL0.50
1,2,3-Trichloropropane ug/LBRL0.50
1,2,4-Trichlorobenzene ug/LBRL0.50
1,2,4-Trimethylbenzene ug/LBRL0.50
1,2-Dibromo-3-chloropropane ug/LBRL2.0
1,2-Dibromoethane ug/LBRL0.50
1,2-Dichlorobenzene ug/LBRL0.50
1,2-Dichloroethane ug/LBRL0.50
1,2-Dichloropropane ug/LBRL0.50
1,3,5-Trimethylbenzene ug/LBRL0.50
1,3-Dichlorobenzene ug/LBRL0.50
1,3-Dichloropropane ug/LBRL0.50
1,4-Dichlorobenzene ug/LBRL0.50
2,2-Dichloropropane ug/LBRL2.0
2-Chlorotoluene ug/LBRL0.50
4-Chlorotoluene ug/LBRL0.50
4-Isopropyltoluene ug/LBRL0.50
Acetone ug/LBRL10
Benzene ug/LBRL0.50
Bromobenzene ug/LBRL0.50
Bromochloromethane ug/LBRL0.50
Bromodichloromethane ug/LBRL0.50
Bromoform ug/LBRL0.50
Bromomethane ug/LBRL1.0
Carbon Tetrachloride ug/LBRL0.50
Chlorobenzene ug/LBRL0.50
Chloroethane ug/LBRL0.50
Chloroform ug/LBRL0.50
Chloromethane ug/LBRL0.50
cis-1,2-Dichloroethylene ug/LBRL0.50
cis-1,3-Dichloropropylene ug/LBRL0.50
Dibromochloromethane ug/LBRL0.50
Dibromomethane ug/LBRL0.50
Dichlorodifluoromethane ug/LBRL1.0
Ethanol ug/LBRL200
Ethylbenzene ug/LBRL0.50
Hexachlorobutadiene ug/LBRL2.0
Isopropyl Ether ug/LBRL0.50
Isopropylbenzene (Cumene)ug/LBRL0.50
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/24/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.48
Project: Glenn Parker PropertyWithers & Ravenel
Cary, NC 27511
Attn: Matt James
Work Order: 0010187
Time Submitted: 1/14/2020 2:25:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0278 - SM6200 B
Blank (P0A0278-BLK1)Prepared & Analyzed: 01/17/20
m,p-Xylenes ug/LBRL1.0
Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0
Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0
Methyl Isobutyl Ketone ug/LBRL1.0
Methylene Chloride ug/LBRL2.0
Methyl-tert-Butyl Ether ug/LBRL1.0
Naphthalene ug/LBRL1.0
n-Butylbenzene ug/LBRL0.50
n-Propylbenzene ug/LBRL0.50
o-Xylene ug/LBRL0.50
sec-Butylbenzene ug/LBRL0.50
Styrene ug/LBRL0.50
tert-Butylbenzene ug/LBRL0.50
Tetrachloroethylene ug/LBRL0.50
Toluene ug/LBRL0.50
trans-1,2-Dichloroethylene ug/LBRL0.50
trans-1,3-Dichloropropylene ug/LBRL0.50
Trichloroethylene ug/LBRL0.50
Trichlorofluoromethane ug/LBRL0.50
Vinyl acetate ug/LBRL5.0
Vinyl chloride ug/LBRL0.50
Xylenes, total ug/LBRL1.5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9547.4
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9446.8
ug/L 50.00 70-130Surrogate: Toluene-d8 9748.5
LCS (P0A0278-BS1)Prepared & Analyzed: 01/17/20
1,1,1,2-Tetrachloroethane ug/L17.0 0.50 20.00 70-13085
1,1,1-Trichloroethane ug/L20.1 0.50 20.00 70-130101
1,1,2,2-Tetrachloroethane ug/L19.2 0.50 20.00 70-13096
1,1,2-Trichloroethane ug/L20.8 0.50 20.00 70-130104
1,1-Dichloroethane ug/L20.6 0.50 20.00 70-130103
1,1-Dichloroethylene ug/L21.4 0.50 20.00 70-130107
1,1-Dichloropropylene ug/L21.8 0.50 20.00 70-130109
1,2,3-Trichlorobenzene ug/L18.0 0.50 20.00 70-13090
1,2,3-Trichloropropane ug/L20.6 0.50 20.00 70-130103
1,2,4-Trichlorobenzene ug/L17.8 0.50 20.00 70-13089
1,2,4-Trimethylbenzene ug/L18.4 0.50 20.00 70-13092
1,2-Dibromo-3-chloropropane ug/L17.2 2.0 20.00 70-13086
1,2-Dibromoethane ug/L20.6 0.50 20.00 70-130103
1,2-Dichlorobenzene ug/L19.4 0.50 20.00 70-13097
1,2-Dichloroethane ug/L19.9 0.50 20.00 70-130100
1,2-Dichloropropane ug/L20.8 0.50 20.00 70-130104
1,3,5-Trimethylbenzene ug/L19.0 0.50 20.00 70-13095
1,3-Dichlorobenzene ug/L19.6 0.50 20.00 70-13098
1,3-Dichloropropane ug/L21.0 0.50 20.00 70-130105
1,4-Dichlorobenzene ug/L19.6 0.50 20.00 70-13098
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/24/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.48
Project: Glenn Parker PropertyWithers & Ravenel
Cary, NC 27511
Attn: Matt James
Work Order: 0010187
Time Submitted: 1/14/2020 2:25:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0278 - SM6200 B
LCS (P0A0278-BS1)Prepared & Analyzed: 01/17/20
2,2-Dichloropropane ug/L20.5 2.0 20.00 70-130103
2-Chlorotoluene ug/L18.5 0.50 20.00 70-13093
4-Chlorotoluene ug/L18.8 0.50 20.00 70-13094
4-Isopropyltoluene ug/L19.3 0.50 20.00 70-13097
Acetone ug/L34.3 10 40.00 40-16086
Benzene ug/L21.1 0.50 20.00 70-130105
Bromobenzene ug/L18.8 0.50 20.00 70-13094
Bromochloromethane ug/L21.9 0.50 20.00 70-130110
Bromodichloromethane ug/L19.1 0.50 20.00 70-13095
Bromoform ug/L14.2 0.50 20.00 70-13071
Bromomethane ug/L16.2 1.0 20.00 60-14081
Carbon Tetrachloride ug/L16.5 0.50 20.00 70-13083
Chlorobenzene ug/L20.8 0.50 20.00 70-130104
Chloroethane ug/L14.7 0.50 20.00 60-14073
Chloroform ug/L20.7 0.50 20.00 70-130103
Chloromethane ug/L18.7 0.50 20.00 60-14093
cis-1,2-Dichloroethylene ug/L20.6 0.50 20.00 70-130103
cis-1,3-Dichloropropylene ug/L21.2 0.50 20.00 70-130106
Dibromochloromethane ug/L16.5 0.50 20.00 70-13083
Dibromomethane ug/L21.0 0.50 20.00 70-130105
Dichlorodifluoromethane ug/L17.7 1.0 20.00 60-14088
Ethanol ug/L510 200 500.0 60-140102
Ethylbenzene ug/L19.7 0.50 20.00 70-13099
Hexachlorobutadiene ug/L21.0 2.0 20.00 70-130105
Isopropyl Ether ug/L20.7 0.50 20.00 70-130103
Isopropylbenzene (Cumene)ug/L19.6 0.50 20.00 70-13098
m,p-Xylenes ug/L40.8 1.0 40.00 70-130102
Methyl Butyl Ketone (2-Hexanone)ug/L18.9 1.0 20.00 60-14094
Methyl Ethyl Ketone (2-Butanone)ug/L20.4 5.0 20.00 60-140102
Methyl Isobutyl Ketone ug/L20.4 1.0 20.00 60-140102
Methylene Chloride ug/L20.6 2.0 20.00 70-130103
Methyl-tert-Butyl Ether ug/L21.0 1.0 20.00 70-130105
Naphthalene ug/L15.3 1.0 20.00 70-13076
n-Butylbenzene ug/L18.0 0.50 20.00 70-13090
n-Propylbenzene ug/L19.2 0.50 20.00 70-13096
o-Xylene ug/L20.2 0.50 20.00 70-130101
sec-Butylbenzene ug/L19.8 0.50 20.00 70-13099
Styrene ug/L20.6 0.50 20.00 70-130103
tert-Butylbenzene ug/L19.9 0.50 20.00 70-130100
Tetrachloroethylene ug/L21.7 0.50 20.00 70-130108
Toluene ug/L20.3 0.50 20.00 70-130101
trans-1,2-Dichloroethylene ug/L21.3 0.50 20.00 70-130107
trans-1,3-Dichloropropylene ug/L20.1 0.50 20.00 70-130100
Trichloroethylene ug/L21.9 0.50 20.00 70-130110
Trichlorofluoromethane ug/L21.4 0.50 20.00 60-140107
Vinyl acetate ug/L18.2 5.0 20.00 60-14091
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/24/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.48
Project: Glenn Parker PropertyWithers & Ravenel
Cary, NC 27511
Attn: Matt James
Work Order: 0010187
Time Submitted: 1/14/2020 2:25:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0278 - SM6200 B
LCS (P0A0278-BS1)Prepared & Analyzed: 01/17/20
Vinyl chloride ug/L18.9 0.50 20.00 60-14094
Xylenes, total ug/L61.0 1.5 60.00 70-130102
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9447.0
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9246.2
ug/L 50.00 70-130Surrogate: Toluene-d8 9748.6
Matrix Spike (P0A0278-MS1)Prepared & Analyzed: 01/17/20 Source: 0010187-01
1,1,1,2-Tetrachloroethane ug/L18.2 0.50 20.00 BRL 70-13091
1,1,1-Trichloroethane ug/L18.9 0.50 20.00 BRL 70-13094
1,1,2,2-Tetrachloroethane ug/L17.9 0.50 20.00 BRL 70-13090
1,1,2-Trichloroethane ug/L19.8 0.50 20.00 BRL 70-13099
1,1-Dichloroethane ug/L19.8 0.50 20.00 BRL 70-13099
1,1-Dichloroethylene ug/L18.3 0.50 20.00 BRL 70-13091
1,1-Dichloropropylene ug/L19.5 0.50 20.00 BRL 70-13097
1,2,3-Trichlorobenzene ug/L15.8 0.50 20.00 BRL 70-13079
1,2,3-Trichloropropane ug/L18.7 0.50 20.00 BRL 70-13094
1,2,4-Trichlorobenzene ug/L16.5 0.50 20.00 BRL 70-13082
1,2,4-Trimethylbenzene ug/L17.4 0.50 20.00 BRL 70-13087
1,2-Dibromo-3-chloropropane ug/L16.1 2.0 20.00 BRL 70-13081
1,2-Dibromoethane ug/L19.6 0.50 20.00 BRL 70-13098
1,2-Dichlorobenzene ug/L18.7 0.50 20.00 BRL 70-13093
1,2-Dichloroethane ug/L18.6 0.50 20.00 BRL 70-13093
1,2-Dichloropropane ug/L19.9 0.50 20.00 BRL 70-130100
1,3,5-Trimethylbenzene ug/L17.8 0.50 20.00 BRL 70-13089
1,3-Dichlorobenzene ug/L18.7 0.50 20.00 BRL 70-13094
1,3-Dichloropropane ug/L20.1 0.50 20.00 BRL 70-130101
1,4-Dichlorobenzene ug/L18.8 0.50 20.00 BRL 70-13094
2,2-Dichloropropane ug/L18.0 2.0 20.00 BRL 70-13090
2-Chlorotoluene ug/L17.6 0.50 20.00 BRL 70-13088
4-Chlorotoluene ug/L18.0 0.50 20.00 BRL 70-13090
4-Isopropyltoluene ug/L17.8 0.50 20.00 BRL 70-13089
Acetone ug/L30.2 10 40.00 1.90 40-16071
Benzene ug/L19.9 0.50 20.00 BRL 70-130100
Bromobenzene ug/L18.5 0.50 20.00 BRL 70-13093
Bromochloromethane ug/L20.8 0.50 20.00 BRL 70-130104
Bromodichloromethane ug/L18.8 0.50 20.00 BRL 70-13094
Bromoform ug/L15.5 0.50 20.00 BRL 70-13077
Bromomethane ug/L14.9 1.0 20.00 BRL 60-14074
Carbon Tetrachloride ug/L16.2 0.50 20.00 BRL 70-13081
Chlorobenzene ug/L20.0 0.50 20.00 BRL 70-130100
Chloroethane ug/L14.9 0.50 20.00 BRL 60-14075
Chloroform ug/L20.1 0.50 20.00 BRL 70-130101
Chloromethane ug/L17.1 0.50 20.00 BRL 60-14086
cis-1,2-Dichloroethylene ug/L19.2 0.50 20.00 BRL 70-13096
cis-1,3-Dichloropropylene ug/L19.9 0.50 20.00 BRL 70-13099
Dibromochloromethane ug/L17.2 0.50 20.00 BRL 70-13086
Dibromomethane ug/L19.7 0.50 20.00 BRL 70-13099
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/24/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.48
Project: Glenn Parker PropertyWithers & Ravenel
Cary, NC 27511
Attn: Matt James
Work Order: 0010187
Time Submitted: 1/14/2020 2:25:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0278 - SM6200 B
Matrix Spike (P0A0278-MS1)Prepared & Analyzed: 01/17/20 Source: 0010187-01
Dichlorodifluoromethane ug/L16.3 1.0 20.00 BRL 60-14082
Ethanol ug/L461 200 500.0 BRL 60-14092
Ethylbenzene ug/L19.1 0.50 20.00 BRL 70-13095
Hexachlorobutadiene ug/L17.8 2.0 20.00 BRL 70-13089
Isopropyl Ether ug/L19.1 0.50 20.00 BRL 70-13095
Isopropylbenzene (Cumene)ug/L18.5 0.50 20.00 BRL 70-13093
m,p-Xylenes ug/L39.1 1.0 40.00 BRL 70-13098
Methyl Butyl Ketone (2-Hexanone)ug/L16.9 1.0 20.00 BRL 60-14085
Methyl Ethyl Ketone (2-Butanone)ug/L17.9 5.0 20.00 BRL 60-14090
Methyl Isobutyl Ketone ug/L17.9 1.0 20.00 BRL 60-14089
Methylene Chloride ug/L19.5 2.0 20.00 BRL 70-13097
Methyl-tert-Butyl Ether ug/L20.4 1.0 20.00 BRL 70-130102
Naphthalene ug/L12.9 1.0 20.00 BRL M70-13064
n-Butylbenzene ug/L16.0 0.50 20.00 BRL 70-13080
n-Propylbenzene ug/L17.7 0.50 20.00 BRL 70-13088
o-Xylene ug/L19.3 0.50 20.00 BRL 70-13097
sec-Butylbenzene ug/L17.7 0.50 20.00 BRL 70-13089
Styrene ug/L19.9 0.50 20.00 BRL 70-13099
tert-Butylbenzene ug/L18.4 0.50 20.00 BRL 70-13092
Tetrachloroethylene ug/L19.8 0.50 20.00 BRL 70-13099
Toluene ug/L19.5 0.50 20.00 BRL 70-13097
trans-1,2-Dichloroethylene ug/L19.2 0.50 20.00 BRL 70-13096
trans-1,3-Dichloropropylene ug/L19.4 0.50 20.00 BRL 70-13097
Trichloroethylene ug/L19.8 0.50 20.00 BRL 70-13099
Trichlorofluoromethane ug/L20.6 0.50 20.00 BRL 60-140103
Vinyl acetate ug/L18.8 5.0 20.00 BRL 60-14094
Vinyl chloride ug/L19.5 0.50 20.00 BRL 60-14098
Xylenes, total ug/L58.4 1.5 60.00 BRL 70-13097
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9447.0
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9246.2
ug/L 50.00 70-130Surrogate: Toluene-d8 9848.9
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/24/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.48
Project: Glenn Parker PropertyWithers & Ravenel
Cary, NC 27511
Attn: Matt James
Work Order: 0010187
Time Submitted: 1/14/2020 2:25:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0278 - SM6200 B
Matrix Spike Dup (P0A0278-MSD1)Prepared & Analyzed: 01/17/20 Source: 0010187-01
1,1,1,2-Tetrachloroethane ug/L17.5 0.50 20.00 BRL 2070-13088 4
1,1,1-Trichloroethane ug/L18.0 0.50 20.00 BRL 2070-13090 5
1,1,2,2-Tetrachloroethane ug/L18.1 0.50 20.00 BRL 2070-13090 1
1,1,2-Trichloroethane ug/L19.6 0.50 20.00 BRL 2070-13098 0.8
1,1-Dichloroethane ug/L19.0 0.50 20.00 BRL 2070-13095 4
1,1-Dichloroethylene ug/L17.4 0.50 20.00 BRL 2070-13087 5
1,1-Dichloropropylene ug/L18.7 0.50 20.00 BRL 2070-13094 4
1,2,3-Trichlorobenzene ug/L16.8 0.50 20.00 BRL 2070-13084 6
1,2,3-Trichloropropane ug/L19.2 0.50 20.00 BRL 2070-13096 2
1,2,4-Trichlorobenzene ug/L16.7 0.50 20.00 BRL 2070-13083 1
1,2,4-Trimethylbenzene ug/L16.8 0.50 20.00 BRL 2070-13084 4
1,2-Dibromo-3-chloropropane ug/L17.4 2.0 20.00 BRL 2070-13087 8
1,2-Dibromoethane ug/L19.3 0.50 20.00 BRL 2070-13097 1
1,2-Dichlorobenzene ug/L18.2 0.50 20.00 BRL 2070-13091 3
1,2-Dichloroethane ug/L18.2 0.50 20.00 BRL 2070-13091 2
1,2-Dichloropropane ug/L19.2 0.50 20.00 BRL 2070-13096 4
1,3,5-Trimethylbenzene ug/L17.2 0.50 20.00 BRL 2070-13086 4
1,3-Dichlorobenzene ug/L18.0 0.50 20.00 BRL 2070-13090 4
1,3-Dichloropropane ug/L19.8 0.50 20.00 BRL 2070-13099 2
1,4-Dichlorobenzene ug/L18.2 0.50 20.00 BRL 2070-13091 3
2,2-Dichloropropane ug/L17.2 2.0 20.00 BRL 2070-13086 4
2-Chlorotoluene ug/L17.0 0.50 20.00 BRL 2070-13085 4
4-Chlorotoluene ug/L17.2 0.50 20.00 BRL 2070-13086 5
4-Isopropyltoluene ug/L17.1 0.50 20.00 BRL 2070-13085 4
Acetone ug/L31.3 10 40.00 1.90 2040-16073 4
Benzene ug/L19.0 0.50 20.00 BRL 2070-13095 4
Bromobenzene ug/L17.8 0.50 20.00 BRL 2070-13089 4
Bromochloromethane ug/L20.1 0.50 20.00 BRL 2070-130100 4
Bromodichloromethane ug/L18.1 0.50 20.00 BRL 2070-13090 4
Bromoform ug/L15.9 0.50 20.00 BRL 2070-13080 3
Bromomethane ug/L14.7 1.0 20.00 BRL 2060-14074 1
Carbon Tetrachloride ug/L16.1 0.50 20.00 BRL 2070-13080 1
Chlorobenzene ug/L19.2 0.50 20.00 BRL 2070-13096 4
Chloroethane ug/L13.9 0.50 20.00 BRL 2060-14070 7
Chloroform ug/L19.3 0.50 20.00 BRL 2070-13097 4
Chloromethane ug/L16.3 0.50 20.00 BRL 2060-14081 5
cis-1,2-Dichloroethylene ug/L18.4 0.50 20.00 BRL 2070-13092 4
cis-1,3-Dichloropropylene ug/L19.5 0.50 20.00 BRL 2070-13097 2
Dibromochloromethane ug/L17.0 0.50 20.00 BRL 2070-13085 0.9
Dibromomethane ug/L19.6 0.50 20.00 BRL 2070-13098 0.9
Dichlorodifluoromethane ug/L15.5 1.0 20.00 BRL 2060-14077 5
Ethanol ug/L488 200 500.0 BRL 2060-14098 6
Ethylbenzene ug/L18.2 0.50 20.00 BRL 2070-13091 5
Hexachlorobutadiene ug/L17.8 2.0 20.00 BRL 2070-13089 0.1
Isopropyl Ether ug/L18.5 0.50 20.00 BRL 2070-13093 3
Isopropylbenzene (Cumene)ug/L17.8 0.50 20.00 BRL 2070-13089 4
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
1/24/20
Level II QC Report
115 Mackenan Dr. BUILDING 117 Project No: 02170214.48
Project: Glenn Parker PropertyWithers & Ravenel
Cary, NC 27511
Attn: Matt James
Work Order: 0010187
Time Submitted: 1/14/2020 2:25:00PM
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
Batch P0A0278 - SM6200 B
Matrix Spike Dup (P0A0278-MSD1)Prepared & Analyzed: 01/17/20 Source: 0010187-01
m,p-Xylenes ug/L37.5 1.0 40.00 BRL 2070-13094 4
Methyl Butyl Ketone (2-Hexanone)ug/L17.5 1.0 20.00 BRL 2060-14088 3
Methyl Ethyl Ketone (2-Butanone)ug/L18.6 5.0 20.00 BRL 2060-14093 4
Methyl Isobutyl Ketone ug/L18.4 1.0 20.00 BRL 2060-14092 3
Methylene Chloride ug/L18.6 2.0 20.00 BRL 2070-13093 5
Methyl-tert-Butyl Ether ug/L20.1 1.0 20.00 BRL 2070-130100 1
Naphthalene ug/L13.9 1.0 20.00 BRL 2070-13070 8
n-Butylbenzene ug/L15.6 0.50 20.00 BRL 2170-13078 2
n-Propylbenzene ug/L17.0 0.50 20.00 BRL 1870-13085 4
o-Xylene ug/L18.4 0.50 20.00 BRL 2070-13092 5
sec-Butylbenzene ug/L17.2 0.50 20.00 BRL 2070-13086 3
Styrene ug/L19.0 0.50 20.00 BRL 2070-13095 5
tert-Butylbenzene ug/L17.6 0.50 20.00 BRL 2070-13088 4
Tetrachloroethylene ug/L19.0 0.50 20.00 BRL 2070-13095 4
Toluene ug/L18.6 0.50 20.00 BRL 2070-13093 5
trans-1,2-Dichloroethylene ug/L18.3 0.50 20.00 BRL 2070-13091 5
trans-1,3-Dichloropropylene ug/L19.0 0.50 20.00 BRL 2070-13095 2
Trichloroethylene ug/L19.0 0.50 20.00 BRL 2070-13095 4
Trichlorofluoromethane ug/L19.8 0.50 20.00 BRL 2060-14099 4
Vinyl acetate ug/L18.9 5.0 20.00 BRL 2060-14094 0.6
Vinyl chloride ug/L18.6 0.50 20.00 BRL 2060-14093 5
Xylenes, total ug/L55.8 1.5 60.00 BRL 2070-13093 5
ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 9447.0
ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9446.9
ug/L 50.00 70-130Surrogate: Toluene-d8 9748.7
Sample Extraction Data
Prep Method: SM6200 B
Lab Number Batch Date/TimeInitialFinal
P0A02780010187-01 01/17/20 10:1110 10mL mL
P0A02780010187-02 01/17/20 10:1110 10mL mL
P0A02780010187-03 01/17/20 10:1110 10mL mL
P0A02780010187-03 01/17/20 10:1110 10mL mL
This report should not be reproduced, except in its entirety, without the written consent of Waypoint Analytical.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]