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HomeMy WebLinkAboutWA-1949_22675_CA_MRP_20190603 WithersRavenel Our People. Your Success. 115 MacKenan Drive | Cary, NC 27511 t: 919.469.3340 | f: 919.467.6008 | www.withersravenel.com | License No. C-0832 Cary | Greensboro | Pittsboro | Raleigh | Wilmington June 3, 2019 State of North Carolina Department of Environment and Natural Resources Federal & State Lead Program Division of Waste Management-Underground Storage Tank Section 1637 Mail Service Center Raleigh, North Carolina 27699-1637 Attn: Mr. Scott Ryals RE: SUBSEQUENT MONITORING REPORT Former Moody’s/Handy’s Country Market 1,100-Gallon and 2,000-Gallon Gasoline USTs 2211 Highway 33 West Chocowinity, Beaufort County, North Carolina Groundwater Incident Number 22675 WR Project Number: 02170214.34 Mr. Ryals: WithersRavenel, Inc. (WR) has completed this Subsequent Groundwater Monitoring Report to document the completion of a limited groundwater sampling event, described in our proposal number TA-03, approved by the Federal & State Lead Program on April 16, 2019. The enclosed report summarizes the results of these recently completed monitoring activities. WR appreciates the opportunity to be of service to the Federal & State Lead Program. Should you have any questions regarding the attached, please do not hesitate to contact Matthew James at (919) 469-3340. Cordially, WithersRavenel Kevin B. Buchanan G. Matthew James, PG Staff Environmental Scientist II Project Manager Former Moody’s / Handy’s Country Mart Incident # 22675 WR Project # 02170214.34 Subsequent Monitoring Report i June 2019 TABLE OF CONTENTS Section A. Site Information .................................................................................................. 1 Section B. Executive Summary ............................................................................................ 2 Section C. Site History and Characterization ....................................................................... 5 Section D. Presentation of Current/Comparison to Historical Assessment Information ... 8 Section E. Conclusions and Recommendations ................................................................... 9 FIGURES Figure 1 General Location Map Figure 2 Site Map Figure 3 Groundwater Hydraulic Gradient Map (ft) – April 30, 2019 Figure 4 Groundwater Analytical Results – May 30, 2019 Figure 5 Receptor Map TABLES Table B-1 Site History – UST/AST System and Other Release Information Table B-4 Summary of Groundwater Analytical Results Table B-5 Public & Private Water Supply Well Information Table B-7 Monitoring & Remediation Well Construction Information APPENDICES Appendix A Laboratory Analytical Report and Chain-of-Custody Appendix B Field Notes Appendix C Photographic Documentation WithersRavenel Our People. Your Success. Former Moody’s / Handy’s Country Mart Incident # 22675 WR Project # 02170214.34 Subsequent Monitoring Report 2 June 2019 Section B. Executive Summary 1. Summary of Activities Associated with Current TA WithersRavenel, Inc. (WR) sampled the following groundwater monitoring wells for VOC analysis by EPA Method 6200B: • MW-308R, MW-309R, MW-0312, MW-0314, TAMW-6, TAMW-7 and TAMW-21. 2. Soil, Groundwater and Free Product Assessment Information Soils No soil samples were obtained in association with the monitoring activities conducted by WR during April 2019. Groundwater Analytical results for groundwater samples obtained from site monitoring wells in April 2019 revealed 15A NCAC 2L Standard violations in each of the wells sampled (• MW-308R, MW- 309R, MW-0312, MW-0314, TAMW-6, TAMW-7 and TAMW-21). Benzene (MW-309R and TAMW-7) was reported at a concentration exceeding the NC GCL for the compound. EDB (1,2- dibromoethane) was also reported in TAMW-7 at a level above the GCL. Based on groundwater elevation measurements from April 30, 2019 in which only a portion of the entire monitoring well network was gauged, the direction of groundwater flow is primarily to the north, in general conformance with previous assertions of groundwater flow. Free Product No free product was measured in any of the wells gauged on the site on April 30, 2019. Historical Extents of Free Product • MW-0313: Free phase product thicknesses ranged from a high of 1.82 ft (December 2018) to 0.11 ft (May 2011). • MW-0314: Free phase product was detected in April 2011 at a thickness of 0.04 ft. • TAMW-7: Free phase product was detected in December 2018 at a thickness of 0.01 ft. 3. Receptor Information Current There are no known impacted receptors. Water supply wells WSW-1, WSW-2, WSW-3, and WSW-4 are located on the subject property and are all within 150 feet of the dissolved phase plume. None of these wells were sampled in association with the current TA. WithersRavenel Our People. Your Success. Former Moody’s / Handy’s Country Mart Incident # 22675 WR Project # 02170214.34 Subsequent Monitoring Report 3 June 2019 Historical Receptor Information As part of the CSA activities, seven private water supply wells were also sampled. Analytical results did not identify the presence of petroleum constituents at concentrations above laboratory detection limits in any of the seven samples. In May 2011, two water supply wells (WSW-1 and WSW-6) were sampled. Analytical results for these two samples did not identify the presence of petroleum constituents at concentrations above the laboratory detection limits. Two water supply wells, WSW-1 and WSW-6 were scheduled for sampling during the July 2014 sampling event. WR personnel received permission from the property owner to sample WSW-1. However, Mr. Jasper Paramore who owns property located 2210 Hwy 33 indicated that his well (WSW-6) was abandoned. Therefore, only WSW-1 was sampled. Analytical results for the sample collected from WSW-1 did not identify the presence of VOCs at concentrations that exceed their respective 2L Standards. During the July 2017 groundwater sampling event WR spoke with the owners of WSW-3 (Rennie Whisenant) and WSW-10 (Nancy Paramore) and they informed WR that their respective water supply wells had been abandoned and that the properties are now connected to municipal water. • WSW-3 is reportedly abandoned and the property connected to municipal water; • WSW-6 is reportedly abandoned and the property connected to municipal water; and • WSW-10 is reportedly abandoned and the property connected to municipal water. Mr. Cox, the tenant of the subject property, informed WR that he and the property owner, Mr. Dixon, had discussed improvements to the property such as connecting to municipal water and repaving the parking lot. 4. Remediation Activities WR completed a surfactant enhanced AFVR event in December 2018. Historical AFVR events have been conducted in the past and periodic monitoring is being conducted to establish plume stability. 5. Recommendations Based on the results of assessment and monitoring activities conducted at the site in association with this TA, WR recommends the following: • Complete an updated receptor survey for the site; • Attempt to connect the subject property to the municipal water system and abandon the four onsite water supply wells WSW-1, WSW-2, WSW-4, and WSW-5; and • Complete a Corrective Action Feasibility Study to develop a remediation plan for the site. WithersRavenel Our People. Your Success. Former Moody’s / Handy’s Country Mart Incident # 22675 WR Project # 02170214.34 Subsequent Monitoring Report 4 June 2019 Section C. Site History and Characterization WithersRavenel (WR) has completed a limited groundwater sampling event at the Former Moody’s/Handy’s Country Market. The following information summarizes the site history and characterization. 1. Description of Site Characteristics The property is located in Chocowinity, Beaufort County, North Carolina (Figure 1). According to the Beaufort County GIS website, http://maps.agdmaps.com/nc/beaufort/, the ±1.18-acre property is presently owned by the Ms. Eva E. Dixon Revocable Living Trust, which obtained sole ownership of the property on the passing of Mr. James R. Dixon on February 28, 2018. The site is identified by the Beaufort County GIS system as parcel # 5655-40-3886. The subject property addressed as 2211 Highway 33 contains four structures; two one-story residential homes, a one-story brick commercial building, and a mobile home. According to the 1991 map entitled “Generalized Geology Map of North Carolina”, this site is located within the Yorktown and Duplin Formations of the Coastal Plain Physiographic Province. The Yorktown Formation is typically characterized as fossiliferous sand with clay and the Duplin Formation is typically characterized as shelly sand, sandy marl and limestone. According to the CSA completed by The Clark Group, the shallow subsurface at the site is primarily underlain by unconsolidated sand, silt, and clay. Generally, silty kaolinitic clay was encountered from the ground surface to approximately 12 feet below land surface (BLS). 2. UST Information Current site conditions and the locations of the former UST basins are illustrated on Figure 2. The following table summarizes information regarding the USTs that were formerly utilized on the property. UST ID NO PRODUCT CAPACITY (GALLONS) DATE INSTALLED DATE REMOVED RELEASE DISCOVERED 1 Gasoline 1,100 Unknown October 2000 Yes 2 Gasoline 2,000 Unknown October 2000 Yes 3 Kerosene 450 Unknown October 2000 No 4 Kerosene 450 Unknown October 2000 No According to historical reports, UST-1 and UST-2 were located adjacent to the southeast facing wall of the brick building while UST-3 and UST-4 were located about 100 feet to the northwest. WithersRavenel Our People. Your Success. Former Moody’s / Handy’s Country Mart Incident # 22675 WR Project # 02170214.34 Subsequent Monitoring Report 5 June 2019 3. Description of Release /General Assessment History The following summary of the assessment history of the subject property is based on WR’s review of historical files for the site: • The closure of four USTs by removal took place in October 2000. In addition to the removal of the USTs, 5 cubic yards of contaminated soil and 47 total cubic yards were disposed of offsite at a permitted facility. • During closure of the gasoline USTs (UST-1 and UST-2), 10 soil samples were collected from the tank pit’s walls and floor. Analytical results for six of the soil samples indicated the presence of petroleum constituents. • During closure of the kerosene USTs (UST-3 and UST-4), two soil samples were collected from the tank pit’s floor. Analytical results for the two soil samples did not identify the presence of petroleum constituents above NCDENR (currently identified as NCDEQ) reportable limits. • In July 2001, one shallow groundwater monitoring well (TA-10) was installed in close proximity to the former gasoline UST pit and sampled. Analytical results for the sample indicated the presence of benzene at a concentration above its 2L Standard. • During early to mid-2002, Hood Richardson, PA conducted a Comprehensive Site Assessment (CSA) on the subject property, during which 12 soil samples were collected and analyzed for VOCs, SVOCs, and EPH and VPH. All 12 samples contained one or more petroleum constituents at concentrations above their respective soil-to- groundwater MSCCs. In addition, three soil samples contained one or more petroleum constituents at concentrations above their respective Residential MSCCs. • During the CSA, 18 groundwater monitoring wells were installed; eight permanent shallow (Type II) wells (TAMW-1 through TAMW-7 and TAMW-21) one deep (Type III) well (TAMW-8), and nine temporary wells (TAMW-17 through TAMW-20 and TAMW-22 through TAMW-26). Analytical results for the samples from wells TAMW-3, TAMW-5 through TAMW-7, TAMW-17, TAMW-18, TAMW-21, and TAMW-22 indicated the presence of one or more petroleum constituents at concentrations above their respective 2L Standards. • As part of the CSA activities, seven private water supply wells were also sampled. Analytical results did not identify the presence of petroleum constituents at concentrations above laboratory detection limits in any of the seven samples. In December 2003 and January 2004, sixteen additional monitoring wells (MW-0301 through MW-0316) were installed at the site. • In January and June 2004, free product was measured in groundwater monitoring well MW-0313. • Three MMPE events were conducted at the site in 2008, 2009, and 2011. WithersRavenel Our People. Your Success. Former Moody’s / Handy’s Country Mart Incident # 22675 WR Project # 02170214.34 Subsequent Monitoring Report 6 June 2019 • In May 2011, Geological Resources, Inc. supervised the installation of four additional groundwater monitoring wells (MW-0319 through MW-0322) and completed a groundwater sampling event. Analytical results from that sampling event indicated 10 out of the 14 wells sampled (MW-0308R, MW-0309R, MW-312, MW-0314, MW-0318, MW-0319, MW-0321, TAMW-6, TAMW-7, and TAMW-21) contained one or more petroleum constituents at concentrations above their respective 2L Standard. In addition, as part of the May 2011 sampling event, two water supply wells (WSW-1 and WSW-6) were sampled. Analytical results for these two samples did not identify the presence of petroleum constituents at concentrations above the laboratory detection limits. • In July 2014, WR personnel mobilized to the former Moody’s Country Market to sample 15 groundwater monitoring wells and two water supply wells. Measurable free phase product (FPP) was observed in MW-0313 at a thickness of 0.67 feet and was therefore not sampled. The analytical results for the groundwater samples from MW-0312, MW- 0314, MW-0320, MW-0321, MW-308R, MW-309R, TAMW-7, TAMW-1, TAMW-21, and TAMW-6 identified concentrations of one or more petroleum constituents that are above their 2L Standard. Additionally, the samples from MW-0309R and TAMW-7 contained EDB and benzene at concentrations that exceed their respective GCLs for groundwater. WR personnel received permission from the property owner to sample WSW-1. However, Mr. Jasper Paramore who owns property located 2210 Hwy 33 indicated that his well (WSW-6) was abandoned. Analytical results for the sample from WSW-1 did not identify the presence of VOCs at concentrations above the laboratory detection limits. o WR personnel interviewed Mr. Erick Jennings, the Water Systems Manager for Beaufort County Water Department, regarding access to municipal water to the area. He stated that a water line runs adjacent to Highway 33 and Bear Creek Road. • In December 2018, WR personnel performed a surfactant enhanced AFVR event including the injection and recovery of Enviroclean® surfactant. Prior to the injection and recovery of the surfactant, WR obtained Notice of Intent permit number WI0700479 from the Water Quality Regional Operations Section of NCDEQ. Free product was measured in wells MW-0313 and TAMW-7. Ultimately, the Enviroclean® surfactant was injected into each of these wells. At the completion of the injection event, monitoring well MW-313 had received approximately 325 gallons of 2% surfactant and TAMW-7 had received approximately 175 gallons of 2% surfactant. Ten days following the injection, an AFVR event was completed in which 2,275 gallons of petroleum contact water were recovered from MW-313 and TAMW-7. Gauging of these wells following the completion of the AFVR event did not reveal the presence of measurable free product. WithersRavenel Our People. Your Success. Former Moody’s / Handy’s Country Mart Incident # 22675 WR Project # 02170214.34 Subsequent Monitoring Report 7 June 2019 4. Information on Receptors/Potential Receptors A receptor survey was conducted as part of the CSA activities. According to the report, the subject property and surrounding properties on NC Highway 33 West are supplied water by domestic water supply wells. The survey identified the presence of 34 supply wells within 1,500 feet of the release area. According to The Clark Group CSA, the closest surface water to the site was a man-made pond approximately 75 feet from the source area. Information obtained from property occupants / owners by WR during the July 2014 and July 2017 sampling events indicate that WSW-3, WSW-6, and WSW-10 have been abandoned and the properties have been connected to municipal water. WithersRavenel Our People. Your Success. Former Moody’s / Handy’s Country Mart Incident # 22675 WR Project # 02170214.34 Subsequent Monitoring Report 8 June 2019 Section D. Presentation of Current/Comparison to Historical Assessment Information On April 30, 2019, WR personnel mobilized to the subject to perform sampling activities in accordance with task authorization TA-03. The current monitoring well layout is illustrated in Figure 2 and well construction information is provided in Table B-7. 1. Groundwater Elevations/Free Product Level Measurements Prior to purging the monitoring wells targeted for sampling in April 2019, WR personnel obtained depth to groundwater measurements. The depth-to-water measurements ranged from 2.92 feet below the top of casing (ft-BTOC) in monitoring well MW-0309R to 6.38 ft-BTOC in monitoring well MW-0314. No measurable free product was noted in any of the wells gauged on April 30, 2019. Based on groundwater elevation measurements from April 30, 2019 in which only a portion of the entire monitoring well network was gauged, the direction of groundwater flow is primarily to the north, in general conformance with previous assertions of groundwater flow. Gradient as modeled based on April 2019 data is depicted on Figure 3. 2. Groundwater Sampling and Analytical Results Monitoring Well Sampling WR personnel obtained groundwater samples from the following monitoring wells: • MW-308R, MW-309R, MW-0312, MW-0314, TAMW-6, TAMW-7 and TAMW-21. After measuring depth-to-water, each sampled well was purged with a virgin polyethylene bailer. Following purging and adequate recharge of groundwater within each well, samples were decanted directly from the bailer(s) into laboratory prepared sample containers holding appropriate preservative as required. Groundwater samples were submitted to Prism Laboratories, Inc. (Prism) for analysis of VOCs by SM6200B. The laboratory analytical report and chain-of-custody record associated with these samples are included in Appendix A. Copies of field notes are included in Appendix B. Photographs of wells sampled in April 2019 are included in Appendix C. Laboratory Results Analytical results for groundwater samples obtained from site monitoring wells in April 2019 revealed 15A NCAC 2L Standard violations in the following wells: • MW-308R, MW-309R, MW-0312, MW-0314, TAMW-6, TAMW-7 and TAMW-21. Analytical results for groundwater samples obtained from site monitoring wells in April 2019 revealed GCL Standard violations in the following wells: • MW-309R (benzene) and TAMW-7 (benzene, EDB) The groundwater analytical results are summarized in Table B-4 and shown on Figure 4. WithersRavenel Our People. Your Success. Former Moody’s / Handy’s Country Mart Incident # 22675 WR Project # 02170214.34 Subsequent Monitoring Report 9 June 2019 Section E. Conclusions and Recommendations The following conclusions can be made from the April 30, 2019 limited groundwater sampling event: • No free product was measured in any of the monitoring wells gauged or sampled in association with this limited groundwater monitoring event. • One or more targeted compounds were reported in samples from each of the wells sampled in association with this event (MW-308R, MW-309R, MW-0312, MW-0314, TAMW-6, TAMW-7 and TAMW-21) at concentrations exceeding their respective 2L Standards. • Benzene (MW-0309R and TAMW-7) and EDB (TAMW-7) were reported at levels exceeding their respective GCL concentrations. • According to the property owners, WSW-3, WSW-6 and WSW-10 have been abandoned are connected to municipal water; The closure of these wells means that there are no directly downgradient active water supply wells. Mr. Cox informed WR that he and Mr. Dixon are open to connecting the site to municipal water and abandoning the onsite supply wells. Based on the information gathered during the recent groundwater and water supply well sampling event, WR recommends the following: • Complete an updated receptor survey for the site; • Attempt to connect the subject property to the municipal water system and abandon the four onsite water supply wells WSW-1, WSW-2, WSW-4, and WSW-5; and • Complete a Corrective Action Feasibility Study to develop a remediation plan for the site. FIGURES KBB MJ DRAWN BY: 05/31/19 02170214.34 5 SCALE:FIGURE NO.: PROJECT NO.:DATE:APPROVED BY:RECEPTOR LOCATIONSWithersRavenel Engineers | Planners | Surveyors 115 MacKenan Drive | Cary, NC 27511 | t: 919.469.3340 | license #: C-0832 |www.withersravenel.com 1"=300'GRAPHIC SCALE1 inch = 300 ft.0300150600FORMER MOODY'S / HANDY'S COUNTRY MARKETINCIDENT # 22675 2211 NC HIGHWAY 33 WESTCHOCOWINITY, BEAUFORT COUNTY, NC TABLES UST IDNumberCurrent/LastContents*PreviousContents*Capacity(in gallons)ConstructionDetails**TankDimensions (diameter x length) (ft)Description ofAssociatedPiping & PumpsDate of TankInstallationStatus ofUST***Was release associated with UST System? (Y/N)1 Gasoline N/A 1,100 Unknown 4 x 12.1Unknown Prior to 1985Permanently Closed by Removal (October 11, 2000)Y2 Gasoline N/A 2,000 Unknown 5.3 x 12.1 Unknown Prior to 1985Permanently Closed by Removal (October 11, 2000)Y3 Kerosene N/A 450 Unknown 3.7 x 5.6Unknown Prior to 1985Permanently Closed by Removal (October 11, 2000)N4 Gasoline N\A 450 Unknown 3.7 x 5.6Unknown Prior to 1985Permanently Closed by Removal (October 11, 2000)NAST IDNumberCurrent/LastContents*PreviousContents*Capacity(in gallons)ConstructionDetails**TankDimensions (diameter x length) (ft)Description ofAssociatedPiping & PumpsDate of TankInstallationStatus ofAST***Was release associated with AST System? (Y/N)N/AN/AN/A N/A N/AN/AN/AN/AN/AN/AIncidentNumberMaterialReleasedDateofRelease22675 Gasoline UnknownNotes:1.) W&R is not aware of any ASTs associated with the subject site.*  Gasoline (leaded or unleaded), Diesel, used oil, waste oil, aviation fuel, etc. or pesticides, non‐halogenated or halogenated solvents, etc**  Fiberglass (single‐ or double‐walled), steel (single‐ or double‐walled), steel with FRP (single‐ or double‐walled), steel with liner, other, unknown***  Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removalTable B‐1Site History:  UST/AST System & Other Release InformationFORMER MOODY'S/HANDY'S COUNTRY MARKETUST release was detected when petroleum contaminatoin was identified in soil samples collected during UST closure activities. 2211 Highway 33 WestChocowinity, Beaufort County, North CarolinaDescription of ReleasePage 1 of 1 Calculated 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,2-Dibromoethane (EDB) 1,2-Dichloroethane 1,3,5-Trimethylbenzene Benzene Di-isopropyl ether Ethylbenzene Hexachloro-1,3-butadiene Isopropylbenzene (Cumene)4-Isopropyltoluene(p-Isopropyltoluene) Methyl-tert-butyl ether Naphthalene Styrene Toluene m&p-Xylene n-Butylbenzene n-Propylbenzene o-Xylene sec-ButylbenzeneTotal Xylene96-18-4 95-63-6 106-93-4 107-06-2 108-67-8 71-43-2 108-20-3 100-41-4 87-68-3 98-82-8 99-87-6 1634-04-4 91-20-3 100-42-5 108-88-3 179601-23-1 104-51-8 103-65-1 95-47-6 135-98-8 NA 7/8/2014 3 2560 <1.0 4.2 694 244 <1.0 1440 <2.0 165 NA <1.0 660 4.1 279 1770 <1.0 390 875 19.8 26457/13/2017 ND 2790 <1.0 <1.0 814 183 <1.0 1150 ND 144 NA 13.2 660 <1.0 149 1350 <1.0 ND 499 <1.0 1849 4/30/2019 ND 3400 <0.51 <0.66 910 120 <0.50 1300 ND 160 30 <0.42 620 7.7 19 1200 110 550 200 42 1400 7/8/2014 7/13/2017 7/8/2014 <10.0 2690 <10.0 24 642 1840 <10.0 2820 <20.0 123 NA 272 880 24.9 15600 9730 <10.0 285 5160 <10.0 14890 7/13/2017 ND 3330 <1.0 <1.0 <1.0 1800 <1.0 3000 ND 133 NA 282 1090 ND 11900 9420 <1.0 ND 5010 <1.0 14430 4/30/2019 ND 5100 <0.51 15 1300 1300 <5 3600 ND 180 65 110 1600 22 9200 12000 <0.76 510 6800 33 19000 7/8/2014 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 NA <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 7/13/2017 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 NA <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 7/8/2014 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 NA <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 7/13/2017 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 NA 1.6 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 7/8/2014 <1.0 <1.0 <1.0 <1.0 <1.0 11.8 <1.0 <1.0 <2.0 1.3 NA 13.3 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.6 <1.0 7/13/2017 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <1.0 NA 1.6 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.5 <1.0 7/8/2014 <1.0 19.5 <1.0 <1.0 2.1 99.7 <1.0 17 <2.0 3.2 NA 14.8 9.4 <1.0 2 8.4 <1.0 3.1 1.2 1.8 9.6 7/13/2017 7/8/2014 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 NA <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 7/13/2017 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 NA <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 7/8/2014 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 NA <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 7/13/2017 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 NA <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 7/8/2014 <10.0 1200 <10.0 <10.0 240 830 <10.0 1090 <20.0 78.4 NA 14.9 386 <10.0 1070 1730 <10.0 172 1010 <10.0 2740 7/13/2017 ND 1270 <10.0 <1.0 <1.0 1840 <1.0 1250 ND 90 NA 14.3 365 <1.0 1990 1920 <1.0 ND 762 <1.0 2682 4/30/2019 ND 1400 <0.51 <0.66 300 110 <0.50 850 ND 76 18 <0.42 350 <0.47 380 1700 <0.76 190 400 16 2100 7/8/2014 <10.0 1540 71.1 131 358 8400 35.5 2140 <20.0 85.7 NA 85.2 530 31.8 20600 6980 <10.0 206 3510 <10.0 10490 7/13/2017 ND 1590 <1.0 127 <1.0 7680 <1.0 1840 ND 74.8 NA 70.8 502 <1.0 16600 5880 <1.0 ND 2970 <1.0 8850 4/30/2019 ND 1500 <50 80 380 6500 <5.0 1700 ND 130 <8.9 <4.2 470 79 15000 5500 <7.6 200 2700 <7.6 8200 TAMW-4 7/13/2017 7/8/2014 <5.0 2280 <5.0 6.5 571 516 <5.0 1370 <10.0 99.7 NA 52.9 738 <5.0 1880 2890 <5.0 261 1990 <5.0 4880 7/13/2017 ND 3540 <1.0 15.4 946 1000 <1.0 2270 ND 164 NA 92.1 966 10.1 1830 3950 <1.0 ND 2550 <1.0 6500 4/30/2019 ND 2700 <0.51 <0.66 640 330 <0.50 1400 ND 110 24 24 550 9.5 480 2200 <0.76 360 1300 30 3500 7/8/2014 <1.0 976 116 126 213 7930 <1.0 1430 <2.0 58.8 NA 377 433 31.1 17400 4370 <1.0 149 2350 <1.0 6720 7/13/2017 ND 1270 71.5 120 <1.0 7610 <1.0 1710 ND 62.4 NA 330 481 <1.0 18500 5170 <1.0 ND 2600 NA 7770 4/30/2019 ND 930 100 76 220 7300 <5.0 2500 ND 110 <8.9 190 230 89 24000 6700 <7.6 140 3700 <7.6 10000 7/8/2014 <1.0 59.3 <1.0 1.3 11.2 198 <1.0 107 <2.0 7.7 NA 1.2 32.5 <1.0 35.7 166 <1.0 14 87.8 51.7 253.8 7/13/2017 <1.0 70.7 <1.0 1.3 NA 431 1.6 113 <2.0 7.6 NA <1.0 43 <1.0 44.9 249 1.8 ND 126 <1.0 375 4/30/2019 ND 150 <0.051 0.63 40 640 1.7 190 ND 13 1.8 <1 62 <0.047 87 560 4.6 28 270 2.6 830 WSW-1 7/8/2014 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 NA <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 0.005 400 0.02 0.4 400 1 70 600 0.4 70 25 20 6 70 600 500 70 70 500 70 500 NL 28,500 50 400 25,000 5,000 70,000 84,500 400 25,000 11,700 20,000 6,000 70,000 260,000 85,500 6,900 3,000 85,500 8,500 85,500 Notes NL = Not Listed ND = Compound not identified at level above laboratory method detection limits. NA =Compound Not Analyzed for by Laboratory or not reported by previous consultant. Result =Result Exceeds Laboratory Detection Limits Result =Result Exceeds 2L Standard Result =Result Exceeds GCL Value SM6200B 2.) Compounds analyzed for by laboratory but are not listed were not detected above laboratory detection limits. See the laboratory report inculded in the Appendix for a full list of consitueints. 3.) NC 2L Standard - North Carolina Groundater Quality Standard as per NC Administrative Code 15A NCAC 02L. 4.) GCLs for Groundwater = NCDEQ UST Section Gross Contamination Levels for Groundwater. MW-0313 Free Phase Product Free Phase Product MW-0314 MW-0318 MW-0319 MW-0320 MW-0321 TAMW-7 NC 2L Standard GCLs for Groundwater 1.) All results provided in ug/L (micrograms per liter) or parts per billion unless otherwise noted. NOT SAMPLED MW-0322 MW-307R MW-308R MW-309R TAMW-6 TAMW-21 TABLE B-4 SUMMARY OF GROUNDWATER ANALYTICAL RESULTS FORMER MOODY'S/HANDY'S COUNTRY MARKET 2211 Highway 33 West Chocowinity, Beaufort County, North Carolina NOT ANALYZED BY METHOD SHOWN Sample ID Sample Date Analytical Method MW-0312 Easting NorthingWSW-1 15000942NC Highway 33 West Chocowinity, NCEva E. Dixon40 Carrow Road Chocowinity, NC 27817Unkown Unkown Unkown 119 Cross-gradient 2554404.98 650920.10WSW-2 15000942NC Highway 33 West Chocowinity, NCEva E. Dixon40 Carrow Road Chocowinity, NC 27817Unkown Unkown Unkown 145 Cross-gradient 2554379.37 650926.03WSW-3 120199202230 Highway 33 West Grimesland, NC 27837Rennie Whisenant2230 Highway 33 West Grimesland, NC 27837263 Down-gradient 2554385.51 651105.84WSW-4 15000942NC Highway 33 West Chocowinity, NCEva E. Dixon40 Carrow Road Chocowinity, NC 27817Unkown Unkown Unkown 96 Up-gradient 2554468.12 650794.57WSW-5 15000942NC Highway 33 West Chocowinity, NCEva E. Dixon40 Carrow Road Chocowinity, NC 27817Unkown Unkown Unkown 88Up-gradient 2554521.46 650789.56WSW-6 120063572210 Highway 33 West Grimesland, NC 27837William Jasper Paramore 2210 Highway 33 West Grimesland, NC 27837413 Down-gradient 2554658.54 651222.80WSW-7 1501464730 Bear Creek Road Grimesland, NC 27837Alva & Kristy Crisp30 Bear Creek Road Grimesland, NC 27837Unkown Unkown Unkown 470 Down-gradient 2554936.02 650931.85WSW-10 1200328935 Bear Creek Road Grimesland, NC 27837Nancy Cherry Paramore35 Bear Creek Road Grimesland, NC 27837357Down/Cross-gradient2554739.77 651092.14 2.) Information regarding the water supply well's use and location were obtained from the Groundwater Monitoring Report dated April 18, 2013 and produced by Crawford Environmental Services. 3.) WR has not performed a receptor survey in association with the subject property and thus the information provided above has not been verified. Well Screen Interval(feet)Notes: 1.) Well location addresses and property owner address were obtained from the Beaufort County GIS Department. Property ownership current as of May 27, 2019.Well IDProperty OwnerWell Coordinates(NC State Plane NAD 83 Feet)Property Owner AddressProperty AddressAbandoned (as of July 2017)Abandoned (as of July 2014)Abandoned (as of July 2017)ParcelNumberWell UseWell Depth(feet)TABLE B-5APUBLIC & PRIVATE WATER SUPPLY WELL INFORMATIONFORMER MOODY'S/HANDY'S COUNTRY MARKET2211 Highway 33 WestChocowinity, Beaufort County, North CarolinaWell Distance from Source Area(feet)Location Relative to Groundwater FlowPage 1 of 1 Easting Northing4/30/2019 NM --- ---4/30/2019 NM --- ---4/30/2019 NM --- ---4/30/2019 NM --- ---4/30/2019 NM --- ---4/30/2019 6.33 --- 45.374/30/2019 5.79 --- 44.834/30/2019 NM --- ---4/30/2019 3.01 --- 44.224/30/2019 NM --- ---4/30/2019 NM --- ---4/30/2019 4.19 --- 44.224/30/2019 2.92 --- 44.534/30/2019 NM --- ---4/30/2019 NM --- ---4/30/2019 5.65 --- 44.814/30/2019 NM------4/30/2019 6.38 --- 44.814/30/2019 NM --- ---4/30/2019 NM --- ---4/30/2019 NM --- ---4/30/2019 NM --- ---4/30/2019 NM --- ---4/30/2019 NM --- ---4/30/2019 NM --- ---1)2)47.50651079.072554613.9112/4/2003MW-0319MW-0320MW-03225/19/2011 2 12.0 2.0 2 - 1211.02MW-0310RMW-0311Well construction information from previous consultant's reports.9.02554429.87NM Denotes "Not Measured".2554458.562554610.082554553.112554467.722554408.632554386.54651070.83651100.72651146.01651113.272554480.732554445.832554391.602554482.862650912.15650872.69650883.03650834.14651000.312554632.142554437.062554470.362554537.4351.6747.232554395.965.015.02650912.32650962.632554337.562554637.322554534.732554454.40651012.11650948.94651029.66651004.54650961.525 - 15 51.649 - 92650912.46650807.40650828.08650859.76650900.842554495.412554494.322554519.732554477.99TABLE B-72211 Highway 33 WestMONITORING & REMEDIATION WELL CONSTRUCTION INFORMATIONWell Casing Diameter(inches)Free Product Thickness(feet)650782.44650891.84FORMER MOODY'S/HANDY'S COUNTRY MARKETWell Coordinates(NC State Plane NAD 83 Feet)Date Water Level MeasuredScreened Interval (feet)Chocowinity, Beaufort County, North CarolinaDate InstalledWell IDGroundwaterElevation (feet)Depth-to-Water from Top-of-Casing(feet)Notes: TAMW-7650879.28Top-of-Casing Elevation (feet)Total Depth (feet)Well Casing Depth (feet)13.0 3.0 3 - 13TAMW-1TAMW-2 TAMW-3TAMW-4TAMW-5RTAMW-6TAMW-8TAMW-21MW-0305MW-0307RMW-0308RMW-0309RMW-0312MW-0313MW-0314MW-0316MW-0317MW-0318MW-03214/8/20024/8/20024/8/20024/8/20024/8/20024/8/20024/30/20021/11/20101/11/20102 11.3 9.0 9 - 11.3 50.6251.705 - 155.015.022 15.0 5.0 5 - 15 50.0350.075 - 155.015.0215.0 5.0 5 - 15 49.484/8/2002 2 30.0 25.0 25 - 30 51.459.02Unknown12/3/2003 2 10.0 2.0 2 - 10 47.5848.741 - 111.02 11.0 1.0 1 - 11 48.4147.452 - 102.010.021/11/20101/11/2010 2 12.0 2.0 2 - 12 47.2848.492 - 152.015.0212/3/200212/4/2003 2 15.0 2.0 2 - 15 50.4650.151 - 141.014.0212/4/200312/4/2003 2 15.0 2.0 2 - 15 51.1948.762 - 152.015.021/11/2010 2 10.0 2.0 2 - 10 46.8946.932 - 102.010.021/11/20105/19/2011212.0 2.0 2 - 12 47.2046.312 - 122.012.025/19/20115/19/2011 2 12.0 2.0 2 - 12 46.86Page 1 of 1 APPENDIX A LABORATORY ANALYTICAL REPORT AND CHAIN-OF-CUSTODY This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Case Narrative 5/10/19 14:21 Withers & Ravenel Matt James 115 Mackenan Dr. BUILDING 117 Cary, NC 27511 Project: Former Moodys Handys Country Store Project No.: 02170214.34 Lab Submittal Date: 05/02/2019 Prism Work Order: 9050079 Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. President/Project Manager Reviewed ByRobbi A. Jones Robbi A. Jones President/Project Manager Data Qualifiers Key Reference: L Parameter reported with possible low bias. LCS recovery below the QC limit. Method Detection LimitMDL Below Reporting LimitBRL Relative Percent DifferenceRPD *Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 31 Sample Receipt Summary 05/10/2019 Prism Work Order: 9050079 Client Sample ID MatrixLab Sample ID Date/Time Sampled Date/Time Received 9050079-01 04/30/19 14:50MW-312 05/02/19 12:45Water 9050079-02 04/30/19 15:10MW-314 05/02/19 12:45Water 9050079-03 04/30/19 14:30MW-308R 05/02/19 12:45Water 9050079-04 04/30/19 16:00MW-309R 05/02/19 12:45Water 9050079-05 04/30/19 15:30TAMW-6 05/02/19 12:45Water 9050079-06 04/30/19 15:50TAMW-7 05/02/19 12:45Water 9050079-07 04/30/19 16:15TAMW-21 05/02/19 12:45Water Samples were received in good condition at 2.7 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 31 Client ID ResultParameterMethod UnitsPrism ID Prism Work Order: 9050079 05/10/2019 Summary of Detections 3400 ug/L9050079-01 MW-312 1,2,4-Trimethylbenzene *SM6200 B 910 ug/L9050079-01 MW-312 1,3,5-Trimethylbenzene *SM6200 B 30 ug/L9050079-01 MW-312 4-Isopropyltoluene *SM6200 B 120 ug/L9050079-01 MW-312 Benzene *SM6200 B 1300 ug/L9050079-01 MW-312 Ethylbenzene *SM6200 B 160 ug/L9050079-01 MW-312 Isopropylbenzene (Cumene)*SM6200 B 1200 ug/L9050079-01 MW-312 m,p-Xylenes *SM6200 B 620 ug/L9050079-01 MW-312 Naphthalene *SM6200 B 110 ug/L9050079-01 MW-312 n-Butylbenzene *SM6200 B 550 ug/L9050079-01 MW-312 n-Propylbenzene *SM6200 B 200 ug/L9050079-01 MW-312 o-Xylene *SM6200 B 42 ug/L9050079-01 MW-312 sec-Butylbenzene *SM6200 B 7.7 ug/L9050079-01 MW-312 Styrene *SM6200 B 19 ug/L9050079-01 MW-312 Toluene *SM6200 B 1400 ug/L9050079-01 MW-312 Xylenes, total *SM6200 B 5100 ug/L9050079-02 MW-314 1,2,4-Trimethylbenzene *SM6200 B 15 ug/L9050079-02 MW-314 1,2-Dichloroethane *SM6200 B 1300 ug/L9050079-02 MW-314 1,3,5-Trimethylbenzene *SM6200 B 65 ug/L9050079-02 MW-314 4-Isopropyltoluene *SM6200 B 1300 ug/L9050079-02 MW-314 Benzene *SM6200 B 3600 ug/L9050079-02 MW-314 Ethylbenzene *SM6200 B 180 ug/L9050079-02 MW-314 Isopropylbenzene (Cumene)*SM6200 B 12000 ug/L9050079-02 MW-314 m,p-Xylenes *SM6200 B 110 ug/L9050079-02 MW-314 Methyl-tert-Butyl Ether *SM6200 B 1600 ug/L9050079-02 MW-314 Naphthalene *SM6200 B 510 ug/L9050079-02 MW-314 n-Propylbenzene *SM6200 B 6800 ug/L9050079-02 MW-314 o-Xylene *SM6200 B 33 ug/L9050079-02 MW-314 sec-Butylbenzene *SM6200 B 22 ug/L9050079-02 MW-314 Styrene *SM6200 B 9200 ug/L9050079-02 MW-314 Toluene *SM6200 B 19000 ug/L9050079-02 MW-314 Xylenes, total *SM6200 B 1400 ug/L9050079-03 MW-308R 1,2,4-Trimethylbenzene *SM6200 B 300 ug/L9050079-03 MW-308R 1,3,5-Trimethylbenzene *SM6200 B 18 ug/L9050079-03 MW-308R 4-Isopropyltoluene *SM6200 B 110 ug/L9050079-03 MW-308R Benzene *SM6200 B 850 ug/L9050079-03 MW-308R Ethylbenzene *SM6200 B 76 ug/L9050079-03 MW-308R Isopropylbenzene (Cumene)*SM6200 B 1700 ug/L9050079-03 MW-308R m,p-Xylenes *SM6200 B 350 ug/L9050079-03 MW-308R Naphthalene *SM6200 B 190 ug/L9050079-03 MW-308R n-Propylbenzene *SM6200 B 400 ug/L9050079-03 MW-308R o-Xylene *SM6200 B 16 ug/L9050079-03 MW-308R sec-Butylbenzene *SM6200 B 380 ug/L9050079-03 MW-308R Toluene *SM6200 B 2100 ug/L9050079-03 MW-308R Xylenes, total *SM6200 B This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 31 Client ID ResultParameterMethod UnitsPrism ID Prism Work Order: 9050079 05/10/2019 Summary of Detections 1500 ug/L9050079-04 MW-309R 1,2,4-Trimethylbenzene *SM6200 B 80 ug/L9050079-04 MW-309R 1,2-Dichloroethane *SM6200 B 380 ug/L9050079-04 MW-309R 1,3,5-Trimethylbenzene *SM6200 B 6500 ug/L9050079-04 MW-309R Benzene *SM6200 B 1700 ug/L9050079-04 MW-309R Ethylbenzene *SM6200 B 130 ug/L9050079-04 MW-309R Isopropylbenzene (Cumene)*SM6200 B 5500 ug/L9050079-04 MW-309R m,p-Xylenes *SM6200 B 470 ug/L9050079-04 MW-309R Naphthalene *SM6200 B 200 ug/L9050079-04 MW-309R n-Propylbenzene *SM6200 B 2700 ug/L9050079-04 MW-309R o-Xylene *SM6200 B 79 ug/L9050079-04 MW-309R Styrene *SM6200 B 15000 ug/L9050079-04 MW-309R Toluene *SM6200 B 8200 ug/L9050079-04 MW-309R Xylenes, total *SM6200 B 2700 ug/L9050079-05 TAMW-6 1,2,4-Trimethylbenzene *SM6200 B 640 ug/L9050079-05 TAMW-6 1,3,5-Trimethylbenzene *SM6200 B 24 ug/L9050079-05 TAMW-6 4-Isopropyltoluene *SM6200 B 330 ug/L9050079-05 TAMW-6 Benzene *SM6200 B 1400 ug/L9050079-05 TAMW-6 Ethylbenzene *SM6200 B 110 ug/L9050079-05 TAMW-6 Isopropylbenzene (Cumene)*SM6200 B 2200 ug/L9050079-05 TAMW-6 m,p-Xylenes *SM6200 B 24 ug/L9050079-05 TAMW-6 Methyl-tert-Butyl Ether *SM6200 B 550 ug/L9050079-05 TAMW-6 Naphthalene *SM6200 B 360 ug/L9050079-05 TAMW-6 n-Propylbenzene *SM6200 B 1300 ug/L9050079-05 TAMW-6 o-Xylene *SM6200 B 30 ug/L9050079-05 TAMW-6 sec-Butylbenzene *SM6200 B 9.5 ug/L9050079-05 TAMW-6 Styrene *SM6200 B 480 ug/L9050079-05 TAMW-6 Toluene *SM6200 B 3500 ug/L9050079-05 TAMW-6 Xylenes, total *SM6200 B 930 ug/L9050079-06 TAMW-7 1,2,4-Trimethylbenzene *SM6200 B 100 ug/L9050079-06 TAMW-7 1,2-Dibromoethane *SM6200 B 76 ug/L9050079-06 TAMW-7 1,2-Dichloroethane *SM6200 B 220 ug/L9050079-06 TAMW-7 1,3,5-Trimethylbenzene *SM6200 B 7300 ug/L9050079-06 TAMW-7 Benzene *SM6200 B 2500 ug/L9050079-06 TAMW-7 Ethylbenzene *SM6200 B 110 ug/L9050079-06 TAMW-7 Isopropylbenzene (Cumene)*SM6200 B 6700 ug/L9050079-06 TAMW-7 m,p-Xylenes *SM6200 B 190 ug/L9050079-06 TAMW-7 Methyl-tert-Butyl Ether *SM6200 B 230 ug/L9050079-06 TAMW-7 Naphthalene *SM6200 B 140 ug/L9050079-06 TAMW-7 n-Propylbenzene *SM6200 B 3700 ug/L9050079-06 TAMW-7 o-Xylene *SM6200 B 89 ug/L9050079-06 TAMW-7 Styrene *SM6200 B 24000 ug/L9050079-06 TAMW-7 Toluene *SM6200 B 10000 ug/L9050079-06 TAMW-7 Xylenes, total *SM6200 B 150 ug/L9050079-07 TAMW-21 1,2,4-Trimethylbenzene *SM6200 B 0.63 ug/L9050079-07 TAMW-21 1,2-Dichloroethane *SM6200 B This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 31 Client ID ResultParameterMethod UnitsPrism ID Prism Work Order: 9050079 05/10/2019 Summary of Detections 40 ug/L9050079-07 TAMW-21 1,3,5-Trimethylbenzene *SM6200 B 1.8 ug/L9050079-07 TAMW-21 4-Isopropyltoluene *SM6200 B 640 ug/L9050079-07 TAMW-21 Benzene *SM6200 B 190 ug/L9050079-07 TAMW-21 Ethylbenzene *SM6200 B 1.7 ug/L9050079-07 TAMW-21 Isopropyl Ether *SM6200 B 13 ug/L9050079-07 TAMW-21 Isopropylbenzene (Cumene)*SM6200 B 560 ug/L9050079-07 TAMW-21 m,p-Xylenes *SM6200 B 62 ug/L9050079-07 TAMW-21 Naphthalene *SM6200 B 4.6 ug/L9050079-07 TAMW-21 n-Butylbenzene *SM6200 B 28 ug/L9050079-07 TAMW-21 n-Propylbenzene *SM6200 B 270 ug/L9050079-07 TAMW-21 o-Xylene *SM6200 B 2.6 ug/L9050079-07 TAMW-21 sec-Butylbenzene *SM6200 B 87 ug/L9050079-07 TAMW-21 Toluene *SM6200 B 830 ug/L9050079-07 TAMW-21 Xylenes, total *SM6200 B This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 31 Laboratory Report 05/10/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Sample Matrix: Water Client Sample ID: MW-312 Prism Sample ID: 9050079-01 Prism Work Order: 9050079 Time Collected: 04/30/19 14:50 Time Submitted: 05/02/19 12:45 02170214.34 Volatile Organic Compounds by GC/MS BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 1.11,1,1,2-Tetrachloroethane BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.611,1,1-Trichloroethane BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.361,1,2,2-Tetrachloroethane BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.661,1,2-Trichloroethane BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.831,1-Dichloroethane BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.831,1-Dichloroethylene BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.511,1-Dichloropropylene BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 4.01,2,3-Trichlorobenzene BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 1.41,2,3-Trichloropropane BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 1.31,2,4-Trichlorobenzene 3400 *SM6200 B P9E0125100505/7/19 16:07 KDMug/L 5.41,2,4-Trimethylbenzene BRL *SM6200 B P9E012510205/7/19 15:33 KDMug/L 1.71,2-Dibromo-3-chloropropane BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.511,2-Dibromoethane BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.761,2-Dichlorobenzene BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.661,2-Dichloroethane BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 1.11,2-Dichloropropane 910 *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.761,3,5-Trimethylbenzene BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.541,3-Dichlorobenzene BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.431,3-Dichloropropane BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.501,4-Dichlorobenzene BRL *SM6200 B P9E012510205/7/19 15:33 KDMug/L 1.12,2-Dichloropropane BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.662-Chlorotoluene BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.504-Chlorotoluene 30 *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.894-Isopropyltoluene BRL *SM6200 B P9E0125101005/7/19 15:33 KDMug/L 3.1Acetone 120 *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.48Benzene BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.57Bromobenzene BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 1.4Bromochloromethane BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.62Bromodichloromethane BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.40Bromoform BRL *SM6200 B P9E012510105/7/19 15:33 KDMug/L 1.8Bromomethane BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 1.1Carbon Tetrachloride BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.62Chlorobenzene BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 2.2Chloroethane BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.76Chloroform BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.79Chloromethane BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.56cis-1,2-Dichloroethylene BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.79cis-1,3-Dichloropropylene BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.81Dibromochloromethane BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.65Dibromomethane BRL *SM6200 B P9E012510105/7/19 15:33 KDMug/L 1.1Dichlorodifluoromethane BRL *SM6200 B P9E01251020005/7/19 15:33 KDMug/L 270Ethanol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 31 Laboratory Report 05/10/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Sample Matrix: Water Client Sample ID: MW-312 Prism Sample ID: 9050079-01 Prism Work Order: 9050079 Time Collected: 04/30/19 14:50 Time Submitted: 05/02/19 12:45 02170214.34 1300 *SM6200 B P9E0125100505/7/19 16:07 KDMug/L 6.1Ethylbenzene BRL *SM6200 B P9E012510205/7/19 15:33 KDMug/L 1.6Hexachlorobutadiene BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.50Isopropyl Ether 160 *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.54Isopropylbenzene (Cumene) 1200 *SM6200 B P9E012510105/7/19 15:33 KDMug/L 1.2m,p-Xylenes BRL *SM6200 B P9E012510105/7/19 15:33 KDMug/L 0.65Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P9E012510505/7/19 15:33 KDMug/L 2.4Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P9E012510105/7/19 15:33 KDMug/L 0.78Methyl Isobutyl Ketone BRL *SM6200 B P9E012510205/7/19 15:33 KDMug/L 0.83Methylene Chloride BRL *SM6200 B P9E012510105/7/19 15:33 KDMug/L 0.42Methyl-tert-Butyl Ether 620 *SM6200 B P9E012510105/7/19 15:33 KDMug/L 1.9Naphthalene 110 *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.76n-Butylbenzene 550 *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.87n-Propylbenzene 200 *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.44o-Xylene 42 *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.76sec-Butylbenzene 7.7 *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.47Styrene BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.88tert-Butylbenzene BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.98Tetrachloroethylene 19 *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.44Toluene BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.70trans-1,2-Dichloroethylene BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 1.2trans-1,3-Dichloropropylene BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.78Trichloroethylene BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.62Trichlorofluoromethane BRL *SM6200 B P9E012510505/7/19 15:33 KDMug/L 0.60Vinyl acetate BRL *SM6200 B P9E0125105.0 5/7/19 15:33 KDMug/L 0.97Vinyl chloride 1400 *SM6200 B P9E012510155/7/19 15:33 KDMug/L 1.5Xylenes, total Surrogate Recovery Control Limits 70-130100 %4-Bromofluorobenzene 70-13095 %Dibromofluoromethane 70-130100 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 31 Laboratory Report 05/10/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Sample Matrix: Water Client Sample ID: MW-314 Prism Sample ID: 9050079-02 Prism Work Order: 9050079 Time Collected: 04/30/19 15:10 Time Submitted: 05/02/19 12:45 02170214.34 Volatile Organic Compounds by GC/MS BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 1.11,1,1,2-Tetrachloroethane BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.611,1,1-Trichloroethane BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.361,1,2,2-Tetrachloroethane BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.661,1,2-Trichloroethane BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.831,1-Dichloroethane BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.831,1-Dichloroethylene BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.511,1-Dichloropropylene BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 4.01,2,3-Trichlorobenzene BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 1.41,2,3-Trichloropropane BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 1.31,2,4-Trichlorobenzene 5100 *SM6200 B P9E01432001005/8/19 22:47 KDMug/L 111,2,4-Trimethylbenzene BRL *SM6200 B P9E014310205/8/19 22:13 KDMug/L 1.71,2-Dibromo-3-chloropropane BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.511,2-Dibromoethane BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.761,2-Dichlorobenzene 15 *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.661,2-Dichloroethane BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 1.11,2-Dichloropropane 1300 *SM6200 B P9E01432001005/8/19 22:47 KDMug/L 151,3,5-Trimethylbenzene BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.541,3-Dichlorobenzene BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.431,3-Dichloropropane BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.501,4-Dichlorobenzene BRL *SM6200 B P9E014310205/8/19 22:13 KDMug/L 1.12,2-Dichloropropane BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.662-Chlorotoluene BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.504-Chlorotoluene 65 *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.894-Isopropyltoluene BRL *SM6200 B P9E0143101005/8/19 22:13 KDMug/L 3.1Acetone 1300 *SM6200 B P9E01432001005/8/19 22:47 KDMug/L 9.5Benzene BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.57Bromobenzene BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 1.4Bromochloromethane BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.62Bromodichloromethane BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.40Bromoform BRL *SM6200 B P9E014310105/8/19 22:13 KDMug/L 1.8Bromomethane BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 1.1Carbon Tetrachloride BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.62Chlorobenzene BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 2.2Chloroethane BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.76Chloroform BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.79Chloromethane BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.56cis-1,2-Dichloroethylene BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.79cis-1,3-Dichloropropylene BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.81Dibromochloromethane BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.65Dibromomethane BRL *SM6200 B P9E014310105/8/19 22:13 KDMug/L 1.1Dichlorodifluoromethane BRL *SM6200 B P9E01431020005/8/19 22:13 KDMug/L 270Ethanol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 31 Laboratory Report 05/10/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Sample Matrix: Water Client Sample ID: MW-314 Prism Sample ID: 9050079-02 Prism Work Order: 9050079 Time Collected: 04/30/19 15:10 Time Submitted: 05/02/19 12:45 02170214.34 3600 *SM6200 B P9E01432001005/8/19 22:47 KDMug/L 12Ethylbenzene BRL *SM6200 B P9E014310205/8/19 22:13 KDMug/L 1.6Hexachlorobutadiene BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.50Isopropyl Ether 180 *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.54Isopropylbenzene (Cumene) 12000 *SM6200 B P9E01432002005/8/19 22:47 KDMug/L 23m,p-Xylenes BRL *SM6200 B P9E014310105/8/19 22:13 KDMug/L 0.65Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P9E014310505/8/19 22:13 KDMug/L 2.4Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P9E014310105/8/19 22:13 KDMug/L 0.78Methyl Isobutyl Ketone BRL *SM6200 B P9E014310205/8/19 22:13 KDMug/L 0.83Methylene Chloride 110 *SM6200 B P9E014310105/8/19 22:13 KDMug/L 0.42Methyl-tert-Butyl Ether 1600 *SM6200 B P9E01432002005/8/19 22:47 KDMug/L 38Naphthalene BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.76n-Butylbenzene 510 *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.87n-Propylbenzene 6800 *SM6200 B P9E01432001005/8/19 22:47 KDMug/L 8.9o-Xylene 33 *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.76sec-Butylbenzene 22 *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.47Styrene BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.88tert-Butylbenzene BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.98Tetrachloroethylene 9200 *SM6200 B P9E01432001005/8/19 22:47 KDMug/L 8.8Toluene BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.70trans-1,2-Dichloroethylene BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 1.2trans-1,3-Dichloropropylene BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.78Trichloroethylene BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.62Trichlorofluoromethane BRL *SM6200 B P9E014310505/8/19 22:13 KDMug/L 0.60Vinyl acetate BRL *SM6200 B P9E0143105.0 5/8/19 22:13 KDMug/L 0.97Vinyl chloride 19000 *SM6200 B P9E01432003005/8/19 22:47 KDMug/L 30Xylenes, total Surrogate Recovery Control Limits 70-130102 %4-Bromofluorobenzene 70-13097 %Dibromofluoromethane 70-13098 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 31 Laboratory Report 05/10/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Sample Matrix: Water Client Sample ID: MW-308R Prism Sample ID: 9050079-03 Prism Work Order: 9050079 Time Collected: 04/30/19 14:30 Time Submitted: 05/02/19 12:45 02170214.34 Volatile Organic Compounds by GC/MS BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 1.11,1,1,2-Tetrachloroethane BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.611,1,1-Trichloroethane BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.361,1,2,2-Tetrachloroethane BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.661,1,2-Trichloroethane BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.831,1-Dichloroethane BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.831,1-Dichloroethylene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.511,1-Dichloropropylene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 4.01,2,3-Trichlorobenzene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 1.41,2,3-Trichloropropane BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 1.31,2,4-Trichlorobenzene 1400 *SM6200 B P9E0125100505/7/19 17:14 KDMug/L 5.41,2,4-Trimethylbenzene BRL *SM6200 B P9E012510205/7/19 16:41 KDMug/L 1.71,2-Dibromo-3-chloropropane BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.511,2-Dibromoethane BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.761,2-Dichlorobenzene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.661,2-Dichloroethane BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 1.11,2-Dichloropropane 300 *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.761,3,5-Trimethylbenzene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.541,3-Dichlorobenzene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.431,3-Dichloropropane BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.501,4-Dichlorobenzene BRL *SM6200 B P9E012510205/7/19 16:41 KDMug/L 1.12,2-Dichloropropane BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.662-Chlorotoluene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.504-Chlorotoluene 18 *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.894-Isopropyltoluene BRL *SM6200 B P9E0125101005/7/19 16:41 KDMug/L 3.1Acetone 110 *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.48Benzene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.57Bromobenzene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 1.4Bromochloromethane BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.62Bromodichloromethane BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.40Bromoform BRL *SM6200 B P9E012510105/7/19 16:41 KDMug/L 1.8Bromomethane BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 1.1Carbon Tetrachloride BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.62Chlorobenzene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 2.2Chloroethane BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.76Chloroform BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.79Chloromethane BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.56cis-1,2-Dichloroethylene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.79cis-1,3-Dichloropropylene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.81Dibromochloromethane BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.65Dibromomethane BRL *SM6200 B P9E012510105/7/19 16:41 KDMug/L 1.1Dichlorodifluoromethane BRL *SM6200 B P9E01251020005/7/19 16:41 KDMug/L 270Ethanol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 31 Laboratory Report 05/10/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Sample Matrix: Water Client Sample ID: MW-308R Prism Sample ID: 9050079-03 Prism Work Order: 9050079 Time Collected: 04/30/19 14:30 Time Submitted: 05/02/19 12:45 02170214.34 850 *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.61Ethylbenzene BRL *SM6200 B P9E012510205/7/19 16:41 KDMug/L 1.6Hexachlorobutadiene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.50Isopropyl Ether 76 *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.54Isopropylbenzene (Cumene) 1700 *SM6200 B P9E012510105/7/19 16:41 KDMug/L 1.2m,p-Xylenes BRL *SM6200 B P9E012510105/7/19 16:41 KDMug/L 0.65Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P9E012510505/7/19 16:41 KDMug/L 2.4Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P9E012510105/7/19 16:41 KDMug/L 0.78Methyl Isobutyl Ketone BRL *SM6200 B P9E012510205/7/19 16:41 KDMug/L 0.83Methylene Chloride BRL *SM6200 B P9E012510105/7/19 16:41 KDMug/L 0.42Methyl-tert-Butyl Ether 350 *SM6200 B P9E012510105/7/19 16:41 KDMug/L 1.9Naphthalene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.76n-Butylbenzene 190 *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.87n-Propylbenzene 400 *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.44o-Xylene 16 *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.76sec-Butylbenzene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.47Styrene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.88tert-Butylbenzene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.98Tetrachloroethylene 380 *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.44Toluene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.70trans-1,2-Dichloroethylene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 1.2trans-1,3-Dichloropropylene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.78Trichloroethylene BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.62Trichlorofluoromethane BRL *SM6200 B P9E012510505/7/19 16:41 KDMug/L 0.60Vinyl acetate BRL *SM6200 B P9E0125105.0 5/7/19 16:41 KDMug/L 0.97Vinyl chloride 2100 *SM6200 B P9E012510155/7/19 16:41 KDMug/L 1.5Xylenes, total Surrogate Recovery Control Limits 70-130100 %4-Bromofluorobenzene 70-13099 %Dibromofluoromethane 70-130103 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 31 Laboratory Report 05/10/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Sample Matrix: Water Client Sample ID: MW-309R Prism Sample ID: 9050079-04 Prism Work Order: 9050079 Time Collected: 04/30/19 16:00 Time Submitted: 05/02/19 12:45 02170214.34 Volatile Organic Compounds by GC/MS BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 111,1,1,2-Tetrachloroethane BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 6.11,1,1-Trichloroethane BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 3.61,1,2,2-Tetrachloroethane BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 6.61,1,2-Trichloroethane BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 8.31,1-Dichloroethane BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 8.31,1-Dichloroethylene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 5.11,1-Dichloropropylene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 401,2,3-Trichlorobenzene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 141,2,3-Trichloropropane BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 131,2,4-Trichlorobenzene 1500 *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 5.41,2,4-Trimethylbenzene BRL *SM6200 B P9E01431002005/8/19 23:21 KDMug/L 171,2-Dibromo-3-chloropropane BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 5.11,2-Dibromoethane BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 7.61,2-Dichlorobenzene 80 *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 6.61,2-Dichloroethane BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 111,2-Dichloropropane 380 *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 7.61,3,5-Trimethylbenzene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 5.41,3-Dichlorobenzene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 4.31,3-Dichloropropane BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 5.01,4-Dichlorobenzene BRL *SM6200 B P9E01431002005/8/19 23:21 KDMug/L 112,2-Dichloropropane BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 6.62-Chlorotoluene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 5.04-Chlorotoluene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 8.94-Isopropyltoluene BRL *SM6200 B P9E014310010005/8/19 23:21 KDMug/L 31Acetone 6500 *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 4.8Benzene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 5.7Bromobenzene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 14Bromochloromethane BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 6.2Bromodichloromethane BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 4.0Bromoform BRL *SM6200 B P9E01431001005/8/19 23:21 KDMug/L 18Bromomethane BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 11Carbon Tetrachloride BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 6.2Chlorobenzene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 22Chloroethane BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 7.6Chloroform BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 7.9Chloromethane BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 5.6cis-1,2-Dichloroethylene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 7.9cis-1,3-Dichloropropylene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 8.1Dibromochloromethane BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 6.5Dibromomethane BRL *SM6200 B P9E01431001005/8/19 23:21 KDMug/L 11Dichlorodifluoromethane BRL *SM6200 B P9E0143100200005/8/19 23:21 KDMug/L 2700Ethanol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 12 of 31 Laboratory Report 05/10/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Sample Matrix: Water Client Sample ID: MW-309R Prism Sample ID: 9050079-04 Prism Work Order: 9050079 Time Collected: 04/30/19 16:00 Time Submitted: 05/02/19 12:45 02170214.34 1700 *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 6.1Ethylbenzene BRL *SM6200 B P9E01431002005/8/19 23:21 KDMug/L 16Hexachlorobutadiene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 5.0Isopropyl Ether 130 *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 5.4Isopropylbenzene (Cumene) 5500 *SM6200 B P9E01431001005/8/19 23:21 KDMug/L 12m,p-Xylenes BRL *SM6200 B P9E01431001005/8/19 23:21 KDMug/L 6.5Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P9E01431005005/8/19 23:21 KDMug/L 24Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P9E01431001005/8/19 23:21 KDMug/L 7.8Methyl Isobutyl Ketone BRL *SM6200 B P9E01431002005/8/19 23:21 KDMug/L 8.3Methylene Chloride BRL *SM6200 B P9E01431001005/8/19 23:21 KDMug/L 4.2Methyl-tert-Butyl Ether 470 *SM6200 B P9E01431001005/8/19 23:21 KDMug/L 19Naphthalene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 7.6n-Butylbenzene 200 *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 8.7n-Propylbenzene 2700 *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 4.4o-Xylene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 7.6sec-Butylbenzene 79 *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 4.7Styrene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 8.8tert-Butylbenzene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 9.8Tetrachloroethylene 15000 *SM6200 B P9E014310005005/8/19 23:55 KDMug/L 44Toluene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 7.0trans-1,2-Dichloroethylene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 12trans-1,3-Dichloropropylene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 7.8Trichloroethylene BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 6.2Trichlorofluoromethane BRL *SM6200 B P9E01431005005/8/19 23:21 KDMug/L 6.0Vinyl acetate BRL *SM6200 B P9E0143100505/8/19 23:21 KDMug/L 9.7Vinyl chloride 8200 *SM6200 B P9E01431001505/8/19 23:21 KDMug/L 15Xylenes, total Surrogate Recovery Control Limits 70-130104 %4-Bromofluorobenzene 70-130100 %Dibromofluoromethane 70-13099 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 13 of 31 Laboratory Report 05/10/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Sample Matrix: Water Client Sample ID: TAMW-6 Prism Sample ID: 9050079-05 Prism Work Order: 9050079 Time Collected: 04/30/19 15:30 Time Submitted: 05/02/19 12:45 02170214.34 Volatile Organic Compounds by GC/MS BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 1.11,1,1,2-Tetrachloroethane BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.611,1,1-Trichloroethane BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.361,1,2,2-Tetrachloroethane BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.661,1,2-Trichloroethane BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.831,1-Dichloroethane BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.831,1-Dichloroethylene BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.511,1-Dichloropropylene BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 4.01,2,3-Trichlorobenzene BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 1.41,2,3-Trichloropropane BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 1.31,2,4-Trichlorobenzene 2700 *SM6200 B P9E0125100505/7/19 18:22 KDMug/L 5.41,2,4-Trimethylbenzene BRL *SM6200 B P9E012510205/7/19 17:48 KDMug/L 1.71,2-Dibromo-3-chloropropane BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.511,2-Dibromoethane BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.761,2-Dichlorobenzene BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.661,2-Dichloroethane BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 1.11,2-Dichloropropane 640 *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.761,3,5-Trimethylbenzene BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.541,3-Dichlorobenzene BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.431,3-Dichloropropane BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.501,4-Dichlorobenzene BRL *SM6200 B P9E012510205/7/19 17:48 KDMug/L 1.12,2-Dichloropropane BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.662-Chlorotoluene BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.504-Chlorotoluene 24 *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.894-Isopropyltoluene BRL *SM6200 B P9E0125101005/7/19 17:48 KDMug/L 3.1Acetone 330 *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.48Benzene BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.57Bromobenzene BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 1.4Bromochloromethane BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.62Bromodichloromethane BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.40Bromoform BRL *SM6200 B P9E012510105/7/19 17:48 KDMug/L 1.8Bromomethane BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 1.1Carbon Tetrachloride BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.62Chlorobenzene BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 2.2Chloroethane BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.76Chloroform BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.79Chloromethane BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.56cis-1,2-Dichloroethylene BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.79cis-1,3-Dichloropropylene BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.81Dibromochloromethane BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.65Dibromomethane BRL *SM6200 B P9E012510105/7/19 17:48 KDMug/L 1.1Dichlorodifluoromethane BRL *SM6200 B P9E01251020005/7/19 17:48 KDMug/L 270Ethanol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 14 of 31 Laboratory Report 05/10/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Sample Matrix: Water Client Sample ID: TAMW-6 Prism Sample ID: 9050079-05 Prism Work Order: 9050079 Time Collected: 04/30/19 15:30 Time Submitted: 05/02/19 12:45 02170214.34 1400 *SM6200 B P9E0125100505/7/19 18:22 KDMug/L 6.1Ethylbenzene BRL *SM6200 B P9E012510205/7/19 17:48 KDMug/L 1.6Hexachlorobutadiene BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.50Isopropyl Ether 110 *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.54Isopropylbenzene (Cumene) 2200 *SM6200 B P9E01251001005/7/19 18:22 KDMug/L 12m,p-Xylenes BRL *SM6200 B P9E012510105/7/19 17:48 KDMug/L 0.65Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P9E012510505/7/19 17:48 KDMug/L 2.4Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P9E012510105/7/19 17:48 KDMug/L 0.78Methyl Isobutyl Ketone BRL *SM6200 B P9E012510205/7/19 17:48 KDMug/L 0.83Methylene Chloride 24 *SM6200 B P9E012510105/7/19 17:48 KDMug/L 0.42Methyl-tert-Butyl Ether 550 *SM6200 B P9E012510105/7/19 17:48 KDMug/L 1.9Naphthalene BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.76n-Butylbenzene 360 *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.87n-Propylbenzene 1300 *SM6200 B P9E0125100505/7/19 18:22 KDMug/L 4.4o-Xylene 30 *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.76sec-Butylbenzene 9.5 *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.47Styrene BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.88tert-Butylbenzene BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.98Tetrachloroethylene 480 *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.44Toluene BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.70trans-1,2-Dichloroethylene BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 1.2trans-1,3-Dichloropropylene BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.78Trichloroethylene BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.62Trichlorofluoromethane BRL *SM6200 B P9E012510505/7/19 17:48 KDMug/L 0.60Vinyl acetate BRL *SM6200 B P9E0125105.0 5/7/19 17:48 KDMug/L 0.97Vinyl chloride 3500 *SM6200 B P9E01251001505/7/19 18:22 KDMug/L 15Xylenes, total Surrogate Recovery Control Limits 70-130100 %4-Bromofluorobenzene 70-13098 %Dibromofluoromethane 70-130102 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 15 of 31 Laboratory Report 05/10/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Sample Matrix: Water Client Sample ID: TAMW-7 Prism Sample ID: 9050079-06 Prism Work Order: 9050079 Time Collected: 04/30/19 15:50 Time Submitted: 05/02/19 12:45 02170214.34 Volatile Organic Compounds by GC/MS BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 111,1,1,2-Tetrachloroethane BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 6.11,1,1-Trichloroethane BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 3.61,1,2,2-Tetrachloroethane BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 6.61,1,2-Trichloroethane BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 8.31,1-Dichloroethane BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 8.31,1-Dichloroethylene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 5.11,1-Dichloropropylene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 401,2,3-Trichlorobenzene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 141,2,3-Trichloropropane BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 131,2,4-Trichlorobenzene 930 *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 5.41,2,4-Trimethylbenzene BRL *SM6200 B P9E01431002005/9/19 0:29 KDMug/L 171,2-Dibromo-3-chloropropane 100 *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 5.11,2-Dibromoethane BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 7.61,2-Dichlorobenzene 76 *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 6.61,2-Dichloroethane BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 111,2-Dichloropropane 220 *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 7.61,3,5-Trimethylbenzene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 5.41,3-Dichlorobenzene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 4.31,3-Dichloropropane BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 5.01,4-Dichlorobenzene BRL *SM6200 B P9E01431002005/9/19 0:29 KDMug/L 112,2-Dichloropropane BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 6.62-Chlorotoluene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 5.04-Chlorotoluene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 8.94-Isopropyltoluene BRL *SM6200 B P9E014310010005/9/19 0:29 KDMug/L 31Acetone 7300 *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 4.8Benzene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 5.7Bromobenzene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 14Bromochloromethane BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 6.2Bromodichloromethane BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 4.0Bromoform BRL *SM6200 B P9E01431001005/9/19 0:29 KDMug/L 18Bromomethane BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 11Carbon Tetrachloride BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 6.2Chlorobenzene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 22Chloroethane BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 7.6Chloroform BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 7.9Chloromethane BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 5.6cis-1,2-Dichloroethylene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 7.9cis-1,3-Dichloropropylene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 8.1Dibromochloromethane BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 6.5Dibromomethane BRL *SM6200 B P9E01431001005/9/19 0:29 KDMug/L 11Dichlorodifluoromethane BRL *SM6200 B P9E0143100200005/9/19 0:29 KDMug/L 2700Ethanol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 16 of 31 Laboratory Report 05/10/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Sample Matrix: Water Client Sample ID: TAMW-7 Prism Sample ID: 9050079-06 Prism Work Order: 9050079 Time Collected: 04/30/19 15:50 Time Submitted: 05/02/19 12:45 02170214.34 2500 *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 6.1Ethylbenzene BRL *SM6200 B P9E01431002005/9/19 0:29 KDMug/L 16Hexachlorobutadiene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 5.0Isopropyl Ether 110 *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 5.4Isopropylbenzene (Cumene) 6700 *SM6200 B P9E01431001005/9/19 0:29 KDMug/L 12m,p-Xylenes BRL *SM6200 B P9E01431001005/9/19 0:29 KDMug/L 6.5Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P9E01431005005/9/19 0:29 KDMug/L 24Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P9E01431001005/9/19 0:29 KDMug/L 7.8Methyl Isobutyl Ketone BRL *SM6200 B P9E01431002005/9/19 0:29 KDMug/L 8.3Methylene Chloride 190 *SM6200 B P9E01431001005/9/19 0:29 KDMug/L 4.2Methyl-tert-Butyl Ether 230 *SM6200 B P9E01431001005/9/19 0:29 KDMug/L 19Naphthalene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 7.6n-Butylbenzene 140 *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 8.7n-Propylbenzene 3700 *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 4.4o-Xylene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 7.6sec-Butylbenzene 89 *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 4.7Styrene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 8.8tert-Butylbenzene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 9.8Tetrachloroethylene 24000 *SM6200 B P9E014310005005/9/19 1:02 KDMug/L 44Toluene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 7.0trans-1,2-Dichloroethylene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 12trans-1,3-Dichloropropylene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 7.8Trichloroethylene BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 6.2Trichlorofluoromethane BRL *SM6200 B P9E01431005005/9/19 0:29 KDMug/L 6.0Vinyl acetate BRL *SM6200 B P9E0143100505/9/19 0:29 KDMug/L 9.7Vinyl chloride 10000 *SM6200 B P9E01431001505/9/19 0:29 KDMug/L 15Xylenes, total Surrogate Recovery Control Limits 70-130105 %4-Bromofluorobenzene 70-13099 %Dibromofluoromethane 70-130101 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 17 of 31 Laboratory Report 05/10/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Sample Matrix: Water Client Sample ID: TAMW-21 Prism Sample ID: 9050079-07 Prism Work Order: 9050079 Time Collected: 04/30/19 16:15 Time Submitted: 05/02/19 12:45 02170214.34 Volatile Organic Compounds by GC/MS BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.111,1,1,2-Tetrachloroethane BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.0611,1,1-Trichloroethane BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.0361,1,2,2-Tetrachloroethane BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.0661,1,2-Trichloroethane BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.0831,1-Dichloroethane BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.0831,1-Dichloroethylene BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.0511,1-Dichloropropylene BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.401,2,3-Trichlorobenzene BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.141,2,3-Trichloropropane BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.131,2,4-Trichlorobenzene 150 *SM6200 B P9E0125105.0 5/7/19 14:59 KDMug/L 0.541,2,4-Trimethylbenzene BRL *SM6200 B P9E012512.0 5/7/19 14:25 KDMug/L 0.171,2-Dibromo-3-chloropropane BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.0511,2-Dibromoethane BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.0761,2-Dichlorobenzene 0.63 *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.0661,2-Dichloroethane BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.111,2-Dichloropropane 40 *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.0761,3,5-Trimethylbenzene BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.0541,3-Dichlorobenzene BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.0431,3-Dichloropropane BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.0501,4-Dichlorobenzene BRL *SM6200 B P9E012512.0 5/7/19 14:25 KDMug/L 0.112,2-Dichloropropane BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.0662-Chlorotoluene BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.0504-Chlorotoluene 1.8 *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.0894-Isopropyltoluene BRL *SM6200 B P9E01251105/7/19 14:25 KDMug/L 0.31Acetone 640 *SM6200 B P9E0125105.0 5/7/19 14:59 KDMug/L 0.48Benzene BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.057Bromobenzene BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.14Bromochloromethane BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.062Bromodichloromethane BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.040Bromoform BRL *SM6200 B P9E012511.0 5/7/19 14:25 KDMug/L 0.18Bromomethane BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.11Carbon Tetrachloride BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.062Chlorobenzene BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.22Chloroethane BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.076Chloroform BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.079Chloromethane BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.056cis-1,2-Dichloroethylene BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.079cis-1,3-Dichloropropylene BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.081Dibromochloromethane BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.065Dibromomethane BRL *SM6200 B P9E012511.0 5/7/19 14:25 KDMug/L 0.11Dichlorodifluoromethane BRL *SM6200 B P9E012512005/7/19 14:25 KDMug/L 27Ethanol This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 18 of 31 Laboratory Report 05/10/2019 ResultParameter Batch ID Report Limit Analysis Date/Time MethodDilution Factor Units MDL Analyst 115 Mackenan Dr. BUILDING 117 Project No.: Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Sample Matrix: Water Client Sample ID: TAMW-21 Prism Sample ID: 9050079-07 Prism Work Order: 9050079 Time Collected: 04/30/19 16:15 Time Submitted: 05/02/19 12:45 02170214.34 190 *SM6200 B P9E0125105.0 5/7/19 14:59 KDMug/L 0.61Ethylbenzene BRL *SM6200 B P9E012512.0 5/7/19 14:25 KDMug/L 0.16Hexachlorobutadiene 1.7 *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.050Isopropyl Ether 13 *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.054Isopropylbenzene (Cumene) 560 *SM6200 B P9E012510105/7/19 14:59 KDMug/L 1.2m,p-Xylenes BRL *SM6200 B P9E012511.0 5/7/19 14:25 KDMug/L 0.065Methyl Butyl Ketone (2-Hexanone) BRL *SM6200 B P9E012515.0 5/7/19 14:25 KDMug/L 0.24Methyl Ethyl Ketone (2-Butanone) BRL *SM6200 B P9E012511.0 5/7/19 14:25 KDMug/L 0.078Methyl Isobutyl Ketone BRL *SM6200 B P9E012512.0 5/7/19 14:25 KDMug/L 0.083Methylene Chloride BRL *SM6200 B P9E012511.0 5/7/19 14:25 KDMug/L 0.042Methyl-tert-Butyl Ether 62 *SM6200 B P9E012511.0 5/7/19 14:25 KDMug/L 0.19Naphthalene 4.6 *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.076n-Butylbenzene 28 *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.087n-Propylbenzene 270 *SM6200 B P9E0125105.0 5/7/19 14:59 KDMug/L 0.44o-Xylene 2.6 *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.076sec-Butylbenzene BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.047Styrene BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.088tert-Butylbenzene BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.098Tetrachloroethylene 87 *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.044Toluene BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.070trans-1,2-Dichloroethylene BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.12trans-1,3-Dichloropropylene BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.078Trichloroethylene BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.062Trichlorofluoromethane BRL *SM6200 B P9E012515.0 5/7/19 14:25 KDMug/L 0.060Vinyl acetate BRL *SM6200 B P9E012510.50 5/7/19 14:25 KDMug/L 0.097Vinyl chloride 830 *SM6200 B P9E012510155/7/19 14:59 KDMug/L 1.5Xylenes, total Surrogate Recovery Control Limits 70-130101 %4-Bromofluorobenzene 70-13095 %Dibromofluoromethane 70-130100 %Toluene-d8 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 19 of 31 5/10/19 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.34 Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Prism Work Order: 9050079 Time Submitted: 5/2/2019 12:45:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9E0125 - SM6200 B Blank (P9E0125-BLK1)Prepared & Analyzed: 05/07/19 1,1,1,2-Tetrachloroethane ug/LBRL0.50 1,1,1-Trichloroethane ug/LBRL0.50 1,1,2,2-Tetrachloroethane ug/LBRL0.50 1,1,2-Trichloroethane ug/LBRL0.50 1,1-Dichloroethane ug/LBRL0.50 1,1-Dichloroethylene ug/LBRL0.50 1,1-Dichloropropylene ug/LBRL0.50 1,2,3-Trichlorobenzene ug/LBRL0.50 1,2,3-Trichloropropane ug/LBRL0.50 1,2,4-Trichlorobenzene ug/LBRL0.50 1,2,4-Trimethylbenzene ug/LBRL0.50 1,2-Dibromo-3-chloropropane ug/LBRL2.0 1,2-Dibromoethane ug/LBRL0.50 1,2-Dichlorobenzene ug/LBRL0.50 1,2-Dichloroethane ug/LBRL0.50 1,2-Dichloropropane ug/LBRL0.50 1,3,5-Trimethylbenzene ug/LBRL0.50 1,3-Dichlorobenzene ug/LBRL0.50 1,3-Dichloropropane ug/LBRL0.50 1,4-Dichlorobenzene ug/LBRL0.50 2,2-Dichloropropane ug/LBRL2.0 2-Chlorotoluene ug/LBRL0.50 4-Chlorotoluene ug/LBRL0.50 4-Isopropyltoluene ug/LBRL0.50 Acetone ug/LBRL10 Benzene ug/LBRL0.50 Bromobenzene ug/LBRL0.50 Bromochloromethane ug/LBRL0.50 Bromodichloromethane ug/LBRL0.50 Bromoform ug/LBRL0.50 Bromomethane ug/LBRL1.0 Carbon Tetrachloride ug/LBRL0.50 Chlorobenzene ug/LBRL0.50 Chloroethane ug/LBRL0.50 Chloroform ug/LBRL0.50 Chloromethane ug/LBRL0.50 cis-1,2-Dichloroethylene ug/LBRL0.50 cis-1,3-Dichloropropylene ug/LBRL0.50 Dibromochloromethane ug/LBRL0.50 Dibromomethane ug/LBRL0.50 Dichlorodifluoromethane ug/LBRL1.0 Ethanol ug/LBRL200 Ethylbenzene ug/LBRL0.50 Hexachlorobutadiene ug/LBRL2.0 Isopropyl Ether ug/LBRL0.50 Isopropylbenzene (Cumene)ug/LBRL0.50 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 20 of 31 5/10/19 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.34 Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Prism Work Order: 9050079 Time Submitted: 5/2/2019 12:45:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9E0125 - SM6200 B Blank (P9E0125-BLK1)Prepared & Analyzed: 05/07/19 m,p-Xylenes ug/LBRL1.0 Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0 Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0 Methyl Isobutyl Ketone ug/LBRL1.0 Methylene Chloride ug/LBRL2.0 Methyl-tert-Butyl Ether ug/LBRL1.0 Naphthalene ug/LBRL1.0 n-Butylbenzene ug/LBRL0.50 n-Propylbenzene ug/LBRL0.50 o-Xylene ug/LBRL0.50 sec-Butylbenzene ug/LBRL0.50 Styrene ug/LBRL0.50 tert-Butylbenzene ug/LBRL0.50 Tetrachloroethylene ug/LBRL0.50 Toluene ug/LBRL0.50 trans-1,2-Dichloroethylene ug/LBRL0.50 trans-1,3-Dichloropropylene ug/LBRL0.50 Trichloroethylene ug/LBRL0.50 Trichlorofluoromethane ug/LBRL0.50 Vinyl acetate ug/LBRL5.0 Vinyl chloride ug/LBRL0.50 Xylenes, total ug/LBRL1.5 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10049.8 ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10150.5 ug/L 50.00 70-130Surrogate: Toluene-d8 9849.2 LCS (P9E0125-BS1)Prepared & Analyzed: 05/07/19 1,1,1,2-Tetrachloroethane ug/L22.5 0.50 20.00 70-130112 1,1,1-Trichloroethane ug/L20.8 0.50 20.00 70-130104 1,1,2,2-Tetrachloroethane ug/L20.8 0.50 20.00 70-130104 1,1,2-Trichloroethane ug/L20.2 0.50 20.00 70-130101 1,1-Dichloroethane ug/L20.0 0.50 20.00 70-130100 1,1-Dichloroethylene ug/L17.8 0.50 20.00 70-13089 1,1-Dichloropropylene ug/L19.3 0.50 20.00 70-13096 1,2,3-Trichlorobenzene ug/L18.9 0.50 20.00 70-13094 1,2,3-Trichloropropane ug/L18.8 0.50 20.00 70-13094 1,2,4-Trichlorobenzene ug/L19.2 0.50 20.00 70-13096 1,2,4-Trimethylbenzene ug/L21.5 0.50 20.00 70-130108 1,2-Dibromo-3-chloropropane ug/L17.8 2.0 20.00 70-13089 1,2-Dibromoethane ug/L20.7 0.50 20.00 70-130103 1,2-Dichlorobenzene ug/L20.9 0.50 20.00 70-130104 1,2-Dichloroethane ug/L20.4 0.50 20.00 70-130102 1,2-Dichloropropane ug/L20.1 0.50 20.00 70-130100 1,3,5-Trimethylbenzene ug/L21.1 0.50 20.00 70-130106 1,3-Dichlorobenzene ug/L20.1 0.50 20.00 70-130101 1,3-Dichloropropane ug/L20.9 0.50 20.00 70-130104 1,4-Dichlorobenzene ug/L20.1 0.50 20.00 70-130100 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 21 of 31 5/10/19 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.34 Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Prism Work Order: 9050079 Time Submitted: 5/2/2019 12:45:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9E0125 - SM6200 B LCS (P9E0125-BS1)Prepared & Analyzed: 05/07/19 2,2-Dichloropropane ug/L20.4 2.0 20.00 70-130102 2-Chlorotoluene ug/L20.5 0.50 20.00 70-130103 4-Chlorotoluene ug/L20.6 0.50 20.00 70-130103 4-Isopropyltoluene ug/L18.6 0.50 20.00 70-13093 Acetone ug/L37.6 10 40.00 40-16094 Benzene ug/L21.4 0.50 20.00 70-130107 Bromobenzene ug/L20.6 0.50 20.00 70-130103 Bromochloromethane ug/L20.0 0.50 20.00 70-130100 Bromodichloromethane ug/L20.5 0.50 20.00 70-130103 Bromoform ug/L21.8 0.50 20.00 70-130109 Bromomethane ug/L19.5 1.0 20.00 60-14098 Carbon Tetrachloride ug/L20.4 0.50 20.00 70-130102 Chlorobenzene ug/L20.6 0.50 20.00 70-130103 Chloroethane ug/L21.4 0.50 20.00 60-140107 Chloroform ug/L20.3 0.50 20.00 70-130102 Chloromethane ug/L20.9 0.50 20.00 60-140104 cis-1,2-Dichloroethylene ug/L21.1 0.50 20.00 70-130105 cis-1,3-Dichloropropylene ug/L21.3 0.50 20.00 70-130107 Dibromochloromethane ug/L20.5 0.50 20.00 70-130103 Dibromomethane ug/L21.5 0.50 20.00 70-130107 Dichlorodifluoromethane ug/L17.4 1.0 20.00 60-14087 Ethanol ug/L425200 500.0 60-14085 Ethylbenzene ug/L21.6 0.50 20.00 70-130108 Hexachlorobutadiene ug/L19.2 2.0 20.00 70-13096 Isopropyl Ether ug/L18.3 0.50 20.00 70-13092 Isopropylbenzene (Cumene)ug/L19.6 0.50 20.00 70-13098 m,p-Xylenes ug/L44.3 1.0 40.00 70-130111 Methyl Butyl Ketone (2-Hexanone)ug/L19.5 1.0 20.00 60-14098 Methyl Ethyl Ketone (2-Butanone)ug/L22.8 5.0 20.00 60-140114 Methyl Isobutyl Ketone ug/L20.2 1.0 20.00 60-140101 Methylene Chloride ug/L19.2 2.0 20.00 70-13096 Methyl-tert-Butyl Ether ug/L19.3 1.0 20.00 70-13096 Naphthalene ug/L19.6 1.0 20.00 70-13098 n-Butylbenzene ug/L19.0 0.50 20.00 70-13095 n-Propylbenzene ug/L21.5 0.50 20.00 70-130108 o-Xylene ug/L21.5 0.50 20.00 70-130108 sec-Butylbenzene ug/L18.8 0.50 20.00 70-13094 Styrene ug/L18.9 0.50 20.00 70-13095 tert-Butylbenzene ug/L18.8 0.50 20.00 70-13094 Tetrachloroethylene ug/L19.0 0.50 20.00 70-13095 Toluene ug/L21.7 0.50 20.00 70-130108 trans-1,2-Dichloroethylene ug/L19.1 0.50 20.00 70-13095 trans-1,3-Dichloropropylene ug/L22.1 0.50 20.00 70-130110 Trichloroethylene ug/L20.8 0.50 20.00 70-130104 Trichlorofluoromethane ug/L17.6 0.50 20.00 60-14088 Vinyl acetate ug/L19.1 5.0 20.00 60-14096 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 22 of 31 5/10/19 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.34 Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Prism Work Order: 9050079 Time Submitted: 5/2/2019 12:45:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9E0125 - SM6200 B LCS (P9E0125-BS1)Prepared & Analyzed: 05/07/19 Vinyl chloride ug/L17.7 0.50 20.00 60-14089 Xylenes, total ug/L65.8 1.5 60.00 70-130110 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10251.2 ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10049.8 ug/L 50.00 70-130Surrogate: Toluene-d8 10150.3 LCS Dup (P9E0125-BSD1)Prepared & Analyzed: 05/07/19 1,1,1,2-Tetrachloroethane ug/L22.4 0.50 20.00 2070-130112 0.3 1,1,1-Trichloroethane ug/L20.1 0.50 20.00 2070-130101 3 1,1,2,2-Tetrachloroethane ug/L21.3 0.50 20.00 2070-130106 2 1,1,2-Trichloroethane ug/L20.1 0.50 20.00 2070-130101 0.3 1,1-Dichloroethane ug/L19.2 0.50 20.00 2070-13096 4 1,1-Dichloroethylene ug/L17.2 0.50 20.00 2070-13086 3 1,1-Dichloropropylene ug/L18.6 0.50 20.00 2070-13093 3 1,2,3-Trichlorobenzene ug/L20.0 0.50 20.00 2070-130100 6 1,2,3-Trichloropropane ug/L20.2 0.50 20.00 2070-130101 7 1,2,4-Trichlorobenzene ug/L19.1 0.50 20.00 2070-13096 0.2 1,2,4-Trimethylbenzene ug/L20.9 0.50 20.00 2070-130104 3 1,2-Dibromo-3-chloropropane ug/L19.8 2.0 20.00 2070-13099 10 1,2-Dibromoethane ug/L21.1 0.50 20.00 2070-130106 2 1,2-Dichlorobenzene ug/L20.4 0.50 20.00 2070-130102 2 1,2-Dichloroethane ug/L20.9 0.50 20.00 2070-130105 2 1,2-Dichloropropane ug/L19.4 0.50 20.00 2070-13097 3 1,3,5-Trimethylbenzene ug/L21.0 0.50 20.00 2070-130105 0.9 1,3-Dichlorobenzene ug/L19.6 0.50 20.00 2070-13098 3 1,3-Dichloropropane ug/L20.8 0.50 20.00 2070-130104 0.5 1,4-Dichlorobenzene ug/L20.2 0.50 20.00 2070-130101 0.5 2,2-Dichloropropane ug/L20.1 2.0 20.00 2070-130101 2 2-Chlorotoluene ug/L19.9 0.50 20.00 2070-13099 3 4-Chlorotoluene ug/L19.8 0.50 20.00 2070-13099 4 4-Isopropyltoluene ug/L18.0 0.50 20.00 2070-13090 4 Acetone ug/L37.9 10 40.00 2040-16095 0.8 Benzene ug/L20.9 0.50 20.00 2070-130104 3 Bromobenzene ug/L20.6 0.50 20.00 2070-130103 0.2 Bromochloromethane ug/L20.0 0.50 20.00 2070-130100 0.05 Bromodichloromethane ug/L20.2 0.50 20.00 2070-130101 1 Bromoform ug/L20.8 0.50 20.00 2070-130104 5 Bromomethane ug/L20.6 1.0 20.00 2060-140103 6 Carbon Tetrachloride ug/L19.6 0.50 20.00 2070-13098 5 Chlorobenzene ug/L20.2 0.50 20.00 2070-130101 2 Chloroethane ug/L20.9 0.50 20.00 2060-140104 3 Chloroform ug/L20.2 0.50 20.00 2070-130101 0.6 Chloromethane ug/L20.6 0.50 20.00 2060-140103 1 cis-1,2-Dichloroethylene ug/L21.0 0.50 20.00 2070-130105 0.5 cis-1,3-Dichloropropylene ug/L21.0 0.50 20.00 2070-130105 1 Dibromochloromethane ug/L20.9 0.50 20.00 2070-130104 2 Dibromomethane ug/L21.8 0.50 20.00 2070-130109 1 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 23 of 31 5/10/19 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.34 Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Prism Work Order: 9050079 Time Submitted: 5/2/2019 12:45:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9E0125 - SM6200 B LCS Dup (P9E0125-BSD1)Prepared & Analyzed: 05/07/19 Dichlorodifluoromethane ug/L16.4 1.0 20.00 2060-14082 6 Ethanol ug/L463200 500.0 2060-14093 9 Ethylbenzene ug/L20.8 0.50 20.00 2070-130104 4 Hexachlorobutadiene ug/L17.7 2.0 20.00 2070-13088 8 Isopropyl Ether ug/L17.9 0.50 20.00 2070-13090 2 Isopropylbenzene (Cumene)ug/L18.9 0.50 20.00 2070-13095 4 m,p-Xylenes ug/L42.7 1.0 40.00 2070-130107 4 Methyl Butyl Ketone (2-Hexanone)ug/L20.6 1.0 20.00 2060-140103 5 Methyl Ethyl Ketone (2-Butanone)ug/L23.4 5.0 20.00 2060-140117 2 Methyl Isobutyl Ketone ug/L22.4 1.0 20.00 2060-140112 11 Methylene Chloride ug/L19.1 2.0 20.00 2070-13095 0.5 Methyl-tert-Butyl Ether ug/L19.7 1.0 20.00 2070-13098 2 Naphthalene ug/L20.3 1.0 20.00 2070-130101 3 n-Butylbenzene ug/L18.0 0.50 20.00 2070-13090 5 n-Propylbenzene ug/L20.4 0.50 20.00 2070-130102 5 o-Xylene ug/L21.2 0.50 20.00 2070-130106 1 sec-Butylbenzene ug/L18.3 0.50 20.00 2070-13092 2 Styrene ug/L18.5 0.50 20.00 2070-13093 2 tert-Butylbenzene ug/L18.3 0.50 20.00 2070-13092 3 Tetrachloroethylene ug/L18.1 0.50 20.00 2070-13090 5 Toluene ug/L21.3 0.50 20.00 2070-130106 2 trans-1,2-Dichloroethylene ug/L18.7 0.50 20.00 2070-13093 2 trans-1,3-Dichloropropylene ug/L21.6 0.50 20.00 2070-130108 2 Trichloroethylene ug/L19.8 0.50 20.00 2070-13099 5 Trichlorofluoromethane ug/L17.0 0.50 20.00 2060-14085 4 Vinyl acetate ug/L19.7 5.0 20.00 2060-14098 3 Vinyl chloride ug/L17.3 0.50 20.00 2060-14086 3 Xylenes, total ug/L63.9 1.5 60.00 2070-130107 3 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10050.0 ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10150.6 ug/L 50.00 70-130Surrogate: Toluene-d8 9949.6 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 24 of 31 5/10/19 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.34 Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Prism Work Order: 9050079 Time Submitted: 5/2/2019 12:45:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9E0143 - SM6200 B Blank (P9E0143-BLK1)Prepared & Analyzed: 05/08/19 1,1,1,2-Tetrachloroethane ug/LBRL0.50 1,1,1-Trichloroethane ug/LBRL0.50 1,1,2,2-Tetrachloroethane ug/LBRL0.50 1,1,2-Trichloroethane ug/LBRL0.50 1,1-Dichloroethane ug/LBRL0.50 1,1-Dichloroethylene ug/LBRL0.50 1,1-Dichloropropylene ug/LBRL0.50 1,2,3-Trichlorobenzene ug/LBRL0.50 1,2,3-Trichloropropane ug/LBRL0.50 1,2,4-Trichlorobenzene ug/LBRL0.50 1,2,4-Trimethylbenzene ug/LBRL0.50 1,2-Dibromo-3-chloropropane ug/LBRL2.0 1,2-Dibromoethane ug/LBRL0.50 1,2-Dichlorobenzene ug/LBRL0.50 1,2-Dichloroethane ug/LBRL0.50 1,2-Dichloropropane ug/LBRL0.50 1,3,5-Trimethylbenzene ug/LBRL0.50 1,3-Dichlorobenzene ug/LBRL0.50 1,3-Dichloropropane ug/LBRL0.50 1,4-Dichlorobenzene ug/LBRL0.50 2,2-Dichloropropane ug/LBRL2.0 2-Chlorotoluene ug/LBRL0.50 4-Chlorotoluene ug/LBRL0.50 4-Isopropyltoluene ug/LBRL0.50 Acetone ug/LBRL10 Benzene ug/LBRL0.50 Bromobenzene ug/LBRL0.50 Bromochloromethane ug/LBRL0.50 Bromodichloromethane ug/LBRL0.50 Bromoform ug/LBRL0.50 Bromomethane ug/LBRL1.0 Carbon Tetrachloride ug/LBRL0.50 Chlorobenzene ug/LBRL0.50 Chloroethane ug/LBRL0.50 Chloroform ug/LBRL0.50 Chloromethane ug/LBRL0.50 cis-1,2-Dichloroethylene ug/LBRL0.50 cis-1,3-Dichloropropylene ug/LBRL0.50 Dibromochloromethane ug/LBRL0.50 Dibromomethane ug/LBRL0.50 Dichlorodifluoromethane ug/LBRL1.0 Ethanol ug/LBRL200 Ethylbenzene ug/LBRL0.50 Hexachlorobutadiene ug/LBRL2.0 Isopropyl Ether ug/LBRL0.50 Isopropylbenzene (Cumene)ug/LBRL0.50 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 25 of 31 5/10/19 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.34 Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Prism Work Order: 9050079 Time Submitted: 5/2/2019 12:45:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9E0143 - SM6200 B Blank (P9E0143-BLK1)Prepared & Analyzed: 05/08/19 m,p-Xylenes ug/LBRL1.0 Methyl Butyl Ketone (2-Hexanone)ug/LBRL1.0 Methyl Ethyl Ketone (2-Butanone)ug/LBRL5.0 Methyl Isobutyl Ketone ug/LBRL1.0 Methylene Chloride ug/LBRL2.0 Methyl-tert-Butyl Ether ug/LBRL1.0 Naphthalene ug/LBRL1.0 n-Butylbenzene ug/LBRL0.50 n-Propylbenzene ug/LBRL0.50 o-Xylene ug/LBRL0.50 sec-Butylbenzene ug/LBRL0.50 Styrene ug/LBRL0.50 tert-Butylbenzene ug/LBRL0.50 Tetrachloroethylene ug/LBRL0.50 Toluene ug/LBRL0.50 trans-1,2-Dichloroethylene ug/LBRL0.50 trans-1,3-Dichloropropylene ug/LBRL0.50 Trichloroethylene ug/LBRL0.50 Trichlorofluoromethane ug/LBRL0.50 Vinyl acetate ug/LBRL5.0 Vinyl chloride ug/LBRL0.50 Xylenes, total ug/LBRL1.5 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10351.7 ug/L 50.00 70-130Surrogate: Dibromofluoromethane 10150.6 ug/L 50.00 70-130Surrogate: Toluene-d8 10049.8 LCS (P9E0143-BS1)Prepared & Analyzed: 05/08/19 1,1,1,2-Tetrachloroethane ug/L21.7 0.50 20.00 70-130108 1,1,1-Trichloroethane ug/L21.0 0.50 20.00 70-130105 1,1,2,2-Tetrachloroethane ug/L21.5 0.50 20.00 70-130108 1,1,2-Trichloroethane ug/L20.5 0.50 20.00 70-130102 1,1-Dichloroethane ug/L19.4 0.50 20.00 70-13097 1,1-Dichloroethylene ug/L17.8 0.50 20.00 70-13089 1,1-Dichloropropylene ug/L19.8 0.50 20.00 70-13099 1,2,3-Trichlorobenzene ug/L18.7 0.50 20.00 70-13094 1,2,3-Trichloropropane ug/L19.8 0.50 20.00 70-13099 1,2,4-Trichlorobenzene ug/L18.7 0.50 20.00 70-13093 1,2,4-Trimethylbenzene ug/L21.3 0.50 20.00 70-130106 1,2-Dibromo-3-chloropropane ug/L18.4 2.0 20.00 70-13092 1,2-Dibromoethane ug/L21.4 0.50 20.00 70-130107 1,2-Dichlorobenzene ug/L20.4 0.50 20.00 70-130102 1,2-Dichloroethane ug/L20.6 0.50 20.00 70-130103 1,2-Dichloropropane ug/L20.0 0.50 20.00 70-130100 1,3,5-Trimethylbenzene ug/L21.3 0.50 20.00 70-130106 1,3-Dichlorobenzene ug/L20.0 0.50 20.00 70-130100 1,3-Dichloropropane ug/L21.4 0.50 20.00 70-130107 1,4-Dichlorobenzene ug/L20.6 0.50 20.00 70-130103 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 26 of 31 5/10/19 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.34 Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Prism Work Order: 9050079 Time Submitted: 5/2/2019 12:45:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9E0143 - SM6200 B LCS (P9E0143-BS1)Prepared & Analyzed: 05/08/19 2,2-Dichloropropane ug/L21.5 2.0 20.00 70-130107 2-Chlorotoluene ug/L20.3 0.50 20.00 70-130102 4-Chlorotoluene ug/L20.5 0.50 20.00 70-130102 4-Isopropyltoluene ug/L18.9 0.50 20.00 70-13095 Acetone ug/L36.6 10 40.00 40-16092 Benzene ug/L21.4 0.50 20.00 70-130107 Bromobenzene ug/L20.7 0.50 20.00 70-130104 Bromochloromethane ug/L21.5 0.50 20.00 70-130108 Bromodichloromethane ug/L20.6 0.50 20.00 70-130103 Bromoform ug/L20.1 0.50 20.00 70-130101 Bromomethane ug/L16.7 1.0 20.00 60-14084 Carbon Tetrachloride ug/L20.9 0.50 20.00 70-130104 Chlorobenzene ug/L20.9 0.50 20.00 70-130105 Chloroethane ug/L18.9 0.50 20.00 60-14094 Chloroform ug/L20.8 0.50 20.00 70-130104 Chloromethane ug/L16.2 0.50 20.00 60-14081 cis-1,2-Dichloroethylene ug/L21.2 0.50 20.00 70-130106 cis-1,3-Dichloropropylene ug/L21.6 0.50 20.00 70-130108 Dibromochloromethane ug/L21.0 0.50 20.00 70-130105 Dibromomethane ug/L21.8 0.50 20.00 70-130109 Dichlorodifluoromethane ug/L10.6 1.0 20.00 L60-14053 Ethanol ug/L448200 500.0 60-14090 Ethylbenzene ug/L22.1 0.50 20.00 70-130110 Hexachlorobutadiene ug/L19.4 2.0 20.00 70-13097 Isopropyl Ether ug/L17.8 0.50 20.00 70-13089 Isopropylbenzene (Cumene)ug/L19.9 0.50 20.00 70-13099 m,p-Xylenes ug/L45.0 1.0 40.00 70-130113 Methyl Butyl Ketone (2-Hexanone)ug/L19.4 1.0 20.00 60-14097 Methyl Ethyl Ketone (2-Butanone)ug/L21.9 5.0 20.00 60-140110 Methyl Isobutyl Ketone ug/L21.0 1.0 20.00 60-140105 Methylene Chloride ug/L18.5 2.0 20.00 70-13092 Methyl-tert-Butyl Ether ug/L19.2 1.0 20.00 70-13096 Naphthalene ug/L19.0 1.0 20.00 70-13095 n-Butylbenzene ug/L19.1 0.50 20.00 70-13095 n-Propylbenzene ug/L21.4 0.50 20.00 70-130107 o-Xylene ug/L21.6 0.50 20.00 70-130108 sec-Butylbenzene ug/L19.1 0.50 20.00 70-13096 Styrene ug/L19.2 0.50 20.00 70-13096 tert-Butylbenzene ug/L19.1 0.50 20.00 70-13096 Tetrachloroethylene ug/L19.2 0.50 20.00 70-13096 Toluene ug/L21.8 0.50 20.00 70-130109 trans-1,2-Dichloroethylene ug/L19.9 0.50 20.00 70-13099 trans-1,3-Dichloropropylene ug/L22.3 0.50 20.00 70-130112 Trichloroethylene ug/L20.8 0.50 20.00 70-130104 Trichlorofluoromethane ug/L16.1 0.50 20.00 60-14081 Vinyl acetate ug/L18.8 5.0 20.00 60-14094 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 27 of 31 5/10/19 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.34 Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Prism Work Order: 9050079 Time Submitted: 5/2/2019 12:45:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9E0143 - SM6200 B LCS (P9E0143-BS1)Prepared & Analyzed: 05/08/19 Vinyl chloride ug/L14.6 0.50 20.00 60-14073 Xylenes, total ug/L66.6 1.5 60.00 70-130111 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10049.8 ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9748.5 ug/L 50.00 70-130Surrogate: Toluene-d8 10150.7 LCS Dup (P9E0143-BSD1)Prepared & Analyzed: 05/08/19 1,1,1,2-Tetrachloroethane ug/L21.8 0.50 20.00 2070-130109 0.8 1,1,1-Trichloroethane ug/L21.9 0.50 20.00 2070-130109 4 1,1,2,2-Tetrachloroethane ug/L21.3 0.50 20.00 2070-130106 1 1,1,2-Trichloroethane ug/L20.8 0.50 20.00 2070-130104 2 1,1-Dichloroethane ug/L19.9 0.50 20.00 2070-13099 2 1,1-Dichloroethylene ug/L18.7 0.50 20.00 2070-13093 4 1,1-Dichloropropylene ug/L19.5 0.50 20.00 2070-13098 1 1,2,3-Trichlorobenzene ug/L19.7 0.50 20.00 2070-13099 5 1,2,3-Trichloropropane ug/L22.4 0.50 20.00 2070-130112 12 1,2,4-Trichlorobenzene ug/L19.1 0.50 20.00 2070-13095 2 1,2,4-Trimethylbenzene ug/L21.7 0.50 20.00 2070-130108 2 1,2-Dibromo-3-chloropropane ug/L19.5 2.0 20.00 2070-13098 6 1,2-Dibromoethane ug/L21.5 0.50 20.00 2070-130108 0.7 1,2-Dichlorobenzene ug/L20.8 0.50 20.00 2070-130104 2 1,2-Dichloroethane ug/L21.5 0.50 20.00 2070-130107 4 1,2-Dichloropropane ug/L20.9 0.50 20.00 2070-130105 4 1,3,5-Trimethylbenzene ug/L21.5 0.50 20.00 2070-130108 1 1,3-Dichlorobenzene ug/L20.1 0.50 20.00 2070-130101 0.3 1,3-Dichloropropane ug/L21.8 0.50 20.00 2070-130109 2 1,4-Dichlorobenzene ug/L20.6 0.50 20.00 2070-130103 0.2 2,2-Dichloropropane ug/L21.3 2.0 20.00 2070-130106 0.8 2-Chlorotoluene ug/L20.9 0.50 20.00 2070-130105 3 4-Chlorotoluene ug/L20.9 0.50 20.00 2070-130105 2 4-Isopropyltoluene ug/L19.1 0.50 20.00 2070-13096 1 Acetone ug/L35.5 10 40.00 2040-16089 3 Benzene ug/L21.8 0.50 20.00 2070-130109 2 Bromobenzene ug/L20.9 0.50 20.00 2070-130104 0.7 Bromochloromethane ug/L21.3 0.50 20.00 2070-130107 0.9 Bromodichloromethane ug/L21.6 0.50 20.00 2070-130108 5 Bromoform ug/L21.6 0.50 20.00 2070-130108 7 Bromomethane ug/L17.5 1.0 20.00 2060-14087 4 Carbon Tetrachloride ug/L20.9 0.50 20.00 2070-130105 0.1 Chlorobenzene ug/L20.8 0.50 20.00 2070-130104 0.6 Chloroethane ug/L18.9 0.50 20.00 2060-14094 0.2 Chloroform ug/L20.8 0.50 20.00 2070-130104 0.1 Chloromethane ug/L15.8 0.50 20.00 2060-14079 2 cis-1,2-Dichloroethylene ug/L21.4 0.50 20.00 2070-130107 0.9 cis-1,3-Dichloropropylene ug/L22.0 0.50 20.00 2070-130110 2 Dibromochloromethane ug/L21.4 0.50 20.00 2070-130107 1 Dibromomethane ug/L22.1 0.50 20.00 2070-130111 2 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 28 of 31 5/10/19 Level II QC Report 115 Mackenan Dr. BUILDING 117 Project No: 02170214.34 Project: Former Moodys Handys Country Store Withers & Ravenel Cary, NC 27511 Attn: Matt James Prism Work Order: 9050079 Time Submitted: 5/2/2019 12:45:00PM Result Limit Reporting Units Level Spike Result Source %REC %REC Limits RPD RPD Limit Notes Analyte Volatile Organic Compounds by GC/MS - Quality Control Batch P9E0143 - SM6200 B LCS Dup (P9E0143-BSD1)Prepared & Analyzed: 05/08/19 Dichlorodifluoromethane ug/L10.6 1.0 20.00 20 L60-14053 0.5 Ethanol ug/L482200 500.0 2060-14096 7 Ethylbenzene ug/L22.2 0.50 20.00 2070-130111 0.5 Hexachlorobutadiene ug/L19.7 2.0 20.00 2070-13098 1 Isopropyl Ether ug/L18.2 0.50 20.00 2070-13091 2 Isopropylbenzene (Cumene)ug/L20.0 0.50 20.00 2070-130100 0.5 m,p-Xylenes ug/L44.7 1.0 40.00 2070-130112 0.7 Methyl Butyl Ketone (2-Hexanone)ug/L20.0 1.0 20.00 2060-140100 3 Methyl Ethyl Ketone (2-Butanone)ug/L22.2 5.0 20.00 2060-140111 1 Methyl Isobutyl Ketone ug/L21.3 1.0 20.00 2060-140107 2 Methylene Chloride ug/L19.6 2.0 20.00 2070-13098 6 Methyl-tert-Butyl Ether ug/L19.5 1.0 20.00 2070-13097 2 Naphthalene ug/L19.9 1.0 20.00 2070-13099 4 n-Butylbenzene ug/L19.0 0.50 20.00 2070-13095 0.1 n-Propylbenzene ug/L21.6 0.50 20.00 2070-130108 0.6 o-Xylene ug/L21.9 0.50 20.00 2070-130110 2 sec-Butylbenzene ug/L19.3 0.50 20.00 2070-13097 1 Styrene ug/L19.6 0.50 20.00 2070-13098 2 tert-Butylbenzene ug/L19.2 0.50 20.00 2070-13096 0.3 Tetrachloroethylene ug/L19.4 0.50 20.00 2070-13097 0.5 Toluene ug/L22.1 0.50 20.00 2070-130110 1 trans-1,2-Dichloroethylene ug/L19.6 0.50 20.00 2070-13098 1 trans-1,3-Dichloropropylene ug/L22.7 0.50 20.00 2070-130114 2 Trichloroethylene ug/L21.0 0.50 20.00 2070-130105 1 Trichlorofluoromethane ug/L15.9 0.50 20.00 2060-14079 1 Vinyl acetate ug/L20.3 5.0 20.00 2060-140101 8 Vinyl chloride ug/L14.5 0.50 20.00 2060-14072 1 Xylenes, total ug/L66.6 1.5 60.00 2070-130111 0.05 ug/L 50.00 70-130Surrogate: 4-Bromofluorobenzene 10150.3 ug/L 50.00 70-130Surrogate: Dibromofluoromethane 9949.6 ug/L 50.00 70-130Surrogate: Toluene-d8 10150.5 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 29 of 31 Sample Extraction Data Prep Method: SM6200 B Lab Number Batch Date/TimeInitialFinal P9E01259050079-01 05/07/19 10:311010mLmL P9E01259050079-01 05/07/19 10:311010mLmL P9E01439050079-02 05/08/19 11:121010mLmL P9E01439050079-02 05/08/19 11:121010mLmL P9E01259050079-03 05/07/19 10:311010mLmL P9E01259050079-03 05/07/19 10:311010mLmL P9E01439050079-04 05/08/19 11:121010mLmL P9E01439050079-04 05/08/19 11:121010mLmL P9E01259050079-05 05/07/19 10:311010mLmL P9E01259050079-05 05/07/19 10:311010mLmL P9E01439050079-06 05/08/19 11:121010mLmL P9E01439050079-06 05/08/19 11:121010mLmL P9E01259050079-07 05/07/19 10:311010mLmL P9E01259050079-07 05/07/19 10:311010mLmL This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 30 of 31 APPENDIX B FIELD NOTES APPENDIX C PHOTOGRAPHS PHOTO # MW-0308R PHOTO # MW-0309R PHOTO # MW-0312 PHOTO # MW-0314 PHOTO # TAMW-6 PHOTO # TAMW-7 PHOTO # TAMW-21