MO-9330_40791_CA_UST61_20180129

UST-61
24-Hour Release and UST Leak Reporting Form.
For Releases This form should be completed and submitted to the UST Section's regional office following a known or suspected release from
an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or
in NC suspected release
(DWM USE ONLY)
Suspected Contamination? (Y/N)
Facility ID Number
Incident # Risk (H,I,L,U)
Confirmed GW Contamination? (Y/N)
Date Leak Discovered
Received On Received By
Confirmed Soil Contamination ?(Y/N)
Comm/Non-Commercial?
Reported by (circle one): Phone, Fax or Report
Samples Taken?(Y/N)
Reg/Non-regulated?
Region
Free Product? (Y/N) If Yes, State Greatest
Thickness
INCIDENT DESCRIPTION
Incident Name:
U1212ard Property
Address:
County: Mecklenburg
Regional Office
(circle one): Asheville, Mooresville, Fayetteville,
City/Town: Charlotte
28210 Zip Code:
Raleigh, Washington, Wilmington, Winston-Salem
Latitude (decimal degrees): 35.150050 Longitude (decimal degrees) : __80.844697
Obtained by:
❑ GPS
Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount
of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors
❑ Topographic map
GIs Address matching
❑ Other
❑ Unknown
Describe location:
Home Heating Oil UST identified during sale of property. Soil borings and
samples
adjacent to UST ends detected petroleum compounds.
Google Earth
HOW RELEASE WAS DISCOVERED (Release code)
(Check one)
❑ Release Detection Equipment or Methods ❑ Visual/Odor
❑ Groundwater Contamination
❑ During UST Closure/Removal ❑ Water in Tank
❑ Surface Water Contamination
® Property Transfer ❑ Water Supply Well Contamination
❑ Other (specify)
SOURCE OF CONTAMINATION
Source of Release Cause of Release Type of Release
Product Type Released
(Check one to indicate primary (Check one to indicate primary (Check one)
(Check one to indicate primary product type
source) cause)
released)
M Tank ❑ Spill Petroleum ❑
Gasoline/ Diesel/ ❑ Diesel/Veg. Oil
❑ Piping ❑Overfill ❑Non -Petroleum a
Kerosene Blend
❑
Heating Oil Vegetable Oil 100%
❑ Dispenser M Corrosion ❑ Both ❑
Other Petroleum ❑ E10 — E20
❑ Submersible Turbine Pump ❑ Physical or Mechanical
Products
❑ E21 E84
Damage Location ❑
❑ Delivery Problem
❑
—
Metals
❑ E85 E99
o
❑ Install Problem (Checkne )
Other Inorganics —
❑ Other ❑ Other ❑
❑Facility
Other Organics ❑ Ethanol 100%
❑ Unknown
❑ Unknown M Residence
❑ E01 — E09
Definitions presented on reverse I Definitions presented on reverse I ❑ Other
Ownership
1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State
Operation Type
1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial
7. Mining
UST Form 61 (02/08) Page 1 of 2

IMPACT ON DRINKING WATER SUPPLIES
Water Supply Wells Affected? 1. Yes
2. No 3. Unknown
Number of Water Supply Wells Affected
Water Supply Wells Contaminated: (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary)
1.
2.
3.
UST SYSTEM OWNER
UST Owner/Company
Point of Contact
Address
Lars Li and
5700 Closeburn Road
City
State
Zip Code
Telephone Number
Charlotte
NC
28210
UST SYSTEM OPERATOR
Same as above
UST Operator/Company
Address
City
State
Zip Code
Telephone Number
LANDOWNER AT LOCATION OF UST INCIDENT
Landowner
Address
Same as owner
City
State
Zip Code
Telephone Number
Draw Sketch of Area (showing two major road intersections) or Attach Map
Map Attached
Person Reporting Incident Patrick Lowery
77777
Company SUMMIT ELT PC
Telephone Number
Title Env Manager
Address 3575 Centre Circle Dr
I Date 1/22/18
UST Form 61 (02/08)
Page 2 of 2
Definitions of Sources
Tank: means the tank that stores the product and is part of the underground storage tank system
Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end -use equipment (Vent, vapor recovery, or fill
lines are excluded.)
Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above
the shear valve)
Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that
connects the submersible turbine pump to the tank
Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.)
Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor
recovery lines, and fill lines)
Unknown: identifies releases for which the source has not been determined
Definitions of Causes
Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser)
Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser)
Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken
components, and components that have changed dimension)
Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust)
Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly
Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells)
Unknown: use when the cause has not been determined

Source: Base Map provided by Mecklenburg County GIS
Location Map
//Ad& Llppard Property
5700 Closeburn Road
SUMMIT Charlotte, NC
f I,
Saussy Burbank
2550 West Tyvola Road
Suite 100
Charlotte, NC 28217
ilk
Checked By\Date: MZ/12/17
Scale
Not to Scale
Figure 1

Page 1 of 1
Table 1.0: Soil Sample Summary Table
All Values in mg/kg
CAS
Analyte
1330-20-7
Xylenes (total)
92-52-4
1,1 - Biphenyl
86-73-7
Fluorene
91-57-6
2-Methylnaphthalene
91-20-3
Naphthalene
67580
Phenanthrene
129-00-0
Pyrene
N/A
Aliphatics, C5-C8
N/A
Aliphatics, C9-C18
N/A
Aliphatics, C19-06
N/A
Aromatics, C9-C22
MSCCs Soil
to Water
Maximum
MSCCs
Residential
Cleanup
T-1 North
1/5/2018
8' bgs
Result RL
T-1 South
1/5/2018
8' bgs
Result RL
4.60E+00
3.13E+03
3.8
3.9
NA
NA
8.4
8.1
8.7
8.1
4.70E+01
6.20E+02
12.0
1.6
13.0
1.6
3.60E+00
6.30E+01
110.0
1.6
110.0
1.6
1.60E-01
3.13E+02
16.0
1.6
16.0
1.6
5.60E+01
4.69E+02
30.0
1.6
32.0
1.6
2.70E+02
4.69E+02
5.2
1.6
5.7
1.6
6.80E+01
9.39E+02
55.0
46.0
36.0
46.0
5.40E+02
1.50E+03
4900.0
460.0
5100.0
460.0
NA
3.10E+04
980.0
610.0
1000.0
610.0
3.10E+01
4.69E+02
4600.0
61.0
4040.0
61.0
ND = Below P ND = Below Method Detection Limit
BOLD = Concentration Above Reference Values
J = Estimated Concentration
5700 C/oseburn Road - Lippard January 22, 2018
Charlotte, NC SUMMIT Project No: 1820.75

1 /23/2018
Property Detail Print View
#"V.
Parcel Information
Parcel ID Account
17125219 INDIVIDUAL
Owner(s)
Owner Name
LIPPARD JOHN BEAUREGARD
LIPPARD DELLA W WIFE
% LIPPARD LARS
Legal Information
Legal Municipality
L13 B2 M8-361 CHARLOTTE
Total Parcel Assessment
Building Land
Features
170100 250000
1700
Sales Information
Sale Price
Stamps
Jan 1 1975 0
Land Use
Use Units
Type
R100 1
LT
Building Information
Bldg Description
Typo
1 Single-Fam
RES
Bldg Story Units
Total SgFt
1 1 STORY 1
4820
Bldg Heat Fuel
Fire Place
1 AIR -DUCTED GAS
1 - FP3
Sub Area
Mailing Address
5700 CLOSEBURN RD
5700 CLOSEBURN RD
5700 CLOSEBURN RD
Date Annexed
Total
421800
Qualify
Parent
Print
Close
Previous
City/State
CHARLOTTE NC 28210
CHARLOTTE NC 28210
CHARLOTTE NC 28210
Special District Fire District Acreage
CITY OF CHARLOTTE 0
Exemptions
Exemption Year Approved Review Date Amount
VI Type
IMP DEED STAMPS
Neighborhood
R120
Legal Ref.
02023-026
Assessment
250000
Year Property Location
1956 5700 CLOSEBURN RD CHARLOTTE
Heated SgFt Foundation Ext. Wall
1998 CRAWL SPACE FACE BRICK -
AC Fixtures Bedrooms Full Baths
AC -CENTRAL 0 3 3
Bldg Description
1 BASE (FIRST FLOOR)
1 PORCH - OPEN - FINISHED
1 PORCH - SCREENED - UNFINISHED
1 CARPORT - FINISHED
1 PORCH - OPEN - FINISHED
1 BASEMENT - UNFINISHED
1 UTILITY - UNFINISHED
Depreciation
Bldg Physical Functional Economic
1 AV - 16.00% - 0.00% -0.00%
Special Features & Yard Items
Bldg Built Type Quantity
1 2005 DECK 1
Notes
Tax Year Notes
2011 Informal Review Request Received
Value Changes
Notice Date
Tax Year
Reason
Feb 8 2011
2011
Countywide Revaluation
Apr 11 2006
2006
Remodeled and/or New Addition
Apr 11 2006
2006
Remodeled Improvements and/or New Additi
Jan 17 2003
2003
Countywide Revaluation
Jan 5 1998
1998
Countywide Revaluation
Oct 8 1991
1991
Reviewed - No change in value
Jan 2 1991
1991
Countywide Revaluation
Units
160.00000
Special
-0.00%
Grantor
Grade Value
AVERAGE 03 170100
3/4 Baths 1/2 Baths
0 0
Size
1998
30
320
440
32
1920
80
Override
- 0.00%
Value
1700
Note Date
04/15/2011
Changed To
Deferred
629700
0
317400
0
317400
0
315900
0
187150
172810
172810
http://meckcama.co.mecklenburg.nc.us/RELookup/Property/Print?parcelld=l 7125219 1 /1

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
SUMMIT Engineering, Laboratory & Testing, P.C.
3575 Centre Circle
Fort Mill, SC 28715
Attention: Patrick Lowery
Project Name: 5700 Closeburn
Project Number: 1820.75
Lot Number:TA09026
Date Completed:01/12/2018
01/12/2018 4:43 PM
Approved and released by:
Project Manager: Lucas Odom
pCCRF
LABORATORY
ACCREDITATION
xEcucxaeu BUREAU dmsio„ofas-e
qe ACCREDITED I50/IEC 17025
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 1 of 38

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: TA09026
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative.
The sample receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC
standards, the Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating
procedures (SOPs), and Shealy policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the
results page or discussed below.
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W" qualifier
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
VPH
Surrogate recovery for the following samples was outside control limits: TA09026-001, TA09026-002. Evidence of matrix interference
is present; therefore, re -extraction and/or re -analysis was not performed.
SVOCs by GC/MS
Due to the large number of spiked analytes, there is a high probability that one or more analytes will recover outside acceptance limits.
The laboratory's SOP allows for 10% of analytes to recover marginally outside criteria. The following analytes recovered marginally
outside LCS/LCSD criteria: 3,3'-Dichlorobenzidine and 2-methyl phenol.
The laboratory control sample (LCS) for analytical batch 61529 exceeded acceptance criteria for the following analytes: pyridine.
These analytes were biased high and were not detected in the samples affected: TA09026-001, TA09026-002.
EPH
Surrogate recovery for the following samples was outside control limits: TA09026-001, TA09026-002. Evidence of matrix interference
is present; therefore, re -extraction and/or re -analysis was not performed.
VOCs by GC/MS
The following sample was diluted due to the nature of the sample matrix: TA09026-001, TA09026-002. The LOQ has been elevated to
reflect the dilution.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 2 of 38

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
SUMMIT Engineering, Laboratory & Testing, P.C.
Lot Number: TA09026
Sample Number Sample ID Matrix Date Sampled Date Received
001 T-1 NORTH Solid 01/05/2018 1400 01/09/2018
002 T-1 SOUTH Solid 01/05/2018 1410 01/09/2018
(2 samples)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 3 of 38

SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
SUMMIT Engineering, Laboratory
& Testing, P.C.
Lot Number: TA09026
Sample Sample ID
Matrix
Parameter
Method
Result Q
Units
Page
001
T-1 NORTH
Solid
Xylenes (total)
8260B
3800
ug/kg
6
001
T-1 NORTH
Solid
1,1'-Biphenyl
8270D
8400
ug/kg
6
001
T-1 NORTH
Solid
Fluorene
8270D
12000
ug/kg
7
001
T-1 NORTH
Solid
2-Methylnaphthalene
8270D
110000
ug/kg
7
001
T-1 NORTH
Solid
Naphthalene
8270D
16000
ug/kg
7
001
T-1 NORTH
Solid
Phenanthrene
8270D
30000
ug/kg
8
001
T-1 NORTH
Solid
Pyrene
8270D
5200
ug/kg
8
001
T-1 NORTH
Solid
C9 - C18 Aliphatics
MADEP-EPH-
4900
mg/kg
8
001
T-1 NORTH
Solid
C19 - C36 Aliphatics
MADEP-EPH-
980
mg/kg
8
001
T-1 NORTH
Solid
C11 - C22 Aromatics
MADEP-EPH-
4100
mg/kg
8
001
T-1 NORTH
Solid
C5 - C8 Aliphatics
MADEP-VPH-
55
mg/kg
9
001
T-1 NORTH
Solid
C9 - C12 Aliphatics
MADEP-VPH-
500
mg/kg
9
001
T-1 NORTH
Solid
C9 - C10 Aromatics
MADEP-VPH-
500
mg/kg
9
002
T-1 SOUTH
Solid
Xylenes (total)
8260B
3900
ug/kg
11
002
T-1 SOUTH
Solid
1,1'-Biphenyl
8270D
8700
ug/kg
11
002
T-1 SOUTH
Solid
Fluorene
8270D
13000
ug/kg
12
002
T-1 SOUTH
Solid
2-Methylnaphthalene
8270D
110000
ug/kg
12
002
T-1 SOUTH
Solid
Naphthalene
8270D
16000
ug/kg
12
002
T-1 SOUTH
Solid
Phenanthrene
8270D
32000
ug/kg
13
002
T-1 SOUTH
Solid
Pyrene
8270D
5700
ug/kg
13
002
T-1 SOUTH
Solid
C9 - C18 Aliphatics
MADEP-EPH-
5100
mg/kg
13
002
T-1 SOUTH
Solid
C19 - C36 Aliphatics
MADEP-EPH-
1000
mg/kg
13
002
T-1 SOUTH
Solid
C11 - C22 Aromatics
MADEP-EPH-
3600
mg/kg
13
002
T-1 SOUTH
Solid
C5 - C8 Aliphatics
MADEP-VPH-
36
mg/kg
14
002
T-1 SOUTH
Solid
C9 - C12 Aliphatics
MADEP-VPH-
370
mg/kg
14
002
T-1 SOUTH
Solid
C9 - C10 Aromatics
MADEP-VPH-
440
mg/kg
14
(26 detections)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 4 of 38

Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: TA09026-001
Description: T-1 NORTH Matrix: Solid
Date Sampled:01/05/2018 1400 % Solids: 76.2 01/09/2018 2030
Date Received: 01 /09/2018
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
2 5035 High 8260B 4 01/11/2018 1455 JM1 61692 5.07
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Acetone
67-64-1
8260B
ND
6400
ug/kg
Benzene
71-43-2
8260B
ND
1600
ug/kg
Bromodichloromethane
75-27-4
8260B
ND
1600
ug/kg
Bromoform
75-25-2
8260B
ND
1600
ug/kg
Bromomethane (Methyl bromide)
74-83-9
8260B
ND
1600
ug/kg
2-Butanone (MEK)
78-93-3
8260B
ND
6400
ug/kg
Carbon disulfide
75-15-0
8260B
ND
1600
ug/kg
Carbon tetrachloride
56-23-5
8260B
ND
1600
ug/kg
Chlorobenzene
108-90-7
8260B
ND
1600
ug/kg
Chloroethane
75-00-3
8260B
ND
1600
ug/kg
Chloroform
67-66-3
8260B
ND
1600
ug/kg
Chloromethane (Methyl chloride)
74-87-3
8260B
ND
1600
ug/kg
Cyclohexane
110-82-7
8260B
ND
1600
ug/kg
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260B
ND
1600
ug/kg
Dibromochloromethane
124-48-1
8260B
ND
1600
ug/kg
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1600
ug/kg
1,2-Dichlorobenzene
95-50-1
8260B
ND
1600
ug/kg
1,3-Dichlorobenzene
541-73-1
8260B
ND
1600
ug/kg
1,4-Dichlorobenzene
106-46-7
8260B
ND
1600
ug/kg
Dichlorodifluoromethane
75-71-8
8260B
ND
1600
ug/kg
1,1-Dichloroethane
75-34-3
8260B
ND
1600
ug/kg
1,2-Dichloroethane
107-06-2
8260B
ND
1600
ug/kg
1,1-Dichloroethene
75-35-4
8260B
ND
1600
ug/kg
cis- 1,2-Dichloroethene
156-59-2
8260B
ND
1600
ug/kg
trans-1,2-Dichloroethene
156-60-5
8260B
ND
1600
ug/kg
1,2-Dichloropropane
78-87-5
8260B
ND
1600
ug/kg
cis- 1,3-Dichloropropene
10061-01-5
8260B
ND
1600
ug/kg
trans- 1,3-Dichloropropene
10061-02-6
8260B
ND
1600
ug/kg
Ethylbenzene
100-41-4
8260B
ND
1600
ug/kg
2-Hexanone
591-78-6
8260B
ND
3200
ug/kg
Isopropylbenzene
98-82-8
8260B
ND
1600
ug/kg
Methyl acetate
79-20-9
8260B
ND
1600
ug/kg
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260B
ND
1600
ug/kg
4-Methyl-2-pentanone
108-10-1
8260B
ND
3200
ug/kg
Methylcyclohexane
108-87-2
8260B
ND
1600
ug/kg
Methylene chloride
75-09-2
8260B
ND
1600
ug/kg
Styrene
100-42-5
8260B
ND
1600
ug/kg
1,1,2,2-Tetrachloroethane
79-34-5
8260B
ND
1600
ug/kg
Tetrachloroethene
127-18-4
8260B
ND
1600
ug/kg
Toluene
108-88-3
8260B
ND
1600
ug/kg
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 5 of 38

Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: TA09026-001
Description: T-1 NORTH Matrix: Solid
Date Sampled:01/05/2018 1400 % Solids: 76.2 01/09/2018 2030
Date Received: 01 /09/2018
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Sample Wt.(g)
2 5035 High
8260B 4 01/11/2018 1455 JM1
61692 5.07
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B
ND
1600
ug/kg
2
1,2,4-Trichlorobenzene
120-82-1 8260B
ND
1600
ug/kg
2
1,1,1-Trichloroethane
71-55-6 8260B
ND
1600
ug/kg
2
1,1,2-Trichloroethane
79-00-5 8260B
ND
1600
ug/kg
2
Trichloroethene
79-01-6 8260B
ND
1600
ug/kg
2
Trichlorofluoromethane
75-69-4 8260B
ND
1600
ug/kg
2
Vinyl chloride
75-01-4 8260B
ND
1600
ug/kg
2
Xylenes (total)
1330-20-7 8260B
3800
3200
ug/kg
2
Run 2 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
102 53-142
Bromofluorobenzene
85 47-138
Toluene-d8
82 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270D 20 01/11/2018 1058 CMP2
01/09/2018 1740 61480
2 3546
8270D 100 01/11/2018 1147 CMP2
01/09/2018 1740 61480
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9 8270D
ND
340
ug/kg
1
Acenaphthylene
208-96-8 8270D
ND
340
ug/kg
1
Acetophenone
98-86-2 8270D
ND
1700
ug/kg
1
Anthracene
120-12-7 8270D
ND
340
ug/kg
1
Atrazine
1912-24-9 8270D
ND
1700
ug/kg
1
Benzaldehyde
100-52-7 8270D
ND
1700
ug/kg
1
Benzo(a)anthracene
56-55-3 8270D
ND
340
ug/kg
1
Benzo(a)pyrene
50-32-8 8270D
ND
340
ug/kg
1
Benzo(b)fluoranthene
205-99-2 8270D
ND
340
ug/kg
1
Benzo(g,h,i)perylene
191-24-2 8270D
ND
340
ug/kg
1
Benzo(k)fluoranthene
207-08-9 8270D
ND
340
ug/kg
1
1,1'-Biphenyl
92-52-4 8270D
8400
1700
ug/kg
1
4-Bromophenyl phenyl ether
101-55-3 8270D
ND
1700
ug/kg
1
Butyl benzyl phthalate
85-68-7 8270D
ND
1700
ug/kg
1
Caprolactam
105-60-2 8270D
ND
1700
ug/kg
1
Carbazole
86-74-8 8270D
ND
1700
ug/kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1 8270D
ND
1700
ug/kg
1
4-Chloro-3-methyl phenol
59-50-7 8270D
ND
1700
ug/kg
1
4-Chloroaniline
106-47-8 8270D
ND
1700
ug/kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N =
Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W =
Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 6 of 38

Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: TA09026-001
Description: T-1 NORTH Matrix: Solid
Date Sampled:01/05/2018 1400 % Solids: 76.2 01/09/2018 2030
Date Received: 01 /09/2018
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 20 01/11/2018 1058 CMP2 01/09/2018 1740 61480
2 3546 8270D 100 01/11/2018 1147 CMP2 01/09/2018 1740 61480
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
bis(2-Chloroethoxy)methane
111-91-1
8270D
ND
1700
ug/kg
bis(2-Chloroethyl)ether
111-44-4
8270D
ND
1700
ug/kg
2-Chloronaphthalene
91-58-7
8270D
ND
1700
ug/kg
2-Chlorophenol
95-57-8
8270D
ND
1700
ug/kg
4-Chlorophenyl phenyl ether
7005-72-3
8270D
ND
1700
ug/kg
Chrysene
218-01-9
8270D
ND
340
ug/kg
Dibenzo(a,h)anthracene
53-70-3
8270D
ND
340
ug/kg
Dibenzofuran
132-64-9
8270D
ND
1700
ug/kg
3,3'-Dichlorobenzidine
91-94-1
8270D
ND
1700
ug/kg
2,4-Dichlorophenol
120-83-2
8270D
ND
1700
ug/kg
Diethylphthalate
84-66-2
8270D
ND
1700
ug/kg
Dimethyl phthalate
131-11-3
8270D
ND
1700
ug/kg
2,4-Dimethylphenol
105-67-9
8270D
ND
1700
ug/kg
Di-n-butyl phthalate
84-74-2
8270D
ND
1700
ug/kg
4,6-Dinitro-2-methylphenol
534-52-1
8270D
ND
8500
ug/kg
2,4-Dinitrophenol
51-28-5
8270D
ND
8500
ug/kg
2,4-Dinitrotoluene
121-14-2
8270D
ND
3300
ug/kg
2,6-Dinitrotoluene
606-20-2
8270D
ND
3300
ug/kg
Di-n-octylphthalate
117-84-0
8270D
ND
1700
ug/kg
bis(2-Ethylhexyl)phthalate
117-81-7
8270D
ND
1700
ug/kg
Fluoranthene
206-44-0
8270D
ND
340
ug/kg
Fluorene
86-73-7
8270D
12000
340
ug/kg
Hexachlorobenzene
118-74-1
8270D
ND
1700
ug/kg
Hexachlorobutadiene
87-68-3
8270D
ND
1700
ug/kg
Hexachlorocyclopentadiene
77-47-4
8270D
ND
8500
ug/kg
Hexachloroethane
67-72-1
8270D
ND
1700
ug/kg
Indeno(1,2,3-c,d)pyrene
193-39-5
8270D
ND
340
ug/kg
Isophorone
78-59-1
8270D
ND
1700
ug/kg
2-Methylnaphthalene
91-57-6
8270D
110000
1700
ug/kg
2-Methylphenol
95-48-7
8270D
ND
1700
ug/kg
3+4-Methylphenol
106-44-5
8270D
ND
3300
ug/kg
Naphthalene
91-20-3
8270D
16000
340
ug/kg
2-Nitroaniline
88-74-4
8270D
ND
3300
ug/kg
3-Nitroaniline
99-09-2
8270D
ND
3300
ug/kg
4-Nitroaniline
100-01-6
8270D
ND
3300
ug/kg
Nitrobenzene
98-95-3
8270D
ND
1700
ug/kg
2-Nitrophenol
88-75-5
8270D
ND
3300
ug/kg
4-Nitrophenol
100-02-7
8270D
ND
8500
ug/kg
N-Nitrosodi-n-propylamine
621-64-7
8270D
ND
1700
ug/kg
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 7 of 38

Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: TA09026-001
Description: T-1 NORTH Matrix: Solid
Date Sampled:01/05/2018 1400 % Solids: 76.2 01/09/2018 2030
Date Received: 01 /09/2018
Semivolatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546
8270D 20 01/11/2018 1058 CMP2 01/09/2018 1740 61480
2 3546
8270D 100 01/11/2018 1147 CMP2 01/09/2018 1740 61480
CAS Analytical
Parameter
Number Method Result Q LOQ
Units
Run
N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 8270D ND 1700
ug/kg
1
Pentachlorophenol
87-86-5 8270D ND 8500
ug/kg
1
Phenanthrene
85-01-8 8270D 30000 340
ug/kg
1
Phenol
108-95-2 8270D ND 1700
ug/kg
1
Pyrene
129-00-0 8270D 5200 340
ug/kg
1
Pyridine
110-86-1 8270D ND 1700
ug/kg
1
2,4,5-Trichlorophenol
95-95-4 8270D ND 1700
ug/kg
1
2,4,6-Trichlorophenol
88-06-2 8270D ND 1700
ug/kg
1
Run 1 Acceptance Run 2 Acceptance
Surrogate
Q % Recovery Limits Q % Recovery Limits
2-Fluorobiphenyl
118 24-137 125 24-137
2-Fluorophenol
79 16-136 61 16-136
Nitrobenzene-d5
121 12-144 119 12-144
Phenol-d5
86 26-148 73 26-148
Terphenyl-d14
96 20-127 91 20-127
2,4,6-Tribromophenol
127 27-128 87 27-128
MA EPH (aliphatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH-
MADEP-EPH-04 1 01/11/2018 1156 PMS 01/10/2018 0915 61511
CAS Analytical
Parameter
Number Method Result Q LOQ
Units
Run
C9 - C18 Aliphatics
MADEP-EPH- 4900 13
mg/kg
1
C19 - C36 Aliphatics
MADEP-EPH- 980 13
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
49 40-140
MA EPH (aromatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH-
MADEP-EPH-04 1 01/11/2018 1425 PMS 01/10/2018 0915 61512
CAS Analytical
Parameter
Number Method Result Q LOQ
Units
Run
C11 - C22 Aromatics
MADEP-EPH- 4100 13
mg/kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W
= Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 8 of 38

Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: TA09026-001
Description: T-1 NORTH Matrix: Solid
Date Sampled:01/05/2018 1400 % Solids: 76.2 01/09/2018 2030
Date Received: 01 /09/2018
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Bromonaphthalene (fractionation 2) N
155 40-140
2-Fluorobiphenyl (fractionation 1)
N
235 40-140
o - Terphenyl (aromatic)
N
158 40-140
MADEP VPH (aliphatics)
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date
Batch
1 VPH
MADEP-VPH-04-1.1
5 01/10/20181328 JJG
61576
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
C5 - C8 Aliphatics
MADEP-VPH- 55
24
mg/kg
1
C9 - C12 Aliphatics
MADEP-VPH- 500
24
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2,5-Dibromotoluene (FID)
N
0.00 70-130
MADEP VPH (aromatics)
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date
Batch
1 VPH
MADEP-VPH-04-1.1
5 01/10/20181328 JJG
61575
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
C9 - C10 Aromatics
MADEP-VPH- 500
8.0
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2,5-Dibromotoluene (PID)
N
0.00 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 9 of 38

Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: TA09026-002
Description: T-1 SOUTH Matrix: Solid
Date Sampled:01/05/2018 1410 % Solids: 76.5 01/09/2018 2030
Date Received: 01 /09/2018
Volatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch Sample Wt.(g)
2 5035 High 8260B 4 01/11/2018 1539 JM1 61692 5.27
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
Acetone
67-64-1
8260B
ND
6200
ug/kg
Benzene
71-43-2
8260B
ND
1500
ug/kg
Bromodichloromethane
75-27-4
8260B
ND
1500
ug/kg
Bromoform
75-25-2
8260B
ND
1500
ug/kg
Bromomethane (Methyl bromide)
74-83-9
8260B
ND
1500
ug/kg
2-Butanone (MEK)
78-93-3
8260B
ND
6200
ug/kg
Carbon disulfide
75-15-0
8260B
ND
1500
ug/kg
Carbon tetrachloride
56-23-5
8260B
ND
1500
ug/kg
Chlorobenzene
108-90-7
8260B
ND
1500
ug/kg
Chloroethane
75-00-3
8260B
ND
1500
ug/kg
Chloroform
67-66-3
8260B
ND
1500
ug/kg
Chloromethane (Methyl chloride)
74-87-3
8260B
ND
1500
ug/kg
Cyclohexane
110-82-7
8260B
ND
1500
ug/kg
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260B
ND
1500
ug/kg
Dibromochloromethane
124-48-1
8260B
ND
1500
ug/kg
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
1500
ug/kg
1,2-Dichlorobenzene
95-50-1
8260B
ND
1500
ug/kg
1,3-Dichlorobenzene
541-73-1
8260B
ND
1500
ug/kg
1,4-Dichlorobenzene
106-46-7
8260B
ND
1500
ug/kg
Dichlorodifluoromethane
75-71-8
8260B
ND
1500
ug/kg
1,1-Dichloroethane
75-34-3
8260B
ND
1500
ug/kg
1,2-Dichloroethane
107-06-2
8260B
ND
1500
ug/kg
1,1-Dichloroethene
75-35-4
8260B
ND
1500
ug/kg
cis- 1,2-Dichloroethene
156-59-2
8260B
ND
1500
ug/kg
trans-1,2-Dichloroethene
156-60-5
8260B
ND
1500
ug/kg
1,2-Dichloropropane
78-87-5
8260B
ND
1500
ug/kg
cis- 1,3-Dichloropropene
10061-01-5
8260B
ND
1500
ug/kg
trans- 1,3-Dichloropropene
10061-02-6
8260B
ND
1500
ug/kg
Ethylbenzene
100-41-4
8260B
ND
1500
ug/kg
2-Hexanone
591-78-6
8260B
ND
3100
ug/kg
Isopropylbenzene
98-82-8
8260B
ND
1500
ug/kg
Methyl acetate
79-20-9
8260B
ND
1500
ug/kg
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260B
ND
1500
ug/kg
4-Methyl-2-pentanone
108-10-1
8260B
ND
3100
ug/kg
Methylcyclohexane
108-87-2
8260B
ND
1500
ug/kg
Methylene chloride
75-09-2
8260B
ND
1500
ug/kg
Styrene
100-42-5
8260B
ND
1500
ug/kg
1,1,2,2-Tetrachloroethane
79-34-5
8260B
ND
1500
ug/kg
Tetrachloroethene
127-18-4
8260B
ND
1500
ug/kg
Toluene
108-88-3
8260B
ND
1500
ug/kg
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 10 of 38

Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: TA09026-002
Description: T-1 SOUTH Matrix: Solid
Date Sampled:01/05/2018 1410 % Solids: 76.5 01/09/2018 2030
Date Received: 01 /09/2018
Volatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch Sample Wt.(g)
2 5035 High
8260B 4 01/11/2018 1539 JM1
61692 5.27
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
1,1,2-Trichloro-1,2,2-Trifluoroethane 76-13-1 8260B
ND
1500
ug/kg
2
1,2,4-Trichlorobenzene
120-82-1 8260B
ND
1500
ug/kg
2
1,1,1-Trichloroethane
71-55-6 8260B
ND
1500
ug/kg
2
1,1,2-Trichloroethane
79-00-5 8260B
ND
1500
ug/kg
2
Trichloroethene
79-01-6 8260B
ND
1500
ug/kg
2
Trichlorofluoromethane
75-69-4 8260B
ND
1500
ug/kg
2
Vinyl chloride
75-01-4 8260B
ND
1500
ug/kg
2
Xylenes (total)
1330-20-7 8260B
3900
3100
ug/kg
2
Run 2 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
94 53-142
Bromofluorobenzene
82 47-138
Toluene-d8
79 68-124
Semivolatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3546
8270D 20 01/11/2018 1123 CMP2
01/09/2018 1740 61480
2 3546
8270D 100 01/11/2018 1212 CMP2
01/09/2018 1740 61480
CAS Analytical
Parameter
Number Method
Result Q
LOQ
Units
Run
Acenaphthene
83-32-9 8270D
ND
350
ug/kg
1
Acenaphthylene
208-96-8 8270D
ND
350
ug/kg
1
Acetophenone
98-86-2 8270D
ND
1700
ug/kg
1
Anthracene
120-12-7 8270D
ND
350
ug/kg
1
Atrazine
1912-24-9 8270D
ND
1700
ug/kg
1
Benzaldehyde
100-52-7 8270D
ND
1700
ug/kg
1
Benzo(a)anthracene
56-55-3 8270D
ND
350
ug/kg
1
Benzo(a)pyrene
50-32-8 8270D
ND
350
ug/kg
1
Benzo(b)fluoranthene
205-99-2 8270D
ND
350
ug/kg
1
Benzo(g,h,i)perylene
191-24-2 8270D
ND
350
ug/kg
1
Benzo(k)fluoranthene
207-08-9 8270D
ND
350
ug/kg
1
1,1'-Biphenyl
92-52-4 8270D
8700
1700
ug/kg
1
4-Bromophenyl phenyl ether
101-55-3 8270D
ND
1700
ug/kg
1
Butyl benzyl phthalate
85-68-7 8270D
ND
1700
ug/kg
1
Caprolactam
105-60-2 8270D
ND
1700
ug/kg
1
Carbazole
86-74-8 8270D
ND
1700
ug/kg
1
bis (2-Chloro-1-methylethyl) ether
108-60-1 8270D
ND
1700
ug/kg
1
4-Chloro-3-methyl phenol
59-50-7 8270D
ND
1700
ug/kg
1
4-Chloroaniline
106-47-8 8270D
ND
1700
ug/kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N =
Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W =
Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 11 of 38

Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: TA09026-002
Description: T-1 SOUTH Matrix: Solid
Date Sampled:01/05/2018 1410 % Solids: 76.5 01/09/2018 2030
Date Received: 01 /09/2018
Semivolatile Organic Compounds by GC/MS
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546 8270D 20 01/11/2018 1123 CMP2 01/09/2018 1740 61480
2 3546 8270D 100 01/11/2018 1212 CMP2 01/09/2018 1740 61480
CAS Analytical
Parameter Number Method Result Q LOQ Units Run
bis(2-Chloroethoxy)methane
111-91-1
8270D
ND
1700
ug/kg
bis(2-Chloroethyl)ether
111-44-4
8270D
ND
1700
ug/kg
2-Chloronaphthalene
91-58-7
8270D
ND
1700
ug/kg
2-Chlorophenol
95-57-8
8270D
ND
1700
ug/kg
4-Chlorophenyl phenyl ether
7005-72-3
8270D
ND
1700
ug/kg
Chrysene
218-01-9
8270D
ND
350
ug/kg
Dibenzo(a,h)anthracene
53-70-3
8270D
ND
350
ug/kg
Dibenzofuran
132-64-9
8270D
ND
1700
ug/kg
3,3'-Dichlorobenzidine
91-94-1
8270D
ND
1700
ug/kg
2,4-Dichlorophenol
120-83-2
8270D
ND
1700
ug/kg
Diethylphthalate
84-66-2
8270D
ND
1700
ug/kg
Dimethyl phthalate
131-11-3
8270D
ND
1700
ug/kg
2,4-Dimethylphenol
105-67-9
8270D
ND
1700
ug/kg
Di-n-butyl phthalate
84-74-2
8270D
ND
1700
ug/kg
4,6-Dinitro-2-methylphenol
534-52-1
8270D
ND
8600
ug/kg
2,4-Dinitrophenol
51-28-5
8270D
ND
8600
ug/kg
2,4-Dinitrotoluene
121-14-2
8270D
ND
3400
ug/kg
2,6-Dinitrotoluene
606-20-2
8270D
ND
3400
ug/kg
Di-n-octylphthalate
117-84-0
8270D
ND
1700
ug/kg
bis(2-Ethylhexyl)phthalate
117-81-7
8270D
ND
1700
ug/kg
Fluoranthene
206-44-0
8270D
ND
350
ug/kg
Fluorene
86-73-7
8270D
13000
350
ug/kg
Hexachlorobenzene
118-74-1
8270D
ND
1700
ug/kg
Hexachlorobutadiene
87-68-3
8270D
ND
1700
ug/kg
Hexachlorocyclopentadiene
77-47-4
8270D
ND
8600
ug/kg
Hexachloroethane
67-72-1
8270D
ND
1700
ug/kg
Indeno(1,2,3-c,d)pyrene
193-39-5
8270D
ND
350
ug/kg
Isophorone
78-59-1
8270D
ND
1700
ug/kg
2-Methylnaphthalene
91-57-6
8270D
110000
1700
ug/kg
2-Methylphenol
95-48-7
8270D
ND
1700
ug/kg
3+4-Methylphenol
106-44-5
8270D
ND
3400
ug/kg
Naphthalene
91-20-3
8270D
16000
350
ug/kg
2-Nitroaniline
88-74-4
8270D
ND
3400
ug/kg
3-Nitroaniline
99-09-2
8270D
ND
3400
ug/kg
4-Nitroaniline
100-01-6
8270D
ND
3400
ug/kg
Nitrobenzene
98-95-3
8270D
ND
1700
ug/kg
2-Nitrophenol
88-75-5
8270D
ND
3400
ug/kg
4-Nitrophenol
100-02-7
8270D
ND
8600
ug/kg
N-Nitrosodi-n-propylamine
621-64-7
8270D
ND
1700
ug/kg
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 12 of 38

Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: TA09026-002
Description: T-1 SOUTH Matrix: Solid
Date Sampled:01/05/2018 1410 % Solids: 76.5 01/09/2018 2030
Date Received: 01 /09/2018
Semivolatile Organic Compounds by GC/MS
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3546
8270D 20 01/11/2018 1123 CMP2 01/09/2018 1740 61480
2 3546
8270D 100 01/11/2018 1212 CMP2 01/09/2018 1740 61480
CAS Analytical
Parameter
Number Method Result Q LOQ
Units
Run
N-Nitrosodiphenylamine (Diphenylamine) 86-30-6 8270D ND 1700
ug/kg
1
Pentachlorophenol
87-86-5 8270D ND 8600
ug/kg
1
Phenanthrene
85-01-8 8270D 32000 350
ug/kg
1
Phenol
108-95-2 8270D ND 1700
ug/kg
1
Pyrene
129-00-0 8270D 5700 350
ug/kg
1
Pyridine
110-86-1 8270D ND 1700
ug/kg
1
2,4,5-Trichlorophenol
95-95-4 8270D ND 1700
ug/kg
1
2,4,6-Trichlorophenol
88-06-2 8270D ND 1700
ug/kg
1
Run 1 Acceptance Run 2 Acceptance
Surrogate
Q % Recovery Limits Q % Recovery Limits
2-Fluorobiphenyl
126 24-137 94 24-137
2-Fluorophenol
80 16-136 60 16-136
Nitrobenzene-d5
119 12-144 128 12-144
Phenol-d5
88 26-148 81 26-148
Terphenyl-d14
97 20-127 96 20-127
2,4,6-Tribromophenol
N 136 27-128 89 27-128
MA EPH (aliphatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH-
MADEP-EPH-04 1 01/11/2018 1226 PMS 01/10/2018 0915 61511
CAS Analytical
Parameter
Number Method Result Q LOQ
Units
Run
C9 - C18 Aliphatics
MADEP-EPH- 5100 13
mg/kg
1
C19 - C36 Aliphatics
MADEP-EPH- 1000 13
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
49 40-140
MA EPH (aromatics)
Run Prep Method
Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH-
MADEP-EPH-04 1 01/11/2018 1454 PMS 01/10/2018 0915 61512
CAS Analytical
Parameter
Number Method Result Q LOQ
Units
Run
C11 - C22 Aromatics
MADEP-EPH- 3600 13
mg/kg
1
LOQ = Limit of Quantitation B =
Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W
= Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 13 of 38

Client: SUMMIT Engineering, Laboratory & Testing, P.C. Laboratory I D: TA09026-002
Description: T-1 SOUTH Matrix: Solid
Date Sampled:01/05/2018 1410 % Solids: 76.5 01/09/2018 2030
Date Received: 01 /09/2018
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2-Bromonaphthalene (fractionation 2)
136 40-140
2-Fluorobiphenyl (fractionation 1)
N
199 40-140
o - Terphenyl (aromatic)
N
151 40-140
MADEP VPH (aliphatics)
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date
Batch
1 VPH
MADEP-VPH-04-1.1
5 01/10/20181357 JJG
61576
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
C5 - C8 Aliphatics
MADEP-VPH- 36
25
mg/kg
1
C9 - C12 Aliphatics
MADEP-VPH- 370
25
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2,5-Dibromotoluene (FID)
N
0.00 70-130
MADEP VPH (aromatics)
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst Prep Date
Batch
1 VPH
MADEP-VPH-04-1.1
5 01/10/20181357 JJG
61575
CAS Analytical
Parameter
Number Method Result Q
LOQ
Units
Run
C9 - C10 Aromatics
MADEP-VPH- 440
8.2
mg/kg
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
2,5-Dibromotoluene (PID)
N
0.00 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
NO = Not detected at or above the LOQ N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 %
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 14 of 38

QC Summary
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 15 of 38

Volatile Organic Compounds by GC/MS - MB
Sample ID: TQ61692-001 Matrix: Solid
Batch: 61692 Prep Method: 5035 High
Analytical Method: 8260B
Parameter
Result
Q Dil
LOQ
Units
Analysis Date
Acetone
ND
1
1000
ug/kg
01/10/2018 1651
Benzene
ND
1
250
ug/kg
01/10/2018 1651
Bromodichloromethane
ND
1
250
ug/kg
01/10/2018 1651
Bromoform
ND
1
250
ug/kg
01/10/2018 1651
Bromomethane (Methyl bromide)
ND
1
250
ug/kg
01/10/2018 1651
2-Butanone (MEK)
ND
1
1000
ug/kg
01/10/2018 1651
Carbon disulfide
ND
1
250
ug/kg
01/10/2018 1651
Carbon tetrachloride
ND
1
250
ug/kg
01/10/2018 1651
Chlorobenzene
ND
1
250
ug/kg
01/10/2018 1651
Chloroethane
ND
1
250
ug/kg
01/10/2018 1651
Chloroform
ND
1
250
ug/kg
01/10/2018 1651
Chloromethane (Methyl chloride)
ND
1
250
ug/kg
01/10/2018 1651
Cyclohexane
ND
1
250
ug/kg
01/10/2018 1651
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
250
ug/kg
01/10/2018 1651
Dibromochloromethane
ND
1
250
ug/kg
01/10/2018 1651
1,2-Dibromoethane (EDB)
ND
1
250
ug/kg
01/10/2018 1651
1,2-Dichlorobenzene
ND
1
250
ug/kg
01/10/2018 1651
1,3-Dichlorobenzene
ND
1
250
ug/kg
01/10/2018 1651
1,4-Dichlorobenzene
ND
1
250
ug/kg
01/10/2018 1651
Dichlorodifluoromethane
ND
1
250
ug/kg
01/10/2018 1651
1,1-Dichloroethane
ND
1
250
ug/kg
01/10/2018 1651
1,2-Dichloroethane
ND
1
250
ug/kg
01/10/2018 1651
1,1-Dichloroethene
ND
1
250
ug/kg
01/10/2018 1651
cis- 1,2-Dichloroethene
ND
1
250
ug/kg
01/10/2018 1651
trans- 1,2-Dichloroethene
ND
1
250
ug/kg
01/10/2018 1651
1,2-Dichloropropane
ND
1
250
ug/kg
01/10/2018 1651
cis- 1,3-Dichloropropene
ND
1
250
ug/kg
01/10/2018 1651
trans- 1,3-Dichloropropene
ND
1
250
ug/kg
01/10/2018 1651
Ethylbenzene
ND
1
250
ug/kg
01/10/2018 1651
2-Hexanone
ND
1
500
ug/kg
01/10/2018 1651
Isopropylbenzene
ND
1
250
ug/kg
01/10/2018 1651
Methyl acetate
ND
1
250
ug/kg
01/10/2018 1651
Methyl tertiary butyl ether (MTBE)
ND
1
250
ug/kg
01/10/2018 1651
4-Methyl-2-pentanone
ND
1
500
ug/kg
01/10/2018 1651
Methylcyclohexane
ND
1
250
ug/kg
01/10/2018 1651
Methylene chloride
ND
1
250
ug/kg
01/10/2018 1651
Styrene
ND
1
250
ug/kg
01/10/2018 1651
1,1,2,2-Tetrachloroethane
ND
1
250
ug/kg
01/10/2018 1651
Tetrachloroethene
ND
1
250
ug/kg
01/10/2018 1651
Toluene
ND
1
250
ug/kg
01/10/2018 1651
1,1,2-Trichloro-1,2,2-Trifluoroethane
ND
1
250
ug/kg
01/10/2018 1651
1,2,4-Trichlorobenzene
ND
1
250
ug/kg
01/10/2018 1651
1,1,1-Trichloroethane
ND
1
250
ug/kg
01/10/2018 1651
1,1,2-Trichloroethane
ND
1
250
ug/kg
01/10/2018 1651
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 16 of 38

Volatile Organic Compounds by GC/MS - MB
Sample ID: TQ61692-001 Matrix: Solid
Batch: 61692 Prep Method: 5035 High
Analytical Method: 8260B
Parameter
Result
Q Dil
LOQ
Units
Analysis Date
Trichloroethene
ND
1
250
ug/kg
01/10/2018 1651
Trichlorofluoromethane
ND
1
250
ug/kg
01/10/2018 1651
Vinyl chloride
ND
1
250
ug/kg
01/10/2018 1651
Xylenes (total)
ND
1
500
ug/kg
01/10/2018 1651
Acceptance
Surrogate Q % Rec Limit
1,2-Dichloroethane-d4 103 53-142
Bromofluorobenzene 93 47-138
Toluene-d8 94 68-124
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 17 of 38

Volatile Organic Compounds by GC/MS - LCS
Sample ID: TQ61692-002 Matrix: Solid
Batch: 61692 Prep Method: 5035 High
Analytical Method: 8260B
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg) Q
Dil
% Rec
Limit
Analysis Date
Acetone
5000
4500
1
90
60-140
01/10/2018 1629
Benzene
2500
2600
1
103
70-130
01/10/2018 1629
Bromodichloromethane
2500
2500
1
101
70-130
01/10/2018 1629
Bromoform
2500
2400
1
96
70-130
01/10/2018 1629
Bromomethane (Methyl bromide)
2500
2200
1
89
70-130
01/10/2018 1629
2-Butanone (MEK)
5000
4700
1
94
60-140
01/10/2018 1629
Carbon disulfide
2500
2800
1
113
70-130
01/10/2018 1629
Carbon tetrachloride
2500
2900
1
115
70-130
01/10/2018 1629
Chlorobenzene
2500
2500
1
102
70-130
01/10/2018 1629
Chloroethane
2500
2400
1
98
70-130
01/10/2018 1629
Chloroform
2500
2700
1
109
70-130
01/10/2018 1629
Chloromethane (Methyl chloride)
2500
2400
1
94
60-140
01/10/2018 1629
Cyclohexane
2500
2900
1
118
70-130
01/10/2018 1629
1,2-Dibromo-3-chloropropane (DBCP)
2500
2100
1
84
70-130
01/10/2018 1629
Dibromochloromethane
2500
2500
1
99
70-130
01/10/2018 1629
1,2-Dibromoethane (EDB)
2500
2500
1
100
70-130
01/10/2018 1629
1,2-Dichlorobenzene
2500
2500
1
99
70-130
01/10/2018 1629
1,3-Dichlorobenzene
2500
2500
1
100
70-130
01/10/2018 1629
1,4-Dichlorobenzene
2500
2500
1
98
70-130
01/10/2018 1629
Dichlorodifluoromethane
2500
2400
1
98
60-140
01/10/2018 1629
1,1-Dichloroethane
2500
2700
1
108
70-130
01/10/2018 1629
1,2-Dichloroethane
2500
2600
1
105
70-130
01/10/2018 1629
1,1-Dichloroethene
2500
2900
1
115
70-130
01/10/2018 1629
cis- 1,2-Dichloroethene
2500
2700
1
108
70-130
01/10/2018 1629
trans- 1,2-Dichloroethene
2500
2700
1
110
70-130
01/10/2018 1629
1,2-Dichloropropane
2500
2500
1
102
70-130
01/10/2018 1629
cis- 1,3-Dichloropropene
2500
2500
1
102
70-130
01/10/2018 1629
trans- 1,3-Dichloropropene
2500
2500
1
99
70-130
01/10/2018 1629
Ethylbenzene
2500
2600
1
103
70-130
01/10/2018 1629
2-Hexanone
5000
4500
1
91
70-130
01/10/2018 1629
Isopropylbenzene
2500
2700
1
107
70-130
01/10/2018 1629
Methyl acetate
2500
2900
1
114
70-130
01/10/2018 1629
Methyl tertiary butyl ether (MTBE)
2500
2700
1
107
70-130
01/10/2018 1629
4-Methyl-2-pentanone
5000
4800
1
95
70-130
01/10/2018 1629
Methylcyclohexane
2500
3000
1
120
70-130
01/10/2018 1629
Methylene chloride
2500
2400
1
95
70-130
01/10/2018 1629
Styrene
2500
2600
1
103
70-130
01/10/2018 1629
1,1,2,2-Tetrachloroethane
2500
2300
1
91
70-130
01/10/2018 1629
Tetrachloroethene
2500
2700
1
107
70-130
01/10/2018 1629
Toluene
2500
2600
1
102
70-130
01/10/2018 1629
1,1,2-Trichloro-1,2,2-Trifluoroethane
2500
3000
1
120
70-130
01/10/2018 1629
1,2,4-Trichlorobenzene
2500
2300
1
92
70-130
01/10/2018 1629
1,1,1-Trichloroethane
2500
2800
1
114
70-130
01/10/2018 1629
1,1,2-Trichloroethane
2500
2300
1
94
70-130
01/10/2018 1629
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 18 of 38

Volatile Organic Compounds by GC/MS - LCS
Sample ID: TQ61692-002
Matrix:
Solid
Batch: 61692
Prep Method:
5035 High
Analytical Method: 8260B
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg) Q
Dil
% Rec
Limit
Analysis Date
Trichloroethene
2500
2700
1
107
70-130
01/10/2018 1629
Trichlorofluoromethane
2500
2900
1
116
70-130
01/10/2018 1629
Vinyl chloride
2500
2600
1
104
70-130
01/10/2018 1629
Xylenes (total)
5000
5000
1
100
70-130
01/10/2018 1629
Acceptance
Surrogate
Q % Rec
Limit
1,2-Dichloroethane-d4 92 53-142
Bromofluorobenzene 91 47-138
Toluene-d8 92 68-124
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 19 of 38

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: TQ61480-001 Matrix: Solid
Batch: 61480 Prep Method: 3546
Analytical Method: 8270D Prep Date: 01/09/2018 1740
Parameter
Result
Q Dil
LOQ
Units
Analysis Date
Acenaphthene
ND
1
13
ug/kg
01/10/2018 1032
Acenaphthylene
ND
1
13
ug/kg
01/10/2018 1032
Acetophenone
ND
1
67
ug/kg
01/10/2018 1032
Anthracene
ND
1
13
ug/kg
01/10/2018 1032
Atrazine
ND
1
67
ug/kg
01/10/2018 1032
Benzaldehyde
ND
1
67
ug/kg
01/10/2018 1032
Benzo(a)anthracene
ND
1
13
ug/kg
01/10/2018 1032
Benzo(a)pyrene
ND
1
13
ug/kg
01/10/2018 1032
Benzo(k)fluoranthene
ND
1
13
ug/kg
01/10/2018 1032
Benzo(g,h,i)perylene
ND
1
13
ug/kg
01/10/2018 1032
Benzo(k)fluoranthene
ND
1
13
ug/kg
01/10/2018 1032
1,1'-Biphenyl
ND
1
67
ug/kg
01/10/2018 1032
4-Bromophenyl phenyl ether
ND
1
67
ug/kg
01/10/2018 1032
Butyl benzyl phthalate
ND
1
67
ug/kg
01/10/2018 1032
Caprolactam
ND
1
67
ug/kg
01/10/2018 1032
Carbazole
ND
1
67
ug/kg
01/10/2018 1032
bis (2-Chloro-1-methylethyl) ether
ND
1
67
ug/kg
01/10/2018 1032
4-Chloro-3-methyl phenol
ND
1
67
ug/kg
01/10/2018 1032
4-Chloroaniline
ND
1
67
ug/kg
01/10/2018 1032
bis(2-Chloroethoxy)methane
ND
1
67
ug/kg
01/10/2018 1032
bis(2-Chloroethyl)ether
ND
1
67
ug/kg
01/10/2018 1032
2-Chloronaphthalene
ND
1
67
ug/kg
01/10/2018 1032
2-Chlorophenol
ND
1
67
ug/kg
01/10/2018 1032
4-Chlorophenyl phenyl ether
ND
1
67
ug/kg
01/10/2018 1032
Chrysene
ND
1
13
ug/kg
01/10/2018 1032
Dibenzo(a,h)anthracene
ND
1
13
ug/kg
01/10/2018 1032
Dibenzofuran
ND
1
67
ug/kg
01/10/2018 1032
3,3'-Dichlorobenzidine
ND
1
67
ug/kg
01/10/2018 1032
2,4-Dichlorophenol
ND
1
67
ug/kg
01/10/2018 1032
Diethylphthalate
ND
1
67
ug/kg
01/10/2018 1032
Dimethyl phthalate
ND
1
67
ug/kg
01/10/2018 1032
2,4-Dimethylphenol
ND
1
67
ug/kg
01/10/2018 1032
Di-n-butyl phthalate
ND
1
67
ug/kg
01/10/2018 1032
4,6-Dinitro-2-methyl phenol
ND
1
330
ug/kg
01/10/2018 1032
2,4-Dinitrophenol
ND
1
330
ug/kg
01/10/2018 1032
2,4-Dinitrotoluene
ND
1
130
ug/kg
01/10/2018 1032
2,6-Dinitrotoluene
ND
1
130
ug/kg
01/10/2018 1032
Di-n-octylphthalate
ND
1
67
ug/kg
01/10/2018 1032
bis(2-Ethylhexyl)phthalate
ND
1
67
ug/kg
01/10/2018 1032
Fluoranthene
ND
1
13
ug/kg
01/10/2018 1032
Fluorene
ND
1
13
ug/kg
01/10/2018 1032
Hexachlorobenzene
ND
1
67
ug/kg
01/10/2018 1032
Hexachlorobutadiene
ND
1
67
ug/kg
01/10/2018 1032
Hexachlorocyclopentadiene
ND
1
330
ug/kg
01/10/2018 1032
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 20 of 38

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: TQ61480-001 Matrix: Solid
Batch: 61480 Prep Method: 3546
Analytical Method: 8270D Prep Date: 01/09/2018 1740
Parameter
Result
Q Dil
LOQ
Units
Analysis Date
Hexachloroethane
ND
1
67
ug/kg
01/10/20181032
Indeno(1,2,3-c,d)pyrene
ND
1
13
ug/kg
01/10/20181032
Isophorone
ND
1
67
ug/kg
01/10/20181032
2-Methyl naphthalene
ND
1
13
ug/kg
01/10/20181032
2-Methylphenol
ND
1
67
ug/kg
01/10/20181032
3+4-Methylphenol
ND
1
130
ug/kg
01/10/20181032
Naphthalene
ND
1
13
ug/kg
01/10/20181032
2-Nitroaniline
ND
1
130
ug/kg
01/10/20181032
3-Nitroaniline
ND
1
130
ug/kg
01/10/20181032
4-Nitroaniline
ND
1
130
ug/kg
01/10/20181032
Nitrobenzene
ND
1
67
ug/kg
01/10/20181032
2-Nitrophenol
ND
1
130
ug/kg
01/10/20181032
4-Nitrophenol
ND
1
330
ug/kg
01/10/20181032
N-Nitrosodi-n-propylamine
ND
1
67
ug/kg
01/10/20181032
N-Nitrosodiphenylamine (Diphenylamine)
ND
1
67
ug/kg
01/10/2018 1032
Pentachlorophenol
ND
1
330
ug/kg
01/10/20181032
Phenanthrene
ND
1
13
ug/kg
01/10/20181032
Phenol
ND
1
67
ug/kg
01/10/20181032
Pyrene
ND
1
13
ug/kg
01/10/20181032
Pyridine
ND
1
67
ug/kg
01/10/20181032
2,4,5-Trichlorophenol
ND
1
67
ug/kg
01/10/20181032
2,4,6-Trichlorophenol
ND
1
67
ug/kg
01/10/20181032
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl
93
24-137
2-Fluorophenol
100
16-136
Nitrobenzene-d5
91
12-144
Phenol-d5
108
26-148
Terphenyl-d14
99
20-127
2,4,6-Tribromophenol
100
27-128
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 21 of 38

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: TQ61480-002 Matrix: Solid
Batch: 61480 Prep Method: 3546
Analytical Method: 8270D Prep Date: 01/09/2018 1740
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg) Q
Dil
% Rec
Limit
Analysis Date
Acenaphthene
670
600
1
89
46-114
01/10/2018 1056
Acenaphthylene
670
600
1
90
44-122
01/10/2018 1056
Acetophenone
670
490
1
73
48-111
01/10/2018 1056
Anthracene
670
620
1
93
50-119
01/10/2018 1056
Atrazine
670
680
1
102
48-116
01/10/2018 1056
Benzaldehyde
670
98
1
15
10-110
01/10/2018 1056
Benzo(a)anthracene
670
600
1
90
47-121
01/10/2018 1056
Benzo(a)pyrene
670
560
1
84
55-134
01/10/2018 1056
Benzo(k)fluoranthene
670
510
1
77
28-139
01/10/2018 1056
Benzo(g,h,i)perylene
670
550
1
83
36-125
01/10/2018 1056
Benzo(k)fluoranthene
670
470
1
71
47-130
01/10/2018 1056
1,1'-Biphenyl
670
630
1
95
49-110
01/10/2018 1056
4-Bromophenyl phenyl ether
670
670
1
100
46-118
01/10/2018 1056
Butyl benzyl phthalate
670
830
1
125
46-128
01/10/2018 1056
Caprolactam
670
740
1
111
43-121
01/10/2018 1056
Carbazole
670
620
1
93
47-128
01/10/2018 1056
bis (2-Chloro-1-methylethyl) ether
670
660
1
99
31-102
01/10/2018 1056
4-Chloro-3-methyl phenol
670
710
1
107
49-118
01/10/2018 1056
4-Chloroaniline
670
410
1
62
17-106
01/10/2018 1056
bis(2-Chloroethoxy)methane
670
590
1
88
39-108
01/10/2018 1056
bis(2-Chloroethyl)ether
670
500
1
76
32-105
01/10/2018 1056
2-Chloronaphthalene
670
540
1
81
31-127
01/10/2018 1056
2-Chlorophenol
670
570
1
86
37-106
01/10/2018 1056
4-Chlorophenyl phenyl ether
670
680
1
102
47-116
01/10/2018 1056
Chrysene
670
600
1
90
45-126
01/10/2018 1056
Dibenzo(a,h)anthracene
670
660
1
99
45-122
01/10/2018 1056
Dibenzofuran
670
670
1
101
45-112
01/10/2018 1056
3,3'-Dichlorobenzidine
670
300 N
1
45
46-113
01/10/2018 1056
2,4-Dichlorophenol
670
610
1
91
41-113
01/10/2018 1056
Diethylphthalate
670
660
1
99
49-123
01/10/2018 1056
Dimethyl phthalate
670
580
1
87
48-120
01/10/2018 1056
2,4-Dimethylphenol
670
690
1
104
33-123
01/10/2018 1056
Di-n-butyl phthalate
670
630
1
94
51-129
01/10/2018 1056
4,6-Dinitro-2-methyl phenol
670
580
1
87
40-130
01/10/2018 1056
2,4-Dinitrophenol
1300
770
1
57
10-113
01/10/2018 1056
2,4-Dinitrotoluene
670
710
1
107
48-124
01/10/2018 1056
2,6-Dinitrotoluene
670
590
1
89
47-125
01/10/2018 1056
Di-n-octylphthalate
670
570
1
85
49-142
01/10/2018 1056
bis(2-Ethylhexyl)phthalate
670
740
1
110
45-128
01/10/2018 1056
Fluoranthene
670
630
1
95
50-123
01/10/2018 1056
Fluorene
670
680
1
102
48-117
01/10/2018 1056
Hexachlorobenzene
670
690
1
103
44-122
01/10/2018 1056
Hexachlorobutadiene
670
590
1
88
33-103
01/10/2018 1056
Hexachlorocyclopentadiene
3300
3200
1
95
18-121
01/10/2018 1056
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 22 of 38

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: TQ61480-002 Matrix: Solid
Batch: 61480 Prep Method: 3546
Analytical Method: 8270D Prep Date: 01/09/2018 1740
Spike
Amount
Result
% Rec
Parameter
(ug/kg)
(ug/kg) Q
Dil
% Rec
Limit
Analysis Date
Hexachloroethane
670
460
1
69
30-96
01/10/20181056
Indeno(1,2,3-c,d)pyrene
670
680
1
102
45-123
01/10/20181056
Isophorone
670
600
1
90
41-113
01/10/20181056
2-Methyl naphthalene
670
700
1
104
40-106
01/10/20181056
2-Methylphenol
670
720 N
1
109
32-107
01/10/20181056
3+4-Methylphenol
670
660
1
99
39-108
01/10/20181056
Naphthalene
670
590
1
89
36-110
01/10/20181056
2-Nitroaniline
670
580
1
87
45-123
01/10/20181056
3-Nitroaniline
670
410
1
61
24-127
01/10/20181056
4-Nitroaniline
670
650
1
98
48-127
01/10/20181056
Nitrobenzene
670
560
1
83
33-114
01/10/20181056
2-Nitrophenol
670
610
1
91
35-108
01/10/20181056
4-Nitrophenol
1300
1100
1
80
18-154
01/10/20181056
N-Nitrosodi-n-propylamine
670
690
1
103
32-115
01/10/20181056
N-Nitrosodiphenylamine (Diphenylamine)
670
640
1
96
53-150
01/10/2018 1056
Pentachlorophenol
1300
1200
1
89
27-138
01/10/20181056
Phenanthrene
670
590
1
88
49-117
01/10/20181056
Phenol
670
640
1
96
36-108
01/10/20181056
Pyrene
670
610
1
91
47-119
01/10/20181056
Pyridine
670
770 N
1
116
10-74
01/10/20181056
2,4,5-Trichlorophenol
670
660
1
99
46-122
01/10/20181056
2,4,6-Trichlorophenol
670
670
1
100
38-115
01/10/20181056
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl
100
24-137
2-Fluorophenol
80
16-136
Nitrobenzene-d5
87
12-144
Phenol-d5 96 26-148
Terphenyl-d14 98 20-127
2,4,6-Tribromophenol 121 27-128
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 23 of 38

MA EPH (aliphatics) - MB
Sample ID: TQ61511-001 Matrix: Solid
Batch: 61511 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 01/10/2018 915
Parameter Result Q Dil LOQ Units Analysis Date
C9 - C18 Aliphatics ND 1 10 mg/kg 01/11/2018 1028
C19 - C36 Aliphatics ND 1 10 mg/kg 01/11/2018 1028
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 88 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 24 of 38

MA EPH (aliphatics) - LCS
Sample ID: TQ61511-002
Matrix: Solid
Batch: 61511
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 01/10/2018 915
Spike
Amount
Result
% Rec
Parameter
(mg/kg)
(mg/kg)
Q Dil % Rec
Limit Analysis Date
C9 - C18 Aliphatics
30
18
1 60
40-140 01/11/2018 1057
C19 - C36 Aliphatics
40
32
1 80
40-140 01/11/2018 1057
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 84 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 25 of 38

MA EPH (aliphatics) - LCSD
Sample ID: TQ61511-003
Matrix: Solid
Batch: 61511
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 01/10/2018 915
Spike
Amount
Result
% Rec
% RPD
Parameter
(mg/kg)
(mg/kg) Q
Dil % Rec % RPD Limit
Limit Analysis Date
C9 - C18 Aliphatics
30
19
1 64 7.1 40-140
25 01/11/2018 1127
C19 - C36 Aliphatics
40
33
1 83 4.0 40-140
25 01/11/2018 1127
Surrogate
Acceptance
Q % Rec Limit
1-Chloro-octadecane (aliphatic) 90 40-140
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 26 of 38

MA EPH (aromatics) - MB
Sample ID: TQ61512-001 Matrix: Solid
Batch: 61512 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 01/10/2018 915
Parameter Result Q Dil LOQ Units Analysis Date
C11 - C22 Aromatics ND 1 10 mg/kg 01/11/2018 1256
Acceptance
Surrogate Q % Rec Limit
2-Bromonaphthalene (fractionation 2) 93 40-140
2-Fluorobiphenyl (fractionation 1) 93 40-140
o - Terphenyl (aromatic) 83 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 27 of 38

MA EPH (aromatics) - LCS
Sample ID: TQ61512-002
Matrix: Solid
Batch: 61512
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 01/10/2018 915
Spike
Amount
Result
% Rec
Parameter
(mg/kg)
(mg/kg) Q
Dil % Rec Limit Analysis Date
C11 - C22 Aromatics
85
69
1 81 40-140 01/11/2018 1325
Surrogate
Q % Rec
Acceptance
Limit
2-Bromonaphthalene (fractionation 2) 93 40-140
2-Fluorobiphenyl (fractionation 1) 97 40-140
o - Terphenyl (aromatic) 85 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 28 of 38

MA EPH (aromatics) - LCSD
Sample ID: TQ61512-003 Matrix: Solid
Batch: 61512 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 01/10/2018 915
Spike
Amount Result % Rec % RPD
Parameter (mg/kg) (mg/kg) Q Dil % Rec % RPD Limit Limit Analysis Date
C11 - C22 Aromatics 85 63 1 74 8.2 40-140 25 01/11/2018 1355
Acceptance
Surrogate Q % Rec Limit
2-Bromonaphthalene (fractionation 2) 82 40-140
2-Fluorobiphenyl (fractionation 1) 88 40-140
o - Terphenyl (aromatic) 78 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 29 of 38

MADEP VPH (aromatics) - MB
Sample ID: TQ61575-001 Matrix: Solid
Batch: 61575 Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Parameter Result Q Dil LOQ Units Analysis Date
C9 - C10 Aromatics ND 1 1.3 mg/kg 01/10/2018 1300
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (PID) 92 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 30 of 38

MADEP VPH (aromatics) - LCS
Sample ID: TQ61575-002 Matrix: Solid
Batch: 61575 Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Spike
Amount Result % Rec
Parameter (mg/kg) (mg/kg) Q Dil % Rec Limit Analysis Date
C9 - C10 Aromatics 1.3 1.4 1 112 70-130 01/10/2018 1203
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (PID) 92 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 31 of 38

MADEP VPH (aromatics) - LCSD
Sample ID: TQ61575-003 Matrix: Solid
Batch: 61575 Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Spike
Amount Result % Rec % RPD
Parameter (mg/kg) (mg/kg) Q Dil % Rec % RPD Limit Limit Analysis Date
C9 - C10 Aromatics 1.3 1.2 1 96 15 70-130 25 01/10/2018 1232
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (PID) 83 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 32 of 38

MADEP VPH (aliphatics) - MB
Sample ID: TQ61576-001 Matrix: Solid
Batch: 61576 Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Parameter Result Q Dil LOQ Units Analysis Date
C5 - C8 Aliphatics ND 1 3.8 mg/kg 01/10/2018 1300
C9 - C12 Aliphatics ND 1 3.8 mg/kg 01/10/2018 1300
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (FID) 88 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 33 of 38

MADEP VPH (aliphatics) - LCS
Sample ID: TQ61576-002
Matrix: Solid
Batch: 61576
Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Spike
Amount
Result
% Rec
Parameter (mg/kg)
(mg/kg) Q
Dil % Rec
Limit Analysis Date
C5 - C8 Aliphatics 7.5
7.9
1 106
70-130 01/10/2018 1203
C9 - C12 Aliphatics 7.5
8.7
1 116
70-130 01/10/2018 1203
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID) 92 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 34 of 38

MADEP VPH (aliphatics) - LCSD
Sample ID: TQ61576-003
Matrix: Solid
Batch: 61576
Prep Method: VPH
Analytical Method: MADEP-VPH-04-1.1
Spike
Amount
Result
% Rec
% RPD
Parameter (mg/kg)
(mg/kg) Q
Dil % Rec % RPD
Limit
Limit Analysis Date
C5 - C8 Aliphatics 7.5
7.1
1 95 10
70-130
25 01/10/2018 1232
C9 - C12 Aliphatics 7.5
8.4
1 111 4.1
70-130
25 01/10/2018 1232
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (FID) 81 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the LOQ
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 35 of 38

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 36 of 38

SHEALY ENVIRONMENTAL SERVICES, INC.
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Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Page 37 of 38

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.ampl4.s Not listed a„ COC-'? _
:rea-size' f'•�"oC 6rrim in diamcLt�r)
c stunple* r-oeived of 9 pli >
s77 samples tree of residua
r'hlSll de5igna LM-R, ere,,.)
in LJIMS?
I-.
Ririe rrewrvawn I R'iLi5a m tGiaipm cu Iur an) NaiuFru bF 3Jr4vI1 —1 V Fd— --- — ••—--••--V--=-,
mplr(3) -wore Teueived inc4)rreC11V prescrw�;.-d Ord were adjusted accordingly
sample receiving m-ilh (I12S #, HN . HC1I NL OH) vsirig Sly 6 _
�rrLple(s) were mceiv::d %�dth bubbles �G mm in diameter.
unples(s) ue a mceived with TRC � 0.5 mgr'L- (ifati'Z1 i.; "r,) and were
9justed acrordiugly in sample receiyin r taWL sodiwn thio5ulfate {Na Sz4 j v'ith hcaly TT]:
C Dilinl ing Vs rater Project Samplc(s) pH verified to bs < 2 Ily Date:
amplu(a) were not received at a pHorti 2 andveere adjusted ncuPrdinglyusing SRi
R barcc,dc 1}113�AS applied by' •t Dato:
;:rL.lue�ts:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
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