23052_Southern Steel_BAR_2020.03.10

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Brownfields Assessment Report Former Southern Steel Facility
3015 Wilkinson Boulevard Charlotte, North Carolina Brownfields Project No. 23052-19-060 H&H Job No. ANR-007
Table of Contents

1.0 Introduction and Background ..................................................................................................... 1
2.0 Brownfields Assessment Activities .............................................................................................. 5
3.0 Soil Assessment Activities ............................................................................................................ 6
3.1 Soil Sampling Methodology ................................................................................................. 6
3.2 Soil Analytical Results ......................................................................................................... 7
4.0 Receptor Survey Activities .......................................................................................................... 8
5.0 Conclusions and Recommendations ......................................................................................... 10

List of Tables

Table 1 Summary of Soil Analytical Data

List of Figures
Figure 1 Site Location Map
Figure 2 Site and Sample Location Map
Figure 3 Receptor Survey Map List of Appendices

Appendix A Boring Logs
Appendix B Laboratory Analytical Reports
Appendix C Brownfields Property Receptor Survey Form

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Brownfields Assessment Report Former Southern Steel Facility
3015 Wilkinson Boulevard Charlotte, North Carolina Brownfields Project No. 23052-19-060 H&H Job No. ANR-007
1.0 Introduction and Background
Hart & Hickman, PC (H&H) has prepared this Brownfields Assessment Report on behalf of
Wilkinson Steel Yard LLC (Prospective Developer or PD) for the industrial property located at
3015 Wilkinson Boulevard in Charlotte, Mecklenburg County, North Carolina (Site). A Site
location map is provided as Figure 1.

The Site consists of one parcel of vacant land (Parcel Identification Number 11701118) that is
approximately 5.2 acres. A Norfolk Southern railroad right-of-way is present along the southern
portion of the Site. The nearby surrounding area of the Site consists of predominantly
industrial/commercial facilities including gas stations, an automotive salvage yard, a school bus
maintenance facility, a railroad maintenance facility, a restaurant, and a liquor store. The Site and
surrounding area are depicted on Figure 2.

The Site consisted of predominantly vacant land with a small structure in the north-central portion
of the Site as of at least 1938. By 1943, an industrial building associated with the former Southern
Steel facility (structural steel fabrication) was present in the western portion of the Site, and several
unpaved paths appear to have been present along the central and eastern portions of the Site. The
Southern Steel facility expanded until the late 1970s or early 1980s. From approximately 2002 until
2009, the Southern Steel facility was utilized for warehousing steel. The Site has consisted of
predominantly vacant land since the Southern Steel facility was demolished in the early 2010s.

H&H conducted Phase II Environmental Site Assessment (ESA) soil and groundwater sampling
activities at the Site in March 2019 to evaluate potential impacts from historical steel fabrication
operations and to provide updated soil and groundwater data for areas where potential impacts

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were previously identified by others in 2011. The results of the Phase II ESA are summarized as
follows:

Soil Assessment
• Lead was detected in samples SB-1 (2-4 ft), SB-3 (1-3 ft), SB-5 (1-3 ft), and SB-8 (2-4 ft)
at concentrations ranging from 826 mg/kg to 1,240 mg/kg, which exceed the North
Carolina Department of Environmental Quality (DEQ) industrial/commercial Preliminary
Soil Remediation Goal (PSRG) of 800 mg/kg and published regional background levels.
Lead was also detected at a concentration above the unrestricted use PSRG and published
regional background levels in one additional soil sample (SB-2) collected at a depth
interval of 1-3 ft below ground surface (bgs). These five soil samples were collected
from the western and central portions of the Site.
• Barium was detected at a concentration above the protection of groundwater PSRG in
one soil sample (SB-9) collected at 1-3 ft bgs in the eastern portion of the Site.
• Volatile organic compounds (VOCs) were not detected above the laboratory method
detection limits (MDLs) in the soil samples.

Groundwater Assessment
• Cobalt and manganese were detected at concentrations above the Site-specific
background concentration and the North Carolina 2L Groundwater Standard (2L
Standard) or Interim Maximum Allowable Concentration (IMAC) in samples TMW-1,
TMW-2, and TMW-3.
• Chromium was detected slightly above the 2L Standard in background sample TMW-4,
but was not detected above the 2L Standard in the non-background wells.
• Trace concentrations of lead were detected in groundwater samples TMW-1 through
TMW-4 at concentrations well below the 2L Standard.
• No VOCs were detected above the MDLs in the groundwater samples.

In September and October 2019, H&H performed soil characterization sampling at the Site to
further evaluate soil conditions in areas that may be disturbed during proposed grading activities

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and for potential soil export and disposal purposes. A summary of the results of the assessment
is provided below.

• Laboratory analytical results indicated the presence of lead in leachate from composite
soil samples B1-A (13.5 mg/L), B1-B (26.0 mg/L), Comp-1 (11.4 mg/L), and Comp-3
(5.8 mg/L) at concentrations above the Environmental Protection Agency (EPA) Toxicity
Characteristic Leaching Procedure (TCLP) regulatory level of 5.0 mg/L.
• Based on the TCLP lead data and recent civil engineering plans which depict the
proposed warehouse buildings, characteristically hazardous soil may be present in an
approximate 0.3-acre area to a depth of at least 4 ft within and adjacent to the west, north,
and east of the proposed Building 1 in the western portion of the Site. Please note that
the soil characterization sampling was generally limited to the areas of proposed
Building 1, Building 2, Building 3, and the area between proposed Buildings 1 and 2.

During soil characterization sampling in October 2019, field screening results of soil in the
southeastern portion of proposed Building 1 showed potential impacts (i.e., elevated
photoionization detector (PID) readings and odor). The results of analysis of a soil sample
collected from that area (soil sample SS-1, 2-4 ft) indicated the presence of chloroform, a
common laboratory contaminant, at an estimated “J-flag” concentration of 0.81 mg/kg, which
exceeds the unrestricted use PSRG of 0.34 mg/kg but is below the industrial/commercial PSRG
of 1.5 mg/kg. The remaining VOC detections were below PSRGs, and no SVOCs were detected
above the MDLs. Metals concentrations in sample SS-1 were generally consistent with
published regional background levels.

The Site received a letter of eligibility for entry into the DEQ Brownfields Program (Brownfields
Project No. 23052-19-060) on October 3, 2019. As noted above, the PD, Wilkinson Steel Yard
LLC, plans to construct three industrial warehouse buildings on the Site.

On January 30, 2020, a kick-off/data gap meeting was held with the PD, DEQ Brownfields
Program personnel, and H&H to discuss Site history, previous environmental assessment
activities at the Site, proposed redevelopment plans, data gaps, and the proposed schedule for

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completing the Brownfields Agreement. During the kick-off meeting, DEQ recommended that
the presence of hexavalent chromium in soil be evaluated at the Site. H&H submitted a
Brownfields Assessment Work Plan (Work Plan) for additional assessment activities, and DEQ
approved the Work Plan in a letter dated February 17, 2020.

Subsequently, on February 19, 2020, Ms. Carolyn Minnich of DEQ requested that the location of
previous soil sample SS-1 (2-4 ft) be re-sampled for VOC/semi-VOC (SVOC) analysis due to high
laboratory dilution factors and field screening results.

In February 2020, H&H conducted soil assessment activities and a sensitive receptor survey in
accordance with the DEQ-approved Work Plan and email correspondence with Ms. Carolyn
Minnich of DEQ. The methods and results of the assessment activities are summarized in the
following sections.

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2.0 Brownfields Assessment Activities
On February 15 and 24, 2020, H&H completed soil assessment activities at the Site to evaluate
the presence of hexavalent chromium in soil at the Site and to assist in the development of an
Environmental Management Plan (EMP) for use during future redevelopment of the Site. The soil
sample locations are depicted on Figure 2.

Prior to conducting assessment activities, H&H contacted North Carolina 811, the public utility
locator, to mark subsurface utilities on the Site. Due to the completion of private utility locating
during multiple prior assessment events at the Site, H&H did not contract a private utility locator
during the February 2020 assessment.

The assessment activities were conducted in general accordance with the DEQ Inactive Hazardous
Sites Branch (IHSB) Guidelines for Assessment and Cleanup dated October 2015 and the most
recent version of the U.S. Environmental Protection Agency (EPA) Region IV Science and
Ecosystem Support (SESD) Field Branches Quality System and Technical Procedures guidance.
The results of the soil assessment are provided in Section 3.0; the receptor survey results are
provided in Section 4.0; and conclusions and recommendations based on the results of the
assessment activities are provided in Section 5.0.

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3.0 Soil Assessment Activities
3.1 Soil Sampling Methodology
H&H advanced six soil borings (SB-10 through SB-15) to a depth of approximately 3 ft bgs
using a decontaminated stainless-steel hand auger. Soil boring locations were near former steel
fabrication areas and proposed warehouse buildings in the western (SB-10 and SB-11), central
(SB-12 and SB-13), and eastern (SB-14 and SB-15) portions of the Site. H&H also advanced
boring SS-1A to approximately 3 ft bgs adjacent to previous sample SS-1, which was collected
in the southeastern portion of proposed Building 1. Boring locations are depicted on Figure 2.

Continuous soil samples were collected from each boring, logged for lithologic description, and
screened for the presence of staining, odors, and volatile organic vapors using a calibrated PID.
Based upon field screening results, no obvious indications of potential soil impacts were
observed. Therefore, one soil sample was collected from each boring at a depth of 1 to 3 ft bgs.
Boring logs including PID readings are provided in Appendix A.

Due to elevated dilution factors for previous soil sample SS-1 (2-4 ft), H&H collected a follow-
up sample from approximately the same location for analysis to further evaluate the presence of
VOCs and SVOCs. Field screening of boring SS-1A indicated the presence of an unusual odor,
potential treated wood fragments, and elevated PID readings at 2-3 ft bgs. Hand auger refusal
was encountered at approximately 3 ft bgs; therefore, follow-up sample SS-1A was collected
from 2-3 ft bgs.

Soil samples selected for laboratory analysis were placed directly into dedicated laboratory-
supplied sample containers; labeled with the sample identification, date, and requested analysis;
and placed in a laboratory-supplied sample cooler with ice. The samples were delivered to Pace
Analytical Laboratory (Pace), a North Carolina-certified laboratory, under standard chain of
custody protocols. Samples SB-10 through SB-15 were analyzed for hexavalent chromium by
EPA Method 7199, and sample SS-1A was analyzed for VOCs by EPA Method 8260D and
SVOCs by EPA Method 8270E.

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For quality assurance purposes, a duplicate soil sample was collected from the SB-12 parent soil
sample and submitted to Pace for analysis of hexavalent chromium by EPA Method 7199.

3.2 Soil Analytical Results

A tabular summary of soil analytical results is presented in Table 1. The laboratory analytical
reports and chain of custody records are provided in Appendix B. The soil analytical results were
compared to the DEQ IHSB unrestricted use and industrial/commercial PSRGs dated
December 2019.

Analytical data indicate that hexavalent chromium was detected in samples SB-10 (3.76 mg/kg),
SB-11 (2.48 mg/kg), SB-13 (3.58 mg/kg), and SB-14 (4.01 mg/kg) at concentrations above the
Unrestricted Use PSRG of 0.31 mg/kg but below the Industrial/Commercial PSRG of 6.5 mg/kg.
Hexavalent chromium was not detected at concentrations above the MDLs in samples SB-12 and
SB-15.

Results of VOC analysis of sample SS-1A (2-3 ft) indicate the presence of naphthalene at a
concentration of 0.981 mg/kg, which is below unrestricted use and industrial/commercial PSRGs
of 4.1 mg/kg and 18 mg/kg, respectively.

Multiple polynuclear aromatic hydrocarbons (PAHs) were detected in sample SS-1A (2-3 ft).
Benzo(a)anthracene (4.05 mg/kg), benzo(a)pyrene (1.76 mg/kg), and benzo(b)fluoranthene
(2.73 mg/kg) were detected above the unrestricted use PSRGs of 1.1 mg/kg, 0.11 mg/kg, and
1.1 mg/kg, respectively. None of the detected PAH concentrations exceed the
industrial/commercial PSRGs.

Analytical data for the duplicate soil sample (SB-Dup-1) are generally consistent with the data for
the parent sample (SB-12). This result indicates good quality control with regard to data
repeatability.

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4.0 Receptor Survey Activities
On February 24, 2020, H&H performed receptor survey activities at the Site and in the nearby area.
The receptor survey included a pedestrian and vehicular survey to obtain information about land
use, water supply, basements, underground utilities, drains, and surface water bodies located within
a 1,500-ft radius of the Site in accordance with the DEQ-approved Work Plan. H&H also utilized
the online Mecklenburg County Groundwater & Wastewater Services (GWS) Well Information
System to check for water supply wells located within a 1,500-ft radius of the Site. In addition,
H&H identified land use, zoning, and underground utilities using other Mecklenburg County online
resources. The Brownfields Property Receptor Survey Form is included as Appendix C, and a
Receptor Survey Map is provided as Figure 3. The results of the receptor survey are summarized
below.

Zoning
The subject Site and nearby surrounding properties are zoned “general industrial” (I-2).

Municipal Water Availability
Municipal water supplied by Charlotte Water is available to the Site and surrounding area. H&H
did not identify sources of public drinking water within 1,500-ft of the Site based on the DEQ
Source Water Assessment Program’s geographic information system (GIS) map. The City of
Charlotte and Mecklenburg County obtain their water from Lake Norman and Mountain Island
Lake. Mountain Island Lake is the closest drinking water source and is located approximately 8.5
miles northwest of the Site. Additionally, H&H observed municipal water meters for the Site and
surrounding properties.

Water Supply Wells
H&H conducted a pedestrian and vehicular survey of properties within a 1,500-ft radius of the Site
to identify potential water supply wells. H&H also utilized the online Mecklenburg County GWS
Well Information System to identify potential water supply wells located within a 1,500-ft radius of
the Site. The nearest active water supply wells that were identified during the receptor survey are
private industrial process wells located approximately 725 ft and 1,000 ft southwest and

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topographically cross-gradient of the Site at the Southern Metals facility (2200 Donald Ross Road).
The identified water supply well locations are depicted on Figure 3.

Surface Water Bodies
An unnamed tributary of Irwin Creek is located in the southwestern portion of the Site. Based on
the DEQ classification system, Irwin Creek is classified as a Class C surface water body. A Class C
surface water body is defined as “waters protected for uses such as secondary recreation, fishing,
wildlife, fish consumption, aquatic life including propagation, survival and maintenance of
biological integrity, and agriculture. Secondary recreation includes wading, boating, and other uses
involving human body contact with water where such activities take place in an infrequent,
unorganized, or incidental manner.”

Subsurface Structures
H&H conducted a visual reconnaissance in the Site area to identify potential subsurface structures
within 1,000 ft of the subject Site. H&H observed evidence of subsurface utilities, including
sanitary sewer, storm sewer, municipal water, electricity, and natural gas, on and adjacent to the
subject Site. Existing utility lines are generally located along the northern and western Site
boundaries and along access roads to the north and northwest of the Site. H&H did not observe any
basements during receptor survey activities.

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5.0 Conclusions and Recommendations
H&H has completed Brownfields assessment activities on the Southern Steel Brownfields Property
located at 3015 Wilkinson Boulevard located in Charlotte, Mecklenburg County, North Carolina
(Brownfields Project No. 23052-19-060). The assessment activities were conducted in
accordance with the DEQ-approved Work Plan and included a receptor survey and soil sampling
to evaluate potential environmental risks associated with redevelopment of the Site. A summary
of the assessment results is provided below.

Receptor Survey
H&H conducted a Brownfields receptor survey for the Site and nearby area. The results of the
receptor survey indicate that municipal water is available to the Site and area within a 1,500-ft
radius of the Site. No sources of public drinking water are within 1,500 ft of the Site. H&H
identified two active industrial process/fire suppression wells located approximately 725 ft and
1,000 ft southwest and topographically cross-gradient of the Site. An unnamed tributary of Irwin
Creek (Class C surface water body) is located in the southwestern portion of the Site. H&H
observed evidence of subsurface utilities, including sanitary sewer, storm sewer, municipal
water, electricity, and natural gas, on the Site and nearby properties. H&H did not identify
basements within a 1,500-ft radius of the Site.

Soil
H&H collected six soil samples for laboratory analysis from three soil borings to evaluate the
presence of hexavalent chromium in shallow soil (1-3 ft) at the Site. Analytical data indicate that
hexavalent chromium was detected in samples SB-10 (3.76 mg/kg), SB-11 (2.48 mg/kg), SB-13
(3.58 mg/kg), and SB-14 (4.01 mg/kg) at concentrations above the unrestricted use PSRG of
0.31 mg/kg but below the industrial/commercial PSRG of 6.5 mg/kg.

During soil characterization sampling in October 2019, field screening results for soil in the
southeastern portion of proposed Building 1 showed potential impacts (i.e., elevated PID
readings and odor). The results of analysis of a soil sample collected from that area (soil sample
SS-1, 2-4 ft) indicated the presence of chloroform, a common laboratory contaminant, at an

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estimated “J-flag” concentration of 0.81 mg/kg, which exceeds the unrestricted use PSRG of
0.34 mg/kg but is below the industrial/commercial PSRG of 1.5 mg/kg. No obvious SVOC or
metals impacts were identified.

Due to elevated laboratory dilution factors and at the request of DEQ, H&H collected a follow-
up soil sample (SS-1A) from the approximate location of sample SS-1. Results of VOC analysis
of sample SS-1A (2-3 ft) indicate the presence of naphthalene at a concentration of 0.981 mg/kg,
which is below unrestricted use and industrial/commercial PSRGs of 4.1 mg/kg and 18 mg/kg,
respectively. The PAHs benzo(a)anthracene (4.05 mg/kg), benzo(a)pyrene (1.76 mg/kg), and
benzo(b)fluoranthene (2.73 mg/kg) were detected above the unrestricted use PSRGs of
1.1 mg/kg, 0.11 mg/kg, and 1.1 mg/kg, respectively. None of the detected PAH concentrations
exceed the industrial/commercial PSRGs.

Table 1
Summary of Soil Analytical Data
Former Southern Steel Facility
Brownfields Project No. 23052-19-060
3015 Wilkinson Boulevard
Charlotte, North Carolina
H&H Job No. ANR-007
Area of Potential Concern
Sample ID SB-10 SB-11 SB-12 SB-Dup-1 SB-13 SB-14 SB-15 SS-1 SS-1A
Date 2/15/2020 2/15/2020 2/15/2020 2/16/2020 2/15/2020 2/15/2020 2/15/2020 10/30/2019 2/24/2020
Depth (ft bgs)1-3 1-3 1-3 1-4 1-3 1-3 1-3 2-4 2-3
VOCs (8260)
n-Butylbenzene NA NA NA NA NA NA NA 3.7 <0.095 780 12,000 ----
sec-Butylbenzene NA NA NA NA NA NA NA 0.88 J <0.0714 1,600 23,000 ----
Chloroform NA NA NA NA NA NA NA 0.81J <0.0357 0.34 1.5 ----
Ethylbenzene NA NA NA NA NA NA NA 1.6 <0.0357 6.1 27 ----
p-Isopropyltoluene NA NA NA NA NA NA NA 34.3 <0.0812 NE NE ----
Methylene chloride NA NA NA NA NA NA NA 2.2 J <0.199 58 650 ----
Naphthalene NA NA NA NA NA NA NA <0.82 0.981 4.1 18 ----1,2,4-Trimethylbenzene NA NA NA NA NA NA NA 0.46 J <0.0657 63 370 ----
SVOCs (8270)Acenaphthene NA NA NA NA NA NA NA <0.98 4.78 720 9,000 ----Acenaphthylene NA NA NA NA NA NA NA <0.9 0.642 720 9,000 ----Anthracene NA NA NA NA NA NA NA <0.99 7.9 3,600 45,000 ----Benzo(a)anthracene NA NA NA NA NA NA NA <1.2 4.05 1.1 21 ----Benzo(a)pyrene NA NA NA NA NA NA NA <1.6 1.76 0.11 2.1 ----Benzo(b)fluoranthene NA NA NA NA NA NA NA <1.5 2.73 1.1 21 ----Benzo(g,h,i)perylene NA NA NA NA NA NA NA <1.5 0.698 NE NE ----Benzo(k)fluoranthene NA NA NA NA NA NA NA <1.6 1.08 11 210 ----Chrysene NA NA NA NA NA NA NA <1.1 3.76 110 2,100 ----Dibenzofuran NA NA NA NA NA NA NA <0.95 2.84 15 210 ----Fluoranthene NA NA NA NA NA NA NA <1.1 14.1 480 6,000 ----Fluorene NA NA NA NA NA NA NA <1.0 5.86 480 6,000 ----Indeno(1,2,3-cd)pyrene NA NA NA NA NA NA NA <1.7 0.703 1.1 21 ----1-Methylnaphthalene NA NA NA NA NA NA NA <1.0 0.924 18 73 ----2-Methylnaphthalene NA NA NA NA NA NA NA <0.97 1.35 48 600 ----Naphthalene NA NA NA NA NA NA NA <0.91 0.702 4.1 18 ----Phenanthrene NA NA NA NA NA NA NA <0.96 18.1 NE NE ----Pyrene NA NA NA NA NA NA NA <0.96 9.6 360 4,500 ----
Metals (6010/6020/7471/7196)
Arsenic NA NA NA NA NA NA NA 3.37 NA 0.68 3.0 1.0 - 18 4.8
Barium NA NA NA NA NA NA NA 86.0 NA 3,100 47,000 50 - 1,000 356
Beryllium NA NA NA NA NA NA NA NA NA 31 470 ND - 2.0 0.11
Cadmium NA NA NA NA NA NA NA 0.168 J NA 14 200 1.0 - 10 (3)4.3 (3)
Chromium (Total)NA NA NA NA NA NA NA 33.4 NA 0.31 6.5 7.0 - 300 65
Hexavalent chromium 3.76 2.48 <0.342 <0.318 3.58 4.01 <0.331 NA NA 0.31 6.5 NE NE
Cobalt NA NA NA NA NA NA NA NA NA 4.7 70 ND - 50 14.2
Lead NA NA NA NA NA NA NA 230 NA 400 800 ND - 50 16
Manganese NA NA NA NA NA NA NA NA NA 2,200 32,000 <8.0 - 3,394 (3)594 (3)
Mercury NA NA NA NA NA NA NA 0.034 NA 2.3 9.7 0.03 - 0.52 0.121NickelNANANANANANANANANA3104,700 ND - 150 23SeleniumNANANANANANANA0.514 J NA 78 1,200 <0.1 - 0.8 0.42
Silver NA NA NA NA NA NA NA <0.171 NA 78 1,200 ND - 5.0 (3)NE
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Preliminary Soil Remediation Goals (PSRGs) (December 2019).
2) Range and mean values of background metals for North Carolina soils taken from Elements in North American Soils by Dragun and Chekiri, 2005.3) Background values for North Carolina soils are not specified; therefore, background values for soils of the southeastern United States are shown.
Soil concentrations are reported in milligrams per kilogram (mg/kg).
Laboratory analytical methods are shown in parentheses.
Underlined values exceed the Residential PSRG and average published background levels for North Carolina soil.
J = estimated concentration between the laboratory method detection limit and the laboratory reporting limit
VOC = volatile organic compounds; SVOCs = semi-volatile organic compounds;
RCRA = Resource Conservation and Recovery Act; NA = not analyzed; NE = Not Established
Published Background Levels
for North Carolina Soil
Residential
PSRGs (1)
Industrial/
Commercial
PSRGs (1)
Range
Background
Soil (2)
Mean
Background
Soil (2)
Screening CriteriaSoutheastern Portion of
Proposed Building 1
Northern Portion of
the Site Central Portion of the Site Eastern Portion of the
Site
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3/5/2020
Table 1
Hart & Hickman, PC
0 2000 4000
APPROXIMATE
SCALE IN FEETN
U.S.G.S. QUADRANGLE MAP
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC)
CHARLOTTE WEST, NORTH CAROLINA 1996
TITLE
PROJECT
SITE LOCATION MAP
FORMER SOUTHERN STEEL FACILITY3015 WILKINSON BOULEVARDCHARLOTTE, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE:
4-25-19 0
1WHI-001
SITE
ANDREW JACKSON HIGHWAYASHLEY ROADASHLEY ROADASHLEY ROADASHLEY ROAD
WILKINSON BOULEVARD WEYLAND AVENUESB-10
SB-11
SB-12
SB-13
SB-14
SB-15
SS-1/
SS1A
REVISION NO. 0
JOB NO. ANR-007
DATE: 3-9-2020
FIGURE NO. 2
FORMER SOUTHERN STEEL FACILITY
3015 WILKINSON BOULEVARD
CHARLOTTE, NORTH CAROLINA
SITE AND SAMPLE LOCATION MAP
LEGEND
SITE PROPERTY BOUNDARY
RAILROAD TRACKS
SOIL BORING LOCATION
PROPOSED BUILDING FOOTPRINT
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
NOTES
1.BASE MAP OBTAINED FROM MECKLENBURG
COUNTY GIS.
2.SOIL SAMPLES SB-10 THROUGH SB-15
COLLECTED BY H&H ON 2/15/2020.
3.SOIL SAMPLES SS-1 AND SS-1A COLLECTED BYH&H ON 10/3/19 AND 2/24/20, RESPECTIVELY. EASTWAY WRECKER SERVICE
(2801 WILKINSON BLVD)
PARKER VETERINARY HOSPITAL
(2820 WILKINSON BLVD)
BBQ KING
(2800 WILKINSON BLVD)
QUIKTRIP
(3025 WILKINSON BLVD)
CHARLOTTE MECKLENBURG SCHOOLS
BUS MAINTENANCE FACILITY
(3101 WILKINSON BLVD)
ABC STORE
(2915 WILKINSON BLVD)
PROPOSED
BUILDING
NO.1
PROPOSED
BUILDING
NO.2
PROPOSED
BUILDING
NO.3
S:\AAA-Master Projects\Roby Realty (ANR)\ANR-007 - 3015 Wilkinson Blvd (former Southern Steel)\Brownfields Assessment\Figures\Site and Sample Location Map.dwg, FIG 2 SITE MAP, 3/10/2020 1:40:18 PM, jdemmerNORFOLK SOUTHERN RAILROAD MAINTENANCE FACILITY(1824 PARKER DRIVE)
REVISION NO. 0
JOB NO. ANR.007
DATE: 3-9-2020
FIGURE NO. 3
FORMER SOUTHERN STEEL FACILITY
3015 WILKINSON BLVD CHARLOTTE,
NORTH CAROLINA
RECEPTOR SURVEY MAP
LEGEND
2923 South Tryon Street-Suite 100
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(f)
License # C-1269 / #C-245 Geology
INSERT A (NTS)
SEE INSERT A WILKINSON BOULEVARD
PARKER DRASHLEY RDDONALD ROSS RDWEYLAND AVESITE PROPERTY BOUNDARY
INDUSTRIAL PROCESS/FIRE
SUPPRESSION WATER
SUPPLY WELL LOCATION
ELECTRICAL LINE
NATURAL GAS LINE
SANITARY SEWER LINE
STORM SEWER LINE
STREAM (PARTIALLY
CULVERTED)
1,500 FT RADIUS
CLOSEST RESIDENTIAL
PROPERTY
WILKINSON BOULEVARD
S:\AAA-Master Projects\Roby Realty (ANR)\ANR-007 - 3015 Wilkinson Blvd (former Southern Steel)\Brownfields Assessment\Figures\Receptor Survey Map.dwg, FIG 3, 3/10/2020 3:24:14 PM, jdemmer

Appendix A Boring Logs
generated using GroundLogs.online
Client:
Project:
Address:
Wilkinson Steel Yard, LLC
ANR-007
3015 Wilkinson Blvd., Charlotte, NC
BORING LOG
Boring No.
Page:
SB-10
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
02/15/2020
Hart & Hickman
Hand Auger
Sean Horgan
Sean Horgan
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
3.0
2.50
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
(0') SILT (ML); few fine-coarse gravel,trace clay, stiff, moist, reddish-brown
(1') Lean CLAY (CL); few fine-medium sand, some silt, medium plasticity, stiff, moist,
reddish-brown
(3') Boring terminated
10.9
11.2
0
1
2
3
4
5
SB-10(1-3')
02/15/2020
generated using GroundLogs.online
Client:
Project:
Address:
Wilkinson Steel Yard, LLC
ANR-007
3015 Wilkinson Blvd., Charlotte, NC
BORING LOG
Boring No.
Page:
SB-11
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
02/15/2020
02/15/2020
Hart & Hickman
Hand Auger
Sean Horgan
Sean Horgan
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
3.0
2.50
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
(0') Sandy SILT (ML); trace fine-coarse gravel and clay, stiff, moist, brown,
some wood debris
(2') As Above: some coarse gravel
(3') Boring terminated
10.2
3.2
0
1
2
3
4
5
SB-11(1-3')
generated using GroundLogs.online
Client:
Project:
Address:
Wilkinson Steel Yard, LLC
ANR-007
3015 Wilkinson Blvd., Charlotte, NC
BORING LOG
Boring No.
Page:
SB-12
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
02/15/2020
02/15/2020
Hart & Hickman
Hand Auger
Sean Horgan
Sean Horgan
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
3.0
2.50
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
(0') Clayey SAND with gravel (SC); dense, moist, brown
(1') Sandy lean CLAY (CL) with gravel; trace silt, medium plasticity, stiff, moist,
light brown
(1.5') Lean CLAY (CL); trace fine-coarse gravel and silt, medium plasticity, stiff,
moist, gray
(3') Boring terminated
4.7
7.4
0
1
2
3
4
5
SB-12(1-3')
generated using GroundLogs.online
Client:
Project:
Address:
Wilkinson Steel Yard, LLC
ANR-007
3015 Wilkinson Blvd., Charlotte, NC
BORING LOG
Boring No.
Page:
SB-13
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
02/15/2020
02/15/2020
Hart & Hickman
Hand Auger
Sean Horgan
Sean Horgan
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
3.0
2.50
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
(0') SILT (ML); some clay, medium stiff, wet, dark reddish-brown
(1') SILT (ML); trace fine-coarse gravel and clay, stiff, moist, dark brown, wood debris
(3') Boring terminated
11.8
7.0
0
1
2
3
4
5
SB-13(1-3')
generated using GroundLogs.online
Client:
Project:
Address:
Wilkinson Steel Yard, LLC
ANR-007
3015 Wilkinson Blvd., Charlotte, NC
BORING LOG
Boring No.
Page:
SB-14
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
02/15/2020
Hart & Hickman
Hand Auger
Sean Horgan
Sean Horgan
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
3.0
2.50
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
(0') Sandy SILT (ML); trace fine-coarse gravel, medium stiff, wet, dark brown
(1') SILT (ML); trace fine-coarse gravel and clay, stiff, wet, brown
(3') Boring terminated
8.0
4.3
0
1
2
3
4
5
SB-14(1-3')
02/15/2020
generated using GroundLogs.online
Client:
Project:
Address:
Wilkinson Steel Yard, LLC
ANR-007
3015 Wilkinson Blvd., Charlotte, NC
BORING LOG
Boring No.
Page:
SB-15
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
02/15/2020
Hart & Hickman
Hand Auger
Sean Horgan
Sean Horgan
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
3.0
2.50
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
(0') Silty SAND (SM); trace fine gravel, medium dense, moist, brown
(1') Sandy SILT (ML); medium stiff, moist, light yellowish-brown
(2.5') SILT (ML); trace clay, stiff, moist, light brown
(3') Boring terminated
11.4
8.5
0
1
2
3
4
5
SB-15(1-3')
02/15/2020
generated using GroundLogs.online
Client:
Project:
Address:
Wilkinson Steel Yard, LLC
ANR-007
3015 Wilkinson Blvd., Charlotte, NC
BORING LOG
Boring No.
Page:
SS-1A
1 of 1
Drilling Start Date:
Drilling End Date:
Drilling Company:
Drilling Method:
Drilling Equipment:
Driller:
Logged By:
2/24/20
2/24/20
Hart & Hickman
Hand Auger
Sean Horgan
Sean Horgan
Boring Depth (ft):
Boring Diameter (in):
Sampling Method(s):
DTW During Drilling (ft):
DTW After Drilling (ft):
Ground Surface Elev. (ft):
Location (X,Y):
3.5
2.50
DEPTH (ft)LITHOLOGYWATER LEVELBORINGCOMPLETIONCOLLECT
Sample TypeTimeBlow CountsRecovery (ft)SOIL/ROCK VISUAL DESCRIPTION
MEASURE
PID (ppm)Lab SampleDEPTH (ft)0
1
2
3
4
5
(0') Sandy SILT (ML); some coarse gravel, medium stiff, moist, yellowish-brown
(1') Sandy SILT (ML); some coarse gravel, stiff, moist, dark reddish-brown
(2') As Above: some dark wood debris present
(3') As Above: No wood
(3.5') Boring terminated
1.6
1.0
68.5
2.3
0
1
2
3
4
5
SS-1A(2-3')

Appendix B Laboratory Analytical Reports
#=CL#
February 28, 2020
LIMS USE: FR - BO CAPPLEMAN
LIMS OBJECT ID: 92466140
92466140
Project:
Pace Project No.:
RE:
Bo Cappleman
Hart & Hickman
2923 South Tryon Street
Charlotte, NC 28203
ANR.007
Dear Bo Cappleman:
Enclosed are the analytical results for sample(s) received by the laboratory on February 20, 2020.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 19
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92466140
ANR.007
Pace Analytical Services National
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 19
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92466140
ANR.007
Lab ID Sample ID Matrix Date Collected Date Received
92466140001 SB-10 (1-3)Solid 02/15/20 00:00 02/20/20 11:38
92466140002 SB-11 (1-3)Solid 02/15/20 00:00 02/20/20 11:38
92466140003 SB-12 (1-3)Solid 02/15/20 00:00 02/20/20 11:38
92466140004 SB-13 (1-3)Solid 02/15/20 00:00 02/20/20 11:38
92466140005 SB-14 (1-3)Solid 02/15/20 00:00 02/20/20 11:38
92466140006 SB-15 (1-3)Solid 02/15/20 00:00 02/20/20 11:38
92466140007 SB-Dup-1 Solid 02/15/20 00:00 02/20/20 11:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 19
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92466140
ANR.007
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92466140001 SB-10 (1-3)SM 2540G 1 PANKDW
EPA 7199 1 PANDGR
92466140002 SB-11 (1-3)SM 2540G 1 PANKDW
EPA 7199 1 PANDGR
92466140003 SB-12 (1-3)SM 2540G 1 PANKDW
EPA 7199 1 PANDGR
92466140004 SB-13 (1-3)SM 2540G 1 PANKDW
EPA 7199 1 PANDGR
92466140005 SB-14 (1-3)SM 2540G 1 PANKDW
EPA 7199 1 PANDGR
92466140006 SB-15 (1-3)SM 2540G 1 PANKBC
EPA 7199 1 PANDGR
92466140007 SB-Dup-1 SM 2540G 1 PANKBC
EPA 7199 1 PANDGR
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 4 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92466140
ANR.007
Sample:SB-10 (1-3)Lab ID:92466140001 Collected:02/15/20 00:00 Received:02/20/20 11:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 78.5 %02/24/20 11:2302/24/20 11:111
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent 3.76 mg/kg 02/24/20 00:02 18540-29-902/23/20 17:001.27 0.325 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2020 08:25 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 5 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92466140
ANR.007
Sample:SB-11 (1-3)Lab ID:92466140002 Collected:02/15/20 00:00 Received:02/20/20 11:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 80.7 %02/24/20 11:2302/24/20 11:111
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent 2.48 mg/kg 02/24/20 01:15 18540-29-902/23/20 17:001.24 0.316 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2020 08:25 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92466140
ANR.007
Sample:SB-12 (1-3)Lab ID:92466140003 Collected:02/15/20 00:00 Received:02/20/20 11:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 74.5 %02/24/20 11:2302/24/20 11:111
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent ND mg/kg 02/24/20 01:23 18540-29-902/23/20 17:001.34 0.342 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2020 08:25 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92466140
ANR.007
Sample:SB-13 (1-3)Lab ID:92466140004 Collected:02/15/20 00:00 Received:02/20/20 11:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 78.3 %02/24/20 11:2302/24/20 11:111
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent 3.58 mg/kg 02/24/20 01:28 18540-29-902/23/20 17:001.28 0.326 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2020 08:25 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92466140
ANR.007
Sample:SB-14 (1-3)Lab ID:92466140005 Collected:02/15/20 00:00 Received:02/20/20 11:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 75.2 %02/24/20 11:2302/24/20 11:111
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent 4.01 mg/kg 02/24/20 01:33 18540-29-902/23/20 17:001.33 0.339 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2020 08:25 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92466140
ANR.007
Sample:SB-15 (1-3)Lab ID:92466140006 Collected:02/15/20 00:00 Received:02/20/20 11:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 76.9 %02/27/20 11:5302/27/20 11:421
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent ND mg/kg 02/24/20 01:38 18540-29-902/23/20 17:001.30 0.331 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2020 08:25 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 19
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92466140
ANR.007
Sample:SB-Dup-1 Lab ID:92466140007 Collected:02/15/20 00:00 Received:02/20/20 11:38 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 80.3 %02/27/20 11:5302/27/20 11:421
Analytical Method: EPA 7199 Preparation Method: 3060AWet Chemistry 7199
Chromium, Hexavalent ND mg/kg 02/24/20 01:43 18540-29-902/23/20 17:001.25 0.318 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2020 08:25 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92466140
ANR.007
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1432872
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Associated Lab Samples:92466140001, 92466140002, 92466140003, 92466140004, 92466140005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3502704-1
Associated Lab Samples:92466140001, 92466140002, 92466140003, 92466140004, 92466140005
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 02/24/20 11:23
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3502704-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1192048-21
R3502704-3SAMPLE DUPLICATE:
Total Solids %97.8 0.345 1097.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/28/2020 08:25 AM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92466140
ANR.007
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1432875
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Associated Lab Samples:92466140006, 92466140007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3503662-1
Associated Lab Samples:92466140006, 92466140007
Matrix:Solid
AnalyzedMDL
Total Solids %0.00100 02/27/20 11:53
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3503662-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1192113-03
R3503662-3SAMPLE DUPLICATE:
Total Solids %89.0 0.357 1089.3
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/28/2020 08:25 AM
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Page 13 of 19
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92466140
ANR.007
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1432503
3060A
EPA 7199
Wet Chemistry 7199
Associated Lab Samples:92466140001, 92466140002, 92466140003, 92466140004, 92466140005, 92466140006, 92466140007
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:R3502308-1
Associated Lab Samples:92466140001, 92466140002, 92466140003, 92466140004, 92466140005, 92466140006, 92466140007
Matrix:Solid
AnalyzedMDL
Chromium, Hexavalent mg/kg ND 1.00 02/23/20 21:080.255
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3502308-2LABORATORY CONTROL SAMPLE:
LCSSpike
Chromium, Hexavalent mg/kg 10.010.0 100 80.0-120
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3502308-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92466140001
R3502308-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Chromium, Hexavalent mg/kg 25.5 77.5 75.0-12589.9 12.7 2025.53.76 23.5 26.7
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
R3502308-6MATRIX SPIKE SAMPLE:
MSSpike
Result
92466140001
Chromium, Hexavalent mg/kg 812852 95.4 75.0-1253.76
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
L1191715-01
R3502308-3SAMPLE DUPLICATE:
Chromium, Hexavalent mg/kg ND 0.00 20ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/28/2020 08:25 AM
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Page 14 of 19
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92466140
ANR.007
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical NationalPAN
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/28/2020 08:25 AM
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Page 15 of 19
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92466140
ANR.007
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92466140001 1432872 1432872SB-10 (1-3)SM 2540 G SM 2540G
92466140002 1432872 1432872SB-11 (1-3)SM 2540 G SM 2540G
92466140003 1432872 1432872SB-12 (1-3)SM 2540 G SM 2540G
92466140004 1432872 1432872SB-13 (1-3)SM 2540 G SM 2540G
92466140005 1432872 1432872SB-14 (1-3)SM 2540 G SM 2540G
92466140006 1432875 1432875SB-15 (1-3)SM 2540 G SM 2540G
92466140007 1432875 1432875SB-Dup-1 SM 2540 G SM 2540G
92466140001 1432503 1432503SB-10 (1-3)3060A EPA 7199
92466140002 1432503 1432503SB-11 (1-3)3060A EPA 7199
92466140003 1432503 1432503SB-12 (1-3)3060A EPA 7199
92466140004 1432503 1432503SB-13 (1-3)3060A EPA 7199
92466140005 1432503 1432503SB-14 (1-3)3060A EPA 7199
92466140006 1432503 1432503SB-15 (1-3)3060A EPA 7199
92466140007 1432503 1432503SB-Dup-1 3060A EPA 7199
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/28/2020 08:25 AM
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Page 16 of 19
Page 17 of 19
Page 18 of 19
Page 19 of 19
#=CL#
February 27, 2020
LIMS USE: FR - BO CAPPLEMAN
LIMS OBJECT ID: 92466478
92466478
Project:
Pace Project No.:
RE:
Bo Cappleman
Hart & Hickman
2923 South Tryon Street
Charlotte, NC 28203
ANR.007
Dear Bo Cappleman:
Enclosed are the analytical results for sample(s) received by the laboratory on February 24, 2020.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 1 of 25
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92466478
ANR.007
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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Page 2 of 25
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92466478
ANR.007
Lab ID Sample ID Matrix Date Collected Date Received
92466478001 SS-1A (2-3)Solid 02/24/20 11:00 02/24/20 12:17
REPORT OF LABORATORY ANALYSIS
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Page 3 of 25
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92466478
ANR.007
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92466478001 SS-1A (2-3)EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CDLK
ASTM D2974-87 1 PASI-CKDF
REPORT OF LABORATORY ANALYSIS
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Page 4 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92466478
ANR.007
Sample:SS-1A (2-3)Lab ID:92466478001 Collected:02/24/20 11:00 Received:02/24/20 12:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene 4780 ug/kg 02/26/20 22:03 83-32-902/25/20 11:014050104010
Acenaphthylene 642 ug/kg 02/26/20 13:56 208-96-802/25/20 11:0140595.7 1
Aniline ND ug/kg 02/26/20 13:56 62-53-302/25/20 11:0140590.8 1
Anthracene 7900 ug/kg 02/26/20 22:03 120-12-702/25/20 11:014050105010
Benzo(a)anthracene 4050 ug/kg 02/26/20 13:56 56-55-302/25/20 11:014051291
Benzo(a)pyrene 1760 ug/kg 02/26/20 13:56 50-32-802/25/20 11:014051751
Benzo(b)fluoranthene 2730 ug/kg 02/26/20 13:56 205-99-202/25/20 11:014051631
Benzo(g,h,i)perylene 698 ug/kg 02/26/20 13:56 191-24-202/25/20 11:014051581
Benzo(k)fluoranthene 1080 ug/kg 02/26/20 13:56 207-08-902/25/20 11:014051701
Benzoic Acid ND ug/kg 02/26/20 13:56 65-85-002/25/20 11:0120204361
Benzyl alcohol ND ug/kg 02/26/20 13:56 100-51-602/25/20 11:018092151
4-Bromophenylphenyl ether ND ug/kg 02/26/20 13:56 101-55-302/25/20 11:014051061
Butylbenzylphthalate ND ug/kg 02/26/20 13:56 85-68-702/25/20 11:014051081
4-Chloro-3-methylphenol ND ug/kg 02/26/20 13:56 59-50-702/25/20 11:018092461
4-Chloroaniline ND ug/kg 02/26/20 13:56 106-47-802/25/20 11:018092481
bis(2-Chloroethoxy)methane ND ug/kg 02/26/20 13:56 111-91-102/25/20 11:014051081
bis(2-Chloroethyl) ether ND ug/kg 02/26/20 13:56 111-44-402/25/20 11:0140585.9 1
2-Chloronaphthalene ND ug/kg 02/26/20 13:56 91-58-702/25/20 11:0140590.1 1
2-Chlorophenol ND ug/kg 02/26/20 13:56 95-57-802/25/20 11:0140594.1 1
4-Chlorophenylphenyl ether ND ug/kg 02/26/20 13:56 7005-72-302/25/20 11:014051051
Chrysene 3760 ug/kg 02/26/20 13:56 218-01-902/25/20 11:014051171
Dibenz(a,h)anthracene ND ug/kg 02/26/20 13:56 53-70-302/25/20 11:014051621
Dibenzofuran 2840 ug/kg 02/26/20 13:56 132-64-902/25/20 11:014051011
1,2-Dichlorobenzene ND ug/kg 02/26/20 13:56 95-50-102/25/20 11:0140587.5 1
1,3-Dichlorobenzene ND ug/kg 02/26/20 13:56 541-73-102/25/20 11:0140591.1 1
1,4-Dichlorobenzene ND ug/kg 02/26/20 13:56 106-46-702/25/20 11:0140589.0 1
3,3'-Dichlorobenzidine ND ug/kg 02/26/20 13:56 91-94-102/25/20 11:018092821
2,4-Dichlorophenol ND ug/kg 02/26/20 13:56 120-83-202/25/20 11:014051341
Diethylphthalate ND ug/kg 02/26/20 13:56 84-66-202/25/20 11:0140587.8 1
2,4-Dimethylphenol ND ug/kg 02/26/20 13:56 105-67-902/25/20 11:014051011
Dimethylphthalate ND ug/kg 02/26/20 13:56 131-11-302/25/20 11:0140591.5 1
Di-n-butylphthalate ND ug/kg 02/26/20 13:56 84-74-202/25/20 11:0140599.8 1
4,6-Dinitro-2-methylphenol ND ug/kg 02/26/20 13:56 534-52-102/25/20 11:018096521
2,4-Dinitrophenol ND ug/kg 02/26/20 13:56 51-28-502/25/20 11:01202012901
2,4-Dinitrotoluene ND ug/kg 02/26/20 13:56 121-14-202/25/20 11:014051071
2,6-Dinitrotoluene ND ug/kg 02/26/20 13:56 606-20-202/25/20 11:014051061
Di-n-octylphthalate ND ug/kg 02/26/20 13:56 117-84-0 v102/25/20 11:014052301
bis(2-Ethylhexyl)phthalate ND ug/kg 02/26/20 13:56 117-81-702/25/20 11:014051321
Fluoranthene 14100 ug/kg 02/26/20 22:03 206-44-002/25/20 11:014050122010
Fluorene 5860 ug/kg 02/26/20 22:03 86-73-702/25/20 11:014050108010
Hexachloro-1,3-butadiene ND ug/kg 02/26/20 13:56 87-68-302/25/20 11:0140598.3 1
Hexachlorobenzene ND ug/kg 02/26/20 13:56 118-74-102/25/20 11:014051031
Hexachlorocyclopentadiene ND ug/kg 02/26/20 13:56 77-47-402/25/20 11:014051621
Hexachloroethane ND ug/kg 02/26/20 13:56 67-72-102/25/20 11:0140592.2 1
Indeno(1,2,3-cd)pyrene 703 ug/kg 02/26/20 13:56 193-39-502/25/20 11:014051851
REPORT OF LABORATORY ANALYSIS
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Page 5 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92466478
ANR.007
Sample:SS-1A (2-3)Lab ID:92466478001 Collected:02/24/20 11:00 Received:02/24/20 12:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Isophorone ND ug/kg 02/26/20 13:56 78-59-102/25/20 11:0140587.9 1
1-Methylnaphthalene 924 ug/kg 02/26/20 13:56 90-12-002/25/20 11:014051081
2-Methylnaphthalene 1350 ug/kg 02/26/20 13:56 91-57-602/25/20 11:014051031
2-Methylphenol(o-Cresol)ND ug/kg 02/26/20 13:56 95-48-702/25/20 11:0140589.6 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 02/26/20 13:56 15831-10-402/25/20 11:014051021
Naphthalene 702 ug/kg 02/26/20 13:56 91-20-302/25/20 11:0140596.8 1
2-Nitroaniline ND ug/kg 02/26/20 13:56 88-74-402/25/20 11:0120202041
3-Nitroaniline ND ug/kg 02/26/20 13:56 99-09-202/25/20 11:0120202151
4-Nitroaniline ND ug/kg 02/26/20 13:56 100-01-602/25/20 11:018092001
Nitrobenzene ND ug/kg 02/26/20 13:56 98-95-302/25/20 11:0140596.6 1
2-Nitrophenol ND ug/kg 02/26/20 13:56 88-75-502/25/20 11:014051251
4-Nitrophenol ND ug/kg 02/26/20 13:56 100-02-702/25/20 11:0120206451
N-Nitrosodimethylamine ND ug/kg 02/26/20 13:56 62-75-902/25/20 11:014051141
N-Nitroso-di-n-propylamine ND ug/kg 02/26/20 13:56 621-64-702/25/20 11:014051131
N-Nitrosodiphenylamine ND ug/kg 02/26/20 13:56 86-30-602/25/20 11:014051031
2,2'-Oxybis(1-chloropropane)ND ug/kg 02/26/20 13:56 108-60-102/25/20 11:014051121
Pentachlorophenol ND ug/kg 02/26/20 13:56 87-86-502/25/20 11:018091851
Phenanthrene 18100 ug/kg 02/26/20 22:03 85-01-802/25/20 11:014050102010
Phenol ND ug/kg 02/26/20 13:56 108-95-202/25/20 11:0140596.6 1
Pyrene 9600 ug/kg 02/26/20 22:03 129-00-002/25/20 11:014050111010
Pyridine ND ug/kg 02/26/20 13:56 110-86-102/25/20 11:014051021
1,2,4-Trichlorobenzene ND ug/kg 02/26/20 13:56 120-82-102/25/20 11:0140592.7 1
2,4,5-Trichlorophenol ND ug/kg 02/26/20 13:56 95-95-402/25/20 11:014051051
2,4,6-Trichlorophenol ND ug/kg 02/26/20 13:56 88-06-202/25/20 11:014051021
Surrogates
Nitrobenzene-d5 (S)66 %02/26/20 13:56 4165-60-002/25/20 11:0123-110 1
2-Fluorobiphenyl (S)52 %02/26/20 13:56 321-60-802/25/20 11:0130-110 1
Terphenyl-d14 (S)68 %02/26/20 13:56 1718-51-002/25/20 11:0128-110 1
Phenol-d6 (S)63 %02/26/20 13:56 13127-88-302/25/20 11:0122-110 1
2-Fluorophenol (S)67 %02/26/20 13:56 367-12-402/25/20 11:0113-110 1
2,4,6-Tribromophenol (S)78 %02/26/20 13:56 118-79-602/25/20 11:0127-110 1
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 02/26/20 17:05 67-64-102/26/20 10:35337031825
Benzene ND ug/kg 02/26/20 17:05 71-43-202/26/20 10:3516830.2 25
Bromobenzene ND ug/kg 02/26/20 17:05 108-86-102/26/20 10:3516845.8 25
Bromochloromethane ND ug/kg 02/26/20 17:05 74-97-502/26/20 10:3516841.4 25
Bromodichloromethane ND ug/kg 02/26/20 17:05 75-27-402/26/20 10:3516832.9 25
Bromoform ND ug/kg 02/26/20 17:05 75-25-202/26/20 10:3516882.2 25
Bromomethane ND ug/kg 02/26/20 17:05 74-83-9 IH02/26/20 10:3533779.5 25
2-Butanone (MEK)ND ug/kg 02/26/20 17:05 78-93-302/26/20 10:35337040125
n-Butylbenzene ND ug/kg 02/26/20 17:05 104-51-802/26/20 10:3516895.0 25
sec-Butylbenzene ND ug/kg 02/26/20 17:05 135-98-802/26/20 10:3516871.4 25
tert-Butylbenzene ND ug/kg 02/26/20 17:05 98-06-602/26/20 10:3516856.9 25
Carbon tetrachloride ND ug/kg 02/26/20 17:05 56-23-502/26/20 10:3516832.3 25
REPORT OF LABORATORY ANALYSIS
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Page 6 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92466478
ANR.007
Sample:SS-1A (2-3)Lab ID:92466478001 Collected:02/24/20 11:00 Received:02/24/20 12:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Chlorobenzene ND ug/kg 02/26/20 17:05 108-90-702/26/20 10:3516832.6 25
Chloroethane ND ug/kg 02/26/20 17:05 75-00-302/26/20 10:3533770.4 25
Chloroform ND ug/kg 02/26/20 17:05 67-66-302/26/20 10:3516835.7 25
Chloromethane ND ug/kg 02/26/20 17:05 74-87-3 v202/26/20 10:3533711025
2-Chlorotoluene ND ug/kg 02/26/20 17:05 95-49-802/26/20 10:3516851.2 25
4-Chlorotoluene ND ug/kg 02/26/20 17:05 106-43-402/26/20 10:3516850.5 25
1,2-Dibromo-3-chloropropane ND ug/kg 02/26/20 17:05 96-12-802/26/20 10:3516885.5 25
Dibromochloromethane ND ug/kg 02/26/20 17:05 124-48-102/26/20 10:3516884.2 25
1,2-Dibromoethane (EDB)ND ug/kg 02/26/20 17:05 106-93-402/26/20 10:3516837.7 25
Dibromomethane ND ug/kg 02/26/20 17:05 74-95-302/26/20 10:3516850.2 25
1,2-Dichlorobenzene ND ug/kg 02/26/20 17:05 95-50-102/26/20 10:3516859.3 25
1,3-Dichlorobenzene ND ug/kg 02/26/20 17:05 541-73-102/26/20 10:3516859.9 25
1,4-Dichlorobenzene ND ug/kg 02/26/20 17:05 106-46-702/26/20 10:3516858.3 25
Dichlorodifluoromethane ND ug/kg 02/26/20 17:05 75-71-802/26/20 10:3533713825
1,1-Dichloroethane ND ug/kg 02/26/20 17:05 75-34-302/26/20 10:3516824.8 25
1,2-Dichloroethane ND ug/kg 02/26/20 17:05 107-06-202/26/20 10:3516833.7 25
1,1-Dichloroethene ND ug/kg 02/26/20 17:05 75-35-402/26/20 10:3516839.1 25
cis-1,2-Dichloroethene ND ug/kg 02/26/20 17:05 156-59-202/26/20 10:3516829.2 25
trans-1,2-Dichloroethene ND ug/kg 02/26/20 17:05 156-60-502/26/20 10:3516833.0 25
1,2-Dichloropropane ND ug/kg 02/26/20 17:05 78-87-502/26/20 10:3516863.3 25
1,3-Dichloropropane ND ug/kg 02/26/20 17:05 142-28-902/26/20 10:3516863.6 25
2,2-Dichloropropane ND ug/kg 02/26/20 17:05 594-20-702/26/20 10:3516816.6 25
1,1-Dichloropropene ND ug/kg 02/26/20 17:05 563-58-602/26/20 10:3516871.4 25
cis-1,3-Dichloropropene ND ug/kg 02/26/20 17:05 10061-01-502/26/20 10:3516876.4 25
trans-1,3-Dichloropropene ND ug/kg 02/26/20 17:05 10061-02-602/26/20 10:3516829.5 25
Diisopropyl ether ND ug/kg 02/26/20 17:05 108-20-302/26/20 10:3516896.3 25
Ethylbenzene ND ug/kg 02/26/20 17:05 100-41-402/26/20 10:3516835.7 25
Hexachloro-1,3-butadiene ND ug/kg 02/26/20 17:05 87-68-302/26/20 10:3516883.2 25
2-Hexanone ND ug/kg 02/26/20 17:05 591-78-602/26/20 10:35168017425
Isopropylbenzene (Cumene)ND ug/kg 02/26/20 17:05 98-82-802/26/20 10:3516848.8 25
p-Isopropyltoluene ND ug/kg 02/26/20 17:05 99-87-602/26/20 10:3516881.2 25
Methylene Chloride ND ug/kg 02/26/20 17:05 75-09-202/26/20 10:3567419925
4-Methyl-2-pentanone (MIBK)ND ug/kg 02/26/20 17:05 108-10-102/26/20 10:35168012625
Methyl-tert-butyl ether ND ug/kg 02/26/20 17:05 1634-04-402/26/20 10:3516896.3 25
Naphthalene 981 ug/kg 02/26/20 17:05 91-20-302/26/20 10:3516814325
n-Propylbenzene ND ug/kg 02/26/20 17:05 103-65-102/26/20 10:3516856.2 25
Styrene ND ug/kg 02/26/20 17:05 100-42-502/26/20 10:3516849.8 25
1,1,1,2-Tetrachloroethane ND ug/kg 02/26/20 17:05 630-20-602/26/20 10:3516841.4 25
1,1,2,2-Tetrachloroethane ND ug/kg 02/26/20 17:05 79-34-502/26/20 10:3516858.3 25
Tetrachloroethene ND ug/kg 02/26/20 17:05 127-18-402/26/20 10:3516853.2 25
Toluene ND ug/kg 02/26/20 17:05 108-88-302/26/20 10:3516854.6 25
1,2,3-Trichlorobenzene ND ug/kg 02/26/20 17:05 87-61-602/26/20 10:3516812025
1,2,4-Trichlorobenzene ND ug/kg 02/26/20 17:05 120-82-102/26/20 10:3516889.2 25
1,1,1-Trichloroethane ND ug/kg 02/26/20 17:05 71-55-602/26/20 10:3516829.3 25
1,1,2-Trichloroethane ND ug/kg 02/26/20 17:05 79-00-502/26/20 10:3516838.1 25
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2020 02:48 PM
Pace Analytical Services, LLC
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Page 7 of 25
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92466478
ANR.007
Sample:SS-1A (2-3)Lab ID:92466478001 Collected:02/24/20 11:00 Received:02/24/20 12:17 Matrix:Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Trichloroethene ND ug/kg 02/26/20 17:05 79-01-602/26/20 10:3516843.8 25
Trichlorofluoromethane ND ug/kg 02/26/20 17:05 75-69-402/26/20 10:3516839.7 25
1,2,3-Trichloropropane ND ug/kg 02/26/20 17:05 96-18-402/26/20 10:3516856.9 25
1,2,4-Trimethylbenzene ND ug/kg 02/26/20 17:05 95-63-602/26/20 10:3516865.7 25
1,3,5-Trimethylbenzene ND ug/kg 02/26/20 17:05 108-67-802/26/20 10:3516856.2 25
Vinyl acetate ND ug/kg 02/26/20 17:05 108-05-402/26/20 10:35168054925
Vinyl chloride ND ug/kg 02/26/20 17:05 75-01-402/26/20 10:3533764.0 25
Xylene (Total)ND ug/kg 02/26/20 17:05 1330-20-702/26/20 10:3533711825
m&p-Xylene ND ug/kg 02/26/20 17:05 179601-23-102/26/20 10:3533779.5 25
o-Xylene ND ug/kg 02/26/20 17:05 95-47-602/26/20 10:3516839.4 25
Surrogates
Toluene-d8 (S)102 %02/26/20 17:05 2037-26-5 D302/26/20 10:3570-130 25
4-Bromofluorobenzene (S)97 %02/26/20 17:05 460-00-402/26/20 10:3570-130 25
1,2-Dichloroethane-d4 (S)91 %02/26/20 17:05 17060-07-002/26/20 10:3570-132 25
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 17.9 %02/24/20 17:120.10 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2020 02:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92466478
ANR.007
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
527142
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples:92466478001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2816494
Associated Lab Samples:92466478001
Matrix:Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 02/26/20 12:561.2
1,1,1-Trichloroethane ug/kg ND 5.0 02/26/20 12:560.87
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 02/26/20 12:561.7
1,1,2-Trichloroethane ug/kg ND 5.0 02/26/20 12:561.1
1,1-Dichloroethane ug/kg ND 5.0 02/26/20 12:560.74
1,1-Dichloroethene ug/kg ND 5.0 02/26/20 12:561.2
1,1-Dichloropropene ug/kg ND 5.0 02/26/20 12:562.1
1,2,3-Trichlorobenzene ug/kg ND 5.0 02/26/20 12:563.6
1,2,3-Trichloropropane ug/kg ND 5.0 02/26/20 12:561.7
1,2,4-Trichlorobenzene ug/kg ND 5.0 02/26/20 12:562.6
1,2,4-Trimethylbenzene ug/kg ND 5.0 02/26/20 12:562.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 02/26/20 12:562.5
1,2-Dibromoethane (EDB)ug/kg ND 5.0 02/26/20 12:561.1
1,2-Dichlorobenzene ug/kg ND 5.0 02/26/20 12:561.8
1,2-Dichloroethane ug/kg ND 5.0 02/26/20 12:561.0
1,2-Dichloropropane ug/kg ND 5.0 02/26/20 12:561.9
1,3,5-Trimethylbenzene ug/kg ND 5.0 02/26/20 12:561.7
1,3-Dichlorobenzene ug/kg ND 5.0 02/26/20 12:561.8
1,3-Dichloropropane ug/kg ND 5.0 02/26/20 12:561.9
1,4-Dichlorobenzene ug/kg ND 5.0 02/26/20 12:561.7
2,2-Dichloropropane ug/kg ND 5.0 02/26/20 12:560.49
2-Butanone (MEK)ug/kg ND 100 02/26/20 12:5611.9
2-Chlorotoluene ug/kg ND 5.0 02/26/20 12:561.5
2-Hexanone ug/kg ND 50.0 02/26/20 12:565.2
4-Chlorotoluene ug/kg ND 5.0 02/26/20 12:561.5
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 02/26/20 12:563.7
Acetone ug/kg ND 100 02/26/20 12:569.4
Benzene ug/kg ND 5.0 02/26/20 12:560.90
Bromobenzene ug/kg ND 5.0 02/26/20 12:561.4
Bromochloromethane ug/kg ND 5.0 02/26/20 12:561.2
Bromodichloromethane ug/kg ND 5.0 02/26/20 12:560.98
Bromoform ug/kg ND 5.0 02/26/20 12:562.4
Bromomethane ug/kg ND 10.0 IH02/26/20 12:562.4
Carbon tetrachloride ug/kg ND 5.0 02/26/20 12:560.96
Chlorobenzene ug/kg ND 5.0 02/26/20 12:560.97
Chloroethane ug/kg ND 10.0 02/26/20 12:562.1
Chloroform ug/kg ND 5.0 02/26/20 12:561.1
Chloromethane ug/kg ND 10.0 v202/26/20 12:563.3
cis-1,2-Dichloroethene ug/kg ND 5.0 02/26/20 12:560.87
cis-1,3-Dichloropropene ug/kg ND 5.0 02/26/20 12:562.3
Dibromochloromethane ug/kg ND 5.0 02/26/20 12:562.5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2020 02:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92466478
ANR.007
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2816494
Associated Lab Samples:92466478001
Matrix:Solid
AnalyzedMDL
Dibromomethane ug/kg ND 5.0 02/26/20 12:561.5
Dichlorodifluoromethane ug/kg ND 10.0 02/26/20 12:564.1
Diisopropyl ether ug/kg ND 5.0 02/26/20 12:562.9
Ethylbenzene ug/kg ND 5.0 02/26/20 12:561.1
Hexachloro-1,3-butadiene ug/kg ND 5.0 02/26/20 12:562.5
Isopropylbenzene (Cumene)ug/kg ND 5.0 02/26/20 12:561.4
m&p-Xylene ug/kg ND 10.0 02/26/20 12:562.4
Methyl-tert-butyl ether ug/kg ND 5.0 02/26/20 12:562.9
Methylene Chloride ug/kg ND 20.0 02/26/20 12:565.9
n-Butylbenzene ug/kg ND 5.0 02/26/20 12:562.8
n-Propylbenzene ug/kg ND 5.0 02/26/20 12:561.7
Naphthalene ug/kg ND 5.0 02/26/20 12:564.2
o-Xylene ug/kg ND 5.0 02/26/20 12:561.2
p-Isopropyltoluene ug/kg ND 5.0 02/26/20 12:562.4
sec-Butylbenzene ug/kg ND 5.0 02/26/20 12:562.1
Styrene ug/kg ND 5.0 02/26/20 12:561.5
tert-Butylbenzene ug/kg ND 5.0 02/26/20 12:561.7
Tetrachloroethene ug/kg ND 5.0 02/26/20 12:561.6
Toluene ug/kg ND 5.0 02/26/20 12:561.6
trans-1,2-Dichloroethene ug/kg ND 5.0 02/26/20 12:560.98
trans-1,3-Dichloropropene ug/kg ND 5.0 02/26/20 12:560.88
Trichloroethene ug/kg ND 5.0 02/26/20 12:561.3
Trichlorofluoromethane ug/kg ND 5.0 02/26/20 12:561.2
Vinyl acetate ug/kg ND 50.0 02/26/20 12:5616.3
Vinyl chloride ug/kg ND 10.0 02/26/20 12:561.9
Xylene (Total)ug/kg ND 10.0 02/26/20 12:563.5
1,2-Dichloroethane-d4 (S)%95 70-132 02/26/20 12:56
4-Bromofluorobenzene (S)%100 70-130 02/26/20 12:56
Toluene-d8 (S)%103 70-130 02/26/20 12:56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2816495LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 49.650 99 70-130
1,1,1-Trichloroethane ug/kg 43.950 88 70-130
1,1,2,2-Tetrachloroethane ug/kg 47.950 96 55-130
1,1,2-Trichloroethane ug/kg 49.950 100 70-130
1,1-Dichloroethane ug/kg 42.550 85 68-130
1,1-Dichloroethene ug/kg 45.250 90 70-130
1,1-Dichloropropene ug/kg 47.350 95 70-130
1,2,3-Trichlorobenzene ug/kg 48.950 98 70-130
1,2,3-Trichloropropane ug/kg 48.250 96 70-130
1,2,4-Trichlorobenzene ug/kg 51.350 103 70-130
1,2,4-Trimethylbenzene ug/kg 48.350 97 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2020 02:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92466478
ANR.007
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2816495LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 51.250 102 57-141
1,2-Dibromoethane (EDB)ug/kg 49.150 98 70-130
1,2-Dichlorobenzene ug/kg 48.250 96 70-130
1,2-Dichloroethane ug/kg 44.550 89 70-130
1,2-Dichloropropane ug/kg 49.850 100 70-130
1,3,5-Trimethylbenzene ug/kg 48.850 98 70-130
1,3-Dichlorobenzene ug/kg 48.250 96 70-130
1,3-Dichloropropane ug/kg 49.850 100 70-130
1,4-Dichlorobenzene ug/kg 49.050 98 70-130
2,2-Dichloropropane ug/kg 44.750 89 70-130
2-Butanone (MEK)ug/kg 100100 100 60-130
2-Chlorotoluene ug/kg 48.950 98 70-130
2-Hexanone ug/kg 103100 103 70-132
4-Chlorotoluene ug/kg 49.150 98 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 102100 102 69-130
Acetone ug/kg 89.3J100 89 49-148
Benzene ug/kg 48.050 96 70-130
Bromobenzene ug/kg 47.050 94 70-130
Bromochloromethane ug/kg 46.550 93 70-130
Bromodichloromethane ug/kg 49.650 99 70-130
Bromoform ug/kg 49.750 99 68-136
Bromomethane ug/kg 56.7 IH5011360-140
Carbon tetrachloride ug/kg 48.750 97 70-130
Chlorobenzene ug/kg 48.450 97 70-130
Chloroethane ug/kg 48.550 97 51-147
Chloroform ug/kg 44.650 89 70-130
Chloromethane ug/kg 36.9 v3507448-130
cis-1,2-Dichloroethene ug/kg 43.250 86 70-130
cis-1,3-Dichloropropene ug/kg 49.550 99 70-130
Dibromochloromethane ug/kg 49.950 100 70-130
Dibromomethane ug/kg 46.850 94 70-130
Dichlorodifluoromethane ug/kg 40.250 80 49-130
Diisopropyl ether ug/kg 45.950 92 66-130
Ethylbenzene ug/kg 46.350 93 70-130
Hexachloro-1,3-butadiene ug/kg 51.650 103 70-130
Isopropylbenzene (Cumene)ug/kg 48.650 97 70-130
m&p-Xylene ug/kg 94.0100 94 70-130
Methyl-tert-butyl ether ug/kg 48.350 97 70-130
Methylene Chloride ug/kg 41.150 82 50-137
n-Butylbenzene ug/kg 49.650 99 70-130
n-Propylbenzene ug/kg 47.850 96 70-130
Naphthalene ug/kg 48.850 98 70-131
o-Xylene ug/kg 47.450 95 70-130
p-Isopropyltoluene ug/kg 49.450 99 70-130
sec-Butylbenzene ug/kg 47.750 95 70-130
Styrene ug/kg 49.550 99 70-130
tert-Butylbenzene ug/kg 42.350 85 69-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 02/27/2020 02:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92466478
ANR.007
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2816495LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 47.850 96 56-130
Toluene ug/kg 46.350 93 70-130
trans-1,2-Dichloroethene ug/kg 43.950 88 70-130
trans-1,3-Dichloropropene ug/kg 50.050 100 70-130
Trichloroethene ug/kg 49.650 99 70-141
Trichlorofluoromethane ug/kg 43.750 87 67-130
Vinyl acetate ug/kg 119100 119 10-136
Vinyl chloride ug/kg 49.250 98 67-130
Xylene (Total)ug/kg 141150 94 70-130
1,2-Dichloroethane-d4 (S)%90 70-132
4-Bromofluorobenzene (S)%96 70-130
Toluene-d8 (S)%100 70-130
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2816496MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92466478001
2816497
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,1,1,2-Tetrachloroethane ug/kg 673 76 52-13383 10 30673ND509561
1,1,1-Trichloroethane ug/kg 673 80 49-13791 12 30673ND542612
1,1,2,2-Tetrachloroethane ug/kg 673 66 39-15074 12 30673ND442499
1,1,2-Trichloroethane ug/kg 673 78 48-14084 7 30673ND525563
1,1-Dichloroethane ug/kg 673 78 46-13588 12 30673ND526594
1,1-Dichloroethene ug/kg 673 71 38-14977 8 30673ND481519
1,1-Dichloropropene ug/kg 673 87 41-14096 11 30673ND583649
1,2,3-Trichlorobenzene ug/kg 673 55 10-15861 10 30673ND371409
1,2,3-Trichloropropane ug/kg 673 71 33-15776 6 30673ND479511
1,2,4-Trichlorobenzene ug/kg 673 55 10-15562 13 30673ND370419
1,2,4-Trimethylbenzene ug/kg 673 74 24-15485 13 30673ND537610
1,2-Dibromo-3-
chloropropane ug/kg 673 59 33-15867 14 30673ND395453
1,2-Dibromoethane (EDB)ug/kg 673 74 40-13680 8 30673ND498541
1,2-Dichlorobenzene ug/kg 673 69 27-14678 12 30673ND466527
1,2-Dichloroethane ug/kg 673 71 49-14082 14 30673ND476549
1,2-Dichloropropane ug/kg 673 83 44-14394 12 30673ND562634
1,3,5-Trimethylbenzene ug/kg 673 81 40-14492 12 30673ND548616
1,3-Dichlorobenzene ug/kg 673 68 33-14080 17 30673ND457539
1,3-Dichloropropane ug/kg 673 76 47-14782 7 30673ND514552
1,4-Dichlorobenzene ug/kg 673 69 35-13978 13 30673ND466528
2,2-Dichloropropane ug/kg 673 81 41-14090 11 30673ND543608
2-Butanone (MEK)ug/kg 1350 62 10-18169 301350ND840J927J
2-Chlorotoluene ug/kg 673 79 38-14792 15 30673ND534619
2-Hexanone ug/kg 1350 63 18-16972 301350ND855J976J
4-Chlorotoluene ug/kg 673 77 36-14587 13 30673ND518589
4-Methyl-2-pentanone
(MIBK)ug/kg 1350 64 16-17573 301350ND868J985J
Acetone ug/kg 1350 48 10-20054 301350ND650J733J
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2020 02:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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Page 12 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92466478
ANR.007
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2816496MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92466478001
2816497
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Benzene ug/kg 673 85 46-13696 13 30673ND572649
Bromobenzene ug/kg 673 77 38-14986 11 30673ND520580
Bromochloromethane ug/kg 673 68 44-14275 10 30673ND455502
Bromodichloromethane ug/kg 673 77 41-14086 11 30673ND520582
Bromoform ug/kg 673 61 34-14568 11 30673ND409458
Bromomethane ug/kg IH6737214-16289 21 30673ND485602
Carbon tetrachloride ug/kg 673 87 44-14199 13 30673ND586666
Chlorobenzene ug/kg 673 80 39-14188 9 30673ND541594
Chloroethane ug/kg 673 57 10-18268 18 30673ND384458
Chloroform ug/kg 673 76 45-14083 8 30673ND514558
Chloromethane ug/kg v36736619-14975 12 30673ND447506
cis-1,2-Dichloroethene ug/kg 673 75 38-15084 11 30673ND505563
cis-1,3-Dichloropropene ug/kg 673 77 30-14487 12 30673ND521586
Dibromochloromethane ug/kg 673 70 36-14575 6 30673ND473502
Dibromomethane ug/kg 673 72 41-14581 11 30673ND488544
Dichlorodifluoromethane ug/kg 673 70 16-14676 9 30673ND469512
Diisopropyl ether ug/kg 673 71 41-14378 10 30673ND478528
Ethylbenzene ug/kg 673 81 35-14489 10 30673ND543599
Hexachloro-1,3-butadiene ug/kg 673 47 10-16053 12 30673ND318359
Isopropylbenzene
(Cumene)
ug/kg 673 82 30-15292 11 30673ND555622
m&p-Xylene ug/kg 1350 80 33-14590 11 301350ND10801210
Methyl-tert-butyl ether ug/kg 673 70 49-14076 8 30673ND469510
Methylene Chloride ug/kg 673 63 10-17472 30673ND423J488J
n-Butylbenzene ug/kg 673 66 10-16075 14 30673ND442506
n-Propylbenzene ug/kg 673 82 24-15990 9 30673ND555608
Naphthalene ug/kg 673 25 10-17137 7 3067398111501230
o-Xylene ug/kg 673 81 31-15091 12 30673ND547615
p-Isopropyltoluene ug/kg 673 75 21-15485 13 30673ND504575
sec-Butylbenzene ug/kg 673 77 19-15987 13 30673ND516586
Styrene ug/kg 673 76 15-15284 10 30673ND513566
tert-Butylbenzene ug/kg 673 75 31-14181 9 30673ND502548
Tetrachloroethene ug/kg 673 80 19-14191 14 30673ND536616
Toluene ug/kg 673 85 31-14698 14 30673ND572660
trans-1,2-Dichloroethene ug/kg 673 79 28-15786 10 30673ND529582
trans-1,3-Dichloropropene ug/kg 673 76 25-14684 9 30673ND515563
Trichloroethene ug/kg 673 88 34-149100 13 30673ND591676
Trichlorofluoromethane ug/kg 673 50 10-16759 17 30673ND337400
Vinyl acetate ug/kg 1350 51 10-20053 301350ND683J708J
Vinyl chloride ug/kg 673 79 36-15591 14 30673ND534614
Xylene (Total)ug/kg 2020 81 29-14890 12 302020ND16301830
1,2-Dichloroethane-d4 (S)%94 70-13297
4-Bromofluorobenzene (S)%97 70-13096
Toluene-d8 (S)%102 70-130104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 02/27/2020 02:48 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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[phone]
Page 13 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92466478
ANR.007
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
526858
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Associated Lab Samples:92466478001
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2815166
Associated Lab Samples:92466478001
Matrix:Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 332 02/26/20 10:2676.1
1,2-Dichlorobenzene ug/kg ND 332 02/26/20 10:2671.9
1,3-Dichlorobenzene ug/kg ND 332 02/26/20 10:2674.8
1,4-Dichlorobenzene ug/kg ND 332 02/26/20 10:2673.1
1-Methylnaphthalene ug/kg ND 332 02/26/20 10:2688.5
2,2'-Oxybis(1-chloropropane)ug/kg ND 332 02/26/20 10:2692.3
2,4,5-Trichlorophenol ug/kg ND 332 02/26/20 10:2686.3
2,4,6-Trichlorophenol ug/kg ND 332 02/26/20 10:2683.5
2,4-Dichlorophenol ug/kg ND 332 02/26/20 10:26110
2,4-Dimethylphenol ug/kg ND 332 02/26/20 10:2682.8
2,4-Dinitrophenol ug/kg ND 1660 02/26/20 10:261060
2,4-Dinitrotoluene ug/kg ND 332 02/26/20 10:2688.0
2,6-Dinitrotoluene ug/kg ND 332 02/26/20 10:2686.9
2-Chloronaphthalene ug/kg ND 332 02/26/20 10:2674.0
2-Chlorophenol ug/kg ND 332 02/26/20 10:2677.3
2-Methylnaphthalene ug/kg ND 332 02/26/20 10:2684.6
2-Methylphenol(o-Cresol)ug/kg ND 332 02/26/20 10:2673.6
2-Nitroaniline ug/kg ND 1660 02/26/20 10:26167
2-Nitrophenol ug/kg ND 332 02/26/20 10:26103
3&4-Methylphenol(m&p Cresol)ug/kg ND 332 02/26/20 10:2683.6
3,3'-Dichlorobenzidine ug/kg ND 664 02/26/20 10:26232
3-Nitroaniline ug/kg ND 1660 02/26/20 10:26176
4,6-Dinitro-2-methylphenol ug/kg ND 664 02/26/20 10:26536
4-Bromophenylphenyl ether ug/kg ND 332 02/26/20 10:2687.2
4-Chloro-3-methylphenol ug/kg ND 664 02/26/20 10:26202
4-Chloroaniline ug/kg ND 664 02/26/20 10:26203
4-Chlorophenylphenyl ether ug/kg ND 332 02/26/20 10:2686.3
4-Nitroaniline ug/kg ND 664 02/26/20 10:26164
4-Nitrophenol ug/kg ND 1660 02/26/20 10:26530
Acenaphthene ug/kg ND 332 02/26/20 10:2685.5
Acenaphthylene ug/kg ND 332 02/26/20 10:2678.6
Aniline ug/kg ND 332 02/26/20 10:2674.6
Anthracene ug/kg ND 332 02/26/20 10:2686.2
Benzo(a)anthracene ug/kg ND 332 02/26/20 10:26106
Benzo(a)pyrene ug/kg ND 332 02/26/20 10:26144
Benzo(b)fluoranthene ug/kg ND 332 02/26/20 10:26134
Benzo(g,h,i)perylene ug/kg ND 332 02/26/20 10:26130
Benzo(k)fluoranthene ug/kg ND 332 02/26/20 10:26140
Benzoic Acid ug/kg ND 1660 02/26/20 10:26358
Benzyl alcohol ug/kg ND 664 02/26/20 10:26176
bis(2-Chloroethoxy)methane ug/kg ND 332 02/26/20 10:2688.7
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92466478
ANR.007
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2815166
Associated Lab Samples:92466478001
Matrix:Solid
AnalyzedMDL
bis(2-Chloroethyl) ether ug/kg ND 332 02/26/20 10:2670.6
bis(2-Ethylhexyl)phthalate ug/kg ND 332 02/26/20 10:26109
Butylbenzylphthalate ug/kg ND 332 02/26/20 10:2688.5
Chrysene ug/kg ND 332 02/26/20 10:2696.4
Di-n-butylphthalate ug/kg ND 332 02/26/20 10:2681.9
Di-n-octylphthalate ug/kg ND 332 02/26/20 10:26189
Dibenz(a,h)anthracene ug/kg ND 332 02/26/20 10:26133
Dibenzofuran ug/kg ND 332 02/26/20 10:2683.1
Diethylphthalate ug/kg ND 332 02/26/20 10:2672.1
Dimethylphthalate ug/kg ND 332 02/26/20 10:2675.1
Fluoranthene ug/kg ND 332 02/26/20 10:26100
Fluorene ug/kg ND 332 02/26/20 10:2688.9
Hexachloro-1,3-butadiene ug/kg ND 332 02/26/20 10:2680.7
Hexachlorobenzene ug/kg ND 332 02/26/20 10:2684.4
Hexachlorocyclopentadiene ug/kg ND 332 02/26/20 10:26133
Hexachloroethane ug/kg ND 332 02/26/20 10:2675.7
Indeno(1,2,3-cd)pyrene ug/kg ND 332 02/26/20 10:26152
Isophorone ug/kg ND 332 02/26/20 10:2672.2
N-Nitroso-di-n-propylamine ug/kg ND 332 02/26/20 10:2693.0
N-Nitrosodimethylamine ug/kg ND 332 02/26/20 10:2693.4
N-Nitrosodiphenylamine ug/kg ND 332 02/26/20 10:2684.8
Naphthalene ug/kg ND 332 02/26/20 10:2679.5
Nitrobenzene ug/kg ND 332 02/26/20 10:2679.3
Pentachlorophenol ug/kg ND 664 02/26/20 10:26152
Phenanthrene ug/kg ND 332 02/26/20 10:2683.7
Phenol ug/kg ND 332 02/26/20 10:2679.3
Pyrene ug/kg ND 332 02/26/20 10:2691.4
Pyridine ug/kg ND 332 02/26/20 10:2684.1
2,4,6-Tribromophenol (S)%81 27-110 02/26/20 10:26
2-Fluorobiphenyl (S)%76 30-110 02/26/20 10:26
2-Fluorophenol (S)%76 13-110 02/26/20 10:26
Nitrobenzene-d5 (S)%74 23-110 02/26/20 10:26
Phenol-d6 (S)%70 22-110 02/26/20 10:26
Terphenyl-d14 (S)%80 28-110 02/26/20 10:26
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2815167LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/kg 14201690 84 52-130
1,2-Dichlorobenzene ug/kg 13201690 78 51-130
1,3-Dichlorobenzene ug/kg 12801690 75 50-130
1,4-Dichlorobenzene ug/kg 12801690 75 49-130
1-Methylnaphthalene ug/kg 14001690 83 55-130
2,2'-Oxybis(1-chloropropane)ug/kg 12601690 74 30-130
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92466478
ANR.007
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2815167LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,5-Trichlorophenol ug/kg 14001690 82 55-130
2,4,6-Trichlorophenol ug/kg 14001690 82 57-130
2,4-Dichlorophenol ug/kg 13801690 81 56-130
2,4-Dimethylphenol ug/kg 16401690 97 51-130
2,4-Dinitrophenol ug/kg 65108470 77 27-133
2,4-Dinitrotoluene ug/kg 15401690 91 61-130
2,6-Dinitrotoluene ug/kg 15301690 90 60-130
2-Chloronaphthalene ug/kg 13501690 80 52-130
2-Chlorophenol ug/kg 13801690 81 54-130
2-Methylnaphthalene ug/kg 13901690 82 54-130
2-Methylphenol(o-Cresol)ug/kg 13201690 78 51-130
2-Nitroaniline ug/kg 25003390 74 51-130
2-Nitrophenol ug/kg 14801690 87 49-130
3&4-Methylphenol(m&p Cresol)ug/kg 13001690 77 11-163
3,3'-Dichlorobenzidine ug/kg 28603390 84 10-132
3-Nitroaniline ug/kg 29103390 86 55-130
4,6-Dinitro-2-methylphenol ug/kg 28503390 84 47-142
4-Bromophenylphenyl ether ug/kg 14201690 84 59-130
4-Chloro-3-methylphenol ug/kg 29603390 87 55-130
4-Chloroaniline ug/kg 29303390 86 54-130
4-Chlorophenylphenyl ether ug/kg 14001690 83 58-130
4-Nitroaniline ug/kg 27803390 82 54-130
4-Nitrophenol ug/kg 72308470 85 48-130
Acenaphthene ug/kg 14101690 83 60-130
Acenaphthylene ug/kg 15701690 92 60-130
Aniline ug/kg 12201690 72 43-130
Anthracene ug/kg 14501690 86 63-130
Benzo(a)anthracene ug/kg 16501690 97 59-130
Benzo(a)pyrene ug/kg 15901690 94 57-130
Benzo(b)fluoranthene ug/kg 16301690 96 54-130
Benzo(g,h,i)perylene ug/kg 17201690 102 59-130
Benzo(k)fluoranthene ug/kg 15001690 89 54-130
Benzoic Acid ug/kg 51308470 61 19-130
Benzyl alcohol ug/kg 27603390 82 50-130
bis(2-Chloroethoxy)methane ug/kg 12301690 73 54-130
bis(2-Chloroethyl) ether ug/kg 12601690 74 48-130
bis(2-Ethylhexyl)phthalate ug/kg 15401690 91 45-134
Butylbenzylphthalate ug/kg 16101690 95 46-138
Chrysene ug/kg 15601690 92 58-130
Di-n-butylphthalate ug/kg 14101690 83 60-130
Di-n-octylphthalate ug/kg 18201690 107 53-130
Dibenz(a,h)anthracene ug/kg 17301690 102 59-130
Dibenzofuran ug/kg 14201690 84 60-130
Diethylphthalate ug/kg 14101690 83 60-130
Dimethylphthalate ug/kg 13801690 81 60-130
Fluoranthene ug/kg 14701690 87 65-130
Fluorene ug/kg 14601690 86 63-130
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92466478
ANR.007
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2815167LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachloro-1,3-butadiene ug/kg 14901690 88 46-130
Hexachlorobenzene ug/kg 13501690 80 58-130
Hexachlorocyclopentadiene ug/kg 16901690 100 23-130
Hexachloroethane ug/kg 14101690 83 47-130
Indeno(1,2,3-cd)pyrene ug/kg 17201690 102 60-130
Isophorone ug/kg 13401690 79 49-130
N-Nitroso-di-n-propylamine ug/kg 12801690 75 47-130
N-Nitrosodimethylamine ug/kg 12201690 72 45-130
N-Nitrosodiphenylamine ug/kg 13001690 77 59-130
Naphthalene ug/kg 14101690 83 55-130
Nitrobenzene ug/kg 14001690 83 49-130
Pentachlorophenol ug/kg 27603390 82 10-132
Phenanthrene ug/kg 14301690 84 62-130
Phenol ug/kg 13901690 82 46-130
Pyrene ug/kg 15701690 93 53-130
Pyridine ug/kg 10101690 60 37-130
2,4,6-Tribromophenol (S)%89 27-110
2-Fluorobiphenyl (S)%80 30-110
2-Fluorophenol (S)%87 13-110
Nitrobenzene-d5 (S)%81 23-110
Phenol-d6 (S)%81 22-110
Terphenyl-d14 (S)%84 28-110
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2815168MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92464168003
2815169
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
1,2,4-Trichlorobenzene ug/kg 1640 86 18-13085 1 301680ND14201420
1,2-Dichlorobenzene ug/kg 1640 84 14-13079 3 301680ND13701330
1,3-Dichlorobenzene ug/kg 1640 81 12-13079 1 301680ND13401320
1,4-Dichlorobenzene ug/kg 1640 80 10-13079 0 301680ND13201320
1-Methylnaphthalene ug/kg 1640 87 12-13086 1 301680ND14301450
2,2'-Oxybis(1-
chloropropane)ug/kg 1640 78 10-13080 5 301680ND12801340
2,4,5-Trichlorophenol ug/kg 1640 87 13-13078 9 301680ND14201300
2,4,6-Trichlorophenol ug/kg 1640 88 17-13079 8 301680ND14301330
2,4-Dichlorophenol ug/kg 1640 88 10-13086 0 301680ND14501440
2,4-Dimethylphenol ug/kg 1640 99 10-13097 0 301680ND16301620
2,4-Dinitrophenol ug/kg 8200 83 10-13077 6 308390ND68106440
2,4-Dinitrotoluene ug/kg 1640 91 24-13083 8 301680ND15001390
2,6-Dinitrotoluene ug/kg 1640 94 23-13085 8 301680ND15401430
2-Chloronaphthalene ug/kg 1640 85 19-13076 10 301680ND14001270
2-Chlorophenol ug/kg 1640 87 10-13086 1 301680ND14201440
2-Methylnaphthalene ug/kg 1640 86 18-13085 2 301680ND14001430
2-Methylphenol(o-Cresol)ug/kg 1640 86 10-13083 2 301680ND14101390
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92466478
ANR.007
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2815168MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92464168003
2815169
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
2-Nitroaniline ug/kg 3280 75 17-13070 5 303360ND24702340
2-Nitrophenol ug/kg 1640 86 10-13090 6 301680ND14101500
3&4-Methylphenol(m&p
Cresol)ug/kg 1640 86 10-13082 3 301680ND14001370
3,3'-Dichlorobenzidine ug/kg 3280 86 10-13085 1 303360ND28302870
3-Nitroaniline ug/kg 3280 88 24-13077 11 303360ND29002600
4,6-Dinitro-2-methylphenol ug/kg 3280 87 10-15293 9 303360ND28703130
4-Bromophenylphenyl ether ug/kg 1640 88 29-13090 5 301680ND14301500
4-Chloro-3-methylphenol ug/kg 3280 88 17-13090 5 303360ND28903030
4-Chloroaniline ug/kg 3280 90 14-13089 1 303360ND29402990
4-Chlorophenylphenyl ether ug/kg 1640 85 25-13077 8 301680ND14001290
4-Nitroaniline ug/kg 3280 83 22-13075 7 303360ND27102520
4-Nitrophenol ug/kg 8200 87 10-13076 11 308390ND71606410
Acenaphthene ug/kg 1640 84 20-13076 8 301680ND13801280
Acenaphthylene ug/kg 1640 95 25-13084 9 301680ND15601420
Aniline ug/kg 1640 79 10-13080 3 301680ND13001340
Anthracene ug/kg 1640 88 29-13089 3 301680ND14501490
Benzo(a)anthracene ug/kg 1640 102 19-130101 2 301680ND16701690
Benzo(a)pyrene ug/kg 1640 97 12-13096 2 301680ND15901620
Benzo(b)fluoranthene ug/kg 1640 104 14-130104 2 301680ND17001740
Benzo(g,h,i)perylene ug/kg 1640 104 10-130105 3 301680ND17101770
Benzo(k)fluoranthene ug/kg 1640 92 14-13090 1 301680ND15101520
Benzoic Acid ug/kg 8200 79 10-13080 3 308390ND65106680
Benzyl alcohol ug/kg 3280 89 13-13084 4 303360ND29302820
bis(2-
Chloroethoxy)methane ug/kg 1640 80 16-13082 5 301680ND13201380
bis(2-Chloroethyl) ether ug/kg 1640 85 11-13080 3 301680ND13901350
bis(2-Ethylhexyl)phthalate ug/kg 1640 93 21-13095 5 301680ND15301600
Butylbenzylphthalate ug/kg 1640 97 23-13099 5 301680ND15901660
Chrysene ug/kg 1640 96 22-13094 0 301680ND15701570
Di-n-butylphthalate ug/kg 1640 85 30-13089 7 301680ND14001490
Di-n-octylphthalate ug/kg 1640 110 23-142109 2 301680ND18001830
Dibenz(a,h)anthracene ug/kg 1640 100 10-130101 4 301680ND16301700
Dibenzofuran ug/kg 1640 86 24-13078 8 301680ND14101310
Diethylphthalate ug/kg 1640 84 26-13076 9 301680ND13801270
Dimethylphthalate ug/kg 1640 83 22-13075 8 301680ND13601250
Fluoranthene ug/kg 1640 89 33-13090 4 301680ND14601510
Fluorene ug/kg 1640 88 22-13079 9 301680ND14401320
Hexachloro-1,3-butadiene ug/kg 1640 90 13-13087 2 301680ND14801450
Hexachlorobenzene ug/kg 1640 82 29-13084 5 301680ND13501420
Hexachlorocyclopentadiene ug/kg 1640 103 10-13096 5 301680ND16901620
Hexachloroethane ug/kg 1640 87 10-13084 0 301680ND14201420
Indeno(1,2,3-cd)pyrene ug/kg 1640 104 10-130102 1 301680ND17101720
Isophorone ug/kg 1640 81 13-13083 5 301680ND13201390
N-Nitroso-di-n-propylamine ug/kg 1640 83 12-13080 2 301680ND13601340
N-Nitrosodimethylamine ug/kg 1640 75 11-13072 1 301680ND12201220
REPORT OF LABORATORY ANALYSIS
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Page 18 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92466478
ANR.007
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
2815168MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92464168003
2815169
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
N-Nitrosodiphenylamine ug/kg 1640 81 15-13084 6 301680ND13301410
Naphthalene ug/kg 1640 85 15-13086 3 301680ND14001450
Nitrobenzene ug/kg 1640 86 12-13084 0 301680ND14101410
Pentachlorophenol ug/kg 3280 84 10-13088 7 303360ND27502940
Phenanthrene ug/kg 1640 85 27-13088 5 301680ND14001480
Phenol ug/kg 1640 90 10-13087 2 301680ND14801460
Pyrene ug/kg 1640 97 19-13097 3 301680ND15901630
Pyridine ug/kg 1640 61 10-13061 2 301680ND10101020
2,4,6-Tribromophenol (S)%88 27-11094
2-Fluorobiphenyl (S)%81 30-11075
2-Fluorophenol (S)%94 13-11094
Nitrobenzene-d5 (S)%83 23-11084
Phenol-d6 (S)%86 22-11084
Terphenyl-d14 (S)%73 28-11074
REPORT OF LABORATORY ANALYSIS
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Page 19 of 25
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92466478
ANR.007
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
526746
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples:92466478001
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92465449005
2814891SAMPLE DUPLICATE:
Percent Moisture %21.5 2 2522.0
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92466478
ANR.007
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3
This analyte exceeded secondary source verification criteria high for the initial calibration. The reported results should be
considered an estimated value.IH
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
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Page 21 of 25
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92466478
ANR.007
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92466478001 526858 526938SS-1A (2-3)EPA 3546 EPA 8270E
92466478001 527142 527165SS-1A (2-3)EPA 5035A EPA 8260D
92466478001 526746SS-1A (2-3)ASTM D2974-87
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Page 22 of 25
Page 23 of 25
Page 24 of 25
Page 25 of 25

Appendix C Brownfields Property Receptor Survey Form
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Site:Southern Steel
Address:3015 Wilkinson Boulevard
City:Charlotte
County:Mecklenburg
Brownfields Project Number: 23052-19-060
Date 3/6/2020
Property and Building Characteristics
a. Provide occupancy and use information.
No buildings are currently on the site.
c. Describe the foundation construction. Include details on type, floor construction, and depth below grade.
e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details.
0
NA
20
5
0
Size of Property (acres)
% of property that is wooded/brush
5.2
20
70
d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air return, and design
considerations (e.g. positive pressure?).
0
BROWNFIELDS PROPERTY RECEPTOR SURVEY
This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the information
requested below. Distances are measured from the site property boundary unless otherwise indicated by the DEQ Brownfield’s
Project Manager (PM).
Current Usage Proposed UsageSurface Conditions
% of property that is grassed areas
% of property that is agricultural crops
% of property that is paved 45
30
10
If an existing building is on-site, please respond to the following. Information can be provided on additional sheets as needed. If
numerous buildings are on-site, consult with your PM as only information on specific buildings may be needed.
b. Describe the construction of the builidng including materials (e.g. wood frame, block), type and size of openings (e.g. windows,
bay doors), and height (number of stories).
% of property that is covered by buildings
Rev. 09/2015 Page 1 of 3
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Surrounding Property Land Use
North
South
East
West
N
Y 350 North
N
Utilities
Is there a septic system on-site? (Y or N) No
Please provide the utility providers for the subject property
a. Natural Gas Piedmont Natural Gas (not currently connected)
b. Sewer Charlotte Water (not currently connected)
c. Electricity Duke Energy (not currently connected)
d. Other __________________________
For surrounding properties, please complete the following table with available information.
Y
Y
N
Y 10-50 N
Y 150 W
N
Y
Zoning/Land Use Proposed Usage Current Use/Occupant
DirectionDistance
(ft)Address
same
Please provide information on the following land uses in the vicinity of the subject site, including a map of the surrounding areas. If
specific receptors are present, please provide addresses of the facilities.
gas station, liquor store, restaurant, veterinary hospital
vacant land and railroad maintenance facility
automotive salvage yard
school bus maintenance facility/parking lot
For the subject property, please provide a map of known buried utilites. If available, include depth to top, construction material, and
diameter of the utilities. In addition, please provide the following information on utilty providers. If additional assessment is
required, the public utility locators should be contacted. This information can then be added to a site map.
Y/N *
Is a school or daycare center within 1,000 ft of the Property?
Specific Land Uses of Interest Y/N *
* If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing specific addresses.
Distance
(ft)
2231 Weyland Ave
* If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with the subject
property.
Is a water line main within 100 ft of Property boundary?
Is a natural gas line main within 100 ft of the Property boundary?
Is a buried telephone/ cable main within 100 ft of the Property boundary?
Is a septic system leach field within 500 ft of the Property boundary?
Direction
northern boundary
same
same
same
Is there a basement within 1,000 ft of the Property
northern/ western boundaries
northern boundary
Is there a residence within 1,000 ft of the Property?
Utility/Potential Receptor
Is a buried electrical cable main within 100 ft of Property boundary?
Is a storm water pipe within 100 ft of the Property boundary?
Is a sanitary sewer within 100 ft of the Property boundary?
Rev. 09/2015 Page 2 of 3
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Water Supply
What is the potable water supply for the property? Public X Private ______
N
Y
(industrial
process)725 SW 2200 Donald Ross Rd
N
Surface Water & Wetlands
Are there surface water features on the
property? (If yes, please complete a. to d.)
Provide Information regarding Surface Water
and Wetlands
Distance
(ft)Direction Address
a. Is the water body naturally developed or
man-made?natural
Y/NWater Supply Wells
Please provide the following information regarding water supply wells in the vicinity of the Property. At a minimum, a windshield
survey within 1,500 ft of the property boundaries should be completed to determine if water supply or irrigation wells may be
present. Information from applicable databases can and should be utilized; however, should not be utilized in lieu of the windshield
survey. If multiple wells are present within the requested radius, please provide a map of the well locations. If needed, please attach
a separate table to list all wells. Please note, the PM may opt for a more extensive water supply well survey if needed.
Yes; unnamed tributary of Irwin Creek
If Private, please provide details of the water supply source (i.e. well location, well construction, etc). If public, please include the
water providers name.
Is a public water supply well within 1 mile of the Property boundary?
Is a private water supply well within 1,500 ft of the Property
boundary?
Is an irrigation well within 1,500 ft of the Property boundary?
Response/Comments
The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in the vicinity of the
Property.
The purpose of this section is to provide information on the water supply for the site and surrounding areas.
rocky/sandy soil
No
b. List the uses of the water body.
c. What is the source of the water for the
water body?
d. What is the nature of the bottom of the
water body (e.g., rocky or concrete bottom,
drainage ways or impoundments)
If no on-site surface water features, what is the
nearest surface water body?
Are there any wetlands present on the property?
If no wetlands on-site, are wetlands suspected
on adjoining properties?
Class C - not a water supply or used for recreational purposes
groundwater and/or stormwater
Rev. 09/2015 Page 3 of 3