MO-9551_40983_CA_LSA_20200213_Phase II Environmental Site Assessment

`Nrtiw�a►n►►�h �.
•` CAR' �•
Phase II ESA
Area 15 Retail Property
510-516 E. 15t" Street and
1138 N. Caldwell Street
Charlotte, North Carolina
H&H Job No. CCR-003
February 13, 2020
hart -4 hickman
SMARTER ENVIRONMENTAL SOLUTIONS
2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301
Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com
704.586.0007 main I 919.847.4241 main

Phase II ESA
Area 15 Retail Property
510-516 E. 15th Street and 1138 N. Caldwell Street
Charlotte, North Carolina
H&H Job No. CCR-003
Table of Contents
1.0 Introduction.............................................................................................................................1
2.0 Phase II ESA Sampling Activities.........................................................................................2
2.1 Utility Locating/Geophysical Survey....................................................................................2
2.2 Soil Sampling........................................................................................................................2
2.3 Water Supply Well Survey....................................................................................................3
2.4 Analytical Results..................................................................................................................4
3.0 Summary and Conclusions.....................................................................................................5
i _!—, _r'r_1-11__
Table 1 Summary of Soil Analytical Results
List of Figures
Figure 1 Site Location Map
Figure 2 Site and Sample Location Map
List of Appendices
Appendix A Soil Boring Logs
Appendix B Laboratory Analytical Reports
i
SAAAA-Master Projects\Carolina Capital Real Estate Partners (CCR)\CCR-003 E. 15th Street\Report\Phase II ESA - Area 15 Property (2-13-20).docx hart : h i c kma n
SMARTER ENVIRONMENTAL SOLUTIONS

Phase II ESA
Area 15 Retail Property
510-516 E. 15th Street and 1138 N. Caldwell Street
Charlotte, North Carolina
H&H Job No. CCR-003
1.0 Introduction
In accordance with our authorized scope of work, Hart & Hickman, PC (H&H) has performed a
Phase II Environmental Site Assessment (ESA) of the commercial property located at 1138 N.
Caldwell Street and 510-516 E. 151h Street in Charlotte, Mecklenburg County, North Carolina (Site
or subject Site). A Site location map is provided as Figure 1.
The Site consists of two contiguous parcels of land (Parcel Identification Numbers 08106504 and
08106505) that total approximately 1.32 acres. The northwestern parcel is developed with an
approximate 1,380-square foot (sq ft) former residence and an approximate 26,237-sq ft multi -
tenant retail building. The former residence is undergoing renovations for a proposed restaurant.
Tenants of the retail building include a food market, art studios, a bicycle repair shop, a dance
studio, and a distillery. The southeastern parcel consists primarily of a gravel parking lot.
H&H recently conducted Phase I ESA activities at the Site and identified the following Recognized
Environmental Condition (REC):
• A heating oil underground storage tank (UST) is located on the northwest side of the retail
building. The Site owner, Mr. Carlos Espin, stated that in 2006/2007, the UST was filled
in place with sand. No closure soil samples were collected during closure of the UST.
Based on the lack of closure soil sampling, H&H identified the heating oil UST as a REC.
In November 2019, H&H performed soil sampling activities at the Site to evaluate potential
impacts from the heating oil UST. The methods and results of the assessment activities are detailed
in the following sections.
1
SAAAA-Master Projects\Carolina Capital Real Estate Partners (CCR)\CCR-003 E. 15th Street\Report\Phase II ESA - Area 15 Property (2-13-20).docx ■
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SMARTER ENVIRONMENTAL 56L UTION5

2.0 Phase 11 ESA Sampling Activities
2.1 Utility Locating/Geophysical Survey
Prior to conducting Phase II ESA sampling activities, H&H contacted North Carolina 811 One -
Call, the public utility locating service, to mark subsurface utilities at the Site. H&H also
contracted Probe Utility Locating, Inc. (PUL), a private utility locator, to screen the proposed
boring locations for subgrade utilities using ground -penetrating radar (GPR) and electromagnetic
methods. PUL also utilized GPR to mark the approximate extent of the heating oil UST. Based
on the results of the GPR survey, the closed -in -place heating oil UST appears to be approximately
500 gallons in capacity.
2.2 Soil Sampling
On November 7, 2019, H&H contracted Mid South Environmental (Mid South) to advance two
borings (SB-1 and SB-2) adjacent to each end of the UST using direct -push technology (DPT)
methods. Soil boring locations are depicted on Figure 2.
A decontaminated stainless -steel hand auger was used to advance each boring to a depth of
approximately 5 ft below ground surface (bgs) to clear the boring of potential subsurface utilities.
Soil borings were then advanced beyond 5 ft bgs using DPT methods. Continuous soil samples
were collected from each boring, logged for lithological description, and field screened for the
presence of staining, odors, and volatile organic vapors using a calibrated photoionization detector
(PID). Based on field screening results, one soil sample was collected for laboratory analysis from
the 6-8 ft depth interval (estimated depth below the UST) in each boring. Soil boring logs
including PID screening results are included in Appendix A.
Soil samples were placed directly into laboratory -supplied glassware, labeled, and placed on ice
in a laboratory -supplied cooler. The cooler was shipped under standard chain of custody protocols
to Pace Analytical Laboratory (Pace) in Huntersville, North Carolina. Soil samples SB-1 (6-8 ft)
and SB-2 (6-8 ft) were analyzed for Total Petroleum Hydrocarbons -Diesel Range Organics (TPH-
2
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SMARTER ENVIRONMENTAL 56L UTION5

DRO) and TPH-Gasoline Range Organics (TPH-GRO) by EPA Method 8015C. H&H submitted
additional soil from SB-1 and SB-2 for "risk -based" analyses in the event that TPH-DRO or
TPH-GRO concentrations exceeded the North Carolina Department of Environmental Quality
(DEQ) Action Levels of 100 mg/kg and 50 mg/kg, respectively. Risk -based analyses for samples
SB-1 and SB-2 included volatile organic compounds (VOCs) by EPA Method 8260D, semi-VOCs
(SVOCs) by EPA Method 8270E, and volatile petroleum hydrocarbons (VPH) and extractable
petroleum hydrocarbons (EPH) by the Massachusetts Department of Environmental Protection
(MADEP) method. Based on the TPH results, only SB-2 was analyzed by the laboratory for risk -
based parameters.
Due to shallow drill rig refusal at depths of 15.5 to 16 ft bgs, Mid South was unable to install
temporary monitoring wells within the borings advanced adjacent to the heating oil UST
Upon completion of soil sampling, the soil borings were properly abandoned with hydrated
bentonite, and the surfaces were restored to approximately match pre -drilling conditions. Because
H&H did not identify evidence of significant soil impacts (i.e., free product) during field activities,
soil cuttings were thin -spread on -Site.
2.3 Water Supply Well Survey
H&H performed a walking and driving reconnaissance within an approximate 500 ft radius of the
UST basin. Properties within 500 ft of the source area appear to be connected to the municipal
water supply (i.e., water meters and fire hydrants observed), and no obvious evidence of water
supply wells was observed. In addition, according to the Mecklenburg County Land Use and
Environmental Services Agency (LUESA) Well Information System, no water supply wells are
depicted on the subject Site or on properties within 500 ft of the UST basin.
3
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SMARTER ENVIRONMENTAL 56L UTION5

2.4 Analytical Results
Soil data were compared to the DEQ UST Section Action Levels for TPH and the Maximum Soil
Contaminant Concentrations (MSCCs) for VOCs, SVOCs, EPH, and VPH. Soil analytical data
are summarized in Table 1. The laboratory analytical report is provided in Appendix B.
Soil analytical data indicate the presence of TPH-DRO in sample SB-2 (6-8 ft) at a concentration
of 1,560 mg/kg, which exceeds the DEQ Action Level of 100 mg/kg. Neither TPH-DRO nor
TPH-GRO were detected in sample SB-1 (6-8 ft) at concentrations above the laboratory method
detection limits (MDLs).
Based on the presence of TPH-DRO in sample SB-2 (6-8 ft) at a concentration above the DEQ
Action Level, the sample was analyzed for VOCs, SVOCs, EPH, and VPH. Analytical data
indicate the presence of naphthalene (9.0 mg/kg), total C9-C22 aromatics (349 mg/kg),
1-methylnaphthalene (8.0 mg/kg), and 2-methylnaphthalene (11.3 mg/kg) at concentrations above
the soil -to -groundwater MSCCs of 0.16 mg/kg, 31 mg/kg, 0.004 mg/kg, and 3.6 mg/kg,
respectively. Total C9-C18 aliphatics (2,358 mg/kg) were detected above the residential MSCC
of 1,500 mg/kg. No constituents were detected at concentrations above the industrial/commercial
MSCCs.
al
SAAAA-Master Projects\Carolina Capital Real Estate Partners (CCR)\CCR-003 E. 15th Street\Report\Phase II ESA - Area 15 Property (2-13-20).docx ■
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SMARTER ENVIRONMENTAL 56L UTION5

3.0 Summary and Conclusions
In November 2019, H&H performed Phase II ESA soil sampling activities at the commercial
property located at 1138 N. Caldwell Street and 510-516 E. 15th Street in Charlotte, Mecklenburg
County, North Carolina. A summary of the results of the Phase II ESA is provided below.
• Soil borings SB-1 and SB-2 were advanced adjacent to each end of an approximate 500-
gallon heating oil UST that was previously closed in place.
• Soil analytical data indicate the presence of TPH-DRO in sample SB-2 (6-8 ft) at a
concentration of 1,560 mg/kg, which exceeds the DEQ Action Level of 100 mg/kg.
• Naphthalene (9.0 mg/kg), total C9-C22 aromatics (349 mg/kg), 1-methylnaphthalene
(8.0 mg/kg), and 2-methylnaphthalene (11.3 mg/kg) were detected in sample SB-2 (6-8 ft)
at concentrations above the soil -to -groundwater MSCCs. Total C9-C18 aliphatics (2,358
mg/kg) were detected in sample SB-2 (6-8 ft) above the residential MSCC of 1,500 mg/kg.
• No water supply wells were identified within 500 ft of the UST basin during a field survey
or on the Mecklenburg County LUESA Well Information System.
Recommendations
H&H recommends that a risk -based No Further Action be pursued through the DEQ UST Section
in accordance with guidelines for non-commercial, non -regulated USTs. Additional tasks to
achieve regulatory closure include completing public notice requirements and filing a Notice of
Residential Petroleum, which will prohibit groundwater use at the Site and designate a "Soil
Restriction Area".
5
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SMARTER ENVIRONMENTAL 56L UTION5

Table 1
Summary of Soil Analytical Results
Area 15 Retail Property
512-516 E. 15th Street and 1128 N. Caldwell Street
Charlotte, North Carolina
H&H Job No. CCR-003
Sample ID
S13-1
SB-2
Action Level
Soil -to -Water
Residential
Industrial/
Commercial
Date
11 /7/2019
11 /7/2019
Area of Potential Concern
Closed in Place Heating Oil UST
MSCC (2)
MSCC (2)
MSCC (2)
Depth (ft bgs)
6-8
6-8
TPH-DRO (8015C)
<2.8
1,560
100
--
--
--
TPH-GRO (8015C)
<1.2
30.7
50
--
--
--
VOCs (8260D)
Acetone
NA
0.025 J
--
24
14,000
360,000
sec -Butyl benzene
NA
0.032
--
3.3
626
16,350
Ethylbenzene
NA
0.0020 J
--
4.9
1,560
40,000
Isopropylbenzene
NA
0.012
--
1.7
1,564
40,880
p-Isopropyltoluene
NA
0.056
--
0.12
100
4,000
4-Methyl-2-pentanone
NA
0.023 J
--
16
9,385
245,280
Naphthalene
NA
9.0
0.16
313
8,176
1,2,3-Trichloropropane
NA
0.0041 J
NE
NE
NE
1,2,4-Trimethylbenzene
NA
7.3
8.5
782
20,440
1,3,5-Trimethylbenzene
NA
0.17
8.3
782
20,440
m&p-Xylene
NA
0.0079 J
4.6
3,129
81,760
EPH/VPH (MADEP)
C5-C8 Aliphatics (VPH)
NA
28.8
--
68
939
24,528
C9-C12 Aliphatics (VPH)
NA
238
--
NE
NE
NE
C9-C18 Aliphatics (EPH)
NA
2,120
540
1,500
40,000
Total C9-C18 Aliphatics
NA
2,358
540
1,500
40,000
C9-C10 Aromatics (VPH)
NA
122
NE
NE
NE
C11-C22 Aromatics (EPH)
NA
227
--
NE
NE
NE
Total C9-C22 Aromatics
NA
349
--
31
469
12,264
C19-C36 Aliphatics (EPH)
NA
<610
--
Immobile
31,000
810,000
SVOCs (8270E)
Dibenzofuran
NA
0.36 J
--
4.7
62
1,635
Fluorene
NA
0.34 J
--
47
620
16,400
1-Methyl naphthalene
NA
8.0
--
0.004
20
100
2-Methyl naphthalene
NA
11.3
3.6
63
1,635
Naphthalene
NA
1.6
--
0.16
313
8,176
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Division of Waste Management Underground Storage Tank (UST) Section Action Level (December 2013).
2) DEQ UST Section Maximum Soil Contaminant Concentrations (MSCCs) (November 2016)
Method number follows parameter in parenthesis.
Soil concentrations are reported in milligrams per kilogram (mg/kg).
Bold values exceed the DEQ Action Level or Soil -to -Groundwater MSCC.
Underlined values exceed the DEQ Residential MSCC.
VOCs = volatile organic compounds; SVOCs = semi-VOCs; EPH = extractable petroleum hydrocarbons; VPH = volatile petroleum hydrocarbons
MADEP = Massachusetts Department of Environmental Protection; ft bgs= feet below ground surface; NE = not established; -- = not applicable
UST = underground storage tank; J = estimated value between the laboratory method detection limit and the laboratory reporting limit
Table 1
S:\AAA-Master Projects\Carolina Capital Real Estate Partners (CCR)\CCR-003 E. 15th Street\Phase II Report for DEQ\Soil Data Table
2/13/2020 Hart & Hickman, PC

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APPROXIMATE TITLE
N 0 2000 4000 SITE LOCATION MAP
SCALE IN FEET PROJECT AREA 15 RETAIL PROPERTY
510-516 E. 151h STREET AND 1138 N. CALDWELL STREET
CHARLOTTE, NORTH CAROLINA
U.S.G.S. QUADRANGLE MAP hart = hickman 2123 South Tryon Street -Suite 10C
Charlotte, North Carolina 28203
CHARLOTTE EAST, NORTH CAROLINA 1991 SMARTER ENVIRONMFNTu,' SOLUTIONS 704-586-0007 (p) 704-586-0373 (I)
DATE: 12-20-19 REVISION NO: 0
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC) JOB NO: CCR-003 FIGURE: 1

\�
LEGEND
SITE PROPERTY BOUNDARY
RESIDENTIAL
PARCEL BOUNDARY
STREAM
0 DUMPSTER
POLE -MOUNTED TRANSFORMER
BETHEL WORSHIP CENTER
oUST HEATING OIL
LLl
(420 E. 15TH STREET)
��� LISOSED-IN-PLACE
Z
RESIDENCES
SOIL SAMPLE LOCATION
W ^
(1204-1226 N. CALDWELL STREET)
Q
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RESTAURANT
(UNDER CONSTRUCTION)
APARTMENT BUILDINGS
NOTE:
(525 & 535 E. 15TH STREET)
G
SB-1
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A 1. AERIAL PHOTOGRAPH OBTAINED FROM MECKLENBURG
•�
COUNTY GIS, DATED 2019.
SB-2,9
FORMER AUTO
REPAIR SHOP
RETAIL
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AS
'1 HUNTER AUTO & WRECKING
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(1107 & 1111 N. DAVIDSON STREET)
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(1200 N. DAVIDSON STREET)
APPROXIMATE
0 80 160
NEENEI
SCALE IN FEET
t
TITLE
SITE AND SAMPLE LOCATION MAP
PR°SECT AREA 15 RETAIL PROPERTY
512-516 E. 15TH STREET AND
1128 N. CALDWELL STREET
CHARLOTTE NORTH CAROLINA
2923 te 100
hart hiekman Clarotte, Tryonarolina2823
Charlotte, North Carolina 28203
704-586-0007(p) 704-586-0373(0
SMARTER ENVIRONMENTAL SOLUTIONS License # C-1269 / #C-245 Geology
DATE: 2-13-20
REVISION NO. 0
JOB NO. CCR-003
FIGURE NO. 2

Appendix A
Boring Logs
hart hickman
SMARTER ENVIRONMENTAL SOLUTION5

Client: paarolina Captial Real Estate
BORING LOG
.
rtners
hart hickman
Project: CCR.003
Boring No. SB-1
SMARTER ENVIRONMENTAL SOLUTIONS
Address: East 15th Street, Charlotte, NC
Page: 1 of 1
Drilling Start Date: 1117/19
Boring Depth (ft): 16.0
Drilling End Date: 1117/19
Boring Diameter (in): 2.50
Drilling Company: Mid South
Sampling Method(s):
Drilling Method: Direct Push
DTW During Drilling (ft):
Drilling Equipment: Geoprobe 54 DT
DTW After Drilling (ft):
Driller: Don Warren
Ground Surface Elev. (ft):
Logged By: Sean Horgan
Location (X,Y):
COLLECT
MEASURE
..
i
J
W
Z
O
.-.
�
O
Jp
w
W
W
0 F
iY
O2
d
H
a)
z
SOIL/ROCK VISUAL DESCRIPTION
n
E
V
Lu
2
J
Q
°gyp
E
E
H
U
3
a�
'o
n
p
m
9
W
0
O
d
J
0 0
(0') Concrete and gravel
4.5
(05) Poorly graded GRAVEL (GP); loose, dry, dark gray
...
(15) Clayey SAND (SC); medium dense, moist, dark reddish -brown
11.8
(2.5') Sandy lean CLAY (CL); medium plasticity, medium stiff, moist, light reddish
15.7
5
5
(5) Well -graded SAND (SW); trace clay, medium dense, moist, light reddish -
brown
28.6
SB-1
(6-8)
14.9
(8') Sandy lean CLAY (CL); medium plasticity, medium stiff, moist, reddish
10
15.0
10
(95) SILT (ML); some clay, stiff, wet, reddish, with manganese mottling
(115) SILT (ML); medium stiff, moist, light brown
20.6
(13') Clayey SAND (SC); dense, wet, dark brown
15.9
15
(14') Poorly graded SAND (SP); trace gravel, medium dense, wet, light gray,
15
Partially Weathered Rock
(16') Boring terminated
20
20
25 25
NOTES: Hole precleared to 5.0' using hand auger. DPT refusal at 16' bgs.
generated using GroundLogs. online

Client: partners Captial Real Estate
BORING LOG
.
hart hickman
Project: CCR.003
Boring No. SB-2
SMARTER ENVIRONMENToI_ SOLUTIONS
Address: East 15th Street, Charlotte, NC
Page: 1 of 1
Drilling Start Date: 1117/19
Boring Depth (ft): 15.5
Drilling End Date: 11/7/19
Boring Diameter (in): 2.50
Drilling Company: Mid South
Sampling Method(s):
Drilling Method: Direct Push
DTW During Drilling (ft):
Drilling Equipment: Geoprobe 54 DT
DTW After Drilling (ft):
Driller: Don Warren
Ground Surface Elev. (ft):
Logged By: Sean Horgan
Location (X,Y):
COLLECT
MEASURE
}
00
J
W
Z
O
=
p
W
J
(� 1—
Z W
ER
d
Z
H
y
SOIL/ROCK VISUAL DESCRIPTION
N
a
af
W
a
O�
a
CL
n
❑
2
J
Q
00p
N
E
U
3
N
0
❑
m
�
W
❑
CJ
d
a
co
m
a
0 0
(0') Concrete
10.8
(0.5') Poorly graded GRAVEL (GP); dry, gray
(1.5') Clayey SAND (SC); medium dense, moist, dark brown,slight petroleum -like odor2,058
i.XXX
5,541
55
(5.5') Well SAND (SW); trace clay, dense, moist, dark brown, odor and
SB-2
(6-8)
dark stainingobserved
4,341
(8') Sandy lean CLAY (CL); medium plasticity, stiff, wet, dark brown, odor
4,706
10
(95) Poorly graded SAND (SP); medium dense, wet, light yellowish -gray, odor
10
2,286
2,298
15
(14.5') Sandy lean CLAY (CL); few fine -coarse gravel, medium plasticity, stiff, moist,
15
brown, odor j
(15.5') Boring terminated
20
20
25 25
NOTES: Hole precleared to 5.0' using hand auger. DPT refusal at 15.5' bgs.
generated using GroundLogs.online

Appendix B
Laboratory Analytical Reports
hart hickman
SMAKtER ENVIRONMENTAL SOLUTIONS

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
February 13, 2020
Bo Cappleman
Hart & Hickman
2923 South Tryon Street
Charlotte, NC 28203
RE: Project: CCR-003
Pace Project No.: 92453047
Dear Bo Cappleman:
Enclosed are the analytical results for sample(s) received by the laboratory on November 08, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Per client request, report revised 2/13/20 to relocate data for SB-3 (0-2) and SB-4 (0-2) to a separate
project.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
1(704)875-9092
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: CCR-003
Pace Project No.: 92453047
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: CCR-003
Pace Project No.: 92453047
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92453047001
92453047002
S13-1 (6-8)
S13-2 (6-8)
Solid
Solid
11/07/19 14:35
11/07/19 14:55
11/08/19 09:10
11/08/19 09:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
CCR-003
92453047
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92453047001
S13-1 (6-8)
EPA 8015C Modified
BAJ
2
PASI-C
EPA 8015C Modified
LMB
2
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92453047002
S13-2 (6-8)
EPA 8015C Modified
BAJ
2
PASI-C
MADEP EPH
BAJ
7
PASI-C
EPA 8015C Modified
LMB
2
PASI-C
MADEP VPH
LMB
6
PASI-C
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 34

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Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CCR-003
Pace Project No.: 92453047
Sample: S13-1 (6-8)
Lab ID: 92453047001 Collected: 11/07/19 14:35 Received: 11/08/19 09:10 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results Units Limit MDL DF Prepared
Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Diesel Range Organics(C10-
ND mg/kg 6.1 2.8 1 11/08/19 21:13
11/11/19 16:21
C28)
Surrogates
n-Pentacosane (S)
54 % 33-129 1 11/08/19 21:13
11/11/19 16:21 629-99-2
Gasoline Range Organics
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030E
Gas Range Organics (C6-C10)
ND mg/kg 6.3 1.2 1 11/09/19 13:00
11/09/19 18:00
Surrogates
4-Bromofluorobenzene (S)
103 % 63-130 1 11/09/19 13:00
11/09/19 18:00 460-00-4
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
16.9 % 0.10 0.10 1
11/08/19 17:54
REPORT OF LABORATORY ANALYSIS
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Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 34

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Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CCR-003
Pace Project No.: 92453047
Sample: S13-2 (6-8)
Lab ID:
92453047002
Collected:
11/07/19
14:55
Received: 11/08/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters
Results
Units
Limit
MDL
DF
Prepared
Analyzed
CAS No.
Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Diesel Range Organics(C10-
1560
mg/kg
30.8
14.2
5
11/08/19 21:13
11/11/19 17:59
C28)
Surrogates
n-Pentacosane (S)
66
%
33-129
5
11/08/19 21:13
11/11/19 17:59
629-99-2
MADEP EPH NC Soil
Analytical
Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)
2120
mg/kg
610
610
50
11/16/19 16:18
11/19/19 12:13
N2
Aliphatic (C19-C36)
ND
mg/kg
610
610
50
11/16/19 16:18
11/19/19 12:13
N2
Aromatic (C11-C22)
227
mg/kg
24.4
24.4
2
11/16/19 16:18
11/19/19 12:13
N2
Surrogates
Nonatriacontane (S)
0
%
40-140
50
11/16/19 16:18
11/19/19 12:13
7194-86-7
S4
o-Terphenyl (S)
68
%
40-140
2
11/16/19 16:18
11/19/19 12:13
84-15-1
2-Fluorobiphenyl (S)
90
%
40-140
2
11/16/19 16:18
11/19/19 12:13
321-60-8
2-Bromonaphthalene (S)
490
%
40-140
2
11/16/19 16:18
11/19/19 12:13
580-13-2
S5
Gasoline Range Organics
Analytical
Method: EPA 8015C
Modified Preparation Method: EPA 5030E
Gas Range Organics (C6-C10)
30.7
mg/kg
6.1
1.2
1
11/09/19 13:00
11/09/19 18:28
Surrogates
4-Bromofluorobenzene (S)
184
%
63-130
1
11/09/19 13:00
11/09/19 18:28
460-00-4
S5
VPH NC Soil
Analytical
Method: MADEP VPH Preparation Method: MADEP VPH
Aliphatic (C05-008)
28.8
mg/kg
3.0
3.0
1
11/13/19 13:47
11/13/19 16:26
N2
Aliphatic (C09-C12)
238
mg/kg
3.0
3.0
1
11/13/19 13:47
11/13/19 16:26
N2
Aliphatic(C09-C12)Adjusted
115
mg/kg
3.0
3.0
1
11/13/19 13:47
11/13/19 16:26
N2
Aromatic (C09-C10)
122
mg/kg
3.0
3.0
1
11/13/19 13:47
11/13/19 16:26
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
236
%
70-130
1
11/13/19 13:47
11/13/19 16:26
460-00-4
S5
4-Bromofluorobenzene (PID) (S)
127
%
70-130
1
11/13/19 13:47
11/13/19 16:26
460-00-4
8270E MSSV Microwave
Analytical
Method: EPA 8270E
Preparation Method:
EPA 3546
Acenaphthene
ND
mg/kg
0.39
0.10
1
11/19/19 07:30
11/19/19 14:10
83-32-9
Acenaphthylene
ND
mg/kg
0.39
0.093
1
11/19/19 07:30
11/19/19 14:10
208-96-8
Aniline
ND
mg/kg
0.39
0.088
1
11/19/19 07:30
11/19/19 14:10
62-53-3
Anthracene
ND
mg/kg
0.39
0.10
1
11/19/19 07:30
11/19/19 14:10
120-12-7
Benzo(a)anthracene
ND
mg/kg
0.39
0.12
1
11/19/19 07:30
11/19/19 14:10
56-55-3
Benzo(a)pyrene
ND
mg/kg
0.39
0.17
1
11/19/19 07:30
11/19/19 14:10
50-32-8
Benzo(b)fluoranthene
ND
mg/kg
0.39
0.16
1
11/19/19 07:30
11/19/19 14:10
205-99-2
Benzo(g,h,i)perylene
ND
mg/kg
0.39
0.15
1
11/19/19 07:30
11/19/19 14:10
191-24-2
Benzo(k)fluoranthene
ND
mg/kg
0.39
0.17
1
11/19/19 07:30
11/19/19 14:10
207-08-9
Benzoic Acid
ND
mg/kg
2.0
0.42
1
11/19/19 07:30
11/19/19 14:10
65-85-0
M1
Benzyl alcohol
ND
mg/kg
0.78
0.21
1
11/19/19 07:30
11/19/19 14:10
100-51-6
4-Bromophenylphenyl ether
ND
mg/kg
0.39
0.10
1
11/19/19 07:30
11/19/19 14:10
101-55-3
Butylbenzylphthalate
ND
mg/kg
0.39
0.10
1
11/19/19 07:30
11/19/19 14:10
85-68-7
4-Chloro-3-methyl phenol
ND
mg/kg
0.78
0.24
1
11/19/19 07:30
11/19/19 14:10
59-50-7
4-Chloroaniline
ND
mg/kg
2.0
0.24
1
11/19/19 07:30
11/19/19 14:10
106-47-8
REPORT OF LABORATORY ANALYSIS
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Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 34

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[phone]
ANALYTICAL RESULTS
Project: CCR-003
Pace Project No.: 92453047
Sample: S13-2 (6-8) Lab ID: 92453047002 Collected: 11/07/19 14:55 Received: 11/08/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546
bis(2-Chloroethoxy)methane
ND
mg/kg
0.39
0.10
1
11/19/19 07:30
11/19/19 14:10
111-91-1
bis(2-Chloroethyl) ether
ND
mg/kg
0.39
0.083
1
11/19/19 07:30
11/19/19 14:10
111-44-4
2-Chloronaphthalene
ND
mg/kg
0.39
0.087
1
11/19/19 07:30
11/19/19 14:10
91-58-7
2-Chlorophenol
ND
mg/kg
0.39
0.091
1
11/19/19 07:30
11/19/19 14:10
95-57-8
4-Chlorophenylphenyl ether
ND
mg/kg
0.39
0.10
1
11/19/19 07:30
11/19/19 14:10
7005-72-3
Chrysene
ND
mg/kg
0.39
0.11
1
11/19/19 07:30
11/19/19 14:10
218-01-9
Dibenz(a,h)anthracene
ND
mg/kg
0.39
0.16
1
11/19/19 07:30
11/19/19 14:10
53-70-3
Dibenzofuran
0.36J
mg/kg
0.39
0.098
1
11/19/19 07:30
11/19/19 14:10
132-64-9
1,2-Dichlorobenzene
ND
mg/kg
0.39
0.085
1
11/19/19 07:30
11/19/19 14:10
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.39
0.088
1
11/19/19 07:30
11/19/19 14:10
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.39
0.086
1
11/19/19 07:30
11/19/19 14:10
106-46-7
3,3'-Dichlorobenzidine
ND
mg/kg
2.0
0.27
1
11/19/19 07:30
11/19/19 14:10
91-94-1
2,4-Dichlorophenol
ND
mg/kg
0.39
0.13
1
11/19/19 07:30
11/19/19 14:10
120-83-2
Diethylphthalate
ND
mg/kg
0.39
0.085
1
11/19/19 07:30
11/19/19 14:10
84-66-2
2,4-Dimethylphenol
ND
mg/kg
0.39
0.098
1
11/19/19 07:30
11/19/19 14:10
105-67-9
Dimethylphthalate
ND
mg/kg
0.39
0.089
1
11/19/19 07:30
11/19/19 14:10
131-11-3
Di-n-butylphthalate
ND
mg/kg
0.39
0.097
1
11/19/19 07:30
11/19/19 14:10
84-74-2
4,6-Dinitro-2-methyl phenol
ND
mg/kg
0.78
0.63
1
11/19/19 07:30
11/19/19 14:10
534-52-1
2,4-Dinitrophenol
ND
mg/kg
2.0
1.3
1
11/19/19 07:30
11/19/19 14:10
51-28-5
2,4-Dinitrotoluene
ND
mg/kg
0.39
0.10
1
11/19/19 07:30
11/19/19 14:10
121-14-2
2,6-Dinitrotoluene
ND
mg/kg
0.39
0.10
1
11/19/19 07:30
11/19/19 14:10
606-20-2
Di-n-octylphthalate
ND
mg/kg
0.39
0.22
1
11/19/19 07:30
11/19/19 14:10
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
mg/kg
0.39
0.13
1
11/19/19 07:30
11/19/19 14:10
117-81-7
Fluoranthene
ND
mg/kg
0.39
0.12
1
11/19/19 07:30
11/19/19 14:10
206-44-0
Fluorene
0.34J
mg/kg
0.39
0.10
1
11/19/19 07:30
11/19/19 14:10
86-73-7
Hexachloro-1,3-butadiene
ND
mg/kg
0.39
0.095
1
11/19/19 07:30
11/19/19 14:10
87-68-3
Hexachlorobenzene
ND
mg/kg
0.39
0.10
1
11/19/19 07:30
11/19/19 14:10
118-74-1
Hexachlorocyclopentadiene
ND
mg/kg
0.39
0.16
1
11/19/19 07:30
11/19/19 14:10
77-47-4
Hexachloroethane
ND
mg/kg
0.39
0.089
1
11/19/19 07:30
11/19/19 14:10
67-72-1
Indeno(1,2,3-cd)pyrene
ND
mg/kg
0.39
0.18
1
11/19/19 07:30
11/19/19 14:10
193-39-5
Isophorone
ND
mg/kg
0.39
0.085
1
11/19/19 07:30
11/19/19 14:10
78-59-1
1-Methylnaphthalene
8.0
mg/kg
2.0
0.52
5
11/19/19 07:30
11/20/19 10:19
90-12-0
2-Methylnaphthalene
11.3
mg/kg
2.0
0.50
5
11/19/19 07:30
11/20/19 10:19
91-57-6
2-Methylphenol(o-Cresol)
ND
mg/kg
0.39
0.087
1
11/19/19 07:30
11/19/19 14:10
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
mg/kg
0.39
0.099
1
11/19/19 07:30
11/19/19 14:10
15831-10-4
Naphthalene
1.6
mg/kg
0.39
0.094
1
11/19/19 07:30
11/19/19 14:10
91-20-3
2-Nitroaniline
ND
mg/kg
2.0
0.20
1
11/19/19 07:30
11/19/19 14:10
88-74-4
3-Nitroaniline
ND
mg/kg
2.0
0.21
1
11/19/19 07:30
11/19/19 14:10
99-09-2
4-Nitroaniline
ND
mg/kg
0.78
0.19
1
11/19/19 07:30
11/19/19 14:10
100-01-6
Nitrobenzene
ND
mg/kg
0.39
0.094
1
11/19/19 07:30
11/19/19 14:10
98-95-3
2-Nitrophenol
ND
mg/kg
0.39
0.12
1
11/19/19 07:30
11/19/19 14:10
88-75-5
4-Nitrophenol
ND
mg/kg
2.0
0.62
1
11/19/19 07:30
11/19/19 14:10
100-02-7
N-Nitrosodimethylamine
ND
mg/kg
0.39
0.11
1
11/19/19 07:30
11/19/19 14:10
62-75-9
N-Nitroso-di-n-propylamine
ND
mg/kg
0.39
0.11
1
11/19/19 07:30
11/19/19 14:10
621-64-7
N-Nitrosodiphenylamine
ND
mg/kg
0.39
0.10
1
11/19/19 07:30
11/19/19 14:10
86-30-6
REPORT OF LABORATORY ANALYSIS
R1
M1
M1
M1
This report shall not be reproduced, except in full,
Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 34

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CCR-003
Pace Project No.: 92453047
Sample: SB-2 (6-8) Lab ID: 92453047002 Collected: 11/07/19 14:55 Received: 11/08/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546
2,2'-Oxybis(1-chloropropane)
ND
mg/kg
0.39
0.11
1
11/19/19 07:30
11/19/19 14:10
108-60-1
Pentachlorophenol
ND
mg/kg
2.0
0.18
1
11/19/19 07:30
11/19/19 14:10
87-86-5
Phenanthrene
ND
mg/kg
0.39
0.099
1
11/19/19 07:30
11/19/19 14:10
85-01-8
Phenol
ND
mg/kg
0.39
0.094
1
11/19/19 07:30
11/19/19 14:10
108-95-2
Pyrene
ND
mg/kg
0.39
0.11
1
11/19/19 07:30
11/19/19 14:10
129-00-0
Pyridine
ND
mg/kg
0.39
0.099
1
11/19/19 07:30
11/19/19 14:10
110-86-1
1,2,4-Trichlorobenzene
ND
mg/kg
0.39
0.090
1
11/19/19 07:30
11/19/19 14:10
120-82-1
2,4,5-Trichlorophenol
ND
mg/kg
0.39
0.10
1
11/19/19 07:30
11/19/19 14:10
95-95-4
2,4,6-Trichlorophenol
ND
mg/kg
0.39
0.098
1
11/19/19 07:30
11/19/19 14:10
88-06-2
Surrogates
Nitrobenzene-d5 (S)
ill
%
23-110
1
11/19/19 07:30
11/19/19 14:10
4165-60-0
2-Fluorobiphenyl (S)
69
%
30-110
1
11/19/19 07:30
11/19/19 14:10
321-60-8
Terphenyl-d14 (S)
81
%
28-110
1
11/19/19 07:30
11/19/19 14:10
1718-51-0
Phenol-d6 (S)
18
%
22-110
1
11/19/19 07:30
11/19/19 14:10
13127-88-3
2-Fluorophenol (S)
70
%
13-110
1
11/19/19 07:30
11/19/19 14:10
367-12-4
2,4,6-Tribromophenol (S)
88
%
27-110
1
11/19/19 07:30
11/19/19 14:10
118-79-6
8260D/5035A Volatile Organics
Analytical
Method: EPA 8260D Preparation Method:
EPA
5035A
Acetone
0.025J
mg/kg
0.091
0.0086
1
11/15/19 11:02
11/15/19 19:51
67-64-1
Benzene
ND
mg/kg
0.0046
0.00082
1
11/15/19 11:02
11/15/19 19:51
71-43-2
Bromobenzene
ND
mg/kg
0.0046
0.0012
1
11/15/19 11:02
11/15/19 19:51
108-86-1
Bromochloromethane
ND
mg/kg
0.0046
0.0011
1
11/15/19 11:02
11/15/19 19:51
74-97-5
Bromodichloromethane
ND
mg/kg
0.0046
0.00089
1
11/15/19 11:02
11/15/19 19:51
75-27-4
Bromoform
ND
mg/kg
0.0046
0.0022
1
11/15/19 11:02
11/15/19 19:51
75-25-2
Bromomethane
ND
mg/kg
0.0091
0.0022
1
11/15/19 11:02
11/15/19 19:51
74-83-9
2-Butanone (MEK)
ND
mg/kg
0.091
0.011
1
11/15/19 11:02
11/15/19 19:51
78-93-3
n-Butylbenzene
ND
mg/kg
0.0046
0.0026
1
11/15/19 11:02
11/15/19 19:51
104-51-8
sec-Butylbenzene
0.032
mg/kg
0.0046
0.0019
1
11/15/19 11:02
11/15/19 19:51
135-98-8
tert-Butyl benzene
ND
mg/kg
0.0046
0.0015
1
11/15/19 11:02
11/15/19 19:51
98-06-6
Carbon tetrachloride
ND
mg/kg
0.0046
0.00087
1
11/15/19 11:02
11/15/19 19:51
56-23-5
Chlorobenzene
ND
mg/kg
0.0046
0.00088
1
11/15/19 11:02
11/15/19 19:51
108-90-7
Chloroethane
ND
mg/kg
0.0091
0.0019
1
11/15/19 11:02
11/15/19 19:51
75-00-3
Chloroform
ND
mg/kg
0.0046
0.00097
1
11/15/19 11:02
11/15/19 19:51
67-66-3
Chloromethane
ND
mg/kg
0.0091
0.0030
1
11/15/19 11:02
11/15/19 19:51
74-87-3
2-Chlorotoluene
ND
mg/kg
0.0046
0.0014
1
11/15/19 11:02
11/15/19 19:51
95-49-8
4-Chlorotoluene
ND
mg/kg
0.0046
0.0014
1
11/15/19 11:02
11/15/19 19:51
106-43-4
1,2-Dibromo-3-chloropropane
ND
mg/kg
0.0046
0.0023
1
11/15/19 11:02
11/15/19 19:51
96-12-8
Dibromochloromethane
ND
mg/kg
0.0046
0.0023
1
11/15/19 11:02
11/15/19 19:51
124-48-1
1,2-Dibromoethane (EDB)
ND
mg/kg
0.0046
0.0010
1
11/15/19 11:02
11/15/19 19:51
106-93-4
Dibromomethane
ND
mg/kg
0.0046
0.0014
1
11/15/19 11:02
11/15/19 19:51
74-95-3
1,2-Dichlorobenzene
ND
mg/kg
0.0046
0.0016
1
11/15/19 11:02
11/15/19 19:51
95-50-1
1,3-Dichlorobenzene
ND
mg/kg
0.0046
0.0016
1
11/15/19 11:02
11/15/19 19:51
541-73-1
1,4-Dichlorobenzene
ND
mg/kg
0.0046
0.0016
1
11/15/19 11:02
11/15/19 19:51
106-46-7
Dichlorodifluoromethane
ND
mg/kg
0.0091
0.0037
1
11/15/19 11:02
11/15/19 19:51
75-71-8
1,1-Dichloroethane
ND
mg/kg
0.0046
0.00067
1
11/15/19 11:02
11/15/19 19:51
75-34-3
REPORT OF LABORATORY ANALYSIS
SO
SO
vl
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ANALYTICAL RESULTS
Project: CCR-003
Pace Project No.: 92453047
Sample: S13-2 (6-8) Lab ID: 92453047002 Collected: 11/07/19 14:55 Received: 11/08/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
1,2-Dichloroethane
ND
mg/kg
0.0046
0.00091
1
11/15/19 11:02
11/15/19 19:51
107-06-2
1,1-Dichloroethene
ND
mg/kg
0.0046
0.0011
1
11/15/19 11:02
11/15/19 19:51
75-35-4
cis-1,2-Dichloroethene
ND
mg/kg
0.0046
0.00079
1
11/15/19 11:02
11/15/19 19:51
156-59-2
trans-1,2-Dichloroethene
ND
mg/kg
0.0046
0.00089
1
11/15/19 11:02
11/15/19 19:51
156-60-5
1,2-Dichloropropane
ND
mg/kg
0.0046
0.0017
1
11/15/19 11:02
11/15/19 19:51
78-87-5
1,3-Dichloropropane
ND
mg/kg
0.0046
0.0017
1
11/15/19 11:02
11/15/19 19:51
142-28-9
2,2-Dichloropropane
ND
mg/kg
0.0046
0.00045
1
11/15/19 11:02
11/15/19 19:51
594-20-7
1,1-Dichloropropene
ND
mg/kg
0.0046
0.0019
1
11/15/19 11:02
11/15/19 19:51
563-58-6
cis-1,3-Dichloropropene
ND
mg/kg
0.0046
0.0021
1
11/15/19 11:02
11/15/19 19:51
10061-01-5
trans- 1,3-Dichloropropene
ND
mg/kg
0.0046
0.00080
1
11/15/19 11:02
11/15/19 19:51
10061-02-6
Diisopropyl ether
ND
mg/kg
0.0046
0.0026
1
11/15/19 11:02
11/15/19 19:51
108-20-3
Ethylbenzene
0.0020J
mg/kg
0.0046
0.00097
1
11/15/19 11:02
11/15/19 19:51
100-41-4
Hexachloro-1,3-butadiene
ND
mg/kg
0.0046
0.0023
1
11/15/19 11:02
11/15/19 19:51
87-68-3
2-Hexanone
ND
mg/kg
0.046
0.0047
1
11/15/19 11:02
11/15/19 19:51
591-78-6
Isopropylbenzene (Cumene)
0.012
mg/kg
0.0046
0.0013
1
11/15/19 11:02
11/15/19 19:51
98-82-8
p-Isopropyltoluene
0.056
mg/kg
0.0046
0.0022
1
11/15/19 11:02
11/15/19 19:51
99-87-6
Methylene Chloride
ND
mg/kg
0.018
0.0054
1
11/15/19 11:02
11/15/19 19:51
75-09-2
4-Methyl-2-pentanone (MIBK)
0.023J
mg/kg
0.046
0.0034
1
11/15/19 11:02
11/15/19 19:51
108-10-1
Methyl-tert-butyl ether
ND
mg/kg
0.0046
0.0026
1
11/15/19 11:02
11/15/19 19:51
1634-04-4
Naphthalene
9.0
mg/kg
0.46
0.39
100
11/15/19 11:02
11/18/1914:33
91-20-3
n-Propylbenzene
ND
mg/kg
0.0046
0.0015
1
11/15/19 11:02
11/15/19 19:51
103-65-1
Styrene
ND
mg/kg
0.0046
0.0013
1
11/15/19 11:02
11/15/19 19:51
100-42-5
1,1,1,2-Tetrachloroethane
ND
mg/kg
0.0046
0.0011
1
11/15/19 11:02
11/15/19 19:51
630-20-6
1,1,2,2-Tetrachloroethane
ND
mg/kg
0.0046
0.0016
1
11/15/19 11:02
11/15/19 19:51
79-34-5
Tetrachloroethene
ND
mg/kg
0.0046
0.0014
1
11/15/19 11:02
11/15/19 19:51
127-18-4
Toluene
ND
mg/kg
0.0046
0.0015
1
11/15/19 11:02
11/15/19 19:51
108-88-3
1,2,3-Trichlorobenzene
ND
mg/kg
0.0046
0.0033
1
11/15/19 11:02
11/15/19 19:51
87-61-6
1,2,4-Trichlorobenzene
ND
mg/kg
0.0046
0.0024
1
11/15/19 11:02
11/15/19 19:51
120-82-1
1,1,1-Trichloroethane
ND
mg/kg
0.0046
0.00079
1
11/15/19 11:02
11/15/19 19:51
71-55-6
1,1,2-Trichloroethane
ND
mg/kg
0.0046
0.0010
1
11/15/19 11:02
11/15/19 19:51
79-00-5
Trichloroethene
ND
mg/kg
0.0046
0.0012
1
11/15/19 11:02
11/15/19 19:51
79-01-6
Trichlorofluoromethane
ND
mg/kg
0.0046
0.0011
1
11/15/19 11:02
11/15/19 19:51
75-69-4
1,2,3-Trichloropropane
0.0041J
mg/kg
0.0046
0.0015
1
11/15/19 11:02
11/15/19 19:51
96-18-4
1,2,4-Trimethylbenzene
7.3
mg/kg
0.46
0.18
100
11/15/19 11:02
11/18/1914:33
95-63-6
1,3,5-Trimethylbenzene
0.17
mg/kg
0.0046
0.0015
1
11/15/19 11:02
11/15/19 19:51
108-67-8
Vinyl acetate
ND
mg/kg
0.046
0.015
1
11/15/19 11:02
11/15/19 19:51
108-05-4
Vinyl chloride
ND
mg/kg
0.0091
0.0017
1
11/15/19 11:02
11/15/19 19:51
75-01-4
Xylene (Total)
ND
mg/kg
0.0091
0.0032
1
11/15/19 11:02
11/15/19 19:51
1330-20-7
m&p-Xylene
0.0079J
mg/kg
0.0091
0.0022
1
11/15/19 11:02
11/15/19 19:51
179601-23-1
o-Xylene
ND
mg/kg
0.0046
0.0011
1
11/15/19 11:02
11/15/19 19:51
95-47-6
Surrogates
Toluene-d8 (S)
122
%
70-130
1
11/15/19 11:02
11/15/19 19:51
2037-26-5
4-Bromofluorobenzene (S)
110
%
70-130
1
11/15/19 11:02
11/15/19 19:51
460-00-4
1,2-Dichloroethane-d4 (S)
75
%
70-132
1
11/15/19 11:02
11/15/19 19:51
17060-07-0
REPORT OF LABORATORY ANALYSIS
IK
IK
v1
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Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 34

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Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: CCR-003
Pace Project No.: 92453047
Sample: S13-2 (6-8) Lab ID: 92453047002 Collected: 11/07/19 14:55 Received: 11/08/19 09:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Report
Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 18.5 % 0.10 0.10 1 11/08/19 18:16
Date: 02/13/2020 01:20 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 10 of 34

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CCR-003
Pace Project No.: 92453047
QC Batch: 508638 Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 5030E Analysis Description: Gasoline Range Organics
Associated Lab Samples: 92453047001, 92453047002
METHOD BLANK: 2730445 Matrix: Solid
Associated Lab Samples: 92453047001, 92453047002
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Gas Range Organics (C6-C10) mg/kg ND 6.0 1.1 11/09/19 16:07
4-Bromofluorobenzene (S) % 94 63-130 11/09/19 16:07
LABORATORY CONTROL SAMPLE:
2730446
Spike
LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
50
53.2
106
70-130
4-Bromofluorobenzene (S)
%
86
63-130
MATRIX SPIKE SAMPLE:
2730448
92452978012
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND
52.3
62.8
119
40-155
4-Bromofluorobenzene (S)
%
95
63-130
SAMPLE DUPLICATE: 2730447
92452978011
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND
ND
30
4-Bromofluorobenzene (S)
%
97
92
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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9800 Kincey Ave. Suite 100
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[phone]
QUALITY CONTROL DATA
Project: CCR-003
Pace Project No.: 92453047
QC Batch: 509289 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Soil
Associated Lab Samples: 92453047002
METHOD BLANK: 2733199
Associated Lab Samples: 92453047002
Parameter
Aliphatic (C05-008)
Aliphatic (C09-C12)
Aromatic (C09-C10)
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
Matrix: Solid
Units
Blank
Result
Reporting
Limit
MDL Analyzed Qualifiers
mg/kg
ND
2.5
2.5 11/13/1914:58 N2
mg/kg
ND
2.5
2.5 11/13/1914:58 N2
mg/kg
ND
2.5
2.5 11/13/1914:58 N2
%
93
70-130
11/13/1914:58
%
94
70-130
11/13/1914:58
LABORATORY CONTROL SAMPLE & LCSD:
2733200
2733201
Spike
LCS LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-CO8)
mg/kg
14.9
13.5 13.6
91
91
70-130 0 25 N2
Aliphatic (C09-C12)
mg/kg
14.9
14.9 15.1
100
101
30-130 1 25 N2
Aromatic (C09-C10)
mg/kg
5
5.0 5.0
100
100
70-130 0 25 N2
4-Bromofluorobenzene (FID) (S)
%
97
100
70-130
4-Bromofluorobenzene (PID) (S)
%
97
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 34

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[phone]
QUALITY CONTROL DATA
Project: CCR-003
Pace Project No.: 92453047
QC Batch: 509746 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A Analysis Description: 8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92453047002
METHOD BLANK: 2735631
Associated Lab Samples: 92453047002
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.0050
0.0012
11/15/19 10:37
1,1,1-Trichloroethane
mg/kg
ND
0.0050
0.00087
11/15/19 10:37
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.0050
0.0017
11/15/19 10:37
1,1,2-Trichloroethane
mg/kg
ND
0.0050
0.0011
11/15/19 10:37
1,1-Dichloroethane
mg/kg
ND
0.0050
0.00074
11/15/19 10:37
1,1-Dichloroethene
mg/kg
ND
0.0050
0.0012
11/15/19 10:37
1,1-Dichloropropene
mg/kg
ND
0.0050
0.0021
11/15/19 10:37
1,2,3-Trichlorobenzene
mg/kg
ND
0.0050
0.0036
11/15/19 10:37
1,2,3-Trichloropropane
mg/kg
ND
0.0050
0.0017
11/15/19 10:37
1,2,4-Trichlorobenzene
mg/kg
ND
0.0050
0.0026
11/15/19 10:37
1,2,4-Trimethylbenzene
mg/kg
ND
0.0050
0.0020
11/15/19 10:37
1,2-Dibromo-3-chloropropane
mg/kg
ND
0.0050
0.0025
11/15/19 10:37
1,2-Dibromoethane (EDB)
mg/kg
ND
0.0050
0.0011
11/15/19 10:37
1,2-Dichlorobenzene
mg/kg
ND
0.0050
0.0018
11/15/19 10:37
1,2-Dichloroethane
mg/kg
ND
0.0050
0.0010
11/15/19 10:37
1,2-Dichloropropane
mg/kg
ND
0.0050
0.0019
11/15/19 10:37
1,3,5-Trimethylbenzene
mg/kg
ND
0.0050
0.0017
11/15/19 10:37
1,3-Dichlorobenzene
mg/kg
ND
0.0050
0.0018
11/15/19 10:37
1,3-Dichloropropane
mg/kg
ND
0.0050
0.0019
11/15/19 10:37
1,4-Dichlorobenzene
mg/kg
ND
0.0050
0.0017
11/15/19 10:37
2,2-Dichloropropane
mg/kg
ND
0.0050
0.00049
11/15/19 10:37
2-Butanone (MEK)
mg/kg
ND
0.10
0.012
11/15/19 10:37
2-Chlorotoluene
mg/kg
ND
0.0050
0.0015
11/15/19 10:37
2-Hexanone
mg/kg
ND
0.050
0.0052
11/15/19 10:37
4-Chlorotoluene
mg/kg
ND
0.0050
0.0015
11/15/19 10:37
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
0.050
0.0037
11/15/19 10:37
Acetone
mg/kg
ND
0.10
0.0094
11/15/19 10:37
Benzene
mg/kg
ND
0.0050
0.00090
11/15/19 10:37
Bromobenzene
mg/kg
ND
0.0050
0.0014
11/15/19 10:37
Bromochloromethane
mg/kg
ND
0.0050
0.0012
11/15/19 10:37
Bromodichloromethane
mg/kg
ND
0.0050
0.00098
11/15/19 10:37
Bromoform
mg/kg
ND
0.0050
0.0024
11/15/19 10:37
Bromomethane
mg/kg
ND
0.010
0.0024
11/15/19 10:37
Carbon tetrachloride
mg/kg
ND
0.0050
0.00096
11/15/19 10:37
Chlorobenzene
mg/kg
ND
0.0050
0.00097
11/15/19 10:37
Chloroethane
mg/kg
ND
0.010
0.0021
11/15/19 10:37
Chloroform
mg/kg
ND
0.0050
0.0011
11/15/19 10:37
Chloromethane
mg/kg
ND
0.010
0.0033
11/15/19 10:37
cis-1,2-Dichloroethene
mg/kg
ND
0.0050
0.00087
11/15/19 10:37
cis-1,3-Dichloropropene
mg/kg
ND
0.0050
0.0023
11/15/19 10:37
Dibromochloromethane
mg/kg
ND
0.0050
0.0025
11/15/19 10:37
ILI
v1
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 34

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Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CCR-003
Pace Project No.: 92453047
METHOD BLANK: 2735631
Associated Lab Samples: 92453047002
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
Dibromomethane
mg/kg
ND
0.0050
0.0015
11/15/19 10:37
Dichlorodifluoromethane
mg/kg
ND
0.010
0.0041
11/15/19 10:37
Diisopropyl ether
mg/kg
ND
0.0050
0.0029
11/15/19 10:37
Ethylbenzene
mg/kg
ND
0.0050
0.0011
11/15/19 10:37
Hexachloro-1,3-butadiene
mg/kg
ND
0.0050
0.0025
11/15/19 10:37
Isopropylbenzene (Cumene)
mg/kg
ND
0.0050
0.0014
11/15/19 10:37
m&p-Xylene
mg/kg
ND
0.010
0.0024
11/15/19 10:37
Methyl-tert-butyl ether
mg/kg
ND
0.0050
0.0029
11/15/19 10:37
Methylene Chloride
mg/kg
ND
0.020
0.0059
11/15/19 10:37
n-Butylbenzene
mg/kg
ND
0.0050
0.0028
11/15/19 10:37
n-Propylbenzene
mg/kg
ND
0.0050
0.0017
11/15/19 10:37
Naphthalene
mg/kg
ND
0.0050
0.0042
11/15/19 10:37
o-Xylene
mg/kg
ND
0.0050
0.0012
11/15/19 10:37
p-Isopropyltoluene
mg/kg
ND
0.0050
0.0024
11/15/19 10:37
sec-Butylbenzene
mg/kg
ND
0.0050
0.0021
11/15/19 10:37
Styrene
mg/kg
ND
0.0050
0.0015
11/15/19 10:37
tert-Butyl benzene
mg/kg
ND
0.0050
0.0017
11/15/19 10:37
Tetrachloroethene
mg/kg
ND
0.0050
0.0016
11/15/19 10:37
Toluene
mg/kg
ND
0.0050
0.0016
11/15/19 10:37
trans-1,2-Dichloroethene
mg/kg
ND
0.0050
0.00098
11/15/19 10:37
trans- 1,3-Dichloropropene
mg/kg
ND
0.0050
0.00088
11/15/19 10:37
Trichloroethene
mg/kg
ND
0.0050
0.0013
11/15/19 10:37
Trichlorofluoromethane
mg/kg
ND
0.0050
0.0012
11/15/19 10:37
Vinyl acetate
mg/kg
ND
0.050
0.016
11/15/19 10:37
Vinyl chloride
mg/kg
ND
0.010
0.0019
11/15/19 10:37
Xylene (Total)
mg/kg
ND
0.010
0.0035
11/15/19 10:37
1,2-Dichloroethane-d4 (S)
%
75
70-132
11/15/19 10:37
4-Bromofluorobenzene (S)
%
95
70-130
11/15/19 10:37
Toluene-d8 (S)
%
116
70-130
11/15/19 10:37
IK
v1
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2735632
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
0.05
0.047
95
70-130
1,1,1-Trichloroethane
mg/kg
0.05
0.060
119
70-130
1,1,2,2-Tetrachloroethane
mg/kg
0.05
0.045
89
55-130
1,1,2-Trichloroethane
mg/kg
0.05
0.051
102
70-130
1,1-Dichloroethane
mg/kg
0.05
0.052
104
68-130
1,1-Dichloroethene
mg/kg
0.05
0.057
113
70-130
1,1-Dichloropropene
mg/kg
0.05
0.053
107
70-130IK
1,2,3-Trichlorobenzene
mg/kg
0.05
0.053
105
70-130
1,2,3-Trichloropropane
mg/kg
0.05
0.048
96
70-130
1,2,4-Trichlorobenzene
mg/kg
0.05
0.052
105
70-130
1,2,4-Trimethylbenzene
mg/kg
0.05
0.048
95
69-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CCR-003
Pace Project No.: 92453047
LABORATORY CONTROL SAMPLE:
Parameter
2735632
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2-Dibromo-3-chloropropane
mg/kg
0.05
0.046
92
57-141
1,2-Dibromoethane (EDB)
mg/kg
0.05
0.051
102
70-130
1,2-Dichlorobenzene
mg/kg
0.05
0.047
94
70-130
1,2-Dichloroethane
mg/kg
0.05
0.048
95
70-130
1,2-Dichloropropane
mg/kg
0.05
0.052
103
70-130
1,3,5-Trimethylbenzene
mg/kg
0.05
0.049
97
70-130
1,3-Dichlorobenzene
mg/kg
0.05
0.051
102
70-130
1,3-Dichloropropane
mg/kg
0.05
0.044
88
70-130
1,4-Dichlorobenzene
mg/kg
0.05
0.049
98
70-130
2,2-Dichloropropane
mg/kg
0.05
0.054
108
70-130
2-Butanone (MEK)
mg/kg
0.1
0.10
105
60-130
2-Chlorotoluene
mg/kg
0.05
0.049
97
70-130
2-Hexanone
mg/kg
0.1
0.093
93
70-132
4-Chlorotoluene
mg/kg
0.05
0.048
96
70-130
4-Methyl-2-pentanone (MIBK)
mg/kg
0.1
0.093
93
69-130
Acetone
mg/kg
0.1
0.10
104
49-148
Benzene
mg/kg
0.05
0.056
111
70-130
Bromobenzene
mg/kg
0.05
0.052
103
70-130
Bromochloromethane
mg/kg
0.05
0.055
109
70-130
Bromodichloromethane
mg/kg
0.05
0.050
99
70-130
Bromoform
mg/kg
0.05
0.046
92
68-136
Bromomethane
mg/kg
0.05
0.050
100
60-140
Carbon tetrachloride
mg/kg
0.05
0.062
124
70-130 v1
Chlorobenzene
mg/kg
0.05
0.051
101
70-130
Chloroethane
mg/kg
0.05
0.055
110
51-147
Chloroform
mg/kg
0.05
0.043
87
70-130
Chloromethane
mg/kg
0.05
0.051
103
48-130
cis-1,2-Dichloroethene
mg/kg
0.05
0.056
111
70-130
cis-1,3-Dichloropropene
mg/kg
0.05
0.053
105
70-130
Dibromochloromethane
mg/kg
0.05
0.041
82
70-130
Dibromomethane
mg/kg
0.05
0.049
98
70-130
Dichlorodifluoromethane
mg/kg
0.05
0.057
114
49-130
Diisopropyl ether
mg/kg
0.05
0.052
104
66-130
Ethylbenzene
mg/kg
0.05
0.048
95
70-130
Hexachloro-1,3-butadiene
mg/kg
0.05
0.051
102
70-130
Isopropylbenzene (Cumene)
mg/kg
0.05
0.052
104
70-130
m&p-Xylene
mg/kg
0.1
0.097
97
70-130
Methyl-tert-butyl ether
mg/kg
0.05
0.049
97
70-130 IK
Methylene Chloride
mg/kg
0.05
0.049
98
50-137
n-Butylbenzene
mg/kg
0.05
0.050
101
70-130
n-Propylbenzene
mg/kg
0.05
0.049
99
70-130
Naphthalene
mg/kg
0.05
0.052
104
70-131
o-Xylene
mg/kg
0.05
0.051
102
70-130
p-Isopropyltoluene
mg/kg
0.05
0.050
99
70-130
sec-Butylbenzene
mg/kg
0.05
0.052
105
70-130
Styrene
mg/kg
0.05
0.048
95
70-130
tert-Butyl benzene
mg/kg
0.05
0.043
86
69-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CCR-003
Pace Project No.: 92453047
LABORATORY CONTROL SAMPLE:
Parameter
2735632
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Tetrachloroethene
mg/kg
0.05
0.057
113
56-130
Toluene
mg/kg
0.05
0.050
100
70-130
trans-1,2-Dichloroethene
mg/kg
0.05
0.052
105
70-130
trans- 1,3-Dichloropropene
mg/kg
0.05
0.047
93
70-130
Trichloroethene
mg/kg
0.05
0.057
114
70-141
Trichlorofluoromethane
mg/kg
0.05
0.056
112
67-130
Vinyl acetate
mg/kg
0.1
0.086
86
10-136
Vinyl chloride
mg/kg
0.05
0.062
124
67-130 v1
Xylene (Total)
mg/kg
0.15
0.15
99
70-130
1,2-Dichloroethane-d4 (S)
%
99
70-132
4-Bromofluorobenzene (S)
%
93
70-130
Toluene-d8 (S)
%
95
70-130
MATRIX SPIKE SAMPLE:
Parameter
2735634
Units
92453338003
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
ND
0.063
0.059
94
52-133
1,1,1-Trichloroethane
mg/kg
ND
0.063
0.075
119
49-137
1,1,2,2-Tetrachloroethane
mg/kg
ND
0.063
0.052
82
39-150
1,1,2-Trichloroethane
mg/kg
ND
0.063
0.054
86
48-140
1,1-Dichloroethane
mg/kg
ND
0.063
0.071
113
46-135
1,1-Dichloroethene
mg/kg
ND
0.063
0.082
130
38-149
1,1-Dichloropropene
mg/kg
ND
0.063
0.084
134
41-1401K
1,2,3-Trichlorobenzene
mg/kg
ND
0.063
0.041
66
10-158
1,2,3-Trichloropropane
mg/kg
ND
0.063
0.053
84
33-157
1,2,4-Trichlorobenzene
mg/kg
ND
0.063
0.049
78
10-155
1,2,4-Trimethylbenzene
mg/kg
ND
0.063
0.077
122
24-154
1,2-Dibromo-3-chloropropane
mg/kg
ND
0.063
0.051
80
33-158
1,2-Dibromoethane (EDB)
mg/kg
ND
0.063
0.048
76
40-136
1,2-Dichlorobenzene
mg/kg
ND
0.063
0.068
108
27-146
1,2-Dichloroethane
mg/kg
ND
0.063
0.051
81
49-140
1,2-Dichloropropane
mg/kg
ND
0.063
0.066
105
44-143
1,3,5-Trimethylbenzene
mg/kg
ND
0.063
0.083
132
40-144
1,3-Dichlorobenzene
mg/kg
ND
0.063
0.077
122
33-140
1,3-Dichloropropane
mg/kg
ND
0.063
0.051
80
47-147
1,4-Dichlorobenzene
mg/kg
ND
0.063
0.073
116
35-139
2,2-Dichloropropane
mg/kg
ND
0.063
0.073
115
41-140
2-Butanone (MEK)
mg/kg
ND
0.13
0.12J
32
10-181
2-Chlorotoluene
mg/kg
ND
0.063
0.085
134
38-147
2-Hexanone
mg/kg
ND
0.13
0.101
81
18-169
4-Chlorotoluene
mg/kg
ND
0.063
0.079
126
36-145
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
0.13
0.111
86
16-175
Acetone
mg/kg
354 ug/kg
0.13
0.37
10
10-200
Benzene
mg/kg
ND
0.063
0.073
117
46-136
Bromobenzene
mg/kg
ND
0.063
0.079
126
38-149
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CCR-003
Pace Project No.: 92453047
MATRIX SPIKE SAMPLE:
2735634
92453338003
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Bromochloromethane
mg/kg
ND
0.063
0.061
97
44-142
Bromodichloromethane
mg/kg
ND
0.063
0.056
89
41-140
Bromoform
mg/kg
ND
0.063
0.048
76
34-145
Bromomethane
mg/kg
ND
0.063
0.065
103
14-162
Carbon tetrachloride
mg/kg
ND
0.063
0.070
111
44-141
Chlorobenzene
mg/kg
ND
0.063
0.073
115
39-141
Chloroethane
mg/kg
ND
0.063
0.082
131
10-182
Chloroform
mg/kg
ND
0.063
0.054
85
45-140
Chloromethane
mg/kg
ND
0.063
0.073
116
19-149
cis-1,2-Dichloroethene
mg/kg
ND
0.063
0.069
109
38-150
cis-1,3-Dichloropropene
mg/kg
ND
0.063
0.055
87
30-144
Dibromochloromethane
mg/kg
ND
0.063
0.053
84
36-145
Dibromomethane
mg/kg
ND
0.063
0.056
89
41-145
Dichlorodifluoromethane
mg/kg
ND
0.063
0.085
134
16-146
Diisopropyl ether
mg/kg
ND
0.063
0.060
95
41-143
Ethylbenzene
mg/kg
ND
0.063
0.080
127
35-144
Hexachloro-1,3-butadiene
mg/kg
ND
0.063
0.047
74
10-160
Isopropylbenzene (Cumene)
mg/kg
ND
0.063
0.091
145
30-152
m&p-Xylene
mg/kg
ND
0.13
0.16
130
33-145
Methyl-tert-butyl ether
mg/kg
ND
0.063
0.068
107
49-140 IK
Methylene Chloride
mg/kg
ND
0.063
0.086
136
10-174
n-Butylbenzene
mg/kg
ND
0.063
0.077
122
10-160
n-Propylbenzene
mg/kg
ND
0.063
0.094
149
24-159
Naphthalene
mg/kg
ND
0.063
0.043
69
10-171
o-Xylene
mg/kg
ND
0.063
0.078
124
31-150
p-Isopropyltoluene
mg/kg
ND
0.063
0.085
134
21-154
sec-Butylbenzene
mg/kg
ND
0.063
0.089
141
19-159
Styrene
mg/kg
ND
0.063
0.068
108
15-152
tert-Butyl benzene
mg/kg
ND
0.063
0.076
120
31-141
Tetrachloroethene
mg/kg
ND
0.063
0.083
132
19-141
Toluene
mg/kg
ND
0.063
0.077
122
31-146
trans-1,2-Dichloroethene
mg/kg
ND
0.063
0.080
127
28-157
trans- 1,3-Dichloropropene
mg/kg
ND
0.063
0.048
76
25-146
Trichloroethene
mg/kg
ND
0.063
0.072
115
34-149
Trichlorofluoromethane
mg/kg
ND
0.063
0.10
158
10-167
Vinyl acetate
mg/kg
ND
0.13
0.061J
48
10-200
Vinyl chloride
mg/kg
ND
0.063
0.094
149
36-155
Xylene (Total)
mg/kg
ND
0.19
0.24
128
29-148
1,2-Dichloroethane-d4 (S)
%
87
70-132
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8(S)
%
102
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CCR-003
Pace Project No.: 92453047
SAMPLE DUPLICATE: 2735633
Parameter
Units
92453338002
Result
Dup
Result RPD
Max
RPD Qualifiers
1,1,1,2-Tetrachloroethane
mg/kg
ND
ND
30
1,1,1-Trichloroethane
mg/kg
ND
ND
30
1,1,2,2-Tetrachloroethane
mg/kg
ND
ND
30
1,1,2-Trichloroethane
mg/kg
ND
ND
30
1,1-Dichloroethane
mg/kg
ND
ND
30
1,1-Dichloroethene
mg/kg
ND
ND
30
1,1-Dichloropropene
mg/kg
ND
ND
301K
1,2,3-Trichlorobenzene
mg/kg
ND
ND
30
1,2,3-Trichloropropane
mg/kg
ND
ND
30
1,2,4-Trichlorobenzene
mg/kg
ND
ND
30
1,2,4-Trimethylbenzene
mg/kg
ND
ND
30
1,2-Dibromo-3-chloropropane
mg/kg
ND
ND
30
1,2-Dibromoethane (EDB)
mg/kg
ND
ND
30
1,2-Dichlorobenzene
mg/kg
ND
ND
30
1,2-Dichloroethane
mg/kg
ND
ND
30
1,2-Dichloropropane
mg/kg
ND
ND
30
1,3,5-Trimethylbenzene
mg/kg
ND
ND
30
1,3-Dichlorobenzene
mg/kg
ND
ND
30
1,3-Dichloropropane
mg/kg
ND
ND
30
1,4-Dichlorobenzene
mg/kg
ND
ND
30
2,2-Dichloropropane
mg/kg
ND
ND
30
2-Butanone (MEK)
mg/kg
ND
0.043J
30
2-Chlorotoluene
mg/kg
ND
ND
30
2-Hexanone
mg/kg
ND
ND
30
4-Chlorotoluene
mg/kg
ND
ND
30
4-Methyl-2-pentanone (MIBK)
mg/kg
ND
ND
30
Acetone
mg/kg
ND
0.20J
30
Benzene
mg/kg
ND
ND
30
Bromobenzene
mg/kg
ND
ND
30
Bromochloromethane
mg/kg
ND
ND
30
Bromodichloromethane
mg/kg
ND
ND
30
Bromoform
mg/kg
ND
ND
30
Bromomethane
mg/kg
ND
ND
30
Carbon tetrachloride
mg/kg
ND
ND
30 v1
Chlorobenzene
mg/kg
ND
ND
30
Chloroethane
mg/kg
ND
ND
30
Chloroform
mg/kg
ND
ND
30
Chloromethane
mg/kg
ND
ND
30
cis-1,2-Dichloroethene
mg/kg
ND
ND
30
cis-1,3-Dichloropropene
mg/kg
ND
ND
30
Dibromochloromethane
mg/kg
ND
ND
30
Dibromomethane
mg/kg
ND
ND
30
Dichlorodifluoromethane
mg/kg
ND
ND
30
Diisopropyl ether
mg/kg
ND
ND
30
Ethylbenzene
mg/kg
ND
ND
30
Hexachloro-1,3-butadiene
mg/kg
ND
ND
30
Isopropylbenzene (Cumene)
mg/kg
ND
ND
30
Results presented on this page are in the units
indicated by the "Units" column except where an alternate unit
is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CCR-003
Pace Project No.: 92453047
SAMPLE DUPLICATE: 2735633
Parameter
Units
92453338002
Result
Dup
Result
m&p-Xylene
mg/kg
ND
ND
Methyl-tert-butyl ether
mg/kg
ND
ND
Methylene Chloride
mg/kg
ND
ND
n-Butylbenzene
mg/kg
ND
ND
n-Propylbenzene
mg/kg
ND
ND
Naphthalene
mg/kg
ND
ND
o-Xylene
mg/kg
ND
ND
p-Isopropyltoluene
mg/kg
ND
ND
sec-Butylbenzene
mg/kg
ND
ND
Styrene
mg/kg
ND
ND
tert-Butyl benzene
mg/kg
ND
ND
Tetrachloroethene
mg/kg
ND
ND
Toluene
mg/kg
ND
ND
trans-1,2-Dichloroethene
mg/kg
ND
ND
trans- 1,3-Dichloropropene
mg/kg
ND
ND
Trichloroethene
mg/kg
ND
ND
Trichlorofluoromethane
mg/kg
ND
ND
Vinyl acetate
mg/kg
ND
ND
Vinyl chloride
mg/kg
ND
ND
Xylene (Total)
mg/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
79
81
4-Bromofluorobenzene (S)
%
95
96
Toluene-d8(S)
%
107
104
Max
RPD RPD Qualifiers
30
30 I K
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30 v1
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CCR-003
Pace Project No.: 92453047
QC Batch: 508576 Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 3546 Analysis Description: 8015 Solid GCSV
Associated Lab Samples: 92453047001, 92453047002
METHOD BLANK: 2730261 Matrix: Solid
Associated Lab Samples: 92453047001, 92453047002
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Diesel Range Organics(C10-C28) mg/kg ND 5.0 2.3 11/11/19 10:52
n-Pentacosane (S) % 77 33-129 11/11/19 10:52
LABORATORY CONTROL SAMPLE:
2730262
Spike
LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
66.2
46.0
69
43-130
n-Pentacosane (S)
%
66
33-129
MATRIX SPIKE SAMPLE:
2730266
92453048001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
3040 76.4
3630
767
10-130 M1
n-Pentacosane(S)
%
110
33-129
SAMPLE DUPLICATE: 2730267
92453047001
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
ND
ND
30
n-Pentacosane (S)
%
54
61
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CCR-003
Pace Project No.: 92453047
QC Batch: 510287 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave
Associated Lab Samples: 92453047002
METHOD BLANK: 2738066
Associated Lab Samples: 92453047002
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
1,2,4-Trichlorobenzene
mg/kg
ND
0.33
0.076
11/19/19 14:19
1,2-Dichlorobenzene
mg/kg
ND
0.33
0.071
11/19/19 14:19
1,3-Dichlorobenzene
mg/kg
ND
0.33
0.074
11/19/19 14:19
1,4-Dichlorobenzene
mg/kg
ND
0.33
0.073
11/19/19 14:19
1-Methylnaphthalene
mg/kg
ND
0.33
0.088
11/19/19 14:19
2,2'-Oxybis(1-chloropropane)
mg/kg
ND
0.33
0.092
11/19/19 14:19
2,4,5-Trichlorophenol
mg/kg
ND
0.33
0.086
11/19/19 14:19
2,4,6-Trichlorophenol
mg/kg
ND
0.33
0.083
11/19/19 14:19
2,4-Dichlorophenol
mg/kg
ND
0.33
0.11
11/19/19 14:19
2,4-Dimethylphenol
mg/kg
ND
0.33
0.082
11/19/19 14:19
2,4-Dinitrophenol
mg/kg
ND
1.6
1.1
11/19/19 14:19
2,4-Dinitrotoluene
mg/kg
ND
0.33
0.087
11/19/19 14:19
2,6-Dinitrotoluene
mg/kg
ND
0.33
0.086
11/19/19 14:19
2-Chloronaphthalene
mg/kg
ND
0.33
0.074
11/19/19 14:19
2-Chlorophenol
mg/kg
ND
0.33
0.077
11/19/19 14:19
2-Methylnaphthalene
mg/kg
ND
0.33
0.084
11/19/19 14:19
2-Methylphenol(o-Cresol)
mg/kg
ND
0.33
0.073
11/19/19 14:19
2-Nitroaniline
mg/kg
ND
1.6
0.17
11/19/19 14:19
2-Nitrophenol
mg/kg
ND
0.33
0.10
11/19/19 14:19
3&4-Methyl phenol (m&p Cresol)
mg/kg
ND
0.33
0.083
11/19/19 14:19
3,3'-Dichlorobenzidine
mg/kg
ND
1.6
0.23
11/19/19 14:19
3-Nitroaniline
mg/kg
ND
1.6
0.18
11/19/19 14:19
4,6-Dinitro-2-methyl phenol
mg/kg
ND
0.66
0.53
11/19/19 14:19
4-Bromophenylphenyl ether
mg/kg
ND
0.33
0.087
11/19/19 14:19
4-ChIoro-3-methyl phenol
mg/kg
ND
0.66
0.20
11/19/19 14:19
4-Chloroaniline
mg/kg
ND
1.6
0.20
11/19/19 14:19
4-Chlorophenylphenyl ether
mg/kg
ND
0.33
0.086
11/19/19 14:19
4-Nitroaniline
mg/kg
ND
0.66
0.16
11/19/19 14:19
4-Nitrophenol
mg/kg
ND
1.6
0.53
11/19/19 14:19
Acenaphthene
mg/kg
ND
0.33
0.085
11/19/19 14:19
Acenaphthylene
mg/kg
ND
0.33
0.078
11/19/19 14:19
Aniline
mg/kg
ND
0.33
0.074
11/19/19 14:19
Anthracene
mg/kg
ND
0.33
0.086
11/19/19 14:19
Benzo(a)anthracene
mg/kg
ND
0.33
0.10
11/19/19 14:19
Benzo(a)pyrene
mg/kg
ND
0.33
0.14
11/19/19 14:19
Benzo(b)fluoranthene
mg/kg
ND
0.33
0.13
11/19/19 14:19
Benzo(g,h,i)perylene
mg/kg
ND
0.33
0.13
11/19/19 14:19
Benzo(k)fluoranthene
mg/kg
ND
0.33
0.14
11/19/19 14:19
Benzoic Acid
mg/kg
ND
1.6
0.36
11/19/19 14:19
Benzyl alcohol
mg/kg
ND
0.66
0.18
11/19/19 14:19
bis(2-Chloroethoxy)methane
mg/kg
ND
0.33
0.088
11/19/19 14:19
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CCR-003
Pace Project No.: 92453047
METHOD BLANK: 2738066
Associated Lab Samples: 92453047002
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
bis(2-Chloroethyl) ether
mg/kg
ND
0.33
0.070
11/19/19 14:19
bis(2-Ethylhexyl)phthalate
mg/kg
ND
0.33
0.11
11/19/19 14:19
Butylbenzylphthalate
mg/kg
ND
0.33
0.088
11/19/19 14:19
Chrysene
mg/kg
ND
0.33
0.096
11/19/19 14:19
Di-n-butylphthalate
mg/kg
ND
0.33
0.081
11/19/19 14:19
Di-n-octylphthalate
mg/kg
ND
0.33
0.19
11/19/19 14:19
Dibenz(a,h)anthracene
mg/kg
ND
0.33
0.13
11/19/19 14:19
Dibenzofuran
mg/kg
ND
0.33
0.082
11/19/19 14:19
Diethylphthalate
mg/kg
ND
0.33
0.072
11/19/19 14:19
Dimethylphthalate
mg/kg
ND
0.33
0.075
11/19/19 14:19
Fluoranthene
mg/kg
ND
0.33
0.10
11/19/19 14:19
Fluorene
mg/kg
ND
0.33
0.088
11/19/19 14:19
Hexachloro-1,3-butadiene
mg/kg
ND
0.33
0.080
11/19/19 14:19
Hexachlorobenzene
mg/kg
ND
0.33
0.084
11/19/19 14:19
Hexachlorocyclopentadiene
mg/kg
ND
0.33
0.13
11/19/19 14:19
Hexachloroethane
mg/kg
ND
0.33
0.075
11/19/19 14:19
Indeno(1,2,3-cd)pyrene
mg/kg
ND
0.33
0.15
11/19/19 14:19
Isophorone
mg/kg
ND
0.33
0.072
11/19/19 14:19
N-Nitroso-di-n-propylamine
mg/kg
ND
0.33
0.092
11/19/19 14:19
N-Nitrosodimethylamine
mg/kg
ND
0.33
0.093
11/19/19 14:19
N-Nitrosodiphenylamine
mg/kg
ND
0.33
0.084
11/19/19 14:19
Naphthalene
mg/kg
ND
0.33
0.079
11/19/19 14:19
Nitrobenzene
mg/kg
ND
0.33
0.079
11/19/19 14:19
Pentachlorophenol
mg/kg
ND
1.6
0.15
11/19/19 14:19
Phenanthrene
mg/kg
ND
0.33
0.083
11/19/19 14:19
Phenol
mg/kg
ND
0.33
0.079
11/19/19 14:19
Pyrene
mg/kg
ND
0.33
0.091
11/19/19 14:19
Pyridine
mg/kg
ND
0.33
0.084
11/19/19 14:19
2,4,6-Tribromophenol (S)
%
88
27-110
11/19/19 14:19
2-Fluorobiphenyl (S)
%
80
30-110
11/19/19 14:19
2-Fluorophenol (S)
%
76
13-110
11/19/19 14:19
Nitrobenzene-d5 (S)
%
77
23-110
11/19/19 14:19
Phenol-d6 (S)
%
76
22-110
11/19/19 14:19
Terphenyl-d14 (S)
%
84
28-110
11/19/19 14:19
Qualifiers
LABORATORY CONTROL SAMPLE:
2738067
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
mg/kg
1.7
1.2
75
52-130
1,2-Dichlorobenzene
mg/kg
1.7
1.3
76
51-130
1,3-Dichlorobenzene
mg/kg
1.7
1.2
75
50-130
1,4-Dichlorobenzene
mg/kg
1.7
1.2
73
49-130
1-Methylnaphthalene
mg/kg
1.7
1.2
74
55-130
2,2'-Oxybis(1-chloropropane)
mg/kg
1.7
1.1
69
30-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CCR-003
Pace Project No.: 92453047
LABORATORY CONTROL SAMPLE:
Parameter
2738067
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,4,5-Trichlorophenol
mg/kg
1.7
1.2
73
55-130
2,4,6-Trichlorophenol
mg/kg
1.7
1.3
76
57-130
2,4-Dichlorophenol
mg/kg
1.7
1.3
75
56-130
2,4-Dimethylphenol
mg/kg
1.7
1.3
79
51-130
2,4-Dinitrophenol
mg/kg
8.3
6.4
77
27-133
2,4-Dinitrotoluene
mg/kg
1.7
1.4
83
61-130
2,6-Dinitrotoluene
mg/kg
1.7
1.4
84
60-130
2-Chloronaphthalene
mg/kg
1.7
1.3
75
52-130
2-Chlorophenol
mg/kg
1.7
1.3
77
54-130
2-Methylnaphthalene
mg/kg
1.7
1.3
75
54-130
2-Methylphenol(o-Cresol)
mg/kg
1.7
1.2
74
51-130
2-Nitroaniline
mg/kg
3.3
2.8
83
51-130
2-Nitrophenol
mg/kg
1.7
1.2
70
49-130
3&4-Methyl phenol (m&p Cresol)
mg/kg
1.7
1.2
71
11-163
3,3'-Dichlorobenzidine
mg/kg
3.3
2.3
69
10-132
3-Nitroaniline
mg/kg
3.3
2.4
72
55-130
4,6-Dinitro-2-methyl phenol
mg/kg
3.3
3.1
92
47-142
4-Bromophenylphenyl ether
mg/kg
1.7
1.4
82
59-130
4-ChIoro-3-methyl phenol
mg/kg
3.3
2.5
76
55-130
4-Chloroaniline
mg/kg
3.3
2.5
76
54-130
4-Chlorophenylphenyl ether
mg/kg
1.7
1.3
77
58-130
4-Nitroaniline
mg/kg
3.3
2.6
79
54-130
4-Nitrophenol
mg/kg
8.3
6.5
78
48-130
Acenaphthene
mg/kg
1.7
1.4
83
60-130
Acenaphthylene
mg/kg
1.7
1.4
86
60-130
Aniline
mg/kg
1.7
1.2
71
43-130
Anthracene
mg/kg
1.7
1.5
91
63-130
Benzo(a)anthracene
mg/kg
1.7
1.5
88
59-130
Benzo(a)pyrene
mg/kg
1.7
1.5
90
57-130
Benzo(b)fluoranthene
mg/kg
1.7
1.5
87
54-130
Benzo(g,h,i)perylene
mg/kg
1.7
1.6
93
59-130
Benzo(k)fluoranthene
mg/kg
1.7
1.5
90
54-130
Benzoic Acid
mg/kg
8.3
6.0
72
19-130
Benzyl alcohol
mg/kg
3.3
2.5
75
50-130
bis(2-Chloroethoxy)methane
mg/kg
1.7
1.3
75
54-130
bis(2-Chloroethyl) ether
mg/kg
1.7
1.3
79
48-130
bis(2-Ethylhexyl)phthalate
mg/kg
1.7
1.3
81
45-134
Butylbenzylphthalate
mg/kg
1.7
1.3
80
46-138
Chrysene
mg/kg
1.7
1.4
82
58-130
Di-n-butylphthalate
mg/kg
1.7
1.3
79
60-130
Di-n-octylphthalate
mg/kg
1.7
1.4
82
53-130
Dibenz(a,h)anthracene
mg/kg
1.7
1.5
88
59-130
Dibenzofuran
mg/kg
1.7
1.3
77
60-130
Diethylphthalate
mg/kg
1.7
1.3
77
60-130
Dimethylphthalate
mg/kg
1.7
1.3
79
60-130
Fluoranthene
mg/kg
1.7
1.4
84
65-130
Fluorene
mg/kg
1.7
1.4
82
63-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CCR-003
Pace Project No.: 92453047
LABORATORY CONTROL SAMPLE:
2738067
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Hexachloro-1,3-butadiene
mg/kg
1.7
1.2
72
46-130
Hexachlorobenzene
mg/kg
1.7
1.3
80
58-130
Hexachlorocyclopentadiene
mg/kg
1.7
1.4
83
23-130
Hexachloroethane
mg/kg
1.7
1.2
74
47-130
Indeno(1,2,3-cd)pyrene
mg/kg
1.7
1.5
91
60-130
Isophorone
mg/kg
1.7
1.2
74
49-130
N-Nitroso-di-n-propylamine
mg/kg
1.7
1.3
76
47-130
N-Nitrosodimethylamine
mg/kg
1.7
1.2
70
45-130
N-Nitrosodiphenylamine
mg/kg
1.7
1.3
79
59-130
Naphthalene
mg/kg
1.7
1.3
78
55-130
Nitrobenzene
mg/kg
1.7
1.2
73
49-130
Pentachlorophenol
mg/kg
3.3
2.7
81
10-132
Phenanthrene
mg/kg
1.7
1.4
86
62-130
Phenol
mg/kg
1.7
1.3
76
46-130
Pyrene
mg/kg
1.7
1.5
91
53-130
Pyridine
mg/kg
1.7
1.1
65
37-130
2,4,6-Tribromophenol (S)
%
84
27-110
2-Fluorobiphenyl (S)
%
72
30-110
2-Fluorophenol(S)
%
73
13-110
Nitrobenzene-d5 (S)
%
70
23-110
Phenol-d6 (S)
%
73
22-110
Terphenyl-d14 (S)
%
73
28-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2738068
2738069
MS
MSD
92453047002
Spike
Spike
MS
MSD
MS MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD
RPD Qual
1,2,4-Trichoorobenzene
mg/kg
ND
2.1
2.1
2.2
2.2
106
105
18-130
2
30
1,2-Dichlorobenzene
mg/kg
ND
2.1
2.1
1.5
1.4
70
69
14-130
3
30
1,3-Dichlorobenzene
mg/kg
ND
2.1
2.1
1.5
1.4
71
70
12-130
3
30
1,4-Dichlorobenzene
mg/kg
ND
2.1
2.1
1.5
1.4
70
69
10-130
3
30
1-Methyl naphthalene
mg/kg
8.0
2.1
2.1
8.2
9.2
9
58
12-130
12
30 M1
2,2'-Oxybis(1-
mg/kg
ND
2.1
2.1
1.3
1.2
60
57
10-130
6
30
chloropropane)
2,4,5-Trichlorophenol
mg/kg
ND
2.1
2.1
1.4
1.5
68
70
13-130
1
30
2,4,6-Trichlorophenol
mg/kg
ND
2.1
2.1
1.8
1.9
85
89
17-130
4
30
2,4-Dichlorophenol
mg/kg
ND
2.1
2.1
2.3
2.3
111
111
10-130
2
30
2,4-Dimethylphenol
mg/kg
ND
2.1
2.1
2.3
2.4
109
115
10-130
3
30
2,4-Dinitrophenol
mg/kg
ND
10.6
10.4
5.1
4.9
49
47
10-130
5
30
2,4-Dinitrotoluene
mg/kg
ND
2.1
2.1
1.9
1.7
88
84
24-130
7
30
2,6-Dinitrotoluene
mg/kg
ND
2.1
2.1
2.1
2.3
100
109
23-130
7
30
2-Chloronaphthalene
mg/kg
ND
2.1
2.1
0.86
0.60
41
29
19-130
35
30 R1
2-Chlorophenol
mg/kg
ND
2.1
2.1
1.7
1.7
80
81
10-130
0
30
2-Methyl naphthalene
mg/kg
11.3
2.1
2.1
10.5
11.4
-42
2
18-130
9
30 M1
2-Methyl phenol(o-Cresol)
mg/kg
ND
2.1
2.1
1.5
1.5
70
70
10-130
1
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC.
Page 24 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CCR-003
Pace Project No.: 92453047
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2738068
2738069
MS
MSD
92453047002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
2-Nitroaniline
mg/kg
ND
4.2
4.2
3.2
3.2
77
77
17-130
1
30
2-Nitrophenol
mg/kg
ND
2.1
2.1
2.9
2.9
138
140
10-130
0
30 M1
3&4-Methylphenol(m&p
mg/kg
ND
2.1
2.1
1.7
1.6
80
78
10-130
4
30
Cresol)
3,3'-Dichlorobenzidine
mg/kg
ND
4.2
4.2
2.9
3.1
68
74
10-130
6
30
3-Nitroaniline
mg/kg
ND
4.2
4.2
2.2
1.91
52
46
24-130
30
4,6-Dinitro-2-methylphenol
mg/kg
ND
4.2
4.2
3.9
4.0
93
97
10-152
3
30
4-Bromophenylphenyl ether
mg/kg
ND
2.1
2.1
1.6
1.6
74
77
29-130
2
30
4-Chloro-3-methylphenol
mg/kg
ND
4.2
4.2
4.7
4.8
110
115
17-130
2
30
4-Chloroaniline
mg/kg
ND
4.2
4.2
4.0
4.2
95
102
14-130
5
30
4-Chlorophenylphenyl ether
mg/kg
ND
2.1
2.1
1.6
1.6
76
76
25-130
1
30
4-Nitroaniline
mg/kg
ND
4.2
4.2
3.5
3.7
83
89
22-130
5
30
4-Nitrophenol
mg/kg
ND
10.6
10.4
9.4
10.3
90
99
10-130
8
30
Acenaphthene
mg/kg
ND
2.1
2.1
1.7
1.8
83
85
20-130
2
30
Acenaphthylene
mg/kg
ND
2.1
2.1
1.7
1.6
78
79
25-130
1
30
Aniline
mg/kg
ND
2.1
2.1
1.6
1.6
78
79
10-130
0
30
Anthracene
mg/kg
ND
2.1
2.1
1.8
1.8
85
86
29-130
0
30
Benzo(a)anth race ne
mg/kg
ND
2.1
2.1
1.6
1.7
77
80
19-130
3
30
Benzo(a)pyrene
mg/kg
ND
2.1
2.1
1.7
1.7
81
83
12-130
1
30
Benzo(b)fluoranthene
mg/kg
ND
2.1
2.1
1.6
1.6
78
78
14-130
1
30
Benzo(g,h,i)perylene
mg/kg
ND
2.1
2.1
1.8
1.9
85
92
10-130
7
30
Benzo(k)fluoranthene
mg/kg
ND
2.1
2.1
1.7
1.7
80
80
14-130
1
30
Benzoic Acid
mg/kg
ND
10.6
10.4
ND
ND
0
0
10-130
30 M1
Benzyl alcohol
mg/kg
ND
4.2
4.2
3.0
3.0
70
71
13-130
0
30
bis(2-
mg/kg
ND
2.1
2.1
2.2
2.2
104
104
16-130
1
30
Chloroethoxy)methane
bis(2-Chloroethyl) ether
mg/kg
ND
2.1
2.1
1.6
1.7
78
80
11-130
2
30
bis(2- Ethyl hexyl)phthalate
mg/kg
ND
2.1
2.1
1.8
1.8
86
87
21-130
0
30
Butylbenzylphthalate
mg/kg
ND
2.1
2.1
1.6
1.6
78
79
23-130
0
30
Chrysene
mg/kg
ND
2.1
2.1
1.5
1.6
73
75
22-130
1
30
Di-n-butylphthalate
mg/kg
ND
2.1
2.1
1.7
1.7
80
80
30-130
1
30
Di-n-octylphthalate
mg/kg
ND
2.1
2.1
1.8
1.9
86
89
23-142
2
30
Dibenz(a,h)anthracene
mg/kg
ND
2.1
2.1
1.8
1.9
85
92
10-130
6
30
Dibenzofuran
mg/kg
0.36J
2.1
2.1
1.6
1.6
60
62
24-130
1
30
Diethylphthalate
mg/kg
ND
2.1
2.1
1.4
1.4
67
67
26-130
1
30
Dimethylphthalate
mg/kg
ND
2.1
2.1
1.4
1.3
66
63
22-130
7
30
Fluoranthene
mg/kg
ND
2.1
2.1
1.7
1.7
80
80
33-130
0
30
Fluorene
mg/kg
0.34J
2.1
2.1
1.9
1.9
72
76
22-130
3
30
Hexachloro-1,3-butadiene
mg/kg
ND
2.1
2.1
2.2
2.2
102
104
13-130
1
30
Hexachlorobenzene
mg/kg
ND
2.1
2.1
1.6
1.7
77
80
29-130
2
30
Hexachlorocyclopentadiene
mg/kg
ND
2.1
2.1
1.3
1.2
60
58
10-130
4
30
Hexachloroethane
mg/kg
ND
2.1
2.1
1.9
1.9
92
93
10-130
0
30
Indeno(1,2,3-cd)pyrene
mg/kg
ND
2.1
2.1
1.8
1.9
85
92
10-130
6
30
Isophorone
mg/kg
ND
2.1
2.1
2.7
2.7
129
131
13-130
1
30 M1
N-Nitroso-di-n-propylamine
mg/kg
ND
2.1
2.1
2.0
2.2
95
105
12-130
8
30
N-Nitrosodimethyl amine
mg/kg
ND
2.1
2.1
1.6
1.5
74
74
11-130
1
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC.
Page 25 of 34

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CCR-003
Pace Project No.: 92453047
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2738068
2738069
MS
MSD
92453047002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
N-Nitrosodiphenylamine
mg/kg
ND
2.1
2.1
1.9
2.2
91
106
15-130
14
30
Naphthalene
mg/kg
1.6
2.1
2.1
2.9
2.5
60
44
15-130
13
30
Nitrobenzene
mg/kg
ND
2.1
2.1
2.6
2.6
123
124
12-130
1
30
Pentachlorophenol
mg/kg
ND
4.2
4.2
3.3
3.5
78
84
10-130
5
30
Phenanthrene
mg/kg
ND
2.1
2.1
1.8
1.8
80
82
27-130
1
30
Phenol
mg/kg
ND
2.1
2.1
1.6
1.6
76
77
10-130
0
30
Pyrene
mg/kg
ND
2.1
2.1
1.7
1.7
81
82
19-130
0
30
Pyridine
mg/kg
ND
2.1
2.1
1.4
1.4
67
68
10-130
1
30
2,4,6-Tribromophenol (S)
%
78
90
27-110
2-Fluorobiphenyl (S)
%
62
66
30-110
2-Fluorophenol(S)
%
71
76
13-110
Nitrobenzene-d5 (S)
%
122
137
23-110
SO
Phenol-d6 (S)
%
69
75
22-110
Terphenyl-d14 (S)
%
63
68
28-110
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC.
Page 26 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CCR-003
Pace Project No.: 92453047
QC Batch: 509971 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Soil
Associated Lab Samples: 92453047002
METHOD BLANK: 2736776
Matrix:
Solid
Associated Lab Samples: 92453047002
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
Aliphatic (C09-C18)
mg/kg
ND
9.9
9.9 11/18/19 16:07 N2
Aliphatic (C19-C36)
mg/kg
ND
9.9
9.9 11/18/19 16:07 N2
Aromatic (C11-C22)
mg/kg
ND
9.9
9.9 11/18/19 16:07 N2
2-Bromonaphthalene (S)
%
98
40-140
11/18/19 16:07
2-Fluorobiphenyl (S)
%
104
40-140
11/18/19 16:07
Nonatriacontane (S)
%
71
40-140
11/18/19 16:07
o-Terphenyl (S)
%
82
40-140
11/18/19 16:07
LABORATORY CONTROL SAMPLE & LCSD:
2736777
2736778
Spike
LCS LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C09-C18)
mg/kg
10
ND ND
46
50
40-140 50 N2
Aliphatic (C19-C36)
mg/kg
13.4
ND ND
70
68
40-140 50 N2
Aromatic (C11-C22)
mg/kg
28.4
22.9 21.5
80
75
40-140 6 50 N2
2-Bromonaphthalene (S)
%
81
81
40-140
2-Fluorobiphenyl (S)
%
98
107
40-140
Nonatriacontane (S)
%
75
66
40-140
o-Terphenyl(S)
%
93
85
40-140
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2736779
2736780
MS
MSD
92453338001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
Aliphatic (C09-C18)
mg/kg
ND
30.4
31.1
ND
ND
23
32
40-140
50 M1,N2
Aliphatic (C19-C36)
mg/kg
ND
40.6
41.2
ND
ND
58
63
40-140
50 N2
Aromatic (C11-C22)
mg/kg
ND
86.4
87.6
49.1
63.7
54
70
40-140
26 50 N2
2-Bromonaphthalene (S)
%
45
40
40-140
2-Fluorobiphenyl (S)
%
87
99
40-140
Nonatriacontane (S)
%
61
66
40-140
o-Terphenyl(S)
%
63
76
40-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC.
Page 27 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CCR-003
Pace Project No.: 92453047
QC Batch: 508535 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92453047001
SAMPLE DUPLICATE: 2729896
92452974001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 26.1 27.1 4 25
SAMPLE DUPLICATE: 2730171
92453047001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 16.9 18.4 8 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: CCR-003
Pace Project No.: 92453047
QC Batch: 508568 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92453047002
SAMPLE DUPLICATE: 2730207
92453056001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 19.9 17.0 15 25
SAMPLE DUPLICATE: 2730208
92453055003 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 13.0 13.2 2 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 34

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: CCR-003
Pace Project No.: 92453047
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
SO Surrogate recovery outside laboratory control limits.
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 02/13/2020 01:20 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 34

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
CCR-003
92453047
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92453047001
SB-1 (6-8)
EPA 3546
508576
EPA 8015C Modified
508695
92453047002
SB-2 (6-8)
EPA 3546
508576
EPA 8015C Modified
508695
92453047002
SB-2 (6-8)
MADEP EPH
509971
MADEP EPH
510288
92453047001
SB-1 (6-8)
EPA 5030B
508638
EPA 8015C Modified
508751
92453047002
SB-2 (6-8)
EPA 5030B
508638
EPA 8015C Modified
508751
92453047002
SB-2 (6-8)
MADEP VPH
509289
MADEP VPH
509845
92453047002
SB-2 (6-8)
EPA 3546
510287
EPA 8270E
510411
92453047002
SB-2 (6-8)
EPA 5035A
509746
EPA 8260D
509770
92453047001
SB-1 (6-8)
ASTM D2974-87
508535
92453047002
SB-2 (6-8)
ASTM D2974-87
508568
Date: 02/13/2020 01:20 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 31 of 34

Document Name:
Document Revised: February 7, 2018
m
aceAnalytical
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
J
F-CAR-CS-033-Rev,06
Pace Carolinas Quality Office
Laboratory receiving samples: .
Asheville ❑ Eden❑ Greenwood ❑ Huntersville [� Raleigh❑ Mechanicsville[]
Sample Condition Client Name: PTojectis WO# : 92453047
Upon ReceiptIII
Courier: ❑Fefd Ex ❑UPS ❑LISPS ❑Client II `�� III III I Ill I■1
❑ Commercial EgRace ❑other: 92453047
Custody Seal Present? ❑Yes [9fdo seals Intact? ❑Yes 0190 /
Date/Initials Person ExaminingContents: /r %�`�r
Packing Material: ❑Bubble Wrap bole Bags -]None❑ Other
Thermometer: Type of Ice: QWet ❑Blue
❑iR Gun ID: 92TQ58
Cooler Temp (°C): �_ Cprrection Factor: Add/Subtract (°C) 0.00C
Cooler Temp Corrected ('t:):
USDA Regulated Soil (Ef N/A, water sample)
Did samples arigi ate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
mv— , n'_
Biological Tissue Frozen?
❑Kane ❑Yes ❑No [DN/A
Temp AolA be above freezing to VC
❑5arnAes out of temp criteria. Samples on ice, cooling process
has hegin
Did samples originate from a foreign source tintern on ally,
Inrlur ine Haviaii and Puerto Ricol? nyeS I A0
comments/Discrepancy:
Chain of Custody Present?
fes
❑No
❑N/A
1.
Samples Arrived within Hold Time?
Yes
[]No
[]N/A
2.
Short Hold Time Analysis 1<72 hr.)?
Oyes
[01/yo
N/A
3.
Rush Turn Around Time Rem?_
[]Yes
❑l o
❑N/A
4.
Sufficient Volume?
Yes
❑No
[]N/A
5.
Correct Containe:s Used?
YY
❑No
[]N/A
6.
-Pace Containers Used?
M es
(:]No
❑N/A
Containers Intact?
QYes
❑No
❑N A
7.
Dissolved analysis: Samples Field Filtered?
❑Y
❑No
©N/A
B.
Sample Labels Match COC?
❑Ves
❑No
❑N/A
9.
-Includes Date/Time/ID/Analysis Matrix:_
/
Headspace in VOA Vials (>5-Gmm)?
❑
-Yes r:o
j9
10.
Trip Blank Present?
❑Yes
[tNn
®/A
11.
Trip Blank Custody Seals Present?
❑Yes
❑Nn
NIA
COMMENTS/SAMPLE DISCREPANCY
Field Data Required? ❑Yes ONO
Lot ID of split containers:
CLIENT NOTIFICATIONIRESOLUTION
Person contacted: Date/T-ime:
Project Manager SCURF Review: < Date: !
r / �
c
Project Manager SRF Review: Date:
Page 32 of 34

Document Name:
Document Revised: February 7, 2018
aeeAnalytica!
5arn le Condition Upon Recelpt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS.033-Rev.06
Pace Carolinas Quality Office
*Check mark top half of box If pH and/or dechlorination Is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project f Wa# : 92453447
PM: KRG Due [late: 11/15/19
CLIENT: 92—Hart Hick
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot d
Note: Whenever there is a discrepancy affecting North Carolina compllance samples, a copy of this form will ue sent lothe Norm Larojina utnrvn Certn�cation UTrice ti.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 33 of 34

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Page 34 of 34

Beverly, Trudy
From: Beverly, Trudy
Sent: Thursday, February 13, 2020 3:14 PM
To: Bo Cappleman
Cc: Joe McLean
Subject: RE: [External] UST Release Reporting Form - Area 15 Retail Property
Received. Thanks Bo.
Have a great day,
Trudy
Trudy Beverly, L.G.
D- I E Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
Q,
Dr" 'el UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy. B everlykncdenn gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: ht_pt s://deg.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: https:Hdeg.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httos://dea.nc. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-ais-mans
File Review Procedures:
hitps://deq.ne. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
bit.ps://deq.nc.gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
https:Hfiles.nc. gov/ncdegfWaste%2OManagement/D WM/UST/Corrective%2OAction/Electronic%2ODocument%2OSubmittal%2OMemo%20UPdate.pdf
https:Hfiles.nc.gov/ncdeq/Waste%20Management/DWM/ JST/Corrective%2OAction/UST°/a20file%20names%20for°/`2OLaserfiche.docx
From: Bo Cappleman [mailto:[e-mail]]
Sent: Thursday, February 13, 2020 2:41 PM
To: Beverly, Trudy <[e-mail]>
Cc: Joe McLean <[e-mail]>
Subject: RE: [External] UST Release Reporting Form - Area 15 Retail Property
External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
[e-mail]
Hi Trudy,
Please see the attached Phase II ESA report which documents the soil sampling at the closed -in -place heating oil
UST. Let me know if you have any questions, and we look forward to hearing from you regarding next steps to close out
this incident.
Regards,
Bo Cappleman, PG, Due Diligence Manager

Hart & Hickman, PC
2923 S Tryon Street, Suite 100 • Charlotte, NC 28203
Direct: 704-887-4623 • Mobile: [phone]
www.harthickman.com 10 0
From: Beverly, Trudy <[e-mail]>
Sent: Monday, February 3, 2020 6:32 AM
To: Bo Cappleman <[e-mail]>
Cc: Joe McLean <[e-mail]>
Subject: RE: [External] UST Release Reporting Form - Area 15 Retail Property
Thank you for the information.
Have a great day,
Trudy
D_ � E
�'• riles
mentJl 4ua ��
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy. B everly(d) ncdenn gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: hops://deq.nc.gov/about/divisions/waste-manaaement/ust
Branch's Above Ground Storage Tanks Website Address: hgps://deg.nc.gov/about/divisions/waste-management/ust/ast-prosram
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://deo.nc. eov/about/divisions/waste-management/waste-management-rules-data/waste-management-eis-mans
File Review Procedures:
https://deq.nc. gov/about/divisions/waste-management/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
hi�2s://deg.nc.gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
https:Hfiles.nc. gov/ncdeq/Waste%20Management/D WM/UST/Corrective%2OAction/Electronic%2ODocument%2OSubmittal%2OMemo%2OUpdate.pdf
htips:Hfiles.nc. gov/ncdeq/Waste%20Management/D WM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: Bo Cappleman [mailto:[e-mail]]
Sent: Saturday, February 1, 2020 4:38 PM
To: Beverly, Trudy <[e-mail]>
Cc: Joe McLean <[e-mail]>
Subject: [External] UST Release Reporting Form - Area 15 Retail Property
External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to
ort.s am nc. ov
Hi Trudy,
Please see the attached 24-Hour Release & UST Leak Reporting Form for a heating oil release that was identified at the
Area 15 retail property located at 510-516 E. 15t" Street and 1138 N. Caldwell Street in Charlotte. Property ownership
was recently transferred to CCRP Area 15 LLC, which intends to seek risk -based regulatory closure through filing an
alternate Notice of Residual Petroleum that will establish a soil restriction area and prohibit groundwater use at the

property. Municipal water supply is available in the site area, and no water supply wells have been identified within at
least 200 ft of the heating oil UST.
A formal report that documents the soil sampling is forthcoming. Please let me know if you have any questions or see
any issues with the plan to achieve regulatory closure.
Regards,
Bo Cappleman, PG, Due Diligence Manager
Hart & Hickman, PC
2923 S Tryon Street, Suite 100 • Charlotte, NC 28203
Direct: 704-887-4623 • Mobile: [phone]
www.harthickman.com I U 0