21015_BrownfieldsAssessmentReport_Five Points Gateway_11-13-19

TABLE OF CONTENTS

A. SITE INFORMATION ..................................................................................................................... 1
B. INTRODUCTION ............................................................................................................................ 2
C. DATA GAPS .................................................................................................................................... 3
D. ENVIRONMENTAL ASSESSMENT ACTIVITIES ....................................................................... 3
E. QUALITY ASSURANCE/QUALITY CONTROL ......................................................................... 5
F. INVESTIGATIVE DERIVED WASTE MANAGEMENT ............................................................. 6
G. 1,500-FOOT RECEPTOR SURVEY ............................................................................................... 6
H. DISCUSSION OF RESULTS ........................................................................................................... 6
I. LIMITATIONS ................................................................................................................................. 7

FIGURES
Figure 1: Site Location Map
Figure 2: Site Map
Figure 3: Potentiometric Surface Map (8/15/19)
Figure 4: Ground Water Quality Map (8/15/19)
Figure 5: Site Vicinity Map

TABLES

Table 1: Summary of Soil Stockpile Sampling Results
Table 2: Well Construction and Gauging Information
Table 3: Summary of Ground Water Sampling Results

APPENDICES

Appendix A: Soil Boring Logs/Monitoring Well Records
Appendix B: Disposal Manifest
Appendix C: Laboratory Analytical Reports – Soil and Ground Water Samples
Appendix D: Brownfields Property Receptor Survey Form
Appendix E: Zoning Map – City of Monroe

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A. SITE INFORMATION

 Site Name: Five Points Gateway Redevelopment
 Location: 320-322 E. Franklin Street
Monroe, Union County, NC
 Land Use: Currently vacant
 Property Owner: City of Monroe
P.O. Box 69
Monroe NC 28111
704-282-4500
 Prospective Developer: City of Monroe
P.O. Box 69
Monroe NC 28111
704-282-4500
 Consultant: Resolve Environmental Services, PLLC (Resolve)
500 Devonport Drive
Matthews, North Carolina 28104
[phone]

 Latitude: 34.982450° North Longitude: 80.547100° West

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B. INTRODUCTION

1. Site
The subject site is an approximately 1.79-acre aggregate parcel, identified as Union County Parcel ID
09231234 (0.434-acre) and 09231233 (1.356-acres) (subject property), currently vacant land in Monroe,
Union County, North Carolina. A Site Location Map is included as Figure 1.

Petroleum and chlorinated compounds, in addition to metals, have been documented in soil and/or ground
water samples previously collected during assessment of the property. The City of Monroe (the Prospective
Developer or PD) has been deemed eligible to obtain a Brownfields agreement with the North Carolina
Department of Environmental Quality (NCDEQ). Brian Borne, primary contact of the PD, has engaged
Resolve Environmental Services, PLLC (Resolve) as the consultant of record for the site. The purpose of
this Brownfields Assessment was to gather additional site information prior to site development in order to
further characterize potential environmental concerns so that such concerns can be resolved during the
Brownfields process.
Based on the June 25, 2019 data gap meeting with the NCDEQ Brownfields Program project manager, the
following data gaps needed to be addressed during the current assessment: (1) conduct a ground water
assessment to determine if vapor intrusion is an issue on a portion of the property. The ground water
assessment include the installation and sampling of three North Carolina Type II monitoring wells at the
site to determine current ground water quality and determine ground water flow direction, (2) complete a
1,500’ radius receptor survey, and (3) update the property survey plat.
2. Background
Based upon the historical information obtained and reviewed during Phase I ESA activities conducted by
Resolve at the site in October 2016, the former presence of gasoline underground storage tanks (USTs) was
identified as recognized environmental condition (REC) on the 320 E. Franklin Street parcel. The USTs
were reportedly present circa 1947-1951. Auto repairs also reportedly took place on the site circa 1947
until an unknown date. In addition, several potential environmental conditions (PECs) were identified on
adjacent properties during Phase I ESA activities including: (1) adjacent property to the west (302 E.
Franklin Street) operated as a gasoline filling station circa 1951-1969, (2) adjacent property to the northeast
(325 E. Franklin Street) operated as a gasoline filling station circa 1951-1976 and (3) adjacent property to
the north (329 E. Franklin Street) operated as a gasoline filling station from at least 1975 through 1989.

3

A Phase II ESA was conducted by Resolve at the site in October/November 2016 to determine if the soil
and ground water had been effected by onsite and/or off-site petroleum and/or auto repair operations. A
concentration of TCE that exceeded the North Carolina Department of Environmental Quality’s (NCDEQ)
Inactive Hazardous Sites Branch (IHSB) Preliminary Soils Remediation Goal (PSRG) was reported in the
soil sample collected from TMW-4-8’. Concentrations of arsenic and chromium that exceeded the PSRG
were detected in each of the soil samples, including the background sample. Concentrations of VOCs and
PAHs that exceeded the NCDEQ maximum allowable concentrations (MACs) and IHSB ground water
screening levels (GWSLs), if established, were reported in the ground water samples collected from TMW-
1 and TMW-3.
Concentrations of metals (arsenic, chromium, lead and/or mercury) that exceeded the MACs and/or GWSLs
(if established) were reported in TMW-1, TMW-2, TMW-3 and “background” sample TMW-5. The
concentrations of benzene, ethylbenzene xylenes, naphthalene, chloroform, 1,2 DCA, 1,2,4-
trimethylbenzene in samples collected from TMW-1 and TMW-3 also exceeded the NCDEQ’s vapor
intrusion screening levels. The concentration of mercury in samples TMW-1, TMW-2 and TMW-3 also
exceed the vapor screening levels.
C. DATA GAPS
Areas identified for further investigation at the subject site as addressed in Resolve’s NCDEQ-approved
work plan are listed below and the proposed sampling locations are shown on the attached Figure 2.

1) Ground water quality in previously sampled locations at the site to determine the potential for
vapor intrusion and ground water flow direction and,
2) 1,500-foot receptor survey/completion of the Brownfields Property Receptor Survey Form
D. ENVIRONMENTAL ASSESSMENT ACTIVITIES
1. Soil Assessment
Soil assessment activities were not included in the work plan or requested by the NCDEQ; however, during
site work on the adjacent property to the south/southwest (City of Monroe’s future “Science Center”),
suspected petroleum-contaminated soils were encountered during the installation of storm water drain
system. When responding to the City’s request to assess the soils, Resolve identified that a portion of the
storm sewer line excavation was located on the subject site. A composite soil sample from the stockpiled
soil from the trench excavation was collected by Resolve personnel on August 2, 2019. The composite soil
sample was submitted to a North Carolina certified laboratory for analyses of volatile organic compounds
(VOCs) by Method 8260, semi-volatile organic compounds (SVOCs) by Method 8270 and for RCRA

4

metals. Subsequently, on August 13, 2019, Resolve returned to the stockpile location, per the NCDEQ
Brownfields Program project manager’s request, to collect an additional grab stockpile sample. The
stockpile sample was submitted to a North Carolina certified laboratory for VOCs by 8260 only.

Concentrations of benzo(a)pyrene, benzo(a)anthracene, arsenic, barium and mercury that exceeded the
Federal EPA Protection of Ground Water Regional Screening Levels (RSLs) and/or NCDEQ’s Protection
of Ground Water Preliminary Soil Remediation Goals (PSRGs) were reported in the initial composite
sample collected on August 2, 2019. However, no detectable concentrations of Method 8260 compounds
were reported in the grab stockpile sample collected on August 13, 2019. A summary of soil analytical
results from stockpile sampling in included in Table 1. Based on the findings, the stockpile soil was
subsequently spread on site (see Figure 2).

2. Ground Water Assessment
Based on the comments made by the NCDEQ during the June 25, 2019 onsite meeting and follow-up e-
mail correspondence dated June 29, 2019, Resolve supervised the installation of three (3) North Carolina
Type II monitoring wells at the site on August 8, 2019. Monitoring well MW-1 was completed to a total
depth of 40 feet below grade level (BGL) with a 20-foot screened interval set to bracket the water table at
the time of installation. Monitoring wells MW-2 and MW-3 were each completed to a total depth of 30
feet, with 20-foot screened intervals set to bracket the water table at the time of installation. The wells
were developed subsequent to installation per the 15A NCAC 02C.0101 regulations. Well construction
details are summarized in Table 2. Monitoring well construction records and associated subsurface boring
logs are included in Appendix A. An updated site map showing monitoring well locations is included as
Figure 2.

Subsequent to well development, the newly installed monitoring wells at the site were gauged, purged and
sampled on August 15, 2019. Field parameters (dissolved oxygen, pH, conductivity, temperature and
turbidity) were measured and once readings became stable, a ground water sample was collected.
Stabilization was defined as three consecutive readings where temperature is within ± 10%, pH is within ±
0.1 SU, and conductivity is ± 5%. The ground water samples from each well were collected by personnel
wearing clean, nitrile glove and clean, disposable Teflon bailers.

The collected ground water samples were submitted to a North Carolina certified laboratory for analysis of
VOCs by Method 8260 and for SVOCs by Method 8270D. Concentrations of benzene and 1,2-DCA that
exceeded the NCDEQ ground water quality standard and/or the Federal EPA Regional maximum

5

contamination level (MCL) was reported in the ground water samples collected from MW-1 and MW-3.
None of the other estimated and/or detectable concentrations of requested method constituents reported in
any of the three ground water samples exceeded the standards. A Ground Water Quality Map is included
as Figure 4. Laboratory analytical results from ground water sampling activities conducted on August 15,
2019 are summarized in Table 3. Copies of laboratory analytical reports are included as Appendix C.

Drill cuttings, development and purge water from the monitoring well installation were containerized in
55-gallon drums and transported off site to a permitted disposal facilities. A disposal manifest has been
included as Appendix B.

The top-of-casing elevations of the monitoring wells were surveyed in order to determine the ground water
flow direction at the site. The depths to ground water in the monitoring wells were measured on August
15, 2019 ranged from 4.44 feet BGL to 9.20 feet BGL. The calculated ground water elevations ranged
from 96.34 feet in MW-3 to 93.05 feet in MW-1. Ground water flow direction across the site was generally
toward the north/northeast. A potentiometric surface map is included as Figure 3.

E. QUALITY ASSURANCE/QUALITY CONTROL
1. Monitoring Well Installation
All down-hole drilling equipment was pressure washed, scrubbed and rinsed prior to use and
between each monitoring well installation location.
2. Monitoring Well Sampling
Monitoring wells were developed using submersible pumps. Monitoring wells were subsequently
purged using a new, disposable Teflon bailer. New nitrile gloves will be worn by field personnel
during sampling activities and changed between sample locations. All field meters were be
properly calibrated and decontaminated prior to use and between sampling locations. Collected
samples will be placed directly into laboratory-supplied sample containers and immediately placed
on ice in a sample cooler. The samples were transported in sealed coolers to the laboratory. Proper
chain of custody procedures were maintained at all times.
3. Duplicates and Trip Blanks
To evaluate laboratory quality control and repeatability, one duplicate ground water sample was
collected from MW-1 and analyzed for VOCs, SVOCs and RCRA metals during the sampling
event and one trip blank sample (for VOCs) accompanied the samples during the sampling event.
Laboratory results for MW-1 and DUP-A showed generally the same compounds at similar

6

concentrations. No detectable concentrations of requested method constituents were reported in
the trip blank.
F. INVESTIGATIVE DERIVED WASTE MANAGEMENT
Soil cuttings from the installation of monitoring wells were be placed into labeled 55-gallon drums and
transported to a permitted disposal facility. Monitoring well development and purge water, as well as
equipment decontamination water was placed in labeled 55-gallon drums and transported to a permitted
disposal facility and properly disposed.
G. 1,500-FOOT RECEPTOR SURVEY
Resolve personnel conducted a reconnaissance and receptor survey of all properties within a radius of
1,500-feet of the site on August 15, 2019. The area of reconnaissance is located within a commercial area
of Monroe, North Carolina. The site is approximately 1.79-acres in size and formerly contained two (2)
structures; however, both have been demolished. Ground cover at this site is primarily paved (or broken
asphalt) with some grassy areas. A small area (approximately 200 square feet) near the southwestern corner
of the property is wooded. Currently, the area is not being used. The majority (80%) of the property ground
cover is capped with asphalt/concrete and was used as a parking lot. Approximately 20% of the property
covered with vegetation and is not being used. Less than 1% is wooded. Municipal water and sewer are
available. Overhead electrical and telephone service are also available to the property.

The site and all properties in the immediate vicinity in each direction are zoned by the Town of Monroe as
Central Business District. No private or municipal water supply wells were identified within 1,500 feet of
the site. No basements or subterranean structures were identified within 1,500 feet of the site during the
reconnaissance.

A 1,500-foot Radius Map showing property boundaries and other site and nearby features is included as
Figure 5. A completed copy of the Brownfields Property Receptor form is attached as Appendix D. An
individual zoning map showing the City of Monroe are included in Appendix E.
H. DISCUSSION OF RESULTS
 Stockpile samples (composite and grab) were collected from petroleum-affected soils discovered
at the site in August 2019. Based on the results, approval of the soil to be returned to the excavation
was granted by the NCDEQ. However, the location of the soils were to be documented for
inclusion in the Brownfields Agreement and Plat.
 Resolve personnel supervised the installation of three (3) North Carolina monitoring wells (MW-1
through MW-3) at the site on August 8, 2019. The measured depths to water ranged from 4.44 feet

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BGL to 9.20 feet BGL. Based on the ground water elevations ranging from 93.05 feet in MW-1 to
96.34 feet in MW-3, ground water flow across the site was generally toward the north/northeast.
 Ground water samples were collected from MW-1, MW-2 and MW-3 on August 15, 2019.
Concentrations of benzene and 1,2-DCA that exceeded the NCDEQ ground water quality standard
and/or the Federal MCL were reported in ground water samples collected from MW-1 and MW-3.
 Resolve personnel conducted a 1,500-foot receptor survey on August 15, 2019. No private water
supply wells were identified within a 1,500-foot radius of the site. The site is zoned by the City of
Monroe as Central Business District, as well as the adjacent properties in the immediate area of the
site.
 Based on the results discussed above, Resolve believes that all outstanding data gaps have been
filled and that no additional assessment is necessary to develop a Brownfields Agreement for the
site.

I. LIMITATIONS
This report has been prepared for the exclusive use of The City of Monroe and the NCDEQ for specific
application to the referenced site in Union County, North Carolina. The assessment was conducted based
on the scope of work and level of effort specified by the NCDEQ and with resources adequate only for that
scope of work. Our findings have been developed in accordance with generally accepted standards of
geology and hydrogeology practices in the State of North Carolina, available information, and our
professional judgment. No other warranty is expressed or implied.

The data that are presented in this report are indicative of conditions that existed at the precise locations
sampled and at the time the samples were collected. In addition, the data obtained from samples would be
interpreted as being meaningful with respect to parameters indicated in the laboratory report. No additional
information can logically be inferred from these data.

FIGURES

Copyright:© 2013 National Geographic Society, i-cubed
FIGURE 1SITE LOCATION MAPMONROE, UNION COUNTY,NORTH CAROLINA
PREPARED BY:RESOLVE ENVIRONMETAL SERVICES, PPLC.NOVEMBER 17, 2016
0 2,000 4,0001,000 Feet
SCALE: 1 INCH = 2,000 FEET
MAP CENTER LOCATIONLATITUDE: 34.982343° NLONGITUDE: 80.546820° W
`
322 E. Franklin St.
³`320 E. Franklin St.`113 W. Morgan St.
RESOLVEENVIRONMENTALSERVICES, PLLCFIGURE 2SITE MAPFIVE POINTS GATEWAY REDEVELOPMENTBROWNFIELDS PROJECT ID: 21050-17-090320-322 E. FRANKLIN STREET, MONROEUNION COUNTY, NCPROJECT NO: 5204
RESOLVEENVIRONMENTALSERVICES, PLLCFIGURE 3POTENTIOMETRIC SURFACE MAP (8/15/19)FIVE POINTS GATEWAY REDEVELOPMENTBROWNFIELDS PROJECT ID: 21050-17-090320-322 E. FRANKLIN STREET, MONROEUNION COUNTY, NCPROJECT NO: 5204
RESOLVEENVIRONMENTALSERVICES, PLLCFIGURE 4GROUND WATER QUALITY MAP (8/15/19)FIVE POINTS GATEWAY REDEVELOPMENTBROWNFIELDS PROJECT ID: 21050-17-090320-322 E. FRANKLIN STREET, MONROEUNION COUNTY, NCPROJECT NO: 5204
SITE
FRANKLIN ST
WINDSOR ST
TALLEYRAND AV
FAIRLEY AV
CHURCH STWINCHESTER AV
MAIN STCHARLOTTE AVCROW ST
HOUSTON STBEASLEY STJEFFERSON ST
LEE STSTEWART STHAYNE STJOHN STMORGAN MILL RDMORGAN ST
MAURICE STBROWN ST
CURTIS ST
MORROW AVHILL STBOYTE STBEARD STCHARLES STEVERETTE ST ENGLISH STMILLER STSKYWAY DRDEPOT ST STAFFORD STBURKE STSMITH ST
SHUTE ST
PLANTERS ST
MCCAULEY STLANCASTER AVALTON STCATAWBA AV
HOUGH STCORRELL ST
NANCE STP E BAZEMORE DRBLAI
R STCROWELL ST
LANE ST HENDERSON STPARKER STSACO STSEABOARD STBISHOP BOWENS DR
RAYMOND STHARRIS LNCOAKLEY ST
MORROW AV MORROW AV BURKE STHAYNE STHAYNE STCROWELL ST
LANE ST
³
FIGURE 2: SITE VICINITY MAPFIVE POINTS GATEWAY DEVELOPMENT320-322 E. FRANKLIN STREETMONROE, UNION COUNTYNORTH CAROLINAINCIDENT NO. <PENDING>GRI NO. 5204
PREPARED BY:RESOLVE ENVIRONMENTAL SERVICES, PLLC.AUGUST 26, 2019
0 300150Feet1 inch = 300 feet
1,500-FOOT RADIUS
1,000-FOOT RADIUS
500-FOOT RADIUS
250-FOOT RADIUS
LEGEND
Subject Site
Union County NC_parcels_2019_03_07
Roads_110317

TABLES
Date: 9/18/19
SW 846
7471
Sample ID Sampling
Method
Date Collected
(mm/dd/yy)
1.2 12 15,600 0.12 0.35 14 36 35 670 3.9 134 440 5.8 5.8 NE 270 1.0
0.3 2.9 NE 0.029 0.011 NE 9 NE 89 0.98 NE 13 0.0015 160 NE NE 0.033
Composite 08/02/2019 0.149 J 0.0553 J 0.0946 J 0.105 J 0.0971 J 0.0797 J 0.109 J 0.119 J 0.185 J 0.103 J 0.0690 J 0.174 J 9.2 76.7 31.0 185 0.27
Grab 08/13/2019 NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR NR
Notes:
• Results reported in mg/kg (milligrams per kilograms)
• PSRG: Preliminary Soil Remediation Goals, published May 2019.
• RSL: Regional Screening Level, published April 2019.
• Concentrations in bold face type exceeded the PSRG and/or RSL.
• J: Estimated value.
• Grab stockpile sample collected on 8/13/2019 was analyzed for VOCs by Method 8260B only, no detecable concentrations anbove the method detection limits were reported in the soil sample.
• NE: Not established.
• NR: Analysis not requested.
SUMMARY OF SOIL STOCKPILE ANALYTICAL RESULTS
STOCKPILE
EPA Protection of Ground Water RSL (mg/kg)MercuryBariumArsenicSW 846 6010
Benzo(a)anthraceneChromiumLeadPhenathreneTABLE 1
FIVE POINTS GATEWAY REDEVELOPMENT
PROJECT ID: 21050-17-090
Method 8270E
PyreneBenzo(a)pyreneBenzo(b)fluorantheneContaminant of Concern 
Analytical Method Ideno(1,2,3-c,d)pyreneNCDEQ Protection of Ground Water
Preliminary Soil Remediation Goals (mg/kg)FluorantheneBis(2-ethylhexyl)phthalateChryseneBenzo(k)fluorantheneBenzo(g,h,i)peryleneDi-n-butyl Phthalate
Date:9/18/19
MW-1 8/8/2019 8/15/2019 20 20-40 40 100.00 6.95 ---93.05
MW-2 8/8/2019 8/15/2019 10 10-30 30 104.88 9.20 ---95.68
MW-3 8/8/2019 8/15/2019 10 10-30 30 100.78 4.44 ---96.34
Notes:
• ft BGS : feet below ground surface.
• NA: Not available.
• NM: Not measured.
Groundwater
Elevation
(ft.)
Comments
TABLE 2
WELL CONSTRUCTION AND GAUGING INFORMATION
FIVE POINTS GATEWAY REDEVELOPMENT
PROJECT ID: 20105-17-090
Well ID
Date
Installed
(mm/dd/yy)
Date Water
Level
Measured
(mm/dd/yy)
Well
Casing
Depth
(ft. BGS)
Screened
Interval
(x to y ft.
BGS)
Bottom
of Well
(ft. BGS)
Top of
Casing
Elevation
(ft.)
Depth to
Water from
Top of
Casing
(ft.)
Free
Product
Thickness
(ft.)
Date: 9/18/19
SW 846
8270E
Well ID
Date
Collected
(mm/dd/yy)
1 600 600 500 6 0.4 70 70 25 70 400 400 700
5 1,000 700 10,000 NE 5 NE NE NE NE NE NE NE
MW-1 08/15/19 2.7 7.6 1.3 9.8 1.2 J 7.0 0.27 J 0.59 J 0.23 J 0.37 J 2.9 1.5 <0.95
MW-2 08/15/19 5.0 6.5 0.73 J 3.6 <1.0 13.1 <0.22 0.58 J <0.21 <0.29 0.38 J <0.27 1.0 J
MW-3 08/15/19 <0.31 5.6 0.56 J 2.9 J <1.0 <0.31 <0.22 <0.24 <0.21 <0.29 <0.32 <0.27 <0.95
DUPLICATE 08/15/19 2.4 7.6 0.85 J 4.2 <1.0 10.8 <0.22 0.43 J <0.21 <0.29 0.32 J <0.27 <0.95
TRIP BLANK 08/15/19 <0.31 <0.30 <0.36 <0.72 <1.0 <0.31 <0.22 <0.24 <0.21 <0.29 <0.32 <0.27 NR
Notes:
• Results reported in micrograms per liter (µg/l).
• < : Less than the method detection limit specified in the laboratory report.
• 2L Standard specified in T15A NCAC 2L.0202.
• MCL: Federal EPA maximum contamination level, published April 2019.
• NE: Not Established
• Concentrations in bold face type exceeded the 2L standard and/or MCL.1,3,5-TrimethylbenzeneDi-n-butyl phthalate2L Standard (µg/l)
EPA Regional MCL (µg/l)1,2-DichloroethaneIsopropylbenzeneDi-isopropyl etherp-Isopropyltoluene(4-Isopropyltoluene)n-Propylbenzene1,2,4-TrimethylbenzeneContaminant of Concern BenzeneTolueneEthylbenzeneTotal XylenesNaphthaleneTABLE 3
SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS
FIVE POINTS GATEWAY REDEVELOPMENT
PROJECT ID: 20105-17-090
Analytical Method SW846 8260D
Page 1 of 1

APPENDICES

APPENDIX A
Soil Boring Logs/Monitoring Well Records

Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Five Points Gateway Redevelopment (Project ID 20105-17-090)
Address 320-322 E. Franklin Street, Monroe NC
Boring Number MW-1 Date Drilled
Sample Method Grab Drilling Method Air Hammer
Completion Details Boring terminated at 40'; completed as MW-1
Driller REDI (License #3580-A)Log By T. Kennedy
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0 0-0.5'Gravel
0.5'-3'Red/tan silty CLAY
2
3'-40'Tan to Gray META-ARGILLITE
4
6
8
10

12
14
16

18
20
22

24
26
28

30
32
34

36
38

40 TD 40'
08/08/19
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Five Points Gateway Redevelopment (Project ID 20105-17-090)
Address 320-322 E. Franklin Street, Monroe NC
Boring Number MW-2 Date Drilled
Sample Method N/A Drilling Method Air Hammer
Completion Details Boring terminated at 30'; completed as MW-2
Driller REDI (License #3580-A)Log By T. Kennedy
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0 0-0.5'Asphalt/Gravel
0.5'-4'Red/tan silty CLAY
2
4 4'-40'Tan to Gray META-ARGILLITE
6
8
10

12
14
16

18
20
22

24
26
28

30 TD 30'
32
34

36
38

40
08/08/19
Resolve Environmental Services, PLLC Phone:[phone]
500 Devonport Drive
Matthews, NC 28104
SUBSURFACE LOG
Project Five Points Gateway Redevelopment (Project ID 20105-17-090)
Address 320-322 E. Franklin Street, Monroe NC
Boring Number MW-3 Date Drilled
Sample Method N/A Drilling Method Air Hammer
Completion Details Boring terminated at 30'; completed as MW-3
Driller REDI (License #3580-A)Log By T. Kennedy
Lab Sample OVA
Depth Sample Interval(ft)ppm LITHOLOGY/COMMENTS
0 0-0.5'Asphalt/Gravel
0.5'-2'Red/tan silty CLAY
2 2'-30'Tan META-ARGILLITE
4
6
8
10

12
14
16

18
20
22

24
26
28

30 TD 30'
32
34

36
38

40
08/08/19
WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip
County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W
6. Is (are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed.
For Internal Use ONLY:
WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip
County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W
6. Is (are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed.
For Internal Use ONLY:
WELL CONSTRUCTION RECORD
This form can be used for single or multiple wells
Form GW-1 North Carolina Department of Environment and Natural Resources – Division of Water 5HVRXUFHV Revised AXJXVW 2013
1. Well Contractor Information:

Well Contractor Name

NC Well Contractor Certification Number

Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, ,QMHFWLRQetc.) 3. Well Use (check well use): Water Supply Well: □Agricultural □Municipal/Public □Geothermal (Heating/Cooling Supply) □Residential Water Supply (single)
□Industrial/Commercial □Residential Water Supply (shared) □Irrigation
Non-Water Supply Well: □Monitoring □Recovery
Injection Well: □Aquifer Recharge □Groundwater Remediation
□Aquifer Storage and Recovery □Salinity Barrier □Aquifer Test □Stormwater Drainage
□Experimental Technology □Subsidence Control
□Geothermal (Closed Loop) □Tracer □Geothermal (Heating/Cooling Return) □Other (explain under #21 Remarks)
4. Date Well(s) Completed: ____________ Well ID#______________________ 5a. Well Location:
Facility/Owner Name Facility ID# (if applicable)

Physical Address, City, and Zip
County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) N W
6. Is (are) the well(s): □Permanent or □Temporary

7. Is this a repair to an existing well: □Yes or □No If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form.
8. Number of wells constructed: For multiple injection or non-water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: (ft.) For multiple wells list all depths if different (example- 3@200’ and 2@100′) 10. Static water level below top of casing: (ft.) If water level is above casing, use “+” 11. Borehole diameter: (in.) 12. Well construction method: (i.e. auger, rotary, cable, direct push, etc.) FOR WATER SUPPLY WELLS ONLY: 13a. Yield (gpm) Method of test: 13b. Disinfection type: Amount:

14. WATER ZONES
FROM TO DESCRIPTION
ft. ft.
ft. ft.
15. OUTER CASING (for multi-cased wells) OR LINER (if applicable) FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
16. INNER CASING OR TUBING (geothermal closed-loop)
FROM TO DIAMETER THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL
ft. ft. in.
ft. ft. in.
18. GROUT
FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT
ft. ft.
ft. ft.
ft. ft.
19. SAND/GRAVEL PACK (if applicable)
FROM TO MATERIAL EMPLACEMENT METHOD
ft. ft.
ft. ft.
20. DRILLING LOG (attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.)
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
ft. ft.
21. REMARKS

22. Certification:
Signature of Certified Well Contractor Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner.
23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617
24b. For Injection Wells ONLY: In addition to sending the form to the address in
24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, 1636 Mail Service Center, Raleigh, NC 27699-1636
24c. For Water Supply & Injection Wells:
Also submit one copy of this form within 30 days of completion ofwell construction to the county health department of the county whereconstructed.
For Internal Use ONLY:

APPENDIX B
Disposal Manifest

APPENDIX C
Laboratory Analytical Reports – Soil and Ground Water Samples

08/26/19
Technical Report for
Resolve Environmental
Monroe Lot 3; Monroe, NC
SGS Job Number: FA66760
Sampling Date: 08/02/19
Report to:
Resolve Environmental
500 Devonport Dr
Matthews, NC 28104
[e-mail]
ATTN: Laura Minor
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Orlando, FL 08/26/19
Reissue #1
e-Hardcopy 2.0
Automated Report
45
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 45
FA66760
Florida 4405 Vineland Road Suite C-15 Orlando, FL 32811 tel: [phone] fax: [phone]

August 26, 2019

Ms. Laura Minor
Resolve
500 Devonport Dr
Matthews, NC 28104

RE: SGS North America Inc. - Orlando job FA66760 Reissue

Dear Ms. Minor,

The final report for job number FA66760 has been edited to reflect requested corrections.
These edits have been incorporated into the revised report.

Metals data reprocessed.

SGS North America Inc. - Orlando apologizes for any inconvenience this may have caused.
Please feel free to contact us if we can be of further assistance.

Sincerely,

SGS North America, Inc. - Orlando

2 of 45
FA66760
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................4
Section 2: Summary of Hits ....................................................................................................5
Section 3: Sample Results ........................................................................................................6
3.1: FA66760-1: STOCKPILE .............................................................................................7
Section 4: Misc. Forms ............................................................................................................13
4.1: Chain of Custody ...........................................................................................................14
Section 5: MS Volatiles - QC Data Summaries .....................................................................16
5.1: Method Blank Summary ................................................................................................17
5.2: Blank Spike Summary ...................................................................................................20
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................23
Section 6: MS Semi-volatiles - QC Data Summaries ............................................................26
6.1: Method Blank Summary ................................................................................................27
6.2: Blank Spike Summary ...................................................................................................29
6.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................31
Section 7: Metals Analysis - QC Data Summaries ................................................................34
7.1: Prep QC MP35931: As,Ba,Cd,Cr,Pb,Se,Ag ..................................................................35
7.2: Prep QC MP35947: Hg ..................................................................................................41 12345673 of 45
FA66760
SGS North America Inc.
Sample Summary
Resolve Environmental
Job No:FA66760
Monroe Lot 3; Monroe, NC
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FA66760-1 08/02/19 15:33 TK 08/07/19 SO Soil STOCKPILE
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
4 of 45
FA667601
Summary of Hits Page 1 of 1
Job Number:FA66760
Account:Resolve Environmental
Project:Monroe Lot 3; Monroe, NC
Collected:08/02/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA66760-1 STOCKPILE
m,p-Xylene a 0.106 J 0.83 0.091 mg/kg SW846 8260D
Benzo(a)anthracene 0.0971 J 0.21 0.021 mg/kg SW846 8270E
Benzo(a)pyrene 0.105 J 0.21 0.025 mg/kg SW846 8270E
Benzo(b)fluoranthene 0.149 J 0.21 0.024 mg/kg SW846 8270E
Benzo(g,h,i)perylene 0.0946 J 0.21 0.022 mg/kg SW846 8270E
Benzo(k)fluoranthene 0.0553 J 0.21 0.028 mg/kg SW846 8270E
Chrysene 0.109 J 0.21 0.022 mg/kg SW846 8270E
Di-n-butyl Phthalate 0.119 J 0.43 0.086 mg/kg SW846 8270E
bis(2-Ethylhexyl)phthalate 0.0797 J 0.43 0.043 mg/kg SW846 8270E
Fluoranthene 0.185 J 0.21 0.021 mg/kg SW846 8270E
Indeno(1,2,3-cd)pyrene 0.103 J 0.21 0.026 mg/kg SW846 8270E
Phenanthrene 0.0690 J 0.21 0.021 mg/kg SW846 8270E
Pyrene 0.174 J 0.21 0.025 mg/kg SW846 8270E
Arsenic 9.2 3.0 mg/kg SW846 6010D
Barium 76.7 60 mg/kg SW846 6010D
Chromium 31.0 3.0 mg/kg SW846 6010D
Lead 185 6.0 mg/kg SW846 6010D
Mercury 0.27 0.045 mg/kg SW846 7471B
(a) Dilution required due to matrix interference (sample foamed).
5 of 45
FA667602
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
6 of 45
FA667603
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:STOCKPILE
Lab Sample ID:FA66760-1 Date Sampled:08/02/19
Matrix:SO - Soil Date Received:08/07/19
Method:SW846 8260D Percent Solids:77.6
Project:Monroe Lot 3; Monroe, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a F0091086.D 1 08/08/19 20:57 SP n/a n/a VF3181
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 4.69 g 5.0 ml 100 ul
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 17 8.3 mg/kg
71-43-2 Benzene ND 0.42 0.10 mg/kg
108-86-1 Bromobenzene ND 0.42 0.083 mg/kg
74-97-5 Bromochloromethane ND 0.42 0.12 mg/kg
75-27-4 Bromodichloromethane ND 0.42 0.083 mg/kg
75-25-2 Bromoform ND 0.42 0.083 mg/kg
78-93-3 2-Butanone (MEK)ND 2.1 0.60 mg/kg
104-51-8 n-Butylbenzene ND 0.42 0.083 mg/kg
135-98-8 sec-Butylbenzene ND 0.42 0.083 mg/kg
98-06-6 tert-Butylbenzene ND 0.42 0.083 mg/kg
56-23-5 Carbon Tetrachloride ND 0.42 0.085 mg/kg
108-90-7 Chlorobenzene ND 0.42 0.083 mg/kg
75-00-3 Chloroethane ND 0.42 0.17 mg/kg
67-66-3 Chloroform ND 0.42 0.11 mg/kg
95-49-8 o-Chlorotoluene ND 0.42 0.083 mg/kg
106-43-4 p-Chlorotoluene ND 0.42 0.083 mg/kg
124-48-1 Dibromochloromethane ND 0.42 0.083 mg/kg
106-93-4 1,2-Dibromoethane ND 0.42 0.083 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.42 0.17 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.42 0.083 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.42 0.083 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.42 0.096 mg/kg
75-34-3 1,1-Dichloroethane ND 0.42 0.15 mg/kg
107-06-2 1,2-Dichloroethane ND 0.42 0.083 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.42 0.083 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.42 0.11 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.42 0.083 mg/kg
78-87-5 1,2-Dichloropropane ND 0.42 0.083 mg/kg
142-28-9 1,3-Dichloropropane ND 0.42 0.083 mg/kg
594-20-7 2,2-Dichloropropane ND 0.42 0.083 mg/kg
563-58-6 1,1-Dichloropropene ND 0.42 0.085 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.42 0.083 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 45
FA6676033.1
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:STOCKPILE
Lab Sample ID:FA66760-1 Date Sampled:08/02/19
Matrix:SO - Soil Date Received:08/07/19
Method:SW846 8260D Percent Solids:77.6
Project:Monroe Lot 3; Monroe, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.42 0.083 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.42 0.19 mg/kg
64-17-5 Ethyl Alcohol ND 33 6.2 mg/kg
100-41-4 Ethylbenzene ND 0.42 0.083 mg/kg
591-78-6 2-Hexanone ND 2.1 0.62 mg/kg
98-82-8 Isopropylbenzene ND 0.42 0.083 mg/kg
99-87-6 p-Isopropyltoluene ND 0.42 0.083 mg/kg
74-83-9 Methyl Bromide ND 0.42 0.17 mg/kg
74-87-3 Methyl Chloride ND 0.42 0.17 mg/kg
75-09-2 Methylene Chloride ND 1.7 0.91 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 2.1 0.62 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.42 0.083 mg/kg
91-20-3 Naphthalene ND 0.42 0.17 mg/kg
103-65-1 n-Propylbenzene ND 0.42 0.083 mg/kg
100-42-5 Styrene ND 0.42 0.083 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.42 0.086 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.42 0.083 mg/kg
127-18-4 Tetrachloroethylene ND 0.42 0.11 mg/kg
108-88-3 Toluene ND 1.7 0.83 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.42 0.12 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.42 0.083 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.42 0.083 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.42 0.083 mg/kg
79-01-6 Trichloroethylene ND 0.42 0.083 mg/kg
75-69-4 Trichlorofluoromethane ND 0.42 0.17 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.42 0.10 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.42 0.083 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.42 0.083 mg/kg
108-05-4 Vinyl Acetate ND 2.1 1.4 mg/kg
75-01-4 Vinyl Chloride ND 0.42 0.083 mg/kg
m,p-Xylene 0.106 0.83 0.091 mg/kg J
95-47-6 o-Xylene ND 0.42 0.083 mg/kg
1330-20-7 Xylene (total)ND 1.2 0.17 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%75-124%
17060-07-0 1,2-Dichloroethane-D4 108%72-135%
2037-26-5 Toluene-D8 95%75-126%
460-00-4 4-Bromofluorobenzene 91%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 45
FA6676033.1
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:STOCKPILE
Lab Sample ID:FA66760-1 Date Sampled:08/02/19
Matrix:SO - Soil Date Received:08/07/19
Method:SW846 8260D Percent Solids:77.6
Project:Monroe Lot 3; Monroe, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Dilution required due to matrix interference (sample foamed).
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 45
FA6676033.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:STOCKPILE
Lab Sample ID:FA66760-1 Date Sampled:08/02/19
Matrix:SO - Soil Date Received:08/07/19
Method:SW846 8270E SW846 3546 Percent Solids:77.6
Project:Monroe Lot 3; Monroe, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X066493.D 1 08/12/19 15:47 MV 08/12/19 10:45 OP76324 SX2738
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 1.1 0.21 mg/kg
59-50-7 4-Chloro-3-methyl Phenol ND 0.21 0.024 mg/kg
95-57-8 2-Chlorophenol ND 0.21 0.026 mg/kg
120-83-2 2,4-Dichlorophenol ND 0.21 0.025 mg/kg
105-67-9 2,4-Dimethylphenol ND 0.21 0.057 mg/kg
51-28-5 2,4-Dinitrophenol a ND 1.1 0.21 mg/kg
534-52-1 4,6-Dinitro-o-cresol ND 0.43 0.086 mg/kg
95-48-7 2-Methylphenol ND 0.21 0.026 mg/kg
3&4-Methylphenol ND 0.21 0.035 mg/kg
88-75-5 2-Nitrophenol ND 0.21 0.023 mg/kg
100-02-7 4-Nitrophenol ND 1.1 0.21 mg/kg
87-86-5 Pentachlorophenol ND 1.1 0.21 mg/kg
108-95-2 Phenol ND 0.21 0.021 mg/kg
88-06-2 2,4,6-Trichlorophenol ND 0.21 0.025 mg/kg
83-32-9 Acenaphthene ND 0.21 0.023 mg/kg
208-96-8 Acenaphthylene ND 0.21 0.021 mg/kg
120-12-7 Anthracene ND 0.21 0.024 mg/kg
56-55-3 Benzo(a)anthracene 0.0971 0.21 0.021 mg/kg J
50-32-8 Benzo(a)pyrene 0.105 0.21 0.025 mg/kg J
205-99-2 Benzo(b)fluoranthene 0.149 0.21 0.024 mg/kg J
191-24-2 Benzo(g,h,i)perylene 0.0946 0.21 0.022 mg/kg J
207-08-9 Benzo(k)fluoranthene 0.0553 0.21 0.028 mg/kg J
100-51-6 Benzyl Alcohol ND 0.21 0.021 mg/kg
101-55-3 4-Bromophenyl phenyl ether ND 0.21 0.022 mg/kg
85-68-7 Butyl benzyl phthalate ND 0.21 0.043 mg/kg
106-47-8 4-Chloroaniline ND 0.21 0.054 mg/kg
111-91-1 bis(2-Chloroethoxy)methane ND 0.21 0.021 mg/kg
111-44-4 bis(2-Chloroethyl)ether ND 0.21 0.025 mg/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 0.21 0.027 mg/kg
91-58-7 2-Chloronaphthalene ND 0.21 0.021 mg/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 0.21 0.021 mg/kg
218-01-9 Chrysene 0.109 0.21 0.022 mg/kg J
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 45
FA6676033.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:STOCKPILE
Lab Sample ID:FA66760-1 Date Sampled:08/02/19
Matrix:SO - Soil Date Received:08/07/19
Method:SW846 8270E SW846 3546 Percent Solids:77.6
Project:Monroe Lot 3; Monroe, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 0.21 0.027 mg/kg
132-64-9 Dibenzofuran ND 0.21 0.021 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.21 0.021 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.21 0.023 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.21 0.029 mg/kg
91-94-1 3,3'-Dichlorobenzidine ND 0.21 0.051 mg/kg
84-66-2 Diethyl Phthalate ND 0.43 0.043 mg/kg
131-11-3 Dimethyl Phthalate ND 0.21 0.043 mg/kg
117-84-0 Di-n-octyl Phthalate ND 0.21 0.043 mg/kg
84-74-2 Di-n-butyl Phthalate 0.119 0.43 0.086 mg/kg J
122-66-7 1,2-Diphenylhydrazine ND 0.21 0.021 mg/kg
117-81-7 bis(2-Ethylhexyl)phthalate 0.0797 0.43 0.043 mg/kg J
206-44-0 Fluoranthene 0.185 0.21 0.021 mg/kg J
86-73-7 Fluorene ND 0.21 0.023 mg/kg
118-74-1 Hexachlorobenzene ND 0.21 0.022 mg/kg
87-68-3 Hexachlorobutadiene ND 0.21 0.022 mg/kg
77-47-4 Hexachlorocyclopentadiene ND 0.21 0.043 mg/kg
67-72-1 Hexachloroethane ND 0.21 0.025 mg/kg
193-39-5 Indeno(1,2,3-cd)pyrene 0.103 0.21 0.026 mg/kg J
78-59-1 Isophorone ND 0.21 0.021 mg/kg
90-12-0 1-Methylnaphthalene ND 0.21 0.021 mg/kg
91-57-6 2-Methylnaphthalene ND 0.21 0.021 mg/kg
91-20-3 Naphthalene ND 0.21 0.021 mg/kg
98-95-3 Nitrobenzene ND 0.21 0.021 mg/kg
621-64-7 N-Nitrosodi-n-propylamine ND 0.21 0.021 mg/kg
86-30-6 N-Nitrosodiphenylamine ND 0.21 0.023 mg/kg
85-01-8 Phenanthrene 0.0690 0.21 0.021 mg/kg J
129-00-0 Pyrene 0.174 0.21 0.025 mg/kg J
120-82-1 1,2,4-Trichlorobenzene ND 0.21 0.025 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 60%40-102%
4165-62-2 Phenol-d5 66%41-100%
118-79-6 2,4,6-Tribromophenol 81%42-108%
4165-60-0 Nitrobenzene-d5 59%40-105%
321-60-8 2-Fluorobiphenyl 68%43-107%
1718-51-0 Terphenyl-d14 70%45-119%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 45
FA6676033.1
SGS North America Inc.
Report of Analysis Page 1 of 1
Client Sample ID:STOCKPILE
Lab Sample ID:FA66760-1 Date Sampled:08/02/19
Matrix:SO - Soil Date Received:08/07/19
Percent Solids:77.6
Project:Monroe Lot 3; Monroe, NC
Metals Analysis
Analyte Result RL Units DF Prep Analyzed By Method Prep Method
Arsenic 9.2 3.0 mg/kg 5 08/09/19 08/09/19 LM SW846 6010D 1 SW846 3050B 3
Barium 76.7 60 mg/kg 5 08/09/19 08/09/19 LM SW846 6010D 1 SW846 3050B 3
Cadmium <1.2 1.2 mg/kg 5 08/09/19 08/09/19 LM SW846 6010D 1 SW846 3050B 3
Chromium 31.0 3.0 mg/kg 5 08/09/19 08/09/19 LM SW846 6010D 1 SW846 3050B 3
Lead 185 6.0 mg/kg 5 08/09/19 08/09/19 LM SW846 6010D 1 SW846 3050B 3
Mercury 0.27 0.045 mg/kg 1 08/12/19 08/12/19 JC SW846 7471B 2 SW846 7471B 4
Selenium <6.0 6.0 mg/kg 5 08/09/19 08/09/19 LM SW846 6010D 1 SW846 3050B 3
Silver <3.0 3.0 mg/kg 5 08/09/19 08/09/19 LM SW846 6010D 1 SW846 3050B 3
(1) Instrument QC Batch: MA16086
(2) Instrument QC Batch: MA16089
(3) Prep QC Batch: MP35931
(4) Prep QC Batch: MP35947
RL = Reporting Limit
12 of 45
FA6676033.1
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
13 of 45
FA667604
FA66760: Chain of Custody
Page 1 of 2
14 of 45
FA6676044.1
Job Number:FA66760 Client:RESOLVE ENVIRONMENTAL
Date / Time Received:8/7/2019 8:45:00 AM Delivery Method:FX
Project:MONROE LOT 3
Airbill #'s:
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
N/A
N/A
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (1.2);
Cooler 1: (2.2);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:1; # of Coolers:N/A
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:BRANDYK Date:Date:8/7/2019 8:45:00 AM
FA66760: Chain of Custody
Page 2 of 2
15 of 45
FA6676044.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
16 of 45
FA667605
Method Blank Summary Page 1 of 3
Job Number:FA66760
Account:RENCM Resolve Environmental
Project:Monroe Lot 3; Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF3181-MB F0091067.D 1 08/08/19 SP n/a n/a VF3181
The QC reported here applies to the following samples:Method: SW846 8260D
FA66760-1
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 200 100 ug/kg
71-43-2 Benzene ND 5.0 1.2 ug/kg
108-86-1 Bromobenzene ND 5.0 1.0 ug/kg
74-97-5 Bromochloromethane ND 5.0 1.5 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 25 7.3 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg
135-98-8 sec-Butylbenzene ND 5.0 1.0 ug/kg
98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/kg
56-23-5 Carbon Tetrachloride ND 5.0 1.0 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.3 ug/kg
95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg
106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.0 1.2 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.8 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.4 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg
142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg
594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/kg
563-58-6 1,1-Dichloropropene ND 5.0 1.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
108-20-3 Di-Isopropyl Ether ND 5.0 2.3 ug/kg
64-17-5 Ethyl Alcohol ND 400 75 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg
17 of 45
FA6676055.1.1
Method Blank Summary Page 2 of 3
Job Number:FA66760
Account:RENCM Resolve Environmental
Project:Monroe Lot 3; Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF3181-MB F0091067.D 1 08/08/19 SP n/a n/a VF3181
The QC reported here applies to the following samples:Method: SW846 8260D
FA66760-1
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 25 7.5 ug/kg
98-82-8 Isopropylbenzene ND 5.0 1.0 ug/kg
99-87-6 p-Isopropyltoluene ND 5.0 1.0 ug/kg
74-83-9 Methyl Bromide ND 5.0 2.0 ug/kg
74-87-3 Methyl Chloride ND 5.0 2.0 ug/kg
75-09-2 Methylene Chloride ND 20 11 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 7.5 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg
108-88-3 Toluene ND 20 10 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.4 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.0 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg
108-05-4 Vinyl Acetate ND 25 16 ug/kg
75-01-4 Vinyl Chloride ND 5.0 1.0 ug/kg
m,p-Xylene ND 10 1.1 ug/kg
95-47-6 o-Xylene ND 5.0 1.0 ug/kg
1330-20-7 Xylene (total)ND 15 2.1 ug/kg
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 97%75-124%
17060-07-0 1,2-Dichloroethane-D4 101%72-135%
2037-26-5 Toluene-D8 97%75-126%
18 of 45
FA6676055.1.1
Method Blank Summary Page 3 of 3
Job Number:FA66760
Account:RENCM Resolve Environmental
Project:Monroe Lot 3; Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF3181-MB F0091067.D 1 08/08/19 SP n/a n/a VF3181
The QC reported here applies to the following samples:Method: SW846 8260D
FA66760-1
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 97%71-133%
19 of 45
FA6676055.1.1
Blank Spike Summary Page 1 of 3
Job Number:FA66760
Account:RENCM Resolve Environmental
Project:Monroe Lot 3; Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF3181-BS F0091068.D 1 08/08/19 SP n/a n/a VF3181
The QC reported here applies to the following samples:Method: SW846 8260D
FA66760-1
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
67-64-1 Acetone 250 311 124 61-152
71-43-2 Benzene 50 51.1 102 76-126
108-86-1 Bromobenzene 50 48.5 97 76-122
74-97-5 Bromochloromethane 50 48.0 96 77-120
75-27-4 Bromodichloromethane 50 55.4 111 74-130
75-25-2 Bromoform 50 53.0 106 76-127
78-93-3 2-Butanone (MEK)250 259 104 75-137
104-51-8 n-Butylbenzene 50 51.5 103 71-128
135-98-8 sec-Butylbenzene 50 50.9 102 79-135
98-06-6 tert-Butylbenzene 50 49.6 99 77-133
56-23-5 Carbon Tetrachloride 50 51.8 104 78-133
108-90-7 Chlorobenzene 50 49.4 99 81-129
75-00-3 Chloroethane 50 42.3 85 68-133
67-66-3 Chloroform 50 52.1 104 72-123
95-49-8 o-Chlorotoluene 50 50.0 100 77-129
106-43-4 p-Chlorotoluene 50 49.4 99 80-134
124-48-1 Dibromochloromethane 50 53.1 106 76-127
106-93-4 1,2-Dibromoethane 50 49.5 99 77-126
75-71-8 Dichlorodifluoromethane 50 40.1 80 68-168
95-50-1 1,2-Dichlorobenzene 50 49.6 99 80-129
541-73-1 1,3-Dichlorobenzene 50 51.0 102 81-129
106-46-7 1,4-Dichlorobenzene 50 50.3 101 76-130
75-34-3 1,1-Dichloroethane 50 52.9 106 73-125
107-06-2 1,2-Dichloroethane 50 52.3 105 74-128
75-35-4 1,1-Dichloroethylene 50 48.0 96 81-136
156-59-2 cis-1,2-Dichloroethylene 50 50.6 101 74-126
156-60-5 trans-1,2-Dichloroethylene 50 50.9 102 70-127
78-87-5 1,2-Dichloropropane 50 53.4 107 74-125
142-28-9 1,3-Dichloropropane 50 48.0 96 76-122
594-20-7 2,2-Dichloropropane 50 53.1 106 77-133
563-58-6 1,1-Dichloropropene 50 50.9 102 75-130
10061-01-5 cis-1,3-Dichloropropene 50 51.5 103 80-123
10061-02-6 trans-1,3-Dichloropropene 50 51.8 104 75-131
108-20-3 Di-Isopropyl Ether 50 47.5 95 75-122
64-17-5 Ethyl Alcohol 1000 943 94 53-154
100-41-4 Ethylbenzene 50 50.3 101 77-123
* = Outside of Control Limits.
20 of 45
FA6676055.2.1
Blank Spike Summary Page 2 of 3
Job Number:FA66760
Account:RENCM Resolve Environmental
Project:Monroe Lot 3; Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF3181-BS F0091068.D 1 08/08/19 SP n/a n/a VF3181
The QC reported here applies to the following samples:Method: SW846 8260D
FA66760-1
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
591-78-6 2-Hexanone 250 248 99 72-133
98-82-8 Isopropylbenzene 50 53.2 106 80-136
99-87-6 p-Isopropyltoluene 50 51.4 103 77-131
74-83-9 Methyl Bromide 50 40.2 80 65-139
74-87-3 Methyl Chloride 50 46.9 94 71-144
75-09-2 Methylene Chloride 50 50.6 101 74-137
108-10-1 4-Methyl-2-pentanone (MIBK)250 245 98 76-132
1634-04-4 Methyl Tert Butyl Ether 50 47.9 96 77-120
91-20-3 Naphthalene 50 52.0 104 79-129
103-65-1 n-Propylbenzene 50 49.6 99 80-135
100-42-5 Styrene 50 50.3 101 78-125
630-20-6 1,1,1,2-Tetrachloroethane 50 53.3 107 78-126
79-34-5 1,1,2,2-Tetrachloroethane 50 50.6 101 71-126
127-18-4 Tetrachloroethylene 50 50.6 101 79-130
108-88-3 Toluene 50 50.3 101 76-124
87-61-6 1,2,3-Trichlorobenzene 50 52.3 105 77-128
120-82-1 1,2,4-Trichlorobenzene 50 51.6 103 78-130
71-55-6 1,1,1-Trichloroethane 50 50.2 100 70-129
79-00-5 1,1,2-Trichloroethane 50 50.2 100 74-124
79-01-6 Trichloroethylene 50 51.8 104 75-128
75-69-4 Trichlorofluoromethane 50 47.1 94 73-145
96-18-4 1,2,3-Trichloropropane 50 48.4 97 74-127
95-63-6 1,2,4-Trimethylbenzene 50 49.3 99 74-123
108-67-8 1,3,5-Trimethylbenzene 50 50.8 102 73-122
108-05-4 Vinyl Acetate 250 269 108 48-164
75-01-4 Vinyl Chloride 50 46.7 93 76-141
m,p-Xylene 100 103 103 80-128
95-47-6 o-Xylene 50 51.2 102 80-132
1330-20-7 Xylene (total)150 154 103 80-129
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 100%75-124%
17060-07-0 1,2-Dichloroethane-D4 100%72-135%
2037-26-5 Toluene-D8 98%75-126%
* = Outside of Control Limits.
21 of 45
FA6676055.2.1
Blank Spike Summary Page 3 of 3
Job Number:FA66760
Account:RENCM Resolve Environmental
Project:Monroe Lot 3; Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VF3181-BS F0091068.D 1 08/08/19 SP n/a n/a VF3181
The QC reported here applies to the following samples:Method: SW846 8260D
FA66760-1
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 96%71-133%
* = Outside of Control Limits.
22 of 45
FA6676055.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA66760
Account:RENCM Resolve Environmental
Project:Monroe Lot 3; Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA66756-4MS F0091087.D 1 08/08/19 SP n/a n/a VF3181
FA66756-4MSD F0091088.D 1 08/08/19 SP n/a n/a VF3181
FA66756-4 a F0091079.D 1 08/08/19 SP n/a n/a VF3181
The QC reported here applies to the following samples:Method: SW846 8260D
FA66760-1
FA66756-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
67-64-1 Acetone 185 J 381 519 88 382 516 87 1 61-152/27
71-43-2 Benzene ND 76.3 46.4 61*76.4 45.8 60*1 76-126/26
108-86-1 Bromobenzene ND 76.3 13.5 18*76.4 12.6 16*7 76-122/32
74-97-5 Bromochloromethane ND 76.3 26.8 35*76.4 25.9 34*3 77-120/24
75-27-4 Bromodichloromethane ND 76.3 42.3 55*76.4 41.1 54*3 74-130/25
75-25-2 Bromoform ND 76.3 33.6 44*76.4 32.1 42*5 76-127/26
78-93-3 2-Butanone (MEK)ND 381 305 80 382 290 76 5 75-137/25
104-51-8 n-Butylbenzene ND 76.3 19.7 26*76.4 20.0 26*2 71-128/35
135-98-8 sec-Butylbenzene ND 76.3 63.8 84 76.4 69.3 91 8 79-135/34
98-06-6 tert-Butylbenzene ND 76.3 84.5 111 76.4 94.0 123 11 77-133/34
56-23-5 Carbon Tetrachloride ND 76.3 74.3 97 76.4 77.9 102 5 78-133/29
108-90-7 Chlorobenzene ND 76.3 17.7 23*76.4 16.8 22*5 81-129/29
75-00-3 Chloroethane ND 76.3 42.5 56*76.4 45.2 59*6 68-133/29
67-66-3 Chloroform ND 76.3 54.0 71*76.4 53.3 70*1 72-123/26
95-49-8 o-Chlorotoluene ND 76.3 40.6 53*76.4 42.5 56*5 77-129/33
106-43-4 p-Chlorotoluene ND 76.3 13.0 17*76.4 12.3 16*6 80-134/33
124-48-1 Dibromochloromethane ND 76.3 39.0 51*76.4 37.0 48*5 76-127/27
106-93-4 1,2-Dibromoethane ND 76.3 12.7 17*76.4 10.9 14*15 77-126/26
75-71-8 Dichlorodifluoromethane ND 76.3 62.0 81 76.4 64.5 84 4 68-168/29
95-50-1 1,2-Dichlorobenzene ND 76.3 16.8 22*76.4 15.7 21*7 80-129/32
541-73-1 1,3-Dichlorobenzene ND 76.3 10.6 14*76.4 9.7 13*9 81-129/33
106-46-7 1,4-Dichlorobenzene ND 76.3 7.0 9*76.4 6.9 9*1 76-130/32
75-34-3 1,1-Dichloroethane ND 76.3 64.4 84 76.4 64.6 85 0 73-125/27
107-06-2 1,2-Dichloroethane ND 76.3 28.8 38*76.4 28.0 37*3 74-128/23
75-35-4 1,1-Dichloroethylene ND 76.3 43.6 57*76.4 47.4 62*8 81-136/28
156-59-2 cis-1,2-Dichloroethylene ND 76.3 27.8 36*76.4 28.0 37*1 74-126/26
156-60-5 trans-1,2-Dichloroethylene ND 76.3 25.6 34*76.4 25.8 34*1 70-127/27
78-87-5 1,2-Dichloropropane ND 76.3 57.1 75 76.4 57.1 75 0 74-125/25
142-28-9 1,3-Dichloropropane ND 76.3 24.8 33*76.4 22.7 30*9 76-122/26
594-20-7 2,2-Dichloropropane ND 76.3 84.7 111 76.4 87.5 114 3 77-133/28
563-58-6 1,1-Dichloropropene ND 76.3 31.6 41*76.4 32.7 43*3 75-130/28
10061-01-5 cis-1,3-Dichloropropene ND 76.3 12.3 16*76.4 10.9 14*12 80-123/26
10061-02-6 trans-1,3-Dichloropropene ND 76.3 7.8 10*76.4 6.8 9*14 75-131/28
108-20-3 Di-Isopropyl Ether ND 76.3 75.3 99 76.4 77.7 102 3 75-122/25
64-17-5 Ethyl Alcohol ND 1530 1670 109 1530 2030 133 19 53-154/42
100-41-4 Ethylbenzene ND 76.3 31.7 42*76.4 31.5 41*1 77-123/31
* = Outside of Control Limits.
23 of 45
FA6676055.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA66760
Account:RENCM Resolve Environmental
Project:Monroe Lot 3; Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA66756-4MS F0091087.D 1 08/08/19 SP n/a n/a VF3181
FA66756-4MSD F0091088.D 1 08/08/19 SP n/a n/a VF3181
FA66756-4 a F0091079.D 1 08/08/19 SP n/a n/a VF3181
The QC reported here applies to the following samples:Method: SW846 8260D
FA66760-1
FA66756-4 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
591-78-6 2-Hexanone ND 381 268 70*382 257 67*4 72-133/26
98-82-8 Isopropylbenzene ND 76.3 53.2 70*76.4 54.3 71*2 80-136/32
99-87-6 p-Isopropyltoluene ND 76.3 53.0 69*76.4 57.1 75*7 77-131/34
74-83-9 Methyl Bromide ND 76.3 43.4 57*76.4 46.7 61*7 65-139/31
74-87-3 Methyl Chloride ND 76.3 63.4 83 76.4 69.2 91 9 71-144/27
75-09-2 Methylene Chloride ND 76.3 61.8 81 76.4 61.8 81 0 74-137/28
108-10-1 4-Methyl-2-pentanone (MIBK)ND 381 375 98 382 368 96 2 76-132/26
1634-04-4 Methyl Tert Butyl Ether ND 76.3 77.2 101 76.4 79.4 104 3 77-120/24
91-20-3 Naphthalene ND 76.3 10.0 13*76.4 9.1 12*9 79-129/33
103-65-1 n-Propylbenzene ND 76.3 32.3 42*76.4 34.3 45*6 80-135/33
100-42-5 Styrene ND 76.3 11.6 15*76.4 10.5 14*10 78-125/30
630-20-6 1,1,1,2-Tetrachloroethane ND 76.3 80.8 106 76.4 83.8 110 4 78-126/27
79-34-5 1,1,2,2-Tetrachloroethane ND 76.3 81.9 107 76.4 84.6 111 3 71-126/30
127-18-4 Tetrachloroethylene ND 76.3 41.9 55*76.4 42.9 56*2 79-130/31
108-88-3 Toluene ND 76.3 36.1 47*76.4 36.5 48*1 76-124/30
87-61-6 1,2,3-Trichlorobenzene ND 76.3 13.6 18*76.4 12.6 16*8 77-128/35
120-82-1 1,2,4-Trichlorobenzene ND 76.3 6.5 9*76.4 6.2 8*5 78-130/34
71-55-6 1,1,1-Trichloroethane ND 76.3 78.3 103 76.4 81.8 107 4 70-129/27
79-00-5 1,1,2-Trichloroethane ND 76.3 46.9 62*76.4 43.8 57*7 74-124/28
79-01-6 Trichloroethylene ND 76.3 25.4 33*76.4 25.5 33*0 75-128/27
75-69-4 Trichlorofluoromethane ND 76.3 64.3 84 76.4 67.6 88 5 73-145/31
96-18-4 1,2,3-Trichloropropane ND 76.3 69.7 91 76.4 68.6 90 2 74-127/27
95-63-6 1,2,4-Trimethylbenzene ND 76.3 43.8 57*76.4 45.7 60*4 74-123/34
108-67-8 1,3,5-Trimethylbenzene ND 76.3 65.5 86 76.4 70.7 93 8 73-122/33
108-05-4 Vinyl Acetate ND 381 35.7 9*382 ND 0*200*48-164/37
75-01-4 Vinyl Chloride ND 76.3 49.8 65*76.4 53.9 71*8 76-141/27
m,p-Xylene ND 153 61.5 40*153 61.1 40*1 80-128/30
95-47-6 o-Xylene ND 76.3 45.3 59*76.4 44.6 58*2 80-132/30
1330-20-7 Xylene (total)ND 229 107 47*229 106 46*1 80-129/30
CAS No.Surrogate Recoveries MS MSD FA66756-4 Limits
1868-53-7 Dibromofluoromethane 105%107%108%75-124%
17060-07-0 1,2-Dichloroethane-D4 97%102%94%72-135%
2037-26-5 Toluene-D8 114%114%137%* b 75-126%
* = Outside of Control Limits.
24 of 45
FA6676055.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA66760
Account:RENCM Resolve Environmental
Project:Monroe Lot 3; Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA66756-4MS F0091087.D 1 08/08/19 SP n/a n/a VF3181
FA66756-4MSD F0091088.D 1 08/08/19 SP n/a n/a VF3181
FA66756-4 a F0091079.D 1 08/08/19 SP n/a n/a VF3181
The QC reported here applies to the following samples:Method: SW846 8260D
FA66760-1
CAS No.Surrogate Recoveries MS MSD FA66756-4 Limits
460-00-4 4-Bromofluorobenzene 121%125%141%* b 71-133%
(a) Confirmation run for surrogate recoveries.
(b) Outside control limits due to matrix interference. Confirmed by reanalysis.
* = Outside of Control Limits.
25 of 45
FA6676055.3.1
SGS North America Inc.
MS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 6
26 of 45
FA667606
Method Blank Summary Page 1 of 2
Job Number:FA66760
Account:RENCM Resolve Environmental
Project:Monroe Lot 3; Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP76324-MB X066492.D 1 08/12/19 MV 08/12/19 OP76324 SX2738
The QC reported here applies to the following samples:Method: SW846 8270E
FA66760-1
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 830 170 ug/kg
59-50-7 4-Chloro-3-methyl Phenol ND 170 19 ug/kg
95-57-8 2-Chlorophenol ND 170 20 ug/kg
120-83-2 2,4-Dichlorophenol ND 170 19 ug/kg
105-67-9 2,4-Dimethylphenol ND 170 44 ug/kg
51-28-5 2,4-Dinitrophenol ND 830 170 ug/kg
534-52-1 4,6-Dinitro-o-cresol ND 330 67 ug/kg
95-48-7 2-Methylphenol ND 170 20 ug/kg
3&4-Methylphenol ND 170 27 ug/kg
88-75-5 2-Nitrophenol ND 170 18 ug/kg
100-02-7 4-Nitrophenol ND 830 170 ug/kg
87-86-5 Pentachlorophenol ND 830 170 ug/kg
108-95-2 Phenol ND 170 17 ug/kg
88-06-2 2,4,6-Trichlorophenol ND 170 19 ug/kg
83-32-9 Acenaphthene ND 170 18 ug/kg
208-96-8 Acenaphthylene ND 170 17 ug/kg
120-12-7 Anthracene ND 170 19 ug/kg
56-55-3 Benzo(a)anthracene ND 170 17 ug/kg
50-32-8 Benzo(a)pyrene ND 170 20 ug/kg
205-99-2 Benzo(b)fluoranthene ND 170 18 ug/kg
191-24-2 Benzo(g,h,i)perylene ND 170 17 ug/kg
207-08-9 Benzo(k)fluoranthene ND 170 22 ug/kg
100-51-6 Benzyl Alcohol ND 170 17 ug/kg
101-55-3 4-Bromophenyl phenyl ether ND 170 17 ug/kg
85-68-7 Butyl benzyl phthalate ND 170 33 ug/kg
106-47-8 4-Chloroaniline ND 170 42 ug/kg
111-91-1 bis(2-Chloroethoxy)methane ND 170 17 ug/kg
111-44-4 bis(2-Chloroethyl)ether ND 170 19 ug/kg
108-60-1 2,2'-Oxybis(1-chloropropane)ND 170 21 ug/kg
91-58-7 2-Chloronaphthalene ND 170 17 ug/kg
7005-72-3 4-Chlorophenyl phenyl ether ND 170 17 ug/kg
218-01-9 Chrysene ND 170 17 ug/kg
53-70-3 Dibenzo(a,h)anthracene ND 170 21 ug/kg
132-64-9 Dibenzofuran ND 170 17 ug/kg
95-50-1 1,2-Dichlorobenzene ND 170 17 ug/kg
541-73-1 1,3-Dichlorobenzene ND 170 18 ug/kg
27 of 45
FA6676066.1.1
Method Blank Summary Page 2 of 2
Job Number:FA66760
Account:RENCM Resolve Environmental
Project:Monroe Lot 3; Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP76324-MB X066492.D 1 08/12/19 MV 08/12/19 OP76324 SX2738
The QC reported here applies to the following samples:Method: SW846 8270E
FA66760-1
CAS No.Compound Result RL MDL Units Q
106-46-7 1,4-Dichlorobenzene ND 170 22 ug/kg
91-94-1 3,3'-Dichlorobenzidine ND 170 40 ug/kg
84-66-2 Diethyl Phthalate ND 330 33 ug/kg
131-11-3 Dimethyl Phthalate ND 170 33 ug/kg
117-84-0 Di-n-octyl Phthalate ND 170 33 ug/kg
84-74-2 Di-n-butyl Phthalate ND 330 67 ug/kg
122-66-7 1,2-Diphenylhydrazine ND 170 17 ug/kg
117-81-7 bis(2-Ethylhexyl)phthalate ND 330 33 ug/kg
206-44-0 Fluoranthene ND 170 17 ug/kg
86-73-7 Fluorene ND 170 18 ug/kg
118-74-1 Hexachlorobenzene ND 170 17 ug/kg
87-68-3 Hexachlorobutadiene ND 170 17 ug/kg
77-47-4 Hexachlorocyclopentadiene ND 170 33 ug/kg
67-72-1 Hexachloroethane ND 170 20 ug/kg
193-39-5 Indeno(1,2,3-cd)pyrene ND 170 20 ug/kg
78-59-1 Isophorone ND 170 17 ug/kg
90-12-0 1-Methylnaphthalene ND 170 17 ug/kg
91-57-6 2-Methylnaphthalene ND 170 17 ug/kg
91-20-3 Naphthalene ND 170 17 ug/kg
98-95-3 Nitrobenzene ND 170 17 ug/kg
621-64-7 N-Nitrosodi-n-propylamine ND 170 17 ug/kg
86-30-6 N-Nitrosodiphenylamine ND 170 18 ug/kg
85-01-8 Phenanthrene ND 170 17 ug/kg
129-00-0 Pyrene ND 170 19 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 170 20 ug/kg
CAS No.Surrogate Recoveries Limits
367-12-4 2-Fluorophenol 72%40-102%
4165-62-2 Phenol-d5 78%41-100%
118-79-6 2,4,6-Tribromophenol 77%42-108%
4165-60-0 Nitrobenzene-d5 68%40-105%
321-60-8 2-Fluorobiphenyl 69%43-107%
1718-51-0 Terphenyl-d14 76%45-119%
28 of 45
FA6676066.1.1
Blank Spike Summary Page 1 of 2
Job Number:FA66760
Account:RENCM Resolve Environmental
Project:Monroe Lot 3; Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP76324-BS X066491.D 1 08/12/19 MV 08/12/19 OP76324 SX2738
The QC reported here applies to the following samples:Method: SW846 8270E
FA66760-1
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
65-85-0 Benzoic Acid 3330 2740 82 36-118
59-50-7 4-Chloro-3-methyl Phenol 1670 1480 89 52-108
95-57-8 2-Chlorophenol 1670 1280 77 48-104
120-83-2 2,4-Dichlorophenol 1670 1460 88 51-105
105-67-9 2,4-Dimethylphenol 1670 1330 80 43-96
51-28-5 2,4-Dinitrophenol 3330 3190 96 40-119
534-52-1 4,6-Dinitro-o-cresol 3330 3390 102 64-121
95-48-7 2-Methylphenol 1670 1170 70 46-107
3&4-Methylphenol 3330 2450 74 44-111
88-75-5 2-Nitrophenol 1670 1540 92 49-104
100-02-7 4-Nitrophenol 3330 3130 94 56-116
87-86-5 Pentachlorophenol 3330 3090 93 61-114
108-95-2 Phenol 1670 1340 80 45-110
88-06-2 2,4,6-Trichlorophenol 1670 1650 99 56-109
83-32-9 Acenaphthene 1670 1360 82 56-109
208-96-8 Acenaphthylene 1670 1430 86 56-106
120-12-7 Anthracene 1670 1420 85 61-110
56-55-3 Benzo(a)anthracene 1670 1530 92 66-111
50-32-8 Benzo(a)pyrene 1670 1420 85 59-104
205-99-2 Benzo(b)fluoranthene 1670 1530 92 67-113
191-24-2 Benzo(g,h,i)perylene 1670 1700 102 67-113
207-08-9 Benzo(k)fluoranthene 1670 1460 88 67-114
100-51-6 Benzyl Alcohol 1670 1190 71 53-108
101-55-3 4-Bromophenyl phenyl ether 1670 1560 94 62-110
85-68-7 Butyl benzyl phthalate 1670 1590 95 65-113
106-47-8 4-Chloroaniline 1670 1280 77 30-115
111-91-1 bis(2-Chloroethoxy)methane 1670 1330 80 48-105
111-44-4 bis(2-Chloroethyl)ether 1670 1160 70 46-103
108-60-1 2,2'-Oxybis(1-chloropropane)1670 1160 70 40-110
91-58-7 2-Chloronaphthalene 1670 1340 80 53-106
7005-72-3 4-Chlorophenyl phenyl ether 1670 1470 88 58-106
218-01-9 Chrysene 1670 1500 90 65-112
53-70-3 Dibenzo(a,h)anthracene 1670 1660 100 68-115
132-64-9 Dibenzofuran 1670 1480 89 57-108
95-50-1 1,2-Dichlorobenzene 1670 1100 66 44-102
541-73-1 1,3-Dichlorobenzene 1670 1100 66 42-100
* = Outside of Control Limits.
29 of 45
FA6676066.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA66760
Account:RENCM Resolve Environmental
Project:Monroe Lot 3; Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP76324-BS X066491.D 1 08/12/19 MV 08/12/19 OP76324 SX2738
The QC reported here applies to the following samples:Method: SW846 8270E
FA66760-1
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
106-46-7 1,4-Dichlorobenzene 1670 1080 65 40-106
91-94-1 3,3'-Dichlorobenzidine 1670 1630 98 36-114
84-66-2 Diethyl Phthalate 1670 1470 88 61-109
131-11-3 Dimethyl Phthalate 1670 1470 88 59-108
117-84-0 Di-n-octyl Phthalate 1670 1650 99 64-119
84-74-2 Di-n-butyl Phthalate 1670 1560 94 63-108
122-66-7 1,2-Diphenylhydrazine 1670 1390 83 58-112
117-81-7 bis(2-Ethylhexyl)phthalate 1670 1630 98 64-115
206-44-0 Fluoranthene 1670 1430 86 60-108
86-73-7 Fluorene 1670 1420 85 58-109
118-74-1 Hexachlorobenzene 1670 1430 86 59-111
87-68-3 Hexachlorobutadiene 1670 1120 67 41-108
77-47-4 Hexachlorocyclopentadiene 1670 1230 74 49-110
67-72-1 Hexachloroethane 1670 1080 65 40-105
193-39-5 Indeno(1,2,3-cd)pyrene 1670 1760 106 66-116
78-59-1 Isophorone 1670 1230 74 42-89
90-12-0 1-Methylnaphthalene 1670 1230 74 49-106
91-57-6 2-Methylnaphthalene 1670 1290 77 47-106
91-20-3 Naphthalene 1670 1200 72 44-104
98-95-3 Nitrobenzene 1670 1220 73 43-108
621-64-7 N-Nitrosodi-n-propylamine 1670 1140 68 48-108
86-30-6 N-Nitrosodiphenylamine 1670 1470 88 62-110
85-01-8 Phenanthrene 1670 1450 87 63-111
129-00-0 Pyrene 1670 1540 92 65-115
120-82-1 1,2,4-Trichlorobenzene 1670 1230 74 45-100
CAS No.Surrogate Recoveries BSP Limits
367-12-4 2-Fluorophenol 71%40-102%
4165-62-2 Phenol-d5 76%41-100%
118-79-6 2,4,6-Tribromophenol 92%42-108%
4165-60-0 Nitrobenzene-d5 71%40-105%
321-60-8 2-Fluorobiphenyl 78%43-107%
1718-51-0 Terphenyl-d14 81%45-119%
* = Outside of Control Limits.
30 of 45
FA6676066.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA66760
Account:RENCM Resolve Environmental
Project:Monroe Lot 3; Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP76324-MS X066495.D 1 08/12/19 MV 08/12/19 OP76324 SX2738
OP76324-MSD X066496.D 1 08/12/19 MV 08/12/19 OP76324 SX2738
FA66913-1 X066494.D 1 08/12/19 MV 08/12/19 OP76324 SX2738
The QC reported here applies to the following samples:Method: SW846 8270E
FA66760-1
FA66913-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
65-85-0 Benzoic Acid ND 3860 557 14*3890 462 12*19 36-118/41
59-50-7 4-Chloro-3-methyl Phenol ND 1930 1550 80 1940 1740 90 12 52-108/21
95-57-8 2-Chlorophenol ND 1930 1280 66 1940 1290 66 1 48-104/26
120-83-2 2,4-Dichlorophenol ND 1930 1380 72 1940 1500 77 8 51-105/27
105-67-9 2,4-Dimethylphenol ND 1930 1420 74 1940 1480 76 4 43-96/23
51-28-5 2,4-Dinitrophenol ND 3860 653 17*3890 433 11*41*40-119/32
534-52-1 4,6-Dinitro-o-cresol ND 3860 1210 31*3890 1190 31*2 64-121/29
95-48-7 2-Methylphenol ND 1930 1210 63 1940 1230 63 2 46-107/24
3&4-Methylphenol ND 3860 2490 65 3890 2560 66 3 44-111/24
88-75-5 2-Nitrophenol ND 1930 1350 70 1940 1390 72 3 49-104/27
100-02-7 4-Nitrophenol ND 3860 2080 54*3890 2380 61 13 56-116/23
87-86-5 Pentachlorophenol ND 3860 827 21*3890 823 21*0 61-114/23
108-95-2 Phenol ND 1930 1430 74 1940 1370 71 4 45-110/24
88-06-2 2,4,6-Trichlorophenol ND 1930 605 31*1940 811 42*29*56-109/25
83-32-9 Acenaphthene 82.2 J 1930 1600 79 1940 1720 84 7 56-109/23
208-96-8 Acenaphthylene ND 1930 1570 81 1940 1720 89 9 56-106/23
120-12-7 Anthracene 352 1930 1400 54*1940 1640 66 16 61-110/21
56-55-3 Benzo(a)anthracene ND 1930 1450 75 1940 1710 88 16 66-111/23
50-32-8 Benzo(a)pyrene ND 1930 1190 62 1940 1420 73 18 59-104/23
205-99-2 Benzo(b)fluoranthene ND 1930 1380 72 1940 1610 83 15 67-113/24
191-24-2 Benzo(g,h,i)perylene ND 1930 1230 64*1940 1470 76 18 67-113/21
207-08-9 Benzo(k)fluoranthene ND 1930 1270 66*1940 1520 78 18 67-114/22
100-51-6 Benzyl Alcohol ND 1930 1170 61 1940 1190 61 2 53-108/24
101-55-3 4-Bromophenyl phenyl ether ND 1930 1560 81 1940 1950 100 22*62-110/21
85-68-7 Butyl benzyl phthalate ND 1930 1650 86 1940 1880 97 13 65-113/20
106-47-8 4-Chloroaniline ND 1930 1040 54 1940 1350 69 26 30-115/30
111-91-1 bis(2-Chloroethoxy)methane ND 1930 1370 71 1940 1390 72 1 48-105/24
111-44-4 bis(2-Chloroethyl)ether ND 1930 1160 60 1940 1160 60 0 46-103/27
108-60-1 2,2'-Oxybis(1-chloropropane)ND 1930 1160 60 1940 1150 59 1 40-110/25
91-58-7 2-Chloronaphthalene ND 1930 1440 75 1940 1560 80 8 53-106/23
7005-72-3 4-Chlorophenyl phenyl ether ND 1930 1520 79 1940 1730 89 13 58-106/21
218-01-9 Chrysene ND 1930 1410 73 1940 1670 86 17 65-112/25
53-70-3 Dibenzo(a,h)anthracene ND 1930 1280 66*1940 1510 78 16 68-115/23
132-64-9 Dibenzofuran ND 1930 1590 82 1940 1750 90 10 57-108/22
95-50-1 1,2-Dichlorobenzene ND 1930 1140 59 1940 1140 59 0 44-102/28
541-73-1 1,3-Dichlorobenzene ND 1930 1130 59 1940 1140 59 1 42-100/30
* = Outside of Control Limits.
31 of 45
FA6676066.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA66760
Account:RENCM Resolve Environmental
Project:Monroe Lot 3; Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP76324-MS X066495.D 1 08/12/19 MV 08/12/19 OP76324 SX2738
OP76324-MSD X066496.D 1 08/12/19 MV 08/12/19 OP76324 SX2738
FA66913-1 X066494.D 1 08/12/19 MV 08/12/19 OP76324 SX2738
The QC reported here applies to the following samples:Method: SW846 8270E
FA66760-1
FA66913-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
106-46-7 1,4-Dichlorobenzene ND 1930 1110 58 1940 1120 58 1 40-106/29
91-94-1 3,3'-Dichlorobenzidine ND 1930 1250 65 1940 1590 82 24 36-114/28
84-66-2 Diethyl Phthalate ND 1930 1520 79 1940 1740 90 13 61-109/20
131-11-3 Dimethyl Phthalate ND 1930 1540 80 1940 1750 90 13 59-108/20
117-84-0 Di-n-octyl Phthalate 51.7 J 1930 1640 82 1940 1910 96 15 64-119/21
84-74-2 Di-n-butyl Phthalate 95.5 J 1930 1630 80 1940 1880 92 14 63-108/19
122-66-7 1,2-Diphenylhydrazine ND 1930 1210 63 1940 1350 69 11 58-112/22
117-81-7 bis(2-Ethylhexyl)phthalate ND 1930 1600 83 1940 1870 96 16 64-115/23
206-44-0 Fluoranthene 27.0 J 1930 1530 78 1940 1840 93 18 60-108/25
86-73-7 Fluorene 145 J 1930 1670 79 1940 1830 87 9 58-109/21
118-74-1 Hexachlorobenzene ND 1930 1460 76 1940 1720 89 16 59-111/21
87-68-3 Hexachlorobutadiene ND 1930 1280 66 1940 1340 69 5 41-108/27
77-47-4 Hexachlorocyclopentadiene ND 1930 890 46*1940 1070 55 18 49-110/31
67-72-1 Hexachloroethane ND 1930 1180 61 1940 1190 61 1 40-105/32
193-39-5 Indeno(1,2,3-cd)pyrene ND 1930 1280 66 1940 1560 80 20 66-116/22
78-59-1 Isophorone ND 1930 1230 64 1940 1260 65 2 42-89/22
90-12-0 1-Methylnaphthalene 779 1930 2270 77 1940 2230 75 2 49-106/26
91-57-6 2-Methylnaphthalene 1190 1930 2820 84 1940 2740 80 3 47-106/27
91-20-3 Naphthalene 262 1930 1610 70 1940 1620 70 1 44-104/27
98-95-3 Nitrobenzene ND 1930 1230 64 1940 1230 63 0 43-108/25
621-64-7 N-Nitrosodi-n-propylamine ND 1930 1160 60 1940 1170 60 1 48-108/27
86-30-6 N-Nitrosodiphenylamine ND 1930 2040 106 1940 2180 112*7 62-110/21
85-01-8 Phenanthrene 371 1930 1850 77 1940 2020 85 9 63-111/22
129-00-0 Pyrene 187 J 1930 1790 83 1940 1960 91 9 65-115/25
120-82-1 1,2,4-Trichlorobenzene ND 1930 1330 69 1940 1380 71 4 45-100/26
CAS No.Surrogate Recoveries MS MSD FA66913-1 Limits
367-12-4 2-Fluorophenol 59%58%65%40-102%
4165-62-2 Phenol-d5 66%66%71%41-100%
118-79-6 2,4,6-Tribromophenol 32%*43%41%* a 42-108%
4165-60-0 Nitrobenzene-d5 64%63%66%40-105%
321-60-8 2-Fluorobiphenyl 74%79%78%43-107%
1718-51-0 Terphenyl-d14 73%81%82%45-119%
* = Outside of Control Limits.
32 of 45
FA6676066.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA66760
Account:RENCM Resolve Environmental
Project:Monroe Lot 3; Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP76324-MS X066495.D 1 08/12/19 MV 08/12/19 OP76324 SX2738
OP76324-MSD X066496.D 1 08/12/19 MV 08/12/19 OP76324 SX2738
FA66913-1 X066494.D 1 08/12/19 MV 08/12/19 OP76324 SX2738
The QC reported here applies to the following samples:Method: SW846 8270E
FA66760-1
(a) Outside control limits due to matrix interference. Confirmed by MS/MSD.
* = Outside of Control Limits.
33 of 45
FA6676066.3.1
SGS North America Inc.
Metals Analysis
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Matrix Spike and Duplicate Summaries
• Blank Spike and Lab Control Sample Summaries
• Serial Dilution Summaries
Orlando, FL
Section 7
34 of 45
FA667607
BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: FA66760
Account: RENCM - Resolve Environmental
Project: Monroe Lot 3; Monroe, NC
QC Batch ID: MP35931 Methods: SW846 6010D
Matrix Type: SOLID Units: mg/kg
Prep Date: 08/09/19
MB
Metal RL IDL MDL raw final
Aluminum 10 .7 1.8
Antimony 1.0 .05 .065
Arsenic 0.50 .065 .1 -0.14 <0.50
Barium 10 .05 .05 0.025 <10
Beryllium 0.25 .01 .025
Cadmium 0.20 .01 .025 0.00050 <0.20
Calcium 250 2.5 2.5
Chromium 0.50 .05 .05 0.030 <0.50
Cobalt 2.5 .01 .025
Copper 1.3 .05 .05
Iron 15 .85 .85
Lead 1.0 .05 .05 -0.030 <1.0
Magnesium 250 1.8 1.8
Manganese 0.75 .025 .025
Molybdenum 2.5 .015 .025
Nickel 2.0 .02 .025
Potassium 500 10 10
Selenium 1.0 .12 .12 -0.080 <1.0
Silver 0.50 .035 .041 -0.010 <0.50
Sodium 500 25 25
Strontium 0.50 .025 .025
Thallium 0.50 .055 .055
Tin 2.5 .045 .045
Titanium 0.50 .025 .025
Vanadium 2.5 .025 .025
Zinc 1.0 .15 .15
Associated samples MP35931: FA66760-1
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
35 of 45
FA6676077.1.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA66760
Account: RENCM - Resolve Environmental
Project: Monroe Lot 3; Monroe, NC
QC Batch ID: MP35931 Methods: SW846 6010D
Matrix Type: SOLID Units: mg/kg
Prep Date: 08/09/19 08/09/19
FA66805-1 QC FA66805-1 Spikelot QC
Metal Original DUP RPD Limits Original MS MPFLICP2 % Rec Limits
Aluminum
Antimony
Arsenic 0.56 0.58 3.5 0-20 0.56 88.9 108 81.9 80-120
Barium 12.2 12.1 0.8 0-20 12.2 97.2 108 78.8N(a) 80-120
Beryllium
Cadmium 0.0 0.0 NC 0-20 0.0 2.3 2.7 85.3 80-120
Calcium
Chromium 3.5 3.9 10.8 0-20 3.5 13.6 10.8 93.6 80-120
Cobalt
Copper
Iron
Lead 2.6 2.7 3.8 0-20 2.6 27.4 27 91.9 80-120
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 0.0 0.0 NC 0-20 0.0 87.6 108 81.2 80-120
Silver 0.0 0.0 NC 0-20 0.0 2.3 2.7 85.3 80-120
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP35931: FA66760-1
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
(a) Spike recovery indicates possible matrix interference and/or sample non-homogeneity.
_________________________________________________________________________________________________________
Page 1
36 of 45
FA6676077.1.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA66760
Account: RENCM - Resolve Environmental
Project: Monroe Lot 3; Monroe, NC
QC Batch ID: MP35931 Methods: SW846 6010D
Matrix Type: SOLID Units: mg/kg
Prep Date: 08/09/19
FA66805-1 Spikelot MSD QC
Metal Original MSD MPFLICP2 % Rec RPD Limit
Aluminum
Antimony
Arsenic 0.56 89.1 112 78.9N(a) 0.2 20
Barium 12.2 103 112 80.9 5.8 20
Beryllium
Cadmium 0.0 2.3 2.81 82.0 0.0 20
Calcium
Chromium 3.5 15.4 11.2 106.0 12.4 20
Cobalt
Copper
Iron
Lead 2.6 29.9 28.1 97.3 8.7 20
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 0.0 88.3 112 78.7N(a) 0.8 20
Silver 0.0 2.3 2.81 82.0 0.0 20
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP35931: FA66760-1
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
(a) Spike recovery indicates possible matrix interference and/or sample non-homogeneity.
_________________________________________________________________________________________________________
Page 2
37 of 45
FA6676077.1.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA66760
Account: RENCM - Resolve Environmental
Project: Monroe Lot 3; Monroe, NC
QC Batch ID: MP35931 Methods: SW846 6010D
Matrix Type: SOLID Units: mg/kg
Prep Date: 08/09/19
BSP Spikelot QC
Metal Result MPFLICP2 % Rec Limits
Aluminum
Antimony
Arsenic 94.2 100 94.2 80-120
Barium 94.4 100 94.4 80-120
Beryllium
Cadmium 2.5 2.5 100.0 80-120
Calcium
Chromium 10.3 10 103.0 80-120
Cobalt
Copper
Iron
Lead 22.7 25 90.8 80-120
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 94.6 100 94.6 80-120
Silver 2.4 2.5 96.0 80-120
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP35931: FA66760-1
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
38 of 45
FA6676077.1.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: FA66760
Account: RENCM - Resolve Environmental
Project: Monroe Lot 3; Monroe, NC
QC Batch ID: MP35931 Methods: SW846 6010D
Matrix Type: SOLID Units: ug/l
Prep Date: 08/09/19
FA66805-1 QC
Metal Original SDL 1:5 %DIF Limits
Aluminum
Antimony
Arsenic 10.5 8.60 18.1 (a) 0-10
Barium 229 280 22.2*(b) 0-10
Beryllium
Cadmium 0.00 0.00 NC 0-10
Calcium
Chromium 64.7 80.7 24.7*(b) 0-10
Cobalt
Copper
Iron
Lead 48.5 52.7 8.7 0-10
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 0.00 0.00 NC 0-10
Silver 0.00 0.00 NC 0-10
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP35931: FA66760-1
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
(b) Serial dilution indicates possible matrix interference.
_________________________________________________________________________________________________________
Page 1
39 of 45
FA6676077.1.4
POST DIGESTATE SPIKE SUMMARY
Login Number: FA66760
Account: RENCM - Resolve Environmental
Project: Monroe Lot 3; Monroe, NC
QC Batch ID: MP35931 Methods: SW846 6010D
Matrix Type: SOLID Units: ug/l
Prep Date: 08/09/19
Sample Final FA66805-1 PS Spike Spike Spike QC
Metal ml ml Raw Corr.** ug/l ml ug/ml ug/l % Rec Limits
Aluminum
Antimony
Arsenic 9.8 10 10.5 10.29 100.8 0.2 5 100 90.5 80-120
Barium 9.8 10 229 224.42 422.4 0.2 12.5 250 79.2*(a) 80-120
Beryllium
Cadmium 9.8 10 43.45 0.2 2.5 50 86.9 80-120
Calcium
Chromium 9.8 10 64.7 63.406 108.1 0.2 2.5 50 89.4 80-120
Cobalt
Copper
Iron
Lead 9.8 10 48.5 47.53 95 0.2 2.5 50 94.9 80-120
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium 9.8 10 82.9 0.2 5 100 82.9 80-120
Silver 9.8 10 41.1 0.2 2.5 50 82.2 80-120
Sodium
Strontium
Thallium
Tin
Titanium
Vanadium
Zinc
Associated samples MP35931: FA66760-1
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(**) Corr. sample result = Raw * (sample volume / final volume)
(anr) Analyte not requested
(a) Spike recovery indicates possible matrix interference and/or sample non-homogeneity.
_________________________________________________________________________________________________________
Page 1
40 of 45
FA6676077.1.5
BLANK RESULTS SUMMARY
Part 2 - Method Blanks
Login Number: FA66760
Account: RENCM - Resolve Environmental
Project: Monroe Lot 3; Monroe, NC
QC Batch ID: MP35947 Methods: SW846 7471B
Matrix Type: SOLID Units: mg/kg
Prep Date: 08/12/19
MB
Metal RL IDL MDL raw final
Mercury 0.042 .0025 .0042 0.00036 <0.042
Associated samples MP35947: FA66760-1
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
41 of 45
FA6676077.2.1
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA66760
Account: RENCM - Resolve Environmental
Project: Monroe Lot 3; Monroe, NC
QC Batch ID: MP35947 Methods: SW846 7471B
Matrix Type: SOLID Units: mg/kg
Prep Date: 08/12/19 08/12/19
FA66717-1 QC FA66717-1 Spikelot QC
Metal Original DUP RPD Limits Original MS HGFLWS1 % Rec Limits
Mercury 0.021 0.020 4.9 0-20 0.021 0.36 0.295 114.7 80-120
Associated samples MP35947: FA66760-1
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
42 of 45
FA6676077.2.2
MATRIX SPIKE AND DUPLICATE RESULTS SUMMARY
Login Number: FA66760
Account: RENCM - Resolve Environmental
Project: Monroe Lot 3; Monroe, NC
QC Batch ID: MP35947 Methods: SW846 7471B
Matrix Type: SOLID Units: mg/kg
Prep Date: 08/12/19
FA66717-1 Spikelot MSD QC
Metal Original MSD HGFLWS1 % Rec RPD Limit
Mercury 0.021 0.34 0.287 111.3 5.7 20
Associated samples MP35947: FA66760-1
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(N) Matrix Spike Rec. outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 2
43 of 45
FA6676077.2.2
SPIKE BLANK AND LAB CONTROL SAMPLE SUMMARY
Login Number: FA66760
Account: RENCM - Resolve Environmental
Project: Monroe Lot 3; Monroe, NC
QC Batch ID: MP35947 Methods: SW846 7471B
Matrix Type: SOLID Units: mg/kg
Prep Date: 08/12/19
BSP Spikelot QC
Metal Result HGFLWS1 % Rec Limits
Mercury 0.27 0.25 108.0 80-120
Associated samples MP35947: FA66760-1
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
_________________________________________________________________________________________________________
Page 1
44 of 45
FA6676077.2.3
SERIAL DILUTION RESULTS SUMMARY
Login Number: FA66760
Account: RENCM - Resolve Environmental
Project: Monroe Lot 3; Monroe, NC
QC Batch ID: MP35947 Methods: SW846 7471B
Matrix Type: SOLID Units: ug/l
Prep Date: 08/12/19
FA66717-1 QC
Metal Original SDL 1:5 %DIF Limits
Mercury 0.197 0.00 100.0(a) 0-10
Associated samples MP35947: FA66760-1
Results < IDL are shown as zero for calculation purposes
(*) Outside of QC limits
(anr) Analyte not requested
(a) Percent difference acceptable due to low initial sample concentration (< 50 times IDL).
_________________________________________________________________________________________________________
Page 1
45 of 45
FA6676077.2.4
09/18/19
Technical Report for
Resolve Environmental
Five Points Gateway; 320/322 Franklin, Monroe, NC
SGS Job Number: FA67097A
Sampling Date: 08/13/19
Report to:
Resolve Environmental
500 Devonport Dr
Matthews, NC 28104
[e-mail]
ATTN: Laura Minor
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Orlando, FL 09/18/19
Reissue #1
e-Hardcopy 2.0
Automated Report
23
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
[e-mail]
1 of 23
FA67097A
Florida  4405 Vineland Road  Suite C-15  Orlando, FL 32811  tel: [phone]  fax: [phone]

September 18, 2019

Ms. Laura Minor
Resolve
500 Devonport Dr
Matthews, NC 28104

RE: SGS North America Inc. - Orlando job FA67097A Reissue

Dear Ms. Minor,

The final report for job number FA67097A has been edited to reflect requested corrections.
These edits have been incorporated into the revised report.

The collection date has been revised.

SGS North America Inc. - Orlando apologies for any inconvenience this may have caused.
Please feel free to contact us if we can be of further assistance.

Sincerely,

SGS North America, Inc. - Orlando

2 of 23
FA67097A
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................4
Section 2: Summary of Hits ....................................................................................................5
Section 3: Sample Results ........................................................................................................6
3.1: FA67097-6: STOCKPILE .............................................................................................7
Section 4: Misc. Forms ............................................................................................................10
4.1: Chain of Custody ...........................................................................................................11
Section 5: MS Volatiles - QC Data Summaries .....................................................................14
5.1: Method Blank Summary ................................................................................................15
5.2: Blank Spike Summary ...................................................................................................18
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................21 123453 of 23
FA67097A
SGS North America Inc.
Sample Summary
Resolve Environmental
Job No:FA67097A
Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FA67097-6 08/13/19 09:43 SB 08/16/19 SO Soil STOCKPILE
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
4 of 23
FA67097A1
Summary of Hits Page 1 of 1
Job Number:FA67097A
Account:Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Collected:08/13/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA67097-6 STOCKPILE
No hits reported in this sample.
5 of 23
FA67097A2
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
6 of 23
FA67097A3
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:STOCKPILE
Lab Sample ID:FA67097-6 Date Sampled:08/13/19
Matrix:SO - Soil Date Received:08/16/19
Method:SW846 8260D Percent Solids:93.8
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 3C6493.D 1 08/19/19 19:45 SP n/a n/a V3C262
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 4.45 g 5.0 ml 100 ul
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 13 6.3 mg/kg
71-43-2 Benzene ND 0.32 0.077 mg/kg
108-86-1 Bromobenzene ND 0.32 0.063 mg/kg
74-97-5 Bromochloromethane ND 0.32 0.094 mg/kg
75-27-4 Bromodichloromethane ND 0.32 0.063 mg/kg
75-25-2 Bromoform ND 0.32 0.063 mg/kg
78-93-3 2-Butanone (MEK)ND 1.6 0.46 mg/kg
104-51-8 n-Butylbenzene ND 0.32 0.063 mg/kg
135-98-8 sec-Butylbenzene ND 0.32 0.063 mg/kg
98-06-6 tert-Butylbenzene ND 0.32 0.063 mg/kg
56-23-5 Carbon Tetrachloride ND 0.32 0.064 mg/kg
108-90-7 Chlorobenzene ND 0.32 0.063 mg/kg
75-00-3 Chloroethane ND 0.32 0.13 mg/kg
67-66-3 Chloroform ND 0.32 0.084 mg/kg
95-49-8 o-Chlorotoluene ND 0.32 0.063 mg/kg
106-43-4 p-Chlorotoluene ND 0.32 0.063 mg/kg
124-48-1 Dibromochloromethane ND 0.32 0.063 mg/kg
106-93-4 1,2-Dibromoethane ND 0.32 0.063 mg/kg
75-71-8 Dichlorodifluoromethane ND 0.32 0.13 mg/kg
95-50-1 1,2-Dichlorobenzene ND 0.32 0.063 mg/kg
541-73-1 1,3-Dichlorobenzene ND 0.32 0.063 mg/kg
106-46-7 1,4-Dichlorobenzene ND 0.32 0.073 mg/kg
75-34-3 1,1-Dichloroethane ND 0.32 0.11 mg/kg
107-06-2 1,2-Dichloroethane ND 0.32 0.063 mg/kg
75-35-4 1,1-Dichloroethylene ND 0.32 0.063 mg/kg
156-59-2 cis-1,2-Dichloroethylene ND 0.32 0.087 mg/kg
156-60-5 trans-1,2-Dichloroethylene ND 0.32 0.063 mg/kg
78-87-5 1,2-Dichloropropane ND 0.32 0.063 mg/kg
142-28-9 1,3-Dichloropropane ND 0.32 0.063 mg/kg
594-20-7 2,2-Dichloropropane ND 0.32 0.063 mg/kg
563-58-6 1,1-Dichloropropene ND 0.32 0.064 mg/kg
10061-01-5 cis-1,3-Dichloropropene ND 0.32 0.063 mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 23
FA67097A33.1
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:STOCKPILE
Lab Sample ID:FA67097-6 Date Sampled:08/13/19
Matrix:SO - Soil Date Received:08/16/19
Method:SW846 8260D Percent Solids:93.8
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 0.32 0.063 mg/kg
108-20-3 Di-Isopropyl Ether ND 0.32 0.15 mg/kg
64-17-5 Ethyl Alcohol ND 25 4.7 mg/kg
100-41-4 Ethylbenzene ND 0.32 0.063 mg/kg
591-78-6 2-Hexanone ND 1.6 0.47 mg/kg
98-82-8 Isopropylbenzene ND 0.32 0.063 mg/kg
99-87-6 p-Isopropyltoluene ND 0.32 0.063 mg/kg
74-83-9 Methyl Bromide ND 0.32 0.13 mg/kg
74-87-3 Methyl Chloride ND 0.32 0.13 mg/kg
75-09-2 Methylene Chloride ND 1.3 0.70 mg/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 1.6 0.47 mg/kg
1634-04-4 Methyl Tert Butyl Ether ND 0.32 0.063 mg/kg
91-20-3 Naphthalene ND 0.32 0.13 mg/kg
103-65-1 n-Propylbenzene ND 0.32 0.063 mg/kg
100-42-5 Styrene ND 0.32 0.063 mg/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 0.32 0.065 mg/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 0.32 0.063 mg/kg
127-18-4 Tetrachloroethylene ND 0.32 0.081 mg/kg
108-88-3 Toluene ND 1.3 0.63 mg/kg
87-61-6 1,2,3-Trichlorobenzene ND 0.32 0.088 mg/kg
120-82-1 1,2,4-Trichlorobenzene ND 0.32 0.063 mg/kg
71-55-6 1,1,1-Trichloroethane ND 0.32 0.063 mg/kg
79-00-5 1,1,2-Trichloroethane ND 0.32 0.063 mg/kg
79-01-6 Trichloroethylene ND 0.32 0.063 mg/kg
75-69-4 Trichlorofluoromethane ND 0.32 0.13 mg/kg
96-18-4 1,2,3-Trichloropropane ND 0.32 0.079 mg/kg
95-63-6 1,2,4-Trimethylbenzene ND 0.32 0.063 mg/kg
108-67-8 1,3,5-Trimethylbenzene ND 0.32 0.063 mg/kg
108-05-4 Vinyl Acetate ND 1.6 1.0 mg/kg
75-01-4 Vinyl Chloride ND 0.32 0.063 mg/kg
m,p-Xylene ND 0.63 0.070 mg/kg
95-47-6 o-Xylene ND 0.32 0.063 mg/kg
1330-20-7 Xylene (total)ND 0.95 0.13 mg/kg
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 101%75-124%
17060-07-0 1,2-Dichloroethane-D4 98%72-135%
2037-26-5 Toluene-D8 90%75-126%
460-00-4 4-Bromofluorobenzene 94%71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 23
FA67097A33.1
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:STOCKPILE
Lab Sample ID:FA67097-6 Date Sampled:08/13/19
Matrix:SO - Soil Date Received:08/16/19
Method:SW846 8260D Percent Solids:93.8
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Dilution required due to matrix interference (sample foamed).
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 23
FA67097A33.1
SGS North America Inc.
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
10 of 23
FA67097A4
FA67097A: Chain of Custody
Page 1 of 3
11 of 23
FA67097A44.1
Job Number:FA67097 Client:RESOLVE ENVIRONMENTAL SERVICES,
Date / Time Received:8/16/2019 8:45:00 AM Delivery Method:FED EX
Project:FIVE POINTS GATEWAY
Airbill #'s:
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (1.0);
Cooler 1: (2.0);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:1Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:1; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:PETERH SP Date:8/16/2019Date:8/16/2019 8:45:00 AM
FA67097A: Chain of Custody
Page 2 of 3
12 of 23
FA67097A44.1
Job Change Order: FA67097
Requested Date: 8/16/2019 Received Date: 8/16/2019
Account Name: Resolve Environmental Due Date: 8/23/2019
Project Five Points Gateway; 320/322 Franklin, Monroe, Deliverable: COMMB
CSR: MM TAT (Days): 7
Sample #: Change: Per client Stockpile sample should be reported in a FA67097-6 separate report. Sample has been moved to FA67097A.
Above Changes Per: Laura Minor Date: 8/16/2019
To Client: This Change Order is confirmation of the revisions, previously discussed with the Client Service Representative.
Page 1 of 1
FA67097A: Chain of Custody
Page 3 of 3
13 of 23
FA67097A44.1
SGS North America Inc.
MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
14 of 23
FA67097A5
Method Blank Summary Page 1 of 3
Job Number:FA67097A
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C262-MB 3C6483.D 1 08/19/19 SP n/a n/a V3C262
The QC reported here applies to the following samples:Method: SW846 8260D
FA67097-6
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 200 100 ug/kg
71-43-2 Benzene ND 5.0 1.2 ug/kg
108-86-1 Bromobenzene ND 5.0 1.0 ug/kg
74-97-5 Bromochloromethane ND 5.0 1.5 ug/kg
75-27-4 Bromodichloromethane ND 5.0 1.0 ug/kg
75-25-2 Bromoform ND 5.0 1.0 ug/kg
78-93-3 2-Butanone (MEK)ND 25 7.3 ug/kg
104-51-8 n-Butylbenzene ND 5.0 1.0 ug/kg
135-98-8 sec-Butylbenzene ND 5.0 1.0 ug/kg
98-06-6 tert-Butylbenzene ND 5.0 1.0 ug/kg
56-23-5 Carbon Tetrachloride ND 5.0 1.0 ug/kg
108-90-7 Chlorobenzene ND 5.0 1.0 ug/kg
75-00-3 Chloroethane ND 5.0 2.0 ug/kg
67-66-3 Chloroform ND 5.0 1.3 ug/kg
95-49-8 o-Chlorotoluene ND 5.0 1.0 ug/kg
106-43-4 p-Chlorotoluene ND 5.0 1.0 ug/kg
124-48-1 Dibromochloromethane ND 5.0 1.0 ug/kg
106-93-4 1,2-Dibromoethane ND 5.0 1.0 ug/kg
75-71-8 Dichlorodifluoromethane ND 5.0 2.0 ug/kg
95-50-1 1,2-Dichlorobenzene ND 5.0 1.0 ug/kg
541-73-1 1,3-Dichlorobenzene ND 5.0 1.0 ug/kg
106-46-7 1,4-Dichlorobenzene ND 5.0 1.2 ug/kg
75-34-3 1,1-Dichloroethane ND 5.0 1.8 ug/kg
107-06-2 1,2-Dichloroethane ND 5.0 1.0 ug/kg
75-35-4 1,1-Dichloroethylene ND 5.0 1.0 ug/kg
156-59-2 cis-1,2-Dichloroethylene ND 5.0 1.4 ug/kg
156-60-5 trans-1,2-Dichloroethylene ND 5.0 1.0 ug/kg
78-87-5 1,2-Dichloropropane ND 5.0 1.0 ug/kg
142-28-9 1,3-Dichloropropane ND 5.0 1.0 ug/kg
594-20-7 2,2-Dichloropropane ND 5.0 1.0 ug/kg
563-58-6 1,1-Dichloropropene ND 5.0 1.0 ug/kg
10061-01-5 cis-1,3-Dichloropropene ND 5.0 1.0 ug/kg
10061-02-6 trans-1,3-Dichloropropene ND 5.0 1.0 ug/kg
108-20-3 Di-Isopropyl Ether ND 5.0 2.3 ug/kg
64-17-5 Ethyl Alcohol ND 400 75 ug/kg
100-41-4 Ethylbenzene ND 5.0 1.0 ug/kg
15 of 23
FA67097A55.1.1
Method Blank Summary Page 2 of 3
Job Number:FA67097A
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C262-MB 3C6483.D 1 08/19/19 SP n/a n/a V3C262
The QC reported here applies to the following samples:Method: SW846 8260D
FA67097-6
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 25 7.5 ug/kg
98-82-8 Isopropylbenzene ND 5.0 1.0 ug/kg
99-87-6 p-Isopropyltoluene ND 5.0 1.0 ug/kg
74-83-9 Methyl Bromide ND 5.0 2.0 ug/kg
74-87-3 Methyl Chloride ND 5.0 2.0 ug/kg
75-09-2 Methylene Chloride ND 20 11 ug/kg
108-10-1 4-Methyl-2-pentanone (MIBK)ND 25 7.5 ug/kg
1634-04-4 Methyl Tert Butyl Ether ND 5.0 1.0 ug/kg
91-20-3 Naphthalene ND 5.0 2.0 ug/kg
103-65-1 n-Propylbenzene ND 5.0 1.0 ug/kg
100-42-5 Styrene ND 5.0 1.0 ug/kg
630-20-6 1,1,1,2-Tetrachloroethane ND 5.0 1.0 ug/kg
79-34-5 1,1,2,2-Tetrachloroethane ND 5.0 1.0 ug/kg
127-18-4 Tetrachloroethylene ND 5.0 1.3 ug/kg
108-88-3 Toluene ND 20 10 ug/kg
87-61-6 1,2,3-Trichlorobenzene ND 5.0 1.4 ug/kg
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.0 ug/kg
71-55-6 1,1,1-Trichloroethane ND 5.0 1.0 ug/kg
79-00-5 1,1,2-Trichloroethane ND 5.0 1.0 ug/kg
79-01-6 Trichloroethylene ND 5.0 1.0 ug/kg
75-69-4 Trichlorofluoromethane ND 5.0 2.0 ug/kg
96-18-4 1,2,3-Trichloropropane ND 5.0 1.3 ug/kg
95-63-6 1,2,4-Trimethylbenzene ND 5.0 1.0 ug/kg
108-67-8 1,3,5-Trimethylbenzene ND 5.0 1.0 ug/kg
108-05-4 Vinyl Acetate ND 25 16 ug/kg
75-01-4 Vinyl Chloride ND 5.0 1.0 ug/kg
m,p-Xylene ND 10 1.1 ug/kg
95-47-6 o-Xylene ND 5.0 1.0 ug/kg
1330-20-7 Xylene (total)ND 15 2.1 ug/kg
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 106%75-124%
17060-07-0 1,2-Dichloroethane-D4 99%72-135%
2037-26-5 Toluene-D8 88%75-126%
16 of 23
FA67097A55.1.1
Method Blank Summary Page 3 of 3
Job Number:FA67097A
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C262-MB 3C6483.D 1 08/19/19 SP n/a n/a V3C262
The QC reported here applies to the following samples:Method: SW846 8260D
FA67097-6
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 95%71-133%
17 of 23
FA67097A55.1.1
Blank Spike Summary Page 1 of 3
Job Number:FA67097A
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C262-BS 3C6482.D 1 08/19/19 SP n/a n/a V3C262
The QC reported here applies to the following samples:Method: SW846 8260D
FA67097-6
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
67-64-1 Acetone 250 271 108 61-152
71-43-2 Benzene 50 50.9 102 76-126
108-86-1 Bromobenzene 50 44.8 90 76-122
74-97-5 Bromochloromethane 50 48.8 98 77-120
75-27-4 Bromodichloromethane 50 53.3 107 74-130
75-25-2 Bromoform 50 48.0 96 76-127
78-93-3 2-Butanone (MEK)250 243 97 75-137
104-51-8 n-Butylbenzene 50 48.7 97 71-128
135-98-8 sec-Butylbenzene 50 46.3 93 79-135
98-06-6 tert-Butylbenzene 50 43.1 86 77-133
56-23-5 Carbon Tetrachloride 50 52.8 106 78-133
108-90-7 Chlorobenzene 50 48.5 97 81-129
75-00-3 Chloroethane 50 59.5 119 68-133
67-66-3 Chloroform 50 51.0 102 72-123
95-49-8 o-Chlorotoluene 50 44.6 89 77-129
106-43-4 p-Chlorotoluene 50 44.6 89 80-134
124-48-1 Dibromochloromethane 50 50.9 102 76-127
106-93-4 1,2-Dibromoethane 50 47.9 96 77-126
75-71-8 Dichlorodifluoromethane 50 47.1 94 68-168
95-50-1 1,2-Dichlorobenzene 50 45.4 91 80-129
541-73-1 1,3-Dichlorobenzene 50 47.3 95 81-129
106-46-7 1,4-Dichlorobenzene 50 47.5 95 76-130
75-34-3 1,1-Dichloroethane 50 49.5 99 73-125
107-06-2 1,2-Dichloroethane 50 47.3 95 74-128
75-35-4 1,1-Dichloroethylene 50 50.1 100 81-136
156-59-2 cis-1,2-Dichloroethylene 50 50.3 101 74-126
156-60-5 trans-1,2-Dichloroethylene 50 48.3 97 70-127
78-87-5 1,2-Dichloropropane 50 50.7 101 74-125
142-28-9 1,3-Dichloropropane 50 44.7 89 76-122
594-20-7 2,2-Dichloropropane 50 50.6 101 77-133
563-58-6 1,1-Dichloropropene 50 51.1 102 75-130
10061-01-5 cis-1,3-Dichloropropene 50 49.8 100 80-123
10061-02-6 trans-1,3-Dichloropropene 50 49.1 98 75-131
108-20-3 Di-Isopropyl Ether 50 45.6 91 75-122
64-17-5 Ethyl Alcohol 1000 905 91 53-154
100-41-4 Ethylbenzene 50 48.1 96 77-123
* = Outside of Control Limits.
18 of 23
FA67097A55.2.1
Blank Spike Summary Page 2 of 3
Job Number:FA67097A
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C262-BS 3C6482.D 1 08/19/19 SP n/a n/a V3C262
The QC reported here applies to the following samples:Method: SW846 8260D
FA67097-6
Spike BSP BSP
CAS No.Compound ug/kg ug/kg %Limits
591-78-6 2-Hexanone 250 226 90 72-133
98-82-8 Isopropylbenzene 50 50.9 102 80-136
99-87-6 p-Isopropyltoluene 50 47.2 94 77-131
74-83-9 Methyl Bromide 50 50.3 101 65-139
74-87-3 Methyl Chloride 50 49.3 99 71-144
75-09-2 Methylene Chloride 50 50.0 100 74-137
108-10-1 4-Methyl-2-pentanone (MIBK)250 226 90 76-132
1634-04-4 Methyl Tert Butyl Ether 50 46.2 92 77-120
91-20-3 Naphthalene 50 44.2 88 79-129
103-65-1 n-Propylbenzene 50 45.2 90 80-135
100-42-5 Styrene 50 48.3 97 78-125
630-20-6 1,1,1,2-Tetrachloroethane 50 50.6 101 78-126
79-34-5 1,1,2,2-Tetrachloroethane 50 44.4 89 71-126
127-18-4 Tetrachloroethylene 50 52.4 105 79-130
108-88-3 Toluene 50 47.9 96 76-124
87-61-6 1,2,3-Trichlorobenzene 50 46.1 92 77-128
120-82-1 1,2,4-Trichlorobenzene 50 48.4 97 78-130
71-55-6 1,1,1-Trichloroethane 50 51.0 102 70-129
79-00-5 1,1,2-Trichloroethane 50 47.0 94 74-124
79-01-6 Trichloroethylene 50 52.2 104 75-128
75-69-4 Trichlorofluoromethane 50 58.1 116 73-145
96-18-4 1,2,3-Trichloropropane 50 41.4 83 74-127
95-63-6 1,2,4-Trimethylbenzene 50 44.1 88 74-123
108-67-8 1,3,5-Trimethylbenzene 50 45.8 92 73-122
108-05-4 Vinyl Acetate 250 238 95 48-164
75-01-4 Vinyl Chloride 50 48.6 97 76-141
m,p-Xylene 100 98.9 99 80-128
95-47-6 o-Xylene 50 47.9 96 80-132
1330-20-7 Xylene (total)150 147 98 80-129
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 99%75-124%
17060-07-0 1,2-Dichloroethane-D4 91%72-135%
2037-26-5 Toluene-D8 93%75-126%
* = Outside of Control Limits.
19 of 23
FA67097A55.2.1
Blank Spike Summary Page 3 of 3
Job Number:FA67097A
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
V3C262-BS 3C6482.D 1 08/19/19 SP n/a n/a V3C262
The QC reported here applies to the following samples:Method: SW846 8260D
FA67097-6
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 97%71-133%
* = Outside of Control Limits.
20 of 23
FA67097A55.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA67097A
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA67079-1MS 3C6505.D 1 08/20/19 SP n/a n/a V3C262
FA67079-1MSD 3C6506.D 1 08/20/19 SP n/a n/a V3C262
FA67079-1 a 3C6491.D 1 08/19/19 SP n/a n/a V3C262
The QC reported here applies to the following samples:Method: SW846 8260D
FA67097-6
FA67079-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
67-64-1 Acetone ND 10300 11000 106 10300 10500 101 5 61-152/27
71-43-2 Benzene ND 2070 2060 100 2070 2100 101 2 76-126/26
108-86-1 Bromobenzene ND 2070 1920 93 2070 2080 100 8 76-122/32
74-97-5 Bromochloromethane ND 2070 1990 96 2070 2050 99 3 77-120/24
75-27-4 Bromodichloromethane ND 2070 2170 105 2070 2230 108 3 74-130/25
75-25-2 Bromoform ND 2070 2090 101 2070 2170 105 4 76-127/26
78-93-3 2-Butanone (MEK)ND 10300 10300 100 10300 10200 99 1 75-137/25
104-51-8 n-Butylbenzene 95.2 J 2070 2030 93 2070 2080 96 2 71-128/35
135-98-8 sec-Butylbenzene 110 J 2070 2060 94 2070 2120 97 3 79-135/34
98-06-6 tert-Butylbenzene ND 2070 1860 90 2070 1890 91 2 77-133/34
56-23-5 Carbon Tetrachloride ND 2070 2130 103 2070 2140 103 0 78-133/29
108-90-7 Chlorobenzene ND 2070 2080 100 2070 2170 105 4 81-129/29
75-00-3 Chloroethane ND 2070 2110 102 2070 2200 106 4 68-133/29
67-66-3 Chloroform ND 2070 2090 101 2070 2090 101 0 72-123/26
95-49-8 o-Chlorotoluene ND 2070 1870 90 2070 1920 93 3 77-129/33
106-43-4 p-Chlorotoluene ND 2070 1870 90 2070 1920 93 3 80-134/33
124-48-1 Dibromochloromethane ND 2070 2310 112 2070 2380 115 3 76-127/27
106-93-4 1,2-Dibromoethane ND 2070 2160 104 2070 2250 109 4 77-126/26
75-71-8 Dichlorodifluoromethane ND 2070 1860 90 2070 1900 92 2 68-168/29
95-50-1 1,2-Dichlorobenzene ND 2070 1920 93 2070 1990 96 4 80-129/32
541-73-1 1,3-Dichlorobenzene ND 2070 1960 95 2070 2010 97 3 81-129/33
106-46-7 1,4-Dichlorobenzene ND 2070 1940 94 2070 2030 98 5 76-130/32
75-34-3 1,1-Dichloroethane ND 2070 2020 98 2070 2040 99 1 73-125/27
107-06-2 1,2-Dichloroethane ND 2070 2000 97 2070 2010 97 0 74-128/23
75-35-4 1,1-Dichloroethylene ND 2070 2060 100 2070 2050 99 0 81-136/28
156-59-2 cis-1,2-Dichloroethylene ND 2070 2040 99 2070 2090 101 2 74-126/26
156-60-5 trans-1,2-Dichloroethylene ND 2070 1950 94 2070 1990 96 2 70-127/27
78-87-5 1,2-Dichloropropane ND 2070 2080 100 2070 2140 103 3 74-125/25
142-28-9 1,3-Dichloropropane ND 2070 2010 97 2070 2090 101 4 76-122/26
594-20-7 2,2-Dichloropropane ND 2070 1930 93 2070 1970 95 2 77-133/28
563-58-6 1,1-Dichloropropene ND 2070 2040 99 2070 2070 100 1 75-130/28
10061-01-5 cis-1,3-Dichloropropene ND 2070 2000 97 2070 2050 99 2 80-123/26
10061-02-6 trans-1,3-Dichloropropene ND 2070 2120 102 2070 2200 106 4 75-131/28
108-20-3 Di-Isopropyl Ether ND 2070 1870 90 2070 1890 91 1 75-122/25
64-17-5 Ethyl Alcohol ND 41400 41300 100 41400 47600 115 14 53-154/42
100-41-4 Ethylbenzene 62.9 J 2070 2130 100 2070 2210 104 4 77-123/31
* = Outside of Control Limits.
21 of 23
FA67097A55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA67097A
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA67079-1MS 3C6505.D 1 08/20/19 SP n/a n/a V3C262
FA67079-1MSD 3C6506.D 1 08/20/19 SP n/a n/a V3C262
FA67079-1 a 3C6491.D 1 08/19/19 SP n/a n/a V3C262
The QC reported here applies to the following samples:Method: SW846 8260D
FA67097-6
FA67079-1 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/kg Q ug/kg ug/kg %ug/kg ug/kg %RPD Rec/RPD
591-78-6 2-Hexanone ND 10300 10100 98 10300 10000 97 1 72-133/26
98-82-8 Isopropylbenzene 63.3 J 2070 2250 106 2070 2320 109 3 80-136/32
99-87-6 p-Isopropyltoluene ND 2070 2030 98 2070 2110 102 4 77-131/34
74-83-9 Methyl Bromide ND 2070 1730 84 2070 1970 95 13 65-139/31
74-87-3 Methyl Chloride ND 2070 2010 97 2070 2020 98 0 71-144/27
75-09-2 Methylene Chloride ND 2070 1910 92 2070 1870 90 2 74-137/28
108-10-1 4-Methyl-2-pentanone (MIBK)ND 10300 10300 100 10300 10400 100 1 76-132/26
1634-04-4 Methyl Tert Butyl Ether ND 2070 1920 93 2070 1960 95 2 77-120/24
91-20-3 Naphthalene 160 J 2070 2140 96 2070 2180 98 2 79-129/33
103-65-1 n-Propylbenzene 131 J 2070 1990 90 2070 2040 92 2 80-135/33
100-42-5 Styrene ND 2070 2090 101 2070 2190 106 5 78-125/30
630-20-6 1,1,1,2-Tetrachloroethane ND 2070 2240 108 2070 2330 113 4 78-126/27
79-34-5 1,1,2,2-Tetrachloroethane ND 2070 2040 99 2070 2030 98 0 71-126/30
127-18-4 Tetrachloroethylene ND 2070 2490 120 2070 2660 129 7 79-130/31
108-88-3 Toluene ND 2070 2050 99 2070 2130 103 4 76-124/30
87-61-6 1,2,3-Trichlorobenzene ND 2070 1990 96 2070 2060 100 3 77-128/35
120-82-1 1,2,4-Trichlorobenzene ND 2070 1880 91 2070 1990 96 6 78-130/34
71-55-6 1,1,1-Trichloroethane ND 2070 2050 99 2070 2060 100 0 70-129/27
79-00-5 1,1,2-Trichloroethane ND 2070 2270 110 2070 2290 111 1 74-124/28
79-01-6 Trichloroethylene ND 2070 2100 101 2070 2130 103 1 75-128/27
75-69-4 Trichlorofluoromethane ND 2070 1020 49*2070 1050 51*3 73-145/31
96-18-4 1,2,3-Trichloropropane ND 2070 1870 90 2070 1890 91 1 74-127/27
95-63-6 1,2,4-Trimethylbenzene 341 2070 2210 90 2070 2270 93 3 74-123/34
108-67-8 1,3,5-Trimethylbenzene 89.3 J 2070 2030 94 2070 2080 96 2 73-122/33
108-05-4 Vinyl Acetate ND 10300 6900 67 10300 6630 64 4 48-164/37
75-01-4 Vinyl Chloride ND 2070 1920 93 2070 2080 100 8 76-141/27
m,p-Xylene 181 J 4140 4380 101 4140 4500 104 3 80-128/30
95-47-6 o-Xylene 82.3 J 2070 2170 101 2070 2230 104 3 80-132/30
1330-20-7 Xylene (total)263 J 6210 6540 101 6210 6730 104 3 80-129/30
CAS No.Surrogate Recoveries MS MSD FA67079-1 Limits
1868-53-7 Dibromofluoromethane 100%98%104%75-124%
17060-07-0 1,2-Dichloroethane-D4 95%92%101%72-135%
2037-26-5 Toluene-D8 98%99%90%75-126%
* = Outside of Control Limits.
22 of 23
FA67097A55.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA67097A
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA67079-1MS 3C6505.D 1 08/20/19 SP n/a n/a V3C262
FA67079-1MSD 3C6506.D 1 08/20/19 SP n/a n/a V3C262
FA67079-1 a 3C6491.D 1 08/19/19 SP n/a n/a V3C262
The QC reported here applies to the following samples:Method: SW846 8260D
FA67097-6
CAS No.Surrogate Recoveries MS MSD FA67079-1 Limits
460-00-4 4-Bromofluorobenzene 94%96%92%71-133%
(a) Dilution required due to matrix interference (sample foamed).
* = Outside of Control Limits.
23 of 23
FA67097A55.3.1
08/22/19
Technical Report for
Resolve Environmental
Five Points Gateway; 320/322 Franklin, Monroe, NC
SGS Job Number: FA67097
Sampling Date: 08/15/19
Report to:
Resolve Environmental
500 Devonport Dr
Matthews, NC 28104
[e-mail]
ATTN: Laura Minor
Total number of pages in report:
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
Test results contained within this data package meet the requirements
of the National Environmental Laboratory Accreditation Program
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Caitlin Brice, M.S.
General Manager
Orlando, FL 08/22/19
e-Hardcopy 2.0
Automated Report
50
SGS is the sole authority for authorizing edits or modifications to this document.
Unauthorized modification of this report is strictly prohibited.
Review standard terms at: http://www.sgs.com/en/terms-and-conditions
The results set forth herein are provided by SGS North America Inc.
Please share your ideas about
how we can serve you better at:
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1 of 50
FA67097
Table of Contents
-1-
Sections:
Section 1: Sample Summary ...................................................................................................3
Section 2: Summary of Hits ....................................................................................................4
Section 3: Sample Results ........................................................................................................6
3.1: FA67097-1: MW-1 ........................................................................................................7
3.2: FA67097-2: MW-2 ........................................................................................................12
3.3: FA67097-3: MW-3 ........................................................................................................17
3.4: FA67097-4: DUPLICATE ............................................................................................23
3.5: FA67097-5: TRIP BLANK ...........................................................................................29
Section 4: Misc. Forms ............................................................................................................32
4.1: Chain of Custody ...........................................................................................................33
Section 5: MS Volatiles - QC Data Summaries .....................................................................36
5.1: Method Blank Summary ................................................................................................37
5.2: Blank Spike Summary ...................................................................................................40
5.3: Matrix Spike/Matrix Spike Duplicate Summary ...........................................................43
Section 6: MS Semi-volatiles - QC Data Summaries ............................................................46
6.1: Method Blank Summary ................................................................................................47
6.2: Blank Spike Summary ...................................................................................................49 1234562 of 50
FA67097
SGS North America Inc.
Sample Summary
Resolve Environmental
Job No:FA67097
Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample ID
This report contains results reported as ND = Not detected. The following applies:
Organics ND = Not detected above the MDL
FA67097-1 08/15/19 09:11 SB 08/16/19 AQ Ground Water MW-1
FA67097-2 08/15/19 09:58 SB 08/16/19 AQ Ground Water MW-2
FA67097-3 08/15/19 08:16 SB 08/16/19 AQ Ground Water MW-3
FA67097-4 08/15/19 00:00 SB 08/16/19 AQ Ground Water DUPLICATE
FA67097-5 08/15/19 00:00 SB 08/16/19 AQ Trip Blank Water TRIP BLANK
3 of 50
FA670971
Summary of Hits Page 1 of 2
Job Number:FA67097
Account:Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Collected:08/15/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
FA67097-1 MW-1
Benzene 2.7 1.0 0.31 ug/l SW846 8260D
1,2-Dichloroethane 7.0 1.0 0.31 ug/l SW846 8260D
Di-Isopropyl Ether 0.59 J 1.0 0.24 ug/l SW846 8260D
Ethylbenzene 1.3 1.0 0.36 ug/l SW846 8260D
Isopropylbenzene 0.27 J 1.0 0.22 ug/l SW846 8260D
p-Isopropyltoluene 0.23 J 1.0 0.21 ug/l SW846 8260D
Naphthalene 1.2 J 5.0 1.0 ug/l SW846 8260D
n-Propylbenzene 0.37 J 1.0 0.29 ug/l SW846 8260D
Toluene 7.6 1.0 0.30 ug/l SW846 8260D
1,2,4-Trimethylbenzene 2.9 1.0 0.32 ug/l SW846 8260D
1,3,5-Trimethylbenzene 1.5 1.0 0.27 ug/l SW846 8260D
m,p-Xylene 6.3 2.0 0.47 ug/l SW846 8260D
o-Xylene 3.6 1.0 0.26 ug/l SW846 8260D
Xylene (total)9.8 3.0 0.72 ug/l SW846 8260D
FA67097-2 MW-2
Benzene 5.0 1.0 0.31 ug/l SW846 8260D
1,2-Dichloroethane 13.1 1.0 0.31 ug/l SW846 8260D
Di-Isopropyl Ether 0.58 J 1.0 0.24 ug/l SW846 8260D
Ethylbenzene 0.73 J 1.0 0.36 ug/l SW846 8260D
Toluene 6.5 1.0 0.30 ug/l SW846 8260D
1,2,4-Trimethylbenzene 0.38 J 1.0 0.32 ug/l SW846 8260D
m,p-Xylene 2.5 2.0 0.47 ug/l SW846 8260D
o-Xylene 1.2 1.0 0.26 ug/l SW846 8260D
Xylene (total)3.6 3.0 0.72 ug/l SW846 8260D
Di-n-butyl Phthalate 1.0 J 4.8 0.95 ug/l SW846 8270E
FA67097-3 MW-3
Ethylbenzene 0.56 J 1.0 0.36 ug/l SW846 8260D
Toluene 5.6 1.0 0.30 ug/l SW846 8260D
m,p-Xylene 2.1 2.0 0.47 ug/l SW846 8260D
o-Xylene 0.79 J 1.0 0.26 ug/l SW846 8260D
Xylene (total)2.9 J 3.0 0.72 ug/l SW846 8260D
FA67097-4 DUPLICATE
Benzene 2.4 1.0 0.31 ug/l SW846 8260D
1,2-Dichloroethane 10.8 1.0 0.31 ug/l SW846 8260D
Di-Isopropyl Ether 0.43 J 1.0 0.24 ug/l SW846 8260D
Ethylbenzene 0.85 J 1.0 0.36 ug/l SW846 8260D
Toluene 7.6 1.0 0.30 ug/l SW846 8260D
4 of 50
FA670972
Summary of Hits Page 2 of 2
Job Number:FA67097
Account:Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Collected:08/15/19
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
1,2,4-Trimethylbenzene 0.32 J 1.0 0.32 ug/l SW846 8260D
m,p-Xylene 2.9 2.0 0.47 ug/l SW846 8260D
o-Xylene 1.3 1.0 0.26 ug/l SW846 8260D
Xylene (total)4.2 3.0 0.72 ug/l SW846 8260D
FA67097-5 TRIP BLANK
No hits reported in this sample.
5 of 50
FA670972
SGS North America Inc.
Sample Results
Report of Analysis
Orlando, FL
Section 3
6 of 50
FA670973
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-1
Lab Sample ID:FA67097-1 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8260D Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 C0135175.D 1 08/20/19 20:43 AJ n/a n/a VC5382
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene 2.7 1.0 0.31 ug/l
108-86-1 Bromobenzene ND 1.0 0.37 ug/l
74-97-5 Bromochloromethane ND 1.0 0.45 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.41 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.0 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.23 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.24 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.31 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.36 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.67 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.22 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.28 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.28 ug/l
75-71-8 Dichlorodifluoromethane a ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.32 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.26 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.34 ug/l
107-06-2 1,2-Dichloroethane 7.0 1.0 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.32 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.28 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.43 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.24 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.34 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.29 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
7 of 50
FA6709733.1
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-1
Lab Sample ID:FA67097-1 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8260D Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
108-20-3 Di-Isopropyl Ether 0.59 1.0 0.24 ug/l J
64-17-5 Ethyl Alcohol ND 200 82 ug/l
100-41-4 Ethylbenzene 1.3 1.0 0.36 ug/l
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene 0.27 1.0 0.22 ug/l J
99-87-6 p-Isopropyltoluene 0.23 1.0 0.21 ug/l J
74-83-9 Methyl Bromide ND 2.0 0.59 ug/l
74-87-3 Methyl Chloride a ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.23 ug/l
91-20-3 Naphthalene 1.2 5.0 1.0 ug/l J
103-65-1 n-Propylbenzene 0.37 1.0 0.29 ug/l J
100-42-5 Styrene ND 1.0 0.22 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.30 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.22 ug/l
108-88-3 Toluene 7.6 1.0 0.30 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.61 ug/l
120-82-1 1,2,4-Trichlorobenzene b ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.47 ug/l
79-01-6 Trichloroethylene ND 1.0 0.35 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene 2.9 1.0 0.32 ug/l
108-67-8 1,3,5-Trimethylbenzene 1.5 1.0 0.27 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.41 ug/l
m,p-Xylene 6.3 2.0 0.47 ug/l
95-47-6 o-Xylene 3.6 1.0 0.26 ug/l
1330-20-7 Xylene (total)9.8 3.0 0.72 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 105%83-118%
17060-07-0 1,2-Dichloroethane-D4 106%79-125%
2037-26-5 Toluene-D8 96%85-112%
460-00-4 4-Bromofluorobenzene 101%83-118%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
8 of 50
FA6709733.1
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-1
Lab Sample ID:FA67097-1 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8260D Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
(b) Associated CCV outside of control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
9 of 50
FA6709733.1
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-1
Lab Sample ID:FA67097-1 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X066578.D 1 08/20/19 18:17 MV 08/20/19 14:30 OP76458 SX2743
Run #2
Initial Volume Final Volume
Run #1 1050 ml 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid a ND 48 9.5 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 4.8 0.56 ug/l
95-57-8 2-Chlorophenol ND 4.8 0.60 ug/l
120-83-2 2,4-Dichlorophenol ND 4.8 0.80 ug/l
105-67-9 2,4-Dimethylphenol ND 4.8 0.70 ug/l
51-28-5 2,4-Dinitrophenol ND 24 4.8 ug/l
534-52-1 4,6-Dinitro-o-cresol a ND 9.5 1.9 ug/l
95-48-7 2-Methylphenol ND 4.8 0.53 ug/l
3&4-Methylphenol ND 4.8 0.93 ug/l
88-75-5 2-Nitrophenol ND 4.8 0.81 ug/l
100-02-7 4-Nitrophenol ND 24 4.8 ug/l
87-86-5 Pentachlorophenol ND 24 4.8 ug/l
108-95-2 Phenol ND 4.8 0.48 ug/l
88-06-2 2,4,6-Trichlorophenol ND 4.8 0.72 ug/l
83-32-9 Acenaphthene ND 4.8 0.60 ug/l
208-96-8 Acenaphthylene ND 4.8 0.61 ug/l
120-12-7 Anthracene ND 4.8 0.76 ug/l
56-55-3 Benzo(a)anthracene ND 4.8 0.72 ug/l
50-32-8 Benzo(a)pyrene ND 4.8 0.75 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.8 0.74 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.8 0.78 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.8 0.82 ug/l
100-51-6 Benzyl Alcohol ND 4.8 0.58 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 4.8 0.81 ug/l
85-68-7 Butyl Benzyl Phthalate ND 4.8 0.95 ug/l
106-47-8 4-Chloroaniline ND 4.8 0.60 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 4.8 0.77 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 4.8 0.70 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 4.8 0.72 ug/l
91-58-7 2-Chloronaphthalene ND 4.8 0.48 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 4.8 0.51 ug/l
218-01-9 Chrysene ND 4.8 0.81 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
10 of 50
FA6709733.1
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-1
Lab Sample ID:FA67097-1 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 4.8 0.77 ug/l
132-64-9 Dibenzofuran ND 4.8 0.57 ug/l
95-50-1 1,2-Dichlorobenzene ND 4.8 0.48 ug/l
541-73-1 1,3-Dichlorobenzene ND 4.8 0.48 ug/l
106-46-7 1,4-Dichlorobenzene ND 4.8 0.48 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 4.8 0.61 ug/l
84-66-2 Diethyl Phthalate ND 4.8 0.95 ug/l
131-11-3 Dimethyl Phthalate ND 4.8 0.95 ug/l
84-74-2 Di-n-butyl Phthalate ND 4.8 0.95 ug/l
117-84-0 Di-n-octyl Phthalate ND 4.8 0.95 ug/l
122-66-7 1,2-Diphenylhydrazine ND 4.8 0.72 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 4.8 0.95 ug/l
206-44-0 Fluoranthene ND 4.8 0.53 ug/l
86-73-7 Fluorene ND 4.8 0.67 ug/l
118-74-1 Hexachlorobenzene ND 4.8 0.66 ug/l
87-68-3 Hexachlorobutadiene ND 4.8 0.48 ug/l
77-47-4 Hexachlorocyclopentadiene ND 4.8 1.7 ug/l
67-72-1 Hexachloroethane ND 4.8 1.6 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.8 0.68 ug/l
78-59-1 Isophorone ND 4.8 0.74 ug/l
90-12-0 1-Methylnaphthalene ND 4.8 0.50 ug/l
91-57-6 2-Methylnaphthalene ND 4.8 0.57 ug/l
91-20-3 Naphthalene ND 4.8 0.48 ug/l
98-95-3 Nitrobenzene ND 4.8 0.89 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 4.8 0.64 ug/l
86-30-6 N-Nitrosodiphenylamine ND 4.8 0.77 ug/l
85-01-8 Phenanthrene ND 4.8 0.82 ug/l
129-00-0 Pyrene ND 4.8 0.65 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 4.8 1.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 29%14-67%
4165-62-2 Phenol-d5 23%10-50%
118-79-6 2,4,6-Tribromophenol 84%33-118%
4165-60-0 Nitrobenzene-d5 76%42-108%
321-60-8 2-Fluorobiphenyl 81%40-106%
1718-51-0 Terphenyl-d14 82%39-121%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
11 of 50
FA6709733.1
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-2
Lab Sample ID:FA67097-2 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8260D Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 C0135176.D 1 08/20/19 21:09 AJ n/a n/a VC5382
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene 5.0 1.0 0.31 ug/l
108-86-1 Bromobenzene ND 1.0 0.37 ug/l
74-97-5 Bromochloromethane ND 1.0 0.45 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.41 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.0 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.23 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.24 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.31 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.36 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.67 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.22 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.28 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.28 ug/l
75-71-8 Dichlorodifluoromethane a ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.32 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.26 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.34 ug/l
107-06-2 1,2-Dichloroethane 13.1 1.0 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.32 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.28 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.43 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.24 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.34 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.29 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
12 of 50
FA6709733.2
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-2
Lab Sample ID:FA67097-2 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8260D Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
108-20-3 Di-Isopropyl Ether 0.58 1.0 0.24 ug/l J
64-17-5 Ethyl Alcohol ND 200 82 ug/l
100-41-4 Ethylbenzene 0.73 1.0 0.36 ug/l J
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.22 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.21 ug/l
74-83-9 Methyl Bromide ND 2.0 0.59 ug/l
74-87-3 Methyl Chloride a ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.23 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.29 ug/l
100-42-5 Styrene ND 1.0 0.22 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.30 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.22 ug/l
108-88-3 Toluene 6.5 1.0 0.30 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.61 ug/l
120-82-1 1,2,4-Trichlorobenzene b ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.47 ug/l
79-01-6 Trichloroethylene ND 1.0 0.35 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.38 1.0 0.32 ug/l J
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.27 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.41 ug/l
m,p-Xylene 2.5 2.0 0.47 ug/l
95-47-6 o-Xylene 1.2 1.0 0.26 ug/l
1330-20-7 Xylene (total)3.6 3.0 0.72 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 106%83-118%
17060-07-0 1,2-Dichloroethane-D4 105%79-125%
2037-26-5 Toluene-D8 96%85-112%
460-00-4 4-Bromofluorobenzene 95%83-118%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
13 of 50
FA6709733.2
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-2
Lab Sample ID:FA67097-2 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8260D Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
(b) Associated CCV outside of control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
14 of 50
FA6709733.2
SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID:MW-2
Lab Sample ID:FA67097-2 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X066579.D 1 08/20/19 18:44 MV 08/20/19 14:30 OP76458 SX2743
Run #2
Initial Volume Final Volume
Run #1 1050 ml 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid a ND 48 9.5 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 4.8 0.56 ug/l
95-57-8 2-Chlorophenol ND 4.8 0.60 ug/l
120-83-2 2,4-Dichlorophenol ND 4.8 0.80 ug/l
105-67-9 2,4-Dimethylphenol ND 4.8 0.70 ug/l
51-28-5 2,4-Dinitrophenol ND 24 4.8 ug/l
534-52-1 4,6-Dinitro-o-cresol a ND 9.5 1.9 ug/l
95-48-7 2-Methylphenol ND 4.8 0.53 ug/l
3&4-Methylphenol ND 4.8 0.93 ug/l
88-75-5 2-Nitrophenol ND 4.8 0.81 ug/l
100-02-7 4-Nitrophenol ND 24 4.8 ug/l
87-86-5 Pentachlorophenol ND 24 4.8 ug/l
108-95-2 Phenol ND 4.8 0.48 ug/l
88-06-2 2,4,6-Trichlorophenol ND 4.8 0.72 ug/l
83-32-9 Acenaphthene ND 4.8 0.60 ug/l
208-96-8 Acenaphthylene ND 4.8 0.61 ug/l
120-12-7 Anthracene ND 4.8 0.76 ug/l
56-55-3 Benzo(a)anthracene ND 4.8 0.72 ug/l
50-32-8 Benzo(a)pyrene ND 4.8 0.75 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.8 0.74 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.8 0.78 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.8 0.82 ug/l
100-51-6 Benzyl Alcohol ND 4.8 0.58 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 4.8 0.81 ug/l
85-68-7 Butyl Benzyl Phthalate ND 4.8 0.95 ug/l
106-47-8 4-Chloroaniline ND 4.8 0.60 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 4.8 0.77 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 4.8 0.70 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 4.8 0.72 ug/l
91-58-7 2-Chloronaphthalene ND 4.8 0.48 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 4.8 0.51 ug/l
218-01-9 Chrysene ND 4.8 0.81 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
15 of 50
FA6709733.2
SGS North America Inc.
Report of Analysis Page 2 of 2
Client Sample ID:MW-2
Lab Sample ID:FA67097-2 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 4.8 0.77 ug/l
132-64-9 Dibenzofuran ND 4.8 0.57 ug/l
95-50-1 1,2-Dichlorobenzene ND 4.8 0.48 ug/l
541-73-1 1,3-Dichlorobenzene ND 4.8 0.48 ug/l
106-46-7 1,4-Dichlorobenzene ND 4.8 0.48 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 4.8 0.61 ug/l
84-66-2 Diethyl Phthalate ND 4.8 0.95 ug/l
131-11-3 Dimethyl Phthalate ND 4.8 0.95 ug/l
84-74-2 Di-n-butyl Phthalate 1.0 4.8 0.95 ug/l J
117-84-0 Di-n-octyl Phthalate ND 4.8 0.95 ug/l
122-66-7 1,2-Diphenylhydrazine ND 4.8 0.72 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 4.8 0.95 ug/l
206-44-0 Fluoranthene ND 4.8 0.53 ug/l
86-73-7 Fluorene ND 4.8 0.67 ug/l
118-74-1 Hexachlorobenzene ND 4.8 0.66 ug/l
87-68-3 Hexachlorobutadiene ND 4.8 0.48 ug/l
77-47-4 Hexachlorocyclopentadiene ND 4.8 1.7 ug/l
67-72-1 Hexachloroethane ND 4.8 1.6 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.8 0.68 ug/l
78-59-1 Isophorone ND 4.8 0.74 ug/l
90-12-0 1-Methylnaphthalene ND 4.8 0.50 ug/l
91-57-6 2-Methylnaphthalene ND 4.8 0.57 ug/l
91-20-3 Naphthalene ND 4.8 0.48 ug/l
98-95-3 Nitrobenzene ND 4.8 0.89 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 4.8 0.64 ug/l
86-30-6 N-Nitrosodiphenylamine ND 4.8 0.77 ug/l
85-01-8 Phenanthrene ND 4.8 0.82 ug/l
129-00-0 Pyrene ND 4.8 0.65 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 4.8 1.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 27%14-67%
4165-62-2 Phenol-d5 17%10-50%
118-79-6 2,4,6-Tribromophenol 85%33-118%
4165-60-0 Nitrobenzene-d5 73%42-108%
321-60-8 2-Fluorobiphenyl 78%40-106%
1718-51-0 Terphenyl-d14 83%39-121%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
16 of 50
FA6709733.2
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-3
Lab Sample ID:FA67097-3 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8260D Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 C0135177.D 1 08/20/19 21:35 AJ n/a n/a VC5382
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.31 ug/l
108-86-1 Bromobenzene ND 1.0 0.37 ug/l
74-97-5 Bromochloromethane ND 1.0 0.45 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.41 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.0 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.23 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.24 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.31 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.36 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.67 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.22 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.28 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.28 ug/l
75-71-8 Dichlorodifluoromethane a ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.32 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.26 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.34 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.32 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.28 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.43 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.24 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.34 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.29 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
17 of 50
FA6709733.3
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-3
Lab Sample ID:FA67097-3 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8260D Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
108-20-3 Di-Isopropyl Ether ND 1.0 0.24 ug/l
64-17-5 Ethyl Alcohol ND 200 82 ug/l
100-41-4 Ethylbenzene 0.56 1.0 0.36 ug/l J
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.22 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.21 ug/l
74-83-9 Methyl Bromide ND 2.0 0.59 ug/l
74-87-3 Methyl Chloride a ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.23 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.29 ug/l
100-42-5 Styrene ND 1.0 0.22 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.30 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.22 ug/l
108-88-3 Toluene 5.6 1.0 0.30 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.61 ug/l
120-82-1 1,2,4-Trichlorobenzene b ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.47 ug/l
79-01-6 Trichloroethylene ND 1.0 0.35 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.32 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.27 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.41 ug/l
m,p-Xylene 2.1 2.0 0.47 ug/l
95-47-6 o-Xylene 0.79 1.0 0.26 ug/l J
1330-20-7 Xylene (total)2.9 3.0 0.72 ug/l J
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 110%83-118%
17060-07-0 1,2-Dichloroethane-D4 108%79-125%
2037-26-5 Toluene-D8 97%85-112%
460-00-4 4-Bromofluorobenzene 95%83-118%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
18 of 50
FA6709733.3
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-3
Lab Sample ID:FA67097-3 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8260D Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
(b) Associated CCV outside of control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
19 of 50
FA6709733.3
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:MW-3
Lab Sample ID:FA67097-3 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X066586.D 1 08/21/19 14:42 MV 08/20/19 14:30 OP76458 SX2744
Run #2
Initial Volume Final Volume
Run #1 1050 ml 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid a ND 48 9.5 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 4.8 0.56 ug/l
95-57-8 2-Chlorophenol ND 4.8 0.60 ug/l
120-83-2 2,4-Dichlorophenol ND 4.8 0.80 ug/l
105-67-9 2,4-Dimethylphenol ND 4.8 0.70 ug/l
51-28-5 2,4-Dinitrophenol a ND 24 4.8 ug/l
534-52-1 4,6-Dinitro-o-cresol a ND 9.5 1.9 ug/l
95-48-7 2-Methylphenol ND 4.8 0.53 ug/l
3&4-Methylphenol ND 4.8 0.93 ug/l
88-75-5 2-Nitrophenol b ND 4.8 0.81 ug/l
100-02-7 4-Nitrophenol ND 24 4.8 ug/l
87-86-5 Pentachlorophenol ND 24 4.8 ug/l
108-95-2 Phenol ND 4.8 0.48 ug/l
88-06-2 2,4,6-Trichlorophenol ND 4.8 0.72 ug/l
83-32-9 Acenaphthene ND 4.8 0.60 ug/l
208-96-8 Acenaphthylene ND 4.8 0.61 ug/l
120-12-7 Anthracene ND 4.8 0.76 ug/l
56-55-3 Benzo(a)anthracene ND 4.8 0.72 ug/l
50-32-8 Benzo(a)pyrene ND 4.8 0.75 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.8 0.74 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.8 0.78 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.8 0.82 ug/l
100-51-6 Benzyl Alcohol ND 4.8 0.58 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 4.8 0.81 ug/l
85-68-7 Butyl Benzyl Phthalate ND 4.8 0.95 ug/l
106-47-8 4-Chloroaniline ND 4.8 0.60 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 4.8 0.77 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 4.8 0.70 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 4.8 0.72 ug/l
91-58-7 2-Chloronaphthalene ND 4.8 0.48 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 4.8 0.51 ug/l
218-01-9 Chrysene ND 4.8 0.81 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
20 of 50
FA6709733.3
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:MW-3
Lab Sample ID:FA67097-3 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 4.8 0.77 ug/l
132-64-9 Dibenzofuran ND 4.8 0.57 ug/l
95-50-1 1,2-Dichlorobenzene ND 4.8 0.48 ug/l
541-73-1 1,3-Dichlorobenzene ND 4.8 0.48 ug/l
106-46-7 1,4-Dichlorobenzene ND 4.8 0.48 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 4.8 0.61 ug/l
84-66-2 Diethyl Phthalate ND 4.8 0.95 ug/l
131-11-3 Dimethyl Phthalate ND 4.8 0.95 ug/l
84-74-2 Di-n-butyl Phthalate ND 4.8 0.95 ug/l
117-84-0 Di-n-octyl Phthalate ND 4.8 0.95 ug/l
122-66-7 1,2-Diphenylhydrazine ND 4.8 0.72 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 4.8 0.95 ug/l
206-44-0 Fluoranthene ND 4.8 0.53 ug/l
86-73-7 Fluorene ND 4.8 0.67 ug/l
118-74-1 Hexachlorobenzene ND 4.8 0.66 ug/l
87-68-3 Hexachlorobutadiene ND 4.8 0.48 ug/l
77-47-4 Hexachlorocyclopentadiene ND 4.8 1.7 ug/l
67-72-1 Hexachloroethane ND 4.8 1.6 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.8 0.68 ug/l
78-59-1 Isophorone ND 4.8 0.74 ug/l
90-12-0 1-Methylnaphthalene ND 4.8 0.50 ug/l
91-57-6 2-Methylnaphthalene ND 4.8 0.57 ug/l
91-20-3 Naphthalene ND 4.8 0.48 ug/l
98-95-3 Nitrobenzene ND 4.8 0.89 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 4.8 0.64 ug/l
86-30-6 N-Nitrosodiphenylamine ND 4.8 0.77 ug/l
85-01-8 Phenanthrene ND 4.8 0.82 ug/l
129-00-0 Pyrene ND 4.8 0.65 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 4.8 1.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 31%14-67%
4165-62-2 Phenol-d5 19%10-50%
118-79-6 2,4,6-Tribromophenol 88%33-118%
4165-60-0 Nitrobenzene-d5 85%42-108%
321-60-8 2-Fluorobiphenyl 85%40-106%
1718-51-0 Terphenyl-d14 86%39-121%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
21 of 50
FA6709733.3
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:MW-3
Lab Sample ID:FA67097-3 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(b) Associated BS outside control limits high. Sample was ND. Associated CCV outside of control limits high,
sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
22 of 50
FA6709733.3
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:DUPLICATE
Lab Sample ID:FA67097-4 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8260D Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 C0135178.D 1 08/20/19 22:02 AJ n/a n/a VC5382
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene 2.4 1.0 0.31 ug/l
108-86-1 Bromobenzene ND 1.0 0.37 ug/l
74-97-5 Bromochloromethane ND 1.0 0.45 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.41 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.0 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.23 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.24 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.31 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.36 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.67 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.22 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.28 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.28 ug/l
75-71-8 Dichlorodifluoromethane a ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.32 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.26 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.34 ug/l
107-06-2 1,2-Dichloroethane 10.8 1.0 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.32 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.28 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.43 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.24 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.34 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.29 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
23 of 50
FA6709733.4
SGS North America Inc.
Report of Analysis Page 2 of 3
Client Sample ID:DUPLICATE
Lab Sample ID:FA67097-4 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8260D Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
108-20-3 Di-Isopropyl Ether 0.43 1.0 0.24 ug/l J
64-17-5 Ethyl Alcohol ND 200 82 ug/l
100-41-4 Ethylbenzene 0.85 1.0 0.36 ug/l J
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.22 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.21 ug/l
74-83-9 Methyl Bromide ND 2.0 0.59 ug/l
74-87-3 Methyl Chloride a ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.23 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.29 ug/l
100-42-5 Styrene ND 1.0 0.22 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.30 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.22 ug/l
108-88-3 Toluene 7.6 1.0 0.30 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.61 ug/l
120-82-1 1,2,4-Trichlorobenzene b ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.47 ug/l
79-01-6 Trichloroethylene ND 1.0 0.35 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene 0.32 1.0 0.32 ug/l J
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.27 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.41 ug/l
m,p-Xylene 2.9 2.0 0.47 ug/l
95-47-6 o-Xylene 1.3 1.0 0.26 ug/l
1330-20-7 Xylene (total)4.2 3.0 0.72 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 104%83-118%
17060-07-0 1,2-Dichloroethane-D4 105%79-125%
2037-26-5 Toluene-D8 99%85-112%
460-00-4 4-Bromofluorobenzene 96%83-118%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA6709733.4
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Report of Analysis Page 3 of 3
Client Sample ID:DUPLICATE
Lab Sample ID:FA67097-4 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8260D Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
(b) Associated CCV outside of control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA6709733.4
SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:DUPLICATE
Lab Sample ID:FA67097-4 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 X066587.D 1 08/21/19 15:09 MV 08/20/19 14:30 OP76458 SX2744
Run #2
Initial Volume Final Volume
Run #1 1050 ml 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid a ND 48 9.5 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 4.8 0.56 ug/l
95-57-8 2-Chlorophenol ND 4.8 0.60 ug/l
120-83-2 2,4-Dichlorophenol ND 4.8 0.80 ug/l
105-67-9 2,4-Dimethylphenol ND 4.8 0.70 ug/l
51-28-5 2,4-Dinitrophenol a ND 24 4.8 ug/l
534-52-1 4,6-Dinitro-o-cresol a ND 9.5 1.9 ug/l
95-48-7 2-Methylphenol ND 4.8 0.53 ug/l
3&4-Methylphenol ND 4.8 0.93 ug/l
88-75-5 2-Nitrophenol b ND 4.8 0.81 ug/l
100-02-7 4-Nitrophenol ND 24 4.8 ug/l
87-86-5 Pentachlorophenol ND 24 4.8 ug/l
108-95-2 Phenol ND 4.8 0.48 ug/l
88-06-2 2,4,6-Trichlorophenol ND 4.8 0.72 ug/l
83-32-9 Acenaphthene ND 4.8 0.60 ug/l
208-96-8 Acenaphthylene ND 4.8 0.61 ug/l
120-12-7 Anthracene ND 4.8 0.76 ug/l
56-55-3 Benzo(a)anthracene ND 4.8 0.72 ug/l
50-32-8 Benzo(a)pyrene ND 4.8 0.75 ug/l
205-99-2 Benzo(b)fluoranthene ND 4.8 0.74 ug/l
191-24-2 Benzo(g,h,i)perylene ND 4.8 0.78 ug/l
207-08-9 Benzo(k)fluoranthene ND 4.8 0.82 ug/l
100-51-6 Benzyl Alcohol ND 4.8 0.58 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 4.8 0.81 ug/l
85-68-7 Butyl Benzyl Phthalate ND 4.8 0.95 ug/l
106-47-8 4-Chloroaniline ND 4.8 0.60 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 4.8 0.77 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 4.8 0.70 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 4.8 0.72 ug/l
91-58-7 2-Chloronaphthalene ND 4.8 0.48 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 4.8 0.51 ug/l
218-01-9 Chrysene ND 4.8 0.81 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:DUPLICATE
Lab Sample ID:FA67097-4 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
53-70-3 Dibenzo(a,h)anthracene ND 4.8 0.77 ug/l
132-64-9 Dibenzofuran ND 4.8 0.57 ug/l
95-50-1 1,2-Dichlorobenzene ND 4.8 0.48 ug/l
541-73-1 1,3-Dichlorobenzene ND 4.8 0.48 ug/l
106-46-7 1,4-Dichlorobenzene ND 4.8 0.48 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 4.8 0.61 ug/l
84-66-2 Diethyl Phthalate ND 4.8 0.95 ug/l
131-11-3 Dimethyl Phthalate ND 4.8 0.95 ug/l
84-74-2 Di-n-butyl Phthalate ND 4.8 0.95 ug/l
117-84-0 Di-n-octyl Phthalate ND 4.8 0.95 ug/l
122-66-7 1,2-Diphenylhydrazine ND 4.8 0.72 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 4.8 0.95 ug/l
206-44-0 Fluoranthene ND 4.8 0.53 ug/l
86-73-7 Fluorene ND 4.8 0.67 ug/l
118-74-1 Hexachlorobenzene ND 4.8 0.66 ug/l
87-68-3 Hexachlorobutadiene ND 4.8 0.48 ug/l
77-47-4 Hexachlorocyclopentadiene ND 4.8 1.7 ug/l
67-72-1 Hexachloroethane ND 4.8 1.6 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 4.8 0.68 ug/l
78-59-1 Isophorone ND 4.8 0.74 ug/l
90-12-0 1-Methylnaphthalene ND 4.8 0.50 ug/l
91-57-6 2-Methylnaphthalene ND 4.8 0.57 ug/l
91-20-3 Naphthalene ND 4.8 0.48 ug/l
98-95-3 Nitrobenzene ND 4.8 0.89 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 4.8 0.64 ug/l
86-30-6 N-Nitrosodiphenylamine ND 4.8 0.77 ug/l
85-01-8 Phenanthrene ND 4.8 0.82 ug/l
129-00-0 Pyrene ND 4.8 0.65 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 4.8 1.0 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
367-12-4 2-Fluorophenol 28%14-67%
4165-62-2 Phenol-d5 17%10-50%
118-79-6 2,4,6-Tribromophenol 84%33-118%
4165-60-0 Nitrobenzene-d5 80%42-108%
321-60-8 2-Fluorobiphenyl 81%40-106%
1718-51-0 Terphenyl-d14 83%39-121%
(a) Associated CCV outside of control limits high, sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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FA6709733.4
SGS North America Inc.
Report of Analysis Page 3 of 3
Client Sample ID:DUPLICATE
Lab Sample ID:FA67097-4 Date Sampled:08/15/19
Matrix:AQ - Ground Water Date Received:08/16/19
Method:SW846 8270E SW846 3510C Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
ABN List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(b) Associated BS outside control limits high. Sample was ND. Associated CCV outside of control limits high,
sample was ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 1 of 3
Client Sample ID:TRIP BLANK
Lab Sample ID:FA67097-5 Date Sampled:08/15/19
Matrix:AQ - Trip Blank Water Date Received:08/16/19
Method:SW846 8260D Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 C0135179.D 1 08/20/19 22:29 AJ n/a n/a VC5382
Run #2
Purge Volume
Run #1 5.0 ml
Run #2
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.31 ug/l
108-86-1 Bromobenzene ND 1.0 0.37 ug/l
74-97-5 Bromochloromethane ND 1.0 0.45 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.41 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.0 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.23 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.24 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.31 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.36 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.67 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.22 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.28 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.28 ug/l
75-71-8 Dichlorodifluoromethane a ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.32 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.26 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.34 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.32 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.28 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.43 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.24 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.34 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.29 ug/l
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 2 of 3
Client Sample ID:TRIP BLANK
Lab Sample ID:FA67097-5 Date Sampled:08/15/19
Matrix:AQ - Trip Blank Water Date Received:08/16/19
Method:SW846 8260D Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
108-20-3 Di-Isopropyl Ether ND 1.0 0.24 ug/l
64-17-5 Ethyl Alcohol ND 200 82 ug/l
100-41-4 Ethylbenzene ND 1.0 0.36 ug/l
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.22 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.21 ug/l
74-83-9 Methyl Bromide ND 2.0 0.59 ug/l
74-87-3 Methyl Chloride a ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.23 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.29 ug/l
100-42-5 Styrene ND 1.0 0.22 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.30 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.22 ug/l
108-88-3 Toluene ND 1.0 0.30 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.61 ug/l
120-82-1 1,2,4-Trichlorobenzene b ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.47 ug/l
79-01-6 Trichloroethylene ND 1.0 0.35 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.32 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.27 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.41 ug/l
m,p-Xylene ND 2.0 0.47 ug/l
95-47-6 o-Xylene ND 1.0 0.26 ug/l
1330-20-7 Xylene (total)ND 3.0 0.72 ug/l
CAS No.Surrogate Recoveries Run# 1 Run# 2 Limits
1868-53-7 Dibromofluoromethane 109%83-118%
17060-07-0 1,2-Dichloroethane-D4 110%79-125%
2037-26-5 Toluene-D8 97%85-112%
460-00-4 4-Bromofluorobenzene 95%83-118%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Report of Analysis Page 3 of 3
Client Sample ID:TRIP BLANK
Lab Sample ID:FA67097-5 Date Sampled:08/15/19
Matrix:AQ - Trip Blank Water Date Received:08/16/19
Method:SW846 8260D Percent Solids:n/a
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
VOA List for NC, May 2012
CAS No.Compound Result RL MDL Units Q
(a) Associated CCV outside of control limits high, sample was ND.
(b) Associated CCV outside of control limits low.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
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Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Orlando, FL
Section 4
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FA670974
FA67097: Chain of Custody
Page 1 of 3
33 of 50
FA6709744.1
Job Number:FA67097 Client:RESOLVE ENVIRONMENTAL SERVICES,
Date / Time Received:8/16/2019 8:45:00 AM Delivery Method:FED EX
Project:FIVE POINTS GATEWAY
Airbill #'s:
Cooler Information
1. Custody Seals Present
2. Custody Seals Intact
4. Cooler temp verification
3. Temp criteria achieved
5. Cooler media
IR Gun
Ice (Bag)
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
2. Samples preserved properly
Sample Information
1. Sample labels present on bottles
5. Sample recvd within HT
4. Condition of sample
3. Sufficient volume/containers recvd for analysis:
Intact
Comments
SM001Rev. Date 05/24/17
SGS Sample Receipt Summary
Cooler Temps (Raw Measured) °C:
Cooler Temps (Corrected) °C:
Cooler 1: (1.0);
Cooler 1: (2.0);
3. Type Of TB Received
W or S N/A
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
Misc. Information
25-Gram 5-GramNumber of Encores:1Number of 5035 Field Kits:Number of Lab Filtered Metals:
Test Strip Lot #s:pH 0-3 230315 pH 10-12 219813A Other: (Specify)
Y or N N/A
Y or N
Therm ID:IR 1; Therm CF:1; # of Coolers:1
Y or N N/A
12. Residual Chlorine Present?
Residual Chlorine Test Strip Lot #:
Technician:Reviewer:PETERH SP Date:8/16/2019Date:8/16/2019 8:45:00 AM
FA67097: Chain of Custody
Page 2 of 3
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FA6709744.1
Job Change Order: FA67097
Requested Date: 8/16/2019 Received Date: 8/16/2019
Account Name: Resolve Environmental Due Date: 8/23/2019
Project Five Points Gateway; 320/322 Franklin, Monroe, Deliverable: COMMB
CSR: MM TAT (Days): 7
Sample #: Change: Per client Stockpile sample should be reported in a FA67097-6 separate report. Sample has been moved to FA67097A.
Above Changes Per: Laura Minor Date: 8/16/2019
To Client: This Change Order is confirmation of the revisions, previously discussed with the Client Service Representative.
Page 1 of 1
FA67097: Chain of Custody
Page 3 of 3
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MS Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 5
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FA670975
Method Blank Summary Page 1 of 3
Job Number:FA67097
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC5382-MB C0135158.D 1 08/20/19 AJ n/a n/a VC5382
The QC reported here applies to the following samples:Method: SW846 8260D
FA67097-1, FA67097-2, FA67097-3, FA67097-4, FA67097-5
CAS No.Compound Result RL MDL Units Q
67-64-1 Acetone ND 25 10 ug/l
71-43-2 Benzene ND 1.0 0.31 ug/l
108-86-1 Bromobenzene ND 1.0 0.37 ug/l
74-97-5 Bromochloromethane ND 1.0 0.45 ug/l
75-27-4 Bromodichloromethane ND 1.0 0.24 ug/l
75-25-2 Bromoform ND 1.0 0.41 ug/l
78-93-3 2-Butanone (MEK)ND 5.0 2.0 ug/l
104-51-8 n-Butylbenzene ND 1.0 0.23 ug/l
135-98-8 sec-Butylbenzene ND 1.0 0.24 ug/l
98-06-6 tert-Butylbenzene ND 1.0 0.31 ug/l
56-23-5 Carbon Tetrachloride ND 1.0 0.36 ug/l
108-90-7 Chlorobenzene ND 1.0 0.20 ug/l
75-00-3 Chloroethane ND 2.0 0.67 ug/l
67-66-3 Chloroform ND 1.0 0.30 ug/l
95-49-8 o-Chlorotoluene ND 1.0 0.22 ug/l
106-43-4 p-Chlorotoluene ND 1.0 0.31 ug/l
124-48-1 Dibromochloromethane ND 1.0 0.28 ug/l
106-93-4 1,2-Dibromoethane ND 2.0 0.28 ug/l
75-71-8 Dichlorodifluoromethane ND 2.0 0.50 ug/l
95-50-1 1,2-Dichlorobenzene ND 1.0 0.32 ug/l
541-73-1 1,3-Dichlorobenzene ND 1.0 0.22 ug/l
106-46-7 1,4-Dichlorobenzene ND 1.0 0.26 ug/l
75-34-3 1,1-Dichloroethane ND 1.0 0.34 ug/l
107-06-2 1,2-Dichloroethane ND 1.0 0.31 ug/l
75-35-4 1,1-Dichloroethylene ND 1.0 0.32 ug/l
156-59-2 cis-1,2-Dichloroethylene ND 1.0 0.28 ug/l
156-60-5 trans-1,2-Dichloroethylene ND 1.0 0.22 ug/l
78-87-5 1,2-Dichloropropane ND 1.0 0.43 ug/l
142-28-9 1,3-Dichloropropane ND 1.0 0.31 ug/l
594-20-7 2,2-Dichloropropane ND 1.0 0.24 ug/l
563-58-6 1,1-Dichloropropene ND 1.0 0.34 ug/l
10061-01-5 cis-1,3-Dichloropropene ND 1.0 0.29 ug/l
10061-02-6 trans-1,3-Dichloropropene ND 1.0 0.21 ug/l
108-20-3 Di-Isopropyl Ether ND 1.0 0.24 ug/l
64-17-5 Ethyl Alcohol ND 200 82 ug/l
100-41-4 Ethylbenzene ND 1.0 0.36 ug/l
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FA6709755.1.1
Method Blank Summary Page 2 of 3
Job Number:FA67097
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC5382-MB C0135158.D 1 08/20/19 AJ n/a n/a VC5382
The QC reported here applies to the following samples:Method: SW846 8260D
FA67097-1, FA67097-2, FA67097-3, FA67097-4, FA67097-5
CAS No.Compound Result RL MDL Units Q
591-78-6 2-Hexanone ND 10 2.0 ug/l
98-82-8 Isopropylbenzene ND 1.0 0.22 ug/l
99-87-6 p-Isopropyltoluene ND 1.0 0.21 ug/l
74-83-9 Methyl Bromide ND 2.0 0.59 ug/l
74-87-3 Methyl Chloride ND 2.0 0.50 ug/l
75-09-2 Methylene Chloride ND 5.0 2.0 ug/l
108-10-1 4-Methyl-2-pentanone (MIBK)ND 5.0 1.0 ug/l
1634-04-4 Methyl Tert Butyl Ether ND 1.0 0.23 ug/l
91-20-3 Naphthalene ND 5.0 1.0 ug/l
103-65-1 n-Propylbenzene ND 1.0 0.29 ug/l
100-42-5 Styrene ND 1.0 0.22 ug/l
630-20-6 1,1,1,2-Tetrachloroethane ND 1.0 0.28 ug/l
79-34-5 1,1,2,2-Tetrachloroethane ND 1.0 0.30 ug/l
127-18-4 Tetrachloroethylene ND 1.0 0.22 ug/l
108-88-3 Toluene ND 1.0 0.30 ug/l
87-61-6 1,2,3-Trichlorobenzene ND 2.0 0.61 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 2.0 0.50 ug/l
71-55-6 1,1,1-Trichloroethane ND 1.0 0.25 ug/l
79-00-5 1,1,2-Trichloroethane ND 1.0 0.47 ug/l
79-01-6 Trichloroethylene ND 1.0 0.35 ug/l
75-69-4 Trichlorofluoromethane ND 2.0 0.50 ug/l
96-18-4 1,2,3-Trichloropropane ND 2.0 0.63 ug/l
95-63-6 1,2,4-Trimethylbenzene ND 1.0 0.32 ug/l
108-67-8 1,3,5-Trimethylbenzene ND 1.0 0.27 ug/l
108-05-4 Vinyl Acetate ND 10 2.0 ug/l
75-01-4 Vinyl Chloride ND 1.0 0.41 ug/l
m,p-Xylene ND 2.0 0.47 ug/l
95-47-6 o-Xylene ND 1.0 0.26 ug/l
1330-20-7 Xylene (total)ND 3.0 0.72 ug/l
CAS No.Surrogate Recoveries Limits
1868-53-7 Dibromofluoromethane 106%83-118%
17060-07-0 1,2-Dichloroethane-D4 104%79-125%
2037-26-5 Toluene-D8 99%85-112%
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FA6709755.1.1
Method Blank Summary Page 3 of 3
Job Number:FA67097
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC5382-MB C0135158.D 1 08/20/19 AJ n/a n/a VC5382
The QC reported here applies to the following samples:Method: SW846 8260D
FA67097-1, FA67097-2, FA67097-3, FA67097-4, FA67097-5
CAS No.Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 98%83-118%
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FA6709755.1.1
Blank Spike Summary Page 1 of 3
Job Number:FA67097
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC5382-BS C0135156.D 1 08/20/19 AJ n/a n/a VC5382
The QC reported here applies to the following samples:Method: SW846 8260D
FA67097-1, FA67097-2, FA67097-3, FA67097-4, FA67097-5
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
67-64-1 Acetone 125 142 114 50-147
71-43-2 Benzene 25 22.2 89 81-122
108-86-1 Bromobenzene 25 20.9 84 80-121
74-97-5 Bromochloromethane 25 19.8 79 76-123
75-27-4 Bromodichloromethane 25 25.5 102 79-123
75-25-2 Bromoform 25 23.0 92 66-123
78-93-3 2-Butanone (MEK)125 143 114 56-143
104-51-8 n-Butylbenzene 25 22.4 90 79-126
135-98-8 sec-Butylbenzene 25 22.4 90 83-133
98-06-6 tert-Butylbenzene 25 21.6 86 80-133
56-23-5 Carbon Tetrachloride 25 24.3 97 76-136
108-90-7 Chlorobenzene 25 21.7 87 82-124
75-00-3 Chloroethane 25 20.5 82 62-144
67-66-3 Chloroform 25 23.0 92 80-124
95-49-8 o-Chlorotoluene 25 22.1 88 81-127
106-43-4 p-Chlorotoluene 25 22.0 88 83-130
124-48-1 Dibromochloromethane 25 23.9 96 78-122
106-93-4 1,2-Dibromoethane 25 23.4 94 75-120
75-71-8 Dichlorodifluoromethane 25 28.0 112 42-167
95-50-1 1,2-Dichlorobenzene 25 21.8 87 82-124
541-73-1 1,3-Dichlorobenzene 25 21.7 87 84-125
106-46-7 1,4-Dichlorobenzene 25 21.3 85 78-120
75-34-3 1,1-Dichloroethane 25 23.0 92 81-122
107-06-2 1,2-Dichloroethane 25 23.8 95 75-125
75-35-4 1,1-Dichloroethylene 25 21.9 88 78-137
156-59-2 cis-1,2-Dichloroethylene 25 21.6 86 78-120
156-60-5 trans-1,2-Dichloroethylene 25 22.3 89 76-127
78-87-5 1,2-Dichloropropane 25 22.8 91 76-124
142-28-9 1,3-Dichloropropane 25 21.9 88 80-118
594-20-7 2,2-Dichloropropane 25 23.9 96 74-139
563-58-6 1,1-Dichloropropene 25 23.0 92 79-131
10061-01-5 cis-1,3-Dichloropropene 25 23.1 92 75-118
10061-02-6 trans-1,3-Dichloropropene 25 23.5 94 80-120
108-20-3 Di-Isopropyl Ether 25 21.2 85 68-123
64-17-5 Ethyl Alcohol 500 434 87 46-145
100-41-4 Ethylbenzene 25 22.4 90 81-121
* = Outside of Control Limits.
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FA6709755.2.1
Blank Spike Summary Page 2 of 3
Job Number:FA67097
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC5382-BS C0135156.D 1 08/20/19 AJ n/a n/a VC5382
The QC reported here applies to the following samples:Method: SW846 8260D
FA67097-1, FA67097-2, FA67097-3, FA67097-4, FA67097-5
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
591-78-6 2-Hexanone 125 130 104 61-129
98-82-8 Isopropylbenzene 25 23.6 94 83-132
99-87-6 p-Isopropyltoluene 25 22.1 88 79-130
74-83-9 Methyl Bromide 25 27.5 110 59-143
74-87-3 Methyl Chloride 25 31.4 126 50-159
75-09-2 Methylene Chloride 25 23.6 94 69-135
108-10-1 4-Methyl-2-pentanone (MIBK)125 129 103 66-122
1634-04-4 Methyl Tert Butyl Ether 25 21.3 85 72-117
91-20-3 Naphthalene 25 20.5 82 63-132
103-65-1 n-Propylbenzene 25 22.1 88 82-133
100-42-5 Styrene 25 22.1 88 78-119
630-20-6 1,1,1,2-Tetrachloroethane 25 24.3 97 77-122
79-34-5 1,1,2,2-Tetrachloroethane 25 23.7 95 72-120
127-18-4 Tetrachloroethylene 25 21.8 87 76-135
108-88-3 Toluene 25 21.5 86 80-120
87-61-6 1,2,3-Trichlorobenzene 25 19.7 79 68-131
120-82-1 1,2,4-Trichlorobenzene 25 19.4 78 73-129
71-55-6 1,1,1-Trichloroethane 25 22.6 90 75-130
79-00-5 1,1,2-Trichloroethane 25 22.5 90 76-119
79-01-6 Trichloroethylene 25 22.0 88 81-126
75-69-4 Trichlorofluoromethane 25 23.2 93 71-156
96-18-4 1,2,3-Trichloropropane 25 24.4 98 77-120
95-63-6 1,2,4-Trimethylbenzene 25 21.9 88 79-120
108-67-8 1,3,5-Trimethylbenzene 25 22.5 90 79-120
108-05-4 Vinyl Acetate 125 131 105 43-154
75-01-4 Vinyl Chloride 25 27.5 110 69-159
m,p-Xylene 50 45.6 91 79-126
95-47-6 o-Xylene 25 22.9 92 80-127
1330-20-7 Xylene (total)75 68.5 91 80-126
CAS No.Surrogate Recoveries BSP Limits
1868-53-7 Dibromofluoromethane 103%83-118%
17060-07-0 1,2-Dichloroethane-D4 106%79-125%
2037-26-5 Toluene-D8 100%85-112%
* = Outside of Control Limits.
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FA6709755.2.1
Blank Spike Summary Page 3 of 3
Job Number:FA67097
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
VC5382-BS C0135156.D 1 08/20/19 AJ n/a n/a VC5382
The QC reported here applies to the following samples:Method: SW846 8260D
FA67097-1, FA67097-2, FA67097-3, FA67097-4, FA67097-5
CAS No.Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 97%83-118%
* = Outside of Control Limits.
42 of 50
FA6709755.2.1
Matrix Spike/Matrix Spike Duplicate Summary Page 1 of 3
Job Number:FA67097
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA67138-31MS C0135168.D 5 08/20/19 AJ n/a n/a VC5382
FA67138-31MSD C0135169.D 5 08/20/19 AJ n/a n/a VC5382
FA67138-31 C0135162.D 1 08/20/19 AJ n/a n/a VC5382
The QC reported here applies to the following samples:Method: SW846 8260D
FA67097-1, FA67097-2, FA67097-3, FA67097-4, FA67097-5
FA67138-31 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
67-64-1 Acetone 12.2 J 625 634 99 625 620 97 2 50-147/21
71-43-2 Benzene ND 125 118 94 125 121 97 3 81-122/14
108-86-1 Bromobenzene ND 125 113 90 125 109 87 4 80-121/14
74-97-5 Bromochloromethane ND 125 110 88 125 115 92 4 76-123/14
75-27-4 Bromodichloromethane ND 125 139 111 125 134 107 4 79-123/19
75-25-2 Bromoform ND 125 118 94 125 122 98 3 66-123/21
78-93-3 2-Butanone (MEK)ND 625 668 107 625 694 111 4 56-143/18
104-51-8 n-Butylbenzene ND 125 119 95 125 118 94 1 79-126/16
135-98-8 sec-Butylbenzene ND 125 119 95 125 117 94 2 83-133/16
98-06-6 tert-Butylbenzene ND 125 116 93 125 114 91 2 80-133/16
56-23-5 Carbon Tetrachloride ND 125 129 103 125 130 104 1 76-136/23
108-90-7 Chlorobenzene ND 125 118 94 125 115 92 3 82-124/14
75-00-3 Chloroethane ND 125 118 94 125 120 96 2 62-144/20
67-66-3 Chloroform ND 125 127 102 125 127 102 0 80-124/15
95-49-8 o-Chlorotoluene ND 125 116 93 125 114 91 2 81-127/15
106-43-4 p-Chlorotoluene ND 125 120 96 125 114 91 5 83-130/15
124-48-1 Dibromochloromethane ND 125 124 99 125 125 100 1 78-122/19
106-93-4 1,2-Dibromoethane ND 125 123 98 125 120 96 2 75-120/13
75-71-8 Dichlorodifluoromethane ND 125 148 118 125 149 119 1 42-167/19
95-50-1 1,2-Dichlorobenzene ND 125 115 92 125 115 92 0 82-124/14
541-73-1 1,3-Dichlorobenzene ND 125 114 91 125 115 92 1 84-125/14
106-46-7 1,4-Dichlorobenzene ND 125 113 90 125 109 87 4 78-120/15
75-34-3 1,1-Dichloroethane ND 125 124 99 125 127 102 2 81-122/15
107-06-2 1,2-Dichloroethane ND 125 127 102 125 126 101 1 75-125/14
75-35-4 1,1-Dichloroethylene ND 125 115 92 125 113 90 2 78-137/18
156-59-2 cis-1,2-Dichloroethylene ND 125 118 94 125 120 96 2 78-120/15
156-60-5 trans-1,2-Dichloroethylene ND 125 122 98 125 122 98 0 76-127/17
78-87-5 1,2-Dichloropropane ND 125 125 100 125 127 102 2 76-124/14
142-28-9 1,3-Dichloropropane ND 125 119 95 125 117 94 2 80-118/13
594-20-7 2,2-Dichloropropane ND 125 130 104 125 124 99 5 74-139/17
563-58-6 1,1-Dichloropropene ND 125 129 103 125 126 101 2 79-131/16
10061-01-5 cis-1,3-Dichloropropene ND 125 121 97 125 128 102 6 75-118/23
10061-02-6 trans-1,3-Dichloropropene ND 125 126 101 125 121 97 4 80-120/22
108-20-3 Di-Isopropyl Ether ND 125 115 92 125 116 93 1 68-123/16
64-17-5 Ethyl Alcohol ND 2500 2420 97 2500 2380 95 2 46-145/30
100-41-4 Ethylbenzene ND 125 122 98 125 118 94 3 81-121/14
* = Outside of Control Limits.
43 of 50
FA6709755.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 2 of 3
Job Number:FA67097
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA67138-31MS C0135168.D 5 08/20/19 AJ n/a n/a VC5382
FA67138-31MSD C0135169.D 5 08/20/19 AJ n/a n/a VC5382
FA67138-31 C0135162.D 1 08/20/19 AJ n/a n/a VC5382
The QC reported here applies to the following samples:Method: SW846 8260D
FA67097-1, FA67097-2, FA67097-3, FA67097-4, FA67097-5
FA67138-31 Spike MS MS Spike MSD MSD Limits
CAS No.Compound ug/l Q ug/l ug/l %ug/l ug/l %RPD Rec/RPD
591-78-6 2-Hexanone ND 625 672 108 625 657 105 2 61-129/18
98-82-8 Isopropylbenzene ND 125 129 103 125 122 98 6 83-132/15
99-87-6 p-Isopropyltoluene ND 125 115 92 125 115 92 0 79-130/16
74-83-9 Methyl Bromide ND 125 122 98 125 128 102 5 59-143/19
74-87-3 Methyl Chloride ND 125 166 133 125 165 132 1 50-159/19
75-09-2 Methylene Chloride ND 125 126 101 125 128 102 2 69-135/16
108-10-1 4-Methyl-2-pentanone (MIBK)ND 625 658 105 625 632 101 4 66-122/16
1634-04-4 Methyl Tert Butyl Ether ND 125 114 91 125 113 90 1 72-117/14
91-20-3 Naphthalene ND 125 104 83 125 105 84 1 63-132/25
103-65-1 n-Propylbenzene ND 125 117 94 125 115 92 2 82-133/15
100-42-5 Styrene ND 125 124 99 125 121 97 2 78-119/23
630-20-6 1,1,1,2-Tetrachloroethane ND 125 128 102 125 125 100 2 77-122/19
79-34-5 1,1,2,2-Tetrachloroethane ND 125 127 102 125 126 101 1 72-120/14
127-18-4 Tetrachloroethylene ND 125 115 92 125 114 91 1 76-135/16
108-88-3 Toluene ND 125 116 93 125 113 90 3 80-120/14
87-61-6 1,2,3-Trichlorobenzene ND 125 98.6 79 125 103 82 4 68-131/25
120-82-1 1,2,4-Trichlorobenzene ND 125 99.5 80 125 100 80 1 73-129/20
71-55-6 1,1,1-Trichloroethane ND 125 125 100 125 125 100 0 75-130/16
79-00-5 1,1,2-Trichloroethane ND 125 122 98 125 122 98 0 76-119/14
79-01-6 Trichloroethylene ND 125 120 96 125 122 98 2 81-126/15
75-69-4 Trichlorofluoromethane ND 125 126 101 125 127 102 1 71-156/21
96-18-4 1,2,3-Trichloropropane ND 125 126 101 125 119 95 6 77-120/16
95-63-6 1,2,4-Trimethylbenzene ND 125 115 92 125 115 92 0 79-120/18
108-67-8 1,3,5-Trimethylbenzene ND 125 117 94 125 117 94 0 79-120/19
108-05-4 Vinyl Acetate ND 625 711 114 625 695 111 2 43-154/14
75-01-4 Vinyl Chloride ND 125 134 107 125 143 114 6 69-159/18
m,p-Xylene ND 250 246 98 250 245 98 0 79-126/15
95-47-6 o-Xylene ND 125 124 99 125 121 97 2 80-127/14
1330-20-7 Xylene (total)ND 375 371 99 375 366 98 1 80-126/15
CAS No.Surrogate Recoveries MS MSD FA67138-31 Limits
1868-53-7 Dibromofluoromethane 104%105%105%83-118%
17060-07-0 1,2-Dichloroethane-D4 104%103%106%79-125%
2037-26-5 Toluene-D8 98%97%96%85-112%
* = Outside of Control Limits.
44 of 50
FA6709755.3.1
Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number:FA67097
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
FA67138-31MS C0135168.D 5 08/20/19 AJ n/a n/a VC5382
FA67138-31MSD C0135169.D 5 08/20/19 AJ n/a n/a VC5382
FA67138-31 C0135162.D 1 08/20/19 AJ n/a n/a VC5382
The QC reported here applies to the following samples:Method: SW846 8260D
FA67097-1, FA67097-2, FA67097-3, FA67097-4, FA67097-5
CAS No.Surrogate Recoveries MS MSD FA67138-31 Limits
460-00-4 4-Bromofluorobenzene 94%92%96%83-118%
* = Outside of Control Limits.
45 of 50
FA6709755.3.1
SGS North America Inc.
MS Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
Orlando, FL
Section 6
46 of 50
FA670976
Method Blank Summary Page 1 of 2
Job Number:FA67097
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP76458-MB X066577.D 1 08/20/19 MV 08/20/19 OP76458 SX2743
The QC reported here applies to the following samples:Method: SW846 8270E
FA67097-1, FA67097-2, FA67097-3, FA67097-4
CAS No.Compound Result RL MDL Units Q
65-85-0 Benzoic Acid ND 50 10 ug/l
59-50-7 4-Chloro-3-methyl Phenol ND 5.0 0.59 ug/l
95-57-8 2-Chlorophenol ND 5.0 0.63 ug/l
120-83-2 2,4-Dichlorophenol ND 5.0 0.84 ug/l
105-67-9 2,4-Dimethylphenol ND 5.0 0.74 ug/l
51-28-5 2,4-Dinitrophenol ND 25 5.0 ug/l
534-52-1 4,6-Dinitro-o-cresol ND 10 2.0 ug/l
95-48-7 2-Methylphenol ND 5.0 0.56 ug/l
3&4-Methylphenol ND 5.0 0.98 ug/l
88-75-5 2-Nitrophenol ND 5.0 0.85 ug/l
100-02-7 4-Nitrophenol ND 25 5.0 ug/l
87-86-5 Pentachlorophenol ND 25 5.0 ug/l
108-95-2 Phenol ND 5.0 0.50 ug/l
88-06-2 2,4,6-Trichlorophenol ND 5.0 0.75 ug/l
83-32-9 Acenaphthene ND 5.0 0.63 ug/l
208-96-8 Acenaphthylene ND 5.0 0.64 ug/l
120-12-7 Anthracene ND 5.0 0.80 ug/l
56-55-3 Benzo(a)anthracene ND 5.0 0.76 ug/l
50-32-8 Benzo(a)pyrene ND 5.0 0.78 ug/l
205-99-2 Benzo(b)fluoranthene ND 5.0 0.78 ug/l
191-24-2 Benzo(g,h,i)perylene ND 5.0 0.82 ug/l
207-08-9 Benzo(k)fluoranthene ND 5.0 0.86 ug/l
100-51-6 Benzyl Alcohol ND 5.0 0.61 ug/l
101-55-3 4-Bromophenyl Phenyl Ether ND 5.0 0.85 ug/l
85-68-7 Butyl Benzyl Phthalate ND 5.0 1.0 ug/l
106-47-8 4-Chloroaniline ND 5.0 0.63 ug/l
111-91-1 bis(2-Chloroethoxy)methane ND 5.0 0.81 ug/l
111-44-4 bis(2-Chloroethyl)ether ND 5.0 0.73 ug/l
108-60-1 2,2'-Oxybis(1-chloropropane)ND 5.0 0.76 ug/l
91-58-7 2-Chloronaphthalene ND 5.0 0.50 ug/l
7005-72-3 4-Chlorophenyl Phenyl Ether ND 5.0 0.54 ug/l
218-01-9 Chrysene ND 5.0 0.85 ug/l
53-70-3 Dibenzo(a,h)anthracene ND 5.0 0.80 ug/l
132-64-9 Dibenzofuran ND 5.0 0.60 ug/l
95-50-1 1,2-Dichlorobenzene ND 5.0 0.50 ug/l
541-73-1 1,3-Dichlorobenzene ND 5.0 0.50 ug/l
47 of 50
FA6709766.1.1
Method Blank Summary Page 2 of 2
Job Number:FA67097
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP76458-MB X066577.D 1 08/20/19 MV 08/20/19 OP76458 SX2743
The QC reported here applies to the following samples:Method: SW846 8270E
FA67097-1, FA67097-2, FA67097-3, FA67097-4
CAS No.Compound Result RL MDL Units Q
106-46-7 1,4-Dichlorobenzene ND 5.0 0.50 ug/l
91-94-1 3,3'-Dichlorobenzidine ND 5.0 0.64 ug/l
84-66-2 Diethyl Phthalate ND 5.0 1.0 ug/l
131-11-3 Dimethyl Phthalate ND 5.0 1.0 ug/l
84-74-2 Di-n-butyl Phthalate ND 5.0 1.0 ug/l
117-84-0 Di-n-octyl Phthalate ND 5.0 1.0 ug/l
122-66-7 1,2-Diphenylhydrazine ND 5.0 0.76 ug/l
117-81-7 bis(2-Ethylhexyl)phthalate ND 5.0 1.0 ug/l
206-44-0 Fluoranthene ND 5.0 0.55 ug/l
86-73-7 Fluorene ND 5.0 0.70 ug/l
118-74-1 Hexachlorobenzene ND 5.0 0.69 ug/l
87-68-3 Hexachlorobutadiene ND 5.0 0.50 ug/l
77-47-4 Hexachlorocyclopentadiene ND 5.0 1.8 ug/l
67-72-1 Hexachloroethane ND 5.0 1.6 ug/l
193-39-5 Indeno(1,2,3-cd)pyrene ND 5.0 0.71 ug/l
78-59-1 Isophorone ND 5.0 0.78 ug/l
90-12-0 1-Methylnaphthalene ND 5.0 0.53 ug/l
91-57-6 2-Methylnaphthalene ND 5.0 0.60 ug/l
91-20-3 Naphthalene ND 5.0 0.50 ug/l
98-95-3 Nitrobenzene ND 5.0 0.93 ug/l
621-64-7 N-Nitrosodi-n-propylamine ND 5.0 0.67 ug/l
86-30-6 N-Nitrosodiphenylamine ND 5.0 0.81 ug/l
85-01-8 Phenanthrene ND 5.0 0.86 ug/l
129-00-0 Pyrene ND 5.0 0.68 ug/l
120-82-1 1,2,4-Trichlorobenzene ND 5.0 1.1 ug/l
CAS No.Surrogate Recoveries Limits
367-12-4 2-Fluorophenol 47%14-67%
4165-62-2 Phenol-d5 35%10-50%
118-79-6 2,4,6-Tribromophenol 87%33-118%
4165-60-0 Nitrobenzene-d5 80%42-108%
321-60-8 2-Fluorobiphenyl 81%40-106%
1718-51-0 Terphenyl-d14 81%39-121%
48 of 50
FA6709766.1.1
Blank Spike Summary Page 1 of 2
Job Number:FA67097
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP76458-BS X066576.D 1 08/20/19 MV 08/20/19 OP76458 SX2743
The QC reported here applies to the following samples:Method: SW846 8270E
FA67097-1, FA67097-2, FA67097-3, FA67097-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
65-85-0 Benzoic Acid 100 39.8 40 10-69
59-50-7 4-Chloro-3-methyl Phenol 50 40.5 81 54-103
95-57-8 2-Chlorophenol 50 38.4 77 52-98
120-83-2 2,4-Dichlorophenol 50 44.8 90 53-103
105-67-9 2,4-Dimethylphenol 50 39.4 79 43-90
51-28-5 2,4-Dinitrophenol 100 80.0 80 44-112
534-52-1 4,6-Dinitro-o-cresol 100 99.0 99 66-121
95-48-7 2-Methylphenol 50 29.6 59 43-90
3&4-Methylphenol 100 54.7 55 36-88
88-75-5 2-Nitrophenol 50 53.4 107*53-102
100-02-7 4-Nitrophenol 100 42.4 42 18-62
87-86-5 Pentachlorophenol 100 94.3 94 61-115
108-95-2 Phenol 50 18.1 36 19-56
88-06-2 2,4,6-Trichlorophenol 50 52.2 104 59-107
83-32-9 Acenaphthene 50 43.8 88 61-107
208-96-8 Acenaphthylene 50 46.2 92 60-104
120-12-7 Anthracene 50 45.2 90 65-108
56-55-3 Benzo(a)anthracene 50 48.3 97 66-111
50-32-8 Benzo(a)pyrene 50 45.3 91 62-107
205-99-2 Benzo(b)fluoranthene 50 47.6 95 65-114
191-24-2 Benzo(g,h,i)perylene 50 52.4 105 66-116
207-08-9 Benzo(k)fluoranthene 50 45.5 91 65-114
100-51-6 Benzyl Alcohol 50 29.0 58 46-94
101-55-3 4-Bromophenyl Phenyl Ether 50 50.1 100 65-109
85-68-7 Butyl Benzyl Phthalate 50 49.7 99 65-112
106-47-8 4-Chloroaniline 50 38.5 77 49-105
111-91-1 bis(2-Chloroethoxy)methane 50 45.0 90 51-102
111-44-4 bis(2-Chloroethyl)ether 50 41.3 83 53-100
108-60-1 2,2'-Oxybis(1-chloropropane)50 40.1 80 45-106
91-58-7 2-Chloronaphthalene 50 45.1 90 57-103
7005-72-3 4-Chlorophenyl Phenyl Ether 50 46.2 92 62-105
218-01-9 Chrysene 50 47.3 95 66-111
53-70-3 Dibenzo(a,h)anthracene 50 52.5 105 66-119
132-64-9 Dibenzofuran 50 43.8 88 61-106
95-50-1 1,2-Dichlorobenzene 50 41.4 83 48-97
541-73-1 1,3-Dichlorobenzene 50 42.0 84 45-95
* = Outside of Control Limits.
49 of 50
FA6709766.2.1
Blank Spike Summary Page 2 of 2
Job Number:FA67097
Account:RENCM Resolve Environmental
Project:Five Points Gateway; 320/322 Franklin, Monroe, NC
Sample File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
OP76458-BS X066576.D 1 08/20/19 MV 08/20/19 OP76458 SX2743
The QC reported here applies to the following samples:Method: SW846 8270E
FA67097-1, FA67097-2, FA67097-3, FA67097-4
Spike BSP BSP
CAS No.Compound ug/l ug/l %Limits
106-46-7 1,4-Dichlorobenzene 50 42.0 84 45-98
91-94-1 3,3'-Dichlorobenzidine 50 53.1 106 46-117
84-66-2 Diethyl Phthalate 50 44.9 90 64-108
131-11-3 Dimethyl Phthalate 50 46.1 92 63-106
84-74-2 Di-n-butyl Phthalate 50 48.4 97 65-107
117-84-0 Di-n-octyl Phthalate 50 49.4 99 62-118
122-66-7 1,2-Diphenylhydrazine 50 43.5 87 61-110
117-81-7 bis(2-Ethylhexyl)phthalate 50 51.0 102 61-117
206-44-0 Fluoranthene 50 45.4 91 63-106
86-73-7 Fluorene 50 43.9 88 62-108
118-74-1 Hexachlorobenzene 50 47.0 94 63-108
87-68-3 Hexachlorobutadiene 50 43.1 86 42-102
77-47-4 Hexachlorocyclopentadiene 50 43.3 87 39-102
67-72-1 Hexachloroethane 50 41.4 83 42-100
193-39-5 Indeno(1,2,3-cd)pyrene 50 54.0 108 64-119
78-59-1 Isophorone 50 40.0 80 43-87
90-12-0 1-Methylnaphthalene 50 41.1 82 53-102
91-57-6 2-Methylnaphthalene 50 41.5 83 51-102
91-20-3 Naphthalene 50 43.5 87 47-100
98-95-3 Nitrobenzene 50 43.0 86 50-104
621-64-7 N-Nitrosodi-n-propylamine 50 37.4 75 52-104
86-30-6 N-Nitrosodiphenylamine 50 47.3 95 64-108
85-01-8 Phenanthrene 50 45.7 91 66-110
129-00-0 Pyrene 50 49.3 99 64-113
120-82-1 1,2,4-Trichlorobenzene 50 44.8 90 45-97
CAS No.Surrogate Recoveries BSP Limits
367-12-4 2-Fluorophenol 46%14-67%
4165-62-2 Phenol-d5 33%10-50%
118-79-6 2,4,6-Tribromophenol 97%33-118%
4165-60-0 Nitrobenzene-d5 83%42-108%
321-60-8 2-Fluorobiphenyl 87%40-106%
1718-51-0 Terphenyl-d14 83%39-121%
* = Outside of Control Limits.
50 of 50
FA6709766.2.1

APPENDIX D
Brownfields Property Receptor Survey Form

North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Site:Five Points Gateway Redevelopment
Address:320-322 E. Franklin Street
City:Monroe
County:Union
Brownfields Project Number:21050-17-090
Property and Building Characteristics
a. Provide occupancy and use information.
No structures on site.
No structures on site.
c. Describe the foundation construction. Include details on type, floor construction, and depth below grade.
Not applicable (NA).
NA
e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details.
NA
Surface Conditions
Size of Property (acres)
% of property that is wooded/brush
If an existing building is on-site, please respond to the following. Information can be provided on additional sheets
as needed. If numerous buildings are on-site, consult with your PM as only information on specific buildings may
be needed.
b. Describe the construction of the builidng including materials (e.g. wood frame, block), type and size of openings
(e.g. windows, bay doors), and height (number of stories).
% of property that is covered by buildings
1.78
1%; None
20%; None
80%; Parking lot
NA
Commercial
Commercial
Commercial
BROWNFIELDS PROPERTY RECEPTOR SURVEY
This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the
information requested below. Distances are measured from the site property boundary unless otherwise indicated
by the DEQ Brownfield’s Project Manager (PM).
Current Usage Proposed Usage
Commercial
Commercial
d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air
return, and design considerations (e.g. positive pressure?).
0%
0%
% of property that is grassed areas
% of property that is agricultural crops
% of property that is paved
Rev. 09/2015 Page 1 of 3
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Surrounding Property Land Use
North
South
East
West
Y 380 South
Y 440, 580 North
Unknown
Utilities
Is there a septic system on-site? (Y or N) ____N_____
Please provide the utility providers for the subject property
a. Natural Gas City of Monroe
b. Sewer
c. Electricity City of Monroe
d. Other
For surrounding properties, please complete the following table with available information.
Y on site
Y on site
N
Y 60 N
Y 30 N
Y 30 N
N
* If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with
the subject property.
Is a water line main within 100 ft of Property boundary?
Is a natural gas line main within 100 ft of the Property boundary?
Is a buried telephone/ cable main within 100 ft of the Property boundary?
Is a septic system leach field within 500 ft of the Property boundary?
Direction
Is there a basement within 1,000 ft of the Property
Distance
(ft)Address
308 E. Windsor St.
Zoning/Land Use
351 Crow St.
322 E. Windsor St.
Direction
Proposed Usage Current Use/Occupant
same
Please provide information on the following land uses in the vicinity of the subject site, including a map of the
surrounding areas. If specific receptors are present, please provide addresses of the facilities.
same
natural area
same
E. Franklin Street/barber shop/beauty salon (commercial)
City of Monroe property; vacant (partial), Science Center
City of Monroe property; vacant
City of Monroe property; parking lot
For the subject property, please provide a map of known buried utilites. If available, include depth to top,
construction material, and diameter of the utilities. In addition, please provide the following information on utilty
providers. If additional assessment is required, the public utility locators should be contacted. This information can
then be added to a site map.
Y/N *
Is a school or daycare center within 1,000 ft of the
Property?
Specific Land Uses of Interest Y/N *
* If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing specific
addresses.
Distance
(ft)Utility/Potential Receptor
Is a buried electrical cable main within 100 ft of Property boundary?
Is a storm water pipe within 100 ft of the Property boundary?
Is a sanitary sewer within 100 ft of the Property boundary?
Is there a residence within 1,000 ft of the Property?
City of Monroe
Rev. 09/2015 Page 2 of 3
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Water Supply
What is the potable water supply for the property? Public ___X___ Private ______
N
N
N
Surface Water & Wetlands
AddressY/NWater Supply Wells
Please provide the following information regarding water supply wells in the vicinity of the Property. At a
minimum, a windshield survey within 1,500 ft of the property boundaries should be completed to determine if
water supply or irrigation wells may be present. Information from applicable databases can and should be utilized;
however, should not be utilized in lieu of the windshield survey. If multiple wells are present within the requested
radius, please provide a map of the well locations. If needed, please attach a separate table to list all wells. Please
note, the PM may opt for a more extensive water supply well survey if needed.
Provide Information regarding Surface Water
and Wetlands
The purpose of this section is to provide information on the water supply for the site and surrounding areas.
No
Are there surface water features on the
property? (If yes, please complete a. to d.)
If Private, please provide details of the water supply source (i.e. well location, well construction, etc). If public,
please include the water providers name.
Distance
(ft)Direction
a. Is the water body naturally developed or
man-made?NA
NA
NA
Is a public water supply well within 1 mile of the Property boundary?
Is a private water supply well within 1,500 ft of the Property
boundary?Is an irrigation well within 1,500 ft of the Property boundary?
Response/Comments
The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in
the vicinity of the Property.
NA
Bearskin Creek approximately 2,500 feet North of site
No
b. List the uses of the water body.
c. What is the source of the water for the
water body?
d. What is the nature of the bottom of the
water body (e.g., rocky or concrete bottom,
drainage ways or impoundments)
If no on-site surface water features, what is the
nearest surface water body?
Are there any wetlands present on the
property? If no wetlands on-site, are wetlands
suspected on adjoining properties?
Rev. 09/2015 Page 3 of 3

APPENDIX E
Zoning Map – City of Monroe

GoMaps
Sources: Esri, HERE, Garmin, USGS, Intermap, INCREMENT P,NRCan, Esri Japan, METI, Esri China (Hong Kong), Esri Korea,Esri (Thailand), NGCC, (c) OpenStreetMap contributors, and theGIS User Community
Parcels
R-40
R-20
R-20-SU
R-15-SU
R-12-SU
R-10
R-10-SU
R-P1-SU
R-MF
R-MH
R-O-SU
B-1-SU
B-3-SU
B-4-SU
B-5-SU
M-U-SU
G-I
G-I-SU
OT
CBD
GB
CD
October 10, 2019 0 0.1 0.20.05 mi
0 0.15 0.30.075 km
1:7,073