October 2019 - Surface Water &Groundwater Assessment Report - Ticar Chemical Co

Former Ticar Chemical Company
32 Old Brevard Road
Asheville, North Carolina
Headwater Project # A19-101B-A03
Prepared for:
Ticar Chemical Company
c/o William Clarke, Esq.
Roberts and Stevens, PA
301 College Street, Suite 400
Asheville, North Carolina

December 11, 2019

Groundwater and Surface Water Assessment
Report

Groundwater and Surface Water Sampling
Report
Former Ticar Chemical Company
32 Old Brevard Road
Asheville, North Carolina
Headwater Project # A19-101B-A03
December 11, 2019
Prepared for
Ticar Chemical Company
c/o William Clarke, Esq.
Roberts and Stevens, PA
301 College Street, Suite 400
Asheville, North Carolina

Prepared by
Headwater Geology, PLLC.
45 South French Broad Avenue, #170
Asheville, North Carolina 28801
__________________________
Adam M. Tripp, PG
Senior Geologist
Firm License # C-566

Former Ticar Chemical Company—Groundwater and Surface Water Monitoring Report

Headwater Geology i
TABLE OF CONTENTS
1 Introduction ............................................................................................................... 1
1.1 Purpose .............................................................................................................................. 1
2 Site Activities ............................................................................................................ 2
2.1 Groundwater Sampling ...................................................................................................... 2
2.2 Surface Water Sampling .................................................................................................... 2
2.3 Sample Analyses ............................................................................................................... 3
3 Results ...................................................................................................................... 4
3.1 Groundwater Results ......................................................................................................... 4
3.2 Surface Water Results ....................................................................................................... 4
4 Risk Evaluation ......................................................................................................... 5
4.1 Vapor Intrusion Risk Evaluation ......................................................................................... 5
4.2 Surface Water Risk Evaluation .......................................................................................... 5
5 Conclusions and Recommendations ........................................................................ 6
6 References ............................................................................................................... 7

FIGURES
Figure 1 Site Location Map
Figure 2 Groundwater and Surface Water Sample Location Map
TABLES
Table 1 Groundwater Elevation Data
Table 2 Field Parameters Summary
Table 3 Water Sampling Analytical Results
APPENIDCES
Appendix A Sampling Logs
Appendix B Laboratory Analytical Report and Chain-of-Custody Form
Appendix C Tier 2 Risk Evaluation Data Sheet

Former Ticar Chemical Company—Groundwater and Surface Water Monitoring Report

Headwater Geology 1
1 Introduction
Headwater Geology, PLLC. (Headwater), on behalf of the Former Ticar Chemical Company (Ticar
Chemical), has completed groundwater and surface water assessment activities at 32 Old
Brevard Road in Asheville, North Carolina (the Site). A Site Location Map is included as Figure 1.
The Site is currently owned by Jedhy, LLC, and has been deemed eligible to participate in the
North Carolina Brownfields Program (Site ID # 17041-13-011). The Site is listed as a North
Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Site (Site ID #
NONCD0002599), under jurisdiction of the Inactive Hazardous Sites Branch (IHSB). Assessment
and remedial activities have been ongoing at the Site since the late-1980s. A thorough summary
of historical activities is documented in the Groundwater and Surface Water Assessment Report,
prepared by Anchor QEA of North Carolina, PLLC (Anchor QEA), and dated May 2018 (Anchor
QEA 2018a).
The most recent assessment activities included the sampling of two groundwater monitoring wells
(OS-03, GW-3). Two surface water samples were also collected from existing surface water
sample locations (SW-1 and SW-2). Activities were performed in general accordance with the
methodology and scope of work described in the Environmental Monitoring Work Plan, prepared
by Headwater, and dated October 11, 2019 (Headwater 2019). The Environmental Monitoring
Work Plan was approved by the DEQ-IHSB and Brownfields Program in emails sent on October
17, 2019.
1.1 Purpose
The purpose of this assessment is to further evaluate surface water and groundwater conditions.
The groundwater assessment data was used to evaluate potential vapor intrusion associated with
a nearby off-Site property (Johnstone Supply, a distributer of refrigeration parts and supplies).
Surface water samples were collected to measure concentrations of contaminates of concern in
surface water and to evaluate potential risk to receptor associated with those concentrations.

Former Ticar Chemical Company—Groundwater and Surface Water Monitoring Report

Headwater Geology 2
2 Site Activities
Assessment activities included the collection of groundwater samples from two monitoring wells
and two surface water samples on October 10, 2019.
2.1 Groundwater Sampling
Groundwater samples were collected at the Site from monitoring wells OS-3 and GW-3 using low-
flow sampling methods on October 10, 2019.
Prior to purging, groundwater levels were measured using a water level meter. Water level
elevation information is included in Table 1. A groundwater sample was collected in monitoring
well GW-3 after field parameters had stabilized. Field parameters (pH, temperature, dissolved
oxygen, specific conductivity, and oxidation reduction potential) were measured every 3 minutes
with a calibrated YSI 556 multi-parameter water quality meter. Turbidity was also measured, using
a Hach 2100Q turbidity meter. Field parameters for groundwater are included in Table 2 and field
logs are included as Appendix A. Parameters were considered stabilized after three consecutive
readings were within the following ranges:
 pH: ± 0.1 unit
 Specific conductivity: ± 3%
 Temperature, dissolved oxygen, and turbidity: ± 10%
 Oxidation reduction potential: ± 10 millivolts
 Turbidity: less than 10 Nephelometric Turbidity Units (NTUs) (if practical)
Due to low water volume in OS-3, the well was pumped dry, allowed to recharge, and then
sampled. Therefore, field parameters had not stabilized before a sample was collected from this
well.
Samples were transferred to laboratory-provided sample containers and placed in a cooler on ice
for delivery to the laboratory.
2.2 Surface Water Sampling
On October 10, 2019, one upstream (SW-1) and one downstream (SW-2) surface water sample
were collected at the locations shown in the attached Figure 2. Samples were collected by
submerging a clean glass container into the stream and then transferring the sample to the
laboratory-provided sample container. The sample containers were placed in a cooler with ice for
delivery to the laboratory.
Former Ticar Chemical Company—Groundwater and Surface Water Monitoring Report

Headwater Geology 3
2.3 Sample Analyses
Surface and groundwater samples were analyzed by Pace Analytical Services, LLC, a North
Carolina-certified laboratory, for volatile organic compounds (VOCs) using the U.S.
Environmental Protection Agency (EPA) Standard Method 8260B.

Former Ticar Chemical Company—Groundwater and Surface Water Monitoring Report

Headwater Geology 4
3 Results
Surface water and groundwater results are summarized in the following subsections.
Groundwater and surface water analytical results are summarized in Table 3. The laboratory
analytical report is included in Appendix B.
Groundwater analytical results were compared to the 15A North Carolina Administrative Code
02L .0202 groundwater standards (2L standards). Surface water analytical results were compared
to the 2B standards or to the EPA Nationally Recommended Water Quality Criteria (NRWQC)
Human Health surface water quality standards, effective June 10, 2019. If no 2L standard was
established for a constituent, results for that constituent were compared to the applicable DEQ
Interim Maximum Allowable Concentration (IMAC). Groundwater results were also compared to
the North Carolina Division of Waste Management (DWM) Non-Residential Vapor Intrusion
Groundwater Screening Levels (GWSLs).
3.1 Groundwater Results
Tetrachloroethene (PCE) was detected above its respective 2L standard (0.7 micrograms per
Liter [µg/L]) in monitoring wells: OS-3 and GW-3. Additionally, PCE was detected above its
respective GWSL (48 µg/L) in monitoring wells OS-3 and GW-3.
In monitoring well OS-3, Trichloroethene (TCE) was detected above its respective 2L standard (3
µg/L), but below the applicable GWSL.
3.2 Surface Water Results
VOCs were not detected above the laboratory reporting limits in either of the two surface water
samples (SW-1 and SW-2).
Former Ticar Chemical Company—Groundwater and Surface Water Monitoring Report

Headwater Geology 5
4 Risk Evaluation
Headwater performed a Tier 1 Risk Screening and Tier 2 Risk Evaluation in accordance with the
guidelines outlined in DEQ’s Technical Guidance for Risk-Based Remediation document dated
March 2017 (DEQ 2017), and the North Carolina Department of Environmental Quality Risk
Calculator User Guide dated May 2019 (DEQ 2019). A risk screening for vapor intrusion
associated with off-Site Johnstone Supply is described in Section 4.1. A risk evaluation associated
with surface water exposure is described in Section 4.2.
4.1 Vapor Intrusion Risk Evaluation
Groundwater Analytical results for sample GW-3, located adjacent to Johnstone Supply and
downgradient of the Site were evaluated to determine if a vapor intrusion risk for this location is
present. Because concentrations of PCE in GW-3 are above the GWSLs, a Tier 2 Risk Evaluation
was performed.
The Tier 2 Risk Evaluation was performed to evaluate the groundwater to indoor air exposure
pathway for non-residential workers. As such, the most elevated concentration of detected
compounds in the monitoring well was used in in the most recent (Version Date: May 2019) DEQ
Risk Calculator.
The cumulative carcinogenic risk and hazard index calculated was below 1.0 E-05, and 1,
respectively. The Tier 2 Risk Evaluation data sheet is included in Appendix C
4.2 Surface Water Risk Evaluation
Surface water analytical results did not exceed the laboratory detection limits in either sample.
Therefore, no unacceptable risk was identified.

Former Ticar Chemical Company—Groundwater and Surface Water Monitoring Report

Headwater Geology 6
5 Conclusions and Recommendations
Groundwater analytical results and the results of a Tier 2 Risk Evaluation indicate that there is
not a vapor intrusion risk present for the Johnstone Supply building (off-Site property, proximate
to well GW-3). No constituents were detected in surface water above laboratory reporting limits.
Concentrations of VOCs decreased in OS-3 but increased in GW-3. Groundwater elevations in
monitoring wells were measured to have increased from previous gauging events, likely a result
of above average regional precipitation in the area. The change in groundwater elevation could
temporarily affect groundwater VOC concentrations and distribution.
Based on these findings, Headwater recommends the following:
 Headwater recommends performing one additional monitoring event of two monitoring
wells (OS-3 [on-Site] and GW-3 [off-Site]) and two surface water sample locations (SW-1
and SW-2) in October 2020 to verify stability of the groundwater plume.
Former Ticar Chemical Company—Groundwater and Surface Water Monitoring Report

Headwater Geology 7
6 References
Anchor QEA 2018a. Groundwater and Surface Water Assessment Report. May
Anchor QEA 2018b. October 2018 Groundwater and Surface Water Assessment Report.
November
DEQ 2017. Technical Guidance for Risk-Based Remediation. March 2017.
DEQ 2019. North Carolina Department of Environmental Quality Risk Calculator User Guide.
May.
Headwater, 2019. Environmental Monitoring Work Plan. October 11

FIGURES
July 23, 2019
USGS7.5-minute Topographic QuadrangleAsheville, North Carolina (1991)Contour Interval = 20 feet
Former Ticar Chemical CompanyOld Brevard RoadAsheville, Buncombe CountyNorth CarolinaHeadwater Project # A19-101B
FIGURE 1SITE LOCATION MAP
NJC
Date :
Prepared by :
0 2,000 4,0001,000 Feet
1 inch = 2,000 feet¯
SOURCE
Legend
Site boundary
Approximate site location
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170 22752
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Overland Industrial Blvd
Morris Rd
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Albany Grey Dr
SW-3
SW-1
!UDRW-3
RW-1
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OS-3
OS-14
OS-10
GP-3
GP-2GP-1
OS-6
OS-4
OS-7
OS-8 GW-2
GW-1
OS-13
OS-12
OS-16
OS-15
OS-11
OS-17
OS-18B
FIGURE 2GROUNDWATER ANDSURFACE WATER SAMPLELOCATION MAP
10/23/2019Revised 11/25/19
Prepared by:NJC
Former Ticar Chemical CompanyOld Brevard RoadAsheville, Buncombe CountyNorth CarolinaHeadwater Project # A19-101B
Date:
0 250 500125Feet
Legend
5ft contours
Streams
Site boundary
#* Surface water sample location
!U Existing groundwater monitoring well
!UD Former groundwater monitoring well
!UD Former temporary well point installation
!UD Former groundwater recovery well
SOURCE
NC One Map:Orthoimagery (2015), Roads, Streams/Rivers of Western NC
Buncombe County GIS: 5ft contours
Note: Well locations and elevations surveyed in March 2018 by Blue Ridge Land Surveying.1 inch = 250 feet
#*
SW-2
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R
d
SW-2 is located approximately 1,200-feet downstream from SW-1
1159 Brevard Rd(Residence)
Johnstone Supply
Country Casuals
!UD OS-18A
!UD
OS-9
!UDRW-2 !U !UD!UD!UD OS-5
OS-1
OS-2
RW-4
!U
!U
TABLES

Table 1
Groundwater Elevation Data
Ticar Chemical Site
Well ID
TOC Elevation
(feet msl)
Depth to
Groundwater *
(feet TOC)
Depth to Bottom
(feet TOC)
Groundwater
Elevation
(feet msl)
Water Column
(feet)
OS-03 2203.19 38.93 43.38 2165.88 6.07
GW-3 2195.29 41.87 59.84 2152.74 17.29
Notes:
msl: feet above mean sea level relative to North America Vertical Datum of 1988
*: Groundwater measurements were made on October 10, 2019.
TOC: Feet below Top of Casing (TOC). TOC elevations were measured on March 18, 2018 by Blue Ridge Land Surveying
relative to North American Vertical Datum of 1984.
Table 2Field Parameters SummaryTicar Chemical SiteNameSample Collection DateDepth to Groundwater *(feet TOC)Specific Conductivity (µS/cm)DO(mg/L)pH (S.U.) ORP (mV) Turbidity (NTU)GW‐310/11/1941.8776.16.755.08391.984.4OS‐310/11/1938.9398.35.765.0352.528.1Notes:msl: feet above mean sea level relative to North America Vertical Datum of 1988*: Groundwater measurements were made on October 10, 2019.TOC: Feet below Top of Casing (TOC). TOC elevations were measured on March 18, 2018 by Blue Ridge Land Surveying relative to North American Vertical Datum of 1984.
Table 3
Water Sampling Analytical Results
Ticar Chemical Site
Depth to
Groundwater *
(feet TOC)
Date Collected:2/2/18 10/1/18 10/10/19 2/2/18 10/1/18 10/10/19
Units:µg/L µg/L µg/L µg/L µg/L µg/L
VOCs by EPA 8260 2L Standards VI-GWSL
1,1,1-Trichlorethane 200 6,200 < 2.0 1.4 < 1.0 < 1.0 0.33 J < 1.0
1,1-Dichlorethane 6 330 < 2.0 0.25 J < 1.0 < 1.0 < 0.5 < 1.0
1,1-Dichlorethene 350 160 < 2.0 < 0.5 < 1.0 < 1.0 < 0.5 < 1.0
Chloroform 70 36 < 2.0 2.4 < 1.0 < 1.0 < 0.5 < 1.0
Cis-1,2-Dichloroethene 70 NL 28.3 34 6.3 1.5 0.58 2.5
Tetrachloroethene 0.7 48 295 290 59 37.9 31 74.4
Trans-1,2-Dichloroethene 100 NL < 2.0 0.84 < 1.0 < 1.0 < 0.5 < 1.0
Trichlororethene 3 4.4 17.5 23 3.8 1.8 0.98 2.1
Surface Water Sample Location:
Date Collected:2/2/18 10/1/18 10/10/19 2/2/18 10/1/18 10/10/19
Units:µg/L µg/L µg/L µg/L µg/L µg/L
VOCs by EPA 8260 2B Standards
1,1,1-Trichlorethane 2500 < 1.0 0.62 < 1.0 < 1.0 < 0.5 < 1.0
1,1-Dichlorethane NL < 1.0 < 0.5 < 1.0 < 1.0 < 0.5 < 1.0
1,1-Dichlorethene 20000 < 1.0 0.26 J < 1.0 < 1.0 < 0.5 < 1.0
Chloroform 2000 < 1.0 < 0.5 < 1.0 < 1.0 < 0.5 < 1.0
Cis-1,2-Dichloroethene 720 < 1.0 1.0 < 1.0 < 1.0 < 0.5 < 1.0
Tetrachloroethene 3.3 3.1 9.7 < 1.0 < 1.0 < 0.5 < 1.0
Trans-1,2-Dichloroethene NL < 1.0 < 0.5 < 1.0 < 1.0 < 0.5 < 1.0
Trichlororethene 30 < 1.0 1.2 < 1.0 < 1.0 < 0.5 < 1.0
Notes:
EPA U.S. Environmental Protection Agency
2L standard North Carolina Administrative Code (NCAC) Title 15A, Chapter 2, Subchapter 2L- Groundwater Classifications and Standards, DENR (Last Amended April 1, 2013)
2B standard North Carolina Administrative Code (NCAC) Title 15A, Chapter 2, Subchapter 2B- Surface Water And Wetland Classifications and Standards for Class C Waters, or
EPA National Recommended Water Quality Criteria DEQ (Last Amended June 10, 2019)
VI-GWSL North Carolina Division of Waste Management Non-Residential Vapor Intrusion Groundwater Screening Levels (last amended February 2018). VI-GWSLs are based
on a target cancer risk (TCR) and hazard quotient (THQ) of 1.0E-05 and 0.2, respectively.
µg/L micrograms per liter
47.1 Indicates constituent was detected above the laboratory reporting limit.
< 1.0 Indicates constituent concentration was not detected above the laboratory reporting limit.
295 Indicates that the constituent concentration was detected above the GWSL Standard and the 2L Standard.
175 Indicates that the constituent concentration was detected above the 2L Standard.
9.7 Indicates that the constituent concentration was detected above the 2B Standard.
NL Not Listed
OS-3 GW-3
SW-1 SW-2
APPENDIX A
Sampling Logs
APPENDIX B
Laboratory Analytical Report and Chain-of-
Custody Form

#=CL#
October 14, 2019
LIMS USE: FR - ADAM TRIPP
LIMS OBJECT ID: 92449235
92449235
Project:
Pace Project No.:
RE:
Mr. Adam Tripp
Headwater Environmental, Inc.
43 College Place, Suite 212
Asheville, NC 28801
TICAR A19-101B 10/10
Dear Mr. Tripp:
Enclosed are the analytical results for sample(s) received by the laboratory on October 10, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Lorri Patton
[e-mail]
Project Manager
1(828)254-7176
Enclosures
cc:Mr. John Haffner, Headwater Environmental, Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 1 of 20
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92449235
TICAR A19-101B 10/10
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 2 of 20
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92449235
TICAR A19-101B 10/10
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92449235001 GW-3 EPA 8260D 63 PASI-CSAS
92449235002 OS-03 EPA 8260D 63 PASI-CSAS
92449235003 SW-1 EPA 8260D 63 PASI-CSAS
92449235004 SW-2 EPA 8260D 63 PASI-CSAS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 3 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92449235
TICAR A19-101B 10/10
Sample:GW-3 Lab ID:92449235001 Collected:10/10/19 12:11 Received:10/10/19 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 10/12/19 07:24 67-64-125.0 1
Benzene ND ug/L 10/12/19 07:24 71-43-21.0 1
Bromobenzene ND ug/L 10/12/19 07:24 108-86-11.0 1
Bromochloromethane ND ug/L 10/12/19 07:24 74-97-5 v21.0 1
Bromodichloromethane ND ug/L 10/12/19 07:24 75-27-41.0 1
Bromoform ND ug/L 10/12/19 07:24 75-25-21.0 1
Bromomethane ND ug/L 10/12/19 07:24 74-83-9 v22.0 1
2-Butanone (MEK)ND ug/L 10/12/19 07:24 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/12/19 07:24 56-23-51.0 1
Chlorobenzene ND ug/L 10/12/19 07:24 108-90-71.0 1
Chloroethane ND ug/L 10/12/19 07:24 75-00-3 v21.0 1
Chloroform ND ug/L 10/12/19 07:24 67-66-35.0 1
Chloromethane ND ug/L 10/12/19 07:24 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/12/19 07:24 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/12/19 07:24 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/19 07:24 96-12-85.0 1
Dibromochloromethane ND ug/L 10/12/19 07:24 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/12/19 07:24 106-93-41.0 1
Dibromomethane ND ug/L 10/12/19 07:24 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/12/19 07:24 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/12/19 07:24 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/12/19 07:24 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/12/19 07:24 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/12/19 07:24 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/12/19 07:24 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/12/19 07:24 75-35-41.0 1
cis-1,2-Dichloroethene 2.5 ug/L 10/12/19 07:24 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/12/19 07:24 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/12/19 07:24 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/12/19 07:24 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/12/19 07:24 594-20-7 v21.0 1
1,1-Dichloropropene ND ug/L 10/12/19 07:24 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/12/19 07:24 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/12/19 07:24 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/12/19 07:24 108-20-31.0 1
Ethylbenzene ND ug/L 10/12/19 07:24 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/12/19 07:24 87-68-31.0 1
2-Hexanone ND ug/L 10/12/19 07:24 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/12/19 07:24 99-87-61.0 1
Methylene Chloride ND ug/L 10/12/19 07:24 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/19 07:24 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/12/19 07:24 1634-04-41.0 1
Naphthalene ND ug/L 10/12/19 07:24 91-20-31.0 1
Styrene ND ug/L 10/12/19 07:24 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/19 07:24 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/19 07:24 79-34-51.0 1
Tetrachloroethene 74.4 ug/L 10/12/19 07:24 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/14/2019 04:04 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 4 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92449235
TICAR A19-101B 10/10
Sample:GW-3 Lab ID:92449235001 Collected:10/10/19 12:11 Received:10/10/19 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D8260D MSV Low Level
Toluene ND ug/L 10/12/19 07:24 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/12/19 07:24 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/12/19 07:24 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/12/19 07:24 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/12/19 07:24 79-00-51.0 1
Trichloroethene 2.1 ug/L 10/12/19 07:24 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/12/19 07:24 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/12/19 07:24 96-18-41.0 1
Vinyl acetate ND ug/L 10/12/19 07:24 108-05-42.0 1
Vinyl chloride ND ug/L 10/12/19 07:24 75-01-41.0 1
Xylene (Total)ND ug/L 10/12/19 07:24 1330-20-71.0 1
m&p-Xylene ND ug/L 10/12/19 07:24 179601-23-12.0 1
o-Xylene ND ug/L 10/12/19 07:24 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)98 %10/12/19 07:24 460-00-470-130 1
1,2-Dichloroethane-d4 (S)120 %10/12/19 07:24 17060-07-070-130 1
Toluene-d8 (S)99 %10/12/19 07:24 2037-26-570-130 1
Sample:OS-03 Lab ID:92449235002 Collected:10/10/19 14:00 Received:10/10/19 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 10/12/19 07:42 67-64-125.0 1
Benzene ND ug/L 10/12/19 07:42 71-43-21.0 1
Bromobenzene ND ug/L 10/12/19 07:42 108-86-11.0 1
Bromochloromethane ND ug/L 10/12/19 07:42 74-97-5 v21.0 1
Bromodichloromethane ND ug/L 10/12/19 07:42 75-27-41.0 1
Bromoform ND ug/L 10/12/19 07:42 75-25-21.0 1
Bromomethane ND ug/L 10/12/19 07:42 74-83-9 v22.0 1
2-Butanone (MEK)ND ug/L 10/12/19 07:42 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/12/19 07:42 56-23-51.0 1
Chlorobenzene ND ug/L 10/12/19 07:42 108-90-71.0 1
Chloroethane ND ug/L 10/12/19 07:42 75-00-3 v21.0 1
Chloroform ND ug/L 10/12/19 07:42 67-66-35.0 1
Chloromethane ND ug/L 10/12/19 07:42 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/12/19 07:42 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/12/19 07:42 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/19 07:42 96-12-85.0 1
Dibromochloromethane ND ug/L 10/12/19 07:42 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/12/19 07:42 106-93-41.0 1
Dibromomethane ND ug/L 10/12/19 07:42 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/12/19 07:42 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/12/19 07:42 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/12/19 07:42 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/12/19 07:42 75-71-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/14/2019 04:04 PM
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Page 5 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92449235
TICAR A19-101B 10/10
Sample:OS-03 Lab ID:92449235002 Collected:10/10/19 14:00 Received:10/10/19 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D8260D MSV Low Level
1,1-Dichloroethane ND ug/L 10/12/19 07:42 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/12/19 07:42 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/12/19 07:42 75-35-41.0 1
cis-1,2-Dichloroethene 6.3 ug/L 10/12/19 07:42 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/12/19 07:42 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/12/19 07:42 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/12/19 07:42 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/12/19 07:42 594-20-7 v21.0 1
1,1-Dichloropropene ND ug/L 10/12/19 07:42 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/12/19 07:42 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/12/19 07:42 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/12/19 07:42 108-20-31.0 1
Ethylbenzene ND ug/L 10/12/19 07:42 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/12/19 07:42 87-68-31.0 1
2-Hexanone ND ug/L 10/12/19 07:42 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/12/19 07:42 99-87-61.0 1
Methylene Chloride ND ug/L 10/12/19 07:42 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/19 07:42 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/12/19 07:42 1634-04-41.0 1
Naphthalene ND ug/L 10/12/19 07:42 91-20-31.0 1
Styrene ND ug/L 10/12/19 07:42 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/19 07:42 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/19 07:42 79-34-51.0 1
Tetrachloroethene 59.0 ug/L 10/12/19 07:42 127-18-41.0 1
Toluene ND ug/L 10/12/19 07:42 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/12/19 07:42 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/12/19 07:42 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/12/19 07:42 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/12/19 07:42 79-00-51.0 1
Trichloroethene 3.8 ug/L 10/12/19 07:42 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/12/19 07:42 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/12/19 07:42 96-18-41.0 1
Vinyl acetate ND ug/L 10/12/19 07:42 108-05-42.0 1
Vinyl chloride ND ug/L 10/12/19 07:42 75-01-41.0 1
Xylene (Total)ND ug/L 10/12/19 07:42 1330-20-71.0 1
m&p-Xylene ND ug/L 10/12/19 07:42 179601-23-12.0 1
o-Xylene ND ug/L 10/12/19 07:42 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)105 %10/12/19 07:42 460-00-470-130 1
1,2-Dichloroethane-d4 (S)106 %10/12/19 07:42 17060-07-070-130 1
Toluene-d8 (S)101 %10/12/19 07:42 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/14/2019 04:04 PM
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Page 6 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92449235
TICAR A19-101B 10/10
Sample:SW-1 Lab ID:92449235003 Collected:10/10/19 13:35 Received:10/10/19 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 10/12/19 05:19 67-64-125.0 1
Benzene ND ug/L 10/12/19 05:19 71-43-21.0 1
Bromobenzene ND ug/L 10/12/19 05:19 108-86-11.0 1
Bromochloromethane ND ug/L 10/12/19 05:19 74-97-5 v21.0 1
Bromodichloromethane ND ug/L 10/12/19 05:19 75-27-41.0 1
Bromoform ND ug/L 10/12/19 05:19 75-25-21.0 1
Bromomethane ND ug/L 10/12/19 05:19 74-83-9 v22.0 1
2-Butanone (MEK)ND ug/L 10/12/19 05:19 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/12/19 05:19 56-23-51.0 1
Chlorobenzene ND ug/L 10/12/19 05:19 108-90-71.0 1
Chloroethane ND ug/L 10/12/19 05:19 75-00-3 v21.0 1
Chloroform ND ug/L 10/12/19 05:19 67-66-35.0 1
Chloromethane ND ug/L 10/12/19 05:19 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/12/19 05:19 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/12/19 05:19 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/19 05:19 96-12-85.0 1
Dibromochloromethane ND ug/L 10/12/19 05:19 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/12/19 05:19 106-93-41.0 1
Dibromomethane ND ug/L 10/12/19 05:19 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/12/19 05:19 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/12/19 05:19 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/12/19 05:19 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/12/19 05:19 75-71-81.0 1
1,1-Dichloroethane ND ug/L 10/12/19 05:19 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/12/19 05:19 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/12/19 05:19 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/12/19 05:19 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/12/19 05:19 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/12/19 05:19 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/12/19 05:19 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/12/19 05:19 594-20-7 v21.0 1
1,1-Dichloropropene ND ug/L 10/12/19 05:19 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/12/19 05:19 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/12/19 05:19 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/12/19 05:19 108-20-31.0 1
Ethylbenzene ND ug/L 10/12/19 05:19 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/12/19 05:19 87-68-31.0 1
2-Hexanone ND ug/L 10/12/19 05:19 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/12/19 05:19 99-87-61.0 1
Methylene Chloride ND ug/L 10/12/19 05:19 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/19 05:19 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/12/19 05:19 1634-04-41.0 1
Naphthalene ND ug/L 10/12/19 05:19 91-20-31.0 1
Styrene ND ug/L 10/12/19 05:19 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/19 05:19 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/19 05:19 79-34-51.0 1
Tetrachloroethene ND ug/L 10/12/19 05:19 127-18-41.0 1
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/14/2019 04:04 PM
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Asheville, NC 28804
[phone]
Page 7 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92449235
TICAR A19-101B 10/10
Sample:SW-1 Lab ID:92449235003 Collected:10/10/19 13:35 Received:10/10/19 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D8260D MSV Low Level
Toluene ND ug/L 10/12/19 05:19 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/12/19 05:19 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/12/19 05:19 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/12/19 05:19 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/12/19 05:19 79-00-51.0 1
Trichloroethene ND ug/L 10/12/19 05:19 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/12/19 05:19 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/12/19 05:19 96-18-41.0 1
Vinyl acetate ND ug/L 10/12/19 05:19 108-05-42.0 1
Vinyl chloride ND ug/L 10/12/19 05:19 75-01-41.0 1
Xylene (Total)ND ug/L 10/12/19 05:19 1330-20-71.0 1
m&p-Xylene ND ug/L 10/12/19 05:19 179601-23-12.0 1
o-Xylene ND ug/L 10/12/19 05:19 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)98 %10/12/19 05:19 460-00-470-130 1
1,2-Dichloroethane-d4 (S)114 %10/12/19 05:19 17060-07-070-130 1
Toluene-d8 (S)101 %10/12/19 05:19 2037-26-570-130 1
Sample:SW-2 Lab ID:92449235004 Collected:10/10/19 13:45 Received:10/10/19 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 10/12/19 05:37 67-64-125.0 1
Benzene ND ug/L 10/12/19 05:37 71-43-21.0 1
Bromobenzene ND ug/L 10/12/19 05:37 108-86-11.0 1
Bromochloromethane ND ug/L 10/12/19 05:37 74-97-5 v21.0 1
Bromodichloromethane ND ug/L 10/12/19 05:37 75-27-41.0 1
Bromoform ND ug/L 10/12/19 05:37 75-25-21.0 1
Bromomethane ND ug/L 10/12/19 05:37 74-83-9 v22.0 1
2-Butanone (MEK)ND ug/L 10/12/19 05:37 78-93-35.0 1
Carbon tetrachloride ND ug/L 10/12/19 05:37 56-23-51.0 1
Chlorobenzene ND ug/L 10/12/19 05:37 108-90-71.0 1
Chloroethane ND ug/L 10/12/19 05:37 75-00-3 v21.0 1
Chloroform ND ug/L 10/12/19 05:37 67-66-35.0 1
Chloromethane ND ug/L 10/12/19 05:37 74-87-31.0 1
2-Chlorotoluene ND ug/L 10/12/19 05:37 95-49-81.0 1
4-Chlorotoluene ND ug/L 10/12/19 05:37 106-43-41.0 1
1,2-Dibromo-3-chloropropane ND ug/L 10/12/19 05:37 96-12-85.0 1
Dibromochloromethane ND ug/L 10/12/19 05:37 124-48-11.0 1
1,2-Dibromoethane (EDB)ND ug/L 10/12/19 05:37 106-93-41.0 1
Dibromomethane ND ug/L 10/12/19 05:37 74-95-31.0 1
1,2-Dichlorobenzene ND ug/L 10/12/19 05:37 95-50-11.0 1
1,3-Dichlorobenzene ND ug/L 10/12/19 05:37 541-73-11.0 1
1,4-Dichlorobenzene ND ug/L 10/12/19 05:37 106-46-71.0 1
Dichlorodifluoromethane ND ug/L 10/12/19 05:37 75-71-81.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/14/2019 04:04 PM
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2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 8 of 20
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92449235
TICAR A19-101B 10/10
Sample:SW-2 Lab ID:92449235004 Collected:10/10/19 13:45 Received:10/10/19 15:45 Matrix:Water
Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit
Analytical Method: EPA 8260D8260D MSV Low Level
1,1-Dichloroethane ND ug/L 10/12/19 05:37 75-34-31.0 1
1,2-Dichloroethane ND ug/L 10/12/19 05:37 107-06-21.0 1
1,1-Dichloroethene ND ug/L 10/12/19 05:37 75-35-41.0 1
cis-1,2-Dichloroethene ND ug/L 10/12/19 05:37 156-59-21.0 1
trans-1,2-Dichloroethene ND ug/L 10/12/19 05:37 156-60-51.0 1
1,2-Dichloropropane ND ug/L 10/12/19 05:37 78-87-51.0 1
1,3-Dichloropropane ND ug/L 10/12/19 05:37 142-28-91.0 1
2,2-Dichloropropane ND ug/L 10/12/19 05:37 594-20-7 v21.0 1
1,1-Dichloropropene ND ug/L 10/12/19 05:37 563-58-61.0 1
cis-1,3-Dichloropropene ND ug/L 10/12/19 05:37 10061-01-51.0 1
trans-1,3-Dichloropropene ND ug/L 10/12/19 05:37 10061-02-61.0 1
Diisopropyl ether ND ug/L 10/12/19 05:37 108-20-31.0 1
Ethylbenzene ND ug/L 10/12/19 05:37 100-41-41.0 1
Hexachloro-1,3-butadiene ND ug/L 10/12/19 05:37 87-68-31.0 1
2-Hexanone ND ug/L 10/12/19 05:37 591-78-65.0 1
p-Isopropyltoluene ND ug/L 10/12/19 05:37 99-87-61.0 1
Methylene Chloride ND ug/L 10/12/19 05:37 75-09-25.0 1
4-Methyl-2-pentanone (MIBK)ND ug/L 10/12/19 05:37 108-10-15.0 1
Methyl-tert-butyl ether ND ug/L 10/12/19 05:37 1634-04-41.0 1
Naphthalene ND ug/L 10/12/19 05:37 91-20-31.0 1
Styrene ND ug/L 10/12/19 05:37 100-42-51.0 1
1,1,1,2-Tetrachloroethane ND ug/L 10/12/19 05:37 630-20-61.0 1
1,1,2,2-Tetrachloroethane ND ug/L 10/12/19 05:37 79-34-51.0 1
Tetrachloroethene ND ug/L 10/12/19 05:37 127-18-41.0 1
Toluene ND ug/L 10/12/19 05:37 108-88-31.0 1
1,2,3-Trichlorobenzene ND ug/L 10/12/19 05:37 87-61-61.0 1
1,2,4-Trichlorobenzene ND ug/L 10/12/19 05:37 120-82-11.0 1
1,1,1-Trichloroethane ND ug/L 10/12/19 05:37 71-55-61.0 1
1,1,2-Trichloroethane ND ug/L 10/12/19 05:37 79-00-51.0 1
Trichloroethene ND ug/L 10/12/19 05:37 79-01-61.0 1
Trichlorofluoromethane ND ug/L 10/12/19 05:37 75-69-41.0 1
1,2,3-Trichloropropane ND ug/L 10/12/19 05:37 96-18-41.0 1
Vinyl acetate ND ug/L 10/12/19 05:37 108-05-42.0 1
Vinyl chloride ND ug/L 10/12/19 05:37 75-01-41.0 1
Xylene (Total)ND ug/L 10/12/19 05:37 1330-20-71.0 1
m&p-Xylene ND ug/L 10/12/19 05:37 179601-23-12.0 1
o-Xylene ND ug/L 10/12/19 05:37 95-47-61.0 1
Surrogates
4-Bromofluorobenzene (S)99 %10/12/19 05:37 460-00-470-130 1
1,2-Dichloroethane-d4 (S)116 %10/12/19 05:37 17060-07-070-130 1
Toluene-d8 (S)99 %10/12/19 05:37 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 10/14/2019 04:04 PM
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Page 9 of 20
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92449235
TICAR A19-101B 10/10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
503152
EPA 8260D
EPA 8260D
8260D MSV Low Level
Associated Lab Samples:92449235001, 92449235002, 92449235003, 92449235004
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2704656
Associated Lab Samples:92449235001, 92449235002, 92449235003, 92449235004
Matrix:Water
Analyzed
1,1,1,2-Tetrachloroethane ug/L ND 1.0 10/12/19 04:07
1,1,1-Trichloroethane ug/L ND 1.0 10/12/19 04:07
1,1,2,2-Tetrachloroethane ug/L ND 1.0 10/12/19 04:07
1,1,2-Trichloroethane ug/L ND 1.0 10/12/19 04:07
1,1-Dichloroethane ug/L ND 1.0 10/12/19 04:07
1,1-Dichloroethene ug/L ND 1.0 10/12/19 04:07
1,1-Dichloropropene ug/L ND 1.0 10/12/19 04:07
1,2,3-Trichlorobenzene ug/L ND 1.0 10/12/19 04:07
1,2,3-Trichloropropane ug/L ND 1.0 10/12/19 04:07
1,2,4-Trichlorobenzene ug/L ND 1.0 10/12/19 04:07
1,2-Dibromo-3-chloropropane ug/L ND 5.0 10/12/19 04:07
1,2-Dibromoethane (EDB)ug/L ND 1.0 10/12/19 04:07
1,2-Dichlorobenzene ug/L ND 1.0 10/12/19 04:07
1,2-Dichloroethane ug/L ND 1.0 10/12/19 04:07
1,2-Dichloropropane ug/L ND 1.0 10/12/19 04:07
1,3-Dichlorobenzene ug/L ND 1.0 10/12/19 04:07
1,3-Dichloropropane ug/L ND 1.0 10/12/19 04:07
1,4-Dichlorobenzene ug/L ND 1.0 10/12/19 04:07
2,2-Dichloropropane ug/L ND 1.0 v210/12/19 04:07
2-Butanone (MEK)ug/L ND 5.0 10/12/19 04:07
2-Chlorotoluene ug/L ND 1.0 10/12/19 04:07
2-Hexanone ug/L ND 5.0 10/12/19 04:07
4-Chlorotoluene ug/L ND 1.0 10/12/19 04:07
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 10/12/19 04:07
Acetone ug/L ND 25.0 10/12/19 04:07
Benzene ug/L ND 1.0 10/12/19 04:07
Bromobenzene ug/L ND 1.0 10/12/19 04:07
Bromochloromethane ug/L ND 1.0 v210/12/19 04:07
Bromodichloromethane ug/L ND 1.0 10/12/19 04:07
Bromoform ug/L ND 1.0 10/12/19 04:07
Bromomethane ug/L ND 2.0 v210/12/19 04:07
Carbon tetrachloride ug/L ND 1.0 10/12/19 04:07
Chlorobenzene ug/L ND 1.0 10/12/19 04:07
Chloroethane ug/L ND 1.0 v210/12/19 04:07
Chloroform ug/L ND 5.0 10/12/19 04:07
Chloromethane ug/L ND 1.0 10/12/19 04:07
cis-1,2-Dichloroethene ug/L ND 1.0 10/12/19 04:07
cis-1,3-Dichloropropene ug/L ND 1.0 10/12/19 04:07
Dibromochloromethane ug/L ND 1.0 10/12/19 04:07
Dibromomethane ug/L ND 1.0 10/12/19 04:07
Dichlorodifluoromethane ug/L ND 1.0 10/12/19 04:07
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/14/2019 04:04 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92449235
TICAR A19-101B 10/10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK:2704656
Associated Lab Samples:92449235001, 92449235002, 92449235003, 92449235004
Matrix:Water
Analyzed
Diisopropyl ether ug/L ND 1.0 10/12/19 04:07
Ethylbenzene ug/L ND 1.0 10/12/19 04:07
Hexachloro-1,3-butadiene ug/L ND 1.0 10/12/19 04:07
m&p-Xylene ug/L ND 2.0 10/12/19 04:07
Methyl-tert-butyl ether ug/L ND 1.0 10/12/19 04:07
Methylene Chloride ug/L ND 5.0 10/12/19 04:07
Naphthalene ug/L ND 1.0 10/12/19 04:07
o-Xylene ug/L ND 1.0 10/12/19 04:07
p-Isopropyltoluene ug/L ND 1.0 10/12/19 04:07
Styrene ug/L ND 1.0 10/12/19 04:07
Tetrachloroethene ug/L ND 1.0 10/12/19 04:07
Toluene ug/L ND 1.0 10/12/19 04:07
trans-1,2-Dichloroethene ug/L ND 1.0 10/12/19 04:07
trans-1,3-Dichloropropene ug/L ND 1.0 10/12/19 04:07
Trichloroethene ug/L ND 1.0 10/12/19 04:07
Trichlorofluoromethane ug/L ND 1.0 10/12/19 04:07
Vinyl acetate ug/L ND 2.0 10/12/19 04:07
Vinyl chloride ug/L ND 1.0 10/12/19 04:07
Xylene (Total)ug/L ND 1.0 10/12/19 04:07
1,2-Dichloroethane-d4 (S)%112 70-130 10/12/19 04:07
4-Bromofluorobenzene (S)%94 70-130 10/12/19 04:07
Toluene-d8 (S)%100 70-130 10/12/19 04:07
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2704657LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 54.250 108 70-130
1,1,1-Trichloroethane ug/L 43.850 88 70-130
1,1,2,2-Tetrachloroethane ug/L 51.750 103 70-130
1,1,2-Trichloroethane ug/L 49.550 99 70-130
1,1-Dichloroethane ug/L 40.750 81 70-130
1,1-Dichloroethene ug/L 48.650 97 70-130
1,1-Dichloropropene ug/L 43.650 87 70-130
1,2,3-Trichlorobenzene ug/L 55.550 111 70-130
1,2,3-Trichloropropane ug/L 53.550 107 70-130
1,2,4-Trichlorobenzene ug/L 53.950 108 70-130
1,2-Dibromo-3-chloropropane ug/L 54.550 109 70-130
1,2-Dibromoethane (EDB)ug/L 52.650 105 70-130
1,2-Dichlorobenzene ug/L 53.150 106 70-130
1,2-Dichloroethane ug/L 52.050 104 70-130
1,2-Dichloropropane ug/L 47.250 94 70-130
1,3-Dichlorobenzene ug/L 52.350 105 70-130
1,3-Dichloropropane ug/L 52.950 106 70-131
1,4-Dichlorobenzene ug/L 51.550 103 70-130
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92449235
TICAR A19-101B 10/10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2704657LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 36.2 v3507269-130
2-Butanone (MEK)ug/L 103100 103 64-135
2-Chlorotoluene ug/L 51.850 104 70-130
2-Hexanone ug/L 120100 120 66-135
4-Chlorotoluene ug/L 52.250 104 70-130
4-Methyl-2-pentanone (MIBK)ug/L 112100 112 70-130
Acetone ug/L 104100 104 61-157
Benzene ug/L 47.050 94 70-130
Bromobenzene ug/L 53.850 108 70-130
Bromochloromethane ug/L 38.1 v3507670-130
Bromodichloromethane ug/L 48.750 97 70-130
Bromoform ug/L 53.950 108 70-130
Bromomethane ug/L 28.1 v3505638-130
Carbon tetrachloride ug/L 47.850 96 70-130
Chlorobenzene ug/L 49.350 99 70-130
Chloroethane ug/L 36.6 v3507337-142
Chloroform ug/L 43.350 87 70-130
Chloromethane ug/L 49.050 98 48-130
cis-1,2-Dichloroethene ug/L 41.250 82 70-130
cis-1,3-Dichloropropene ug/L 52.250 104 70-130
Dibromochloromethane ug/L 52.750 105 70-130
Dibromomethane ug/L 45.650 91 70-130
Dichlorodifluoromethane ug/L 43.750 87 53-134
Diisopropyl ether ug/L 52.650 105 70-135
Ethylbenzene ug/L 50.750 101 70-130
Hexachloro-1,3-butadiene ug/L 50.750 101 68-132
m&p-Xylene ug/L 103100 103 70-130
Methyl-tert-butyl ether ug/L 46.350 93 70-130
Methylene Chloride ug/L 45.150 90 67-132
Naphthalene ug/L 56.750 113 70-130
o-Xylene ug/L 52.050 104 70-131
p-Isopropyltoluene ug/L 53.050 106 70-130
Styrene ug/L 52.050 104 70-130
Tetrachloroethene ug/L 51.550 103 69-130
Toluene ug/L 46.850 94 70-130
trans-1,2-Dichloroethene ug/L 40.850 82 70-130
trans-1,3-Dichloropropene ug/L 52.050 104 70-130
Trichloroethene ug/L 46.550 93 70-130
Trichlorofluoromethane ug/L 41.750 83 63-130
Vinyl acetate ug/L 120100 120 55-143
Vinyl chloride ug/L 41.350 83 70-131
Xylene (Total)ug/L 155150 103 70-130
1,2-Dichloroethane-d4 (S)%94 70-130
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%98 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 10/14/2019 04:04 PM
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92449235
TICAR A19-101B 10/10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2704659MATRIX SPIKE SAMPLE:
MSSpike
Result
92448479001
1,1,1,2-Tetrachloroethane ug/L 20.920 104 73-134ND
1,1,1-Trichloroethane ug/L 19.920 99 82-143ND
1,1,2,2-Tetrachloroethane ug/L 23.820 119 70-136ND
1,1,2-Trichloroethane ug/L 22.220 111 70-135ND
1,1-Dichloroethane ug/L 19.620 98 70-139ND
1,1-Dichloroethene ug/L 23.820 119 70-154ND
1,1-Dichloropropene ug/L 19.720 98 70-149ND
1,2,3-Trichlorobenzene ug/L 22.220 111 70-135ND
1,2,3-Trichloropropane ug/L 24.420 122 71-137ND
1,2,4-Trichlorobenzene ug/L 22.220 111 73-140ND
1,2-Dibromo-3-chloropropane ug/L 22.820 114 65-134ND
1,2-Dibromoethane (EDB)ug/L 20.920 105 70-137ND
1,2-Dichlorobenzene ug/L 22.020 110 70-133ND
1,2-Dichloroethane ug/L 20.920 104 70-137ND
1,2-Dichloropropane ug/L 20.120 100 70-140ND
1,3-Dichlorobenzene ug/L 22.220 111 70-135ND
1,3-Dichloropropane ug/L 20.420 102 70-143ND
1,4-Dichlorobenzene ug/L 21.920 110 70-133ND
2,2-Dichloropropane ug/L 16.6 v3208361-148ND
2-Butanone (MEK)ug/L 44.440 111 60-139ND
2-Chlorotoluene ug/L 20.820 104 70-144ND
2-Hexanone ug/L 47.7 v14011965-138ND
4-Chlorotoluene ug/L 21.220 106 70-137ND
4-Methyl-2-pentanone (MIBK)ug/L 50.440 126 65-135ND
Acetone ug/L 55.540 139 60-148ND
Benzene ug/L 20.820 104 70-151ND
Bromobenzene ug/L 20.820 104 70-136ND
Bromochloromethane ug/L 22.0 v32011070-141ND
Bromodichloromethane ug/L 21.520 108 70-138ND
Bromoform ug/L 24.220 121 63-130ND
Bromomethane ug/L 16.9 v3208515-152ND
Carbon tetrachloride ug/L 21.020 105 70-143ND
Chlorobenzene ug/L 21.420 107 70-138ND
Chloroethane ug/L 24.7 v32012452-163ND
Chloroform ug/L 20.620 103 70-139ND
Chloromethane ug/L 23.320 117 41-139ND
cis-1,2-Dichloroethene ug/L 19.620 98 70-141ND
cis-1,3-Dichloropropene ug/L 21.820 109 70-137ND
Dibromochloromethane ug/L 20.420 102 70-134ND
Dibromomethane ug/L 21.120 105 70-138ND
Dichlorodifluoromethane ug/L 28.020 140 47-155ND
Diisopropyl ether ug/L 22.720 114 63-144ND
Ethylbenzene ug/L 22.920 114 66-153ND
Hexachloro-1,3-butadiene ug/L 24.020 120 65-149ND
m&p-Xylene ug/L 47.740 119 69-152ND
Methyl-tert-butyl ether ug/L 19.120 96 54-156ND
Methylene Chloride ug/L 25.820 129 42-159ND
REPORT OF LABORATORY ANALYSIS
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Asheville, NC 28804
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92449235
TICAR A19-101B 10/10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2704659MATRIX SPIKE SAMPLE:
MSSpike
Result
92448479001
Naphthalene ug/L 21.720 109 61-148ND
o-Xylene ug/L 24.120 121 70-148ND
p-Isopropyltoluene ug/L 23.220 116 70-146ND
Styrene ug/L 23.720 119 70-135ND
Tetrachloroethene ug/L 20.820 104 59-143ND
Toluene ug/L 22.320 112 59-148ND
trans-1,2-Dichloroethene ug/L 19.620 98 70-146ND
trans-1,3-Dichloropropene ug/L 22.720 114 70-135ND
Trichloroethene ug/L 21.120 106 70-147ND
Trichlorofluoromethane ug/L 23.020 115 70-148ND
Vinyl acetate ug/L 45.840 115 49-151ND
Vinyl chloride ug/L 24.120 120 70-156ND
Xylene (Total)ug/L 71.860 120 63-158ND
1,2-Dichloroethane-d4 (S)%98 70-130
4-Bromofluorobenzene (S)%113 70-130
Toluene-d8 (S)%107 70-130
Parameter Units
Dup
Result QualifiersRPDResult
92448908002
2704658SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L NDND
1,1,1-Trichloroethane ug/L NDND
1,1,2,2-Tetrachloroethane ug/L NDND
1,1,2-Trichloroethane ug/L NDND
1,1-Dichloroethane ug/L NDND
1,1-Dichloroethene ug/L NDND
1,1-Dichloropropene ug/L NDND
1,2,3-Trichlorobenzene ug/L NDND
1,2,3-Trichloropropane ug/L NDND
1,2,4-Trichlorobenzene ug/L NDND
1,2-Dibromo-3-chloropropane ug/L NDND
1,2-Dibromoethane (EDB)ug/L NDND
1,2-Dichlorobenzene ug/L NDND
1,2-Dichloroethane ug/L NDND
1,2-Dichloropropane ug/L NDND
1,3-Dichlorobenzene ug/L NDND
1,3-Dichloropropane ug/L NDND
1,4-Dichlorobenzene ug/L NDND
2,2-Dichloropropane ug/L ND v2ND
2-Butanone (MEK)ug/L NDND
2-Chlorotoluene ug/L NDND
2-Hexanone ug/L ND v1ND
4-Chlorotoluene ug/L NDND
4-Methyl-2-pentanone (MIBK)ug/L NDND
Acetone ug/L NDND
REPORT OF LABORATORY ANALYSIS
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Asheville, NC 28804
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92449235
TICAR A19-101B 10/10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result QualifiersRPDResult
92448908002
2704658SAMPLE DUPLICATE:
Benzene ug/L NDND
Bromobenzene ug/L NDND
Bromochloromethane ug/L ND v2ND
Bromodichloromethane ug/L NDND
Bromoform ug/L NDND
Bromomethane ug/L ND v2ND
Carbon tetrachloride ug/L NDND
Chlorobenzene ug/L NDND
Chloroethane ug/L ND v2ND
Chloroform ug/L NDND
Chloromethane ug/L NDND
cis-1,2-Dichloroethene ug/L NDND
cis-1,3-Dichloropropene ug/L NDND
Dibromochloromethane ug/L NDND
Dibromomethane ug/L NDND
Dichlorodifluoromethane ug/L NDND
Diisopropyl ether ug/L NDND
Ethylbenzene ug/L NDND
Hexachloro-1,3-butadiene ug/L NDND
m&p-Xylene ug/L NDND
Methyl-tert-butyl ether ug/L NDND
Methylene Chloride ug/L NDND
Naphthalene ug/L NDND
o-Xylene ug/L NDND
p-Isopropyltoluene ug/L NDND
Styrene ug/L NDND
Tetrachloroethene ug/L NDND
Toluene ug/L NDND
trans-1,2-Dichloroethene ug/L NDND
trans-1,3-Dichloropropene ug/L NDND
Trichloroethene ug/L NDND
Trichlorofluoromethane ug/L NDND
Vinyl acetate ug/L NDND
Vinyl chloride ug/L NDND
Xylene (Total)ug/L NDND
1,2-Dichloroethane-d4 (S)%111116
4-Bromofluorobenzene (S)%109100
Toluene-d8 (S)%10199
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92449235
TICAR A19-101B 10/10
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.v3
REPORT OF LABORATORY ANALYSIS
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Asheville, NC 28804
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Page 16 of 20
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92449235
TICAR A19-101B 10/10
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92449235001 503152GW-3 EPA 8260D
92449235002 503152OS-03 EPA 8260D
92449235003 503152SW-1 EPA 8260D
92449235004 503152SW-2 EPA 8260D
REPORT OF LABORATORY ANALYSIS
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Page 17 of 20
Page 18 of 20
Page 19 of 20
Page 20 of 20
APPENDIX C
Tier 2 Risk Evaluation Data Sheet

Risk for Individual Pathways Output Form 1A
Version Date: May 2019
Basis: May 2019 EPA RSL Table
Site ID: Ticar Chemical Site
Exposure Unit ID: Groundwater to Indoor Air - Vicinity of Monitoring Well GW-3
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Soil NC NC NC
Groundwater Use*NC NC NC
Soil NC NC NC
Groundwater Use*NC NC NC
Construction Worker Soil NC NC NC
Soil NC NC NC
Surface Water*NC NC NC
Receptor Pathway Carcinogenic
Risk Hazard Index Risk exceeded?
Groundwater to Indoor Air NC NC NC
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Groundwater to Indoor Air 1.4E-06 4.0E-01 NO
Soil Gas to Indoor Air NC NC NC
Indoor Air NC NC NC
Pathway Source
Source Soil NC
Source Groundwater NC
Source Soil NC
Source Groundwater NC
3. NM = Not Modeled
4. NC = Pathway not complete
2. * = If concentrations in groundwater exceed the NC 2L Standards or IMAC, or concentrations in surface water exceed the
NC 2B Standards, appropriate remediation and/or institutional control measures will be necessary to be eligible for a risk-based
closure.
Surface Water Exceedence of 2B at Receptor?
Exceedence of 2B at Receptor?
VAPOR INTRUSION CALCULATORS
Resident
Non-Residential Worker
CONTAMINANT MIGRATION CALCULATORS
Target Receptor Concentrations Exceeded?
Groundwater Exceedence of 2L at Receptor?
Exceedence of 2L at Receptor?
1.If lead concentrations were entered in the exposure point concentration tables, see the individual calculator sheets for lead
concentrations in comparison to screening levels. Note that lead is not included in cumulative risk calculations.
Notes:
DIRECT CONTACT SOIL AND WATER CALCULATORS
Resident
Non-Residential Worker
Recreator/Trespasser
North Carolina DEQ Risk Calculator