22081_FormerPEValve_Brownfields Assessment Report_11.06.2019

REPORT OF ENVIRONMENTAL BROWNFIELD ASSESSMENT
FORMER PE VALVE MANUFACTURING
1140 SWEETEN CREEK ROAD
ASHEVILLE, BUNCOMBE COUNTY, NORTH CAROLINA
ECS PROJECT 49:7572-B
NCDEQ BROWNFIELDS ID NO. 22018-18-11

PREPARED FOR:
MR. PETER HALL

NOVEMBER 6, 2019
Report of Environmental Assessment
Former PE Valve Manufacturing
ECS Project No. 49:7572-B
November 6, 2019

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TABLE OF CONTENTS

1.0 PROJECT INFORMATION ...........................................................................................................1
2.0 SCOPE OF SERVICES ..................................................................................................................2
3.0 RESULTS ..................................................................................................................................4
4.0 CONCLUSIONS .........................................................................................................................5
5.0 RECOMMENDATIONS ...............................................................................................................5
6.0 QUALIFICATIONS OF REPORT ....................................................................................................5

FIGURES

Figure 1 Site Topographic Map
Figure 2 Site Location Map
Figure 3 Soil Gas Sample Location Map

TABLES

Table 1 Coordinate Table of Soil Gas Sampling Points
Table 2 Summary of Soil Gas Analytical Results

APPENDICES

Appendix A Photograph Log
Appendix B Laboratory Analytical Data and Chain of Custody Records
Appendix C Brownfields Survey Form

Report of Environmental Assessment
Former PE Valve Manufacturing
ECS Project No. 49:7572-B
November 6, 2019

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1.0 PROJECT INFORMATION

The former PE Valve property is located at 1140 Sweeten Creek Road in Ashville, Buncombe County,
North Carolina (Figure 1). The property is approximately 1.63 acres in size and is currently utilized as a
vacant lot. A Limited Phase II Environmental Site Assessment (Phase II ESA) dated March 8, 2010 and
completed by Bunnell-Lammons Engineering, Inc. (BLE) indicated that BLE also previously completed a
Phase I Environmental Site Assessment (Phase I ESA) dated March 4, 2010 for the subject property. The
Phase I ESA indicated that a 30,302 square foot industrial manufacturing building was developed on the
subject property which was previously used for textile manufacturing. In 1968, the building was used as
a valve manufacturing facility. During the completion of the Phase I ESA, the building was vacant. The
Phase I ESA identified the following recognized environmental conditions (RECs) with respect to the
subject site:

 Rusted 55-gallon drums located on the southern side of the building, of which the historic
contents are unknown;
 An above ground storage tank (AST) located on the southern side of the building;
 Staining along the northern wall of the building;
 A loading dock with floor drains;
 Two ASTs located on the interior of the building;
 Multiple 55-gallon drums and 5-gallon buckets of waste oil, waste coolant, and unidentified
liquids inside the building;
 Heavy staining on the floor of the building; and
 A network of floor drains located inside the building.

As part of the assessment activities conducted by BLE for the Limited Phase II ESA, four borings were
advanced for the purposes of collecting groundwater samples. The borings were located topographically
downgradient and west of the building (BL-1), downgradient and near the northwest corner of the
subject property (BL-2), downgradient of an AST and near the southwest corner of the building (BL-3),
and adjacent to the loading dock (BL-4). The borings were advanced with a Geoprobe® drill rig to refusal,
which was approximately 25 feet below the ground surface (bgs). Groundwater was identified at
approximately 20 feet bgs. Four hand auger borings were advanced within the building for the purposes
of collecting soil samples. The borings were located adjacent to 55-gallon drums, ASTs, and 5-gallon
buckets (HAB-1), inside the machining room where heavy staining was observed (HAB-2), inside the
paint room (HAB-3), and adjacent to a floor drain in the southern portion of the building (HAB-4).

Trichloroethene (TCE) was identified at concentrations above the North Carolina 2L Groundwater
Quality Standard (NC2LGWQS) in groundwater samples BL-2, BL-3, and BL-4. Chromium was identified at
concentrations above the Inactive Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goal
(PSRG) in soil samples HAB-1, HAB-2, and HAB-2. Selenium was identified at a concentration above the
IHSB PSRG in soil sample HAB-4.

ECS conducted a Soil and Groundwater Assessment at the subject property similar in scope to the Phase
II ESA conducted by BLE (ECS Project Number 49-7572, dated October 11, 2018). However, during the
assessment conducted by ECS, the building was no longer present and the property was undeveloped.
ECS’ Soil and Groundwater Assessment included six soil borings for the collection of soil samples. Arsenic
Report of Environmental Assessment
Former PE Valve Manufacturing
ECS Project No. 49:7572-B
November 6, 2019

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and hexavalent chromium were identified at concentrations exceeding the IHSB Health-Based PSRGs in
each of the soil samples. Three of the soil borings were advanced for the collection of groundwater
samples. A fourth groundwater sample was collected from the northwestern corner of the subject
property. The groundwater sample collected from the southern portion of the subject property
identified TCE at a concentration exceeding the NC2LGWQS and the Vapor Intrusion Screening Levels
(VISLs). ECS recommended a soil gas assessment be conducted to evaluate vapor intrusion concerns and
concluded that the property appears to be a candidate for eligibility into the North Carolina Brownfields
Program (NCBP).

After ECS conducted the assessment, the property owner, Mr. Peter Hall, applied for eligibility into the
NCBP. On May 2, 2019, Mr. Hall obtained a Letter of Eligibility from the NCBP. The NCBP also requested
additional assessment. According to a Request for Additional Assessment (RAA) letter dated June 14,
2019, the NCBP requested soil gas sampling, a historical file review, and the completion of a Brownfields
Receptor Survey.

This report summarizes the findings from the assessment activities which were performed as outlined in
a work plan previously generated by ECS and approved by the NCBP.

2.0 SCOPE OF SERVICES

The environmental assessment consisted of the collection of soil gas samples. Drilling activities were
conducted using a direct push type Geoprobe® drill rig. The drilling subcontractor used for this project
was JG Drilling of Easley, South Carolina. Soil gas monitoring points were installed and samples collected
on September 5, 2019. A photographic log documenting the field activities is provided in Appendix A.

2.1 Public and Private Utility Locate

Prior to implementing the field activities, ECS contacted North Carolina public utility locate service (811)
to locate/mark public utilities at the site. In addition, ECS contracted with Blood Hound, LLC to
locate/mark private underground utilities at the site. Required separation distances between subsurface
activities and marked utilities (typically 30-inches) were maintained during the field activities.

2.2 Soil Gas Sample Point Installation Activities

On September 5, 2019, ECS installed five (5) temporary soil gas sample points and were identified as SG-1
through SG-5. The locations of the sample points are shown in Figure 3. Each soil gas sample was
constructed by drilling a 1.5-inch diameter boring using a Geoprobe® drill rig to a depth of
approximately 10 feet bgs.

A probe consisting of vapor implant and Nylafow or teflon® tubing was placed into each boring. The
space around and approximately 6 inches above the vapor implant was backfilled with sand. The space
above the sand was sealed with hydrated bentonite. The vapor probe and tubing was purged by
removing three volumes of the probe and associated tubing prior to sampling after allowing the
bentonite to hydrate for at least 30 minutes.

Report of Environmental Assessment
Former PE Valve Manufacturing
ECS Project No. 49:7572-B
November 6, 2019

3
Before collecting the soil gas sample, helium gas was used to serve as a quality assurance/quality control
measure to verify the integrity of the probe seal. A plastic container was placed and sealed over the
sampling point and purged with laboratory grade helium. During the purging stage, a steady supply of
helium was released from the tank via a hose placed through the wall of the plastic container. A helium
detector was connected to the sampling port and the air stream being purged was measured for helium
using the detector to evaluate the integrity of the seal. If the concentration of measured helium
concentration was less than 10 percent of the helium concentration inside the shroud, the seal on the
soil gas probe was considered to be tight and not leaking. If the test results are not acceptable, ECS took
steps to achieve a better seal and repeat the test until the results are acceptable. A shut-in test was also
conducted to check the sampling set-up for leaks prior to initiating sampling.

2.3 Soil Gas Sample Collection

On September 5, 2019 ECS collected soil gas samples from each of the five (5) sample points (SG-1
through SG-5 and a duplicate sample [designated SG-6] was collected from sampling point SG-5).

After leak testing and prior to sampling, the sample train was purged of approximately 3 tubing
volumes. The tubing was then connected to a pre-evacuated and pre-cleaned Summa canister for
sampling. ECS utilized 1-liter Summa canisters which were batch certified by laboratory. Soil gas was
collected from the sampling points at a rate of 200 milliliters per minute. The Summa canisters were
submitted to Con-Test Analytical Laboratory (Con-Test) for analyses for volatile organic compounds
(VOCs) by EPA Method TO-15. North Carolina does not certify laboratories for analyses of air/soil gas
samples. ECS requested that the laboratory analyze the samples for the most current and applicable
standards from the National Environmental Laboratory Accreditation Conference (NELAC) Program. The
duplicate soil gas sample (SG-6) was also submitted for laboratory analysis by EPA Method TO-15.

ECS maintained chain-of-custody (COC) procedures throughout the sample collection and transportation
process. Copies of the COCs are included in Appendix B.

2.4 Sample Point Coordinates

Using a handheld global positioning system (GPS) device, ECS recorded the coordinate locations of each
sample collection points. Table 1 summarizes the recorded coordinate data.

2.5 Brownfields Receptor Survey

ECS performed a Brownfields receptor survey. This survey was performed by researching various data
sources through the internet and a windshield survey of the area. The Brownfields receptor survey was
completed using the form provided by the NCBP. This form and associated attachments are included as
Appendix C.

Report of Environmental Assessment
Former PE Valve Manufacturing
ECS Project No. 49:7572-B
November 6, 2019

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3.0 RESULTS

3.1 Soil Gas Sample Results

Laboratory analysis indicates that VOCs were detected in several soil gas samples collected on
September 5, 2019. ECS compared detected concentrations for VOCs to sub-slab and exterior Vapor
Intrusion Screening Levels (VISL) for residential and non-residential scenarios. The laboratory data and
comparison data are shown in Table 2.

Laboratory results for sample SG-1 indicate detections of several VOCs above their respective method
detection limits. Of these detections, the concentration of TCE (270 ug/m3) exceeded both the
residential and non-residential soil gas VISLs (14 and 180 ug/m3, respectively).

Laboratory results for sample SG-2 indicate detections of several VOCs above their respective method
detection limits. Of these detections, the concentration of 1,3-Butadiene (32 ug/m3) exceeded the
residential soil gas VISL of 14 ug/m3, but below the non-residential soil gas VISL of 180 ug/m3.

Laboratory results for sample SG-3 indicate detections of several VOCs above their respective method
detection limits. Of these detections, the concentration of TCE (490 ug/m3) exceeded both the
residential and non-residential soil gas VISLs. The concentration of 1,3-Butadiene (27 ug/m3) exceeded
the residential soil gas VISL, but below the non-residential soil gas VISL. In addition, the concentration of
Chloroform (41 ug/m3) is at the residential VISL (41 ug/m3), but below its non-residential VISL (180
ug/m3).

Laboratory results for sample SG-4 indicate detections of several VOCS above their respective method
detection limits. Of these detections, the concentration of 1,3-Butadiene (18 ug/m3) exceeded the
residential soil gas VISL, but below the non-residential soil gas VISL.

Laboratory results for sample SG-5 indicate detections of several VOCS above their respective method
detection limits. Of these detections, the concentration of TCE at 90 ug/m3 is above its residential VISL,
but below its non-residential VISL. The concentration of 1,3-Butadiene (24 ug/m3) exceeded the
residential soil gas VISL, but below the non-residential soil gas VISL.

Laboratory results for sample SG-6 (Duplicate sample of SG-5) indicate detections of several VOCS above
their respective method detection limits. Of these detections, the concentration of TCE at 78 ug/m3 is
above its residential VISL but below its non-residential VISL. The concentration of 1,3-Butadiene (25
ug/m3) exceeded the residential soil gas VISL, but below the non-residential soil gas VISL.

The laboratory analytical results are included as Appendix B.

Based on the results of the soil gas analysis exceeding the residential and non-residential VISLs, ECS
input the detections into the NCDEQ, Risk Calculator for Vapor Intrusion for residential and non-
residential soil gas to indoor air. Based on the results of the risk calculator, the soil gas concentrations
identified in samples SG-1, SG-3, SG-5, and SG-6 exceed the acceptable risk for residential properties;
however, none of the soil gas concentrations exceeded the acceptable risk for non-residential
properties.
Report of Environmental Assessment
Former PE Valve Manufacturing
ECS Project No. 49:7572-B
November 6, 2019
5
3.2 Brownfields Survey
The Brownfields receptor survey identified residences in the vicinity of the site. In addition, several
utilities are provided to the vicinity of the subject property including municipal water service and storm
sewer collection by the City of Asheville, sanitary sewer service by the Metropolitan Sewerage District,
electricity by Duke Energy, and natural gas by PSNC. Two private water supply wells were observed
northeast-east approximately 720 feet and 900 feet from the site. The nearest surface water body is
Sweeten Creek located approximately 2,000 feet east of the site. The Brownfields receptor survey is
included as Appendix C.
4.0 CONCLUSIONS
Based on the results of the field activities and laboratory analysis, ECS concludes the following:
TCE was detected in soil gas samples, SG-1 and SG-3, at concentrations above residential and non-
residential VISLs. TCE was detected in soil gas samples SG-5 and SG-6 at concentrations above the
residential VISL, but below non-residential VISL. 1,3-Butadiene was detected in soil gas samples SG-
2, SG-3, SG-4, SG-5, and SG-6 at concentrations above the residential VISL, but below the non-
residential VISL). Chloroform was detected in soil gas sample SG-3 at a concentration at the
residential VISL, but below the non-residential VISL.
According to the NCDEQ Risk Calculator, the concentrations identified in samples SG-1, SG-3, SG-5,
and SG-6 represent a residential soil gas to indoor risk at the locations sampled.
The Brownfields receptor survey identified residences in the vicinity of the site. In addition, several
utilities are provided to the vicinity of the subject property including municipal water service. Two
private water supply wells were observed northeast-east approximately 720 feet and 900 feet from
the site. The nearest surface water body is Sweeten Creek located approximately 2,000 feet east of
the site.
5.0 RECOMMENDATIONS
Based on the results of this Brownfields assessment, ECS recommends the following:
If residential development is proposed on the site, a vapor mitigation system appears to be
required; however, if the site is to be redeveloped as an industrial/commercial facility (as is
proposed in the Brownfields Property Application), a vapor mitigation system may not be required.
A copy of this report should be submitted to the NCBP for their review.
6.0 QUALIFICATIONS OF REPORT
The activities and evaluative approaches used in this assessment are consistent with those normally
employed in environmental assessment projects of this type. Our evaluation of site conditions has been
based on our understanding of the site project information and the data obtained during our field
activities. This report was prepared for the express use of Mr. Peter Hall. Use of this report by other
individuals or companies implies their acceptance of the General Conditions of Service of the original
contract.

FIGURES

FIGURE 1SITE TOPOGRAPHIC MAP
FORMER PE VALVE
1140 SWEETEN CREEK ROAD
ASHEVILLE, BUNCOMBE COUNTY,
NORTH CAROLINA
ECS PROJECT NO. 49-7572-B
SOURCE:
USGS TOPOGRAPHIC MAP
ASHEVILLE, NORTH CAROLINAQUADRANGLE
DATED 1961, PHOTOREVISED 1991
SITE
FIGURE 2
SITE LOCATION MAP
FORMER PE VALVE FACILITY1140 SWEETEN CREEK ROAD
ASHEVILLE, BUNCOMBE COUNTY,
NORTH CAROLINA
ECS PROJECT NO. 49-7572-B
SOURCE:
GOOGLE EARTH, DATED 2015
SCALE:
LEGEND
= 100 FEET
FIGURE 3
SOIL GAS SAMPLE LOCATION MAP
FORMER PE VALVE FACILITY1140 SWEETEN CREEK ROAD
ASHEVILLE, BUNCOMBE COUNTY,
NORTH CAROLINA
ECS PROJECT NO. 49-7572-B
SOURCE:
GOOGLE EARTH, DATED 2015
SCALE:
SOIL GAS SAMPLE LOCATION
APPROXIMATE SITE BOUNDARY
LEGEND
= 100 FEET
SG-5
SG-3
SG-2SG-1
SG-4

TABLES

TABLE 1: COORDINATE TABLE OF SOIL GAS SAMPLING POINTS
Former PE Valve Manufacturing
1140 Sweeten Creek Road
Asheville, Buncombe County, North Carolina
ECS PROJECT NO. 49-7572-B

Point Description Longitude Latitude
SG-1 W 82°52'10.79" (dms)N 35°54'37.24" (dms)
SG-2 W 82°52'08.03" (dms)N 35°54'37.28" (dms)
SG-3 W 82°52'09.96" (dms)N 35°54'33.32" (dms)
SG-4 W 82°52'07.01" (dms)N 35°54'07.01" (dms)
SG-5 W 82°52'30.02" (dms)N 35°54'09.24" (dms)
Notes:
1. Field Data obtained on September 5, 2019
2. Horizontal Coordinates based on the North Carolina State Plane Coordinate System (NAD 83).
TABLE 2: SUMMARY OF SOIL GAS ANALYTICAL RESULTS
Former PE Valve Manufacturing1140 Sweeten Creek Road
Asheville, Buncombe County, North Carolina
ECS PROJECT NO. 49-7572-B
Sample ID SG-1 SG-2 SG-3 SG-4 SG-5 SG-6
Collection Date
Acetone 270 370 220 550 240 250 220,000 2,700,000
Benzene 12 45 12 37 29 29 120 1,600
1,3-Butadiene <0.44 32 27 18 25 25 14 180
2-Butanone (MEK)29 37 25 98 43 25 35,000 440,000
Carbon Disulfide 2.9J 26 5.9J 16 9.0 8.5 4,900 61,000
Chloroform 21 <0.98 41 <0.98 <0.98 <0.98 41 530
Chloromethane <0.83 <0.83 <0.83 <0.83 4.0 1.9 6,300 7,900
Cyclohexane 19 18 25 23 18 22 42,000 530,000
Dichlorodifluoromethane (F12)2.3 1.9 2.6 1.6 1.7 1.7 700 8,800
cis-1,2-Dichloroethylene <0.79 <0.79 4.0 75 <0.79 <0.79 NS NS
trans-1,2-Dichloroethene 58 39 48 51 41 37 NS NS
Ethanol 44 36 150 190 120 130 NS NS
Ethyl acetate 21 <0.72 16 19 21 13 490 6,100
Ethylbenzene 4.9 17 4.1 6.1 8.5 8.3 370 4,900
4-Ethyltoluene 1.1 <0.98 1.2 <0.98 1.3 1.3 NS NS
n-Heptane 11 32 12 20 18 18 2,800 35,000
n-Hexane 36 75 27J 48 46 44 4,900 61,000
Isopropanol 14 J 21 20 29 20 20 1,400 18,000
Methylene Chloride 2.0J <6.9 <6.9 <6.9 <6.9 <6.9 4,200 53,000
4-Methyl-2-pentanone (MIBK)16 39 8.4 12 17 12 21,000 260,000
Naphthalene 0.94 J <1.0 1.2 (V-35, Z-01)<1.0 1.1 (V-35, Z-01)<1.0 21 260
Propene (Propylene)440 280 240 180 310 310 21,000 260,000
Styrene 5.2 4.0 5.6 4.4 5.3 4.9 7,000 88,000
Tetrachloroethene 13 <1.4 1.3J <1.4 <1.4 <1.4 280 3,500
Toluene 49 200 42 100 120 110 35,000 440,000
1,1,1-Trichloroethane 6.8 <1.1 46 <1.1 <1.1 <1.1 35,000 440,000
Trichloroethylene 270 <1.1 790 13 90 78 14 180
Trichlorofluoromethane 960 14 1,500 35 5.5 5.4 NS NS
1,3,5-Trimethylbenzene <0.98 1.9 0.92J <0.98 1.1 1.0 420 5,300
Vinyl chloride <0.51 <0.51 <0.51 3.8 <0.51 <0.51 560 2,800
m,p-Xylene 15 56 15 20 27 26 700 8,800
o-Xylene 5.4 16 5.8 6.8 9.7 8.3 700 8,800
Notes:
Results presented in micrograms per cubic meter (ug/m3)
VALUE in bold indicates concentration is greater than Residential sub-slab and exterior VISL
VALUE underlined indicate concentration is greater than Non-Residential sub-slab and exterior soil VISLV-35: Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this
compound. Reported result is estimated.
Z-01: Compound fails the method requirement of 70-130% recovery for the LCS. Is classified by the lab as a difficult
compound and passes the in house limits of 50-150%.
J: Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentrationVISL: vapor intrusion screening level
VISLs published by the North Carolina Department of Environmental Quality - Inactive Hazardous Sites Branch in February 2018.
ANALYTICAL RESULTS Residential Sub-Slab
and Exterior VISL ug/m3
Non-Residential Sub-
Slab and Exterior Soil
VISL ug/m3
9/5/19
Volatile Organic Compounds by EPA Method TO-15

APPENDIX A

PHOTOGRAPHIC LOG
FORMER PE VALVE MANUFACTURING
1140 SWEETEN CREEK ROAD
ASHEVILLE, BUNCOMBE COUNTY, NORTH CAROLINA
Brownfields Project ID: 22081-18-11
ECS Project No. 49-7572-B
Photograph 1: General view of soil gas sampling activities.
Photograph 2: General view of drilling for MW-4 installation.
PHOTOGRAPHIC LOG
FORMER PE VALVE MANUFACTURING
1140 SWEETEN CREEK ROAD
ASHEVILLE, BUNCOMBE COUNTY, NORTH CAROLINA
Brownfields Project ID: 22081-18-11
ECS Project No. 49-7572-B
Photograph 3: General view of soil gas sampling activities.

APPENDIX B

39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
September 12, 2019
Jim Bevers
ECS Southeast - Asheville, NC
1900 Hendersonville Road, Suite 10
Asheville, NC 28806
Project Location: 1140 Sweeten Creek Road, Ashville, NC
Client Job Number:
Project Number: 49-7572-B
Laboratory Work Order Number: 19I0247
Enclosed are results of analyses for samples received by the laboratory on September 5, 2019. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
QA Officer
Katherine Allen
Laboratory Manager
Daren Damboragian
Page 1 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
9/12/2019ECS Southeast - Asheville, NC
1900 Hendersonville Road, Suite 10
Asheville, NC 28806
ATTN: Jim Bevers
49-7572-B
19I0247
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
1140 Sweeten Creek Road, Ashville, NC
SG-1 19I0247-01 Soil Gas EPA TO-15
SG-2 19I0247-02 Soil Gas EPA TO-15
SG-3 19I0247-03 Soil Gas EPA TO-15
SG-4 19I0247-04 Soil Gas EPA TO-15
SG-5 19I0247-05 Soil Gas EPA TO-15
SG-6 19I0247-06 Soil Gas EPA TO-15
Page 2 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
EPA TO-15
Qualifications:
Laboratory fortified blank /laboratory control sample recovery outside of control limits. Data validation is not affected since all results are
"not detected" for all samples in this batch for this compound and bias is on the high side.
Analyte & Samples(s) Qualified:
1,2,4-Trichlorobenzene
B240276-BS1
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
Naphthalene
19I0247-03[SG-3], 19I0247-05[SG-5], B240276-BS1
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data validation is not affected since
sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
1,2,4-Trichlorobenzene
B240276-BS1
Compound fails the method requirement of 70-130% recovery for the LCS. Is classified by the lab as a difficult compound and passes the in
house limits of 50-150%.
Analyte & Samples(s) Qualified:
Naphthalene
19I0247-03[SG-3], 19I0247-05[SG-5], B240276-BS1
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 3 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1140 Sweeten Creek Road, Ashv
Date Received: 9/5/2019
Work Order: 19I0247Sample Description/Location:
Field Sample #: SG-1
Sample ID: 19I0247-01
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -2
Receipt Vacuum(in Hg): -3.6
Sampled: 9/5/2019 10:57
Canister ID: 2302
Flow Controller ID: 4298
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 110 8.0 9/10/19 23:37 BRF2704192.8 6.6
Benzene 3.7 0.20 9/10/19 23:37 BRF1240.640.082 0.26
Benzyl chloride ND 0.20 9/10/19 23:37 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 9/10/19 23:37 BRFND41.30.074 0.49
Bromoform ND 0.20 9/10/19 23:37 BRFND42.10.090 0.93
Bromomethane ND 0.20 9/10/19 23:37 BRFND40.780.14 0.53
1,3-Butadiene ND 0.20 9/10/19 23:37 BRFND40.440.13 0.28
2-Butanone (MEK)9.8 8.0 9/10/19 23:37 BRF294240.31 0.92
Carbon Disulfide 0.94 2.0 9/10/19 23:37 BRFJ2.9 46.20.14 0.43
Carbon Tetrachloride ND 0.20 9/10/19 23:37 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 9/10/19 23:37 BRFND40.920.098 0.45
Chloroethane ND 0.20 9/10/19 23:37 BRFND40.530.12 0.32
Chloroform 4.2 0.20 9/10/19 23:37 BRF2140.980.074 0.36
Chloromethane ND 0.40 9/10/19 23:37 BRFND40.830.14 0.28
Cyclohexane 5.5 0.20 9/10/19 23:37 BRF1940.690.14 0.49
Dibromochloromethane ND 0.20 9/10/19 23:37 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 9/10/19 23:37 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 9/10/19 23:37 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 9/10/19 23:37 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 9/10/19 23:37 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.47 0.20 9/10/19 23:37 BRF2.3 40.990.087 0.43
1,1-Dichloroethane ND 0.20 9/10/19 23:37 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 9/10/19 23:37 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 9/10/19 23:37 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 9/10/19 23:37 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene 15 0.20 9/10/19 23:37 BRF5840.790.081 0.32
1,2-Dichloropropane ND 0.20 9/10/19 23:37 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 9/10/19 23:37 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 9/10/19 23:37 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 9/10/19 23:37 BRFND41.40.10 0.70
1,4-Dioxane ND 2.0 9/10/19 23:37 BRFND47.21.3 4.6
Ethanol 23 8.0 9/10/19 23:37 BRF444153.6 6.7
Ethyl Acetate 5.8 0.20 9/10/19 23:37 BRF2140.720.15 0.54
Ethylbenzene 1.1 0.20 9/10/19 23:37 BRF4.9 40.870.12 0.50
4-Ethyltoluene 0.22 0.20 9/10/19 23:37 BRF1.1 40.980.12 0.60
Heptane 2.7 0.20 9/10/19 23:37 BRF1140.820.12 0.48
Hexachlorobutadiene ND 0.20 9/10/19 23:37 BRFND42.10.092 0.98
Hexane 10 8.0 9/10/19 23:37 BRF364280.35 1.2
2-Hexanone (MBK)ND 0.20 9/10/19 23:37 BRFND40.820.12 0.48
Isopropanol 5.8 8.0 9/10/19 23:37 BRFJ144200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 9/10/19 23:37 BRFND40.720.10 0.36
Methylene Chloride 0.59 2.0 9/10/19 23:37 BRFJ2.0 46.90.24 0.84
4-Methyl-2-pentanone (MIBK)4.0 0.20 9/10/19 23:37 BRF1640.820.096 0.39
Naphthalene 0.18 0.20 9/10/19 23:37 BRFJ0.94 41.00.15 0.80
Propene 260 80 9/11/19 0:17 BRF440401402.0 3.4
Styrene 1.2 0.20 9/10/19 23:37 BRF5.2 40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 9/10/19 23:37 BRFND41.40.089 0.61
Page 4 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1140 Sweeten Creek Road, Ashv
Date Received: 9/5/2019
Work Order: 19I0247Sample Description/Location:
Field Sample #: SG-1
Sample ID: 19I0247-01
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28
Final Vacuum(in Hg): -2
Receipt Vacuum(in Hg): -3.6
Sampled: 9/5/2019 10:57
Canister ID: 2302
Flow Controller ID: 4298
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 1.9 0.20 9/10/19 23:37 BRF1341.40.11 0.75
Tetrahydrofuran ND 0.20 9/10/19 23:37 BRFND40.590.13 0.39
Toluene 13 0.20 9/10/19 23:37 BRF4940.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 9/10/19 23:37 BRFND41.50.14 1.0
1,1,1-Trichloroethane 1.3 0.20 9/10/19 23:37 BRF6.8 41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 9/10/19 23:37 BRFND41.10.082 0.45
Trichloroethylene 51 0.20 9/10/19 23:37 BRF27041.10.081 0.43
Trichlorofluoromethane (Freon 11)170 0.80 9/10/19 23:37 BRF96044.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 9/10/19 23:37 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene ND 0.20 9/10/19 23:37 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 9/10/19 23:37 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 9/10/19 23:37 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 9/10/19 23:37 BRFND40.510.13 0.32
m&p-Xylene 3.6 0.40 9/10/19 23:37 BRF1541.70.23 1.00
o-Xylene 1.3 0.20 9/10/19 23:37 BRF5.4 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)111 9/11/19 0:1770-130
4-Bromofluorobenzene (1)113 9/10/19 23:3770-130
Page 5 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1140 Sweeten Creek Road, Ashv
Date Received: 9/5/2019
Work Order: 19I0247Sample Description/Location:
Field Sample #: SG-2
Sample ID: 19I0247-02
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -25
Final Vacuum(in Hg): -2
Receipt Vacuum(in Hg): -5.1
Sampled: 9/5/2019 10:32
Canister ID: 2345
Flow Controller ID: 4301
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 160 8.0 9/11/19 0:57 BRF3704192.8 6.6
Benzene 14 0.20 9/11/19 0:57 BRF4540.640.082 0.26
Benzyl chloride ND 0.20 9/11/19 0:57 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 9/11/19 0:57 BRFND41.30.074 0.49
Bromoform ND 0.20 9/11/19 0:57 BRFND42.10.090 0.93
Bromomethane ND 0.20 9/11/19 0:57 BRFND40.780.14 0.53
1,3-Butadiene 15 0.20 9/11/19 0:57 BRF3240.440.13 0.28
2-Butanone (MEK)12 8.0 9/11/19 0:57 BRF374240.31 0.92
Carbon Disulfide 8.3 2.0 9/11/19 0:57 BRF2646.20.14 0.43
Carbon Tetrachloride ND 0.20 9/11/19 0:57 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 9/11/19 0:57 BRFND40.920.098 0.45
Chloroethane ND 0.20 9/11/19 0:57 BRFND40.530.12 0.32
Chloroform ND 0.20 9/11/19 0:57 BRFND40.980.074 0.36
Chloromethane ND 0.40 9/11/19 0:57 BRFND40.830.14 0.28
Cyclohexane 5.3 0.20 9/11/19 0:57 BRF1840.690.14 0.49
Dibromochloromethane ND 0.20 9/11/19 0:57 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 9/11/19 0:57 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 9/11/19 0:57 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 9/11/19 0:57 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 9/11/19 0:57 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.38 0.20 9/11/19 0:57 BRF1.9 40.990.087 0.43
1,1-Dichloroethane ND 0.20 9/11/19 0:57 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 9/11/19 0:57 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 9/11/19 0:57 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 9/11/19 0:57 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene 9.7 0.20 9/11/19 0:57 BRF3940.790.081 0.32
1,2-Dichloropropane ND 0.20 9/11/19 0:57 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 9/11/19 0:57 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 9/11/19 0:57 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 9/11/19 0:57 BRFND41.40.10 0.70
1,4-Dioxane ND 2.0 9/11/19 0:57 BRFND47.21.3 4.6
Ethanol 19 8.0 9/11/19 0:57 BRF364153.6 6.7
Ethyl Acetate ND 0.20 9/11/19 0:57 BRFND40.720.15 0.54
Ethylbenzene 3.9 0.20 9/11/19 0:57 BRF1740.870.12 0.50
4-Ethyltoluene ND 0.20 9/11/19 0:57 BRFND40.980.12 0.60
Heptane 7.8 0.20 9/11/19 0:57 BRF3240.820.12 0.48
Hexachlorobutadiene ND 0.20 9/11/19 0:57 BRFND42.10.092 0.98
Hexane 21 8.0 9/11/19 0:57 BRF754280.35 1.2
2-Hexanone (MBK)ND 0.20 9/11/19 0:57 BRFND40.820.12 0.48
Isopropanol 8.7 8.0 9/11/19 0:57 BRF214200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 9/11/19 0:57 BRFND40.720.10 0.36
Methylene Chloride ND 2.0 9/11/19 0:57 BRFND46.90.24 0.84
4-Methyl-2-pentanone (MIBK)9.6 0.20 9/11/19 0:57 BRF3940.820.096 0.39
Naphthalene ND 0.20 9/11/19 0:57 BRFND41.00.15 0.80
Propene 160 8.0 9/11/19 0:57 BRF2804140.20 0.34
Styrene 0.94 0.20 9/11/19 0:57 BRF4.0 40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 9/11/19 0:57 BRFND41.40.089 0.61
Page 6 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1140 Sweeten Creek Road, Ashv
Date Received: 9/5/2019
Work Order: 19I0247Sample Description/Location:
Field Sample #: SG-2
Sample ID: 19I0247-02
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -25
Final Vacuum(in Hg): -2
Receipt Vacuum(in Hg): -5.1
Sampled: 9/5/2019 10:32
Canister ID: 2345
Flow Controller ID: 4301
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene ND 0.20 9/11/19 0:57 BRFND41.40.11 0.75
Tetrahydrofuran ND 0.20 9/11/19 0:57 BRFND40.590.13 0.39
Toluene 52 0.20 9/11/19 0:57 BRF20040.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 9/11/19 0:57 BRFND41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 9/11/19 0:57 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 9/11/19 0:57 BRFND41.10.082 0.45
Trichloroethylene ND 0.20 9/11/19 0:57 BRFND41.10.081 0.43
Trichlorofluoromethane (Freon 11)2.4 0.80 9/11/19 0:57 BRF1444.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 9/11/19 0:57 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene ND 0.20 9/11/19 0:57 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene 0.40 0.20 9/11/19 0:57 BRF1.9 40.980.13 0.62
Vinyl Acetate ND 4.0 9/11/19 0:57 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 9/11/19 0:57 BRFND40.510.13 0.32
m&p-Xylene 13 0.40 9/11/19 0:57 BRF5641.70.23 1.00
o-Xylene 3.7 0.20 9/11/19 0:57 BRF1640.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)112 9/11/19 0:5770-130
Page 7 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1140 Sweeten Creek Road, Ashv
Date Received: 9/5/2019
Work Order: 19I0247Sample Description/Location:
Field Sample #: SG-3
Sample ID: 19I0247-03
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -26.5
Final Vacuum(in Hg): -2.5
Receipt Vacuum(in Hg): -5.9
Sampled: 9/5/2019 11:42
Canister ID: 2329
Flow Controller ID: 4368
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 94 8.0 9/11/19 1:38 BRF2204192.8 6.6
Benzene 3.8 0.20 9/11/19 1:38 BRF1240.640.082 0.26
Benzyl chloride ND 0.20 9/11/19 1:38 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 9/11/19 1:38 BRFND41.30.074 0.49
Bromoform ND 0.20 9/11/19 1:38 BRFND42.10.090 0.93
Bromomethane ND 0.20 9/11/19 1:38 BRFND40.780.14 0.53
1,3-Butadiene 12 0.20 9/11/19 1:38 BRF2740.440.13 0.28
2-Butanone (MEK)8.6 8.0 9/11/19 1:38 BRF254240.31 0.92
Carbon Disulfide 1.9 2.0 9/11/19 1:38 BRFJ5.9 46.20.14 0.43
Carbon Tetrachloride ND 0.20 9/11/19 1:38 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 9/11/19 1:38 BRFND40.920.098 0.45
Chloroethane ND 0.20 9/11/19 1:38 BRFND40.530.12 0.32
Chloroform 8.5 0.20 9/11/19 1:38 BRF4140.980.074 0.36
Chloromethane ND 0.40 9/11/19 1:38 BRFND40.830.14 0.28
Cyclohexane 7.2 0.20 9/11/19 1:38 BRF2540.690.14 0.49
Dibromochloromethane ND 0.20 9/11/19 1:38 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 9/11/19 1:38 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 9/11/19 1:38 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 9/11/19 1:38 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 9/11/19 1:38 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.52 0.20 9/11/19 1:38 BRF2.6 40.990.087 0.43
1,1-Dichloroethane ND 0.20 9/11/19 1:38 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 9/11/19 1:38 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 9/11/19 1:38 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene 1.0 0.20 9/11/19 1:38 BRF4.0 40.790.082 0.32
trans-1,2-Dichloroethylene 12 0.20 9/11/19 1:38 BRF4840.790.081 0.32
1,2-Dichloropropane ND 0.20 9/11/19 1:38 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 9/11/19 1:38 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 9/11/19 1:38 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 9/11/19 1:38 BRFND41.40.10 0.70
1,4-Dioxane ND 2.0 9/11/19 1:38 BRFND47.21.3 4.6
Ethanol 80 8.0 9/11/19 1:38 BRF1504153.6 6.7
Ethyl Acetate 4.4 0.20 9/11/19 1:38 BRF1640.720.15 0.54
Ethylbenzene 0.95 0.20 9/11/19 1:38 BRF4.1 40.870.12 0.50
4-Ethyltoluene 0.24 0.20 9/11/19 1:38 BRF1.2 40.980.12 0.60
Heptane 2.9 0.20 9/11/19 1:38 BRF1240.820.12 0.48
Hexachlorobutadiene ND 0.20 9/11/19 1:38 BRFND42.10.092 0.98
Hexane 7.6 8.0 9/11/19 1:38 BRFJ274280.35 1.2
2-Hexanone (MBK)ND 0.20 9/11/19 1:38 BRFND40.820.12 0.48
Isopropanol 8.2 8.0 9/11/19 1:38 BRF204200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 9/11/19 1:38 BRFND40.720.10 0.36
Methylene Chloride ND 2.0 9/11/19 1:38 BRFND46.90.24 0.84
4-Methyl-2-pentanone (MIBK)2.1 0.20 9/11/19 1:38 BRF8.4 40.820.096 0.39
Naphthalene 0.24 0.20 9/11/19 1:38 BRFV-35, Z-01 1.2 41.00.15 0.80
Propene 140 8.0 9/11/19 1:38 BRF2404140.20 0.34
Styrene 1.3 0.20 9/11/19 1:38 BRF5.6 40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 9/11/19 1:38 BRFND41.40.089 0.61
Page 8 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1140 Sweeten Creek Road, Ashv
Date Received: 9/5/2019
Work Order: 19I0247Sample Description/Location:
Field Sample #: SG-3
Sample ID: 19I0247-03
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -26.5
Final Vacuum(in Hg): -2.5
Receipt Vacuum(in Hg): -5.9
Sampled: 9/5/2019 11:42
Canister ID: 2329
Flow Controller ID: 4368
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene 0.19 0.20 9/11/19 1:38 BRFJ1.3 41.40.11 0.75
Tetrahydrofuran ND 0.20 9/11/19 1:38 BRFND40.590.13 0.39
Toluene 11 0.20 9/11/19 1:38 BRF4240.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 9/11/19 1:38 BRFND41.50.14 1.0
1,1,1-Trichloroethane 8.4 0.20 9/11/19 1:38 BRF4641.10.075 0.41
1,1,2-Trichloroethane ND 0.20 9/11/19 1:38 BRFND41.10.082 0.45
Trichloroethylene 150 0.20 9/11/19 1:38 BRF79041.10.081 0.43
Trichlorofluoromethane (Freon 11)270 2.0 9/11/19 2:17 BRF150010110.29 1.6
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 9/11/19 1:38 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene ND 0.20 9/11/19 1:38 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene 0.19 0.20 9/11/19 1:38 BRFJ0.92 40.980.13 0.62
Vinyl Acetate ND 4.0 9/11/19 1:38 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 9/11/19 1:38 BRFND40.510.13 0.32
m&p-Xylene 3.4 0.40 9/11/19 1:38 BRF1541.70.23 1.00
o-Xylene 1.3 0.20 9/11/19 1:38 BRF5.8 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)112 9/11/19 1:3870-130
4-Bromofluorobenzene (1)112 9/11/19 2:1770-130
Page 9 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1140 Sweeten Creek Road, Ashv
Date Received: 9/5/2019
Work Order: 19I0247Sample Description/Location:
Field Sample #: SG-4
Sample ID: 19I0247-04
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28.5
Final Vacuum(in Hg): -2
Receipt Vacuum(in Hg): -4.5
Sampled: 9/5/2019 11:18
Canister ID: 2301
Flow Controller ID: 4367
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 230 20 9/11/19 3:38 BRF55010486.9 16
Benzene 12 0.20 9/11/19 2:58 BRF3740.640.082 0.26
Benzyl chloride ND 0.20 9/11/19 2:58 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 9/11/19 2:58 BRFND41.30.074 0.49
Bromoform ND 0.20 9/11/19 2:58 BRFND42.10.090 0.93
Bromomethane ND 0.20 9/11/19 2:58 BRFND40.780.14 0.53
1,3-Butadiene 8.0 0.20 9/11/19 2:58 BRF1840.440.13 0.28
2-Butanone (MEK)33 8.0 9/11/19 2:58 BRF984240.31 0.92
Carbon Disulfide 5.1 2.0 9/11/19 2:58 BRF1646.20.14 0.43
Carbon Tetrachloride ND 0.20 9/11/19 2:58 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 9/11/19 2:58 BRFND40.920.098 0.45
Chloroethane ND 0.20 9/11/19 2:58 BRFND40.530.12 0.32
Chloroform ND 0.20 9/11/19 2:58 BRFND40.980.074 0.36
Chloromethane ND 0.40 9/11/19 2:58 BRFND40.830.14 0.28
Cyclohexane 6.7 0.20 9/11/19 2:58 BRF2340.690.14 0.49
Dibromochloromethane ND 0.20 9/11/19 2:58 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 9/11/19 2:58 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 9/11/19 2:58 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 9/11/19 2:58 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 9/11/19 2:58 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.33 0.20 9/11/19 2:58 BRF1.6 40.990.087 0.43
1,1-Dichloroethane ND 0.20 9/11/19 2:58 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 9/11/19 2:58 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 9/11/19 2:58 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene 19 0.20 9/11/19 2:58 BRF7540.790.082 0.32
trans-1,2-Dichloroethylene 13 0.20 9/11/19 2:58 BRF5140.790.081 0.32
1,2-Dichloropropane ND 0.20 9/11/19 2:58 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 9/11/19 2:58 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 9/11/19 2:58 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 9/11/19 2:58 BRFND41.40.10 0.70
1,4-Dioxane ND 2.0 9/11/19 2:58 BRFND47.21.3 4.6
Ethanol 100 8.0 9/11/19 2:58 BRF1904153.6 6.7
Ethyl Acetate 5.3 0.20 9/11/19 2:58 BRF1940.720.15 0.54
Ethylbenzene 1.4 0.20 9/11/19 2:58 BRF6.1 40.870.12 0.50
4-Ethyltoluene ND 0.20 9/11/19 2:58 BRFND40.980.12 0.60
Heptane 4.9 0.20 9/11/19 2:58 BRF2040.820.12 0.48
Hexachlorobutadiene ND 0.20 9/11/19 2:58 BRFND42.10.092 0.98
Hexane 14 8.0 9/11/19 2:58 BRF484280.35 1.2
2-Hexanone (MBK)ND 0.20 9/11/19 2:58 BRFND40.820.12 0.48
Isopropanol 12 8.0 9/11/19 2:58 BRF294200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 9/11/19 2:58 BRFND40.720.10 0.36
Methylene Chloride ND 2.0 9/11/19 2:58 BRFND46.90.24 0.84
4-Methyl-2-pentanone (MIBK)2.9 0.20 9/11/19 2:58 BRF1240.820.096 0.39
Naphthalene ND 0.20 9/11/19 2:58 BRFND41.00.15 0.80
Propene 110 8.0 9/11/19 2:58 BRF1804140.20 0.34
Styrene 1.0 0.20 9/11/19 2:58 BRF4.4 40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 9/11/19 2:58 BRFND41.40.089 0.61
Page 10 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1140 Sweeten Creek Road, Ashv
Date Received: 9/5/2019
Work Order: 19I0247Sample Description/Location:
Field Sample #: SG-4
Sample ID: 19I0247-04
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -28.5
Final Vacuum(in Hg): -2
Receipt Vacuum(in Hg): -4.5
Sampled: 9/5/2019 11:18
Canister ID: 2301
Flow Controller ID: 4367
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene ND 0.20 9/11/19 2:58 BRFND41.40.11 0.75
Tetrahydrofuran ND 0.20 9/11/19 2:58 BRFND40.590.13 0.39
Toluene 27 0.20 9/11/19 2:58 BRF10040.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 9/11/19 2:58 BRFND41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 9/11/19 2:58 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 9/11/19 2:58 BRFND41.10.082 0.45
Trichloroethylene 2.4 0.20 9/11/19 2:58 BRF1341.10.081 0.43
Trichlorofluoromethane (Freon 11)6.2 0.80 9/11/19 2:58 BRF3544.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 9/11/19 2:58 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene ND 0.20 9/11/19 2:58 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene ND 0.20 9/11/19 2:58 BRFND40.980.13 0.62
Vinyl Acetate ND 4.0 9/11/19 2:58 BRFND4140.095 0.34
Vinyl Chloride 1.5 0.20 9/11/19 2:58 BRF3.8 40.510.13 0.32
m&p-Xylene 4.7 0.40 9/11/19 2:58 BRF2041.70.23 1.00
o-Xylene 1.6 0.20 9/11/19 2:58 BRF6.8 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)110 9/11/19 3:3870-130
4-Bromofluorobenzene (1)112 9/11/19 2:5870-130
Page 11 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1140 Sweeten Creek Road, Ashv
Date Received: 9/5/2019
Work Order: 19I0247Sample Description/Location:
Field Sample #: SG-5
Sample ID: 19I0247-05
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -1
Receipt Vacuum(in Hg): -3.7
Sampled: 9/5/2019 12:03
Canister ID: 2328
Flow Controller ID: 4203
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 100 8.0 9/11/19 4:19 BRF2404192.8 6.6
Benzene 9.0 0.20 9/11/19 4:19 BRF2940.640.082 0.26
Benzyl chloride ND 0.20 9/11/19 4:19 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 9/11/19 4:19 BRFND41.30.074 0.49
Bromoform ND 0.20 9/11/19 4:19 BRFND42.10.090 0.93
Bromomethane ND 0.20 9/11/19 4:19 BRFND40.780.14 0.53
1,3-Butadiene 11 0.20 9/11/19 4:19 BRF2540.440.13 0.28
2-Butanone (MEK)14 8.0 9/11/19 4:19 BRF434240.31 0.92
Carbon Disulfide 2.9 2.0 9/11/19 4:19 BRF9.0 46.20.14 0.43
Carbon Tetrachloride ND 0.20 9/11/19 4:19 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 9/11/19 4:19 BRFND40.920.098 0.45
Chloroethane ND 0.20 9/11/19 4:19 BRFND40.530.12 0.32
Chloroform ND 0.20 9/11/19 4:19 BRFND40.980.074 0.36
Chloromethane 1.9 0.40 9/11/19 4:19 BRF4.0 40.830.14 0.28
Cyclohexane 5.3 0.20 9/11/19 4:19 BRF1840.690.14 0.49
Dibromochloromethane ND 0.20 9/11/19 4:19 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 9/11/19 4:19 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 9/11/19 4:19 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 9/11/19 4:19 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 9/11/19 4:19 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.34 0.20 9/11/19 4:19 BRF1.7 40.990.087 0.43
1,1-Dichloroethane ND 0.20 9/11/19 4:19 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 9/11/19 4:19 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 9/11/19 4:19 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 9/11/19 4:19 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene 10 0.20 9/11/19 4:19 BRF4140.790.081 0.32
1,2-Dichloropropane ND 0.20 9/11/19 4:19 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 9/11/19 4:19 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 9/11/19 4:19 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 9/11/19 4:19 BRFND41.40.10 0.70
1,4-Dioxane ND 2.0 9/11/19 4:19 BRFND47.21.3 4.6
Ethanol 65 8.0 9/11/19 4:19 BRF1204153.6 6.7
Ethyl Acetate 5.9 0.20 9/11/19 4:19 BRF2140.720.15 0.54
Ethylbenzene 2.0 0.20 9/11/19 4:19 BRF8.5 40.870.12 0.50
4-Ethyltoluene 0.27 0.20 9/11/19 4:19 BRF1.3 40.980.12 0.60
Heptane 4.5 0.20 9/11/19 4:19 BRF1840.820.12 0.48
Hexachlorobutadiene ND 0.20 9/11/19 4:19 BRFND42.10.092 0.98
Hexane 13 8.0 9/11/19 4:19 BRF464280.35 1.2
2-Hexanone (MBK)ND 0.20 9/11/19 4:19 BRFND40.820.12 0.48
Isopropanol 8.3 8.0 9/11/19 4:19 BRF204200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 9/11/19 4:19 BRFND40.720.10 0.36
Methylene Chloride ND 2.0 9/11/19 4:19 BRFND46.90.24 0.84
4-Methyl-2-pentanone (MIBK)4.2 0.20 9/11/19 4:19 BRF1740.820.096 0.39
Naphthalene 0.22 0.20 9/11/19 4:19 BRFV-35, Z-01 1.1 41.00.15 0.80
Propene 180 8.0 9/11/19 4:19 BRF3104140.20 0.34
Styrene 1.3 0.20 9/11/19 4:19 BRF5.3 40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 9/11/19 4:19 BRFND41.40.089 0.61
Page 12 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1140 Sweeten Creek Road, Ashv
Date Received: 9/5/2019
Work Order: 19I0247Sample Description/Location:
Field Sample #: SG-5
Sample ID: 19I0247-05
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27
Final Vacuum(in Hg): -1
Receipt Vacuum(in Hg): -3.7
Sampled: 9/5/2019 12:03
Canister ID: 2328
Flow Controller ID: 4203
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene ND 0.20 9/11/19 4:19 BRFND41.40.11 0.75
Tetrahydrofuran ND 0.20 9/11/19 4:19 BRFND40.590.13 0.39
Toluene 31 0.20 9/11/19 4:19 BRF12040.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 9/11/19 4:19 BRFND41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 9/11/19 4:19 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 9/11/19 4:19 BRFND41.10.082 0.45
Trichloroethylene 17 0.20 9/11/19 4:19 BRF9041.10.081 0.43
Trichlorofluoromethane (Freon 11)0.97 0.80 9/11/19 4:19 BRF5.5 44.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 9/11/19 4:19 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene ND 0.20 9/11/19 4:19 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene 0.22 0.20 9/11/19 4:19 BRF1.1 40.980.13 0.62
Vinyl Acetate ND 4.0 9/11/19 4:19 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 9/11/19 4:19 BRFND40.510.13 0.32
m&p-Xylene 6.3 0.40 9/11/19 4:19 BRF2741.70.23 1.00
o-Xylene 2.2 0.20 9/11/19 4:19 BRF9.7 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)111 9/11/19 4:1970-130
Page 13 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1140 Sweeten Creek Road, Ashv
Date Received: 9/5/2019
Work Order: 19I0247Sample Description/Location:
Field Sample #: SG-6
Sample ID: 19I0247-06
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27.5
Final Vacuum(in Hg): -1
Receipt Vacuum(in Hg): -4
Sampled: 9/5/2019 12:03
Canister ID: 2339
Flow Controller ID: 4202
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Acetone 100 8.0 9/11/19 5:00 BRF2504192.8 6.6
Benzene 8.9 0.20 9/11/19 5:00 BRF2940.640.082 0.26
Benzyl chloride ND 0.20 9/11/19 5:00 BRFND41.00.044 0.23
Bromodichloromethane ND 0.20 9/11/19 5:00 BRFND41.30.074 0.49
Bromoform ND 0.20 9/11/19 5:00 BRFND42.10.090 0.93
Bromomethane ND 0.20 9/11/19 5:00 BRFND40.780.14 0.53
1,3-Butadiene 11 0.20 9/11/19 5:00 BRF2540.440.13 0.28
2-Butanone (MEK)8.5 8.0 9/11/19 5:00 BRF254240.31 0.92
Carbon Disulfide 2.7 2.0 9/11/19 5:00 BRF8.5 46.20.14 0.43
Carbon Tetrachloride ND 0.20 9/11/19 5:00 BRFND41.30.065 0.41
Chlorobenzene ND 0.20 9/11/19 5:00 BRFND40.920.098 0.45
Chloroethane ND 0.20 9/11/19 5:00 BRFND40.530.12 0.32
Chloroform ND 0.20 9/11/19 5:00 BRFND40.980.074 0.36
Chloromethane 0.91 0.40 9/11/19 5:00 BRF1.9 40.830.14 0.28
Cyclohexane 6.3 0.20 9/11/19 5:00 BRF2240.690.14 0.49
Dibromochloromethane ND 0.20 9/11/19 5:00 BRFND41.70.066 0.57
1,2-Dibromoethane (EDB)ND 0.20 9/11/19 5:00 BRFND41.50.078 0.60
1,2-Dichlorobenzene ND 0.20 9/11/19 5:00 BRFND41.20.096 0.58
1,3-Dichlorobenzene ND 0.20 9/11/19 5:00 BRFND41.20.10 0.62
1,4-Dichlorobenzene ND 0.20 9/11/19 5:00 BRFND41.20.12 0.73
Dichlorodifluoromethane (Freon 12)0.34 0.20 9/11/19 5:00 BRF1.7 40.990.087 0.43
1,1-Dichloroethane ND 0.20 9/11/19 5:00 BRFND40.810.061 0.25
1,2-Dichloroethane ND 0.20 9/11/19 5:00 BRFND40.810.076 0.31
1,1-Dichloroethylene ND 0.20 9/11/19 5:00 BRFND40.790.081 0.32
cis-1,2-Dichloroethylene ND 0.20 9/11/19 5:00 BRFND40.790.082 0.32
trans-1,2-Dichloroethylene 9.3 0.20 9/11/19 5:00 BRF3740.790.081 0.32
1,2-Dichloropropane ND 0.20 9/11/19 5:00 BRFND40.920.071 0.33
cis-1,3-Dichloropropene ND 0.20 9/11/19 5:00 BRFND40.910.070 0.32
trans-1,3-Dichloropropene ND 0.20 9/11/19 5:00 BRFND40.910.073 0.33
1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)ND 0.20 9/11/19 5:00 BRFND41.40.10 0.70
1,4-Dioxane ND 2.0 9/11/19 5:00 BRFND47.21.3 4.6
Ethanol 71 8.0 9/11/19 5:00 BRF1304153.6 6.7
Ethyl Acetate 3.5 0.20 9/11/19 5:00 BRF1340.720.15 0.54
Ethylbenzene 1.9 0.20 9/11/19 5:00 BRF8.3 40.870.12 0.50
4-Ethyltoluene 0.27 0.20 9/11/19 5:00 BRF1.3 40.980.12 0.60
Heptane 4.4 0.20 9/11/19 5:00 BRF1840.820.12 0.48
Hexachlorobutadiene ND 0.20 9/11/19 5:00 BRFND42.10.092 0.98
Hexane 13 8.0 9/11/19 5:00 BRF444280.35 1.2
2-Hexanone (MBK)ND 0.20 9/11/19 5:00 BRFND40.820.12 0.48
Isopropanol 8.0 8.0 9/11/19 5:00 BRF204200.25 0.60
Methyl tert-Butyl Ether (MTBE)ND 0.20 9/11/19 5:00 BRFND40.720.10 0.36
Methylene Chloride ND 2.0 9/11/19 5:00 BRFND46.90.24 0.84
4-Methyl-2-pentanone (MIBK)2.9 0.20 9/11/19 5:00 BRF1240.820.096 0.39
Naphthalene ND 0.20 9/11/19 5:00 BRFND41.00.15 0.80
Propene 180 8.0 9/11/19 5:00 BRF3104140.20 0.34
Styrene 1.2 0.20 9/11/19 5:00 BRF4.9 40.850.12 0.53
1,1,2,2-Tetrachloroethane ND 0.20 9/11/19 5:00 BRFND41.40.089 0.61
Page 14 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL RESULTS
Project Location: 1140 Sweeten Creek Road, Ashv
Date Received: 9/5/2019
Work Order: 19I0247Sample Description/Location:
Field Sample #: SG-6
Sample ID: 19I0247-06
Sample Matrix: Soil Gas
Initial Vacuum(in Hg): -27.5
Final Vacuum(in Hg): -1
Receipt Vacuum(in Hg): -4
Sampled: 9/5/2019 12:03
Canister ID: 2339
Flow Controller ID: 4202
Sub Description/Location:
Canister Size: 1 liter
Flow Controller Type: Fixed-Orifice
Flow Controller Calibration
RPD Pre and Post-Sampling:
Sample Type: 10 min
RLResults AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
EPA TO-15
ppbv ug/m3
MDL MDL
Tetrachloroethylene ND 0.20 9/11/19 5:00 BRFND41.40.11 0.75
Tetrahydrofuran ND 0.20 9/11/19 5:00 BRFND40.590.13 0.39
Toluene 29 0.20 9/11/19 5:00 BRF11040.750.10 0.39
1,2,4-Trichlorobenzene ND 0.20 9/11/19 5:00 BRFND41.50.14 1.0
1,1,1-Trichloroethane ND 0.20 9/11/19 5:00 BRFND41.10.075 0.41
1,1,2-Trichloroethane ND 0.20 9/11/19 5:00 BRFND41.10.082 0.45
Trichloroethylene 14 0.20 9/11/19 5:00 BRF7841.10.081 0.43
Trichlorofluoromethane (Freon 11)0.96 0.80 9/11/19 5:00 BRF5.4 44.50.12 0.65
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)ND 0.80 9/11/19 5:00 BRFND46.10.12 0.93
1,2,4-Trimethylbenzene ND 0.20 9/11/19 5:00 BRFND40.980.13 0.63
1,3,5-Trimethylbenzene 0.21 0.20 9/11/19 5:00 BRF1.0 40.980.13 0.62
Vinyl Acetate ND 4.0 9/11/19 5:00 BRFND4140.095 0.34
Vinyl Chloride ND 0.20 9/11/19 5:00 BRFND40.510.13 0.32
m&p-Xylene 5.9 0.40 9/11/19 5:00 BRF2641.70.23 1.00
o-Xylene 1.9 0.20 9/11/19 5:00 BRF8.3 40.870.12 0.54
Surrogates % Recovery % REC Limits
4-Bromofluorobenzene (1)112 9/11/19 5:0070-130
Page 15 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: TO-15 Prep-EPA TO-15
Lab Number [Field ID]Batch Date
Pressure
Dilution
Pre
Dilution
Pre-Dil
Initial
mL
Pre-Dil
Final
mL
Default
Injection
mL
Actual
Injection
mL
19I0247-01 [SG-1]B240276 1.5 1 N/A 1000 400 150 09/10/19
19I0247-01RE1 [SG-1]B240276 1.5 1 N/A 1000 400 15 09/10/19
19I0247-02 [SG-2]B240276 1.5 1 N/A 1000 400 150 09/10/19
19I0247-03 [SG-3]B240276 1.5 1 N/A 1000 400 150 09/10/19
19I0247-03RE1 [SG-3]B240276 1.5 1 N/A 1000 400 60 09/10/19
19I0247-04 [SG-4]B240276 1.5 1 N/A 1000 400 150 09/10/19
19I0247-04RE1 [SG-4]B240276 1.5 1 N/A 1000 400 60 09/10/19
19I0247-05 [SG-5]B240276 1.5 1 N/A 1000 400 150 09/10/19
19I0247-06 [SG-6]B240276 1.5 1 N/A 1000 400 150 09/10/19
Page 16 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B240276 - TO-15 Prep
Blank (B240276-BLK1)Prepared & Analyzed: 09/10/19
1.4NDAcetone
0.035NDBenzene
0.035NDBenzyl chloride
0.035NDBromodichloromethane
0.035NDBromoform
0.035NDBromomethane
0.035ND1,3-Butadiene
1.4ND2-Butanone (MEK)
0.35NDCarbon Disulfide
0.035NDCarbon Tetrachloride
0.035NDChlorobenzene
0.035NDChloroethane
0.035NDChloroform
0.070NDChloromethane
0.035NDCyclohexane
0.035NDDibromochloromethane
0.035ND1,2-Dibromoethane (EDB)
0.035ND1,2-Dichlorobenzene
0.035ND1,3-Dichlorobenzene
0.035ND1,4-Dichlorobenzene
0.035NDDichlorodifluoromethane (Freon 12)
0.035ND1,1-Dichloroethane
0.035ND1,2-Dichloroethane
0.035ND1,1-Dichloroethylene
0.035NDcis-1,2-Dichloroethylene
0.035NDtrans-1,2-Dichloroethylene
0.035ND1,2-Dichloropropane
0.035NDcis-1,3-Dichloropropene
0.035NDtrans-1,3-Dichloropropene
0.035ND1,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
0.35ND1,4-Dioxane
1.4NDEthanol
0.035NDEthyl Acetate
0.035NDEthylbenzene
0.035ND4-Ethyltoluene
0.035NDHeptane
0.035NDHexachlorobutadiene
1.4NDHexane
0.035ND2-Hexanone (MBK)
1.4NDIsopropanol
0.035NDMethyl tert-Butyl Ether (MTBE)
0.35NDMethylene Chloride
0.035ND4-Methyl-2-pentanone (MIBK)
0.035NDNaphthalene
1.4NDPropene
0.035NDStyrene
Page 17 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B240276 - TO-15 Prep
Blank (B240276-BLK1)Prepared & Analyzed: 09/10/19
0.035ND1,1,2,2-Tetrachloroethane
0.035NDTetrachloroethylene
0.035NDTetrahydrofuran
0.035NDToluene
0.035ND1,2,4-Trichlorobenzene
0.035ND1,1,1-Trichloroethane
0.035ND1,1,2-Trichloroethane
0.035NDTrichloroethylene
0.14NDTrichlorofluoromethane (Freon 11)
0.14ND1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
0.035ND1,2,4-Trimethylbenzene
0.035ND1,3,5-Trimethylbenzene
0.70NDVinyl Acetate
0.035NDVinyl Chloride
0.070NDm&p-Xylene
0.035NDo-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1129.00
LCS (B240276-BS1)Prepared & Analyzed: 09/10/19
5.00 70-1301075.35Acetone
5.00 70-13086.84.34Benzene
5.00 70-1301145.68Benzyl chloride
5.00 70-13083.64.18Bromodichloromethane
5.00 70-1301035.17Bromoform
5.00 70-1301015.07Bromomethane
5.00 70-13093.14.661,3-Butadiene
5.00 70-13092.94.642-Butanone (MEK)
5.00 70-13094.74.74Carbon Disulfide
5.00 70-13086.34.32Carbon Tetrachloride
5.00 70-13089.14.45Chlorobenzene
5.00 70-13098.14.90Chloroethane
5.00 70-13088.64.43Chloroform
5.00 70-13087.64.38Chloromethane
5.00 70-13076.03.80Cyclohexane
5.00 70-13089.74.48Dibromochloromethane
5.00 70-13085.24.261,2-Dibromoethane (EDB)
5.00 70-1301175.831,2-Dichlorobenzene
5.00 70-1301115.551,3-Dichlorobenzene
5.00 70-1301125.611,4-Dichlorobenzene
5.00 70-13093.84.69Dichlorodifluoromethane (Freon 12)
5.00 70-13088.64.431,1-Dichloroethane
5.00 70-13084.44.221,2-Dichloroethane
5.00 70-13085.94.301,1-Dichloroethylene
5.00 70-13085.94.29cis-1,2-Dichloroethylene
5.00 70-13087.14.36trans-1,2-Dichloroethylene
5.00 70-13076.63.831,2-Dichloropropane
Page 18 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ug/m3 Spike Level
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Flag/Qual Analyte
Air Toxics by EPA Compendium Methods - Quality Control
QUALITY CONTROL
RL
ppbv
Results RL Results ppbv
Batch B240276 - TO-15 Prep
LCS (B240276-BS1)Prepared & Analyzed: 09/10/19
5.00 70-13080.84.04cis-1,3-Dichloropropene
5.00 70-13084.94.24trans-1,3-Dichloropropene
5.00 70-13098.04.901,2-Dichloro-1,1,2,2-tetrafluoroethane
(Freon 114)
5.00 70-1301185.881,4-Dioxane
5.00 70-1301085.40Ethanol
5.00 70-13093.04.65Ethyl Acetate
5.00 70-13086.44.32Ethylbenzene
5.00 70-13098.14.914-Ethyltoluene
5.00 70-13083.54.18Heptane
5.00 70-1301246.22Hexachlorobutadiene
5.00 70-13090.14.50Hexane
5.00 70-13089.94.492-Hexanone (MBK)
5.00 70-1301035.14Isopropanol
5.00 70-13085.54.28Methyl tert-Butyl Ether (MTBE)
5.00 70-13084.24.21Methylene Chloride
5.00 70-13092.94.644-Methyl-2-pentanone (MIBK)
5.00 Z-01, V-3570-1301487.42Naphthalene *
5.00 70-13083.84.19Propene
5.00 70-13091.74.58Styrene
5.00 70-13093.54.671,1,2,2-Tetrachloroethane
5.00 70-13089.14.45Tetrachloroethylene
5.00 70-1301015.07Tetrahydrofuran
5.00 70-13084.54.22Toluene
5.00 L-01, V-3670-1301487.391,2,4-Trichlorobenzene *
5.00 70-13076.43.821,1,1-Trichloroethane
5.00 70-13085.64.281,1,2-Trichloroethane
5.00 70-13085.54.28Trichloroethylene
5.00 70-1301085.40Trichlorofluoromethane (Freon 11)
5.00 70-13093.34.671,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
5.00 70-1301055.241,2,4-Trimethylbenzene
5.00 70-13099.14.961,3,5-Trimethylbenzene
5.00 70-13096.24.81Vinyl Acetate
5.00 70-13094.04.70Vinyl Chloride
10.0 70-13092.89.28m&p-Xylene
5.00 70-13089.44.47o-Xylene
8.00 70-130Surrogate: 4-Bromofluorobenzene (1)1149.09
Page 19 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Note: Blank Subtraction is not performed unless otherwise noted
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
RL Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
LCS Laboratory Control Sample
Laboratory Control SampleLCS Dup Duplicate Laboratory Control Sample
MS Matrix Spike Sample
MS Dup Duplicate Matrix Spike Sample
REC Recovery
QC Quality Control
ppbv Parts per billion volume
EPA United States Environmental Protection Agency
Percent Recovery% REC
ND Not Detected
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
Not ApplicableN/A
DL Detection Limit
Not CalculatedNC
LFB/LCS Lab Fortified Blank/Lab Control Sample
ORP Oxidation-Reduction Potential
Not dry weight correctedwet
Percent weight% wt
KilogramKg
Gramg
Milligrammg
Microgramg
Nanogramng
LiterL
MillilitermL
Microliter L
Cubic Meterm3
Extractable Petroleum HydrocarbonsEPH
Volatile Petroleum HydrocarbonsVPH
Air Petroleum HydrocarbonsAPH
Flame Ionization DetectorFID
Photo Ionization DetectorPID
FLAG/QUALIFIER SUMMARY
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank /laboratory control sample recovery outside of control limits. Data validation is not
affected since all results are "not detected" for all samples in this batch for this compound and bias is on the high
side.
L-01
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this
compound. Reported result is estimated.
V-35
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side. Data
validation is not affected since sample result was "not detected" for this compound.
V-36
Compound fails the method requirement of 70-130% recovery for the LCS. Is classified by the lab as a difficult
compound and passes the in house limits of 50-150%.
Z-01
Page 20 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYST
Thomas P. HniteckiTPH
PDF Management StationSTATION
Kerry K. McGeeKKM
Christine M. FarinaCF2
Brittany R. FiskBRF
Page 21 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Initial Cal Check (S039721-ICV1 )Lab File ID: G1923934.D Analyzed: 08/28/19 12:54
Bromochloromethane (1)443826 8.54 448077 8.54 60 - 14099 0.0000 +/-0.50
1,4-Difluorobenzene (1)1177845 10.32 1185200 10.32 60 - 14099 0.0000 +/-0.50
Chlorobenzene-d5 (1)1032941 14.697 1038060 14.697 60 - 140100 0.0000 +/-0.50
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
Calibration Check (S040217-CCV1 )Lab File ID: G1925306.D Analyzed: 09/10/19 12:45
Bromochloromethane (1)395554 8.54 448077 8.54 60 - 14088 0.0000 +/-0.50
1,4-Difluorobenzene (1)1092243 10.32 1185200 10.32 60 - 14092 0.0000 +/-0.50
Chlorobenzene-d5 (1)979636 14.697 1038060 14.697 60 - 14094 0.0000 +/-0.50
LCS (B240276-BS1 )Lab File ID: G1925307.D Analyzed: 09/10/19 13:25
Bromochloromethane (1)409823 8.54 395554 8.54 60 - 140104 0.0000 +/-0.50
1,4-Difluorobenzene (1)1132366 10.32 1092243 10.32 60 - 140104 0.0000 +/-0.50
Chlorobenzene-d5 (1)1049039 14.697 979636 14.697 60 - 140107 0.0000 +/-0.50
Blank (B240276-BLK1 )Lab File ID: G1925309.D Analyzed: 09/10/19 14:54
Bromochloromethane (1)402545 8.54 395554 8.54 60 - 140102 0.0000 +/-0.50
1,4-Difluorobenzene (1)1072991 10.32 1092243 10.32 60 - 14098 0.0000 +/-0.50
Chlorobenzene-d5 (1)994200 14.697 979636 14.697 60 - 140101 0.0000 +/-0.50
SG-1 (19I0247-01 )Lab File ID: G1925324.D Analyzed: 09/10/19 23:37
Bromochloromethane (1)370932 8.54 395554 8.54 60 - 14094 0.0000 +/-0.50
1,4-Difluorobenzene (1)1078389 10.32 1092243 10.32 60 - 14099 0.0000 +/-0.50
Chlorobenzene-d5 (1)1007618 14.697 979636 14.697 60 - 140103 0.0000 +/-0.50
SG-1 (19I0247-01RE1 )Lab File ID: G1925325.D Analyzed: 09/11/19 00:17
Bromochloromethane (1)377512 8.54 395554 8.54 60 - 14095 0.0000 +/-0.50
1,4-Difluorobenzene (1)1057703 10.32 1092243 10.32 60 - 14097 0.0000 +/-0.50
Chlorobenzene-d5 (1)944070 14.697 979636 14.697 60 - 14096 0.0000 +/-0.50
SG-2 (19I0247-02 )Lab File ID: G1925326.D Analyzed: 09/11/19 00:57
Bromochloromethane (1)368022 8.533 395554 8.54 60 - 14093 -0.0070 +/-0.50
1,4-Difluorobenzene (1)1060095 10.32 1092243 10.32 60 - 14097 0.0000 +/-0.50
Chlorobenzene-d5 (1)996797 14.697 979636 14.697 60 - 140102 0.0000 +/-0.50
SG-3 (19I0247-03 )Lab File ID: G1925327.D Analyzed: 09/11/19 01:38
Bromochloromethane (1)367811 8.54 395554 8.54 60 - 14093 0.0000 +/-0.50
1,4-Difluorobenzene (1)1067096 10.32 1092243 10.32 60 - 14098 0.0000 +/-0.50
Chlorobenzene-d5 (1)1001629 14.697 979636 14.697 60 - 140102 0.0000 +/-0.50
Page 22 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
INTERNAL STANDARD AREA AND RT SUMMARY
EPA TO-15
RTResponseInternal Standard Area %RT DiffResponse
Reference
RT
Reference Area %
Limits
RT Diff
Limit Q
SG-3 (19I0247-03RE1 )Lab File ID: G1925328.D Analyzed: 09/11/19 02:17
Bromochloromethane (1)363013 8.54 395554 8.54 60 - 14092 0.0000 +/-0.50
1,4-Difluorobenzene (1)1062768 10.32 1092243 10.32 60 - 14097 0.0000 +/-0.50
Chlorobenzene-d5 (1)981767 14.697 979636 14.697 60 - 140100 0.0000 +/-0.50
SG-4 (19I0247-04 )Lab File ID: G1925329.D Analyzed: 09/11/19 02:58
Bromochloromethane (1)376619 8.54 395554 8.54 60 - 14095 0.0000 +/-0.50
1,4-Difluorobenzene (1)1083531 10.32 1092243 10.32 60 - 14099 0.0000 +/-0.50
Chlorobenzene-d5 (1)1023724 14.697 979636 14.697 60 - 140105 0.0000 +/-0.50
SG-4 (19I0247-04RE1 )Lab File ID: G1925330.D Analyzed: 09/11/19 03:38
Bromochloromethane (1)377337 8.54 395554 8.54 60 - 14095 0.0000 +/-0.50
1,4-Difluorobenzene (1)1082107 10.32 1092243 10.32 60 - 14099 0.0000 +/-0.50
Chlorobenzene-d5 (1)1009600 14.697 979636 14.697 60 - 140103 0.0000 +/-0.50
SG-5 (19I0247-05 )Lab File ID: G1925331.D Analyzed: 09/11/19 04:19
Bromochloromethane (1)384476 8.54 395554 8.54 60 - 14097 0.0000 +/-0.50
1,4-Difluorobenzene (1)1103757 10.32 1092243 10.32 60 - 140101 0.0000 +/-0.50
Chlorobenzene-d5 (1)1036496 14.697 979636 14.697 60 - 140106 0.0000 +/-0.50
SG-6 (19I0247-06 )Lab File ID: G1925332.D Analyzed: 09/11/19 05:00
Bromochloromethane (1)387854 8.534 395554 8.54 60 - 14098 -0.0060 +/-0.50
1,4-Difluorobenzene (1)1105445 10.32 1092243 10.32 60 - 140101 0.0000 +/-0.50
Chlorobenzene-d5 (1)1040768 14.697 979636 14.697 60 - 140106 0.0000 +/-0.50
Page 23 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S040217-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.9248679A -7.5 304.63 0.99961265.00Acetone
0.7040865A -15.8 304.21 0.83623785.00Benzene
0.7973411A 7.1 305.36 0.74443445.00Benzyl chloride
0.5189688A -18.4 304.08 0.63603055.00Bromodichloromethane
0.468053A 2.9 305.14 0.45504915.00Bromoform
0.5244371A -3.1 304.84 0.54132125.00Bromomethane
0.4521982A -10.8 304.46 0.50716885.001,3-Butadiene
1.209386A -15.9 304.21 1.4377265.002-Butanone (MEK)
1.714772A -10.8 304.46 1.9227635.00Carbon Disulfide
0.4536265A -15.1 304.24 0.53432965.00Carbon Tetrachloride
0.729092A -10.6 304.47 0.81570025.00Chlorobenzene
0.3065149A -5.6 304.72 0.32457535.00Chloroethane
1.306797A -13.2 304.34 1.5053385.00Chloroform
0.546021A -17.0 304.15 0.65780215.00Chloromethane
0.2964351A -24.5 303.78 0.39262855.00Cyclohexane
0.5389153A -8.8 304.56 0.59077775.00Dibromochloromethane
0.4776713A -14.4 304.28 0.55789985.001,2-Dibromoethane (EDB)
0.5483114A 9.0 305.45 0.50315635.001,2-Dichlorobenzene
0.62245A 6.8 305.34 0.58266515.001,3-Dichlorobenzene
0.6141301A 8.6 305.43 0.5654365.001,4-Dichlorobenzene
1.290261A -17.5 304.12 1.5644055.00Dichlorodifluoromethane (Freon 12)
1.115539A -15.9 304.21 1.3260735.001,1-Dichloroethane
0.7984386A -18.9 304.05 0.98468945.001,2-Dichloroethane
0.9589952A -16.5 304.18 1.1478185.001,1-Dichloroethylene
0.8027182A -16.4 304.18 0.96023265.00cis-1,2-Dichloroethylene
0.8345399A -16.0 304.20 0.99320255.00trans-1,2-Dichloroethylene
0.2637962A -25.7 303.72 0.35490555.001,2-Dichloropropane
0.4167278A -17.6 304.12 0.50593535.00cis-1,3-Dichloropropene
0.352077A -18.0 304.10 0.42958615.00trans-1,3-Dichloropropene
1.50411A -1.1 304.95 1.5201345.001,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
0.1110932A -8.6 304.57 0.12148585.001,4-Dioxane
0.1613009A -2.0 304.90 0.16451035.00Ethanol
0.2150543A -7.9 304.60 0.23350695.00Ethyl Acetate
1.174631A -14.4 304.28 1.372735.00Ethylbenzene
1.227083A -3.2 304.84 1.2672815.004-Ethyltoluene
0.2225014A -16.2 304.19 0.26558315.00Heptane
0.3086747A 6.1 305.30 0.29095965.00Hexachlorobutadiene
0.7452191L -11.6 304.42 0.88199185.00Hexane
Page 24 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CONTINUING CALIBRATION CHECK
EPA TO-15
S040217-CCV1
COMPOUND TYPE CCV MIN (#)CCV LIMIT (#)CCV ICAL
CONC. (ppbv)% DIFF / DRIFTRESPONSE FACTOR
STD
0.5012294A -20.6 303.97 0.63147455.002-Hexanone (MBK)
0.9010431A -6.0 304.70 0.95826045.00Isopropanol
1.604842A -16.4 304.18 1.9200895.00Methyl tert-Butyl Ether (MTBE)
0.717855A -19.0 304.05 0.88594165.00Methylene Chloride
0.5301282A -15.2 304.24 0.62524415.004-Methyl-2-pentanone (MIBK)
0.7894116A 24.4 306.22 0.63467515.00Naphthalene
0.4920936A -19.0 304.05 0.60737565.00Propene
0.683021A -6.9 304.66 0.73358725.00Styrene
0.6757008A -10.2 304.49 0.75229625.001,1,2,2-Tetrachloroethane
0.3904471A -10.2 304.49 0.43465195.00Tetrachloroethylene
0.2379245A -13.8 304.31 0.27604855.00Tetrahydrofuran
0.9224128A -15.9 304.21 1.0964045.00Toluene
0.3483024A 28.7 306.44 0.27053115.001,2,4-Trichlorobenzene
0.4580607A -18.6 304.07 0.56291675.001,1,1-Trichloroethane
0.3220804A -13.7 304.32 0.37310615.001,1,2-Trichloroethane
0.2979337A -16.9 304.15 0.35871675.00Trichloroethylene
1.33154A 2.6 305.13 1.2982285.00Trichlorofluoromethane (Freon 11)
1.229114A -9.0 304.55 1.3502655.001,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
0.9663687A 1.4 305.07 0.95318085.001,2,4-Trimethylbenzene
1.008201A -1.8 304.91 1.0263565.001,3,5-Trimethylbenzene
1.859686A -8.9 304.56 2.04035.00Vinyl Acetate
0.6194168A -8.7 304.57 0.67807755.00Vinyl Chloride
0.9134756A -8.1 309.19 0.994156610.0m&p-Xylene
0.9277503A -10.9 304.46 1.041015.00o-Xylene
* Values outside of QC limits
# Column to be used to flag Response Factor and %Diff/Drift values with an asterisk
Page 25 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,NY,ME,NHAcetone
AIHA,FL,NJ,NY,ME,NH,VABenzene
AIHA,FL,NJ,NY,ME,NH,VABenzyl chloride
AIHA,NJ,NY,ME,NH,VABromodichloromethane
AIHA,NJ,NY,ME,NH,VABromoform
AIHA,FL,NJ,NY,ME,NHBromomethane
AIHA,NJ,NY,ME,NH,VA1,3-Butadiene
AIHA,FL,NJ,NY,ME,NH,VA2-Butanone (MEK)
AIHA,NJ,NY,ME,NH,VACarbon Disulfide
AIHA,FL,NJ,NY,ME,NH,VACarbon Tetrachloride
AIHA,FL,NJ,NY,ME,NH,VAChlorobenzene
AIHA,FL,NJ,NY,ME,NH,VAChloroethane
AIHA,FL,NJ,NY,ME,NH,VAChloroform
AIHA,FL,NJ,NY,ME,NH,VAChloromethane
AIHA,NJ,NY,ME,NH,VACyclohexane
AIHA,NY,ME,NHDibromochloromethane
AIHA,NJ,NY,ME,NH1,2-Dibromoethane (EDB)
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichlorobenzene
AIHA,NJ,NY,ME,NH1,3-Dichlorobenzene
AIHA,FL,NJ,NY,ME,NH,VA1,4-Dichlorobenzene
AIHA,NY,ME,NHDichlorodifluoromethane (Freon 12)
AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,1-Dichloroethylene
AIHA,FL,NY,ME,NH,VAcis-1,2-Dichloroethylene
AIHA,NJ,NY,ME,NH,VAtrans-1,2-Dichloroethylene
AIHA,FL,NJ,NY,ME,NH,VA1,2-Dichloropropane
AIHA,FL,NJ,NY,ME,NH,VAcis-1,3-Dichloropropene
AIHA,NY,ME,NHtrans-1,3-Dichloropropene
AIHA,NJ,NY,ME,NH,VA1,2-Dichloro-1,1,2,2-tetrafluoroethane (Freon 114)
AIHA,NJ,NY,ME,NH,VA1,4-Dioxane
AIHAEthanol
AIHAEthyl Acetate
AIHA,FL,NJ,NY,ME,NH,VAEthylbenzene
AIHA,NJ4-Ethyltoluene
AIHA,NJ,NY,ME,NH,VAHeptane
AIHA,NJ,NY,ME,NH,VAHexachlorobutadiene
AIHA,FL,NJ,NY,ME,NH,VAHexane
AIHA2-Hexanone (MBK)
AIHA,NY,ME,NHIsopropanol
AIHA,FL,NJ,NY,ME,NH,VAMethyl tert-Butyl Ether (MTBE)
AIHA,FL,NJ,NY,ME,NH,VAMethylene Chloride
AIHA,FL,NJ,NY,ME,NH4-Methyl-2-pentanone (MIBK)
NY,ME,NHNaphthalene
AIHAPropene
AIHA,FL,NJ,NY,ME,NH,VAStyrene
AIHA,FL,NJ,NY,ME,NH,VA1,1,2,2-Tetrachloroethane
Page 26 of 30
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
EPA TO-15 in Air
AIHA,FL,NJ,NY,ME,NH,VATetrachloroethylene
AIHATetrahydrofuran
AIHA,FL,NJ,NY,ME,NH,VAToluene
AIHA,NJ,NY,ME,NH,VA1,2,4-Trichlorobenzene
AIHA,FL,NJ,NY,ME,NH,VA1,1,1-Trichloroethane
AIHA,FL,NJ,NY,ME,NH,VA1,1,2-Trichloroethane
AIHA,FL,NJ,NY,ME,NH,VATrichloroethylene
AIHA,NY,ME,NHTrichlorofluoromethane (Freon 11)
AIHA,NJ,NY,ME,NH,VA1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
AIHA,NJ,NY,ME,NH1,2,4-Trimethylbenzene
AIHA,NJ,NY,ME,NH1,3,5-Trimethylbenzene
AIHA,FL,NJ,NY,ME,NH,VAVinyl Acetate
AIHA,FL,NJ,NY,ME,NH,VAVinyl Chloride
AIHA,FL,NJ,NY,ME,NH,VAm&p-Xylene
AIHA,FL,NJ,NY,ME,NH,VAo-Xylene
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2020
M-MA100Massachusetts DEPMA 06/30/2020
PH-0567Connecticut Department of Publilc HealthCT 09/30/2019
10899 NELAPNew York State Department of HealthNY 04/1/2020
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2020
LAO00112Rhode Island Department of HealthRI 12/30/2019
652North Carolina Div. of Water QualityNC 12/31/2019
MA007 NELAPNew Jersey DEPNJ 06/30/2020
E871027 NELAPFlorida Department of HealthFL 06/30/2020
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2020
2011028State of MaineME 06/9/2021
460217Commonwealth of VirginiaVA 12/14/2019
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2020
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2020
25703North Carolina Department of HealthNC-DW 07/31/2020
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2020
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APPENDIX C

North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Rev. 09/2015 Page 1 of 5
Site:Former PE Valve Manufacturing
Address:1140 Sweeten Creek Road
City:Asheville
County:Buncombe
Brownfields Project Number:22081-18-11
Property and Building Characteristics
a. Provide occupancy and use information.
The property is currently undeveloped.
The property is currently undeveloped.
c. Describe the foundation construction. Include details on type, floor construction, and depth below grade.
The property is currently undeveloped.
The property is currently undeveloped.
e. Are any subslab ventilation systems or moisture barriers in place? If so, please provide details.
The property is currently undeveloped.
% of property that is covered by buildings
If an existing building is on-site, please respond to the following. Information can be provided on additional
sheets as needed. If numerous buildings are on-site, consult with your PM as only information on specific
buildings may be needed.
b. Describe the construction of the builidng including materials (e.g. wood frame, block), type and size of openings
(e.g. windows, bay doors), and height (number of stories).
BROWNFIELDS PROPERTY RECEPTOR SURVEY
This form was created to clarify and simplify preparing a receptor survey for a brownfield site. Please provide the
information requested below. Distances are measured from the site property boundary unless otherwise indicated
by the DEQ Brownfield’s Project Manager (PM).
Current Usage Proposed UsageSurface Conditions
% of property that is grassed areas
% of property that is agricultural crops
% of property that is paved NA
NA0
NA
NA
NA
NA
Size of Property (acres)
% of property that is wooded/brush
~ 1.63
~ 20
~ 80
d. Describe the HVAC system in the building. Include available details on type, equipment location, source of air
return, and design considerations (e.g. positive pressure?).
0
0
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Rev. 09/2015 Page 2 of 5
Surrounding Property Land Use
North - High
Density Single
FamilySouth -
Commercial
IndustrialEast - High
Density Single
Family
West - Commercial
Industrial
N
Y Adj W, E, & S
N,
unknown
See Figures
Same
Same
Same
Is there a basement within 1,000 ft of the Property?
Is there a residence within 1,000 ft of the Property?
Residences followed by commercial businesses
Vacant land followed by residences
Sweeten Creek Road followed by a residence and Car Dr.
automotive
Is a school or daycare center within 1,000 ft of the
Property?
Specific Land Uses of Interest Y/N *
* If numerous facilities of interest are present, their locations can be placed on a map in lieu of providing specific
addresses.
DirectionDistance
(ft)Address
Same
Please provide information on the following land uses in the vicinity of the subject site, including a map of the
surrounding areas. If specific receptors are present, please provide addresses of the facilities.
West Chapel Road followed by Sunset Cemetery
Zoning/Land Use Proposed Usage Current Use/Occupant
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Rev. 09/2015 Page 3 of 5
Utilities
Is there a septic system on-site? (Y or N) __N______
Please provide the utility providers for the subject property
a. Natural Gas ___PSNC
b. Sewer ___MSD
c. Electricity __Duke Energy
d. Other ___Stormwater
City of Asheville Water
For surrounding properties, please complete the following table with available information.
Y 5 W
Y On site W
N
Y 75 W
Y 5 W
N
N
A water main runs along the west side of Sweeten Creek Road
with a hydrant at the northwest corner of the site. Secondary
waterline within northbound lane of Sweeted Creek Road ending
near southwest corner of the site.
* If yes, please provide a map or detailed information (distance, direction, depth) of the utility in correlation with
the subject property. A map showing locations of utilities is attached. ECS Southeast, LLP observed evidence of underground and
aboveground utilities running in a North-South direction along Sweeten Creek Road. Utilities included sanitary sewer, potable water, natural gas, telephone, and electric.
Is a water line main within 100 ft of Property boundary?
Is a natural gas line main within 100 ft of the Property boundary?
Is a buried telephone/ cable main within 100 ft of the Property boundary?
Is a septic system leach field within 500 ft of the Property boundary?
Direction
Duke Energy lines are overhead lines which run along the east
side of Sweeten Creek Road.A stormwater line runs along the right-of-way of Sweeten Creek
Road with inlets at the curb, actual location unknown.
Utility/Potential Receptor
Is a buried electrical cable main within 100 ft of Property boundary?
Is a storm water pipe within 100 ft of the Property boundary?
Is a sanitary sewer within 100 ft of the Property boundary?
A sewer line transects the northern portion of the property and
runs along the east side of Sweeten Creek Road.
A natural gas line runs along the east side of Sweeten Creek
Road.
For the subject property, please provide a map of known buried utilites. If available, include depth to top,
construction material, and diameter of the utilities. In addition, please provide the following information on utilty
providers. If additional assessment is required, the public utility locators should be contacted. This information
can then be added to a site map.
Y/N *Distance
(ft)
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Rev. 09/2015 Page 4 of 5
Water Supply
What is the potable water supply for the property? Public __X____ Private ______
N
Y 720, 900 NE
27 W Chapel
Road
12 Bowen
Legacy Trail
N,
unknown
Is a private water supply well within 1,500 ft of the Property
boundary?
Is an irrigation well within 1,500 ft of the Property boundary?
AddressY/NWater Supply Wells
Please provide the following information regarding water supply wells in the vicinity of the Property. At a
minimum, a windshield survey within 1,500 ft of the property boundaries should be completed to determine if
water supply or irrigation wells may be present. Information from applicable databases can and should be
utilized; however, should not be utilized in lieu of the windshield survey. If multiple wells are present within the
requested radius, please provide a map of the well locations. If needed, please attach a separate table to list all
wells. Please note, the PM may opt for a more extensive water supply well survey if needed.
If Private, please provide details of the water supply source (i.e. well location, well construction, etc). If public,
please include the water providers name.
The purpose of this section is to provide information on the water supply for the site and surrounding areas.
Distance
(ft)Direction
Is a public water supply well within 1 mile of the Property boundary?
North Carolina Department of Environmental Quality
Division of Waste Management
Brownfields Program
Rev. 09/2015 Page 5 of 5
Surface Water & Wetlands
NA
Sweeten Creek approximately 2,000 feet east
No/No
b. List the uses of the water body.
c. What is the source of the water for the
water body?
d. What is the nature of the bottom of the
water body (e.g., rocky or concrete bottom,
drainage ways or impoundments)
If no on-site surface water features, what is the
nearest surface water body?
Are there any wetlands present on the
property? If no wetlands on-site, are wetlands
suspected on adjoining properties?
NA
NA
Response/Comments
The purpose of this section is to provide information on the presence of surface waters and/or wetlands on, or in
the vicinity of the Property.
a. Is the water body naturally developed or
man-made?NA
Are there surface water features on the
property? (If yes, please complete a. to d.)
Provide Information regarding Surface Water
and Wetlands
No
FIGURE 1
SITE LOCATION MAPFORMER PE VALVE
1140 SWEETEN CREEK ROAD
ASHEVILLE, BUNCOMBE COUNTY,
NORTH CAROLINA
ECS PROJECT NO. 49-7572-B
SOURCE:
USGS TOPOGRAPHIC MAP
ASHEVILLE, NORTH CAROLINAQUADRANGLE
DATED 1961, PHOTOREVISED 1991
SITE
FIGURE 2
AERIAL MAPFORMER PE VALVE FACILITY
1140 SWEETEN CREEK ROAD
ASHEVILLE, BUNCOMBE COUNTY,
NORTH CAROLINA
ECS PROJECT NO. 49-7572-B
SOURCE:
GOOGLE EARTH, DATED 2015
SCALE:
APPROXIMATE SITE BOUNDARY
LEGEND
= 100 FEET
FIGURE 3
RESIDENTIAL PROPERTY MAPFORMER PE VALVE FACILITY
1140 SWEETEN CREEK ROAD
ASHEVILLE, BUNCOMBE COUNTY,
NORTH CAROLINA
ECS PROJECT NO. 49-7572-B
SOURCE:
GOOGLE EARTH, DATED 2019
SCALE:
= 500 FEET
APPROXIMATE SITE BOUNDARY
LEGEND
RESIDENTIAL AREAS WITHIN 1,000 FEET
FIGURE 4
UTILITIES MAPFORMER PE VALVE FACILITY
1140 SWEETEN CREEK ROAD
ASHEVILLE, BUNCOMBE COUNTY,
NORTH CAROLINA
ECS PROJECT NO. 49-7572-B
SOURCE:
GOOGLE EARTH, DATED 2015
SCALE:
APPROXIMATE SITE BOUNDARY
LEGEND
= 100 FEET
SANITARY SEWER
WATER LINE
STORM SEWER
NATURAL GAS
FIGURE 5
OBSERVED WATER SUPPLY WELL LOCATION
MAPFORMER PE VALVE FACILITY
1140 SWEETEN CREEK ROAD
ASHEVILLE, BUNCOMBE COUNTY,
NORTH CAROLINA
ECS PROJECT NO. 49-7572-B
SOURCE:
GOOGLE EARTH, DATED 2019
SCALE:
= 500 FEET
APPROXIMATE SITE BOUNDARY
LEGEND
RESIDENTIAL AREAS WITHIN 1,000 FEET
OBSERVED WATER SUPPLY WELLS