MO-8827_40338_CA_MRP_20180316_Monitoring Report March 2018

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\I
Civil-Geotechnical-Surveying
March 16, 2018
Brett Morris
Hydrogeologist
North Carolina Department of Environmental Quality
601 East Center Avenue, Suite 301
Mooresville, NC 28115
Re: Transmittal of Monitoring Report
Six-O-One Stop
5661 Highway 601 South
Concord, Cabarrus County, North Carolina
Incident Number: 40338
Risk Classification: High
Dear Mr. Morris:
On behalf of our client, Mr. Marc Glover, operator of Six-O-One Stop, Concord
Engineering and Surveying, Inc. (CESI) has prepared the attached Monitoring Report for
the facility which is located at 5661 Highway 601 South, Concord, North Carolina.
CESI apologizes for the tardiness of the report. Should you have any questions, please
do not hesitate to contact me at [phone].
Sincerely,
Steven E. Irminger, P.E.
Senior Engineer
45 Spring Street, SW P.O. Box 268 Concord, NC 28026-0268 704-786-5404
www.cesicgs.com NC License Number C-0263

Monitoring Report
A. Site Information
1. Site Identification
Date of Report: March 16, 2018
Facility I.D.: 4753 UST Incident Number (if known): 40338
Site Name: Six-O-One Stop
Site Street Address: 5661 Highway 601 South
'City/Town: Concord Zip Code: 28025 County: Cabarrus
'Description of Geographical Data Point (e.g., diesel fill port): Center of onsite building
'Location Method (GPS, topographical map, other): Topographic Map
'Latitude (decimal degrees): 35.339270 Longitude (decimal degrees):-80.520200
2. Information about Contacts Associated with the Leaking UST System
BUST Owner: Marc Glover
Address: 5661 Highway 601 South, Concord, North Carolina 28025 Tel.: [phone]
BUST Operator: Marc Glover
Address: 5661 Highway 601 South, Concord, North Carolina 28025 Tel: [phone]
Property Owner: Misenheimer, Sydnie, Lynne
Address: 38288A Gold Hill Road, Richfield, North Carolina 28137 Tel.:
Property Occupant: Marc Glover.
Address: 5661 Highway 601 South, Concord, North Carolina 28025 Tel: [phone]
Consultant/Contractor: CESI Land Development Services
Address: P.O. Box 268 Tel: [phone]
Analytical Laboratory: Pace Analytical, Inc. State Certification No. 37712
Address: 9800 Kincey Avenue, Huntersville, North Carolina Tel: [phone]
3. Information about Release
'Date Discovered: January 17, 2014
Estimated Quantity of Release: Unknown
Cause of Release: Unknown
Source of Release (Dispenser/Piping/UST): Unknown
'Sizes and contents of UST system(s) from which the release occurred):
(3) 6,000 gallon gasoline USTs
(1) 2,000 gallon diesel UST
(1) 550 gallon kerosene UST
(1) 550 gallon used oil UST
4. Certification
I, Steven Irminger, a Professional Engineer for CESI Land Development Services, do certify that the information contained
in this report is correct and accurate to the best of my knowledge. CESI Land Development Services is licensed to practice
engineering in North Carolina. The certification number of the company or corporation is C-0263.
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Monitoring Report
Six-O-One Stop Property
March 18, 2018
Page No. 2
B. Executive Summary
No free product was observed on the on the property during the monitoring property.
During the monitoring period, groundwater samples were collected from all eight monitoring
wells and from one neighboring water supply well. Groundwater samples from the wells were
collected on January 21, 2018, and submitted to Pace Analytical, Inc. (Pace) for analysis by EPA
Method SM6200 B. The analytical results of water samples from three monitoring wells were
reported at concentrations that exceed the 15A NCAC 2L standard. One of these water samples
was reported with a benzene concentration greater than the Gross Contamination Level (GCL).
Analysis of groundwater samples collected from the remaining five monitoring wells and the
water supply well were reported to be below the sample detection limit.
Based on isoconcentration contour diagrams prepared for dissolved hydrocarbons reported in
groundwater samples collected January 21, 2018, the horizontal and vertical extent of dissolved
petroleum hydrocarbons appear similar to the distribution of dissolved petroleum hydrocarbons
reported in groundwater samples collected May 1, 2017. The data suggests that the dissolved
hydrocarbon plume is stable but rebounding because of residual contaminated soil.

Monitoring Report
Six-O-One Stop Property
March 18, 2018
Page No. 3
C. Table of Contents
A.
Site Information................................................................................................................................................1
B.
Executive Summary..........................................................................................................................................2
C.
Table of Contents.............................................................................................................................................3
D.
Site History and Characterization.....................................................................................................................5
E.
Presentation of Current Site Assessment Information......................................................................................7
F.
Free Product Removal......................................................................................................................................8
G.
Soil and Groundwater Remediation..................................................................................................................9
H.
Conclusions and Recommendations.................................................................................................................9
LIST OF FIGURES
FIGURE 1
Street Atlas
FIGURE 2
Topographic Location Map
FIGURE 3
Site Layout
FIGURE 4
Sensitive Receptor Map
FIGURE 5
Land Use Map
FIGURE 6
Soil Sample Location Map
FIGURE 7
Monitoring Well Location Map
FIGURE 8
Benzene Isoconcentration Map November 21, 2016
FIGURE 9
MTBE Isoconcentration Map November 21, 2016
FIGURE 10
Piezometric Surface Contour Diagram November 21, 2016
LIST OF TABLES
B-1
Site History — UST/AST Information
B-2
Site History — Owner/Operator Information
B-3
Soil Analytical Summary
B-4
Groundwater Analytical Summary
B-5
Receptor Information
B-6
Adjoining Parcel Ownership
B-7
Well Construction Information
B-8
NOT USED
B-9
Groundwater Elevations
B-10
Land Use

Monitoring Report
Six-O-One Stop Property
March 18, 2018
Page No. 4
LIST OF APPENDICES
APPENDIX I DENR Correspondence
APPENDIX 2 Laboratory Reports and Chain -of -Custody Records

Monitoring Report
Six-O-One Stop Property
March 18, 2018
Page No. 5
D. Site History and Characterization
Since submittal of the CSA on March 4, 2016, no changes have occurred regarding the
ownership or operation of the Property. The owner and operator information is listed on the
cover of this report and in Table B-2. All of the underground storage tanks at this Property were
removed in December 2013, and no new USTs have been installed. Information regarding the
former underground storage tanks (USTs) is provided on Table B-1. A Street Atlas showing the
location of the Property is provided as Figure 1. The Property location is shown on a portion of
a United States Geological Survey Topographical Quadrangle Map as Figure 2. The location of
the former tanks is shown on a Property Layout as Figure 3.
The tanks of this report were underground. No evidence of aboveground storage tanks were
observed or reported. No spills have been reported for the facility other than the discovery
January 17, 2014, of petroleum parameters in soil samples collected from beneath the gasoline
USTs, diesel and kerosene USTs, and the gasoline dispenser piping. The analytical results of
soil samples collected September 8, 2014, from beneath the dispensers were reported to the
DENR in a letter dated January 16, 2015.
The precise source and timing of contamination is not known. All of the USTs were observed
for evidence of corrosion or damage. No significant corrosion or damage was observed. Further
release was prevented by pump out of the USTs prior to their removal from the ground.
Removal of source material (contaminated soil) was initiated immediately following removal of
tanks. Field screening results indicated that the areas of greatest contamination were beneath the
northern ends of the gasoline USTs, the southern end of the kerosene and diesel USTs and the
elbow of the gasoline dispenser lines. No historical UST releases, non -UST releases, or off -site
releases have been reported.
Site Characteristics: The Property consists of one irregular -shaped parcel located at the
northwest quadrant of the intersection of Highway 601 south and Cold Springs Road. The area
of the parcel is approximately 2.67-acres and is improved with a gas station/convenience store/
automobile service facility. The Property location is shown on a Street Atlas as Figure 1.
According to the Cabarrus County Tax Assessor's GIS website, the Property Parcel Number is
55486177360000.
Site Vicinity Characteristics: The Property vicinity is primarily residential and commercial use
along U.S. Highway 61, with residential and agricultural land use away from the U.S. Highway
601 corridor.
LOCATION
PROPERTY
TOPOGRAPHIC
POSITION
North adjoining
5600 Cold Springs Road, residence owned
Cross gradient.
by John Plyer (5600 Clod Springs Road,
Concord, NC 28025
Northwest
5625 Highway 601 South, vacant land owned
Down gradient.
adjoining
by Estate of Elma Saunders (140 Crescent
Street, Kanna olis, NC 28081

Monitoring Report March 18, 2018
Six-O-One Stop Property Page No. 6
East adjoining
Cold Springs Road, beyond which is 5651
Down gradient.
Cold Springs Road, residence owned by
Lanney Griffin (5651 Cold Springs Road,
Concord, NC 28025).
Southeast adjoining
Cold Springs Road, beyond which is 5807
Down gradient.
Highway 601 South, residence owned by
Robert L. Price (5807 Highway 601 South,
Concord, NC 28025).
South Adjoining
Highway 601 South, beyond which is 5770
Down gradient
Highway 601 South, residence owned by
Margie Church (2767 Dale Earnhardt Blvd.,
Kanna olis, NC 28083
Southwest
Highway 601 South, beyond which is 5664
Down gradient
Adjoining
Highway 601 South, residence owned by
Dorethea Young (4906 Fenwick Place,
Concord, NC 28025
West Adjoining
Highway 601 South, beyond which is 5727
Up gradient
Old Monroe Circle, residence owned by
Karen Sarver (5727 Old Monroe Circle,
Concord, NC 28025
Water Supply: The Property is provided water from the City of Concord. One inactive potable
well was observed on the northern portion of the Property. Adjoining properties are provided
potable water by wells and by municipal water from a main located along Highway 601. All of
the adjoining residential properties appear to be connected to private wells for potable water
needs except for the adjoining southeast property, which is attached to the municipal water
supply. Information requests from the properties to the south and southwest, were not returned.
A water main owned by the City of Concord is located along Highway 601. The adjoining
properties are numbered on the Sensitive Receptor Map (Figure 4). The key to the numbered
locations is provided in Table B-5.
Topography. CESI obtained a copy of the USGS 7.5-minute topographic map, Concord, North
Carolina Quadrangle, dated 1991. A copy of a portion of the topographic map showing the
Property location is provided on Figure 2. The elevation of the Property is approximately 630
feet above mean sea level (msl). Based upon the topographic contours observed on the USGS
topographic contour map, the Property is located on a southwest to northeast trending ridge. The
slope is generally downward toward the east although the extreme western portion of the
Property slopes toward the northwest.
Vegetation: The Property consists of the building footprint, asphalt pavement, two canopies, a
propane AST, and grass turf.
Surface Water: No surface water was observed on the Property. The nearest surface water
indicated on the topographic map is an unnamed stream located approximately 1,000 feet
northwest of the Property.

Monitoring Report
Six-O-One Stop Property
March 18, 2018
Page No. 7
Wells: One inactive potable well was observed on the northern portion of the Property.
Buildings: The Property is improved with one single -story commercial building. The building
is occupied by a convenience store and two automobile service bays. No other USTs or ASTs
(other than one propane AST) were observed onsite. The Property Layout is shown as Figure 3.
Surface Cover: The majority of the Property surface is covered by the building, asphalt parking
lot, and turf.
Soil Type: According to the USDA web -based soil survey of Cabarrus County, the surficial Soil
at the Property is composed of Urban Land Complex.
List of all Prior Reports Submitted:
UST Closure Report; CESI; April 4, 2014
Limited Site Assessment; CESI; May 2, 2015
Comprehensive Site Assessment; CESI; March 2, 2016
Monitoring Report; CESI; January 16, 2016
Plume Stability Report; CESI; July 10, 2017
Summarize implementation of the remedial plan proposed in the CAP.
A CAP has not been prepared for the site.
E. Presentation of Current Site Assessment Information
On January 21, 2018, CESI personnel measured the depth to water using a washed interface probe
capable of measuring phase separated liquids as thin as 0.01 feet. No free product was encountered
during the reporting period.
A groundwater sample was collected from water supply well 2 on January 21, 2018. The water
sample were collected from the hose bib nearest to the onsite well and not through a hose. The
water was allowed to flow for five minutes prior to collection of a sample directly into the
laboratory supplied sample containers. The water samples were analyzed for volatile organic
compounds using EPA Method SM 6200B. Based on the analytical report, no parameters were
reported above the sample detection limit. A copy of the laboratory report and chain of custody
record is provided in Appendix 2. CESI attempted to retrieve a water sample from the onsite water
supply well (well 1) but was unable to lower a bailer because of interference from the downhole
pump cable and discharge line. This well is disconnected from the electrical supply and has
reportedly not been used for many years. The owner of water well number 3 refused CESI access to
the water well. The owner of water well number 4 stated that the well is not used and is not
accessible.

Monitoring Report March 18, 2018
Six-O-One Stop Property Page No. 8
On January 21, 2018, CESI personnel collected groundwater samples from wells MW-1 to MW-
8. The wells were purged of three casing volumes or to dryness using a new polyethylene
bailer. The wells were allowed to recover and a water sample was then collected for laboratory
analysis. The water samples were collected into laboratory supplied sample bottles and
immediately placed on ice. The samples were transported to Pace using Chain -of -Custody
protocol. CESI requested that Pace analyze the water samples for VOCs using EPA Method
SM6200B. The results of the groundwater analyses are summarized on Table B-4. A copy of
the laboratory report and chain -of -custody record is provided in Appendix 3. Analysis of
groundwater samples from the monitoring wells revealed gasoline parameters greater than the
North Carolina Administrative Code (NCAC) 15A 2L standard in wells MW-I, MW-2, MW-7,
MW-8. The benzene concentration in well MW-2 was reported at a concentration greater than
the GCL for benzene. None of the other tested parameters exceeded GCL's. The analytical
results for benzene and MTBE were posted on a Site Layout and contoured. The resulting
isoconcentration contour diagrams for benzene and MTBE are provided as Figure 8 and Figure
9, respectively. Based on a comparison of prior isoconcentration contour diagrams and those
prepared from the January 21, 2018, sampling event, the dissolved hydrocarbon plume appears to
be stable. However, concentrations increased in several wells indicating that rebound from
adsorbed hydrocarbons is occurring.
According to the Geologic Map of North Carolina 1985, the Property is located in the Piedmont
Physiographic Province. The dominant rocks in this region are composed mainly of
metamorphosed mudstone and argillite of the Cenozoic Era. The rocks are thin to thick bedded,
with bedding planes and angular cleavage common and occur interbedded with metasandstone,
metaconglomerate, and metavolcanic rock. This area is geologically characterized by a thin
layer of red Saprolite over fractured bedrock. Saprolite is defined as soft, earthy, clay -rich,
thoroughly decomposed rock formed in place by chemical weathering of igneous and
metamorphic rocks. The term is applied to any unconsolidated residual material underlying the
soil and grading to bedrock below. Bedrock was not observed at the surface in the vicinity of
the Property. Drilling of monitoring wells encountered a blocky, well consolidated mudstone
from approximately 12-feet below grade to the maximum depth penetrated of 50-feet below
grade.
Depth to groundwater: Depth to groundwater measurements at the site revealed depth to water
approximately 23 feet below grade. A summary of the water level data is provided on Table B-9.
The piezometric surface contour diagram from data recorded January 21, 2018, is toward the east.
The piezometric surface contour diagram is provided as Figure 10.
No free product has been observed onsite. Based on the groundwater analytical results of samples
collected January 21, 2018, the areal extent of dissolved hydrocarbons appears to be defined except
to the south for benzene and MTBE and to the west for MTBE. However, based on the low
concentrations on the perimeter wells, it appears that the dissolved hydrocarbon plume has not
migrated offsite. The vertical extent of impact has been defined in the deep screen well MW-8.
F. Free Product Removal
No free product has been observed at the site.

Monitoring Report
Six-O-One Stop Property
March 18, 2018
Page No. 9
G. Soil and Groundwater Remediation
No remediation has been implemented at this site.
H. Conclusions and Recommendations
Concentrations of dissolved benzene persist at levels above GCLs in well MW-2. Interviews
with the owners of water supply wells 2 and 3 on January 21, 2018, stated that they did not want
to connect to municipal water.
CESI recommends preparation of a full scale CAP designed to reduce dissolved groundwater
concentrations to below the 2L standard.

FIGURES

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Site Name: Highway Six O One Stop
5661 South Highway 601
CESI Land Development Services Concord, NC 28025
Project Number: 131148

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Site Name: Highway Six O One Stop
5661 South Highway 601
CESI Land Development Services Concord, NC 28025
Project Number: 131148

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Site Name: Highway Six O One Stop
5661 South Highway 601
CESI Land Development Services Concord, NC 28025
Project Number: 131148

4
LEGEND
2
Receptor ID (Refer to Table B5)
Subject Property
FIGURE 4 SENSITIVE RECEPTORS Not To Scale N T
Site Name: Highway Six O One Stop
5661 South Highway 601
CESI Land Development Services Concord, NC 28025
Project Number: 131148

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FIGURE 5 LAND USE Not To Scale N ?
Site Name: Highway Six O One Stop
CESI Land men Develo t Services 5661 South Highway 601
p Concord, NC 28025
Project Number: 131148

TABLES

Appendix B
Reporting Tables
Table B-1: Site History — UST/AST System and Other Release Information
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop
Description
Was release
UST ID
Current/Last
Previous
Capacity (in
Construction
Tank
of Associated
Date Tank
Status of
associated
Number
Contents *
Contents *
gallons)
Details **
Dimensions
Piping and
Installed
UST ***
with the UST
Pumps
System?
1
Gasoline
None
6,000
Single wall
16'L 8'D
Single wall
1961
Removed
Yes
steel
steel
2013
2
Gasoline
None
6,000
Single wall
16'L 8'D
Single wall
1961
Removed
Yes
steel
steel
2013
Add additional records as necessary
AST ID
Number
Current/Last
Contents *
Previous
Contents *
Capacity (in
gallons)
Construction
Details **
Tank
Dimensions
Description
of Associated
Piping and
Pumps
Date Tank
Installed
Status of
AST ***
Was release
associated
with the AST
System?
Add additional records as necessary
FIncident
Number
Material
Released
Date of
Release
Description of Release
Add additional records as necessary
* Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non -halogenated or halogenated solvents, etc.
** Fiberglass (single- or double -walled), steel (single- or double -walled), steel with FRP (single- or double -walled), steel with liner, other, unknown.
*** Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal (specify
date)
Change 2

Table B-1: Site History — UST/AST System and Other Release Information
Revision Date: 3/2/2014 Incident Number and Name: 40338 Six O One Stop
Description
Was release
UST ID
Current/Last
Previous
Capacity (in
Construction
Tank
of Associated
Date Tank
Status of
associated
Number
Contents *
Contents *
gallons)
Details **
Dimensions
Piping and
Installed
UST ***
with the UST
Pumps
System?
3
Gasoline
None
6,000
Single wall
16'L 8'D
Single wall
1961
Removed
Yes
steel
steel
2013
4
Kerosene
None
550
Single wall
6'L 4'D
Single wall
1978
Removed
Yes
steel
steel
2013
Add additional records as necessary
AST ID
Number
Current/Last
Contents *
Previous
Contents *
Capacity (in
gallons)
Construction
Details **
Tank
Dimensions
Description
of Associated
Piping and
Pumps
Date Tank
Installed
Status of
AST ***
Was release
associated
with the AST
System?
Add additional records as necessary
FIncident
Number
Material
Released
Date of
Release
Description of Release
Add additional records as necessary
* Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non -halogenated or halogenated solvents, etc.
** Fiberglass (single- or double -walled), steel (single- or double -walled), steel with FRP (single- or double -walled), steel with liner, other, unknown.
*** Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal (specify
date)

Table B-1: Site History — UST/AST System and Other Release Information
Revision Date: 3/2/2014 Incident Number and Name: 40338 Six O One Stop
Description
Was release
UST ID
Current/Last
Previous
Capacity (in
Construction
Tank
of Associated
Date Tank
Status of
associated
Number
Contents *
Contents *
gallons)
Details **
Dimensions
Piping and
Installed
UST ***
with the UST
Pumps
System?
5
Diesel
None
2,000
Single wall
13.5'L 5'D
Single wall
1978
Removed
Yes
steel
steel
2013
6
Used oil
None
550
Single wall
6'L 4'D
Single wall
1985
Removed
Yes
steel
steel
2014
Add additional records as necessary
AST ID
Number
Current/Last
Contents *
Previous
Contents *
Capacity (in
gallons)
Construction
Details **
Tank
Dimensions
Description
of Associated
Piping and
Pumps
Date Tank
Installed
Status of
AST ***
Was release
associated
with the AST
S stem?
Add additional records as necessary
Incident
Number
Material
Released
Date of
Release
Description of Release
Add additional records as necessary
* Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non -halogenated or halogenated solvents, etc.
** Fiberglass (single- or double -walled), steel (single- or double -walled), steel with FRP (single- or double -walled), steel with liner, other, unknown.
* * * Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal (specify
date)

Appendix B
Reporting Tables
Table B-1: Site History — UST/AST System and Other Release Information
Revision Date: Incident Number and Name:
UST ID
Number
Current/Last
Contents *
Previous
Contents *
Capacity (in
gallons)
Construction
Details **
Tank
Dimensions
Description
of Associated
Piping and
Pumps
Date Tank
Installed
Status of
UST ***
Was release
associated
with the UST
System?
Add additional records as necessary
AST ID
Number
Current/Last
Contents *
Previous
Contents *
Capacity (in
gallons)
Construction
Details **
Tank
Dimensions
Description
of Associated
Piping and
Pumps
Date Tank
Installed
Status of
AST ***
Was release
associated
with the AST
System?
Add additional records as necessary
FIncident
Number
Material
Released
Date of
Release
Description of Release
Add additional records as necessary
* Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non -halogenated or halogenated solvents, etc.
** Fiberglass (single- or double -walled), steel (single- or double -walled), steel with FRP (single- or double -walled), steel with liner, other, unknown.
*** Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal (specify
date)
Change 2

Appendix B
Reporting Tables
Table B-1: Site History — UST/AST System and Other Release Information
Revision Date: Incident Number and Name:
UST ID
Number
Current/Last
Contents *
Previous
Contents *
Capacity (in
gallons)
Construction
Details **
Tank
Dimensions
Description
of Associated
Piping and
Pumps
Date Tank
Installed
Status of
UST ***
Was release
associated
with the UST
System?
Add additional records as necessary
AST ID
Number
Current/Last
Contents *
Previous
Contents *
Capacity (in
gallons)
Construction
Details **
Tank
Dimensions
Description
of Associated
Piping and
Pumps
Date Tank
Installed
Status of
AST ***
Was release
associated
with the AST
System?
Add additional records as necessary
FIncident
Number
Material
Released
Date of
Release
Description of Release
Add additional records as necessary
* Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non -halogenated or halogenated solvents, etc.
** Fiberglass (single- or double -walled), steel (single- or double -walled), steel with FRP (single- or double -walled), steel with liner, other, unknown.
*** Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal (specify
date)
Change 2

Appendix B
Reporting Tables
Table B-1: Site History — UST/AST System and Other Release Information
Revision Date: Incident Number and Name:
UST ID
Number
Current/Last
Contents *
Previous
Contents *
Capacity (in
gallons)
Construction
Details **
Tank
Dimensions
Description
of Associated
Piping and
Pumps
Date Tank
Installed
Status of
UST ***
Was release
associated
with the UST
System?
Add additional records as necessary
AST ID
Number
Current/Last
Contents *
Previous
Contents *
Capacity (in
gallons)
Construction
Details **
Tank
Dimensions
Description
of Associated
Piping and
Pumps
Date Tank
Installed
Status of
AST ***
Was release
associated
with the AST
System?
Add additional records as necessary
FIncident
Number
Material
Released
Date of
Release
Description of Release
Add additional records as necessary
* Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non -halogenated or halogenated solvents, etc.
** Fiberglass (single- or double -walled), steel (single- or double -walled), steel with FRP (single- or double -walled), steel with liner, other, unknown.
*** Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal (specify
date)
Change 2

Appendix B
Reporting Tables
Table B-2: Site History - UST/AST Owner/Operator and Other Responsible
Party Information
Revision Date: 01/16/2017 Incident Number and Name: 40338 Six O One Stop
UST ID Number
00-0-0000004753
Facility ID Number
4753
Name of Owner
Dates of Operation
(mm/dd/yy to mm/dd/yy)
Six O One Station, LLC
Current
Street Address
304 S. Second Street
City
State
Zip
Telephone Number
Albemarle
NC
28001
Name of Operator
Dates of Operation
(mm/dd/yy to mm/dd/yy)
Marc Glover
Current
Street Address
5661 Highway 601 S.
City
State
Zip
Telephone Number
Concord
NC
28025
704-786-0600
Incident Number
Name of Other Responsible Party
Dates of Release(s)
(mm/dd/yy to mm/dd/yy)
Street Address
City
State
Zip
Telephone Number
Add additional records for all owners, operators and responsible parties as necessary.

Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop
Appendix B
Reporting Tables
Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
8015
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
(m/dd/yy)
(eg.
(ft BGS)
(Closure
Tank pit
, 20Day,
1)
LSA,
x
etc.)Tank
H
l
12/12/13
gas tank
11
Closure
266
North
Tank 1
12/12/13
gas tank
1 1
Closure
8.9
South
Tank 2
12/13/13
gastank
11
Closure
11.7
North
Tank 2
12/13/13
gastan
11
Closure
<6.1
South
k
Minimum Reporting Limit (mg/kg)
Varies
Soil to groundwater MSCC (mg/kg)
10
Residential MSCC (mg/kg)
10
Industrial/Commercial MSCC (mg/kg)
10
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
Change 2

Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop
Appendix B
Reporting Tables
Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
8015
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
(m/dd/yy)
(eg.
(ft BGS)
(Closure
Tank pit
, 20Day,
1)
LSA,
x
etc.)Tank
H
12/13/13
gas tank
11
Closure
132
North
Tank 3
12/13/13
gastank
11
Closure
<6.6
South
Minimum Reporting Limit (mg/kg)
Varies
Soil to groundwater MSCC (mg/kg)
10
Residential MSCC (mg/kg)
10
Industrial/Commercial MSCC (mg/kg)
10
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
Change 2

Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop
Appendix B
Reporting Tables
Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
VPH
VPH
VPH
8260
8260
8260
8260
8260
8260
8260
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
o
�,
(m/dd/yy)
(eg.
(ft BGS)
(Closure00
Tank pit
20Day,
o
CIA
o
;2
o~
°
�
y
y
1)
LSA,
U
�,
U
o,
U
of
�
o
o.
p.
°
u,
a�
a�
etc.
o
U
0
U
0
U
y
o
N
cn
East side
E1
12/13/13
gas UST
16
Closure
284
683
231
1.430
7.420
1.060
1.310
2.910
31.800
12.200
pit
West side
E2
12/13/13
gas UST
16
Closure
43.2
85.9
57.6
<0.777
2.230
<0.777
<0.777
1.540
13.400
3.290
pit
East
East side
12/16/13
diesel
11
Closure
241
681
397
1.360
1.460
<0.634
0.720
3.460
34.000
4.110
Wall
UST pit
South side
E3
12/13/13
gas UST
16
Closure
106
512
209
<1.290
6.110
<1.290
<1.290
3.530
28.400
10.400
pit
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
68
540
31
4.3
4.9
1.7
0.12
0.16
8.5
8.3
Residential MSCC (mg/kg)
939
1500
469
626
1560
1564
100
313
782
782
Industrial/Commercial MSCC (mg/kg)
24528
40000
12264
16350
40000
40880
4000
8176
20440
20440
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
10 Change 2

Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop
Appendix B
Reporting Tables
Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
8260
8270
8260
8260
8260
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
N
(m/dd/yy)
(eg.
(ft BGS)
(Closure
Tank pit
20Day,
1)
LSA,
r"
88
etc.)
o
°
F�
East side
E1
12/13/13
gas UST
16
Closure
39.700
36.900
2.850
<0.712
<0.712
pit
West side
E2
12/13/13
gas UST
16
Closure
8.390
7.490
0.905
1.910
<0.790
pit
East
East side
12/16/13
diesel
11
Closure
5.100
5.100
<0.634
1.920
<0.634
Wall
UST pit
South side
E3
12/13/13
gas UST
16
Closure
38.700
32.600
6.110
3.180
3.110
pit
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
4.6
4.6
4.6
1.7
4.3
Residential MSCC (mg/kg)
3129
3129
3129
626
1200
Industrial/Commercial MSCC (mg/kg)
81760
81760
81760
16350
32000
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
11 Change 2

Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop
Appendix B
Reporting Tables
Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
VPH
VPH
VPH
8260
8260
8260
8260
8260
8260
8260
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
o
�,
(m/dd/yy)
(eg.
(ft BGS)
(Closurecc
Tank pit
20Day,
o
CIA
o
;2
o~
°
�
y
y
1)
LSA,
U
v,
U
o,
U
of
�
o
o.
u
°
u,
c,
c,
etc.
o
U
0
U
0
U
y
o
N
cn
South
South side
12/16/13
diesel
11
Closure
50.1
133
38.2
1.570
3.530
0.880
0.959
1.630
14.7
6.930
Wall
UST pit
North side
E4
12/13/13
gas UST
16
Closure
244
579
278
0.846
4.930
<0.760
<0.760
2.590
16.600
5.760
pit
Bottom
E5
12/13/13
gas UST
18
Closure
147
1260
<0.251
8.910
1.260
1.760
7.380
48.500
14.600
pit
North
North side
12/16/13
diesel
11
Closure
<2.5
<2.5
<2.5
<0.0049
<0.0049
<0.0049
<0.0049
<0.0049
<0.0049
<0.0049
Wall
UST pit
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
68
540
31
4.3
4.9
1.7
0.12
0.16
8.5
8.3
Residential MSCC (mg/kg)
939
1500
469
626
1560
1564
100
313
782
782
Industrial/Commercial MSCC (mg/kg)
24528
40000
12264
16350
40000
40880
4000
8176
20440
20440
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
12 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
8260
8260
8260
8260
8260
8260
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
N
(m/dd/yy)
(eg.
(ft BGS)
(Closure
Tank pit
20Day,
;
C
1)
LSA,
r"
46
°
etc.)
>
u
�,
South
South side
12/16/13
diesel
11
Closure
5.650
5.650
<0.822
3.600
<0.822
<0.822
Wall
UST pit
North side
E4
12/13/13
gas UST
16
Closure
29.500
22.300
7.190
2.500
<0.760
<0.760
pit
North side
E5
12/13/13
gas UST
18
Closure
65.500
46.900
18.600
4.770
10.800
1.110
pit
North
North side
12/16/13
diesel
11
Closure
<0.0049
<0.0049
<0.0049
<0.0049
<0.0049
<0.0049
Wall
UST pit
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
4.6
4.6
4.6
1.7
4.3
0.0056
Residential MSCC (mg/kg)
3129
3129
3129
626
1200
18
Industrial/Commercial MSCC (mg/kg)
81760
81760
81760
16350
32000
164
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
13 Change 2

Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop
Appendix B
Reporting Tables
Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
VPH
VPH
VPH
8260
8260
8260
8260
8260
8260
8260
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
o
�,
(m/dd/yy)
(eg.
(ft BGS)
(Closure00
Tank pit
20Day,
o
CIA
o
;2
o~
°
�
y
y
1)
LSA,
U
U
U
o
u
c,
c,
etc.
o
U
0
U
0
U
�
�
o
• ;
�
N • �,
cn • �,
West
West side
12/16/13
diesel
11
Closure
<2.2
2.6
<0.0045
<0.0045
<0.0045
<0.0045
<0.0045
<0.0045
<0.0045
<0.0045
Wall
UST pit
Gas
L1
12/31/13
dispenser
3.5
Closure
236
764
307
3.220
10.300
1.460
1.540
9.650
53.900
16.900
line
Gas
L2
12/31/13
dispenser
3.5
Closure
<41.7
754
341
4.370
8.050
<3.340
<3.340
14.100
66.900
20.400
line
Gas
L3
12/31/13
dispenser
3.5
Closure
69.5
237
83.4
0.0136
0.0177
0.0086
0.0099
0.0235
0.192
0.0628
line
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
68
540
31
4.3
4.9
1.7
0.12
0.16
8.5
8.3
Residential MSCC (mg/kg)
939
1500
469
626
1560
1564
100
313
782
782
Industrial/Commercial MSCC (mg/kg)
24528
40000
12264
16350
40000
40880
4000
8176
20440
20440
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
14 Change 2

Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop
Appendix B
Reporting Tables
Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
8260
8270
8270
8260
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
N
(m/dd/yy)
(eg.
(ft BGS)
(Closure
Tank pit
20Day,
;
w
1)
LSA,
46
etc.)
West
West side
12/16/13
diesel
11
Closure
<0.0045
<0.0045
<0.0045
<0.0045
<0.0045
<0.0045
0.0141
Wall
UST pit
Gas
L1
12/31/13
dispenser
3.5
Closure
47.000
44.300
2.690
7.080
<1.410
<1.410
<1.410
line
Gas
L2
12/31/13
dispenser
3.5
Closure
56.600
40.500
16.100
7.520
3.590
<3.340
<3.340
line
Gas
L3
12/31/13
dispenser
3.5
Closure
0.125
0.0791
0.0462
0.0351
<0.0054
<0.0054
<0.0054
line
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
4.6
4.6
4.6
1.7
4.3
0.0056
0.091
Residential MSCC (mg/kg)
3129
3129
3129
626
1200
18
350
Industrial/Commercial MSCC (mg/kg)
81760
81760
81760
16350
32000
164
3100
Indicate detection limit for contaminants when analyzed, but not detected
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram
(e.g., < 1, 10, 42)
Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
15 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
VPH
VPH
VPH
8260
8260
8260
8260
8260
8260
8260
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
o
�,
(m/dd/yy)
(eg.
(ft BGS)
(Closurecc
Tank pit
20Day,
o
CIA
o
;2
o~
°
�
y
y
1)
LSA,
U
v,
U
o,
U
of
�
o
Q
u
°
u,
c,
c,
etc.
o
U
0
U
0
U
y
o
N
cn
Gas
L4
12/31/13
dispenser
12
Closure
196
451
118
2.260
10.300
1.520
<1.370
2.490
27.900
8.790
line
Gas
L5
12/31/13
dispenser
12
Closure
209
346
102
0.158
1.090
0.342
0.262
0.397
0.201
0.556
line
Gas
L6
12/31/13
dispenser
12
Closure
209
607
180
<2.810
7.770
<2.810
<2.810
3.240
23.000
8.090
line
East Wall
Bottom
12/16/13
diesel
14
Closure
<2.2
2.6
<2.2
<0.0045
<0.0045
<0.0045
<0.0045
<0.0045
<0.0045
<0.0045
(Bottom)
UST pit
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
68
540
31
4.3
4.9
1.7
0.12
0.16
8.5
8.3
Residential MSCC (mg/kg)
939
1500
469
626
1560
1564
100
313
782
782
Industrial/Commercial MSCC (mg/kg)
24528
40000
12264
16350
40000
40880
4000
8176
20440
20440
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
s Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg.
Results
milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
mg/kgResidential MSCC.
16 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
8260
8270
8270
8260
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
N
(m/dd/yy)
(eg.
(ft BGS)
(Closure
�
Tank pit
20Day,
1)
LSA,
N
etc.)
o
H
Gas
L4
12/31/13
dispenser
12
Closure
59.500
42.300
17.300
5.570
8.270
<1.370
<1.370
<1.370
line
Gas
L5
12/31/13
dispenser
12
Closure
1.040
0.898
0.142
0.807
0.388
0.0093
<0.0055
0.115
line
Gas
L6
12/31/13
dispenser
12
Closure
37.500
27.000
10.400
4.560
2.940
<2.810
<2.810
<2.810
line
East Wall
Bottom
12/16/13
diesel
14
Closure
<0.009
<0.009
<0.0045
<0.0045
<0.0045
<0.0045
0.0141
<0.0045
(Bottom)
UST pit
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
4.6
4.6
4.6
1.7
4.3
0.0056
0.091
4.3
Residential MSCC (mg/kg)
3129
3129
3129
626
1200
18
350
626
Industrial/Commercial MSCC (mg/kg)
81760
81760
81760
16350
32000
164
3100
16350
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
s Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg.
Results
milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
mg/kgResidential MSCC.
17 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
VPH x
VPHa
VPHc
EPHb
EPHy
EPHd
8260
8260
8260
8260
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
(m/dd/yy)
(eg.
(ft BGS)
(Closure
Tank pit
20Day,
00
N
U
O
U
oo
U
D
U
N
U
1)
LSA,
�.
U
U
U
U
U
etc.)
U
U
WOttom
Used
1/9/14
8
Closure
<1.3
5.4
3.0
<11.7
<11.7
<11.7
16.1
14.7
0.453
0.583
O 1 UST
Used
W°t
1/9/14
7
Closure
<2.8
<2.8
<2.8
<13.6
<13.6
<13.6
16.4
16.4
<4.470
<4.470
Oil UST
Used
WO East
1/9/14
7
Closure
<1.7
<1.7
<1.7
<13.1
<13.1
<13.1
14.8
14.8
<0.431
<0.431
Oil UST
WOrth
1/9/14
Used
7
Closure
<1.8
25.2
14.8
14.2
32.7
<11.5
39.4
26.3
<3.800
<3.800
O 1 UST
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
Immob
68
540
31
ile
540
31
39
290
Residential MSCC (mg/kg)
939
1500
469
31000
1500
469
88
620
Industrial/Commercial MSCC (mg/kg)
24528
40000
12264
810000
40000
12264
780
16400
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg. Groundwater MSCC. Red shading indicates exceedance of
mg/kg =milligrams per kilogram Residential MSCC.
18 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
VPH
VPH
VPH
EPH
EPH
EPH
8260
8260
8260
8260
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
(m/dd/yy)
(eg.
(ft BGS)
(Closure
Tank pit
20Day,
1
o
1)
LSA,
°
¢
N
etc.)
°'
"
7
WOttom
Used
1/9/14
Oil UST
8
Closure
3.5
0.437
<0.0029
<0.0029
Used
W°t
1/9/14
Oil UST
7
Closure
66.4
<4.470
0.439
<0.0073
Used
WO East
1/9/14
7
Closure
10.1
<0.431
0.0662
<0.0031
Oil UST
Used
N O h
1/9/14
Oil UST
7
Closure
46.2
<3.800
0.077
0.0035
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
270
3.3
24
0.16
270
0.35
Residential MSCC (mg/kg)
469
626
14000
313
400
0.88
Industrial/Commercial MSCC (mg/kg)
12264
16350
360000
8176
400
8
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg. Yellow shading indicates exceedance of Soil to
mg/kg =milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
19 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
8015
8015
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
(m/dd/yy)
(eg.
(ft BGS)
(Closure
O
O
Tank pit
, 20Day,
Q
1)
LSA,
x
x
etc.)
a
a
Tank 5
Dies12/16/13
8
Closure
1210
10.7
South
UST
Tank 4
12/16/13
Kero
6
Closure
<5.6
<6.7
North
UST
Tank 4
12/16/13
KeroUST
6
Closure
200
19.2
South
Tank 5
12/16/13
Diesel
8
Closure
<5.9
<7.1
North
Minimum Reporting Limit (mg/kg)
10
10
Soil to groundwater MSCC (mg/kg)
10
10
Residential MSCC (mg/kg)
10
10
Industrial/Commercial MSCC (mg/kg)
10
10
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg. Groundwater MSCC. Red shading indicates exceedance of
mg/kg =milligrams per kilogram Residential MSCC.
20 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
8015
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
(m/dd/yy)
(eg.
(ft BGS)
(Closure
Tank pit
, 20Day,
1)
LSA,
x
etc.)
H
Displ
09/08/14
dispenser
1-2
LSA
1,510
Disp2
09/08/14
dispenser
1-2
LSA
759
Disp3
09/08/14
dispenser
1-2
LSA
6,110
Disp4
09/08/14
dispenser
1 1-2
LSA
909
Minimum Reporting Limit (mg/kg)
10
Soil to groundwater MSCC (mg/kg)
10
Residential MSCC (mg/kg)
10
Industrial/Commercial MSCC (mg/kg)
10
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
s Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg.
Results
milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
mg/kgResidential MSCC.
21 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
8015
Contaminant of Concern 4
0
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
U
U
eq
U
(m/dd/yy)
(eg.
(ft BGS)
(Closure
0
c
e°e
5
Tank pit
20Day,
C7
U
U
U
^
1)
LSA,
a
io
E o
etc.)
E-O
W
%
I tN
0
Disp5
09/08/14
dispenser
1-2
LSA
172
NA
NA
NA
NA
NA
NA
NA
Diesel E
09/08/14
Diesel
3-5
Closure
NA
52.0
<23.8
50.1
458
614
5'
tank pit
Diesel E
09/08/14
Diesel
tank
8-10
Closure
NA
25.5
<11.6
22.7
706.5
419.7
<384
<384
10,
pit
Diesel N
09/08/14
Diesel
3-5
Closure
NA
<12.4
17.4
<12.4
<14.9
<14.9
<410
<410
5'
tank pit
Minimum Reporting Limit (mg/kg)
10
10
10
10
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
Immob
10
NR
ile
NR
540
31
4
3600
Residential MSCC (mg/kg)
1120000
10
NR
31000
NR
1500
469
63000
Industrial/Commercial MSCC (mg/kg)
320000
163500
10
NR
810000
NR
40000
12264
00
1 0
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg. Yellow shading indicates exceedance of Soil to
mg/kg =milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
22 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
Contaminant of Concern 4
N
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
U
U
U
(m/dd/yy)
(eg.
(ft BGS)
(Closure
4,
e°e
Tank pit
20Day,
U
U
U
^
1)
LSA,
x
x
x
io
io
etc.)
a
a
+
+
Diesel N
09/08/14
Diesel
8-10
Closure
<10.9
<10.9
<10.9
<13.4
<13.4
<361
<361
10,
tank pit
Diesel S
09/08/14
Diesel
3-5
Closure
<11.3
<11.3
<11.3
<144.3
<49.5
<372
<372
5'
tank pit
Diesel S
09/08/14
Diesel
tank
8-10
Closure
<12.3
<12.3
<12.3
<145.3
<50.5
<405
<405
10,
pit
Kerosene
09/08/14
Diesel
3-5
Closure
<12.4
<12.4
<12.4
indeter
indeter
<409
<409
W 5,
tank pit
minate
minate
Minimum Reporting Limit (mg/kg)
10
10
10
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
NR
i�ob
NR
540
31
4
3600
l
Residential MSCC (mg/kg)
0000
NR
31000
NR
1500
469
63000
0
Industrial/Commercial MSCC (mg/kg)
320000
163500
NR
810000
NR
40000
12264
00
0
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg. Yellow shading indicates exceedance of Soil to
mg/kg =milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
23 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
�
8015
8015
Contaminant of Concern 4
N
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
U
U
U
(m/dd/yy)
(eg.
(ft BGS)
(Closure
4,
e°e
Tank pit
20Day,
U
U
U
^
1)
LSA,
x
x
x
io
io
etc.)
a
a
+
+
C�
U
--
N
Kerosene
Diesel
Indeter
Indeter
W 10,
09/08/14
tank pit
8_10
Closure
<12.6
<12.6
<12.6
minate
minate
<414
<414
Center
09/08/14
Diesel
8_10
Closure
<11.0
<11.0
<11.0
<13.6
<13.2
<364
<363
10,
tank pit
Minimum Reporting Limit (mg/kg)
10
10
10
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
Immob
NR
NR
540
31
4
3600
ile
Residential MSCC (mg/kg)
0000
NR
31000
NR
1500
469
63000
0
Industrial/Commercial MSCC (mg/kg)
320000
163500
NR
810000
NR
40000
12264
00
0
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
Results must be reported in mg/kg.
mg/kg =milligrams per kilogram Yellow shading indicates exceedance of Soil to
Groundwater MSCC. Red shading indicates exceedance of
Residential MSCC.
24 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
Contaminant of Concern 4
o
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
U
(m/dd/yy)
(eg.
(ft BGS)
(Closure
Tank pit
20Day,
00
o
�'
o
1)
LSA,
etc.)
U
U
1 U
M
10/28/14
Pas tank
24-26
LSA
<2.8
3.5
<2.8
6.8
<22.2
261
MW-2
Gas
10/28/14
dispenser
18-20
LSA
<3.1
3.3
<3.1
9.5
<22.7
18-20
lines
MW-3
10/28/14
Diesel
20-22
LSA
<11.5
<11.5
<11.5
<5.7
20-22
tank pit
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
68
540
31
91
0.02
Residential MSCC (mg/kg)
939
1500
12264
350000
85
Industrial/Commercial MSCC (mg/kg)
310000
24528
40000
469
763
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
s Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg.
Results
milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
mg/kgResidential MSCC.
25 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
Contaminant of Concern 4
y
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
(m/dd/yy)
(eg.
(ft BGS)
(Closure00
o
N
Tank pit
20Day,
o
CIA
o
Q
c
1
LSA
U
U
U
o
NAl
o
y
etc.
U
U
U
i
ZE�
SB-2
10/7/15
8-10
CSA
<1.4
<1.4
<1.4
70.9
SB-7
10/7/15
8-10
CSA
<1.5
<1.5
<1.5
3.8
3.2
6.4
3.3
8.7
6.7
SB-7
10/7/15
13-15
CSA
8.1
3.3
6.2
SB-4
10/7/15
3-5
CSA
<1.3
<1.3
<1.3
<62
<3.1
<3.1
5.7
<3.1
7.4
<6.2
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
68
540
31
24
0.0056
0.37
4.9
91
0.16
4.6
Residential MSCC (mg/kg)
939
1500
12264
14000
18
156
1560
350000
313
3129
Industrial/Commercial MSCC (mg/kg)
3310000
24528
40000
469
360000
164
4088
40000
8176
81760
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
s Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg.
Results
milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
mg/kgResidential MSCC.
26 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
N
o
(m/dd/yy)
(eg.
(ft BGS)
(Closure
N
4
U
Tank pit
20Day,
o
r.
'_2
a
°
1
LSA,
'
o
Q,
etc.)
SB-6
10/7/15
3-5
CSA
392
1150
914
_
SB-6
10/7/15
8-10
CSA
296
349
162
_
SB-6
10/7/15
13-15
CSA
120
91.6
34.8
<709
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
68
540
31
0.0056
4.3
4.3
4.9
1.7
0.12
0.16
Residential MSCC (mg/kg)
939
1500
12264
18
626
626
1560
1564
100
313
Industrial/Commercial MSCC (mg/kg)
24528
40000
469
164
16350
16350
40000
40880
4000
8176
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
s Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg.
Results
milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
mg/kgResidential MSCC.
27 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
Contaminant of Concern 4
r
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
r
(m/dd/yy)
(eg.
(ft BGS)
(Closure
-�
o
Tank pit
20Day,
1)
LSA,
a�
4
1
etc.)
ti
O
o
SB-6
10/7/15
3-5
CSA
828
SB-6
10/7/15
8-10
CSA
<1620
_
SB-6
10/7/15
13-15
CSA
<709
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
1.7
1.5
4.3
8.5
8.3
4.6
4.6
4.6
0.37
Residential MSCC (mg/kg)
626
3128
1200
782
782
3129
3129
3129
156
Industrial/Commercial MSCC (mg/kg)
16350
81760
32000
20440
20440
81760
81760
81760
4088
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
s Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg.
Results
milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
mg/kgResidential MSCC.
28 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
(m/dd/yy)
(eg.
(ft BGS)
(Closure
c
N
Tank pit
20Day,
r.
Q,
1)
LSA
N
°
75 l
°'
4 N
N
;
P.
48
DC
etc.)
w
Z
SB-4
10/7/15
13-15
CSA
6.7
3.9
9.8
10.4
5.4
14.7
3.8
15.7
5.8
10
SB-5
10/7/15
13-15
CSA
13.4
9.0
12.1
<2.6
<2.6
16.9
14.0
63.6
41.2
22.4
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
0.0056
0.37
4.9
91
0.16
4.3
8.5
4.6
4.6
4.6
Residential MSCC (mg/kg)
18
156
1560
350000
313
1200
782
3129
3129
3129
Industrial/Commercial MSCC (mg/kg)
310000
164
4088
40000
8176
32000
20440
81760
81760
81760
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
s Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg.
Results
milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
mg/kgResidential MSCC.
29 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
N
or.
(m/dd/yy)
(eg.
(ft BGS)
(Closure
°'
Tank pit
20Day,
c
y
y
1)
LSA,
Q.
°
p.
°
etc.)
�
2
w
SB-7
10/7/15
8-10
CSA
6.7
14.2
5.9
37.5
14.4
12.1
52.4
47.2
7.8
350
SB-4
10/7/15
3-5
CSA
<3.1
<3.1
<3.1
5.7
<3.1
<3.1
7.4
<3.1
14.7
8.1
SB-5
10/7/15
13-15
CSA
22.4
<2.6
<2.6
12.1
<2.6
<2.6
<2.6
<2.6
16.9
14.0
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
4.6
4.3
4.3
4.9
1.7
0.12
0.16
1.7
4.3
8.5
Residential MSCC (mg/kg)
3129
626
626
1560
1564
100
313
626
1200
782
Industrial/Commercial MSCC (mg/kg)
81760
16350
16350
40000
40880
4000
8176
16350
32000
20440
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
s Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg.
Results
milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
mg/kgResidential MSCC.
30 Change 2

Appendix B
Reporting Tables
Table B-3: Summary of Soil Sampling Results
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Analytical Method (e.g., VOC by EPA 8260)
Contaminant of Concern 4
Sample
Date
Source
Sample
Incident
ID
Collected
Area
Depth
Phase
a
(m/dd/yy)
(eg.
(ft BGS)
(Closure
4
4
Tank pit
20Day,
o
°
o
1)
LSA
A?
etc.)
SB-7
10/7/15
8-10
CSA
67.8
135
80.1
55.1
SB-5
10/7/15
13-15
CSA
3.9
63.6
41.2
22.4
7.8
14.0
Minimum Reporting Limit (mg/kg)
Varies
Varies
Varies
Varies
Varies
Varies
Soil to groundwater MSCC (mg/kg)
8.3
4.6
4.6
4.6
0.37
8.5
Residential MSCC (mg/kg)
782
3129
3129
3129
20
782
Industrial/Commercial MSCC (mg/kg)
20440
81760
81760
81760
180
20440
Indicate detection limit for contaminants when analyzed, but not detected (e.g., < 1, 10, 42)
List any contaminant detected above the method detection limit
MSCC = maximum soil contaminant concentration
ft. BGS = feet below ground surface
s Yellow shading indicates exceedance of Soil to
Results must be reported in mg/kg.
Results
milligrams per kilogram Groundwater MSCC. Red shading indicates exceedance of
mg/kgResidential MSCC.
31 Change 2

TABLE B-4
SUMMARY OF GROUNDWATER ANALYSES
SIX-O-ONE STOP
5661 HIGHWAY 601
CONCORD, NORTH CAROLINA 28025
Sample
Location
Sample Date
Benzene
Dilso-
propylether
Ethylbenzene
Isopropyl-
benzene
Methyl-tert-
butyl -ether
Naphthalene
N-propyl-
benzene
Toluene
1,2,4-
Trimethyl-
benzene
1,3,5-
Trimethyl-
benzene
m&p Xylenes
o-xylene
MW-1
11/12/2014
326
86.9
79.7
7
201
82
16
46.1
127
40.9
353
143
MW-1
10/12/2015
735
275
294
26.7
413
308
54.5
83.6
428
95.7
583
58.6
MW-1
11/21/2016
290
105
78.5
11.8
98.2
96.4
14.6
18.7
130
22.4
112
29.8
MW-1
5/1/2017
172
26
115
12.9
26.4
73.4
18.3
17.5
80.8
<1.0
72.9
53.6
MW-1
1/21/2018
117
33.2
65.4
10.9
37.1
63.0
11.9
11.9
76.6
<1.0
60.8
5.7
MW-2
11/12/2014
3810
1430
1270
70.7
66
242
169
3600
1420
365
4230
2980
MW-2
10/12/2015
7440
3190
1800
91.5
224
397
194
2210
1460
403
3880
2220
MW-2
10/14/2016
9680
3910
2940
90.7
182
492
226
584
1810
449
6170
2160
MW-2
12/13/2016
6830
4220
1760
101
238
302
276
269
1470
424
3010
791
MW-2
5/1/2017
2250
1160
556
21.7
64.7
92.3
ND
706
570
ND
1900
1750
MW-2
1/21/2018
8570
3240
2860
84.8
132
469
241
174
1760
432
5120
148
MW-3
11/12/2014
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
2.2
1.1
MW-3
10/12/2015
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<1.0
<0.5
MW-3
11/21/2016
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<1.0
<0.5
MW-3
5/1/2017
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
M W-3
1/21/2018
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-4
10/12/2015
<0.50
22.1
<0.50
<0.50
21.1
<2.0
<0.50
<0.50
<0.50
<0.50
<1.0
<0.5
MW-4
11/21/2016
<0.50
14
<0.50
<0.50
30
<2.0
<0.50
<0.50
<0.50
<0.50
<1.0
<0.5
MW-4
5/1/2017
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
M W-4
1/21/2018
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-5
10/12/2015
<0.50
<0.50
<0.50
<0.50
1.5
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
M W-5
11/21/2016
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-5
5/1/2017
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
M W-5
1/21/2018
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-6
10/12/2015
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-6
11/21/2016
<0.50
<0.50
<0.50
<0.50
6.2
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-6
5/1/2017
<0.50
<0.50
<0.50
<0.50
4.4
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
M W-6
1/21/2018
<0.50
<0.50
<0.50
<0.50
4.9
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
MW-7
10/12/2015
1.3
394
4.9
2.2
235
<2.0
2.5
<0.50
4.8
7.9
4.1
<1.2
MW-7
11/21/2016
10.7
144
23.3
19.4
57.2
3.3
14.4
2.1
22.8
13.3
9.3
<0.50
MW-7
5/1/2017
4
5.1
23
13.6
1.2
3.1
15
0.92
22.4
11.9
3.5
<0.50
MW-7
1/21/2018
8.1
22.6
55.0
25.2
6.9
6.9
37.8
1.7
79.7
37.4
29.0
<0.50
MW-8
10/12/2015
5.4
87.4
0.52
<0.50
375
<2.0
<0.50
<0.50
1.2
<0.50
1.2
<0.5
M W-8
11/21/2016
<0.50
28.5
<0.50
<0.50
98
<2.0
<0.50
<0.50
<0.50
<0.50
1.2
<0.50
MW-8
5/1/2017
<0.50
26.6
<0.50
<0.50
100
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
M W-8
1/21/2018
<0.50
<0.50
<0.50
<0.50
<0.50
<2.0
<0.50
<0.50
<0.50
<0.50
<0.50
<0.50
NCAC 2L Standard
1
600
70
20
6
70
600
400
400
500
500
GCL
5000
84500
25000
20000
6000
30000
260000
28500
25000
85500
85500
Notes: Yellow shading indicates exceedance of 2L
Red shading indicated exccedance of Gross Contaminant levells

Appendix B
Reporting Tables
Table B-5: Public and Private Water Supply Well and Other Receptor Information
Revision Date: 4/28/2015 Incident Number and Name: Six O One Stop Facility ID#: 4753
Public and Private Water Supply Wells
Latitude/
Distance
Longitude *
Well
Well
Well
from
Well Owner/ User
(decimal
Well
Depth
Type
Casing
Screen
source
c
Well #
(indicate which)
Address
Phone Number
degrees)
Use
(ft
of
Depth (ft.
Interval
area of
¢
BGS)
Well
BGS)
`x to y ft.
release
p
3
**
BGS)
(ft.)
.o
1
Owner/Marc Glover
5661 S. US
704-786-0600
35.339520/-
Not
Unk
Bored
Unk
Unk
80
Down
601
80.520421
used
2
Owner/Lanny
5651 Cold
35.339047/-
Drinki
Unk
Unk
Unk
Unk
404
Down
Griffin
Springs Road
80.518840
ng
3
Owner/John Plyer
5600 Cold
35.339763/-
Drinki
100
Unk
Unk
Unk
250
Down
Springs Rd
80.519646
ng
4
User/Ann
5807 US Hwy
35.337841/-
Not
Unk
Unk
Unk
Unk
700
Down
Huffstetler
601
80.518725
used
Other Receptors
(Other public water supplies, reservoirs, supply lines, surface water bodies, wellhead protection areas, recharge areas for deep aquifers, subsurface structures)
Latitude/ Longitude of
Up or
Distance from
Receptor
Description
Location
*
any significant point(s)
Contact
Phone
Usage
down-
source area of
ID
(describe to left)
Number
gradient
release (ft.)
(decimal de rees)
5
Pond
1017' NW
35.342343 /-80.519621
John
Unk
Down
1017
Plyer
* The location must be sufficiently accurate and precise to allow easy recovery of lost or damaged wells or replication of sampling points.
** Ft BGS = feet below ground surface
42 Change 2

Appendix B
Reporting Tables
Table B-6: Property Owners/ Occupants
Revision Date: 4/28/2015 Incident No. and Name: 40338 Six O One Stop Facility ID#: 4753
Tax Parcel
Owner/ Occupant Name
Number/
(Last, First MI)
Address
Map ID
Plyer, John
55486270610000
A5600
Cold Springs Road, Concord, NC 28025
Vacant land owned by Estate of
5625 Highway 601 South Concord, NC 28025, vacant
55486241930000
Saunders, Elma
land owned by Estate of Elma Saunders (140 Crescent
/2
Street, Kannapolis, NC 28081)
Griffin, Lanney
55487107460000
/3
5651 Cold Springs Road, Concord, NC 28025
Price, Robert L.
55486194340000
A5807
Highway 601 South, Concord, NC 28025
Unknown resident/ Church, Margie
5770 Highway 601 South, Concord, NC 28025,
55486162190000
/5
residence owned by Maggie Church (2767 Dale
Earnhardt Blvd., Kannapolis, NC 28083)
Unknown resident/ Young, Dorothea
5664 Highway 601 South, Concord, NC 28025,
55486165090000
/6
residence owned by Dorethea Young (4906 Fenwick
Place, Concord, NC 28025)
Unknown resident/ Sarver, Karen
55486147270000
5727 Old Monroe Circle, residence owned by Karen
/7
Sarver (5727 Old Monroe Circle, Concord, NC 28025)
Vacant land owned by Estate of
560 Highway 601 South Concord, NC 28025, vacant
55486241930000
Saunders, Elma
land owned by Estate of Elma Saunders (140 Crescent
/8
Street, Kannapolis, NC 28081)
43 Change 2

Appendix B
Reporting Tables
Table B-7: Monitoring and Remediation Well Construction Information
Revision Date: 3/2/2016 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Date
Date
Well
Well
Screened
Depth
Top of
Depth to
Free
Groundwater
Latitude/
Well
Installed
Water
Casing
Casing
Interval
of Well
Casing
Water
Product
Elevation*
Longitude
ID
(m/dd/yy)
Level
Diameter
Depth
(x to y—
(ft.
Elevation*
from Top
Thickness
(ft.)
(decimal
Measured
(in.)
(ft.
ft. BGS)
BGS)
(ft.)
of Casing
** (ft.)
degrees)***
(m/dd/yy)
BGS)
(ft.)
MW-1
10/28/2014
11/12/2014
2
20
20 to 30
30
98.92
22.87
0
76.05
35.339266/-
80.520191
MW-2
10/28/2014
11/12/2014
2
20
20 to 30
30
99.76
23.77
0
75.99
35.339206/-
80.520266
35.339108/-
MW-3
10/28/2014
11/12/2014
2
20
20 to 30
30
100.00
24.52
0
75.48
80.520021
MW-4
10/10/2015
10/12/2015
2
25
25 to 35
35
0
35.339150/-
80.520081
MW-5
10/10/2015
10/12/2015
2
25
25 to 35
35
0
35.339150/-
80.520081
MW-6
10/10/2015
10/12/2015
2
25
25 to 35
35
0
35.339150/-
80.520081
35.339150/-
MW-7
10/10/2015
10/12/2015
2
25
25 to 35
35
0
80.520081
MW-8
10/10/2015
10/12/2015
2
40
45 to 50
50
0
35.339150/-
80.520081
ft BGS = feet below ground
* Reference Point for Elevation Measurements North side casing MW-3 . Assumed Elevation: 100.00 ft.
** If free product is present in a well, groundwater elevation is calculated by: [Top of Casing Elevation - Depth to Water] + [free product thickness x 0.8581]
*** The location must be sufficiently accurate and precise to allow easy recovery of lost or damaged wells.
44 Change 2

Appendix G
Contaminant Sources Other than USTs
Table B-8A: Free Product Recovery Information
Revision Date: Incident Number and Name: Facilitv ID#:
Date
(m/dd/yy)
Well
ID #
Product
yp (gas
Type
diesel,
etc.)
Free
Product
Recovery
Method*
Product
Thickness
before
Recovery
(inches)
Product
Thickness
after
Recovery
(inches)
Amount of
Vaporized
Product
Amount of
Liquid
(Water
and
Product)
Amount
of Liquid
Product
Total
Amount of
Product
Recovered
(gallons)
(Present all calculations in an attachment)
* Bailing, Skimming, Aggressive Fluid Vapor Recovery, Mobile Multiphase Extraction, etc,
Table 13-813: Cumulative Volume of Free Product Recovered from Site
Date of Recovery
Event (m/dd/yy)
Total Volume Recovered from Site During
Current Recovery Event (gallons)
Cumulative Total of Volume Recovered to Date
from All Recovery Events (gallons)
45 Change 2

Appendix G
Contaminant Sources Other than USTs
Table B-9: Current and Historical Groundwater Elevations and Free Product Thickness
Revision Date: 4/28/2015 Incident Number and Name: 40338 Six O One Stop Facility ID#: 4753
Well ID
#
Date
Screened Interval
(top of screen,
bottom of screen)
Depth to Water*
Uncorrected
(feet)
Free
Product
Thickness
(feet)
Depth to Water*
Corrected
for Free Product
Thickness(feet)
Top of
Casing
Elevation
(MSL)
Groundwater
Surface
Elevation
(MSL)
MW-1
11/12/2014
20-30
22.87
NA
22.87
98.92
76.05
MW-1
10/12/2015
20 - 30
23.04
NA
23.04
98.92
75.88
MW-1
11/21/2016
20 - 30
23.31
NA
23.31
98.92
75.88
MW-2
11/12/2014
20 - 30
23.77
NA
23.77
99.76
75.99
MW-2
10/12/2015
20 - 30
23.95
NA
23.95
99.76
75.81
MW-2
11/21/2016
20 - 30
24.16
NA
24.16
99.76
75.81
MW-3
11/12/2014
20 - 30
24.52
NA
24.52
100.00
75.48
MW-3
10/12/2015
20 - 30
25.10
NA
25.10
100.00
74.9
MW-3
11/21/2016
20 - 30
25.13
NA
25.13
100.00
74.9
MW-4
10/12/2015
25 - 35
22.62
NA
22.62
98.75
76.13
MW-4
11/21/2016
25 - 35
22.74
NA
22.74
98.75
76.13
MW-5
10/12/2015
25 - 35
24.53
NA
24.53
100.08
75.55
MW-5
11/21/2016
25 - 35
24.36
NA
24.36
100.08
75.55
46 Change 2

Appendix G
Contaminant Sources Other than USTs
MW-6
10/12/2015
25 - 35
25.81
NA
25.81
99.43
73.62
MW-6
11/21/2016
25 - 35
26.03
NA
26.03
99.43
73.62
MW-7
10/12/2015
25 - 35
24.40
NA
24.40
98.65
73.85
MW-7
11/21/2016
25 - 35
24.57
NA
24.57
98.65
73.85
MW-8
10/12/2015
45 - 50
26.38
NA
26.38
99.85
73.47
MW-8
11/21/2016
45 - 50
25.58
NA
25.58
99.85
73.47
*Depth to Water is measured from Top of Casing
47 Change 2

Appendix G
Contaminant Sources Other than USTs
Table B-10: Land Use
Revision Date: 4/28/2015 Incident Number and Name: 40338 Six O One Stop
Facility ID#: 4753
Map ID #
Date
Determined
Land Use Feature
(include zoning)
Location
(complete street address if applicable)
Distance and
Direction from
Source Area
1
4/27/2015
Limited
Subject Property
Subject Property
Commercial (LC)
zoning district
2
4/27/2015
Agricultural Open
All adjoining and surrounding properties within 2,000 feet
All adjoining and
(AO) Space zoning
surrounding
district
properties within
2,000 feet
48 Change 2

APPENDIX I

Waste Management
ENVIRONMENTAL QUALITY
February 9, 2018
CERTIFIED MAIL
RETURN RECEIPT REQUESTED 7016 1370 0000 2590 0029
Attention: Marc Glover, Registered Agent
SixOOneStop, Inc.
5661 Highway 601 S.
Concord, NC 28025
Dear.Mr. Glover:
ROY COOPER
Governor
MICHAEL S. REGAN
secretary
MICHAEL SCOTT
Director
Re: Notice of Violation of 15A NCAC 2L .0400
Risk -based Assessment and Corrective Action for
Petroleum Underground Storage Tanks
SixOOne Stop
5661 Highway, 601 South, Cabarrus County
Incident Number: 40338
Risk Classification: High
Information received by this office of the UST Section, Division of Waste Management, .on April 30,
2014 confirms a release or discharge from a petroleum underground storage tank (UST) system at the above -
referenced location. Records indicate that you are the owner or operator of this UST system. This letter
explains the violation(s) and associated corrective action(s) you must take as a result of the release or
discharge in accordance with North Carolina statutes and rules. The UST Section, Division of Waste
Management, administers the state's rules for USTs and the required response for petroleum releases. Those
rules -are located in Title 15A, Subchapter 2L and Title 15A, Subchapter 2N of the North Carolina
Administrative Code (NCAC).
VIOLATION 1:
Failure to submit a groundwater monitoring report with the requested updated receptor information and
updated plume stability analysis to the UST Section in accordance with the Notice of Regulatory
Requirements dated October 3, 2017 (attached).
VIOLATION 2:
Failure to submit a letter report to document attempt(s) to try and obtain. necessary agreements for risk -
reduction. Please refer the Notice of Regulatory Requirements dated October 3, 2017 (attached).
REQUIRED CORRECTIVE ACTION:
Based on the determination that the risk posed by the discharge or release at the subject site is high, you must
comply with assessment requirements pursuant to Title 15A NCAC 2L .0407(b). Please submit a
groundwater monitoring report, including an updated plume stability analysis and updated receptor survey,
within 30 days from the date of this Notice. Furthermore, submit documentation to demonstrate attempts to
try and obtain necessary agreements for risk -reduction within 30 days from the date of this Notice. Please
refer to the Notice of Regulatory Requirements dated October 3, 2017.
State of North Carolina I Environmental Quality I Waste Management
Mooresville Regional Office 1610 East Center Avenue, Suite 301 I Mooresville, NC 28115
704 6631.699

Please take the corrective action(s) for the above violation(s) as necessary to bring the site into
compliance. Corrective actions must be taken and reported to the Mooresville Regional Office, within 3 0
days from the date of this notice, unless otherwise noted in the above corrective actions, to avoid
recommendation of civil penalties for continuing violations.
Penalties may be assessed for the violation(s) described within this Notice of Violation. Your
prompt attention to the items described herein is required. Failure to comply with the State's rules, in the
manner and time specified, may result in the assessment of additional civil penalties and/or the use of other
enforcement mechanisms available to the State. Each day that a violation continues may be considered a
separate violation.
Please note that performing assessment and cleanup work that is not required under 15A NCAC 2L
.0400 is not reimbursable from the Commercial or Noncommercial Leaking Petroleum Underground Storage
Tank Cleanup Funds.
If you have any questions regarding the actions that must be taken or the rules mentioned in this
letter, please contact Brett Morris at (704) 235-21.68 or by the address for the Mooresville Regional Office
listed below. If you have any questions regarding trust fund eligibility or reimbursement, please contact the
UST Section Trust Fund Branch at [phone].
Sincerely,
\� a
onald araban, P . .
Regional Supervisor
Mooresville Regional Office
UST Section, Division of Waste Management, NCDEQ
Attachment: October 3, 2017 Notice of Regulatory Requirements
cc: Dr. William F. Pilkington — Cabarrus County Health Alliance
Steven Irminger — CESI
State of North Carolina I Environmental Quality I Waste Management
Mooresville Regional Office 1 610 East Center Avenue, Suite 301 I Mooresville, NC 281.15
704 6631.699

..... ..■...11m...- • 0
Waste Management
ENV1R NIMEHTAL ObALITY
Attention: Marc Glover, Registered Agent
SixoOneStop, Inc.
5661 Highway 601 S.
Concord, NC 28025
ROY COOPER
MIC:H.AEL S.. AEGAN
Secretary
MICHAEL SCOTT
Director
October 23,.2017
Re: Notice of Regulatory Requirements.
15A NCAC 2L .0407(b)
Six0One Stop
5661 Highway 601 South, Cabarrus, County
Incident Number: 40138
Risk Classification: High
Dear Mr. Glover:
The UST Section has reviewed the most recent groundwater sampling data/ plume stability report.
The risk ,posed by the discharge or release at the subject site is classified by the Department 'of
Environmental Quality as High' due to the existence of nearby water supply wells.
Please conduct a semi-annual groundwater monitoring event within 30 days from the date of this
Notice. Include groundwater sampling results from all incident monitoring wells.and all water supply
wells within 1000 feet of the release.. After you receive the requested groundwater monitoring, results
please include in the -report an update to the plume stability analysis utilizing the new groundwater data.
Submit a monitoring report to present the results/findings within 45 days from the date of this Notice to my
attention at the Mooresville Regional Office listed below.
Please note that information that was recently reported indicates that a water line .does not exist
within the search radius on Cold Springs Road. Because the receptor information does not report any
water supply wells on several properties identified on Cold Springs Road, the source for a water supply for
these properties remains unclear. Therefore, please update the receptor information to identify all water
supply wells within.1000 feet of the release and provide clarification as to the source of water usage for
each property. Include the requested receptor information in the monitoring report requested above.
In effort to help determine whether corrective action through active remediation is necessary,
connections to public water must be evaluated as a potential cost effective alternative moving forward.
The goal of public water connections is to minimize the risk to potentially threatened water supply wells
on nearby properties. Specifically, you must reasonably attempt to obtain agreements for connections to
public water from all the users of all the water supply wells that are located within 500 feet of the source:
area. Also, you must attempt to obtain agreements for connections to public water from all users of all the
water supply wells used for potable purposes which are located within 1000 feet downgradient of the
source area. Additionally, an attempt must be made to obtain. agreements from water supply well owners
to abandon all the water supply wells that are within 250 feet of the release.
State of North Carolina I Environmental Quality I waste Management
Mooresville Regional TCffice 1 610 East Center Avenue, Suite 3011 Mooresville, -NC 28115
704 6631699

Although a water line extension may be needed to connect some or all of the above -mentioned
DI-0—pertes obtainin a eements is the first ste _towards determinin _if all necessary water connections _
will , e a ease. �le o on. If all. agreen�en requ'eae— above can be ob a e�. 90 AMIl`nezessWr ate
connections/abandonments can be completed, then further evaluation will be later requested. However, if .
water connections/well abandonments cannot be accomplished, then other active remediation options will
likely be necessary.
Therefore, please submit a letter report, including the agreements requested above, to my attention
at the Mooresville Regional Office; UST Section, within 45 days from the date of this notice. If
agreements cannot be reached with all the necessary water supply well owners/users mention above, then
you must document your attempt(s) .by detailing all efforts to try and obtain such agreements in the letter
report requested above.
All groundwater sampling and reporting must be conducted in accordance with the most recent
version of the Guidelines for Assessment and Corrective. Action for UST Releases. Failure to comply in
the manner and time specified. may result hi the assessment of civil penalties and/or the use of .other
enforcement mechanisms. If you have questions regarding the information contained in this letter, please
contact me at (704) 23 5-2168 or by: the address for the Mooresville- Regional Office listed below.
S' Rely,
� t s
Brett orris
Hydrogeologist
Mooresvllk Regional Office
UST Section, Division of Wane 1Vlanagement,l�dCDEQ
cc: Steven Irminger - CESI, PO Box 268, Concord, NC 28026
State. of North Carolina. I Environmental Quality i waste Management
Mooresville P:egional:ofke 1 610 East Center Avenue, Suite 3011 Mooresville; NC 28115
704 6631699.

APPENDIX 2

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
January 26, 2018
Mr. Steve Irminger
Irminger Consulting
7015 Erinbrook Road
Concord, NC 28025
RE: Project: 601
Pace Project No.: 92370403
Dear Mr. Irminger:
Enclosed are the analytical results for sample(s) received by the laboratory on January 23, 2018.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
/I
Nicole Gasiorowski
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 36

acmnalytical
www.pacelabs.com
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: 601
Pace Project No.: 92370403
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 36

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
601
92370403
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92370403001
MW-1
SM
6200B
SWB
63
PASI-C
92370403002
MW-2
SM
6200B
CAH
63
PASI-C
92370403003
MW-3
SM
6200B
CAH
63
PASI-C
92370403004
MW-4
SM
6200B
CAH
63
PASI-C
92370403005
MW-5
SM
6200B
CAH
63
PASI-C
92370403006
MW-6
SM
6200B
CAH
63
PASI-C
92370403007
MW-7
SM
6200B
CAH
63
PASI-C
92370403008
MW-8
SM
6200B
CAH
63
PASI-C
92370403009
WSW-1
SM
6200B
CAH
63
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 36

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601
Pace Project No.: 92370403
Sample: MW-1 Lab ID: 92370403001 Collected: 01/21/18 11:00 Received: 01/23/18 11:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method: SM 6200B
Benzene
117
ug/L
1.0
2
01/26/18 12:17
71-43-2
Bromobenzene
ND
ug/L
1.0
2
01/26/18 12:17
108-86-1
Bromochloromethane
ND
ug/L
1.0
2
01/26/18 12:17
74-97-5
Bromodichloromethane
ND
ug/L
1.0
2
01/26/18 12:17
75-27-4
Bromoform
ND
ug/L
1.0
2
01/26/18 12:17
75-25-2
Bromomethane
ND
ug/L
10.0
2
01/26/18 12:17
74-83-9
n-Butylbenzene
ND
ug/L
1.0
2
01/26/18 12:17
104-51-8
sec-Butylbenzene
ND
ug/L
1.0
2
01/26/18 12:17
135-98-8
tert-Butyl benzene
ND
ug/L
1.0
2
01/26/18 12:17
98-06-6
Carbon tetrachloride
ND
ug/L
1.0
2
01/26/18 12:17
56-23-5
Chlorobenzene
ND
ug/L
1.0
2
01/26/18 12:17
108-90-7
Chloroethane
ND
ug/L
2.0
2
01/26/18 12:17
75-00-3
Chloroform
ND
ug/L
1.0
2
01/26/18 12:17
67-66-3
Chloromethane
ND
ug/L
2.0
2
01/26/18 12:17
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
2
01/26/18 12:17
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
2
01/26/18 12:17
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
2
01/26/18 12:17
96-12-8
Dibromochloromethane
ND
ug/L
1.0
2
01/26/18 12:17
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
2
01/26/18 12:17
106-93-4
Dibromomethane
ND
ug/L
1.0
2
01/26/18 12:17
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
2
01/26/18 12:17
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
2
01/26/18 12:17
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
2
01/26/18 12:17
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
2
01/26/18 12:17
75-71-8
1,1-Dichloroethane
ND
ug/L
1.0
2
01/26/18 12:17
75-34-3
1,2-Dichloroethane
ND
ug/L
1.0
2
01/26/18 12:17
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
2
01/26/18 12:17
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
2
01/26/18 12:17
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
1.0
2
01/26/18 12:17
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
2
01/26/18 12:17
78-87-5
1,3-Dichloropropane
ND
ug/L
1.0
2
01/26/18 12:17
142-28-9
2,2-Dichloropropane
ND
ug/L
1.0
2
01/26/18 12:17
594-20-7
1,1-Dichloropropene
ND
ug/L
1.0
2
01/26/18 12:17
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
1.0
2
01/26/18 12:17
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
2
01/26/18 12:17
10061-02-6
Diisopropyl ether
33.2
ug/L
1.0
2
01/26/18 12:17
108-20-3
Ethylbenzene
65.4
ug/L
1.0
2
01/26/18 12:17
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
4.0
2
01/26/18 12:17
87-68-3
Isopropylbenzene (Cumene)
10.9
ug/L
1.0
2
01/26/18 12:17
98-82-8
Methylene Chloride
ND
ug/L
4.0
2
01/26/18 12:17
75-09-2
Methyl-tert-butyl ether
37.1
ug/L
1.0
2
01/26/18 12:17
1634-04-4
Naphthalene
63.0
ug/L
4.0
2
01/26/18 12:17
91-20-3
n-Propylbenzene
11.9
ug/L
1.0
2
01/26/18 12:17
103-65-1
Styrene
ND
ug/L
1.0
2
01/26/18 12:17
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
1.0
2
01/26/18 12:17
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
1.0
2
01/26/18 12:17
79-34-5
Tetrachloroethene
ND
ug/L
1.0
2
01/26/18 12:17
127-18-4
REPORT OF LABORATORY
ANALYSIS
This report shall not
be reproduced, except in full,
Date: 01 /26/2018 04:57 PM
without
the written consent
of Pace Analytical Services, LLC.
Page 4 of 36

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601
Pace Project No.: 92370403
Sample: MW-1 Lab ID: 92370403001 Collected: 01/21/18 11:00 Received: 01/23/18 11:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 01/26/2018 04:57 PM
Analytical Method: SM 6200B
11.9
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
76.6
ug/L
ND
ug/L
ND
ug/L
60.8
ug/L
5.7
ug/L
102 %
99 %
99 %
1.0
2
01/26/1812:17
108-88-3
4.0
2
01 /26/18 12:17
87-61-6
4.0
2
01/26/1812:17
120-82-1
1.0
2
01 /26/18 12:17
71-55-6
1.0
2
01/26/1812:17
79-00-5
1.0
2
01 /26/18 12:17
79-01-6
2.0
2
01/26/1812:17
75-69-4
1.0
2
01/26/1812:17
96-18-4
1.0
2
01/26/1812:17
95-63-6
1.0
2
01/26/1812:17
108-67-8
2.0
2
01 /26/18 12:17
75-01-4
2.0
2
01/26/1812:17
179601-23-1
1.0
2
01/26/1812:17
95-47-6
70-130
2
01/26/1812:17
17060-07-0
70-130
2
01/26/1812:17
460-00-4
70-130
2
01/26/1812:17
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 36

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601
Pace Project No.: 92370403
Sample: MW-2 Lab ID: 92370403002 Collected: 01/21/18 12:00 Received: 01/23/18 11:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method: SM 6200B
Benzene
8570
ug/L
25.0
50
01/25/18 23:39
71-43-2
Bromobenzene
ND
ug/L
25.0
50
01/25/18 23:39
108-86-1
Bromochloromethane
ND
ug/L
25.0
50
01/25/18 23:39
74-97-5
Bromodichloromethane
ND
ug/L
25.0
50
01/25/18 23:39
75-27-4
Bromoform
ND
ug/L
25.0
50
01/25/18 23:39
75-25-2
Bromomethane
ND
ug/L
250
50
01/25/18 23:39
74-83-9
n-Butylbenzene
ND
ug/L
25.0
50
01/25/18 23:39
104-51-8
sec-Butylbenzene
ND
ug/L
25.0
50
01/25/18 23:39
135-98-8
tert-Butyl benzene
ND
ug/L
25.0
50
01/25/18 23:39
98-06-6
Carbon tetrachloride
ND
ug/L
25.0
50
01/25/18 23:39
56-23-5
Chlorobenzene
ND
ug/L
25.0
50
01/25/18 23:39
108-90-7
Chloroethane
ND
ug/L
50.0
50
01/25/18 23:39
75-00-3 M1
Chloroform
ND
ug/L
25.0
50
01/25/18 23:39
67-66-3
Chloromethane
ND
ug/L
50.0
50
01/25/18 23:39
74-87-3
2-Chlorotoluene
ND
ug/L
25.0
50
01/25/18 23:39
95-49-8
4-Chlorotoluene
ND
ug/L
25.0
50
01/25/18 23:39
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
50.0
50
01/25/18 23:39
96-12-8
Dibromochloromethane
ND
ug/L
25.0
50
01/25/18 23:39
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
25.0
50
01/25/18 23:39
106-93-4
Dibromomethane
ND
ug/L
25.0
50
01/25/18 23:39
74-95-3
1,2-Dichlorobenzene
ND
ug/L
25.0
50
01/25/18 23:39
95-50-1
1,3-Dichlorobenzene
ND
ug/L
25.0
50
01/25/18 23:39
541-73-1
1,4-Dichlorobenzene
ND
ug/L
25.0
50
01/25/18 23:39
106-46-7
Dichlorodifluoromethane
ND
ug/L
25.0
50
01/25/18 23:39
75-71-8
1,1-Dichloroethane
ND
ug/L
25.0
50
01/25/18 23:39
75-34-3
1,2-Dichloroethane
ND
ug/L
25.0
50
01/25/18 23:39
107-06-2
1,1-Dichloroethene
ND
ug/L
25.0
50
01/25/18 23:39
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
25.0
50
01/25/18 23:39
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
25.0
50
01/25/18 23:39
156-60-5
1,2-Dichloropropane
ND
ug/L
25.0
50
01/25/18 23:39
78-87-5
1,3-Dichloropropane
ND
ug/L
25.0
50
01/25/18 23:39
142-28-9
2,2-Dichloropropane
ND
ug/L
25.0
50
01/25/18 23:39
594-20-7
1,1-Dichloropropene
ND
ug/L
25.0
50
01/25/18 23:39
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
25.0
50
01/25/18 23:39
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
25.0
50
01/25/18 23:39
10061-02-6
Diisopropyl ether
3240
ug/L
25.0
50
01/25/18 23:39
108-20-3
Ethylbenzene
2860
ug/L
25.0
50
01/25/18 23:39
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
100
50
01/25/18 23:39
87-68-3
Isopropylbenzene (Cumene)
84.8
ug/L
25.0
50
01/25/18 23:39
98-82-8
Methylene Chloride
ND
ug/L
100
50
01/25/18 23:39
75-09-2
Methyl-tert-butyl ether
132
ug/L
25.0
50
01/25/18 23:39
1634-04-4 M1
Naphthalene
469
ug/L
100
50
01/25/18 23:39
91-20-3
n-Propylbenzene
241
ug/L
25.0
50
01/25/18 23:39
103-65-1
Styrene
ND
ug/L
25.0
50
01/25/18 23:39
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
25.0
50
01/25/18 23:39
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
25.0
50
01/25/18 23:39
79-34-5
Tetrachloroethene
ND
ug/L
25.0
50
01/25/18 23:39
127-18-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /26/2018 04:57 PM
without
the written consent
of Pace Analytical Services, LLC.
Page 6 of 36

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601
Pace Project No.: 92370403
Sample: MW-2 Lab ID: 92370403002 Collected: 01/21/18 12:00 Received: 01/23/18 11:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 01/26/2018 04:57 PM
Analytical Method: SM 6200B
174
ug/L
25.0
50
01/25/18 23:39
108-88-3
ND
ug/L
100
50
01/25/18 23:39
87-61-6
ND
ug/L
100
50
01/25/18 23:39
120-82-1
ND
ug/L
25.0
50
01/25/18 23:39
71-55-6
ND
ug/L
25.0
50
01/25/18 23:39
79-00-5
ND
ug/L
25.0
50
01/25/18 23:39
79-01-6
ND
ug/L
50.0
50
01/25/18 23:39
75-69-4
ND
ug/L
25.0
50
01/25/18 23:39
96-18-4 M1
1760
ug/L
25.0
50
01/25/18 23:39
95-63-6
432
ug/L
25.0
50
01/25/18 23:39
108-67-8
ND
ug/L
50.0
50
01/25/18 23:39
75-01-4
5120
ug/L
50.0
50
01/25/18 23:39
179601-23-1
148
ug/L
25.0
50
01/25/18 23:39
95-47-6
98
%
70-130
50
01/25/18 23:39
17060-07-0
100
%
70-130
50
01/25/18 23:39
460-00-4
100
%
70-130
50
01/25/18 23:39
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 36

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601
Pace Project No.: 92370403
Sample: MW-3 Lab ID: 92370403003 Collected: 01/21/18 10:00 Received: 01/23/18 11:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method: SM 6200B
Benzene
ND
ug/L
0.50
1
01/25/18 18:39
71-43-2
Bromobenzene
ND
ug/L
0.50
1
01/25/18 18:39
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
01/25/18 18:39
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
01/25/18 18:39
75-27-4
Bromoform
ND
ug/L
0.50
1
01/25/18 18:39
75-25-2
Bromomethane
ND
ug/L
5.0
1
01/25/18 18:39
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
01/25/18 18:39
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
01/25/18 18:39
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
01/25/18 18:39
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
01/25/18 18:39
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
01/25/18 18:39
108-90-7
Chloroethane
ND
ug/L
1.0
1
01/25/18 18:39
75-00-3
Chloroform
ND
ug/L
0.50
1
01/25/18 18:39
67-66-3
Chloromethane
ND
ug/L
1.0
1
01/25/18 18:39
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
01/25/18 18:39
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
01/25/18 18:39
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
01/25/18 18:39
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
01/25/18 18:39
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
01/25/18 18:39
106-93-4
Dibromomethane
ND
ug/L
0.50
1
01/25/18 18:39
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 18:39
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 18:39
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 18:39
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
01/25/18 18:39
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
01/25/18 18:39
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
01/25/18 18:39
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
01/25/18 18:39
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
01/25/18 18:39
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
01/25/18 18:39
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
01/25/18 18:39
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
01/25/18 18:39
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
01/25/18 18:39
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
01/25/18 18:39
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
01/25/18 18:39
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
01/25/18 18:39
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
01/25/18 18:39
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
01/25/18 18:39
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
01/25/18 18:39
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
01/25/18 18:39
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
01/25/18 18:39
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
01/25/18 18:39
1634-04-4
Naphthalene
ND
ug/L
2.0
1
01/25/18 18:39
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
01/25/18 18:39
103-65-1
Styrene
ND
ug/L
0.50
1
01/25/18 18:39
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
01/25/18 18:39
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
01/25/18 18:39
79-34-5
Tetrachloroethene
ND
ug/L
0.50
1
01/25/18 18:39
127-18-4
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /26/2018 04:57 PM
without
the written consent
of Pace Analytical Services, LLC.
Page 8 of 36

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601
Pace Project No.: 92370403
Sample: MW-3 Lab ID: 92370403003 Collected: 01/21/18 10:00 Received: 01/23/18 11:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 01/26/2018 04:57 PM
Analytical Method: SM 6200B
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
100 %
96 %
100 %
0.50
1
01 /25/18 18:39
108-88-3
2.0
1
01/25/1818:39
87-61-6
2.0
1
01 /25/18 18:39
120-82-1
0.50
1
01/25/1818:39
71-55-6
0.50
1
01/25/1818:39
79-00-5
0.50
1
01/25/1818:39
79-01-6
1.0
1
01/25/1818:39
75-69-4
0.50
1
01/25/1818:39
96-18-4
0.50
1
01/25/1818:39
95-63-6
0.50
1
01 /25/18 18:39
108-67-8
1.0
1
01/25/1818:39
75-01-4
1.0
1
01 /25/18 18:39
179601-23-1
0.50
1
01/25/1818:39
95-47-6
70-130
1
01 /25/18 18:39
17060-07-0
70-130
1
01/25/1818:39
460-00-4
70-130
1
01/25/1818:39
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 36

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601
Pace Project No.: 92370403
Sample: MW-4 Lab ID: 92370403004 Collected: 01/21/18 10:30 Received: 01/23/18 11:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method: SM 6200B
Benzene
ND
ug/L
0.50
1
01/25/18 18:57
71-43-2
Bromobenzene
ND
ug/L
0.50
1
01/25/18 18:57
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
01/25/18 18:57
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
01/25/18 18:57
75-27-4
Bromoform
ND
ug/L
0.50
1
01/25/18 18:57
75-25-2
Bromomethane
ND
ug/L
5.0
1
01/25/18 18:57
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
01/25/18 18:57
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
01/25/18 18:57
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
01/25/18 18:57
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
01/25/18 18:57
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
01/25/18 18:57
108-90-7
Chloroethane
ND
ug/L
1.0
1
01/25/18 18:57
75-00-3
Chloroform
ND
ug/L
0.50
1
01/25/18 18:57
67-66-3
Chloromethane
ND
ug/L
1.0
1
01/25/18 18:57
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
01/25/18 18:57
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
01/25/18 18:57
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
01/25/18 18:57
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
01/25/18 18:57
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
01/25/18 18:57
106-93-4
Dibromomethane
ND
ug/L
0.50
1
01/25/18 18:57
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 18:57
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 18:57
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 18:57
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
01/25/18 18:57
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
01/25/18 18:57
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
01/25/18 18:57
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
01/25/18 18:57
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
01/25/18 18:57
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
01/25/18 18:57
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
01/25/18 18:57
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
01/25/18 18:57
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
01/25/18 18:57
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
01/25/18 18:57
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
01/25/18 18:57
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
01/25/18 18:57
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
01/25/18 18:57
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
01/25/18 18:57
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
01/25/18 18:57
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
01/25/18 18:57
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
01/25/18 18:57
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
01/25/18 18:57
1634-04-4
Naphthalene
ND
ug/L
2.0
1
01/25/18 18:57
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
01/25/18 18:57
103-65-1
Styrene
ND
ug/L
0.50
1
01/25/18 18:57
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
01/25/18 18:57
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
01/25/18 18:57
79-34-5
Tetrachloroethene
ND
ug/L
0.50
1
01/25/18 18:57
127-18-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /26/2018 04:57 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 36

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601
Pace Project No.: 92370403
Sample: MW-4 Lab ID: 92370403004 Collected: 01/21/18 10:30 Received: 01/23/18 11:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 01/26/2018 04:57 PM
Analytical Method: SM 6200B
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
100 %
97 %
100 %
0.50
1
01 /25/18 18:57
108-88-3
2.0
1
01/25/1818:57
87-61-6
2.0
1
01 /25/18 18:57
120-82-1
0.50
1
01/25/1818:57
71-55-6
0.50
1
01/25/1818:57
79-00-5
0.50
1
01/25/1818:57
79-01-6
1.0
1
01/25/1818:57
75-69-4
0.50
1
01/25/1818:57
96-18-4
0.50
1
01/25/1818:57
95-63-6
0.50
1
01 /25/18 18:57
108-67-8
1.0
1
01/25/1818:57
75-01-4
1.0
1
01 /25/18 18:57
179601-23-1
0.50
1
01/25/1818:57
95-47-6
70-130
1
01 /25/18 18:57
17060-07-0
70-130
1
01/25/1818:57
460-00-4
70-130
1
01/25/1818:57
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 36

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601
Pace Project No.: 92370403
Sample: MW-5 Lab ID: 92370403005 Collected: 01/21/18 09:30 Received: 01/23/18 11:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method: SM 6200B
Benzene
ND
ug/L
0.50
1
01/25/18 19:15
71-43-2
Bromobenzene
ND
ug/L
0.50
1
01/25/18 19:15
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
01/25/18 19:15
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
01/25/18 19:15
75-27-4
Bromoform
ND
ug/L
0.50
1
01/25/18 19:15
75-25-2
Bromomethane
ND
ug/L
5.0
1
01/25/18 19:15
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
01/25/18 19:15
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
01/25/18 19:15
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
01/25/18 19:15
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
01/25/18 19:15
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
01/25/18 19:15
108-90-7
Chloroethane
ND
ug/L
1.0
1
01/25/18 19:15
75-00-3
Chloroform
ND
ug/L
0.50
1
01/25/18 19:15
67-66-3
Chloromethane
ND
ug/L
1.0
1
01/25/18 19:15
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
01/25/18 19:15
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
01/25/18 19:15
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
01/25/18 19:15
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
01/25/18 19:15
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
01/25/18 19:15
106-93-4
Dibromomethane
ND
ug/L
0.50
1
01/25/18 19:15
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 19:15
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 19:15
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 19:15
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
01/25/18 19:15
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
01/25/18 19:15
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
01/25/18 19:15
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
01/25/18 19:15
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
01/25/18 19:15
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
01/25/18 19:15
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
01/25/18 19:15
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
01/25/18 19:15
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
01/25/18 19:15
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
01/25/18 19:15
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
01/25/18 19:15
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
01/25/18 19:15
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
01/25/18 19:15
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
01/25/18 19:15
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
01/25/18 19:15
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
01/25/18 19:15
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
01/25/18 19:15
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
01/25/18 19:15
1634-04-4
Naphthalene
ND
ug/L
2.0
1
01/25/18 19:15
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
01/25/18 19:15
103-65-1
Styrene
ND
ug/L
0.50
1
01/25/18 19:15
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
01/25/18 19:15
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
01/25/18 19:15
79-34-5
Tetrachloroethene
ND
ug/L
0.50
1
01/25/18 19:15
127-18-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /26/2018 04:57 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 36

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601
Pace Project No.: 92370403
Sample: MW-5 Lab ID: 92370403005 Collected: 01/21/18 09:30 Received: 01/23/18 11:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 01/26/2018 04:57 PM
Analytical Method: SM 6200B
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
100 %
100 %
102 %
0.50
1
01 /25/18 19:15
108-88-3
2.0
1
01/25/1819:15
87-61-6
2.0
1
01 /25/18 19:15
120-82-1
0.50
1
01/25/1819:15
71-55-6
0.50
1
01/25/1819:15
79-00-5
0.50
1
01/25/1819:15
79-01-6
1.0
1
01/25/1819:15
75-69-4
0.50
1
01/25/1819:15
96-18-4
0.50
1
01/25/1819:15
95-63-6
0.50
1
01 /25/18 19:15
108-67-8
1.0
1
01/25/1819:15
75-01-4
1.0
1
01 /25/18 19:15
179601-23-1
0.50
1
01/25/1819:15
95-47-6
70-130
1
01 /25/18 19:15
17060-07-0
70-130
1
01/25/1819:15
460-00-4
70-130
1
01/25/1819:15
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 36

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601
Pace Project No.: 92370403
Sample: MW-6 Lab ID: 92370403006 Collected: 01/21/18 09:00 Received: 01/23/18 11:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method: SM 6200B
Benzene
ND
ug/L
0.50
1
01/25/18 19:32
71-43-2
Bromobenzene
ND
ug/L
0.50
1
01/25/18 19:32
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
01/25/18 19:32
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
01/25/18 19:32
75-27-4
Bromoform
ND
ug/L
0.50
1
01/25/18 19:32
75-25-2
Bromomethane
ND
ug/L
5.0
1
01/25/18 19:32
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
01/25/18 19:32
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
01/25/18 19:32
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
01/25/18 19:32
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
01/25/18 19:32
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
01/25/18 19:32
108-90-7
Chloroethane
ND
ug/L
1.0
1
01/25/18 19:32
75-00-3
Chloroform
ND
ug/L
0.50
1
01/25/18 19:32
67-66-3
Chloromethane
ND
ug/L
1.0
1
01/25/18 19:32
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
01/25/18 19:32
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
01/25/18 19:32
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
01/25/18 19:32
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
01/25/18 19:32
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
01/25/18 19:32
106-93-4
Dibromomethane
ND
ug/L
0.50
1
01/25/18 19:32
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 19:32
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 19:32
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 19:32
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
01/25/18 19:32
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
01/25/18 19:32
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
01/25/18 19:32
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
01/25/18 19:32
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
01/25/18 19:32
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
01/25/18 19:32
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
01/25/18 19:32
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
01/25/18 19:32
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
01/25/18 19:32
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
01/25/18 19:32
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
01/25/18 19:32
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
01/25/18 19:32
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
01/25/18 19:32
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
01/25/18 19:32
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
01/25/18 19:32
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
01/25/18 19:32
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
01/25/18 19:32
75-09-2
Methyl-tert-butyl ether
4.9
ug/L
0.50
1
01/25/18 19:32
1634-04-4
Naphthalene
ND
ug/L
2.0
1
01/25/18 19:32
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
01/25/18 19:32
103-65-1
Styrene
ND
ug/L
0.50
1
01/25/18 19:32
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
01/25/18 19:32
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
01/25/18 19:32
79-34-5
Tetrachloroethene
ND
ug/L
0.50
1
01/25/18 19:32
127-18-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /26/2018 04:57 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 36

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601
Pace Project No.: 92370403
Sample: MW-6 Lab ID: 92370403006 Collected: 01/21/18 09:00 Received: 01/23/18 11:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 01/26/2018 04:57 PM
Analytical Method: SM 6200B
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
100 %
101 %
100 %
0.50
1
01 /25/18 19:32
108-88-3
2.0
1
01/25/1819:32
87-61-6
2.0
1
01 /25/18 19:32
120-82-1
0.50
1
01/25/1819:32
71-55-6
0.50
1
01/25/1819:32
79-00-5
0.50
1
01/25/1819:32
79-01-6
1.0
1
01/25/1819:32
75-69-4
0.50
1
01/25/1819:32
96-18-4
0.50
1
01/25/1819:32
95-63-6
0.50
1
01 /25/18 19:32
108-67-8
1.0
1
01/25/1819:32
75-01-4
1.0
1
01 /25/18 19:32
179601-23-1
0.50
1
01/25/1819:32
95-47-6
70-130
1
01 /25/18 19:32
17060-07-0
70-130
1
01/25/1819:32
460-00-4
70-130
1
01/25/1819:32
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 36

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601
Pace Project No.: 92370403
Sample: MW-7 Lab ID: 92370403007 Collected: 01/21/18 11:30 Received: 01/23/18 11:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method: SM 6200B
Benzene
8.1
ug/L
0.50
1
01/25/18 19:50
71-43-2
Bromobenzene
ND
ug/L
0.50
1
01/25/18 19:50
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
01/25/18 19:50
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
01/25/18 19:50
75-27-4
Bromoform
ND
ug/L
0.50
1
01/25/18 19:50
75-25-2
Bromomethane
ND
ug/L
5.0
1
01/25/18 19:50
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
01/25/18 19:50
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
01/25/18 19:50
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
01/25/18 19:50
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
01/25/18 19:50
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
01/25/18 19:50
108-90-7
Chloroethane
ND
ug/L
1.0
1
01/25/18 19:50
75-00-3
Chloroform
1.0
ug/L
0.50
1
01/25/18 19:50
67-66-3
Chloromethane
ND
ug/L
1.0
1
01/25/18 19:50
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
01/25/18 19:50
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
01/25/18 19:50
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
01/25/18 19:50
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
01/25/18 19:50
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
01/25/18 19:50
106-93-4
Dibromomethane
ND
ug/L
0.50
1
01/25/18 19:50
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 19:50
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 19:50
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 19:50
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
01/25/18 19:50
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
01/25/18 19:50
75-34-3
1,2-Dichloroethane
0.69
ug/L
0.50
1
01/25/18 19:50
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
01/25/18 19:50
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
01/25/18 19:50
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
01/25/18 19:50
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
01/25/18 19:50
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
01/25/18 19:50
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
01/25/18 19:50
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
01/25/18 19:50
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
01/25/18 19:50
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
01/25/18 19:50
10061-02-6
Diisopropyl ether
22.6
ug/L
0.50
1
01/25/18 19:50
108-20-3
Ethylbenzene
55.0
ug/L
0.50
1
01/25/18 19:50
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
01/25/18 19:50
87-68-3
Isopropylbenzene (Cumene)
25.2
ug/L
0.50
1
01/25/18 19:50
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
01/25/18 19:50
75-09-2
Methyl-tert-butyl ether
6.9
ug/L
0.50
1
01/25/18 19:50
1634-04-4
Naphthalene
6.9
ug/L
2.0
1
01/25/18 19:50
91-20-3
n-Propylbenzene
37.8
ug/L
0.50
1
01/25/18 19:50
103-65-1
Styrene
ND
ug/L
0.50
1
01/25/18 19:50
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
01/25/18 19:50
630-20-6
1,1,2,2-Tetrachloroethane
2.9
ug/L
0.50
1
01/25/18 19:50
79-34-5
Tetrachloroethene
ND
ug/L
0.50
1
01/25/18 19:50
127-18-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /26/2018 04:57 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 36

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601
Pace Project No.: 92370403
Sample: MW-7 Lab ID: 92370403007 Collected: 01/21/18 11:30 Received: 01/23/18 11:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 01/26/2018 04:57 PM
Analytical Method: SM 6200B
1.7
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
79.7
ug/L
37.4
ug/L
ND
ug/L
29.0
ug/L
ND
ug/L
100 %
104 %
99 %
0.50
1
01 /25/18 19:50
108-88-3
2.0
1
01/25/1819:50
87-61-6
2.0
1
01 /25/18 19:50
120-82-1
0.50
1
01/25/1819:50
71-55-6
0.50
1
01/25/1819:50
79-00-5
0.50
1
01/25/1819:50
79-01-6
1.0
1
01/25/1819:50
75-69-4
0.50
1
01/25/1819:50
96-18-4
0.50
1
01/25/1819:50
95-63-6
0.50
1
01 /25/18 19:50
108-67-8
1.0
1
01/25/1819:50
75-01-4
1.0
1
01 /25/18 19:50
179601-23-1
0.50
1
01/25/1819:50
95-47-6
70-130
1
01 /25/18 19:50
17060-07-0
70-130
1
01/25/1819:50
460-00-4
70-130
1
01/25/1819:50
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 36

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601
Pace Project No.: 92370403
Sample: MW-8 Lab ID: 92370403008 Collected: 01/21/18 02:00 Received: 01/23/18 11:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method: SM 6200B
Benzene
ND
ug/L
0.50
1
01/25/18 20:07
71-43-2
Bromobenzene
ND
ug/L
0.50
1
01/25/18 20:07
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
01/25/18 20:07
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
01/25/18 20:07
75-27-4
Bromoform
ND
ug/L
0.50
1
01/25/18 20:07
75-25-2
Bromomethane
ND
ug/L
5.0
1
01/25/18 20:07
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
01/25/18 20:07
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
01/25/18 20:07
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
01/25/18 20:07
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
01/25/18 20:07
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
01/25/18 20:07
108-90-7
Chloroethane
ND
ug/L
1.0
1
01/25/18 20:07
75-00-3
Chloroform
ND
ug/L
0.50
1
01/25/18 20:07
67-66-3
Chloromethane
ND
ug/L
1.0
1
01/25/18 20:07
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
01/25/18 20:07
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
01/25/18 20:07
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
01/25/18 20:07
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
01/25/18 20:07
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
01/25/18 20:07
106-93-4
Dibromomethane
ND
ug/L
0.50
1
01/25/18 20:07
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 20:07
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 20:07
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 20:07
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
01/25/18 20:07
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
01/25/18 20:07
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
01/25/18 20:07
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
01/25/18 20:07
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
01/25/18 20:07
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
01/25/18 20:07
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
01/25/18 20:07
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
01/25/18 20:07
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
01/25/18 20:07
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
01/25/18 20:07
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
01/25/18 20:07
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
01/25/18 20:07
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
01/25/18 20:07
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
01/25/18 20:07
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
01/25/18 20:07
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
01/25/18 20:07
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
01/25/18 20:07
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
01/25/18 20:07
1634-04-4
Naphthalene
ND
ug/L
2.0
1
01/25/18 20:07
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
01/25/18 20:07
103-65-1
Styrene
ND
ug/L
0.50
1
01/25/18 20:07
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
01/25/18 20:07
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
01/25/18 20:07
79-34-5
Tetrachloroethene
ND
ug/L
0.50
1
01/25/18 20:07
127-18-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /26/2018 04:57 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 36

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ANALYTICAL RESULTS
Project: 601
Pace Project No.: 92370403
Sample: MW-8 Lab ID: 92370403008 Collected: 01/21/18 02:00 Received: 01/23/18 11:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 01/26/2018 04:57 PM
Analytical Method: SM 6200B
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
98 %
97 %
100 %
0.50
1
01/25/18 20:07
108-88-3
2.0
1
01/25/18 20:07
87-61-6
2.0
1
01/25/18 20:07
120-82-1
0.50
1
01/25/18 20:07
71-55-6
0.50
1
01/25/18 20:07
79-00-5
0.50
1
01/25/18 20:07
79-01-6
1.0
1
01/25/18 20:07
75-69-4
0.50
1
01/25/18 20:07
96-18-4
0.50
1
01/25/18 20:07
95-63-6
0.50
1
01/25/18 20:07
108-67-8
1.0
1
01/25/18 20:07
75-01-4
1.0
1
01/25/18 20:07
179601-23-1
0.50
1
01/25/18 20:07
95-47-6
70-130
1
01/25/18 20:07
17060-07-0
70-130
1
01/25/18 20:07
460-00-4
70-130
1
01/25/18 20:07
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 19 of 36

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ANALYTICAL RESULTS
Project: 601
Pace Project No.: 92370403
Sample: WSW-1 Lab ID: 92370403009 Collected: 01/21/18 12:30 Received: 01/23/18 11:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method: SM 6200B
Benzene
ND
ug/L
0.50
1
01/25/18 20:25
71-43-2
Bromobenzene
ND
ug/L
0.50
1
01/25/18 20:25
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
01/25/18 20:25
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
01/25/18 20:25
75-27-4
Bromoform
ND
ug/L
0.50
1
01/25/18 20:25
75-25-2
Bromomethane
ND
ug/L
5.0
1
01/25/18 20:25
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
01/25/18 20:25
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
01/25/18 20:25
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
01/25/18 20:25
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
01/25/18 20:25
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
01/25/18 20:25
108-90-7
Chloroethane
ND
ug/L
1.0
1
01/25/18 20:25
75-00-3
Chloroform
ND
ug/L
0.50
1
01/25/18 20:25
67-66-3
Chloromethane
ND
ug/L
1.0
1
01/25/18 20:25
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
01/25/18 20:25
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
01/25/18 20:25
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
01/25/18 20:25
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
01/25/18 20:25
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
01/25/18 20:25
106-93-4
Dibromomethane
ND
ug/L
0.50
1
01/25/18 20:25
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 20:25
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 20:25
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
01/25/18 20:25
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
01/25/18 20:25
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
01/25/18 20:25
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
01/25/18 20:25
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
01/25/18 20:25
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
01/25/18 20:25
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
01/25/18 20:25
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
01/25/18 20:25
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
01/25/18 20:25
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
01/25/18 20:25
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
01/25/18 20:25
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
01/25/18 20:25
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
01/25/18 20:25
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
01/25/18 20:25
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
01/25/18 20:25
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
01/25/18 20:25
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
01/25/18 20:25
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
01/25/18 20:25
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
01/25/18 20:25
1634-04-4
Naphthalene
ND
ug/L
2.0
1
01/25/18 20:25
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
01/25/18 20:25
103-65-1
Styrene
ND
ug/L
0.50
1
01/25/18 20:25
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
01/25/18 20:25
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
01/25/18 20:25
79-34-5
Tetrachloroethene
ND
ug/L
0.50
1
01/25/18 20:25
127-18-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /26/2018 04:57 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 36

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: 601
Pace Project No.: 92370403
Sample: WSW-1 Lab ID: 92370403009 Collected: 01/21/18 12:30 Received: 01/23/18 11:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 01/26/2018 04:57 PM
Analytical Method: SM 6200B
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
97 %
100 %
100 %
0.50
1
01/25/18 20:25
108-88-3
2.0
1
01/25/18 20:25
87-61-6
2.0
1
01/25/18 20:25
120-82-1
0.50
1
01/25/18 20:25
71-55-6
0.50
1
01/25/18 20:25
79-00-5
0.50
1
01/25/18 20:25
79-01-6
1.0
1
01/25/18 20:25
75-69-4
0.50
1
01/25/18 20:25
96-18-4
0.50
1
01/25/18 20:25
95-63-6
0.50
1
01/25/18 20:25
108-67-8
1.0
1
01/25/18 20:25
75-01-4
1.0
1
01/25/18 20:25
179601-23-1
0.50
1
01/25/18 20:25
95-47-6
70-130
1
01/25/18 20:25
17060-07-0
70-130
1
01/25/18 20:25
460-00-4
70-130
1
01/25/18 20:25
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 21 of 36

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
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QUALITY CONTROL DATA
Project: 601
Pace Project No.: 92370403
QC Batch: 395524 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Associated Lab Samples: 92370403002, 92370403003, 92370403004, 92370403005, 92370403006, 92370403007, 92370403008,
92370403009
METHOD BLANK: 2192598 Matrix: Water
Associated Lab Samples: 92370403002, 92370403003, 92370403004, 92370403005, 92370403006, 92370403007, 92370403008,
92370403009
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
01/25/18 17:46
1,1,1-Trichloroethane
ug/L
ND
0.50
01/25/18 17:46
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
01/25/18 17:46
1,1,2-Trichloroethane
ug/L
ND
0.50
01/25/18 17:46
1,1-Dichloroethane
ug/L
ND
0.50
01/25/18 17:46
1,1-Dichloroethene
ug/L
ND
0.50
01/25/18 17:46
1,1-Dichloropropene
ug/L
ND
0.50
01/25/18 17:46
1,2,3-Trichlorobenzene
ug/L
ND
2.0
01/25/18 17:46
1,2,3-Trichloropropane
ug/L
ND
0.50
01/25/18 17:46
1,2,4-Trichlorobenzene
ug/L
ND
2.0
01/25/18 17:46
1,2,4-Trimethylbenzene
ug/L
ND
0.50
01/25/18 17:46
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
01/25/18 17:46
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
01/25/18 17:46
1,2-Dichlorobenzene
ug/L
ND
0.50
01/25/18 17:46
1,2-Dichloroethane
ug/L
ND
0.50
01/25/18 17:46
1,2-Dichloropropane
ug/L
ND
0.50
01/25/18 17:46
1,3,5-Trimethylbenzene
ug/L
ND
0.50
01/25/18 17:46
1,3-Dichlorobenzene
ug/L
ND
0.50
01/25/18 17:46
1,3-Dichloropropane
ug/L
ND
0.50
01/25/18 17:46
1,4-Dichlorobenzene
ug/L
ND
0.50
01/25/18 17:46
2,2-Dichloropropane
ug/L
ND
0.50
01/25/18 17:46
2-Chlorotoluene
ug/L
ND
0.50
01/25/18 17:46
4-Chlorotoluene
ug/L
ND
0.50
01/25/18 17:46
Benzene
ug/L
ND
0.50
01/25/18 17:46
Bromobenzene
ug/L
ND
0.50
01/25/18 17:46
Bromochloromethane
ug/L
ND
0.50
01/25/18 17:46
Bromodichloromethane
ug/L
ND
0.50
01/25/18 17:46
Bromoform
ug/L
ND
0.50
01/25/18 17:46
Bromomethane
ug/L
ND
5.0
01/25/18 17:46
Carbon tetrachloride
ug/L
ND
0.50
01/25/18 17:46
Chlorobenzene
ug/L
ND
0.50
01/25/18 17:46
Chloroethane
ug/L
ND
1.0
01/25/18 17:46
Chloroform
ug/L
ND
0.50
01/25/18 17:46
Chloromethane
ug/L
ND
1.0
01/25/18 17:46
cis-1,2-Dichloroethene
ug/L
ND
0.50
01/25/18 17:46
cis-1,3-Dichloropropene
ug/L
ND
0.50
01/25/18 17:46
Dibromochloromethane
ug/L
ND
0.50
01/25/18 17:46
Dibromomethane
ug/L
ND
0.50
01/25/18 17:46
Dichlorodifluoromethane
ug/L
ND
0.50
01/25/18 17:46
Diisopropyl ether
ug/L
ND
0.50
01/25/18 17:46
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 01 /26/2018 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 36

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QUALITY CONTROL DATA
Project: 601
Pace Project No.: 92370403
METHOD BLANK: 2192598 Matrix: Water
Associated Lab Samples: 92370403002, 92370403003, 92370403004, 92370403005, 92370403006, 92370403007, 92370403008,
92370403009
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Ethylbenzene
ug/L
ND
0.50
01/25/18 17:46
Hexachloro-1,3-butadiene
ug/L
ND
2.0
01/25/18 17:46
Isopropylbenzene (Cumene)
ug/L
ND
0.50
01/25/18 17:46
m&p-Xylene
ug/L
ND
1.0
01/25/18 17:46
Methyl-tert-butyl ether
ug/L
ND
0.50
01/25/18 17:46
Methylene Chloride
ug/L
ND
2.0
01/25/18 17:46
n-Butylbenzene
ug/L
ND
0.50
01/25/18 17:46
n-Propylbenzene
ug/L
ND
0.50
01/25/18 17:46
Naphthalene
ug/L
ND
2.0
01/25/18 17:46
o-Xylene
ug/L
ND
0.50
01/25/18 17:46
sec-Butylbenzene
ug/L
ND
0.50
01/25/18 17:46
Styrene
ug/L
ND
0.50
01/25/18 17:46
tert-Butyl benzene
ug/L
ND
0.50
01/25/18 17:46
Tetrachloroethene
ug/L
ND
0.50
01/25/18 17:46
Toluene
ug/L
ND
0.50
01/25/18 17:46
trans-1,2-Dichloroethene
ug/L
ND
0.50
01/25/18 17:46
trans- 1,3-Dichloropropene
ug/L
ND
0.50
01/25/18 17:46
Trichloroethene
ug/L
ND
0.50
01/25/18 17:46
Trichlorofluoromethane
ug/L
ND
1.0
01/25/18 17:46
Vinyl chloride
ug/L
ND
1.0
01/25/18 17:46
1,2-Dichloroethane-d4 (S)
%
95
70-130
01/25/18 17:46
4-Bromofluorobenzene (S)
%
96
70-130
01/25/18 17:46
Toluene-d8 (S)
%
99
70-130
01/25/18 17:46
LABORATORY CONTROL SAMPLE:
Parameter
2192599
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
50
47.1
94
60-140
1,1,1-Trichloroethane
ug/L
50
48.0
96
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
47.0
94
60-140
1,1,2-Trichloroethane
ug/L
50
50.5
101
60-140
1,1-Dichloroethane
ug/L
50
49.0
98
60-140
1,1-Dichloroethene
ug/L
50
53.4
107
60-140
1,1-Dichloropropene
ug/L
50
48.2
96
60-140
1,2,3-Trichlorobenzene
ug/L
50
50.8
102
60-140
1,2,3-Trichloropropane
ug/L
50
67.6
135
60-140
1,2,4-Trichlorobenzene
ug/L
50
52.5
105
60-140
1,2,4-Trimethylbenzene
ug/L
50
49.9
100
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
49.4
99
60-140
1,2-Dibromoethane (EDB)
ug/L
50
49.2
98
60-140
1,2-Dichlorobenzene
ug/L
50
48.6
97
60-140
1,2-Dichloroethane
ug/L
50
47.2
94
60-140
1,2-Dichloropropane
ug/L
50
48.1
96
60-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /26/2018 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 36

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601
Pace Project No.: 92370403
LABORATORY CONTROL SAMPLE:
Parameter
2192599
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3,5-Trimethylbenzene
ug/L
50
49.6
99
60-140
1,3-Dichlorobenzene
ug/L
50
48.9
98
60-140
1,3-Dichloropropane
ug/L
50
48.3
97
60-140
1,4-Dichlorobenzene
ug/L
50
48.2
96
60-140
2,2-Dichloropropane
ug/L
50
52.6
105
60-140
2-Chlorotoluene
ug/L
50
49.1
98
60-140
4-Chlorotoluene
ug/L
50
49.1
98
60-140
Benzene
ug/L
50
48.0
96
60-140
Bromobenzene
ug/L
50
49.7
99
60-140
Bromochloromethane
ug/L
50
49.5
99
60-140
Bromodichloromethane
ug/L
50
47.6
95
60-140
Bromoform
ug/L
50
48.4
97
60-140
Bromomethane
ug/L
50
49.3
99
60-140
Carbon tetrachloride
ug/L
50
47.1
94
60-140
Chlorobenzene
ug/L
50
46.5
93
60-140
Chloroethane
ug/L
50
50.9
102
60-140
Chloroform
ug/L
50
44.3
89
60-140
Chloromethane
ug/L
50
42.9
86
60-140
cis-1,2-Dichloroethene
ug/L
50
50.4
101
60-140
cis-1,3-Dichloropropene
ug/L
50
50.2
100
60-140
Dibromochloromethane
ug/L
50
47.4
95
60-140
Dibromomethane
ug/L
50
49.7
99
60-140
Dichlorodifluoromethane
ug/L
50
43.7
87
60-140
Diisopropyl ether
ug/L
50
51.6
103
60-140
Ethylbenzene
ug/L
50
48.6
97
60-140
Hexachloro-1,3-butadiene
ug/L
50
50.1
100
60-140
Isopropylbenzene (Cumene)
ug/L
50
48.8
98
60-140
m&p-Xylene
ug/L
100
99.9
100
60-140
Methyl-tert-butyl ether
ug/L
50
48.1
96
60-140
Methylene Chloride
ug/L
50
43.1
86
60-140
n-Butylbenzene
ug/L
50
50.2
100
60-140
n-Propylbenzene
ug/L
50
49.6
99
60-140
Naphthalene
ug/L
50
53.4
107
60-140
o-Xylene
ug/L
50
49.0
98
60-140
sec-Butylbenzene
ug/L
50
50.0
100
60-140
Styrene
ug/L
50
48.0
96
60-140
tert-Butyl benzene
ug/L
50
41.0
82
60-140
Tetrachloroethene
ug/L
50
45.6
91
60-140
Toluene
ug/L
50
47.3
95
60-140
trans-1,2-Dichloroethene
ug/L
50
51.6
103
60-140
trans- 1,3-Dichloropropene
ug/L
50
51.5
103
60-140
Trichloroethene
ug/L
50
48.2
96
60-140
Trichlorofluoromethane
ug/L
50
44.5
89
60-140
Vinyl chloride
ug/L
50
49.9
100
60-140
1,2-Dichloroethane-d4 (S)
%
97
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
99
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /26/2018 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 36

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601
Pace Project No.: 92370403
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2192600
2192601
MS
MSD
92370403002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD
Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
1000
1000
1100
1090
110
109
60-140
1
1,1,1-Trichloroethane
ug/L
ND
1000
1000
1150
1170
115
117
60-140
2
1,1,2,2-Tetrachloroethane
ug/L
ND
1000
1000
1010
998
101
100
60-140
2
1,1,2-Trichloroethane
ug/L
ND
1000
1000
1110
1090
111
109
60-140
1
1,1-Dichloroethane
ug/L
ND
1000
1000
1140
1140
114
114
60-140
1
1,1-Dichloroethene
ug/L
ND
1000
1000
1320
1340
132
134
60-140
1
1,1-Dichloropropene
ug/L
ND
1000
1000
1160
1150
116
115
60-140
1
1,2,3-Trichlorobenzene
ug/L
ND
1000
1000
1100
1120
110
112
60-140
2
1,2,3-Trichloropropane
ug/L
ND
1000
1000
1410
1440
141
144
60-140
2 M1
1,2,4-Trichlorobenzene
ug/L
ND
1000
1000
1150
1120
115
112
60-140
2
1,2,4-Trimethylbenzene
ug/L
1760
1000
1000
2920
2920
116
116
60-140
0
1,2-Dibromo-3-chloropropane
ug/L
ND
1000
1000
1020
1030
102
103
60-140
1
1,2-Dibromoethane (EDB)
ug/L
ND
1000
1000
1090
1110
109
111
60-140
2
1,2-Dichlorobenzene
ug/L
ND
1000
1000
1050
1050
105
105
60-140
0
1,2-Dichloroethane
ug/L
ND
1000
1000
1050
1060
105
106
60-140
1
1,2-Dichloropropane
ug/L
ND
1000
1000
1090
1120
109
112
60-140
3
1,3,5-Trimethylbenzene
ug/L
432
1000
1000
1580
1590
115
116
60-140
0
1,3-Dichlorobenzene
ug/L
ND
1000
1000
1090
1100
109
110
60-140
1
1,3-Dichloropropane
ug/L
ND
1000
1000
1070
1080
107
108
60-140
0
1,4-Dichlorobenzene
ug/L
ND
1000
1000
1070
1080
107
108
60-140
1
2,2-Dichloropropane
ug/L
ND
1000
1000
1080
1100
108
110
60-140
2
2-Chlorotoluene
ug/L
ND
1000
1000
1170
1200
117
120
60-140
2
4-Chlorotoluene
ug/L
ND
1000
1000
1130
1110
113
111
60-140
1
Benzene
ug/L
8570
1000
1000
9490
9570
92
100
60-140
1
Bromobenzene
ug/L
ND
1000
1000
1070
1110
107
111
60-140
4
Bromochloromethane
ug/L
ND
1000
1000
1070
1090
107
109
60-140
2
Bromodichloromethane
ug/L
ND
1000
1000
1070
1060
107
106
60-140
1
Bromoform
ug/L
ND
1000
1000
1050
1070
105
107
60-140
2
Bromomethane
ug/L
ND
1000
1000
640
808
64
81
60-140
23
Carbon tetrachloride
ug/L
ND
1000
1000
1200
1180
120
118
60-140
1
Chlorobenzene
ug/L
ND
1000
1000
1090
1070
109
107
60-140
1
Chloroethane
ug/L
ND
1000
1000
1520
1490
152
149
60-140
2 M1
Chloroform
ug/L
ND
1000
1000
1020
1040
102
104
60-140
2
Chloromethane
ug/L
ND
1000
1000
1010
1030
101
103
60-140
1
cis-1,2-Dichloroethene
ug/L
ND
1000
1000
1140
1160
114
116
60-140
2
cis-1,3-Dichloropropene
ug/L
ND
1000
1000
1090
1090
109
109
60-140
0
Dibromochloromethane
ug/L
ND
1000
1000
1030
1050
103
105
60-140
2
Dibromomethane
ug/L
ND
1000
1000
1090
1090
109
109
60-140
0
Dichlorodifluoromethane
ug/L
ND
1000
1000
1020
1050
102
105
60-140
3
Diisopropyl ether
ug/L
3240
1000
1000
4340
4350
110
111
60-140
0
Ethylbenzene
ug/L
2860
1000
1000
3980
3980
112
112
60-140
0
Hexachloro-1,3-butadiene
ug/L
ND
1000
1000
1100
1150
110
115
60-140
4
Isopropylbenzene(Cumene)
ug/L
84.8
1000
1000
1260
1260
118
117
60-140
1
m&p-Xylene
ug/L
5120
2000
2000
7390
7430
114
116
60-140
0
Methyl-tert-butyl ether
ug/L
132
1000
1000
1200
ND
107
-13
60-140
M1
Methylene Chloride
ug/L
ND
1000
1000
991
990
99
99
60-140
0
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /26/2018 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 36

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601
Pace Project No.: 92370403
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2192600
2192601
MS
MSD
92370403002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
ND
1000
1000
1160
1140
116
114
60-140
1
n-Propylbenzene
ug/L
241
1000
1000
1400
1420
116
118
60-140
2
Naphthalene
ug/L
469
1000
1000
1650
1630
118
116
60-140
1
o-Xylene
ug/L
148
1000
1000
1300
1300
116
116
60-140
0
sec-Butylbenzene
ug/L
ND
1000
1000
1210
1210
121
121
60-140
0
Styrene
ug/L
ND
1000
1000
1120
1110
112
111
60-140
1
tert-Butyl benzene
ug/L
ND
1000
1000
967
974
97
97
60-140
1
Tetrachloroethene
ug/L
ND
1000
1000
1080
1140
108
114
60-140
6
Toluene
ug/L
174
1000
1000
1270
1290
110
112
60-140
1
trans-1,2-Dichloroethene
ug/L
ND
1000
1000
1210
1210
121
121
60-140
0
trans- 1,3-Dichloropropene
ug/L
ND
1000
1000
1050
1080
105
108
60-140
3
Trichloroethene
ug/L
ND
1000
1000
1160
1150
116
115
60-140
0
Trichlorofluoromethane
ug/L
ND
1000
1000
1130
1080
113
108
60-140
4
Vinyl chloride
ug/L
ND
1000
1000
1230
1230
123
123
60-140
1
1,2-Dichloroethane-d4 (S)
%
96
97
70-130
4-Bromofluorobenzene (S)
%
103
100
70-130
Toluene-d8(S)
%
100
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /26/2018 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 36

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601
Pace Project No.: 92370403
QC Batch: 395556 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Associated Lab Samples: 92370403001
METHOD BLANK: 2192874
Associated Lab Samples: 92370403001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
01/26/18 02:33
1,1,1-Trichloroethane
ug/L
ND
0.50
01/26/18 02:33
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
01/26/18 02:33
1,1,2-Trichloroethane
ug/L
ND
0.50
01/26/18 02:33
1,1-Dichloroethane
ug/L
ND
0.50
01/26/18 02:33
1,1-Dichloroethene
ug/L
ND
0.50
01/26/18 02:33
1,1-Dichloropropene
ug/L
ND
0.50
01/26/18 02:33
1,2,3-Trichlorobenzene
ug/L
ND
2.0
01/26/18 02:33
1,2,3-Trichloropropane
ug/L
ND
0.50
01/26/18 02:33
1,2,4-Trichlorobenzene
ug/L
ND
2.0
01/26/18 02:33
1,2,4-Trimethylbenzene
ug/L
ND
0.50
01/26/18 02:33
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
01/26/18 02:33
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
01/26/18 02:33
1,2-Dichlorobenzene
ug/L
ND
0.50
01/26/18 02:33
1,2-Dichloroethane
ug/L
ND
0.50
01/26/18 02:33
1,2-Dichloropropane
ug/L
ND
0.50
01/26/18 02:33
1,3,5-Trimethylbenzene
ug/L
ND
0.50
01/26/18 02:33
1,3-Dichlorobenzene
ug/L
ND
0.50
01/26/18 02:33
1,3-Dichloropropane
ug/L
ND
0.50
01/26/18 02:33
1,4-Dichlorobenzene
ug/L
ND
0.50
01/26/18 02:33
2,2-Dichloropropane
ug/L
ND
0.50
01/26/18 02:33
2-Chlorotoluene
ug/L
ND
0.50
01/26/18 02:33
4-Chlorotoluene
ug/L
ND
0.50
01/26/18 02:33
Benzene
ug/L
ND
0.50
01/26/18 02:33
Bromobenzene
ug/L
ND
0.50
01/26/18 02:33
Bromochloromethane
ug/L
ND
0.50
01/26/18 02:33
Bromodichloromethane
ug/L
ND
0.50
01/26/18 02:33
Bromoform
ug/L
ND
0.50
01/26/18 02:33
Bromomethane
ug/L
ND
5.0
01/26/18 02:33
Carbon tetrachloride
ug/L
ND
0.50
01/26/18 02:33
Chlorobenzene
ug/L
ND
0.50
01/26/18 02:33
Chloroethane
ug/L
ND
1.0
01/26/18 02:33
Chloroform
ug/L
ND
0.50
01/26/18 02:33
Chloromethane
ug/L
ND
1.0
01/26/18 02:33
cis-1,2-Dichloroethene
ug/L
ND
0.50
01/26/18 02:33
cis-1,3-Dichloropropene
ug/L
ND
0.50
01/26/18 02:33
Dibromochloromethane
ug/L
ND
0.50
01/26/18 02:33
Dibromomethane
ug/L
ND
0.50
01/26/18 02:33
Dichlorodifluoromethane
ug/L
ND
0.50
01/26/18 02:33
Diisopropyl ether
ug/L
ND
0.50
01/26/18 02:33
Ethylbenzene
ug/L
ND
0.50
01/26/18 02:33
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /26/2018 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 36

aceAnalytical
-pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601
Pace Project No.: 92370403
METHOD BLANK: 2192874
Associated Lab Samples: 92370403001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
2.0
01/26/18 02:33
Isopropylbenzene (Cumene)
ug/L
ND
0.50
01/26/18 02:33
m&p-Xylene
ug/L
ND
1.0
01/26/18 02:33
Methyl-tert-butyl ether
ug/L
ND
0.50
01/26/18 02:33
Methylene Chloride
ug/L
ND
2.0
01/26/18 02:33
n-Butylbenzene
ug/L
ND
0.50
01/26/18 02:33
n-Propylbenzene
ug/L
ND
0.50
01/26/18 02:33
Naphthalene
ug/L
ND
2.0
01/26/18 02:33
o-Xylene
ug/L
ND
0.50
01/26/18 02:33
sec-Butylbenzene
ug/L
ND
0.50
01/26/18 02:33
Styrene
ug/L
ND
0.50
01/26/18 02:33
tert-Butyl benzene
ug/L
ND
0.50
01/26/18 02:33
Tetrachloroethene
ug/L
ND
0.50
01/26/18 02:33
Toluene
ug/L
ND
0.50
01/26/18 02:33
trans-1,2-Dichloroethene
ug/L
ND
0.50
01/26/18 02:33
trans- 1,3-Dichloropropene
ug/L
ND
0.50
01/26/18 02:33
Trichloroethene
ug/L
ND
0.50
01/26/18 02:33
Trichlorofluoromethane
ug/L
ND
1.0
01/26/18 02:33
Vinyl chloride
ug/L
ND
1.0
01/26/18 02:33
1,2-Dichloroethane-d4 (S)
%
95
70-130
01/26/18 02:33
4-Bromofluorobenzene (S)
%
97
70-130
01/26/18 02:33
Toluene-d8 (S)
%
102
70-130
01/26/18 02:33
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2192875
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
47.0
94
60-140
1,1,1-Trichloroethane
ug/L
50
45.1
90
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
46.4
93
60-140
1,1,2-Trichloroethane
ug/L
50
49.0
98
60-140
1,1-Dichloroethane
ug/L
50
47.0
94
60-140
1,1-Dichloroethene
ug/L
50
52.8
106
60-140
1,1-Dichloropropene
ug/L
50
45.0
90
60-140
1,2,3-Trichlorobenzene
ug/L
50
46.4
93
60-140
1,2,3-Trichloropropane
ug/L
50
49.6
99
60-140
1,2,4-Trichlorobenzene
ug/L
50
46.2
92
60-140
1,2,4-Trimethylbenzene
ug/L
50
45.6
91
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
45.4
91
60-140
1,2-Dibromoethane (EDB)
ug/L
50
49.1
98
60-140
1,2-Dichlorobenzene
ug/L
50
46.8
94
60-140
1,2-Dichloroethane
ug/L
50
50.1
100
60-140
1,2-Dichloropropane
ug/L
50
47.5
95
60-140
1,3,5-Trimethylbenzene
ug/L
50
45.6
91
60-140
1,3-Dichlorobenzene
ug/L
50
45.3
91
60-140
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /26/2018 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 36

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601
Pace Project No.: 92370403
LABORATORY CONTROL SAMPLE:
Parameter
2192875
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichloropropane
ug/L
50
49.3
99
60-140
1,4-Dichlorobenzene
ug/L
50
44.5
89
60-140
2,2-Dichloropropane
ug/L
50
42.1
84
60-140
2-Chlorotoluene
ug/L
50
44.8
90
60-140
4-Chlorotoluene
ug/L
50
44.9
90
60-140
Benzene
ug/L
50
47.1
94
60-140
Bromobenzene
ug/L
50
45.6
91
60-140
Bromochloromethane
ug/L
50
49.1
98
60-140
Bromodichloromethane
ug/L
50
46.9
94
60-140
Bromoform
ug/L
50
45.4
91
60-140
Bromomethane
ug/L
50
43.1
86
60-140
Carbon tetrachloride
ug/L
50
48.1
96
60-140
Chlorobenzene
ug/L
50
46.5
93
60-140
Chloroethane
ug/L
50
49.6
99
60-140
Chloroform
ug/L
50
47.9
96
60-140
Chloromethane
ug/L
50
40.7
81
60-140
cis-1,2-Dichloroethene
ug/L
50
47.1
94
60-140
cis-1,3-Dichloropropene
ug/L
50
47.7
95
60-140
Dibromochloromethane
ug/L
50
48.4
97
60-140
Dibromomethane
ug/L
50
50.7
101
60-140
Dichlorodifluoromethane
ug/L
50
38.9
78
60-140
Diisopropyl ether
ug/L
50
47.4
95
60-140
Ethylbenzene
ug/L
50
47.2
94
60-140
Hexachloro-1,3-butadiene
ug/L
50
46.1
92
60-140
Isopropylbenzene (Cumene)
ug/L
50
47.7
95
60-140
m&p-Xylene
ug/L
100
93.8
94
60-140
Methyl-tert-butyl ether
ug/L
50
46.9
94
60-140
Methylene Chloride
ug/L
50
42.2
84
60-140
n-Butylbenzene
ug/L
50
43.9
88
60-140
n-Propylbenzene
ug/L
50
45.0
90
60-140
Naphthalene
ug/L
50
48.0
96
60-140
o-Xylene
ug/L
50
46.9
94
60-140
sec-Butylbenzene
ug/L
50
45.7
91
60-140
Styrene
ug/L
50
47.3
95
60-140
tert-Butyl benzene
ug/L
50
39.5
79
60-140
Tetrachloroethene
ug/L
50
46.7
93
60-140
Toluene
ug/L
50
47.1
94
60-140
trans-1,2-Dichloroethene
ug/L
50
50.0
100
60-140
trans- 1,3-Dichloropropene
ug/L
50
45.7
91
60-140
Trichloroethene
ug/L
50
50.5
101
60-140
Trichlorofluoromethane
ug/L
50
43.2
86
60-140
Vinyl chloride
ug/L
50
46.5
93
60-140
1,2-Dichloroethane-d4 (S)
%
98
70-130
4-Bromofluorobenzene (S)
%
102
70-130
Toluene-d8 (S)
%
100
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /26/2018 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 36

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601
Pace Project No.: 92370403
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2192876
2192877
MS
MSD
92370364010
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD
Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
20.8
21.2
104
106
60-140
2
1,1,1-Trichloroethane
ug/L
ND
20
20
21.7
21.7
109
108
60-140
0
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
17.2
20.7
86
104
60-140
18
1,1,2-Trichloroethane
ug/L
ND
20
20
19.4
20.7
97
103
60-140
7
1,1-Dichloroethane
ug/L
ND
20
20
21.7
22.0
109
110
60-140
1
1,1-Dichloroethene
ug/L
ND
20
20
25.2
25.1
126
126
60-140
0
1,1-Dichloropropene
ug/L
ND
20
20
22.0
22.0
110
110
60-140
0
1,2,3-Trichlorobenzene
ug/L
ND
20
20
20.8
21.7
104
109
60-140
4
1,2,3-Trichloropropane
ug/L
ND
20
20
17.2
21.3
86
106
60-140
21
1,2,4-Trichlorobenzene
ug/L
ND
20
20
21.3
21.6
106
108
60-140
2
1,2,4-Trimethylbenzene
ug/L
ND
20
20
22.0
21.0
110
105
60-140
5
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
14.7
19.8
73
99
60-140
30
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
19.2
21.3
96
106
60-140
10
1,2-Dichlorobenzene
ug/L
ND
20
20
20.8
21.0
104
105
60-140
1
1,2-Dichloroethane
ug/L
ND
20
20
21.0
23.3
105
116
60-140
10
1,2-Dichloropropane
ug/L
ND
20
20
20.1
20.7
101
103
60-140
3
1,3,5-Trimethylbenzene
ug/L
ND
20
20
22.0
20.8
110
104
60-140
6
1,3-Dichlorobenzene
ug/L
ND
20
20
20.9
20.8
105
104
60-140
1
1,3-Dichloropropane
ug/L
ND
20
20
20.0
22.2
100
111
60-140
11
1,4-Dichlorobenzene
ug/L
ND
20
20
20.5
20.2
102
101
60-140
1
2,2-Dichloropropane
ug/L
ND
20
20
22.5
22.3
112
111
60-140
1
2-Chlorotoluene
ug/L
ND
20
20
21.3
20.6
106
103
60-140
3
4-Chlorotoluene
ug/L
ND
20
20
21.4
20.7
107
104
60-140
3
Benzene
ug/L
0.66
20
20
21.6
21.5
105
104
60-140
0
Bromobenzene
ug/L
ND
20
20
21.0
20.7
105
104
60-140
1
Bromochloromethane
ug/L
ND
20
20
20.1
21.9
101
110
60-140
9
Bromodichloromethane
ug/L
ND
20
20
19.8
20.5
99
102
60-140
3
Bromoform
ug/L
ND
20
20
16.4
17.3
82
86
60-140
5
Bromomethane
ug/L
ND
20
20
18.4
21.0
92
105
60-140
13
Carbon tetrachloride
ug/L
ND
20
20
23.2
22.7
116
114
60-140
2
Chlorobenzene
ug/L
ND
20
20
21.7
21.6
108
108
60-140
0
Chloroethane
ug/L
ND
20
20
23.6
24.7
118
124
60-140
5
Chloroform
ug/L
ND
20
20
21.6
21.8
108
109
60-140
1
Chloromethane
ug/L
ND
20
20
21.1
21.3
105
107
60-140
1
cis-1,2-Dichloroethene
ug/L
9.3
20
20
31.1
31.5
109
111
60-140
1
cis-1,3-Dichloropropene
ug/L
ND
20
20
20.1
20.8
100
104
60-140
3
Dibromochloromethane
ug/L
ND
20
20
19.2
20.3
96
102
60-140
6
Dibromomethane
ug/L
ND
20
20
19.4
21.8
97
109
60-140
12
Dichlorodifluoromethane
ug/L
ND
20
20
23.6
23.6
118
118
60-140
0
Diisopropyl ether
ug/L
ND
20
20
19.8
20.8
99
104
60-140
5
Ethylbenzene
ug/L
ND
20
20
22.5
21.7
112
109
60-140
4
Hexachloro-1,3-butadiene
ug/L
ND
20
20
24.3
23.3
122
116
60-140
4
Isopropylbenzene (Cumene)
ug/L
ND
20
20
22.5
22.0
112
110
60-140
2
m&p-Xylene
ug/L
ND
40
40
44.4
43.9
111
110
60-140
1
Methyl-tert-butyl ether
ug/L
ND
20
20
18.3
21.2
92
106
60-140
15
Methylene Chloride
ug/L
ND
20
20
18.8
20.1
94
101
60-140
7
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /26/2018 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 36

aceAnalytical
—pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: 601
Pace Project No.: 92370403
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2192876
2192877
MS
MSD
92370364010
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
ND
20
20
22.7
21.2
113
106
60-140
7
n-Propylbenzene
ug/L
ND
20
20
22.6
21.1
113
106
60-140
7
Naphthalene
ug/L
ND
20
20
18.0
21.4
90
107
60-140
17
o-Xylene
ug/L
ND
20
20
21.7
21.2
109
106
60-140
2
sec-Butylbenzene
ug/L
ND
20
20
23.3
21.6
117
108
60-140
8
Styrene
ug/L
ND
20
20
21.1
21.3
106
107
60-140
1
tert-Butyl benzene
ug/L
ND
20
20
19.5
18.1
97
91
60-140
7
Tetrachloroethene
ug/L
21.5
20
20
44.7
44.6
116
116
60-140
0
Toluene
ug/L
ND
20
20
21.9
21.5
109
107
60-140
2
trans-1,2-Dichloroethene
ug/L
ND
20
20
24.1
23.3
120
117
60-140
3
trans- 1,3-Dichloropropene
ug/L
ND
20
20
18.9
20.2
94
101
60-140
6
Trichloroethene
ug/L
4.4
20
20
27.5
27.7
115
117
60-140
1
Trichlorofluoromethane
ug/L
ND
20
20
21.2
21.5
106
108
60-140
1
Vinyl chloride
ug/L
ND
20
20
23.9
24.1
119
120
60-140
1
1,2-Dichloroethane-d4 (S)
%
90
99
70-130
4-Bromofluorobenzene (S)
%
99
103
70-130
Toluene-d8(S)
%
100
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /26/2018 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 36

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: 601
Pace Project No.: 92370403
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 01 /26/2018 04:57 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 36

aceAnalytical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: 601
Pace Project No.: 92370403
Lab ID
Sample ID
QC
Batch Method
QC Batch
92370403001
MW-1
SM
6200B
395556
92370403002
MW-2
SM
6200B
395524
92370403003
MW-3
SM
6200B
395524
92370403004
MW-4
SM
6200B
395524
92370403005
MW-5
SM
6200B
395524
92370403006
MW-6
SM
6200B
395524
92370403007
MW-7
SM
6200B
395524
92370403008
MW-8
SM
6200B
395524
92370403009
WSW-1
SM
6200E
395524
Date: 01/26/2018 04:57 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical Method
Analytical
Batch
Page 33 of 36

Document Name: Document Revised: August 4, 2017
27cmnaVical
Sample Condition Upon Receipt(SCUR) Page 1 of 2
Document No.: Issuing Authority:
F-CAR-CS-033-Rev.04 Pace Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[—]
t Name:
Courier: LJFed Ex
❑ Commercial ❑Pace
Greenwood ❑ HuntersvilWe[]--° —� Raleigh[:] Mechanicsville[]
] Project ff: W0# : 92370403
❑Other: rertt�
II I III I II I I I I i�l� III
�� 92370403
Custody Seal Present? Elves�A►a� Seals Intact? Elves -Rro
Date/Initials Person Examining Contents:
Packing Material: ❑Bubble Wrap ❑Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: J nlD: []Yes ❑No QPI/A'
plat —[JBlue ❑None
�FRC,uT eoflcg:
Correction Factor: ooler Temp orrected VC): t7ti G Temp should be above freezing to VC
❑Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil'EQ"RTA7-water sample]
Did samples originatein a quarantine zone within the United States: CA, NY, or SC (check maps)7 Did samples originate from a foreign source (internationally,
I�Ypc "I INn inrli,dinc Hawaii and Pnprtn nirn17F-1)(ac r {"INA
Comments/Discrepancy:
Chain of Custody Present?
s
❑No ❑N/A
1.
Samples Arrived within Hold Time?
-r
.• QYas
❑No []N/A
2.
Short Hold Time Analysis (<72 hr,l?
❑Yes Qftr• ❑N/A
3.
Rush Turn Around Time Requested?
es ­
[]No ❑N/A
4.
Sufficient Volume?
es
❑No ❑N/A
S.
Correct Containers used?
-Pace Containers Used?
Yes
QJI-Tr
❑No ❑N/A
❑No ❑N/A
6.
Containers Intact?
es
[-]No ❑N/A
7.
Dissolved analysis: Samples Field Htered?
❑Yes
No
g.
Sample Labels Match COC?
-includes Date/Time/ID/Analysis Matrix:
es
[]NO ❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
[-]Yes �--EJ1T---0NIA
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
�o ❑N/A
❑No /A
11.
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample Discrepancy:
Lot ID of split containers:
Date/Time:
Field Data Required? LIYes LjNo
Project Manager SCURF Review: r Date: 0 f 4S 1
Project Manager SRF Review: _ Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will he sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Page 34 of 36

Document Name:
Document Revised: August 4, 2017
22,417aVical
Sample Condition Upon Receipt(SOUR)
Page 2 of 2
Document No.:
issuing Authority
F-CAR-CS•033-Rev.04
Pace Quality Office
*Check mark top half of box if pH and/or dechlorination
Project # wog
: g2370403
is verified and within the acceptance range for
preservation samples.
PM:
NMG
Due Date:
02/06/18
"Bottom half of box is to list number of bottles
CLIENT:
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