22074_Gathing Motos_Final Shallow Soil - East Office Tower

‘Wood’ is a trading name for John Wood Group PLC and its subsidiaries
REPORT OF SOIL CHARACTERIZATION FOR BENEFICIAL REUSE
SHALLOW SOIL (EAST OFFICE BUILDING)
FORMER GATHINGS MOTOR COMPANY
1100 and 1200 South Tryon Street
Charlotte, North Carolina
Brownfields Project Number 22074-18-060
PREPARED FOR:
TRYON STREET INVESTORS, LLC
Care of Spectrum Development Company, LLC
300 South Tryon Street, Ste. 200
Charlotte, North Carolina 28202
PREPARED BY:
WOOD ENVIRONMENT & INFRASTRUCTURE SOLUTIONS,INC.
2801 Yorkmont Road, Suite 100
Charlotte, North Carolina 28208
JANUARY 23, 2020
Report of Soil Characterization for Beneficial Reuse –Shallow Soil (East Office Tower)January 23, 2020
Former Gathings Motor Company
1100 and 1200 South Tryon Street, Charlotte, North Carolina
Wood Project Number: 6228-18-0495
ii
TABLE OF CONTENTS
1.0 PROJECT INFORMATION AND PURPOSE...........................................................................................................................1
2.0 ASSESSMENT ACTIVITIES..........................................................................................................................................................2
2.1 Boring Layout and Underground Utility Survey...................................................................................................2
2.2 Soil Sampling and Analyses.........................................................................................................................................2
3.0 RESULTS...........................................................................................................................................................................................3
3.1 Volatile Organic Compounds ......................................................................................................................................3
3.2 Semi-Volatile Organic Compounds ..........................................................................................................................4
3.3 Total Metals........................................................................................................................................................................4
3.4 Leachability (TCLP)...........................................................................................................................................................5
4.0 CONCLUSIONS AND RECOMMENDATIONS.....................................................................................................................5
LIST OF TABLES
Table 1 Soil Sampling Analysis Plan –Shallow Soil (East Office Building)
Table 2 Summary of Detected Volatile Organic Compounds (VOCs)
Analytical Results –Shallow Soil (East Office Building)
Table 3 Summary of Detected Semi-Volatile Organic Compounds (SVOC)
and Total Metal Analytical Results –Shallow Soil (East Office Building)
Table 4 Summary of Detected Toxicity Characteristic Leaching Procedure Analytical Results –
Shallow Soil (East Office Building)
LIST OF FIGURES
Figure 1 Site Topo
Figure 2 Sampling Grid on Cut/Fill Plan
LIST OF APPENDICES
Appendix A Laboratory Analytical Reports and Chain-of-Custody Forms
Report of Soil Characterization for Beneficial Reuse –Shallow Soil (East Office Tower)January 23, 2020
Former Gathings Motor Company
1100 and 1200 South Tryon Street, Charlotte, North Carolina
Wood Project Number: 6228-18-0495
1
1.0 PROJECT INFORMATION AND PURPOSE
The subject site consists of four parcels encompassing approximately 4.9 acres situated at the intersection
of South Tryon Street and West Carson Boulevard in Charlotte, North Carolina (Figure 1). Under separate
work plans, Wood previous performed shallow and deep soil characterization of soil that was to be
generated during the construction of the propose West Office Tower on the western portion of the site
and the Parking Garage on the southern portion of the site.
The Prospective Developer (PD) recently provided information regarding soil that will be graded related to
the proposed East Office Tower which will eventually be constructed on the eastern portion of the site.
Historical information reviewed by Wood indicates that the land area to be redeveloped as the East Office
Tower was formerly occupied by a gasoline station (Top Gas & Oil, 1100 and 1120 South Tryon Street)
from at least 1960 to 1986. Review of a regulatory database report revealed that the site was identified on
the leaking underground storage tank (LUST) and underground storage tank (UST) lists. The site was also
identified on the Historical Auto Stations list as Tops of Charlotte (1100 & 1120 South Tryon Street) for
the years 1959, 1964, 1969, 1974, 1979 and 1984.The purpose of the soil characterization is to evaluate if
concentrations of contaminants are identified in the soil to be exported that exceed the Inactive
Hazardous Sites Branch (IHSB) Preliminary Soil Remediation Goals (PSRGs) for Health Based Residential or
Protection of Groundwater (PoG).
According to the cut/fill analysis provided to Wood the grading activities will include an average of two to
four feet of soil to be removed across this portion of the site. The estimated volume of soil to be graded is
approximately 2,100 cubic yards.This assessment does not include characterization of the soil to be
generated during drilling of the foundation shafts for the proposed East Office Tower.
Wood developed a written work plan (dated November 26, 2019) to characterize the shallow soil to be
removed for beneficial reuse and submitted the work plan to the North Carolina Department of
Environmental Quality (NCDEQ), Brownfields Program (BFP) for review. Ms. Carolyn Minnich of the BFP
approved the work plan on December 5, 2019.The assessment activities were performed in general
accordance with the most recent Inactive Hazardous Sites Branch (IHSB) Program Guidelines for
Assessment and Cleanup (http://portal.ncdenr.org/web/wm/sf/ihs/ihsguide), dated October 2015 and the
most recent versions of the U.S. Environmental Protection Agency (EPA) Region IV Science and Ecosystem
Support Division (SESD) Field Branches Quality System and Technical Procedures guidance.
Report of Soil Characterization for Beneficial Reuse –Shallow Soil (East Office Tower)January 23, 2020
Former Gathings Motor Company
1100 and 1200 South Tryon Street, Charlotte, North Carolina
Wood Project Number: 6228-18-0495
2
2.0 ASSESSMENT ACTIVITIES
2.1 Boring Layout and Underground Utility Survey
In the work plan, Wood proposed to advance one soil boring within a 30 x 30 foot grid pattern (Figure 2)
on the eastern portion of the site. A total of 27 shallow borings were advanced within the area to be
affected by mass grading and were “grouped” into three sample “block” areas (Block IDs 11, 12, and 13) as
shown on the figure. Block IDs 1 through 10 were completed earlier in 2019 prior to the grading
operations for the West Office Tower and Parking Garage.The soil assessment/characterization effort was
planned to evaluate the depth horizon beginning at the existing grade and extending to five feet or less
below the existing grade for the presence of contaminants.The boring locations were approved by the
BFP and were marked in the field and recorded on a Trimble GeoExplorer XH 6000 Series hand-held
Global Positioning System (GPS) unit for future reference.
Prior to conducting the soil assessment activities, Wood contacted the North Carolina 811 public
underground utility location service. Furthermore, on December 5, 2019, Wood personnel visited the site
to perform Ground-Penetrating Radar (GPR) and Electromagnetic (EM) surveys to attempt to detect
metallic objects such as pipes, tanks or underground utility lines. The purpose of this effort was to
minimize the potential for probing into underground utilities buried at the properties.
2.2 Soil Sampling and Analyses
On December 9, 2019, Wood personnel and Carolina Soil Investigations, LLC (CSI), our probing
subcontractor licensed in the State of North Carolina, mobilized to the site to advance soil borings
approved by the BFP. CSI advanced a MacroCore®soil sampler to a depth of five feet below existing
grade at each boring location using Geoprobe®6610 direct-push rig.To minimize the potential for cross-
contamination between samples, a new polyvinyl chloride (PVC) sleeve (tube) was inserted into the
sampler for each soil boring. Wood field personnel collected soil cores from the sleeve at each boring
location from the depth range shown on the cut/fill analysis (see Table 1). Visual and olfactory
observations and the soil types relative to the soil samples were recorded by our field personnel.
To select “discrete” samples that were retained for analysis of Volatile Organic Compounds (VOCs), Wood
personnel donned a new pair of nitrile gloves and split the soil core removed from the liner longitudinally.
A representative portion of one-half of the sample was placed directly in VOC sample containers and the
remaining half was placed in a re-sealable plastic bag to be screened in the field using an Organic Vapor
Analyzer (OVA) equipped with a flame ionization detector (FID). The results of the field screening were
recorded by field personnel and ranged from 0.05 parts per million (ppm)to 5.57 ppm Based on the
Report of Soil Characterization for Beneficial Reuse –Shallow Soil (East Office Tower)January 23, 2020
Former Gathings Motor Company
1100 and 1200 South Tryon Street, Charlotte, North Carolina
Wood Project Number: 6228-18-0495
3
results of the field screening, one “discrete” sample per block area was selected for laboratory analysis for
VOCs using EPA Method 8260B.
Regarding the samples that were retained for analysis of Semi-volatile Organic Compounds (SVOCs) and
total metals, the remaining representative portions of the soil cores collected from the appropriate depth
interval were placed in laboratory sample containers. These “discrete” samples were combined in the
laboratory by laboratory personnel as a “composite” sample (11-COMP, 12-COMP, and 13-COMP)as
shown on Table 1. Each “composite” soil sample was placed into laboratory-provided containers for
analysis of SVOCs by EPA Method 8270E,Resource Conservation and Recovery Act (RCRA) Metals (total)
by EPA Method 6020B/7471B, and hexavalent chromium (Cr VI) by EPA Method 7199. The soil samples
were placed in a cooler with ice and shipped to Con-Test Analytical Laboratory (Con-Test) in East
Longmeadow, Massachusetts. Soil samples were maintained under a chain-of-custody protocol.A soil
field duplicate QA/QC sample (Dup-1)was collected and analyzed for VOCs.A soil field duplicate QA/QC
sample (Dup-2)was composited by laboratory personnel and analyzed for SVOCs and total metals. One
trip blank was analyzed for VOCs.In addition, “composite” sample 12-COMP was analyzed by the Toxicity
Characteristic Leaching Procedure (TCLP) for VOC, SVOC and the 8 RCRA metals, and “composite” samples
11-COMP and 13-COMP were analyzed by TCLP for mercury.
Following the completion of the soil sampling activities, the borings were backfilled with the soil cores
and/or bentonite to the ground surface.
3.0 RESULTS
The results of the laboratory analyses are summarized on Tables 2,3 and 4. The laboratory analytical
reports and chain-of-custody forms are included as Appendix A to this report. The following subsections
include discussion of the findings.
3.1 Volatile Organic Compounds
The results of the laboratory analysis for VOCs are summarized on Table 2.No detectable concentrations
were identified in the “discrete” samples collected from Block 11 (sample 11-2) and Block 13 (sample 13-
7). Several VOC concentrations were identified in the sample collected from Block 12 (sample 12-4).
However, none of the concentrations exceeded their respective IHSB PSRGs for Health Based Residential,
Health Based Industrial/Commercial or PoG.Furthermore, three of the concentrations were J-flagged,
indicating the concentrations were identified at a level above the method detection limit (MDL), but below
the reporting limit (RL) and is considered an estimate.
Report of Soil Characterization for Beneficial Reuse –Shallow Soil (East Office Tower)January 23, 2020
Former Gathings Motor Company
1100 and 1200 South Tryon Street, Charlotte, North Carolina
Wood Project Number: 6228-18-0495
4
3.2 Semi-Volatile Organic Compounds
The results of the laboratory analysis for SVOCs are summarized on Table 3. No detectable
concentrations were identified in the “composite” sample collected from Block 11 (sample 11-COMP) and
no detectable concentrations other than fluoranthene was identified in the “composite” sample collected
from Block 13 (sample 13-COMP). In addition, the concentration of fluoranthene identified in sample 13-
COMP was J-flagged and did not exceed the IHSB PSRGs.
Several SVOC concentrations were identified in the “composite” sample collected from Block 12 (sample
12-COMP). However,with the exception of benzo(a)pyrene,none of the concentrations identified
exceeded their respective IHSB PSRGs.The concentration of benzo(a)pyrene identified in sample 12-
COMP was J-flagged and exceeded the IHSB Health Based Residential and PoG PSRGs for benzo(a)pyrene.
3.3 Total Metals
The results of the laboratory analysis for total metals are summarized on Table 3. The analysis identified
the following:
Varying concentrations of total barium, cadmium, lead, mercury, selenium and silver were
identified in “composite”soil samples collected for this assessment. None of the concentrations
exceeded either the IHSB Health Based Residential, Health Based Industrial/Commercial or PoG
PSRGs.
Detectable concentrations of total arsenic ranging from 0.76 milligrams per kilogram (mg/kg)to
2.3 mg/kg were identified in the “composite” soil samples collected for this assessment.These
concentrations exceeded the IHSB Health Based Residential PSRG of 0.68 mg/kg, but did not
exceed the IHSB, Health Based Industrial/Commercial or PoG PSRGs. According to published
literature, these concentrations are within the typical range of “naturally-occurring” arsenic levels
in soil in the Piedmont of North Carolina.
Detectable concentrations of total chromium ranging from 8.0 to 23 mg/kg were identified in the
“composite” soil samples collected for this assessment.In addition, no detectable concentrations
of Cr VI were identified in the “composite” samples. Based on the results of the Cr VI analysis, the
total chromium concentrations identified during this assessment could be classified as trivalent
chromium (Cr III). In addition, according to published literature, the concentrations of total
chromium are within the typical range of “naturally-occurring” arsenic levels in soil in the
Piedmont of North Carolina.
Report of Soil Characterization for Beneficial Reuse –Shallow Soil (East Office Tower)January 23, 2020
Former Gathings Motor Company
1100 and 1200 South Tryon Street, Charlotte, North Carolina
Wood Project Number: 6228-18-0495
5
3.4 Leachability (TCLP)
The results of the TCLP laboratory analysis are summarized on Table 4. No detectable leachable mercury
concentrations were identified in “composite” samples 11-COMP and 13-COMP. No detectable leachable
VOC and SVOC concentrations were identified in “composite” sample 12-COMP.Leachable concentrations
of barium, chromium, and lead were identified in sample 12-COMP. However, the concentrations were J-
flagged and did not exceed their respective EPA Maximum Concentrations of Contaminant for the Toxicity
Characteristic.
4.0 CONCLUSIONS AND RECOMMENDATIONS
Based on the findings of this assessment, Wood offers the following conclusions and recommendations:
The 27 borings advanced in the area of the proposed East Office Tower did not encounter areas
of debris fill that should not be considered soil.
None of the VOC concentrations detected in the “discrete” soil samples exceeded their respective
IHSB Health Based Residential, Health Based Industrial/Commercial or PoG PSRGs.
Benzo(a)pyrene was identified in “composite” sample 12-COMP at a J-flagged concentration
which exceeded the IHSB Health Based Residential and PoG PSRGs for benzo(a)pyrene. No other
SVOC concentrations detected in the soil samples exceeded their respective IHSB PSRGs.
Arsenic concentrations were identified in the “composite” soil samples which exceeded the IHSB
Health Based Residential PSRG for arsenic, but did not exceed the IHSB, Health Based
Industrial/Commercial or PoG PSRGs. In addition,the concentrations are within the typical range
of “naturally-occurring” arsenic levels in soil in the Piedmont of North Carolina.
No detectable concentrations of Cr VI were identified in the “composite” soil samples and
therefore the total chromium concentrations identified in the three “composite” soil samples
could be classified as Cr III.
Based on the results of this assessment,the soil in the area of the proposed East Office Tower
could be used as fill material at the subject property or transported to another Brownfields
property (contingent on approval of the BFP and property owner/recipient) if the use of the
affected soil as beneficial fill will not increase the potential for risk to human health at that site.
Furthermore, the BFP may approve relocation of material that meets the Beneficial Fill Rule to
non-Brownfields properties.
Report of Soil Characterization for Beneficial Reuse –Shallow Soil (East Office Tower)January 23, 2020
Former Gathings Motor Company
1100 and 1200 South Tryon Street, Charlotte, North Carolina
Wood Project Number: 6228-18-0495
TABLES
Block ID Boring ID Boring Depth
(Feet, BGS)
"Discrete"
Sample IDs
Sample Depth
Intervals
(Feet, BGS)
Analytical Parameters
for "Discrete" Samples
"Composite" Sample
IDs
Analytical Parameters
for "Composite"
Samples
Total Number of
samples
11-1 11-1 0.0-1.0
11-2 11-2 0.0-2.0
11-3 11-3 0.0-2.0
11-4 11-4 0.0-3.0
11-5 11-5 0.0-3.0
11-6 11-6 0.0-2.0
11-7 11-7 0.0-3.0
11-8 11-8 0.0-2.0
12-1 12-1 0.0-2.0
12-2 12-2 0.0-2.0
12-3 12-3 0.0-2.0
12-4 12-4 0.0-2.0
12-5 12-5 0.0-2.0
12-6 12-6 0.0-3.0
12-7 12-7 0.0-3.0
12-8 12-8 0.0-3.0
12-9 12-9 0.0-4.0
13-1 13-1 0.0-4.0
13-2 13-2 0.0-3.0
13-3 13-3 0.0-3.0
13-4 13-4 0.0-3.0
13-5 13-5 0.0-2.0
13-6 13-6 0.0-2.0
13-7 13-7 0.0-3.0
13-8 13-8 0.0-3.0
13-9 13-9 0.0-3.0
13-10 13-10 0.0-4.0
Notes:
1. BGS = Below Ground Surface Prepared By/Date:LMM 12/27/2019
2. VOCs = Volatile Organic Compounds Checked By/Date:AJF 1/16/2020
3. SVOC = Semi-Volatile Organic Compounds
4. Shaded "discrete" sample ID indicates sample selected for VOCs analysis
1 VOC
1 Composite SVOCs and
Total Metals
SVOCs and Metals
(1 Sample)13-Comp
1 VOC
1 Composite SVOCs and
Total Metals
SVOCs and Metals
(1 Sample)12-Comp
11 5 feet
1 VOC
1 Composite SVOCs and
Total Metals
SVOCs and Metals
(1 Sample)11-Comp
"Discrete" sample 11-2
selected for VOCs
analysis based on field
screening
Brownfields Project Number: 22074-18-060
Charlotte, North Carolina
Former Gathings Motor Company
Table 1: Soil Sampling Analysis Plan - Shallow Soil (East Office Building)
Wood Project Number: 6228-18-0495
13
12
5 feet
5 feet
"Discrete" sample 13-7
selected for VOCs
analysis based on field
screening
"Discrete" sample 12-4
selected for VOCs
analysis based on field
screening
Block ID Block 11 Block 12 Block 13 Block 12
Sample ID 11-2 12-4 13-7 DUP-1
Sample Depth 0-2 0-2 0-3 0-2
Date Sampled 12/9/2019 12/9/2019 12/9/2019 12/9/2019
Benzene <0.0019 0.0011 J <0.0018 <0.0020 1.2 5.4 0.01
Tert-Butyl Alcohol (TBA)<0.038 0.066 <0.036 <0.039 ------
n-Butylbenzene <0.0019 0.0018 J <0.0018 <0.0020 780 12,000 4.5
Ethylbenzene <0.0019 0.0079 <0.0018 <0.0020 6.1 27 13
Isopropylbenzene (Cumene)<0.0019 0.0010 J <0.0018 <0.0020 410 2,100 2.3
Naphthalene <0.0038 0.0059 <0.0036 <0.0039 4.1 18 0.39
n-Propylbenzene <0.0019 0.0028 <0.0018 <0.0020 780 5,100 2.6
Toluene <0.0019 0.0026 <0.0018 <0.0020 990 9,700 8.3
1,2,4-Trimethylbenzene <0.0019 0.016 <0.0018 <0.0020 63 370 12
1,3,5-Trimethylbenzene <0.0019 0.0045 <0.0018 <0.0020 56 320 11
m&p Xylene <0.0038 0.027 <0.0036 <0.0039 240 1,020 19.6
o-Xylene <0.0019 0.010 <0.0018 <0.0020 140 590 9.8
Notes:
1. Concentrations shown in milligrams per kilogram (mg/kg)Prepared By/Date: LMM 12/27/2019
2. Depths shown in feet below ground surface Checked By/Date AJF 1/16/2020
3. Constituents detected above Reporting Limits and J-flagged results are shown, see laboratory report for full constituent list
4. PSRGs = North Carolina Department of Environmental Quality, Inactive Hazardous Sites Branch, Preliminary Soil Remediation Goals, dated December 2019
5. -- = No PSRG listed
6. J = Indicates compound was detected at a concentration below the Reporting Limit (lowest calibration standard), detection is considered an estimate
Residential
Health Based
PSRGs
Industrial/
Commercial
Health Based
PSRGs
Protection of
Groundwater
PSRGs
Wood Project Number: 6228-18-0495
Charlotte, North Carolina
Former Gathings Motor Company
Table 2: Summary of Detected Volatile Organic Compounds (VOCs) Analytical Results - Shallow Soil (East Office Building)
Brownfields Project Number: 22074-18-060
Block ID Block 11 Block 12 Block 13 Block 12
Sample ID 11-COMP 12-COMP 13-COMP Dup-2
Sample Depth 0-3 0-3 0-3 0-3
Date Sampled 12/9/2019 12/9/2019 12/9/2019 12/9/2019 Range Mean
Benzo(a)pyrene <0.21 0.15 J <0.21 <0.21 0.11 2.1 0.12
Benzo(b)fluoranthene <0.21 0.22 <0.21 <0.21 1.1 21 1.2
Chrysene <0.21 0.19 J <0.21 <0.21 110 2,100 36
Fluoranthene <0.21 0.38 0.15 J 0.13 J 480 6,000 670
2-Methylnaphthalene <0.21 0.20 J <0.21 <0.21 48 600 3.1
Phenanthrene <0.21 0.24 <0.21 <0.21 ----134
Pyrene <0.21 0.29 <0.21 <0.21 360 4,500 440
Arsenic 2.3 2.0 0.76 1.5 0.68 3.0 5.8 1.0-18 4.8
Barium 34 39 17 35 3,100 47,000 580 50-1,000 356
Cadmium 0.13 J 0.13 J 0.052 J 0.13 J 14 200 3.0 0.01-10 4.3
Chromium 21 23 8.0 28.0 23,000 350,000 360,000 7-300 65
Lead 34 35 13 33 400 800 270 ND-50 16
Mercury 0.12 0.22 0.026 J 0.07 2.3 9.7 1.0 0.03-0.52 0.121
Selenium 0.72 J 0.47 J <1.7 0.33 J 78 1,200 2.1 <0.1-0.8 0.42
Silver 0.029 J 0.036 J <0.10 0.032 J 78 1,200 3.4 ND-5.0 NS
Hexavalent Chromium <1.0 <1.0 <1.0 NA 0.31 6.5 3.8 NL NL
Notes:
1. Concentrations shown in milligrams per kilogram (mg/kg)Prepared By/Date:LMM 12/27/2019
2. Depths shown in feet below ground surface Checked By/Date:AJF 1/16/2020
3. Constituents detected above Reporting Limits and J-flagged results are shown, see laboratory report for full constituent list
4. PSRGs = North Carolina Department of Environmental Quality, Inactive Hazardous Sites Branch, Preliminary Soil Remediation Goals, dated December 2019
5. -- = No PSRG listed
6. Bold values indicates concentration exceeded Residential Health Based PSRG and PoG PSRG
7. Bold and shaded values indicates concentration exceeded Residential Health Based PSRG and concentrations reflect "naturally occurring" metals in soil
8. ND = Not detected
9. J = Indicates compound was detected at a concentration below the Reporting Limit (lowest calibration standard), detection is considered an estimate
Wood Project Number: 6228-18-0495
Brownfields Project Number: 22074-18-060
Charlotte, North Carolina
Former Gathings Motor Company
Table 3: Summary of Detected Semi-Volatile Organic Compounds (SVOCs) and Total Metals Analytical Results - Shallow Soil (East Office Building)
Residential
Health Based
PSRGs
SVOCs
Not Applicable
Regional Background Metals in Soil*
Total Metals
Protection of
Groundwater
PSRGs
Industrial/
Commercial
Health Based
PSRGs
Block ID Block 11 Block 12 Block 13
Sample ID 11-COMP 12-COMP 13-COMP
Sample Depth 0-3 0-3 0-3
Date Sampled 12/9/2019 12/9/2019 12/9/2019
Barium NA 0.31 J NA 100
Chromium NA 0.0028 J NA 5
Lead NA 0.017 J NA 5
Notes:
1. Concentrations shown in milligrams per liter (mg/L)
2. Depths shown in feet below ground surface
3. Constituents detected above Reporting Limits and J-flagged results are shown, see laboratory report for full constituent list
4. NA = Not analyzed
5. TCLP Regulatory Limits = EPA Maximum Concentrations of Contaminant for the Toxicity Characteristic
6. J = Indicates compound was detected at a concentration below the Reporting Limit (lowest calibration standard), detection is considered an estimate
TCLP Regulatory Limits
Table 4: Summary of Detected Toxicity Characteristic Leaching Procedure Analytical Results - Shallow Soil (East Office
Building)
Former Gathings Motor Company
Charlotte, North Carolina
Brownfields Project Number: 22074-18-060
Wood Project Number: 6228-18-0495
Report of Soil Characterization for Beneficial Reuse –Shallow Soil (East Office Tower)January 23, 2020
Former Gathings Motor Company
1100 and 1200 South Tryon Street, Charlotte, North Carolina
Wood Project Number: 6228-18-0495
FIGURES
USGS The National Map: National Boundaries Dataset, National ElevationDataset, Geographic Names Information System, National HydrographyDataset, National Land Cover Database, National Structures Dataset, andNational Transportation Dataset; U.S. Census Bureau - TIGER/Line; HERERoad Data. Data Refreshed July, 2017.
PREPARED BY: LM DATE: 7/12/2018 DATE: 7/12/2018CHECKED BY: MM
Site Boundary
Document Path: F:\AMEC_Projects\2018\6228-18-0495\MXD\Topo.mxd¯
PROJECT NO: 6228-18-0495 FIGURE NO: 1
SITE TOPOSpectrum South Tryon Parcels South Tryon Street
Charlotte, North Carolina
0 1,000 2,000500Feet
1-1 1-2 1-3 1-4 1-5
1-61-71-81-91-102-1
2-2
2-3
2-4
2-5
2-6
2-7
2-8
2-9
2-10
3-1 3-2 3-3 3-4 3-5
3-103-93-83-73-6
4-1 4-2 4-3 4-4 4-5
4-6 4-7 4-8 4-9 4-10
5-1 5-2 5-3 5-4 5-5
5-6 5-7 5-8 5-9 5-10
6-1 6-2 6-3
6-4 6-5 6-6
6-7 6-8 6-106-9
7-1 7-2 7-3
7-4
7-5
7-6 7-7 7-8
7-9 7-10
8-1 8-2
8-3 8-4
8-5 8-6
8-7 8-8
8-9 8-10
9-1 9-2
9-3 9-4
9-5 9-6
10-1 10-2 10-3 10-4 10-5
10-6 10-7
10-8
10-9
10-10
10-11
10-12
Sampling Grid on Cut/Fill PlanFormer Gathings Motor CompanyProposed East Office Tower1100 South Tryon StreetCharlotte, North CarolinaBrownfields Project #: 22074-18-060
PROJECT NO.:FIGURE NO.:6228-18-0495 2Document Path: F:\AMEC_Projects\2018\6228-18-0495\MXD\Sampling_Gridcutupdate.mxd Prepared By: LMM 1/23/20; Checked by RCF 1/23/19
0 60 12030Feet
LEGEND
Composite Sample "Block" Area
Boring Location and Designation6-3
11-1 11-2 11-3 11-6
11-4 11-5 11-7
11-8
12-1
12-2
12-4 12-3
12-512-612-7
12-8
12-9
13-1 13-2 13-3 13-4 13-5
13-6
13-713-813-913-10
Report of Soil Characterization for Beneficial Reuse –Shallow Soil (East Office Tower)January 23, 2020
Former Gathings Motor Company
1100 and 1200 South Tryon Street, Charlotte, North Carolina
Wood Project Number: 6228-18-0495
APPENDIX A
LABORATORY ANALYTICAL REPORTS AND CHAIN-OF-CUSTODY FORMS
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
December 20, 2019
Rob Foster
Wood - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
Project Location: Charlotte, NC
Client Job Number:
Project Number: 6228-18-0495
Laboratory Work Order Number: 19L0324
Enclosed are results of analyses for samples received by the laboratory on December 9, 2019. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 81
Table of Contents
Table of Contents
Sample Summary 4
Case Narrative 5
Sample Results 9
19L0324-02 9
19L0324-12 12
19L0324-24 15
19L0324-28 18
19L0324-29 22
19L0324-30 26
19L0324-31 30
19L0324-32 33
19L0324-33 37
Sample Preparation Information 39
QC Data 41
Volatile Organic Compounds by GC/MS 41
B248105 41
B248317 45
Semivolatile Organic Compounds by GC/MS 51
B248288 51
B248463 59
Metals Analyses (Total) 64
B248355 64
B248457 64
B248472 64
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) 65
Page 2 of 81
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Table of Contents (continued)
B248245 65
Flag/Qualifier Summary 66
Certifications 67
Chain of Custody/Sample Receipt 75
Page 3 of 81
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
12/20/2019
Wood - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
ATTN: Rob Foster
6228-18-0495
19L0324
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Charlotte, NC
11-2 19L0324-02 Soil SM 2540G
SW-846 8260D
12-4 19L0324-12 Soil SM 2540G
SW-846 8260D
13-7 19L0324-24 Soil SM 2540G
SW-846 8260D
11-COMP 19L0324-28 Soil SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8270E
12-COMP 19L0324-29 Soil SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8270E
13-COMP 19L0324-30 Soil SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8270E
DUP-1 19L0324-31 Soil SM 2540G
SW-846 8260D
DUP-2 19L0324-32 Soil SM 2540G
SW-846 6020B
SW-846 7471B
SW-846 8270E
Trip Blank 19L0324-33 Trip Blank Water SW-846 8260D
[TOC_1]Sample Summary[TOC]
Page 4 of 81
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
For method 6010, all dilutions were performed and per standard operating procedure.
[TOC_1]Case Narrative[TOC]
Page 5 of 81
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
SW-846 8260D
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not
affected since all results are "not detected" for associated samples in this batch and bias is on the high side.
Analyte & Samples(s) Qualified:
L-02
Vinyl Chloride
B248317-BS1, B248317-BSD1
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.Analyte & Samples(s) Qualified:
L-04
tert-Amyl Methyl Ether (TAME)
19L0324-33[Trip Blank], B248317-BLK1, B248317-BS1, B248317-BSD1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
V-05
1,2,3-Trichlorobenzene
19L0324-33[Trip Blank], B248317-BLK1, B248317-BS1, B248317-BSD1, S043786-CCV1
Chloromethane
19L0324-02[11-2], 19L0324-12[12-4], 19L0324-24[13-7], 19L0324-31[DUP-1], B248105-BLK1, B248105-BS1, B248105-BSD1, S043650-CCV1
tert-Amyl Methyl Ether (TAME)
19L0324-33[Trip Blank], B248317-BLK1, B248317-BS1, B248317-BSD1, S043786-CCV1
tert-Butyl Ethyl Ether (TBEE)
19L0324-33[Trip Blank], B248317-BLK1, B248317-BS1, B248317-BSD1, S043786-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected
since sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-20
trans-1,4-Dichloro-2-butene
B248317-BS1, B248317-BSD1, S043786-CCV1
Vinyl Chloride
B248317-BS1, B248317-BSD1, S043786-CCV1
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-34
Bromomethane
19L0324-02[11-2], 19L0324-12[12-4], 19L0324-24[13-7], 19L0324-31[DUP-1], B248105-BLK1, B248105-BS1, B248105-BSD1, S043650-CCV1
SW-846 8270E
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits. Reported value for this
compound is likely to be biased on the low side.
Analyte & Samples(s) Qualified:
L-04
Pyridine
19L0324-32[DUP-2], B248463-BLK1, B248463-BS1, B248463-BSD1
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits. RPD
between the two LFB/LCS results is within method specified criteria.
Analyte & Samples(s) Qualified:
L-07
Hexachlorocyclopentadiene
B248463-BSD1
Hexachloroethane
B248463-BSD1
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Matrix spike recovery and/or matrix spike duplicate recovery outside of control limits. Possibility of sample matrix effects that lead to a low
bias for reported result or non-homogeneous sample aliquots cannot be eliminated.
Analyte & Samples(s) Qualified:
MS-09
Aniline
19L0324-28RE1[11-COMP], B248288-MS1, B248288-MSD1
Benzidine
19L0324-28RE1[11-COMP], B248288-MS1, B248288-MSD1
Pyridine
19L0324-28RE1[11-COMP], B248288-MS1, B248288-MSD1
Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the two MS/MSD results is
within method specified criteria.Analyte & Samples(s) Qualified:
MS-22
Benzoic Acid
B248288-MS1
Pentachlorophenol
B248288-MS1
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any reported value for this
compound.Analyte & Samples(s) Qualified:
R-05
Benzidine
19L0324-32[DUP-2], B248463-BLK1, B248463-BS1, B248463-BSD1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
V-05
Benzidine
19L0324-28RE1[11-COMP], 19L0324-29RE1[12-COMP], 19L0324-30RE1[13-COMP], B248288-BLK1, B248288-BS1, B248288-BSD1, B248288-MS1, B248288-MSD1,
B248463-BS1, B248463-BSD1, S043755-CCV1, S043799-CCV1, S043945-CCV1
Pyridine
19L0324-28RE1[11-COMP], 19L0324-29RE1[12-COMP], 19L0324-30RE1[13-COMP], B248288-BLK1, B248288-BS1, B248288-BSD1, B248288-MS1, B248288-MSD1,
S043755-CCV1, S043799-CCV1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for this compound.
Analyte & Samples(s) Qualified:
V-06
N-Nitrosodimethylamine
B248463-BS1, B248463-BSD1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected
since sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-20
Bis(2-chloroisopropyl)ether
19L0324-32[DUP-2], B248463-BLK1, S043890-CCV1
N-Nitrosodimethylamine
19L0324-32[DUP-2], B248463-BLK1, S043890-CCV1
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-34
Benzoic Acid
19L0324-28RE1[11-COMP], 19L0324-29RE1[12-COMP], 19L0324-30RE1[13-COMP], 19L0324-32[DUP-2], B248288-BLK1, B248288-BS1, B248288-BSD1,
B248288-MS1, B248288-MSD1, B248463-BLK1, B248463-BS1, B248463-BSD1, S043755-CCV1, S043799-CCV1, S043890-CCV1, S043945-CCV1
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this compound. Reported result is
estimated.
Analyte & Samples(s) Qualified:
V-35
Benzidine
19L0324-28RE1[11-COMP], 19L0324-29RE1[12-COMP], 19L0324-30RE1[13-COMP], 19L0324-32[DUP-2], B248288-BLK1, B248288-BS1, B248288-BSD1,
B248288-MS1, B248288-MSD1, B248463-BLK1, B248463-BS1, B248463-BSD1, S043755-CCV1, S043799-CCV1, S043890-CCV1, S043945-CCV1
Page 7 of 81
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 8 of 81
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-02
Field Sample #: 11-2
Sample Matrix: Soil
Sampled: 12/9/2019 09:50
[TOC_2]19L0324-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.095 12/11/19 8:11 MFFmg/Kg dry0.022 12/11/19SW-846 8260D1Acetone
ND 0.0057 12/11/19 8:11 MFFmg/Kg dry0.0024 12/11/19SW-846 8260D1Acrylonitrile
ND 0.00095 12/11/19 8:11 MFFmg/Kg dry0.00066 12/11/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00066 12/11/19SW-846 8260D1Benzene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00076 12/11/19SW-846 8260D1Bromobenzene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.0013 12/11/19SW-846 8260D1Bromochloromethane
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00057 12/11/19SW-846 8260D1Bromodichloromethane
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.0013 12/11/19SW-846 8260D1Bromoform
ND 0.0095 12/11/19 8:11 MFFmg/Kg dry0.0040 12/11/19SW-846 8260D1V-34Bromomethane
ND 0.038 12/11/19 8:11 MFFmg/Kg dry0.017 12/11/19SW-846 8260D12-Butanone (MEK)
ND 0.038 12/11/19 8:11 MFFmg/Kg dry0.020 12/11/19SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00066 12/11/19SW-846 8260D1n-Butylbenzene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00095 12/11/19SW-846 8260D1sec-Butylbenzene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00085 12/11/19SW-846 8260D1tert-Butylbenzene
ND 0.00095 12/11/19 8:11 MFFmg/Kg dry0.00057 12/11/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0057 12/11/19 8:11 MFFmg/Kg dry0.0041 12/11/19SW-846 8260D1Carbon Disulfide
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00076 12/11/19SW-846 8260D1Carbon Tetrachloride
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00066 12/11/19SW-846 8260D1Chlorobenzene
ND 0.00095 12/11/19 8:11 MFFmg/Kg dry0.00066 12/11/19SW-846 8260D1Chlorodibromomethane
ND 0.019 12/11/19 8:11 MFFmg/Kg dry0.0014 12/11/19SW-846 8260D1Chloroethane
ND 0.0038 12/11/19 8:11 MFFmg/Kg dry0.00066 12/11/19SW-846 8260D1Chloroform
ND 0.0095 12/11/19 8:11 MFFmg/Kg dry0.0061 12/11/19SW-846 8260D1V-05Chloromethane
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00076 12/11/19SW-846 8260D12-Chlorotoluene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00076 12/11/19SW-846 8260D14-Chlorotoluene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.0010 12/11/19SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.00095 12/11/19 8:11 MFFmg/Kg dry0.00095 12/11/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00057 12/11/19SW-846 8260D1Dibromomethane
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00066 12/11/19SW-846 8260D11,2-Dichlorobenzene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00066 12/11/19SW-846 8260D11,3-Dichlorobenzene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00076 12/11/19SW-846 8260D11,4-Dichlorobenzene
ND 0.0038 12/11/19 8:11 MFFmg/Kg dry0.0020 12/11/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.019 12/11/19 8:11 MFFmg/Kg dry0.0012 12/11/19SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00066 12/11/19SW-846 8260D11,1-Dichloroethane
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.0012 12/11/19SW-846 8260D11,2-Dichloroethane
ND 0.0038 12/11/19 8:11 MFFmg/Kg dry0.0010 12/11/19SW-846 8260D11,1-Dichloroethylene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00076 12/11/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00085 12/11/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.0012 12/11/19SW-846 8260D11,2-Dichloropropane
ND 0.00095 12/11/19 8:11 MFFmg/Kg dry0.00066 12/11/19SW-846 8260D11,3-Dichloropropane
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00085 12/11/19SW-846 8260D12,2-Dichloropropane
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00085 12/11/19SW-846 8260D11,1-Dichloropropene
ND 0.00095 12/11/19 8:11 MFFmg/Kg dry0.00066 12/11/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.00095 12/11/19 8:11 MFFmg/Kg dry0.00066 12/11/19SW-846 8260D1trans-1,3-Dichloropropene
ND 0.019 12/11/19 8:11 MFFmg/Kg dry0.0017 12/11/19SW-846 8260D1Diethyl Ether
[TOC_1]Sample Results[TOC]
Page 9 of 81
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-02
Field Sample #: 11-2
Sample Matrix: Soil
Sampled: 12/9/2019 09:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.00095 12/11/19 8:11 MFFmg/Kg dry0.00057 12/11/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.095 12/11/19 8:11 MFFmg/Kg dry0.054 12/11/19SW-846 8260D11,4-Dioxane
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00076 12/11/19SW-846 8260D1Ethylbenzene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00095 12/11/19SW-846 8260D1Hexachlorobutadiene
ND 0.019 12/11/19 8:11 MFFmg/Kg dry0.010 12/11/19SW-846 8260D12-Hexanone (MBK)
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00066 12/11/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00076 12/11/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0038 12/11/19 8:11 MFFmg/Kg dry0.00085 12/11/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.019 12/11/19 8:11 MFFmg/Kg dry0.0067 12/11/19SW-846 8260D1Methylene Chloride
ND 0.019 12/11/19 8:11 MFFmg/Kg dry0.0072 12/11/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0038 12/11/19 8:11 MFFmg/Kg dry0.00066 12/11/19SW-846 8260D1Naphthalene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00066 12/11/19SW-846 8260D1n-Propylbenzene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00057 12/11/19SW-846 8260D1Styrene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.0017 12/11/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.00095 12/11/19 8:11 MFFmg/Kg dry0.00085 12/11/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.0012 12/11/19SW-846 8260D1Tetrachloroethylene
ND 0.0095 12/11/19 8:11 MFFmg/Kg dry0.0021 12/11/19SW-846 8260D1Tetrahydrofuran
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00076 12/11/19SW-846 8260D1Toluene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00057 12/11/19SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00076 12/11/19SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00066 12/11/19SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00095 12/11/19SW-846 8260D11,1,1-Trichloroethane
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.0011 12/11/19SW-846 8260D11,1,2-Trichloroethane
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00095 12/11/19SW-846 8260D1Trichloroethylene
ND 0.0095 12/11/19 8:11 MFFmg/Kg dry0.0010 12/11/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.0010 12/11/19SW-846 8260D11,2,3-Trichloropropane
ND 0.0095 12/11/19 8:11 MFFmg/Kg dry0.00085 12/11/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00076 12/11/19SW-846 8260D11,2,4-Trimethylbenzene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00057 12/11/19SW-846 8260D11,3,5-Trimethylbenzene
ND 0.0095 12/11/19 8:11 MFFmg/Kg dry0.0010 12/11/19SW-846 8260D1Vinyl Chloride
ND 0.0038 12/11/19 8:11 MFFmg/Kg dry0.0016 12/11/19SW-846 8260D1m+p Xylene
ND 0.0019 12/11/19 8:11 MFFmg/Kg dry0.00066 12/11/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 93.6 12/11/19 8:1170-130
Toluene-d8 97.7 12/11/19 8:1170-130
4-Bromofluorobenzene 101 12/11/19 8:1170-130
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-02
Field Sample #: 11-2
Sample Matrix: Soil
Sampled: 12/9/2019 09:50
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
78.3 12/12/19 18:34 adb% Wt 12/12/19SM 2540G1% Solids
Page 11 of 81
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-12
Field Sample #: 12-4
Sample Matrix: Soil
Sampled: 12/9/2019 11:05
[TOC_2]19L0324-12[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.093 12/11/19 8:38 MFFmg/Kg dry0.022 12/11/19SW-846 8260D1Acetone
ND 0.0056 12/11/19 8:38 MFFmg/Kg dry0.0023 12/11/19SW-846 8260D1Acrylonitrile
ND 0.00093 12/11/19 8:38 MFFmg/Kg dry0.00065 12/11/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
0.0011 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00065 12/11/19SW-846 8260D1JBenzene
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00074 12/11/19SW-846 8260D1Bromobenzene
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.0013 12/11/19SW-846 8260D1Bromochloromethane
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00056 12/11/19SW-846 8260D1Bromodichloromethane
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.0013 12/11/19SW-846 8260D1Bromoform
ND 0.0093 12/11/19 8:38 MFFmg/Kg dry0.0039 12/11/19SW-846 8260D1V-34Bromomethane
ND 0.037 12/11/19 8:38 MFFmg/Kg dry0.016 12/11/19SW-846 8260D12-Butanone (MEK)
0.066 0.037 12/11/19 8:38 MFFmg/Kg dry0.019 12/11/19SW-846 8260D1tert-Butyl Alcohol (TBA)
0.0018 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00065 12/11/19SW-846 8260D1Jn-Butylbenzene
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00093 12/11/19SW-846 8260D1sec-Butylbenzene
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00084 12/11/19SW-846 8260D1tert-Butylbenzene
ND 0.00093 12/11/19 8:38 MFFmg/Kg dry0.00056 12/11/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0056 12/11/19 8:38 MFFmg/Kg dry0.0040 12/11/19SW-846 8260D1Carbon Disulfide
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00074 12/11/19SW-846 8260D1Carbon Tetrachloride
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00065 12/11/19SW-846 8260D1Chlorobenzene
ND 0.00093 12/11/19 8:38 MFFmg/Kg dry0.00065 12/11/19SW-846 8260D1Chlorodibromomethane
ND 0.019 12/11/19 8:38 MFFmg/Kg dry0.0014 12/11/19SW-846 8260D1Chloroethane
ND 0.0037 12/11/19 8:38 MFFmg/Kg dry0.00065 12/11/19SW-846 8260D1Chloroform
ND 0.0093 12/11/19 8:38 MFFmg/Kg dry0.0060 12/11/19SW-846 8260D1V-05Chloromethane
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00074 12/11/19SW-846 8260D12-Chlorotoluene
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00074 12/11/19SW-846 8260D14-Chlorotoluene
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.0010 12/11/19SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.00093 12/11/19 8:38 MFFmg/Kg dry0.00093 12/11/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00056 12/11/19SW-846 8260D1Dibromomethane
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00065 12/11/19SW-846 8260D11,2-Dichlorobenzene
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00065 12/11/19SW-846 8260D11,3-Dichlorobenzene
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00074 12/11/19SW-846 8260D11,4-Dichlorobenzene
ND 0.0037 12/11/19 8:38 MFFmg/Kg dry0.0020 12/11/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.019 12/11/19 8:38 MFFmg/Kg dry0.0012 12/11/19SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00065 12/11/19SW-846 8260D11,1-Dichloroethane
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.0012 12/11/19SW-846 8260D11,2-Dichloroethane
ND 0.0037 12/11/19 8:38 MFFmg/Kg dry0.0010 12/11/19SW-846 8260D11,1-Dichloroethylene
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00074 12/11/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00084 12/11/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.0012 12/11/19SW-846 8260D11,2-Dichloropropane
ND 0.00093 12/11/19 8:38 MFFmg/Kg dry0.00065 12/11/19SW-846 8260D11,3-Dichloropropane
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00084 12/11/19SW-846 8260D12,2-Dichloropropane
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00084 12/11/19SW-846 8260D11,1-Dichloropropene
ND 0.00093 12/11/19 8:38 MFFmg/Kg dry0.00065 12/11/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.00093 12/11/19 8:38 MFFmg/Kg dry0.00065 12/11/19SW-846 8260D1trans-1,3-Dichloropropene
ND 0.019 12/11/19 8:38 MFFmg/Kg dry0.0017 12/11/19SW-846 8260D1Diethyl Ether
Page 12 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-12
Field Sample #: 12-4
Sample Matrix: Soil
Sampled: 12/9/2019 11:05
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.00093 12/11/19 8:38 MFFmg/Kg dry0.00056 12/11/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.093 12/11/19 8:38 MFFmg/Kg dry0.054 12/11/19SW-846 8260D11,4-Dioxane
0.0079 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00074 12/11/19SW-846 8260D1Ethylbenzene
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00093 12/11/19SW-846 8260D1Hexachlorobutadiene
ND 0.019 12/11/19 8:38 MFFmg/Kg dry0.010 12/11/19SW-846 8260D12-Hexanone (MBK)
0.0010 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00065 12/11/19SW-846 8260D1JIsopropylbenzene (Cumene)
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00074 12/11/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0037 12/11/19 8:38 MFFmg/Kg dry0.00084 12/11/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.019 12/11/19 8:38 MFFmg/Kg dry0.0066 12/11/19SW-846 8260D1Methylene Chloride
ND 0.019 12/11/19 8:38 MFFmg/Kg dry0.0071 12/11/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
0.0059 0.0037 12/11/19 8:38 MFFmg/Kg dry0.00065 12/11/19SW-846 8260D1Naphthalene
0.0028 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00065 12/11/19SW-846 8260D1n-Propylbenzene
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00056 12/11/19SW-846 8260D1Styrene
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.0017 12/11/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.00093 12/11/19 8:38 MFFmg/Kg dry0.00084 12/11/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.0012 12/11/19SW-846 8260D1Tetrachloroethylene
ND 0.0093 12/11/19 8:38 MFFmg/Kg dry0.0020 12/11/19SW-846 8260D1Tetrahydrofuran
0.0026 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00074 12/11/19SW-846 8260D1Toluene
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00056 12/11/19SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00074 12/11/19SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00065 12/11/19SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00093 12/11/19SW-846 8260D11,1,1-Trichloroethane
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.0011 12/11/19SW-846 8260D11,1,2-Trichloroethane
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00093 12/11/19SW-846 8260D1Trichloroethylene
ND 0.0093 12/11/19 8:38 MFFmg/Kg dry0.0010 12/11/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0019 12/11/19 8:38 MFFmg/Kg dry0.0010 12/11/19SW-846 8260D11,2,3-Trichloropropane
ND 0.0093 12/11/19 8:38 MFFmg/Kg dry0.00084 12/11/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
0.016 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00074 12/11/19SW-846 8260D11,2,4-Trimethylbenzene
0.0045 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00056 12/11/19SW-846 8260D11,3,5-Trimethylbenzene
ND 0.0093 12/11/19 8:38 MFFmg/Kg dry0.0010 12/11/19SW-846 8260D1Vinyl Chloride
0.027 0.0037 12/11/19 8:38 MFFmg/Kg dry0.0016 12/11/19SW-846 8260D1m+p Xylene
0.010 0.0019 12/11/19 8:38 MFFmg/Kg dry0.00065 12/11/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 97.6 12/11/19 8:3870-130
Toluene-d8 98.2 12/11/19 8:3870-130
4-Bromofluorobenzene 103 12/11/19 8:3870-130
Page 13 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-12
Field Sample #: 12-4
Sample Matrix: Soil
Sampled: 12/9/2019 11:05
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
82.1 12/12/19 18:34 adb% Wt 12/12/19SM 2540G1% Solids
Page 14 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-24
Field Sample #: 13-7
Sample Matrix: Soil
Sampled: 12/9/2019 12:30
[TOC_2]19L0324-24[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.090 12/11/19 9:06 MFFmg/Kg dry0.021 12/11/19SW-846 8260D1Acetone
ND 0.0054 12/11/19 9:06 MFFmg/Kg dry0.0023 12/11/19SW-846 8260D1Acrylonitrile
ND 0.00090 12/11/19 9:06 MFFmg/Kg dry0.00063 12/11/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00063 12/11/19SW-846 8260D1Benzene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00072 12/11/19SW-846 8260D1Bromobenzene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.0013 12/11/19SW-846 8260D1Bromochloromethane
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00054 12/11/19SW-846 8260D1Bromodichloromethane
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.0013 12/11/19SW-846 8260D1Bromoform
ND 0.0090 12/11/19 9:06 MFFmg/Kg dry0.0038 12/11/19SW-846 8260D1V-34Bromomethane
ND 0.036 12/11/19 9:06 MFFmg/Kg dry0.016 12/11/19SW-846 8260D12-Butanone (MEK)
ND 0.036 12/11/19 9:06 MFFmg/Kg dry0.019 12/11/19SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00063 12/11/19SW-846 8260D1n-Butylbenzene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00090 12/11/19SW-846 8260D1sec-Butylbenzene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00081 12/11/19SW-846 8260D1tert-Butylbenzene
ND 0.00090 12/11/19 9:06 MFFmg/Kg dry0.00054 12/11/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0054 12/11/19 9:06 MFFmg/Kg dry0.0039 12/11/19SW-846 8260D1Carbon Disulfide
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00072 12/11/19SW-846 8260D1Carbon Tetrachloride
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00063 12/11/19SW-846 8260D1Chlorobenzene
ND 0.00090 12/11/19 9:06 MFFmg/Kg dry0.00063 12/11/19SW-846 8260D1Chlorodibromomethane
ND 0.018 12/11/19 9:06 MFFmg/Kg dry0.0014 12/11/19SW-846 8260D1Chloroethane
ND 0.0036 12/11/19 9:06 MFFmg/Kg dry0.00063 12/11/19SW-846 8260D1Chloroform
ND 0.0090 12/11/19 9:06 MFFmg/Kg dry0.0058 12/11/19SW-846 8260D1V-05Chloromethane
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00072 12/11/19SW-846 8260D12-Chlorotoluene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00072 12/11/19SW-846 8260D14-Chlorotoluene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00099 12/11/19SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.00090 12/11/19 9:06 MFFmg/Kg dry0.00090 12/11/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00054 12/11/19SW-846 8260D1Dibromomethane
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00063 12/11/19SW-846 8260D11,2-Dichlorobenzene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00063 12/11/19SW-846 8260D11,3-Dichlorobenzene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00072 12/11/19SW-846 8260D11,4-Dichlorobenzene
ND 0.0036 12/11/19 9:06 MFFmg/Kg dry0.0019 12/11/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.018 12/11/19 9:06 MFFmg/Kg dry0.0012 12/11/19SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00063 12/11/19SW-846 8260D11,1-Dichloroethane
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.0012 12/11/19SW-846 8260D11,2-Dichloroethane
ND 0.0036 12/11/19 9:06 MFFmg/Kg dry0.00099 12/11/19SW-846 8260D11,1-Dichloroethylene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00072 12/11/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00081 12/11/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.0012 12/11/19SW-846 8260D11,2-Dichloropropane
ND 0.00090 12/11/19 9:06 MFFmg/Kg dry0.00063 12/11/19SW-846 8260D11,3-Dichloropropane
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00081 12/11/19SW-846 8260D12,2-Dichloropropane
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00081 12/11/19SW-846 8260D11,1-Dichloropropene
ND 0.00090 12/11/19 9:06 MFFmg/Kg dry0.00063 12/11/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.00090 12/11/19 9:06 MFFmg/Kg dry0.00063 12/11/19SW-846 8260D1trans-1,3-Dichloropropene
ND 0.018 12/11/19 9:06 MFFmg/Kg dry0.0016 12/11/19SW-846 8260D1Diethyl Ether
Page 15 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-24
Field Sample #: 13-7
Sample Matrix: Soil
Sampled: 12/9/2019 12:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.00090 12/11/19 9:06 MFFmg/Kg dry0.00054 12/11/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.090 12/11/19 9:06 MFFmg/Kg dry0.052 12/11/19SW-846 8260D11,4-Dioxane
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00072 12/11/19SW-846 8260D1Ethylbenzene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00090 12/11/19SW-846 8260D1Hexachlorobutadiene
ND 0.018 12/11/19 9:06 MFFmg/Kg dry0.0098 12/11/19SW-846 8260D12-Hexanone (MBK)
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00063 12/11/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00072 12/11/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0036 12/11/19 9:06 MFFmg/Kg dry0.00081 12/11/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.018 12/11/19 9:06 MFFmg/Kg dry0.0064 12/11/19SW-846 8260D1Methylene Chloride
ND 0.018 12/11/19 9:06 MFFmg/Kg dry0.0069 12/11/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0036 12/11/19 9:06 MFFmg/Kg dry0.00063 12/11/19SW-846 8260D1Naphthalene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00063 12/11/19SW-846 8260D1n-Propylbenzene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00054 12/11/19SW-846 8260D1Styrene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.0016 12/11/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.00090 12/11/19 9:06 MFFmg/Kg dry0.00081 12/11/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.0012 12/11/19SW-846 8260D1Tetrachloroethylene
ND 0.0090 12/11/19 9:06 MFFmg/Kg dry0.0020 12/11/19SW-846 8260D1Tetrahydrofuran
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00072 12/11/19SW-846 8260D1Toluene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00054 12/11/19SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00072 12/11/19SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00063 12/11/19SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00090 12/11/19SW-846 8260D11,1,1-Trichloroethane
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.0011 12/11/19SW-846 8260D11,1,2-Trichloroethane
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00090 12/11/19SW-846 8260D1Trichloroethylene
ND 0.0090 12/11/19 9:06 MFFmg/Kg dry0.00099 12/11/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00099 12/11/19SW-846 8260D11,2,3-Trichloropropane
ND 0.0090 12/11/19 9:06 MFFmg/Kg dry0.00081 12/11/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00072 12/11/19SW-846 8260D11,2,4-Trimethylbenzene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00054 12/11/19SW-846 8260D11,3,5-Trimethylbenzene
ND 0.0090 12/11/19 9:06 MFFmg/Kg dry0.00099 12/11/19SW-846 8260D1Vinyl Chloride
ND 0.0036 12/11/19 9:06 MFFmg/Kg dry0.0015 12/11/19SW-846 8260D1m+p Xylene
ND 0.0018 12/11/19 9:06 MFFmg/Kg dry0.00063 12/11/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 97.5 12/11/19 9:0670-130
Toluene-d8 98.1 12/11/19 9:0670-130
4-Bromofluorobenzene 102 12/11/19 9:0670-130
Page 16 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-24
Field Sample #: 13-7
Sample Matrix: Soil
Sampled: 12/9/2019 12:30
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
81.6 12/12/19 18:35 adb% Wt 12/12/19SM 2540G1% Solids
Page 17 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-28
Field Sample #: 11-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 9:45:00AM
Stop Date/Time: 12/9/2019 10:30:00AM
[TOC_2]19L0324-28[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.21 12/16/19 15:11 KLBmg/Kg dry0.11 12/13/19SW-846 8270E1Acenaphthene
ND 0.21 12/16/19 15:11 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Acenaphthylene
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.16 12/13/19SW-846 8270E1Acetophenone
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.10 12/13/19SW-846 8270E1MS-09Aniline
ND 0.21 12/16/19 15:11 KLBmg/Kg dry0.11 12/13/19SW-846 8270E1Anthracene
ND 0.82 12/16/19 15:11 KLBmg/Kg dry0.22 12/13/19SW-846 8270E1MS-09, V-05, V-35Benzidine
ND 0.21 12/16/19 15:11 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Benzo(a)anthracene
ND 0.21 12/16/19 15:11 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Benzo(a)pyrene
ND 0.21 12/16/19 15:11 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Benzo(b)fluoranthene
ND 0.21 12/16/19 15:11 KLBmg/Kg dry0.12 12/13/19SW-846 8270E1Benzo(g,h,i)perylene
ND 0.21 12/16/19 15:11 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Benzo(k)fluoranthene
ND 1.2 12/16/19 15:11 KLBmg/Kg dry0.74 12/13/19SW-846 8270E1V-34Benzoic Acid
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.17 12/13/19SW-846 8270E1Bis(2-chloroethoxy)methane
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.21 12/13/19SW-846 8270E1Bis(2-chloroethyl)ether
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.29 12/13/19SW-846 8270E1Bis(2-chloroisopropyl)ether
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.12 12/13/19SW-846 8270E1Bis(2-Ethylhexyl)phthalate
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.12 12/13/19SW-846 8270E14-Bromophenylphenylether
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Butylbenzylphthalate
ND 0.21 12/16/19 15:11 KLBmg/Kg dry0.11 12/13/19SW-846 8270E1Carbazole
ND 0.82 12/16/19 15:11 KLBmg/Kg dry0.17 12/13/19SW-846 8270E14-Chloroaniline
ND 0.82 12/16/19 15:11 KLBmg/Kg dry0.17 12/13/19SW-846 8270E14-Chloro-3-methylphenol
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.12 12/13/19SW-846 8270E12-Chloronaphthalene
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.15 12/13/19SW-846 8270E12-Chlorophenol
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.15 12/13/19SW-846 8270E14-Chlorophenylphenylether
ND 0.21 12/16/19 15:11 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Chrysene
ND 0.21 12/16/19 15:11 KLBmg/Kg dry0.12 12/13/19SW-846 8270E1Dibenz(a,h)anthracene
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Dibenzofuran
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.12 12/13/19SW-846 8270E1Di-n-butylphthalate
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.12 12/13/19SW-846 8270E11,2-Dichlorobenzene
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.12 12/13/19SW-846 8270E11,3-Dichlorobenzene
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.11 12/13/19SW-846 8270E11,4-Dichlorobenzene
ND 0.21 12/16/19 15:11 KLBmg/Kg dry0.16 12/13/19SW-846 8270E13,3-Dichlorobenzidine
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.12 12/13/19SW-846 8270E12,4-Dichlorophenol
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.17 12/13/19SW-846 8270E1Diethylphthalate
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.15 12/13/19SW-846 8270E12,4-Dimethylphenol
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.16 12/13/19SW-846 8270E1Dimethylphthalate
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.37 12/13/19SW-846 8270E14,6-Dinitro-2-methylphenol
ND 0.82 12/16/19 15:11 KLBmg/Kg dry0.57 12/13/19SW-846 8270E12,4-Dinitrophenol
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.20 12/13/19SW-846 8270E12,4-Dinitrotoluene
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.20 12/13/19SW-846 8270E12,6-Dinitrotoluene
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.19 12/13/19SW-846 8270E1Di-n-octylphthalate
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.12 12/13/19SW-846 8270E11,2-Diphenylhydrazine/Azobenzene
ND 0.21 12/16/19 15:11 KLBmg/Kg dry0.12 12/13/19SW-846 8270E1Fluoranthene
ND 0.21 12/16/19 15:11 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Fluorene
Page 18 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-28
Field Sample #: 11-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 9:45:00AM
Stop Date/Time: 12/9/2019 10:30:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.11 12/13/19SW-846 8270E1Hexachlorobenzene
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.16 12/13/19SW-846 8270E1Hexachlorobutadiene
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.35 12/13/19SW-846 8270E1Hexachlorocyclopentadiene
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Hexachloroethane
ND 0.21 12/16/19 15:11 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Indeno(1,2,3-cd)pyrene
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Isophorone
ND 0.21 12/16/19 15:11 KLBmg/Kg dry0.11 12/13/19SW-846 8270E11-Methylnaphthalene
ND 0.21 12/16/19 15:11 KLBmg/Kg dry0.14 12/13/19SW-846 8270E12-Methylnaphthalene
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.16 12/13/19SW-846 8270E12-Methylphenol
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.15 12/13/19SW-846 8270E13/4-Methylphenol
ND 0.21 12/16/19 15:11 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Naphthalene
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.25 12/13/19SW-846 8270E12-Nitroaniline
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.17 12/13/19SW-846 8270E13-Nitroaniline
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.16 12/13/19SW-846 8270E14-Nitroaniline
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.17 12/13/19SW-846 8270E1Nitrobenzene
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.17 12/13/19SW-846 8270E12-Nitrophenol
ND 0.82 12/16/19 15:11 KLBmg/Kg dry0.30 12/13/19SW-846 8270E14-Nitrophenol
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.22 12/13/19SW-846 8270E1N-Nitrosodimethylamine
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.12 12/13/19SW-846 8270E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.19 12/13/19SW-846 8270E1N-Nitrosodi-n-propylamine
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Pentachloronitrobenzene
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.29 12/13/19SW-846 8270E1Pentachlorophenol
ND 0.21 12/16/19 15:11 KLBmg/Kg dry0.11 12/13/19SW-846 8270E1Phenanthrene
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Phenol
ND 0.21 12/16/19 15:11 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Pyrene
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.12 12/13/19SW-846 8270E1MS-09, V-05Pyridine
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.16 12/13/19SW-846 8270E11,2,4,5-Tetrachlorobenzene
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.14 12/13/19SW-846 8270E11,2,4-Trichlorobenzene
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.15 12/13/19SW-846 8270E12,4,5-Trichlorophenol
ND 0.42 12/16/19 15:11 KLBmg/Kg dry0.15 12/13/19SW-846 8270E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 57.9 12/16/19 15:1130-130
Phenol-d6 58.0 12/16/19 15:1130-130
Nitrobenzene-d5 55.2 12/16/19 15:1130-130
2-Fluorobiphenyl 76.1 12/16/19 15:1130-130
2,4,6-Tribromophenol 66.4 12/16/19 15:1130-130
p-Terphenyl-d14 66.2 12/16/19 15:1130-130
Page 19 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-28
Field Sample #: 11-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 9:45:00AM
Stop Date/Time: 12/9/2019 10:30:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
2.3 0.20 12/18/19 16:23 MJHmg/Kg dry0.038 12/17/19SW-846 6020B5Arsenic
21 5.1 12/18/19 16:23 MJHmg/Kg dry0.15 12/17/19SW-846 6020B5Chromium
34 2.0 12/18/19 16:23 MJHmg/Kg dry0.026 12/17/19SW-846 6020B5Lead
0.12 0.030 12/14/19 11:45 AJLmg/Kg dry0.0091 12/13/19SW-846 7471B1Mercury
0.72 1.6 12/18/19 16:23 MJHmg/Kg dry0.12 12/17/19SW-846 6020B5JSelenium
0.029 0.10 12/18/19 16:23 MJHmg/Kg dry0.018 12/17/19SW-846 6020B5JSilver
34 10 12/18/19 16:23 MJHmg/Kg dry0.090 12/17/19SW-846 6020B5Barium
0.13 0.41 12/18/19 16:23 MJHmg/Kg dry0.018 12/17/19SW-846 6020B5JCadmium
Page 20 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-28
Field Sample #: 11-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 9:45:00AM
Stop Date/Time: 12/9/2019 10:30:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
80.1 12/12/19 21:01 adb% Wt 12/12/19SM 2540G1% Solids
Page 21 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-29
Field Sample #: 12-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 10:35:00AM
Stop Date/Time: 12/9/2019 11:40:00AM
[TOC_2]19L0324-29[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.22 12/16/19 15:37 KLBmg/Kg dry0.12 12/13/19SW-846 8270E1Acenaphthene
ND 0.22 12/16/19 15:37 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Acenaphthylene
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.17 12/13/19SW-846 8270E1Acetophenone
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.10 12/13/19SW-846 8270E1Aniline
ND 0.22 12/16/19 15:37 KLBmg/Kg dry0.12 12/13/19SW-846 8270E1Anthracene
ND 0.85 12/16/19 15:37 KLBmg/Kg dry0.23 12/13/19SW-846 8270E1V-05, V-35Benzidine
ND 0.22 12/16/19 15:37 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Benzo(a)anthracene
0.15 0.22 12/16/19 15:37 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1JBenzo(a)pyrene
0.22 0.22 12/16/19 15:37 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Benzo(b)fluoranthene
ND 0.22 12/16/19 15:37 KLBmg/Kg dry0.13 12/13/19SW-846 8270E1Benzo(g,h,i)perylene
ND 0.22 12/16/19 15:37 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Benzo(k)fluoranthene
ND 1.3 12/16/19 15:37 KLBmg/Kg dry0.76 12/13/19SW-846 8270E1V-34Benzoic Acid
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.18 12/13/19SW-846 8270E1Bis(2-chloroethoxy)methane
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.22 12/13/19SW-846 8270E1Bis(2-chloroethyl)ether
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.30 12/13/19SW-846 8270E1Bis(2-chloroisopropyl)ether
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.13 12/13/19SW-846 8270E1Bis(2-Ethylhexyl)phthalate
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.13 12/13/19SW-846 8270E14-Bromophenylphenylether
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Butylbenzylphthalate
ND 0.22 12/16/19 15:37 KLBmg/Kg dry0.12 12/13/19SW-846 8270E1Carbazole
ND 0.85 12/16/19 15:37 KLBmg/Kg dry0.18 12/13/19SW-846 8270E14-Chloroaniline
ND 0.85 12/16/19 15:37 KLBmg/Kg dry0.18 12/13/19SW-846 8270E14-Chloro-3-methylphenol
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.13 12/13/19SW-846 8270E12-Chloronaphthalene
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.15 12/13/19SW-846 8270E12-Chlorophenol
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.15 12/13/19SW-846 8270E14-Chlorophenylphenylether
0.19 0.22 12/16/19 15:37 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1JChrysene
ND 0.22 12/16/19 15:37 KLBmg/Kg dry0.13 12/13/19SW-846 8270E1Dibenz(a,h)anthracene
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Dibenzofuran
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.13 12/13/19SW-846 8270E1Di-n-butylphthalate
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.13 12/13/19SW-846 8270E11,2-Dichlorobenzene
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.13 12/13/19SW-846 8270E11,3-Dichlorobenzene
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.12 12/13/19SW-846 8270E11,4-Dichlorobenzene
ND 0.22 12/16/19 15:37 KLBmg/Kg dry0.17 12/13/19SW-846 8270E13,3-Dichlorobenzidine
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.13 12/13/19SW-846 8270E12,4-Dichlorophenol
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.18 12/13/19SW-846 8270E1Diethylphthalate
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.15 12/13/19SW-846 8270E12,4-Dimethylphenol
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.17 12/13/19SW-846 8270E1Dimethylphthalate
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.39 12/13/19SW-846 8270E14,6-Dinitro-2-methylphenol
ND 0.85 12/16/19 15:37 KLBmg/Kg dry0.59 12/13/19SW-846 8270E12,4-Dinitrophenol
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.21 12/13/19SW-846 8270E12,4-Dinitrotoluene
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.21 12/13/19SW-846 8270E12,6-Dinitrotoluene
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.19 12/13/19SW-846 8270E1Di-n-octylphthalate
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.13 12/13/19SW-846 8270E11,2-Diphenylhydrazine/Azobenzene
0.38 0.22 12/16/19 15:37 KLBmg/Kg dry0.13 12/13/19SW-846 8270E1Fluoranthene
ND 0.22 12/16/19 15:37 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Fluorene
Page 22 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-29
Field Sample #: 12-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 10:35:00AM
Stop Date/Time: 12/9/2019 11:40:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.12 12/13/19SW-846 8270E1Hexachlorobenzene
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.17 12/13/19SW-846 8270E1Hexachlorobutadiene
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.36 12/13/19SW-846 8270E1Hexachlorocyclopentadiene
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Hexachloroethane
ND 0.22 12/16/19 15:37 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Indeno(1,2,3-cd)pyrene
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Isophorone
ND 0.22 12/16/19 15:37 KLBmg/Kg dry0.12 12/13/19SW-846 8270E11-Methylnaphthalene
0.20 0.22 12/16/19 15:37 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1J2-Methylnaphthalene
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.17 12/13/19SW-846 8270E12-Methylphenol
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.15 12/13/19SW-846 8270E13/4-Methylphenol
ND 0.22 12/16/19 15:37 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Naphthalene
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.26 12/13/19SW-846 8270E12-Nitroaniline
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.18 12/13/19SW-846 8270E13-Nitroaniline
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.17 12/13/19SW-846 8270E14-Nitroaniline
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.18 12/13/19SW-846 8270E1Nitrobenzene
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.18 12/13/19SW-846 8270E12-Nitrophenol
ND 0.85 12/16/19 15:37 KLBmg/Kg dry0.31 12/13/19SW-846 8270E14-Nitrophenol
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.23 12/13/19SW-846 8270E1N-Nitrosodimethylamine
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.13 12/13/19SW-846 8270E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.19 12/13/19SW-846 8270E1N-Nitrosodi-n-propylamine
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Pentachloronitrobenzene
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.30 12/13/19SW-846 8270E1Pentachlorophenol
0.24 0.22 12/16/19 15:37 KLBmg/Kg dry0.12 12/13/19SW-846 8270E1Phenanthrene
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Phenol
0.29 0.22 12/16/19 15:37 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Pyrene
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.13 12/13/19SW-846 8270E1V-05Pyridine
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.17 12/13/19SW-846 8270E11,2,4,5-Tetrachlorobenzene
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.14 12/13/19SW-846 8270E11,2,4-Trichlorobenzene
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.15 12/13/19SW-846 8270E12,4,5-Trichlorophenol
ND 0.44 12/16/19 15:37 KLBmg/Kg dry0.15 12/13/19SW-846 8270E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 58.0 12/16/19 15:3730-130
Phenol-d6 59.7 12/16/19 15:3730-130
Nitrobenzene-d5 55.4 12/16/19 15:3730-130
2-Fluorobiphenyl 78.0 12/16/19 15:3730-130
2,4,6-Tribromophenol 65.5 12/16/19 15:3730-130
p-Terphenyl-d14 68.0 12/16/19 15:3730-130
Page 23 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-29
Field Sample #: 12-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 10:35:00AM
Stop Date/Time: 12/9/2019 11:40:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
2.0 0.21 12/18/19 16:26 MJHmg/Kg dry0.040 12/17/19SW-846 6020B5Arsenic
23 5.3 12/18/19 16:26 MJHmg/Kg dry0.15 12/17/19SW-846 6020B5Chromium
35 2.1 12/18/19 16:26 MJHmg/Kg dry0.028 12/17/19SW-846 6020B5Lead
0.22 0.032 12/14/19 11:51 AJLmg/Kg dry0.0095 12/13/19SW-846 7471B1Mercury
0.47 1.7 12/18/19 16:26 MJHmg/Kg dry0.13 12/17/19SW-846 6020B5JSelenium
0.036 0.11 12/18/19 16:26 MJHmg/Kg dry0.019 12/17/19SW-846 6020B5JSilver
39 11 12/18/19 16:26 MJHmg/Kg dry0.094 12/17/19SW-846 6020B5Barium
0.13 0.43 12/18/19 16:26 MJHmg/Kg dry0.019 12/17/19SW-846 6020B5JCadmium
Page 24 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-29
Field Sample #: 12-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 10:35:00AM
Stop Date/Time: 12/9/2019 11:40:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
77.5 12/12/19 21:02 adb% Wt 12/12/19SM 2540G1% Solids
Page 25 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-30
Field Sample #: 13-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 11:50:00AM
Stop Date/Time: 12/9/2019 12:50:00PM
[TOC_2]19L0324-30[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.21 12/16/19 16:02 KLBmg/Kg dry0.11 12/13/19SW-846 8270E1Acenaphthene
ND 0.21 12/16/19 16:02 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Acenaphthylene
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.16 12/13/19SW-846 8270E1Acetophenone
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.10 12/13/19SW-846 8270E1Aniline
ND 0.21 12/16/19 16:02 KLBmg/Kg dry0.11 12/13/19SW-846 8270E1Anthracene
ND 0.82 12/16/19 16:02 KLBmg/Kg dry0.22 12/13/19SW-846 8270E1V-05, V-35Benzidine
ND 0.21 12/16/19 16:02 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Benzo(a)anthracene
ND 0.21 12/16/19 16:02 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Benzo(a)pyrene
ND 0.21 12/16/19 16:02 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Benzo(b)fluoranthene
ND 0.21 12/16/19 16:02 KLBmg/Kg dry0.12 12/13/19SW-846 8270E1Benzo(g,h,i)perylene
ND 0.21 12/16/19 16:02 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Benzo(k)fluoranthene
ND 1.2 12/16/19 16:02 KLBmg/Kg dry0.74 12/13/19SW-846 8270E1V-34Benzoic Acid
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.17 12/13/19SW-846 8270E1Bis(2-chloroethoxy)methane
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.21 12/13/19SW-846 8270E1Bis(2-chloroethyl)ether
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.29 12/13/19SW-846 8270E1Bis(2-chloroisopropyl)ether
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.12 12/13/19SW-846 8270E1Bis(2-Ethylhexyl)phthalate
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.12 12/13/19SW-846 8270E14-Bromophenylphenylether
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Butylbenzylphthalate
ND 0.21 12/16/19 16:02 KLBmg/Kg dry0.11 12/13/19SW-846 8270E1Carbazole
ND 0.82 12/16/19 16:02 KLBmg/Kg dry0.17 12/13/19SW-846 8270E14-Chloroaniline
ND 0.82 12/16/19 16:02 KLBmg/Kg dry0.17 12/13/19SW-846 8270E14-Chloro-3-methylphenol
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.12 12/13/19SW-846 8270E12-Chloronaphthalene
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.15 12/13/19SW-846 8270E12-Chlorophenol
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.15 12/13/19SW-846 8270E14-Chlorophenylphenylether
ND 0.21 12/16/19 16:02 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Chrysene
ND 0.21 12/16/19 16:02 KLBmg/Kg dry0.12 12/13/19SW-846 8270E1Dibenz(a,h)anthracene
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Dibenzofuran
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.12 12/13/19SW-846 8270E1Di-n-butylphthalate
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.12 12/13/19SW-846 8270E11,2-Dichlorobenzene
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.12 12/13/19SW-846 8270E11,3-Dichlorobenzene
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.11 12/13/19SW-846 8270E11,4-Dichlorobenzene
ND 0.21 12/16/19 16:02 KLBmg/Kg dry0.16 12/13/19SW-846 8270E13,3-Dichlorobenzidine
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.12 12/13/19SW-846 8270E12,4-Dichlorophenol
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.17 12/13/19SW-846 8270E1Diethylphthalate
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.15 12/13/19SW-846 8270E12,4-Dimethylphenol
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.16 12/13/19SW-846 8270E1Dimethylphthalate
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.37 12/13/19SW-846 8270E14,6-Dinitro-2-methylphenol
ND 0.82 12/16/19 16:02 KLBmg/Kg dry0.57 12/13/19SW-846 8270E12,4-Dinitrophenol
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.20 12/13/19SW-846 8270E12,4-Dinitrotoluene
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.20 12/13/19SW-846 8270E12,6-Dinitrotoluene
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.19 12/13/19SW-846 8270E1Di-n-octylphthalate
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.12 12/13/19SW-846 8270E11,2-Diphenylhydrazine/Azobenzene
0.15 0.21 12/16/19 16:02 KLBmg/Kg dry0.12 12/13/19SW-846 8270E1JFluoranthene
ND 0.21 12/16/19 16:02 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Fluorene
Page 26 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-30
Field Sample #: 13-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 11:50:00AM
Stop Date/Time: 12/9/2019 12:50:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.11 12/13/19SW-846 8270E1Hexachlorobenzene
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.16 12/13/19SW-846 8270E1Hexachlorobutadiene
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.35 12/13/19SW-846 8270E1Hexachlorocyclopentadiene
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Hexachloroethane
ND 0.21 12/16/19 16:02 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Indeno(1,2,3-cd)pyrene
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Isophorone
ND 0.21 12/16/19 16:02 KLBmg/Kg dry0.11 12/13/19SW-846 8270E11-Methylnaphthalene
ND 0.21 12/16/19 16:02 KLBmg/Kg dry0.14 12/13/19SW-846 8270E12-Methylnaphthalene
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.16 12/13/19SW-846 8270E12-Methylphenol
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.15 12/13/19SW-846 8270E13/4-Methylphenol
ND 0.21 12/16/19 16:02 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Naphthalene
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.25 12/13/19SW-846 8270E12-Nitroaniline
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.17 12/13/19SW-846 8270E13-Nitroaniline
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.16 12/13/19SW-846 8270E14-Nitroaniline
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.17 12/13/19SW-846 8270E1Nitrobenzene
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.17 12/13/19SW-846 8270E12-Nitrophenol
ND 0.82 12/16/19 16:02 KLBmg/Kg dry0.30 12/13/19SW-846 8270E14-Nitrophenol
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.22 12/13/19SW-846 8270E1N-Nitrosodimethylamine
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.12 12/13/19SW-846 8270E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.19 12/13/19SW-846 8270E1N-Nitrosodi-n-propylamine
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Pentachloronitrobenzene
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.29 12/13/19SW-846 8270E1Pentachlorophenol
ND 0.21 12/16/19 16:02 KLBmg/Kg dry0.11 12/13/19SW-846 8270E1Phenanthrene
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.15 12/13/19SW-846 8270E1Phenol
ND 0.21 12/16/19 16:02 KLBmg/Kg dry0.14 12/13/19SW-846 8270E1Pyrene
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.12 12/13/19SW-846 8270E1V-05Pyridine
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.16 12/13/19SW-846 8270E11,2,4,5-Tetrachlorobenzene
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.14 12/13/19SW-846 8270E11,2,4-Trichlorobenzene
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.15 12/13/19SW-846 8270E12,4,5-Trichlorophenol
ND 0.42 12/16/19 16:02 KLBmg/Kg dry0.15 12/13/19SW-846 8270E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 59.2 12/16/19 16:0230-130
Phenol-d6 59.4 12/16/19 16:0230-130
Nitrobenzene-d5 56.5 12/16/19 16:0230-130
2-Fluorobiphenyl 79.6 12/16/19 16:0230-130
2,4,6-Tribromophenol 70.2 12/16/19 16:0230-130
p-Terphenyl-d14 68.2 12/16/19 16:0230-130
Page 27 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-30
Field Sample #: 13-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 11:50:00AM
Stop Date/Time: 12/9/2019 12:50:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
0.76 0.21 12/18/19 16:28 MJHmg/Kg dry0.039 12/17/19SW-846 6020B5Arsenic
8.0 5.2 12/18/19 16:28 MJHmg/Kg dry0.15 12/17/19SW-846 6020B5Chromium
13 2.1 12/18/19 16:28 MJHmg/Kg dry0.027 12/17/19SW-846 6020B5Lead
0.026 0.031 12/14/19 11:52 AJLmg/Kg dry0.0093 12/13/19SW-846 7471B1JMercury
ND 1.7 12/18/19 16:28 MJHmg/Kg dry0.12 12/17/19SW-846 6020B5Selenium
ND 0.10 12/18/19 16:28 MJHmg/Kg dry0.019 12/17/19SW-846 6020B5Silver
17 10 12/18/19 16:28 MJHmg/Kg dry0.092 12/17/19SW-846 6020B5Barium
0.052 0.42 12/18/19 16:28 MJHmg/Kg dry0.018 12/17/19SW-846 6020B5JCadmium
Page 28 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-30
Field Sample #: 13-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 11:50:00AM
Stop Date/Time: 12/9/2019 12:50:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
80.1 12/12/19 21:02 adb% Wt 12/12/19SM 2540G1% Solids
Page 29 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-31
Field Sample #: DUP-1
Sample Matrix: Soil
Sampled: 12/9/2019 11:40
[TOC_2]19L0324-31[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.098 12/11/19 9:33 MFFmg/Kg dry0.023 12/11/19SW-846 8260D1Acetone
ND 0.0059 12/11/19 9:33 MFFmg/Kg dry0.0024 12/11/19SW-846 8260D1Acrylonitrile
ND 0.00098 12/11/19 9:33 MFFmg/Kg dry0.00069 12/11/19SW-846 8260D1tert-Amyl Methyl Ether (TAME)
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00069 12/11/19SW-846 8260D1Benzene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00078 12/11/19SW-846 8260D1Bromobenzene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.0014 12/11/19SW-846 8260D1Bromochloromethane
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00059 12/11/19SW-846 8260D1Bromodichloromethane
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.0014 12/11/19SW-846 8260D1Bromoform
ND 0.0098 12/11/19 9:33 MFFmg/Kg dry0.0041 12/11/19SW-846 8260D1V-34Bromomethane
ND 0.039 12/11/19 9:33 MFFmg/Kg dry0.017 12/11/19SW-846 8260D12-Butanone (MEK)
ND 0.039 12/11/19 9:33 MFFmg/Kg dry0.020 12/11/19SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00069 12/11/19SW-846 8260D1n-Butylbenzene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00098 12/11/19SW-846 8260D1sec-Butylbenzene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00088 12/11/19SW-846 8260D1tert-Butylbenzene
ND 0.00098 12/11/19 9:33 MFFmg/Kg dry0.00059 12/11/19SW-846 8260D1tert-Butyl Ethyl Ether (TBEE)
ND 0.0059 12/11/19 9:33 MFFmg/Kg dry0.0042 12/11/19SW-846 8260D1Carbon Disulfide
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00078 12/11/19SW-846 8260D1Carbon Tetrachloride
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00069 12/11/19SW-846 8260D1Chlorobenzene
ND 0.00098 12/11/19 9:33 MFFmg/Kg dry0.00069 12/11/19SW-846 8260D1Chlorodibromomethane
ND 0.020 12/11/19 9:33 MFFmg/Kg dry0.0015 12/11/19SW-846 8260D1Chloroethane
ND 0.0039 12/11/19 9:33 MFFmg/Kg dry0.00069 12/11/19SW-846 8260D1Chloroform
ND 0.0098 12/11/19 9:33 MFFmg/Kg dry0.0063 12/11/19SW-846 8260D1V-05Chloromethane
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00078 12/11/19SW-846 8260D12-Chlorotoluene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00078 12/11/19SW-846 8260D14-Chlorotoluene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.0011 12/11/19SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.00098 12/11/19 9:33 MFFmg/Kg dry0.00098 12/11/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00059 12/11/19SW-846 8260D1Dibromomethane
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00069 12/11/19SW-846 8260D11,2-Dichlorobenzene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00069 12/11/19SW-846 8260D11,3-Dichlorobenzene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00078 12/11/19SW-846 8260D11,4-Dichlorobenzene
ND 0.0039 12/11/19 9:33 MFFmg/Kg dry0.0021 12/11/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 0.020 12/11/19 9:33 MFFmg/Kg dry0.0013 12/11/19SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00069 12/11/19SW-846 8260D11,1-Dichloroethane
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.0013 12/11/19SW-846 8260D11,2-Dichloroethane
ND 0.0039 12/11/19 9:33 MFFmg/Kg dry0.0011 12/11/19SW-846 8260D11,1-Dichloroethylene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00078 12/11/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00088 12/11/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.0013 12/11/19SW-846 8260D11,2-Dichloropropane
ND 0.00098 12/11/19 9:33 MFFmg/Kg dry0.00069 12/11/19SW-846 8260D11,3-Dichloropropane
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00088 12/11/19SW-846 8260D12,2-Dichloropropane
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00088 12/11/19SW-846 8260D11,1-Dichloropropene
ND 0.00098 12/11/19 9:33 MFFmg/Kg dry0.00069 12/11/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.00098 12/11/19 9:33 MFFmg/Kg dry0.00069 12/11/19SW-846 8260D1trans-1,3-Dichloropropene
ND 0.020 12/11/19 9:33 MFFmg/Kg dry0.0018 12/11/19SW-846 8260D1Diethyl Ether
Page 30 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-31
Field Sample #: DUP-1
Sample Matrix: Soil
Sampled: 12/9/2019 11:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.00098 12/11/19 9:33 MFFmg/Kg dry0.00059 12/11/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 0.098 12/11/19 9:33 MFFmg/Kg dry0.056 12/11/19SW-846 8260D11,4-Dioxane
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00078 12/11/19SW-846 8260D1Ethylbenzene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00098 12/11/19SW-846 8260D1Hexachlorobutadiene
ND 0.020 12/11/19 9:33 MFFmg/Kg dry0.011 12/11/19SW-846 8260D12-Hexanone (MBK)
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00069 12/11/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00078 12/11/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 0.0039 12/11/19 9:33 MFFmg/Kg dry0.00088 12/11/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 0.020 12/11/19 9:33 MFFmg/Kg dry0.0070 12/11/19SW-846 8260D1Methylene Chloride
ND 0.020 12/11/19 9:33 MFFmg/Kg dry0.0074 12/11/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 0.0039 12/11/19 9:33 MFFmg/Kg dry0.00069 12/11/19SW-846 8260D1Naphthalene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00069 12/11/19SW-846 8260D1n-Propylbenzene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00059 12/11/19SW-846 8260D1Styrene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.0018 12/11/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.00098 12/11/19 9:33 MFFmg/Kg dry0.00088 12/11/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.0013 12/11/19SW-846 8260D1Tetrachloroethylene
ND 0.0098 12/11/19 9:33 MFFmg/Kg dry0.0022 12/11/19SW-846 8260D1Tetrahydrofuran
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00078 12/11/19SW-846 8260D1Toluene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00059 12/11/19SW-846 8260D11,2,3-Trichlorobenzene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00078 12/11/19SW-846 8260D11,2,4-Trichlorobenzene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00069 12/11/19SW-846 8260D11,3,5-Trichlorobenzene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00098 12/11/19SW-846 8260D11,1,1-Trichloroethane
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.0012 12/11/19SW-846 8260D11,1,2-Trichloroethane
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00098 12/11/19SW-846 8260D1Trichloroethylene
ND 0.0098 12/11/19 9:33 MFFmg/Kg dry0.0011 12/11/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.0011 12/11/19SW-846 8260D11,2,3-Trichloropropane
ND 0.0098 12/11/19 9:33 MFFmg/Kg dry0.00088 12/11/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00078 12/11/19SW-846 8260D11,2,4-Trimethylbenzene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00059 12/11/19SW-846 8260D11,3,5-Trimethylbenzene
ND 0.0098 12/11/19 9:33 MFFmg/Kg dry0.0011 12/11/19SW-846 8260D1Vinyl Chloride
ND 0.0039 12/11/19 9:33 MFFmg/Kg dry0.0017 12/11/19SW-846 8260D1m+p Xylene
ND 0.0020 12/11/19 9:33 MFFmg/Kg dry0.00069 12/11/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 95.6 12/11/19 9:3370-130
Toluene-d8 97.5 12/11/19 9:3370-130
4-Bromofluorobenzene 102 12/11/19 9:3370-130
Page 31 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-31
Field Sample #: DUP-1
Sample Matrix: Soil
Sampled: 12/9/2019 11:40
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
80.2 12/17/19 9:15 CBM% Wt 12/16/19SM 2540G1% Solids
Page 32 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-32
Field Sample #: DUP-2
Sample Matrix: Soil
Sampled: 12/9/2019 00:00
[TOC_2]19L0324-32[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.21 12/18/19 15:36 BGLmg/Kg dry0.11 12/16/19SW-846 8270E1Acenaphthene
ND 0.21 12/18/19 15:36 BGLmg/Kg dry0.14 12/16/19SW-846 8270E1Acenaphthylene
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.16 12/16/19SW-846 8270E1Acetophenone
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.10 12/16/19SW-846 8270E1Aniline
ND 0.21 12/18/19 15:36 BGLmg/Kg dry0.11 12/16/19SW-846 8270E1Anthracene
ND 0.82 12/18/19 15:36 BGLmg/Kg dry0.22 12/16/19SW-846 8270E1R-05, V-35Benzidine
ND 0.21 12/18/19 15:36 BGLmg/Kg dry0.14 12/16/19SW-846 8270E1Benzo(a)anthracene
ND 0.21 12/18/19 15:36 BGLmg/Kg dry0.14 12/16/19SW-846 8270E1Benzo(a)pyrene
ND 0.21 12/18/19 15:36 BGLmg/Kg dry0.14 12/16/19SW-846 8270E1Benzo(b)fluoranthene
ND 0.21 12/18/19 15:36 BGLmg/Kg dry0.12 12/16/19SW-846 8270E1Benzo(g,h,i)perylene
ND 0.21 12/18/19 15:36 BGLmg/Kg dry0.14 12/16/19SW-846 8270E1Benzo(k)fluoranthene
ND 1.2 12/18/19 15:36 BGLmg/Kg dry0.74 12/16/19SW-846 8270E1V-34Benzoic Acid
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.17 12/16/19SW-846 8270E1Bis(2-chloroethoxy)methane
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.21 12/16/19SW-846 8270E1Bis(2-chloroethyl)ether
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.29 12/16/19SW-846 8270E1V-20Bis(2-chloroisopropyl)ether
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.12 12/16/19SW-846 8270E1Bis(2-Ethylhexyl)phthalate
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.12 12/16/19SW-846 8270E14-Bromophenylphenylether
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.15 12/16/19SW-846 8270E1Butylbenzylphthalate
ND 0.21 12/18/19 15:36 BGLmg/Kg dry0.11 12/16/19SW-846 8270E1Carbazole
ND 0.82 12/18/19 15:36 BGLmg/Kg dry0.17 12/16/19SW-846 8270E14-Chloroaniline
ND 0.82 12/18/19 15:36 BGLmg/Kg dry0.17 12/16/19SW-846 8270E14-Chloro-3-methylphenol
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.12 12/16/19SW-846 8270E12-Chloronaphthalene
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.15 12/16/19SW-846 8270E12-Chlorophenol
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.15 12/16/19SW-846 8270E14-Chlorophenylphenylether
ND 0.21 12/18/19 15:36 BGLmg/Kg dry0.14 12/16/19SW-846 8270E1Chrysene
ND 0.21 12/18/19 15:36 BGLmg/Kg dry0.12 12/16/19SW-846 8270E1Dibenz(a,h)anthracene
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.15 12/16/19SW-846 8270E1Dibenzofuran
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.12 12/16/19SW-846 8270E1Di-n-butylphthalate
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.12 12/16/19SW-846 8270E11,2-Dichlorobenzene
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.12 12/16/19SW-846 8270E11,3-Dichlorobenzene
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.11 12/16/19SW-846 8270E11,4-Dichlorobenzene
ND 0.21 12/18/19 15:36 BGLmg/Kg dry0.16 12/16/19SW-846 8270E13,3-Dichlorobenzidine
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.12 12/16/19SW-846 8270E12,4-Dichlorophenol
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.17 12/16/19SW-846 8270E1Diethylphthalate
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.15 12/16/19SW-846 8270E12,4-Dimethylphenol
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.16 12/16/19SW-846 8270E1Dimethylphthalate
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.37 12/16/19SW-846 8270E14,6-Dinitro-2-methylphenol
ND 0.82 12/18/19 15:36 BGLmg/Kg dry0.57 12/16/19SW-846 8270E12,4-Dinitrophenol
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.20 12/16/19SW-846 8270E12,4-Dinitrotoluene
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.20 12/16/19SW-846 8270E12,6-Dinitrotoluene
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.19 12/16/19SW-846 8270E1Di-n-octylphthalate
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.12 12/16/19SW-846 8270E11,2-Diphenylhydrazine/Azobenzene
0.13 0.21 12/18/19 15:36 BGLmg/Kg dry0.12 12/16/19SW-846 8270E1JFluoranthene
ND 0.21 12/18/19 15:36 BGLmg/Kg dry0.15 12/16/19SW-846 8270E1Fluorene
Page 33 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-32
Field Sample #: DUP-2
Sample Matrix: Soil
Sampled: 12/9/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Semivolatile Organic Compounds by GC/MS
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.11 12/16/19SW-846 8270E1Hexachlorobenzene
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.16 12/16/19SW-846 8270E1Hexachlorobutadiene
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.35 12/16/19SW-846 8270E1Hexachlorocyclopentadiene
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.14 12/16/19SW-846 8270E1Hexachloroethane
ND 0.21 12/18/19 15:36 BGLmg/Kg dry0.15 12/16/19SW-846 8270E1Indeno(1,2,3-cd)pyrene
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.15 12/16/19SW-846 8270E1Isophorone
ND 0.21 12/18/19 15:36 BGLmg/Kg dry0.11 12/16/19SW-846 8270E11-Methylnaphthalene
ND 0.21 12/18/19 15:36 BGLmg/Kg dry0.14 12/16/19SW-846 8270E12-Methylnaphthalene
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.16 12/16/19SW-846 8270E12-Methylphenol
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.15 12/16/19SW-846 8270E13/4-Methylphenol
ND 0.21 12/18/19 15:36 BGLmg/Kg dry0.14 12/16/19SW-846 8270E1Naphthalene
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.25 12/16/19SW-846 8270E12-Nitroaniline
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.17 12/16/19SW-846 8270E13-Nitroaniline
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.16 12/16/19SW-846 8270E14-Nitroaniline
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.17 12/16/19SW-846 8270E1Nitrobenzene
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.17 12/16/19SW-846 8270E12-Nitrophenol
ND 0.82 12/18/19 15:36 BGLmg/Kg dry0.30 12/16/19SW-846 8270E14-Nitrophenol
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.22 12/16/19SW-846 8270E1V-20N-Nitrosodimethylamine
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.12 12/16/19SW-846 8270E1N-Nitrosodiphenylamine/Diphenylamine
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.19 12/16/19SW-846 8270E1N-Nitrosodi-n-propylamine
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.15 12/16/19SW-846 8270E1Pentachloronitrobenzene
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.29 12/16/19SW-846 8270E1Pentachlorophenol
ND 0.21 12/18/19 15:36 BGLmg/Kg dry0.11 12/16/19SW-846 8270E1Phenanthrene
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.15 12/16/19SW-846 8270E1Phenol
ND 0.21 12/18/19 15:36 BGLmg/Kg dry0.14 12/16/19SW-846 8270E1Pyrene
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.12 12/16/19SW-846 8270E1L-04Pyridine
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.16 12/16/19SW-846 8270E11,2,4,5-Tetrachlorobenzene
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.14 12/16/19SW-846 8270E11,2,4-Trichlorobenzene
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.15 12/16/19SW-846 8270E12,4,5-Trichlorophenol
ND 0.42 12/18/19 15:36 BGLmg/Kg dry0.15 12/16/19SW-846 8270E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 58.3 12/18/19 15:3630-130
Phenol-d6 60.8 12/18/19 15:3630-130
Nitrobenzene-d5 56.2 12/18/19 15:3630-130
2-Fluorobiphenyl 79.3 12/18/19 15:3630-130
2,4,6-Tribromophenol 64.2 12/18/19 15:3630-130
p-Terphenyl-d14 70.8 12/18/19 15:3630-130
Page 34 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-32
Field Sample #: DUP-2
Sample Matrix: Soil
Sampled: 12/9/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Metals Analyses (Total)
1.5 0.21 12/18/19 16:31 MJHmg/Kg dry0.038 12/17/19SW-846 6020B5Arsenic
28 5.1 12/18/19 16:31 MJHmg/Kg dry0.15 12/17/19SW-846 6020B5Chromium
33 2.1 12/18/19 16:31 MJHmg/Kg dry0.027 12/17/19SW-846 6020B5Lead
0.074 0.032 12/17/19 12:39 AJLmg/Kg dry0.0096 12/16/19SW-846 7471B1Mercury
0.33 1.6 12/18/19 16:31 MJHmg/Kg dry0.12 12/17/19SW-846 6020B5JSelenium
0.032 0.10 12/18/19 16:31 MJHmg/Kg dry0.019 12/17/19SW-846 6020B5JSilver
35 10 12/18/19 16:31 MJHmg/Kg dry0.091 12/17/19SW-846 6020B5Barium
0.13 0.41 12/18/19 16:31 MJHmg/Kg dry0.018 12/17/19SW-846 6020B5JCadmium
Page 35 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-32
Field Sample #: DUP-2
Sample Matrix: Soil
Sampled: 12/9/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
79.1 12/17/19 9:15 CBM% Wt 12/16/19SM 2540G1% Solids
Page 36 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-33
Field Sample #: Trip Blank
Sample Matrix: Trip Blank Water
Sampled: 12/9/2019 00:00
[TOC_2]19L0324-33[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 50 12/14/19 4:53 EEHg/L3.8 12/13/19SW-846 8260D1Acetone
ND 5.0 12/14/19 4:53 EEHg/L0.52 12/13/19SW-846 8260D1Acrylonitrile
ND 1.0 12/14/19 4:53 EEHg/L0.14 12/13/19SW-846 8260D1L-04, V-05tert-Amyl Methyl Ether (TAME)
ND 1.0 12/14/19 4:53 EEHg/L0.18 12/13/19SW-846 8260D1Benzene
ND 1.0 12/14/19 4:53 EEHg/L0.15 12/13/19SW-846 8260D1Bromobenzene
ND 1.0 12/14/19 4:53 EEHg/L0.32 12/13/19SW-846 8260D1Bromochloromethane
ND 0.50 12/14/19 4:53 EEHg/L0.16 12/13/19SW-846 8260D1Bromodichloromethane
ND 1.0 12/14/19 4:53 EEHg/L0.46 12/13/19SW-846 8260D1Bromoform
ND 2.0 12/14/19 4:53 EEHg/L0.78 12/13/19SW-846 8260D1Bromomethane
ND 20 12/14/19 4:53 EEHg/L1.9 12/13/19SW-846 8260D12-Butanone (MEK)
ND 20 12/14/19 4:53 EEHg/L4.2 12/13/19SW-846 8260D1tert-Butyl Alcohol (TBA)
ND 1.0 12/14/19 4:53 EEHg/L0.21 12/13/19SW-846 8260D1n-Butylbenzene
ND 1.0 12/14/19 4:53 EEHg/L0.16 12/13/19SW-846 8260D1sec-Butylbenzene
ND 1.0 12/14/19 4:53 EEHg/L0.17 12/13/19SW-846 8260D1tert-Butylbenzene
ND 0.50 12/14/19 4:53 EEHg/L0.16 12/13/19SW-846 8260D1V-05tert-Butyl Ethyl Ether (TBEE)
ND 5.0 12/14/19 4:53 EEHg/L4.4 12/13/19SW-846 8260D1Carbon Disulfide
ND 1.0 12/14/19 4:53 EEHg/L0.11 12/13/19SW-846 8260D1Carbon Tetrachloride
ND 1.0 12/14/19 4:53 EEHg/L0.15 12/13/19SW-846 8260D1Chlorobenzene
ND 0.50 12/14/19 4:53 EEHg/L0.21 12/13/19SW-846 8260D1Chlorodibromomethane
ND 2.0 12/14/19 4:53 EEHg/L0.35 12/13/19SW-846 8260D1Chloroethane
ND 2.0 12/14/19 4:53 EEHg/L0.17 12/13/19SW-846 8260D1Chloroform
ND 2.0 12/14/19 4:53 EEHg/L0.45 12/13/19SW-846 8260D1Chloromethane
ND 1.0 12/14/19 4:53 EEHg/L0.12 12/13/19SW-846 8260D12-Chlorotoluene
ND 1.0 12/14/19 4:53 EEHg/L0.14 12/13/19SW-846 8260D14-Chlorotoluene
ND 5.0 12/14/19 4:53 EEHg/L0.53 12/13/19SW-846 8260D11,2-Dibromo-3-chloropropane (DBCP)
ND 0.50 12/14/19 4:53 EEHg/L0.19 12/13/19SW-846 8260D11,2-Dibromoethane (EDB)
ND 1.0 12/14/19 4:53 EEHg/L0.37 12/13/19SW-846 8260D1Dibromomethane
ND 1.0 12/14/19 4:53 EEHg/L0.16 12/13/19SW-846 8260D11,2-Dichlorobenzene
ND 1.0 12/14/19 4:53 EEHg/L0.12 12/13/19SW-846 8260D11,3-Dichlorobenzene
ND 1.0 12/14/19 4:53 EEHg/L0.13 12/13/19SW-846 8260D11,4-Dichlorobenzene
ND 2.0 12/14/19 4:53 EEHg/L0.31 12/13/19SW-846 8260D1trans-1,4-Dichloro-2-butene
ND 2.0 12/14/19 4:53 EEHg/L0.26 12/13/19SW-846 8260D1Dichlorodifluoromethane (Freon 12)
ND 1.0 12/14/19 4:53 EEHg/L0.16 12/13/19SW-846 8260D11,1-Dichloroethane
ND 1.0 12/14/19 4:53 EEHg/L0.41 12/13/19SW-846 8260D11,2-Dichloroethane
ND 1.0 12/14/19 4:53 EEHg/L0.32 12/13/19SW-846 8260D11,1-Dichloroethylene
ND 1.0 12/14/19 4:53 EEHg/L0.13 12/13/19SW-846 8260D1cis-1,2-Dichloroethylene
ND 1.0 12/14/19 4:53 EEHg/L0.31 12/13/19SW-846 8260D1trans-1,2-Dichloroethylene
ND 1.0 12/14/19 4:53 EEHg/L0.20 12/13/19SW-846 8260D11,2-Dichloropropane
ND 0.50 12/14/19 4:53 EEHg/L0.11 12/13/19SW-846 8260D11,3-Dichloropropane
ND 1.0 12/14/19 4:53 EEHg/L0.20 12/13/19SW-846 8260D12,2-Dichloropropane
ND 2.0 12/14/19 4:53 EEHg/L0.16 12/13/19SW-846 8260D11,1-Dichloropropene
ND 0.50 12/14/19 4:53 EEHg/L0.13 12/13/19SW-846 8260D1cis-1,3-Dichloropropene
ND 0.50 12/14/19 4:53 EEHg/L0.23 12/13/19SW-846 8260D1trans-1,3-Dichloropropene
ND 2.0 12/14/19 4:53 EEHg/L0.34 12/13/19SW-846 8260D1Diethyl Ether
Page 37 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/9/2019
Work Order: 19L0324Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0324-33
Field Sample #: Trip Blank
Sample Matrix: Trip Blank Water
Sampled: 12/9/2019 00:00
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Volatile Organic Compounds by GC/MS
ND 0.50 12/14/19 4:53 EEHg/L0.17 12/13/19SW-846 8260D1Diisopropyl Ether (DIPE)
ND 50 12/14/19 4:53 EEHg/L22 12/13/19SW-846 8260D11,4-Dioxane
ND 1.0 12/14/19 4:53 EEHg/L0.13 12/13/19SW-846 8260D1Ethylbenzene
ND 0.60 12/14/19 4:53 EEHg/L0.47 12/13/19SW-846 8260D1Hexachlorobutadiene
ND 10 12/14/19 4:53 EEHg/L1.5 12/13/19SW-846 8260D12-Hexanone (MBK)
ND 1.0 12/14/19 4:53 EEHg/L0.17 12/13/19SW-846 8260D1Isopropylbenzene (Cumene)
ND 1.0 12/14/19 4:53 EEHg/L0.20 12/13/19SW-846 8260D1p-Isopropyltoluene (p-Cymene)
ND 1.0 12/14/19 4:53 EEHg/L0.25 12/13/19SW-846 8260D1Methyl tert-Butyl Ether (MTBE)
ND 5.0 12/14/19 4:53 EEHg/L0.34 12/13/19SW-846 8260D1Methylene Chloride
ND 10 12/14/19 4:53 EEHg/L1.7 12/13/19SW-846 8260D14-Methyl-2-pentanone (MIBK)
ND 5.0 12/14/19 4:53 EEHg/L0.31 12/13/19SW-846 8260D1Naphthalene
ND 1.0 12/14/19 4:53 EEHg/L0.13 12/13/19SW-846 8260D1n-Propylbenzene
ND 1.0 12/14/19 4:53 EEHg/L0.11 12/13/19SW-846 8260D1Styrene
ND 1.0 12/14/19 4:53 EEHg/L0.27 12/13/19SW-846 8260D11,1,1,2-Tetrachloroethane
ND 0.50 12/14/19 4:53 EEHg/L0.22 12/13/19SW-846 8260D11,1,2,2-Tetrachloroethane
ND 1.0 12/14/19 4:53 EEHg/L0.18 12/13/19SW-846 8260D1Tetrachloroethylene
ND 10 12/14/19 4:53 EEHg/L0.51 12/13/19SW-846 8260D1Tetrahydrofuran
ND 1.0 12/14/19 4:53 EEHg/L0.14 12/13/19SW-846 8260D1Toluene
ND 5.0 12/14/19 4:53 EEHg/L0.57 12/13/19SW-846 8260D1V-051,2,3-Trichlorobenzene
ND 1.0 12/14/19 4:53 EEHg/L0.40 12/13/19SW-846 8260D11,2,4-Trichlorobenzene
ND 1.0 12/14/19 4:53 EEHg/L0.30 12/13/19SW-846 8260D11,3,5-Trichlorobenzene
ND 1.0 12/14/19 4:53 EEHg/L0.20 12/13/19SW-846 8260D11,1,1-Trichloroethane
ND 1.0 12/14/19 4:53 EEHg/L0.16 12/13/19SW-846 8260D11,1,2-Trichloroethane
ND 1.0 12/14/19 4:53 EEHg/L0.24 12/13/19SW-846 8260D1Trichloroethylene
ND 2.0 12/14/19 4:53 EEHg/L0.33 12/13/19SW-846 8260D1Trichlorofluoromethane (Freon 11)
ND 2.0 12/14/19 4:53 EEHg/L0.25 12/13/19SW-846 8260D11,2,3-Trichloropropane
ND 1.0 12/14/19 4:53 EEHg/L0.32 12/13/19SW-846 8260D11,1,2-Trichloro-1,2,2-trifluoroethane
(Freon 113)
ND 1.0 12/14/19 4:53 EEHg/L0.18 12/13/19SW-846 8260D11,2,4-Trimethylbenzene
ND 1.0 12/14/19 4:53 EEHg/L0.14 12/13/19SW-846 8260D11,3,5-Trimethylbenzene
ND 2.0 12/14/19 4:53 EEHg/L0.45 12/13/19SW-846 8260D1Vinyl Chloride
ND 2.0 12/14/19 4:53 EEHg/L0.30 12/13/19SW-846 8260D1m+p Xylene
ND 1.0 12/14/19 4:53 EEHg/L0.17 12/13/19SW-846 8260D1o-Xylene
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 97.2 12/14/19 4:5370-130
Toluene-d8 98.3 12/14/19 4:5370-130
4-Bromofluorobenzene 93.8 12/14/19 4:5370-130
Page 38 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]Batch Date
B248207 12/12/1919L0324-02 [11-2]
B248207 12/12/1919L0324-12 [12-4]
B248207 12/12/1919L0324-24 [13-7]
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]Batch Date
B248245 12/12/1919L0324-28 [11-COMP]
B248245 12/12/1919L0324-29 [12-COMP]
B248245 12/12/1919L0324-30 [13-COMP]
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]Batch Date
B248451 12/16/1919L0324-31 [DUP-1]
B248451 12/16/1919L0324-32 [DUP-2]
Prep Method: SW-846 3050B-SW-846 6020B
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B248472 12/17/191.53 50.019L0324-28 [11-COMP]
B248472 12/17/191.51 50.019L0324-29 [12-COMP]
B248472 12/17/191.50 50.019L0324-30 [13-COMP]
B248472 12/17/191.54 50.019L0324-32 [DUP-2]
Prep Method: SW-846 7471-SW-846 7471B
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B248355 12/13/190.617 50.019L0324-28 [11-COMP]
B248355 12/13/190.613 50.019L0324-29 [12-COMP]
B248355 12/13/190.603 50.019L0324-30 [13-COMP]
Prep Method: SW-846 7471-SW-846 7471B
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B248457 12/16/190.595 50.019L0324-32 [DUP-2]
Prep Method: SW-846 5035-SW-846 8260D
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B248105 12/11/196.75 10.019L0324-02 [11-2]
B248105 12/11/196.55 10.019L0324-12 [12-4]
B248105 12/11/196.80 10.019L0324-24 [13-7]
B248105 12/11/196.37 10.019L0324-31 [DUP-1]
[TOC_1]Sample Preparation Information[TOC]
Page 39 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 5030B-SW-846 8260D
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
B248317 12/13/195 5.0019L0324-33 [Trip Blank]
Prep Method: SW-846 3546-SW-846 8270E
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B248288 12/13/1930.0 1.0019L0324-28RE1 [11-COMP]
B248288 12/13/1930.0 1.0019L0324-29RE1 [12-COMP]
B248288 12/13/1930.0 1.0019L0324-30RE1 [13-COMP]
Prep Method: SW-846 3546-SW-846 8270E
Lab Number [Field ID]Batch DateInitial [g]Final [mL]
B248463 12/16/1930.4 1.0019L0324-32 [DUP-2]
Page 40 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Volatile Organic Compounds by GC/MS[TOC]
Batch B248105 - SW-846 5035
[TOC_3]B248105[TOC]
Blank (B248105-BLK1) Prepared & Analyzed: 12/11/19
Acetone mg/Kg wet0.10ND
Acrylonitrile mg/Kg wet0.0060ND
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010ND
Benzene mg/Kg wet0.0020ND
Bromobenzene mg/Kg wet0.0020ND
Bromochloromethane mg/Kg wet0.0020ND
Bromodichloromethane mg/Kg wet0.0020ND
Bromoform mg/Kg wet0.0020ND
Bromomethane mg/Kg wet0.010 V-34ND
2-Butanone (MEK)mg/Kg wet0.040ND
tert-Butyl Alcohol (TBA)mg/Kg wet0.040ND
n-Butylbenzene mg/Kg wet0.0020ND
sec-Butylbenzene mg/Kg wet0.0020ND
tert-Butylbenzene mg/Kg wet0.0020ND
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010ND
Carbon Disulfide mg/Kg wet0.0060ND
Carbon Tetrachloride mg/Kg wet0.0020ND
Chlorobenzene mg/Kg wet0.0020ND
Chlorodibromomethane mg/Kg wet0.0010ND
Chloroethane mg/Kg wet0.020ND
Chloroform mg/Kg wet0.0040ND
Chloromethane mg/Kg wet0.010 V-05ND
2-Chlorotoluene mg/Kg wet0.0020ND
4-Chlorotoluene mg/Kg wet0.0020ND
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020ND
1,2-Dibromoethane (EDB)mg/Kg wet0.0010ND
Dibromomethane mg/Kg wet0.0020ND
1,2-Dichlorobenzene mg/Kg wet0.0020ND
1,3-Dichlorobenzene mg/Kg wet0.0020ND
1,4-Dichlorobenzene mg/Kg wet0.0020ND
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040ND
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020ND
1,1-Dichloroethane mg/Kg wet0.0020ND
1,2-Dichloroethane mg/Kg wet0.0020ND
1,1-Dichloroethylene mg/Kg wet0.0040ND
cis-1,2-Dichloroethylene mg/Kg wet0.0020ND
trans-1,2-Dichloroethylene mg/Kg wet0.0020ND
1,2-Dichloropropane mg/Kg wet0.0020ND
1,3-Dichloropropane mg/Kg wet0.0010ND
2,2-Dichloropropane mg/Kg wet0.0020ND
1,1-Dichloropropene mg/Kg wet0.0020ND
cis-1,3-Dichloropropene mg/Kg wet0.0010ND
trans-1,3-Dichloropropene mg/Kg wet0.0010ND
Diethyl Ether mg/Kg wet0.020ND
Diisopropyl Ether (DIPE)mg/Kg wet0.0010ND
1,4-Dioxane mg/Kg wet0.10ND
Ethanol mg/Kg wet0.20ND
Ethylbenzene mg/Kg wet0.0020ND
Hexachlorobutadiene mg/Kg wet0.0020ND
2-Hexanone (MBK)mg/Kg wet0.020ND
Isopropylbenzene (Cumene)mg/Kg wet0.0020ND
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020ND
[TOC_1]QC Data[TOC]
Page 41 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248105 - SW-846 5035
Blank (B248105-BLK1) Prepared & Analyzed: 12/11/19
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040ND
Methylene Chloride mg/Kg wet0.020 J0.0033
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020ND
Naphthalene mg/Kg wet0.0040ND
n-Propylbenzene mg/Kg wet0.0020ND
Styrene mg/Kg wet0.0020ND
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020ND
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010ND
Tetrachloroethylene mg/Kg wet0.0020ND
Tetrahydrofuran mg/Kg wet0.010ND
Toluene mg/Kg wet0.0020ND
1,2,3-Trichlorobenzene mg/Kg wet0.0020ND
1,2,4-Trichlorobenzene mg/Kg wet0.0020ND
1,3,5-Trichlorobenzene mg/Kg wet0.0020ND
1,1,1-Trichloroethane mg/Kg wet0.0020ND
1,1,2-Trichloroethane mg/Kg wet0.0020ND
Trichloroethylene mg/Kg wet0.0020ND
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010ND
1,2,3-Trichloropropane mg/Kg wet0.0020ND
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010ND
1,2,4-Trimethylbenzene mg/Kg wet0.0020ND
1,3,5-Trimethylbenzene mg/Kg wet0.0020ND
Vinyl Chloride mg/Kg wet0.010ND
m+p Xylene mg/Kg wet0.0040ND
o-Xylene mg/Kg wet0.0020ND
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 91.40.0457
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 98.60.0493
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1010.0506
LCS (B248105-BS1) Prepared & Analyzed: 12/11/19
Acetone mg/Kg wet0.10 0.200 70-16094.40.189
Acrylonitrile mg/Kg wet0.0060 0.0200 70-13091.60.0183
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010 0.0200 70-13097.10.0194
Benzene mg/Kg wet0.0020 0.0200 70-13089.10.0178
Bromobenzene mg/Kg wet0.0020 0.0200 70-13094.20.0188
Bromochloromethane mg/Kg wet0.0020 0.0200 70-1301120.0225
Bromodichloromethane mg/Kg wet0.0020 0.0200 70-13088.70.0177
Bromoform mg/Kg wet0.0020 0.0200 70-1301100.0220
Bromomethane mg/Kg wet0.010 0.0200 V-3440-13086.60.0173
2-Butanone (MEK)mg/Kg wet0.040 0.200 70-16091.90.184
tert-Butyl Alcohol (TBA)mg/Kg wet0.040 0.200 40-13092.20.184
n-Butylbenzene mg/Kg wet0.0020 0.0200 70-13080.40.0161
sec-Butylbenzene mg/Kg wet0.0020 0.0200 70-13095.40.0191
tert-Butylbenzene mg/Kg wet0.0020 0.0200 70-16091.90.0184
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010 0.0200 70-13093.90.0188
Carbon Disulfide mg/Kg wet0.0060 0.200 70-13087.60.175
Carbon Tetrachloride mg/Kg wet0.0020 0.0200 70-13093.40.0187
Chlorobenzene mg/Kg wet0.0020 0.0200 70-1301030.0207
Chlorodibromomethane mg/Kg wet0.0010 0.0200 70-1301020.0205
Chloroethane mg/Kg wet0.020 0.0200 J70-13091.30.0183
Chloroform mg/Kg wet0.0040 0.0200 70-13088.00.0176
Chloromethane mg/Kg wet0.010 0.0200 V-0570-13076.70.0153
Page 42 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248105 - SW-846 5035
LCS (B248105-BS1) Prepared & Analyzed: 12/11/19
2-Chlorotoluene mg/Kg wet0.0020 0.0200 70-13094.70.0189
4-Chlorotoluene mg/Kg wet0.0020 0.0200 70-13089.90.0180
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020 0.0200 70-13095.80.0192
1,2-Dibromoethane (EDB)mg/Kg wet0.0010 0.0200 70-1301040.0208
Dibromomethane mg/Kg wet0.0020 0.0200 70-1301080.0217
1,2-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-13098.10.0196
1,3-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-13095.50.0191
1,4-Dichlorobenzene mg/Kg wet0.0020 0.0200 70-13090.30.0181
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040 0.0200 70-13090.40.0181
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020 0.0200 J40-16079.90.0160
1,1-Dichloroethane mg/Kg wet0.0020 0.0200 70-13092.00.0184
1,2-Dichloroethane mg/Kg wet0.0020 0.0200 70-1301010.0202
1,1-Dichloroethylene mg/Kg wet0.0040 0.0200 70-13087.60.0175
cis-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 70-13086.50.0173
trans-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 70-13091.60.0183
1,2-Dichloropropane mg/Kg wet0.0020 0.0200 70-13098.20.0196
1,3-Dichloropropane mg/Kg wet0.0010 0.0200 70-1301010.0202
2,2-Dichloropropane mg/Kg wet0.0020 0.0200 70-13083.70.0167
1,1-Dichloropropene mg/Kg wet0.0020 0.0200 70-13088.10.0176
cis-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 70-13099.20.0198
trans-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 70-13093.70.0187
Diethyl Ether mg/Kg wet0.020 0.0200 J70-13089.50.0179
Diisopropyl Ether (DIPE)mg/Kg wet0.0010 0.0200 70-13088.90.0178
1,4-Dioxane mg/Kg wet0.10 0.200 40-16096.00.192
Ethylbenzene mg/Kg wet0.0020 0.0200 70-13086.30.0173
Hexachlorobutadiene mg/Kg wet0.0020 0.0200 70-1601010.0203
2-Hexanone (MBK)mg/Kg wet0.020 0.200 70-16090.90.182
Isopropylbenzene (Cumene)mg/Kg wet0.0020 0.0200 70-1301010.0201
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020 0.0200 70-13090.50.0181
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040 0.0200 70-13094.40.0189
Methylene Chloride mg/Kg wet0.020 0.0200 40-1601150.0230
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020 0.200 70-16092.10.184
Naphthalene mg/Kg wet0.0040 0.0200 40-13088.90.0178
n-Propylbenzene mg/Kg wet0.0020 0.0200 70-13089.50.0179
Styrene mg/Kg wet0.0020 0.0200 70-13097.70.0195
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020 0.0200 70-1301050.0211
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010 0.0200 70-13097.00.0194
Tetrachloroethylene mg/Kg wet0.0020 0.0200 70-1301000.0201
Tetrahydrofuran mg/Kg wet0.010 0.0200 70-1301010.0202
Toluene mg/Kg wet0.0020 0.0200 70-13091.80.0184
1,2,3-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-13097.30.0195
1,2,4-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-13093.90.0188
1,3,5-Trichlorobenzene mg/Kg wet0.0020 0.0200 70-13092.40.0185
1,1,1-Trichloroethane mg/Kg wet0.0020 0.0200 70-13086.10.0172
1,1,2-Trichloroethane mg/Kg wet0.0020 0.0200 70-13095.40.0191
Trichloroethylene mg/Kg wet0.0020 0.0200 70-13093.90.0188
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010 0.0200 70-13090.40.0181
1,2,3-Trichloropropane mg/Kg wet0.0020 0.0200 70-1301010.0203
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010 0.0200 70-13092.10.0184
1,2,4-Trimethylbenzene mg/Kg wet0.0020 0.0200 70-13085.10.0170
1,3,5-Trimethylbenzene mg/Kg wet0.0020 0.0200 70-13093.40.0187
Page 43 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248105 - SW-846 5035
LCS (B248105-BS1) Prepared & Analyzed: 12/11/19
Vinyl Chloride mg/Kg wet0.010 0.0200 40-13083.10.0166
m+p Xylene mg/Kg wet0.0040 0.0400 70-13090.70.0363
o-Xylene mg/Kg wet0.0020 0.0200 70-13091.70.0183
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 91.50.0457
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 98.50.0492
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1010.0505
LCS Dup (B248105-BSD1) Prepared & Analyzed: 12/11/19
Acetone mg/Kg wet0.10 0.200 2570-16093.3 1.090.187
Acrylonitrile mg/Kg wet0.0060 0.0200 2570-13093.0 1.520.0186
tert-Amyl Methyl Ether (TAME)mg/Kg wet0.0010 0.0200 2570-13093.4 3.880.0187
Benzene mg/Kg wet0.0020 0.0200 2570-13085.5 4.120.0171
Bromobenzene mg/Kg wet0.0020 0.0200 2570-13096.6 2.520.0193
Bromochloromethane mg/Kg wet0.0020 0.0200 2570-130109 2.620.0219
Bromodichloromethane mg/Kg wet0.0020 0.0200 2570-13088.3 0.4520.0177
Bromoform mg/Kg wet0.0020 0.0200 2570-130107 2.400.0214
Bromomethane mg/Kg wet0.010 0.0200 25 V-3440-13079.2 8.930.0158
2-Butanone (MEK)mg/Kg wet0.040 0.200 2570-16094.8 3.120.190
tert-Butyl Alcohol (TBA)mg/Kg wet0.040 0.200 2540-13092.0 0.2390.184
n-Butylbenzene mg/Kg wet0.0020 0.0200 2570-13080.2 0.2490.0160
sec-Butylbenzene mg/Kg wet0.0020 0.0200 2570-13093.2 2.330.0186
tert-Butylbenzene mg/Kg wet0.0020 0.0200 2570-16091.2 0.7650.0182
tert-Butyl Ethyl Ether (TBEE)mg/Kg wet0.0010 0.0200 2570-13093.1 0.8560.0186
Carbon Disulfide mg/Kg wet0.0060 0.200 2570-13084.0 4.110.168
Carbon Tetrachloride mg/Kg wet0.0020 0.0200 2570-13089.7 4.040.0179
Chlorobenzene mg/Kg wet0.0020 0.0200 2570-130102 1.270.0204
Chlorodibromomethane mg/Kg wet0.0010 0.0200 2570-130101 0.9820.0203
Chloroethane mg/Kg wet0.020 0.0200 25 J70-13085.9 6.090.0172
Chloroform mg/Kg wet0.0040 0.0200 2570-13086.2 2.070.0172
Chloromethane mg/Kg wet0.010 0.0200 25 V-0570-13074.5 2.910.0149
2-Chlorotoluene mg/Kg wet0.0020 0.0200 2570-13093.6 1.170.0187
4-Chlorotoluene mg/Kg wet0.0020 0.0200 2570-13088.7 1.340.0177
1,2-Dibromo-3-chloropropane (DBCP)mg/Kg wet0.0020 0.0200 2570-13099.1 3.390.0198
1,2-Dibromoethane (EDB)mg/Kg wet0.0010 0.0200 2570-130106 1.710.0212
Dibromomethane mg/Kg wet0.0020 0.0200 2570-130106 2.430.0212
1,2-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-13097.8 0.3060.0196
1,3-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-13095.1 0.4200.0190
1,4-Dichlorobenzene mg/Kg wet0.0020 0.0200 2570-13092.3 2.190.0185
trans-1,4-Dichloro-2-butene mg/Kg wet0.0040 0.0200 2570-13097.9 7.970.0196
Dichlorodifluoromethane (Freon 12)mg/Kg wet0.020 0.0200 25 J40-16073.7 8.070.0147
1,1-Dichloroethane mg/Kg wet0.0020 0.0200 2570-13089.7 2.530.0179
1,2-Dichloroethane mg/Kg wet0.0020 0.0200 2570-130102 1.180.0204
1,1-Dichloroethylene mg/Kg wet0.0040 0.0200 2570-13080.8 8.080.0162
cis-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 2570-13085.4 1.280.0171
trans-1,2-Dichloroethylene mg/Kg wet0.0020 0.0200 2570-13088.1 3.900.0176
1,2-Dichloropropane mg/Kg wet0.0020 0.0200 2570-13095.4 2.890.0191
1,3-Dichloropropane mg/Kg wet0.0010 0.0200 2570-13098.5 2.310.0197
2,2-Dichloropropane mg/Kg wet0.0020 0.0200 2570-13080.1 4.400.0160
1,1-Dichloropropene mg/Kg wet0.0020 0.0200 2570-13083.0 5.960.0166
cis-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 2570-13096.3 2.970.0193
trans-1,3-Dichloropropene mg/Kg wet0.0010 0.0200 2570-13097.5 3.970.0195
Diethyl Ether mg/Kg wet0.020 0.0200 25 J70-13092.0 2.750.0184
Page 44 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248105 - SW-846 5035
LCS Dup (B248105-BSD1) Prepared & Analyzed: 12/11/19
Diisopropyl Ether (DIPE)mg/Kg wet0.0010 0.0200 2570-13087.7 1.360.0175
1,4-Dioxane mg/Kg wet0.10 0.200 5040-16092.2 4.050.184
Ethylbenzene mg/Kg wet0.0020 0.0200 2570-13087.1 0.9230.0174
Hexachlorobutadiene mg/Kg wet0.0020 0.0200 2570-16095.8 5.580.0192
2-Hexanone (MBK)mg/Kg wet0.020 0.200 2570-16092.5 1.780.185
Isopropylbenzene (Cumene)mg/Kg wet0.0020 0.0200 2570-13095.3 5.410.0191
p-Isopropyltoluene (p-Cymene)mg/Kg wet0.0020 0.0200 2570-13090.2 0.3320.0180
Methyl tert-Butyl Ether (MTBE)mg/Kg wet0.0040 0.0200 2570-13093.7 0.7440.0187
Methylene Chloride mg/Kg wet0.020 0.0200 2540-160109 5.720.0217
4-Methyl-2-pentanone (MIBK)mg/Kg wet0.020 0.200 2570-16092.3 0.2390.185
Naphthalene mg/Kg wet0.0040 0.0200 2540-13087.2 1.930.0174
n-Propylbenzene mg/Kg wet0.0020 0.0200 2570-13085.8 4.220.0172
Styrene mg/Kg wet0.0020 0.0200 2570-13095.4 2.380.0191
1,1,1,2-Tetrachloroethane mg/Kg wet0.0020 0.0200 2570-130106 0.7570.0212
1,1,2,2-Tetrachloroethane mg/Kg wet0.0010 0.0200 2570-13098.3 1.330.0197
Tetrachloroethylene mg/Kg wet0.0020 0.0200 2570-13097.4 3.030.0195
Tetrahydrofuran mg/Kg wet0.010 0.0200 2570-13095.7 5.590.0191
Toluene mg/Kg wet0.0020 0.0200 2570-13089.2 2.870.0178
1,2,3-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-13093.5 3.980.0187
1,2,4-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-13090.3 3.910.0181
1,3,5-Trichlorobenzene mg/Kg wet0.0020 0.0200 2570-13094.5 2.250.0189
1,1,1-Trichloroethane mg/Kg wet0.0020 0.0200 2570-13084.1 2.350.0168
1,1,2-Trichloroethane mg/Kg wet0.0020 0.0200 2570-13098.4 3.100.0197
Trichloroethylene mg/Kg wet0.0020 0.0200 2570-13091.1 3.030.0182
Trichlorofluoromethane (Freon 11)mg/Kg wet0.010 0.0200 2570-13086.0 4.990.0172
1,2,3-Trichloropropane mg/Kg wet0.0020 0.0200 2570-130106 5.000.0213
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
mg/Kg wet0.010 0.0200 2570-13085.2 7.780.0170
1,2,4-Trimethylbenzene mg/Kg wet0.0020 0.0200 2570-13085.3 0.2350.0171
1,3,5-Trimethylbenzene mg/Kg wet0.0020 0.0200 2570-13089.5 4.260.0179
Vinyl Chloride mg/Kg wet0.010 0.0200 2540-13079.8 4.050.0160
m+p Xylene mg/Kg wet0.0040 0.0400 2570-13088.8 2.120.0355
o-Xylene mg/Kg wet0.0020 0.0200 2570-13088.9 3.100.0178
mg/Kg wet 0.0500 70-130Surrogate: 1,2-Dichloroethane-d4 91.40.0457
mg/Kg wet 0.0500 70-130Surrogate: Toluene-d8 98.80.0494
mg/Kg wet 0.0500 70-130Surrogate: 4-Bromofluorobenzene 1020.0511
Batch B248317 - SW-846 5030B
[TOC_3]B248317[TOC]
Blank (B248317-BLK1) Prepared: 12/13/19 Analyzed: 12/14/19
Acetone g/L50ND
Acrylonitrile g/L5.0ND
tert-Amyl Methyl Ether (TAME)g/L0.50 L-04, V-05ND
Benzene g/L1.0ND
Bromobenzene g/L1.0ND
Bromochloromethane g/L1.0ND
Bromodichloromethane g/L0.50ND
Bromoform g/L1.0ND
Bromomethane g/L2.0ND
2-Butanone (MEK)g/L20ND
tert-Butyl Alcohol (TBA)g/L20ND
n-Butylbenzene g/L1.0ND
sec-Butylbenzene g/L1.0ND
Page 45 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248317 - SW-846 5030B
Blank (B248317-BLK1) Prepared: 12/13/19 Analyzed: 12/14/19
tert-Butylbenzene g/L1.0ND
tert-Butyl Ethyl Ether (TBEE)g/L0.50 V-05ND
Carbon Disulfide g/L5.0ND
Carbon Tetrachloride g/L1.0ND
Chlorobenzene g/L1.0ND
Chlorodibromomethane g/L0.50ND
Chloroethane g/L2.0ND
Chloroform g/L2.0 J0.23
Chloromethane g/L2.0ND
2-Chlorotoluene g/L1.0ND
4-Chlorotoluene g/L1.0ND
1,2-Dibromo-3-chloropropane (DBCP)g/L5.0ND
1,2-Dibromoethane (EDB)g/L0.50ND
Dibromomethane g/L1.0ND
1,2-Dichlorobenzene g/L1.0ND
1,3-Dichlorobenzene g/L1.0ND
1,4-Dichlorobenzene g/L1.0ND
trans-1,4-Dichloro-2-butene g/L2.0ND
Dichlorodifluoromethane (Freon 12)g/L2.0ND
1,1-Dichloroethane g/L1.0ND
1,2-Dichloroethane g/L1.0ND
1,1-Dichloroethylene g/L1.0ND
cis-1,2-Dichloroethylene g/L1.0ND
trans-1,2-Dichloroethylene g/L1.0ND
1,2-Dichloropropane g/L1.0ND
1,3-Dichloropropane g/L0.50ND
2,2-Dichloropropane g/L1.0ND
1,1-Dichloropropene g/L2.0ND
cis-1,3-Dichloropropene g/L0.50ND
trans-1,3-Dichloropropene g/L0.50ND
Diethyl Ether g/L2.0ND
Diisopropyl Ether (DIPE)g/L0.50ND
1,4-Dioxane g/L50ND
Ethylbenzene g/L1.0ND
Hexachlorobutadiene g/L0.60ND
2-Hexanone (MBK)g/L10ND
Isopropylbenzene (Cumene)g/L1.0ND
p-Isopropyltoluene (p-Cymene)g/L1.0ND
Methyl tert-Butyl Ether (MTBE)g/L1.0ND
Methylene Chloride g/L5.0ND
4-Methyl-2-pentanone (MIBK)g/L10ND
Naphthalene g/L2.0ND
n-Propylbenzene g/L1.0ND
Styrene g/L1.0ND
1,1,1,2-Tetrachloroethane g/L1.0ND
1,1,2,2-Tetrachloroethane g/L0.50ND
Tetrachloroethylene g/L1.0ND
Tetrahydrofuran g/L10ND
Toluene g/L1.0ND
1,2,3-Trichlorobenzene g/L5.0 V-05ND
1,2,4-Trichlorobenzene g/L1.0ND
1,3,5-Trichlorobenzene g/L1.0ND
Page 46 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248317 - SW-846 5030B
Blank (B248317-BLK1) Prepared: 12/13/19 Analyzed: 12/14/19
1,1,1-Trichloroethane g/L1.0ND
1,1,2-Trichloroethane g/L1.0ND
Trichloroethylene g/L1.0ND
Trichlorofluoromethane (Freon 11)g/L2.0ND
1,2,3-Trichloropropane g/L2.0ND
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
g/L1.0ND
1,2,4-Trimethylbenzene g/L1.0ND
1,3,5-Trimethylbenzene g/L1.0ND
Vinyl Chloride g/L2.0ND
m+p Xylene g/L2.0ND
o-Xylene g/L1.0ND
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 98.724.7
g/L 25.0 70-130Surrogate: Toluene-d8 95.423.9
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 93.623.4
LCS (B248317-BS1) Prepared: 12/13/19 Analyzed: 12/14/19
Acetone g/L50 100 70-160126126
Acrylonitrile g/L5.0 10.0 70-13011011.0
tert-Amyl Methyl Ether (TAME)g/L0.50 10.0 V-05, L-0470-13065.1 *6.51
Benzene g/L1.0 10.0 70-13083.88.38
Bromobenzene g/L1.0 10.0 70-13096.89.68
Bromochloromethane g/L1.0 10.0 70-13097.09.70
Bromodichloromethane g/L0.50 10.0 70-13099.99.99
Bromoform g/L1.0 10.0 70-13010110.1
Bromomethane g/L2.0 10.0 40-16097.89.78
2-Butanone (MEK)g/L20 100 40-160109109
tert-Butyl Alcohol (TBA)g/L20 100 40-160110110
n-Butylbenzene g/L1.0 10.0 70-13010610.6
sec-Butylbenzene g/L1.0 10.0 70-13010510.5
tert-Butylbenzene g/L1.0 10.0 70-13010410.4
tert-Butyl Ethyl Ether (TBEE)g/L0.50 10.0 V-0570-13078.37.83
Carbon Disulfide g/L5.0 100 70-13093.793.7
Carbon Tetrachloride g/L1.0 10.0 70-13098.59.85
Chlorobenzene g/L1.0 10.0 70-13096.39.63
Chlorodibromomethane g/L0.50 10.0 70-13010010.0
Chloroethane g/L2.0 10.0 70-13088.58.85
Chloroform g/L2.0 10.0 70-13091.79.17
Chloromethane g/L2.0 10.0 40-16010210.2
2-Chlorotoluene g/L1.0 10.0 70-13097.09.70
4-Chlorotoluene g/L1.0 10.0 70-13010210.2
1,2-Dibromo-3-chloropropane (DBCP)g/L5.0 10.0 70-13010310.3
1,2-Dibromoethane (EDB)g/L0.50 10.0 70-13096.89.68
Dibromomethane g/L1.0 10.0 70-13094.19.41
1,2-Dichlorobenzene g/L1.0 10.0 70-13010110.1
1,3-Dichlorobenzene g/L1.0 10.0 70-13010310.3
1,4-Dichlorobenzene g/L1.0 10.0 70-13010110.1
trans-1,4-Dichloro-2-butene g/L2.0 10.0 V-2070-13013013.0
Dichlorodifluoromethane (Freon 12)g/L2.0 10.0 40-16077.77.77
1,1-Dichloroethane g/L1.0 10.0 70-13089.68.96
1,2-Dichloroethane g/L1.0 10.0 70-13010410.4
1,1-Dichloroethylene g/L1.0 10.0 70-13010210.2
cis-1,2-Dichloroethylene g/L1.0 10.0 70-13092.19.21
Page 47 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248317 - SW-846 5030B
LCS (B248317-BS1) Prepared: 12/13/19 Analyzed: 12/14/19
trans-1,2-Dichloroethylene g/L1.0 10.0 70-13093.19.31
1,2-Dichloropropane g/L1.0 10.0 70-13095.29.52
1,3-Dichloropropane g/L0.50 10.0 70-13097.99.79
2,2-Dichloropropane g/L1.0 10.0 40-13075.77.57
1,1-Dichloropropene g/L2.0 10.0 70-13093.19.31
cis-1,3-Dichloropropene g/L0.50 10.0 70-13098.19.81
trans-1,3-Dichloropropene g/L0.50 10.0 70-13096.09.60
Diethyl Ether g/L2.0 10.0 70-13095.89.58
Diisopropyl Ether (DIPE)g/L0.50 10.0 70-13010910.9
1,4-Dioxane g/L50 100 40-130101101
Ethylbenzene g/L1.0 10.0 70-13010210.2
Hexachlorobutadiene g/L0.60 10.0 70-13011011.0
2-Hexanone (MBK)g/L10 100 70-160128128
Isopropylbenzene (Cumene)g/L1.0 10.0 70-13010510.5
p-Isopropyltoluene (p-Cymene)g/L1.0 10.0 70-13099.09.90
Methyl tert-Butyl Ether (MTBE)g/L1.0 10.0 70-13085.78.57
Methylene Chloride g/L5.0 10.0 70-13099.99.99
4-Methyl-2-pentanone (MIBK)g/L10 100 70-160131131
Naphthalene g/L2.0 10.0 40-13010010.0
n-Propylbenzene g/L1.0 10.0 70-13010610.6
Styrene g/L1.0 10.0 70-13093.49.34
1,1,1,2-Tetrachloroethane g/L1.0 10.0 70-13010610.6
1,1,2,2-Tetrachloroethane g/L0.50 10.0 70-13010610.6
Tetrachloroethylene g/L1.0 10.0 70-13010210.2
Tetrahydrofuran g/L10 10.0 70-13010510.5
Toluene g/L1.0 10.0 70-13096.09.60
1,2,3-Trichlorobenzene g/L5.0 10.0 V-0570-13010110.1
1,2,4-Trichlorobenzene g/L1.0 10.0 70-13010310.3
1,3,5-Trichlorobenzene g/L1.0 10.0 70-13010210.2
1,1,1-Trichloroethane g/L1.0 10.0 70-13096.99.69
1,1,2-Trichloroethane g/L1.0 10.0 70-13094.49.44
Trichloroethylene g/L1.0 10.0 70-13098.79.87
Trichlorofluoromethane (Freon 11)g/L2.0 10.0 70-13010010.0
1,2,3-Trichloropropane g/L2.0 10.0 70-13011011.0
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
g/L1.0 10.0 70-13093.49.34
1,2,4-Trimethylbenzene g/L1.0 10.0 70-13096.49.64
1,3,5-Trimethylbenzene g/L1.0 10.0 70-13010210.2
Vinyl Chloride g/L2.0 10.0 V-20, L-0240-160331*33.1
m+p Xylene g/L2.0 20.0 70-13010320.5
o-Xylene g/L1.0 10.0 70-13010410.4
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10225.5
g/L 25.0 70-130Surrogate: Toluene-d8 98.724.7
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 96.124.0
Page 48 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248317 - SW-846 5030B
LCS Dup (B248317-BSD1) Prepared: 12/13/19 Analyzed: 12/14/19
Acetone g/L50 100 2570-160119 5.47119
Acrylonitrile g/L5.0 10.0 2570-130104 6.5410.4
tert-Amyl Methyl Ether (TAME)g/L0.50 10.0 25 L-04, V-0570-13060.1 7.99*6.01
Benzene g/L1.0 10.0 2570-13084.3 0.5958.43
Bromobenzene g/L1.0 10.0 2570-13096.6 0.2079.66
Bromochloromethane g/L1.0 10.0 2570-13099.2 2.249.92
Bromodichloromethane g/L0.50 10.0 2570-130102 1.6910.2
Bromoform g/L1.0 10.0 2570-13099.7 1.109.97
Bromomethane g/L2.0 10.0 2540-16097.3 0.5139.73
2-Butanone (MEK)g/L20 100 2540-160101 7.32101
tert-Butyl Alcohol (TBA)g/L20 100 2540-160106 4.43106
n-Butylbenzene g/L1.0 10.0 2570-130108 2.7110.8
sec-Butylbenzene g/L1.0 10.0 2570-130108 2.1610.8
tert-Butylbenzene g/L1.0 10.0 2570-130106 1.8110.6
tert-Butyl Ethyl Ether (TBEE)g/L0.50 10.0 25 V-0570-13071.7 8.807.17
Carbon Disulfide g/L5.0 100 2570-13095.4 1.7695.4
Carbon Tetrachloride g/L1.0 10.0 2570-13097.6 0.9189.76
Chlorobenzene g/L1.0 10.0 2570-13099.6 3.379.96
Chlorodibromomethane g/L0.50 10.0 2570-13099.6 0.6019.96
Chloroethane g/L2.0 10.0 2570-13090.5 2.239.05
Chloroform g/L2.0 10.0 2570-13090.3 1.549.03
Chloromethane g/L2.0 10.0 2540-160100 1.6810.0
2-Chlorotoluene g/L1.0 10.0 2570-13095.5 1.569.55
4-Chlorotoluene g/L1.0 10.0 2570-130101 0.78610.1
1,2-Dibromo-3-chloropropane (DBCP)g/L5.0 10.0 2570-13098.4 4.379.84
1,2-Dibromoethane (EDB)g/L0.50 10.0 2570-13094.9 1.989.49
Dibromomethane g/L1.0 10.0 2570-13090.6 3.799.06
1,2-Dichlorobenzene g/L1.0 10.0 2570-130102 1.3810.2
1,3-Dichlorobenzene g/L1.0 10.0 2570-130104 0.77110.4
1,4-Dichlorobenzene g/L1.0 10.0 2570-130103 1.9610.3
trans-1,4-Dichloro-2-butene g/L2.0 10.0 25 V-2070-130126 3.6812.6
Dichlorodifluoromethane (Freon 12)g/L2.0 10.0 2540-16076.6 1.437.66
1,1-Dichloroethane g/L1.0 10.0 2570-13090.1 0.5569.01
1,2-Dichloroethane g/L1.0 10.0 2570-130104 0.77010.4
1,1-Dichloroethylene g/L1.0 10.0 2570-130103 1.0710.3
cis-1,2-Dichloroethylene g/L1.0 10.0 2570-13093.1 1.089.31
trans-1,2-Dichloroethylene g/L1.0 10.0 2570-13094.8 1.819.48
1,2-Dichloropropane g/L1.0 10.0 2570-13096.0 0.8379.60
1,3-Dichloropropane g/L0.50 10.0 2570-13098.6 0.7129.86
2,2-Dichloropropane g/L1.0 10.0 2540-13077.3 2.097.73
1,1-Dichloropropene g/L2.0 10.0 2570-13094.1 1.079.41
cis-1,3-Dichloropropene g/L0.50 10.0 2570-13098.7 0.6109.87
trans-1,3-Dichloropropene g/L0.50 10.0 2570-13092.8 3.399.28
Diethyl Ether g/L2.0 10.0 2570-13095.0 0.8399.50
Diisopropyl Ether (DIPE)g/L0.50 10.0 2570-130108 1.1110.8
1,4-Dioxane g/L50 100 5040-130104 3.14104
Ethylbenzene g/L1.0 10.0 2570-130102 0.098310.2
Hexachlorobutadiene g/L0.60 10.0 2570-130120 8.4112.0
2-Hexanone (MBK)g/L10 100 2570-160118 7.94118
Isopropylbenzene (Cumene)g/L1.0 10.0 2570-130105 0.38110.5
p-Isopropyltoluene (p-Cymene)g/L1.0 10.0 2570-130102 2.7910.2
Methyl tert-Butyl Ether (MTBE)g/L1.0 10.0 2570-13079.9 7.007.99
Page 49 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248317 - SW-846 5030B
LCS Dup (B248317-BSD1) Prepared: 12/13/19 Analyzed: 12/14/19
Methylene Chloride g/L5.0 10.0 2570-13097.7 2.239.77
4-Methyl-2-pentanone (MIBK)g/L10 100 2570-160126 4.25126
Naphthalene g/L2.0 10.0 2540-130101 0.99310.1
n-Propylbenzene g/L1.0 10.0 2570-130103 2.3010.3
Styrene g/L1.0 10.0 2570-13094.3 0.9599.43
1,1,1,2-Tetrachloroethane g/L1.0 10.0 2570-130107 1.3210.7
1,1,2,2-Tetrachloroethane g/L0.50 10.0 2570-130102 3.8510.2
Tetrachloroethylene g/L1.0 10.0 2570-130103 0.68110.3
Tetrahydrofuran g/L10 10.0 2570-130106 1.2310.6
Toluene g/L1.0 10.0 2570-13095.6 0.4189.56
1,2,3-Trichlorobenzene g/L5.0 10.0 25 V-0570-130104 3.2110.4
1,2,4-Trichlorobenzene g/L1.0 10.0 2570-130106 3.2510.6
1,3,5-Trichlorobenzene g/L1.0 10.0 2570-130111 7.7011.1
1,1,1-Trichloroethane g/L1.0 10.0 2570-13094.8 2.199.48
1,1,2-Trichloroethane g/L1.0 10.0 2570-13094.4 0.009.44
Trichloroethylene g/L1.0 10.0 2570-13095.9 2.889.59
Trichlorofluoromethane (Freon 11)g/L2.0 10.0 2570-130102 2.1710.2
1,2,3-Trichloropropane g/L2.0 10.0 2570-130105 5.0210.5
1,1,2-Trichloro-1,2,2-trifluoroethane (Freon
113)
g/L1.0 10.0 2570-13095.4 2.129.54
1,2,4-Trimethylbenzene g/L1.0 10.0 2570-13096.8 0.4149.68
1,3,5-Trimethylbenzene g/L1.0 10.0 2570-130100 1.0910.0
Vinyl Chloride g/L2.0 10.0 25 L-02, V-2040-160322 2.73*32.2
m+p Xylene g/L2.0 20.0 2570-130101 1.4720.2
o-Xylene g/L1.0 10.0 2570-130102 1.7410.2
g/L 25.0 70-130Surrogate: 1,2-Dichloroethane-d4 10125.3
g/L 25.0 70-130Surrogate: Toluene-d8 98.024.5
g/L 25.0 70-130Surrogate: 4-Bromofluorobenzene 95.223.8
Page 50 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]Semivolatile Organic Compounds by GC/MS[TOC]
Batch B248288 - SW-846 3546
[TOC_3]B248288[TOC]
Blank (B248288-BLK1) Prepared: 12/13/19 Analyzed: 12/14/19
Acenaphthene mg/Kg wet0.17ND
Acenaphthylene mg/Kg wet0.17ND
Acetophenone mg/Kg wet0.34ND
Aniline mg/Kg wet0.34ND
Anthracene mg/Kg wet0.17ND
Benzidine mg/Kg wet0.66 V-05, V-35ND
Benzo(a)anthracene mg/Kg wet0.17ND
Benzo(a)pyrene mg/Kg wet0.17ND
Benzo(b)fluoranthene mg/Kg wet0.17ND
Benzo(g,h,i)perylene mg/Kg wet0.17ND
Benzo(k)fluoranthene mg/Kg wet0.17ND
Benzoic Acid mg/Kg wet1.0 V-34ND
Bis(2-chloroethoxy)methane mg/Kg wet0.34ND
Bis(2-chloroethyl)ether mg/Kg wet0.34ND
Bis(2-chloroisopropyl)ether mg/Kg wet0.34ND
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34ND
4-Bromophenylphenylether mg/Kg wet0.34ND
Butylbenzylphthalate mg/Kg wet0.34ND
Carbazole mg/Kg wet0.17ND
4-Chloroaniline mg/Kg wet0.66ND
4-Chloro-3-methylphenol mg/Kg wet0.66ND
2-Chloronaphthalene mg/Kg wet0.34ND
2-Chlorophenol mg/Kg wet0.34ND
4-Chlorophenylphenylether mg/Kg wet0.34ND
Chrysene mg/Kg wet0.17ND
Dibenz(a,h)anthracene mg/Kg wet0.17ND
Dibenzofuran mg/Kg wet0.34ND
Di-n-butylphthalate mg/Kg wet0.34ND
1,2-Dichlorobenzene mg/Kg wet0.34ND
1,3-Dichlorobenzene mg/Kg wet0.34ND
1,4-Dichlorobenzene mg/Kg wet0.34ND
3,3-Dichlorobenzidine mg/Kg wet0.17ND
2,4-Dichlorophenol mg/Kg wet0.34ND
Diethylphthalate mg/Kg wet0.34ND
2,4-Dimethylphenol mg/Kg wet0.34ND
Dimethylphthalate mg/Kg wet0.34ND
4,6-Dinitro-2-methylphenol mg/Kg wet0.34ND
2,4-Dinitrophenol mg/Kg wet0.66ND
2,4-Dinitrotoluene mg/Kg wet0.34ND
2,6-Dinitrotoluene mg/Kg wet0.34ND
Di-n-octylphthalate mg/Kg wet0.34ND
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34ND
Fluoranthene mg/Kg wet0.17ND
Fluorene mg/Kg wet0.17ND
Hexachlorobenzene mg/Kg wet0.34ND
Hexachlorobutadiene mg/Kg wet0.34ND
Hexachlorocyclopentadiene mg/Kg wet0.34ND
Hexachloroethane mg/Kg wet0.34ND
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17ND
Isophorone mg/Kg wet0.34ND
1-Methylnaphthalene mg/Kg wet0.17ND
2-Methylnaphthalene mg/Kg wet0.17ND
Page 51 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248288 - SW-846 3546
Blank (B248288-BLK1) Prepared: 12/13/19 Analyzed: 12/14/19
2-Methylphenol mg/Kg wet0.34ND
3/4-Methylphenol mg/Kg wet0.34ND
Naphthalene mg/Kg wet0.17ND
2-Nitroaniline mg/Kg wet0.34ND
3-Nitroaniline mg/Kg wet0.34ND
4-Nitroaniline mg/Kg wet0.34ND
Nitrobenzene mg/Kg wet0.34ND
2-Nitrophenol mg/Kg wet0.34ND
4-Nitrophenol mg/Kg wet0.66ND
N-Nitrosodimethylamine mg/Kg wet0.34ND
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34ND
N-Nitrosodi-n-propylamine mg/Kg wet0.34ND
Pentachloronitrobenzene mg/Kg wet0.34ND
Pentachlorophenol mg/Kg wet0.34ND
Phenanthrene mg/Kg wet0.17ND
Phenol mg/Kg wet0.34ND
Pyrene mg/Kg wet0.17ND
Pyridine mg/Kg wet0.34 V-05ND
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34ND
1,2,4-Trichlorobenzene mg/Kg wet0.34ND
2,4,5-Trichlorophenol mg/Kg wet0.34ND
2,4,6-Trichlorophenol mg/Kg wet0.34ND
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 73.64.91
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 73.14.87
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 68.42.28
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 94.83.16
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 90.56.03
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 79.82.66
LCS (B248288-BS1) Prepared: 12/13/19 Analyzed: 12/14/19
Acenaphthene mg/Kg wet0.17 1.67 40-14067.81.13
Acenaphthylene mg/Kg wet0.17 1.67 40-14072.41.21
Acetophenone mg/Kg wet0.34 1.67 40-14065.91.10
Aniline mg/Kg wet0.34 1.67 10-14053.60.893
Anthracene mg/Kg wet0.17 1.67 40-14073.11.22
Benzidine mg/Kg wet0.66 1.67 V-05, V-3540-14097.71.63
Benzo(a)anthracene mg/Kg wet0.17 1.67 40-14073.91.23
Benzo(a)pyrene mg/Kg wet0.17 1.67 40-14072.01.20
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 40-14071.11.18
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 40-14070.81.18
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 40-14073.91.23
Benzoic Acid mg/Kg wet1.0 1.67 V-3430-13061.71.03
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 40-14062.31.04
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 40-14060.11.00
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 40-14083.21.39
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 40-14066.91.12
4-Bromophenylphenylether mg/Kg wet0.34 1.67 40-14073.31.22
Butylbenzylphthalate mg/Kg wet0.34 1.67 40-14068.81.15
Carbazole mg/Kg wet0.17 1.67 40-14069.71.16
4-Chloroaniline mg/Kg wet0.66 1.67 10-14051.50.859
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 30-13078.51.31
2-Chloronaphthalene mg/Kg wet0.34 1.67 40-14061.81.03
Page 52 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248288 - SW-846 3546
LCS (B248288-BS1) Prepared: 12/13/19 Analyzed: 12/14/19
2-Chlorophenol mg/Kg wet0.34 1.67 30-13068.11.14
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 40-14075.51.26
Chrysene mg/Kg wet0.17 1.67 40-14072.61.21
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 40-14070.41.17
Dibenzofuran mg/Kg wet0.34 1.67 40-14076.61.28
Di-n-butylphthalate mg/Kg wet0.34 1.67 40-14070.11.17
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 40-14060.91.02
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 40-14058.10.968
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 40-14058.40.974
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 20-14072.81.21
2,4-Dichlorophenol mg/Kg wet0.34 1.67 30-13076.91.28
Diethylphthalate mg/Kg wet0.34 1.67 40-14073.01.22
2,4-Dimethylphenol mg/Kg wet0.34 1.67 30-13067.21.12
Dimethylphthalate mg/Kg wet0.34 1.67 40-14073.51.22
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 30-13060.21.00
2,4-Dinitrophenol mg/Kg wet0.66 1.67 30-13045.80.763
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 40-14071.81.20
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 40-14074.91.25
Di-n-octylphthalate mg/Kg wet0.34 1.67 40-14062.91.05
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34 1.67 40-14069.61.16
Fluoranthene mg/Kg wet0.17 1.67 40-14075.81.26
Fluorene mg/Kg wet0.17 1.67 40-14073.91.23
Hexachlorobenzene mg/Kg wet0.34 1.67 40-14077.11.28
Hexachlorobutadiene mg/Kg wet0.34 1.67 40-14070.31.17
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 40-14049.90.832
Hexachloroethane mg/Kg wet0.34 1.67 40-14055.40.923
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 40-14076.41.27
Isophorone mg/Kg wet0.34 1.67 40-14068.51.14
1-Methylnaphthalene mg/Kg wet0.17 1.67 40-14070.91.18
2-Methylnaphthalene mg/Kg wet0.17 1.67 40-14081.41.36
2-Methylphenol mg/Kg wet0.34 1.67 30-13065.41.09
3/4-Methylphenol mg/Kg wet0.34 1.67 30-13071.71.19
Naphthalene mg/Kg wet0.17 1.67 40-14067.21.12
2-Nitroaniline mg/Kg wet0.34 1.67 40-14077.41.29
3-Nitroaniline mg/Kg wet0.34 1.67 30-14063.11.05
4-Nitroaniline mg/Kg wet0.34 1.67 40-14071.21.19
Nitrobenzene mg/Kg wet0.34 1.67 40-14066.01.10
2-Nitrophenol mg/Kg wet0.34 1.67 30-13070.31.17
4-Nitrophenol mg/Kg wet0.66 1.67 30-13078.01.30
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 40-14074.81.25
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34 1.67 40-14075.21.25
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 40-14066.11.10
Pentachloronitrobenzene mg/Kg wet0.34 1.67 40-14077.51.29
Pentachlorophenol mg/Kg wet0.34 1.67 30-13054.40.907
Phenanthrene mg/Kg wet0.17 1.67 40-14074.01.23
Phenol mg/Kg wet0.34 1.67 30-13066.31.10
Pyrene mg/Kg wet0.17 1.67 40-14075.31.26
Pyridine mg/Kg wet0.34 1.67 V-0530-14032.70.545
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 40-14071.01.18
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 40-14069.21.15
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 30-13076.71.28
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 30-13075.81.26
Page 53 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248288 - SW-846 3546
LCS (B248288-BS1) Prepared: 12/13/19 Analyzed: 12/14/19
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 70.84.72
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 72.14.81
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 65.92.20
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 92.93.10
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 93.26.21
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 82.42.75
LCS Dup (B248288-BSD1) Prepared: 12/13/19 Analyzed: 12/14/19
Acenaphthene mg/Kg wet0.17 1.67 3040-14064.3 5.211.07
Acenaphthylene mg/Kg wet0.17 1.67 3040-14067.9 6.501.13
Acetophenone mg/Kg wet0.34 1.67 3040-14058.0 12.80.966
Aniline mg/Kg wet0.34 1.67 5010-14045.6 16.10.760
Anthracene mg/Kg wet0.17 1.67 3040-14069.1 5.661.15
Benzidine mg/Kg wet0.66 1.67 30 V-05, V-3540-140101 3.681.69
Benzo(a)anthracene mg/Kg wet0.17 1.67 3040-14068.3 7.841.14
Benzo(a)pyrene mg/Kg wet0.17 1.67 3040-14067.4 6.681.12
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 3040-14067.1 5.701.12
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 3040-14068.4 3.481.14
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 3040-14068.9 6.981.15
Benzoic Acid mg/Kg wet1.0 1.67 50 V-34, J30-13058.4 5.460.973
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 3040-14057.1 8.720.951
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 3040-14053.0 12.50.883
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 3040-14072.8 13.31.21
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 3040-14060.3 10.41.00
4-Bromophenylphenylether mg/Kg wet0.34 1.67 3040-14067.6 8.151.13
Butylbenzylphthalate mg/Kg wet0.34 1.67 3040-14062.9 8.991.05
Carbazole mg/Kg wet0.17 1.67 3040-14066.5 4.641.11
4-Chloroaniline mg/Kg wet0.66 1.67 3010-14051.6 0.07760.859
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 3030-13073.1 7.171.22
2-Chloronaphthalene mg/Kg wet0.34 1.67 3040-14058.6 5.350.976
2-Chlorophenol mg/Kg wet0.34 1.67 3030-13059.9 12.90.998
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 3040-14071.0 6.121.18
Chrysene mg/Kg wet0.17 1.67 3040-14067.9 6.691.13
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 3040-14069.6 1.141.16
Dibenzofuran mg/Kg wet0.34 1.67 3040-14071.8 6.391.20
Di-n-butylphthalate mg/Kg wet0.34 1.67 3040-14065.1 7.311.09
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14053.8 12.50.896
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14051.7 11.70.861
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14052.9 9.840.882
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 5020-14070.6 3.071.18
2,4-Dichlorophenol mg/Kg wet0.34 1.67 3030-13070.1 9.281.17
Diethylphthalate mg/Kg wet0.34 1.67 3040-14069.3 5.291.15
2,4-Dimethylphenol mg/Kg wet0.34 1.67 3030-13063.4 5.791.06
Dimethylphthalate mg/Kg wet0.34 1.67 3040-14068.5 6.981.14
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 3030-13057.2 5.110.953
2,4-Dinitrophenol mg/Kg wet0.66 1.67 3030-13045.3 1.100.754
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 3040-14068.3 4.941.14
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 3040-14069.9 6.911.16
Di-n-octylphthalate mg/Kg wet0.34 1.67 3040-14056.9 10.00.948
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34 1.67 3040-14064.4 7.701.07
Fluoranthene mg/Kg wet0.17 1.67 3040-14071.7 5.451.20
Fluorene mg/Kg wet0.17 1.67 3040-14069.6 6.051.16
Page 54 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248288 - SW-846 3546
LCS Dup (B248288-BSD1) Prepared: 12/13/19 Analyzed: 12/14/19
Hexachlorobenzene mg/Kg wet0.34 1.67 3040-14071.9 6.981.20
Hexachlorobutadiene mg/Kg wet0.34 1.67 3040-14061.1 14.01.02
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 3040-14042.7 15.50.712
Hexachloroethane mg/Kg wet0.34 1.67 3040-14050.3 9.580.838
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 3040-14071.6 6.461.19
Isophorone mg/Kg wet0.34 1.67 3040-14062.5 9.221.04
1-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14063.1 11.61.05
2-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14073.3 10.41.22
2-Methylphenol mg/Kg wet0.34 1.67 3030-13058.8 10.60.980
3/4-Methylphenol mg/Kg wet0.34 1.67 3030-13063.3 12.41.05
Naphthalene mg/Kg wet0.17 1.67 3040-14060.9 9.771.02
2-Nitroaniline mg/Kg wet0.34 1.67 3040-14074.8 3.471.25
3-Nitroaniline mg/Kg wet0.34 1.67 3030-14061.4 2.731.02
4-Nitroaniline mg/Kg wet0.34 1.67 3040-14069.9 1.731.17
Nitrobenzene mg/Kg wet0.34 1.67 3040-14058.8 11.50.980
2-Nitrophenol mg/Kg wet0.34 1.67 3030-13064.4 8.731.07
4-Nitrophenol mg/Kg wet0.66 1.67 5030-13076.3 2.181.27
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 3040-14069.2 7.801.15
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34 1.67 3040-14069.9 7.221.17
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 3040-14057.7 13.60.961
Pentachloronitrobenzene mg/Kg wet0.34 1.67 3040-14073.7 5.031.23
Pentachlorophenol mg/Kg wet0.34 1.67 3030-13048.0 12.60.800
Phenanthrene mg/Kg wet0.17 1.67 3040-14069.4 6.471.16
Phenol mg/Kg wet0.34 1.67 3030-13059.3 11.10.988
Pyrene mg/Kg wet0.17 1.67 3040-14068.8 9.051.15
Pyridine mg/Kg wet0.34 1.67 30 V-0530-14030.9 5.660.515
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 3040-14065.4 8.241.09
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 3040-14061.9 11.11.03
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 3030-13072.9 5.031.22
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 3030-13070.4 7.391.17
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 61.74.11
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 63.84.26
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 59.41.98
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 85.32.84
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 85.05.67
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 74.22.47
Matrix Spike (B248288-MS1) Prepared: 12/13/19 Analyzed: 12/16/19 Source: 19L0324-28
Acenaphthene mg/Kg dry0.21 2.08 40-14056.71.18 ND
Acenaphthylene mg/Kg dry0.21 2.08 40-14059.11.23 ND
Acetophenone mg/Kg dry0.42 2.08 40-14051.71.07 ND
Aniline mg/Kg dry0.42 2.08 MS-0940-14038.3 *0.797 ND
Anthracene mg/Kg dry0.21 2.08 40-14059.81.24 ND
Benzidine mg/Kg dry0.82 2.08 MS-09, V-05,
V-35, J
40-14017.8 *0.370 ND
Benzo(a)anthracene mg/Kg dry0.21 2.08 40-14061.41.28 ND
Benzo(a)pyrene mg/Kg dry0.21 2.08 40-14060.31.25 ND
Benzo(b)fluoranthene mg/Kg dry0.21 2.08 40-14059.21.23 ND
Benzo(g,h,i)perylene mg/Kg dry0.21 2.08 40-14055.41.15 ND
Benzo(k)fluoranthene mg/Kg dry0.21 2.08 40-14061.21.27 ND
Benzoic Acid mg/Kg dry1.2 2.08 MS-22, V-34, J40-14027.5 *0.572 ND
Bis(2-chloroethoxy)methane mg/Kg dry0.42 2.08 40-14048.31.00 ND
Bis(2-chloroethyl)ether mg/Kg dry0.42 2.08 40-14046.90.975 ND
Page 55 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248288 - SW-846 3546
Matrix Spike (B248288-MS1) Prepared: 12/13/19 Analyzed: 12/16/19 Source: 19L0324-28
Bis(2-chloroisopropyl)ether mg/Kg dry0.42 2.08 40-14065.41.36 ND
Bis(2-Ethylhexyl)phthalate mg/Kg dry0.42 2.08 40-14050.51.05 ND
4-Bromophenylphenylether mg/Kg dry0.42 2.08 40-14060.61.26 ND
Butylbenzylphthalate mg/Kg dry0.42 2.08 40-14053.51.11 ND
Carbazole mg/Kg dry0.21 2.08 40-14053.41.11 ND
4-Chloroaniline mg/Kg dry0.82 2.08 40-14047.10.979 ND
4-Chloro-3-methylphenol mg/Kg dry0.82 2.08 30-13059.91.25 ND
2-Chloronaphthalene mg/Kg dry0.42 2.08 40-14052.91.10 ND
2-Chlorophenol mg/Kg dry0.42 2.08 30-13053.91.12 ND
4-Chlorophenylphenylether mg/Kg dry0.42 2.08 40-14060.01.25 ND
Chrysene mg/Kg dry0.21 2.08 40-14061.21.27 ND
Dibenz(a,h)anthracene mg/Kg dry0.21 2.08 40-14053.21.11 ND
Dibenzofuran mg/Kg dry0.42 2.08 40-14062.21.29 ND
Di-n-butylphthalate mg/Kg dry0.42 2.08 40-14054.91.14 ND
1,2-Dichlorobenzene mg/Kg dry0.42 2.08 40-14047.00.978 ND
1,3-Dichlorobenzene mg/Kg dry0.42 2.08 40-14045.00.937 ND
1,4-Dichlorobenzene mg/Kg dry0.42 2.08 40-14045.50.946 ND
3,3-Dichlorobenzidine mg/Kg dry0.21 2.08 40-14066.91.39 ND
2,4-Dichlorophenol mg/Kg dry0.42 2.08 30-13060.01.25 ND
Diethylphthalate mg/Kg dry0.42 2.08 40-14056.81.18 ND
2,4-Dimethylphenol mg/Kg dry0.42 2.08 30-13055.21.15 ND
Dimethylphthalate mg/Kg dry0.42 2.08 40-14058.71.22 ND
4,6-Dinitro-2-methylphenol mg/Kg dry0.42 2.08 30-13042.30.881 ND
2,4-Dinitrophenol mg/Kg dry0.82 2.08 J30-13033.10.689 ND
2,4-Dinitrotoluene mg/Kg dry0.42 2.08 40-14056.71.18 ND
2,6-Dinitrotoluene mg/Kg dry0.42 2.08 40-14059.51.24 ND
Di-n-octylphthalate mg/Kg dry0.42 2.08 40-14048.31.00 ND
1,2-Diphenylhydrazine/Azobenzene mg/Kg dry0.42 2.08 40-14057.21.19 ND
Fluoranthene mg/Kg dry0.21 2.08 40-14064.01.33 ND
Fluorene mg/Kg dry0.21 2.08 40-14059.61.24 ND
Hexachlorobenzene mg/Kg dry0.42 2.08 40-14063.91.33 ND
Hexachlorobutadiene mg/Kg dry0.42 2.08 40-14053.91.12 ND
Hexachlorocyclopentadiene mg/Kg dry0.42 2.08 30-13033.30.693 ND
Hexachloroethane mg/Kg dry0.42 2.08 40-14042.60.886 ND
Indeno(1,2,3-cd)pyrene mg/Kg dry0.21 2.08 40-14060.11.25 ND
Isophorone mg/Kg dry0.42 2.08 40-14054.11.13 ND
1-Methylnaphthalene mg/Kg dry0.21 2.08 40-14055.81.16 ND
2-Methylnaphthalene mg/Kg dry0.21 2.08 40-14064.61.34 ND
2-Methylphenol mg/Kg dry0.42 2.08 30-13051.21.06 ND
3/4-Methylphenol mg/Kg dry0.42 2.08 30-13056.01.16 ND
Naphthalene mg/Kg dry0.21 2.08 40-14055.21.15 ND
2-Nitroaniline mg/Kg dry0.42 2.08 40-14064.61.34 ND
3-Nitroaniline mg/Kg dry0.42 2.08 40-14053.91.12 ND
4-Nitroaniline mg/Kg dry0.42 2.08 40-14051.11.06 ND
Nitrobenzene mg/Kg dry0.42 2.08 40-14052.01.08 ND
2-Nitrophenol mg/Kg dry0.42 2.08 30-13053.91.12 ND
4-Nitrophenol mg/Kg dry0.82 2.08 30-13059.41.24 ND
N-Nitrosodimethylamine mg/Kg dry0.42 2.08 40-14056.71.18 ND
N-Nitrosodiphenylamine/Diphenylamine mg/Kg dry0.42 2.08 40-14060.71.26 ND
N-Nitrosodi-n-propylamine mg/Kg dry0.42 2.08 40-14052.01.08 ND
Pentachloronitrobenzene mg/Kg dry0.42 2.08 40-14062.91.31 ND
Pentachlorophenol mg/Kg dry0.42 2.08 MS-2230-13024.8 *0.515 ND
Page 56 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248288 - SW-846 3546
Matrix Spike (B248288-MS1) Prepared: 12/13/19 Analyzed: 12/16/19 Source: 19L0324-28
Phenanthrene mg/Kg dry0.21 2.08 40-14062.81.31 ND
Phenol mg/Kg dry0.42 2.08 30-13053.01.10 ND
Pyrene mg/Kg dry0.21 2.08 40-14063.51.32 ND
Pyridine mg/Kg dry0.42 2.08 MS-09, V-0540-14023.2 *0.483 ND
1,2,4,5-Tetrachlorobenzene mg/Kg dry0.42 2.08 40-14059.41.24 ND
1,2,4-Trichlorobenzene mg/Kg dry0.42 2.08 40-14055.41.15 ND
2,4,5-Trichlorophenol mg/Kg dry0.42 2.08 30-13062.41.30 ND
2,4,6-Trichlorophenol mg/Kg dry0.42 2.08 30-13059.91.25 ND
mg/Kg dry 8.32 30-130Surrogate: 2-Fluorophenol 55.64.62
mg/Kg dry 8.32 30-130Surrogate: Phenol-d6 57.74.80
mg/Kg dry 4.16 30-130Surrogate: Nitrobenzene-d5 53.62.23
mg/Kg dry 4.16 30-130Surrogate: 2-Fluorobiphenyl 76.23.17
mg/Kg dry 8.32 30-130Surrogate: 2,4,6-Tribromophenol 68.85.72
mg/Kg dry 4.16 30-130Surrogate: p-Terphenyl-d14 65.02.71
Matrix Spike Dup (B248288-MSD1) Prepared: 12/13/19 Analyzed: 12/16/19 Source: 19L0324-28
Acenaphthene mg/Kg dry0.21 2.08 3040-14062.9 10.31.31 ND
Acenaphthylene mg/Kg dry0.21 2.08 3040-14066.6 12.01.39 ND
Acetophenone mg/Kg dry0.42 2.08 3040-14059.4 13.91.23 ND
Aniline mg/Kg dry0.42 2.08 30 MS-0940-14039.4 2.93*0.820 ND
Anthracene mg/Kg dry0.21 2.08 3040-14066.8 11.11.39 ND
Benzidine mg/Kg dry0.82 2.08 30 V-05, V-35,
MS-09, J
40-14022.0 21.0*0.457 ND
Benzo(a)anthracene mg/Kg dry0.21 2.08 3040-14068.8 11.41.43 ND
Benzo(a)pyrene mg/Kg dry0.21 2.08 3040-14068.2 12.31.42 ND
Benzo(b)fluoranthene mg/Kg dry0.21 2.08 3040-14065.4 9.951.36 ND
Benzo(g,h,i)perylene mg/Kg dry0.21 2.08 3040-14057.4 3.441.19 ND
Benzo(k)fluoranthene mg/Kg dry0.21 2.08 3040-14068.7 11.51.43 ND
Benzoic Acid mg/Kg dry1.2 2.08 30 V-34, J40-14040.70.847 ND
Bis(2-chloroethoxy)methane mg/Kg dry0.42 2.08 3040-14055.4 13.71.15 ND
Bis(2-chloroethyl)ether mg/Kg dry0.42 2.08 3040-14054.9 15.71.14 ND
Bis(2-chloroisopropyl)ether mg/Kg dry0.42 2.08 3040-14076.9 16.21.60 ND
Bis(2-Ethylhexyl)phthalate mg/Kg dry0.42 2.08 3040-14058.9 15.41.23 ND
4-Bromophenylphenylether mg/Kg dry0.42 2.08 3040-14067.9 11.31.41 ND
Butylbenzylphthalate mg/Kg dry0.42 2.08 3040-14064.4 18.61.34 ND
Carbazole mg/Kg dry0.21 2.08 3040-14061.7 14.41.28 ND
4-Chloroaniline mg/Kg dry0.82 2.08 3040-14044.9 4.700.934 ND
4-Chloro-3-methylphenol mg/Kg dry0.82 2.08 3030-13067.6 12.11.41 ND
2-Chloronaphthalene mg/Kg dry0.42 2.08 3040-14058.3 9.711.21 ND
2-Chlorophenol mg/Kg dry0.42 2.08 3030-13062.9 15.51.31 ND
4-Chlorophenylphenylether mg/Kg dry0.42 2.08 3040-14067.7 12.11.41 ND
Chrysene mg/Kg dry0.21 2.08 3040-14067.3 9.371.40 ND
Dibenz(a,h)anthracene mg/Kg dry0.21 2.08 3040-14061.9 15.21.29 ND
Dibenzofuran mg/Kg dry0.42 2.08 3040-14070.1 12.01.46 ND
Di-n-butylphthalate mg/Kg dry0.42 2.08 3040-14061.9 12.01.29 ND
1,2-Dichlorobenzene mg/Kg dry0.42 2.08 3040-14054.6 14.91.14 ND
1,3-Dichlorobenzene mg/Kg dry0.42 2.08 3040-14052.6 15.51.09 ND
1,4-Dichlorobenzene mg/Kg dry0.42 2.08 3040-14053.6 16.31.11 ND
3,3-Dichlorobenzidine mg/Kg dry0.21 2.08 3040-14069.3 3.561.44 ND
2,4-Dichlorophenol mg/Kg dry0.42 2.08 3030-13067.9 12.51.41 ND
Diethylphthalate mg/Kg dry0.42 2.08 3040-14063.7 11.41.32 ND
2,4-Dimethylphenol mg/Kg dry0.42 2.08 3030-13063.0 13.21.31 ND
Dimethylphthalate mg/Kg dry0.42 2.08 3040-14064.7 9.661.35 ND
Page 57 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248288 - SW-846 3546
Matrix Spike Dup (B248288-MSD1) Prepared: 12/13/19 Analyzed: 12/16/19 Source: 19L0324-28
4,6-Dinitro-2-methylphenol mg/Kg dry0.42 2.08 3030-13050.4 17.41.05 ND
2,4-Dinitrophenol mg/Kg dry0.82 2.08 30 J30-13037.6 12.70.782 ND
2,4-Dinitrotoluene mg/Kg dry0.42 2.08 3040-14063.2 10.91.31 ND
2,6-Dinitrotoluene mg/Kg dry0.42 2.08 3040-14067.2 12.21.40 ND
Di-n-octylphthalate mg/Kg dry0.42 2.08 3040-14057.0 16.51.18 ND
1,2-Diphenylhydrazine/Azobenzene mg/Kg dry0.42 2.08 3040-14065.7 13.91.37 ND
Fluoranthene mg/Kg dry0.21 2.08 3040-14070.9 10.31.48 ND
Fluorene mg/Kg dry0.21 2.08 3040-14066.3 10.61.38 ND
Hexachlorobenzene mg/Kg dry0.42 2.08 3040-14072.2 12.21.50 ND
Hexachlorobutadiene mg/Kg dry0.42 2.08 3040-14063.6 16.41.32 ND
Hexachlorocyclopentadiene mg/Kg dry0.42 2.08 3030-13042.2 23.50.877 ND
Hexachloroethane mg/Kg dry0.42 2.08 3040-14049.7 15.31.03 ND
Indeno(1,2,3-cd)pyrene mg/Kg dry0.21 2.08 3040-14064.1 6.341.33 ND
Isophorone mg/Kg dry0.42 2.08 3040-14061.5 12.81.28 ND
1-Methylnaphthalene mg/Kg dry0.21 2.08 3040-14063.1 12.31.31 ND
2-Methylnaphthalene mg/Kg dry0.21 2.08 3040-14073.5 12.91.53 ND
2-Methylphenol mg/Kg dry0.42 2.08 3030-13060.9 17.31.27 ND
3/4-Methylphenol mg/Kg dry0.42 2.08 3030-13063.1 12.01.31 ND
Naphthalene mg/Kg dry0.21 2.08 3040-14062.8 12.81.31 ND
2-Nitroaniline mg/Kg dry0.42 2.08 3040-14071.6 10.31.49 ND
3-Nitroaniline mg/Kg dry0.42 2.08 3040-14058.8 8.621.22 ND
4-Nitroaniline mg/Kg dry0.42 2.08 3040-14058.8 13.91.22 ND
Nitrobenzene mg/Kg dry0.42 2.08 3040-14059.9 14.01.25 ND
2-Nitrophenol mg/Kg dry0.42 2.08 3030-13062.4 14.71.30 ND
4-Nitrophenol mg/Kg dry0.82 2.08 3030-13069.8 16.11.45 ND
N-Nitrosodimethylamine mg/Kg dry0.42 2.08 3040-14068.5 18.91.43 ND
N-Nitrosodiphenylamine/Diphenylamine mg/Kg dry0.42 2.08 3040-14069.3 13.31.44 ND
N-Nitrosodi-n-propylamine mg/Kg dry0.42 2.08 3040-14059.5 13.51.24 ND
Pentachloronitrobenzene mg/Kg dry0.42 2.08 3040-14069.5 9.911.45 ND
Pentachlorophenol mg/Kg dry0.42 2.08 3030-13032.4 26.70.674 ND
Phenanthrene mg/Kg dry0.21 2.08 3040-14068.2 8.301.42 ND
Phenol mg/Kg dry0.42 2.08 3030-13061.5 14.81.28 ND
Pyrene mg/Kg dry0.21 2.08 3040-14069.0 8.301.43 ND
Pyridine mg/Kg dry0.42 2.08 30 V-05, MS-0940-14026.5 13.1*0.551 ND
1,2,4,5-Tetrachlorobenzene mg/Kg dry0.42 2.08 3040-14068.1 13.61.42 ND
1,2,4-Trichlorobenzene mg/Kg dry0.42 2.08 3040-14063.7 14.01.32 ND
2,4,5-Trichlorophenol mg/Kg dry0.42 2.08 3030-13068.9 9.871.43 ND
2,4,6-Trichlorophenol mg/Kg dry0.42 2.08 3030-13068.2 13.01.42 ND
mg/Kg dry 8.32 30-130Surrogate: 2-Fluorophenol 64.65.37
mg/Kg dry 8.32 30-130Surrogate: Phenol-d6 65.85.47
mg/Kg dry 4.16 30-130Surrogate: Nitrobenzene-d5 59.42.47
mg/Kg dry 4.16 30-130Surrogate: 2-Fluorobiphenyl 84.73.52
mg/Kg dry 8.32 30-130Surrogate: 2,4,6-Tribromophenol 76.96.39
mg/Kg dry 4.16 30-130Surrogate: p-Terphenyl-d14 72.33.01
Page 58 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248463 - SW-846 3546
[TOC_3]B248463[TOC]
Blank (B248463-BLK1) Prepared: 12/16/19 Analyzed: 12/18/19
Acenaphthene mg/Kg wet0.17ND
Acenaphthylene mg/Kg wet0.17ND
Acetophenone mg/Kg wet0.34ND
Aniline mg/Kg wet0.34ND
Anthracene mg/Kg wet0.17ND
Benzidine mg/Kg wet0.66 R-05, V-35ND
Benzo(a)anthracene mg/Kg wet0.17ND
Benzo(a)pyrene mg/Kg wet0.17ND
Benzo(b)fluoranthene mg/Kg wet0.17ND
Benzo(g,h,i)perylene mg/Kg wet0.17ND
Benzo(k)fluoranthene mg/Kg wet0.17ND
Benzoic Acid mg/Kg wet1.0 V-34ND
Bis(2-chloroethoxy)methane mg/Kg wet0.34ND
Bis(2-chloroethyl)ether mg/Kg wet0.34ND
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 V-20ND
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34ND
4-Bromophenylphenylether mg/Kg wet0.34ND
Butylbenzylphthalate mg/Kg wet0.34ND
Carbazole mg/Kg wet0.17ND
4-Chloroaniline mg/Kg wet0.66ND
4-Chloro-3-methylphenol mg/Kg wet0.66ND
2-Chloronaphthalene mg/Kg wet0.34ND
2-Chlorophenol mg/Kg wet0.34ND
4-Chlorophenylphenylether mg/Kg wet0.34ND
Chrysene mg/Kg wet0.17ND
Dibenz(a,h)anthracene mg/Kg wet0.17ND
Dibenzofuran mg/Kg wet0.34ND
Di-n-butylphthalate mg/Kg wet0.34ND
1,2-Dichlorobenzene mg/Kg wet0.34ND
1,3-Dichlorobenzene mg/Kg wet0.34ND
1,4-Dichlorobenzene mg/Kg wet0.34ND
3,3-Dichlorobenzidine mg/Kg wet0.17ND
2,4-Dichlorophenol mg/Kg wet0.34ND
Diethylphthalate mg/Kg wet0.34ND
2,4-Dimethylphenol mg/Kg wet0.34ND
Dimethylphthalate mg/Kg wet0.34ND
4,6-Dinitro-2-methylphenol mg/Kg wet0.34ND
2,4-Dinitrophenol mg/Kg wet0.66ND
2,4-Dinitrotoluene mg/Kg wet0.34ND
2,6-Dinitrotoluene mg/Kg wet0.34ND
Di-n-octylphthalate mg/Kg wet0.34ND
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34ND
Fluoranthene mg/Kg wet0.17ND
Fluorene mg/Kg wet0.17ND
Hexachlorobenzene mg/Kg wet0.34ND
Hexachlorobutadiene mg/Kg wet0.34ND
Hexachlorocyclopentadiene mg/Kg wet0.34ND
Hexachloroethane mg/Kg wet0.34ND
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17ND
Isophorone mg/Kg wet0.34ND
1-Methylnaphthalene mg/Kg wet0.17ND
2-Methylnaphthalene mg/Kg wet0.17ND
Page 59 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248463 - SW-846 3546
Blank (B248463-BLK1) Prepared: 12/16/19 Analyzed: 12/18/19
2-Methylphenol mg/Kg wet0.34ND
3/4-Methylphenol mg/Kg wet0.34ND
Naphthalene mg/Kg wet0.17ND
2-Nitroaniline mg/Kg wet0.34ND
3-Nitroaniline mg/Kg wet0.34ND
4-Nitroaniline mg/Kg wet0.34ND
Nitrobenzene mg/Kg wet0.34ND
2-Nitrophenol mg/Kg wet0.34ND
4-Nitrophenol mg/Kg wet0.66ND
N-Nitrosodimethylamine mg/Kg wet0.34 V-20ND
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34ND
N-Nitrosodi-n-propylamine mg/Kg wet0.34ND
Pentachloronitrobenzene mg/Kg wet0.34ND
Pentachlorophenol mg/Kg wet0.34ND
Phenanthrene mg/Kg wet0.17ND
Phenol mg/Kg wet0.34ND
Pyrene mg/Kg wet0.17ND
Pyridine mg/Kg wet0.34 L-04ND
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34ND
1,2,4-Trichlorobenzene mg/Kg wet0.34ND
2,4,5-Trichlorophenol mg/Kg wet0.34ND
2,4,6-Trichlorophenol mg/Kg wet0.34ND
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 64.74.31
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 64.54.30
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 62.42.08
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 82.82.76
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 75.15.01
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 77.12.57
LCS (B248463-BS1) Prepared: 12/16/19 Analyzed: 12/19/19
Acenaphthene mg/Kg wet0.17 1.67 40-14060.31.00
Acenaphthylene mg/Kg wet0.17 1.67 40-14060.11.00
Acetophenone mg/Kg wet0.34 1.67 40-14055.90.932
Aniline mg/Kg wet0.34 1.67 10-14051.60.861
Anthracene mg/Kg wet0.17 1.67 40-14063.41.06
Benzidine mg/Kg wet0.66 1.67 V-05, R-05, V-3540-14089.11.48
Benzo(a)anthracene mg/Kg wet0.17 1.67 40-14063.41.06
Benzo(a)pyrene mg/Kg wet0.17 1.67 40-14062.21.04
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 40-14062.91.05
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 40-14062.91.05
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 40-14063.41.06
Benzoic Acid mg/Kg wet1.0 1.67 V-34, J30-13050.20.836
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 40-14054.30.905
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 40-14052.80.880
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 40-14075.01.25
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 40-14059.70.995
4-Bromophenylphenylether mg/Kg wet0.34 1.67 40-14064.81.08
Butylbenzylphthalate mg/Kg wet0.34 1.67 40-14059.00.983
Carbazole mg/Kg wet0.17 1.67 40-14060.11.00
4-Chloroaniline mg/Kg wet0.66 1.67 10-14048.50.808
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 30-13068.41.14
2-Chloronaphthalene mg/Kg wet0.34 1.67 40-14054.50.908
Page 60 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248463 - SW-846 3546
LCS (B248463-BS1) Prepared: 12/16/19 Analyzed: 12/19/19
2-Chlorophenol mg/Kg wet0.34 1.67 30-13057.00.950
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 40-14064.41.07
Chrysene mg/Kg wet0.17 1.67 40-14062.51.04
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 40-14061.21.02
Dibenzofuran mg/Kg wet0.34 1.67 40-14065.31.09
Di-n-butylphthalate mg/Kg wet0.34 1.67 40-14062.11.04
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 40-14050.20.836
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 40-14048.30.805
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 40-14048.70.811
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 20-14067.81.13
2,4-Dichlorophenol mg/Kg wet0.34 1.67 30-13066.01.10
Diethylphthalate mg/Kg wet0.34 1.67 40-14061.51.02
2,4-Dimethylphenol mg/Kg wet0.34 1.67 30-13057.50.959
Dimethylphthalate mg/Kg wet0.34 1.67 40-14063.71.06
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 30-13058.20.970
2,4-Dinitrophenol mg/Kg wet0.66 1.67 30-13045.10.751
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 40-14060.51.01
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 40-14064.11.07
Di-n-octylphthalate mg/Kg wet0.34 1.67 40-14057.50.958
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34 1.67 40-14065.21.09
Fluoranthene mg/Kg wet0.17 1.67 40-14065.01.08
Fluorene mg/Kg wet0.17 1.67 40-14062.71.05
Hexachlorobenzene mg/Kg wet0.34 1.67 40-14066.21.10
Hexachlorobutadiene mg/Kg wet0.34 1.67 40-14057.90.965
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 40-14043.60.727
Hexachloroethane mg/Kg wet0.34 1.67 40-14047.60.794
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 40-14066.81.11
Isophorone mg/Kg wet0.34 1.67 40-14061.11.02
1-Methylnaphthalene mg/Kg wet0.17 1.67 40-14058.50.975
2-Methylnaphthalene mg/Kg wet0.17 1.67 40-14068.01.13
2-Methylphenol mg/Kg wet0.34 1.67 30-13058.00.966
3/4-Methylphenol mg/Kg wet0.34 1.67 30-13062.51.04
Naphthalene mg/Kg wet0.17 1.67 40-14056.40.940
2-Nitroaniline mg/Kg wet0.34 1.67 40-14070.01.17
3-Nitroaniline mg/Kg wet0.34 1.67 30-14055.50.925
4-Nitroaniline mg/Kg wet0.34 1.67 40-14061.31.02
Nitrobenzene mg/Kg wet0.34 1.67 40-14058.20.971
2-Nitrophenol mg/Kg wet0.34 1.67 30-13058.80.979
4-Nitrophenol mg/Kg wet0.66 1.67 30-13070.61.18
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 V-0640-14067.21.12
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34 1.67 40-14065.81.10
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 40-14060.11.00
Pentachloronitrobenzene mg/Kg wet0.34 1.67 40-14067.21.12
Pentachlorophenol mg/Kg wet0.34 1.67 30-13053.20.886
Phenanthrene mg/Kg wet0.17 1.67 40-14064.61.08
Phenol mg/Kg wet0.34 1.67 30-13059.10.985
Pyrene mg/Kg wet0.17 1.67 40-14062.81.05
Pyridine mg/Kg wet0.34 1.67 L-0430-14029.4 *0.490
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 40-14060.41.01
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 40-14056.80.947
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 30-13064.51.07
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 30-13063.01.05
Page 61 of 81
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248463 - SW-846 3546
LCS (B248463-BS1) Prepared: 12/16/19 Analyzed: 12/19/19
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 61.04.07
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 63.84.25
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 57.61.92
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 80.42.68
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 80.95.40
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 71.02.37
LCS Dup (B248463-BSD1) Prepared: 12/16/19 Analyzed: 12/19/19
Acenaphthene mg/Kg wet0.17 1.67 3040-14049.2 20.20.821
Acenaphthylene mg/Kg wet0.17 1.67 3040-14049.2 19.90.820
Acetophenone mg/Kg wet0.34 1.67 3040-14046.3 18.90.771
Aniline mg/Kg wet0.34 1.67 5010-14037.0 33.00.617
Anthracene mg/Kg wet0.17 1.67 3040-14052.6 18.60.877
Benzidine mg/Kg wet0.66 1.67 30 R-05, V-05, V-3540-14053.2 50.4 *0.887
Benzo(a)anthracene mg/Kg wet0.17 1.67 3040-14052.4 19.10.873
Benzo(a)pyrene mg/Kg wet0.17 1.67 3040-14051.0 19.80.849
Benzo(b)fluoranthene mg/Kg wet0.17 1.67 3040-14052.2 18.50.871
Benzo(g,h,i)perylene mg/Kg wet0.17 1.67 3040-14051.1 20.70.852
Benzo(k)fluoranthene mg/Kg wet0.17 1.67 3040-14053.1 17.60.885
Benzoic Acid mg/Kg wet1.0 1.67 50 V-34, J30-13044.3 12.50.738
Bis(2-chloroethoxy)methane mg/Kg wet0.34 1.67 3040-14044.6 19.70.743
Bis(2-chloroethyl)ether mg/Kg wet0.34 1.67 3040-14043.6 19.20.726
Bis(2-chloroisopropyl)ether mg/Kg wet0.34 1.67 3040-14062.2 18.71.04
Bis(2-Ethylhexyl)phthalate mg/Kg wet0.34 1.67 3040-14048.4 21.00.806
4-Bromophenylphenylether mg/Kg wet0.34 1.67 3040-14053.2 19.80.886
Butylbenzylphthalate mg/Kg wet0.34 1.67 3040-14048.5 19.50.808
Carbazole mg/Kg wet0.17 1.67 3040-14049.9 18.50.832
4-Chloroaniline mg/Kg wet0.66 1.67 30 J10-14036.6 27.90.611
4-Chloro-3-methylphenol mg/Kg wet0.66 1.67 3030-13055.6 20.70.927
2-Chloronaphthalene mg/Kg wet0.34 1.67 3040-14045.8 17.20.764
2-Chlorophenol mg/Kg wet0.34 1.67 3030-13047.4 18.40.789
4-Chlorophenylphenylether mg/Kg wet0.34 1.67 3040-14053.3 18.90.888
Chrysene mg/Kg wet0.17 1.67 3040-14052.0 18.30.867
Dibenz(a,h)anthracene mg/Kg wet0.17 1.67 3040-14053.7 13.00.896
Dibenzofuran mg/Kg wet0.34 1.67 3040-14053.2 20.50.886
Di-n-butylphthalate mg/Kg wet0.34 1.67 3040-14051.3 19.10.855
1,2-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14042.4 16.90.706
1,3-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14040.5 17.60.675
1,4-Dichlorobenzene mg/Kg wet0.34 1.67 3040-14041.4 16.10.690
3,3-Dichlorobenzidine mg/Kg wet0.17 1.67 5020-14053.7 23.30.894
2,4-Dichlorophenol mg/Kg wet0.34 1.67 3030-13053.7 20.50.895
Diethylphthalate mg/Kg wet0.34 1.67 3040-14051.5 17.60.859
2,4-Dimethylphenol mg/Kg wet0.34 1.67 3030-13043.3 28.30.721
Dimethylphthalate mg/Kg wet0.34 1.67 3040-14051.1 21.90.852
4,6-Dinitro-2-methylphenol mg/Kg wet0.34 1.67 3030-13047.9 19.40.798
2,4-Dinitrophenol mg/Kg wet0.66 1.67 3030-13041.3 8.750.688
2,4-Dinitrotoluene mg/Kg wet0.34 1.67 3040-14050.3 18.50.838
2,6-Dinitrotoluene mg/Kg wet0.34 1.67 3040-14052.3 20.30.871
Di-n-octylphthalate mg/Kg wet0.34 1.67 3040-14046.8 20.50.780
1,2-Diphenylhydrazine/Azobenzene mg/Kg wet0.34 1.67 3040-14053.9 19.00.899
Fluoranthene mg/Kg wet0.17 1.67 3040-14054.4 17.90.906
Fluorene mg/Kg wet0.17 1.67 3040-14050.6 21.40.843
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B248463 - SW-846 3546
LCS Dup (B248463-BSD1) Prepared: 12/16/19 Analyzed: 12/19/19
Hexachlorobenzene mg/Kg wet0.34 1.67 3040-14055.4 17.80.923
Hexachlorobutadiene mg/Kg wet0.34 1.67 3040-14048.4 17.90.806
Hexachlorocyclopentadiene mg/Kg wet0.34 1.67 30 L-0740-14034.6 22.9*0.577
Hexachloroethane mg/Kg wet0.34 1.67 30 L-0740-14039.6 18.5*0.659
Indeno(1,2,3-cd)pyrene mg/Kg wet0.17 1.67 3040-14054.9 19.60.915
Isophorone mg/Kg wet0.34 1.67 3040-14049.7 20.60.828
1-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14048.2 19.30.803
2-Methylnaphthalene mg/Kg wet0.17 1.67 3040-14056.2 19.00.937
2-Methylphenol mg/Kg wet0.34 1.67 3030-13046.6 21.80.776
3/4-Methylphenol mg/Kg wet0.34 1.67 3030-13049.9 22.30.832
Naphthalene mg/Kg wet0.17 1.67 3040-14047.2 17.90.786
2-Nitroaniline mg/Kg wet0.34 1.67 3040-14057.4 19.80.956
3-Nitroaniline mg/Kg wet0.34 1.67 3030-14045.6 19.60.760
4-Nitroaniline mg/Kg wet0.34 1.67 3040-14050.1 20.00.836
Nitrobenzene mg/Kg wet0.34 1.67 3040-14048.0 19.40.799
2-Nitrophenol mg/Kg wet0.34 1.67 3030-13048.3 19.50.805
4-Nitrophenol mg/Kg wet0.66 1.67 5030-13058.8 18.20.980
N-Nitrosodimethylamine mg/Kg wet0.34 1.67 30 V-0640-14056.2 17.80.936
N-Nitrosodiphenylamine/Diphenylamine mg/Kg wet0.34 1.67 3040-14054.8 18.10.914
N-Nitrosodi-n-propylamine mg/Kg wet0.34 1.67 3040-14049.7 19.00.828
Pentachloronitrobenzene mg/Kg wet0.34 1.67 3040-14055.6 18.90.927
Pentachlorophenol mg/Kg wet0.34 1.67 3030-13042.7 22.00.711
Phenanthrene mg/Kg wet0.17 1.67 3040-14053.8 18.30.897
Phenol mg/Kg wet0.34 1.67 3030-13047.6 21.60.793
Pyrene mg/Kg wet0.17 1.67 3040-14051.7 19.40.862
Pyridine mg/Kg wet0.34 1.67 30 L-0430-14023.5 22.4*0.391
1,2,4,5-Tetrachlorobenzene mg/Kg wet0.34 1.67 3040-14050.3 18.20.839
1,2,4-Trichlorobenzene mg/Kg wet0.34 1.67 3040-14048.4 16.10.806
2,4,5-Trichlorophenol mg/Kg wet0.34 1.67 3030-13053.8 18.10.896
2,4,6-Trichlorophenol mg/Kg wet0.34 1.67 3030-13051.6 19.80.861
mg/Kg wet 6.67 30-130Surrogate: 2-Fluorophenol 49.73.31
mg/Kg wet 6.67 30-130Surrogate: Phenol-d6 51.03.40
mg/Kg wet 3.33 30-130Surrogate: Nitrobenzene-d5 47.61.59
mg/Kg wet 3.33 30-130Surrogate: 2-Fluorobiphenyl 64.12.14
mg/Kg wet 6.67 30-130Surrogate: 2,4,6-Tribromophenol 64.54.30
mg/Kg wet 3.33 30-130Surrogate: p-Terphenyl-d14 57.01.90
Page 63 of 81
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Metals Analyses (Total) - Quality Control
QUALITY CONTROL
[TOC_2]Metals Analyses (Total)[TOC]
Batch B248355 - SW-846 7471
[TOC_3]B248355[TOC]
Blank (B248355-BLK1) Prepared: 12/13/19 Analyzed: 12/14/19
Mercury mg/Kg wet0.025ND
LCS (B248355-BS1) Prepared: 12/13/19 Analyzed: 12/14/19
Mercury mg/Kg wet0.39 7.61 72.7-127.31259.50
LCS Dup (B248355-BSD1) Prepared: 12/13/19 Analyzed: 12/14/19
Mercury mg/Kg wet0.39 7.61 2072.7-127.3120 3.839.14
Batch B248457 - SW-846 7471
[TOC_3]B248457[TOC]
Blank (B248457-BLK1) Prepared: 12/16/19 Analyzed: 12/17/19
Mercury mg/Kg wet0.025ND
LCS (B248457-BS1) Prepared: 12/16/19 Analyzed: 12/17/19
Mercury mg/Kg wet0.39 7.61 72.7-127.385.66.51
LCS Dup (B248457-BSD1) Prepared: 12/16/19 Analyzed: 12/17/19
Mercury mg/Kg wet0.38 7.61 2072.7-127.375.5 12.55.75
Batch B248472 - SW-846 3050B
[TOC_3]B248472[TOC]
Blank (B248472-BLK1) Prepared: 12/17/19 Analyzed: 12/18/19
Arsenic mg/Kg wet0.17ND
Chromium mg/Kg wet4.2ND
Lead mg/Kg wet1.7ND
Selenium mg/Kg wet1.3ND
Silver mg/Kg wet0.083ND
Barium mg/Kg wet8.3ND
Cadmium mg/Kg wet0.33ND
LCS (B248472-BS1) Prepared: 12/17/19 Analyzed: 12/18/19
Arsenic mg/Kg wet2.0 143 83.2-117.5106152
Chromium mg/Kg wet49 101 82.4-116.8100101
Lead mg/Kg wet20 125 82.4-116.8103129
Selenium mg/Kg wet16 77.9 79.3-120.710884.4
Silver mg/Kg wet0.98 34.3 81-119.210234.9
Barium mg/Kg wet98 415 82.7-117.6100415
Cadmium mg/Kg wet3.9 56.2 82.9-117.310257.3
LCS Dup (B248472-BSD1) Prepared: 12/17/19 Analyzed: 12/18/19
Arsenic mg/Kg wet2.0 143 3083.2-117.5113 5.94161
Chromium mg/Kg wet49 101 3082.4-116.8105 4.69106
Lead mg/Kg wet20 125 3082.4-116.8110 6.51137
Selenium mg/Kg wet16 77.9 3079.3-120.7112 3.4887.3
Silver mg/Kg wet0.99 34.3 3081-119.2110 7.2637.6
Barium mg/Kg wet99 415 2082.7-117.6107 6.57444
Cadmium mg/Kg wet3.9 56.2 2082.9-117.3101 0.85656.8
Page 64 of 81
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Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) - Quality Control
QUALITY CONTROL
[TOC_2]Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)[TOC]
Batch B248245 - % Solids
[TOC_3]B248245[TOC]
Duplicate (B248245-DUP1) Prepared & Analyzed: 12/12/19 Source: 19L0324-28
% Solids % Wt 201.3879.0 80.1
Page 65 of 81
Table of Contents
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FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits.
Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is
on the high side.
L-02
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits.
Reported value for this compound is likely to be biased on the low side.
L-04
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits. RPD between the two LFB/LCS results is within method specified criteria.
L-07
Matrix spike recovery and/or matrix spike duplicate recovery outside of control limits. Possibility of sample
matrix effects that lead to a low bias for reported result or non-homogeneous sample aliquots cannot be
eliminated.
MS-09
Either matrix spike or MS duplicate is outside of control limits, but the other is within limits. RPD between the
two MS/MSD results is within method specified criteria.
MS-22
Laboratory fortified blank duplicate RPD is outside of control limits. Reduced precision is anticipated for any
reported value for this compound.
R-05
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for
this compound.
V-05
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side for
this compound.
V-06
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side.
Data validation is not affected since sample result was "not detected" for this compound.
V-20
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound. Reported result is estimated.
V-34
Initial calibration verification (ICV) did not meet method specifications and was biased on the high side for this
compound. Reported result is estimated.
V-35
[TOC_1]Flag/Qualifier Summary[TOC]
Page 66 of 81
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 6020B in Soil
NY,VA,NH,NC,MEArsenic
NY,NC,MEChromium
NY,NC,MELead
NY,VA,NH,NC,MESelenium
NY,NC,MESilver
NY,NCBarium
NY,NC,MECadmium
SW-846 7471B in Soil
CT,NH,NY,NC,ME,VAMercury
SW-846 8260D in Soil
NCAcetone
NCAcrylonitrile
NCtert-Amyl Methyl Ether (TAME)
NCBenzene
NCBromobenzene
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCtert-Butyl Alcohol (TBA)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCtert-Butyl Ethyl Ether (TBEE)
NCCarbon Disulfide
NCCarbon Tetrachloride
NCChlorobenzene
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromo-3-chloropropane (DBCP)
NC1,2-Dibromoethane (EDB)
NCDibromomethane
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCtrans-1,4-Dichloro-2-butene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
[TOC_1]Certifications[TOC]
Page 67 of 81
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8260D in Soil
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiethyl Ether
NCDiisopropyl Ether (DIPE)
NC1,4-Dioxane
NCEthylbenzene
NCHexachlorobutadiene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
NC1,1,1,2-Tetrachloroethane
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCTetrahydrofuran
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,3,5-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
SW-846 8260D in Water
NCAcetone
NCAcrylonitrile
NCtert-Amyl Methyl Ether (TAME)
NCBenzene
NCBromobenzene
Page 68 of 81
Table of Contents
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8260D in Water
NCBromochloromethane
NCBromodichloromethane
NCBromoform
NCBromomethane
NC2-Butanone (MEK)
NCtert-Butyl Alcohol (TBA)
NCn-Butylbenzene
NCsec-Butylbenzene
NCtert-Butylbenzene
NCtert-Butyl Ethyl Ether (TBEE)
NCCarbon Disulfide
NCCarbon Tetrachloride
NCChlorobenzene
NCChlorodibromomethane
NCChloroethane
NCChloroform
NCChloromethane
NC2-Chlorotoluene
NC4-Chlorotoluene
NC1,2-Dibromo-3-chloropropane (DBCP)
NC1,2-Dibromoethane (EDB)
NCDibromomethane
NC1,2-Dichlorobenzene
NC1,3-Dichlorobenzene
NC1,4-Dichlorobenzene
NCtrans-1,4-Dichloro-2-butene
NCDichlorodifluoromethane (Freon 12)
NC1,1-Dichloroethane
NC1,2-Dichloroethane
NC1,1-Dichloroethylene
NCcis-1,2-Dichloroethylene
NCtrans-1,2-Dichloroethylene
NC1,2-Dichloropropane
NC1,3-Dichloropropane
NC2,2-Dichloropropane
NC1,1-Dichloropropene
NCcis-1,3-Dichloropropene
NCtrans-1,3-Dichloropropene
NCDiethyl Ether
NCDiisopropyl Ether (DIPE)
NC1,4-Dioxane
NCEthylbenzene
NCHexachlorobutadiene
NC2-Hexanone (MBK)
NCIsopropylbenzene (Cumene)
NCp-Isopropyltoluene (p-Cymene)
NCMethyl tert-Butyl Ether (MTBE)
Page 69 of 81
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8260D in Water
NCMethylene Chloride
NC4-Methyl-2-pentanone (MIBK)
NCNaphthalene
NCn-Propylbenzene
NCStyrene
NC1,1,1,2-Tetrachloroethane
NC1,1,2,2-Tetrachloroethane
NCTetrachloroethylene
NCTetrahydrofuran
NCToluene
NC1,2,3-Trichlorobenzene
NC1,2,4-Trichlorobenzene
NC1,3,5-Trichlorobenzene
NC1,1,1-Trichloroethane
NC1,1,2-Trichloroethane
NCTrichloroethylene
NCTrichlorofluoromethane (Freon 11)
NC1,2,3-Trichloropropane
NC1,1,2-Trichloro-1,2,2-trifluoroethane (Freon 113)
NC1,2,4-Trimethylbenzene
NC1,3,5-Trimethylbenzene
NCVinyl Chloride
NCm+p Xylene
NCo-Xylene
SW-846 8270E in Soil
CT,NY,NH,ME,NC,VAAcenaphthene
CT,NY,NH,ME,NC,VAAcenaphthylene
NY,NH,ME,NC,VAAcetophenone
NY,NH,ME,NC,VAAniline
CT,NY,NH,ME,NC,VAAnthracene
CT,NY,NH,ME,NC,VABenzidine
CT,NY,NH,ME,NC,VABenzo(a)anthracene
CT,NY,NH,ME,NC,VABenzo(a)pyrene
CT,NY,NH,ME,NC,VABenzo(b)fluoranthene
CT,NY,NH,ME,NC,VABenzo(g,h,i)perylene
CT,NY,NH,ME,NC,VABenzo(k)fluoranthene
NY,NH,ME,NC,VABenzoic Acid
CT,NY,NH,ME,NC,VABis(2-chloroethoxy)methane
CT,NY,NH,ME,NC,VABis(2-chloroethyl)ether
CT,NY,NH,ME,NC,VABis(2-chloroisopropyl)ether
CT,NY,NH,ME,NC,VABis(2-Ethylhexyl)phthalate
CT,NY,NH,ME,NC,VA4-Bromophenylphenylether
CT,NY,NH,ME,NC,VAButylbenzylphthalate
NCCarbazole
CT,NY,NH,ME,NC,VA4-Chloroaniline
CT,NY,NH,ME,NC,VA4-Chloro-3-methylphenol
Page 70 of 81
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CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270E in Soil
CT,NY,NH,NC,VA2-Chloronaphthalene
CT,NY,NH,ME,NC,VA2-Chlorophenol
CT,NY,NH,ME,NC,VA4-Chlorophenylphenylether
CT,NY,NH,ME,NC,VAChrysene
CT,NY,NH,ME,NC,VADibenz(a,h)anthracene
CT,NY,NH,ME,NC,VADibenzofuran
CT,NY,NH,ME,NC,VADi-n-butylphthalate
NY,NH,ME,NC,VA1,2-Dichlorobenzene
NY,NH,ME,NC,VA1,3-Dichlorobenzene
NY,NH,ME,NC,VA1,4-Dichlorobenzene
CT,NY,NH,ME,NC,VA3,3-Dichlorobenzidine
CT,NY,NH,ME,NC,VA2,4-Dichlorophenol
CT,NY,NH,ME,NC,VADiethylphthalate
CT,NY,NH,ME,NC,VA2,4-Dimethylphenol
CT,NY,NH,ME,NC,VADimethylphthalate
CT,NY,NH,ME,NC,VA4,6-Dinitro-2-methylphenol
CT,NY,NH,ME,NC,VA2,4-Dinitrophenol
CT,NY,NH,ME,NC,VA2,4-Dinitrotoluene
CT,NY,NH,ME,NC,VA2,6-Dinitrotoluene
CT,NY,NH,ME,NC,VADi-n-octylphthalate
NY,NH,ME,NC,VA1,2-Diphenylhydrazine/Azobenzene
CT,NY,NH,ME,NC,VAFluoranthene
NY,NH,ME,NC,VAFluorene
CT,NY,NH,ME,NC,VAHexachlorobenzene
CT,NY,NH,ME,NC,VAHexachlorobutadiene
CT,NY,NH,ME,NC,VAHexachlorocyclopentadiene
CT,NY,NH,ME,NC,VAHexachloroethane
CT,NY,NH,ME,NC,VAIndeno(1,2,3-cd)pyrene
CT,NY,NH,ME,NC,VAIsophorone
NC1-Methylnaphthalene
CT,NY,NH,ME,NC,VA2-Methylnaphthalene
CT,NY,NH,ME,NC,VA2-Methylphenol
CT,NY,NH,ME,NC,VA3/4-Methylphenol
CT,NY,NH,ME,NC,VANaphthalene
CT,NY,NH,ME,NC,VA2-Nitroaniline
CT,NY,NH,ME,NC,VA3-Nitroaniline
CT,NY,NH,ME,NC,VA4-Nitroaniline
CT,NY,NH,ME,NC,VANitrobenzene
CT,NY,NH,ME,NC,VA2-Nitrophenol
CT,NY,NH,ME,NC,VA4-Nitrophenol
CT,NY,NH,ME,NC,VAN-Nitrosodimethylamine
CT,NY,NH,ME,NC,VAN-Nitrosodi-n-propylamine
NY,NCPentachloronitrobenzene
CT,NY,NH,ME,NC,VAPentachlorophenol
CT,NY,NH,ME,NC,VAPhenanthrene
CT,NY,NH,ME,NC,VAPhenol
CT,NY,NH,ME,NC,VAPyrene
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270E in Soil
CT,NY,NH,ME,NC,VAPyridine
NY,NC1,2,4,5-Tetrachlorobenzene
CT,NY,NH,ME,NC,VA1,2,4-Trichlorobenzene
CT,NY,NH,ME,NC,VA2,4,5-Trichlorophenol
CT,NY,NH,ME,NC,VA2,4,6-Trichlorophenol
NC2-Fluorophenol
SW-846 8270E in Water
CT,NY,NC,ME,NH,VAAcenaphthene
CT,NY,NC,ME,NH,VAAcenaphthylene
NY,NCAcetophenone
CT,NY,NC,ME,VAAniline
CT,NY,NC,ME,NH,VAAnthracene
CT,NY,NC,ME,NH,VABenzidine
CT,NY,NC,ME,NH,VABenzo(a)anthracene
CT,NY,NC,ME,NH,VABenzo(a)pyrene
CT,NY,NC,ME,NH,VABenzo(b)fluoranthene
CT,NY,NC,ME,NH,VABenzo(g,h,i)perylene
CT,NY,NC,ME,NH,VABenzo(k)fluoranthene
NY,NC,ME,NH,VABenzoic Acid
CT,NY,NC,ME,NH,VABis(2-chloroethoxy)methane
CT,NY,NC,ME,NH,VABis(2-chloroethyl)ether
CT,NY,NC,ME,NH,VABis(2-chloroisopropyl)ether
CT,NY,NC,ME,NH,VABis(2-Ethylhexyl)phthalate
CT,NY,NC,ME,NH,VA4-Bromophenylphenylether
CT,NY,NC,ME,NH,VAButylbenzylphthalate
NCCarbazole
CT,NY,NC,ME,NH,VA4-Chloroaniline
CT,NY,NC,ME,NH,VA4-Chloro-3-methylphenol
CT,NY,NC,ME,NH,VA2-Chloronaphthalene
CT,NY,NC,ME,NH,VA2-Chlorophenol
CT,NY,NC,ME,NH,VA4-Chlorophenylphenylether
CT,NY,NC,ME,NH,VAChrysene
CT,NY,NC,ME,NH,VADibenz(a,h)anthracene
CT,NY,NC,ME,NH,VADibenzofuran
CT,NY,NC,ME,NH,VADi-n-butylphthalate
CT,NY,NC,ME,NH,VA1,2-Dichlorobenzene
CT,NY,NC,ME,NH,VA1,3-Dichlorobenzene
CT,NY,NC,ME,NH,VA1,4-Dichlorobenzene
CT,NY,NC,ME,NH,VA3,3-Dichlorobenzidine
CT,NY,NC,ME,NH,VA2,4-Dichlorophenol
CT,NY,NC,ME,NH,VADiethylphthalate
CT,NY,NC,ME,NH,VA2,4-Dimethylphenol
CT,NY,NC,ME,NH,VADimethylphthalate
CT,NY,NC,ME,NH,VA4,6-Dinitro-2-methylphenol
CT,NY,NC,ME,NH,VA2,4-Dinitrophenol
CT,NY,NC,ME,NH,VA2,4-Dinitrotoluene
Page 72 of 81
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270E in Water
CT,NY,NC,ME,NH,VA2,6-Dinitrotoluene
CT,NY,NC,ME,NH,VADi-n-octylphthalate
NY,NC1,2-Diphenylhydrazine/Azobenzene
CT,NY,NC,ME,NH,VAFluoranthene
NY,NC,ME,NH,VAFluorene
CT,NY,NC,ME,NH,VAHexachlorobenzene
CT,NY,NC,ME,NH,VAHexachlorobutadiene
CT,NY,NC,ME,NH,VAHexachlorocyclopentadiene
CT,NY,NC,ME,NH,VAHexachloroethane
CT,NY,NC,ME,NH,VAIndeno(1,2,3-cd)pyrene
CT,NY,NC,ME,NH,VAIsophorone
NC1-Methylnaphthalene
CT,NY,NC,ME,NH,VA2-Methylnaphthalene
CT,NY,NC,NH,VA2-Methylphenol
CT,NY,NC,NH,VA3/4-Methylphenol
CT,NY,NC,ME,NH,VANaphthalene
CT,NY,NC,ME,NH,VA2-Nitroaniline
CT,NY,NC,ME,NH,VA3-Nitroaniline
CT,NY,NC,ME,NH,VA4-Nitroaniline
CT,NY,NC,ME,NH,VANitrobenzene
CT,NY,NC,ME,NH,VA2-Nitrophenol
CT,NY,NC,ME,NH,VA4-Nitrophenol
CT,NY,NC,ME,NH,VAN-Nitrosodimethylamine
CT,NY,NC,ME,NH,VAN-Nitrosodi-n-propylamine
NCPentachloronitrobenzene
CT,NY,NC,ME,NH,VAPentachlorophenol
CT,NY,NC,ME,NH,VAPhenanthrene
CT,NY,NC,ME,NH,VAPhenol
CT,NY,NC,ME,NH,VAPyrene
CT,NY,NC,ME,NH,VAPyridine
NY,NC1,2,4,5-Tetrachlorobenzene
CT,NY,NC,ME,NH,VA1,2,4-Trichlorobenzene
CT,NY,NC,ME,NH,VA2,4,5-Trichlorophenol
CT,NY,NC,ME,NH,VA2,4,6-Trichlorophenol
NC2-Fluorophenol
Page 73 of 81
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2022
M-MA100Massachusetts DEPMA 06/30/2020
PH-0567Connecticut Department of Publilc HealthCT 09/30/2021
10899 NELAPNew York State Department of HealthNY 04/1/2020
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2020
LAO00112Rhode Island Department of HealthRI 12/30/2019
652North Carolina Div. of Water QualityNC 12/31/2020
MA007 NELAPNew Jersey DEPNJ 06/30/2020
E871027 NELAPFlorida Department of HealthFL 06/30/2020
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2020
2011028State of MaineME 06/9/2021
460217Commonwealth of VirginiaVA 12/14/2020
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2020
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2020
25703North Carolina Department of HealthNC-DW 07/31/2020
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2020
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
December 24, 2019
Rob Foster
Wood - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
Project Location: Charlotte, NC
Client Job Number:
Project Number: 6228-18-0495
Laboratory Work Order Number: 19L0639
Enclosed are results of analyses for samples received by the laboratory on December 16, 2019. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 16
Table of Contents
Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 5
19L0639-01 5
19L0639-02 6
19L0639-03 7
Flag/Qualifier Summary 8
Certifications 9
Chain of Custody/Sample Receipt 10
Page 2 of 16
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
12/24/2019
Wood - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
ATTN: Rob Foster
6228-18-0495
19L0639
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Charlotte, NC
11-COMP 19L0639-01 Soil -CT PH-0197/NY11742
12-COMP 19L0639-02 Soil -CT PH-0197/NY11742
13-COMP 19L0639-03 Soil -CT PH-0197/NY11742
[TOC_1]Sample Summary[TOC]
Page 3 of 16
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
[TOC_1]Case Narrative[TOC]
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Tod E. Kopyscinski
Laboratory Director
Page 4 of 16
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/16/2019
Work Order: 19L0639Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0639-01
Field Sample #: 11-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 9:45:00AM
Stop Date/Time: 12/9/2019 10:30:00AM
[TOC_2]19L0639-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Hex Chromium 7199
ND 1 12/19/19 0:00 PALmg/Kg0.255 Hex Chromium 71991Hex Chromium 7199
[TOC_1]Sample Results[TOC]
Page 5 of 16
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/16/2019
Work Order: 19L0639Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0639-02
Field Sample #: 12-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 10:35:00AM
Stop Date/Time: 12/9/2019 11:40:00AM
[TOC_2]19L0639-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Hex Chromium 7199
ND 1 12/19/19 0:00 PALmg/Kg0.255 Hex Chromium 71991Hex Chromium 7199
Page 6 of 16
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/16/2019
Work Order: 19L0639Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0639-03
Field Sample #: 13-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 11:50:00AM
Stop Date/Time: 12/9/2019 12:50:00PM
[TOC_2]19L0639-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
Hex Chromium 7199
ND 1 12/19/19 0:00 PALmg/Kg0.255 Hex Chromium 71991Hex Chromium 7199
Page 7 of 16
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
[TOC_1]Flag/Qualifier Summary[TOC]
Page 8 of 16
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
No certified Analyses included in this Report
[TOC_1]Certifications[TOC]
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2022
M-MA100Massachusetts DEPMA 06/30/2020
PH-0567Connecticut Department of Publilc HealthCT 09/30/2021
10899 NELAPNew York State Department of HealthNY 04/1/2020
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2020
LAO00112Rhode Island Department of HealthRI 12/30/2019
652North Carolina Div. of Water QualityNC 12/31/2020
MA007 NELAPNew Jersey DEPNJ 06/30/2020
E871027 NELAPFlorida Department of HealthFL 06/30/2020
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2020
2011028State of MaineME 06/9/2021
460217Commonwealth of VirginiaVA 12/14/2020
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2020
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2020
25703North Carolina Department of HealthNC-DW 07/31/2020
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2020
Page 9 of 16
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Analyze samples -28, -29 & -30 for Cr VI by method 7199 per Rob F. -KKM 12/16/1919L0639Page 10 of 16
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19L0639Analyze samples -28, -29 & -30 for Cr VI by method 7199 per Rob F. -KKM 12/16/19010203Page 13 of 16
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
January 6, 2020
Rob Foster
Wood - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
Project Location: Charlotte, NC
Client Job Number:
Project Number: 6228-18-0495
Laboratory Work Order Number: 19L0652
Enclosed are results of analyses for samples received by the laboratory on December 16, 2019. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
Kerry K. McGee
Project Manager
Page 1 of 27
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Table of Contents
Sample Summary 3
Case Narrative 4
Sample Results 5
19L0652-01 5
19L0652-02 7
19L0652-03 11
Sample Preparation Information 13
QC Data 14
TCLP - Volatile Organic Compounds by GC/MS 14
B249379 14
TCLP - Semivolatile Organic Compounds by GC/MS 15
B249006 15
TCLP - Metals Analyses 17
B248902 17
B249001 17
Flag/Qualifier Summary 18
Certifications 19
Chain of Custody/Sample Receipt 21
Page 2 of 27
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ANALYTICAL SUMMARY
1/6/2020
Wood - Charlotte
2801 Yorkmont Rd, Suite 100
Charlotte, NC 28208
ATTN: Rob Foster
6228-18-0495
19L0652
The results of analyses performed on the following samples submitted to the CON-TEST Analytical Laboratory are found in this report.
PROJECT LOCATION:
PURCHASE ORDER NUMBER:
PROJECT NUMBER:
REPORT DATE:
WORK ORDER NUMBER:
FIELD SAMPLE #LAB ID:MATRIX TESTSAMPLE DESCRIPTION SUB LAB
Charlotte, NC
11-COMP 19L0652-01 Soil -
SM 2540G
SW-846 6010D
SW-846 7470A
12-COMP 19L0652-02 Soil SM 2540G
SW-846 6010D
SW-846 7470A
SW-846 8260D
SW-846 8270D-E
13-COMP 19L0652-03 Soil -
SM 2540G
SW-846 6010D
SW-846 7470A
[TOC_1]Sample Summary[TOC]
Page 3 of 27
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
[TOC_1]Case Narrative[TOC]
SW-846 8260D
Qualifications:
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits. Data validation is not
affected since all results are "not detected" for associated samples in this batch and bias is on the high side.
Analyte & Samples(s) Qualified:
L-02
Vinyl Chloride
B249379-BS1, B249379-BSD1
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side. Data validation is not affected
since sample result was "not detected" for this compound.
Analyte & Samples(s) Qualified:
V-20
Vinyl Chloride
B249379-BS1, B249379-BSD1, S044364-CCV1
SW-846 8270D-E
Qualifications:
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for this compound.
Analyte & Samples(s) Qualified:
V-05
Pentachlorophenol
B249006-BLK1, B249006-BS1, B249006-BSD1, S044167-CCV1
The results of analyses reported only relate to samples submitted to the Con-Test Analytical Laboratory for testing.
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
Lisa A. Worthington
Technical Representative
Page 4 of 27
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/16/2019
Work Order: 19L0652Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0652-01
Field Sample #: 11-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 9:45:00AM
Stop Date/Time: 12/9/2019 10:30:00AM
[TOC_2]19L0652-01[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
80.1 12/16/19 15:38 JS% Wt 12/16/19SM 2540G1% Solids
[TOC_1]Sample Results[TOC]
Page 5 of 27
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/16/2019
Work Order: 19L0652Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0652-01
Field Sample #: 11-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 9:45:00AM
Stop Date/Time: 12/9/2019 10:30:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
TCLP - Metals Analyses
ND 0.00010 12/24/19 9:21 CJVmg/L0.000034 12/23/19SW-846 7470A1Mercury
Page 6 of 27
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/16/2019
Work Order: 19L0652Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0652-02
Field Sample #: 12-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 10:35:00AM
Stop Date/Time: 12/9/2019 11:40:00AM
[TOC_2]19L0652-02[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
77.5 12/16/19 15:38 JS% Wt 12/16/19SM 2540G1% Solids
Page 7 of 27
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/16/2019
Work Order: 19L0652Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0652-02
Field Sample #: 12-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 10:35:00AM
Stop Date/Time: 12/9/2019 11:40:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
TCLP - Volatile Organic Compounds by GC/MS
ND 0.010 1/3/20 18:37 EEHmg/L0.0018 1/3/20SW-846 8260D10Benzene
ND 0.20 1/3/20 18:37 EEHmg/L0.019 1/3/20SW-846 8260D102-Butanone (MEK)
ND 0.010 1/3/20 18:37 EEHmg/L0.0011 1/3/20SW-846 8260D10Carbon Tetrachloride
ND 0.010 1/3/20 18:37 EEHmg/L0.0015 1/3/20SW-846 8260D10Chlorobenzene
ND 0.020 1/3/20 18:37 EEHmg/L0.0017 1/3/20SW-846 8260D10Chloroform
ND 0.010 1/3/20 18:37 EEHmg/L0.0013 1/3/20SW-846 8260D101,4-Dichlorobenzene
ND 0.010 1/3/20 18:37 EEHmg/L0.0041 1/3/20SW-846 8260D101,2-Dichloroethane
ND 0.010 1/3/20 18:37 EEHmg/L0.0032 1/3/20SW-846 8260D101,1-Dichloroethylene
ND 0.010 1/3/20 18:37 EEHmg/L0.0018 1/3/20SW-846 8260D10Tetrachloroethylene
ND 0.010 1/3/20 18:37 EEHmg/L0.0024 1/3/20SW-846 8260D10Trichloroethylene
ND 0.020 1/3/20 18:37 EEHmg/L0.0045 1/3/20SW-846 8260D10Vinyl Chloride
Surrogates % Recovery Recovery Limits Flag/Qual
1,2-Dichloroethane-d4 90.7 1/3/20 18:3770-130
Toluene-d8 95.6 1/3/20 18:3770-130
4-Bromofluorobenzene 97.9 1/3/20 18:3770-130
Page 8 of 27
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/16/2019
Work Order: 19L0652Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0652-02
Field Sample #: 12-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 10:35:00AM
Stop Date/Time: 12/9/2019 11:40:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
TCLP - Semivolatile Organic Compounds by GC/MS
ND 0.050 1/6/20 8:54 KLBmg/L0.0016 12/24/19SW-846 8270D-E12,4-Dinitrotoluene
ND 0.050 1/6/20 8:54 KLBmg/L0.0022 12/24/19SW-846 8270D-E1Hexachlorobenzene
ND 0.050 1/6/20 8:54 KLBmg/L0.0030 12/24/19SW-846 8270D-E1Hexachlorobutadiene
ND 0.050 1/6/20 8:54 KLBmg/L0.0026 12/24/19SW-846 8270D-E1Hexachloroethane
ND 0.050 1/6/20 8:54 KLBmg/L0.0023 12/24/19SW-846 8270D-E12-Methylphenol
ND 0.050 1/6/20 8:54 KLBmg/L0.0010 12/24/19SW-846 8270D-E13/4-Methylphenol
ND 0.050 1/6/20 8:54 KLBmg/L0.0020 12/24/19SW-846 8270D-E1Nitrobenzene
ND 0.050 1/6/20 8:54 KLBmg/L0.0017 12/24/19SW-846 8270D-E1Pentachlorophenol
ND 0.025 1/6/20 8:54 KLBmg/L0.014 12/24/19SW-846 8270D-E1Pyridine
ND 0.050 1/6/20 8:54 KLBmg/L0.0024 12/24/19SW-846 8270D-E12,4,5-Trichlorophenol
ND 0.050 1/6/20 8:54 KLBmg/L0.0017 12/24/19SW-846 8270D-E12,4,6-Trichlorophenol
Surrogates % Recovery Recovery Limits Flag/Qual
2-Fluorophenol 75.0 1/6/20 8:5415-110
Phenol-d6 79.6 1/6/20 8:5415-110
Nitrobenzene-d5 79.2 1/6/20 8:5430-130
2-Fluorobiphenyl 88.4 1/6/20 8:5430-130
2,4,6-Tribromophenol 86.5 1/6/20 8:5415-110
p-Terphenyl-d14 79.9 1/6/20 8:5430-130
Page 9 of 27
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/16/2019
Work Order: 19L0652Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0652-02
Field Sample #: 12-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 10:35:00AM
Stop Date/Time: 12/9/2019 11:40:00AM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
TCLP - Metals Analyses
ND 0.050 12/26/19 15:08 MJHmg/L0.0095 12/24/19SW-846 6010D1Arsenic
ND 0.00010 12/24/19 9:23 CJVmg/L0.000034 12/23/19SW-846 7470A1Mercury
0.31 0.50 12/26/19 15:08 MJHmg/L0.0059 12/24/19SW-846 6010D1JBarium
ND 0.010 12/26/19 15:08 MJHmg/L0.0016 12/24/19SW-846 6010D1Cadmium
0.0028 0.050 12/26/19 15:08 MJHmg/L0.0023 12/24/19SW-846 6010D1JChromium
0.017 0.10 12/26/19 15:08 MJHmg/L0.0060 12/24/19SW-846 6010D1JLead
ND 0.050 12/26/19 15:08 MJHmg/L0.016 12/24/19SW-846 6010D1Selenium
ND 0.050 12/26/19 15:08 MJHmg/L0.0034 12/24/19SW-846 6010D1Silver
Page 10 of 27
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/16/2019
Work Order: 19L0652Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0652-03
Field Sample #: 13-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 11:50:00AM
Stop Date/Time: 12/9/2019 12:50:00PM
[TOC_2]19L0652-03[TOC]
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
Units
Date
PreparedMethod
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
80.1 12/16/19 15:38 JS% Wt 12/16/19SM 2540G1% Solids
Page 11 of 27
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Date Received: 12/16/2019
Work Order: 19L0652Sample Description:Project Location: Charlotte, NC
Sample ID: 19L0652-03
Field Sample #: 13-COMP
Sample Matrix: Soil
Start Date/Time: 12/9/2019 11:50:00AM
Stop Date/Time: 12/9/2019 12:50:00PM
AnalystAnalyzedDilutionFlag/QualRLResultsAnalyte
Date/Time
DL Units
Date
PreparedMethod
TCLP - Metals Analyses
ND 0.00010 12/24/19 9:24 CJVmg/L0.000034 12/23/19SW-846 7470A1Mercury
Page 12 of 27
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]Batch Date
B248467 12/16/1919L0652-01 [11-COMP]
B248467 12/16/1919L0652-02 [12-COMP]
B248467 12/16/1919L0652-03 [13-COMP]
Prep Method: SW-846 3010A-SW-846 6010D
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
Leachates were extracted on 12/19/2019 per SW-846 1311 in Batch B248620
B249001 12/24/1950.0 50.019L0652-02 [12-COMP]
Prep Method: SW-846 7470A Prep-SW-846 7470A
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
Leachates were extracted on 12/19/2019 per SW-846 1311 in Batch B248620
B248902 12/23/196.00 6.0019L0652-01 [11-COMP]
B248902 12/23/196.00 6.0019L0652-02 [12-COMP]
B248902 12/23/196.00 6.0019L0652-03 [13-COMP]
Prep Method: SW-846 5030B-SW-846 8260D
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
Leachates were extracted on 12/19/2019 per SW-846 1311 in Batch B248732
B249379 01/03/205.00 5.0019L0652-02 [12-COMP]
Prep Method: SW-846 3510C-SW-846 8270D-E
Lab Number [Field ID]Batch DateInitial [mL]Final [mL]
Leachates were extracted on 12/19/2019 per SW-846 1311 in Batch B248620
B249006 12/24/19200 1.0019L0652-02 [12-COMP]
[TOC_1]Sample Preparation Information[TOC]
Page 13 of 27
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
TCLP - Volatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]TCLP - Volatile Organic Compounds by GC/MS[TOC]
Batch B249379 - SW-846 5030B
[TOC_3]B249379[TOC]
Blank (B249379-BLK1) Prepared & Analyzed: 01/03/20
Benzene mg/L0.010ND
2-Butanone (MEK)mg/L0.20ND
Carbon Tetrachloride mg/L0.010ND
Chlorobenzene mg/L0.010ND
Chloroform mg/L0.020ND
1,4-Dichlorobenzene mg/L0.010ND
1,2-Dichloroethane mg/L0.010ND
1,1-Dichloroethylene mg/L0.010ND
Tetrachloroethylene mg/L0.010ND
Trichloroethylene mg/L0.010ND
Vinyl Chloride mg/L0.020ND
mg/L 0.0250 70-130Surrogate: 1,2-Dichloroethane-d4 86.80.0217
mg/L 0.0250 70-130Surrogate: Toluene-d8 95.50.0239
mg/L 0.0250 70-130Surrogate: 4-Bromofluorobenzene 96.60.0241
LCS (B249379-BS1) Prepared & Analyzed: 01/03/20
Benzene mg/L0.0010 0.0100 70-13087.50.00875
2-Butanone (MEK)mg/L0.020 0.100 40-1601020.102
Carbon Tetrachloride mg/L0.0010 0.0100 70-1301040.0104
Chlorobenzene mg/L0.0010 0.0100 70-1301030.0103
Chloroform mg/L0.0020 0.0100 70-13086.40.00864
1,4-Dichlorobenzene mg/L0.0010 0.0100 70-1301010.0101
1,2-Dichloroethane mg/L0.0010 0.0100 70-1301090.0109
1,1-Dichloroethylene mg/L0.0010 0.0100 70-1301110.0111
Tetrachloroethylene mg/L0.0010 0.0100 70-1301140.0114
Trichloroethylene mg/L0.0010 0.0100 70-1301000.0100
Vinyl Chloride mg/L0.0020 0.0100 L-02, V-2040-160364*0.0364
mg/L 0.0250 70-130Surrogate: 1,2-Dichloroethane-d4 91.50.0229
mg/L 0.0250 70-130Surrogate: Toluene-d8 96.80.0242
mg/L 0.0250 70-130Surrogate: 4-Bromofluorobenzene 98.00.0245
LCS Dup (B249379-BSD1) Prepared & Analyzed: 01/03/20
Benzene mg/L0.0010 0.0100 2570-13088.3 0.9100.00883
2-Butanone (MEK)mg/L0.020 0.100 2540-160110 7.160.110
Carbon Tetrachloride mg/L0.0010 0.0100 2570-130104 0.4820.0104
Chlorobenzene mg/L0.0010 0.0100 2570-130107 3.520.0107
Chloroform mg/L0.0020 0.0100 2570-13087.2 0.9220.00872
1,4-Dichlorobenzene mg/L0.0010 0.0100 2570-130105 4.280.0105
1,2-Dichloroethane mg/L0.0010 0.0100 2570-130109 0.09200.0109
1,1-Dichloroethylene mg/L0.0010 0.0100 2570-130111 0.1810.0111
Tetrachloroethylene mg/L0.0010 0.0100 2570-130119 4.550.0119
Trichloroethylene mg/L0.0010 0.0100 2570-130106 5.240.0106
Vinyl Chloride mg/L0.0020 0.0100 25 L-02, V-2040-160364 0.0274*0.0364
mg/L 0.0250 70-130Surrogate: 1,2-Dichloroethane-d4 94.80.0237
mg/L 0.0250 70-130Surrogate: Toluene-d8 97.60.0244
mg/L 0.0250 70-130Surrogate: 4-Bromofluorobenzene 1000.0250
[TOC_1]QC Data[TOC]
Page 14 of 27
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
TCLP - Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
[TOC_2]TCLP - Semivolatile Organic Compounds by GC/MS[TOC]
Batch B249006 - SW-846 3510C
[TOC_3]B249006[TOC]
Blank (B249006-BLK1) Prepared: 12/24/19 Analyzed: 12/27/19
2,4-Dinitrotoluene mg/L0.050ND
Hexachlorobenzene mg/L0.050ND
Hexachlorobutadiene mg/L0.050ND
Hexachloroethane mg/L0.050ND
2-Methylphenol mg/L0.050ND
3/4-Methylphenol mg/L0.050ND
Nitrobenzene mg/L0.050ND
Pentachlorophenol mg/L0.050 V-05ND
Pyridine mg/L0.025ND
2,4,5-Trichlorophenol mg/L0.050ND
2,4,6-Trichlorophenol mg/L0.050ND
mg/L 1.00 15-110Surrogate: 2-Fluorophenol 75.50.755
mg/L 1.00 15-110Surrogate: Phenol-d6 79.70.797
mg/L 0.500 30-130Surrogate: Nitrobenzene-d5 82.60.413
mg/L 0.500 30-130Surrogate: 2-Fluorobiphenyl 95.00.475
mg/L 1.00 15-110Surrogate: 2,4,6-Tribromophenol 95.90.959
mg/L 0.500 30-130Surrogate: p-Terphenyl-d14 89.60.448
LCS (B249006-BS1) Prepared: 12/24/19 Analyzed: 12/27/19
2,4-Dinitrotoluene mg/L0.050 0.250 40-14087.70.219
Hexachlorobenzene mg/L0.050 0.250 40-14077.30.193
Hexachlorobutadiene mg/L0.050 0.250 40-14063.00.157
Hexachloroethane mg/L0.050 0.250 40-14068.10.170
2-Methylphenol mg/L0.050 0.250 30-13080.10.200
3/4-Methylphenol mg/L0.050 0.250 30-13079.00.197
Nitrobenzene mg/L0.050 0.250 40-14080.00.200
Pentachlorophenol mg/L0.050 0.250 V-0530-13046.30.116
Pyridine mg/L0.025 0.250 10-14043.40.109
2,4,5-Trichlorophenol mg/L0.050 0.250 30-13076.90.192
2,4,6-Trichlorophenol mg/L0.050 0.250 30-13072.90.182
mg/L 1.00 15-110Surrogate: 2-Fluorophenol 76.60.766
mg/L 1.00 15-110Surrogate: Phenol-d6 79.60.796
mg/L 0.500 30-130Surrogate: Nitrobenzene-d5 79.00.395
mg/L 0.500 30-130Surrogate: 2-Fluorobiphenyl 95.70.478
mg/L 1.00 15-110Surrogate: 2,4,6-Tribromophenol 96.00.960
mg/L 0.500 30-130Surrogate: p-Terphenyl-d14 84.00.420
LCS Dup (B249006-BSD1) Prepared: 12/24/19 Analyzed: 12/27/19
2,4-Dinitrotoluene mg/L0.050 0.250 2040-14092.2 5.050.231
Hexachlorobenzene mg/L0.050 0.250 2040-14081.2 4.870.203
Hexachlorobutadiene mg/L0.050 0.250 2040-14066.4 5.320.166
Hexachloroethane mg/L0.050 0.250 5040-14071.6 5.010.179
2-Methylphenol mg/L0.050 0.250 2030-13084.2 4.970.210
3/4-Methylphenol mg/L0.050 0.250 2030-13084.7 6.990.212
Nitrobenzene mg/L0.050 0.250 2040-14085.6 6.760.214
Pentachlorophenol mg/L0.050 0.250 50 V-0530-13047.4 2.390.118
Pyridine mg/L0.025 0.250 5010-14044.6 2.640.112
2,4,5-Trichlorophenol mg/L0.050 0.250 2030-13079.1 2.870.198
2,4,6-Trichlorophenol mg/L0.050 0.250 5030-13075.4 3.350.188
mg/L 1.00 15-110Surrogate: 2-Fluorophenol 80.60.806
mg/L 1.00 15-110Surrogate: Phenol-d6 85.10.851
mg/L 0.500 30-130Surrogate: Nitrobenzene-d5 84.00.420
Page 15 of 27
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
TCLP - Semivolatile Organic Compounds by GC/MS - Quality Control
QUALITY CONTROL
Batch B249006 - SW-846 3510C
LCS Dup (B249006-BSD1) Prepared: 12/24/19 Analyzed: 12/27/19
mg/L 0.500 30-130Surrogate: 2-Fluorobiphenyl 99.70.498
mg/L 1.00 15-110Surrogate: 2,4,6-Tribromophenol 99.20.992
mg/L 0.500 30-130Surrogate: p-Terphenyl-d14 89.50.448
Page 16 of 27
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Result Limit
Reporting
Units Level
Spike
Result
Source
%REC
%REC
Limits RPD
RPD
Limit Notes Analyte
TCLP - Metals Analyses - Quality Control
QUALITY CONTROL
[TOC_2]TCLP - Metals Analyses[TOC]
Batch B248902 - SW-846 7470A Prep
[TOC_3]B248902[TOC]
Blank (B248902-BLK1) Prepared: 12/23/19 Analyzed: 12/24/19
Mercury mg/L0.00010ND
LCS (B248902-BS1) Prepared: 12/23/19 Analyzed: 12/24/19
Mercury mg/L0.00010 0.00400 80-1201000.00401
LCS Dup (B248902-BSD1) Prepared: 12/23/19 Analyzed: 12/24/19
Mercury mg/L0.00010 0.00400 2080-12096.4 3.800.00386
Batch B249001 - SW-846 3010A
[TOC_3]B249001[TOC]
Blank (B249001-BLK1) Prepared: 12/24/19 Analyzed: 12/26/19
Arsenic mg/L0.050ND
Barium mg/L0.50ND
Cadmium mg/L0.010ND
Chromium mg/L0.050ND
Lead mg/L0.10ND
Selenium mg/L0.050ND
Silver mg/L0.050ND
LCS (B249001-BS1) Prepared: 12/24/19 Analyzed: 12/26/19
Arsenic mg/L0.050 0.500 80-12098.70.493
Barium mg/L0.50 0.500 J80-12097.40.487
Cadmium mg/L0.010 0.500 80-12097.10.486
Chromium mg/L0.050 0.500 80-12095.20.476
Lead mg/L0.10 0.500 80-12094.40.472
Selenium mg/L0.050 0.500 80-1201010.504
Silver mg/L0.050 0.500 80-1201060.528
LCS Dup (B249001-BSD1) Prepared: 12/24/19 Analyzed: 12/26/19
Arsenic mg/L0.050 0.500 2080-120100 1.570.501
Barium mg/L0.50 0.500 20 J80-12098.7 1.260.493
Cadmium mg/L0.010 0.500 2080-12098.2 1.080.491
Chromium mg/L0.050 0.500 2080-12096.5 1.370.483
Lead mg/L0.10 0.500 2080-12096.3 2.020.481
Selenium mg/L0.050 0.500 2080-120104 3.070.520
Silver mg/L0.050 0.500 2080-120106 0.4340.530
Matrix Spike (B249001-MS1) Prepared: 12/24/19 Analyzed: 12/26/19 Source: 19L0652-03
Arsenic mg/L0.050 0.500 75-12597.70.488 ND
Barium mg/L0.50 0.500 75-12594.00.722 0.251
Cadmium mg/L0.010 0.500 75-12594.30.471 ND
Chromium mg/L0.050 0.500 75-12592.90.467 0.00249
Lead mg/L0.10 0.500 75-12589.90.474 0.0248
Selenium mg/L0.050 0.500 75-12591.60.458 ND
Silver mg/L0.050 0.500 75-1251020.510 ND
Page 17 of 27
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
*QC result is outside of established limits.
Wide recovery limits established for difficult compound.
Wide RPD limits established for difficult compound.
#Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
RL Reporting Limit is at the level of quantitation (LOQ)
DL Detection Limit is the lower limit of detection determined by the MDL study
MCL Maximum Contaminant Level
ND Not Detected
Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag).
J
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits.
Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is
on the high side.
L-02
Continuing calibration verification (CCV) did not meet method specifications and was biased on the low side for
this compound.
V-05
Continuing calibration verification (CCV) did not meet method specifications and was biased on the high side.
Data validation is not affected since sample result was "not detected" for this compound.
V-20
[TOC_1]Flag/Qualifier Summary[TOC]
Page 18 of 27
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 6010D in Water
NY,CT,NC,ME,NH,VAArsenic
NY,CT,ME,NC,NH,VABarium
NY,CT,ME,NC,NH,VACadmium
NY,CT,ME,NC,NH,VAChromium
NY,CT,ME,NC,NH,VALead
CT,ME,NC,NH,NY,VASelenium
CT,ME,NC,NH,NY,VASilver
SW-846 7470A in Water
CT,ME,NC,NH,NY,VAMercury
SW-846 8260D in Soil
ME,NY,CT,NC,VABenzene
ME,NY,CT,NC,VA2-Butanone (MEK)
ME,NY,CT,NC,VACarbon Tetrachloride
ME,NY,CT,NC,VAChlorobenzene
ME,NY,CT,NC,VAChloroform
ME,NY,CT,NC,VA1,4-Dichlorobenzene
ME,NY,CT,NC,VA1,2-Dichloroethane
ME,NY,CT,NC,VA1,1-Dichloroethylene
ME,NY,VAHexachlorobutadiene
ME,NY,CT,NC,VATetrachloroethylene
ME,NY,CT,NC,VATrichloroethylene
ME,NY,CT,NC,VAVinyl Chloride
SW-846 8270D-E in Soil
ME,NC,NH,NY,VA1,4-Dichlorobenzene
ME,NC,NH,NY,CT,VA2,4-Dinitrotoluene
ME,NC,NH,NY,CT,VAHexachlorobenzene
ME,NC,NH,NY,CT,VAHexachlorobutadiene
ME,NC,NH,NY,CT,VAHexachloroethane
ME,NC,NH,NY,CT,VA2-Methylphenol
ME,NC,NH,NY,CT,VA3/4-Methylphenol
ME,NC,NH,NY,CT,VANitrobenzene
ME,NC,NH,NY,CT,VAPentachlorophenol
ME,NC,NH,NY,CT,VAPyridine
ME,NC,NH,NY,CT,VA2,4,5-Trichlorophenol
ME,NC,NH,NY,CT,VA2,4,6-Trichlorophenol
NC2-Fluorophenol
SW-846 8270D-E in Water
ME,NC,NH,NY,VA1,4-Dichlorobenzene
ME,NC,NH,CT,NY,VA2,4-Dinitrotoluene
ME,NC,NH,CT,NY,VAHexachlorobenzene
ME,NC,NH,CT,NY,VAHexachlorobutadiene
ME,NC,NH,CT,NY,VAHexachloroethane
ME,NC,NH,CT2-Methylphenol
ME,NC,NH,CT3/4-Methylphenol
ME,NC,NH,CT,NY,VANitrobenzene
[TOC_1]Certifications[TOC]
Page 19 of 27
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39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CertificationsAnalyte
CERTIFICATIONS
Certified Analyses included in this Report
SW-846 8270D-E in Water
ME,NC,NH,CT,NY,VAPentachlorophenol
ME,NC,NH,CT,NY,VAPyridine
ME,NC,NH,CT,NY,VA2,4,5-Trichlorophenol
ME,NC,NH,CT,NY,VA2,4,6-Trichlorophenol
NC2-Fluorophenol
The CON-TEST Environmental Laboratory operates under the following certifications and accreditations:
Code Description Number Expires
100033AIHA-LAP, LLC - ISO17025:2017AIHA 03/1/2022
M-MA100Massachusetts DEPMA 06/30/2020
PH-0567Connecticut Department of Publilc HealthCT 09/30/2021
10899 NELAPNew York State Department of HealthNY 04/1/2020
2516 NELAPNew Hampshire Environmental LabNH-S 02/5/2020
LAO00112Rhode Island Department of HealthRI 12/30/2020
652North Carolina Div. of Water QualityNC 12/31/2020
MA007 NELAPNew Jersey DEPNJ 06/30/2020
E871027 NELAPFlorida Department of HealthFL 06/30/2020
LL015036Vermont Department of Health Lead LaboratoryVT 07/30/2020
2011028State of MaineME 06/9/2021
460217Commonwealth of VirginiaVA 12/14/2020
2557 NELAPNew Hampshire Environmental LabNH-P 09/6/2020
VT-255716Vermont Department of Health Drinking WaterVT-DW 06/12/2020
25703North Carolina Department of HealthNC-DW 07/31/2020
68-05812Commonwealth of Pennsylvania DEPPA 06/30/2020
Page 20 of 27
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Activate sample 19L0652-02 (19L0324-29) for TCLP VOCs, TCLP SVOCs & TCLP RCRA-8 metals per Leanna M. -KKM 12/27/19Page 21 of 27
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Activate sample 19L0652-02 (19L0324-29) for TCLP VOCs, TCLP SVOCs & TCLP RCRA-8 metals per Leanna M. -KKM 12/27/19Page 22 of 27
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Activate sample 19L0652-02 (19L0324-29) for TCLP VOCs, TCLP SVOCs & TCLP RCRA-8 metals per Leanna M. -KKM 12/27/19Page 23 of 27
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Activate sample 19L0652-02 (19L0324-29) for TCLP VOCs, TCLP SVOCs & TCLP RCRA-8 metals per Leanna M. -KKM 12/27/19Page 24 of 27
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19L0652Page 25 of 27
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