21014_Dicey Mills_Pond Closure and Additional Brownfields Assessment Report_20191101

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Pond Closure and Additional Brownfields Assessment Report Former Dicey Mills
430 Neisler Street Shelby, North Carolina H&H Job No. DCY-001
Table of Contents
Section Page No. 1.0 Introduction ............................................................................................................................ 1
2.0 Background Information....................................................................................................... 2
2.1 Brief Site History .................................................................................................................. 2
2.2 Previous Assessment Activities ............................................................................................ 3
3.0 Pond Closure Scope of Work ................................................................................................ 7
3.1 Stormwater Permit ................................................................................................................ 7
3.2 Dewatering Activities ........................................................................................................... 7
3.3 Clearing and Grading Activities ........................................................................................... 8
3.4 Site Contingency Activities .................................................................................................. 9
4.0 Additional Brownfields Assessment Activities .................................................................. 12
4.1 Final Grade Soil Sampling ................................................................................................. 12
4.2 Groundwater Sampling ....................................................................................................... 13
4.3 Groundwater Flow and Hydraulic Gradients...................................................................... 14
4.4 Quality Assurance/Quality Control .................................................................................... 14
5.0 Analytical Laboratory Results ............................................................................................ 15
5.1 Soil Analytical Results ....................................................................................................... 15
5.2 Groundwater Analytical Results ......................................................................................... 16
6.0 Summary and Conclusions.................................................................................................. 17

List of Tables
Table 1 Summary of Groundwater Geochemical Data
Table 2 Summary of Well Construction and Groundwater Elevation Data
Table 3 Summary of Soil Analytical Data – Final Grade Samples
Table 4 Summary of Groundwater Analytical Data

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List of Figures
Figure 1 Site Location Map
Figure 2 Site Map
Figure 3 Shallow Groundwater Potentiometric Map

List of Appendices
Appendix A Grading Plan
Appendix B Laboratory Analytical Reports
Appendix C Summary of Previous Brownfields Assessment Results

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Pond Closure and Additional Brownfields Assessment Report
Former Dicey Mills 430 Neisler Street Shelby, North Carolina H&H Job No. DCY-001

1.0 Introduction

Hart & Hickman, PC (H&H) has prepared this Pond Closure and Additional Brownfields
Assessment Report for the former Dicey Mills facility located at 430 Neisler Street in Shelby,
Cleveland County, North Carolina (Site). The Site was determined eligible for the North
Carolina Department of Environmental Quality (DEQ) Brownfields Program in April 2017, and
a Brownfields Agreement is in the process of being completed (Brownfields Project No. 21014-
17-023). A Site Location Map is provided as Figure 1. The Site is comprised of three parcels of
land totaling approximately 23.89 acres and is developed with an approximately 160,000 square
foot (SF) main building, an approximately 4,000 SF storage building, and associated parking
areas. The remainder of the Site is undeveloped land.

Textile manufacturing operations ceased at the facility in 2016. The main building is planned to
be leased to various users for warehousing and distribution purposes. Five ponds were located in
the southern and western portions of the Site and were previously used to manage process water
from textile manufacturing operations prior to discharge into the municipal sewer system and to
store freshwater from the First Broad River for use in the plant operations. Because the on-Site
ponds were no longer needed to manage wastewater prior to discharge to the sanitary sewer and
the City of Shelby had requested that the discharge of surface water to the sanitary sewer cease,
the former ponds were closed in accordance with the DEQ-approved Pond Closure Work Plan
Revision-1 (Work Plan) dated August 9, 2018.

In addition, DEQ Brownfields requested that groundwater samples from the four existing
permanent groundwater monitoring wells at the Site (MW-1 through MW-4) be collected. Based
on discussions with the DEQ Brownfields Project Manager, Ms. Jordan Thompson, the

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groundwater sampling was to be conducted in accordance with the previously approved
Brownfields Assessment Work Plan dated July 21, 2017. A brief Site history and summary of
previous assessment activities are presented in Section 2 below.

2.0 Background Information

2.1 Brief Site History

The Site was developed in the late 1950s with portions of the current building. The building was
expanded over time through the mid-1990s. From the late 1950s to the early 2000s, the Site
building was utilized for weaving, fabric finishing, yarn manufacturing, olefin filament yarn
extrusion, and textile dyeing/printing operations. The Site was used for weaving, fabric
finishing, and olefin filament yarn extrusion from the early 2000s until March 2015.
Subsequently, a portion of the Site building was leased to Valdese Weavers and used for olefin
filament yarn extrusion and yarn production until December 2016. Since that time, the Site has
remained vacant.

Floor drains inside the building formerly collected wastewater that discharged to an outfall pipe
and then a series of ponds located south and west of the building. The outfall pipe from the plant
discharged to Pond #1, Pond #1 discharged into Pond #2, Pond #2 discharged into Pond #4, and
the discharge from Pond #4 entered the municipal sewer system. An out of use process water
pond (Pond #3) was also located south of the Site building and was historically utilized to store
excess process water prior to discharge to the sanitary sewer. At that time, the process water was
routed from the discharge pipe to Pond #1, Pond #2, Pond #3, Pond #4, and finally the City of
Shelby sanitary sewer system. In addition, a Freshwater Pond was located between Pond #3 and
Pond #4 that was used to store freshwater from the nearby Broad River prior to use in plant
operations. The locations of the former ponds are depicted on Figure 2.

Because the on-Site ponds were no longer needed to manage wastewater prior to discharge to the
sanitary sewer and the City of Shelby had requested that the discharge of surface water to the

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sanitary sewer cease, the former ponds were properly closed in-place and discharge to the City of
Shelby sewer system was eliminated. The ponds were unlined and contained predominantly
rainwater at the time of closure. Pond closure activities are discussed further in Section 3.

2.2 Previous Assessment Activities

A brief summary of previous assessment activities conducted at the Site is provided below.

H&H reviewed an Underground Storage Tank (UST) Closure Report from October 1996
completed by Royster Oil Company, Inc. (Royster). Royster reported that a 20,000-gallon fuel
oil UST and a 10,000-gallon fuel oil UST were removed from the Site from within two separate
containment basins in the eastern portion of the Site and confirmation samples were collected
from the base of the excavations (Incident No. 18281). The soil samples were analyzed for oil
and grease by EPA Method 9071. Soil impacts were not identified above the DEQ Action
Levels at that time. DEQ initially filed the closure documentation as a leaking UST incident
with impacts present above Action Levels. However, following correspondence between the Site
owner, DEQ, and Royster, a Notice of No Further Action (NFA) was issued for the fuel oil
USTs.

Southeastern Geologic Services, Inc. (SES) completed a UST Closure Report for the Site in
February 1997. The report indicates that a 1,000-gallon gasoline UST was discovered in January
1997 during construction of an eastern addition to the Site building (Incident No. 18747).
Following removal of the orphaned UST, total petroleum hydrocarbons (TPH) were identified
above DEQ Action Levels in soil and petroleum constituents were identified in groundwater
above DEQ 2L Groundwater Quality Standards (2L Standards) but below DEQ-defined Gross
Contaminant Levels (GCLs) in a monitoring well located immediately adjacent to the orphaned
UST location. Downgradient monitoring wells did not contain impacts above laboratory method
detection limits. DEQ issued a NFA for the release in August 1998. The NFA indicates that
groundwater on the Site is not suitable for use as a water supply and that the Site is not suitable
for residential use (including homes, daycare centers, schools, or recreation areas).

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Blue Ridge Environmental Services, Inc. (BRE) conducted a limited Phase II Environmental Site
Assessment (ESA) at the Site in February 2016. BRE advanced two soil borings and installed
two temporary monitoring wells to evaluate the potential for impact associated with the ponds.
The soil borings were advanced within Pond #1 and Pond #2, and the temporary monitoring
wells were installed south of Pond #2 and west of Pond #4. Results of analysis of the soil
samples indicated bis(2-ethylhexyl) phthalate, antimony, and cobalt were detected at
concentrations above the DEQ Inactive Hazardous Sites Branch (IHSB) Protection of
Groundwater Preliminary Soil Remediation Goals (PSRGs), although background concentrations
of metals were not determined. The results of analysis of the groundwater samples indicated the
presence of trichloroethylene (TCE) downgradient of Pond #2 at a concentration of 9.10 µg/L
(versus the 2L Standard of 3 µg/L). Several metals were also detected above 2L Standards in the
samples but may have been associated with sample turbidity.

To further assess the potential for impact from historical operations, H&H performed soil and
sub-slab soil vapor assessment activities at the Site in August 2016. H&H’s assessment
activities focused on evaluating potential risks associated with redevelopment of the Site and
included collection and analysis of soil samples from exterior locations on the Site to evaluate
potential concerns associated with direct contact with soil and collection and analysis of sub-slab
soil vapor samples to evaluate the vapor intrusion pathway. The results of analysis of the soil
samples did not indicate significant soil impacts in exterior areas of the Site. Hexavalent
chromium was detected in the soil boring located adjacent to the wastewater outfall pipe south of
the former manufacturing building at a concentration of 0.87 mg/kg, which slightly exceeds the
Residential PSRG of 0.31 mg/kg but is below the Industrial PSRG of 6.5 mg/kg.

The results of the analysis of the sub-slab soil vapor samples indicated that TCE was detected in
the samples located below the storage building, and the western, south-central, and north-central
portions of the former manufacturing building at concentrations exceeding the DEQ Division of
Waste Management (DWM) Non-Residential Soil Gas Screening Level (SGSL). Additionally,
TCE was detected in the sub-slab soil vapor sample collected from the northern portion of the

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former manufacturing building at a concentration slightly below the Non-Residential SGSL. No
other volatile organic compounds (VOCs) were detected in the sub-slab vapor samples above the
Non-Residential SGSLs.

Based upon the results of the sub-slab soil vapor sampling, H&H collected indoor air samples in
select locations to further evaluate the potential for vapor intrusion into the Site buildings. The
results of the indoor air samples indicated that TCE was detected in the sample collected from
the west-central portion of the main Site building at a concentration slightly exceeding the
conservative DEQ Non-Residential Indoor Air Screening Level (IASL). No other compounds
were detected at concentrations exceeding the IASLs. H&H used the DEQ Risk Calculator at the
time (August 2016 Version) to calculate cumulative potential carcinogenic and non-carcinogenic
risks for a worker based on the indoor air results. The results of the cumulative risk calculations
indicated that the calculated cumulative lifetime incremental cancer risks (LICRs) do not exceed
the acceptable risk range of 1 x 10-4 to 1 x 10-6 and the calculated non-carcinogenic hazard index
(HI) values do not exceed the acceptable threshold level of 1.

To further evaluate the sediment in the ponds, H&H collected sediment samples from each pond
for laboratory analysis in August and November 2016. Based on the results of the sediment
assessment, sediment in Ponds #1, #3, and #4 contain concentrations of antimony at levels
exceeding background and Residential and/or Industrial PSRGs. Additionally, several
compounds were detected above Protection of Groundwater PSRGs primarily in the samples
from Pond #3 and Pond #4 including n-butylbenzene, 1,2,4-trimethylbenzene, bis(2-ethylhexyl)
phthalate, toluene, and/or zinc. Sediment in Pond #2 and the Freshwater Pond does not appear to
be significantly impacted.

To further assess groundwater conditions at the Site, H&H installed and collected groundwater
samples from four permanent shallow Type II groundwater monitoring wells at the Site (MW-1
through MW-4) in October 2017 (see Figure 2). MW-1 was installed west (and downgradient)
of the central portion of the former manufacturing building. MW-2 was installed downgradient
of the former dye house in the southeastern portion of the Site. MW-3 was installed adjacent to

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and downgradient of Pond #3 and MW-4 was installed adjacent to and downgradient of Pond #4.
The results of the groundwater assessment indicated that TCE was detected in the groundwater
sample collected from MW-1 (7.6 µg/L) and MW-4 (110 µg/L) at concentrations above the 2L
Standard of 3 µg/L. Manganese was detected at concentrations above the 2L Standard of 50
µg/L in the groundwater samples collected from MW-1, MW-2 and MW-4 and thallium was
detected at an estimated concentration slightly above the DEQ Interim Maximum Allowable
Concentration (IMAC) of 0.2 µg/L in the groundwater sample collected from MW-2.

Based on the results of the August and November 2016 sediment assessment activities, select
sediment samples were analyzed for Synthetic Precipitation Leaching Procedure (SPLP) leachate
analyses. SPLP analytical results were compared to 2L Standards or the IMAC (if no 2L
Standard is established). Based upon the SPLP results, antimony and bis(2-ethylhexyl) phthalate
posed a potential Site-specific leaching concern in the sediment in Pond #3 and Pond #4.
However, the October 2017 groundwater sampling event indicated that antimony and bis(2-
ethylhexyl) phthalate were not detected in groundwater immediately downgradient of Pond #3
(MW-3) and Pond #4 (MW-4) at concentrations exceeding laboratory reporting limits.
Therefore, the antimony and bis(2-ethylhexyl) phthalate concentrations in the sediment in Pond
#3 and Pond #4 do not appear to pose a significant Site-specific leaching concern.

An unnamed intermittent tributary of the First Broad River traverses the southern Site boundary.
To evaluate the potential for impact to surface water in the tributary, H&H collected two surface
water samples from the tributary. One surface water sample was collected from an upstream
location, and one surface water sample was collected from a downstream location. Analytical
results indicate trace concentrations of the polynuclear aromatic hydrocarbons (PAHs)
fluoranthene, naphthalene, phenanthrene, and pyrene were detected in the upstream sample. No
PAHs were detected in the downstream sample. Metals concentrations detected in the
downstream tributary sample were similar or lower to those detected in the upstream tributary
sample.

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3.0 Pond Closure Scope of Work

3.1 Stormwater Permit

The pond closure activities involved land disturbance of an approximately 3.4-acre area.
Therefore, the pond closure activities were subject to stormwater permitting. H&H prepared a
Notice of Intent (NOI) application and developed a Stormwater Pollution Prevention Plan
(SWPPP) for stormwater coverage under General Permit NCG010000. The SWPPP was
prepared in accordance with the requirements of the National Pollutant Discharge Elimination
System (NPDES) program under the provisions of 40 CFR 122.26. H&H received the NPDES
General Permit on April 1, 2019, which expires on March 31, 2024. As part of the NPDES
General Permit, an Erosion and Sediment Control Plan (E&SC Plan) was prepared to manage
stormwater within the disturbance area. The E&SC Plan was approved by DEQ on April 29,
2019 (Project ID: CLEVE-2019-015). H&H contracted with Elite Environmental Services
(Elite) of Clover, South Carolina to perform pond closure activities. Erosion and sediment
control measures were implemented by Elite prior to beginning land clearing and grading
activities.

3.2 Dewatering Activities

Initial pond closure activities consisted of dewatering the remaining stormwater from the ponds
for discharge into the municipal sewer system. Pond dewatering activities were conducted under
Dicey Mill Inc.’s current Industrial User Permit (IUP; No. 1001) with the City of Shelby for
discharge to the First Broad Wastewater Treatment Plant (WWTP) under NPDES No. NC0024538.
Pond #1 and Pond #2 were dry; therefore, no water was discharged to the municipal sewer
system from these ponds. Water in Pond #3 was pumped via an electronic submersible pump
into Pond #4 for discharge to the municipal sewer system. In total, approximately 3,190,000
gallons of water were discharged into the municipal sewer system during pond dewatering.

In accordance with the City of Shelby Sewer Use Ordinance, total suspended solids (TSS) of the

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discharged water did not exceed 250 mg/L. Daily periodic measurements of TSS were collected
by Elite using a TSS meter during dewatering. A series of drum filters were utilized to reduce
TSS prior to discharge to the municipal sewer.

3.3 Clearing and Grading Activities
Concurrent with dewatering activities, vegetation within the 3.4-acre disturbance area was
cleared and removed by Hensley & Sons Tree Service. Downed timber and brush were hauled
off-Site for disposal.

Upon completion of dewatering, land clearing and timber removal, grading and filling activities
began at Pond #1 and moved westward to Pond #3 and Pond #4. The fill material consisted of
the berm walls which were pushed into the fill areas as well as cut soil from within the
disturbance area.

As indicated on the grading plan provided in Appendix A and summarized in the table below,
approximately 1,300 cubic yards (CY) net volume of soil was cut during re-grading activities.
Therefore, imported fill soil was not required to fill the ponds and obtain the desired grades. The
1,300 CY of surplus soil was subsequently thin spread across the disturbance area.

Cut/Fill Volumes Ponds #1 through #3
Area
Pond 4 and Freshwater
Pond Area
Total Volumes
Cut Volume (CY) +1,200 +6,500 +7,700
Fill Volume (CY) -700 -5,700 -6,400
Net Volume (CY) +500 +800 +1,300

Gravel was imported to the Site to aid in filling and for soil stabilization/geotechnical purposes.
The gravel was new (not recycled) and was sourced from an established commercial quarry.
Additionally, the concrete cinderblocks and concrete slab associated with the former freshwater
settling pit were crushed and used along with the imported gravel. To aid with drying and
solidification of Pond #4 sediment, and as approved by DEQ via email dated July 31, 2019,

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approximately 128 tons of 33-Grade Portland cement powder was imported to the Site. The
Portland cement was mixed with the in-situ sediment via a longarm excavator and allowed 48 to
72 hours cure time prior to cover.

Geogrid fencing was utilized as a “marker” and for increased stabilization and was placed on top
of the sediment in Ponds #1, #3, and #4 prior to covering the sediment to serve as an indicator
that impacted sediment is being encountered should excavation occur in the area in the future.
After placement of the “marker”, Ponds #1, #3, and #4 were filled with a minimum two foot
layer of compacted fill material during re-grading. Pond #2 and the Freshwater Pond were not
filled with soil due to the lack of significant impacts identified in the pond sediment.

To ensure positive drainage, the finished surface of each filled pond (Ponds #1, #3, and #4) was
sloped in a gentle southwesterly direction towards the unnamed tributary of the First Broad
River. To prevent rainwater from collecting within Pond #2 and the Freshwater Pond, the
embankments were strategically breached to allow positive drainage in a natural stormwater flow
direction towards the unnamed tributary of the First Broad River.

Following completion of grading activities, the graded and disturbed areas were seeded to
produce an erosion resistant vegetative cover and the temporary erosion controls were removed.
Note that perimeter silt fencing remains in-place until a minimum 80% vegetative cover has been
established and the NPDES General Permit is closed.

3.4 Site Contingency Activities

In accordance with the Site Contingency Plan outlined in the DEQ-approved Work Plan, H&H
personnel was on-Site to document initial pond closure activities. Once pond closure and
grading activities progressed, H&H provided field oversight on an approximate once a week
basis. H&H also remained on call and available on an as-needed basis should potential issues
have arisen.

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H&H received notification of one such issue on June 13, 2019 as documented in the WWTP
Upset, Spill, or Bypass Event Summary Letter dated July 17, 2019. As part of the planned
closure of Pond #4, two outlet spillways were constructed on the southwest and south-central
portions of Pond #4 to allow stormwater to discharge from the pond during closure activities.
Per the DEQ-approved E&SC Plan, stormwater discharged during grading activities was
intended to pass through a series of sediment controls and ultimately a sediment fence before
leaving the disturbance area. The south-central spillway appears to have been cut too deep on
June 10, 2019; which allowed suspended sediment in Pond #4 to be discharged along with the
stormwater. The suspended pond sediment flowed downgradient in a southwesterly direction
towards an unnamed tributary of the First Broad River. Sediment and erosion control measures
located downgradient of the south-central spillway subsequently failed resulting in the release of
a portion of the pond sediment outside the disturbance area.

The downgradient portion of the sediment flow path migrated outside the disturbance area and
entered the unnamed tributary to the First Broad River, located along the southern Site boundary
and approximately 240 ft southwest of Pond #4. The south-central spillway was closed on June
13, 2019 to allow for repairs to the existing sediment control measures and the installation of
additional sediment control measures, including a series of sediment tubes, straw swales, two
sediment detention ponds, and a sediment filter sack.

On June 14, 2019, H&H personnel met Mr. Andrew Pitner of the DEQ Division of Water
Resources (DWR) and Ms. Jordan Thompson of the DEQ Brownfields Program at the Site to
survey the extent of the release, determine a remediation strategy, and devise a sampling plan to
assess the potential for impact to the unnamed tributary from the sediment discharge.

Based on the June 14, 2019 meeting, the extent of sediment migration observed in the on-Site
unnamed tributary was determined to encompass an approximate 300 ft section of the creek. The
First Broad River was not observed to have been impacted by the sediment release. To evaluate
the potential for impact to sediment and surface water in the on-Site tributary, H&H collected
three sediment and three surface water samples from the unnamed tributary to the First Broad

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River for laboratory analysis of VOCs by EPA Method 8260, semi-volatile organic compounds
(SVOCs) by EPA Method 8270, and hazardous substance list (HSL) metals by EPA Methods
6020/7471. Additionally, surface water samples were collected for laboratory analysis of pH
(EPA Method SM 4500) and hardness (EPA Method 200.7). Figures and summary data tables
from previous Brownfield assessments are provided in Appendix C.

Pond #4 sediment observed in the on-Site tributary stream bed between the determined outfall
and termination points was removed using hand tools on June 17 and 18, 2019 and placed back
into Pond #4. Additionally, Pond #4 sediment observed deposited inside the disturbance area
and outside the disturbance area (prior to reaching the creek) was removed utilizing a skid-steer
and hand tools on June 17, 2019 and placed back into Pond #4. In total, approximately 0.25
cubic yards of sediment was recovered and returned to Pond #4 to be subsequently covered with
the “marker” and clean soil cap.

Laboratory analytical results of the surface water samples collected from the on-Site unnamed
tributary indicated that VOCs, SVOCs, and metals were not detected in any of the samples at
concentrations above 2B Standards for Class C waters. The laboratory analysis of pH and total
hardness were within the range of Site-specific background. The laboratory analytical results for
the sediment samples collected from the on-Site unnamed tributary stream bed indicated that
VOCs, SVOCs, and metals were not detected at concentrations above PSRGs and background
for metals.

Based on the results of the unnamed tributary sediment and surface water sampling event, the
tributary did not appear to have been significantly impacted by the suspended sediment release
from Pond #4.

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4.0 Additional Brownfields Assessment Activities

The additional assessment activities were performed in general accordance with the DEQ –
IHSB Guidelines for Assessment and Cleanup dated October 2015 and most recent version of the
U.S. EPA Region IV Science and Ecosystem Support (SESD) Field Branches Quality System
and Technical Procedures guidance, the DEQ-approved Pond Closure Work Plan Revision-1
dated August 9, 2018 and the DEQ-approved Brownfields Assessment Work Plan dated July 21,
2017.

H&H conducted additional Brownfields assessment activities at the Site between September 9
and September 16, 2019. A discussion of the methods, analytical results, and conclusions of the
additional Brownfields assessment activities are provided in the following sections.

4.1 Final Grade Soil Sampling

Following completion of pond closure and grading activities, H&H conducted representative
final grade soil sampling from within the areas of the closed ponds (Ponds #1, #3, and #4). One
composite sample was collected from each of Pond #1 and #3 and three composite samples from
Pond #4. Each composite sample consisted of five sample aliquots collected from 0 to 2 ft below
ground surface (bgs) from the former pond locations. The shallow soil borings were advanced
using a decontaminated hand auger and the soil from the borings was field screened for the
presence of odor, staining, and elevated photoionization detector (PID) readings. The sample
aliquots were collected from representative locations within the ponds and field-composited
using a decontaminated stainless-steel mixing bowl and spoon. Samples collected for VOC
analysis were grab samples collected from the sample aliquot most indicative of potential impact
based on field screening results. PID results were low (< 5 ppm) and did not indicate significant
impact. Furthermore, indications of odors or staining were not observed. Therefore, VOC
samples were collected from the centrally located aliquot sample from each composite sample
area.

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Following sample collection, the samples were submitted to a North Carolina certified laboratory
for analysis of VOCs by EPA Method 8260, SVOCs by EPA Method 8270, and Resource
Conservation and Recovery Act (RCRA) metals by EPA Methods 6020/7471. The RCRA
metals include arsenic, barium, cadmium, chromium, lead, mercury, selenium, and silver. The
locations of the final grade composite samples are presented on Figure 2.

4.2 Groundwater Sampling

H&H conducted a groundwater sampling event at the Site on September 9, 2019 that included
existing monitor wells MW-1 through MW-4. Prior to sampling, depth-to-water measurements
were collected from the top-of-casing utilizing a decontaminated electronic water level indicator.
Well locations are depicted on Figure 2.

A bladder pump with new dedicated tubing was used to purge and sample each well using low
flow purging and sampling methods. The bladder pump was placed in the approximate mid-
portion of the saturated screened interval of the well. During purging, field measurements of pH,
specific conductivity, temperature, dissolved oxygen (DO), and oxidation reduction potential
(ORP) were measured with a YSI Pro Plus water quality meter equipped with a flow-through
cell, and turbidity was measured using a Hach 2100Q turbidity meter. Water levels were
measured during the purging process to ensure the pump rate did not cause significant drawdown
of the water column, and samples were collected following stabilization of field parameters.

Once stabilization was reached, groundwater samples were collected using low-flow sampling
techniques and for VOCs, the “soda-straw” method. Geochemical parameters were collected at
the time of groundwater sample collection and are summarized in Table 1.

Following sample collection, samples were submitted to Pace Analytical Services, LLC (Pace)
for analysis of VOCs by EPA Method 8260, SVOCs by EPA Method 8270, and HSL metals by
EPA Methods 6020/7470/7471. The HSL metals include antimony, arsenic, beryllium,

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cadmium, chromium, copper, lead, manganese, mercury, nickel, selenium, silver, thallium, and
zinc.

4.3 Groundwater Flow and Hydraulic Gradients

The top of casing elevations of the four permanent monitoring wells were previously determined
using survey techniques, which were referenced to an arbitrary datum of 100.00 ft at the MW-1
top of casing.

A summary of well construction and groundwater elevation data is provided in Table 2. A
shallow aquifer potentiometric map generated from the water table elevations is provided as
Figure 3. As indicated on the figure, the general direction of shallow groundwater flow in the
investigation area is to the west towards the First Broad River.

4.4 Quality Assurance/Quality Control
H&H utilized standard quality assurance/quality control (QA/QC) processes during the
additional Brownfields assessment activities. Non-dedicated sampling equipment, including the
hand auger, the mixing bowl and spoon, and the water level meter were decontaminated using
Liquinox® detergent prior to and between each sampling location. H&H wore nitrile gloves
while handling samples, and the groundwater samples were collected using dedicated tubing.
Soil and groundwater samples were collected in laboratory-provided containers and placed on ice
immediately upon collection.

For field and laboratory QA/QC purposes, H&H collected one duplicate groundwater sample
(DUP-4) from monitoring well MW-3. The duplicate sample was analyzed for the same
compounds as the parent sample. The results of analysis of the duplicate sample is provided in
Table 4 and indicate good analytical repeatability for the duplicate sample.

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5.0 Analytical Laboratory Results

The results of analysis of the composite soil samples are summarized in Table 3, the results of
analysis of the groundwater samples are summarized in Table 4. Laboratory analytical data
reports and chain-of-custody records are included in Appendix B.

5.1 Soil Analytical Results

Soil analytical results were compared to the DEQ IHSB Soil to Water, Residential, and
Industrial/Commercial PSRGs dated May 2019. Metals concentrations were first compared to
Site specific background levels and published regional background levels for North Carolina
soils before comparison to the PSRGs.

VOCs
Laboratory analytical results indicate that multiple petroleum-related compounds were detected
in each of the former Ponds #1, #3, and #4 locations at trace levels above laboratory method
detection limits, but below PSRGs. No VOCs were detected at concentrations above PSRGs.

SVOCs
Laboratory analytical results indicate that no SVOCs were detected in any of the composite soil
samples at concentrations above laboratory method detection limits.

Metals
The results of the metals analyses indicate that arsenic was detected in each of the composite
samples at concentrations ranging from 3.61 mg/kg to 7.43 mg/kg, which are generally within
the range of Site-specific background (4.2 mg/kg to 5.2 mg/kg) and are within the range of
published regional background levels for North Carolina soils. Several of the arsenic detections
are above PSRGs. Although the arsenic detections are above PSRGs, they are generally similar
in concentration and are consistent with background levels. No other metals were detected at

16
S:\AAA-Master Projects\Dicey Mills - DCY\Pond Closure\Final Report\Pond Closure and Add BF Asmnt Report.doc
concentrations above PSRGs.

5.2 Groundwater Analytical Results

Laboratory analytical results were compared to the 2L Standards, the DEQ IMACs (if a 2L
Standard is not established), and the DEQ DWM Non-Residential Groundwater Vapor Intrusion
Screening Levels (VISLs).

VOCs
Laboratory analytical results indicate that TCE was detected in groundwater samples from MW-
1 (40.6 µg/L) and MW-4 (3.5 µg/L) at concentrations above the 2L Standard of 3 µg/L and the
Non-Residential VISL of 4.4 µg/L. Monitoring well MW-1 is located downgradient of the
former manufacturing building and MW-4 is located downgradient of Pond #4. No other VOCs
were detected at concentrations exceeding 2L Standards or Non-Residential VISLs.

SVOCs
Analytical results indicate that no SVOCs were detected in any of the groundwater samples at
concentrations above laboratory method detection limits.

Metals
Analytical results indicate that the metals manganese and thallium were detected at
concentrations exceeding 2L Standards. Manganese was detected at concentrations of 65.8 µg/L
(MW-1) and 221 µg/L (MW-2), which exceed the 2L Standard of 50 µg/L. Manganese is
frequently detected above the 2L Standard in groundwater within the Piedmont of North
Carolina. Because a background groundwater sample was not collected, it is not possible to
evaluate if the detected manganese concentrations are associated with potential Site impacts or
background.

Thallium was detected in one sample (MW-2, downgradient of the dye house) at an estimated
concentration of 0.236 J µg/L, which slightly exceeds the IMAC of 0.2 µg/L. As indicated in

17
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Table 1 and Table 4, turbidity was low (< 10 NTU) in all of the groundwater samples including
MW-1 (turbidity of 5.4 NTU) and MW-2 (turbidity of 9.8 NTU); therefore, it is unlikely that the
manganese and thallium concentrations are associated with suspended sediment in the samples.

6.0 Summary and Conclusions

H&H has completed pond closure and additional Brownfields assessment activities at the former
Dicey Mills facility located at 430 Neisler Street in Shelby, Cleveland County, North Carolina.
A brief summary of the closure activities and the results of the additional assessment activities
are provided below.

• In accordance with the DEQ-approved Work Plan, Pond #1, Pond #3, and Pond #4 were
closed in-place and capped with clean soil. Pond closure activities included obtaining a
stormwater permit, dewatering existing stormwater in Pond #3 and Pond #4, clearing the
3.4-acre disturbance area, covering impacted sediment with a “marker” to serve as an
indicator that impacted sediment is being encountered should excavation occur in the area
in the future, re-grading the disturbance area to fill the former ponds in-place, and
covering the former ponds with a minimum two ft thick soil cap.

• The results of the groundwater assessment indicate that TCE is the primary compound
above the 2L Standard in groundwater and was detected downgradient of the former
manufacturing building and Pond #4. Comparison of the data from the October 2017
sampling event to the September 2019 sampling event indicate that TCE concentrations
in groundwater may be increasing slightly in the central portion of the Site (from 9.5
µg/L to 40.6 µg/L) and may be decreasing in the western portion of the Site (from 110
µg/L to 32.5 µg/L). However, a contaminant trend cannot be established at this time
based on the limited analytical database for the Site.

• The results of the final grade sampling did not indicate impact above PSRGs and
background levels for metals.

18
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• Previous sub-slab soil vapor and indoor air assessment has indicated that there is not a
significant risk for exposure to building occupants. Further, based upon the relatively
low concentration of TCE detected in MW-4 and the distance to the First Broad River
from MW-4 (approximately 850 ft), the potential for impact to the river from the Site
groundwater appears to be low.

• Although impacts are present in groundwater in the central and western portions of the
Site, based on the results of the previous surface water sampling events conducted in
October 2017 and June 2019, the groundwater impacts have not resulted in impact to the
surface water in the unnamed tributary along the southern portion of the Site.

Tables
Table 1Summary of Groundwater Geochemical Data Former Dicey MillsShelby, North CarolinaH&H Job No. DCY-001Sample IDMW-1 MW-2 MW-3 MW-4Sample Date9/9/2019 9/9/2019 9/9/2019 9/9/2019ParameterpH (SU)4.2 4.96 4.82 5.36Temperature (°C)26.5 18.4 18.6 17.9Specific Conductivity (µS/cm)98.1259.4 100.1 111.6Dissolved Oxygen (mg/L) 5.15 5.61 2.45 5.30Oxidation Reduction Potential (mV) 188.2 153.8 156.7 137.5Turbidity (NTU)5.4 9.8 5.3 7.8Notes:mg/L = milligrams per literµS/cm = microsiemens per centimeter; SU = standard unitsmV = millivolts; NTU = nephelometric turbidity unitsS:\AAA-Master Projects\Dicey Mills - DCY\Brownfields\Tables\Analytical Data Tables11/1/2019Table 1 (Page 1 of 1)Hart & Hickman, PC
Table 2Summary of Well Construction and Groundwater Elevation Data Former Dicey Mills Shelby, North Carolina H&H Job No. DCY-001MW-1 10/10/2017 Shallow 100.0047237 - 4736.8063.20MW-2 10/11/2017 Shallow 103.1948238 - 4839.2263.97MW-3 10/10/2017 Shallow76.1228218 - 2821.0155.11MW-4 10/10/2017 Shallow69.0030220 - 3025.7143.29Notes:MW = permanent monitoring well; TOC = top of casing; ft = feetDepth to groundwater measurements collected on 9/9/2019*Elevations are approximate and are referenced to an arbitrary datum of 100.00 ft at MW-1Groundwater Elevation*Well ID Date InstalledTotal Well Depth (ft below TOC)Well Diameter (inches)Screen Interval (ft)Static Depth to Water (ft below TOC)Screened ZoneTOC Elevation (ft)S:\AAA-Master Projects\Dicey Mills - DCY\Brownfields\Tables\Analytical Data Tables11/1/2019Table 2 (Page 1 of 1)Hart & Hickman, PC
Table 3Summary of Soil Analytical Data - Final Grade Samples Former Dicey MillsShelby, North CarolinaH&H Job No. DCY-001LocationPond 1 Pond 3Sample IDP1 P3 P4A P4B P4CBackground-1 Background-2Date9/16/2019 9/16/2019 9/16/2019 9/16/2019 9/16/20198/12/2016 8/12/2016Depth (ft)**0-2 0-2 0-2 0-2 0-2 Range Mean 0-2 0-2VOCs (8260) mg/kgEthylbenzene1.2 J2.5 J1.4 J<5.5<5.9136.127----NANAToluene6.0 D64.2 J<6.5<5.51.9 J8.39909,700----NANAm&p-Xylene3.9 J8.5 J<13.0<11.13.4 J9.8120500----NANAo-Xylene1.6 J3.2 J<6.5<5.51.5 J9.8140590----NANASVOCs (8270) mg/kgNDNDNDNDND----------NANAMetals (6020/7471) mg/kgArsenic7.437.215.713.616.255.80.683.01.0 - 184.84.25.2Barium88.610510380.395.45803,10047,000 50 - 1,000 356NANACadmium0.0959 J<0.561 <0.589 <0.586 <0.5603.0142001.0 - 10* 4.3<0.55<0.60Chromium83.810195.010988.7360,00023,000350,000 7.0 - 300 651828Lead4.484.4511.410.59.37270400800ND - 50162025Mercury0.0109 J 0.00896 J 0.0132 J 0.0168 J 0.00680 J1.02.39.7 0.03 - 0.52 0.1210.0520.037Selenium<0.570 <0.5610.6430.7070.393 J2.1781,160 <0.1 - 0.8 0.42<1.2<1.3Silver<0.570 <0.561 <0.589 <0.586 <0.5603.4781,200 ND - 5.0 NS0.042 J0.052 JNotes:1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB)Preliminary Soil Remediation Goals (PSRGs) (May 2019)2) Range and mean values of background metals for North Carolina soils taken from Elements inNorth American Soils by Dragun and Chekiri, 2005* = Range and mean values of background metals for Southeastern USA soils** = VOC samples collected as grab samples from within specified depth intervalSoil concentrations are reported in milligrams per kilogram (mg/kg)Laboratory analytical methods are shown in parenthesesLess than values indicate laboratory reporting limitsND = Not Detected; VOCs = Volatile Organic Compounds; SVOCs = Semi-VOCsNA = Not Analyzed; NE = Not Established; -- = Not Applicable; NS = Not SpecifiedJ = Estimated concentration between laboratory method detection limit and reporting limitD6 = The precision between the sample and laboratory duplicate sample exceeded control limitPond 4Screening Criteria (1)BackgroundProtection of Groundwater PSRGsResidential PSRGsIndustrial/ Commercial PSRGsRegional Background Metals in Soil (2)S:\AAA-Master Projects\Dicey Mills - DCY\Brownfields\Tables\Analytical Data Tables11/1/2019Table 3 (Page 1 of 1)Hart & Hickman, PC
Table 4Summary of Groundwater Analytical Data Former Dicey MillsShelby, North CarolinaH&H Job No. DCY-001Area of ConcernSample IDMW-1 DUP-3 MW-1DUP-4Date10/12/2017 10/12/2017 9/9/2019 10/13/2017 9/9/2019 10/12/2017 9/9/2019 9/9/2019 10/12/2017 9/9/2019VOCs (8260) µg/LAcetone6,00019,000,000<50<50<25<50<25<50<25<25<50<25Chloroform70360.28 J<2.0<5.01.3 J<5.0<2.0<5.0<5.00.85 J<5.01,4-Dichlorobenzene6110<1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0cis-1,2-DichloroethyleneNE<1.0 <1.02.6<1.0 <1.0 <1.0 <1.0 <1.0 <1.00.72 JToluene60016,0000.25 J 0.27 J<1.00.69 J<1.0<1.0<1.0<1.0<1.0<1.0Trichloroethylene34.47.69.540.6<1.0<1.00.50 J<1.0<1.011032.5SVOCs (8270) µg/L----BRLBRLBRLBRLBRLBRLBRLBRLBRLBRLMetals (6020/7470/7471) µg/LAntimony1*NE<2.0<2.0<2.00.20 J<2.00.21 J<2.0<2.0<2.0<2.0ArsenicNE<2.0<2.0<2.0<2.0<2.0<2.0<2.0<2.0<2.0<2.0Beryllium4*NE0.57 J 0.57 J 0.625 J 0.48 J 0.382 J<0.80<2.0<2.0<0.80<2.0Cadmium2NE<1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0<1.0Chromium10NE1.5 J1.3 J1.17 J30.907 J 1.2 J1.13 J 0.821 J 1.3 J<2.0Copper1,000NE6.4 J6.6 J 0.632 J221.29 J<101.35 J 0.528 J<100.568 JLead15NE0.84 J 0.83 J 0.933 J51.10 J<2.00.858 J 0.702 J<2.00.894 JManganese50NE18017065.8990221357.486.2911012.4Mercury10.750.039 J 0.040 J<0.20.039 J<0.20.038 J<0.2<0.20.039 J<0.2Nickel100NE1.2 J3.6 J 0.983 J 3.6 J<2.01.2 J<2.0<2.01.6 J<2.0Thallium0.2*NE<0.40<0.40<2.00.21 J 0.236 J<0.40<2.0<2.0<0.40<2.0Zinc1,000NE20 J239.60 J1703.78 J<20<25<25<202.70 JTurbidity (NTU)----5.48.19.83.88.57.8Notes:1) North Carolina 15A NCAC 02L Groundwater Standards (2L Standards) (April 2013)2) North Carolina Department of Environmental Quality (DEQ) - Division of Waste Management (DWM)Non-Residential Vapor Intrusion Groundwater Screening Levels (GWSLs; dated February 2018)* = 2L Standard is not established; therefore Interim Maximum Allowable Concentrations (IMACs) are shownConcentrations are reported in micrograms per liter (µg/L)Laboratory analytical methods are shown in parenthesesBold values exceed a 2L Standard (April 2013)Underlined values exceed the Non-Residential GWSLsJ = estimated value between the laboratory detection limit and the laboratory reporting limitBRL = Below Reporting Limit; VOCs = Volatile Organic Compounds; SVOCs = Semi-Volatile Organic Compounds-- = Not Applicable; NS = Not Specified; NTU = Nephelometric Turbidity UnitNon-detect values indicate laboratory reporting limitDowngradient of Former Dye HouseWest of Central Portion of Former Manufacturing BuildingMW-2 MW-3 MW-45.3North Carolina 2L Groundwater Standards (1)Non-Residential GWSLs (2)8.1Downgradient of Pond #4Downgradient of Pond #3S:\AAA-Master Projects\Dicey Mills - DCY\Brownfields\Tables\Analytical Data Tables11/1/2019Table 4 (Page 1 of 1)Hart & Hickman, PC1070

Figures
SITE LOCATION MAP
FORMER DICEY MILLS430 NEISLER STREETSHELBY, NORTH CAROLINA
DATE:
JOB NO:
REVISION NO:
FIGURE NO:
6/15/2016 0
1DCY-001
0 2000 4000
APPROXIMATE
SCALE IN FEET
N
U.S.G.S. QUADRANGLE MAP7.5 MINUTE SERIES (TOPOGRAPHIC)
2923 S. Tryon Street, Suite 100Charlotte, NC 28203704.586.0007(p) 704.586.0373(f)
SHELBY, NORTH CAROLINA 2002
SITE
I
N
T
E
RM
I
T
T
E
N
T

S
T
R
E
AM
HHSB-1
MW-1
MW-2
MW-3
MW-4
LEGEND
SITE PROPERTY BOUNDARY
HIGH-TENSION POWER LINES
ABOVEGROUND STORAGE TANK
UNDERGROUND STORAGE TANK
(CLOSED IN-PLACE)
SOIL BORING LOCATION
TYPE II MONITORING WELL
LOCATION
POST-CLOSURE COMPOSITE
SAMPLE
JOB NO. DCY-001
REVISION NO. 0DATE: 10-30-19
FIGURE NO. 2
FORMER DICEY MILLS
430 NEISLER STREET
SHELBY, NORTH CAROLINA
SITE MAP W.
D
I
XO
N

B
OU
L
E
V
A
RD
NEISLER STREETMELODY LANEFIRST BROAD RIVER2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
POND #3: FORMER PROCESS WATER
(CLOSED IN-PLACE)
POND #2: FORMER PROCESS WATER (BREACHED)
POND #1: FORMER PROCESS WATER (CLOSED IN-PLACE)
FORMER FRESHWATER POND
(BREACHED)POND HOUSE
FORMER FABRIC
PRINTING OPERATION
POND 4: FORMER PROCESS WATER
(CLOSED IN-PLACE)
OUT-OF-USE VARSOL AST
VACANT STORAGE BUILDING
OUTFALL PIPE
FORMER MAINTENANCE SHOP
FORMER DYEHOUSE
FORMER FUEL OIL
UST & GASOLINE UST
OUT-OF-USE
FUEL OIL AST
FORMER WEAVING/SPINNING OPERATION
OUT-OF-USE
WASTE OIL AST
FORMER MANUFACTURING BUILDING
TRANSFORMER SUBSTATION
OUT-OF-USE FUEL OIL UST
P4C
P4B
P4A
P3
P1
S:\AAA-Master Projects\Dicey Mills - DCY\Phase II ESA\Figures\Figures.dwg, FIG 2, 10/30/2019 11:09:17 AM, sperry
I
N
T
E
RM
I
T
T
E
N
T

S
T
R
E
AM
MW-1
MW-2
MW-3
MW-4
(63.20)
(55.11)
(43.29)45505560(63.97)
LEGEND
SITE PROPERTY BOUNDARY
TYPE II MONITORING WELL LOCATION
GROUNDWATER ELEVATION (FT)
GROUNDWATER ELEVATION CONTOUR
(FT)
INFERRED GROUNDWATER FLOW
DIRECTION
JOB NO. DCY-001
REVISION NO. 0DATE: 10-30-19
FIGURE NO. 3
FORMER DICEY MILLS
430 NEISLER STREET
SHELBY, NORTH CAROLINA
SHALLOW GROUNDWATER
POTENTIOMETRIC MAPW.
D
I
X
ON

BO
U
L
E
V
AR
D
NEISLER STREETMELODY LANEFIRST BROAD RIVER2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
NOTES:
1. ELEVATIONS ARE APPROXIMATE & BASED ON AN
ARBITRARY DATUM OF 100.00 FT AT MW-1.
2. GROUNDWATER ELEVATIONS COLLECTED ON 9/9/19.
(63.20)
41
POND #3: FORMER PROCESS WATER
(CLOSED IN-PLACE)
POND #2: FORMER PROCESS WATER (BREACHED)
POND #1: FORMER PROCESS WATER (CLOSED IN-PLACE)
FORMER FRESHWATER POND
(BREACHED)
POND 4: FORMER PROCESS WATER
(CLOSED IN-PLACE)S:\AAA-Master Projects\Dicey Mills - DCY\Phase II ESA\Figures\Figures.dwg, FIG 4, 10/30/2019 11:40:01 AM, sperry

Appendix A Grading Plan
195.5195194
1
9
3
.
5
1
9
3192.5192191.51911
9
0
196194.5189.51
9
8
1
9
7196.5190.5200.5199200199.5187.5186.5
18
6
18
5
18
4
.
5
1
8
4183.5183182.51
8
1
.
5181180.5180179.517918
5
.
5
182189
188.5
201.5196186
185.5
185
184.5
184.5
184
183.5
183186185
202201188187.5185.5
185
1
8
0
1
7
9
.
5 201.520119
8
.
5
197.5
188
18
7178.519
7182.5183.5201.5
188.518
0
.
5
1
9
1
.
5
19118918
6
201199.5198
196192
189.5
189188.5187.51
8
6
.
5
186.5186185
184.
5
18
2
.
5
179
191
NC Center for Geographic Information & Analysis
Document Path: S:\AAA-Master Projects\Dicey Mills - DCY\Pond Closure\Erosion & Sediment Control Plan\GIS Model\Pond Breaching Regrading Plan.mxdPond Breaching Regrading PlanLEGEND
Current Elevation (m)
1m contours
0.5m contours
Grading Plan (m)
1m contours
0.5m contours
Cut/Fill
2 - 3.75 m fill
1 - 2 m fill
0 - 1 m fill
No Fill
0 - 1.5 m cut
1.5 - 3 m cut
Site Property Boundary
Ponds
Streams
GRADING PLAN
FORMER DICEY MILLS430 NEISLER STREET
SHELBY, NORTH CAROLINA
DATE: 11-1-2019
JOB NO. DCY-001
REVISION NO. 0
FIGURE NO. 3
U
0 60 12030
Feet
2923 South Tryon Street - Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License #C-1269 / #C-245 Geology1":60'
POND 4
FRESHWATERPOND
POND 3
POND 2
POND 1
Overall:Pond 4 and FW Pond Area: Ponds 1-3 Area:
Cut: 7,700 cy Cut: 6,500 cy Cut: 1,200 cy
Fill: 6,400 cy Fill: 5,700 cy Fill: 700 cy
Net: 1,300 cy cut Net: 800 cy net Net: 500 cy cut

Appendix B
Laboratory Analytical Reports
#=CL#
September 17, 2019
LIMS USE: FR - BRETT LAWRENCE
LIMS OBJECT ID: 92444875
92444875
Project:
Pace Project No.:
RE:
Brett Lawrence
Hart & Hickman
2923 South Tryon St.
Suite 100
Charlotte, NC 28203
DCY.001
Dear Brett Lawrence:
Enclosed are the analytical results for sample(s) received by the laboratory on September 10, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager
1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 1 of 45
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92444875
DCY.001
Pace Analytical National Certification IDs
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 45
#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92444875
DCY.001
Lab ID Sample ID Matrix Date Collected Date Received
92444875001 MW-1 Water 09/09/19 15:20 09/10/19 07:11
92444875002 MW-2 Water 09/09/19 15:55 09/10/19 07:11
92444875003 MW-3 Water 09/09/19 13:10 09/10/19 07:11
92444875004 MW-4 Water 09/09/19 10:55 09/10/19 07:11
92444875005 DUP-4 Water 09/09/19 00:00 09/10/19 07:11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 3 of 45
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92444875
DCY.001
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92444875001 MW-1 EPA 6020B 12 PANLD
EPA 7470A 1 PANTCT
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92444875002 MW-2 EPA 6020B 12 PANLD
EPA 7470A 1 PANTCT
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92444875003 MW-3 EPA 6020B 12 PANLD
EPA 7470A 1 PANTCT
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92444875004 MW-4 EPA 6020B 12 PANLD
EPA 7470A 1 PANTCT
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
92444875005 DUP-4 EPA 6020B 12 PANLD
EPA 7470A 1 PANTCT
EPA 8270E 74 PASI-CPKS
EPA 8260D 63 PASI-CSAS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
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[phone]
Page 4 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92444875
DCY.001
Sample: MW-1 Lab ID: 92444875001 Collected: 09/09/19 15:20 Received: 09/10/19 07:11 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015Metals (ICPMS) 6020B
Antimony ND ug/L 09/14/19 16:24 7440-36-009/14/19 12:402.00 0.754 1
Arsenic ND ug/L 09/14/19 16:24 7440-38-209/14/19 12:402.00 0.250 1
Beryllium 0.625J ug/L 09/14/19 16:24 7440-41-7 J09/14/19 12:402.00 0.120 1
Cadmium ND ug/L 09/14/19 16:24 7440-43-909/14/19 12:401.00 0.160 1
Chromium 1.17J ug/L 09/14/19 16:24 7440-47-3 B,J09/14/19 12:402.00 0.540 1
Copper 0.632J ug/L 09/14/19 16:24 7440-50-8 B,J09/14/19 12:405.00 0.520 1
Lead 0.933J ug/L 09/14/19 16:24 7439-92-1 B,J09/14/19 12:402.00 0.240 1
Manganese 65.8 ug/L 09/14/19 16:24 7439-96-509/14/19 12:405.00 0.250 1
Nickel 0.983J ug/L 09/14/19 16:24 7440-02-0 J09/14/19 12:402.00 0.350 1
Silver ND ug/L 09/14/19 16:24 7440-22-409/14/19 12:402.00 0.310 1
Thallium ND ug/L 09/14/19 16:24 7440-28-009/14/19 12:402.00 0.190 1
Zinc 9.60J ug/L 09/14/19 16:24 7440-66-6 J09/14/19 12:4025.0 2.56 1
Analytical Method: EPA 7470A Preparation Method: 7470AMercury 7470A
Mercury ND ug/L 09/15/19 20:41 7439-97-609/13/19 10:370.200 0.0490 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 09/11/19 17:58 83-32-909/11/19 13:2410.0 1.6 1
Acenaphthylene ND ug/L 09/11/19 17:58 208-96-809/11/19 13:2410.0 1.6 1
Aniline ND ug/L 09/11/19 17:58 62-53-309/11/19 13:2410.0 1.9 1
Anthracene ND ug/L 09/11/19 17:58 120-12-709/11/19 13:2410.0 1.7 1
Benzo(a)anthracene ND ug/L 09/11/19 17:58 56-55-309/11/19 13:2410.0 1.8 1
Benzo(a)pyrene ND ug/L 09/11/19 17:58 50-32-809/11/19 13:2410.0 2.1 1
Benzo(b)fluoranthene ND ug/L 09/11/19 17:58 205-99-209/11/19 13:2410.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 09/11/19 17:58 191-24-209/11/19 13:2410.0 1.4 1
Benzo(k)fluoranthene ND ug/L 09/11/19 17:58 207-08-909/11/19 13:2410.0 1.9 1
Benzoic Acid ND ug/L 09/11/19 17:58 65-85-009/11/19 13:2450.0 43.0 1
Benzyl alcohol ND ug/L 09/11/19 17:58 100-51-609/11/19 13:2420.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 09/11/19 17:58 101-55-309/11/19 13:2410.0 1.6 1
Butylbenzylphthalate ND ug/L 09/11/19 17:58 85-68-709/11/19 13:2410.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 09/11/19 17:58 59-50-709/11/19 13:2420.0 2.8 1
4-Chloroaniline ND ug/L 09/11/19 17:58 106-47-809/11/19 13:2420.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 09/11/19 17:58 111-91-109/11/19 13:2410.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/11/19 17:58 111-44-409/11/19 13:2410.0 1.8 1
2-Chloronaphthalene ND ug/L 09/11/19 17:58 91-58-709/11/19 13:2410.0 1.5 1
2-Chlorophenol ND ug/L 09/11/19 17:58 95-57-809/11/19 13:2410.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/11/19 17:58 7005-72-309/11/19 13:2410.0 1.6 1
Chrysene ND ug/L 09/11/19 17:58 218-01-909/11/19 13:2410.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 09/11/19 17:58 53-70-309/11/19 13:2410.0 1.6 1
Dibenzofuran ND ug/L 09/11/19 17:58 132-64-909/11/19 13:2410.0 1.5 1
1,2-Dichlorobenzene ND ug/L 09/11/19 17:58 95-50-109/11/19 13:2410.0 1.3 1
1,3-Dichlorobenzene ND ug/L 09/11/19 17:58 541-73-109/11/19 13:2410.0 1.5 1
1,4-Dichlorobenzene ND ug/L 09/11/19 17:58 106-46-709/11/19 13:2410.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/11/19 17:58 91-94-109/11/19 13:2420.0 3.0 1
2,4-Dichlorophenol ND ug/L 09/11/19 17:58 120-83-209/11/19 13:2410.0 1.4 1
Diethylphthalate ND ug/L 09/11/19 17:58 84-66-209/11/19 13:2410.0 2.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
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9800 Kincey Ave. Suite 100
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Page 5 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92444875
DCY.001
Sample: MW-1 Lab ID: 92444875001 Collected: 09/09/19 15:20 Received: 09/10/19 07:11 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dimethylphenol ND ug/L 09/11/19 17:58 105-67-909/11/19 13:2410.0 1.4 1
Dimethylphthalate ND ug/L 09/11/19 17:58 131-11-309/11/19 13:2410.0 1.6 1
Di-n-butylphthalate ND ug/L 09/11/19 17:58 84-74-209/11/19 13:2410.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 09/11/19 17:58 534-52-109/11/19 13:2420.0 15.2 1
2,4-Dinitrophenol ND ug/L 09/11/19 17:58 51-28-509/11/19 13:2450.0 40.5 1
2,4-Dinitrotoluene ND ug/L 09/11/19 17:58 121-14-209/11/19 13:2410.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/11/19 17:58 606-20-209/11/19 13:2410.0 1.4 1
Di-n-octylphthalate ND ug/L 09/11/19 17:58 117-84-009/11/19 13:2410.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/11/19 17:58 117-81-709/11/19 13:246.0 2.1 1
Fluoranthene ND ug/L 09/11/19 17:58 206-44-009/11/19 13:2410.0 1.7 1
Fluorene ND ug/L 09/11/19 17:58 86-73-709/11/19 13:2410.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 09/11/19 17:58 87-68-309/11/19 13:2410.0 2.0 1
Hexachlorobenzene ND ug/L 09/11/19 17:58 118-74-109/11/19 13:2410.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 09/11/19 17:58 77-47-409/11/19 13:2410.0 1.7 1
Hexachloroethane ND ug/L 09/11/19 17:58 67-72-109/11/19 13:2410.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/11/19 17:58 193-39-509/11/19 13:2410.0 1.6 1
Isophorone ND ug/L 09/11/19 17:58 78-59-109/11/19 13:2410.0 1.6 1
1-Methylnaphthalene ND ug/L 09/11/19 17:58 90-12-009/11/19 13:2410.0 1.4 1
2-Methylnaphthalene ND ug/L 09/11/19 17:58 91-57-609/11/19 13:2410.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 09/11/19 17:58 95-48-709/11/19 13:2410.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/11/19 17:58 15831-10-409/11/19 13:2410.0 1.2 1
Naphthalene ND ug/L 09/11/19 17:58 91-20-309/11/19 13:2410.0 1.4 1
2-Nitroaniline ND ug/L 09/11/19 17:58 88-74-409/11/19 13:2420.0 4.2 1
3-Nitroaniline ND ug/L 09/11/19 17:58 99-09-209/11/19 13:2420.0 2.3 1
4-Nitroaniline ND ug/L 09/11/19 17:58 100-01-609/11/19 13:2420.0 2.2 1
Nitrobenzene ND ug/L 09/11/19 17:58 98-95-309/11/19 13:2410.0 2.1 1
2-Nitrophenol ND ug/L 09/11/19 17:58 88-75-509/11/19 13:2410.0 1.4 1
4-Nitrophenol ND ug/L 09/11/19 17:58 100-02-709/11/19 13:2450.0 3.5 1
N-Nitrosodimethylamine ND ug/L 09/11/19 17:58 62-75-909/11/19 13:2410.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/11/19 17:58 621-64-709/11/19 13:2410.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 09/11/19 17:58 86-30-609/11/19 13:2410.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/11/19 17:58 108-60-109/11/19 13:2410.0 2.8 1
Pentachlorophenol ND ug/L 09/11/19 17:58 87-86-509/11/19 13:2425.0 2.2 1
Phenanthrene ND ug/L 09/11/19 17:58 85-01-809/11/19 13:2410.0 1.7 1
Phenol ND ug/L 09/11/19 17:58 108-95-209/11/19 13:2410.0 0.92 1
Pyrene ND ug/L 09/11/19 17:58 129-00-009/11/19 13:2410.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 09/11/19 17:58 120-82-109/11/19 13:2410.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 09/11/19 17:58 95-95-409/11/19 13:2410.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/11/19 17:58 88-06-209/11/19 13:2410.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)35 %09/11/19 17:58 4165-60-009/11/19 13:2413-130 1
2-Fluorobiphenyl (S)33 %09/11/19 17:58 321-60-809/11/19 13:2413-130 1
Terphenyl-d14 (S)86 %09/11/19 17:58 1718-51-009/11/19 13:2425-130 1
Phenol-d6 (S)18 %09/11/19 17:58 13127-88-309/11/19 13:2410-130 1
2-Fluorophenol (S)26 %09/11/19 17:58 367-12-409/11/19 13:2410-130 1
2,4,6-Tribromophenol (S)48 %09/11/19 17:58 118-79-609/11/19 13:2410-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 6 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92444875
DCY.001
Sample: MW-1 Lab ID: 92444875001 Collected: 09/09/19 15:20 Received: 09/10/19 07:11 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 09/12/19 12:57 67-64-125.0 6.2 1
Benzene ND ug/L 09/12/19 12:57 71-43-21.0 0.15 1
Bromobenzene ND ug/L 09/12/19 12:57 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 09/12/19 12:57 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 09/12/19 12:57 75-27-41.0 0.26 1
Bromoform ND ug/L 09/12/19 12:57 75-25-21.0 0.62 1
Bromomethane ND ug/L 09/12/19 12:57 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 09/12/19 12:57 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 09/12/19 12:57 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 09/12/19 12:57 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/12/19 12:57 75-00-31.0 0.49 1
Chloroform ND ug/L 09/12/19 12:57 67-66-35.0 2.3 1
Chloromethane ND ug/L 09/12/19 12:57 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 09/12/19 12:57 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 09/12/19 12:57 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 09/12/19 12:57 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 09/12/19 12:57 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 09/12/19 12:57 106-93-41.0 0.26 1
Dibromomethane ND ug/L 09/12/19 12:57 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 09/12/19 12:57 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 09/12/19 12:57 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 09/12/19 12:57 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 09/12/19 12:57 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 09/12/19 12:57 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 09/12/19 12:57 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 09/12/19 12:57 75-35-41.0 0.24 1
cis-1,2-Dichloroethene 2.6 ug/L 09/12/19 12:57 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 09/12/19 12:57 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 09/12/19 12:57 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 09/12/19 12:57 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 09/12/19 12:57 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 09/12/19 12:57 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 09/12/19 12:57 10061-01-5 L11.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 09/12/19 12:57 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 09/12/19 12:57 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 09/12/19 12:57 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 09/12/19 12:57 87-68-31.0 0.44 1
2-Hexanone ND ug/L 09/12/19 12:57 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 09/12/19 12:57 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 09/12/19 12:57 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/12/19 12:57 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 09/12/19 12:57 1634-04-41.0 0.28 1
Naphthalene ND ug/L 09/12/19 12:57 91-20-31.0 0.35 1
Styrene ND ug/L 09/12/19 12:57 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 09/12/19 12:57 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 09/12/19 12:57 79-34-51.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92444875
DCY.001
Sample: MW-1 Lab ID: 92444875001 Collected: 09/09/19 15:20 Received: 09/10/19 07:11 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Tetrachloroethene ND ug/L 09/12/19 12:57 127-18-41.0 0.16 1
Toluene ND ug/L 09/12/19 12:57 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 09/12/19 12:57 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 09/12/19 12:57 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 09/12/19 12:57 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 09/12/19 12:57 79-00-51.0 0.24 1
Trichloroethene 40.6 ug/L 09/12/19 12:57 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 09/12/19 12:57 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 09/12/19 12:57 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 09/12/19 12:57 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 09/12/19 12:57 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 09/12/19 12:57 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 09/12/19 12:57 179601-23-12.0 0.41 1
o-Xylene ND ug/L 09/12/19 12:57 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)99 %09/12/19 12:57 460-00-470-130 1
1,2-Dichloroethane-d4 (S)82 %09/12/19 12:57 17060-07-070-130 1
Toluene-d8 (S)102 %09/12/19 12:57 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92444875
DCY.001
Sample: MW-2 Lab ID: 92444875002 Collected: 09/09/19 15:55 Received: 09/10/19 07:11 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015Metals (ICPMS) 6020B
Antimony ND ug/L 09/14/19 16:28 7440-36-009/14/19 12:402.00 0.754 1
Arsenic ND ug/L 09/14/19 16:28 7440-38-209/14/19 12:402.00 0.250 1
Beryllium 0.382J ug/L 09/14/19 16:28 7440-41-7 J09/14/19 12:402.00 0.120 1
Cadmium ND ug/L 09/14/19 16:28 7440-43-909/14/19 12:401.00 0.160 1
Chromium 0.907J ug/L 09/14/19 16:28 7440-47-3 B,J09/14/19 12:402.00 0.540 1
Copper 1.29J ug/L 09/14/19 16:28 7440-50-8 B,J09/14/19 12:405.00 0.520 1
Lead 1.10J ug/L 09/14/19 16:28 7439-92-1 B,J09/14/19 12:402.00 0.240 1
Manganese 221 ug/L 09/15/19 20:36 7439-96-509/14/19 12:4010.0 0.500 2
Nickel ND ug/L 09/14/19 16:28 7440-02-009/14/19 12:402.00 0.350 1
Silver ND ug/L 09/14/19 16:28 7440-22-409/14/19 12:402.00 0.310 1
Thallium 0.236J ug/L 09/14/19 16:28 7440-28-0 J09/14/19 12:402.00 0.190 1
Zinc 3.78J ug/L 09/14/19 16:28 7440-66-6 J09/14/19 12:4025.0 2.56 1
Analytical Method: EPA 7470A Preparation Method: 7470AMercury 7470A
Mercury ND ug/L 09/15/19 20:48 7439-97-609/13/19 10:370.200 0.0490 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 09/11/19 18:49 83-32-909/11/19 13:2410.0 1.6 1
Acenaphthylene ND ug/L 09/11/19 18:49 208-96-809/11/19 13:2410.0 1.6 1
Aniline ND ug/L 09/11/19 18:49 62-53-309/11/19 13:2410.0 1.9 1
Anthracene ND ug/L 09/11/19 18:49 120-12-709/11/19 13:2410.0 1.7 1
Benzo(a)anthracene ND ug/L 09/11/19 18:49 56-55-309/11/19 13:2410.0 1.8 1
Benzo(a)pyrene ND ug/L 09/11/19 18:49 50-32-809/11/19 13:2410.0 2.1 1
Benzo(b)fluoranthene ND ug/L 09/11/19 18:49 205-99-209/11/19 13:2410.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 09/11/19 18:49 191-24-209/11/19 13:2410.0 1.4 1
Benzo(k)fluoranthene ND ug/L 09/11/19 18:49 207-08-909/11/19 13:2410.0 1.9 1
Benzoic Acid ND ug/L 09/11/19 18:49 65-85-009/11/19 13:2450.0 43.0 1
Benzyl alcohol ND ug/L 09/11/19 18:49 100-51-609/11/19 13:2420.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 09/11/19 18:49 101-55-309/11/19 13:2410.0 1.6 1
Butylbenzylphthalate ND ug/L 09/11/19 18:49 85-68-709/11/19 13:2410.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 09/11/19 18:49 59-50-709/11/19 13:2420.0 2.8 1
4-Chloroaniline ND ug/L 09/11/19 18:49 106-47-809/11/19 13:2420.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 09/11/19 18:49 111-91-109/11/19 13:2410.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/11/19 18:49 111-44-409/11/19 13:2410.0 1.8 1
2-Chloronaphthalene ND ug/L 09/11/19 18:49 91-58-709/11/19 13:2410.0 1.5 1
2-Chlorophenol ND ug/L 09/11/19 18:49 95-57-809/11/19 13:2410.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/11/19 18:49 7005-72-309/11/19 13:2410.0 1.6 1
Chrysene ND ug/L 09/11/19 18:49 218-01-909/11/19 13:2410.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 09/11/19 18:49 53-70-309/11/19 13:2410.0 1.6 1
Dibenzofuran ND ug/L 09/11/19 18:49 132-64-909/11/19 13:2410.0 1.5 1
1,2-Dichlorobenzene ND ug/L 09/11/19 18:49 95-50-109/11/19 13:2410.0 1.3 1
1,3-Dichlorobenzene ND ug/L 09/11/19 18:49 541-73-109/11/19 13:2410.0 1.5 1
1,4-Dichlorobenzene ND ug/L 09/11/19 18:49 106-46-709/11/19 13:2410.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/11/19 18:49 91-94-109/11/19 13:2420.0 3.0 1
2,4-Dichlorophenol ND ug/L 09/11/19 18:49 120-83-209/11/19 13:2410.0 1.4 1
Diethylphthalate ND ug/L 09/11/19 18:49 84-66-209/11/19 13:2410.0 2.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
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Page 9 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92444875
DCY.001
Sample: MW-2 Lab ID: 92444875002 Collected: 09/09/19 15:55 Received: 09/10/19 07:11 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dimethylphenol ND ug/L 09/11/19 18:49 105-67-909/11/19 13:2410.0 1.4 1
Dimethylphthalate ND ug/L 09/11/19 18:49 131-11-309/11/19 13:2410.0 1.6 1
Di-n-butylphthalate ND ug/L 09/11/19 18:49 84-74-209/11/19 13:2410.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 09/11/19 18:49 534-52-109/11/19 13:2420.0 15.2 1
2,4-Dinitrophenol ND ug/L 09/11/19 18:49 51-28-509/11/19 13:2450.0 40.5 1
2,4-Dinitrotoluene ND ug/L 09/11/19 18:49 121-14-209/11/19 13:2410.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/11/19 18:49 606-20-209/11/19 13:2410.0 1.4 1
Di-n-octylphthalate ND ug/L 09/11/19 18:49 117-84-009/11/19 13:2410.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/11/19 18:49 117-81-709/11/19 13:246.0 2.1 1
Fluoranthene ND ug/L 09/11/19 18:49 206-44-009/11/19 13:2410.0 1.7 1
Fluorene ND ug/L 09/11/19 18:49 86-73-709/11/19 13:2410.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 09/11/19 18:49 87-68-309/11/19 13:2410.0 2.0 1
Hexachlorobenzene ND ug/L 09/11/19 18:49 118-74-109/11/19 13:2410.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 09/11/19 18:49 77-47-409/11/19 13:2410.0 1.7 1
Hexachloroethane ND ug/L 09/11/19 18:49 67-72-109/11/19 13:2410.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/11/19 18:49 193-39-509/11/19 13:2410.0 1.6 1
Isophorone ND ug/L 09/11/19 18:49 78-59-109/11/19 13:2410.0 1.6 1
1-Methylnaphthalene ND ug/L 09/11/19 18:49 90-12-009/11/19 13:2410.0 1.4 1
2-Methylnaphthalene ND ug/L 09/11/19 18:49 91-57-609/11/19 13:2410.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 09/11/19 18:49 95-48-709/11/19 13:2410.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/11/19 18:49 15831-10-409/11/19 13:2410.0 1.2 1
Naphthalene ND ug/L 09/11/19 18:49 91-20-309/11/19 13:2410.0 1.4 1
2-Nitroaniline ND ug/L 09/11/19 18:49 88-74-409/11/19 13:2420.0 4.2 1
3-Nitroaniline ND ug/L 09/11/19 18:49 99-09-209/11/19 13:2420.0 2.3 1
4-Nitroaniline ND ug/L 09/11/19 18:49 100-01-609/11/19 13:2420.0 2.2 1
Nitrobenzene ND ug/L 09/11/19 18:49 98-95-309/11/19 13:2410.0 2.1 1
2-Nitrophenol ND ug/L 09/11/19 18:49 88-75-509/11/19 13:2410.0 1.4 1
4-Nitrophenol ND ug/L 09/11/19 18:49 100-02-709/11/19 13:2450.0 3.5 1
N-Nitrosodimethylamine ND ug/L 09/11/19 18:49 62-75-909/11/19 13:2410.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/11/19 18:49 621-64-709/11/19 13:2410.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 09/11/19 18:49 86-30-609/11/19 13:2410.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/11/19 18:49 108-60-109/11/19 13:2410.0 2.8 1
Pentachlorophenol ND ug/L 09/11/19 18:49 87-86-509/11/19 13:2425.0 2.2 1
Phenanthrene ND ug/L 09/11/19 18:49 85-01-809/11/19 13:2410.0 1.7 1
Phenol ND ug/L 09/11/19 18:49 108-95-209/11/19 13:2410.0 0.92 1
Pyrene ND ug/L 09/11/19 18:49 129-00-009/11/19 13:2410.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 09/11/19 18:49 120-82-109/11/19 13:2410.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 09/11/19 18:49 95-95-409/11/19 13:2410.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/11/19 18:49 88-06-209/11/19 13:2410.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)70 %09/11/19 18:49 4165-60-009/11/19 13:2413-130 1
2-Fluorobiphenyl (S)69 %09/11/19 18:49 321-60-809/11/19 13:2413-130 1
Terphenyl-d14 (S)92 %09/11/19 18:49 1718-51-009/11/19 13:2425-130 1
Phenol-d6 (S)39 %09/11/19 18:49 13127-88-309/11/19 13:2410-130 1
2-Fluorophenol (S)56 %09/11/19 18:49 367-12-409/11/19 13:2410-130 1
2,4,6-Tribromophenol (S)73 %09/11/19 18:49 118-79-609/11/19 13:2410-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
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Page 10 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92444875
DCY.001
Sample: MW-2 Lab ID: 92444875002 Collected: 09/09/19 15:55 Received: 09/10/19 07:11 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 09/12/19 13:32 67-64-125.0 6.2 1
Benzene ND ug/L 09/12/19 13:32 71-43-21.0 0.15 1
Bromobenzene ND ug/L 09/12/19 13:32 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 09/12/19 13:32 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 09/12/19 13:32 75-27-41.0 0.26 1
Bromoform ND ug/L 09/12/19 13:32 75-25-21.0 0.62 1
Bromomethane ND ug/L 09/12/19 13:32 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 09/12/19 13:32 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 09/12/19 13:32 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 09/12/19 13:32 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/12/19 13:32 75-00-31.0 0.49 1
Chloroform ND ug/L 09/12/19 13:32 67-66-35.0 2.3 1
Chloromethane ND ug/L 09/12/19 13:32 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 09/12/19 13:32 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 09/12/19 13:32 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 09/12/19 13:32 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 09/12/19 13:32 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 09/12/19 13:32 106-93-41.0 0.26 1
Dibromomethane ND ug/L 09/12/19 13:32 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 09/12/19 13:32 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 09/12/19 13:32 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 09/12/19 13:32 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 09/12/19 13:32 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 09/12/19 13:32 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 09/12/19 13:32 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 09/12/19 13:32 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 09/12/19 13:32 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 09/12/19 13:32 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 09/12/19 13:32 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 09/12/19 13:32 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 09/12/19 13:32 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 09/12/19 13:32 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 09/12/19 13:32 10061-01-5 L11.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 09/12/19 13:32 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 09/12/19 13:32 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 09/12/19 13:32 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 09/12/19 13:32 87-68-31.0 0.44 1
2-Hexanone ND ug/L 09/12/19 13:32 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 09/12/19 13:32 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 09/12/19 13:32 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/12/19 13:32 108-10-15.0 4.5 1
Methyl-tert-butyl ether 0.95J ug/L 09/12/19 13:32 1634-04-41.0 0.28 1
Naphthalene ND ug/L 09/12/19 13:32 91-20-31.0 0.35 1
Styrene ND ug/L 09/12/19 13:32 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 09/12/19 13:32 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 09/12/19 13:32 79-34-51.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92444875
DCY.001
Sample: MW-2 Lab ID: 92444875002 Collected: 09/09/19 15:55 Received: 09/10/19 07:11 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Tetrachloroethene ND ug/L 09/12/19 13:32 127-18-41.0 0.16 1
Toluene ND ug/L 09/12/19 13:32 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 09/12/19 13:32 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 09/12/19 13:32 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 09/12/19 13:32 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 09/12/19 13:32 79-00-51.0 0.24 1
Trichloroethene ND ug/L 09/12/19 13:32 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 09/12/19 13:32 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 09/12/19 13:32 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 09/12/19 13:32 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 09/12/19 13:32 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 09/12/19 13:32 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 09/12/19 13:32 179601-23-12.0 0.41 1
o-Xylene ND ug/L 09/12/19 13:32 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)99 %09/12/19 13:32 460-00-470-130 1
1,2-Dichloroethane-d4 (S)83 %09/12/19 13:32 17060-07-070-130 1
Toluene-d8 (S)102 %09/12/19 13:32 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92444875
DCY.001
Sample: MW-3 Lab ID: 92444875003 Collected: 09/09/19 13:10 Received: 09/10/19 07:11 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015Metals (ICPMS) 6020B
Antimony ND ug/L 09/14/19 16:32 7440-36-009/14/19 12:402.00 0.754 1
Arsenic ND ug/L 09/14/19 16:32 7440-38-209/14/19 12:402.00 0.250 1
Beryllium ND ug/L 09/14/19 16:32 7440-41-709/14/19 12:402.00 0.120 1
Cadmium ND ug/L 09/14/19 16:32 7440-43-909/14/19 12:401.00 0.160 1
Chromium 1.13J ug/L 09/14/19 16:32 7440-47-3 B,J09/14/19 12:402.00 0.540 1
Copper 1.35J ug/L 09/14/19 16:32 7440-50-8 B,J09/14/19 12:405.00 0.520 1
Lead 0.858J ug/L 09/14/19 16:32 7439-92-1 B,J09/14/19 12:402.00 0.240 1
Manganese 7.48 ug/L 09/14/19 16:32 7439-96-509/14/19 12:405.00 0.250 1
Nickel ND ug/L 09/14/19 16:32 7440-02-009/14/19 12:402.00 0.350 1
Silver ND ug/L 09/14/19 16:32 7440-22-409/14/19 12:402.00 0.310 1
Thallium ND ug/L 09/14/19 16:32 7440-28-009/14/19 12:402.00 0.190 1
Zinc ND ug/L 09/14/19 16:32 7440-66-609/14/19 12:4025.0 2.56 1
Analytical Method: EPA 7470A Preparation Method: 7470AMercury 7470A
Mercury ND ug/L 09/15/19 20:50 7439-97-609/13/19 10:370.200 0.0490 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 09/11/19 19:40 83-32-909/11/19 13:2410.0 1.6 1
Acenaphthylene ND ug/L 09/11/19 19:40 208-96-809/11/19 13:2410.0 1.6 1
Aniline ND ug/L 09/11/19 19:40 62-53-309/11/19 13:2410.0 1.9 1
Anthracene ND ug/L 09/11/19 19:40 120-12-709/11/19 13:2410.0 1.7 1
Benzo(a)anthracene ND ug/L 09/11/19 19:40 56-55-309/11/19 13:2410.0 1.8 1
Benzo(a)pyrene ND ug/L 09/11/19 19:40 50-32-809/11/19 13:2410.0 2.1 1
Benzo(b)fluoranthene ND ug/L 09/11/19 19:40 205-99-209/11/19 13:2410.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 09/11/19 19:40 191-24-209/11/19 13:2410.0 1.4 1
Benzo(k)fluoranthene ND ug/L 09/11/19 19:40 207-08-909/11/19 13:2410.0 1.9 1
Benzoic Acid ND ug/L 09/11/19 19:40 65-85-009/11/19 13:2450.0 43.0 1
Benzyl alcohol ND ug/L 09/11/19 19:40 100-51-609/11/19 13:2420.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 09/11/19 19:40 101-55-309/11/19 13:2410.0 1.6 1
Butylbenzylphthalate ND ug/L 09/11/19 19:40 85-68-709/11/19 13:2410.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 09/11/19 19:40 59-50-709/11/19 13:2420.0 2.8 1
4-Chloroaniline ND ug/L 09/11/19 19:40 106-47-809/11/19 13:2420.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 09/11/19 19:40 111-91-109/11/19 13:2410.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/11/19 19:40 111-44-409/11/19 13:2410.0 1.8 1
2-Chloronaphthalene ND ug/L 09/11/19 19:40 91-58-709/11/19 13:2410.0 1.5 1
2-Chlorophenol ND ug/L 09/11/19 19:40 95-57-809/11/19 13:2410.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/11/19 19:40 7005-72-309/11/19 13:2410.0 1.6 1
Chrysene ND ug/L 09/11/19 19:40 218-01-909/11/19 13:2410.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 09/11/19 19:40 53-70-309/11/19 13:2410.0 1.6 1
Dibenzofuran ND ug/L 09/11/19 19:40 132-64-909/11/19 13:2410.0 1.5 1
1,2-Dichlorobenzene ND ug/L 09/11/19 19:40 95-50-109/11/19 13:2410.0 1.3 1
1,3-Dichlorobenzene ND ug/L 09/11/19 19:40 541-73-109/11/19 13:2410.0 1.5 1
1,4-Dichlorobenzene ND ug/L 09/11/19 19:40 106-46-709/11/19 13:2410.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/11/19 19:40 91-94-109/11/19 13:2420.0 3.0 1
2,4-Dichlorophenol ND ug/L 09/11/19 19:40 120-83-209/11/19 13:2410.0 1.4 1
Diethylphthalate ND ug/L 09/11/19 19:40 84-66-209/11/19 13:2410.0 2.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92444875
DCY.001
Sample: MW-3 Lab ID: 92444875003 Collected: 09/09/19 13:10 Received: 09/10/19 07:11 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dimethylphenol ND ug/L 09/11/19 19:40 105-67-909/11/19 13:2410.0 1.4 1
Dimethylphthalate ND ug/L 09/11/19 19:40 131-11-309/11/19 13:2410.0 1.6 1
Di-n-butylphthalate ND ug/L 09/11/19 19:40 84-74-209/11/19 13:2410.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 09/11/19 19:40 534-52-109/11/19 13:2420.0 15.2 1
2,4-Dinitrophenol ND ug/L 09/11/19 19:40 51-28-509/11/19 13:2450.0 40.5 1
2,4-Dinitrotoluene ND ug/L 09/11/19 19:40 121-14-209/11/19 13:2410.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/11/19 19:40 606-20-209/11/19 13:2410.0 1.4 1
Di-n-octylphthalate ND ug/L 09/11/19 19:40 117-84-009/11/19 13:2410.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/11/19 19:40 117-81-709/11/19 13:246.0 2.1 1
Fluoranthene ND ug/L 09/11/19 19:40 206-44-009/11/19 13:2410.0 1.7 1
Fluorene ND ug/L 09/11/19 19:40 86-73-709/11/19 13:2410.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 09/11/19 19:40 87-68-309/11/19 13:2410.0 2.0 1
Hexachlorobenzene ND ug/L 09/11/19 19:40 118-74-109/11/19 13:2410.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 09/11/19 19:40 77-47-409/11/19 13:2410.0 1.7 1
Hexachloroethane ND ug/L 09/11/19 19:40 67-72-109/11/19 13:2410.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/11/19 19:40 193-39-509/11/19 13:2410.0 1.6 1
Isophorone ND ug/L 09/11/19 19:40 78-59-109/11/19 13:2410.0 1.6 1
1-Methylnaphthalene ND ug/L 09/11/19 19:40 90-12-009/11/19 13:2410.0 1.4 1
2-Methylnaphthalene ND ug/L 09/11/19 19:40 91-57-609/11/19 13:2410.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 09/11/19 19:40 95-48-709/11/19 13:2410.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/11/19 19:40 15831-10-409/11/19 13:2410.0 1.2 1
Naphthalene ND ug/L 09/11/19 19:40 91-20-309/11/19 13:2410.0 1.4 1
2-Nitroaniline ND ug/L 09/11/19 19:40 88-74-409/11/19 13:2420.0 4.2 1
3-Nitroaniline ND ug/L 09/11/19 19:40 99-09-209/11/19 13:2420.0 2.3 1
4-Nitroaniline ND ug/L 09/11/19 19:40 100-01-609/11/19 13:2420.0 2.2 1
Nitrobenzene ND ug/L 09/11/19 19:40 98-95-309/11/19 13:2410.0 2.1 1
2-Nitrophenol ND ug/L 09/11/19 19:40 88-75-509/11/19 13:2410.0 1.4 1
4-Nitrophenol ND ug/L 09/11/19 19:40 100-02-709/11/19 13:2450.0 3.5 1
N-Nitrosodimethylamine ND ug/L 09/11/19 19:40 62-75-909/11/19 13:2410.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/11/19 19:40 621-64-709/11/19 13:2410.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 09/11/19 19:40 86-30-609/11/19 13:2410.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/11/19 19:40 108-60-109/11/19 13:2410.0 2.8 1
Pentachlorophenol ND ug/L 09/11/19 19:40 87-86-509/11/19 13:2425.0 2.2 1
Phenanthrene ND ug/L 09/11/19 19:40 85-01-809/11/19 13:2410.0 1.7 1
Phenol ND ug/L 09/11/19 19:40 108-95-209/11/19 13:2410.0 0.92 1
Pyrene ND ug/L 09/11/19 19:40 129-00-009/11/19 13:2410.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 09/11/19 19:40 120-82-109/11/19 13:2410.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 09/11/19 19:40 95-95-409/11/19 13:2410.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/11/19 19:40 88-06-209/11/19 13:2410.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)53 %09/11/19 19:40 4165-60-009/11/19 13:2413-130 1
2-Fluorobiphenyl (S)50 %09/11/19 19:40 321-60-809/11/19 13:2413-130 1
Terphenyl-d14 (S)109 %09/11/19 19:40 1718-51-009/11/19 13:2425-130 1
Phenol-d6 (S)28 %09/11/19 19:40 13127-88-309/11/19 13:2410-130 1
2-Fluorophenol (S)39 %09/11/19 19:40 367-12-409/11/19 13:2410-130 1
2,4,6-Tribromophenol (S)57 %09/11/19 19:40 118-79-609/11/19 13:2410-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
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Page 14 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92444875
DCY.001
Sample: MW-3 Lab ID: 92444875003 Collected: 09/09/19 13:10 Received: 09/10/19 07:11 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 09/12/19 13:50 67-64-125.0 6.2 1
Benzene ND ug/L 09/12/19 13:50 71-43-21.0 0.15 1
Bromobenzene ND ug/L 09/12/19 13:50 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 09/12/19 13:50 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 09/12/19 13:50 75-27-41.0 0.26 1
Bromoform ND ug/L 09/12/19 13:50 75-25-21.0 0.62 1
Bromomethane ND ug/L 09/12/19 13:50 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 09/12/19 13:50 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 09/12/19 13:50 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 09/12/19 13:50 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/12/19 13:50 75-00-31.0 0.49 1
Chloroform ND ug/L 09/12/19 13:50 67-66-35.0 2.3 1
Chloromethane ND ug/L 09/12/19 13:50 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 09/12/19 13:50 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 09/12/19 13:50 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 09/12/19 13:50 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 09/12/19 13:50 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 09/12/19 13:50 106-93-41.0 0.26 1
Dibromomethane ND ug/L 09/12/19 13:50 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 09/12/19 13:50 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 09/12/19 13:50 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 09/12/19 13:50 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 09/12/19 13:50 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 09/12/19 13:50 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 09/12/19 13:50 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 09/12/19 13:50 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 09/12/19 13:50 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 09/12/19 13:50 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 09/12/19 13:50 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 09/12/19 13:50 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 09/12/19 13:50 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 09/12/19 13:50 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 09/12/19 13:50 10061-01-5 L11.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 09/12/19 13:50 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 09/12/19 13:50 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 09/12/19 13:50 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 09/12/19 13:50 87-68-31.0 0.44 1
2-Hexanone ND ug/L 09/12/19 13:50 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 09/12/19 13:50 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 09/12/19 13:50 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/12/19 13:50 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 09/12/19 13:50 1634-04-41.0 0.28 1
Naphthalene ND ug/L 09/12/19 13:50 91-20-31.0 0.35 1
Styrene ND ug/L 09/12/19 13:50 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 09/12/19 13:50 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 09/12/19 13:50 79-34-51.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
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Page 15 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92444875
DCY.001
Sample: MW-3 Lab ID: 92444875003 Collected: 09/09/19 13:10 Received: 09/10/19 07:11 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Tetrachloroethene ND ug/L 09/12/19 13:50 127-18-41.0 0.16 1
Toluene ND ug/L 09/12/19 13:50 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 09/12/19 13:50 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 09/12/19 13:50 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 09/12/19 13:50 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 09/12/19 13:50 79-00-51.0 0.24 1
Trichloroethene ND ug/L 09/12/19 13:50 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 09/12/19 13:50 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 09/12/19 13:50 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 09/12/19 13:50 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 09/12/19 13:50 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 09/12/19 13:50 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 09/12/19 13:50 179601-23-12.0 0.41 1
o-Xylene ND ug/L 09/12/19 13:50 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)98 %09/12/19 13:50 460-00-470-130 1
1,2-Dichloroethane-d4 (S)83 %09/12/19 13:50 17060-07-070-130 1
Toluene-d8 (S)102 %09/12/19 13:50 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 16 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92444875
DCY.001
Sample: MW-4 Lab ID: 92444875004 Collected: 09/09/19 10:55 Received: 09/10/19 07:11 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015Metals (ICPMS) 6020B
Antimony ND ug/L 09/14/19 16:36 7440-36-009/14/19 12:402.00 0.754 1
Arsenic ND ug/L 09/14/19 16:36 7440-38-209/14/19 12:402.00 0.250 1
Beryllium ND ug/L 09/14/19 16:36 7440-41-709/14/19 12:402.00 0.120 1
Cadmium ND ug/L 09/14/19 16:36 7440-43-909/14/19 12:401.00 0.160 1
Chromium ND ug/L 09/14/19 16:36 7440-47-309/14/19 12:402.00 0.540 1
Copper 0.568J ug/L 09/14/19 16:36 7440-50-8 B,J09/14/19 12:405.00 0.520 1
Lead 0.894J ug/L 09/14/19 16:36 7439-92-1 B,J09/14/19 12:402.00 0.240 1
Manganese 12.4 ug/L 09/14/19 16:36 7439-96-509/14/19 12:405.00 0.250 1
Nickel ND ug/L 09/14/19 16:36 7440-02-009/14/19 12:402.00 0.350 1
Silver ND ug/L 09/14/19 16:36 7440-22-409/14/19 12:402.00 0.310 1
Thallium ND ug/L 09/14/19 16:36 7440-28-009/14/19 12:402.00 0.190 1
Zinc 2.70J ug/L 09/14/19 16:36 7440-66-6 J09/14/19 12:4025.0 2.56 1
Analytical Method: EPA 7470A Preparation Method: 7470AMercury 7470A
Mercury ND ug/L 09/15/19 20:52 7439-97-609/13/19 10:370.200 0.0490 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 09/11/19 20:05 83-32-909/11/19 13:2410.0 1.6 1
Acenaphthylene ND ug/L 09/11/19 20:05 208-96-809/11/19 13:2410.0 1.6 1
Aniline ND ug/L 09/11/19 20:05 62-53-309/11/19 13:2410.0 1.9 1
Anthracene ND ug/L 09/11/19 20:05 120-12-709/11/19 13:2410.0 1.7 1
Benzo(a)anthracene ND ug/L 09/11/19 20:05 56-55-309/11/19 13:2410.0 1.8 1
Benzo(a)pyrene ND ug/L 09/11/19 20:05 50-32-809/11/19 13:2410.0 2.1 1
Benzo(b)fluoranthene ND ug/L 09/11/19 20:05 205-99-209/11/19 13:2410.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 09/11/19 20:05 191-24-209/11/19 13:2410.0 1.4 1
Benzo(k)fluoranthene ND ug/L 09/11/19 20:05 207-08-909/11/19 13:2410.0 1.9 1
Benzoic Acid ND ug/L 09/11/19 20:05 65-85-009/11/19 13:2450.0 43.0 1
Benzyl alcohol ND ug/L 09/11/19 20:05 100-51-609/11/19 13:2420.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 09/11/19 20:05 101-55-309/11/19 13:2410.0 1.6 1
Butylbenzylphthalate ND ug/L 09/11/19 20:05 85-68-709/11/19 13:2410.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 09/11/19 20:05 59-50-709/11/19 13:2420.0 2.8 1
4-Chloroaniline ND ug/L 09/11/19 20:05 106-47-809/11/19 13:2420.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 09/11/19 20:05 111-91-109/11/19 13:2410.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/11/19 20:05 111-44-409/11/19 13:2410.0 1.8 1
2-Chloronaphthalene ND ug/L 09/11/19 20:05 91-58-709/11/19 13:2410.0 1.5 1
2-Chlorophenol ND ug/L 09/11/19 20:05 95-57-809/11/19 13:2410.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/11/19 20:05 7005-72-309/11/19 13:2410.0 1.6 1
Chrysene ND ug/L 09/11/19 20:05 218-01-909/11/19 13:2410.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 09/11/19 20:05 53-70-309/11/19 13:2410.0 1.6 1
Dibenzofuran ND ug/L 09/11/19 20:05 132-64-909/11/19 13:2410.0 1.5 1
1,2-Dichlorobenzene ND ug/L 09/11/19 20:05 95-50-109/11/19 13:2410.0 1.3 1
1,3-Dichlorobenzene ND ug/L 09/11/19 20:05 541-73-109/11/19 13:2410.0 1.5 1
1,4-Dichlorobenzene ND ug/L 09/11/19 20:05 106-46-709/11/19 13:2410.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/11/19 20:05 91-94-109/11/19 13:2420.0 3.0 1
2,4-Dichlorophenol ND ug/L 09/11/19 20:05 120-83-209/11/19 13:2410.0 1.4 1
Diethylphthalate ND ug/L 09/11/19 20:05 84-66-209/11/19 13:2410.0 2.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92444875
DCY.001
Sample: MW-4 Lab ID: 92444875004 Collected: 09/09/19 10:55 Received: 09/10/19 07:11 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dimethylphenol ND ug/L 09/11/19 20:05 105-67-909/11/19 13:2410.0 1.4 1
Dimethylphthalate ND ug/L 09/11/19 20:05 131-11-309/11/19 13:2410.0 1.6 1
Di-n-butylphthalate ND ug/L 09/11/19 20:05 84-74-209/11/19 13:2410.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 09/11/19 20:05 534-52-109/11/19 13:2420.0 15.2 1
2,4-Dinitrophenol ND ug/L 09/11/19 20:05 51-28-509/11/19 13:2450.0 40.5 1
2,4-Dinitrotoluene ND ug/L 09/11/19 20:05 121-14-209/11/19 13:2410.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/11/19 20:05 606-20-209/11/19 13:2410.0 1.4 1
Di-n-octylphthalate ND ug/L 09/11/19 20:05 117-84-009/11/19 13:2410.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/11/19 20:05 117-81-709/11/19 13:246.0 2.1 1
Fluoranthene ND ug/L 09/11/19 20:05 206-44-009/11/19 13:2410.0 1.7 1
Fluorene ND ug/L 09/11/19 20:05 86-73-709/11/19 13:2410.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 09/11/19 20:05 87-68-309/11/19 13:2410.0 2.0 1
Hexachlorobenzene ND ug/L 09/11/19 20:05 118-74-109/11/19 13:2410.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 09/11/19 20:05 77-47-409/11/19 13:2410.0 1.7 1
Hexachloroethane ND ug/L 09/11/19 20:05 67-72-109/11/19 13:2410.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/11/19 20:05 193-39-509/11/19 13:2410.0 1.6 1
Isophorone ND ug/L 09/11/19 20:05 78-59-109/11/19 13:2410.0 1.6 1
1-Methylnaphthalene ND ug/L 09/11/19 20:05 90-12-009/11/19 13:2410.0 1.4 1
2-Methylnaphthalene ND ug/L 09/11/19 20:05 91-57-609/11/19 13:2410.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 09/11/19 20:05 95-48-709/11/19 13:2410.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/11/19 20:05 15831-10-409/11/19 13:2410.0 1.2 1
Naphthalene ND ug/L 09/11/19 20:05 91-20-309/11/19 13:2410.0 1.4 1
2-Nitroaniline ND ug/L 09/11/19 20:05 88-74-409/11/19 13:2420.0 4.2 1
3-Nitroaniline ND ug/L 09/11/19 20:05 99-09-209/11/19 13:2420.0 2.3 1
4-Nitroaniline ND ug/L 09/11/19 20:05 100-01-609/11/19 13:2420.0 2.2 1
Nitrobenzene ND ug/L 09/11/19 20:05 98-95-309/11/19 13:2410.0 2.1 1
2-Nitrophenol ND ug/L 09/11/19 20:05 88-75-509/11/19 13:2410.0 1.4 1
4-Nitrophenol ND ug/L 09/11/19 20:05 100-02-709/11/19 13:2450.0 3.5 1
N-Nitrosodimethylamine ND ug/L 09/11/19 20:05 62-75-909/11/19 13:2410.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/11/19 20:05 621-64-709/11/19 13:2410.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 09/11/19 20:05 86-30-609/11/19 13:2410.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/11/19 20:05 108-60-109/11/19 13:2410.0 2.8 1
Pentachlorophenol ND ug/L 09/11/19 20:05 87-86-509/11/19 13:2425.0 2.2 1
Phenanthrene ND ug/L 09/11/19 20:05 85-01-809/11/19 13:2410.0 1.7 1
Phenol ND ug/L 09/11/19 20:05 108-95-209/11/19 13:2410.0 0.92 1
Pyrene ND ug/L 09/11/19 20:05 129-00-009/11/19 13:2410.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 09/11/19 20:05 120-82-109/11/19 13:2410.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 09/11/19 20:05 95-95-409/11/19 13:2410.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/11/19 20:05 88-06-209/11/19 13:2410.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)55 %09/11/19 20:05 4165-60-009/11/19 13:2413-130 1
2-Fluorobiphenyl (S)55 %09/11/19 20:05 321-60-809/11/19 13:2413-130 1
Terphenyl-d14 (S)99 %09/11/19 20:05 1718-51-009/11/19 13:2425-130 1
Phenol-d6 (S)28 %09/11/19 20:05 13127-88-309/11/19 13:2410-130 1
2-Fluorophenol (S)37 %09/11/19 20:05 367-12-409/11/19 13:2410-130 1
2,4,6-Tribromophenol (S)60 %09/11/19 20:05 118-79-609/11/19 13:2410-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92444875
DCY.001
Sample: MW-4 Lab ID: 92444875004 Collected: 09/09/19 10:55 Received: 09/10/19 07:11 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 09/12/19 14:25 67-64-125.0 6.2 1
Benzene ND ug/L 09/12/19 14:25 71-43-21.0 0.15 1
Bromobenzene ND ug/L 09/12/19 14:25 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 09/12/19 14:25 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 09/12/19 14:25 75-27-41.0 0.26 1
Bromoform ND ug/L 09/12/19 14:25 75-25-21.0 0.62 1
Bromomethane ND ug/L 09/12/19 14:25 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 09/12/19 14:25 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 09/12/19 14:25 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 09/12/19 14:25 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/12/19 14:25 75-00-31.0 0.49 1
Chloroform ND ug/L 09/12/19 14:25 67-66-35.0 2.3 1
Chloromethane ND ug/L 09/12/19 14:25 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 09/12/19 14:25 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 09/12/19 14:25 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 09/12/19 14:25 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 09/12/19 14:25 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 09/12/19 14:25 106-93-41.0 0.26 1
Dibromomethane ND ug/L 09/12/19 14:25 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 09/12/19 14:25 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 09/12/19 14:25 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 09/12/19 14:25 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 09/12/19 14:25 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 09/12/19 14:25 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 09/12/19 14:25 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 09/12/19 14:25 75-35-41.0 0.24 1
cis-1,2-Dichloroethene 0.72J ug/L 09/12/19 14:25 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 09/12/19 14:25 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 09/12/19 14:25 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 09/12/19 14:25 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 09/12/19 14:25 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 09/12/19 14:25 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 09/12/19 14:25 10061-01-5 L11.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 09/12/19 14:25 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 09/12/19 14:25 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 09/12/19 14:25 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 09/12/19 14:25 87-68-31.0 0.44 1
2-Hexanone ND ug/L 09/12/19 14:25 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 09/12/19 14:25 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 09/12/19 14:25 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/12/19 14:25 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 09/12/19 14:25 1634-04-41.0 0.28 1
Naphthalene ND ug/L 09/12/19 14:25 91-20-31.0 0.35 1
Styrene ND ug/L 09/12/19 14:25 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 09/12/19 14:25 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 09/12/19 14:25 79-34-51.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
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Page 19 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92444875
DCY.001
Sample: MW-4 Lab ID: 92444875004 Collected: 09/09/19 10:55 Received: 09/10/19 07:11 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Tetrachloroethene ND ug/L 09/12/19 14:25 127-18-41.0 0.16 1
Toluene ND ug/L 09/12/19 14:25 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 09/12/19 14:25 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 09/12/19 14:25 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 09/12/19 14:25 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 09/12/19 14:25 79-00-51.0 0.24 1
Trichloroethene 32.5 ug/L 09/12/19 14:25 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 09/12/19 14:25 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 09/12/19 14:25 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 09/12/19 14:25 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 09/12/19 14:25 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 09/12/19 14:25 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 09/12/19 14:25 179601-23-12.0 0.41 1
o-Xylene ND ug/L 09/12/19 14:25 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)104 %09/12/19 14:25 460-00-470-130 1
1,2-Dichloroethane-d4 (S)87 %09/12/19 14:25 17060-07-070-130 1
Toluene-d8 (S)95 %09/12/19 14:25 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
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Page 20 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92444875
DCY.001
Sample: DUP-4 Lab ID: 92444875005 Collected: 09/09/19 00:00 Received: 09/10/19 07:11 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3015Metals (ICPMS) 6020B
Antimony ND ug/L 09/14/19 16:40 7440-36-009/14/19 12:402.00 0.754 1
Arsenic ND ug/L 09/14/19 16:40 7440-38-209/14/19 12:402.00 0.250 1
Beryllium ND ug/L 09/14/19 16:40 7440-41-709/14/19 12:402.00 0.120 1
Cadmium ND ug/L 09/14/19 16:40 7440-43-909/14/19 12:401.00 0.160 1
Chromium 0.821J ug/L 09/14/19 16:40 7440-47-3 B,J09/14/19 12:402.00 0.540 1
Copper 0.528J ug/L 09/14/19 16:40 7440-50-8 B,J09/14/19 12:405.00 0.520 1
Lead 0.702J ug/L 09/14/19 16:40 7439-92-1 B,J09/14/19 12:402.00 0.240 1
Manganese 6.29 ug/L 09/14/19 16:40 7439-96-509/14/19 12:405.00 0.250 1
Nickel ND ug/L 09/14/19 16:40 7440-02-009/14/19 12:402.00 0.350 1
Silver ND ug/L 09/14/19 16:40 7440-22-409/14/19 12:402.00 0.310 1
Thallium ND ug/L 09/14/19 16:40 7440-28-009/14/19 12:402.00 0.190 1
Zinc ND ug/L 09/14/19 16:40 7440-66-609/14/19 12:4025.0 2.56 1
Analytical Method: EPA 7470A Preparation Method: 7470AMercury 7470A
Mercury ND ug/L 09/15/19 20:54 7439-97-609/13/19 10:370.200 0.0490 1
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
Acenaphthene ND ug/L 09/11/19 20:31 83-32-909/11/19 13:2410.0 1.6 1
Acenaphthylene ND ug/L 09/11/19 20:31 208-96-809/11/19 13:2410.0 1.6 1
Aniline ND ug/L 09/11/19 20:31 62-53-309/11/19 13:2410.0 1.9 1
Anthracene ND ug/L 09/11/19 20:31 120-12-709/11/19 13:2410.0 1.7 1
Benzo(a)anthracene ND ug/L 09/11/19 20:31 56-55-309/11/19 13:2410.0 1.8 1
Benzo(a)pyrene ND ug/L 09/11/19 20:31 50-32-809/11/19 13:2410.0 2.1 1
Benzo(b)fluoranthene ND ug/L 09/11/19 20:31 205-99-209/11/19 13:2410.0 1.9 1
Benzo(g,h,i)perylene ND ug/L 09/11/19 20:31 191-24-209/11/19 13:2410.0 1.4 1
Benzo(k)fluoranthene ND ug/L 09/11/19 20:31 207-08-909/11/19 13:2410.0 1.9 1
Benzoic Acid ND ug/L 09/11/19 20:31 65-85-009/11/19 13:2450.0 43.0 1
Benzyl alcohol ND ug/L 09/11/19 20:31 100-51-609/11/19 13:2420.0 2.6 1
4-Bromophenylphenyl ether ND ug/L 09/11/19 20:31 101-55-309/11/19 13:2410.0 1.6 1
Butylbenzylphthalate ND ug/L 09/11/19 20:31 85-68-709/11/19 13:2410.0 1.6 1
4-Chloro-3-methylphenol ND ug/L 09/11/19 20:31 59-50-709/11/19 13:2420.0 2.8 1
4-Chloroaniline ND ug/L 09/11/19 20:31 106-47-809/11/19 13:2420.0 2.8 1
bis(2-Chloroethoxy)methane ND ug/L 09/11/19 20:31 111-91-109/11/19 13:2410.0 1.8 1
bis(2-Chloroethyl) ether ND ug/L 09/11/19 20:31 111-44-409/11/19 13:2410.0 1.8 1
2-Chloronaphthalene ND ug/L 09/11/19 20:31 91-58-709/11/19 13:2410.0 1.5 1
2-Chlorophenol ND ug/L 09/11/19 20:31 95-57-809/11/19 13:2410.0 1.2 1
4-Chlorophenylphenyl ether ND ug/L 09/11/19 20:31 7005-72-309/11/19 13:2410.0 1.6 1
Chrysene ND ug/L 09/11/19 20:31 218-01-909/11/19 13:2410.0 1.7 1
Dibenz(a,h)anthracene ND ug/L 09/11/19 20:31 53-70-309/11/19 13:2410.0 1.6 1
Dibenzofuran ND ug/L 09/11/19 20:31 132-64-909/11/19 13:2410.0 1.5 1
1,2-Dichlorobenzene ND ug/L 09/11/19 20:31 95-50-109/11/19 13:2410.0 1.3 1
1,3-Dichlorobenzene ND ug/L 09/11/19 20:31 541-73-109/11/19 13:2410.0 1.5 1
1,4-Dichlorobenzene ND ug/L 09/11/19 20:31 106-46-709/11/19 13:2410.0 2.1 1
3,3'-Dichlorobenzidine ND ug/L 09/11/19 20:31 91-94-109/11/19 13:2420.0 3.0 1
2,4-Dichlorophenol ND ug/L 09/11/19 20:31 120-83-209/11/19 13:2410.0 1.4 1
Diethylphthalate ND ug/L 09/11/19 20:31 84-66-209/11/19 13:2410.0 2.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
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Page 21 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92444875
DCY.001
Sample: DUP-4 Lab ID: 92444875005 Collected: 09/09/19 00:00 Received: 09/10/19 07:11 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 3510C8270E RVE
2,4-Dimethylphenol ND ug/L 09/11/19 20:31 105-67-909/11/19 13:2410.0 1.4 1
Dimethylphthalate ND ug/L 09/11/19 20:31 131-11-309/11/19 13:2410.0 1.6 1
Di-n-butylphthalate ND ug/L 09/11/19 20:31 84-74-209/11/19 13:2410.0 1.8 1
4,6-Dinitro-2-methylphenol ND ug/L 09/11/19 20:31 534-52-109/11/19 13:2420.0 15.2 1
2,4-Dinitrophenol ND ug/L 09/11/19 20:31 51-28-509/11/19 13:2450.0 40.5 1
2,4-Dinitrotoluene ND ug/L 09/11/19 20:31 121-14-209/11/19 13:2410.0 1.2 1
2,6-Dinitrotoluene ND ug/L 09/11/19 20:31 606-20-209/11/19 13:2410.0 1.4 1
Di-n-octylphthalate ND ug/L 09/11/19 20:31 117-84-009/11/19 13:2410.0 1.8 1
bis(2-Ethylhexyl)phthalate ND ug/L 09/11/19 20:31 117-81-709/11/19 13:246.0 2.1 1
Fluoranthene ND ug/L 09/11/19 20:31 206-44-009/11/19 13:2410.0 1.7 1
Fluorene ND ug/L 09/11/19 20:31 86-73-709/11/19 13:2410.0 1.6 1
Hexachloro-1,3-butadiene ND ug/L 09/11/19 20:31 87-68-309/11/19 13:2410.0 2.0 1
Hexachlorobenzene ND ug/L 09/11/19 20:31 118-74-109/11/19 13:2410.0 1.7 1
Hexachlorocyclopentadiene ND ug/L 09/11/19 20:31 77-47-409/11/19 13:2410.0 1.7 1
Hexachloroethane ND ug/L 09/11/19 20:31 67-72-109/11/19 13:2410.0 2.0 1
Indeno(1,2,3-cd)pyrene ND ug/L 09/11/19 20:31 193-39-509/11/19 13:2410.0 1.6 1
Isophorone ND ug/L 09/11/19 20:31 78-59-109/11/19 13:2410.0 1.6 1
1-Methylnaphthalene ND ug/L 09/11/19 20:31 90-12-009/11/19 13:2410.0 1.4 1
2-Methylnaphthalene ND ug/L 09/11/19 20:31 91-57-609/11/19 13:2410.0 1.4 1
2-Methylphenol(o-Cresol)ND ug/L 09/11/19 20:31 95-48-709/11/19 13:2410.0 1.2 1
3&4-Methylphenol(m&p Cresol)ND ug/L 09/11/19 20:31 15831-10-409/11/19 13:2410.0 1.2 1
Naphthalene ND ug/L 09/11/19 20:31 91-20-309/11/19 13:2410.0 1.4 1
2-Nitroaniline ND ug/L 09/11/19 20:31 88-74-409/11/19 13:2420.0 4.2 1
3-Nitroaniline ND ug/L 09/11/19 20:31 99-09-209/11/19 13:2420.0 2.3 1
4-Nitroaniline ND ug/L 09/11/19 20:31 100-01-609/11/19 13:2420.0 2.2 1
Nitrobenzene ND ug/L 09/11/19 20:31 98-95-309/11/19 13:2410.0 2.1 1
2-Nitrophenol ND ug/L 09/11/19 20:31 88-75-509/11/19 13:2410.0 1.4 1
4-Nitrophenol ND ug/L 09/11/19 20:31 100-02-709/11/19 13:2450.0 3.5 1
N-Nitrosodimethylamine ND ug/L 09/11/19 20:31 62-75-909/11/19 13:2410.0 1.2 1
N-Nitroso-di-n-propylamine ND ug/L 09/11/19 20:31 621-64-709/11/19 13:2410.0 2.2 1
N-Nitrosodiphenylamine ND ug/L 09/11/19 20:31 86-30-609/11/19 13:2410.0 1.7 1
2,2'-Oxybis(1-chloropropane)ND ug/L 09/11/19 20:31 108-60-109/11/19 13:2410.0 2.8 1
Pentachlorophenol ND ug/L 09/11/19 20:31 87-86-509/11/19 13:2425.0 2.2 1
Phenanthrene ND ug/L 09/11/19 20:31 85-01-809/11/19 13:2410.0 1.7 1
Phenol ND ug/L 09/11/19 20:31 108-95-209/11/19 13:2410.0 0.92 1
Pyrene ND ug/L 09/11/19 20:31 129-00-009/11/19 13:2410.0 2.1 1
1,2,4-Trichlorobenzene ND ug/L 09/11/19 20:31 120-82-109/11/19 13:2410.0 1.5 1
2,4,5-Trichlorophenol ND ug/L 09/11/19 20:31 95-95-409/11/19 13:2410.0 1.4 1
2,4,6-Trichlorophenol ND ug/L 09/11/19 20:31 88-06-209/11/19 13:2410.0 1.5 1
Surrogates
Nitrobenzene-d5 (S)66 %09/11/19 20:31 4165-60-009/11/19 13:2413-130 1
2-Fluorobiphenyl (S)65 %09/11/19 20:31 321-60-809/11/19 13:2413-130 1
Terphenyl-d14 (S)108 %09/11/19 20:31 1718-51-009/11/19 13:2425-130 1
Phenol-d6 (S)37 %09/11/19 20:31 13127-88-309/11/19 13:2410-130 1
2-Fluorophenol (S)49 %09/11/19 20:31 367-12-409/11/19 13:2410-130 1
2,4,6-Tribromophenol (S)74 %09/11/19 20:31 118-79-609/11/19 13:2410-137 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 22 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92444875
DCY.001
Sample: DUP-4 Lab ID: 92444875005 Collected: 09/09/19 00:00 Received: 09/10/19 07:11 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Acetone ND ug/L 09/12/19 14:43 67-64-125.0 6.2 1
Benzene ND ug/L 09/12/19 14:43 71-43-21.0 0.15 1
Bromobenzene ND ug/L 09/12/19 14:43 108-86-11.0 0.22 1
Bromochloromethane ND ug/L 09/12/19 14:43 74-97-51.0 0.34 1
Bromodichloromethane ND ug/L 09/12/19 14:43 75-27-41.0 0.26 1
Bromoform ND ug/L 09/12/19 14:43 75-25-21.0 0.62 1
Bromomethane ND ug/L 09/12/19 14:43 74-83-92.0 0.62 1
2-Butanone (MEK)ND ug/L 09/12/19 14:43 78-93-35.0 3.3 1
Carbon tetrachloride ND ug/L 09/12/19 14:43 56-23-51.0 0.22 1
Chlorobenzene ND ug/L 09/12/19 14:43 108-90-71.0 0.23 1
Chloroethane ND ug/L 09/12/19 14:43 75-00-31.0 0.49 1
Chloroform ND ug/L 09/12/19 14:43 67-66-35.0 2.3 1
Chloromethane ND ug/L 09/12/19 14:43 74-87-31.0 0.39 1
2-Chlorotoluene ND ug/L 09/12/19 14:43 95-49-81.0 0.20 1
4-Chlorotoluene ND ug/L 09/12/19 14:43 106-43-41.0 0.20 1
1,2-Dibromo-3-chloropropane ND ug/L 09/12/19 14:43 96-12-85.0 0.26 1
Dibromochloromethane ND ug/L 09/12/19 14:43 124-48-11.0 0.41 1
1,2-Dibromoethane (EDB)ND ug/L 09/12/19 14:43 106-93-41.0 0.26 1
Dibromomethane ND ug/L 09/12/19 14:43 74-95-31.0 0.46 1
1,2-Dichlorobenzene ND ug/L 09/12/19 14:43 95-50-11.0 0.29 1
1,3-Dichlorobenzene ND ug/L 09/12/19 14:43 541-73-11.0 0.22 1
1,4-Dichlorobenzene ND ug/L 09/12/19 14:43 106-46-71.0 0.26 1
Dichlorodifluoromethane ND ug/L 09/12/19 14:43 75-71-81.0 0.23 1
1,1-Dichloroethane ND ug/L 09/12/19 14:43 75-34-31.0 0.27 1
1,2-Dichloroethane ND ug/L 09/12/19 14:43 107-06-21.0 0.34 1
1,1-Dichloroethene ND ug/L 09/12/19 14:43 75-35-41.0 0.24 1
cis-1,2-Dichloroethene ND ug/L 09/12/19 14:43 156-59-21.0 0.29 1
trans-1,2-Dichloroethene ND ug/L 09/12/19 14:43 156-60-51.0 0.25 1
1,2-Dichloropropane ND ug/L 09/12/19 14:43 78-87-51.0 0.19 1
1,3-Dichloropropane ND ug/L 09/12/19 14:43 142-28-91.0 0.16 1
2,2-Dichloropropane ND ug/L 09/12/19 14:43 594-20-71.0 0.27 1
1,1-Dichloropropene ND ug/L 09/12/19 14:43 563-58-61.0 0.21 1
cis-1,3-Dichloropropene ND ug/L 09/12/19 14:43 10061-01-5 L11.0 0.30 1
trans-1,3-Dichloropropene ND ug/L 09/12/19 14:43 10061-02-61.0 0.31 1
Diisopropyl ether ND ug/L 09/12/19 14:43 108-20-31.0 0.22 1
Ethylbenzene ND ug/L 09/12/19 14:43 100-41-41.0 0.26 1
Hexachloro-1,3-butadiene ND ug/L 09/12/19 14:43 87-68-31.0 0.44 1
2-Hexanone ND ug/L 09/12/19 14:43 591-78-65.0 0.57 1
p-Isopropyltoluene ND ug/L 09/12/19 14:43 99-87-61.0 0.21 1
Methylene Chloride ND ug/L 09/12/19 14:43 75-09-25.0 3.7 1
4-Methyl-2-pentanone (MIBK)ND ug/L 09/12/19 14:43 108-10-15.0 4.5 1
Methyl-tert-butyl ether ND ug/L 09/12/19 14:43 1634-04-41.0 0.28 1
Naphthalene ND ug/L 09/12/19 14:43 91-20-31.0 0.35 1
Styrene ND ug/L 09/12/19 14:43 100-42-51.0 0.27 1
1,1,1,2-Tetrachloroethane ND ug/L 09/12/19 14:43 630-20-61.0 0.34 1
1,1,2,2-Tetrachloroethane ND ug/L 09/12/19 14:43 79-34-51.0 0.22 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 45
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92444875
DCY.001
Sample: DUP-4 Lab ID: 92444875005 Collected: 09/09/19 00:00 Received: 09/10/19 07:11 Matrix: Water
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D8260D MSV Low Level
Tetrachloroethene ND ug/L 09/12/19 14:43 127-18-41.0 0.16 1
Toluene ND ug/L 09/12/19 14:43 108-88-31.0 0.24 1
1,2,3-Trichlorobenzene ND ug/L 09/12/19 14:43 87-61-61.0 0.34 1
1,2,4-Trichlorobenzene ND ug/L 09/12/19 14:43 120-82-11.0 0.22 1
1,1,1-Trichloroethane ND ug/L 09/12/19 14:43 71-55-61.0 0.18 1
1,1,2-Trichloroethane ND ug/L 09/12/19 14:43 79-00-51.0 0.24 1
Trichloroethene ND ug/L 09/12/19 14:43 79-01-61.0 0.22 1
Trichlorofluoromethane ND ug/L 09/12/19 14:43 75-69-41.0 0.31 1
1,2,3-Trichloropropane ND ug/L 09/12/19 14:43 96-18-41.0 0.35 1
Vinyl acetate ND ug/L 09/12/19 14:43 108-05-42.0 1.4 1
Vinyl chloride ND ug/L 09/12/19 14:43 75-01-41.0 0.24 1
Xylene (Total)ND ug/L 09/12/19 14:43 1330-20-71.0 0.63 1
m&p-Xylene ND ug/L 09/12/19 14:43 179601-23-12.0 0.41 1
o-Xylene ND ug/L 09/12/19 14:43 95-47-61.0 0.22 1
Surrogates
4-Bromofluorobenzene (S)98 %09/12/19 14:43 460-00-470-130 1
1,2-Dichloroethane-d4 (S)83 %09/12/19 14:43 17060-07-070-130 1
Toluene-d8 (S)103 %09/12/19 14:43 2037-26-570-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92444875
DCY.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1345073
3015
EPA 6020B
Metals (ICPMS) 6020B
Associated Lab Samples: 92444875001, 92444875002, 92444875003, 92444875004, 92444875005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3450849-1
Associated Lab Samples:92444875001, 92444875002, 92444875003, 92444875004, 92444875005
Matrix: Water
AnalyzedMDL
Antimony ug/L ND 2.00 09/14/19 14:550.754
Arsenic ug/L ND 2.00 09/14/19 14:550.250
Beryllium ug/L ND 2.00 09/14/19 14:550.120
Cadmium ug/L ND 1.00 09/14/19 14:550.160
Chromium ug/L 0.654J 2.00 J09/14/19 14:550.540
Copper ug/L 2.80J 5.00 J09/14/19 14:550.520
Lead ug/L 0.523J 2.00 J09/14/19 14:550.240
Manganese ug/L ND 5.00 09/14/19 14:550.250
Nickel ug/L ND 2.00 09/14/19 14:550.350
Silver ug/L ND 2.00 09/14/19 14:550.310
Thallium ug/L ND 2.00 09/14/19 14:550.190
Zinc ug/L ND 25.0 09/14/19 14:552.56
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3450849-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3450849-3
Antimony ug/L 53.550.0 107 80.0-12010653.0 0.917 20
Arsenic ug/L 49.350.0 98.7 80.0-12010451.8 4.87 20
Beryllium ug/L 47.150.0 94.3 80.0-12095.447.7 1.17 20
Cadmium ug/L 50.450.0 101 80.0-12010351.7 2.50 20
Chromium ug/L 52.350.0 105 80.0-12010753.3 1.90 20
Copper ug/L 48.350.0 96.5 80.0-12097.148.6 0.598 20
Lead ug/L 50.850.0 102 80.0-12010050.1 1.27 20
Manganese ug/L 50.650.0 101 80.0-12010552.3 3.26 20
Nickel ug/L 53.050.0 106 80.0-12010854.2 2.28 20
Silver ug/L 50.850.0 102 80.0-12010150.3 0.898 20
Thallium ug/L 50.050.0 99.9 80.0-12010050.0 0.0537 20
Zinc ug/L 51.250.0 102 80.0-12011557.5 11.6 20
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3450849-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1138430-01
R3450849-6
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Antimony ug/L 50.0 106 75.0-125110 3.51 2050.0ND 53.2 55.1
Arsenic ug/L 50.0 98.2 75.0-12598.6 0.378 2050.0ND 49.6 49.8
Beryllium ug/L 50.0 96.3 75.0-12597.0 0.700 2050.0ND 48.1 48.5
Cadmium ug/L 50.0 106 75.0-125109 2.66 2050.0ND 53.2 54.7
Chromium ug/L 50.0 100 75.0-125103 2.21 2050.0ND 50.2 51.4
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
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Huntersville, NC 28078
[phone]
Page 25 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92444875
DCY.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3450849-5MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1138430-01
R3450849-6
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Copper ug/L 50.0 90.2 75.0-12591.2 1.10 2050.0ND 47.1 47.7
Lead ug/L 50.0 98.1 75.0-12599.5 1.32 2050.0ND 50.9 51.6
Manganese ug/L 50.0 98.2 75.0-12597.7 0.467 2050.0ND 52.5 52.2
Nickel ug/L 50.0 97.1 75.0-125102 4.55 2050.0ND 49.9 52.2
Silver ug/L 50.0 101 75.0-125103 1.64 2050.0ND 50.5 51.3
Thallium ug/L 50.0 103 75.0-125103 0.761 2050.0ND 51.3 51.6
Zinc ug/L 50.0 97.5 75.0-125107 9.03 2050.0ND 48.8 53.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92444875
DCY.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1344922
7470A
EPA 7470A
Mercury 7470A
Associated Lab Samples: 92444875001, 92444875002, 92444875003, 92444875004, 92444875005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3450879-1
Associated Lab Samples:92444875001, 92444875002, 92444875003, 92444875004, 92444875005
Matrix: Water
AnalyzedMDL
Mercury ug/L ND 0.200 09/15/19 19:550.0490
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3450879-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3450879-3
Mercury ug/L 2.953.00 98.3 80.0-1201003.00 1.68 20
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 27 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92444875
DCY.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
497337
EPA 8260D
EPA 8260D
8260D MSV Low Level
Associated Lab Samples: 92444875001, 92444875002, 92444875003, 92444875004, 92444875005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2677953
Associated Lab Samples:92444875001, 92444875002, 92444875003, 92444875004, 92444875005
Matrix: Water
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/L ND 1.0 09/12/19 11:290.34
1,1,1-Trichloroethane ug/L ND 1.0 09/12/19 11:290.18
1,1,2,2-Tetrachloroethane ug/L ND 1.0 09/12/19 11:290.22
1,1,2-Trichloroethane ug/L ND 1.0 09/12/19 11:290.24
1,1-Dichloroethane ug/L ND 1.0 09/12/19 11:290.27
1,1-Dichloroethene ug/L ND 1.0 09/12/19 11:290.24
1,1-Dichloropropene ug/L ND 1.0 09/12/19 11:290.21
1,2,3-Trichlorobenzene ug/L ND 1.0 09/12/19 11:290.34
1,2,3-Trichloropropane ug/L ND 1.0 09/12/19 11:290.35
1,2,4-Trichlorobenzene ug/L ND 1.0 09/12/19 11:290.22
1,2-Dibromo-3-chloropropane ug/L ND 5.0 09/12/19 11:290.26
1,2-Dibromoethane (EDB)ug/L ND 1.0 09/12/19 11:290.26
1,2-Dichlorobenzene ug/L ND 1.0 09/12/19 11:290.29
1,2-Dichloroethane ug/L ND 1.0 09/12/19 11:290.34
1,2-Dichloropropane ug/L ND 1.0 09/12/19 11:290.19
1,3-Dichlorobenzene ug/L ND 1.0 09/12/19 11:290.22
1,3-Dichloropropane ug/L ND 1.0 09/12/19 11:290.16
1,4-Dichlorobenzene ug/L ND 1.0 09/12/19 11:290.26
2,2-Dichloropropane ug/L ND 1.0 09/12/19 11:290.27
2-Butanone (MEK)ug/L ND 5.0 09/12/19 11:293.3
2-Chlorotoluene ug/L ND 1.0 09/12/19 11:290.20
2-Hexanone ug/L ND 5.0 09/12/19 11:290.57
4-Chlorotoluene ug/L ND 1.0 09/12/19 11:290.20
4-Methyl-2-pentanone (MIBK)ug/L ND 5.0 09/12/19 11:294.5
Acetone ug/L ND 25.0 09/12/19 11:296.2
Benzene ug/L ND 1.0 09/12/19 11:290.15
Bromobenzene ug/L ND 1.0 09/12/19 11:290.22
Bromochloromethane ug/L ND 1.0 09/12/19 11:290.34
Bromodichloromethane ug/L ND 1.0 09/12/19 11:290.26
Bromoform ug/L ND 1.0 09/12/19 11:290.62
Bromomethane ug/L ND 2.0 09/12/19 11:290.62
Carbon tetrachloride ug/L ND 1.0 09/12/19 11:290.22
Chlorobenzene ug/L ND 1.0 09/12/19 11:290.23
Chloroethane ug/L ND 1.0 09/12/19 11:290.49
Chloroform ug/L ND 5.0 09/12/19 11:292.3
Chloromethane ug/L ND 1.0 09/12/19 11:290.39
cis-1,2-Dichloroethene ug/L ND 1.0 09/12/19 11:290.29
cis-1,3-Dichloropropene ug/L ND 1.0 09/12/19 11:290.30
Dibromochloromethane ug/L ND 1.0 09/12/19 11:290.41
Dibromomethane ug/L ND 1.0 09/12/19 11:290.46
Dichlorodifluoromethane ug/L ND 1.0 09/12/19 11:290.23
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
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Page 28 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92444875
DCY.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2677953
Associated Lab Samples:92444875001, 92444875002, 92444875003, 92444875004, 92444875005
Matrix: Water
AnalyzedMDL
Diisopropyl ether ug/L ND 1.0 09/12/19 11:290.22
Ethylbenzene ug/L ND 1.0 09/12/19 11:290.26
Hexachloro-1,3-butadiene ug/L ND 1.0 09/12/19 11:290.44
m&p-Xylene ug/L ND 2.0 09/12/19 11:290.41
Methyl-tert-butyl ether ug/L ND 1.0 09/12/19 11:290.28
Methylene Chloride ug/L ND 5.0 09/12/19 11:293.7
Naphthalene ug/L ND 1.0 09/12/19 11:290.35
o-Xylene ug/L ND 1.0 09/12/19 11:290.22
p-Isopropyltoluene ug/L ND 1.0 09/12/19 11:290.21
Styrene ug/L ND 1.0 09/12/19 11:290.27
Tetrachloroethene ug/L ND 1.0 09/12/19 11:290.16
Toluene ug/L ND 1.0 09/12/19 11:290.24
trans-1,2-Dichloroethene ug/L ND 1.0 09/12/19 11:290.25
trans-1,3-Dichloropropene ug/L ND 1.0 09/12/19 11:290.31
Trichloroethene ug/L ND 1.0 09/12/19 11:290.22
Trichlorofluoromethane ug/L ND 1.0 09/12/19 11:290.31
Vinyl acetate ug/L ND 2.0 09/12/19 11:291.4
Vinyl chloride ug/L ND 1.0 09/12/19 11:290.24
Xylene (Total)ug/L ND 1.0 09/12/19 11:290.63
1,2-Dichloroethane-d4 (S)%81 70-130 09/12/19 11:29
4-Bromofluorobenzene (S)%99 70-130 09/12/19 11:29
Toluene-d8 (S)%101 70-130 09/12/19 11:29
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2677954LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/L 56.250 112 70-130
1,1,1-Trichloroethane ug/L 53.850 108 70-130
1,1,2,2-Tetrachloroethane ug/L 54.150 108 70-130
1,1,2-Trichloroethane ug/L 60.150 120 70-130
1,1-Dichloroethane ug/L 53.950 108 70-130
1,1-Dichloroethene ug/L 55.250 110 70-130
1,1-Dichloropropene ug/L 56.050 112 70-130
1,2,3-Trichlorobenzene ug/L 56.550 113 70-130
1,2,3-Trichloropropane ug/L 60.650 121 70-130
1,2,4-Trichlorobenzene ug/L 56.950 114 70-130
1,2-Dibromo-3-chloropropane ug/L 57.650 115 70-130
1,2-Dibromoethane (EDB)ug/L 55.750 111 70-130
1,2-Dichlorobenzene ug/L 53.750 107 70-130
1,2-Dichloroethane ug/L 45.950 92 70-130
1,2-Dichloropropane ug/L 56.850 114 70-130
1,3-Dichlorobenzene ug/L 51.850 104 70-130
1,3-Dichloropropane ug/L 59.850 120 70-131
1,4-Dichlorobenzene ug/L 52.350 105 70-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 29 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92444875
DCY.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2677954LABORATORY CONTROL SAMPLE:
LCSSpike
2,2-Dichloropropane ug/L 54.250 108 69-130
2-Butanone (MEK)ug/L 106100 106 64-135
2-Chlorotoluene ug/L 51.650 103 70-130
2-Hexanone ug/L 120100 120 66-135
4-Chlorotoluene ug/L 51.950 104 70-130
4-Methyl-2-pentanone (MIBK)ug/L 125100 125 70-130
Acetone ug/L 131100 131 61-157
Benzene ug/L 59.350 119 70-130
Bromobenzene ug/L 53.550 107 70-130
Bromochloromethane ug/L 53.050 106 70-130
Bromodichloromethane ug/L 54.150 108 70-130
Bromoform ug/L 57.250 114 70-130
Bromomethane ug/L 42.950 86 38-130
Carbon tetrachloride ug/L 54.850 110 70-130
Chlorobenzene ug/L 51.050 102 70-130
Chloroethane ug/L 52.950 106 37-142
Chloroform ug/L 50.750 101 70-130
Chloromethane ug/L 52.850 106 48-130
cis-1,2-Dichloroethene ug/L 52.450 105 70-130
cis-1,3-Dichloropropene ug/L 65.8 L150132 70-130
Dibromochloromethane ug/L 56.750 113 70-130
Dibromomethane ug/L 55.850 112 70-130
Dichlorodifluoromethane ug/L 49.350 99 53-134
Diisopropyl ether ug/L 60.150 120 70-135
Ethylbenzene ug/L 52.350 105 70-130
Hexachloro-1,3-butadiene ug/L 59.650 119 68-132
m&p-Xylene ug/L 107100 107 70-130
Methyl-tert-butyl ether ug/L 49.950 100 70-130
Methylene Chloride ug/L 50.650 101 67-132
Naphthalene ug/L 54.850 110 70-130
o-Xylene ug/L 53.850 108 70-131
p-Isopropyltoluene ug/L 56.250 112 70-130
Styrene ug/L 56.550 113 70-130
Tetrachloroethene ug/L 55.650 111 69-130
Toluene ug/L 54.750 109 70-130
trans-1,2-Dichloroethene ug/L 53.750 107 70-130
trans-1,3-Dichloropropene ug/L 63.550 127 70-130
Trichloroethene ug/L 55.950 112 70-130
Trichlorofluoromethane ug/L 45.550 91 63-130
Vinyl acetate ug/L 104100 104 55-143
Vinyl chloride ug/L 54.850 110 70-131
Xylene (Total)ug/L 161150 107 70-130
1,2-Dichloroethane-d4 (S)%86 70-130
4-Bromofluorobenzene (S)%98 70-130
Toluene-d8 (S)%102 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92444875
DCY.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2677956MATRIX SPIKE SAMPLE:
MSSpike
Result
92444477003
1,1,1,2-Tetrachloroethane ug/L 23.720 118 73-134ND
1,1,1-Trichloroethane ug/L 22.720 114 82-143ND
1,1,2,2-Tetrachloroethane ug/L 23.220 116 70-136ND
1,1,2-Trichloroethane ug/L 21.520 107 70-135ND
1,1-Dichloroethane ug/L 23.920 119 70-139ND
1,1-Dichloroethene ug/L 23.220 116 70-154ND
1,1-Dichloropropene ug/L 23.420 117 70-149ND
1,2,3-Trichlorobenzene ug/L 25.220 126 70-135ND
1,2,3-Trichloropropane ug/L 23.520 117 71-137ND
1,2,4-Trichlorobenzene ug/L 25.320 126 73-140ND
1,2-Dibromo-3-chloropropane ug/L 24.220 121 65-134ND
1,2-Dibromoethane (EDB)ug/L 23.720 118 70-137ND
1,2-Dichlorobenzene ug/L 23.520 117 70-133ND
1,2-Dichloroethane ug/L 21.520 107 70-137ND
1,2-Dichloropropane ug/L 24.920 124 70-140ND
1,3-Dichlorobenzene ug/L 24.020 120 70-135ND
1,3-Dichloropropane ug/L 25.520 128 70-143ND
1,4-Dichlorobenzene ug/L 22.220 111 70-133ND
2,2-Dichloropropane ug/L 21.120 105 61-148ND
2-Butanone (MEK)ug/L 91.4 M140149 60-13931.8
2-Chlorotoluene ug/L 23.420 117 70-144ND
2-Hexanone ug/L 56.2 M140140 65-138ND
4-Chlorotoluene ug/L 23.220 116 70-137ND
4-Methyl-2-pentanone (MIBK)ug/L 44.340 108 65-135ND
Acetone ug/L 24940 107 60-148206
Benzene ug/L 25.220 126 70-151ND
Bromobenzene ug/L 24.520 122 70-136ND
Bromochloromethane ug/L 23.320 116 70-141ND
Bromodichloromethane ug/L 25.020 125 70-138ND
Bromoform ug/L 23.420 117 63-130ND
Bromomethane ug/L 21.120 106 15-152ND
Carbon tetrachloride ug/L 23.720 118 70-143ND
Chlorobenzene ug/L 23.620 118 70-138ND
Chloroethane ug/L 20.220 101 52-163ND
Chloroform ug/L 22.320 112 70-139ND
Chloromethane ug/L 25.520 128 41-139ND
cis-1,2-Dichloroethene ug/L 23.420 117 70-141ND
cis-1,3-Dichloropropene ug/L 22.020 110 70-137ND
Dibromochloromethane ug/L 24.120 120 70-134ND
Dibromomethane ug/L 25.020 125 70-138ND
Dichlorodifluoromethane ug/L 23.520 117 47-155ND
Diisopropyl ether ug/L 23.020 115 63-144ND
Ethylbenzene ug/L 25.120 126 66-153ND
Hexachloro-1,3-butadiene ug/L 25.620 128 65-149ND
m&p-Xylene ug/L 49.240 123 69-152ND
Methyl-tert-butyl ether ug/L 16.920 85 54-156ND
Methylene Chloride ug/L 20.620 103 42-159ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92444875
DCY.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2677956MATRIX SPIKE SAMPLE:
MSSpike
Result
92444477003
Naphthalene ug/L 25.020 125 61-148ND
o-Xylene ug/L 24.820 124 70-148ND
p-Isopropyltoluene ug/L 23.620 118 70-146ND
Styrene ug/L 25.020 125 70-135ND
Tetrachloroethene ug/L 25.720 129 59-143ND
Toluene ug/L 22.620 113 59-148ND
trans-1,2-Dichloroethene ug/L 21.420 107 70-146ND
trans-1,3-Dichloropropene ug/L 22.220 111 70-135ND
Trichloroethene ug/L 25.120 126 70-147ND
Trichlorofluoromethane ug/L 20.620 103 70-148ND
Vinyl acetate ug/L 36.340 91 49-151ND
Vinyl chloride ug/L 25.320 126 70-156ND
Xylene (Total)ug/L 74.060 123 63-158ND
1,2-Dichloroethane-d4 (S)%93 70-130
4-Bromofluorobenzene (S)%99 70-130
Toluene-d8 (S)%92 70-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92444468002
2677955SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/L ND 30ND
1,1,1-Trichloroethane ug/L ND 30ND
1,1,2,2-Tetrachloroethane ug/L ND 30ND
1,1,2-Trichloroethane ug/L ND 30ND
1,1-Dichloroethane ug/L ND 30ND
1,1-Dichloroethene ug/L ND 30ND
1,1-Dichloropropene ug/L ND 30ND
1,2,3-Trichlorobenzene ug/L ND 30ND
1,2,3-Trichloropropane ug/L ND 30ND
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dibromo-3-chloropropane ug/L ND 30ND
1,2-Dibromoethane (EDB)ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,2-Dichloroethane ug/L ND 30ND
1,2-Dichloropropane ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,3-Dichloropropane ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
2,2-Dichloropropane ug/L ND 30ND
2-Butanone (MEK)ug/L ND 30ND
2-Chlorotoluene ug/L ND 30ND
2-Hexanone ug/L ND 30ND
4-Chlorotoluene ug/L ND 30ND
4-Methyl-2-pentanone (MIBK)ug/L ND 30ND
Acetone ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92444875
DCY.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92444468002
2677955SAMPLE DUPLICATE:
Benzene ug/L ND 30ND
Bromobenzene ug/L ND 30ND
Bromochloromethane ug/L ND 30ND
Bromodichloromethane ug/L ND 30ND
Bromoform ug/L ND 30ND
Bromomethane ug/L ND 30ND
Carbon tetrachloride ug/L ND 30ND
Chlorobenzene ug/L ND 30ND
Chloroethane ug/L ND 30ND
Chloroform ug/L ND 30ND
Chloromethane ug/L ND 30ND
cis-1,2-Dichloroethene ug/L ND 30ND
cis-1,3-Dichloropropene ug/L ND 30ND
Dibromochloromethane ug/L ND 30ND
Dibromomethane ug/L ND 30ND
Dichlorodifluoromethane ug/L ND 30ND
Diisopropyl ether ug/L ND 30ND
Ethylbenzene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
m&p-Xylene ug/L ND 30ND
Methyl-tert-butyl ether ug/L ND 30ND
Methylene Chloride ug/L ND 30ND
Naphthalene ug/L ND 30ND
o-Xylene ug/L ND 30ND
p-Isopropyltoluene ug/L ND 30ND
Styrene ug/L ND 30ND
Tetrachloroethene ug/L ND 30ND
Toluene ug/L ND 30ND
trans-1,2-Dichloroethene ug/L ND 30ND
trans-1,3-Dichloropropene ug/L ND 30ND
Trichloroethene ug/L ND 30ND
Trichlorofluoromethane ug/L ND 30ND
Vinyl acetate ug/L ND 30ND
Vinyl chloride ug/L ND 30ND
Xylene (Total)ug/L ND 30ND
1,2-Dichloroethane-d4 (S)%8179
4-Bromofluorobenzene (S)%10499
Toluene-d8 (S)%92109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
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9800 Kincey Ave. Suite 100
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[phone]
Page 33 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92444875
DCY.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
497140
EPA 3510C
EPA 8270E
8270E Water MSSV RVE
Associated Lab Samples: 92444875001, 92444875002, 92444875003, 92444875004, 92444875005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2676847
Associated Lab Samples:92444875001, 92444875002, 92444875003, 92444875004, 92444875005
Matrix: Water
AnalyzedMDL
1,2,4-Trichlorobenzene ug/L ND 10.0 09/11/19 16:411.5
1,2-Dichlorobenzene ug/L ND 10.0 09/11/19 16:411.3
1,3-Dichlorobenzene ug/L ND 10.0 09/11/19 16:411.5
1,4-Dichlorobenzene ug/L ND 10.0 09/11/19 16:412.1
1-Methylnaphthalene ug/L ND 10.0 09/11/19 16:411.4
2,2'-Oxybis(1-chloropropane)ug/L ND 10.0 09/11/19 16:412.8
2,4,5-Trichlorophenol ug/L ND 10.0 09/11/19 16:411.4
2,4,6-Trichlorophenol ug/L ND 10.0 09/11/19 16:411.5
2,4-Dichlorophenol ug/L ND 10.0 09/11/19 16:411.4
2,4-Dimethylphenol ug/L ND 10.0 09/11/19 16:411.4
2,4-Dinitrophenol ug/L ND 50.0 09/11/19 16:4140.5
2,4-Dinitrotoluene ug/L ND 10.0 09/11/19 16:411.2
2,6-Dinitrotoluene ug/L ND 10.0 09/11/19 16:411.4
2-Chloronaphthalene ug/L ND 10.0 09/11/19 16:411.5
2-Chlorophenol ug/L ND 10.0 09/11/19 16:411.2
2-Methylnaphthalene ug/L ND 10.0 09/11/19 16:411.4
2-Methylphenol(o-Cresol)ug/L ND 10.0 09/11/19 16:411.2
2-Nitroaniline ug/L ND 20.0 09/11/19 16:414.2
2-Nitrophenol ug/L ND 10.0 09/11/19 16:411.4
3&4-Methylphenol(m&p Cresol)ug/L ND 10.0 09/11/19 16:411.2
3,3'-Dichlorobenzidine ug/L ND 20.0 09/11/19 16:413.0
3-Nitroaniline ug/L ND 20.0 09/11/19 16:412.3
4,6-Dinitro-2-methylphenol ug/L ND 20.0 09/11/19 16:4115.2
4-Bromophenylphenyl ether ug/L ND 10.0 09/11/19 16:411.6
4-Chloro-3-methylphenol ug/L ND 20.0 09/11/19 16:412.8
4-Chloroaniline ug/L ND 20.0 09/11/19 16:412.8
4-Chlorophenylphenyl ether ug/L ND 10.0 09/11/19 16:411.6
4-Nitroaniline ug/L ND 20.0 09/11/19 16:412.2
4-Nitrophenol ug/L ND 50.0 09/11/19 16:413.5
Acenaphthene ug/L ND 10.0 09/11/19 16:411.6
Acenaphthylene ug/L ND 10.0 09/11/19 16:411.6
Aniline ug/L ND 10.0 09/11/19 16:411.9
Anthracene ug/L ND 10.0 09/11/19 16:411.7
Benzo(a)anthracene ug/L ND 10.0 09/11/19 16:411.8
Benzo(a)pyrene ug/L ND 10.0 09/11/19 16:412.1
Benzo(b)fluoranthene ug/L ND 10.0 09/11/19 16:411.9
Benzo(g,h,i)perylene ug/L ND 10.0 09/11/19 16:411.4
Benzo(k)fluoranthene ug/L ND 10.0 09/11/19 16:411.9
Benzoic Acid ug/L ND 50.0 09/11/19 16:4143.0
Benzyl alcohol ug/L ND 20.0 09/11/19 16:412.6
bis(2-Chloroethoxy)methane ug/L ND 10.0 09/11/19 16:411.8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 34 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92444875
DCY.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2676847
Associated Lab Samples:92444875001, 92444875002, 92444875003, 92444875004, 92444875005
Matrix: Water
AnalyzedMDL
bis(2-Chloroethyl) ether ug/L ND 10.0 09/11/19 16:411.8
bis(2-Ethylhexyl)phthalate ug/L ND 6.0 09/11/19 16:412.1
Butylbenzylphthalate ug/L ND 10.0 09/11/19 16:411.6
Chrysene ug/L ND 10.0 09/11/19 16:411.7
Di-n-butylphthalate ug/L ND 10.0 09/11/19 16:411.8
Di-n-octylphthalate ug/L ND 10.0 09/11/19 16:411.8
Dibenz(a,h)anthracene ug/L ND 10.0 09/11/19 16:411.6
Dibenzofuran ug/L ND 10.0 09/11/19 16:411.5
Diethylphthalate ug/L ND 10.0 09/11/19 16:412.4
Dimethylphthalate ug/L ND 10.0 09/11/19 16:411.6
Fluoranthene ug/L ND 10.0 09/11/19 16:411.7
Fluorene ug/L ND 10.0 09/11/19 16:411.6
Hexachloro-1,3-butadiene ug/L ND 10.0 09/11/19 16:412.0
Hexachlorobenzene ug/L ND 10.0 09/11/19 16:411.7
Hexachlorocyclopentadiene ug/L ND 10.0 09/11/19 16:411.7
Hexachloroethane ug/L ND 10.0 09/11/19 16:412.0
Indeno(1,2,3-cd)pyrene ug/L ND 10.0 09/11/19 16:411.6
Isophorone ug/L ND 10.0 09/11/19 16:411.6
N-Nitroso-di-n-propylamine ug/L ND 10.0 09/11/19 16:412.2
N-Nitrosodimethylamine ug/L ND 10.0 09/11/19 16:411.2
N-Nitrosodiphenylamine ug/L ND 10.0 09/11/19 16:411.7
Naphthalene ug/L ND 10.0 09/11/19 16:411.4
Nitrobenzene ug/L ND 10.0 09/11/19 16:412.1
Pentachlorophenol ug/L ND 25.0 09/11/19 16:412.2
Phenanthrene ug/L ND 10.0 09/11/19 16:411.7
Phenol ug/L ND 10.0 09/11/19 16:410.92
Pyrene ug/L ND 10.0 09/11/19 16:412.1
2,4,6-Tribromophenol (S)%88 10-137 09/11/19 16:41
2-Fluorobiphenyl (S)%80 13-130 09/11/19 16:41
2-Fluorophenol (S)%70 10-130 09/11/19 16:41
Nitrobenzene-d5 (S)%82 13-130 09/11/19 16:41
Phenol-d6 (S)%54 10-130 09/11/19 16:41
Terphenyl-d14 (S)%115 25-130 09/11/19 16:41
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2676848LABORATORY CONTROL SAMPLE:
LCSSpike
1,2,4-Trichlorobenzene ug/L 28.350 57 30-130
1,2-Dichlorobenzene ug/L 29.250 58 30-130
1,3-Dichlorobenzene ug/L 28.850 58 20-130
1,4-Dichlorobenzene ug/L 28.850 58 30-130
1-Methylnaphthalene ug/L 34.050 68 30-130
2,2'-Oxybis(1-chloropropane)ug/L 42.450 85 20-130
2,4,5-Trichlorophenol ug/L 31.650 63 40-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 35 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92444875
DCY.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2676848LABORATORY CONTROL SAMPLE:
LCSSpike
2,4,6-Trichlorophenol ug/L 32.550 65 40-130
2,4-Dichlorophenol ug/L 31.950 64 31-130
2,4-Dimethylphenol ug/L 32.150 64 30-130
2,4-Dinitrophenol ug/L 242250 97 30-130
2,4-Dinitrotoluene ug/L 42.450 85 49-130
2,6-Dinitrotoluene ug/L 35.950 72 50-130
2-Chloronaphthalene ug/L 28.750 57 30-130
2-Chlorophenol ug/L 32.950 66 30-130
2-Methylnaphthalene ug/L 35.750 71 30-130
2-Methylphenol(o-Cresol)ug/L 30.550 61 30-130
2-Nitroaniline ug/L 85.0100 85 40-130
2-Nitrophenol ug/L 31.650 63 20-130
3&4-Methylphenol(m&p Cresol)ug/L 31.050 62 20-130
3,3'-Dichlorobenzidine ug/L 88.4100 88 10-150
3-Nitroaniline ug/L 88.5100 88 40-130
4,6-Dinitro-2-methylphenol ug/L 106100 106 40-130
4-Bromophenylphenyl ether ug/L 44.850 90 30-130
4-Chloro-3-methylphenol ug/L 70.2100 70 30-130
4-Chloroaniline ug/L 72.7100 73 20-130
4-Chlorophenylphenyl ether ug/L 37.250 74 20-130
4-Nitroaniline ug/L 93.7100 94 40-130
4-Nitrophenol ug/L 180250 72 10-130
Acenaphthene ug/L 34.550 69 30-130
Acenaphthylene ug/L 34.650 69 30-130
Aniline ug/L 27.350 55 20-130
Anthracene ug/L 51.250 102 50-130
Benzo(a)anthracene ug/L 54.550 109 50-130
Benzo(a)pyrene ug/L 54.650 109 50-130
Benzo(b)fluoranthene ug/L 54.850 110 50-130
Benzo(g,h,i)perylene ug/L 54.050 108 50-130
Benzo(k)fluoranthene ug/L 54.450 109 50-130
Benzoic Acid ug/L 129250 51 10-130
Benzyl alcohol ug/L 62.9100 63 20-130
bis(2-Chloroethoxy)methane ug/L 34.750 69 30-130
bis(2-Chloroethyl) ether ug/L 35.250 70 30-130
bis(2-Ethylhexyl)phthalate ug/L 52.050 104 50-130
Butylbenzylphthalate ug/L 51.850 104 50-150
Chrysene ug/L 57.050 114 50-130
Di-n-butylphthalate ug/L 52.650 105 50-130
Di-n-octylphthalate ug/L 49.250 98 50-130
Dibenz(a,h)anthracene ug/L 54.250 108 40-130
Dibenzofuran ug/L 34.550 69 40-130
Diethylphthalate ug/L 45.650 91 40-130
Dimethylphthalate ug/L 41.850 84 40-130
Fluoranthene ug/L 55.750 111 30-130
Fluorene ug/L 38.850 78 20-130
Hexachloro-1,3-butadiene ug/L 28.950 58 10-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 36 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92444875
DCY.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2676848LABORATORY CONTROL SAMPLE:
LCSSpike
Hexachlorobenzene ug/L 40.850 82 30-130
Hexachlorocyclopentadiene ug/L 25.850 52 10-150
Hexachloroethane ug/L 28.950 58 10-130
Indeno(1,2,3-cd)pyrene ug/L 54.050 108 40-130
Isophorone ug/L 31.750 63 30-130
N-Nitroso-di-n-propylamine ug/L 36.950 74 30-130
N-Nitrosodimethylamine ug/L 31.650 63 10-130
N-Nitrosodiphenylamine ug/L 47.050 94 30-130
Naphthalene ug/L 35.050 70 20-130
Nitrobenzene ug/L 32.150 64 20-130
Pentachlorophenol ug/L 107100 107 10-140
Phenanthrene ug/L 50.750 101 50-130
Phenol ug/L 24.350 49 10-130
Pyrene ug/L 54.950 110 50-130
2,4,6-Tribromophenol (S)%89 10-137
2-Fluorobiphenyl (S)%60 13-130
2-Fluorophenol (S)%56 10-130
Nitrobenzene-d5 (S)%64 13-130
Phenol-d6 (S)%45 10-130
Terphenyl-d14 (S)%102 25-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2676849MATRIX SPIKE SAMPLE:
MSSpike
Result
92444875001
1,2,4-Trichlorobenzene ug/L 31.150 62 30-130ND
1,2-Dichlorobenzene ug/L 30.850 62 30-130ND
1,3-Dichlorobenzene ug/L 30.450 61 20-130ND
1,4-Dichlorobenzene ug/L 30.250 60 30-130ND
1-Methylnaphthalene ug/L 37.150 74 30-130ND
2,2'-Oxybis(1-chloropropane)ug/L 42.650 85 20-130ND
2,4,5-Trichlorophenol ug/L 33.850 68 40-130ND
2,4,6-Trichlorophenol ug/L 35.250 70 40-130ND
2,4-Dichlorophenol ug/L 33.450 67 31-130ND
2,4-Dimethylphenol ug/L 33.450 67 30-130ND
2,4-Dinitrophenol ug/L 250250 100 30-130ND
2,4-Dinitrotoluene ug/L 44.050 88 49-130ND
2,6-Dinitrotoluene ug/L 39.050 78 50-130ND
2-Chloronaphthalene ug/L 30.650 61 30-130ND
2-Chlorophenol ug/L 32.450 65 30-130ND
2-Methylnaphthalene ug/L 38.950 78 30-130ND
2-Methylphenol(o-Cresol)ug/L 30.850 62 30-130ND
2-Nitroaniline ug/L 90.5100 91 40-130ND
2-Nitrophenol ug/L 31.850 64 20-130ND
3&4-Methylphenol(m&p Cresol)ug/L 29.750 59 20-130ND
3,3'-Dichlorobenzidine ug/L 91.9100 92 10-150ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 37 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92444875
DCY.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2676849MATRIX SPIKE SAMPLE:
MSSpike
Result
92444875001
3-Nitroaniline ug/L 92.0100 92 40-130ND
4,6-Dinitro-2-methylphenol ug/L 106100 106 40-130ND
4-Bromophenylphenyl ether ug/L 45.550 91 30-130ND
4-Chloro-3-methylphenol ug/L 76.7100 77 30-130ND
4-Chloroaniline ug/L 76.7100 77 20-130ND
4-Chlorophenylphenyl ether ug/L 39.750 79 20-130ND
4-Nitroaniline ug/L 99.2100 99 40-130ND
4-Nitrophenol ug/L 163250 65 10-130ND
Acenaphthene ug/L 37.350 75 30-130ND
Acenaphthylene ug/L 37.750 75 30-130ND
Aniline ug/L 28.750 57 20-130ND
Anthracene ug/L 52.250 104 50-130ND
Benzo(a)anthracene ug/L 56.650 113 50-130ND
Benzo(a)pyrene ug/L 54.550 109 50-130ND
Benzo(b)fluoranthene ug/L 54.550 109 50-130ND
Benzo(g,h,i)perylene ug/L 56.450 113 50-130ND
Benzo(k)fluoranthene ug/L 55.950 112 50-130ND
Benzoic Acid ug/L 121250 48 10-130ND
Benzyl alcohol ug/L 62.7100 63 20-130ND
bis(2-Chloroethoxy)methane ug/L 35.550 71 30-130ND
bis(2-Chloroethyl) ether ug/L 35.350 71 30-130ND
bis(2-Ethylhexyl)phthalate ug/L 54.650 109 50-130ND
Butylbenzylphthalate ug/L 52.750 105 50-150ND
Chrysene ug/L 57.550 115 50-130ND
Di-n-butylphthalate ug/L 54.750 109 50-130ND
Di-n-octylphthalate ug/L 52.450 105 50-130ND
Dibenz(a,h)anthracene ug/L 56.450 113 40-130ND
Dibenzofuran ug/L 37.550 75 40-130ND
Diethylphthalate ug/L 47.450 95 40-130ND
Dimethylphthalate ug/L 43.650 87 40-130ND
Fluoranthene ug/L 56.850 114 30-130ND
Fluorene ug/L 41.650 83 20-130ND
Hexachloro-1,3-butadiene ug/L 31.050 62 10-130ND
Hexachlorobenzene ug/L 41.350 83 30-130ND
Hexachlorocyclopentadiene ug/L 28.250 56 10-150ND
Hexachloroethane ug/L 30.450 61 10-130ND
Indeno(1,2,3-cd)pyrene ug/L 55.950 112 40-130ND
Isophorone ug/L 34.750 69 30-130ND
N-Nitroso-di-n-propylamine ug/L 37.850 76 30-130ND
N-Nitrosodimethylamine ug/L 30.050 60 10-130ND
N-Nitrosodiphenylamine ug/L 48.050 96 30-130ND
Naphthalene ug/L 37.250 74 20-130ND
Nitrobenzene ug/L 33.450 67 20-130ND
Pentachlorophenol ug/L 106100 106 10-140ND
Phenanthrene ug/L 50.850 102 50-130ND
Phenol ug/L 21.850 44 10-130ND
Pyrene ug/L 55.850 112 50-130ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 38 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92444875
DCY.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2676849MATRIX SPIKE SAMPLE:
MSSpike
Result
92444875001
2,4,6-Tribromophenol (S)%95 10-137
2-Fluorobiphenyl (S)%68 13-130
2-Fluorophenol (S)%55 10-130
Nitrobenzene-d5 (S)%71 13-130
Phenol-d6 (S)%41 10-130
Terphenyl-d14 (S)%106 25-130
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92444875002
2676850SAMPLE DUPLICATE:
1,2,4-Trichlorobenzene ug/L ND 30ND
1,2-Dichlorobenzene ug/L ND 30ND
1,3-Dichlorobenzene ug/L ND 30ND
1,4-Dichlorobenzene ug/L ND 30ND
1-Methylnaphthalene ug/L ND 30ND
2,2'-Oxybis(1-chloropropane)ug/L ND 30ND
2,4,5-Trichlorophenol ug/L ND 30ND
2,4,6-Trichlorophenol ug/L ND 30ND
2,4-Dichlorophenol ug/L ND 30ND
2,4-Dimethylphenol ug/L ND 30ND
2,4-Dinitrophenol ug/L ND 30ND
2,4-Dinitrotoluene ug/L ND 30ND
2,6-Dinitrotoluene ug/L ND 30ND
2-Chloronaphthalene ug/L ND 30ND
2-Chlorophenol ug/L ND 30ND
2-Methylnaphthalene ug/L ND 30ND
2-Methylphenol(o-Cresol)ug/L ND 30ND
2-Nitroaniline ug/L ND 30ND
2-Nitrophenol ug/L ND 30ND
3&4-Methylphenol(m&p Cresol)ug/L ND 30ND
3,3'-Dichlorobenzidine ug/L ND 30ND
3-Nitroaniline ug/L ND 30ND
4,6-Dinitro-2-methylphenol ug/L ND 30ND
4-Bromophenylphenyl ether ug/L ND 30ND
4-Chloro-3-methylphenol ug/L ND 30ND
4-Chloroaniline ug/L ND 30ND
4-Chlorophenylphenyl ether ug/L ND 30ND
4-Nitroaniline ug/L ND 30ND
4-Nitrophenol ug/L ND 30ND
Acenaphthene ug/L ND 30ND
Acenaphthylene ug/L ND 30ND
Aniline ug/L ND 30ND
Anthracene ug/L ND 30ND
Benzo(a)anthracene ug/L ND 30ND
Benzo(a)pyrene ug/L ND 30ND
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 39 of 45
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92444875
DCY.001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92444875002
2676850SAMPLE DUPLICATE:
Benzo(b)fluoranthene ug/L ND 30ND
Benzo(g,h,i)perylene ug/L ND 30ND
Benzo(k)fluoranthene ug/L ND 30ND
Benzoic Acid ug/L ND 30ND
Benzyl alcohol ug/L ND 30ND
bis(2-Chloroethoxy)methane ug/L ND 30ND
bis(2-Chloroethyl) ether ug/L ND 30ND
bis(2-Ethylhexyl)phthalate ug/L ND 30ND
Butylbenzylphthalate ug/L ND 30ND
Chrysene ug/L ND 30ND
Di-n-butylphthalate ug/L ND 30ND
Di-n-octylphthalate ug/L ND 30ND
Dibenz(a,h)anthracene ug/L ND 30ND
Dibenzofuran ug/L ND 30ND
Diethylphthalate ug/L ND 30ND
Dimethylphthalate ug/L ND 30ND
Fluoranthene ug/L ND 30ND
Fluorene ug/L ND 30ND
Hexachloro-1,3-butadiene ug/L ND 30ND
Hexachlorobenzene ug/L ND 30ND
Hexachlorocyclopentadiene ug/L ND 30ND
Hexachloroethane ug/L ND 30ND
Indeno(1,2,3-cd)pyrene ug/L ND 30ND
Isophorone ug/L ND 30ND
N-Nitroso-di-n-propylamine ug/L ND 30ND
N-Nitrosodimethylamine ug/L ND 30ND
N-Nitrosodiphenylamine ug/L ND 30ND
Naphthalene ug/L ND 30ND
Nitrobenzene ug/L ND 30ND
Pentachlorophenol ug/L ND 30ND
Phenanthrene ug/L ND 30ND
Phenol ug/L ND 30ND
Pyrene ug/L ND 30ND
2,4,6-Tribromophenol (S)%8773
2-Fluorobiphenyl (S)%7569
2-Fluorophenol (S)%5956
Nitrobenzene-d5 (S)%7870
Phenol-d6 (S)%4339
Terphenyl-d14 (S)%11592
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
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Page 40 of 45
#=QL#
QUALIFIERS
Pace Project No.:
Project:
92444875
DCY.001
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical NationalPAN
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
Analyte was detected in the associated method blank.B
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.L1
Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
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Page 41 of 45
#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92444875
DCY.001
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92444875001 1345073 1345073MW-1 3015 EPA 6020B
92444875002 1345073 1345073MW-2 3015 EPA 6020B
92444875003 1345073 1345073MW-3 3015 EPA 6020B
92444875004 1345073 1345073MW-4 3015 EPA 6020B
92444875005 1345073 1345073DUP-4 3015 EPA 6020B
92444875001 1344922 1344922MW-1 7470A EPA 7470A
92444875002 1344922 1344922MW-2 7470A EPA 7470A
92444875003 1344922 1344922MW-3 7470A EPA 7470A
92444875004 1344922 1344922MW-4 7470A EPA 7470A
92444875005 1344922 1344922DUP-4 7470A EPA 7470A
92444875001 497140 497297MW-1 EPA 3510C EPA 8270E
92444875002 497140 497297MW-2 EPA 3510C EPA 8270E
92444875003 497140 497297MW-3 EPA 3510C EPA 8270E
92444875004 497140 497297MW-4 EPA 3510C EPA 8270E
92444875005 497140 497297DUP-4 EPA 3510C EPA 8270E
92444875001 497337MW-1 EPA 8260D
92444875002 497337MW-2 EPA 8260D
92444875003 497337MW-3 EPA 8260D
92444875004 497337MW-4 EPA 8260D
92444875005 497337DUP-4 EPA 8260D
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/17/2019 09:27 PM
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[phone]
Page 42 of 45
Page 43 of 45
Page 44 of 45
Page 45 of 45
#=CL#
September 24, 2019
LIMS USE: FR - BRETT LAWRENCE
LIMS OBJECT ID: 92445872
92445872
Project:
Pace Project No.:
RE:
Brett LawrenceHart & Hickman2923 South Tryon St.Suite 100Charlotte, NC 28203
DCY-001
Dear Brett Lawrence:
Enclosed are the analytical results for sample(s) received by the laboratory on September 17, 2019.
The results relate only to the samples included in this report. Results reported herein conform to themost current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Godwin
[e-mail]
Project Manager1(704)875-9092
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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[phone]
Page 1 of 44
#=CP#
CERTIFICATIONS
Pace Project No.:
Project:
92445872
DCY-001
Pace Analytical National Certification IDs
12065 Lebanon Road, Mt. Juliet, TN 37122
Alabama Certification #: 40660
Alaska Certification 17-026
Arizona Certification #: AZ0612
Arkansas Certification #: 88-0469
California Certification #: 2932
Canada Certification #: 1461.01
Colorado Certification #: TN00003
Connecticut Certification #: PH-0197
DOD Certification: #1461.01
EPA# TN00003
Florida Certification #: E87487
Georgia DW Certification #: 923
Georgia Certification: NELAP
Idaho Certification #: TN00003
Illinois Certification #: 200008
Indiana Certification #: C-TN-01
Iowa Certification #: 364
Kansas Certification #: E-10277
Kentucky UST Certification #: 16
Kentucky Certification #: 90010
Louisiana Certification #: AI30792
Louisiana DW Certification #: LA180010
Maine Certification #: TN0002
Maryland Certification #: 324
Massachusetts Certification #: M-TN003
Michigan Certification #: 9958
Minnesota Certification #: 047-999-395
Mississippi Certification #: TN00003
Missouri Certification #: 340
Montana Certification #: CERT0086
Nebraska Certification #: NE-OS-15-05
Nevada Certification #: TN-03-2002-34
New Hampshire Certification #: 2975
New Jersey Certification #: TN002
New Mexico DW Certification
New York Certification #: 11742
North Carolina Aquatic Toxicity Certification #: 41
North Carolina Drinking Water Certification #: 21704
North Carolina Environmental Certificate #: 375
North Dakota Certification #: R-140
Ohio VAP Certification #: CL0069
Oklahoma Certification #: 9915
Oregon Certification #: TN200002
Pennsylvania Certification #: 68-02979
Rhode Island Certification #: LAO00356
South Carolina Certification #: 84004
South Dakota Certification
Tennessee DW/Chem/Micro Certification #: 2006
Texas Certification #: T 104704245-17-14
Texas Mold Certification #: LAB0152
USDA Soil Permit #: P330-15-00234
Utah Certification #: TN00003
Virginia Certification #: VT2006
Vermont Dept. of Health: ID# VT-2006
Virginia Certification #: 460132
Washington Certification #: C847
West Virginia Certification #: 233
Wisconsin Certification #: 9980939910
Wyoming UST Certification #: via A2LA 2926.01
A2LA-ISO 17025 Certification #: 1461.01
A2LA-ISO 17025 Certification #: 1461.02
AIHA-LAP/LLC EMLAP Certification #:100789
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
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#=SS#
SAMPLE SUMMARY
Pace Project No.:
Project:
92445872
DCY-001
Lab ID Sample ID Matrix Date Collected Date Received
92445872001 P1 Solid 09/16/19 10:00 09/17/19 12:13
92445872002 P3 Solid 09/16/19 11:00 09/17/19 12:13
92445872003 P4A Solid 09/16/19 12:00 09/17/19 12:13
92445872004 P4B Solid 09/16/19 12:35 09/17/19 12:13
92445872005 P4C Solid 09/16/19 13:00 09/17/19 12:13
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
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Page 3 of 44
#=SA#
SAMPLE ANALYTE COUNT
Pace Project No.:
Project:
92445872
DCY-001
Lab ID Sample ID Method
Analytes
Reported LaboratoryAnalysts
92445872001 P1 EPA 6020B 7 PANJPD
EPA 7471B 1 PANTCT
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANJHH
92445872002 P3 EPA 6020B 7 PANJPD
EPA 7471B 1 PANTCT
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANJHH
92445872003 P4A EPA 6020B 7 PANJPD
EPA 7471B 1 PANTCT
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANJHH
92445872004 P4B EPA 6020B 7 PANJPD
EPA 7471B 1 PANTCT
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANJHH
92445872005 P4C EPA 6020B 7 PANJPD
EPA 7471B 1 PANTCT
EPA 8270E 75 PASI-CBPJ
EPA 8260D 70 PASI-CCL
ASTM D2974-87 1 PASI-CKDF
SM 2540G 1 PANJHH
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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Huntersville, NC 28078
[phone]
Page 4 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92445872
DCY-001
Sample: P1 Lab ID: 92445872001 Collected: 09/16/19 10:00 Received: 09/17/19 12:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051Metals (ICPMS) 6020B
Arsenic 7.43 mg/kg 09/21/19 14:31 7440-38-209/21/19 11:230.570 0.143 5
Barium 88.6 mg/kg 09/21/19 14:31 7440-39-309/21/19 11:231.14 0.182 5
Cadmium 0.0959J mg/kg 09/21/19 14:31 7440-43-9 PH09/21/19 11:230.570 0.0912 5
Chromium 83.8 mg/kg 09/21/19 14:31 7440-47-3 MH09/21/19 11:231.14 0.308 5
Lead 4.48 mg/kg 09/21/19 14:31 7439-92-1 PH09/21/19 11:230.570 0.137 5
Selenium ND mg/kg 09/21/19 14:31 7782-49-2 PH09/21/19 11:230.570 0.217 5
Silver ND mg/kg 09/21/19 14:31 7440-22-409/21/19 11:230.570 0.177 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 0.0109J mg/kg 09/19/19 20:08 7439-97-609/19/19 12:510.0342 0.00319 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 09/18/19 14:33 83-32-909/18/19 08:32383 98.5 1
Acenaphthylene ND ug/kg 09/18/19 14:33 208-96-809/18/19 08:32383 90.6 1
Aniline ND ug/kg 09/18/19 14:33 62-53-309/18/19 08:32383 85.9 1
Anthracene ND ug/kg 09/18/19 14:33 120-12-709/18/19 08:32383 99.3 1
Benzo(a)anthracene ND ug/kg 09/18/19 14:33 56-55-309/18/19 08:32383 122 1
Benzo(a)pyrene ND ug/kg 09/18/19 14:33 50-32-809/18/19 08:32383 166 1
Benzo(b)fluoranthene ND ug/kg 09/18/19 14:33 205-99-209/18/19 08:32383 154 1
Benzo(g,h,i)perylene ND ug/kg 09/18/19 14:33 191-24-209/18/19 08:32383 150 1
Benzo(k)fluoranthene ND ug/kg 09/18/19 14:33 207-08-909/18/19 08:32383 161 1
Benzoic Acid ND ug/kg 09/18/19 14:33 65-85-009/18/19 08:321910 413 1
Benzyl alcohol ND ug/kg 09/18/19 14:33 100-51-609/18/19 08:32765 203 1
4-Bromophenylphenyl ether ND ug/kg 09/18/19 14:33 101-55-309/18/19 08:32383 100 1
Butylbenzylphthalate ND ug/kg 09/18/19 14:33 85-68-709/18/19 08:32383 102 1
4-Chloro-3-methylphenol ND ug/kg 09/18/19 14:33 59-50-709/18/19 08:32765 233 1
4-Chloroaniline ND ug/kg 09/18/19 14:33 106-47-809/18/19 08:321910 234 1
bis(2-Chloroethoxy)methane ND ug/kg 09/18/19 14:33 111-91-109/18/19 08:32383 102 1
bis(2-Chloroethyl) ether ND ug/kg 09/18/19 14:33 111-44-409/18/19 08:32383 81.3 1
2-Chloronaphthalene ND ug/kg 09/18/19 14:33 91-58-709/18/19 08:32383 85.2 1
2-Chlorophenol ND ug/kg 09/18/19 14:33 95-57-809/18/19 08:32383 89.1 1
4-Chlorophenylphenyl ether ND ug/kg 09/18/19 14:33 7005-72-309/18/19 08:32383 99.4 1
Chrysene ND ug/kg 09/18/19 14:33 218-01-909/18/19 08:32383 111 1
Dibenz(a,h)anthracene ND ug/kg 09/18/19 14:33 53-70-309/18/19 08:32383 153 1
Dibenzofuran ND ug/kg 09/18/19 14:33 132-64-909/18/19 08:32383 95.7 1
1,2-Dichlorobenzene ND ug/kg 09/18/19 14:33 95-50-109/18/19 08:32383 82.8 1
1,3-Dichlorobenzene ND ug/kg 09/18/19 14:33 541-73-109/18/19 08:32383 86.2 1
1,4-Dichlorobenzene ND ug/kg 09/18/19 14:33 106-46-709/18/19 08:32383 84.2 1
3,3'-Dichlorobenzidine ND ug/kg 09/18/19 14:33 91-94-109/18/19 08:321910 267 1
2,4-Dichlorophenol ND ug/kg 09/18/19 14:33 120-83-209/18/19 08:32383 126 1
Diethylphthalate ND ug/kg 09/18/19 14:33 84-66-209/18/19 08:32383 83.0 1
2,4-Dimethylphenol ND ug/kg 09/18/19 14:33 105-67-909/18/19 08:32383 95.3 1
Dimethylphthalate ND ug/kg 09/18/19 14:33 131-11-309/18/19 08:32383 86.5 1
Di-n-butylphthalate ND ug/kg 09/18/19 14:33 84-74-209/18/19 08:32383 94.4 1
4,6-Dinitro-2-methylphenol ND ug/kg 09/18/19 14:33 534-52-109/18/19 08:32765 617 1
REPORT OF LABORATORY ANALYSIS
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Page 5 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92445872
DCY-001
Sample: P1 Lab ID: 92445872001 Collected: 09/16/19 10:00 Received: 09/17/19 12:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 09/18/19 14:33 51-28-509/18/19 08:321910 1220 1
2,4-Dinitrotoluene ND ug/kg 09/18/19 14:33 121-14-209/18/19 08:32383 101 1
2,6-Dinitrotoluene ND ug/kg 09/18/19 14:33 606-20-209/18/19 08:32383 100 1
Di-n-octylphthalate ND ug/kg 09/18/19 14:33 117-84-009/18/19 08:32383 218 1
bis(2-Ethylhexyl)phthalate ND ug/kg 09/18/19 14:33 117-81-709/18/19 08:32383 125 1
Fluoranthene ND ug/kg 09/18/19 14:33 206-44-009/18/19 08:32383 116 1
Fluorene ND ug/kg 09/18/19 14:33 86-73-709/18/19 08:32383 102 1
Hexachloro-1,3-butadiene ND ug/kg 09/18/19 14:33 87-68-309/18/19 08:32383 93.0 1
Hexachlorobenzene ND ug/kg 09/18/19 14:33 118-74-109/18/19 08:32383 97.2 1
Hexachlorocyclopentadiene ND ug/kg 09/18/19 14:33 77-47-4 v209/18/19 08:32383 153 1
Hexachloroethane ND ug/kg 09/18/19 14:33 67-72-109/18/19 08:32383 87.2 1
Indeno(1,2,3-cd)pyrene ND ug/kg 09/18/19 14:33 193-39-509/18/19 08:32383 175 1
Isophorone ND ug/kg 09/18/19 14:33 78-59-109/18/19 08:32383 83.2 1
1-Methylnaphthalene ND ug/kg 09/18/19 14:33 90-12-009/18/19 08:32383 102 1
2-Methylnaphthalene ND ug/kg 09/18/19 14:33 91-57-609/18/19 08:32383 97.4 1
2-Methylphenol(o-Cresol)ND ug/kg 09/18/19 14:33 95-48-709/18/19 08:32383 84.8 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 09/18/19 14:33 15831-10-409/18/19 08:32383 96.3 1
Naphthalene ND ug/kg 09/18/19 14:33 91-20-309/18/19 08:32383 91.6 1
2-Nitroaniline ND ug/kg 09/18/19 14:33 88-74-409/18/19 08:321910 193 1
3-Nitroaniline ND ug/kg 09/18/19 14:33 99-09-209/18/19 08:321910 203 1
4-Nitroaniline ND ug/kg 09/18/19 14:33 100-01-609/18/19 08:32765 189 1
Nitrobenzene ND ug/kg 09/18/19 14:33 98-95-309/18/19 08:32383 91.4 1
2-Nitrophenol ND ug/kg 09/18/19 14:33 88-75-509/18/19 08:32383 118 1
4-Nitrophenol ND ug/kg 09/18/19 14:33 100-02-709/18/19 08:321910 610 1
N-Nitrosodimethylamine ND ug/kg 09/18/19 14:33 62-75-909/18/19 08:32383 108 1
N-Nitroso-di-n-propylamine ND ug/kg 09/18/19 14:33 621-64-709/18/19 08:32383 107 1
N-Nitrosodiphenylamine ND ug/kg 09/18/19 14:33 86-30-609/18/19 08:32383 97.7 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 09/18/19 14:33 108-60-1 v109/18/19 08:32383 106 1
Pentachlorophenol ND ug/kg 09/18/19 14:33 87-86-509/18/19 08:321910 175 1
Phenanthrene ND ug/kg 09/18/19 14:33 85-01-809/18/19 08:32383 96.4 1
Phenol ND ug/kg 09/18/19 14:33 108-95-209/18/19 08:32383 91.4 1
Pyrene ND ug/kg 09/18/19 14:33 129-00-009/18/19 08:32383 105 1
Pyridine ND ug/kg 09/18/19 14:33 110-86-109/18/19 08:32383 96.8 1
1,2,4-Trichlorobenzene ND ug/kg 09/18/19 14:33 120-82-109/18/19 08:32383 87.7 1
2,4,5-Trichlorophenol ND ug/kg 09/18/19 14:33 95-95-409/18/19 08:32383 99.4 1
2,4,6-Trichlorophenol ND ug/kg 09/18/19 14:33 88-06-209/18/19 08:32383 96.2 1
Surrogates
Nitrobenzene-d5 (S)39 %09/18/19 14:33 4165-60-009/18/19 08:3223-110 1
2-Fluorobiphenyl (S)42 %09/18/19 14:33 321-60-809/18/19 08:3230-110 1
Terphenyl-d14 (S)56 %09/18/19 14:33 1718-51-009/18/19 08:3228-110 1
Phenol-d6 (S)42 %09/18/19 14:33 13127-88-309/18/19 08:3222-110 1
2-Fluorophenol (S)45 %09/18/19 14:33 367-12-409/18/19 08:3213-110 1
2,4,6-Tribromophenol (S)60 %09/18/19 14:33 118-79-609/18/19 08:3227-110 1
REPORT OF LABORATORY ANALYSIS
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Page 6 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92445872
DCY-001
Sample: P1 Lab ID: 92445872001 Collected: 09/16/19 10:00 Received: 09/17/19 12:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 09/21/19 17:42 67-64-109/21/19 11:49105 9.9 1
Benzene ND ug/kg 09/21/19 17:42 71-43-209/21/19 11:495.2 0.94 1
Bromobenzene ND ug/kg 09/21/19 17:42 108-86-109/21/19 11:495.2 1.4 1
Bromochloromethane ND ug/kg 09/21/19 17:42 74-97-509/21/19 11:495.2 1.3 1
Bromodichloromethane ND ug/kg 09/21/19 17:42 75-27-409/21/19 11:495.2 1.0 1
Bromoform ND ug/kg 09/21/19 17:42 75-25-209/21/19 11:495.2 2.6 1
Bromomethane ND ug/kg 09/21/19 17:42 74-83-9 v209/21/19 11:4910.5 2.5 1
2-Butanone (MEK)ND ug/kg 09/21/19 17:42 78-93-309/21/19 11:49105 12.4 1
n-Butylbenzene ND ug/kg 09/21/19 17:42 104-51-809/21/19 11:495.2 2.9 1
sec-Butylbenzene ND ug/kg 09/21/19 17:42 135-98-809/21/19 11:495.2 2.2 1
tert-Butylbenzene ND ug/kg 09/21/19 17:42 98-06-609/21/19 11:495.2 1.8 1
Carbon tetrachloride ND ug/kg 09/21/19 17:42 56-23-509/21/19 11:495.2 1.0 1
Chlorobenzene ND ug/kg 09/21/19 17:42 108-90-709/21/19 11:495.2 1.0 1
Chloroethane ND ug/kg 09/21/19 17:42 75-00-3 v209/21/19 11:4910.5 2.2 1
Chloroform ND ug/kg 09/21/19 17:42 67-66-309/21/19 11:495.2 1.1 1
Chloromethane ND ug/kg 09/21/19 17:42 74-87-3 L1,v209/21/19 11:4910.5 3.4 1
2-Chlorotoluene ND ug/kg 09/21/19 17:42 95-49-809/21/19 11:495.2 1.6 1
4-Chlorotoluene ND ug/kg 09/21/19 17:42 106-43-409/21/19 11:495.2 1.6 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/21/19 17:42 96-12-809/21/19 11:495.2 2.7 1
Dibromochloromethane ND ug/kg 09/21/19 17:42 124-48-109/21/19 11:495.2 2.6 1
1,2-Dibromoethane (EDB)ND ug/kg 09/21/19 17:42 106-93-409/21/19 11:495.2 1.2 1
Dibromomethane ND ug/kg 09/21/19 17:42 74-95-309/21/19 11:495.2 1.6 1
1,2-Dichlorobenzene ND ug/kg 09/21/19 17:42 95-50-109/21/19 11:495.2 1.8 1
1,3-Dichlorobenzene ND ug/kg 09/21/19 17:42 541-73-109/21/19 11:495.2 1.9 1
1,4-Dichlorobenzene ND ug/kg 09/21/19 17:42 106-46-709/21/19 11:495.2 1.8 1
Dichlorodifluoromethane ND ug/kg 09/21/19 17:42 75-71-8 L1,v209/21/19 11:4910.5 4.3 1
1,1-Dichloroethane ND ug/kg 09/21/19 17:42 75-34-309/21/19 11:495.2 0.77 1
1,2-Dichloroethane ND ug/kg 09/21/19 17:42 107-06-209/21/19 11:495.2 1.0 1
1,1-Dichloroethene ND ug/kg 09/21/19 17:42 75-35-409/21/19 11:495.2 1.2 1
cis-1,2-Dichloroethene ND ug/kg 09/21/19 17:42 156-59-209/21/19 11:495.2 0.91 1
trans-1,2-Dichloroethene ND ug/kg 09/21/19 17:42 156-60-509/21/19 11:495.2 1.0 1
1,2-Dichloropropane ND ug/kg 09/21/19 17:42 78-87-509/21/19 11:495.2 2.0 1
1,3-Dichloropropane ND ug/kg 09/21/19 17:42 142-28-909/21/19 11:495.2 2.0 1
2,2-Dichloropropane ND ug/kg 09/21/19 17:42 594-20-709/21/19 11:495.2 0.52 1
1,1-Dichloropropene ND ug/kg 09/21/19 17:42 563-58-609/21/19 11:495.2 2.2 1
cis-1,3-Dichloropropene ND ug/kg 09/21/19 17:42 10061-01-509/21/19 11:495.2 2.4 1
trans-1,3-Dichloropropene ND ug/kg 09/21/19 17:42 10061-02-609/21/19 11:495.2 0.91 1
Diisopropyl ether ND ug/kg 09/21/19 17:42 108-20-309/21/19 11:495.2 3.0 1
Ethylbenzene 1.2J ug/kg 09/21/19 17:42 100-41-409/21/19 11:495.2 1.1 1
Hexachloro-1,3-butadiene ND ug/kg 09/21/19 17:42 87-68-309/21/19 11:495.2 2.6 1
2-Hexanone ND ug/kg 09/21/19 17:42 591-78-609/21/19 11:4952.3 5.4 1
Isopropylbenzene (Cumene)ND ug/kg 09/21/19 17:42 98-82-809/21/19 11:495.2 1.5 1
p-Isopropyltoluene ND ug/kg 09/21/19 17:42 99-87-609/21/19 11:495.2 2.5 1
Methylene Chloride ND ug/kg 09/21/19 17:42 75-09-209/21/19 11:4920.9 6.2 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/21/19 17:42 108-10-109/21/19 11:4952.3 3.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 7 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92445872
DCY-001
Sample: P1 Lab ID: 92445872001 Collected: 09/16/19 10:00 Received: 09/17/19 12:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 09/21/19 17:42 1634-04-409/21/19 11:495.2 3.0 1
Naphthalene ND ug/kg 09/21/19 17:42 91-20-309/21/19 11:495.2 4.4 1
n-Propylbenzene ND ug/kg 09/21/19 17:42 103-65-109/21/19 11:495.2 1.7 1
Styrene ND ug/kg 09/21/19 17:42 100-42-509/21/19 11:495.2 1.5 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/21/19 17:42 630-20-609/21/19 11:495.2 1.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/21/19 17:42 79-34-509/21/19 11:495.2 1.8 1
Tetrachloroethene ND ug/kg 09/21/19 17:42 127-18-409/21/19 11:495.2 1.7 1
Toluene 6.0 ug/kg 09/21/19 17:42 108-88-3 D609/21/19 11:495.2 1.7 1
1,2,3-Trichlorobenzene ND ug/kg 09/21/19 17:42 87-61-609/21/19 11:495.2 3.7 1
1,2,4-Trichlorobenzene ND ug/kg 09/21/19 17:42 120-82-109/21/19 11:495.2 2.8 1
1,1,1-Trichloroethane ND ug/kg 09/21/19 17:42 71-55-609/21/19 11:495.2 0.91 1
1,1,2-Trichloroethane ND ug/kg 09/21/19 17:42 79-00-509/21/19 11:495.2 1.2 1
Trichloroethene ND ug/kg 09/21/19 17:42 79-01-609/21/19 11:495.2 1.4 1
Trichlorofluoromethane ND ug/kg 09/21/19 17:42 75-69-4 L1,v209/21/19 11:495.2 1.2 1
1,2,3-Trichloropropane ND ug/kg 09/21/19 17:42 96-18-409/21/19 11:495.2 1.8 1
1,2,4-Trimethylbenzene ND ug/kg 09/21/19 17:42 95-63-609/21/19 11:495.2 2.0 1
1,3,5-Trimethylbenzene ND ug/kg 09/21/19 17:42 108-67-809/21/19 11:495.2 1.7 1
Vinyl acetate ND ug/kg 09/21/19 17:42 108-05-4 L109/21/19 11:4952.3 17.0 1
Vinyl chloride ND ug/kg 09/21/19 17:42 75-01-4 L1,v209/21/19 11:4910.5 2.0 1
Xylene (Total)ND ug/kg 09/21/19 17:42 1330-20-709/21/19 11:4910.5 3.7 1
m&p-Xylene 3.9J ug/kg 09/21/19 17:42 179601-23-109/21/19 11:4910.5 2.5 1
o-Xylene 1.6J ug/kg 09/21/19 17:42 95-47-609/21/19 11:495.2 1.2 1
Surrogates
Toluene-d8 (S)108 %09/21/19 17:42 2037-26-509/21/19 11:4970-130 1
4-Bromofluorobenzene (S)101 %09/21/19 17:42 460-00-409/21/19 11:4970-130 1
1,2-Dichloroethane-d4 (S)95 %09/21/19 17:42 17060-07-009/21/19 11:4970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.5 %09/17/19 16:060.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 87.7 %09/23/19 15:3409/23/19 15:271
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 8 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92445872
DCY-001
Sample: P3 Lab ID: 92445872002 Collected: 09/16/19 11:00 Received: 09/17/19 12:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051Metals (ICPMS) 6020B
Arsenic 7.21 mg/kg 09/21/19 15:14 7440-38-209/21/19 11:230.561 0.140 5
Barium 105 mg/kg 09/21/19 15:14 7440-39-309/21/19 11:231.12 0.180 5
Cadmium ND mg/kg 09/21/19 15:14 7440-43-909/21/19 11:230.561 0.0898 5
Chromium 101 mg/kg 09/21/19 15:14 7440-47-309/21/19 11:231.12 0.303 5
Lead 4.45 mg/kg 09/21/19 15:14 7439-92-109/21/19 11:230.561 0.135 5
Selenium ND mg/kg 09/21/19 15:14 7782-49-209/21/19 11:230.561 0.213 5
Silver ND mg/kg 09/21/19 15:14 7440-22-409/21/19 11:230.561 0.174 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 0.00896J mg/kg 09/19/19 20:10 7439-97-609/19/19 12:510.0337 0.00314 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 09/18/19 15:06 83-32-909/18/19 08:32366 94.2 1
Acenaphthylene ND ug/kg 09/18/19 15:06 208-96-809/18/19 08:32366 86.7 1
Aniline ND ug/kg 09/18/19 15:06 62-53-309/18/19 08:32366 82.2 1
Anthracene ND ug/kg 09/18/19 15:06 120-12-709/18/19 08:32366 95.0 1
Benzo(a)anthracene ND ug/kg 09/18/19 15:06 56-55-309/18/19 08:32366 117 1
Benzo(a)pyrene ND ug/kg 09/18/19 15:06 50-32-809/18/19 08:32366 159 1
Benzo(b)fluoranthene ND ug/kg 09/18/19 15:06 205-99-209/18/19 08:32366 148 1
Benzo(g,h,i)perylene ND ug/kg 09/18/19 15:06 191-24-209/18/19 08:32366 143 1
Benzo(k)fluoranthene ND ug/kg 09/18/19 15:06 207-08-909/18/19 08:32366 154 1
Benzoic Acid ND ug/kg 09/18/19 15:06 65-85-009/18/19 08:321830 395 1
Benzyl alcohol ND ug/kg 09/18/19 15:06 100-51-609/18/19 08:32732 194 1
4-Bromophenylphenyl ether ND ug/kg 09/18/19 15:06 101-55-309/18/19 08:32366 96.1 1
Butylbenzylphthalate ND ug/kg 09/18/19 15:06 85-68-709/18/19 08:32366 97.5 1
4-Chloro-3-methylphenol ND ug/kg 09/18/19 15:06 59-50-709/18/19 08:32732 223 1
4-Chloroaniline ND ug/kg 09/18/19 15:06 106-47-809/18/19 08:321830 224 1
bis(2-Chloroethoxy)methane ND ug/kg 09/18/19 15:06 111-91-109/18/19 08:32366 97.8 1
bis(2-Chloroethyl) ether ND ug/kg 09/18/19 15:06 111-44-409/18/19 08:32366 77.8 1
2-Chloronaphthalene ND ug/kg 09/18/19 15:06 91-58-709/18/19 08:32366 81.6 1
2-Chlorophenol ND ug/kg 09/18/19 15:06 95-57-809/18/19 08:32366 85.2 1
4-Chlorophenylphenyl ether ND ug/kg 09/18/19 15:06 7005-72-309/18/19 08:32366 95.1 1
Chrysene ND ug/kg 09/18/19 15:06 218-01-909/18/19 08:32366 106 1
Dibenz(a,h)anthracene ND ug/kg 09/18/19 15:06 53-70-309/18/19 08:32366 146 1
Dibenzofuran ND ug/kg 09/18/19 15:06 132-64-909/18/19 08:32366 91.5 1
1,2-Dichlorobenzene ND ug/kg 09/18/19 15:06 95-50-109/18/19 08:32366 79.2 1
1,3-Dichlorobenzene ND ug/kg 09/18/19 15:06 541-73-109/18/19 08:32366 82.4 1
1,4-Dichlorobenzene ND ug/kg 09/18/19 15:06 106-46-709/18/19 08:32366 80.6 1
3,3'-Dichlorobenzidine ND ug/kg 09/18/19 15:06 91-94-109/18/19 08:321830 255 1
2,4-Dichlorophenol ND ug/kg 09/18/19 15:06 120-83-209/18/19 08:32366 121 1
Diethylphthalate ND ug/kg 09/18/19 15:06 84-66-209/18/19 08:32366 79.4 1
2,4-Dimethylphenol ND ug/kg 09/18/19 15:06 105-67-909/18/19 08:32366 91.2 1
Dimethylphthalate ND ug/kg 09/18/19 15:06 131-11-309/18/19 08:32366 82.8 1
Di-n-butylphthalate ND ug/kg 09/18/19 15:06 84-74-209/18/19 08:32366 90.3 1
4,6-Dinitro-2-methylphenol ND ug/kg 09/18/19 15:06 534-52-109/18/19 08:32732 590 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 9 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92445872
DCY-001
Sample: P3 Lab ID: 92445872002 Collected: 09/16/19 11:00 Received: 09/17/19 12:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 09/18/19 15:06 51-28-509/18/19 08:321830 1170 1
2,4-Dinitrotoluene ND ug/kg 09/18/19 15:06 121-14-209/18/19 08:32366 97.0 1
2,6-Dinitrotoluene ND ug/kg 09/18/19 15:06 606-20-209/18/19 08:32366 95.8 1
Di-n-octylphthalate ND ug/kg 09/18/19 15:06 117-84-009/18/19 08:32366 209 1
bis(2-Ethylhexyl)phthalate ND ug/kg 09/18/19 15:06 117-81-709/18/19 08:32366 120 1
Fluoranthene ND ug/kg 09/18/19 15:06 206-44-009/18/19 08:32366 111 1
Fluorene ND ug/kg 09/18/19 15:06 86-73-709/18/19 08:32366 98.0 1
Hexachloro-1,3-butadiene ND ug/kg 09/18/19 15:06 87-68-309/18/19 08:32366 89.0 1
Hexachlorobenzene ND ug/kg 09/18/19 15:06 118-74-109/18/19 08:32366 93.0 1
Hexachlorocyclopentadiene ND ug/kg 09/18/19 15:06 77-47-4 v209/18/19 08:32366 146 1
Hexachloroethane ND ug/kg 09/18/19 15:06 67-72-109/18/19 08:32366 83.4 1
Indeno(1,2,3-cd)pyrene ND ug/kg 09/18/19 15:06 193-39-509/18/19 08:32366 168 1
Isophorone ND ug/kg 09/18/19 15:06 78-59-109/18/19 08:32366 79.6 1
1-Methylnaphthalene ND ug/kg 09/18/19 15:06 90-12-009/18/19 08:32366 97.5 1
2-Methylnaphthalene ND ug/kg 09/18/19 15:06 91-57-609/18/19 08:32366 93.2 1
2-Methylphenol(o-Cresol)ND ug/kg 09/18/19 15:06 95-48-709/18/19 08:32366 81.1 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 09/18/19 15:06 15831-10-409/18/19 08:32366 92.1 1
Naphthalene ND ug/kg 09/18/19 15:06 91-20-309/18/19 08:32366 87.7 1
2-Nitroaniline ND ug/kg 09/18/19 15:06 88-74-409/18/19 08:321830 184 1
3-Nitroaniline ND ug/kg 09/18/19 15:06 99-09-209/18/19 08:321830 194 1
4-Nitroaniline ND ug/kg 09/18/19 15:06 100-01-609/18/19 08:32732 181 1
Nitrobenzene ND ug/kg 09/18/19 15:06 98-95-309/18/19 08:32366 87.4 1
2-Nitrophenol ND ug/kg 09/18/19 15:06 88-75-509/18/19 08:32366 113 1
4-Nitrophenol ND ug/kg 09/18/19 15:06 100-02-709/18/19 08:321830 584 1
N-Nitrosodimethylamine ND ug/kg 09/18/19 15:06 62-75-909/18/19 08:32366 103 1
N-Nitroso-di-n-propylamine ND ug/kg 09/18/19 15:06 621-64-709/18/19 08:32366 103 1
N-Nitrosodiphenylamine ND ug/kg 09/18/19 15:06 86-30-609/18/19 08:32366 93.4 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 09/18/19 15:06 108-60-1 v109/18/19 08:32366 102 1
Pentachlorophenol ND ug/kg 09/18/19 15:06 87-86-509/18/19 08:321830 168 1
Phenanthrene ND ug/kg 09/18/19 15:06 85-01-809/18/19 08:32366 92.2 1
Phenol ND ug/kg 09/18/19 15:06 108-95-209/18/19 08:32366 87.4 1
Pyrene ND ug/kg 09/18/19 15:06 129-00-009/18/19 08:32366 101 1
Pyridine ND ug/kg 09/18/19 15:06 110-86-109/18/19 08:32366 92.6 1
1,2,4-Trichlorobenzene ND ug/kg 09/18/19 15:06 120-82-109/18/19 08:32366 83.9 1
2,4,5-Trichlorophenol ND ug/kg 09/18/19 15:06 95-95-409/18/19 08:32366 95.1 1
2,4,6-Trichlorophenol ND ug/kg 09/18/19 15:06 88-06-209/18/19 08:32366 92.0 1
Surrogates
Nitrobenzene-d5 (S)54 %09/18/19 15:06 4165-60-009/18/19 08:3223-110 1
2-Fluorobiphenyl (S)58 %09/18/19 15:06 321-60-809/18/19 08:3230-110 1
Terphenyl-d14 (S)68 %09/18/19 15:06 1718-51-009/18/19 08:3228-110 1
Phenol-d6 (S)56 %09/18/19 15:06 13127-88-309/18/19 08:3222-110 1
2-Fluorophenol (S)56 %09/18/19 15:06 367-12-409/18/19 08:3213-110 1
2,4,6-Tribromophenol (S)73 %09/18/19 15:06 118-79-609/18/19 08:3227-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92445872
DCY-001
Sample: P3 Lab ID: 92445872002 Collected: 09/16/19 11:00 Received: 09/17/19 12:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 09/21/19 18:07 67-64-109/21/19 11:49186 17.5 1
Benzene ND ug/kg 09/21/19 18:07 71-43-209/21/19 11:499.3 1.7 1
Bromobenzene ND ug/kg 09/21/19 18:07 108-86-109/21/19 11:499.3 2.5 1
Bromochloromethane ND ug/kg 09/21/19 18:07 74-97-509/21/19 11:499.3 2.3 1
Bromodichloromethane ND ug/kg 09/21/19 18:07 75-27-409/21/19 11:499.3 1.8 1
Bromoform ND ug/kg 09/21/19 18:07 75-25-209/21/19 11:499.3 4.5 1
Bromomethane ND ug/kg 09/21/19 18:07 74-83-9 v209/21/19 11:4918.6 4.4 1
2-Butanone (MEK)ND ug/kg 09/21/19 18:07 78-93-309/21/19 11:49186 22.1 1
n-Butylbenzene ND ug/kg 09/21/19 18:07 104-51-809/21/19 11:499.3 5.2 1
sec-Butylbenzene ND ug/kg 09/21/19 18:07 135-98-809/21/19 11:499.3 3.9 1
tert-Butylbenzene ND ug/kg 09/21/19 18:07 98-06-609/21/19 11:499.3 3.1 1
Carbon tetrachloride ND ug/kg 09/21/19 18:07 56-23-509/21/19 11:499.3 1.8 1
Chlorobenzene ND ug/kg 09/21/19 18:07 108-90-709/21/19 11:499.3 1.8 1
Chloroethane ND ug/kg 09/21/19 18:07 75-00-3 v209/21/19 11:4918.6 3.9 1
Chloroform ND ug/kg 09/21/19 18:07 67-66-309/21/19 11:499.3 2.0 1
Chloromethane ND ug/kg 09/21/19 18:07 74-87-3 L1,v209/21/19 11:4918.6 6.1 1
2-Chlorotoluene ND ug/kg 09/21/19 18:07 95-49-809/21/19 11:499.3 2.8 1
4-Chlorotoluene ND ug/kg 09/21/19 18:07 106-43-409/21/19 11:499.3 2.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/21/19 18:07 96-12-809/21/19 11:499.3 4.7 1
Dibromochloromethane ND ug/kg 09/21/19 18:07 124-48-109/21/19 11:499.3 4.6 1
1,2-Dibromoethane (EDB)ND ug/kg 09/21/19 18:07 106-93-409/21/19 11:499.3 2.1 1
Dibromomethane ND ug/kg 09/21/19 18:07 74-95-309/21/19 11:499.3 2.8 1
1,2-Dichlorobenzene ND ug/kg 09/21/19 18:07 95-50-109/21/19 11:499.3 3.3 1
1,3-Dichlorobenzene ND ug/kg 09/21/19 18:07 541-73-109/21/19 11:499.3 3.3 1
1,4-Dichlorobenzene ND ug/kg 09/21/19 18:07 106-46-709/21/19 11:499.3 3.2 1
Dichlorodifluoromethane ND ug/kg 09/21/19 18:07 75-71-8 L1,v209/21/19 11:4918.6 7.6 1
1,1-Dichloroethane ND ug/kg 09/21/19 18:07 75-34-309/21/19 11:499.3 1.4 1
1,2-Dichloroethane ND ug/kg 09/21/19 18:07 107-06-209/21/19 11:499.3 1.9 1
1,1-Dichloroethene ND ug/kg 09/21/19 18:07 75-35-409/21/19 11:499.3 2.2 1
cis-1,2-Dichloroethene ND ug/kg 09/21/19 18:07 156-59-209/21/19 11:499.3 1.6 1
trans-1,2-Dichloroethene ND ug/kg 09/21/19 18:07 156-60-509/21/19 11:499.3 1.8 1
1,2-Dichloropropane ND ug/kg 09/21/19 18:07 78-87-509/21/19 11:499.3 3.5 1
1,3-Dichloropropane ND ug/kg 09/21/19 18:07 142-28-909/21/19 11:499.3 3.5 1
2,2-Dichloropropane ND ug/kg 09/21/19 18:07 594-20-709/21/19 11:499.3 0.92 1
1,1-Dichloropropene ND ug/kg 09/21/19 18:07 563-58-609/21/19 11:499.3 3.9 1
cis-1,3-Dichloropropene ND ug/kg 09/21/19 18:07 10061-01-509/21/19 11:499.3 4.2 1
trans-1,3-Dichloropropene ND ug/kg 09/21/19 18:07 10061-02-609/21/19 11:499.3 1.6 1
Diisopropyl ether ND ug/kg 09/21/19 18:07 108-20-309/21/19 11:499.3 5.3 1
Ethylbenzene 2.5J ug/kg 09/21/19 18:07 100-41-409/21/19 11:499.3 2.0 1
Hexachloro-1,3-butadiene ND ug/kg 09/21/19 18:07 87-68-309/21/19 11:499.3 4.6 1
2-Hexanone ND ug/kg 09/21/19 18:07 591-78-609/21/19 11:4992.8 9.6 1
Isopropylbenzene (Cumene)ND ug/kg 09/21/19 18:07 98-82-809/21/19 11:499.3 2.7 1
p-Isopropyltoluene ND ug/kg 09/21/19 18:07 99-87-609/21/19 11:499.3 4.5 1
Methylene Chloride ND ug/kg 09/21/19 18:07 75-09-209/21/19 11:4937.1 11.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/21/19 18:07 108-10-109/21/19 11:4992.8 6.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92445872
DCY-001
Sample: P3 Lab ID: 92445872002 Collected: 09/16/19 11:00 Received: 09/17/19 12:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 09/21/19 18:07 1634-04-409/21/19 11:499.3 5.3 1
Naphthalene ND ug/kg 09/21/19 18:07 91-20-309/21/19 11:499.3 7.9 1
n-Propylbenzene ND ug/kg 09/21/19 18:07 103-65-109/21/19 11:499.3 3.1 1
Styrene ND ug/kg 09/21/19 18:07 100-42-509/21/19 11:499.3 2.7 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/21/19 18:07 630-20-609/21/19 11:499.3 2.3 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/21/19 18:07 79-34-509/21/19 11:499.3 3.2 1
Tetrachloroethene ND ug/kg 09/21/19 18:07 127-18-409/21/19 11:499.3 2.9 1
Toluene 4.2J ug/kg 09/21/19 18:07 108-88-309/21/19 11:499.3 3.0 1
1,2,3-Trichlorobenzene ND ug/kg 09/21/19 18:07 87-61-609/21/19 11:499.3 6.6 1
1,2,4-Trichlorobenzene ND ug/kg 09/21/19 18:07 120-82-109/21/19 11:499.3 4.9 1
1,1,1-Trichloroethane ND ug/kg 09/21/19 18:07 71-55-609/21/19 11:499.3 1.6 1
1,1,2-Trichloroethane ND ug/kg 09/21/19 18:07 79-00-509/21/19 11:499.3 2.1 1
Trichloroethene ND ug/kg 09/21/19 18:07 79-01-609/21/19 11:499.3 2.4 1
Trichlorofluoromethane ND ug/kg 09/21/19 18:07 75-69-4 L1,v209/21/19 11:499.3 2.2 1
1,2,3-Trichloropropane ND ug/kg 09/21/19 18:07 96-18-409/21/19 11:499.3 3.1 1
1,2,4-Trimethylbenzene ND ug/kg 09/21/19 18:07 95-63-609/21/19 11:499.3 3.6 1
1,3,5-Trimethylbenzene ND ug/kg 09/21/19 18:07 108-67-809/21/19 11:499.3 3.1 1
Vinyl acetate ND ug/kg 09/21/19 18:07 108-05-4 L109/21/19 11:4992.8 30.2 1
Vinyl chloride ND ug/kg 09/21/19 18:07 75-01-4 L1,v209/21/19 11:4918.6 3.5 1
Xylene (Total)ND ug/kg 09/21/19 18:07 1330-20-709/21/19 11:4918.6 6.5 1
m&p-Xylene 8.5J ug/kg 09/21/19 18:07 179601-23-109/21/19 11:4918.6 4.4 1
o-Xylene 3.2J ug/kg 09/21/19 18:07 95-47-609/21/19 11:499.3 2.2 1
Surrogates
Toluene-d8 (S)106 %09/21/19 18:07 2037-26-509/21/19 11:4970-130 1
4-Bromofluorobenzene (S)100 %09/21/19 18:07 460-00-409/21/19 11:4970-130 1
1,2-Dichloroethane-d4 (S)93 %09/21/19 18:07 17060-07-009/21/19 11:4970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 9.6 %09/17/19 16:060.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 89.1 %09/23/19 15:3409/23/19 15:271
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92445872
DCY-001
Sample: P4A Lab ID: 92445872003 Collected: 09/16/19 12:00 Received: 09/17/19 12:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051Metals (ICPMS) 6020B
Arsenic 5.71 mg/kg 09/21/19 15:17 7440-38-209/21/19 11:230.589 0.147 5
Barium 103 mg/kg 09/21/19 15:17 7440-39-309/21/19 11:231.18 0.188 5
Cadmium ND mg/kg 09/21/19 15:17 7440-43-909/21/19 11:230.589 0.0942 5
Chromium 95.0 mg/kg 09/21/19 15:17 7440-47-309/21/19 11:231.18 0.318 5
Lead 11.4 mg/kg 09/21/19 15:17 7439-92-109/21/19 11:230.589 0.141 5
Selenium 0.643 mg/kg 09/21/19 15:17 7782-49-209/21/19 11:230.589 0.224 5
Silver ND mg/kg 09/21/19 15:17 7440-22-409/21/19 11:230.589 0.182 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 0.0132J mg/kg 09/19/19 20:13 7439-97-609/19/19 12:510.0353 0.00330 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 09/18/19 15:40 83-32-909/18/19 08:32381 97.9 1
Acenaphthylene ND ug/kg 09/18/19 15:40 208-96-809/18/19 08:32381 90.1 1
Aniline ND ug/kg 09/18/19 15:40 62-53-309/18/19 08:32381 85.4 1
Anthracene ND ug/kg 09/18/19 15:40 120-12-709/18/19 08:32381 98.7 1
Benzo(a)anthracene ND ug/kg 09/18/19 15:40 56-55-309/18/19 08:32381 121 1
Benzo(a)pyrene ND ug/kg 09/18/19 15:40 50-32-809/18/19 08:32381 165 1
Benzo(b)fluoranthene ND ug/kg 09/18/19 15:40 205-99-209/18/19 08:32381 153 1
Benzo(g,h,i)perylene ND ug/kg 09/18/19 15:40 191-24-209/18/19 08:32381 149 1
Benzo(k)fluoranthene ND ug/kg 09/18/19 15:40 207-08-909/18/19 08:32381 160 1
Benzoic Acid ND ug/kg 09/18/19 15:40 65-85-009/18/19 08:321900 410 1
Benzyl alcohol ND ug/kg 09/18/19 15:40 100-51-609/18/19 08:32761 202 1
4-Bromophenylphenyl ether ND ug/kg 09/18/19 15:40 101-55-309/18/19 08:32381 99.9 1
Butylbenzylphthalate ND ug/kg 09/18/19 15:40 85-68-709/18/19 08:32381 101 1
4-Chloro-3-methylphenol ND ug/kg 09/18/19 15:40 59-50-709/18/19 08:32761 232 1
4-Chloroaniline ND ug/kg 09/18/19 15:40 106-47-809/18/19 08:321900 233 1
bis(2-Chloroethoxy)methane ND ug/kg 09/18/19 15:40 111-91-109/18/19 08:32381 102 1
bis(2-Chloroethyl) ether ND ug/kg 09/18/19 15:40 111-44-409/18/19 08:32381 80.8 1
2-Chloronaphthalene ND ug/kg 09/18/19 15:40 91-58-709/18/19 08:32381 84.7 1
2-Chlorophenol ND ug/kg 09/18/19 15:40 95-57-809/18/19 08:32381 88.6 1
4-Chlorophenylphenyl ether ND ug/kg 09/18/19 15:40 7005-72-309/18/19 08:32381 98.8 1
Chrysene ND ug/kg 09/18/19 15:40 218-01-909/18/19 08:32381 110 1
Dibenz(a,h)anthracene ND ug/kg 09/18/19 15:40 53-70-309/18/19 08:32381 152 1
Dibenzofuran ND ug/kg 09/18/19 15:40 132-64-909/18/19 08:32381 95.1 1
1,2-Dichlorobenzene ND ug/kg 09/18/19 15:40 95-50-109/18/19 08:32381 82.3 1
1,3-Dichlorobenzene ND ug/kg 09/18/19 15:40 541-73-109/18/19 08:32381 85.7 1
1,4-Dichlorobenzene ND ug/kg 09/18/19 15:40 106-46-709/18/19 08:32381 83.7 1
3,3'-Dichlorobenzidine ND ug/kg 09/18/19 15:40 91-94-109/18/19 08:321900 265 1
2,4-Dichlorophenol ND ug/kg 09/18/19 15:40 120-83-209/18/19 08:32381 126 1
Diethylphthalate ND ug/kg 09/18/19 15:40 84-66-209/18/19 08:32381 82.6 1
2,4-Dimethylphenol ND ug/kg 09/18/19 15:40 105-67-909/18/19 08:32381 94.8 1
Dimethylphthalate ND ug/kg 09/18/19 15:40 131-11-309/18/19 08:32381 86.0 1
Di-n-butylphthalate ND ug/kg 09/18/19 15:40 84-74-209/18/19 08:32381 93.9 1
4,6-Dinitro-2-methylphenol ND ug/kg 09/18/19 15:40 534-52-109/18/19 08:32761 613 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 13 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92445872
DCY-001
Sample: P4A Lab ID: 92445872003 Collected: 09/16/19 12:00 Received: 09/17/19 12:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 09/18/19 15:40 51-28-509/18/19 08:321900 1220 1
2,4-Dinitrotoluene ND ug/kg 09/18/19 15:40 121-14-209/18/19 08:32381 101 1
2,6-Dinitrotoluene ND ug/kg 09/18/19 15:40 606-20-209/18/19 08:32381 99.5 1
Di-n-octylphthalate ND ug/kg 09/18/19 15:40 117-84-009/18/19 08:32381 217 1
bis(2-Ethylhexyl)phthalate ND ug/kg 09/18/19 15:40 117-81-709/18/19 08:32381 125 1
Fluoranthene ND ug/kg 09/18/19 15:40 206-44-009/18/19 08:32381 115 1
Fluorene ND ug/kg 09/18/19 15:40 86-73-709/18/19 08:32381 102 1
Hexachloro-1,3-butadiene ND ug/kg 09/18/19 15:40 87-68-309/18/19 08:32381 92.5 1
Hexachlorobenzene ND ug/kg 09/18/19 15:40 118-74-109/18/19 08:32381 96.6 1
Hexachlorocyclopentadiene ND ug/kg 09/18/19 15:40 77-47-4 v209/18/19 08:32381 152 1
Hexachloroethane ND ug/kg 09/18/19 15:40 67-72-109/18/19 08:32381 86.7 1
Indeno(1,2,3-cd)pyrene ND ug/kg 09/18/19 15:40 193-39-509/18/19 08:32381 174 1
Isophorone ND ug/kg 09/18/19 15:40 78-59-109/18/19 08:32381 82.7 1
1-Methylnaphthalene ND ug/kg 09/18/19 15:40 90-12-009/18/19 08:32381 101 1
2-Methylnaphthalene ND ug/kg 09/18/19 15:40 91-57-609/18/19 08:32381 96.9 1
2-Methylphenol(o-Cresol)ND ug/kg 09/18/19 15:40 95-48-709/18/19 08:32381 84.3 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 09/18/19 15:40 15831-10-409/18/19 08:32381 95.7 1
Naphthalene ND ug/kg 09/18/19 15:40 91-20-309/18/19 08:32381 91.1 1
2-Nitroaniline ND ug/kg 09/18/19 15:40 88-74-409/18/19 08:321900 191 1
3-Nitroaniline ND ug/kg 09/18/19 15:40 99-09-209/18/19 08:321900 202 1
4-Nitroaniline ND ug/kg 09/18/19 15:40 100-01-609/18/19 08:32761 188 1
Nitrobenzene ND ug/kg 09/18/19 15:40 98-95-309/18/19 08:32381 90.9 1
2-Nitrophenol ND ug/kg 09/18/19 15:40 88-75-509/18/19 08:32381 118 1
4-Nitrophenol ND ug/kg 09/18/19 15:40 100-02-709/18/19 08:321900 606 1
N-Nitrosodimethylamine ND ug/kg 09/18/19 15:40 62-75-909/18/19 08:32381 107 1
N-Nitroso-di-n-propylamine ND ug/kg 09/18/19 15:40 621-64-709/18/19 08:32381 107 1
N-Nitrosodiphenylamine ND ug/kg 09/18/19 15:40 86-30-609/18/19 08:32381 97.1 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 09/18/19 15:40 108-60-1 v109/18/19 08:32381 106 1
Pentachlorophenol ND ug/kg 09/18/19 15:40 87-86-509/18/19 08:321900 174 1
Phenanthrene ND ug/kg 09/18/19 15:40 85-01-809/18/19 08:32381 95.8 1
Phenol ND ug/kg 09/18/19 15:40 108-95-209/18/19 08:32381 90.9 1
Pyrene ND ug/kg 09/18/19 15:40 129-00-009/18/19 08:32381 105 1
Pyridine ND ug/kg 09/18/19 15:40 110-86-109/18/19 08:32381 96.3 1
1,2,4-Trichlorobenzene ND ug/kg 09/18/19 15:40 120-82-109/18/19 08:32381 87.2 1
2,4,5-Trichlorophenol ND ug/kg 09/18/19 15:40 95-95-409/18/19 08:32381 98.8 1
2,4,6-Trichlorophenol ND ug/kg 09/18/19 15:40 88-06-209/18/19 08:32381 95.6 1
Surrogates
Nitrobenzene-d5 (S)50 %09/18/19 15:40 4165-60-009/18/19 08:3223-110 1
2-Fluorobiphenyl (S)55 %09/18/19 15:40 321-60-809/18/19 08:3230-110 1
Terphenyl-d14 (S)62 %09/18/19 15:40 1718-51-009/18/19 08:3228-110 1
Phenol-d6 (S)53 %09/18/19 15:40 13127-88-309/18/19 08:3222-110 1
2-Fluorophenol (S)54 %09/18/19 15:40 367-12-409/18/19 08:3213-110 1
2,4,6-Tribromophenol (S)70 %09/18/19 15:40 118-79-609/18/19 08:3227-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 14 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92445872
DCY-001
Sample: P4A Lab ID: 92445872003 Collected: 09/16/19 12:00 Received: 09/17/19 12:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 09/21/19 18:32 67-64-109/21/19 11:49130 12.3 1
Benzene ND ug/kg 09/21/19 18:32 71-43-209/21/19 11:496.5 1.2 1
Bromobenzene ND ug/kg 09/21/19 18:32 108-86-109/21/19 11:496.5 1.8 1
Bromochloromethane ND ug/kg 09/21/19 18:32 74-97-509/21/19 11:496.5 1.6 1
Bromodichloromethane ND ug/kg 09/21/19 18:32 75-27-409/21/19 11:496.5 1.3 1
Bromoform ND ug/kg 09/21/19 18:32 75-25-209/21/19 11:496.5 3.2 1
Bromomethane ND ug/kg 09/21/19 18:32 74-83-909/21/19 11:4913.0 3.1 1
2-Butanone (MEK)ND ug/kg 09/21/19 18:32 78-93-309/21/19 11:49130 15.5 1
n-Butylbenzene ND ug/kg 09/21/19 18:32 104-51-809/21/19 11:496.5 3.7 1
sec-Butylbenzene ND ug/kg 09/21/19 18:32 135-98-809/21/19 11:496.5 2.8 1
tert-Butylbenzene ND ug/kg 09/21/19 18:32 98-06-609/21/19 11:496.5 2.2 1
Carbon tetrachloride ND ug/kg 09/21/19 18:32 56-23-509/21/19 11:496.5 1.2 1
Chlorobenzene ND ug/kg 09/21/19 18:32 108-90-709/21/19 11:496.5 1.3 1
Chloroethane ND ug/kg 09/21/19 18:32 75-00-309/21/19 11:4913.0 2.7 1
Chloroform ND ug/kg 09/21/19 18:32 67-66-309/21/19 11:496.5 1.4 1
Chloromethane ND ug/kg 09/21/19 18:32 74-87-3 L109/21/19 11:4913.0 4.3 1
2-Chlorotoluene ND ug/kg 09/21/19 18:32 95-49-809/21/19 11:496.5 2.0 1
4-Chlorotoluene ND ug/kg 09/21/19 18:32 106-43-409/21/19 11:496.5 2.0 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/21/19 18:32 96-12-809/21/19 11:496.5 3.3 1
Dibromochloromethane ND ug/kg 09/21/19 18:32 124-48-109/21/19 11:496.5 3.3 1
1,2-Dibromoethane (EDB)ND ug/kg 09/21/19 18:32 106-93-409/21/19 11:496.5 1.5 1
Dibromomethane ND ug/kg 09/21/19 18:32 74-95-309/21/19 11:496.5 1.9 1
1,2-Dichlorobenzene ND ug/kg 09/21/19 18:32 95-50-109/21/19 11:496.5 2.3 1
1,3-Dichlorobenzene ND ug/kg 09/21/19 18:32 541-73-109/21/19 11:496.5 2.3 1
1,4-Dichlorobenzene ND ug/kg 09/21/19 18:32 106-46-709/21/19 11:496.5 2.3 1
Dichlorodifluoromethane ND ug/kg 09/21/19 18:32 75-71-8 L109/21/19 11:4913.0 5.4 1
1,1-Dichloroethane ND ug/kg 09/21/19 18:32 75-34-309/21/19 11:496.5 0.96 1
1,2-Dichloroethane ND ug/kg 09/21/19 18:32 107-06-209/21/19 11:496.5 1.3 1
1,1-Dichloroethene ND ug/kg 09/21/19 18:32 75-35-409/21/19 11:496.5 1.5 1
cis-1,2-Dichloroethene ND ug/kg 09/21/19 18:32 156-59-209/21/19 11:496.5 1.1 1
trans-1,2-Dichloroethene ND ug/kg 09/21/19 18:32 156-60-509/21/19 11:496.5 1.3 1
1,2-Dichloropropane ND ug/kg 09/21/19 18:32 78-87-509/21/19 11:496.5 2.5 1
1,3-Dichloropropane ND ug/kg 09/21/19 18:32 142-28-909/21/19 11:496.5 2.5 1
2,2-Dichloropropane ND ug/kg 09/21/19 18:32 594-20-709/21/19 11:496.5 0.64 1
1,1-Dichloropropene ND ug/kg 09/21/19 18:32 563-58-609/21/19 11:496.5 2.8 1
cis-1,3-Dichloropropene ND ug/kg 09/21/19 18:32 10061-01-509/21/19 11:496.5 3.0 1
trans-1,3-Dichloropropene ND ug/kg 09/21/19 18:32 10061-02-609/21/19 11:496.5 1.1 1
Diisopropyl ether ND ug/kg 09/21/19 18:32 108-20-309/21/19 11:496.5 3.7 1
Ethylbenzene 1.4J ug/kg 09/21/19 18:32 100-41-409/21/19 11:496.5 1.4 1
Hexachloro-1,3-butadiene ND ug/kg 09/21/19 18:32 87-68-309/21/19 11:496.5 3.2 1
2-Hexanone ND ug/kg 09/21/19 18:32 591-78-609/21/19 11:4965.2 6.8 1
Isopropylbenzene (Cumene)ND ug/kg 09/21/19 18:32 98-82-809/21/19 11:496.5 1.9 1
p-Isopropyltoluene ND ug/kg 09/21/19 18:32 99-87-609/21/19 11:496.5 3.1 1
Methylene Chloride ND ug/kg 09/21/19 18:32 75-09-209/21/19 11:4926.1 7.7 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/21/19 18:32 108-10-109/21/19 11:4965.2 4.9 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 15 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92445872
DCY-001
Sample: P4A Lab ID: 92445872003 Collected: 09/16/19 12:00 Received: 09/17/19 12:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 09/21/19 18:32 1634-04-409/21/19 11:496.5 3.7 1
Naphthalene ND ug/kg 09/21/19 18:32 91-20-309/21/19 11:496.5 5.5 1
n-Propylbenzene ND ug/kg 09/21/19 18:32 103-65-109/21/19 11:496.5 2.2 1
Styrene ND ug/kg 09/21/19 18:32 100-42-509/21/19 11:496.5 1.9 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/21/19 18:32 630-20-609/21/19 11:496.5 1.6 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/21/19 18:32 79-34-509/21/19 11:496.5 2.3 1
Tetrachloroethene ND ug/kg 09/21/19 18:32 127-18-409/21/19 11:496.5 2.1 1
Toluene 1'ug/kg 09/21/19 18:32 108-88-309/21/19 11:496.5 2.1 1
1,2,3-Trichlorobenzene ND ug/kg 09/21/19 18:32 87-61-609/21/19 11:496.5 4.7 1
1,2,4-Trichlorobenzene ND ug/kg 09/21/19 18:32 120-82-109/21/19 11:496.5 3.5 1
1,1,1-Trichloroethane ND ug/kg 09/21/19 18:32 71-55-609/21/19 11:496.5 1.1 1
1,1,2-Trichloroethane ND ug/kg 09/21/19 18:32 79-00-509/21/19 11:496.5 1.5 1
Trichloroethene ND ug/kg 09/21/19 18:32 79-01-609/21/19 11:496.5 1.7 1
Trichlorofluoromethane ND ug/kg 09/21/19 18:32 75-69-4 L109/21/19 11:496.5 1.5 1
1,2,3-Trichloropropane ND ug/kg 09/21/19 18:32 96-18-409/21/19 11:496.5 2.2 1
1,2,4-Trimethylbenzene ND ug/kg 09/21/19 18:32 95-63-609/21/19 11:496.5 2.5 1
1,3,5-Trimethylbenzene ND ug/kg 09/21/19 18:32 108-67-809/21/19 11:496.5 2.2 1
Vinyl acetate ND ug/kg 09/21/19 18:32 108-05-4 L109/21/19 11:4965.2 21.3 1
Vinyl chloride ND ug/kg 09/21/19 18:32 75-01-4 L109/21/19 11:4913.0 2.5 1
Xylene (Total)ND ug/kg 09/21/19 18:32 1330-20-709/21/19 11:4913.0 4.6 1
m&p-Xylene 1'ug/kg 09/21/19 18:32 179601-23-109/21/19 11:4913.0 3.1 1
o-Xylene 1'ug/kg 09/21/19 18:32 95-47-609/21/19 11:496.5 1.5 1
Surrogates
Toluene-d8 (S)108 %09/21/19 18:32 2037-26-509/21/19 11:4970-130 1
4-Bromofluorobenzene (S)104 %09/21/19 18:32 460-00-409/21/19 11:4970-130 1
1,2-Dichloroethane-d4 (S)95 %09/21/19 18:32 17060-07-009/21/19 11:4970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 13.8 %09/17/19 16:070.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 84.9 %09/23/19 15:3409/23/19 15:271
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 16 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92445872
DCY-001
Sample: P4B Lab ID: 92445872004 Collected: 09/16/19 12:35 Received: 09/17/19 12:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051Metals (ICPMS) 6020B
Arsenic 3.61 mg/kg 09/21/19 15:21 7440-38-209/21/19 11:230.586 0.146 5
Barium 80.3 mg/kg 09/21/19 15:21 7440-39-309/21/19 11:231.17 0.187 5
Cadmium ND mg/kg 09/21/19 15:21 7440-43-909/21/19 11:230.586 0.0937 5
Chromium 109 mg/kg 09/21/19 15:21 7440-47-309/21/19 11:231.17 0.316 5
Lead 10.5 mg/kg 09/21/19 15:21 7439-92-109/21/19 11:230.586 0.141 5
Selenium 0.707 mg/kg 09/21/19 15:21 7782-49-209/21/19 11:230.586 0.222 5
Silver ND mg/kg 09/21/19 15:21 7440-22-409/21/19 11:230.586 0.182 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 0.0168J mg/kg 09/19/19 20:15 7439-97-609/19/19 12:510.0351 0.00328 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 09/18/19 16:13 83-32-909/18/19 08:32392 101 1
Acenaphthylene ND ug/kg 09/18/19 16:13 208-96-809/18/19 08:32392 92.7 1
Aniline ND ug/kg 09/18/19 16:13 62-53-309/18/19 08:32392 87.9 1
Anthracene ND ug/kg 09/18/19 16:13 120-12-709/18/19 08:32392 102 1
Benzo(a)anthracene ND ug/kg 09/18/19 16:13 56-55-309/18/19 08:32392 125 1
Benzo(a)pyrene ND ug/kg 09/18/19 16:13 50-32-809/18/19 08:32392 170 1
Benzo(b)fluoranthene ND ug/kg 09/18/19 16:13 205-99-209/18/19 08:32392 158 1
Benzo(g,h,i)perylene ND ug/kg 09/18/19 16:13 191-24-209/18/19 08:32392 153 1
Benzo(k)fluoranthene ND ug/kg 09/18/19 16:13 207-08-909/18/19 08:32392 165 1
Benzoic Acid ND ug/kg 09/18/19 16:13 65-85-009/18/19 08:321960 422 1
Benzyl alcohol ND ug/kg 09/18/19 16:13 100-51-609/18/19 08:32783 208 1
4-Bromophenylphenyl ether ND ug/kg 09/18/19 16:13 101-55-309/18/19 08:32392 103 1
Butylbenzylphthalate ND ug/kg 09/18/19 16:13 85-68-709/18/19 08:32392 104 1
4-Chloro-3-methylphenol ND ug/kg 09/18/19 16:13 59-50-709/18/19 08:32783 239 1
4-Chloroaniline ND ug/kg 09/18/19 16:13 106-47-809/18/19 08:321960 240 1
bis(2-Chloroethoxy)methane ND ug/kg 09/18/19 16:13 111-91-109/18/19 08:32392 105 1
bis(2-Chloroethyl) ether ND ug/kg 09/18/19 16:13 111-44-409/18/19 08:32392 83.2 1
2-Chloronaphthalene ND ug/kg 09/18/19 16:13 91-58-709/18/19 08:32392 87.2 1
2-Chlorophenol ND ug/kg 09/18/19 16:13 95-57-809/18/19 08:32392 91.1 1
4-Chlorophenylphenyl ether ND ug/kg 09/18/19 16:13 7005-72-309/18/19 08:32392 102 1
Chrysene ND ug/kg 09/18/19 16:13 218-01-909/18/19 08:32392 114 1
Dibenz(a,h)anthracene ND ug/kg 09/18/19 16:13 53-70-309/18/19 08:32392 157 1
Dibenzofuran ND ug/kg 09/18/19 16:13 132-64-909/18/19 08:32392 97.9 1
1,2-Dichlorobenzene ND ug/kg 09/18/19 16:13 95-50-109/18/19 08:32392 84.7 1
1,3-Dichlorobenzene ND ug/kg 09/18/19 16:13 541-73-109/18/19 08:32392 88.2 1
1,4-Dichlorobenzene ND ug/kg 09/18/19 16:13 106-46-709/18/19 08:32392 86.2 1
3,3'-Dichlorobenzidine ND ug/kg 09/18/19 16:13 91-94-109/18/19 08:321960 273 1
2,4-Dichlorophenol ND ug/kg 09/18/19 16:13 120-83-209/18/19 08:32392 129 1
Diethylphthalate ND ug/kg 09/18/19 16:13 84-66-209/18/19 08:32392 85.0 1
2,4-Dimethylphenol ND ug/kg 09/18/19 16:13 105-67-909/18/19 08:32392 97.6 1
Dimethylphthalate ND ug/kg 09/18/19 16:13 131-11-309/18/19 08:32392 88.5 1
Di-n-butylphthalate ND ug/kg 09/18/19 16:13 84-74-209/18/19 08:32392 96.6 1
4,6-Dinitro-2-methylphenol ND ug/kg 09/18/19 16:13 534-52-109/18/19 08:32783 631 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 17 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92445872
DCY-001
Sample: P4B Lab ID: 92445872004 Collected: 09/16/19 12:35 Received: 09/17/19 12:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 09/18/19 16:13 51-28-509/18/19 08:321960 1250 1
2,4-Dinitrotoluene ND ug/kg 09/18/19 16:13 121-14-209/18/19 08:32392 104 1
2,6-Dinitrotoluene ND ug/kg 09/18/19 16:13 606-20-209/18/19 08:32392 102 1
Di-n-octylphthalate ND ug/kg 09/18/19 16:13 117-84-009/18/19 08:32392 223 1
bis(2-Ethylhexyl)phthalate ND ug/kg 09/18/19 16:13 117-81-709/18/19 08:32392 128 1
Fluoranthene ND ug/kg 09/18/19 16:13 206-44-009/18/19 08:32392 118 1
Fluorene ND ug/kg 09/18/19 16:13 86-73-709/18/19 08:32392 105 1
Hexachloro-1,3-butadiene ND ug/kg 09/18/19 16:13 87-68-309/18/19 08:32392 95.2 1
Hexachlorobenzene ND ug/kg 09/18/19 16:13 118-74-109/18/19 08:32392 99.4 1
Hexachlorocyclopentadiene ND ug/kg 09/18/19 16:13 77-47-4 v209/18/19 08:32392 157 1
Hexachloroethane ND ug/kg 09/18/19 16:13 67-72-109/18/19 08:32392 89.2 1
Indeno(1,2,3-cd)pyrene ND ug/kg 09/18/19 16:13 193-39-509/18/19 08:32392 179 1
Isophorone ND ug/kg 09/18/19 16:13 78-59-109/18/19 08:32392 85.1 1
1-Methylnaphthalene ND ug/kg 09/18/19 16:13 90-12-009/18/19 08:32392 104 1
2-Methylnaphthalene ND ug/kg 09/18/19 16:13 91-57-609/18/19 08:32392 99.7 1
2-Methylphenol(o-Cresol)ND ug/kg 09/18/19 16:13 95-48-709/18/19 08:32392 86.8 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 09/18/19 16:13 15831-10-409/18/19 08:32392 98.5 1
Naphthalene ND ug/kg 09/18/19 16:13 91-20-309/18/19 08:32392 93.8 1
2-Nitroaniline ND ug/kg 09/18/19 16:13 88-74-409/18/19 08:321960 197 1
3-Nitroaniline ND ug/kg 09/18/19 16:13 99-09-209/18/19 08:321960 208 1
4-Nitroaniline ND ug/kg 09/18/19 16:13 100-01-609/18/19 08:32783 193 1
Nitrobenzene ND ug/kg 09/18/19 16:13 98-95-309/18/19 08:32392 93.5 1
2-Nitrophenol ND ug/kg 09/18/19 16:13 88-75-509/18/19 08:32392 121 1
4-Nitrophenol ND ug/kg 09/18/19 16:13 100-02-709/18/19 08:321960 624 1
N-Nitrosodimethylamine ND ug/kg 09/18/19 16:13 62-75-909/18/19 08:32392 110 1
N-Nitroso-di-n-propylamine ND ug/kg 09/18/19 16:13 621-64-709/18/19 08:32392 110 1
N-Nitrosodiphenylamine ND ug/kg 09/18/19 16:13 86-30-609/18/19 08:32392 99.9 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 09/18/19 16:13 108-60-1 v109/18/19 08:32392 109 1
Pentachlorophenol ND ug/kg 09/18/19 16:13 87-86-509/18/19 08:321960 179 1
Phenanthrene ND ug/kg 09/18/19 16:13 85-01-809/18/19 08:32392 98.6 1
Phenol ND ug/kg 09/18/19 16:13 108-95-209/18/19 08:32392 93.5 1
Pyrene ND ug/kg 09/18/19 16:13 129-00-009/18/19 08:32392 108 1
Pyridine ND ug/kg 09/18/19 16:13 110-86-109/18/19 08:32392 99.1 1
1,2,4-Trichlorobenzene ND ug/kg 09/18/19 16:13 120-82-109/18/19 08:32392 89.7 1
2,4,5-Trichlorophenol ND ug/kg 09/18/19 16:13 95-95-409/18/19 08:32392 102 1
2,4,6-Trichlorophenol ND ug/kg 09/18/19 16:13 88-06-209/18/19 08:32392 98.4 1
Surrogates
Nitrobenzene-d5 (S)56 %09/18/19 16:13 4165-60-009/18/19 08:3223-110 1
2-Fluorobiphenyl (S)58 %09/18/19 16:13 321-60-809/18/19 08:3230-110 1
Terphenyl-d14 (S)69 %09/18/19 16:13 1718-51-009/18/19 08:3228-110 1
Phenol-d6 (S)55 %09/18/19 16:13 13127-88-309/18/19 08:3222-110 1
2-Fluorophenol (S)57 %09/18/19 16:13 367-12-409/18/19 08:3213-110 1
2,4,6-Tribromophenol (S)77 %09/18/19 16:13 118-79-609/18/19 08:3227-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92445872
DCY-001
Sample: P4B Lab ID: 92445872004 Collected: 09/16/19 12:35 Received: 09/17/19 12:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 09/21/19 18:57 67-64-109/21/19 11:49111 10.5 1
Benzene ND ug/kg 09/21/19 18:57 71-43-209/21/19 11:495.5 0.99 1
Bromobenzene ND ug/kg 09/21/19 18:57 108-86-109/21/19 11:495.5 1.5 1
Bromochloromethane ND ug/kg 09/21/19 18:57 74-97-509/21/19 11:495.5 1.4 1
Bromodichloromethane ND ug/kg 09/21/19 18:57 75-27-409/21/19 11:495.5 1.1 1
Bromoform ND ug/kg 09/21/19 18:57 75-25-209/21/19 11:495.5 2.7 1
Bromomethane ND ug/kg 09/21/19 18:57 74-83-9 v209/21/19 11:4911.1 2.6 1
2-Butanone (MEK)ND ug/kg 09/21/19 18:57 78-93-309/21/19 11:49111 13.2 1
n-Butylbenzene ND ug/kg 09/21/19 18:57 104-51-809/21/19 11:495.5 3.1 1
sec-Butylbenzene ND ug/kg 09/21/19 18:57 135-98-809/21/19 11:495.5 2.3 1
tert-Butylbenzene ND ug/kg 09/21/19 18:57 98-06-609/21/19 11:495.5 1.9 1
Carbon tetrachloride ND ug/kg 09/21/19 18:57 56-23-509/21/19 11:495.5 1.1 1
Chlorobenzene ND ug/kg 09/21/19 18:57 108-90-709/21/19 11:495.5 1.1 1
Chloroethane ND ug/kg 09/21/19 18:57 75-00-3 v209/21/19 11:4911.1 2.3 1
Chloroform ND ug/kg 09/21/19 18:57 67-66-309/21/19 11:495.5 1.2 1
Chloromethane ND ug/kg 09/21/19 18:57 74-87-3 L1,v209/21/19 11:4911.1 3.6 1
2-Chlorotoluene ND ug/kg 09/21/19 18:57 95-49-809/21/19 11:495.5 1.7 1
4-Chlorotoluene ND ug/kg 09/21/19 18:57 106-43-409/21/19 11:495.5 1.7 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/21/19 18:57 96-12-809/21/19 11:495.5 2.8 1
Dibromochloromethane ND ug/kg 09/21/19 18:57 124-48-109/21/19 11:495.5 2.8 1
1,2-Dibromoethane (EDB)ND ug/kg 09/21/19 18:57 106-93-409/21/19 11:495.5 1.2 1
Dibromomethane ND ug/kg 09/21/19 18:57 74-95-309/21/19 11:495.5 1.7 1
1,2-Dichlorobenzene ND ug/kg 09/21/19 18:57 95-50-109/21/19 11:495.5 2.0 1
1,3-Dichlorobenzene ND ug/kg 09/21/19 18:57 541-73-109/21/19 11:495.5 2.0 1
1,4-Dichlorobenzene ND ug/kg 09/21/19 18:57 106-46-709/21/19 11:495.5 1.9 1
Dichlorodifluoromethane ND ug/kg 09/21/19 18:57 75-71-8 L1,v209/21/19 11:4911.1 4.6 1
1,1-Dichloroethane ND ug/kg 09/21/19 18:57 75-34-309/21/19 11:495.5 0.81 1
1,2-Dichloroethane ND ug/kg 09/21/19 18:57 107-06-209/21/19 11:495.5 1.1 1
1,1-Dichloroethene ND ug/kg 09/21/19 18:57 75-35-409/21/19 11:495.5 1.3 1
cis-1,2-Dichloroethene ND ug/kg 09/21/19 18:57 156-59-209/21/19 11:495.5 0.96 1
trans-1,2-Dichloroethene ND ug/kg 09/21/19 18:57 156-60-509/21/19 11:495.5 1.1 1
1,2-Dichloropropane ND ug/kg 09/21/19 18:57 78-87-509/21/19 11:495.5 2.1 1
1,3-Dichloropropane ND ug/kg 09/21/19 18:57 142-28-909/21/19 11:495.5 2.1 1
2,2-Dichloropropane ND ug/kg 09/21/19 18:57 594-20-709/21/19 11:495.5 0.55 1
1,1-Dichloropropene ND ug/kg 09/21/19 18:57 563-58-609/21/19 11:495.5 2.3 1
cis-1,3-Dichloropropene ND ug/kg 09/21/19 18:57 10061-01-509/21/19 11:495.5 2.5 1
trans-1,3-Dichloropropene ND ug/kg 09/21/19 18:57 10061-02-609/21/19 11:495.5 0.97 1
Diisopropyl ether ND ug/kg 09/21/19 18:57 108-20-309/21/19 11:495.5 3.2 1
Ethylbenzene ND ug/kg 09/21/19 18:57 100-41-409/21/19 11:495.5 1.2 1
Hexachloro-1,3-butadiene ND ug/kg 09/21/19 18:57 87-68-309/21/19 11:495.5 2.7 1
2-Hexanone ND ug/kg 09/21/19 18:57 591-78-609/21/19 11:4955.4 5.7 1
Isopropylbenzene (Cumene)ND ug/kg 09/21/19 18:57 98-82-809/21/19 11:495.5 1.6 1
p-Isopropyltoluene ND ug/kg 09/21/19 18:57 99-87-609/21/19 11:495.5 2.7 1
Methylene Chloride ND ug/kg 09/21/19 18:57 75-09-209/21/19 11:4922.2 6.5 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/21/19 18:57 108-10-109/21/19 11:4955.4 4.1 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 19 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92445872
DCY-001
Sample: P4B Lab ID: 92445872004 Collected: 09/16/19 12:35 Received: 09/17/19 12:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 09/21/19 18:57 1634-04-409/21/19 11:495.5 3.2 1
Naphthalene ND ug/kg 09/21/19 18:57 91-20-309/21/19 11:495.5 4.7 1
n-Propylbenzene ND ug/kg 09/21/19 18:57 103-65-109/21/19 11:495.5 1.9 1
Styrene ND ug/kg 09/21/19 18:57 100-42-509/21/19 11:495.5 1.6 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/21/19 18:57 630-20-609/21/19 11:495.5 1.4 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/21/19 18:57 79-34-509/21/19 11:495.5 1.9 1
Tetrachloroethene ND ug/kg 09/21/19 18:57 127-18-409/21/19 11:495.5 1.8 1
Toluene 1'ug/kg 09/21/19 18:57 108-88-309/21/19 11:495.5 1.8 1
1,2,3-Trichlorobenzene ND ug/kg 09/21/19 18:57 87-61-609/21/19 11:495.5 4.0 1
1,2,4-Trichlorobenzene ND ug/kg 09/21/19 18:57 120-82-109/21/19 11:495.5 2.9 1
1,1,1-Trichloroethane ND ug/kg 09/21/19 18:57 71-55-609/21/19 11:495.5 0.96 1
1,1,2-Trichloroethane ND ug/kg 09/21/19 18:57 79-00-509/21/19 11:495.5 1.3 1
Trichloroethene ND ug/kg 09/21/19 18:57 79-01-609/21/19 11:495.5 1.4 1
Trichlorofluoromethane ND ug/kg 09/21/19 18:57 75-69-4 L1,v209/21/19 11:495.5 1.3 1
1,2,3-Trichloropropane ND ug/kg 09/21/19 18:57 96-18-409/21/19 11:495.5 1.9 1
1,2,4-Trimethylbenzene ND ug/kg 09/21/19 18:57 95-63-609/21/19 11:495.5 2.2 1
1,3,5-Trimethylbenzene ND ug/kg 09/21/19 18:57 108-67-809/21/19 11:495.5 1.9 1
Vinyl acetate ND ug/kg 09/21/19 18:57 108-05-4 L109/21/19 11:4955.4 18.1 1
Vinyl chloride ND ug/kg 09/21/19 18:57 75-01-4 L1,v209/21/19 11:4911.1 2.1 1
Xylene (Total)ND ug/kg 09/21/19 18:57 1330-20-709/21/19 11:4911.1 3.9 1
m&p-Xylene 1'ug/kg 09/21/19 18:57 179601-23-109/21/19 11:4911.1 2.6 1
o-Xylene 1'ug/kg 09/21/19 18:57 95-47-609/21/19 11:495.5 1.3 1
Surrogates
Toluene-d8 (S)108 %09/21/19 18:57 2037-26-509/21/19 11:4970-130 1
4-Bromofluorobenzene (S)101 %09/21/19 18:57 460-00-409/21/19 11:4970-130 1
1,2-Dichloroethane-d4 (S)94 %09/21/19 18:57 17060-07-009/21/19 11:4970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 16.3 %09/17/19 16:070.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 85.4 %09/23/19 15:3409/23/19 15:271
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 20 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92445872
DCY-001
Sample: P4C Lab ID: 92445872005 Collected: 09/16/19 13:00 Received: 09/17/19 12:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 6020B Preparation Method: 3051Metals (ICPMS) 6020B
Arsenic 6.25 mg/kg 09/21/19 15:24 7440-38-209/21/19 11:230.560 0.140 5
Barium 95.4 mg/kg 09/21/19 15:24 7440-39-309/21/19 11:231.12 0.179 5
Cadmium ND mg/kg 09/21/19 15:24 7440-43-909/21/19 11:230.560 0.0896 5
Chromium 88.7 mg/kg 09/21/19 15:24 7440-47-309/21/19 11:231.12 0.302 5
Lead 9.37 mg/kg 09/21/19 15:24 7439-92-109/21/19 11:230.560 0.134 5
Selenium 0.393J mg/kg 09/21/19 15:24 7782-49-209/21/19 11:230.560 0.213 5
Silver ND mg/kg 09/21/19 15:24 7440-22-409/21/19 11:230.560 0.174 5
Analytical Method: EPA 7471B Preparation Method: 7471AMercury 7471B
Mercury 0.00680J mg/kg 09/19/19 20:18 7439-97-609/19/19 12:510.0336 0.00314 1
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
Acenaphthene ND ug/kg 09/18/19 16:46 83-32-909/18/19 08:32376 96.7 1
Acenaphthylene ND ug/kg 09/18/19 16:46 208-96-809/18/19 08:32376 89.0 1
Aniline ND ug/kg 09/18/19 16:46 62-53-309/18/19 08:32376 84.4 1
Anthracene ND ug/kg 09/18/19 16:46 120-12-709/18/19 08:32376 97.5 1
Benzo(a)anthracene ND ug/kg 09/18/19 16:46 56-55-309/18/19 08:32376 120 1
Benzo(a)pyrene ND ug/kg 09/18/19 16:46 50-32-809/18/19 08:32376 163 1
Benzo(b)fluoranthene ND ug/kg 09/18/19 16:46 205-99-209/18/19 08:32376 152 1
Benzo(g,h,i)perylene ND ug/kg 09/18/19 16:46 191-24-209/18/19 08:32376 147 1
Benzo(k)fluoranthene ND ug/kg 09/18/19 16:46 207-08-909/18/19 08:32376 158 1
Benzoic Acid ND ug/kg 09/18/19 16:46 65-85-009/18/19 08:321880 406 1
Benzyl alcohol ND ug/kg 09/18/19 16:46 100-51-609/18/19 08:32752 199 1
4-Bromophenylphenyl ether ND ug/kg 09/18/19 16:46 101-55-309/18/19 08:32376 98.7 1
Butylbenzylphthalate ND ug/kg 09/18/19 16:46 85-68-709/18/19 08:32376 100 1
4-Chloro-3-methylphenol ND ug/kg 09/18/19 16:46 59-50-709/18/19 08:32752 229 1
4-Chloroaniline ND ug/kg 09/18/19 16:46 106-47-809/18/19 08:321880 230 1
bis(2-Chloroethoxy)methane ND ug/kg 09/18/19 16:46 111-91-109/18/19 08:32376 100 1
bis(2-Chloroethyl) ether ND ug/kg 09/18/19 16:46 111-44-409/18/19 08:32376 79.9 1
2-Chloronaphthalene ND ug/kg 09/18/19 16:46 91-58-709/18/19 08:32376 83.7 1
2-Chlorophenol ND ug/kg 09/18/19 16:46 95-57-809/18/19 08:32376 87.5 1
4-Chlorophenylphenyl ether ND ug/kg 09/18/19 16:46 7005-72-309/18/19 08:32376 97.6 1
Chrysene ND ug/kg 09/18/19 16:46 218-01-909/18/19 08:32376 109 1
Dibenz(a,h)anthracene ND ug/kg 09/18/19 16:46 53-70-309/18/19 08:32376 150 1
Dibenzofuran ND ug/kg 09/18/19 16:46 132-64-909/18/19 08:32376 94.0 1
1,2-Dichlorobenzene ND ug/kg 09/18/19 16:46 95-50-109/18/19 08:32376 81.4 1
1,3-Dichlorobenzene ND ug/kg 09/18/19 16:46 541-73-109/18/19 08:32376 84.7 1
1,4-Dichlorobenzene ND ug/kg 09/18/19 16:46 106-46-709/18/19 08:32376 82.7 1
3,3'-Dichlorobenzidine ND ug/kg 09/18/19 16:46 91-94-109/18/19 08:321880 262 1
2,4-Dichlorophenol ND ug/kg 09/18/19 16:46 120-83-209/18/19 08:32376 124 1
Diethylphthalate ND ug/kg 09/18/19 16:46 84-66-209/18/19 08:32376 81.6 1
2,4-Dimethylphenol ND ug/kg 09/18/19 16:46 105-67-909/18/19 08:32376 93.7 1
Dimethylphthalate ND ug/kg 09/18/19 16:46 131-11-309/18/19 08:32376 85.0 1
Di-n-butylphthalate ND ug/kg 09/18/19 16:46 84-74-209/18/19 08:32376 92.7 1
4,6-Dinitro-2-methylphenol ND ug/kg 09/18/19 16:46 534-52-109/18/19 08:32752 606 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
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Page 21 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92445872
DCY-001
Sample: P4C Lab ID: 92445872005 Collected: 09/16/19 13:00 Received: 09/17/19 12:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8270E Preparation Method: EPA 35468270E MSSV Microwave
2,4-Dinitrophenol ND ug/kg 09/18/19 16:46 51-28-509/18/19 08:321880 1200 1
2,4-Dinitrotoluene ND ug/kg 09/18/19 16:46 121-14-209/18/19 08:32376 99.6 1
2,6-Dinitrotoluene ND ug/kg 09/18/19 16:46 606-20-209/18/19 08:32376 98.3 1
Di-n-octylphthalate ND ug/kg 09/18/19 16:46 117-84-009/18/19 08:32376 214 1
bis(2-Ethylhexyl)phthalate ND ug/kg 09/18/19 16:46 117-81-709/18/19 08:32376 123 1
Fluoranthene ND ug/kg 09/18/19 16:46 206-44-009/18/19 08:32376 114 1
Fluorene ND ug/kg 09/18/19 16:46 86-73-709/18/19 08:32376 101 1
Hexachloro-1,3-butadiene ND ug/kg 09/18/19 16:46 87-68-309/18/19 08:32376 91.4 1
Hexachlorobenzene ND ug/kg 09/18/19 16:46 118-74-109/18/19 08:32376 95.5 1
Hexachlorocyclopentadiene ND ug/kg 09/18/19 16:46 77-47-4 v209/18/19 08:32376 150 1
Hexachloroethane ND ug/kg 09/18/19 16:46 67-72-109/18/19 08:32376 85.7 1
Indeno(1,2,3-cd)pyrene ND ug/kg 09/18/19 16:46 193-39-509/18/19 08:32376 172 1
Isophorone ND ug/kg 09/18/19 16:46 78-59-109/18/19 08:32376 81.7 1
1-Methylnaphthalene ND ug/kg 09/18/19 16:46 90-12-009/18/19 08:32376 100 1
2-Methylnaphthalene ND ug/kg 09/18/19 16:46 91-57-609/18/19 08:32376 95.7 1
2-Methylphenol(o-Cresol)ND ug/kg 09/18/19 16:46 95-48-709/18/19 08:32376 83.3 1
3&4-Methylphenol(m&p Cresol)ND ug/kg 09/18/19 16:46 15831-10-409/18/19 08:32376 94.6 1
Naphthalene ND ug/kg 09/18/19 16:46 91-20-309/18/19 08:32376 90.0 1
2-Nitroaniline ND ug/kg 09/18/19 16:46 88-74-409/18/19 08:321880 189 1
3-Nitroaniline ND ug/kg 09/18/19 16:46 99-09-209/18/19 08:321880 199 1
4-Nitroaniline ND ug/kg 09/18/19 16:46 100-01-609/18/19 08:32752 186 1
Nitrobenzene ND ug/kg 09/18/19 16:46 98-95-309/18/19 08:32376 89.8 1
2-Nitrophenol ND ug/kg 09/18/19 16:46 88-75-509/18/19 08:32376 116 1
4-Nitrophenol ND ug/kg 09/18/19 16:46 100-02-709/18/19 08:321880 599 1
N-Nitrosodimethylamine ND ug/kg 09/18/19 16:46 62-75-909/18/19 08:32376 106 1
N-Nitroso-di-n-propylamine ND ug/kg 09/18/19 16:46 621-64-709/18/19 08:32376 105 1
N-Nitrosodiphenylamine ND ug/kg 09/18/19 16:46 86-30-609/18/19 08:32376 95.9 1
2,2'-Oxybis(1-chloropropane)ND ug/kg 09/18/19 16:46 108-60-1 v109/18/19 08:32376 104 1
Pentachlorophenol ND ug/kg 09/18/19 16:46 87-86-509/18/19 08:321880 172 1
Phenanthrene ND ug/kg 09/18/19 16:46 85-01-809/18/19 08:32376 94.7 1
Phenol ND ug/kg 09/18/19 16:46 108-95-209/18/19 08:32376 89.8 1
Pyrene ND ug/kg 09/18/19 16:46 129-00-009/18/19 08:32376 103 1
Pyridine ND ug/kg 09/18/19 16:46 110-86-109/18/19 08:32376 95.1 1
1,2,4-Trichlorobenzene ND ug/kg 09/18/19 16:46 120-82-109/18/19 08:32376 86.1 1
2,4,5-Trichlorophenol ND ug/kg 09/18/19 16:46 95-95-409/18/19 08:32376 97.6 1
2,4,6-Trichlorophenol ND ug/kg 09/18/19 16:46 88-06-209/18/19 08:32376 94.5 1
Surrogates
Nitrobenzene-d5 (S)28 %09/18/19 16:46 4165-60-009/18/19 08:3223-110 1
2-Fluorobiphenyl (S)31 %09/18/19 16:46 321-60-809/18/19 08:3230-110 1
Terphenyl-d14 (S)54 %09/18/19 16:46 1718-51-009/18/19 08:3228-110 1
Phenol-d6 (S)30 %09/18/19 16:46 13127-88-309/18/19 08:3222-110 1
2-Fluorophenol (S)25 %09/18/19 16:46 367-12-409/18/19 08:3213-110 1
2,4,6-Tribromophenol (S)54 %09/18/19 16:46 118-79-609/18/19 08:3227-110 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
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Page 22 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92445872
DCY-001
Sample: P4C Lab ID: 92445872005 Collected: 09/16/19 13:00 Received: 09/17/19 12:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Acetone ND ug/kg 09/21/19 19:22 67-64-109/21/19 11:49118 11.2 1
Benzene ND ug/kg 09/21/19 19:22 71-43-209/21/19 11:495.9 1.1 1
Bromobenzene ND ug/kg 09/21/19 19:22 108-86-109/21/19 11:495.9 1.6 1
Bromochloromethane ND ug/kg 09/21/19 19:22 74-97-509/21/19 11:495.9 1.5 1
Bromodichloromethane ND ug/kg 09/21/19 19:22 75-27-409/21/19 11:495.9 1.2 1
Bromoform ND ug/kg 09/21/19 19:22 75-25-209/21/19 11:495.9 2.9 1
Bromomethane ND ug/kg 09/21/19 19:22 74-83-9 v209/21/19 11:4911.8 2.8 1
2-Butanone (MEK)ND ug/kg 09/21/19 19:22 78-93-309/21/19 11:49118 14.1 1
n-Butylbenzene ND ug/kg 09/21/19 19:22 104-51-809/21/19 11:495.9 3.3 1
sec-Butylbenzene ND ug/kg 09/21/19 19:22 135-98-809/21/19 11:495.9 2.5 1
tert-Butylbenzene ND ug/kg 09/21/19 19:22 98-06-609/21/19 11:495.9 2.0 1
Carbon tetrachloride ND ug/kg 09/21/19 19:22 56-23-509/21/19 11:495.9 1.1 1
Chlorobenzene ND ug/kg 09/21/19 19:22 108-90-709/21/19 11:495.9 1.1 1
Chloroethane ND ug/kg 09/21/19 19:22 75-00-3 v209/21/19 11:4911.8 2.5 1
Chloroform ND ug/kg 09/21/19 19:22 67-66-309/21/19 11:495.9 1.3 1
Chloromethane ND ug/kg 09/21/19 19:22 74-87-3 L1,v209/21/19 11:4911.8 3.9 1
2-Chlorotoluene ND ug/kg 09/21/19 19:22 95-49-809/21/19 11:495.9 1.8 1
4-Chlorotoluene ND ug/kg 09/21/19 19:22 106-43-409/21/19 11:495.9 1.8 1
1,2-Dibromo-3-chloropropane ND ug/kg 09/21/19 19:22 96-12-809/21/19 11:495.9 3.0 1
Dibromochloromethane ND ug/kg 09/21/19 19:22 124-48-109/21/19 11:495.9 3.0 1
1,2-Dibromoethane (EDB)ND ug/kg 09/21/19 19:22 106-93-409/21/19 11:495.9 1.3 1
Dibromomethane ND ug/kg 09/21/19 19:22 74-95-309/21/19 11:495.9 1.8 1
1,2-Dichlorobenzene ND ug/kg 09/21/19 19:22 95-50-109/21/19 11:495.9 2.1 1
1,3-Dichlorobenzene ND ug/kg 09/21/19 19:22 541-73-109/21/19 11:495.9 2.1 1
1,4-Dichlorobenzene ND ug/kg 09/21/19 19:22 106-46-709/21/19 11:495.9 2.0 1
Dichlorodifluoromethane ND ug/kg 09/21/19 19:22 75-71-8 L1,v209/21/19 11:4911.8 4.9 1
1,1-Dichloroethane ND ug/kg 09/21/19 19:22 75-34-309/21/19 11:495.9 0.87 1
1,2-Dichloroethane ND ug/kg 09/21/19 19:22 107-06-209/21/19 11:495.9 1.2 1
1,1-Dichloroethene ND ug/kg 09/21/19 19:22 75-35-409/21/19 11:495.9 1.4 1
cis-1,2-Dichloroethene ND ug/kg 09/21/19 19:22 156-59-209/21/19 11:495.9 1.0 1
trans-1,2-Dichloroethene ND ug/kg 09/21/19 19:22 156-60-509/21/19 11:495.9 1.2 1
1,2-Dichloropropane ND ug/kg 09/21/19 19:22 78-87-509/21/19 11:495.9 2.2 1
1,3-Dichloropropane ND ug/kg 09/21/19 19:22 142-28-909/21/19 11:495.9 2.2 1
2,2-Dichloropropane ND ug/kg 09/21/19 19:22 594-20-709/21/19 11:495.9 0.58 1
1,1-Dichloropropene ND ug/kg 09/21/19 19:22 563-58-609/21/19 11:495.9 2.5 1
cis-1,3-Dichloropropene ND ug/kg 09/21/19 19:22 10061-01-509/21/19 11:495.9 2.7 1
trans-1,3-Dichloropropene ND ug/kg 09/21/19 19:22 10061-02-609/21/19 11:495.9 1.0 1
Diisopropyl ether ND ug/kg 09/21/19 19:22 108-20-309/21/19 11:495.9 3.4 1
Ethylbenzene ND ug/kg 09/21/19 19:22 100-41-409/21/19 11:495.9 1.3 1
Hexachloro-1,3-butadiene ND ug/kg 09/21/19 19:22 87-68-309/21/19 11:495.9 2.9 1
2-Hexanone ND ug/kg 09/21/19 19:22 591-78-609/21/19 11:4959.2 6.1 1
Isopropylbenzene (Cumene)ND ug/kg 09/21/19 19:22 98-82-809/21/19 11:495.9 1.7 1
p-Isopropyltoluene ND ug/kg 09/21/19 19:22 99-87-609/21/19 11:495.9 2.9 1
Methylene Chloride ND ug/kg 09/21/19 19:22 75-09-209/21/19 11:4923.7 7.0 1
4-Methyl-2-pentanone (MIBK)ND ug/kg 09/21/19 19:22 108-10-109/21/19 11:4959.2 4.4 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 23 of 44
#=AR#
ANALYTICAL RESULTS
Pace Project No.:
Project:
92445872
DCY-001
Sample: P4C Lab ID: 92445872005 Collected: 09/16/19 13:00 Received: 09/17/19 12:13 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimit
Report
Analytical Method: EPA 8260D Preparation Method: EPA 5035A8260D/5035A Volatile Organics
Methyl-tert-butyl ether ND ug/kg 09/21/19 19:22 1634-04-409/21/19 11:495.9 3.4 1
Naphthalene ND ug/kg 09/21/19 19:22 91-20-309/21/19 11:495.9 5.0 1
n-Propylbenzene ND ug/kg 09/21/19 19:22 103-65-109/21/19 11:495.9 2.0 1
Styrene ND ug/kg 09/21/19 19:22 100-42-509/21/19 11:495.9 1.8 1
1,1,1,2-Tetrachloroethane ND ug/kg 09/21/19 19:22 630-20-609/21/19 11:495.9 1.5 1
1,1,2,2-Tetrachloroethane ND ug/kg 09/21/19 19:22 79-34-509/21/19 11:495.9 2.0 1
Tetrachloroethene ND ug/kg 09/21/19 19:22 127-18-409/21/19 11:495.9 1.9 1
Toluene 1.9J ug/kg 09/21/19 19:22 108-88-309/21/19 11:495.9 1.9 1
1,2,3-Trichlorobenzene ND ug/kg 09/21/19 19:22 87-61-609/21/19 11:495.9 4.2 1
1,2,4-Trichlorobenzene ND ug/kg 09/21/19 19:22 120-82-109/21/19 11:495.9 3.1 1
1,1,1-Trichloroethane ND ug/kg 09/21/19 19:22 71-55-609/21/19 11:495.9 1.0 1
1,1,2-Trichloroethane ND ug/kg 09/21/19 19:22 79-00-509/21/19 11:495.9 1.3 1
Trichloroethene ND ug/kg 09/21/19 19:22 79-01-609/21/19 11:495.9 1.5 1
Trichlorofluoromethane ND ug/kg 09/21/19 19:22 75-69-4 L1,v209/21/19 11:495.9 1.4 1
1,2,3-Trichloropropane ND ug/kg 09/21/19 19:22 96-18-409/21/19 11:495.9 2.0 1
1,2,4-Trimethylbenzene ND ug/kg 09/21/19 19:22 95-63-609/21/19 11:495.9 2.3 1
1,3,5-Trimethylbenzene ND ug/kg 09/21/19 19:22 108-67-809/21/19 11:495.9 2.0 1
Vinyl acetate ND ug/kg 09/21/19 19:22 108-05-4 L109/21/19 11:4959.2 19.3 1
Vinyl chloride ND ug/kg 09/21/19 19:22 75-01-4 L1,v209/21/19 11:4911.8 2.2 1
Xylene (Total)ND ug/kg 09/21/19 19:22 1330-20-709/21/19 11:4911.8 4.1 1
m&p-Xylene 3.4J ug/kg 09/21/19 19:22 179601-23-109/21/19 11:4911.8 2.8 1
o-Xylene 1.5J ug/kg 09/21/19 19:22 95-47-609/21/19 11:495.9 1.4 1
Surrogates
Toluene-d8 (S)106 %09/21/19 19:22 2037-26-509/21/19 11:4970-130 1
4-Bromofluorobenzene (S)101 %09/21/19 19:22 460-00-409/21/19 11:4970-130 1
1,2-Dichloroethane-d4 (S)97 %09/21/19 19:22 17060-07-009/21/19 11:4970-132 1
Analytical Method: ASTM D2974-87Percent Moisture
Percent Moisture 12.5 %09/17/19 16:070.10 0.10 1
Analytical Method: SM 2540G Preparation Method: SM 2540 GTotal Solids 2540 G-2011
Total Solids 89.3 %09/23/19 15:3409/23/19 15:271
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 24 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92445872
DCY-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1349231
3051
EPA 6020B
Metals (ICPMS) 6020B
Associated Lab Samples: 92445872001, 92445872002, 92445872003, 92445872004, 92445872005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3453176-1
Associated Lab Samples:92445872001, 92445872002, 92445872003, 92445872004, 92445872005
Matrix: Solid
AnalyzedMDL
Arsenic mg/kg ND 0.500 09/21/19 14:210.125
Barium mg/kg ND 1.00 09/21/19 14:210.160
Cadmium mg/kg ND 0.500 09/21/19 14:210.0800
Chromium mg/kg ND 1.00 09/21/19 14:210.270
Lead mg/kg ND 0.500 09/21/19 14:210.120
Selenium mg/kg ND 0.500 09/21/19 14:210.190
Silver mg/kg ND 0.500 09/21/19 14:210.155
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3453176-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3453176-3
Arsenic mg/kg 88.8100 88.8 80.0-12095.395.3 6.96 20
Barium mg/kg 113100 113 80.0-12097.897.8 14.1 20
Cadmium mg/kg 94.3100 94.3 80.0-120102102 7.54 20
Chromium mg/kg 93.9100 93.9 80.0-12099.199.1 5.47 20
Lead mg/kg 91.1100 91.1 80.0-120100100 9.83 20
Selenium mg/kg 96.5100 96.5 80.0-120104104 7.17 20
Silver mg/kg 19.720.0 98.7 80.0-12010621.2 7.35 20
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3453176-6MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
92445872001
R3453176-7
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Arsenic mg/kg 22.8 96.0 75.0-12598.2 2.13 2022.87.43 117 119
Barium mg/kg 22.8 95.1 75.0-125118 12.4 2022.888.6 197 223
Cadmium mg/kg 22.8 111 75.0-125109 1.40 2022.80.0959 127 125
Chromium mg/kg MH22.8 107 75.0-125126 10.1 2022.883.8 205 227
Lead mg/kg 22.8 109 75.0-125111 1.94 2022.84.48 128 131
Selenium mg/kg 22.8 113 75.0-125109 4.07 2022.8ND 129 124
Silver mg/kg 4.56 115 75.0-125113 2.01 204.56ND 26.2 25.7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 25 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92445872
DCY-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1348788
7471A
EPA 7471B
Mercury 7471B
Associated Lab Samples: 92445872001, 92445872002, 92445872003, 92445872004, 92445872005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3452694-1
Associated Lab Samples:92445872001, 92445872002, 92445872003, 92445872004, 92445872005
Matrix: Solid
AnalyzedMDL
Mercury mg/kg ND 0.0300 09/19/19 19:200.00280
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3452694-2LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
R3452694-3
Mercury mg/kg 0.4900.500 98.0 80.0-12096.10.480 2.01 20
Parameter Units
MS
Result
% Rec
Limits Qual% RecConc.
R3452694-4MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
MSSpike
Result
L1140007-02
R3452694-5
MSD
Result
MSD
% Rec RPD RPD
Max
MSDMS
Spike
Conc.
Mercury mg/kg 0.500 85.1 75.0-12586.7 1.56 200.5000.0968 0.522 0.531
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 26 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92445872
DCY-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
499141
EPA 5035A
EPA 8260D
8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92445872001, 92445872002, 92445872003, 92445872004, 92445872005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2686540
Associated Lab Samples:92445872001, 92445872002, 92445872003, 92445872004, 92445872005
Matrix: Solid
AnalyzedMDL
1,1,1,2-Tetrachloroethane ug/kg ND 5.0 09/21/19 12:141.2
1,1,1-Trichloroethane ug/kg ND 5.0 09/21/19 12:140.87
1,1,2,2-Tetrachloroethane ug/kg ND 5.0 09/21/19 12:141.7
1,1,2-Trichloroethane ug/kg ND 5.0 09/21/19 12:141.1
1,1-Dichloroethane ug/kg ND 5.0 09/21/19 12:140.74
1,1-Dichloroethene ug/kg ND 5.0 09/21/19 12:141.2
1,1-Dichloropropene ug/kg ND 5.0 09/21/19 12:142.1
1,2,3-Trichlorobenzene ug/kg ND 5.0 09/21/19 12:143.6
1,2,3-Trichloropropane ug/kg ND 5.0 09/21/19 12:141.7
1,2,4-Trichlorobenzene ug/kg ND 5.0 09/21/19 12:142.6
1,2,4-Trimethylbenzene ug/kg ND 5.0 09/21/19 12:142.0
1,2-Dibromo-3-chloropropane ug/kg ND 5.0 09/21/19 12:142.5
1,2-Dibromoethane (EDB)ug/kg ND 5.0 09/21/19 12:141.1
1,2-Dichlorobenzene ug/kg ND 5.0 09/21/19 12:141.8
1,2-Dichloroethane ug/kg ND 5.0 09/21/19 12:141.0
1,2-Dichloropropane ug/kg ND 5.0 09/21/19 12:141.9
1,3,5-Trimethylbenzene ug/kg ND 5.0 09/21/19 12:141.7
1,3-Dichlorobenzene ug/kg ND 5.0 09/21/19 12:141.8
1,3-Dichloropropane ug/kg ND 5.0 09/21/19 12:141.9
1,4-Dichlorobenzene ug/kg ND 5.0 09/21/19 12:141.7
2,2-Dichloropropane ug/kg ND 5.0 09/21/19 12:140.49
2-Butanone (MEK)ug/kg ND 100 09/21/19 12:1411.9
2-Chlorotoluene ug/kg ND 5.0 09/21/19 12:141.5
2-Hexanone ug/kg ND 50.0 09/21/19 12:145.2
4-Chlorotoluene ug/kg ND 5.0 09/21/19 12:141.5
4-Methyl-2-pentanone (MIBK)ug/kg ND 50.0 09/21/19 12:143.7
Acetone ug/kg ND 100 09/21/19 12:149.4
Benzene ug/kg ND 5.0 09/21/19 12:140.90
Bromobenzene ug/kg ND 5.0 09/21/19 12:141.4
Bromochloromethane ug/kg ND 5.0 09/21/19 12:141.2
Bromodichloromethane ug/kg ND 5.0 09/21/19 12:140.98
Bromoform ug/kg ND 5.0 09/21/19 12:142.4
Bromomethane ug/kg ND 10.0 v109/21/19 12:142.4
Carbon tetrachloride ug/kg ND 5.0 09/21/19 12:140.96
Chlorobenzene ug/kg ND 5.0 09/21/19 12:140.97
Chloroethane ug/kg ND 10.0 v109/21/19 12:142.1
Chloroform ug/kg ND 5.0 09/21/19 12:141.1
Chloromethane ug/kg ND 10.0 v109/21/19 12:143.3
cis-1,2-Dichloroethene ug/kg ND 5.0 09/21/19 12:140.87
cis-1,3-Dichloropropene ug/kg ND 5.0 09/21/19 12:142.3
Dibromochloromethane ug/kg ND 5.0 09/21/19 12:142.5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
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Page 27 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92445872
DCY-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2686540
Associated Lab Samples:92445872001, 92445872002, 92445872003, 92445872004, 92445872005
Matrix: Solid
AnalyzedMDL
Dibromomethane ug/kg ND 5.0 09/21/19 12:141.5
Dichlorodifluoromethane ug/kg ND 10.0 v109/21/19 12:144.1
Diisopropyl ether ug/kg ND 5.0 09/21/19 12:142.9
Ethylbenzene ug/kg ND 5.0 09/21/19 12:141.1
Hexachloro-1,3-butadiene ug/kg ND 5.0 09/21/19 12:142.5
Isopropylbenzene (Cumene)ug/kg ND 5.0 09/21/19 12:141.4
m&p-Xylene ug/kg ND 10.0 09/21/19 12:142.4
Methyl-tert-butyl ether ug/kg ND 5.0 09/21/19 12:142.9
Methylene Chloride ug/kg ND 20.0 09/21/19 12:145.9
n-Butylbenzene ug/kg ND 5.0 09/21/19 12:142.8
n-Propylbenzene ug/kg ND 5.0 09/21/19 12:141.7
Naphthalene ug/kg ND 5.0 09/21/19 12:144.2
o-Xylene ug/kg ND 5.0 09/21/19 12:141.2
p-Isopropyltoluene ug/kg ND 5.0 09/21/19 12:142.4
sec-Butylbenzene ug/kg ND 5.0 09/21/19 12:142.1
Styrene ug/kg ND 5.0 09/21/19 12:141.5
tert-Butylbenzene ug/kg ND 5.0 09/21/19 12:141.7
Tetrachloroethene ug/kg ND 5.0 09/21/19 12:141.6
Toluene ug/kg ND 5.0 09/21/19 12:141.6
trans-1,2-Dichloroethene ug/kg ND 5.0 09/21/19 12:140.98
trans-1,3-Dichloropropene ug/kg ND 5.0 09/21/19 12:140.88
Trichloroethene ug/kg ND 5.0 09/21/19 12:141.3
Trichlorofluoromethane ug/kg ND 5.0 v109/21/19 12:141.2
Vinyl acetate ug/kg ND 50.0 09/21/19 12:1416.3
Vinyl chloride ug/kg ND 10.0 v109/21/19 12:141.9
Xylene (Total)ug/kg ND 10.0 09/21/19 12:143.5
1,2-Dichloroethane-d4 (S)%93 70-132 09/21/19 12:14
4-Bromofluorobenzene (S)%104 70-130 09/21/19 12:14
Toluene-d8 (S)%105 70-130 09/21/19 12:14
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2686541LABORATORY CONTROL SAMPLE:
LCSSpike
1,1,1,2-Tetrachloroethane ug/kg 53.050 106 70-130
1,1,1-Trichloroethane ug/kg 57.250 114 70-130
1,1,2,2-Tetrachloroethane ug/kg 47.850 96 55-130
1,1,2-Trichloroethane ug/kg 52.950 106 70-130
1,1-Dichloroethane ug/kg 55.450 111 68-130
1,1-Dichloroethene ug/kg 59.850 120 70-130
1,1-Dichloropropene ug/kg 59.850 120 70-130
1,2,3-Trichlorobenzene ug/kg 49.650 99 70-130
1,2,3-Trichloropropane ug/kg 48.450 97 70-130
1,2,4-Trichlorobenzene ug/kg 48.050 96 70-130
1,2,4-Trimethylbenzene ug/kg 49.950 100 69-130
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
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Page 28 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92445872
DCY-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2686541LABORATORY CONTROL SAMPLE:
LCSSpike
1,2-Dibromo-3-chloropropane ug/kg 47.650 95 57-141
1,2-Dibromoethane (EDB)ug/kg 51.150 102 70-130
1,2-Dichlorobenzene ug/kg 48.750 97 70-130
1,2-Dichloroethane ug/kg 52.750 105 70-130
1,2-Dichloropropane ug/kg 55.350 111 70-130
1,3,5-Trimethylbenzene ug/kg 50.250 100 70-130
1,3-Dichlorobenzene ug/kg 49.150 98 70-130
1,3-Dichloropropane ug/kg 53.050 106 70-130
1,4-Dichlorobenzene ug/kg 48.850 98 70-130
2,2-Dichloropropane ug/kg 57.650 115 70-130
2-Butanone (MEK)ug/kg 115100 115 60-130
2-Chlorotoluene ug/kg 48.950 98 70-130
2-Hexanone ug/kg 97.6100 98 70-132
4-Chlorotoluene ug/kg 49.250 98 70-130
4-Methyl-2-pentanone (MIBK)ug/kg 99.4100 99 69-130
Acetone ug/kg 115100 115 49-148
Benzene ug/kg 56.650 113 70-130
Bromobenzene ug/kg 51.350 103 70-130
Bromochloromethane ug/kg 54.450 109 70-130
Bromodichloromethane ug/kg 53.950 108 70-130
Bromoform ug/kg 49.050 98 68-136
Bromomethane ug/kg 70.0 F3,v150140 60-140
Carbon tetrachloride ug/kg 53.150 106 70-130
Chlorobenzene ug/kg 49.850 100 70-130
Chloroethane ug/kg 68.6 v150137 51-147
Chloroform ug/kg 56.950 114 70-130
Chloromethane ug/kg 87.0 F3,L1,v150174 48-130
cis-1,2-Dichloroethene ug/kg 54.450 109 70-130
cis-1,3-Dichloropropene ug/kg 57.750 115 70-130
Dibromochloromethane ug/kg 50.550 101 70-130
Dibromomethane ug/kg 51.350 103 70-130
Dichlorodifluoromethane ug/kg 156 F3,IK,L1,v150311 49-130
Diisopropyl ether ug/kg 59.250 118 66-130
Ethylbenzene ug/kg 50.950 102 70-130
Hexachloro-1,3-butadiene ug/kg 47.550 95 70-130
Isopropylbenzene (Cumene)ug/kg 51.350 103 70-130
m&p-Xylene ug/kg 102100 102 70-130
Methyl-tert-butyl ether ug/kg 55.550 111 70-130
Methylene Chloride ug/kg 49.350 99 50-137
n-Butylbenzene ug/kg 47.750 95 70-130
n-Propylbenzene ug/kg 50.750 101 70-130
Naphthalene ug/kg 47.650 95 70-131
o-Xylene ug/kg 51.750 103 70-130
p-Isopropyltoluene ug/kg 50.350 101 70-130
sec-Butylbenzene ug/kg 52.050 104 70-130
Styrene ug/kg 50.050 100 70-130
tert-Butylbenzene ug/kg 45.550 91 69-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
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Huntersville, NC 28078
[phone]
Page 29 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92445872
DCY-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2686541LABORATORY CONTROL SAMPLE:
LCSSpike
Tetrachloroethene ug/kg 50.150 100 56-130
Toluene ug/kg 52.650 105 70-130
trans-1,2-Dichloroethene ug/kg 57.950 116 70-130
trans-1,3-Dichloropropene ug/kg 54.750 109 70-130
Trichloroethene ug/kg 57.650 115 70-141
Trichlorofluoromethane ug/kg 71.8 L1,v150144 67-130
Vinyl acetate ug/kg 149 L1100149 10-136
Vinyl chloride ug/kg 72.4 F3,L1,v150145 67-130
Xylene (Total)ug/kg 154150 103 70-130
1,2-Dichloroethane-d4 (S)%99 70-132
4-Bromofluorobenzene (S)%97 70-130
Toluene-d8 (S)%98 70-130
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2687239MATRIX SPIKE SAMPLE:
MSSpike
Result
92445872002
1,1,1,2-Tetrachloroethane ug/kg 20.422.4 91 52-133ND
1,1,1-Trichloroethane ug/kg 22.122.4 99 49-137ND
1,1,2,2-Tetrachloroethane ug/kg 19.922.4 89 39-150ND
1,1,2-Trichloroethane ug/kg 20.222.4 90 48-140ND
1,1-Dichloroethane ug/kg 22.422.4 100 46-135ND
1,1-Dichloroethene ug/kg 24.822.4 110 38-149ND
1,1-Dichloropropene ug/kg 21.622.4 96 41-140ND
1,2,3-Trichlorobenzene ug/kg 19.922.4 89 10-158ND
1,2,3-Trichloropropane ug/kg 21.822.4 97 33-157ND
1,2,4-Trichlorobenzene ug/kg 19.422.4 86 10-155ND
1,2,4-Trimethylbenzene ug/kg 22.022.4 89 24-154ND
1,2-Dibromo-3-chloropropane ug/kg 20.022.4 89 33-158ND
1,2-Dibromoethane (EDB)ug/kg 19.922.4 89 40-136ND
1,2-Dichlorobenzene ug/kg 19.822.4 88 27-146ND
1,2-Dichloroethane ug/kg 20.622.4 92 49-140ND
1,2-Dichloropropane ug/kg 20.722.4 92 44-143ND
1,3,5-Trimethylbenzene ug/kg 20.922.4 93 40-144ND
1,3-Dichlorobenzene ug/kg 20.022.4 89 33-140ND
1,3-Dichloropropane ug/kg 20.122.4 90 47-147ND
1,4-Dichlorobenzene ug/kg 19.822.4 88 35-139ND
2,2-Dichloropropane ug/kg 23.122.4 103 41-140ND
2-Butanone (MEK)ug/kg 33.9J44.9 76 10-181ND
2-Chlorotoluene ug/kg 19.622.4 88 38-147ND
2-Hexanone ug/kg 42.5J44.9 95 18-169ND
4-Chlorotoluene ug/kg 19.922.4 89 36-145ND
4-Methyl-2-pentanone (MIBK)ug/kg 41.5J44.9 92 16-175ND
Acetone ug/kg 39.5J44.9 88 10-200ND
Benzene ug/kg 22.822.4 102 46-136ND
Bromobenzene ug/kg 20.422.4 91 38-149ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 30 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92445872
DCY-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
MS
Result
% Rec
Limits Qualifiers% RecConc.
2687239MATRIX SPIKE SAMPLE:
MSSpike
Result
92445872002
Bromochloromethane ug/kg 20.722.4 92 44-142ND
Bromodichloromethane ug/kg 21.622.4 96 41-140ND
Bromoform ug/kg 19.822.4 88 34-145ND
Bromomethane ug/kg 26.822.4 120 14-162ND
Carbon tetrachloride ug/kg 22.222.4 99 44-141ND
Chlorobenzene ug/kg 20.522.4 91 39-141ND
Chloroethane ug/kg 25.422.4 113 10-182ND
Chloroform ug/kg 21.222.4 94 45-140ND
Chloromethane ug/kg 23.422.4 104 19-149ND
cis-1,2-Dichloroethene ug/kg 21.622.4 96 38-150ND
cis-1,3-Dichloropropene ug/kg 21.022.4 94 30-144ND
Dibromochloromethane ug/kg 19.222.4 86 36-145ND
Dibromomethane ug/kg 21.022.4 94 41-145ND
Dichlorodifluoromethane ug/kg 24.222.4 108 16-146ND
Diisopropyl ether ug/kg 21.122.4 94 41-143ND
Ethylbenzene ug/kg 22.722.4 90 35-1442.5J
Hexachloro-1,3-butadiene ug/kg 20.222.4 90 10-160ND
Isopropylbenzene (Cumene)ug/kg 21.522.4 96 30-152ND
m&p-Xylene ug/kg 49.344.9 91 33-1458.5J
Methyl-tert-butyl ether ug/kg 22.022.4 98 49-140ND
Methylene Chloride ug/kg ND22.4 21 10-174ND
n-Butylbenzene ug/kg 20.422.4 91 10-160ND
n-Propylbenzene ug/kg 21.122.4 94 24-159ND
Naphthalene ug/kg 20.222.4 90 10-171ND
o-Xylene ug/kg 23.522.4 90 31-1503.2J
p-Isopropyltoluene ug/kg 20.322.4 91 21-154ND
sec-Butylbenzene ug/kg 21.422.4 96 19-159ND
Styrene ug/kg 20.322.4 91 15-152ND
tert-Butylbenzene ug/kg 18.422.4 82 31-141ND
Tetrachloroethene ug/kg 20.322.4 90 19-141ND
Toluene ug/kg 30.022.4 70 31-1464.2-
trans-1,2-Dichloroethene ug/kg 22.022.4 98 28-157ND
trans-1,3-Dichloropropene ug/kg 20.322.4 91 25-146ND
Trichloroethene ug/kg 21.422.4 95 34-149ND
Trichlorofluoromethane ug/kg 24.222.4 108 10-167ND
Vinyl acetate ug/kg 29.2J44.9 65 10-200ND
Vinyl chloride ug/kg 23.422.4 104 36-155ND
Xylene (Total)ug/kg 72.867.3 108 29-148ND
1,2-Dichloroethane-d4 (S)%104 70-132
4-Bromofluorobenzene (S)%101 70-130
Toluene-d8 (S)%101 70-130
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 31 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92445872
DCY-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92445872001
2687238SAMPLE DUPLICATE:
1,1,1,2-Tetrachloroethane ug/kg ND 30ND
1,1,1-Trichloroethane ug/kg ND 30ND
1,1,2,2-Tetrachloroethane ug/kg ND 30ND
1,1,2-Trichloroethane ug/kg ND 30ND
1,1-Dichloroethane ug/kg ND 30ND
1,1-Dichloroethene ug/kg ND 30ND
1,1-Dichloropropene ug/kg ND 30ND
1,2,3-Trichlorobenzene ug/kg ND 30ND
1,2,3-Trichloropropane ug/kg ND 30ND
1,2,4-Trichlorobenzene ug/kg ND 30ND
1,2,4-Trimethylbenzene ug/kg 2.6J 30ND
1,2-Dibromo-3-chloropropane ug/kg ND 30ND
1,2-Dibromoethane (EDB)ug/kg ND 30ND
1,2-Dichlorobenzene ug/kg ND 30ND
1,2-Dichloroethane ug/kg ND 30ND
1,2-Dichloropropane ug/kg ND 30ND
1,3,5-Trimethylbenzene ug/kg ND 30ND
1,3-Dichlorobenzene ug/kg ND 30ND
1,3-Dichloropropane ug/kg ND 30ND
1,4-Dichlorobenzene ug/kg ND 30ND
2,2-Dichloropropane ug/kg ND 30ND
2-Butanone (MEK)ug/kg ND 30ND
2-Chlorotoluene ug/kg ND 30ND
2-Hexanone ug/kg ND 30ND
4-Chlorotoluene ug/kg ND 30ND
4-Methyl-2-pentanone (MIBK)ug/kg ND 30ND
Acetone ug/kg ND 30ND
Benzene ug/kg ND 30ND
Bromobenzene ug/kg ND 30ND
Bromochloromethane ug/kg ND 30ND
Bromodichloromethane ug/kg ND 30ND
Bromoform ug/kg ND 30ND
Bromomethane ug/kg ND 30ND
Carbon tetrachloride ug/kg ND 30ND
Chlorobenzene ug/kg ND 30ND
Chloroethane ug/kg ND 30ND
Chloroform ug/kg ND 30ND
Chloromethane ug/kg ND 30ND
cis-1,2-Dichloroethene ug/kg ND 30ND
cis-1,3-Dichloropropene ug/kg ND 30ND
Dibromochloromethane ug/kg ND 30ND
Dibromomethane ug/kg ND 30ND
Dichlorodifluoromethane ug/kg ND 30ND
Diisopropyl ether ug/kg ND 30ND
Ethylbenzene ug/kg 1.6J 301.2J
Hexachloro-1,3-butadiene ug/kg ND 30ND
Isopropylbenzene (Cumene)ug/kg ND 30ND
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 32 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92445872
DCY-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92445872001
2687238SAMPLE DUPLICATE:
m&p-Xylene ug/kg 7.5J 303.9J
Methyl-tert-butyl ether ug/kg ND 30ND
Methylene Chloride ug/kg ND 30ND
n-Butylbenzene ug/kg ND 30ND
n-Propylbenzene ug/kg ND 30ND
Naphthalene ug/kg ND 30ND
o-Xylene ug/kg 2.5J 301.6J
p-Isopropyltoluene ug/kg ND 30ND
sec-Butylbenzene ug/kg ND 30ND
Styrene ug/kg ND 30ND
tert-Butylbenzene ug/kg ND 30ND
Tetrachloroethene ug/kg ND 30ND
Toluene ug/kg 9.5 D645306.0
trans-1,2-Dichloroethene ug/kg ND 30ND
trans-1,3-Dichloropropene ug/kg ND 30ND
Trichloroethene ug/kg ND 30ND
Trichlorofluoromethane ug/kg ND 30ND
Vinyl acetate ug/kg ND 30ND
Vinyl chloride ug/kg ND 30ND
Xylene (Total)ug/kg ND 30ND
1,2-Dichloroethane-d4 (S)%9595
4-Bromofluorobenzene (S)%103101
Toluene-d8 (S)%106108
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 33 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92445872
DCY-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
498143
EPA 3546
EPA 8270E
8270E Solid MSSV Microwave
Associated Lab Samples: 92445872001, 92445872002, 92445872003, 92445872004, 92445872005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2682038
Associated Lab Samples:92445872001, 92445872002, 92445872003, 92445872004, 92445872005
Matrix: Solid
AnalyzedMDL
1,2,4-Trichlorobenzene ug/kg ND 330 09/17/19 12:3675.6
1,2-Dichlorobenzene ug/kg ND 330 09/17/19 12:3671.4
1,3-Dichlorobenzene ug/kg ND 330 09/17/19 12:3674.3
1,4-Dichlorobenzene ug/kg ND 330 09/17/19 12:3672.6
1-Methylnaphthalene ug/kg ND 330 09/17/19 12:3687.9
2,2'-Oxybis(1-chloropropane)ug/kg ND 330 09/17/19 12:3691.7
2,4,5-Trichlorophenol ug/kg ND 330 09/17/19 12:3685.7
2,4,6-Trichlorophenol ug/kg ND 330 09/17/19 12:3682.9
2,4-Dichlorophenol ug/kg ND 330 09/17/19 12:36109
2,4-Dimethylphenol ug/kg ND 330 09/17/19 12:3682.2
2,4-Dinitrophenol ug/kg ND 1650 09/17/19 12:361050
2,4-Dinitrotoluene ug/kg ND 330 09/17/19 12:3687.4
2,6-Dinitrotoluene ug/kg ND 330 09/17/19 12:3686.3
2-Chloronaphthalene ug/kg ND 330 09/17/19 12:3673.5
2-Chlorophenol ug/kg ND 330 09/17/19 12:3676.8
2-Methylnaphthalene ug/kg ND 330 09/17/19 12:3684.0
2-Methylphenol(o-Cresol)ug/kg ND 330 09/17/19 12:3673.1
2-Nitroaniline ug/kg ND 1650 09/17/19 12:36166
2-Nitrophenol ug/kg ND 330 09/17/19 12:36102
3&4-Methylphenol(m&p Cresol)ug/kg ND 330 09/17/19 12:3683.0
3,3'-Dichlorobenzidine ug/kg ND 1650 09/17/19 12:36230
3-Nitroaniline ug/kg ND 1650 09/17/19 12:36175
4,6-Dinitro-2-methylphenol ug/kg ND 660 09/17/19 12:36532
4-Bromophenylphenyl ether ug/kg ND 330 09/17/19 12:3686.6
4-Chloro-3-methylphenol ug/kg ND 660 09/17/19 12:36201
4-Chloroaniline ug/kg ND 1650 09/17/19 12:36202
4-Chlorophenylphenyl ether ug/kg ND 330 09/17/19 12:3685.7
4-Nitroaniline ug/kg ND 660 09/17/19 12:36163
4-Nitrophenol ug/kg ND 1650 09/17/19 12:36526
Acenaphthene ug/kg ND 330 09/17/19 12:3684.9
Acenaphthylene ug/kg ND 330 09/17/19 12:3678.1
Aniline ug/kg ND 330 09/17/19 12:3674.1
Anthracene ug/kg ND 330 09/17/19 12:3685.6
Benzo(a)anthracene ug/kg ND 330 09/17/19 12:36105
Benzo(a)pyrene ug/kg ND 330 09/17/19 12:36143
Benzo(b)fluoranthene ug/kg ND 330 09/17/19 12:36133
Benzo(g,h,i)perylene ug/kg ND 330 09/17/19 12:36129
Benzo(k)fluoranthene ug/kg ND 330 09/17/19 12:36139
Benzoic Acid ug/kg ND 1650 09/17/19 12:36356
Benzyl alcohol ug/kg ND 660 09/17/19 12:36175
bis(2-Chloroethoxy)methane ug/kg ND 330 09/17/19 12:3688.1
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92445872
DCY-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: 2682038
Associated Lab Samples:92445872001, 92445872002, 92445872003, 92445872004, 92445872005
Matrix: Solid
AnalyzedMDL
bis(2-Chloroethyl) ether ug/kg ND 330 09/17/19 12:3670.1
bis(2-Ethylhexyl)phthalate ug/kg ND 330 09/17/19 12:36108
Butylbenzylphthalate ug/kg ND 330 09/17/19 12:3687.9
Chrysene ug/kg ND 330 09/17/19 12:3695.8
Di-n-butylphthalate ug/kg ND 330 09/17/19 12:3681.4
Di-n-octylphthalate ug/kg ND 330 09/17/19 12:36188
Dibenz(a,h)anthracene ug/kg ND 330 09/17/19 12:36132
Dibenzofuran ug/kg ND 330 09/17/19 12:3682.5
Diethylphthalate ug/kg ND 330 09/17/19 12:3671.6
Dimethylphthalate ug/kg ND 330 09/17/19 12:3674.6
Fluoranthene ug/kg ND 330 09/17/19 12:3699.7
Fluorene ug/kg ND 330 09/17/19 12:3688.3
Hexachloro-1,3-butadiene ug/kg ND 330 09/17/19 12:3680.2
Hexachlorobenzene ug/kg ND 330 09/17/19 12:3683.8
Hexachlorocyclopentadiene ug/kg ND 330 09/17/19 12:36132
Hexachloroethane ug/kg ND 330 09/17/19 12:3675.2
Indeno(1,2,3-cd)pyrene ug/kg ND 330 09/17/19 12:36151
Isophorone ug/kg ND 330 09/17/19 12:3671.7
N-Nitroso-di-n-propylamine ug/kg ND 330 09/17/19 12:3692.4
N-Nitrosodimethylamine ug/kg ND 330 09/17/19 12:3692.8
N-Nitrosodiphenylamine ug/kg ND 330 09/17/19 12:3684.2
Naphthalene ug/kg ND 330 09/17/19 12:3679.0
Nitrobenzene ug/kg ND 330 09/17/19 12:3678.8
Pentachlorophenol ug/kg ND 1650 09/17/19 12:36151
Phenanthrene ug/kg ND 330 09/17/19 12:3683.1
Phenol ug/kg ND 330 09/17/19 12:3678.8
Pyrene ug/kg ND 330 09/17/19 12:3690.8
Pyridine ug/kg ND 330 09/17/19 12:3683.5
2,4,6-Tribromophenol (S)%82 27-110 09/17/19 12:36
2-Fluorobiphenyl (S)%70 30-110 09/17/19 12:36
2-Fluorophenol (S)%67 13-110 09/17/19 12:36
Nitrobenzene-d5 (S)%73 23-110 09/17/19 12:36
Phenol-d6 (S)%75 22-110 09/17/19 12:36
Terphenyl-d14 (S)%98 28-110 09/17/19 12:36
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2682039LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2682040
1,2,4-Trichlorobenzene ug/kg 11901640 73 52-130751260 6 30
1,2-Dichlorobenzene ug/kg 11201640 68 51-130711190 6 30
1,3-Dichlorobenzene ug/kg 11201640 68 50-130711190 6 30
1,4-Dichlorobenzene ug/kg 11201640 68 49-130701180 6 30
1-Methylnaphthalene ug/kg 12401640 76 55-130791320 6 30
2,2'-Oxybis(1-chloropropane)ug/kg 15401640 94 30-130961610 4 30
REPORT OF LABORATORY ANALYSIS
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Page 35 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92445872
DCY-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2682039LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2682040
2,4,5-Trichlorophenol ug/kg 11901640 72 55-130761270 7 30
2,4,6-Trichlorophenol ug/kg 12201640 75 57-130781310 7 30
2,4-Dichlorophenol ug/kg 12601640 77 56-130801350 7 30
2,4-Dimethylphenol ug/kg 12901640 79 51-130821380 7 30
2,4-Dinitrophenol ug/kg 59208200 72 27-133786560 10 30
2,4-Dinitrotoluene ug/kg 12501640 77 61-130811360 8 30
2,6-Dinitrotoluene ug/kg 12801640 78 60-130841410 10 30
2-Chloronaphthalene ug/kg 11901640 72 52-130761270 7 30
2-Chlorophenol ug/kg 12201640 74 54-130771290 6 30
2-Methylnaphthalene ug/kg 12501640 76 54-130801340 7 30
2-Methylphenol(o-Cresol)ug/kg 11701640 71 51-130731220 5 30
2-Nitroaniline ug/kg 22503280 69 51-130742470 9 30
2-Nitrophenol ug/kg 13101640 80 49-130831390 6 30
3&4-Methylphenol(m&p Cresol)ug/kg 11801640 72 11-163751250 6 30
3,3'-Dichlorobenzidine ug/kg 23703280 72 10-132792660 12 30
3-Nitroaniline ug/kg 20803280 63 55-130692310 10 30
4,6-Dinitro-2-methylphenol ug/kg 28703280 88 47-142953190 10 30
4-Bromophenylphenyl ether ug/kg 13701640 84 59-130891500 9 30
4-Chloro-3-methylphenol ug/kg 24403280 74 55-130792650 8 30
4-Chloroaniline ug/kg 22703280 69 54-130732460 8 30
4-Chlorophenylphenyl ether ug/kg 12901640 79 58-130831390 7 30
4-Nitroaniline ug/kg 22403280 68 54-130752510 11 30
4-Nitrophenol ug/kg 54008200 66 48-130726010 11 30
Acenaphthene ug/kg 12301640 75 60-130791320 8 30
Acenaphthylene ug/kg 13401640 82 60-130871460 8 30
Aniline ug/kg 10701640 65 43-130671130 5 30
Anthracene ug/kg 13201640 81 63-130871460 10 30
Benzo(a)anthracene ug/kg 14101640 86 59-130941570 11 30
Benzo(a)pyrene ug/kg 14801640 90 57-130971630 10 30
Benzo(b)fluoranthene ug/kg 14301640 87 54-130921550 8 30
Benzo(g,h,i)perylene ug/kg 14901640 91 59-130981650 10 30
Benzo(k)fluoranthene ug/kg 14301640 87 54-130931560 8 30
Benzoic Acid ug/kg 47908200 58 19-130625210 8 30
Benzyl alcohol ug/kg 24203280 74 50-130762560 6 30
bis(2-Chloroethoxy)methane ug/kg 12401640 75 54-130791320 6 30
bis(2-Chloroethyl) ether ug/kg 12501640 76 48-130781310 5 30
bis(2-Ethylhexyl)phthalate ug/kg 14701640 90 45-134931560 6 30
Butylbenzylphthalate ug/kg 14801640 91 46-138951590 7 30
Chrysene ug/kg 13201640 80 58-130881470 11 30
Di-n-butylphthalate ug/kg 13601640 83 60-130881470 8 30
Di-n-octylphthalate ug/kg 17201640 105 53-1301111860 8 30
Dibenz(a,h)anthracene ug/kg 15001640 91 59-1301001670 11 30
Dibenzofuran ug/kg 12101640 74 60-130781300 7 30
Diethylphthalate ug/kg 12301640 75 60-130791330 8 30
Dimethylphthalate ug/kg 12401640 76 60-130801350 8 30
Fluoranthene ug/kg 14101640 86 65-130931570 11 30
Fluorene ug/kg 12701640 78 63-130831390 9 30
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.Date: 09/24/2019 04:27 PM
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Huntersville, NC 28078
[phone]
Page 36 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92445872
DCY-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
2682039LABORATORY CONTROL SAMPLE & LCSD:
LCSSpike LCSD
% Rec RPD
Max
RPD
LCSD
Result
2682040
Hexachloro-1,3-butadiene ug/kg 11701640 72 46-130741250 6 30
Hexachlorobenzene ug/kg 12701640 78 58-130831390 9 30
Hexachlorocyclopentadiene ug/kg 11701640 72 23-130721210 3 30
Hexachloroethane ug/kg 11301640 69 47-130711190 5 30
Indeno(1,2,3-cd)pyrene ug/kg 14901640 91 60-130991660 11 30
Isophorone ug/kg 12501640 76 49-130791330 6 30
N-Nitroso-di-n-propylamine ug/kg 12001640 73 47-130761270 6 30
N-Nitrosodimethylamine ug/kg 12701640 78 45-130791330 5 30
N-Nitrosodiphenylamine ug/kg 12901640 79 59-130851420 10 30
Naphthalene ug/kg 12301640 75 55-130781310 6 30
Nitrobenzene ug/kg 11801640 72 49-130751250 6 30
Pentachlorophenol ug/kg 24703280 75 10-132822760 11 30
Phenanthrene ug/kg 13601640 83 62-130901510 11 30
Phenol ug/kg 12301640 75 46-130781310 6 30
Pyrene ug/kg 14101640 86 53-130921550 9 30
Pyridine ug/kg 9901640 60 37-130631060 7 30
2,4,6-Tribromophenol (S)%89 27-11093
2-Fluorobiphenyl (S)%73 30-11075
2-Fluorophenol (S)%69 13-11071
Nitrobenzene-d5 (S)%75 23-11077
Phenol-d6 (S)%71 22-11073
Terphenyl-d14 (S)%88 28-11091
REPORT OF LABORATORY ANALYSIS
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[phone]
Page 37 of 44
#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92445872
DCY-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
498288
ASTM D2974-87
ASTM D2974-87
Dry Weight/Percent Moisture
Associated Lab Samples: 92445872001, 92445872002, 92445872003, 92445872004, 92445872005
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92445695001
2682690SAMPLE DUPLICATE:
Percent Moisture %12.5 0 2512.5
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92445902008
2682691SAMPLE DUPLICATE:
Percent Moisture %32.6 6 2534.8
REPORT OF LABORATORY ANALYSIS
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#=QC#
QUALITY CONTROL DATA
Pace Project No.:
Project:
92445872
DCY-001
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
QC Batch:
QC Batch Method:
Analysis Method:
Analysis Description:
1350512
SM 2540 G
SM 2540G
Total Solids 2540 G-2011
Associated Lab Samples: 92445872001, 92445872002, 92445872003, 92445872004, 92445872005
Parameter Units
Blank
Result
Reporting
Limit Qualifiers
METHOD BLANK: R3453876-1
Associated Lab Samples:92445872001, 92445872002, 92445872003, 92445872004, 92445872005
Matrix: Solid
AnalyzedMDL
Total Solids %0.00100 09/23/19 15:34
Parameter Units
LCS
Result
% Rec
Limits Qualifiers% RecConc.
R3453876-2LABORATORY CONTROL SAMPLE:
LCSSpike
Total Solids %50.050.0 100 85.0-115
Parameter Units
Dup
Result
Max
RPD QualifiersRPDResult
92445872001
R3453876-3SAMPLE DUPLICATE:
Total Solids %89.9 2.52 1087.7
REPORT OF LABORATORY ANALYSIS
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#=QL#
QUALIFIERS
Pace Project No.:
Project:
92445872
DCY-001
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision andbias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte isa combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean-Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPAMethod 8260.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
Pace Analytical NationalPAN
Pace Analytical Services - CharlottePASI-C
ANALYTE QUALIFIERS
The precision between the sample and sample duplicate exceeded laboratory control limits.D6
The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside thelaboratory's control limits. The result is estimated.F3
The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result shouldbe considered an estimated value.IK
Analyte detected below the reporting limit, therefore result is an estimate. This qualifier is also used for all TICs.J
Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associatedsamples may be biased high.L1
Matrix spike recovery and/or matrix spike duplicate recovery was above laboratory control limits. Result may be biasedhigh.MH
The analyte failed the method required serial dilution test and/or subsequent post-spike criteria. These failures indicatematrix interference.PH
The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in theassociated samples may have a high bias.v1
The continuing calibration verification was below the method acceptance limit. The analyte was not detected in theassociated samples and the sensitivity of the instrument was verified with a reporting limit check standard.v2
REPORT OF LABORATORY ANALYSIS
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#=CR#
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Project No.:
Project:
92445872
DCY-001
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
Analytical
Batch
92445872001 1349231 1349231P13051 EPA 6020B
92445872002 1349231 1349231P33051 EPA 6020B
92445872003 1349231 1349231P4A3051 EPA 6020B
92445872004 1349231 1349231P4B3051 EPA 6020B
92445872005 1349231 1349231P4C3051 EPA 6020B
92445872001 1348788 1348788P17471A EPA 7471B
92445872002 1348788 1348788P37471A EPA 7471B
92445872003 1348788 1348788P4A7471A EPA 7471B
92445872004 1348788 1348788P4B7471A EPA 7471B
92445872005 1348788 1348788P4C7471A EPA 7471B
92445872001 498143 498199P1EPA 3546 EPA 8270E
92445872002 498143 498199P3EPA 3546 EPA 8270E
92445872003 498143 498199P4AEPA 3546 EPA 8270E
92445872004 498143 498199P4BEPA 3546 EPA 8270E
92445872005 498143 498199P4CEPA 3546 EPA 8270E
92445872001 499141 499149P1EPA 5035A EPA 8260D
92445872002 499141 499149P3EPA 5035A EPA 8260D
92445872003 499141 499149P4AEPA 5035A EPA 8260D
92445872004 499141 499149P4BEPA 5035A EPA 8260D
92445872005 499141 499149P4CEPA 5035A EPA 8260D
92445872001 498288P1ASTM D2974-87
92445872002 498288P3ASTM D2974-87
92445872003 498288P4AASTM D2974-87
92445872004 498288P4BASTM D2974-87
92445872005 498288P4CASTM D2974-87
92445872001 1350512 1350512P1SM 2540 G SM 2540G
92445872002 1350512 1350512P3SM 2540 G SM 2540G
92445872003 1350512 1350512P4ASM 2540 G SM 2540G
92445872004 1350512 1350512P4BSM 2540 G SM 2540G
92445872005 1350512 1350512P4CSM 2540 G SM 2540G
REPORT OF LABORATORY ANALYSIS
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Page 42 of 44
Page 43 of 44
Page 44 of 44

Appendix C
Summary of Previous Brownfields Assessment Results
Table 1
Summary of Soil Analytical Data
Former Dicey Mills
Shelby, North Carolina
H&H Job No. DCY-001
Area of Concern
Sample ID HHSB-1 DUP-1
Date
Depth (ft bgs)
VOCs (8260) mg/kg ----BRL BRL
SVOCs (8270) mg/kg ----BRL BRL
Notes:
1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB)
Preliminary Soil Remediation Goals (PSRGs) (October 2017)
Soil concentrations are reported in milligrams per kilogram (mg/kg)
Laboratory analytical methods are shown in parentheses
VOCs = Volatile Organic Compounds; SVOCs = Semi-Volatile Organic Compounds
-- = not applicable; BRL = below laboratory reporting limit; ft bgs = feet below ground surface
Industrial/
Commercial
PSRGs (1)
(mg/kg)
Residential
PSRGs (1)
(mg/kg)10/10/2017
Screening Criteria Out-of-Use Fuel Oil UST
12-14
S:\AAA-Master Projects\Dicey Mills - DCY\Brownfields\Tables\Analytical Data Tables2/7/2018
Table 1 (Page 1 of 1)
Hart & Hickman, PC
Table 2
Summary of Groundwater Analytical DataFormer Dicey Mills
Shelby, North CarolinaH&H Job No. DCY-001
Area of Concern
Downgradient of
Former Dye House
Downgradient of Pond #3 Downgradient of Pond #4
Sample ID MW-1 DUP-3 MW-2 MW-3 MW-4 Trip Blank
Date 10/12/2017 10/12/2017 10/13/2017 10/12/2017 10/12/2017 10/12/2017
VOCs (8260) µg/L
Acetone 6,000 19,000,000 <50 <50 <50 <50 <50 8.3 JChloroform7035.5 0.28 J <2.0 1.3 J <2.0 0.85 J <2.01,4-Dichlorobenzene 6 113 <1.0 <1.0 <1.0 <1.0 <1.0 1.1Toluene 600 16,100 0.25 J 0.27 J 0.69 J <1.0 <1.0 <1.0Trichloroethylene34.35 7.6 9.5 <1.0 0.50 J 110 <1.0
SVOCs (8270) µg/L BRL BRL BRL BRL BRL
Metals (6020/7470/7471) µg/L
Antimony 1*NS <2.0 <2.0 0.20 J 0.21 J <2.0
Beryllium 4*NS 0.57 J 0.57 J 0.48 J <0.80 <0.80Cadmium2NS<1.0 <1.0 <1.0 <1.0 <1.0Chromium10NS1.5 J 1.3 J 3 1.2 J 1.3 JCopper1,000 NS 6.4 J 6.6 J 22 <10 <10Lead15NS0.84 J 0.83 J 5 <2.0 <2.0Manganese50NS18017099035110Mercury10.747 0.039 J 0.040 J 0.039 J 0.038 J 0.039 JNickel100NS1.2 J 3.6 J 3.6 J 1.2 J 1.6 JThallium0.2*NS <0.40 <0.40 0.21 J <0.40 <0.40Zinc1,000 NS 20 J 23 170 <20 <20
Turbidity (NTU)NA NA 8.10 3.77 8.48
Notes:1) North Carolina 15A NCAC 02L Groundwater Standards (2L Standards) (April 2013)2) North Carolina Department of Environmental Quality (DEQ) - Division of Waste Management (DWM)
Non-Residential Vapor Intrusion Groundwater Screening Levels (GWSLs) (October 2017)* = DEQ Interim Maximum Allowable Concentrations (IMACs) (if a 2L Standard is not specified)Concentrations are reported in micrograms per liter (µg/L)
Laboratory analytical methods are shown in parenthesesBold values exceed a 2L Standard (April 2013)Bold and underlined values exceed the Non-Residential GWSLsJ = estimated value between the laboratory detection limit and the laboratory reporting limitBRL = Below Reporting Limit; VOCs = Volatile Organic Compounds; SVOCs = Semi-Volatile Organic Compounds
-- = Not Applicable; NS = Not Specified; NTU = Nephelometric Turbidity Unit
North Carolina 2L
Groundwater
Standards (1)
West of Central Portion of
Former Manufacturing Building
Non-Residential
Vapor Intrusion
Groundwater
Screening
Levels (2)
8.09
S:\AAA-Master Projects\Dicey Mills - DCY\Brownfields\Tables\Analytical Data Tables2/7/2018
Table 2 (Page 1 of 1)
Hart & Hickman, PC
Table 3
Summary of Surface Water Analytical Data
Former Dicey Mills
Shelby, North Carolina
H&H Job No. DCY-001
Area of Concern
Downstream
Tributary
Sample ID SW-1 DUP-2 SW-2
Date 10/11/2017 10/11/2017 10/11/2017
VOCs (8260) µg/L BRL BRL BRL
SVOCs (8270) µg/LFluoranthene NS <0.46 0.056 J <0.48NaphthaleneNS0.11 J <1 <0.96PhenanthreneNS<0.046 0.074 <0.048PyreneNS<0.93 0.038 J <0.96
Metals (6020/7470/7471/7196) µg/L
Antimony NS 0.28 J 0.30 J 0.24 JChromium183.07 1.4 J 1.4 J 1.0 JCopper3.64 1.6 J 1.5 J 0.84 JIronNS330250280Lead13.88 0.55 J 0.53 J 0.28 JManganeseNS27298.8Mercury0.012 0.039 J 0.042 J 0.039 JNickel250.93 J 0.93 J <10
Notes:
1) North Carolina 15A NCAC 02B Surface Water Quality Standards for Class C Surface Waters using the most stringent of Freshwater and Human Health criteria (September 2017)
VOCs = Volatile Organic Compounds; SVOCs = Semi-Volatile Organic CompoundsConcentrations are reported in micrograms per liter (µg/L)
Laboratory analytical methods are shown in parenthesesJ = estimated value between the laboratory detection limit and the laboratory reporting limit
NS = Not Specified; BRL = below reporting limit
North Carolina 2B
Surface Water
Standards (1)
Upstream Tributary
S:\AAA-Master Projects\Dicey Mills - DCY\Brownfields\Tables\Analytical Data Tables2/7/2018
Table 3 (Page 1 of 1)
Hart & Hickman, PC
Table 4
Summary of Well Construction and Groundwater Elevation Data
Former Dicey Mills
Shelby, North Carolina
H&H Job No. DCY-001
MW-1 10/10/2017 Shallow 100.00 47 2 37 - 47 40.10 59.90
MW-2 10/11/2017 Shallow 103.19 48 2 38 - 48 42.05 61.14
MW-3 10/10/2017 Shallow 76.12 28 2 18 - 28 22.72 53.40
MW-4 10/10/2017 Shallow 69.00 30 2 20 - 30 24.48 44.52
Notes:
MW = permanent monitoring well; TOC = top of casing; ft = feet
Depth to groundwater measurements collected on 10/12/2017
*Elevations are approximate and are referenced to an arbitrary datum of 100.00 ft at MW-1
Groundwater
Elevation*Well ID Date Installed
Total Well
Depth (ft below
TOC)
Well Diameter
(inches)
Screen Interval
(ft)
Static Depth to
Water (ft below
TOC)
Screened Zone TOC Elevation
(ft)
S:\AAA-Master Projects\Dicey Mills - DCY\Brownfields\Tables\Analytical Data Tables
2/7/2018
Table 4 (Page 1 of 1)
Hart & Hickman, PC
Table 5
Summary of Groundwater and Surface Water Geochemical Data
Former Dicey Mills
Shelby, North Carolina
H&H Job No. DCY-001
Sample ID MW-1 MW-2 MW-3 MW-4 SW-1*SW-2*
Sample Date 10/12/2017 10/13/2017 10/12/2017 10/12/2017 10/11/2017 10/11/2017
Parameter
pH (SU)4.66 5.67 5.36 5.66 6.34 6.97Temperature (°C)19.7 19.3 20.4 20.3 22.3 23.8
Specific Conductivity (mS/cm)0.066 0.163 0.103 0.100 0.168 0.164
Dissolved Oxygen (mg/L) 6.66 4.19 2.18 5.30 4.64 5.45
Oxidation Reduction Potential (mV)190.4 94.2 116.7 137.2 125.6 159.9Turbidity (NTU)8.09 8.10 3.77 8.48 26.8 5.25
Notes:
mg/L = milligrams per liter
mS/cm = milisiemens per centimeter; SU = standard units
mV = millivolts; NTU = nephelometric turbidity units
*Sample collected from the unnamed tributary of the First Broad River
S:\AAA-Master Projects\Dicey Mills - DCY\Brownfields\Tables\Analytical Data Tables
2/7/2018
Table 5 (Page 1 of 1)
Hart & Hickman, PC
I
N
T
E
RM
I
T
T
E
N
T

S
T
R
E
AM
HHSB-1
SW-1
SW-2
MW-1
MW-2
MW-3
MW-4
LEGEND
SITE PROPERTY BOUNDARY
HIGH-TENSION POWER LINES
ABOVEGROUND STORAGE TANK
UNDERGROUND STORAGE TANK
SOIL BORING LOCATION
TYPE II MONITORING WELL
LOCATION
SURFACE WATER SAMPLE
LOCATION JOB NO. DCY-001
REVISION NO. 0DATE: 12-11-17
FIGURE NO. 2
FORMER DICEY MILLS
430 NEISLER STREET
SHELBY, NORTH CAROLINA
SAMPLE LOCATION MAPW.
D
I
XO
N

B
OU
L
E
V
A
RD
NEISLER STREETMELODY LANEFIRST BROAD RIVER2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
POND #3: FORMER
PROCESS WATER
POND #2: FORMER PROCESS WATER
POND #1: FORMER PROCESS WATER
FORMER FRESHWATER POND
POND HOUSE
FORMER FABRIC
PRINTING OPERATION
FORMER SETTLING PIT FOR
FRESHWATER INTAKE
PUMP HOUSE
POND 4: FORMER PROCESS WATER OUT-OF-USE VARSOL AST
VACANT STORAGE BUILDING
OUTFALL PIPE
FORMER MAINTENANCE SHOP
FORMER DYEHOUSE
FORMER FUEL OIL
UST & GASOLINE UST
OUT-OF-USE
FUEL OIL AST
FORMER WEAVING/SPINNING OPERATION
AIR COMPRESSORS W/
OBSERVED STAINING
AIR COMPRESSORS W/
OBSERVED STAINING
WASTE OIL AST
FORMER MANUFACTURING BUILDING
TRANSFORMER SUBSTATION
OUT-OF-USE FUEL OIL UST
S:\AAA-Master Projects\Dicey Mills - DCY\Phase II ESA\Figures\Figures.dwg, FIG 2, 12/11/2017 4:22:40 PM, zbarlow
I
N
T
E
RM
I
T
T
E
N
T

S
T
R
E
AM
MW-1
MW-2
MW-3
MW-4
(59.90)
(53.40)
(44.52)45505560(61.14)
LEGEND
SITE PROPERTY BOUNDARY
TYPE II MONITORING WELL LOCATION
GROUNDWATER ELEVATION (FT)
GROUNDWATER ELEVATION CONTOUR
(FT)
INFERRED GROUNDWATER FLOW
DIRECTION
JOB NO. DCY-001
REVISION NO. 0DATE: 12-11-17
FIGURE NO. 3
FORMER DICEY MILLS
430 NEISLER STREET
SHELBY, NORTH CAROLINA
GROUNDWATER ELEVATION CONTOUR MAPW.
D
I
XO
N

B
OU
L
E
V
A
RD
NEISLER STREETMELODY LANEFIRST BROAD RIVER2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
NOTE:
ELEVATIONS ARE APPROXIMATE & BASED ON AN ARBITRARY
DATUM OF 100.00 FT AT MW-1.
(59.90)
45
S:\AAA-Master Projects\Dicey Mills - DCY\Phase II ESA\Figures\Figures.dwg, FIG 3, 12/11/2017 10:56:19 AM, zbarlow
Table 1 Summary of Surface Water Analytical ResultsDicey Mills, Inc.430 Neisler StreetShelby, North CarolinaH&H Job No. DCY-001LocationOutfall Downstream UpstreamSample IDSW-1 SW-3 BKG-1Date6/14/2019 6/14/2019 6/14/2019Acute (3)Chronic (3)VOCs (8260) (µg/L)NDNDNDNDND------SVOCs (8270) (µg/L)NDNDNDNDND-- ----HSL Metals (6020/7471) (µg/L)Antimony<0.93 <0.93 <0.93 <0.93 <0.93NENE 640Arsenic<0.34 <0.34 <0.34 <0.34 <0.34340150 --Beryllium<0.30 <0.30 <0.30 <0.30 <0.30656.5 --Cadmium<0.22 <0.22 <0.22 <0.22 <0.220.640.12 --Chromium<0.90 <0.90 <0.90 <0.90 <0.90146.2219.02 --Copper<4.7 <4.7 <4.7 <4.7 <4.72.812.17 --Lead<0.44 <0.44 <0.44 <0.44 <0.4410.180.40 --Manganese 11 10 10<3.8 <3.8NENE 100Mercury<0.20 <0.20 <0.20 <0.20 <0.200.0120.012 --Nickel<0.83 <0.83 <0.83 <0.83 <0.83114.8912.76 --Selenium<0.98 <0.98 <0.98 <0.98 <0.9855--Silver<0.34 <0.34 <0.34 <0.34 <0.340.180.06 --Thallium<0.84 <0.84 <0.84 <0.84 <0.842 (4)2 (4) --Zinc<1020 22 21 20 28.6928.93 --pH (SM4500) 5.75.75.85.75.6--pH (Field Measured) (5)6.26.05.9--Total Hardness (200.7) (mg/L)2019191919--Notes:1) North Carolina 15A NCAC 2B Water Quality Standards (2B Standards) for Class C Surface Waters (June 2019) 2) Class C 2B Standard not established; U.S. EPA National Recommended Water Quality Criteria for Aquatic Life & Human Health3) 2B Standards calculated using the NCDEQ Hardness-Dependent Metal Calculator dated June 10, 2019 using Site-specific hardness value average4) Class C 2B Standard not established; NC In-Stream Target Values for Surface Waters5) pH was measured in the field at each sample location using a calibrated YSI Pro Plus MeterpH concentrations are presented in pH Standard UnitsBold indicates exceedance of 2B Standard, or EPA NRWQC if no 2B Standard, and background for pHµg/L = micrograms per liter VOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; HSL = Hazardous Substance ListNE = not established; ND = not detected; -- = not applicableSamples were collected from an unnamed tributary to the First Broad River, a Class C surface water bodyNon-detect values are reported to the laboratory method detection limit6.0 - 9.0EPA NRWQC (2)Screening Criteria100SW-2 / DUP-16/14/2019Endpoint of Observed Sediment 2B Standards (1)6.3S:\AAA-Master Projects\Dicey Mills - DCY\Pond Closure\Sediment Release\Analytical Data Tables7/16/2019Table 1 (Page 1 of 1)Hart & Hickman, PC
Table 2Summary of Sediment Analytical ResultsDicey Mills, Inc.430 Neisler StreetShelby, North CarolinaH&H Job No. DCY-001LocationStream - Sediment Flow Path OutfallStream - MidstreamStream - BackgroundSample IDSED-1SED-3SED-4 SOURCE BKG-1Date6/14/20196/14/2019 6/14/2019 6/14/2019 6/14/2019Depth* (ft bgs)0 - 0.50 - 0.50 - 0.50 - 0.50 - 0.5VOCs (8260) (mg/kg)Acetone<0.00150.028<0.0016 <0.00120.055 0.27<0.00142512,000 140,000-- --4-Isopropyl toluene<0.0013 <0.0013 <0.0016 <0.0012200.017<0.00141.24NE NE-- --Methyl Ethyl Ketone (2-Butanone)<0.0012 <0.0012 <0.0015 <0.0011 <0.00140.20<0.0013175,500 40,000-- --SVOCs (8270) (mg/kg)m- & p- Cresol (3/4-Methylphenol)<0.17 <0.17 <0.19 <0.18 <0.191.3<0.180.64(3)630(3)8,200(3)----HSL Metals (6020/7471) (mg/kg)Antimony<0.44 <0.44 <0.48 <0.45 <0.47 <0.56 <0.460.96.3 93<1.0 - 8.8 0.76Arsenic3.6 4.7 3.5 4.1 4.8 6.6 4.5 5.80.68 31.0 - 18 4.8Beryllium<0.15 <0.15 <0.16 <0.151.2 1.1<0.166331 470ND - 2.0 0.11Cadmium<0.12 <0.12 <0.13 <0.12 <0.13 <0.15 <0.12314 2001.0 - 10 4.3Chromium (Total)18 55 10 9.1 36 26.0 83.0 3.80.31 6.57.0 - 300 65Copper<0.618.5 7.2 3.1 9.2 7.2 6.3 700630 9,3003.0 - 100 34Lead4.5 5.6 4.3 4.6 16 25 5.6 270400 800ND - 50 50Manganese46 46 43 42 310 360 52 65380 5,6008.0 - 3,394 594Mercury<0.0855 <0.0869 <0.0632 <0.07920.159 0.117<0.068812.3 100.03 - 0.52 0.121Nickel2.8 3.0 2.4 3.4 8.9 7.4 3.3 130310 4,700ND - 150 23Selenium2.1 1.2<0.35 <0.332.72.1<0.352.178 1,200<0.1 - 0.8 0.42Silver<0.14 <0.14 <0.16 <0.15 <0.15 <0.18 <0.153.478 1,200ND - 5.0 NEThallium<0.18 <0.18 <0.20 <0.620.68<0.23<0.190.280.162.3NENEZinc17131315150140191,2004,700 70,00025 - 12456Notes:1) North Carolina Department of Environmental Quality (DEQ) Inactive Hazardous Sites Branch (IHSB) Health Based Preliminary Soil Remediation Goals (PSRGs) (May 2019)2) North Carolina Published Background Metals from Elements in North American Soils (2nd Edition; Dragun, Chekiri)3) Value based on lower of m- cresol and p- cresol PSRGs * = VOCs were collected as grab samples from within the specified intervalBOLD indicates concentration exceeds the Protection of Groundwater PSRG and background for metalsUnderline indicates concentration exceeds the Residential PSRG and background for metalsItalicized indicates concentration exceeds the Industrial/Commercial PSRGs and background for metalsLaboratory analytical methods are shown in parenthesesVOCs = volatile organic compounds; SVOCs = semi-volatile organic compounds; HSL = Hazardous Substance ListNE = not established; ND = not detected; ft bgs = feet below ground surface; -- = not applicableNon-detect values are reported to the laboratory method detection limitNorth Carolina Published Background Metals(2)Range MeanResidential PSRGs Industrial/Commercial PSRGsScreening Criteria (1) Protection of Groundwater PSRGsSED-2 / DUP-16/14/20190 - 0.5Stream - EndpointInside Silt Fence - Sediment Flow PathS:\AAA-Master Projects\Dicey Mills - DCY\Pond Closure\Sediment Release\Analytical Data Tables7/16/2019Table 2 (Page 1 of 1)Hart & Hickman, PC
REVISION NO. 0
JOB NO. DCY-001
DATE: 7-12-19
FIGURE NO. 2
FORMER DICEY MILLS
430 NEISLER STREET
SHELBY, NORTH CAROLINA
SAMPLE LOCATION MAP
LEGEND
SITE PROPERTY BOUNDARY
PARCEL BOUNDARY
SURFACE WATER FEATURE
DISTURBANCE AREA (3.4 ACRES)
SEDIMENT SAMPLE LOCATION
SURFACE WATER SAMPLE LOCATION
2923 South Tryon Street-Suite 100Charlotte, North Carolina 28203704-586-0007(p) 704-586-0373(f)License # C-1269 / #C-245 Geology
POND 4
FRESHWATER
POND
POND 3
POND 2
POND 1
SPILLWAY
SPILLWAY FIRST BROAD RIVERUNNAMED TRIBUTARY NEISLER STREETKTC BROADCASTING
(1511 W. DIXON BOULEVARD)
DAYS INN
(1431 W. DIXON BOULEVARD)
NOTES:
1. AERIAL IMAGERY OBTAINED FROM CLEVELAND
COUNTY GIS (2018).
2. SAMPLES WERE COLLECTED BY H&H ON 6/14/19.
NEISLER STREET SOLAR
SOURCE
SW-2
SED-2
SW-3
SED-3
SW-1
SED-1
BKG-1
BKG-1
SED-4
S:\AAA-Master Projects\Dicey Mills - DCY\Pond Closure\Erosion & Sediment Control Plan\Figures\Site Map.dwg, FIG 2, 7/12/2019 10:47:59 AM, SVincentUNDEVELOPED
LAND
UNDEVELOPED
LAND
UNDEVELOPED
LAND
WAREHOUSE(439 NEISLER STREET)
NCDOT OFFICE(435 NEISLER STREET)