Loading...
HomeMy WebLinkAboutMO-9543_40975_CA_IAR_20180529_Initial Abatement Action ReportInitial Abatement Action Report Truck Parts Services Site Charlotte, North Carolina Geoscience Project No. CH16.0148.EV Prepared For: Cindy Lane Development, LLC 4601 Charlotte Park Drive, Suite 350 Charlotte, North Carolina 28217 May 29, 2018 Prepared By: GEoSCENCE GROUP 500 Clanton Road, Suite % Charlotte, North Carolina 28217 Phone (704) 525-2003 Facsimile (704) 525-2051 April 20, 2018 Consulting Engineers GEoSCIENCE GROUP North Carolina Department of Environmental Quality Division of Waste Management 610 East Center Avenue, Suite 301 Mooresville, North Carolina 28115 Attention: Underground Storage Tank Section Reference: Initial Abatement Action Report Truck Parts Services Site Charlotte, North Carolina Geoscience Project No. CH16.0148.EV Incident No. PENDING This Initial Abatement Action Report summarizes the removal of an underground storage tank (UST) that was formerly used to store heating oil for a former commercial building. Site Name: Truck Parts Services Site UST Owner/Operator: Unknown Consultant: Geoscience Group, hic. 500 Clanton Road, Suite K Charlotte, North Carolina 28217 (704)525-2003 Site Location: 5007 Statesville Road Charlotte, North Carolina 28269 Property Owner: Cindy Lane Development, LLC 4601 Charlotte Park Drive, Suite 350 Charlotte, North Carolina 28217 Laboratory: Prism Laboratories, Inc. 449 Springbrook Lane Charlotte, North Carolina 28224 (704)529-6364 Date Discovered: July 17, 2017 Latitude/Longitude: 35.2878760/-80.8369580 Quantity of Release: Unknown Cause of Release: Tank Corrosion Source of Release: UST System Contents/Size: Heating Oil, 550-gal. I, Thomas e;'ViVpka Professional Engineer for Geoscience Group, Inc., do certify that the inforrnntytiSjtis report is correct and accurate to the best of my knowledge. .• a .iaE.SS,._ •._ North 035050 Geoscience Group, Inc. is licensed to practice engineering in North Carolina. The certification number of the company is F-0585. Enclosures Pl.../EN 016/145-T aPmt S.A i UST/Cb RpAn Qarto ri -,o_.. a .._ V_. a -i!na IF 11"1one - „ ., NC: L'ice,nsc Sit K a21? F04fi5 Geoscience Project No. CH16.0148.EV April 20, 2018 Page 2 SITE HISTORFAND CHARACTERIZATION The subject property is a 2.8t acre tract located along the western side of Statesville Road approximately 370 feet south of its intersection with Cochrane Drive in Charlotte, North Carolina. The site is comprised of Mecklenburg County Tax Parcel ID Nos. 04115612 and 04115613. Until recently, the site was occupied by four (4) buildings and their associated outbuildings. The buildings included: a commercial building (5007-5009 Statesville Road) built in 1940 and occupied by Red Sea Grocery III and Nates Used Tire Shop; an office/warehouse built in 1920 and occupied by Truck Parts Service, Inc.; a duplex residence (5015-5017 Statesville Road) built in 1963; and a single-family residence (4927 Statesville Road) built in 1907. These former buildings were demolished just prior to our recent sampling activities. The former buildings are shown on Figure CH16.148-A in Appendix II. The installation and usage dates for the former storage tank (UST-1) are not known. As shown on the Site Layout Figure, No. CH16.148-A, UST-1 was located approximately six (6) feet west of the former commercial building (5007-5009 Statesville Road) on Parcel No. 04115613. No other USTs have been encountered on Parcel No. 04115613, and no other USTs are known to have been used at the parcel. However, two (2) gasoline USTs (5,000 gallon and 2,000 gallon) were removed from Parcel No. 04115612. The release associated with he former USTs at Parcel No. 04115612 is being assessed under the State Lead Program as Incident No. 19087 — Joe Mullis General Store. Based on review of the 1985 Geologic Map of North Carolina, the subject site is located within the Charlotte Belt of the Piedmont Physiographic Province. This Province is generally characterized by igneous intrusive and metamorphic bedrock that is Permian to Ordovician in age. The intrusive rock is typically overlain with a layer of soil and weathered rock, ranging in thickness from 0 to 150 feet. Bedrock within the Charlotte Belt consists primarily of the diorite -granite complex, with the granite appearing to be the predominant component of the complex. According to the Geologic Map, the subject site is underlain with granitic rock. According to the 1972 "Derita, North Carolina" United States Geological Survey (USGS) 7.5- minute quadrangle map (Figure CH16.148-B), the subject site is located between approximately 800 and 812 feet above mean sea level (MSL). The ground surface across the Project site generally slopes downward toward the north and northwest. The low elevation of 800 feet MSL is located at the northwestern property corner and the high elevation of 812 feet MSL is located on the southeastern portion of the site. CLOSURE PROCEDURES Geoscience was on site from February 12, 2018 through February 14, 2018 to monitor the removal of UST-1. EVO Corporation (EVO) was contracted to remove the tank and excavate contaminated soils encountered beneath the UST. Prior to excavation, a vacuum truck was used to remove residual fluids from the tank. Approximately 530 gallons Geoscience Project No. CHI6.0148.EV April 20, 2018 Page 3 Of water mixed with fuel oil were removed from UST-1. The product removed from the tank was transported to EVO's facility for proper disposal. A copy of the Certificate of Disposal for the product are included in Appendix V for your review. As shown in Photographs 1 through 4 in Appendix III, the clean overburden on top of the tank was removed and stockpiled on -site. The tank was then removed from the ground. As is visible in Photograph 5, the exterior of the UST-1 exhibited staining and obvious corrosion through holes. The tank was subsequently transported to EVO's facility for proper disposal. A copy of the Tank Disposal Certificate is included in Appendix V. UST-1 was approximately 95 inches long and 42 inches in diameter for an estimated capacity of 550 gallons. SITE INVESTIGATION Prior to the tank closure (July 2017), Geoscience mobilized to the site to monitor the advancement two (2) geoprobe soil borings (UST-1 and UST-2) adjacent to the UST. that was identified during the geophysics survey. These borings were each advanced to a depth of 20 feet BGS. The retrieved soil samples were screened with a photoionization detector (PID) for the presence of volatile organic compounds. The PID readings are summarized in the table below: PID Readings (ppm) Location Depth (ft BGS) 6 8 10 12 14 16 18 UST-1 207 164 115 109 105 100 13.6 UST-2 215 253 --- 186 168 152 57.9 One soil sample was selected for laboratory analysis from each boring location. The selected soil samples were placed in laboratory -provided containers, packed on ice, and transported in a cooler under appropriate chain -of custody procedures to Prism Laboratories, Inc. for chemical analysis. In accordance with UST Section protocols, the samples collected at UST-1 and UST-2 were analyzed for total petroleum hydrocarbons in the gasoline (TPH-GRO) and diesel ranges (TPH-DRO), as well as total lead and total chromium. TPH-DRO was detected in the samples from UST-1 and UST-2 at concentrations of 300 and 16,000 mg/kg, respectively. In addition, TPH-GRO was detected in sample UST-2 at a concentration of 860 mg/kg. These concentrations exceed the action levels of 100 mg/kg and 50 mg/kg established by the UST Section for TPH-DRO and TPH-GRO, respectively. In addition, Sample UST-2 exhibited slightly elevated levels of chromium and lead. Based on these results, it was apparent prior to removal of the tank that a release has occurred from UST-1. Geoscience Project No. CH16.0148.EV April 20, 2018 Page 4 Following the collection of the soil samples, boring UST-2 was completed as a one -inch diameter temporary monitoring well (TW-1) screened from 20 to 30 feet below the ground surface (BGS). TW-I was subsequently developed and purged in accordance with NCDEQ guidelines. One (1) groundwater sample was collected from the temporary monitoring well. The groundwater sample was placed in laboratory -provided containers, packed on ice, and transported in a cooler under appropriate chain -of custody procedures to Prism Laboratories, Inc. for chemical analysis. The sample was analyzed for VOCs and Semi-VOCs by Methods 8260 and 8270, as well as for volatile and extractable petroleum hydrocarbons by MADEP methods. The results of the groundwater sample analysis are listed on Table B-4: Summary of Groundwater Sampling Results (Appendix I). As shown, the following compounds were detected at concentrations exceeding North Carolina Groundwater (2L) Standards in the monitoring well: 1-methylnaphthalene; 2-methylnaphthalene; naphthalene; 1,2,4-trimethylbenzene; 1,3,5-himethylbenzene; benzene; ethylbenzene; xylenes; C9-C18 aliphatic compounds; and C9-C22 aromatic compounds. Based on these results, it was apparent that the release from UST-1 had impacted the groundwater beneath the tank basin. SOIL REMEDL9TION The UST -I tank basin was over -excavated laterally and vertically in an effort to remediate the impacted soils. The final excavation measured approximately thirty-eight (38) feet long, thirteen (13) feet wide, and thirteen (13) feet deep. The horizontal extent of the excavation was determined by screening the excavated soils with a photo -ionization detector. Excavation was terminated in the vertical direction upon reaching the full arm extension that the excavation equipment (mini -excavator) was able to achieve. The excavated soils were loaded directly onto trucks and transported to EVO's facility for proper disposal. A total of 52.45 tons of impacted soil were hauled off -site for treatment. Copies of the manifests and Certificate of Disposal for the impacted soil are included in Appendix V for your review. Upon completion of the soil removal, confirmatory soil samples (S-1 through S er -5) we obtained from the bottom and sidewalk of the UST-1 excavation. The soil samples were submitted to Prism under appropriate chain -of -custody for chemical analyses using EPA Method 8260 (volatile organics), EPA Method 8270 (semi -volatile organics), and MADEP VPH/EPH (aliphatic and aromatic hydrocarbons). The excavation was subsequently backfilled with compacted clean soil from an off -site location. The analytical results of the confirmatory soil samples are summarized in Table B-3 in Appendix I. As indicated on the table, C9-C22 aromatic and C9-CI8 aliphatic hydrocarbons were detected in sample S-1 (bottom) at concentrations exceeding their respective "residential" maximum soil contaminant concentrations (MSCCs). In addition, 1,2,4-trimethylbenzene, 4-isopropyltoluene, naphthalene, and C5-C8ahphafic compounds Geoscience Project No. CH16.0148.EV April 20, 2018 Page 5 exceeded their respective "soil to groundwater" MSCCs in sample S-1. Furthermore, C9-C22 aromatic compounds exceeded "soil to groundwater" MSCC in sample S-5. No other exceedances of applicable cleanup standards were encountered in the confirmation samples. Copies of the laboratory test reports are included in Appendix IV. POTENTIAL RECEPTORS Geoscience did not conduct a receptor survey as part of this assessment. However, the receptor survey conducted as part of the Joe Mullis General Store release (Incident No. 19087) identified at least two (2) water supply wells within 1,500 feet of the subject Property: WSW-1 at 5014 Statesville Road, and WSW-2 at 5001 Jane Avenue. These water supply wells were sampled at least 8 times between 2002 and 2014 as part of the ongoing monitoring of the Joe Mullis General Store release. The most recent sample data (August 8, 2014) reviewed by Geoscience indicated that no contaminant concentrations were detected in the water supply well samples at concentrations that exceed 2L Standards. Please note that the State Lead Program may have more recent groundwater quality information for these wells. CONCLUSIONS Geoscience has observed and documented the closure of a UST formerly located at 5007 Statesville Road in Charlotte, North Carolina. The tank was previously used to store heating oil and was approximately 550 gallons in capacity. The installation and usage dates of the tank are not known. Soil sampling conducted before and following removal of the UST confirm that the soils immediately beneath the tank have been impacted by a release of petroleum. Soils remain in place that exceed both the soil to groundwater and residential MSCCs. However, none of the detected compounds are present at concentrations that exceed their respective commercial/industrial MSCCs. A sample collected from a temporary monitoring well (TMW-I) installed adjacent to UST-1 Prior to its closure indicates that the groundwater beneath the UST-1 basin has been impacted by the release at concentrations that exceed 2L Standards. However, none of the detected contaminants exceeded their "Gross Contamination Level". Although the groundwater has been impacted, the closest water supply wells to the UST-1 release (WSW- 1 and WSW-2) have been sampled regularly in association with the ongoing assessment of the Joe Mullis General Store release (Incident No. 19087). The reported sample results suggest that the water supply wells have not been significantly impacted by petroleum contaminants. Geoscience Project No. CH16.0148.EV April 20, 2018 Page 6 Given that the closest water supply well is over 500 feet from the release, has not been impacted, and is being monitored on a regular basis by the State Lead program, Geoscience, on behalf of our client, requests that the heating oil release from UST-1 be classified a "Low Risk". We further request that the incident be closed pending the recordation of a Notice of Residual Petroleum approved by the UST Section. APPENDIXI Tables: Table B-l: Site History - UST/AST System and Other Release Information Table B-2: Site History - UST/AST Owner/Operator and Other Responsible Party Information Table B-3: Summary of Soil Sampling Results Table B-4: Summary of Groundwater Sampling Results ■& ■ E .. «§ )}� \§/ » ) 00 % (D .w.2 , -- !§tf k / « )Q\ k2 ) kk 07r � 0 IX Cc )[ f f� // \ I� E� aE 2 %»E( / / ;4= 0 - �}-- / E w ) #� EM CL ■— ) °zE 2 z§ /� CL - /\ )z ) §a o 2! %2 $ ; 7 ) \ k) ! _ fA a! 6 - �2 .- - ■§ z k�CD k� �� } }� k - �M � . �■ £2 2 : E E E ■( 2; 2 §f §/§ §_ §. < y ![ $/a .i±■ $ o& _ § /§ / %z �� �2 $« .$§ . 2 o . /2\ *gym 7 �§ m $ »� )2 ■`® ■_® ■ RCL �2 `/. 3» . �« ■a � .91 9 a7 ■w k Lz. —10 OzC` . S . co )\ s �E ) I) C< 0§ 3z E T>�62 7 $ \ Z� ° /}$0 » L) 3 u a u}E 61 $■ E .� 2 G £. Revision Date: March 5, 2018 Incident Number: Table B-3: Summary Of Soil Sampling Results Pending Site Name: Truck Parts Services Analytical Method 5g/k 3 550 8260 (mg/kg) 8270 (mg/kg) MADEP-VPH / EPH (mg/kg) (mg/kg) (mg/kg) Contaminants of Concern „ o 0 0 3 i4 a ¢ G c7 A O t .Y T o D D L m m m W 1j .a Q Date Sample Depth x x u E E o ? z �. ii ; >. T % N °o .c m Q o Sample ID w a. Qc 'c a E '' U A ❑ o X c c ° m "' Collected (R) F. r✓ H w Z w z U U a d, U U _d U N r N U UST-1 7/17/2017 15 <1.0 300 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA UST-2 7/17/2017 20 860 16,000 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA S-1 2/12/2018 13 NA NA <1.4 11 4.3 1.3 <071 1.5 0.90 9.7 1.8 1.6 1.1 1.01 20 31 <0.45 0.87 15 0.27J 88 3,300 23J 1,000 S-2 2/13/2018 11 NA NA 0.079 <0.0057 -0.0057 <0.0057 0.0058J 10.0057 <0.0057 <0.011 <0.0057 <0.0057 <U057 <0017 <0.45 <0.45 <0.45 <0.45 <0.45 <0.45 10.19 0.87J 14,0 <.5 S-3 2/13/2018 11 NA NA <0.061 <0.0061 <0.0061 <0.0061 <0.012 <0.0061 <0,0061 <0.012 <0.0061 <0.0061 <0.0061 <0.018 <0.43 <0.43 <0.43 <0.43 <0.43 <0.43 <0.18 8.83 <3.8 0,62J S-4 2/13/2018 11 NA NA 0,067 J <0.0068 <0.0068 <0.0068 0,0052 J 10,0068 <0.0068 <0.014 -0,0068 <0.0068 <0.0068 <0.020 <0.49 <0.49 0.62 <0.49 <0.49 <0.49 <0.21 1.2 J <4.3 <.7 S-5 2/13/2018 11 NA NA <0.a5 0.027 0.0035J 0.0037J <0.013 <0.0065 <0.0065 0.033 0.0031J <0,0065 0.0034J <0.019 <0.52 <0.52 <0.52 <0s2 <0.52 <0.52 11 227 <k 120 TPH-GRO/DRO Action Limit 50 100 -- -- --- -- ---- ---- ---- ---- ---- ---- ---- ---- ---- ---- ---- Soil-to-Groundwater MSCCs ---- ---- 24 8.5 8.3 0.12 0.4 4.9 1.7 0.16 4.3 1.7 3.3 4.6 0.004 3.6 120 47 0.16 56 68 540 # 31 Residential MSCCs ---- ---- 14,000 782 782 100 22 1,560 1,564 313 626 626 626 3,129 20 63 62,571 620 313 469 939 1,500 31,000 469 Industrial/Commercial MSCCs ---- ---- 360,000 20,440 20,440 4,000 1 570 40,000 40,880 8,176 16,350 1 16,350 1 16,350 81,760 100 1,635 1,635,200 16,400 8176 12,264 24,528 40,000 1 810,000 12,264 Notes: mg/kg : Milligram per kilogram NA : Not Analyzed J : Estimated Concentration Detected But Below Reporting Limit # : Health Based Level > 100% Revision Date: 11/9/2017 TableB-4: Summary of Groundwater Sampling Results Incident No.: PENDING Project Name: Truck Parts Services Analytical Method SVOCS by 8270 (µg/L) VOCs by 8260 (µg/L) EPH/VPH (pg/L) Contaminant of Concern c c C C c C y1 C c 41 C V -6W L L 4 N t W . 'C W H C W C p1 > W C C C N W L t n E n n c o c z a > X > G 0 , v 6. o o m' m u u u Well ID Date Depth to Water m t m w z H w o E c z m a u :. J, Collected (ft) `) ` u y ry N rl ti 7/20/2017 22.05 130 170 <7.1 64 280 440 35 15 21 2.4 95 24 150 1.5 J 810 16 29 90 12 4.2 120 2,880 2,360 TW-1 7/21/2017 22,05 100 130 111 70 330 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NC 2L Standard 1 30 30,000 6,000 6 400 400 25 6,000 1 600 70 Soo 100 6 70 70 500 70 70 400 700 200 Gross Contamination Level 1,000 12,500 1,700,000 NL 6,000 28,500 25,000 11,700 6,000,000 5,000 84,500 180 85,500 100,000 6,000 6,900 30,000 85,500 8,500 15,000 NL NL NL Notes: J - Detected At Concentration Below Reporting Limit, Result Is An Estimated Concentration NL - Not Listed NA - Not Analyzed Residential Vapor Intrusion Screening Levels Table dated October 2017. APPENDIX II Figures: Figure No. CH16.148-A - Site Layout Figure No. CH16.148-B - 1972 USGS Topographic Map Figure No. CH15.145-C - Sample Location Diagram UST-1 LDcatioll, SITE 2.88± ACRES 0 REVISED: ANP J ■ Jr H�Bh $^h',� /a 1 \ ,T' ! y� . j(1 Wf➢isms Memoi�h �+ ' Road I(aol. 3rd.Yo -'; V ; cRh -� J S teanik �waa - ` �� O �7{ Sch 5 PT j0 ti h u V 91 mChy �764 r' J �°� `� � �' . �i��'.� �• SITE . t Diltoix j ��a..t..'. ( - _ Twig, pp'{� �� �.•- 4'-�y._r. a � § a ,;'•Low Eaet 3FotiedalC V•.-"��-----• '•�" - `^^ - t ,(--` y Nevin Vocatlni �'. e*JiF vsTGB V -. _ \ Training CEnt.r 1 J ' .a �a6n f o3 r_Ch C� - � `_� _ .::. raz � 1 I� �V: � sr! :�i• •�••� aV` PO O 1 l e� is p Jam. DDisposal�.. Prince of Pearter,',_ .�'a+ : ant Ns Cb t � "'.,""�'-�� Y_ ��•N�aron.7iei8hfs - 1 t Y> _i ` � 1.r (•op�m-1-h , ���� C ;�� Rom•. �� / ommvttitY Gentle? Ii `7 a E hs s • �\-{/` -� .�(( w`ecce�i^tce1''''�'7lF._ ' , •�_�� j4� _ .I -/ "///� � � /% � i�`��►��: o +'Eilr Mali 9F�i�lij P .A � _ j, ��. a'�•� �1 � �\i���l, �� � I lr��y t bary 76i ,Nh r Rethl$hem a '' ✓ ,�i� C, u eeraf,Ly Pnrk / sy o•r 1�,. `Rr nve_` ` i�� �. A. —.t �— Tom... y/ �"� .�Atanda GEOSCIENCE GROUP, INC. CHARLOTTE, NORTH CAROLINA SCALE: I"= 2,000' APPROVED BY: DRAWN BY: USGS NDATE: March 2, 2018 REVISED: ANP TRUCK PARTS SERVICES SITE CHARLOTTE, NORTH CAROLINA 1972 USGS TOPOGRAPHIC MAP FIGURE NUMBER CH16.148-B L Statesville Road 00 � � o ti r-------------i m I v I I I 0 I I LL I I I I I I I 1; w O V w W � x m a U CUi� a � a � n e w 0 0 J v E 0 1P APPENDIX III Site Photographs qz Cr a rI LL"'V m APPENDIX IV Laboratory Reports Rsr L480ngi0PIE; MG Geoscience Group Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 NC Certification No. 402 Full -Service Analytical & NC Drinking Water Celt No. 37735 Environmental Solutions SC Certification No. 99012 Project: Truck Part Service Lab Submittal Date: 07/17/2017 Prism Work Order: 7070278 Case Narrative 07/31 /2017 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. a --.-I Angela D. Overcash VP Laboratory Services Data Qualifiers Key Reference V Reviewed By Terri W. Cole For Angela D. Overcash Project Manager CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken. D RPD value outside of the control limits. DM Sample diluted and RL increased due to the matrix. DO Surrogates diluted out. E Estimated concentration above the calibration range J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag). M Matrix spike outside of the control limits. MC Sample concentration too high for recovery evaluation. MI Matrix spike outside of the control limits. Matrix interference suspected. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529.6364 - Toll Free Number: 14001529.6364 - Fax: 704/525-0409 page 1 of 50 PAR I S M Full eervme Anagecal e �x. ueoanma Ec me Environmental aolutiona Sample Receipt Summary 07/31/2017 Prism Work Order: 7070278 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received UST-1 7070278-01 Solid 07/17/17 07/17/17 UST-2 7070278-02 Solid 07/17/17 07/17/17 Lift-1 7070278-03 Solid 07/17/17 07/17/17 Lift-2 7070278-04 Solid 07/17/17 07/17/17 GP-1 7070278-05 Solid 07/17/17 07/17/17 GP-2 7070278-06 Solid 07/17/17 07/17/17 GP-3 7070278-07 Solid 07/17/17 07/17/17 GP-4 7070278-08 Solid 07/17/17 07/17/17 Samples were received at 10.2 degrees C. See case narrative for further information. This report should not be reproduced, except in its entirety, without the written consent or Prism Laboratories, Inc. 449 apringbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1400/529.6364 - Fax: 704/5254409 Page 2 of 50 irrP R I S n Full Service Analytical 6 $,--'vtB+:"<' iEa�x� Summary of Detections 07/31/2017 Prism Work Order: 7070278 Prism ID Client ID Parameter Method Result Units 7070278-01 UST-1 Diesel Range Organics *8015C 300 m9ft dry 7070278-01 USTA Chromium •6010D 92 mg/kg dry 7070278-01 UST-1 Lead •601 OD 6.5 mg/kg dry 7070278-02 UST-2 Diesel Range Organics '8015C 16000 mg/kg dry 7070278-02 UST-2 Gasoline Range Organics •8015C 860 mg/kg dry 7070278-02 UST-2 Chromium •601 OD 250 DM mg/kg dry 7070278-02 UST-2 Lead •60101) 33 DM mg/kg dry 7070278-03 Lift-1 Hexavalent Chromium •7196A 1.4 mg/kg dry 7070278-03 Lift-1 Barium •60101) 41 mg/kg dry 7070278-03 Lift-1 Chromium •6010D 8.5 mg/kg dry 7070278-03 Lift-1 Lead *601 OD 5.0 mg/kg dry 7070278-03 Lift-1 Acetone 82608 0.016 1 mg/kg dry 7070278-04 Lift-2 Hexavalent Chromium •7196A 1.2 mg/kg dry 7070278-04 Lift-2 Arsenic '60101) 15 DM mg/kg dry 7070278-04 Lift-2 Barium •6010D 61 DM mg/kg dry 7070278-04 Lift-2 Chromium •6010D 110 DM mg/kg dry 7070278-04 Lift-2 Lead •6010D 5.9 DM mg/kg dry 7070278-04 Lift-2 Acetone 8260B 0.067 J mg/kg dry 7070278-05 GP-1 Hexavalent Chromium •7196A 0.82 mg/kg dry 7070278-05 GP-1 Barium •6010D 13 DM mg/kg dry 7070278-05 GP-1 Chromium '6010D 55 DM mi dry 7070278-05 GP-1 Lead •6010D 34 DM mg/kg dry 7070278-05 GP-1 Selenium •6010D 9.9 DM mg/kg dry 7070278-05 GP-1 Acetone 8260B 0.034 1 mg/kg dry 7070278-06 GP-2 Benzoic Acid 8270D 2.0 mg/kg dry 7070278-06 GP-2 Hexavalent Chromium •7196A 0.55 mg/kg dry 7070278-06 GP-2 Mercury •7471B 0.031 mg/kg dry 7070278-06 GP-2 Arsenic •6010D 0.35 mg/kg dry 7070278-06 GP-2 Barium '60101) 16 mg/kg dry 7070278-06 GP-2 Chromium •6010D 16 mg/kg dry 7070278-06 GP-2 Lead *6010D 7.3 mgft dry 7070278-06 GP-2 Selenium *60101) 2.0 mg/kg dry 7070278-07 GP-3 Hexavalent Chromium •7196A 1.3 mg/kg dry 7070278-07 GP-3 Mercury •7471B 0.087 mg/kg dry 7070278-07 GP-3 Barium •6010D 21 mg/kg dry 7070278-07 GP-3 Chromium •6010D 38 mg/kg dry 7070278-07 GP-3 Lead •6010D 6.5 mg/kg dry 7070278-07 GP-3 Selenium •6010D 2.7 mg/kg dry 7070278-07 GPJ Acetone 8260E 0.048 1 mg/kg dry 7070278-08 GP-4 Hexavalent Chromium *7196A 0.55 mg/kg dry 7070278-08 GP-4 Arsenic •60101) 0.77 mg/kg dry 7070278-08 GP-4 Barium •6010D 16 mg&g dry 7070278-08 GP-4 Chromium •6010D 9.0 mg/kg dry 7070278-08 GP-4 Lead •6010D 4.0 mg/kg dry This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7ONS29.6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 3 of 50 This report should not be reproduced, except in its entirety, without the written consent of Pdsm Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 20224-0643 Phone: 7041529.6364 - Toll Free Number: 14001529-6364 - Fax: 704/525-0409 Page 4 of 50 Pisnn r°i'Ser,meAnai„,ea,a Laboratory Report / Envronmental Solutions _._ 07/31/2017 Geoscience Group Project: Truck Part Service Client Sample ID: UST-1 Attn: Tom Hassett Prism Sample ID: 7070278-01 500-K Clanton Rd. Prism Work Order: 7070278 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/17/17 10:58 Time Submitted: 07117/17 15:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Diesel Range Organics by GCIFID Diesel Range Organics 300 mg/kg dry 49 19 5 '8015C 7/19/17 17:06 2RC P700258 Surrogate o-Terphenyl Gasoline Range Organics by GC/FID Recovery Control Limits 104 % 49-124 Gasoline Range Organics BRL mg/kg dry 6.7 1.0 50 '8015C 7124/17 20:32 ANG P7G0359 Surrogate Recovery Control Limits a,a,a-TdBuorotoluene 130 % 50-137 General Chemistry Parameters % Solids 71.6 % by 0.100 0.100 1 •SM2540 G 7118/17 14:30 JLB P7GD278 Weight Total Metals Chromium 92 mg/kg dry 0.35 0.058 1 •6010D 7/21117 19:16 JAB P7G0320 Lead 6.5 mg/kg dry 0.35 0.065 1 '6010D 7121/17 19:16 JAB P7G0320 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. "Is Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0643 Phone: 7041529.6364-Toll Free Number: 1-800/529-6364- Fax: 704/S25-0409 Page 5 Df 50 I, Y I S `v'n �1 Full Servl<e Analytical fl Envlronmentel aolutlons Laboratory Report 07/31/2017 Geoscience Group Project: Truck Part Service Client Sample ID: UST-2 Attn: Tom Hassett Prism Sample ID: 7070278-02 500-K Clanton Rd. Prism Work Order: 7070278 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/17/17 10:37 Time Submitted: 07/17/17 15:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/rime ID Diesel Range Organics by GC/FID Diesel Range Organics 16000 mg/kg dry $60 93 100 •8015C 7131/17 9:49 ZRC P7G0460 Surrogate Recovery Control Limits o-Terphenyl 0 % 49-124 DO Gasoline Range Organics by GC/FID Gasoline Range Organics 860 mg/kg dry 76 11 500 •8015C 7/24/17 21:28 ANG P7G0359 Surrogate Recovery Control Limits a,a,a-Tneuorotoluene 120 % 50-137 General Chemistry Parameters %Solids 67.4 %by 0.100 0.100 1 •SM2540G 7118/1714:30 JLB P7G0278 Weight Total Metals Chromium Lead 250 OM mg/kg dry 33 DM mg/kg dry 1.8 0.31 5 •6010D 1.8 0.34 5 •60118D 712511716:51 JAB P7G0320 7126/17 16:51 JAB P7G0320 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratones, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number: 1.8001529.6364 - Fax: 7041526-0409 Page 6 of 50 P R I SqM Full Service Analytical 8 aaoa�� ,Es, M ronmental Solutions Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Sample Matrix: Solid Laboratory Report 07/31/2017 Client Sample ID: Lift-1 Prism Sample ID: 7070278-03 Prism Work Order: 7070278 Time Collected: 07/17/17 10:33 Time Submitted: 07/17/17 15:45 Parameter Result Units Report MDL Diluton Method Analysis Analyst Batch Limit Factor Date rime ID General Chemistry Parameters %Solids 76.5 %by 0.100 0,100 1 •SM2540G 7118/1714:30 JLB P7G0278 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Tdchlorobenzene BRL mg/kg dry 0.43 0.067 1 8270D 7/20/17 15:06 JMV P7G0259 1,2-Dichlorobenzene BRL mg/kg dry 0.43 0.065 1 8270D 7/20/17 15:06 JMV P7G0259 1,3-Dichlorobenzene BRL mg/kg dry 0.43 0.061 1 8270D 7/20/17 15:06 JMV P7G0259 1,4-Dichlorobenzene BRL mg/kg dry 0.43 0.063 1 8270D 7/20/17 15:06 JMV P7G0259 1-Methylnaphthalene BRL mg/kg dry 0.43 0.083 1 8270D 7/20/17 15:06 JMV P7G0259 2,4,6-Tdchlorophenol BRL mg/kg dry 0.43 0.081 1 8270D 7/20117 15:06 JMV P7G0259 2,4-Dichlorophenol BRL mg/kg dry 0.43 0.083 1 8270D 7/20/17 15:06 JMV P7G0259 2,4-Dimelhylphenol BRL CCV mg/kg dry 0.43 0.066 1 8270D 7/20/17 15:06 JMV P7G0259 2,4-Dinitrophenol BRL mg/kg dry 0.43 0.060 1 8270D 7120/17 15:06 JMV P7G0259 2,4-Dinitrotoluene BRL mg/kg dry 0.43 0.052 1 8270D 7/20117 15:06 JMV P7G0259 2,6-Dinitrotoluene BRL mg/kg dry 0.43 0.057 1 8270D 7/20/17 15:06 JMV P7G0259 2-Chloronaphthalene BRL mg/kg dry 0.43 0.062 1 8270D 7/20/17 15:06 JMV P7130259 2-Chlorophenol BRL mg/kg dry 0.43 0.061 1 8270D 7120/17 15:06 JMV P7G0259 2-Methylnaphthalene BRL mgkg dry 0.43 0.069 1 8270D 7/20117 15:06 JMV P7G0259 2-Methylphenol BRL mg/kg dry 0.43 0.055 1 8270D 7120117 15:06 JMV P7130259 2-Nitrophenol BRL mg/kg dry 0.43 0.078 1 82700 7120/17 15:06 JMV P7G0259 3,T-Dichlombenzidine BRL mg/kg dry 0.43 0.085 1 8270D 7/20117 15:06 JMV P7G0259 3/4-Methylphenol BRL mg/kg dry 0.43 0.053 1 8270D 7/20/17 15:06 JMV P7G0259 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.43 0.065 1 82700 7120/17 15:06 JMV P7G0259 4-Bromophenyl phenyl ether BRL mg/kg dry 0.43 0.074 1 8270D 7/20117 15:06 JMV P7130259 4-Chloro-3-methylphenol BRL mg/kg dry 0.43 0.060 1 8270D 7/20117 15:06 JMV P7G0259 4-Chloroaniline BRL mg/kg dry 0.43 0.052 1 82700 7/20117 15:06 JMV P7G0259 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.43 0.056 1 8270D 7120/17 15:06 JMV P7G0259 4-Nitrophenol BRL mg/kg dry 0.43 0.066 1 8270D 7/20/17 15:06 JMV P7G0259 Acensphthene BRL rrl dry 0.43 0.059 1 8270D 7/20117 15:06 JMV P7G0259 Acenaphthylene BRL mg/kg dry 0.43 0.062 1 8270D 7/20/17 15:06 JMV P7G0259 Anthracene BRL mg/kg dry 0.43 0.069 1 8270D 7/20117 15:06 JMV P7G0259 Azobenzene BRL mg/kg dry 0.43 0.057 1 8270D 7/20/17 16:06 JMV P7G0259 Benzo(a)anthracene BRL mgkg dry 0.43 0.056 1 8270D 7120/17 15:06 JMV P7G0259 Benzo(a)pyrene BRL mg/kg dry 0.43 0.047 1 8270D 7120/17 15:06 JMV P7G0259 Benzo(b)fluoranthene BRL mgft dry 0.43 0.050 1 8270D 7/20/17 15:06 JMV P7G0259 Benzo(g,h,i)perylene BRL rl dry 0.43 0.047 1 8270D 7120/17 15:06 JMV P7G0259 Benzo(k)fluoranthene BRL mg/kg dry 0.43 0.057 1 8270D 7/20/17 15:06 JMV P7130259 Benzoic Acid BRL mg/kg dry 0.43 0.036 1 8270D 7120/17 15:06 JMV P7G0259 Senzyl alcohol BRL mg/kg dry 0.43 0.057 1 8270D 7120117 15:06 JMV P7G0259 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.43 0.075 1 8270D 7/20/17 15:06 JMV P7G0259 Bis(2-Chlomethyl)ether BRL mg/kg dry 0.43 0.061 1 8270D 7120/17 16:06 JMV P7G0259 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.43 0.074 1 8270D 7/20/17 15:06 JMV P7130259 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.43 0.064 1 82700 7120/17 15:06 JMV P7G0259 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboretodes, Inc. 449 Spdngbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: l-000/529-6364-Fax: 704/525-0409 Page7oT 50 PRISM I rEz,erviceAnalytical a nv�o.meliredavivro�s Laboratory Report 07/31/2017 Geoscience Group Project: Truck Part Service Client Sample ID: Lift-1 Attn: Tom Hassett Prism Sample ID: 7070278-03 500-K Clanton Rd. Prism Work Order: 7070278 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/17/17 10:33 Time Submitted: 07/17/17 15:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Ys Batch Limit Factor Daterrime ID Butyl benzyl phthalate BRL mg/kg dry 0.43 0.061 1 8270D 7/20/17 16:06 JMV P7G0259 Chrysene BRL mg/kg dry 0.43 0.054 1 8270D 7120/17 15:06 JMV P7130259 Dibenzo(a,h)anthracene BRL mg/kg dry 0.43 0.052 1 8270D 7/20/17 15:06 JMV P7130259 Dibenzofuran BRL mg/kg dry 0.43 0.066 1 8270D 7120/17 15:06 JMV P71210259 Diethyl phthalate BRL mg/kg dry 0.43 0.059 1 8270D 7/20/17 15:06 JMV P7130259 DimeOryl phthalate BRL militia dry 0.43 0.057 1 8270D 7/20/17 15:06 JMV P7G0259 Di-n-butyl phthalate BRL mg/kg dry 0.43 0.061 1 8270D 7/20/17 15:06 JMV P7130259 Di-n-octyl phthalate BRL mg/kg dry 0.43 0.053 1 8270D 7120117 15:06 JMV P7130259 Fluoranthene BRL mglkg dry 0.43 0.055 1 8270D 7/20117 15:06 JMV P7130259 Fluorene BRL mg/kg dry 0.43 0.062 1 8270D 7120/17 16:06 JMV P7G0259 Hexachlombenzene BRL mg/kg dry 0.43 0.068 1 8270D 7/20/17 15:06 JMV P7G0259 Hexachlorobutadiene BRL mg/kg dry 0.43 0.077 1 8270D 7/20117 15:06 JMV P7G0259 Hexachlomcyclopentadiene BRL mgft dry 0.43 0.077 1 8270D 7120/17 15:06 JMV P7130259 Hexachloroethane BRL mglkg dry 0.43 0.072 1 8270D 7/20/17 15:06 JMV P7G0259 Indeno(1,2,3-od)pyrene BRL mg/kg dry 0.43 0.049 1 8270D 7/20/17 15:06 JMV P7G0259 Isophorone BRL mg*g dry 0.43 0.058 1 8270D 7120/17 15:06 JMV P7G0259 Naphthalene BRL mg/kg dry 0.43 0.069 1 8270D 7/20/17 15:06 JMV P7130259 Nitrobenzene BRL mg/kg dry 0.43 0.061 1 8270D 7/20/17 15:06 JMV P7130259 N-Nitroso-di-n-propylamine BRL militia dry 0.43 0.068 1 8270D 7/20/17 15:06 JMV P7G0259 N-Nitrosodiphenylamine BRL mg/kg dry 0.43 0.066 1 8270D 7/20/17 15:06 JMV P7130259 Pentachlorophenol BRL mi dry 0.43 0.051 1 8270D 7120/17 15:06 JMV P7G0259 Phenanthrene BRL mg/kg dry 0.43 0.056 1 8270D 7/20117 15:06 JMV P7130259 Phenol BRL mg/kg dry 0.43 0.064 1 8270D 7/20117 15:06 JMV P7130259 Pyrene BRL militia dry 0.43 0.067 1 8270D 7/20/17 15:06 JMV P7G0259 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 90 % 39-132 2-Fluorobiphenyl 80 % 44-115 2-Fluorophenol 86 % 35-115 Nhmbenzene-d5 79 % 37-122 Phenol-05 84 % 34-121 Terphenyl-014 101 % 54-127 Total Metals Hexavalent Chromium 1.4 mg/Irg dry 0.52 0.17 1 M96A 7/24/17 10:00 BMS P700274 Mercury BRL mg/kg dry 0.027 0.0025 1 '7471B 7120117 11:32 JAB P7G0287 Arsenic BRL mg/kg dry 0.33 0.040 1 '6010D 7/24/17 14:38 JAB P7G0320 Barium 41 mglkg dry 0.66 0.096 1 -60100 7121117 19:59 JAB P700320 Cadmium BRL mg/kg dry 0.33 0.0088 1 '6010D 7/24/17 14:38 JAB P7G0320 Chromium 8.5 mg/kg dry 0.33 0.055 1 '6010D 7121117 19:59 JAB P7G0320 Lead 5.0 militia dry 0.33 0.061 1 '6010D 7121117 19:59 JAB P700320 Selenium BRL mg/kg dry 0.66 0.16 1 •6010D 7121/17 19:59 JAB P7G0320 Silver BRL mg/kg dry 0.33 0.0081 1 '6010D 7/21/17 19:59 JAB P7100320 Volatile Organic Compounds by GUMS This report should not be reproduced, except in its enOrety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704/529.6364 - Toll Free Number: 1.800/529-6364 - Fax: 704/525-0409 Page 8 of 50 P R i M I Fun -Service Analyocai a Laboratory Report t uaS Es,.c EOVitVnmental solutions 07/31/2017 Geoscience Group Project: Truck Part Service Client Sample ID: Lift-1 Attn:Tom Hassett Prism Sample ID: 7070278-03 500-K Clanton Rd. Prism Work Order: 7070278 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/17/17 10:33 Time Submitted: 07/17/17 15:45 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID 1,1.1,2-Tetmchloroethans BRL mg/kg dry 0.0029 0.00024 1 8260B 7/26117 13:26 ANG P7G0413 1,1,1-Tdchloroethane BRL mg/kg dry 0.0029 0.00014 1 8260B 7126/17 13:26 ANG P7G0413 1,1,2,2-Tetmchloroethane BRL mg/kg dry 0.0029 0.00020 1 8260B 7/26117 13:26 ANG P7G0413 1,1,2-Trichloroethane BRL mg/kg dry 0.0029 0.00026 1 8260B 7126/17 13:26 ANG P7G0413 1,1-Dichloroethane BRL mg/kg dry 0.0029 0.000081 1 8260B 7/26117 13:26 ANG P7G0413 1.1-Dichloroethylene BRL mg/kg dry 0.0029 0.00013 1 8260B 7/26117 13:26 ANG P7G0413 1,1-Dichloropropylene BRL mg/kg dry 0.0029 0.00016 1 8260B 7126117 13:26 ANG P7G0413 1,2,3-Tdchlorobenzene BRL mg/kg dry 0.0029 0.00017 1 8260B 7/26/17 13:26 ANG P7G0413 1,2,3-Trichloropropane BRL mg/kg dry 0.0029 0.00037 1 8260B 7/26/17 13:26 ANG P7G0413 1,24-Trichlorobenzene BRL mglkg dry 0.0029 0.00022 1 8260B 7126/17 13:26 ANG P7G0413 1,2,4THmethylbenzene BRL mg/kg dry 0.0029 0.00022 1 8260B 7/26117 13:26 ANG P7130413 1,2-Dibromoethane BRL mglkg dry 0.0029 0.00012 1 8260B 7/26/17 13:26 ANG P7G0413 1,2-Dichlombenzene BRL mg/kg dry 0.0029 0.00014 1 8260B 7126/17 13:26 ANG P7G0413 1,2-Dichioroethane BRL mg/kg dry 0.0029 0.00017 1 8260B 7/26/17 13:26 ANG P7130413 1,2-Dichloropropane BRL mg/kg dry 0.0029 0.00018 1 8260B 7126/17 13:26 ANG P7G0413 1,3,5-Tdmethylbenzene BRL mg/kg dry 0.0029 0.00022 1 8260B 7126/17 13:26 ANG P7G0413 1,3-Dichlombemene BRL mg/kg dry 0.0029 0.00019 1 8260B 7/26/17 13:26 ANG P7GD413 1,3-Dichloropropane BRL mg/kg dry 0.0029 0.00015 1 8260B 7/26/17 13:26 ANG P7GD413 1,4-Dichlorobenzene BRL mglkg dry 0.0029 0.00011 1 8260B 7/26117 13:26 ANG P7G0413 2,2-Dichloropropane BRL mg/kg dry 0.0029 0.00014 1 8260B 7126/17 13:26 ANG P7G0413 2-Chlorotoluene BRL mg/kg dry 0.0029 0.00015 1 8260B 7/26117 13:26 ANG P7G0413 4-Chlorotoluene BRL mg/kg dry 0.0029 0.00017 1 8260B 7126117 13:26 ANG P7G0413 4-Isopropyholuene BRL mg/kg dry 0.0029 0.00014 1 8260B 7/26/17 13:26 ANG P7G0413 Acetone 0.016 J mg/kg dry 0.029 0.00071 1 8260B 7126117 13:26 ANG P7430413 Benzene BRL mg/kg dry 0.0017 0.00017 1 8260B 7/26/17 13:26 ANG P7G0413 Bromobenzene BRL mg/kg dry 0.0029 0.00024 1 8260B 7126117 13:26 ANG P7G0413 Bromochloromethane BRL mg/kg dry 0.0029 0.00016 1 8260B 7/26117 13:26 ANG P7G0413 Bromodichloromethane BRL mg/kg dry 0.0029 0.00016 1 8260B 7/26117 13:26 ANG P7130413 Bromoform BRL mg/kg dry 0.0029 0,00033 1 8260B 7126/17 13:26 ANG P7G0413 Bromomethane BRL mg/kg dry 0.0058 0.00036 1 8260B 7126117 13:26 ANG P7G0413 Carbon Tetrachloride BRL mg/kg dry 0.0029 0.00014 1 8260B 7126117 13:26 ANG P7G0413 Chlombenzene BRL mg/kg dry 0.0029 0.00015 1 82608 7126/17 13:26 ANG P7G0413 Chlomethane BRL mglkg dry 0.0058 0.00024 1 8260B 7/26117 13:26 ANG P7G0413 Chloroform BRL mg/kg dry 0.0029 0.00021 1 8260B 7/26/17 13:26 ANG P7G0413 Chloromethane BRL mglkg dry 0.0029 0.00020 1 8260B 7126/17 13:26 ANG P7G0413 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0029 0.00012 1 8260B 7126117 13:26 ANG P7G0413 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0029 0.000098 1 8260B 7126117 13:26 ANG P7G0413 Dibromochloromethane BRL mg/kg dry 0.0029 0.00012 1 8260B 7/26/17 13:26 ANG P7G0413 Dichlorodi0uoromethane BRL mg/kg dry 0.0029 0.00013 1 8260B 7/26/17 13:26 ANG P7G0413 Ethylbenzene BRL mg/kg dry 0.0029 0.00011 1 8260B 7/26/17 13:26 ANG P7G0413 Isopropyl Ether BRL mglkg dry 0.0029 0.00012 1 9260B 7/26/17 13:26 ANG P7GD413 IsopropNbenzene (Cumene) BRL mglkg dry 0.0029 0.00017 1 8260B 7126/17 13:26 ANG P7G0413 m,µXylenes BRL mg/kg dry 0.0058 0.00027 1 8260B 7126/17 13:26 ANG P7G0413 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1.8001529-6364- Fax: 7041525-0409 1 Page 9of 50 r-i O I S I Fun-eervlee Analytical s PR Eavlmnmental Solutions R, Laboratory Report 07/31/2017 �QJfEgvNc' Geoscienre Group Project: Truck Part Service Client Sample ID: Lift-1 Attn: Tom Hassett Prism Sample ID: 7070278-03 500-K Clanton Rd. Prism Work Order. 7070278 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/17/17 10:33 Time Submitted: 07/1711715:45 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Mehyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.029 0.00026 1 8260B 7/26117 13:26 ANG P7GD413 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.058 0.00026 1 82608 7/26117 13:26 ANG P7130413 Methyl Isobutyl Ketone BRL mg/kg dry 0.029 0oD025 1 8260B 7/26/17 13:26 ANG P7GO413 Methylene Chloride BRL mg/kg dry 0.0D58 0.00016 1 8260B 726117 13:26 ANG P7G0413 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0058 0.000093 1 8260B 7126/17 13:26 ANG P7G0413 Naphthalene BRL ni dry 0.0058 0.000092 1 8260B 7126117 13:26 ANG P7130413 n-Butylbemene BRL mg/kg dry 0.0029 0.00015 1 8260B 7/26117 13:26 ANG P7430413 n-Propylbenzene BRL mg/kg dry 0.0029 0.00017 1 8260B 726/17 13:26 ANG P7G0413 o-Xylene BRL mg/kg dry 0.0029 0.00012 1 82608 7/26117 13:26 ANG P7130413 sec-Butylbenzene BRL mg/kg dry 0.0029 0.00014 1 8260B 7/26/17 13:26 ANG P7130413 Styrene BRL mg/kg dry 0.0029 0.00018 1 8260B 726117 13:26 ANG P7130413 tert-Butylbenzene BRL m9ft dry 0.0029 0.000098 1 8260B 726/17 13:26 ANG P7G0413 Tetrachlomethylene BRL mg/kg dry 0.0029 0.00014 1 8260B 726117 13:26 ANG P7G0413 Toluene BRL mg/kg dry 0.0029 0.00017 1 8260B 726117 13:26 ANG P7GD413 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0029 0,00017 1 8260B 726/17 13:26 ANG P7G0413 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0029 0.00015 1 8260B 7/26/17 13:26 ANG P7G0413 Trichloroethylene BRL mg/kg dry 0.0029 0.00019 1 8260B 7/26117 13:26 ANG P7130413 Tdchlorofluwamethane BRL mg/kg dry 0.0029 0.00019 1 8260B 726H7 13:26 ANG P7130413 Vinyl acetate BRL mg/kg dry 0.015 0.00D40 1 8260B 726/17 13:26 ANG P7130413 Vinyl chloride BRL mg/kg dry 0.0029 0.00014 1 8260B 726117 13:26 ANG P74310413 Xylenes, total BRL mg&g dry 0.0087 0.00054 1 8260B 726/17 13:26 ANG P7GD413 Surrogate Recovery Control Limits 4-Bromofluorobenzene 102 % 70.130 Dibromofluoromethane 103 % 84-123 Toluene-d8 95% 76.129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7OW529-6364 -Toll Free Number: 1-9001529.6364 - Fax: 70415254" Page 10 of 50 F R S M Fuu senlce Analy cal 8 Laboratory Report � u�Toe 5 He e�� mrAnemsl smurocc 07/31/2017 Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Sample Matrix: Solid Client Sample ID: Lift-2 Prism Sample ID: 7070278-04 Prism Work Order: 7070278 Time Collected: 07/17/17 10:26 Time Submitted: 07117/17 15:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Daterrime ID General Chemistry Parameters %Solids 69.2 %by 0.100 0.100 1 •SM2540G 711811714:30 JLB P700278 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.48 0.074 1 8270D 7120/17 15:28 JMV P7G0259 1,2-Dichlorobenzene BRL mg/kg dry 0.48 0.072 1 8270D 7120/17 15:28 JMV P7G0259 1,3-Dichlorobenzene BRL mg/kg dry 0.48 0.067 1 82701) 7/20/17 15:28 JMV P7G0259 1,4-Dichlorobenzene BRL mg/kg dry 0.48 0.070 1 8270D 7/20/17 15:28 JMV P7G0259 1-Methylnaphthalene BRL mg/kg dry 0.48 0.092 1 8270D 7120117 15:28 JMV P7G0259 2,4,6-Tnchlorophenol BRL mg/kg dry 0.48 0.089 1 8270D 7/20/17 15:28 JMV P7G0259 2,4-Dichlorophenol BRL mg/kg dry 0.48 0.092 1 8270D 7120117 15:28 JMV P7G0259 2,4-Dimethylphend BRL CCV mg/kg dry 0.48 0.073 1 8270D 7/20/17 15:28 JMV P7G0259 2,4-Dinitmphenol BRL mg/kg dry 0.48 0.067 1 8270D 7120/17 15:28 JMV P7G0259 2,4-Dinitrotoluene BRL mg/kg dry 0.48 0.058 1 8270D 7/20/17 15:28 JMV P7G0259 2,6-Dinkratoluene BRL mg/kg dry 0.48 0.063 1 8270D 7120/17 15:28 JMV P7G0259 2-Chloronaphthalene BRL mg/kg dry 0.48 0.069 1 8270D 7/20/17 15:28 JMV P7G0259 2-Chlorophenol BRL mg/kg dry 0.48 0.068 1 8270D 7/20/17 15:28 JMV P7G0259 2-Methylnaphthalene BRL mg/kg dry 0.48 0.076 1 8270D 7/20/17 15:28 JMV P7G0259 2-Methylphenol BRL mg/kg dry 0.48 0.061 1 8270D 7/20/17 15:28 JMV P7G0259 2-Nitrophenol BRL mg/kg dry 0.48 0.087 1 8270D 7/20/17 15:28 JMV P7G0259 3,3'-1)ichlorobemidine BRL mg/kg dry 0.48 0.094 1 8270D 7120/17 15:28 JMV P7G0259 3/4-Methylphenol BRL mg/kg dry 0.48 0,059 1 8270D 7/20/17 16:28 JMV P7G0259 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.48 0.072 1 8270D 7120/17 15:28 JMV P7G0259 4-Bromophenyl phenyl ether BRL mg/kg dry 0.48 0.082 1 8270D 7/20117 15:28 JMV P7G0259 4-Chloro-3-methylphenol BRL mg/kg dry 0.48 0.067 1 8270D 7/20/17 15:28 JMV P7G0259 4-Chlomaniline BRL mg/kg dry 0.48 0.057 1 8270D 7120/17 15:28 JMV P7G0259 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.48 0.062 1 82701) 7120/17 16:28 JMV P7G0259 4-Nitrophenol BRL mg/kg dry 0.48 0.074 1 8270D 7120117 15:28 JMV P7G0259 Acenaphthene BRL mg/kg dry 0.48 0.065 1 8270D 7/20/17 15:28 JMV P7G0259 Acenaphthylene BRL mg/kg dry 0.48 0.069 - 1 8270D 7/20/17 15:28 JMV P7G0259 Anthracene BRL mg/kg dry OAS 0.077 1 8270D 7/20117 15:28 JMV P7130259 Azobenzene BRL mg/kg dry 0.48 0.063 1 8270D 7/20/17 15:28 JMV P7G0259 Benzo(a)anthracene BRL mg/kg dry 0.48 0.062 1 8270D 7/20117 15:28 JMV P7(30259 Senzo(a)pyrone BRL mg/kg dry OAS 0.052 1 8270D 7120/17 15:28 JMV P7G0259 Benzo(b)fluoranthene BRL mg/kg dry 0.48 0.055 1 8270D 7/20/17 15:28 JMV P7G0259 Benzo(g,hJ)perylene BRL mgft dry 0.48 0,052 1 8270D 7120/17 15:28 JMV P7G0259 Benzo(k)fluoranthene BRL mg/kg dry 0.48 0.063 1 8270D 7/20117 16:28 JMV P7G0259 Benzoic Acid BRL mg/kg dry 0.48 0.040 1 8270D 7/20117 15:28 JMV P7G0259 Benzyl alcohol BRL mg/kg dry 0.48 0.063 1 82701) 7/20/17 15:28 JMV P7G0259 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.48 0.083 1 8270D 7/20117 15:28 JMV P7G0259 Bis(2-Chlormthyl)ether BRL mg/kg dry 0.48 0.067 1 8270D 7/20/17 15:28 JMV P7G0259 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.48 0.082 1 8270D 7120/17 15:28 JMV P7G0259 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.48 0.071 1 8270D 7/20/17 15:28 JMV P7G0259 This report should not be reproduced, except in its entirety, without the written consent of Pnsm Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364-Toll Free Number: 1-8001529-6i364- Fax: 704/526-0409 Page 11 of 50 PRISgM Full -Service Analytical Laboratory Report Endmnmemal Saluuous 07/31/2017 Geoscience Group Project: Truck Part Service Client Sample ID: Lift-2 Attn: Tom Hassett Prism Sample ID: 7070278-04 500-K Clanton Rd. Prism Work Order: 7070278 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/17/17 10:26 Time Submitted: 07/17/17 15:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Butyl beryl phthalate BRL mg/kg dry Chrysene BRL mg/kg dry Dibenzo(a,h)anthracene BRL mg/kg dry Diberofumn BRL mg/kg dry Diethyl phthalate BRL mg/kg dry Dimethyl phthalate BRL mg/kg dry Di-n-butyl phthalate BRL mg/kg dry Di-n-octyl phthalate BRL mg/kg dry Fluorenthene BRL mgft dry Fluorene BRL mi dry Hexachlorobenzene BRL mg/kg dry Hexachlorobutadiene BRL mg/kg dry Hexachlorocyclopentadiene BRL mi dry Hexachlomethane BRL mg/kg dry Indeno(1,2,3-cd)pyrene BRL mg/kg dry Isophorone BRL mg/kg dry Naphthalene BRL mg/kg dry Nitrobenzene BRL mg/kg dry N-Nitroso-di-n-propylamine BRL mglkg dry N-Nibosodiphenylamine BRL mi dry Pentachlorophenol BRL mg/kg dry Phenanthrene BRL mg/kg dry Phenol BRL mg/kg dry Pyrene BRL mg/kg dry Total Metals 0.48 0.068 1 8270D 7/20/17 15:28 JMV P7G0259 0.48 0.060 1 8270D 7/20117 15:28 JMV P7130259 0.48 0.058 1 8270D 7/20117 15:28 JMV P7130259 0.48 0.073 1 8270D 720/17 15:28 JMV P7G0259 0.48 0.066 1 8270D 7/20117 15:28 JMV P7130259 0.48 0.063 1 8270D 7120117 15:28 JMV P7G0259 0.48 0.068 1 8270D 7120117 15:28 JMV P7G0259 0.48 0.059 1 8270D 7/20/17 15:28 JMV P7G0259 0.48 0.061 1 8270D 7/20/17 15:28 JMV P7G0259 0.48 0.069 1 8270D 7/20/17 15:28 JMV P7G0259 0.48 0.076 1 8270D 7120/17 16:28 JMV P7G0259 0.48 0.086 1 8270D 7/20/17 15:28 JMV P7G0259 0.48 0.085 1 8270D 7120/17 15:28 JMV P7G0259 0.48 0.080 1 8270D 7/20/17 15:28 JMV P7130259 0.48 0.055 1 8270D 720/17 15:28 JMV P7G0259 0.48 0.065 1 8270D 7/20/17 15:28 JMV P7130259 OAS 0.077 1 8270D 7/20117 15:28 JMV P7G0259 0.48 0.068 1 8270D 7/20/17 15:28 JMV P7G0259 0.48 0.075 1 8270D 7/20/17 15:28 JMV P7G0259 0.48 0.073 1 8270D 720/17 15:28 JMV P7G0269 0.48 0.056 1 8270D 7/20/17 15:28 JMV P7G0259 0.48 0.062 1 8270D 7/20/17 15:28 JMV P7130259 0.48 0.070 1 8270D 720/171528 JMV P7130259 0.48 0.063 1 8270D 7/20/17 15:28 JMV P7G0259 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 83 % 39-132 2-Fluombiphenyl 71 % 44-115 2-Fluorophenol 73 % 35-115 Nmobenzeml 69 % 37-122 Phenol-d5 72 % 34-121 Terphenyl-04 94 % 54-127 Hexavalent Chromium 1.2 mg/kg dry 0.58 0.19 1 '7196A 724/17 10:00 BMS P700274 Mercury BRL mg/kg dry 0.029 0.0028 1 •7471B 7/20/17 11:37 JAB P7G0287 Arsenic 15 DM mg/kg dry 1.8 0.22 5 '6010D 725/17 17:00 JAB P7G0320 Badum 61 DM mg/kg dry 3.7 0.53 5 •601010, 726/17 14:08 JAB P7G0320 Cadmium BRL DM mg/kg dry 1.8 0.049 5 •6010D 726/17 14:08 JAB P7G0320 Chromium 110 OM mg/kg dry 1.8 0.31 5 '6010D 726117 14:08 JAB P700320 Lead 6.9 DM mg/kg dry 1.8 0.34 5 '60100 726/17 14:08 JAB P700320 Selenium BRL DM mg/kg dry 3.7 0.87 5 •6010D 7/26/17 14:08 JAB P7G0320 Silver BRL DM mg/kg dry 1.8 0.045 5 •6010D 7/26/17 14:08 JAB P7G0320 Volatile Organic Compounds by GC/MS This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 -Toll Free Number: 1-800/529-6364 - Fix: 704/525-0409 Page 12 of 50 P R I S Y I I rwi san'ica Anainmai s ueov..o ss vc Env ronmentai eoluuons Laboratory Report 07/31/2017 Geoscienoe Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Sample Matrix: Solid Client Sample ID: Lift-2 Prism Sample ID: 7070278-04 Prism Work Order: 7070278 Time Collected: 07/17/17 10:26 Time Submitted: 07/17/17 15:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Datefrime ID 11,1,2-Tetrachloroethane BRL mg/kg dry 0.0070 0.00058 1 8260B 7126117 13:53 ANG P7GO413 1,1,1-Trichloroethane BRL mg/kg dry 0.0070 0,00034 1 8260B 7126/17 13:53 ANG P7130413 1,1,2,2-Tetmchloroethane BRL mg/kg dry 0.0070 0.00048 1 8260B 7126117 13:53 ANG P7G0413 1,1,2-Tdchlorcethane BRL mg/kg dry 0.0070 0.00062 1 8260B 7126/17 13:53 ANG P7GO413 1,1-Dichloroethane BRL mg/kg dry 0.0070 0,00020 1 82608 7126117 13:53 ANG P7GO413 11-Dichloroethylene BRL mg/kg dry 0.0070 0.00031 1 8260B 7/26117 13:53 ANG P7GO413 1,1-Dichloropropylene BRL mg/kg dry 0.0070 0.00039 1 8260B 7/26/17 13:53 ANG P7GO413 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0070 0.00040 1 8260B 7/26/17 13:53 ANG P7GO413 1,2,3-Trichloropropane BRL mg/kg dry 0.0070 0.00090 1 8260B 7/26/17 13:53 ANG P7GO413 1,24-Trichlorobenzene BRL mg/kg dry 0.0070 0.00052 1 8260B 7/26/17 13:53 ANG P7GO413 1,2,4-Tdmethylbenzene BRL mg/kg dry 0.0070 0.00054 1 8260B 7126/17 13:53 ANG P7GO413 1,2-Dibromoethane BRL mg/kg dry 0.0070 0.00028 1 8260B 7/26/17 13:53 ANG P7GD413 1,2-Dichlorobenzene BRL mg/kg dry 0.0070 0.00033 1 8260B 7/26M7 13:53 ANG P7GO413 1,2-Dichloroethane BRL mg/kg dry 0.0070 0.00042 1 8260B 7/26/17 13:53 ANG P7GD413 1,2-Dichloropmpane BRL mg/kg dry 0.0070 0.00044 1 8260B 7126117 13:53 ANG P7G0413 1,3,5-Tdmethylbenzene BRL mg/kg dry 0.0070 0.00053 1 8260B 7/26117 13:53 ANG P7GO413 1,3-Dichlorobenzene BRL mg/kg dry 0.0070 0.00D47 1 8260B 7/26/17 13:53 ANG P7GO413 1,3-Dichlompropane BRL mg/kg dry 0.0070 0.00035 1 8260B 7126117 13:53 ANG P7G0413 1,4-Dichlorobenzene BRL mg/kg dry 0.0070 0.00028 1 8260B 7/26/17 13:53 ANG P7GD413 2,2-Dichloropropane BRL mg/kg dry 0.0070 0.00033 1 8260B 7/26117 13:53 ANG P7GO413 2-Chlorololuene BRL mg/kg dry 0.0070 0.00036 1 8260B 7/26117 13:53 ANG P7GO413 4-Chlorotoluene BRL mgft dry 0.0070 0.00042 1 8260B 7126/17 13:53 ANG P7G0413 4-Isopropyltoluene BRL mg/kg dry 0.0070 0.00034 1 8260B 7/26/17 13:53 ANG P7GO413 Acetone 0.067 J mi dry 0.070 0.0017 1 9260B 7126117 13:53 ANG P7GO413 Benzene BRL mg/kg dry 0.0042 0.00D41 1 8260B 7/26/17 13:53 ANG P7GO413 Bromobenzene BRL mg/kg dry 0.0070 0.00059 1 8260B 7/26117 13:53 ANG P7GO413 Bromochloromethane BRL mg/kg dry 0.0070 0.00039 1 8260B 7126117 13:53 ANG P7GO413 Bromodichloromethane BRL mg/kg dry 0.0070 0.00039 1 82609 7/26117 13:53 ANG P7G0413 Bromoform BRL mg/kg dry 0.0070 0.00080 1 8260B 7/26117 13:53 ANG P7GO413 Bromomethane BRL mg/kg dry 0.014 0.00087 1 8260B 7126117 13:53 ANG P7GO413 Carbon Tetrachloride BRL mg/kg dry 0.0070 0.00035 1 8260B 7126/17 13:53 ANG P7G0413 Chlorobenzene BRL mg/kg dry 0.0070 0.00037 1 8260B 7/26117 13:53 ANG P7GO413 Chloroethane BRL mg/kg dry 0.014 0.00059 1 8260B 7/26/17 13:53 ANG P7G0413 Chloroform BRL mg/kg dry 0.0070 0.00051 1 82608 7126/17 13:53 ANG P7GO413 Chloromethene BRL mg/kg dry 0.0070 D.00D47 1 8260B 7/26117 13:53 ANG P7G0413 cis-1,2-Dichlomethylene BRL mg/kg dry 0.0070 0.00030 1 8260B 7/26/17 13:53 ANG P7GO413 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0070 0.00024 1 8260B 7/26/17 13:53 ANG P7GO413 Dibromochloromethane BRL mg/kg dry 0.0070 0.00029 1 8260B 7/26/17 13:53 ANG P7GO413 Dichlorodieuoromethane BRL mg/kg dry 0.0070 0.00032 1 8260B 7/26/17 13:63 ANG P7GO413 Ethylbenzene BRL mglkg dry 0.0070 0.00027 1 9260B 7/26/17 13:53 ANG P7GO413 Isopropyl Ether BRL mg/kg dry 0.0070 0.00029 1 8260B 7126117 13:53 ANG P7130413 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0070 0.00042 1 8260B 7/26/17 13:53 ANG P7GD413 m,p-Xylenes BRL mg/kg dry 0.014 0.00065 1 8260B 7126/17 13:53 ANG P7GO413 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364-Toll Free Number: l-8001529-6364-Fax: 7041525-0409 Page 13 of 50 PR R I S iL n Fu165ervice Analytical s � v' Envlronmcntal Solutions s Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Laboratory Report 07/31/2017 Project: Truck Part Service Client Sample ID: Lift-2 Prism Sample ID: 7070278-04 Prism Work Order: 7070278 Sample Matrix: Solid Time Collected: 07/17/17 10:26 Time Submitted: 07/17/17 15:45 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Dalerrime Batch ID Methyl Butyi Ketone (2-Hexanone) BRL mg/kg dry 0.070 0.00064 1 8260B 7126/17 13:53 ANG P7G0413 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.14 0.00064 1 8260B 7/26/17 13:53 ANG P7130413 Methyl Isobutyl Ketone BRL mg/kg dry 0.070 0.00060 1 8260B 7/26/17 13:53 ANG P7G0413 Methylene Chloride BRL mg/kg dry 0.014 0.00040 1 8260B 7/26/17 13:53 ANG P7130413 Methyl-tert-Butyl Ether BRL mg/kg dry 0.014 0.00023 1 8260B 7/26/17 13:53 ANG P7G0413 Naphthalene BRL mg/kg dry 0.014 0.00022 1 82608 7/26/17 13:53 ANG P7130413 n-Butylbemene BRL mg/kg dry 0.0070 0.00036 1 8260B 7/26/17 13:53 ANG P7G0413 n-Propylbenzene BRL mg/kg dry 0.0070 0.00042 1 8260B 7126/17 13:53 ANG P7G0413 c-Xylene BRL mg/kg dry 0.0070 0.00029 1 8260B 7126/17 13:53 ANG P7G0413 sec-Butylbenzene BRL ni dry 0.0070 0.00034 1 8260B 7126/17 13:53 ANG P7G0413 Styrene BRL mg/kg dry 0.0070 0.00042 1 8260B 7126/17 13:53 ANG P7130413 ten-Butylbenzene BRL mg/kg dry 0.0070 0.00024 1 8260B 7126/17 13:53 ANG P7G0413 Tetrechlomethylene BRL mg/kg dry 0.0070 0.00033 1 8260B 7/26/17 13:53 ANG P7G0413 Toluene BRL mgkg dry 0.0070 0.00040 1 8260B 7/26/17 13:53 ANG P7G0413 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0070 0.00042 1 8260B 7/26/17 13:53 ANG P7G0413 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0070 0.00037 1 8260E 7/26/17 13:53 ANG P7130413 Trichlomethylene BRL mg/kg dry 0.0070 0.00046 1 8260B 7/26117 13:53 ANG P7G0413 Trichlorofluoromethane BRL mg/kg dry 0.0070 0,00045 1 8260B 7126/17 13:53 ANG P71210413 Vinyl acetate BRL mg/kg dry 0.035 0.00096 1 8260B 7/26/17 13:53 ANG P7G0413 Vinyl chloride BRL mg/kg dry 0.0070 0.00034 1 8260B 7126/17 13:53 ANG P7G0413 Xylenes, total BRL mg/kg dry 0.021 0.0013 1 8260B 7/26117 13:53 ANG P7430413 Surrogate Recovery Control Limits 4-Bromofluorobenzene 101 % 70-130 Dibromofluoromethane 104 % 84-123 Toluen"S 97 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529.6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 14 of 50 �, I sem Full -Service Analytical & uewua ies me Envi�onmentel Solutions Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Sample Matrix: Solid Laboratory Report 07/31/2017 Client Sample ID: GP-1 Prism Sample ID: 7070278-05 Prism Work Order: 7070278 Time Collected: 07/17/17 14:55 Time Submitted: 07/17/17 15:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/rime ID General Chemistry Parameters %Solids 73.0 %by 0.100 0.100 1 •SM2540G 7/1811714:30 JLB P7G0278 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.45 0.070 1 8270D 7/20/17 15:51 JMV P7G0259 1,2-Dichlorobenzene BRL mg/kg dry 0.45 0.068 1 8270D 7/20117 15:51 JMV P7G0259 1,3-Dichlorobenzene BRL mg/kg dry 0.45 0.063 1 8270D 7/20/17 15:51 JMV P7G0259 1,4-Dichlorobenzene BRL mg/kg dry 0.45 0.066 1 6270D 7/20/17 15:51 JMV P7G0259 1-Methylnaphthalene BRL mg/kg dry 0.45 0.087 1 8270D 7/20/17 16:51 JMV P7G0259 2,4,6-Tdchlorophenol BRL mg/kg dry 0.45 0.084 1 8270D 7/20/17 15:51 JMV P7G0259 2,4-Dichlorophenol BRL mg/kg dry 0.45 0.087 1 8270D 7/20/17 15:51 JMV P7G0259 2,4-Dimethylphenal BRL CCV mg/kg dry 0.45 0.069 1 B270D 7/20/17 15:51 JMV P7G0259 2,4-Dinftrophenol BRL mg/kg dry 0.45 0.063 1 8270D 7/20/17 15:51 JMV P7G0259 2,4-Dindrotoluene BRL mg/kg dry 0.45 0.055 1 8270D 7120117 15:51 JMV P7G0259 2,6-Dinitrotoluene BRL mg/kg dry 0.46 0.060 1 8270D 7120/17 15:51 JMV P7G0259 2-Chlomnaphthalene BRL mg/kg dry 0.45 0.065 1 8270D 7120/17 15:51 JMV P7G0259 2-Chlorophenol BRL mg/kg dry 0.45 0.064 1 8270D 7/20/17 15:51 JMV P7G0259 2-Methylnaphthalene BRL mg/kg dry 0.45 0.072 1 8270D 7/20117 15:51 JMV P7G0259 2-Methylphenol BRL mg/kg dry 0.45 0.058 1 8270D 7/20/17 15:51 JMV P7G0259 2-Nitrophenol BRL mg/kg dry 0.45 0.082 1 8270D 7/20117 15:51 JMV P7G0259 3,3'-Dichlombenzidine BRL mg/kg dry 0.45 0.089 1 8270D 7/20/17 15:51 JMV P7G0259 3/4-Methylphenol BRL mg/kg dry 0.45 0.056 1 8270D 7/20117 15:51 JMV P7G0259 4,6-Dinibo-2-methylphenol BRL mg/kg dry 0.45 0.068 1 8270D 7/20/17 15:51 JMV P7G0259 4-Bromophenyl phenyl ether BRL mg/kg dry 0.45 0.077 1 8270D 7/20/17 15:51 JMV P7G0259 4-Chloro-3-methylphenol BRL mg/kg dry 0.45 0.063 1 8270D 7120/17 15:51 JMV P7G0259 4-Chloroaniline BRL mg/kg dry 0.45 0.054 1 8270D 7/20/17 15:51 JMV P7G0259 4-Chlomphenyl phenyl ether BRL mg/kg dry 0.45 0.059 1 8270D 7/20/17 15:51 JMV P7G0259 4-Nitrophenol BRL mg/kg dry 0.45 0.069 1 82701) 7120117 15:51 JMV P7G0259 Acenaphthene BRL mg/kg dry 0.45 0.061 1 8270D 7/20/17 15:51 JMV P7G0259 Acenaphthylene BRL mg/kg dry 0.45 0.065 1 8270D 720117 15:51 JMV P7G0259 Anthtacene BRL mg/kg dry 0.45 0.073 1 8270D 7120117 15:51 JMV P7G0259 Azobenzene BRL mg/kg dry 0.45 0.059 1 8270D 720/17 15:51 JMV P7G0259 Benzo(a)anthracene BRL mg/kg dry 0.45 0.059 1 8270D 7/20/17 15:51 JMV P7G0259 Benzo(a)pyrene BRL mg/kg dry 0.45 0.049 1 8270D 7/20/17 15:51 JMV P7G0259 Benzo(b)fluoranthene BRL mg/kg dry 0A5 0.052 1 8270D 7/20117 15:51 JMV P7G0269 Benzo(g,h,i)peMene BRL mg/kg dry 0.45 0.049 1 8270D 720117 15:51 JMV P7G0259 Benzo(k)fluoranthene BRL mg/kg dry 0.45 0.059 1 8270D 7/20/17 15:51 JMV P7G0259 Benzoic Add BRL mg/kg dry 0.45 0.038 1 8270D 7/20117 15:51 JMV P7G0259 Benzyl alcohol BRL mg/kg dry 0.46 0.059 1 8270D 720/17 15:51 JMV P7G0259 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.45 0.078 1 8270D 7/20117 15:51 JMV P7G0259 BiS(2-Chloroethyl)ether BRL mg/kg dry 0.45 0.064 1 82700 7120117 15:51 JMV P7G0259 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.45 0.077 1 8270D 7/20/17 15:51 JMV P7G0259 BIS(2-Ethylhexyl)phthelate BRL mg/kg dry 0.45 0.067 1 8270D 7120117 15:51 JMV P7G0259 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. "a Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6394 - Toll Free Number: 1-900/529.6364- Fax: 704/525-0409 Page 15of50 �P R I S M Fuh server A Soy, s Ew,anme ,e aoiouo s A-1, ..Es,- Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Sample Matrix: Solid Laboratory Report 07/31 /2017 Client Sample ID: GP-1 Prism Sample ID: 7070278-05 Prism Work Order: 7070278 Time Collected: 07/17/17 14:55 Time Submitted: 07/17/17 15:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Butyl henzyl phthalate BRL mg/kg dry 0.45 0.064 1 82700 7120117 15:51 JMV P7G0259 Chrysene BRL mg/kg dry 0.45 0.057 1 8270D 7/20/17 15:51 JMV P7G0259 Dibenzo(a,h)anthrecene BRL mg/kg dry 0.45 0.055 1 8270D 7/20/17 15:51 JMV P7G0259 Dibenzofuran BRL mg/kg dry 0.45 0.068 1 8270D 7/20/17 15:51 JMV P7G0259 Diethyl phthalate BRL mg/kg dry 0.45 0.062 1 8270D 7/20/17 15:51 JMV P7G0259 Dimethyl phthalate BRL mg/kg dry 0.45 0.059 1 8270D 7/20/17 15:51 JMV P7G0259 Di-n-butyl phthalate BRL mg/kg dry 0.45 0.064 1 8270D 7120117 15:51 JMV P7G0259 Di-n-octyl phthalate BRL mg/kg dry 0.45 0.055 1 8270D 7120/17 15:51 JMV P7G0259 Fluoranthene BRL mg/kg dry 0.45 0.057 1 8270D 7/20/17 15:51 JMV P7G0259 Fluorene BRL mg/kg dry 0.45 0.065 1 a270D 7/20/17 15:51 JMV P7G0259 Hexachlorobenzene BRL mgft dry 0.45 0.071 1 8270D 7/20/17 15:51 JMV P7G0259 Hexachlorobutediene BRL mg/kg dry 0.45 0.081 1 8270D 7/20/17 15:51 JMV P7G0259 Hexachlorocydopentadiene BRL mg/kg dry 0.45 0.080 1 8270D 7/20/17 15:51 JMV P7G0259 Hexachloroethane BRL mg/kg dry 0.45 0.075 1 8270D 7120/17 15:51 JMV P7G0259 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0,45 0.052 1 8270D 7120/17 15:51 JMV P7G0259 Isophorone BRL mg/kg dry 0.45 0.061 1 8270D 7120/17 15:51 JMV P7G0259 Naphthalene BRL mg/kg dry 0.45 0.072 1 8270D 7120117 15:51 JMV P7G0259 Nitrobenzene BRL mg/kg dry 0.45 0.064 1 8270D 7/20/17 15:51 JMV P7G0259 N-Nimoso-di-n-propylamine BRL mg/kg dry 0.45 0.071 1 8270D 7/20/17 15:51 JMV P7G0259 N-Nitrosodiphenylamine BRL mg/kg dry 0.45 0.068 1 8270D 7/20117 15:51 JMV P7G0259 Pentachlorophenol BRL mg/kg dry 0.45 0.053 1 8270D 7120/17 15:51 JMV P7G0259 Phenanthrene BRL mg/kg dry 0.45 0.059 1 8270D 7/20/17 15:51 JMV P7G0259 Phenol BRL mg/kg dry 0.45 0.066 1 8270D 7/20117 15:51 JMV P7G0259 Pyrene BRL mg/kg dry 0.45 0.060 1 8270D 7/20117 15:51 JMV P7G0259 Surrogate Recovery Control Limits 2,4,6-Tribromophencl 61 % 39-132 2-Fluorobiphenyl 56 % 44-115 2-Fluorophenol 59 % 35-115 Nitrobenzened5 54 % 37-122 Phenol-d5 59 % 34-121 Terphenyldl4 75% 54-127 Total Metals Hexavalerd Chromium 0.82 mg/kg dry 0.64 0.18 1 '7196A 7/24/1710:00 BMS P700274 Mercury BRL mg/kg dry 0.028 0.0027 1 •7471B 7/20117 11:41 JAB P7G0287 Arsenic BRL DM mg/kg dry 1.7 0.21 5 •6010D 7125/17 17:10 JAB P7G0320 Barium 13 DM mg/kg dry 3.4 0.50 5 •601013 7/26117 14:18 JAB P700320 Cadmium BRL DM mg/kg dry 1.7 0.046 5 •6010D 7126/17 14:18 JAB P7G0320 Chromium 55 DM mg/kg dry 1.7 0.29 5 •6010D 7125/17 17:10 JAB P7G0320 Lead 34 DM mg/kg dry 1.7 0.32 5 •6010D 7125117 17:10 JAB P7G0320 Selenium 9.9 DM mii dry 3.4 0.81 5 •60101) 7/25/17 17:10 JAB P760320 Silver BRL OM mg/kg dry 1.7 0,042 5 •6010D 7125/17 17:10 JAB P7G0320 Volatile Organic Compounds by GC/MS This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 70415296364 -Toll Free Number: 1.80015296364 - Fax: 7041525-0409 Page 16 of 50 �P R I S Laboratory Report �. wu serums nnaiytmai a Env ronmental Solutions a r; we 07/31/2017 Geoscience Group Project: Truck Part Service Client Sample ID: GP-1 Attn:Tom Hassett Prism Sample ID: 7070278-05 500-K Clanton Rd. Prism Work Order: 7070278 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/17/17 14:55 Time Submitted: 07/17/17 15:45 Parameter Result Units Report Limit MOIL Dilution Factor Method Analysis Date/rime Analyst Batch ID 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0042 0.00034 1 8260B 7/26117 14:21 ANG P7G0413 1,1,1-Trichloroethane BRL mg/kg dry 0.0042 0.00020 1 8260B 7/26/17 14:21 ANG P7G0413 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0042 0.00028 1 8260B 7/26117 14:21 ANG P7G0413 1,1,2-Trichloroethane BRL mg/kg dry 0.0042 0.00037 1 8260B 7/26117 14:21 ANG P7G0413 1,1-Dichlorcethane BRL mg/kg dry 0.0042 0.00012 1 8260B 7/26/17 14:21 ANG P7G0413 1,1-Dichloroethylene BRL mg/kg dry 0.0042 0.00018 1 8260B 7/26/17 14:21 ANG P7G0413 1,1-Dichlompropylene BRL mgft dry 0.0042 0.00023 1 8260B 7126/17 14:21 ANG P7G0413 1,2,3-Tdchlorobemene BRL mg/kg dry 0.0042 0.00024 1 82608 7126117 14:21 ANG P7GD413 1,2,3-Trichloropropane BRL mg*g dry 0.0042 0.00053 1 8260B 7126117 14:21 ANG P7G0413 1,2,4-Tdchlorobenzene BRL mg/kg dry 0,0042 0.00031 1 8260B 7/26/17 14:21 ANG P7G0413 1,2,4-Trimethylbenzene BRL mg/kg dry 0,0042 0.00032 1 8260B 7/26/17 14:21 ANG P7GD413 1,2-Dibromcethane BRL mg/kg dry 0.0042 0.00017 1 8260B 7/26/17 14:21 ANG P7G0413 1,2-Dichlorobenzene BRL mg/kg dry 0.0042 0.00020 1 8260B 7/26/17 14:21 ANG P7GD413 1,2-Dichlomethane BRL mg/kg dry 0.0042 0.00025 1 8260B 7/26/17 14:21 ANG P7G0413 1,2-Dichloropropane BRL mg/kg dry 0.0042 0.00026 1 8260B 7/26117 14:21 ANG P7G0413 1,3,5-Tdmethylbenzene BRL mg/kg dry 0.0042 0,00031 1 8260B 7/26117 14:21 ANG P7G0413 1,3-Dichlombenzene BRL mg/kg dry 0.0042 0.00028 1 8260B 7/26/17 14:21 ANG P7G0413 1,3-Dichloropropane BRL mg/kg dry 0.0042 0.00021 1 8260B 7/26/17 14:21 ANG P7130413 1,4-Dichlombenzene BRL mg/kg dry 0.0042 0.00016 1 8260B 7/26/17 14:21 ANG P7G0413 2,2-Dichloropropane BRL mg/kg dry 0.0042 0.00020 1 8260B 7/26/17 14:21 ANG P7G0413 2-Chlorotoluene BRL mg/kg dry 0.0042 0.00021 1 8260B 7/26117 14:21 ANG P7GD413 4-Chlorotoluene BRL mg/kg dry 0,0042 0.00025 1 8260B 7/26/17 14:21 ANG P7G0413 4-Isopropyltoluene BRL mg/kg dry 0.0042 0.00020 1 8260B 7/26117 1421 ANG P7G0413 Acetone 0.034 J mg/kg dry 0.042 0.0010 1 8260B 7126/17 14:21 ANG P700413 Benzene BRL mg/kg dry 0.0025 0.00024 1 a260B 7/26/17 14:21 ANG P7GD413 Bromobenzene BRL mg/kg dry 0,0042 0.00035 1 8260B 7/26/17 14:21 ANG P7G0413 Bromochloromethane BRL mg/kg dry 0.0042 0.00023 1 8260B 7/26/17 14:21 ANG P7G0413 Bromodichloromethane BRL mg/kg dry 0.0042 0.00023 1 8260B 7/26/17 14:21 ANG P7G0413 Bromoform BRL mg/kg dry 0.0042 0.00047 1 8260B 7/26/17 14:21 ANG P7GD413 Bromomethane BRL mg/kg dry 0.0083 0.00051 1 8260B 7/26/17 14:21 ANG P7G0413 Carbon Tetrachloride BRL mg/kg dry 0.0042 0.00021 1 8260B 7/26/17 14:21 ANG P7G0413 Chlorobenzene BRL mg/kg dry 0.0042 0.00022 1 8260B 7/26/17 14:21 ANG P7G0413 Chloroethane BRL mg/kg dry 0.0083 0-00035 1 8260B 7126117 14:21 ANG P7G0413 Chloroform BRL mg/kg dry 0.0042 0.00030 1 8260B 7/26/17 14:21 ANG P7G0413 Chloromethane BRL mg/kg dry 0.0042 0.00028 1 8260B 7126/17 14:21 ANG P7G0413 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0042 0.00018 1 8260B 7/26/17 14:21 ANG P7G0413 cis-1,3-Dichloropropylene BRL mglkg dry 0.0042 0.00014 1 8260B 7/26117 14:21 ANG P7G0413 Dibromochloromethane BRL mg/kg dry 0.0042 0.00017 1 8260B 7126117 14:21 ANG P7G0413 Dichlorodi8uoromethane BRL mg/kg dry 0.0042 0.00019 1 826015 7/26/17 14:21 ANG P7G0413 Ethylbenzene BRL mg/kg dry 0.0042 0.00016 1 8260B 7/26/17 14:21 ANG P7G0413 Isopropyl Ether BRL mg/kg dry 0.0042 0.00017 1 8260B 7/26/17 14:21 ANG P7GD413 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0042 0,00025 1 8260B 7126/17 14:21 ANG P7G0413 m,p-Xylenes BRL mgekg dry 0.0083 0.00038 1 8260B 7/26/17 14:21 ANG P7GD413 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spdngbrook Road - P.O. Box 240543 - Charlotte, NC 29224-0543 Phone: 7041S29.6364 - Toll Free Number: 1-800/529.6364 - Fax: 7041525-0409 Page 17 of 50 Full PR I SaM I EnV semee al SOl ufla s P` EnvUOnmeMal Solutions AMIN Laboratory Report 07/31/2017 Geoscience Group Project: Truck Part Service Client Sample ID: GP-1 Attn: Tom Hassett Prism Sample ID: 7070278-05 500-K Clanton Rd. Prism Work Order: 7070278 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/17/17 14:55 Time Submitted: 07/17/17 15:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DateMme ID MelhN Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.042 0.00038 1 8260B 7/26/17 14:21 ANG P7G0413 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.083 0.00038 1 8260B 7/26/17 14:21 ANG P7G0413 Methyl Isobutyl Ketone BRL mg/kg dry 0.042 0.00035 1 8260B 7126/17 14:21 ANG P7G0413 Methylene Chloride BRL mg/kg dry 0.0083 0.00023 1 8260B 7/26/17 14:21 ANG P7G0413 Methyl-tert-Butyl Ether BRL mg/kg dry 0.0083 0.00013 1 8260B 7126/17 14:21 ANG P7130413 Naphthalene BRL mg/kg dry 0.0083 0.00013 1 82608 7126117 14:21 ANG P7130413 n-Bulylbenzene BRL mg/kg dry 0.0042 0.00021 1 8260B 7126/17 14:21 ANG P7G0413 n-Propylbenzene BRL mg/kg dry 0.0042 0.00025 1 8260B 7126117 14:21 ANG P7G0413 o-Xylene BRL mi dry 0.0042 0.00017 1 8260B 7/26117 14:21 ANG P7130413 sec-Butylbenzene BRL mg/kg dry 0.0042 0.00020 1 8260B 7126117 14:21 ANG P7G0413 Styrene BRL mg/kg dry 0.0042 0.00025 1 8260B 7/26/17 14:21 ANG P7G0413 tert-Butylbenzene BRL mg/kg dry 0.0042 0.00014 1 8260B 7/26/17 14:21 ANG P7G0413 Tetrachloroethylene BRL mg/kg dry 0.0042 0.00020 1 8260B 7126/17 14:21 ANG P7G0413 Toluene BRL mg/kg dry 0.0042 0.00024 1 8260B 7/26/17 14:21 ANG P7130413 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0042 0.00025 1 8260B 7/26/17 14:21 ANG P7G0413 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0042 0.00022 1 8260B 7126/17 14:21 ANG P7130413 Trichloroelhylene BRL mg/kg dry 0.0042 0.00027 1 8260B 7126117 14:21 ANG P7G0413 Tdchloro8uoromethane BRL mg/kg dry 0.0042 0.00027 1 8260B 7/26/17 14:21 ANG P7G0413 Vinyl acetate BRL mg/kg dry 0.021 0.00057 1 82608 7/26/17 14:21 ANG P7G0413 Vinyl chloride BRL mg/kg dry 0.0042 0.00020 1 8260B 7/26/17 14:21 ANG P7G0413 Xylenes, total BRL mg/kg dry 0.012 0.00078 1 8260B 7/26117 14:21 ANG P7130413 Surrogate Recovery Control Limits 4-Bromoeuorobenzene 103 % 70-130 Dibromofluoromethane 104 % 84-123 Toluene-08 98 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 2405" - Charlotte, NC 28224-0543 Phone: 704/529.6364-Toll Free Number: l-8001629-6364- Fax: 704/525-0409 Page 18o150 P R I SqM I i wi_sa.vma „s e uo- u"s Emlronmental Solutions Geoscienoe Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Sample Matrix: Solid Laboratory Report 07/31/2017 Client Sample ID: GP-2 Prism Sample ID: 7070278-06 Prism Work Order: 7070278 Time Collected: 07/17/17 15:13 Time Submitted: 07/17/17 15:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DateMme ID General Chemistry Parameters %Solids 79.8 %by 0.100 0.100 1 •SM25400 7/18/1714:30 JLB P7130278 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichiorobenzene BRL mg/kg dry 0.41 0.064 1 8270D 7/20117 16:14 JMV P7G0259 1,2-Dichlorobemene BRL mg/kg dry 0.41 0.063 1 8270D 7/20117 16:14 JMV P7G0259 1,3-Dichiorobenzene BRL mg/kg dry 0A1 0.058 1 8270D 7120/17 16:14 JMV P7G0259 1,4-Dichlorobenzene BRL mg/kg dry 0.41 0.060 1 8270D 7/20/17 16:14 JMV P7130259 1-Methyinaphthalene BRL mg/kg dry 0.41 0.080 1 8270D 7/20/17 16:14 JMV P7G0259 2,4,6-Thchiomphenol BRL mg/kg dry 0.41 0.077 1 8270D 7/20117 16:14 JMV P7130259 2,4-Dichlorophenol BRL mg/kg dry 0.41 0.080 1 9270D 7120/17 16:14 JMV P7G0259 2,4-Dimethyiphenol BRL CCV mg/kg dry 0.41 0.063 1 8270D 7/20117 16:14 JMV P7130259 2,4-Dinhrophenol BRL mg/kg dry 0.41 0.058 1 8270D 7/20117 16:14 JMV P7G0259 2,4-Dinibotoluene BRL mg/kg dry 0.41 0.050 1 8270D 7/20/17 16:14 JMV P7G0259 2,6-Din6otoluene BRL mg/kg dry 0.41 0.055 1 8270D 7120/17 16:14 JMV P7G0259 2-Chloronaphthalene BRL mg/kg dry 0.41 0,060 1 8270D 7/20/17 16:14 JMV P7G0259 2-Chlorophenol BRL mg/kg dry 0.41 0.059 1 8270D 7120/17 16:14 JMV P7130259 2-Methylnaphthelene BRL mg/kg dry 0.41 0.066 1 8270D 7/20/17 16:14 JMV P7130259 2-Methylphenol BRL mg/kg dry 0.41 0.053 1 8270D 7/20117 16:14 JMV P7G0259 2-Nitrophenol BRL mg/kg dry 0.41 0.075 1 8270D 7/20/17 16:14 JMV P7G0259 3,3' Dichlorobenzidine BRL mg/kg dry 0.41 0.082 1 8270D 7120/17 16:14 JMV P7G0259 3/4-Methylphenol BRL mg/kg dry 0.41 0.051 1 8270D 7/20117 16:14 JMV P7G0259 4,6-Dinhro-2-methy phenol BRL mg/kg dry 0.41 0.062 1 8270D 7120117 16:14 JMV P7G0259 4-Bromophenyl phenyl ether BRL mg/kg dry 0.41 0.071 1 8270D 7/20117 16:14 JMV P7G0259 4-Chloro-3-methylphenol BRL mg/kg dry 0.41 0.058 1 8270D 7/20117 16:14 JMV P7G0259 4-Chioroaniline BRL mg/kg dry 0.41 0.050 1 8270D 7/20117 16:14 JMV P7G0259 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.41 0.054 1 8270D 7/20117 16:14 JMV P7G0259 4-Nitrophenol BRL mg/kg dry 0.41 0.064 1 8270D 7/20117 16:14 JMV P7G0259 Acenaphthene BRL mg/kg dry 0.41 0.056 1 8270D 7/20/17 16:14 JMV P7G0259 Acenaphthylene BRL mg/kg dry 0.41 0,060 1 8270D 7/20/17 16:14 JMV P7130259 Anthracene BRL mg/kg dry 0.41 0.067 1 8270D 7/20/17 16:14 JMV P7130259 Azobenzene BRL mg/kg dry 0.41 0.055 1 8270D 7/20/17 16:14 JMV P7G0259 Benzo(a)anthracene BRL mg/kg dry 0.41 0.054 1 8270D 7/20/17 16:14 JMV P7G0259 Benzo(s)pyrene BRL mg/kg dry 0.41 0.045 1 8270D 7120117 16:14 JMV P7G0259 Benzo(b)fluoranthene BRL mg/kg dry 0.41 0.048 1 8270D 7/20/17 16:14 JMV P7G0259 Benzo(g,h,i)peMene BRL mg/kg dry 0.41 0.045 1 8270D 7120117 16:14 JMV P7G0259 Benzo(k)fluoranthene BRL mg/kg dry 0.41 0.054 1 8270D 7/20/17 16:14 JMV P7G0259 Benzoic Acid 2.0 mg/kg dry 0.41 0.036 1 8270D 7/20/17 16:14 JMV P700259 Benzyl alcohol BRL mg/kg dry 0.41 0.054 1 8270D 7/20117 16:14 JMV P7G0259 bis(2-Chioroethoxy)methene BRL mg/kg dry 0A1 0.072 1 8270D 7/20/17 16:14 JMV P7130259 Sis(2-Chloroethyl)ether BRL mgkg dry 0.41 0.058 1 8270D 7/20/17 16:14 JMV P7G0259 Sis(2-chloroisopropyl)ether BRL mg/kg dry 0.41 0.071 1 6270D 7/20/17 16:14 JMV P7G0259 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.41 0.061 1 82700 7/20/17 16:14 JMV P7G0259 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charaane, NC 29224-0643 Phone: 7041529.6364 - Toll Free Number: 1.8001529.6364 - Fax: 704/525-0409 Page 19 of 50 F.V usoam qas we 'ce AnalytcalRISM Euvrormemai Solutions ssR Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, INC 28217 Project: Truck Part Service Sample Matrix: Solid Laboratory Report 07131/2017 Client Sample ID: GP-2 Prism Sample ID: 7070278-06 Prism Work Order: 7070278 Time Collected: 07/17/17 15:13 Time Submitted: 07/17/17 15:45 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Butyl benzyl phthalate BRL mglkg dry 0.41 0.059 1 8270D 7/20/17 16:14 JMV P7G0259 Chrysene BRL mg/kg dry 0.41 0.052 1 8270D 7120/17 16:14 JMV P7130259 Dibenzo(a,h)anthracene BRL ml dry 0Al 0.050 1 8270D 7/20/17 16:14 JMV P7430259 Dibemofuran BRL rl dry 0.41 0.063 1 8270D 7120/17 16:14 JMV P7G0259 Diethyl phthalate BRL ml dry 0.41 0.057 1 8270D 7/20/17 16:14 JMV P7130259 Dimethyl phthalate BRL mg/kg dry 0.41 0.055 1 8270D 7/20/17 16:14 JMV P7G0259 Di-n-butyl phthalate BRL mg/kg dry 0.41 0.059 1 82700 7120117 16:14 JMV P7G0259 Di-n-octyl phthalate BRL ml dry 0.41 0.051 1 8270D 7120117 16:14 JMV P7G0259 Fluoranthene BRL mg/kg dry 0.41 0.053 1 8270D 7/20/17 16:14 JMV P7G0259 Fluorene BRL ml dry 0.41 0.059 1 8270D 7/20/17 16:14 JMV P7G0259 Hamchlorobenzene BRL mg/kg dry 0.41 0.066 1 8270D 7/20/17 16:14 JMV P7130259 Hexachlombutediene BRL mg/kg dry 0.41 0.074 1 8270D 7120/17 16:14 JMV P7G0259 Hexachlorocydopentadiene BRL mg/kg dry 0.41 0.074 1 8270D 7/20/17 16:14 JMV P7G0259 Hexachlomethane BRL mg/kg dry 0.41 0.069 1 8270D 7/20/17 16:14 JMV P7G0259 Indeno(1,2,3-nd)pyrene BRL ml dry 0.41 0.D47 1 8270D 7/20/17 16:14 JMV P7G0259 Isophorone BRL mg/kg dry 0.41 0.056 1 8270D 7/20/17 16:14 JMV P7G0259 Naphthalene BRL ml dry 0.41 0.066 1 8270D 7120/17 16:14 JMV P7G0259 Nitrobenzene BRL rl dry 0.41 0.059 1 8270D 7120/17 16:14 JMV P7130259 N-Nitroso-di-n-propylamine BRL ml dry 0A1 0.065 1 8270D 7120/17 16:14 JMV P7G0259 N-Nitrosodiphenylamine BRL mglkg dry 0.41 0.063 1 8270D 7/20/17 16:14 JMV P7G0259 Pentachlorophenol BRL mg/kg dry 0.41 0.049 1 8270D 7120117 16:14 JMV P7430259 Phenanthrene BRL mg/kg dry 0.41 0.054 1 8270D 7/20117 16:14 JMV P7G0259 Phenol BRL mg/kg dry 0A1 0.061 1 8270D 7120117 16:14 JMV P7130259 Pyrene BRL mglkg dry 0.41 0.055 1 8270D 7120/17 16:14 JMV P7G0259 Surmgate Recovery Control Limits 2,4,6-Tribromophenol 71 % 39-132 2-Fluorobiphenyl 62 % 44-115 2-Fluorophenol 63 % 35-115 Nitrobenzene-d5 57% 37-122 Phenol-d5 65 % 34-121 TerphenylEl4 77 % 54-127 Total Metals Hexavalent Chromium 0.55 ml dry 0.50 0.16 1 '7196A 7/24/17 10:00 ISMS P760274 Mercury 0.031 al dry 0.026 0.0025 1 '7471B 712011711:46 JAB P700287 Arsenic 0.35 ml dry 0.31 0.039 1 '6010D 7124/1715:06 JAB P760320 Barium 18 ml dry 0.63 0.092 1 '6010D 7MI17 20:29 JAB P700320 Cadmium BRL mg/kg dry 0.31 0.0084 1 •6010D 7/24/17 15:08 JAB P7430320 Chromium 16 ml dry 0.31 0.063 1 '6010D 7121/17 20:29 JAB P7G0320 Lead 7.3 mg/kg dry 0.31 0.059 1 '6010D 7/21/17 20:29 JAB P700320 Selenium 2.0 ml dry 0.63 0.15 1 '6010D 7121/17 20:29 JAB P7G0320 Silver BRL mg/kg dry 0.31 0.0078 1 •6010D 7/21117 20:29 JAB P7G0320 Volatile Organic Compounds by GC/MS This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number. l-8001529-6364- Fax: 704/525-0409 Page 200f 50 r� O M I /� Fuu eervlce nnalyt�cai 8 R.FR Environmental Solutions Isom er,ss,Ne Laboratory Report 07/31/2017 Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Sample Matrix: Solid Client Sample ID: GP-2 Prism Sample ID: 7070278-06 Prism Work Order: 7070278 Time Collected: 07/17/17 15:13 Time Submitted: 07/17/17 15:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Ys Batch Limit Factor Date rime ID 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0053 0.00043 1 8260B 7126/17 14:48 ANG P7G0413 1,11-Ttichlomethane BRL mg8tg dry 0.0053 0.00026 1 8260B 7126/17 14:48 ANG P7130413 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0053 0.00036 1 8260B 7126/17 14:48 ANG P7130413 1,1,2-Trichloroethane BRL mg/kg dry 0.0053 0.00047 1 8260B 7/26/17 14:48 ANG P7130413 1,1-Dichloroethane BRL mg/kg dry 0,0053 0.00015 1 8260B 7/26/17 14:48 ANG P7130413 1,1-Dichlomethylene BRL mg/kg dry 0.0053 0.00023 1 8260B 7126/17 14:48 ANG P7130413 1,1-Dichloropropylene BRL mg/kg dry 0.0053 0.00029 1 8260B 7126/17 14:48 ANG P7G0413 1,2,3-Tichoorobenzene BRL mg/kg dry 0.0053 0.00030 1 8260B 7/26/17 14:48 ANG P7G0413 1,2,3-Tdchloropropane BRL mg/kg dry 0.0053 0.00067 1 8260B 7/26/17 14:48 ANG P7G0413 1,2,4-Tnchlorobenzene BRL mg/kg dry 0.0053 0.00039 1 8260B 7126117 14:48 ANG P7G0413 1,2,4-Trimethylbenzene BRL mg/kg dry 0.0053 0.00040 1 8260B 7126/17 14:48 ANG P7G0413 1,2-Dibromoethans BRL mg/kg dry 0.0053 0.00021 1 8260B 7/26117 14:48 ANG P7G0413 1,2-Dichlorobenzene BRL mg/kg dry 0.0053 0.00025 1 8260B 7126117 14:48 ANG P7G0413 12-Dichloroethane BRL mg/kg dry 0.0053 0.00031 1 82608 7/26/17 14:48 ANG P7G0413 1,2-Dichloropropane BRL mg/kg dry 0.0053 0.00033 1 8260B 7126/17 14:48 ANG P7G0413 1,3,5-Tdmethylbenzene BRL mg/kg dry 0.0053 0.00040 1 8260B 7/26117 14:48 ANG P7G0413 1,3-Dichlorobenzene BRL mg/kg dry 0.0053 0.00035 1 8260B 7/26/17 14:48 ANG P7G0413 1,3-Dichloropropane BRL mg/kg dry 0.0053 0.00026 1 8260B 7/26117 14:48 ANG P7G0413 1,4-Dichlorobenzene BRL mg/kg dry 0.0053 0.00021 1 8260B 7126/17 14:48 ANG P7G0413 2,2-Dichloropropane BRL mg/kg dry 0.0053 0.00025 1 8260B 7/26/17 14:48 ANG P7G0413 2-Chlorotoluene BRL mg/kg dry 0,0053 0.00027 1 8260B 7126117 14:48 ANG P7G0413 4-Chlorotoluene BRL mg/kg dry 0.0053 0.00031 1 8260B 7/26117 14:48 ANG P7G0413 4-Isopropyltoluene BRL mg/kg dry 0.0053 0.00025 1 8260B 7/26117 14:48 ANG P7130413 Acetone BRL mg/kg dry 0.053 0.0013 1 8260B 7/26/17 14:48 ANG P7G0413 Benzene BRL mg/kg dry 0.0032 0.00031 1 8260B 7/26/17 14:48 ANG P7G0413 Bromobenzene BRL mg/kg dry 0.0053 0.00044 1 8260B 7/26/17 14:48 ANG P7G0413 Bromochlommethane BRL mg/kg dry 0.0053 0.00029 1 8260B 7/26/17 14:48 ANG P7G0413 Bromodichloromethane BRL mg/kg dry 0.0053 0.00029 1 8260B 7126/17 14:48 ANG P7G0413 Bromoform BRL mg/kg dry 0.0053 0.00060 1 8260B 7126/17 14:48 ANG P7G0413 Bromomethane BRL mg/kg dry 0.011 0,00066 1 82608 7/26/17 14:48 ANG P7130413 Carbon Tetrachloride BRL mg/kg dry 0.0053 0.00026 1 8260B 7126117 14:48 ANG P7G0413 Chlombenzene BRL mg/kg dry 0.0053 0.00028 1 8260B 7/26/17 14:48 ANG P7G0413 Chloroethane BRL mg/kg dry 0.011 0.00044 1 8260B 7/26/17 14:48 ANG P7G0413 Chloroform BRL mg/kg dry 0.0053 0.00038 1 8260B 7/26/17 14:48 ANG P7130413 Chloromethane BRL mg/kg dry 0.0053 0.00035 1 8260B 7/26/17 14:48 ANG P7130413 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0053 0.00022 1 8260B 7126/17 14:48 ANG P7G6413 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0053 0.00018 1 8260B 7/26/17 14:48 ANG P7G0413 Dibromochloromethane BRL mg/kg dry 0.0053 0.00022 1 8260B 7/26117 14:48 ANG P7130413 Dichlorodieuoromethane BRL mg/kg dry 0.0053 0.00024 1 82608 7/26/17 14:48 ANG P7G0413 Ethylbenzene BRL mg/kg dry 0.0053 0.00020 1 8260B 7/26117 14:48 ANG P7G0413 Isopropyl Ether BRL mg/kg dry 0.0053 0.00022 1 8260B 7/26/17 14:48 ANG P7130413 Isopropylbenzene (Cumene) BRL mg/kg dry 0,0053 0.00031 1 82608 7/26/17 14:48 ANG P7130413 m,p-Xylenes BRL mg/kg dry 0.011 0.00049 1 8260B 7/26/17 14:48 ANG P7G0413 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 26224-0643 Phone: 704/529-0354-Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page21 Df50 "- tRISM I Wn aery ce analNical8 Laboratory Report am env.onmemai sewunoa 07/31/2017 Geoscience Group Project: Truck Part Service Client Sample ID: GP-2 Attn: Tom Hassett Prism Sample ID: 7070278-06 500-K Clanton Rd. Prism Work Order: 7070278 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/17/17 15:13 Time Submitted: 07/17/17 15:45 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date7rime Analyst Batch ID Methyl Butyl Ketone (2-Hexanone) BRL mgkg dry 0.053 0.00046 1 8260B 7126117 14:48 ANG P7130413 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.11 0.00048 1 8260B 7/26/17 14:48 ANG P7130413 Methyl Isobutyl Ketone BRL mg/kq dry 0.053 0.00045 1 8260B 7126117 14:48 ANG P7G0413 Methylene Chloride BRL mg/kg dry 0.011 0.00030 1 8260B 7/26/17 14A8 ANG P7130413 Methyl-tert-Butyl Ether BRL mg/kg dry 0.011 0,00017 1 8260B 7126117 14:48 ANG P7G0413 Naphthalene BRL mgkg dry 0.011 0.00017 1 8260B 7126117 14:48 ANG P7G0413 n-Butylbenzene BRL mg/kg dry 0.0053 0.00027 1 8260B 7/26/17 14A8 ANG P7130413 n-Propylbenzene BRL mg/kg dry 0.0053 0.00031 1 8260B 7126/17 14:48 ANG P7G0413 o-Xylene BRL mg/kg dry 0.0053 0.00022 1 8260B 7/26/17 14:48 ANG P7G0413 sec-Butylbenzene BRL mi dry 0.0053 0.00026 1 8260B 7126117 14A8 ANG P7G0413 Styrene BRL - mg/kg dry 0.0053 0.00032 1 8260B 7126117 14:46 ANG P7130413 ten-Butylbenzene BRL mg/kg dry 0.0053 0.00018 1 8260B 7/26/17 14:48 ANG P7130413 Tetrechloroethylene BRL mg/kg dry 0.0053 0.00025 1 8260B 7126/17 14:48 ANG P7G0413 Toluene BRL mg/kg dry 0.0053 0.00030 1 8260B 7126/17 14:48 ANG P7130413 trans-1,2-Dichlomethylene BRL mg/kg dry 0.0053 0.00032 1 8260B 7/26117 14:48 ANG P7G0413 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0053 0,00028 1 8260B 7/26/17 14:48 ANG P7G0413 Tdchloroethylene BRL mg/kg dry 0.0053 0.00034 1 8260B 7/26/17 14:48 ANG P7G0413 Tdchlorofluoromethane BRL mg/kg dry 0.0053 0.00034 1 8260B 7/26117 14:48 ANG P7G0413 Vinyl acetate BRL mg/kg dry 0.026 0.00072 1 8260B 7126/17 14:48 ANG P7G0413 Vinyl chloride BRL mg/kg dry 0,0053 0.00026 1 8260B 7/26117 14:48 ANG P7G0413 Xylenes, total BRL mg*g dry 0.016 0.00099 1 8260B 7126/17 14:48 ANG P7430413 Surrogate Recovery Control Limits 4-Bromofluorobemens 99 % 70-130 Dibromofluoromethane 100 % 84-123 Toluene118 97 % 76-129 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.4364 - Toll Free Number: 1-8001529.6364 - Fax: 704/525-0409 Page 22 of 50 PRISMI E er,reeallutia ro me ra Solutions weow..on,es,Hc Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Sample Matrix: Solid Laboratory Report 07/31/2017 Client Sample ID: GP-3 Prism Sample ID: 7070278-07 Prism Work Order: 7070278 Time Collected: 07/17/17 14:24 Time Submitted: 07/17/17 15:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date rime ID General Chemistry Parameters %Solids 78A %by 0.100 0.100 1 •SM25400 7MB/1714:30 JLB P7G0278 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Tichlorobenzene BRL mg/kg dry 0.42 0.065 1 8270D 7120/17 16:37 JMV P7G0259 1,2-Dichlorobenzene BRL mglkg dry 0.42 0.064 1 8270D 7120117 16:37 JMV P7G0259 1,3-Dichlorobenzene BRL mg/kg dry 0.42 0.059 1 8270D 7/20117 16:37 JMV P7G0259 1,4-Dichlorobenzene BRL mg/kg dry 0.42 0.061 1 8270D 7/20/17 16:37 JMV P7G0259 1-Methylnaphthalene BRL mg/kg dry 0.42 0.081 1 8270D 7120117 16:37 JMV P7G0259 2,4,6-Tdchlorophenol BRL mglkg dry 0.42 0.079 1 8270D 7/20/17 16:37 JMV P7G0259 2,4-Dichlomphenol BRL mg/kg dry 0.42 0.081 1 8270D 7120/17 16:37 JMV P7130259 2,4-Dimethylphenol BRL CCV mg/kg dry 0.42 0.064 1 8270D 7120/17 16:37 JMV P7G0259 2,4-Dinitrophenol BRL mg/kg dry 0.42 0,059 1 8270D 7120/17 16:37 JMV P7G0259 2,4-Dinihotoluene BRL mg/kg dry 0.42 0.051 1 9270D 7/20/17 16:37 JMV P7G0259 2,6-Dinitrotoluene BRL mg/kg dry 0.42 0.056 1 8270D 7120117 16:37 JMV P7G0259 2-Chloronaphthalene BRL mg/kg dry 0.42 0.061 1 8270D 7/20/17 16:37 JMV P7G0259 2-Chlorophenol BRL mg*g dry 0.42 0,059 1 8270D 7/20/17 16:37 JMV P7G0259 2-McBryinaphthalene BRL mg/kg dry 0.42 0,067 1 8270D 7120/17 16:37 JMV P7130259 2-Methylphenol BRL mg/kg dry 0.42 0.054 1 8270D 7120117 16:37 JMV P7G0259 2-Nitrophenol BRL mg/kg dry 0.42 0.076 1 8270D 7/20/17 16:37 JMV P7G0259 3,3'-Dichlorobenzidine BRL mg/kg dry 0.42 0.083 1 82700 7120/17 16:37 JMV P7G0259 3/4-Methylphenol BRL mg/kg dry 0.42 0.052 1 8270D 7120/17 16:37 JMV P71210259 4,6-Dinftn -2-methylphenol BRL mg/kg dry 0.42 0.063 1 8270D 7/20117 16:37 JMV P7G0259 4-Bromophenyl phenyl ether BRL mg/kg dry 0.42 0.072 1 8270D 7120/17 16:37 JMV P7G0259 4-Chloro-3-methylphenol BRL mg/kg dry 0.42 0.059 1 8270D 7120/17 16:37 JMV P7G0259 4-Chloroaniline, BRL mglkg dry 0.42 0.050 1 927013 7/20117 16:37 JMV P7G0259 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.42 0.054 1 8270D 7/20/17 16:37 JMV P7G0259 4-Nitrophenol BRL mg/kg dry 0.42 0.065 1 8270D 7120117 16:37 JMV P7G0259 Acensphthene BRL mg/kg dry 0.42 0.057 1 82701) 7/20/17 16:37 JMV P7G0259 Acenaphthylene BRL mg/kg dry 0.42 0.061 1 8270D 7120/17 16:37 JMV P7130259 Anthmcene BRL nrl dry 0.42 0.068 1 8270D 7/20117 16:37 JMV P7G0259 Azobenzene BRL mg/kg dry 0.42 0.055 1 9270D 7120/17 16:37 JMV P7G0259 Benzo(a)anthracene BRL mglkg dry 0.42 0.055 1 8270D 7/20117 16:37 JMV P7G0259 Benzo(a)pymne BRL mg/kg dry 0.42 0.045 1 82700 7/20117 16:37 JMV P7G0259 Benzo(b) luoranlhene BRL mg/kg dry 0.42 0.049 1 8270D 7/20/17 16:37 JMV P7G0259 Benzo(g,h,i)perylene BRL mg/kg dry 0.42 0.046 1 8270D 7/20/17 16:37 JMV P7G0259 Benzo(k)fluomnthene BRL mg8(g dry 0.42 0.055 1 B270D 7120/17 16:37 JMV P7130259 Benzoic Add BRL mg/kg dry 0.42 0.035 1 9270D 7120/17 16:37 JMV P7G0259 Benzyl alcohol BRL mg/kg dry 0.42 0.055 1 8270D 7/20117 16:37 JMV P7G0259 bis(2-Chloroethoxy)methene BRL mg/kg dry 0.42 0.073 1 8270D 7/20/17 16:37 JMV P7G0259 Bis(2-Chloroethy1)ether BRL mg/kg dry 0.42 0.059 1 8270D 7/20/17 16:37 JMV P7G0259 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.42 0.072 1 8270D 7/20/17 16:37 JMV P7G0259 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.42 0.062 1 8270D 7/20/17 16:37 JMV P7G0259 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-OS43 Phone: 7041529.6364 -Toll Free Number: 1-8001529-6364 -Fax: 7041525-0409 Page 23 Gf 50 R! S M I Fall-Servlce Analytical a weoenroe,es,w. Environmental Solutions Laboratory Report 07/31/2017 Geoscience Group Project: Truck Part Service Client Sample ID: GP-3 Attn: Tom Hassett Prism Sample ID: 7070278-07 500-K Clanton Rd. Prism Work Order: 7070278 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/17/17 14:24 Time Submitted: 07/17/1715:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Butyl benzyl phthalate BRL mglkg dry 0.42 0.060 1 6270D 7/20117 16:37 JMV P7430259 Chrysene BRL mg/kg dry 0.42 0.053 1 82700 7120/17 16:37 JMV P7130259 Dibenzo(a,h)anthracene BRL mg/kg dry 0.42 0.051 1 8270D 7120117 16:37 JMV P7G0259 Dilyamofuran BRL mglkg dry 0.42 0.064 1 8270D 7/20117 16:37 JMV P7G0259 Diethyl phthalate BRL mg/kg dry 0.42 0.058 1 8270D 7120/17 16:37 JMV P7130259 Dimethyl phthalate BRL mglkg dry 0.42 0.055 1 8270D 7/20/17 16:37 JMV P7G0259 Di-n-butyl phthalate BRL mg/kg dry 0.42 0.060 1 8270D 7120/17 16:37 JMV P7G0259 Di-n-octyl phthalate BRL mg/kg dry 0.42 0.052 1 8270D 7/20/17 16:37 JMV P7130259 Fluoramhene BRL mg/kg dry 0.42 0.053 1 8270D 7120/17 16:37 JMV P7430259 Fluorene BRL mg/kg dry 0.42 0.060 1 8270D 7120/17 16:37 JMV P7G0259 Hexechlorobenzene BRL mg/kg dry 0.42 0.067 1 8270D 7120117 16:37 JMV P7G0259 Hexachlorobutadiene BRL mg/kg dry 0.42 0.075 1 8270D 7/20/17 16:37 JMV P7130259 Hexechlomcyclopentediene BRL mg/kg dry 0.42 0.075 1 8270D 7/20/17 16:37 JMV P7130259 Hexachloroethane BRL mg/kg dry 0.42 0.070 1 8270D 7/20117 16:37 JMV P7G0259 Indeno(1,2,3-od)pyrene BRL mglkg dry 0.42 0.048 1 8270D 7/20/17 16:37 JMV P7G0259 Isophorone BRL mg/kg dry 0.42 0.057 1 8270D 7120/17 16:37 JMV P7130259 Naphthalene BRL mg/kg dry 0.42 0.067 1 8270D 7/20/17 16:37 JMV P7G0259 Nitrobenzene BRL mg/kg dry 0.42 0.060 1 8270D 7120117 16:37 JMV P7G0259 N-Nitroso-di-n-propNamine BRL mglkg dry 0.42 0.066 1 8270D 7/20/17 16:37 JMV P7G0259 N-Nitrosodiphenylamine BRL mg/kg dry 0.42 0.064 1 8270D 7/20117 16:37 JMV P7G0259 Pentachlomphenol BRL mg/kg dry 0.42 0.050 1 8270D 7120/17 16:37 JMV P7G0259 Phenenthrene BRL mg/kg dry 0.42 0.054 1 8270D 7120117 16:37 JMV P7G0259 Phenol BRL mglkg dry 0.42 0.062 1 8270D 7/20/17 16:37 JMV P7G0259 Pyrene BRL mg/kg dry 0.42 0.055 1 8270D 7/20/17 1637 JMV P7130259 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 81 % 39-132 2-Fluorobiphenyl 69 % 44-115 2-Fluorophenol 72 % 35-115 Nitrobenzened5 67 % 37.122 Phenol-d5 73 % 34-121 Terphenyl-dl4 93 % 54-127 Total Metals Hexavalent Chromium 1.3 mg/kg dry 0.52 0d7 1 '7196A 7124117 10:00 Bills P7G0274 Mercury 0.087 mg/kg dry 0.027 0.0026 1 '74718 7120/1711:60 JAB P7G0287 Arsenic BRL mg/kg dry 0.33 0.040 1 '6010D 7/24117 15:23 JAB P7G0320 Barium 21 mglkg dry 0.65 0.095 1 '60101) 7/21/17 20:37 JAB P7G0320 Cadmium BRL mg/kg dry 0.33 0.0087 1 '6010D 7/24117 15:23 JAB P7G0320 Chromium 38 mg/kg dry 0.33 0.054 1 '60101) 7121117 20:37 JAB P700320 Lead 6.5 mg/kg dry 0.33 0.060 1 '6010D 7121117 20:37 JAB P700320 Selenium 2.7 mg/kg dry 0.65 0.15 1 'BOtOD 7121117 20:37 JAB P7G0320 Silver BRL mg/kg dry 0.33 0.0081 1 '6010D 7/21117 20:37 JAB P7G0320 Volatile Organic Compounds by GC/MS This report should not be reproduced, except in its entirety, without the written consent of Pdsm Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Tali Free Number: l-000/529-6364- Fax: 70415254409 Page 24of50 PRISMFY1$eNCBA"a„�"a'x Laboratory Report Environmental 5o1allons uao4..roares +� 07/31/2017 Geoscience Group Project: Truck Part Service Client Sample ID: GP-3 Attn: Tom Hassett Prism Sample ID: 7070278-07 500-K Clanton Rd. Prism Work Order: 7070278 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/17/17 14:24 Time Submitted: 07/17/17 15:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0.0063 0.00052 1 8260B 7126/17 15:16 ANG P7G0413 1,1,1-Trichloroethane BRL mglkg dry 0.0063 0,00031 1 8260B 7/26117 15:16 ANG P7G0413 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0063 0.00043 1 8260B 7126/17 15:16 ANG P7G0413 1,1,2-Tdchloroethane BRL mg/kg dry 0.0063 0.00056 1 8260B 7/26117 15:16 ANG P7G0413 1,1-Dichloroethane BRL mg/kg dry 0.0063 0.00018 1 8260B 7126117 15:16 ANG P7G0413 1,1-Dichloroethylene BRL mg/kg dry 0.0063 0.00028 1 8260B 7126117 16:16 ANG P7G0413 1,1-Dichloropropylene BRL mg/kg dry 0.0063 0.00035 1 82608 7126/17 15:16 ANG P7G0413 1,2,3-Tdchlorobenzene BRL mg/kg dry 0.0063 0.00036 1 8260B 7/26/17 15:16 ANG P7G0413 1,2,3-Tdchloropropane BRL mg/kg dry 0.0063 0.00081 1 8260B 7/26117 15:16 ANG P7GD413 1,2,4-Tdchlorobenzene BRL mg/kg dry 0.0063 0.00047 1 8260B 7126/17 15:16 ANG P7G0413 1,2,4-Tdmethylbenzene BRL mg/kg dry 0.0063 0.00048 1 8260B 7/26117 15:16 ANG P7G0413 1,2-Dibromoethane BRL mg/kg dry 0.0063 0.00025 1 82608 7126/17 15:16 ANG P7G6413 1,2-Dichlombenzene BRL mg/kg dry 0,0063 0.00030 1 8260B 7/26/17 15:16 ANG P7GD413 1,2-Dichloroemane BRL mg/kg dry 0.0063 0.00038 1 8260B 7/26/17 15:16 ANG P7G0413 1,2-Dichloropropane BRL mg/kg dry 0.0063 0.00039 1 8260B 7/26/17 15:16 ANG P7GD413 1,3,5-Tdmethylbeozene BRL mg/kg dry 0,0063 0.00048 1 82608 7126/17 15:16 ANG P7G0413 1,3-Dichlorobenzene BRL mg/kg dry 0.0063 0.00042 1 8260B 7126117 15:16 ANG P7G0413 1,3-Dichloropropane BRL mg/kg dry 0.0063 0.00032 1 8260B 7126/17 15:16 ANG P7GD413 1,4-Dichlorobenzene BRL mg/kg dry 0.0063 0.00025 1 8260B 7126117 15:16 ANG P7G0413 2,2-Dichloropropane BRL mg/kg dry 0.0063 0.00030 1 8260B 7/26117 15:16 ANG P7G0413 2-Chlorotoluene BRL mg/kg dry 0.0063 0.00033 1 8260B 7/26117 15:16 ANG P7G0413 4-Chlorotoluene BRL mg/kg dry 0.0063 0.00038 1 8260B 7/26/17 15:16 ANG P7G0413 4-Isopropyltoluene BRL mg/1Sg dry 0.0063 0.00030 1 8260B 7/26117 15:16 ANG P7G0413 Acetone 0.048 J mglkg dry 0.063 0.0016 1 8260B 7/26117 15:16 ANG P7G0413 Benzene BRL mg/kg dry 0.0038 0.00037 1 8260B 7126/17 15:16 ANG P7G0413 Bromobenzene BRL mg/kg dry 0.0063 0.00053 1 8260B 7/26117 15:16 ANG P7G0413 Bromochloromethane BRL mg/kg dry 0.0063 0.00035 1 8260B 7126117 15:16 ANG P7G0413 Bromodichloromethane BRL mg/kg dry 0.0063 0.00035 1 82608 7/26/17 15:16 ANG P7G0413 Bromoform BRL mg/kg dry 0,0063 0.00072 1 8260B 7/26/17 15:16 ANG P7G0413 Bromomethene BRL mg/kg dry 0.013 0.00078 1 8260B 7126117 15:16 ANG P7G0413 Carbon Tetrachloride BRL mg/kg dry 0.0063 0.00031 1 82606 7/26/17 15:16 ANG P7G0413 Chlorobenzene BRL mg/kg dry 0.0063 0.00034 1 8260B 7/26/17 15:16 ANG P7G0413 Chlormthene BRL mg/kg dry 0.013 0.00053 1 8260B 7/26/17 15:16 ANG P7G0413 Chloroform BRL mg/kg dry 0.0063 0.00046 1 8260B 7126/17 15:16 ANG P7G0413 Chloromethane BRL mg/kg dry 0.0063 0.00043 1 8260B 7/26/17 15:16 ANG P7G0413 cis-12-Dichlorcethylene BRL mglkg dry 0.0063 0.D0027 1 8260B 7126/17 15:16 ANG P7G0413 cis-1,3-Dichloropropylene BRL mg/kg dry 0,0063 0.00021 1 8260B 7/26/17 15:16 ANG P7G0413 Dibromochloromethane BRL mg/kg dry 0.0063 0.00026 1 8260B 7126117 15:16 ANG P7G0413 DichlorodiIluoromethane BRL mg/kg dry 0.0063 0.00029 1 8260B 7/26/17 15:16 ANG P7G0413 Ethylbenzene BRL mg/kg dry 0.0063 0.00024 1 8260B 7/26/17 15:16 ANG P7G0413 Isopropyl Ether BRL mg/kg dry 0.0063 0.00026 1 8260B 7/26/17 15:16 ANG P7G0413 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0063 0.00037 1 8260B 7/26/17 15:16 ANG P7G0413 m,p-XAenes BRL mg/kg dry 0.013 0.00058 1 8260B 7/26/17 15:16 ANG P7G0413 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0643 Phone: 7041529-6364- Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Page 25 Gf 50 Laboratory Report PY' Full -Service Analytical 8 R I S M I enm.nnmemsi anmtions 07/31/2017 Geoscience Group Project: Truck Part Service Client Sample ID: GP-3 Attn: Tom Hassett Prism Sample ID: 7070278-07 500-K Clanton Rd. Prism Work Order: 7070278 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/17/17 14:24 Time Submitted: 07/17/17 15:45 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/rime Analyst Batch ID Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.063 0.00057 1 8260B 7126117 15:16 ANG P7G0413 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.13 0.00057 1 8260B 7/26/17 15:16 ANG P7G0413 Methyl Isobutyl Ketone BRL mg/kg dry 0.063 0.00054 1 8260B 7/26/17 15:16 ANG P7G0413 Methylene Chloride BRL mg/kg dry 0.013 0.00036 1 82606 7/26/17 15:16 ANG P7G0413 Methyl-tert-Butyl Ether BRL mg/kg dry 0.013 0.00020 1 8260B 7/26117 15:16 ANG P7130413 Naphthalene BRL mg/kg dry 0.013 0.00020 1 8260B 7/26/17 15:16 ANG P7130413 n-Butylbenzene BRL mg/kg dry 0.0063 0.00032 1 8260B 7/26/17 15:16 ANG P7130413 n-Propylbenzene BRL mg/kg dry 0.0063 0.00038 1 a260B 7/26/17 15:16 ANG P7130413 o-Xylene BRL mg/kg dry 0.0063 0.00026 1 8260B 7126117 15:16 ANG P7130413 sec-Butylbenzene BRL mg/kg dry 0.0063 0.00031 1 8260B 7/26/17 15:16 ANG P7130413 Styrene BRL mg/kg dry 0.0063 0.00038 1 8260B 7/26/17 15:16 ANG P7G0413 tert-Butylbenzene BRL mg/kg dry 0.0063 0.00021 1 8260B 7/26/17 15:16 ANG P7G0413 Tetrachlommthylene BRL mg/kg dry 0.0063 0.00030 1 8260B 7/26/17 15:16 ANG P7130413 Toluene BRL mg/kg dry 0.0063 0.00036 1 8260B 7126117 15:16 ANG P7G0413 trans-1,2.Dichloroethylene BRL mg/kg dry 0.0063 0.00038 1 8260B 7/26117 15:16 ANG P7130413 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0063 0.00033 1 8260B 7/26117 15:16 ANG P7130413 Trichloroethylene BRL mg*g dry 0.0063 0.00041 1 8260B 7126/17 15:16 ANG P7130413 Tdchloro8uoromethene BRL mg/kg dry 0.0063 0.00041 1 8260B 7/26/17 15:16 ANG P7G0413 Vinyl acetate BRL mg/kg dry 0.032 0.00087 1 8260B 7/26/17 15:16 ANG P7130413 Vinyl chloride BRL mg/kg dry 0.0063 0.00031 1 8260B 7/26/17 15:16 ANG P7130413 Xylenes, total BRL mg/kg dry 0.019 0.0012 1 8260B 7126117 15:16 ANG P7430413 Surrogate Recovery Control Limits 4-Bromolluorobenzene 102 % 70-130 Dibromolluoromethane 102 % 84-123 Toluene-da 96 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, INC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 1.8001529-6364 - Fax: 7041526-0409 Page 26 of 50 RISMI FU05erv1CM.1,0ca1& Laboratory Report En .o�men,a ao,ot o s 07/31/2017 Geoscienae Group Project: Truck Part Service Client Sample ID: GP4 Attn: Tom Hassett Prism Sample ID: 7070278-08 500-K Clanton Rd. Prism Work Order: 7070278 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/17/17 14:15 Time Submitted: 07/17/17 15:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID General Chemistry Parameters %Solids 79.9 %by 0.100 0.100 1 *SM2548G 7/18M7 14:30 JLB P760278 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.41 0.064 1 8270D 7/20117 16:59 JMV P7G0259 1,2-Dichlorobenzene BRL mg/kg dry 0.41 0.063 1 8270D 7120/17 16:59 JMV P7G0259 1,3-Dichlorobenzene BRL mg/kg dry 0.41 0.058 1 8270D 7/20/17 16:59 JMV P7G0259 1,4-Dichlorobenzene BRL mg/kg dry 0.41 0.060 1 8270D 7120117 16:59 JMV P7G0259 1-Methylnaphthalene BRL mg/kg dry 0.41 0.080 1 8270D 7/20/17 16:59 JMV P7G0259 2,4,6-Tdchfamphenol BRL mg/kg dry 0.41 0.077 1 8270D 7/20/17 16:59 JMV P7G0259 2,4-Dichlorophenol BRL mg/kg dry 0.41 0.080 1 8270D 7120/17 16:59 JMV P7G0259 2,4-Dimethylphenol BRL CCV mg/kg dry 0.41 0.063 1 B270D 7/20117 16:59 JMV P7G0259 2,4-Dinitrophenol BRL mg/kg dry 0.41 0.058 1 8270D 7/20117 16:59 JMV P7G0259 2,4-Dinitrotoluene BRL mg/kg dry 0.41 0.050 1 8270D 7120/17 16:59 JMV P7G0259 2,6-DinBrotoluene BRL mg/kg dry 0.41 0.055 1 8270D 7/20117 16:59 JMV P7G0259 2-Chloronaphthalene BRL mg/kg 9 k9 dry 0.41 0.060 1 8270D 7/20/17 16:59 JMV P7G0258 2-Chlorophenol BRL mg/kg dry 0.41 0.059 1 8270D 7120/17 16:59 JMV P7G0259 2-Methylnaphthalene BRL mg/kg dry 0.41 0.066 1 8270D 7/20117 16:69 JMV P7G0259 2-Methylphenol BRL mg/kg dry 0Al 0.053 1 8270D 7120117 16:59 JMV P7G0259 2-Nitrophenol BRL mg/kg dry 0.41 0.075 1 8270D 7120117 16:59 JMV P7G0259 3,3' 131chlorobenzidine BRL mg/kg dry 0.41 0.082 1 8270D 7/20117 16:59 JMV P7G0259 3/4-Methylphenol BRL mg/kg dry 0.41 0.051 1 82700 7120/17 16:59 JMV P7G0259 4,6-Dinttro-2-methylphenol BRL mg/kg dry 0.41 0.062 1 8270D 7/20117 16:59 JMV P7G0259 4-Bromophenyl phenyl ether BRL mg/kg dry 0.41 0.071 1 8270D 7120/17 16:59 JMV P7G0259 4-Chloro3-methylphenol BRL mg/kg dry 0.41 0.058 1 8270D 7/20/17 16:59 JMV P7G0259 4-Chloroaniline BRL mg/kg dry 0.41 0.050 1 8270D 7/20/17 16:59 JMV P7G0259 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.41 0.054 1 8270D 7120117 16:59 JMV P7G0259 4-Nitrophenol BRL mg/kg dry 0.41 0.064 1 8270D 7/20117 16:59 JMV P7G0259 Acenaphthene BRL mg/kg dry 0.41 0.056 1 8270D 7120117 16:59 JMV P7G0259 Acenaphthylene BRL mg/kg dry 0.41 0.060 1 8270D 7/20117 16:59 JMV P7G0259 Anthracene BRL mg/kg dry 0.41 0.067 1 8270D 7/20/17 16:59 JMV P7G0259 Azobenzene BRL mg/kg dry 0.41 0.055 1 8270D 7120117 16:59 JMV P7G0259 Senzo(a)anthmcene BRL m /k 9 9 dry 0.41 0.054 i 8270D 7/20H7 16:59 JMV P7G0259 Benzo(a)pyrene BRL mg/kg dry 0.41 0.D45 1 8270D 7/20/17 16:59 JMV P7G0259 Benzo(b)fluoranthene BRL mg/kg dry 0.41 0.048 1 8270D 7/20117 16:59 JMV P7G0259 Benzo(g,h,i)perylene BRL mg/kg dry 0.41 0.045 1 8270D 7/20/17 16:59 JMV P7G0259 Benzo(k)fluoranthene BRL mg/kg dry 0.41 0.054 1 8270D 7/20/17 16:59 JMV P7G0259 Benzoic Acid BRL mg/kg dry 0.41 0.035 1 8270D 7/20/17 16:59 JMV P7G0259 Benzyl alcohol BRL mg/kg dry 0.41 0.054 1 8270D 7/20/17 16:59 JMV P7G0259 bis(2-Chlorcethoxy)methane BRL mg/kg dry 0.41 0.072 1 6270D 7/20/17 16:59 JMV P7G0259 Bls(2-Chloroethyl)ether BRL mg/kg dry 0.41 0.058 1 8270D 7120/17 16:59 JMV P7G0259 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0A1 0.071 1 9270D 7120/17 16:59 JMV P7G0259 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.41 0.061 1 8270D 7/20117 16:59 JMV P7G0259 This report should not be reproduced, except in its enOrety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, INC 28224-0543 Phone: 704/529-0364 - Toll Free Number: 1.8001529.6364 - Fax: 7041525-0409 Page 27 of 50 k. Full -Service Analytical b egR ISM I Environmental Solutions Laboratory Report 07/31/2017 Geoscience Group Project: Truck Part Service Client Sample ID: GP4 Attn: Tom Hassett Prism Sample ID: 7070278-08 500-K Clanton Rd. Prism Work Order: 7070278 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/17/17 14:15 Time Submitted: 07/17/17 15:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Butyl benzyl phthalate BRL mg/kg dry 0.41 0.059 1 8270D 7/20117 16:59 JMV P7130259 Chrysene BRL mg/kg dry 0.41 0.052 1 8270D 7/20/17 16:59 JMV P7130259 Dibenzo(a,h)anthracene BRL mglkg dry 0.41 0.050 1 8270D 7120117 16:59 JMV P7130259 Dibenzofuran BRL mg/kg dry 0.41 0.063 1 8270D 7/20117 16:59 JMV P7130259 Diethyl phthalate BRL mg/kg dry 0.41 0.057 1 8270D 7120/17 16:59 JMV P7130259 Dimethyl phthalate BRL mg/kg dry 0.41 0.055 1 8270D 7/20117 16:59 JMV P7G0259 Di-n-butyl phthalate BRL mg/kg dry 0.41 0.059 1 8270D 7120/17 16:59 JMV P7130259 Di-n-octyl phthalate BRL mg/kg dry 0.41 0.051 1 8270D 7/20117 16:59 JMV P7G0259 Fluoranthene BRL mglkg dry 0.41 0.053 1 8270D 7120117 16:59 JMV P7G0259 Fluorene BRL mg/kg dry 0A1 0.059 1 8270D 7/20/17 16:59 JMV P7G0259 Hexachlorobenzens BRL mg/kg dry 0.41 0.066 1 8270D 7/20/17 16:59 JMV P7G0259 Hexachlorobutediene BRL mg/kg dry 0.41 0.074 1 8270D 7/20/17 16:59 JMV P7130259 Hexachlorocydopentadiene BRL mg/kg dry 0.41 0.074 1 827013 7120/17 16:59 JMV P7G0259 Hexachloroethane BRL mg/kg dry 0.41 0.069 1 8270D 7120117 16:59 JMV P7130259 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.41 0.047 1 8270D 7120/17 16:59 JMV P7130259 Isophorone BRL mg/kg dry 0.41 0.056 1 82700 7/20/17 16:59 JMV P7130259 Naphthalene BRL mglkg dry 0.41 0.066 1 8270D 7/20117 16:59 JMV P7130259 Nitrobenzene BRL mg/kg dry 0.41 0.059 1 8270D 7120/17 16:59 JMV P7G0259 N-Nitroso-all-n-propylamine BRL mg/kg dry 0.41 0.065 1 8270D 7/20117 16:59 JMV P7130259 N-Nitrosodiphenylamine BRL mg/kg dry 0.41 0.063 1 8270D 7/20/17 16:59 JMV P7130259 Pentachlorophenol BRL mg/kg dry 0.41 0.049 1 8270D 7/20/17 16:59 JMV P7G0259 Phenanthrene BRL mg/kg dry 0.41 0.054 1 8270D 7/20/17 16:59 JMV P7G0259 Phenol BRL mg/kg dry 0.41 0.061 1 8270D 7120/17 16:59 JMV P7430259 Pyrene BRL mglkg dry 0.41 0.055 1 8270D 7/20117 16:59 JMV P7G0259 Surrogate Recovery Control Limits 2A.6-Tribromophenol 81 % 39-132 2-Fluorobiphenyl 89 % 44-116 2-Fluorophenol 72 % 35-115 Nitrobenzened5 66 % 37-122 Phenold5 72 % 34-121 Terphenyl-d14 93 % 54-127 Total Metals Hexavalent Chromium 0.55 mg/kg dry 0.49 0.16 1 '7196A 7124/17 10:00 BMS P7G0274 Mercury BRL mg/kg dry 0.023 0.0022 1 '7471B 7120/1711:55 JAB P7430287 Arsenic 0.77 mg/kg dry 0.31 0.038 1 '6010D 7124/17 15:33 JAB P7G0320 Barium 16 mgikg dry 0.62 0.091 1 '60101) 7/21/17 20:47 JAB P7130320 Cadmium BRL mg/kg dry 0.31 0.0083 1 '6010D 7/24/17 15:33 JAB P7130320 Chromium 9.0 mgtkg dry 0.31 0.052 1 '6010D 7121117 20:47 JAB P7G0320 Lead 4.0 mg/kg dry 0.31 0.05E 1 '6010D 7121117 20:47 JAB P700320 Selenium BRL mg/kg dry 0.62 0.15 1 '6010D 7121117 20:47 JAB P7130320 Silver BRL mg/kg dry 0.31 0.0077 1 '6010D 7/21/17 20:47 JAB P7G0320 Volatile Organic Compounds by GUMS This report should not be reproduced, except in its enOrety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 29224-0543 Phone: 7041529-0364-Toll Free Number: l-8001529.6364- Fax: 7041525-0409 Page 28 of50 PRISM FWi-Servicepnal ica18 Laboratory Report Environmental Solutions aemmn,Ex, n 07/3112017 Geoscience Group Project: Truck Part Service Client Sample ID: GP-4 Attn: Tom Hassett Prism Sample ID: 7070278-08 500-K Clanton Rd. Prism Work Order: 7070278 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/17/17 14:15 Time Submitted: 07117117 15:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/rime ID 1,1,1,2-Tetrachlomethene BRL mg/kg dry 0.0071 0.00058 1 8260B 7/26/17 15:43 ANG P7G0413 1,1,1-Trichloroethane BRL mglkg dry 0.0071 0.00034 1 8260B 7/26/17 15:43 ANG P7G0413 1,1,2,2-Tetrachlomethane BRL mg/kg dry 0.0071 0.00048 1 8260B 7126117 15:43 ANG P7G0413 1,1,2-Trichloroethane BRL mg/kg dry 0.0071 0.00063 1 8260B 7/26/17 15:43 ANG P7G0413 1,1-Dichlomethane BRL mg/kg dry 0.0071 0.00020 1 8260B 7/26/17 15:43 ANG P7G0413 1,1-Dichloroethylene BRL mglkg dry 0.0071 0.00031 1 8260B 7126/17 15:43 ANG P7G0413 1,1-Dichlompmpylene BRL mg/kg dry 0.0071 0.00039 1 8260B 7/26/17 15:43 ANG P7G0413 1,2,3-Tdchlombemene BRL mg/kg dry 0.0071 0.00040 1 8260B 7/26/17 15:43 ANG P7G0413 1,2,3-Trichloropropane BRL mg/kg dry 0.0071 0.00090 1 82608 7126/17 15:43 ANG P7G0413 1,2,4-Tichoorobenzene BRL mglkg dry 0.0071 0.00053 1 8260B 7/26/17 15:43 ANG P7G0413 1,2,4-Trimethylbemene BRL mg/kg dry 0.0071 0.00054 1 8260B 7126117 15:43 ANG P7G0413 1,2-Dibromoethane BRL mg/kg dry 0.0071 0.00028 1 8260B 7/26/17 15:43 ANG P7G0413 1,2-Dichlorobenzene BRL mglkg dry 0.0071 0.00033 1 8260B 7/26117 15:43 ANG P7G0413 1,2-Dichloroethane BRL mg/kg dry 0.0071 0.00042 1 8260B 7126117 15:43 ANG P7G0413 1,2-Dichloropropane BRL mglkg dry 0.0071 0.000" 1 8260B 7126/17 15:43 ANG P7G0413 1,3,5-Trimethylbenzene BRL mg/kg dry 0.0071 0.00053 1 8260B 7/26/17 15:43 ANG P7G0413 1,3-Dichlorobenzene BRL mg/kg dry 0.0071 0.00047 i 8260B 7/26/17 15.43 ANG P7G0413 1,3-Dichloropropane BRL mg/kg dry 0.0071 0.00035 1 82608 7/26/17 15:43 ANG P7G0413 1,4-Dichlorobenzene BRL mg/kg dry 0.0071 0.00028 1 8260B 7/26/17 15:43 ANG P7G0413 2,2-Dichloropropane BRL mg/kg dry 0.0071 0.00034 1 8260B 7126/17 16:43 ANG P7G0413 2-Chlomtoluene BRL mg/kg dry 0,0071 0.00036 1 8260B 7/26117 15:43 ANG P7G0413 4-Chlomtoluene BRL mg/kg dry 0,0071 0.00042 1 8260B 7/26/17 15:43 ANG P7G0413 4-Isopropyltoluene BRL mg/kg dry 0.0071 0.00034 1 8260B 7/26117 15:43 ANG P7G0413 Acetone BRL mg/kg dry 0,071 0.0017 1 8260B 7126/17 15:43 ANG P7G0413 Benzene BRL mg/kg dry 0.0042 0.00041 1 8260B 7/26117 15:43 ANG P7G0413 Bromobenzene BRL mglkg dry 0.0071 0.00059 1 8260B 7126/17 15:43 ANG P7G0413 Bromochloromethane BRL mg/kg dry 0.0071 0.00039 1 8260B 7/26/17 15:43 ANG P7G0413 Bromodichloromethane BRL mg/kg dry 0.0071 0.00039 1 8260B 7126/17 15:43 ANG P7G0413 Bromoform BRL mg/kg dry 0.0071 0.00060 1 8260B 7126/17 15:43 ANG P7G0413 Bromomethane BRL mg/kg dry 0.014 0.00087 1 826013 7/26/17 15:43 ANG P7G0413 Carbon Tetrachloride BRL mglkg dry 0.0071 0.00035 1 8260B 7126117 15:43 ANG P7G0413 Chlombenzene BRL mg/kg dry 0.0071 0.00037 1 8260B 7126/17 15:43 ANG P7G0413 Chloroethane BRL mg/kg dry 0.014 0.00059 1 8260B 7/26/17 15:43 ANG P7G0413 Chloroform BRL mg/kg dry 0.0071 0.00051 1 8260B 7/26/17 15:43 ANG P7G0413 Chloromethane BRL mg/kg dry 0.0071 0.00047 1 82608 7/26/17 15:43 ANG P7G0413 cis-1,2-Dichlomethylene BRL mg/kg dry 0.0071 0.00030 1 8260B 7126/17 15:43 ANG P7G0413 cis-1,3-Dichlompropylene BRL mg/kg dry 0.0071 0.00024 1 8260B 7/26/17 15:43 ANG P7G0413 Dibromochlommethane BRL mg/kg dry 0.0071 0.00029 1 8260B 7/26117 15:43 AND P7G0413 Dichlorodi8uoromethane BRL mg/kg dry 0.0071 0.00032 1 8260B 7/26/17 15:43 ANG P7G0413 Ethylbenzene BRL mg/kg dry 0.0071 0.00027 1 8260B 7126/17 15:43 ANG P7G0413 Isopropyl Ether BRL mg/kg dry 0.0071 0.00029 1 8260B 7/26/17 15:43 ANG P7G0413 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0071 0.00042 1 8260B 7/26/17 16:43 ANG P7G0413 m,p-Xylenes BRL mg/kg dry 0.014 0.00065 1 8260B 7126/17 15:43 ANG P7G0413 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Read - P.O. Box 240543 - Charlotte, NC 29224-0643 Phone: 7041529-6364 - Toll Free Number: l-8001529.6364- Fax: 7041526-0400 Page 29 of 50 Full-Serviee Laboratory Report Analytical 6 P S M Emtronmentai smmio"a �C's 07/31/2017 Geoscience Group Project: Truck Part Service Client Sample ID: GP-4 Attn: Tom Hassett Prism Sample ID: 7070278-08 500-K Clanton Rd. Prism Work Order: 7070278 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 07/17/17 14:15 Time Submitted: 07/17/17 15:45 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/rime Analyst Batch ID Methyl Butyl Ketone (2-He canon) BRL ni dry 0.071 0.00064 1 8260B 7126/17 15:43 ANG P7G0413 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.14 0.00064 1 8260B 7/26/17 16:43 ANG P7130413 Methyl Isobutyl Ketone BRL mg/kg dry 0.071 0.00060 1 8260B 7126/17 15:43 ANG P7G0413 Methylene Chloride BRL mg/kg dry 0.014 0.00040 1 8260B 7/26/17 15:43 ANG P7GD413 Methyl-tert-Butyl Ether BRL mg/kg dry 0.014 0.00023 1 8260B 7/26117 15:43 ANG P7G0413 Naphthalene BRL ni dry 0.014 0.00022 1 8260B 7126/17 15:43 ANG P7130413 n-Butylbenzene BRL mg29 dry 0.0071 0.00036 1 8260B 7126/17 15:43 ANG P7G0413 n-Propylbenzene BRL mgtkg dry 0.0071 0.00042 1 8260B 7/26/17 15:43 ANG P7G0413 o-Xylene BRL mg/kg dry 0.0071 0.00029 1 8260B 7/26/17 15:43 ANG P7130413 sec-Butylbenzene BRL mg1kg dry 0.0071 0.00034 1 8260B 7/26/17 15:43 ANG P7G0413 Styrene BRL mg/kg dry 0.0071 0.00043 1 8260B 7/26/17 15:43 ANG P7G0413 tert-Butylbenzene BRL mg/kg dry 0.0071 0.00024 1 8260B 7/26/17 15:43 ANG P7GD413 Tetrachloroethylene BRL mg/kg dry 0.0071 0.00034 1 82608 7/26/17 15:43 ANG P7130413 Toluene BRL mg/kg dry 0.0071 0.00041 1 8260B 726117 15:43 ANG P7G0413 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0071 0.00042 1 8260B 7/26117 15:43 ANG P7G0413 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0071 0.00037 1 8260B 7126/17 15:43 ANG P7G0413 Tdchlorcelhylene BRL ni dry 0.0071 0.00046 1 82608 7126117 15:43 ANG P7G0413 Trichlomfluoromethane BRL mgfkg dry 0,0071 0.00046 1 8260B 7126/17 15:43 ANG P7130413 Vinyl acetate BRL mglkg dry 0.035 0.00097 1 8260B 7/26117 15:43 ANG P7G0413 Vinyl chloride BRL mg/kg dry 0.0071 0.00034 1 82608 726/17 15:43 ANG P7G0413 Xylenes, total BRL mglkg dry 0.021 0.0013 1 8260B 7/26/17 15:43 ANG P7G0413 Surrogate Recovery Control Limits 4-Bromolluorobenzene 101 % 70-130 Dibromofluoromethane 104 % 84-123 Toluene-d8 96 % 76-129 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 26224-0543 Phone: 7041529.6364 - Toll Free Number: 1.800/529-6364 - Fax: 7041525-0409 Page 30 of 50 3=n^� IS I� �I I E- iService al 8lytkel s >~• ' V I Environmental Solutions s�?, uaoA.,eq,�,.e Geoscienoe Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GCIMS - Quality Control Analyte Batch MOM - 5035 Reporting Result Limit Units Level II QC Report 7/31/17 Prism Work Order: 7070278 Time Submitted: 7/17/2017 3:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P7GO413-BLK7) Prepared $ Analyzed: 07/26/17 1, 1, 1,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,1-Trichloroethane BRL 0.0050 mg/kg wet 1,1,2,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,2-Tdchlorcethane BRL 0.0050 mg/kg wet 1,1-Dichlorcethane BRL 0.0050 mg/kg wet 1,1-Dichloroethylene BRL 0.0050 mg/kg wet 1,1-Dichloropropylene BRL 0.0050 mg/kg wet 1,2,3-Tdchlorobemene BRL 0.0050 mg/kg wet 1,2,3-Tdchloropmpane BRL 0.0050 mg/kg wet 1,24-Tdchlorobenzene BRL 0.0050 mg/kg wet 1,2,4-Tdmethylbenzene BRL 0.0050 mg/kg wet 1,2-Dibromoethans BRL 0.0050 mg/kg wet 1,2-Dichlorobenzene BRL 0.0050 mg/kg wet 1,2-Dichloroethene BRL 0.0050 mg/kg wet 1,2-Dichloropropane BRL 0.0050 mg/kg wet 1,3,5-Tdmethylbenzene BRL 0.0050 mg/kg wet 1,3-Dichlorobenzene BRL 0.0050 mg/kg wet 1,3-Dichloropropane BRL 0.0050 mg/kg wet 1,4-Dichlorobenzene BRL 0.0050 mg/kg wet 2,2-Dichloropropane BRL 0.0050 mg/kg wet 2-Chlorotoluene BRL 0.0050 mg/kg wet 4-Chlorotoluene BRL 0.0050 mg/kg wet 4-Isopropyltoluene BRL 0.0050 mg/kg wet Acetone BRL 0.050 mg/kg wet Benzene BRL 0.0030 mg/kg wet Bromobenzene BRL 0.0050 mg/kg wet Bromochloromethane BRL 0.0050 mg/kg wet Bromodichloromeatane BRL 0.0050 mg/kg wet Bromoform BRL 0.0050 mg/kg wet Bromomethane BRL 0,010 mg/kg wet Carbon Tetrachloride BRL 0.0050 mg/kg wet Chlorobenzene BRL 0.0050 mg/kg wet Chlomethane BRL 0.010 mg/kg wet Chloroform BRL 0.0050 mg/kg wet Chloromethene BRL 0.0050 mg/kg wet cis-1,2-Dichloroethylene BRL 0,0050 mg/kg wet cis-1,3-Dichloropropylene BRL 0.0050 m9/k9 wet Dibromochloromethans BRL 0.0050 mg/kg wet Dichlorodi0uommethane BRL 0.0050 mg/kg wet Ethylbenzene BRL 0.0050 mg/kg wet Isopropyl Ether BRL 0.0050 mg/kg wet Isopropylbemene (Cumene) BRL 0.0050 mg/kg wet m,p-Xylenes BRL 0.010 mg/kg wet Methyl Butyl Ketone (2-Hexanone) BRL 0,050 mg/kg wet Methyl Ethyl Ketone (2-Butanone) BRL 0.10 mg/kg wet Methyl Isobutyl Ketone BRL 0.050 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spdngbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toll Free Number: 1-9001529-6364 - Fax: 7041525-0409 Page 31 of 50 Full-S PRISM I Environmental rvlce al Solutions s Environmental Solutions `uawuropres ixc Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GCIMS - Quality Control Analyte Reporting Result Limit Units Level II QC Report 7/31/17 Prism Work Order: 7070278 Time Submitted: 7/17/2017 3:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P7130413 - 5035 Blank (P7GO413-BLKI) Prepared $ Analyzed: 07/26/17 Methylene Chloride BRL 0.010 mg/kg wet Methyl-tert-Butyl Ether BRL 0.010 mg/kg wet Naphthalene BRL 0.010 mg/kg wet n-Butylbenzene BRL 0.0050 mg/kg wet n-Propylbenzene BRL 0.0050 mg/kg wet o-Xylene BRL 0.0050 mg/kg wet seo-Butylbenzene BRL 0.0050 mg/kg wet Styrene BRL 0.0050 mg/kg wet tert-Butylbenzene BRL 0.0050 mglkg wet Tetrachloroethylene BRL 0.0050 mg/kg wet Toluene BRL 0.0050 mg/kg wet trans-1,2-Dichloroethylene BRL 0.0050 mglkg wet trans-1,3-Dichloropropylene BRL 0.0050 mg/kg wet Trichlomethylene BRL 0.0050 mg/kg wet Trichloro0uoromethane BRL 0.0050 mg/kg wet Vinyl acetate BRL 0.025 mg/kg wet Vinyl chloride BRL 0.0050 mg/kg wet Xylenes, total SRL 0.015 mg/kg wet Surrogate: 4-Bmmofluombenzene 51.4 u91L W.00 103 70-130 Surrogate: Dibromofluoromethane 50.8 u91L 50.00 102 84-123 Surrogate: Toluene-18 48.2 u91L 50.00 96 76-129 LCS (P7GO413-BSI) Prepared 8 Analyzed: 07/26I17 1,1,1,2-Tetrachloroethane 0.0438 0.0050 mg/kg wet 0.05000 88 72-115 1,1,1-Tdchlorcethane 0.0448 0.0050 mglkg wet 0.05000 90 67-131 1,1,2,2-Tebachloroethane 0.0434 0.0050 mg/kg wet 0.05000 87 56-126 1,1,2-Trichlomethane 0.0437 0.0050 mg/kg wet 0.05000 87 70-133 1,1-Dichloroethane 0.0465 0.0060 mglkg wet 0.05000 93 74-127 1,1-Dichloroethylene 0.0460 0.0050 mg/kg wet 0.05000 92 67-149 1,1-Dichloropropylene 0.0438 0.0050 mg/kg wet 0.05000 88 71-130 1,2,3-Trichlorobenzene 0.0480 0.0050 mg/kg wet 0.05000 96 68-130 1,2,3-Tdchloropropane 0.0415 0.0050 mg/kg wet 0.05000 83 60-137 1,2,4-Trichlorobemene 0.0453 0.0050 ni wet 0.05000 91 66-125 1,2,4-Trimethylbenzene 0.0457 0.0050 mg/kg wet 0.05000 91 69-129 1,2-Dibromoethane 0.0471 0.0050 mg/kg wet 0.06000 94 70-132 1,2-Dichlorobenzene 0.0458 0.0050 mg/kg wet 0.05000 92 72-123 1,2-Dichloroethane 0.0447 0.0050 mg/kg wet 0.05000 89 68-128 1,2-Dichloropmpane 0.0452 0.0050 mg/kg wet 0.05000 90 73-130 1,3,5-Trimethylbenzene 0.0453 0.0050 mg/kg wet 0.05000 91 69-128 1,3-Dichlorobemene 0.0450 0.0050 mg" wet 0.05000 90 71-120 1,3-Dichloropropane 0.0424 0.0050 ni wet 0.05000 85 75-124 1,4-Dichlombemene 0.0443 0.0050 mg/kg wet 0.06000 89 71-123 2,2-Dichloropropane 0.0462 0.0050 mglkg wet 0.05000 92 50-142 2-Chlorololuene 0.0453 0.0050 mg/kg wet 0.05000 91 67-124 4-Chlorotoluene 0.0445 0.0050 mg/kg wet 0.05000 89 71-126 4-Isopropyltoluene 0.0463 0.0050 ni wet 0.05000 93 68-129 Acetone 0.0997 0.050 mg/kg wet 0.1000 100 29-198 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spdngbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/52g-6364 - Fax: 704/5254409 Page 32 of 50 P R I S I� /I cuu se me anainicei a roq'EeV�' Envrzonmental Solutions Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GC/MS - Quality Control Analyte Reporting Result Limit Units Level II QC Report 7/31/17 Prism Work Order: 7070278 Time Submitted: 7/17/2017 3:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P7G0413 - 5035 LCS (P7G041343SI) Prepared & Analyzed: 07/26117 Benzene 0.0462 0.0030 mg/kg wet 0.05000 92 74-127 Bromobenzene 0.0440 0.0050 mg/kg wet 0.05000 88 73-125 Bromochloromethene 0.0448 0.0050 mg/kg wet 0.05000 90 72-134 Bromodichloromethene 0.0469 0.0050 mg/kg wet 0,05000 94 75-122 Bromofonn 0.0447 0.0050 mg/kg wet 0.05000 89 66-135 Bromomethane 0.0566 0.010 mg/kg wet 0.05000 113 20-180 Carbon Tetmchlonde 0.0473 0.0050 mg/kg wet 0.05000 95 64-143 Chlorobenzene 0.0446 0.0050 mg/kg wet 0.05000 89 74.118 Chloroethane 0.0656 0.010 mg/kg wet 0.05000 131 33-149 Chloroform 0.0456 0.0050 mg/kg wet 0.05000 91 73-127 Chlommethene 0.0538 0.0050 mg/kg wet 0.05000 108 45-143 cis-1,2-Dichloroethylene 0.0458 0.0050 mg/kg wet 0.05000 92 76-134 cis-1,3-Dichloropropylene 0.0461 0.0050 mg/kg wet 0.05000 92 71-125 Dibromochloromethane 0.0445 0,0050 mg/kg wet 0.05000 89 73-122 Dichlorodi8uoromethane 0.0641 0.0050 mg/kg wet 0.05000 128 26-146 Ethylbenzene 0.0449 0.0050 mg/kg wet 0.05000 90 74-128 Isopropyl Ether 0.0460 0.0050 mg/kg wet 0.05000 92 59-159 Isopropylbenzene (Cumene) 0.0444 0.0050 mg/kg wet 0.05000 89 68-126 m,p-Xylenes 0.0912 0.010 mg/kg wet 0.1000 91 75-124 Methyl Butyl Ketone (2-Hexanone) 0.0473 0.050 mg/kg wet 0.05000 95 61-157 Methyl Ethyl Ketone (2-Butanone) 0.0463 0.10 mg/kg wet 0.05000 93 J 63-149 Methyl Isobulyl Ketone 0.0479 0.050 mg/kg wet 0.05000 96 ,1 57-162 Methylene Chloride 0.0440 0.010 mg/kg wet 0.05000 88 74-129 Methyl -tent -Butyl Ether 0.0512 0.010 mg/kg wet 0.05000 102 70-130 Naphthalene 0.0481 0.010 mg/kg wet 0.05000 96 57-157 n-Butylbenzene 0.0466 0.0050 mg/kg wet 0.05000 93 65-135 n-Propylbenzene 0.0443 0.0050 mg/kg wet 0.05000 89 67-130 o-Xylene 0.0447 0.0050 mg/kg wet 0.05000 89 74-126 sec-Bulylbenzene 0.0446 0.0050 mg/kg wet 0.05000 89 66-131 Styrene 0.0468 0.0050 mg/kg wet 0.05oo0 94 77-121 tert-Buylbenzene 0.0434 0.0050 mg/kg wet 0.05000 87 67-132 Temachloroethylene 0.0432 0.0050 mg/kg wet 0.05000 86 68-130 Toluene 0.0464 0.0050 mg/kg wet 0.05000 93 71-129 trans-1,2-Dichloroethylene 0.0465 0.0050 mg/kg wet 0.05000 93 73.132 trans-1,3-Dichloropmpylene 0.0450 0.0050 mg/kg wet 0.05000 90 68-123 Tdchloroethylene 0.0443 0.0050 mg&g wet 0,05000 89 75-133 Trichlorofluoromethane 0.0530 0.0050 mg/kg wet 0.05000 106 44-146 Vinyl acetate 0.0536 0.025 mg/kg wet 0.05000 107 85-161 Vinyl chloride 0.0573 0.0050 mg/kg wet 0.05000 115 48-147 Xylenes, total 0.136 0.015 mg/kg wet 0.1500 91 74-126 Surrogate: 4-Bromofluorobenzene 48.8 ug/L 50.00 98 70-130 Surrogate: Dibromofluoromethane 49.6 00 50.00 99 84-123 Surrogate: Toluene-18 48.0 091L 50.00 96 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 29224-0543 Phone: 704/529E364-Toll Free Number: 1-8001529-6364- Fax: 7041525.0409 Page33of50 �P:R f S M l rnii aer�,oe nnsiymcsi 4 Envponmanlel Solutions �_\ UBw TorIE 1 C Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GCIMS - Quality Control Analyte Reporting Result Limit Units Level H QC Report 7131/17 Prism Work Order: 7070278 Time Submitted: 7/17/2017 3:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P7GO413 - 5035 LCS Dup (P7GO41343SD1) Prepared & Analyzed: 07/26/17 1,1,1,2-Tetrachlomathane 0.0443 0.0050 mg/kg wet 0.05000 89 72-115 1 20 1,1,1-Tdchloroethane 0,0426 0.0050 mg/kg wet 0.05000 85 67-131 5 20 1,1,2,2-Tetrachloroethane 0.0445 0A050 mg/kg wet 0.05000 89 56-126 3 20 1,1,2-Trichlomethane 0.0436 0.0050 mg/kg wet 0.05000 87 74133 0.2 20 1,1-Dichlomethane 0.0444 0.0050 mg/kg wet 0.05000 89 74-127 5 20 1,1-Dichloroethylene 0.0442 0.0050 mg/kg wet 0.05000 88 67-149 4 20 1,1-Dichloropropylene 0.0422 0.0050 mg/kg wet 0.05000 84 71-130 4 20 1,2,3-T6chlorobenzene 0.0470 0.0050 mg/kg wet 0.05000 94 68-130 2 20 1,2,3-Tdchlompropane 0.0435 0.0050 mg/kg wet 0.05000 87 60-137 5 20 1,2,4-Tdchlorobenzene 0.0448 0.0050 mg/kg wet 0.05000 90 66-125 1 20 1,2,4-Tdmethylbenzene 0.0455 0.0050 mg/kg wet 0.05000 91 69-129 0.4 20 1,2-Dibromcethane 0.0483 0.0050 mg/kg wet 0.05000 97 70-132 3 20 1,2-Dichlorobenzene 0.0456 0.0050 mg/kg wet 0.05000 91 72-123 0.6 20 1,2-Dichloroethane 0.0443 0.0050 mg/kg wet 0.05000 89 68-128 0.9 20 1,2-Dichlompropane 0.0444 0.0050 mg/kg wet 0.05000 89 73-130 2 20 1,3,5-7rimethylbenzene 0.0449 0.0050 mg/kg wet 0.05000 90 69-128 1 20 1,3-Dichlorobenzene 0.0443 0,0050 mg/kg wet 0.05000 89 71-120 2 20 1,3-Dichloropropane 0.0436 0.0050 mg/kg wet 0.05000 87 75-124 3 20 1,4-Dichlorobenzene 0.0436 0.0050 mg/kg wet 0.05000 87 71-123 2 20 2,2-Dichloropropane 0.0450 0.0050 mg/kg wet 0.05000 90 50-142 3 20 2-Chlorotoluene 0.0447 0.0050 mg/kg wet 0.05000 89 67-124 1 20 4-Chlorotoluene 0.0444 0.0050 mg/kg wet 0.05000 89 71-126 0.3 20 4-Isopropyholuene 0.0451 0.0050 mg/kg wet 0.05000 90 68-129 2 20 Acetone 0.103 0.050 mg/kg wet 0.1000 103 29-198 4 20 Benzene 0.0460 0.0030 mg/kg wet 0.05000 90 74-127 3 20 Bromobenzene 0.0442 0.0050 mg/kg wet 0.05000 88 73-125 0.4 20 Bromochloromethane 0.0432 0.0050 mg/kg wet 0.05000 86 72-134 4 20 Bromodichlommethane 0.0465 0.0050 mg/kg wet 0.05000 93 75-122 0.8 20 Bromofonn 0.0463 0.0050 mg/kg wet 0.05000 93 66-135 4 20 Bromomethane 0.0509 0.010 mg/kg wet 0.05000 102 20-180 10 20 Carbon Tetrachloride 0.0454 0.0050 mg/kg wet 0.05000 91 64-143 4 20 Chlorobenzene 0.0447 0.0050 mg/kg wet 0.05000 89 74-118 0.2 20 Chloroethane 0.0597 0.010 mg/kg wet 0.05000 119 33-149 9 20 Chloroform 0.0445 0.0050 mg/kg wet 0.05000 89 73-127 2 20 Chloromethane 0.0481 0.0050 mg/kg wet 0.05000 96 45-143 11 20 cis-1,2-Dichloroethylene 0,0450 0.0050 mg/kg wet 0.05000 90 76-134 2 20 cis-1,3-Dichloropropylene 0.0457 0.0050 mg/kg wet 0.05000 91 71-125 0.9 20 Dibromochloromethane 0.0464 0.0050 mg/kg wet 0.05000 93 73-122 4 20 Dichlorodi0uoromethane 0.0589 0.0050 mg/kg wet 0.05000 118 26-146 8 20 Ethylbenzene 0.0443 0.0050 mg/kg wet 0.05000 89 74-128 2 20 Isopropyl Ether 0.0457 0.0050 mg/kg wet 0.05D00 91 59-159 0.7 20 Isopropylbenzene (Cumene) 0.0438 0.0050 mg/kg wet 0.05000 88 68-126 1 20 m,p-Xylenes 0.0894 0.010 mg/kg wet 0.1000 89 75124 2 20 Methyl Butyl Ketone (2-Hexanone) 0.0493 0.050 mg/kg wet 0.05000 99 61-157 4 20 J Methyl Ethyl Ketone (2-Butanone) 0.0466 0.10 mg/kg wet 0o5000 93 63-149 0.6 20 J Methyl Isobutyl Ketone 0.0483 0.050 mg/kg wet 0.05000 97 57-162 0.9 20 J This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Spdngbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Tell Free Number: l-0001529-6364- Fax: 7041525-0409 Page 34 7750 ARR I SaM I Pull.aervice Ans Ytica ueoxnm ,Ev we Environmental Solutions Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GC/MS - Quality Control Reporting Result Limit Units Batch P7GO413 - 6035 Level II QC Report 7/31/17 Prism Work Order: 7070278 Time Submitted: 7/17/2017 3:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (P7GO413-BSD1) Prepared & Analyzed: 07/26/17 Methylene Chlonde 0.0428 0.010 mg/kg wet 0.05000 86 74-129 3 20 Methyl-tert-Butyl Ether 0.0488 0.010 mg/kg wet 0.05000 98 70-130 5 20 Naphthalene 0.0492 0.010 mg/kg wet 0.05000 98 57-157 2 20 n-Butylbenzene 0.0447 0.0050 mg/kg wet oo500o 89 65-135 4 20 n-Propylbenzene 0.0434 0.0050 mg/kg wet 0.05000 87 67-130 2 20 o­Xylene 0.0443 0.0050 mg/kg wet oo500o 89 74-126 0.9 20 sec-Butylbenzene 0.0440 0.0050 mg/kg wet 0.05000 88 66-131 2 20 Styrene 0.0473 0.0050 mg/kg wet 0.05000 95 77-121 1 20 tert-Butylbenzene 0.0424 0.0050 mg/kg wet 0.05000 85 67-132 2 20 Tetrachlonoethylene 0.0424 0.0050 mg/kg wet 0.05000 85 68-130 2 20 Toluene 0.0448 0.0050 mg/kg wet 0.05000 90 71-129 4 20 trans-1,2-Dichloroethylene 0.0450 0.0050 mg/kg wet 0.05000 90 73-132 3 20 trans-1,3-Dichlompropylene 0.0451 0.0050 mg84g wet 0.05000 90 68-123 0.3 20 Trichloroethylene 0.0432 0.0050 mg/kg wet 0.05000 86 75-133 2 20 Tnchloro8uoromethene 0.0494 0.0050 mg/kg wet 0.06000 99 44-146 7 20 Vinyl acetate 0.0521 0.025 mg/kg wet 0.05000 104 85-161 3 20 Vinyl chloride 0.0532 0.0050 mg/kg wet 0.05000 106 48-147 7 20 Xylenes, total 0.134 0.015 mg/kg wet 0.1500 89 74-126 2 20 Surrogate: 4-BromoBuombenzene 50.2 ug/L 50.00 100 70-130 Surrogate: Dibromo8uoromethane 49.5 u91L 50.00 99 84-123 Surrogate: Toluene-d8 48.6 ug/L 50.00 98 76429 This report should not be reproduced, except in its entirety, without the written consent or Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Tall Free Number: 1-800/529-6364 - Fax: 7041525-0409 Page 35 of 50 9'P R I S M i hen $erm ee nnarynoar 4 �, ffi... Env'ronmental eorvuons �$!it"t�k`:: �.sowroniss iaa Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P7G0259 - 3546 Reporting Result Limit Units Level II QC Report 7/31/17 Prism Work Order: 7070278 Time Submitted: 7/17/2017 3:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank(P7G0259-BLK7) Prepared: 07/18/17 Analyzed: 07/20/17 1,2,4-T6chlorobenzene BRL 0.33 mg/kg wet 1,2-Dichlorobenzene BRL 0.33 mg/kg wet 1,3-Dichlorobenzene BRL 0.33 mg/kg wet 1,4-Dichlorobenzene BRL 0.33 mg/kg wet 1-Methylnaphthalene BRL 0.33 mg/kg wet 2,4,6-Trichlorophenol BRL 0.33 mg/kg wet 2,4-Dichlorophenel BRL 0.33 mg/kg wet 2,4-Dimethylphenol BRL 0.33 mg/kg wet 2,4-Dintrophenol BRL 0.33 mg/kg wet 2,4-Diniaotoluene BRL 0.33 mg/kg wet 2,6-DinOotoluene BRL 0.33 mg/kg wet 2-Chloronaphthalene BRL 0.33 mg/kg wet 2-Chlorophenol BRL 0.33 mg/kg wet 2-Methylnaphthalene BRL 0.33 mg/kg wet 2-Methylphenol BRL 0.33 mg/kg wet 2-Nitrophenol BRL 0.33 mg/kg wet 3,3'-Dichlorobenzidine BRL 0.33 mg/kg wet 3/4-Methylphenol BRL 0.33 mg/kg wet 4,6-Dini0o-2-methylphenol BRL 0.33 mg/kg wet 4-Bromophenyl phenyl ether BRL 0.33 mg/kg wet 4-Chloro-3-methylphenol BRL 0.33 mllft wet 4-Chloroaniline BRL 0.33 mg/kg wet 4-Chlorophenyl phenyl ether BRL 0.33 mg/kg wet 4-Nitrophenol BRL 0.33 mg/kg wet Acenaphthene BRL 0.33 mglkg wet Acenaphthylene BRL 0.33 mg/kg wet Anthracene BRL 0.33 mg/kg wet Azobenzene BRL 0.33 mg/kg wet Benzo(a)anthracene BRL 0.33 mg/kg wet Benzo(a)pyrene BRL 0.33 mg/kg wet Benzo(b)fluorenthene BRL 0.33 mgAg wet Benzo(g,h,i)perylene BRL 0.33 mg/kg wet Benzo(k) luorenthene BRL 0.33 mg/kg wet Benzoic Add BRL 0.33 mg/kg wet Benzyl alcohol BRL 0.33 mg/kg wet bis(2-Chloroethoxy)methane BRL 0.33 mg/kg wet Bis(2-Chloroethyl)ether BRL 0.33 mg/kg wet Bis(2-chloroisopropyl)ether BRL 0.33 mg/kg wet Bis(2-Ethylhexyl)phthalate BRL 0.33 mg/kg wet Butyl benzyl phthalate BRL 0.33 mg/kg wet Chrysene BRL 0.33 mg/kg wet Dibenzo(a,h)anthmcene BRL 0.33 mglkg wet Dibenmfuran BRL 0.33 mg/kg wet Diethyl phthalate BRL 0.33 mg/kg wet Dimethyl phthalate BRL 0.33 mglkg wet Di-n-butyl phthalate BRL 0.33 mg/kg wet This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. "a Spdngbrook Road - P.O. Box 240543 - Charlotte, NC 29224-0543 Phone: 7041529-6364 -Toll Free Number: 1-80015294364 - Fax: 7041525-0400 Page 36 of 50 P R I S M I Evn-sa.moe nnalnleai s Environmental Solurlons � 4Bmn'mpIEA,K Geoscienoe Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Reporting Result Limit Units Level II QC Report 7/31/17 Prism Work Order: 7070278 Time Submitted: 7/17/2017 3:45:OOPM Spike Source hREC RPD Level Result %REC Limits RPD Limit NM Batch P7GO259 - 3546 Blank (P7GO259-BLK1) Prepared: 07/18/17 Analyzed: 07I20/17 Di-n-octyl phthalate BRL 0.33 mg/kg wet Fluoranthene BRL 0.33 mg/kg wet Fluorene BRL 0.33 mg/kg wet Hexachlorobenzene BRL 0.33 mg/kg wet Hexachlorobutadiene BRL 0.33 mg/kg wet Hexachlorocyclopentadiene BRL 0.33 mg/kg wet Hexachloroethane BRL 0.33 mg/kg wet Indeno(1,2,3-cd)pyrene BRL 0.33 mg/kg wet Isophorone BRL 0.33 mg/kg wet Naphthalene BRL 0.33 mg/kg wet Nitrobenzene BRL 0.33 mg/kg wet N-Nitroso-di-n-propylamine BRL 0.33 mg/kg wet N-Nitrosodiphenylamine BRL 0.33 mg/kg wet Pentachlorophenol BRL 0.33 mg/kg wet Phenanthrene BRL 0.33 mg/kg wet Phenol BRL 0.33 mg/kg wet Pyrene BRL 0.33 mg/kg wet Surrogate: 2,4,6-Tdbromcpheno/ 3.32 mg/kg wet 3.333 99 39-132 Surrogate: 2-F/uombipheny/ 1.46 mg/kg wet 1.667 88 44-115 Surrogate: 2-Fluorophenol 3.07 mg/kg wet 3.333 92 35-115 Surrogate: Nitrobenzene-d5 1.38 mg/kg wet 1.667 83 37-122 Surrogate: Pheno/CS 2.98 mg/kg wet 3.333 90 34-121 Surrogate: Terphenyl-014 1.88 mg/kg wet 1.667 113 54-127 LCS (P7GO259-BSI) Prepared: 07/18/17 Analyzed: 07/20/17 12,4-Trichlorobenzene 1.14 0.33 mg/kg wet 1.667 68 7W118 1,2-Dichlorobenzene 1.21 0.33 mg/kg wet 1.667 72 33-117 1,3-Dichlorobenzene 1.18 0.33 mg/kg wet 1.667 71 30-115 1,4-Dichlorobemene 1.18 0.33 mg/kg wet 1.667 71 31-115 1-Methylnaphthalene 1.31 0.33 mg/kg wet 1.667 79 4D-119 2,4,6-Trichlorophenol 1.64 0.33 mg/kg wet 1.667 93 39-126 2,4-Dichlorophenol 1.30 0.33 mg/kg wet 1.667 78 40-122 2,4-Dimethylphenol 1.64 0.33 mg/kg wet 1.667 99 30-127 2,4-Dini rophenol 1.84 0.33 mg/kg wet 1.667 110 27-129 2,4-Dinftrotoluene 1.63 0.33 mg/kg wet 1.667 98 48-126 2,6-Dinfttoluene 1.63 0.33 mg/kg wet 1.667 98 46-124 2-Chloronaphthalene 1.43 0.33 mg/kg wet 1.667 86 41-114 2-Chlorophenol 1.54 0.33 mg/kg wet 1.667 92 34-121 2-Methylnaphthalene 1.26 0.33 mg/kg wet 1.667 76 38-122 2-Methylphenol 1.59 0.33 mg/kg wet 1.667 95 32-122 2-Nibophenol 1.30 0.33 mg/kg wet 1.667 78 36-123 3,3' Dichlorobenzidine 1.66 0.33 mg/kg wet 1.667 100 22-121 3/4-Methylphenol 1.44 0.33 mg/kg wet 1.667 86 34-119 4,6-Dinitro-2-med ylphenol 1.68 0.33 mg/kg wet 1.667 100 29-132 4-Bromophenyl phenyl ether 1.45 0.33 mg/kg wet 1.667 87 46-124 4-Chloro-3-methylphenol 1.47 0.33 mg/kg wet 1.667 88 45-122 4-Chloroaniline 1.21 0.33 mg/kg wet 1.667 73 17-106 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbreok Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529.6364 - Toll Free Number: 1.800/529.6364- Fax: 704/525-0409 Page 37 of 50 iY Full -Service Analyllcai 8 &IP R I S M I Environmental Solutions �:,�ueauron,rs,uc Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, INC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Reporting Result Limit Units Level 11 QC Report 7/31/17 Prism Work Order: 7070278 Time Submitted: 7/17/2017 3:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P7GO259 - 3546 LCS (P7G0259-BSI) Prepared: 07/18/17 Analyzed: 07/20/17 4-Chlorophenyl phenyl ether 1.44 0.33 mg/kg wet 1.667 86 45-121 4-Nitrophenol 1.76 0.33 mg/kg wet 1.667 105 30-132 Acenaphthene 1.52 0.33 mg/kg wet 1.667 91 40-123 Acenaphthylene 1.50 0.33 mg/kg wet 1.667 90 32-132 Anthracene 1.61 0.33 mglkg wet 1.667 97 47-123 Azobenzene 1.71 0.33 mg/kg wet 1.667 103 39-125 Benzo(a)anthracene 1.61 0.33 mg/kg wet 1,667 97 49-126 Benzo(a)pyrene 1.53 0.33 mg/kg wet 1.667 92 45-129 Benzo(b)fluoranthene 1.55 0.33 mg/kg wet 1.667 93 45.132 Benzo(g,h,i)perylene 1.41 0.33 mg/kg wet 1.667 85 43-134 Benzo(k)6uoranthene 1.52 0.33 mg/kg wet 1.667 91 47-132 Benzoic Acid 1.15 0.33 mg/kg wet 1.667 69 10-83 Benzyl alcohol 1.43 0.33 mg/kg wet 1.667 86 29-122 bis(2-Chlorcethoxy)methane 1.24 0.33 mg/kg wet 1.667 74 36-121 Sis(2-Chloroethyl)ether 1.23 0.33 mg/kg wet 1.667 74 31-120 Bis(2-chlorolsopropyl)ether 1.42 0.33 mg/kg wet 1.667 85 33-131 Bis(2-Ethylhexyl)phthalate 1.64 0.33 mg/kg wet 1,667 98 51-133 Butyl benzyl phthalate 1.64 0.33 mg/kg wet 1.667 98 48-132 Chrysene 1.58 0.33 mg/kg wet 1.667 95 50-124 Dibenzo(a,h)anthracene 1.53 0.33 mg/kg wet 1.667 92 45-134 Dibenzofunm 1.54 0.33 mg/kg wet 1.667 92 44-120 Diethyl phthalate 1.55 0.33 mg/kg wet 1.667 93 W124 Dimethyl phthalate 1.50 0.33 mg/kg wet 1.667 90 48-124 Di-n-butyl phthalate 1.68 0.33 mg/kg wet 1.667 95 51-126 Di-n-octyl phthalate 1.67 0.33 mg/kg wet 1.667 100 45A40 Fluoranthene 1.60 0.33 mg/kg wet 1,667 96 50-127 Fluorene 1.53 0.33 mg/kg wet 1.667 92 43-125 Hexachlorobenzene 1.50 0.33 mg/kg wet 1.667 90 45-122 Hexachlorobutadiene 1.21 0.33 mg/kg wet 1.667 73 32-123 Hexachlorocydopentadiene 0.561 0.33 mg/kg wet 1.667 34 32-117 Hexachloroethane 1.16 0.33 mg/kg wet 1.667 69 28-117 Indeno(1,2,3-od)pyrene 1.55 0.33 mg/kg wet 1.667 93 45-133 Isophorone 1.35 0.33 mg/kg wet 1.667 81 30-122 Naphthalene 1.24 0.33 mg/kg wet 1.667 74 35-123 Nitrobenzene 1.27 0.33 mg/kg wet 1.667 76 34-122 N-Nitroso-di-n-propylamine 1.50 0.33 mg/kg wet 1.667 90 36-120 N-Nitrosodiphenylarnme 1.89 0.33 mg/kg wet 1.667 113 38-127 Pemachlorophenol 1.73 0.33 mg/kg wet 1.667 104 25-133 Phenanthrene 1.62 0.33 mg/kg wet 1.667 97 50-121 Phenol 1.42 0.33 mg/kg wet 1.667 85 34-121 Pyrene 1.57 0.33 mg/kg wet 1.667 94 47-127 Surrogate: 2,4,6-Tnbromopheno/ 3.11 mg/kg wet 3.333 93 39-132 Surrogate: 2-Ruorobiphenyl 1.37 mg/kg wet 1.667 82 44-115 Surrogate: 2-F/uorophenol 2.89 mi; t0 wet 3.333 87 35-115 Surrogate: NBrobenzened5 1.20 mg/kg wet 1.667 72 37-122 Surrogate: Phenold5 2.84 m9*9 wet 3.333 85 34-121 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 1-8001529.6364 - Fax:704/525-0409 Page 38 oT 50 }P Full -Service Analytical & ISM I Environmental Soiutlons �aaaw.aa,rs,ne Geoscienoe Group Attn: Tom Hassell 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GC/MS - Quality Control Anaiyle Reporting Result Limit Units Level II QC Report 7/31/17 Prism Work Order: 7070278 Time Submitted: 7/17/2017 3:45:0013M Spike Source %REC RPD Level Result %REC Limits RPD i i,.,a u,.t Batch 127130259.3546 LCS (P7G0259-BSI) Prepared: 07/18/17 Analyzed: 07/20/17 Surrogate: Terphenyl-d14 1.67 mg/kg wet 1,667 f00 54-127 LCS Oup (P7G0259-BSD1) Prepared: 07/18/17 Analyzed: 07/20/17 1,2,4-Tdchlorobenzene 1.11 0.33 mg/kg wet 1.667 66 34-118 3 20 1,2-Dichlorobenzene 1.17 0.33 mg/kg wet 1.667 70 33-117 3 20 1,3-Dichlombemene 1.16 0.33 mg/kg wet 1.667 70 30-116 2 20 1,4-Dichlorobenzene 1.14 0.33 mg/kg wet 1.667 68 31-116 3 20 1-Methylnaphthalene 1.28 0.33 mg/kg wet 1.667 77 40-119 3 20 2,4,6-Tdchlorophenol 1.54 0.33 mg/kg wet 1.667 92 39-126 0.6 20 2,4-Dichlorophenol 1.28 0.33 mg/kg wet 1.667 77 40-122 1 20 2,4-Dimethylphenol 1.62 0.33 mg/kg wet 1.667 97 30-127 1 20 2,4-Dinhrophenol 1.90 0.33 mg/kg wet 1.667 114 27-129 3 20 2,4-Dinhrotoluene 1.61 0.33 mg/kg wet 1.667 97 48-126 1 20 2,6-Dinhrotoluene 1.62 0.33 mg/kg wet 1.667 97 46-124 0.5 20 2-Chlomnaphthalene 1.37 0.33 mg/kg wet 1.667 82 41-114 4 20 2-Chlorophenol 1.47 0.33 mg/kg wet 1.667 88 34-121 5 20 2-Methylnaphthalene 1.22 0.33 mg/kg wet 1.667 73 38-122 3 20 2-Methylphenol 1.53 0.33 mg/kg wet 1.667 92 32-122 4 20 2-Nhrophenol 1.25 0.33 mg/kg wet 1.667 75 36-123 4 20 30-Dichlorobenzidine 1.68 0.33 mg/kg wet 1.667 101 22-121 1 20 3/4-Methylphenol 1.40 0.33 mg/kg wet 1.667 84 34-119 2 20 4,6-Dinibo-2-methylphenol 1.69 0.33 mg/kg wet 1.667 101 29-132 1 20 4-Bromophenyl phenyl ether 1.42 0.33 mg/kg wet 1.667 85 46-124 2 20 4-Chloro-3-methylphenol 1.44 0.33 mg/kg wet 1.667 86 45-122 2 20 4-Chloroaniline 1.18 0.33 mg/kg wet 1.667 71 17-106 3 20 4-Chlorophenyl phenyl ether 1.43 0.33 mg/kg wet 1.667 86 45-121 0.8 20 4-Nitrophenol 1.75 0.33 mg/kg wet 1.667 105 30-132 0.3 20 Amnaphthene 1.51 0.33 mg/kg wet 1.667 91 40-123 0.9 20 Amnaphthylene 1.46 0.33 mg/kg wet 1.667 88 32-132 3 20 Anthracene 1.62 0.33 mg/kg wet 1.667 97 47-123 0.6 20 Azobenzene 1.66 0.33 mg/kg wet 1.667 99 39-125 3 20 Benzo(a)anthmcene 1.60 0.33 mg/kg wet 1.667 96 49-126 1 20 Benzo(a)pyrene 1,55 0.33 mg/kg wet 1.667 93 45-129 1 20 Benzo(b)fluomnthene 1.56 0.33 mg/kg wet 1.667 94 45-132 0.7 20 Benzo(g,h,i)peMene 1.43 0.33 mg/kg wet 1.667 86 43-134 1 20 Benzo(k)fluuranthene 1.55 0.33 mg/kg wet 1.667 93 47-132 2 20 Benzoic Acid 1.23 0.33 mg&g wet 1.667 74 10-83 7 20 Senzyl alcohol 1.37 0.33 mg/kg wet 1.667 82 29-122 4 20 bis(2-Chloroethoxy)methene 1.18 0.33 mg/kg wet 1.667 71 36-121 5 20 Bis(2-Chloroethyl)ether 1.18 0.33 mg/kg wet 1,667 71 31-120 5 20 Bis(2-chlomisopropyl)ether 1.36 0.33 mg/kg wet 1.667 81 33-131 4 20 Bis(2-Ethylhexyl)phthelate 1.66 0.33 mg/kg wet 1.667 100 51-133 1 20 Butyl benzyl phthalate 1.65 0.33 mg/kg wet 1.667 99 48-132 0.9 20 Chrysene 1.58 0.33 mg/kg wet 1.667 95 50-124 0.1 20 Dibenzo(a,h)anthmcene 1.57 0.33 mg/kg wet 1.667 94 45.134 2 40 Dibenzofuran 1.52 0.33 mg/kg wet 1.667 91 44-120 1 20 Diethyl phthalate 1.55 0.33 mg/kg wet 1.667 93 50-124 0.04 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. "Is Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529.6364-Toll Free Number. l-800/529-6364-Fax: 7041525-0409 Page 39 of 50 PRISM I Fo-aameA>.Wfla,a Environmental Sduuons uawnow,es,xc Geoscience Group Attn: Tom Hasselt 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P7130259 - 3546 Reporting Result Limit Units Level II QC Report 7/31/17 Prism Work Order: 7070278 Time Submitted: 7/17/2017 3:45:OOPM Spike Source /REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (P7G0259-BSD1) Prepared: 07/18/17 Analyzed: 07/20/17 Dimethyl phthalate 1.49 0.33 mg/kg wet 1.667 90 48-124 0.4 20 Di-n-butyl phthalate 1.61 0.33 mg/kg wet 1.667 96 51-128 1 20 Di-n-octyl phthalate 1.71 0.33 mgtkg wet 1.667 103 45-140 2 20 Fluoranthene 1.62 0.33 mg/kg wet 1.667 97 50-127 1 20 Fluorene 1.61 0.33 mg/kg wet 1.667 91 43-125 2 20 Hexachlorobenzene 1.51 0.33 mg/kg wet 1.667 90 45-122 0.3 20 Hexachlorobutadiene 1.17 0.33 mg/kg wet 1.667 70 32-123 3 20 Hexachlomcydopentadiene 0.536 0.33 mg/kg wet 1.667 32 32-117 4 20 Hexachloroethane 1.12 0.33 mg/kg wet 1.667 67 28-117 3 20 Indeno(1,2,3-cd)pyrene 1.56 0.33 mg/kg wet 1.667 93 45-133 0.3 20 Isophorone 1.31 0.33 mg/kg wet 1.667 79 30-122 3 20 Naphthalene 1.20 0.33 mg/kg wet 1.667 72 35123 3 20 Nitrobenzene 1.23 0.33 mg/kg wet 1.667 74 34-122 3 20 N-Niboso-di-n-propylamine 1.45 0.33 mg/kg wet 1.667 87 36-120 3 20 N-Nitrosodiphenylamine 1.88 0.33 mg/kg wet 1.667 113 38-127 0.2 20 Pentachlorophenol 1.80 0.33 mg/kg wet 1.667 108 25-133 4 20 Phenanthrene 1.60 0.33 mg/kg wet 1.667 96 50-121 0.7 20 Phenol 1.38 0.33 mg/kg wet 1.667 83 34-121 3 20 Pyrene 1.57 0.33 mg/kg wet 1.667 94 47-127 0.1 20 Surrogate: 2,4,6-Tnbromophenol 3.07 mg/kg wet 3.333 92 39-132 Surrogate: 2-Fluorobtphenyl 1.35 mgft wet 1.667 81 44-115 Surrogate: 2-Fluorophenot 2.78 mg/kg wet 3.333 83 35-115 Surrogate: Mimbenzened5 1.15 mg*g wet 1.667 69 37-122 Surrogate: Phenold5 2.73 mg kg wet 3.333 82 34-121 Surrogate: Terphenyldl4 1.68 mg/kg wet 1.667 101 54-127 Matrix Spike (P700259.MS7) Source: 7070278.04 Prepared: 07/18/17 Analyzed: 07/20/17 1,2,4-Tdchlorobenzene 1.30 0.47 mg/kg dry 2.398 BRL 54 34-118 1,2-Dichlombenzene 1.35 0.47 mg/kg dry 2.398 BRL 56 33A 17 1,3-Dichlorobenzene 1.33 0.47 mg/kg dry 2.398 BRL 56 30-116 1,4-Dichlombenzene 1.32 0.47 mg/kg dry 2.398 BRL 55 31-115 i-Methylnaphthalene 1.58 0.47 mg/kg dry 2.398 BRL 66 40AI9 2,4,6-Trichlorophenol 1.73 0.47 mg/kg dry 2.398 BRL 72 39-126 2,4-Dichlorophenol 1.48 0.47 mg/kg dry 2.398 BRL 62 40-122 2,4-Dimethylphenol 1.36 0.47 mgtkg dry 2.398 BRL 57 30-127 2,4-Dinitrophenol 2.57 0.47 mg/kg dry 2.398 BRL 107 27-129 2,4-Dinitrotoluene 2.10 OA7 mgtkg dry 2.398 BRL 88 48-126 2,6-DinBrotoluene 2.08 0.47 mg/kg dry 2.398 BRL 87 46-124 2-Chloronaphthalene 1.69 0.47 mg/kg dry 2.398 BRL 70 41-114 2-Chlorophenol 1A4 OA7 mg/kg dry 2.398 BRL 68 34-121 2-Methylnaphthalene 1.50 0.47 mg/kg dry 2.398 BRL 63 38-122 2-Methylphenol 1.62 0.47 mgtkg dry 2.398 BRL 68 32-122 2-Nitrophenol 1.52 0.47 mpg dry 2.398 BRL 63 36-123 3,3'-Dichlorobenzidine 0.195 0.47 mg/kg dry 2.398 BRL 6 22-121 M i 3/4-Methylphenol 1.49 OA7 mg/kg dry 2.398 BRL 62 34-119 4,6-Dinttro-2-methylphenol 2.18 0.47 mg/kg dry 2.398 BRL 91 29-132 4-Bromophenyl phenyl ether 1.87 0.47 mg/kg dry 2.398 BRL 78 46-124 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529.6364-Toll Free Number: 1-800I529-6354- Fax: 704/525.0409 Page40of50 P R ISM I Full earvlce Analytical a Geoscienoe Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GCIMS - Quality Control Analyte Reporting Result Limit Units Level II QC Report 7131/17 Prism Work Order: 7070278 Time Submitted: 7/17/2017 3:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch 137GO259 - 3546 Matrix Spike(P7G0259-MS1) Source: 7070278.04 Prepared: 07/18/17 Analyzed: 07/20/17 4-Chlorc-3-methylphenol 1.76 0.47 mg/kg dry 2.398 BRL 73 45-122 4-Chloroaniline 0.985 0.47 mg/kg dry 2.398 BRL 41 17-106 4-Chlorophenyl phenyl ether 1.85 0.47 mg/kg dry 2.398 BRL 77 45-121 4-Nibophenol 2.39 0.47 mg/kg dry 2.398 BRL 100 30-132 Acenaphthene 1.90 0.47 mg/kg dry 2.398 BRL 79 40-123 Acenaphthylene 1.79 0.47 mg/kg dry 2.398 BRL 74 32-132 Anthrecene 2.04 0.47 mg/kg dry 2.398 BRL 85 47-123 Azobenzene 2.16 0.47 mg/kg dry 2.398 BRL 90 39-125 Benzo(a)anthracene 2.08 0.47 mg/kg dry 2.398 BRL 87 49-126 Benzc(a)pyrene 1.96 0.47 mg/kg dry 2.398 BRL 82 45-129 Senzo(b)fluomnthene 2.04 0.47 mg/kg dry 2.398 BRL 85 45-132 Benzo(g,h,i)perylene 1.86 0.47 mg/kg dry 2.398 BRL 77 43-134 Benzo(k)fluoranthene 2.00 0.47 mg/kg dry 2.398 BRL 83 47-132 Benzoic Acid 1.78 0.47 mg/kg dry 2.398 BRL 74 10-83 Benzyl alcohol 1.75 0.47 mg/kg dry 2.398 BRL 73 29-122 bis(2-Chloroethoxy)nethane 1.44 0.47 mg/kg dry 2.398 BRL 60 36-121 Bis(2-Chloroethyl)ether 1.42 0.47 mg/kg dry 2.398 BRL 59 31-120 Bis(2-chloroisopropyl)ether 1.63 0.47 mg/kg dry 2.398 BRL 68 33-131 BIs(2-Ethylhexyl)phthalate 2.57 0.47 mg/kg dry 2.398 BRL 107 51-133 Butyl benzyl phthalate 2.22 0.47 mg/kg dry 2.398 BRL 93 48-132 Chrysene 2.11 0.47 mg/kg dry 2,398 BRL 88 50-124 Dibenzo(a,h)anthracene 2.04 0.47 mg/kg dry 2.398 BRL 85 45-134 Dibemofumn 1.93 0.47 mg/kg dry 2.398 BRL 80 44-120 Diethyl phthalate 2.04 0.47 mg/kg dry 2.398 BRL 85 50-124 Dimethyl phthalate 1.92 0.47 mg/kg dry 2.398 BRL 80 48-124 Di-n-butyl phthalate 2.13 0.47 mg/kg dry 2.398 BRL 89 51-128 Di-n-octyl phthalate 2.24 0.47 mg/kg dry 2.398 BRL 93 45-140 Fluoranthene 2.12 0-.47 mg/kg dry 2.398 BRL 88 50-127 Fluorene 1.99 0.47 mg/kg dry 2.398 BRL 83 43-125 Hexachlorobenzene 1.93 0.47 mg/kg dry 2.398 BRL 81 45-122 Hexachlorobutadiene 1.37 0.47 mg/kg dry 2.398 BRL 57 32-123 Hexachlorocyciopentadiene 0.553 0.47 mg/kg dry 2.398 BRL 23 32-117 M Hexachloroethane 129 0.47 mg/kg dry 2.398 BRL 54 28-117 Indeno(1,2,3-cd)pyrene 2.03 0.47 mg/kg dry 2.398 BRL 84 45-133 Isophorone 1.64 0.47 mg/kg dry 2.398 BRL 68 30-122 Naphthalene 1 A7 0.47 mg/kg dry 2.398 BRL 61 35-123 Nitrobenzene 1.50 0.47 mg/kg dry 2.398 BRL 62 34-122 N-Nitroso-di-n-propylamine 1.74 0.47 mg/kg dry 2.398 BRL 72 36-120 N-Nitmsodiphenylamine 1.88 0.47 mg/kg dry 2.398 BRL 78 38-127 Pentachlorophenol 2.36 0.47 mg/kg dry 2.398 BRL 98 25-133 Phenanthrene 2.08 0.47 mglkg dry 2.398 BRL 87 50-121 Phenol 1.55 0.47 mg/kg dry 2.398 BRL 65 34-121 Pyrene 2.08 0.47 mglkg dry 2.398 BRL 87 47-127 Surrogate: 2,4,6-Tdbromopheno/ 3.54 mg*g dry 4.796 74 39-132 Surrogate: 2-Fluorobiphenyl 1.66 mg/kg dry 2.398 69 44-115 Surrogate: 2-Fluoropheno/ 2.97 mg/kg dry 4.796 62 35-115 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529.6364 -Toll Free Number. 1-800/529.6364 - Fax: 7041525-0409 Page 41 Df 50 /"P R I SpM I Full eeryce A.W,flOai B ens ronmen:al smmmns Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P7130259 - 3546 Reporting Result Limit Units Level II QC Report 7131117 Prism Work Order: 7070278 Time Submitted: 7/17/2017 3:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Matrix Spike (P7GO259-MS1) Source: 7070278.04 Prepared: 07/18/17 Analyzed: 07/20/17 Surrogate: NSrobenzene-d5 1.42 mWkg dry 2.398 59 37-122 Surrogate: Phenol-d5 3.12 mq&9 dry 4.796 65 34-121 Surrogate: Terpheny4-04 2.22 mg4r9 dry 2.398 92 54-127 Matrix Spike Oup (P7G0259-MSD1) Source: 7070278-04 Prepared: 07/18/17 Analyzed: 07/20/17 1,2,4-Tdchlorobenzene 1.65 0.48 mg/kg dry 2.407 BRL 68 34-118 23 20 D 1,2-Dichlombenzene 1.85 0.48 mg/kg dry 2.407 BRL 77 33-117 31 20 D 1,3-Dichlombenzene 1.87 0.48 mg/kg dry 2.407 BRL 78 30-115 34 20 D IA-Dichlorobenzene 1.83 0.48 mg/kg dry 2.407 BRL 76 31-115 33 20 D 1-Methylnaphthalene 1.79 0.48 mg/kg dry 2.407 BRL 74 40.119 12 20 2,4,6-Tdchlorophend 1.75 0.48 mg/kg dry 2.407 BRL 73 39-126 1 20 2,4-Dichlomphenol 1.63 0.48 mg/kg dry 2.407 BRL 68 40-122 10 20 2,4-Dimethylphenol 1.55 0.48 mg/kg dry 2.407 BRL 64 30-127 13 20 2,4-Dinftrophenol 1.68 0.48 mg/kg dry 2.407 BRL 70 27-129 41 20 D 2,4-Dinitrotoluene 2.06 0.48 mg/kg dry 2.407 BRL 86 48-126 2 20 2,6-Dinitrotoluene 2.12 0.48 mg/kg dry 2.407 BRL 88 46-124 2 20 2-Chloronaphthalene 1.91 0.48 mg/kg dry 2.407 BRL 79 41-114 12 20 2-Chlorophenol 2.00 0.48 mg/kg dry 2.407 BRL 83 34-121 20 20 2-Methylnaphthalene 1.74 0.48 mg/kg dry 2.407 BRL 72 38-122 14 20 2-Methyiphenol 1.88 0.48 mgecg dry 2.407 BRL 78 32-122 15 20 2-Nitrophenol 2.66 0.48 mg/kg dry 2.407 BRL 110 36-123 55 20 D 3,T-Dichlombenzidine 0.180 0.48 mgft dry 2.407 BRL 7 22-121 8 20 M. J 3/4-Methylphenol 1.73 0.48 mg/kg dry 2.407 BRL 72 34-119 15 20 4,6-Dinhro-2-methyiphenol 1.74 0.48 mg/kg dry 2.407 BRL 72 29-132 22 20 D 4-Bromophenyl phenyl ether 1.83 0.48 mg/kg dry 2.407 BRL 76 46-124 2 20 4-Chloro-3-methylphenol 1.83 0.48 mg/kg dry 2.407 BRL 76 45-122 4 20 4-Chloroaniline 0.482 0.48 mg/kg dry 2.407 BRL 20 17-106 68 20 D 4-Chlomphenyl phenyl ether 1.87 0.46 mg/kg dry 2.407 BRL 78 45-121 1 20 4-Nlbophenol 1.43 0.48 mg/kg dry 2.407 BRL 59 30-132 50 20 D Acenaphthene 1.95 0.48 mg/kg dry 2.407 BRL 81 40-123 2 20 Acenaphthylene 1.97 0.48 mg/kg dry 2.407 BRL 82 32-132 10 20 Anthracene 2.04 0.48 mg/kg dry 2.407 BRL 85 47-123 0.3 20 Azobenzene 2.16 0.48 mg/kg dry 2,407 BRL 90 39-125 0.4 20 Benzo(a)anthracene 2.01 0.48 mg/kg dry 2.407 BRL 83 49-126 4 20 Benzo(s)pyrene 1.94 0.48 mg/kg dry 2.407 BRL 81 45-129 1 20 Benzo(b)8uoranthene 1.96 0.48 mg/kg dry 2.407 BRL 81 45.132 4 20 Benzo(g,h,i)perylene 1.78 0.48 mg/kg dry 2.407 BRL 74 43-134 4 20 Benzo(k)fluoranthene 1.93 0.48 mg/kg dry 2.407 BRL 80 47-132 4 20 Benzoic Add 0.809 0.48 mg/kg dry 2.407 BRL 34 10-83 75 20 D Benzyl alcohol 2.06 0.48 mg/kg dry 2.407 BRL 86 29-122 17 20 bis(2-Chloroethoxy)methane 1.66 0.48 mg/kg dry 2.407 BRL 69 36-121 14 20 Bis(2-Chlomethyl)sther 2.62 0.48 mg/kg dry 2.407 BRL 109 31-120 60 20 D Bis(2-chloroisopropyl)ether 2.05 0.48 mg/kg dry 2.407 BRL 85 33-131 23 20 D Bis(2-Ethylhexyl)ph1halate 2.09 0.48 mg/kg dry 2.407 BRL 87 51-133 20 20 Butyl benzyl phthalate 2.07 0.48 mg/kg dry 2.407 BRL 86 48-132 7 20 Chrysene 1.99 0.48 mg/kg dry 2.407 BRL 83 50-124 6 20 Dibenzo(a,h)anmracene 1.94 0.48 mg/kg dry 2.407 BRL 80 45-134 5 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laborstodes, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-OS43 Phone: 704/529-6364 - Toll Free Number: 1-800/529.6364- Fax: 70415254409 Page 42 of 50 / P I San A I Full-aervlce Analytical & �+( ueoAna es,xc Envlronmantel SOWticna Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GUMS - Quality Control Reporting Result Limit Units Batch P7GO259 - 3546 Level II QC Report 7/31/17 Prism Work Order: 7070278 Time Submitted: 7/17/2017 3:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Matrix Spike Dup(P7G0259-MSD1) Source: 7070278-04 Prepared: 07/18/17 Analyzed: 07/20/17 Dibenzofuran 2.02 0.48 mg/kg dry 2.407 BRL 84 44-120 4 20 Diethyl phthalate 1.96 0.48 mg/kg dry 2,407 BRL 82 50-124 4 20 Dimethyl phthalate 1.96 0.48 mg/kg dry 2.407 BRL 81 48-124 2 20 DFn-butyl phthalate 1.99 0.48 nV&g dry 2.407 BRL a3 51.128 7 20 Di-n-octyl phthalate 2.07 0.48 mg/kg dry 2.407 BRL 86 45-140 8 20 Fluorenthene 2.01 0.48 mglkg dry 2.407 BRL 83 60-127 5 20 Fluorene 1.99 0.46 mg/kg dry 2.407 BRL 83 43-126 0.2 20 Hexachlorobenzene 1.91 0.48 mg/kg dry 2.407 BRL 79 45-122 1 20 Hexachlorobutadiene 1.75 0.48 mgft dry 2.407 BRL 73 32-123 24 20 D Hexachlorocyclopentadiene 0.821 0.48 mg/kg dry 2.407 BRL 34 32-117 39 20 D Hexachloroethane 1.83 0.48 mg/kg dry 2.407 BRL 76 28-117 35 20 D Indeno(1,2,3-cd)pyrene 1.96 0.48 mg/kg dry 2.407 BRL 81 45-133 3 20 Isophorone 1.85 0.48 mg/kg dry 2.407 BRL 77 30-122 12 20 Naphthalene 1.77 0.48 m9ft dry 2.407 BRL 74 36-123 18 20 Nitrobenzene 1.82 0.48 mg/kg dry 2.407 BRL 76 34-122 20 20 N-Nitroso-di-n-propylamine 2.04 0.48 mg/kg dry 2.407 BRL 85 35-120 16 20 N-Nitrosodiphenylamine 1.83 0.48 m9ft dry 2A07 BRL 76 38-127 2 20 Pentachlorophenol 2.14 0.46 mg/kg dry 2.407 BRL 89 25-133 10 20 Phenanthrene 2.04 0.48 mg/kg dry 2.407 BRL 65 50-121 2 20 Phenol 1.85 0.48 mg/kg dry 2A07 BRL 77 34-121 18 20 Pyrene 2.01 0.46 mg/kg dry 2.407 BRL 84 47-127 3 20 Surrogate: 2,4,6-Tribmmopheno/ 7.32 mg&g dry 9.628 76 39-132 Surrogate: 2-Fluombiphenyl 3.58 m9/k9 dry 4.814 74 44-115 Surrogate: 2-Fluomphenol 7.03 mg4rg dry 9.628 73 35-115 Sunogate: Nitrobenzene-d5 3.44 mgrkg dry 4.814 72 37-122 Surrogate: Phenol-d5 7.19 m9*9 dry 9.628 75 34-121 Surrogate: Terphenyl414 4.07 mg4r9 dry 4.814 85 54-127 This report should not be reproduced, except in its entirety, without the written consent of Prism laboratories, Inc. 449 Spdngbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 -Toll Free Number: 1-8001529.6364 - Fax: 704/525-0409 Page 43 of 50 P R I S M Level II QC Report Fun-aervlce Analytical 8 Envlronmentei Solutions 7131117 P a. Geoscien a Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Gasoline Range Organic by GCIFID - quality Control Prism Work Order: 7070278 Time Submitted: 7/17/2017 3:45:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch MOM - 5035 Blank (P7G0359-BLK1) Prepared & Analyzed: 07/24/17 Gasoline Range Organics BRL 5.0 mglkg wet Surrogate: a,as-TnBuorololuene 5.25 mgft 5,000 105 50-137 LCS (P700359-11151) Prepared & Analyzed: 07124117 Gasoline Range Organics 51.6 5.0 mi wet 50.00 103 41-138 Surrogate: a,a,a-TriSuorololuens 4.25 mg/kg 5.000 85 50-137 LCS Dup (P7G0359-BSDI) Prepared & Analyzed: 07/24/17 Gasoline Range Organios 62.3 5.0 mg/kg wet 50.00 125 41-138 19 20 Surrogate: a,a,a-TriSuorotoluene 5.30 mg4ig &000 106 50-137 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrcok Road - P.O. Box 240543 - Charlotte, INC 28224-0543 Phone: 7041529-6364 -Toll Free Number: 14001529-6364 - Fax: 7041525-0400 Page 44 of 50 R I S M I Fuil-Service Analyncel a Environmental SOlutions Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Diesel Range Organics by GC/FID - Quality Control Reporting Result Limit Units Batch 137GO258 - 3546 Level II QC Report 7131117 Prism Work Order: 7070278 Time Submitted: 7/17/2017 3:45:0013M Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank(P7G025843LKI) Prepared: 07/18/17 Analyzed: 07/19/17 Diesel Range Organics BRL 7.0 mglkg wet Surrogate: o-Tarphenyl 1.50 m9ft wet 1.333 113 49-124 LCS (MI11258-BSI) Prepared: 07/18/17 Analyzed: 07/19/17 Diesel Range Organics 63.0 7.0 m9ft wet 66.67 94 65-109 Surrogate: o-Terphenyl 1.40 nvkg wet 1.333 105 49-124 LCS Dup (M0258433DI) Prepared: 07/18/17 Analyzed: 07/19/17 Diesel Range Organics 66.3 7.0 mgft wet 66.67 99 55-109 5 20 Surrogate: o-70phenyl 1.44 m9*9 wet 1.333 - 108 49-124 Batch M0460.3550C GC Blank(P7GO46043LK1) Prepared: 07/28/17 Anayzed: 07/29/17 Diesel Range Organics BRL 5.8 mgft wet Surrogate : o-Terphenyl 0.970 mg4lg wet 1.333 73 49-124 LCS(P7G0460-BSI) Prepared: 07/28/17 Analyzed: 07/29/17 Diesel Range Organics 68.1 5.8 mgft wet 66.67 97 55-109 Surrogate: o-Terphenyl 0.910 mgrkg wet 1.333 68 49-124 LCS Dup (127G046043SDI) Prepared: 07/2&17 Analyzed: 07/29/17 Diesel Range Organics 68.3 5.8 mglkg wet 66.67 103 55-109 16 20 Surrogate: o-7erphenyl 1.06 mgft wet 1.333 79 49-124 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704IS29-6364 -Toll Free Number: 1-800IS29.6364 - Fax: 704/5254W9 Page 45 of 50 �F3R I S M I Fuvirormro al Solutions s Environmental Solutions T'ueaumnirs iw Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Total Metals - Quality Control Project: Truck Part Service Level II QC Report 7131/17 Prism Work Order: 7070278 Time Submitted: 7/17/2017 3:45:OOPM Reporting Spike Source %REC RPD Analyle Result Lima Units Level Result %REC Limits RPD Limit Notes Batch P7130274-3060A Blank(P7GO274-BLKI) Prepared: 0721117 Analyzed: 0724/17 Hexavalent Chromium BRL 0.40 mg/kg wet LCS (P71310274-8151) Prepared: 07/21/17 Analyzed: 0724/17 Hexavalent Chromium 17.8 0.40 mg/kg wet 16.00 111 80-120 Matrix Spike(P7G027448SI) Source: 7070278.08 Prepared: 0721/17 Analyzed: 0724/17 Haxavalent Chromium 12.0 0.48 mg/kg dry 19.25 0.646 60 75-125 M Matrix Spike Dup (P7G0274-MSDI) Source: 7070278.08 Prepared: 0721/17 Analyzed: 0724/17 Hexavelenl Chromium 11.2 0.49 mglkg dry 19.63 0.546 64 75-125 7 20 M Post Spike(P7GO274-PSI) Source: 7070278-08 Prepared: 0721/17 Analyzed: 0724117 Hexavalent Chromium 0.243 m9ft 0.4000 0.0109 58 85-115 M Batch MOW - 747113 Blank (P7G0287-BLKI) Prepared & Analyzed: 0720117 Mercury BRL 0.020 mglkg wet LCS (P7G0287-BSI) Prepared & Analyzed: 0720/17 Mercury OA35 0.020 mglkg wet 0.4167 104 80-120 Batch 137GO320-3050B Blank (P7G0320-BLK1) Prepared & Analyzed: 0721117 Arsenic BRL 0.25 mglkg wet Barium BRL 0.50 mglkg wet Cadmium BRL 0.25 mg/kg wet Chromium BRL 0.25 mg/kg wet Lead BRL 0.25 mgft wet Selenium BRL 0.50 mglkg wet Silver BRL 0.25 mg1k; wet This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041528-6364 - Toll Free Number: l-8001529-6364- Fax: 704/525.0409 Page 46 of 50 L Level It QC Report ISM I Fun -Service Anelyncsl S Envlronman4l Samlona 7/31/17 Tuew.onea ixc Geoscience Group Project: Truck Part Service Prism Work Order: 7070278 Attn: Tom Hassett Time Submitted: 7/17/2017 3:45:OOPM 500-K Clanton Rd. Charlotte, NC 28217 Total Metals - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P7GO320 - 3050B LCS (107130320-BS7) Prepared & Analyzed: 07/21/17 Arsenic 24.2 0.25 mg/kg wet 25.00 97 80-120 Barium 25.5 0.50 mg/kg wet 25.00 102 80-120 Cadmium 22.1 0.25 mg/kg wet 25.00 88 80-120 Chromium 25.0 0.25 mgkg wet 25.00 100 W120 Lead 24.0 0.25 mg/kg Wet 25.00 96 80-120 Selenium 23A 0.50 m9ft wet 25.00 94 W120 Silver 9.95 0.25 mg/kg wet 10.00 100 80-120 Matrix Spike (P7GO320-MS7) Source: 7070278.01 Prepared & Analyzed: 07/21/17 Arsenic 77.8 0.35 mg/kg dry 35.12 57.0 59 75-125 MI Barium 186 0.70 mg/kg dry 35.12 171 44 75-125 E. MC Cadmium 20.2 0.35 mg/kg dry 35.12 0.420 56 75-125 MI Chromium 126 0.35 mg/kg dry 35.12 91.9 98 75-125 Lead 28.8 0.35 mg*g dry 35.12 6.51 63 75-125 MI Selenium 21.0 0.70 mg/4 dry 35.11 SRL 60 75-125 MI Silver 12A 0.35 mg&g dry 14.05 BRL 88 75-125 Matrix Spike Dup (127GO320-1111SD1) Sourr e: 7070278.01 Prepared & Analyzed: 07/21/17 Arsenic 72.5 0.36 mg/kg dry 35.30 57.0 44 75-126 7 20 MI Barium 208 0.71 mg/kg dry 36.29 171 105 75-125 11 20 E. MC Cadmium 19.6 0.35 mg/kg dry 3529 0.420 54 75-125 3 20 MI Chromium 126 0.35 mg/kg dry 35.30 91.9 96 75-125 0.4 20 Lead 28.9 0.35 mg/kg dry 35.30 6.51 63 75-125 0.1 20 MI Selenium 22.1 0.71 mg/kg dry 3529 BRL 63 75-125 5 20 MI Silver 12.0 0.35 mg/kg dry 14.12 BRL 85 75-125 3 20 Post Spike (P700320-PS7) Source: 7070278.01 Prepared & Analyzed: 07/21/17 Arsenic 2.35 mglL 1.000 1.63 72 80-120 MI Barium 5.55 mg/L 1.000 4.88 67 80-120 E, MC Cadmium 0.579 mg/L 1.000 0.0120 57 80-120 M1 Chromium 3.29 mg/L 1.000 2.63 66 80-120 MI Lead 0.824 mg/L 1.000 0,186 64 80-120 MI Selenium 0.580 mg/L 0.9998 -0.166 58 80-120 MI Silver 0.337 mg/L 0.4000 -0.00622 84 80-120 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Read - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Page 47 of 50 Sample Extraction Data Prep Method: 3546 Lab Number Batch Initial Final Date/rime 7070278-01 P7130258 30.05 g 1 mL 07/18/17 12:65 Prep Method: 3550C GC Lab Number Batch Initial Final Date/rime 7070278-02 P7130460 30.04 g 1 mL 07/28/17 13:30 Prep Method: 5035 Lab Number Batch Initial Final Daternme 7070278-01 P7GG359 5.21 g 5 mL 07/24/17 14:25 7070278-02 P7G0359 4.87 g 5 mL 07/24/17 14:25 Prep Method: Solids, Dry Weight Lab Number Batch Initial Final Daterrime 7070278-01 P7G0278 30 g 30 g 07/18/17 1430 7070278-02 P7G0278 30 g 30 g 07/18/17 1430 7070278-03 P7G0278 30 g 30 g 07/18/17 14:30 7070278-04 P7G0278 30 g 30 g 07/18/17 14:30 7070278-05 P7G0278 30 g 30 g 07/18/17 14:30 7070278-06 P7G0278 30 g 30 g 07/18/17 14:30 7070278-07 P7G0278 30 g 30 g 07/18/17 14:30 7070278-08 P7G0278 30 g 30 g 07/18/17 14:30 Prep Method: 3546 Lab Number Batch Initial Final Daternme 7070278-03 P7G0259 30.04 g 1 mL 07118/17 12:55 7070278-04 P7130259 30.01 g 1 mL 07/18/17 12:55 7070278-05 P7G0259 30.11 g 1 mL 07/18/17 12:55 7070278-06 P7G0259 30.06 g 1 mL 07/18/17 12:65 7070278-07 P7130259 30.12 g i mL 07/18/17 12:65 7070278-08 P7G0259 30.03 g 1 mL 07/18/17 12:55 Prep Method: 3959E Lab Number Batch Initial Final Data/rime 7070278-01 P7G0320 2.01 g 50 mL 67/21/17 8:00 7070278-02 P7G0320 2.01 g 50 mL 07/21/17 8:00 7070278-03 P7G0320 1.99 g 50 mL 07/21/17 8:00 7070278-03 P7G0320 1.99 g 50 mL 07/21/17 8:00 7070278-04 P7G0320 1.98 g 50 mL 07/21/17 8:00 7070278-04 P7130320 1.98 g 50 mL 07/21/17 8:00 7070278-05 P7G0320 2 g 50 mL 07/21/17 8:00 7070278-05 P7G0320 2 g 50 mL 07/21/17 8:00 7070278-05 P7G0320 2 g 50 mL 07/21/17 8:00 7070278-06 P7G0320 1.99 g 50 mL 07/21/17 8:00 7070278-06 P7130320 1.99 g 50 mL 07/21/17 8:00 7070278-07 P7G0320 1.96 g 60 mL 07/21/17 8:00 7070278-07 P7G0320 1.96 g 50 mL 07/21/17 8:00 7070278-08 P7G0320 2.01 g 50 mL 07/21/17 8:00 7070278-08 P7G0320 2.01 g 50 mL 07/21/17 8:00 Prep Method: 3060A Lab Number Batch Initial Final Daternme 7070278-03 P7G0274 2.51 g 100 mL 07/21/17 10:55 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Read - P.O. Box 240543 - Charlotte, NC 282244)543 Phone: 704/629-6364-Tall Free Number: l-8001529-6364-Fax: 704/5254M Page 48 Df 50 Sample Extraction Data Prep Method: 3060A Lab Number Batch Initial Final Date/rime 7070278-04 P7G0274 2.48 g 100 mL 07/21/17 10:55 7070278-05 P7G0274 2.54 g 100 mL 07/21/17 10:55 7070278-06 P7G0274 2.52 g 100 mL 07121117 10:55 7070278-07 P7G0274 2.47 g 100 mL 07/21/17 10:55 7070278-08 P7G0274 2.53 g 100 mL 07/21/17 10:55 Prep Method: 7471 B Lab Number Batch Initial Final Date/Time 7070278-03 P7G0287 0.59 It 50 mL 07/20/17 8:00 7070278-04 P7G0287 0.59 g 50 mL 07/20/17 8:00 7070278-05 P7G0287 0.58 g 50 mL 07/20/17 8:00 7070278-06 P7G0287 0.58 g 50 mL 07/20/17 8:00 7070278-07 P7G0287 0.56 g 50 mL 07/20/17 8:00 7070278-08 P7G0287 0.65 g 50 mL 07/20/17 8:00 Prep Method: 5035 Lab Number Batch Initial Final Date/rime 7070278-03 P7G0413 11.24 g 5 mL 07/26/17 8:06 7070278-04 P7GO413 5.14 g 5 mL 07/26/17 806 7070278-05 P7G0413 8.22 g 5 mL 07/26/17 806 7070278-06 P7G0413 5.94 g 5 mL 07/26/17 8:06 7070278-07 P7G0413 5.04 g 5 mL 07/26/17 8:06 7070278-08 P7G0413 4.43 g 5 mL 07/26/17 8:06 This report should not be reproduced, except in its enthety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704IS29-6364 - Toll Free Number: 1.800/629-6364.1 ": 7041525-0409 Page 49 of 50 O o90 I $ In 3 a;FaOM � e o IL o o c c T Z T w •e n�° pmm c^ 0 B < a y z m O I '.. C .. n0a aw mn ' m a F1 3 6 c`. C. O =NoLp P. mo A N r S CC c ? d a� _ O H Sol 39oz�v ma_ ° = ti Zr •spy c � m 3_. c O 05 x a a �i i 9 m m ,c oz tD.'� � p a wa ��r Z n i^'ow m m C1 m m g 0 OOA a A °ate- Or° D i ma O ay�m wn'o w ° - 4, s„mmao$ ^figo vme � Of+ „ �m w o~ nC n n Zr%00 o l dw m;o y o o ado T z= m r v 7 o m c a o 0 ° m y m Z a n pp m o I S m Q Q w I zC w m m F o � r E. Z �O 3 m ac CD 5 3 Ji ;r n t` h a 3 C K 5so w D - C n M Y [ 9 S m F°n Fo % �>RL A e ,C,ww W c _. m v m y 9 r n m pp r 30 � �"PRISM r:._- 1A90aATOnIE$ INC. Geoscience Group Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 NC Certification No. 402 Full -Service Analytical & NC Drinking Water Cert No, 37735 Environmental Solutions SC Certification No. 99012 Project: Truck Part Service Lab Submittal Date: 07120/2017 Prism Work Order: 7070346 Case Narrative 08/03/2017 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. a"_1 Angela D. Overcash VP Laboratory Services Reviewed By Angela D. Overcash VP Laboratory Services Data Qualifiers Key Reference: A The CCV result is below the established QC limits. This compound was not detected in samples down the MDL. D RPD value outside of the control limits. J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag). L Parameter reported with possible low bias. LCS recovery below the QC limit. L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 24OS43 - Charlotte, NC 26224-0643 Phone: 7041529-6364-Toll Free Number: 1400/529-6364 - Fm: 7041525-0409 Page 1 of 31 PER I S n V%� Full -Service Pnalyticel 6 1 I1E$r�' Envlmnmental Solullons Sample Receipt Summary 08/03/2017 Prism Work Order: 7070346 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received TWA 7070346-01 Water 07/20/17 07/20/17 TW-2 7070346-02 Water 07/20/17 07/20/17 TW-3 7070346-03 Water 07/20/17 07/20/17 Samples were received at 21.3 degrees C. See case narrative for further information. This report should not be reproduced, except in its entirety, without the written consent of Prism Labondor es, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041526-0409 Page 2 of 31 Fum ll-Service Analytical & R ISM I Envlronental Solutions ..Yffie'. "..,aa,Es.,.. Summary of Detections 08103/2017 Prism Work Order: 7070346 Prism ID Client ID Parameter Method Result Units 7070346-01 TW-1 C9-C18 Aliphatics MADEPEPH 480 ug/L 7070346-01 TW-1 C11-C22 Aromatics MADEP EPH 860 ug/L 7070346-01 TWA 1-Methylnaphthalene 8270D 130 ug/L 7070346-01 TW-1 2-Methylnaphthalene 8270D 170 ug/L 7070346-01 TWA Diethyl phthalate 8270D 64 ug/L 7070346-01 TWA Naphthalene 8270D 280 ug/L 7070346-01 TWA 1,2,4-Trimethylbenzene 8260E "0 ug/L 7070346-01 TW-1 1,3,5-Trimethylbenzene 8260E 35 ug/L 7070346-01 TW-1 4-Isopropyltoluene 82608 15 ug/L 7070346-01 TWA Acetone 8260E 21 ug/L 7070346-01 TWA Benzene 8260B 2.4 ug/L 7070346-01 TWA Ethylbenzene 8260B 95 ug/L 7070346-01 TWA Isopropylbenzene (Cumene) 8260E 24 ug/L 7070346-01 TWA m,p-Xylenes 8260E 150 ug/L 7070346-01 TWA Methyl Isobutyl Ketone 8260E 1.5 1 ug/L 7070346-01 TWA Naphthalene 8260E 810 ug/L 7070346-01 TWA n-Butylbenzene 8260E 16 ug/L 7070346-01 TW-1 n-Propylbenzene 8260E 29 ug/L 7070346-01 TWA o-Xylene 8260E 90 ug/L 7070346-01 TWA sec-Butylbenzene 8260E 12 ug/L 7070346-01 TWA tert-Butylbenzene 8260B 4.2 ug/L 7070346-01 TWA C5-C8 Aliphatics MADEPVPH 120 ug/L 7070346-01 TW-1 C9-C12 Aliphatics MADEPVPH 2400 ug/L 7070346-01 TW-1 C9-Cl0 Aromatics MADEPVPH 1500 ug/L 7070346-03 TW-3 Chloroform 8260B 2.1 ug/L 7070346-03 TW3 Tnchloroethylene 8260B 0.51 ug/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1.800/529-6364 - Fax: 704/525-0409 Page 3 of 31 efl Fe11 Ss mice AnalyVcal x SeM Envbenmeme solutio�e Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Sample Matrix: Water Laboratory Report 08/0312017 Client Sample ID: TW-1 Prism Sample ID: 7070346-01 Prism Work Order: 7070346 Time Collected: 07/20/17 14:13 Time Submitted: 07/20/17 16:40 Parameter Result Units Report MOIL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9L78 Allphatim 480 ug/L 350 22 1 MADEP EPH 7/27117 14:57 ZRC P7G0415 C19-C36 Aliphatics BRL ug/L 500 63 1 MADEP EPH 7/27/17 14:57 ZRC P7G0415 C11-C22 Aromatics 860 ug/L 100 55 1 MADEP EPH 7127117 14:57 ZRC P7G0415 Surrogate Recovery Control Limits 1-Chlorooctadecane 41 % 40-140 o-Terphenyl 52 % 40-140 2-Fluorobiphenyl 90 % 40-140 2-Bromonaphthalene 99 % 40-140 Semivolatile Organic Compounds by GC/MS 1,2,4-Tdchlorobenzene BRL ug/L 15 2.7 1 8270D 7/25/17 16:10 JMV P7G0369 1,2-Dichlorobemene BRL ug/L 15 2.5 1 8270D 7125117 16:10 JMV P7G0369 1,3-Dichlorobenzene BRL ug/L 15 2.9 1 8270D 7/25/17 16:10 JMV P7G0369 1A-Dichlorobenzene BRL ug/L 15 2.5 1 8270D 7/25117 16:10 JMV P7G0369 1-Methylnaphthalene 130 ug/L 15 4.0 1 8270D 7125117 16:10 JMV P7G0369 2,4,5-Trichlorophenol BRL ug/L 15 2.5 1 8270D 7/25/17 16:10 JMV P7G0369 2,4,6-Tdchlorophenol BRL ug/L 15 2.8 1 8270D 7/25/17 16:10 JMV P7G0369 2,4-Dichlorophenol BRL ug/L 15 3.9 1 8270D 7/26117 16:10 JMV P7G0369 2,4-Dimethylphenol BRL ug/L 15 5.3 1 8270D 7/25/17 16:10 JMV P7G0369 2,4-Dinttrophenol BRL ug/L 15 4.2 1 8270D 7125/17 16:10 JMV P7G0369 2,4-Dinibotoluene BRL ug/L 15 2.2 1 8270D 7125/17 16:10 JMV P7G0369 2,6-DiniOotoluene BRL ug/L 15 1.7 1 8270D 7/25/17 16:10 JMV P7G0369 2-Chloronaphthelene BRL ug/L 15 4.2 1 8270D 7/25117 16:10 JMV P7G0369 2-Chlorophenol BRL ug/L 15 2.9 1 8270D 7/25/17 16:10 JMV P7G0369 2-Methylnaphthalene 170 ug/L 15 3.7 1 6270D 7r25/1716:10 JMV P7G0389 2-Methylphenol BRL ug/L 15 2.8 1 8270D 7125/17 16:10 JMV P7G0369 2-Nitroaniline BRL ug/L 15 2.2 1 8270D 7/25/17 16:10 JMV P7130369 2-Nitrophenol BRL ug/L 15 3.6 1 8270D 7/25117 16:10 JMV P7G0369 3,3'-Dichlorobemidine BRL ug/L 15 2.2 1 8270D 7/25/17 16:10 JMV P7G0369 3/4-Methylphenol BRL ug/L 15 2.4 1 8270D 7/25/17 16:10 JMV P7G0369 3-Nitroanilins BRL ug/L 15 2.1 1 8270D 7/25117 16:10 JMV P7G0369 4,6-Dinitro-2-methylphenol BRL ug/L 15 2A 1 8270D 7/25/17 16:10 JMV P7G0369 4-Bromophenyl phenyl ether BRL ug/L 15 2.0 1 8270D 7/25/17 16:10 JMV P7130369 4-Chloro3methylphenol BRL ug/L 15 3.6 1 8270D 7125/17 16:10 JMV P7G0369 4-Chlomaniline BRL ug/L 15 3.8 1 8270D 7/25/17 16:10 JMV P7G0369 4-Chlorophenyl phenyl ether BRL ug/L 15 2.0 1 8270D 7125/17 16:10 JMV P7G0369 4-Nitroaniline BRLA ug/L 15 1.4 1 8270D 7/25117 16:10 JMV P7G0369 4-Nitrophenol BRL ug/L 15 0.92 1 8270D 7/25/17 16:10 JMV P7G0369 Acenaphthene BRL ug/L 15 2.8 1 82701) 7/25117 16:10 JMV P7G0369 Acenaphthylene BRL ug/L 15 3.1 1 8270D 7/25/17 16:10 JMV P7G0369 Aniline BRL ug/L 15 3.7 1 8270D 7/25/17 16:10 JMV P7G0369 Anthrecene BRL ug/L 15 2.2 1 8270D 7/25/17 16:10 JMV P71210369 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224.OS43 Phone: 7041529.6364 - Toll Free Number: 1.800/529-6364 - Fax: 704/5254409 Page 4 of 31 P R I SeM FWbServlce Anal ical & Envl.cnmanta se n, ons Laboratory Report 08/03/2017 Geoscience Group Project: Truck Part Service Client Sample ID: TW-1 Attn: Tom Hassett Prism Sample ID: 7070346-01 500-K Clanton Rd. Prism Work Order: 7070346 Charlotte, NC 28217 Sample Matrix: Water Time Collected: 07/20/17 14:13 Time Submitted: 07/20/17 16:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date rime ID Azobenzene BRL ug/L 15 2.8 1 8270D 7125/17 16:10 JMV P7G0369 Benzo(a)anthracene BRL ug/L 15 2.2 1 8270D 712511716:10 JMV P7G0369 Benzo(a)pyrene BRL ug/L 15 2.2 1 8270D 7/25117 16:10 JMV P7G0369 Benzo(b)fluoranthene BRL ug/L 15 1.8 1 11270D 7/25/17 16:10 JMV P7G0369 Benzo(g,h,i)perylene BRL ug/L 15 2.1 1 8270D 7/25/17 16:10 JMV P7G0369 Benzo(k)fluorenthene BRL ug/L 15 2.2 1 8270D 7125/17 16:10 JMV P7G0369 Benzoic Acid BRL ug/L 150 7.2 1 82700 7/25117 16:10 JMV P7G0369 Benzyl alcohol BRL ug/L 15 3.3 1 8270D 7/25/17 16:10 JMV P7G0369 bis(2-Chloroethoxy)methane BRL ug/L 15 4.0 1 8270D 7/25/17 16:10 JMV P7G0369 Bis(2-ChlomethyWther BRL ug/L 15 3.6 1 8270D 7/25117 16:10 JMV P7G0369 Bis(2-chloroisopropylether BRL ug/L 15 3.0 1 8270D 7125/17 16:10 JMV P7G0369 Sis(2-Ethylhexyl)phthalate BRL ug/L 15 2.0 1 8270D 7/25117 16:10 JMV P7G0369 Butyl benzyl phthalate BRL ug/L 15 2.1 1 8270D 7/25117 16:10 JMV P7G0369 Chrysene BRL ug/L 15 2.2 1 8270D 7/25117 16:10 JMV P7G0369 Dibenzo(a,h)anthracene BRL ug/L 15 1.8 1 8270D 7/25/17 16:10 JMV P7G0369 Dibenzofuran BRL ug/L 15 2.7 1 8270D 7/25117 16:10 JMV P7G0369 Diethyl phthalate 64 ug/L 15 5.1 1 8270D 7125117 16:10 JMV P700369 Dimethyl phthalate BRL ug/L 15 2.2 1 8270D 7/25117 16:10 JMV P7G0369 Di-n-butyl phthalate BRL ug/L 15 2.6 1 8270D 7125/17 16:10 JMV P7G0369 Di-n-octyl phthalate BRL ug/L 15 2.0 1 8270D 7/25/17 16:10 JMV P7G0369 Fluoranthene BRL ug/L 15 2.6 1 8270D 7/25/17 16:10 JMV P7G0369 Fluorene BRL ug/L 15 2.6 1 8270D 7125/17 16:10 JMV P7G0369 Hemchlorobenzene BRL ug/L 15 2.0 1 8270D 7/25/17 16:10 JMV P7G0369 Hexachlorobutediene BRL ug/L 15 3.3 1 8270D 7125/17 16:10 JMV P7G0369 Hexachlorocydopentadiene BRL ug/L 15 2.7 1 8270D 7/25/17 16:10 JMV P7G0369 Hexachlorcethane BRL ug/L 15 2.7 1 8270D 712511716:10 JMV P7G0369 Indeno(1,2,3.od)pyrene BRL ug/L 15 6.0 1 8270D 7/25/17 16:10 JMV P7G0369 Isophorone BRL ug/L 15 3.9 1 8270D 712511716:10 JMV P7G0369 Naphthalene 280 ug/L 15 4.0 1 82700 712511716:10 JMV P7G0369 Nitrobenzene BRL ug/L 15 3.9 1 8270D 7125/17 16:10 JMV P7G0369 N-Niboso-di-n-propylamine BRL ug/L 15 3.4 1 8270D 7125/17 16:10 JMV P7G0369 N-Nitrosodiphenylarnme BRL uglL 15 2.0 1 8270D 7/25/17 16:10 JMV P7G0369 Pentachlorophenol BRL ug/L 15 1.9 1 8270D 7125/17 16:10 JMV P7G0369 Phenanthrene BRL ug/L 15 2.3 1 8270D 7/25117 16:10 JMV P7G0369 Phenol BRL ug/L 15 1.5 1 8270D 7/25117 16:10 JMV P7G0369 Pyrene BRL ug/L 15 2.2 1 8270D 725/17 16:10 JMV P7G0369 Surrogate Recovery Control Limits 2,4,6-Tdbromophenol 87% 43-140 2-Fluorobiphenyl 77 % 44-119 2-Fluorophenol 53 % 19-119 Nitrobenzened5 64 % 44-120 Phenold5 43 % 11-52 Terphenyld14 96% 50-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 2405" - Charlotte, NC 28224-0643 Phone: 704152963" -Toll Free Number: 1-800/52963" - Fax: 704/525-0409 Page 5 of 31 PR ISM I Full-ServlceAnalytical & Laboratory Report Environmental Solutions 08/03/2017 Geoscience Group Project: Truck Part Service Client Sample ID: TW-1 Attn: Tom Hassett Prism Sample ID: 7070346-01 500-K Clanton Rd. Prism Work Order: 7070346 Charlotte, NC 28217 Sample Matrix: Water Time Collected: 07/20/17 14:13 Time Submitted: 07/20/17 16:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/rime ID Volatile Organic Compounds by GC/MS 1,1,1,2-Tatrachloroethans BRL ug/L 0.50 0.11 1 8260B 7/31117 18:18 KOM P7G0491 11,1-Tdchloroethane BRL ug/L 0.50 0.061 1 8260B 7/31117 18:18 KOM P7GO491 1,1,2,2-Tetrachloroethane BRL ug/L 0.50 0.036 1 8260B 7131/17 18:18 KOM P7GO491 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260B 7131117 18:18 KOM P7G0491 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 8260B 7/31/17 18:18 KOM P7G0491 1,1-Dichiorcethylene BRL ug/L 0.50 0.083 1 8260B 7/31/17 18:18 KOM P7GO491 1,1-Dohlompropylene BRL ug/L 0.50 0.051 1 8260B 7/31/17 18:18 KOM P7GO491 1,2,3-Tdchiorobemene BRL ug/L 2.0 0.40 1 8260B 7/31117 18:18 KOM P7G0491 1,2,3-Tdchloropropane BRL ug/L 1.0 0.14 1 8260B 7131/17 18:18 KOM P7130491 1,2,4-Tdchlombenzene BRL ug/L 1.0 0.13 1 8260B 7/31117 18:18 KOM P7G0491 1,2,4-Trlmethylbenzene 440 ug/L 5.0 0.54 10 8260B 7131117 18:44 KOM P700491 1,2-Dibromo-3-chloropmpane BRL ug/L 2.0 0.17 1 8260B 7/31117 18:18 KOM P7G0491 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 8260B 7131/17 18:18 KOM P7GO491 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260B 7/31117 18:18 KOM P7G0491 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 8260B 7/31/17 18:18 KOM P7130491 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260B 7/31/17 18:18 KOM P7G0491 1,3,5.Trimethylbenzene 35 ug/L 0.50 0.076 1 8260B 7/31117 18:18 KOM P7G0491 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260B 7/31117 18:18 KOM P7G0491 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260B 7/31/17 18:18 KOM P7G0491 1,4-Dichiorobemene BRL ug/L 0.50 0.050 1 8260B 7/31117 18:18 KOM P7GO491 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260B 7/31/17 18:18 KOM P7GO491 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260B 7/31/17 18:18 KOM P7GO491 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260B 7131117 18:18 KOM P7GO491 44sepropyltoluene 15 ug/L 0.50 0.089 1 82608 7/31/17 18:18 KOM P7GO491 Acetone 21 ug/L 5.0 0.31 1 8260B 7131117 18:18 KOM P760491 Acrolein BRL ug/L 20 0.20 1 82608 7/31/17 18:18 KOM P7130491 Acrylonitdle BRL ug/L 20 0.20 1 8260B 7131117 18:18 KOM P7GO491 Benzene 2.4 ug/L 0.50 0.048 1 8260B 7131117 18:18 KOM P7GO491 Bromobenzene BRL ug/L 0.50 0.067 1 8260B 7/31/17 18:18 KOM P7G0491 Bromochloromethane BRL ug/L 0.50 0.14 1 8260B 7131117 18:18 KOM P7GO491 Bromodichloromethane BRL ug/I. 0.50 0.062 1 8260B 7/31/17 18:18 KOM P7G0491 Bromofoml BRL ug/L 1.0 0.040 1 82608 7/31117 18:18 KOM P7130491 Bromomethane BRL ug/L 1.0 0.18 1 8260B 7131/17 18:18 KOM P7GO491 Carbon disuaide BRL ug/L 5.0 0.075 1 8260B 7/31/17 18:18 KOM P7GO491 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260B 7131/17 18:18 KOM P7GO491 Chlorobenzene BRL ug/L 0.50 0.062 1 8260B 7/31/17 18:18 KOM P7GO491 Chioroethane BRL ug/L 0.50 0.22 1 8260B 7/31/17 18:18 KOM P7G0491 Chloroform BRL ug/L 0.50 0.076 1 8260B 7/31117 18:18 KOM P7G0491 Chloromethene BRL ug/L 0.50 0,079 1 8260B 7131/17 18:18 KOM P7G0491 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.056 1 8260B 7/31/17 18:18 KOM P7GO491 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260B 7/31117 18:18 KOM P7G0491 Dibromochloromethene BRL ug/L 0.50 0.081 1 8260B 7/31/17 18:18 KOM P7GO491 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spdngbrook Road - P.O. Box 240543 - Charlotte, NC 26224-0643 Phone: 7041529-6364 - Tall Free Number: l-900/529-0364- Fax: 70415254409 Page 6of 31 &MIJI,ISM Laboratory Report Full -Service Analytical 8 Enmmnmema� smmlo"s OB/03/2017 , uaaa„� Ill .� Geoscience Group Project: Truck Part Service Client Sample ID: TW-1 Attn: Tom Hassett Prism Sample ID: 7070346-01 500-K Clanton Rd. Prism Work Order: 7070346 Charlotte, NC 28217 Sample Matrix: Water Time Collected: 07/20/17 14:13 Time Submitted: 07/20/17 16:40 Parameter Result Units Report MOIL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Dibromomethans BRL ug/L 0.50 0.065 1 8260B 7/31/17 18:18 KDM P7G0491 Dichlorodifluoromethane BRL ug/L 1.0 0.11 1 8260B 7131/17 18:18 KDM P7G0491 Ethylbenzene 95 u91L 5.0 0.61 10 B2608 7/31/1718:44 KDM P7G0491 Hexachlorobutediene BRL ug/L 2.0 0.16 1 8260B 7/31/17 18:18 KDM P7G0491 Isopropyl Ether BRL ug/L 0.50 0.050 1 8260B 7131/17 18:18 KDM P7G0491 Isopropylbenzene (Cumene) 24 ug/L 0.50 0.054 1 6269B 7131/17 18:18 KDM P7430491 m,p-Xylenes 150 ug/L 1.0 0.12 1 826013 7131117 18:18 KDM P760491 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260B 7/31/17 18:18 KDM P7G0491 Methyl Ethyl Ketone (2-Butenone) BRL ug/L 5.0 0.24 1 8260B 7131/17 18:18 KDM P7G0491 Methyl Isobutyl Ketone 1.5 J ug/L 5.0 0.078 1 8260B 7131117 18:18 KDM P7G0491 Methylene Chloride BRL ug/L 1.0 0.083 1 8260B 7/31117 18:18 KDM P7G0491 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 8260B 7/31/17 18:18 KDM P7G0491 Naphthalene 810 ug/L 10 1.9 10 82608 713111718:44 KDM P7G0491 n-ButAbenzene 16 ug/L 1.0 0.076 1 0260B 7131117 18:18 KDM P7G0491 n-Propylbenzene 29 ug/L 0.50 0.087 1 8260B 7131117 18:18 KDM P700491 o.Xylene 90 ug/L 0.50 0.044 1 8260B 7131/17 18:18 KDM P760491 sec-Butylbenzene 12 ug/L 0.50 0.076 1 8260B 7131/17 18:18 KDM P7GW91 Styrene BRL ug/L 0.60 0.047 1 8260B 7/31117 18:18 KDM P7G0491 tent-Butylbenzene 4.2 ug/L 0.50 0.088 1 B260B 7131/17 18:18 KDM P7G0491 Tetrachloroethylene BRL ug/L 0.50 0.098 1 8260B 7/31117 18:18 KDM P7G0491 Toluene BRL ug/L 0.50 0.044 1 8260B 7/31117 18:18 KDM P7130491 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 8260B 7131/17 18:18 KDM P7G0491 trans-1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 B260B 7/31117 18:18 KDM P7G0491 TdchloroethNene BRL ug/L 0.50 0.078 1 8260B 7131117 18:18 KDM P7G0491 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 8260B 7/31/17 18:18 KDM P7G0491 Vinyl acetate BRL ug/L 2.0 0.060 1 8260B 7/31/17 18:18 KDM P7G0491 Vinyl chloride BRL ug/L 0.50 0.097 1 8260B 7/31117 1898 KDM P7G0491 Surrogate Recovery Control Limits 4-13mmofluorobenzene 97 % 80-124 Dibromofluoromethane 105 % 75-129 Toluene-d8 94 % 77-123 Volatile Petroleum Hydrocarbons by GC/PID/FID C6-C8 Allphatc 120 ug1L 50 6.1 1 MADEP VPH 7127117 19:30 ANG P760439 C9-C12 Aliphatic 2400 u91L Soo 19 10 MADEPVPH 7/28M7 9:41 ANG P700439 C9-C10 Aromatic 1500 ug/L Soo 2.8 10 MADEP VPH 7128/17 9:41 ANG P7430439 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 86 % 70-130 2,5-Dibromotoluene(FID) 101 % 70-130 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 2822"543 Phone: 704/529-0364-Toll Free Number. l-600/529-6364-Fax:7041625-0409 Page7of31 IFWbService sriR ISM Environmental Solutions Laboratory Report 08/03/2017 Geoscience Group Project: Truck Part Service Client Sample ID: TW-2 Attn: Tom Hassett Prism Sample ID: 7070346-02 600-K Clanton Rd. Prism Work Order: 7070346 Charlotte, NC 28217 Sample Matrix: Water Time Collected: 07/20/17 14:32 Time Submitted: 07/20/17 16:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/rime ID Semivolatile Organic Compounds by GC/MS 1,2,4-Tdchlorobenzene BRL ug/L 10 1.8 1 8270D 7/25117 16:32 JMV P7130369 1,2-Dichlombenzene BRL ug/L 10 1.6 1 8270D 7125/17 16:32 JMV P7G0369 1,3-Dichlorobenzene BRL ug/L 10 1.9 1 8270D 7/25/17 16:32 JMV P7130369 1,4-Dichlorobenzene BRL ug/L 10 1.6 1 8270D 725/17 16:32 JMV P7130369 1-Methylnaphthalene BRL ug/L 10 2.6 1 8270D 7/25/17 16:32 JMV P7G0369 2,4,5-Trichlorophenol BRL ug/L 10 1.6 1 82700 725117 16:32 JMV P7G0369 2,4,6-Tdchlorophenol BRL ug/L 10 1.8 1 B270D 7/25117 16:32 JMV P7130369 2,4-Dichlorophenol BRL ug/L 10 2.6 1 8270D 7125/17 16:32 JMV P7G0369 2,4-Dimethylphenol BRL ug/L 10 3A 1 8270D 7125/17 16:32 JMV P7G0369 2.4-Dinitmphenol BRL ug/L 10 2.7 1 8270D 725117 16:32 JMV P7430369 2,4-Dinibotoluene BRL ug/L 10 1.4 1 8270D 7125/17 16:32 JMV P7G0369 2.6-Dinitrotoluene BRL ug/L 10 1.1 1 8270D 725117 16:32 JMV P7130369 2-Chloronaphthalene BRL ug/L 10 2.7 1 8270D 7125117 16:32 JMV P7G0369 2-Chlorophenol BRL ug/L 10 1.9 1 8270D 725/17 16:32 JMV P7130369 2-Methylnaphthalene BRL ug/L 10 2.4 1 8270D 7125117 16:32 JMV P7G0369 2-Methylphenol BRL ug/L 10 1.8 1 8270D 725117 16:32 JMV P7G0369 2-Nitroaniline BRL ug/L 10 1A 1 8270D 7125117 16:32 JMV P7G0369 2-Nitrophenol BRL ug/L 10 2.4 1 a270D 725117 16:32 JMV P7G0369 3,3'-Dichlorobenzidine BRL ug/L 10 1.4 1 8270D 7/25117 16:32 JMV P7GD369 3/4-Methylphenol BRL ug/L 10 1.5 1 8270D 726117 16:32 JMV P7G0369 3-Nitroaniline BRL ug/L 10 1A 1 8270D 7/25117 16:32 JMV P7G0369 4,6-Dlntbo-2-methylphenol BRL ug/L 10 1.4 1 8270D 7125117 16:32 JMV P7430369 4-Bmmophenyl phenyl ether BRL ug/L 10 1.3 1 8270D 7/25117 16:32 JMV P7G0369 4-Chloro-3-methylphenol BRL ug/L 10 2.4 1 8270D 725117 16:32 JMV P7130369 4-Chloroaniline BRL ug/L 10 2A 1 8270D 7/2611716:32 JMV P7130369 4-Chlorophenyl phenyl ether BRL ug/L 10 1.3 1 82700 726117 16:32 JMV P7G0369 4-Nitroaniline BRLA ug/L 10 0.93 1 8270D 7/25/17 16:32 JMV P7G0369 4-Nitrophenol BRL ug/L 10 0.60 1 B270D 7/25/17 16:32 JMV P7G0369 Aoenaphthene BRL ug/L 10 1.8 1 8270D 7/25117 16:32 JMV P7130369 Acenaphthylene BRL ug/L 10 2.0 1 8270D 7125/17 16:32 JMV P7G0369 Aniline BRL ug/L 10 2.4 1 8270D 725117 16:32 JMV P7130369 Anthracene BRL ug/L 10 1.4 1 8270D 7125/17 16:32 JMV P7130369 Azobenzene BRL ug/L 10 1.8 1 8270D 7125/17 16:32 JMV P7G0369 Benzo(a)anthracene BRL ug/L 10 1.4 1 8270D 7/25117 16:32 JMV P7GD369 Benzo(a)pyrene BRL ug/L 10 1.4 1 8270D 725/17 16:32 JMV P7G0369 Benzo(b)0uomnthene BRL ug/L 10 1.1 1 8270D 7/25117 16:32 JMV P7430369 Benzo(g,hJ)peMene BRL ug/L 10 1.4 1 8270D 7125117 16:32 JMV P7G0369 Benzo(k)(luoranthene BRL ug/L 10 1.4 1 8270D 7/25/17 16:32 JMV P7430369 Benzoic Acid BRL ug/L 100 4.7 1 8270D 7/25/17 16:32 JMV P7G0369 Benzyl alcohol BRL ug/L 10 2.1 1 8270D 7125/17 16:32 JMV P7130369 bis(2-Chloroethoxy)methane BRL ug/L 10 2.6 1 a270D 7/25/17 16:32 JMV P7130369 Bis(2-Chlomethyl)ether BRL ug/L 10 2.3 1 8270D 725/17 16:32 JMV P7G0369 This report should not be reproduced, except in its entirety, without the wrdten consent of Prism Laboratories, Inc. 449 8pringbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 704/529-6384 - Toll Free Number: 14001529-6364 - Fax: 7041526-0409 Page 8 of 31 I") ump�Es�xc Environmental Solutions -RISM Laboratory Report 08/03/2017 Geoscience Group Project: Truck Part Service Client Sample ID: TW-2 Attn:Tom Hassett Prism Sample ID: 7070346-02 500-K Clanton Rd. Prism Work Order: 7070346 Charlotte, NC 28217 Sample Matrix: Water Time Collected: 07/20/17 14:32 Time Submitted: 07/20/17 16:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Daterrime ID Bis(2-chloroisopropyl)ether BRL ug/L 10 2.0 1 8270D 7125/17 16:32 JMV P7G0369 Bis(2-Ethylhexyl)phthalate BRL ug/L 10 1.3 1 8270D 7125/17 16:32 JMV P7G0369 Butyl benzyl phthalate BRL ug/L 10 1.4 1 8270D 7125/17 16:32 JMV P7130369 Chrysene BRL ug/L 10 1.4 1 8270D 7/25/17 16:32 JMV P7G0369 Dibenzo(a,h)anthracene BRL ug/L 10 1.2 1 8270D 7/25117 16:32 JMV P7G0369 Dibenzofuran BRL ug/L 10 1.8 1 8270D 7125/17 16:32 JMV P7G0369 Diethyl phthalate BRL ug/L 10 3.3 1 8270D 7/25/17 16:32 JMV P7G0369 Dimethyl phthalate BRL ug/L 10 1.4 1 8270D 7/25/17 16:32 JMV P7G0369 Di-n-butyl phthalate BRL ug/L 10 1.7 1 8270D 7125117 16:32 JMV P7G0369 Di-n-octyl phthalate BRL uglL 10 1.3 1 8270D 7125/17 16:32 JMV P7G0369 Fluoranthene BRL ug/L 10 1.7 1 8270D 7125/17 16:32 JMV P7130369 Flucrene BRL ug/L 10 1.7 1 8270D 7/25/17 16:32 JMV P7G0369 Hexachlorobenzene BRL ug/L 10 1.3 1 8270D 7125/17 16:32 JMV P7G0369 Hexachlorobutediene BRL ugli- 10 2.1 1 8270D 7/25/17 16:32 JMV P7G0369 Hexachlorocyclopentadiene BRL ug/L 10 1.7 1 8270D 7/25/17 16:32 JMV P7130369 Hexachlomethane BRL ug/L 10 1.7 1 8270D 7/25117 16:32 JMV P7G0369 Indeno(1,2,3-cd)pyrene BRL ug/L 10 3.9 1 8270D 725117 16:32 JMV P7G0369 Isophorone BRL ug/L 10 2.5 1 8270D 7/25/17 16:32 JMV P7G0369 Naphthalene BRL ug/L 10 2.6 1 8270D 7/25/17 16:32 JMV P7G0369 Nitrobenzene BRL ug/L 10 2.6 1 8270D 7/25117 16:32 JMV P7G0369 N-Nitroso-di-n-propylamine BRL ug/L 10 2.2 1 8270D 725/17 16:32 JMV P7G0369 N-Nibosodiphenylamine BRL ug/L 10 1.3 1 8270D 725117 16:32 JMV P7G0369 Pentachlomphenol BRL ug/L 10 1.2 1 8270D 7125117 16:32 JMV P7G0369 Phenanthrene BRL ug/L 10 1.5 1 8270D 7/25/17 16:32 JMV P7G0369 Phenol BRL ug/L 10 0.98 1 B270D 7125/17 16:32 JMV P7G0369 Pyrene BRL ug/L 10 1.4 1 8270D 725/17 1632 JMV P7G0369 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 66 % 43-140 2-Fluorobiphenyl 61 % 44-119 2-Fluorophenol 41 % 19-119 Nitrobemened5 52 % 44-120 Phenol-d5 28 % 1152 Terphenyl-014 72 % 50-134 Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachlormthane BRL ug/L 0.50 0.11 1 82608 7131/17 17:28 KDM P7GD491 MA-Trichloroethane BRL ug/L 0.50 0.061 1 8260B 7/31117 17:28 KDM P7130491 1,1,2,2-Tetrachlorcethane BRL ug/L 0.50 0.036 1 8260B 7131/17 17:28 KDM P7GD491 1,1,2-Trichlorcethane BRL ug/L 0.50 0.066 1 8260B 7/31/17 17:28 KDM P7G0491 1,1-Dichloroethane BRL ug/L 0.50 0.D83 1 8260B 7131117 1728 KDM P7GD491 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260B 7/31117 17:28 KDM P7G0491 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 82609 7/31/17 17:28 KDM P7G0491 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 8260B 7131/17 17:28 KDM P7130491 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 8260B 7131/17 17:28 KDM P7G0491 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 249543 - Charlotte, NC 28224-0643 Phone: 7041529-6364 -Toll Free Number: 1.800/5294364 -Fax: 704/525-0409 Page 9 of 31 In EmFull-Service Analytical a wsorwmx,rs,xc lronmental Solutlans Laboratory Report 08/03/2017 Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, INC 28217 Project: Truck Part Service Sample Matrix: Water Client Sample ID: TW-2 Prism Sample ID: 7070346-02 Prism Work Order: 7070346 Time Collected: 07/20/17 14:32 Time Submitted: 07/20/17 16:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Daternme ID 1,2,4-Trichlorobemene BRL ug/L 1.0 0.13 1 8260B 7/31/17 17:28 KOM P7130491 1,2,4-Trimethylbenzene BRL ug/L 0.50 0.054 1 82608 7131/17 17:28 KDM P7130491 1,2-Dibiomo-3chloropropane BRL ug/L 2.0 0.17 1 8260B 7/31/17 17:28 KDM P7G0491 1,2-Dibromoethene BRL ug/L 0.50 0.051 1 8260B 7131117 17:28 KDM P7G0491 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260B 7/31117 17:28 KDM P7130491 1,2-Dichlomelhane BRL ug/L 0.50 0.066 1 8260B 7131117 17:28 KDM P7G0491 1,2-Dichlompropane BRL ug/L 0.50 0.11 1 8260B 7131/17 17:28 KDM P7130491 1,3,5-Trimethylbenzene BRL ug/L 0.50 0.076 1 8260B 7/31/17 17:28 KDM P7130491 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260B 7/31/17 17:28 KDM P7G0491 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 8260B 7/31117 17:28 KDM P7130491 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260B 7/31117 17:28 KDM P7130491 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260B 7131/17 17:28 KDM P7430491 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260B 7/31/17 17:28 KDM P7130491 4-Chlorotoluene BRL ug/L 0.50 0.050 1 8260B 7/31/17 17:28 KDM P7430491 4-Isopropyholuene BRL ug/L 9 0.50 0.089 1 82608 7/31/17 17:28 KDM P7130491 Acetone BRL ug/L 5.0 0.31 1 8260B 7/31/17 17:28 KDM P7GO491 Acrolein BRL ug/L 20 0.20 1 82608 7131/17 17:28 KOM P7430491 Acrylonibile BRL ug/L 9 20 0.20 1 82608 7/31/17 17:28 KDM P7G0491 Benzene BRL ug/L 0.50 0.048 1 8260B 7/31/17 17:28 KDM P7G0491 Bromobenzene BRL ug/L 0.50 0.057 1 8260B 7/31/17 17:28 KDM P7130491 Bromochloromethane BRL ug/L 0.50 0.14 1 8260B 7/31117 17:28 KDM P7GO491 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260B 7/31/17 17:28 KDM P7430491 Bromofonll BRL ug/L 1.0 0.040 1 82608 7/31/17 17:28 KDM P7130491 Bromomethane BRL ug/L 1.0 0.18 1 B260B 7131/17 17:28 KDM P7GO491 Carbon disulfide BRL ug/L 5.0 0.075 1 8260B 7131/17 17:28 KDM P7430491 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260E 7/31/17 17:28 KDM P7G0491 Chlorobenzene BRL ug/L 0.50 0.062 1 8260B 7/31/17 17:28 KDM P7GO491 Chloruethane BRL ug/L 0.50 0.22 1 8260B 7/31/17 17:28 KOM P7130491 Chloroform BRL ug/L 0.50 0.076 1 8260B 7/31/17 17:28 KDM P7130491 Chlommethane BRL ug/L 0.50 0.079 1 8260B 7/31/17 17:28 KDM P7GO491 cis-1,2-Dichlolnethylene BRL ug/L 0.60 0.056 1 8260B 7/31117 17:28 KDM P7130491 cis-1,3-Dichloropropylene BRL ug/L 0.60 0.079 1 8260B 7131117 17:28 KDM P7130491 Dibromochloromethane BRL ug/L 0.50 0.081 1 8260B 7/31117 17:28 KDM P7GO491 Dibromomethane BRL ug/L 0.50 0.065 1 8260B 7/31/17 17:28 KDM P7G0491 Dichlorodieuoromethane BRL ug/L 1.0 0.11 1 8260B 7/31/17 17:28 KDM P7G0491 Ethylbenzene BRL ug/L 0.50 0.061 1 8260B 7131117 17:28 KDM P7GO491 Hemchlombutadiene BRL ug/L 2.0 0.16 1 8260B 7/31117 17:28 KDM P7130491 Isopropyl Ether BRL ug/L 0.50 0.050 1 8260B 7131/17 17:28 KDM P7430491 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 82608 7131/17 17:28 KDM P7130491 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260B 7131117 17:28 KDM P7130491 Methyl Butyl Ketone (2-Hexamme) BRL ug/L 5.0 0.065 1 8260B 7131/17 17:28 KDM P7430491 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 8260B 7131117 17:28 KDM P7G0491 Methyl Isobutyl Ketone BRL ug/L 9 5.0 0.078 1 8260B 7/31/17 17:28 KDM P7130491 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.C. Box 240543 - Charlotte, NC 282244U3 Phone: 7041529.6364 - Toll Free Number: 1.8001529.6364 - Fax: 7041525-WO Page 15 of 31 �P�R i S M l FW Environmental anSolutio s Environmental Solutions Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Sample Matrix: Water Laboratory Report 08/03/2017 Client Sample ID: TW-2 Prism Sample ID: 7070346-02 Prism Work Order: 7070346 Time Collected: 07/20/17 14:32 Time Submitted: 07/20/17 16:40 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Methylene Chloride BRL ug/L 1.0 0.083 1 8260B 7/31117 17:28 KDM P7130491 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 8260E 7131/17 17:28 KDM P7G0491 Naphthalene BRL ug/L 1.0 0.19 1 8260B 7/31/17 17:28 KDM P7130491 n-Butylbenzene BRL ug/L 1.0 0.076 1 8260B 7/31117 17:28 KDM P7G0491 n-Propylbenzene BRL u /L 9 0.50 0.087 1 8260B 7/31/17 17:28 KDM P7G0491 o-Xylene BRL ug/L 0.50 0.044 1 8260B 7/31/17 17:28 KDM P7G0491 sec-Butylbenzene BRL ug/L 0.50 0.076 1 8260B 7131/17 17:28 KDM P7G0491 Styrene BRL ug/L 0.50 0.047 1 8260B 7131117 17:28 KDM P7130491 tert-Butylbenzene BRL ug/L 0.50 0.088 1 82608 7/31117 1728 KDM P7G0491 Tetrachloroethylene BRL ug/L 0.50 0.098 1 8260B 7131/17 17:28 KDM P7130491 Toluene BRL ug/L 0.50 0.044 1 a260B 7/31/17 17:28 KDM P7G0491 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 8260B 7/31/17 17:28 KDM P7G0491 trans-1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 82608 7131/17 1728 KDM P7G0491 Trichloroethylene BRL ug/L 0.50 0.078 1 8260B 7/31/17 17:28 KDM P7G0491 Trichloro9uoromethane BRL ug/L 0.50 0.062 1 8260B 7131/17 17:28 KDM P7130491 Vinyl acetate BRL ug/L 2.0 0.060 1 0260B 7/31117 17:28 KDM P7430491 Vinyl chloride BRL ug/L 0.60 0.097 1 82608 7/31/17 172A KnM P7G0441 Surrogate Recovery Control Limits 4-Bromolluorobarzene 91 % 80-124 Dibromo0uoromethane 109 % 75-129 Toluene-08 91 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529.6364 - Toll Free Number: 1.8001529.6364 - Fax: 7041526-0409 Page 11 of 31 r] pl� �t Full-5emce Analytical 8 �lfueoa ro ss we E O I Snvironmental SONt one Laboratory Report 0a/03/2017 Geoscience Group Project: Truck Part Service Client Sample ID: TW-3 Attn: Tom Hassett Prism Sample ID: 7070346-03 600-K Clanton Rd. Prism Work Order: 7070346 Charlotte, NC 28217 Sample Matrix: Water Time Collected: 07/20/17 14:41 Time Submitted: 07/20/17 16:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Datemme ID Semivolatile Organic Compounds by GCS11S 1,2,4-Trichlombenzene BRL ug/L 10 1.8 1 8270D 7125/17 16:54 JMV P7G0369 1,2-Dichlorobenzene BRL ug/L 10 1.6 1 8270D 7/25/17 16:54 JMV P7G0369 1.3-Dichlorobenzene BRL ug/L 10 1.9 1 8270D 7125/17 16:54 JMV P7G0369 1,4-Dichlorobenzene BRL ug/L 10 1.6 1 8270D 7/25117 16:54 JMV P7130369 1-Methylnaphthelene BRL ug/L 10 2.6 1 8270D 7125/17 16:54 JMV P7G0369 2,4,5-Trichlorophenol BRL ug/L 10 1.6 1 a270D 7125/17 16:54 JMV P7G0369 2,4,6-Trichlorophenol BRL ug/L 10 1.8 1 8270D 7/25/17 16:54 JMV P7130369 2,4-Dichlorophenol BRL ug/L 10 2.6 1 8270D 7125/17 16:54 JMV P7G0369 2,4-Dimethylphenol BRL ug/L 10 3A 1 8270D 7/25117 16:54 JMV P7130369 2,4-Dinttrophenol BRL ug/L 10 2.7 1 8270D 7/25117 16:54 JMV P7G0369 2,4-Dinitrotoluene BRL ug/L 10 1.4 1 8270D 7125/17 16:54 JMV P7130369 2,6-Dinitrotoluene BRL uglL 10 1.1 1 8270D 7/25/17 16:54 JMV P7G0369 2-Chloronaphthalene BRL ug/L 10 2.7 1 8270D 7125/17 16:54 JMV P7130369 2-Chlomphenol BRL ug/L 10 1.9 1 8270D 7/25/17 16:54 JMV P7430369 2-Methylnaphthalene BRL ug/L 10 2.4 1 8270D 7/25/17 16:54 JMV P7G0369 2-Methylphenol BRL ug/L 10 1.8 1 8270D 7/25/17 16:54 JMV P7G0369 2-Nitroaniline BRL ug/L 10 1.4 1 8270D 7125/17 16:54 JMV P7G0369 2-Nibophenol BRL ug/L 10 2.4 1 8270D 7/25117 16:54 JMV P7130369 3,3'-Dichlorobenzidine BRL ug/L 10 1.4 1 8270D 7125/17 16:54 JMV P7G0369 3/4-Methylphenol BRL ug/L 10 1.5 1 8270D 7/25117 16:54 JMV P7130369 3-Nitroaniline BRL ug/L 10 1.4 1 8270D 7125117 16:54 JMV P7G0369 4,6-Dinitro-2-methylphenol BRL ug/L 10 1.4 1 8270D 7125/17 16:54 JMV P7G0369 4-Bromophenyl phenyl ether BRL ug/L 10 1.3 1 8270D 7/25/17 16:54 JMV P7G0369 4-Chloro-3-meihylphenol BRL ug/L 10 2.4 1 8270D 7126117 16:54 JMV P7G0369 4-Chlomaniline BRL ug/L 10 2.4 1 8270D 7/25/17 16:54 JMV P7G0369 4-Chlorophenyl phenyl ether BRL ug/L 10 1.3 1 8270D 7126117 16:54 JMV P7G0369 4-Nitroanllme BRLA ug/L 10 0.93 1 a270D 7/26/1716:54 JMV P7G0369 4-Nitrophenol BRL ug/L 10 0.60 1 8270D 7/25/17 16:54 JMV P7G0369 Acenaphthene BRL ug/L 10 1.8 1 8270D 7/25/17 16:54 JMV P7G0369 Acenaphthylene BRL ug/L 10 2.0 1 8270D 7/25/17 16:54 JMV P7130369 Aniline BRL ug/L 10 2A 1 a2701) 7/25/17 16:54 JMV P7G0369 Anthracene BRL ug/L 10 1.4 1 8270D 7125117 16:54 JMV P7G0369 Azobenzene BRL ug/L 10 1.8 1 82700 7/25/17 16:54 JMV P7130369 Benzo(a)anthrecene BRL ug/L 10 1.4 1 8270D 7/25117 16:54 JMV P7G0369 Benzo(a)pynme BRL ug/L 10 1.4 1 a270D 7/25/17 16:54 JMV P7130369 Benzo(b)fluoranthene BRL ug/L 10 1.1 1 8270D 725117 16:54 JMV P7130369 Benzo(g.h,l)perylene BRL ug/L 10 1.4 1 8270D 72511716:64 JMV P7130369 Benzo(k)fluoranthene BRL ug/L 10 1.4 1 8270D 7/25/17 16:54 JMV P7130369 Benzoic Acid BRL ug/L 100 4.7 1 a270D 7125117 16:54 JMV P7G0369 Benzyl alcohol BRL ug/L 10 2A 1 8270D 7125R7 16:54 JMV P7130369 bis(2-Chloroethoxy)methane BRL ug/L 10 2.6 1 8270D 7125117 16:54 JMV P7G0369 Bis(2-Chloroethyl)ether BRL ug/L 10 2.3 1 a270D 725/17 16:54 JMV P7130369 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spdngbrook Road - P.O. Box 240543 - Charlotte, NC 26224-0543 Phone: 704/529-0364 -Toll Free Number: 1-8001529-6364 -Fax: 7041625-0409 Page 12 of 31 r ' P R I SqM I ra° Sarelce Analytical s uwarm es uc Env ronmental Solutions Geoscience Group Project: Truck Part Service Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Sample Matrix: Water Laboratory Report 08/03/2017 Client Sample ID: TW-3 Prism Sample ID: 7070346-03 Prism Work Order: 7070346 Time Collected: 07/20/17 14:41 Time Submitted: 07/20/17 16:40 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date77ime Analyst Batch ID Bis(2-chloroisopropyl)ether BRL ug/L 10 2.0 1 8270D 7/25/17 16:54 JMV P7G0369 Bis(2-Ethylhexyl)phthalate BRL ug/L 10 1.3 1 8270D 7/25/17 16:54 JMV P7G0369 Butyl benzyl phthalate BRL ug/L 10 1.4 1 8270D 7/25/17 16:54 JMV P7G0369 Chrysene BRL ug/L 10 1A 1 8270D 7125/17 16:54 JMV P7130369 Dibenzo(a,h)angnacene BRL ug/L 10 1.2 1 8270D 7/25117 16:54 JMV P7G0369 Dibenzoturen BRL ug/L 10 1.8 1 8270D 7125/17 16:54 JMV P7130369 Diethyl phthalate BRL ug/L 10 3.3 1 52701) 7/25/17 16:54 JMV P7430369 Dimethyl phthalate BRL ug/L 10 1.4 1 8270D 7125/17 16:54 JMV P7130369 Di-n-butyl phthalate BRL ug/L 10 1.7 1 8270D 7/25/17 16:54 JMV P7G0369 Di-n-octyl phthalate BRL ug/L 10 1.3 1 8270D 7/25117 16:54 JMV P7430369 Fluoranthene BRL ug/L 10 1.7 1 8270D 7125/17 16:54 JMV P7G0369 Humana BRL ug/L 10 1.7 1 8270D 7125117 16:54 JMV P7130369 Hexachlorobenzene BRL ug/L 10 1.3 1 8270D 7/25117 16:54 JMV P7G0369 Hexachlorobutadiene BRL ug/L 10 2.1 1 8270D 7/25/17 16:54 JMV P7130369 Hexachlorocydopentadiene BRL ug/L 10 1.7 1 8270D 7125/17 16:54 JMV P7G0369 Hexachlorcethane BRL ug/L 10 1.7 1 8270D 7/25/17 16:54 JMV P7130369 Indeno(1,2,3-cd)pyrene BRL ug/L 10 3.9 1 8270D 7/25/17 16:54 JMV P7G0369 Isophorone BRL ug/L 10 2.5 1 8270D 7125117 16:54 JMV P7130369 Naphthalene BRL ug/L 10 2.6 1 8270D 7/25/17 16:54 JMV P7430369 Nitrobenzene BRL ug/L 10 2.6 1 8270D 7125117 16:64 JMV P7130369 N-Nitroso-di-n-propylamine BRL ug/L 10 2.2 1 8270D 7/25/17 16:54 JMV P7130369 N-Nitmwdiphenylamine BRL ug/L 10 1.3 1 8270D 7/25117 16:54 JMV P7G0369 Pentachlorophenol BRL ug/L 10 1.2 1 8270D 7125117 16:54 JMV P7G0369 Phenanthrene BRL ug/L 10 1.5 1 8270D 7/26117 16:54 JMV P7G0369 Phenol BRL ug/L 10 0.98 1 8270D 7/25/17 16:54 JMV P7G0369 Pyrene BRL ug/L 10 1.4 1 8270D 7/26/17 16:54 JMV P7G0369 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 80 % 43-140 2-Fluorobiphenyl 72 % 44-119 2-Fluorophenol 44 % 19-119 Nitrobenzene-05 59 % 44-120 Phenol-d5 30 % 11-52 Terphenyl-014 93 % 50-134 Volatile Organic Compounds by GC/MS 1,1,1,2-Tetrachloroethane BRL ug/L 0.50 0.11 1 8260B 7/31/17 17:53 KDM P7GD491 1,1,1-Tdchloroethane BRL ug/L 0.50 0.061 1 8260B 7/31/1717:53 KDM P7430491 1, 1,2,2-Tatmchlomethane BRL ug/L 0.50 0.036 1 8260B 7131/17 17:53 KDM P7130491 1,1,2-Trichloroethane BRL ug/L 0.50 0.066 1 8260B 7131/17 17:53 KDM P7G0491 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 82608 7131/17 17:53 KDM P7G0491 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 8260B 7/31117 17:53 KDM P7G0491 1,1-Dichloropropylene BRL ug/L 0.50 0.061 1 8260B 7131/17 17:53 KDM P7130491 1,2,3-Tdchlorobenzene BRL ug/L 2.0 0.40 1 8260B 7131/17 17:53 KDM P7130491 1,2,3-Trchloropropane BRL ug/L 1.0 0.14 1 8260B 7131/17 17:53 KDM P7130491 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 704/529-6364 -Toll Free Number: 1-800/629-6364 -Fax: 7041525-0409 page 13 of 31 -x.: Full -Service Analytical 6 `P R I S M I Envbcnmental solutions Laboratory Report 08/03/2017 Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, INC 28217 Project: Truck Part Service Sample Matrix: Water Client Sample ID: TW-3 Prism Sample ID: 7070346-03 Prism Work Order: 7070346 Time Collected: 07/20/17 14:41 Time Submitted: 07/20/17 16:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/I-ime ID 1,2,47richlorobenzene BRL ug/L 1.0 0.13 1 8260B 7131/17 17:53 KOM P7GO491 1,2,4-Trimethylbenzene BRL ug/L 0.50 0.054 1 8260B 7131117 17:53 KOM P7G0491 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 8260B 7/31/17 17:53 KOM P7GO491 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 82608 7131/17 17:53 KOM P7G0491 1,2-Dichlorobenzene BRL ug/L 0.50 0.076 1 8260B 7/31/17 17:53 KOM P7GO491 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 82608 7131117 17:53 KOM P7GD491 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 8260B 7/31/17 17:53 KOM P7GO491 1,3,5-Trimethylbenzene BRL ug/L 0.50 0.076 1 8260B 7131/17 17:53 KOM P7GO491 1,3-Dichlorobenzene BRL ug/L 0.50 0.054 1 8260B 7131/17 17:53 KOM P7G0491 1,3-Dichloropropene BRL ug/L 0.50 0.043 1 82608 7/31117 17:53 KOM P7GO491 1,4-Dichlorobenzene BRL ug/L 0.50 0.050 1 8260B 7/31/17 17:53 KOM P7GO491 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 8260B 7/31/17 17:53 KOM P7G0491 2-Chlorotoluene BRL ug/L 0.50 0.066 1 8260B 7131117 17:53 KOM P7GO491 4-Chlomtoluene BRL ug/L 0.50 0.050 1 8260B 7/31/17 17:53 KOM P7GD491 4-Isopropyltoluene BRL ug/L 0.50 0.089 1 8260B 7131117 17:53 KOM P7GD491 Acetone BRL ug/L 5.0 0.31 1 8260B 7131/17 17:53 KOM P7GO491 Acrolein BRL ug/L 20 0.20 1 8260B 7131/17 17:53 KOM P7GD491 Acrylonitrile BRL ug/L 20 0.20 1 8260B 7/31/17 17:53 KOM P7G0491 Benzene BRL ug/L 0.60 0.048 1 8260B 7/31/17 17:53 KOM P7130491 Bromobenzene BRL ug/L 0.50 0.057 1 8260B 7/31/17 17:53 KOM P7GO491 Bromochlommethane BRL ug/L 0.50 0.14 1 8260B 7/31/17 17:53 KOM P7G0491 Bromodichloromethane BRL ug/L 0.50 0.062 1 8260B 7/31117 17:63 KOM P7GO491 Bromofonn BRL ug/L 1.0 0.040 1 8260B 7/31/17 17:53 KOM P7G0491 Bromomethene BRL ug/L 1.0 0.18 1 82608 7131/17 17:53 KOM P7GO491 Carbon disuKde BRL ug/L 5.0 0.075 1 8260B 7/31/17 17:53 KOM P7GD491 . Carbon Tetrachloride BRL ug/L 0.50 0.11 1 8260B 7131117 17:63 KOM P7GO491 Chlorobenzene BRL ug/L 0.50 0.062 1 8260B 7/31/17 17:53 KOM P7GD491 Chloroethane BRL ug/L 0.50 0.22 1 8260B 7/31117 17:63 KOM P7GO491 Chloroform 2.1 ug/L 0.50 0.076 1 8260B 7131/17 17:53 KOM P700491 Chloromethane BRL ug/L 0.50 0.079 1 8260B 7/31/17 17:53 KOM P7GD491 cis-1,2-Dichlorcethylene BRL ug/L 0.50 0.056 1 82608 7131/17 17:53 KOM P7GO491 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 8260B 7131/17 17:53 KOM P7GO491 Dibromochlommethane BRL ug/L 0.50 0.081 1 8260B 7/31/17 17:53 KOM P7GD491 Dibromomethane BRL ug/L 0.50 0.065 1 8260B 7131/17 17:53 KOM P7G0491 Dlchiorodilluoromethane BRL ug/L 1.0 0.11 1 8260B 7131/17 17:53 KOM P7GO491 Ethylbenzene BRL ug/L 0.50 0,061 1 8260B 7/31117 17:53 KOM P7GO491 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 8260B 7131/17 17:53 KOM P7GO491 Isopropyl Ether BRL ug/L 9 0.50 0.050 1 8260B 7/31/17 17:53 KOM P7(30491 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 8260B 7/31117 17:53 KOM P7GO491 m,p-Xylenes BRL ug/L 1.0 0.12 1 8260B 7/31/17 17:53 KOM P7G0491 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 8260B 7131117 17:53 KOM P7G0491 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 8260B 7/31117 17:63 KOM P7GO491 Methyl Isobutyl Ketone BRL ug/L 5.0 0.078 1 8260B 7131117 17:53 KOM P7G0491 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Bpringbrook Road - P.O. Box 240643 - Charlotte, NC 26224-0543 Phone: 7041529-6364-Toll Free Number: 1-8001529-6364- Fax: 704/525-0409 Page 14 of 31 �P I S M I n °_ae loa Ansl noel a s _uewnroe'ssu� Environmental Solutions Laboratory Report 08/03/2017 Geoscience Group Project: Truck Part Service Client Sample ID: TW-3 Attn: Tom Hassett Prism Sample ID: 7070346-03 500-K Clanton Rd. Prism Work Order: 7070346 Charlotte, NC 28217 Sample Matrix: Water Time Collected: 07/20/17 14:41 Time Submitted: 07/20/17 16:40 Parameter Result Units Report MDL Dilution Method Analysis Analyst -Batch Limit Factor Date/Time ID Methylene Chloride BRL ug/L 1.0 0.083 1 8260B 7/31/17 17:53 KDM P7G0491 Methyl4en-Butyl Ether BRL ug/L 0.50 0.042 1 8260B 7/31117 17:53 KDM P7130491 Naphthalene BRL ug/L 1.0 0.19 1 8260B 7/31/17 17:53 KDM P7130491 n-Butylbenzene BRL ug/L 1.0 0.076 1 82608 7/31/17 17:53 KDM P7130491 n-Propylbenzene BRL ug/L 0.50 0.087 1 8260B 7131117 17:53 KDM P7G0491 o-Xylene BRL ug/L 0.50 0.044 1 82608 7131/17 17:53 KDM P7G0491 sec-Butylbenzene BRL ug/L 0.50 0.076 1 8260B 7/31117 17:53 KDM P7130491 Styrene BRL ug/L 0.50 0.047 1 8260B 7/31117 17:53 KDM P71210491 tert-Butylbenzene BRL ug/L 0.50 0.088 1 8260B 7131/17 17:53 KDM P7G0491 Tetrachloroethylene BRL ug/L 0.50 0.098 1 8260B 7/31117 17:53 KDM P7130491 Toluene BRL ug/L 0.50 0.044 1 8260B 7131/17 17:53 KDM P7G0491 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 8260B 7/31117 17:53 KDM P7G0491 trans-1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 8260B 7131/17 17:53 KDM P7G0491 Trichloroethylene 0.51 ug/L 0.50 0.078 1 8260B 7131/17 17:53 KDM P7G0491 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 8260B 7131117 17:53 KDM 1`7130491 Vinyl acetate BRL ug/L 2.0 0.060 1 8260B 7/31117 17:53 KDM P7130491 Vinyl chloride BRL ug/L 0.50 0.097 1 8260B 7/31117 17:53 KDM P7G0491 Surrogate Recovery Control Limits 4-BromoBuorobenzene 101 % 80-124 Dibromofluoromethane 119 % 75-129 Toluene-d8 96 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7WS29.6364 - Toll Free Number: 1-800/529.6364 - Fax: 7041526-0409 Page 15 of 31 �PR I S M Environmental Solutions usoa,ron,cc,xe Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GC/MS - Quality Control Analyte Reporting Result Limit Units Level II QC Report 813/17 Prism Work Order: 7070346 Time Submitted: 7/20/2017 4:40:OOPM Spike Source %REC RPD Level Result %REC Limits RPn l imit lu Batch P7G0491 - 5030B Blank (127G8491-BLKt) Prepared &Analyzed: 07/31/17 1,1,1,2-Tetrachloroethane BRL 0.50 ug/L 1,1,1-Trichloroethane BRL 0.50 ug/L 1,1,2,2-Tetrechloroethane BRL 0.50 ug/L 1,1,2-Tdchlomethane BRL 0.50 ug/L 1,1-Dichlomethane BRL 0.50 ug/L 1,1-Dichloroethylene BRL 0.50 ug/L 1,1-Dichloropropylene BRL 0.50 ug/L 1,2,3-Trichlorobenzene BRL 2.0 ug/L 1,2,3-Trichlompropane BRL 1.0 ug/L 1,24-Trichlorobenzene BRL 1.0 ug/L 1,2,4-Trimethylbenzene BRL 0.50 ug/L 12-Dibmmo-3-chloropropane BRL 2.0 ug/L 1,2-Dibromcethane BRL 0.50 ug/L 1,2-Dichlombenzene BRL 0.50 ug/L 1,2-Dichlomethane BRL 0.50 ug/L 1,2-Dichloropropane BRL 0.50 ug/L 1,3,5-Thmethylbenzene BRL 0.50 ug/L 1,3-Dichlorobenzene BRL 0.50 ug/L 1,3-Dichloropropane BRL 0.50 ug/L 1,4-Dichlorobenzene BRL 0.50 ug/L 2,2-Dichloropropane BRL 2.0 ug/L 2-Chlorotoluene BRL 0.50 ug/L 4-Chlomtoluene BRL 0.50 ug/L 4-Isopropyholuene BRL 0.50 ug/L Acetone BRL 5.0 ug/L Acrolein BRL 20 ug/L Acrylonibile BRL 20 ug/L Benzene BRL 0.50 ug/L Bremobenzene BRL 0.50 ug/L Bromochloromethane BRL 0.50 ug/L Bromodichloromethane BRL 0.50 ug/L Bromoform BRL 1.0 ug/L Bromomethane BRL 1.0 ug/L Carbon disuKde BRL &0 ug/L Carbon Tetrachloride BRL 0.50 ug/L Chlorobenzene BRL 0.50 ug/L Chloroethane BRL 0.50 ug/L Chloroform BRL 0.50 ug/L Chloromethane BRL 0.50 ug/L cis-1,2-Dichloroethylene BRL 0.50 ug/L cis-1,3-Dichloropropylene BRL 0.50 ug/L Dibromochloromethane BRL 0.50 ug/L Dibromomethane BRL 0.50 ug/L Dichlorodifluoromethane BRL 1.0 ug/L Ethylbenzene BRL 0,50 ug/L Hexachlorobutediene BRL 2.0 uglL This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 26224-0543 Phone: 7041529-6364 - Toll Free Number: 1-800/529.6364 - Fax: 7041525.0409 Page 16 of 31 e[LAII A Full -Service Analytical & R M . Environmental SWutions Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GC/MS - Quality Control Reporting Result Limit Units Batch P71310491 •5030B Level II QC Report 8/3/17 Prism Work Order: 7070346 Time Submitted: 7/20/2017 4:40:00PM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P708491-BLK1) Prepared & Analyzed: 07/31/17 Isopropyl Ether BRL 0.50 ug/L Isopropylbenzene (Cumene) BRL 0.50 ug/L m,p-Xylenes BRL 1.0 ug/L Methyl Butyl Ketone (2-Hemnone) BRL 5.0 ug/L Methyl Ethyl Ketone (2-Butanone) BRL 5.0 ug/L Methyl Isobutyl Ketone BRL 5.0 ug/L Methylene Chloride BRL 1.0 ug/L Methyl-tert-Butyl Ether BRL 0.60 ug/L Naphthalene BRL 1.0 ug/L n-Butylbenzene BRL 1.0 ug/L n-Propylbenzene BRL 0.50 ug/L o-Xylene BRL 0.50 ug/L sec-Butylbenzene BRL 0.50 ug/L Styrene BRL 0.50 ug/L tort-Butylbemene BRL 0.50 ug/L Tetrachloroethylene BRL 0.50 ug/L Toluene BRL 0.50 ug/L trans-1.2-Dichlomethylene BRL 0.50 ug/L trans-1,3-Dichloropropylene BRL 0.50 ug/L Thchloruethylene BRL 0.50 ug/L Tdchloro0uoromethane BRL 0.50 ug/L Vinyl acetate BRL 2.0 ug/L Vinyl chloride BRL 0.50 ug/L Tentatively Identified Compounds Not Detected ug/L Surrogate: 4-Bromofluorobenzene 51.5 IWL 50.00 103 80-124 Surrogate: Dibromofluommethane 58.0 u91L 50.00 116 75-129 Surrogate: Toluene-d8 49.5 uyL 50.00 99 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 -Toll Free Number: 1-800/529.6364 - Fax: 7041325-0409 Page 17 of 31 PR I S M Full-Servlce Analytical 8 eoanro Environmental Solutions �' w ales r,w Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GCIMS - Quality Control Reporting Result Limit Units Batch P7G0491 - 5030B Level II QC Report 8/3/17 Prism Work Order: 7070346 Time Submitted: 7/20/2017 4:40:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P7G04914351) Prepared 8 Analyzed: 07/31/17 1,1,1,2-Tetrechlorcethane 19.8 0.50 ug/L 20.00 99 79-134 1,1,1-Trichlomathane 23.8 0.50 ug/L 20.00 119 75-136 1,1,2,2-Tetrechiamethane 19.0 0.50 ug/L 20.00 95 62-127 1,1,2-Tdchloroethane 22.1 0.50 ug/L 20.00 111 70-140 1,1-Dichlomethane 21.0 0.50 ug/L 20.00 105 78-130 1,1-Dichloroethylene 22.4 0.50 ug/L 20.00 112 70-154 1,1-Dichloropropylene 21.8 0.50 ug/L 20.00 109 71-136 1,2,3-Tdchlorobenzene 20.9 2.0 ug/L 20.00 104 58-144 1,2,3-Trichloropropane 19.9 1.0 ug/L 20.00 99 71-127 1,24-Tdchlorobenzene 21.7 1.0 ug/L 20.00 109 66-139 1,2,4-Tdmethylbenzene 21.4 0.50 ug/L 20.00 107 75-133 1,2-Dibromo-3-chloropropane 21.6 2.0 ug/L 20.00 107 63-134 1,2-Dibromcethane 23.1 0.50 ug/L 20.00 115 77-135 1,2-Dichlorobenzene 20.7 0.50 ug/L 20.00 103 78-128 1,2-Dichloroethane 23.4 0.50 ug/L 20.00 117 68-131 1,2-Dichloropropane 19.8 0.50 ug/L 20.00 99 77-130 1,3,5-Tdmethylbenzene 21.0 0.50 ug/L 20.00 105 75-131 1,3-Dichlorobenzene 20.4 0.50 ug/L 20.00 102 77-125 1,3-Dichloropropane 20.0 0.50 ug/L 20.00 100 76-132 1,4-Dichlorobenzene 20.0 0.50 ug/L 20.00 100 75-126 2,2-Dichloropropane 23.3 2.0 ug/L 20.00 117 29-149 2-Chlorotoluene 20.7 0.50 ug/L 20.00 104 74-126 4-Chlorotoluene 21.0 0.50 ug/L 20.00 106 78-129 4-Isopropyttoluene 22.1 0.50 ug/L 20.00 110 69-132 Acetone 47.2 5.0 ug/L 40.00 118 40-166 Acroleln 32.7 20 ug/L 40.00 82 70-130 AcryloniMle 44.6 20 ug/L 40.00 111 81-127 Benzene 21.2 0.50 ug/L 20.00 106 77-128 Bromobenzene 18.9 0.50 ug/L 20.00 94 78-129 Bromochloromethane 21.6 0.50 ug/L 20.00 108 78-135 Bromodichloromethane 22.3 0.50 ug/L 20.00 111 76-138 Bromoform 20.0 1.0 ug/L 20.00 100 71-136 Bromomethane 13.1 1.0 ug/L 20.00 65 41-168 Carbon disulfide 20.0 5.0 ug/L 20.00 100 59-135 Carbon Tetrachloride 23.8 0.50 ug/L 20.00 119 72-142 Chlorobenzene 20.4 0.50 ug/L 20.00 102 78-119 Chlomethane 17.4 0.50 ug/L 20.00 87 57-142 Chloroform 21.5 0.50 ug/L 20.00 107 77-130 Chloromethane 15.3 0.50 ug/L 20.00 77 47-145 cis-1,2-Dichloroethylene 21.9 0.50 ug/L 20.00 109 76-141 cis-1,3-Dichloropropylene 22.3 0.50 ug/L 20.00 112 65-140 Dibromochloromethene 21.3 0.50 ug/L 20.00 107 75-134 Dibromomethane 21.7 0.50 ug/L 20.00 109 76-138 Dichlorodlguoromethane 18.7 1.0 ug/L 20.00 93 28-163 Ethylbenzene 20.6 0.50 ug/L 20.00 103 80-127 Hexachlorobutadiene 23.4 2.0 ug/L 20.00 117 61-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041629-6364 - Toll Free Number: 1-6001529.6364 - Fax: 704/6254409 Paae 18 Of 31 L011, rR I SxM I rmi ron ee al So ioei a ueoxaio es xa Env ronmentel Solutions Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GCIMS - Quality Control Reporting Result Limit Units Level II QC Report 8/3/17 Prism Work Order: 7070346 Time Submitted: 7/20/2017 4:40:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch M1114911 -5030B LCS (P7G049143St) Prepared & Analyzed: 07/31/17 Isopropyl Ether 21.3 0.50 ug/L 20.00 107 60-154 Isopropylbeozene (Cumens) 20.2 0.50 ug/L 20.00 101 70-130 m,p-Xylenes 42.2 1.0 ug/L 40.00 106 77-133 Methyl Butyl Ketone (2-Hexanone) 22.9 5.0 ug/L 20.00 115 64-137 Methyl Ethyl Ketone (2-Butanone) 24.1 5.0 ug/L 20.00 121 71-134 Methyl IsobuM Ketone 24.8 5.0 ug/L 20.00 124 69-134 Methylene Chlonde 20.3 1.0 ug/L 20.00 102 73-131 Methyl -tart -Butyl Ether 22.7 0.50 ug/L 20.00 113 68-135 Naphthalene 20.7 1.0 ug/L 20.00 104 64-136 n-Butylbenzene 21.1 1.0 ug/L 20.00 106 68-134 n-Propylbenzene 20.0 0.50 ug/L 20.00 100 72-132 o-Xylene 20.8 0.50 ug/L 20.00 104 78-128 sec-Butylbenzene 20.6 0.50 ug/L 20.00 103 71-131 Styrene 21.6 0.50 ug/L 20o0 108 78-129 tert-Butylbenzene 19.8 0.50 ug/L 20.00 99 70-132 Tetrachloroethylene 20.5 0.50 ug/L 20.00 102 80-129 Toluene 21.0 0.50 ug/L 20.00 105 76-131 tans-1,2-Dichlomethylene 22.4 . 0.50 ug/L 20.00 112 76-135 trans-1,3-Dichloropropylene 22.8 0.50 ug/L 20.00 114 67-140 Tdchloroethylene 21.5 0.50 ug/L 20.00 108 77-133 Trichlorolluoromethane 23.5 0.50 ug/L 20.00 118 62-148 Vinyl acetate 24.1 2.0 ug/L 20.00 120 34-167 Vinyl chloride 21.0 0.50 ug/L 20.00 105 57-141 Surrogate: 4-Bromotluombenzene 51.4 ug/L 50.00 103 80-124 Surrogate: Dibromo0uoromethane 51.6 u92 50.00 103 75.129 Surrogate: ToluenedS 47.8 U91L 50.00 96 77-123 LCS Dup (P760491-BSD1) Prepared & Analyzed: 07/31/17 1,1,1,2-Tetrechloroethane 20.8 0.50 ug/L 20.00 104 79-134 5 20 1,1,1-Trichloroethane 23.8 0.50 ug/L 20.00 119 75-136 0.08 20 1,1,2,2-Tetrachloroethane 19.3 0.50 ug/L 20.00 96 62-127 1 20 1,1,2-Trichloroethane 21.1 0.50 ug/L 20.00 106 70A40 5 20 1,1-Dichlomethane 20.6 0.50 ug/L 20.00 103 78.130 2 20 1,1-Dichloroethylene 22.6 0.50 ug/L 20.00 113 70-164 1 20 1,1-Dichloropropylene 21.2 0.50 ug/L 20.00 106 71-136 3 20 1,2,3-Trichlorobenzene 21.3 2.0 ug/L 20.00 107 58-144 2 20 1,2,3-Trichloropropane 20.6 1.0 ug/L 20.00 103 71-127 4 20 1,2A-Tdchlorobenzene 22.0 1.0 ug/L 20.00 110 66-139 1 20 1,2,4-Tdmethylbenzene 21.4 0.50 ug/L 20.00 107 75-133 0.09 20 1,2-Dibromo-3-chloropropane 22.2 2.0 ug/L 20.00 111 63-134 3 20 1,2-Dibromoethane 22.9 0.50 ug/L 20.00 114 77-135 1 20 1,2-Dichlorobenzene 20.8 0.50 ug/L 20.00 104 7a-128 0.7 20 1,2-Dichlomethane 23.4 0.50 ug/L 20.00 117 68-131 0.09 20 1,2-Dichloropropane 19.9 0.50 ug/L 20.00 100 77-130 0.8 20 1,3,5-Trimethylbenzene 21.6 0.50 ug/L 20.00 108 75-131 2 20 1,3-Dichlorobenzene 21.0 0.50 ug/L 20.00 105 77-125 3 20 1,3-Dichlompropane 20.7 0.50 ug/L 20.00 103 76-132 3 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Read - P.O. Box 240543 - Charlotte, NC 28224.0643 Phone: 704/529-6364 - Toll Free Number: 14001529-6364 - Fax: 7041525.0409 Page 19 of 31 ,PRISNl♦\ n6tra Analytical s M IFEulvonniontal Solutions Uagi/.1pFEA iNC Geoscience Group Attn:Tom Hassell 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GC/MS - Quality Control Analyte Reporting Result Limit Units Level 11 QC Report 8/3/17 Prism Work Order: 7070346 Time Submitted: 7/20/2017 4:40:0013M Spike Source XREC RPD Level Result %REC Limits RPD Limit Notes Batch P7GD491 - 5030B LCS Dup (P7G0491.BSD1) Prepared 8 Analyzed: 07/31/17 1,4-Dichlorobenzene 20A 0.50 ug/L 20.00 102 75-126 2 20 2,2-Dichloropropane 23.6 2.0 ug/L 20.00 118 29-149 1 20 2-Chlomtoluene 20.8 0.50 ug/L 20.00 104 74-126 0.2 20 4-Chlorotoluene 21.1 0.50 ug/L 20.00 105 78-129 0.5 20 4-Isopropyltoluene 22.7 0.50 ug/L 20.00 113 69-132 3 20 Acetone 46A 6.0 ug/L 40.00 115 40-166 2 20 Acrolein 35.6 20 ug/L 40.00 89 70-130 9 20 Acrylonitrile 42.6 20 ug/L 40.00 106 81-127 5 20 Benzene 21.4 0.50 ug/L 20.00 107 77-128 1 20 Bromobenzene 19.3 0.50 ug/L 20.00 97 78-129 2 20 Bromochloromethane 21.8 0.50 ug/L 20.00 109 78-135 1 20 Bromodichloromethane 21.8 0.50 ug/L 20.00 109 76-138 2 20 Bromoform 20.1 1.0 ug/L 20.00 100 71-135 0.3 20 Bromomethane 14.1 1.0 ug/L 20.00 70 41-168 7 20 Carbon disuKde 20.1 5.0 ug/L 20.00 100 59-135 0.3 20 Carbon Tetrachloride 24.1 0.50 ug/L 20.00 120 72-142 1 20 Chlorobenzene 20.9 0.50 ug/L 20.00 105 78-119 3 20 Chloroethane 17.8 0.50 ug/L 20.00 89 57-142 2 20 Chloroform 21.7 0.50 ug/L 20.00 109 77-130 1 20 Chloromethane 15.5 0.50 ug/L 20.00 77 47-145 1 20 cis-1,2-Dichloroethylene 22.3 0.50 ug/L 20.00 112 76-141 2 20 cis-1,3-Dichloropropylene 22.6 0.50 ug/L 20.00 113 65-140 1 20 Dibromochloromethane 21.7 0.60 ug/L 20.00 109 75-134 2 20 Dibromomethane 21.4 0.50 ug/L 20.00 107 76-138 2 20 Dichlorodifluoromethane 18.4 1.0 ug/L 20.00 92 28-163 1 20 Ethylbenzene 21.0 0.50 ug/L 20.00 105 80-127 2 20 Hemchlombutediene 23.3 2.0 ug/L 20.00 116 61-134 0.4 20 Isopropyl Ether 21.4 0.60 ug/L 20.00 107 60-154 0.4 20 Isopropylbenzene(Cumene) 21.0 0.50 ug/L 20.00 105 70-130 4 20 nip-Xylenes 43.2 1.0 ug/L 40.00 108 77-133 2 20 Methyl Butyl Ketone (2-Hexanone) 20.5 5.0 ug/L 20.00 103 64-137 11 20 Methyl Ethyl Ketone(2-Butenone) 23.8 5.0 ug/L 20.00 119 71-134 1 20 Methyl lsobutyl Ketone 24.0 5.0 ug/L 20.00 120 69-134 4 20 Methylene Chloride 20.0 1.0 ug/L 20.00 100 73-131 1 20 Methyl-tert-Butyl Ether 22.7 0.50 ug/L 20.00 114 68-135 0.3 20 Naphthalene 20.8 1.0 ug/L 20.00 104 64-136 0.1 20 n-Bulylbenzene 21.4 1.0 ug/L 20.00 107 68-134 1 20 n-Propylbenzene 20.3 0.50 ug/L 20.00 102 72-132 1 20 o-Xylene 21.2 0.50 ug/L 20.00 106 78-128 2 20 sec-Butylbenzene 21.2 0.50 ug/L 20.00 106 71-131 3 20 Styrene 22.2 0.50 ugA 20.00 111 78-129 3 20 tart-Butylbenzene 20.5 0.50 ui 20.00 103 70-132 3 20 Tetrachlomethylene 20.4 0.50 ug/L 20.00 102 80-129 0.2 20 Toluene 21.2 0.50 ug/L 20.00 106 76-131 1 20 trans-1,2-Dichloroethylene 22.8 0.60 ug/L 20.00 114 76-135 2 20 trans-1,3-Dichloropropylene 22.1 0.50 ug/L 20.00 111 67-140 3 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7WS29-6364- Toll Free Number. 1.8001529-6364-Far: 704/525-WO Page 20 of 31 f rb. P R I S M I Full Sary ca Analytical 8 Environmental SoluHnns Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GC/MS - Quality Control Analyte Reporting Result Limit Units Level II QC Report 8/3117 Prism Work Order: 7070346 Time Submitted: 7/20/2017 4:40:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P7G0491 - 5030B LCS Cup (P7G0491-BSD1) Prepared & Analyzed: 07/31/17 Trichloroethylene 21.0 0.50 ug/L 20.00 105 77-133 2 20 Tdchlorofluoromethane 21.9 0.50 ug/L 20.00 109 62-148 7 20 Vinyl acetate 23.7 2.0 ug/L 20.00 118 34-167 2 20 Vinyl chloride 20.6 0.50 ug/L 20.00 103 57-141 2 20 Surrogate: 4-Bromofluorobenzene 50.5 ug/L 50.00 101 80-124 Surrogate: Dibromofluoromethane 51.4 ug/L 50.00 103 75-129 Surrogate: Toluene -de 49.3 U91L 50.00 99 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number: 1.8001529.6364 - Fax: 7041525-0409 Page 21 of 31 5:. PRISM I Fnviron ice analytical 8 Environmental Solunons —�:. uewoonisa �w Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GCIMS - Quality Control Reporting Result Limit Units Batch MOM -351CC MS Level II QC Report 8/3/17 Prism Work Order: 7070346 Time Submitted: 7/20/2017 4:40:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P7GO369-BLK7) Prepared $ Analyzed: 07/25/17 1,2,4-Tdchlorobemene BRL 10 ugA 1,243Ichlorobenzene BRL 10 ug/L 1,3-Dichlorobenzene BRL 10 ug/L 1,4-Dichlorobenzene BRL 10 ug/L 1-Methylnaphthalene BRL 10 ug/L 2,4,5-Tdchlorephenol BRL 10 ug/L 2,4,6-Tdchlorophenol BRL 10 ug/L 2,4-Dichlorophenol BRL 10 ug/L 2,4-Dimethylphenol BRL 10 ug/L 2,4-Dinitmphenol BRL 10 ug/L 2,4-Dinitrotoluene BRL 10 ug/L 2,6-Dinibotoluens BRL 10 ug/L 2-Chlomnaphthalene BRL 10 ug/L 2-Chlorophenol BRL 10 ug/L 2-Methylnaphthalene BRL 10 ug/L 2-Methylphenol BRL 10 ug/L 2-Niboaniline BRL 10 ug/L 2-Nitrophenol BRL 10 ug/L 3,3'-Dichlombenzidine BRL 10 ug/L 3/4-Methylphenol BRL 10 ugA 3-Niboaniline - BRL 10 ug/L 4,6-Dinibo-2-methAphenol BRL 10 ug/L 4-Bromophenyl phenyl ether BRL 10 ug/L 4-Chloro-3-methylphenol BRL 10 ug/L 4-Chlomaniline BRL 10 ug/L 4-Chlomphenyl phenyl ether BRL 10 ug/L 4-Nilroaniline BRL 10 ug/L 4-Nitrophenol BRL 10 ug/L Acenaphthene BRL 10 ug/L Acenaphthylene BRL 10 ugA Aniline BRL 10 ug/L Anthracene BRL 10 ugA Azobenzene BRL 10 ug/L Benzo(a)anthracene BRL 10 ug/L Bemo(a)pyrene BRL 10 ug/L Benzo(b)fluoranthene BRL 10 ug/L Benzo(g,hJ)perylene BRL 10 ug/L Benzo(k)fluoranthene BRL 10 ug/L Benzoic Acid BRL 100 ug/L Benzyl alcohol BRL 10 ug/L bis(2-Chlormthoxy)methane BRL 10 ug/L Bis(2-Chloroethyl)ether BRL 10 ug/L Sis(2-chloroisopropyl)ether BRL 10 ug/L Bis(2-Ethylhexyl)ph1halate BRL 10 ug/L Butyl benzyl phthalate BRL 10 ugA Chrysene BRL 10 ug/L This report should not be reproduced, except in its entirety, without the written cement of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Chadotts, NC 29224-0543 Phone: 7041529-6364 - Toll Free Number..l-9001529.6364- Fax: 704/525-0409 Page 22 ci 31 PG Full -Service Analytical & R I SqM I Envlranm J sei ,laae Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Result Limit Units Batch P760369-3510C MS Level II QC Report 8/3/17 Prism Work Order: 7070346 Time Submitted: 7/20/2017 4:40:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P7GO369-BLK1) Prepared & Analyzed: 07/25/17 Dibenzo(a,h)anthracene BRL 10 ug/L Dibenzofuran BRL 10 ug/L Diethyl phthalate BRL 10 ug/L Dimethyl phthalate BRL 10 ug/L Di-n-butyl phthalate BRL 10 ug/L Di-noctyl phthalate BRL 10 ug/L Fluoranthene BRL 10 ug/L Fluorene BRL 10 ug/L Hexachlombenzene BRL 10 ug/L Hexachlorobutadiene BRL 10 ug/L Hexachlorocydopentadiene BRL 10 ug/L Hexachlomethane BRL 10 ug/L Indeno(1,2,3-cd)pyrene BRL 10 ug/L Isophorone BRL 10 ug/L Naphthalene BRL 10 ug/L Nitrobenzene BRL 10 ug/L N-Nhroso-di-n-propylamine BRL 10 ug/L N-Nitrosodiphenylamine BRL 10 ug/L Pentachlorophenol BRL 10 ug/L Phenanthrene BRL 10 ug/L Phenol BRL 10 ug/L Pyrene BRL 10 ug/L Surrogate: Z4,6-Tribmmopheno/ 81.9 UO 100.0 82 43-140 Surrogate: 2-Fluorobipheno 32.6 ug/L 50.00 65 44-119 Surrogate: 2-F/uoropheno/ 46.2 u91L 100.0 46 19-119 Surrogate: Nitrobenzened5 29.1 ug/L 50.00 58 44420 Surrogate: Phenol-d5 30.5 u91L 100.0 31 11-52 Surrogate: Terphenyl-dM 47.6 u91L 50.00 95 50-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratcries, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0S43 Phone: 7041529-6364 - Toll Free Number: 1-8001529.6364-Fax: 7041525-0409 Page 23 of 31 'AFu11-Se"ice Analytical B rR I SpM I Environmental Solution. M Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semlvolatile Organic Compounds by GCIMS - Quality Control Reporting Result Limit Units Batch P7G0369 - 3510C MS Level II QC Report 8/3117 Prism Work Order: 7070346 Time Submitted: 7/20/2017 4:40:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P7G0369-BS1) Prepared & Analyzed: 07/25/17 1,2,4-Tdchlarobenzene 25.3 10 ug/L 50.00 51 29-126 1,2-Dichlorobenzene 24.2 10 ug/L 50.00 48 32-111 1,3-Dichlambemene 23.1 10 ug/L 50.00 46 28-110 14-Dichlorobenzene 23.1 10 ug/L 50.00 46 29-112 1-Methylnaphthalene 30.9 10 ug/L 50.00 62 41-119 2,4,5-Tdchlorophenol 37.6 10 ug/L 50.00 75 53-123 2,4,6-Tdchlorophenol 36.3 10 ug/L 50.00 73 W125 2,4-Dichlorophenol 32.0 10 ug/L 50.00 64 47-121 2,4-Dimethylphenol 41.3 10 ug/L 50.00 83 31-124 2,4-Dinibophenol 26.6 10 ug/L 50.00 53 23-143 2,4-Dinibotoluene 36.3 10 ug/L 50.00 73 57-128 2,6-Dinibotoluene 37.6 10 ug/L 50.00 75 57-124 2-Chloronaphthalene 33.1 10 ug/L 50.00 66 40-116 2-Chlomphenol 31.7 10 ug/L 50.00 63 38-117 2-Methylnaphthalene 29.9 10 ug/L 50.00 60 40-121 2-Methylphenol 32.2 10 ug/L 50.00 64 30-117 2-Niboaniline 32.8 10 ug/L 50.00 66 55-127 2-Nitrophenol 31.4 10 ug/L 50.00 63 47-123 3,Y-Dichlorobenzidine 39.0 10 ug/L 50.00 78 27-129 3/4-Methylphenol 24.7 10 ug/L 50.00 49 29.110 3-Nitrmniline 36.0 10 ug/L 50.00 70 41-128 4,6-Dinibo-2-methyphenol 31.8 10 ug/L 50.00 64 44-137 4-Bromophenyl phenyl ether 34.8 10 ug/L 50.00 70 55-124 4-Chlorc-3-methylphenol 34.9 10 ug/L 50.00 70 52-119 4-Chlomerilline 36.4 10 ug/L 50.00 73 33-117 4-Chlorophenyl phenyl ether 32.6 10 ug/L 50.00 65 53-121 4-Nitroaniline 30.4 10 ug/L 50.00 61 45-135 4-Nitrophenol 14.5 10 ug/L 50.00 29 10-77 Acenaphthene 34.0 10 ug/L 50.00 68 47-122 Acenaphthylene 35.7 10 ug/L 50.00 71 41-130 Aniline 50.6 10 ug/L 50.00 101 12-197 Anthramne 38.8 10 ug/L 50.00 78 57-123 Azobenzene 37.9 10 ug/L 50.00 76 61-116 Benzo(a)anthracene 37.0 10 ug/L 50.00 74 58-125 Senzo(a)pymne 37.7 10 ug/L 50.00 75 54-128 Benzo(b)fluorenthene 38.5 10 ug/L 50.00 77 53-131 Benzo(g,h,i)peMene 36.6 10 ug/L 50.00 73 50-134 Benzo(k)0uoramhene 36.3 10 ug/L 50.00 73 57-129 Benzoic Acid BRL 100 ug/L 50.00 10-125 L Benzyl alcohol 30.0 10 ug/L 50.00 60 31-112 bis(2-Chloraethoxy)methane 30.2 10 ug/L 50.00 60 48-120 Bis(2-Chkm:ethyl)ether 28.8 10 ug/L 50.00 58 43-118 Bis(2chlomisopropylather 25.4 10 ug/L 50.00 51 37-130 8is(2-Ethylhexyl)phthalate 36.8 10 ug/L 60.00 74 55-135 Butyl benzyl phthalate 34.7 10 ug/L 50.00 69 53-134 Chrysene 37.8 10 ug/L 50.00 76 59-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. "11 Spdngbrook Road - P.O. Box 240643 - Charlotte, NC 29224-0643 Phone: 7041629-6364 - Toll Free Number: l-800/529.6364-Fax: 7WS25-0409 Page 240131 Full -Service Anal ncal 6 Lt.PFR I S M I Environmental s lutian, . ��aroe�Es �Na Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, INC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Result Limit Units Level II QC Report 8/3117 Prism Work Order: 7070346 Time Submitted: 7/20/2017 4:40:001PM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P7G0369 - 3510C MS LCS (107130369-13SI) Prepared $ Analyzed: 07/25/17 Dibenzo(a,h)anthracene 36.1 10 ug/L 50.00 72 51-134 Dibenzofumn 36.3 10 ug/L 50.00 73 53-118 Diethyl phthalate 36.2 10 ug/L 50.00 72 56-125 Dimethyl phthalate 34.1 10 ug/L 50.00 68 45-127 Di-n-butyl phthalate 39.2 10 ug/L 50.00 78 59-127 Di-n-octyl phthalate 37.7 10 ug/L 50.00 75 51-140 Fluoranthene 36.1 10 ug/L Moo 72 57-128 Fluorene 34.1 10 ug/L 50.00 68 52-124 Hexachlorobenzene 37.7 10 ug/L 50.00 75 53-125 Hamchlorobutadiene 24.1 10 ug/L 50.00 48 22-124 Hexachlorocydopentadiene 26.3 10 ug/L 50.00 53 32-117 Hexachlomethane 21.1 10 ug/L 50.00 42 21-115 Indeno(1,2,3-cd)pynme 38.3 10 ug/L 50.00 77 52-134 Isophorone 32A 10 ug/L 50.00 65 42-124 Naphthalene 29.6 10 ug/L 50.00 59 40-121 Nitrobenzene 27.4 10 ug/L 50.00 55 45-121 N-Niuoso-di-n-propylamine 31.4 10 ug/L 50.00 63 49-119 N-Nitrosodiphenylemine 46.7 10 ug/L 50.00 93 51-123 Pentachlorophenol 40.8 10 ug/L 50.00 82 35-138 Phenanthrene 38.2 10 ug/L 50.00 76 59-120 Phenol 17.4 10 ug/L 50.00 35 12-58 Pyrene 37.2 10 ug/L 50.00 74 57-126 Surrogate: 2,4,6-Tribromopheno/ 77.2 ug/L 1000 77 43140 Surrogate: 2-Fluorobipheny4 34.6 U91L 50.00 69 44-119 Surrogate: 2-Fluomphenol 43.7 U91L 100.0 44 19-119 Surrogate: Nitrobenzene-05 30.1 ug& 50.00 60 44-120 Surrogate: Pheno/d5 29.3 U91L 100.0 29 11-52 Surrogate: Terphenyld14 44.3 U91L 50.00 89 50-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704IS29-6364 - Toll Free Number: 1.800/629.6364 - Fax: 704/525.0409 Page 25 of 31 P R f S M l r°° ae.° ce n ai>tieai a Env ronmental Solutions .._. _ uaoanow,Ea,rvc. Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Analyte Result Limit Units Level 11 QC Report 813/17 Prism Work Order: 7070346 Time Submitted: 7/20/2017 4:40:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P7GO369 - 3510C MS - LCS Dup (P7GO36943SD7) Prepared & Analyzed: 07/25/17 1,2,4-Tdchlorobenzene 26.3 10 ug/L 50.00 53 29-126 4 20 1,2-Dichlorobenzene 26.1 10 ug/L 50.00 52 32-111 8 20 1,3-Dichlorobenzene 24.4 10 ug/L 50.00 49 28-110 6 20 1,4-Dichlorobenzene 24.6 10 ug/L 50.00 49 29-112 6 20 1-Methylnaphthelene 32.3 10 ug/L 50.00 65 41-119 4 20 2,4,5-Tdchlorophenol 39.2 10 ug/L 50.00 78 53-123 4 20 2,4,6-Tdchlorophenol 36.9 10 ug/L 50.00 74 50-125 2 20 2,4-Dichlorophenol 33.7 10 ug/L 50.00 67 47-121 5 20 2,4-Dimethylphenol 42.0 10 ug/L 50.00 84 31-124 2 20 2,4-Dinitrophenol 28.8 10 ug/L 50.00 58 23-143 8 20 2,4-Dinitrotoluene 37.0 10 ug/L 50.00 74 57-128 2 20 2,6-Dinkratoluene 38.8 10 ug/L 50.00 78 57-124 3 20 2-Chlomnaphthalene 33.9 10 ug/L 50.00 68 40-116 2 20 2-Chlorophenol 34.4 10 ug/L 50.00 69 38-117 8 20 2-Methylnaphthelene 31.2 10 ug/L 50.00 62 40-121 4 20 2-Methylphenol 33.8 10 ug/L 50.00 68 30-117 5 20 2-Nitroaniline 32.7 10 ug/L 50.00 65 55-127 0.4 20 2-Nitrophenol 33.7 10 ug/L 50.00 67 47-123 7 20 30-Dichlorobenzidine 41.5 10 ug/L 50.00 83 27-129 6 20 3/4-Methylphenol 26A 10 ug/L 50.00 53 29-110 7 20 3-Nitroaniline 37.3 10 ug/L 50.00 75 41-128 6 20 4,6-Diniho-2-methylphenol 33.6 10 ug/L 60.00 67 44-137 5 20 4-Bromophenyl phenyl ether 36.4 10 ug/L 50.00 73 55-124 4 20 4-Chloro-3-methylphenol 37.1 10 ug/L 50.00 74 52-119 6 20 4-Chloroaniline 40.6 10 ug/L 50.00 81 33-117 11 20 4-Chlomphenyl phenyl ether 34.3 10 ug/L 50.00 69 53-121 5 20 4-Nitroaniline 30.8 10 ug/L 50.00 62 45-135 1 20 4-Nitrophenol 16.3 10 ug/L 50.00 31 10-77 5 20 Acenaphthene 34.8 10 ug/L 50.00 70 47-122 2 20 Acenaphthylene 36.8 10 ug/L 50.00 74 41-130 3 20 Aniline 64.0 10 ug/L 50.00 128 12-197 23 20 D Anthracene 40.3 10 ug/L 50.00 81 57-123 4 20 Azobenzene 39.0 10 ug/L 50.00 78 61-116 3 20 Benzo(a)ardhrecene 38.2 10 ug/L 50.00 76 68-125 3 20 Bemo(a)pyrene 37A 10 ug/L 50.00 75 54-128 0.8 20 Benzo(b)fluomnthene 38.9 10 ug/L 50.00 78 63-131 1 20 Benzo(g,h,i)perylene 36.4 10 ug/L 50.00 73 50-134 0.4 20 Benzo(k)fluomnthene 36.7 10 ug/L 50.00 73 57-129 1 20 Benzoic Acid 4.73 100 ug/L 50.00 9 10-125 29 20 D, L, J Benzyl alcohol 32.4 10 ug/L 50.00 65 31-112 8 20 bis(2-Chlorcethoxy)rnethane 32.3 10 ug/L 50.00 65 48-120 7 20 Bis(2-Chloroethyl)ether 26.2 10 ug/L 50.00 52 43-118 9 20 Bis(2-chloro1sopropyl)ather 27.6 10 ug/L 50.00 55 37-130 8 20 Bis(2-Ethylhexyl)phthalate 37.9 10 ug/L 50.00 76 55-135 3 20 Butyl benzyl phthalate 36.0 10 ug/L 50.00 72 53-134 4 20 Chrysene 39.6 10 ug/L 50.00 79 59-123 5 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1-800/629-6364 - Fax: 7041525-0409 Page 26 of 31 rR I SI V I �I I Fumll aery ce Analytical - Env'nmental Solutions Ili5 �D,.,e rs „� Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch MOM - 3510C MS Reporting Result Limit Units Level II OC Report 8/3/17 Prism Work Order: 7070346 Time Submitted: 7/20/2017 4:40:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Cup (P7G036943SD7) Prepared 8 Analyzed: 07/25/17 Dibenzo(a,h)anthmcene 73.0 10 ug/L 50.00 146 51-134 68 20 D, L2 Dibenzofumn 37.2 10 ug/L 50.00 74 53-118 2 20 Diethyl phthalate 37.0 10 ug/L 50.00 74 56.125 2 20 Dimethyl phthalate 35.3 10 ug/L 50.00 71 45-127 3 20 Di-n-butyl phthalate 40.5 10 ug/L 50.00 81 59-127 3 20 Di-n-octyl phthalate 39.0 10 ug/L 50.00 78 51-140 4 20 Fluoranthene 37.9 10 ug/L 50.00 76 57-128 5 20 Fluorene 35.4 10 ug/L 50.00 71 52-124 4 20 Hexachlorobenzene 39.1 10 ug/L 60.00 78 53-125 4 20 Hexachlorobutadiene 25.1 10 ug/L 50.00 50 22-124 4 20 Hexachlorocydopentadiene 27.3 10 ug/L 50.00 55 32-117 3 20 Hemchlomethane 23.2 10 ug/L 50.00 46 21-115 9 20 Indeno(1,2,3.cd)pyrene 37.8 10 ug/L 50.00 76 52-134 1 20 Isophorone 34.0 10 ug/L 50.00 68 42-124 5 20 Naphthalene 31.0 10 ug/L 50,00 62 40-121 4 20 Nitrobenzene 29.0 10 ug/L 50.00 58 45-121 6 20 N-Nitroso-di-n-propylamine 32.2 10 ug/L 50.00 64 49-119 2 20 N-Nitmsodiphenylamine 47.7 10 ug/L 50.00 95 51-123 2 20 Pentachlorophenol 41.9 10 ug/L 50.00 84 35-138 3 20 Phenanthrene 39.8 10 ug/L 50.00 80 59-120 4 20 Phenol %2 10 ug/L 50.00 38 12-58 10 20 Pyrene 37.9 10 ug/L 50.00 76 57-126 2 20 Surrogate: 2,4,6-Tribromophenol 80.8 u91L 100.0 81 43-140 Surmgate: 2-Fluorobiphenyl 36.8 u9/L 50.00 72 44-119 Surrogate: 2-F/uorophenol 48.4 u91L 100.0 48 19-119 Surrogate: Nitrobenzene-d5 31.7 ug/L 50.00 63 44-120 Surrogate: Phenol -al 32.4 ug/L 100.0 32 11-52 Surrogate: Terpheny4414 45.7 ug/L 50.00 91 50-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spdngbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0643 Phone: 7041529-6364 - Toll Free Number: 1-8001629-6364-Few 7041525.0409 Page 27 of 31 M PS R I Full -Service Analytical & ,, I ISM Environmental Soiotians Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Petroleum Hydrocarbons by GC/PIDIFID - Quality Control Reporting Result Limit Units Batch MUM - MADEP VPH Level II QC Report 8/3117 Prism Work Order: 7070346 Time Submitted: 7/20/2017 4:40:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (107430439-BLK7) Prepared & Analyzed: 07/27/17 CS-C8 Aliphatics BRL 50 ug/L C9-C12 Aliphatics BRL 50 ug/L C9-C10 Aromatics BRL 50 ug/L Surrogate: 2,5-Dibromotoluene (PID) 93.7 ug/L 100.0 94 70-130 Surrogate: 2,5-Dibromotoluene (FID) 107 ug/L 100.0 107 70-130 LCS (P7130439-BS1) Prepared & Analyzed: 07/27/17 C5-08 Aliphatics 360 50 ug/L 300.0 120 70-130 C9-C10 Aromatics 92.2 50 ug/L 100.0 92 70-130 C9-Cl2 Aliphatic 354 50 ug/L 300.0 118 70-130 Surrogate: 2,5-Dibromotoluene (PID) 90.3 U91L 100.0 90 70-130 Surrogate: 2,5-Dibromoto/uene (FID) 103 ug/L 100.0 103 70-130 LCS Dup (P7GO439-OSDt) Prepared & Analyzed: 07/27/17 CS-C8 Aliphatics 343 50 ug/L 300.0 114 70-130 5 50 C9-C10 Aromatics 90.8 50 ug/L 100.0 91 70-130 2 50 CO-Cl 2 Aliphatic 345 50 ug/L 300.0 115 70-130 3 50 Surrogate: 2,5-Dibromotoluene (PID) 89.7 ug/L 100.0 90 70-130 Surrogate: 2,5-Dibromotoluene (FID) 102 ug/L 100.0 102 70-130 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. "a Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 704/629-6364 - Toll Free Number: 1-0001529-0364 - Fex: 704/525-0409 Page 28 of 31 'V'>� I FWvlroFaervmWice Analytical a Ennenial aoLona �frnae$INL Geoscience Group Attn: Tam Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Extractable Petroleum Hydrocarbons by GCIFID - Quality Control Analyte Reporting Result Limit Units Level II QC Report 813/17 Prism Work Order: 7070346 Time Submitted: 7/20/2017 4:40:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P7GO415 - MADEP EPH (W) Blank (P7G0415-BLK7) Prepared: 07/26/17 Analyzed: 07/27/17 C9-C78NiphaOce 24.9 350 ug/L J C19-C36Aliphatics SRL 500 ug/L Cl1-C22 Aromatics BRL 100 ug/L Surrogate: 1-Chlorooctadecane 12.1 ug/L 20.00 61 40-140 Surrogate: o-Tomhenyl 13.0 u91L 20.00 65 40-140 Surrogate: 2-Fluorobipheny/ 34.1 ug2 40.00 85 40-140 Surrogate: 2-Bromonaphtha/ene 42.2 ug/L 40.00 106 40-140 LCS (P7GO415-BS1) Prepared: 07/26/17 AnaWW: 07/27/17 co-c18Aliphatics 309 350 ug/L Sol 51 40-140 J CID-C36 Aliphatics 650 Soo uglL 800.0 69 40-140 C11-C22 Aromatics 1400 100 119/1. 1700 83 40-140 Surrogate: 1-Chlorooctadecane 13.6 ugA 20.00 68 40-140 Surrogate: 0-Terphenyl 14.3 ug/L 20.00 72 40-140 Surrogate: 2-Fluorobipheny4 35.3 ug/L 40.00 a8 40-140 Surrogate:2-Bromonephthalene 40.3 ug/L 40.00 101 40-140 LCS Dup (P7GO41543SD1) Prepared- 07/26/17 Analyzed- 07/27/17 C9-C18 Aliphatics 291 350 uglL 600.0 49 40.140 6 50 J C19-C36Aliphatios 518 500 ug/L 800.0 65 40-140 6 50 C11-C22 Aromatics 1390 100 L%A 1700 82 40-140 1 50 Surrogate: l-Chlorooctedecane 12.8 u91L 20.00 64 40-140 Surrogate: o-Terphenyl 14.0 u91L 20.00 70 40-140 Surrogate: 2-FluorobiphenN 35.0 ug/L 40A0 87 40-140 Surrogate: 2-Bromonaphthalene 38.9 ug/L 40.00 97 40-140 This report should not be reproduced, except in its entirety, without the written consent of Pdsm Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041629-6364 - Toll Free Number: 1-800/529-6364-Fax:7041525-0409 Page 29 of 31 Sample Extraction Data Prep Method: MADEP EPH (M Lab Number Batch Initial Final Date/Time 7070346-01 P7G0415 1000 mL 2 mL 07/26/17 12:30 Prop Method: 351 CC MS Lab Number Batch Initial Final Date/Time 7070346-01 P7G0369 650 mL 1 mL 07/25/17 8:20 7070346-02 P7GD369 1000 mL 1 mL 07/25/17 8:20 7070346-03 P7G0369 1000 mL 1 mL 07/25/17 8:20 Prep Method: 5030E Lab Number Batch Initial Final Date/Time 7070346-01 P7G0491 10 mL 10 mL 07/31/17 10:26 7070346-01 P7G0491 10 mL 10 mL 07/31/17 10:26 7070346-02 P7G0491 10 mL 10 mL 07/31/17 10:26 7070346-03 P7G0491 10 mL 10 mL 07/31/17 10:26 Prep Method: MADEP VPH (W( Lab Number Batch Initial Final DabuTime 7070346-01 P7G0439 44 mL 44 mL 07/27/17 15:03 7070346-01 P7GD439 44 mL 44 mL 07/27/17 15:03 This report should not be reproduced, except in its entirety, without the written consent of Prism Labomtodes, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/52946364 -Toll Free Number: 1.800/529-6364 -Fax: 704152541409 Page 30 of 31 Y_ (S ❑ ❑ Q 'O g e VJ 3 C' $ c < ga U wppppp p � g� m N f t W � 0 g' 3 a I yv g 'o X3 ro = o z m r a a'°`O m m I m m m � O W W wm TN i� NC \ g� 8� �a m i � m g 0 3 a 2 pa ma°m1 99c� ' o r r o m 0 0Z T w m n w-D � � h F 4 m � r m m c° ami mS ' 1 ram W y 3 omnal G o .8 W g r m 1N o 111 mAN� M W Is 0 ❑ � = i i'p" o p W �4 F p yc, f• W m =N O �a � OZEU A Qv m n Cry III1II w yy mC O fil ° NJ � N ' Ccpg42 m C q ¢om.. O ❑ yN mF. RAp ti 7�,5 r $ 3 p f.' `fj- y ry S �N �f Y w \ COO 3 o m () 24 m w�i m RI \C p a � 5 � m 0_ pc o m y m Z \ ,p ( N I" 0 IA r m �IZm°.Z-� mi z °o w I w I I r r ( Z O M Ia z A O a 22 0 z z S r � Q 3 9 w �s' w z NC n Y�`•j e R v C i n ?_ IT 30 $ >22 w w II�_ -1 O IT o�N 2 z p2 G S 91 03 6 Z C bf 0 ` m CA } e O v 9 m�; m _p O•i v n ,a M � � 1 a 1 I.i 1 PRISM Full -Service Analytical Environmental Solutions a: IAWRATORM INC Geoscience Group Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 NC Certifici lion No. 402 NC Drinking Water Cart No. 37735 SC Certification No. 99012 Project: Truck Part Service Lab Submittal Date: 07/21/2017 Prism Work Order: 7070398 Case Narrative 07/31 /2017 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are Flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. a --.-I Angela D. Overcash VP Laboratory Services Data Qualifiers Key Reference w Reviewed By Terri W. Cole For Angela D. Overcash Project Manager A The CCV result is below the established QC limits. This compound was not detected in samples down the MDL. D RPD value outside of the control limits. J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag). L Parameter reported with possible low bias. LCS recovery below the QC limit. L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529.6364-Toll Free Number: 1-8001529-6364-Fax:704/525-0409 Page 1 of 13 P R I S IVI I Fuu Service venal ecal Eam.enmemai ammmna Sample Receipt Summary 07/31/2017 Prism Work Order: 7070398 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received TW-1 7070398-01 Water 07/21/17 07/21/17 Samples were received in good condition at 5.8 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of P65m Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Tall Free Number: 1-8001529-6364 - Fax: 704/525-Mg Page 2 of 13 Summary of Detections Scrnce Analytical & P I S M R FnmFull ronmemal snwrrons 07/31/2017 Prism Work Order: 7070398 Pdsm ID Client ID Parameter Method Result Units 7070398-01 TW-1 C9-C18 Aliphatics MADEPEPH 460 ug/L 7070398-01 TW-1 C11-C22 Aromatics MADEP EPH 720 ug/L 7070398-01 TW-1 1-Methylnaphthalene 8270D 100 ug/L 7070398-01 TW-1 2-Methylnaphthalene 8270D 130 ug/L 7070398-01 TW-1 Benzoic Acid 8270D 11 .l ug/L 7070398-01 TW-1 Diethyl phthalate 8270D 70 ug/L 7070398-01 TW-1 Naphthalene 8270D 330 ug/L This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0S43 Phone: 7041529-6364 -Toll Free Number; 1-8001529.6364 - Fax:7041525-0409 Page 3 of 13 PR I SpM I Fmbae "ice aoaln si a „roA m ,Es � Eaowno�s Laboratory Report 07/31/2017 Geoscience Group Project: Truck Part Service Client Sample ID: TW-1 Attn: Tom Hassett Prism Sample ID: 7070398-01 500-K Clanton Rd. Prism Work Order: 7070398 Charlotte, NC 28217 Sample Matrix: Water Time Collected: 07/21/17 09:21 Time Submitted: 07/21/17 10:50 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/rime ID Extractable Petroleum Hydrocarbons by GCOD C9-C18 Aliphatics 460 ug/L 9 350 22 1 MADEP EPH 72711716:46 7RC P7G0415 C19-C36 Aliphatics BRL ug/L 500 63 1 MADEP EPH 7/27117 16:46 ZRC P7G0415 C11-C22 Aromatics 720 ug/L 100 55 1 MADEP EPH 7127117 16:46 7Rc P7G9N6 Surrogate Recovery Control Limits 1-Chlorooctedecene 42 % 40-140 o-Terphenyl 54 % 40-140 2-Fluorobiphenyl 88 % 40-140 2-Bromonaphthalene 92 % 40-140 Semivolatile Organic Compounds by GC/MS 1,24-Tichoorobenzene BRL ug/L 10 1.8 1 8270D 7/25/17 19:07 JMV P7G0369 1,2-Dichlorobenzene BRL ug/L 10 1.6 1 8270D 725117 19:07 JMV P7G0369 1,3-Dichlorobenzene BRL ug/L 10 1.9 1 8270D 725117 19:07 JMV P7G0369 1,4-Dichlorobenzene BRL ug/L 10 1.6 1 8270D 725/17 19:07 JMV P7G0369 1-Methyinaphd,alene 100 ug/L 9 10 2.6 1 8270D 725/1719:07 JMV P7G0369 2,4,5-Tdchlorophenol BRL ug/L 10 1.6 1 8270D 7125/17 19:07 JMV P7G0369 2,4,6-Trichlomphenol BRL ug/L 10 1.8 1 8270D 7/25/17 19:07 JMV P7130369 2,4-Dichlorophenol BRL ug/L 10 2.6 1 8270D 7/25117 19:07 JMV P7G0369 2.4-Dimethylphenol BRL ug/L 10 3.4 1 8270D 7/25/17 19:07 JMV P7130369 2,4-Dinitrophenol BRL ug/L 10 2.7 1 8270D 7126/17 19:07 JMV P7G0369 2,4-Dinitrotoluene BRL ug/L 10 1.4 1 82700 725/17 19:07 JMV P7130369 2,6-Dinitrotoluene BRL ug/L 10 1.1 1 8270D 7/25117 19:07 JMV P7G0369 2-Chlomnaphthalene BRL u /L 9 10 2.7 1 8270D 7/25/17 19:07 JMV P7G0369 2-Chlorophenol BRL ug/L 10 1.9 1 8270D 7/25117 19:07 JMV P7G0369 2-Methylnaphthalene 130 ug/L 10 2.4 1 8270D 7/25/17 19:07 JMV P7G0369 2-Methylphenol BRL ug/L 10 1.8 1 8270D 725/17 19:07 JMV P7130369 2-Nitroaniline BRL ug/L 10 1A 1 8270D 7/25117 19:07 JMV P7G0369 2-Nitrophenol BRL ug/L 10 2.4 1 8270D 7125/17 19:07 JMV P7G0369 3,3' 01chlorobenzidine BRL ug/L 10 1.4 1 8270D 725117 19:07 JMV P7130369 3/4-Methylphenol BRL ug/L 10 1.5 1 8270D 7125/17 19:07 JMV P7G0369 3-Nitroaniline BRL ug/L 10 1.4 1 8270D 7125/17 19:07 JMV P7G0369 4,6-Dinitro-2-methylphenol BRL ug/L 10 1.4 1 8270D 7/25/17 19:07 JMV P7G0369 4-Bromophenyl phenyl ether BRL ug/L 10 1.3 1 8270D 7/25117 19:07 JMV P7G0369 4-Chloro-3-methylphenol BRL ug/L 10 2.4 1 8270D 725/17 19:07 JMV P7G0369 4-Chloroanilins BRL ug/L 10 2.4 1 8270D 7/25117 19:07 JMV P7G0369 4-Chlorophenyl phenyl ether BRL ug/L 10 1.3 1 8270D 7125117 19:07 JMV P7G0369 4-Nitroaniline BRLA ug/L 10 0.93 1 8270D 7125/17 19:07 JMV P7G0369 4-Nitrophenol BRL ug/L 10 0.60 1 8270D 7/25/17 19:07 JMV P7G0369 Acenaphthene BRL ug/L 10 1.8 1 8270D 7125/17 19:07 JMV P7G0369 Acenaphthylene BRL ug/L 10 2.0 1 8270D 7/25117 19:07 JMV P7130369 Aniline BRL ug/L 10 2.4 1 a270D 7/25117 19:07 JMV P7G0369 Anthracene BRL ug/L 10 1.4 1 8270D 725/17 19:07 JMV P7430369 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. "a Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1.8001529.6364 - Fax: 704/52541409 Page 4 of 13 P Z�P R I S M I Fun service nnalrilcai s (' p.... Environmental Solu9onA Laboratory Report 07131/2017 Geoscience Group Project: Truck Part Service Client Sample ID: TW-1 Attn: Tom Hassett Prism Sample ID: 7070398-01 500-K Clanton Rd. Prism Work Order: 7070398 Charlotte, NC 28217 Sample Matrix: Water Time Collected: 07/21/17 09:21 Time Submitted: 07/21/17 10:50 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Azobenzene BRL ug/L 10 1.8 1 8270D 7125117 19:07 JMV P7G(Y369 Benzo(a)anthracene BRL ug/L 10 1.4 1 8270D 7/25/17 19:07 JMV P7G0369 Benzo(a)pyrene BRL ug/L 9 10 1.4 1 8270D 7/25/17 19:07 JMV P7G0369 Benzo(b)luoronthene BRL ug/L 10 1.1 1 8270D 7/25/17 19:07 JMV P7G0369 Benzo(g,hJ)perylene BRL ug/L 10 1.4 1 8270D 7125/17 19:07 JMV P7G0369 Benzo(k)fluoranthene BRL ug/L 10 1.4 1 8270D 7125117 19:07 JMV P7G0369 Benzoic Add 11 J ugh 100 4.7 1 8270D 7125117 19:07 JMV P7G0369 Benzyl alcohol BRL ug/L 10 2.1 1 8270D 7/25117 19:07 JMV P7G0369 bis(2-Chloroethoxy)methane BRL ug/L 10 2.6 1 8270D 7/25/17 19:07 JMV P7G0369 Bis(2-Chloroethyl)ether BRL ug/L 10 2.3 1 8270D 7/25/17 19:07 JMV P7G0369 Bis(2-chloroisopropyl)ether BRL ug/L 10 2.0 1 8270D 7/25/17 19:07 JMV P7G0369 Bis(2-Ethylhexy4phthalate BRL ug/L 10 1.3 1 8270D 7125/17 19:07 JMV P7G0369 Butyl benzyl phthalate BRL ug/L 10 1.4 1 8270D 7125117 19:07 JMV P7G0369 Chrysene BRL ug/L 10 1.4 1 8270D 7/25/17 19:07 JMV P7G0369 Dibenzo(a,h)anthracene BRL ug/L 10 1.2 1 82700 7125/17 19:07 JMV P7G0369 Dibenzofumn BRL ug/L 10 1.8 1 8270D 7/25117 19:07 JMV P7G0369 Diethyl phthalate 70 ug/L 10 3.3 1 82700 7125117 19:07 JMV P7G0369 Dimethyl phthalate BRL ug/L 10 1.4 1 8270D 7125/17 19:07 JMV P7G0369 Di-n-butyl phthalate BRL ug/L 10 1.7 1 8270D 7/26/17 19:07 JMV P7G0369 Di-n-octyl phthalate BRL ug/L 10 1.3 1 8270D 7/25/17 19:07 JMV P7G0369 Fluoranthene BRL ug/L 10 1.7 1 8270D 7125117 19:07 JMV P7130369 Fluorene BRL ug/L 10 1.7 1 8270D 7/25/17 19:07 JMV P7G0369 Hexachlorobenzene BRL ug/L 10 1.3 1 8270D 7/25/17 19:07 JMV P7G0369 Hexachlombutadiene BRL ug/L 10 2.1 1 8270D 7/25117 19:07 JMV P7G0369 Hexachlorocydopentadiene BRL ug/L 10 1.7 1 8270D 7/25117 19:07 JMV P7G0369 Hexachloroethane BRL ug/L 10 1.7 1 8270D 7125/17 19:07 JMV P7G0369 Indeno(1,2,3-cd)pyrene BRL ug/L 10 3.9 1 8270D 7/25M7 19:07 JMV P7G0369 Isophorone BRL ug/L 10 2.5 1 8270D 7125117 19:07 JMV P7G0369 Naphthalene 330 ug/L 50 13 5 8270D 7/26/17 11:46 JMV P7G0369 Nitrobenzene BRL ug/L 10 2.6 1 8270D 7/26/17 19:07 JMV P7G0369 N-Nitroso-dl-n-propylamine BRL ug/L 10 2.2 1 8270D 7125/17 19:07 JMV P7G0369 N-Nitrosodiphenylemine BRL ug/L 10 1.3 1 8270D 7126117 19:07 JMV P7G0369 Pentachlorophenol BRL ug/L 10 1.2 1 82700 7/25117 19:07 JMV P7G0369 Phenanthrene BRL ug/L 10 1.5 1 8270D 7/26/17 19:07 JMV P7G0369 Phenol BRL ug/L 10 0.98 1 82700 7125117 19:07 JMV P7G0369 Pyrene BRL ug/L 10 1.4 1 8270D 7/25/17 19:07 JMV P7G0369 Surrogate Recovery Control Limits 2,4,8-Tribromophenol 83 % 43-140 2-Fluorobiphenyl 76 % 44-119 2-Fluorophenol 55 % 19-119 Nitrobenzene-d5 70 % 44-120 Phenol-d5 36 % 11-52 Terphenyl-dl4 92 % 50-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 704/529.6364- Toll FroeNumber. l-800/529-6364-Fax:7041526-0409 Page 5 of 13 Full-Sarvlce Analytical & R I SpM Envlranm¢n,al sciatica. uaaa..a I, „x Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, INC 28217 Project: Truck Part Service Samivolatile Organic Compounds by GC/MS - Quality Control Analyte Reporting Result Limit Units Level II QC Report 7/31/17 Prism Work Order: 7070398 Time Submitted: 7/21/2017 10:50:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch 137430369 - 351 OC MS Blank (P7GO369-BLK1) Prepared & Analyzed: 07/25/17 1,2,4-Tdchlorobenzene BRL 10 ug/L 1,2-Dichlorobemene BRL 10 ui 1,3-Dichlorobenzene BRL 10 ug/L 1,4-Dichlorobenzene BRL 10 ug/L 1-Methylnaphthalene BRL 10 ug/L 2,4,5-Tdchlorophenol BRL 10 ug/L 2,4,6-Tdchlomphenol BRL 10 ug/L 2,4-Dichlomphenol BRL 10 ug/L 2,4-Dimethylphenol BRL 10 ug/L 2,4-Dinitrophenol BRL 10 ug/L 2,4-Dinibotoluene BRL 10 ug/L 2,6-Dinitrotoluene BRL 10 ug/L 2-Chloronaphthalene BRL 10 ug/L 2-Chlorophenol BRL 10 ug/L 2-Methylnaphthalene BRL 10 ug/L 2-Methylphenol BRL 10 ug/L 2-Nitroaniline BRL 10 ug/L 2-Nitrophenol BRL 10 ug/L 3,3' Dichlorobenzidine BRL 10 ug/L 3/4-Methylphenol BRL 10 ug/L 3-Nilmaniline BRL 10 ug/L 4,6-Din0ro-2-methylphenol BRL 10 ug/L 4-Bromophenyl phenyl ether BRL 10 ug/L 4-Chloro-3-methylphenol BRL 10 ug/L 4-Chloroaniline BRL 10 ug/L 4-Chlorophenyl phenyl ether BRL 10 ug/L 4-Nitroaniline BRL 10 ug/L 4-Nibophenol BRL 10 ug/L Acenaphthene BRL 10 ug/L Acenaphthylene BRL 10 ug/L Aniline BRL 10 ug/L Anthrocene BRL 10 ug/L Azobenzene BRL 10 ug/L Senzo(a)anthracene BRL 10 ug/L Bemo(e)pyrene BRL 10 ug/L Benzo(b)fluoranthene BRL 10 ug/L Benzo(g,h,i)perylene BRL 10 ug/L Benza(k)nuoranthene BRL 10 ug/L Benzoic Acid BRL 100 ug/L Benzyl alcohol BRL 10 ug/L bis(2-Chlormthoxy)rnethane BRL 10 ug/L Bis(2-Chlomethyl)ether BRL 10 ug/L Bis(2-chloroisopropyl)ather BRL 10 ug/L Bis(2-Ethylhexyl)phthalate BRL 10 ug/L Butyl benzyl phthalate BRL 10 ug/L Chrysene BRL 10 ug/L This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364-Toll Free Number: l-8001529.6364- Fax: 704/525-0409 Page 6of 13 h R IJ M I Full -Service Hnaly[ cal a Eom.onmencel sowuoos ... YBoxniOnlEA ll.`G Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Chadotte, NC 28217 Project: Truck Part Service Semlvolatile Organic Compounds by GC/MS - Quality Control Analyte Reporting Result Limit Units Level II QC Report 7/31/17 Prism Work Order: 7070398 Time Submitted: 7/21/2017 10:50:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch 137GO369 -351DC MS Blank (P7GO36943LK1) Prepared & Analyzed: 07/25/17 Dibenzo(a,h)anthracene BRL 10 ug/L Dibenzofuran BRL 10 ug/L Diethyl phthalate BRL 10 ug/L Dimethyl phthalate BRL 10 ug/L Di-n-butyl phthalate BRL 10 ug/L Di-n-octyl phthalate BRL 10 ug/L Fluoranthene BRL 10 ug/L Fluorene BRL 10 ug/L Hexachlombenzene BRL 10 ug/L Hexachlorobutadiene BRL 10 ug/L Hexachlorocydopentadiene BRL 10 ug/L Hexachloroethane BRL 10 ug/L Indeno(1,2,3-od)pyrene BRL 10 ug/L Isophorone BRL 10 ug/L Naphthalene BRL 10 ug/L Nitmbenzene BRL 10 ug/L N-Nitroso-di-n-propylamine BRL 10 ug/L N-Nitrosodiphenylamine BRL 10 ug/L Pentachlorophenol BRL 10 ug/L Phenanthrene BRL 10 ug/L Phenol BRL 10 ug/L Pyrene BRL 10 ug/L Surrogate: 2,4,6-Tribromopheno/ 81.9 ug/L 100.0 82 43-140 Surrogate: 2-F/uorobipheny/ 32.6 u91L 50.00 65 44-119 Surrogate: 2-Fluomphenol 46.2 u91L 100.0 46 19-119 Surrogate: Ndmbenzened5 29.1 ug4. 50.00 58 44-120 Surrogate: Phenold5 30.5 u91L 100.0 31 11-52 Surrogate: TerphenyPM4 47.6 u9A 50.00 95 50-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224.0643 Phone: 7041629-6364 - Toll Free Number: 1.8001529-6364 - Fax: 704/525-0409 Page 7 of 13 .FOR I S aa�..oAM I E-�Aron mvmane,eAi Solutions Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, INC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Reporting Result Limit Units Level II QC Report 7/31/17 Prism Work Order: 7070398 Time Submitted: 7/21/2017 10:50:o0AM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch 127130369 - 3510C MS LCS (P7G0369-BSI) Prepared &Analyzed• 07/25/17 1,2,4-Tdchlorobenzene 25.3 10 ug/L 50.00 51 29-126 1,2-Dichlorobenzene 24.2 10 ug/L 50.00 48 32-111 1,3-Dichlorobenzene 23.1 10 ug/L 60.00 46 28-110 1,4-Dichlorobenzene 23.1 10 ug/L 50.00 46 29-112 1-Methylnaphthalene 30.9 10 ug/L 50.00 62 41-119 2,4,5-Trichlorophenol 37.6 10 ug/L 50.00 75 53-123 2,4,6-Tdchlorophenol 36.3 10 ug/L 50.00 73 50-125 2,4-Dichlomphenol 32.0 10 ug/L 50.00 64 47-121 2,4-Dimethylphenol 41.3 10 ug/L 50.00 83 31-124 2,4-Dinibophenol 26.6 10 ug/L 50.00 53 23-143 2,4-Dinibotoluene 36.3 10 ug/L 50.00 73 57-128 2,6-Dinitrotoluene 37.6 10 ug/L 50.00 75 57-124 2-Chloronaphthalene 33.1 10 ug/L 50.00 66 40-116 2-Chlorophenol 31.7 10 ug/L 50.00 63 38-117 2-Methylnaphthalene 29.9 10 ug/L 50.00 60 40-121 2-Methylphenol 32.2 10 ug/L 50.00 64 30-117 2-Nitroaniline 32.8 10 ug/L 50.00 66 65-127 2-Nitrophenol 31.4 10 ug/L 50.00 63 47-123 30-Dichlorobenzidine 39.0 10 ug/L 50.00 78 27-129 3/4-Methylphenol 24.7 10 ug/L 50.00 49 29-110 3-Nitroaniline 35.0 10 ug/L 50.00 70 41-128 4,6-Dinitro-2-methylphenol 31.8 10 ug/L 50.00 64 44-137 4-Bromophenyl phenyl ether 34.8 10 ug/L 50.00 70 55-124 4-Chloro-3-methylphenol 34.9 10 ug/L 50.00 70 52-119 4-Chloroaniline 36.4 10 ug/L 50.00 73 33-117 4-Chlorophenyl phenyl ether 32.6 10 ug/L 50.00 65 53-121 4-Nitroaniline 30A 10 ug/L 50.00 61 45-135 4-Nitrophenol 14.5 10 ug/L 50.00 29 10-77 Acenaphthene 34.0 10 ug/L 50.00 68 47-122 Acenaphthylene 35.7 10 ug/L 50.00 71 41-130 Aniline 50.6 10 ug/L 50.00 101 12-197 Anthracene 38.8 10 ug/L 50.00 78 57-123 Azobenzene 37.9 10 ug/L 50.00 76 61-116 Benzo(a)anthracene 37.0 10 ug/L 50.00 74 58-125 Benzo(a)pyrene 37.7 10 ug/L 50.00 75 54-128 Benzo(b)fiuoranthene 38.5 10 ug/L 60.00 77 53-131 Benzo(g,h,i)perylene 36.6 10 ug/L 50.00 73 50-134 Benzo(k)fluoranthene 36.3 10 ug/L 50.00 73 57-129 Benzoic Acid BRL 100 ug/L 50.00 10-125 L Benzyl alcohol 30.0 10 ug/L 50.00 60 31-112 bis(2-Chloroethoxy)methene 30.2 10 ug/L 50.00 60 48-120 8is(2-Chloroethyl)ether 28.8 10 ug/L 50.00 58 43-118 Bis(2-chlorolsopropyl)ether 25.4 10 ug/L 50.00 51 37-130 Sis(2-Ethylhexyl)phthalale 36.8 10 ug/L 50.00 74 55-136 Butyl benzyl phthalate 34.7 10 ug/L 50oo 69 53-134 Chrysene 37.8 10 ug/L 50,00 76 59-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spdngbrook Road - P.O. Box 240543 - CharloBe, NC 28224-0543 Phone: 70M529.6364-Toll Free Number: 1-800/529-6364 - Fax: 7041525-0409 Page 80 13 P'R I S M I Fu0-Service al Solutions It s Environmental Solutions i"u.eoxmm�ies ixe, Geosclence Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semlvolatile Organic Compounds by GC/MS - Quality Control Analyte Reporting Result Limit Units Level II QC Report 7/31117 Prism Work Order: 7070398 Time Submitted: 7/21/2017 10:50:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P700369 - 351 OC MS LCS (P700389-BSI) Prepared &Analyzed: 07/25/17 Dibenzo(a,h)anthracene 36.1 10 ug/L 50.00 72 51-134 --- Dibenzofuren 36.3 10 ug/L 50.00 73 53-118 Diethyl phthalate 36.2 10 ug/L 50.00 72 56-125 Dime" phthalate 34.1 10 ug/L 50.00 68 45-127 Di-n-butyl phthalate 392 10 ug/L 50.00 78 59-127 Dl-n-octyl phthalate 37.7 10 ug/L 50.00 75 51-140 Fluoramhene 36.1 10 ug/L 50.00 72 57-128 Fluorene 34.1 10 ug/L 60.00 68 52-124 Hexachlorobenzene 37.7 10 ug/L 50.00 75 53-125 Hexachlorobutediene 24.1 10 ug/L 50.00 48 22-124 Hexachlorocydopentadiene 26.3 10 ug/L 60.00 53 32-117 Hexachloroethane 21.1 10 ug/L 50.00 42 21-115 Indeno(1,2,3-cd)pyrene 38.3 10 ug/L 50.00 77 52-134 Isephorone 32.4 10 ug/L 50.00 65 42-124 Naphthalene 29.6 10 ug/L 50.00 59 40-121 Nitrobenzene 27A 10 uglL 50.00 65 45-121 N-Nitroso-di-n-propylamme 31A 10 ug/L 50.00 63 49-119 N-Nitrosodiphenylamine 46.7 10 ug/L 50.00 93 51-123 Pentachlomphenol 40.8 10 ug/L 50.00 a2 35-138 Phenanthrene 38.2 10 ug/L 50.00 76 59-120 Phenol 17A 10 ug/L 50.00 35 12-58 Pyrene 37.2 10 ug/L 50.00 74 57-126 Surrogate: 2,4,6-Tribromophenol 77.2 U91L 100.0 77 43-140 Surrogate:2-Fluorobiphenyl 34.6 ug/L 50.00 69 44-119 Surrogate: 2-Fluompheno/ 43.7 U91L 100.0 44 19-119 Surrogate: Nilrobenzene45 30.1 U91L 50.00 60 44-120 Surrogate: Phenol-d5 29.3 ug/L 100.0 29 11-52 Surrogate: Terpheny4414 44.3 bVL 50.00 89 60-134 This report should not be reproduced, except in its en0rety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529.6364 - Toll Free Number. 1-800/5296364 - Fax: 7041525-0409 Page 9 of 13 :�P R I SpM I Fmi-iroseries Analytical a ueow.o res,xs Envnmental5mutiotions Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Result Limit Units Batch P7G0369 - 3510C MS Level II QC Report 7/31117 Prism Work Order: 7070398 Time Submitted: 7/21/2017 10:50:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (P76036943SD1) Prepared 8 Analyzed: 07/25/17 1,2,4-Tdchlorobamene 26.3 10 ug/L 50.00 53 29-126 4 20 1,2-Dichlombenzene 26.1 10 ug/L 50.00 52 32-111 8 20 1,3-Dichlorobenzene 24.4 10 ug/L 60.00 49 28-110 6 20 1,4-Dichlombenzene 24.6 10 ug/L 50.00 49 29-112 6 20 1-Methylnaphthalene 32.3 10 ug/L 50.00 65 41-119 4 20 2,4,5-Trichlorophenol 39.2 10 ug/L 50.00 78 53-123 4 20 2,4,6-Trichlorophenol 36.9 10 ug/L 50.00 74 50-125 2 20 2,4-Dichlorophenol 33.7 10 ug/L 50.00 67 47-121 5 20 2,4-Dimethylphenol 42.0 10 ug/L 50.00 84 31-124 2 20 2,4-Dintlrophenol 28.8 10 ug/L 50.00 58 23-143 8 20 2,4-Dinkrotoluene 37.0 10 ug/L 50.00 74 57-128 2 20 2,6-Dinitrotoluene 38.8 10 ug/L 50.00 78 57-124 3 20 2-Chloronaphthalene 33.9 10 ug/L 50.00 68 40-116 2 20 2-Chlorophenol 34.4 10 ug/L 50.00 69 38-117 8 20 2-Methylnaphthalene 31.2 10 ug/L 50.00 62 40-121 4 20 2-Methylphenol 33.8 10 ug/L 50.00 68 30-117 5 20 2-Nitroaniline 32.7 10 ug/L 50.00 65 55-127 0.4 20 2-Nitrophenol 33.7 10 ugh 50.00 67 47-123 7 20 3,3'-Dichlorobenzidine 41.5 10 ug/L 50.00 83 27-129 6 20 3/4-Methylphenol 26.4 10 ug/L 50.00 53 29-110 7 20 3-Nitroaniline 37.3 10 ug/L 50.00 75 41-128 6 20 4,6-Dinibo-2-methylphenol 33.6 10 ug/L 50.00 67 44-137 5 20 4-Bromophenyl phenyl ether 36.4 10 ug/L 50.00 73 55-124 4 20 4-Chloro-3-methylphenol 37.1 10 ug/L 60.00 74 52-119 6 20 4-Chloroaniline 40.6 10 ug/L 50.00 81 33-117 11 20 4-Chlorophenyl phenyl ether 34.3 10 ug/L 50.00 69 53-121 5 20 4-Nitroaniline 30.8 10 ug/L 50.00 62 45-135 1 20 4-Nftrophenol 15.3 10 ug/L 50.00 31 10-77 5 20 Acenaphthene 34.8 10 ug/L 50.00 70 47-122 2 20 Acenaphthylene 36.8 10 ug/L 50.00 74 41-130 3 20 Aniline 64.0 10 ug/L 50.00 128 12-197 23 20 D Anthracene 40.3 10 ug/L 50.00 81 57-123 4 20 Azobenzene 39.0 10 ug/L 50.00 78 61-116 3 20 Benzo(a)anthrecene 38.2 10 ug/L 50.00 76 58-125 3 20 Benzo(a)pyrene 37.4 10 ug/L 60.00 75 54-128 0.8 20 Benzo(b)fluomnthene 38.9 10 ug/L 50.00 78 53-131 1 20 Benzo(g,h,i)perylene, 36.4 10 ug/L 50.00 73 50-134 0.4 20 Benzo(k)fluorenthene, 36.7 10 ug/L 50.00 73 57-129 1 20 Benzoic Acid 4.73 100 ug/L 50.00 9 10-125 29 20 D, L, J Benzyl alcohol 32.4 10 ug/L 50.00 65 31-112 8 20 bis(2-Chloroethoxy)nnethane 32.3 10 ug/L 50.00 65 48-120 7 20 Bis(2-Chloroethyl)ether 26.2 10 ug/L 50.00 52 43-118 9 20 Bis(2-chloroisopropyl)ether, 27.6 10 ug/L 50.00 55 37-130 8 20 Bis(2-Ethylhexyl)phthalate 37.9 10 ug/L 50.00 76 55-135 3 20 Butyl benzyl phthalate 36.0 10 ug/L 50.00 72 53-134 4 20 Chrysene 39.6 10 ug/L 50.00 79 59-123 5 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Read - P.O. Box 240543 - Cherlofte, NC 29224.0543 Phone: 7041529-6364- Toll Free Number: 1-800/52M64- Fax: 704152S.0409 Page 10 of 13 F? R I SnM Full Ser ce Analyncel & uawu*o ca,xc Envlronmentel solutions Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Result Limit Units Batch 127G0369 - 3510C MS Level II QC Report 7/31/17 Prism Work Order: 7070398 Time Submitted: 7/21/2017 10:50:00AM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (P7G0369-BSD1) Prepared & Analyzed: 07/25/17 Dibenzo(a,h)anthmcene 73.0 10 ug/L 50.00 146 51-134 68 20 D, L2 Dibenzofuran 37.2 10 ug/L 50.00 74 53-118 2 20 Diethyl phthalate 37.0 10 ug/L 50.00 74 56-125 2 20 Dimethyl phthalate 35.3 10 ug/L 50.00 71 45-127 3 20 Di-n-butyl phthalate 40.5 10 ug/L 50.00 81 59-127 3 20 Di-n-octyl phthalate 39.0 10 ug/L 50.00 78 51-140 4 20 Fluoranthene 37.9 10 ug/L 50.00 76 57-128 5 20 Fluorene 35.4 10 ug/L 50.00 71 52-124 4 20 Hexachlombenzene 39.1 10 ug/L 50.00 78 53-125 4 20 Hexachlorobutadiene 25.1 10 ug/L 50.00 50 22-124 4 20 Hexachlorocydopentediene 27.3 10 ug/L 50.00 55 32-117 3 20 Hexachlomethane 23.2 10 ug/L 50.00 46 21-115 9 20 Indeno(1,2,3-cd)pyrene 37.8 10 ug/L 50.00 76 52-134 1 20 Isophorone 34.0 10 ug/L 50.00 68 42-124 5 20 Naphthalene 31.0 10 ug/L 50.00 62 40-121 4 20 Nitrobenzene 29.0 10 ug/L 50.00 58 45-121 6 20 N-Nitroso-di-n-propylamine 32.2 10 ug/L 50.00 64 49-119 2 20 N-Nitrosodiphenylamine 47.7 10 ug/L 50.00 95 51-123 2 20 Pentachlomphenol 41.9 10 ug/L 50.00 84 35-138 3 20 Phenanthrene 39.8 10 ug/L 60.00 80 59-120 4 20 Phenol 19.2 10 ug/L 50.00 38 12-58 10 20 Pyrene 37.9 10 ug/L 50.00 76 57-126 2 20 Surrogate: 2,4,6-Tnbromopheno/ 80.8 u91L 100.0 81 43-140 Surrogate: 2-Fluorobiphenyl 35.8 u9/L 50.00 72 44-119 Surrogate: 2-F/uomphenol 48.4 u91L 100.0 48 19-119 Surrogate: Ndrobenzen"5 31.7 u91L 50.00 63 44-120 Surrogate: Phenol-05 32.4 u91L 100.0 32 1152 Surrogate: Terpheny4414 45.7 u91L 50,00 91 50-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratones, Inc. 449 Spdn9brook Road - P.O. Box 24060 - charlotte, NC 25224-0543 Phone: 7041629-6364 -Toll Free Number: 1.8001529.6364 - Fax: 7041525-0409 Page 11 of 13 R R I SqM E ropmen An Sonia a � rw.: enmronmemeiamuuons Geoscienoe Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Extractable Petroleum Hydrocarbons by GCIFID -Quality Control Analyte Reporting Result Limit Units Level II QC Report 7131/17 Prism Work Order: 7070398 Time Submitted: 7/21/2017 10:50:OOAM Spike Source %REC RPD Level Result %REC Limits RPD Limit Noter Batch P7GO415 - MADEP EPH (IN) Blank (P713041543LKI) Prepared: 07/26/17 Analyzed: 07/27/17 C9-Cl8Aliphatics 24.9 350 ug/L C19-C36Aliphatics BRL Soo ug/L J C11-C22 Aromatics BRL 100 ug/L Surrogate: l-Chlorooctadecane 12.1 ug/L 20.00 61 40-140 Surrogate: o-Terpheny/ 13.0 ug/L 20.00 65 40-140 Surrogate: 2-171uorobipheny/ 34.1 ug/L 40.00 85 40-140 Surrogate: 2-Bromonaphthalene 42.2 ug/L 40.00 106 40-140 LCS (P70041543S1) Prepared: 07/26/17 Analyzed: 07/27/17 C9-C18 Aliphatics 309 350 ug/L 600.0 51 40-140-1 C19-C36AIiphaOcs 550 500 ug/L eoao 69 40-140 C11-C22 Aromatics 1400 100 ug/L 1700 83 40-140 Surrogate: l-Chlorooctadecane 13.6 ug/L 20.00 68 40-140 Sumtgate: o-Terpheny/ 14.3 ug/L 20.00 72 40-140 Surrogate: 2-F/uorobipheny4 35.3 ug/L 40.00 88 40-140 Surrogate: 2-Bromonaphthalene 40.3 ug/L 40.00 101 40-140 LCS Dup (P7GO415.BSD1) Prepared: 07/26/17 Analyzed: 07/27/17 C9-C18 Aliphatics 291 350 ug/L 600.0 49 40-140 6 50 C19-C36 Aliphatice 518 500 ug/L 800.0 65 40-140 6 50 C11-C22 Aromatics 1390 100 ug/L 1700 82 40-140 1 50 Surrogate: l-Chlorooctedecane 12.8 ugrL 20.00 64 40-140 Surrogate: o-Terphenyl 14.0 ug/L 20.00 70 40-140 Surrogate: 2-F/uorobipheny/ 35.0 u91L 40.00 87 40-140 Surrogate: 2-Bromonaphthalene 38.9 ug/L 40.00 97 40-140 Sample Extraction Data Prep Method: MADEP EPH (VV) Lab Number Batch Initial Final DatwTlme 7070398-01 P7G0415 1000 mL 2 mL 07/26/17 12:30 Prep Method: 361 OC Me Lab Number Batch Initial Final Daternme 7070398-01 P7GO369 1000 mL 1 mL 07/26/17 1030 7070398-01 P7GO369 1000 mL 1 mL 07/25/17 10:30 This report should not be reproduced, except in its entirety, without the written consent of Pdsm Laborstodes, Inc. 449 Springbrook Read - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Tall Free Number. 1.8001529-6364 - Fax: 7041525-0409 Page 12 of 13 c 12 WE j❑ 0 9❑ s � e a � m m m m i IN v r CL �D Dim m SS m r-� 02 •p Gq �I .. o o e e ��' � � Z p $ a o m o i OZp o 3$ nC� np ih., aeQ i 9m m O D p cNi w m m 5 DOC 22 ON r z a nD W 8 or A ..� Z m� V c q '•�' zoe,,, •c r z, o» � m uma o�A m � Z C O N m aim oa m m CZ m o. m m n w n0 sa sm of psm coo, z m m'bmwm p m m �a m Y a� m�DOa 5 .. Dm g CCg pma�?4+06 m <5: m A �.n�yy mD $ np 1 amp Oz'm D p ❑ OZm g a. mm w oPna o ° m fA7 a M. pam 5 v^yms'�dd�`aem Am'm � 7D n0 _ o f d V) r C 300 _ nm yy m pA m 3 O W m co n m i S m S 6 O r O C a m Z O N Z CL n a m a I00m 3 44y 'I=m0 `w mlfp IAi ti za 'I e z I °�$ I � 1 1 IT I m n i O i f.Y m 2z m t' W om p 4 s '. g a Y ON � ID E PRISM 1A90NAT0elE5, INC Geoscience Group Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 NC Certification No. 402 Full -Service Analytical $ NC Drinking Water Cart No. 37735 Environmental Solutions SC Certification No. 99012 Project: Truck Part Service Lab Submittal Date: 02/13/2018 Prism Work Order: 8020233 Case Narrative 02/27/2018 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. a,..-1 Angela D. Overcash VP Laboratory Services 1Et - J Reviewed By Terri W. Cole For Angela D. Overcash Project Manager This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P,O- Box 240643 - Charlotte, NC 28224-0543 Phone: 704/52M364 -Toll Free Number: f-800/629-6364 - Fax: 704/62"409 Pnni a 1 of Data Qualifiers Key Reference A CCV result below range. Analyte not detected in sample. As Internal standard is below range. All associated analytes flagged as IN. CCV CCV result is above the control limits. Analyte not detected in the sample. No further action taken. DM Sample diluted and RL increased due to the matrix. DO Surrogates diluted out. IN Low Internal Standard response. Compound not detected. No further action taken. J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag). M Matrix spike outside of the control limits. RLM Sample container suspected to have low methanol content. Results possibly biased high. SR Surrogate recovery outside the QC limits. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Pnsm Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 704/629-6364 - Toll Free Number: 1-8001629-6364 - Fax: 704/626-0409 Paqe 2 of 52 P R I S R� I Full -Service Analytical 8 w� Environmental Solutions 4e.a,. — Sample Receipt Summary 02/27/2018 Prism Work Order: 8020233 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received S1 8020233-01 Solid 02/12/18 02/13/18 S2 8020233-02 Solid 02/13/18 02/13/18 S3 8020233-03 Solid 02/13/18 02/13/18 S4 8020233-04 Solid 02/13/18 02/13/18 S5 8020233-05 Solid 02/13/18 02/13/18 Samples were received in good condition at 5.4 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364- Toll Free Number: 1-800/529-6364 - Fax: 704/625-0409 Pace 527-1 x ; ISM �� a FWI-Service Analytical& (( Environmental Solutions �uwnmoniee,xc Summary of Detections 02/27/2018 Prism Work Order: 8020233 Prism ID Client ID Parameter Method Result Units 8020233-01 St C9-C18 Aliphatics MADEP EPH 2200 mg/kg dry 8020233-01 S1 C19-C36 Aliphatics MADEP EPH 23 1 -A/kg dry 8020233-01 S1 C11-C22 Aromatics MADEP EPH 410 mg/kg dry 8020233-01 S1 1-Methylnaphthalene 8270D 20 mg/kg dry 8020233-01 S1 2-Methylnaphthalene 8270D 31 mg/kg dry 8020233-01 S1 Fluorene 8270D 0.87 mg/kg dry 8020233-01 S1 Naphthalene 8270D 15 mg/kg dry 8020233-01 S1 Phenanthrene 8270D 0,27 1 mg/kg dry 8020233-01 S1 1,2,4-Trimethylbenzene 8260E 11 mg/kg dry 8020233-01 S1 1,3,5-Trimethylbenzene 8260B 4.3 mg/kg dry 8020233-01 S1 4-isopropyltoluene 8260E 1.3 mg/kg dry 8020233-01 S1 Ethylbenzene 8260E 1.5 mg/kg dry 8020233-01 S1 Isopropylbenzene (Cumene) 8260E 0.80 mg/kg dry 8020233-01 S1 m,p-Xylenes 8260E 1.0 mg/kg dry 8020233-01 S1 Naphthalene 8260E 9.7 mg/kg dry 8020233-01 S1 n-Butylbenzene 8260E 1.8 mg/kg dry 8020233-01 S1 n-Propylbenzene 8260B 1.6 mg/kg dry 8020233-01 S1 sec-Butylbenzene 8260E 1.1 mg/kg dry 8020233-01 S1 tert-Butylbenzene 8260B 0,16 1 mg/kg dry 8020233-01 S1 Xylenes, total 8260E 1.0 1 mg/kg dry 8020233-01 S1 C5-C8 Aliphatics MADEP VPH 88 mg/kg dry 8020233-01 S1 C9-C12 Aliphatics MADEP VPH 1100 mg/kg dry 8020233-01 s1 C9-C10 Aromatics MADEP VPH 590 mg/kg dry 8020233-02 S2 C9-C18 Aliphatics MADEP EPH 0.87 1 mg/kg dry 8020233-02 S2 Acetone 8260E 0.079 mg/kg dry 8020233-02 S2 Bromomethane 8260B 0.0058 1 mg/kg dry 8020233-03 S3 C9-C18 Aliphatics MADEP EPH 5.2 d mg/kg dry 8020233-03 S3 C9-C12 Aliphatics MADEP VPH 3.6 1 mg/kg dry 8020233-03 S3 C9-C10 Aromatics MADEP VPH 0.62 1 mg/kg dry 8020233-04 S4 C9-C 18 Aliphatics MADEP EPH 1.2 1 mg/kg dry 8020233-04 S4 Benzoic Acid 8270D 0.62 mg/kg dry 8020233-04 S4 Acetone 8260E 0.067 1 mg/kg dry 8020233-04 S4 Bromomethane 8260E 0.0052 1 mg/kg dry 8020233-05 S5 C9-C18 Aliphatics MADEP EPH 6.8 1 mg/kg dry 8020233-05 S5 1,2,4-Trimethylbenzene 8260E 0.027 mg/kg dry 8020233-05 S5 1,3,5-Trimethylbenzene 8260B 0.0035 ,I mg/kg dry 8020233-05 S5 4-Isopropyltoluene 8260E 0.0037 1 mg/kg dry 8020233-05 S5 Naphthalene 8260B 0.033 mg/kg dry 8020233-05 S5 n-Butylbenzene 8260B 0.0031 J mg/kg dry 8020233-05 S5 sec-Butylbenzene 8260B 0.0034 J mg/kg dry 8020233-05 S5 C5-C8 Aliphatics MADEP VPH 11 mg/kg dry 8020233-05 S5 C9-C12 Aliphatics MADEP VPH 220 mg/kg dry 8020233-05 S5 CS-Cl 0 Aromatics MADEP VPH 120 mg/kg dry This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 -Charlotte, NC 28224-0543 Phone: 704/529.6364-Toll Free Number: 1-8001629-6364 - Fax: 7041626-0409 Page 4of 2— �rF.l I IS M I Full- entel Service Analytical & T EnvlronmSolutions LMOMNPIFA MG Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Sample Matrix: Solid Laboratory Report 02/27/2018 Client Sample ID: S1 Prism Sample ID: 8020233-01 Prism Work Order: 8020233 Time Collected: 02/12/18 11:21 Time Submitted: 02/13/18 15:18 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Daterrime ID Extractable Petroleum Hydrocarbons by GC/FID CS -CIS Aliphatics 2200 mg/kg dry 170 1.1 5 MADEP EPH 2116118 9:17 ZRC PBB0289 CIS-C36 Alipha0cs 23 J mg/kg dry 34 4.1 1 MADEP EPH 2116/18 2:14 ZRC PSB0289 C11-C22 Aromatics 410 mg/kg dry 14 2.6 1 MADEP EPH 2/16/18 2:14 ZRC P880289 Surrogate Recovery Control Limns 1-Chlorooctadecane 65 % 40-140 o-Terphenyl 67 % 40-140 2-Fluorobiphenyl 108 % 40-140 2-Bromonaphthalene 86 % 40-140 General Chemistry Parameters % Solids 72.6 % by 0.100 0.100 1 SM2640 G 2114118 16:00 BJC PBE0281 �1 ltiall r Weight Semivolatile Organic Compounds by GC/MS 1 RL 1,2,4-Tnchlorobenzene BRL IN mg/kg dry 0.45 0.071 1 8270D 2119/18 16:46 JMV Pe130345 1,2-Dichlorobenzene BRL mg/kg dry 0.45 0.069 1 8270D 2/19/18 16:46 JMV P8130345 1,3-Dichlorobenzene BRL mg/kg dry 0.45 0.064 1 B270D 2/19118 16:46 JMV PBB0345 1,4-Dichlorobenzene BRL mg/kg dry 0.45 0.067 1 8270D 2/19/18 16:46 JMV P8130345 1-Methylnaphthalene 20 mg/kg dry 4.6 0.88 10 8270D 2120118 10:16 JMV P880346 2,4,6-Trichlorophenol BRL mg/kg dry 0.45 0.085 1 8270D 2/19118 16:46 JMV P880345 2,4-Dichlorophenol BRL IN mg/kg dry 0.45 0.088 1 8270D 2/19/18 16:46 JMV PSE0345 2,4-Dimethylphenol BRL IN mg/kg dry 0.45 0.070 1 8270D 2/19/18 16:46 JMV PBB0345 2,4-Dinitrophenol BRLCCV mg/kg dry 045 0.064 1 8270D 2/19/18 16:46 JMV P8B0345 2,4-Dinitrotoluene BRLA mg/kg dry 0.45 0.055 1 8270D 2/19118 16:46 JMV P8130345 2,6-Dinitrotoluene BRL mg/kg dry 0.45 0.061 1 8270D 2/19/18 16:46 JMV PBB0345 2-Chloronaphlhalene BRL mg/kg dry 0.45 0.066 1 8270D 2/19/18 16:46 JMV P8B0345 2-Chlorophenol BRL mg/kg dry 0.45 0,065 1 8270D 2/19/18 16:46 JMV PBB0345 2-Methylnaphthalene 31 mg/kg dry 4.5 0.73 10 8270D 2120118 10:16 JMV P880346 2-Methylphenol BRL mg/kg dry OA5 0.058 1 8270D 2/19/18 16:46 JMV P8130345 2-Nitrophenol BRL IN mg/kg dry 0.45 0.083 1 8270D 2119/18 16:46 JMV P880345 3,3'-Dichlorobenzidine BRL mg/kg dry 0.45 0.090 1 6270D 2/19/18 16:46 JMV PBB0345 3/4-Methylphenol BRL mg/kg dry 0.45 0.056 1 8270D 2/19118 16:46 JMV P8130345 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.45 0.068 1 8270D 2r19/18 16:46 JMV P8B0345 4-Bromophenyl phenyl ether BRL mg/kg dry 0.45 0.078 1 8270D 2119118 16:46 JMV PBB0345 4-Chloro-3-methylphenol BRL IN mg/kg dry 0,45 0.064 1 8270D 2/19/18 16:46 JMV P880345 4-Chloroaniline BRL IN mg/kg dry 0.45 0.055 1 8270D 2/19/18 16:46 JMV PBB0345 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.45 0.059 1 8270D 2/19/18 16:46 JMV P880345 4-Nitrophenol BRL mg/kg dry 0.45 0.070 1 8270D 2/19/18 16:46 JMV PBB0345 Acenaphthene BRL mg/kg dry 0.45 0.062 1 8270D 2/19/18 16:46 JMV P8130345 Acenaphthylene BRL mg/kg dry OA5 0,066 1 8270D 2/19/18 16:46 JMV P8130345 Anthracene BRL mg/kg dry 0,45 0.073 1 8270D 2/19/18 16:46 JMV P8B0345 Azobenzene BRL mg/kg dry 0.45 0.060 1 8270D 2119/18 16:46 JMV P8130345 Benzo(a)anthracene BRL mg/kg dry 0.45 0.060 1 8270D 2/19/18 16:46 JMV POB0345 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-OW Phone: 704/529-6364-Toll Free Number: l-8001529-6364- Fax: 704/526-0409 Page 5of52 R I S M I Full -Service Analytical a .._ ueonw Environmental Solutions Laboratory Report 02127/201a Geoscience Group Project: Truck Part Service Client Sample ID: S1 Attn: Tom Hassett Prism Sample ID: 8020233-01 500-K Clanton Rd. Prism Work Order: 8020233 Charlotte, INC 28217 Sample Matrix: Solid Time Collected: 02/12/18 11:21 Time Submitted: 02/13/18 15:18 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(a)pyrene BRL mg/kg dry 0.45 0.049 1 8270D 2/19/18 16:46 JMV PBB0345 Benzo(b)Fluorenthene BRL mg/kg dry 0.45 0,053 1 8270D 2/19/18 16:46 JMV P880345 Benzo(g,h,i)perylene BRL mg/kg dry 0.45 0.050 1 8270D 2119/18 16:46 JMV PBB0345 Benzo(k)Fluoranthene BRL mg/kg dry 0.45 0.060 1 8270D 2119/18 16:46 JMV PBB0345 Benzoic Acid BRUIN mg/kg dry 0.45 0.038 1 8270D 2/19/18 16:46 JMV PBS0345 Benzyl alcohol BRL mg/kg dry 0,45 0.060 1 8270D 2/19/18 16:46 JMV P8130345 bis(2-Chloroethoxy)methane BRL IN mg/kg dry 0.45 0.079 1 8270D 2/19118 16:46 JMV P880345 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.45 0.064 1 8270D 2/19/18 16:46 JMV PBB0345 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.46 0.078 1 8270D 2/19/18 1646 JMV P8130345 Bis(2-Ethylhexyl)phthalate - BRL mg/kg dry 0.45 0,068 1 8270D 2/19/18 16:46 JMV PBB0345 Butyl benzyl phthalate BRL mg/kg dry 0.45 0.065 1 8270D 2/19/18 16:46 JMV P880345 Chrysene BRL mg/kg dry 0.45 0.057 1 8270D 2/19/18 16:46 JMV P8130345 Dibenzo(a,h)anthracene BRL mg/kg dry 0.45 0.055 1 8270D 2/19118 16:46 JMV PBB0345 Dibenzofumn BRL mg/kg dry 0.45 0.069 1 8270D 2/19/18 16:46 JMV PBB0345 Diethyl phthalate BRL mg/kg dry 0.45 0.063 1 8270D 2/19118 16:46 JMV PBB0345 Dimethyl phthalate BRL mg/kg dry 0.45 0.060 1 8270D 2119/18 16:46 JMV P880345 Di-n-butyl phthalate BRL mg/kg dry 0.45 0,065 1 8270D 2119/18 16:46 JMV PBB0345 Di-n-octyl phthalate BRL mg/kg dry 0.45 0.056 1 8270D 2/19/18 16:46 JMV P8B0345 Fluoranthene BRL mg/kg dry 0.45 0.058 1 8270D 2/19/18 16:46 JMV P8130345 Fluorene 0.87 mg/kg dry 0.45 0.066 1 8270D 2119/18 16:46 JMV P8190345 Hexachlorobenzene BRL mg/kg dry 0.45 0.072 1 8270D 2/19/18 16:46 JMV P8130345 Hexachlorobutadiene BRL IN mg/kg dry 0.45 0.082 1 8270D 2/19118 16:46 JMV P6B0345 Hexachlorocyclopentediene BRL mg/kg dry 0.45 0.081 1 8270D 2/19/18 16:46 JMV PfIB0345 Hexachloroethane BRL mg/kg dry 0.45 0.076 1 8270D 2/19/18 16:46 JMV P8130345 Indeno(1,2,3-od)pyrene BRL mg/kg dry 0.45 0.052 1 8270D 2/19/18 16:46 JMV PBB0345 Isophorone BRUIN mg/kg dry 0.45 0.062 1 8270D 2/19/18 16:46 JMV P8B0345 Naphthalene 16 mg/kg dry 4.5 0.73 10 8270D 2120118 10:16 JMV PBB0346 Nitrobenzene BRUIN mg/kg dry 0.45 0.065 1 8270D 2/19/18 16:46 JMV P8B0345 N-Nitroso-di-n-propylamine BRL mg/kg dry 0.45 0.072 1 8270D 2/19/18 16:46 JMV PBB0345 N-Nitrosodiphenylamine BRL mg/kg dry 0.45 0.069 1 6270D 2/19/18 16:46 JMV P8B0345 Pentachlorophenol BRL mg/kg dry 0.45 0.054 1 8270D 2/19118 16:46 JMV PBB0345 Phenanthrene 0.27 J mg/kg dry 0.46 0.069 1 82700 2/19118 16:46 JMV P8130346 Phenol BRL mg/kg dry 0.45 0.067 1 8270D 2/19118 16:46 JMV PBB0345 Pyrene BRL mg/kg dry 0.45 0.060 1 8270D 2/19/18 16:46 JMV P8130345 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 106 % 39-132 2-Fluorobiphenyl 86 % 44-115 2-Fluorophenol 78 % 35-115 Nitrobenzene-d5 46 % 37-122 Phenol-d5 76 % 34-121 Terphenyl-d14 83 % 54-127 Volatile Organic Compounds by GC/MS (Medium Level) DM 1,1,1,2-Tetrachloroethane BRL mg/kg dry 0,36 0.091 50 8260B 2/22118 6:08 ANG P8130410 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Chadotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/629-6364- Fax: 704/625.0409 Page 6of52 1 eRISM I Laboratory Report Z Full -Service Analylical8 Envtronmentel Solutions 02/27/2018 `4"ueommnrecinc Geoscience Group Project: Truck Part Service Client Sample ID: S1 Attn: Tom Hassett Prism Sample ID: 8020233-01 500-K Clanton Rd. Prism Work Order: 8020233 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 02/12/18 11:21 Time Submitted: 02/13/18 15:18 Parameter Result Units Report MDL DIIutKn Method Analysis Analyst Batch Limit Factor Date/rime ID 1, 1, 1-Trichloroethane BRL mg/kg dry 0.36 0,083 50 8260B 2/22118 6:08 ANG PBB0410 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.36 0.069 50 8260B 2/22/18 6:08 ANG P880410 1, 1,2-Trichloroethane BRL mg/kg dry 0.36 0.087 50 8260B 2/22118 6:08 ANG P880410 1,1-Dichloroethane BRL mg/kg dry 0.36 0.094 50 0260B 2/22/18 6:08 ANG PSB0410 1,1-Dichloroethylene BRL mg/kg dry 0.36 0.10 50 8260B 2/22/18 6:08 ANG P8B0410 1,1-Dichloropropylene BRL mg/kg dry 0.36 0,081 50 8260B 2/22118 6:08 ANG PBB0410 1,2,3-Trichlorobenzene BRL mg/kg dry 0.71 0.084 50 8260B 2/22/18 6:08 ANG 1`8130410 1,2,3-Trichlompropane BRL mg/kg dry 0.36 0.13 50 8260B 2/22/18 6:08 ANG PBBD410 1,2,4-Trichlorobenzene BRL mg/kg dry 0.71 0,078 50 8260B 2/22/18 6:08 ANG P8B0410 1,2A.Trimethylbenzene 11 mg/kg dry 0.36 0.079 50 8260B 2122118 6:08 ANG P8B0410 1,2-Dibromoethane BRL mg/kg dry 0.36 0.080 50 82608 2/22118 6:08 ANG PBBD410 1,2-Dichlorobenzene BRL mg/kg dry 0,36 0.079 50 8260B 2/22/18 6:08 ANG P8B0410 1,2-Dichloroethane BRL mg/kg dry 0.36 0.077 50 6260B 2/22/18 6,08 ANG P8130410 1,2-Dichloropropane BRL mg/kg dry 0,36 0.071 50 8260B 2/22/18 6:08 ANG P8B0410 1,3,6-Trimethylbenzene 4.3 mg/kg dry 0.36 0.088 50 8260B 2/22118 6:08 ANG P8B0410 1,3-Dichlorobenzene BRL mg/kg dry 0.36 0.070 50 8260B 2/22/18 6:08 ANG P8130410 1,3-Dichloropropane BRL mg/kg dry 0.36 0.086 50 8260B 2122116 6:08 ANG P8130410 1,4-Dichlorobenzene BRL mg/kg dry 0.36 0.094 50 8260B 2/22/18 6:08 ANG P8130410 2,2-Dichloropropane BRL mg/kg dry 0,36 0.081 50 8260B 2/22/18 6:08 ANG P8B0410 2-Chlorotoluene BRL mg/kg dry 0.36 0.09B 50 8260B 2/22118 6:08 ANG PBB0410 4-Chlorotoluene BRL mg/kg dry 0.36 0.083 50 8260B 2/22118 6:08 ANG P8B0410 44sopropyltoluene 1.3 mg/kg dry 0.36 0.090 60 8260B 2/22/18 6:08 ANG P8130410 Acetone BRL mg/kg dry 14 0.27 50 8260B 2/22/18 6:08 ANG P8130410 Benzene BRL mg/kg dry 0.36 0.080 50 8260B 2/22/1B 6:08 ANG PBB0410 Bromobenzene BRL mg/kg dry 0.36 0,084 50 8260B 2/22/18 6:08 ANG PBB0410 Bromochloromethane BRL mg/kg dry 0.36 0,094 50 8260B 2122/18 6:08 ANG P8B0410 Bromodichloromethane BRL mg/kg dry 0.36 0.081 50 8260B 2/22/18 6:08 ANG PBB0410 Bromoform BRL mg/kg dry 0.36 0,097 50 8260B 2/22/18 6:08 ANG P8B0410 Bromomethane BRL mg/kg dry 0.71 0.093 50 8260B 2/22/18 6:08 ANG P880410 Carbon Tetrachloride BRL mg/kg dry 0.36 0.086 50 8260B 2/22/18 6:08 ANG P8B0410 Chlorobenzene BRL mg/kg dry 0.36 0.072 50 8260B 2/22/18 6:08 ANG P8150410 Chloroethane BRL mg/kg dry 0.71 0.074 50 82608 2/22/18 6:08 ANG P8130410 Chloroform BRL mg/kg dry 0.36 0.083 50 8260B 2/22/18 6:08 ANG P8B0410 Chloromethane BRL mg/kg dry 0.71 0.080 50 8260B 2/22/18 6:08 ANG P880410 cis-1,2-Dichloroethylene BRL mg/kg dry 0.36 0.075 50 8260B 2122/18 6:08 ANG PBB0410 cis-1,3-Dichloropropylene BRL mg/kg dry 0.36 0,079 50 8260B 2/22/18 6:08 ANG P8130410 Dibromochloromethane BRL mg/kg dry 0,36 0.076 50 8260B 2122/18 6:08 ANG PBB0410 Dichlorodi0uoromethane BRL mg/kg dry 0.71 0.092 50 8260B 2/22/18 698 ANG P8B0410 Ethylbenzene 1.5 mg/kg dry 0.36 0.081 60 8260B 2/22118 6:08 ANG PSB0410 Isopropyl Ether BRL mg/kg dry 0.36 0.075 50 8260B 2/22/18 6:08 ANG P8B0410 Isopropylbenzene (Cumene) 0.80 mg/kg dry 0.36 0.083 50 8260B 2122118 6:08 ANG P8110410 m,p-Xylenes 1.0 mg/kg dry 0.71 0.17 60 8260B 2/22/18 6:08 ANG P880410 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 1A 0,081 50 8260B 2/22/18 6:08 ANG P8130410 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 704/629-6364 - Toll Free Number: l-800/629.6364- Fax: 7041626-0409 Paoe7of52 �. ' S M I full -Service Analytical a Evironmentat solutions tABOPI.IOFIEA ING Laboratory Report 02/27/2018 Geoscience Group Project: Truck Part Service Client Sample ID: S1 Attn: Tom Hassett Prism Sample ID: 8020233-01 500-K Clanton Rd. Prism Work Order: 8020233 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 02/12/18 11:21 Time Submitted: 02/13118 15:16 Parameter Result Units Report MDL Dilution - Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 1.4 oo59 50 8260B 2/22/18 6:08 ANG P8B0410 Methyl lsobutyl Ketone BRL mg/kg dry 1.4 0.063 50 8260B 2/22/I8 6:08 ANG PBB0410 Methylene Chloride BRL mg/kg dry 0.36 0,077 50 8260B 2/22I8 6:08 ANG P8B0410 Methyl -ten -Butyl Ether BRL mg/kg dry 0.36 0.075 50 82606 2/22r1B 6:08 ANG P8B0410 Naphthalene 9.7 mg/kg dry 0.71 0.064 60 826013 2/22/18 6:08 ANG P8B0410 n-Butylbenzene 1.8 mg/kg dry 0.36 0.071 60 8260B 2122M8 6:08 ANG P8B0410 n-Propylbenzene 1.6 mg/kg dry 0.36 0.084 60 82608 2/22/t8 6:08 ANG P8B0410 o-Xylene BRL mg/kg dry 0,36 0.079 50 8260B 2/22/18 698 ANG P8B0410 sec-Butylbenzene 1.1 mg/kg dry 0.36 0.089 60 8260B 2122118 6:138 ANG P8B0410 Styrene BRL mg/kg dry 0.36 0.079 50 8260B 2122/18 6:08 ANG P8B0410 tert-Butylbenzene 0.16 J mg/kg dry 0.36 0.083 60 8260B 2122118 6:08 ANG P880410 Tetmchloroethylene BRL mg/kg dry 0.36 0.076 50 8260B 2(22118 6:08 ANG PBB0410 Toluene BRL mg/kg dry 0,36 0.076 50 8260B 2122118 6:08 ANG PBB0410 trans-1,2-Dichloroethylene BRL mg/kg dry 0.36 0.082 50 8260B WWI 6:08 ANG PBB0410 tmns-1,3-Dichloropropylene BRL mg/kg dry 0.36 0,076 50 8260B 2/22118 6:08 ANG P8B0410 Tnchloroethylene BRL mg/kg dry 0.36 0.077 50 82608 2122118 6:08 ANG P8B0410 Trichloro0uoromethane BRL mg/kg dry 0.71 0.10 50 8260B 2(22/18 6:08 ANG PBB0410 Vinyl acetate BRL mg/kg dry 1.4 , 0.059 50 8260B 2rOJ18 6:08 ANG P8B0410 Vinyl chloride BRL mg/kg dry 0.71 0o99 50 8260B 2/2P/IB 6:06 ANG P880410 Xylenes, total 1.0 J _ _ mg/kg dry 1.1 0.26 60 8260B 2/22H0 6:08 ANG P8B0410 Surrogate Recovery Control Limits 4-Bromofluorobenzene 96 % 70-130 Dibromo0uoromethane 97 % 70430 Toluene-d8 105 % 70-130 Volatile Petroleum Hydrocarbons by GC/PID/FID C6-C8 Aliphatics 88 mg/kg dry 66 1.8 1000 MADEP VPH 211M111 21:50 ANG/J PBB0270 C9-C12 Aliphatics 1100 mg/kg dry 66 2.9 1000 MADEP VPH 2/14118 21:60 ANG/J P8B0270 C9-010 Aromatics _ _ _ — _690 _ mg/kg dry 66 0.63 1000 MADEP VPH 2/14N8 21:60 ANG/J P880270 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 0 % 70-130 DO 2,5-Dibromotoluene (FID) 0 % 70-130 DO This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240W - Charlotte, NC 28224-0643 Phone: 704/629-6364-Toll Free Number: 1-800/629-6364- Fax: 704/626-0409 Page 8 of 52 /�� iISM Fu[I-ServlceMeMical a Laboratory Report i`wewemxreaixc Environmental Soleflons 02/27/2018 Geoscience Group Project: Truck Part Service Client Sample ID: S2 Attn: Tom Hassett Prism Sample ID: 8020233-02 500-K Clanton Rd. Prism Work Order: 8020233 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 02/13/18 09:31 Time Submitted: 02/13/18 15:18 Parameter Result Units Report MOIL Dilution Method Analysis Analyst Batch Limit Factor Date/rime ID Extractable Petroleum Hydrocarbons by GC/FID C9-C18 Aliphatics 0.87 J mg/kg dry 34 0.22 1 MADEP EPH 2116/18 2:61 ZRC P8190289 C19-C36 Aliphatics BRL mg/kg dry 34 4.0 1 MADEP EPH 2116/18 2:51 ZRC PBB0289 C11-C22 Aromatics BRL mg/kg dry 13 2.4 1 MADEP EPH 2/16/18 2:51 ZRC P8B0289 Surrogate Recovery Control Limits 1-Chlorooctadecane 85 % 40-140 o-Terphenyl 84 % 40-140 2-Fluorobiphenyl 90 % 40-140 2-Bromonaphthalene 90 % 40-140 General Chemistry Parameters % Solids 73.5 % by 0.100 0.100 1 SM2540 G 2/14118 16:00 BJC P880281 1w.4µ Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichoorobenzene BRL mg/kg dry 0.45 0.070 1 8270D 2/19118 17:08 JMV P880345 1,2-Dichlorobenzene BRL mg/kg dry 0.45 0,068 1 8270D 2/19118 17.08 JMV PBB0345 1,3-Dichlorobenzene BRL mg/kg dry 0,45 0.063 1 8270D 2/19118 17:08 JMV P880346 1,4-Dichlorobenzene BRL mg/kg dry 0.45 0,066 1 8270D 2/19/18 17:08 JMV PBB0345 1-Methylnaphthalene BRL mg/kg dry 0.45 0,086 1 8270D 2/19/18 17:08 JMV P880345 2,4,6-Trichiorophenol BRL mg/kg dry 0.45 0.084 1 8270D 2119/18 17:08 JMV PBB0345 2,4-Dichlorophenol BRL mg/kg dry 0.45 0.087 1 8270D 2/19/18 17:08 JMV PBB0345 2,4-Dimethylphenol BRL mg/kg dry 0.45 0.069 1 8270D 2119/18 17:08 JMV P880345 2,4-Dinitrophenol BRLCCV mg/kg dry 0.45 0,063 1 8270D 2/19/18 17:08 JMV P8130345 2,4-Dinitrotoluene BRLA mg/kg dry 0.45 0.054 1 8270D 2/19118 17:08 JMV P8B0345 2,6-Dinitrotoluene BRL mg/kg dry 0,45 0.060 1 8270D 2/19/18 17:08 JMV PBB0345 2-Chloronaphthalene BRL mg/kg dry 0.45 0.065 1 8270D 2/19/18 17:08 JMV P8B0345 2-Chlorophenol BRL mg/kg dry 0.45 0,063 1 8270D 2/19/18 17:08 JMV PBB0345 2-Methylnaphthalene BRL mg/kg dry 0.45 0.072 1 8270D 2/19118 17:08 JMV P8B0345 2-Methylphenol BRL mg/kg dry 0.45 0.057 1 8270D 2/19118 17:08 JMV PBB0345 2-Nitrophenol BRL mg/kg dry 0.45 0.082 1 8270D 2/19/18 17:08 JMV P8130345 3,3'-Dichlorobenzidine BRL mg/kg dry 0.45 0.088 1 8270D 2119/18 17:08 JMV P8130345 3/4-Methylphenol BRL mg/kg dry 0.45 0.055 1 8270D 2/19/18 17:08 JMV P8B0345 4,6-Dimtro-2-methylphenol BRL mg/kg dry 0.45 0.067 1 8270D 2/19/18 17:08 JMV P8130345 4-Bromophenyl phenyl ether BRL mg/kg dry 0.45 0.077 1 8270D 2/19/18 17:08 JMV P8B0345 4-Chloro-3-methylphenol BRL mg/kg dry 0,45 0.063 1 8270D 2/19/18 17:08 JMV P8130345 4-Chloroaniline BRL mg/kg dry 0.45 0.054 1 8270D 2/19118 17:08 JMV P8130345 4-Chlorophenyl phenyl ether BRL mg/kg dry 0A5 0.058 1 8270D 2/19/18 17:08 JMV P880345 4-Nilrophenol BRL mg/kg dry 0.45 0.069 1 8270D 2/19118 17:08 JMV P8B0345 Acenaphthene BRL mg/kg dry 0.45 0.061 1 82701) 2/19/18 17:08 JMV PBB0345 Acenaphthylene BRL mg/kg dry 0.45 0.065 1 8270D 2/19/18 17:08 JMV PSB0345 Anthracene BRL mg/kg dry 0.45 0.072 1 8270D 2/19/18 17:08 JMV PBB0345 Azobenzene BRL mg/kg dry 0.45 0.059 1 8270D 2/19/18 17:08 JMV PBB0345 Benzo(a)anthmcene BRL mg/kg dry 0.45 0.059 1 8270D 2/19/18 17:08 JMV PBB0345 Benzo(a)pyrene BRL mg/kg dry 0.45 0.048 1 8270D 2/19/18 17:08 JMV P8B0345 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 704/629-6364 - Toll FreeNumber: 1-8001529-6364- Fax: 704/525-0409 Page 9of52 ���1LLLv(w I S M Fuli-Service Analytical 8 1Environmental Laboratory Report ��; U90MlOPIEA RIe Solutlona 02/27/2018 Geoscience Group Project: Truck Part Service Client Sample ID: S2 Attn:Tom Hassett Prism Sample ID: 8020233-02 500-K Clanton Rd. Prism Work Order: 8020233 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 02/13/18 09:31 Time Submitted: 02/13/18 15:18 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Benzo(b)fluoranthene BRL mg/kg dry 0.45 0.052 1 8270D 2/19/18 17:08 JMV P8B0345 Benzo(g,hJ)perylene BRL mg/kg dry 0.45 0.049 1 8270D 2/19/18 17:08 JMV P8130345 Benzo(k)fuoranthene BRL mg/kg dry DA5 0.059 1 8270D 2/19118 17:08 JMV PBB0345 Benzoic Acid BRL mg/kg dry 0,45 0.038 1 8270D 2/19118 17:08 JMV PBB0345 Benzyl alcohol BRL mg/kg dry 0.45 0.059 1 8270D 2/19/18 17:08 JMV PBB0345 bis(2-Chloroethoxy)methane BRL mg/kg dry 0,45 0.078 1 8270D 2119/18 17:08 JMV P880345 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.45 0.063 1 8270D 2/19/18 17:08 JMV P880345 Bis(2-chloroisopmpyl)ether BRL mg/kg dry 0.45 0,077 1 8270D 2/1911B 17:08 JMV P8130345 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry 0.45 0.066 1 8270D 2119/18 17:08 JMV P8130345 Butyl benzyl phthalate BRL mg/kg dry 0A5 0.064 1 8270D 2/19/18 17:08 JMV P880345 Chrysene BRL mg/kg dry 0.45 0.056 1 8270D 2/19118 17:08 JMV P8130345 Dibenzo(a,h)anthracene BRL mg/kg dry 0.45 0.055 1 8270D 2/19/18 17:08 JMV P8130345 Dibenzofu m BRL mg/kg dry 0.45 0.068 1 8270D 2/19/18 17:08 JMV P880345 Diethyl phthalate BRL mg/kg dry 0.45 0,062 1 8270D 2/19/18 17:08 JMV PBB0345 Dimethyl phthalate BRL mg/kg dry 0.45 0.059 1 8270D 2/19/18 17:08 JMV PBB0345 Di-n-butyl phthalate BRL mg/kg dry 0.45 0.064 1 8270D 2/19/18 17:08 JMV P8B0345 Di-n-octyl phthalate BRL mg/kg dry 0.46 0,055 1 8270D 2/19/18 17:08 JMV PBB0345 Fluomnthene BRL mg/kg dry 0.45 0.057 1 8270D 2/19/18 17:08 JMV POB0345 Fluorene BRL mg/kg dry 0.45 0o64 1 8270D 2/19/18 17:08 JMV P8130345 Hexachlorobenzene BRL mg/kg dry 0.45 0.071 1 8270D 2/19/18 17:08 JMV PBB0345 Hexachlombmadiene BRL mg/kg dry 0.45 0.080 1 8270D 2/19/18 17:08 JMV P8130345 Hexachlonocyclopentadiene BRL mg/kg dry 0.45 0.080 1 8270D 2/19/18 17:08 JMV P8130345 Hexachlomethane BRL mg/kg dry 0.45 0,075 1 8270D 2119118 17:08 JMV P8B0345 Indeno(1,2,3cd)pyrene BRL mg/kg dry 0,45 0,051 1 8270D 2/19/18 17:08 JMV PBB0345 Isophorone BRL mg/kg dry 0.45 0.061 1 8270D 2/19/18 17:08 JMV P8130345 Naphthalene BRL mg/kg dry OAS 0.072 1 8270D 2/19118 17:08 JMV P8B0345 Nitrobenzene BRL mg/kg dry 0.45 0.064 1 8270D 2/19/18 17:08 JMV P8130345 N-Nitrosc-di-n-propylamine BRL mg/kg dry 0.45 0.071 1 8270D 2/19/18 17:08 JMV P8B0345 N-Nitmsodiphenylamine BRL mg/kg dry 0.45 0,068 1 8270D 2/19118 17:08 JMV P8B0345 Pentachlomphenol BRL mg/kg dry 0,45 0.053 1 8270D 2/19/18 17:06 JMV PBB0345 Phenanthrene BRL mg/kg dry 0.45 0.058 1 8270D 2119/18 17:08 JMV P880345 Phenol BRL mg/kg dry 0.45 0,066 1 8270D 2/19/18 17:08 JMV P8B0345 Pyrene BRL mg/kg dry 0.45 0.059 1 8270D 2/19/18 17:08 JMV PBB0345 Surrogate Recovery Control Limits 2,4,6-Tribmmophenol 78 % 39-132 2-Fluorobiphenyl 82 % 44-115 2-Fluorophenol 73 % 35-115 Nitrobenzene-d5 73 % 37-122 Phenol-d5 74 % 34-121 Terphenyl-d14 78 % 54-127 Volatile Organic Compounds by GC/MS 1, 1, 1,2-Tetmchlomethane BRL mg/kg dry 0.0057 0.00047 1 8260B 2/21/18 23:39 ANG PBB0397 1,1,1-Trichloroethane BRL mg/kg dry 0o057 0.00028 1 8260B 2/21/18 23:39 ANG P8130397 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, INC 28224-0643 Phone: 704/529-6364-Toll Free Number: 1-800/629-6364 - Fax: 7041626-0409 Page 10of52 ISM T"'ueoxnronias ixc Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Fun -Service Analytical $ Environmental Solution% Project: Truck Part Service Sample Matrix: Solid Laboratory Report 02/27/201 B Client Sample ID: S2 Prism Sample ID: 8020233-02 Prism Work Order: 8020233 Time Collected: 02/13/18 09:31 Time Submitted: 02/13/18 15:18 Parameter Result Units Report MDL Dilution Method Analysis Analyst Balch Limit Factor Date/Time ID 1,1,2,2-Tetrachlomethane BRL mg/kg dry 0.0057 0.00039 1 8260B 2/21118 23:39 ANG P8B0397 1, 1,2-Trichlomethane BRL mg/kg dry 0.0057 0.00051 1 8260B 2/21118 23:39 ANG 1`880397 1,1-Dichloroethane BRL mg/kg dry 0.0057 0.00016 1 8260B 2/21/18 23:39 ANG P8130397 1,1-Dichloroethylene BRL mg/kg dry 0.0057 0.00025 1 8260B 2/21/18 23:39 ANG P8130397 1,1-Dichloropropylene BRL mg/kg dry 0.0057 0.00031 1 82608 2121118 23:39 ANG P8190397 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0057 0.00033 1 8260B 2/21/18 23:39 ANG PBB0397 1,2,3-Trichloropropane BRL mg/kg dry 0.0057 0.00073 1 82608 2/21/18 2399 ANG P8130397 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0057 0.00043 1 8260B 2/21118 23:39 ANG P8B0397 1,2,4-Trimethylbenzene BRL mg/kg dry 0.0057 0.00044 1 8260B 2/21/18 23:39 ANG P8B0397 1,2-Dibromoethane BRL mg/kg dry 0.0057 0.00023 1 8260B 2/21/18 23:39 ANG P8B0397 1,2-Dichlorobenzene BRL mg/kg dry 0.0057 0.00027 1 8260B 2/21/18 23:39 ANG PBB0397 1,2-Dichloroethane BRL mg/kg dry O.OD57 0.00034 1 0260B 2/21/18 23:39 ANG PBB0397 1,2-Dichloropropane BRL mg/kg dry DD057 0.00036 1 8260B 2/21/18 2399 ANG P8130397 13,5-Tdmethylbenzene BRL mg/kg dry 0.0057 0,00043 1 8260B 2/21/18 23:39 ANG PBB0397 1,3-Dichlorobenzene BRL mg/kg dry 0.0057 0.00038 1 8260B 2/21118 23.39 ANG P880397 1,3-Dichloropropane BRL mg/kg dry 0.0057 0.00029 1 8260B 2/21/18 23:39 ANG P8B0397 1,4-Dichlorobenzene BRL mg/kg dry 0.0057 0.00023 1 8260B 2121118 23:39 ANG P8B0397 2,2-Dichloropropane BRL mg/kg dry 0.0057 0.00027 1 8260B 2/21/18 23:39 ANG PBB0397 2-Chlorololuene BRL mg/kg dry 0.0057 0.00030 1 8260B 2121118 23:39 ANG P8B0397 4-Chlorotoluene BRL mg/kg dry 0.0057 0.00034 1 8260B 2121/18 23:39 ANG PBB0397 4-Isopropyltoluene BRL mg/kg dry 0.0057 0.00028 1 8260B 2/21/18 23:39 ANG P880397 Acetone 0.079 mg/kg dry 0.057 0.0014 1 8260B 2121118 23:39 ANG P8130397 Benzene BRL mg/kg dry 0.0034 0.00033 1 8260B 2/21/18 23:39 ANG PBB0397 Bromobenzene BRL mg/kg dry 0.0057 0.00048 1 8260B 2/21/18 23:39 ANG P880397 Bromochloromethane BRL mg/kg dry 0.0057 0.00032 1 8260B 2/21/18 23:39 ANG P8130397 Bromodichloromethane BRL mg/kg dry 0.0057 0,00032 1 8260B 2/21/18 23:39 ANG PBB0397 Bromoform BRL mg/kg dry 0.0057 0.00065 1 8260B 2/21/18 23:39 ANG PBB0397 Bromomethane 0.0068 J mg/kg dry 0.011 0.00071 1 8260B 2121118 23:39 ANG P880397 Carbon Tetrachloride BRL mg/kg dry 0.0057 0.00029 1 8260B 2/21/18 23:39 ANG P8B0397 Chlorobenzene BRL mg/kg dry 0.0057 0.00030 1 8260B 2/21/18 23:39 ANG PBB0397 Chloroethane BRL mg/kg dry 0.011 0.00048 1 8260B 2/21118 23:39 ANG P880397 Chloroform BRL mg/kg dry 0.0057 0.00041 1 82606 2/21/18 23:39 ANG P860397 Chloromethane BRL mg/kg dry 0.0057 0,00039 1 8260B 2/21118 23:39 ANG P880397 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0057 0.00024 1 8260B 2/21/18 23:39 ANG P8130397 cis-1,3-Dichloropropylene BRL mg/kg dry 0,0057 0.00019 1 8260B 2/21/18 23:39 ANG P880397 Dibromochloromethene BRL mg/kg dry 0.0057 0.00024 1 82603 2/21/18 23:39 ANG PBB0397 Dichlorodifluoromethane BRL mg/kg dry 0.0057 0.00026 1 8260B 2/21/18 23:39 ANG P8B0397 Ethylbenzene BRL mg/kg dry 0.0057 0.00022 1 8260B 2/21/18 23:39 ANG PBB0397 Isopropyl Ether BRL mg/kg dry 0.0057 0.00023 1 8260B 221/18 23:39 ANG P8130397 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0057 0.00034 1 8260B 2/21/18 23:39 ANG PBB0397 m,p-Xylenes BRL mg/kg dry 0.011 0.00053 1 8260B 2/21118 23:39 ANG P8130397 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.057 0.00052 1 8260B 2/21118 23:39 ANG PBB0397 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0A 1 0.00052 1 8260B 2/21118 23:39 ANG P880397 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364-Fax: 7041625-0409 Page 11 of 2 Full -Service AnalNical fl ARISMLaboratory Environmental soletioas Report m'vso.a, roc 02/27/2018 Geoscience Group Project: Truck Part Service Client Sample ID: S2 Attn: Tom Hassett Prism Sample ID: 8020233-02 500-K Clanton Rd. Prism Work Order: 8020233 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 02/13/18 09:31 Time Submitted: D2/13/18 15:18 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Isobutyl Ketone BRL mg/kg dry 0,057 0.00049 1 8260B 2/21/18 23:39 ANG P8130397 Methylene Chloride BRL mg/kg dry 0.011 0.00032 1 8260B 2/21/18 23:39 ANG P860397 Methyl-tert-Butyl Ether BRL mg/kg dry 0.011 0,00018 1 8260B 2121118 2339 ANG PBB0397 Naphthalene BRL mg/Kg dry 0.011 0.00018 1 8260B 2/21/18 2339 ANG P8B0397 n-Butylbenzene BRL -9/kg dry 0.0057 0.00029 1 8260B 2/21/18 23:39 ANG P890397 n-Propylbenzene BRL mg/kg dry 0.0057 0.00034 1 8260B 2/21/18 23:39 ANG P880397 c-Xylene BRL mg/kg dry 0.0057 0,00024 1 8260B 2/21118 23:39 ANG PBB0397 sec-Butylbenzene BRL mg/kg dry 0.0057 0.00028 1 8260B 2/21/18 23:39 ANG P8B0397 Styrene BRL mg/kg dry 0.0057 0,00035 1 8260B 2/21118 23:39 ANG P8130397 tert-Butylbenzene BRL mg/kg dry 0.0057 0.00019 1 8260B 2/21118 23:39 ANG P8B0397 Tetrachlomethylene BRL mg/kg dry 00057 0,00027 1 8260B 2121/182339 ANG P8B0397 Toluene BRL mg/kg dry 00057 0.00033 1 8260B 2/21/18 23:39 ANG PBB0397 trans-12-Dichlomelhylene BRL mg/kg dry 0,0057 0.00034 1 8260B 2121/16 23:39 ANG PBB0397 trans-1,3-Dichloropmpylene BRL mg/kg dry 0.0057 0.00030 1 8260B 2/21/18 23:39 ANG P8B0397 Trichloroethylene BRL mg/kg dry 0,0057 0.00037 1 8260B 2121/18 23:39 ANG P8130397 Trichlorofluoromethane BRL mg/kg dry 0.0057 0.00037 1 8260B 2/21/18 23:39 ANG PBB0397 Vinyl acetate BRL mg/kg dry 0.029 0.00079 1 8260B 2/21118 23:39 ANG P880397 Vinyl chloride BRL mg/kg dry 0.0057 0.00028 1 8260B 2/21118 23:39 ANG P8130397 Xylenes, total BRL mg/kg dry 0.017 0.0011 1 8260B 2/21/18 23:39 AND PBB0397 - Surrogate Recovery Control Limits 4-13mmofluorobenzene 103 % 70-130 Dibromofluommelhane 103 % 84-123 Toluene-d8 102 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID RLM C6-C8 Aliphatics BRL mg/kg dry 6.0 0.19 100 MADEP VPH 2/14118 19:57 ANG/J PBB0270 C9-C12 Aliphatics BRL mg/kg dry 6.0 0.31 100 MADEP VPH 2/14/18 19:57 ANG/J PBB0270 C9-C10Aromatics BRL mg/kg dry 6.0 0,067 100 MADEP VPH 2114/18 19:57 ANG/J P8130270 Surrogate Recovery Control Limits 2,5-Dibromaloluene (PID) 129 % 70-130 2,5-Dibromotoluene (FID) 131 % 70130 SR This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 -Charlotte, INC 26224-0543 Phone: 70416296364- Toll Free Number: 1 -800/629-6364 - Fax: 704/626-0409 Page 120f52 PRISMI `till-5ervc.An8111W.1 a Laboratory Report Environmemal Solutions �woxmvxiEA ixc 02/27/201 B Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Sample Matrix: Solid Client Sample ID: S3 Prism Sample ID: 8020233-03 Prism Work Order: 8020233 Time Collected: 02/13/18 09:50 Time Submitted: 02113118 15:18 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-C18 Aliphadcs 6.2 J mania dry 32 0.21 1 MADEP EPH 2116118 3:27 ZRC PBB0289 C19-C36 Aliphatics BRL mg/kg dry 32 3.8 1 MADEP EPH 2/16/18 3:27 ZRC P880289 C11-C22 Aromatics _ _ BRL mg/kg dry 13 2.3 1 MADEP EPH 2/16/18 3:27 ZRC P8130289 Surrogate Recovery Control Limits 1-Chlorooctademne 84 % 40-140 o-Terphenyl 86 % 40-140 2-Fluorobiphenyl 93 % 40-140 2-Bromonaphthalene 86 % 40-140 General Chemistry Parameters % Solids 76.8 % by 0.100 0.100 1 SM2640 G 2/14118 16:00 BJC P8B0281 Weight Semivolatile Organic Compounds by GUMS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.43 0.067 1 8270D 2/19/18 17:30 JMV P8150345 1,2-Dichlorobenzene BRL mg/kg dry 0.43 0.065 1 8270D 2/19/18 17:30 JMV P8130345 1,3-Dichlorobenzene BRL mg/kg dry 0.43 0.061 1 8270D 2/19/18 17:30 JMV PBB0345 1,4-Dichlorobenzene BRL mg/kg dry 0.43 0.063 1 8270D 2/19/18 17:30 JMV P8130345 1-Methylnaphthalene BRL mg/kg dry 0.43 0,083 1 8270D 2/19/18 17:30 JMV P8130345 2,4,6-Trichlomphenol BRL mg/kg dry 0.43 0.081 1 8270D 2/19118 17:30 JMV PBB0345 2,4-Dichlomphenol BRL mg/kg dry O A3 0.083 1 8270D 2/19/18 17:30 JMV P8B0345 2,4-Dimethylphenol BRL mg/kg dry 0.43 0.066 1 8270D 2/19/10 17:30 JMV P8130345 2,4-Dinitrophenol BRL CCV mg/kg dry DA3 0.060 1 8270D 2M 9/18 17:30 JMV P880345 2,4-Dinitrotoluene BRLA mg/kg dry 0.43 0.052 1 8270D 2/19/18 17:30 JMV PBB0345 2,6-Dinitrotoluene BRL mg/kg dry 0,43 0.057 1 8270D 2/19/18 17:30 JMV PBB0345 2-Chloronaphthalene BRL mg/kg dry 0.43 0.062 1 8270D 2M9/18 17:30 JMV PBB0345 2-Chlorophenol BRL mg/kg dry 0.43 0.061 1 8270D 2/19118 17:30 JMV PBB0345 2-Methylnaphthalene BRL mg/kg dry 0.43 0.069 1 8270D 2/19/18 17:30 JMV P8130345 2-Methylphenol BRL mg/kg dry 0A3 0.055 1 8270D 2/19118 17:30 JMV P8B0345 2-Nitrophenol BRL mg/kg dry 0.43 0,078 1 8270D 2/19/18 17:30 JMV P8130345 3,3'-Dichlorobenzidine BRL mg/kg dry 0.43 0.085 1 8270D 2/19/18 1730 JMV P8B0345 3/4-Methylphenol BRL mg/kg dry 0.43 0.053 1 8270D 2/19/18 17:30 JMV P8B0345 4,6-Dinitm-2-methylphenol BRL mg/kg dry 0.43 0.065 1 8270D 2119118 17:30 JMV PBB0345 4-Bromophenyl phenyl ether BRL mg/kg dry 0.43 0.074 1 8270D 2119/18 17:30 JMV P8130345 4-Chlon-3-methylphenol BRL mg/kg dry 0.43 0.060 1 8270D 2/19/18 17:30 JMV P8130345 4-Chloroaniline BRL mg/kg dry 0.43 0.052 1 8270D 2/19/18 17:30 JMV PBB0345 4-Chlomphenyl phenyl ether BRL mg/kg dry 0.43 0.056 1 8270D 2/19/18 17:30 JMV P8B0345 4-Nitrophenol BRL mg/kg dry 0.43 0.066 1 8270D 2119118 1790 JMV P8130345 Acenaphthene BRL mg/kg dry 0.43 0.058 1 8270D 2/19/18 17:30 JMV P8B0345 Acenaphthylene BRL mg/kg dry 0,43 0.062 1 8270D 2/19118 17:30 JMV P8130345 Anthracene BRL mg/kg dry 0.43 0.069 1 8270D 2/19/18 17:30 JMV PBB0345 Azobenzene BRL mg/kg dry 0.43 0.057 1 827DD 2/19/18 17:30 JMV P8130345 Benzo(a)anthracene BRL mg/kg dry 0.43 0,056 1 8270D 2/19/18 17:30 JMV PSB0345 Benzo(a)pyrene BRL mg/kg dry 0A3 0.046 1 8270D 2/19118 17:30 JMV P8150345 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 704/629-6364- Toll Free Number: 1-8001629-6364 - Fax: 7041626-0409 r Page 13 of 52 /,GdPR I S M I Fvlbeerviceal solutions 3 Env rie mice A alytical & tABOP.ttOpIE& . Laboratory Report 02/27/2018 Geoscience Group Project: Truck Part Service Client Sample ID: S3 Attn: Tom Hassett Prism Sample ID: 8020233-03 500-K Clanton Rd. Prism Work Order: 8020233 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 02/13/18 09:50 Time Submitted: 02/13/18 15:18 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Daterrime ID Benzo(b)Fluoranthene BRL mg/kg dry 0.43 0.050 1 8270D 2/19/18 17:30 JMV PBB0345 Benzo(g,h,i)perylene BRL mg/kg dry 0.43 0.047 1 8270D 2/19/18 17:30 JMV P8130345 Benzo(k)Fluoranthene BRL mg/kg dry 0.43 0.056 1 8270D 2119/18 17:30 JMV P8130345 Benzoic Acid BRL mg/kg dry 0,43 0.036 1 8270D 2119/18 17:30 JMV P8130345 Benzyl alcohol BRL mg/kg dry 0,43 0.057 1 8270D 2/19/18 17:30 JMV P8130345 bis(2-Chloroethoxy)methane BRL mg/kg dry 0.43 0.075 1 8270D 2/19/18 17:30 JMV PBB0345 Bis(2-Chloroethyl)ether BRL mg/kg dry 0.43 0.061 1 8270D 2119/18 17:30 JMV P880345 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.43 0.073 1 8270D 2/19/18 17:30 JMV PBB0345 Bis(2-Ethylhexyl)phthelate BRL mg/kg dry 0.43 0.064 1 8270D 2/19/18 17:30 JMV P880345 Butyl benzyl phthalate BRL mg/kg dry 0.43 0.061 1 8270D 2/19/18 17:30 JMV PBB0345 Chrysene BRL mg/kg dry OA3 0,054 1 8270D 2/19/18 17:30 JMV P8130345 Dibenzo(a,h)anthmcene BRL mg/kg dry 0,43 0.052 1 8270D 2/19/18 1730 JMV P8130345 Dibenzofumn BRL mg/kg dry OA3 0.065 1 8270D 2/19118 17:30 JMV P8130345 Diethyl phthalate BRL mg/kg dry 0.43 0.059 1 8270D 2/19/18 17:30 JMV P8B0345 Dimethyl phthalate BRL mg/kg dry DA3 0.057 1 8270D 2/19118 17:30 JMV PBB0345 Di-n-butyl phthalate BRL mg/kg dry 0.43 0.061 1 8270D 2/19/18 17:30 JMV PBB0345 Di-n-octyl phthalate BRL mg/kg dry 0.43 0.053 1 8270D 2/19/18 17:30 JMV P8130345 Fluoranthene BRL mg/kg dry 0.43 0,055 1 8270D 2/19118 17:30 JMV P8130345 Fluorene BRL mg/kg dry 0.43 0.062 1 8270D 2/19/18 17:30 JMV PBB0345 Hexachlorobenzene BRL mg/kg dry 0.43 0,068 1 8270D 2/19/18 17:30 JMV P8130345 Hexachlorobutat iene BRL mgAg dry 0.43 0.077 1 8270D 2/19/18 17:30 JMV P8130345 Hexachlorocyclopentadiene BRL mg/kg dry 0.43 0.077 1 8270D 2/19118 17:30 JMV P8BO345 Hexachloroethane BRL mg/kg dry 0.43 0.072 1 8270D 2/19118 17:30 JMV P880345 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.43 0.049 1 8270D 2/19/18 17:30 JMV P8B0345 Isophorone BRL mg/kg dry 0.43 0.058 1 82700 2119/18 17:30 JMV P880345 Naphthalene BRL mg/kg dry 0.43 0.069 1 8270D 2/19118 17:30 JMV P880345 Nitrobenzene BRL mg/kg dry 0.43 0.061 1 8270D 2/19/18 17:30 JMV P8B0345 N-Nitroso-di-n-propylamme BRL mg/kg dry 0.43 0.068 1 8270D 2/19118 17:30 JMV P8130345 N-Nitrosodiphenylemine BRL mg/kg dry 0.43 0.065 1 8270D 2/19/18 17:30 JMV P880345 Pentachlorophenol BRL mg/kg dry 0,43 0,051 1 8270D 2/19/18 17:30 JMV P8130345 Phenanthrene BRL mg/kg dry 0.43 0,056 1 8270D 2/19118 17:30 JMV P8B0345 Phenol BRL mg/kg dry 0.43 0.063 1 8270D 2119118 17:30 JMV PSB0345 Pyrene BRL mg/kg dry 0.43 0.057 1 8270D 2/19118 17:30 JMV PBB0345 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 79 % 39-132 2-Fluorobiphenyl 73 % 44-115 2-Fluorophenol 63 % 35-115 Nitrobenzene-d5 60 % 37-122 Phenol-d5 65 % 34-121 Terphenyl-d14 78 % 54-127 Volatile Organic Compounds by GC/MS 1, 1, 1,2-Tetmchloroethane BRL mg/kg dry 0.0061 0.00050 1 8260B 2122/18 0:07 ANG P8B0397 1, 1,1-Trichloroethane BRL mg/kg dry 0.0061 0.00029 1 8260B 2/22/18 0:07 ANG P880397 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 704/62M364-Toll Free Number: 1-800/629-6364- Fax: 704/62"409 Page 14of52 LakRlSM I x"weoaaa„„a,„. Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 aull-SemiceAnalyncal& Environmemal 5o1a1i"ns Project: Truck Part Service Sample Matrix: Solid Laboratory Report 02/27/2018 Client Sample ID: S3 Prism Sample ID: 8020233-03 Prism Work Order: 8020233 Time Collected: 02/13/18 09:50 Time Submitted: 02/13/18 15:18 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0061 0.00041 1 8260B 2/22/18 0:07 ANG PBB0397 1, 1,2-Ticchooroethane BRL mg/kg dry 0.0061 0.00054 1 8260B 2122/18 0:07 ANG P8B0397 1,1-Dichloroethane BRL mg/kg dry 0.0061 0.00017 1 82608 2/22/18 0:07 ANG P8B0397 1,1-Dichloroethylene BRL mg/kg dry 0.0061 0.00027 1 8260B 2122/18 007 ANG P8B0397 1,1-Dichloropropylene BRL mg/kg dry 0.0061 0,00033 1 8260B 2/22118 0:07 ANG PBB0397 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0061 0.00034 1 8260B 2/22/18 0:07 ANG P8B0397 1,2,3-Trichloropropane BRL mg/kg dry 0.0061 0.00077 1 8260B 2/22/18 0:07 ANG P8B0397 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0061 0.00045 1 8260B 2/22/18 0:07 ANG P8130397 1,2,4-T(methylbenzene BRL mg/kg dry 0,0061 0,00046 1 8260B 2/22/18 0:07 ANG P8B0397 1,2-Dibromoethane BRL mg/kg dry 0.0061 0,00024 1 8260B 2/22/18 0:07 ANG P8B0397 1,2-Dichlorobenzene BRL mg/kg dry 0.0061 0.00028 1 8260B 2/22/18 0:07 ANG P8B0397 1,2-Dichloroethane BRL mg/kg dry 0.0061 0,00036 1 6260B 2122118 0:07 ANG P8B0397 1,2-Dichloropropane BRL mg/kg dry 0,0061 0.00038 1 8260B 2/22/18 0:07 ANG P8B0397 1,3,5-Trimethylbenzene BRL mg/kg dry 0.0061 0.00046 1 8260B 2/22/18 0:07 ANG P8B0397 1,3-Dichlorobenzene BRL mg/kg dry 0.0061 0,00040 1 8260B 2122118 0:07 ANG P8B0397 1,3-Dichloropropane BRL mg/kg dry 0,0061 0.00030 1 8280B 2/22/18 0:07 ANG PBB0397 1,4-Dichlorobenzene BRL mg/kg dry 0.0061 0.00024 1 8260B 2/22/18 0:07 ANG P8B0397 2,2-Dichloropropane BRL mg/kg dry 0,0061 0.00029 1 8260B 2/22118 0:07 ANG PBB0397 2-Chlorotoluene BRL mg/kg dry 0.0061 0.00031 1 8260B 2122/18 0:07 ANG PBB0397 4-Chlorotoluene BRL mg/kg dry 0.0061 0.00036 1 0260B 2/22/18 0:07 ANG P880397 44sopropyltoluene BRL mg/kg dry 0.0061 0.00029 1 8260B 2122/18 0:07 ANG PBB0397 Acetone BRL mg/kg dry 0.061 0,0015 1 82608 2/22/18 0:07 ANG P8B0397 Benzene BRL mg/kg dry 0.0036 0,00035 1 8260B 2/22/18 0:07 ANG POB0397 Bromobenzene BRL mg/kg dry 0.0061 0.00050 1 8260B 2/22/18 0:07 ANG P880397 Bromochloromethane BRL mg/kg dry 0.0061 0,00033 1 8260B 2/22118 0:07 ANG PBB0397 Bromodichioromethane BRL mg/kg dry 0.0061 0.00034 1 8260B 2/22/18 0:07 ANG P8B0397 Bromoform BRL mg/kg dry 0.0061 0.00069 1 8260B 2/22/18 0:07 ANG PBB0397 Bromomethane BRL mg/kg dry 0.012 0.00075 1 82608 2/22/18 0:07 ANG PBS0397 Carbon Tetrachloride BRL mg/kg dry 0.0061 0,00030 1 8260B 2/22/18 0:07 ANG P8130397 Chlorobenzene BRL mg/kg dry 0.0061 0.00032 1 8260B 2/22/16 0:07 ANG 1`8130397 Chloroethane BRL mg/kg dry 0.012 0.00050 1 8260B 2/22/18 0:07 ANG P8B0397 Chloroform BRL mg/kg dry 0.0061 0.00044 1 82608 2122/18 0:07 ANG P8B0397 Chloromethane BRL mg/kg dry 0.0061 0.00041 1 8260B 2/22/16 0:07 ANG P8B0397 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0061 0,00026 1 8260B 2122/18 0:07 ANG P8B0397 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0061 0.00020 1 8260B 2122/16 0:07 ANG P8B0397 Dibromochloromethane BRL mg/kg dry 0.0061 0.00025 1 8260B 2/22/18 0:07 ANG PBB0397 Dichlorodi8uoromethane BRL mg/kg dry 0.0061 0.00027 1 8260B 2/22/18 0:07 ANG P8B0397 Ethylbenzene BRL mg/kg dry 0.0061 0,00023 1 8260B 2/22/18 0:07 ANG P8130397 Isopropyl Ether BRL mg/kg dry 0.0061 0,00025 1 8260B 2122/18 0:07 ANG P8130397 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0061 0.00036 1 8260B 2/22/18 0:07 ANG PBB0397 m,p-Xylenes BRL mg/kg dry 0.012 0,00056 1 8260B 2/22118 0:07 ANG P8B0397 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.061 0.00055 1 8260B 2122118 0:07 ANG PBB0397 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.12 0.00055 1 8260B 2/22/18 0:07 ANG P880397 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 704/529-6364-Toll Free Number; l-8001629-6364- Fax: 7041626-0409 Page 15of52 P.R I S M I rutt_6ervice Analytical a Laboratory Report Enmrommantat somttons 02/27/2018 ueo,vnronms me Geoscience Group Project: Truck Part Service Client Sample ID: S3 Attn: Tom Hassett Prism Sample ID: 8020233-03 500-K Clanton Rd. Prism Work Order: 8020233 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 02/13/18 09:50 Time Submitted: 02/13/18 15:18 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Methyl Isobutyl Ketone BRL Methylene Chloride BRL Methyl-tert-Butyl Ether BRL Naphthalene BRL n-Butylbenzene BRL n-Propylbenzene BRL c-Xylene BRL sec-Butylbenzene BRL Styrene BRL tert-Butylbenzene BRL Tetrachlomethylene BRL Toluene BRL trans-1,2-Dichlorcethylene BRL trans-1,3-Dichloropropylene BRL Trichloroethylene BRL Trichlorofluoromethane BRL Vinyl acetate BRL Vinyl chloride BRL Xylenes, total BRL mg/kg dry 0.061 0.00052 1 8260B 2122/10 0:07 ANG P8B0397 mg/kg dry 0,012 0.00034 1 8260B 2/22/18 0:07 ANG P8B0397 m9/k9 dry 0.012 0.00019 1 8260B 2/22/18 0:07 ANG P8B0397 mg/kg dry 0.012 0.00019 1 8260B 2/22/18 0:07 ANG P8130397 mg/kg dry 0.0061 0.00031 1 8260B 2/22/18 0:07 ANG P8B0397 mg/kg dry 0.0061 0.00036 1 8260B 2/22/18 0:07 ANG P880397 mg/kg dry 0.0061 0.00025 1 8260B 2/22118 0:07 ANG P8B0397 mg/kg dry 0.0061 0.00029 1 8260B 2/22/18 0:07 ANG PBB0397 mg/kg dry 0.0061 0.00036 1 B260B 2/22/18 0:07 ANG P8B0397 mg/kg dry 0.0061 0,00020 1 8260B 2/22/18 0:07 ANG P8130397 mg/kg dry 0.0061 0.00029 1 8260B 2/22/18 0:07 ANG PBB0397 mg/kg dry 0.0061 0.00035 1 8260B 2/22/18 0:07 ANG P8130397 mg/kg dry 0,0061 0.00036 1 8260B 2/22/18 0:07 ANG P8130397 mg/kg dry 0,0061 0.00032 1 8260B 2/22/18 0:07 ANG P8B0397 mg/kg dry 0,0061 0.00039 1 8260B 2122/18 0:07 ANG P860397 mg/kg dry 0.0061 0.00039 1 8260B 2/22118 0:07 ANG PBB0397 mg/kg dry 0.030 0.00083 1 8260B 2/22116 0:07 ANG PBB0397 mg/kg dry 0.0061 0.00029 1 8260B 2/22/18 0:07 ANG P880397 mg/kg dry 0.018 0.0011 1 8260B 2/22/18 0:07 ANG PBB0397 Surrogate Recovery Control Limits 4-Bromofluorobenzene 102 % 70-130 Dibromofluoromethane 103 % 84-123 Toluene-d8 102 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID RLM C5-C8 Aliphatics BRL mg/kg dry 5A 0.18 100 MADEP VPH 2/14/18 20:26 ANG/J P8B0270 C9-C12 Allphatics 3.6 J mg/kg dry 6.4 0.28 100 MADEP VPH 2114118 20:26 ANG/J P8B0270 C9-C10 Aromatics 0.62 J mg/kg dry SA 0.061 100 MADEP VPH 2/14118 20:26 ANG/J P8130270 Surrogate Recovery Control Limits 2,5-Dibrom0t0luene (PID) 159 % 70-130 SR 2,5-Dibromotoluene (Flo) 160 % 70-130 SR This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, INC 28224-0643 Phone: 704/529-6364 - Toll Free Number: l-B00/529-6364- Fax: 70416264409 Page16of52 r W vISM I r°Il6ervineAnal„icala Environmental Solutions "usoxnrox,w ixc Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Sample Matrix: Solid Laboratory Report 02/27/2018 Client Sample ID: S4 Prism Sample ID: 8020233-04 Prism Work Order: 8020233 Time Collected: 02/13/18 10:05 Time Submitted: 02/13118 15:18 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Extractable Petroleum Hydrocarbons by GC/FID C9-C18 Aliphatics 1.2 J mgrkg dry 36 0.23 1 MADEP EPH 2/16118 4:04 ZRC P8B0289 C79-C36 Aliphatcs BRL mg/kg dry 36 4.3 1 MADEP EPH 2116118 4:04 ZRC P8B0289 C11-022Aromatics _ BRL _ _mg/kg dry 15 2.6 1 MADEP EPH 2/16/18 4:04 ZRC P8B0289 Surrogate Recovery Control Limits 1-Chlorooctadeczne 77 % 40-140 o-Terphenyl 77 % 40-140 2-Fluorobiphenyl 89 % 40-140 2-Bromonaphthalene 60 % 40-140 General Chemistry Parameters Solids 67.0 % by 0.100 0.100 1 SM2540 G 2114118 16:00 BJC PSB0281 Weight Semivolatile Organic Compounds by GC/MS f:V 1,2,4-Trichlorobenzene BRL mg/kg dry 0.49 0,077 1 8270D 2/19118 17:52 JMV PBB0345 1,2-Dichlorobenzene BRL mg/kg dry 0,49 0.075 1 8270D 2/19118 17:52 JMV P8B0345 1,3-Dichlorobenzene BRL mg/kg dry 0.49 0.069 1 8270D 2/19118 17:52 JMV PBB0345 1,4-Dichlorobenzene BRL mg/kg dry 0.49 0.072 1 8270D 2/19/18 17:52 JMV P880345 1-Methylnaphthalene BRL mg/kg dry 0.49 0,095 1 8270D 2/19118 17:52 JMV PBB0345 2,4,6-Trichlorophenoi BRL mg/kg dry 0.49 0.092 1 8270D 2/19/18 17:52 JMV PBB0345 2,4-Dichlorophenol BRL mg/kg dry 0.49 0,095 1 8270D 2/19/18 17:52 JMV P8B0345 2,4-Dimethyiphenol BRL mg/kg dry 0,49 0.076 1 8270D 2/19/18 17:52 JMV PBB0345 2,4-Dinitrophenol BRL CCV mg/kg dry 0.49 0.069 1 8270D 2/19118 17:52 JMV P8B0345 2,4-Dinitrotoluene BRLA mg/kg dry 0.49 0.060 1 8270D 2/19/18 17:52 JMV PBB0345 2,6-Dinitrotoluene BRL mg/kg dry 0.49 0.066 1 8270D 2/19118 17:52 JMV P8B0345 2-Chloronaphthalene BRL mg/kg dry 0.49 0.071 1 8270D 2119/18 17:52 JMV PBB0345 2-Chlorophenol BRL mg/kg dry 0.49 0.070 1 8270D 2119/18 17:52 JMV P8B0345 2-Methylnaphthalene BRL mg/kg dry 0.49 0.079 1 8270D 2/19/18 17:52 JMV P8B0345 2-Melhylphenol BRL mg/kg dry 0.49 0.063 1 8270D 2/19/18 17:52 JMV PBB0345 2-NBrophenol BRL mg/kg dry 0A9 0,090 1 6270D 2/19118 17:52 JMV P8B0345 30-Dichiorobenzidine BRL mg/kg dry 0.49 0.097 1 8270D 2/19/18 17:52 JMV P8B0345 3/4-Methylphenol BRL mg/kg dry 0.49 0.061 1 8270D 2/19/18 17:52 JMV P8B0345 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.49 0.074 1 8270D 2119/18 17:52 JMV P8B0345 4-Bromophenyl phenyl ether BRL mg/kg dry 0.49 0.085 1 8270D 2/19118 17:52 JMV P8B0345 4-Chloro-3-methylphenol BRL mg/kg dry OAS 0.069 1 8270D 2/19118 17:52 JMV PBB0345 4-Chloroaniline BRL mg/kg dry 0.49 0.059 1 8270D 2119118 17:52 JMV P8B0345 4-Chlorophenyl phenyl ether BRL mg/kg dry 0,49 0.064 1 8270D 2/19/18 17:52 JMV PBB0345 4-Nitrophenol BRL mg/kg dry 0.49 0.076 1 8270D 2119118 17:52 JMV P8B0345 Acenaphthene BRL ml dry 0.49 0.067 1 8270D 2/19/18 17:52 JMV PBB0345 Acenaphthylene BRL mg/kg dry 0A9 0.071 1 8270D 2119/18 17:52 JMV PBB0345 Anthracene BRL mg/kg dry 0.49 0.079 1 8270D 2/19/18 17:52 JMV PSB0345 Azobenzene BRL mg/kg dry 0.49 0,065 1 8270D 2/19/18 17:52 JMV PBB0345 Benzo(a)anthracene BRL mg/kg dry 0.49 0.064 1 8270D 2/19118 17:52 JMV PBB0345 Bemo(e)pyrene BRL mg/kg dry 0.49 0.053 1 8270D 2/19/18 17:52 JMV PBB0345 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spdngbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041529-6364- Toll Free Number: 1-8001629-6364 - Fax: 7041625-0409 Page 17 of 52 PRISMI Laboratory Report s a Full-aervlce Analytical 4 Environmental Solutions 02/27/2018 W'sasurosxa roc Geoscience Group Project: Truck Part Service Client Sample ID: S4 Attn:Tom Hassett Prism Sample ID: 8020233-04 500-K Clanton Rd. Prism Work Order: 8020233 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 02/13/18 10:05 Time Submitted: 02/13/18 15:18 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Datelrime ID Benzo(b)fluomnthene BRL mg/kg dry 0.49 0.057 1 8270D 2119/18 17:52 JMV F%B0345 Benzo(g,h,i)perylene BRL mg/kg dry 0.49 0.054 1 8270D 2/19/18 17:52 JMV P8BO345 Benzo(k)fluoranthene BRL mg/kg dry 049 0.065 1 8270D 2/19118 17:52 JMV P8B0345 Benzoic Acid 0.62 mg/kg dry 0.49 0.041 1 8270D 2119118 17:52 JMV P8B0346 Benzyl alcohol BRL mg/kg dry 0,49 0.065 1 8270D 2/19118 17:52 JMV P8B0345 bis(2-Chloroethoxy)methane BRL mg/kg dry OA9 0.086 1 8270D 2/19118 17:52 JMV P8B0345 Bis(2-Chloroethyl)ether BRL mg/kg dry 0,49 0.070 1 8270D 2/19118 17:52 JMV P8B0345 Bis(2-chloroisopropyl)ether BRL mg/kg dry 0.49 0.084 1 8270D 2/19118 17:52 JMV PBB0345 Bis(2-Ethylhexyl)phthalate BRL mg/kg dry OA9 0.073 1 8270D 2/19/18 17:52 JMV P8B0345 Butyl benzyl phthalate BRL mg/kg dry 0,49 0,070 1 8270D 2/19/18 17:52 JMV P880345 Chrysene BRL mg/kg dry 0.49 0,062 1 8270D 2/19/18 17:52 JMV P8BO345 Dibenzo(a,h)anthmcene BRL mg/kg dry 0.49 0,060 1 8270D 2/19/18 11:52 JMV PBB0345 Dibenzofuran BRL mg/kg dry 0.49 0.075 1 8270D 2/19/18 17:52 JMV PBB0345 Diethyl phthalate BRL mg/kg dry OA9 0,068 1 8270D 2119/18 17:52 JMV POB0345 Dimethyl phthalate BRL mg/kg dry 0.49 0.065 1 8270D 2119/18 17:52 JMV PBB0345 Di-n-butyl phthalate BRL mg/kg dry 0.49 0.070 1 8270D 2/19118 17:52 JMV P8B0345 Di-n-ocryl phthalate BRL mg/kg dry OA9 0.061 1 8270D 2/19/18 17:52 JMV PBB0345 Fluoranthene BRL mg/kg dry 0,49 0.063 1 8270D 2/19/18 17:52 JMV P880345 Fluorene BRL mg/kg dry 0.49 0,071 1 8270D 2/19118 17:52 JMV PBB0345 Hexachlorobenzene BRL mg/kg dry 0,49 0.078 1 8270D 2119/18 17:52 JMV P8BO345 Hexachlorobutadiene BRL rrg/kg dry 0.49 0.089 1 8270D 2/19118 17:52 JMV P8B0345 Hexachlorocyclopentadiene BRL mg/kg dry 0.49 0.088 1 8270D 2/19/18 17:52 JMV PBB0345 Hexachloroethane BRL mg/kg dry 0.49 0.083 1 8270D 2/19/18 1752 JMV P8B0345 Indeno(1,2,3-cd)pyrene BRL mg/kg dry 0.49 0.057 1 8270D 2/19/18 17:52 JMV P8B0345 Isophorone BRL mg/kg dry 0,49 0.067 1 8270D 2119/18 17:52 JMV PBB0345 Naphthalene BRL mg/kg dry 0.49 0.079 1 8270D 2/19/18 17:52 JMV P8B0345 Nitrobenzene BRL mg/kg dry OA9 0.070 1 8270D 2/19/18 17:52 JMV PBB0345 N-Nitrosodi-n-propylamine BRL mg/kg dry 0.49 0.078 1 8270D 2/19/18 17:52 JMV P8BO345 N-Nitrosodiphenylemine BRL mg/kg dry 049 0.075 1 8270D 2/19118 17:52 JMV PBB0345 Pentechiorophenol BRL mg/kg dry 0.49 0,058 1 8270D 2119/18 17:52 JMV PBB0345 Phenanthrene BRL mg/kg dry 0.49 0.064 1 8270D 2/19/18 17:52 JMV PBB0345 Phenol BRL mg/kg dry 0,49 0.073 1 8270D 2/19/18 17:52 JMV PBB0345 Pyrene _ BRL mg/kg dry 0.49 0.065 1 8270D 2/19/18 17:52 JMV P8130345 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 78 % 39-132 2-Fluorobiphenyl 79 % 44-115 2-Fluorophenol 71 % 35-115 Nitrobenzened5 72 % 37-122 Phenol-d5 73 % 34-121 Terpheny1-d14 78% 54-127 Volatile Organic Compounds by GC1MS 1, 1, 1,2-Tetrachloroethane BRL mg/kg dry 0.0068 0.00056 1 8260B 2/22/18 0:35 ANG PBB0397 1,1,1-Trichloroethane BRL mg/kg dry 0.0068 0.00033 1 8260B 2/22/18 0:35 ANG PBB0397 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364- Tall Free Number: 1.8001629-6364 - Fax: 7041626-0409 Page 18 of 52 � 1• Is n I Full -Service Analytical s Laboratory Report ' V' Environmemal Solutions 02/27/2018 IwmMiOgIE41NG Geoscience Group Project: Truck Part Service Client Sample ID: S4 Attn: Tom Hassett Prism Sample ID: 8020233-04 500-K Clanton Rd. Prism Work Order: 8020233 Charlotte, INC 28217 Sample Matrix: Solid Time Collected: 02/13/18 10:05 Time Submitted: 02/13/18 15:18 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Dalefrime ID 1,1,2,2-Tetrachloroethane BRL mg/kg dry 0.0068 0.00046 1 8260B 2/22118 0:35 ANG PBB0397 1, 1,2-Trichloroethane BRL mg/kg dry 0.0068 0.00060 1 8260B 2122/18 0:35 ANG PBB0397 1,1-Dichloroethane BRL mg/kg dry 0.0068 0.00019 1 8260B 2122118 0:35 ANG P8130397 1,1-Dichloroethylene BRL mg/kg dry 0.0068 0.00030 1 8260B 2/22/18 0:35 ANG P880397 1,1-Dichloropropylene BRL mg/kg dry 0.0068 0,00037 1 8260B 2122118 0:35 ANG PBB0397 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0068 0,00039 1 8260B 2/22/18 0:35 ANG PBB0397 1,2,3-Trichloropropane BRL mg/kg dry 0.0068 0,00087 1 B260B 2122/18 0:35 ANG P8130397 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0068 0.00051 1 8260B 2/22/18 0:35 ANG P8B0397 1,2,4-Trimethylbenzene BRL mg/kg dry 0.0068 0.00052 1 8260B 2/22/18 0:35 ANG P8130397 1,2-Dibromoethane BRL mg/kg dry 0,0068 0.00027 1 8260B 2/22/18 0:35 ANG P8B0397 1,2-Dichlorobenzene BRL mg/kg dry 0,0068 0.00032 1 82608 2/22/18 0:35 ANG P8B0397 1,2-Dichloroethane BRL mg/kg dry 0.0068 0.00041 1 8260B 2/22/18 035 ANG P8130397 1,2-Dichloropropane BRL mg/kg dry 0.0068 0.00042 1 8260B 2/22118 0:35 ANG P8B0397 1,3,5-Trimethylbenzene BRL mg/kg dry 0.0068 0.00051 1 8260B 2/22/18 0:35 ANG P8130397 1,3-Dichlorobenzene BRL mg/kg dry 0.0068 0.00045 1 8260B 2/22/18 035 ANG P8B0397 1,3-Dichloropropane BRL mg/kg dry 0.0068 0.00034 1 8260B 2/22/18 0:35 ANG P8130397 1,4-Dichlorobenzene BRL mg/kg dry 0.0068 0.00027 1 8260B 2122/18 0:35 ANG PBB0397 2,2-Dichloropropane BRL mg/kg dry 0.0068 0.00032 1 8260B 2/22118 0:35 ANG PBB0397 2-Chlorotoluene BRL mg/kg dry 0,0068 0,00035 1 8260B 2/22/18 0:35 ANG P8130397 4-Chlorotoluene BRL mg/kg dry 0.0068 0.00041 1 8260B 2/22/18 0:35 ANG P8130397 4-Isopropyltoluene BRL mg/kg dry 0.0068 0.00033 1 8260B 2/22/18 0:35 ANG P8B0397 Acetone 0.067 J mg/kg dry 0.068 0.0017 1 8260B 2/22118 0:36 ANG PBB0397 Benzene BRL mg/kg dry 0.0041 0.00040 1 8260B 2/22/18 0:35 ANG P8130397 Bmmobenzene BRL mg/kg dry 0,0068 0.00057 1 8260B 2/22/18 0:35 ANG P8B0397 Bromochloromethane BRL mg/kg dry 0,0068 0,00037 1 B260B 2/22/18 0:35 ANG PBB0397 Bromodichloromethane BRL mg/kg dry 0.0068 0.00038 1 8260B 2/22/18 0:35 ANG P880397 Bromoform BRL mg/kg dry 0.0068 0.00077 1 8260B 2/22/18 0:35 ANG P8B0397 Bromomethane 0.0062 J mg/kg dry 0.014 0.00084 1 8260B 2122118 0:36 ANG PBB0397 Carbon Tetrachloride BRL mg/kg dry 0.0068 0.00034 1 82608 2/22/18 0:35 ANG P860397 Chlorobenzene BRL mg/kg dry 0.0068 0.00036 1 8260B 2122118 0:35 ANG PBB0397 Chloroethane BRL mg/kg dry 0.014 0.00057 1 8260B 2122/18 0:35 ANG P8B0397 Chloroform BRL mg/kg dry 0.0068 0.00049 1 8260B 2/22/18 0:35 ANG PBB0397 Chdromelhane BRL mg/kg dry 0.0068 0.00046 1 8260B 2122/18 0:35 ANG P8B0397 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0068 0o0029 1 8260B 2/22118 035 ANG PBB0397 cis-1,3-Dichloropropylene BRL mg/kg dry 0,0068 0,00023 1 8260B 2/22/18 0:35 ANG P8130397 Dibromochloromethane BRL mg/kg dry 0.0068 0.00028 1 82608 2/22/18 035 ANG PBB0397 Dichiorodifluoromethane BRL mg/kg dry 0.0068 0.00031 1 8260B 2/22/18 0:35 ANG P8130397 Ethylbenzene BRL mg/kg dry 0.0068 0.00026 1 6260B 2/22/18 0:35 ANG PBB0397 Isopropyl Ether BRL mg/kg dry 0.0068 0.00028 1 8260B 2/22/18 0:35 ANG PBB0397 Isopropylbenzene (Cumene) BRL mg/kg dry 0.0068 0.00040 1 8260B 2/22118 0:35 ANG P880397 m,p-Xylenes BRL mg/kg dry 0,014 0.00063 1 8260B 2/22/18 0:35 ANG PBB0397 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.068 0,00062 1 8260B 2/22118 0:35 ANG P8130397 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.14 0.00062 1 8260B 2/22/18 0:35 ANG PBB0397 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toll Free Number: l-8001529-6364-Fax: 7041626-0409 Page 19 oi52 PRISM I Full-SemiceAnalytical8 EnWn.0 .ental aolmlona Laboratory Report 02/27/2018 aaauroa,Es 1. Geoscience Group Project: Truck Part Service Client Sample ID: S4 Attn: Tom Hassett Prism Sample ID: 8020233-04 500-K Clanton Rd. Prism Work Order: 8020233 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 02/13/18 10:05 Time Submitted: 02/13/18 15:18 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DatelTime ID Methyl Isobutyl Ketone BRL mg/kg dry 0.068 0.00058 1 8260B 2/22/18 0:35 ANG P8130397 Methylene Chloride BRL mg/kg dry 0.014 0.00038 1 82608 2/22/18 0:35 ANG PBB0397 Methyl-tert-Butyl Ether BRL mg/kg dry 0014 0.00022 1 8260B 2122/18 0:35 ANG P8130397 Naphthalene BRL mg/kg dry 0.014 0.00022 1 8260B 2122/18 0:35 ANG P8B0397 n-Butylbenzene BRL mg/kg dry 0.0068 0.00035 1 8260B 2/22/18 0:35 ANG PBB0397 n-Propylbenzene BRL mg/kg dry 0.0068 0.00040 1 B260B 2/22/18 0:35 ANG PBB0397 c-Xylene BRL mg/kg dry 0.006B 0.00028 1 8260B 2/22118 0:35 ANG PBB0397 see-Butylbenzene BRL mg/kg dry 0,0068 0.00033 1 8260B 2/22/16 0:35 ANG P8B0397 Styrene BRL mg/kg dry 0.0068 0.00041 1 82608 2/22/18 0:35 ANG P880397 tert-Butylbenzene BRL mg/kg dry 0.0068 0,00023 1 8260B 2/22118 0:35 ANG PBB0397 Tetmchloroethylene BRL mg/kg dry 0.0068 0.00032 1 8260B 2/22/18 0:35 ANG PBB0397 Toluene BRL mg/kg dry 0.0068 0.00039 1 8260B 2/22/lB 0:35 ANG P880397 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0068 0.00041 1 8260B 2/22/18 0:35 ANG PBB0397 Vans-1,3-Dichloropropylene BRL mg/kg dry 0.0068 0.00036 1 8260B 2/22118 0:35 ANG P8B0397 Trichloroethylene BRL mg/Icg dry 0.0068 0.00044 1 8260B 2/22118 0:35 ANG PBB0397 Trichlorofluoromethane BRL mg/kg dry 0,0068 0.00044 1 8260B 2/22/18 0:35 ANG PBB0397 Vinyl acetate BRL mg/kg dry 0.034 0,00093 1 8260B 2/22118 0:35 ANG P8B0397 Vinyl chloride BRL mg/kg dry 0.006E 0.00033 1 8260B 2/22118 0:35 ANG PBB0397 Xylenes, total BRL ni dry 0.020 0,0013 1 8260B 2/22/18 095 ANG PBB0397 Surrogate Recovery Control Limts 4-BromoOuorobemene 100 % 70-130 Dibromo0uoromethane 104 % 84-123 Toluene-d8 102 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID RLM C5-C8 Aliphatics BRL mg/kg dry 6A 0.21 100 MADEP VPH 2114/18 20:54 ANG/J P8130270 C9-C12 Aliphatics BRL mg/kg dry 6.4 0.33 100 MADEP VPH 2/14/18 20:54 ANG/J P8130270 C9-C10 Aromatics BRL mg/kg dry 6A 0.072 100 MADEP VPH 2114/18 2054 ANG/J PBB0270 Surrogate Recovery Control Limits 2,5-Dibromotoluene (PID) 160 % 70-130 SR 2,5-Dibromotoluene (FID) 162 % 70-130 SR This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0643 Phone: 7041629-6364 - Toll Free Number: l-8001629-6364-Fax: 704/626-0409 Page 20 o152 /p' ISM Laboratory Report Full -Service Analytical 4 Environmental solutions 02/27/2018 u.oxmnua ian Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, INC 28217 Project: Truck Part Service Sample Matrix: Solid Client Sample ID: S5 Prism Sample ID: 8020233-05 Prism Work Order: 8020233 Time Collected: 02/13/18 15:01 Time Submitted: 02/13118 15:18 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Datef ime ID Extractable Petroleum Hydrocarbons by GC/FID C9-Ct8 Aliphatics 6.8 J mg/kg dry 39 0.26 1 MADEP EPH 2116118 6:17 ZRC P8B0289 C19-C36 Alipha8cs BRL mg/kg dry 39 4.6 1 MADEP EPH 2/16/18 5:17 ZRC P8130289 C11-C22Aromatics _ BRL mg/kg dry 16 2.8 1 MADEP EPH 2/16/18 5:17 ZRC PBB0289 Surrogate Recovery Control Limits 1-Chlorcoctadecane 74 % 40-140 o-Terphenyl 69 % 40-140 2-Fluorobiphenyl 85 % 40-140 2-Bromonaphthalene 68 % 40-140 General Chemistry Parameters % Solids 63.0 % by 0.100 0.100 1 SM2540 G 2114118 16:00 BJC P8130281 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene BRL mg/kg dry 0.52 0.081 1 8270D 2J19/18 18:14 JMV PBB0345 1,2-Dichlorobenzene BRL mg/kg dry 0.52 0.079 1 8270D 2/19/18 18:14 JMV P880345 1,3-Dichlorobenzene BRL mg/kg dry 0.52 0.074 1 8270D 2/19/18 18:14 JMV PBB0345 1,4-Dichlorobenzene BRL mg/kg dry 0,52 0.076 1 8270D 2/19/18 18:14 JMV P880345 1-Methylnaphthalene BRL mg/kg dry 0.52 0.10 1 8270D 2/19/18 18:14 JMV P880345 2,4,6-Trichlorophenol BRL mg/kg dry 0.52 0,098 1 8270D 2/19/18 18:14 JMV PBB0345 2,4-Dichlomphenol BRL mg/kg dry 0.52 0.10 1 8270D 2119118 18:14 JMV P8B0345 2,4-Dimethylphenol BRL mg/kg dry 0.52 oollo 1 8270D 2/19/18 18:14 JMV PBB0345 2,4-Dinitmphenol BRL CCV mg/kg dry 0.52 0.073 1 8270D 2/19/18 18:14 JMV PBB0345 2,4-Dinitrotoluene BRLA mg/kg dry 0.52 0.063 1 8270D 2/19/18 18:14 JMV P860345 2,6-Dinitmtoluene BRL mg/kg dry 0.52 0.069 1 8270D 2/19/18 18:14 JMV PBB0345 2-Chloronaphthalene BRL mg/kg dry 0.52 0.076 1 8270D 2/19/18 18:14 JMV PBB0345 2-Chlomphenol BRL mg/kg dry 0.52 0.074 1 8270D 2/19/18 16:14 JMV P880345 2-Methylnaphthalene BRL mg/kg dry 0,52 0,084 1 8270D 2/19/18 18:14 JMV P8150345 2-Methylphenol BRL mg/kg dry 0.52 0.067 1 8270D 2/19118 18:14 JMV P8130345 2-Nitrophenol BRL mg/kg dry 0,52 0.095 1 8270D 2/19118 18:14 JMV PBB0345 3,3'-Dichlorobenzidine BRL mg/kg dry 0.52 0.10 1 8270D 2/19/18 18:14 JMV PBB0345 3/4-Methylphenol BRL mg/kg dry 0.52 0.064 1 8270D 2/19118 18:14 JMV P8B0345 4,6-Dinitro-2-methylphenol BRL mg/kg dry 0.52 0.078 1 8270D 2119/18 18:14 JMV PBB0345 4-Bromophenyl phenyl ether BRL mg/kg dry 0.52 0.090 1 6270D 2/19118 18:14 JMV P8B0345 4-Chloro-3-methylphenol BRL mg/kg dry 0.52 0.073 1 8270D 2/19/18 18:14 JMV PBB0345 4-Chloroaniline BRL mg/kg dry 0,52 0.063 1 8270D 2/19/18 18:14 JMV PfIB0345 4-Chlorophenyl phenyl ether BRL mg/kg dry 0.52 0.068 1 8270D 2/19/18 18:14 JMV PBB0345 4-Nitrophenol BRL mg/kg dry 0.52 0,081 1 8270D 211911818:14 JMV P8130345 Acenaphthene BRL mg/kg dry 0.52 0.071 1 8270D 2119/18 18:14 JMV P880345 Acenaphthylene BRL mg/kg dry 0.52 0,076 1 8270D 2/19/18 18:14 JMV P8130345 Anthracene BRL mg/kg dry 0,52 0.084 1 8270D 2/19/18 18:14 JMV P8B0345 Azobenzene BRL mg/kg dry 0.52 0.069 1 8270D 2/19118 18:14 JMV PBB0345 Benzo(a)anthracene BRL mg/k9 dry 0.52 0.068 1 8270D 2/19/18 18:14 JMV PBB0345 Benzo(a)pyrene BRL mg/kg dry 0.52 0.056 1 8270D 2/19/18 18:14 JMV P8130345 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364- Toll Free Number: 1-8001629-6364 - Fax: 7041526-0409 Page 21 of 52 Laboratory Report W' S ^ � I Full -Service al Sol do s ' V' Environmental Solutions 02/27/2018 'p .`ssa cnl a we Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Sample Matrix: Solid Client Sample ID: S5 Prism Sample ID: 8020233-05 Prism Work Order: 8020233 Time Collected: 02/13/18 15:01 Time Submitted: 02/13/18 15:18 Parameter Result Units Report MIX Dilution Method Analysis Analyst Batch Limit Factor Date rime ID Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluomnthene Benzoic Acid Benzyl alcohol bis(2-Chloroethoxy) methane Bis(2-Chloroethyl)ether Bis(2-chloroisopropyl)ether Bis(2-Ethylhexyl)phthalate Butyl benzyl phthalate Chrysene Dibenzo(a,h)anthracene Dihenzofuran Diethyl phthalate Dimethyl phthalate Di-n-butyl phthalate Di-n-octyl phthalate Fluoranthene Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane mdeno(1,2,3-cd)pyrene sophorone Naphthalene Nitrobenzene N-Nitroso-di-n-propylamine N-NRrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL BRL mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry ml dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry mg/kg dry 0,52 0.52 0.52 0.52 0.52 0.52 0,52 0.52 0.52 0.52 0.52 0.52 052 0.52 0.52 0.52 0.52 0.52 0.52 0,52 0.52 0.52 0,52 0.52 0,52 0.52 0.52 0.52 0.52 0.52 0.52 0.52 0.52 0.061 0.057 0.068 0.044 0.069 0.091 0,074 0.089 0.078 0,074 0.066 0.064 0.079 0.072 0.069 0,074 0.064 0,067 0.075 0.083 0,094 0.093 0.087 0.060 0,071 0.084 0.074 0,082 0.079 0.062 0.068 0.077 0.069 Surrogate 2,4,6-Tdbromophenol 2-Fluorobiphenyl 2-Fluorophenol Nitrobenzene-d5 Phenol-t15 Terphenyl-dl4 1 1 1 7 1 1 1 1 1 1 1 i 1 1 1 1 1 1 1 i 1 1 1 1 1 1 1 1 8270D 8270D 8270D 8270D 8270D B270D 8270D 8270D 8270D 8270D 8270D 8270D 8270D 8270D 8270D 8270D 8270D 8270D 8270D 8270D 8270D 8270D 8270D 8270D 8270D 8270D 8270D 82701) 6270D 8270D 8270D 8270D 8270D Recover 2119118 18:14 2/19118 18:14 2/19118 18:14 2/19/18 18:14 2/19118 18:14 2/19118 18:14 2/19/18 18:14 2119/18 18:14 2119118 18:14 2119/18 18:14 2/19/1 B 18:14 2/19118 18:14 2/19/18 18:14 2/19/18 18:14 2/19/18 18:14 2/19/18 18:14 2119118 18:14 2/19/18 18:14 2/19118 18:14 2/19118 18:14 2/19/18 18:14 2/19/18 18:14 2/19/18 18:14 2M9/18 18:14 2/19/18 18:14 2/19118 1874 2/19/18 18:14 2/19/18 18:14 2/19118 16:14 2119/18 16:14 2/19/18 18:14 2/19118 18:14 2/19/18 18:14 JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV JMV PBB0345 PBB0345 PBB0345 P8B0345 PBB0345 PBB0345 P8B0345 P8B0345 P8B0345 P8B0345 P8B0345 PBB0345 P880345 PBB0345 P860345 P8B0345 PBB0345 P880345 P860345 P880345 P8B0345 P8B0345 P8B0345 PBB0345 P8B0345 P8B0345 P8B0345 P880345 P8B0345 P8B0345 P880345 P8B0345 P8B0345 Control Limits 77 % 39-132 78 % 44-115 72 % 35-115 70 % 37-122 72 % 34-121 75 % 54-127 Volatile Organic Compounds by GC/MS 1,1,1,2-Tetmchloroethane BRL mg/kg dry 0.0055 0.00053 1 8260B 2/14118 18:32 ANG PBB0263 1,1,1-Trichloroethane BRL mg/kg dry 0.0065 0.00031 1 8260B 2/14/18 18.32 ANG P8130263 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041629-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/625-0409 Page 22 Df 52 71 £flailI n Full-aeMce Analytical8 'V' EmironmeMel SOWnonc ueorwmwea me Laboratory Report 02/27/2018 Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Sample Matrix: Solid Client Sample ID: S5 Prism Sample ID: 8020233-05 Prism Work Order: 8020233 Time Collected: 02/13/18 15:01 Time Submitted: 02/13/18 15:18 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID 1, 1,2,2-Tetmchloroethane BRL mg/kg dry 0.0065 0.00044 1 8260B 2/14/18 18:32 ANG PBB0263 1,1,2-Trichlomelhane BRL mg/kg dry 0.0065 0.00057 1 8260B 2/14118 18:32 ANG PBB0263 1,1.Dichloroethane BRL mg/kg dry 0.0065 0.00018 1 8260B 2/14/18 18:32 ANG P8130263 1,1-Dichloroethylene BRL mg/kg dry 0.0065 0.00029 1 8260B 2114/18 18:32 ANG P880263 1,1-Dichloropropylene BRL mg/kg dry 0.0065 0.00036 1 8260B 2/14/18 18:32 ANG P8130263 1,2,3-Trichlorobenzene BRL mg/kg dry 0.0065 0.00037 1 8260B 2/14118 18:32 ANG P8130263 1,2,3-Trichloropropane BRL mg/kg dry 0.0065 0.00083 1 0260B 2/14/18 18:32 ANG PBB0263 1,2,4-Trichlorobenzene BRL mg/kg dry 0.0065 0.00048 1 8260B 2/14/18 18:32 ANG P8B0263 1,2,4-Trimethylbenzene 0.027 mglkg dry 0.0066 0.00040 1 8260B 2/14/18 18:32 ANG P8130263 1,2-Dibromoethane BRL mg/kg dry 0,0065 0.00026 1 8260B 2/14/18 18:32 ANG PBB0263 1,2-Dichlorobenzene BRL mg/kg dry 0.0065 0,00030 1 6260B 2114/18 18:32 ANG P800263 1,2-Dichloroethane BRL mg/kg dry 0.0065 0-00039 1 8260B 2/14/18 18:32 ANG P8130263 1,2-Dichloropropane BRL mg/kg dry 0,0065 0.00040 1 8260B 2/14/18 18:32 ANG PBB0263 1,3,5-Trimethylbenzene 0.0036 J mg/kg dry 0.0066 0.00049 1 8260B 2114118 18:32 ANG P8130263 1,3-Dichlorobenzene BRL mg/kg dry 0.0065 0.00043 1 8260B 2/14/18 18:32 ANG PBB0263 1,3-Dichloropropane BRL mg/kg dry 0.0065 0,00033 1 8260B 2/14/18 18:32 ANG P8130263 1,4-Dichlorobenzene BRL mg/kg dry 0.0065 0.00026 1 8260B 2/14/18 18:32 ANG P880263 2,2-Dichloropropane BRL mg1kg dry 0.0065 0.00031 1 8260B 2/14118 18:32 ANG PBB0263 2-Chlorotoluene BRL mg/kg dry 0.0065 0.00033 1 8260B 2/14/18 18:32 ANG P8130263 4-Chlorotoluene BRL mg/kg dry 0.0065 0.00039 1 6260B 2/14/18 18:32 ANG P8150263 4-Isopropyholuene 0.0037 J mg/kg dry 0.0066 0.00031 1 82608 2/14118 18:32 ANG P8130263 Acetone BRL mg/kg dry 0.065 0.0016 1 8260B 2/14/18 18:32 ANG PBB0263 Benzene BRL mglkg dry 0.0039 0.00038 1 8260B 2/14/18 18:32 ANG P8B0263 Bromobenzene BRL mg/kg dry 0.0065 0.00054 1 8260B 2114/18 18:32 ANG P8130263 Bromochloromethane BRL mglkg dry 0.0065 0,00036 1 8260B 2/14/18 18:32 ANG PBB0263 Bromodichloromethane BRL mg/kg dry 0.0055 0.00036 1 8260B 2114/16 18:32 ANG P880263 Bromofonn BRL mg/kg dry 0.0065 0.00074 1 8260B 2/14118 18:32 ANG PBB0263 Bromomethane BRL mg/kg dry 0.013 0.00080 1 8260B 2/14118 18:32 ANG P8130263 Carbon Tetrachloride BRL mg/kg dry 0.0065 0.00032 1 8260B 2/14118 18:32 ANG P8190263 Chlorobenzene BRL mg/kg dry 0.0065 0.00034 1 8260B 2/14/18 18:32 ANG P8B0263 Chloroelhane BRL mg/kg dry 0.013 0.00054 1 8260B 2/14/18 18:32 ANG P8B0263 Chloroform BRL mg/kg dry 0.0065 0.00047 1 8260B 2/14/18 18:32 ANG P8B0263 Chloromethane BRL mg/kg dry 0.0065 0.00044 1 82608 2/14/18 18:32 ANG PSB0263 cis-1,2-Dichloroethylene BRL mg/kg dry 0.0065 0.00028 1 8260B 2/14/18 18:32 ANG PBB0263 cis-1,3-Dichloropropylene BRL mg/kg dry 0.0065 0.00022 1 8260B 2/14/18 18:32 ANG PBB0263 Dibromochloromethane BRL mg/kg dry 0.0065 0.00027 1 8260B 2/14/18 18:32 ANG P8B0263 Dichlorodifluoromethane BRL mg/kg dry 0.0065 0.00029 1 6260B 2114/18 18:32 ANG P8130263 Ethylbenzene BRL mg/kg dry 0.0065 0.00025 1 8260B 2/14/18 18:32 ANG P8B0263 Isopropyl Ether BRL mg/kg dry 0.0065 0.00026 1 8260B 2114118 18:32 ANG PBB0263 Isopropylbenzene(Cumene) BRL mg/kg dry 0.0065 0.00038 1 8260B 2/14/18 18:32 ANG PBB0263 m,p-Xylenes BRL mg/kg dry 0.013 0.00060 1 8260B 2/14118 18:32 ANG P8130263 Methyl Butyl Ketone (2-Hexanone) BRL mg/kg dry 0.065 0.00059 1 8260B 2/14/18 18:32 ANG P8130263 Methyl Ethyl Ketone (2-Butanone) BRL mg/kg dry 0.13 0.00059 1 8260B 2/14/18 18:32 ANG P8130263 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toll Free Number: l-8001529-6364-Fax: 704/626-0409 Page 23 of 52 W Full -Service Analytical& R. ISM I Environmental Solutions vaee,aae�� �e� Laboratory Report 02/27/2018 Geoscience Group Project: Truck Part Service Client Sample ID: S5 Attn: Tom Hassett Prism Sample ID: 8020233-05 500-K Clanton Rd. Prism Work Order: 8020233 Charlotte, NC 28217 Sample Matrix: Solid Time Collected: 02113/18 15:01 Time Submitted: 02/13118 15:18 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/rime ID Methyl Isobutyl Ketone BRL mg/kg dry 0,065 0.00055 1 6260B 211411B 18:32 ANG PBB0263 Methylene 61hlonde BRL mg/kg dry 0.013 0.00036 1 8260B 2/14/18 10:32 ANG PBB0263 Methyl-tert-Butyl Ether BRL mg/kg dry 0.013 0.00021 1 8260B 2/14/18 1832 ANG P8B0263 Naphthalene 0.033 mg/kg dry 0.013 0.00020 1 8260B 2114118 18:32 ANG P8130263 n-Butylbenzene 0.0031 J mg/kg dry 0.0066 0.00033 1 82608 2M4/18 18:32 ANG P8130263 n-Propylbenzene BRL mg/kg dry 0.0065 0.00038 1 8260B 2/14/18 18:32 ANG P8B0263 o-Xylene BRL mg/kg dry 0o065 0,00027 1 6260B 2/14/18 1832 ANG P8130263 sec-Butylbenzene 0.0034 J mg/kg dry 0.0065 0.00031 1 8260B 2114118 18:32 ANG P8B0263 Styrene BRL mg/kg dry 0.0065 000039 1 82608 2/14/18 18:32 ANG P8130263 tert-Butylbenzene BRL mg/kg dry 0.0065 0.00022 1 8260B 2/14118 18:32 ANG P8180263 Tetrachloroethylene BRL mg/kg dry 0.0065 0.00031 1 8260B 2/14/18 18:32 ANG PBB0263 Toluene BRL mg/kg dry 0,0065 0.00037 1 82606 2/14118 18:32 ANG PBB0263 trans-1,2-Dichloroethylene BRL mg/kg dry 0.0065 0.00039 1 8260B 2/14/18 18:32 ANG PBB0263 trans-1,3-Dichloropropylene BRL mg/kg dry 0.0065 0,00034 1 8260B 2/14/18 18:32 ANG P880263 Trichloroethylene BRL mg/kg dry 0.0065 0.00042 1 8260B 2/14/18 18:32 ANG PBB0263 Trichlorofluoromethane BRL mg/kg dry 0.0065 0.00042 1 8260B 2/14/18 18:32 ANG POB0263 Vinyl acetate - BRL mg/kg dry 0.032 0,00089 1 8260B 2/14/18 18:32 ANG PBB0263 Vinyl chloride BRL mg/kg dry 0.0065 0.00031 1 8260B 2/14118 18:32 ANG P8130263 Xylenes, total BRL mg/kg dry 0,019 0,0012 1 8260B 2/14/18 18:32 ANG P8B0263 Surrogate Recovery Control Limits 4-Bromofluorobenzene 97 % 70-130 Dibromofluoromethane 104 % 84-123 Toluene -dB 89 % 76-129 Volatile Petroleum Hydrocarbons by GC/PID/FID RLM C5-C8 Aliphatics 11 mg/kg dry 6.3 0.20 100 MADEP VP14 2114118 21:22 ANG/J P8B0270 C9-C12 Aliphatics 220 mg/kg dry 6.3 0.33 100 MADEP VPH 2/14/18 21:22 ANG/J P8130270 C9-C10 Aromatics 120 mg/kg dry 6.3 0.070 100 MADEP VPH 2/14118 21:22 ANG/J PSB0270 Surrogate Recovery Control Limits 2,5-Dibromotoluene(PID) 147% 70-130 SR 2,5-Dibromotoluene (FID) 155 % 70-130 SR This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 704/629-6364- Toll Free Number: t-800/629-6364- Fax: 704/526-0409 Page 24of52 P R i S M I Euvir erv,ce cel 8 Environmental al alS000ns Faeorwropiee,,.c Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GC/MS - Quality Control Analyte Reporting Result Limit Units Level II QC Report 2127/18 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:00PM Spike Source %RED RPD Level Result %REC Limits RPD Limit Notes Batch P8130263 - 5035 Blank(P8B0263•BLK1)_ _ Prepared B Analyzed: 02/14/18 1,1,1,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,1-Trichloroethane BRL 0.0050 mg/kg wet 1, 1,2,2-Tetmchloroethane BRL 0M50 mg/kg wet 1,1,2-Trichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethylene BRL 0,0050 mg/kg wet 1,1-Dichloropropylene BRL 0.0050 mg/kg wet 1,2,3-Trichlorobenzene BRL 0.0050 mg/kg wet 1,2,3-Trichloropropane BRL 0.0050 mg/kg wet 1,2,4-Trichlorobenzene BRL 0.0050 mg/kg wet 1,2,4-Trimethylbenzene BRL 0,0050 mg/kg wet 1,2-Dibromoethane BRL 0.0050 mg/kg wet 1,2-Dichlorobenzene BRL 0.0050 mg/kg wet 1,2-Dichloroethane BRL 0,0050 mg/kg wet 1,2-Dichloropropane BRL 0.0050 mg/kg wet 1,3,5-Trimethylbenzene BRL 0.0050 mg/kg wet 1,3-Dichlorobenzene BRL 0.0050 mg/kg wet 1,3-Dichloropropane BRL 0.0050 mg/kg wet 1,4-Dichlorobenzene BRL 0.0050 mg/kg wet 2,2-Dichloropropane BRL 0,0050 mg/kg wet 2-Chlorotoluene BRL 0.0050 mg/kg wet 4-Chlorotoluene BRL 0.0050 mg/kg wet 4-Isopropyltoluene BRL 0.0050 mg/kg wet Acetone BRL 0.050 mg/kg wet Benzene BRL 0.0030 mg/kg wet Bromobenzene BRL 0.0050 mg/kg wet Bromochloromethane BRL 0.0050 mg/kg wet Bromodichloromethane BRL 0.0050 mg/kg wet Bromoform BRL 0.0050 mg/kg wet Bromomethane BRL 0.010 mg/kg wet Carbon Tetrachlonde BRL 0.0050 mg/kg wet Chlorobenzene BRL 0.0050 mg/kg wet Chioroethane BRL 0.010 mg/kg wet Chloroform BRL 0,0050 mg/kg wet Chioromethane BRL 0,0050 mg/kg wet cis-1,2-Dichloroethylene BRL 0.0050 mg/kg wet cis-1,3-Dichloropropylene BRL 0.0050 mg/kg wet Dibromochloromethane BRL 0.0050 mg/kg wet Dichlorodi8uoromethane BRL 0M50 mg/kg wet Ethylbenzene BRL 0.0050 mg/kg wet Isopropyl Ether BRL 0.0050 mg/kg wet Isopropylbenzene (Cumene) BRL 0.0050 mg/kg wet m,p-Xylenes BRL 0.010 mg/kg wet Methyl Butyl Ketone (2-Hexanone) BRL 0.050 mg/kg wet Methyl Ethyl Ketone (2-Butanone) BRL 0,10 mg/kg wet Methyl Isobutyl Ketone BRL 0.050 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road -P.O. Box 240643 -Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1-800/52M364-Fax: 7041526-0409 Page 25 of52 GARf a Full -Service Analytical & I S M I Environme rtal Solu Iona vsox.nansa Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GC/MS - Quality Control Analyte Reporting Result Limit Units Level II QC Report 2/27/18 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P830263-5035 Blank (PBB0263-BLKI) Prepared & Analyzed: 02/14/18 Methylene Chloride BRL 0.010 mg/kg wet Methyl-tert-Butyl Ether BRL 0.010 mg/kg wet Naphthalene BRL 0.010 mg/kg wet n-Butylbenzene BRL 0.0050 mg/kg wet n-Propylbenzene BRL 0.0050 mg/kg wet o-Xylene BRL 0.0050 mg/kg wet sec-Butylbenzene BRL 0.0050 mg/kg wet Styrene BRL 0.0050 mg/kg wet tert-Butylbenzene BRL 0.0050 mg/kg wet Tetrachloroethylene BRL 0.0050 mg/kg wet Toluene BRL 0,0050 m9/k9 wet trans-72-Dichloroethylene BRL 0,0050 mg/kg wet trans-1,3-Dichloropropylene BRL 0,0050 mg/kg wet Trichloroethylene BRL 0,0050 mg/kg wet Trichloro0uoromethane BRL 0,0050 mg/kg wet Vinyl acetate BRL 0.025 mg/kg wet Vinyl chloride BRL 0.0050 mg/kg wet Xylenes, total BRL 0,015 mg/kg wet Tentatively Identified Compounds Not Detected mg/kg wet Surrogate: 4-Bromofluorobenzene 50.8 ug/L 50.00 102 70-130 Surrogate: Dibromofluoromethane 48.3 ug/L 50.00 97 84-123 Surrogate: Toluene-d8 45.5 U91L 50,00 91 76-129 LCS (PBB0263-BSI) _ - Prepared & Analyzed: 02/14/18 1,1,1,2-Tetrachloroethane 0.0465 0.0060 mg/kg wet 0.05000 93 72-115 1,1,1-Tdchloroethane 0.0456 0.0050 mg/kg wet 0.05000 91 67-131 1, 1,2,2-Tetrachloroethane 0.0403 0.0050 mg/kg wet 0.05000 81 56-126 1,1,2-Trichloroethane 0,0436 0.0050 mg/kg wet 0.05000 87 70-133 1,1-Dichloroethane 0.0460 0.0050 mg/kg wet 0.05000 92 74-127 1,1-Dichloroethylene 0.0521 0,0050 mg/kg wet 0.05000 104 67-149 1,1-Dichloropropylene 0,0499 0,0050 mg/kg wet 0.05000 100 71-130 1,2,3-Trichlorobenzene 0.0399 0.0050 mg/kg wet 0.05000 BO 68-130 1,2,3-Trichloropropane 0.0394 0.0050 mg/kg wet 0.05000 79 60-137 1,2,4-Trichlorobenzene 0.0412 0.0050 mg/kg wet 0.05000 82 66-125 1,2,4-Trimethylbenzene 0.0411 0.0050 mg/kg wet 0.05000 82 69.129 1,2-Dibromoethane 0.0435 0.0050 mg/kg wet 0.05000 87 70-132 1,2-Dichlorobenzene 0.0403 0.0050 mg/kg wet 0.05000 81 72-123 1,2-Dichloroethane 0.0479 0.0050 mg/kg wet 0,05000 96 68-128 1,2-Dichloropropane 0.0484 0.0050 mg/kg wet 0.05000 97 73-130 1,3,5-Trimethylbenzene 0,0405 0.0050 mg/kg wet 0.05000 81 69-128 1 3-Dichlorobenzene 0.0399 0.0050 mg/kg wet 0.05000 80 71-120 1,3-Dichloropropane 0.0449 0,0050 mg/kg wet 0.05000 90 75-124 1,4-Dichlorobenzene 0.0406 0,0050 mg/kg wet 0.05000 81 71-123 2,2-Dichloropropane 0.0474 0.0050 mg/kg wet 0.05000 95 50-142 2-Chlorotoluene 0.0400 0.0050 mg/kg wet 0.05000 80 67-124 4-Chlorotoluene 0.0405 0.0050 mg/kg wet 0.05000 81 71-126 4-I60propyltoluene 0.0394 0,0050 mg/kg wet 0.05000 79 68-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0843 Phone: 704/529-6364 - Toll Free Number; l-800/629-6364- Fax: 7041626-0409 Page 26 of 52 LGAiR T-u1 S M I Full -Service Analytical & Environmental Solutions eonmm�iea we Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, INC 28217 Project: Truck Part Service Volatile Organic Compounds by GCIMS -Quality Control Analyte Batch P8B0263 - 5035 Reporting Result Limit Units Level II QC Report 2/27/1 B Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:o0PM Spike Source hREC RPD Level Result %REC Limits RPD Limit Notes LCS(PBB0263-BSI) _ _ Prepared&_Analyzed: 02/14/18 Acetone 0,100 0.050 mg/kg wet 0.1000 100 29-198 Benzene 0o472 0.0030 mg/kg wet 0.05000 94 74-127 Bromobenzene 0,0398 0.0050 mg/Kg wet 0.05000 80 73-125 Bromochloromethane 0.0468 0.0050 mg/kg wet 0.05000 94 72-134 Bromodichioromethane 0.0495 0,0050 mg/kg wet 0.05000 99 75-122 Bromoform 0.0458 0,0050 mg/kg wet 0.05000 92 66-135 Bromomethane 0.0479 0,010 mg/kg wet 0.05000 96 20-180 Carbon Tetrachloride 0.0481 0.0050 mg/kg wet 0.05000 96 64-143 Chlorobenzene 0.0443 0.0050 mg/kg wet 0.05000 89 74-118 Chloroethane 0.0430 0.010 mg/kg wet 0.05000 86 33-149 Chloroform 0.0499 0.0050 mg/kg wet 0.05000 100 73-127 Chloromethane 0A472 0.0050 mg/kg wet 0,05000 94 45-143 cis-1,2-Dichloroethylene 0.0484 0.0050 mg/kg wet 0.05000 97 76-134 cis- 1,3-Dichloropropylene 0.0502 O.DO50 mg/kg wet 0.05000 100 71-125 Dibromochloromethane 0.0456 0.0050 mg/kg wet 0,05000 91 73-122 Dichlorodifluoromethane 0.0406 0.0050 mg/kg wet 0.05000 81 26-146 Ethylbenzene 0,0454 0.0050 mg/kg wet D.05000 91 74-128 Isopropyl Ether 0.0473 0.0050 mg/kg wet 0,05000 95 59-159 Isopropylbenzene (Cumene) O.D408 0.0050 mg/kg wet 0,05000 82 68-126 m,p-Xylenes 0.0908 0.010 mg/kg wet 0.1000 91 75-124 Methyl Butyl Ketone (2-Hexanone) 0.0456 0.050 mg/kg wet 0.05000 91 61-157 J Methyl Ethyl Ketone (2-Butanone) 0.0490 0.10 mg/kg wet 0.05000 98 63-149 J Methyl Isobutyl Ketone 0.0510 0.050 mg/kg wet 0,05000 102 57-162 Methylene Chloride 0.0479 0.010 mg/kg wet 0.05000 96 74-129 Methyl-tert-Butyl Ether 0.D483 0.01D mg/kg wet 0.05000 97 M130 Naphthalene 0.0406 0.010 mg/kg wet 0,05000 81 57-157 n-Bulylbenzene Do409 0.0050 mg/kg wet 0.05000 82 65-135 n-Propylbenzene 0.0411 0.0050 mg/kg wet 0.05000 82 67-130 o-Xylene 0.0449 0.0050 mg/kg wet 0,05000 90 74-126 seo8utylbenzene 0.0408 0.0050 mg/kg wet 0.05000 82 66-131 Styrene 0.0460 00050 mg/kg wet 0.05000 92 77-121 tert-Butylbenzene 0.0397 0.0050 mg/kg wet 0.05000 79 67-132 Tetrachioroethylene 0,0478 0.0050 mg/kg wet 0.05000 96 68-130 Toluene 0.0478 0.0050 mg/kg wet 0.05000 96 71-129 trans-1,2-Dichloroethylene 0.0480 0.0050 mg/kg wet 0,05000 96 73-132 trans-1,3-Dichloropropylene 0,0508 0.0050 mg/kg wet 0.05000 102 68-123 Trichloroethylene 0.0484 0.0050 mg/kg wet 0.05000 97 75-133 Trichlorolluoromethane 0.0490 0.0050 mg/kg wet 0.05000 98 44-146 Vinyl acetate 0.0669 0.025 mg/kg wet 0.05000 114 85-161 Vinyl chloride 0.0463 0.0050 mg/kg wet 0.05000 93 48-147 Xylenes, total 0.136 0.015 mg/kg wet 0.1500 90 74-126 Surrogate: 4-BromoNuombenzene 48.4 ug/L 50.00 97 70-130 Surrogate. Dibromofluoromethane 47.1 ug/L 50.00 94 84-123 Surrogate: Toluene-0 44.9 u91L 50.00 90 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toll Free Number: l-8001629-6364-Fax: 704/626-0409 Page 27 of 52 RRISM I Full -Service Analytloal & J' V' Environmental Solutions Geoscience Group Attn: Tom Hassell: 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GCIMS - Quality Control Analyte Batch P8BO263 - 5035 Reporting Result Limit Units Level II QC Report 2/27/1 B Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:OOPM Spike Source %REC RPD Level Result % REC Limits RPD Limit Notes LCS Cup (P8130263-19SDI) Prepared & Analyzed: 02/14/18 1,1,1,2-Tetrachloroethane 0.0469 0.0050 mg/kg wet 0.05000 94 72-115 0.9 20 1,11-Trichloroethane 0.0455 0,0050 mg/kg wet 0.05000 91 67-131 0.2 20 1, 1,2,2-Tetmchloroethane o0415 0,0050 mg/kg wet 0.05000 83 56-126 3 20 1,1,2-Trichloroethane 0.0454 0.0050 mg/kg wet 0.05000 91 70-133 4 20 1,1-Dichloroethane 0.0460 0,0050 mg/kg wet 0.05000 92 74-127 0.2 20 1,1-Dichloroethylene 0,0506 0.0050 mg/kg wet 0,05000 101 67-149 3 - 20 1,1-Dichioropropylene 0.0502 OoD50 mg/kg wet 0.05000 100 71-130 0.6 20 1,2,3-Trichlorobenzene 0.0407 0.0050 mg/kg wet 0.05000 81 68-130 2 20 1,2,3-Thchloropropane 0,0404 0.0050 mg/kg wet 0.05000 81 60-137 2 20 1,2,4-Trichlorobenzene 0.0418 0.0050 mg/kg wet 0.05000 84 66-125 1 20 1,2,4-Trimethylbenzene 0.0399 0.0050 mg/kg wet 0,05000 80 69-129 3 20 1,2-Dibromoethane 0.0460 0,0050 mg/kg wet 0,05000 92 70-132 6 20 1,2-Dichlorobenzene 0.0410 0.0050 mg/kg wet 0,05000 82 72-123 2 20 1,2-Dichloroethane 0.0498 0,0050 mg/kg wet D.05000 100 68-128 4 20 1,2-Dichloropropane 0.0501 0.0050 mg/kg wet 0.05000 100 73-130 3 20 1,3,5-Trimethylbenzene 0.0392 0.0050 mg/kg wet 0,05000 78 69-128 3 20 1,3-Dichlorobenzene 0.0397 0.0050 mg/kg wet 0.05000 79 71-120 0.4 20 1,3-Dichloropropane 0.0456 0.0050 mg/kg wet o05000 91 75-124 2 20 1,4-Dichlorobenzene 0.0404 0o050 mg/kg wet 0.05000 81 71-123 0.4 20 2,2-Dichlompropane 0.0480 0.0050 rri wet 0o5000 96 50-142 1 20 2-Chlorotoluene 0,0394 0.0050 mg/kg wet 0.05000 79 67-124 1 20 4-Chlorotoluene oo399 0.0050 mg/kg wet 0.05000 80 71-126 1 20 4-Isopropyltoluene 0,0380 OoD50 mg/kg wet 0.05000 76 68-129 3 20 Acetone 0,114 0.050 mg/kg wet 0.1000 114 29-198 13 20 Benzene 0,0474 0.0030 mg/kg wet 0.05000 95 74-127 0.3 20 Bromobenzene 0o395 0,0050 mg/kg wet 0.05000 79 73-125 D.8 20 Bromochlommethane 0,0498 0.0050 mg/kg wet 0.05000 100 72-134 6 20 Bromodichloromethane 0o503 0.0050 mg/kg wet 0.05000 101 75-122 2 20 Bromoform 0.0480 0.005D mg/kg wet 0.05000 96 66-135 5 20 Bromomethane 0.0524 0,010 mg/kg wet 0.05000 105 20-180 9 20 Carbon Tetrachloride 00479 0.0050 mg/kg wet 0.05000 96 64-143 0.4 20 Chiorobenzene 0.0440 0.0050 mg/kg wet 0.05000 88 74-118 0.6 20 Chloroethane 0.0425 0.010 mg/kg wet 0.05000 85 33-149 1 20 Chloroform 0.0519 0.0050 mg/kg wet 0.05000 104 73-127 4 20 Chloromethane 0.0526 0.0050 mg/kg wet 0.05000 105 45-143 11 20 cis-1,2-Dichloroethylene 0.0494 0.0050 mg/kg wet 0.05000 99 76-134 2 20 cis-1,3-Dichlororimpylene 0.0526 0.0050 mg/kg wet - 0.05000 105 71-125 5 20 Dibromochloromethane 0.0469 0.0050 mg/kg wet 0,05000 94 73-122 3 20 Dichloroditluoromethene 0.0388 0.0050 mg/kg wet 0o5000 78 26-146 5 20 Ethylbenzene 0.0440 0.0050 mg/kg wet 0.05000 88 74A28 3 20 Isopropyl Ether 0.0494 0.0050 mg/kg wet 0.05000 99 59-159 5 20 Isopropylbenzene (Cumene) 0.0395 0.0050 mg/kg wet 0,05000 79 66-126 3 20 m,p-Xylenes 0.0889 0A10 mg/kg wet 0.1000 89 75-124 2 20 Methyl Butyl Ketone (2-Hexanone) 0.0474 0.050 mg/kg wet 0.05000 95 61-157 4 20 J Methyl Ethyl Ketone(2-Butanone) 0.0546 0A0 mg/kg wet 0,05000 1D9 63-149 11 20 J Methyl lsobutyl Ketone 0.0544 0.050 mg/kg wet 0.05000 109 57-162 6 20 Phis report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toll Free Number: 1-800/629-6364 - Fax: 7041626-0409 Page 28 of 52 ` a I Full-Servlce Analytical & 1� re ISM Environmental Solutions �'wowrtoPlEa ING Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GC/MS -Quality Control Anatyte Batch PBB0263 - 5036 Reporting Result Limit Units Level II QC Report 2127/18 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:OOPM Spike Source %REC RPD Level Result % REC Limits RPD Limit Notes LCS Cup (P8B0263-BSD1) _ _ _ Prepared & Analyzed: 02/14/18 Methylene Chloride 00504 0010 mg/kg wet 0,05000 101 74-129 5 20 Methyl-tert-Butyl Ether 0.0474 0.010 mg/kg wet 0,05000 95 70-130 2 20 Naphthalene 0o414 0.010 mg/kg wet 0.05000 83 57-157 2 20 n-Butylbenzene 0,0397 0,0050 mg/kg wet 0.05000 79 65-135 3 20 n-Propylbenzene 0.0394 0.0050 mg/kg wet 0.05000 79 67-130 4 20 o-Xylene 0.0442 0.0050 mg/kg wet 0.05000 88 74-126 2 20 sec-Bulylbenzene 0.0393 0.0050 mg/kg wet 0,05000 79 66-131 4 20 Styrene 0.0459 0.0050 mg/kg wet 0,05000 92 77-121 0.2 20 ten-Butylbenzene 0.0388 0.0050 mg/kg wet 0.05000 78 67-132 2 20 Tetmchloroethylene 0,0472 0.0050 mg/kg wet 0,05000 94 68-130 1 20 Toluene 0.0476 0.0050 mg/kg wet 0.05000 95 71-129 0.3 20 trans-1,2-Dichloroethylene 0.0472 0,0050 mg/kg wet 0.05000 94 73-132 2 20 trans-1,3-Dichloropropylene 0,0531 0.0050 mg/kg wet 0.05000 106 68-123 4 20 Tdchloroethylene 0.0492 0.0050 mg/kg wet 0,05000 98 75-133 2 20 Trichlorofluoromethane 0.0496 0.0050 mg/kg wet 0.05000 99 44-146 1 20 Vinyl acetate 0.0614 0.025 mg/kg wet 0,05000 123 85-161 8 20 Vinyl chloride 0o460 0.0050 mg/kg wet 0.05000 92 48-147 0.7 20 Xylenes, total 0.133 0.015 mg/kg wet 0.1500 89 74-126 2 20 Surrogate: 4-Bromotluorobenzene 47.4 ug/L 50.00 95 70-130 Surrogate: Dibromofluoromethane 49.0 U91L 50.00 98 64-123 Surrogate: Toluene-d8 44.6 ug/L 50.00 90 76-129 Batch PBB0397 -5035 Blank (P8B0397-BLK1) - _ Prepared & Analyzed: 02/21/18 1,1,1,2-Tetrachloroethane BRL 0o050 mg/kg wet 1,1,1-Trichlomethane BRL 0A050 mg/kg wet 1,1,2,2-Tetrachloroethane BRL 0,0050 mg/kg wet 1,1,2-Trichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethylene BRL 0.0050 mg/kg wet 1,1-Dichloropropylene BRL 0.0050 mg/kg wet 1,2,3-Trichlorobenzene BRL 0.0050 mg/kg wet 1,2,3-Trichloropropane BRL 0.0050 mg/kg wet 1,2,4-Trichlorobenzene BRL 0.0050 mg/kg wet 1,2,4-Tdmethylbenzene BRL 0.0050 mg/kg wet 1,2-Dibromcethane BRL 0.0050 mg/kg wet 1,2-Dichlorobenzene BRL 0.0050 mg/kg wet 1,2-Dichloroethane BRL 0.0050 mg/kg wet 1,2-Dichloropropane BRL 0.0050 mg/kg wet 1,3,5-Tdmethylbenzene BRL 0.0050 mg/kg wet 1,3-Dichlorobenzene BRL 0,0050 mg/kg wet 1,3-Dichloropropane BRL 0.0050 mg/kg wet 1,4-Dichlorobenzene BRL 0.0050 mg/kg wet 2,2-Dichloropropane BRL 0.0050 mg/kg wet 2-Chiorotoluene BRL 0.0050 mg/kg wet 4-Chlorotoluene BRL 0.0050 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0843 Phone: 7041629-6364- Toll Free Number. 1-800/529-6364 - Fax: 7041626-0409 Page 29 of 52 /Ni a I S � I Fvll-6clive Analytical & ' V' Environmental Solutions t°'uaoxwroxaa we Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch 138130397.5035 Reporting Result Limit Units Level II QC Report 2/27/18 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank(PSB0397-BLK1) _ Prepared & Analyzed: 02/21/18 4-Isopropyltoluene BRL 0.0050 mg/kg wet Acetone BRL 0.050 mg/kg wet Benzene BRL 0.0030 mg/kg wet Bromobenzene BRL 0.0050 mg/kg wet Bromochloromethane BRL 0.0050 mg/kg wet Bromodichloromethane BRL 0.0050 mg/kg wet Bromofonn BRL 0o050 mg/kg wet Bromomethane BRL 0.010 mg/kg wet Carbon Tetrachloride BRL 0.0050 mg/kg wet Chlorobenzene BRL 0.0050 mg/kg wet Chloroethane BRL 0.010 mg/kg wet Chloroform BRL 0.0050 mg/kg wet Chloromethane BRL 0.0050 mg/kg wet cis-1,2-Dichlocethylene BRL 0.0050 mg/kg wet cis-1,3-Dichloropropylene BRL 0.0050 mg/kg wet Dibromochloromethane BRL 0.0050 mg/kg wet Dichlorodifluoromethane BRL 0.0050 mg/kg wet Ethylbenzene BRL 0.0050 mg/kg wet Isopropyl Ether BRL 0.0050 mg/kg wet isopropylbenzene (Cumene) BRL 0,0050 mg/kg wet m,p-Xylenes BRL 0,010 mg/kg wet Methyl Butyl Ketone (2-Hexanone) BRL 0.050 mg/kg wet Methyl Ethyl Ketone (2-Butanone) BRL 0.10 mg/kg wet Methyl Isobutyl Ketone BRL 0.050 ni wet Methylene Chloride BRL 0.010 mg/kg wet Methyl-tert-Butyl Ether BRL 0.010 mg/kg wet Naphthalene BRL 0.010 mg/kg wet n-Butylbenzene BRL 0.0050 mg/kg wet n-Propylbenzene BRL 0.0050 mg/kg wet o-Xylene BRL 0.0050 mg/kg wet sec-Butylbenzene BRL 0.0050 mg/kg wet Styrene BRL 0,0050 mg/kg wet lert-Butylbenzene BRL 0.0050 mg/kg wet Tetrachloroethylene BRL 0.0050 mg/kg wet Toluene BRL 0.0050 ni wet trans-1,2-Dichlorcethylene BRL 0.0050 mg/kg wet trans-1,3-Dichloropropylene BRL 0.0050 mg/kg wet Trichloroethylene BRL 0.0050 mg/kg wet Trichlorofluoromethane BRL 0,0050 mg/kg wet Vinyl acetate BRL 0.025 mg/kg wet Vinyl chloride BRL 0,0050 mg/kg wet Xylenes, total BRL 0.015 mg/kg wet Surrogate: 4-Bromofluorobenzene 50.9 ug/L 50.00 102 70-130 Surrogate: DibromoFluoromethane 50.4 ug/L 50.00 101 84423 Surrogate: Toluene -de 505 ug/L 50.00 101 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, INC 28224-0543 Phone: 7041629-6364 - Toll Free Number: 1-8001629-6364 - Fax: 704/526-M9 Page 30 of 52 RR(\1 A //� FuliService Analyilcel & EE FR I V 1 Y 1 Environmarrcel Solutions Yumrwrox,e¢,ac Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NO 28217 Project: Truck Part Service Volatile Organic Compounds by GC/MS - Quality Control Analyte Reporting Result Limit Units Level II QC Report 2127/18 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:0013M Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P8B0397.6035 LCS (P8B0397-BS1) Prepared & Analyzed: 02/21/18 1, 1, 1,2-Tetrachloroethane 0,0514 0.0050 mg/kg wet 0.05000 103 72-115 1,1,1-Trichloroethane 0.0453 0.0050 mg/kg wet 0.05000 91 67-131 1, 1,2,2-Tetmchloroethane 0.0512 0.0050 mg/kg wet 0,05000 102 56-126 1,1,2-Tichloroethane 0.0496 0.0050 mg/kg wet 0.05000 99 70-133 1,1-Dichloroethane 0.0438 0.0050 mg/kg wet 0.05000 88 74-127 1,1-Dichloroethylene 0.0466 0.0050 mg/kg wet 0.05000 93 67-149 1,1-Dichloropropylene 0.0460 0.0050 mg/kg wet 0,05000 92 71-130 1,2,3-Trichlorobenzene 0.0496 0.0050 mg/kg wet 0,05000 99 68-130 1,2,3-Trichforopropane 0.0514 0.0050 mg/kg wet 0.05000 103 60-137 1,2,4-Trichlorobenzene 0.0490 0.0050 mg/kg wet 0.05000 98 66-125 1,2,4-Trimethylbenzene 0.0506 0.0050 mg/kg wet 0,05000 101 69-129 1,2-Dibromoethane 0.0486 0.0050 mg/kg wet 0.05000 97 70-132 1,2-Dichlorobenzene 0.0511 0,0050 mg/kg wet 0.05000 102 72-123 1,2-Dichloroethane 0.0478 0.0050 mg/kg wet 0.05000 96 68-128 1,2-Dichloropropane 0,0482 0.0050 mg/kg wet 0.05000 96 73-130 1,3,5-Trimethylbenzene 0.0494 0,0050 mg/kg wet 0.05000 99 69-128 1,3-Dichlorobenzene 0,0494 0.0050 mg/kg wet 0,05000 99 71-120 1,3-Dichloropropane 0.0497 0.0050 mg/kg wet 0,05000 99 75-124 1,4-Dichlorobenzene 0.0495 0,0050 mg/kg wet 0.05000 99 71-123 2,2-Dichloropropane 0.0429 0,0050 mg/kg wet 0.05000 86 50-142 2-Chlomtoluene 0,0487 0.0050 mg/kg wet 0,05000 97 67-124 4-Chlorotoluene 0.0501 0.0050 mg/kg wet 0.05000 100 71-126 4-Isopropyltoluene 0,0480 0.0050 mg/kg wet 0.05000 96 68-129 Acetone 0.0904 0.050 mg/kg wet 0.1000 90 29-198 Benzene 0.0470 0.0030 mg/kg wet 0,05000 94 74-127 Bromobenzene 0.0491 0.0050 mg/kg wet 0.05000 98 73-125 Bromochloromethane 0.0478 0,0050 mg/kg wet 0.05000 96 72-134 Bromodichloromethane 0.0506 0.0050 mg/kg wet 0.05000 101 75-122 Bromoform 0.0534 0.0050 mg/kg wet 0.05000 107 66-135 Bromomethane 0.0522 0.010 mg/kg wet 0.05000 104 20-180 Carbon Tetrachloride 0.0466 0.0050 mg/kg wet 0.05000 93 64-143 Chlorobenzene 0.0483 0.0050 mg/kg wet 0.05000 97 74-118 Chloroethane 0.0532 0.010 mg/kg wet 0.06000 106 33-149 Chloroform 0.0449 0.0050 mg/kg wet 0.05000 90 73-127 Chloromethane 0.0539 0.0050 mg/kg wet 0.05000 108 45-143 cis-1,2-Dichloroethylene 0.0459 0.0050 mg/kg wet 0.05000 92 76-134 cis-1,3-Dichloropropylene 0,0479 0.0050 mg/kg wet 0.05000 96 71-125 Dibromochloromethane 0.0533 0.0050 mg/kg wet 0.05000 107 73-122 Dichlorodifluoromethane 0.0463 0.0050 mg/kg wet 0.05000 93 26-146 Ethylbenzene 0.0481 0.0050 mg/kg wet 0.05000 96 74-128 Isopropyl Ether 0.0465 0.0050 mg/kg wet 0.05000 93 59-159 Isopropylbenzene (Cumene) 0.0497 0M50 mg/kg wet 0.05000 99 68-126 m,p-Xylenes 0.0963 0.010 mg/kg wet 0.1000 96 75-124 Methyl Butyl Ketone (2-Hexanone) 0.0452 0,050 mg/kg wet 005000 90 61-157 Methyl Ethyl Ketone (2-Butanone) 0.0407 0.10 mg/kg wet 0.05000 81 63-149 Methyl Isobulyl Ketone 0.0458 0.050 mg/kg wet 0.05000 92 57-162 J J J This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, INC 28224-0643 Phone: 70416294364 - Toll Free Number: 1-800/629-6364 - Fax: 7041626-0409 Page 31 of 52 R' V r V I I Fuvironmce al Solutions N EnvLonmenieluil bone �ueoenronae we Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, INC 28217 Project: Truck Part Service Volatile Organic Compounds by GCIMS - Quality Control Analyte Batch PBB0397 - 5035 Reporting Result Limit Units Level II 1 Report 2127/1B Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:OOPM Spike Source /REC RPD Level Result %REC Limits RPD Limit Notes LCS (P8130397-13SI) _ _ _- _ Prepared & Analyzed: 02/21/18 Methylene Chloride 0.0446 0.010 mg/kg wet 0.05000 89 74-129 Methyl -ten -Butyl Ether 0,0478 0.010 mg/kg wet 0,05000 96 70-130 Naphthalene 0,0490 0.010 mg/kg wet 0.05000 96 57-157 n-Butylbenzene 0,0481 0.0050 mg/kg wet 0.05000 96 65-135 n-Propylbenzene 0.0496 0,0050 mg/kg wet 0.05000 99 67-130 o-Xylene 0,0483 0.0050 mg/kg wet 0.05000 97 74-126 sec-Butylbenzene 0.0496 0.0050 mg/kg wet 0.05000 99 66-131 Styrene 0.0497 0,0050 mg/kg wet 0.05000 99 77-121 ten-Butylbenzene 0.0497 0.0050 mg/kg wet 0.05000 99 67-132 Tetrachloroethylene 0.0438 0.0050 mg/kg wet 0.05000 88 68-130 Toluene 0.0465 0.0050 mg/kg wet 0.05000 93 71-129 trans-1,2-Dichloroethylene 0,0461 0.0050 mg/kg wet 0.05000 92 73-132 trans-1,3-Dichlorcpropylene 0.0482 0.0050 mg/kg wet 0.05000 96 68-123 Tnchloroelhylene 0.0464 0.0050 mg/kg wet 0.05000 93 75-133 Trichloroflucromethane 00496 0.0050 mg/kg wet 0,05000 99 44-146 Vinyl acetate 0.0522 0.025 mg/kg wet 0,05000 104 85-161 Vinyl chloride 0.0464 0,0050 mg/kg wet 0.05000 93 48-147 Xylenes, total 0.145 0.015 mg/kg wet 0,1500 96 74-126 Surrogate: 4-Bromofluombenzene 50.4 U91L 50.00 101 70-130 Surrogate: Dibromofluoromethane 50.1 u97L 50.00 100 84-123 Surrogate: Toluene -de 51.2 ug/L 50.00 102 76-129 LCS Dup (P8130397-13SD1) _ - _ - _ Prepared & Analyzed: 02/21/18 1,1,1,2-Tetrachloroethane 0.0499 0.0050 mg/kg wet 0.05000 100 72-115 3 20 1,1,1-Trichloroethane 0.0415 0.0050 mg/kg wet 0.05000 83 67-131 9 20 1, 1,2,2-Tetrachloroethane 0.0508 0.0050 mg/k9 wet 0.05000 102 56-126 0.9 20 1,1,2-Trichloroethane 0.0490 0.0050 mg/kg wet 0.05000 98 70-133 1 20 1,1-Dichloroethane 0.0409 0.0050 mgft wet 0.05000 82 74-127 7 20 1,1-Dichloroethylene 0.0403 0.0050 mg/kg wet 0.05000 81 67-149 15 20 1,1-Dichloropropylene 0.0419 0,0050 mg/kg wet 0,05000 84 71-130 9 20 1,2,3-Tnchlorobenzene 0.0481 0.0050 mg/kg wet 0.05000 96 68-130 3 20 1,2,3-Trichloropropane 0,0511 0,0050 mg/kg wet 0.05000 102 60-137 0.5 20 1,2,4-Trichlorobenzene 0.0478 0.0050 mg/kg wet 0.05000 96 66-125 2 20 1,2,4-Trimethylbenzene 0.0481 0.0050 mg/kg wet 0.05000 96 69-129 5 20 1,2-Dibromoethane 0.0485 0,0050 mg/kg wet 0.05000 97 70-132 0.2 20 1,2-Dichlorobenzene 0.0491 0,0050 mgft wet 0.05000 98 72-123 4 20 1,2-Dichloroethane 0.0470 0.0050 mg/kg wet 0.05000 94 68-128 2 20 1,2-Dichloropropane 0.0462 0,0050 mg/kg wet 0.05000 92 73-130 4 20 1,3,5-Trimethylbenzene 0.0464 0.0050 mg/kg wet 0.05000 93 69-128 6 20 1,3-Dichlorobenzene 0.0473 0.0050 mg/kg wet 0.05000 95 71-120 4 20 1,3-Dichloropropane 0.0491 0.0050 mg/kg wet 0.05000 98 75-124 1 20 1,4Dichlorobenzene 0.0479 0.0050 mg/kg wet 0.05000 96 71-123 3 20 2,2-Dichloropropane 0,0398 0.0050 mg/kg wet 0.05000 80 50-142 7 20 2-Chlorotoluene 0.0462 0.0050 mg/kg wet 0,05000 92 67-124 5 20 4-Chlorotoluene 0.0482 0.0050 mg/kg wet 0.05000 96 71-126 4 20 4-Isopropyltoluene 0,0449 0.0050 mg/k9 wet 005000 90 68-129 7 20 Acetone 0.0902 0 050 mg/kg wet 0,1000 90 29-198 0.3 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 -Charlotte, NC 28224-0643 Phone: 704/629-6364-Toll Free Number: l-800/62"364- Fax: 7041626-0409 Page 32 of 52 'A a Full -Service Malytical a 4dP I S M I Environma nal Solutions P"umamAiea Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GCIMS - quality Control Analyte Batch P8B0397 -6036 Reporting Result Limit Units Level II QC Repoli 2127/18 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:O0PM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (PBB0397-BSDt) _ _ _ Prepared & Analyzed_: 02/21/18 Benzene 0.0448 0.0030 mg/kg wet 0.05000 90 74-127 5 20 Bromobenzene 0.0478 0.0050 mg/kg wet 0.05000 96 73-125 3 20 Bronwchloromethane 0.0468 0.0050 mg/kg wet 0.05000 94 72-134 2 20 Bromodichloromethane 0.0485 0.0050 mg/kg wet 0.05000 97 75-122 4 20 Bromoform 0,0534 0.0050 mg/kg wet 0.05000 107 66-135 0.09 20 eromomethane 0.0492 0.010 mg/kg wet 0,05000 98 20-180 6 20 Carbon Tetrachloride 0.0428 0.0050 mg/kg wet 0.05000 86 64-143 9 20 Chlorobenzene 0,0458 0,0050 mg/kg wet 0.05000 92 74-118 5 20 Chloroethane 0.0498 0.010 mg/kg wet O.o5000 100 33-149 7 20 Chlorofoml 0.0431 0,0050 mg/kg wet 0.05000 86 73-127 4 20 Chloromethane 0.0484 0.0050 mg/kg wet 0.05000 97 45-143 11 20 cis-1,2-Dichloroethylene 0.0438 0.0050 mg/kg wet a05000 88 76-134 5 20 cis-1,3-Dichloropropylene 0.0465 0.0050 mg/kg wet 0.05000 93 71-125 3 20 Dibromochloromethane 0.0522 0.0050 mg/kg wet 0,05000 104 73-122 2 20 Dichlorodifluoromethane 0.04D6 Do050 mg/kg wet D.O5000 81 26-146 13 20 Ethylbenzene 0.0448 0,0050 mg/kg wet 0.05000 90 74-128 7 20 Isopropyl Ether 0.0451 0,0050 mg/kg wet 0,05000 90 59-159 3 20 Isopropylbenzene (Cumene) 0,0468 0,0050 mg/kg wet 0.05000 94 68-126 6 20 m,p-Xylenes 0.0907 0.010 mg/kg wet 0.1000 91 75-124 6 20 Methyl Butyl Ketone (2-Hexanone) 0.0459 0,050 mg/kg wet 0.05000 92 61-157 2 20 J Methyl Ethyl Ketone (2-Butanone) 0.0421 0.10 mg/kg wet 0.05000 84 63-149 3 20 J Methyl Isobutyl Ketone 0.0464 0.050 mg/kg wet 0,05000 93 57-162 1 20 J Methylene Chloride 0.0428 0.010 mg/kg wet 0.05000 86 74-129 4 20 Methyl-tert-Butyl Ether 0.0475 0.010 mg/kg wet 0.05000 95 70-130 0.5 20 Naphthalene 0.0487 0.010 mg/kg wet 0.05000 97 57-157 0.7 20 n-Butylbenzene 0.0448 0.0050 mg/kg wet 0.05000 90 65-135 7 20 n-Propylbenzene 0.0466 0.0050 mg/kg wet 0.05000 93 67-130 6 20 o-Xylene 0.0457 0.0050 mg/kg wet 0.05000 91 74-126 6 20 sec-Butylbenzene 0.0461 0,0050 mg/kg wet oo5000 92 66-131 7 20 Styrene 0,0475 0.0050 mg/kg wet 0.05000 95 77-121 5 20 tert-Bulylbenzene 0.0462 0.0050 mg/kg wet 0.05000 92 67-132 7 20 1'etrachloroethylene 0.0403 0.0050 mg/kg wet 0.05000 81 68-130 8 20 Toluene 0.0441 0.0050 mg/kg wet 0,05000 88 71-129 5 20 trans-1,2-Dichlorcethylene 0.0432 0.0050 mg/kg wet 0,05000 Be 73-132 7 20 trans-1,3-Dichloropmpylene 0.0467 0.0050 mg/kg wet 0,05000 93 68-123 3 20 Tnchloreethylene 0.0438 0.0050 mg/kg wet 0.05000 88 75-133 6 20 Trichlorofluoromethane 0.0448 0.0050 mg/kg wet 0.05000 90 44-146 10 20 Vinyl acetate 0.0522 0.025 mg/kg wet 0.05000 1 D4 85-161 0.02 20 Vinyl chloride 0.0428 0.0050 mg/kg wet 0.05000 86 48-147 8 20 Xylenes, total 0.136 0.015 mg/kg wet 0.1500 91 74-126 6 20 Surrogate: 4-Bromofluorobenzene 50.7 ug/L 50.00 101 70-130 Surrogate: Dibmmofluoromethane 51.0 ug/L 50.00 102 64-123 Surrogate: Toluene-d8 51.5 U91L 50.00 103 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P,O. Box 240643 - Charlotte, NC 28224-0643 Phone: 704/629-6364 - Tali Free Number: 1-8001629-6364 - Fax: 7041626-0409 Page 33 of 52 A-,FR,o I S M F-HServioe Analytical & Environmental Solutions ueonnron,sa lac Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GCIMS (Medium Level) - Quality Control Reporting Result Limit Units Batch P8130410 - 5035 Level II QC Report 2/27/18 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:OOPM Spike Source %RED RPD Level Result %REC Limits RPD Limit Notes Blank (13880410-BLK7) Prepared 8 Analyzed: 02/21/18 1,1,1,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,1-Trichloroethane BRL 0.0050 mg/kg wet 1,/,2,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,2-Trichlomethane BRL 0.0050 mg/kg wet 1,1-Dichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethylene BRL 0.0050 mg/kg wet 1,1-Dichloropropylene BRL 0.0050 mg/kg wet 1,2,3-Trichlorobenzene BRL 0,010 mg/kg wet 1,2,3Jnchloropropane BRL 0.0050 mg/kg wet 1,2,4-Tdchlombenzene BRL 0.010 mg/kg wet 1,2,4-Trimethylbenzene BRL 0,0050 mg/kg wet 1,2-Dibromoethane BRL 0.0050 mg/kg wet 1,2-Dichlorobenzene BRL 0.0050 mg/kg wet 1,2-Dichloroethane BRL 0,0050 mg/kg wet 1,2-Dichloropropane BRL 0.0050 mg/kg wet 1,3,5-Trimethylbenzene BRL Dc050 mg/kg wet 1,3-Dichlorobenzene BRL 0-0050 mg/kg wet 1,3-Dichloropropane BRL 0,0050 mg/kg wet 1,4-Dichlorobenzene BRL 0.0050 mg/kg wet 2,2-Dichloropropane BRL 0.0050 mg/kg wet 2-Chloraloluene BRL 0.0050 mg/kg wet 4-Chlorotoluene BRL 0,0050 mg/kg wet 4-Isopropyltoluene BRL 0.0050 mg/kg wet Acetone BRL 0.020 mg/kg wet Benzene BRL 0.0050 mg/kg wet Bromobenzene BRL 0.0050 mg/kg wet Bromochloromethane BRL 0.0050 mg/kg wet Bromodichloromethane BRL 0.0050 mg/kg wet Bromoform BRL O.D050 mg/kg wet Bromomelhane BRL 0.010 mg/kg wet Carbon Tetrachloride BRL 0.0050 mg/kg wet Chlorobenzene BRL 0,0050 mg/kg wet Chloroethane BRL 0.010 mg/kg wet Chloroform BRL 0.0050 mg/kg wet Chloromethane BRL 0.010 mg/kg wet cis-1,2-Dichloroethylene BRL 0.0050 mg/kg wet cisA,3-Dichloropropylene BRL 0.0050 mg/kg wet Dibromochloromethane BRL 0.0050 mg/kg wet Dichlorodifluoromethane BRL 0.010 mg/kg wet Ethylbenzene BRL 0.0050 mg/kg wet Isopropyl Ether BRL 0.0050 mg/kg wet Isopropylbenzene (Cumene) BRL 0.0050 mg/kg wet m,p-Xylenes BRL 0.010 mg/kg wet Methyl Butyl Ketone (2-Hexanone) BRL 0.020 mg/kg wet Methyl Ethyl Ketone (2-Butanone) BRL 0,020 mg/kg wet Methyl Isobutyl Ketone BRL 0,020 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041629-6364- Toil Free Number: 1-800/629-6364 - Fax: 7041525-0409 Page 34 of 52 �W,M ISM n n I Full -Service Analytical & J'vf Environmental Solutions 4'umrAron��e:c Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control Analyte Batch PSB0410 -5035 Reporting Result Limit Units Level II QC Report 2/27/18 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P8B0410-BLK1) _ _ Prepared & Analyzed: 02/21/18 Methylene Chloride BRL 0.0050 mg/kg wet _ Methyl-tert-Butyl Ether BRL 0.0050 mg/kg wet Naphthalene BRL 0.010 mg/kg wet n-Butylbenzene BRL 0.0050 mg/kg wet n-Propylbenzene BRL 0,0050 mg/kg wet o-Xylene BRL 0.0050 mg/kg wet seo-Butylbenzene BRL 0.0050 mg/kg wet Styrene BRL 0.0050 mg/kg wet tert-Butylbenzene BRL 0.0050 mg/kg wet Tetrechloroethylene BRL 0.0050 mg/kg wet Toluene BRL 0.0050 mg/kg wet trans-1,2-Dicheroethylene BRL 0,0050 mg/kg wet trans-1,3-Dichloropropylene BRL 0.0050 mg/kg wet Trichioroethylene BRL 0,0050 mg/kg wet Trichlora8uoromethane BRL 0.010 mg/kg wet Vinyl acetate BRL 0.020 mg/kg wet Vinyl chloride BRL 0,010 mg/kg wet Xylenes, total BRL 0.015 mg/kg wet Surrogate: 4-Bromofluorobenzene 50.9 ug/L 50.00 102 70-130 Surrogate. Dibromofluommethane 50.4 ug/L 50.00 101 70-130 Sumogate: Toluene-d8 50.5 ug/L 50,00 101 70-130 LCS (P8B0410-BS1) _ Prepared 8 Analyzed: 02/21/18 1, 1, 1,2-Tetrachloroethane 0.0514 0.0050 mg/kg wet 0.05000 103 _ 72-115 1,1,1-Trichooroethane 0.0453 0.0050 mg/kg wet 0.05000 91 72-123 1,1,2,2-Tetrachlomethane 0.0512 0.0050 mg/kg wet 0.05000 102 62-127 1,1,2-Trichloroethane 0.0496 0.0050 mg/kg wet 0.05000 - 99 73-123 1,1-Dichloroethane 0.0438 0.0050 mg/kg wet 0.05000 68 73-119 1,1-Dichloroethylene 0.0466 0.0050 mg/kg wet 0.05000 93 59-157 1,1-Dichloropropylene 0,0460 O.p050 mg/kg wet 0.05000 92 70-129 1,2,3-Tichoorobenzene 0.0496 0.010 mg/kg wet 0.05000 99 59-133 1,2,3-Trichloropropene 0.0514 0.0050 mg/kg wet 0,05000 103 52-137 1,24-Trichlorobenzene 0.0490 0.010 mg/kg wet 0.05000 98 66-123 1,2,4-Trimethylbenzene 0.0506 0.0050 mg/kg wet 0.05000 101 69-126 1,2-Dibromoethane 0.0486 0.0050 mg/kg wet 0.05000 97 69-127 1,2-Dichlorobenzene 0,0511 0.0050 mg/kg wet 0.05000 102 70-121 1,2-Dichloroethane 0.0478 0.0050 mg/kg wet 0.05000 96 69-125 1,2-Dichloropropane 0.0482 0.0050 mg/kg wet 0.05000 96 75-124 1,3,5-Trimethylbenzene 0.0494 0.0050 mg/kg wet 0.05000 99 69-124 1,3-Dichlorobenzene 0.0494 0.0050 mg/kg wet 0.05000 99 70-121 1,3-Dichloropropane 0.0497 0.0050 mg/kg wet 0.05000 99 70-124 IA-Dichlorobenzene 0.0495 0.0050 mg/kg wet 0.05000 99 71-119 2,2-Dichloropropane 0.0429 0.0050 mg/kg wet 0.05000 86 46-154 2-Chlorotoluene 0.0487 0,0050 mg/kg wet 0,05000 97 70-121 4-Chlorotoluene 0.0501 0.0050 mg/kg wet 0.05000 100 72-126 4-Isopropyltoluene 0,0480 0.0050 mg/kg wet 0.05000 96 71-126 Acetone 0.0904 0.020 mg/kg wet 0A000 90 12-196 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toll Free Number: l-800/629-6364-Fax: 7041626-0409 Page 35 of 52 �. I S n %' I Full -Service Analytical a `, ,r 4 ' y' Environmental Solutions '6'ueonnroa,es ecc Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GCIMS (Medium Level) - Quality Control Analyte Batch PBB0410 - 5035 Reporting Result Limit Units Level II QC Report 2/27118 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P8B0410-BSI) Prepared & Analyzed: 02/21/18 Benzene 0.0470 0.0050 mg/kg wet 0.05000 94 74-123 Bromobenzene 0.0491 0.0050 mg/kg wet 0,05000 98 66-122 Bromochloromethane 0.0478 0.0050 mg/kg wet 0.05000 96 73-128 Bromodichloromethane 0,0506 0.0050 mg/kg wet 0.05000 101 76-123 Brom0form 0.0534 0.0050 mg/kg wet 0.05000 107 71-124 Bromomethane 0.0522 0.010 mg/kg wet 0,05000 104 56-145 Carbon Tetrachloride 0.0466 0.0050 mg/kg wet 0.05000 93 67-140 Chlorobenzene 0.0483 0.0050 mg/kg wet 0,05000 97 74-121 Chloroethane 0.0532 0.010 mg/kg wet 0,05000 106 64-142 Chloroform 0.0449 0.0050 mg/kg wet 0,05000 90 75-125 Chloromethane 0,0539 0.010 mg/kg wet 0.05000 108 54-132 cis-1,2-Dichloroethylene 0.0459 0.0050 mg/kg wet 0.05000 92 68-132 cis-1,3-Dichloropropylene 0.0479 0.0050 mg/kg wet 0.05000 96 75-128 Dibromochloromethane 0,0533 0.0050 mg/kg wet 0.05000 107 71-121 Dichlomdi0uoromethane 0.0463 0.010 mg/kg wet 0.05000 93 39-178 Elhyibenzene 0.0481 0.0050 mg/kg wet 0.05000 96 69-125 Isopropyl Ether 0,0465 0.0050 mg/kg wet 0.05000 93 77-123 Isopropylbenzene (Cumene) 0.0497 0.0050 mg/kg wet 0.05000 99 68-129 m,p-Xyienes oo963 0.010 mg/kg wet 0.1000 96 64-125 Methyl Butyl Ketone (2-Hexanone) 0.0452 0.020 mg/kg wet 0.05000 90 54-139 Methyl Ethyl Ketone (2-Butanone) 0.0407 0.020 mg/kg wet 0.05000 81 34-165 Methyl Isobutyl Ketone 0.0458 0.020 mg/kg wet 0.05000 92 63-130 Methylene Chloride 0.0446 0.0050 mg/kg wet 0.05000 89 65-135 Methyl-tert-Butyl Ether 0.0478 0.0050 mg/kg wet 0.05000 96 62-123 Naphthalene 0.0490 0.010 mg/kg wet 0,05000 98 58-129 n-Butylbenzene 0A481 0.0050 mg/kg wet 0.05000 96 71-126 n-Propylbenzene 0.0496 0.0050 mg/kg wet 0.05000 99 68-128 o-Xylene 0.0483 0.0050 mg/kg wet 0.05000 97 69-121 sec-Butylbenzene OA496 0.0050 mg/kg wet 0.05000 99 71-128 Styrene 0.0497 0,0050 mg/kg wet 0.05000 99 67-129 tert-Butylbenzene 0.0497 0.0050 mg/kg wet 0.05000 99 71-126 Tetrachloroethylene 0.0438 0.0050 mg/kg wet 0,05000 88 71-124 Toluene 0,0465 0.0050 mg/kg wet 0.05000 93 74-122 trans-1,2-Dichloroethylene 0.0461 0.0050 ni wet 0.05000 92 69-129 trans-1,3-Dichloropropylene 0.0482 0.0050 mg/kg wet 0.05000 96 74-127 Trichloroethylene 0o464 0.0050 mg/kg wet 0.05000 93 68-133 Trichloro8uoromethene 0.0496 0.010 mg/kg wet 0.05000 99 60-138 Vinyl acetate 0.0522 0.020 mg/kg wet 0.05000 104 14-179 Vinyl chloride 0.0464 0.010 mg/kg wet 0.05000 93 69-135 Xylenes, total 0.145 0.015 mg/kg wet 0.1500 96 74-126 Surrogate: 4-Bromofluorobenzene 50.4 U91L 50.00 101 70-130 Surrogate: Dlbromofluoromethene 50.1 ug/L 50,00 100 70-130 Surrogate: Toluen"S 51.2 U91L 50.00 102 70-130 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 704/629.6364-Toll Free Number: l-800/529-6364- Fax: 7041626-0409 Page36Df52 A R FAnalyrlcalIt/rw'x I S M I Enull-Service vironmental Solutions ��i�"womronisa,xa Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GCIMS (Medium Level) - Quality Control Analyte Batch P8B0410-5035 Reporting Result Limit Units Level II QC Report 2127/18 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:00PIA Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS pop (P880410-BSD1) Prepared & Analyzed: 02/21/18 11,1,2-Tetrachloroethane 0,0499 0.0050 mg/kg wet 0,05000 100 72-115 3 20 1,1,1-Trichooroethane 0,0415 0.0050 mg/kg wet 0,05000 83 72-123 9 20 1,1,2,2-Tetmchloroethane 0.0508 0.0050 mg/kg wet 0,05000 102 62-127 0.9 20 1, 1,2-Trichloroethane 0.0490 0.0050 mg/kg wet 0.05000 98 73-123 1 20 1,1-Dichloroethane 0.0409 0.0050 mg/kg wet 0.05000 82 73-119 7 20 1,1-Dichloroethylene 0.0403 0,0050 mg/kg wet 0.05000 81 59-157 15 20 1,1-Dichloropropylene 0.0419 0.0050 mg/kg wet 0,05000 84 70-129 9 20 1,2,3-Tnchlorobenzene 0.0481 0.010 mg/kg wet 0.05000 96 59-133 3 20 1,2,3-Trichloropropane 0.0511 0.0050 mg/kg wet 0.05000 102 52-137 0.5 20 1,2,4-Tdchlorobenzens 0.0478 0.010 ni wet 0.05000 96 66-123 2 20 1,2,4-Trimethylbenzene 0.0481 0.0050 mg/kg wet 0,05000 96 69-126 5 20 1,2-Ditimmoethane 0,0485 0.0050 mg/kg wet 0.05000 97 69-127 0.2 20 1,2-Dichlorobenzene 0.0491 0,0050 mg/kg wet 0.05000 98 70-121 4 20 1,2-Dichloroethane 0.0470 0.0050 mg/kg wet 0.05000 94 69-125 2 20 1,2-Dichloropropane 0.0462 0.0050 mg/kg wet 0.05000 92 75-124 4 20 1,3,5-Trimethylbenzene 0.0464 0.0050 mg/kg wet 0.05000 93 69-124 6 20 1,3-Dichlorobenzene 0,0473 0.0050 mg/kg wet 0.05000 95 70-121 4 20 1,3-Dichloropropane 0.0491 0,0050 mg/kg wet O.05000 go 70-124 1 20 1,4-Dichlorobenzene 0.0479 0.0050 mg/kg wet 0.05000 96 71-119 3 20 2,2-Dichloropropane 0.0398 0.0050 nrl wet 0.05000 80 46-154 7 20 2-Chlorotoluene 0.0462 0.0050 mg/kg wet 0,05000 92 70-121 5 20 4-Chlorotoluene 0.0482 0.0050 mg/kg wet 0.05000 96 72-126 4 20 4-Isopropyltoluene 0.0449 0.0050 mg/kg wet 0o5000 90 71-126 7 20 Acetone 0.0902 0.020 mg/kg wet 0.1000 g0 12-196 0.3 20 Benzene 0.0448 0.0050 mg/kg wet 0.05000 90 74-123 5 20 Bromobenzene 0o478 0.0050 mg/kg wet 0,05000 96 66-122 3 20 Bromochloromethane O.0468 0.0050 mg/kg wet 0,05000 94 73-128 2 20 Bromodichloromethane 0o,185 0.0050 mg/kg wet o05000 97 76-123 4 20 Bromoform 0.0534 0.D050 mg/kg wet 0.05000 107 71-124 0.09 20 Bromomethane 0.0492 0.010 mg/kg wet 0.05000 98 56-145 6 20 Carbon Tetrachloride O.D428 0.0050 mg/kg wet 0.05000 86 67-140 9 20 Chlorobenzene 0.0458 0.0050 mg/kg wet 0.05000 92 74-121 5 20 Chloroethane 0.0498 0.010 mg/kg wet 0.05000 100 64-142 7 20 Chloroform 0.0431 0.0050 mg/kg wet 0.05000 86 75-125 4 20 Chloromethane 0.D484 0.010 mg/kg wet 0.05000 97 54-132 11 20 cis-1,2-Dichloroethylene 0,0438 0.0050 mg/kg wet 0,05000 88 66-132 5 20 cis-1,3-Dichloropropylene 0.0465 0.0050 mg/kg wet 0.05000 93 75-128 3 20 Dibromochloromethane 0,0522 Oo050 mg/kg wet 0.05000 104 71-121 2 20 Dichiomdifluoromethane 0.0406 0.010 mg/kg wet 0.05000 81 39-178 13 20 Ethylbenzene Do,148 0.0050 mg/kg wet 0.05000 90 69-125 7 20 Isopropyl Ether 0.0451 0.0050 mg/kg wet 0.05000 90 77-123 3 20 Isopropylbenzene(Cumene) 0.0468 0.0050 mg/kg wet 0,05000 94 68-129 6 20 m,p-Xylenes 0.0907 0.010 mg/kg wet 0.1000 91 64-125 6 20 Methyl Butyl Ketone (2-Hexanone) 0.0459 0o20 mg/kg wet 0.05000 92 54-139 2 20 Methyl Ethyl Ketone (2-Butenone) 0.0421 0.020 mg/kg wet 0.05000 84 34-165 3 20 Methyl Isobutyl Ketone 0.0464 0,020 mg/kg wet 0.05000 93 63-130 1 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O- Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364- Toll Free Number: 1-8001629-6364 - Fax: 7041625-0409 Page 37 of 52 �Ra I S M Full -Service Analy[Icai A Environmental a"ca$ I `✓ueonmomw. ixc Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Organic Compounds by GCIMS (Medium Level) - Quality Control Reporting Result Limit Units Batch PBB0410 - 5035 Level II QC Report 2127/18 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes _LCS Cup (PBB0410-BSDt) _ _ Prepared & Analyzed: 02/21/18 Methylene Chloride 0.0428 0.0050 mg/kg wet 0,05000 86 65-135 4 20 Methyl-lert-Butyl Ether 0.0475 0.0050 mg/kg wet 0.05000 95 62-123 0.5 20 Naphthalene 0.0487 0,010 mg/kg wet 0.05000 97 58-129 0.7 20 n-Butylbenzene 0.0448 0.0050 mg/kg wet 0.05000 90 71-126 7 20 n-Propylbenzene 00466 0.0050 mg/kg wet 0.05000 93 68-128 6 20 o-Xylene 0.0457 0.0050 mg/kg wet 0.05000 91 69-121 6 20 sec-Butylbenzene 0.0461 0.0050 mg/kg wet 0,05000 92 71-128 7 20 Styrene 0.0475 0.0050 mg/kg wet 0,05000 95 67-129 5 20 tert-Butylbenzene 0.0462 0.0050 mg/kg wet 0.05000 92 71-126 7 20 Tetrachloroethylene 0.0403 0.0050 mg/kg wet 0.05000 81 71-124 8 20 Toluene 0.0441 0,0050 mg/kg wet 0,05000 88 74-122 5 20 trans-1,2-Dichloroethylene 0.0432 0.0050 mg/kg wet 0.05000 86 69-129 7 20 trans-1,3-Dichloropropylene 0.0467 0.0050 mg/kg wet 0.05000 93 74-127 3 20 Trichloroethylene 0.0438 0.0050 mg/kg wet 0,05000 88 68-133 6 20 Trichlomfluoromethane 0.0448 0.010 mg/kg wet 0.05000 90 60-138 10 20 Vinyl acetate 0.0522 0.020 mg/kg wet 0.05000 104 14-179 0.02 20 Vinyl chloride 0,0428 0.010 mg/kg wet 0.05000 86 69-135 8 20 Xylenes, total 0,136 0.015 mg/kg wet 0.1500 91 74-126 6 200 Surrogate: 4-Bromoftuorobenzene 50.7 ug/L 50,00 101 70430 Surrogate: Dibromofluoromethane 51.0 ug/L 50.00 102 70-130 Surrogate: Toluene-0 51.6 ug/L 50,00 103 70-130 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 -Charlotte, NC 28224-0643 Phone: 704/529-6364-Toll Free Number: 1-8001629-6364 - Fax: 7041626-0409 Page 38 of 52 R I S M I Fuil-fiervice A aly icel & Environmental Solutions LNa0Mleala3 �xc Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semivolattle Organic Compounds by GCIMS - Quality Control Reporting Result Limit Units Batch PBB0345 - 3546 Level II QC Report 2/27/18 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank(PBB0345-BLK1) Prepared & Analyzed: 02/19/18 1,2,4-Trichlorobenzene BRL 0.33 _ mg/kg wet 1,2-Dichlorobenzene BRL 0,33 mg/kg wet 1,3-Dichlorobenzene BRL 0,33 mg/kg wet 1,4-Dichlorobenzene BRL 0.33 mg/kg wet 1-Methylnaphthalene BRL 0.33 mg/kg wet 2,4,6-Trichlorophenol BRL 0.33 mg/kg wet 2,4-Dichlorophenol BRL 0.33 mg/kg wet 2,4-Dimethylphenoi BRL 0.33 mg/kg wet 2,4-Dinitrophenol BRL 0.33 mg/kg wet 2,4-Dinitrotoluene BRL 0,33 mg/kg wet 2,6-Dinitrotoluene BRL 0.33 mg/kg wet 2-Chloronaphthalene BRL 0,33 mg/kg wet 2-Chlorophenol BRL 0.33 mg/kg wet 2-Methylnaphthalene BRL 0,33 mg/kg wet 2-Methylphenol BRL 0.33 mg/kg wet 2-Nitrophenol BRL 0.33 mg/kg wet 3,3'-Dichlorobenzidine BRL 0.33 mg/kg wet 3/4-Methylphenol BRL 0.33 mg/kg wet 4,6-Dinitm-2-methylphenol BRL 0.33 mg/kg wet 4-Bromophenyl phenyl ether BRL 0.33 mg/kg wet 4-Chloro-3-methylphenol BRL 0.33 mg/kg wet 4-Chloroaniline BRL 0.33 mg/kg wet 4-Chlorophenyl phenyl ether BRL 0.33 mg/kg wet 4-Nitrophenol BRL 0.33 mg/kg wet Acenaphthene BRL 0.33 mg/kg wet Acenaphthylene BRL o33 mg/kg wet Anthracene BRL 0.33 mg/kg wet AZobenzene BRL 0.33 mg/kg wet Benzoia)anthracene BRL 0.33 mg/kg wet Benzo(a)pyrene BRL 0.33 mg/kg wet Benzo(b)0uoranthene BRL 0.33 mg/kg wet Benzo(g,h,i)perylene BRL 0.33 mg/kg wet Benzo(k)0uomnthene BRL 0.33 mg/kg wet Benzoic Acid BRL 0.33 mg/kg wet Benzyl alcohol BRL 0.33 mg/kg wet bis(2-Chloroethoxy)methane BRL 0.33 mg/kg wet Bis(2-Chloroethyl)ether BRL 0.33 mg/kg wet Bis(2-chloroisopropyl)ether BRL 0.33 mg/kg wet Bis(2-Ethylhexyl)phthalate BRL 0.33 mg/kg wet Butyl benzyl phthalate BRL 0.33 mg/kg wet Chrysene BRL 0.33 mg/kg wet Dibenzo(eh)anthrecene BRL 0.33 mg/kg wet Dibenzofuran BRL 0.33 mg/kg wet Diethyl phthalate BRL 0.33 mg/kg wet Dimethyl phthalate BRL 0.33 mg/kg wet Di-n-butyl phthalate BRL 0.33 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 77-1 Phone: 704/629-0364- Toll Free Number: "00/529-6364-Fax: 704/526-04H Page 39 of 52 s T R Full -Service Analytical & ' V f Environmental Solutions uacanronse ma Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, INC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GC/MS - Quality Control Analyle Batch MOM - 3546 Reporting Result Limit Units Level II QC Report 2/27/18 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P880345-BLK1) Prepared & Analyzed: 02/19/18 Di-n-octyl phthalate BRL 0,33 mg/kg wet Fluoranthene BRL 0.33 mg/kg wet Fluorene BRL 0.33 mg/kg wet Hexachlorobenzene BRL 0.33 mg/kg wet Hexachlorobutadiene BRL 0.33 mg/kg wet Hexachlorocyclopentadiene BRL 0.33 mg/kg wet Hexachloroethane BRL 0.33 mg/kg wet Indeno(1,2,3-cd)pyrene BRL 0.33 mg/kg wet Isophorone BRL 0.33 mg/kg wet Naphthalene BRL 0.33 mg/kg wet Nitrobenzene BRL 0.33 mg/kg wet N-Nitroso-di-n-propylarnme BRL 0,33 mg/kg wet N-Nimosodiphenylarnme BRL 0,33 mg/kg wet Pentachlorophenol BRL 0.33 mg/kg wet Phenanlhrene BRL 0.33 mg/kg wet Phenol BRL 0.33 mg/kg wet Pyrene BRL 0.33 mg/kg wet Surrogate: 2,4,6-Tdbromophenol 2.96 mg/kg wet 3.333 89 39-132 Surrogate: 2-Fluorobiphenyl 1.51 mg/kg wet 1.667 90 44415 Surrogate: 2-Fluorophenol 271 mg/kg wet 3.333 81 35-115 Surrogate: Nitrobenzene-d5 1.35 mg/kg wet 1.667 81 37-122 Surrogate: Phenol-d5 2.76 mg/kg wet 3.333 63 34-121 Surrogate. Terphenyl-dl4 1.48 mg/kg wet 1.667 89 54-127 LCS (PRB0345-BSI) _ _ _ Prepared & Analyzed: 02/19/18 1,2,4-Trichlorobenzene 1.03 0.33 mglkg wet 1.667 62 34-118 1,2-Dichlorobenzene 1.07 0.33 mg/kg wet 1,667 64 33-117 1,3-Dichlorobenzene 1.02 0.33 mg/kg wet 1,667 61 30-115 1,4-Dichlorobenzene 1A3 0.33 mg/kg wet 1.667 62 31-115 1-Methylnaphthalene 1.19 0.33 mg/kg wet 1.667 72 40-119 2,46-Tnchlorophenol 1.34 0.33 mg/kg wet 1,667 80 39-126 2,4-Dichlorophenol 1.16 0.33 mg/kg wet 1,667 70 40-122 2,4-Dimethylphenol 1.34 0.33 mg/kg wet 1.667 80 30-127 2,4-Dinitrophenol 1.59 0.33 mg/kg wet 1.667 96 27-129 2,4-Dinitrotoluene 1.04 0,33 mg/kg wet 1667 63 48-126 2,6-Dinitrotoluene 1.40 0.33 mg/kg wet 1.667 84 46-124 2-Chloronaphthalene 1.27 0.33 mg/kg wet 1.667 76 41-114 2-Chlorophenol 1.22 0.33 ri wet 1.667 73 34-121 2-Methylnaphthalene 1,14 0.33 mg/kg wet 1.667 68 38-122 2-Methylphenol 1,29 0.33 mg/kg wet 1.667 78 32-122 2-Nitrophenol 1.08 0.33 mg/kg wet 1,667 65 36-123 3,3'-Dichlorobenzidine 1,40 0.33 mg/kg wet 1.667 84 22-121 3/4-Methylphenol 1,25 0.33 mg/kg wet 1.667 75 34-119 4,6-Dinitro-2-methylphenol 1,44 0.33 mg/kg wet 1.667 87 29-132 4-Bromophenyl phenyl ether 1.30 0.33 mg/kg wet 1 S67 78 46-124 4-Chlcro-3-methylphenol 1.23 0.33 mg/kg wet 1.667 74 45-122 4-CMoroaniline 1.12 0.33 mg/kg wet 1,667 67 17-106 This report should not be reproduced, except in its entirety, without the written consent of Prism Lab0Mtories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629.6364-Toll Free Number: 1-8001629-6364 - Fax: 7041626-0409 Page 40of52 &&Mua I S M I run-Servlee Analytical & Environmental solutions :ueouroxisx ac Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GC/MS - Quality Control Reporting Result Limit Units Batch P8B0345 -3546 Level II QC Report 2/27/18 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:00PM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P8B0345-BSI) Prepared 8 Analyzed: 02/19/18 4-Chlorophenyl phenyl ether 1.34 0.33 mg/kg wet 1,667 80 45-121 4-Nitrophenol 1.51 0.33 mg/kg wet 1.667 91 30-132 Acenaphthene T34 0.33 mg/kg wet 1.667 81 40-123 Acenaphthylene 1.42 0,33 mg/kg wet 1.667 85 32-132 Anthracene 1.49 0.33 mg/kg wet 1.667 90 47-123 Azobenzene 1.41 0.33 mg/kg wet 1.667 84 39-125 Benzo(a)anthmcene 1,45 0.33 mg/kg wet 1667 87 49-126 Benzo(a)pyrone 1 43 0,33 mg/kg wet 1,667 86 45-129 Senzo(b)fluoranthene 1AS 0.33 mg/kg wet 1.667 89 45-132 Benzo(g,h,i)perylene 1.28 0.33 mg/kg wet 1.667 77 43-134 Benzo(k)fluoranthene 1.32 0.33 mg/kg wet 1.667 79 47-132 Benzoic Acid 1.23 0.33 mg/kg wet 1.667 74 10-83 Benzyl alcohol 1A1 0.33 mg/kg wet 1.667 67 29-122 bis(2-Chforoethoxy)methane 1.12 0.33 mg/kg wet 1a67 67 36-121 Bis(2-Chloroethyl)ether 1.12 0.33 mg/kg wet 1,667 67 31-120 Bis(2-chloroisopropyl)ether 1.05 0.33 mg/kg wet 1.667 63 33-131 Sis(2-Ethylhexyl)phthalate 1As 0.33 mg/kg wet 1a67 90 51-133 Butyl benzyl phthalate 1,44 0.33 mg/kg wet 1.667 86 48-132 Chrysene 1.48 0.33 mg/kg wet 1.667 89 50-124 Dibenzo(a,h)anthracene 1.78 0.33 mg/kg wet 1.667 107 45-134 Dibenzo/uran T32 0.33 mg/kg wet 1.687 79 44-120 Diethyl phthafate 1.34 0.33 mg/kg wet 1.667 81 50-124 Dimethyl phthalate 1.31 0.33 mg/kg wet 1.667 79 48-124 Di-n-butyl phthalate 1.48 0.33 mg/kg wet 1.667 89 51-128 Di-n-octyl phthalate 1.56 0.33 mg/kg wet 1.667 93 45-140 Fluomnthene 1.50 0.33 mg/kg wet 1.667 90 50-127 Fluorene 1.39 0.33 mg/kg wet 1.667 83 43-125 Hexachlorobenzene 1.27 0.33 mg/kg wet 1.667 76 45-122 Hexachlorobutadiene 1.03 0.33 mg/kg wet 1.667 62 32-123 Hexachlorooyclopentadiene 1.23 0.33 mg/kg wet 1.667 74 32-117 Hexachlomethane 1.02 0.33 mg/kg web 1a67 61 28-117 Indeno(1,2,3-cd)pyrene 138 0.33 mg/kg wet 1.667 83 45-133 Isophorone 1.10 0.33 mg/kg wet 1.667 66 30-122 Naphthalene 1.09 0,33 mg/k9 wet 1.667 66 35-123 Nitrobenzene 0.946 0.33 mg/kg wet 1.667 57 34-122 N-Nitroso-di-n-propylamine 1.25 0.33 mg/kg wet 1.667 75 36A20 N-Nitrosodiphenylamine 1.69 0.33 mg/kg wet 1,667 101 38-127 Pentachlorophenol 1.94 0.33 mg/kg wet 1.667 116 25-133 Phenanthrene 1.50 0.33 mg/kg wet 1,667 90 50-121 Phenol 1.27 0.33 mg/kg wet 1.667 76 34-121 Pyrene 146 0.33 mg/kg wet 1,667 87 47-127 Surrogate: 2,4,6-Tribromophenot 2.87 mg/kg wet 3.333 86 39-132 Surrogate: 2-Flucrobiphenyl 1,39 mg/kg wet 1.667 84 44-115 Surrogate: 2-Fluorophenol 2.61 mg7kg wet 3.3a3 75 35-115 Surrogate: Nitrobenzene-0 1,08 mg/kg wet 1.667 65 37-122 Surrogate: PhenoW5 2.54 mg/kg wet 3.333 76 34-121 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toll Free Number: 1-8001629-6364 - Fax: 704/525-g409 Page 41 Of rJ2 �P R I S M I Environments] ry en s] Solutions E Environmental 6olvtlons 'i"ueosmusies me Geoscience Group Attn: Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P860345 - 3546 Reporting Result Limit Units Level 11 QC Report 2/27/18 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (PSB0345-BS1) Prepared & Analyzed: 02/19/18 Surrogate: Terphenyl-d14 1.45 mgdrg wet 1.667 87 54-127 LCS Dup (P8B0345-BSD1) Prepared & Analyzed: 02/19/18 1,2,4-Trichlorobenzene 1.02 0.33 mg/kg wet 1.667 61 34-118 0.9 20 1,2-Dichlorobenzene 1.05 0.33 mg/kg wet 1.667 63 33-117 1 20 1,3-Dichlorobenzene 1.04 0.33 mg/kg wet 1.667 62 30-115 2 20 1,4-Dichlorobenzene 1.02 C33 mg/kg wet 1.667 61 31-115 1 20 1-Melhylnaphthalene 1.17 0.33 mg/kg wet 1,667 70 40-119 2 20 2,4,6-Trichlorophenol 1.32 0,33 mg/kg wet 1.667 79 39-126 1 20 2,4-Dichlorophenol 1.15 0.33 mg/kg wet 1.667 69 40-122 0.9 20 2,4-Dimethylphenol 1.31 0.33 mg/kg wet 1.667 78 30-127 2 20 2,4-Dinitrophenol 1.50 0,33 mg/kg wet 1.667 90 27-129 6 20 2,4-Dinitrotoluene 1.01 0.33 mg/kg wet 1.667 61 48-126 4 20 2,6-Dinitrotoluene 1,35 0.33 mg/kg wet 1.667 81 46-124 4 20 2-Chloronaphthalene 125 0.33 mg/kg wet 1S67 75 41-114 2 20 2-Chlorophenol 1,22 0.33 mg/kg wet 1.667 73 34-121 0.2 20 2-Methylnaphthalene 1.12 0.33 mg/kg wet 1.667 67 38-122 1 20 2-Melhylphenol 1 30 0.33 mg/kg wet 1.667 78 32-122 0.4 20 2-Nilrophenol 1.08 0.33 mg/kg wet 1.667 65 36-123 0.8 20 3,3'.Dichlorobenzidine 1,34 0.33 mg/kg wet 1.667 80 22-121 4 20 3/4-Methylphenol 1.22 0,33 mg/kg wet 1.667 73 34-119 2 20 4,6-Dinitro-2-methylphenol 1.39 0.33 mg/kg wet 1,667 83 29-132 4 20 4-Bromophenyl phenyl ether 1.26 0.33 mg/kg wet 1.667 75 46-124 3 20 4-Chloro-3-methylphenol 1.21 0,33 mg/kg wet 1.667 73 45-122 2 20 4-Chioroaniline 1.09 0.33 mg/kg wet 1.667 66 17-106 3 20 4-Chlorophenyl phenyl ether 1.30 0.33 mg/kg wet 1,667 78 45-121 3 20 4-Nitrophenol 1.48 0.33 mg/kg wet 1.667 89 30-132 2 20 Acenaphthene 1.32 0.33 mg/kg wet 1,667 79 40-123 2 20 Acenaphthylene 1.40 0,33 mg/kg wet 1.667 84 32-132 1 20 Anthrecene 1.46 0.33 mg/kg wet 1.667 87 47-123 3 20 Azobenzene 1.40 0.33 mg/kg wet 1.667 84 39-125 0.7 20 Benzo(a)anthnecene 1.40 0.33 mg/kg wet 1,667 84 49-126 3 20 Benzo(a)pyrene 1.38 033 mg/kg wet 1.667 83 45-129 4 20 Benzo(b)fluoranthene 1.38 0.33 ni wet 1,667 83 45-132 7 20 Benzo(g,h,i)perylene 1.24 0.33 mg/kg wet 1.667 74 43-134 3 20 Benzo(k)fluoranthene 1.33. 0.33 mg/kg wet 1.667 80 47-132 0.3 20 Benzoic Acid 1C8 0.33 mg/kg wet 1.667 65 10-83 12 20 Benzyl alcohol 1.10 0.33 mg/kg wet 1,667 66 29-122 0.9 20 bis(2-Chloroethoxy)methane 1.07 0.33 mg/kg wet 1.667 64 36-121 4 20 Bis(2-Chloroethyoether 0.976 0.33 mg/kg wet 1.667 59 31-120 14 20 Bis(2chl0roisopr0pyl)ether 1.04 0.33 mg/kg wet 1,667 62 33-131 0.6 20 Bis(2-Ethylhexyl)phthalate 1.46 0,33 mg/kg wet 1.667 87 51-133 3 20 Butyl benzyl phthalate 1.37 0.33 mg/kg wet 1.667 82 48-132 5 20 Chrysene 1.40 0.33 mg/kg wet 1.667 84 50-124 6 20 Dibenzo(a,h)snthmcene 1.57 0,33 mg/kg wet 1.667 94 45-134 13 20 Dibenzofuran 1.31 0.33 mg/kg wet 1.667 78 44-120 1 20 Diethyl phthalate 1.31 0.33 mg/kg wet 1.667 78 50-124 3 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, INC 28224-0643 Phone: 704/629-6364 - Toll Free Number: t-8001529-6364- Fax: 704/525-0409 Page42Df52 slk p n I F ncnivlce Analytical a ' V' Envinnmental Solutions �L$'ueoavoxas we Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GC/MS -Quality Control Analyte Batch PBB0345 - 3546 Reporting Result Limit Units Level II QC Report 2/27118 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:00PM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Quit (P8130345-BSD1) Prepared & Analyzed: 02/19/18 Dimethyl phthalate 1.28 0.33 mg/kg wet 1.667 77 48-124 2 20 Di-n-butyl phthalate 1.43 0.33 mg/kg wet 1.667 86 51-128 3 20 Di-n-octyl phthalate 1.52 0.33 mg/kg wet 1.667 91 45-140 3 20 Fluoranthene 1.48 0.33 mg/kg wet 1,667 89 50-127 1 20 Fluorene 1.37 0.33 mg/kg wet 1,667 82 43-125 1 20 Hexachlorobenzene 1.19 0.33 mg/kg wet 1.667 71 45-122 6 20 Hexachlorobutediene 1,03 0.33 mg/kg wet 1,667 62 32-123 0.2 20 Hexachlorocyclopentadiene 1.17 0,33 mg/kg wet 1.667 70 32-117 4 20 Hexachloroethane 1.02 0.33 mg/kg wet 1.667 61 28-117 0.7 20 Indeno(1,2,3-cd)pyrene 1.34 0.33 mg/kg wet 1.667 81 45-133 3 20 Isophorone 1.08 0.33 mg/kg wet 1,667 65 30-122 1 20 Naphthalene 1.09 0.33 mg/kg wet 1,667 65 35-123 0.6 20 Nitrobenzene 0.946 0.33 mg/kg wet 1,667 57 34-122 0 20 N-Nitmso-di-n-propylamine 1.25 0.33 mg/kg wet 1,667 75 36-120 0.1 20 N-Nitrosodiphenylamine 1.64 0.33 mg/kg wet 1.667 98 38-127 3 20 Pentachlorophenol 1-85 0.33 mg/kg wet 1,667 111 25-133 5 20 Phenanthrene 1.45 0.33 mg/kg wet 1.667 - 87 50-121 3 20 Phenol 1.26 0,33 mg/kg wet 1,667 76 34-121 0.5 20 Pyrene 1.44 0,33 mg/kg wet 1,667 87 47-127 0.9 20 Surrogate: 2,4,6-Tribromophenol 2.69 mg/kg wet 3.333 81 39-132 Surrogate: 2-Fluombiphenyl 1.33 mg/kg wet 1.667 80 44-116 Surrogate: 2-Fluomphenol 2.43 mg/kg wet 3,333 73 35-115 Surrogate: Nitrobenzene-d5 1.05 mg/kg wet 1.667 63 37-122 Surrogate: Phenol-d5 2.45 mg/kg wet 3.333 73 34-121 Surrogate: Terphenybd14 1.35 mg/kg wet 1,667 81 64-127 Matrix Spike (P8B0345-MS1) Source: 8020233-01 Prepared: 02/19/18 Analyzed: 02/20/18 1,2,4-Trichlombenzene 2.58 0.45 mg/kg dry 2.297 BRL 112 34-1 88 1,2-Dichlorbenzene 1.38 0.45 mg/kg dry 2.297 BRL 60 33-117 1,3-Dichlombenzene 1.34 0,45 mg/kg dry 2.297 BRL 58 30-115 1,4-Dichlombenzene 1.29 0.45 mgtkg dry 2,297 BRL 56 31-116 1-Methylnaphthalene 45900000 0.45 mg/kg dry 2.297 20.3 NR 40-11P M 2,4,6-Trichlorophenol 1.73 0.45 mg/kg dry 2,297 BRL 75 39-126 2,4-Dichlomphenol 3,50 0.45 mg/kg dry 2297 BRL 153 40-122 M 2,4-Dimethylphenol 5.33 0,45 mg/kg dry 2.297 BRL 232 30-127 NI 2,4-DinitrophenDl 1.81 0.45 mg/kg dry 2.297 BRL 79 27-129 2,4-Dinitmtoluene 1.26 0.45 mg/kg dry 2.297 BRL 55 48-126 2,6-Dinitrotoluene 1.69 0,45 mg/kg dry 2.297 BRL 73 46-124 2-Chloronaphthalene 0.935 0.45 mg/kg dry 2.297 BRL 41 41-114 2-Chlorophenol 1.32 0.45 mg/kg dry 2.297 BRL 57 34-121 2-Methylnaphthalene 45900000 0.45 mg/kg dry 2.297 30.8 NR 38-122 M 2-Methylphenol 1.62 0.45 mg/kg dry 2,297 BRL 70 32-122 2-Nilmphenol 4.05 0,45 mg/kg dry 2.297 BRL 176 36-123 M 3,3'-Dichlorobemidine 0.825 0.45 mg/kg dry 2.297 BRL 36 22-121 3/4-Methylphenol 1 36 0.45 mglkg dry 2.297 BRL 59 34-119 4,6-DinitrD-2-methylphenol 1.53 0.45 mg/kg dry 2.297 BRL 67 29-132 4-Bromophenyl phenyl ether 1.57 0.45 mg/kg dry 2.297 BRL 68 46-124 This report should not be reproduced, except in its entirety, without the written consent of Prism laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 -Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1-800/529.6364 - Fax: 7041626-0409 Page 43 Ot 52 IWRfSM I Fufl Service Analvtical8 Environmental Solutions Anroe,[41Nc Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P8BO345 - 3646 Reporting Result Limit Units Level II QC Report 2/27/18 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Matrix Spike (128130346-M51) Source: 8020233-01 Prepared: 02/19/18 Analyzed: 02/20/18 4-Chloro-3-methylphenol 420 0.45 mg/kg dry 2.297 BRL 183 45-122 M 4-Chloroaniline 1,40 0.45 mg/kg dry 2.297 BRL 61 17-106 4-Chlorophenyl phenyl ether 1.91 0.45 mg/kg dry 2.297 BRL 53 45-121 4-Nitrophenoi 1 79 0.45 mg/kg dry 2,297 BRL 78 30-132 Acenaphthene 1.84 0.45 mg/kg dry 2,297 BRL 80 40-123 Acensphthylene 1.99 0.45 mg/kg dry 2.297 BRL 86 32-132 Anthracene 1.90 OAS mg/kg dry 2.297 BRL 83 47-123 Azobenzene 1.62 045 mg/kg dry 2.297 BRL 70 39-125 Benzo(a)anthracene 1.79 0.45 mg/kg dry 2.297 BRL 78 49-126 Benzo(a)pyrene 1.76 0.45 mg/kg dry 2.297 BRL 76 45-129 Benzo(b)fluoranthene 1.76 0.45 mg/kg dry 2.297 BRL 77 45-132 Benzo(g,h,i)perylene 1,53 0.45 mg/kg dry 2.297 BRL 67 43-134 Benzo(k)fluoranthene 1.72 0.45 mg/kg dry 2.297 BRL 75 47-132 Benzoic Acid 2A7 0.45 mg/kg dry 2,297 BRL 95 10-63 M Benzyl alcohol 1,34 0,45 mg/kg dry 2.297 BRL 58 29-122 bis(2-Chloroethoxy)methene 2.29 0.45 mg/kg dry 2,297 BRL 100 36-121 Bis(2-Chloroethyi)ether 2,33 0.45 mg/kg dry 2,297 BRL 102 31-120 Bis(2-chlcroisopropyl)ether 1.08 0,45 mg/kg dry 2.297 BRL 47 33-131 Bis(2-Ethylhexyl)phthalate 1.84 0.45 mg/kg dry 2,297 BRL 80 51-133 Butyl benzyl phthalate 1.75 0,45 mg/kg dry 2.297 BRL 76 48-132 Chrysene 2.17 0.45 mg/kg dry 2.297 BRL 94 50-124 Dibenzo(a,h)anthrecene 2.60 0.45 mg/kg dry 2.297 BRL 113 45-134 Dibenzofuren 2.14 0.45 mg/kg dry 2.297 BRL 93 44-120 Diethyl phthalate 1.82 0.45 mg/kg dry 2.297 BRL 79 50-124 Dimethyl phthalate 1.58 0.45 mg/kg dry 2.297 BRL 69 49-124 Di-n-butyl phthalate 1.83 0.45 mg/kg dry 2.297 BRL 79 51-128 Di-n-octyl phthalate 1.95 0.45 mg/kg dry 2.297 BRL 85 45-140 Fluoranthene 1.88 0.45 mg/kg dry 2.297 BRL 82 50-127 Fluorene 2.69 0.45 mg/kg dry 2,297 0.869 79 43-125 Hexachlorobenzene 1,52 0.45 mg/kg dry 2.297 BRL 66 45-122 Hexachlorobutadiene 2.81 0.45 mg/kg dry 2.297 BRL 122 32-123 Hexachlorocyclopentadiene BRL 0.45 mg/kg dry 2.297 BRL 32-117 M Hexachloroethane 5.52 0.45 mg/kg dry 2297 BRL 240 28-117 M Indeno(1,2,3-cd)pyrene 1.64 0.45 mg/kg dry 2.297 BRL 71 45-133 Isophorone 4,62 0.45 mg/kg dry 2.297 BRL 201 30-122 M Naphthalene 45900000 0.45 mg/kg dry 2.297 15.0 NR 35-123 M Nitrobenzene 2.12 0,45 mg/kg dry 2.297 BRL 92 34-122 N-Nitroso-di-n-propylamme 1.59 OAS mg/kg dry 2,297 BRL 69 36-120 N-Nitrosodiphenylamine 2.71 0,45 mg/kg dry 2.297 BRL 118 38-127 Pentachlorophenol 2.43 0.45 mg/kg dry 2.297 BRL 106 25-133 Phenanthrene 2.06 0.45 mg/kg dry 2.297 0266 78 50-121 Phenol 147 0.45 mg/kg dry 2.297 BRL 64 34-121 Pyrene 1.81 0.45 mg/kg dry 2.297 BRL 79 47-127 Surrogate: 2,4,6-Tribmmophenol 4.13 mg7kg dry 4,593 90 39-132 Surrogate: 2-Fluorobiphenyl 1,72 mg/kg dry 2,297 75 44-115 Surrogate: 2-Fluomphenol 3,33 mg*g dry 4,593 72 35-115 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041529-6364 - Toll Free Number: 1-600/629-6364-Fax: 7041626-0409 Page 44 of 52 13R I S M I `WkServ'ee Malyticel a Environmental Solutions •'uaoaaoxiu ixc Level II QC Report 2/27/18 Geoscience Group Project: Truck Part Service Prism Work Order: 8020233 Attn: Tom Hassett Time Submitted: 2/13/2018 3:18:OOPM 500-K Clanton Rd. Charlotte, NC 28217 Semivolatile Organic Compounds by GCIMS - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch PSB0345 - 3546 Matrix Spike (P8B0345-MS7) Source: 8020233-01 Prepared: 02/19/18 Analyzed: 02/20/18 Surrogate: Nitrobenzene-d5 3,62 _ mg/kg dry 2.297 158 37-122 SR Surrogate: Phenol-d5 3.16 mg/kg dry 4.593 69 34-121 Surrogate. Terphenyl-d14 1.74 mg/kg dry 2297 76 54-127 Matrix Spike Dup (P8B0345-MSD1) Source: 8020233-01 Prepared: 02/19/18 Analyzed: 02/20/18 1,2,4-Trcchlorobenzene 2.58 0.45 mg/kg dry 2.294 BRL 112 34-118 0.2 20 1,2-Dichlorobenzene 1.43 0.45 mg/kg dry 2.294 BRL 62 33-117 3 20 1,3-Dichlorobenzene 1.36 0.45 mg/kg dry 2.294 BRL 59 30-115 2 20 1,4-Dichlorobenzene 1.35 0.45 mg/kg dry 2.294 BRL 59 31-115 4 20 1-Methylnaphthalene 45900000 0,45 mg/kg dry 2.294 20.3 NR 40-119 0.1 20 M 2,4,6-Trichlorophenol 1.82 0,45 mg/kg dry 2.294 BRL 79 39-126 5 20 2,4-Dichlorophenol 3.43 0.45 m9/k9 dry 2.294 BRL 150 40-122 2 20 M 2,4-Dimethylphenol 0.591 0.45 mg/kg dry 2.294 BRL 26 30-127 160 20 M 2,4-Dinitrophenol 1.90 0.45 mg/kg dry 2.294 BRL 83 27-129 5 20 2,4-Dinitmtoluene 1.37 0.45 mg/kg dry 2.294 BRL 60 48-126 8 20 2,6-Dinitrotoluene 1.83 0.45 mg/kg dry 2.294 BRL 80 46-124 8 20 2-Chloronaphthalene 1,10 0,45 mg/kg dry 2.294 BRL 48 41-114 16 20 2-Chlorophenol 1.38 0.45 mg/kg dry 2.294 BRL 60 34-121 4 20 2-Methylnaphthalene 45900000 0.45 mg/kg dry 2.294 30.B NR 38-122 0.1 20 M 2-Methylphenol 1.75 OAS m9/tr9 dry 2.294 BRL 76 32-122 8 20 2-Nitrophenol 1.75 0.45 mg/kg dry 2,294 BRL 76 36-123 79 20 M 3,3'-Dichlorobenzidme 1.22 045 mg/kg dry 2.294 BRL 53 22-121 38 20 M 3/4-Methylphenol 1A4 0.45 mg/kg dry 2.294 BRL 63 34-119 6 20 4,6-Dinitm-2-methylphenol 1.65 0.45 mg/kg dry 2.294 BRL 72 29-132 7 20 4-Bromophenyl phenyl ether 1.68 0.45 mg/kg dry 2.294 BRL 73 46-124 7 20 4-Chlom-3-methylphenol 0.968 0.45 mg/kg dry 2.294 BRL 42 45-122 125 20 4-Chloroaniline 0.707 0.45 mg/kg dry 2,294 BRL 31 17-106 66 20 M M 4-Chlomphenyl phenyl ether 1.95 0.45 mg/kg dry 2.294 BRL 85 45-121 2 20 4-Nitrophenol 1,97 0.45 mg/kg dry 2,294 BRL 86 30-132 10 20 Acenaphthene 1.91 0,45 mg/kg dry 2.294 BRL 83 40-123 4 20 Acenaphthylene 2.04 0.45 mg/kg dry 2.294 BRL 89 32-132 3 20 Anthracene 1,96 0.45 mg/kg dry 2.294 BRL 85 47-123 3 20 Azobenzene 1.91 0.45 mg/kg dry 2.294 BRL 83 39-125 17 20 Benzo(a)anthmcene 1.87 0.45 mg/kg dry 2.294 BRL 81 49-126 4 20 Benzola)pyrene 1.84 0.45 mg/kg dry 2.294 BRL 80 45-129 5 20 Benzo(b)fluoranthene 1.83 0.45 mg/k9 dry 2,294 BRL 80 45-132 4 20 Benzo(g,h,i)perylene 1.56 0.45 mg/kg dry 2.294 BRL 68 43-134 2 20 Benzo(k)fluoranthene 1.80 OAS mg/kg dry 2.294 BRL 78 47-132 5 20 Benzoic Acid 1.26 0.45 mg/kg dry 2.294 BRL 55 10-83 53 20 M Benzyl alcohol 1.39 OAS mg/kg dry 2.294 BRL 60 29-122 4 20 bis(2-Chloroethoxy)methane 2,29 0.45 mg/kg dry 2.294 BRL 100 36-121 0.3 20 Bis (2-Chloroethyl) ether 2,90 0.45 mg/kg dry 2.294 BRL 126 31-120 22 20 M Bis(2-chloroisopropyl)ether 1.11 0.45 mg/kg dry 2.294 BRL 49 33-131 3 20 Bis(2-Ethylhexyl)phthalate 2.00 0.45 mg/kg dry 2.294 BRL 87 51-133 8 20 Butyl benzyl phthalate 1.85 0.45 mg/kg dry 2.294 BRL 81 48-132 6 20 Chrysene 1.78 0.45 mg/kg dry 2,294 BRL 77 50-124 20 20 Dibenzo(a,h)anthracene 1.56 0.45 mg/kg dry 2,294 BRL 68 45-134 50 20 M This report should not be reproduced, except in its entirety, without the written consent of Prism Labomtodes, Inc 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 7041529-6364- Toll Free Number: 1-800/5294364- Fax: 7041626,0409 Page 45 of 52 `'R I S M I Fun -Service Analyticai a Environmental Solutions ti`ueoxmoxiea iNe Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Semlvolatile Organic Compounds by GCIMS - Quality Control Reporting Result Limit Units Batch P8B0346-3646 Level II QC Report 2127/18 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Matrix Spike Dup JP8B0345-MSD1) _ _ Source: 8020233-01 _ Prepared: 02/19/18 Analyzed: 02/20/18 Dibenzofuran 2.13 0.45 mg/kg dry 2294 BRL 93 44-120 0.3 20 Diethyl phthalate 1.89 0.45 mg/kg dry 2.294 BRL 82 50-124 4 20 Dimethyl phthalate 1.52 0.46 mg/kg dry 2.294 BRL 66 48-124 4 20 Di-n-butyl phthalate 1,93 0.45 mg/kg dry 2,294 BRL 84 51-128 5 20 Di-n-octyl phthalate 2.10 0,45 mg/kg dry 2.294 BRL 91 45-140 7 20 Fluoranthene 2.01 0.45 mg/kg dry 2.294 BRL 87 50-127 7 20 Fluorene 2,63 0,45 mg/kg dry 2.294 0.869 77 43-125 2 20 Hexachlorobemene 1.56 0.45 mg/kg dry 2.294 BRL 68 45-122 3 20 Hexachlorobutadiene 2,84 0A5 mg/kg dry 2.294 BRL 124 32-123 1 20 M Hexachlorocyclopentadiene BRL 0.45 mg/kg dry 2.294 BRL 32-117 20 M Hexachloroethane 4.54 0,45 mg/kg dry 2,294 BRL 198 28-117 20 2D M Indeno(1,2,3-od)pyrene 2,09 045 mg/kg dry 2,294 BRL 91 45-133 24 20 M Isophorone 45900000 045 mg/kg dry 2,294 BRL Nit 30-122 200 20 M Naphthalene 45900000 0.45 mg/kg dry 2.294 15.0 NR 35-123 0.1 20 M Nitrobenzene 225 0.45 mg/kg dry 2,294 BRL 98 34-122 6 20 N-Nitroso-di-n-propylarnme 0,886 0.45 mg/kg dry 2.294 BRL 39 36-120 57 20 M N-Nitrosodiphenylamine 2.74 0.45 mg/kg dry 2,294 BRL 119 38-127 0.8 20 Pentachlorophenol 2.59 0.45 mg/kg dry 2.294 BRL 113 25-133 6 20 Phenanthrene 2.13 0.45 mg/kg dry 2.294 0,266 81 50-121 3 20 Phenol 1.64 0.45 mg/kg dry 2.294 BRL 71 34-121 10 20 Pyrene 1.96 0.45 mg/kg dry 2.294 BRL 85 47-127 8 20 Surrogate: 2,4,6-Tnbromophenol 4,29 mglkg dry 4.587 94 39-132 Surrogate: 2-Fluorobiphenyl 1.79 mglkg dry 2,294 78 44-115 Surrogate: 2-Fluorophenol 3.34 mglkg dry 4.587 73 35-115 Surrogate: Nitrobenzene-d5 4.01 mglkg dry 2.294 175 37-122 SR Surrogate: Phenol-d5 3.17 mglkg dry 4,587 69 34-121 Surrogate: Terphenyl-d14 1.82 mg/kg dry 2.294 79 54-127 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 -Charlotte, NC 28224-0643 Phone: 704/62a6364-Toll Free Number: 14f001629-6364- Fax: 7041626-0409 Page 46o 552 ,� R I S M I Funlms=:e Mal luti-o & Environmental SOWtiona �L,anMTOn,aA iaG Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control Analyte Reporting Result Limit Units Level II QC Report 2127118 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:OOPM Spike Source %RED RPD Level Result %REC Limits RPD Limit Notes Batch P8B0270 - MADEP VPH (S) Blank (P8B0270-BLK1) _ _ _ Prepared & Analyzed: 02/14/18 C5-C8 Aliphatics BRL 5.0 mg/kg wet C9-C12Aliphatics BRL 5.0 mg/kg wet C9-Cl0 Aromatics BRL 5.0 mg/kg wet Surrogate: 25-Dibromotoluene (PID) 9680 ug/L 10000 97 70-130 Surrogate: 2,5-Dibromotoluene (FID) 9670 ug/L 10000 97 70430 LCS (PBB0270-BS1) C5-C8 Aliphatics 20.1 C9-C10 Aromatics 5.83 C9-C12 Aliphatic 18.8 Surrogate: 2, 5-Dibromotoluene (PID) 9160 Surrogate: 2,5-Dibromotoluene (FID) 9210 LCS Dup(P8B0270-BSDI) C5-C8 Aliphatics 20.1 C9-C10 Aromatics 6.23 C9-C12 Aliphatic 19.7 Surrogate: 2,5-Dibromotoluene (PID) 9320 Surrogate: 2,5-Dibromotoluene (FID) 9390 _ Prepared & Analyzed: 02/14/18 5.0 mg/kg wet 16.00 125 70-130 5.0 mg/kg wet 5.333 109 70-130 5.0 mg/kg wet 16.00 116 70-130 ug/L 10000 92 70-130 U91L 10000 92. 70-130 ___ _Prepared & Analyzed: 02/14/18 5.0 mg/kg wet 16,00 126 70-130 0.2 - 50 5.0 mg/kg wet 5.333 117 70-130 7 50 5.0 mg/kg wet 16.00 123 70-130 4 50 ug/L 10000 93 70-130 ug/L 10000 94 70-130 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc, 449 Spdngbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 704/529-6364 - Toll Free Number: 1-8001629-6364 - Fax: 7041526-0409 Page 47 of 52 R I S M I FnnServica Analynoal 3 Environmental alyticalr. ueowroxieb ixe Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, INC 28217 Project: Truck Part Service Extractable Petroleum Hydrocarbons by GCIFID - Quality Control Analyte Reporting Result Limit Units Level II QC Report 2/27/18 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch P860289 - 3546 Blank (P8B0289-BLK1) Prepared & Analyzed: 02/15/18 C9-Cl8 Aliphatics C19-C36 Aliphatics C11-C22 Aromatics Surrogate: 1-Chlorooctadecane Surrogate: o-Terphenyl Surrogate: 2-Fluorobiphenyl Surrogate: 2-Bromonaphthalene LCS(P8B0289-851) CB-C18 Aliphatics C19-C36 Aliphatics C11-C22 Aromatics Surrogate: 1-Chlorooctadecane Surrogate: o-Terphenyl Surrogate: 2-Fluorobiphenyl Surrogate: 2-Bromonaphthalene LCS_Pup (P8B0289-BS_D1) C9-Cl8 Aliphatics C19-C36 Aliphatics C11-C22 Aromatics Surrogate: 1-Chlorooctadecane Surrogate: o-Terphenyl Surrogate: 2-Fluoroblphenyl Surrogate: 2-Bromonaphthalene Matrix Spike (P8B0289-MS1) C9-Cl8 Aliphatics C19-C36 Aliphatics C11-C22 Aromatics Surrogate: 1-Chlorooctadecane Surrogate: o-Terphenyl Surrogate: 2-Fluorobiphenyl Surrogate: 2-Bromonaphthalene 0a80 25 mg/kg wet BRL 25 mg/kg wet BRL 10 mg/kg wet 1.63 mg7kg wet 1.36 mg/kg wet 2.83 mg7kg wet 2.66 mgrkg wet 44.7 78.6 156 1.70 1.69 3,44 3.44 50.7 89.6 160 1.69 1.68 3.52 3.52 2,000 82 40-140 2.000 68 40-140 4.000 71 40-140 4.000 66 40-140 J Prepared&Analyzed: 02/15/18 25 mg/kg wet 60.00 74 40-140 25 mg/kg wet 80.00 98 40-140 10 mg/kg wet 170.0 92 40-140 mg/kg wet 2.000 85 40-140 mg/kg wet 2.000 84 40-140 mg/kg wet 4.000 86 40-140 mg7kg wet 4.000 86 40-140 Prepared & Analyzed: 02/15/18 25 mglkg wet 60.00 85 40-140 13 25 mg/kg wet 80.00 112 40-140 13 10 mg/kg wet 170.0 94 40-140 3 mg/kg wet 2.000 85 40-140 mg/kg wet 2.000 84 40-140 mg7kg wet 4.000 88 40-140 mg7kg wet 4.000 88 40-140 Source: 8020233-03 Prepared & Analyzed: 02/15/18 70.2 32 mg/kg dry 77.55 5.23 84 40-140 108 32 mg/kg dry 103.4 BRL 104 40-140 208 13 mg/kg dry 219.7 BRL 95 40-140 2.14 mg/kg dry 2.585 83 40-140 2.05 mg7kg dry 2.585 79 40-140 4.36 mg7kg dry 5,170 84 40-140 4.53 mg/kg dry 5.170 88 40-140 50 50 50 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 704/62M364 - Toll Free Number: 1-8001629-6364 - Fax: 704/525-0409 Page 48 Df 52 §OtR ISM I Fun -Service Analytical 4 Environmental solutions Pusommsisa isa Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, NC 28217 Project: Truck Part Service Extractable Petroleum Hydrocarbons by GCIFID - Quality Control Analyte Reporting Result Limit Units Level II QC Report 2/27/18 Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Batch PSB0289-3546 Matrix Spike Dup (P880289-MSD1) _ Source: 8020233-03 Prepared: 02/15/18 Analyzed: 02/16/18 CID-C18Aliphatics 68.3 32 mg/kg dry 77.93 5.23 81 _ 40-140 3 50 C19-C36 Aliphatics 118 32 mg/kg dry 103.9 BRL 113 40-140 9 50 C11-C22 Aromatics 192 13 mg/kg dry 220.8 BRL 87 40-140 8 5o Surrogate: 1-Chiorooctadecene 2.27 mg/kg dry 2,598 87 40-140 Surrogate: o-Terphenyl 1.96 mg/kg dry 2,598 76 40-140 Surrogate: 2-Fluorobiphenyl 4.36 mg/kg tlry 5.195 84 40-140 Surrogate: 2-Bromonaphthalene 4.18 mglkg dry 5.195 80 40-140 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc, 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Toll Free Number: 1-800/629-6364 - Fax: 7041625-0409 Page 49 of 52 ,LPAR M I Full -Service Analytical & jqEnvironmental Solutions ,[e ixc Geoscience Group Attn:Tom Hassett 500-K Clanton Rd. Charlotte, INC 28217 General Chemistry Parameters -Quality Control Analyte Level II QC Report 2127/18 Project: Truck Part Service Prism Work Order: 8020233 Time Submitted: 2/13/2018 3:18:OOPM Reporting Spike Source %REC RPD Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P8B0281 - Solids, Dry Weight Duplicate (P880281-DUP1) Source: 8020233-04 Prepared & Analyzed: 02/14/18 % Solids 67.0 0.100 % by Weight 67.0 0 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Sprin9brook Road - P.O. Box 240643 -Charlotte, NC 28224-0543 Phone: 7041529-6364- Toll Free Number: 1-800/629-6364 - Fax: 7041625-0409 Page 50 of 52 Sample Extraction Data Prep Method: Lab Number 3646 Batch Initial Final Date/Time 8020233-01 PBB0289 10.06 g 2 mL 02/15/18 1010 8020233-01 P880289 10.06 g 2 mL 02/15/18 1010 8020233-02 PBB0289 10.08 g 2 mL 02/15/18 1010 8020233-03 P8130289 10.11 g 2 mL 02/15/18 1010 8020233-04 P8130289 10.27 g 2 mL 02/15/18 1010 8020233-05 PBB0289 10.21 g 2 mL 02/15/18 1010 Prep Method: Solids, Dry Weight Lab Number Batch Initial Final Date/Time - 8020233-01 PBB0281 30 g 30 g 02/14/18 16:00 8020233-02 P8B0281 30 g 30 g 02/14/18 16:00 B020233-03 PBB0281 30 g 30 g 02/14/18 16:00 8020233-04 PBB0281 30 g 30 g 02/14/18 16:00 8020233-05 PBB0281 30 g 30 g 02/14/18 16:00 Prep Method: 3646 Lab Number Batch Initial Final Date/Time 8020233-01 P8B0345 30.01 g 1 mL 02/19/18 10:30 8020233-01 PBB0345 30.01 g 1 mL 02/19/18 10:30 8020233-02 P880345 30.08 g 1 mL 02/19/18 1030 8020233-03 P8B0345 30.03 g 1 mL 02/19/18 1030 8020233-04 PBB0345 30.01 g 1 mL 02/19/18 10:30 8020233-05 P8130345 30.08 g 1 mL 02/19/18 1030 Prep Method: 5036 Lab Number Batch Initial Final Date/Time 8020233-02 PBB0397 5a3 g 5 mL 02/21/18 13:33 8020233-03 P8130397 5,38 g 5 mL 02/21/18 13:33 8020233-04 P8B0397 5.48 g 5 mL 02/21/18 13:33 8020233-05 P8130263 6.12 g 5 mL 02/14/18 11:52 Prep Method: 6036 Lab Number Batch Initial Final Date/Time 8020233-01 P8B0410 4.83 g 5 mL 02/21/18 11:16 Prep Method: MADEP VPH (S) Lab Number Batch Initial Final Date/Time 8020233-01 P8B0270 18.38 g 16 mL O2/14/18 14:18 8020233-02 Pe130270 17.04 g 16 mL 02/14/18 14:18 8020233-03 P8130270 17.93 g 16 mL 02/14/18 14:18 8020233-D4 P880270 17,51 g 16 mL 02/14/18 14:18 8020233-05 P8130270 19.02 g 16 mL 02/14/18 14:18 This report should not be reproduced, except in its entirety, without the when consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041629-6364-Toll Free Number: l-8001629-6364-Fax: 704/626-0409 Page 51 of 52 00 2 m m 0 0 N p Qzo ceCD mOm nm8 a ��3$ a rr -m m o o'1 Q N s OF m _ y. 1, C, 3 V- �: m CL o <,-gym var' �M cz a �0�a Q Q�°' a a s� a~ 'U Tw z 2 Z.. o Vo °ems w B p a S= O z 15 m N n v x G �'•� F..> S Cn d o o p O QA$ av 3, ro '� MO O} r'� C QO 3 rn 02 d' � w s i C)DS _ Z o ... - or0r cti rnz .. $ P r V tTl C.% w I m w Q QO my �^ A o - .- t� w r $ o s N 639 s° a w T �^ h G) M F co y A rn � n O m R c, 48g)m 9 A o m tic mm m�w' ry18<!$ 5- N3 III y pNpau xm QQO�N a m'6 w 0A w O pAp� w G m off m �A " A<R-" m 3 - SID m °NNQ -Om CC QG .. 8 -J6 -. R 3A 2 O o �T°3 T O gm� 00 N m.m m 0m 5' o o m y m p m F Y m0 '� Z Z S 0 \l, sSN m a o A m me 'ti oQ Lp ' m 0 Off � �$ � �m (Z]� m �a wD m§5mc m m d0 TZ _• NP -Dj, `m�o m m V GI O Td4��.q <mm Dz _ 0 0 s s d Q� 4.yv V' L7,� N e JN `; 0 0 o d m m 0 Om A m rT% m ® m n .od. T a ° 3 m yy c S o a 0 g 0 m Z 5 n o a jl 5< m ca c� 3 rn0l m z a IZ m 0 g Mi 6 a ra y 3 w I I � m z r .A G z L I D m i �.,& 3-1 ' tam z ��(��� 2Sm z T m m n 000 m � 3 ° ma r� Sz 0 APPENDIX V Disposal Documents IIE'VD CORPORATION 1703 Vergrave Sheet Winston -Salvo, NC 27107 ph 336-725-55" faX 33B-725.6244 TANK DISPOSAL CERTIFICATE Tank Owner: Cindy Lane Development, LLC Site Address: 5007 Statesville Road Charlotte, NC Description of Tanks: Transporter. EC Project #: Tank Number 1 Evo Corporation 021816 Disposal Certification: Size of Tank 550 Gallons Contents #2 Fuel Oil Evo Corporation does hereby certify that the above named storage tank was transported to Triad Metal Recycling in Yadkinville, NC for proper disposal and recycling, �rcvc CORPORATION 1703 Vargrm $treat Winston-Salem, NO 27107 ph 336-725-5944 fax, 336-725-6244 CERTIFICATE OF DISPOSAL Evo Corporation does hereby certify that 530 gallons of non -hazardous contaminated water received on 2/12/2018 from: Generator: Cindy Lane Development, LLC Originating at: 5007 Statesville Road Charlotte, NC EC Waste ID #: 021816 has been disposed of by Evo Corporation in a manner approved by the North Carolina Department of Environmental Quality. Signature Thomas W. Hammett CEO Evo Corporation rwE:3 CORPORATION 1703 Vargrave Street Winston-Salem, NC 27107 ph 336-725-5W {ax 336-725-6244 CERTIFICATE OF DISPOSAL Evo Corporation does hereby certify that 52.45 tons of non-bazardous contaminated material received on 2/12i2018, 2/13/2018 and 2/15/2018 from: Generator. Cindy Lane Development, LLC Originating at: 5007 Statesville Road Charlotte, NC EC Waste ID 4: 021816 has been disposed of by Evo Corporation in a manner approved by the North Carolina Department of Environmental Quality. Signature Thomas W. Hammett CEO Evo Corporation EVO CORPORATION 1703 Vargrave Street, Winston-Salem, NC 27107 www.evocorp.net NON -HAZARDOUS MATERIALS MANIFEST n4 n4 venerator. bOul Phone: Site Address: esv e City/State: Charlotte NC Contact: Tom Hassett Gross Weight (Ibs): Empty Weight (Ibs): Net Weight (lbs): Quantity .Cw Material: _ 1Jgs4-tr qkv, Contaminant: #2 Fuel Oil Tons Drums Pails Sacs Yards E;9� Transporter: Evo CorpoPhone: ration 336-725-5844 Truck M t(02 Contact: Tony Disher As the transporter, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport In commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. EVO CORPORATION 1703 Vargrave Street Winston-Salem, NC 27107 Evo Project #: Phone: (336) 725-5844 Contact: Tony Disher 021816 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and�9;4isposal In a manner that has been authorized by the, State of North Carolina. Date: Ew cwponlion, 2008 i r_am EVO CORPORATION 1703 Vargrave Street, Winston-Salem, NC 27107 www.evocorp.het NON -HAZARDOUS MATERIALS MANIFEST n4n,-%4 Generator: Phone: Site Address: City/State: Otte Contact: Tom Hassett Gross Weight (Ibs): I I,un Empty Weight (Ibs): LA 6 ) Net Weight (lbs): -io�30 Quantity Z3 Evo C ation Transporter: rpor Truck#: Material: soil Contaminant: #2 Fuel OR 6)Drums Pails Sacs Phone: Yards Other: 336-725-5844 Contact: Tony Disher As the transporter, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured and are In proper condition for transport In commerce under the applicable regulations governing transportation, and I hereby receive this material for deliverflF414elacility designate. n Driver EVO CORPORATION 1703 Vargrave Street Winston-Salem, NC 27107 Evo Project #: Phone: (336) 725-5844 Contact: Tony Disher 021816 1 certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina. Evo corpomiion, 2008 cr_an,) EVO CORPORATION 1703 Vargrave Street, Winston-Salem, NC 27107 www.evocorp.ilet NON -HAZARDOUS MATERIALS MANIFEST Generator: Phone: Site Address: City/State: Charlotte NC Contact: Tom Ha ssett Gross Weight (Ibs): `7 / / Zo soli Material: Empty Weight (lbs): 3 y%LD Contaminant: Net Weight (Ibs): 3 6,`lOU Quantity Transporter: Evo Corporation Truck #: 2 / Z' #2 Fuel Oil on Drums Pails Sacs Yards Other. Phone: 336-725-5844 Contact: Tony Disher As the transporter, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured and are In proper condition for transport in commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. EVO CORPORATION 1703 Vargrave Street Winston-Salem, NC 27107 Evo Project #: Phone: (336) 725-5844 Contact: Tony Disher 021816 I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material for treatment and/or disposal in a manner that has been authorized by the State of North Carolina, Evo Cmpomion, 2008 'v Cr enn litisEVO CORPVargrave Street, nOQRATION n-Salem, NC 7107 www.evocorp.net NON -HAZARDOUS MATERIALS MANIFEST nA n4'1 Generator: Phone: Site Address: Statesville City/State: CharliRtte RC Contact: Tom Hassett M` A2ffift BrA§VESCR PT 0..QUA,NtTIUVEIOH° '.' Gross Weight (Ibs): i _)3 SLI) Material: Sot Empty Weight (Ibs): G25 7100 Contaminant: #2 Fuel Oil Net Weight (Ibs): Quantity I Ib 7 f I ons Drums Pails Sacs Yards Other: OR€d OFtTER I- �ORMiS�I©N�# : t � Transporter: Evo Corporation Phone: 336-725-5844 Truck #: /0/ Contact: Tony Disher As the transporter, I certify that the materials described above being shipped under this non -hazardous materials manifest are properly classified, packaged, labeled, secured and are in proper condition for transport In commerce under the applicable regulations governing transportation, and I hereby receive this material for delivery to the facility designate. EVO CORPORATION 1703 Vargrave Street Winston-Salem, NC 27107 Evo Project M 021816 Phone: (336) 725-5844 Contact: Tony Disher I certify that the carrier has delivered the materials described above to this facility, and 1 hereby accept this material for treatment and or disposal in a manner that has been authorized by the State of North Carolina. Facilitv Signature: Date: Ew CotpomNon, 2008 Scale Ticket This is to certify that the following described merchandise was weighed, counted, or measured by a public or deputy welghmaster, and when property signed and sealed shall be prima facia evidence of the accuracy of the weight shown as prescribed by law. Feb 15 2018 `:Ticket : 1112 Dust. Name: EYD Truck I8: 214 p b Z 8 1 to Trailer ID: 311 '-:`Weigh Fee: 1 Guiktrip 1844 2798 Lam St Kamapolis,NC 28083 Axle 1 : 18188 1b Axle 2 : 33528 lb Axle 3 : 38340 lh r: Total : 81%6 lb DRIVER IN TRUCK UNLESS CHECKED HERE: 30, 2018 41656 PUBLIC WEIGHMASTER'S CERTIFICATE OF WEIGHT & MEASURE IMPRINT SEAL HERE (IF APPLICABLE) FULLWEIGH TICKET# , (IF REWEIGH) 1054925 st�:x� t;iftts�t€ AUTOMATED TRUCE{ SCALE CIT r__,eE t.frtnp trt;r ­rT lb fz; :i[ "i�-Vc ej rkEACLfiL```�p tat4 -rid cfil•Fa.OldCa;IGttnS�qr7rar.Gs`tit.fYItR:YC,t=�S'yik:�`id"itw¢r=Cr+rr;ki Y+ta2tr±tflc� of 14 a,+f S-m1IACa rrt M;,n ...t. M'EIOa{'1YF'wSTW`6 W- VA.W'E PAY: 11 Ynn 4+'+ One r-i6t U§t rs ft:-"m Irep F`;�A•��,�,y,y.. ii.8 C! t,-;, `AI k;'Ak2I P,&AO a LOjI MtY (Ei1 tnr4 k'F-s antF Cr6rk;fh.[�,�t�E?rJ.r.tft - - ' 14p K'r,-t#,,alla4ci�P�t'tA'r�:ffat.ar?=�tettl,M;dt i,.tia #CCad Er �'Pa7p-'Siq - i: l F r 4va our "ipnt to r 3ta t=m, ni.r r .I irk: t 1i+ cc i;l k7e E;«tv0� Oa 8t�4{xC+;r r:.:xte II wn ��f.pM'q C4r F�:ylfEaSFiLo, t{ji If=rolv4 oJL&dT Im Otf"Wrioti%iWE. 1'OU.m pCti THEt '4XMi6mPOP,r ME"WpLELA i P :?'�f N.1deterl ru,4ne:;t 4 cy.nY Gifu � .. "- .. ' r,�kAT r^.�:tL�C.:t'f(a;'y'Ccre:Jr`�17€r'rs Yx3py.tV€12t;:..ii:$,''".S,i�Cnt;'TdkF'«a`}p:4t0(f Wdtet G�93;3?3u3fAr:r_:7 qY f1AmIF IdkiE.LY e`�-t stT: cl #hn T.iFi^n- S t:.; g,�f01 r,trt rTM it name r*Oaa ON ythM®i+ur s:t F.'1.1E:a:aC^Rn('rnyR"tt'taee_zrrr..cm4-p.•:n?*.'.-# - _ ➢iGLE f rz. 6 3r5V7256WC ATIOH: t tIT1Ft AFG'CF Getk:GitrT]CilfsrSiiFi� .)Wy `j h? f±tc Pa+pP�t4 Gf r'+s-' M ':ti V K', c7C+.Kri.IB"i a -Z Avl 495 FILI37A 8S rXIT 71 SA,L=JP.d fir. ��t:,T-Ayi']k _cair-55'c'i w' lr >a t# i1 .4i; �rjt Y+ml Lute f d a, , cc:„ rryo� r_Imz:j u ttaa rkub >r Ligt'ad, er_1nln,:. of rYrint*Ty7 r. , 'Jy r , 'I 6t7d`E{fOj,.j Apte•F.+rPa twF.lz`[t Ht"rcT t 3tr,n a rt.a Crmtntve,e ,tyrr.. itsS C� rriLet� 4 ,«CE1^istt»StEt:�ce' 4 trr,.: ,awct... FREIGHT C.Eyyg.� F11h 7Cq r Wt:T Vt4.. WPIEEP R`-€ X j .i r t$4i i!F'Cd!t,'fl-rJeati"+;'. 3iz MmEn rivt v.€agr{ 1t 4T1 i FfiFIYFk:t» Foss Recycling Winston Salem 1459 Tboonwille PkO gnu m-wcM. Nc 27107 'lime: pUl7R8 gt<* t ra; �ean•n•�i. �r.-. � aT33FF lat®siel USC CMH EXPENSE Sinkut Nu. in OIL Sngpllsr-! vLats No Vehlple :Sarkis,# my Grnta T&2* 47, 3$0 NMTHWOUM F'UWG W fMTER UOMtEXP1FnjM30,2D%8 INLESSSMEO Nass€oa fr..+9+nCs 1n Yc:cllgq 6ara Vsluu: mass kyllaYn9='lll� I:uFtwkre t psaiana, lazdMAAAMq, Retaurust+lilcy ►specstso"z values: GLculy aw of 11111111111 P14M : 1 15:25#41 9Gis. 04 12 M ZVI6 1-t4 1. ig i" inns Irma 7W-30i M iM rant* rt: A43 x.t wsght 47 , 380 l.as