MO-4523_14987_CA_MRP_20190925_Groundwater Monitoring Report

1rerracon
September 25, 2019
Mr. Jeff Walston
North Carolina Department of Transportation
Roadside Environmental Unit
1 South Wilmington Street
Raleigh, North Carolina 27601
Re: Groundwater Monitoring Report
Mt. Pleasant Maintenance Yard
NCDEQ UST Section Incident No. 14987
150 Dutch Road
Mt. Pleasant, Cabarrus County, North Carolina
Project No. 71177023
Dear Mr. Walston:
Terracon Consultants, Inc. (Terracon) is pleased to submit the attached groundwater
monitoring report for the above referenced site. This investigation was performed in general
accordance with the scope of services presented in Terracon's proposal dated May 14, 2019,
which meets the requirements of the Acknowledgement of Report Receipt from the North
Carolina Department of Environmental Quality (NCDEQ) dated February 5, 2019.
We appreciate the opportunity to be of service to you on this project. If there are any questions
regarding this report please do not hesitate to contact us.
Sincerely,
Terracon Consultants, Inc.
Haley . Martin, PG
Project Geologist
Michael T. Jordan; PG, RSM
Senior Geologist
frX. Fabriziani
for Scientist
Terracon Consultants, Inc. 2701 Westport Road Charlotte, North Carolina 28208
P (704) 509-1.777 F [phone] terracon.com

Groundwater Monitoring Report
Mt. Pleasant Maintenance Yard
Mt. Pleasant, Cabarrus County, North Carolina
September 25, 2019
Terracon Project No. 71177023
Prepared for:
North Carolina Department of Transportation
Raleigh, North Carolina
Prepared by:
Terracon Consultants, Inc.
Raleigh, North Carolina

Groundwater Monitoring Report
Mt. Pleasant Maintenance Yard
Mt. Pleasant, Cabarrus County, North Carolina
September 25, 2019
Terracon Project No. 71177023
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fig Haley H. artin, PG
Project Geologist
Jstin F Iziani
Seni r S entist
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Michael T. Jor�,Zp
Senior Geologic R,,,_, N
Terracon Consultants, Inc. 2701 Westport Road Charlotte, North Carolina 28208
P [phone] F [phone] terracon.com

Groundwater Monitoring Report
NCDOT Mt. Pleasant Maintenance Yard Irerracon
September 25, 2019 Terracon Project No. 71177023
TABLE OF CONTENTS
1.0 INTRODUCTION.............................................................................................................1
1.1
Site Description....................................................................................................1
1.2
Site Operational History.......................................................................................1
1.3
Site Investigation History......................................................................................2
1.4
Historical Receptor Information............................................................................2
1.5
Site Remedial History..........................................................................................2
1.6
Site Regulatory Status.........................................................................................3
1.7
Objectives and Scope of Work.............................................................................3
1.8
Standard of Care..................................................................................................3
1.9
Additional Scope Limitations................................................................................4
2.0 Receptor Information....................................................................................................4
2.1 Private Water Supply Wells..................................................................................4
2.2 Surface Water......................................................................................................5
2.3 Land Use and Places of Public Gathering............................................................5
3.0 FIELD ACTIVITIES AND METHODS..............................................................................5
3.1
Water Supply Well Sampling................................................................................5
3.2
Site Inspection and Well Network Evaluation.......................................................5
3.3
Water Level Measurements.................................................................................6
3.4
Groundwater Sample Collection...........................................................................6
3.5
Sample Analysis..................................................................................................7
3.6
Quality Assurance/Quality Control Samples.........................................................7
4.0 RESULTS.......................................................................................................................7
4.1 Groundwater Flow System...................................................................................7
4.2 Groundwater Analytical Results...........................................................................8
4.3 Evaluation for Vapor Intrusion..............................................................................8
4.4 Quality Control.....................................................................................................8
4.5 Data Review and Validation.................................................................................8
5.0 FINDINGS AND RECOMMENDATIONS.........................................................................9
6.0 REFERENCES................................................................................................................9
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Groundwater Monitoring Report
NCDOT Mt. Pleasant Maintenance Yard
September 25, 2019 Terracon Project No. 71177023
FIGURES
Figure 1. Topographic Map
Figure 2. Site Diagram
Figure 3. Receptor Survey Map
Figure 4. Shallow Groundwater Elevation Map (August 2019)
TABLES
Irerracon
Table 1. Water Supply Well Inventory
Table 2. Monitoring Well Construction Details and Water Level Elevations in Monitoring Wells
Table 3. Geochemical Field Parameters in Monitoring Wells (August 2019)
Table 4. Summary of Groundwater Analytical Data
APPENDIX A Analytical Report and Chain of Custody Record
APPENDIX B Historical Groundwater Analysis Tables
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Groundwater Monitoring Report
NCDOT Mt. Pleasant Maintenance Yard I rerracon
September 25, 2019 Terracon Project No. 71177023
1.0 INTRODUCTION
Terracon has prepared this Groundwater Monitoring Report on behalf of the North Carolina
Department of Transportation (NCDOT) Roadside Environmental Unit. It presents the findings of
recent field activities conducted by Terracon at the Mt. Pleasant Maintenance Facility (the site),
located at 150 Dutch Road in Mt. Pleasant, Cabarrus County, North Carolina (Figure 1).
1.1 Site Description
The site is located at 150 Dutch Road approximately 650 feet north of its intersection with NC
Highway 73 in Mt. Pleasant, Cabarrus County, North Carolina. The site is bisected by Dutch Road.
Topography at the site slopes gently to the west towards Dutch Buffalo Creek, which is located
along the western property boundary.
The site is currently occupied by the NCDOT Cabarrus County Maintenance Yard. The site is
primarily asphalt -paved with isolated lawn and landscaped areas. Several buildings are located on
the site including various administrative offices, maintenance shops, and storage buildings.
Various NCDOT machinery, vehicles, and equipment are also staged on the site. The surrounding
area is primarily used for agricultural and rural residential purposes. The Cabarrus Correction
Center is located south of the site.
1.2 Site Operational History
The site is currently occupied by the NCDOT Mt. Pleasant Maintenance Yard. Dating back to 1958,
12 underground petroleum storage tanks (USTs) have been maintained at the site. The USTs have
contained gasoline, diesel, kerosene, or waste oil. Nine (9) of the USTs have been removed from
the site, while three (3) remain in -place and are currently active. The following table provide details
on the current and former on -site USTs.
UST ID
Size (gallons)
Contents
Date Installed
Date Removed
1
3,000
Waste oil
09/26/1969
02/14/1990
2
2I5
Kerosene
09/29/1958
02/14/1990
3
2,000
Kerosene
09/29/1958
02/14/1990
4
2,000
Gasoline
09/29/1958
02/14/1990
5
6,000
Gasoline
08/30/1970
02/23/1990
6
10,000
Gasoline
1972?
03/28/1991
7
10,000
Gasoline
08/29/1972
03/28/1991
8
10,000
Diesel
08/29/1973
03/28/1991
9
2,000
Waste oil
October 1989
05/31/2005
10
10,000
Gasoline
02/14/1990
Currently in use
11
10,000
Diesel
02/14/1990
Currently in use
12
1 2,000
Waste oil
02/14/1990
Currently in use
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Groundwater Monitoring Report Irerracon
NCDOT Mt. Pleasant Maintenance Yard
September 25, 2019 Terracon Project No. 71177023
1.3 Site Investigation History
The site was first investigated in May 1992 when three (3) monitoring wells were installed following
the removal of USTs 1 through 8 in 1990 and 1991. Additional data regarding the identification,
location, or analytical results associated with these wells was not available in the NCDEQ incident
file associated with the site.
Thirteen (13) monitoring wells (MW-1 through MW-10 and TP-1 through TP-3) were reported to
have been located at the site (ECS, 1997). Groundwater has been estimated to flow to the north.
Petroleum constituent concentrations are known to have historically been identified in monitoring
wells MW-2, MW-4, MW-6, MW-7, MW-8, and MW-9. Free product was historically measured in
monitoring well MW-6 (1.5 inches on November 14, 1996 [ECS, 1997]). Naphthalene was detected
at a concentration of 197 micrograms per liter (ug/L) during the November 22, 1996 sampling event
(ECS, 1997).
Residual soil contamination has been reported in the vicinity of USTs 1 and 5 (ECS, 1997). The
most recent investigation occurred in 2005 after the removal of UST 9 (2,000-gallon waste oil
UST).
1.4 Historical Receptor Information
Subsurface utilities consisting of water, sewer, and storm drain lines are present at the site
generally buried at depths up to 3 feet below land surface (bls). Existing on -site buildings are
constructed as slab -on -grade; thus, crawlspaces are not present.
The closest surface water feature is Dutch Buffalo Creek, which extends along the western
property boundary. Seven (7) water supply wells were previously identified within 1,500 feet of the
source area (ECS, 1997). Public water is available to the site and surrounding properties by the
Town of Mt. Pleasant.
1.5 Site Remedial History
Remedial activities at the site have been limited to the removal of USTs and over -excavation of
soils near the USTs. USTs 1 through 8 were removed in 1990 and 1991. Approximately 185 cubic
yards of soil was reportedly removed and spread on the site with NCDEQ approval. The location
of the spread soils is unknown. UST 9 was removed in 2005. Excavated soils were not reported
during the removal of UST 9.
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Groundwater Monitoring Report
NCDOT Mt. Pleasant Maintenance Yard Irerracon
September 25, 2019 Terracon Project No. 71177023
1.6 Site Regulatory Status
NCDEQ issues a Notice of Regulatory Requirements (NORR) that indicated the site's risk ranking
was "High" (NCDEQ 2018). The NORR stated the following requirements:
sample the existing on -site monitoring wells on a semi-annual basis (May and November);
and
sample water supply wells within 1,000 feet of the site.
The NORR indicated a monitoring report summarizing the requested activities should be submitted
to the NCDEQ by November 30, 2018. Terracon submitted a request for an extension to Ms. Trudy
Beverly of the NCDEQ — Mooresville Regional Office. Ms. Beverly granted an extension until
December 14, 2018.
NCDEQ indicated that the next semi-annual sampling event should occur in May 2019 and the
monitoring report summarizing the requested activities be submitted by June 30, 2019 (NCDEQ
2019). Terracon submitted a request for an extension to Ms. Trudy Beverly of the NCDEQ
Mooresville Regional Office. Ms. Beverly granted an extension until September 27, 2019.
1.7 Objectives and Scope of Work
The objective of the scope of work was to monitor the dissolved phase plume conditions and
sample supply wells. This report contains a summary of the following activities and results:
sampling of the existing monitoring well network;
sampling of supply wells within 1,000 feet of the source area; and
recommendations for future site activities.
1.8 Standard of Care
Terracon's services were performed in a manner consistent with generally accepted practices of
the profession undertaken in similar studies in the same geographical area during the same time
period. Terracon makes no warranties, either express or implied, regarding the findings,
conclusions, or recommendations. Please note that Terracon does not warrant the work of
laboratories, regulatory agencies, or other third parties supplying information used in the
preparation of the report. These services were performed in accordance with the scope of work
agreed with you, our client, as reflected in our proposal.
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Groundwater Monitoring Report Irerracon
NCDOT Mt. Pleasant Maintenance Yard
September 25, 2019 Terracon Project No. 71177023
1.9 Additional Scope Limitations
Findings, conclusions, and recommendations resulting from these services are based upon
information derived from the on -site activities and other services performed under this scope of
work; such information is subject to change over time. Subsurface conditions may vary from those
encountered at specific borings or wells or during other surveys, tests, assessments,
investigations, or exploratory services; the data, interpretations, findings, and our
recommendations are based solely upon data obtained at the time and within the scope of these
services.
2.0 RECEPTOR INFORMATION
2.1 Private Water Supply Wells
Terracon conducted a windshield water supply well survey on February 3, 2017 in an attempt to
locate water supply wells within a 1,500-foot radius from the site boundary. During the visual
reconnaissance, properties were assumed to have a water supply well if a wellhead cover was
observed, such as faux rock, concrete block, or ornamental `wishing well' style structures. Results
are summarized on Table 1 and Figure 3.
Terracon identified the following items:
The service area provided by the Town of Mt. Pleasant Water and Sewer Department
includes properties within a 1,500-foot radius of the site.
Visual evidence of four (4) private water supply wells was identified based on the
reconnaissance survey (Figure 3). Two (2) water supply wells were identified within a
1,000-foot radius of the site.
Terracon contacted the Town of Mt. Pleasant Water and Sewer Department in an effort to
determine if developed properties identified within a 1,500-foot radius of the site had a water
account. Based on information provided by Ms. Amy Schueneman of the Town of Mt. Pleasant,
the properties within the 1,500-foot radius to the north and one property to the south of the site are
not connected to municipal water. There are two water supply wells (WSW-2 and WSW-3) located
between the 500 foot and 1,000 foot -radius. There are potentially four water supply wells (WSW-
1, WSW-4, WSW-5 and WSW-6) located between the 1,000 foot and 1,500-foot radius. Property
owners located greater than 1,000 feet from the source area were not directly contacted nor were
water supply well questionnaires issued to property owners. As such, the use of each suspected
well (potable water or irrigation) located greater than 1,000 feet from the site was not confirmed.
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Groundwater Monitoring Report
NCDOT Mt. Pleasant Maintenance Yard I rerracon
September 25, 2019 Terracon Project No. 71177023
2.2 Surface Water
Surface water in the vicinity of the site is part of the Yadkin -Pee Dee River Basin. Dutch Buffalo
Creek is located approximately 300 feet to the west of the source area. A pond is also located
approximately 400 feet to the north of the source area. Surface water runoff at the site generally
flows to the west and southwest towards Dutch Buffalo Creek that is located along the west side
of the property. Surface water features are shown on an excerpt from the Mount Pleasant, NC 7.5-
Minute Topographic Quadrangle Map, which is depicted on Figure 1.
2.3 Land Use and Places of Public Gathering
Terracon did not identify properties considered places of public gathering within 1,500 feet of the
site. According to the Cabarrus County GIS database, land use within 1,500 feet of the site is
primarily residential and agricultural with some light commercial.
3.0 FIELD ACTIVITIES AND METHODS
Sampling activities were conducted in general accordance with NCDEQ's requests (2018 and
2019). Field activities conducted during the August 2019 field events included collection of water
level measurements, groundwater samples from 10 monitoring wells, and an attempt to collect a
groundwater sample from two water supply wells (WSW-2 and WSW-3). Site wells are shown on
Figure 2 and supply wells are shown on Figure 3.
3.1 Water Supply Well Sampling
Terracon was unable to collect samples from the water supply wells located within 1,000 feet of
the site (WSW-2 and WSW-3) during the August 2019 sampling event. Supply wells located
greater than 1,000 feet (wells WSW-1, WSW-4, WSW-5 and WSW-6) from the source area were
not included in the August 2019 sampling event per the NCDEQs September 2018 NORR.
Terracon staff knocked on the door of the residence where WSW-2 is located but a minor answered
the door and the property owner was not home to authorize sampling. The property owner of WSW-
3 answered the door but stated he was not interested in having his well sampled.
3.2 Site Inspection and Well Network Evaluation
Terracon conducted an inspection of site monitoring wells. Monitoring well construction details are
provided on Table 2. The following summarizes observations:
Several wells (MW-2, MW-3, MW-4, and TP-3) could not be located and were likely paved
over based on information gathered from discussions with NCDOT employees at the site
office. Based on available historical documents, these wells were last located in 1996.
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Groundwater Monitoring Report
NCDOT Mt. Pleasant Maintenance Yard Irerracon
September 25, 2019 Terracon Project No. 71177023
Monitoring well MW-6 was not able to be sampled. The well appears to be constructed of
corrugated plastic pipe and the well is not vertical. MW-6 bends at approximately three feet
below grade which prevented the purging and sampling of the well.
New monitoring wells MW-4R and MW-6R were installed on November 3, 2017 to replace
MW-4 and MW-6.
The majority of the wells were in good condition.
During the August 2019 groundwater sampling event, water level measurements and groundwater
samples were collected from the following nine monitoring wells:
Shallow monitoring wells:
MW-1
MW-4R
MW-5
Deep monitoring well:
MW-10
3.3 Water Level Measurements
MW-6R MW-9
MW-7 TP-1
MW-8 TP-2
Water level measurements were collected from accessible site monitoring wells on
August 14, 2019 to estimate the groundwater flow direction and horizontal and vertical hydraulic
gradients. The water levels were measured with an electronic water level probe that was
decontaminated before and after each use. The water level measurements were converted to
water level elevations using existing top -of -casing elevation data for each well (Table 2). The water
level elevations were used to prepare a water level contour map to estimate the shallow
groundwater flow directions at the site, as discussed in Section 4.1 of this report.
3.4 Groundwater Sample Collection
Groundwater samples were collected using a peristaltic pump. Low flow purging and sampling
techniques were used to the extent practical for each well. During purging, the field geochemical
parameters of temperature, pH, conductivity, dissolved oxygen (DO), and oxidation-reduction
potential (ORP) were measured using a handheld YSI 556 multiparameter probe units. Purging
continued until pH and conductivity parameters stabilized. Table 3 summarizes indicator
parameter measurements of temperature, pH, specific conductance, DO, and ORP.
Sampling equipment was thoroughly decontaminated with phosphate -free soap and distilled water
prior to fieldwork and between each well to prevent cross -contamination. New polyethylene tubing
was used during the purging and sampling of each monitoring well. Decontamination water and
purge water was poured on the land surface.
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Groundwater Monitoring Report
NCDOT Mt. Pleasant Maintenance Yard I rerracon
September 25, 2019 Terracon Project No. 71177023
3.5 Sample Analysis
Once collected, the groundwater samples were placed in appropriately labeled containers and
packed on ice pending delivery to Shealy Environmental Services, Inc. (Shealy). Water samples
collected in the field remained in the presence of a project representative until picked up by Shealy
personnel and delivered to the laboratory in West Columbia, South Carolina. A completed chain -
of -custody record was provided with the cooler containing groundwater samples.
The following analytical methods were requested on the chain -of -custody for the wells sampled in
August 2019:
Volatile organic compounds (VOCs) by EPA Method 8260,
Semi -volatile organic compounds (SVOCs) by EPA Method 8270, and
MADEP Methods extractable petroleum hydrocarbons (EPH) and volatile petroleum
hydrocarbons (VPH).
3.6 Quality Assurance/Quality Control Samples
The quality assurance/quality control (QA/QC) sampling included one trip blank. A QA/QC sample
was submitted to the laboratory for analysis of VOCs by EPA Method 8260.
4.0 RESULTS
Field and laboratory analytical results from the soil and groundwater sampling events conducted
in August 2019 are discussed in detail below. Laboratory analytical reports from Shealy were
reviewed and validated to ensure that they met specific data -quality objectives. Laboratory
analytical results are provided in Appendix A.
4.1 Groundwater Flow System
Water level measurements were collected from the site monitoring wells on August 14, 2019. The
depth -to -water measurements and the converted water level elevations are listed in Table 2. Depth
to water measurements for the shallow wells (10 to 15 feet bls) ranged from approximately 3.60 to
7.91 feet bls.
Water elevations were used to produce a potentiometric surface elevation map for the shallow
wells (Figure 4). Based on the water level measurements collected in August 2019, the
groundwater flow direction in the shallow aquifer zone appears directed to the north.
The groundwater flow direction is generally consistent with historical site data. Shallow
groundwater had a horizontal gradient of approximately 0.023 feet per foot (ft/ft).
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Groundwater Monitoring Report
NCDOT Mt. Pleasant Maintenance Yard I rerracon
September 25, 2019 Terracon Project No. 71177023
4.2 Groundwater Analytical Results
Laboratory analytical results and field parameter results from the August 2019 sampling event are
described below. Constituent concentrations in groundwater are presented in Table 4.
Groundwater analytical results for VOCs, SVOCs, EPH, and VPH were compared with their NCAC
2L groundwater quality standards (2L standards).
4.2.1 Monitoring Well Network
Groundwater samples were collected from 10 permanent monitoring wells on August 14, 2019.
Groundwater concentrations in the samples collected from the permanent monitoring well network
are presented in Table 4.
4.3 Evaluation for Vapor Intrusion
Based on the Interstate Technology and Regulatory Council (ITRC) Petroleum Vapor Intrusion
(PVI) guidance, additional evaluation of the PVI pathway for the dissolved -phase plume is not
warranted. The on -site buildings are not likely at potential risk for PVI based on the observed
groundwater concentration data and average vertical extent of the vadose zone at the site.
4.4 Quality Control
The trip blank sample did not contain compounds at concentrations above laboratory method
detection limits. A copy of the laboratory analytical report is provided in Appendix A.
4.5 Data Review and Validation
This section provides an evaluation of the laboratory analytical data for the completeness of data
package deliverables. Additionally, field data were reviewed to verify completion of required
documentation. A copy of the laboratory analytical reports is provided in Appendix A.
Field activities were documented on groundwater sampling logs. Groundwater samples were
appropriately labeled, stored in sample containers on ice, and delivered to Shealy in good condition
and properly preserved. The sample container chain -of -custody forms were forwarded with the
samples to the analytical laboratory.
The samples were analyzed for parameters as detailed in Section 3.5. For the August 2019
sampling event, one trip blank accompanied the cooler sent to the laboratory for analysis of VOCs
by EPA Method 8260. VOCs were not detected in trip blank.
EPH constituents (C9-C18 Aliphatic range) were detected in the method blank for the prep batch
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Groundwater Monitoring Report Irerracon
NCDOT Mt. Pleasant Maintenance Yard
September 25, 2019 Terracon Project No. 71177023
that contained samples MW-1, MW-4R, MW-5, MW-6R, MW-7, MW-8, MW-9, MW-10, TP-1 and
TP-2. Samples MW-1, MW-4R, MW-5, MW-7 and MW-10 did not contain detections of the target
analyte; therefore, the laboratory did not re -extract the samples. Samples TP-1, TP-2, MW-6R,
MW-8, and MW-9 had detections of C9-C18 Aliphatic; therefore, the samples were re -extracted
and re -analyzed outside of holding time. Both sets of data are included in the laboratory analytical
report provided in Appendix A. Although samples were analyzed outside of hold time after
re -extraction, the data associated with samples TP-1, TP-2, MW-6R, MW-8, and MW-9 is believed
to be a reflection of on -site conditions. After re -extraction of select samples, the sample criteria
were met. The surrogate, laboratory control sample, and matrix spike and matrix spike duplicate
(MS/MSD) recoveries and precision on client samples were all within the advisory limits. MS/MSDs
that were performed on non -project samples were not evaluated because matrix similarity to
project samples could not be assumed.
5.0 FINDINGS AND RECOMMENDATIONS
The findings of this report are as follows:
Groundwater in the shallow aquifer (3 to 25 feet bls) is estimated to flow north;
C9-C22 Aromatics were detected at a concentration above its 2L Standard in MW-6R.
Compounds were not detected above 2L Standards in the remaining nine monitoring wells
sampled;
Terracon was unable to collect samples from two water supply wells (WSW-2 and WSW-
3) during the August 2019 sampling event.
The on -site buildings are not likely at potential risk for PVI based on the observed
groundwater concentration data and average vertical extent of the vadose zone at the site.
Based on the current and historical results, Terracon offers the following recommendations:
Conduct at least one (1) additional sampling event of monitoring well network to monitor
for temporal trends particularly in monitoring well MW-6R.
Abandon damaged monitoring well MW-6.
6.0 REFERENCES
ECS, 1997. Engineering Consulting Services, Ltd (ECS). "Comprehensive Site Assessment -
North Carolina Department of Transportation Cabarrus County Maintenance Yard." January 24,
1997.
NCDENR, 2010. North Carolina Administrative Code. "North Carolina's Groundwater Quality
Standards", Title 15A, Chapter 2L. Revised April 1, 2013.
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Groundwater Monitoring Report
NCDOT Mt. Pleasant Maintenance Yard Irerracon
September 25, 2019 Terracon Project No. 71177023
NCDEQ, 2018. Underground Storage Tank Section, Division of Waste Management. "Notice of
Regulatory Requirements". Letter prepared for NCDOT Roadside Environmental Unit. September
13, 2018.
NCDEQ, 2019. UST Section, DWM. "Acknowledgement of Report Receipt". Letter prepared for
NCDOT Roadside Environmental Unit. February 5, 2019.
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FIGURES

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TOPOGRAPHIC MAP IMAGE COURTESY OF THE U.S. GEOLOGICAL SURVEY
QUADRANGLES INCLUDE: MOUNT PLEASANT, NC (1/1/2002) and LOCUST, NC (1/1/1983).
TOPOGRAPHIC MAP Exhibit
Irerracon Mt. Pleasant Maintenance Yard
2020 Starita Rd Ste E 150 Dutch Road
Charlotte, NC 28206.1298 Mt. Pleasant, NC
Drawn by:
HHM
Scale:
=2 .0000o
Checked by:
MTJ
File Name:
e:
71177ozi 1
Approved by: MTJ
Date: Sept. 2019

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PURPOSES
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-
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Project Manager:
Project No.
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71177023
SITE DIAGRAM
Figure
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Scale: 1"= 100'
Irerracon
Mt. Pleasant Maintenance Yard
Checked by: MTJ
FileNa
71177023.2
2701 Westport Road
150 Dutch Road
2
pprovedby: MTJ
Date:
Charlotte, INC
Mt. Pleasant, North Carolina
Sept. 2019

Project Manager:
Project
FJD
71No.
7117700
Irerracon
2701 Westport Road
P
Charlotte, INC
Receptor Survey Ma
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Figure
Drawn by:
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Scale:
l ir,=soo ft
Mt. Pleasant Maintenance Yard
150 Dutch Road
Mt. Pleasant, NC
3
Checked by:
MTJ
File Name:
71177023
Approved by:
Date:
MTJ
I Sept.2019

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Main C ffice
TP-3
--. *'W,,
Legend
A— Estimated direction of
groundwater flow
Approximate location of
Groundwater elevation
groundwater monitoring well
(98.42) ( ) based on arbitrary
Well not located/destroyed
datum of 100 feet
97 Inferred groundwater
- - - - Approximate fence line
— — — — elevation contour
F1 Building Footprint
NM = Not Measured
� � I (NM)
Canopy
TP=I-
(NM)
R 2604 I '
98 9.100- - - - - -- - -;,
-------- pr � ' -
------'�------= --
t
t a
'- MW 1
(95.27)
�t
-� Truck Storage 9e
Office
DIAGRAM IS FOR GENERAL LOCATION ONLY,
AND IS NOT INTENDED FOR CONSTRUCTION
PURPOSES
MW-6R
(NM) MW-9 "1
MW-10 (100.50)
(99.24)
I
Project Manager:
Project No.
SURFICIAL GROUNDWATER ELEVATION MAP
FJD
71177023
Figure
g
Drawn by:
Scale:
Irerracon
(August 2019)
HHM
1"=60ft
Mt. Pleasant Maintenance Yard
4
Checked by:
FlleNarne:
MTJ
71177023.4
2701 Westport Road
150 Dutch Road
pprovedby: MTJ
Date: Sept. 2019
Charlotte, NC
Mt. Pleasant, North Carolina

TABLES

Table 1
Water Supply Well Inventory
Mt. Pleasant Maintenance Yard
Mt. Pleasant, Cabarrus County, NC
Terracon Project No. 71177023
Distance/Directions
Well No.
Property Owner
Mailing Address
Property Address
Well Status/Use
V11unicipal Water
Parcel No.
Comments
from source area
P.O. Box 43
9670 NC Highway 73 E
No well observed and no
WSW-1
Frank A. James
1,300 feet south
Potable
Not Connected
56709317260000
Mt. Pleasant, NC 28124
Mt. Pleasant, NC 28124
municipal water connection
Terracon did not receive a
211 Dutch Road
211 Durch Road
WSW-2
Warren Torraz McClure
800 feet north
Potable
Not Connected
56708157310000
response to requests to sample
Mt. Pleasant, NC 28124
Mt. Pleasant, NC 28124
well.
210 Dutch Road
210 Dutch Road
WSW-3
Jason P. Barnhardt
1,000 feet north
Potable
Not Connected
56709347870000
Well observed
Mt. Pleasant NC 28124
Mt. Pleasant NC 28124
Spencer Thomas Jr. and
219 Dutch Road
219 Dutch Road
WSW-4
1,250 feet north
Potable
Not Connected
56709421300000
Well observed
Daisy Thomas
Mt. Pleasant, NC 28124
Mt. Pleasant, NC 28124
Jay F. Northup III and
811 West State Road
224 Dutch Road
WSW-5
1,350 feet north
Potable
Not Connected
56709472030000
Well observed
Laurie Northup
Cortland, NY 13045
Mt. Pleasant, NC 28124
Jimmie D. Vanover and
P.O. Box 1756 Concord,
231 Dutch Road
WSW-6
1,450 feet north
Potable
Not Connected
56709422790000
No municipal water connection.
Della K. Vanover
NC 28206
Mt. Pleasant NC 28124
Notes:
1 = Not connected to municipal water as of date, according to Ms. Amy Shueneman of the Town of Mt. Pleasant.

Table 2
Monitoring Well Construction Details and Water Level Elevations in Monitoring Wells
Mt. Pleasant Maintenance Yard
Mt. Pleasant, Cabarrus County, NC
Terracon Project No. 71177023
Well ID
Date Installed
( mm/dd/yy)
Well Diameter
(in)
Screen Interval
(ft bls )
Top -of -Casing
* ( )
Elevation ft
Date Measured
mm dd
( / /yy)
Total Depth
ft bls
( )
Depth to
Water (ft
bTOC)
Groundwater
Elevation )
Elevation ft
Casing
Mount
Well Status
SURFICIAL MONITORING WELLS
MW-1
05/13/92 - 05/15/92
2
4.5 - 14.5
103.18
01/25/17
15.0
5.0
98.18
flush
Active
11/02/17
8.0
95.22
05/30/18
6.7
96.48
11/14/18
5.48
97.70
08/14/19
7.91
95.27
MW-2
05/13/92 - 05/15/92
2
4.5 - 14.5
101.69
NM
15.6
NM
NM
flush
Destroyed/Paved Over
MW-3
05/13/92 - 05/15/92
2
5.0 - 15.0
99.47
NM
15.5
NM
NM
flush
Destroyed/Paved Over
MW-4
10/19/1992
2
4.0 - 14.0
102.77
NM
15.3
NM
NM
flush
Destroyed/Paved Over
MW-4R
11/6/2017
2
4.65 - 14.65
NS
11/06/17
14.7
6.71
NM
flush
Active
05/30/18
6.47
NM
11/14/18
4.76
NM
08/14/19
6.57
NM
MW-5
10/19/1992
2
4.0 - 14.0
100
01/25/17
15.2
4.79
95.21
flush
Active
11/02/17
6.11
93.89
05/30/18
5.34
94.66
11/14/18
4.42
95.58
08/14/19
5.79
94.21
MW-6
10/19/1992
2
4.0 - 14.0
104.54
NM
15.3
NM
NM
flush
Damaged
MW-6R
11/6/2017
2
5.16 - 15.16
NS
11/06/17
15.16
5.55
NM
flush
Active
05/30/18
4.42
NM
11/14/18
3.91
NM
08/14/19
3.75
NM
MW-7
11/12/96 - 11/13/96
2
5.0 - 10.0
105.21
01/25/17
10.0
5.14
100.07
flush
Active
11/02/17
6.79
98.42
05/30/18
6.18
99.03
11/14/18
5.37
99.84
08/14/19
6.48
98.73
MW-8
11/12/96 - 11/13/96
2
5.0 - 10.0
105.67
01/25/17
10.0
3.49
102.18
flush
Active
11/02/17
6.06
99.61
05/30/18
4.52
101.15
11/14/18
3.3
102.37
08/14/19
4.87
100.80
MW-9
11/12/96 - 11/13/96
2
5.0 - 10.0
104.1
01/25/17
10.0
3.19
100.91
flush
Active
11/02/17
4.35
99.75
05/30/18
3.21
100.89
11/14/18
3.11
100.99
08/14/19
3.60
100.50
TP-1
Unknown
4
Unknown
Unknown
01/25/17
11.75
3.44
NM
flush
Active
11/02/17
5.49
NM
05/30/18
4.12
NM
11/14/18
3.11
NM
08/14/19
5.10
NM
TP-2
Unknown
4
Unknown
Unknown
01/25/17
11.0
4.44
NM
flush
Active
11/02/17
6.38
NM
05/30/18
5.02
NM
11/14/18
4.02
NM
08/14/19
6.07
NM
TP-3
Unknown
Unknown
Unknown
105.39
NM
Unknown
NM
NM
flush
Destroyed/Paved Over
DEEP
MONITORING WELL
MW-10
11/12/96 - 11/13/96
2
72.5 - 92.5
103.79
01/25/17
92.5
5.01
98.78
flush
Active
05/30/18
3.55
100.24
11/14/18
2.42
101.37
08/14/19
4.55
99.24
NOTES:
*Top of casing elevation based on an assumed datum of 100 feet.
Monitoring wells MW-2, MW-3, MW-4 and TP-3 have not been located and are presumed destroyed.
Monitoring wells MW-4R and MW-6R were installed on 11/2/17 to replace MW-4 and MW-6 and have not been surveyed.
ft bTOC = feet below top of casing
ft bls = feet below land surface
in = inches
NM = Not Measured
NS = Not Surveyed

Table 3
Geochemical Field Parameters in Monitoring Wells (August 2019)
Mt. Pleasant Maintenance Yard
150 Dutch Road
Mt. Pleasant, Cabarrus County, North Carolina
Terracon Project No. 71177023
Sample ID
Field Parameter
(units)
Conductivity
(PS/cm)
Dissolved Oxygen
(mg/L)
ORP
(mV)
pH
(SU)
Temperature
( C )
Sample Date
MW-1
08/14/19
784
0.21
253.2
6.22
28.8
MW-4R
08/14/19
694
0.18
-131.7
6.89
26.7
MW-5
08/14/19
1,445
0.21
176.9
5.64
27.1
MW-6R
08/14/19
379.6
0.4
-199.8
6.28
28.1
MW-7
08/14/19
331
0.57
25.4
6.25
27.5
MW-8
08/14/19
1,634
0.18
93.7
6.91
27.5
MW-9
08/14/19
334.8
0.23
-148.8
6.28
32.5
MW-10
08/14/19
829
1.30
237.5
6.47
25
TP-1
08/14/19
449
0.24
290.3
6.76
24.8
TP-2
08/14/19
281.2
0.58
9.8
6.71
25.6
NOTES:
µS/cm = microsiemens per centimeter
mg/L = micrograms per liter
mV = millivolts
SU = Standard Units
C = degrees celsius

Table 4
Summary of Groundwater Analytical Data
Mt. Pleasant Maintenance Yard
Mt. Pleasant, Cabarrus County, NC
Terracon Project No. 71177023
N
QOOu
CN
w
�
E
L
E
O
ca
E
U
r
L
W
O
-2
U
H
.
X
N
O
a
W
2
H
C
3.
X
0
H
N
t
N
Q
G!
A
L
Q
x
L
V
ii
Nr
`-. r
O
6
p
U
Y
L
,
N
m
O.
>
?
C
G
0)
a
N
N
L
C
Z
yl
L
y
dGO
QO
N`
N
V
O1O
U
W
V
U
u
G
QO
N
U
Sample ID
a
Smple
EPA Method 8260
i EPA Method 8270
MADEP
SURFICIAL MONITORING WELLS
01/25/17
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<0.5
<0.8
<0.8
<4.0
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
NA
NA
NA
11/02/17
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
<4.0
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
NA
NA
NA
MW-1
05/30/18
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
2.81
<8.0
<4.0
0.91
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
11/14/18
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
<4.0
<8.0
1.4J
<4.0
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
08/14/19
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
<4.0
2.6 BJ
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
<110
<75
<75
11/06/17
2.11
<0.5
<0.5
1.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
<4.0
<8.0
<4.0
0.851
<0.8
<0.8
<0.8
<0.8
NA
NA
NA
05/30/18
<10
<0.5
<0.5
<0.5
1 <0.5
<0.5
1 <0.5
<5.0
1 <0.5
<0.5
1 <1.0
<0.8
<0.8
<4.0
1 <8.0
<4.0
0.92.1
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
MW-411
11/14/18
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
<4.0
<8.0
6.0
<4.0
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
08/14/19
S.1J
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<1.0
<0.5
<0.5
<4.0
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
01/25/17
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<0.5
<0.8
<0.8
<4.0
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
NA
NA
NA
11/02/17
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
<4.0
<8.0
1.71
0.87J
<0.8
<0.8
<0.8
<0.8
NA
NA
NA
VW-5
05/30/18
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
2.8J
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
11/14/18
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
<4.0
<8.0
3.11
<4.0
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
08/14/19
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
<4.0
<8.0
24
<4.0
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
11/06/17
3.3J
<0.5
0.91
7.7
<0.5
4.1
<0.5
4.0J
<0.5
<0.5
<1.0
<0.8
<0.8
<4.0
<8.0
6.2
<4.0
<0.8
<0.8
<0.8
<0.8
NA
NA
NA
05/30/18
<10
<0.5
<0.5
<0.5
0.57
1.2
2.3
2.81
<0.5
<0.5
<1.0
5.2
<0.8
2.41
<8.0
<4.0
1.31
6.4
<0.8
<0.8
<0.8
400
100
<75
M W-6R
11/14/18*
<10
<0.5
<0.5
<0.5
<0.5
0.76
1.8
1.7J
<0.5
<0.5
<1.0
3.6
0.58J
<4.0
<8.0
2.2J
0.981
4.9
<0.8
<0.8
<0.8
370
97
<75
08/14/19
<10
<0.5
<0.5
<0.5
<0.5
1.1
1.5
2.51
<0.5
<0.5
<1.0
2.5
0.42J
<4.0
<8.0
<4.0
<4.0
3.0
0.29J
0.49J
1.4
509
110
17J
01/25/17
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<0.5
<0.8
<0.8
<4.0
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
NA
NA
NA
11/02/17
<10
<0.5
<0.5
0.67
<0.5
<0.5
<0.5
<5.0
<0.5
0.54
0.63)
<0.8
<0.8
1 <4.0
<8.0
<4.0
1 <4.0
<0.8
1 <0.8
<0.8
<0.8
NA
NA
NA
MW-7
05/30/18
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
1 <1.0
<0.8
<0.8
<4.0
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
11/14/18
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
<4.0
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
08/14/19
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
<4.0
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
01/25/17
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<0.5
<0.8
<0.8
<4.0
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
NA
NA
NA
11/02/17
3.9J
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
0.46J
<0.5
<0.5
<0.8
<0.8
<4.0
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
NA
NA
NA
MW-8
05/30/18
2.21
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
2.0
<0.5
<1.0
<0.8
<0.8
2.61
<8.0
<4.0
1.11
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
11/14/18
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
3.9
<0.5
<1.0
<0.8
<0.8
<4.0
<8.0
3.2J
0.95J
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
08/14/19
4.71
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
1.4
<0.5
<1.0
<0.8
<0.8
<4.0
3.3131
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
7.21
<110
<75
01/25/17
13
<0.5
<0.5
<0.5
<0.5
2.6
2.4
4.51
<0.5
<0.5
<0.5
1.3
1.3
<4.0
<8.0
<4.0
<4.0
1.4
<0.8
1.4
<0.8
NA
NA
NA
11/02/17
6.1J
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<0.5
<0.8
<0.8
<4.0
2.4J
<4.0
1.1J
<0.8
<0.8
1.2
<0.8
NA
NA
NA
MW-9
05/30/18
9.11
<0.5
<0.5
<0.5
0.49J
0.45J
1.6
<5.0
<0.5
<0.5
<1.0
1.1
1.1
2.31
<8.0
<4.0
0.82J
1.1
<0.8
<0.8
<0.8
60
57J
<75
11/14/18
8.91
<0.5
<0.5
<0.5
<0.5
1.3
2.0
1.5J
<0.5
<0.5
<1.0
<0.8
<0.8
<4.0
<8.0
2.2J
<4.0
<0.8
<0.8
<0.8
<0.8
87
95
<75
08/14/19
6.21
<0.50
<0.5
<0.5
<0.5
0.45J
0.65
<5.0
<0.5
<0.5
<1.0
0.28)
<0.8
2.31
5.2 BJ
<4.0
<4.0
0.23J
<0.8
<0.8
<0.8
30
33 J
31 J
01/26/17
3.41
0.8
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<0.5
<0.8
<0.8
<4.0
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
NA
NA
NA
11/02/17
<10
<0.5
<0.5
<0.5
1 <0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<0.5
<0.8
<0.8
<4.0
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
NA
NA
NA
TP-1
05/30/18
3.21
<0.5
<0.5
<0.5
2.7
0.54
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
2.41
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
11/14/18
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
<4.0
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
08/14/19
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
<4.0
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
01/26/17
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<0.5
<0.8
<0.8
<4.0
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
NA
NA
NA
11/02/17
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<0.5
<0.8
<0.8
<4.0
<8.0
1 <4.0
<4.0
<0.8
<0.8
<0.8
<0.8
NA
NA
NA
TP-2
05/30/18
4.91
<0.5
<0.5
<0.5
2.0
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
2.71
<8.0
<4.0
1.21
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
11/14/18
3.9J
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
<4.0
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
08/14/19
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
<4.0
3.4 BJ
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
DEEP MONITORING WELL
01/25/17
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<0.5
<0.8
<0.8
<4.0
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
NA
NA
NA
05/30/18
<10
<0.5
<0.5
<0.5
0.49J
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
2.4.1
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
M W-10
11/14/18
2.5.1
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
<4.0
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
08/14/19
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<1.0
<0.8
<0.8
1.1.1
2.6BJ
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
WATER SUPPLY WELLS
5/30/2018
<10
<0.5
<0.5
<0.5
1.0
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
<4.0
<8.0
<4.0
<4.0
<0.8
<0.8
<0.8
<0.8
<100
<75
<75
WSW-3
11/14/18
<10
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<5.0
<0.5
<0.5
<1.0
<0.8
<0.8
<4.0
<8.0
<4.0
<4.0
<0.8
1.1
1.6
<0.8
<100
<75
<75
NCAC 2L GWQS
6,000
1
0.6
70
3
NS
70
NS
20
600
20
80
2000
3
4,000
6,000
700
300
30
6
200
200
700
400
Notes: 1) Compounds detected in one or more samples are shown. * Dibenzofuran (1.01 µg/L) was detected in MW-6R during the 11/14/18 sampling event.
2) Concentrations are reported in micrograms per liter (µg/L).
3) NCAC 2L GWQS = North Carolina Administrative Code Subchapter 2L Groundwater Quality Standards (April 1, 2013).
4) Values in BOLD were detected above the method detection limit. Values shaded are above the NCAC 2L GWQS.
5) J = Estimated value above the detection limit.
6) NS=Standard not established
7) NA = Not analyzed
8) B = Detected in the laboratory method blank

APPENDIX A
Analytical Reports and Chain of Custody Records

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Terracon Consultants, Inc.
2701 Westport Road
Charlotte, NC 28208
Attention: Flora D'Souza
Project Name: Mt. Pleasant Maintenance Yard
Project Number: 71177023
Lot Number:UH15076, UH15078 & UH15079
Date Completed:09/03/2019
09/03/2019 10:22 PM
Approved and released by:
Project Manager: Cathy S. Dover
P�. F d
AM
AC CF ED I T E D
qB
11900 ELAP
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
1 of 198

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terracon Consultants, Inc.
Lot Number: UH15076
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
VPH
Surrogate recovery for sample UH15076-003 (MW-6R) was outside control limits. Evidence of matrix
interference is present; therefore, re -analysis was not performed.
EPH
The method blank for prep batch 27085 contained C9-C18 Aliphatic range greater than the acceptance
criteria. The associated samples: UH15076-001 (MW-4R) and UH15076-002(MW-5), did not contain
detections for the target analyte; therefore, re -extraction of the samples was not performed. The data has
been reported.
C9-Cl8 Aliphatic was detected above the reporting limit (RL) in the method blank associated with prep
batch 27085 as well as in the following sample: UH15076-003 (MW-6R). This associated sample was re -
extracted and re -analyzed outside of holding time. Both sets of data have been reported.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
2 of 198

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terracon Consultants, Inc.
Lot Number: UH15078
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
EPH
The method blank for prep batch 27085 contained C9-C18 Aliphatic range greater than the acceptance
criteria. The associated samples: UH15078-001 (MW-1) and UH15078-002(MW-10), did not contain
detections for the target analyte; therefore, re -extraction of the samples was not performed. The data has
been reported.
C9-Cl8 Aliphatic was detected above the reporting limit (RL) in the method blank associated with prep
batch 27085 as well as in the following sample: UH15077-002 (MW-9). This associated sample was re -
extracted and re -analyzed outside of holding time. Both sets of data have been reported.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
3 of 198

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Terracon Consultants, Inc.
Lot Number: UH15079
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved NELAC standards, the Shealy Environmental Services, Inc. ("Shealy") Quality
Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy policies. Any
exceptions to the NELAC standards, the QAMP, SOPS or policies are qualified on the results page or
discussed below.
SVOA 8270E
Surrogate recovery for sample UH15079-002 (TP-2) was outside control limits. Re -extraction was
performed outside of holding time with acceptable results. Both sets of data have been reported.
EPH
The method blank for prep batch 27085 contained C9-C18 Aliphatic range greater than the acceptance
criteria. The associated sample UH15079-003 (MW-7), did not contain detections for the target analyte;
therefore, re -extraction of the samples was not performed. The data has been reported.
C9-Cl8 Aliphatic was detected above the reporting limit (RL) in the method blank associated with prep
batch 27085 as well as in the following samples: UH15079-001 (TP-1), UH15079-002 (TP-2), and
UH15079-004 (MW-8). This associated sample were re -extracted outside of holding time. Both sets of
data have been reported.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the
cover page.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
4 of 198

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Terracon Consultants, Inc.
Lot Number: UH15076
Project Name: Mt. Pleasant Maintenance Yard
Project Number: 71177023
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
MW-4R
Aqueous
08/14/20191315
08/15/2019
002
MW-5
Aqueous
08/14/20191305
08/15/2019
003
MW-6R
Aqueous
08/14/20191410
08/15/2019
(3 samples)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
5 of 198

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Terracon Consultants, Inc.
Lot Number: UH15078
Project Name: Mt. Pleasant Maintenance Yard
Project Number: 71177023
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
MW-1
Aqueous
08/14/20191435
08/15/2019
002
MW-9
Aqueous
08/14/20191535
08/15/2019
003
MW-10
Aqueous
08/14/20191540
08/15/2019
004
Trip Blank
Aqueous
08/14/2019
08/15/2019
(4 samples)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
6 of 198

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Terracon Consultants, Inc.
Lot Number: UH15079
Project Name: Mt. Pleasant Maintenance Yard
Project Number: 71177023
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
TIP-1
Aqueous
08/14/20191015
08/15/2019
002
TIP-2
Aqueous
08/14/20191025
08/15/2019
003
MW-7
Aqueous
08/14/20191135
08/15/2019
004
MW-8
Aqueous
08/14/20191145
08/15/2019
(4 samples)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
7 of 198

SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
Terracon Consultants, Inc.
Lot Number: UH15076
Project Name: Mt. Pleasant Maintenance Yard
Project Number: 71177023
Sample Sample ID
Matrix Parameter Method
Result
Q
Units
Page
001
MW-4R
Aqueous Acetone 8260D
5.1
J
ug/L
5
002
MW-5
Aqueous Diethylphthalate 8270E
24
ug/L
15
003
MW-6R
Aqueous Cyclohexane 8260D
1.1
ug/L
21
003
MW-6R
Aqueous Isopropylbenzene 8260D
1.5
ug/L
21
003
MW-6R
Aqueous Methylcyclohexane 8260D
2.5
J
ug/L
21
003
MW-6R
Aqueous Acenaphthene 8270E
2.5
ug/L
23
003
MW-6R
Aqueous Anthracene 8270E
0.42
J
ug/L
23
003
MW-6R
Aqueous Fluorene 8270E
3.0
ug/L
23
003
MW-6R
Aqueous 2-Methylnaphthalene 8270E
0.29
J
ug/L
24
003
MW-6R
Aqueous Naphthalene 8270E
0.49
J
ug/L
24
003
MW-6R
Aqueous Phenanthrene 8270E
1.4
ug/L
24
003
MW-6R
Aqueous C11 - C22 Aromatics MADEP-EPH-
410
H
ug/L
25
003
MW-6R
Aqueous C5 - C8 Aliphatics MADEP-VPH-
17
J
ug/L
27
003
MW-6R
Aqueous C9 - C12 Aliphatics MADEP-VPH-
110
ug/L
27
003
MW-6R
Aqueous C9 - C10 Aromatics MADEP-VPH-
99
ug/L
28
(15 detections)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
8 of 198

SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
Terracon Consultants, Inc.
Lot Number: UH15078
Project Name: Mt. Pleasant Maintenance Yard
Project Number: 71177023
Sample Sample ID
Matrix Parameter Method
Result
Q
Units
Page
001
MW-1
Aqueous Caprolactam 8270E
2.6
BJ
ug/L
7
002
MW-9
Aqueous Acetone 8260D
6.2
J
ug/L
13
002
MW-9
Aqueous Cyclohexane 8260D
0.45
J
ug/L
13
002
MW-9
Aqueous Isopropylbenzene 8260D
0.65
ug/L
13
002
MW-9
Aqueous Acenaphthene 8270E
0.28
J
ug/L
15
002
MW-9
Aqueous Caprolactam 8270E
5.2
BJ
ug/L
15
002
MW-9
Aqueous bis(2-Ethylhexyl)phthalate 8270E
2.3
J
ug/L
15
002
MW-9
Aqueous Fluorene 8270E
0.23
J
ug/L
15
002
MW-9
Aqueous C5 - C8 Aliphatics MADEP-VPH-
31
J
ug/L
21
002
MW-9
Aqueous C9 - C12 Aliphatics MADEP-VPH-
33
J
ug/L
21
002
MW-9
Aqueous C9 - C10 Aromatics MADEP-VPH-
30
ug/L
22
003
MW-10
Aqueous Caprolactam 8270E
2.6
BJ
ug/L
25
003
MW-10
Aqueous bis(2-Ethylhexyl)phthalate 8270E
1.1
J
ug/L
25
(13 detections)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
9 of 198

SHEALY ENVIRONMENTAL SERVICES, INC.
Detection Summary
Terracon Consultants, Inc.
Lot Number: UH15079
Project Name: Mt. Pleasant Maintenance Yard
Project Number: 71177023
Sample Sample ID
Matrix Parameter Method
Result
Q
Units
Page
002
TP-2
Aqueous Caprolactam 8270E
3.4
BJ
ug/L
17
004
MW-8
Aqueous Acetone 8260D
4.7
J
ug/L
35
004
MW-8
Aqueous Methyl tertiary butyl ether 8260D
1.4
ug/L
35
004
MW-8
Aqueous Caprolactam 8270E
3.3
BJ
ug/L
37
004
MW-8
Aqueous C9 - C10 Aromatics MADEP-VPH-
7.2
J
ug/L
44
(5 detections)
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
10 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-001
Description: MW-4R Matrix: Aqueous
Date Sampled:08/14/2019 1315 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 08/17/2019 0014 ALR1
26199
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
5.1 J
10
4.0
ug/L
1
Benzene
71-43-2
8260D
ND
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
ND
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
ND
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
ND
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
ND
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
ND
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
ND
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
ND
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
0.50
0.40
ug/L
1
Cyclohexane
110-82-7
8260D
ND
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
ND
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
ND
0.50
0.40
ug/L
1
1,3-Dichlorobenzene
541-73-1
8260D
ND
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
0.50
0.40
ug/L
1
Dichlorodifluoromethane
75-71-8
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
8260D
ND
0.50
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
0.50
0.40
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
ND
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Isopropylbenzene
98-82-8
8260D
ND
0.50
0.40
ug/L
1
Methyl acetate
79-20-9
8260D
ND
1.0
0.40
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
0.50
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylcyclohexane
108-87-2
8260D
ND
5.0
0.40
ug/L
1
Methylene chloride
75-09-2
8260D
ND
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
0.50
0.41
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
0.50
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
8260D
ND
1.0
0.42
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
8260D
ND
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
0.50
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
11 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-001
Description: MW-4R Matrix: Aqueous
Date Sampled:08/14/2019 1315 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 08/17/2019 0014 ALR1 26199
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichloroethene
79-01-6
8260D
ND
0.50
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
0.50
0.40
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
100 70-130
102 70-130
106 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
12 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-001
Description: MW-4R Matrix: Aqueous
Date Sampled:08/14/2019 1315 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
8270E
1 08/22/2019 1909 SCD
08/19/2019 1653 26336
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.80
0.20
ug/L
1
Acenaphthylene
208-96-8
8270E
ND
0.80
0.20
ug/L
1
Acetophenone
98-86-2
8270E
ND
4.0
0.50
ug/L
1
Anthracene
120-12-7
8270E
ND
0.80
0.20
ug/L
1
Atrazine
1912-24-9
8270E
ND
4.0
0.50
ug/L
1
Benzaldehyde
100-52-7
8270E
ND
8.0
0.50
ug/L
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.80
0.20
ug/L
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.80
0.20
ug/L
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.80
0.20
ug/L
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.80
0.20
ug/L
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.80
0.20
ug/L
1
1,1'-Biphenyl
92-52-4
8270E
ND
4.0
0.50
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
4.0
0.50
ug/L
1
Butyl benzyl phthalate
85-68-7
8270E
ND
4.0
0.50
ug/L
1
Caprolactam
105-60-2
8270E
ND
8.0
1.0
ug/L
1
Carbazole
86-74-8
8270E
ND
4.0
0.50
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
4.0
0.50
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
4.0
0.50
ug/L
1
4-Chloroaniline
106-47-8
8270E
ND
8.0
0.50
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
4.0
0.50
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
4.0
0.50
ug/L
1
2-Chloronaphthalene
91-58-7
8270E
ND
4.0
0.50
ug/L
1
2-Chlorophenol
95-57-8
8270E
ND
4.0
0.50
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
4.0
0.50
ug/L
1
Chrysene
218-01-9
8270E
ND
0.80
0.20
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.80
0.20
ug/L
1
Dibenzofuran
132-64-9
8270E
ND
4.0
0.50
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
4.0
1.8
ug/L
1
2,4-Dichlorophenol
120-83-2
8270E
ND
8.0
1.0
ug/L
1
Diethylphthalate
84-66-2
8270E
ND
4.0
0.50
ug/L
1
Dimethyl phthalate
131-11-3
8270E
ND
4.0
0.50
ug/L
1
2,4-Dimethylphenol
105-67-9
8270E
ND
4.0
1.0
ug/L
1
Di-n-butyl phthalate
84-74-2
8270E
ND
4.0
0.50
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
20
1.0
ug/L
1
2,4-Dinitrophenol
51-28-5
8270E
ND
20
1.0
ug/L
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
8.0
0.50
ug/L
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
8.0
0.50
ug/L
1
Di-n-octylphthalate
117-84-0
8270E
ND
4.0
0.50
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
4.0
0.50
ug/L
1
Fluoranthene
206-44-0
8270E
ND
0.80
0.20
ug/L
1
Fluorene
86-73-7
8270E
ND
0.80
0.20
ug/L
1
Hexachlorobenzene
118-74-1
8270E
ND
4.0
0.50
ug/L
1
Hexachlorobutadiene
87-68-3
8270E
ND
4.0
0.50
ug/L
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
20
2.0
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
13 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-001
Description: MW-4R Matrix: Aqueous
Date Sampled:08/14/2019 1315 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 08/22/2019 1909 SCD 08/19/2019 1653 26336
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexachloroethane
67-72-1
8270E
ND
4.0
1.0
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.80
0.20
ug/L
1
Isophorone
78-59-1
8270E
ND
4.0
0.50
ug/L
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.80
0.20
ug/L
1
2-Methylphenol
95-48-7
8270E
ND
4.0
1.0
ug/L
1
3+4-Methylphenol
106-44-5
8270E
ND
4.0
1.5
ug/L
1
Naphthalene
91-20-3
8270E
ND
0.80
0.20
ug/L
1
2-Nitroaniline
88-74-4
8270E
ND
8.0
0.50
ug/L
1
3-Nitroaniline
99-09-2
8270E
ND
8.0
1.0
ug/L
1
4-Nitroaniline
100-01-6
8270E
ND
8.0
1.5
ug/L
1
Nitrobenzene
98-95-3
8270E
ND
4.0
1.5
ug/L
1
2-Nitrophenol
88-75-5
8270E
ND
4.0
1.0
ug/L
1
4-Nitrophenol
100-02-7
8270E
ND
20
2.0
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
4.0
0.50
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
4.0
0.50
ug/L
1
Pentachlorophenol
87-86-5
8270E
ND
20
2.0
ug/L
1
Phenanthrene
85-01-8
8270E
ND
0.80
0.20
ug/L
1
Phenol
108-95-2
8270E
ND
4.0
0.50
ug/L
1
Pyrene
129-00-0
8270E
ND
0.80
0.20
ug/L
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
4.0
0.50
ug/L
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
4.0
0.50
ug/L
1
Run
1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
50
37-129
2-Fluorophenol
35
24-127
Nitrobenzene-d5
55
38-127
Phenol-d5
47
28-128
Terphenyl-d14
67
10-148
2,4,6-Tribromophenol
67
35-144
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
14 of 198

MADEP EPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-001
Description: MW-4R Matrix: Aqueous
Date Sampled:08/14/2019 1315 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 08/30/2019 0225 CHG 08/26/2019 2111 27084
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C11 - C22 Aromatics MADEP-EPH-04 ND 100 100 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl (aromatic)
2-Fluorobiphenyl (fractionation 1)
2-Bromonaphthalene (fractionation 2)
78 40-140
115 40-140
104 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
15 of 198

MADEP EPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-001
Description: MW-4R Matrix: Aqueous
Date Sampled:08/14/2019 1315 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 08/29/2019 2258 CHG 08/26/2019 2111 27085
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C18 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 1
C19 - C36 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
79 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
16 of 198

MADEP VPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-001
Description: MW-4R Matrix: Aqueous
Date Sampled:08/14/2019 1315 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 08/16/2019 2121 STM 26200
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C5 - C8 Aliphatics MADEP-VPH- ND 75 15 ug/L 1
C9 - C12 Aliphatics MADEP-VPH- ND 75 15 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
102 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
17 of 198

MADEP VPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-001
Description: MW-4R Matrix: Aqueous
Date Sampled:08/14/2019 1315 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 08/16/2019 2121 STM 26201
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C10 Aromatics MADEP-VPH- ND 25 5.0 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
102 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
18 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-002
Description: MW-5 Matrix: Aqueous
Date Sampled:08/14/2019 1305 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 08/17/2019 0038 ALR1
26199
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
ND
10
4.0
ug/L
1
Benzene
71-43-2
8260D
ND
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
ND
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
ND
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
ND
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
ND
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
ND
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
ND
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
ND
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
0.50
0.40
ug/L
1
Cyclohexane
110-82-7
8260D
ND
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
ND
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
ND
0.50
0.40
ug/L
1
1,3-Dichlorobenzene
541-73-1
8260D
ND
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
0.50
0.40
ug/L
1
Dichlorodifluoromethane
75-71-8
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
8260D
ND
0.50
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
0.50
0.40
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
ND
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Isopropylbenzene
98-82-8
8260D
ND
0.50
0.40
ug/L
1
Methyl acetate
79-20-9
8260D
ND
1.0
0.40
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
0.50
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylcyclohexane
108-87-2
8260D
ND
5.0
0.40
ug/L
1
Methylene chloride
75-09-2
8260D
ND
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
0.50
0.41
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
0.50
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
8260D
ND
1.0
0.42
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
8260D
ND
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
0.50
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
19 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-002
Description: MW-5 Matrix: Aqueous
Date Sampled:08/14/2019 1305 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 08/17/2019 0038 ALR1 26199
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichloroethene
79-01-6
8260D
ND
0.50
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
0.50
0.40
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
104 70-130
104 70-130
111 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
20 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-002
Description: MW-5 Matrix: Aqueous
Date Sampled:08/14/2019 1305 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
8270E
1 08/22/2019 1933 SCD
08/19/2019 1653 26336
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.80
0.20
ug/L
1
Acenaphthylene
208-96-8
8270E
ND
0.80
0.20
ug/L
1
Acetophenone
98-86-2
8270E
ND
4.0
0.50
ug/L
1
Anthracene
120-12-7
8270E
ND
0.80
0.20
ug/L
1
Atrazine
1912-24-9
8270E
ND
4.0
0.50
ug/L
1
Benzaldehyde
100-52-7
8270E
ND
8.0
0.50
ug/L
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.80
0.20
ug/L
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.80
0.20
ug/L
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.80
0.20
ug/L
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.80
0.20
ug/L
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.80
0.20
ug/L
1
1,1'-Biphenyl
92-52-4
8270E
ND
4.0
0.50
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
4.0
0.50
ug/L
1
Butyl benzyl phthalate
85-68-7
8270E
ND
4.0
0.50
ug/L
1
Caprolactam
105-60-2
8270E
ND
8.0
1.0
ug/L
1
Carbazole
86-74-8
8270E
ND
4.0
0.50
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
4.0
0.50
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
4.0
0.50
ug/L
1
4-Chloroaniline
106-47-8
8270E
ND
8.0
0.50
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
4.0
0.50
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
4.0
0.50
ug/L
1
2-Chloronaphthalene
91-58-7
8270E
ND
4.0
0.50
ug/L
1
2-Chlorophenol
95-57-8
8270E
ND
4.0
0.50
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
4.0
0.50
ug/L
1
Chrysene
218-01-9
8270E
ND
0.80
0.20
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.80
0.20
ug/L
1
Dibenzofuran
132-64-9
8270E
ND
4.0
0.50
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
4.0
1.8
ug/L
1
2,4-Dichlorophenol
120-83-2
8270E
ND
8.0
1.0
ug/L
1
Diethylphthalate
84-66-2
8270E
24
4.0
0.50
ug/L
1
Dimethyl phthalate
131-11-3
8270E
ND
4.0
0.50
ug/L
1
2,4-Dimethylphenol
105-67-9
8270E
ND
4.0
1.0
ug/L
1
Di-n-butyl phthalate
84-74-2
8270E
ND
4.0
0.50
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
20
1.0
ug/L
1
2,4-Dinitrophenol
51-28-5
8270E
ND
20
1.0
ug/L
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
8.0
0.50
ug/L
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
8.0
0.50
ug/L
1
Di-n-octylphthalate
117-84-0
8270E
ND
4.0
0.50
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
4.0
0.50
ug/L
1
Fluoranthene
206-44-0
8270E
ND
0.80
0.20
ug/L
1
Fluorene
86-73-7
8270E
ND
0.80
0.20
ug/L
1
Hexachlorobenzene
118-74-1
8270E
ND
4.0
0.50
ug/L
1
Hexachlorobutadiene
87-68-3
8270E
ND
4.0
0.50
ug/L
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
20
2.0
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
21 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-002
Description: MW-5 Matrix: Aqueous
Date Sampled:08/14/2019 1305 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 08/22/2019 1933 SCD 08/19/2019 1653 26336
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexachloroethane
67-72-1
8270E
ND
4.0
1.0
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.80
0.20
ug/L
1
Isophorone
78-59-1
8270E
ND
4.0
0.50
ug/L
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.80
0.20
ug/L
1
2-Methylphenol
95-48-7
8270E
ND
4.0
1.0
ug/L
1
3+4-Methylphenol
106-44-5
8270E
ND
4.0
1.5
ug/L
1
Naphthalene
91-20-3
8270E
ND
0.80
0.20
ug/L
1
2-Nitroaniline
88-74-4
8270E
ND
8.0
0.50
ug/L
1
3-Nitroaniline
99-09-2
8270E
ND
8.0
1.0
ug/L
1
4-Nitroaniline
100-01-6
8270E
ND
8.0
1.5
ug/L
1
Nitrobenzene
98-95-3
8270E
ND
4.0
1.5
ug/L
1
2-Nitrophenol
88-75-5
8270E
ND
4.0
1.0
ug/L
1
4-Nitrophenol
100-02-7
8270E
ND
20
2.0
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
4.0
0.50
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
4.0
0.50
ug/L
1
Pentachlorophenol
87-86-5
8270E
ND
20
2.0
ug/L
1
Phenanthrene
85-01-8
8270E
ND
0.80
0.20
ug/L
1
Phenol
108-95-2
8270E
ND
4.0
0.50
ug/L
1
Pyrene
129-00-0
8270E
ND
0.80
0.20
ug/L
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
4.0
0.50
ug/L
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
4.0
0.50
ug/L
1
Run
1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
48
37-129
2-Fluorophenol
31
24-127
Nitrobenzene-d5
53
38-127
Phenol-d5
41
28-128
Terphenyl-d14
77
10-148
2,4,6-Tribromophenol
55
35-144
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
22 of 198

MADEP EPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-002
Description: MW-5 Matrix: Aqueous
Date Sampled:08/14/2019 1305 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 08/30/2019 0254 CHG 08/26/2019 2111 27084
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C11 - C22 Aromatics MADEP-EPH-04 ND 100 100 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl (aromatic)
2-Fluorobiphenyl (fractionation 1)
2-Bromonaphthalene (fractionation 2)
84 40-140
129 40-140
123 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
23 of 198

MADEP EPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-002
Description: MW-5 Matrix: Aqueous
Date Sampled:08/14/2019 1305 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 08/29/2019 2327 CHG 08/26/2019 2111 27085
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C18 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 1
C19 - C36 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
78 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
24 of 198

MADEP VPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-002
Description: MW-5 Matrix: Aqueous
Date Sampled:08/14/2019 1305 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 08/16/2019 2150 STM 26200
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C5 - C8 Aliphatics MADEP-VPH- ND 75 15 ug/L 1
C9 - C12 Aliphatics MADEP-VPH- ND 75 15 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
96 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
25 of 198

MADEP VPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-002
Description: MW-5 Matrix: Aqueous
Date Sampled:08/14/2019 1305 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 08/16/2019 2150 STM 26201
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C10 Aromatics MADEP-VPH- ND 25 5.0 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
96 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
26 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-003
Description: MW-6R Matrix: Aqueous
Date Sampled:08/14/2019 1410 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 08/17/2019 0102 ALR1
26199
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
ND
10
4.0
ug/L
1
Benzene
71-43-2
8260D
ND
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
ND
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
ND
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
ND
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
ND
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
ND
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
ND
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
ND
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
0.50
0.40
ug/L
1
Cyclohexane
110-82-7
8260D
1.1
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
ND
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
ND
0.50
0.40
ug/L
1
1,3-Dichlorobenzene
541-73-1
8260D
ND
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
0.50
0.40
ug/L
1
Dichlorodifluoromethane
75-71-8
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
8260D
ND
0.50
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
0.50
0.40
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
ND
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Isopropylbenzene
98-82-8
8260D
1.5
0.50
0.40
ug/L
1
Methyl acetate
79-20-9
8260D
ND
1.0
0.40
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
0.50
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylcyclohexane
108-87-2
8260D
2.5 J
5.0
0.40
ug/L
1
Methylene chloride
75-09-2
8260D
ND
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
0.50
0.41
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
0.50
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
8260D
ND
1.0
0.42
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
8260D
ND
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
0.50
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
27 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-003
Description: MW-6R Matrix: Aqueous
Date Sampled:08/14/2019 1410 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 08/17/2019 0102 ALR1 26199
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichloroethene
79-01-6
8260D
ND
0.50
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
0.50
0.40
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
103 70-130
103 70-130
108 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
28 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-003
Description: MW-6R Matrix: Aqueous
Date Sampled:08/14/2019 1410 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
8270E
1 08/24/2019 1607 SCD
08/19/2019 1653 26336
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9
8270E
2.5
0.80
0.20
ug/L
1
Acenaphthylene
208-96-8
8270E
ND
0.80
0.20
ug/L
1
Acetophenone
98-86-2
8270E
ND
4.0
0.50
ug/L
1
Anthracene
120-12-7
8270E
0.42 J
0.80
0.20
ug/L
1
Atrazine
1912-24-9
8270E
ND
4.0
0.50
ug/L
1
Benzaldehyde
100-52-7
8270E
ND
8.0
0.50
ug/L
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.80
0.20
ug/L
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.80
0.20
ug/L
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.80
0.20
ug/L
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.80
0.20
ug/L
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.80
0.20
ug/L
1
1,1'-Biphenyl
92-52-4
8270E
ND
4.0
0.50
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
4.0
0.50
ug/L
1
Butyl benzyl phthalate
85-68-7
8270E
ND
4.0
0.50
ug/L
1
Caprolactam
105-60-2
8270E
ND
8.0
1.0
ug/L
1
Carbazole
86-74-8
8270E
ND
4.0
0.50
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
4.0
0.50
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
4.0
0.50
ug/L
1
4-Chloroaniline
106-47-8
8270E
ND
8.0
0.50
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
4.0
0.50
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
4.0
0.50
ug/L
1
2-Chloronaphthalene
91-58-7
8270E
ND
4.0
0.50
ug/L
1
2-Chlorophenol
95-57-8
8270E
ND
4.0
0.50
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
4.0
0.50
ug/L
1
Chrysene
218-01-9
8270E
ND
0.80
0.20
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.80
0.20
ug/L
1
Dibenzofuran
132-64-9
8270E
ND
4.0
0.50
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
4.0
1.8
ug/L
1
2,4-Dichlorophenol
120-83-2
8270E
ND
8.0
1.0
ug/L
1
Diethylphthalate
84-66-2
8270E
ND
4.0
0.50
ug/L
1
Dimethyl phthalate
131-11-3
8270E
ND
4.0
0.50
ug/L
1
2,4-Dimethylphenol
105-67-9
8270E
ND
4.0
1.0
ug/L
1
Di-n-butyl phthalate
84-74-2
8270E
ND
4.0
0.50
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
20
1.0
ug/L
1
2,4-Dinitrophenol
51-28-5
8270E
ND
20
1.0
ug/L
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
8.0
0.50
ug/L
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
8.0
0.50
ug/L
1
Di-n-octylphthalate
117-84-0
8270E
ND
4.0
0.50
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
4.0
0.50
ug/L
1
Fluoranthene
206-44-0
8270E
ND
0.80
0.20
ug/L
1
Fluorene
86-73-7
8270E
3.0
0.80
0.20
ug/L
1
Hexachlorobenzene
118-74-1
8270E
ND
4.0
0.50
ug/L
1
Hexachlorobutadiene
87-68-3
8270E
ND
4.0
0.50
ug/L
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
20
2.0
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
29 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-003
Description: MW-6R Matrix: Aqueous
Date Sampled:08/14/2019 1410 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 08/24/2019 1607 SCD 08/19/2019 1653 26336
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexachloroethane
67-72-1
8270E
ND
4.0
1.0
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.80
0.20
ug/L
1
Isophorone
78-59-1
8270E
ND
4.0
0.50
ug/L
1
2-Methylnaphthalene
91-57-6
8270E
0.29 J
0.80
0.20
ug/L
1
2-Methylphenol
95-48-7
8270E
ND
4.0
1.0
ug/L
1
3+4-Methylphenol
106-44-5
8270E
ND
4.0
1.5
ug/L
1
Naphthalene
91-20-3
8270E
0.49 J
0.80
0.20
ug/L
1
2-Nitroaniline
88-74-4
8270E
ND
8.0
0.50
ug/L
1
3-Nitroaniline
99-09-2
8270E
ND
8.0
1.0
ug/L
1
4-Nitroaniline
100-01-6
8270E
ND
8.0
1.5
ug/L
1
Nitrobenzene
98-95-3
8270E
ND
4.0
1.5
ug/L
1
2-Nitrophenol
88-75-5
8270E
ND
4.0
1.0
ug/L
1
4-Nitrophenol
100-02-7
8270E
ND
20
2.0
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
4.0
0.50
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
4.0
0.50
ug/L
1
Pentachlorophenol
87-86-5
8270E
ND
20
2.0
ug/L
1
Phenanthrene
85-01-8
8270E
1.4
0.80
0.20
ug/L
1
Phenol
108-95-2
8270E
ND
4.0
0.50
ug/L
1
Pyrene
129-00-0
8270E
ND
0.80
0.20
ug/L
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
4.0
0.50
ug/L
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
4.0
0.50
ug/L
1
Run
1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
54
37-129
2-Fluorophenol
33
24-127
Nitrobenzene-d5
60
38-127
Phenol-d5
45
28-128
Terphenyl-d14
70
10-148
2,4,6-Tribromophenol
73
35-144
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
30 of 198

MADEP EPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-003
Description: MW-6R Matrix: Aqueous
Date Sampled:08/14/2019 1410 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 MADEP-EPH- MADEP-EPH-04 1 08/30/2019 1604 CHG 08/29/2019 0911 27388
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C11 - C22 Aromatics MADEP-EPH- 410 H 100 100 ug/L 2
Run 2 Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl (aromatic) H 95 40-140
2-Fluorobiphenyl (fractionation 1) H 105 40-140
2-Bromonaphthalene (fractionation 2) H 97 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
31 of 198

MADEP EPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-003
Description: MW-6R Matrix: Aqueous
Date Sampled:08/14/2019 1410 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 MADEP-EPH- MADEP-EPH-04 1 08/30/2019 0819 CHG 08/29/2019 0911 27385
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C18 Aliphatics MADEP-EPH-04 ND H 100 100 ug/L 2
C19 - C36 Aliphatics MADEP-EPH-04 ND H 100 100 ug/L 2
Run 2 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic) H 73 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
32 of 198

MADEP VPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-003
Description: MW-6R Matrix: Aqueous
Date Sampled:08/14/2019 1410 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 08/16/2019 2219 STM 26200
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C5 - C8 Aliphatics MADEP-VPH- 17 J 75 15 ug/L 1
C9 - C12 Aliphatics MADEP-VPH- 110 75 15 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
N 138 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
33 of 198

MADEP VPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15076-003
Description: MW-6R Matrix: Aqueous
Date Sampled:08/14/2019 1410 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 08/16/2019 2219 STM 26201
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C10 Aromatics MADEP-VPH- 99 25 5.0 ug/L 1
Run Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
122 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
34 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-001
Description: MW-1 Matrix: Aqueous
Date Sampled:08/14/2019 1435 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 08/17/2019 0125 ALR1
26199
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
ND
10
4.0
ug/L
1
Benzene
71-43-2
8260D
ND
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
ND
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
ND
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
ND
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
ND
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
ND
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
ND
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
ND
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
0.50
0.40
ug/L
1
Cyclohexane
110-82-7
8260D
ND
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
ND
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
ND
0.50
0.40
ug/L
1
1,3-Dichlorobenzene
541-73-1
8260D
ND
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
0.50
0.40
ug/L
1
Dichlorodifluoromethane
75-71-8
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
8260D
ND
0.50
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
0.50
0.40
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
ND
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Isopropylbenzene
98-82-8
8260D
ND
0.50
0.40
ug/L
1
Methyl acetate
79-20-9
8260D
ND
1.0
0.40
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
0.50
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylcyclohexane
108-87-2
8260D
ND
5.0
0.40
ug/L
1
Methylene chloride
75-09-2
8260D
ND
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
0.50
0.41
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
0.50
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
8260D
ND
1.0
0.42
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
8260D
ND
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
0.50
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
35 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-001
Description: MW-1 Matrix: Aqueous
Date Sampled:08/14/2019 1435 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 08/17/2019 0125 ALR1 26199
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichloroethene
79-01-6
8260D
ND
0.50
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
0.50
0.40
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
102 70-130
102 70-130
110 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
36 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-001
Description: MW-1 Matrix: Aqueous
Date Sampled:08/14/2019 1435 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
8270E
1 08/22/2019 2022 SCD
08/19/2019 1653 26336
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.80
0.20
ug/L
1
Acenaphthylene
208-96-8
8270E
ND
0.80
0.20
ug/L
1
Acetophenone
98-86-2
8270E
ND
4.0
0.50
ug/L
1
Anthracene
120-12-7
8270E
ND
0.80
0.20
ug/L
1
Atrazine
1912-24-9
8270E
ND
4.0
0.50
ug/L
1
Benzaldehyde
100-52-7
8270E
ND
8.0
0.50
ug/L
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.80
0.20
ug/L
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.80
0.20
ug/L
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.80
0.20
ug/L
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.80
0.20
ug/L
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.80
0.20
ug/L
1
1,1'-Biphenyl
92-52-4
8270E
ND
4.0
0.50
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
4.0
0.50
ug/L
1
Butyl benzyl phthalate
85-68-7
8270E
ND
4.0
0.50
ug/L
1
Caprolactam
105-60-2
8270E
2.6 BJ
8.0
1.0
ug/L
1
Carbazole
86-74-8
8270E
ND
4.0
0.50
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
4.0
0.50
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
4.0
0.50
ug/L
1
4-Chloroaniline
106-47-8
8270E
ND
8.0
0.50
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
4.0
0.50
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
4.0
0.50
ug/L
1
2-Chloronaphthalene
91-58-7
8270E
ND
4.0
0.50
ug/L
1
2-Chlorophenol
95-57-8
8270E
ND
4.0
0.50
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
4.0
0.50
ug/L
1
Chrysene
218-01-9
8270E
ND
0.80
0.20
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.80
0.20
ug/L
1
Dibenzofuran
132-64-9
8270E
ND
4.0
0.50
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
4.0
1.8
ug/L
1
2,4-Dichlorophenol
120-83-2
8270E
ND
8.0
1.0
ug/L
1
Diethylphthalate
84-66-2
8270E
ND
4.0
0.50
ug/L
1
Dimethyl phthalate
131-11-3
8270E
ND
4.0
0.50
ug/L
1
2,4-Dimethylphenol
105-67-9
8270E
ND
4.0
1.0
ug/L
1
Di-n-butyl phthalate
84-74-2
8270E
ND
4.0
0.50
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
20
1.0
ug/L
1
2,4-Dinitrophenol
51-28-5
8270E
ND
20
1.0
ug/L
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
8.0
0.50
ug/L
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
8.0
0.50
ug/L
1
Di-n-octylphthalate
117-84-0
8270E
ND
4.0
0.50
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
4.0
0.50
ug/L
1
Fluoranthene
206-44-0
8270E
ND
0.80
0.20
ug/L
1
Fluorene
86-73-7
8270E
ND
0.80
0.20
ug/L
1
Hexachlorobenzene
118-74-1
8270E
ND
4.0
0.50
ug/L
1
Hexachlorobutadiene
87-68-3
8270E
ND
4.0
0.50
ug/L
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
20
2.0
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
37 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-001
Description: MW-1 Matrix: Aqueous
Date Sampled:08/14/2019 1435 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 08/22/2019 2022 SCD 08/19/2019 1653 26336
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexachloroethane
67-72-1
8270E
ND
4.0
1.0
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.80
0.20
ug/L
1
Isophorone
78-59-1
8270E
ND
4.0
0.50
ug/L
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.80
0.20
ug/L
1
2-Methylphenol
95-48-7
8270E
ND
4.0
1.0
ug/L
1
3+4-Methylphenol
106-44-5
8270E
ND
4.0
1.5
ug/L
1
Naphthalene
91-20-3
8270E
ND
0.80
0.20
ug/L
1
2-Nitroaniline
88-74-4
8270E
ND
8.0
0.50
ug/L
1
3-Nitroaniline
99-09-2
8270E
ND
8.0
1.0
ug/L
1
4-Nitroaniline
100-01-6
8270E
ND
8.0
1.5
ug/L
1
Nitrobenzene
98-95-3
8270E
ND
4.0
1.5
ug/L
1
2-Nitrophenol
88-75-5
8270E
ND
4.0
1.0
ug/L
1
4-Nitrophenol
100-02-7
8270E
ND
20
2.0
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
4.0
0.50
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
4.0
0.50
ug/L
1
Pentachlorophenol
87-86-5
8270E
ND
20
2.0
ug/L
1
Phenanthrene
85-01-8
8270E
ND
0.80
0.20
ug/L
1
Phenol
108-95-2
8270E
ND
4.0
0.50
ug/L
1
Pyrene
129-00-0
8270E
ND
0.80
0.20
ug/L
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
4.0
0.50
ug/L
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
4.0
0.50
ug/L
1
Run
1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
49
37-129
2-Fluorophenol
45
24-127
Nitrobenzene-d5
52
38-127
Phenol-d5
43
28-128
Terphenyl-d14
67
10-148
2,4,6-Tribromophenol
59
35-144
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
38 of 198

MADEP EPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-001
Description: MW-1 Matrix: Aqueous
Date Sampled:08/14/2019 1435 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 08/30/2019 0324 CHG 08/26/2019 2111 27084
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C11 - C22 Aromatics MADEP-EPH-04 ND 110 110 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl (aromatic)
2-Fluorobiphenyl (fractionation 1)
2-Bromonaphthalene (fractionation 2)
83 40-140
127 40-140
98 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
39 of 198

MADEP EPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-001
Description: MW-1 Matrix: Aqueous
Date Sampled:08/14/2019 1435 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 08/29/2019 2357 CHG 08/26/2019 2111 27085
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C18 Aliphatics MADEP-EPH-04 ND 110 110 ug/L 1
C19 - C36 Aliphatics MADEP-EPH-04 ND 110 110 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
81 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
40 of 198

MADEP VPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-001
Description: MW-1 Matrix: Aqueous
Date Sampled:08/14/2019 1435 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 08/16/2019 2247 STM 26200
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C5 - C8 Aliphatics MADEP-VPH- ND 75 15 ug/L 1
C9 - C12 Aliphatics MADEP-VPH- ND 75 15 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
98 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
41 of 198

MADEP VPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-001
Description: MW-1 Matrix: Aqueous
Date Sampled:08/14/2019 1435 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 08/16/2019 2247 STM 26201
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C10 Aromatics MADEP-VPH- ND 25 5.0 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
100 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
42 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-002
Description: MW-9 Matrix: Aqueous
Date Sampled:08/14/2019 1535 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 08/17/2019 0149 ALR1
26199
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
6.2 J
10
4.0
ug/L
1
Benzene
71-43-2
8260D
ND
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
ND
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
ND
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
ND
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
ND
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
ND
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
ND
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
ND
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
0.50
0.40
ug/L
1
Cyclohexane
110-82-7
8260D
0.45 J
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
ND
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
ND
0.50
0.40
ug/L
1
1,3-Dichlorobenzene
541-73-1
8260D
ND
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
0.50
0.40
ug/L
1
Dichlorodifluoromethane
75-71-8
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
8260D
ND
0.50
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
0.50
0.40
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
ND
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Isopropylbenzene
98-82-8
8260D
0.65
0.50
0.40
ug/L
1
Methyl acetate
79-20-9
8260D
ND
1.0
0.40
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
0.50
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylcyclohexane
108-87-2
8260D
ND
5.0
0.40
ug/L
1
Methylene chloride
75-09-2
8260D
ND
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
0.50
0.41
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
0.50
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
8260D
ND
1.0
0.42
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
8260D
ND
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
0.50
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
43 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-002
Description: MW-9 Matrix: Aqueous
Date Sampled:08/14/2019 1535 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 08/17/2019 0149 ALR1 26199
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichloroethene
79-01-6
8260D
ND
0.50
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
0.50
0.40
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
102 70-130
101 70-130
109 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
44 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-002
Description: MW-9 Matrix: Aqueous
Date Sampled:08/14/2019 1535 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
8270E
1 08/22/2019 2047 SCD
08/19/2019 1653 26336
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9
8270E
0.28 J
0.80
0.20
ug/L
1
Acenaphthylene
208-96-8
8270E
ND
0.80
0.20
ug/L
1
Acetophenone
98-86-2
8270E
ND
4.0
0.50
ug/L
1
Anthracene
120-12-7
8270E
ND
0.80
0.20
ug/L
1
Atrazine
1912-24-9
8270E
ND
4.0
0.50
ug/L
1
Benzaldehyde
100-52-7
8270E
ND
8.0
0.50
ug/L
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.80
0.20
ug/L
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.80
0.20
ug/L
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.80
0.20
ug/L
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.80
0.20
ug/L
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.80
0.20
ug/L
1
1,1'-Biphenyl
92-52-4
8270E
ND
4.0
0.50
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
4.0
0.50
ug/L
1
Butyl benzyl phthalate
85-68-7
8270E
ND
4.0
0.50
ug/L
1
Caprolactam
105-60-2
8270E
5.2 BJ
8.0
1.0
ug/L
1
Carbazole
86-74-8
8270E
ND
4.0
0.50
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
4.0
0.50
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
4.0
0.50
ug/L
1
4-Chloroaniline
106-47-8
8270E
ND
8.0
0.50
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
4.0
0.50
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
4.0
0.50
ug/L
1
2-Chloronaphthalene
91-58-7
8270E
ND
4.0
0.50
ug/L
1
2-Chlorophenol
95-57-8
8270E
ND
4.0
0.50
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
4.0
0.50
ug/L
1
Chrysene
218-01-9
8270E
ND
0.80
0.20
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.80
0.20
ug/L
1
Dibenzofuran
132-64-9
8270E
ND
4.0
0.50
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
4.0
1.8
ug/L
1
2,4-Dichlorophenol
120-83-2
8270E
ND
8.0
1.0
ug/L
1
Diethylphthalate
84-66-2
8270E
ND
4.0
0.50
ug/L
1
Dimethyl phthalate
131-11-3
8270E
ND
4.0
0.50
ug/L
1
2,4-Dimethylphenol
105-67-9
8270E
ND
4.0
1.0
ug/L
1
Di-n-butyl phthalate
84-74-2
8270E
ND
4.0
0.50
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
20
1.0
ug/L
1
2,4-Dinitrophenol
51-28-5
8270E
ND
20
1.0
ug/L
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
8.0
0.50
ug/L
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
8.0
0.50
ug/L
1
Di-n-octylphthalate
117-84-0
8270E
ND
4.0
0.50
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
2.3 J
4.0
0.50
ug/L
1
Fluoranthene
206-44-0
8270E
ND
0.80
0.20
ug/L
1
Fluorene
86-73-7
8270E
0.23 J
0.80
0.20
ug/L
1
Hexachlorobenzene
118-74-1
8270E
ND
4.0
0.50
ug/L
1
Hexachlorobutadiene
87-68-3
8270E
ND
4.0
0.50
ug/L
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
20
2.0
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
45 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-002
Description: MW-9 Matrix: Aqueous
Date Sampled:08/14/2019 1535 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 08/22/2019 2047 SCD 08/19/2019 1653 26336
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexachloroethane
67-72-1
8270E
ND
4.0
1.0
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.80
0.20
ug/L
1
Isophorone
78-59-1
8270E
ND
4.0
0.50
ug/L
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.80
0.20
ug/L
1
2-Methylphenol
95-48-7
8270E
ND
4.0
1.0
ug/L
1
3+4-Methylphenol
106-44-5
8270E
ND
4.0
1.5
ug/L
1
Naphthalene
91-20-3
8270E
ND
0.80
0.20
ug/L
1
2-Nitroaniline
88-74-4
8270E
ND
8.0
0.50
ug/L
1
3-Nitroaniline
99-09-2
8270E
ND
8.0
1.0
ug/L
1
4-Nitroaniline
100-01-6
8270E
ND
8.0
1.5
ug/L
1
Nitrobenzene
98-95-3
8270E
ND
4.0
1.5
ug/L
1
2-Nitrophenol
88-75-5
8270E
ND
4.0
1.0
ug/L
1
4-Nitrophenol
100-02-7
8270E
ND
20
2.0
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
4.0
0.50
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
4.0
0.50
ug/L
1
Pentachlorophenol
87-86-5
8270E
ND
20
2.0
ug/L
1
Phenanthrene
85-01-8
8270E
ND
0.80
0.20
ug/L
1
Phenol
108-95-2
8270E
ND
4.0
0.50
ug/L
1
Pyrene
129-00-0
8270E
ND
0.80
0.20
ug/L
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
4.0
0.50
ug/L
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
4.0
0.50
ug/L
1
Run
1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
50
37-129
2-Fluorophenol
36
24-127
Nitrobenzene-d5
59
38-127
Phenol-d5
46
28-128
Terphenyl-d14
70
10-148
2,4,6-Tribromophenol
64
35-144
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
46 of 198

MADEP EPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-002
Description: MW-9 Matrix: Aqueous
Date Sampled:08/14/2019 1535 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run
Prep Method
Analytical Method Dilution
Analysis Date Analyst
Prep Date Batch
1
MADEP-EPH-
MADEP-EPH-04 1
08/28/2019 0055 CHG
08/26/2019 2111 27084
2
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 1704 CHG
08/29/2019 0911 27388
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C11 - C22 Aromatics MADEP-EPH-04 ND 100 100 ug/L 1
Run 1 Acceptance Run 2 Acceptance
Surrogate Q % Recovery Limits Q % Recovery Limits
o - Terphenyl (aromatic)
2-Fluorobiphenyl (fractionation 1)
2-Bromonaphthalene (fractionation 2)
73 40-140 H 95 40-140
122 40-140 H 109 40-140
100 40-140 H 98 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
47 of 198

MADEP EPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-002
Description: MW-9 Matrix: Aqueous
Date Sampled:08/14/2019 1535 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run
Prep Method
Analytical Method Dilution
Analysis Date Analyst
Prep Date Batch
1
MADEP-EPH-
MADEP-EPH-04 1
08/28/2019 0055 CHG
08/26/2019 2111 27084
2
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 1704 CHG
08/29/2019 0911 27388
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C11 - C22 Aromatics MADEP-EPH-04 ND H 100 100 ug/L 2
Run 1 Acceptance Run 2 Acceptance
Surrogate Q % Recovery Limits Q % Recovery Limits
o - Terphenyl (aromatic)
2-Fluorobiphenyl (fractionation 1)
2-Bromonaphthalene (fractionation 2)
73 40-140 H 95 40-140
122 40-140 H 109 40-140
100 40-140 H 98 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
48 of 198

MADEP EPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-002
Description: MW-9 Matrix: Aqueous
Date Sampled:08/14/2019 1535 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run
Prep Method
Analytical Method Dilution
Analysis Date Analyst
Prep Date Batch
1
MADEP-EPH-
MADEP-EPH-04 1
08/27/2019 2127 CHG
08/26/2019 2111 27085
2
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 0918 CHG
08/29/2019 0911 27385
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C18 Aliphatics MADEP-EPH- 110 B 100 100 ug/L 1
C19 - C36 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 1
Run 1 Acceptance Run 2 Acceptance
Surrogate Q % Recovery Limits Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
68 40-140 H 76 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
49 of 198

MADEP EPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-002
Description: MW-9 Matrix: Aqueous
Date Sampled:08/14/2019 1535 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run
Prep Method
Analytical Method Dilution
Analysis Date Analyst
Prep Date Batch
1
MADEP-EPH-
MADEP-EPH-04 1
08/27/2019 2127 CHG
08/26/2019 2111 27085
2
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 0918 CHG
08/29/2019 0911 27385
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C18 Aliphatics MADEP-EPH-04 ND H 100 100 ug/L 2
C19 - C36 Aliphatics MADEP-EPH-04 ND H 100 100 ug/L 2
Run 1 Acceptance Run 2 Acceptance
Surrogate Q % Recovery Limits Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
68 40-140 H 76 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
50 of 198

MADEP VPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-002
Description: MW-9 Matrix: Aqueous
Date Sampled:08/14/2019 1535 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 08/16/2019 2316 STM 26200
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C5 - C8 Aliphatics MADEP-VPH- 31 J 75 15 ug/L 1
C9 - C12 Aliphatics MADEP-VPH- 33 J 75 15 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
118 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
51 of 198

MADEP VPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-002
Description: MW-9 Matrix: Aqueous
Date Sampled:08/14/2019 1535 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 08/16/2019 2316 STM 26201
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C10 Aromatics MADEP-VPH- 30 25 5.0 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
118 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
52 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-003
Description: MW-10 Matrix: Aqueous
Date Sampled:08/14/2019 1540 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 08/17/2019 0213 ALR1
26199
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
ND
10
4.0
ug/L
1
Benzene
71-43-2
8260D
ND
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
ND
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
ND
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
ND
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
ND
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
ND
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
ND
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
ND
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
0.50
0.40
ug/L
1
Cyclohexane
110-82-7
8260D
ND
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
ND
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
ND
0.50
0.40
ug/L
1
1,3-Dichlorobenzene
541-73-1
8260D
ND
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
0.50
0.40
ug/L
1
Dichlorodifluoromethane
75-71-8
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
8260D
ND
0.50
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
0.50
0.40
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
ND
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Isopropylbenzene
98-82-8
8260D
ND
0.50
0.40
ug/L
1
Methyl acetate
79-20-9
8260D
ND
1.0
0.40
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
0.50
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylcyclohexane
108-87-2
8260D
ND
5.0
0.40
ug/L
1
Methylene chloride
75-09-2
8260D
ND
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
0.50
0.41
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
0.50
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
8260D
ND
1.0
0.42
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
8260D
ND
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
0.50
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
53 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-003
Description: MW-10 Matrix: Aqueous
Date Sampled:08/14/2019 1540 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 08/17/2019 0213 ALR1 26199
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichloroethene
79-01-6
8260D
ND
0.50
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
0.50
0.40
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
101 70-130
103 70-130
110 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
54 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-003
Description: MW-10 Matrix: Aqueous
Date Sampled:08/14/2019 1540 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
8270E
1 08/22/2019 2111 SCD
08/19/2019 1653 26336
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.80
0.20
ug/L
1
Acenaphthylene
208-96-8
8270E
ND
0.80
0.20
ug/L
1
Acetophenone
98-86-2
8270E
ND
4.0
0.50
ug/L
1
Anthracene
120-12-7
8270E
ND
0.80
0.20
ug/L
1
Atrazine
1912-24-9
8270E
ND
4.0
0.50
ug/L
1
Benzaldehyde
100-52-7
8270E
ND
8.0
0.50
ug/L
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.80
0.20
ug/L
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.80
0.20
ug/L
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.80
0.20
ug/L
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.80
0.20
ug/L
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.80
0.20
ug/L
1
1,1'-Biphenyl
92-52-4
8270E
ND
4.0
0.50
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
4.0
0.50
ug/L
1
Butyl benzyl phthalate
85-68-7
8270E
ND
4.0
0.50
ug/L
1
Caprolactam
105-60-2
8270E
2.6 BJ
8.0
1.0
ug/L
1
Carbazole
86-74-8
8270E
ND
4.0
0.50
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
4.0
0.50
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
4.0
0.50
ug/L
1
4-Chloroaniline
106-47-8
8270E
ND
8.0
0.50
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
4.0
0.50
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
4.0
0.50
ug/L
1
2-Chloronaphthalene
91-58-7
8270E
ND
4.0
0.50
ug/L
1
2-Chlorophenol
95-57-8
8270E
ND
4.0
0.50
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
4.0
0.50
ug/L
1
Chrysene
218-01-9
8270E
ND
0.80
0.20
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.80
0.20
ug/L
1
Dibenzofuran
132-64-9
8270E
ND
4.0
0.50
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
4.0
1.8
ug/L
1
2,4-Dichlorophenol
120-83-2
8270E
ND
8.0
1.0
ug/L
1
Diethylphthalate
84-66-2
8270E
ND
4.0
0.50
ug/L
1
Dimethyl phthalate
131-11-3
8270E
ND
4.0
0.50
ug/L
1
2,4-Dimethylphenol
105-67-9
8270E
ND
4.0
1.0
ug/L
1
Di-n-butyl phthalate
84-74-2
8270E
ND
4.0
0.50
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
20
1.0
ug/L
1
2,4-Dinitrophenol
51-28-5
8270E
ND
20
1.0
ug/L
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
8.0
0.50
ug/L
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
8.0
0.50
ug/L
1
Di-n-octylphthalate
117-84-0
8270E
ND
4.0
0.50
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
1.1 J
4.0
0.50
ug/L
1
Fluoranthene
206-44-0
8270E
ND
0.80
0.20
ug/L
1
Fluorene
86-73-7
8270E
ND
0.80
0.20
ug/L
1
Hexachlorobenzene
118-74-1
8270E
ND
4.0
0.50
ug/L
1
Hexachlorobutadiene
87-68-3
8270E
ND
4.0
0.50
ug/L
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
20
2.0
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
55 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-003
Description: MW-10 Matrix: Aqueous
Date Sampled:08/14/2019 1540 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 08/22/2019 2111 SCD 08/19/2019 1653 26336
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexachloroethane
67-72-1
8270E
ND
4.0
1.0
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.80
0.20
ug/L
1
Isophorone
78-59-1
8270E
ND
4.0
0.50
ug/L
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.80
0.20
ug/L
1
2-Methylphenol
95-48-7
8270E
ND
4.0
1.0
ug/L
1
3+4-Methylphenol
106-44-5
8270E
ND
4.0
1.5
ug/L
1
Naphthalene
91-20-3
8270E
ND
0.80
0.20
ug/L
1
2-Nitroaniline
88-74-4
8270E
ND
8.0
0.50
ug/L
1
3-Nitroaniline
99-09-2
8270E
ND
8.0
1.0
ug/L
1
4-Nitroaniline
100-01-6
8270E
ND
8.0
1.5
ug/L
1
Nitrobenzene
98-95-3
8270E
ND
4.0
1.5
ug/L
1
2-Nitrophenol
88-75-5
8270E
ND
4.0
1.0
ug/L
1
4-Nitrophenol
100-02-7
8270E
ND
20
2.0
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
4.0
0.50
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
4.0
0.50
ug/L
1
Pentachlorophenol
87-86-5
8270E
ND
20
2.0
ug/L
1
Phenanthrene
85-01-8
8270E
ND
0.80
0.20
ug/L
1
Phenol
108-95-2
8270E
ND
4.0
0.50
ug/L
1
Pyrene
129-00-0
8270E
ND
0.80
0.20
ug/L
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
4.0
0.50
ug/L
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
4.0
0.50
ug/L
1
Run
1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
44
37-129
2-Fluorophenol
37
24-127
Nitrobenzene-d5
48
38-127
Phenol-d5
41
28-128
Terphenyl-d14
68
10-148
2,4,6-Tribromophenol
55
35-144
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
56 of 198

MADEP EPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-003
Description: MW-10 Matrix: Aqueous
Date Sampled:08/14/2019 1540 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 08/30/2019 0353 CHG 08/26/2019 2111 27084
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C11 - C22 Aromatics MADEP-EPH-04 ND 100 100 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl (aromatic)
2-Fluorobiphenyl (fractionation 1)
2-Bromonaphthalene (fractionation 2)
79 40-140
123 40-140
105 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
57 of 198

MADEP EPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-003
Description: MW-10 Matrix: Aqueous
Date Sampled:08/14/2019 1540 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 08/30/2019 0027 CHG 08/26/2019 2111 27085
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C18 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 1
C19 - C36 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
78 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
58 of 198

MADEP VPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-003
Description: MW-10 Matrix: Aqueous
Date Sampled:08/14/2019 1540 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 08/17/2019 2039 JJG 26245
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C5 - C8 Aliphatics MADEP-VPH- ND 75 15 ug/L 1
C9 - C12 Aliphatics MADEP-VPH- ND 75 15 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
122 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
59 of 198

MADEP VPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15078-003
Description: MW-10 Matrix: Aqueous
Date Sampled:08/14/2019 1540 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 08/17/2019 2039 JJG 26244
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C10 Aromatics MADEP-VPH- ND 25 5.0 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
125 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
60 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory I D: UH 15078-004
Description: Trip Blank Matrix: Aqueous
Date Sampled:08/14/2019 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 08/17/2019 0237 ALR1
26199
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
ND
10
4.0
ug/L
1
Benzene
71-43-2
8260D
ND
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
ND
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
ND
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
ND
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
ND
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
ND
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
ND
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
ND
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
0.50
0.40
ug/L
1
Cyclohexane
110-82-7
8260D
ND
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
ND
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
ND
0.50
0.40
ug/L
1
1,3-Dichlorobenzene
541-73-1
8260D
ND
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
0.50
0.40
ug/L
1
Dichlorodifluoromethane
75-71-8
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
8260D
ND
0.50
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
0.50
0.40
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
ND
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Isopropylbenzene
98-82-8
8260D
ND
0.50
0.40
ug/L
1
Methyl acetate
79-20-9
8260D
ND
1.0
0.40
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
0.50
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylcyclohexane
108-87-2
8260D
ND
5.0
0.40
ug/L
1
Methylene chloride
75-09-2
8260D
ND
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
0.50
0.41
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
0.50
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
8260D
ND
1.0
0.42
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
8260D
ND
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
0.50
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
61 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory I D: UH 15078-004
Description: Trip Blank Matrix: Aqueous
Date Sampled:08/14/2019 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 08/17/2019 0237 ALR1 26199
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichloroethene
79-01-6
8260D
ND
0.50
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
0.50
0.40
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
102 70-130
101 70-130
108 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
62 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15079-001
Description: TP-1 Matrix: Aqueous
Date Sampled:08/14/2019 1015 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 08/17/2019 0301 ALR1
26199
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
ND
10
4.0
ug/L
1
Benzene
71-43-2
8260D
ND
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
ND
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
ND
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
ND
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
ND
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
ND
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
ND
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
ND
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
0.50
0.40
ug/L
1
Cyclohexane
110-82-7
8260D
ND
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
ND
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
ND
0.50
0.40
ug/L
1
1,3-Dichlorobenzene
541-73-1
8260D
ND
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
0.50
0.40
ug/L
1
Dichlorodifluoromethane
75-71-8
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
8260D
ND
0.50
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
0.50
0.40
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
ND
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Isopropylbenzene
98-82-8
8260D
ND
0.50
0.40
ug/L
1
Methyl acetate
79-20-9
8260D
ND
1.0
0.40
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
0.50
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylcyclohexane
108-87-2
8260D
ND
5.0
0.40
ug/L
1
Methylene chloride
75-09-2
8260D
ND
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
0.50
0.41
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
0.50
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
8260D
ND
1.0
0.42
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
8260D
ND
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
0.50
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
63 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15079-001
Description: TP-1 Matrix: Aqueous
Date Sampled:08/14/2019 1015 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 08/17/2019 0301 ALR1 26199
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichloroethene
79-01-6
8260D
ND
0.50
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
0.50
0.40
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
100 70-130
101 70-130
107 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
64 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15079-001
Description: TP-1 Matrix: Aqueous
Date Sampled:08/14/2019 1015 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
8270E
1 08/22/2019 2136 SCD
08/19/2019 1653 26336
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.80
0.20
ug/L
1
Acenaphthylene
208-96-8
8270E
ND
0.80
0.20
ug/L
1
Acetophenone
98-86-2
8270E
ND
4.0
0.50
ug/L
1
Anthracene
120-12-7
8270E
ND
0.80
0.20
ug/L
1
Atrazine
1912-24-9
8270E
ND
4.0
0.50
ug/L
1
Benzaldehyde
100-52-7
8270E
ND
8.0
0.50
ug/L
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.80
0.20
ug/L
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.80
0.20
ug/L
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.80
0.20
ug/L
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.80
0.20
ug/L
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.80
0.20
ug/L
1
1,1'-Biphenyl
92-52-4
8270E
ND
4.0
0.50
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
4.0
0.50
ug/L
1
Butyl benzyl phthalate
85-68-7
8270E
ND
4.0
0.50
ug/L
1
Caprolactam
105-60-2
8270E
ND
8.0
1.0
ug/L
1
Carbazole
86-74-8
8270E
ND
4.0
0.50
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
4.0
0.50
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
4.0
0.50
ug/L
1
4-Chloroaniline
106-47-8
8270E
ND
8.0
0.50
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
4.0
0.50
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
4.0
0.50
ug/L
1
2-Chloronaphthalene
91-58-7
8270E
ND
4.0
0.50
ug/L
1
2-Chlorophenol
95-57-8
8270E
ND
4.0
0.50
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
4.0
0.50
ug/L
1
Chrysene
218-01-9
8270E
ND
0.80
0.20
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.80
0.20
ug/L
1
Dibenzofuran
132-64-9
8270E
ND
4.0
0.50
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
4.0
1.8
ug/L
1
2,4-Dichlorophenol
120-83-2
8270E
ND
8.0
1.0
ug/L
1
Diethylphthalate
84-66-2
8270E
ND
4.0
0.50
ug/L
1
Dimethyl phthalate
131-11-3
8270E
ND
4.0
0.50
ug/L
1
2,4-Dimethylphenol
105-67-9
8270E
ND
4.0
1.0
ug/L
1
Di-n-butyl phthalate
84-74-2
8270E
ND
4.0
0.50
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
20
1.0
ug/L
1
2,4-Dinitrophenol
51-28-5
8270E
ND
20
1.0
ug/L
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
8.0
0.50
ug/L
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
8.0
0.50
ug/L
1
Di-n-octylphthalate
117-84-0
8270E
ND
4.0
0.50
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
4.0
0.50
ug/L
1
Fluoranthene
206-44-0
8270E
ND
0.80
0.20
ug/L
1
Fluorene
86-73-7
8270E
ND
0.80
0.20
ug/L
1
Hexachlorobenzene
118-74-1
8270E
ND
4.0
0.50
ug/L
1
Hexachlorobutadiene
87-68-3
8270E
ND
4.0
0.50
ug/L
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
20
2.0
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
65 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory ID:UH15079-001
Description: TP-1 Matrix: Aqueous
Date Sampled:08/14/2019 1015 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 08/22/2019 2136 SCD 08/19/2019 1653 26336
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexachloroethane
67-72-1
8270E
ND
4.0
1.0
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.80
0.20
ug/L
1
Isophorone
78-59-1
8270E
ND
4.0
0.50
ug/L
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.80
0.20
ug/L
1
2-Methylphenol
95-48-7
8270E
ND
4.0
1.0
ug/L
1
3+4-Methylphenol
106-44-5
8270E
ND
4.0
1.5
ug/L
1
Naphthalene
91-20-3
8270E
ND
0.80
0.20
ug/L
1
2-Nitroaniline
88-74-4
8270E
ND
8.0
0.50
ug/L
1
3-Nitroaniline
99-09-2
8270E
ND
8.0
1.0
ug/L
1
4-Nitroaniline
100-01-6
8270E
ND
8.0
1.5
ug/L
1
Nitrobenzene
98-95-3
8270E
ND
4.0
1.5
ug/L
1
2-Nitrophenol
88-75-5
8270E
ND
4.0
1.0
ug/L
1
4-Nitrophenol
100-02-7
8270E
ND
20
2.0
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
4.0
0.50
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
4.0
0.50
ug/L
1
Pentachlorophenol
87-86-5
8270E
ND
20
2.0
ug/L
1
Phenanthrene
85-01-8
8270E
ND
0.80
0.20
ug/L
1
Phenol
108-95-2
8270E
ND
4.0
0.50
ug/L
1
Pyrene
129-00-0
8270E
ND
0.80
0.20
ug/L
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
4.0
0.50
ug/L
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
4.0
0.50
ug/L
1
Run
1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
49
37-129
2-Fluorophenol
35
24-127
Nitrobenzene-d5
56
38-127
Phenol-d5
43
28-128
Terphenyl-d14
69
10-148
2,4,6-Tribromophenol
60
35-144
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
66 of 198

MADEP EPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15079-001
Description: TP-1 Matrix: Aqueous
Date Sampled:08/14/2019 1015 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run
Prep Method
Analytical Method Dilution
Analysis Date Analyst
Prep Date Batch
1
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 0423 CHG
08/26/2019 2111 27084
2
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 1803 CHG
08/29/2019 0911 27388
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C11 - C22 Aromatics MADEP-EPH-04 ND 100 100 ug/L 1
Run 1 Acceptance Run 2 Acceptance
Surrogate Q % Recovery Limits Q % Recovery Limits
o - Terphenyl (aromatic)
2-Fluorobiphenyl (fractionation 1)
2-Bromonaphthalene (fractionation 2)
89 40-140 H 87 40-140
126 40-140 H 103 40-140
120 40-140 H 92 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
67 of 198

MADEP EPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15079-001
Description: TP-1 Matrix: Aqueous
Date Sampled:08/14/2019 1015 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run
Prep Method
Analytical Method Dilution
Analysis Date Analyst
Prep Date Batch
1
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 0423 CHG
08/26/2019 2111 27084
2
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 1803 CHG
08/29/2019 0911 27388
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C11 - C22 Aromatics MADEP-EPH-04 ND H 100 100 ug/L 2
Run 1 Acceptance Run 2 Acceptance
Surrogate Q % Recovery Limits Q % Recovery Limits
o - Terphenyl (aromatic)
2-Fluorobiphenyl (fractionation 1)
2-Bromonaphthalene (fractionation 2)
89 40-140 H 87 40-140
126 40-140 H 103 40-140
120 40-140 H 92 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
68 of 198

MADEP EPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15079-001
Description: TP-1 Matrix: Aqueous
Date Sampled:08/14/2019 1015 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run
Prep Method
Analytical Method Dilution
Analysis Date Analyst
Prep Date Batch
1
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 0056 CHG
08/26/2019 2111 27085
2
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 1137 CHG
08/29/2019 0911 27385
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C18 Aliphatics MADEP-EPH- 100 B 100 100 ug/L 1
C19 - C36 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 1
Run 1 Acceptance Run 2 Acceptance
Surrogate Q % Recovery Limits Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
88 40-140 H 76 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
69 of 198

MADEP EPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15079-001
Description: TP-1 Matrix: Aqueous
Date Sampled:08/14/2019 1015 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run
Prep Method
Analytical Method Dilution
Analysis Date Analyst
Prep Date Batch
1
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 0056 CHG
08/26/2019 2111 27085
2
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 1137 CHG
08/29/2019 0911 27385
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C18 Aliphatics MADEP-EPH-04 ND H 100 100 ug/L 2
C19 - C36 Aliphatics MADEP-EPH-04 ND H 100 100 ug/L 2
Run 1 Acceptance Run 2 Acceptance
Surrogate Q % Recovery Limits Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
88 40-140 H 76 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
70 of 198

MADEP VPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15079-001
Description: TP-1 Matrix: Aqueous
Date Sampled:08/14/2019 1015 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 08/17/2019 2108 JJG 26245
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C5 - C8 Aliphatics MADEP-VPH- ND 75 15 ug/L 1
C9 - C12 Aliphatics MADEP-VPH- ND 75 15 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
97 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
71 of 198

MADEP VPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory ID:UH15079-001
Description: TP-1 Matrix: Aqueous
Date Sampled:08/14/2019 1015 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 08/17/2019 2108 JJG 26244
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C10 Aromatics MADEP-VPH- ND 25 5.0 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
99 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
72 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-002
Description: TP-2 Matrix: Aqueous
Date Sampled:08/14/2019 1025 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 08/17/2019 0325 ALR1
26199
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
ND
10
4.0
ug/L
1
Benzene
71-43-2
8260D
ND
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
ND
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
ND
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
ND
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
ND
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
ND
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
ND
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
ND
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
0.50
0.40
ug/L
1
Cyclohexane
110-82-7
8260D
ND
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
ND
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
ND
0.50
0.40
ug/L
1
1,3-Dichlorobenzene
541-73-1
8260D
ND
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
0.50
0.40
ug/L
1
Dichlorodifluoromethane
75-71-8
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
8260D
ND
0.50
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
0.50
0.40
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
ND
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Isopropylbenzene
98-82-8
8260D
ND
0.50
0.40
ug/L
1
Methyl acetate
79-20-9
8260D
ND
1.0
0.40
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
0.50
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylcyclohexane
108-87-2
8260D
ND
5.0
0.40
ug/L
1
Methylene chloride
75-09-2
8260D
ND
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
0.50
0.41
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
0.50
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
8260D
ND
1.0
0.42
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
8260D
ND
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
0.50
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
73 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-002
Description: TP-2 Matrix: Aqueous
Date Sampled:08/14/2019 1025 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 08/17/2019 0325 ALR1 26199
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichloroethene
79-01-6
8260D
ND
0.50
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
0.50
0.40
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
102 70-130
102 70-130
110 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
74 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-002
Description: TP-2 Matrix: Aqueous
Date Sampled:08/14/2019 1025 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
8270E
1 08/24/2019
1631 SCD
08/19/2019 1653 26336
2 3520C
8270E
1 08/31/2019 1350 SCD
08/29/2019 1724 27488
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.80
0.20
ug/L
1
Acenaphthylene
208-96-8
8270E
ND
0.80
0.20
ug/L
1
Acetophenone
98-86-2
8270E
ND
4.0
0.50
ug/L
1
Anthracene
120-12-7
8270E
ND
0.80
0.20
ug/L
1
Atrazine
1912-24-9
8270E
ND
4.0
0.50
ug/L
1
Benzaldehyde
100-52-7
8270E
ND
8.0
0.50
ug/L
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.80
0.20
ug/L
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.80
0.20
ug/L
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.80
0.20
ug/L
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.80
0.20
ug/L
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.80
0.20
ug/L
1
1,1'-Biphenyl
92-52-4
8270E
ND
4.0
0.50
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
4.0
0.50
ug/L
1
Butyl benzyl phthalate
85-68-7
8270E
ND
4.0
0.50
ug/L
1
Caprolactam
105-60-2
8270E
3.4 BJ
8.0
1.0
ug/L
1
Carbazole
86-74-8
8270E
ND
4.0
0.50
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
4.0
0.50
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
4.0
0.50
ug/L
1
4-Chloroaniline
106-47-8
8270E
ND
8.0
0.50
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
4.0
0.50
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
4.0
0.50
ug/L
1
2-Chloronaphthalene
91-58-7
8270E
ND
4.0
0.50
ug/L
1
2-Chlorophenol
95-57-8
8270E
ND
4.0
0.50
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
4.0
0.50
ug/L
1
Chrysene
218-01-9
8270E
ND
0.80
0.20
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.80
0.20
ug/L
1
Dibenzofuran
132-64-9
8270E
ND
4.0
0.50
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
4.0
1.8
ug/L
1
2,4-Dichlorophenol
120-83-2
8270E
ND
8.0
1.0
ug/L
1
Diethylphthalate
84-66-2
8270E
ND
4.0
0.50
ug/L
1
Dimethyl phthalate
131-11-3
8270E
ND
4.0
0.50
ug/L
1
2,4-Dimethylphenol
105-67-9
8270E
ND
4.0
1.0
ug/L
1
Di-n-butyl phthalate
84-74-2
8270E
ND
4.0
0.50
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
20
1.0
ug/L
1
2,4-Dinitrophenol
51-28-5
8270E
ND
20
1.0
ug/L
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
8.0
0.50
ug/L
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
8.0
0.50
ug/L
1
Di-n-octylphthalate
117-84-0
8270E
ND
4.0
0.50
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
4.0
0.50
ug/L
1
Fluoranthene
206-44-0
8270E
ND
0.80
0.20
ug/L
1
Fluorene
86-73-7
8270E
ND
0.80
0.20
ug/L
1
Hexachlorobenzene
118-74-1
8270E
ND
4.0
0.50
ug/L
1
Hexachlorobutadiene
87-68-3
8270E
ND
4.0
0.50
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
75 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-002
Description: TP-2 Matrix: Aqueous
Date Sampled:08/14/2019 1025 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run
Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date Batch
1
3520C
8270E
1 08/24/2019 1631 SCD
08/19/2019 1653 26336
2
3520C
8270E
1 08/31/2019 1350 SCD
08/29/2019 1724 27488
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexachlorocyclopentadiene
77-47-4
8270E
ND
20
2.0
ug/L
1
Hexachloroethane
67-72-1
8270E
ND
4.0
1.0
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.80
0.20
ug/L
1
Isophorone
78-59-1
8270E
ND
4.0
0.50
ug/L
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.80
0.20
ug/L
1
2-Methylphenol
95-48-7
8270E
ND
4.0
1.0
ug/L
1
3+4-Methylphenol
106-44-5
8270E
ND
4.0
1.5
ug/L
1
Naphthalene
91-20-3
8270E
ND
0.80
0.20
ug/L
1
2-Nitroaniline
88-74-4
8270E
ND
8.0
0.50
ug/L
1
3-Nitroaniline
99-09-2
8270E
ND
8.0
1.0
ug/L
1
4-Nitroaniline
100-01-6
8270E
ND
8.0
1.5
ug/L
1
Nitrobenzene
98-95-3
8270E
ND
4.0
1.5
ug/L
1
2-Nitrophenol
88-75-5
8270E
ND
4.0
1.0
ug/L
1
4-Nitrophenol
100-02-7
8270E
ND
20
2.0
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
4.0
0.50
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
4.0
0.50
ug/L
1
Pentachlorophenol
87-86-5
8270E
ND
20
2.0
ug/L
1
Phenanthrene
85-01-8
8270E
ND
0.80
0.20
ug/L
1
Phenol
108-95-2
8270E
ND
4.0
0.50
ug/L
1
Pyrene
129-00-0
8270E
ND
0.80
0.20
ug/L
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
4.0
0.50
ug/L
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
4.0
0.50
ug/L
1
Run
1 Acceptance
Run 2
Acceptance
Surrogate
Q % Recovery Limits
Q % Recovery
Limits
2-Fluorobiphenyl
42
37-129
H
77
37-129
2-Fluorophenol
N 21
24-127
H
48
24-127
Nitrobenzene-d5
45
38-127
H
64
38-127
Phenol-d5
32
28-128
H
61
28-128
Terphenyl-d14
80
10-148
H
98
10-148
2,4,6-Tribromophenol
69
35-144
H
65
35-144
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
76 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-002
Description: TP-2 Matrix: Aqueous
Date Sampled:08/14/2019 1025 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
8270E
1 08/24/2019
1631 SCD
08/19/2019
1653 26336
2 3520C
8270E
1 08/31/2019 1350 SCD
08/29/2019
1724 27488
CAS
Analytical
Parameter
Number
Method
Result
Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9
8270E
ND
H
0.80
0.20
ug/L
2
Acenaphthylene
208-96-8
8270E
ND
H
0.80
0.20
ug/L
2
Acetophenone
98-86-2
8270E
ND
H
4.0
0.50
ug/L
2
Anthracene
120-12-7
8270E
ND
H
0.80
0.20
ug/L
2
Atrazine
1912-24-9
8270E
ND
H
4.0
0.50
ug/L
2
Benzaldehyde
100-52-7
8270E
ND
H
8.0
0.50
ug/L
2
Benzo(a)anthracene
56-55-3
8270E
ND
H
0.80
0.20
ug/L
2
Benzo(a)pyrene
50-32-8
8270E
ND
H
0.80
0.20
ug/L
2
Benzo(b)fluoranthene
205-99-2
8270E
ND
H
0.80
0.20
ug/L
2
Benzo(g,h,i)perylene
191-24-2
8270E
ND
H
0.80
0.20
ug/L
2
Benzo(k)fluoranthene
207-08-9
8270E
ND
H
0.80
0.20
ug/L
2
1,1'-Biphenyl
92-52-4
8270E
ND
H
4.0
0.50
ug/L
2
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
H
4.0
0.50
ug/L
2
Butyl benzyl phthalate
85-68-7
8270E
ND
H
4.0
0.50
ug/L
2
Caprolactam
105-60-2
8270E
ND
H
8.0
1.0
ug/L
2
Carbazole
86-74-8
8270E
ND
H
4.0
0.50
ug/L
2
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
H
4.0
0.50
ug/L
2
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
H
4.0
0.50
ug/L
2
4-Chloroaniline
106-47-8
8270E
ND
H
8.0
0.50
ug/L
2
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
H
4.0
0.50
ug/L
2
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
H
4.0
0.50
ug/L
2
2-Chloronaphthalene
91-58-7
8270E
ND
H
4.0
0.50
ug/L
2
2-Chlorophenol
95-57-8
8270E
ND
H
4.0
0.50
ug/L
2
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
H
4.0
0.50
ug/L
2
Chrysene
218-01-9
8270E
ND
H
0.80
0.20
ug/L
2
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
H
0.80
0.20
ug/L
2
Dibenzofuran
132-64-9
8270E
ND
H
4.0
0.50
ug/L
2
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
H
4.0
1.8
ug/L
2
2,4-Dichlorophenol
120-83-2
8270E
ND
H
8.0
1.0
ug/L
2
Diethylphthalate
84-66-2
8270E
ND
H
4.0
0.50
ug/L
2
Dimethyl phthalate
131-11-3
8270E
ND
H
4.0
0.50
ug/L
2
2,4-Dimethylphenol
105-67-9
8270E
ND
H
4.0
1.0
ug/L
2
Di-n-butyl phthalate
84-74-2
8270E
ND
H
4.0
0.50
ug/L
2
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
H
20
1.0
ug/L
2
2,4-Dinitrophenol
51-28-5
8270E
ND
H
20
1.0
ug/L
2
2,4-Dinitrotoluene
121-14-2
8270E
ND
H
8.0
0.50
ug/L
2
2,6-Dinitrotoluene
606-20-2
8270E
ND
H
8.0
0.50
ug/L
2
Di-n-octylphthalate
117-84-0
8270E
ND
H
4.0
0.50
ug/L
2
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
H
4.0
0.50
ug/L
2
Fluoranthene
206-44-0
8270E
ND
H
0.80
0.20
ug/L
2
Fluorene
86-73-7
8270E
ND
H
0.80
0.20
ug/L
2
Hexachlorobenzene
118-74-1
8270E
ND
H
4.0
0.50
ug/L
2
Hexachlorobutadiene
87-68-3
8270E
ND
H
4.0
0.50
ug/L
2
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
77 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-002
Description: TP-2 Matrix: Aqueous
Date Sampled:08/14/2019 1025 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 08/24/2019 1631 SCD 08/19/2019 1653 26336
2 3520C 8270E 1 08/31/2019 1350 SCD 08/29/2019 1724 27488
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexachlorocyclopentadiene
77-47-4
8270E
ND
H
20
2.0
ug/L
Hexachloroethane
67-72-1
8270E
ND
H
4.0
1.0
ug/L
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
H
0.80
0.20
ug/L
Isophorone
78-59-1
8270E
ND
H
4.0
0.50
ug/L
2-Methylnaphthalene
91-57-6
8270E
ND
H
0.80
0.20
ug/L
2-Methylphenol
95-48-7
8270E
ND
H
4.0
1.0
ug/L
3+4-Methylphenol
106-44-5
8270E
ND
H
4.0
1.5
ug/L
Naphthalene
91-20-3
8270E
ND
H
0.80
0.20
ug/L
2-Nitroaniline
88-74-4
8270E
ND
H
8.0
0.50
ug/L
3-Nitroaniline
99-09-2
8270E
ND
H
8.0
1.0
ug/L
4-Nitroaniline
100-01-6
8270E
ND
H
8.0
1.5
ug/L
Nitrobenzene
98-95-3
8270E
ND
H
4.0
1.5
ug/L
2-Nitrophenol
88-75-5
8270E
ND
H
4.0
1.0
ug/L
4-Nitrophenol
100-02-7
8270E
ND
H
20
2.0
ug/L
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
H
4.0
0.50
ug/L
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
H
4.0
0.50
ug/L
Pentachlorophenol
87-86-5
8270E
ND
H
20
2.0
ug/L
Phenanthrene
85-01-8
8270E
ND
H
0.80
0.20
ug/L
Phenol
108-95-2
8270E
ND
H
4.0
0.50
ug/L
Pyrene
129-00-0
8270E
ND
H
0.80
0.20
ug/L
2,4,5-Trichlorophenol
95-95-4
8270E
ND
H
4.0
0.50
ug/L
2,4,6-Trichlorophenol
88-06-2
8270E
ND
H
4.0
0.50
ug/L
Run 1
Acceptance
Run 2
Acceptance
Surrogate
Q % Recovery
Limits
Q
% Recovery
Limits
2-Fluorobiphenyl
42
37-129
H
77
37-129
2-Fluorophenol
N 21
24-127
H
48
24-127
Nitrobenzene-d5
45
38-127
H
64
38-127
Phenol-d5
32
28-128
H
61
28-128
Terphenyl-d14
80
10-148
H
98
10-148
2,4,6-Tribromophenol
69
35-144
H
65
35-144
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
78 of 198

MADEP EPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-002
Description: TP-2 Matrix: Aqueous
Date Sampled:08/14/2019 1025 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run
Prep Method
Analytical Method Dilution
Analysis Date Analyst
Prep Date Batch
1
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 0452 CHG
08/26/2019 2111 27084
2
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 1833 CHG
08/29/2019 0911 27388
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C11 - C22 Aromatics MADEP-EPH-04 ND 100 100 ug/L 1
Run 1 Acceptance Run 2 Acceptance
Surrogate Q % Recovery Limits Q % Recovery Limits
o - Terphenyl (aromatic)
2-Fluorobiphenyl (fractionation 1)
2-Bromonaphthalene (fractionation 2)
79 40-140 H 96 40-140
125 40-140 H 112 40-140
117 40-140 H 100 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
79 of 198

MADEP EPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-002
Description: TP-2 Matrix: Aqueous
Date Sampled:08/14/2019 1025 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run
Prep Method
Analytical Method Dilution
Analysis Date Analyst
Prep Date Batch
1
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 0452 CHG
08/26/2019 2111 27084
2
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 1833 CHG
08/29/2019 0911 27388
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C11 - C22 Aromatics MADEP-EPH-04 ND H 100 100 ug/L 2
Run 1 Acceptance Run 2 Acceptance
Surrogate Q % Recovery Limits Q % Recovery Limits
o - Terphenyl (aromatic)
2-Fluorobiphenyl (fractionation 1)
2-Bromonaphthalene (fractionation 2)
79 40-140 H 96 40-140
125 40-140 H 112 40-140
117 40-140 H 100 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
80 of 198

MADEP EPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-002
Description: TP-2 Matrix: Aqueous
Date Sampled:08/14/2019 1025 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run
Prep Method
Analytical Method Dilution
Analysis Date Analyst
Prep Date Batch
1
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 0126 CHG
08/26/2019 2111 27085
2
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 1207 CHG
08/29/2019 0911 27385
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C18 Aliphatics MADEP-EPH- 100 B 100 100 ug/L 1
C19 - C36 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 1
Run 1 Acceptance Run 2 Acceptance
Surrogate Q % Recovery Limits Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
82 40-140 H 77 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
81 of 198

MADEP EPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-002
Description: TP-2 Matrix: Aqueous
Date Sampled:08/14/2019 1025 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run
Prep Method
Analytical Method Dilution
Analysis Date Analyst
Prep Date Batch
1
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 0126 CHG
08/26/2019 2111 27085
2
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 1207 CHG
08/29/2019 0911 27385
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C18 Aliphatics MADEP-EPH-04 ND H 100 100 ug/L 2
C19 - C36 Aliphatics MADEP-EPH-04 ND H 100 100 ug/L 2
Run 1 Acceptance Run 2 Acceptance
Surrogate Q % Recovery Limits Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
82 40-140 H 77 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
82 of 198

MADEP VPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-002
Description: TP-2 Matrix: Aqueous
Date Sampled:08/14/2019 1025 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 08/17/2019 2137 JJG 26245
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C5 - C8 Aliphatics MADEP-VPH- ND 75 15 ug/L 1
C9 - C12 Aliphatics MADEP-VPH- ND 75 15 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
98 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
83 of 198

MADEP VPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-002
Description: TP-2 Matrix: Aqueous
Date Sampled:08/14/2019 1025 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 08/17/2019 2137 JJG 26244
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C10 Aromatics MADEP-VPH- ND 25 5.0 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
98 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
84 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-003
Description: MW-7 Matrix: Aqueous
Date Sampled:08/14/2019 1135 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 08/17/2019 0348 ALR1
26199
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
ND
10
4.0
ug/L
1
Benzene
71-43-2
8260D
ND
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
ND
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
ND
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
ND
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
ND
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
ND
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
ND
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
ND
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
0.50
0.40
ug/L
1
Cyclohexane
110-82-7
8260D
ND
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
ND
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
ND
0.50
0.40
ug/L
1
1,3-Dichlorobenzene
541-73-1
8260D
ND
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
0.50
0.40
ug/L
1
Dichlorodifluoromethane
75-71-8
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
8260D
ND
0.50
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
0.50
0.40
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
ND
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Isopropylbenzene
98-82-8
8260D
ND
0.50
0.40
ug/L
1
Methyl acetate
79-20-9
8260D
ND
1.0
0.40
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
ND
0.50
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylcyclohexane
108-87-2
8260D
ND
5.0
0.40
ug/L
1
Methylene chloride
75-09-2
8260D
ND
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
0.50
0.41
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
0.50
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
8260D
ND
1.0
0.42
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
8260D
ND
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
0.50
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
85 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-003
Description: MW-7 Matrix: Aqueous
Date Sampled:08/14/2019 1135 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 08/17/2019 0348 ALR1 26199
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichloroethene
79-01-6
8260D
ND
0.50
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
0.50
0.40
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
100 70-130
102 70-130
107 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
86 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-003
Description: MW-7 Matrix: Aqueous
Date Sampled:08/14/2019 1135 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
8270E
1 08/22/2019 2225 SCD
08/19/2019 1653 26336
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.80
0.20
ug/L
1
Acenaphthylene
208-96-8
8270E
ND
0.80
0.20
ug/L
1
Acetophenone
98-86-2
8270E
ND
4.0
0.50
ug/L
1
Anthracene
120-12-7
8270E
ND
0.80
0.20
ug/L
1
Atrazine
1912-24-9
8270E
ND
4.0
0.50
ug/L
1
Benzaldehyde
100-52-7
8270E
ND
8.0
0.50
ug/L
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.80
0.20
ug/L
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.80
0.20
ug/L
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.80
0.20
ug/L
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.80
0.20
ug/L
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.80
0.20
ug/L
1
1,1'-Biphenyl
92-52-4
8270E
ND
4.0
0.50
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
4.0
0.50
ug/L
1
Butyl benzyl phthalate
85-68-7
8270E
ND
4.0
0.50
ug/L
1
Caprolactam
105-60-2
8270E
ND
8.0
1.0
ug/L
1
Carbazole
86-74-8
8270E
ND
4.0
0.50
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
4.0
0.50
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
4.0
0.50
ug/L
1
4-Chloroaniline
106-47-8
8270E
ND
8.0
0.50
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
4.0
0.50
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
4.0
0.50
ug/L
1
2-Chloronaphthalene
91-58-7
8270E
ND
4.0
0.50
ug/L
1
2-Chlorophenol
95-57-8
8270E
ND
4.0
0.50
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
4.0
0.50
ug/L
1
Chrysene
218-01-9
8270E
ND
0.80
0.20
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.80
0.20
ug/L
1
Dibenzofuran
132-64-9
8270E
ND
4.0
0.50
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
4.0
1.8
ug/L
1
2,4-Dichlorophenol
120-83-2
8270E
ND
8.0
1.0
ug/L
1
Diethylphthalate
84-66-2
8270E
ND
4.0
0.50
ug/L
1
Dimethyl phthalate
131-11-3
8270E
ND
4.0
0.50
ug/L
1
2,4-Dimethylphenol
105-67-9
8270E
ND
4.0
1.0
ug/L
1
Di-n-butyl phthalate
84-74-2
8270E
ND
4.0
0.50
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
20
1.0
ug/L
1
2,4-Dinitrophenol
51-28-5
8270E
ND
20
1.0
ug/L
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
8.0
0.50
ug/L
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
8.0
0.50
ug/L
1
Di-n-octylphthalate
117-84-0
8270E
ND
4.0
0.50
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
4.0
0.50
ug/L
1
Fluoranthene
206-44-0
8270E
ND
0.80
0.20
ug/L
1
Fluorene
86-73-7
8270E
ND
0.80
0.20
ug/L
1
Hexachlorobenzene
118-74-1
8270E
ND
4.0
0.50
ug/L
1
Hexachlorobutadiene
87-68-3
8270E
ND
4.0
0.50
ug/L
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
20
2.0
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
87 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-003
Description: MW-7 Matrix: Aqueous
Date Sampled:08/14/2019 1135 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 08/22/2019 2225 SCD 08/19/2019 1653 26336
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexachloroethane
67-72-1
8270E
ND
4.0
1.0
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.80
0.20
ug/L
1
Isophorone
78-59-1
8270E
ND
4.0
0.50
ug/L
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.80
0.20
ug/L
1
2-Methylphenol
95-48-7
8270E
ND
4.0
1.0
ug/L
1
3+4-Methylphenol
106-44-5
8270E
ND
4.0
1.5
ug/L
1
Naphthalene
91-20-3
8270E
ND
0.80
0.20
ug/L
1
2-Nitroaniline
88-74-4
8270E
ND
8.0
0.50
ug/L
1
3-Nitroaniline
99-09-2
8270E
ND
8.0
1.0
ug/L
1
4-Nitroaniline
100-01-6
8270E
ND
8.0
1.5
ug/L
1
Nitrobenzene
98-95-3
8270E
ND
4.0
1.5
ug/L
1
2-Nitrophenol
88-75-5
8270E
ND
4.0
1.0
ug/L
1
4-Nitrophenol
100-02-7
8270E
ND
20
2.0
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
4.0
0.50
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
4.0
0.50
ug/L
1
Pentachlorophenol
87-86-5
8270E
ND
20
2.0
ug/L
1
Phenanthrene
85-01-8
8270E
ND
0.80
0.20
ug/L
1
Phenol
108-95-2
8270E
ND
4.0
0.50
ug/L
1
Pyrene
129-00-0
8270E
ND
0.80
0.20
ug/L
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
4.0
0.50
ug/L
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
4.0
0.50
ug/L
1
Run
1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
48
37-129
2-Fluorophenol
32
24-127
Nitrobenzene-d5
57
38-127
Phenol-d5
42
28-128
Terphenyl-d14
78
10-148
2,4,6-Tribromophenol
60
35-144
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
88 of 198

MADEP EPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-003
Description: MW-7 Matrix: Aqueous
Date Sampled:08/14/2019 1135 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 08/30/2019 0522 CHG 08/26/2019 2111 27084
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C11 - C22 Aromatics MADEP-EPH-04 ND 100 100 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
o - Terphenyl (aromatic)
2-Fluorobiphenyl (fractionation 1)
2-Bromonaphthalene (fractionation 2)
78 40-140
122 40-140
95 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
89 of 198

MADEP EPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-003
Description: MW-7 Matrix: Aqueous
Date Sampled:08/14/2019 1135 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 MADEP-EPH- MADEP-EPH-04 1 08/30/2019 0155 CHG 08/26/2019 2111 27085
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C18 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 1
C19 - C36 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
80 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
90 of 198

MADEP VPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-003
Description: MW-7 Matrix: Aqueous
Date Sampled:08/14/2019 1135 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 08/17/2019 2205 JJG 26245
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C5 - C8 Aliphatics MADEP-VPH- ND 75 15 ug/L 1
C9 - C12 Aliphatics MADEP-VPH- ND 75 15 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
101 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
91 of 198

MADEP VPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-003
Description: MW-7 Matrix: Aqueous
Date Sampled:08/14/2019 1135 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 08/17/2019 2205 JJG 26244
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C10 Aromatics MADEP-VPH- ND 25 5.0 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
103 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
92 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-004
Description: MW-8 Matrix: Aqueous
Date Sampled:08/14/2019 1145 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 5030B 8260D
1 08/17/2019 0412 ALR1
26199
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acetone
67-64-1
8260D
4.7 J
10
4.0
ug/L
1
Benzene
71-43-2
8260D
ND
0.50
0.40
ug/L
1
Bromodichloromethane
75-27-4
8260D
ND
0.50
0.40
ug/L
1
Bromoform
75-25-2
8260D
ND
0.50
0.40
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260D
ND
0.50
0.40
ug/L
1
2-Butanone (MEK)
78-93-3
8260D
ND
10
2.0
ug/L
1
Carbon disulfide
75-15-0
8260D
ND
0.50
0.40
ug/L
1
Carbon tetrachloride
56-23-5
8260D
ND
0.50
0.40
ug/L
1
Chlorobenzene
108-90-7
8260D
ND
0.50
0.40
ug/L
1
Chloroethane
75-00-3
8260D
ND
0.50
0.40
ug/L
1
Chloroform
67-66-3
8260D
ND
0.50
0.40
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260D
ND
0.50
0.40
ug/L
1
Cyclohexane
110-82-7
8260D
ND
0.50
0.40
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260D
ND
0.50
0.40
ug/L
1
Dibromochloromethane
124-48-1
8260D
ND
0.50
0.40
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichlorobenzene
95-50-1
8260D
ND
0.50
0.40
ug/L
1
1,3-Dichlorobenzene
541-73-1
8260D
ND
0.50
0.40
ug/L
1
1,4-Dichlorobenzene
106-46-7
8260D
ND
0.50
0.40
ug/L
1
Dichlorodifluoromethane
75-71-8
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethane
75-34-3
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloroethane
107-06-2
8260D
ND
0.50
0.40
ug/L
1
1,1-Dichloroethene
75-35-4
8260D
ND
0.50
0.40
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260D
ND
0.50
0.40
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260D
ND
0.50
0.40
ug/L
1
1,2-Dichloropropane
78-87-5
8260D
ND
0.50
0.40
ug/L
1
cis- 1,3-Dichloropropene
10061-01-5
8260D
ND
0.50
0.40
ug/L
1
trans- 1,3-Dichloropropene
10061-02-6
8260D
ND
0.50
0.40
ug/L
1
Ethylbenzene
100-41-4
8260D
ND
0.50
0.40
ug/L
1
2-Hexanone
591-78-6
8260D
ND
10
2.0
ug/L
1
Isopropylbenzene
98-82-8
8260D
ND
0.50
0.40
ug/L
1
Methyl acetate
79-20-9
8260D
ND
1.0
0.40
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260D
1.4
0.50
0.40
ug/L
1
4-Methyl-2-pentanone
108-10-1
8260D
ND
10
2.0
ug/L
1
Methylcyclohexane
108-87-2
8260D
ND
5.0
0.40
ug/L
1
Methylene chloride
75-09-2
8260D
ND
0.50
0.40
ug/L
1
Styrene
100-42-5
8260D
ND
0.50
0.41
ug/L
1
1,1,2,2-Tetrachloroethane
79-34-5
8260D
ND
0.50
0.40
ug/L
1
Tetrachloroethene
127-18-4
8260D
ND
0.50
0.40
ug/L
1
Toluene
108-88-3
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
8260D
ND
1.0
0.42
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
8260D
ND
0.50
0.40
ug/L
1
1,1,1-Trichloroethane
71-55-6
8260D
ND
0.50
0.40
ug/L
1
1,1,2-Trichloroethane
79-00-5
8260D
ND
0.50
0.40
ug/L
1
LOQ = Limit of Quantitation B = Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
93 of 198

Volatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-004
Description: MW-8 Matrix: Aqueous
Date Sampled:08/14/2019 1145 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260D 1 08/17/2019 0412 ALR1 26199
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Trichloroethene
79-01-6
8260D
ND
0.50
0.40
ug/L
1
Trichlorofluoromethane
75-69-4
8260D
ND
0.50
0.40
ug/L
1
Vinyl chloride
75-01-4
8260D
ND
0.50
0.40
ug/L
1
Xylenes (total)
1330-20-7
8260D
ND
1.0
0.40
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
Bromofluorobenzene
1,2-Dichloroethane-d4
Toluene-d8
103 70-130
103 70-130
110 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
94 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-004
Description: MW-8 Matrix: Aqueous
Date Sampled:08/14/2019 1145 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3520C
8270E
1 08/22/2019 2249 SCD
08/19/2019 1653 26336
CAS
Analytical
Parameter
Number
Method
Result Q
LOQ
DL
Units
Run
Acenaphthene
83-32-9
8270E
ND
0.80
0.20
ug/L
1
Acenaphthylene
208-96-8
8270E
ND
0.80
0.20
ug/L
1
Acetophenone
98-86-2
8270E
ND
4.0
0.50
ug/L
1
Anthracene
120-12-7
8270E
ND
0.80
0.20
ug/L
1
Atrazine
1912-24-9
8270E
ND
4.0
0.50
ug/L
1
Benzaldehyde
100-52-7
8270E
ND
8.0
0.50
ug/L
1
Benzo(a)anthracene
56-55-3
8270E
ND
0.80
0.20
ug/L
1
Benzo(a)pyrene
50-32-8
8270E
ND
0.80
0.20
ug/L
1
Benzo(b)fluoranthene
205-99-2
8270E
ND
0.80
0.20
ug/L
1
Benzo(g,h,i)perylene
191-24-2
8270E
ND
0.80
0.20
ug/L
1
Benzo(k)fluoranthene
207-08-9
8270E
ND
0.80
0.20
ug/L
1
1,1'-Biphenyl
92-52-4
8270E
ND
4.0
0.50
ug/L
1
4-Bromophenyl phenyl ether
101-55-3
8270E
ND
4.0
0.50
ug/L
1
Butyl benzyl phthalate
85-68-7
8270E
ND
4.0
0.50
ug/L
1
Caprolactam
105-60-2
8270E
3.3 BJ
8.0
1.0
ug/L
1
Carbazole
86-74-8
8270E
ND
4.0
0.50
ug/L
1
bis (2-Chloro-1-methylethyl) ether
108-60-1
8270E
ND
4.0
0.50
ug/L
1
4-Chloro-3-methyl phenol
59-50-7
8270E
ND
4.0
0.50
ug/L
1
4-Chloroaniline
106-47-8
8270E
ND
8.0
0.50
ug/L
1
bis(2-Chloroethoxy)methane
111-91-1
8270E
ND
4.0
0.50
ug/L
1
bis(2-Chloroethyl)ether
111-44-4
8270E
ND
4.0
0.50
ug/L
1
2-Chloronaphthalene
91-58-7
8270E
ND
4.0
0.50
ug/L
1
2-Chlorophenol
95-57-8
8270E
ND
4.0
0.50
ug/L
1
4-Chlorophenyl phenyl ether
7005-72-3
8270E
ND
4.0
0.50
ug/L
1
Chrysene
218-01-9
8270E
ND
0.80
0.20
ug/L
1
Dibenzo(a,h)anthracene
53-70-3
8270E
ND
0.80
0.20
ug/L
1
Dibenzofuran
132-64-9
8270E
ND
4.0
0.50
ug/L
1
3,3'-Dichlorobenzidine
91-94-1
8270E
ND
4.0
1.8
ug/L
1
2,4-Dichlorophenol
120-83-2
8270E
ND
8.0
1.0
ug/L
1
Diethylphthalate
84-66-2
8270E
ND
4.0
0.50
ug/L
1
Dimethyl phthalate
131-11-3
8270E
ND
4.0
0.50
ug/L
1
2,4-Dimethylphenol
105-67-9
8270E
ND
4.0
1.0
ug/L
1
Di-n-butyl phthalate
84-74-2
8270E
ND
4.0
0.50
ug/L
1
4,6-Dinitro-2-methylphenol
534-52-1
8270E
ND
20
1.0
ug/L
1
2,4-Dinitrophenol
51-28-5
8270E
ND
20
1.0
ug/L
1
2,4-Dinitrotoluene
121-14-2
8270E
ND
8.0
0.50
ug/L
1
2,6-Dinitrotoluene
606-20-2
8270E
ND
8.0
0.50
ug/L
1
Di-n-octylphthalate
117-84-0
8270E
ND
4.0
0.50
ug/L
1
bis(2-Ethylhexyl)phthalate
117-81-7
8270E
ND
4.0
0.50
ug/L
1
Fluoranthene
206-44-0
8270E
ND
0.80
0.20
ug/L
1
Fluorene
86-73-7
8270E
ND
0.80
0.20
ug/L
1
Hexachlorobenzene
118-74-1
8270E
ND
4.0
0.50
ug/L
1
Hexachlorobutadiene
87-68-3
8270E
ND
4.0
0.50
ug/L
1
Hexachlorocyclopentadiene
77-47-4
8270E
ND
20
2.0
ug/L
1
LOQ = Limit of Quantitation B =
Detected in the method blank
E = Quantitation of
compound exceeded the calibration range
DL = Detection Limit
NO = Not detected at or above the DL N =
Recovery is out of criteria
P = The RPD between two GC columns exceeds 40 %
J = Estimated result <
LOQ and > DL
H = Out of holding time W =
Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
95 of 198

Semivolatile Organic Compounds by GC/MS
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-004
Description: MW-8 Matrix: Aqueous
Date Sampled:08/14/2019 1145 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 3520C 8270E 1 08/22/2019 2249 SCD 08/19/2019 1653 26336
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Hexachloroethane
67-72-1
8270E
ND
4.0
1.0
ug/L
1
Indeno(1,2,3-c,d)pyrene
193-39-5
8270E
ND
0.80
0.20
ug/L
1
Isophorone
78-59-1
8270E
ND
4.0
0.50
ug/L
1
2-Methylnaphthalene
91-57-6
8270E
ND
0.80
0.20
ug/L
1
2-Methylphenol
95-48-7
8270E
ND
4.0
1.0
ug/L
1
3+4-Methylphenol
106-44-5
8270E
ND
4.0
1.5
ug/L
1
Naphthalene
91-20-3
8270E
ND
0.80
0.20
ug/L
1
2-Nitroaniline
88-74-4
8270E
ND
8.0
0.50
ug/L
1
3-Nitroaniline
99-09-2
8270E
ND
8.0
1.0
ug/L
1
4-Nitroaniline
100-01-6
8270E
ND
8.0
1.5
ug/L
1
Nitrobenzene
98-95-3
8270E
ND
4.0
1.5
ug/L
1
2-Nitrophenol
88-75-5
8270E
ND
4.0
1.0
ug/L
1
4-Nitrophenol
100-02-7
8270E
ND
20
2.0
ug/L
1
N-Nitrosodi-n-propylamine
621-64-7
8270E
ND
4.0
0.50
ug/L
1
N-Nitrosodiphenylamine (Diphenylamine)
86-30-6
8270E
ND
4.0
0.50
ug/L
1
Pentachlorophenol
87-86-5
8270E
ND
20
2.0
ug/L
1
Phenanthrene
85-01-8
8270E
ND
0.80
0.20
ug/L
1
Phenol
108-95-2
8270E
ND
4.0
0.50
ug/L
1
Pyrene
129-00-0
8270E
ND
0.80
0.20
ug/L
1
2,4,5-Trichlorophenol
95-95-4
8270E
ND
4.0
0.50
ug/L
1
2,4,6-Trichlorophenol
88-06-2
8270E
ND
4.0
0.50
ug/L
1
Run
1 Acceptance
Surrogate
Q % Recovery Limits
2-Fluorobiphenyl
50
37-129
2-Fluorophenol
31
24-127
Nitrobenzene-d5
55
38-127
Phenol-d5
45
28-128
Terphenyl-d14
74
10-148
2,4,6-Tribromophenol
63
35-144
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
96 of 198

MADEP EPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-004
Description: MW-8 Matrix: Aqueous
Date Sampled:08/14/2019 1145 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run
Prep Method
Analytical Method Dilution
Analysis Date Analyst
Prep Date Batch
1
MADEP-EPH-
MADEP-EPH-04 1
08/28/2019 0125 CHG
08/26/2019 2111 27084
2
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 1933 CHG
08/29/2019 0911 27388
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C11 - C22 Aromatics MADEP-EPH-04 ND 100 100 ug/L 1
Run 1 Acceptance Run 2 Acceptance
Surrogate Q % Recovery Limits Q % Recovery Limits
o - Terphenyl (aromatic)
2-Fluorobiphenyl (fractionation 1)
2-Bromonaphthalene (fractionation 2)
78 40-140 H 83 40-140
127 40-140 H 105 40-140
91 40-140 H 95 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
97 of 198

MADEP EPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-004
Description: MW-8 Matrix: Aqueous
Date Sampled:08/14/2019 1145 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run
Prep Method
Analytical Method Dilution
Analysis Date Analyst
Prep Date Batch
1
MADEP-EPH-
MADEP-EPH-04 1
08/28/2019 0125 CHG
08/26/2019 2111 27084
2
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 1933 CHG
08/29/2019 0911 27388
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C11 - C22 Aromatics MADEP-EPH-04 ND H 110 110 ug/L 2
Run 1 Acceptance Run 2 Acceptance
Surrogate Q % Recovery Limits Q % Recovery Limits
o - Terphenyl (aromatic)
2-Fluorobiphenyl (fractionation 1)
2-Bromonaphthalene (fractionation 2)
78 40-140 H 83 40-140
127 40-140 H 105 40-140
91 40-140 H 95 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
98 of 198

MADEP EPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-004
Description: MW-8 Matrix: Aqueous
Date Sampled:08/14/2019 1145 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run
Prep Method
Analytical Method Dilution
Analysis Date Analyst
Prep Date Batch
1
MADEP-EPH-
MADEP-EPH-04 1
08/27/2019 2157 CHG
08/26/2019 2111 27085
2
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 1306 CHG
08/29/2019 0911 27385
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C18 Aliphatics MADEP-EPH- 120 B 100 100 ug/L 1
C19 - C36 Aliphatics MADEP-EPH-04 ND 100 100 ug/L 1
Run 1 Acceptance Run 2 Acceptance
Surrogate Q % Recovery Limits Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
69 40-140 H 73 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
99 of 198

MADEP EPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-004
Description: MW-8 Matrix: Aqueous
Date Sampled:08/14/2019 1145 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run
Prep Method
Analytical Method Dilution
Analysis Date Analyst
Prep Date Batch
1
MADEP-EPH-
MADEP-EPH-04 1
08/27/2019 2157 CHG
08/26/2019 2111 27085
2
MADEP-EPH-
MADEP-EPH-04 1
08/30/2019 1306 CHG
08/29/2019 0911 27385
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C18 Aliphatics MADEP-EPH-04 ND H 110 110 ug/L 2
C19 - C36 Aliphatics MADEP-EPH-04 ND H 110 110 ug/L 2
Run 1 Acceptance Run 2 Acceptance
Surrogate Q % Recovery Limits Q % Recovery Limits
1-Chloro-octadecane (aliphatic)
69 40-140 H 73 40-140
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
100 of 198

MADEP VPH (aliphatics)
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-004
Description: MW-8 Matrix: Aqueous
Date Sampled:08/14/2019 1145 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 08/18/2019 0125 JJG 26245
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C5 - C8 Aliphatics MADEP-VPH- ND 75 15 ug/L 1
C9 - C12 Aliphatics MADEP-VPH- ND 75 15 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (FID)
119 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
101 of 198

MADEP VPH (aromatics)
Client:Terracon Consultants, Inc. Laboratory I D: UH 15079-004
Description: MW-8 Matrix: Aqueous
Date Sampled:08/14/2019 1145 Project Name: Mt. Pleasant Maintenance
Date Received:08/15/2019 Project Number: 71177023
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 VPH MADEP-VPH-18-2.1 1 08/18/2019 0125 JJG 26244
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
C9 - C10 Aromatics MADEP-VPH- 7.2 J 25 5.0 ug/L 1
Run 1 Acceptance
Surrogate Q % Recovery Limits
2,5-Dibromotoluene (PID)
117 70-130
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit
NO = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL
H = Out of holding time W = Reported on wet weight basis
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
102 of 198

QC Summary
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
103 of 198

Volatile Organic Compounds by GC/MS - MB
Sample ID: UQ26199-001 Matrix: Aqueous
Batch: 26199 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
10
4.0
ug/L
08/16/2019 2106
Benzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Bromodichloromethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Bromoform
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Bromomethane (Methyl bromide)
ND
1
0.50
0.40
ug/L
08/16/2019 2106
2-Butanone (MEK)
ND
1
10
2.0
ug/L
08/16/2019 2106
Carbon disulfide
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Carbon tetrachloride
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Chlorobenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Chloroethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Chloroform
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Chloromethane (Methyl chloride)
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Cyclohexane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Dibromochloromethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,2-Dibromoethane (EDB)
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,2-Dichlorobenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,3-Dichlorobenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,4-Dichlorobenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Dichlorodifluoromethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,1-Dichloroethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,2-Dichloroethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,1-Dichloroethene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
cis- 1,2-Dichloroethene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
trans- 1,2-Dichloroethene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,2-Dichloropropane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
cis- 1,3-Dichloropropene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
trans- 1,3-Dichloropropene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Ethylbenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
2-Hexanone
ND
1
10
2.0
ug/L
08/16/2019 2106
Isopropylbenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Methyl acetate
ND
1
1.0
0.40
ug/L
08/16/2019 2106
Methyl tertiary butyl ether (MTBE)
ND
1
0.50
0.40
ug/L
08/16/2019 2106
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
08/16/2019 2106
Methylcyclohexane
ND
1
5.0
0.40
ug/L
08/16/2019 2106
Methylene chloride
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Styrene
ND
1
0.50
0.41
ug/L
08/16/2019 2106
1,1,2,2-Tetrachloroethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Tetrachloroethene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Toluene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,1,2-Trichloro-1,2,2-Trifluoroethane
ND
1
1.0
0.42
ug/L
08/16/2019 2106
1,2,4-Trichlorobenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,1,1-Trichloroethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,1,2-Trichloroethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
itell no SLT-]

Volatile Organic Compounds by GC/MS - MB
Sample ID: UQ26199-001 Matrix: Aqueous
Batch: 26199 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Trichloroethene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Trichlorofluoromethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Vinyl chloride
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Xylenes (total)
ND
1
1.0
0.40
ug/L
08/16/2019 2106
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 101 70-130
1,2-Dichloroethane-d4 100 70-130
Toluene-d8 108 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
105 of 198

Volatile Organic Compounds by GC/MS - LCS
Sample ID: UQ26199-002
Matrix: Aqueous
Batch: 26199
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
90
1
90
60-140
08/16/2019 1938
Benzene
50
48
1
96
70-130
08/16/2019 1938
Bromodichloromethane
50
49
1
99
70-130
08/16/2019 1938
Bromoform
50
43
1
86
70-130
08/16/2019 1938
Bromomethane (Methyl bromide)
50
50
1
99
70-130
08/16/2019 1938
2-Butanone (MEK)
100
96
1
96
70-130
08/16/2019 1938
Carbon disulfide
50
46
1
91
70-130
08/16/2019 1938
Carbon tetrachloride
50
53
1
106
70-130
08/16/2019 1938
Chlorobenzene
50
48
1
97
70-130
08/16/2019 1938
Chloroethane
50
47
1
93
70-130
08/16/2019 1938
Chloroform
50
46
1
92
70-130
08/16/2019 1938
Chloromethane (Methyl chloride)
50
47
1
94
60-140
08/16/2019 1938
Cyclohexane
50
48
1
97
70-130
08/16/2019 1938
1,2-Dibromo-3-chloropropane (DBCP)
50
48
1
96
70-130
08/16/2019 1938
Dibromochloromethane
50
51
1
101
70-130
08/16/2019 1938
1,2-Dibromoethane (EDB)
50
50
1
101
70-130
08/16/2019 1938
1,2-Dichlorobenzene
50
49
1
99
70-130
08/16/2019 1938
1,3-Dichlorobenzene
50
50
1
99
70-130
08/16/2019 1938
1,4-Dichlorobenzene
50
48
1
96
70-130
08/16/2019 1938
Dichlorodifluoromethane
50
52
1
103
60-140
08/16/2019 1938
1,1-Dichloroethane
50
46
1
91
70-130
08/16/2019 1938
1,2-Dichloroethane
50
48
1
95
70-130
08/16/2019 1938
1,1-Dichloroethene
50
48
1
96
70-130
08/16/2019 1938
cis- 1,2-Dichloroethene
50
47
1
93
70-130
08/16/2019 1938
trans- 1,2-Dichloroethene
50
48
1
96
70-130
08/16/2019 1938
1,2-Dichloropropane
50
46
1
93
70-130
08/16/2019 1938
cis- 1,3-Dichloropropene
50
50
1
100
70-130
08/16/2019 1938
trans- 1,3-Dichloropropene
50
51
1
101
70-130
08/16/2019 1938
Ethylbenzene
50
50
1
100
70-130
08/16/2019 1938
2-Hexanone
100
100
1
103
70-130
08/16/2019 1938
Isopropylbenzene
50
51
1
102
70-130
08/16/2019 1938
Methyl acetate
50
50
1
100
70-130
08/16/2019 1938
Methyl tertiary butyl ether (MTBE)
50
45
1
90
70-130
08/16/2019 1938
4-Methyl-2-pentanone
100
99
1
99
70-130
08/16/2019 1938
Methylcyclohexane
50
51
1
103
70-130
08/16/2019 1938
Methylene chloride
50
44
1
89
70-130
08/16/2019 1938
Styrene
50
52
1
104
70-130
08/16/2019 1938
1,1,2,2-Tetrachloroethane
50
50
1
100
70-130
08/16/2019 1938
Tetrachloroethene
50
51
1
103
70-130
08/16/2019 1938
Toluene
50
49
1
98
70-130
08/16/2019 1938
1,1,2-Trichloro-1,2,2-Trifluoroethane
50
52
1
103
70-130
08/16/2019 1938
1,2,4-Trichlorobenzene
50
51
1
103
70-130
08/16/2019 1938
1,1,1-Trichloroethane
50
49
1
98
70-130
08/16/2019 1938
1,1,2-Trichloroethane
50
49
1
98
70-130
08/16/2019 1938
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Volatile Organic Compounds by GC/MS - LCS
Sample ID: UQ26199-002
Matrix: Aqueous
Batch: 26199
Prep Method: 5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit
Analysis Date
Trichloroethene
50
51
1 101
70-130
08/16/2019 1938
Trichlorofluoromethane
50
50
1 101
70-130
08/16/2019 1938
Vinyl chloride
50
48
1 95
70-130
08/16/2019 1938
Xylenes (total)
100
99
1 99
70-130
08/16/2019 1938
Surrogate
Q % Rec
Acceptance
Limit
Bromofluorobenzene 90 70-130
1,2-Dichloroethane-d4 93 70-130
Toluene-d8 96 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: UQ26336-001 Matrix: Aqueous
Batch:26336 Prep Method: 3520C
Analytical Method: 8270E Prep Date: 08/19/2019 1653
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acenaphthene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Acenaphthylene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Acetophenone
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Anthracene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Atrazine
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Benzaldehyde
ND
1
8.0
0.50
ug/L
08/22/2019 1642
Benzo(a)anthracene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Benzo(a)pyrene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Benzo(k)fluoranthene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Benzo(g,h,i)perylene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Benzo(k)fluoranthene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
1,1'-Biphenyl
ND
1
4.0
0.50
ug/L
08/22/2019 1642
4-Bromophenyl phenyl ether
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Butyl benzyl phthalate
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Caprolactam
4.5 J
1
8.0
1.0
ug/L
08122/20191642
Carbazole
ND
1
4.0
0.50
ug/L
08/22/2019 1642
bis (2-Chloro-1-methylethyl) ether
ND
1
4.0
0.50
ug/L
08/22/2019 1642
4-Chloro-3-methyl phenol
ND
1
4.0
0.50
ug/L
08/22/2019 1642
4-Chloroaniline
ND
1
8.0
0.50
ug/L
08/22/2019 1642
bis(2-Chloroethoxy)methane
ND
1
4.0
0.50
ug/L
08/22/2019 1642
bis(2-Chloroethyl)ether
ND
1
4.0
0.50
ug/L
08/22/2019 1642
2-Chloronaphthalene
ND
1
4.0
0.50
ug/L
08/22/2019 1642
2-Chlorophenol
ND
1
4.0
0.50
ug/L
08/22/2019 1642
4-Chlorophenyl phenyl ether
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Chrysene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Dibenzo(a,h)anthracene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Dibenzofuran
ND
1
4.0
0.50
ug/L
08/22/2019 1642
3,3'-Dichlorobenzidine
ND
1
4.0
1.8
ug/L
08/22/2019 1642
2,4-Dichlorophenol
ND
1
8.0
1.0
ug/L
08/22/2019 1642
Diethylphthalate
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Dimethyl phthalate
ND
1
4.0
0.50
ug/L
08/22/2019 1642
2,4-Dimethylphenol
ND
1
4.0
1.0
ug/L
08/22/2019 1642
Di-n-butyl phthalate
ND
1
4.0
0.50
ug/L
08/22/2019 1642
4,6-Dinitro-2-methyl phenol
ND
1
20
1.0
ug/L
08/22/2019 1642
2,4-Dinitrophenol
ND
1
20
1.0
ug/L
08/22/2019 1642
2,4-Dinitrotoluene
ND
1
8.0
0.50
ug/L
08/22/2019 1642
2,6-Dinitrotoluene
ND
1
8.0
0.50
ug/L
08/22/2019 1642
Di-n-octylphthalate
ND
1
4.0
0.50
ug/L
08/22/2019 1642
bis(2-Ethylhexyl)phthalate
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Fluoranthene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Fluorene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Hexachlorobenzene
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Hexachlorobutadiene
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Hexachlorocyclopentadiene
ND
1
20
2.0
ug/L
08/22/2019 1642
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
108 of 198

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: UQ26336-001 Matrix: Aqueous
Batch:26336 Prep Method: 3520C
Analytical Method: 8270E Prep Date: 08/19/2019 1653
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Hexachloroethane
ND
1
4.0
1.0
ug/L
08/22/20191642
Indeno(1,2,3-c,d)pyrene
ND
1
0.80
0.20
ug/L
08/22/20191642
Isophorone
ND
1
4.0
0.50
ug/L
08/22/20191642
2-Methyl naphthalene
ND
1
0.80
0.20
ug/L
08/22/20191642
2-Methylphenol
ND
1
4.0
1.0
ug/L
08/22/20191642
3+4-Methylphenol
ND
1
4.0
1.5
ug/L
08/22/20191642
Naphthalene
ND
1
0.80
0.20
ug/L
08/22/20191642
2-Nitroaniline
ND
1
8.0
0.50
ug/L
08/22/20191642
3-Nitroaniline
ND
1
8.0
1.0
ug/L
08/22/20191642
4-Nitroaniline
ND
1
8.0
1.5
ug/L
08/22/20191642
Nitrobenzene
ND
1
4.0
1.5
ug/L
08/22/20191642
2-Nitrophenol
ND
1
4.0
1.0
ug/L
08/22/20191642
4-Nitrophenol
ND
1
20
2.0
ug/L
08/22/20191642
N-Nitrosodi-n-propylamine
ND
1
4.0
0.50
ug/L
08/22/20191642
N-Nitrosodiphenylamine (Diphenylamine)
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Pentachlorophenol
ND
1
20
2.0
ug/L
08/22/20191642
Phenanthrene
ND
1
0.80
0.20
ug/L
08/22/20191642
Phenol
ND
1
4.0
0.50
ug/L
08/22/20191642
Pyrene
ND
1
0.80
0.20
ug/L
08/22/20191642
2,4,5-Trichlorophenol
ND
1
4.0
0.50
ug/L
08/22/20191642
2,4,6-Trichlorophenol
ND
1
4.0
0.50
ug/L
08/22/20191642
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 48 37-129
2-Fluorophenol 30 24-127
Nitrobenzene-d5
55
38-127
Phenol-d5
38
28-128
Terphenyl-d 14
71
10-148
2,4,6-Tribromophenol
50
35-144
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
iDR]no SLIT-]

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: UQ26336-002
Matrix: Aqueous
Batch:26336
Prep Method:
3520C
Analytical Method: 8270E
Prep Date: 08/19/2019 1653
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acenaphthene
40
24
1
59
30-122
08/22/2019 1706
Acenaphthylene
40
25
1
61
30-130
08/22/2019 1706
Acetophenone
40
33
1
83
30-130
08/22/2019 1706
Anthracene
40
23
1
57
30-123
08/22/2019 1706
Atrazine
40
25
1
62
30-130
08/22/2019 1706
Benzaldehyde
40
18
1
46
20-115
08/22/2019 1706
Benzo(a)anthracene
40
25
1
63
40-125
08/22/2019 1706
Benzo(a)pyrene
40
22
1
56
40-128
08/22/2019 1706
Benzo(k)fluoranthene
40
24
1
60
30-130
08/22/2019 1706
Benzo(g,h,i)perylene
40
31
1
77
30-130
08/22/2019 1706
Benzo(k)fluoranthene
40
24
1
60
30-130
08/22/2019 1706
1,1'-Biphenyl
40
24
1
59
30-130
08/22/2019 1706
4-Bromophenyl phenyl ether
40
22
1
55
30-124
08/22/2019 1706
Butyl benzyl phthalate
40
32
1
81
30-130
08/22/2019 1706
Caprolactam
40
32
1
80
30-130
08/22/2019 1706
Carbazole
40
23
1
58
30-130
08/22/2019 1706
bis (2-Chloro-1-methylethyl) ether
40
41
1
102
30-130
08/22/2019 1706
4-Chloro-3-methyl phenol
40
30
1
74
30-123
08/22/2019 1706
4-Chloroaniline
40
22
1
54
12-157
08/22/2019 1706
bis(2-Chloroethoxy)methane
40
27
1
68
30-130
08/22/2019 1706
bis(2-Chloroethyl)ether
40
35
1
87
30-130
08/22/2019 1706
2-Chloronaphthalene
40
24
1
61
30-130
08/22/2019 1706
2-Chlorophenol
40
28
1
71
30-130
08/22/2019 1706
4-Chlorophenyl phenyl ether
40
22
1
55
30-121
08/22/2019 1706
Chrysene
40
24
1
59
30-130
08/22/2019 1706
Dibenzo(a,h)anthracene
40
28
1
69
30-130
08/22/2019 1706
Dibenzofuran
40
23
1
58
30-118
08/22/2019 1706
3,3'-Dichlorobenzidine
40
21
1
52
10-126
08/22/2019 1706
2,4-Dichlorophenol
40
24
1
59
30-121
08/22/2019 1706
Diethylphthalate
40
27
1
69
40-125
08/22/2019 1706
Dimethyl phthalate
40
26
1
64
40-127
08/22/2019 1706
2,4-Dimethylphenol
40
28
1
71
20-125
08/22/2019 1706
Di-n-butyl phthalate
40
26
1
66
40-127
08/22/2019 1706
4,6-Dinitro-2-methyl phenol
40
21
1
53
30-130
08/22/2019 1706
2,4-Dinitrophenol
80
41
1
51
11-126
08/22/2019 1706
2,4-Dinitrotoluene
40
25
1
62
30-130
08/22/2019 1706
2,6-Dinitrotoluene
40
25
1
64
30-130
08/22/2019 1706
Di-n-octylphthalate
40
32
1
79
30-130
08/22/2019 1706
bis(2-Ethylhexyl)phthalate
40
32
1
80
30-130
08/22/2019 1706
Fluoranthene
40
22
1
55
40-128
08/22/2019 1706
Fluorene
40
24
1
59
30-124
08/22/2019 1706
Hexachlorobenzene
40
26
1
64
30-125
08/22/2019 1706
Hexachlorobutadiene
40
23
1
56
24-110
08/22/2019 1706
Hexachlorocyclopentadiene
200
100
1
52
22-122
08/22/2019 1706
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
ifiGZ.iitiRT:1

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: UQ26336-002
Matrix: Aqueous
Batch:26336
Prep Method:
3520C
Analytical Method: 8270E
Prep Date: 08/19/2019 1653
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
Hexachloroethane
40
28
1
69
30-130
08/22/20191706
Indeno(1,2,3-c,d)pyrene
40
26
1
66
30-130
08/22/20191706
Isophorone
40
29
1
72
30-130
08/22/20191706
2-Methyl naphthalene
40
25
1
61
40-132
08/22/20191706
2-Methylphenol
40
34
1
86
30-130
08/22/20191706
3+4-Methylphenol
40
34
1
85
30-130
08/22/20191706
Naphthalene
40
25
1
62
30-130
08/22/20191706
2-Nitroaniline
40
28
1
71
30-130
08/22/20191706
3-Nitroaniline
40
21
1
53
30-130
08/22/20191706
4-Nitroaniline
40
28
1
70
30-135
08/22/20191706
Nitrobenzene
40
28
1
69
30-130
08/22/20191706
2-Nitrophenol
40
26
1
65
30-130
08/22/20191706
4-Nitrophenol
80
51
1
63
30-130
08/22/20191706
N-Nitrosodi-n-propylamine
40
33
1
83
30-130
08/22/20191706
N-Nitrosodiphenylamine (Diphenylamine)
40
22
1
56
30-123
08/22/2019 1706
Pentachlorophenol
80
41
1
51
30-130
08/22/20191706
Phenanthrene
40
23
1
59
40-123
08/22/20191706
Phenol
40
29
1
73
30-130
08/22/20191706
Pyrene
40
25
1
62
40-126
08/22/20191706
2,4,5-Trichlorophenol
40
22
1
55
30-123
08/22/20191706
2,4,6-Trichlorophenol
40
24
1
60
30-130
08/22/20191706
Surrogate
Q % Rec
Acceptance
Limit
2-Fluorobiphenyl
57
37-129
2-Fluorophenol
69
24-127
Nitrobenzene-d5
70
38-127
Phenol-d5
75
28-128
Terphenyl-d 14
69
10-148
2,4,6-Tribromophenol
64
35-144
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
ififiriitiRT:1

Semivolatile Organic Compounds by GC/MS - MS
Sample ID: UH15076-001MS
Matrix: Aqueous
Batch:26336
Prep Method: 3520C
Analytical Method: 8270E
Prep Date: 08/19/2019 1653
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acenaphthene
ND
80
46
1
57
30-122
08/23/2019 0003
Acenaphthylene
ND
80
45
1
57
30-130
08/23/2019 0003
Acetophenone
ND
80
59
1
73
30-130
08/23/2019 0003
Anthracene
ND
80
46
1
58
30-123
08/23/2019 0003
Atrazine
ND
80
49
1
61
30-130
08/23/2019 0003
Benzaldehyde
ND
80
32
1
40
20-115
08/23/2019 0003
Benzo(a)anthracene
ND
80
49
1
61
40-125
08/23/2019 0003
Benzo(a)pyrene
ND
80
45
1
56
40-128
08/23/2019 0003
Benzo(k)fluoranthene
ND
80
47
1
58
30-130
08/23/2019 0003
Benzo(g,h,i)perylene
ND
80
41
1
51
30-130
08/23/2019 0003
Benzo(k)fluoranthene
ND
80
45
1
56
30-130
08/23/2019 0003
1,1'-Biphenyl
ND
80
43
1
54
30-130
08/23/2019 0003
4-Bromophenyl phenyl ether
ND
80
42
1
53
30-124
08/23/2019 0003
Butyl benzyl phthalate
ND
80
63
1
78
30-130
08/23/2019 0003
Caprolactam
ND
80
57
1
71
30-130
08/23/2019 0003
Carbazole
ND
80
48
1
60
30-130
08/23/2019 0003
bis (2-Chloro-1-methylethyl) ether
ND
80
69
1
87
30-130
08/23/2019 0003
4-Chloro-3-methyl phenol
ND
80
55
1
69
30-123
08/23/2019 0003
4-Chloroaniline
ND
80
35
1
44
10-130
08/23/2019 0003
bis(2-Chloroethoxy)methane
ND
80
49
1
61
30-130
08/23/2019 0003
bis(2-Chloroethyl)ether
ND
80
60
1
76
30-130
08/23/2019 0003
2-Chloronaphthalene
ND
80
43
1
54
30-130
08/23/2019 0003
2-Chlorophenol
ND
80
52
1
65
30-130
08/23/2019 0003
4-Chlorophenyl phenyl ether
ND
80
41
1
52
30-121
08/23/2019 0003
Chrysene
ND
80
46
1
58
30-130
08/23/2019 0003
Dibenzo(a,h)anthracene
ND
80
41
1
52
30-130
08/23/2019 0003
Dibenzofuran
ND
80
46
1
57
30-118
08/23/2019 0003
3,3'-Dichlorobenzidine
ND
80
39
1
49
10-126
08/23/2019 0003
2,4-Dichlorophenol
ND
80
45
1
56
30-121
08/23/2019 0003
Diethylphthalate
ND
80
55
1
69
40-125
08/23/2019 0003
Dimethyl phthalate
ND
80
49
1
61
40-127
08/23/2019 0003
2,4-Dimethylphenol
ND
80
52
1
66
20-125
08/23/2019 0003
Di-n-butyl phthalate
ND
80
53
1
67
40-127
08/23/2019 0003
4,6-Dinitro-2-methyl phenol
ND
80
41
1
51
30-130
08/23/2019 0003
2,4-Dinitrophenol
ND
160
84
1
53
30-130
08/23/2019 0003
2,4-Dinitrotoluene
ND
80
50
1
62
30-130
08/23/2019 0003
2,6-Dinitrotoluene
ND
80
47
1
59
30-130
08/23/2019 0003
Di-n-octylphthalate
ND
80
66
1
82
30-130
08/23/2019 0003
bis(2-Ethylhexyl)phthalate
ND
80
65
1
81
70-131
08/23/2019 0003
Fluoranthene
ND
80
43
1
54
40-128
08/23/2019 0003
Fluorene
ND
80
45
1
56
30-124
08/23/2019 0003
Hexachlorobenzene
ND
80
51
1
64
30-125
08/23/2019 0003
Hexachlorobutadiene
ND
80
41
1
51
24-110
08/23/2019 0003
Hexachlorocyclopentadiene
ND
400
170
1
42
22-122
08/23/2019 0003
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
ifipZ6i1111 3

Semivolatile Organic Compounds by GC/MS - MS
Sample ID: UH15076-001MS
Matrix: Aqueous
Batch:26336
Prep Method: 3520C
Analytical Method: 8270E
Prep Date: 08/19/2019 1653
Sample
Spike
Amount
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Hexachloroethane
ND
80
49
1
61
30-130
08/23/2019 0003
Indeno(1,2,3-c,d)pyrene
ND
80
40
1
50
30-130
08/23/2019 0003
Isophorone
ND
80
51
1
64
30-130
08/23/2019 0003
2-Methyl naphthalene
ND
80
43
1
54
40-132
08/23/2019 0003
2-Methylphenol
ND
80
74
1
92
30-130
08/23/2019 0003
3+4-Methylphenol
ND
80
63
1
78
30-130
08/23/2019 0003
Naphthalene
ND
80
46
1
57
30-130
08/23/2019 0003
2-Nitroaniline
ND
80
54
1
68
30-130
08/23/2019 0003
3-Nitroaniline
ND
80
41
1
51
30-130
08/23/2019 0003
4-Nitroaniline
ND
80
51
1
64
30-135
08/23/2019 0003
Nitrobenzene
ND
80
50
1
63
30-130
08/23/2019 0003
2-Nitrophenol
ND
80
47
1
59
30-130
08/23/2019 0003
4-Nitrophenol
ND
160
120
1
78
30-130
08/23/2019 0003
N-Nitrosodi-n-propylamine
ND
80
60
1
75
30-130
08/23/2019 0003
N-Nitrosodiphenylamine (Diphenylamine)
ND
80
44
1
56
30-123
08/23/2019 0003
Pentachlorophenol
ND
160
83
1
52
30-130
08/23/2019 0003
Phenanthrene
ND
80
45
1
56
40-123
08/23/2019 0003
Phenol
ND
80
53
1
67
30-130
08/23/2019 0003
Pyrene
ND
80
52
1
65
40-126
08/23/2019 0003
2,4,5-Trichlorophenol
ND
80
45
1
56
30-123
08/23/2019 0003
2,4,6-Trichlorophenol
ND
80
43
1
54
30-130
08/23/2019 0003
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 51 37-129
2-Fluorophenol 62 24-127
Nitrobenzene-d5 58 38-127
Phenol-d5 66 28-128
Terphenyl-d 14 66 10-148
2,4,6-Tribromophenol 64 35-144
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
113 of 198

Semivolatile Organic Compounds by GC/MS - MSD
Sample ID: UH15076-001MID
Matrix: Aqueous
Batch:26336
Prep Method:
3520C
Analytical Method: 8270E
Prep Date: 08/19/2019 1653
Sample
Spike
Amount
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec % RPD
Limit
Limit
Analysis Date
Acenaphthene
ND
80
47
1
59
3.9
30-122
40
08/23/2019 0027
Acenaphthylene
ND
80
48
1
60
5.9
30-130
40
08/23/2019 0027
Acetophenone
ND
80
59
1
74
0.68
30-130
40
08/23/2019 0027
Anthracene
ND
80
46
1
58
0.39
30-123
40
08/23/2019 0027
Atrazine
ND
80
47
1
59
3.8
30-130
40
08/23/2019 0027
Benzaldehyde
ND
80
25
1
32
23
20-115
40
08/23/2019 0027
Benzo(a)anthracene
ND
80
53
1
66
7.5
40-125
40
08/23/2019 0027
Benzo(a)pyrene
ND
80
49
1
62
9.8
40-128
40
08/23/2019 0027
Benzo(k)fluoranthene
ND
80
46
1
57
1.8
30-130
40
08/23/2019 0027
Benzo(g,h,i)perylene
ND
80
35
1
44
15
30-130
40
08/23/2019 0027
Benzo(k)fluoranthene
ND
80
48
1
60
7.1
30-130
40
08/23/2019 0027
1,1'-Biphenyl
ND
80
47
1
59
8.0
30-130
40
08/23/2019 0027
4-Bromophenyl phenyl ether
ND
80
43
1
53
0.71
30-124
40
08/23/2019 0027
Butyl benzyl phthalate
ND
80
64
1
80
1.9
30-130
40
08/23/2019 0027
Caprolactam
ND
80
69
1
86
19
30-130
40
08/23/2019 0027
Carbazole
ND
80
48
1
60
0.79
30-130
40
08/23/2019 0027
bis (2-Chloro-1-methylethyl) ether
ND
80
69
1
87
0.026
30-130
40
08/23/2019 0027
4-Chloro-3-methyl phenol
ND
80
57
1
72
4.7
30-123
40
08/23/2019 0027
4-Chloroaniline
ND
80
33
1
41
6.8
10-130
40
08/23/2019 0027
bis(2-Chloroethoxy)methane
ND
80
54
1
68
11
30-130
40
08/23/2019 0027
bis(2-Chloroethyl)ether
ND
80
58
1
73
3.3
30-130
40
08/23/2019 0027
2-Chloronaphthalene
ND
80
47
1
59
7.6
30-130
40
08/23/2019 0027
2-Chlorophenol
ND
80
51
1
63
2.3
30-130
40
08/23/2019 0027
4-Chlorophenyl phenyl ether
ND
80
44
1
55
6.2
30-121
40
08/23/2019 0027
Chrysene
ND
80
46
1
58
0.74
30-130
40
08/23/2019 0027
Dibenzo(a,h)anthracene
ND
80
41
1
51
1.7
30-130
40
08/23/2019 0027
Dibenzofuran
ND
80
47
1
59
3.1
30-118
40
08/23/2019 0027
3,3'-Dichlorobenzidine
ND
80
41
1
52
5.7
10-126
40
08/23/2019 0027
2,4-Dichlorophenol
ND
80
49
1
61
8.9
30-121
40
08/23/2019 0027
Diethylphthalate
ND
80
56
1
70
1.3
40-125
40
08/23/2019 0027
Dimethyl phthalate
ND
80
53
1
66
8.3
40-127
40
08/23/2019 0027
2,4-Dimethylphenol
ND
80
56
1
71
7.3
20-125
40
08/23/2019 0027
Di-n-butyl phthalate
ND
80
57
1
71
6.9
40-127
40
08/23/2019 0027
4,6-Dinitro-2-methyl phenol
ND
80
42
1
53
3.3
30-130
40
08/23/2019 0027
2,4-Dinitrophenol
ND
160
85
1
53
0.10
30-130
40
08/23/2019 0027
2,4-Dinitrotoluene
ND
80
51
1
64
3.6
30-130
40
08/23/2019 0027
2,6-Dinitrotoluene
ND
80
51
1
63
7.7
30-130
40
08/23/2019 0027
Di-n-octylphthalate
ND
80
62
1
78
5.9
30-130
40
08/23/2019 0027
bis(2-Ethylhexyl)phthalate
ND
80
67
1
83
3.1
70-131
40
08/23/2019 0027
Fluoranthene
ND
80
43
1
54
0.36
40-128
40
08/23/2019 0027
Fluorene
ND
80
47
1
58
3.8
30-124
40
08/23/2019 0027
Hexachlorobenzene
ND
80
48
1
60
5.1
30-125
40
08/23/2019 0027
Hexachlorobutadiene
ND
80
47
1
59
16
24-110
40
08/23/2019 0027
Hexachlorocyclopentadiene
ND
400
190
1
48
13
22-122
40
08/23/2019 0027
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
114 of 198

Semivolatile Organic Compounds by GC/MS - MSD
Sample ID: UH15076-001MID
Matrix: Aqueous
Batch:26336
Prep Method:
3520C
Analytical Method: 8270E
Prep Date: 08/19/2019 1653
Sample
Spike
Amount
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L)
(ug/L)
Q Dil
% Rec % RPD
Limit
Limit
Analysis Date
Hexachloroethane
ND
80
53
1
66
6.7
30-130
40
08/23/2019 0027
Indeno(1,2,3-c,d)pyrene
ND
80
39
1
48
3.1
30-130
40
08/23/2019 0027
Isophorone
ND
80
58
1
72
12
30-130
40
08/23/2019 0027
2-Methyl naphthalene
ND
80
49
1
61
12
40-132
40
08/23/2019 0027
2-Methylphenol
ND
80
72
1
90
3.0
30-130
40
08/23/2019 0027
3+4-Methylphenol
ND
80
60
1
75
4.7
30-130
40
08/23/2019 0027
Naphthalene
ND
80
49
1
61
6.2
30-130
40
08/23/2019 0027
2-Nitroaniline
ND
80
58
1
72
6.4
30-130
40
08/23/2019 0027
3-Nitroaniline
ND
80
39
1
49
4.2
30-130
40
08/23/2019 0027
4-Nitroaniline
ND
80
55
1
69
7.1
30-135
40
08/23/2019 0027
Nitrobenzene
ND
80
55
1
69
8.6
30-130
40
08/23/2019 0027
2-Nitrophenol
ND
80
51
1
64
7.6
30-130
40
08/23/2019 0027
4-Nitrophenol
ND
160
130
1
83
6.7
30-130
40
08/23/2019 0027
N-Nitrosodi-n-propylamine
ND
80
61
1
76
1.5
30-130
40
08/23/2019 0027
N-Nitrosodiphenylamine (Diphenylamine)
ND
80
46
1
58
4.2
30-123
40
08/23/2019 0027
Pentachlorophenol
ND
160
83
1
52
0.11
30-130
40
08/23/2019 0027
Phenanthrene
ND
80
44
1
55
1.9
40-123
40
08/23/2019 0027
Phenol
ND
80
54
1
68
2.1
30-130
40
08/23/2019 0027
Pyrene
ND
80
49
1
61
6.1
40-126
40
08/23/2019 0027
2,4,5-Trichlorophenol
ND
80
48
1
60
7.9
30-123
40
08/23/2019 0027
2,4,6-Trichlorophenol
ND
80
48
1
60
9.8
30-130
40
08/23/2019 0027
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 57 37-129
2-Fluorophenol 59 24-127
Nitrobenzene-d5 66 38-127
Phenol-d5 66 28-128
Terphenyl-d 14 70 10-148
2,4,6-Tribromophenol 66 35-144
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
isF7.ii5RU

MADEP EPH (aromatics) - MB
Sample ID: UQ27084-001 Matrix: Aqueous
Batch: 27084 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 08/26/2019 2111
Parameter Result Q Dil LOQ DL Units Analysis Date
C11 - C22 Aromatics ND 1 100 100 ug/L 08/27/2019 2227
Acceptance
Surrogate Q % Rec Limit
o - Terphenyl (aromatic) 85 40-140
2-Fluorobiphenyl (fractionation 1) 123 40-140
2-Bromonaphthalene (fractionation 2) 111 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP EPH (aromatics) - LCS
Sample ID: UQ27084-002
Matrix: Aqueous
Batch: 27084
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 08/26/2019 2111
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec Limit Analysis Date
C11 - C22 Aromatics
850
740
1 87 40-140 08/27/2019 2257
Surrogate
Q % Rec
Acceptance
Limit
o - Terphenyl (aromatic) 92 40-140
2-Fluorobiphenyl (fractionation 1) 130 40-140
2-Bromonaphthalene (fractionation 2) 113 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP EPH (aromatics) - LCSD
Sample ID: UQ27084-003 Matrix: Aqueous
Batch: 27084 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 08/26/2019 2111
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
C11 - C22 Aromatics 850 740 1 87 0.89 40-140 25 08/27/2019 2326
Surrogate
o - Terphenyl (aromatic)
2-Fluorobiphenyl (fractionation 1)
2-Bromonaphthalene (fractionation 2)
Acceptance
Q % Rec Limit
92
40-140
129
40-140
112
40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
118 of 198

MADEP EPH (aliphatics) - MB
Sample ID: UQ27085-001 Matrix: Aqueous
Batch: 27085 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 08/26/2019 2111
Parameter Result Q Dil LOQ DL Units Analysis Date
C9 - C18 Aliphatics 100 1 100 100 ug/L 08/27/2019 1859
C19 - C36 Aliphatics ND 1 100 100 ug/L 08/27/2019 1859
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) 81 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
li 111i R1 no 5LIT:]

MADEP EPH (aliphatics) - LCS
Sample ID: UQ27085-002
Matrix: Aqueous
Batch: 27085
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 08/26/2019 2111
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit Analysis Date
C9 - C18 Aliphatics
300
260
1 88
40-140 08/27/2019 1928
C19 - C36 Aliphatics
400
380
1 95
40-140 08/27/2019 1928
Surrogate
Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic) 83 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
120 of 198

MADEP EPH (aliphatics) - LCSD
Sample ID: UQ27085-003
Matrix: Aqueous
Batch: 27085
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 08/26/2019 2111
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil % Rec % RPD Limit
Limit Analysis Date
C9 - C18 Aliphatics
300
300
1 99 12 40-140
25 08/27/2019 1958
C19 - C36 Aliphatics
400
400
1 100 5.0 40-140
25 08/27/2019 1958
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) 83 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
iPAW6i501.1

MADEP EPH (aliphatics) - MB
Sample ID: UQ27385-001 Matrix: Aqueous
Batch: 27385 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 08/29/2019 911
Parameter Result Q Dil LOQ DL Units Analysis Date
C9 - C18 Aliphatics ND 1 100 100 ug/L 08/30/2019 0552
C19 - C36 Aliphatics ND 1 100 100 ug/L 08/30/2019 0552
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) 83 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
122 of 198

MADEP EPH (aliphatics) - LCS
Sample ID: UQ27385-002
Matrix: Aqueous
Batch: 27385
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 08/29/2019 911
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
Limit Analysis Date
C9 - C18 Aliphatics
300
170
1 57
40-140 08/30/2019 0621
C19 - C36 Aliphatics
400
410
1 102
40-140 08/30/2019 0621
Surrogate
Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic) 87 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
iP4c37itiRT:1

MADEP EPH (aliphatics) - LCSD
Sample ID: UQ27385-003
Matrix: Aqueous
Batch: 27385
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 08/29/2019 911
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil % Rec % RPD Limit
Limit Analysis Date
C9 - C18 Aliphatics
300
180
1 60 6.1 40-140
25 08/30/2019 0650
C19 - C36 Aliphatics
400
410
1 103 0.11 40-140
25 08/30/2019 0650
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) 86 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP EPH (aromatics) - MB
Sample ID: UQ27388-001 Matrix: Aqueous
Batch: 27388 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 08/29/2019 911
Parameter Result Q Dil LOQ DL Units Analysis Date
C11 - C22 Aromatics ND 1 100 100 ug/L 08/30/2019 1336
Acceptance
Surrogate Q % Rec Limit
o - Terphenyl (aromatic) 94 40-140
2-Fluorobiphenyl (fractionation 1) 104 40-140
2-Bromonaphthalene (fractionation 2) 91 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
125 of 198

MADEP EPH (aromatics) - LCS
Sample ID: UQ27388-002
Matrix: Aqueous
Batch: 27388
Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date: 08/29/2019 911
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil % Rec Limit Analysis Date
C11 - C22 Aromatics
850
710
1 83 40-140 08/30/2019 1405
Surrogate
Q % Rec
Acceptance
Limit
o - Terphenyl (aromatic) 92 40-140
2-Fluorobiphenyl (fractionation 1) 105 40-140
2-Bromonaphthalene (fractionation 2) 89 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
` 06 1111W

MADEP EPH (aromatics) - LCSD
Sample ID: UQ27388-003 Matrix: Aqueous
Batch: 27388 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 08/29/2019 911
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
C11 - C22 Aromatics 850 710 1 83 0.089 40-140 25 08/30/2019 1435
Surrogate
o - Terphenyl (aromatic)
2-Fluorobiphenyl (fractionation 1)
2-Bromonaphthalene (fractionation 2)
Acceptance
Q % Rec Limit
89
40-140
102
40-140
88
40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
if��Z.iiSRU

MADEP VPH (aliphatics) - MB
Sample ID: UQ26200-001 Matrix: Aqueous
Batch: 26200 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Parameter Result Q Dil LOQ DL Units Analysis Date
C5 - C8 Aliphatics ND 1 75 15 ug/L 08/16/2019 1859
C9 - C12 Aliphatics ND 1 75 15 ug/L 08/16/2019 1859
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (FID) 101 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP VPH (aliphatics) - LCS
Sample ID: UQ26200-002
Matrix: Aqueous
Batch: 26200
Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount
Result
% Rec
Parameter (ug/L)
(ug/L) Q
Dil % Rec
Limit Analysis Date
C5 - C8 Aliphatics 150
150
1 100
70-130 08/16/2019 1831
C9 - C12 Aliphatics 180
170
1 98
70-130 08/16/2019 1831
Surrogate Q % Rec
Acceptance
Limit
2,5-Dibromotoluene (FID) 106 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

MADEP VPH (aromatics) - MB
Sample ID: UQ26201-001 Matrix: Aqueous
Batch: 26201 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Parameter Result Q Dil LOQ DL Units Analysis Date
C9 - C10 Aromatics ND 1 25 5.0 ug/L 08/16/2019 1859
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (PID) 100 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
130 of 198

MADEP VPH (aromatics) - LCS
Sample ID: UQ26201-002 Matrix: Aqueous
Batch: 26201 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
C9 - C10 Aromatics 25 26 1 106 70-130 08/16/2019 1831
Acceptance
Surrogate Q % Rec Limit
2,5-Dibromotoluene (PID) 108 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15076
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
131 of 198

Volatile Organic Compounds by GC/MS - MB
Sample ID: UQ26199-001 Matrix: Aqueous
Batch: 26199 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
10
4.0
ug/L
08/16/2019 2106
Benzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Bromodichloromethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Bromoform
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Bromomethane (Methyl bromide)
ND
1
0.50
0.40
ug/L
08/16/2019 2106
2-Butanone (MEK)
ND
1
10
2.0
ug/L
08/16/2019 2106
Carbon disulfide
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Carbon tetrachloride
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Chlorobenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Chloroethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Chloroform
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Chloromethane (Methyl chloride)
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Cyclohexane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Dibromochloromethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,2-Dibromoethane (EDB)
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,2-Dichlorobenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,3-Dichlorobenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,4-Dichlorobenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Dichlorodifluoromethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,1-Dichloroethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,2-Dichloroethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,1-Dichloroethene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
cis- 1,2-Dichloroethene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
trans- 1,2-Dichloroethene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,2-Dichloropropane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
cis- 1,3-Dichloropropene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
trans- 1,3-Dichloropropene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Ethylbenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
2-Hexanone
ND
1
10
2.0
ug/L
08/16/2019 2106
Isopropylbenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Methyl acetate
ND
1
1.0
0.40
ug/L
08/16/2019 2106
Methyl tertiary butyl ether (MTBE)
ND
1
0.50
0.40
ug/L
08/16/2019 2106
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
08/16/2019 2106
Methylcyclohexane
ND
1
5.0
0.40
ug/L
08/16/2019 2106
Methylene chloride
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Styrene
ND
1
0.50
0.41
ug/L
08/16/2019 2106
1,1,2,2-Tetrachloroethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Tetrachloroethene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Toluene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,1,2-Trichloro-1,2,2-Trifluoroethane
ND
1
1.0
0.42
ug/L
08/16/2019 2106
1,2,4-Trichlorobenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,1,1-Trichloroethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,1,2-Trichloroethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
132 of 198

Volatile Organic Compounds by GC/MS - MB
Sample ID: UQ26199-001 Matrix: Aqueous
Batch: 26199 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Trichloroethene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Trichlorofluoromethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Vinyl chloride
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Xylenes (total)
ND
1
1.0
0.40
ug/L
08/16/2019 2106
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 101 70-130
1,2-Dichloroethane-d4 100 70-130
Toluene-d8 108 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
133 of 198

Volatile Organic Compounds by GC/MS - LCS
Sample ID: UQ26199-002
Matrix:
Aqueous
Batch: 26199
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
90
1
90
60-140
08/16/2019 1938
Benzene
50
48
1
96
70-130
08/16/2019 1938
Bromodichloromethane
50
49
1
99
70-130
08/16/2019 1938
Bromoform
50
43
1
86
70-130
08/16/2019 1938
Bromomethane (Methyl bromide)
50
50
1
99
70-130
08/16/2019 1938
2-Butanone (MEK)
100
96
1
96
70-130
08/16/2019 1938
Carbon disulfide
50
46
1
91
70-130
08/16/2019 1938
Carbon tetrachloride
50
53
1
106
70-130
08/16/2019 1938
Chlorobenzene
50
48
1
97
70-130
08/16/2019 1938
Chloroethane
50
47
1
93
70-130
08/16/2019 1938
Chloroform
50
46
1
92
70-130
08/16/2019 1938
Chloromethane (Methyl chloride)
50
47
1
94
60-140
08/16/2019 1938
Cyclohexane
50
48
1
97
70-130
08/16/2019 1938
1,2-Dibromo-3-chloropropane (DBCP)
50
48
1
96
70-130
08/16/2019 1938
Dibromochloromethane
50
51
1
101
70-130
08/16/2019 1938
1,2-Dibromoethane (EDB)
50
50
1
101
70-130
08/16/2019 1938
1,2-Dichlorobenzene
50
49
1
99
70-130
08/16/2019 1938
1,3-Dichlorobenzene
50
50
1
99
70-130
08/16/2019 1938
1,4-Dichlorobenzene
50
48
1
96
70-130
08/16/2019 1938
Dichlorodifluoromethane
50
52
1
103
60-140
08/16/2019 1938
1,1-Dichloroethane
50
46
1
91
70-130
08/16/2019 1938
1,2-Dichloroethane
50
48
1
95
70-130
08/16/2019 1938
1,1-Dichloroethene
50
48
1
96
70-130
08/16/2019 1938
cis- 1,2-Dichloroethene
50
47
1
93
70-130
08/16/2019 1938
trans- 1,2-Dichloroethene
50
48
1
96
70-130
08/16/2019 1938
1,2-Dichloropropane
50
46
1
93
70-130
08/16/2019 1938
cis- 1,3-Dichloropropene
50
50
1
100
70-130
08/16/2019 1938
trans- 1,3-Dichloropropene
50
51
1
101
70-130
08/16/2019 1938
Ethylbenzene
50
50
1
100
70-130
08/16/2019 1938
2-Hexanone
100
100
1
103
70-130
08/16/2019 1938
Isopropylbenzene
50
51
1
102
70-130
08/16/2019 1938
Methyl acetate
50
50
1
100
70-130
08/16/2019 1938
Methyl tertiary butyl ether (MTBE)
50
45
1
90
70-130
08/16/2019 1938
4-Methyl-2-pentanone
100
99
1
99
70-130
08/16/2019 1938
Methylcyclohexane
50
51
1
103
70-130
08/16/2019 1938
Methylene chloride
50
44
1
89
70-130
08/16/2019 1938
Styrene
50
52
1
104
70-130
08/16/2019 1938
1,1,2,2-Tetrachloroethane
50
50
1
100
70-130
08/16/2019 1938
Tetrachloroethene
50
51
1
103
70-130
08/16/2019 1938
Toluene
50
49
1
98
70-130
08/16/2019 1938
1,1,2-Trichloro-1,2,2-Trifluoroethane
50
52
1
103
70-130
08/16/2019 1938
1,2,4-Trichlorobenzene
50
51
1
103
70-130
08/16/2019 1938
1,1,1-Trichloroethane
50
49
1
98
70-130
08/16/2019 1938
1,1,2-Trichloroethane
50
49
1
98
70-130
08/16/2019 1938
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
134 of 198

Volatile Organic Compounds by GC/MS - LCS
Sample ID: UQ26199-002
Matrix:
Aqueous
Batch: 26199
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
Trichloroethene
50
51
1
101
70-130
08/16/2019 1938
Trichlorofluoromethane
50
50
1
101
70-130
08/16/2019 1938
Vinyl chloride
50
48
1
95
70-130
08/16/2019 1938
Xylenes (total)
100
99
1
99
70-130
08/16/2019 1938
Acceptance
Surrogate
Q % Rec
Limit
Bromofluorobenzene 90 70-130
1,2-Dichloroethane-d4 93 70-130
Toluene-d8 96 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
135 of 198

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: UQ26336-001 Matrix: Aqueous
Batch: 26336 Prep Method: 3520C
Analytical Method: 8270E Prep Date: 08/19/2019 1653
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acenaphthene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Acenaphthylene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Acetophenone
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Anthracene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Atrazine
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Benzaldehyde
ND
1
8.0
0.50
ug/L
08/22/2019 1642
Benzo(a)anthracene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Benzo(a)pyrene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Benzo(k)fluoranthene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Benzo(g,h,i)perylene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Benzo(k)fluoranthene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
1,1'-Biphenyl
ND
1
4.0
0.50
ug/L
08/22/2019 1642
4-Bromophenyl phenyl ether
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Butyl benzyl phthalate
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Caprolactam
4.5 J
1
8.0
1.0
ug/L
08/22/2019 1642
Carbazole
ND
1
4.0
0.50
ug/L
08/22/2019 1642
bis (2-Chloro-1-methylethyl) ether
ND
1
4.0
0.50
ug/L
08/22/2019 1642
4-Chloro-3-methyl phenol
ND
1
4.0
0.50
ug/L
08/22/2019 1642
4-Chloroaniline
ND
1
8.0
0.50
ug/L
08/22/2019 1642
bis(2-Chloroethoxy)methane
ND
1
4.0
0.50
ug/L
08/22/2019 1642
bis(2-Chloroethyl)ether
ND
1
4.0
0.50
ug/L
08/22/2019 1642
2-Chloronaphthalene
ND
1
4.0
0.50
ug/L
08/22/2019 1642
2-Chlorophenol
ND
1
4.0
0.50
ug/L
08/22/2019 1642
4-Chlorophenyl phenyl ether
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Chrysene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Dibenzo(a,h)anthracene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Dibenzofuran
ND
1
4.0
0.50
ug/L
08/22/2019 1642
3,3'-Dichlorobenzidine
ND
1
4.0
1.8
ug/L
08/22/2019 1642
2,4-Dichlorophenol
ND
1
8.0
1.0
ug/L
08/22/2019 1642
Diethylphthalate
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Dimethyl phthalate
ND
1
4.0
0.50
ug/L
08/22/2019 1642
2,4-Dimethylphenol
ND
1
4.0
1.0
ug/L
08/22/2019 1642
Di-n-butyl phthalate
ND
1
4.0
0.50
ug/L
08/22/2019 1642
4,6-Dinitro-2-methyl phenol
ND
1
20
1.0
ug/L
08/22/2019 1642
2,4-Dinitrophenol
ND
1
20
1.0
ug/L
08/22/2019 1642
2,4-Dinitrotoluene
ND
1
8.0
0.50
ug/L
08/22/2019 1642
2,6-Dinitrotoluene
ND
1
8.0
0.50
ug/L
08/22/2019 1642
Di-n-octylphthalate
ND
1
4.0
0.50
ug/L
08/22/2019 1642
bis(2-Ethylhexyl)phthalate
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Fluoranthene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Fluorene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Hexachlorobenzene
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Hexachlorobutadiene
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Hexachlorocyclopentadiene
ND
1
20
2.0
ug/L
08/22/2019 1642
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
136 of 198

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: UQ26336-001 Matrix: Aqueous
Batch: 26336 Prep Method: 3520C
Analytical Method: 8270E Prep Date: 08/19/2019 1653
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Hexachloroethane
ND
1
4.0
1.0
ug/L
08/22/20191642
Indeno(1,2,3-c,d)pyrene
ND
1
0.80
0.20
ug/L
08/22/20191642
Isophorone
ND
1
4.0
0.50
ug/L
08/22/20191642
2-Methyl naphthalene
ND
1
0.80
0.20
ug/L
08/22/20191642
2-Methylphenol
ND
1
4.0
1.0
ug/L
08/22/20191642
3+4-Methylphenol
ND
1
4.0
1.5
ug/L
08/22/20191642
Naphthalene
ND
1
0.80
0.20
ug/L
08/22/20191642
2-Nitroaniline
ND
1
8.0
0.50
ug/L
08/22/20191642
3-Nitroaniline
ND
1
8.0
1.0
ug/L
08/22/20191642
4-Nitroaniline
ND
1
8.0
1.5
ug/L
08/22/20191642
Nitrobenzene
ND
1
4.0
1.5
ug/L
08/22/20191642
2-Nitrophenol
ND
1
4.0
1.0
ug/L
08/22/20191642
4-Nitrophenol
ND
1
20
2.0
ug/L
08/22/20191642
N-Nitrosodi-n-propylamine
ND
1
4.0
0.50
ug/L
08/22/20191642
N-Nitrosodiphenylamine (Diphenylamine)
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Pentachlorophenol
ND
1
20
2.0
ug/L
08/22/20191642
Phenanthrene
ND
1
0.80
0.20
ug/L
08/22/20191642
Phenol
ND
1
4.0
0.50
ug/L
08/22/20191642
Pyrene
ND
1
0.80
0.20
ug/L
08/22/20191642
2,4,5-Trichlorophenol
ND
1
4.0
0.50
ug/L
08/22/20191642
2,4,6-Trichlorophenol
ND
1
4.0
0.50
ug/L
08/22/20191642
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 48 37-129
2-Fluorophenol 30 24-127
Nitrobenzene-d5
55
38-127
Phenol-d5
38
28-128
Terphenyl-d 14
71
10-148
2,4,6-Tribromophenol
50
35-144
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
137 of 198

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: UQ26336-002
Matrix:
Aqueous
Batch: 26336
Prep Method:
3520C
Analytical Method: 8270E
Prep Date:
08/19/2019 1653
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acenaphthene
40
24
1
59
30-122
08/22/2019 1706
Acenaphthylene
40
25
1
61
30-130
08/22/2019 1706
Acetophenone
40
33
1
83
30-130
08/22/2019 1706
Anthracene
40
23
1
57
30-123
08/22/2019 1706
Atrazine
40
25
1
62
30-130
08/22/2019 1706
Benzaldehyde
40
18
1
46
20-115
08/22/2019 1706
Benzo(a)anthracene
40
25
1
63
40-125
08/22/2019 1706
Benzo(a)pyrene
40
22
1
56
40-128
08/22/2019 1706
Benzo(k)fluoranthene
40
24
1
60
30-130
08/22/2019 1706
Benzo(g,h,i)perylene
40
31
1
77
30-130
08/22/2019 1706
Benzo(k)fluoranthene
40
24
1
60
30-130
08/22/2019 1706
1,1'-Biphenyl
40
24
1
59
30-130
08/22/2019 1706
4-Bromophenyl phenyl ether
40
22
1
55
30-124
08/22/2019 1706
Butyl benzyl phthalate
40
32
1
81
30-130
08/22/2019 1706
Caprolactam
40
32
1
80
30-130
08/22/2019 1706
Carbazole
40
23
1
58
30-130
08/22/2019 1706
bis (2-Chloro-1-methylethyl) ether
40
41
1
102
30-130
08/22/2019 1706
4-Chloro-3-methyl phenol
40
30
1
74
30-123
08/22/2019 1706
4-Chloroaniline
40
22
1
54
12-157
08/22/2019 1706
bis(2-Chloroethoxy)methane
40
27
1
68
30-130
08/22/2019 1706
bis(2-Chloroethyl)ether
40
35
1
87
30-130
08/22/2019 1706
2-Chloronaphthalene
40
24
1
61
30-130
08/22/2019 1706
2-Chlorophenol
40
28
1
71
30-130
08/22/2019 1706
4-Chlorophenyl phenyl ether
40
22
1
55
30-121
08/22/2019 1706
Chrysene
40
24
1
59
30-130
08/22/2019 1706
Dibenzo(a,h)anthracene
40
28
1
69
30-130
08/22/2019 1706
Dibenzofuran
40
23
1
58
30-118
08/22/2019 1706
3,3'-Dichlorobenzidine
40
21
1
52
10-126
08/22/2019 1706
2,4-Dichlorophenol
40
24
1
59
30-121
08/22/2019 1706
Diethylphthalate
40
27
1
69
40-125
08/22/2019 1706
Dimethyl phthalate
40
26
1
64
40-127
08/22/2019 1706
2,4-Dimethylphenol
40
28
1
71
20-125
08/22/2019 1706
Di-n-butyl phthalate
40
26
1
66
40-127
08/22/2019 1706
4,6-Dinitro-2-methyl phenol
40
21
1
53
30-130
08/22/2019 1706
2,4-Dinitrophenol
80
41
1
51
11-126
08/22/2019 1706
2,4-Dinitrotoluene
40
25
1
62
30-130
08/22/2019 1706
2,6-Dinitrotoluene
40
25
1
64
30-130
08/22/2019 1706
Di-n-octylphthalate
40
32
1
79
30-130
08/22/2019 1706
bis(2-Ethylhexyl)phthalate
40
32
1
80
30-130
08/22/2019 1706
Fluoranthene
40
22
1
55
40-128
08/22/2019 1706
Fluorene
40
24
1
59
30-124
08/22/2019 1706
Hexachlorobenzene
40
26
1
64
30-125
08/22/2019 1706
Hexachlorobutadiene
40
23
1
56
24-110
08/22/2019 1706
Hexachlorocyclopentadiene
200
100
1
52
22-122
08/22/2019 1706
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
138 of 198

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: UQ26336-002
Matrix:
Aqueous
Batch: 26336
Prep Method:
3520C
Analytical Method: 8270E
Prep Date:
08/19/2019 1653
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
Hexachloroethane
40
28
1
69
30-130
08/22/20191706
Indeno(1,2,3-c,d)pyrene
40
26
1
66
30-130
08/22/20191706
Isophorone
40
29
1
72
30-130
08/22/20191706
2-Methyl naphthalene
40
25
1
61
40-132
08/22/20191706
2-Methylphenol
40
34
1
86
30-130
08/22/20191706
3+4-Methylphenol
40
34
1
85
30-130
08/22/20191706
Naphthalene
40
25
1
62
30-130
08/22/20191706
2-Nitroaniline
40
28
1
71
30-130
08/22/20191706
3-Nitroaniline
40
21
1
53
30-130
08/22/20191706
4-Nitroaniline
40
28
1
70
30-135
08/22/20191706
Nitrobenzene
40
28
1
69
30-130
08/22/20191706
2-Nitrophenol
40
26
1
65
30-130
08/22/20191706
4-Nitrophenol
80
51
1
63
30-130
08/22/20191706
N-Nitrosodi-n-propylamine
40
33
1
83
30-130
08/22/20191706
N-Nitrosodiphenylamine (Diphenylamine)
40
22
1
56
30-123
08/22/2019 1706
Pentachlorophenol
80
41
1
51
30-130
08/22/20191706
Phenanthrene
40
23
1
59
40-123
08/22/20191706
Phenol
40
29
1
73
30-130
08/22/20191706
Pyrene
40
25
1
62
40-126
08/22/20191706
2,4,5-Trichlorophenol
40
22
1
55
30-123
08/22/20191706
2,4,6-Trichlorophenol
40
24
1
60
30-130
08/22/20191706
Acceptance
Surrogate
Q % Rec
Limit
2-Fluorobiphenyl
57
37-129
2-Fluorophenol
69
24-127
Nitrobenzene-d5
70
38-127
Phenol-d5
75
28-128
Terphenyl-d 14
69
10-148
2,4,6-Tribromophenol
64
35-144
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
139 of 198

MADEP EPH (aromatics) - MB
Sample ID: UQ27084-001 Matrix: Aqueous
Batch: 27084 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 08/26/2019 2111
Parameter Result Q Dil LOQ DL Units Analysis Date
C11 - C22 Aromatics ND 1 100 100 ug/L 08/27/2019 2227
Acceptance
Surrogate Q % Rec Limit
o - Terphenyl (aromatic) 85 40-140
2-Fluorobiphenyl (fractionation 1) 123 40-140
2-Bromonaphthalene (fractionation 2) 111 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
140 of 198

MADEP EPH (aromatics) - LCS
Sample ID: UQ27084-002
Matrix:
Aqueous
Batch: 27084
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/26/2019 2111
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec Limit Analysis Date
C11 - C22 Aromatics
850
740
1
87 40-140 08/27/2019 2257
Surrogate
Q % Rec
Acceptance
Limit
o - Terphenyl (aromatic) 92 40-140
2-Fluorobiphenyl (fractionation 1) 130 40-140
2-Bromonaphthalene (fractionation 2) 113 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
141 of 198

MADEP EPH (aromatics) - LCSD
Sample ID: UQ27084-003
Matrix:
Aqueous
Batch: 27084
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/26/2019 2111
Spike
Amount
Result
% Rec % RPD
Parameter
(ug/L)
(ug/L) Q Dil % Rec
% RPD Limit Limit Analysis Date
C11 - C22 Aromatics
850
740 1 87
0.89 40-140 25 08/27/2019 2326
Surrogate
o - Terphenyl (aromatic)
2-Fluorobiphenyl (fractionation 1)
2-Bromonaphthalene (fractionation 2)
Acceptance
Q % Rec Limit
92
40-140
129
40-140
112
40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
142 of 198

MADEP EPH (aliphatics) - MB
Sample ID: UQ27085-001 Matrix: Aqueous
Batch: 27085 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 08/26/2019 2111
Parameter Result Q Dil LOQ DL Units Analysis Date
C9 - C18 Aliphatics 100 1 100 100 ug/L 08/27/2019 1859
C19 - C36 Aliphatics ND 1 100 100 ug/L 08/27/2019 1859
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) 81 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
143 of 198

MADEP EPH (aliphatics) - LCS
Sample ID: UQ27085-002
Matrix:
Aqueous
Batch: 27085
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/26/2019 2111
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit Analysis Date
C9 - C18 Aliphatics
300
260
1
88
40-140 08/27/2019 1928
C19 - C36 Aliphatics
400
380
1
95
40-140 08/27/2019 1928
Surrogate
Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic) 83 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
144 of 198

MADEP EPH (aliphatics) - LCSD
Sample ID: UQ27085-003
Matrix:
Aqueous
Batch: 27085
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/26/2019 2111
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
% RPD Limit
Limit Analysis Date
C9 - C18 Aliphatics
300
300
1 99
12 40-140
25 08/27/2019 1958
C19 - C36 Aliphatics
400
400
1 100
5.0 40-140
25 08/27/2019 1958
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) 83 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
145 of 198

MADEP EPH (aliphatics) - MB
Sample ID: UQ27385-001 Matrix: Aqueous
Batch: 27385 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 08/29/2019 911
Parameter Result Q Dil LOQ DL Units Analysis Date
C9 - C18 Aliphatics ND 1 100 100 ug/L 08/30/2019 0552
C19 - C36 Aliphatics ND 1 100 100 ug/L 08/30/2019 0552
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) 83 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
146 of 198

MADEP EPH (aliphatics) - LCS
Sample ID: UQ27385-002
Matrix:
Aqueous
Batch: 27385
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/29/2019 911
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit Analysis Date
C9 - C18 Aliphatics
300
170
1
57
40-140 08/30/2019 0621
C19 - C36 Aliphatics
400
410
1
102
40-140 08/30/2019 0621
Surrogate
Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic) 87 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
147 of 198

MADEP EPH (aliphatics) - LCSD
Sample ID: UQ27385-003
Matrix:
Aqueous
Batch: 27385
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/29/2019 911
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
% RPD Limit
Limit Analysis Date
C9 - C18 Aliphatics
300
180
1 60
6.1 40-140
25 08/30/2019 0650
C19 - C36 Aliphatics
400
410
1 103
0.11 40-140
25 08/30/2019 0650
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) 86 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
148 of 198

MADEP EPH (aromatics) - MB
Sample ID: UQ27388-001 Matrix: Aqueous
Batch: 27388 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 08/29/2019 911
Parameter Result Q Dil LOQ DL Units Analysis Date
C11 - C22 Aromatics ND 1 100 100 ug/L 08/30/2019 1336
Acceptance
Surrogate Q % Rec Limit
o - Terphenyl (aromatic) 94 40-140
2-Fluorobiphenyl (fractionation 1) 104 40-140
2-Bromonaphthalene (fractionation 2) 91 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
149 of 198

MADEP EPH (aromatics) - LCS
Sample ID: UQ27388-002
Matrix:
Aqueous
Batch: 27388
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/29/2019 911
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec Limit Analysis Date
C11 - C22 Aromatics
850
710
1
83 40-140 08/30/2019 1405
Surrogate
Q % Rec
Acceptance
Limit
o - Terphenyl (aromatic) 92 40-140
2-Fluorobiphenyl (fractionation 1) 105 40-140
2-Bromonaphthalene (fractionation 2) 89 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
150 of 198

MADEP EPH (aromatics) - LCSD
Sample ID: UQ27388-003
Matrix:
Aqueous
Batch: 27388
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/29/2019 911
Spike
Amount
Result
% Rec % RPD
Parameter
(ug/L)
(ug/L) Q Dil % Rec
% RPD Limit Limit Analysis Date
C11 - C22 Aromatics
850
710 1 83
0.089 40-140 25 08/30/2019 1435
Surrogate
o - Terphenyl (aromatic)
2-Fluorobiphenyl (fractionation 1)
2-Bromonaphthalene (fractionation 2)
Acceptance
Q % Rec Limit
89
40-140
102
40-140
88
40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
151 of 198

MADEP VPH (aliphatics) - MB
Sample ID: UQ26200-001 Matrix: Aqueous
Batch: 26200 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Parameter Result Q Dil LOQ DL Units Analysis Date
C5 - C8 Aliphatics ND 1 75 15 ug/L 08/16/2019 1859
C9 - C12 Aliphatics ND 1 75 15 ug/L 08/16/2019 1859
Acceptance
Surrogate Q % Rec Limit
25-Dibromotoluene (FID) 101 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
152 of 198

MADEP VPH (aliphatics) - LCS
Sample ID: UQ26200-002
Matrix:
Aqueous
Batch: 26200
Prep Method:
VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit Analysis Date
C5 - C8 Aliphatics
150
150
1
100
70-130 08/16/2019 1831
C9 - C12 Aliphatics
180
170
1
98
70-130 08/16/2019 1831
Surrogate
Q % Rec
Acceptance
Limit
25-Dibromotoluene (FID) 106 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
153 of 198

MADEP VPH (aromatics) - MB
Sample ID: UQ26201-001 Matrix: Aqueous
Batch: 26201 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Parameter Result Q Dil LOQ DL Units Analysis Date
C9 - C10 Aromatics ND 1 25 5.0 ug/L 08/16/2019 1859
Acceptance
Surrogate Q % Rec Limit
25-Dibromotoluene (PID) 100 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
154 of 198

MADEP VPH (aromatics) - LCS
Sample ID: UQ26201-002 Matrix: Aqueous
Batch: 26201 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
C9 - C10 Aromatics 25 26 1 106 70-130 08/16/2019 1831
Acceptance
Surrogate Q % Rec Limit
25-Dibromotoluene (PID) 108 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
155 of 198

MADEP VPH (aromatics) - MB
Sample ID: UQ26244-001 Matrix: Aqueous
Batch: 26244 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Parameter Result Q Dil LOQ DL Units Analysis Date
C9 - C10 Aromatics ND 1 25 5.0 ug/L 08/17/2019 1931
Acceptance
Surrogate Q % Rec Limit
25-Dibromotoluene (PID) 107 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
156 of 198

MADEP VPH (aromatics) - LCS
Sample ID: UQ26244-002 Matrix: Aqueous
Batch: 26244 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
C9 - C10 Aromatics 25 25 1 102 70-130 08/17/2019 1833
Acceptance
Surrogate Q % Rec Limit
25-Dibromotoluene (PID) 103 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
157 of 198

MADEP VPH (aromatics) - LCSD
Sample ID: UQ26244-003 Matrix: Aqueous
Batch: 26244 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
C9 - C10 Aromatics 25 27 1 108 5.7 70-130 25 08/17/2019 1902
Acceptance
Surrogate Q % Rec Limit
25-Dibromotoluene (PID) 104 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
158 of 198

MADEP VPH (aliphatics) - MB
Sample ID: UQ26245-001 Matrix: Aqueous
Batch: 26245 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Parameter Result Q Dil LOQ DL Units Analysis Date
C5 - C8 Aliphatics ND 1 75 15 ug/L 08/17/2019 1931
C9 - C12 Aliphatics ND 1 75 15 ug/L 08/17/2019 1931
Acceptance
Surrogate Q % Rec Limit
25-Dibromotoluene (FID) 105 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
159 of 198

MADEP VPH (aliphatics) - LCS
Sample ID: UQ26245-002
Matrix:
Aqueous
Batch: 26245
Prep Method:
VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit Analysis Date
C5 - C8 Aliphatics
150
160
1
109
70-130 08/17/2019 1833
C9 - C12 Aliphatics
180
180
1
100
70-130 08/17/2019 1833
Surrogate
Q % Rec
Acceptance
Limit
25-Dibromotoluene (FID) 99 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
160 of 198

MADEP VPH (aliphatics) - LCSD
Sample ID: UQ26245-003
Matrix: Aqueous
Batch: 26245
Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil % Rec % RPD
Limit
Limit Analysis Date
C5 - C8 Aliphatics
150
170
1 115 5.4
70-130
25 08/17/2019 1902
C9 - C12 Aliphatics
180
180
1 105 4.7
70-130
25 08/17/2019 1902
Acceptance
Surrogate Q % Rec Limit
25-Dibromotoluene (FID) 102 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15078
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
161 of 198

Volatile Organic Compounds by GC/MS - MB
Sample ID: UQ26199-001 Matrix: Aqueous
Batch: 26199 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acetone
ND
1
10
4.0
ug/L
08/16/2019 2106
Benzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Bromodichloromethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Bromoform
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Bromomethane (Methyl bromide)
ND
1
0.50
0.40
ug/L
08/16/2019 2106
2-Butanone (MEK)
ND
1
10
2.0
ug/L
08/16/2019 2106
Carbon disulfide
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Carbon tetrachloride
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Chlorobenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Chloroethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Chloroform
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Chloromethane (Methyl chloride)
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Cyclohexane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,2-Dibromo-3-chloropropane (DBCP)
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Dibromochloromethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,2-Dibromoethane (EDB)
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,2-Dichlorobenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,3-Dichlorobenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,4-Dichlorobenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Dichlorodifluoromethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,1-Dichloroethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,2-Dichloroethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,1-Dichloroethene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
cis- 1,2-Dichloroethene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
trans- 1,2-Dichloroethene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,2-Dichloropropane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
cis- 1,3-Dichloropropene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
trans- 1,3-Dichloropropene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Ethylbenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
2-Hexanone
ND
1
10
2.0
ug/L
08/16/2019 2106
Isopropylbenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Methyl acetate
ND
1
1.0
0.40
ug/L
08/16/2019 2106
Methyl tertiary butyl ether (MTBE)
ND
1
0.50
0.40
ug/L
08/16/2019 2106
4-Methyl-2-pentanone
ND
1
10
2.0
ug/L
08/16/2019 2106
Methylcyclohexane
ND
1
5.0
0.40
ug/L
08/16/2019 2106
Methylene chloride
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Styrene
ND
1
0.50
0.41
ug/L
08/16/2019 2106
1,1,2,2-Tetrachloroethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Tetrachloroethene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Toluene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,1,2-Trichloro-1,2,2-Trifluoroethane
ND
1
1.0
0.42
ug/L
08/16/2019 2106
1,2,4-Trichlorobenzene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,1,1-Trichloroethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
1,1,2-Trichloroethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
162 of 198

Volatile Organic Compounds by GC/MS - MB
Sample ID: UQ26199-001 Matrix: Aqueous
Batch: 26199 Prep Method: 5030E
Analytical Method: 8260D
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Trichloroethene
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Trichlorofluoromethane
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Vinyl chloride
ND
1
0.50
0.40
ug/L
08/16/2019 2106
Xylenes (total)
ND
1
1.0
0.40
ug/L
08/16/2019 2106
Acceptance
Surrogate Q % Rec Limit
Bromofluorobenzene 101 70-130
1,2-Dichloroethane-d4 100 70-130
Toluene-d8 108 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
163 of 198

Volatile Organic Compounds by GC/MS - LCS
Sample ID: UQ26199-002
Matrix:
Aqueous
Batch: 26199
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acetone
100
90
1
90
60-140
08/16/2019 1938
Benzene
50
48
1
96
70-130
08/16/2019 1938
Bromodichloromethane
50
49
1
99
70-130
08/16/2019 1938
Bromoform
50
43
1
86
70-130
08/16/2019 1938
Bromomethane (Methyl bromide)
50
50
1
99
70-130
08/16/2019 1938
2-Butanone (MEK)
100
96
1
96
70-130
08/16/2019 1938
Carbon disulfide
50
46
1
91
70-130
08/16/2019 1938
Carbon tetrachloride
50
53
1
106
70-130
08/16/2019 1938
Chlorobenzene
50
48
1
97
70-130
08/16/2019 1938
Chloroethane
50
47
1
93
70-130
08/16/2019 1938
Chloroform
50
46
1
92
70-130
08/16/2019 1938
Chloromethane (Methyl chloride)
50
47
1
94
60-140
08/16/2019 1938
Cyclohexane
50
48
1
97
70-130
08/16/2019 1938
1,2-Dibromo-3-chloropropane (DBCP)
50
48
1
96
70-130
08/16/2019 1938
Dibromochloromethane
50
51
1
101
70-130
08/16/2019 1938
1,2-Dibromoethane (EDB)
50
50
1
101
70-130
08/16/2019 1938
1,2-Dichlorobenzene
50
49
1
99
70-130
08/16/2019 1938
1,3-Dichlorobenzene
50
50
1
99
70-130
08/16/2019 1938
1,4-Dichlorobenzene
50
48
1
96
70-130
08/16/2019 1938
Dichlorodifluoromethane
50
52
1
103
60-140
08/16/2019 1938
1,1-Dichloroethane
50
46
1
91
70-130
08/16/2019 1938
1,2-Dichloroethane
50
48
1
95
70-130
08/16/2019 1938
1,1-Dichloroethene
50
48
1
96
70-130
08/16/2019 1938
cis- 1,2-Dichloroethene
50
47
1
93
70-130
08/16/2019 1938
trans- 1,2-Dichloroethene
50
48
1
96
70-130
08/16/2019 1938
1,2-Dichloropropane
50
46
1
93
70-130
08/16/2019 1938
cis- 1,3-Dichloropropene
50
50
1
100
70-130
08/16/2019 1938
trans- 1,3-Dichloropropene
50
51
1
101
70-130
08/16/2019 1938
Ethylbenzene
50
50
1
100
70-130
08/16/2019 1938
2-Hexanone
100
100
1
103
70-130
08/16/2019 1938
Isopropylbenzene
50
51
1
102
70-130
08/16/2019 1938
Methyl acetate
50
50
1
100
70-130
08/16/2019 1938
Methyl tertiary butyl ether (MTBE)
50
45
1
90
70-130
08/16/2019 1938
4-Methyl-2-pentanone
100
99
1
99
70-130
08/16/2019 1938
Methylcyclohexane
50
51
1
103
70-130
08/16/2019 1938
Methylene chloride
50
44
1
89
70-130
08/16/2019 1938
Styrene
50
52
1
104
70-130
08/16/2019 1938
1,1,2,2-Tetrachloroethane
50
50
1
100
70-130
08/16/2019 1938
Tetrachloroethene
50
51
1
103
70-130
08/16/2019 1938
Toluene
50
49
1
98
70-130
08/16/2019 1938
1,1,2-Trichloro-1,2,2-Trifluoroethane
50
52
1
103
70-130
08/16/2019 1938
1,2,4-Trichlorobenzene
50
51
1
103
70-130
08/16/2019 1938
1,1,1-Trichloroethane
50
49
1
98
70-130
08/16/2019 1938
1,1,2-Trichloroethane
50
49
1
98
70-130
08/16/2019 1938
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
164 of 198

Volatile Organic Compounds by GC/MS - LCS
Sample ID: UQ26199-002
Matrix:
Aqueous
Batch: 26199
Prep Method:
5030E
Analytical Method: 8260D
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
Trichloroethene
50
51
1
101
70-130
08/16/2019 1938
Trichlorofluoromethane
50
50
1
101
70-130
08/16/2019 1938
Vinyl chloride
50
48
1
95
70-130
08/16/2019 1938
Xylenes (total)
100
99
1
99
70-130
08/16/2019 1938
Acceptance
Surrogate
Q % Rec
Limit
Bromofluorobenzene 90 70-130
1,2-Dichloroethane-d4 93 70-130
Toluene-d8 96 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
165 of 198

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: UQ26336-001 Matrix: Aqueous
Batch: 26336 Prep Method: 3520C
Analytical Method: 8270E Prep Date: 08/19/2019 1653
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acenaphthene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Acenaphthylene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Acetophenone
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Anthracene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Atrazine
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Benzaldehyde
ND
1
8.0
0.50
ug/L
08/22/2019 1642
Benzo(a)anthracene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Benzo(a)pyrene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Benzo(k)fluoranthene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Benzo(g,h,i)perylene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Benzo(k)fluoranthene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
1,1'-Biphenyl
ND
1
4.0
0.50
ug/L
08/22/2019 1642
4-Bromophenyl phenyl ether
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Butyl benzyl phthalate
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Caprolactam
4.5 J
1
8.0
1.0
ug/L
08/22/2019 1642
Carbazole
ND
1
4.0
0.50
ug/L
08/22/2019 1642
bis (2-Chloro-1-methylethyl) ether
ND
1
4.0
0.50
ug/L
08/22/2019 1642
4-Chloro-3-methyl phenol
ND
1
4.0
0.50
ug/L
08/22/2019 1642
4-Chloroaniline
ND
1
8.0
0.50
ug/L
08/22/2019 1642
bis(2-Chloroethoxy)methane
ND
1
4.0
0.50
ug/L
08/22/2019 1642
bis(2-Chloroethyl)ether
ND
1
4.0
0.50
ug/L
08/22/2019 1642
2-Chloronaphthalene
ND
1
4.0
0.50
ug/L
08/22/2019 1642
2-Chlorophenol
ND
1
4.0
0.50
ug/L
08/22/2019 1642
4-Chlorophenyl phenyl ether
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Chrysene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Dibenzo(a,h)anthracene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Dibenzofuran
ND
1
4.0
0.50
ug/L
08/22/2019 1642
3,3'-Dichlorobenzidine
ND
1
4.0
1.8
ug/L
08/22/2019 1642
2,4-Dichlorophenol
ND
1
8.0
1.0
ug/L
08/22/2019 1642
Diethylphthalate
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Dimethyl phthalate
ND
1
4.0
0.50
ug/L
08/22/2019 1642
2,4-Dimethylphenol
ND
1
4.0
1.0
ug/L
08/22/2019 1642
Di-n-butyl phthalate
ND
1
4.0
0.50
ug/L
08/22/2019 1642
4,6-Dinitro-2-methyl phenol
ND
1
20
1.0
ug/L
08/22/2019 1642
2,4-Dinitrophenol
ND
1
20
1.0
ug/L
08/22/2019 1642
2,4-Dinitrotoluene
ND
1
8.0
0.50
ug/L
08/22/2019 1642
2,6-Dinitrotoluene
ND
1
8.0
0.50
ug/L
08/22/2019 1642
Di-n-octylphthalate
ND
1
4.0
0.50
ug/L
08/22/2019 1642
bis(2-Ethylhexyl)phthalate
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Fluoranthene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Fluorene
ND
1
0.80
0.20
ug/L
08/22/2019 1642
Hexachlorobenzene
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Hexachlorobutadiene
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Hexachlorocyclopentadiene
ND
1
20
2.0
ug/L
08/22/2019 1642
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
166 of 198

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: UQ26336-001 Matrix: Aqueous
Batch: 26336 Prep Method: 3520C
Analytical Method: 8270E Prep Date: 08/19/2019 1653
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Hexachloroethane
ND
1
4.0
1.0
ug/L
08/22/20191642
Indeno(1,2,3-c,d)pyrene
ND
1
0.80
0.20
ug/L
08/22/20191642
Isophorone
ND
1
4.0
0.50
ug/L
08/22/20191642
2-Methyl naphthalene
ND
1
0.80
0.20
ug/L
08/22/20191642
2-Methylphenol
ND
1
4.0
1.0
ug/L
08/22/20191642
3+4-Methylphenol
ND
1
4.0
1.5
ug/L
08/22/20191642
Naphthalene
ND
1
0.80
0.20
ug/L
08/22/20191642
2-Nitroaniline
ND
1
8.0
0.50
ug/L
08/22/20191642
3-Nitroaniline
ND
1
8.0
1.0
ug/L
08/22/20191642
4-Nitroaniline
ND
1
8.0
1.5
ug/L
08/22/20191642
Nitrobenzene
ND
1
4.0
1.5
ug/L
08/22/20191642
2-Nitrophenol
ND
1
4.0
1.0
ug/L
08/22/20191642
4-Nitrophenol
ND
1
20
2.0
ug/L
08/22/20191642
N-Nitrosodi-n-propylamine
ND
1
4.0
0.50
ug/L
08/22/20191642
N-Nitrosodiphenylamine (Diphenylamine)
ND
1
4.0
0.50
ug/L
08/22/2019 1642
Pentachlorophenol
ND
1
20
2.0
ug/L
08/22/20191642
Phenanthrene
ND
1
0.80
0.20
ug/L
08/22/20191642
Phenol
ND
1
4.0
0.50
ug/L
08/22/20191642
Pyrene
ND
1
0.80
0.20
ug/L
08/22/20191642
2,4,5-Trichlorophenol
ND
1
4.0
0.50
ug/L
08/22/20191642
2,4,6-Trichlorophenol
ND
1
4.0
0.50
ug/L
08/22/20191642
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl 48 37-129
2-Fluorophenol 30 24-127
Nitrobenzene-d5
55
38-127
Phenol-d5
38
28-128
Terphenyl-d 14
71
10-148
2,4,6-Tribromophenol
50
35-144
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
167 of 198

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: UQ26336-002
Matrix:
Aqueous
Batch: 26336
Prep Method:
3520C
Analytical Method: 8270E
Prep Date:
08/19/2019 1653
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acenaphthene
40
24
1
59
30-122
08/22/2019 1706
Acenaphthylene
40
25
1
61
30-130
08/22/2019 1706
Acetophenone
40
33
1
83
30-130
08/22/2019 1706
Anthracene
40
23
1
57
30-123
08/22/2019 1706
Atrazine
40
25
1
62
30-130
08/22/2019 1706
Benzaldehyde
40
18
1
46
20-115
08/22/2019 1706
Benzo(a)anthracene
40
25
1
63
40-125
08/22/2019 1706
Benzo(a)pyrene
40
22
1
56
40-128
08/22/2019 1706
Benzo(k)fluoranthene
40
24
1
60
30-130
08/22/2019 1706
Benzo(g,h,i)perylene
40
31
1
77
30-130
08/22/2019 1706
Benzo(k)fluoranthene
40
24
1
60
30-130
08/22/2019 1706
1,1'-Biphenyl
40
24
1
59
30-130
08/22/2019 1706
4-Bromophenyl phenyl ether
40
22
1
55
30-124
08/22/2019 1706
Butyl benzyl phthalate
40
32
1
81
30-130
08/22/2019 1706
Caprolactam
40
32
1
80
30-130
08/22/2019 1706
Carbazole
40
23
1
58
30-130
08/22/2019 1706
bis (2-Chloro-1-methylethyl) ether
40
41
1
102
30-130
08/22/2019 1706
4-Chloro-3-methyl phenol
40
30
1
74
30-123
08/22/2019 1706
4-Chloroaniline
40
22
1
54
12-157
08/22/2019 1706
bis(2-Chloroethoxy)methane
40
27
1
68
30-130
08/22/2019 1706
bis(2-Chloroethyl)ether
40
35
1
87
30-130
08/22/2019 1706
2-Chloronaphthalene
40
24
1
61
30-130
08/22/2019 1706
2-Chlorophenol
40
28
1
71
30-130
08/22/2019 1706
4-Chlorophenyl phenyl ether
40
22
1
55
30-121
08/22/2019 1706
Chrysene
40
24
1
59
30-130
08/22/2019 1706
Dibenzo(a,h)anthracene
40
28
1
69
30-130
08/22/2019 1706
Dibenzofuran
40
23
1
58
30-118
08/22/2019 1706
3,3'-Dichlorobenzidine
40
21
1
52
10-126
08/22/2019 1706
2,4-Dichlorophenol
40
24
1
59
30-121
08/22/2019 1706
Diethylphthalate
40
27
1
69
40-125
08/22/2019 1706
Dimethyl phthalate
40
26
1
64
40-127
08/22/2019 1706
2,4-Dimethylphenol
40
28
1
71
20-125
08/22/2019 1706
Di-n-butyl phthalate
40
26
1
66
40-127
08/22/2019 1706
4,6-Dinitro-2-methyl phenol
40
21
1
53
30-130
08/22/2019 1706
2,4-Dinitrophenol
80
41
1
51
11-126
08/22/2019 1706
2,4-Dinitrotoluene
40
25
1
62
30-130
08/22/2019 1706
2,6-Dinitrotoluene
40
25
1
64
30-130
08/22/2019 1706
Di-n-octylphthalate
40
32
1
79
30-130
08/22/2019 1706
bis(2-Ethylhexyl)phthalate
40
32
1
80
30-130
08/22/2019 1706
Fluoranthene
40
22
1
55
40-128
08/22/2019 1706
Fluorene
40
24
1
59
30-124
08/22/2019 1706
Hexachlorobenzene
40
26
1
64
30-125
08/22/2019 1706
Hexachlorobutadiene
40
23
1
56
24-110
08/22/2019 1706
Hexachlorocyclopentadiene
200
100
1
52
22-122
08/22/2019 1706
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
168 of 198

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: UQ26336-002
Matrix:
Aqueous
Batch: 26336
Prep Method:
3520C
Analytical Method: 8270E
Prep Date:
08/19/2019 1653
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
Hexachloroethane
40
28
1
69
30-130
08/22/20191706
Indeno(1,2,3-c,d)pyrene
40
26
1
66
30-130
08/22/20191706
Isophorone
40
29
1
72
30-130
08/22/20191706
2-Methyl naphthalene
40
25
1
61
40-132
08/22/20191706
2-Methylphenol
40
34
1
86
30-130
08/22/20191706
3+4-Methylphenol
40
34
1
85
30-130
08/22/20191706
Naphthalene
40
25
1
62
30-130
08/22/20191706
2-Nitroaniline
40
28
1
71
30-130
08/22/20191706
3-Nitroaniline
40
21
1
53
30-130
08/22/20191706
4-Nitroaniline
40
28
1
70
30-135
08/22/20191706
Nitrobenzene
40
28
1
69
30-130
08/22/20191706
2-Nitrophenol
40
26
1
65
30-130
08/22/20191706
4-Nitrophenol
80
51
1
63
30-130
08/22/20191706
N-Nitrosodi-n-propylamine
40
33
1
83
30-130
08/22/20191706
N-Nitrosodiphenylamine (Diphenylamine)
40
22
1
56
30-123
08/22/2019 1706
Pentachlorophenol
80
41
1
51
30-130
08/22/20191706
Phenanthrene
40
23
1
59
40-123
08/22/20191706
Phenol
40
29
1
73
30-130
08/22/20191706
Pyrene
40
25
1
62
40-126
08/22/20191706
2,4,5-Trichlorophenol
40
22
1
55
30-123
08/22/20191706
2,4,6-Trichlorophenol
40
24
1
60
30-130
08/22/20191706
Acceptance
Surrogate
Q % Rec
Limit
2-Fluorobiphenyl
57
37-129
2-Fluorophenol
69
24-127
Nitrobenzene-d5
70
38-127
Phenol-d5
75
28-128
Terphenyl-d 14
69
10-148
2,4,6-Tribromophenol
64
35-144
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
169 of 198

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: UQ27488-001 Matrix: Aqueous
Batch: 27488 Prep Method: 3520C
Analytical Method: 8270E Prep Date: 08/29/2019 1724
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Acenaphthene
ND
1
0.80
0.20
ug/L
08/31/2019 1210
Acenaphthylene
ND
1
0.80
0.20
ug/L
08/31/2019 1210
Acetophenone
ND
1
4.0
0.50
ug/L
08/31/2019 1210
Anthracene
ND
1
0.80
0.20
ug/L
08/31/2019 1210
Atrazine
ND
1
4.0
0.50
ug/L
08/31/2019 1210
Benzaldehyde
ND
1
8.0
0.50
ug/L
08/31/2019 1210
Benzo(a)anthracene
ND
1
0.80
0.20
ug/L
08/31/2019 1210
Benzo(a)pyrene
ND
1
0.80
0.20
ug/L
08/31/2019 1210
Benzo(k)fluoranthene
ND
1
0.80
0.20
ug/L
08/31/2019 1210
Benzo(g,h,i)perylene
ND
1
0.80
0.20
ug/L
08/31/2019 1210
Benzo(k)fluoranthene
ND
1
0.80
0.20
ug/L
08/31/2019 1210
1,1'-Biphenyl
ND
1
4.0
0.50
ug/L
08/31/2019 1210
4-Bromophenyl phenyl ether
ND
1
4.0
0.50
ug/L
08/31/2019 1210
Butyl benzyl phthalate
ND
1
4.0
0.50
ug/L
08/31/2019 1210
Caprolactam
ND
1
8.0
1.0
ug/L
08/31/2019 1210
Carbazole
ND
1
4.0
0.50
ug/L
08/31/2019 1210
bis (2-Chloro-1-methylethyl) ether
ND
1
4.0
0.50
ug/L
08/31/2019 1210
4-Chloro-3-methyl phenol
ND
1
4.0
0.50
ug/L
08/31/2019 1210
4-Chloroaniline
ND
1
8.0
0.50
ug/L
08/31/2019 1210
bis(2-Chloroethoxy)methane
ND
1
4.0
0.50
ug/L
08/31/2019 1210
bis(2-Chloroethyl)ether
ND
1
4.0
0.50
ug/L
08/31/2019 1210
2-Chloronaphthalene
ND
1
4.0
0.50
ug/L
08/31/2019 1210
2-Chlorophenol
ND
1
4.0
0.50
ug/L
08/31/2019 1210
4-Chlorophenyl phenyl ether
ND
1
4.0
0.50
ug/L
08/31/2019 1210
Chrysene
ND
1
0.80
0.20
ug/L
08/31/2019 1210
Dibenzo(a,h)anthracene
ND
1
0.80
0.20
ug/L
08/31/2019 1210
Dibenzofuran
ND
1
4.0
0.50
ug/L
08/31/2019 1210
3,3'-Dichlorobenzidine
ND
1
4.0
1.8
ug/L
08/31/2019 1210
2,4-Dichlorophenol
ND
1
8.0
1.0
ug/L
08/31/2019 1210
Diethylphthalate
ND
1
4.0
0.50
ug/L
08/31/2019 1210
Dimethyl phthalate
ND
1
4.0
0.50
ug/L
08/31/2019 1210
2,4-Dimethylphenol
ND
1
4.0
1.0
ug/L
08/31/2019 1210
Di-n-butyl phthalate
ND
1
4.0
0.50
ug/L
08/31/2019 1210
4,6-Dinitro-2-methyl phenol
ND
1
20
1.0
ug/L
08/31/2019 1210
2,4-Dinitrophenol
ND
1
20
1.0
ug/L
08/31/2019 1210
2,4-Dinitrotoluene
ND
1
8.0
0.50
ug/L
08/31/2019 1210
2,6-Dinitrotoluene
ND
1
8.0
0.50
ug/L
08/31/2019 1210
Di-n-octylphthalate
ND
1
4.0
0.50
ug/L
08/31/2019 1210
bis(2-Ethylhexyl)phthalate
ND
1
4.0
0.50
ug/L
08/31/2019 1210
Fluoranthene
ND
1
0.80
0.20
ug/L
08/31/2019 1210
Fluorene
ND
1
0.80
0.20
ug/L
08/31/2019 1210
Hexachlorobenzene
ND
1
4.0
0.50
ug/L
08/31/2019 1210
Hexachlorobutadiene
ND
1
4.0
0.50
ug/L
08/31/2019 1210
Hexachlorocyclopentadiene
ND
1
20
2.0
ug/L
08/31/2019 1210
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
170 of 198

Semivolatile Organic Compounds by GC/MS - MB
Sample ID: UQ27488-001 Matrix: Aqueous
Batch: 27488 Prep Method: 3520C
Analytical Method: 8270E Prep Date: 08/29/2019 1724
Parameter
Result Q
Dil
LOQ
DL
Units
Analysis Date
Hexachloroethane
ND
1
4.0
1.0
ug/L
08/31/20191210
Indeno(1,2,3-c,d)pyrene
ND
1
0.80
0.20
ug/L
08/31/20191210
Isophorone
ND
1
4.0
0.50
ug/L
08/31/20191210
2-Methyl naphthalene
ND
1
0.80
0.20
ug/L
08/31/20191210
2-Methylphenol
ND
1
4.0
1.0
ug/L
08/31/20191210
3+4-Methylphenol
ND
1
4.0
1.5
ug/L
08/31/20191210
Naphthalene
ND
1
0.80
0.20
ug/L
08/31/20191210
2-Nitroaniline
ND
1
8.0
0.50
ug/L
08/31/20191210
3-Nitroaniline
ND
1
8.0
1.0
ug/L
08/31/20191210
4-Nitroaniline
ND
1
8.0
1.5
ug/L
08/31/20191210
Nitrobenzene
ND
1
4.0
1.5
ug/L
08/31/20191210
2-Nitrophenol
ND
1
4.0
1.0
ug/L
08/31/20191210
4-Nitrophenol
ND
1
20
2.0
ug/L
08/31/20191210
N-Nitrosodi-n-propylamine
ND
1
4.0
0.50
ug/L
08/31/20191210
N-Nitrosodiphenylamine (Diphenylamine)
ND
1
4.0
0.50
ug/L
08/31/2019 1210
Pentachlorophenol
ND
1
20
2.0
ug/L
08/31/20191210
Phenanthrene
ND
1
0.80
0.20
ug/L
08/31/20191210
Phenol
ND
1
4.0
0.50
ug/L
08/31/20191210
Pyrene
ND
1
0.80
0.20
ug/L
08/31/20191210
2,4,5-Trichlorophenol
ND
1
4.0
0.50
ug/L
08/31/20191210
2,4,6-Trichlorophenol
ND
1
4.0
0.50
ug/L
08/31/20191210
Surrogate Q % Rec Acceptance
Limit
2-Fluorobiphenyl
83
37-129
2-Fluorophenol
52
24-127
Nitrobenzene-d5
68
38-127
Phenol-d5
63
28-128
Terphenyl-d 14
100
10-148
2,4,6-Tribromophenol
66
35-144
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
171 of 198

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: UQ27488-002
Matrix:
Aqueous
Batch: 27488
Prep Method:
3520C
Analytical Method: 8270E
Prep Date:
08/29/2019 1724
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L)
Q Dil
% Rec
Limit
Analysis Date
Acenaphthene
40
31
1
78
30-122
08/31/2019 1235
Acenaphthylene
40
33
1
84
30-130
08/31/2019 1235
Acetophenone
40
32
1
80
30-130
08/31/2019 1235
Anthracene
40
32
1
80
30-123
08/31/2019 1235
Atrazine
40
38
1
94
30-130
08/31/2019 1235
Benzaldehyde
40
20
1
50
20-115
08/31/2019 1235
Benzo(a)anthracene
40
32
1
80
40-125
08/31/2019 1235
Benzo(a)pyrene
40
31
1
78
40-128
08/31/2019 1235
Benzo(k)fluoranthene
40
27
1
68
30-130
08/31/2019 1235
Benzo(g,h,i)perylene
40
56
N 1
141
30-130
08/31/2019 1235
Benzo(k)fluoranthene
40
33
1
82
30-130
08/31/2019 1235
1,1'-Biphenyl
40
32
1
79
30-130
08/31/2019 1235
4-Bromophenyl phenyl ether
40
31
1
78
30-124
08/31/2019 1235
Butyl benzyl phthalate
40
34
1
84
30-130
08/31/2019 1235
Caprolactam
40
39
1
97
30-130
08/31/2019 1235
Carbazole
40
32
1
79
30-130
08/31/2019 1235
bis (2-Chloro-1-methylethyl) ether
40
27
1
67
30-130
08/31/2019 1235
4-Chloro-3-methyl phenol
40
31
1
78
30-123
08/31/2019 1235
4-Chloroaniline
40
40
1
101
12-157
08/31/2019 1235
bis(2-Chloroethoxy)methane
40
30
1
76
30-130
08/31/2019 1235
bis(2-Chloroethyl)ether
40
30
1
76
30-130
08/31/2019 1235
2-Chloronaphthalene
40
32
1
80
30-130
08/31/2019 1235
2-Chlorophenol
40
33
1
82
30-130
08/31/2019 1235
4-Chlorophenyl phenyl ether
40
32
1
80
30-121
08/31/2019 1235
Chrysene
40
33
1
82
30-130
08/31/2019 1235
Dibenzo(a,h)anthracene
40
52
1
130
30-130
08/31/2019 1235
Dibenzofuran
40
32
1
80
30-118
08/31/2019 1235
3,3'-Dichlorobenzidine
40
27
1
67
10-126
08/31/2019 1235
2,4-Dichlorophenol
40
30
1
75
30-121
08/31/2019 1235
Diethylphthalate
40
32
1
81
40-125
08/31/2019 1235
Dimethyl phthalate
40
34
1
86
40-127
08/31/2019 1235
2,4-Dimethylphenol
40
36
1
91
20-125
08/31/2019 1235
Di-n-butyl phthalate
40
33
1
83
40-127
08/31/2019 1235
4,6-Dinitro-2-methyl phenol
40
33
1
82
30-130
08/31/2019 1235
2,4-Dinitrophenol
80
52
1
65
11-126
08/31/2019 1235
2,4-Dinitrotoluene
40
38
1
95
30-130
08/31/2019 1235
2,6-Dinitrotoluene
40
35
1
87
30-130
08/31/2019 1235
Di-n-octylphthalate
40
25
1
63
30-130
08/31/2019 1235
bis(2-Ethylhexyl)phthalate
40
31
1
76
30-130
08/31/2019 1235
Fluoranthene
40
33
1
81
40-128
08/31/2019 1235
Fluorene
40
32
1
79
30-124
08/31/2019 1235
Hexachlorobenzene
40
37
1
93
30-125
08/31/2019 1235
Hexachlorobutadiene
40
29
1
72
24-110
08/31/2019 1235
Hexachlorocyclopentadiene
200
120
1
61
22-122
08/31/2019 1235
LOQ = Limit of Quantitation
DL = Detection Limit
LOD = Limit of Detection
P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
J = Estimated result < LOQ and > DL + = RPD is out of criteria
ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
172 of 198

Semivolatile Organic Compounds by GC/MS - LCS
Sample ID: UQ27488-002
Matrix:
Aqueous
Batch: 27488
Prep Method:
3520C
Analytical Method: 8270E
Prep Date:
08/29/2019 1724
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit
Analysis Date
Hexachloroethane
40
29
1
72
30-130
08/31/20191235
Indeno(1,2,3-c,d)pyrene
40
49
1
122
30-130
08/31/20191235
Isophorone
40
31
1
77
30-130
08/31/20191235
2-Methyl naphthalene
40
31
1
77
40-132
08/31/20191235
2-Methylphenol
40
36
1
91
30-130
08/31/20191235
3+4-Methylphenol
40
32
1
79
30-130
08/31/20191235
Naphthalene
40
32
1
81
30-130
08/31/20191235
2-Nitroaniline
40
34
1
84
30-130
08/31/20191235
3-Nitroaniline
40
29
1
72
30-130
08/31/20191235
4-Nitroaniline
40
40
1
100
30-135
08/31/20191235
Nitrobenzene
40
30
1
75
30-130
08/31/20191235
2-Nitrophenol
40
33
1
82
30-130
08/31/20191235
4-Nitrophenol
80
50
1
63
30-130
08/31/20191235
N-Nitrosodi-n-propylamine
40
31
1
78
30-130
08/31/20191235
N-Nitrosodiphenylamine (Diphenylamine)
40
31
1
79
30-123
08/31/2019 1235
Pentachlorophenol
80
49
1
61
30-130
08/31/20191235
Phenanthrene
40
30
1
76
40-123
08/31/20191235
Phenol
40
30
1
75
30-130
08/31/20191235
Pyrene
40
34
1
86
40-126
08/31/20191235
2,4,5-Trichlorophenol
40
29
1
73
30-123
08/31/20191235
2,4,6-Trichlorophenol
40
31
1
78
30-130
08/31/20191235
Acceptance
Surrogate
Q % Rec
Limit
2-Fluorobiphenyl
79
37-129
2-Fluorophenol
78
24-127
Nitrobenzene-d5
76
38-127
Phenol-d5
78
28-128
Terphenyl-d 14
96
10-148
2,4,6-Tribromophenol
78
35-144
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
173 of 198

MADEP EPH (aromatics) - MB
Sample ID: UQ27084-001 Matrix: Aqueous
Batch: 27084 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 08/26/2019 2111
Parameter Result Q Dil LOQ DL Units Analysis Date
C11 - C22 Aromatics ND 1 100 100 ug/L 08/27/2019 2227
Acceptance
Surrogate Q % Rec Limit
o - Terphenyl (aromatic) 85 40-140
2-Fluorobiphenyl (fractionation 1) 123 40-140
2-Bromonaphthalene (fractionation 2) 111 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
174 of 198

MADEP EPH (aromatics) - LCS
Sample ID: UQ27084-002
Matrix:
Aqueous
Batch: 27084
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/26/2019 2111
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec Limit Analysis Date
C11 - C22 Aromatics
850
740
1
87 40-140 08/27/2019 2257
Surrogate
Q % Rec
Acceptance
Limit
o - Terphenyl (aromatic) 92 40-140
2-Fluorobiphenyl (fractionation 1) 130 40-140
2-Bromonaphthalene (fractionation 2) 113 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
175 of 198

MADEP EPH (aromatics) - LCSD
Sample ID: UQ27084-003
Matrix:
Aqueous
Batch: 27084
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/26/2019 2111
Spike
Amount
Result
% Rec % RPD
Parameter
(ug/L)
(ug/L) Q Dil % Rec
% RPD Limit Limit Analysis Date
C11 - C22 Aromatics
850
740 1 87
0.89 40-140 25 08/27/2019 2326
Surrogate
o - Terphenyl (aromatic)
2-Fluorobiphenyl (fractionation 1)
2-Bromonaphthalene (fractionation 2)
Acceptance
Q % Rec Limit
92
40-140
129
40-140
112
40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
176 of 198

MADEP EPH (aliphatics) - MB
Sample ID: UQ27085-001 Matrix: Aqueous
Batch: 27085 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 08/26/2019 2111
Parameter Result Q Dil LOQ DL Units Analysis Date
C9 - C18 Aliphatics 100 1 100 100 ug/L 08/27/2019 1859
C19 - C36 Aliphatics ND 1 100 100 ug/L 08/27/2019 1859
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) 81 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
177 of 198

MADEP EPH (aliphatics) - LCS
Sample ID: UQ27085-002
Matrix:
Aqueous
Batch: 27085
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/26/2019 2111
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit Analysis Date
C9 - C18 Aliphatics
300
260
1
88
40-140 08/27/2019 1928
C19 - C36 Aliphatics
400
380
1
95
40-140 08/27/2019 1928
Surrogate
Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic) 83 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
178 of 198

MADEP EPH (aliphatics) - LCSD
Sample ID: UQ27085-003
Matrix:
Aqueous
Batch: 27085
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/26/2019 2111
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
% RPD Limit
Limit Analysis Date
C9 - C18 Aliphatics
300
300
1 99
12 40-140
25 08/27/2019 1958
C19 - C36 Aliphatics
400
400
1 100
5.0 40-140
25 08/27/2019 1958
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) 83 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
179 of 198

MADEP EPH (aliphatics) - MB
Sample ID: UQ27385-001 Matrix: Aqueous
Batch: 27385 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 08/29/2019 911
Parameter Result Q Dil LOQ DL Units Analysis Date
C9 - C18 Aliphatics ND 1 100 100 ug/L 08/30/2019 0552
C19 - C36 Aliphatics ND 1 100 100 ug/L 08/30/2019 0552
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) 83 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
180 of 198

MADEP EPH (aliphatics) - LCS
Sample ID: UQ27385-002
Matrix:
Aqueous
Batch: 27385
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/29/2019 911
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit Analysis Date
C9 - C18 Aliphatics
300
170
1
57
40-140 08/30/2019 0621
C19 - C36 Aliphatics
400
410
1
102
40-140 08/30/2019 0621
Surrogate
Q % Rec
Acceptance
Limit
1-Chloro-octadecane (aliphatic) 87 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
181 of 198

MADEP EPH (aliphatics) - LCSD
Sample ID: UQ27385-003
Matrix:
Aqueous
Batch: 27385
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/29/2019 911
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil % Rec
% RPD Limit
Limit Analysis Date
C9 - C18 Aliphatics
300
180
1 60
6.1 40-140
25 08/30/2019 0650
C19 - C36 Aliphatics
400
410
1 103
0.11 40-140
25 08/30/2019 0650
Acceptance
Surrogate Q % Rec Limit
1-Chloro-octadecane (aliphatic) 86 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
182 of 198

MADEP EPH (aromatics) - MB
Sample ID: UQ27388-001 Matrix: Aqueous
Batch: 27388 Prep Method: MADEP-EPH-04
Analytical Method: MADEP-EPH-04 Prep Date: 08/29/2019 911
Parameter Result Q Dil LOQ DL Units Analysis Date
C11 - C22 Aromatics ND 1 100 100 ug/L 08/30/2019 1336
Acceptance
Surrogate Q % Rec Limit
o - Terphenyl (aromatic) 94 40-140
2-Fluorobiphenyl (fractionation 1) 104 40-140
2-Bromonaphthalene (fractionation 2) 91 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
183 of 198

MADEP EPH (aromatics) - LCS
Sample ID: UQ27388-002
Matrix:
Aqueous
Batch: 27388
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/29/2019 911
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec Limit Analysis Date
C11 - C22 Aromatics
850
710
1
83 40-140 08/30/2019 1405
Surrogate
Q % Rec
Acceptance
Limit
o - Terphenyl (aromatic) 92 40-140
2-Fluorobiphenyl (fractionation 1) 105 40-140
2-Bromonaphthalene (fractionation 2) 89 40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
184 of 198

MADEP EPH (aromatics) - LCSD
Sample ID: UQ27388-003
Matrix:
Aqueous
Batch: 27388
Prep Method:
MADEP-EPH-04
Analytical Method: MADEP-EPH-04
Prep Date:
08/29/2019 911
Spike
Amount
Result
% Rec % RPD
Parameter
(ug/L)
(ug/L) Q Dil % Rec
% RPD Limit Limit Analysis Date
C11 - C22 Aromatics
850
710 1 83
0.089 40-140 25 08/30/2019 1435
Surrogate
o - Terphenyl (aromatic)
2-Fluorobiphenyl (fractionation 1)
2-Bromonaphthalene (fractionation 2)
Acceptance
Q % Rec Limit
89
40-140
102
40-140
88
40-140
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
185 of 198

MADEP VPH (aromatics) - MB
Sample ID: UQ26244-001 Matrix: Aqueous
Batch: 26244 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Parameter Result Q Dil LOQ DL Units Analysis Date
C9 - C10 Aromatics ND 1 25 5.0 ug/L 08/17/2019 1931
Acceptance
Surrogate Q % Rec Limit
25-Dibromotoluene (PID) 107 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
186 of 198

MADEP VPH (aromatics) - LCS
Sample ID: UQ26244-002 Matrix: Aqueous
Batch: 26244 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
C9 - C10 Aromatics 25 25 1 102 70-130 08/17/2019 1833
Acceptance
Surrogate Q % Rec Limit
25-Dibromotoluene (PID) 103 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
187 of 198

MADEP VPH (aromatics) - LCSD
Sample ID: UQ26244-003 Matrix: Aqueous
Batch: 26244 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
C9 - C10 Aromatics 25 27 1 108 5.7 70-130 25 08/17/2019 1902
Acceptance
Surrogate Q % Rec Limit
25-Dibromotoluene (PID) 104 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
188 of 198

MADEP VPH (aliphatics) - MB
Sample ID: UQ26245-001 Matrix: Aqueous
Batch: 26245 Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Parameter Result Q Dil LOQ DL Units Analysis Date
C5 - C8 Aliphatics ND 1 75 15 ug/L 08/17/2019 1931
C9 - C12 Aliphatics ND 1 75 15 ug/L 08/17/2019 1931
Acceptance
Surrogate Q % Rec Limit
25-Dibromotoluene (FID) 105 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
189 of 198

MADEP VPH (aliphatics) - LCS
Sample ID: UQ26245-002
Matrix:
Aqueous
Batch: 26245
Prep Method:
VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount
Result
% Rec
Parameter
(ug/L)
(ug/L) Q
Dil
% Rec
Limit Analysis Date
C5 - C8 Aliphatics
150
160
1
109
70-130 08/17/2019 1833
C9 - C12 Aliphatics
180
180
1
100
70-130 08/17/2019 1833
Surrogate
Q % Rec
Acceptance
Limit
25-Dibromotoluene (FID) 99 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
190 of 198

MADEP VPH (aliphatics) - LCSD
Sample ID: UQ26245-003
Matrix: Aqueous
Batch: 26245
Prep Method: VPH
Analytical Method: MADEP-VPH-18-2.1
Spike
Amount
Result
% Rec
% RPD
Parameter
(ug/L)
(ug/L) Q
Dil % Rec % RPD
Limit
Limit Analysis Date
C5 - C8 Aliphatics
150
170
1 115 5.4
70-130
25 08/17/2019 1902
C9 - C12 Aliphatics
180
180
1 105 4.7
70-130
25 08/17/2019 1902
Acceptance
Surrogate Q % Rec Limit
25-Dibromotoluene (FID) 102 70-130
LOQ = Limit of Quantitation P = The RPD between two GC columns exceeds 40 % N = Recovery is out of criteria
DL = Detection Limit J = Estimated result < LOQ and > DL + = RPD is out of criteria
LOD = Limit of Detection ND = Not detected at or above the DL
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: UH15079
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
191 of 198

Chain of Custody
and
Miscellaneous Documents
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
192 of 198

SHEALY ENVIRONMENTAL SERVICES, INC.
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
193 of 198

SHEALY ENVIRONMENTAL SERVICES, INC.
Khmly r?nvinxvornlna 5,1 Inc- Pnp 1 of 1
rr�-nranr Nwnher M001 &C 14 :iRccdye dk.m; A,7rl013
Sample Receipt Checkiist ( R "
Client; Te,rakoR Cv,)Ier Inspected b :'date: CjN4Nrr-M? GUISf19 URJS076
Ivieam ofTMEript_ ® SE.SI _❑ Client ❑ UPS 1:.aL Othef:
❑ Y No J. Were custody seals prcarnt 4n [he oaolerf?
.'e
No
CIA 12.
Jf q�stodY Isla v.'ere Mscrit, 4rcro th intnet and unbroken?
p1I Strip 1i1, N A CIA -urine Strip ID: NA Vested by; NA
OriginaI winlCimturo upon receipt ! Defi',-rd (CorFec.ted) remperature ulrnn Tmtc pl. %Solid Sriap-Oip TD: NA _
=,9 } 2,4 -C, hlA r XA -C NA J NA nr_ NA eN±} °q_-
4dthod_ ®Temperature Blaaak ❑Against Bottin IR Gual ID: 5 1R Gun CAATtctiuu Factor
eihiA azoolant: ® Wtr t ❑ 1oe Flovks❑ Lory Ice ❑ Nonc
Yes
❑Nor
NA
3, lftcmUcratnrcaEi I an}' a>,olerexceeded-{IgC',v.'a Proj�ctl+lsnagcrNoti ed7
PEA *K%Nnlifledby_ plwne I email I' f4ce-lo-face (Circle one).
❑ Yes
❑ -No
® NA
4. Ts the commcmiak councr's packing slip attached to this Tun-n?
ED Yes
❑Na
.5. Were propermrtrxly pTocedares(rzlinquiahPa!rcuvi%vd)follo+ked?
Ytis
NO
6, Were samplo ILk; listed an Ille c.
0 Y-,s
❑ No
7. Wcrc L� EDs lis eJ on ali mamplo aontair5ers?
0 Y:�-
❑ Nu
8- Was collection date & tirnc, listed on the [ OU!
® Yen
❑ Np
9- Ww� �,wlieotioix date & time listed on alb saample canlaincrV
® Yex
❑ No
10- Did all oontainer labol infrnmaticm (ID, dote, tilttte) ag1\+c with the C{]C?
® YCs
❑ No
1 l- lVcrt: iCnL; (r) be performcd listed ki n8 COC'
YGa
El No
11. Did all samples arrive in tho proper comtainars for ew-h tit andlor in goad condixion
(unbmk+]t4, lic6 on, tic.)?
Yaa
❑ No
113- Wai; adequatc sample volume uvadable?
Yes
❑ N1
1 d- Were all samples recksived wi rhin 1, the balding timc or 48 hours, %k-Nuk VeT comes firth?
ices
No
15- Were arty saakpl0,5 rrrntaintrn missiuk . exce83 (circle me, S= les Not listrid on MCI
fl Yes
Na
] NA
16. For�'OA. n.twi RSK-1?5 sautlpks. wm- kntlahl pre[oeent "pca�siz "{;a"ur 6uim is diaLliew)
in any of aw VIDA vielS?
0 Y+�i
No
NA
17. Were all D1UYn cmis,'nutrianl roles rem ed at a pH 6f < '
❑ Y en
❑ Nu
0 NA
I & Were all c snide samp143s ci%� at a YT � 12 mid sulfides LC5 rccciveE 21t a p11 ? 97
El yn
❑ I+fu
m ichlorine?
19. Wcro app is bl�NHsfIICN'cyatti p oll625 ( 0-3rnVJ1.�:gac4les free o residual
❑ I'`
❑ N°
Z NA
0, Wcm client renkadwrequescs (i.C, roqua;ted di]utionK 1+I&USD 4c nMium, tic---
cturccily tramcribad from tl-m COC into the courment se.etian to LIM?
® ycla
Ne}
21 Wm the =tn number list xl Oil :tic co:itai r - labs]? if es, Quom # 21497
SKruple 1'reacrr-ation (Mu�1 be 4�ipl�led for env sample(5} modtrec#ly pdesen7ed oruid1 hcadapuc�j
Samplc(s) NA Vrere u�advod inovrrcc#ly p3;4:# d acid were �1 djuxrrd I=Clydinglyr
In sar. pir. rxriviiT With NA _rnL of cimle nn& Td2KM, I IN03,11c1, N0014 using 5R .'� NA
Time of pre scr+ation NA If morn thin r,ne re&;a trati%,e is noodcd. p1cm9e rmte im the ooamnem below,
amplc(s) NA w= =ucivcd with bubbles 7,6 min in diameter-
Samples(s) NA WI -Fe ra>oeived with'I'RG �- 4.5 rnWL (IC€1 l� Ls rto ) ami wcrc
'listed accordiugly in sample, receiving with sodium thimulaLle (Nn2$2Q3) with Shealy III; NA
SR barcado lak-is uppliml by- DMlq?ETB Dale: HAS19
E:rrrrinients.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
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SHEALY ENVIRONMENTAL SERVICES, INC.
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Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SHEALY ENVIRONMENTAL SERVICES, INC.
Sllr `IYEn-.:runmenlni Cnu Pape L a= L
Dac=ml Liw76ur:MliUU]Rl-14 hflL� v� DuLc: 6'2.Ml9
Sample Receipt Checklist (SRQ
Client: Tcrrucun Cooler Inspected byjate- l3ml + m f ORf[5l19 LVr17c UH.1511M
eam of receipu m S f'S] ❑ Cli aa' ❑ UPS ❑ FedrA ❑ flrlier-
❑ YrA
® Na
11. Were cu=dy seals present an the cooler?
7'cs
No
NA
2_ TC cu4-LwJ • 6tr aI6 wr rc prcwni., w rt: thpv intact =J unbroken?
Td SLrip FD: NA Chlrni no Rtri; TT]_ NA 'TCLiW by; NA _
On2ttial to m]'lemft a uprm eemijpt I T*riwd (Correctet'I) tryrrLptra m upmi oroipt V.SoUd Sfw-Ctitp K),- NA
2.9 12.9 'C NA rNA C NA }NA °C NA i?xA oC
N'IcLknarl: ❑Tt-mperaiurc fil�rnk ❑ linst E3DUlrs ZR Gun M. 5 1K Ciun C'oLTectron Nectar: U `C
Mcl.'Lwd of -Coo [LkLW ® %VQt lac ❑ lee Paola ❑ ll Lce ❑ Done
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'L. If I�r�;reraLurc of arty crroltr cxcetAcd 6.0°G, Prnjcxt F�lanager 1� oti#ied7
1'M eras Notifrad b}. phone ?email .'tact [ face (.- hale one),
❑ , r ❑ No
O NA
4. 6 the t:nmrncri;ial ciruricr's puWg slip attachod to this form"
[{ Yt�
❑ Wtr
5_ Wi-re pFvpm �-.u�Auciv prac edwvt F (mliruluiahQdhwQivod) fol]owiX
Yes
❑ No
b. Wcre sample I s Lasted on (he COO?
'r' :.
❑ No
7, Were sample U)s listed on all satrrple cantninem?
r .' , ❑ No
8, '-#ar cD1lM1i0n date & MMC listed DE the C OC-'
IZI 'r-- ❑ No
9, Wi< c011=tion data & 1�mc listed on all sainple coutainet ?
0 , . � ❑ No
10, Did oil u�ntairber faM i forrantion (ID. date, t6Lre) agree with Llke COC?
Yes
❑ No
11 _ Wore Lam} to be p rf{sI7l M I l,9ted on dw COS
© Yes
❑ No
r 2, Did all samples ariive in the proper coutahims far each test am&or in good conch ticm
(iinbrokm lids *n, elc,)? _
Ye%
❑ N.
13. Was adequate sample volume available?
Ed Y cs
ONo
14_ Were sit Sample* rwui-rrxl within !'i the haldirrg tuna or 48 hem. whiohcvcr comes fLLstf
Yes
No
15_ Were any samples contoineri mLSitn +cxcc 5(cimiC Ono) sampdcs Not 1had onGCC?
❑ Yes
0Nu
fl NA
16. ForV0A urvd RSK-175 ,sanipIcs, w fc bubbics present>"pea-;~ire" ('l.-Cr fitntn in dfameti
in any of the VOA vials'}
❑ Ycx
No
bd NA
17_ l --,, all DRO!nwalslnutri,ant samples received at a pH of k 2?
❑ Ye&l
C No
21 NA
18. Were all cyunide tram s reecived ai a pff �- 12 and nulfidc sampkg ropcivcd at a pld > 9'�
❑ Yes
El 3vb
NA
19_ wera all apphcab a N1-iJ 'KN+cyan' a-LphenoL+b25 (� 0-5tft 'L) tmtn&s f e of residual
c]slorure?
❑ Ya1
❑ No
17 INA
20. Wcro clier:t mmarksirequeats (Le. requested dilutians, MSeV91) d2Aig-rnatinnq, etc...j
concc-ly tmnscnbed frorn the CDC ini n lire o=nnen t £ectiun in UM ?
® Yes
NOJ
121, Was the quote narnber listed an the comainer lard? Fyc,_ 2l I97
umplc
]PL��ervation t;l!rlLrat lac eomplctcd for an}' ssmple(sj i�xc.rrrrectly ltreservved or with lreadspa�cG.)
,'aLnple(s) NA wart rcc6vcd iwerrc fivdy prc,scrved and u'Crc adjusted accordiagiy
iu sample receivinj� tvitik NA xnL of uircfe tm�,; 142304, '03, HC:3, NaOE using SR # NA
Time o f pre-;ennation NA If morn than one prescnratn'c is rKcdcd, please note to the c 3snmem below-
Santple(s) NA 4"Irc mclwivc4 with babbirs --6 ou n in diamcicr,
samplQgA) NA w= rxciw d with 'i'RC r} 0,5 niWL (if #19 is w) and ware
adju,ited acowdingly in sarnp[o irwev-tng with sodium ttva8u1fatc (Na25zC3) with Shealy TD- LTA
SR barcode labeLs npplW by; D ihUP'PB Dmw; o[Ill5l14 - .
C:OM111terus'.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SHEALY ENVIRONMENTAL SERVICES, INC.
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197 of 198

SHEALY ENVIRONMENTAL SERVICES, INC.
bl c ly Fnwnr.mcumI. S nICec, r-nc. Pub t of f
Romwnew Kf lwr. MnDl pit rb 1:11LL i-.r Rae: Mb-M H
Sample Receipt CiheMist ( RQ
C'I�rnl '1'ciraavn ('" Tzizr�-IMilwiilni&TAMr.Tu1 08;15119 i;vl;q- 131:115079
sans of receipt: 0 SISI f'lient 0 TJ15S 0 WDC O$W, 1
❑ Yes
0 No
I t- werc cwauldy seulrl re:SCnt sin the 4 rnoler? -- —
NA
2. If cu 5tgd Seals were 1kr2 ut were they, intact and m9E token? -----
pU $Irix ID: NA Chloxjsv Strip ID; NA Tt��tjd by= NA
Ur;g6al. Lerhp,'ratirre LLPM Ytr*ipl ?Derived (CLTI*Ct&b Idruperritrrte upCM rar;eipL %Solid Snap -Cup 1D=
2..y 12.9 }C. NA JNA ce NA 1Nk 4C NA rhA GC
ieriiad- ®'t cn iprratur 1#lank ❑ Agaitwt 33at#les llt C;un 11J: 5 JR (iun C:onection Factor; 0 "C
.Method ofcoolanu 0 Wet Ice ❑ Ice Par -lc; ❑ Dry Ice ❑ Tonne
❑ Yr;
❑ No
® Wk
3, If temperamula of airy 000ler exceeded 6,0".C, Am Projeci Manager Notified?
PM was Notilod b}; phone.-' email ! fNe-w-fare (oucl$ out).
❑ Yvs
❑ No
O KA
4. 1m the cpmmerraat a 1nrier's pagkiug slip attached to dus fiolni''
21 Yvz
❑ NO
5- Wt= 13rvpm crtsbydy S%Cdwv%C {rgli ui51�C r�CCcCl{^G Fa1JQwW4
® Yes
❑ Ko
& Were sample Ws listed on the COC?
0 Yeal
❑ NO
7, Were sample IDS listed on all san>,ple " ntainers?
® Yes
❑ No
2, Was collectr m date & rime listed out t1w Cs(AC':'
Q No
9. Was cDllectlon dace & tune listed on ail sample crmtainerx?
L 1 Yes
❑ No
10. Did sll oontaituer label inimu>ntiou (ID, date, 6016) agme willr Llae COC?
I. yes
❑ No
I I . Were tests to be performed listed on die COC,)
i ' ;
❑ Na
11 Did all samples arrive in then prope�f cxmtabiers for each rest u&or in good cotTditlui
(unbrol=6lids M16 stc)?
1�1 Yes
❑ No
13, Wo s adequate ie voltune av-aJlable?
0 Yes
0 No
14, Wcrc al l samples rarrivc d Within 'h die holding tune or 4tC hours, whieliever comes first'd
Yeii
❑ 14cl
15- Were rrn • ramplcs emledners 5mnpk3 Not 1LgUd on CCO.,
❑ Y r;
®1*]sr
El N
16, For VOAand SIC-1? SrlCl�}lcs,''CC� buhb:cs prescnt?"pea-size" (::'tYfitnm in diatriererj
�in? ny of thrVOA vials`
Yes
NoN,
17- Vere of I ftNeasutrient sp€es rriyn'
d at a pH of < 7
❑ 'Yes
No
ONA
18, Were all cyanide saalples received at a plf� 12 aril sulfite rumplvk rcuuivt�d uL d pR'- 4?
❑ `r-sss
❑ No
� NA19-
Worc a]I applicable NH..;'ll�WryaniderphamoP625 (<{1.im L) samples tea of residual
cblarine?
Yes No
0 Ncometiv
20, 'Were client remarkVrequests (i-e- requened dilutiatis, M%WS D designa6cnvq, etc-.)
Transcribed f -am dye COC into the comment secdon in LINPS?
-Z Yes
Nal
21- Was the goom munbelr listed an the container label? If T&r Qwte N 2107
�:irttple Preaerusfion (Must be aomp]ct>~d for any samplc(s) incorrectly preserved or with headspacc.)
Sample(4) NA were M"irvd incorrectly prGsotV-Cd And WM adjusted acu+n1i11;;1...
in siwnplt: riving with NA mL uCcircic {jrYC: H2804, pNO3, HCI, NuOK ueirrd 5R k NA
ime o(preservgl_i on NA If mom then one pri% vativc it ncodcd, plcwr, note in the commcm below.
fu rpJ ) NA wrre rmnc %vd with bubblm `-6 mm in riiameiee-
Sarnplc,.s(s) NA were rcrcivod with 1 KC° �- 0.5 mgI (1(#19 is ne) mid wean
adjusted accordingly En sample rroei%i g with sodium thiosuffatQ, (Na2S: yr with Shealy ID: NA
SR bexcodc labrls applied by; D'{R1E rB Du= Q81 ] SI19
C'ommcntx: 4'-71jme labeled 11,25 on castainers, time -on CoC is 1 l ; 35. Onc container from s2impl c Ni!W-7 is labeled as
MW-2 on container,
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
198 of 198

APPENDIX B
Historical Groundwater Analysis Tables

TABLE 4
GEOCHEMICAL ANALYSES OF GROUNDWATER SAMPLING
NOYEMBRR 14 1996
aniple
Location
sample
Late
All Compounds
610 list by Method 625
Diesel Rangc Organics
by Method 35101M
m
IVf W-6
Not sarn led - 1.5" of free product observed on 1 if 14196.
M -7
11/14/96
<50
630
M �
11/14196
450
10.9
M -9
11/14196
<0
300
W-10
11/14/96
<50
not analyzed
TABLES
GI&OCHEMICAL ANALYSES OF GROU D ATER SAMPLING:
NOVEMBER 22,1996
Sample
Location
Sample
Date
Method 602
Method 625
u
-2
11122l9
MTBE: 6.b
B L <10
M -3
11 /22196
S L< 1
B 2L <l 0
W-4
11/22196
benzene: 2.3
MTBE: 5.1
BQL (<10)
-5
11 /22J96
B L <1
B L <I 0
M -6
11/22/96
ethylbenzene; 50
toluene: 57
x lencs: 412
anthracene: 145
fluorene: 103
na hLMene: 197
TP-1
11/22/96
B L <l
$ L <I0
TP-3
11/22/96
B L � 1 02
1 BQI. <l0
Data from the January 24, 1997 Comprehensive Site Assessment prepared by Engineering
Consulting Services, Ltd.

Beverly, Trudy
From: Beverly, Trudy
Sent: Thursday, September 26, 2019 2:46 PM
To: DSouza, Flora J
Subject: RE: [External] Mt. Pleasant DOT report
Thank Flora.
Trudy
Trudy Beverly, L.G.
IEQ��
Hydrogeologist, Division of Waste Management
_ North Carolina Department of Environmental Quality
Leparlran[oi Lnnronm catGmY�R` UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy. B everlykncdenn gov
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https:Hfiles.nc.gov/ncdeq/Waste%20Management/DViM[UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx
From: DSouza, Flora J [mailto:[e-mail]]
Sent: Thursday, September 26, 2019 2:40 PM
To: Beverly, Trudy <[e-mail]>
Subject: [External] Mt. Pleasant DOT report
VRExternal email. Do not click links or open attachments unless you verify. Send all suspicious email as an
[e-mail]
Trudy,
Attached is the report for the Mt. Pleasant DOT site. I will also put a hard copy in the mail.
Thank you,
Flora J. D'Souza, CHMM
Senior Scientist I Environmental
Terracon
2701 Westport Road I Charlotte, North Carolina 28208
P (704) 509-17771 F (704) 509-18881 M [phone]

Direct [phone]
Flora.Dsouza(Merracon.com I terracon.com
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