5002_JacksonCounty_MSWLF_GW_FID1387225_20200109

�DJUNR USE ONLY: []Paper Report El Electronic Data - Email CD (data loaded: Yes / No) Doc/Event #:
NC DENR Environmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
• Prepare one form for each individually monitored unit.
• Please type or print legibly.
• Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
• Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
• Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(i).
• Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Anchor QEA of North Carolina, PLLC
Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address:
Name: Alec Macbeth
E-mail: [e-mail]
Phone: [phone]
NC Landfill Rule: Actual sampling dates (e.g.,
Facility name: Facility Address: _ Facility Permit # f (.0500 or. 1600) October 20-24, 2006)
Jackson County Municipal Solid US Highway 441 58-02 f .1600 October 22 through 24, 2019
Waste Landfill DillsbOro, North Carolina 28725
Environmental Status: (Check all that apply)
❑ Initial/Background Monitoring ❑ Detection Monitoring Q Assessment Monitoring Corrective Action
T e of data submitted: (Check all that apply)
X Groundwater monitoring data from monitoring wells
Groundwater monitoring data from private water supply wells
X Leachate monitoring data
X Surface water monitoring data
Methane gas monitoring data
R Corrective action data (specify)
Other(specify)
Natural Attenuation Parameters
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct.
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification Including the possibility of a fine and imprisonment.
Alec Macbeth, PG
Senior Scientist
828-281-3350
Facility Representatives Name (Print) r Title (Area Code) Telephone Nu
January 9, 2020 Affix NC Lice
Signature v[w , Date
231 Haywood Street, Asheville, North Carolina 28801 47 ' 0K?t r:_I a
a @e �wR r�Mc.�ata u,
Facility Representative Address 'UOUWM
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NC PE Firm License Number (if applicable effective May 1, 2009) e�f Br F 1 isv
Revised 612009
Seal

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January 2020 ANCHOR
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02Z QEAA"
Fall 2019
Semiannual Water Quality Monitoring Report
Prepared for Jackson County Solid Waste Department

January 2020
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02
Fall 2019
Semiannual Water Quality Monitoring Report
Prepared for
Jackson County Solid Waste Department
401 Grindstaff Cove Road
Sylva, North Carolina 28779
O-ea-IL-o�
Alec Macbeth, PG
Project Geologist
Prepared by
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Project Number: C91480-01.01
\\asheville1\asheville\Projects\Jackson County\Dillsboro GW\ Repo rts\2019\Fall\Text\Semiannual Water Quality Report_010720.docx

TABLE OF CONTENTS
1 Introduction
1
2 Semiannual Monitoring...........................................................................................................3
2.1 Groundwater, Surface Water, Domestic Well, and Leachate Sampling..........................................3
2.1.1 Monitoring Well Purging and Sampling Methods.................................................................3
2.1.2 Surface Water Sampling Methods................................................................................................4
2.1.3 Leachate Sampling Methods..........................................................................................................4
2.1.4 Domestic Well Sampling Methods...............................................................................................5
2.2 Sample Handling, Documentation, and Analysis....................................................................................5
3 Findings........................................................................................................................................7
3.1
Groundwater.........................................................................................................................................................7
3.1.1 Field Parameters..................................................................................................................................8
3.1.2 Appendix II Metals..............................................................................................................................8
3.1.3 Appendix II VOCs and 1,4-Dioxane..............................................................................................9
3.1.4 Natural Attenuation Parameters.................................................................................................
10
3.2
Surface Water....................................................................................................................................................10
3.2.1 Field Parameters...............................................................................................................................10
3.2.2 Appendix II Metals...........................................................................................................................10
3.2.3 Appendix II VOCs and 1,4-Dioxane...........................................................................................
11
3.3
Leachate...............................................................................................................................................................11
3.4
Domestic Well....................................................................................................................................................
11
3.4.1 Field Parameters...............................................................................................................................11
3.4.2 VOCs......................................................................................................................................................11
3.5
Groundwater Flow Directions......................................................................................................................12
4 Summary....................................................................................................................................13
4.1 Groundwater Quality......................................................................................................................................13
4.1.1 Metals....................................................................................................................................................13
4.1.2 Volatile Organic Compounds....................................................................................................... 13
4.1.3 Field Parameters and Other Constituents............................................................................... 13
4.2 Surface Water Quality.....................................................................................................................................13
4.3 Leachate Quality............................................................................................................................................... 14
4.4 Domestic Well Water Quality......................................................................................................................14
Fall 2019 Semiannual
Water Quality Monitoring Report i January 2020

5 Future Activities........................................................................................................................15
6 References.................................................................................................................................16
TABLES
Table 1 Summary of Laboratory Analyses Performed on Samples
Table 2 Well Construction Details and Corresponding Elevations
Table 3 Summary of Analytical Results
Table 4 Mass Removal Calculations for Volatile Organic Compounds (VOCs) Detected in
the Leachate Sample (LT-01)
FIGURES
Figure 1
Site Location Map
Figure 2
Site Layout Map
Figure 3
Generalized Groundwater Flow Direction
Figure 4
Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time
(Monitoring Well MW-01)
Figure 5
Hydrograph and Benzene Concentration vs. Time (Monitoring Well MW-01)
Figure 6
Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time
(Monitoring Well MW-05R)
Figure 7
Hydrograph and Benzene Concentration vs. Time (Monitoring Well MW-05R)
Figure 8
Hydrograph and Vinyl Chloride Concentration vs. Time
(Monitoring Well MW-05R)
Figure 9
Hydrograph and Benzene Concentration vs. Time (Monitoring Well MW-07)
APPENDICES
Appendix A Well Sampling Logs, and Equipment Documentation and Instrument Calibration
Data Sheets
Appendix B Reports of Laboratory Analysis, Chain -of -Custody Documentation,
and Certificates of Analysis
Fall 2019 Semiannual
Water Quality Monitoring Report ii January 2020

ABBREVIATIONS
pg/L micrograms per liter
PS/cm microsiemens per centimeter
213 standard North Carolina surface water quality standards, as defined in 15A NCAC 213
2L standard North Carolina groundwater quality standards, as defined in 15A NCAC 2L .0202
AM Analytical Method
bgs below ground surface
BOD biochemical oxygen demand
CAER Corrective Action Evaluation Report
CAP Corrective Action Plan
COD chemical oxygen demand
DENR North Carolina Department of Environment and Natural Resources
DEQ North Carolina Department of Environmental Quality
DO dissolved oxygen
DWM Division of Waste Management
EPA U.S. Environmental Protection Agency
IMAC interim maximum allowable concentration
MDL method detection limit
mg/L milligrams per liter
MNA monitored natural attenuation
MSWLF Municipal Solid Waste Landfill
mV millivolts
NCAC North Carolina Administrative Code
NTU Nephelometric Turbidity Unit
ORP oxidation reduction potential
PWR Partially Weathered Rock
SC specific conductivity
Site Closed Municipal Solid Waste Landfill, approximately 0.75 miles west of Dillsboro,
North Carolina, on the northeast side of Old Dillsboro Road (Old U.S. Highway 74)
SM Standard Method
SU Standard Unit
SVOC semivolatile organic compound
SWS Solid Waste Section
TOC total organic carbon
TWSA Tuckasegee Water & Sewer Authority
VOC volatile organic compound
Fall 2019 Semiannual
Water Quality Monitoring Report iii January 2020

1 Introduction
The Jackson County Solid Waste Department maintains a closed Municipal Solid Waste Landfill
(MSWLF; the Site) approximately 0.75 mile west of Dillsboro, North Carolina, on the northeast side of
Old Dillsboro Road (Old U.S. Highway 74; Figure 1). Water quality monitoring at the landfill is
governed by the North Carolina Department of Environmental Quality (DEQ), Division of Waste
Management (DWM), Solid Waste Section (SWS), under Permit No. 50-02 issued to Jackson County.
The landfill permit requires semiannual monitoring of groundwater and surface water quality.
Since October 2007, when Anchor QEA of North Carolina, PLLC (formerly Altamont Environmental,
Inc. [Altamont]), began performing water quality monitoring events at the Site, groundwater quality
monitoring has indicated persistent low-level concentrations of constituents that exceed
groundwater quality standards. In response to the continued exceedances of the analyzed
constituents, an Assessment of Corrective Measures was submitted to the North Carolina Department
of Environment and Natural Resources (DENR; now the DEQ) on September 7, 2010 (Altamont 2010).
A Corrective Action Plan (CAP; Altamont 2011) was implemented upon approval by the DENR, as
recorded in the September 1, 2011 letter regarding "Approval of the County's Corrective Action Plan"
(DENR 2011). The implemented remedy includes the extraction of leachate through dedicated
submersible pumps installed within landfill gas extraction wells and disposal of the leachate into the
Tuckasegee Water & Sewer Authority (TWSA) collection system. In addition to the leachate
extraction, groundwater natural attenuation parameters are monitored, and natural attenuation
processes are evaluated. As discussed in the CAP, a corrective action evaluation report is prepared
every 5 years. The evaluation report analyzes the progress of the approved corrective action remedy
based on semiannual water quality monitoring data. The remedy was implemented in a phased
approach, with full implementation occurring on September 6, 2013. The first Five -Year Corrective
Action Evaluation Report (CAER), submitted by Altamont on October 31, 2016 (Altamont 2016),
concluded that the current conditions of the monitored natural attenuation (MNA) parameters and
Site geochemical parameters allow for the slow degradation of the select contaminants identified in
the CAER. The second CAER is scheduled to be submitted in 2021.
This report serves as the second semiannual water quality monitoring report for 2019. The report
provides an evaluation of groundwater and surface water quality. The water quality monitoring
network is presented in Figure 2. The generalized groundwater flow direction in the upper parts of
the underlying aquifer system is provided in Figure 3.
In addition to groundwater and surface water monitoring, this report includes volatile organic
compound (VOC) analysis of the extracted leachate and one domestic water well.
The water samples collected from selected monitoring points during the spring sampling event were
analyzed for a range of parameters, as presented in Section 2.2 and Table 1.
Fall 2019 Semiannual
Water Quality Monitoring Report 1 January 2020

The fall 2019 sampling event was performed on October 22, 23, and 24, 2019, and is being reported
in accordance with requirements stipulated in the DEQ Solid Waste Management Rules codified
under Title 15A, Subchapter 13B of the North Carolina Administrative Code (NCAC).
Fall 2019 Semiannual
Water Quality Monitoring Report 2 January 2020

2 Semiannual Monitoring
2.1 Groundwater, Surface Water, Domestic Well, and Leachate
Sampling
The Site monitoring wells (MW-01, MW-02, MW-03, MW-04, MW-05R, MW-06, and MW-07), surface
water sample locations (SW-01 and SW-02), leachate sample location (LT-01), and domestic well
(DW-01) were sampled on October 22, 23, and 24, 2019, by Anchor QEA. Static groundwater level
measurements and field parameter data are included on the sampling logs presented in Appendix A.
Field equipment calibration logs for the YSI Professional Plus Multiparameter Water Quality Meter
and the Hach 2100Q Turbidimeter are also provided in Appendix A. The full suite of groundwater
and surface water laboratory analytical results is presented in the laboratory analysis reports in
Appendix B.
Monitoring wells MW-01 and MW-06 are the Site's upgradient monitoring wells. MW-03 and MW-
05R are located in the midgradient portion of the Site and MW-02, MW-04, and MW-07 monitor
downgradient portions of the Site. As summarized in Table 2, the total depths of the monitoring
wells range from 40 to 110 feet below ground surface (bgs). The geology of the screened intervals of
the monitoring wells is as follows:
• Saprolite': MW-04 and MW-05R
• Partially Weathered Rock (PWR)Z: MW-03
• Bedrock3: MW-01, MW-02, MW-06, and MW-07
The locations of the monitoring wells, surface water samples, leachate, and domestic well sample
locations are shown in Figure 2.
2.7. 7 Monitoring Well Purging and Sampling Methods
Before the monitoring wells were sampled, the static water level was gauged in each well, and an
initial round of field parameters was measured (consisting of pH, specific conductivity [SC], dissolved
oxygen [DO], turbidity, temperature, and oxidation reduction potential [ORP]).
Anchor QEA personnel used either low -flow techniques or disposable bailers to purge the
monitoring wells and collect groundwater samples. The total depth, condition of the casing, and
groundwater recharge rate determined the purging and sample collection method employed at each
monitoring well.
Saprolite is the result of in -place weathering that produces soil -like material that retains relict features of the parent rock
z PWR is generally found above the bedrock and is softer than bedrock, but not as soft as Saprolite.
s Bedrock is solid competent rock that underlies Saprolite and partially weathered rock.
Fall 2019 Semiannual
Water Quality Monitoring Report 3 January 2020

2.1.1.1 Monitoring Wells
Four of the monitoring wells (MW-03, MW-04, MW-06, and MW-07) were purged using low -flow
techniques in accordance with the procedures described by the U.S. Environmental Protection
Agency (EPA) in Low -Flow (Minimal Drawdown) Ground -Water Sampling Procedures (EPA 1996).
During purging, the field parameters (pH, SC, DO, ORP, turbidity, and temperature) were measured
and recorded approximately every 3 minutes. Well purging continued until these parameters had
generally stabilized for three consecutive readings. The required stabilization criteria are determined
by the EPA Region 4 Science and Ecosystem Support Division in Operating Procedure: Groundwater
Sampling (EPA 2017) and are summarized as follows:
• pH values within ± 0.1 Standard Unit (SU)
• SC values within ± 5%
• Temperature, DO, and turbidity values within ± 10%
• ORP values within ± 10 millivolts (mV)
Once the parameters had stabilized, a groundwater sample was collected by a technician wearing a
new pair of nitrile gloves, using laboratory -supplied sample containers.
Because of their slow recharge rates, monitoring wells MW-01, MW-02, and MW-05R were purged
and sampled using disposable polyethylene bailers. The wells were purged of three successive well
volumes or purged dry, whichever occurred first. Monitoring well MW-5R was purged and sampled
on October 23, 2019. Monitoring well MW-02 was purged dry on October 22, and sampled on
October 23 after the well had had sufficient time to recharge. Monitoring well MW-01 was purged
and sampled on October 24, 2019. A round of field parameters was measured and recorded at the
start of purging and after each consecutive well volume had been purged.
Field parameter data are shown in the well sampling logs included in Appendix A.
2.7.2 Surface Water Sampling Methods
Surface water samples SW-01 and SW-02 were collected on October 22, 2019, at designated
locations from the Tuckasegee River, which is adjacent to and southwest of the landfill (Figure 2).
Sampling location SW-01 is assumed to represent surface water quality upstream of the landfill, and
sampling location SW-02 is assumed to represent surface water quality downstream of the landfill.
One round of field parameters was measured and recorded at each surface water sampling location
immediately prior to collecting the sample (Appendix A). The surface water samples were collected in
laboratory -provided sample containers by a technician wearing a new pair of nitrile gloves.
2.7.3 Leachate Sampling Methods
Dedicated bottom -loading air -powered pumps, air pressure lines, and a leachate force main
collection system are installed at the landfill. Pumps are installed in landfill gas extraction wells
Fall 2019 Semiannual
Water Quality Monitoring Report 4 January 2020

EW-1 R, EW-2R, EW-31R, EW-4, EW-5, EW-6, EW-7, EW-8, EW-9, and EW-10. The gas extraction well
locations are presented in Figure 2. The leachate is pumped from the wells into a flow equalization
tank, which is connected to the TWSA wastewater collection system.
The flow equalization tank is east of the landfill, adjacent to the existing landfill gas flare. A grab
sample of leachate (LT-01) was acquired on October 22, 2019, by collecting a sample as the leachate
entered the flow equalization tank. One round of field parameters was measured and recorded after
the sample was collected (Appendix A).
2.7.4 Domestic Well Sampling Methods
The domestic well water sample (DW-01, owned by Mr. Frank Wilkie) was collected on October 24,
2019, from an outside spigot at the residence located at 318 Joe Wilkey Road, bordering the
northern boundary of the landfill (Figure 2). The well was purged of 30 gallons each prior to sample
collection. One round of field parameters was measured and recorded after the 30 gallons had been
purged. The domestic well water sample was collected in laboratory -provided sample containers by a
technician wearing a new pair of nitrile gloves.
Attempts to sample the second domestic water well (DW-2, owned by Mr. Joshua Bulla at
138 Joe Wilkey Road) were unsuccessful, because the owner could not be contacted.
2.2 Sample Handling, Documentation, and Analysis
Field parameters and additional observations pertaining to the Site sampling locations are provided
in the sampling logs (Appendix A). Following sample collection, each groundwater, surface water,
leachate, and domestic well water sample was immediately placed on ice in a sample cooler for
transport to Prism Laboratories, Inc., a North Carolina -certified laboratory in Charlotte,
North Carolina. The groundwater samples collected from the monitoring wells were analyzed for the
following parameters (Table 1):
• Appendix II metals, including mercury, using EPA Methods 6020B and 7470A
• Appendix II VOCs, using EPA Method 8260D
• Appendix II semivolatile organic compounds (SVOCs), using EPA Method 8270E
— This analysis was not performed on samples collected from MW-04 and MW-07
because of an inadvertent miscount of bottle ware.
• 1,4-Dioxane, using EPA Method 8260DSIM
• MNA parameters:
— Alkalinity, using Standard Method (SM) 2320B
— Biochemical oxygen demand (5-day; BOD), using SM 5210B
— Carbon dioxide, ethane, ethene, and methane, using Analytical Method (AM) 20GAX
— Hydrogen (only in MW-03, MW-04, MW-06, and MW-07), using AM20GAX
Fall 2019 Semiannual
Water Quality Monitoring Report 5 January 2020

— Chemical oxygen demand (COD), using SM 5220D
— Chloride, nitrate, and sulfate, using EPA Method 9056A
— Ferrous iron, using SM 3500-Fe D
— Sulfide, using SM 4500-5 F
— Total organic carbon (TOC), using SM 5310B
— Volatile fatty acids, using AM23G
The surface water samples were analyzed for the following parameters:
• Appendix II metals, including mercury, using EPA Methods 6020B and 7470A
• Appendix II VOCs, using EPA Method 8260D
• Appendix II SVOCs, using EPA Method 8270E
• 1,4-Dioxane, using EPA Method 8260DSIM
• Hardness, using SM2340C
The leachate sample was analyzed for the following parameters:
• Appendix II VOCs, using EPA Method 8260D
The domestic well sample was analyzed for the following parameters:
• VOCs, using EPA Method 524.2
The SWS issued the memorandum "1,4-Dioxane Analysis, Solid Waste Section Limits, and Laboratory
Analytical Methods" dated May 29, 2018, which requires the analysis of 1,4-dioxane at landfills after
July 1, 2018 (DEQ 2018a). Per this memorandum, 1,4-dioxane was included in the sampling suite for
Site monitoring wells and surface water samples beginning with the October 2018 sampling event.
Appendix I and II parameters are identified in Appendix I and II of the Code of Federal
Regulations (CFR), Title 40, Part 258.
Proper chain -of -custody documentation procedures were followed during collection and
transportation of each sample (Appendix B). Five trip blank samples for quality control/quality
assurance purposes were included in the sample coolers and analyzed for Appendix II VOCs and for
1,4-dioxane when applicable. The reports of the laboratory analyses are provided in Appendix B.
Laboratory analyses performed on the samples are summarized in Table 1.
Fall 2019 Semiannual
Water Quality Monitoring Report 6 January 2020

3 Findings
The field parameter data and laboratory analytical results for the groundwater samples (from
monitoring wells MW-01 through MW-07), surface water samples (SW-01 and SW-02), leachate
sample (LT-01), and domestic well sample (DW-01) collected at the landfill are included in
Appendices A and B. The results are also submitted separately to the DEQ DWM SWS in the
Electronic Data Deliverable format (DENR 2014).
As stipulated in the May 2010 DWM documents referenced in the preceding paragraph, all
laboratory analytical results were reported and appropriately qualified as follows:
• Non -Detections: Non -detections (non -detects) are values reported by the laboratory as below
the method detection limits (MDLs). They are tabulated in Table 3 and flagged with a "U" qualifier.
The MDL is the minimum concentration of a substance that can be measured and reported by a
laboratory with 99% confidence that the constituent concentration is greater than zero.
• Estimated or "J" Qualified: A "Y' qualifier is used by the laboratory for parameters that are
detected at estimated concentrations greater than the MDL but less than the laboratory's
method reporting limit. The method reporting limit is the minimum concentration of a target
analyte that can be accurately determined by the referenced method.
• Groundwater Quality Standard: Detected concentrations of constituents in groundwater
samples were compared to applicable North Carolina groundwater quality standards. For
most constituents, this standard is the 2L standard, defined in 15A NCAC 2L .0202. Detected
concentrations of analytes in groundwater with no established 2L standard were compared to
the interim maximum allowable concentrations (IMACs) for Class GA and GSA groundwater (in
accordance with 15A NCAC 02L .0202 [c]). For the purposes of this report, groundwater
standards were taken from the October 15, 2018 list published by the NC SWS (DEQ 2018b).
• 2B Standard: Detections of analytes in surface water samples were compared to the
surface -water quality standards 2B standards, defined in 15A NCAC 2B. Hardness -dependent
2B surface water standards were calculated using the average analyzed hardness value
(calculated from the upstream and downstream surface water sampling location results) via
the most stringent hardness -dependent metal calculation.
Table 3 presents a summary of detected concentrations of analytes that exceeded their respective
2L standard, IMAC, or 2B standard.
3.1 Groundwater
Measured field parameters and analytical results for groundwater samples collected from the
monitoring wells during the fall 2019 sampling event are discussed in the following sections and
summarized in Table 3.
Fall 2019 Semiannual
Water Quality Monitoring Report 7 January 2020

3.7.7 Field Parameters
Field parameter measurements were obtained from monitoring wells MW-01, MW-02, MW-03, MW-
04, MW-05R, MW-06, and MW-07. The pH readings ranged from 5.34 to 7.02 SU. Of these
monitoring wells, the pH values for MW-01, MW-02, MW-03, MW-04, MW-06, and MW-07 were
below the 2L Standard pH range of 6.5 to 8.5 SU.
The measured turbidity was measured at 2.14 to 127 Nephelometric Turbidity Units (NTU). Generally,
the higher values were measured at the monitoring wells (MW-1, MW-02, and MW-05R) that were
purged and sampled using the bailer method (Section 2.1.1). The bailers were lowered gently to
minimize water column disturbance when the samples were collected. The lowest turbidity
(2.14 NTU) was measured in the groundwater sample collected from monitoring well MW-06.
DO concentrations at the Site ranged from 0.83 milligram per liter (mg/L) in monitoring well MW-03
to 10.45 mg/L in monitoring well MW-02. SC concentrations at the Site ranged from
68.3 microsiemens per centimeter (pS/cm) in monitoring well MW-06 to 740 pS/cm in monitoring
well MW-07. ORP concentrations at the Site ranged from -55.5 mV in monitoring well MW-05R to
359.4 mV in monitoring well MW-04. Groundwater standards are not established for DO, SC, or ORP.
These measured field parameter values are consistent with historical data.
3.7.2 Appendix 11 Metals
Twelve metals were detected in the monitoring well samples. Two of these metals, cobalt and
vanadium, were detected at concentrations above their respective 2L or IMAC water quality
standards in the groundwater samples collected from one or more of the monitoring wells during
the fall 2019 water quality monitoring event.
Cobalt was detected above its IMAC (1 micrograms per liter [pg/L]) in groundwater samples collected
from each of the monitoring wells. Cobalt concentrations in these samples ranged from an estimated
1.3 pg/L (MW-07) to 150 pg/L (MW-01). Historically, cobalt has been present at concentrations
above its applicable water quality standard in groundwater samples from each of the seven
monitoring wells.
Vanadium was detected in the groundwater sample collected from MW-02 at a concentration of
11 pg/L, exceeding its 2L standard of 0.03 pg/L. Historically, vanadium has been present at
concentrations above its water quality standard in samples collected from multiple groundwater
monitoring wells at the Site.
Fall 2019 Semiannual
Water Quality Monitoring Report 8 January 2020

3.7.3 Appendix 11 VOCs and 7,4-Dioxane
Fourteen VOCs were detected in one or more of the monitoring wells. Four of these VOCs
(1,4-dichlorobenzene; benzene; vinyl chloride; and 1,4-dioxane) were detected at concentrations above
their respective 2L standards in the groundwater samples collected from one or more monitoring wells.
Except for 1,4-dioxane, concentration -versus -time graphs (trend plots) were created for the monitoring
wells that have historically exhibited VOC concentrations above the associated 2L standards (Figures 4
through 9). As noted in Section 2.2, 1,4 dioxane has only been analyzed for since October 2018. This
compound will be included in the trend plots in future semiannual reports, as warranted.
The detected concentration of 1,4-dichlorobenzene exceeded its 2L standard (6 pg/L) in monitoring
well MW-01 (8 pg/L) and MW-05R (7.9 pg/L). The historical 1,4-dichlorobenzene concentration trend
in MW-01 remains relatively stable (Figure 4).
Benzene was detected at concentrations above its 2L standard of 1 pg/L in three monitoring
wells: MW-01 (1.6 pg/L), MW-05R (2.1 pg/L), and MW-07 (1.2 pg/L). Overall, historical benzene
concentration trends in monitoring wells MW-01, MW-05R, and MW-07 have been stable and
slightly above the 2L standard (Figures 5, 7, and 9).
The concentration of vinyl chloride in the sample collected from one monitoring well, MW-05R,
(1.8 pg/L) was above the compound's 2L standard (0.03 pg/L). A trend plot for vinyl chloride
concentrations in MW-05R is presented in Figure 8 and shows a steady trend of concentrations
above the 2L standard. Vinyl chloride was not detected in the other monitoring wells during this
sampling event (Table 3). Historically, vinyl chloride has exceeded its 2L standard in monitoring wells
MW-04, MW-05R, and MW-07, located in the southwestern part of the landfill.
The detected concentrations of 1,4-dioxane exceeded its 2L standard (3 pg/L) in MW-02, MW-03,
MW-04, MW-05R, and MW-07, with concentrations ranging from 4.0 pg/L (MW-02) to 18 pg/L (MW-
07). 1,4-Dioxane was not detected in monitoring wells MW-01 or MW-06. The fall 2019 sampling
event represents the third sampling event that 1,4-dioxane was included in the analytical suite, in
accordance with the SWS May 29, 2018 memorandum (DEQ 2018a).
A review of historical groundwater data indicates that four VOCs (1,4-dichlorobe nzene; benzene;
tetrachloroethene (not detected at concentrations above its 2L standard in fall 2019); and vinyl
chloride) have been detected at relatively consistent concentrations for the past several years. As
described in Section 3.2.3, historical surface water samples from the Tuckasegee River, which likely
receives discharge from the saprolite groundwater -bearing zone, have consistently shown no
detections of these compounds, or other VOCs.
Fall 2019 Semiannual
Water Quality Monitoring Report 9 January 2020

3.7.4 Natural Attenuation Parameters
During this sampling event, the groundwater samples were analyzed for MNA parameters as
described in Section 2.2 (Table 1). The results of these analyses are summarized in Table 3. These
parameters were detected in one or more groundwater samples collected from the monitoring wells.
Many of these parameters do not have established groundwater standards. Of the parameters that
do have established groundwater standards, chloride and sulfate, there were no exceedances. An in-
depth analysis of the MNA parameters that apply to the Site's select contaminants was presented in
the first Five -Year CAER (Altamont 2016). The CAER concluded that the MNA data provide evidence
that both reductive degradation and aerobic degradation are occurring in different portions of the
Site. The current data on the MNA parameters will be used in the second Five -Year CAER (scheduled
for 2021) to evaluate the degradation processes at the Site.
3.2 Surface Water
The following sections summarize the measured field parameters and analytical results associated
with the two surface water samples collected during the fall 2019 sampling event.
3.2.7 Field Parameters
The pH readings for the upstream (SW-1) and downstream (SW-2) surface water samples collected
during the fall 2019 sampling event were 7.44 and 7.43 SU, respectively. The pH readings for both
surface water samples were within the 2B standard range of 6.0 to 9.0 SU.
The turbidity values measured in SW-01 (8.00 NTUs) and SW-02 (6.31 NTUs) were below the 2B
standard, which is established at less than or equal to 50 NTU for the receiving water in streams not
designated as trout waters.
DO was measured at a concentration of 10.54 mg/L in SW-01 and 10.02 mg/L in SW-02. The
2B standard is established as greater than or equal to 5.0 mg/L; thus, each sample is within the
acceptable DO range.
SC concentrations in surface water samples SW-01 and SW-02 were recorded at 38.6 and
38.5 pS/cm, respectively. ORP values for SW-01 and SW-02 were 190.3 and 188.5 mV. These
concentrations of SC and ORP are consistent with historical data for both surface water samples. 2B
standards do not exist for these parameters.
3.2.2 Appendix 11 Metals
Two metals (barium and zinc) were detected in both surface water sampling locations. Neither of
these metals were detected at concentrations exceeding their applicable 2B standards.
Fall 2019 Semiannual
Water Quality Monitoring Report 10 January 2020

3.2.3 Appendix 11 VOCs and 7,4-Dioxane
Acetone was detected at a concentration below the 213 standard in SW-01 and SW-02. No other
VOCs were detected at concentrations above their respective MDLs in either the upstream or
downstream surface water samples.
3.3 Leachate
Seven VOCs (1,4-dichlorobenzene [3.7 pg/L]; acetone [6.0 pg/L]; benzene [1.7 pg/L]; chlorobenzene
[3.8 pg/L]; ethylbenzene [1.6 pg/L]; o-xylene [1.1 pg/L]; toluene [estimated 0.39 pg/L]; and total
xylenes [1.7 pg/L]) were detected in the leachate sample (LT-01).
On September 1, 2012, leachate extraction was initiated following installation of leachate extraction
pumps in the 10 landfill gas extraction wells at the Site (Figure 2). Due to a temporary malfunction
with the leachate flow meter, an accurate calculation of cumulative leachate removed can no longer
be obtained. Therefore, the total volume of leachate removed since September 2012 is not known.
However, based on readings taken from the leachate totalizer during the October 2019 monitoring
events, approximately 261,250 gallons of leachate were discharged through a permanent connection
to the TWSA between October 18, 2018, and October 22, 2019 (Table 4).
In fall 2013, the active portion of the approved corrective action remedy was initiated. Based on the
leachate analytical results for the sample collected on October 22, 2019, Anchor QEA estimates that
approximately 0.04 pound of VOCs was removed with the extracted leachate between the October
2018 and the October 2019 sampling events. Mass removal calculations are included in Table 4.
3.4 Domestic Well
The following sections summarize measured field parameters and analytical results associated with
the domestic well water sample collected during the fall 2019 sampling event.
3.4.7 Field Parameters
The pH reading for the domestic well sample (DW-01) was 6.85 SU, which is within the 2L standard
range of 6.5 to 8.5 SU.
Turbidity measured in DW-01 was 2.39 NTUs. DO was measured at a concentration of 5.57 mg/L in
DW-01. SC and ORP values in DW-01 were recorded at 79.2 pS/cm and 116.6 mV, respectively. These
parameters do not have established water quality standards.
3.4.2 VOCs
No VOCs were detected at concentrations above their respective MDLs in the domestic well water
samples.
Fall 2019 Semiannual
Water Quality Monitoring Report 11 January 2020

3.5 Groundwater Flow Directions
Groundwater levels in the saprolite, PWR, and bedrock are monitored at the Site. Three of the
bedrock monitoring wells (MW-01, MW-02, and MW-06) are located in the northern and
northwestern portions of the Site (Figure 3; Table 2). The fourth bedrock monitoring well (MW-07) is
located southwest of the landfill (Figure 3). The fall 2018 water level data collected from these four
bedrock wells were used to determine the generalized bedrock groundwater flow direction, which is
to the southwest (Figure 3).
PWR monitoring well MW-03 and saprolite monitoring wells MW-04 and MW-05R (Figure 3) are
located in the south-central and southern parts of the landfill, respectively. The fall 2019 water level
data collected from monitoring wells MW-03, MW-04, and MW-05R (Table 2) indicate that
groundwater flow direction in the combined saprolite and PWR zones is generally to the south-
southwest, toward the Tuckasegee River (Figure 3).
Fall 2019 Semiannual
Water Quality Monitoring Report 12 January 2020

4 Summary
The second semiannual water quality monitoring event of 2019 for the Jackson County closed
MSWLF was performed on October 22, 23, and 24, 2019. Appendices A and B and Table 3 provide
detailed analytical results and field data summarizing the groundwater, surface water, and leachate
quality at the landfill.
4.1 Groundwater Quality
4.7.7 Metals
Two metals (cobalt and vanadium) were detected at concentrations above their associated
groundwater quality standards in one or more of the monitoring wells (Table 3). Cobalt
concentrations exceeded its 2L standard in all of the collected groundwater samples. These results
are consistent with historical data.
4.7.2 Volatile Organic Compounds
Four VOCs (1,4-dichlorobenzene; benzene; vinyl chloride; and 1,4-dioxane) were detected at
concentrations above their respective 2L standards (Table 3) in one or more monitoring wells.
Concentration -versus -time graphs were created for samples from monitoring wells that had VOC
concentrations above their 2L standards, with the exception of 1,4-dioxane. The graphs are provided
as Figures 4 through 9.
4.7.3 Field Parameters and Other Constituents
Six of the seven of the samples collected from the monitoring wells had pH readings outside of the
2L standard range (6.5 to 8.5 SU). These results are consistent with historical data and are
characteristic of the natural groundwater quality of the region. Turbidity readings ranged from 2.14
NTUs (MW-06) to 127 NTUs (MW-05R).
Natural attenuation parameters (alkalinity, BOD, COD, chloride, carbon dioxide, hydrogen, ferrous
iron, methane, nitrate, sulfate, and TOC) were detected at various concentrations in groundwater
samples collected from one or more of the monitoring wells. Natural attenuation parameters are
being monitored to fulfill CAP requirements; further evaluation of these parameters will be
performed in the second Five -Year CAER (scheduled for 2021).
4.2 Surface Water Quality
No metals were detected at or above the applicable 2B standards for surface water during this
monitoring event. Concentrations in the upstream sample exceeded concentrations in the
downstream sample for all metals that were detected. No VOCs were detected at or above the
applicable surface water standards. Field parameters measured in both surface water samples,
Fall 2019 Semiannual
Water Quality Monitoring Report 13 January 2020

including pH, turbidity, and DO, were within the 2B standards established for these parameters.
Based on these data, the groundwater migrating from the landfill toward the Tuckasegee River does
not appear to be impacting surface water quality with regard to metals and VOCs.
4.3 Leachate Quality
The leachate sample (LT-01) was collected from the flow equalization tank and analyzed for
Appendix I VOCs and metals. Seven VOCs were detected in the leachate sample (Table 3). There are
no established water quality standards for leachate.
4.4 Domestic Well Water Quality
No VOCs were detected at concentrations above their respective MDLs in the domestic well water
samples.
Fall 2019 Semiannual
Water Quality Monitoring Report 14 January 2020

5 Future Activities
Anchor QEA will continue to monitor the water quality on a semiannual basis at the Jackson County
closed MSWLF. During spring 2020, domestic well owners will be contacted, and groundwater
samples will be collected from domestic wells if permitted by the well owner, and if possible, based
on well pump operability. Domestic well samples will be analyzed for VOCs only. Samples will be
collected from the monitoring wells, surface water monitoring points, and leachate flow equalization
tank during spring and fall 2020. In addition to the natural attenuation parameters that were added
to the monitoring requirements as part of the CAP, the analytical suites associated with the current
and future sampling events are outlined in the 2011 CAP (Altamont 2011) and the first Five -Year
CAER (Altamont 2016). The upcoming sampling event parameters are as follows:
Sampling Event
Spring 2020
Analytical Suite
(not inclusive of natural attenuation parameters)
Appendix I VOCs (including 1,4-dioxane)
Appendix I Metals
Sulfide
Appendix II VOCs (including 1,4-dioxane)
Appendix II Metals
Fall 2020 Appendix II Herbicides
Appendix II Pesticides
Appendix II SVOCs
Sulfide
J
Fall 2019 Semiannual
Water Quality Monitoring Report 15 January 2020

6 References
Altamont (Altamont Environmental, Inc.), 2010. Assessment of Corrective Measures. Prepared for the
North Carolina Department of Environment and Natural Resources. September 7, 2010.
Altamont, 2011. Corrective Action Plan. Prepared for the North Carolina Department of Environment
and Natural Resources. June 30, 2011.
Altamont, 2016. Five -Year Corrective Action Evaluation Report. Prepared for the North Carolina
Department of Environmental Quality. October 31, 2016.
DEN (North Carolina Department of Environmental and Natural Resources), 2011. Letter to:
Altamont Environmental, Inc. Regarding: Approval of the County's Corrective Action Plan.
September 1, 2011.
DENR, Division of Waste Management), 2014. Memorandum Re: Groundwater, Surface Water, Soil,
Sediment, and Landfill Gas Electronic Document Submittal, November 5, 2014.
DEQ (North Carolina Department of Environmental Quality), 2018a. Memorandum to: Solid Waste
Directors, Landfill Owners/Operators, and North Carolina Certified Laboratories. Regarding:
1,4-Dioxane Analysis, Solid Waste Section Limits, and Laboratory Analytical Methods.
May 29, 2018.
DEQ, 2018b. "Groundwater Protection Compliance Standards — Constituents List". Last modified
October 15, 2018. Available at:
https:Hedocs.deq.nc.gov/WasteManagement/0/edoc/l 257181/SWS_EnviroMonitoring_Const
ituents_List.pdf?searchid=13f8efb1-eel 1-485a-b03f-718f2287b271
EPA (U.S. Environmental Protection Agency), 1996. Low -Flow (Minimal Drawdown) Ground -Water
Sampling Procedures. OSWER, EPA/540/5-95/504.
EPA, 2017. Science and Ecosystem Support Division. Operating Procedure: Groundwater Sampling.
April 26, 2017.
Fall 2019 Semiannual
Water Quality Monitoring Report 16 January 2020

Tables

Table 1
Summary of Laboratory Analyses Performed on Samples
Groundwater Samples
Analysis
Metals
Mercury
VOCS
SVOCS
- ioxane
Sample Name
Date
Collected
EPA 6020B
EPA 7470A
EPA 8260D
EPA 8270E
EPA 8260SIM
MW-01
10/24/2019
X
X
X
X
X
MW-02
10/23/2019
X
X
X
X
X
MW-03
10/23/2019
X
X
X
X
X
MW-04
10/22/2019
X
X
X
X
MW-05R
10/23/2019
X
X
X
X
X
MW-06
10/23/2019
X
X
X
X
X
MW-07
10/22/2019
X
X
X
X
Surface Water, Leachate, Domestic Well, and Quality Control Samples
Analysis
Metals
Mercury
VOCs
- ioxane
SVOCS
Hardness
Sample Name
Date
Collected
EPA 6020B
EPA 7470A
EPA 8260D
EPA 524.2
EPA 8260SIM
EPA 8270E
SM 2340C
DW-01
10/24/2019
X
SW-01
10/22/2019
X
X
X
X
X
X
SW-02
10/22/2019
X
X
X
X
X
X
LT-01
10/22/2019
X
X
Trip Blank (1)
10/22/2019
X
X
Trip Blank (2)
10/23/2019
X
X
Trip Blank (3)
10/24/2019
X
X
Trip Blank (DW)
10/24/2019
Groundwater Samples: Natural Attenuation Parameters
Analysis
Total
Alkalinity
to pH 4.5
BOD
COD
Volatile Fatty
Acids
Ferrous Iron
Nitrate
as N
Chloride
Sulfate
TOC
Sulfide
Ethane,
Ethene,
Methane
Hydrogen
Carbon
Dioxide
Sample Name
Date
Collected
SM 2320B
SM 5210B
SM 5220D
AM23G
SM 3500-Fe D
EPA 9056A
SM 5310B
SM4500-S F
AM20GAX
MW-01
10/24/2019
X
X
X
X
X
X
X
X
X
X
X
X
MW-02
10/23/2019
X
X
X
X
X
X
X
X
X
X
X
X
MW-03
10/22/2019
X
X
X
X
X
X
X
X
X
X
X
X
X
MW-04
10/23/2019
X
X
X
X
X
X
X
X
X
X
X
X
X
MW-05R
10/23/2019
X
X
X
X
X
X
X
X
X
X
X
X
MW-06
10/22/2019
X
X
X
X
X
X
X
X
X
X
X
X
X
MW-07
01/00/1900
X
X
X
X
X
X
I X
X
X
X
X
X
X
Notes:
Appendix I constituents were analyzed per Title 40 Code of Federal Regulations, Part 258.
AM: Analytical Method
Blank cell: Analysis was not performed on that sample.
BOD: biochemical oxygen demand
COD: chemical oxygen demand
EPA: U.S. Environmental Protection Agency (method)
SIM: Selective Ion Monitoring
SM: Standard Method
SVOC: semivolatile organic compound
TOC: total organic carbon
VOC: volatile organic compound
Fall 2019 Semiannual Water Quality Monitoring Report Page 1 of 1
Jackson County Closed Municipal Solid Waste Landfill January 2020

Table 2
Well Construction Details and Corresponding Elevations
Depth to
Depth to
Elevation of
Ground
Depth To
Approximate
Approximate
Top of
Bottom of
Top Elevation
Bottom of
Surface
TOC
Stick Up
Total Well
Water
Depth to
Top of Bedrock
Screened
Screened
of Screened
Screened
Geology of
Source of Well
Elevation
Elevation
(feet
Depth
(feet below
Groundwater
Bedrock
Elevation
Interval
Interval
Interval
Interval
Screened
Construction
Facility Permit
Well ID
Date Drilled
(feet)
(feet)
above gs)
(feet bgs)
TOC)
Elevation (feet)
(feet bgs)
(feet)
(feet bgs)
(feet bgs)
(feet)
(feet)
Interval
Information
MW-01
04/23/1992
2,169.40
2,171.42
2.0
110.5
94.85
2,076.57
83.0
2,086.40
95.0
110.0
2,074.40
2,059.40
Bedrock
MW-02
04/22/1992
2,013.15
2,015.38
2.3
60.7
43.09
1,972.29
13.0
2,000.15
45.0
60.0
1,968.15
1,953.15
Bedrock
Partially
S&ME, Inc.
MW-03
04/21/1992
2,044.16
2,045.53
1.3
65.5
48.60
1,996.93
57.0
1,987.16
48.5
63.5
1,995.66
1,980.66
50-02
Weathered Rock
MW-04
04/21/1992
1,978.68
1,980.77
1 2.0
43.0
26.86
1,953.91
NA
NA
25.0
40.0
1,953.68
1,938.68
Saprolite
MW-05R
01/26/2012
2,027.98
2,030.95
2.8
54.0
47.14
1,983.81
NA
NA
44.0
54.0
1,983.98
1,973.98
Saprolite
Altamont
MW-06
03/23/2004
2,136.58
2,139.57
3.0
94.0
78.77
2,060.80
47.6
2,088.98
84.6
94.6
2,051.98
2,041.98
Bedrock
Environmental, Inc.
MW-07
07/30/2010
1,978.71
1,981.29
2.6
95.0
32.66
1,948.63
44.0
1,935.00
70.0
95.0
1 1,908.71
1,883.71
Bedrock
Notes:
Elevations associated with wells MW-01, MW-02, MW-03, MW-04, and MW-06 are measured relative to mean sea level and are based on surveying completed by Davenport & Associates, Inc.
Elevations associated with wells MW-05R and MW-07 are measured relative to horizontal North American Datum 83 and are based on surveying completed by Wes Cole Land Surveying, PA.
Depth to water was measured on October 22, 23, and 24, 2019.
Depth to bedrock and screened interval for MW-01 through MW-04 was taken from S&ME, Inc., boring logs completed April 21 through 23, 1992.
Depth to bedrock and screened interval for MW-06 was taken from an Altamont Environmental, Inc., boring log completed March 23, 2004.
Depth to bedrock and screened interval for MW-07 was taken from an Altamont Environmental, Inc., boring log completed July 30, 2010.
Death to bedrock and screened interval for MW-05R was taken from an Altamont Environmental, Inc., borina lop completed January 26, 2012.
Monitoring well MW-05 was abandoned on January 26, 2012, by NYEG Drilling, LLC. Monitoring well MW-05R was installed by NYEG Drilling, LLC, on January 26, 2012, as a replacement to MW-05.
Monitoring well MW-05R was surveyed by Wes Cole Land Surveying, PA, on September 28, 2012.
bgs: below ground surface
gs: ground surface
NA: not applicable
TOC: top of casing
Fall 2019 Semiannual Water Quality Monitoring Report Page 1 of 1
Jackson County Closed Municipal Solid Waste Landfill January 2020

Table 3
Summary of Analytical Results
Lab Certification
Lab Method
Metals
402
EPA 602013, 7470A
EPA 200.7
Parameter
v
'C
L
Q
_
a
CO
3
'E
a
V
=
•O
L.
V
=
o
V
i
o
V
a
Y
"
Z
E
•�
a
to
H
>
N
&A
a
C
2
CAS Number
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7440-48-4
7440-50-8
7439-92-1
7440-02-0
7782-49-2
7440-31-5
7440-62-2
7440-66-6
NE
SWS ID
14
1s
34
51
53
54
131
152
183
195
209
213
NE
Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
Sample Name
Collect Date
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Groundwater Samples
MW-01
10/24/2019
0.34 U
120
0.22 U
0.90 U
150
4.7 U
0.44 U
17
0.98 U
1.9 U
1.5 U
22
NA
MW-02
10/23/2019
1.3
76
0.22 U
7.7
12
7.2 J
2.0
4.9
3.2 J
1.9 U
11
35
NA
MW-03
10/23/2019
0.62 J
200
0.42 J
2.5 J
12
7.7 J
0.44 U
17
0.98 U
3.6 J
1.5 U
21
NA
MW-04
10/22/2019
0.34 U
92
0.24 J
0.90 U
2.0
4.7 U
0.44 U
1.7 J
1.0 J
3.2 J
1.5 U
15 J
NA
MW-05R
10/23/2019
0.42 J
120
0.60 J
0.90 U
10
4.7 U
0.44 U
4.3
0.98 U
1.9 U
1.5 U
17 J
NA
MW-06
10/23/2019
0.34 U
57
0.34 J
0.90 U
6.8
4.7 U
0.44 U
14
0.98 U
4.9 J
1.5 U
24
NA
MW-07
10/22/2019
0.34 U
450
0.22 U
0.90 U
1.3 J
4.7 U
0.44 U
7.1
0.98 U
1.9 U
1.5 U
21
NA
Leachate Sample
LT-01
10/22/2019
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Surface Water Samples
SW-01
10/22/2019
0.34 U
19
0.22 U
0.90 U
0.70 U
4.7 U
0.44 U
0.83 U
0.98 U
1.9 U
1.5 U
16 J
13,000
SW-02
10/22/2019
0.34 U
18
0.22 U
0.90 U
0.70 U
4.7 U
0.44 U
0.83 U
0.98 U
1.9 U
1.5 U
17 J
15,000
Domestic Well Sample
DW-01
10/24/2019
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Quality Control Samples
Trip Blank (1)
10/22/2019
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Trip Blank (2)
10/23/2019
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Trip Blank (3)
10/24/2019
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Trip Blank (DW)
10/24/2019
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
MDL
0.34
3.2
0.22
0.90
0.70
4.7
0.44
0.83
0.98
1.9
1.5
10
35
Laboratory and
Regulatory
MRL
1.0
10
1.0
3.0
2.0
10
1.0
3.0
5.0
5.0
5.0
20
910
Thresholds
2L
10
700
2
10
NE
1,000
15
100
20
NE
0.03
1,000
NE
IMAC
NE
NE
NE
NE
1
NE
NE
NE
NE
2000
NE
NE
NE
213
10
21,000
0.10*
14.81*
4
1.67*
0.28*
9.86*
5
770
NE
22.15*
NE
Fall 2019 Semiannual Water Quality Monitoring Report Page 1 of 5
Jackson County Closed Municipal Solid Waste Landfill January 2020

Table 3
Summary of Analytical Results
Volatile Organic Compounds
Lab Certification
402, 618
EPA 8260D, 524.2
EPA 8260SIM
Lab Method
v
a
�
d
a,
N
s
t
N
Gr
y
O
0
C
N
M
i
d
O
O
O
N
N
O
t
t
d
=
r
O
O
O
'a
O
a
O
as+
y
v
N
N
O
i
+'
Gl
02
C
v
v
O
O
N
X
G
O
Gi
CGi
0O
Parameter
N
OO
6-
X
i
a
i
o
_
AN
�+
Q
ca
V
W
E
z
o
>
x
108-38-3/
CAS Number
75-34-3
106-46-7
67-64-1
71-43-2
108-90-7
74-87-3
156-59-2
100-41-4
106-42-3
91-20-3
95-47-6
127-18-4
109-99-9
108-88-3
79-01-6
75-01-4
1330-20-7
123-91-1
SWSID
75
71
3
16
39
137
78
110
359
148
408
192
458
196
201
211
346
10
Units
pg/L
pg/L
I pg/L
Ng/L
pg/L
pg/L
pg/L
pg/L
pg/L
Ng/L
Ng/L
Ng/L
pg/L
pg/L
pg/L
I pg/L
pg/L
pg/L
Sample Name
Collect Date
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Groundwater Samples
MW-01
10/24/2019
2.3
8.0
31
1.6
1.8
0.29 U
4.7
0.31 U
1.0
1.5
0.40 J
0.37 J
0.68 U
0.35 U
0.47 J
0.41 U
1.4 J
0.14 U
MW-02
10/23/2019
0.29 U
0.42 U
2.3 J
0.34 U
0.34 U
0.29 U
0.44 J
0.31 U
0.73 U
0.67 J
0.40 U
0.31 U
0.68 U
0.35 U
0.46 U
0.41 U
1.1 U
4.0
MW-03
10/23/2019
0.30 J
2.9
3.4 J
0.66
6.3
0.29 U
0.96
0.31 U
0.73 U
0.45 U
0.40 U
0.31 U
0.68 U
0.35 U
0.46 U
0.41 U
1.1 U
5.6
MW-04
10/22/2019
0.29 U
2.0
3.3 J
0.34 U
1.5
0.29 U
0.74
0.31 U
0.73 U
0.45 U
0.40 U
0.31 U
0.68 U
0.35 U
0.46 U
0.41 U
1.1 U
5.4
MW-05R
10/23/2019
0.29 U
7.9
5.7
2.1
9.7
0.29 U
4.7
0.31 U
0.73 U
0.45 U
0.40 U
0.31 U
7.7 J
0.35 U
0.46 U
1.8
1.1 U
5.8
MW-06
10/23/2019
1.6
2.1
3.5 J
0.34 U
0.34 U
0.29 U
1.2
0.31 U
0.73 U
0.45 U
0.40 U
0.31 U
0.68 U
0.35 U
0.46 U
0.41 U
1.1 U
0.14 U
MW-07
10/22/2019
0.29 U
4.4
4.5 J
1.2
4.4
0.29 U
2.2
0.31 U
0.73 U
0.45 U
0.40 U
0.31 U
0.68 U
0.35 U
0.46 U
0.41 U
1.1 U
18
Leachate Sample
LT-01
10/22/2019
0.29 U
3.7
6.0
1.7
3.8
0.29 U
0.40 U
1.6
0.73 U
0.45 U
1.1
0.31 U
0.68 U
0.39 J
0.46 U
0.41 U
1.7
NA
Surface Water Samples
SW-01
10/22/2019
0.29 U
0.42 U
4.8 J
0.34 U
0.34 U
0.29 U
0.40 U
0.31 U
0.73 U
0.45 U
0.40 U
0.31 U
0.68 U
0.35 U
0.46 U
0.41 U
1.1 U
0.14 U
SW-02
10/22/2019
0.29 U
0.42 U
3.9 J
0.34 U
0.34 U
0.29 U
0.40 U
0.31 U
0.73 U
0.45 U
0.40 U
0.31 U
0.68 U
0.35 U
0.46 U
0.41 U
1.1 U
0.14 U
Domestic Well Sample
DW-01
1 10/24/2019
0.5 U
0.5 U
NA
0.5 U
0.5 U
NA
0.5 U
0.5 U
NA
NA
NA
0.5 U
NA
0.5 U
0.5 U
0.5 U
1 U
NA
Quality Control Samples
Trip Blank (1)
10/22/2019
0.29 U
0.42 U
2.7 J
0.34 U
0.34 U
0.57
0.40 U
0.31 U
0.73 U
0.45 U
0.40 U
0.31 U
0.68 U
0.35 U
0.46 U
0.41 U
1.1 U
0.14 U
Trip Blank (2)
10/23/2019
0.29 U
0.42 U
2.7 J
0.34 U
0.34 U
0.29 U
0.40 U
0.31 U
0.73 U
0.45 U
0.40 U
0.31 U
0.68 U
0.35 U
0.46 U
0.41 U
1.1 U
0.14 U
Trip Blank (3)
10/24/2019
0.29 U
0.42 U
2.6 J
0.34 U
0.34 U
0.29 U
0.40 U
0.31 U
0.73 U
0.45 U
0.40 U
0.31 U
0.68 U
0.35 U
0.46 U
0.41 U
1.1 U
0.14 U
Trip Blank (DW)
10/24/2019
0.5 U
0.5 U
NA
0.5 U
0.5 U
NA
0.5 U
0.5 U
NA
NA
NA
0.5 U
NA
0.5 U
0.5 U
0.5 U
1 U
NA
MDL
0.29
0.42/0.25
0.70
0.34/0.25
0.34/0.25
0.29
0.4 / 0.25
0.31 / 0.25
0.73
0.45
0.40
0.31 / 0.25
0.68
0.35 / 0.25
0.46 / 0.25
0.41 / 0.39
1.1 / 0.25
0.14
Laboratory and
M RL
0.5
0.5/0.5
5.0
0.5/0.5
0.5/0.5
0.5
0.5/0.5
0.5/0.5
1.0
1.0
0.5
0.5/0.5
10
0.5/0.5
0.5/0.5
0.5/0.5
1.5 / 1.0
2.0
Regulatory
Thresholds
2L
6
6
6,000
1
50
3
70
600
NE
6
NE
0.7
NE
600
3
0.03
500
3
IMAC
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
213
100
1 900
1 2,000
1 51
1 800
1 2.6
720
97
670
12
600
120
110,000
11
30
2.4
670
80
Fall 2019 Semiannual Water Quality Monitoring Report Page 2 of 5
Jackson County Closed Municipal Solid Waste Landfill January 2020

Table 3
Summary of Analytical Results
Lab Certification
Lab Method
SVOC
562
Natural Attenuation Parameters
402,618
EPA 8270D, 8270E
SM 2320B
SM 5210B
EPA 9056A
SM 5220D
SM 3500-Fe-D
EPA 9056A
EPA 9056A
SM4500-S F
SM 5310 B
AM23G
Parameter
d
d
c
o
v
Q
a
�
s
a
v
+�
m u,
a
stA
L
Q
Z
Z
=i
o
r
Q
O
CO
O
s
V
Q
O
V
Li
C
o
=
Z
VI
fC
�
Z
{A
3
H
6J
O
Q
d
V
Q
Q
•i
r
0
CO
Q
.
o
LL
CAS Number
106-46-7
117-81-7
84-66-2
91-20-3
SW337
SW316
16887-00-6
SW317
NA
SW303
14808-79-8
184-96-258
C-012
64-19-7
107-92-6
64-18-6
SWSID
71
111
90
166
337
316
301
317
334
303
315
187
357
NE
NE
NE
Units
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
pg/L
mg/L
mg/L
mg/L
mg/L
Sample Name
Collect Date
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Groundwater Samples
MW-01
10/24/2019
6.6 J
1.4 J
0.82 U
1.2 J
91,000
8,400
1500
53,000
34,000 HT
54 U
480 U
16,000
17.7
0.36
0.10 U
0.50 U
MW-02
10/23/2019
1.4 U
1.4 U
0.82 U
1.2 U
46,000
210 U BB
27,000
19,000 J
51 U HT
170 J
21,000
830 U
5.24
0.35
0.10 U
0.50 U
MW-03
10/23/2019
1.4 U
1.4 U
1.3 J
1.2 U
78,000
210 U BB
31,000
23,000 J
51 U HT
7,600
4,400
35,000
11.0
0.10 U
0.10 U
0.50 U
MW-04
10/22/2019
NA
NA
NA
NA
100,000
820 BB, J, B
47,000
10,000 U
51 U HT
5,300
78,000
11,000
5.91
0.10 U
0.10 U
0.50 U
MW-05R
10/23/2019
5.0 J
1.4 U
0.82 U
1.2 U
260,000
18,000 BB, B
61,000
58,000
2,000 HT
1101
480 U
30,000
18.0
0.56
0.10 U
0.50 U
MW-06
10/23/2019
1.4 U
1.4 U
2.3 J
1.2 U
24,000
210 U BB
1,100
10,000 U
51 U HT
240
710 J
30,000
8.18
0.10 U
0.10 U
0.50 U
MW-07
10/22/2019
NA
NA
NA
NA
240,000
1,700 BB, J, B
75,000
13,000 J
74 HT, J
110.1
22,000
12,000
10.6
0.10 U
0.10 U
0.50 U
Leachate Sample
LT-01
10/22/2019
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Surface Water Samples
SW-01
10/22/2019
1.4 U
1.4 U
0.82 U
1.2 U
NA
NA
NA
NA
NA
NA
NA
1,200 J
NA
NA
NA
NA
SW-02
10/22/2019
1.4 U
1.4 U
0.82 U
1.2 U
NA
NA
NA
NA
NA
NA
NA
830 U
NA
NA
NA
NA
Domestic Well Sample
DW-01
10/24/2019
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Quality Control Samples
Trip Blank (1)
10/22/2019
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Trip Blank (2)
10/23/2019
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Trip Blank (3)
10/24/2019
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Trip Blank (DW)
10/24/2019
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
MDL
1.4
1.40
0.82
1.20
770
210
380
10,000
51
54
480
830
0.3 / 0.6
0.025
0.0070
0.098
Laboratory and
Regulatory
MRL
10
20
10
10
5,000
2,000
1,000
50,000
5,000
200
2,000
2,000
2/4
0.1
0.1
0.5
Thresholds
2L
6
3
6,000
6
NE
NE
250,000
NE
NE
NE
250,000
NE
NE
NE
NE
NE
IMAC
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
5,000
NE
NE
2B
900
5
600
12
20,000
NE
230,000
NE
1,000
NE
NE
NE
NE
NE
NE
NE
Fall 2019 Semiannual Water Quality Monitoring Report Page 3 of 5
Jackson County Closed Municipal Solid Waste Landfill January 2020

Table 3
Summary of Analytical Results
Lab Certification
Lab Method
Natural Attenuation Parameters
402, 618
Field Parameters
5445 (pH only)
AM20GAX
Parameter
N
O
s
a,
2
c
41
W
c
41
W
a
X
O
=
o
m
V
N
0
>+
2
a
°1
%
0
y
>
c
"
G
i
3
i
0
H
+�+
?
W
C
O
0
v
a
{n
O
0
+.
U
C
O
x o
O O.
=
H
CAS Number
74-82-8
74-84-0
74-85-1
124-38-9
1333-74-0
7782-44-7
SW325
SW323
SW336
SW320
SW330
SWS ID
456
332
331
459
420
356
325
323
336
320
NE
Sample Name
Units
pg/L
pg/L
pg/L
mg/L
nM
mg/L
°C
PS/Cm
mV
SU
NTU
Collect Date
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Groundwater Samples
MW-01
10/24/2019
740
0.10 U
0.10 U
150
NA
5.11
14.9
227.7
52.1
6.00
15.1
MW-02
10/23/2019
0.50 U
0.10 U
0.10 U
49
NA
10.45
13.5
216.6
123.1
6.34
13.8
MW-03
10/23/2019
15
0.010 U
0.027
260
21
0.83
15.2
362.2
263.7
5.87
18.6
MW-04
10/22/2019
110
0.014
0.010 U
330
100
6.42
16.0
556.1
359.4
5.89
2.93
MW-05R
10/23/2019
3400
0.32
0.15
58
NA
1.51
17.9
701
-55.5
7.02
127
MW-06
10/23/2019
14
0.010 U
0.034
250
14
3.24
16.1
68.3
301.9
5.34
2.14
MW-07
10/22/2019
47
0.020
0.065
490
3.4
1.16
16.1
740
193.8
6.11
5.62
Leachate Sample
LT-01
10/22/2019
NA
NA
NA
NA
NA
3.90
26.1
3,303
-16.7
6.95
15.1
Surface Water Samples
SW-01
10/22/2019
NA
NA
NA
NA
NA
10.54
17.5
38.6
190.3
7.44
8.00
SW-02
10/22/2019
NA
NA
NA
NA
NA
10.02
18.3
38.5
188.5
7.43
6.31
Domestic Well Sample
DW-01
10/24/2019
NA
NA
NA
NA
NA
5.57
16.0
79.2
116.6
6.85
2.39
Quality Control Samples
Trip Blank (1)
10/22/2019
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Trip Blank (2)
10/23/2019
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Trip Blank (3)
10/24/2019
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Trip Blank (DW)
10/24/2019
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
Laboratory and
Regulatory
Thresholds
MDL
0.022 / 0.094
0.003 / 0.011
0.005 / 0.008
0.47 / 0.82
0.75 / 7.5
NA
NA
NA
NA
NA
NA
MRL
0.1 / 0.5
0.01 / 0.1
0.01 / 0.1
2/5
1 / 10
NA
NA
NA
NA
NA
NA
2L
NE
NE
NE
NE
NE
NE
NE
NE
NE
6.5-8.5
NE
IMAC
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
2B
NE
NE
NE
NE
NE
> 5.0
NE
NE
NE
6.0-9.0
<_ 50
Fall 2019 Semiannual Water Quality Monitoring Report Page 4 of 5
Jackson County Closed Municipal Solid Waste Landfill January 2020

Table 3
Summary of Analytical Results
Notes:
Only results, MDLs, MRLs, certification numbers, and methods for detected constituents are listed in this table. Please refer to the Prism Report of Laboratory Analysis for further details.
°C: degrees Celsius
Ng/L: micrograms per liter
pS/cm: microsiemens per centimeter
213: surface water standard per North Carolina Administrative Code (NCAC), Title 15A: Department of Environmental Quality, Subchapter 213: Surface Water and Wetland Standards (last amended June 2016). Where no 2B standard exists, the most stringent, applicable standards were
selected from the EPA Nationally Recommended Water Quality Criteria for Aquatic Life and Human Health or the North Carolina Protective Values for Surface Waters (current as of September 22, 2017).
2L: groundwater standard per NCAC, Title 15A: Department of Environmental Quality, Subchapter 2L: Groundwater Classifications and Standards (amended April 1, 2013)
B: a laboratory data qualifier used for parameters that were detected in the associated laboratory blank at a concentration greater than one half of the reporting limit
BB: a laboratory data qualifier used to indicate the blank is outside the control limits, but the validity of the data is not affected
BOD: biochemical oxygen demand
CAS Number: a unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters
COD: chemical oxygen demand
Collect Date: the date on which the sample was collected in the field
EPA: U.S. Environmental Protection Agency (Method)
HT: a laboratory data qualifier used to indicate the sample was received and analyzed outside of the hold time
IMAC: Interim Maximum Allowable Concentration. Analytes that do not have an established 2L standard were compared to the IMAC in accordance with 15A NCAC 02L .0202 (c).
J: a laboratory data qualifier used for parameters detected at estimated concentrations above the MDL, but below the MRL
Lab Method: the analytical method used to analyze the constituents
MDL: method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero
mg/L: milligrams per liter
MRL: method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method
mV: millivolt
NA: not analyzed
NE: not established
nM: nanomoles
NTU: Nephelometric Turbidity Units
Result: analytical data reported by the laboratory, or field data collected by Anchor QEA
Shaded cell indicates a result in exceedance of the 2L standard or IMAC, or greater than or equal to the GWPS (if no 2L or IMAC exists) and 2B standard, if applicable
SU: Standard Unit
SVOC: semivolatile organic compound
SWS ID: Solid Waste Section Identification Number
TOC: total organic carbon
U: a laboratory data qualifier used for parameters not detected at concentrations above the MDL
*: 2B surface water standard calculated using average analyzed hardness value (calculated from the upstream and downstream sampling location results) via the most stringent hardness -dependent metal calculation, per NCAC Title 15A: Department of Environmental Quality,
Subchapter 2B - Surface Water and Wetland Standards (last amended September 2017).
Fall 2019 Semiannual Water Quality Monitoring Report Page 5 of 5
Jackson County Closed Municipal Solid Waste Landfill January 2020

Table 4
Mass Removal Calculations for Volatile Organic Compounds (VOCs) Detected in the Leachate Sample (LT-01)
Sample Dates
Detected Volatile Organic
Compounds
Concentration
in LT-01
(mg/L)
Cumulative
Flow at Gauge
(gallons)
Differential
Flow
(gallons)
Mass
Removed
(pounds)
Estimated Cumulative
Mass Removed
(pounds)
Beginning
Ending
09/01/2012
10/25/2012
1,4-Dichlorobenzene
0.0034
11,500
11,500
0.00033
4-Meth I-2- entanone (MIBK)
0.0021
J
0.00020
Acetone
0.0292
0.00280
Benzene
0.0021
0.00020
Chlorobenzene
0.0029
0.00028
cis-1,2-Dichloroethene
0.00063
J
0.00006
Dichlorodifluoro-methane
0.00093
J
0.00009
Eth (benzene
0.0102
0.00098
Naphthalene
0.0069
0.00066
Styrene
0.00033
J
0.00003
Toluene
0.003
0.00029
X lene (Total)
10.0094
0.00090
Total
0.00682
0.00682
10/26/2012
04/11/2013
1,4-Dichlorobenzene
0.006
65,500
54,000
0.00270
Acetone
0.012
J
0.00540
Benzene
0.0011
0.00049
Carbon disulfide
0.0067
J
0.00301
Chlorobenzene
0.0024
J
0.00108
cis-1,2-Dichloroethene
0.00058
J
0.00026
Eth (benzene
0.0083
0.00373
Toluene
0.00059
J
0.00027
X lene (Total)
0.0078
0.00351
Total
0.02045
0.02727
04/12/2013
10/08/2013
1,4-Dichlorobenzene
0.0055
114,737
49,237
0.00226
4-Meth I-2- entanone (MIBK)
0.0012
J
0.00049
Benzene
0.0020
0.00082
Chlorobenzene
0.0039
0.00160
cis-1,2-Dichloroethene
0.00080
J
0.00033
Eth (benzene
0.0151
0.00619
Naphthalene
0.0184
0.00754
Toluene
0.0012
0.00049
X lene (Total)
0.0090
0.00369
Total
0.02341
0.05068
10/09/2013
04/08/2014
1,4-Dichlorobenzene
0.0056
168,821
54,084
0.00252
Benzene
0.0018
0.00081
Chlorobenzene
0.0051
0.00230
cis-1,2-Dichloroethene
0.00049
J
0.00022
Eth (benzene
10.0047
1
0.00212
Toluene
10.00041
1 J
0.00018
X lene (Total)
10.0021
1 J
0.00095
Total
0.00910
0.05978
04/08/2014
10/23/2014
1,4-Dichlorobenzene
0.0053
179,652
10,831
0.00048
Benzene
0.0014
0.00013
Chlorobenzene
0.003
0.00027
cis-1,2-Dichloroethene
0.00049
J
0.00004
Eth (benzene
0.0027
0.00024
Toluene
10.00051
1 J
0.00005
X lene (Total)
10.0014
1 J
0.00013
Total
0.00133
0.06111
10/23/2014
04/21/2015
1,2,3-Trimethyl benzene
0.00062
219,965
40,3 3
0.0002
1,2,4-Trimethyl benzene
0.00076
0.00026
2-Chlorotoluene
0.00067
0.00022
1,4-Dichlorobenzene
0.0059
0.00198
Acetone
0.00790
0.00265
Benzene
0.0022
0.00074
Chlorobenzene
0.003
0.00101
Eth (benzene
0.0056
0.00188
Isopropyl benzene
0.0013
0.00044
Methy Tert-but I -Ether
0.0013
0.00044
Na thalene
0.024
0.00806
n-Propylbenzene
0.00088
0.00030
Tetrah drofuran
0.089
0.02988
Toluene
0.00054
J
0.00018
Vin I Chloride
0.00038
0.000 3
X lene (Total)
10.0030
J
0.00101
TotaT
0.04937
0.11048
04/21/2015
10/13/2015
1,4-Dichlorobenzene
0.00600
256,685
36,720
0.00183
2-Butanone
0.00960
J
0.00294
Benzene
0.00210
0.00064
Chlorobenzene
0.0040
0.00122
Eth (benzene
0.00710
0.00217
m, -X lenes
0.0014
0.00043
Naphthalene
0.021
0.00642
o-X lene
0.0017
0.00052
Tetrah drofuran
0.062
0.01896
Toluene
0.00058
J
0.00018
Total X lenes
10.0031
J
0.00095
Total
0.03626
0.14674
Fall 2019 Semiannual Water Quality Monitoring Report Page 1 of 2
Jackson County Closed Municipal Solid Waste Landfill January 2020

Table 4
Mass Removal Calculations for Volatile Organic Compounds (VOCs) Detected in the Leachate Sample (LT-01)
Sample Dates
Detected Volatile Organic
Compounds
Concentration
in LT-01
(mg/L)
Cumulative
Flow at Gauge
(gallons)
Differential
Flow
(gallons)
Mass
Removed
(pounds)
Estimated Cumulative
Mass Removed
(pounds)
Beginning
Ending
10/13/2015
04/05/2016
1,4-Dichlorobenzene
0.00590
315,663
58,978
0.00290
Benzene
0.00170
0.00083
Chlorobenzene
0.0038
0.00187
Eth (benzene
0.00500
0.00246
m, -X lenes
0.0010
0.00049
o-X lene
0.0015
0.00074
Toluene
10.00063
J
0.00031
Total X lenes
10.0025
1 J
0.00123
Total
0.01082
0.15756
04/05/2016 10/11/20161 No detected compounds. 331,010 15,347
0.00000
Total
0.00000
0.15756
10/11/2016
03/21/2017
1,4-Dichlorobenzene
0.0046
334,212 3,202
0.00012
Acetone
0.0094
J
0.00025
Benzene
0.0015
0.00004
Chlorobenzene
0.0043
0.00011
Eth (benzene
0.0014
0.00004
m, -X lenes
0.0006
J
0.00002
o-X lene
0.00092
0.00002
Tetrah drofuran
0.066
0.00176
Total X lenes
0.0015
J
0.00004
Total
0.00241
0.15997
03/21/2017
10/11/2017
1,4-Dichlorobenzene
0.0041
364,760 30,548
0.00 04
Acetone
0.0067
J
1
1
0.00170
Acetonitrile
0.008
J
Benzene
0.00061
0.00016
Chlorobenzene
10.0012
1
0.00031
Eth (benzene
10.00087
1
0.00022
Naphthalene
10.0012
Tetrah drofuran
10.12
1
0.03053
Total
0.03630
0.19627
03/21/2018
10/18/2018
1,4-Dichlorobenzene
0.0028
1,784,710 159,341
0.00372
Acetone
0.017
0.02256
Benzene
0.0012
0.00159
Chlorobenzene
0.0024
0.00318
Eth (benzene
0.0018
0.00239
m, -X lenes
0.00038
J
0.00050
Methylene Chloride
0.00034
J
0.00045
o-X lene
0.00060
0.00080
X lenes, Total
0.00098
J
0.00130
Total
0.04
0.23
10/18/2018
10/22/2019
1,4-Dichlorobenzene
0.0037
2,045,960
261,250
0.00805
Acetone
0.006
0.01305
Benzene
0.0017
0.00370
Chlorobenzene
0.0038
0.00827
Eth (benzene
0.0016
0.00348
o-Xylene
0.00110
0.00239
Toluene
0.00039
J
0.00085
X lenes, Total
0.0017
J
0.00370
Total
0.04
0.28
Notes:
1. No VOCs were detected in the leachate sample collected during the October 2016 sampling event.
Only detected volatile organic compounds (VOCs) in leachate sample LT-01 are included in the mass removal calculation.
Leachate extraction at the landfill was initiated on September 1, 2012.
Extraction volume measurements were recorded and provided by Jackson County staff.
Anchor QEA bases mass removal calculations on the assumption that the VOCs concentration in one sampling event is representative of leachate quality until the next sampling event occurs,
and that the leachate removal system has a 100% removal and treatment efficiency.
Due to a malfunction with the leachate totalizer, cumulative flow values are only accurate through October 11, 2017. From October 18, 2018, forward, the indicated cumulative flow value is only
used to calculate the differential flow, and cannot be relied upon to accurately represent cumulative flow.
Represents the total flow between the LT-01 sample dates.
Estimated cumulative mass removed and treated is estimated based upon a conversion of milligrams to pounds and liters to gallons and the multiplication of the concentration by the
differential flow for the specified period.
Formula: ((concentration[mg/L])*(2.2e-6 Ib)/(0.264 gal))*(Differential flow). However, due to a failure of the leachate totalizer, the mass removed from October 11, 2017, through March 21, 2018,
is not known and is not included in the total mass removed.
mg/L: milligrams per liter
J: Indicates laboratory estimated concentration is above the adjusted method detection limit and below the adjusted reporting limit.
Fall 2019 Semiannual Water Quality Monitoring Report Page 2 of 2
Jackson County Closed Municipal Solid Waste Landfill January 2020

Figures

LI
UA
�� 1(� _'� � _., „� • `� +lf# III. ---• ��
� � r„ `L•i �:L.` �y��� f � i ///�/ it 2
\1 �JP\ f l
LEGEND: SOURCES:
1. BaUSGS Topographic Maps Greens
® Site Parcel Boundary Creekk and Whittier 7.5-minute Quadrangles
2. Parcel: Jackson County GIS
0 2,000
Feet
Publish Date: 2019/12/03, 11:47 AM I User: alesueur
Filepath:\\orcas\gisVobs\JacksonCounty_NC_1480\Maps\2019\FallWaterQuality\AQ_Fig01_JacksonCounty_FaIIWQ_SiteLocationMap.mxd
)P, ANCHOR Figure 1
Q E A Site Location Map
Fall 2019 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill

SW-02
`
r4u A "PG
LEGEND:
41- Monitoring Well — Road
Landfill Gas Extraction Well Elevation Contour (20-Foot Interval)
® Domestic Well Sample Location 0 Property Boundary
Leachate Sample Location and
Flow Equalization Tank
0 Surface Water Sample Location
M W -05 R ,j�
MW-07 M -04~ 40�, �
NOTE:
Sample locations are approximate.
SOURCES: 0
Aerial Imagery: Esri Online Services
Contours, Roads, and Parcels: Jackson County GIS
Publish Date: 2019/12/03, 11:58 AM I User: alesueur
Filepath:\\orcas\gis\Jobs\JacksonCounty_NC_1480\Maps\2019\FallWaterQuality\AQ_Fig02_JacksonCounty_FaIIWQ_SampleLocationMap.mxd
0 500
Feet
kZANCHOR Figure 2
QEA-- Site Layout Map
Anchor QEA of North Carolina, PLLC
Fall 2019 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill

LEGEND:
® Saprolite Monitoring Well — Stream
® PWR Monitoring Well — Road
® Bedrock Monitoring Well Elevation Contour (20-Foot Interval)
Property Boundary (1,996.93) Groundwater Elevation
(October 22, 23, and 24, 2019)
MW-02
972.29)
amm-nn
x�o
F o
�o
200, 2O2o
210C
2�4p
2120 aG"C'
O
ta\`��eGtOG�
t
Ge oq feat
Q� dot
•MW-03 0
(1,996.93) N
°AO °so d U
\ •N � m
3
9 tO?
MW-04
(1,953.91)
Wilkey
Gy Q
GCE
MW-05R
983�8/1)
/Z
NOTES:
1. Monitoring well locations are approximate.
2. Groundwater elevations and flow direction are updated on a semiannual basis following sample collection events
in March and October.
3. Groundwater flow direction is based on groundwater elevations from all Site monitoring wells. Direction is
calculated based on depth to water measured on October 22, 23, and 24, 2019.
4. Last names of property owners are shown in parcels that border the landfill property.
5. PWR: partially weathered rock
6. Groundwater elevation in feet (North American Vertical Datum 1988)
Publish Date: 2019/12/03, 12:05 PM I User: alesueur
Filepath:\\orcas\gis\lobs\JacksonCounty_NC_1480\Maps\2019\FallWaterQuality\AQ-Fig03_JacksonCounty_FaIIWQ_GroundwaterElevationMap.mxd
VIV
0
Wilkey
1 --ey-2-0
0
N
I ij
SOURCES:
1. Elevation contours, roads, and parcels: Jackson County GIS
2. Groundwater elevations: calculated from surveys
performed by Davenport & Associates, Inc. (MW-01, MW-02,
MW-03, MW-04, and MW-06) and Wes Cole Land Surveying,
PA (MW-05R and MW-07)
RD
0
0 200
Feet
N
0
Z}�
ANCHOR Figure 3
QEA—`-�" Generalized Groundwater Flow Direction
Anchor QEA of North Carolina, PLLC
Fall 2019 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill

Figure 4
Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time
(Monitoring Well MW-01)
20
18
16
IN
I
r- r- 00 00 M M O O N N ro rn Ln Ln l0 LD r— r W CO M M
O O O O O O O O O O O O O O O O O O O O O O O O O O
N N N N N N [V N N N N N cV N N N N N N N N N N N N N
a--L L a--L L L a--L a--L L a--L L �--L
Q U Q U Q U Q U U Q U Q U 0- U 0- U Q U 0- U � U � U M U
U
Q 0 Q 0 Q 0 Q 0 Q 0 Q 0 Q 0 Q 0 Q 0 Q 0 g 0 2 0 2 0
Notes:
1. 2L Standard = 6 micrograms per liter (µg/L )
2. "J' indicates result is estimated by laboratory.
3. "<" indicates result is less than method detection limit.
4. Oct 2017 result reported in semivolatile organic compound list.
Fall 2019 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02
Sampling Date
O 1,4-Dichlorobenzene
2L Standard
tGroundwater Elevation
2078
2076
2074
O
.a
2072 a,
W
L
a,
�a
3
2070 =
3
O
,L^
V
2068
2066
2064
January 2020

Figure 5
Hydrograph and Benzene Concentration vs. Time
(Monitoring Well MW-01)
12
IN
4
2
I
r- r` 00 00 M M O O N N M M Ln Ln l0 LD I� r 00 00 M M
O O O O O O O O O O O O O O O O O O O O O O O O O O
N N N N N N [V N N N N N N N N N N N N N N N N N N N
Q U Q U Q U Q U Q U U Q U 0-U 0-U Q U 0-U ro U M U M U
Q 0 Q 0 Q 0 Q 0 Q 0 Q 0 Q 0 Q 0 Q 0 Q 0 g 0 2 0 2 0
Notes:
1. 2L Standard = 1 microgram per liter (µg/L)
2. "J" indicates result is estimated by laboratory.
3. "U" indicates result is less than method detection limit.
Sampling Date
O Benzene
21- Standard
* Groundwater Elevation
2078.00
2076.00
2074.00
2072.00
2070.00
2066.00
2064.00
Fall 2019 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02 January 2020

Figure 6
Hydrograph and 1,4-Dichlorobenzene Concentration vs. Time
Monitoring Well MW-0511
12
It
I
N N m m v v
0 0 C. Co 0 0
N N N N N N
}+ L }+ U
Notes: Q 0 Q 0 Q 0
Constituent concentration after January 2012 was found in MW-05R.
Constituent concentration before January 2012 was found in MW-05.
Groundwater elevation in October 2011 was interpolated.
2L Standard = 6 µg/L
"J" indicates result is estimated by laboratory
"<" indicates result is less than method detection limit
Oct, 2017 result reported in semi -volatile organic compound list
Fall 2019 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02
it
u,
i2
r
r
o0
0o
rn rn
0
0
0
0
0
0
0
0
0 0
N
N
N
N
N
N
N
N
N N
Q
V
Q
V
(p
V
(6
V
(6 V
Sampling Date
1,4-Dichlorobenzene
2L Standard
--*—Groundwater Elevation
•::
•..
a�
1984
1978
1976
January 2020

Figure 7
Hydrograph and Benzene Concentration vs. Time
(Monitoring Well MW-SR)
3
2.5
1
0.5
0
N
N
m
m
�n
in
r
r`
D1 6l
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O O
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N N
Q
U
Q
U
Q
U
Q
U
Q
U
c6
U
cO
U
f6 U
Q
O
Q
O
Q
O
Q
O
Q
O
O
O
O
Notes: Sampling Date
1. 2L Standard = 1 microgram per liter (µg/L)
2. "J" indicates result is estimated by laboratory.
3. "<" indicates result is less than method detection limit.
Fall 2019 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02
Benzene
2L Standard
Groundwater Elevation
.;.
1987
1985
0
V
1983
W
L
GJ
r
M
1981
C
7
0
Q
1979
1977
1975
January 2020

Figure 8
Hydrograph and Vinyl Chloride Concentration vs. Time
(Monitoring Well MW-0511)
4
3.5
0.5
0
O
O
O
O
O
O
O
O
O
O
O
O
O
O
O O
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N N
Q
V
Q
V
Q
V
Q
V
Q
V
r6
V
c6
V
cp V
Q
0
Q
0
Q
0
Q
0
Q
0
0
0
0
Notes:
1. 2L Standard = 0.03 microgram per liter (µg/L)
2. "J" indicates result is estimated by laboratory.
3. "<" indicates result is less than method detection limit.
Fall 2019 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02
Sampling Date
IIIIIIIIIIIIIIIIIIIIIIIIIIIIVinyl Chloride
21- Standard
--*—Groundwater Elevation
•::
•:.
1984
1980
0
1978
1976
January 2020

Figure 9
Hydrograph and Benzene Concentration vs. Time
(Monitoring Well MW-7)
2
1.8
1.6
J
1.4
c
0
a 1.2
L
V
0 1
G!
C
0
N 0.8
C
OG
0.6
0.4
0.2
0
N N cn m - Ln Ln Q0 Q0 r r` 00 00 M 0')
O O O O O O O O O O O O O O O O O O
N N N N N rV N N N fV N lV rV N N fV N N
Q U Q U Q V Q V Q V Q V (6 V (6 V c6 V
Q O Q O Q O Q O Q O Q O O g O O
Notes:
1. 2L Standard = 1 microgram per liter (µg/L)
2. "J" indicates result is estimated by laboratory.
3. "<" indicates result is less than method detection limit.
Fall 2019 Semiannual Water Quality Monitoring Report
Jackson County Closed Municipal Solid Waste Landfill, Permit No. 50-02
Sampling Date
Benzene
2L Standard
Groundwater Elevation
1951
1950
a
a,
1950 0
W
L
GJ
ar
M
1949
C
7
0
L
0
1949
m
January 2020

Appendix A
Well Sampling Logs, and Equipment
Documentation and Instrument
Calibration Data Sheets

ANCHOR
QEA �`'`r"
Well Sampling Log
Date: j Well Name: ./[\V—[) I
Project Name:
��� (D Lr
Project Number.
�� �[.�`Q
Weather
Sampling Personnel:
LAY(,�
Sample Time:
Well Information:
Well Depth in Feet (WD): p
Well Diameter.
r�
Water Level in Feet (WL):!�
Type of Casing:
_
�v Ci
Length of Water Column: J r,64
feet
Screen Interval:
{tip]
(WD) - (WL) = (LWC)
Flush Mount / Stick-LI
ll
One Casing Volume: ..[. ,�
gallons
omments: , � : � I n (�
(LWC) x (WCV)
Three Casing Volumes: 7 g c��1 GI U
gallons
Tagged
Actual Volume Purged: ''�v (�
gallons
bottom at:
�—
Well Casing Volumes (WCV)
1" = 0.041 Gal/Ft" = 0. al/F 3" = 0.38 Gal/Ft 4" = 0.66 Gal/Ft 6" = 1.5 Gal/Ft 8" = 2.6 Gal/Ft 12" = 5.8 GaVR
Purge
i I
er-T to Dedicated Pump Whale Pump Grundfos Other.
Sample Method:
e -
ai -
Dedicated Pump Whale Pump Grundfos Other.
Oxidation
a Ions
Temp
Dissolved
I Specific Cond.
pH (S.U.)
Reduction
I Turbidity
Reading
Time
Purged
(°C)
Oxygen (mg/L)
(PS/cm)
report to 0.T S.U.
Potential (MV)
j (NTU)
Comments
1
lJ2
t•�ri,ki
1E
"e �
-1-V.`
-5-15B
4
1
a
w J
5
6
7
9
We
10
Notes:
Samples are analyzed immediately upon collection.
°C: degrees Celsius
pS/cm: micro-Siemen per centimeter
mg/L: milligrams per liter
mV: millivolt
NTU: nephelometric turbidity units
S.U.: Standard Units
Protective Casing: f Pad: " Lock: Vegetation: Access: I
Sampling Personnel Signature: +
Date: ro `?,At / L 9
initial if well information and sampling data has been verified _
well was tagged after sampling was complete

`IGVIv
ZANCHOR
QEA
Well Sampling Log
lop,3/1ci
Date. (617z1),1
Well Name: kw -OD -
Project Name:
�acye6vy-,
Project Number.
Cq q -
Weather.
Sampling Personnel:
MV,4v
Sample Time: 1017,6— olalw
Well Information:
Well Depth in Feet (WD):
Well Diameter.
Water Level in Feet (WL): 3,
Type of Casing:
CJ
Length of Water Column: 17. 6 i feet
Screen Intel' I.
(WD) - (WL) = (LWC)�
Flush Mount /
One Casing Volume: a,Vy gallons
Comments: �!
a lock—
(LWC) x (WCV)
_ _
Three Casing Volumes: q.00 gallons
Tagged _�—
Actual Volume Purged: ^4 gallons
bottom at:
Well Casing Volumes (WCV)
1" = 0.041 Gal/F 2" = 0.17 Gal/F 3" = 0.38 Gal/Ft 4" = 0.66 Gal/Ft 6" = 1.5 Gal/Ft 8" = 2.6 Gal/Ft 12" = 5.8 Gal/Ft
Purge Method:
iler-Disp. � Bailer -Teflon Dedicated Pump Whale Pump Grundfos Other.
Sample Method:
Bailer-Dis . Bailer -Teflon Dedicated Pump Whale Pump Grundfos Other.
Oxidation
Gallons
Temp
Dissolved
Specific Cond. pH (S.U.)
Reduction
Turbidity
Reading
Time
Purged
(°C)
Oxygen (mg/L)
(PS/cm) report to 0.1 S.U.
Potential (mV)
(NTU)
Comments
1
I
' r r�l
1H.4
Q
r
.fir
2-5,
,I
2
. vU
�F
S. 6
�. ►
'f•
1
4
75
r
.-
ram• � .��'
5
to
ro r
i
6.34
7. 1
6
7
8
9
10
Notes:
Samples are analyzed immediately upon collection.
°C: degrees Celsius
uS/cm: micro-Siemen per centimeter
mg/L: milligrams per liter
mv: millivolt
NTU: nephelometric turbidity units
S.U.: Standard Units
Protective Casing: [:G' Pad: - F- Lock:u W1 Vegetation: Access:C.,_�_`i
Sampling Personnel Signature:
Date: to
initial if well information and sampling data has been verified _
well was tagged after sampling was complete

ANCHOR
Low -Flow Sampling Log
Date: I 1,2,3+ `Gta Well Name: �AW -d__�?
Project Name:
a(16C(X) Co &:-
Project Number: l
•-C)(.0 i
Location:
_Da
Personnel:
CeWeather.
"V►1G
e'
Well Information:
Screen Interval:$,
Depth to Water:
Well Diameter:
Pump Intake:
Drawdown Set:
Used (circle):
Comments:
�j '" l0 �j �.� bgs Arrive at Well: 0r 50
1�o toc Start Time:
01 On in Sample Time:
toc Finish Sample Time: I D90
d toc Leave Well:
iktPump
Peristaltic Bladd Other (description):
��� � � Purge Rate: '
Total Purge Volume: �o.,)
Pump Speed: j
Time
DTW
(feet)
Temp
VQ
DO Specific Cond.
(mg/L) (pS)
pH (S.U.)
report to 0.1.
ORP
(m1)
Turbidity
(NTU)
Comments
as
� a
Amlaei
(�
a
yr
U
-,
443
I �:
i.
AG.ai]
�L
r
5 , -
L-
qrqb
!Time between recharge during sample collection:
Sampling Personnel Signature:
Date:
Notes:
Stabilization
3 successive readings, 3 minutes apart:
within +/- 10% DO and turbidity; +/- 3% Conductivity, +/- 0.1 PH unit; +/- 10 mV for ORP
from EPA - Low -Flow (Minimal Drowdown) Groundwater Sampling Procedures, April 1996 (Rev 2010)
Samples are analyzed immediately upon collection.
pS: micro-Siemen
°C: degrees Celsius
bgs: below ground surface
DO: dissolved oxygen
mg/L: milligrams per liter
mv: millivolt
NTU: nephelometric turbidity units
ORP: oxidation reduction potential
S.U.: standard units
toc: top of casing
initial if well information and sampling data has been verified
well was tagged after sampling was complete ��

lkzANCHOR
QEA
Low -Flow Sampling Log
Date: l r,l72f ►Cd Well Name: RA W-[A-
Project Name: _-5'0LC" J Project Number: Cr 0)
Location: XM (0a-D WC,
Personnel: DAYX . CP Weather: �iy(, S
Well Information: ��
Screen Interval: i bgs Arrive at Well:
Depth to Water: w%l for toc Start Time:
Well Diameter: in Sample Time:
Pump Intake: ZC3 toc Finish Sample Time:
Drawdown Set: 3 toc Leave Well: i
Pump Used (circle): Peristaltic Bladder Other (description):
Comments /(] p.-� .�rj r11LiZ�rCSeo�^�% Purge Rate:
Tagged bottom at: —Total Purge Volume:
Pump Speed:
3QD (At;L jryt,�
Time
DTW
(feet)
Temp
VQ
DO
(mg/0
Specific Cond.
(PS)
pH (S.U.)
report to 0.7.
ORP
(m1)
Turbidity
(NTU)
Comments
Dli4
1
'G
915,
-
1
i
9
�" i
S.
rJ- 1
�47•
�'l
2 13✓
.0
3
Time between recharge during sample collection:
Sampling Personnel Signature: /W//Date:
0
Notes: v
V
Stabilization
3 successive readings, 3 minutes apart:
'y`
l ep
within +/- 70% DO and turbidity'+/- 3% Conductivity,, 0.1 pH unit +/- 70 mV for ORP; _ T
from EPA - Low -Flow (Minimal Drowdown) Groundwater
Sampling Procedures,_April 1996 (Rev 2010)
Samples are analyzed immediately upon collection.
pS: micro-Siemen
mv: millivolt
°C: degrees Celsius
NTU: nephelometric turbidity units
bgs: below ground surface
ORP: oxidation reduction potential
DO: dissolved oxygen
S.U.: standard units
mg/L: milligrams per liter
toc: top of casing
initial if well information and sampling data has been verified MW_
well was tagged after sampling was complete

�kzANCHOR
QEA
Well Sampling Log
Date: (01* i Well Name: KW- C) r—
Project Name:
Saakm
Project Number.
-(
Weather.
1�
Sampling Personnel:
M
't
Sample Time: e:L
Well Information:
Well Depth in Feet (WD): 5t. O
Well Diameter.
Water Level in Feet (WL): t-t . !4•
Type of Casing:
Length of Water Column: 67, 9,
feet
Interval:
Screen;tic:k-Up
(WD) - (WL) = (LWC)
Flush Mount
One Casing Volume: l r
gallons
Comments:
(LWC) x (WCV)
Three Casing Volumes: ° — 3 , j
gallons
Tagged
Actual Volume Purged: �aC;
gallons
bottom at:
-
Well Casing Volumes (WCV)
1'` = 0.041 Gal/
2" = 0.17 C,al/
3" = 0.38 Gal/Ft 4" = 0.66 Gal/Ft 6" = 1.5 Gal/Ft 8" = 2.6 Gal/Ft 12" = 5.8 Gal/Ft
Purge Method:
Bailer-Disp.
Bailer -Teflon
Dedicated Pump Whale Pump Grundfos Other.
Sample Method:
Bailer-Dis
Bailer -Teflon
Dedicated Pump Whale Pump Grundfos Other.
Oxidation
Gallons
Temp
Dissolved Specific Cond.
pH (S.U.)
Reduction
Turbidity
Reading
Time
Purged
(°C)
Oxygen (mg/L) (p5/cm)
report to 0. S.U.
Potential (m1/)
(NTU)
Comments
2
oqog
2.
l✓
I n
-7!
'©, °
4
''2
z.2.�
1 Z2
��
)
2
- �-
5
V6
(_-
6
7
8
9
10
Notes:
Samples are analyzed immediately upon collection.
°C: degrees Celsius
NS/cm: micro-Siemen per centimeter
mg/L: milligrams per liter
mv: millivolt
NTU: nephelometric turbidity units
S.U.: Standard Units
Protective Casing: ,(I-Lv Pad:_ Lock: Vegetation: j�jf Access:
Sampling Personnel Signature:
V (Ork4-
Date: o f ? 311.1
initial if well information and sampling data has been verified [ 1 K
well was tagged after sampling was complete

Ilk 7, ANCHOR
Low -Flow Samplinq Loq Date: I C4 Well Name: INAA 1I- M,-t
Project Name:
,
Project Number: 14k—N-61
Location:
c,
Personnel:
[
Weather.
Well Information:
Screen Interval: `l bgs Arrive at Well: Q,
Depth to Water. 79-7 toc Start Time:
Well Diameter: in Sample Time: t l
Pump Intake: toc Finish Sample Time:
Drawdown Set: cls toc Leave Well:
Pump Used (circle): Peristaltic Bladd Other (description):
Comments:staI,,*( -A 3" _, - m M7,n[Ipo .— 16-a Purge Rate: /,
Tagged bottom at: �— Total Purge Volume: L t , L✓
Pump Speed: D /�S �" 1.3s
Time
DTW
(feet)
Temp
VQ
DO
(mg/L)
Specific Cond.
OAS)
pH (S.U.)
report to 0.7.
ORP
(mv)
Turbidity
(NTU)
Comments
-214
7 rr
/F.�
`" '4
-11.7
S.4(q
�7Sy
3.2 11
F r
-2-0r
st
Jr,-, �'
r 'V.0
2- 1
b. r
Is 4
4
_2 7. 6'
_11.2'"
/ r
_i
3l
-
l� 3
q./0
LE1
_ _
7
'.
.2 fla
1
1'
.2.-8
r r
�'
.,
J- �
7
/.�
1-2 r
—i.04
��
r�T
/ 7
ICI _ 3
Time between recharge during sample collection:
f
Sampling Personnel Signature:
Date: `' C
Notes:
Stabilization
3 successive readings, 3 minutes apart:
ry /�l
Ir w U ✓P�
within +/- 10% DO and turbidity, +/- 3% Conductivity, +/- 0,1 PH unit' +/- 70 mV forORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2010)
Samples are analyzed immediately upon collection.
pS: micro-Siemen
mv: millivolt
°C: degrees Celsius
NTU: nephelometric turbidity units
bgs: below ground surface
ORP: oxidation reduction potential
DO: dissolved oxygen
S.U.: standard units
mg/L: milligrams per liter
toc: top of casing
initial if well information and sampling data has been verifiedy
AML—
well was tagged after sampling was complete _�

ANCHOR
QEA�` �S
Low -Flow Sampling Log
Date: {f) 1­2 -J iG Well Name: MAJ -0'-Ir—
Project Name:
_ ar C'VA Ct), i �=
Project Number: _ Gr(tQ -ol oo
Location:
Personnel:
U"4LL1�
Weather:���
Well Information:
Screen Interval:
bgs
Arrive at Well:
4 �;
Depth to Water:
j�,�JJ,,GJ
oY�
toc
Start Time:
Well Diameter:
_;�
in
Sample Time:
Pump Intake:
rn_
toc
Finish Sample Time: 13"
Drawdown Set:
5
toc
Leave Well:�Q
Pump Used (circle):
Peristaltic Bladder
Other (description):
Comments:
CIVZWo
` na;&r'jj
alr81b
Purge Rate:
—[ n�-
`
Total Purge
Volume:
��
Pump Speed:
�'�.•
DTW
Temp
DO
Specific Cond.
pH (S.U.)
ORP
Turbidity
Time
(feet)
(°C)
(mg/L)
(pS)
report to 0.1.
(mv)
(NTU) Comments
iaa�'
32-Yo '_ 6.8 _
_-7_54
�5_
4 7�
340.2
1 10-G
1-130
_32-87 16.4
.�7SWaI
2,qy •3.
A-F-9
L23_3
3K:1 rg 16.1
6,6?
-- 700
�. l7
2 .�G
3.33
73 q'
6- ,3
_203- 3 .17
3
la39 .3-;
--qO . IC-1
2-.*16
739
-6 L
_-ao'1.3
�� � .
32•Y /6.0
I-Gi'
73q
�- !1
JU-p
-7 41
124E
32. YO _ l L_.
1,40
73 7 _
L2
)?7.-
125Lf
3�,97. 16•1
s.37
1257
3Z.,5 i.C.l
Time, between recharge during sample collection:
Sampling Personnel Signature:AZ
Date: ICf
.r
Notes:
Stabilization
3 successive readings, 3 minutes apart:
within +/- 70% DO and turbidity' +/- 3% Conductivity,' +/-
0.1 pH unit +/- 70 mV for ORP
from EPA - Low -Flow (Minimal Drawdown) Groundwater Sampling Procedures, April 1996 (Rev 2010)
Samples are analyzed immediately upon collection.
NS: micro-Siemen
mv: millivolt
°C: degrees Celsius
NTU: nephelometric turbidity units
bgs: below ground surface
ORP: oxidation reduction potential
DO: dissolved oxygen
S.U.: standard units
mg/L: milligrams per liter
toc: top of casing
Analytes
Sampled
Comments
VOCs (' B)
Nitroaromatic
Perchlorate (6850)
TOC (SM20 5310C)
Cl-, 504-, NO2, NO3 (300.0)
52- (4500 S2 D)
DHGs (8015B)
Mol, ular
Vqta.l 10al-

ANCHOR
F. �� AA
—v QEA
Sampling Log
Project Name: ' VY l C L f—' Date:_��3� f I
Project Number. �� I D V — 0 ( 1 d1 Weather.
Sampling Personnel:
Sample Name:
Comments: 'j` 11nSlG�.Q� dhl�
Sample Method:
Grab Syringe
Pump
Bailer-Disp.
Other.
Dissolved :
j Oxidation
Temp
Specific Cond, Oxygen
PH (S.l).}
Reduction
Turbidity
Time {C]
(KS) (mg/L)
• report to 0.] 5.U.
Potential (mV)
' (hlTli)
6.�
33v3 .go
, qS
-l6.7
!
I� ampling Container
Number of Containers
l.,Requested Analysis
500 mL Plastic
250 mL Plastic
125 mL Plastic
40 mL Glass
l(�
1 L Glass
Other .
Vegetation:
Access:
Sampling Personnel Signature:
Notes:
PS: micro-Siemen per cubic centimeter
°C: degrees Celsius
mg/L: milligrams per liter
mv: millivolt
NTU: nephelometric turbidity units
S.U.: standard units
Date: to 171/1 q
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: SM 4500 O G-2011
PH: SM 4500-H' B-2011
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Comments

ANCHOR
QfA
Surface Water Sampling Log
Anchor QEA of North Carolina, PILLC
231 Haywood Stree'
Asheville, North Carolina 2880'
Project Name: Co
Project Number:%ii41�0 --ot
Sampling Personnel: A416477
Sample Name:- &V — 0 1
Comments:
tYZrA'VI
Date: J011?7I 10
Weather:
Sample Method:
Syringe
Pump
Bailer-Disp. Other.
Z!
$(
4.
, Vnn!e
-Dissolved
S06cific
R eduction
Potikllall (in
-
Turbidity"
J
NTU),,
P
t
16- 5q
3&G
7 —7 —1
i
:nL"rNumber-of
-C& tai' 1p7
'rl
Requested Analysis A'k
500 mL Plastic
WA
ga
250 mL Plastic
125 mL Plastic
40 mL Glass
1 L Glass
Other
I�u I4AZk::A
Vegetation: Access:. Paz I I -az
PYIX I J'A'L/ M W
Sampling Personnel Signature:
Notes:
Samples are analyzed immeffi—aiely.pon collection.
*C: degrees Celsius
PS/cm: micro-Siemen per cubic centimeter
mg/L milligrams per liter
mv: millivolt
NTU: nephelometric turbidity units
S.U.: standard units
Date: (c7
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity. EPA Method 120.1, Rev. 1982
DO: SM 4500 0 G-2011
pH: SM 4500-H' B-2011
Page 1 of 1

ZANCHOR
QEA 4...c..v
Surface Water Sampling Log
Project Name: �50,6+0QvyA C
Project Number.
Sampling Personnel: inn 1�
Sample Name: ^ r -0
Comments: -V[ JA^ 6�-
Date:
Weather:
ISample Method: ( Grab Syringe Pump Bailer-Disp. Other:
Sampling Container t , E Number of Confainers yT Requester
500 mL Plastic ' YI
250 mL Plastic f
125 mL Plastic
40 mL Glass
1 L Glass Z O� W
Other _
Vegetation: (�
Sampling Personnel Signature: // e
Notes:
Samples are analyzed immediately upon collection
"C: degrees Celsius
PS/cm: micro-Siemen per cubic centimeter
mg/L: milligrams per liter
mv: millivolt
NTU: nephelometric turbidity units 4
S.U.: standard units
VL.(
W
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
(%S
Access: �-� -�T W.P L f t? S (S
Date: In
, C, 2-/ i q
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev. 1982
DO: SM 4500 O G-2011
pH: SM 4500-H` B-2011
Page 1 of 1

ANCHOR
QEA 4`
Sampling Log
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Project Name: -19 C�
Date:
i (' `),L f
Project NumberLg WI)
�v
- 01 4
Weather
Sampling Personnel:
Ls -(A>
Sample Name:
_
Comments:
Sample Method: Grab
Syringe Pump
Bailer-Disp.
Other.
Dissolved j
O.xidatinn
-
Temp . Specific Cond.
Oxygen pti (5.tl.)
Rc�duc#ian I
Turhicli ,
Time (`C) (FPS)
img/l ] report to 4.1 S.U.
Potential (mV)
(NTU) Carrtiments -
.
1
1 0 z
Sainpling Container
Number of Containers
RegUested Analysis
500 mL Plastic
250 mL Plastic
— - - — — - —
125 mL Plastic
— -
40 mL Glass
5 .2-
- —
1 L Glass
— — —
Other
I
Vegetation: Q�j
Access:
Sampling Personnel Signature:
Date: tar / l
Notes:
Method Reference:
PS: micro-Siemen per cubic centimeter
Temperature: SM 2550 B-2010
°C: degrees Celsius
Specific conductivity. EPA.Method 120.1, Rev.
1982
mg/L: milligrams per liter
DO: SM 4500 O G-2011
mv: millivolt
pH: SM 4500-1-1' B-2011
NTU: nephelometric turbidity units
S.U.: standard units
Page 1 of 1

EquiprrtentType:
. 5er;ai Number
Siatid. ':
Date of ii -
150-ft Water Level
26154
Solinist
150-ft Water Level
22754
Solinist
150-ft Water Level
150
Testwell
150-ft Drawdown
MP30 1527
QED .
Other
Select Turbidimeter.
Hach 2100Q (s/n 151006045207)
HF Scientific MicroTPW (s/n 2006016
rnstrurhen! Reading
(Haah2100Q)
Calibration
01h17U- ._
- -300, .Tt7 M NTV
Expiration Date:
6G
Cal:, n
�(J
Cal: `.q r _ Cal7. /��,� ,
V' * l0 1�UtJ
Tim cf?P!°1.
Time g.®- Time:
Verification (10 NTU): . r, 3
Time: ,1
10�NTUC�Exlon Date:
Y.51 •pr0essi¢nal Plus MuItl
Ipstnsment Readings
Dissolved Oxygen
Initial:
A
66- / ; �
Cal:
�0
mmHg:
Lit (a
PH 7 S.U.
Initi
pHmV:
Cal:
report to 0.1 S.U.
rQ,�
PH 4 S.U.
report to 0.1 S.U.
Initial; • ��
1—yl
pHmV:
--
Ca3'661
pH 10 S.U.
Initial
pHmV:
Cal:„
report to 0.1 S.U.r
I j
QC* pH.7 S.U.
report to0.7S.U.
AM Time:
Meas:
--1-, 0 7�r
Mid Day Time:
Spec.Cond. I Initial: Cal: I�Time:
bn pS/cm** t 000
QC*: AM ® Time: Meas: Mid Day Time:
vo Ps/cm q, Veo u L a
r
itial: Cal: Ternerature (°C)
DO— mV q ( ,) y K v
ANCHOR
�•.� QEA �'
Equipment Documentation and Instrument Calibration Data Sheet
CALIBRATION DOCUMENTATION
Project Name: &A Person Conducting Calibration:
Project Number. 61It" -(A, _ Date of Calibration:
Project Location: pit 14" � � Date of Field Measurements:
EQUIPMENT DOCUMENTATION'
Equipment or meters used to take measurements (e.g., water level meters, survey equipment):
5)
Ir%trurnent Reading
(HF Scientific MictoTpW)
1;Ott0.>YTU 1 10.0 NTU 8.03
:al:
ime:
'erificatl
ime:
aratno
empera
�4
,r:Meter Wri 1.813101802)
MY
pHmV:
Tiffmryrye-
V
pHmV-.
Tim n -
Check:
PM Time:
Check:
PM Time:
lime:
Ov,a�rl{
sR
x
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Calibration
Signature: Date: b 7 2,1 q
Notes:
1. Electronic equipment calibrated according to the manufacturer's operation manual.
2. Specific Conductivity should be calibrated according to values representative of historic range.
3. Order of Calibration is as follows: Specific Conductivity, pH 7, pH 4, pH 16, DO, ORP, QC checks.
4. QC Acceptable Ranges: pH +/- 0.1 S.U. and Specific Conductivity 10% of the true value. If QC readings are out of range, the instrument needs to be recalibrated.
5. * Indicates that a QC check must be performed in the morning, afternoon, and the end of the day, or every four hours:
6. ** Indicates to choose a Specific Conductivity buffer of 1413, 447, 84, or 23 mS which is closest to historical readings from the project location.
Method Reference: Temperature: SM 2550 B-2070 I Specific conductivity: EPA Method 720.7, Rev. 19a2 I DO: SM 4500 0 G-2077 I pH: SM 4500-H+ B-2011
NA
Date
Page 1 of 1

ANCHOR
.� QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 79001
Equipment Documentation and Instrument Calibration Data Sheet
CALIBRATION DOCUMENTATION
Project Name: ZfQCknr. CIA C0- (/F Person Conducting Calibration:
Project Number. C -®L,a I Date of Calibration: .3 --
Project Location: C _ Date of Field Measurements:
EQUIPMENT DOCUMENTATION
Equipment or meters used to take measurements (e.g., water level meters, survey equipment):
failR IN , e
seria wumtmr
-"Sraii
D;teof. ust
150-ft Water Level
26154
Solinist
150-ft Water Level
22754
Solinist
150-ft Water Level
150
Testwell
150-ft Drawdown
MP30 1527
QED
' Other
Select Turbidimeter. Hach 21000 (s/n 151006045207)
HF Scientific MicroTPW (s/n 200601045)
Instroment Reading In3trumrttt Read.inti
L-- (Ha4h2100Q) CUF scientific MicroTP14I}
Calibration to Ntu 100 NTU 800 NTU 1,000 NT'11 10:9 HTt1 4-21
p2 '
Expiratipn Date: _;L0 i Dto �' �. /llq� 1 i J
C i
mar. Lai 104 Cal-, Cal: Cal: Cal:
c 0%— �
-t r rLL 7 �= Timem
sTime, Tim � � Time: Time: Ti7 e:
Verification (10 NTU): Verification: Ver' n: Verifi
Tim 10 NTU Cal. Expiration Date: Time: Time: Time:
rIffI PP
Signature: �� !10l.mil t � I
Date:
Notes: 1-�
1. Electronic equipment calibrated according to the manufacturer's operation manual.
2. Specific Conductivity should be calibrated according to values representative of historic range.
3.Order of Calibration is as follows: Specific Conductivity, pH 7, pH 4, pH 10, DO, ORP, QC checks.
4. QC Acceptable Ranges: pH +/- 0.1 S.U. and Specific Conductivity 10% of the true value. If QC readings are out of range, the instrument needs to be recalibrated.
S. * Indicates that a QC check must be performed in the morning, afternoon, and the end of the day, or every four hours.
6. ** Indicates to choose a Specific Conductivity buffer of 1413, 447, 84, or 23'mS which is closest to historical readings from the project location.
Method Reference: Temperature: SM 2550 B-2010 I Specific conductivity: EPA Method 120.1, Rev. 1982 1 DO: SM 4500 O G-2077 I pH: SM 4500-H+ B-2011
Page 1 of 1

ANCHOR
QEA
Equipment Documentation and Instrument Calibration Data Sheet
CALIBRATION DOCUMENTATION
Project Name: �Q.Cij (din �J (l�i Person Conducting Calibration: K
Project Number. edf4% -6J Date of Calibration:
Project Location: a`1 L t2C&7j, INC, Date of Field Measurements: J
Equipment or meters used to take measurements'(e.g., water level meters, survey equipment):
Equipment Type
Serial Number
Brand
Date of Use>
150-ft Water Level
26154
Solinist
150-ft Water Level
22754
Solinist
150-ft Water Level
150
Testwell
150-ft Drawdown
MP30-1527
QED
Other
Select Turbidimeter. Hach 2100Q (s/n 151006045207)
HF Scientific MicroTPW (s/n.200601045)
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
YSI Professional Plus Multiparameter Meter (sin 18B101802)
Instrument Readings
Initial: Cal: mmHg: Temperature (°C): Time:
iti"i
Dissolved Oxygen / .0.
7-70.1 l r
_
Calibration Expiration Date
NA
PH 7 S.U. Initial: pH 2 i �, Cal: fl J
TimeeY C7 /�
report to0.1S.U. 0 v,()tD
/ ] pr �, y
�J r12wo
PH 4 report to 0.1 S.U. U. Initial: i � p V: Cal: 00 pHmV: Time.. 15
Q7 17 a zo
111/ '
PH 10 S.U. Initial: pHmV: Cal: p V: Time:
report to 0.7 S.U. Q,O? / 7-) 10, () / `�� C2!
O�1-20ZG
QC* pH 7 S.U. A��1jT' as: Mid Day Time: Check PM Time:
report to 0.1 S.U. V� G+ , q
Check: /
��/ dZU
Spec. Cond. Initial: Cal: f� Time: p
S/cm** '°I g E /V oo V O 0 f
��2V l
Qe*: AM Time: Meeaas: Mid Day Time:
l
Check: ` `{/�
r (
PS/Cm �) -1 i
pt�' !
Initial: Cal: Tem*perrlaturel(°C): Time:
mV r7 nr. 1 1s✓ , C1 C&. — 7
/ /ry
f �l mid/l
Signature: Date:
Notes:
1. Electronic equipment calibrated according to the manufacturer's operation manual.
2. Specific Conductivity should be calibrated according to values representative of historic range.
3.Order of Calibration is as follows: Specific Conductivity, pH 7, pH 4, pH 1Q DO, ORP, QC checks.
4. QC Acceptable Ranges: pH +/- 0.1 S.U. and Specific Conductivity 10% of the true value. If QC readings are out of range, the instrument needs to be recalibrated.
5. * Indicates that a QC check must be performed in the morning, afternoon, and the end of the day, or every four hours.
6. ** Indicates to choose a Specific Conductivity buffer of 1413, 447, 84, or 23 mS which is closest to historical readings from the project location.
Method Reference: Temperature: SM 2550 B-2070 I Specific conductivity: EPA Method 120.1, Rev. 1982 1 DO: SM 4500 0 G-2017
I pH: SM 4500-H+ B-2011
Page 1 of 1

Appendix B
Reports of Laboratory Analysis,
Chain -of -Custody Documentation,
and Certificates of Analysis

LP R I S M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Anchor QEA of North Carolina, PLLC
Alec Macbeth
231 Haywood Street
Asheville, NC 28801
NC Certification No. 402 Case Narrative
NC Drinking Water Cert No. 37735 11 /8/19 14:31
SC Certification No. 99012
Project: Jackson Cty Landfill 2019 Fall Samplling
Project No.: 50-02
Lab Submittal Date: 10/23/2019
Prism Work Order: 9100361
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
8270 App II analysis was subcontracted to AES. TOC analysis was subcontracted to Pace Analytical Gulf
Coast. Laboratory reports are attached.
Prism Summary of Detections does not include subcontracted data.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones Reviewed By Robbi A. Jones
President/Project Manager President/Project Manager
Data Qualifiers Key Reference:
B Analyte is found in the associated blank at a concentration >1/2 RL.
BB Blank value is outside of the control limits. Validity of the data not affected.
HT Sample received and analyzed outside of the hold time.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 67

Sample Receipt Summary
R I IS M
Full -Service Analytical R
Environmental Solutions
11/08/2019
&GIE
LABORATORIES, INC.
Prism Work Order: 9100361
Client Sample ID
Lab Sample ID
Matrix
Date/Time Sampled Date/Time Received
MW-04
9100361-01
Water
10/22/19 11:26 10/23/19 11:03
MW-07
9100361-02
Water
10/22/19 12:57 10/23/19 11:03
SW-01
9100361-03
Water
10/22/19 14:05 10/23/19 11:03
SW-02
9100361-04
Water
10/22/19 14:30 10/23/19 11:03
LT-01
9100361-05
Water
10/22/19 14:58 10/23/19 11:03
TB-01
9100361-06
Water
10/22/19 0:00 10/23/19 11:03
Samples were received in good condition at 4.7 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 2 of 67

/r P R I S M Full -Service Analytical s
Environmental Solutions
LABORATOR
Summary of Detections
11 /08/201 S
Prism Work Order: 9100361
Prism ID
Client ID
Parameter
Method
Result
Units
9100361-01
MW-04
Chloride
9056A
47000
ug/L
9100361-01
MW-04
Nitrate as N
9056A
5300
ug/L
9100361-01
MW-04
Sulfate
9056A
78000
ug/L
9100361-01
MW-04
Biochemical Oxygen Demand
SM5210 B
820
BB, J,
ug/L
B
9100361-01
MW-04
Sulfide
SM4500-S F
11000
ug/L
9100361-01
MW-04
Total Alkalinity to pH 4.5
SM2320 B
100000
ug/L
9100361-01
MW-04
Barium
6020E
92
ug/L
9100361-01
MW-04
Cadmium
6020B
0.24
J
ug/L
9100361-01
MW-04
Cobalt
6020E
2.0
ug/L
9100361-01
MW-04
Nickel
6020B
1.7
J
ug/L
9100361-01
MW-04
Selenium
6020B
1.0
J
ug/L
9100361-01
MW-04
Tin
6020B
3.2
J
ug/L
9100361-01
MW-04
Zinc
6020B
15
J
ug/L
9100361-01
MW-04
1,4-Dichlorobenzene
8260D
2.0
ug/L
9100361-01
MW-04
Acetone
8260D
3.3
J
ug/L
9100361-01
MW-04
Chlorobenzene
8260D
1.5
ug/L
9100361-01
MW-04
cis-1,2-Dichloroethylene
8260D
0.74
ug/L
9100361-01
MW-04
1,4-Dioxane
8260D SIM
5.4
ug/L
9100361-02
MW-07
Chloride
9056A
75000
ug/L
9100361-02
MW-07
Nitrate as N
9056A
110
J
ug/L
9100361-02
MW-07
Sulfate
9056A
22000
ug/L
9100361-02
MW-07
Biochemical Oxygen Demand
SM5210 B
1700
BB, J,
ug/L
B
9100361-02
MW-07
Chemical Oxygen Demand
SM5220 D
13000
J
ug/L
9100361-02
MW-07
Ferrous Iron
SM3500-Fe D
74
HT, J
ug/L
9100361-02
MW-07
Sulfide
SM4500-S F
12000
ug/L
9100361-02
MW-07
Total Alkalinity to pH 4.5
SM2320 B
240000
ug/L
9100361-02
MW-07
Barium
6020B
450
ug/L
9100361-02
MW-07
Cobalt
6020B
1.3
J
ug/L
9100361-02
MW-07
Nickel
6020B
7.1
ug/L
9100361-02
MW-07
Zinc
6020E
21
ug/L
9100361-02
MW-07
1,4-Dichlorobenzene
8260D
4.4
ug/L
9100361-02
MW-07
Acetone
8260D
4.5
J
ug/L
9100361-02
MW-07
Benzene
8260D
1.2
ug/L
9100361-02
MW-07
Chlorobenzene
8260D
4.4
ug/L
9100361-02
MW-07
cis-1,2-Dichloroethylene
8260D
2.2
ug/L
9100361-02
MW-07
1,4-Dioxane
8260D SIM
18
ug/L
9100361-03
SW-01
Hardness
SM2340 C
13000
ug/L
9100361-03
SW-01
Barium
6020B
19
ug/L
9100361-03
SW-01
Zinc
6020B
16
J
ug/L
9100361-03
SW-01
Acetone
8260D
4.8
J
ug/L
9100361-04
SW-02
Hardness
SM2340 C
15000
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 3 of 67

/P R I S Full -Service Analytical s
Environmental Solutions
� LABORATORIES, INC.
Summary of Detections
11 /08/201
Prism Work Order: 9100361
Prism ID
Client ID
Parameter
Method
Result
Units
9100361-04
SW-02
Barium
6020B
18
ug/L
9100361-04
SW-02
Zinc
6020B
17
J
ug/L
9100361-04
SW-02
Acetone
8260D
3.9
J
ug/L
9100361-05
LT-01
1,4-Dichlorobenzene
8260D
3.7
ug/L
9100361-05
LT-01
Acetone
8260D
6.0
ug/L
9100361-05
LT-01
Benzene
8260D
1.7
ug/L
9100361-05
LT-01
Chlorobenzene
8260D
3.8
ug/L
9100361-05
LT-01
Ethylbenzene
8260D
1.6
ug/L
9100361-05
LT-01
o-Xylene
8260D
1.1
ug/L
9100361-05
LT-01
Toluene
8260D
0.39
.1
ug/L
9100361-05
LT-01
Xylenes, total
8260D
1.7
ug/L
9100361-06
TB-01
Acetone
8260D
2.7
J
ug/L
9100361-06
TB-01
Chloromethane
8260D
0.57
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 67

PRISM Laboratory Report
Full -Service Analytical &
Environmental Solutions 11/08/2019
LABORATORIES, INC.
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Client Sample ID: MW-04
Attn: Alec Macbeth Samplling Prism Sample ID: 9100361-01
231 Haywood Street Project No.: 50-02 Prism Work Order: 9100361
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/22/19 11:26
Time Submitted: 10/23/19 11:03
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Anions by Ion Chromatography
Chloride
47000
ug/L
NE
1000
380
1
9056A
10/24/19 1:39 BMS
P9J0423
Nitrate as N
5300
ug/L
10000
200
54
1
9056A
10/24/19 1:39 BMS
P9J0423
Sulfate
78000
ug/L
250000
2000
480
1
9056A
10/24/19 1:39 BMS
P9JO423
General Chemistry Parameters
Biochemical Oxygen Demand
820
BB,
ug/L
NE
2000
210
1
SM5210 B
10/24/19 11:20CBM
P9J0483
J, B
Chemical Oxygen Demand
<10000
ug/L
NE
50000
10000
1
SM5220 D
10/24/19 11:12SLS
P9JO436
Ferrous Iron
<51
HT
ug/L
NE
200
51
1
SM3500-Fe D
10/23/19 15:20BMS
P9JO408
Sulfide
11000
ug/L
1000
2000
830
1
SM4500-S F
10/29/19 9:45 CBM
P9JO504
Total Alkalinity to pH 4.5
100000
ug/L
NE
5000
770
1
SM2320 B
10/31/19 10:28CLB
P9J0537
Total Metals
Mercury
<0.034
ug/L
0.2
0.20
0.034
1
7470A
10/29/19 16:21JAB
P9JO493
Antimony
<0.93
ug/L
6
3.0
0.93
1
6020B
10/28/19 15:OOMMR
P9JO440
Arsenic
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 15:OOMMR
P9JO440
Barium
92
ug/L
100
10
3.2
1
6020B
10/28/19 15:00MMR
P9JO440
Beryllium
<0.30
ug/L
1
1.0
0.30
1
6020B
10/28/19 15:OOMMR
P9JO440
Cadmium
0.24
J
ug/L
1
1.0
0.22
1
6020B
10/28/19 15:001111MR
P9JO440
Chromium
<0.90
ug/L
10
3.0
0.90
1
6020B
10/28/19 15:OOMMR
P9JO440
Cobalt
2.0
ug/L
10
2.0
0.70
1
6020B
10/28/19 15:001111MR
P9JO440
Copper
<4.7
ug/L
10
10
4.7
1
6020B
10/28/19 15:OOMMR
P9JO440
Lead
<0.44
ug/L
10
1.0
0.44
1
6020B
10/28/19 15:OOMMR
P9J0440
Nickel
1.7
J
ug/L
50
3.0
0.83
1
6020B
10/28/19 15:00MMR
P9JO440
Selenium
1.0
J
ug/L
10
5.0
0.98
1
6020B
10/28/19 15:OOMMR
P9JO440
Silver
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 15:OOMMR
P9JO440
Thallium
<0.84
ug/L
5.5
2.0
0.84
1
6020B
10/28/19 15:OOMMR
P9J0440
Tin
3.2
J
ug/L
100
5.0
1.9
1
6020B
10/28/19 15:001111MR
P9JO440
Vanadium
<1.5
ug/L
25
5.0
1.5
1
6020B
10/28/19 15:OOMMR
P9J0440
Zinc
15
J
ug/L
10
20
10
1
6020B
10/28/19 15:00MMR
P9JO440
Volatile Organic Compounds by GC/MS
1,1,1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19 6:55 KDM
P9K0048
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19 6:55 KDM
P91<0048
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
11/2/19 6:55 KDM
P9K0048
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
11/2/19 6:55 KDM
P91<0048
1,1-Dichloroethane
<0.29
ug/L
5
0.50
0.29
1
8260D
11/2/19 6:55 KDM
P9K0048
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19 6:55 KDM
P91<0048
1, 1 -Dichloropropylene
<0.37
ug/L
5
0.50
0.37
1
8260D
11/2/19 6:55 KDM
P9K0048
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
11/2/19 6:55 KDM
P91<0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 67

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No.: 50-02
Sample Matrix: Water
Laboratory Report
11/08/2019
Client Sample ID: MW-04
Prism Sample ID: 9100361-01
Prism Work Order: 9100361
Time Collected: 10/22/19 11:26
Time Submitted: 10/23/19 11:03
Parameter
Result Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,2,4-Trichlorobenzene
<0.44
ug/L
10
1.0
0.44
1
8260D
11/2/19
6:55
KDM
P9K0048
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
11/2/19
6:55
KDM
P9K0048
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
11/2/19
6:55
KDM
P9K0048
1,2-Dichlorobenzene
<0.28
ug/L
5
0.50
0.28
1
8260D
11/2/19
6:55
KDM
P9K0048
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19
6:55
KDM
P9K0048
1,2-Dichloropropane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
6:55
KDM
P9K0048
1,3-Dichlorobenzene
<0.40
ug/L
5
0.50
0.40
1
8260D
11/2/19
6:55
KDM
P9K0048
1,3-Dichloropropane
<0.40
ug/L
1
0.50
0.40
1
8260D
11/2/19
6:55
KDM
P9K0048
1,4-Dichlorobenzene
2.0
ug/L
1
0.50
0.42
1
8260D
11/2/19
6:55
KDM
P91(0048
2,2-Dichloropropane
<0.26
ug/L
15
2.0
0.26
1
8260D
11/2/19
6:55
KDM
P91<0048
Acetone
3.3
j ug/L
100
5.0
0.70
1
8260D
11/2/19
6:55
KDM
P9K0048
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
11/2/19
6:55
KDM
P91<0048
Acrolein
<1.2
ug/L
53
20
1.2
1
8260D
11/2/19
6:55
KDM
P9K0048
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
11/2/19
6:55
KDM
P91<0048
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
11/2/19
6:55
KDM
P9K0048
Benzene
<0.34
ug/L
1
0.50
0.34
1
8260D
11/2/19
6:55
KDM
P91<0048
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
11/2/19
6:55
KDM
P9K0048
Bromodichloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
6:55
KDM
P91<0048
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
11/2/19
6:55
KDM
P9K0048
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
11/2/19
6:55
KDM
P91<0048
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
11/2/19
6:55
KDM
P9K0048
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
11/2/19
6:55
KDM
P91<0048
Chlorobenzene
1.5
ug/L
3
0.50
0.34
1
8260D
11/2/19
6:55
KDM
P9K0048
Chloroethane
<0.43
ug/L
10
0.50
0.43
1
8260D
11/2/19
6:55
KDM
P9K0048
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
11/2/19
6:55
KDM
P91<0048
Chloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
6:55
KDM
P9K0048
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
11/2/19
6:55
KDM
P91<0048
cis-1,2-Dichloroethylene
0.74
ug/L
2
0.50
0.40
1
8260D
11/2/19
6:55
KDM
P9K0048
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
11/2/19
6:55
KDM
P9K0048
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
11/2/19
6:55
KDM
P9K0048
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
11/2/19
6:55
KDM
P9K0048
Dichlorodifluoromethane
<0.47
ug/L
5
5.0
0.47
1
8260D
11/2/19
6:55
KDM
P9K0048
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
11/2/19
6:55
KDM
P9K0048
Ethylbenzene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
6:55
KDM
P9K0048
Hexachlorobutadiene
<0.24
ug/L
10
2.0
0.24
1
8260D
11/2/19
6:55
KDM
P9K0048
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
11/2/19
6:55
KDM
P9K0048
m,p-Xylenes
<0.73
ug/L
NE
1.0
0.73
1
8260D
11/2/19
6:55
KDM
P9K0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 67

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 11/08/2019
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Client Sample ID: MW-04
Attn: Alec Macbeth Samplling Prism Sample ID: 9100361-01
231 Haywood Street Project No.: 50-02 Prism Work Order: 9100361
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/22/19 11:26
Time Submitted: 10/23/19 11:03
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
11/2/19
6:55
KDM
P91<0048
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
11/2/19
6:55
KDM
P9K0048
Methyl Ethyl Ketone (2-Butanone)
<0.78
ug/L
100
5.0
0.78
1
8260D
11/2/19
6:55
KDM
P91<0048
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
11/2/19
6:55
KDM
P9K0048
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
11/2/19
6:55
KDM
P91<0048
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
11/2/19
6:55
KDM
P9K0048
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1
8260D
11/2/19
6:55
KDM
P91<0048
Naphthalene
<0.45
ug/L
10
1.0
0.45
1
8260D
11/2/19
6:55
KDM
P9K0048
o-Xylene
<0.40
ug/L
NE
0.50
0.40
1
8260D
11/2/19
6:55
KDM
P91<0048
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
11/2/19
6:55
KDM
P9K0048
Styrene
<0.26
ug/L
1
0.50
0.26
1
8260D
11/2/19
6:55
KDM
P91<0048
Tetrachloroethylene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
6:55
KDM
P9K0048
Tetrahydrofuran
<0.68
ug/L
NE
10
0.68
1
8260D
11/2/19
6:55
KDM
P91<0048
Toluene
<0.35
ug/L
1
0.50
0.35
1
8260D
11/2/19
6:55
KDM
P9K0048
trans- 1,2-Dichloroethylene
<0.27
ug/L
5
0.50
0.27
1
8260D
11/2/19
6:55
KDM
P91<0048
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1
8260D
11/2/19
6:55
KDM
P9K0048
trans- 1,4-Dichloro-2-butene
<0.22
ug/L
100
10
0.22
1
8260D
11/2/19
6:55
KDM
P91<0048
Trichloroethylene
<0.46
ug/L
1
0.50
0.46
1
8260D
11/2/19
6:55
KDM
P9K0048
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1
8260D
11/2/19
6:55
KDM
P91<0048
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1
8260D
11/2/19
6:55
KDM
P9K0048
Vinyl chloride
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19
6:55
KDM
P91<0048
Xylenes, total
<1.1
ug/L
5
1.5
1.1
1
8260D
11/2/19
6:55
KDM
P9K0048
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
98 %
80-124
Dibromofluoromethane
100 %
75-129
Toluene-d8
99 %
77-123
Volatile Organic Compounds by GC/MS SIM
1,4-Dioxane
5.4
ug/L
10
2.0
0.14
1
8260D SIM
10/23/19
17:40TBL
P9J0395
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 67

Laboratory Report
Full -Service
Analytical &
P R S M Environmental
LABORATORIES INC.
Solutions
11/08/2019
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2019
Fall
Client Sample ID: MW-07
Attn: Alec Macbeth
Samplling
Prism Sample ID: 9100361-02
231 Haywood Street
Project No.:
50-02
Prism Work Order: 9100361
Asheville, NC 28801
Sample Matrix:
Water
Time Collected: 10/22/19 12:57
Time Submitted: 10/23/19 11:03
Parameter
Result Units
SWSL
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
Anions by Ion Chromatography
Chloride
75000
ug/L
NE
1000
380
1 9056A 10/24/19 2:25 BMS
P9J0423
Nitrate as N
110
J ug/L
10000
200
54
1 9056A 10/24/19 2:25 BMS
P9J0423
Sulfate
22000
ug/L
250000
2000
480
1 9056A 10/24/19 2:25 BMS
P9J0423
General Chemistry Parameters
Biochemical Oxygen Demand
1700
BB, ug/L
NE
2000
210
1 SM5210 B 10/24/19 11:20CBM
P9J0483
J, B
Chemical Oxygen Demand
13000
J ug/L
NE
50000
10000
1 SM5220 D 10/24/19 11:12 SLS
P9J0436
Ferrous Iron
74
HT, ug/L
NE
200
51
1 SM3500-Fe D 10/23/19 15:20BMS
P9J0408
J
Sulfide
12000
ug/L
1000
2000
830
1 SM4500-S F 10/29/19 9:45 CBM
P9J0504
Total Alkalinity to pH 4.5
240000
ug/L
NE
5000
770
1 SM2320 B 10/31/19 10:28CLB
P9J0537
Total Metals
Mercury
<0.034
ug/L
0.2
0.20
0.034
1
7470A
10/29/19 16:25JAB
P9J0493
Antimony
<0.93
ug/L
6
3.0
0.93
1
6020B
10/28/19 15:07MMR
P9J0440
Arsenic
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 15:07MMR
P9J0440
Barium
450
ug/L
100
10
3.2
1
6020B
10/28/19 15:07MMR
P9J0440
Beryllium
<0.30
ug/L
1
1.0
0.30
1
6020B
10/28/19 15:07MMR
P9J0440
Cadmium
<0.22
ug/L
1
1.0
0.22
1
6020B
10/28/19 15:07MMR
P9J0440
Chromium
<0.90
ug/L
10
3.0
0.90
1
6020B
10/28/19 15:07MMR
P9J0440
Cobalt
1.3 J
ug/L
10
2.0
0.70
1
6020B
10/28/19 15:07MMR
P9J0440
Copper
<4.7
ug/L
10
10
4.7
1
6020B
10/28/19 15:07MMR
P9J0440
Lead
<0.44
ug/L
10
1.0
0.44
1
6020B
10/28/19 15:07MMR
P9J0440
Nickel
7.1
ug/L
50
3.0
0.83
1
6020B
10/28/19 15:07MMR
P9J0440
Selenium
<0.98
ug/L
10
5.0
0.98
1
6020B
10/28/19 15:07MMR
P9J0440
Silver
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 15:07MMR
P9J0440
Thallium
<0.84
ug/L
5.5
2.0
0.84
1
6020B
10/28/19 15:07MMR
P9J0440
Tin
<1.9
ug/L
100
5.0
1.9
1
6020B
10/28/19 15:07MMR
P9J0440
Vanadium
<1.5
ug/L
25
5.0
1.5
1
6020B
10/28/19 15:07MMR
P9J0440
Zinc
21
ug/L
10
20
10
1
6020B
10/28/19 15:07MMR
P9J0440
Volatile Organic Compounds by GUMS
1, 1, 1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19 7:21 KDM
P91<0048
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19 7:21 KDM
P9K0048
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
11/2/19 7:21 KDM
P91<0048
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
11/2/19 7:21 KDM
P9K0048
1,1-Dichloroethane
<0.29
ug/L
5
0.50
0.29
1
8260D
11/2/19 7:21 KDM
P91<0048
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19 7:21 KDM
P9K0048
1, 1 -Dichloropropylene
<0.37
ug/L
5
0.50
0.37
1
8260D
11/2/19 7:21 KDM
P91<0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 67

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No.: 50-02
Sample Matrix: Water
Laboratory Report
11/08/2019
Client Sample ID: MW-07
Prism Sample ID: 9100361-02
Prism Work Order: 9100361
Time Collected: 10/22/19 12:57
Time Submitted: 10/23/19 11:03
Parameter
Result Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
11/2/19
7:21
KDM
P9K0048
1,2,4-Trichlorobenzene
<0.44
ug/L
10
1.0
0.44
1
8260D
11/2/19
7:21
KDM
P9K0048
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
11/2/19
7:21
KDM
P9K0048
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
11/2/19
7:21
KDM
P9K0048
1,2-Dichlorobenzene
<0.28
ug/L
5
0.50
0.28
1
8260D
11/2/19
7:21
KDM
P9K0048
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19
7:21
KDM
P9K0048
1,2-Dichloropropane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
7:21
KDM
P9K0048
1,3-Dichlorobenzene
<0.40
ug/L
5
0.50
0.40
1
8260D
11/2/19
7:21
KDM
P9K0048
1,3-Dichloropropane
<0.40
ug/L
1
0.50
0.40
1
8260D
11/2/19
7:21
KDM
P9K0048
1,4-Dichlorobenzene
4.4
ug/L
1
0.50
0.42
1
8260D
11/2/19
7:21
KDM
P9K0048
2,2-Dichloropropane
<0.26
ug/L
15
2.0
0.26
1
8260D
11/2/19
7:21
KDM
P9K0048
Acetone
4.5
1 ug/L
100
5.0
0.70
1
8260D
11/2/19
7:21
KDM
P9K0048
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
11/2/19
7:21
KDM
P9K0048
Acrolein
<1.2
ug/L
53
20
1.2
1
8260D
11/2/19
7:21
KDM
P91<0048
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
11/2/19
7:21
KDM
P9K0048
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
11/2/19
7:21
KDM
P91<0048
Benzene
1.2
ug/L
1
0.50
0.34
1
8260D
11/2/19
7:21
KDM
P9K0048
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
11/2/19
7:21
KDM
P9K0048
Bromodichloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
7:21
KDM
P91<0048
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
11/2/19
7:21
KDM
P9K0048
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
11/2/19
7:21
KDM
P91<0048
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
11/2/19
7:21
KDM
P9K0048
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
11/2/19
7:21
KDM
P91<0048
Chlorobenzene
4.4
ug/L
3
0.50
0.34
1
8260D
11/2/19
7:21
KDM
P9K0048
Chloroethane
<0.43
ug/L
10
0.50
0.43
1
8260D
11/2/19
7:21
KDM
P9K0048
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
11/2/19
7:21
KDM
P9K0048
Chloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
7:21
KDM
P9K0048
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
11/2/19
7:21
KDM
P9K0048
cis-1,2-Dichloroethylene
2.2
ug/L
2
0.50
0.40
1
8260D
11/2/19
7:21
KDM
P9K0048
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
11/2/19
7:21
KDM
P9K0048
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
11/2/19
7:21
KDM
P9K0048
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
11/2/19
7:21
KDM
P9K0048
Dichlorodifluoromethane
<0.47
ug/L
5
5.0
0.47
1
8260D
11/2/19
7:21
KDM
P9K0048
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
11/2/19
7:21
KDM
P9K0048
Ethylbenzene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
7:21
KDM
P9K0048
Hexachlorobutadiene
<0.24
ug/L
10
2.0
0.24
1
8260D
11/2/19
7:21
KDM
P9K0048
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
11/2/19
7:21
KDM
P9K0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 67

Laboratory Report
Full -Service Analytical &
P R S M
Environmental Solutions
LABORATORIES INC.
11/08/2019
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2019
Fall
Client
Sample ID:
MW-07
Attn: Alec Macbeth
Samplling
Prism
Sample ID:
9100361-02
231 Haywood Street
Project No.:
50-02
Prism
Work Order:
9100361
Asheville, NC 28801
Sample Matrix:
Water
Time
Collected: 10/22/19 12:57
Time
Submitted: 10/23/19
11:03
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
m,p-Xylenes
<0.73
ug/L
NE
1.0
0.73
1
8260D
11/2/19
7:21
KDM
P91<0048
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
11/2/19
7:21
KDM
P9K0048
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
11/2/19
7:21
KDM
P91<0048
Methyl Ethyl Ketone (2-Butanone)
<0.78
ug/L
100
5.0
0.78
1
8260D
11/2/19
7:21
KDM
P9K0048
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
11/2/19
7:21
KDM
P91<0048
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
11/2/19
7:21
KDM
P9K0048
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
11/2/19
7:21
KDM
P91<0048
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1
8260D
11/2/19
7:21
KDM
P9K0048
Naphthalene
<0.45
ug/L
10
1.0
0.45
1
8260D
11/2/19
7:21
KDM
P91<0048
o-Xylene
<0.40
ug/L
NE
0.50
0.40
1
8260D
11/2/19
7:21
KDM
P9K0048
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
11/2/19
7:21
KDM
P91<0048
Styrene
<0.26
ug/L
1
0.50
0.26
1
8260D
11/2/19
7:21
KDM
P9K0048
Tetrachloroethylene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
7:21
KDM
P91<0048
Tetrahydrofuran
<0.68
ug/L
NE
10
0.68
1
8260D
11/2/19
7:21
KDM
P9K0048
Toluene
<0.35
ug/L
1
0.50
0.35
1
8260D
11/2/19
7:21
KDM
P91<0048
trans- 1,2-Dichloroethylene
<0.27
ug/L
5
0.50
0.27
1
8260D
11/2/19
7:21
KDM
P9K0048
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1
8260D
11/2/19
7:21
KDM
P91<0048
trans- 1,4-Dich loro-2-butene
<0.22
ug/L
100
10
0.22
1
8260D
11/2/19
7:21
KDM
P9K0048
Trichloroethylene
<0.46
ug/L
1
0.50
0.46
1
8260D
11/2/19
7:21
KDM
P91<0048
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1
8260D
11/2/19
7:21
KDM
P9K0048
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1
8260D
11/2/19
7:21
KDM
P91<0048
Vinyl chloride
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19
7:21
KDM
P9K0048
Xylenes, total
<1.1
ug/L
5
1.5
1.1
1
8260D
11/2/19
7:21
KDM
P9K0048
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
80-124
Dibromofluoromethane
100 %
75-129
Toluene-d8
99 %
77-123
Volatile Organic Compounds by GUMS SIM
1,4-Dioxane
18
ug/L
10
2.0
0.14
1
8260D SIM
10/23/19 18:05TBL
P9J0395
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 67

�Full-Service Analytical
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
11 /08/2019
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No.: 50-02
Sample Matrix: Water
Client Sample ID: SW-01
Prism Sample ID: 9100361-03
Prism Work Order: 9100361
Time Collected: 10/22/19 14:05
Time Submitted: 10/23/19 11:03
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Hardness 13000 ug/L 5000 570 1 SM2340 C 10/28/19 13:50 BMS P9J0482
Total Metals
Mercury
<0.034
ug/L
0.2
0.20
0.034
1
7470A
10/29/19 16:28JAB
P9J0493
Antimony
<0.93
ug/L
6
3.0
0.93
1
6020B
10/28/19 15:14MMR
P9J0440
Arsenic
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 15:14MMR
P9J0440
Barium
19
ug/L
100
10
3.2
1
6020B
10/28/19 15:14MMR
P9J0440
Beryllium
<0.30
ug/L
1
1.0
0.30
1
6020B
10/28/19 15:14MMR
P9J0440
Cadmium
<0.22
ug/L
1
1.0
0.22
1
6020B
10/28/19 15:14MMR
P9J0440
Chromium
<0.90
ug/L
10
3.0
0.90
1
6020B
10/28/19 15:14MMR
P9J0440
Cobalt
<0.70
ug/L
10
2.0
0.70
1
6020B
10/28/19 15:14MMR
P9J0440
Copper
<4.7
ug/L
10
10
4.7
1
6020B
10/28/19 15:14MMR
P9J0440
Lead
<0.44
ug/L
10
1.0
0.44
1
6020B
10/28/19 15:14MMR
P9J0440
Nickel
<0.83
ug/L
50
3.0
0.83
1
6020B
10/28/19 15:14MMR
P9J0440
Selenium
<0.98
ug/L
10
5.0
0.98
1
6020B
10/28/19 15:14MMR
P9J0440
Silver
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 15:14MMR
P9J0440
Thallium
<0.84
ug/L
5.5
2.0
0.84
1
6020B
10/28/19 15:14MMR
P9J0440
Tin
<1.9
ug/L
100
5.0
1.9
1
6020B
10/28/19 15:14MMR
P9J0440
Vanadium
<1.5
ug/L
25
5.0
1.5
1
6020B
10/28/19 15:14MMR
P9J0440
Zinc
16 J
ug/L
10
20
10
1
6020B
10/28/19 15:14MMR
P9J0440
Volatile Organic Compounds by GC/MS
1, 1, 1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19 7:47 KDM
P9K0048
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19 7:47 KDM
P91<0048
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
11/2/19 7:47 KDM
P9K0048
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
11/2/19 7:47 KDM
P91<0048
1,1-Dichloroethane
<0.29
ug/L
5
0.50
0.29
1
8260D
11/2/19 7:47 KDM
P9K0048
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19 7:47 KDM
P91<0048
1, 1 -Dichloropropylene
<0.37
ug/L
5
0.50
0.37
1
8260D
11/2/19 7:47 KDM
P9K0048
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
11/2/19 7:47 KDM
P91<0048
1,2,4-Trichlorobenzene
<0.44
ug/L
10
1.0
0.44
1
8260D
11/2/19 7:47 KDM
P9K0048
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
11/2/19 7:47 KDM
P91<0048
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
11/2/19 7:47 KDM
P9K0048
1,2-Dichlorobenzene
<0.28
ug/L
5
0.50
0.28
1
8260D
11/2/19 7:47 KDM
P91<0048
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19 7:47 KDM
P9K0048
1,2-Dichloropropane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19 7:47 KDM
P91<0048
1,3-Dichlorobenzene
<0.40
ug/L
5
0.50
0.40
1
8260D
11/2/19 7:47 KDM
P9K0048
1,3-Dichloropropane
<0.40
ug/L
1
0.50
0.40
1
8260D
11/2/19 7:47 KDM
P91<0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 67

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No.: 50-02
Sample Matrix: Water
Laboratory Report
11/08/2019
Client Sample ID: SW-01
Prism Sample ID: 9100361-03
Prism Work Order: 9100361
Time Collected: 10/22/19 14:05
Time Submitted: 10/23/19 11:03
Parameter
Result Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,4-Dichlorobenzene
<0.42
ug/L
1
0.50
0.42
1
8260D
11/2/19
7:47
KDM
P91<0048
2,2-Dichloropropane
<0.26
ug/L
15
2.0
0.26
1
8260D
11/2/19
7:47
KDM
P9K0048
Acetone
4.8
J ug/L
100
5.0
0.70
1
8260D
11/2/19
7:47
KDM
P9K0048
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
11/2/19
7:47
KDM
P9K0048
Acrolein
<1.2
ug/L
53
20
1.2
1
8260D
11/2/19
7:47
KDM
P91<0048
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
11/2/19
7:47
KDM
P9K0048
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
11/2/19
7:47
KDM
P91<0048
Benzene
<0.34
ug/L
1
0.50
0.34
1
8260D
11/2/19
7:47
KDM
P9K0048
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
11/2/19
7:47
KDM
P91<0048
Bromodichloromethane
<0,29
ug/L
1
0.50
0.29
1
8260D
11/2/19
7:47
KDM
P9K0048
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
11/2/19
7:47
KDM
P91<0048
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
11/2/19
7:47
KDM
P9K0048
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
11/2/19
7:47
KDM
P91<0048
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
11/2/19
7:47
KDM
P91<0048
Chlorobenzene
<0.34
ug/L
3
0.50
0.34
1
8260D
11/2/19
7:47
KDM
P91<0048
Chloroethane
<0.43
ug/L
10
0.50
0.43
1
8260D
11/2/19
7:47
KDM
P9K0048
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
11/2/19
7:47
KDM
P91<0048
Chloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
7:47
KDM
P9K0048
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
11/2/19
7:47
KDM
P91<0048
cis- 1,2-Dichloroethylene
<0.40
ug/L
2
0.50
0.40
1
8260D
11/2/19
7:47
KDM
P9K0048
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
11/2/19
7:47
KDM
P91<0048
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
11/2/19
7:47
KDM
P9K0048
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
11/2/19
7:47
KDM
P91<0048
Dichlorodifluoromethane
<0.47
ug/L
5
5.0
0.47
1
8260D
11/2/19
7:47
KDM
P91<0048
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
11/2/19
7:47
KDM
P91<0048
Ethylbenzene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
7:47
KDM
P9K0048
Hexachlorobutadiene
<0.24
ug/L
10
2.0
0.24
1
8260D
11/2/19
7:47
KDM
P91<0048
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
11/2/19
7:47
KDM
P9K0048
m,p-Xylenes
<0.73
ug/L
NE
1.0
0.73
1
8260D
11/2/19
7:47
KDM
P91<0048
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
11/2/19
7:47
KDM
P9K0048
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
11/2/19
7:47
KDM
P91<0048
Methyl Ethyl Ketone (2-Butanone)
<0.78
ug/L
100
5.0
0.78
1
8260D
11/2/19
7:47
KDM
P9K0048
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
11/2/19
7:47
KDM
P91<0048
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
11/2/19
7:47
KDM
P9K0048
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
11/2/19
7:47
KDM
P91<0048
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1
8260D
11/2/19
7:47
KDM
P9K0048
Naphthalene
<0.45
ug/L
10
1.0
0.45
1
8260D
11/2/19
7:47
KDM
P91<0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 67

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 11/08/2019
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Client Sample ID: SW-01
Attn: Alec Macbeth Samplling Prism Sample ID: 9100361-03
231 Haywood Street Project No.: 50-02 Prism Work Order: 9100361
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/22/19 14:05
Time Submitted: 10/23/19 11:03
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
o-Xylene
<0.40
ug/L
NE
0.50
0.40
1
8260D
11/2/19
7:47
KDM
P91<0048
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
11/2/19
7:47
KDM
P9K0048
Styrene
<0.26
ug/L
1
0.50
0.26
1
8260D
11/2/19
7:47
KDM
P91<0048
Tetrachloroethylene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
7:47
KDM
P9K0048
Tetrahydrofuran
<0.68
ug/L
NE
10
0.68
1
8260D
11/2/19
7:47
KDM
P91<0048
Toluene
<0.35
ug/L
1
0.50
0.35
1
8260D
11/2/19
7:47
KDM
P9K0048
trans- 1,2-Dichloroethylene
<0.27
ug/L
5
0.50
0.27
1
8260D
11/2/19
7:47
KDM
P91<0048
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1
8260D
11/2/19
7:47
KDM
P9K0048
trans- 1,4-Dichloro-2-butene
<0.22
ug/L
100
10
0.22
1
8260D
11/2/19
7:47
KDM
P91<0048
Trichloroethylene
<0.46
ug/L
1
0.50
0.46
1
8260D
11/2/19
7:47
KDM
P9K0048
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1
8260D
11/2/19
7:47
KDM
P91<0048
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1
8260D
11/2/19
7:47
KDM
P9K0048
Vinyl chloride
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19
7:47
KDM
P91<0048
Xylenes, total
<1.1
ug/L
5
1.5
1.1
1
8260D
11/2/19
7:47
KDM
P9K0048
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
80-124
Dibromofluoromethane
101 %
75-129
Toluene-d8
99 %
77-123
Volatile Organic Compounds by GC/MS SIM
1,4-Dioxane
<0.14
ug/L
10
2.0
0.14
1
8260D SIM
10/23/19 18:30TBL
P9J0395
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 13 of 67

�Full-Service Analytical
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
11 /08/2019
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No.: 50-02
Sample Matrix: Water
Client Sample ID: SW-02
Prism Sample ID: 9100361-04
Prism Work Order: 9100361
Time Collected: 10/22/19 14:30
Time Submitted: 10/23/19 11:03
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
General Chemistry Parameters
Hardness 15000 ug/L 5000 570 1 SM2340 C 10/28/19 13:50 BMS P9J0482
Total Metals
Mercury
<0.034
ug/L
0.2
0.20
0.034
1
7470A
10/29/19 16:32JAB
P9J0493
Antimony
<0.93
ug/L
6
3.0
0.93
1
6020B
10/28/19 15:20MMR
P9J0440
Arsenic
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 15:20MMR
P9J0440
Barium
18
ug/L
100
10
3.2
1
6020B
10/28/19 15:20MMR
P9J0440
Beryllium
<0.30
ug/L
1
1.0
0.30
1
6020B
10/28/19 15:20MMR
P9J0440
Cadmium
<0.22
ug/L
1
1.0
0.22
1
6020B
10/28/19 15:20MMR
P9J0440
Chromium
<0.90
ug/L
10
3.0
0.90
1
6020B
10/28/19 15:20MMR
P9J0440
Cobalt
<0.70
ug/L
10
2.0
0.70
1
6020B
10/28/19 15:20MMR
P9J0440
Copper
<4.7
ug/L
10
10
4.7
1
6020B
10/28/19 15:20MMR
P9J0440
Lead
<0.44
ug/L
10
1.0
0.44
1
6020B
10/28/19 15:20MMR
P9J0440
Nickel
<0.83
ug/L
50
3.0
0.83
1
6020B
10/28/19 15:20MMR
P9J0440
Selenium
<0.98
ug/L
10
5.0
0.98
1
6020B
10/28/19 15:20MMR
P9J0440
Silver
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 15:20MMR
P9J0440
Thallium
<0.84
ug/L
5.5
2.0
0.84
1
6020B
10/28/19 15:20MMR
P9J0440
Tin
<1.9
ug/L
100
5.0
1.9
1
6020B
10/28/19 15:20MMR
P9J0440
Vanadium
<1.5
ug/L
25
5.0
1.5
1
6020B
10/28/19 15:20MMR
P9J0440
Zinc
17 J
ug/L
10
20
10
1
6020B
10/28/19 15:20MMR
P9J0440
Volatile Organic Compounds by GC/MS
1, 1, 1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19 8:13 KDM
P9K0048
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19 8:13 KDM
P91<0048
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
11/2/19 8:13 KDM
P9K0048
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
11/2/19 8:13 KDM
P91<0048
1,1-Dichloroethane
<0.29
ug/L
5
0.50
0.29
1
8260D
11/2/19 8:13 KDM
P9K0048
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19 8:13 KDM
P91<0048
1, 1 -Dichloropropylene
<0.37
ug/L
5
0.50
0.37
1
8260D
11/2/19 8:13 KDM
P9K0048
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
11/2/19 8:13 KDM
P91<0048
1,2,4-Trichlorobenzene
<0.44
ug/L
10
1.0
0.44
1
8260D
11/2/19 8:13 KDM
P9K0048
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
11/2/19 8:13 KDM
P91<0048
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
11/2/19 8:13 KDM
P9K0048
1,2-Dichlorobenzene
<0.28
ug/L
5
0.50
0.28
1
8260D
11/2/19 8:13 KDM
P91<0048
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19 8:13 KDM
P9K0048
1,2-Dichloropropane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19 8:13 KDM
P91<0048
1,3-Dichlorobenzene
<0.40
ug/L
5
0.50
0.40
1
8260D
11/2/19 8:13 KDM
P9K0048
1,3-Dichloropropane
<0.40
ug/L
1
0.50
0.40
1
8260D
11/2/19 8:13 KDM
P91<0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 67

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No.: 50-02
Sample Matrix: Water
Laboratory Report
11/08/2019
Client Sample ID: SW-02
Prism Sample ID: 9100361-04
Prism Work Order: 9100361
Time Collected: 10/22/19 14:30
Time Submitted: 10/23/19 11:03
Parameter
Result Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,4-Dichlorobenzene
<0.42
ug/L
1
0.50
0.42
1
8260D
11/2/19
8:13
KDM
P91<0048
2,2-Dichloropropane
<0.26
ug/L
15
2.0
0.26
1
8260D
11/2/19
8:13
KDM
P9K0048
Acetone
3.9
J ug/L
100
5.0
0.70
1
8260D
11/2/19
8:13
KDM
P9K0048
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
11/2/19
8:13
KDM
P9K0048
Acrolein
<1.2
ug/L
53
20
1.2
1
8260D
11/2/19
8:13
KDM
P91<0048
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
11/2/19
8:13
KDM
P9K0048
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
11/2/19
8:13
KDM
P91<0048
Benzene
<0.34
ug/L
1
0.50
0.34
1
8260D
11/2/19
8:13
KDM
P9K0048
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
11/2/19
8:13
KDM
P91<0048
Bromodichloromethane
<0,29
ug/L
1
0.50
0.29
1
8260D
11/2/19
8:13
KDM
P9K0048
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
11/2/19
8:13
KDM
P91<0048
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
11/2/19
8:13
KDM
P9K0048
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
11/2/19
8:13
KDM
P91<0048
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
11/2/19
8:13
KDM
P9K0048
Chlorobenzene
<0.34
ug/L
3
0.50
0.34
1
8260D
11/2/19
8:13
KDM
P91<0048
Chloroethane
<0.43
ug/L
10
0.50
0.43
1
8260D
11/2/19
8:13
KDM
P9K0048
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
11/2/19
8:13
KDM
P91<0048
Chloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
8:13
KDM
P9K0048
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
11/2/19
8:13
KDM
P91<0048
cis- 1,2-Dichloroethylene
<0.40
ug/L
2
0.50
0.40
1
8260D
11/2/19
8:13
KDM
P9K0048
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
11/2/19
8:13
KDM
P91<0048
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
11/2/19
8:13
KDM
P9K0048
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
11/2/19
8:13
KDM
P91<0048
Dichlorodifluoromethane
<0.47
ug/L
5
5.0
0.47
1
8260D
11/2/19
8:13
KDM
P9K0048
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
11/2/19
8:13
KDM
P91<0048
Ethylbenzene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
8:13
KDM
P9K0048
Hexachlorobutadiene
<0.24
ug/L
10
2.0
0.24
1
8260D
11/2/19
8:13
KDM
P91<0048
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
11/2/19
8:13
KDM
P9K0048
m,p-Xylenes
<0.73
ug/L
NE
1.0
0.73
1
8260D
11/2/19
8:13
KDM
P91<0048
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
11/2/19
8:13
KDM
P9K0048
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
11/2/19
8:13
KDM
P91<0048
Methyl Ethyl Ketone (2-Butanone)
<0.78
ug/L
100
5.0
0.78
1
8260D
11/2/19
8:13
KDM
P9K0048
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
11/2/19
8:13
KDM
P91<0048
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
11/2/19
8:13
KDM
P9K0048
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
11/2/19
8:13
KDM
P91<0048
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1
8260D
11/2/19
8:13
KDM
P9K0048
Naphthalene
<0.45
ug/L
10
1.0
0.45
1
8260D
11/2/19
8:13
KDM
P91<0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 67

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 11/08/2019
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Client Sample ID: SW-02
Attn: Alec Macbeth Samplling Prism Sample ID: 9100361-04
231 Haywood Street Project No.: 50-02 Prism Work Order: 9100361
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/22/19 14:30
Time Submitted: 10/23/19 11:03
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
o-Xylene
<0.40
ug/L
NE
0.50
0.40
1
8260D
11/2/19
8:13
KDM
P91<0048
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
11/2/19
8:13
KDM
P9K0048
Styrene
<0.26
ug/L
1
0.50
0.26
1
8260D
11/2/19
8:13
KDM
P91<0048
Tetrachloroethylene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
8:13
KDM
P9K0048
Tetrahydrofuran
<0.68
ug/L
NE
10
0.68
1
8260D
11/2/19
8:13
KDM
P91<0048
Toluene
<0.35
ug/L
1
0.50
0.35
1
8260D
11/2/19
8:13
KDM
P9K0048
trans- 1,2-Dichloroethylene
<0.27
ug/L
5
0.50
0.27
1
8260D
11/2/19
8:13
KDM
P91<0048
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1
8260D
11/2/19
8:13
KDM
P9K0048
trans- 1,4-Dichloro-2-butene
<0.22
ug/L
100
10
0.22
1
8260D
11/2/19
8:13
KDM
P91<0048
Trichloroethylene
<0.46
ug/L
1
0.50
0.46
1
8260D
11/2/19
8:13
KDM
P9K0048
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1
8260D
11/2/19
8:13
KDM
P91<0048
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1
8260D
11/2/19
8:13
KDM
P9K0048
Vinyl chloride
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19
8:13
KDM
P91<0048
Xylenes, total
<1.1
ug/L
5
1.5
1.1
1
8260D
11/2/19
8:13
KDM
P9K0048
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
80-124
Dibromofluoromethane
100 %
75-129
Toluene-d8
99 %
77-123
Volatile Organic Compounds by GC/MS SIM
1,4-Dioxane
<0.14
ug/L
10
2.0
0.14
1
8260D SIM
10/23/19 18:55TBL
P9J0395
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 16 of 67

�Full-Service Analytical
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
11 /08/2019
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No.: 50-02
Sample Matrix: Water
Client Sample ID: LT-01
Prism Sample ID: 9100361-05
Prism Work Order: 9100361
Time Collected: 10/22/19 14:58
Time Submitted: 10/23/19 11:03
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GUMS
1, 1, 1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19
8:39
KDM
P91<0048
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
8:39
KDM
P9K0048
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
11/2/19
8:39
KDM
P91<0048
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
11/2/19
8:39
KDM
P9K0048
1,1-Dichloroethane
<0.29
ug/L
5
0.50
0.29
1
8260D
11/2/19
8:39
KDM
P91<0048
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19
8:39
KDM
P9K0048
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
11/2/19
8:39
KDM
P91<0048
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
11/2/19
8:39
KDM
P9K0048
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
11/2/19
8:39
KDM
P91<0048
1,2-Dichlorobenzene
<0.28
ug/L
5
0.50
0.28
1
8260D
11/2/19
8:39
KDM
P9K0048
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19
8:39
KDM
P91<0048
1,2-Dichloropropane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
8:39
KDM
P9K0048
1,4-Dichlorobenzene
3.7
ug/L
1
0.50
0.42
1
8260D
11/2/19
8:39
KDM
P91(0048
Acetone
6.0
ug/L
100
5.0
0.70
1
8260D
11/2/19
8:39
KDM
P9K0048
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
11/2/19
8:39
KDM
P9K0048
Benzene
1.7
ug/L
1
0.50
0.34
1
8260D
11/2/19
8:39
KDM
P9K0048
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
11/2/19
8:39
KDM
P9K0048
Bromodichloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
8:39
KDM
P9K0048
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
11/2/19
8:39
KDM
P9K0048
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
11/2/19
8:39
KDM
P9K0048
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
11/2/19
8:39
KDM
P9K0048
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
11/2/19
8:39
KDM
P9K0048
Chlorobenzene
3.8
ug/L
3
0.50
0.34
1
8260D
11/2/19
8:39
KDM
P9K0048
Chloroethane
<0.43
ug/L
10
0.50
0.43
1
8260D
11/2/19
8:39
KDM
P9K0048
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
11/2/19
8:39
KDM
P9K0048
Chloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
8:39
KDM
P9K0048
cis- 1,2-Dichloroethylene
<0.40
ug/L
5
0.50
0.40
1
8260D
11/2/19
8:39
KDM
P9K0048
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
11/2/19
8:39
KDM
P9K0048
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
11/2/19
8:39
KDM
P9K0048
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
11/2/19
8:39
KDM
P9K0048
Ethylbenzene
1.6
ug/L
1
0.50
0.31
1
8260D
11/2/19
8:39
KDM
P9K0048
m,p-Xylenes
<0.73
ug/L
NE
1.0
0.73
1
8260D
11/2/19
8:39
KDM
P9K0048
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
11/2/19
8:39
KDM
P91<0048
Methyl Ethyl Ketone (2-Butanone)
<0.78
ug/L
100
5.0
0.78
1
8260D
11/2/19
8:39
KDM
P9K0048
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
11/2/19
8:39
KDM
P91<0048
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
11/2/19
8:39
KDM
P9K0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 67

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 11/08/2019
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Client Sample ID: LT-01
Attn: Alec Macbeth Samplling Prism Sample ID: 9100361-05
231 Haywood Street Project No.: 50-02 Prism Work Order: 9100361
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/22/19 14:58
Time Submitted: 10/23/19 11:03
Parameter
Result
Units
SWSL
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1
8260D
11/2/19
8:39
KDM
P91<0048
o-Xylene
1.1
ug/L
NE
0.50
0.40
1
8260D
11/2/19
8:39
KDM
P91<0048
Styrene
<0.26
ug/L
1
0.50
0.26
1
8260D
11/2/19
8:39
KDM
P91<0048
Tetrachloroethylene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
8:39
KDM
P91<0048
Toluene
0.39 j
ug/L
1
0.50
0.35
1
8260D
11/2/19
8:39
KDM
P9K0048
trans- 1,2-Dichloroethylene
<0.27
ug/L
5
0.50
0.27
1
8260D
11/2/19
8:39
KDM
P91<0048
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1
8260D
11/2/19
8:39
KDM
P91<0048
trans- IIA-Dich loro-2-butene
<0.22
ug/L
100
10
0.22
1
8260D
11/2/19
8:39
KDM
P91<0048
Trichloroethylene
<0.46
ug/L
1
0.50
0.46
1
8260D
11/2/19
8:39
KDM
P91<0048
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1
8260D
11/2/19
8:39
KDM
P91<0048
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1
8260D
11/2/19
8:39
KDM
P91<0048
Vinyl chloride
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19
8:39
KDM
P91<0048
Xylenes, total
1.7
ug/L
5
1.5
1.1
1
8260D
11/2/19
8:39
KDM
P9K0048
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
98 %
80-124
Dibromofluoromethane
100 %
75-129
Toluene-d8
99 %
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 18 of 67

�Full-Service Analytical s
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
11 /08/2019
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No.: 50-02
Sample Matrix: Water
Client Sample ID: TB-01
Prism Sample ID: 9100361-06
Prism Work Order: 9100361
Time Collected: 10/22/19 00:00
Time Submitted: 10/23/19 11:03
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GUMS
1, 1, 1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19
3:00
KDM
P91<0048
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
3:00
KDM
P9K0048
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
11/2/19
3:00
KDM
P91<0048
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
11/2/19
3:00
KDM
P9K0048
1,1-Dichloroethane
<0.29
ug/L
5
0.50
0.29
1
8260D
11/2/19
3:00
KDM
P91<0048
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19
3:00
KDM
P9K0048
1, 1 -Dichloropropylene
<0.37
ug/L
5
0.50
0.37
1
8260D
11/2/19
3:00
KDM
P91<0048
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
11/2/19
3:00
KDM
P9K0048
1,2,4-Trichlorobenzene
<0.44
ug/L
10
1.0
0.44
1
8260D
11/2/19
3:00
KDM
P91<0048
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
11/2/19
3:00
KDM
P9K0048
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
11/2/19
3:00
KDM
P91<0048
1,2-Dichlorobenzene
<0.28
ug/L
5
0.50
0.28
1
8260D
11/2/19
3:00
KDM
P9K0048
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19
3:00
KDM
P91<0048
1,2-Dichloropropane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
3:00
KDM
P9K0048
1,3-Dichlorobenzene
<0.40
ug/L
5
0.50
0.40
1
8260D
11/2/19
3:00
KDM
P91<0048
1,3-Dichloropropane
<0.40
ug/L
1
0.50
0.40
1
8260D
11/2/19
3:00
KDM
P9K0048
1,4-Dichlorobenzene
<0.42
ug/L
1
0.50
0.42
1
8260D
11/2/19
3:00
KDM
P91<0048
2,2-Dichloropropane
<0.26
ug/L
15
2.0
0.26
1
8260D
11/2/19
3:00
KDM
P9K0048
Acetone
2.7 1
ug/L
100
5.0
0.70
1
8260D
11/2/19
3:00
KDM
P9K0048
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
11/2/19
3:00
KDM
P9K0048
Acrolein
<1.2
ug/L
53
20
1.2
1
8260D
11/2/19
3:00
KDM
P91<0048
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
11/2/19
3:00
KDM
P9K0048
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
11/2/19
3:00
KDM
P91<0048
Benzene
<0.34
ug/L
1
0.50
0.34
1
8260D
11/2/19
3:00
KDM
P9K0048
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
11/2/19
3:00
KDM
P91<0048
Bromodichloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
3:00
KDM
P9K0048
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
11/2/19
3:00
KDM
P91<0048
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
11/2/19
3:00
KDM
P9K0048
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
11/2/19
3:00
KDM
P91<0048
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
11/2/19
3:00
KDM
P9K0048
Chlorobenzene
<0.34
ug/L
3
0.50
0.34
1
8260D
11/2/19
3:00
KDM
P91<0048
Chloroethane
<0.43
ug/L
10
0.50
0.43
1
8260D
11/2/19
3:00
KDM
P9K0048
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
11/2/19
3:00
KDM
P91<0048
Chloromethane
0.57
ug/L
1
0.50
0.29
1
8260D
11/2/19
3:00
KDM
P9K0048
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
11/2/19
3:00
KDM
P9K0048
cis- 1,2-Dichloroethylene
<0.40
ug/L
2
0.50
0.40
1
8260D
11/2/19
3:00
KDM
P91<0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 67

Laboratory Report
Full -Service Analytical &
P R S M
Environmental Solutions
LABORATORIES INC.
11/08/2019
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2019
Fall
Client
Sample ID:
TB-01
Attn: Alec Macbeth
Samplling
Prism
Sample ID:
9100361-06
231 Haywood Street
Project No.:
50-02
Prism
Work Order:
9100361
Asheville, NC 28801
Sample Matrix:
Water
Time
Collected: 10/22/19 00:00
Time
Submitted: 10/23/19
11:03
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
11/2/19
3:00
KDM
P91<0048
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
11/2/19
3:00
KDM
P9K0048
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
11/2/19
3:00
KDM
P91<0048
Dichlorodifluoromethane
<0.47
ug/L
5
5.0
0.47
1
8260D
11/2/19
3:00
KDM
P9K0048
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
11/2/19
3:00
KDM
P91<0048
Ethylbenzene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
3:00
KDM
P9K0048
Hexachlorobutadiene
<0.24
ug/L
10
2.0
0.24
1
8260D
11/2/19
3:00
KDM
P91<0048
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
11/2/19
3:00
KDM
P9K0048
m,p-Xylenes
<0.73
ug/L
NE
1.0
0.73
1
8260D
11/2/19
3:00
KDM
P91<0048
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
11/2/19
3:00
KDM
P9K0048
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
11/2/19
3:00
KDM
P91<0048
Methyl Ethyl Ketone (2-Butanone)
<0,78
ug/L
100
5.0
0.78
1
8260D
11/2/19
3:00
KDM
P9K0048
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
11/2/19
3:00
KDM
P91<0048
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
11/2/19
3:00
KDM
P9K0048
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
11/2/19
3:00
KDM
P91<0048
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1
8260D
11/2/19
3:00
KDM
P9K0048
Naphthalene
<0.45
ug/L
10
1.0
0.45
1
8260D
11/2/19
3:00
KDM
P91<0048
o-Xylene
<0.40
ug/L
NE
0.50
0.40
1
8260D
11/2/19
3:00
KDM
P9K0048
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
11/2/19
3:00
KDM
P91<0048
Styrene
<0.26
ug/L
1
0.50
0.26
1
8260D
11/2/19
3:00
KDM
P9K0048
Tetrachloroethylene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
3:00
KDM
P91<0048
Tetrahydrofuran
<0.68
ug/L
NE
10
0.68
1
8260D
11/2/19
3:00
KDM
P9K0048
Toluene
<0.35
ug/L
1
0.50
0.35
1
8260D
11/2/19
3:00
KDM
P91<0048
trans- 1,2-Dichloroethylene
<0.27
ug/L
5
0.50
0.27
1
8260D
11/2/19
3:00
KDM
P9K0048
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1
8260D
11/2/19
3:00
KDM
P91<0048
trans- 1,4-Dich loro-2-butene
<0.22
ug/L
100
10
0.22
1
8260D
11/2/19
3:00
KDM
P9K0048
Trichloroethylene
<0.46
ug/L
1
0.50
0.46
1
8260D
11/2/19
3:00
KDM
P91<0048
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1
8260D
11/2/19
3:00
KDM
P9K0048
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1
8260D
11/2/19
3:00
KDM
P91<0048
Vinyl chloride
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19
3:00
KDM
P9K0048
Xylenes, total
<1.1
ug/L
5
1.5
1.1
1
8260D
11/2/19
3:00
KDM
P91<0048
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
99 %
80-124
Dibromofluoromethane
100 %
75-129
Toluene-d8
100 %
77-123
Volatile Organic Compounds by GUMS SIM
1,4-Dioxane
<0.14
ug/L
10
2.0
0.14
1
8260D SIM
10/23/19 17:15TBL
P9J0395
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 67

Full -Service Analytical &
14LANKO�TORIES�
S M Environmental Solutions
INC.
Level II QC Report
11/8/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall
Attn: Alec Macbeth Samplling
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Prism Work Order: 9100361
Time Submitted: 10/23/2019 11:03:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9K0048 - 5030B
Blank (P9K0048-BLK1)
Prepared: 11/01/19 Analyzed: 11/02/19
1,1,1,2-Tetrachloroethane
BRL
0.50
ug/L
1,1,1,2-Tetrachloroethane
BRL
0.50
ug/L
1,1,1-Trichloroethane
BRL
0.50
ug/L
1,1,1-Trichloroethane
BRL
0.50
ug/L
1,1,2,2-Tetrachloroethane
BRL
0.50
ug/L
1,1,2,2-Tetrachloroethane
BRL
0.50
ug/L
1,1,2-Trichloroethane
BRL
0.50
ug/L
1,1,2-Trichloroethane
BRL
0.50
ug/L
1,1-Dichloroethane
BRL
0.50
ug/L
1,1-Dichloroethane
BRL
0.50
ug/L
1,1-Dichloroethylene
BRL
0.50
ug/L
1,1-Dichloroethylene
BRL
0.50
ug/L
1, 1 -Dichloropropylene
BRL
0.50
ug/L
1,2,3-Trichloropropane
BRL
1.0
ug/L
1,2,3-Trichloropropane
BRL
1.0
ug/L
1,2,4-Trichlorobenzene
BRL
1.0
ug/L
1,2-Dibromo-3-chloropropane
BRL
2.0
ug/L
1,2-Dibromo-3-chloropropane
BRL
2.0
ug/L
1,2-Dibromoethane
BRL
0.50
ug/L
1,2-Dibromoethane
BRL
0.50
ug/L
1,2-Dichlorobenzene
BRL
0.50
ug/L
1,2-Dichlorobenzene
BRL
0.50
ug/L
1,2-Dichloroethane
BRL
0.50
ug/L
1,2-Dichloroethane
BRL
0.50
ug/L
1,2-Dichloropropane
BRL
0.50
ug/L
1,2-Dichloropropane
BRL
0.50
ug/L
1,3-Dichlorobenzene
BRL
0.50
ug/L
1,3-Dichloropropane
BRL
0.50
ug/L
1,4-Dichlorobenzene
BRL
0.50
ug/L
1,4-Dichlorobenzene
BRL
0.50
ug/L
2,2-Dichloropropane
BRL
2.0
ug/L
Acetone
BRL
5.0
ug/L
Acetone
BRL
5.0
ug/L
Acetonitrile
BRL
10
ug/L
Acrolein
BRL
20
ug/L
Acrylonitrile
BRL
20
ug/L
Acrylonitrile
BRL
20
ug/L
Allyl Chloride (3-Chloropropylene)
BRL
10
ug/L
Benzene
BRL
0.50
ug/L
Benzene
BRL
0.50
ug/L
Bromochloromethane
BRL
2.0
ug/L
Bromochloromethane
BRL
2.0
ug/L
Bromodichloromethane
BRL
0.50
ug/L
Bromodichloromethane
BRL
0.50
ug/L
Bromoform
BRL
1.0
ug/L
Bromoform
BRL
1.0
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 21 of 67

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/8/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Prism Work Order: 9100361
Attn: Alec Macbeth Samplling Time Submitted: 10/23/2019 11:03:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9KO048 - 5030B
Blank (1391<0048-BLK1)
Prepared: 11/01/19 Analyzed: 11/02/19
Bromomethane
BRL
1.0
ug/L
Bromomethane
BRL
1.0
ug/L
Carbon disulfide
BRL
5.0
ug/L
Carbon disulfide
BRL
5.0
ug/L
Carbon Tetrachloride
BRL
2.0
ug/L
Carbon Tetrachloride
BRL
2.0
ug/L
Chlorobenzene
BRL
0.50
ug/L
Chlorobenzene
BRL
0.50
ug/L
Chloroethane
BRL
0.50
ug/L
Chloroethane
BRL
0.50
ug/L
Chloroform
BRL
0.50
ug/L
Chloroform
BRL
0.50
ug/L
Chloromethane
BRL
0.50
ug/L
Chloromethane
BRL
0.50
ug/L
Chloroprene
BRL
10
ug/L
cis-1,2-Dichloroethylene
BRL
0.50
ug/L
cis-1,2-Dichloroethylene
BRL
0.50
ug/L
cis-1,3-Dichloropropylene
BRL
0.50
ug/L
cis-1,3-Dichloropropylene
BRL
0.50
ug/L
Dibromochloromethane
BRL
0.50
ug/L
Dibromochloromethane
BRL
0.50
ug/L
Dibromomethane
BRL
2.0
ug/L
Dibromomethane
BRL
2.0
ug/L
Dichlorodifluoromethane
BRL
5.0
ug/L
Ethyl Methacrylate
BRL
10
ug/L
Ethylbenzene
BRL
0.50
ug/L
Ethylbenzene
BRL
0.50
ug/L
Hexachlorobutadiene
BRL
2.0
ug/L
Isobutyl alcohol
BRL
50
ug/L
m,p-Xylenes
BRL
1.0
ug/L
m,p-Xylenes
BRL
1.0
ug/L
Methacrylonitrile
BRL
10
ug/L
Methyl Butyl Ketone (2-Hexanone)
BRL
5.0
ug/L
Methyl Butyl Ketone (2-Hexanone)
BRL
5.0
ug/L
Methyl Ethyl Ketone (2-Butanone)
BRL
5.0
ug/L
Methyl Ethyl Ketone (2-Butanone)
BRL
5.0
ug/L
Methyl Iodide
BRL
5.0
ug/L
Methyl Iodide
BRL
5.0
ug/L
Methyl Isobutyl Ketone
BRL
5.0
ug/L
Methyl Isobutyl Ketone
BRL
5.0
ug/L
Methyl Methacrylate
BRL
10
ug/L
Methylene Chloride
BRL
1.0
ug/L
Methylene Chloride
BRL
1.0
ug/L
Naphthalene
BRL
1.0
ug/L
o-Xylene
BRL
0.50
ug/L
o-Xylene
BRL
0.50
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 67

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/8/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall
Attn: Alec Macbeth Samplling
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Prism Work Order: 9100361
Time Submitted: 10/23/2019 11:03:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9KO048 - 5030B
Blank (P9K0048-BLK1)
Prepared: 11/01/19 Analyzed:
11/02/19
Propionitrile (Ethyl Cyanide)
BRL
10
ug/L
Styrene
BRL
0.50
ug/L
Styrene
BRL
0.50
ug/L
Tetrachloroethylene
BRL
0.50
ug/L
Tetrachloroethylene
BRL
0.50
ug/L
Tetrahydrofuran
BRL
10
ug/L
Toluene
BRL
0.50
ug/L
Toluene
BRL
0.50
ug/L
trans-1,2-Dichloroethylene
BRL
0.50
ug/L
trans-1,2-Dichloroethylene
BRL
0.50
ug/L
trans-1,3-Dichloropropylene
BRL
0.50
ug/L
trans-1,3-Dichloropropylene
BRL
0.50
ug/L
trans-1,4-Dichloro-2-butene
BRL
10
ug/L
trans-1,4-Dichloro-2-butene
BRL
10
ug/L
Trichloroethylene
BRL
0.50
ug/L
Trichloroethylene
BRL
0.50
ug/L
Trichlorofluoromethane
BRL
0.50
ug/L
Trichlorofluoromethane
BRL
0.50
ug/L
Vinyl acetate
BRL
2.0
ug/L
Vinyl acetate
BRL
2.0
ug/L
Vinyl chloride
BRL
0.50
ug/L
Vinyl chloride
BRL
0.50
ug/L
Xylenes, total
BRL
1.5
ug/L
Xylenes, total
BRL
1.5
ug/L
Surrogate:4-Bromofluorobenzene
49.4
ug/L
50.00
99
80-124
Surrogate:4-Bromofluorobenzene
49.4
ug/L
50.00
99
80-124
Surrogate: Dibromofluoromethane
49.0
ug/L
50.00
98
75-129
Surrogate: Dibromofluoromethane
49.0
ug/L
50.00
98
75-129
Surrogate: Toluene-d8
50.2
ug/L
50.00
100
77-123
Surrogate: Toluene-d8
50.2
ug/L
50.00
100
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 67

P R I S M Full -Service Analytical s
Environmental Solutions
LABCFATCRIES, NC.
Level II QC Report
11/8/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall
Attn: Alec Macbeth Samplling
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Prism Work Order: 9100361
Time Submitted: 10/23/2019 11:03:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P91<0048 - 5030B
LCS (P9K0048-BSI)
Prepared: 11/01/19 Analyzed: 11/02/19
1,1,1,2-Tetrachloroethane
20.6
0.50
ug/L
20.00
103
79-134
1,1,1,2-Tetrachloroethane
20.6
0.50
ug/L
20.00
103
79-134
1,1,1-Trichloroethane
21.2
0.50
ug/L
20.00
106
75-136
1,1,1-Trichloroethane
21.2
0.50
ug/L
20.00
106
75-136
1,1,2,2-Tetrachloroethane
21.0
0.50
ug/L
20.00
105
62-127
1,1,2,2-Tetrachloroethane
21.0
0.50
ug/L
20.00
105
62-127
1,1,2-Trichloroethane
20.8
0.50
ug/L
20.00
104
70-140
1,1,2-Trichloroethane
20.8
0.50
ug/L
20.00
104
70-140
1,1-Dichloroethane
20.6
0.50
ug/L
20.00
103
78-130
1,1-Dichloroethane
20.6
0.50
ug/L
20.00
103
78-130
1,1-Dichloroethylene
21.2
0.50
ug/L
20.00
106
70-154
1,1-Dichloroethylene
21.2
0.50
ug/L
20.00
106
70-154
1, 1 -Dichloropropylene
22.6
0.50
ug/L
20.00
113
71-136
1,2,3-Trichloropropane
20.5
1.0
ug/L
20.00
102
71-127
1,2,3-Trichloropropane
20.5
1.0
ug/L
20.00
102
71-127
1,2,4-Trichlorobenzene
21.3
1.0
ug/L
20.00
107
66-139
1,2-Dibromo-3-chloropropane
21.1
2.0
ug/L
20.00
106
63-134
1,2-Dibromo-3-chloropropane
21.1
2.0
ug/L
20.00
106
63-134
1,2-Dibromoethane
21.2
0.50
ug/L
20.00
106
77-135
1,2-Dibromoethane
21.2
0.50
ug/L
20.00
106
77-135
1,2-Dichlorobenzene
20.8
0.50
ug/L
20.00
104
78-128
1,2-Dichlorobenzene
20.8
0.50
ug/L
20.00
104
78-128
1,2-Dichloroethane
19.6
0.50
ug/L
20.00
98
68-131
1,2-Dichloroethane
19.6
0.50
ug/L
20.00
98
68-131
1,2-Dichloropropane
20.7
0.50
ug/L
20.00
103
77-130
1,2-Dichloropropane
20.7
0.50
ug/L
20.00
103
77-130
1,3-Dichlorobenzene
20.3
0.50
ug/L
20.00
102
77-125
1,3-Dichloropropane
21.3
0.50
ug/L
20.00
106
76-132
1,4-Dichlorobenzene
20.3
0.50
ug/L
20.00
102
75-126
1,4-Dichlorobenzene
20.3
0.50
ug/L
20.00
102
75-126
2,2-Dichloropropane
20.3
2.0
ug/L
20.00
102
29-149
Acetone
40.2
5.0
ug/L
40.00
101
40-166
Acetone
40.2
5.0
ug/L
40.00
101
40-166
Acetonitrile
21.3
10
ug/L
20.00
106
70-130
Acrolein
41.6
20
ug/L
40.00
104
70-130
Acrylonitrile
37.3
20
ug/L
40.00
93
81-127
Acrylonitrile
37.3
20
ug/L
40.00
93
81-127
Allyl Chloride (3-Chloropropylene)
18.8
10
ug/L
20.00
94
70-130
Benzene
20.3
0.50
ug/L
20.00
101
77-128
Benzene
20.3
0.50
ug/L
20.00
101
77-128
Bromochloromethane
20.8
2.0
ug/L
20.00
104
78-135
Bromochloromethane
20.8
2.0
ug/L
20.00
104
78-135
Bromodichloromethane
20.9
0.50
ug/L
20.00
104
76-138
Bromodichloromethane
20.9
0.50
ug/L
20.00
104
76-138
Bromoform
21.9
1.0
ug/L
20.00
109
71-135
Bromoform
21.9
1.0
ug/L
20.00
109
71-135
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 67

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/8/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Prism Work Order: 9100361
Attn: Alec Macbeth Samplling Time Submitted: 10/23/2019 11:03:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9KO048 - 5030B
LCS (P9K0048-BSI)
Prepared: 11/01/19 Analyzed: 11/02/19
Bromomethane
28.7
1.0
ug/L
20.00
143
41-168
Bromomethane
28.7
1.0
ug/L
20.00
143
41-168
Carbon disulfide
22.2
5.0
ug/L
20.00
111
59-135
Carbon disulfide
22.2
5.0
ug/L
20.00
111
59-135
Carbon Tetrachloride
21.8
2.0
ug/L
20.00
109
72-142
Carbon Tetrachloride
21.8
2.0
ug/L
20.00
109
72-142
Chlorobenzene
20.0
0.50
ug/L
20.00
100
78-119
Chlorobenzene
20.0
0.50
ug/L
20.00
100
78-119
Chloroethane
20.4
0.50
ug/L
20.00
102
57-142
Chloroethane
20.4
0.50
ug/L
20.00
102
57-142
Chloroform
20.1
0.50
ug/L
20.00
101
77-130
Chloroform
20.1
0.50
ug/L
20.00
101
77-130
Chloromethane
23.9
0.50
ug/L
20.00
120
47-145
Chloromethane
23.9
0.50
ug/L
20.00
120
47-145
Chloroprene
21.0
10
ug/L
20.00
105
70-130
cis-1,2-Dichloroethylene
19.4
0.50
ug/L
20.00
97
76-141
cis-1,2-Dichloroethylene
19.4
0.50
ug/L
20.00
97
76-141
cis-1,3-Dichloropropylene
22.2
0.50
ug/L
20.00
111
65-140
cis-1,3-Dichloropropylene
22.2
0.50
ug/L
20.00
111
65-140
Dibromochloromethane
21.5
0.50
ug/L
20.00
107
75-134
Dibromochloromethane
21.5
0.50
ug/L
20.00
107
75-134
Dibromomethane
20.7
2.0
ug/L
20.00
104
76-138
Dibromomethane
20.7
2.0
ug/L
20.00
104
76-138
Dichlorodifluoromethane
26.4
5.0
ug/L
20.00
132
28-163
Ethyl Methacrylate
20.8
10
ug/L
20.00
104
70-130
Ethylbenzene
20.8
0.50
ug/L
20.00
104
80-127
Ethylbenzene
20.8
0.50
ug/L
20.00
104
80-127
Hexachlorobutadiene
21.9
2.0
ug/L
20.00
110
61-134
Isobutyl alcohol
20.0
50
ug/L
20.00
100
70-130 J
m,p-Xylenes
42.6
1.0
ug/L
40.00
107
77-133
m,p-Xylenes
42.6
1.0
ug/L
40.00
107
77-133
Methacrylonitrile
20.0
10
ug/L
20.00
100
70-130
Methyl Butyl Ketone (2-Hexanone)
21.5
5.0
ug/L
20.00
108
64-137
Methyl Butyl Ketone (2-Hexanone)
21.5
5.0
ug/L
20.00
108
64-137
Methyl Ethyl Ketone (2-Butanone)
19.8
5.0
ug/L
20.00
99
71-134
Methyl Ethyl Ketone (2-Butanone)
19.8
5.0
ug/L
20.00
99
71-134
Methyl Iodide
21.2
5.0
ug/L
20.00
106
70-130
Methyl Iodide
21.2
5.0
ug/L
20.00
106
70-130
Methyl Isobutyl Ketone
20.7
5.0
ug/L
20.00
104
69-134
Methyl Isobutyl Ketone
20.7
5.0
ug/L
20.00
104
69-134
Methyl Methacrylate
20.9
10
ug/L
20.00
104
70-130
Methylene Chloride
18.7
1.0
ug/L
20.00
93
73-131
Methylene Chloride
18.7
1.0
ug/L
20.00
93
73-131
Naphthalene
21.8
1.0
ug/L
20.00
109
64-136
o-Xylene
20.9
0.50
ug/L
20.00
105
78-128
o-Xylene
20.9
0.50
ug/L
20.00
105
78-128
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 67

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/8/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Prism Work Order: 9100361
Attn: Alec Macbeth Samplling Time Submitted: 10/23/2019 11:03:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9KO048 - 5030B
LCS (P9K0048-BSI)
Prepared: 11/01/19 Analyzed: 11/02/19
Propionitrile (Ethyl Cyanide)
20.3
10
ug/L
20.00
101
70-130
Styrene
22.0
0.50
ug/L
20.00
110
78-129
Styrene
22.0
0.50
ug/L
20.00
110
78-129
Tetrachloroethylene
21.9
0.50
ug/L
20.00
110
80-129
Tetrachloroethylene
21.9
0.50
ug/L
20.00
110
80-129
Tetrahydrofuran
19.4
10
ug/L
20.00
97
70-130
Toluene
20.6
0.50
ug/L
20.00
103
76-131
Toluene
20.6
0.50
ug/L
20.00
103
76-131
trans-1,2-Dichloroethylene
20.0
0.50
ug/L
20.00
100
76-135
trans-1,2-Dichloroethylene
20.0
0.50
ug/L
20.00
100
76-135
trans-1,3-Dichloropropylene
21.8
0.50
ug/L
20.00
109
67-140
trans-1,3-Dichloropropylene
21.8
0.50
ug/L
20.00
109
67-140
trans-1,4-Dichloro-2-butene
20.0
10
ug/L
20.00
100
70-130
trans-1,4-Dichloro-2-butene
20.0
10
ug/L
20.00
100
70-130
Trichloroethylene
20.4
0.50
ug/L
20.00
102
77-133
Trichloroethylene
20.4
0.50
ug/L
20.00
102
77-133
Trichlorofluoromethane
23.6
0.50
ug/L
20.00
118
62-148
Trichlorofluoromethane
23.6
0.50
ug/L
20.00
118
62-148
Vinyl acetate
21.4
2.0
ug/L
20.00
107
34-167
Vinyl acetate
21.4
2.0
ug/L
20.00
107
34-167
Vinyl chloride
22.6
0.50
ug/L
20.00
113
57-141
Vinyl chloride
22.6
0.50
ug/L
20.00
113
57-141
Xylenes, total
63.6
1.5
ug/L
60.00
106
77-133
Xylenes, total
63.6
1.5
ug/L
60.00
106
77-133
Surrogate:4-Bromofluorobenzene
50.1
ug/L
50.00
100
80-124
Surrogate:4-Bromofluorobenzene
50.1
ug/L
50.00
100
80-124
Surrogate: Dibromofluoromethane
49.0
ug/L
50.00
98
75-129
Surrogate: Dibromofluoromethane
49.0
ug/L
50.00
98
75-129
Surrogate: Toluene-d8
50.6
ug/L
50.00
101
77-123
Surrogate: Toluene-d8
50.6
ug/L
50.00
101
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 26 of 67

P R I S M Full -Service Analytical s
Environmental Solutions
LABCFATCRIES, NC.
Level II QC Report
11/8/19
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No: 50-02
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P91<0048 - 5030B
Prism Work Order: 9100361
Time Submitted: 10/23/2019 11:03:OOAM
Reporting Spike Source
Result Limit Units Level Result %REC
%REC RPD
Limits RPD Limit
Notes
LCS Dup (P9K0048-BSD1)
Prepared: 11/01/19 Analyzed: 11/02/19
1,1,1,2-Tetrachloroethane
20.4
0.50
ug/L
20.00
102
79-134
1
20
1,1,1,2-Tetrachloroethane
20.4
0.50
ug/L
20.00
102
79-134
1
20
1,1,1-Trichloroethane
20.7
0.50
ug/L
20.00
103
75-136
3
20
1,1,1-Trichloroethane
20.7
0.50
ug/L
20.00
103
75-136
3
20
1,1,2,2-Tetrachloroethane
21.4
0.50
ug/L
20.00
107
62-127
2
20
1,1,2,2-Tetrachloroethane
21.4
0.50
ug/L
20.00
107
62-127
2
20
1,1,2-Trichloroethane
20.6
0.50
ug/L
20.00
103
70-140
0.9
20
1,1,2-Trichloroethane
20.6
0.50
ug/L
20.00
103
70-140
0.9
20
1,1-Dichloroethane
20.2
0.50
ug/L
20.00
101
78-130
2
20
1,1-Dichloroethane
20.2
0.50
ug/L
20.00
101
78-130
2
20
1,1-Dichloroethylene
20.6
0.50
ug/L
20.00
103
70-154
3
20
1,1-Dichloroethylene
20.6
0.50
ug/L
20.00
103
70-154
3
20
1, 1 -Dichloropropylene
21.7
0.50
ug/L
20.00
108
71-136
4
20
1,2,3-Trichloropropane
21.4
1.0
ug/L
20.00
107
71-127
4
20
1,2,3-Trichloropropane
21.4
1.0
ug/L
20.00
107
71-127
4
20
1,2,4-Trichlorobenzene
21.0
1.0
ug/L
20.00
105
66-139
2
20
1,2-Dibromo-3-chloropropane
22.4
2.0
ug/L
20.00
112
63-134
6
20
1,2-Dibromo-3-chloropropane
22.4
2.0
ug/L
20.00
112
63-134
6
20
1,2-Dibromoethane
21.3
0.50
ug/L
20.00
107
77-135
0.6
20
1,2-Dibromoethane
21.3
0.50
ug/L
20.00
107
77-135
0.6
20
1,2-Dichlorobenzene
20.8
0.50
ug/L
20.00
104
78-128
0.05
20
1,2-Dichlorobenzene
20.8
0.50
ug/L
20.00
104
78-128
0.05
20
1,2-Dichloroethane
19.2
0.50
ug/L
20.00
96
68-131
2
20
1,2-Dichloroethane
19.2
0.50
ug/L
20.00
96
68-131
2
20
1,2-Dichloropropane
20.4
0.50
ug/L
20.00
102
77-130
1
20
1,2-Dichloropropane
20.4
0.50
ug/L
20.00
102
77-130
1
20
1,3-Dichlorobenzene
20.0
0.50
ug/L
20.00
100
77-125
1
20
1,3-Dichloropropane
21.2
0.50
ug/L
20.00
106
76-132
0.4
20
1,4-Dichlorobenzene
20.0
0.50
ug/L
20.00
100
75-126
2
20
1,4-Dichlorobenzene
20.0
0.50
ug/L
20.00
100
75-126
2
20
2,2-Dichloropropane
19.6
2.0
ug/L
20.00
98
29-149
4
20
Acetone
42.3
5.0
ug/L
40.00
106
40-166
5
20
Acetone
42.3
5.0
ug/L
40.00
106
40-166
5
20
Acetonitrile
21.5
10
ug/L
20.00
107
70-130
1
20
Acrolein
43.1
20
ug/L
40.00
108
70-130
4
20
Acrylonitrile
39.4
20
ug/L
40.00
98
81-127
5
20
Acrylonitrile
39.4
20
ug/L
40.00
98
81-127
5
20
Allyl Chloride (3-Chloropropylene)
18.5
10
ug/L
20.00
93
70-130
2
20
Benzene
19.9
0.50
ug/L
20.00
100
77-128
2
20
Benzene
19.9
0.50
ug/L
20.00
100
77-128
2
20
Bromochloromethane
20.6
2.0
ug/L
20.00
103
78-135
1
20
Bromochloromethane
20.6
2.0
ug/L
20.00
103
78-135
1
20
Bromodichloromethane
20.7
0.50
ug/L
20.00
103
76-138
1
20
Bromodichloromethane
20.7
0.50
ug/L
20.00
103
76-138
1
20
Bromoform
22.4
1.0
ug/L
20.00
112
71-135
2
20
Bromoform
22.4
1.0
ug/L
20.00
112
71-135
2
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 of 67

P R I S M Full -Service Analytical s
Environmental Solutions
LABCFATCRIES, NC.
Level II QC Report
11/8/19
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No: 50-02
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P91<0048 - 5030B
Prism Work Order: 9100361
Time Submitted: 10/23/2019 11:03:OOAM
Reporting Spike Source
Result Limit Units Level Result %REC
%REC RPD
Limits RPD Limit
Notes
LCS Dup (P9K0048-BSD1)
Prepared: 11/01/19 Analyzed: 11/02/19
Bromomethane
26.6
1.0
ug/L
20.00
133
41-168
8
20
Bromomethane
26.6
1.0
ug/L
20.00
133
41-168
8
20
Carbon disulfide
21.4
5.0
ug/L
20.00
107
59-135
4
20
Carbon disulfide
21.4
5.0
ug/L
20.00
107
59-135
4
20
Carbon Tetrachloride
21.1
2.0
ug/L
20.00
105
72-142
4
20
Carbon Tetrachloride
21.1
2.0
ug/L
20.00
105
72-142
4
20
Chlorobenzene
19.6
0.50
ug/L
20.00
98
78-119
2
20
Chlorobenzene
19.6
0.50
ug/L
20.00
98
78-119
2
20
Chloroethane
19.7
0.50
ug/L
20.00
99
57-142
3
20
Chloroethane
19.7
0.50
ug/L
20.00
99
57-142
3
20
Chloroform
20.0
0.50
ug/L
20.00
100
77-130
0.7
20
Chloroform
20.0
0.50
ug/L
20.00
100
77-130
0.7
20
Chloromethane
25.1
0.50
ug/L
20.00
125
47-145
5
20
Chloromethane
25.1
0.50
ug/L
20.00
125
47-145
5
20
Chloroprene
20.3
10
ug/L
20.00
102
70-130
3
20
cis-1,2-Dichloroethylene
19.0
0.50
ug/L
20.00
95
76-141
2
20
cis-1,2-Dichloroethylene
19.0
0.50
ug/L
20.00
95
76-141
2
20
cis-1,3-Dichloropropylene
21.8
0.50
ug/L
20.00
109
65-140
2
20
cis-1,3-Dichloropropylene
21.8
0.50
ug/L
20.00
109
65-140
2
20
Dibromochloromethane
21.3
0.50
ug/L
20.00
107
75-134
0.7
20
Dibromochloromethane
21.3
0.50
ug/L
20.00
107
75-134
0.7
20
Dibromomethane
20.7
2.0
ug/L
20.00
103
76-138
0.1
20
Dibromomethane
20.7
2.0
ug/L
20.00
103
76-138
0.1
20
Dichlorodifluoromethane
24.6
5.0
ug/L
20.00
123
28-163
7
20
Ethyl Methacrylate
21.1
10
ug/L
20.00
105
70-130
1
20
Ethylbenzene
20.4
0.50
ug/L
20.00
102
80-127
2
20
Ethylbenzene
20.4
0.50
ug/L
20.00
102
80-127
2
20
Hexachlorobutadiene
20.8
2.0
ug/L
20.00
104
61-134
5
20
Isobutyl alcohol
20.7
50
ug/L
20.00
103
70-130
4
20 1
m,p-Xylenes
41.8
1.0
ug/L
40.00
104
77-133
2
20
m,p-Xylenes
41.8
1.0
ug/L
40.00
104
77-133
2
20
Methacrylonitrile
20.7
10
ug/L
20.00
104
70-130
3
20
Methyl Butyl Ketone (2-Hexanone)
22.6
5.0
ug/L
20.00
113
64-137
5
20
Methyl Butyl Ketone (2-Hexanone)
22.6
5.0
ug/L
20.00
113
64-137
5
20
Methyl Ethyl Ketone (2-Butanone)
21.0
5.0
ug/L
20.00
105
71-134
5
20
Methyl Ethyl Ketone (2-Butanone)
21.0
5.0
ug/L
20.00
105
71-134
5
20
Methyl Iodide
20.2
5.0
ug/L
20.00
101
70-130
5
20
Methyl Iodide
20.2
5.0
ug/L
20.00
101
70-130
5
20
Methyl Isobutyl Ketone
21.6
5.0
ug/L
20.00
108
69-134
4
20
Methyl Isobutyl Ketone
21.6
5.0
ug/L
20.00
108
69-134
4
20
Methyl Methacrylate
21.4
10
ug/L
20.00
107
70-130
2
20
Methylene Chloride
18.6
1.0
ug/L
20.00
93
73-131
0.2
20
Methylene Chloride
18.6
1.0
ug/L
20.00
93
73-131
0.2
20
Naphthalene
22.3
1.0
ug/L
20.00
111
64-136
2
20
o-Xylene
20.4
0.50
ug/L
20.00
102
78-128
2
20
o-Xylene
20.4
0.50
ug/L
20.00
102
78-128
2
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 67

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/8/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Prism Work Order: 9100361
Attn: Alec Macbeth Samplling Time Submitted: 10/23/2019 11:03:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9KO048 - 5030B
LCS Dup (P9K0048-BSD1)
Prepared: 11/01/19 Analyzed: 11/02/19
Propionitrile (Ethyl Cyanide)
21.0
10
ug/L
20.00
105
70-130
3
20
Styrene
21.5
0.50
ug/L
20.00
108
78-129
2
20
Styrene
21.5
0.50
ug/L
20.00
108
78-129
2
20
Tetrachloroethylene
21.1
0.50
ug/L
20.00
106
80-129
4
20
Tetrachloroethylene
21.1
0.50
ug/L
20.00
106
80-129
4
20
Tetrahydrofuran
20.9
10
ug/L
20.00
104
70-130
7
20
Toluene
20.1
0.50
ug/L
20.00
101
76-131
2
20
Toluene
20.1
0.50
ug/L
20.00
101
76-131
2
20
trans-1,2-Dichloroethylene
19.5
0.50
ug/L
20.00
98
76-135
3
20
trans-1,2-Dichloroethylene
19.5
0.50
ug/L
20.00
98
76-135
3
20
trans-1,3-Dichloropropylene
21.8
0.50
ug/L
20.00
109
67-140
0.05
20
trans-1,3-Dichloropropylene
21.8
0.50
ug/L
20.00
109
67-140
0.05
20
trans-1,4-Dichloro-2-butene
20.6
10
ug/L
20.00
103
70-130
3
20
trans-1,4-Dichloro-2-butene
20.6
10
ug/L
20.00
103
70-130
3
20
Trichloroethylene
19.6
0.50
ug/L
20.00
98
77-133
4
20
Trichloroethylene
19.6
0.50
ug/L
20.00
98
77-133
4
20
Trichlorofluoromethane
22.8
0.50
ug/L
20.00
114
62-148
3
20
Trichlorofluoromethane
22.8
0.50
ug/L
20.00
114
62-148
3
20
Vinyl acetate
21.8
2.0
ug/L
20.00
109
34-167
2
20
Vinyl acetate
21.8
2.0
ug/L
20.00
109
34-167
2
20
Vinyl chloride
21.7
0.50
ug/L
20.00
109
57-141
4
20
Vinyl chloride
21.7
0.50
ug/L
20.00
109
57-141
4
20
Xylenes, total
62.2
1.5
ug/L
60.00
104
77-133
2
20
Xylenes, total
62.2
1.5
ug/L
60.00
104
77-133
2
20
Surrogate:4-Bromofluorobenzene
49.9
ug/L
50.00
100
80-124
Surrogate:4-Bromofluorobenzene
49.9
ug/L
50.00
100
80-124
Surrogate: Dibromofluoromethane
49.9
ug/L
50.00
100
75-129
Surrogate: Dibromofluoromethane
49.9
ug/L
50.00
100
75-129
Surrogate: Toluene-d8
50.5
ug/L
50.00
101
77-123
Surrogate: Toluene-d8
50.5
ug/L
50.00
101
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 of 67

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/8/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall
Attn: Alec Macbeth Samplling
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS SIM - Quality Control
Prism Work Order: 9100361
Time Submitted: 10/23/2019 11:03:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9J0395 - 5030B
Blank (P9J0395-BLK1)
Prepared & Analyzed: 10/23/19
1,4-Dioxane
BRL 2.0 ug/L
LCS (P9J0395-BS1)
Prepared &Analyzed: 10/23/19
1,4-Dioxane
50.4 2.0 ug/L
50.00 101 55-145
LCS Dup (P9J0395-BSD1)
Prepared &Analyzed: 10/23/19
1,4-Dioxane
51.1 2.0 ug/L
50.00 102 55-145 1 30
Matrix Spike (P9J0395-MS1)
Source: 9100361-06
Prepared & Analyzed: 10/23/19
1,4-Dioxane
52.4 2.0 ug/L
50.00 BRL 105 55-145
Matrix Spike Dup (P9J0395-MSD1)
Source: 9100361-06
Prepared & Analyzed: 10/23/19
1,4-Dioxane
54.0 2.0 ug/L
50.00 BRL 108 55-145 3 30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 67

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/8/19
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Total Metals - Quality Control
Analyte
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No: 50-02
Prism Work Order: 9100361
Time Submitted: 10/23/2019 11:03:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9J0440 - 3005A
Blank (P9J0440-BLK1)
Prepared: 10/25/19 Analyzed: 10/28/19
Antimony
BRL
3.0
ug/L
Arsenic
BRL
1.0
ug/L
Barium
BRL
10
ug/L
Beryllium
BRL
1.0
ug/L
Cadmium
BRL
1.0
ug/L
Chromium
BRL
3.0
ug/L
Cobalt
BRL
2.0
ug/L
Copper
BRL
10
ug/L
Lead
BRL
1.0
ug/L
Nickel
BRL
3.0
ug/L
Selenium
BRL
5.0
ug/L
Silver
BRL
1.0
ug/L
Thallium
BRL
2.0
ug/L
Tin
BRL
5.0
ug/L
Vanadium
BRL
5.0
ug/L
Zinc
BRL
20
ug/L
LCS (P9J0440-BS1)
Prepared: 10/25/19 Analyzed: 10/28/19
Antimony
102
3.0
ug/L
100.0
102
80-120
Arsenic
100
1.0
ug/L
100.0
100
80-120
Barium
106
10
ug/L
100.0
106
80-120
Beryllium
101
1.0
ug/L
100.0
101
80-120
Cadmium
101
1.0
ug/L
100.0
101
80-120
Chromium
100
3.0
ug/L
100.0
100
80-120
Cobalt
105
2.0
ug/L
100.0
105
80-120
Copper
104
10
ug/L
100.0
104
80-120
Lead
101
1.0
ug/L
100.0
101
80-120
Nickel
105
3.0
ug/L
100.0
105
80-120
Selenium
104
5.0
ug/L
100.0
104
80-120
Silver
100
1.0
ug/L
100.0
100
80-120
Thallium
101
2.0
ug/L
100.0
101
80-120
Tin
101
5.0
ug/L
100.0
101
80-120
Vanadium
99.9
5.0
ug/L
100.0
100
80-120
Zinc
105
20
ug/L
100.0
105
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 of 67

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/8/19
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Total Metals - Quality Control
Analyte
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No: 50-02
Prism Work Order: 9100361
Time Submitted: 10/23/2019 11:03:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9J0493 - 7470A
Blank (P9J0493-BLK1) Prepared & Analyzed: 10/29/19
Mercury BRL 0.20 ug/L
LCS (P9J0493-BS1) Prepared &Analyzed: 10/29/19
Mercury 10.0 0.20 ug/L 9.375 107 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 32 of 67

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/8/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall
Attn: Alec Macbeth Samplling
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Anions by Ion Chromatography - Quality Control
Prism Work Order: 9100361
Time Submitted: 10/23/2019 11:03:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9JO423 - NO PREP
Blank (P9J0423-BLK1)
Prepared & Analyzed: 10/23/19
Chloride
BRL
1000
ug/L
Nitrate as N
BRL
200
ug/L
Sulfate
BRL
2000
ug/L
LCS (P9J0423-BS1)
Prepared &Analyzed: 10/23/19
Chloride
40600
1000
ug/L
40000 101
80-120
Nitrate as N
3910
210
ug/L
4000 98
80-120
Sulfate
40700
2100
ug/L
40000 102
80-120
Matrix Spike (P9J0423-MS2)
Source: 9100361-01
Prepared & Analyzed: 10/24/19
Chloride
88400
1000
ug/L
40000 47400 103
80-120
Nitrate as N
9320
210
ug/L
4000 5320 100
80-120
Sulfate
119000
2100
ug/L
40000 78400 103
80-120
Matrix Spike Dup (P9J0423-MSD2)
Source: 9100361-01
Prepared & Analyzed: 10/24/19
Chloride
87000
1000
ug/L
40000 47400 99
80-120 2 15
Nitrate as N
9260
210
ug/L
4000 5320 99
80-120 0.7 15
Sulfate
118000
2100
ug/L
40000 78400 100
80-120 0.8 15
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 of 67

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/8/19
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
General Chemistry Parameters - Quality Control
Analyte
Project: Jackson Cty Landfill 2019 Fall Prism Work Order: 9100361
Samplling Time Submitted: 10/23/2019 11:03:OOAM
Project No: 50-02
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9J0408 - NO PREP
Blank (P9J0408-BLK1) Prepared & Analyzed: 10/23/19
Ferrous Iron BRL 200 ug/L
LCS (P9J0408-BS1) Prepared &Analyzed: 10/23/19
Ferrous Iron 2080 200 ug/L 2000 104 90-110
Matrix Spike (P9J0408-MS1) Source: 9100361-02 Prepared & Analyzed: 10/23/19
Ferrous Iron 2050 200 ug/L 2000 74.0 99 80-120
Matrix Spike Dup (P9J0408-MSD1) Source: 9100361-02 Prepared & Analyzed: 10/23/19
Ferrous Iron 2070 200 ug/L 2000 74.0 100 80-120 0.7
Batch P9J0436 - NO PREP
20
Blank (P9J0436-BLK1)
Prepared & Analyzed: 10/25/19
Chemical Oxygen Demand
BRL 50000 ug/L
LCS (P9J0436-BS1)
Prepared &Analyzed: 10/24/19
Chemical Oxygen Demand
497000 50000 ug/L
500000 99 90-110
Matrix Spike (P9J0436-MS2)
Source: 9100361-02
Prepared & Analyzed: 10/24/19
Chemical Oxygen Demand
514000 50000 ug/L
500000 12700 100 80-120
Matrix Spike Dup (P9J0436-MSD2)
Source: 9100361-02
Prepared & Analyzed: 10/24/19
Chemical Oxygen Demand
497000 50000 ug/L
500000 12700 97 80-120 3 20
Batch P9J0482 - NO PREP
Blank (P9J0482-BLK1) Prepared & Analyzed: 10/28/19
Hardness BRL 5000 ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 of 67

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/8/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Prism Work Order: 9100361
Attn: Alec Macbeth Samplling Time Submitted: 10/23/2019 11:03:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9JO482 - NO PREP
LCS (P9J0482-BS1) Prepared &Analyzed: 10/28/19
Hardness 50000 5000 ug/L 50000 100 90-110
Matrix Spike (P9J0482-MS1) Source: 9100361-03 Prepared & Analyzed: 10/28/19
Hardness 24500 5000 ug/L 10000 13000 115 80-120
Matrix Spike Dup (P9J0482-MSD1) Source: 9100361-03 Prepared & Analyzed: 10/28/19
Hardness 24000 5000 ug/L 10000 13000 110 80-120 2 20
Batch P9JO483 - NO PREP
Blank (P9J0483-BLK1) Prepared & Analyzed: 10/24/19
Biochemical Oxygen Demand 500 2000 ug/L BB, J
LCS (P9J0483-BS1) Prepared &Analyzed: 10/24/19
Biochemical Oxygen Demand 210000 2000 ug/L 198000 108 84.6-115.4 BB, B
Duplicate (P9J0483-DUP1) Source: 9100361-01 Prepared &Analyzed: 10/24/19
Biochemical Oxygen Demand 680 2000 ug/L 820 19 30 BB, J, B
Batch P9J0504 - SM4500-S C
Blank (P9J0504-BLK1) Prepared & Analyzed: 10/29/19
Sulfide BRL 2000 ug/L
LCS (P9J0504-BS1) Prepared &Analyzed: 10/29/19
Sulfide 9700 2000 ug/L 10000 97 70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 of 67

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
General Chemistry Parameters - Quality Control
Analyte
Batch P9J0504 - SM4500-S C
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No: 50-02
Level II QC Report
11/8/19
Prism Work Order: 9100361
Time Submitted: 10/23/2019 11:03:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Matrix Spike (P9J0504-MS1) Source: 9100361-01 Prepared & Analyzed: 10/29/19
Sulfide 19400 2000 ug/L 10000 11200 82 70-130
Matrix Spike Dup (P9J0504-MSD1) Source: 9100361-01 Prepared & Analyzed: 10/29/19
Sulfide 19200 2000 ug/L 10000 11200 80 70-130 1 20
Batch P9JO537 - NO PREP
Blank (P9J0537-BLK1) Prepared &Analyzed: 10/31/19
Total Alkalinity to pH 4.5 BRL 5000 ug/L
LCS (P9J0537-BSI) Prepared &Analyzed: 10/31/19
Total Alkalinity to pH 4.5 250000 5000 ug/L 250000 100 90-110
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 36 of 67

Sample Extraction Data
Prep Method: SM4500-S C
Lab Number
Batch
Initial
Final
Date/Time
9100361-01
P9J0504
200
mL
200 mL
10/29/19 9:45
9100361-02
P9J0504
200
mL
200 mL
10/29/19 9:45
Prep Method: 3005A
Lab Number
Batch
Initial
Final
Date/Time
9100361-01
P9J0440
50
mL
50 mL
10/25/19 8:44
9100361-02
P9J0440
50
mL
50 mL
10/25/19 8:44
9100361-03
P9J0440
50
mL
50 mL
10/25/19 8:44
9100361-04
P9J0440
50
mL
50 mL
10/25/19 8:44
Prep Method: 7470A
Lab Number
Batch
Initial
Final
Date/Time
9100361-01
P9J0493
20
mL
30 mL
10/29/19 9:18
9100361-02
P9J0493
20
mL
30 mL
10/29/19 9:18
9100361-03
P9J0493
20
mL
30 mL
10/29/19 9:18
9100361-04
P9J0493
20
mL
30 mL
10/29/19 9:18
Prep Method: 5030E
Lab Number
Batch
Initial
Final
Date/Time
9100361-01
P91<0048
10
mL
10 mL
11/01/19 8:01
9100361-02
P91<0048
10
mL
10 mL
11/01/19 8:01
9100361-03
P91<0048
10
mL
10 mL
11/01/19 8:01
9100361-04
P91<0048
10
mL
10 mL
11/01/19 8:01
9100361-05
P91<0048
10
mL
10 mL
11/01/19 8:01
9100361-06
P91<0048
10
mL
10 mL
11/01/19 8:01
Prep Method: 5030E
Lab Number
Batch
Initial
Final
Date/Time
9100361-01
P9J0395
5
mL
5 mL
10/23/19 14:52
9100361-02
P9J0395
5
mL
5 mL
10/23/19 14:52
9100361-03
P9J0395
5
mL
5 mL
10/23/19 14:52
9100361-04
P9J0395
5
mL
5 mL
10/23/19 14:52
9100361-06
P9J0395
5
mL
5 mL
10/23/19 14:52
Subcontracted Analyses
The following analyses
were subcontracted to Analytical
Environmental Services,
Inc.
Lab Number
Analysis
9100361-03
8270 (App. II)
9100361-04
8270 (App. II)
The following analyses
were subcontracted to Pace Analytical Gulf Coast
Lab Number
Analysis
9100361-01
TOC (Sub)
9100361-02
TOC (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 37 of 67

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38 of 67

ACCESS
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte NC 282240543
ATTENTION
Robbi A. Jones
PROJECT ID
9100361
LABORATORY REPORT NUMBER
1910021
DATE
October 30, 2019
Primary Data Review By Secondary Data Review By
Ashley Amick
Chris Pafford Project Manager, Access Analytical
Project Manager, AES [e-mail]
PLEASE NOTE:
Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),
3080 Presidential Drive, Atlanta, GA 30340.
AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582,
NELAP certified laboratory # E87582
AIHA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, PCiM Asbestos,
Gravimetric), Environmental Lead (Paint, Soil, Dust wipes, Air), and Environmental Microbiology (Fungal)
Direct Examination.
Local support services for this project are provided by Access Analytical. Inc. Access Analytical is a
representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll fee at 983.315.4243
Page I Page 39 of 67

��PRISMI S Fullironmee Analytical s
' Environmental Solutions
SUBCONTRACT ORDER
Ccnifscutiots: iyELAC 1SACE
Prism Laboratories, Inc. NC_✓ Sc— Other
!
9100361 NIA
SF.1'IDI NC. LAEt033�.1TORY:
1LEC £3 V IN G LA B DRA f 01
t Prism Laboratories, Inc.
Analytical Environmental Scivices, Inc.
P. 0. Box 240543
3080 Presidential Parkway
Charlotte, NC 28224-0543
Atlanta, GA 30340
Phone: [phone]
Phonc :[phone]
Fax: [phone]
Fax: NA
Project Manager: Robbi A. Jones
Analysis Due Expires LabOratnryID Comments
Sample ID: 9100361-03 Water Sampled: I O/22119 14:05 ylo — o 1
3270 (App. 11) 10/29119 14:05 8270 App 11 List
C'mom mrs Supplied: i—
G k f i <ee-5 Lc,.
Sample ID: 9100361-04 1 Water Sampled: 10/22/19 14:30 w -
8270 (App. 11) 10129/19 14:30 8270 App 11 List
Cmnnincrc Supplied:
R elcased Jay Ca;, Recmcd Ih Dale
lWcased By Date Received By L Date
RrlcasM By 1. mi Received FI
76 L Page 1 or 1
Page 40 of 67

Analytical Environmental Services, Inc
Date: 30-Oct-19
Client:
Prism Laboratories
Client Sample ID:
SW-01
Lab Order
1910021
Tag Number:
9100361-03
Project Name:
9100361
Collection Date:
10/22/2019 2:05:00 PM
Lab ID:
1910021-OOIA
Matrix:
Aqueous
Analyses Result Qua[
MDL
ReportingUnits
Limit
BatchlD DF
Date Analyzed
Analyst
APPENDIXII-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
1,2,4,5-Tetrachlorobenzene
BRL
1.3
10
ug/L
286923 1
10/25/2019 20:47
YH
1,2,4-Trichlorobenzcne
BRL
1.4
10
ug/L
286923 1
10/25/2019 20:47
YH
1,2-Dichlorobenzene
BRL
1.2
10
ug/L
286923 1
10/25/2019 20:47
YH
1.3-Dichlorobenzene
BRL
1.3
10
ug/L
286923 1
10/25/2019 20:47
YH
1,3-Dinitrobenzene
BRL
1.1
20
ug/L
286923 1
10/25/2019 20:47
YH
1.4-Dichlorobenzene
BRL
1.4
10
ug/L
286923 1.
10/25/2019 20:47
YH
1.4-Napthoquinone
BRL
1.7
10
ug/L
286923 1
10/25/2019 20:47
YH
1-Naphthylamine
BRL
3 0
10
ug/L
286923 1
10/25/2019 20:47
YH
2,3,4,6-Tetrachlorophenol
BRL
1.1
10
ug/L
286923 1
10/25/2019 20:47
YH
2.4;5-Trichlorophenol
BRL
0.99
10
ug/L
286923 1
10/25/2019 20:47
YH
2,4;6-Trichlorophenol
BRL
1.3
10
ug/L
286923 1•
10/25/2019 20:47
YH
2.4-Dichlorophenol
BRL
1.0
10
ug/L
286923 1
10/25/2019 20:47
YH
2,4-Dimethylphenol
BRL
0.72
50
ug/L
286923 1
10/25/2019 20:47
YH
2.4-Dinitrophenol
BRL
5.5
50
ug/L
286923 f
10/25/2019 20:47
YH
2,4-Dinitrotoluene
BRL
1.1
10
ug/L
286923 1
10/25/2019 20:47
YH
2;6-Dichlorophenol
BRL
0.95
10
ug/L
286923 1
10/25/2019 20:47
YH
2.6-Dinitrotoluene
BRL
1.3
10
ug/L
286923 1
10/25/2019 20:47
YH
2-Acetylaminofluorene
BRL
1.1
20
ug/L
286923 I
10/25/2019 20:47
YH
2-Chloronaphthalene
BRL
1.8
10
ug/L
286923 1
10/25/2019 20:47
YH
2-Chlorophenol
BRL
1.2
10
ug/L
286923 1
10/25/2019 20:47
YH
2-Methylnaphthalene
BRL
1.2
10
ug/L
286923 }•
10/25/2019 20:47
YH
2-Methylphenol
BRL
1 3
10
ug/L
286923 f
10/25/2019 20:47
YH
2-Naphthylamine
BRL
1 7
10
ug/L
286923 1.
10/25/2019 20:47
YH
2-Nitroaniline
BRL
1 9
50
ug/L
286923 1
10/25/2019 20:47
YH
2-Nitrophenol
BRL
1.6
10
ug/L
286923 1
10/25/2019 20:47
YH
3.3'-Dichlorobenzidine
BRL
1 1
20
ug/L
286923 1
10/25/2019 20:47
YH
3,3'-Dimethy1benzidine
BRL
54
20
tig/L
286923 I
10/25/2019 20:47
YH
3,4-Methylphenol
BRL
2 3
10
ttg/L
286923 1
10/25/2019 20:47
YH
3-Methyleholanthrene
BRL
1 1
10
ug/L
286923 1
10/25/2019 20:47
YH
3-Nitroaniline
BRL
1 2
50
ug/L
286923 1
10/25/2019 20:47
YH
4.6-Dinitro-2-methylphenol
BRL
1 3
50
ug/L
286923 1
10/25/2019 20:47
YH
4-Aminobiphenyl
BRL
24
20
ug/L
286923 1
10/25/2019 20:47
YH
4-Bromophenyl phenyl ether
BRL
14
10
ug/L
286923 1
10/25/2019 20:47
YH
4-Chloro-3-methylphenol
BRL
0.81
20
ug/L
286923 1
10/25/2019 20:47
YH
4-Chloroaniline
BRL
2 1
20
ugiL
286923 t
10/25/2019 20 47
YH
4-Chlorophenyl phenyl ether
BRL
1 3
10
ug/L
286923 1
10/25/2019 20:47
YH
4-Nitroaniline
BRL
13
20
ug/L
286923 1
10/25/2019 20:47
YH
4-Nitrophenol
BRL
077
50
ug/L
286923 1
10/25/2019 20:47
YH
QnPllricrst ` Value exceeds masnnum contaminant Icscl
E L-sumated
taluc abosc
quanulauon mnsc
BRL Not Detected al NIDL
S Spike Reco-, outside lunns due to malnx
H Holding times for preparation or analysts exceeded
> Grauer than
R¢u It value
N Analpe not NELAC certified
J Estimated
%attic detected
below Reporting Lmnt
B Analyze detected In the associated method blank
a Leos Than
Result salue
Page Page 41 of 67

Analytical Environmental Services, Inc
Date: 30-Oct-19
Client:
Prism Laboratories
Client Sample ID:
SW-01
Lab Order
1910021
Tag Number:
9100361-03
Project Name:
9100361
Collection Date:
10/22/2019 2:05:00 PM
Lab 1D:
1910021-OOIA
Matrix:
Aqueous
Analyses Result Qua[
MDL
ReportingUnits
Limit
BatchlD DF
Date Analyzed
Analyst
APPENDIXII-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
5-Nitro-o-toluidine
BRL
0.66
10
ug/L
286923 I
10/25/2019 20:47
YH
7,12-Dimethylbenz(a)anthracene
BRL
1.4
10
ug/L
286923 I
10/25/2019 20:47
YH
Acenaphthene
BRL
1 1
10
ug/L
286923 I
10/25/2019 20:47
YH
Acenaphthylene
BRL
1.1
10
ug/L
286923 1
10/25/2019 20:47
YH
Acetophenone
BRL
2 1
10
ug/L
286923 1
10/25/2019 20:47
YH
Anthracene
BRL
0.82
10
ug/L
286923 1
10/25/2019 20:47
YH
Benz(a)anthracene
BRL
0.96
10
ug/L
286923 1
10/25/2019 20:47
YH
Benzo(a)pyrene
BRL
0.96
10
ug/L
286923 1
10/25/2019 20:47
YH
Benzo(b)fluoranthene
BRL
1,5
10
ug/L
286923 1
10/25/2019 20:47
YH
Benzo(g,h,i)perylene
BRL
1.3
10
ug/L
286923 1
10/25/2019 20:47
YH
Benzo(k)fluoranthene
BRL
1 5
10
ug/L
286923 1
10/25/2019 20:47
YH
Benzy] alcohol
BRL
14
20
ug/L
286923 1
10/25/2019 20:47
YH
Bis(2-chloroethoxy)methane
BRL
1 1
10
ug/L
286923 1
10/25/2019 20:47
YH
Bis(2-chloroethyl)ether
BRL
1 2
10
ug/L
286923 1
10/25/2019 20:47
YH
Bis(2-chloroisopropyl)ether
BRL
1 5
10
ug/L
286923 1
10/25/2019 20:47
YH
Bis(2-ethy1hexy1)phtha1ate
BRL
1.4
20
ug/L
286923 1
10/25/2019 20:47
YH
Butyl benzyl phthalate
BRL
0.84
10
ug/L
286923 1
10/25/2019 20:47
YH
Chlorobenzilate
BRL
0.57
10
ug/L
286923 1
10/25/2019 20:47
YH
Chrysene
BRL
093
10
ug/L
286923 1
10/25/2019 20:47
YH
Di-n-butyl phthalate
BRL
1 1
10
ug/L
286923 1
10/25/2019 20:47
YH
Di-n-octyl phthalate
BRL
1 6
10
ug/L
286923 1
10/25/2019 20:47
YH
Diallate
BRL
084
10
ug/L
286923 1
10/25/2019 20:47
YH
Dibenz(a,h)anthracene
BRL
1.4
10
ug/L
286923 i
10/25/2019 20:47
YH
Dibenzofuran
BRL
I 1
10
ug/L
286923 1
10/25/2019 20:47
YH
Diethyl phthalate
BRL
0.82
10
ug/L
286923 1
10/25/2019 20:47
YH
Dimethoate
BRL
0.45
20
ug/L
286923 1
10/25/2019 20:47
YH
Dimethyl phthalate
BRL
1 0
10
ug/L
286923 1
10/25/2019 20:47
YH
Diphenylamine
BRL
10
10
ug/L
286923 1,
10/25/2019 20:47
YH
Disultbton
BRL
0.68
10
ug/L
286923 1
10/25/2019 20:47
YH
Ethvl methanesulfonate
BRL
1 1
20
ugiL
286923 1
10/25/2019 20:47
YH
Famphur
BRL
072
20
ug/L
286923 1
10/28/2019 14:19
YH
Fluoranthene
BRL
1 0
10
ug/L
286923 1
10/25/2019 20:47
YH
Fluorene
BRL
1.2
10
r:,/L
286923 1
10/25/2019 20:47
YH
IIexachlorobenzene
BRL
I 1
10
ug/L
286923 1
10/25/2019 20:47
YH
HexachIorobutadiene
BRL
12
10
up.'L
286923 1
10/25/2019 20:47
YH
HexachlorocycIopentadiene
BRL
21
10
tt:%L
286923 I
10/25/2019 20:47
YH
H ex a Ch l o roeth a n e
BRL
1 3
10
1.141/1
286923 1
10/25/2019 20:47
YH
Hexachloropropene
BRL
1 0
10
uaL
286923 6
10/25/2019 20:47
YH
Qnal}ners: Value exceeds maximum cumammant level
E Estimated
value abo,e quanmanon ranee
BRL Nol Detected m NlDL
S Spike Renown
outside hnuts due to matrix
H Holding umes for preparation or analysts exceeded
> Greaser than RLwuh value
N An,,Mc not NELAC centred
3 Estunated
value detected
below Reporune Lmut
a Analvte detected m the associated method blank
< Less than
Result saluc
Page 42 of 67

Analytical Environmental Services, Inc
Date: 30-Oct-19
Client:
Prism Laboratories
Client Sample ID:
SW-01
Lab Order
1910021
Tag Number:
9100361-03
Project Name:
9100361
Collection Date:
10/22/2019 2:05:00 PM
Lab 1D:
1910021-OOIA
Matrix:
Aqueous
Analyses Result Qual
MDL
Reporting
Limit
UnitsBatchlD
DF
Date Analyzed
Analyst
APPENDIX II-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
Indeno(1;2,3-cd)pyrene
BRL
1.2
10
ug/L
286923 1
10/25/2019 20:47
YH
Isodrin
BRL
1.2
20
ug/L
286923 1
10/25/2019 20:47
YH
lsophorone
BRL
0.86
10
ug/L
286923 1
10/25/2019 20:47
YH
Isosafrole
BRL
1.1
10
ug/L
286923 1
10/25/2019 20:47
YH
Kepone
BRL
1.4
50
ug/L
286923 1
10/28/201914:19
YH
Methapyrilene
BRL
6.4
20
ug/L
286923 1
10/25/2019 20:47
YH
Methyl methanesulfonate
BRL
13
10
ug/L
286923 1
10/25/2019 20:47
YH
Methyl parathion
BRL
0.85
10
ug/L
286923 1
10/25/2019 20:47
YH
N-Nitroso-di-n-butylamine
BRL
1.8
10
ug/L
286923 1
10/25/2019 20:47
YH
N-Nitrosodi-n-propylamine
BRL
0.82
10
ug/L
286923 1
10/25/2019 20:47
YH
N-Nitrosodiethylamine
BRL
1.2
20
ug/L
286923 1
10/25/2019 20:47
YH
N-Nitrosodimethylamine
BRL
1.7
20
ug/L
286923 1
10/25/2019 20:47
YH
N-Nitrosodiphenylamine
BRL
0-90
50
ug/L
286923 1
10/25/2019 20:47
YH
N-Nitrosomethylethylamine
BRL
1-00
10
ug/L
286923 I
10/25/2019 20:47
YH
N-Nitrosopiperidine
BRL
0.86
20
ug/L
286923 I
10/25/2019 20:47
YH
N-Nitrosopyrrolidine
BRL
1.2
40
ug/L
286923 1
10/25/2019 20:47
YH
Naphthalene
BRL
1.2
10
ug/L
286923 1
10/25/2019 20:47
YH
Nitrobenzene
BRL
1.2
10
ug/L
286923 1
10/25/2019 20:47
YH
0,0;0-Triethyl phosphorothioate
BRL
3.6
10
ttg/L
286923 1
10/25/2019 20:47
YH
o-Toluidine
BRL
2.1
20
❑g/L
286923 1
10/25/2019 20:47
YH
p-Dimethylaminoazobenzene
BRL
0,65
10
ug/L
286923 1
10/25/2019 20:47
YH
p-Phenylenediamine
BRL
55
500
ug/L
286923 1
10/25/2019 20:47
YH
Parathion
BRL
1.3
10
ug/L
286923 1
10/25/2019 20:47
YH
Pentachlorobenzene
BRL
094
10
ug/L
286923 1
10/25/2019 20:47
YH
Pcntachloronitrobenzene
BRL
096
20
ug/L
286923 1
10/25/2019 20:47
YH
Pentachlorophenol
BRL
0.62
50
ug/L
286923 i
10/25/2019 20:47
YH
Phenacetin
BRL
0.85
20
ug/L
286923 1
10/25/2019 20:47
YH
Phenanthrene
BRL
0.86
10
ug/L
286923 l
10/25/2019 20:47
YH
Phenol
BRL
0.77
10
ug/L
286923 1
10/25/2019 20:47
YH
Phorate
BRL
094
10
ug/L
286923 1:
10/25/2019 20:47
YH
Pronamide
BRL
11
10
ug/L
286923 1
10/25/2019 20:47
YH
pvrene
BRL
0-83
10
ug/L
286923 I
10/25/2019 20:47
YH
Safi -Ole
BRL
12
20
oe/L
286923 I
10/25/2019 20:47
YH
Svm-Trinitrobenzene
BRL
098
10
ug/L
286923 1
10/25/201920:47
YH
Thionazin
BRL
0 81
20
u%i/L
286923 1
10/25/2019 20:47
YH
Surr:2.4.6-Tribromophenol
72.9
0
47-127
"..REC
286923 1
10/25/201920.47
YH
Surr:2-Pluorobiphenyl
69.6
0
474-119
%REC
286923 1
10/25/2019 20:47
YH
Sun-: 2-Pluorophenol
469
0
26 2-120
'NAEC
286923 1
10/25/2019 20:47
Yll
QrtnlVBn-st Value exceeds ntaxmmm contammani Ietel
E Estimmed
%aluc abose
quantitation range
BRL Not Detected m NIDL
S Spike Recoserp outside hnuts due to matrix
H Holding times for preparation or analysts exceeded
= Greater than Resuh -lue
N Anedxte not NELAC certified
1 Estunated
value detected below Reporting Limo
B Anah•te detected in the associated method blank
- Less than
Re,uh v;due
Page I Page 43 of 67

Analytical Environmental Services, Inc
Date: 30-Oct-19
Client:
Prism Laboratories
Client Sample ID:
SW-01
Lab Order
1910021
Tag Number:
9100361-03
Project Name:
9100361
Collection Date:
10/22/2019 2:05:00 PM
Lab ID:
1910021-OOIA
Matrix:
Aqueous
Analyses Result Qual MDL ReportingUnits BatchlD DF Date Analyzed Analyst
Limit
APPENDIXII-SEMIVOLATILE ORGANICS SW8270E (SW3510C)
Surr: 4-Terphenyl-d 14 60.5 0 45-133 %REC 286923 1 10/25/2019 20:47 YH
Sum Nitrobenzene-d5 74.3 0 41.9-121 %REC 286923 1 10/25/2019 20:47 YH
Surr: Phenol-d5 32.8 0 17.8-120 %REC 286923 1 10/25/2019 20:47 YH
QUpljfiers; • Value exceeds maximum contammam level
6RL Nol Deleacd w NIDL
FI Holding times for prcparauon or analysis csceeded
N Auals to not NELAC certified
D Analrte delectcd in the associated method blank
E Estimated \clue above quanulauon ranee
S Spike Recosen outside limns due to matrix
Greater than Result value
1 EsUmaled salue delectcd We, Reporun- Luiw
Less than Resuh salue
Page I Page 44 of 67

Analytical Environmental Services, Inc
Date: 30-Oct-19
Client:
Prism Laboratories
Client Sample ID:
SW-02
Lab Order
1910021
Tag Number:
9100361-04
Project Name:
9100361
Collection Date:
10/22/2019 2:30:00 PM
Lab ID:
1910021-002A
Matrix:
Aqueous
Analyses Result Qua]
MDL
ReportingUnits
Limit
BatchID
DF
Date Analyzed Analyst
APPENDIX] I-SEM]VOLATILE ORGANICS
SW8270E
(SW3510C)
1,2,4,5-Tetrachlorobenzene
BRL
1.3
10
ug/L
286923
1
10/25/2019 21:14
YH
1.2.4-Trichlorobenzene
BRL
1.4
10
ug/L
286923
i
10/25/2019 21:14
YH
1.2-Dichlorobenzene
BRL
1.2
10
ug/L
286923
j'
10/25/2019 21:14
YH
1.3-Dichlorobenzene
BRL
1.3
10
ug/L
286923
[
10/25/2019 21:14
YH
1.3-Dinitrobenzene
BRL
1.1
20
ug/L
286923
1
10/25/2019 21:14
YH
1,4-Dichlorobenzene
BRL
1.4
10
ug/L
286923
1
10/25/2019 21:14
YH
1,4-Napthoquinone
BRL
1.7
10
ug/L
286923
1
10/25/2019 21:14
YH
1-Naphthylamine
BRL
3.0
10
ug/L
286923
1:
10/25/2019 21:14
YH
2,3,4,6-Tetrachlorophenol
BRL
1.1
10
ug/L
286923
F
10/25/2019 21:14
YH
2,4,5-Trichlorophenol
BRL
0.99
10
ug/L
286923
1:
10/25/2019 21:14
YH
2.4,6-Trichlorophenol
BRL
1.3
10
ug/L
286923
1
10/25/2019 21:14
YH
2.4-Dichlorophenol
BRL
1.0
10
ug/L
286923
1
10/25/2019 21:14
YH
2,4-Dimethylphenol
BRL
0.72
50
ug/L
286923
1
10/25/2019 21:14
YH
2,4-Dinitrophenol
BRL
5.5
50
ug/L
286923
1
10/25/2019 21:14
YH
2.4-Dinitrotoluene
BRL
1.1
10
ug/L
286923
1
10/25/2019 21:14
YH
2,6-Dichlorophenol
BRL
0.95
10
ug/L
286923
1
10/25/2019 21:14
YH
2.6-Dinitrotoluene
BRL
1.3
10
ug/L
286923
1
10/25/2019 21:14
YH
2-Acetylaminofluorene
BRL
1.1
20
ug/L
286923
1
10/25/2019 21:14
YH
2-Chloronaphthalene
BRL
1.8
10
ug/L
286923
1
10/25/2019 21:14
YH
2-Chlorophenol
BRL
1.2
10
ug/L
286923
1
10/25/2019 21:14
YH
2-MethyInaphthaIene
BRL
1.2
10
ug/L
286923
1
10/25/2019 21:14
YH
2-Methylphenot
BRL
1.3
10
ug/L
286923
1
10/25/2019 21:14
YH
2-Naphthylamine
BRL
17
10
ug/L
286923
1
10/25/2019 21:14
YH
2-Nitroaniline
BRL
19
50
ug/L
286923
1
10/25/2019 21:14
YH
2-N itrophenol
BRL
1.6
10
ug/L
286923
1.
10/25/2019 21:14
YH
3.Y-DichIorobenzidine
BRL
1.1
20
ug/L
286923
1.
10/25/2019 21:14
YH
3.3'-Dimethy Ibenzidine
BRL
54
20
ug/L
286923
1
10/25/2019 21:14
YH
3,4-Methylphenol
BRL
2.3
10
up/L
286923
t
10/25/2019 21:14
YH
3-MethvIchofanthrene
BRL
1.1
10
m /L
286923
1'
10/25/2019 21:14
YH
3-Nitroaniline
BRL
12
50
ug/L
286923
I
10/25/201921:14
YH
4,6-Dinitro-2-methyl phenol
BRL
1 3
50
ug/L
286923
I.
10/25/2019 21:14
YH
4-Aminobiphenyl
BRL
2.4
20
qn/L
286923
I
10/25/2019 21:14
YH
4-Bromophenyl phenyl ether
BRL
1 4
10
ug/L
286923
1i
10/25/2019 21:14
YH
4-Chloro-3-methylphenol
BRL
0.81
20
uciL
286923
It
10/25/2019 21:14
YH
4-Chloroaniline
BRL
21
20
ug/L
286923
1.
10/25/2019 21:14
YH
4-Chlorophenyl phenyl ether
BRL
1 3
10
ue/L
286923
1.
10/25/2019 21:14
YH
4-Nitroaniline
BRL
1 3
20
ue/L
286923
I
10/25/2019 21:14
YH
4-Nitrophenol
BRL
077
50
ug-L
286923
t'
10/25/2019 21:14
YH
Qualifiers: \'aloe exceeds ma�inmot contaminant level
E Esnnlated
eAo, abose
quanutaoon rank
BRL Not Detected at MDL
S Spike Reco%m owSide lintits due to inatnx
H Holding notes for preparation or analysis exceeded
> Greater than Result salue
N Anahte not NELAC certified
J Estnnated
saluc detected below Reporlme
Lotm
B Anal, to deterred m the associated method blank
- Less than
Result \aloe
Page I Page 45 of 67

Analytical Environmental Services, Inc
Date: 30-Oct-19
Client:
Prism Laboratories
Client Sample ID:
SW-02
Lab Order
1910021
Tag Number:
9100361-04
Project Name:
9100361
Collection Date:
10/22/2019 2:30:00 PM
Lab ID:
1910021-002A
Matrix:
Aqueous
Analyses Result Qual MDL ReportingUnits BatchlD DF Date Analyzed Analyst
Limit
APPENDIXII-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
5-Nitro-o-toluidine
BRL
066
10
ub/L
286923
1
10/25/2019 21:14
YH
7,12-Dimethy1benz(a)anthracene
BRL
14
10
ug/L
286923
1
10/25/2019 21:14
YH
Acenaphthene
BRL
1 1
10
us/L
286923
1
10/25/2019 21:14
YH
Acenaphthylene
BRL
1 1
10
us/L
286923
1
10/25/2019 21:14
YH
Acetophenone
BRL
2.1
10
ug/L
286923
I
10/25/2019 21:14
YH
Anthracene
BRL
0.82
10
ug/L
286923
l
10/25/2019 21:14
YH
Benz(a)anthracene
BRL
0.96
10
ug/L
286923
1
10/25/2019 21:14
YH
Benzo(a)pyrene
BRL
096
10
ug/L
286923
1
10/25/2019 21:14
YH
Benzo(b)fluoranthene
BRL
1.5
10
ug/L
286923
1
10/25/2019 21:14
YH
Benzo(g.h,i)perylene
BRL
1.3
10
ug/L
286923
1
10/25/2019 21:14
YH
Benzo(k)fluoranthene
BRL
1.5
10
ug/L
286923
l
10/25/2019 21:14
YH
Benzvl alcohol
BRL
1A
20
ug/L
286923
1
10/25/2019 21:14
YH
Bis(2-chloroethoxy)methane
BRL
1.1
10
ug/L
286923
1
10/25/2019 21:14
YH
Bis(2-chloroethyl)etlier
BRL
1.2
10
ug/L
286923
I
10/25/2019 21:14
YH
Bis(2-chloroisopropyl)ether
BRL
1.5
10
ug/L
286923
1
10/25/2019 21:14
YH
Bis(2-ethylhexyl)phthalate
BRL
1,4
20
ug/L
286923
1
10/25/2019 21:14
YH
Butyl benzyl phthalate
BRL
0.84
10
ug/L
286923
1
10/25/2019 21:14
YH
Chlorobenzilate
BRL
0.57
10
ug/L
286923
1
10/25/2019 21:14
YH
Chrysene
BRL
0.93
10
ug/L
286923
1
10/25/2019 21:14
YH
Di-n-butyl phthalate
BRL
1.1
10
ug/L
286923
1
10/25/2019 21:14
YH
Di-n-octyl phthalate
BRL
1.6
10
ug/L
286923
1
10/25/2019 21:14
YH
Diallate
BRL
0.84
10
ug/L
286923
1
10/25/2019 21:14
YH
Dibenz(a_h)anthracene
BRL
1 4
10
ug/L
286923
I
10/25/2019 21:14
YH
Dibenzofuran
BRL
1.1
10
ug/L
286923
l
10/25/2019 21:14
YH
Diethyl phthalate
BRL
0.82
10
ug/L
286923
1
10/25/2019 21:14
YH
Dimethoate
BRL
0.45
20
ug/L
286923
1
10/25/2019 21:14
YH
Dimethyl phthalate
BRL
1 0
10
ug/L
286923
1
10/25/2019 21:14
YH
Diphenylamine
BRL
1.0
10
ug/L
286923
1
10/25/2019 21:14
YH
Disulfolon
BRL
0.68
10
ug/L
286923
1
10/25/2019 21:14
YH
Ethvl methanesulfonate
BRL
1.1
20
ug/L
286923
1
10/25/2019 21:14
YH
Famphur
BRL
0.72
20
u,/L
286923
1
10/28/201919:45
YH
Fluoranthene
BRL
10
10
ue/L
286923
I
10/25/201921:14
YH
Fluorene
BRL
1 2
10
tw/L
286923
1
10/25/2019 21:14
YH
Hexachlorobenzene
BRL
1 1
10
ug/L
286923
1
10/25/2019 21:14
YH
Hexachlorobutadiene
BRL
1 2
10
ug/L
286923
1
10/25/2019 21:14
YH
Hexachlorocyclopentadiene
BRL
21
10
uF/L
286923
1
10/25/201921:14
YH
Hcxachloroethane
BRL
13
10
ug/L
286923
1
10/25/201921:14
YH
Hcxachloropropene
BRL
1.0
10
up/L
286923
1
10/25/2019 21:14
YH
Qualifiers; r Value eseceds maximum comannnam level
E Esunnaied salve abose
quanWauon range
BRL Not Detected at MIDI-
S Spike Recosery outside Inuits due to
maim
H Holding times for preparation or analysis exceeded
> Grcaier
than Result salue
N Anal.'Ie not NELAC certified
J Esumated
salve detected
below Reporting
Lund
n Aualctc detected in the associated method blank
Less
than Result salue
Page I Page 46 of 67

Analytical Environmental Services, Inc
Date: 30-Oct-19
Client:
Prism Laboratories
Client Sample ID:
SW-02
Lab Order
1910021
Tag Number:
9100361-04
Project Name:
9100361
Collection Date:
10/22/2019 2:30:00 PM
Lab ID:
1910021-002A
Matrix:
Aqueous
Analyses Result Qual
MDL
ReportingUnits
Limit
BatchlD DF
Date Analyzed
Analyst
APPENDIXII-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
Indeno(1,2,3-cd)pyrene
BRL
1.2
10
ug/L
286923 1
10/25/2019 21:14
YH
Isodrin
BRL
1.2
20
ug/L
286923 1
10/25/2019 21:14
YH
Isophorone
BRL
0.86
10
ug/L
286923 1
10/25/2019 21:14
YH
Isosafrole
BRL
1.1
10
ug/L
286923 1
10/25/2019 21:14
YH
Kepone
BRL
1.4
50
ug/L
286923 1
10/28/201919:45
YH
Methapyrilene
BRL
6.4
20
ug/L
286923 1
10/25/2019 21:14
YH
Methyl methanesulfonate
BRL
1.3
10
ug/L
286923 1
10/25/2019 21:14
YH
Methyl parathion
BRL
0,85
10
ug/L
286923 1
10/25/2019 21:14
YH
N-Nitroso-di-n-butylamine
BRL
1.8
10
ug/L
286923 1
10/25/2019 21:14
YH
N-Nitrosodi-n-propylamine
BRL
0.82
10
ug/L
286923 1
10/25/2019 21:14
YH
N-Nitrosodiethylamine
BRL
12
20
ug/L
286923 1
10/25/2019 21:14
YH
N-Nitrosodimethylamine
BRL
17
20
ug/L
286923 1
10/25/2019 21:14
YH
N-Nitrosodiphenylamine
BRL
090
50
ug/L
286923 1:
10/25/2019 21:14
YH
N-Nitrosomethylethylamine
BRL
1 00
10
ug/L
286923 1
10/25/2019 21:14
YH
N-Nitrosopiperidine
BRL
0.86
20
ug/L
286923 1
10/25/2019 21:14
YH
N-Nitrosopynrolidine
BRL
1.2
40
ug/L
286923 1
10/25/2019 21:14
YH
Naphthalene
BRL
1.2
10
ug/L
286923 1
10/25/2019 21:14
YH
Nitrobenzene
BRL
1.2
10
ug/L
286923 1
10/25/2019 21:14
YH
0,0,0-Triethylphosphorothioate
BRL
3.6
10
ug/L
286923 1
10/25/2019 21:14
YH
o-Toluidine
BRL
2.1
20
ug/L
286923 l
10/25/2019 21:14
YH
p-Dimethylam inoazobenzene
BRL
065
10
ug/L
286923 1
10/25/2019 21:14
YH
p-Phenylenediamine
BRL
55
500
ug/L
286923 1
10/25/2019 21:14
YH
Parathion
BRL
1.3
10
ug/L
286923 1'
10/25/2019 21:14
YH
Pentachlorobenzene
BRL
0.94
10
ug/L
286923 1
10/25/2019 21:14
YH
Pentachloronitrobenzene
BRL
096
20
ug/L
286923 I
10/25/2019 21:14
YH
Pentachlorophenol
BRL
0.62
50
ug/L
286923 I.
10/25/2019 21:14
YH
Phenacetin
BRL
0.85
20
ug/L
286923 1
10/25/2019 21:14
YH
Phenanthrene
BRL
0.86
10
ug/L
286923 1•
10/25/2019 21:14
YH
Phenol
BRL
077
10
ug/L
286923 f
10/25/2019 21:14
YH
Phorate
BRL
094
10
ug/L
286923 1
10/25/2019 21:14
YH
Pronamide
BRL
1.1
10
ug/L
286923 1
10/25/2019 21:14
YH
Pvrene
BRL
0.83
10
rig/L
286923 1
10/25/2019 21:14
YH
Safrole
BRL
1.2
20
ug/L
286923 1
10/25/2019 21:14
YH
Svm-Trinitrobenzene
BRL
098
10
ug/L
286923 l
10/25/2019 21:14
YH
Thionazin
BRL
0.81
20
ug/L
286923 l
10/25/2019 21:14
YH
SUIT:2.4.6-Tribromophenol
77
0
47-127
%REC
286923 1
10/25/201921:14
YH
Sun-: 2-Fluorobiphenyl
748
0
47 4-1 19
0-REC
286923 1
10/25/2019 21:14
YH
Sun-: 2-Fluorophenol
234 S
0
26.2-120
96REC
286923 1
10/25/2019 21:14
YH
Qu alifiersr \'attic exceeds maximum contammam level
E Estimated
\alue ibose
quanmation ranee
BRL Not Detected ai \IDL
S Spike Recor en• outside
hnuis due to matrix
H Holdmc times Ibr preparation or analysts exceeded
> Greater than Result 11luc
N Analvte not NELAC certified
J Estimated
salve detected
belo, Reportmc Limn
B Analvie detected in die associated inethod blank
< Less than
Result \line
Page I Page 47 of 67

Analytical Environmental Services, Inc
Date: 30-Oct-19
Zlient:
Prism Laboratories
Client Sample ID:
SW-02
Lab Order
1910021
Tag Number:
9100361-04
Project Name:
9100361
Collection Date:
10/22/2019 2:30:00 PM
Lab ID:
1910021-002A
Matrix:
Aqueous
Analyses Result Qual MDL ReportingUnits BatchID DF Date Analyzed Analyst
Limit
APPENDIXII-SEMIVOLATILE ORGANICS SW8270E (SW3510C)
Surr: 4-Terphenyl-d14 56.5 0 45-133 %REC 286923 1 10/25/2019 21:14 YH
Surr: Nitrobenzene-d5 83.1 0 41.9-121 %REC 286923 1 10/25/201921:14 YH
Surr: Phenol-d5 15.3 S 0 17.8-120 %REC 286923 1 10/25/201921:14 YH
Qualifiers: " Value exceeds maximum comanunaut level
BRL Not Dclecled at hIDL
FI Holding unties for preparation or analysis exceeded
N Anah to not NELAC tended
B Analtvle detected to the associated nuthod blank
E Estimated value above quanulatton range
S Spike Recohc)' outside limits due to malnx
> Greater than Result halue
J Estimated salue detected below Reporting Ltmu
Less than Result salue
Page 1 Page 48 of 67

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Page 56 of 67

ACCESS
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
ATTENTION
RobbiJones
PROJECTID
9100361
LABORATORY REPORT NUMBER
219102434
DATE
10/28/2019
Primary Data Review By
Authorized Signature
PLEASE NOTE:
Secondary Data Review By
Ashley B. Amick
Project Manager, Access Analytical, Inc.
[e-mail]
Unless otherwise noted, all analysis on this report performed at Pace Analytical Gulf Coast, 7979
Innovation Park Dr., Baton Rouge, LA 70820.
- Pace Gulf Coast is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab #
LA-01955, NELAP certified laboratory # 01955
- Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a
representative of Pace Guld Coast serving clients in the SC/NC/GA areas. All questions regarding this report
should be directed to your local Access Analytical representative at 803.781.4243 or toll free at 888.315.4243.
Lab Report#: 219102434 Page 1 of 11
Page 57 of 67

a ce Analytical
i
r
LELAP CERTIFICATE NUMBER: 01955
DOD -FLAP ACCREDITATION NUMBER: 74960
ANALYTICAL RESULTS
Pace Analytical Gulf Coast
7979 Innovation Park Dr.
Baton Rouge, LA 70820
[phone]
Report Date 10/28/2019
�11
ortp 219102434
�11�11
II �11 1�1 III 111 1�1 III
Project 9100361
Deliver To Additional Recipients
Robbi Jones NONE
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
800-529-6364
P�ccR
ISO
17025 TNI .
PJ LA fgQr
NoD FLAP
Lab Report#: 219102434 Page 2 of 11
Page 58 of 67

10
Pare Analytical
Report#: 219102434
Project ID: 9100361 Report Date: 10/28/2019
Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period the samples will be disposed in accordance with Pace Gulf Coast's Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
ND Indicates the result was Not Detected at the specified reporting limit
NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed in the Field
DL Detection Limit
LOD Limit of Detection
LOQ Limit of Quantitation
RE Re -analysis
CF HPLC or GC Confirmation
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or I Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
* Indicates a non -compliant or not applicable QC recovery or RPD — see narrative
E Organics - The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
L Reporting Limits adjusted to meet risk -based limit.
P RPD between primary and confirmation result is greater than 40
DL Diluted analysis —when appended to Client Sample ID
Sample receipt at Pace Gulf Coast is documented through the attached chain of custody. In accordance with NELAC, this report shall be
reproduced only in full and with the written permission of Pace Gulf Coast. The results contained within this report relate only to the samples
reported. The documented results are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if
applicable.
Authorized Signature
Pace Gulf Coast Report 219102434
Lab Report#: 219102434 Page 3 of 11
Page 59 of 67

Report#: 219102434
c CeAnJ/jltvl
Project ID: 9100361 Report Date: 10/28/2019
Certifications
Certification
Certification Number
DOD ELAP
74960
Alabama
01955
Arkansas
88-0655
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentucky
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
missis Sippi
01955
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
Washington
C929
USDA Soil Permit
P330-16-00234
Lab Report#: 219102434 Page 4 of 11
Page 60 of 67

Report#: 219102434
� : aeeM,7l�frcal
Project ID: 9100361 Report Date: 10/28/2019
Case Narrative
Client: Access Analytical Report: 219102434
Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found for the analyzed sample(s).
Lab Report#: 219102434 Page 5 of 11
Page 61 of 67

aceAnahli�ar Report#: 219102434
Project ID: 9100361
LAB ID Client ID
21910243401 MW-04
21910243402 MW-07
Sample Summary
Matrix Collect Date/Time
Water 10/22/201911:26
Water 10/22/201912:57
Report Date: 10/28/2019
Receive Date/Time
10/24/2019 10:10
10/24/2019 10:10
Lab Report#: 219102434 Page 6 of 11
Page 62 of 67

Report#: 219102434
� _, ceAr�al}�icar
Project ID: 9100361 Report Date: 10/28/2019
Summary of Compounds Detected
Collect Date 10/22/2019 11:26 LAB ID 21910243401
W-04
Receive Date 10/24/2019 10:10 Matrix Water
SM 5310 B-2011
CAS# Parameter Result DL LOQ Units
C-012 Total Organic Carbon 5.91 0.600 4.00 mg/L
Collect Date 10/22/2019 12:57 LAB ID 21910243402
MW-07
Receive Date 10/24/2019 10:10 Matrix Water
SM 5310 B-2011
CAS# Parameter
C-012 Total Organic Carbon
Result DL LOQ Units
10.6 0.600 4.00 mg/L
Lab Report#: 219102434
Page 7 of 11
Page 63 of 67

'!2ceAP,313dical
FMW-04
Report#: 219102434
Project ID: 9100361
Sample Results
Report Date: 10/28/2019
Collect Date 10/22/2019 11:26 LAB ID 21910243401
Receive Date 10/24/2019 10:10 Matrix Water
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 2 10/25/2019 23:10 PLH 670080
CAS#
C-012
MW-07
Parameter
Total Organic Carbon
Collect Date 10/22/2019 12:57
Receive Date 10/24/2019 10:10
Result DL LOQ Units
5.91 0.600 4.00 mg/L
LAB ID 21910243402
Matrix Water
i Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA 2 10/25/2019 23:30 PLH 670080
CAS# Parameter Result DL LOQ Units
C-012 Total Organic Carbon 10.6 0.600 4.00 mg/L
Lab Report#: 219102434 Page 8 of 11
Page 64 of 67

Report#: 219102434
i _ • conalytii;af
Project lD: 9100361
General Chemistry QC Summary
Report Date: 10/28/2019
Analytical Batch Client ID
MB670080
LCS670080
670080 LAB ID
1975365
1975366
Sample Type
MB
LCS
Prep Date
NA
NA
Analysis Date
10/25/2019 14:56
10/25/2019 13:56
Matrix
Water
Water
SM 5310 B-2011
units
mg/L
Spike
Result I %R
Control
I
Result
DL
Added
Limits%R
Total Organic Carbon I C-012
0.458J
1 0.300
50.0
50.1 100
90 - 110
Lab Report#: 219102434 Page 9 of 11
Page 65 of 67

Client ID: 4565 - Access Analytical
S°G: 219/02434 III i li li I III Ills
PM: °L" III i II II 1 ill I III
-� PRISM Full- unmen Analytical s v ..
� Env.rcnmenial Solutions
SUBCONTRACT ORDER
Cnlii,catian: LJ1C= li
Prism Laboratories, Inc. NC SC Other
9100361 N/A
ti};YRS\r_1_.�1 RATORT: RE 1'F.1V1N G L A BOR AT013Y:
Prism Lobomorics. inc. Pace Analyiinl O%Of Coast
P. O. Bux 240543 10791 Cm mcy Blvd
Charlol(c, NC'_3224-0543 Baton Rwgc. LA 70116
Phone: [phone] Vane ;(225) 767 %DO
Fax: [phone] r= (2717617.5711
Project Manager. Robbi A. Jones
Analysis
Due
Expires
La''bomtory lb Comments
W
\/
Sample 1D: 9300361-01
Water
Sampled: ]11221193]:26
TOC (Suh)
11 A 9119 11!26
SM 5310B
r'munr+rpi:c Sa/@ilrCC.
hew-b
�a
5-ample 1D: 9100361-02
1Vatcr
Sampled: 10/22i1972:57
TOC (Sub)
1 I.^,9%19 12:5'
SM 5310B
Cbmeir. era SuppiicJ:
.... ..ii •..
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Page 66 of 67

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I Page 67 of 67 1

LP R I S M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Anchor QEA of North Carolina, PLLC
Alec Macbeth
231 Haywood Street
Asheville, NC 28801
NC Certification No. 402 Case Narrative
NC Drinking Water Cert No. 37735 11/14/19 11:05
SC Certification No. 99012
Project: Jackson Cty Landfill 2019 Fall Samplling
Project No.: 50-02
Lab Submittal Date: 10/24/2019
Prism Work Order: 9100380
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Method 8270 analysis was subcontracted to AES. TOC was subcontracted to GCAL. Laboratory reports
are attached.
Prism Summary of Detections does not include subcontracted data.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones Reviewed By Robbi A. Jones
President/Project Manager President/Project Manager
Data Qualifiers Key Reference:
B Analyte is found in the associated blank at a concentration >1/2 RL.
BB Blank value is outside of the control limits. Validity of the data not affected.
HT Sample received and analyzed outside of the hold time.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 70

Sample Receipt Summary
R I IS M
Full -Service Analytical R
Environmental Solutions
11/14/2019
&GIE
LABORATORIES, INC.
Prism Work Order: 9100380
Client Sample ID
Lab Sample ID
Matrix
Date/Time Sampled Date/Time Received
MW-02
9100380-01
Water
10/23/19 9:26 10/24/19 9:10
MW-03
9100380-02
Water
10/23/19 10:26 10/24/19 9:10
MW-05R
9100380-03
Water
10/23/19 14:32 10/24/19 9:10
MW-06
9100380-04
Water
10/23/19 12:54 10/24/19 9:10
TB-02
9100380-05
Water
10/23/19 0:00 10/24/19 9:10
Samples were received in good condition at 3.3 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 2 of 70

/r P R I S M Full -Service Analytical s
Environmental Solutions
LABORATOR
Summary of Detections
11 /14/201 S
Prism Work Order: 9100380
Prism ID
Client ID
Parameter
Method
Result
Units
9100380-01
MW-02
Chloride
9056A
27000
ug/L
9100380-01
MW-02
Nitrate as N
9056A
170
J
ug/L
9100380-01
MW-02
Sulfate
9056A
21000
ug/L
9100380-01
MW-02
Chemical Oxygen Demand
SM5220 D
19000
J
ug/L
9100380-01
MW-02
Total Alkalinity to pH 4.5
SM2320 B
46000
ug/L
9100380-01
MW-02
Arsenic
6020B
1.3
ug/L
9100380-01
MW-02
Barium
6020B
76
ug/L
9100380-01
MW-02
Chromium
6020B
7.7
ug/L
9100380-01
MW-02
Cobalt
6020B
12
ug/L
9100380-01
MW-02
Copper
6020B
7.2
J
ug/L
9100380-01
MW-02
Lead
6020B
2.0
ug/L
9100380-01
MW-02
Nickel
6020B
4.9
ug/L
9100380-01
MW-02
Selenium
6020B
3.2
J
ug/L
9100380-01
MW-02
Vanadium
6020B
11
ug/L
9100380-01
MW-02
Zinc
6020B
35
ug/L
9100380-01
MW-02
Acetone
8260D
2.3
J
ug/L
9100380-01
MW-02
cis-1,2-Dichloroethylene
8260D
0.44
J
ug/L
9100380-01
MW-02
Naphthalene
8260D
0.67
.1
ug/L
9100380-01
MW-02
1,4-Dioxane
8260D SIM
4.0
ug/L
9100380-02
MW-03
Chloride
9056A
31000
ug/L
9100380-02
MW-03
Nitrate as N
9056A
7600
ug/L
9100380-02
MW-03
Sulfate
9056A
4400
ug/L
9100380-02
MW-03
Chemical Oxygen Demand
SM5220 D
23000
J
ug/L
9100380-02
MW-03
Sulfide
SM4500-S F
35000
ug/L
9100380-02
MW-03
Total Alkalinity to pH 4.5
SM2320 B
78000
ug/L
9100380-02
MW-03
Arsenic
6020B
0.62
J
ug/L
9100380-02
MW-03
Barium
6020B
200
ug/L
9100380-02
MW-03
Cadmium
6020B
0.42
J
ug/L
9100380-02
MW-03
Chromium
6020B
2.5
J
ug/L
9100380-02
MW-03
Cobalt
6020B
12
ug/L
9100380-02
MW-03
Copper
6020B
7.7
J
ug/L
9100380-02
MW-03
Nickel
6020B
17
ug/L
9100380-02
MW-03
Tin
6020B
3.6
J
ug/L
9100380-02
MW-03
Zinc
6020B
21
ug/L
9100380-02
MW-03
1,1-Dichloroethane
8260D
0.30
J
ug/L
9100380-02
MW-03
1,4-Dichlorobenzene
8260D
2.9
ug/L
9100380-02
MW-03
Acetone
8260D
3.4
J
ug/L
9100380-02
MW-03
Benzene
8260D
0.66
ug/L
9100380-02
MW-03
Chlorobenzene
8260D
6.3
ug/L
9100380-02
MW-03
cis-1,2-Dichloroethylene
8260D
0.96
ug/L
9100380-02
MW-03
1,4-Dioxane
8260D SIM
5.6
ug/L
9100380-03
MW-05R
Chloride
9056A
61000
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 3 of 70

/P R I S Full -Service Analytical
Environmental Solutions
� LABORATORIES, INC.
Summary of Detections
11 /14/2019
Prism Work Order: 9100380
Prism ID
Client ID
Parameter
Method
Result
Units
9100380-03
MW-05R
Nitrate as N
9056A
110
J
ug/L
9100380-03
MW-05R
Biochemical Oxygen Demand
SM5210 B
18000
BB, B
ug/L
9100380-03
MW-05R
Chemical Oxygen Demand
SM5220 D
58000
ug/L
9100380-03
MW-05R
Ferrous Iron
SM3500-Fe D
2000
HT
ug/L
9100380-03
MW-05R
Sulfide
SM4500-S F
30000
ug/L
9100380-03
MW-05R
Total Alkalinity to pH 4.5
SM2320 B
260000
ug/L
9100380-03
MW-05R
Arsenic
6020B
0.42
J
ug/L
9100380-03
MW-05R
Barium
6020B
120
ug/L
9100380-03
MW-05R
Cadmium
6020B
0.60
J
ug/L
9100380-03
MW-05R
Cobalt
6020B
10
ug/L
9100380-03
MW-05R
Nickel
6020B
4.3
ug/L
9100380-03
MW-05R
Zinc
6020B
17
J
ug/L
9100380-03
MW-05R
1,4-Dichlorobenzene
8260D
7.9
ug/L
9100380-03
MW-05R
Acetone
8260D
5.7
ug/L
9100380-03
MW-05R
Benzene
8260D
2.1
ug/L
9100380-03
MW-05R
Chlorobenzene
8260D
9.7
ug/L
9100380-03
MW-05R
cis-1,2-Dichloroethylene
8260D
4.7
ug/L
9100380-03
MW-05R
Tetrahydrofuran
8260D
7.7
J
ug/L
9100380-03
MW-05R
Vinyl chloride
8260D
1.8
ug/L
9100380-03
MW-05R
1,4-Dioxane
8260D SIM
5.8
ug/L
9100380-04
MW-06
Chloride
9056A
1100
ug/L
9100380-04
MW-06
Nitrate as N
9056A
240
ug/L
9100380-04
MW-06
Sulfate
9056A
710
J
ug/L
9100380-04
MW-06
Sulfide
SM4500-S F
30000
ug/L
9100380-04
MW-06
Total Alkalinity to pH 4.5
SM2320 B
24000
ug/L
9100380-04
MW-06
Barium
6020B
57
ug/L
9100380-04
MW-06
Cadmium
6020B
0.34
J
ug/L
9100380-04
MW-06
Cobalt
6020B
6.8
ug/L
9100380-04
MW-06
Nickel
6020B
14
ug/L
9100380-04
MW-06
Tin
6020B
4.9
J
ug/L
9100380-04
MW-06
Zinc
6020B
24
ug/L
9100380-04
MW-06
1,1-Dichloroethane
8260D
1.6
ug/L
9100380-04
MW-06
1,4-Dichlorobenzene
8260D
2.1
ug/L
9100380-04
MW-06
Acetone
8260D
3.5
.1
ug/L
9100380-04
MW-06
cis-1,2-Dichloroethylene
8260D
1.2
ug/L
9100380-05
TB-02
Acetone
8260D
2.7
J
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 70

PRISM Laboratory Report
Full -Service Analytical &
Environmental Solutions 11/14/2019
LABORATORIES, INC.
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Client Sample ID: MW-02
Attn: Alec Macbeth Samplling Prism Sample ID: 9100380-01
231 Haywood Street Project No.: 50-02 Prism Work Order: 9100380
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/23/19 09:26
Time Submitted: 10/24/19 09:10
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Anions by Ion Chromatography
Chloride
27000
ug/L
NE
1000
380
1
9056A
10/24/19 15:09BMS
P9J0437
Nitrate as N
170
J
ug/L
10000
200
54
1
9056A
10/24/19 15:09BMS
P9J0437
Sulfate
21000
ug/L
250000
2000
480
1
9056A
10/24/19 15:09BMS
P9J0437
General Chemistry Parameters
Biochemical Oxygen Demand
<210
BB
ug/L
NE
2000
210
1
SM5210 B
10/24/19 15:02CBM
P9J0483
Chemical Oxygen Demand
19000
J
ug/L
NE
50000
10000
1
SM5220 D
10/28/19 11:36SLS
P9J0486
Ferrous Iron
<51
HT
ug/L
NE
200
51
1
SM3500-Fe D
10/24/15 15:35BMS
P9J0473
Sulfide
<830
ug/L
1000
2000
830
1
SM4500-S F
10/29/19 9:45 CBM
P9J0504
Total Alkalinity to pH 4.5
46000
ug/L
NE
5000
770
1
SM2320 B
10/31/19 10:28CLB
P9J0537
Total Metals
Mercury
<0.034
ug/L
0.2
0.20
0.034
1
7470A
10/29/19 16:36JAB
P9J0493
Antimony
<0.93
ug/L
6
3.0
0.93
1
6020B
10/28/19 15:27MMR
P9J0440
Arsenic
1.3
ug/L
10
1.0
0.34
1
6020B
10/28/19 15:27MMR
P9J0440
Barium
76
ug/L
100
10
3.2
1
6020B
10/28/19 15:27MMR
P9J0440
Beryllium
<0.30
ug/L
1
1.0
0.30
1
6020B
10/28/19 15:27MMR
P9J0440
Cadmium
<0.22
ug/L
1
1.0
0.22
1
6020B
10/28/19 15:27MMR
P9J0440
Chromium
7.7
ug/L
10
3.0
0.90
1
6020B
10/28/19 15:27MMR
P9J0440
Cobalt
12
ug/L
10
2.0
0.70
1
6020B
10/28/19 15:27MMR
P9J0440
Copper
7.2
J
ug/L
10
10
4.7
1
6020B
10/28/19 15:27MMR
P9J0440
Lead
2.0
ug/L
10
1.0
0.44
1
6020B
10/28/19 15:27MMR
P9J0440
Nickel
4.9
ug/L
50
3.0
0.83
1
6020B
10/28/19 15:27MMR
P9J0440
Selenium
3.2
J
ug/L
10
5.0
0.98
1
6020B
10/28/19 15:27MMR
P9J0440
Silver
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 15:27MMR
P9J0440
Thallium
<0.84
ug/L
5.5
2.0
0.84
1
6020B
10/28/19 15:27MMR
P9J0440
Tin
<1.9
ug/L
100
5.0
1.9
1
6020B
10/28/19 15:27MMR
P9J0440
Vanadium
11
ug/L
25
5.0
1.5
1
6020B
10/28/19 15:27MMR
P9J0440
Zinc
35
ug/L
10
20
10
1
6020B
10/28/19 15:27MMR
P9J0440
Volatile Organic Compounds by GUMS
1, 1, 1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19 9:05 KDM
P9K0048
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19 9:05 KDM
1`91<0048
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
11/2/19 9:05 KDM
P9K0048
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
11/2/19 9:05 KDM
1`91<0048
1,1-Dichloroethane
<0.29
ug/L
5
0.50
0.29
1
8260D
11/2/19 9:05 KDM
P9K0048
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19 9:05 KDM
1`91<0048
1, 1 -Dichloropropylene
<0.37
ug/L
5
0.50
0.37
1
8260D
11/2/19 9:05 KDM
P9K0048
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
11/2/19 9:05 KDM
1`91<0048
1,2,4-Trichlorobenzene
<0.44
ug/L
10
1.0
0.44
1
8260D
11/2/19 9:05 KDM
P9K0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 70

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No.: 50-02
Sample Matrix: Water
Laboratory Report
11/14/2019
Client Sample ID: MW-02
Prism Sample ID: 9100380-01
Prism Work Order: 9100380
Time Collected: 10/23/19 09:26
Time Submitted: 10/24/19 09:10
Parameter
Result Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
11/2/19
9:05
KDM
P9K0048
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
11/2/19
9:05
KDM
P9K0048
1,2-Dichlorobenzene
<0.28
ug/L
5
0.50
0.28
1
8260D
11/2/19
9:05
KDM
P9K0048
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19
9:05
KDM
P9K0048
1,2-Dichloropropane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
9:05
KDM
P9K0048
1,3-Dichlorobenzene
<0.40
ug/L
5
0.50
0.40
1
8260D
11/2/19
9:05
KDM
P9K0048
1,3-Dichloropropane
<0.40
ug/L
1
0.50
0.40
1
8260D
11/2/19
9:05
KDM
P9K0048
1,4-Dichlorobenzene
<0.42
ug/L
1
0.50
0.42
1
8260D
11/2/19
9:05
KDM
P9K0048
2,2-Dichloropropane
<0.26
ug/L
15
2.0
0.26
1
8260D
11/2/19
9:05
KDM
P9K0048
Acetone
2.3
1 ug/L
100
5.0
0.70
1
8260D
11/2/19
9:05
KDM
P9K0048
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
11/2/19
9:05
KDM
P9K0048
Acrolein
<1.2
ug/L
53
20
1.2
1
8260D
11/2/19
9:05
KDM
P9K0048
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
11/2/19
9:05
KDM
P9K0048
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
11/2/19
9:05
KDM
P9K0048
Benzene
<0.34
ug/L
1
0.50
0.34
1
8260D
11/2/19
9:05
KDM
P91<0048
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
11/2/19
9:05
KDM
P9K0048
Bromodichloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
9:05
KDM
P9K0048
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
11/2/19
9:05
KDM
P9K0048
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
11/2/19
9:05
KDM
P9K0048
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
11/2/19
9:05
KDM
P9K0048
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
11/2/19
9:05
KDM
P9K0048
Chlorobenzene
<0.34
ug/L
3
0.50
0.34
1
8260D
11/2/19
9:05
KDM
P9K0048
Chloroethane
<0.43
ug/L
10
0.50
0.43
1
8260D
11/2/19
9:05
KDM
P9K0048
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
11/2/19
9:05
KDM
P9K0048
Chloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
9:05
KDM
P9K0048
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
11/2/19
9:05
KDM
P9K0048
cis-1,2-Dichloroethylene
0.44
J ug/L
2
0.50
0.40
1
8260D
11/2/19
9:05
KDM
P91(0048
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
11/2/19
9:05
KDM
P9K0048
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
11/2/19
9:05
KDM
P9K0048
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
11/2/19
9:05
KDM
P9K0048
Dichlorodifluoromethane
<0.47
ug/L
5
5.0
0.47
1
8260D
11/2/19
9:05
KDM
P9K0048
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
11/2/19
9:05
KDM
P9K0048
Ethylbenzene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
9:05
KDM
P9K0048
Hexachlorobutadiene
<0.24
ug/L
10
2.0
0.24
1
8260D
11/2/19
9:05
KDM
P9K0048
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
11/2/19
9:05
KDM
P9K0048
m,p-Xylenes
<0.73
ug/L
NE
1.0
0.73
1
8260D
11/2/19
9:05
KDM
P9K0048
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
11/2/19
9:05
KDM
P9K0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 70

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 11/14/2019
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Client Sample ID: MW-02
Attn: Alec Macbeth Samplling Prism Sample ID: 9100380-01
231 Haywood Street Project No.: 50-02 Prism Work Order: 9100380
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/23/19 09:26
Time Submitted: 10/24/19 09:10
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
11/2/19
9:05
KDM
P91<0048
Methyl Ethyl Ketone (2-Butanone)
<0.78
ug/L
100
5.0
0.78
1
8260D
11/2/19
9:05
KDM
P9K0048
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
11/2/19
9:05
KDM
P91<0048
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
11/2/19
9:05
KDM
P9K0048
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
11/2/19
9:05
KDM
P91<0048
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1
8260D
11/2/19
9:05
KDM
P9K0048
Naphthalene
0.67 J
ug/L
10
1.0
0.45
1
8260D
11/2/19
9:05
KDM
P9K0048
o-Xylene
<0.40
ug/L
NE
0.50
0.40
1
8260D
11/2/19
9:05
KDM
P9K0048
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
11/2/19
9:05
KDM
P91<0048
Styrene
<0.26
ug/L
1
0.50
0.26
1
8260D
11/2/19
9:05
KDM
P9K0048
Tetrachloroethylene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
9:05
KDM
P91<0048
Tetrahydrofuran
<0.68
ug/L
NE
10
0.68
1
8260D
11/2/19
9:05
KDM
P9K0048
Toluene
<0.35
ug/L
1
0.50
0.35
1
8260D
11/2/19
9:05
KDM
P91<0048
trans- 1,2-Dichloroethylene
<0.27
ug/L
5
0.50
0.27
1
8260D
11/2/19
9:05
KDM
P9K0048
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1
8260D
11/2/19
9:05
KDM
P91<0048
trans- 1,4-Dich loro-2-butene
<0.22
ug/L
100
10
0.22
1
8260D
11/2/19
9:05
KDM
P9K0048
Trichloroethylene
<0.46
ug/L
1
0.50
0.46
1
8260D
11/2/19
9:05
KDM
P91<0048
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1
8260D
11/2/19
9:05
KDM
P9K0048
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1
8260D
11/2/19
9:05
KDM
P91<0048
Vinyl chloride
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19
9:05
KDM
P9K0048
Xylenes, total
<1.1
ug/L
5
1.5
1.1
1
8260D
11/2/19
9:05
KDM
P91<0048
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
80-124
Dibromofluoromethane
101 %
75-129
Toluene-d8
99 %
77-123
Volatile Organic Compounds by GUMS SIM
1,4-Dioxane
4.0
ug/L
10
2.0
0.14
1
8260D SIM
10/25/19 14:10TBL
P9J0421
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 70

�Full-Service Analytical
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
11 /14/2019
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No.: 50-02
Sample Matrix: Water
Client Sample ID: MW-03
Prism Sample ID: 9100380-02
Prism Work Order: 9100380
Time Collected: 10/23/19 10:26
Time Submitted: 10/24/19 09:10
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Anions by Ion Chromatography
Chloride
31000
ug/L
NE
1000
380
1
9056A
10/24/19 15:24BMS
P9J0437
Nitrate as N
7600
ug/L
10000
200
54
1
9056A
10/24/19 15:24BMS
P9J0437
Sulfate
4400
ug/L
250000
2000
480
1
9056A
10/24/19 15:24BMS
P9J0437
General Chemistry Parameters
Biochemical Oxygen Demand
<210 BB
ug/L
NE
2000
210
1
SM5210 B
10/24/19 15:02CBM
P9J0483
Chemical Oxygen Demand
23000 J
ug/L
NE
50000
10000
1
SM5220 D
10/28/19 11:36SLS
P9J0486
Ferrous Iron
<51 HT
ug/L
NE
200
51
1
SM3500-Fe D
10/24/15 15:35BMS
P9J0473
Sulfide
35000
ug/L
1000
2000
830
1
SM4500-S F
10/29/19 9:45 CBM
P9J0504
Total Alkalinity to pH 4.5
78000
ug/L
NE
5000
770
1
SM2320 B
10/31/19 10:28CLB
P9J0537
Total Metals
Mercury
<0.034
ug/L
0.2
0.20
0.034
1
7470A
10/29/19 16:40JAB
P9J0493
Antimony
<0.93
ug/L
6
3.0
0.93
1
6020B
10/28/19 15:34MMR
P9J0440
Arsenic
0.62
J
ug/L
10
1.0
0.34
1
6020B
10/28/19 15:34MMR
P9J0440
Barium
200
ug/L
100
10
3.2
1
6020B
10/28/19 15:34MMR
P9J0440
Beryllium
<0.30
ug/L
1
1.0
0.30
1
6020B
10/28/19 15:34MMR
P9J0440
Cadmium
0.42
J
ug/L
1
1.0
0.22
1
6020B
10/28/19 15:34MMR
P9J0440
Chromium
2.5
J
ug/L
10
3.0
0.90
1
6020B
10/28/19 15:34MMR
P9J0440
Cobalt
12
ug/L
10
2.0
0.70
1
6020B
10/28/19 15:34MMR
P9J0440
Copper
7.7
J
ug/L
10
10
4.7
1
6020B
10/28/19 15:34MMR
P9J0440
Lead
<0.44
ug/L
10
1.0
0.44
1
6020B
10/28/19 15:34MMR
P9J0440
Nickel
17
ug/L
50
3.0
0.83
1
6020B
10/28/19 15:34MMR
P9J0440
Selenium
<0.98
ug/L
10
5.0
0.98
1
6020B
10/28/19 15:34MMR
P9J0440
Silver
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 15:34MMR
P9J0440
Thallium
<0.84
ug/L
5.5
2.0
0.84
1
6020B
10/28/19 15:34MMR
P9J0440
Tin
3.6
J
ug/L
100
5.0
1.9
1
6020B
10/28/19 15:34MMR
P9J0440
Vanadium
<1.5
ug/L
25
5.0
1.5
1
6020B
10/28/19 15:34MMR
P9J0440
Zinc
21
ug/L
10
20
10
1
6020B
10/28/19 15:34MMR
P9J0440
Volatile Organic Compounds
by GC/MS
1,1,1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19 9:32 KDM
P91<0048
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19 9:32 KDM
P9K0048
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
11/2/19 9:32 KDM
P91<0048
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
11/2/19 9:32 KDM
P9K0048
1,1-Dichloroethane
0.30
J
ug/L
5
0.50
0.29
1
8260D
11/2/19 9:32 KDM
P91(0048
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19 9:32 KDM
P9K0048
1, 1 -Dichloropropylene
<0.37
ug/L
5
0.50
0.37
1
8260D
11/2/19 9:32 KDM
P91<0048
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
11/2/19 9:32 KDM
P9K0048
1,2,4-Trichlorobenzene
<0.44
ug/L
10
1.0
0.44
1
8260D
11/2/19 9:32 KDM
P91<0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 70

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No.: 50-02
Sample Matrix: Water
Laboratory Report
11/14/2019
Client Sample ID: MW-03
Prism Sample ID: 9100380-02
Prism Work Order: 9100380
Time Collected: 10/23/19 10:26
Time Submitted: 10/24/19 09:10
Parameter
Result Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
11/2/19
9:32
KDM
P9K0048
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
11/2/19
9:32
KDM
P9K0048
1,2-Dichlorobenzene
<0.28
ug/L
5
0.50
0.28
1
8260D
11/2/19
9:32
KDM
P9K0048
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19
9:32
KDM
P9K0048
1,2-Dichloropropane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
9:32
KDM
P9K0048
1,3-Dichlorobenzene
<0.40
ug/L
5
0.50
0.40
1
8260D
11/2/19
9:32
KDM
P9K0048
1,3-Dichloropropane
<0.40
ug/L
1
0.50
0.40
1
8260D
11/2/19
9:32
KDM
P9K0048
1,4-Dichlorobenzene
2.9
ug/L
1
0.50
0.42
1
8260D
11/2/19
9:32
KDM
P9K0048
2,2-Dichloropropane
<0.26
ug/L
15
2.0
0.26
1
8260D
11/2/19
9:32
KDM
P9K0048
Acetone
3.4
1 ug/L
100
5.0
0.70
1
8260D
11/2/19
9:32
KDM
P9K0048
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
11/2/19
9:32
KDM
P9K0048
Acrolein
<1.2
ug/L
53
20
1.2
1
8260D
11/2/19
9:32
KDM
P91<0048
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
11/2/19
9:32
KDM
P9K0048
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
11/2/19
9:32
KDM
P91<0048
Benzene
0.66
ug/L
1
0.50
0.34
1
8260D
11/2/19
9:32
KDM
P9K0048
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
11/2/19
9:32
KDM
P9K0048
Bromodichloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
9:32
KDM
P91<0048
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
11/2/19
9:32
KDM
P9K0048
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
11/2/19
9:32
KDM
P91<0048
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
11/2/19
9:32
KDM
P9K0048
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
11/2/19
9:32
KDM
P91<0048
Chlorobenzene
6.3
ug/L
3
0.50
0.34
1
8260D
11/2/19
9:32
KDM
P9K0048
Chloroethane
<0.43
ug/L
10
0.50
0.43
1
8260D
11/2/19
9:32
KDM
P9K0048
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
11/2/19
9:32
KDM
P9K0048
Chloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
9:32
KDM
P9K0048
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
11/2/19
9:32
KDM
P9K0048
cis-1,2-Dichloroethylene
0.96
ug/L
2
0.50
0.40
1
8260D
11/2/19
9:32
KDM
P9K0048
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
11/2/19
9:32
KDM
P9K0048
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
11/2/19
9:32
KDM
P9K0048
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
11/2/19
9:32
KDM
P9K0048
Dichlorodifluoromethane
<0.47
ug/L
5
5.0
0.47
1
8260D
11/2/19
9:32
KDM
P9K0048
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
11/2/19
9:32
KDM
P9K0048
Ethylbenzene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
9:32
KDM
P9K0048
Hexachlorobutadiene
<0.24
ug/L
10
2.0
0.24
1
8260D
11/2/19
9:32
KDM
P9K0048
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
11/2/19
9:32
KDM
P9K0048
m,p-Xylenes
<0.73
ug/L
NE
1.0
0.73
1
8260D
11/2/19
9:32
KDM
P9K0048
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
11/2/19
9:32
KDM
P9K0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 70

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 11/14/2019
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Client Sample ID: MW-03
Attn: Alec Macbeth Samplling Prism Sample ID: 9100380-02
231 Haywood Street Project No.: 50-02 Prism Work Order: 9100380
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/23/19 10:26
Time Submitted: 10/24/19 09:10
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
11/2/19
9:32
KDM
P91<0048
Methyl Ethyl Ketone (2-Butanone)
<0.78
ug/L
100
5.0
0.78
1
8260D
11/2/19
9:32
KDM
P9K0048
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
11/2/19
9:32
KDM
P91<0048
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
11/2/19
9:32
KDM
P9K0048
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
11/2/19
9:32
KDM
P91<0048
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1
8260D
11/2/19
9:32
KDM
P9K0048
Naphthalene
<0.45
ug/L
10
1.0
0.45
1
8260D
11/2/19
9:32
KDM
P91<0048
o-Xylene
<0.40
ug/L
NE
0.50
0.40
1
8260D
11/2/19
9:32
KDM
P9K0048
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
11/2/19
9:32
KDM
P91<0048
Styrene
<0.26
ug/L
1
0.50
0.26
1
8260D
11/2/19
9:32
KDM
P9K0048
Tetrachloroethylene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
9:32
KDM
P91<0048
Tetrahydrofuran
<0.68
ug/L
NE
10
0.68
1
8260D
11/2/19
9:32
KDM
P9K0048
Toluene
<0.35
ug/L
1
0.50
0.35
1
8260D
11/2/19
9:32
KDM
P91<0048
trans- 1,2-Dichloroethylene
<0.27
ug/L
5
0.50
0.27
1
8260D
11/2/19
9:32
KDM
P9K0048
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1
8260D
11/2/19
9:32
KDM
P91<0048
trans- 1,4-Dich loro-2-butene
<0.22
ug/L
100
10
0.22
1
8260D
11/2/19
9:32
KDM
P9K0048
Trichloroethylene
<0.46
ug/L
1
0.50
0.46
1
8260D
11/2/19
9:32
KDM
P91<0048
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1
8260D
11/2/19
9:32
KDM
P9K0048
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1
8260D
11/2/19
9:32
KDM
P91<0048
Vinyl chloride
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19
9:32
KDM
P9K0048
Xylenes, total
<1.1
ug/L
5
1.5
1.1
1
8260D
11/2/19
9:32
KDM
P9K0048
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
99 %
80-124
Dibromofluoromethane
100 %
75-129
Toluene-d8
99 %
77-123
Volatile Organic Compounds by GUMS SIM
1,4-Dioxane
5.6
ug/L
10
2.0
0.14
1
8260D SIM
10/25/19 14:35TBL
P9J0421
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 70

�Full-Service Analytical
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
11 /14/2019
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No.: 50-02
Sample Matrix: Water
Client Sample ID: MW-05R
Prism Sample ID: 9100380-03
Prism Work Order: 9100380
Time Collected: 10/23/19 14:32
Time Submitted: 10/24/19 09:10
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Anions by Ion Chromatography
Chloride
61000
ug/L
NE
1000
380
1 9056A
10/24/19 15:39BMS
P9J0437
Nitrate as N
110 J
ug/L
10000
200
54
1 9056A
10/24/19 15:39BMS
P9J0437
Sulfate
<480
ug/L
250000
2000
480
1 9056A
10/24/19 15:39BMS
P9J0437
General Chemistry Parameters
Biochemical Oxygen Demand
18000 BB,
ug/L
NE
2000
210
1 SM5210 B
10/24/19 15:02CBM
P9J0483
B
Chemical Oxygen Demand
Ferrous Iron
Sulfide
Total Alkalinity to pH 4.5
Total Metals
58000
2000
30000
260000
HT
ug/L
ug/L
ug/L
ug/L
NE
NE
1000
NE
50000
200
2000
5000
10000
51
830
770
1
1
1
1
SM5220 D
SM3500-Fe D
SM4500-S F
SM2320 B
10/28/19 11:36SLS
10/24/15 15:35BMS
10/29/19 9:45 CBM
10/31/19 10:28CLB
P9J0486
P9J0473
P9J0504
P9J0537
Mercury
<0.034
ug/L
0.2
0.20
0.034
1
7470A
10/29/19 16:44JAB
P9J0493
Antimony
<0.93
ug/L
6
3.0
0.93
1
6020B
10/28/19 15:40MMR
P9J0440
Arsenic
0.42
J
ug/L
10
1.0
0.34
1
6020B
10/28/19 15:40MMR
P9J0440
Barium
120
ug/L
100
10
3.2
1
6020B
10/28/19 15:40MMR
P9J0440
Beryllium
<0.30
ug/L
1
1.0
0.30
1
6020B
10/28/19 15:40MMR
P9J0440
Cadmium
0.60
J
ug/L
1
1.0
0.22
1
6020B
10/28/19 15:40MMR
P9J0440
Chromium
<0.90
ug/L
10
3.0
0.90
1
6020B
10/28/19 15:40MMR
P9J0440
Cobalt
10
ug/L
10
2.0
0.70
1
6020B
10/28/19 15:40MMR
P9J0440
Copper
<4.7
ug/L
10
10
4.7
1
6020B
10/28/19 15:40MMR
P9J0440
Lead
<0.44
ug/L
10
1.0
0.44
1
6020B
10/28/19 15:40MMR
P9J0440
Nickel
4.3
ug/L
50
3.0
0.83
1
6020B
10/28/19 15:40MMR
P9J0440
Selenium
<0.98
ug/L
10
5.0
0.98
1
6020B
10/28/19 15:40MMR
P9J0440
Silver
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 15:40MMR
P9J0440
Thallium
<0.84
ug/L
5.5
2.0
0.84
1
6020B
10/28/19 15:40MMR
P9J0440
Tin
<1.9
ug/L
100
5.0
1.9
1
6020B
10/28/19 15:40MMR
P9J0440
Vanadium
<1.5
ug/L
25
5.0
1.5
1
6020B
10/28/19 15:40MMR
P9J0440
Zinc
17
J
ug/L
10
20
10
1
6020B
10/28/19 15:40MMR
P9J0440
Volatile Organic Compounds by GUMS
1, 1, 1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19 9:58 KDM
P91<0048
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19 9:58 KDM
P9K0048
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
11/2/19 9:58 KDM
P91<0048
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
11/2/19 9:58 KDM
P9K0048
1,1-Dichloroethane
<0.29
ug/L
5
0.50
0.29
1
8260D
11/2/19 9:58 KDM
P91<0048
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19 9:58 KDM
P9K0048
1, 1 -Dichloropropylene
<0.37
ug/L
5
0.50
0.37
1
8260D
11/2/19 9:58 KDM
P91<0048
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
11/2/19 9:58 KDM
P9K0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 70

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No.: 50-02
Sample Matrix: Water
Laboratory Report
11/14/2019
Client Sample ID: MW-05R
Prism Sample ID: 9100380-03
Prism Work Order: 9100380
Time Collected: 10/23/19 14:32
Time Submitted: 10/24/19 09:10
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,2,4-Trichlorobenzene
<0.44
ug/L
10
1.0
0.44
1
8260D
11/2/19
9:58
KDM
P9K0048
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
11/2/19
9:58
KDM
P9K0048
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
11/2/19
9:58
KDM
P9K0048
1,2-Dichlorobenzene
<0.28
ug/L
5
0.50
0.28
1
8260D
11/2/19
9:58
KDM
P9K0048
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19
9:58
KDM
P9K0048
1,2-Dichloropropane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
9:58
KDM
P9K0048
1,3-Dichlorobenzene
<0.40
ug/L
5
0.50
0.40
1
8260D
11/2/19
9:58
KDM
P9K0048
1,3-Dichloropropane
<0.40
ug/L
1
0.50
0.40
1
8260D
11/2/19
9:58
KDM
P9K0048
1,4-Dichlorobenzene
7.9
ug/L
1
0.50
0.42
1
8260D
11/2/19
9:58
KDM
P9K0048
2,2-Dichloropropane
<0.26
ug/L
15
2.0
0.26
1
8260D
11/2/19
9:58
KDM
P91<0048
Acetone
5.7
ug/L
100
5.0
0.70
1
8260D
11/2/19
9:58
KDM
P9K0048
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
11/2/19
9:58
KDM
P9K0048
Acrolein
<1.2
ug/L
53
20
1.2
1
8260D
11/2/19
9:58
KDM
P91<0048
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
11/2/19
9:58
KDM
P9K0048
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
11/2/19
9:58
KDM
P91<0048
Benzene
2.1
ug/L
1
0.50
0.34
1
8260D
11/2/19
9:58
KDM
P9K0048
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
11/2/19
9:58
KDM
P9K0048
Bromodichloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
9:58
KDM
P9K0048
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
11/2/19
9:58
KDM
P9K0048
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
11/2/19
9:58
KDM
P9K0048
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
11/2/19
9:58
KDM
P9K0048
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
11/2/19
9:58
KDM
P9K0048
Chlorobenzene
9.7
ug/L
3
0.50
0.34
1
8260D
11/2/19
9:58
KDM
P91<0048
Chloroethane
<0.43
ug/L
10
0.50
0.43
1
8260D
11/2/19
9:58
KDM
P9K0048
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
11/2/19
9:58
KDM
P9K0048
Chloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
9:58
KDM
P9K0048
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
11/2/19
9:58
KDM
P9K0048
cis-1,2-Dichloroethylene
4.7
ug/L
2
0.50
0.40
1
8260D
11/2/19
9:58
KDM
P91<0048
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
11/2/19
9:58
KDM
P9K0048
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
11/2/19
9:58
KDM
P9K0048
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
11/2/19
9:58
KDM
P9K0048
Dichlorodifluoromethane
<0.47
ug/L
5
5.0
0.47
1
8260D
11/2/19
9:58
KDM
P9K0048
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
11/2/19
9:58
KDM
P9K0048
Ethylbenzene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
9:58
KDM
P9K0048
Hexachlorobutadiene
<0.24
ug/L
10
2.0
0.24
1
8260D
11/2/19
9:58
KDM
P9K0048
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
11/2/19
9:58
KDM
P9K0048
m,p-Xylenes
<0.73
ug/L
NE
1.0
0.73
1
8260D
11/2/19
9:58
KDM
P9K0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 70

Laboratory Report
Full -Service Analytical &
P R S M
Environmental Solutions
LABORATORIES INC.
11/14/2019
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2019
Fall
Client
Sample ID:
MW-05R
Attn: Alec Macbeth
Samplling
Prism
Sample ID:
9100380-03
231 Haywood Street
Project No.:
50-02
Prism
Work Order:
9100380
Asheville, NC 28801
Sample Matrix:
Water
Time
Collected: 10/23/19 14:32
Time
Submitted: 10/24/19
09:10
Parameter
Result Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
11/2/19 9:58
KDM
P91<0048
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
11/2/19 9:58
KDM
P9K0048
Methyl Ethyl Ketone (2-Butanone)
<0.78
ug/L
100
5.0
0.78
1
8260D
11/2/19 9:58
KDM
P91<0048
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
11/2/19 9:58
KDM
P9K0048
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
11/2/19 9:58
KDM
P91<0048
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
11/2/19 9:58
KDM
P9K0048
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1
8260D
11/2/19 9:58
KDM
P91<0048
Naphthalene
<0.45
ug/L
10
1.0
0.45
1
8260D
11/2/19 9:58
KDM
P9K0048
o-Xylene
<0.40
ug/L
NE
0.50
0.40
1
8260D
11/2/19 9:58
KDM
P91<0048
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
11/2/19 9:58
KDM
P9K0048
Styrene
<0.26
ug/L
1
0.50
0.26
1
8260D
11/2/19 9:58
KDM
P91<0048
Tetrachloroethylene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19 9:58
KDM
P9K0048
Tetrahydrofuran
7.7
J ug/L
NE
10
0.68
1
8260D
11/2/19 9:58
KDM
P91<0048
Toluene
<0.35
ug/L
1
0.50
0.35
1
8260D
11/2/19 9:58
KDM
P9K0048
trans- 1,2-Dichloroethylene
<0.27
ug/L
5
0.50
0.27
1
8260D
11/2/19 9:58
KDM
P91<0048
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1
8260D
11/2/19 9:58
KDM
P9K0048
trans- IIA-Dich loro-2-butene
<0.22
ug/L
100
10
0.22
1
8260D
11/2/19 9:58
KDM
P91<0048
Trichloroethylene
<0.46
ug/L
1
0.50
0.46
1
8260D
11/2/19 9:58
KDM
P9K0048
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1
8260D
11/2/19 9:58
KDM
P91<0048
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1
8260D
11/2/19 9:58
KDM
P9K0048
Vinyl chloride
1.8
ug/L
1
0.50
0.41
1
8260D
11/2/19 9:58
KDM
P91<0048
Xylenes, total
<1.1
ug/L
5
1.5
1.1
1
8260D
11/2/19 9:58
KDM
P91<0048
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
80-124
Dibromofluoromethane
100 %
75-129
Toluene-d8
99 %
77-123
Volatile Organic Compounds by GUMS SIM
1,4-Dioxane
5.8
ug/L
10
2.0
0.14
1
8260D SIM
10/25/19 15:00TBL
P9J0421
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 70

Laboratory Report
Full -Service
P R S M
Analytical &
Environmental
LABORATORIES INC.
Solutions
11/14/2019
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill
2019
Fall
Client Sample ID: MW-06
Attn: Alec Macbeth
Samplling
Prism Sample ID: 9100380-04
231 Haywood Street
Project No.:
50-02
Prism Work Order: 9100380
Asheville, NC 28801
Sample Matrix:
Water
Time Collected: 10/23/19 12:54
Time Submitted: 10/24/19 09:10
Parameter
Result Units
SWSL
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
Anions by Ion Chromatography
Chloride
1100
ug/L
NE
1000
380
1 9056A 10/24/19 15:54BMS
P9J0437
Nitrate as N
240
ug/L
10000
200
54
1 9056A 10/24/19 15:54BMS
P9J0437
Sulfate
710
J ug/L
250000
2000
480
1 9056A 10/24/19 15:54BMS
P9J0437
General Chemistry Parameters
Biochemical Oxygen Demand
<210
BB ug/L
NE
2000
210
1 SM5210 B 10/24/19 15:02CBM
P9J0483
Chemical Oxygen Demand
<10000
ug/L
NE
50000
10000
1 SM5220 D 10/28/19 11:36SLS
P9J0486
Ferrous Iron
<51
HT ug/L
NE
200
51
1 SM3500-Fe D 10/24/15 15:35BMS
P9J0473
Sulfide
30000
ug/L
1000
2000
830
1 SM4500-S F 10/29/19 9:45 CBM
P9J0504
Total Alkalinity to pH 4.5
24000
ug/L
NE
5000
770
1 SM2320 B 10/31/19 10:28CLB
P9J0537
Total Metals
Mercury
<0.034
ug/L
0.2
0.20
0.034
1
7470A
10/29/19 16:47JAB
P9J0493
Antimony
<0.93
ug/L
6
3.0
0.93
1
6020B
10/28/19 15:47MMR
P9J0440
Arsenic
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 15:47MMR
P9J0440
Barium
57
ug/L
100
10
3.2
1
6020B
10/28/19 15:47MMR
P9J0440
Beryllium
<0.30
ug/L
1
1.0
0.30
1
6020B
10/28/19 15:47MMR
P9J0440
Cadmium
0.34 J
ug/L
1
1.0
0.22
1
6020B
10/28/19 15:47MMR
P9J0440
Chromium
<0.90
ug/L
10
3.0
0.90
1
6020B
10/28/19 15:47MMR
P9J0440
Cobalt
6.8
ug/L
10
2.0
0.70
1
6020B
10/28/19 15:47MMR
P9J0440
Copper
<4.7
ug/L
10
10
4.7
1
6020B
10/28/19 15:47MMR
P9J0440
Lead
<0.44
ug/L
10
1.0
0.44
1
6020B
10/28/19 15:47MMR
P9J0440
Nickel
14
ug/L
50
3.0
0.83
1
6020B
10/28/19 15:47MMR
P9J0440
Selenium
<0.98
ug/L
10
5.0
0.98
1
6020B
10/28/19 15:47MMR
P9J0440
Silver
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 15:47MMR
P9J0440
Thallium
<0.84
ug/L
5.5
2.0
0.84
1
6020B
10/28/19 15:47MMR
P9J0440
Tin
4.9 J
ug/L
100
5.0
1.9
1
6020B
10/28/19 15:47MMR
P9J0440
Vanadium
<1.5
ug/L
25
5.0
1.5
1
6020B
10/28/19 15:47MMR
P9J0440
Zinc
24
ug/L
10
20
10
1
6020B
10/28/19 15:47MMR
P9J0440
Volatile Organic Compounds by GUMS
1, 1, 1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19 10:24 KDM
P9K0048
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19 10:24 KDM
P91<0048
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
11/2/19 10:24 KDM
P9K0048
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
11/2/19 10:24 KDM
P91<0048
1,1-Dichloroethane
1.6
ug/L
5
0.50
0.29
1
8260D
11/2/19 10:24 KDM
P9K0048
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19 10:24 KDM
P9K0048
1, 1 -Dichloropropylene
<0.37
ug/L
5
0.50
0.37
1
8260D
11/2/19 10:24 KDM
P91<0048
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
11/2/19 10:24 KDM
P9K0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 70

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No.: 50-02
Sample Matrix: Water
Laboratory Report
11/14/2019
Client Sample ID: MW-06
Prism Sample ID: 9100380-04
Prism Work Order: 9100380
Time Collected: 10/23/19 12:54
Time Submitted: 10/24/19 09:10
Parameter
Result Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,2,4-Trichlorobenzene
<0.44
ug/L
10
1.0
0.44
1
8260D
11/2/19 10:24 KDM
P9K0048
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
11/2/19 10:24 KDM
P9K0048
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
11/2/19 10:24 KDM
P9K0048
1,2-Dichlorobenzene
<0.28
ug/L
5
0.50
0.28
1
8260D
11/2/19 10:24 KDM
P9K0048
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19 10:24 KDM
P9K0048
1,2-Dichloropropane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19 10:24 KDM
P9K0048
1,3-Dichlorobenzene
<0.40
ug/L
5
0.50
0.40
1
8260D
11/2/19 10:24 KDM
P9K0048
1,3-Dichloropropane
<0.40
ug/L
1
0.50
0.40
1
8260D
11/2/19 10:24 KDM
P9K0048
1,4-Dichlorobenzene
2.1
ug/L
1
0.50
0.42
1
8260D
11/2/19 10:24 KDM
P91(0048
2,2-Dichloropropane
<0.26
ug/L
15
2.0
0.26
1
8260D
11/2/19 10:24 KDM
P91<0048
Acetone
3.5
j ug/L
100
5.0
0.70
1
8260D
11/2/19 10:24 KDM
P9K0048
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
11/2/19 10:24 KDM
P91<0048
Acrolein
<1.2
ug/L
53
20
1.2
1
8260D
11/2/19 10:24 KDM
P9K0048
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
11/2/19 10:24 KDM
P91<0048
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
11/2/19 10:24 KDM
P9K0048
Benzene
<0.34
ug/L
1
0.50
0.34
1
8260D
11/2/19 10:24 KDM
P91<0048
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
11/2/19 10:24 KDM
P9K0048
Bromodichloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19 10:24 KDM
P91<0048
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
11/2/19 10:24 KDM
P9K0048
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
11/2/19 10:24 KDM
P91<0048
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
11/2/19 10:24 KDM
P9K0048
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
11/2/19 10:24 KDM
P91<0048
Chlorobenzene
<0.34
ug/L
3
0.50
0.34
1
8260D
11/2/19 10:24 KDM
P9K0048
Chloroethane
<0.43
ug/L
10
0.50
0.43
1
8260D
11/2/19 10:24 KDM
P91<0048
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
11/2/19 10:24 KDM
P9K0048
Chloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19 10:24 KDM
P91<0048
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
11/2/19 10:24 KDM
P9K0048
cis-1,2-Dichloroethylene
1.2
ug/L
2
0.50
0.40
1
8260D
11/2/19 10:24 KDM
P9K0048
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
11/2/19 10:24 KDM
P91<0048
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
11/2/19 10:24 KDM
P9K0048
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
11/2/19 10:24 KDM
P91<0048
Dichlorodifluoromethane
<0.47
ug/L
5
5.0
0.47
1
8260D
11/2/19 10:24 KDM
P9K0048
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
11/2/19 10:24 KDM
P91<0048
Ethylbenzene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19 10:24 KDM
P9K0048
Hexachlorobutadiene
<0.24
ug/L
10
2.0
0.24
1
8260D
11/2/19 10:24 KDM
P91<0048
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
11/2/19 10:24 KDM
P9K0048
m,p-Xylenes
<0.73
ug/L
NE
1.0
0.73
1
8260D
11/2/19 10:24 KDM
P91<0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 70

P R S M Laboratory Report
Full -Service Analytical &
Environmental Solutions 11/14/2019
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Client Sample ID: MW-06
Attn: Alec Macbeth Samplling Prism Sample ID: 9100380-04
231 Haywood Street Project No.: 50-02 Prism Work Order: 9100380
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/23/19 12:54
Time Submitted: 10/24/19 09:10
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
11/2/19 10:24 KDM
P91<0048
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
11/2/19 10:24 KDM
P9K0048
Methyl Ethyl Ketone (2-Butanone)
<0.78
ug/L
100
5.0
0.78
1
8260D
11/2/19 10:24 KDM
P91<0048
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
11/2/19 10:24 KDM
P9K0048
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
11/2/19 10:24 KDM
P91<0048
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
11/2/19 10:24 KDM
P9K0048
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1
8260D
11/2/19 10:24 KDM
P91<0048
Naphthalene
<0.45
ug/L
10
1.0
0.45
1
8260D
11/2/19 10:24 KDM
P9K0048
o-Xylene
<0.40
ug/L
NE
0.50
0.40
1
8260D
11/2/19 10:24 KDM
P91<0048
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
11/2/19 10:24 KDM
P9K0048
Styrene
<0.26
ug/L
1
0.50
0.26
1
8260D
11/2/19 10:24 KDM
P91<0048
Tetrachloroethylene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19 10:24 KDM
P9K0048
Tetrahydrofuran
<0.68
ug/L
NE
10
0.68
1
8260D
11/2/19 10:24 KDM
P91<0048
Toluene
<0.35
ug/L
1
0.50
0.35
1
8260D
11/2/19 10:24 KDM
P9K0048
trans- 1,2-Dichloroethylene
<0.27
ug/L
5
0.50
0.27
1
8260D
11/2/19 10:24 KDM
P91<0048
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1
8260D
11/2/19 10:24 KDM
P9K0048
trans- 1,4-Dichloro-2-butene
<0.22
ug/L
100
10
0.22
1
8260D
11/2/19 10:24 KDM
P91<0048
Trichloroethylene
<0.46
ug/L
1
0.50
0.46
1
8260D
11/2/19 10:24 KDM
P9K0048
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1
8260D
11/2/19 10:24 KDM
P91<0048
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1
8260D
11/2/19 10:24 KDM
P9K0048
Vinyl chloride
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19 10:24 KDM
P91<0048
Xylenes, total
<1.1
ug/L
5
1.5
1.1
1
8260D
11/2/19 10:24 KDM
P9K0048
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
99 %
80-124
Dibromofluoromethane
99 %
75-129
Toluene-d8
99 %
77-123
Volatile Organic Compounds by GC/MS SIM
1,4-Dioxane
<0.14
ug/L
10
2.0
0.14
1
8260D SIM
10/25/19 15:25TBL
P9J0421
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 70

�Full-Service Analytical s
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
11 /14/2019
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No.: 50-02
Sample Matrix: Water
Client Sample ID: TB-02
Prism Sample ID: 9100380-05
Prism Work Order: 9100380
Time Collected: 10/23/19 00:00
Time Submitted: 10/24/19 09:10
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GUMS
1, 1, 1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19
3:26
KDM
P91<0048
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
3:26
KDM
P9K0048
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
11/2/19
3:26
KDM
P91<0048
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
11/2/19
3:26
KDM
P9K0048
1,1-Dichloroethane
<0.29
ug/L
5
0.50
0.29
1
8260D
11/2/19
3:26
KDM
P91<0048
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19
3:26
KDM
P9K0048
1, 1 -Dichloropropylene
<0.37
ug/L
5
0.50
0.37
1
8260D
11/2/19
3:26
KDM
P91<0048
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
11/2/19
3:26
KDM
P9K0048
1,2,4-Trichlorobenzene
<0.44
ug/L
10
1.0
0.44
1
8260D
11/2/19
3:26
KDM
P91<0048
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
11/2/19
3:26
KDM
P9K0048
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
11/2/19
3:26
KDM
P91<0048
1,2-Dichlorobenzene
<0.28
ug/L
5
0.50
0.28
1
8260D
11/2/19
3:26
KDM
P9K0048
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19
3:26
KDM
P91<0048
1,2-Dichloropropane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
3:26
KDM
P9K0048
1,3-Dichlorobenzene
<0.40
ug/L
5
0.50
0.40
1
8260D
11/2/19
3:26
KDM
P91<0048
1,3-Dichloropropane
<0.40
ug/L
1
0.50
0.40
1
8260D
11/2/19
3:26
KDM
P9K0048
1,4-Dichlorobenzene
<0.42
ug/L
1
0.50
0.42
1
8260D
11/2/19
3:26
KDM
P91<0048
2,2-Dichloropropane
<0.26
ug/L
15
2.0
0.26
1
8260D
11/2/19
3:26
KDM
P9K0048
Acetone
2.7 1
ug/L
100
5.0
0.70
1
8260D
11/2/19
3:26
KDM
P9K0048
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
11/2/19
3:26
KDM
P9K0048
Acrolein
<1.2
ug/L
53
20
1.2
1
8260D
11/2/19
3:26
KDM
P91<0048
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
11/2/19
3:26
KDM
P9K0048
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
11/2/19
3:26
KDM
P91<0048
Benzene
<0.34
ug/L
1
0.50
0.34
1
8260D
11/2/19
3:26
KDM
P9K0048
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
11/2/19
3:26
KDM
P91<0048
Bromodichloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
3:26
KDM
P9K0048
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
11/2/19
3:26
KDM
P91<0048
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
11/2/19
3:26
KDM
P9K0048
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
11/2/19
3:26
KDM
P91<0048
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
11/2/19
3:26
KDM
P9K0048
Chlorobenzene
<0.34
ug/L
3
0.50
0.34
1
8260D
11/2/19
3:26
KDM
P91<0048
Chloroethane
<0.43
ug/L
10
0.50
0.43
1
8260D
11/2/19
3:26
KDM
P9K0048
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
11/2/19
3:26
KDM
P91<0048
Chloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
3:26
KDM
P9K0048
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
11/2/19
3:26
KDM
P91<0048
cis- 1,2-Dichloroethylene
<0.40
ug/L
2
0.50
0.40
1
8260D
11/2/19
3:26
KDM
P9K0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 17 of 70

Laboratory Report
Full -Service Analytical &
P R S M
Environmental Solutions
LABORATORIES INC.
11/14/2019
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2019
Fall
Client
Sample ID:
TB-02
Attn: Alec Macbeth
Samplling
Prism
Sample ID:
9100380-05
231 Haywood Street
Project No.:
50-02
Prism
Work Order:
9100380
Asheville, NC 28801
Sample Matrix:
Water
Time
Collected: 10/23/19 00:00
Time
Submitted: 10/24/19
09:10
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
11/2/19
3:26
KDM
P91<0048
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
11/2/19
3:26
KDM
P9K0048
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
11/2/19
3:26
KDM
P91<0048
Dichlorodifluoromethane
<0.47
ug/L
5
5.0
0.47
1
8260D
11/2/19
3:26
KDM
P9K0048
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
11/2/19
3:26
KDM
P91<0048
Ethylbenzene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
3:26
KDM
P9K0048
Hexachlorobutadiene
<0.24
ug/L
10
2.0
0.24
1
8260D
11/2/19
3:26
KDM
P91<0048
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
11/2/19
3:26
KDM
P9K0048
m,p-Xylenes
<0.73
ug/L
NE
1.0
0.73
1
8260D
11/2/19
3:26
KDM
P91<0048
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
11/2/19
3:26
KDM
P9K0048
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
11/2/19
3:26
KDM
P91<0048
Methyl Ethyl Ketone (2-Butanone)
<0,78
ug/L
100
5.0
0.78
1
8260D
11/2/19
3:26
KDM
P9K0048
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
11/2/19
3:26
KDM
P91<0048
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
11/2/19
3:26
KDM
P9K0048
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
11/2/19
3:26
KDM
P91<0048
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1
8260D
11/2/19
3:26
KDM
P9K0048
Naphthalene
<0.45
ug/L
10
1.0
0.45
1
8260D
11/2/19
3:26
KDM
P91<0048
o-Xylene
<0.40
ug/L
NE
0.50
0.40
1
8260D
11/2/19
3:26
KDM
P9K0048
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
11/2/19
3:26
KDM
P91<0048
Styrene
<0.26
ug/L
1
0.50
0.26
1
8260D
11/2/19
3:26
KDM
P9K0048
Tetrachloroethylene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
3:26
KDM
P91<0048
Tetrahydrofuran
<0.68
ug/L
NE
10
0.68
1
8260D
11/2/19
3:26
KDM
P9K0048
Toluene
<0.35
ug/L
1
0.50
0.35
1
8260D
11/2/19
3:26
KDM
P91<0048
trans- 1,2-Dichloroethylene
<0.27
ug/L
5
0.50
0.27
1
8260D
11/2/19
3:26
KDM
P9K0048
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1
8260D
11/2/19
3:26
KDM
P91<0048
trans- 1,4-Dich loro-2-butene
<0.22
ug/L
100
10
0.22
1
8260D
11/2/19
3:26
KDM
P9K0048
Trichloroethylene
<0.46
ug/L
1
0.50
0.46
1
8260D
11/2/19
3:26
KDM
P91<0048
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1
8260D
11/2/19
3:26
KDM
P9K0048
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1
8260D
11/2/19
3:26
KDM
P91<0048
Vinyl chloride
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19
3:26
KDM
P9K0048
Xylenes, total
<1.1
ug/L
5
1.5
1.1
1
8260D
11/2/19
3:26
KDM
P91<0048
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
101
%
80-124
Dibromofluoromethane
98 %
75-129
Toluene-d8
99 %
77-123
Volatile Organic Compounds by GUMS SIM
1,4-Dioxane
<0.14
ug/L
10
2.0
0.14
1
8260D SIM
10/25/19 13:19TBL
P9J0421
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 70

,ot P R I IS M Full -Service Analytical s
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
11/14/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall
Attn: Alec Macbeth Samplling
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Prism Work Order: 9100380
Time Submitted: 10/24/2019 9:10:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P91K0048 - 5030B
Blank (P9K0048-BLK1)
Prepared: 11/01/19 Analyzed: 11/02/19
1,1,1,2-Tetrachloroethane
BRL
0.50
ug/L
1,1,1-Trichloroethane
BRL
0.50
ug/L
1,1,2,2-Tetrachloroethane
BRL
0.50
ug/L
1,1,2-Trichloroethane
BRL
0.50
ug/L
1,1-Dichloroethane
BRL
0.50
ug/L
1,1-Dichloroethylene
BRL
0.50
ug/L
1,1-Dichloropropylene
BRL
0.50
ug/L
1,2,3-Trichloropropane
BRL
1.0
ug/L
1,2,4-Trichlorobenzene
BRL
1.0
ug/L
1,2-Dibromo-3-chloropropane
BRL
2.0
ug/L
1,2-Dibromoethane
BRL
0.50
ug/L
1,2-Dichlorobenzene
BRL
0.50
ug/L
1,2-Dichloroethane
BRL
0.50
ug/L
1,2-Dichloropropane
BRL
0.50
ug/L
1,3-Dichlorobenzene
BRL
0.50
ug/L
1,3-Dichloropropane
BRL
0.50
ug/L
1,4-Dichlorobenzene
BRL
0.50
ug/L
2,2-Dichloropropane
BRL
2.0
ug/L
Acetone
BRL
5.0
ug/L
Acetonitrile
BRL
10
ug/L
Acrolein
BRL
20
ug/L
Acrylonitrile
BRL
20
ug/L
Allyl Chloride (3-Chloropropylene)
BRL
10
ug/L
Benzene
BRL
0.50
ug/L
Bromochloromethane
BRL
2.0
ug/L
Bromodichloromethane
BRL
0.50
ug/L
Bromoform
BRL
1.0
ug/L
Bromomethane
BRL
1.0
ug/L
Carbon disulfide
BRL
5.0
ug/L
Carbon Tetrachloride
BRL
2.0
ug/L
Chlorobenzene
BRL
0.50
ug/L
Chloroethane
BRL
0.50
ug/L
Chloroform
BRL
0.50
ug/L
Chloromethane
BRL
0.50
ug/L
Chloroprene
BRL
10
ug/L
cis-1,2-Dichloroethylene
BRL
0.50
ug/L
cis-1,3-Dichloropropylene
BRL
0.50
ug/L
Dibromochloromethane
BRL
0.50
ug/L
Dibromomethane
BRL
2.0
ug/L
Dichlorodifluoromethane
BRL
5.0
ug/L
Ethyl Methacrylate
BRL
10
ug/L
Ethylbenzene
BRL
0.50
ug/L
Hexachlorobutadiene
BRL
2.0
ug/L
Isobutyl alcohol
BRL
50
ug/L
m,p-Xylenes
BRL
1.0
ug/L
Methacrylonitrile
BRL
10
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 19 of 70

P R I S M Full -Service Analytical s
Environmental Solutions
LABCFATCRIES, NC.
Level II QC Report
11/14/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Prism Work Order: 9100380
Attn: Alec Macbeth Samplling Time Submitted: 10/24/2019 9:10:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P911<0048 - 5030B
Blank (P9K0048-BLK1)
Prepared: 11/01/19 Analyzed: 11/02/19
Methyl Butyl Ketone (2-Hexanone)
BRL
5.0
ug/L
Methyl Ethyl Ketone (2-Butanone)
BRL
5.0
ug/L
Methyl Iodide
BRL
5.0
ug/L
Methyl Isobutyl Ketone
BRL
5.0
ug/L
Methyl Methacrylate
BRL
10
ug/L
Methylene Chloride
BRL
1.0
ug/L
Naphthalene
BRL
1.0
ug/L
o-Xylene
BRL
0.50
ug/L
Propionitrile (Ethyl Cyanide)
BRL
10
ug/L
Styrene
BRL
0.50
ug/L
Tetrachloroethylene
BRL
0.50
ug/L
Tetrahydrofuran
BRL
10
ug/L
Toluene
BRL
0.50
ug/L
trans- 1,2-Dichloroethylene
BRL
0.50
ug/L
trans- 1,3-Dichloropropylene
BRL
0.50
ug/L
trans-1,4-Dichloro-2-butene
BRL
10
ug/L
Trichloroethylene
BRL
0.50
ug/L
Trichlorofluoromethane
BRL
0.50
ug/L
Vinyl acetate
BRL
2.0
ug/L
Vinyl chloride
BRL
0.50
ug/L
Xylenes, total
BRL
1.5
ug/L
Surrogate:4-Bromofluorobenzene
49.4
ug/L
50.00
99
80-124
Surrogate: Dibromofluoromethane
49.0
ug/L
50.00
98
75-129
Surrogate: Toluene-d8
50.2
ug/L
50.00
100
77-123
LCS (P9KO048-BS1)
Prepared: 11/01/19 Analyzed:
11/02/19
1,1,1,2-Tetrachloroethane
20.6
0.50
ug/L
20.00
103
79-134
1,1,1-Trichloroethane
21.2
0.50
ug/L
20.00
106
75-136
1,1,2,2-Tetrachloroethane
21.0
0.50
ug/L
20.00
105
62-127
1,1,2-Trichloroethane
20.8
0.50
ug/L
20.00
104
70-140
1,1-Dichloroethane
20.6
0.50
ug/L
20.00
103
78-130
1,1-Dichloroethylene
21.2
0.50
ug/L
20.00
106
70-154
1, 1 -Dichloropropylene
22.6
0.50
ug/L
20.00
113
71-136
1,2,3-Trichloropropane
20.5
1.0
ug/L
20.00
102
71-127
1,2,4-Trichlorobenzene
21.3
1.0
ug/L
20.00
107
66-139
1,2-Dibromo-3-chloropropane
21.1
2.0
ug/L
20.00
106
63-134
1,2-Dibromoethane
21.2
0.50
ug/L
20.00
106
77-135
1,2-Dichlorobenzene
20.8
0.50
ug/L
20.00
104
78-128
1,2-Dichloroethane
19.6
0.50
ug/L
20.00
98
68-131
1,2-Dichloropropane
20.7
0.50
ug/L
20.00
103
77-130
1,3-Dichlorobenzene
20.3
0.50
ug/L
20.00
102
77-125
1,3-Dichloropropane
21.3
0.50
ug/L
20.00
106
76-132
1,4-Dichlorobenzene
20.3
0.50
ug/L
20.00
102
75-126
2,2-Dichloropropane
20.3
2.0
ug/L
20.00
102
29-149
Acetone
40.2
5.0
ug/L
40.00
101
40-166
Acetonitrile
21.3
10
ug/L
20.00
106
70-130
Acrolein
41.6
20
ug/L
40.00
104
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 of 70

P R I S M Full-ServiceAnalytical s
Environmental Solutions
LABCFATCRIES, NC.
Level II QC Report
11/14/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall
Attn: Alec Macbeth Samplling
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Prism Work Order: 9100380
Time Submitted: 10/24/2019 9:10:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P911<0048 - 5030B
LCS (P91<0048-13SI)
Prepared: 11/01/19 Analyzed: 11/02/19
Acrylonitrile
37.3
20
ug/L
40.00
93
81-127
Allyl Chloride (3-Chloropropylene)
18.8
10
ug/L
20.00
94
70-130
Benzene
20.3
0.50
ug/L
20.00
101
77-128
Bromochloromethane
20.8
2.0
ug/L
20.00
104
78-135
Bromodichloromethane
20.9
0.50
ug/L
20.00
104
76-138
Bromoform
21.9
1.0
ug/L
20.00
109
71-135
Bromomethane
28.7
1.0
ug/L
20.00
143
41-168
Carbon disulfide
22.2
5.0
ug/L
20.00
111
59-135
Carbon Tetrachloride
21.8
2.0
ug/L
20.00
109
72-142
Chlorobenzene
20.0
0.50
ug/L
20.00
100
78-119
Chloroethane
20.4
0.50
ug/L
20.00
102
57-142
Chloroform
20.1
0.50
ug/L
20.00
101
77-130
Chloromethane
23.9
0.50
ug/L
20.00
120
47-145
Chloroprene
21.0
10
ug/L
20.00
105
70-130
cis-1,2-Dichloroethylene
19.4
0.50
ug/L
20.00
97
76-141
cis-1,3-Dichloropropylene
22.2
0.50
ug/L
20.00
111
65-140
Dibromochloromethane
21.5
0.50
ug/L
20.00
107
75-134
Dibromomethane
20.7
2.0
ug/L
20.00
104
76-138
Dichlorodifluoromethane
26.4
5.0
ug/L
20.00
132
28-163
Ethyl Methacrylate
20.8
10
ug/L
20.00
104
70-130
Ethylbenzene
20.8
0.50
ug/L
20.00
104
80-127
Hexachlorobutadiene
21.9
2.0
ug/L
20.00
110
61-134
Isobutyl alcohol
20.0
50
ug/L
20.00
100
70-130 J
m,p-Xylenes
42.6
1.0
ug/L
40.00
107
77-133
Methacrylonitrile
20.0
10
ug/L
20.00
100
70-130
Methyl Butyl Ketone (2-Hexanone)
21.5
5.0
ug/L
20.00
108
64-137
Methyl Ethyl Ketone (2-Butanone)
19.8
5.0
ug/L
20.00
99
71-134
Methyl Iodide
21.2
5.0
ug/L
20.00
106
70-130
Methyl Isobutyl Ketone
20.7
5.0
ug/L
20.00
104
69-134
Methyl Methacrylate
20.9
10
ug/L
20.00
104
70-130
Methylene Chloride
18.7
1.0
ug/L
20.00
93
73-131
Naphthalene
21.8
1.0
ug/L
20.00
109
64-136
o-Xylene
20.9
0.50
ug/L
20.00
105
78-128
Propionitrile (Ethyl Cyanide)
20.3
10
ug/L
20.00
101
70-130
Styrene
22.0
0.50
ug/L
20.00
110
78-129
Tetrachloroethylene
21.9
0.50
ug/L
20.00
110
80-129
Tetrahydrofuran
19.4
10
ug/L
20.00
97
70-130
Toluene
20.6
0.50
ug/L
20.00
103
76-131
trans- 1,2-Dichloroethylene
20.0
0.50
ug/L
20.00
100
76-135
trans- 1,3-Dichloropropylene
21.8
0.50
ug/L
20.00
109
67-140
trans-1,4-Dichloro-2-butene
20.0
10
ug/L
20.00
100
70-130
Trichloroethylene
20.4
0.50
ug/L
20.00
102
77-133
Trichlorofluoromethane
23.6
0.50
ug/L
20.00
118
62-148
Vinyl acetate
21.4
2.0
ug/L
20.00
107
34-167
Vinyl chloride
22.6
0.50
ug/L
20.00
113
57-141
Xylenes, total
63.6
1.5
ug/L
60.00
106
77-133
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 21 of 70

P R I S M Full -Service Analytical s
Environmental Solutions
LABCFATCRIES, NC.
Level II QC Report
11/14/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Prism Work Order: 9100380
Attn: Alec Macbeth Samplling Time Submitted: 10/24/2019 9:10:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P91<0048 - 5030B
LCS (P9K0048-BSI)
Prepared: 11/01/19 Analyzed: 11/02/19
Surrogate:4-Bromofluorobenzene
50.1
ug/L
50.00
100
80-124
Surrogate: Dibromofluoromethane
49.0
ug/L
50.00
98
75-129
Surrogate: Toluene-d8
50.6
ug/L
50.00
101
77-123
LCS Dup (P9KO048-BSD1)
Prepared: 11/01/19 Analyzed:
11/02/19
1,1,1,2-Tetrachloroethane
20.4
0.50
ug/L
20.00
102
79-134
1
20
1,1,1-Trichloroethane
20.7
0.50
ug/L
20.00
103
75-136
3
20
1,1,2,2-Tetrachloroethane
21.4
0.50
ug/L
20.00
107
62-127
2
20
1,1,2-Trichloroethane
20.6
0.50
ug/L
20.00
103
70-140
0.9
20
1,1-Dichloroethane
20.2
0.50
ug/L
20.00
101
78-130
2
20
1,1-Dichloroethylene
20.6
0.50
ug/L
20.00
103
70-154
3
20
1, 1 -Dichloropropylene
21.7
0.50
ug/L
20.00
108
71-136
4
20
1,2,3-Trichloropropane
21.4
1.0
ug/L
20.00
107
71-127
4
20
1,2,4-Trichlorobenzene
21.0
1.0
ug/L
20.00
105
66-139
2
20
1,2-Dibromo-3-chloropropane
22.4
2.0
ug/L
20.00
112
63-134
6
20
1,2-Dibromoethane
21.3
0.50
ug/L
20.00
107
77-135
0.6
20
1,2-Dichlorobenzene
20.8
0.50
ug/L
20.00
104
78-128
0.05
20
1,2-Dichloroethane
19.2
0.50
ug/L
20.00
96
68-131
2
20
1,2-Dichloropropane
20.4
0.50
ug/L
20.00
102
77-130
1
20
1,3-Dichlorobenzene
20.0
0.50
ug/L
20.00
100
77-125
1
20
1,3-Dichloropropane
21.2
0.50
ug/L
20.00
106
76-132
0.4
20
1,4-Dichlorobenzene
20.0
0.50
ug/L
20.00
100
75-126
2
20
2,2-Dichloropropane
19.6
2.0
ug/L
20.00
98
29-149
4
20
Acetone
42.3
5.0
ug/L
40.00
106
40-166
5
20
Acetonitrile
21.5
10
ug/L
20.00
107
70-130
1
20
Acrolein
43.1
20
ug/L
40.00
108
70-130
4
20
Acrylonitrile
39.4
20
ug/L
40.00
98
81-127
5
20
Allyl Chloride (3-Chloropropylene)
18.5
10
ug/L
20.00
93
70-130
2
20
Benzene
19.9
0.50
ug/L
20.00
100
77-128
2
20
Bromochloromethane
20.6
2.0
ug/L
20.00
103
78-135
1
20
Bromodichloromethane
20.7
0.50
ug/L
20.00
103
76-138
1
20
Bromoform
22.4
1.0
ug/L
20.00
112
71-135
2
20
Bromomethane
26.6
1.0
ug/L
20.00
133
41-168
8
20
Carbon disulfide
21.4
5.0
ug/L
20.00
107
59-135
4
20
Carbon Tetrachloride
21.1
2.0
ug/L
20.00
105
72-142
4
20
Chlorobenzene
19.6
0.50
ug/L
20.00
98
78-119
2
20
Chloroethane
19.7
0.50
ug/L
20.00
99
57-142
3
20
Chloroform
20.0
0.50
ug/L
20.00
100
77-130
0.7
20
Chloromethane
25.1
0.50
ug/L
20.00
125
47-145
5
20
Chloroprene
20.3
10
ug/L
20.00
102
70-130
3
20
cis-1,2-Dichloroethylene
19.0
0.50
ug/L
20.00
95
76-141
2
20
cis-1,3-Dichloropropylene
21.8
0.50
ug/L
20.00
109
65-140
2
20
Dibromochloromethane
21.3
0.50
ug/L
20.00
107
75-134
0.7
20
Dibromomethane
20.7
2.0
ug/L
20.00
103
76-138
0.1
20
Dichlorodifluoromethane
24.6
5.0
ug/L
20.00
123
28-163
7
20
Ethyl Methacrylate
21.1
10
ug/L
20.00
105
70-130
1
20
Ethylbenzene
20.4
0.50
ug/L
20.00
102
80-127
2
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 of 70

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/14/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Prism Work Order: 9100380
Attn: Alec Macbeth Samplling Time Submitted: 10/24/2019 9:10:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9KO048 - 5030B
LCS Dup (P9K0048-BSD1)
Prepared: 11/01/19 Analyzed: 11/02/19
Hexachlorobutadiene
20.8
2.0
ug/L
20.00
104
61-134
5
20
Isobutyl alcohol
20.7
50
ug/L
20.00
103
70-130
4
20 1
m,p-Xylenes
41.8
1.0
ug/L
40.00
104
77-133
2
20
Methacrylonitrile
20.7
10
ug/L
20.00
104
70-130
3
20
Methyl Butyl Ketone (2-Hexanone)
22.6
5.0
ug/L
20.00
113
64-137
5
20
Methyl Ethyl Ketone (2-Butanone)
21.0
5.0
ug/L
20.00
105
71-134
5
20
Methyl Iodide
20.2
5.0
ug/L
20.00
101
70-130
5
20
Methyl Isobutyl Ketone
21.6
5.0
ug/L
20.00
108
69-134
4
20
Methyl Methacrylate
21.4
10
ug/L
20.00
107
70-130
2
20
Methylene Chloride
18.6
1.0
ug/L
20.00
93
73-131
0.2
20
Naphthalene
22.3
1.0
ug/L
20.00
ill
64-136
2
20
o-Xylene
20.4
0.50
ug/L
20.00
102
78-128
2
20
Propionitrile (Ethyl Cyanide)
21.0
10
ug/L
20.00
105
70-130
3
20
Styrene
21.5
0.50
ug/L
20.00
108
78-129
2
20
Tetrachloroethylene
21.1
0.50
ug/L
20.00
106
80-129
4
20
Tetrahydrofuran
20.9
10
ug/L
20.00
104
70-130
7
20
Toluene
20.1
0.50
ug/L
20.00
101
76-131
2
20
trans-1,2-Dichloroethylene
19.5
0.50
ug/L
20.00
98
76-135
3
20
trans-1,3-Dichloropropylene
21.8
0.50
ug/L
20.00
109
67-140
0.05
20
trans-1,4-Dichloro-2-butene
20.6
10
ug/L
20.00
103
70-130
3
20
Trichloroethylene
19.6
0.50
ug/L
20.00
98
77-133
4
20
Trichlorofluoromethane
22.8
0.50
ug/L
20.00
114
62-148
3
20
Vinyl acetate
21.8
2.0
ug/L
20.00
109
34-167
2
20
Vinyl chloride
21.7
0.50
ug/L
20.00
109
57-141
4
20
Xylenes, total
62.2
1.5
ug/L
60.00
104
77-133
2
20
Surrogate:4-Bromofluorobenzene
49.9
ug/L
50.00
100
80-124
Surrogate: Dibromofluoromethane
49.9
ug/L
50.00
100
75-129
Surrogate: Toluene-d8
50.5
ug/L
50.00
101
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 70

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/14/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall
Attn: Alec Macbeth Samplling
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS SIM - Quality Control
Prism Work Order: 9100380
Time Submitted: 10/24/2019 9:10:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9JO421 - 5030B
Blank (P9J0421-BLK1)
Prepared & Analyzed: 10/25/19
1,4-Dioxane
BRL 2.0 ug/L
LCS (P9J0421-BS1)
Prepared &Analyzed: 10/25/19
1,4-Dioxane
43.0 2.0 ug/L
50.00 86
55-145
LCS Dup (P9J0421-BSD1)
Prepared &Analyzed: 10/25/19
1,4-Dioxane
43.9 2.0 ug/L
50.00 88
55-145 2 30
Matrix Spike (P9J0421-MS1)
Source: 9100380-05
Prepared & Analyzed: 10/25/19
1,4-Dioxane
46.2 2.0 ug/L
50.00 BRL 92
55-145
Matrix Spike Dup (P9J0421-MSD1)
Source: 9100380-05
Prepared & Analyzed: 10/25/19
1,4-Dioxane
47.6 2.0 ug/L
50.00 BRL 95
55-145 3 30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 of 70

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/14/19
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Total Metals - Quality Control
Analyte
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No: 50-02
Prism Work Order: 9100380
Time Submitted: 10/24/2019 9:10:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9JO440 - 3005A
Blank (P9J0440-BLK1)
Prepared: 10/25/19 Analyzed: 10/28/19
Antimony
BRL
3.0
ug/L
Arsenic
BRL
1.0
ug/L
Barium
BRL
10
ug/L
Beryllium
BRL
1.0
ug/L
Cadmium
BRL
1.0
ug/L
Chromium
BRL
3.0
ug/L
Cobalt
BRL
2.0
ug/L
Copper
BRL
10
ug/L
Lead
BRL
1.0
ug/L
Nickel
BRL
3.0
ug/L
Selenium
BRL
5.0
ug/L
Silver
BRL
1.0
ug/L
Thallium
BRL
2.0
ug/L
Tin
BRL
5.0
ug/L
Vanadium
BRL
5.0
ug/L
Zinc
BRL
20
ug/L
LCS (P9J0440-BS1)
Prepared: 10/25/19 Analyzed: 10/28/19
Antimony
102
3.0
ug/L
100.0
102
80-120
Arsenic
100
1.0
ug/L
100.0
100
80-120
Barium
106
10
ug/L
100.0
106
80-120
Beryllium
101
1.0
ug/L
100.0
101
80-120
Cadmium
101
1.0
ug/L
100.0
101
80-120
Chromium
100
3.0
ug/L
100.0
100
80-120
Cobalt
105
2.0
ug/L
100.0
105
80-120
Copper
104
10
ug/L
100.0
104
80-120
Lead
101
1.0
ug/L
100.0
101
80-120
Nickel
105
3.0
ug/L
100.0
105
80-120
Selenium
104
5.0
ug/L
100.0
104
80-120
Silver
100
1.0
ug/L
100.0
100
80-120
Thallium
101
2.0
ug/L
100.0
101
80-120
Tin
101
5.0
ug/L
100.0
101
80-120
Vanadium
99.9
5.0
ug/L
100.0
100
80-120
Zinc
105
20
ug/L
100.0
105
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 of 70

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/14/19
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Total Metals - Quality Control
Analyte
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No: 50-02
Prism Work Order: 9100380
Time Submitted: 10/24/2019 9:10:OOAM
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9JO493 - 7470A
Blank (P9J0493-BLK1) Prepared & Analyzed: 10/29/19
Mercury BRL 0.20 ug/L
LCS (P9J0493-BS1) Prepared &Analyzed: 10/29/19
Mercury 10.0 0.20 ug/L 9.375 107 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 26 of 70

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/14/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall
Attn: Alec Macbeth Samplling
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Anions by Ion Chromatography - Quality Control
Prism Work Order: 9100380
Time Submitted: 10/24/2019 9:10:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9JO437 - NO PREP
Blank (P9J0437-BLK1)
Prepared & Analyzed: 10/24/19
Chloride
BRL
1000
ug/L
Nitrate as N
BRL
200
ug/L
Sulfate
BRL
2000
ug/L
LCS (P9J0437-BS1)
Prepared &Analyzed: 10/24/19
Chloride
41900
1000
ug/L
40000 105 80-120
Nitrate as N
4040
210
ug/L
4000 101 80-120
Sulfate
42400
2100
ug/L
40000 106 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 27 of 70

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/14/19
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
General Chemistry Parameters - Quality Control
Analyte
Batch P9J0473 - NO PREP
Project: Jackson Cty Landfill 2019 Fall Prism Work Order: 9100380
Samplling Time Submitted: 10/24/2019 9:10:OOAM
Project No: 50-02
Reporting Spike Source %REC RPD
Result Limit Units Level Result %REC Limits RPD Limit Notes
Blank (P9J0473-BLK1)
Prepared & Analyzed: 10/24/19
Ferrous Iron
BRL 200 ug/L
LCS (P9J0473-BS1)
Prepared &Analyzed: 10/24/19
Ferrous Iron
2020 200 ug/L
2000 101 90-110
Matrix Spike (P9J0473-MS1)
Source: 9100380-04
Prepared & Analyzed: 10/24/19
Ferrous Iron
2050 200 ug/L
2000 BRL 103 80-120
Matrix Spike Dup (P9J0473-MSD1)
Source: 9100380-04
Prepared & Analyzed: 10/24/19
Ferrous Iron
2000 200 ug/L
2000 BRL 100 80-120 3 20
Batch P9J0483 - NO PREP
Blank (P9J0483-BLK1) Prepared & Analyzed: 10/24/19
Biochemical Oxygen Demand 500 2000 ug/L BB, J
LCS (P9J0483-BS1) Prepared &Analyzed: 10/24/19
Biochemical Oxygen Demand 210000 2000 ug/L 198000 108 84.6-115.4 BB, B
Batch P9J0486 - NO PREP
Blank (P9JO486-BLK1) Prepared & Analyzed: 10/28/19
Chemical Oxygen Demand BRL 50000 ug/L
LCS (P9J0486-BS1) Prepared &Analyzed: 10/28/19
Chemical Oxygen Demand 519000 50000 ug/L 500000 104 90-110
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 of 70

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/14/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall
Attn: Alec Macbeth Samplling
231 Haywood Street Project No: 50-02
Asheville, NC 28801
General Chemistry Parameters - Quality Control
Prism Work Order: 9100380
Time Submitted: 10/24/2019 9:10:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9JO504 - SM4500-S C
Blank (P9J0504-BLK1) Prepared & Analyzed: 10/29/19
Sulfide BRL 2000 ug/L
LCS (P9J0504-BS1) Prepared &Analyzed: 10/29/19
Sulfide 9700 2000 ug/L 10000 97 70-130
Batch P9JO537 - NO PREP
Blank (P9J0537-BLK1) Prepared &Analyzed: 10/31/19
Total Alkalinity to pH 4.5 BRL 5000 ug/L
LCS (P9J0537-BSI) Prepared &Analyzed: 10/31/19
Total Alkalinity to pH 4.5 250000 5000 ug/L 250000 100 90-110
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 29 of 70

Sample Extraction Data
Prep Method: SM4500-S C
Lab Number
Batch
Initial
Final
Date/Time
9100380-01
P9J0504
200
mL
200 mL
10/29/19
9:45
9100380-02
P9J0504
200
mL
200 mL
10/29/19
9:45
9100380-03
P9J0504
200
mL
200 mL
10/29/19
9:45
9100380-04
P9J0504
200
mL
200 mL
10/29/19
9:45
Prep Method: 3005A
Lab Number
Batch
Initial
Final
Date/Time
9100380-01
P9J0440
50
mL
50 mL
10/25/19
8:44
9100380-02
P9J0440
50
mL
50 mL
10/25/19
8:44
9100380-03
P9J0440
50
mL
50 mL
10/25/19
8:44
9100380-04
P9J0440
50
mL
50 mL
10/25/19
8:44
Prep Method: 7470A
Lab Number
Batch
Initial
Final
Date/Time
9100380-01
P9J0493
20
mL
30 mL
10/29/19
9:18
9100380-02
P9J0493
20
mL
30 mL
10/29/19
9:18
9100380-03
P9J0493
20
mL
30 mL
10/29/19
9:18
9100380-04
P9J0493
20
mL
30 mL
10/29/19
9:18
Prep Method: 5030E
Lab Number
Batch
Initial
Final
Date/Time
9100380-01
P91<0048
10
mL
10 mL
11/01/19
8:01
9100380-02
P91<0048
10
mL
10 mL
11/01/19
8:01
9100380-03
P91<0048
10
mL
10 mL
11/01/19
8:01
9100380-04
P91<0048
10
mL
10 mL
11/01/19
8:01
9100380-05
P91<0048
10
mL
10 mL
11/01/19
8:01
Prep Method: 5030B
Lab Number
Batch
Initial
Final
Date/Time
9100380-01
P9J0421
5
mL
5 mL
10/25/19
9:00
9100380-02
P9J0421
5
mL
5 mL
10/25/19
9:00
9100380-03
P9J0421
5
mL
5 mL
10/25/19
9:00
9100380-04
P9J0421
5
mL
5 mL
10/25/19
9:00
9100380-05
P9J0421
5
mL
5 mL
10/25/19
9:00
Subcontracted Analyses
The following analyses
were subcontracted
to Analytical
Environmental Services,
Inc.
Lab Number
Analysis
9100380-01
8270 (App. II)
9100380-02
8270 (App. II)
9100380-03
8270 (App. II)
9100380-04
8270 (App. II)
The following analyses
were subcontracted
to Pace Analytical Gulf Coast
Lab Number
Analysis
9100380-01
TOC (Sub)
9100380-02
TOC (Sub)
9100380-03
TOC (Sub)
9100380-04
TOC (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 of 70

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Page
31Wof

ACCESS
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte NC 282240543
ATTENTION
Robbi A. Jones
PROJECTID
9100380
LABORATORY REPORT NUMBER
191OS56
DATE
November 04, 2019
Primate Data Review By Secondary Data Review By
Chris Pafford
Project Manager, AES
PLEASE NOTE:
Ashley Amick
Project Manager, Access Analytical
aamickp,axs-inc.com
Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),
3080 Presidential Drive, Atlanta, GA 30340.
AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582,
NELAP certified laboratory # E87582
AIHA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, PCNI Asbestos,
Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal)
Direct Examination.
Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a
representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll tee at 883.315.4243
Page I Page 32 of 70

S�� �S :%io,, / r2S--�
i5 j� �PI n n IEnvir inenMce Analytical 8
v Envirtxitnental SolutionsV1
PRISM
i uaaN,l Liltia47G tf ,
SUBCONTRACT ORDER �~
Ccrtiftcation: 1-AC` USACE
Prism Laboratories, Inc. NC I ' SC_ Other
9] 00380 NVA�
SENDING LAB RLCCIV] NG LABO-WORYf, -
Prism Laboratories, Inc. Analytical Fnvironmental Services, Inc.
P. O. Box 240543 3080 Presidential Parkway W
Charlotte, NC 28224-0543 Atlanta, GA 30340
Phone: [phone] Phone :[phone] ��
Fax:[phone] Fax: NA
Project Manager Robbi A. Jones
V
Analysis Due Expires n Laboratory ID Comments
Sample ID: 91110380-01 Water Sampled: l(IJI;.;}1909;i 6
8270 (App. 11) I013i1l19 flly:3(r� 8270App Il List
Cmlrniurrc S�rlrp7irJ- _
Samptle ID: 9100380-02 Water st..)6lcd:l0l23lI9IU:26�
8270 (App.11) 10/30/19 10:26 8270 App I] List
Canainecc Supplied: .
Sample ID: 9100380-03 Water Sampled: 10123/19 14:32.
8270 (App. II) 10/31V 1.9 14:32 8270 Anp TI List
C'nnrainrer Supplied:
Sample ID: 9100380-04 Water Sampled: 10/23/19 12:54 r h w _ a b
3270 (App, lT) tl/ w.19 12:54 327DApp if List
Cnnfa mm, .Suppl irrl:
Rci�,,..cd I iJ,�
Date
R moist P.
U�
�
Da:c
IdAll
Released 13"
Date
I e Vlv'j i'
1 &• S
Dptc
Released By
Dalc
Itrcci%•ed By
Date
ilckaacd BY
Do.
Received Elx
Dale
Page 1 of 1
Page I Page 33 of 70

Analytical Environmental Services, Inc
Date: 4-Nov-19
Client:
Prism Laboratories
Client Sample 1D:
MW-02
Lab Order
1910S56
Tag Number:
9100380-01
Project Name:
9100380
Collection Date:
10/23/2019 9:26:00 AM
Lab ID:
1910S56-OOIA
Matrix:
Aqueous
Analyses Result Qua]
MDL
ReportingUnits
Limit
BatchID DF
Date Analyzed Analyst
APPENDIXII-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
1,2,4,5-Tetrachlorobenzene
BRL
1.3
10
ug/L
287151 1
11/01/2019 13:39
YH
1,2,4-Triclilorobenzene
BRL
1.4
10
ug/L
287151 1
11/01/2019 13:39
YH
1.2-Dichlorobenzene
BRL
1.2
10
ug/L
287151 1
11/01/2019 13:39
YH
].3-Dichlorobenzene
BRL
1.3
10
ug/L
287151 1
11/01/2019 13:39
YH
1.3-Dinitrobenzene
BRL
1.1
20
ug/L
287151 1
11/01/2019 13:39
YH
1.4-Dichlorobenzene
BRL
1.4
10
ug/L
287151 1
11/01/2019 13:39
YH
1,4-Napthoquinone
BRL
1.7
10
ug/L
287151 1
11/01/2019 13:39
YH
1-Naphthylamine
BRL
3.0
10
ug/L
287151 1
11/01/2019 13:39
YH
2,3,4,6-Tetrachlorophenol
BRL
1.1
10
ug/L
287151 1
11/01/2019 13:39
YH
2,4,5-Trichlorophenol
BRL
0.99
10
ug/L
287151 1
11/01/2019 13:39
YH
2,4,6-Trichlorophenol
BRL
13
10
ug/L
287151 1
11/01/2019 13:39
YH
2,4-Dichlorophenol
BRL
1.0
10
ug/L
287151 1
11/01/2019 13:39
YH
2,4-Dimethylphenol
BRL
0.72
50
ug/L
287151 1
11/01/2019 13:39
YH
2.4-Dinitrophenol
BRL
5.5
50
ug/L
287151 1
11/01/2019 13:39
YH
2.4-Dinitrotoluene
BRL
1.1
10
ug/L
287151 1
11/01/2019 13:39
YH
2,6-Dielilorophenol
BRL
0.95
10
ug/L
287151 1
11/01/2019 13:39
YH
2,6-Dinitrotoluene
BRL
1.3
10
ug/L
287151 1
11/01/2019 13:39
YH
2-Acetylaminofluorene
BRL
1.1
20
ug/L
287151 1
11/01/2019 13:39
YH
2-Chloronaphthalene
BRL
1.8
10
ug/L
287151 1
11/01/2019 13:39
YH
2-Chlorophenol
BRL
1.2
10
ug/L
287151 1
11/01/2019 13:39
YH
2-Methylnaphthalene
BRL
1.2
10
ug/L
287151 1
11/01/2019 13:39
YH
2-Methylphenol
BRL
1.3
10
ug/L
287151 1
11/01/2019 13:39
YH
2-Naphthylamine
BRL
1.7
10
ug/L
287151 1
11/01/2019 13:39
YH
2-Nitroaniline
BRL
1-9
50
ug/L
287151 1
11/01/2019 13:39
YH
2-Nitrophenol
BRL
1.6
10
ug/L
287151 1
11/01/2019 13:39
YH
3.3'-Dichlorobenzidine
BRL
1.1
20
ug/L
287151 1
11/01/2019 13:39
YH
3,3'-Dimethylbenzidine
BRL
5.4
20
ug/L
287151 1
11/01/2019 13:39
YH
3,4-Methylphenol
BRL
2.3
10
ug/L
287151 1
11/01/2019 13:39
YH
3-Methyl cholanthrene
BRL
11
10
ug/L
287151 1
11/01/2019 13:39
YH
3-Nitroaniline
BRL
1.2
50
ue/L
287151 1
11/01/2019 13:39
YH
4.6-Dinitro-2-methylphenol
BRL
1.3
50
ug/L
287151 1
11/01/2019 13:39
YH
4-Aminobiphenyl
BRL
2.4
20
ug/L
287151 1
11/01/2019 13:39
YH
4-Bromophenyl phenyl ether
BRL
1.4
10
ug/L
287151 1
11/01/2019 13:39
YH
4-Chloro-3-methylphenol
BRL
0.81
20
ug/L
287151 1
11/01/2019 13:39
YH
4-Chloroaniline
BRL
21
20
ug/L
287151 1
11/01/2019 13:39
YH
4-Chlorophenyl phenyl ether
BRL
1 3
10
ug/L
287151 1
11/01/2019 13:39
YH
4-Nitroaniline
BRL
13
20
ug/L
287151 1
11/01/2019 13:39
YH
4-Nitrophenol
BRL
0.77
50
ug/L
287151 1
11/01/2019 13:39
YH
QuW1111 a•s: ' Value exceeds rttaxunum comaminant level
E- Estimated
%aloe abo%e
quantnation range
BRL Nat Detected at NlDL
S Spike Reco%en• outside limns due to matrix
li Holding times for preparation or analysis exceeded
- Greater than Result %aluc
N Anal..te not NELAC ceniGed
J Estimated
%slue detected
below Reporting Lunit
B Analeie defected m the associated method blank
< Less than
Result %alue
Page J Page 34 of 70

Analytical Environmental Services, Inc
Date: 4-Nov-19
Client:
Prism Laboratories
Client Sample ID:
MW-02
Lab Order
191 OS56
Tag Number:
9100380-01
Project Name:
9100380
Collection Date:
10/23/2019 9:26:00 AM
Lab ID:
191OS56-OOIA
Matrix:
Aqueous
Analyses Result Qual
MDL
ReportingUnits
Limit
BatchID DF
Date Analyzed
Analyst
APPENDIXII-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
5-Nitro-o-toluidine
BRL
0.66
10
ug/L
287151 1
11/01/2019 13:39
YH
7,12-Dimethylbenz(a)anthracene
BRL
1.4
10
ug/L
287151 1
11/01/2019 13:39
YH
Acenaphthene
BRL
1.1
10
ug/L
287151 1
11/01/2019 13:39
YH
Accnaphthylene
BRL
1.1
10
ug/L
287151 1
11/01/2019 13:39
YH
Acetophenone
BRL
2.1
10
ug/L
287151 1
11/01/2019 13:39
YH
Anthracene
BRL
0.82
10
ug/L
287151 1
11/01/2019 13:39
YH
Benz(a)anthracene
BRL
0.96
10
ug/L
287151 1
11/01/2019 13:39
YH
Benzo(a)pyrene
BRL
O.96
10
ug/L
287151 1
11/01/2019 13:39
YH
Benzo(b)fluoranthene
BRL
1.5
10
ug/L
287151 1
11/01/2019 13:39
YH
Benzo(g,h;i)perylene
BRL
13
10
ug/L
287151 1
11/01/2019 13:39
YH
Benzo(k)fluoranthene
BRL
1.5
10
ug/L
287151 1
11/01/2019 13:39
YH
Benzyl alcohol
BRL
14
20
ug/L
287151 1
11/01/2019 13:39
YH
Bis(2-chloroethoxy)methane
BRL
1.1
10
ug/L
287151 1
11/01/2019 13:39
YH
Bis(2-chloroethyl)ether
BRL
12
10
ug/L
287151 1
11/01/2019 13:39
YH
Bis(2-chloroisopropyl)ether
BRL
15
10
ug/L
287151 1
11/01/2019 13:39
YH
Bis(2-ethylhexyl)phthalate
BRL
14
20
ug/L
287151 1
11/01/2019 13:39
YH
Butyl benzyl phthalate
BRL
0.84
10
ug/L
287151 1
11/01/2019 13:39
YH
Chlorobenzilate
BRL
0.57
10
ug/L
287151 1
11/01/2019 13:39
YH
Chrysene
BRL
0.93
10
ug/L
287151 1
11/01/2019 13:39
YH
Di-n-butyl phthalate
BRL
11
10
ug/L
287151 1
11/01/2019 13:39
YH
Di-n-octyl phthalate
BRL
16
10
ug/L
287151 1
11/01/2019 13:39
YH
Diallate
BRL
0.84
10
ug/L
287151 1
11/01/2019 13:39
YH
Dibenz(a,h)anthracene
BRL
14
10
ug/L
287151 1
11/01/2019 13:39
YH
Dibenzoturan
BRL
11
10
ug/L
287151 1
11/01/2019 13:39
YH
Diethyl phthalate
BRL
0.82
10
itg/L
287151 1
11/01/2019 13:39
YH
Dimethoate
BRL
0.45
20
ug/L
287151 1
11/01/2019 13:39
YH
Dimethyl phthalate
BRL
1.0
10
ug/L
287151 1
11/01/2019 13:39
YH
Diphenylamine
BRL
1.0
10
ug/L
287151 1
11/01/2019 13:39
YH
Disulfoton
BRL
0.68
10
ug/L
287151 1
11/01/2019 13:39
YH
Ethyl methanesulfonate
BRL
1.1
20
ug/L
287151 1
11/01/2019 13:39
YH
Famphur
BRL
0.72
20
ug/L
287151 1
11/01/2019 13:39
YH
Fluoranthene
BRL
1.0
10
ug/L
287151 1
11/01/2019 13:39
YH
Fluorene
BRL
12
10
ug/L
287151 1
11/01/2019 13:39
YH
Hexachlorobenzene
BRL
1 1
10
ug/L
287151 1
11/01/2019 13:39
YH
Hexachlorobutadiene
BRL
12
10
ug/L
287151 1
11/01/2019 13:39
YH
Hexachlorocyclopentadiene
BRL
21
10
ul!iL
287151 1
11/01/201913:39
YH
Hexachloroelhane
BRL
13
10
e/L
287151 1
11/01/2019 13:39
YH
Hexachloropropenc
BRL
10
10
ug/L
287151 1
11/01/2019 13:39
YH
Qualifiers: ' \;due exceeds maximum contaminant level
E Estimated
value abose
quanmauon ranee
BRL Not Detected 21 NIDL
S Spike Reco-ry outside
limns due io matrix
I I Holdme limes foi preparation or analysts exceeded
> G—icr than Result value
N Analyn not NELAC cenifed
1 Estimated
salve detected
bel— Reportme Lmnt
B Anal vie detected in the associa ied method blank
Less than
Result salue
Page I Page 35 of 70

Analytical Environmental Services, Inc
Date: 4-Nov-19
Client:
Prism Laboratories
Client Sample ID;
MW-02
Lab Order
1910S56
Tag Number:
9100380-01
Project Name:
9100380
Collection Date:
10/23/2019 9:26:00 AM
Lab ID:
1910S56-OOIA
Matrix:
Aqueous
Analyses Result Qual
MDL
Reporting
Limit
UnitsBatchID
DF
Date Analyzed
Analyst
APPENDIXII-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
lndeno(1,2,3-cd)pyrene
BRL
1.2
10
ug/L
287151 1
11/01/2019 13:39
YH
lsodrin
BRL
1.2
20
ug/L
287151 1
11/01/2019 13:39
YH
lsophorone
BRL
0.86
10
ug/L
287151 1
11/01/2019 13:39
YH
Isosafrole
BRL
1.1
10
ug/L
287151 1
11/01/2019 13:39
YH
Kepone
BRL
1.4
50
ug/L
287151 1
11/01/2019 13:39
YH
Methapyrilene
BRL
6.4
20
ug/L
287151 1
11/01/2019 13:39
YH
Methyl methanesulfonate
BRL
1.3
10
ug/L
287151 1
11/01/2019 13:39
YH
Methyl parathion
BRL
0.85
10
ug/L
287151 1
11/01/2019 13:39
YH
N-Nitroso-di-n-butylamine
BRL
1.8
10
ug/L
287151 1
11/01/2019 13:39
YH
N-Nitrosodi-n-propylamine
BRL
0.82
10
ug/L
287151 1
11/01/2019 13:39
YH
N-Nitrosodiethylamine
BRL
1.2
20
ug/L
287151 1
11/01/2019 13:39
YH
N-Nitrosodimethylamine
BRL
1.7
20
ug/L
287151 1
11/01/2019 13:39
YH
N-Nitrosodiphenylamine
BRL
0.90
50
ug/L
287151 1
11/01/2019 13:39
YH
N-Nitrosomethyl ethyl amine
BRL
1.00
10
ug/L
287151 1
11/01/2019 13:39
YH
N-Nitrosopiperi dine
BRL
0.86
20
ug/L
287151 1
11/01/2019 13:39
YH
N-Nitrosopyrrolidine
BRL
1.2
40
ug/L
287151 1
11/01/2019 13:39
YH
Naphthalene
BRL
1.2
10
ug/L
287151 1
11/01/2019 13:39
YH
Nitrobenzene
BRL
12
10
ug/L
287151 1
11/01/2019 13:39
YH
0,0,0-Triethylphosphorothioate
BRL
3.6
10
ng/L
287151 1
11/01/2019 13:39
YH
o-Toluidine
BRL
21
20
ug/L
287151 1
11/01/2019 13:39
YH
p-Dimethylaminoazobenzene
BRL
0.65
10
ug/L
287151 1
11/01/2019 13:39
YH
p-Phenylenediamine
BRL
55
500
ug/L
287151 1
11/01/2019 13:39
YH
Parathion
BRL
13
10
ug/L
287151 1
11/01/2019 13:39
YH
Pentachlorobenzene
BRL
0.94
10
ug/L
287151 1
11/01/2019 13:39
YH
Pen tach loronitrobenzene
BRL
0.96
20
ug/L
287151 1
11/01/2019 13:39
YH
Pentachlorophenol
BRL
0.62
5o
ug/L
287151 1
11/01/2019 13:39
YH
Phenacetin
BRL
0.85
20
rtg/L
287151 1
11/01/2019 13:39
YH
Phenanthrene
BRL
0.86
10
ug/L
287151 1
11/01/2019 13:39
YH
Phenol
BRL
0.77
10
ug/L
287151 1
11/01/2019 13:39
YH
Phorate
BRL
094
10
ug/L
287151 1
11/01/2019 13:39
YH
Pronamide
BRL
11
10
rig/L
287151 1
11/01/2019 13:39
YH
Pyrene
BRL
0.83
10
ug/L
287151 1
11/01/2019 13:39
YH
Safi-ole
BRL
1.2
20
ug/L
287151 1
11/01/2019 13:39
YH
Syni-Trinilrobenzene
BRL
0.98
10
ug/L
287151 1
11/01/2019 13:39
YH
Thionazin
BRL
0.81
20
ug/L
287151 1
11/01/2019 13:39
YH
Sun•:2.4.6-Tribromophenol
82
0
47-127
'%REC
287151 1
11/01/201913.39
YH
Sun•:2-Fluorobiphenyl
89.7
0
474-119
%REC
287151 1
11/01/2019 13:39
YH
Sun•:2-Fluorophenol
33.8
0
262-120
%REC
287151 1
11/01/2019 13:39
YH
Qualifiers: ' Value exceeds inaximum contaminant level
E Estimated
value above
quantitation ranee
BRL Not Defected at \1DL
5 spike Recovery outside Innus due to matrrx
H Holdmu limes for preparation or analysis exceeded
> Greater than Result value
N Ana [.vie not NELAC certified
J Estimated
value detected belo, Reporting Lunn
Analvte detected m the associated method blank
< Less than
Result value
Page I Page 36 of 70

Analytical Environmental Services, Inc
Date: 4-Nov-19
Client:
Prism Laboratories
Client Sample ID:
MW-02
Lab Order
1910S56
Tag Number:
9100380-01
Project Name:
9100380
Collection Date:
10/23/2019 9:26:00 AM
Lab ID:
1910S56-OOIA
Matrix:
Aqueous
Analyses Result Qual MDL ReportingUnits BatchID DF Date Analyzed Analyst
Limit
APPENDIXII-SEMIVOLATILE ORGANICS SW8270E (SW3510C)
Surr: 4-Terphenyl-d 14 6T5 0 45-133 /REC 28715) 111/01/201913:39 YH
Surr: Nitrobenzene-d5 99.7 0 41.9-121 /REC 287151 1 11/01/2019 13:39 YH
Surr: Phenol-d5 16.5 S 0 17.8-120 %REC 287151 I 11/01/2019 13:39 YH
Qualifiers: ' Value exceeds maximum contaminant level
BRL Not Detected at MDL
H Holding umes for preparation or analvsys exceeded
N AnalVLC not NELAC ccrttGed
B Analvte detected in the associated method blank
E Estimated value above quaninalion range
S Spike Recovery outside hunts due to matrix
Grater than Result value
J Estimated value detected below Reporting Linui
Less than Result value
Page I Page 37 of 70

Analytical Environmental Services, Inc
Date: 4-Nov-19
Client:
Prism Laboratories
Client Sample ID:
MW-03
Lab Order
191OS56
Tag Number:
9100380-02
Project Name:
9100380
Collection Date:
10/23/2019 10:26:00 AM
Lab ID:
191OS56-002A
Matrix:
Aqueous
Analyses Result Qual
MDL
ReportingUnits
Limit
BatchID DF
Date Analyzed
Analyst
APPENDIXII-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
1.2,4,5-Tetrachlorobenzene
BRL
1.3
10
ug/L
287151 1
11/01/2019 14:07
YH
1,2,4-Trichlorobenzene
BRL
1.4
10
ug/L
287151 1
11/01/2019 14:07
YH
1.2-Dichlorobenzene
BRL
1.2
10
ug/L
287151 1
11/01/2019 14:07
YH
1.3-Dichlorobenzene
BRL
1.3
10
ug/L
287151 1
11/01/2019 14:07
YH
1,3-Dinitrobenzene
BRL
1.1
20
ug/L
287151 1
11/01/2019 14:07
YH
1,4-Dichlorobenzene
BRL
1.4
10
ug/L
287151 1
11/01/2019 14:07
YH
1,4-Napthoquinone
BRL
1.7
10
ug/L
287151 1
11/01/2019 14:07
YH
1-Naphthylamine
BRL
30
10
ug/L
287151 1
11/01/2019 14:07
YH
2.3,4,6-Tetrachlorophenol
BRL
1.1
10
ug/L
287151 1
11/01/2019 14:07
YH
2.4,5-Trichlorophenol
BRL
0.99
10
ug/L
287151 1
11/01/2019 14:07
YH
2,4,6-Trichlorophenol
BRL
1.3
10
ug/L
287151 1
11/01/2019 14:07
YH
2,4-Dichlorophenol
BRL
1.0
10
ug/L
287151 1
11/01/2019 14:07
YH
2,4-Dimethylphenol
BRL
0.72
50
ug/L
287151 1
11/01/2019 14:07
YH
2,4-Dinitrophenol
BRL
5.5
50
ug/L
287151 1
11/01/2019 14:07
YH
2.4-Dinitrotoluene
BRL
1.1
10
ug/L
287151 1
11/01/2019 14:07
YH
2.6-Dichloroplienol
BRL
0.95
10
ug/L
287151 1
11/01/2019 14:07
YH
2.6-Dinitrotoluene
BRL
1.3
10
ug/L
287151 1
11/01/2019 14:07
YH
2-Acetylaminofluorene
BRL
1.1
20
ug/L
287151 1
11/01/2019 14:07
YH
2-Chloronaphthalene
BRL
1.8
10
ug/L
287151 1
11/01/2019 14:07
YH
2-Chlorophenol
BRL
1.2
10
ug/L
287151 1
11/01/2019 14:07
YH
2-Methylnaphthalene
BRL
1.2
10
ug/L
287151 1
11/01/2019 14:07
YH
2-Methylphenol
BRL
1.3
10
ug/L
287151 1
11/01/2019 14:07
YH
2-Naphthylamine
BRL
1.7
10
ug/L
287151 1
11/01/2019 14:07
YH
2-Nitroaniline
BRL
1.9
50
ug/L
287151 1
11/01/2019 14:07
YH
2-Nitrophenol
BRL
1.6
10
ug/L
287151 1
11/01/2019 14:07
YH
3.3"-Dichlorobenzidine
BRL
11
20
ug/L
287151 .1
11/01/2019 14:07
YH
3,3"-Dimethylbenzidine
BRL
5.4
20
ug/L
287151 1
11/01/2019 14:07
YH
3.4-Methylphenol
BRL
2 3
10
tig/L
287151 1
11/01/2019 14:07
YH
3-Methy1cholanthrene
BRL
1 1
10
ug/L
287151 1
11/01/2019 14:07
YH
3-Nitroaniline
BRL
12
50
ug/L
287151 1
11/01/2019 14:07
YH
4.6-Dinitro-2-methylphenol
BRL
13
50
It/L
287151 1
11/01/2019 14:07
YH
4-Aminobiphenyl
BRL
24
20
ug/L
287151 1
11/01/2019 1407
YH
4-Bromophenyl phenyl ether
BRL
1 4
10
ug/L
287151 1
11/01/2019 14:07
YH
4-Chloro-3-methylphenol
BRL
0.81
20
ug/L
287151 1
11/01/20191407
YH
4-Chloroandine
BRL
21
20
ug/L
287151 1
11/01/2019 14:07
YH
4-Chlorophenyl phenyl ether
BRL
1 3
10
ug/L
287151 1
11/01/2019 14:07
YH
4-Nitroaniline
BRL
13
20
ug/L
287151 1
11/01/2019 14:07
YH
4-Nitrophenol
BRL
077
50
ug/L
287151 1
11/01/2019 14:07
YH
Qualifiers: ` Value exceeds maxunum contaminant level
E Estimated
salue abose
quanutation ranee
BRL Not Detected at N1DL
S Spike Recoven outside limns due to matrix
H Holding tunes for preparation or analesis exceeded
> Greaier than Result salve
N Anahte not NELAC eenified
J Eswnaied
salue detected below Reporting Limn
B Analete detected m the associated method blank
< Less than
Result salue
Page 38 of 70

Analytical Environmental Services, Inc
Date: 4-Nov-19
Client:
Prism Laboratories
Client Sample ID:
MW-03
Lab Order
191 OS56
Tag Number:
9100380-02
Project Name:
9100380
Collection Date:
10/23/2019 10:26:00 AM
Lab ID:
1910S56-002A
Matrix:
Aqueous
Analyses Result Qual
MDL
ReportingUnits
Limit
BatchID DF
Date Analyzed Analyst
APPENDIXII-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
5-Nitro-o-toluidine
BRL
0.66
10
ug/L
287151 1
11/01/2019 14:07
YH
7,12-Dimethylbenz(a)anthracene
BRL
14
10
ug/L
287151 1
11/01/2019 14:07
YH
Acenaphthene
BRL
11
l0
ug/L
287151 1
11/01/2019 14:07
YH
Acenaphthylene
BRL
1.1
10
ug/L
287151 1
11/01/2019 14:07
YH
Acetophenone
BRL
2.1
10
ug/L
287151 1
11/01/2019 14:07
YH
Anthracene
BRL
0,82
10
ug/L
287151 1
11/01/2019 14:07
YH
Benz(a)anthracene
BRL
0.96
10
ug/L
287151 1
11/01/2019 14:07
YH
Benzo(a)pyrene
BRL
0.96
10
ug/L
287151 1
11/01/2019 14:07
YH
Benzo(b)fluoranthene
BRL
1.5
10
ug/L
287151 1
11/01/2019 14:07
YH
Bcnzo(g,hJ)perylene
BRL
1.3
10
ug/L
287151 1
11/01/2019 14:07
YH
Benzo(k)fluoranthene
BRL
15
10
ug/L
287151 1
11/01/2019 14:07
YH
Benzyl alcohol
BRL
1.4
20
ug/L
287151 1
11/01/2019 14:07
YH
Bis(2-chloroethoxy)methane
BRL
1.1
10
ug/L
287151 1
11/01/2019 14:07
YH
Bis(2-chloroethyl)ether
BRL
1.2
10
ug/L
287151 1
11/01/2019 14:07
YH
Bis(2-chloroisopropyl)ether
BRL
1.5
10
ug/L
287151 1
11/01/2019 14:07
YH
Bis(2-ethylhexyl)phthalate
BRL
14
20
ug/L
287151 1
11/01/2019 14:07
YH
Butyl benzyl phthalate
BRL
0.84
10
ug/L
287151 1
11/01/2019 14:07
YH
Chlorobenzilate
BRL
0.57
10
ug/L
287151 1
11/01/2019 14:07
YH
Chrysene
BRL
0.93
10
ug/L
287151 1
11/01/2019 14:07
YH
Di-n-butyl phthalate
BRL
1 1
10
ug/L
287151 1
11/01/2019 14:07
YH
Di-n-octyl phthalate
BRL
1.6
10
ug/L
287151 1
11/01/2019 14:07
YH
Diallate
BRL
0.84
10
ug/L
287151 1
11/01/2019 14:07
YH
Dibenz(a,h)anthracene
BRL
1.4
10
ug/L
287151 1
11/01/2019 14:07
YH
Dibenzofuran
BRL
1.1
10
ug/L
287151 1
11/01/2019 14:07
YH
Diethyl phthalate
1.3 J
0.82
10
ug/L
287151 1
11/01/2019 14:07
YH
Dimethoate
BRL
0.45
20
ug/L
287151 1
11/01/2019 14:07
YH
Dimethylphthalate
BRL
1.0
10
ug/L
287151 1
11/01/20191407
YH
Diphenylamine
BRL
1.0
10
ug/L
287151 1
11/01/2019 14:07
YH
Disulfoton
BRL
0.68
10
ug/L
287151 1
11/01/2019 14:07
YH
Ethyl methanesulfonate
BRL
1.1
20
ug/L
287151 1
11/01/2019 14:07
YH
Famphur
BRL
0.72
20
ug/L
287151 1
11/01/2019 14:07
YH
Fluoranthene
BRL
10
10
ug/L
287151 1
11/01/2019 14:07
YH
Fluorene
BRL
12
10
ug/L
287151 1
11/01/2019 14:07
YH
Hexachlorobenzene
BRL
I 1
10
ug/L
287151 1
11/01/20191407
YH
I-lexachlorobutadiene
BRL
12
10
ug/L
287151 1
11/01/20191407
YH
Hexachlorocyclopentadienc
BRL
2.1
10
ug/L
287151 1
11/01/20191407
YH
Hexachloroethane
BRL
13
10
ug/L
287151 1
11/01/2019 14:07
YH
Hexachloropropene
BRL
1.0
10
ug/L
287151 1
11/01/2019 14:07
YH
Qualifiers: s Value exceedsmax, con .....mnt level
E Estimaied
- lue abore quantitation ranee
BRL Not Detected at N1DL
S Spike Reco—, outside
limns due to matrix
H Holding times for preparation or analysis exceeded
> Greater than Result r
alue
N Analeie not NELAC cenified
J Esumated
%clue deiecied bel—, Reporting Lmw
B Anil) to deiected in the associated method blank
I Less than
Result Value
Page I Page 39 of 70

Analytical Environmental Services, Inc
Date: 4-Nov-19
Client:
Prism Laboratories
Client Sample ID:
MW-03
Lab Order
191OS56
Tag Number:
9100380-02
Project Name:
9100380
Collection Date:
10/23/2019 10:26:00 AM
Lab ID:
191OS56-002A
Matrix:
Aqueous
Analyses Result Qual
MDL
Reporting
Limit
Units
BatchID DT
Date Analyzed
Analyst
APPENDIXII-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
Indeno(1,2,3-ed)pyrene
BRL
1.2
10
ug/L
287151 1
11/01/201914:07
YH
Isodrin
BRL
1.2
20
ug/L
287151 1
11/01/201914:07
YH
Isophorone
BRL
0.86
10
ug/L
287151 1
11/01/201914:07
YH
Isosafrole
BRL
1.1
10
ug/L
287151 1
11/01/201914:07
YH
Kepone
BRL
1.4
50
ug/L
287151 1
11/01/201914:07
YH
Methapyrilene
BRL
6.4
20
ug/L
287151 1
11/01/201914:07
YH
Methyl methanesulfonate
BRL
L3
10
ug/L
287151 1
11/01/2019 1407
YH
Methyl parathion
BRL
0.85
10
ug/L
287151 1
11/01/2019 14:07
YH
N-Nitroso-di-n-butylamine
BRL
1.8
10
ug/L
287151 l
11/01/201914:07
YH
N-Nitrosodi-n-propylamine
BRL
0.82
10
ug/L
287151 I
11/01/201914:07
YH
N-Nitrosodiethylamine
BRL
1.2
20
ug/L
287151 1
11/01/201914:07
YH
N-Nitrosodimethylamine
BRL
1.7
20
ug/L
287151 1
11/01/201914:07
YH
N-Nitrosodiphenylamine
BRL
0.90
50
ug/L
287151 1
11/01/201914:07
YH
N-Nitrosomethylethylamine
BRL
1.00
10
ug/L
287151 1
11/01/201914:07
YH
N-Nitrosopiperidine
BRL
0.86
20
ug/L
287151 t
11/01/201914:07
YH
N-Nitrosopyrrolidine
BRL
12
40
ug/L
287151 1
11/01/201914:07
YH
Naphthalene
BRL
L2
10
ug/L
287151 1
11/01/201914:07
YH
Nitrobenzene
BRL
1.2
10
ug/L
287151 1
11/01/201914:07
YH
0,0,0-Triethylphosphorothioate
BRL
3.6
10
ug/L
287151 1
11/01/201914:07
YH
o-Toluidine
BRL
2.1
20
ug/L
287151 1
11/01/201914:07
YH
p-Dimethylaminoazobenzene
BRL
0.65
10
ug/L
287151 1
11/01/201914:07
YH
p-Phenylenediamine
BRL
55
500
ug/L
287151 1
11/01/201914:07
YH
Parathion
BRL
1.3
10
ug/L
287151 1
11/01/201914.07
YH
Pen tachlorobenzene
BRL
0.94
10
ug/L
287151 1
11/01/201914:07
YH
Pentachloronitrobenzene
BRL
0.96
20
ug/L
287151 1
11/01/201914:07
YH
Pentachlorophenol
BRL
0.62
50
ug/L
287151 1
11/01/201914:07
YH
Phenacetin
BRL
0.85
20
ug/L
287151 1
11/01/201914:07
YH
Phenanthrene
BRL
0.86
10
ug/L
287151 1
11/01/201914.07
YH
Phenol
BRL
0.77
10
ug/L
287151 1
11/01/201914:07
YH
Phorate
BRL
0.94
10
ug/L
287151 1
11/01/201914:07
YH
Pronamide
BRL
1.1
10
ug/L
287151 1
11/01/201914:07
YH
Pvrene
BRL
0.83
10
ug/L
287151 1
11/01/20191407
YH
Safi -Ole
BRL
1.2
20
ug/L
287151 1
11/01/20191407
YH
Sym-Trinitroben zene
BRL
0.98
10
ug/L
287151 1
11/01/20191407
YH
Thionazin
BRL
0.81
20
ug/L
287151 1
11/01/201914:07
YH
Surr:2.4.6-Tribromophenol
359 S
0
47-127
%REC
287151 .1
11/01/201914:07
YH
Surr:2-Fluorobiphenyl
51.5
0
47.4-119
o/REC
287151 1
11/01/201914:07
YH
Surr:2-Fluorophenol
14 S
0
262-120
°bREC
287151 1
11/01/201914:07
YH
Qualifiers: e Value exceeds ntaumunt contannnant Iecel
E Est mated Value above
quanutat- range
BRL Not Detected at NIDL
S Spike Recosery outside
Imtns due to ntatris
FI Holding notes for preparation or analvsis exceeded
- Greater than Result Value
N Analgte not NELAC ceniGed
J Estn mated
va Inc detect ed below Report me Lunn
D Analrtc detected in the associated method blank
- Less titan
Result Valuc
Page J Page 40 of 70

Analytical Environmental Services, Inc
Date: 4-Nov-19
Client:
Prism Laboratories
Client Sample ID:
MW-03
Lab Order
191 OS56
Tag Number:
9100380-02
Project Name:
9100380
Collection Date:
10/23/2019 10:26:00 AM
Lab ID:
191OS56-002A
Matrix:
Aqueous
Analyses Result Qual MDL Reporting Units BatchID DF Date Analyzed Analyst
Limit
APPENDIXII-SEMIVOLATILE ORGANICS SW8270E (SW3510C)
Surr: 4-Terphenyl-d 14 34.8 S 0 45-133 %REC 287151 1 11/01/201914:07 YH
Surr: Nitrobenzene-d5 52.1 0 41.9-121 %REC 287151 I 11/01/2019 14:07 YH
Surr: Phenol-d5 8.66 S 0 17.8-120 %REC 287151 I 11/01/2019 14:07 YH
Qualifiers: ' Value exceeds maximum conianunant level
BRL Not Dciectcd ai NIDL
H Holding limes for preparation or analcsis exceeded
N Analyte not NELAC certified
B Analyte deieci d in the associated method blank
E Estimaled %slue abote quantiiauon range
5 spike Recot cry outside limns due to matnx
> Greater than Result salue
J Estimated ialuc detected below Reporting Limn
Less than Result %slue
Page 1 Page 41 of 70

Analytical Environmental Services, Inc
Date: 4-Nov-19
Client:
Prism Laboratories
Client Sample ID:
MW-05R
Lab Order
191OS56
Tag Number:
9100380-03
Project Name:
9100380
Collection Date:
10/23/2019 2:32:00 PM
Lab ID:
191OS56-003A
Matrix:
Aqueous
Analyses Result Qual
MDL
ReportingUnits
Limit
BatchID DF
Date Analyzed
Analyst
APPENDIXII-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
1,2,4,5-Tetrachlorobenzene
BRL
1.3
10
ug/L
287151 I
11/01/201914:35
YH
1,2,4-Trichlorobenzene
BRL
1.4
10
ug/L
287151 1
11/01/2019 14:35
YH
1,2-Dichlorobenzene
BRL
1.2
10
ug/L
287151 1
11/01/2019 14:35
YH
1,3-Di chlorobenzene
BRL
13
10
ug/L
287151 1
11/01/2019 14:35
YH
1,3-Dinitrobenzene
BRL
1.1
20
ug/L
287151 1
11/01/2019 14:35
YH
1,4-Dichlorobenzene
5.0 J
1.4
10
ug/L.
287151 1
11/01/2019 14:35
YH
1,4-Napthoquinone
BRL
1.7
10
ug/L
287151 1
11/01/2019 14:35
YH
1-Naphthylamine
BRL
3.0
10
ug/L
287151 1
11/01/2019 14:35
YH
2.3;4,6-Tetrachlorophenol
BRL
1.1
10
ug/L
287151 1
11/01/2019 14:35
YH
2,4.5-Trichlorophenol
BRL
0.99
10
ug/L
287151 1
11/01/2019 14:35
YH
2,4,6-Trichlorophenol
BRL
1.3
10
ug/L
287151 1
11/01/2019 14:35
YH
2.4-Dichlorophenol
BRL
1.0
10
ug/L
287151 1
11/01/2019 14:35
YH
2.4-Dimethylphenol
BRL
072
50
ug/L
287151 1
11/01/2019 14:35
YH
2.4-Dinitrophenol
BRL
5.5
50
ug/L
287151 1
11/01/2019 14:35
YH
2.4-Dinitrotoluene
BRL
1.1
10
ug/L
287151 1
11/01/2019 14:35
YH
2,6-Dichlorophenol
BRL
0.95
10
ug/L
287151 1
11/01/2019 14:35
YH
2,6-Dinitrotoluene
BRL
1.3
10
ug/L
287151 1
11/01/2019 14:35
YH
2-Acetylaminofluorene
BRL
1.1
20
ug/L
287151 I
11/01/2019 14:35
YH
2-Chloronaphthalene
BRL
18
10
ug/L
287151 1.
11/01/2019 14:35
YH
2-Chlorophenol
BRL
12
10
ug/L
287151 1
11/01/2019 14:35
YH
2-Methylnaphthalene
BRL
12
10
ug/L
287151 1•
11/01/2019 14:35
YH
2-Methylphenol
BRL
13
10
ug/L
287151 1.
11/01/2019 14:35
YH
2-Naphthylamine
BRL
1.7
10
ug/L
287151 1
11/01/2019 14:35
YH
2-Nitroaniline
BRL
19
50
ug/L
287151 1
11/01/20191435
YH
2-Nitrophenol
BRL
16
10
ug/L
287151 1
11/01/2019 14:35
YH
3.3"-Dichlorobenzidine
BRL
1.1
20
ug/L
287151 1
11/01/2019 14:35
YH
3.3"-Dimethylbenzidine
BRL
5.4
20
ug/L
287151 1
11/01/2019 14:35
YH
3.4-Methylphenol
BRL
2.3
10
ug/L
287151 1
11/01/2019 14:35
YH
3-Methy1cholanthrene
BRL
11
10
ug/L
287151 1
11/01/2019 14:35
YH
3-Nitroaniline
BRL
12
50
ug/L
287151 1
11/01/2019 14:35
YH
4,6-Dinitro-2-methylphenol
BRL
1.3
50
ug/L
287151 1
11/01/2019 14:35
YH
4-Aminobiphenyl
BRL
2.4
20
tig/L
287151 1
11/01/201914:35
YH
4-Bromophenyl phenyl ether
BRL
1 4
10
ug/L
287151 1
11/01/2019 14:35
YH
4-Chloro-3-methylphenol
BRL
0 81
20
ug/L
287151 1
11/01/2019 14:35
YH
4-Chloroaniline
BRL
21
20
ug/L
287151 1
11/01/2019 14:35
YH
4-Chlorophenyl phenyl ether
BRL
1.3
10
ttg/L
287151 1
11/01/2019 14:35
YH
4-Nitroaniline
BRL
1.3
20
ug/L
287151 1
11/01/2019 14:35
YH
4-Nitrophenol
BRL
077
50
ttg/L
287151 1
11/01/201914:35
YH
Qualifiers: ' Value exceeds ntaummn contatmnant level
E Estimated value above
quanwauon ranee
BRL Not Detected at NIDL
S Spike Ree-cry
outside units due to matrix
H Holding limes for preparation or analysts exceeded
- Grauer
than Result � alue
N Analete riot NELAC certded
J Estimated value detected
below Reporting Lint
B Analete detected in the associated method blank
I Less than Result salue
Page 1 Page 42 of 70

Analytical Environmental Services, Inc
Date: 4-Nov-19
Client:
Prism Laboratories
Client Sample ID:
MW-05R
Lab Order
191OS56
Tag Number:
9100380-03
Project Name:
9100380
Collection Date:
10/23/2019 2:32:00 PM
Lab 1D:
191 OS56-003A
Matrix:
Aqueous
Analyses Result Qual
MDL
ReportingUnits
Limit
BatchID
DF Date Analyzed Analyst
APPENDIXII-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
5-Nitro-o-toluidine
BRL
0.66
10
ug/L
287151
1
11/01/2019 14:35
YH
7,12-Dimethylbenz(a)anthracene
BRL
1.4
10
ug/L
287151
1
11/01/2019 14:35
YH
Acenaphthene
BRL
1.1
10
ug/L
287151
1
11/01/2019 14:35
YH
Acenaphthylene
BRL
1.1
10
ug/L
287151
1
11/01/2019 14:35
YH
Acetophenone
BRL
2.1
10
ug/L
287151
1
11/01/2019 14:35
YH
Anthracene
BRL
0.82
10
ug/L
287151
1
11/01/2019 14:35
YH
Benz(a)anthracene
BRL
0.96
10
ug/L
287151
1
11/01/2019 14:35
YH
Benzo(a)pyrene
BRL
0.96
10
ug/L
287151
1
11/01/2019 14:35
YH
Benzo(b)fluoranthene
BRL
1.5
10
ug/L
287151
1
11/01/2019 14:35
YH
Benzo(g,h,i)perylene
BRL
1.3
10
ug/L
287151
I
11/01/2019 14:35
YH
Benzo(k)fluoranthene
BRL
1.5
10
ug/L
287151
1
11/01/2019 14:35
YH
Benzyl alcohol
BRL
1.4
20
ug/L
287151
1
11/01/2019 14:35
YH
Bis(2-chloroethoxy)methane
BRL
1.1
10
ug/L
287151
1
11/01/2019 14:35
YH
Bis(2-chloroethyl)ether
BRL
1.2
10
ug/L
287151
1
11/01/2019 14:35
YH
Bis(2-chloroisopropyl)ether
BRL
1.5
10
ug/L
287151
1
11/01/2019 14:35
YH
Bis(2-ethylhexyl)phthalate
BRL
1.4
20
ug/L
287151
1
11/01/2019 14:35
YH
Butyl benzyl phthalate
BRL
0.84
10
ug/L
287151
1
11/01/2019 14:35
YH
Chlorobenzilate
BRL
0.57
10
ug/L
287151
1
11/01/2019 14:35
YH
Chrysene
BRL
0.93
10
ug/L
287151
1
11/01/2019 14:35
YH
Di-n-butyl phthalate
BRL
1.1
10
ug/L
287151
I:
11/01/2019 14:35
YH
Di-n-octyl phthalate
BRL
1.6
10
ug/L
287151
1
11/01/2019 14:35
YH
Diallate
BRL
0.84
10
ug/L
287151
1
11/01/2019 14:35
YH
Dibenz(a,h)anthracene
BRL
1.4
10
ug/L
287151
1
11/01/2019 14:35
YH
Dibenzofuran
BRL
1.1
10
ug/L
287151
T
11/01/2019 14:35
YH
Diethyl phthalate
BRL
0.82
10
ug/L
287151
I
11/01/2019 14:35
YH
Dimethoate
BRL
0.45
20
ug/L
287151
1
11/01/2019 14:35
YH
Dimethyl phthalate
BRL
1.0
10
ug/L
287151
1
11/01/2019 14:35
YH
Diphenylamine
BRL
1.0
10
ug/L
287151
1
11/01/2019 14:35
YH
Disulfoton
BRL
0.68
10
ug/L
287151
1
11/01/2019 14:35
YH
Ethyl methanesulfonate
BRL
1.1
20
ug/L
287151
1
11/01/2019 14:35
YH
Famphur
BRL
0.72
20
ug/L
287151
1
11/01/2019 14:35
YH
Fluoranthene
BRL
1.0
10
ug/L
287151
1
11/01/20191435
YH
Fluorene
BRL
1.2
10
ug/L
287151
1
11/01/201914:35
YH
Hexachlorobenzene
BRL
1.1
10
ug/L
287151
1
11/01/2019 14 35
YH
Hexachlorobutadiene
BRL
12
10
ug/L
287151
1
11/01/2019 14:35
YH
Hexachlorocyclopentadiene
BRL
21
10
ttg/L
287151
1
11/01/2019 14:35
YH
Hexachloroethane
BRL
13
10
ug/L
287151
.1
11/01/2019 14:35
YH
Hexachloropropene
BRL
10
10
ug/L
287151
.1
11/01/2019 14:35
YH
QualirwP : r %'slue Phu %nil uut van umnu Pit Iowl
E Estimated
value abosc
quanutauon range
BRL Not Deiected at \IDL
S Spike Recovery outside limns due to matrix
H Holding umes for prepamuon or analysis exceeded
> Greater than Result s alue
N Analxm not NEL\C certified
J Estimated
talue detected
below Reporting
Lmut
B Analvle detected in the associated method blank
I Less than
Result value
Page 1 Page 43 of 70

Analytical Environmental Services, Inc
Date: 4-Nov-19
Client:
Prism Laboratories
Client Sample 1D:
MW-05R
Lab Order
191OS56
Tag Number:
9100380-03
Project Name:
9100380
Collection Date:
10/23/2019 2:32:00 PM
Lab ID:
191 OS56-003A
Matrix:
Aqueous
Analyses Result Qual
MDL
ReportingUnits
Limit
BatchlD DF
Date Analyzed
Analyst
APPENDIXII-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
Indeno(1,2,3-cd)pyrene
BRL
1.2
10
ug/L
287151 1
11/01/2019 14:35
YH
Isodrin
BRL
12
20
ug/L
287151 1
11/01/2019 14:35
YH
Isophorone
BRL
0.86
10
ug/L,
287151 1
11/01/2019 14:35
YH
Isosafrole
BRL
1.1
10
ug/L.
287151 1
11/01/2019 14:35
YH
Kepone
BRL
1.4
50
ug/L
287151 1
11/01/2019 14:35
YH
Methapyrilene
BRL
6.4
20
ug/L
287151 1
11/01/2019 14:35
YH
Methyl methanesulfonate
BRL
1.3
10
ug/L
287151 1
11/01/2019 14:35
YH
Methyl parathion
BRL
0.85
10
ug/L
287151 1
11/01/2019 14:35
YH
N-Nitroso-di-n-butylamine
BRL
1.8
10
ug/L
287151 1
11/01/2019 14:35
YH
N-Nitrosodi-n-propylamine
BRL
0.82
10
ug/L
287151 1
11/01/2019 14:35
YH
N-Nitrosodiethylamine
BRL
1.2
20
ug/L
287151 1
11/01/2019 14:35
YH
N-Nitrosodimethylamine
BRL
1.7
20
ug/L
287151 1
11/01/2019 14:35
YH
N-Nitrosodiphenylamine
BRL
0.90
50
ug/L
287151 1
11/01/2019 14:35
YH
N-Nitrosomethylethylamine
BRL
1.00
10
ug/L
287151 1
11/01/2019 14:35
YH
N-Nitrosopiperidine
BRL
0.86
20
ug/L
287151 1
11/01/2019 14:35
YH
N-Nitrosopyrrolidine
BRL
1.2
40
ug/L
287151 1
11/01/2019 14:35
YH
Naphthalene
BRL
1.2
10
ug/L
287151 1
11/01/2019 14:35
YH
Nitrobenzene
BRL
1.2
10
ug/L.
287151 1
11/01/2019 14:35
YH
0,0,0-Triethylphosphorothioate
BRL
3.6
10
ug/L
287151 .1
11/01/2019 14:35
YH
o-Toluidine
BRL
21
20
ug/L
287151 1
11/01/2019 14:35
YH
p-Dimethylaminoazobenzene
BRL
0.65
10
ug/L
287151 1
11/01/2019 14:35
YH
p-Phenylenediamine
BRL
55
500
❑g/L
287151 I
11/01/2019 14:35
YH
Parathion
BRL
1.3
10
ug/L
287151 1
11/01/201914:35
YH
Pentachlorobenzene
BRL
0.94
10
ug/L
287151 1
11/01/2019 14:35
YH
Pentachloronitrobenzene
BRL
0,96
20
ug/L
287151 1
11/01/20191435
YH
Pentachlorophenol
BRL
0.62
50
ug/L
287151 1
11/01/2019 14:35
YH
Phenacetin
BRL
0.85
20
ug/L
287151 1
11/01/2019 14:35
YH
Phenanthrene
BRL
0.86
10
ttg/L
287151 1
11/01/2019 14:35
YH
Phenol
BRL
077
10
ug/L
287151 1
11/01/2019 14:35
YH
Phorate
BRL
0.94
10
ug/L
287151 1
11/01/2019 14:35
YH
Pronamide
BRL
11
10
ug/L
287151 l
11/01/2019 14:35
YH
Pyrene
BRL
0 83
10
ug/L
287151 1
11/01/2019 14:35
YH
Safrole
BRL
12
20
ug/L
287151 1
11/01/2019 14:35
YH
Svm-Trinitrobenzene
BRL
098
10
ug/L
287151 1
11/01/2019 14:35
YH
Thionazin
BRL
081
20
ug/L
287151 1
11/01/2019 14:35
YH
Surr:2.4.6-Tribromophenol
89
0
47-127
%REC
287151 1
11/01/2019 14:35
YH
Surr:2-Fluorobiphenyl
86
0
47,4-119
"NREC
287151 1
11/01/20191435
YH
SUIT: 2-Fluorophenol
35.7
0
26.2-120
ONREC
287151 1
11/01/2019 14:35
YH
Qualifiers: ' Value exceeds maxunum coniannnam lv%el
E Estunaied
%alue above
quanutation range
BRL Not Deiecled ai AIDL
S Spike Recoeery outside limns due to mains
FI Holding times for preparmon or analysis exceeded
- Greater than
Result value
N Analyte not NELAC ceru Ged
1 Estimated
talue detected
below Reporting Lmw
B Anal vie detected in the assona i ed method blank
Less than
Result 1.1ov
Page 1 Page 44 of 70

Analytical Environmental Services, Inc
Date: 4-Nov-19
Client:
Prism Laboratories
Client Sample ID:
MW-05R
Lab Order
191OS56
Tag Number:
9100380-03
Project Name-
9100380
Collection Date:
10/23/2019 2:32:00 PM
Lab ID:
191 OS56-003A
Matrix:
Aqueous
Analyses Result Qua] MDL ReportingUnits BatchID DF Date Analyzed Analyst
Limit
APPENDIXII-SEMIVOLATILE ORGANICS SW8270E (SW3510C)
Surr:4-Terphenyl-d14 39.9 S 0 45-133 %REC 287151 1 11/01/201914:35 YH
Surr: Nitrobenzene-d5 100 0 41.9-121 %REC 287151 1 11/01/2019 14:35 YH
Surr: Phenol-d5 22.2 0 17.8-120 %REC 287151 1 11/01/2019 14:35 YH
Qualifiers: ' Value exceeds maximum contammant level
BRL Not Detected m NIDL
H Holding tines for preparation or nnalyvs exceeded
N Analvtc not NELAC ceniGcd
B Anahte detected in the associated method blank
E Estimated value above quantitation range
S Spike Recovery outside limits due to matrix
> Greater than Result value
1 Estimated value detected below Reporting Lima
< Less than Result talue
Page 1 Page 45 of 70

Analytical Environmental Services, Inc
Date: 4-Nov-19
Client:
Prism Laboratories
Client Sample ID:
MW-06
Lab Order
191 OS56
Tag Number:
9100380-04
Project Name:
9100380
Collection Date:
10/23/2019 12:54:00 PM
Lab 1D:
191OS56-004A
Matrix:
Aqueous
Analyses Result Qual
MDL
ReportingUnits
Limit
BatchID DF
Date Analyzed
Analyst
APPENDIXII-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
1,2,4,5-Tetrachlorobenzene
BRL
13
10
ug/L
287151 1
11/01/201915:04
YH
1,2,4-Trichlorobenzene
BRL
1.4
10
ug/L
287151 1
11/01/201915:04
YH
1,2-Dichlorobenzene
BRL
1.2
10
ug/L
287151 1
11/01/201915:04
YH
1.3-Dichlorobenzene
BRL
13
10
ug/L
287151 1
11/01/201915:04
YH
1,3-Dinitrobenzene
BRL
11
20
ug/L
287151 1
11/01/201915:04
YH
1,4-Dichlorobenzene
BRL
14
10
ug/L
287151 1
11/01/201915:04
YH
1,4-Napthoquinone
BRL
1.7
10
ug/L
287151 1
11/01/201915:04
YH
1-Naphthylamine
BRL
10
10
ug/L
287151 1
11/01/201915:04
YH
2,3,4,6-Tetrachlorophenol
BRL
1.1
10
ug/L
287151 1
11/01/201915:04
YH
2,4,5-Trichlorophenol
BRL
0.99
10
ug/L.
287151 1
11/01/201915:04
YH
2,4,6-Trichloropbenol
BRL
1.3
10
ug/L
287151 1
11/01/201915:04
YH
2,4-Dichlorophenol
BRL
1.0
10
ug/L
287151 1
11/01/201915:04
YH
2,4-Dimethylphenol
BRL
0,72
50
ug/L
287151 1
11/01/201915:04
YH
2,4-Dinitrophenol
BRL
5.5
50
ug/L
287151 1
11/01/201915:04
YH
2,4-Dinitrotoluene
BRL
1.1
10
ug/L
287151 1
11/01/201915:04
YH
2,6-Dichlorophenol
BRL
0,95
10
ug/L
287151 1
11/01/201915:04
YH
2,6-Dinitrotoluene
BRL
1.3
10
ug/L
287151 1
11/01/201915:04
YH
2-Acetylaminofluorene
BRL
1.1
20
ug/L
287151 1
11/01/201915:04
YH
2-Chloronaphthalene
BRL
1.8
10
ug/L
287151 1
11/01/201915:04
YH
2-Chlorophenol
BRL
12
10
ug/L
287151 1
11/01/201915:04
YH
2-Methylnaphthalene
BRL
12
10
ug/L
287151 1
11/01/201915:04
YH
2-Methylphenol
BRL
1.3
10
ug/L
287151 1
11/01/201915:04
YH
2-Naphthylamine
BRL
17
10
ug/L
287151 1
11/01/201915:04
YH
2-Nitroaniline
BRL
19
50
ug/L
287151 1
11/01/201915:04
YH
2-Nitrophenol
BRL
16
10
ug/L
287151 1
11/01/201915:04
YH
33"-Dich1orobenzidine
BRL
11
20
ug/L
287151 1
11/01/201915:04
YH
3,3"-Dimethylbenzidine
BRL
54
20
ug/L
287151 1
11/01/201915:04
YH
3,4-Methylphenol
BRL
23
10
ug/L
287151 1
11/01/2019 15:04
YH
3-Methyleholanthrene
BRL
11
10
ug/L
287151 1
11/01/201915:04
YH
3-Nitroaniline
BRL
12
50
ug/L
287151 1
11/01/201915:04
YH
4,6-Dinitro-2-methylphenol
BRL
13
50
ug/L
287151 1
11/01/201915:04
YH
4-Aminobiphenyl
BRL
2.4
20
ug/L
287151 1
11/01/201915:04
YH
4-Bromophenyl phenyl ether
BRL
1 4
10
ug/L
287151 1
11/01/2019 1504
YH
4-Chloro-3-methylphenol
BRL
0.81
20
ug/L
287151 1
11/01/201915:04
YH
4-Chloroaniline
BRL
21
20
ug/L
287151 1
11/01/201915:04
YH
4-Chlorophenyl phenyl ether
BRL
1 3
10
ug/L
287151 1
11/01/2019 15:04
YH
4-Nitro-aniline
BRL
1.3
20
ug/L
287151 1
11/01/20191504
YH
4-Nitrophenol
BRL
0.77
50
ug/L
287151 1
11/01/20191504
YH
Qualifiers: ' Value exceeds maxunum contanunant le%el
E Esummed
value above
quanwauon ranee
BRL Not Detected m N•IDL
S Spike Recovery onside limns due io matrix
H Holding times for preparation or anahsis exceeded
I Greater than Result value
N Analate not NELAC ccni(ed
1 Estimated
value detected below Reporune Limn
B Analvie detected in the associated method blank
- Less than
Result value
Page 1 Page 46 of 70

Analytical Environmental Services, Inc
Date: 4-Nov-19
Client:
Prism Laboratories
Client Sample ID:
MW-06
Lab Order
191OS56
Tag Number:
9100380-04
Project Name:
9100380
Collection Date:
10/23/2019 12:54:00 PM
Lab ID:
191OS56-004A
Matrix:
Aqueous
Analyses Result Qua]
MDL
Reporting
Limit
Units
BatchlD DF
Date Analyzed
Analyst
APPENDIXII-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
5-Nitro-o-toluidine
BRL
0.66
10
ug/L
287151 1
11/01/2019 15:04
YH
7,12-Dimethylbenz(a)anthracene
BRL
1.4
10
ug/L.
287151 1
11/01/2019 15:04
YH
Acenaplithene
BRL
1.1
10
ug/L
287151 1
11/01/2019 15:04
YH
Acenaphthylene
BRL
1.1
10
ug/L
287151 1
11/01/2019 15:04
YH
Acetophenone
BRL
2.1
10
ug/L
287151 1
11/01/2019 15:04
YH
Anthracene
BRL
0.82
10
ug/L
287151 1
11/01/2019 15:04
YH
Benz(a)anthracene
BRL
0.96
10
ug/L
287151 1
11/01/2019 15:04
YH
Benzo(a)pyrene
BRL
0.96
10
ug/L
287151 1
11/01/2019 15:04
YH
Benzo(b)fluoranthene
BRL
1.5
10
ug/L
287151 1
11/01/2019 15:04
YH
Benzo(g_h,i)perylene
BRL
1.3
10
ug/L
287151 1
11/01/2019 15:04
YH
Benzo(k)fluoranthene
BRL
15
10
ug/L
287151 1
11/01/2019 15:04
YH
Benzy] alcohol
BRL
1.4
20
ug/L
287151 1
11/01/2019 15:04
YH
Bis(2-chloroethoxy)methane
BRL
11
10
ug/L
287151 1
11/01/2019 15:04
YH
Bis(2-chloroethyl)ether
BRL
1.2
10
ug/L
287151 t
11/01/2019 15:04
YH
Bis(2-chloroisopropyl)ether
BRL
15
10
ug/L
287151 I
11/01/2019 15:04
YH
Bis(2-ethy1hexy1)phtha1ate
BRL
1.4
20
ug/L
287151 1
11/01/2019 15:04
YH
Butyl benzy] phthalate
BRL
0.84
10
ug/L
287151 l
11/01/2019 15:04
YH
Chlorobenzilate
BRL
0.57
10
ug/L
287151 1
11/01/2019 15:04
YH
Chrysene
BRL
0.93
10
ug/L
287151 1
11/01/2019 15:04
YH
Di-n-butyl phthalate
BRL
1 1
10
ug/L
287151 1
11/01/2019 15:04
YH
Di-n-octyl phthalate
BRL
1.6
10
ug/L
287151 1
11/01/2019 15:04
YH
Diallate
BRL
0.84
10
ug/L
287151 1
11/01/20191504
YH
Dibenz(a.h)anthracene
BRL
1.4
10
ug/L
287151 1
11/01/2019 15:04
YH
Dibenzofuran
BRL
Ll
10
ug/L
287151 1
11/01/2019 15:04
YH
Diethyl phthalate
2.3 J
0.82
10
ug/L
287151 1
11/01/2019 15:04
YH
Dimethoate
BRL
0.45
20
ug/L
287151 1
11/01/2019 15:04
YH
Dimethyl phthalate
BRL
1.0
10
ug/L
287151 1
11/01/2019 15:04
YH
Diphenylamine
BRL
10
10
ug/L
287151 1
11/01/2019 15:04
YH
Disulfoton
BRL
068
10
ug/L
287151 1
11/01/2019 15:04
YH
Ethyl methanesulfonate
BRL
1 1
20
ug/L
287151 1
11/01/2019 15:04
YH
Famphur
BRL
072
20
ug/L
287151 1
11/01/2019 15:04
YH
Fluoranthene
BRL
10
10
ug/L
287151 1
11/01/2019 15:04
YH
Fluorene
BRL
12
10
ug/L
287151 1
11/01/2019 15:04
YH
Hexachlorobenzene
BRL
1 1
10
ug/L
287151 1
11/01/2019 15:04
YH
Hexachlorobutadiene
BRL
12
10
ug/L
287151 1
11/01/2019 15:04
YH
Hexachlorocyclopentadiene
BRL
21
10
ug/L
287151 1
11/01/2019 15:04
YH
Hexachloroethane
BRL
13
10
ug/L
287151 1
11/01/2019 15:04
YH
Hexachloropropene
BRL
10
10
ug/L
287151 I
11/01/2019 15:04
YH
Qualifiers: * \'a Iue exceeds maxwnmm con lainmant Iescl
E Esumaled
aIuc abose
quanutation ranee
BRL Not Detected at NIDL
S Spike Recosery outside hnuts due to matrix
H Holding lures for preparation or analysis exceeded
- Greater than
Result salue
N Analyne not NEL AC cenificd
J Esumaled
value detected below Reporting Lmut
B Analvte detected in the associated method blank
< Less than
Result \clue
Page 1 Page 47 of 70

Analytical Environmental Services, Inc
Date: 4-Nov-19
Client:
Prism Laboratories
Client Sample ID:
MW-06
Lab Order
1910S56
Tag Number:
9100380-04
Project Name:
9100380
Collection Date:
10/23/2019 12:54:00 PM
Lab ID:
191 OS56-004A
Matrix:
Aqueous
Analyses Result Qual
MDL
ReportingUnits
Limit
BatchID DF
Date Analyzed Analyst
APPENDIXII-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
Ind eno(1,2,3-cd)pyrene
BRL
1.2
10
ug/L.
287151 1
11/01/2019 15:04
YH
Isodrin
BRL
1.2
20
ug/L
287151 1
11/01/2019 15:04
YH
Isophorone
BRL
0.86
10
ug/L
287151 1
11/01/2019 15:04
YH
Isosafrole
BRL
1.1
10
ug/L.
287151 1
11/01/2019 15:04
YH
Kepone
BRL
1A
50
ug/L
287151 1
11/01/2019 15:04
YH
Methapyrilene
BRL
6.4
20
ug/L
287151 1
11/01/2019 15:04
YH
Methyl methanesulfonate
BRL
1.3
10
ug/L
287151 1
11/01/2019 15:04
YH
Methyl parathion
BRL
0.85
10
ug/L
287151 1
11/01/2019 15:04
YH
N-Nitroso-di-n-butylamine
BRL
1,8
10
ug/L
287151 1
11/01/2019 15:04
YH
N-Nitrosodi-n-propylamine
BRL
0.82
10
ug/L
287151 1
11/01/2019 15:04
YH
N-Nitrosodiethylamine
BRL
1.2
20
ug/L
287151 1
11/01/2019 15:04
YH
N-Nitrosodimethylamine
BRL
1.7
20
ug/L
287151 1
11/01/2019 15:04
YH
N-Nitrosodiphenylamine
BRL
0.90
50
ug/L
287151 1
11/01/2019 15:04
YH
N-Nitrosomethylethylamine
BRL
1.00
10
ug/L
287151 1
11/01/2019 15:04
YH
N-Nitrosopiperidine
BRL
0.86
20
ug/L
287151 1
11/01/2019 15:04
YH
N-Nitrosopyrrolidine
BRL
1.2
40
ug/L
287151 1
11/01/2019 15:04
YH
Naphthalene
BRL
1.2
10
ug/L,
287151 1
11/01/2019 15:04
YH
Nitrobenzene
BRL
1.2
10
ug/L
287151 1
11/01/2019 15:04
YH
0,0,0-Triethylphosphorothioate
BRL
3.6
10
ug/L
287151 1
11/01/2019 15:04
YH
o-Toluidine
BRL
2.1
20
ug/L
287151 1
11/01/2019 15:04
YH
p-Dimethylaminoazobenzene
BRL
0.65
10
ug/L
287151 1
11/01/201915:04
YH
p-Phenylenediamine
BRL
55
500
ug/L
287151 1
11/01/2019 15:04
YH
Parathion
BRL
1.3
10
ug/L
287151 1
11/01/2019 15:04
YH
Pentachlorobenzene
BRL
0.94
10
ug/L
287151 1
11/01/2019 15:04
YH
Pen tachIoronitrobenzene
BRL
0,96
20
ug/L
287151 1
11/01/2019 15:04
YH
Pentachlorophenol
BRL
0,62
50
ug/L
287151 1
11/01/2019 15:04
YH
Phenacetin
BRL
0,85
20
ug/L
287151 1
11/01/2019 15:04
Y11
Phenanthrene
BRL
0.86
10
ug/L
287151 1
11/01/2019 15:04
YH
Phenol
BRL
0.77
10
ug/L
287151 1
11/01/2019 15:04
YH
Phorate
BRL
0.94
10
ug/L
287151 1
11/01/2019 15:04
YH
Pronamide
BRL
11
10
ug/L
287151 1
11/01/2019 15:04
YH
Pyrene
BRL
0.83
10
ug/L
287151 1
11/01/2019 15:04
YH
Safrole
BRL
12
20
ug/L
287151 1
11/01/2019 15:04
YH
Syni-Trinitrobenzene
BRL
0.98
10
trg/L
287151 1
11/01/2019 15:04
YH
Thionazin
BRL
0.81
20
ug/L
287151 1
11/01/20191504
YH
SUIT:2.4.6-Tribromophenol
80.8
0
47-127
%REC
287151 1
11/01/20191504
YH
SUIT: 2-Fluorobiphenyl
83.4
0
47.4-119
%REC
287151 1
11/01/2019 15:04
YH
Surr:2-Fluorophenol
33.3
0
26.2-120
°oREC
287151 1
11/01/2019 15:04
YH
Qualifiers: " Value esceeds maximum comainmam le%el
E Esumaled
gal tic abosc
quanl i la Lion range
BRL Nor Detected at hIDL
S Spike Recover)- outside hunt due to matrix
H Holding Lines for preparation or anal -is exceeded
- Greater than Result value
N Anahvre not NELAC cerii icd
i Estimated
iluc detected
below Reponmg Lunn
B Analcfe defected in the associated method blank
< Less than
Result -lue
Page 1 Page 48 of 70

Analytical Environmental Services, Inc
Date: 4-Nov-19
Client:
Prism Laboratories
Client Sample ID:
MW-06
Lab Order
191 OS56
Tag Number:
9100380-04
Project Name:
9100380
Collection Date:
10/23/2019 12:54:00 PM
Lab ID:
191 OS56-004A
Matrix:
Aqueous
Reporting
Analyses Result
y
Qual
MDL
Units BatchID
DF Date Analyzed
Analyst
Limit
APPENDIXII-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
Surr: 4-Terphenyl-d 14
53.1
0
45-133
%REC 287151
1 11/01/201915:04
YH
Surr: Nitrobenzene-d5
94
0
41.9-121
%REC 287151
1 11/01/2019 15:04
YH
Surr: Phenol-d5
20
0
17.8-120
%REC 287151
1 11/01/2019 15:04
YH
Qualifiers: * Value exceeds maximum comnmmant level
BRL Not Detected at MDL
H Holding tmres for preparation or analysts exceeded
N Anal,te not NELAC certified
B Analyte detected in the associated inedtod blank
E Estimated value above quantization range
S Spike Recovery outside limns due to maznx
> Greater than Result value
J Estimated value detected below Reporting Limn
< Less than Result value
Page 1 Page 49 of 70

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Page 52 of 70

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Page 54 of 70

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n to r, 7 rrl 7 O 0\ N G\ I, rr) O r '.I*
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Page 59 of 70

ACCESS
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
ATTENTION
Robbi Jones
PROJECTID
9100380
LABORATORY REPORT NUMBER
219103020
DATE
11/08/2019
Primary Data Review By
Authorized Signature
PLEASE NOTE:
Secondary Data Review By
Ashley B. Amick
Project Manager, Access Analytical, Inc.
[e-mail]
- Unless otherwise noted, all analysis on this report performed at Pace Analytical Gulf Coast, 7979
Innovation Park Dr., Baton Rouge, LA 70820.
Pace Gulf Coast is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab #
LA-01955, NELAP certified laboratory # 01955
Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a
representative of Pace Guld Coast serving clients in the SC/NC/GA areas. All questions regarding this report
should be directed to your local Access Analytical representative at 803.781.4243 or toll free at 888.315.4243
Lab Report#: 219103020
Page 1 of 11
Page 60 of 70

ace Analytical
LELAP CERTIFICATE NUMBER: 01955
DOD -FLAP ACCREDITATION NUMBER: 74960
ANALYTICAL RESULTS
Pace Analytical Gulf Coast
7979 Innovation Park Dr.
Baton Rouge, LA 70820
[phone]
Report Date 11/08/2019
Report pu 2„19103020
II 111111 111�1 III �11 �11 �11 111
Project 9100380
Deliver To Additional Recipients
Robbi Jones NONE
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
L 800-529-6364
1 S 0
PJLA�17025�
Testtog r��,,,�•r. �gDgFl�
Doi} EtAF
Lab Report#: 219103020
Page 61 of 70

/01
*gacmnalyhval
Report#: 219103020
Project ID: 9100380
Report Date: 11/08/2019
Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
retention period the samples will be disposed in accordance with Pace Gulf Coast's Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
ND Indicates the result was Not Detected at the specified reporting limit
NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed in the Field
DL Detection Limit
LOD Limit of Detection
LOCI Limit of Quantitation
RE Re -analysis
CIF HPLC or GC Confirmation
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or I Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
' Indicates a non -compliant or not applicable QC recovery or RPD — see narrative
E Organics - The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
L Reporting Limits adjusted to meet risk -based limit.
P RPD between primary and confirmation result is greater than 40
DL Diluted analysis —when appended to Client Sample ID
Sample receipt at Pace Gulf Coast is documented through the attached chain of custody. In accordance with NELAC, this report shall be
reproduced only in full and with the written permission of Pace Gulf Coast. The results contained within this report relate only to the samples
reported. The documented results are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if
applicable.
Authorized Signature
Pace Gulf Coast Report 219103020
Lab Report#: 219103020 Page 3 of 11
Page 62 of 70

seAnalytrcal /01 Report#: 219103020
Project ID: 9100380
Certifications
Report Date: 11/08/2019
Certification
Certification Number
DOD ELAP
74960
Alabama
01955
Arkansas
88-0655
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentucky
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
Mississippi
01955
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
Washington
C929
USDA Soil Permit
P330-16-00234
Lab Report#: 219103020 Pa e 4 of 11
Page 63 of 70

Report#: 219103020
2ceAnalyth2lceAnalyth2l'
Project ID: 9100380 Report Date: 11/08/2019
Case Narrative
Client: Access Analytical Report: 219103020
Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found for the analyzed sample(s).
Lab Report#: 219103020 Page 5 of 11
Page 64 of 70

LAB ID
Report#: 219103020
Project ID: 9100380
Report Date: 11/08/2019
Sample Summary
Client ID Matrix Collect Date/Time Receive Date/Time
21910302001
MW-02
Water
10/23/2019 09:26
10/30/2019 09:35
21910302002
MW-03
Water
10/23/2019 10:26
10/30/2019 09:35
21910302003
MW-05R
Water
10/23/2019 14:32
10/30/2019 09:35
21910302004
MW-06
Water
10/23/2019 12:54
10/30/2019 09:35
Lab Report#: 219103020 Page 6 of 11
Page 65 of 70

'?
f:In!A171ha, Ii
Report#: 219103020
Project ID: 9100380 Report Date: 11/08/2019
Summary of Compounds Detected
Collect Date 10/23/2019 09:26 LAB ID 21910302001
MW-02
Receive Date 10/30/2019 09:35 Matrix Water
SM 5310 B-2011
CAS# Parameter
C-012 Total Organic Carbon
Result
DL
I
LOQ
Units
5.24
0.300
2.00
mg/L
Collect Date 10/23/2019 10:26 LAB ID 21910302002
MW-03
Receive Date 10/30/2019 09:35 Matrix Water
SM 5310 B-2011
CAS#
Parameter
Result
DL
LOQ
Units
C-012
Total Organic Carbon
11.0
0.300
2.00
mg/L
Collect Date 10/23/2019 14:32
LAB ID
21910302003
MW-05R
Receive Date 10/30/2019 09:35
Matrix
Water
SM 5310 B-2011
CAS#
Parameter
Result
DL
LOQ
Units
C-012
Total Organic Carbon
18.0
0.300
2.00
mg/L
Collect Date 10/23/2019 12:54 LAB ID 21910302004
MW-06
Receive Date 10/30/2019 09:35 Matrix Water
SM 5310 B-2011
CAS# Parameter
C-012 Total Organic Carbon
Result DL LOQ Units
8.18 0.300 2.00 mg/L
Lab Report#: 219103020

Report#: 219103020
/ aceAnalytica!✓ Project ID: 9100380
Sample Results
Collect Date 10/23/2019 09:26
MW-02 Receive Date 10/30/2019 09:35
Report Date: 11/08/2019
LAB ID 21910302001
Matrix Water
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/07/2019 08:46 PLH 670778
CAS#
Parameter
Result
DL
LOQ
Units
C-012
Total Organic Carbon
5.24
0.300
2.00
mg/L
Collect Date 10/23/2019 10:26 LAB ID 21910302002
W-03
Receive Date 10/30/2019 09:35 Matrix Water
SM 5310 B-2011
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/07/2019 09:04 PLH 670778
CAS#
Parameter
Result
DL
LOQ
Units
C-012
Total Organic Carbon
11.0
0.300
2.00
mglL
Collect Date 10/23/2019 14:32 LAB ID 21910302003
MW-05R
Receive Date 10/30/2019 09:35 Matrix Water
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/07/2019 09:28 PLH 670778
CAS# Parameter
C-012 Total Organic Carbon
Result
DL
LOQ
Units
18.0
0.300
2.00
mg/L
Collect Date 10/23/2019 12:54 LAB ID 21910302004
W-06
Receive Date 10/30/2019 09:35 Matrix Water
SM 5310 B-2011
Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA 1 11/07/2019 21:19 PLH 670891
CAS# Parameter
C-012 Total Organic Carbon
Result DL LOQ Units
8.18 0.300 2.00 mg/L
Lab Report#: 219103020

Report#: 219103020
• aceAr�alv�;ral
Project ID: 9100380 Report Date: 11/08/2019
General Chemistry QC Summary
Analytical Batch Client ID
MB670778
LCS670778
670778 LAB ID
1979033
1979034
Sample Type
MB
LCS
Prep Date
NA
NA
Analysis Date
11/07/2019 03:16
11/07/2019 02:28
Matrix
Water
Water
SM 5310 B-2011
Units
mg/L
Spike
Result
%R
Control
Result
DL
Added
Limits%R
Total Organic Carbon I C-012
0.3000
0.3001
50.01
48.3197
1 90 - 110
Analytical Batch Client ID
MB670891
LCS670891
670891 LAB ID
1979630
1979631
Sample Type
MB
LCS
Prep Date
NA
NA
Analysis Date
11/07/2019 20:07
11/07/2019 19:15
Matrix
Water
Water
SM 5310 B-2011
Units
mg/L
Spike
Result
%R
Control
Result
DL
Added
Limits%R
Total Organic Carbon C-012
0.3000
0.300
50.01
51.2
102
90 - 110
Lab Report#: 219103020 Page 9 of 11
Page 68 of 70

r
DO
CT
.-O
CD
o
w
cD
o
Client ID: 4565 - Access Analytical
;� t C• G. 03020
PM: DLH
P I S!
1 [
Y"1 Envi cnmental 51 lat ons
G A. 14C /- 1 v rl ..1 „ J J
_._.cal
SUBCONTRACT ORDER
(l r7 ^ D
(J`.�l�l {•n
Certification: ty�L3C� USACE`
Prism Laboratories, Inc. ,} S' SC Other
5�5-314-1 � �1 C
9100350 NIA�
SEVDIN'G LABORATORY:
RECEIVPNG L.180RA'1YJ11Y:
Prism Laboratories, Inc.
PaccAnalyncal Gulf'Coost
1'. O, no\ 2'0543
10731 Coursey Blvd
Charintic, NC 2S224-0543
Baton Rougc, LA 70916
Phone:[phone]
Phone :[phone]
Fa\:704-5-,5-0409
Fns:[phone]
Project �Tanagn•: Robbi A. Joncs
Analysis Due Expires Laboratory ID Comments
Sampk 1D: 9300380-01 Water Sampled: 10/23/1909:26 p) 1. ~U L
TOC (Sub) I IP0119 09:26 S%f 531 OB
CnnrnL:ers SuppGcJ:
tici-
mt�_a3
�a-
$mnpin ID: 91003SO-02
W.I., Sampled: 10/1-3/19 10,26
,'I'OC (Sun)
11/20/19 10:26
SM 5310E
'omaincnr 5::ppficd:
�
m Uj =o5,
Sample TD: 9100330-03
water Sampled: 10/23/19 14:32
TOC (Sub)
I I110i 19 1432
SRt 511 OB
'nn:aim•,; Supplier.!:
� T- W-� 0 (-
Sample ID: 910O3SIHld
SVater Sampled: 10/23/79 7L•s4
I
TOC (Sub)
1100!19 12:54
Sbl 5310E
'anrn:nccc SuypJin,'.
it
2 I
IC
Datc itr; 11 c:, Rt Uatc
Rcleaad y DateAce i. f,
Rcicascd By i:o:c Rcct•r.•cd By ( Dam
I:cl,_•is�•1 Wy fair Reenvt.� R5' I):n_
Page 1 0l 1
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| Page 7od7 1

LP R I S M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Anchor QEA of North Carolina, PLLC
Alec Macbeth
231 Haywood Street
Asheville, NC 28801
NC Certification No. 402 Case Narrative
NC Drinking Water Cert No. 37735 11/15/19 14:28
SC Certification No. 99012
Project: Jackson Cty Landfill 2019 Fall Samplling
Project No.: 50-02
Lab Submittal Date: 10/25/2019
Prism Work Order: 9100391
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
Method 8270 analysis was subcontracted to AES. TOC analysis was subcontracted to Pace Analytical
Gulf Coast. Laboratory reports are attached.
Prism Summary of Detections does not include subcontracted data.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
HT Sample received and analyzed outside of the hold time.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 47

Sample Receipt Summary
FullAnalytical
S
Jfipxk/L
s
EnviService ronmental Solutions
I M
11/15/2019
BORATORIES, INC.
Prism Work Order: 9100391
Client Sample ID Lab Sample ID Matrix
Date/Time Sampled Date/Time Received
MW-01 9100391-01 Water
10/24/19 12:13 10/25/19 8:55
TB-03 9100391-02 Water
10/24/19 0:00 10/25/19 8:55
Samples were received in good condition at 2.7 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 2 of 47

/r P R I S M Full -Service Analytical s
Environmental Solutions
LABORATOR
Summary of Detections
11 /15/201 S
Prism Work Order: 9100391
Prism ID
Client ID
Parameter
Method
Result
Units
9100391-01
MW-01
Chloride
9056A
1500
ug/L
9100391-01
MW-01
Biochemical Oxygen Demand
SM5210 B
8400
ug/L
9100391-01
MW-01
Chemical Oxygen Demand
SM5220 D
53000
ug/L
9100391-01
MW-01
Ferrous Iron
SM3500-Fe D
34000
HT
ug/L
9100391-01
MW-01
Sulfide
SM4500-S F
16000
ug/L
9100391-01
MW-01
Total Alkalinity to pH 4.5
SM2320 B
91000
ug/L
9100391-01
MW-01
Barium
6020B
120
ug/L
9100391-01
MW-01
Cobalt
6020B
150
ug/L
9100391-01
MW-01
Nickel
6020B
17
ug/L
9100391-01
MW-01
Zinc
6020B
22
ug/L
9100391-01
MW-01
1,1-Dichloroethane
8260D
2.3
ug/L
9100391-01
MW-01
1,4-Dichlorobenzene
8260D
8.0
ug/L
9100391-01
MW-01
Acetone
8260D
31
ug/L
9100391-01
MW-01
Benzene
8260D
1.6
ug/L
9100391-01
MW-01
Chlorobenzene
8260D
1.8
ug/L
9100391-01
MW-01
cis-1,2-Dichloroethylene
8260D
4.7
ug/L
9100391-01
MW-01
m,p-Xylenes
8260D
1.0
ug/L
9100391-01
MW-01
Naphthalene
8260D
1.5
ug/L
9100391-01
MW-01
o-Xylene
8260D
0.40
J
ug/L
9100391-01
MW-01
Tetrachloroethylene
8260D
0.37
J
ug/L
9100391-01
MW-01
Trichloroethylene
8260D
0.47
J
ug/L
9100391-01
MW-01
Xylenes, total
8260D
1.4
J
ug/L
9100391-02
TB-03
Acetone
8260D
2.6
J
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 3 of 47

%j6P R I S M Full -Service Analytical
Environmental Solutions
LABORATORIES, INC.
Laboratory Report
11 /15/2019
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No.: 50-02
Sample Matrix: Water
Client Sample ID: MW-01
Prism Sample ID: 9100391-01
Prism Work Order: 9100391
Time Collected: 10/24/19 12:13
Time Submitted: 10/25/19 08:55
Parameter
Result
Units
SWSL
Report
Limit
MDL
Dilution
Factor
Method
Analysis Analyst
Date/Time
Batch
ID
Anions by Ion Chromatography
Chloride
1500
ug/L
NE
1000
380
1
9056A
10/25/19 18:44BMS
P9JO477
Nitrate as N
<54
ug/L
10000
200
54
1
9056A
10/25/19 18:44BMS
P9JO477
Sulfate
<480
ug/L
250000
2000
480
1
9056A
10/25/19 18:44BMS
P9JO477
General Chemistry Parameters
Biochemical Oxygen Demand
8400
ug/L
NE
2000
210
1
SM5210 B
10/25/19 17:34CBM
P9JO484
Chemical Oxygen Demand
53000
ug/L
NE
50000
10000
1
SM5220 D
10/28/19 11:36SLS
P9J0486
Ferrous Iron
34000 HT
ug/L
NE
5000
1300
1
SM3500-Fe D
10/25/15 15:OOBMS
P9JO473
Sulfide
16000
ug/L
1000
2000
830
1
SM4500-S F
10/29/19 9:45 CBM
P9JO504
Total Alkalinity to pH 4.5
91000
ug/L
NE
5000
770
1
SM2320 B
10/31/19 10:28CLB
P9J0537
Total Metals
Mercury
<0.034
ug/L
0.2
0.20
0.034
1
7470A
10/29/19 16:51JAB
P9JO493
Antimony
<0.93
ug/L
6
3.0
0.93
1
6020B
10/30/19 16:36MMR
P9JO521
Arsenic
<0.34
ug/L
10
1.0
0.34
1
6020B
10/30/19 16:36MMR
P9JO521
Barium
120
ug/L
100
10
3.2
1
6020B
10/30/19 16:36MMR
P9JO521
Beryllium
<0.30
ug/L
1
1.0
0.30
1
6020B
10/30/19 16:36MMR
P9JO521
Cadmium
<0.22
ug/L
1
1.0
0.22
1
6020B
10/30/19 16:36MMR
P9JO521
Chromium
<0.90
ug/L
10
3.0
0.90
1
6020B
10/30/19 16:36MMR
P9JO521
Cobalt
150
ug/L
10
2.0
0.70
1
6020B
10/30/19 16:36MMR
P9JO521
Copper
<4.7
ug/L
10
10
4.7
1
6020B
10/30/19 16:36MMR
P9JO521
Lead
<0.44
ug/L
10
1.0
0.44
1
6020B
10/30/19 16:36MMR
P9J0521
Nickel
17
ug/L
50
3.0
0.83
1
6020B
10/30/19 16:36MMR
129J0521
Selenium
<0.98
ug/L
10
5.0
0.98
1
6020B
10/30/19 16:36MMR
P9JO521
Silver
<0.34
ug/L
10
1.0
0.34
1
6020B
10/30/19 16:36MMR
P9JO521
Thallium
<0.84
ug/L
5.5
2.0
0.84
1
6020B
10/30/19 16:36MMR
P9JO521
Tin
<1.9
ug/L
100
5.0
1.9
1
6020B
10/30/19 16:36MMR
P9JO521
Vanadium
<1.5
ug/L
25
5.0
1.5
1
6020B
10/30/19 16:36MMR
P9JO521
Zinc
22
ug/L
10
20
10
1
6020B
10/30/19 16:36MMR
P9JO521
Volatile Organic Compounds by GC/MS
1, 1, 1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19 10:50 KDM
P9KO048
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19 10:50 KDM
P91<0048
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
11/2/19 10:50 KDM
P9KO048
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
11/2/19 10:50 KDM
P91<0048
1,1-Dichloroethane
2.3
ug/L
5
0.50
0.29
1
8260D
11/2/19 10:50 KDM
P9KO048
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19 10:50 KDM
P9KO048
1, 1 -Dichloropropylene
<0.37
ug/L
5
0.50
0.37
1
8260D
11/2/19 10:50 KDM
P91<0048
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
11/2/19 10:50 KDM
P9KO048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 47

Full -Service Analytical &
P R S M Environmental Solutions
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No.: 50-02
Sample Matrix: Water
Laboratory Report
11/15/2019
Client Sample ID: MW-01
Prism Sample ID: 9100391-01
Prism Work Order: 9100391
Time Collected: 10/24/19 12:13
Time Submitted: 10/25/19 08:55
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,2,4-Trichlorobenzene
<0.44
ug/L
10
1.0
0.44
1
8260D
11/2/19 10:50 KDM
P9K0048
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
11/2/19 10:50 KDM
P9K0048
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
11/2/19 10:50 KDM
P9K0048
1,2-Dichlorobenzene
<0.28
ug/L
5
0.50
0.28
1
8260D
11/2/19 10:50 KDM
P9K0048
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19 10:50 KDM
P9K0048
1,2-Dichloropropane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19 10:50 KDM
P9K0048
1,3-Dichlorobenzene
<0.40
ug/L
5
0.50
0.40
1
8260D
11/2/19 10:50 KDM
P9K0048
1,3-Dichloropropane
<0.40
ug/L
1
0.50
0.40
1
8260D
11/2/19 10:50 KDM
P9K0048
1,4-Dichlorobenzene
8.0
ug/L
1
0.50
0.42
1
8260D
11/2/19 10:50 KDM
P9K0048
2,2-Dichloropropane
<0.26
ug/L
15
2.0
0.26
1
8260D
11/2/19 10:50 KDM
P91<0048
Acetone
31
ug/L
100
5.0
0.70
1
8260D
11/2/19 10:50 KDM
P9K0048
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
11/2/19 10:50 KDM
P9K0048
Acrolein
<1.2
ug/L
53
20
1.2
1
8260D
11/2/19 10:50 KDM
P91<0048
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
11/2/19 10:50 KDM
P9K0048
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
11/2/19 10:50 KDM
P91<0048
Benzene
1.6
ug/L
1
0.50
0.34
1
8260D
11/2/19 10:50 KDM
P9K0048
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
11/2/19 10:50 KDM
P9K0048
Bromodichloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19 10:50 KDM
P9K0048
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
11/2/19 10:50 KDM
P9K0048
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
11/2/19 10:50 KDM
P9K0048
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
11/2/19 10:50 KDM
P9K0048
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
11/2/19 10:50 KDM
P9K0048
Chlorobenzene
1.8
ug/L
3
0.50
0.34
1
8260D
11/2/19 10:50 KDM
P91<0048
Chloroethane
<0.43
ug/L
10
0.50
0.43
1
8260D
11/2/19 10:50 KDM
P9K0048
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
11/2/19 10:50 KDM
P9K0048
Chloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19 10:50 KDM
P9K0048
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
11/2/19 10:50 KDM
P9K0048
cis-1,2-Dichloroethylene
4.7
ug/L
2
0.50
0.40
1
8260D
11/2/19 10:50 KDM
P91<0048
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
11/2/19 10:50 KDM
P9K0048
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
11/2/19 10:50 KDM
P9K0048
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
11/2/19 10:50 KDM
P9K0048
Dichlorodifluoromethane
<0.47
ug/L
5
5.0
0.47
1
8260D
11/2/19 10:50 KDM
P9K0048
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
11/2/19 10:50 KDM
P9K0048
Ethylbenzene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19 10:50 KDM
P9K0048
Hexachlorobutadiene
<0.24
ug/L
10
2.0
0.24
1
8260D
11/2/19 10:50 KDM
P9K0048
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
11/2/19 10:50 KDM
P9K0048
m,p-Xylenes
1.0
ug/L
NE
1.0
0.73
1
8260D
11/2/19 10:50 KDM
P9K0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 47

Laboratory Report
Full -Service Analytical &
P R S M
Environmental Solutions
LABORATORIES INC.
11/15/2019
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2019
Fall
Client
Sample ID:
MW-01
Attn: Alec Macbeth
Samplling
Prism
Sample ID:
9100391-01
231 Haywood Street
Project No.:
50-02
Prism
Work Order:
9100391
Asheville, NC 28801
Sample Matrix:
Water
Time
Collected: 10/24/19 12:13
Time
Submitted: 10/25/19
08:55
Parameter
Result Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
11/2/19 10:50 KDM
P91<0048
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
11/2/19 10:50 KDM
P9K0048
Methyl Ethyl Ketone (2-Butanone)
<0.78
ug/L
100
5.0
0.78
1
8260D
11/2/19 10:50 KDM
P91<0048
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
11/2/19 10:50 KDM
P9K0048
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
11/2/19 10:50 KDM
P91<0048
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
11/2/19 10:50 KDM
P9K0048
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1
8260D
11/2/19 10:50 KDM
P91<0048
Naphthalene
1.5
ug/L
10
1.0
0.45
1
8260D
11/2/19 10:50 KDM
P91<0048
o-Xylene
0.40
J ug/L
NE
0.50
0.40
1
8260D
11/2/19 10:50 KDM
P9K0048
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
11/2/19 10:50 KDM
P91<0048
Styrene
<0.26
ug/L
1
0.50
0.26
1
8260D
11/2/19 10:50 KDM
P9K0048
Tetrachloroethylene
0.37
J ug/L
1
0.50
0.31
1
8260D
11/2/19 10:50 KDM
P91<0048
Tetrahydrofuran
<0.68
ug/L
NE
10
0.68
1
8260D
11/2/19 10:50 KDM
P9K0048
Toluene
<0.35
ug/L
1
0.50
0.35
1
8260D
11/2/19 10:50 KDM
P91<0048
trans- 1,2-Dichloroethylene
<0,27
ug/L
5
0.50
0.27
1
8260D
11/2/19 10:50 KDM
P9K0048
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1
8260D
11/2/19 10:50 KDM
P91<0048
trans- 1,4-Dich loro-2-butene
<0,22
ug/L
100
10
0.22
1
8260D
11/2/19 10:50 KDM
P9K0048
Trichloroethylene
0.47
J ug/L
1
0.50
0.46
1
8260D
11/2/19 10:50 KDM
P91<0048
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1
8260D
11/2/19 10:50 KDM
P9K0048
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1
8260D
11/2/19 10:50 KDM
P91<0048
Vinyl chloride
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19 10:50 KDM
P9K0048
Xylenes, total
1.4
J ug/L
5
1.5
1.1
1
8260D
11/2/19 10:50 KDM
P91<0048
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
100 % 80-124
Dibromofluoromethane
100 % 75-129
Toluene-d8
99 % 77-123
Volatile Organic Compounds by GUMS SIM
1,4-Dioxane
<0.14
ug/L
10
2.0
0.14
1
8260D SIM
10/25/19 15:50TBL
P9J0421
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 47

�Full-Service Analytical s
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
11 /15/2019
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Jackson Cty Landfill 2019 Fall
Samplling
Project No.: 50-02
Sample Matrix: Water
Client Sample ID: TB-03
Prism Sample ID: 9100391-02
Prism Work Order: 9100391
Time Collected: 10/24/19 00:00
Time Submitted: 10/25/19 08:55
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GUMS
1, 1, 1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19
3:52
KDM
P91<0048
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
3:52
KDM
P9K0048
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
11/2/19
3:52
KDM
P91<0048
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
11/2/19
3:52
KDM
P9K0048
1,1-Dichloroethane
<0.29
ug/L
5
0.50
0.29
1
8260D
11/2/19
3:52
KDM
P91<0048
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
11/2/19
3:52
KDM
P9K0048
1, 1 -Dichloropropylene
<0.37
ug/L
5
0.50
0.37
1
8260D
11/2/19
3:52
KDM
P91<0048
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
11/2/19
3:52
KDM
P9K0048
1,2,4-Trichlorobenzene
<0.44
ug/L
10
1.0
0.44
1
8260D
11/2/19
3:52
KDM
P91<0048
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
11/2/19
3:52
KDM
P9K0048
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
11/2/19
3:52
KDM
P91<0048
1,2-Dichlorobenzene
<0.28
ug/L
5
0.50
0.28
1
8260D
11/2/19
3:52
KDM
P9K0048
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19
3:52
KDM
P91<0048
1,2-Dichloropropane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
3:52
KDM
P9K0048
1,3-Dichlorobenzene
<0.40
ug/L
5
0.50
0.40
1
8260D
11/2/19
3:52
KDM
P91<0048
1,3-Dichloropropane
<0.40
ug/L
1
0.50
0.40
1
8260D
11/2/19
3:52
KDM
P9K0048
1,4-Dichlorobenzene
<0.42
ug/L
1
0.50
0.42
1
8260D
11/2/19
3:52
KDM
P91<0048
2,2-Dichloropropane
<0.26
ug/L
15
2.0
0.26
1
8260D
11/2/19
3:52
KDM
P9K0048
Acetone
2.6 1
ug/L
100
5.0
0.70
1
8260D
11/2/19
3:52
KDM
P9K0048
Acetonitrile
<3.0
ug/L
55
10
3.0
1
8260D
11/2/19
3:52
KDM
P9K0048
Acrolein
<1.2
ug/L
53
20
1.2
1
8260D
11/2/19
3:52
KDM
P91<0048
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
11/2/19
3:52
KDM
P9K0048
Allyl Chloride (3-Chloropropylene)
<0.75
ug/L
10
10
0.75
1
8260D
11/2/19
3:52
KDM
P91<0048
Benzene
<0.34
ug/L
1
0.50
0.34
1
8260D
11/2/19
3:52
KDM
P9K0048
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
11/2/19
3:52
KDM
P91<0048
Bromodichloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
3:52
KDM
P9K0048
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
11/2/19
3:52
KDM
P91<0048
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
11/2/19
3:52
KDM
P9K0048
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
11/2/19
3:52
KDM
P91<0048
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
11/2/19
3:52
KDM
P9K0048
Chlorobenzene
<0.34
ug/L
3
0.50
0.34
1
8260D
11/2/19
3:52
KDM
P91<0048
Chloroethane
<0.43
ug/L
10
0.50
0.43
1
8260D
11/2/19
3:52
KDM
P9K0048
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
11/2/19
3:52
KDM
P91<0048
Chloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
11/2/19
3:52
KDM
P9K0048
Chloroprene
<0.86
ug/L
20
10
0.86
1
8260D
11/2/19
3:52
KDM
P91<0048
cis- 1,2-Dichloroethylene
<0.40
ug/L
2
0.50
0.40
1
8260D
11/2/19
3:52
KDM
P9K0048
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 47

Laboratory Report
Full -Service Analytical &
P R S M
Environmental Solutions
LABORATORIES INC.
11/15/2019
Anchor QEA of North Carolina, PLLC
Project: Jackson Cty Landfill 2019
Fall
Client
Sample ID:
TB-03
Attn: Alec Macbeth
Samplling
Prism
Sample ID:
9100391-02
231 Haywood Street
Project No.:
50-02
Prism
Work Order:
9100391
Asheville, NC 28801
Sample Matrix:
Water
Time
Collected: 10/24/19 00:00
Time
Submitted: 10/25/19
08:55
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
11/2/19
3:52
KDM
P91<0048
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
11/2/19
3:52
KDM
P9K0048
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
11/2/19
3:52
KDM
P91<0048
Dichlorodifluoromethane
<0.47
ug/L
5
5.0
0.47
1
8260D
11/2/19
3:52
KDM
P9K0048
Ethyl Methacrylate
<0.26
ug/L
10
10
0.26
1
8260D
11/2/19
3:52
KDM
P91<0048
Ethylbenzene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
3:52
KDM
P9K0048
Hexachlorobutadiene
<0.24
ug/L
10
2.0
0.24
1
8260D
11/2/19
3:52
KDM
P91<0048
Isobutyl alcohol
<20
ug/L
100
50
20
1
8260D
11/2/19
3:52
KDM
P9K0048
m,p-Xylenes
<0.73
ug/L
NE
1.0
0.73
1
8260D
11/2/19
3:52
KDM
P91<0048
Methacrylonitrile
<0.57
ug/L
100
10
0.57
1
8260D
11/2/19
3:52
KDM
P9K0048
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
11/2/19
3:52
KDM
P91<0048
Methyl Ethyl Ketone (2-Butanone)
<0,78
ug/L
100
5.0
0.78
1
8260D
11/2/19
3:52
KDM
P9K0048
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
11/2/19
3:52
KDM
P91<0048
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
11/2/19
3:52
KDM
P9K0048
Methyl Methacrylate
<0.27
ug/L
30
10
0.27
1
8260D
11/2/19
3:52
KDM
P91<0048
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1
8260D
11/2/19
3:52
KDM
P9K0048
Naphthalene
<0.45
ug/L
10
1.0
0.45
1
8260D
11/2/19
3:52
KDM
P91<0048
o-Xylene
<0.40
ug/L
NE
0.50
0.40
1
8260D
11/2/19
3:52
KDM
P9K0048
Propionitrile (Ethyl Cyanide)
<2.1
ug/L
150
10
2.1
1
8260D
11/2/19
3:52
KDM
P91<0048
Styrene
<0.26
ug/L
1
0.50
0.26
1
8260D
11/2/19
3:52
KDM
P9K0048
Tetrachloroethylene
<0.31
ug/L
1
0.50
0.31
1
8260D
11/2/19
3:52
KDM
P91<0048
Tetrahydrofuran
<0.68
ug/L
NE
10
0.68
1
8260D
11/2/19
3:52
KDM
P9K0048
Toluene
<0.35
ug/L
1
0.50
0.35
1
8260D
11/2/19
3:52
KDM
P91<0048
trans- 1,2-Dichloroethylene
<0.27
ug/L
5
0.50
0.27
1
8260D
11/2/19
3:52
KDM
P9K0048
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1
8260D
11/2/19
3:52
KDM
P91<0048
trans- 1,4-Dich loro-2-butene
<0.22
ug/L
100
10
0.22
1
8260D
11/2/19
3:52
KDM
P9K0048
Trichloroethylene
<0.46
ug/L
1
0.50
0.46
1
8260D
11/2/19
3:52
KDM
P91<0048
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1
8260D
11/2/19
3:52
KDM
P9K0048
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1
8260D
11/2/19
3:52
KDM
P91<0048
Vinyl chloride
<0.41
ug/L
1
0.50
0.41
1
8260D
11/2/19
3:52
KDM
P9K0048
Xylenes, total
<1.1
ug/L
5
1.5
1.1
1
8260D
11/2/19
3:52
KDM
P91<0048
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
100 %
80-124
Dibromofluoromethane
100 %
75-129
Toluene-d8
100 %
77-123
Volatile Organic Compounds by GUMS SIM
1,4-Dioxane
<0.14
ug/L
10
2.0
0.14
1
8260D SIM
10/25/19 13:44TBL
P9J0421
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 47

,ot P R I IS M Full -Service Analytical s
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
11/15/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall
Attn: Alec Macbeth Samplling
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Prism Work Order: 9100391
Time Submitted: 10/25/2019 8:55:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P91K0048 - 5030B
Blank (P9K0048-BLK1)
Prepared: 11/01/19 Analyzed: 11/02/19
1,1,1,2-Tetrachloroethane
BRL
0.50
ug/L
1,1,1-Trichloroethane
BRL
0.50
ug/L
1,1,2,2-Tetrachloroethane
BRL
0.50
ug/L
1,1,2-Trichloroethane
BRL
0.50
ug/L
1,1-Dichloroethane
BRL
0.50
ug/L
1,1-Dichloroethylene
BRL
0.50
ug/L
1,1-Dichloropropylene
BRL
0.50
ug/L
1,2,3-Trichloropropane
BRL
1.0
ug/L
1,2,4-Trichlorobenzene
BRL
1.0
ug/L
1,2-Dibromo-3-chloropropane
BRL
2.0
ug/L
1,2-Dibromoethane
BRL
0.50
ug/L
1,2-Dichlorobenzene
BRL
0.50
ug/L
1,2-Dichloroethane
BRL
0.50
ug/L
1,2-Dichloropropane
BRL
0.50
ug/L
1,3-Dichlorobenzene
BRL
0.50
ug/L
1,3-Dichloropropane
BRL
0.50
ug/L
1,4-Dichlorobenzene
BRL
0.50
ug/L
2,2-Dichloropropane
BRL
2.0
ug/L
Acetone
BRL
5.0
ug/L
Acetonitrile
BRL
10
ug/L
Acrolein
BRL
20
ug/L
Acrylonitrile
BRL
20
ug/L
Allyl Chloride (3-Chloropropylene)
BRL
10
ug/L
Benzene
BRL
0.50
ug/L
Bromochloromethane
BRL
2.0
ug/L
Bromodichloromethane
BRL
0.50
ug/L
Bromoform
BRL
1.0
ug/L
Bromomethane
BRL
1.0
ug/L
Carbon disulfide
BRL
5.0
ug/L
Carbon Tetrachloride
BRL
2.0
ug/L
Chlorobenzene
BRL
0.50
ug/L
Chloroethane
BRL
0.50
ug/L
Chloroform
BRL
0.50
ug/L
Chloromethane
BRL
0.50
ug/L
Chloroprene
BRL
10
ug/L
cis-1,2-Dichloroethylene
BRL
0.50
ug/L
cis-1,3-Dichloropropylene
BRL
0.50
ug/L
Dibromochloromethane
BRL
0.50
ug/L
Dibromomethane
BRL
2.0
ug/L
Dichlorodifluoromethane
BRL
5.0
ug/L
Ethyl Methacrylate
BRL
10
ug/L
Ethylbenzene
BRL
0.50
ug/L
Hexachlorobutadiene
BRL
2.0
ug/L
Isobutyl alcohol
BRL
50
ug/L
m,p-Xylenes
BRL
1.0
ug/L
Methacrylonitrile
BRL
10
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 9 of 47

P R I S M Full -Service Analytical s
Environmental Solutions
LABCFATCRIES, NC.
Level II QC Report
11/15/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Prism Work Order: 9100391
Attn: Alec Macbeth Samplling Time Submitted: 10/25/2019 8:55:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P911<0048 - 5030B
Blank (P9K0048-BLK1)
Prepared: 11/01/19 Analyzed: 11/02/19
Methyl Butyl Ketone (2-Hexanone)
BRL
5.0
ug/L
Methyl Ethyl Ketone (2-Butanone)
BRL
5.0
ug/L
Methyl Iodide
BRL
5.0
ug/L
Methyl Isobutyl Ketone
BRL
5.0
ug/L
Methyl Methacrylate
BRL
10
ug/L
Methylene Chloride
BRL
1.0
ug/L
Naphthalene
BRL
1.0
ug/L
o-Xylene
BRL
0.50
ug/L
Propionitrile (Ethyl Cyanide)
BRL
10
ug/L
Styrene
BRL
0.50
ug/L
Tetrachloroethylene
BRL
0.50
ug/L
Tetrahydrofuran
BRL
10
ug/L
Toluene
BRL
0.50
ug/L
trans- 1,2-Dichloroethylene
BRL
0.50
ug/L
trans- 1,3-Dichloropropylene
BRL
0.50
ug/L
trans-1,4-Dichloro-2-butene
BRL
10
ug/L
Trichloroethylene
BRL
0.50
ug/L
Trichlorofluoromethane
BRL
0.50
ug/L
Vinyl acetate
BRL
2.0
ug/L
Vinyl chloride
BRL
0.50
ug/L
Xylenes, total
BRL
1.5
ug/L
Surrogate:4-Bromofluorobenzene
49.4
ug/L
50.00
99
80-124
Surrogate: Dibromofluoromethane
49.0
ug/L
50.00
98
75-129
Surrogate: Toluene-d8
50.2
ug/L
50.00
100
77-123
LCS (P9KO048-BS1)
Prepared: 11/01/19 Analyzed:
11/02/19
1,1,1,2-Tetrachloroethane
20.6
0.50
ug/L
20.00
103
79-134
1,1,1-Trichloroethane
21.2
0.50
ug/L
20.00
106
75-136
1,1,2,2-Tetrachloroethane
21.0
0.50
ug/L
20.00
105
62-127
1,1,2-Trichloroethane
20.8
0.50
ug/L
20.00
104
70-140
1,1-Dichloroethane
20.6
0.50
ug/L
20.00
103
78-130
1,1-Dichloroethylene
21.2
0.50
ug/L
20.00
106
70-154
1, 1 -Dichloropropylene
22.6
0.50
ug/L
20.00
113
71-136
1,2,3-Trichloropropane
20.5
1.0
ug/L
20.00
102
71-127
1,2,4-Trichlorobenzene
21.3
1.0
ug/L
20.00
107
66-139
1,2-Dibromo-3-chloropropane
21.1
2.0
ug/L
20.00
106
63-134
1,2-Dibromoethane
21.2
0.50
ug/L
20.00
106
77-135
1,2-Dichlorobenzene
20.8
0.50
ug/L
20.00
104
78-128
1,2-Dichloroethane
19.6
0.50
ug/L
20.00
98
68-131
1,2-Dichloropropane
20.7
0.50
ug/L
20.00
103
77-130
1,3-Dichlorobenzene
20.3
0.50
ug/L
20.00
102
77-125
1,3-Dichloropropane
21.3
0.50
ug/L
20.00
106
76-132
1,4-Dichlorobenzene
20.3
0.50
ug/L
20.00
102
75-126
2,2-Dichloropropane
20.3
2.0
ug/L
20.00
102
29-149
Acetone
40.2
5.0
ug/L
40.00
101
40-166
Acetonitrile
21.3
10
ug/L
20.00
106
70-130
Acrolein
41.6
20
ug/L
40.00
104
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 47

P R I S M Full-ServiceAnalytical s
Environmental Solutions
LABCFATCRIES, NC.
Level II QC Report
11/15/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall
Attn: Alec Macbeth Samplling
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Prism Work Order: 9100391
Time Submitted: 10/25/2019 8:55:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P911<0048 - 5030B
LCS (P91<0048-13SI)
Prepared: 11/01/19 Analyzed: 11/02/19
Acrylonitrile
37.3
20
ug/L
40.00
93
81-127
Allyl Chloride (3-Chloropropylene)
18.8
10
ug/L
20.00
94
70-130
Benzene
20.3
0.50
ug/L
20.00
101
77-128
Bromochloromethane
20.8
2.0
ug/L
20.00
104
78-135
Bromodichloromethane
20.9
0.50
ug/L
20.00
104
76-138
Bromoform
21.9
1.0
ug/L
20.00
109
71-135
Bromomethane
28.7
1.0
ug/L
20.00
143
41-168
Carbon disulfide
22.2
5.0
ug/L
20.00
111
59-135
Carbon Tetrachloride
21.8
2.0
ug/L
20.00
109
72-142
Chlorobenzene
20.0
0.50
ug/L
20.00
100
78-119
Chloroethane
20.4
0.50
ug/L
20.00
102
57-142
Chloroform
20.1
0.50
ug/L
20.00
101
77-130
Chloromethane
23.9
0.50
ug/L
20.00
120
47-145
Chloroprene
21.0
10
ug/L
20.00
105
70-130
cis-1,2-Dichloroethylene
19.4
0.50
ug/L
20.00
97
76-141
cis-1,3-Dichloropropylene
22.2
0.50
ug/L
20.00
111
65-140
Dibromochloromethane
21.5
0.50
ug/L
20.00
107
75-134
Dibromomethane
20.7
2.0
ug/L
20.00
104
76-138
Dichlorodifluoromethane
26.4
5.0
ug/L
20.00
132
28-163
Ethyl Methacrylate
20.8
10
ug/L
20.00
104
70-130
Ethylbenzene
20.8
0.50
ug/L
20.00
104
80-127
Hexachlorobutadiene
21.9
2.0
ug/L
20.00
110
61-134
Isobutyl alcohol
20.0
50
ug/L
20.00
100
70-130 J
m,p-Xylenes
42.6
1.0
ug/L
40.00
107
77-133
Methacrylonitrile
20.0
10
ug/L
20.00
100
70-130
Methyl Butyl Ketone (2-Hexanone)
21.5
5.0
ug/L
20.00
108
64-137
Methyl Ethyl Ketone (2-Butanone)
19.8
5.0
ug/L
20.00
99
71-134
Methyl Iodide
21.2
5.0
ug/L
20.00
106
70-130
Methyl Isobutyl Ketone
20.7
5.0
ug/L
20.00
104
69-134
Methyl Methacrylate
20.9
10
ug/L
20.00
104
70-130
Methylene Chloride
18.7
1.0
ug/L
20.00
93
73-131
Naphthalene
21.8
1.0
ug/L
20.00
109
64-136
o-Xylene
20.9
0.50
ug/L
20.00
105
78-128
Propionitrile (Ethyl Cyanide)
20.3
10
ug/L
20.00
101
70-130
Styrene
22.0
0.50
ug/L
20.00
110
78-129
Tetrachloroethylene
21.9
0.50
ug/L
20.00
110
80-129
Tetrahydrofuran
19.4
10
ug/L
20.00
97
70-130
Toluene
20.6
0.50
ug/L
20.00
103
76-131
trans- 1,2-Dichloroethylene
20.0
0.50
ug/L
20.00
100
76-135
trans- 1,3-Dichloropropylene
21.8
0.50
ug/L
20.00
109
67-140
trans-1,4-Dichloro-2-butene
20.0
10
ug/L
20.00
100
70-130
Trichloroethylene
20.4
0.50
ug/L
20.00
102
77-133
Trichlorofluoromethane
23.6
0.50
ug/L
20.00
118
62-148
Vinyl acetate
21.4
2.0
ug/L
20.00
107
34-167
Vinyl chloride
22.6
0.50
ug/L
20.00
113
57-141
Xylenes, total
63.6
1.5
ug/L
60.00
106
77-133
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 47

P R I S M Full -Service Analytical s
Environmental Solutions
LABCFATCRIES, NC.
Level II QC Report
11/15/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Prism Work Order: 9100391
Attn: Alec Macbeth Samplling Time Submitted: 10/25/2019 8:55:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P91<0048 - 5030B
LCS (P9K0048-BSI)
Prepared: 11/01/19 Analyzed: 11/02/19
Surrogate:4-Bromofluorobenzene
50.1
ug/L
50.00
100
80-124
Surrogate: Dibromofluoromethane
49.0
ug/L
50.00
98
75-129
Surrogate: Toluene-d8
50.6
ug/L
50.00
101
77-123
LCS Dup (P9KO048-BSD1)
Prepared: 11/01/19 Analyzed:
11/02/19
1,1,1,2-Tetrachloroethane
20.4
0.50
ug/L
20.00
102
79-134
1
20
1,1,1-Trichloroethane
20.7
0.50
ug/L
20.00
103
75-136
3
20
1,1,2,2-Tetrachloroethane
21.4
0.50
ug/L
20.00
107
62-127
2
20
1,1,2-Trichloroethane
20.6
0.50
ug/L
20.00
103
70-140
0.9
20
1,1-Dichloroethane
20.2
0.50
ug/L
20.00
101
78-130
2
20
1,1-Dichloroethylene
20.6
0.50
ug/L
20.00
103
70-154
3
20
1, 1 -Dichloropropylene
21.7
0.50
ug/L
20.00
108
71-136
4
20
1,2,3-Trichloropropane
21.4
1.0
ug/L
20.00
107
71-127
4
20
1,2,4-Trichlorobenzene
21.0
1.0
ug/L
20.00
105
66-139
2
20
1,2-Dibromo-3-chloropropane
22.4
2.0
ug/L
20.00
112
63-134
6
20
1,2-Dibromoethane
21.3
0.50
ug/L
20.00
107
77-135
0.6
20
1,2-Dichlorobenzene
20.8
0.50
ug/L
20.00
104
78-128
0.05
20
1,2-Dichloroethane
19.2
0.50
ug/L
20.00
96
68-131
2
20
1,2-Dichloropropane
20.4
0.50
ug/L
20.00
102
77-130
1
20
1,3-Dichlorobenzene
20.0
0.50
ug/L
20.00
100
77-125
1
20
1,3-Dichloropropane
21.2
0.50
ug/L
20.00
106
76-132
0.4
20
1,4-Dichlorobenzene
20.0
0.50
ug/L
20.00
100
75-126
2
20
2,2-Dichloropropane
19.6
2.0
ug/L
20.00
98
29-149
4
20
Acetone
42.3
5.0
ug/L
40.00
106
40-166
5
20
Acetonitrile
21.5
10
ug/L
20.00
107
70-130
1
20
Acrolein
43.1
20
ug/L
40.00
108
70-130
4
20
Acrylonitrile
39.4
20
ug/L
40.00
98
81-127
5
20
Allyl Chloride (3-Chloropropylene)
18.5
10
ug/L
20.00
93
70-130
2
20
Benzene
19.9
0.50
ug/L
20.00
100
77-128
2
20
Bromochloromethane
20.6
2.0
ug/L
20.00
103
78-135
1
20
Bromodichloromethane
20.7
0.50
ug/L
20.00
103
76-138
1
20
Bromoform
22.4
1.0
ug/L
20.00
112
71-135
2
20
Bromomethane
26.6
1.0
ug/L
20.00
133
41-168
8
20
Carbon disulfide
21.4
5.0
ug/L
20.00
107
59-135
4
20
Carbon Tetrachloride
21.1
2.0
ug/L
20.00
105
72-142
4
20
Chlorobenzene
19.6
0.50
ug/L
20.00
98
78-119
2
20
Chloroethane
19.7
0.50
ug/L
20.00
99
57-142
3
20
Chloroform
20.0
0.50
ug/L
20.00
100
77-130
0.7
20
Chloromethane
25.1
0.50
ug/L
20.00
125
47-145
5
20
Chloroprene
20.3
10
ug/L
20.00
102
70-130
3
20
cis-1,2-Dichloroethylene
19.0
0.50
ug/L
20.00
95
76-141
2
20
cis-1,3-Dichloropropylene
21.8
0.50
ug/L
20.00
109
65-140
2
20
Dibromochloromethane
21.3
0.50
ug/L
20.00
107
75-134
0.7
20
Dibromomethane
20.7
2.0
ug/L
20.00
103
76-138
0.1
20
Dichlorodifluoromethane
24.6
5.0
ug/L
20.00
123
28-163
7
20
Ethyl Methacrylate
21.1
10
ug/L
20.00
105
70-130
1
20
Ethylbenzene
20.4
0.50
ug/L
20.00
102
80-127
2
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 47

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/15/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Prism Work Order: 9100391
Attn: Alec Macbeth Samplling Time Submitted: 10/25/2019 8:55:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9KO048 - 5030B
LCS Dup (P9K0048-BSD1)
Prepared: 11/01/19 Analyzed: 11/02/19
Hexachlorobutadiene
20.8
2.0
ug/L
20.00
104
61-134
5
20
Isobutyl alcohol
20.7
50
ug/L
20.00
103
70-130
4
20 1
m,p-Xylenes
41.8
1.0
ug/L
40.00
104
77-133
2
20
Methacrylonitrile
20.7
10
ug/L
20.00
104
70-130
3
20
Methyl Butyl Ketone (2-Hexanone)
22.6
5.0
ug/L
20.00
113
64-137
5
20
Methyl Ethyl Ketone (2-Butanone)
21.0
5.0
ug/L
20.00
105
71-134
5
20
Methyl Iodide
20.2
5.0
ug/L
20.00
101
70-130
5
20
Methyl Isobutyl Ketone
21.6
5.0
ug/L
20.00
108
69-134
4
20
Methyl Methacrylate
21.4
10
ug/L
20.00
107
70-130
2
20
Methylene Chloride
18.6
1.0
ug/L
20.00
93
73-131
0.2
20
Naphthalene
22.3
1.0
ug/L
20.00
ill
64-136
2
20
o-Xylene
20.4
0.50
ug/L
20.00
102
78-128
2
20
Propionitrile (Ethyl Cyanide)
21.0
10
ug/L
20.00
105
70-130
3
20
Styrene
21.5
0.50
ug/L
20.00
108
78-129
2
20
Tetrachloroethylene
21.1
0.50
ug/L
20.00
106
80-129
4
20
Tetrahydrofuran
20.9
10
ug/L
20.00
104
70-130
7
20
Toluene
20.1
0.50
ug/L
20.00
101
76-131
2
20
trans-1,2-Dichloroethylene
19.5
0.50
ug/L
20.00
98
76-135
3
20
trans-1,3-Dichloropropylene
21.8
0.50
ug/L
20.00
109
67-140
0.05
20
trans-1,4-Dichloro-2-butene
20.6
10
ug/L
20.00
103
70-130
3
20
Trichloroethylene
19.6
0.50
ug/L
20.00
98
77-133
4
20
Trichlorofluoromethane
22.8
0.50
ug/L
20.00
114
62-148
3
20
Vinyl acetate
21.8
2.0
ug/L
20.00
109
34-167
2
20
Vinyl chloride
21.7
0.50
ug/L
20.00
109
57-141
4
20
Xylenes, total
62.2
1.5
ug/L
60.00
104
77-133
2
20
Surrogate:4-Bromofluorobenzene
49.9
ug/L
50.00
100
80-124
Surrogate: Dibromofluoromethane
49.9
ug/L
50.00
100
75-129
Surrogate: Toluene-d8
50.5
ug/L
50.00
101
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/15/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall
Attn: Alec Macbeth Samplling
231 Haywood Street Project No: 50-02
Prism Work Order: 9100391
Time Submitted: 10/25/2019 8:55:OOAM
Asheville, NC 28801
Volatile Organic Compounds by GC/MS SIM - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9JO421 - 5030B
Blank (P9J0421-BLK1) Prepared & Analyzed: 10/25/19
1,4-Dioxane BRL 2.0 ug/L
LCS (P9J0421-BS1) Prepared &Analyzed: 10/25/19
1,4-Dioxane 43.0 2.0 ug/L 50.00 86 55-145
LCS Dup (P9J0421-BSD1) Prepared &Analyzed: 10/25/19
1,4-Dioxane 43.9 2.0 ug/L 50.00 88 55-145 2 30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 47

Level II QC Report
P R I IS M Full -Service Analytical 11/15/19
Environmental Solutions
. LABORATORIES, INC.
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Prism Work Order: 9100391
Attn: Alec Macbeth Samplling Time Submitted: 10/25/2019 8:55:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9J0493 - 7470A
Blank (P9J0493-BLK1) Prepared & Analyzed: 10/29/19
Mercury BRL 0.20 ug/L
LCS (P9J0493-BS1) Prepared &Analyzed: 10/29/19
Mercury 10.0 0.20 ug/L 9.375 107 80-120
Batch P9J0521 - 3005A
Blank (P9J0521-BLK1)
Prepared & Analyzed: 10/30/19
Antimony
BRL
3.0
ug/L
Arsenic
BRL
1.0
ug/L
Barium
BRL
10
ug/L
Beryllium
BRL
1.0
ug/L
Cadmium
BRL
1.0
ug/L
Chromium
BRL
3.0
ug/L
Cobalt
BRL
2.0
ug/L
Copper
BRL
10
ug/L
Lead
BRL
1.0
ug/L
Nickel
BRL
3.0
ug/L
Selenium
BRL
5.0
ug/L
Silver
BRL
1.0
ug/L
Thallium
BRL
2.0
ug/L
Tin
BRL
5.0
ug/L
Vanadium
BRL
5.0
ug/L
Zinc
BRL
20
ug/L
LCS (P9J0521-BS1)
Prepared &Analyzed: 10/30/19
Antimony
106
3.0
ug/L
100.0 106
80-120
Arsenic
99.5
1.0
ug/L
100.0 99
80-120
Barium
99.5
10
ug/L
100.0 100
80-120
Beryllium
102
1.0
ug/L
100.0 102
80-120
Cadmium
102
1.0
ug/L
100.0 102
80-120
Chromium
105
3.0
ug/L
100.0 105
80-120
Cobalt
105
2.0
ug/L
100.0 105
80-120
Copper
104
10
ug/L
100.0 104
80-120
Lead
102
1.0
ug/L
100.0 102
80-120
Nickel
104
3.0
ug/L
100.0 104
80-120
Selenium
105
5.0
ug/L
100.0 105
80-120
Silver
102
1.0
ug/L
100.0 102
80-120
Thallium
96.6
2.0
ug/L
100.0 97
80-120
Tin
102
5.0
ug/L
100.0 102
80-120
Vanadium
104
5.0
ug/L
100.0 104
80-120
Zinc
106
20
ug/L
100.0 106
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 47

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/15/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall
Attn: Alec Macbeth Samplling
231 Haywood Street Project No: 50-02
Asheville, NC 28801
Anions by Ion Chromatography - Quality Control
Prism Work Order: 9100391
Time Submitted: 10/25/2019 8:55:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9JO477 - NO PREP
Blank (P9J0477-BLK1)
Prepared & Analyzed: 10/25/19
Chloride
BRL
1000
ug/L
Nitrate as N
BRL
200
ug/L
Sulfate
BRL
2000
ug/L
LCS (P9J0477-BS1)
Prepared &Analyzed: 10/25/19
Chloride
41300
1000
ug/L
40000 103
80-120
Nitrate as N
3970
210
ug/L
4000 99
80-120
Sulfate
42000
2100
ug/L
40000 105
80-120
Matrix Spike (P9J0477-MS1)
Source: 9100391-01
Prepared & Analyzed: 10/25/19
Chloride
42200
1000
ug/L
40000 1510 102
80-120
Nitrate as N
3930
210
ug/L
4000 BRL 98
80-120
Sulfate
41100
2100
ug/L
40000 BRL 103
80-120
Matrix Spike Dup (P9J0477-MSD1)
Source: 9100391-01
Prepared & Analyzed: 10/25/19
Chloride
42900
1000
ug/L
40000 1510 103
80-120 2 15
Nitrate as N
4010
210
ug/L
4000 BRL 100
80-120 2 15
Sulfate
42100
2100
ug/L
40000 BRL 105
80-120 2 15
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 of 47

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/15/19
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall
Attn: Alec Macbeth Samplling
231 Haywood Street Project No: 50-02
Asheville, NC 28801
General Chemistry Parameters - Quality Control
Prism Work Order: 9100391
Time Submitted: 10/25/2019 8:55:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9J0473 - NO PREP
Blank (P9J0473-BLK1) Prepared & Analyzed: 10/24/19
Ferrous Iron BRL 200 ug/L
LCS (P9J0473-BS1) Prepared &Analyzed: 10/24/19
Ferrous Iron 2020 200 ug/L 2000 101 90-110
Batch P9J0484 - NO PREP
Blank (P9J0484-BLK1)
Biochemical Oxygen Demand
LCS (P9J0484-BS1)
Biochemical Oxygen Demand
Batch P9JO486 - NO PREP
Prepared & Analyzed: 10/25/19
BRL 2000 ug/L
Prepared & Analyzed: 10/25/19
190000 2000 ug/L 198000 94 84.6-115.4
Blank (P9JO486-BLK1) Prepared & Analyzed: 10/28/19
Chemical Oxygen Demand BRL 50000 ug/L
LCS (P9J0486-BS1) Prepared &Analyzed: 10/28/19
Chemical Oxygen Demand 519000 50000 ug/L 500000 104 90-110
Batch P9J0504 - SM4500-S C
Blank (P9J0504-BLK1) Prepared & Analyzed: 10/29/19
Sulfide BRL 2000 ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Level II QC Report
P R I IS M Full -Service Analytical 11/15/19
Environmental Solutions
. LABORATORIES, INC.
Anchor QEA of North Carolina, PLLC Project: Jackson Cty Landfill 2019 Fall Prism Work Order: 9100391
Attn: Alec Macbeth Samplling Time Submitted: 10/25/2019 8:55:OOAM
231 Haywood Street Project No: 50-02
Asheville, NC 28801
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9JO504 - SM4500-S C
LCS (P9J0504-BS1)
Prepared &Analyzed: 10/29/19
Sulfide
9700
2000 ug/L
10000 97 70-130
Batch P9JO537 - NO PREP
Blank (P9J0537-BLK1)
Prepared &Analyzed: 10/31/19
Total Alkalinity to pH 4.5
BRL
5000 ug/L
LCS (P9J0537-BS1)
Prepared &Analyzed: 10/31/19
Total Alkalinity to pH 4.5
250000
5000 ug/L
250000 100 90-110
Sample Extraction
Data
Prep Method: SM4500-S C
Lab Number
Batch
Initial
Final
Date/Time
9100391-01
P9J0504
200 mL
200 mL
10/29/19 9:45
Prep Method: 3005A
Lab Number
Batch
Initial
Final
Date/Time
9100391-01
P9J0521
50 mL
50 mL
10/30/19 7:46
Prep Method: 7470A
Lab Number
Batch
Initial
Final
Date/Time
9100391-01
P9J0493
20 mL
30 mL
10/29/19 9:18
Prep Method: 5030E
Lab Number
Batch
Initial
Final
Date/Time
9100391-01
P91<0048
10 mL
10 mL
11/01/19 8:01
9100391-02
P9K0048
10 mL
10 mL
11/01/19 8:01
Prep Method: 5030E
Lab Number
Batch
Initial
Final
Date/Time
9100391-01
P9J0421
5 mL
5 mL
10/25/19 9:00
9100391-02
P9J0421
5 mL
5 mL
10/25/19 9:00
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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Subcontracted Analyses
The following analyses were subcontracted to Analytical Environmental Services, Inc.
Lab Number Analysis
9100391-01 8270 (App. 11)
The following analyses were subcontracted to Pace Analytical Gulf Coast
Lab Number Analysis
9100391-01 TOC (Sub)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 47

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C7
ACCESS
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte NC 282240543
ATTENTION
Robbi A. Jones
PROJECT ID
9100391
LABORATORY REPORT NUMBER
191OS57
DATE
November 04, 2019
Primary Data Review By Secondary Data Review By
Ashley Amick
Chris Pafford
Project Manager, Access Analytical
Project Manager, AES [e-mail]
PLEASE NOTE:
Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc),
3080 Presidential Drive, Atlanta, GA 30340.
AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582,
NELAP certified laboratory # E87582
- AIHA-LAP,LLC Laboratory 1D:100671 for Industrial Hygiene samples (Organics, Metals, PCM Asbestos,
Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal)
Direct Examination.
- Local support services for this project are provided by Access Analytical; Inc. Access Analytical is a
representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed
to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243
Page I Page 21 of 47

lull-
/ orica Analytical 'PRlSM Envirorontal Solutions ns
� t:.t+mtaroaira me
SENDING LAROVA7'ORY:
' Prism Laboratories, Inc.
P. O. Box 240543
Charlotte, NC 29224-0543
Phone: [phone]
Fax:[phone]
Project Manager: Robbi A. Jones
t
SUBCONTRACT ORDER
Certificatit+n: �4ELAC USACL
Prism Laboratories, Inc. NCB SC_ Other
9100391 N/A
RECEIVING LA l3RATORY-
Analytical Environmental Services, Inc.
3090 Presidential Parkway
Atlanta, GA 30340
Phone :[phone]
Fax: NA
Analysis Due Expires A�LaWratMIID Comments
Sample ID: 9100391-01 Water Sampled: 1012411912:13 r ►7 i -
8270 (App. 11) 10/31/19 12:13 8270 App 11 List
Cnntnine'-S& I
nod; � �—
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4
Released ray Date Rt:¢e o•td 13 A_. �� D: tc
Released By Date Received By I-i D;ttc.
I'tdr-,5cd Dy Datc Received By Umc
Page 1 of 1
Page Page 22 of 47

Analytical Environmental Services, Inc
Date: 4-Nov-19
Client:
Prism Laboratories
Client Sample ID:
MW-01
Lab Order
191OS57
Tag Number:
9100391-01
Project Name:
9100391
Collection Date:
10/24/2019 12:13:00 PM
Lab ID:
191OS57-OOIA
Matrix:
Aqueous
Analyses Result
y Qual
MDL
Reporting
Limit
Units
BatchID DF
DatcAnalyzed Analyst
APPENDIXII-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
1,2.4,5-Tetrachlorobenzene
BRL
1.3
10
ug/L
287151 1
11/01/2019 15:31
YH
1,2,4-Trichlorobenzene
BRL
1.4
10
ug/L
287151 1
11/01/2019 15:31
YH
1,2-Dichlorobenzene
BRL
1.2
10
ug/L
287151 1
11/01/2019 15:31
YH
1.3-Dichlorobenzene
BRL
13
10
ug/L
287151 1
11/01/2019 15:31
YH
1,3-Dinitrobenzene
BRL
1.1
20
ug/L
287151 1
11/01/2019 15:31
YH
1,4-Dichlorobenzene
6.6 J
1.4
10
ug/L
287151 1
11/01/201915:31
YH
1,4-Napthoquinone
BRL
1.7
10
ug/L
287151 1
11/01/2019 15:31
YH
1-Naphthylamine
BRL
3.0
10
ug/L
287151 1.
11/01/2019 15:31
YH
2,3,4.6-Tetra chi orophenol
BRL
1.1
10
ug/L
287151 1
11/01/2019 15:31
YH
2,4,5-Trichlorophenol
BRL
0.99
10
ug/L
287151 t
11/01/2019 15:31
YH
2,4,6-Trichlorophenol
BRL
1.3
10
ug/L
287151 I
11/01/2019 15:31
YH
2,4-Dichlorophenol
BRL
1.0
10
ug/L
287151 1
11/01/2019 15:31
YH
2,4-Dimethylphenol
BRL
0.72
50
ug/L
287151 1
11/01/2019 15:31
YH
2.4-Dinitrophenol
BRL
5.5
50
ug/L
287151 1
11/01/2019 15:31
YH
2,4-Dinitrotoluene
BRL
1.1
10
ug/L
287151 1
11/01/2019 15:31
YH
2,6-Dichlorophenol
BRL
0.95
10
ug/L
287151 1
11/01/2019 15:31
YH
2,6-Dinitrotoluene
BRL
13
10
ug/L
287151 1
11/01/2019 15:31
YH
2-Acetylaminofluorene
BRL
11
20
ug/L
287151 1
11/01/2019 15:31
YH
2-Chloronaphthalene
BRL
1.8
10
ug/L
287151 1
11/01/2019 15:31
YH
2-Chlorophenol
BRL
1.2
10
ug/L
287151 1
11/01/201915-31
YH
2-M ethyl naphthalene
BRL
1.2
10
ug/L
287151 1
11/01/2019 15:31
YH
2-Methylphenol
BRL
13
10
ug/L
287151 1
11/01/2019 15:31
YH
2-Naphthylamine
BRL
17
10
ug/L
287151 1
11/01/2019 15:31
YH
2-Nitroaniline
BRL
19
50
ug/L
287151 1
11/01/2019 15:31
YH
2-Nitrophenol
BRL
16
10
ug/L
287151 1
11/01/2019 15:31
YH
3.3'-Dichlorobenzidine
BRL
1.1
20
ug/L
287151 1
11/01/2019 15:31
YH
3.3'-Dimethylbenzidine
BRL
5.4
20
ug/L
287151 1
11/01/2019 15:31
YH
3,4-Methylphenol
BRL
2.3
10
uw/L
287151 1
11/01/2019 15:31
YH
3-Methylcholanthrene
BRL
1.1
10
ttg/L
287151 1
11/01/2019 15:31
YH
3-Nitroaniline
BRL
12
50
ug/L
287151 1
11/01/201915:31
YH
4,6-Dinitro-2-methylphenol
BRL
1.3
50
ug/L
287151 1
11/01/2019 15:31
YH
4-Aminobiphenyl
BRL
24
20
ug/L
287131 1
11/01/2019 15:31
YH
4-Bromophenyl phenyl ether
BRL
1 4
10
ug/L
287151 1
11/01/2019 15:31
YH
4-Chloro-3-methylphenol
BRL
081
20
ug/L
287151 1
11/01/2019 15:31
YH
4-Chloroaniline
BRL
21
20
ug/L
287151 1
11/01/2019 15:31
YH
4-Chlorophenyl phenyl ether
BRL
1 3
10
ug/L
287151 1
11/01/2019 15:31
YH
4-Nitroaniline
BRL
13
20
u4A
287151 1
11/01/2019 15:31
YH
4-Nitrophenol
BRL
077
50
ug/L
287151 [
11/01/201915:31
YH
Q1404rws: ' Value esceeds masmnmt contaminant level
E Estnnated
value abose
quanniauon range
BRL Not Deiccted at VIDL
S Spike Recovery outside hnnts due to mains
H Holding times for preparation or onalysis exceeded
- Grcviter than
Result Value
N Anahte not NELAC cernfed
1 Estima led
NaILie detected below Reporu ne Li not
Analrte detected in the associated method blank
K Less than
Result %clue
Page I Page 23 of 47

Analytical Environmental Services, Inc
Date: 4-Nov-19
Client:
Prism Laboratories
Client Sample ID:
MW-01
Lab Order
1910S57
Tag Number:
9100391-01
Project Name:
9100391
Collection Date:
10/24/2019 12:13:00 PM
Lab ID:
1910S57-OOIA
Matrix:
Aqueous
Analyses Result Qual
MDL
ReportingUnits
Limit
BatchID DF Date Analyzed
Analyst
APPENDIXII-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
5-Nitro-o-toluidine
BRL
0.66
10
ug/L
287151 1
11/01/201915:31
YH
7,12-Dimethylbenz(a)anthracene
BRL
1.4
10
ug/L
287151 1
11/01/2019 15:31
YH
Acenaphthene
BRL
1.1
10
ug/L
287151 1
11/01/2019 15:31
YH
Acenaphthylene
BRL
1.1
10
ug/L
287151 1
11/01/2019 15:31
YH
Acetophenone
BRL
2.1
10
ug/L
287151 1
11/01/2019 15:31
YH
Anthracene
BRL
0.82
10
ug/L
287151 1
11/01/2019 15:31
YH
Benz(a)anthracene
BRL
0.96
10
ug/L
287151 1
11/01/2019 15:31
YH
Benzo(a)pyrene
BRL
0.96
10
ug/L
287151 1
11/01/2019 15:31
YH
Benzo(b)fluoranthene
BRL
1.5
10
ug/L
287151 1
11/01/2019 15:31
YH
Benzo(g,h,i)perylene
BRL
1.3
10
ug/L
287151 1
11/01/2019 15:31
YH
Benzo(k)fluoranthene
BRL
1.5
10
ug/L
287151 1
11/01/2019 15:31
YH
Benzyl alcohol
BRL
1.4
20
ug/L
287151 1
11/01/2019 15:31
YH
Bis(2-chloroethoxy)methane
BRL
1.1
10
ug/L
287151 1
11/01/2019 15:31
YH
Bis(2-chloroethyl)ether
BRL
1.2
10
ug/L
287151 1
11/01/2019 15:31
YH
Bis(2-chloroisopropyl)ether
BRL
1.5
10
ug/L
287151 1
11/01/2019 15:31
YH
Bis(2-ethylhexyl)phthalate
1.4 1
1.4
20
ug/L
287151 1
11/01/2019 15:31
YH
Butyl benzyl phthalate
BRL
0.84
10
ug/L
287151 1
11/01/2019 15:31
YH
Chlorobenzilate
BRL
0.57
10
ug/L
287151 1
11/01/2019 15:31
YH
Chrysene
BRL
093
10
ug/L
287151 1
11/01/2019 15:31
YH
Di-n-butyl phthalate
BRL
1 1
10
ug/L
287151 1
11/01/2019 15:31
YH
Di-n-octyl phthalate
BRL
1 6
10
ug/L
287151 1
11/01/2019 15:31
YH
Diallate
BRL
0.84
10
ug/L
287151 1
11/01/2019 15:31
YH
Dibenz(a,h)anthracene
BRL
14
10
ug/L
287151 1
11/01/2019 15:31
YH
Dibenzofuran
BRL
1.1
10
ug/L
287151 1
11/01/2019 15:31
YH
Diethyl phthalate
BRL
0.82
10
ug/L
287151 1
11/01/2019 15:31
YH
Dimethoate
BRL
0.45
20
ug/L
287151 1
11/01/2019 15:31
YH
Dimethyl phthalate
BRL
1.0
10
ug/L
287151 1
11/01/2019 15:31
YH
Diphenylamine
BRL
1.0
10
ug/L
287151 1
11/01/2019 15:31
YH
Disulfoton
BRL
0,68
10
ug/L
287151 1
11/01/2019 15:31
YH
Ethyl methanesulfonate
BRL
1 1
20
ug/L
287151 1
11/01/2019 15:31
YH
Famphur
BRL
0.72
20
ug/L
287151 1
11/01/201915:31
YH
Fluoranthene
BRL
10
10
ug/L
287151 1
11/01/2019 15:31
YH
Fluorene
BRL
12
10
uLA
287151 1
11/01/2019 15:31
YH
Hexachlorobenzene
BRL
1 1
10
ug/L
287151 1
11/01/2019 15:31
YH
Hexachlorobutadiene
BRL
12
10
ug/L
287151 1
11/01/201915:31
YH
Hexachlorocyclopentadiene
BRL
2.1
10
ug/L
287151 l
11/01/201915.31
YH
Hexachloroethane
BRL
13
10
LILA
287151 1
11/01/2019 15:31
YH
Hexachloropropene
BRL
10
10
ug/L
287151 1
11/01/201915.31
YH
Qnalifiers: • Value exceeds maximum contaminant le-1
E Eslimaled
4alue above
quantitution range
BRL Not netecled at NIO L
S Spike Recos m outside Innns due to mmnx
H Holding nines for preparation or analvsts exceeded
> Greater than Result %clue
N Ana lyre not NELAC certified
J Estimated
salue detected
below Reporung Limn
B Analyse detected in the associated method blank
- Less than
Result salue
Page I Page 24 of 47

Analytical Environmental Services, Inc
Date: 4-Nov-19
Client:
Prism Laboratories
Client Sample 1D:
MW-01
Lab Order
1910S57
Tag Number:
9100391-01
Project Name:
9100391
Collection Date:
10/24/2019 12:13:00 PM
Lab ID:
1910S57-OOIA
Matrix:
Aqueous
Analyses Result Qua[
MDL
ReportingUnits
Limit
BatchID DF Date Analyzed
Analyst
APPENDIXII-SEMIVOLATILE ORGANICS
SW8270E
(SW3510C)
Indeno(1,2,3-cd)pyrene
BRL
1.2
10
ug/L
287151 1
11/01/2019 15:31
YH
Isodrin
BRL
1.2
20
ug/L
287151 1
11/01/2019 15:31
YH
Isophorone
BRL
0.86
10
ug/L.
287151 1
11/01/2019 15:31
YH
Isosafrole
BRL
1.1
10
ug/L
287151 1
11/01/2019 15:31
YH
Kepone
BRL
1.4
50
ug/L
287151 1
11/01/2019 15:31
YH
Methapyrilene
BRL
6.4
20
ug/L.
287151 1
11/01/2019 15:31
YH
Methyl methanesulfonate
BRL
1.3
10
ug/L
287151 1
11/01/2019 15:31
YH
Methyl parathion
BRL
0.85
10
ug/L.
287151 1
11/01/2019 15:31
YH
N-Nitroso-di-n-butylamine
BRL
1.8
10
ug/L
287151 1
11/01/2019 15:31
YH
N-Nitrosodi-n-propylamine
BRL
0.82
10
ug/L
287151 1
11/01/2019 15:31
YH
N-Nitrosodiethylamine
BRL
1.2
20
ug/L
287151 1
11/01/2019 15:31
YH
N-Nitrosodimethylamine
BRL
1.7
20
ug/L
287151 1
11/01/2019 15:31
YH
N-Nitrosodiphenylamine
BRL
0.90
50
ug/L
287151 1
11/01/2019 15:31
YH
N-Nitrosomethylethylamine
BRL
1.00
10
ug/L
287151 1
11/01/2019 15:31
YH
N-Nitrosopiperidine
BRL
0.86
20
ug/L
287151 1
11/01/2019 15:31
YH
N-Nitrosopyrrolidine
BRL
1.2
40
ug/L
287151 1
11/01/2019 15:31
YH
Naphthalene
1.2 J
1.2
10
ug/L
287151 1
11/01/2019 15:31
YH
Nitrobenzene
BRL
1.2
10
ug/L
287151 1
11/01/2019 15:31
YH
0,0,0-Triethylphosphorothioate
BRL
3.6
10
ug/L
287151 1
11/01/2019 15:31
YH
o-Toluidine
BRL
2.1
20
ug/L
287151 l
11/01/2019 15:31
YH
p-Dimethylaminoazobenzene
BRL
0.65
10
ug/L
287151 l
11/01/2019 15:31
YH
p-Phenylenediamine
BRL
55
500
ug/L
287151 1
11/01/2019 15:31
YH
Parathion
BRL
1.3
10
ug/L
287151 1
11/01/2019 15:31
YH
Pentachlorobenzene
BRL
0.94
10
ug/L
287151 1
11/01/2019 15:31
YH
Pentachloronitrobenzene
BRL
0.96
20
ug/L
287151 1
11/01/2019 15:31
YH
Pentachlorophenol
BRL
0.62
50
ug/L
287151 1
11/01/2019 15:31
YH
Phenacetin
BRL
0.85
20
ug/L
287151 1
11/01/2019 15:31
YH
Phenanthrene
BRL
0.86
10
ug/L
287151 1.
11/01/2019 15:31
YH
Phenol
BRL
0.77
10
ug/L
287151 1
11/01/2019 15:31
YH
Phorate
BRL
0.94
10
ug/L
287151 l
11/01/2019 15:31
YH
Pronamide
BRL
I 1
10
ug/L
287151 t
11/01/2019 15:31
YH
Pyrene
BRL
0.83
10
ug/L
287151 1
11/01/2019 15:31
YH
Safrole
BRL
12
20
ug/L
287151 1
11/01/2019 15:31
YH
Sym-Trinitrobenzene
BRL
0.98
10
ug/L
287151 1
11/01/2019 15:31
YH
Thionazin
BRL
0.81
20
ug/L
287151 1
11/01/2019 15:31
YH
Surr:2.4.6-Tribromophenol
84.7
0
47-127
%REC
287151 1
11/01/2019 15:31
YH
Sun:2-Fluorobiphenyl
84.2
0
47.4-119
%REC
287151 1
11/01/2019 15:31
YH
SUIT: 2-Fluorophenol
34.4
0
26.2-120
%REC
287151 1
11/01/2019 15:31
YH
QuiliGees: Value exceeds maximum commnunant level
E Estimated
value abose
quanWauon ranee
BRL Not Detected at hIDL
S Spike Recovery owside lunns due io mains
H Holdme umes for preparation or analysis exceeded
> Grcner dtan
Result Value
N Anal_ to not NELAC -ufied
J Estnnated
value detected below Reporun_ Lunn
B Analyse detected m the associated method blank
< Less than
Resuh value
Page I Page 25 of 47

Analytical Environmental Services, Inc
Client: Prism Laboratories
Lab Order 1910S57
Project Name: 9100391
Lab ID: 1910S57-OOIA
Analyses
Date: 4-Nov-19
Client Sample 1D:
MW-01
Tag Number:
9100391-01
Collection Date:
10/24/2019 12:13:00 PM
Matrix:
Aqueous
Result Reporting
Qual MDL Limit Units BatchID DF Date Analyzed Analyst
APPENDIXII-SEMIVOLATILE ORGANICS SW8270E (SW3510C)
Surr: 4-Terphenyl-d 14 43.8 S 0 45-133 %REC 287151 1 11/01/201915:31 YH
Surr: Nitrobenzene-d5 99 0 41.9-121 %REC 287151 1 11/01/2019 15:31 YH
Surr: Phenol-d5 19.5 0 17.8-120 %REC 287151 1 11/01/2019 15:31 YH
Qualifies: " Value exceeds maximum contaminant level
nRL Not Detected at NIDL
H Holding times for preparation or analysis exceeded
N Analvte not NELAC certified
D Analvte detected m the associated method blank
E Estimated value above quanulauon range
S Spike Recovery outside limits due to matrix
> Greater than Result value
J Estimated value detected below Reporting Limit
< Less than Result alue
Page q Page 26 of 47

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Page 36 of 47

ACCESS
ANALYTICAL, INC.
ANALYTICAL REPORT
CLIENT
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
ATTENTION
Robbi Jones
PROJECTID
9100391
LABORATORY REPORT NUMBER
219103021
DATE
11 /08/2019
Primary Data Review By
Authorized Signature
PLEASE NOTE:
Secondary Data Review By
Ashley 8. Amrck
Project Manager, Access Analytical, Inc.
[e-mail]
Unless otherwise noted, all analysis on this report performed at Pace Analytical Gulf Coast, 7979
Innovation Park Dr., Baton Rouge, LA 70820.
- Pace Gulf Coast is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab #
LA-01955, NELAP certified laboratory # 01955
- Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a
representative of Pace Guld Coast serving clients in the SC/NC/GA areas All questions regarding this report
should be directed to your local Access Analytical representative at 803.781.4243 or toll free at 888.315.4243.
Lab Report#: 219103021
Page 37 of 47

(� aceAnalytical
LELAP CERTIFICATE NUMBER: 01955
DOD -FLAP ACCREDITATION NUMBER: 74960
ANALYTICAL RESULTS
PERFORMED BY
Pace Analytical Gulf Coast
7979Innovation Park Dr.
Baton Rouge, LA 70820
[phone]
Report Date 11/08/2019
IReport N 2II19^3II030E1
Project 9100391
Deliver To Additional Recipients
Robbi Jones NONE
Prism Laboratories
PO Box 240543
Charlotte, NC 28224
800-529-6364
17025/
PJTesting �I.• 180W -
DOD EIAP
Lab Report#: 219103021 Pa e 2 of 11
Page 38 of 47

/ .. �acewza�yticai'
Report#: 219103021
Project ID: 9100391
Report Date: 11/08/2019
Laboratory Endorsement
Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Followng this
retention period the samples will be disposed in accordance with Pace Gulf Coast's Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
ND Indicates the result was Not Detected at the specified reporting limit
NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030
DO Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLD Indicates the analysis was performed in the Field
DL Detection Limit
LOD Limit of Detection
LOCI Limit of Quantitation
RE Re -analysis
CIF HPLC or GC Confirmation
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
J or I Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
* Indicates a non -compliant or not applicable QC recovery or RPD — see narrative
E Organics - The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
L Reporting Limits adjusted to meet risk -based limit.
P RPD between primary and confirmation result is greater than 40
DL Diluted analysis —when appended to Client Sample ID
Sample receipt at Pace Gulf Coast is documented through the attached chain of custody. In accordance with NELAC, this report shall be
reproduced only in full and with the written permission of Pace Gulf Coast. The results contained within this report relate only to the samples
reported. The documented results are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if
applicable.
(—)
Authorized Signature
Pace Gulf Coast Report 219103021
Lab Report#: 219103021 Page 3 of 11
Page 39 of 47

,� ..•�tceAnalyticaf
Report#: 219103021
Project ID: 9100391
Certifications
Report Date: 11/08/2019
Certification
Certification Number
DOD ELAP
74960
Alabama
01955
Arkansas
88-0655
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentucky
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
mississi2pi
01955
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
Washington
C929
USDA Soil Permit
P330-16-00234
Lab Report#: 219103021 Page 4 of 11
Page 40 of 47

Report#: 219103021
4COAMI1 OcW
Project ID: 9160341
Case Narrative
Client: Access Analytical Report: 219103021
Report Date: 11/08/2019
Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found for the analyzed sample(s).
Lab Report#: 219103021 Pa e 5 of 11
Page 41 of 47

LAB ID
21910302101
Report#: 219103021
Project ID: 9100391
Sample Summary
Client ID Matrix Collect Date/Time
Report Date: 11/08/2019
Receive Date/Time
MW-01 Water 10/24/2019 12:13 10/30/2019 09:35
Lab Report#:219103021
Page 6 of 11
Page 42 of 47

f . ;ce�ly�tic�r
Report#: 219103021
Project ID: 9100391
Report Date: 11/08/2019
Summary of Compounds Detected
Collect Date 10/24/2019 12:13 LAB ID 21910302101
MW-01 Receive Date 10/30/2019 09:35 Matrix Water
SM 5310 B-2011
CAS# Parameter Result DL LOQ Units
C-012 Total Organic Carbon 17.7 0.300 2.00 mg/L
Lab Report#: 219103021
Page 43 of 47

Report#: 219103021
3ceAnalyheal
Project ID: 9100391 Report Date: 11/08/2019
MW-01
SM 5310 B-2011
Sample Results
Collect Date 10/24/2019 12:13
Receive Date 10/30/2019 09:35
LAB ID 21910302101
Matrix Water
Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch
NA NA NA 1 11/07/2019 21:41 PLH 670891
CAS#
C-012
Parameter
Total Organic Carbon
Result DL LOQ Units
17.7 0.300 2.00 mg/L
Lab Report#: 219103021 Pa e 8 of 11
Page 44 of 47

Report#: 219103021
.�GeR+ralldical
Project ID: 9100391
General Chemistry QC Summary
Analytical Batch
670891
Client ID
MB670891
LAB ID
1979630
Sample Type
MB
Prep Date
NA
Analysis Date
11/07/2019 20:07
Matrix
Water
SM 5310 B-2011
_ Result
Total Organic Carbon C-012 I 0.3000
Report Date: 11/08/2019
LCS670891
1979631
LCS
NA
11/07/2019 19:15
Water
mg/L
Spike
Result
%R
Control
DL
Added
Limits%R
0.300
50.01
51.2
102
90 - 110
Lab Report#: 219103021
Pa e9of11
Page 45 of 47

r
m
Q
X
CD
10
0
w
0
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Client ID: 4565 - Access Analytical
SDG: 219103021
PRISMEnvliorimental Solutions i} /1 PM: DLH
SUBCONTRACT ORDER
0 Cenifca:lnn:f\ELM: i;SACE
/V\ Prism Laboratories, Inc. T-JC l! SC Olhcr
IJUL iJ � 9100391 N;n
FK'Nn?-X'f LA110RATUM RRECEIVINGLA13ORATORY•
Prism Laboratories, Inc, Pue_ Analytical Gufftaast
P. 0. Box 240543 107SI Coursey Blvd
Charlotte, NC 28224-0543 13➢ton Rau¢c- L.x 70315
Phone: [phone] Phone :[phone]f)8
Fax:[phone] Fmt:(2I:)767-5717
Project Manager: Robbi A .Tones
Analysis Due Expires LaboraloryM Comn-m
Sample ID: 9100391-01 \Yater Sampled: 10124tl9 12:13 M w
TOC (Sub) 11121,119 12:13 S1d 5310H
A(A vCN HG�
R�leafcyjiyv IIalc Rcc,i •�[,r �Cr�'[� Da
Released SW Dale Rceriecc By Dot_
Re!e.l d By DJIe RfUk(4( I)\ 1. .
Page 1 of 1
Page 46 of 47

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Page 47 of 47

PR I S M Full -Service Analytical Environmental Solutions
LAvORATORIPS, INC.
Anchor QEA of North Carolina, PLLC
Alec Macbeth
231 Haywood Street
Asheville, NC 28801
NC Certification No. 402 Case Narrative
NC Drinking Water Cert No. 37735 11/11/19 14:03
SC Certification No. 99012
Project: Jackson Cty Landfill 2019 Fall Samplling
Project No.: 50-02
Lab Submittal Date: 10/25/2019
Prism Work Order: 9100392
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
7 ' a_.
?rw--
RobbiA.Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 5pringbrnok Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

Sample Receipt Summary
,� P R I S M I mI Full -Service Analytical 11 /11 /2019
Environental Solutionss
LIG�nATOAIES. INC.
Prism Work Order: 9100392
Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received
DW-01 9100392-01 Water 10/24/19 13:17 10/25/19 8:55
TB-DW 9100392-02 Water 10/24/19 0:00 10/25/19 8:55
Samples were received in good condition at 2.6 degrees C unless otherwise noted
This iupuit should nut be reproduced, except in its entirety, without the written consent of Priam Laboratoriee, Inc.
449 Springbrook Road • P.O. Box 240543 - C:harintte, NC: 78774-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

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Pke Analytical
j www.pacelabs.com
November 07, 2019
Robbi A. Jones
Prism Laboratories, Inc.
P.O. Box 240543
Charlotte, NC 28224
RE: Project: 9100392
Pace Project No.: 92451455
Dear Robbi Jones:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on October 29, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Angela Overcash, Prism
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC
Page 1 of 13

0
mace Analytical
' www.pacelabs.com
t
CERTIFICATIONS
Project: 9100392
Pace Project No.: 92451455
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Missouri Certification #: 236
Alaska DEC- CS/UST/LUST
Montana Certification #: Cert 0074
Alabama Certification #: 41320
Nebraska Certification: NE-OS-28-14
Arizona Certification# AZO819
New Hampshire Certification #: 2958
Colorado Certification: FL NELAC Reciprocity
New Jersey Certification #: FL022
Connecticut Certification #: PH-0216
New York Certification #: 11608
Delaware Certification: FL NELAC Reciprocity
North Carolina Environmental Certificate #: 667
Florida Certification #: E83079
North Carolina Certification #: 12710
Georgia Certification #: 955
North Dakota Certification #: R-216
Guam Certification: FL NELAC Reciprocity
Oklahoma Certification #: D9947
Hawaii Certification: FL NELAC Reciprocity
Pennsylvania Certification #: 68-00547
Illinois Certification #: 200068
Puerto Rico Certification #: FLO1264
Indiana Certification: FL NELAC Reciprocity
South Carolina Certification: #96042001
Kansas Certification #: E-10383
Tennessee Certification #: TN02974
Kentucky Certification #: 90050
Texas Certification: FL NELAC Reciprocity
Louisiana Certification #: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Virginia Environmental Certification #: 460165
Maryland Certification: #346
West Virginia Certification #: 9962C
Michigan Certification #: 9911
Wisconsin Certification #: 399079670
Mississippi Certification: FL NELAC Reciprocity
Wyoming (EPA Region 8): FL NELAC Reciprocity
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Face Analytical Services, LLt;. Page 2 of 13

accAnalytical
www.pacelabs.com
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.
9100392
92451455
Analytes
Lab ID
Sample ID
Method Analysts Reported Laboratory
92451455001
DW-01
EPA 524.2 JLR 24 PASI-O
92451455002
TB-DW
EPA 524.2 JLR 24 PASI-O
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
wdhuu[ [lie wiitten consent ul PaceAnalylical Seivwues, LLC Page 3 of 13

aceAnalytical
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Project: 9100392
Pace Project No.: 92451455
Sample: DW-01 Lab ID: 92451455001 Collected: 10/24/19 13:17 Received: 10/29/19 15:51 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
524.2 MSV Analytical Method: EPA 524.2
Benzene
ND
mg/L
0.00050
1
11/06/19 11:18
71-43-2
Carbon tetrachloride
ND
mg/L
0.00050
1
11/06/19 11:18
56-23-5
Chlorobenzene
ND
mg/L
0.00050
1
11/06/19 11:18
108-90-7
1,2-Dichlorobenzene
ND
mg/L
0.00050
1
11/06/19 11:18
95-50-1
1,4-Dichlorobenzene
ND
mg/L
0.00050
1
11/06/19 11:18
106-46-7
1,2-Dichloroethane
ND
mg/L
0.00050
1
11/06/19 11:18
107-06-2
1,1-Dichloroethene
ND
mg/L
0.00050
1
11/06/19 11:18
75-35-4
cis-1,2-Dichloroethene
ND
mg/L
0.00050
1
11/06/19 11:18
156-59-2
trans-1,2-Dichloroethene
ND
mg/L
0.00050
1
11/06/19 11:18
156-60-5
1,2-Dichloropropane
ND
mg/L
0.00050
1
11/06/19 11:18
78-87-5
Ethylbenzene
ND
mg/L
0.00050
1
11/06/19 11:18
100-41-4
Methylene Chloride
ND
mg/L
0.0010
1
11/02/19 03:58
75-09-2
Styrene
ND
mg/L
0.00050
1
11/06/19 11:18
100-42-5
Tetra chl o roethene
ND
mg/L
0.00050
1
11/06/19 11:18
127-18-4
Toluene
ND
mg/L
0.00050
1
11/06/19 11:18
108-88-3
1,2,4-Trichlorobe nzene
ND
mg/L
0.00050
1
11/06/1911-18
120-82-1
1,1,1-Trichloroethane
ND
mg/L
0.00050
1
11/06/19 11:18
71-55-6
1,1,2-Trichloroethane
ND
mg/L
0.00050
1
11106/1911:18
79-00-5
Trichloroethene
ND
mg/L
0.00050
1
11/06/19 11:18
79-01-6
Vinyl chloride
ND
mg/L
0.00050
1
11/06/19 11:18
75-01-4
Xylene (Total)
ND
mg/L
0.0010
1
11/06/19 11:18
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
98
%
70-130
1
11/06/19 11:18
460-00-4
Toluene-d8 (S)
98
%
70-130
1
11/06/19 11:18
2037-26-5
1,2-Dichloroethane-d4 (S)
108
%
70-130
1
11/06/19 11:18
17060-07-0
Sample: TB-DW Lab ID: 92451455002 Collected: 10/24/19 00:00 Received: 10/29/19 15:51 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
524.2 MSV Analytical Method: EPA 524.2
Benzene
ND
mg/L
0.00050
1
11/06/1910:54
71-43-2
Carbon tetrachloride
ND
mg/L
0.00050
1
11/06/19 10:54
56-23-5
Chlorobenzene
ND
mg/L
0.00050
1
11/06/1910:54
108-90-7
1,2-Dichlorobenzene
ND
mg/L
0.00050
1
11/06/1910:54
95-50-1
1,4-Dichlorobenzene
ND
mg/L
0.00050
1
11/06/1910:54
106-46-7
1,2-Dichloroethane
ND
mg/L
0.00050
1
11/06/1910:54
107-06-2
1,1-Dichloroethene
ND
mg/L
0.00050
1
11/06/1910:54
75-35-4
cis-1,2-Dichloroethene
ND
mg/L
0.00050
1
11/06/1910:54
156-59-2
trans-1,2-Dichloroethene
ND
mg/L
0.00050
1
11/06/1910:54
156-60-5
1,2-Dichloropropane
ND
mg/L
0.00050
1
11/06/1910:54
78-87-5
Ethylbenzene
ND
mg/L
0.00050
1
11106/1910:54
100-41-4
Methylene Chloride
ND
mg/L
0.0010
1
11/02/19 03:32
75-09-2
Styrene
ND
mg/L
0.00050
1
11/06/1910:54
100-42-5
Tetrachloroethene
ND
mg/L
0.00050
1
11/06/1910:54
127-18-4
Toluene
ND
mg/L
0.00050
1
11/06/1910:54
108-88-3
REPORT OF LABORATORY
ANALYSIS
This report shall not
be reproduced, except in full,
Date: '11/07/20'19 02.23 PM
wdlwut
the written uunsent of Peue Anelyhwl
Sei vines, LLC.
Page 4 of '13

aceAnalytical
' www.paceiabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: 9100392
Pace Project No.: 92451455
Sample: TB-DW Lab ID: 92451455002 Collected: 10/24/19 00:00 Received: 10/29/19 15:51 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
524.2 MSV Analytical Method: EPA 524.2
1,2,4-Trichlorobenzene
ND
mg/L
0.00050
1
11/06/19 10:54
120-82-1
1,1,1-Trichloroethane
ND
mg/L
0.00050
1
11/06/19 10:54
71-55-6
1,1,2-Trichloroethane
ND
mg/L
0.00050
1
11/06/19 10:54
79-00-5
Trichloroethene
ND
mg/L
0.00050
1
11/06/19 10:54
79-01-6
Vinyl chloride
ND
mg/L
0.00050
1
11/06/19 10:54
75-01-4
Xylene (Total)
ND
mg/L
0.0010
1
11/06/19 10:54
1330-20-7
Surrogates
4-Bromofluorobenzene (S)
97
%
70-130
1
11/06/19 10:54
460-00-4
Toluene-d8 (S)
99
%
70-130
1
11/06/19 10:54
2037-26-5
1,2-Dichloroethane-d4 (S)
111
%
70-130
1
11/06/19 10:54
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/07/2019 02:23 PM without the written consent of face Analytical Services, LLC:. Page 5 of 13

aceAnalytical"
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QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
9100392
Pace Project No.:
92451455
QC Batch:
583681 Analysis Method: EPA 524.2
QC Batch Method:
EPA 524.2 Analysis Description: 524.2 MSV
Associated Lab Samples: 92451455001, 92451455002
METHOD BLANK: 3173338 Matrix: Water
Associated Lab Samples: 92451455001, 92451455002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Methylene Chloride
mg/L
ND
0.0010
11/02/19 02:13
1,2-Dichloroethane-d4 (S)
%
99
70-130
11/02/19 02:13
4-Bromofluorobenzene (S)
%
98
70-130
11/02/19 02:13
Toluene-d8 (S)
%
98
70-130
11/02/19 02:13
LABORATORY CONTROL SAMPLE & LCSD:
3173339
3173340
Spike
LCS LCSD
LCS
LCSD
% Rec Max
Parameter
Units Conc.
Result Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Methylene Chloride
mg/L 0.04
0.041 0.034
102
85
70-130 17 20
1,2-Dichloroethane-d4 (S)
%
96
97
70-130
4-Bromofluorobenzene (S)
%
105
105
70-130
Toluene-d8 (S)
%
100
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/07/2010 02:23 PM wilhuul the writluri =wunt ul Puce Aiwlyliuul Suiviuua, LLC.
Paye 6 of 13

r
mace Analytical
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QUALITY CONTROL DATA
Project: 9100392
Pace Project No.: 92451455
QC Batch: 584736 Analysis Method: EPA 524.2
QC Batch Method: EPA 524.2 Analysis Description: 524.2 MSV
Associated Lab Samples: 92451455001, 92451455002
METHOD BLANK: 3179024
Associated Lab Samples: 92451455001, 92451455002
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1-Trichloroethane
mg/L
ND
0.00050
11/06/19 10:30
1,1,2-Trichloroethane
mg/L
ND
0.00050
11/06/19 10:30
1,1-Dichloroethene
mg/L
ND
0.00050
11/06/19 10:30
1,2,4-Trichlorobenzene
mg/L
ND
0.00050
11/06/19 10:30
1,2-Dichlorobenzene
mg/L
ND
0.00050
11/06/19 10:30
1,2-Dichloroethane
mg/L
ND
0.00050
11/06/19 10:30
1,2-Dichloropropane
mg/L
ND
0.00050
11/06/19 10:30
1,4-Dichlorobenzene
mg/L
ND
0.00050
11/06/19 10:30
Benzene
mg/L
NO
0.00050
11/06/19 10:30
Carbon tetrachloride
mg/L
ND
0.00050
11/06/19 10:30
Chlorobenzene
mg/L
ND
0.00050
11/06/19 10:30
cis-1,2-Dichloroethene
mg/L
ND
0.00050
11/06/19 10:30
Ethylbenzene
mg/L
ND
0.00050
11/06/19 10:30
Styrene
mg/L
ND
0.00050
11/06/19 10:30
Tetrachloroethene
mg/L
ND
0.00050
11/06/19 10:30
Toluene
mg/L
ND
0.00050
11/06/19 10:30
trans-1,2-Dichloroethene
mg/L
ND
0.00050
11/06/19 10:30
Trichloroethene
mg/L
ND
0.00050
11/06/19 10:30
Vinyl chloride
mg/L
ND
0.00050
11/06/19 10:30
Xylene (Total)
mg/L
ND
0.0010
11/06/19 10:30
1,2-Dichloroethane-d4 (S)
%
110
70-130
11/06/19 10:30
4-Bromofluorobenzene (S)
%
98
70-130
11/06/19 10:30
Toluene-d8 (S)
%
100
70-130
11/06/19 10:30
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
3179025
Units
Spike
Conc.
3179026
LCS LCSD
Result Result
LCS
% Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD Qualifiers
1,1,1-Trichloroethane
mg/L
0.01
0.010
0.0099
100
99
70-130
1
20
1,1,2-Trichloroethane
mg/L
0.01
0.0098
0.0098
98
98
70-130
0
20
1,1-Dichloroethene
mg/L
0.01
0.0092
0.0091
92
91
70-130
1
20
1,2,4-Trichlorobenzene
mg/L
0.01
0.0095
0.0093
95
93
70-130
3
20
1,2-Dichlorobenzene
mg/L
0.01
0.010
0.0096
100
96
70-130
4
20
1,2-Dichloroethane
mg/L
0.01
0.0094
0.0094
94
94
70-130
1
20
1,2-Dichloropropane
mg/L
0,01
0.0093
0.0092
93
92
70-130
1
20
1,4-Dichlorobenzene
mg/L
0.01
0.0096
0.0095
96
95
70-130
2
20
Benzene
mg/L
0.01
0.0099
0.0099
99
99
70-130
0
20
Carbon tetrachloride
mg/L
0.01
0.010
0.010
104
104
70-130
0
20
Chlorobenzene
mg/L
0.01
0.0094
0.0094
94
94
70-130
0
20
cis-1,2-Dichloroethene
mg/L
0.01
0.0087
0.0086
87
86
70-130
1
20
Ethylbenzene
mg/L
0.01
0.0096
0.0096
96
96
70-130
1
20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/07/2019 02:23 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 13

.PaceAnalytical
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QUALITY CONTROL DATA
Project: 9100392
Pace Project No.: 92451455
LABORATORY CONTROL SAMPLE & LCSD:
3179025
3179026
Spike
LCS
LCSD
LCS
LCSD
% Rec
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
Styrene
mg/L
0.01
0.0099
0.0099
99
99
70-130
Tetrachloroethene
mg/L
0.01
0.0097
0.010
97
100
70-130
Toluene
mg/L
0.01
0.0092
0.0091
92
91
70-130
trans-1,2-Dichloroethene
mg/L
0.01
0.0093
0.0093
93
93
70-130
Trichloroethene
mg/L
0.01
0.0083
0.0085
83
85
70-130
Vinyl chloride
mg/L
0.01
0.0092
0.0095
92
95
70-130
Xylene (Total)
mg/L
0.03
0.030
0.029
99
98
70-130
1,2-Dichloroethane-d4 (S)
%
106
105
70-130
4-Bromofluorobenzene (S)
%
100
100
70-130
Toluene-d8 (S)
%
98
102
70-130
RPD
Pace Analytical Services, LLC
9800 Kincey Ave, Suite 100
Huntersville, NC 28078
[phone]
Max
RPD
0 20
3 20
2 20
0 20
2 20
3 20
1 20
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/07/2019 02:23 PM without the written consent of Pace Analytical Services, LLC
Qualifiers
Page 8 of 13

FaceAnalytical
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QUALIFIERS
Project: 9100392
Pace Project No.- 92451455
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270_ The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-O Pace Analytical Services - Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in Full,
Date: 11/07/2019 02:23 PM without the written consent of Pace Analytical Services, LLC Page 9 of 13

0
(:�.;a'ce Analytical
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: 9100392
Pace Project No.: 92451455
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
92451455001
DW-01
EPA 524.2
583681
92451455001
DW-01
EPA 524.2
584736
92451455002
TB-DW
EPA 524.2
583681
92451455002
TB-DW
EPA 524.2
584736
Date: 11/07/2019 02:23 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
Page 10 of 13

Document Name: Document Revised: February 7, 2018
Sample Condition Upon Receipt(SCUR) Page 1 of 2
aceAr�ytical A Document No.: Issuing Authority:
F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
Laboratory receiving samples: f
Asheville ❑ Eden[:] Greenwood ❑ Huntersville © Raleigh❑ Mechanicsville❑
Sample Condi4on Client Name: W® ; 92451455
n Project M
f
�gli[ler: _ i^}Felj )«x nitPS ❑L}SPS �F Clien_t_ _ II II12 III I I III II II I III
❑ Commercial ❑Pare []Other: L 92451455
Custody Seal Present? ❑Yes [2No Seals Intact? ❑Yes ❑No
Packing Material: El Bubble Wrap ❑Bubble Bags [:]None Er Other
Thermometer:
D[R sun lD: 92TO49 Type of Ice: (Net ❑Blue
Cooler Temp ('C): U Correction Factor: Add/Subtract ('C) 0.0
Cooler Temp Corrected ('C):
USDA Regulated Sol] ( N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
7j
Date/Initials Person Examining Contents: 10r()
Biological Tissue Frozen?
❑None
Temp should be above freezing to 6°C
❑samples out of temp criteria. Samples on ice, cooling process
hasbegun
Did samples originate from a foreign source (internationally,
i—;w inv w...n and mi—mmem'? I7Yvc rlNo
Comments/Dlscrepanc :
Chain of Custody Present?
[2res
❑No
N/A
1.
Samples Arrived within Hold Time?
[9�es
[]No
❑N/A
2.
Short Hold Time Analysis (02 hr.)?
❑Yes
©No
❑N/A
3.
Rush Turn Around Time Requested?
[]Yes
No
[]N/A
4.
Sufficient Volume?
fF
i,r❑No
[]NIA
S.
Correct Containers Used?
Y s
[:]No
[:]N/A
6.
-Pace Containers Used?
❑No
❑N/a
Containers Intact?
,,)!jyes
LrJYes
❑No
LJNIA
7.
Dissjlved analysis: Samples Field Filtered?
❑Yes
❑No
i /A
B. -
Sample Labels Match COC?
❑ices
❑No
❑N/A
9.
-Includes Date/Time/ID/Analysis Matrix:
Headspace in VOA Vials (>5-6mm)7
❑Yes
No
❑N/A
10.
Trip Blank Present?
®4es
❑vn
[-]N/A
11.
Trip Blank Custody Seals Present?
❑Yes
No
N/A
COMMENTS/SAMPLE DISCREPANCY
V C' C
4 Ai l rV;o/= f1 (U J r—c I� �" S .ii'7r raw ' t Lo iD of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: 1�L �y" f Date/Time:
Project Manager SCURF Review:
Project Manager SRF Review:
Field Data Required? ❑Yes ❑No
e,II"L -1i,,L)C)
Date:
Date:
Page 11 of 13

Document Name: - Document Revised: February 7,1018
Sample Candition Upon Recelpt(SCUR Page 1 of 2
ac�AnaV cal Document No.: Issuing Authority:
F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Collform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHS
**Bottom half of box Is to list number of bottle
Project a E WO# : g2451455
PM: MWB Due Date: 11/22/19
CLIENT: 92—Prism
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pH Adjustment Log for Preserved Samples
Sample ID Type of Preservative off upon receipt Date preservation adjusted Time preservation Amount of Freservative Lot It
adjusted added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will he sent to the North Carolina DEHNR Certification Office (i.e.
Dut of hold, Incorrect preservative, out of temp, Incorrect containers.
Page 12 of 13

Full-Srruice Analytical &
.-;,"PRISM I Environmental Solutions
f �
SUBCONTRACT ORDER r
CcrliCicatian: ?+ S :1r._ USACE
Prism Laboratories, Inc. .C,
9100392 NDi_
SENDING LABORATORY:
Prism Laboro;orics, Inc.
P. O. Box 240543
Chnrloitc, )\C 28224-0543
Phone: [phone]
Fnx: 704-525-0409
Project idanagcr: Robbi A. Jones
Analysls
Due Expires
Sample ID: 9100397-01 Wafer Sampled: 10/24J19 13:17
5242 (Sub)
Cow.wers S'up'+hrd'
Sample ID: 9100392-02
524.2 (Sub)
Cp1147i11e1l5.Sr+ ipGed
� 'I -ICE L'
11(07119 13:17
TttCEIVTNG L ABORATORV
Pace Analytical, Inc
9800, KinceyAvenue Suite 100
Huntersville, NC 28078
Phone ,[phone]
9 ,)u
Fax: [phone]
1 1
Laboratory ID Comments
Wafer S2mpled:l0/2411900:0Q
11/07/19 00:00
B
it<i:astd !iv Daic
Rcr. ivcJ By
.I
. -
i2r!cascd iiy i)a:i
ilecci••cu B;'
f?ou
Pace 1 c! 1
Page '13 of 13

Full -Su rvsce Analytical &
Environmental Solutions
.��4p0ppA7EIFilES ING
Anchor QEA of North Carolina, PLLC
Alec Macbeth
231 Haywood Street
Asheville, NC 28801
NC Certification No.402 Case Narrative
NC Drinking Water Cart No. 37735 11 /14/19 15:27
SC Certification No. 99012
Project: Jackson Cty Landfill 2019 Fall Samplling
Project No.: 50-02
Lab Submittal Date: 10/25/2019
Prism Work Order: 9100393
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
CO2, Hydrogen, Methane, Ethane, Ethene and VFA analysissubcontracted to Pace /M icroseeps.
Laboratory report is attached with a total page count of 29 pages.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
V'�' e�- A — °r - ;-'ram
Robbi A. Jones
President/Project Manager
Data Qualifiers Key Reference:
Reviewed By Robbi A. Jones
President/Project Manager
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-8001529-6364 - Fax: [phone]

PRISMSample
rrr�.unrr.nica nx.
Full-Servkce Analytical 8
Environmental solutions
Receipt Summary
11 /14/2019
Prism Work Order: 9100393
Client Sample ID
Lab Sample ID
Matrix
Date/Time Sampled Date/Time Received
MW-01
9100393-01
Water
10/24/19 12:13 10/25/19 8:55
MW-02
9100393-02
Water
10/23/19 9:26 10/25/19 8:55
MW-03
9100393-03
Water
10/23/19 10:26 10/25/19 8:55
MW-04
9100393-04
Water
10/22/19 11:26 10/25/19 8:55
MW-05R
9100393-05
Water
10/23/19 14:32 10/25/19 8:55
MW-06
9100393-06
Water
10/23/19 12:54 10/25/19 8:55
MW-07
9100393-07
Water
10/22/19 12:57 10/25/19 8:55
Samples were received in good condition at 2.6 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.U. Box 240543 - Charlotte, NG 28224-Ob43
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]

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acleAnalytical
November 11, 2019
Robbi A. Jones
Prism Laboratories, Inc.
P.O. Box 240543
Charlotte, NC 28224-0543
RE: 9100393
Pace Workorder." 31949
Dear Robbi Jones:
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Enclosed are the analytical results for sample(s) received by the laboratory on Tuesday, October 29, 2019.
Results reported herein conform to the most current NELAC standards, where applicable, unless otherwise
narrated in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Ruth Welsh 11/11/2019
[e-mail]
Customer Service Representative
Enclosures
As a valued client we would appreciate your comments on our service.
Please email [e-mail].
Report ID: 31949 - 1225522
CERTIFICATE OF ANALYSIS
ne��1�= This report shall not be reproduced. except in full,
without the written conseni of Pace Analytical Energy Services LLC
Total Number of Pages 26
Page 1 of 23

aceAnalytical
LABORATORY ACCREDITATIONS & CERTIFICATIONS
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Accreditor: Pennsylvania Department of Environmental Protection, Bureau of Laboratories
Accreditation ID: 02-00538
Scope: NELAP Non -Potable Water
Accreditor: West Virginia Department of Environmental Protection, Division of Water and Waste
Management
Accreditation ID: 395
Scope: Non -Potable Water
Accreditor:
Accreditation ID:
Scope:
Accreditor:
Accreditation ID:
Scope:
Accreditor:
Accreditation ID:
Scope:
South Carolina Department of Health and Environmental Control, Office of Environmental
Laboratory Certification
89009003
Clean Water Act (CWA); Resource Conservation and Recovery Act (RCRA)
State of Virginia
460201
Non -Potable Water
NELAP: New Jersey, Department of Environmental Protection
PA026
Non -Potable Water
Accreditor: NELAP: New York, Department of Health Wadsworth Center
Accreditation ID: 11815
Scope: Non -Potable Water
Accreditor: State of Connecticut, Department of Public Health, Division of Environmental Health
Accreditation ID: PH-0263
Scope: Clean Water Act (CWA) Resource Conservation and Recovery Act (RCRA)
Accreditor: NELAP: Texas, Commission on Environmental Quality
Accreditation ID: T104704453-09-TX
Scope: Non -Potable Water
Accreditor: State of New Hampshire
Accreditation ID: 299409
Scope: Non -potable water
Accreditor: State of Georgia
Accreditation ID: Chapter 391-3-26
Scope: As per the Georgia EPD Rules and Regulations for Commercial Laboratories, PAES is
accredited by the Pennsylvania Department of Environmental Protection Bureau of
Laboratories under the National Environmental Laboratory Approval Program (NELAC).
Report ID: 31949 - 1225522
r- CERTIFICATE OF ANALYSIS
nela4 This report shall not be reproduced, except in Full,
without the written consent of Pace Analytical Energy Services LLC.
Page 2 of 23

aceAnalytical
I
SAMPLE SUMMARY
Workorder: 31949 9100393
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID
Sample ID
Matrix
Date Collected
Date Received
319490001
MW-01
Water
10/24/2019 12:13
10/29/2019 11:30
319490002
MW-02
Water
10/23/2019 09:26
10/29/2019 11:30
319490003
M W-03
Water
10/23/2019 10:26
10/29/2019 11:30
319490004
MW-03
Bubble Strip
10/23/2019 10:26
10/29/2019 11:30
319490005
M W-04
Water
10/22/2019 11:26
10/29/2019 11:30
319490006
MW-04
Bubble Strip
10/22/2019 11:26
10/29/2019 11:30
319490007
MW-05R
Water
10/23/2019 14:32
10/29/2019 11:30
319490008
MW-06
Water
10/23/2019 12:54
10/29/2019 11:30
319490009
MW-06
Bubble Strip
10/23/2019 12:54
10/29/2019 11:30
319490010
M W-07
Water
10/22/2019 12:57
10/29/2019 11:30
319490011
MW-07
Bubble Strip
10/22/2019 12:57
10/29/2019 11:30
Report ID: 31949 - 1225522 Page 3 of 23
CERTIFICATE OF ANALYSIS
'r1BC' This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

aceAnalytical
PROJECT SUMMARY
Workorder: 31949 9100393
Workorder Comments
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Samples 31949 (0005, 0010) were analyzed outside the hold time of 14 days from collection for the Volatile Fatty acids. Method
AM23G.
Batch Comments
Batch: EDON/4258 -Low Level Volatile Fatty Acids
The matrix spike and/or spike duplicate, recovery or relative percent difference; accuracy influenced by the reference sample
319240001. Analyte iso-Hexanoic acid. Batch acceptance based on laboratory control sample recovery.
Report ID: 31949 - 1225522
^� CERTIFICATE OF ANALYSIS
n ^� This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC
Page 4 of 23

aceAnalytical
ANALYTICAL RESULTS
Workorder: 31949 9100393
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 319490001
Sample ID: MW-01
Date Received: 10/29/2019 11:30 Matrix: Water
Date Collected: 10/24/2019 12:13
Parameters
Results Units
PQL
MDL DF
Analyzed
By
Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.20 U mg/I
0.20
0.048 1
11/6/2019 00:03
KB
Acetic Acid
0.36 mg/I
0.10
0.025 1
11/6/2019 00:03
KB
Propionic Acid
0.10 U mg/I
0.10
0.0020 1
11/6/2019 00:03
KB
Formic Acid
0.50 U mg/I
0.50
0.098 1
11/6/2019 00:03
KB
Butyric Acid
0.10 U mg/I
0.10
0.0070 1
11/6/2019 00:03
KB
Pyruvic Acid
0.10 U mg/I
0.10
0.0050 1
11/6/2019 00:03
KB
i-PentanoicAcid
0.10 U mg/I
0.10
0.0050 1
11/6/2019 00:03
KB
Pentanoic Acid
0.10 U mg/I
0.10
0.011 1
11/6/2019 00:03
KB
i-HexanoicAcid
0.20 U mg/I
0.20
0.011 1
11/6/2019 00:03
KB
M5
HexanoicAcid
0.20 U mg/I
0.20
0.032 1
11/6/2019 00:03
KB
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
740 ug/I
0.50
0.094 1
11/4/2019 09:42
TD
n
Ethane
0.10 U ug/I
0.10
0.011 1
11/4/2019 09:42
TD
n
Ethene
0.10 U ug/I
0.10
0.0080 1
11/4/2019 09:42
TD
n
Carbon Dioxide
150 mg/I
5.0
0.47 1
11/4/2019 09:42
TD
n
Report ID: 31949 - 1225522 Page 5 of 23
r CERTIFICATE OF ANALYSIS
ne1QC This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC

aceAnalytical
I
ANALYTICAL RESULTS
Workorder: 31949 9100393
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID:
319490002
Date Received:
10/29/2019 11:30 Matrix: Water
Sample ID:
MW-02
Date Collected:
10/23/2019 09:26
Parameters Results Units PQL MDL DF Analyzed By Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.20 U mg/I
0.20
0.048 1
11/6/2019 00:56
KB
Acetic Acid
0.35 mg/I
0.10
0.025 1
11/6/2019 00:56
KB
Propionic Acid
0.10U mg/I
0.10
0.0020 1
11/6/2019 00:56
KB
Formic Acid
0.50U mg/I
0.50
0.098 1
11/6/2019 00:56
KB
Butyric Acid
0.10U mg/I
0.10
0.0070 1
11/6/2019 00:56
KB
Pyruvic Acid
0.10 U mg/I
0.10
0.0050 1
11/6/2019 00:56
KB
i-PentanoicAcid
0.10U mg/I
0.10
0.0050 1
11/6/2019 00:56
KB
Pentanoic Acid
0.10 U mg/I
0.10
0.011 1
11/6/2019 00:56
KB
i-HexanoicAcid
0.20U mg/I
0.20
0.011 1
11/6/2019 00:56
KB
Hexanoic Acid
0.20 U mg/I
0.20
0.032 1
11/6/2019 00:56
KB
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
0.50 U ug/I
0.50
0.094 1
11/4/2019 09:55
TD
Ethane
0.10 U ug/I
0.10
0.011 1
11/4/2019 09:55
TD
Ethene
0.10 U ug/I
0.10
0.0080 1
11/4/2019 09:55
TD
Carbon Dioxide
49 mg/I
5.0
0,47 1
11/4/2019 09:55
TD
Report ID: 31949 - 1225522
CERTIFICATE OF ANALYSIS
`►ne�_ This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC
t
M5
n
n
n
n
Page 6 of 23

V
PaccAnalytical
I
ANALYTICAL RESULTS
Workorder: 31949 9100393
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID:
319490003
Date Received:
10/29/2019 11:30 Matrix: Water
Sample ID:
MW-03
Date Collected:
10/23/2019 10:26
Parameters Results Units PQL MDL DF Analyzed By Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.20 U mg/I
0.20
0.048 1
11/6/2019 01:50
KB
Acetic Acid
0.10 U mg/I
0.10
0.025 1
11/6/2019 01:50
KB
PropionicAcid
0.10 U mg/I
0.10
0.0020 1
11/6/2019 01:50
KB
Formic Acid
0.50U mg/I
0.50
0.098 1
11/6/2019 01:50
KB
Butyric Acid
0.10 U mg/I
0.10
0.0070 1
11/6/2019 01:50
KB
Pyruvic Acid
0.10 U mg/I
0.10
0.0050 1
11/6/2019 01:50
KB
i-Pentanoic Acid
0.10 U mg/I
0.10
0.0050 1
11/6/2019 01:50
KB
Pentanoic Acid
0.10 U mg/I
0.10
0.011 1
11/6/2019 01:50
KB
i-Hexanoic Acid
0.20 U mg/I
0.20
0.011 1
11/6/2019 01:50
KB
Hexanoic Acid
0.20 U mg/I
0.20
0.032 1
11/6/2019 01:50
KB
Report ID: 31949 - 1225522
CERTIFICATE OF ANALYSIS
y This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC-
MR
Page 7 of 23

accAnalytical
ANALYTICAL RESULTS
Workorder: 31949 9100393
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 319490004
Sample ID: MW-03
Date Received: 10/29/2019 11:30 Matrix:
Date Collected: 10/23/2019 10:26
Bubble Strip
Parameters
Results Units
PQL
MDL DF
Analyzed By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
15 ug/I
0.10
0.022 1
10/31/2019 07:10 TD
n
Ethane
0.010 U ug/I
0.010
0.0030 1
10/31/2019 07:10 TD
n
Ethene
0.027 ug/I
0.010
0.0050 1
10/31/2019 07:10 TD
n
Carbon Dioxide
260 mg/I
2.0
0.82 1
10/31/2019 07:10 TD
n
Hydrogen
21 nM
1.0
0.75 1
10/31/2019 07:10 TD
n
Report ID: 31949 - 1225522 Page 8 of 23
CERTIFICATE OF ANALYSIS
r1elaC'; This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

aceAnalytical
ANALYTICAL RESULTS
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Workorder: 31949 9100393
Lab ID: 319490005 Date Received: 10/29/2019 11:30 Matrix: Water
Sample ID: MW-04 Date Collected: 10/22/2019 11:26
Parameters Results Units PQL MDL DF Analyzed By Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.20 U mg/I
0.20
0.048 1
11/6/2019 02:43
KB
Acetic Acid
0.10 U mg/I
0.10
0.025 1
11/6/2019 02:43
KB
Propionic Acid
0.10 U mg/I
0.10
0.0020 1
11/6/2019 02:43
KB
Formic Acid
0.50 U mg/I
0.50
0.098 1
11/6/2019 02:43
KB
Butyric Acid
0.10U mg/I
0.10
0.0070 1
11/6/2019 02:43
KB
PyruvicAcid
0.10U mg/I
0.10
0.0050 1
11/6/2019 02:43
KB
i-PentanoicAcid
0.10 U mg/I
0.10
0.0050 1
11/6/2019 02:43
KB
PentanoicAcid
0.10 U mg/I
0.10
0.011 1
11/6/2019 02:43
KB
i-Hexanoic Acid
0.20 U mg/I
0.20
0.011 1
11/6/2019 02:43
KB
HexanoicAcid
0.20 U mg/I
0.20
0.032 1
11/6/2019 02:43
KB
Report ID: 31949 - 1225522
GEKI IFIGATE OF ANALYSIS
��+i ^��' This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC
H1
H1
H1
H1
H1
H1
H1
H1
H1,M5
H1
Page 9 of 23

i
� iceAnalytical
f�
I
Workorder: 31949 9100393
ANALYTICAL RESULTS
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID:
319490006
Date Received:
10/29/2019 11:30 Matrix: Bubble Strip
Sample ID:
MW-04
Date Collected:
10/22/2019 11:26
Parameters Results Units PQL MDL DF Analyzed By Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
110 ug/I
0.10
0.022 1
10/31/2019 07:27 TD
Ethane
0.014 ug/I
0.010
0.0030 1
10/31/2019 07:27 TD
Ethene
0.010 U ug/I
0.010
0.0050 1
10/31/2019 07:27 TD
Carbon Dioxide
330 mg/I
2.0
0.82 1
10/31/2019 07:27 TD
Hydrogen
100 nM
10
7.5 10
10/31/2019 08:15 TD
Report ID: 31949 - 1225522
CERTIFICATE OF ANALYSIS
:> �e�C This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
n
n
n
n
do
Page 10 of 23

laceAnalyfical
ANALYTICAL RESULTS
Workorder: 31949 9100393
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID:
319490007
Date Received:
10/29/2019 11:30 Matrix: Water
Sample ID:
MW-05R
Date Collected:
10/23/2019 14:32
Parameters Results Units PQL MDL DF Analyzed By Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.20 U mg/I
0.20
0.048 1
11/6/2019 03:36
KB
Acetic Acid
0.56 mg/I
0.10
0.025 1
11/6/2019 03:36
KB
Propionic Acid
0.10 U mg/I
0.10
0.0020 1
11/6/2019 03:36
KB
Formic Acid
0.50 U mg/1
0.50
0.098 1
11/6/2019 03:36
KB
Butyric Acid
0.10 U mg/I
0.10
0.0070 1
11/6/2019 03:36
KB
Pyruvic Acid
0.10 U mg/I
0.10
0.0050 1
11/6/2019 03:36
KB
i-PentanoicAcid
0.10 U mg/I
0.10
0.0050 1
11/6/2019 03:36
KB
Pentanoic Acid
0.10 U mg/I
0.10
0.011 1
11/6/2019 03:36
KB
i-HexanoicAcid
0.20 U mg/I
0.20
0.011 1
11/6/2019 03:36
KB
HexanoicAcid
0.20 U mg/I
0.20
0.032 1
11/6/2019 03:36
KB
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
3400 ug/l
0.50
0.094 1
11/4/2019 10:08
TD
Ethane
0.32 ug/l
0.10
0.011 1
11/4/2019 10:08
TD
Ethene
0.15 ug/I
0.10
00080 1
11/4/2019 10:08
TD
Carbon Dioxide
58 mg/I
5.0
0.47 1
11/4/2019 10:08
TD
Report ID: 31949 - 1225522
CERTIFICATE OF ANALYSIS
`�� ^� This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC
M5
n
n
n
n
Page 11 of 23

aceAnalytical
ANALYTICAL RESULTS
Workorder: 31949 9100393
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID:
319490008
Date Received:
10/29/2019 11:30 Matrix: Water
Sample ID:
MW-06
Date Collected:
10/23/2019 12:54
Parameters Results Units PQL MDL DF Analyzed By Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.20 U mg/I
0.20
0.048 1
11/6/2019 04:30
KB
Acetic Acid
0.10 U mg/I
0.10
0.025 1
11/6/2019 04:30
KB
Propionic Acid
0.10 U mg/I
0.10
0.0020 1
11/6/2019 04:30
KB
Formic Acid
0.50 U mg/I
0.50
0.098 1
11/6/2019 04:30
KB
Butyric Acid
0.10 U mg/I
0.10
0.0070 1
11/6/2019 04:30
KB
Pyruvic Acid
0.10 U mg/1
0.10
0.0050 1
11/6/2019 04:30
KB
i-Pentanoic Acid
0.10 U mg/I
0.10
0.0050 1
11/6/2019 04:30
KB
Pentanoic Acid
0.10 U mg/I
0.10
0.011 1
11/6/2019 04:30
KB
i-HexanoicAcid
0.20 U mg/I
0.20
0.011 1
11/6/2019 04:30
KB
HexanoicAcid
0.20 U mg/I
0.20
0.032 1
11/6/2019 04:30
KB
Report ID: 31949 - 1225522
4 CERTIFICATE OF ANALYSIS
r" elai .- This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC
M5
Page 12 of 23

l '
Pace Analytical Energy Services LLC
220 William Pitt Way
aceAnalytical
Pittsburgh, PA
-
-�
Phone: [phone]
Fax: [phone]
ANALYTICAL RESULTS
Workorder: 31949 9100393
Lab ID: 319490009
Date Received: 10/29/2019 11:30
Matrix: Bubble Strip
Sample ID: MW-06
Date Collected: 10/23/2019 12:54
Parameters
Results Units
PQL MDL DF Analyzed By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
14 ug/I
0.10 0.022 1 10/31/2019 07:45 TD
n
Ethane
0.010 U ug/I
0.010 0.0030 1 10/31/2019 07:45 TD
n
Ethene
0.034 ug/I
0.010 0.0050 1 10/31/2019 07:45 TD
n
Carbon Dioxide
250 mg/I
2.0 0.82 1 10/31/2019 07:45 TD
n
Hydrogen
14 nM
1.0 0.75 1 10/31/2019 07:45 TD
n
Report ID: 31949 - 1225522 Page 13 of23
CERTIFICATE OF ANALYSIS
r ���ae = This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

r
eAnalytical
Workorder: 31949 9100393
ANALYTICAL RESULTS
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID:
319490010
Date Received:
10/29/2019 11:30 Matrix: Water
Sample ID:
MW-07
Date Collected:
10/22/2019 12:57
Parameters Results Units PQL MDL DF Analyzed By Qualifiers
EDonors - PAES
Analysis Desc: AM23G
Analytical Method: AM23G
Lactic Acid
0.20 U mg/I
0.20
0.048 1
11/6/2019 05:23
KB
Acetic Acid
0.10 U mg/I
0.10
0.025 1
11/6/2019 05:23
KB
Propionic Acid
0.10 U mg/I
0.10
0.0020 1
11/6/2019 05:23
KB
Formic Acid
0.50 U mg/I
0.50
0.098 1
11/6/2019 05:23
KB
Butyric Acid
0.10 U mg/I
0.10
0.0070 1
11/6/2019 05:23
KB
Pyruvic Acid
0.10 U mg/I
0.10
0.0050 1
11/6/2019 05:23
KB
i-PentanoicAcid
0.10 U mg/I
0.10
0.0050 1
11/6/2019 05:23
KB
Pentanoic Acid
0.10 U mg/I
0.10
0.011 1
11/6/2019 05:23
KB
i-HexanoicAcid
0.20 U mg/I
0.20
0.011 1
11/6/2019 05:23
KB
Hexanoic Acid
0.20 U mg/I
0.20
0.032 1
11/6/2019 05:23
KB
Report ID: 31949 - 1225522
CERTIFICATE OF ANALYSIS
n�� = This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
H1
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H1
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H1
H1
H1,M5
H1
Page 14 of 23

aceAnalytical
ANALYTICAL RESULTS
Workorder: 31949 9100393
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Lab ID: 319490011
Sample ID: MW-07
Date Received: 10/29/2019 11:30 Matrix:
Date Collected: 10/22/2019 12:57
Bubble Strip
Parameters
Results Units
PQL
MDL DF
Analyzed By
Qualifiers
RISK - PAES
Analysis Desc: AM20GAX
Analytical Method: AM20GAX
Methane
47 ug/I
0.10
0.022 1
10/31/2019 07:59 TD
n
Ethane
0.020 ug/1
0.010
0.0030 1
10/31/2019 07:59 TD
n
Ethene
0.065 ug/I
0.010
0.0050 1
10/31/2019 07:59 TD
n
Carbon Dioxide
490 mg/I
2.0
0.82 1
10/31/2019 07:59 TD
n
Hydrogen
3.4 nM
1.0
0.75 1
10/31/2019 07:59 TD
n
Report ID: 31949 - 1225522 Page 15 of 23
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aceAnalytical
ANALYTICAL RESULTS QUALIFIERS
Workorder: 31949 9100393
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
DEFINITIONS/QUALIFIERS
MDL Method Detection Limit. Can be used synonymously with LOD; Limit Of Detection.
PQL Practical Quanitation Limit. Can be used synonymously with LOQ; Limit Of Quantitation.
ND Not detected at or above reporting limit.
DF Dilution Factor.
S Surrogate.
RPD Relative Percent Difference.
% Rec Percent Recovery.
U Indicates the compound was analyzed for, but not detected at or above the noted concentration.
J Estimated concentration greater than the set method detection limit (MDL) and less than the set reporting limit (PQL).
n The laboratory does not hold NELAP/TNI accreditation for this method or analyte.
H1 The sample was prepared or the analysis was conducted outside the method specific holding time.
d The analyte concentration was determined from a dilution.
M5 The matrix spike duplicate sample recovery was outside laboratory control limits.
Report ID: 31949 - 1225522
CERTIFICATE OF ANALYSIS
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Page 16 of 23

Pace Analytical Energy Services LLC
220 William Pitt Way
�aceAnalytical
Pittsburgh, 15238
82
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Workorder: 31949 9100393
QC Batch: DISG/7884
Analysis Method: AM20GAX
QC Batch Method: AM20GAX
Associated Lab Samples: 319490004, 319490006, 319490009, 319490011
METHOD BLANK: 64067
Blank Reporting
Parameter
Units
Result Limit Qualifiers
RISK
Methane
ug/1
0.10 U 0.10 n
Ethane
ug/1
0.010 U 0.010 n
Ethene
ug/1
0.010 U 0.010 n
METHOD BLANK: 64068
Blank Reporting
Parameter
Units
Result Limit Qualifiers
RISK
Carbon Dioxide
mg/I
2.0 U 2.0 n
METHOD BLANK: 64069
Blank Reporting
Parameter
Units
Result Limit Qualifiers
RISK
Hydrogen
nM
1.0 U 1.0 n
LABORATORY CONTROL SAMPLE & LCSD:
64070 64073
Spike LCS LCSD LCS LCSD
% Rec
Max
Parameter
Units
Conc. Result Result % Rec % Rec
Limit
RPD
RPD
Qualifiers
Methane
ug/I
8.1 8.0 8.0 99 99
80-120
0.29
20
n
Ethane
ug/1
6.4 6.4 6.4 99 100
80-120
0.24
20
n
Ethene
ug/1
16 16 16 100 100
80-120
0.25
20
n
LABORATORY CONTROL SAMPLE & LCSD:
64071 64074
Spike LCS LCSD LCS LCSD
% Rec
Max
Parameter
Units
Conc. Result Result % Rec % Rec
Limit
RPD
RPD
Qualifiers
Carbon Dioxide
mg/I
97 87 87 89 90
80-120
0,51
20
n
Report ID: 31949 - 1225522
Page 17 of 23
CERTIFICATE OF ANALYSIS
��I��
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services
LLC.

Pace Analytical Energy Services LLC
ow! William Pitt Way
,,1 CtceAnalytical Pittsburgh, PA15238
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA
Workorder: 31949 9100393
LABORATORY CONTROL SAMPLE & LCSD: 64072 64075
Spike LCS LCSD LCS LCSD % Rec Max
Parameter Units Conc. Result Result % Rec % Rec Limit RPD RPD Qualifiers
Hydrogen nM 24 24 24 98 98 80-120 0.27 20 n
Report ID: 31949 - 1225522 Page 18 of 23
CERTIFICATE OF ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC

1,ceAnalytical
Workorder: 31949 9100393
QUALITY CONTROL DATA
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
QC Batch: DISG/7891
Analysis Method:
AM20GAX
QC Batch Method: AM20GAX
Associated Lab Samples: 319490001, 319490002,
319490007
METHOD BLANK: 64135
Blank
Reporting
Parameter Units
Result
Limit Qualifiers
RISK
Methane ug/I
0.50 U
0.50 n
Ethane ug/I
0.10 U
0.10 n
Ethene ug/1
0.10 U
0.10 n
METHOD BLANK: 64136
Blank
Reporting
Parameter Units
Result
Limit Qualifiers
RISK
Carbon Dioxide mg/I
5.0 U
5.0 n
LABORATORY CONTROL SAMPLE & LCSD:
64137
64139
Spike LCS
LCSD LCS
LCSD
% Rec
Max
Parameter Units
Conc. Result
Result % Rec
% Rec
Limit
RPD
RPD
Qualifiers
Methane ugA
750 730
800 98
106
80-120
8.7
20
n
Ethane ugA
38 34
40 91
106
80-120
15
20
n
Ethene ugA
35 32
38 92
107
80-120
16
20
n
LABORATORY CONTROL SAMPLE & LCSD:
64138
64140
Spike LCS
LCSD LCS
LCSD
% Rec
Max
Parameter Units
Conc. Result
Result % Rec
% Rec
Limit
RPD
RPD
Qualifiers
Carbon Dioxide mg/I 120 120 130 105 109 80-120 3.2 20 n
Report ID: 31949 - 1225522
neh
CERTIFICATE OF ANALYSIS
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Page 19 of 23

Pace Analytical Energy Services LLC
220 William Pitt Way
ceAnalytical Pittsburgh, PA15238
Phone: [phone]
Fax: [phone]
i
QUALITY CONTROL DATA
Workorder: 31949 9100393
QC Batch: EDON/4258
Analysis Method:
AM23G
QC Batch Method: AM23G
Associated Lab Samples:
319490001, 319490002, 319490003, 319490005,
319490007, 319490008,
319490010
METHOD BLANK: 64193
Blank
Reporting
Parameter
Units
Result
Limit Qualifiers
EDonors
Lactic Acid
mgA
0.20 U
0.20
Acetic Acid
mgA
0.10 U
0.10
Propionic Acid
mg/I
0.10 U
0.10
Formic Acid
mg/1
0.50 U
0.50
Butyric Acid
mg/1
0.10 U
0.10
Pyruvic Acid
mg/1
0.10 U
0.10
i-Pentanoic Acid
mg/1
0.10 U
0.10
Pentanoic Acid
mg/I
0.10 U
0.10
i-Hexanoic Acid
mg/1
0.20 U
0.20 M5
Hexanoic Acid
mg/1
0.20 U
0.20
LABORATORY CONTROL SAMPLE:
64194
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result %
Rec
Limits
Qualifiers
Lactic Acid
mg/I
2
2.1
104
70-130
Acetic Acid
mgA
2
2.0
99
70-130
Propionic Acid
mg/1
2
2.0
103
70-130
Formic Acid
mg/I
2
1.9
94
70-130
Butyric Acid
mg/I
2
2.0
100
70-130
Pyruvic Acid
mg/I
2
1.8
92
70-130
i-Pentanoic Acid
mg/I
2
2.0
99
70-130
Pentanoic Acid
mg/I
2
2.0
98
70-130
i-Hexanoic Acid
mg/I
2
2.0
98
70-130
M5
Hexanoic Acid
mg/I
2
1.9
94
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 64195
64196
Original:
319240001
Original Spike
MS MSD
MS
MSD % Rec Max
Parameter
Units
Result Conc.
Result Result
% Rec
% Rec Limit RPD RPD
Qualifiers
EDonors
Lactic Acid
mg/1
0.26 2
1.9 2.1
84
90 70-130 6.3 30
Acetic Acid
mg/1
0.1 2
2.1 2.1
100
100 70-130 0.23 30
Report ID: 31949 - 1225522
Page 20 of 23
CERTIFICATE OF ANALYSIS
�� '' ^,.
This report shall
not be reproduced, except
in full,
without the written consent
of Pace Analytical Energy Services LLC.

�aceAnalytical
I
QUALITY CONTROL DATA
Workorder: 31949 9100393
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
64195
64196
Original:
319240001
Original
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Result
Result
% Rec
% Rec
Limit
RPD
RPD Qualifiers
PropionicAcid
mg/1
0.0094
2
2.0
2.0
100
100
70-130
0.21
30
Formic Acid
mg/1
0.27
2
2.0
2.0
85
86
70-130
1.7
30
Butyric Acid
mg/1
0.025
2
1.9
2.0
96
98
70-130
2.4
30
Pyruvic Acid
mg/1
0.061
2
1.7
1.7
81
84
70-130
3.4
30
i-Pentanoic Acid
mg/1
0.19
2
2.0
2.1
92
94
70-130
1.6
30
Pentanoic Acid
mg/1
0.018
2
1.8
1.9
91
96
70-130
5.3
30
i-HexanoicAcid
mg/1
0
2
1.5
1.4
74
69
70-130
7.6
30 M5
Hexanoic Acid
mg/1
0.023
2
1.6
1.8
77
88
70-130
13
30
Report ID: 31949 - 1225522 Page 21 of 23
CERTIFICATE OF ANALYSIS
n��a� This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.

aceAnalytical
QUALITY CONTROL DATA QUALIFIERS
Workorder: 31949 9100393
QUALITY CONTROL PARAMETER QUALIFIERS
M5 The matrix spike duplicate sample recovery was outside laboratory control limits.
The laboratory does not hold NELAP/TNI accreditation for this method or analyte.
Report ID: 31949 - 1225522
CERTIFICATE OF ANALYSIS
�� '� This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC
Pace Analytical Energy Services LLC
220 William Pitt VVay
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
Page 22 of 23

Pace Analytical
Workorder: 31949 9100393
Pace Analytical Energy Services LLC
220 William Pitt Way
Pittsburgh, PA 15238
Phone: [phone]
Fax: [phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Analysis
Lab ID
Sample ID
Prep Method Prep Batch Analysis Method
Batch
319490004
MW-03
AM20GAX
DISG/7884
319490006
MW-04
AM20GAX
DISG/7884
319490009
MW-06
AM20GAX
DISG/7884
319490011
MW-07
AM20GAX
DISG/7884
319490001
MW-01
AM20GAX
DISG/7891
319490002
MW-02
AM20GAX
DISG/7891
319490007
MW-05R
AM20GAX
DISG/7891
319490001
MW-01
AM23G
EDON/4258
319490002
MW-02
AM23G
EDON/4258
319490003
MW-03
AM23G
EDON/4258
319490005
MW-04
AM23G
EDON/4258
319490007
MW-05R
AM23G
EDON/4258
319490008
MW-06
AM23G
EDON/4258
319490010
MW-07
AM23G
EDON/4258
Report ID: 31949 - 1225522
CERTIFICATE OF ANALYSIS
nelac This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Energy Services LLC.
Page 23 of 23

r 1
Full-Sumce Analytical & j
/PRISM Enviroo mental Solutions
SUBCONTRACT ORDER
Certification:
NELAC
:SAGE
Prism
Laboratories, inc.
NC_
SC—
0(hcr ^~
9100393
N/A
S . 1 ' 1.a130R T RV
RECEIVING LtkB011AT0RY:
Prism Laboratories, Inc,
Microseeps/Pace
P. 0. Box 210543
qq
220 William Pitt Way
Charlotte, NC 28224-0543
Pittsburgh, PA 15238
Phorc: 800-529-CuG4
Phone :(4 ] 2) 826-5245
Fax: [phone]
Pax: [phone]
Project Manager: Robbi A. Zones
r
C
.Analysis
Due Expires
Laboratory ID
Comments
M Ll — 0
Sample ID: 9100393-01
Water Sampled: 10124119 12:13
Melhane, Ednnc, Ethcr:c (AM20GP 10,'25/19 12:13
Voiaule Fatty Ands (Sub)
10/31/19 12:13
Carbon DioxideANUOGAX
I1/07/19 12:13
CnrraF�rrjrr�arSujyll!/e�:.
x IBC uoa
- -
i
f'r� w - a L.
Sample )D:
�i'a ler Sampled: 3.00231)909:2d
-
Carbon Dio
11/06/19 092!i
J1E(hcr--(A4MG
Nict anc, Et0ir
]0/24/19 09:26
Volatile Fatt10;30/i9
09:2G
Su
rno J
Sample 10:9100393-03
y;lter Sampled: 10/23/19 10:26
Carbon Dioxide A!.120GAX
11/06/19 10:26
Hvdroccn A\:20GAX
11,106119 10:26
Mlcihanc Elhanc, E! cnc ;:11sLUG:`
10/24119 10:26
Vbl a 6lc Fa ev A c: di ;Sub)
10/30"19 10:26
C—whwrs SuPpil.'d
j
U l D
Sample ID: 9100393-04
!a ler Sampled: 10/22/19 11:26
Vn!atac =anv Acids fSub)
10129:119 I L26
Ilydrolx❑ ANQuG—AX
11/051q9 1126
1012'119 I1:26
Cmban Anx;d,AN-1_U(,AX
IIi05/1911:26
t0 -i,S
Rele-,led R.•
"D'Is
Rccc:vcd By
Dmc
Rcleaccd l3; I if
Dote
Rcccrvttl B-,-
tJalc
Rc`::a.•: -F}
Dan;
Rccmcd 13)
J
Page 1 of 2

SUBCONTRACT ORDER
Certification_ NELAC USACF:
Prism
Laboratories, Inc_
NC SC__ Cl[Itcr
9100393
NIA
Analysis Due
Expires
LaboratoryID Comments
Containers Supplied:
Sample ]D: 9100393-05 Water
Sampled: 10/23/19 ]4:32
Y»Iu-v�R
Carbon Dioxide AM20GAX
11/06/19 14:32
Methane, Ethane, Etltcne (AM20Gt
10/24119 14:32
Volatile Fatty Acids (Sub)
1013011914:32
/� 1 l� ✓�
,✓/ `
ConlainersSupplied:
I
Sample 1D: 910039" Water
Sampled: I O1i3119 12:54
_ n)YJ ~ V
Carbon Dioxide AM20GAX
Hydrogen AM20GAX
Methane, Ethane, Elhenc (A
Volatile Fatty Acids (Sub)
Conlainer:c Suppled:
Sample ID: 9100393-07
1 IJ06/19 12:54
11/06/19 12:54
10/24/19 12:54
1080/19 12:54
atrr S2mpled:10122/1912:57
Volatile Fatty Acids (Sub) 10/29/19 12:57
Carbon DioxideANS20GAX 11/05/19 12:57
Hydrogen A1vI20GAX 11105/19 12:57
Methane, Ethane, Ethcnc (AM20G 4 10/23/19 12:57
Containers Supplied: 1 j
C� l�.�tti i l+t.Clii�
10 Leb•ICI
G�
Rcic:tscd tay
Date Received By
Rd '
cased B Y Date ucceivcd By {` 6t C-�-"
Released -By Date ;iceei:•ed By
• r
Ke;easer'. By Date Received B}'
Uate
Datc
Date
Date /
} Page2of2
4

Cooler Receipt Form
Client Name: i��y. C i Y? Project: ` % 1 ! �` %`j,-" Lab Work Order:
A. Shipping/Container Information (circle appropriate response)
Courier: redEx�% UPS USPS Client Other: Air bill Presen . Yes :No
�' .
7. .�
Tracking Number: 1V
Custody Seal on Cooler/Box Present: Yes LNo f Seals Intact: Yes No
Cooler/Box Packing Material: Bu l,le Wrap Absorbent Foam Other:
-
Type of Ice: /Wet Blue None Ice Intact: f Yes ,Melted
� r
Cooler Temperature: L' Radiation Screened: Yes EO
Chain of Custody Present: Yes No
Comments:
B. Laboratory Assignment/Log-in (check appropriate response)
YES
NO
N/A
Comment
Reference non -Conformance
Chain of Custody properly filled out
Chain of Custody relinquished
Sampler Name & Signature on COC
Containers intact
v
Were samples in separate bags
V
Sample container labels match COC
Sample name/date and time collected
Sufficient volume provided
PAES containers used
L�
Are containers properly preserved for the requested testing?
(as labeled)
If an unknown preservation state, were containers checked?
Exception: VOA's coliform
If yes, see pH form.
Was volume for dissolved testing field filtered, as noted on
the COC? Was volume received in a preserved container?
`—
Headspace present?
Comments:
Cooler contents examined/received by
Date: - - '
Project Manager Review : Date: 02-2s
F-PAE-Q-009-rep-. 01. 3 Oct2017