5802_MadisonCounty_MSWLF_GW_FID1387224_20200108

LLJY--. _H [-]PaperReport [:]Electronic Data - Email CD data loaded: Yes / No Doc/Event #:
' NC DENR Environmental Monitoring
Division of Waste Management - Solid Waste Reporting Form
Notice: This form and any information attached to it are "Public Records" as defined in NC General Statute 132-1. As such, these documents are
available for inspection and examination by any person upon request (NC General Statute 132-6).
Instructions:
• Prepare one form for each individually monitored unit
• Please type or print legibly.
Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification
must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing
condition, etc.).
Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits.
Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the
facility (NCAC 13B .1629 (4)(a)(1).
Send the original signed and sealed fonn, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste
Section, 1646 Mail Service Center, Raleigh, NC 27699-1646.
Solid Waste Monitoring Data Submittal Information
Name of entity submitting data (laboratory, consultant, facility owner):
Anchor QEA of North Carolina, PLLC
Contact for questions about data formatting. Include data preparers name, telephone number and E-mail address:
Name: Alec Macbeth
E-mail: amacbeth(cDanchoraea.com
Facility name: Facility Address:
Madison County Closed Solid 389 Long Branch Road
Waste Facility Marshall, NC 28753
Environmental Status: (Check all that apply)
Initial/Background Monitoring ❑X Detection Monitoring
Type of data submitted: (Check all that apply)
p( Groundwater monitoring data from monitoring wells
Groundwater monitoring data from private water supply wells
I Leachate monitoring data
X� Surface water monitoring data
Phone: [phone]
NC Landfill Rule:
Facility Permit # (.0500 or .1600)
58-02 .0500
❑ Assessment Monitoring
❑
Methane gas monitoring data
Corrective action data (specify)
Other(specify)
Actual sampling dates (e.g.,
October 20-24, 2006)
ctober 17, 2019
Corrective Action
Notification attached?
No. No groundwater or surface water standards were exceeded.
X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water
monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and
preliminary analysis of the cause and significance of any concentration.
❑ Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample
values and explosive methane gas limits.
Certification
To the best of my knowledge, the Informatbin reported and statements made on this data submittal and attachments are true and correct
Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas
levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there
are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment
Alec Macbeth, PG Projec tGeologis t 828-281-3350
Facility Representative Name (Print) Title (Area Code) Telephone Number
az &, 7V -7- �, January 6, 2020 Affix NC Licensed/ Professional Geologist Seal
Signature Date
231 Haywood Street Asheville, North Carolina 28806
Facility Representative Address
P-1649
NC PE Firm License Number (if applicable effective May 1, 2009)
Revised 6/2009

January 2020
Madison County Closed Solid Waste Facility, Permit No. 58-02
ti9
INZANCHOR
QEA
Fall 2019
Semiannual Water Quality Monitoring Report
Prepared for Madison County, North Carolina

January 2020
Madison County Closed Solid Waste Facility, Permit No. 58-02
Fall 2019
Semiannual Water Quality Monitoring Report
Prepared for
Madison County, North Carolina
Post Office Box 579
Marshall, North Carolina 28753
Alec Macbeth, PG
Prepared by
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Project Number: C91500-01.01
\\ashevillel\asheville\Projects\Madison County\Reports\2019\Fall\58-02 - Closed\Text\Fall 2019 Semiannual Water Quality Report _010320.docx

TABLE OF CONTENTS
1 Introduction
2 Methods
1
2
2.1 Monitoring Well Sampling Methods...........................................................................................................2
2.1.1 Monitoring Wells MW-01 OLD, MW-02 OLD, and BG SPRING OLD...............................2
2.1.2 Monitoring Wells MW-03 OLD and MW-04 OLD...................................................................2
2.2 Surface Water Sampling Methods................................................................................................................3
2.3 Domestic Well Sampling Methods...............................................................................................................3
2.4 Sample Handling, Documentation, and Analysis....................................................................................3
3 Findings........................................................................................................................................5
3.1 Groundwater.........................................................................................................................................................5
3.1.1 Field Parameters..................................................................................................................................6
3.1.2 RCRA Metals..........................................................................................................................................6
3.1.3 Appendix I VOCs..................................................................................................................................6
3.2 Surface Water.......................................................................................................................................................6
3.2.1 Field Parameters..................................................................................................................................7
3.2.2 RCRA Metals..........................................................................................................................................7
3.2.3 Appendix I VOCs..................................................................................................................................7
3.3 Site Hydrogeology..............................................................................................................................................7
4 Summary......................................................................................................................................8
4.1 Future Activities...................................................................................................................................................8
5 References...................................................................................................................................9
TABLES
Table 1 Summary of Laboratory Analyses Performed on Samples
Table 2 Summary of Detected Constituents
FIGURES
Figure 1 Site Location Map
Figure 2 Sample Location Map
Fall 2019 Semiannual
Water Quality Monitoring Report i January 2020

APPENDICES
Appendix A Sampling Logs and Equipment Documentation and Instrument Calibration Data
Sheets
Appendix B Report of Laboratory Analysis and Chain -of -Custody Documentation
Fall 2019 Semiannual
Water Quality Monitoring Report ii January 2020

ABBREVIATIONS
µg/L
micrograms per liter
µS/cm
microsiemens per centimeter
213 standard
surface water quality standards defined in 15A NCAC 213
2L standard
groundwater quality standards defined in 15A NCAC 2L .0202
Closed Landfill
closed municipal solid waste landfill
DEQ
North Carolina Department of Environmental Quality
DO
dissolved oxygen
DWM
Division of Waste Management
EPA
U.S. Environmental Protection Agency
IMAC
interim maximum allowable concentration
MDL
method detection limit
mg/L
milligrams per liter
MRL
method reporting limit
mV
millivolt
NCAC
North Carolina Administrative Code
NTU
Nephelometric Turbidity Units
ORP
oxidation reduction potential
RCRA
Resource Conservation and Recovery Act
SC
specific conductivity
SESD
EPA Region 4 Science and Ecosystem Support Division
SU
Standard Units
SWS
Solid Waste Section
TOC
top of well casing
VOC
volatile organic compound
Fall 2019 Semiannual
Water Quality Monitoring Report iii January 2020

Introduction
The Madison County Solid Waste Department maintains a closed municipal solid waste landfill
(Closed Landfill), located near the intersection of U.S. Highway 25/70 Bypass and Long Branch Road
(State Route 1582) in Madison County, North Carolina. The site location is presented in Figure 1.
The Closed Landfill is permitted by the North Carolina Department of Environmental Quality (DEQ),
Division of Waste Management (DWM), under Permit No. 58-02, which requires semiannual
monitoring of groundwater and surface water quality. This report, prepared by Anchor QEA of North
Carolina, PLLC, is being submitted in accordance with monitoring requirements for closed landfills as
stipulated in DEQ DWM Permit No. 58-02 issued to the Madison County Solid Waste Department,
with regulations codified in the DEQ Solid Waste Management Rules, Title 15A, Subchapter 13B,
Section .1600 of the North Carolina Administrative Code (15A North Carolina Administrative Code
[NCAC] 13B .1600).
This report describes the second semiannual groundwater and surface water quality monitoring
event performed in 2019. The water quality monitoring network for the Closed Landfill consists of
four monitoring wells (MW-01 OLD, MW-02 OLD, MW-03 OLD, and MW-04 OLD), a background
groundwater quality sampling location (BG SPRING OLD), and two surface water sampling locations
(SW-01 OLD [upstream] and SW-02 OLD [downstream]) located along Profitt Branch (Figure 2).
Monitoring wells MW-03 OLD and MW-04 OLD are installed in bedrock near the top of a ridge in the
western part of the landfill parcel. Monitoring wells MW-01 OLD and MW-02 OLD are at lower
elevations within topographic drainages in the southern part of the landfill parcel and are screened
in the upper saturated zone.
The water sample collected from background sampling location BG SPRING OLD is treated as a
groundwater sample for the following reasons:
• Groundwater does not discharge to the ground surface at the sampling point.
• Construction of the sampling point is similar to that of a temporary monitoring well and is
located upslope and upgradient of a springhead.
• The sampling point consists of a PVC casing extending below ground surface with a screened
interval from which groundwater is collected and recharges.
Fall 2019 Semiannual
Water Quality Monitoring Report 1 January 2020

2 Methods
Groundwater samples and a surface water sample were collected at the Closed Landfill by
Anchor QEA personnel on October 17, 2019.
2.1 Monitoring Well Sampling Methods
Prior to groundwater sample collection from the monitoring wells, the static water level was
measured and recorded to calculate the well's volume. At each sample location, an initial round of
field parameters (consisting of pH, specific conductivity [SC], dissolved oxygen [DO], oxidation
reduction potential [ORP], turbidity, and temperature) was measured and recorded. Water level
measurements, field parameters, and observations pertaining to water quality are included in the
sampling logs in Appendix A.
2. 7. 7 Monitoring Wells MW-01 OLD, MW-02 OLD, and BG SPRING OLD
Following initial field parameter collection, groundwater monitoring wells MW-01 OLD and
MW-02 OLD and sampling point BG SPRING OLD were each purged using a new disposable
polyethylene bailer. MW-01 OLD and BG SPRING OLD were purged and sampled with a disposable
bailer due to poor well access. MW-02 OLD was purged and sampled with a disposable bailer
because this monitoring well recharges too slowly to be sampled via low -flow methods. As each
consecutive well volume was removed with the bailer, an additional round of groundwater
parameters was recorded. Each well was purged until a minimum of three well volumes had been
removed and field parameters had stabilized, or until the well had been bailed dry. Monitoring well
MW-02 OLD, which was bailed dry after approximately two well volumes had been purged, was
allowed to recharge prior to collecting the groundwater sample.
A groundwater sample was collected by a technician wearing a new pair of non -reactive nitrile
gloves. Each sample was placed directly into laboratory -supplied sample containers.
2. 7.2 Monitoring Wells MW-03 OLD and MW-04 OLD
Monitoring wells MW-03 OLD and MW-04 OLD were purged and sampled with a bladder pump
using low -flow techniques in accordance with the procedures described in Low -Flow (Minimal
Drawdown) Ground -Water Sampling Procedures (Puls and Barcelona 1996). During purging, pH, SC,
DO, ORP, turbidity, and temperature were measured and recorded approximately every 3 minutes.
Well purging continued until these parameters had stabilized for three consecutive readings. The
following required stabilization criteria have been established by the U.S. Environmental Protection
Agency (EPA) Region 4 Science and Ecosystem Support Division Operating Procedure: Groundwater
Sampling (EPA SESD 2017):
• pH values within ± 0.1 unit
Fall 2019 Semiannual
Water Quality Monitoring Report 2 January 2020

• SC values within ± 5%
Temperature, DO, and turbidity values within ± 10%
Following stabilization of these parameters, a groundwater sample was collected by a technician
wearing a new pair of non -reactive nitrile gloves. Each sample was placed directly into
laboratory -supplied sample containers.
2.2 Surface Water Sampling Methods
Surface water samples SW-01 OLD and SW-02 OLD are collected semiannually at designated locations
along Profitt Branch, which flows adjacent to the Closed Landfill's southern boundary in a westerly
direction (Figure 2). The surface water sample collected at the SW-01 OLD location is interpreted to
represent surface water quality upstream of the Closed Landfill, and the surface water sample collected
at the SW-02 OLD location is interpreted to represent surface water quality downstream of the Closed
Landfill. Surface water sample SW-01 OLD was not collected during the fall 2019 sampling event due an
absence of surface water. For the sample SW-02 OLD, one set of field parameters, including
temperature, pH, SC, DO, ORP, and turbidity was measured and recorded at the surface water sampling
location prior to sample collection (Appendix A). The one surface water sample was collected and
transferred into laboratory -supplied sample containers by a technician wearing a new pair of non -
reactive nitrile gloves.
2.3 Domestic Well Sampling Methods
Anchor QEA personnel attempted to contact the resident of the property owned by Mrs. J.V. Edwards
(99 Log Branch Road, Marshall, North Carolina) but was not able to make contact. As such,
Anchor QEA was unable to collect a sample from the water supply well (DW-01) owned by Mrs.
Edwards during the fall 2019 sampling event.
2.4 Sample Handling, Documentation, and Analysis
Field parameters and additional observations pertaining to water quality sampling at the
Closed Landfill sampling locations are provided in the sampling logs in Appendix A. Following
sample collection, groundwater and surface water samples were immediately placed on ice in sample
coolers for transport to Prism Laboratories, Inc. (Prism), a laboratory certified in North Carolina and
located in Raleigh, North Carolina. Anchor QEA submitted all collected groundwater and surface
water samples to Prism for the following analyses:
Appendix I volatile organic compounds (VOCs), using EPA Method 8260B
— Appendix I parameters are identified in Appendix I of the Code of Federal Regulations,
Title 40, Part 258 (40 Code of Federal Regulations 258).
Fall 2019 Semiannual
Water Quality Monitoring Report 3 January 2020

• Eight Resource Conservation and Recovery Act (RCRA) metals, using EPA Methods 601 OD
and 7470A
• 1,4-Dioxane, using method 8260SIM
The North Carolina DEQ, DWM Solid Waste Section (SWS) issued the memorandum "1,4-Dioxane
Analysis, Solid Waste Section Limits, and Laboratory Analytical Methods", dated May 29, 2018, which
requires the analysis of 1,4-dioxane at landfills after July 1, 2018 (DEQ 2018a). Per this memorandum,
1,4-dioxane was included in the sampling suite for site monitoring wells and surface water samples
during the fall 2019 sampling event.
A summary of laboratory analyses performed on the samples is provided in Table 1. Trip blanks,
provided by the laboratory and stored in each sample cooler, were analyzed for Appendix I VOCs
and 1,4-dioxane. Proper chain -of -custody documentation procedures were followed during
collection and transport of each sample. The laboratory analytical reports and chain -of -custody
documentation are included in Appendix B.
Fall 2019 Semiannual
Water Quality Monitoring Report 4 January 2020

3 Findings
The field parameter data and laboratory analytical results for the groundwater, surface water, and
trip blank samples collected at the Closed Landfill are included in Appendices A and B, respectively,
and are also submitted separately to the DEQ DWM SWS in the Electronic Data Deliverable format
(DENR 2014).
All laboratory analytical results were reported and appropriately qualified as follows:
• Non -Detections: Non -detections are values reported by the laboratory as "below method
detection limits (MDLs)" and are flagged with a "U" qualifier in Table 2. The MDL is the
minimum concentration of a substance that can be measured and reported by a laboratory
with 99% confidence that the constituent concentration is greater than zero.
• Estimated or "J" Qualified: A "Y' qualifier is used by the laboratory for parameters that are
detected at estimated concentrations greater than the MDL but less than the laboratory's
method reporting limit (MRL). The MRL is the minimum concentration of a target analyte that
can be accurately determined by the referenced method.
• Groundwater Quality Standards: Detected concentrations of constituents in groundwater
samples were compared to applicable North Carolina groundwater quality standards. For
most constituents, this standard is the 2L standard, defined in 15A NCAC 02L .0202. Detected
concentrations of analytes in groundwater with no established 2L standard were compared to
the interim maximum allowable concentrations (IMAC) for Class GA and GSA groundwater (in
accordance with 15A NCAC 02L .0202). For the purposes of this report, groundwater
standards were taken from the October 15, 2018 list published by the North Carolina SWS
(DEQ 2018b).
• 2B Standard: Detections of analytes in surface water samples were compared to the surface
water quality standards described in 15A NCAC 02B (213 standards). Hardness -dependent
2B surface water standards were calculated using the average analyzed hardness value
(calculated from the upstream and downstream surface water sampling location results) via
the most stringent hardness -dependent metal calculation.
Table 2 summarizes the field parameter results and laboratory analytical results for detected
constituents. The following discussion outlines constituents detected at concentrations that
exceeded their respective groundwater quality standards or 2B standards.
3.1 Groundwater
The following sections summarize the results of field parameter and laboratory analyses of
groundwater samples collected on October 17, 2019.
Fall 2019 Semiannual
Water Quality Monitoring Report 5 January 2020

3.7. 7 Field Parameters
The pH readings obtained from monitoring wells MW-01 OLD, MW-03 OLD, and BG-SPRING OLD
(6.07 to 6.48 Standard Units [SU]) were less than the range for pH (6.5 to 8.5 SU) specified in the
2L standard (Table 2). The pH readings obtained from monitoring wells MW-02 OLD (7.06) and
MW-04 OLD (6.57) were within the 2L standard.
Turbidity in the monitoring wells ranged from 1.92 Nephelometric Turbidity Units (NTUs) in
monitoring well MW-03 OLD to 98.3 NTUs in MW-01 OLD. Measured DO values ranged from
0.58 milligrams per liter (mg/L) in MW-03 OLD to 7.66 mg/L in MW-02 OLD. Specific conductivity
values ranged from 154.9 microsiemens per centimeter (pS/cm) in BG-SPRING OLD to 1,007 pS/cm in
MW-03 OLD. ORP values in the monitoring wells ranged from -29.3 millivolts (mV) in MW-03 OLD to
151.9 mV in BG-SPRING OLD (Table 2). These parameters do not have established groundwater
quality standards. Concentrations of field parameters are generally consistent with historical
concentrations.
3.7.2 RCRA Metals
Four metals (arsenic, barium, chromium, and lead) were detected in groundwater samples collected
from one or more monitoring wells (Table 2). Except for barium, these detections were all estimated
concentrations (J-flagged) and occurred in a maximum of two of the wells. Only barium exceeded its
2L standard of 700 micrograms per liter (pg/L) in the samples collected from two monitoring wells,
MW-03 OLD (920 pg/L) and MW-04 OLD (720 pg/L). Barium was also detected at 130 pg/L in the
background sampling location, BG SPRING OLD.
3.7.3 Appendix 1 VOCs and 7,4-Dioxane
Twelve VOCs were detected in groundwater samples collected from one or more of the
monitoring wells (Table 2). Of the detected compounds, three (1,4-dichlorobenzene, 1,4-dioxane,
and vinyl chloride) were detected at concentrations above the associated groundwater quality
standard. These exceedances occurred in a single monitoring well, MW-01 OLD, as follows:
• 1,4-Dichlorobenzene at 6.0 pg/L
• 1,4-Dioxane at 9.0 pg/L
• Vinyl chloride at 0.96 pg/L
The VOC detections are generally consistent with historical data.
3.2 Surface Water
The following sections summarize the results of laboratory and field parameter analyses of surface
water sample SW-02 OLD.
Fall 2019 Semiannual
Water Quality Monitoring Report 6 January 2020

3.2. 7 Field Parameters
The pH reading collected from SW-02 OLD was 8.01 SU. The reading was within the 2B standard
range established at 6.0 to 9.0 SU. The turbidity reading collected from SW-02 OLD was 2.74 NTUs.
The reading was below the 2B standard of 50 NTUs. The DO reading collected from SW-02 OLD was
11.28 mg/L. The value is within the 2B standard for Class C waters (greater than or equal to
5.0 mg/L). The SC measurement in SW-02 OLD was recorded at 186.4 pS/cm. The ORP value for this
sample was recorded at 113.1 mV (Table 2). These parameters do not have established surface water
quality standards.
3.2.2 RCRA Metals
One metal was detected in the surface water sample collected at SW-2 OLD. Barium was detected at
a concentration (46 pg/L) less than its respective 2B standard in SW-02 OLD (Table 2).
3.2.3 Appendix 1 VOCs
Acetone was detected in the sample collected from SW-02 OLD at 6.0 pg/L, which is below the
2B standard of 2,000 µg/L. Acetone is a common laboratory artifact. No other VOCs were detected in
the surface water sample.
3.3 Site Hydrogeology
Groundwater levels were measured in the four monitoring wells, MW-01 OLD, MW-02 OLD,
MW-03 OLD, and MW-04 OLD, at the Closed Landfill at depths of 6.39, 8.16, 42.42, and 43.33 feet
below the top of the well casing (TOC), respectively (Appendix A).
The spatial distributions and screened intervals of the monitoring wells at the Closed Landfill prohibit
an accurate calculation of groundwater flow direction. However, within the upper saturated zone, the
shallow groundwater is interpreted to generally mimic topography, flowing primarily southward
toward Profitt Branch. The Closed Landfill is situated on the southwest side of a knoll with an
elevation of approximately 2,100 feet above mean sea level and slopes downward toward
Profitt Branch.
Fall 2019 Semiannual
Water Quality Monitoring Report 7 January 2020

4 Summary
Anchor QEA completed the second semiannual water quality monitoring event of 2019 at the
Closed Landfill on October 17, 2019. Table 1 summarizes the sampling and analyses that were
performed. Table 2, the field sampling logs (Appendix A), and the Prism Reports of Laboratory Analysis
(Appendix B) provide detailed analytical results and field data related to groundwater and surface water
quality at the Closed Landfill. The following bullets summarize the results of the sampling event:
• The detected concentration of barium exceeded its 2L standard of 700 pg/L in the samples
collected from two of the monitoring wells, MW-03 OLD (920 pg/L) and MW-04 OLD
(720 pg/L). Barium was also detected in the background monitoring well at 130 pg/L.
• Three VOCs, 1,4-dichlorobenzene (6.0 pg/L), 1,4-dioxane (9.0 pg/L), and vinyl chloride
(0.96 pg/L) were detected in the sample collected from MW-01 OLD at concentrations
exceeding the associated groundwater quality standards (2L standards). These detections are
comparable to analytical results since spring 2018.
• The measured depths to groundwater in the upper saturated zone within the topographic
drainages at the landfill ranged from 6.39 to 8.16 feet below TOC. The groundwater depths in
the bedrock monitoring wells at top of the ridge ranged from 42.42 to 43.33 feet TOC. The
shallow groundwater is interpreted to generally mimic topography, flowing primarily
southward toward Profitt Branch.
4.1 Future Activities
Anchor QEA will continue to measure field parameters and collect water quality samples from
groundwater and surface water monitoring points associated with the Closed Landfill. Water quality
samples will be submitted to a North Carolina -certified laboratory for analysis of RCRA metals and
Appendix I VOCs, including 1,4-dioxane, on a semiannual basis. The next sampling event is scheduled
for March 2020.
Fall 2019 Semiannual
Water Quality Monitoring Report 8 January 2020

5 References
DENR (North Carolina Department of Environmental and Natural Resources, Division of Waste
Management), 2014. Memorandum Re: Groundwater, Surface Water, Soil, Sediment, and
Landfill Gas Electronic Document Submittal, November 5, 2014.
DEQ (North Carolina Department of Environmental Quality), 2018a. Memorandum to: Solid Waste
Directors, Landfill Owners/Operators, and North Carolina -certified Laboratories. Regarding:
1,4-Dioxane Analysis, Solid Waste Section Limits, and Laboratory Analytical Methods.
May 29, 2018.
DEQ (North Carolina Department of Environmental Quality), 2018b. "Groundwater Protection
Compliance Standards — Constituents List". Last modified October 15, 2018. Available at:
https://edocs.deq.nc.gov/WasteManagement/0/edoc/l257181/SWS EnviroMonitoring Const
ituents List.pdf?searchid=13f8efbl-eel 1-485a-b03f-718f2287b271
EPA SESD (U.S. Environmental Protection Agency Science and Ecosystem Support Division), 2017.
Operating Procedure: Groundwater Sampling. April 26, 2017.
Puls, R.W., and M.J. Barcelona, 1996. Low -Flow (Minimal Drowdown) Ground -Water Sampling
Procedures. Prepared for the U.S. Environmental Protection Agency, Office of Solid Waste and
Emergency Response. EPA/540/5-95/504. April 1996.
Fall 2019 Semiannual
Water Quality Monitoring Report 9 January 2020

Tables

Table 1
Summary of Laboratory Analyses Performed on Samples
Groundwater Samples
Facility Permit
Well ID
Collect Date
Appendix I VOCs and
1,4-Dioxane
RCRA Metals
EPA 8260B & 8260B
SIM
EPA 6020B
EPA 7470A
58-02
MW-01 OLD
10/17/2019
X
X
58-02
MW-02 OLD
10/17/2019
X
X
58-02
MW-03 OLD
10/17/2019
X
X
58-02
MW-04 OLD
10/17/2019
X
X
58-02
BG SPRING OLD
10/17/2019
X
X
Surface Water Samples
Appendix I VOCs and
RCRA Metals
Total Hardness
1,4-Dioxane
EPA 8260B & 8260B
EPA 6020B
Facility Permit
Sample ID
Collect Date
SIM
EPA 7470A
EPA SM 2340C
58-02
SW-02 OLD
10/17/2019
X
X
X
Quality Control Samples
Facility Permit
Sample ID
Collect Date
Appendix I VOCs and
1,4-Dioxane
EPA 8260B & 8260B
SIM
58-02
TRIP BLANK (MW OLD)
10/17/2019
X
58-02
TRIP BLANK (SW OLD)
10/17/2019
X
Notes:
Analyses include Appendix I constituents per the Code of Federal Regulations (40 CFR Part 258).
A sample could not be collected from the Edwards's residence domestic water supply sample, DW-01 OLD, during this sampling event.
A sample could not be collected from the upstream surface water sampling location, SW-01 OLD, during this sampling event, because of absence of surface water.
EPA: U.S. Environmental Protection Agency
RCRA: Resource Conservation and Recovery Act
SM: standard method
SIM: selective ion monitoring
VOC: volatile organic compound
Fall 2019 Semiannual Water Quality Monitoring Report Page 1 of 1
Madison County Closed Municipal Solid Waste Landfill, Permit Number 58-02 January 2020

Table 2
Summary of Detected Constituents
Lab Certification
Metals
402
Hardness
402
VOCs (Appendix 1)
402
Lab Method
EPA 6020B & 7470A
SM 2340C
EPA 8260B
& 8260B SIM
Parameter
Arsenic
Barium
Chromium
Lead
Hardness
Acetone
Benzene
Chlorobenzene
Chloroethane
cis-1,2-
Dichloroethylene
1,2-Dichlorobenzene
1,4-Dichlorobenzene
1, 1 -Dichloroethane
1,2-Dichloropropane
CAS Number
7440-38-2
7440-39-3
7440-47-3
7439-92-1
NA
67-64-1
71-43-2
108-90-7
75-00-3
156-59-2
95-50-1
106-46-7
75-34-3
78-87-5
SWS ID
14
15
51
131
NA
3
16
39
41
78
69
71
75
82
Units
Ng/L
I Ng/L
Ng/L
Ng/L
Ng/L
Ng/L
Ng/L
Ng/L
Ng/L
I Ng/L
Ng/L
Ng/L
Ng/L
Ng/L
Sample ID
Collect Date
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Monitoring Well Samples
MW-01 OLD
10/17/2019
0.52 J
550
2.3 J
0.69 J
NA
0.70 U
0.82
4.0
1.8
3.4
0.72
6.0
1.1
0.32
MW-02 OLD
10/17/2019
0.34 U
50
0.90 U
0.44 U
NA
6.1
0.34 U
0.34 U
0.43 U
0.40 U
0.28 U
0.42 U
0.94
0.29 U
MW-03 OLD
10/17/2019
0.34 U
920
0.90 U
0.44 U
NA
8.0
0.89
5.3
0.85
0.67
0.45 J
0.42 U
0.29 U
0.29 U
MW-04 OLD
10/17/2019
0.34 U
720
0.90 U
0.44 U
NA
18
0.34 U
2.4
0.87
0.40 U
0.28 U
1.2
0.29 U
0.29 U
BG SPRING OLD
10/17/2019
0.34 U
130
2.5 J
0.49 J
NA
6.5
0.34 U
0.34 U
0.43 U
0.40 U
0.28 U
0.42 U
0.29 U
0.29 U
Surface Water Samples
SW-02 OLD
10/17/2019
0.34 U
46
0.90 U
0.44 U
56,000
6.0
0.34 U
0.34 U
0.43 U
0.40 U
0.28 U
0.42 U
0.29 U
0.29 U
Quality Control Sample
TRIP BLANK (MW OLD)
10/17/2019
NA
NA
NA
NA
NA
3.6 J
0.34 U
0.34 U
0.43 U
0.40 U
0.42 U
0.29 U
TRIP BLANK (SW OLD)
10/17/2019
NA
NA
NA
NA
NA
4.0 J
0.34 U
0.34 U
0.43 U
0.40 U
0.28 U
0.42 U
0.29 U
0.29 U
MDL
0.34
3.2
0.90
0.44
570
0.70
0.34
0.34
0.43
0.40
0.190
0.42
0.29
0.250
MRL
1.0
10
3.0
1.0
5,000
5.0
0.50
0.50
0.50
0.50
1.00
0.50
0.50
1.00
2L
10
700
10
15
NE
6,000
1
50
3,000
70
20
6
6
0.6
IMAC
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
213
10
21,000
46.10*
1.33"
NE
2,000
51
800
NE
720
3,000
900
100
31
Fall 2019 Semiannual Water Quality Monitoring Report Page 1 of 3
Madison County Closed Municipal Solid Waste Landfill, Permit No. 58-02 January 2020

Table 2
Summary of Detected Constituents
Lab Certification
VOCs (Appendix 1)
402
Field Parameters
5445 (pH, Dissolved Oxygen, Specific Conductivity, and Temperature only)
Lab Method
EPA 8260B & 8260B SIM
Parameter
1,4-Dioxane
o-Xylene
Trichloroethylene
trans-1,2-
Dichloroethene
Vinyl Chloride
Total
Xylenes
pH
Turbidity
Dissolved
Oxygen
Temperature
Specific
Conductivity
Oxidation
Reduction
Potential
CAS Number
123-91-1
95-47-6
79-01-6
156-60-5
75-01-4
1330-20-7
SW320
SW330
SW356
7782-44-7
SW323
SW336
SWSID 422
408
201
79
211
1 346
320
330
1 356
325
323
336
Units Ng/L
Ng/L
Ng/L
Ng/L
Ng/L
Ng/L
SU
NTU
mg/L
°CI
PS/cm
mV
Sample ID
Collect Date Result
Result 4-Result
Result
Result
Result
Result
Result
Result
Result
Result
Result
Monitoring Well Samples
MW-01 OLD
10/17/2019
9.0
0.40 U
0.46 J
0.33
0.96
1.1 U
6.37
98.3
2.21
15.4
789
33.2
MW-02 OLD
10/17/2019
0.14 U
0.40 U
0.46 U
0.27 U
0.41 U
1.1 U
7.06
9.95
7.66
15.1
216.0
129.9
MW-03 OLD
10/17/2019
0.14 U
0.40 U
0.46 U
0.27 U
0.41 U
1.1 U
6.48
1.92
0.58
15.1
1,007
-29.3
MW-04 OLD
10/17/2019
1.0 J
0.45 J
0.46 U
0.27 U
0.41 U
1.1 J
6.57
3.43
2.62
19.4
885
38.1
BG SPRING OLD
10/17/2019
0.14 U
0.40 U
0.46 U
0.27 U
0.41 U
1.1 U
6.07
27.2
1.40
16.8
154.9
151.9
Surface Water Samples
SW-02 OLD
10/17/2019
0.14 U
0.40 U
0.46 U
0.27 U
0.41 U
1.1 U
8.01
2.74
11.28
11.5
186.4
113.1
Quality Control Sample
TRIP BLANK (MW OLD)
10/17/2019
0.14 U
0.40 U
0.46 U
0.41 U
1.1 U
NA
NA
NA
NA
NA
NA
TRIP BLANK (SW OLD)
10/17/2019
0.14 U
0.40 U
0.46 U
0.27 U
0.41 U
1.1 U
NA
NA
NA
NA
NA
NA
MDL
0.14
0.40
0.46
0.230
0.41
1.1
NA
NA
NA
NA
NA
NA
MRL
2.0
0.50
0.50
1.00
0.50
1.5
NA
NA
NE
NE
NE
NE
2L
3
500
3
100
0.03
500
6.5-8.5
NE
NE
NE
NE
NE
IMAC
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
NE
2B
80
600
30
4,000
2.4
670
6.0-9.0
50
_> 5.0
NE
NE
NE
Fall 2019 Semiannual Water Quality Monitoring Report Page 2 of 3
Madison County Closed Municipal Solid Waste Landfill, Permit No. 58-02 January 2020

Table 2
Summary of Detected Constituents
Notes:
Only detected constituents are listed in this table. Please refer to the Prism laboratory analysis reports (Appendix B) for further details.
Shaded cell: indicates a result in exceedance of the 2L, IMAC, or 2B standard
Ng/L: micrograms per liter
pS/cm: microsiemens per centimeter
213: surface water standard, per North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2B - Surface Water and Wetland Standards (last
amended September 2017), or standard obtained from National Criteria per EPA table (current as of May 15, 2013)
2L: groundwater standard, per North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2L - Groundwater Classifications and Standards (last
amended October 15, 2018)
CAS Number: a unique number assigned by the Chemical Abstracts Service (CAS) to all identified parameters
Collect Date: the date on which the sample was collected in the field
EPA: U.S. Environmental Protection Agency (method)
IMAC: interim maximum allowable concentration, per Appendix 1 of the 2L standards
J: a laboratory data qualifier used for parameters detected at estimated concentrations above MDL but below MRL
Lab Method: the analytical method used to analyze the constituents
MDL: method detection limit, which is the minimum concentration of a substance that can be measured and reported with 99 percent confidence that the analyte concentration is
greater than zero
mg/L: milligrams per liter
MRL: method reporting limit, which is the minimum concentration of a target analyte that can be accurately determined by the referenced method
mV: millivolt
NA: not applicable
NE: not established
NTU: Nephelometric Turbidity Unit
Result: analytical data reported by the laboratory, or field data collected by Anchor QEA
SM: Standard Method
SU: Standard Unit
SWS ID: Solid Waste Section identification number
U: laboratory data qualifier used for parameters not detected at concentrations above MDL
VOC: volatile organic compound
*: 2B surface water standard calculated using average analyzed hardness value (calculated from the upstream and downstream sampling location results) via the most stringent hardness -
dependent metal calculation, per North Carolina Administrative Code, Title 15A: Department of Environmental Quality, Subchapter 2B - Surface Water and Wetland Standards (last
amended September 2017).
Fall 2019 Semiannual Water Quality Monitoring Report Page 3 of 3
Madison County Closed Municipal Solid Waste Landfill, Permit No. 58-02 December 2019

Figures

J V
f� pftp. .i
CEnr gip-\•e
r J', \� f 11Madieoa Se
ca
Woe
\C\
C-
�: V C
�� � � I �tr!^i ♦ a �
LEGEND: SOURCES:
Basemap: USGS 1:24,000 Scale Topo Maps, Marshall 0 2,000
® Landfill Parcel Quadrangle, 1990
Parcels: Madison County GIS Feet
Publish Date: 2019/12/03, 7A6 PM I User: cpatterson
Filepath: Q:Vobs\MadisonCounty_NC_1500\Maps\2019\FallWaterQualityWQF01-Site Location Map -Closed LF_FaIIWQ2019.mxd
ANCHOR Figure 1
QEA- Site Location Map
Anchor QEA of North Carolina, PLLC
Fall 2019 Semiannual Water Quality Report
Madison County Closed Municipal Solid Waste Landfill, Permit No. 58-02

Publish Date: 2019/12/05, 3:38 PM I User: cpatterson
Filepath: Q:Vobs\MadisonCounty_NC_1500\Maps\2019\FallWaterQualityWQF02_SampleLocationMap_ClosedLF_FaIIWQ2019.mxd
kzANCHOR Figure 2
QEA�- Sample Location Map
Anchor QEA of North Carolina, PLLC
Fall 2019 Semiannual Water Quality Report
Madison County Closed Municipal Solid Waste Landfill, Permit No. 58-02

Appendix A
Sampling Logs and Equipment
Documentation and Instrument
Calibration Data Sheets

ANCHOR
Well Sampling Lo
p 9 9 .Date: IA((-7 l l5 Well Name:
Project Name:. MalisOv) a C owd, P—
Project Number. r,d O2 Weather.
Sampling Personnel: U c ,
t 6 ,� 3--r� Sample Time:
Well Information: Well Depth in Feet (WD): 20.
Well Diameter: lIM Water Level in Feet (WL): . 3 Y
Type of Casing: _�� Length of Water Column; V feet
Screen Interval: Qi. (WD) -(WL) = (LWC)
Flush Moun Stick- p One Casing Volume: 45
gallons
Comments: (LWC) x (WM
Three Casing Volumes: 7 ,� gallons
Tagged p
bottom at ' O Actual Volume Purged: �, �� 5 gallons
Z. E j
Notes:
Samples are analyzed immediately upon collection.
°C: degrees Celsius
pS/cm: micro-Siemen per centimeter
mg/L milligrams per liter
mV: millivolt
NTU: nephelometric turbidity units
S.U: Standard Units
Protective Casing: Pad: Lock Vegetation: —W Access:
Sampling Personnel Signature: Date: `1%1
initial if well information and sampling data has been verified
well was tagged after sampling was complete

ANCHOR
QEA; AL.4..AL..e
y Well Sampling Log Date: j'� f'I Well Name: KAW—d 2 o LC)
Project Name: IV AIA ism a. uowd,
Project Number. CKGDO — Q I , -r 0- O 2,
Weather.
Sampling Personnel: �. ((� —y'-Y Sample Time:
Well Information:
Well Depth in Feet (WD):
Well Diameter.
Water Level in Feet (WL):
Type of Casing: vG
Length of Water Column;
feet
Screen Int I: OL
(WD) - (WL) = (LWC)
Flush Mount Stick-U
One Casing Volume:
°.
gallons
Comments:
(LWC) x (WCV)
Three Casing Volumes:
'" 1
gallons
Tagged
bottom at:
Actual Volume Purged:
^. f Z
_
gallons
Notes:
Samples are analyzed immediately upon collection.
degrees Celsius
pS/cm: micro-Siemen per centimeter
R
mg/L: milligrams per liter
mv: millivolt
NTU: nephelometric turbidity units
S.U.: Standard Units
LProtective Casing: l Pad: _ Lock _ / Vegetation: J Access:
Sampling Personnel Signature: LIIL--�'11 �J �Date:
initial if well information and sampling data has been verified
well wastagged after sampling was complete

, ANCHOR
GEA
f 4 Well Sampling Log
Date: I d
Well Name:
I tl(a 6LD
Project Name: MM ISM Gj, CLOW,
k_�
Project Number. C� Sd � — Q `
Z Weather
Sampling Personnel: C.LdAd,iLx � f C
L
_' Sample Time:
1 5�
Well Information:
Well Depth in Feet (WD):
1(4.2,5
Well Diameter
Water Level in Feet (WL):
(4 , 7 3
Type of Casing: P
Length of Water Column: W 'L,
_
feet
Screen Interval: y` D�.
(WD) - (WL) = (LWC)
Flush Mount Stick-up
One Casing Volume:
/
0. % 10
gallons
Comments:
(LWC) x (WCV)
Three Casing Volumes:
2
gallons
Tagged /� r i
bottom at: 10 10
Actual Volume Purged:
l.�
gallons
/'
Notes:
Samples are analyzed immediately upon collection.
°C degrees Celsius
pS/cm: micro-Siemen per centimeter
mg/L: milligrams per liter
mv: millivolt
NTU: nephelometric turbidity units
S.0 : Standard Units
Protective Casing: Pad: Lock Vegetation: Access:
Sampling Personnel Signature: Date:
initial if well information and sampling data has been verified _
well was tagged after sampling was complete

ANCHOR
Low -Flow Sampling Log
Date: a7 ` 1.Well Name: f111W :05 ®(,D
1 Project Name: t,;OACO_ Gloirc
Project Number. djzlGJQO. 0
'SAS 6�1
Location:MOOSkal NG
Personnel: C
iNfY�
Well Information:
Screen Interval: �bgs
Arrive at Well: ,-
Depth to Watery24
tot
Start Time: �3
Well Diameter. , in
Sample Time: i q
Pump Intake: N Lis toc
Finish Sample Time: 3S.
Drawdown Set: L toc
Leave Well:
Pump Used (circle): Peri�ZBIad,,.erOther (description):Comments:
•LA/1—
Purge hate:
Z d 11t���Wu1�t
Tagged bottom at: -,2 M
Total Purge Volume:
Pump.Speed:
ft-
DTW
Temp
DO
Specific Cond.
PH ($.U.)
ORP
Turbidity
i
Tune
(feet)
A'Cj:
`�n!9�) ._
f+5)
r orExa7'.:
[vmrrrenis
-
t33X
.TL
uo
4.4
42. i�?
IS7,
d &
co l
(0a.L
Time between rechTr9e during sample collection:
Sampling Personnel Signature:
Date: IbIl —1 el
Notes:
Stabilization
3 successive readings, 3 minutes apart:
within +/- 10% DO and turbidity, +/- 3% Conductivity, +/- 0.1 pH unit +/- 10 mV lbr ORP
from EPA - Cow -Flow (Minimal Drowdown) Groundwater Sampling Procedures, April 1996 (Rev 2010)
Samples are analyzed immediately upon collection.
pS: micro-Siemen mv: millivolt
°C: degrees Celsius NTU: nephelometric turbidity units
bgs: below ground surface ORP: oxidation reduction potential
DO: dissolved oxygen S.U.: standard units
mg/L• milligrams per liter toc: top of casing
initial if well information and sampling data has been verified
�., ,
_
well was tagged after sampling was complete _

I
ANCHOR
QEA
Low -Flow Sampling Log
Date: to
I
Well Name: MW 0
Project Name: tr60AQ _ C(D�<A LF
Project Number �t
15oa - O 1. D iAs 6
Location: VS 1 WC,
Personnel: r'�D 4G�
+�
Weather.
1400- swyl f
Well Information:
Screen Interval: —61 bgs
—
Arrive at Well:
Depth to Water. a toc
Start Time:
Well Diameter `� in
Sample Time:
Pump Intake: ti'�M _ toc
Finish Sample Time:.J 316
Drawdown Set: , 13, t toc
Leave Well:
(3 2 0
Pump Used (circle): Peristaltic Bladder. Other (description):
Comments:
Purge Rate:
Tagged bottom at: [
Total Purge Volume:
Pump Speed:
PTVif
TOM
DO
Specific Cond. E
pM (S U.)
ORP
Turbidity,
Tme
Meet)
d
y
{rlsg/L}
{}tS)
rep""I to 0.1.
mn
5L1
'L
C -72t
io
L5?- a
�y
�. z7'
70
3' 7
..:�b.
L43 `
^ .Ion
-7
collection:
Sampling Personnel Signature: �� Date:
Notes: 111
Stabilization
3 successive readings, 3 minutes apart
within +/- 10% Do and turbidity; +/- 3% Conductivity; +/- a I PH unit; +/- 10 mV for ORP
from EPA - Low -Flow (Minlmol Drowdown) Groundwater Sampling Procedures, April 1996 (Rev 2010)
Samples are analyzed immediately upon collection.
NS: micro-Siemen mv: millivolt
T. degrees Celsius NTU: nephelometric turbidity units
bgs: below ground surface ORP: oxidation reduction potential
DO: dissolved oxygen S.U.: standard units
mg/L: milligrams per liter toc: top.of casing
initial if well information and sampling data has been verified _
well was tagged after sampling was complete _
M
Comments

AW�N++ ��CHOR
Project Name
Project Number. C Q o (_ o f n-, 02- l
Sampling Personnel:
Sample Name: ��/�l.(y ( O Lp
Comments: ri AhA
Date: (UJ 17
Weather GI)/
Sample Method: Grab Syringe Pump Bailer•Div.
DiddWon
Reduction Spec#f~ic coed. I tikyiyan pH ts.ii.) �luction
Tame CQ ll�s) i { rtglL} report to 0. T S.U.. Potential JmV)
I
I
Sampling Container_ Numberoi; Gontalneri
500 mL Plastic
• l
250 mL Plastic
12.5 mL Plastic
i
40 mL Glass
1 L Glass
Outer
Vegetation:
Sampling Personnel Signature:
Notes:
P& micro-Siemen per cubic centimeter
°C: degrees Celsius
mg/L• milligrams per liter
mV: millivolt
NTU: nephelometric turbidity units
S.U.: standard units
Other:
Requested Analysis
Access:
Turbidity ..
(#sTU)
Date: t C—
Method Reference:
Temperature: SM 2550 B-2010
Specific conductivity: EPA Method 120.1, Rev.1982
DO: SM 4500 O G-2011
pH: SM 4500-H' B-2011
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28901
Comresetsis
Page 1 of 1

ANCHOR
Surface Water Sampling tog
Project Name:Madd�f3Y160 Cl04eoc UF
Project Number C[ (J 66 0-2—
Samplirig Personnel: L �G. .
Sample Name: wbtlp
Comments:
U
Vegetation:
F"1
Sampling .Personnel Signature:
Notes:
Samples are analyzed immediately upon collection.
'C: degrees Celsius
ps/cm: micro-Siemen per cubic centimeter
mg/L: milligrams per liter.
my millivolt
NTU: nephelometric turbidity units
S.U.: standard units
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
Date: tp ' C17 h .`l..
Weather.
i if , f e� ado oN e, cukv"/ —
Access:
„�- Date:
i
Method Reference:
Temperature: SM 2550 B-2010
Speck conductivity: EPA Method 120.1, Rev.1982
DO: SM 4500 0 G-2011
PH: SM 4500-H' B-2011
Page 1 of 1

I jR ANCHOR
V.� QEA��.4.��
Surface Water Sampling Log
Project Name: j�/1a� ClyS.eo� UV:7 Date:
Project Number. ; Weather
Sampling Personnel: v rP
Sample Name: 6 L6,
Comments: Ja"s�``e�
DVI-Ol DLO.
Sample Method: Grab Syringe Pump Bailer-Disp.
Time. � %mp f•C IGxygeftn �yay �. � Aific Ccuxi. � rF rH o D, f 5, iJr_ .�' P Rntial�(ml
Other
Turt�ldlty .
(NIrU)
IN55 � H.5 I II.ZS � 186.4 1 g.G/ 1 /15.1 1,2-11�1
Vegetation: Access:
Sampling .Personnel Signature: pate:
Notes: Method Reference:
Samples are analyzed immediately upon collection. Temperature: SM 2550 B-2010
°C: degrees Celsius Speck conductivity: EPA Method 120.1, Rev. 1982
pS/cm: micro-Siemen per cubic centimeter DO SM 4500 O G-2011
mg/L milligrams per liter. pH: SM 4500-H ` B-2011
mV: millivolt
NTU: nephelometric turbidity units
S.U.: standard units
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
9;
Comments
Page 1, of 1

ANCHOR
4-1
QEA 4L-4C-1
Equipment Documentation and Instrument Calibration Data Sheet
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville, North Carolina 28801
1/ r
CALIBRATION DOCUMENTATION
Project Name:. s�1.';e)n 6" %_w .,o/,dya /e Person Conducting Calibration: 0krt,�"? t
Project Number. -�jl r ' f ,0 _ Date of Calibration:
Project Location: /bq{ _J��Ml Date of Field Measurements: Ft7 d f'i
Equipment or meters used to take measurements (e.g., water level meters, survey equipment):
Equipment Type
Serial Number
Brand
Date of Use
150-ft Water Level
26154
Solinist
150-ft Water Level
22754
Solinist
150-ft Water Level
150
Testwell
150-ft Drawdown
MP30-1527
QED
Other
Select Turbidimeter.
Hach 2100Q (s/n 151006045207)
HF Scientific MicroTPW (s/n 200601045)
Calibration
Expiration Date:
Instrument Reading
(Hach 2100Q)
Instrument Reading
(HF Scientific MicroTPIM1�
20 NTU
100 NTU
800 NTU
1,000 NTU
10.0 NTU
0.02 NTU
C'/-v.2 v
z, Z(:ev
q 17,3 v
Cal-Rl1 �f
GV ld L%.
Cal-
/ l� / v1b�tJL1
Cal: y
i.1 c/o
Cal:
Cal:
Cal:
Time,-,
V
Time
Timer J�u
Time:
Time:
Time:
Verification (10 NTU):In* j
Verification:
Verification:
Verification:
Time: 10 NTU Cal. piration Date:
lI 6 2 6 A U
Time:
Time:
Time:
rvoies:
1. Electronic equipment calibrated according to the manufacturer's operation manual,
2. Specific Conductivity should be calibrated according to values representative of historic range.
3. Order of Calibration is as follows: Specific Conductivity, pH 7, pH 4, pH 1Q DO, ORP, QC checks.
4. QC Acceptable Ranges: pH +/- 0.1 S.U. and Specific Conductivity 10% of the true value. If QC readings are out of range, the instrument needs to be recalibrated.
5. * Indicates that a QC check must be performed in the morning, afternoon, and the end of the day, or every four hours.
6. ** Indicates to choose a Specific Conductivity buffer of 1413, 447, 84, or 23 mS which is closest to historical readings from the project location.
Method Reference: Temperature: SM 2550 8-2010 I Specific conductivity: EPA Method 120.7, Rev. 1982 1 DO: SM 4500 O G-2017 I pH: SM 4500-H+ 8-2071
Page 1 of 1

ANCHOR
4 QEA
Equipment Documentation and Instrument Calibration Data Sheet
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Asheville. North Carolina 28801
4�] / CALIBRATION DOCUMENTATION 1
Project Name: /V,�dl`sp/) . &aAA ,. ob'd L✓asle Person Conducting Calibration: I-Ar &-Han ie �/�/��►
Project Number: CV 50 U — 0/. 1 Date of Calibration: /("J /� _2(j,/Q
Project Location: ��Ql SIs¢ f f N�� Date of Field Measurements: /0/ j4120—)—?
EQUIPMENT DOCUMENTATION
Equipment or meters used to take measurements (e.g., water level meters, survey equipment):
Equipment Type
Serial Number
Brand
Date of Use
150-ft Water Level
26154
Solinist
150-ft Water Level
22754
Solinist
150-ft Water Level
150
Testwell
150-ft Drawdown
MP30-1527
QED
Other
Select Turbidimeter.
Hach 2100Q (s/n 151006045207)
HF Scientific MicroTPW (s/n 200601045)
Instrument Reading
Instrument Reading
(Hach 2100Q)
(HF Scientific MicroTPW)
Calibration
20 NTU
100 NTU 800 NTU
1,000 NTU
10.0 NTU
0.02 NTU
Expiration Date:
1200
Cal: ,
612020 202�
Cal: Cal:
/ IOu 800 0
Cal:
Cal:
Cal:
Time:
755
Time: Time: �5S
756
Time:
Time:
Time:
Verification (10 NTU): /0. 7
Verification:
Verification:
Verification:
Timed �Q
10 NTU Cal. Expiration Da
Time: Time:
Time:
Time:
YSI Professional Plus Multiparameter Meter (s/n 18B'101802)
Instrument Readings
Calibration Expiration Date
Initial:
Cal:
mmHg:
Temperature CC):
Time:
Dissolved Oxygen
/Q2 /;
`f
00 0
/ V
—IS7 l
//r
2o. Cv
_ L o
0816-
NA
pH 7 S.U.
Initial:
706
.
Cal::
.
Timee:: f�
p �7
Q
report to0.1S.U.
/.0)
V7�8
,90-� �
PH 4 S.U.
Initial:
pHmV:
Cal:
4-00
pHmV:
Time:
C ?(
reportto 0.7 S.U.
% .08
Q803
.202G
PH 10 S.U.
Initial: I r
mV: C
Cal: 0
p V: CAP
Time:
oql 2.O�G
report to 0.7 S.U.
Il p/
QC* pH 7 S.U.
AM Time:
CS�
Meas:
73 2
Mid Day Time:
Check:
PM Time:
Check:
��/� ���`v
reportto 0.7 S.U.
C ,gP
Spec. Cond.
Initial:: /
Cal:
! 0� ©
Time:
Time:
0 7� 1
c�
�� � 7
pS/cm**
b A
-,-
QC*:
AM Time:
Maas:
Mid Day Time:
Check:
PM Time:
Check:
/2
22
Q
�g
� f/ �/�U/f
PS/Cm
CAP
ORP 264.0 mV
Initica�l:
1C t�o
Cal:
TemperatureeCQ:
2l7^
Time:
�%. -�0
[Signature: rW�
Date:
! 011 1 o!
Notes:
1. Electronic equipment calibrated according to the manufacturer's operation manual.
2. Specific Conductivity should be calibrated according to values representative of historic range.
3. Order of Calibration is as follows: Specific Conductivity, pH 7, pH 4, pH 10, DO, ORP, QC checks.
4. QC Acceptable Ranges: pH +/- 0.1 S.U. and Specific Conductivity 10% of the true value. If QC readings are out of range, the instrument needs to be recalibrated
5. * Indicates that a QC check must be performed in the morning, afternoon, and the end of the day, or every four hours.
6. ** Indicates to choose a Specific Conductivity buffer of 1413, 447, 84, or 23 mS which is closest to historical readings from the project location.
Method Reference: Temperature: SM 2550 8-2070 I Specific conductivity: EPA Method 120.1, Rev. 7982 1 DO: SM 4500 O G-2017 I pH: SM 4500-H+ 8-2077
Page 1 of 1

ANCHOR
..a QEA
Anchor QEA of North Carolina, PLLC
231 Haywood Street
Equipment Documentation and Instrument Calibration Data Sheet
Asheville, North Carolina 28801
/ ! y CALIBRATION DOCUMENTATION p 1
Project Name: lwd"dJ��/I �fi�/t�I SCJ1"f �dS%�C Person Conducting Calibration: Ot-l_s'�%t�2A )W1e_JV4
Project Number: C�/640 -t7A, N _ _ Date of Calibration: 10V %/ 20JI _
Project Location: f"1erJS�Lc.�1_ AIG Date of Field Measurements: J //20Y q
EQUIPMENT DOCUMENTATION
Equipment or meters used to take measurements (e.g., water level meters, survey equipment):
Equipment Type
Serial Number
Brand
Date of Use
150-ft Water Level
26154
Solinist
150-ft Water Level
22754
Solinist
150-ft Water Level
150
Testwell
150-ft Drawdown
MP30-1527
QED
Other
Select Turbidimeter:
Hach 21000 (s/n 151006045207)
HF Scientific MicroTPW (s/n 200601045)
Calibration
Expiration Date:
Instrument Reading
(Hach 21000)
Instrument Reading
(HF Scientific MicroTPW)
20 NTU
100 NTU
800 NTU
1,000 NTU
10.0 NTU
0.02 NTU
126
_0.2Q
`�G20
CaI:,U ZO
C�:o� /DU
Cal�r1 9U'
Cal:
Cal:
Cal:
Time:U�,L�
Time:,_7s l
Time:,
J
Time:
Time:
Time:
Verification (10 NTU): 7
Verification:
Verification:
Verification:
Time: �-
0`?5s
10 NTU Cal. Expiration Date:
L .2o
Time:
Time:
Time:
YSI Professional Plus Multiparameter Meter (s/n 1813701802)
Instrument Readings
Calibration Expiration Date
Dissolved Oxygen
Initial:
I !
Cal:
1/i�
/V .
mmHg:
�/yl*!�
7il V
Temperature (IC):
'd (�
11-
Time:
,{.rC4
U -
NA
pH 7 S.U.
report to 0.1 S.U.
Initi C1
o-L�
pHmV:
�j;ZD
Cal: -7-
Time:
—7
0 V120_�
PH 4 S.U.
report to 0.7 S.0
Initial:
j
pHmV:
Ca��
pH
Tn.
7S3�
PH 10 S.U.
reportto 0.1 S.U.
Initial:,
Y. 6�
pHmV:
/n.,
Cal: !
! 0 c 01
mV•
Gk,a
Time:
0?�-o~
(�
O ( -2,0
QC* pH 7 S.U.
report to 0.1 S.U.
AM Time:
08o C11
Meas:
7,03
Mid Day Time:
Check:
PM Time:
Check:
cop
0
Spec. Cond.
Ns/cm**
Initial:
s; )
Cal:
/Goo
Time:
d74Z,
/
Ci/2W2017
QC*:
PS/cm
AM Time:
Q�V�
Meaass::
C (1�
Mid Day Time:
Check:
PM Time:
Check:
"P
�% !
)/7
�G2.
ORP G mV
Initial: 1 /�
_ l.V
Cal:
�G2:)
Temperature (°C):
aoo .
Tiryle= r) I
V 6o
��` p
1 1 /�//Xj l
Signature: �r� - . Date: of -7 / I
Notes:
1. Electronic equipment calibrated according to the manufacturer's operation manual.
2, Specific Conductivity should be calibrated according to values representative of historic range.
3. Order of Calibration is as follows: Specific Conductivity, pH 7, pH 4, pH 10, DO, ORP, QC checks.
4. QC Acceptable Ranges: pH +/- 0.1 S.U. and Specific Conductivity 10% of the true value. If QC readings are out of range, the instrument needs to be recalibrated.
5. * Indicates that a QC check must be performed in the morning, afternoon, and the end of the day, or every four hours.
6. ** Indicates to choose a Specific Conductivity buffer of 1413, 447, 84, or 23 mS which is closest to historical readings from the project location. •
Method Reference: Temperature: SM 2550 8-2070 I Specific conductivity: EPA Method 120.1, Rev. 7982 1 DO: SM 4500 O G-207 7 I pH: SM 4500-H+ 8-2077
Page 1 of 1

Appendix B
Report of Laboratory Analysis and
Chain -of -Custody Documentation

LP R I S M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Anchor QEA of North Carolina, PLLC
Alec Macbeth
231 Haywood Street
Asheville, NC 28801
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Project: Madison Closed Landfill
Lab Submittal Date: 10/18/2019
Prism Work Order: 9100306
Case Narrative
10/31/19 15:20
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones Reviewed By Robbi A. Jones
President/Project Manager President/Project Manager
Data Qualifiers Key Reference:
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 24

Sample Receipt Summary
�P R I S M
Full -Service Analytical
s
Environmental Solutions
10/31/2019
LABORATORIES, INC.
Prism Work Order: 9100306
Client Sample ID
Lab Sample ID
Matrix
Date/Time Sampled Date/Time Received
MW-01 OLD
9100306-01
Water
10/17/19 11:08 10/18/19 8:20
MW-02 OLD
9100306-02
Water
10/17/19 14:25 10/18/19 8:20
MW-03 OLD
9100306-03
Water
10/17/19 13:44 10/18/19 8:20
MW-04 OLD
9100306-04
Water
10/17/19 12:38 10/18/19 8:20
BIG Spring OLD
9100306-05
Water
10/17/19 15:31 10/18/19 8:20
Trip Blank
9100306-06
Water
10/17/19 0:00 10/18/19 8:20
Samples were received in good condition at 2.9 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 2 of 24

/r P R I S M Full -Service Analytical s
Environmental Solutions
LABORATOR
Summary of Detections
10/31 /201 g
Prism Work Order: 9100306
Prism ID
Client ID
Parameter
Method
Result
Units
9100306-01
MW-01 OLD
Arsenic
6020B
0.52
.1 ug/L
9100306-01
MW-01 OLD
Barium
6020B
550
ug/L
9100306-01
MW-01 OLD
Chromium
6020B
2.3
J ug/L
9100306-01
MW-01 OLD
Lead
6020B
0.69
J ug/L
9100306-01
MW-01 OLD
1,1-Dichloroethane
8260D
1.1
ug/L
9100306-01
MW-01 OLD
1,2-Dichlorobenzene
8260D
0.72
ug/L
9100306-01
MW-01 OLD
1,2-Dichloropropane
8260D
0.32
J ug/L
9100306-01
MW-01 OLD
1,4-Dichlorobenzene
8260D
6.0
ug/L
9100306-01
MW-01 OLD
Benzene
8260D
0.82
ug/L
9100306-01
MW-01 OLD
Chlorobenzene
8260D
4.0
ug/L
9100306-01
MW-01 OLD
Chloroethane
8260D
1.8
ug/L
9100306-01
MW-01 OLD
cis-1,2-Dichloroethylene
8260D
3.4
ug/L
9100306-01
MW-01 OLD
trans-1,2-Dichloroethylene
8260D
0.33
J ug/L
9100306-01
MW-01 OLD
Trichloroethylene
8260D
0.46
J ug/L
9100306-01
MW-01 OLD
Vinyl chloride
8260D
0.96
ug/L
9100306-01
MW-01 OLD
1,4-Dioxane
8260D SIM
9.0
ug/L
9100306-02
MW-02 OLD
Barium
6020B
50
ug/L
9100306-02
MW-02 OLD
1,1-Dichloroethane
8260D
0.94
ug/L
9100306-02
MW-02 OLD
Acetone
8260D
6.1
ug/L
9100306-03
MW-03 OLD
Barium
6020B
920
ug/L
9100306-03
MW-03 OLD
1,2-Dichlorobenzene
8260D
0.45
J ug/L
9100306-03
MW-03 OLD
1,4-Dichlorobenzene
8260D
3.4
ug/L
9100306-03
MW-03 OLD
Acetone
8260D
8.0
ug/L
9100306-03
MW-03 OLD
Benzene
8260D
0.89
ug/L
9100306-03
MW-03 OLD
Chlorobenzene
8260D
5.3
ug/L
9100306-03
MW-03 OLD
Chloroethane
8260D
0.85
ug/L
9100306-03
MW-03 OLD
cis-1,2-Dichloroethylene
8260D
0.67
ug/L
9100306-04
MW-04 OLD
Barium
6020B
720
ug/L
9100306-04
MW-04 OLD
1,4-Dichlorobenzene
8260D
1.2
ug/L
9100306-04
MW-04 OLD
Acetone
8260D
18
ug/L
9100306-04
MW-04 OLD
Chlorobenzene
8260D
2.4
ug/L
9100306-04
MW-04 OLD
Chloroethane
8260D
0.87
ug/L
9100306-04
MW-04 OLD
o-Xylene
8260D
0.45
J ug/L
9100306-04
MW-04 OLD
Xylenes, total
8260D
1.1
J ug/L
9100306-04
MW-04 OLD
1,4-Dioxane
8260D SIM
1.0
J ug/L
9100306-05
BG Spring OLD
Barium
6020B
130
ug/L
9100306-05
BG Spring OLD
Chromium
6020B
2.5
J ug/L
9100306-05
BG Spring OLD
Lead
6020B
0.49
J ug/L
9100306-05
BG Spring OLD
Acetone
8260D
6.5
ug/L
9100306-06
Trip Blank
Acetone
8260D
3.6
J ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte,
Phone: [phone] - Toll Free Number: 1-800/529-6364
NC 28224-0543
- Fax: [phone]
Page 3 of 24

This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 24

PRISM Laboratory Report
Full -Service Analytical &
Environmental Solutions 10/31/2019
LABORATORIES, INC.
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill Client Sample ID: MW-01 OLD
Attn: Alec Macbeth Prism Sample ID: 9100306-01
231 Haywood Street Prism Work Order: 9100306
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/17/19 11:08
Time Submitted: 10/18/19 08:20
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Total Metals
Mercury
<0.034
ug/L
0.2
0.20
0.034
1
7470A
10/29/19 15:54JAB
P9J0493
Arsenic
0.52
J
ug/L
10
1.0
0.34
1
6020B
10/28/19 14:14MMR
P9J0440
Barium
550
ug/L
100
10
3.2
1
6020B
10/28/19 14:14MMR
P9J0440
Cadmium
<0.22
ug/L
1
1.0
0.22
1
6020B
10/28/19 14:14MMR
P9J0440
Chromium
2.3
J
ug/L
10
3.0
0.90
1
6020B
10/28/19 14:14MMR
P9J0440
Lead
0.69
J
ug/L
10
1.0
0.44
1
6020B
10/28/19 14:14MMR
P9J0440
Selenium
<0.98
ug/L
10
5.0
0.98
1
6020B
10/28/19 14:14MMR
P9J0440
Silver
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 14:14MMR
P9J0440
Volatile Organic Compounds by GUMS
1, 1, 1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
10/28/19 21:42KDM
P9J0489
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 21:42KDM
P9J0489
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
10/28/19 21:42KDM
P9J0489
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
10/28/19 21:42KDM
P9J0489
1,1-Dichloroethane
1.1
ug/L
5
0.50
0.29
1
8260D
10/28/19 21:42KDM
P9J0489
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
10/28/19 21:42KDM
P9J0489
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
10/28/19 21:42KDM
P9J0489
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
10/28/19 21:42KDM
P9J0489
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
10/28/19 21:42KDM
P9J0489
1,2-Dichlorobenzene
0.72
ug/L
5
0.50
0.28
1
8260D
10/28/19 21:42KDM
P9J0489
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
10/28/19 21:42KDM
P9J0489
1,2-Dichloropropane
0.32
J
ug/L
1
0.50
0.29
1
8260D
10/28/19 21:42KDM
P9J0489
1,4-Dichlorobenzene
6.0
ug/L
1
0.50
0.42
1
8260D
10/28/19 21:42KDM
P9J0489
Acetone
<0.70
ug/L
100
5.0
0.70
1
8260D
10/28/19 21:42KDM
P9J0489
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
10/28/19 21:42KDM
P9J0489
Benzene
0.82
ug/L
1
0.50
0.34
1
8260D
10/28/19 21:42 KDM
P9J0489
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
10/28/19 21:42KDM
P9J0489
Bromodichloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 21:42KDM
P9J0489
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
10/28/19 21:42KDM
P9J0489
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
10/28/19 21:42KDM
P9J0489
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
10/28/19 21:42KDM
P9J0489
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
10/28/19 21:42KDM
P9J0489
Chlorobenzene
4.0
ug/L
3
0.50
0.34
1
8260D
10/28/19 21:42KDM
P9J0489
Chloroethane
1.8
ug/L
10
0.50
0.43
1
8260D
10/28/19 21:42KDM
P9J0489
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
10/28/19 21:42KDM
P9J0489
Chloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 21:42KDM
P9J0489
cis-1,2-Dichloroethylene
3.4
ug/L
5
0.50
0.40
1
8260D
10/28/19 21:42KDM
P9J0489
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
10/28/19 21:42KDM
P9J0489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 24

PRISMLaboratory Report
Full -Service Analytical &
Environmental Solutions 10/31/2019
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill Client Sample ID: MW-01 OLD
Attn: Alec Macbeth Prism Sample ID: 9100306-01
231 Haywood Street Prism Work Order: 9100306
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/17/19 11:08
Time Submitted: 10/18/19 08:20
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
10/28/19 21:42KDM
P9J0489
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
10/28/19 21:42KDM
P9J0489
Ethylbenzene
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 21:42KDM
P9J0489
m,p-Xylenes
<0.73
ug/L
NE
1.0
0.73
1
8260D
10/28/19 21:42KDM
P9J0489
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
10/28/19 21:42KDM
P9J0489
Methyl Ethyl Ketone (2-Butanone)
<0.78
ug/L
100
5.0
0.78
1
8260D
10/28/19 21:42KDM
P9J0489
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
10/28/19 21:42KDM
P9J0489
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
10/28/19 21:42KDM
P9J0489
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1
8260D
10/28/19 21:42KDM
P9J0489
o-Xylene
<0.40
ug/L
NE
0.50
0.40
1
8260D
10/28/19 21:42KDM
P9J0489
Styrene
<0.26
ug/L
1
0.50
0.26
1
8260D
10/28/19 21:42KDM
P9J0489
Tetrachloroethylene
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 21:42KDM
P9J0489
Tetrahydrofuran
<0.68
ug/L
NE
10
0.68
1
8260D
10/28/19 21:42KDM
P9J0489
Toluene
<0.35
ug/L
1
0.50
0.35
1
8260D
10/28/19 21:42KDM
P9J0489
trans-1,2-Dichloroethylene
0.33 J
ug/L
5
0.50
0.27
1
8260D
10/28/19 21:42KDM
P9J0489
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1
8260D
10/28/19 21:42KDM
P9J0489
trans- 1,4-Dichloro-2-butene
<0.22
ug/L
100
10
0.22
1
8260D
10/28/19 21:42KDM
P9J0489
Trichloroethylene
0.46 J
ug/L
1
0.50
0.46
1
8260D
10/28/19 21:42KDM
P9J0489
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1
8260D
10/28/19 21:42KDM
P9J0489
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1
8260D
10/28/19 21:42KDM
P9J0489
Vinyl chloride
0.96
ug/L
1
0.50
0.41
1
8260D
10/28/19 21:42 KDM
P9J0489
Xylenes, total
<1.1
ug/L
5
1.5
1.1
1
8260D
10/28/19 21:42KDM
P9J0489
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
97 %
80-124
Dibromofluoromethane
109 % 75-129
Toluene-d8
98 %
77-123
Volatile Organic Compounds by GUMS SIM
1,4-Dioxane
9.0
ug/L
10
2.0
0.14
1
8260D SIM
10/21/19 19:14TBL
P9J0332
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 24

Laboratory Report
Full -Service
Analytical &
,.PRISM Environmental
LABORATORIES INC.
Solutions
10/31/2019
Anchor QEA of North Carolina, PLLC
Project: Madison Closed Landfill
Client Sample ID:
MW-02 OLD
Attn: Alec Macbeth
Prism Sample ID:
9100306-02
231 Haywood Street
Prism Work Order: 9100306
Asheville, NC 28801
Sample Matrix: Water
Time Collected: 10/17/19 14:25
Time Submitted:
10/18/19 08:20
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Total Metals
Mercury
<0.034
ug/L
0.2
0.20
0.034
1
7470A
10/29/19 15:58JAB
P9J0493
Arsenic
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 14:20MMR
P9J0440
Barium
50
ug/L
100
10
3.2
1
6020B
10/28/19 14:20MMR
P9J0440
Cadmium
<0.22
ug/L
1
1.0
0.22
1
6020B
10/28/19 14:20MMR
P9J0440
Chromium
<0.90
ug/L
10
3.0
0.90
1
6020B
10/28/19 14:20MMR
P9J0440
Lead
<0.44
ug/L
10
1.0
0.44
1
6020B
10/28/19 14:20MMR
P9J0440
Selenium
<0.98
ug/L
10
5.0
0.98
1
6020B
10/28/19 14:20MMR
P9J0440
Silver
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 14:20MMR
P9J0440
Volatile Organic Compounds by GUMS
1, 1, 1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
10/28/19 22:16KDM
P9J0489
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 22:16KDM
P9J0489
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
10/28/19 22:16KDM
P9J0489
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
10/28/19 22:16KDM
P9J0489
1,1-Dichloroethane
0.94
ug/L
5
0.50
0.29
1
8260D
10/28/19 22:16KDM
P9J0489
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
10/28/19 22:16KDM
P9J0489
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
10/28/19 22:16KDM
P9J0489
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
10/28/19 22:16KDM
P9J0489
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
10/28/19 22:16KDM
P9J0489
1,2-Dichlorobenzene
<0.28
ug/L
5
0.50
0.28
1
8260D
10/28/19 22:16KDM
P9J0489
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
10/28/19 22:16KDM
P9J0489
1,2-Dichloropropane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 22:16KDM
P9J0489
1,4-Dichlorobenzene
<0.42
ug/L
1
0.50
0.42
1
8260D
10/28/19 22:16KDM
P9J0489
Acetone
6.1
ug/L
100
5.0
0.70
1
8260D
10/28/19 22:16KDM
P9J0489
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
10/28/19 22:16KDM
P9J0489
Benzene
<0.34
ug/L
1
0.50
0.34
1
8260D
10/28/19 22:16KDM
P9J0489
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
10/28/19 22:16KDM
P9J0489
Bromodichloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 22:16KDM
P9J0489
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
10/28/19 22:16KDM
P9J0489
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
10/28/19 22:16KDM
P9J0489
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
10/28/19 22:16KDM
P9J0489
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
10/28/19 22:16KDM
P9J0489
Chlorobenzene
<0.34
ug/L
3
0.50
0.34
1
8260D
10/28/19 22:16KDM
P9J0489
Chloroethane
<0.43
ug/L
10
0.50
0.43
1
8260D
10/28/19 22:16KDM
P9J0489
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
10/28/19 22:16KDM
P9J0489
Chloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 22:16KDM
P9J0489
cis- 1,2-Dichloroethylene
<0.40
ug/L
5
0.50
0.40
1
8260D
10/28/19 22:16KDM
P9J0489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 24

PRISMLaboratory Report
Full -Service Analytical &
Environmental Solutions 10/31/2019
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill Client Sample ID: MW-02 OLD
Attn: Alec Macbeth Prism Sample ID: 9100306-02
231 Haywood Street Prism Work Order: 9100306
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/17/19 14:25
Time Submitted: 10/18/19 08:20
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
10/28/19 22:16KDM
P9J0489
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
10/28/19 22:16KDM
P9J0489
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
10/28/19 22:16KDM
P9J0489
Ethylbenzene
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 22:16KDM
P9J0489
m,p-Xylenes
<0.73
ug/L
NE
1.0
0.73
1
8260D
10/28/19 22:16KDM
P9J0489
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
10/28/19 22:16KDM
P9J0489
Methyl Ethyl Ketone (2-Butanone)
<0.78
ug/L
100
5.0
0.78
1
8260D
10/28/19 22:16KDM
P9J0489
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
10/28/19 22:16KDM
P9J0489
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
10/28/19 22:16KDM
P9J0489
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1
8260D
10/28/19 22:16KDM
P9J0489
o-Xylene
<0.40
ug/L
NE
0.50
0.40
1
8260D
10/28/19 22:16KDM
P9J0489
Styrene
<0.26
ug/L
1
0.50
0.26
1
8260D
10/28/19 22:16KDM
P9J0489
Tetrachloroethylene
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 22:16KDM
P9J0489
Tetrahydrofuran
<0.68
ug/L
NE
10
0.68
1
8260D
10/28/19 22:16KDM
P9J0489
Toluene
<0.35
ug/L
1
0.50
0.35
1
8260D
10/28/19 22:16KDM
P9J0489
trans- 1,2-Dichloroethylene
<0.27
ug/L
5
0.50
0.27
1
8260D
10/28/19 22:16KDM
P9J0489
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1
8260D
10/28/19 22:16KDM
P9J0489
trans- 1,4-Dich loro-2-butene
<0.22
ug/L
100
10
0.22
1
8260D
10/28/19 22:16KDM
P9J0489
Trichloroethylene
<0.46
ug/L
1
0.50
0.46
1
8260D
10/28/19 22:16KDM
P9J0489
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1
8260D
10/28/19 22:16KDM
P9J0489
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1
8260D
10/28/19 22:16KDM
P9J0489
Vinyl chloride
<0.41
ug/L
1
0.50
0.41
1
8260D
10/28/19 22:16KDM
P9J0489
Xylenes, total
<1.1
ug/L
5
1.5
1.1
1
8260D
10/28/19 22:16KDM
P9J0489
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
99 %
80-124
Dibromofluoromethane
110 % 75-129
Toluene-d8
100 % 77-123
Volatile Organic Compounds by GUMS SIM
1,4-Dioxane
<0.14
ug/L
10
2.0
0.14
1
8260D SIM
10/21/19 19:39TBL
P9J0332
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 24

Laboratory Report
Full -Service
Analytical &
,.PRISM Environmental
LABORATORIES INC.
Solutions
10/31/2019
Anchor QEA of North Carolina, PLLC
Project: Madison Closed Landfill
Client Sample ID:
MW-03 OLD
Attn: Alec Macbeth
Prism Sample ID:
9100306-03
231 Haywood Street
Prism Work Order: 9100306
Asheville, NC 28801
Sample Matrix: Water
Time Collected: 10/17/19 13:44
Time Submitted:
10/18/19 08:20
Parameter
Result Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Total Metals
Mercury
<0.034
ug/L
0.2
0.20
0.034
1
7470A
10/29/19 16:02JAB
P9J0493
Arsenic
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 14:27MMR
P9J0440
Barium
920
ug/L
100
10
3.2
1
6020B
10/28/19 14:27MMR
P9J0440
Cadmium
<0.22
ug/L
1
1.0
0.22
1
6020B
10/28/19 14:27MMR
P9J0440
Chromium
<0.90
ug/L
10
3.0
0.90
1
6020B
10/28/19 14:27MMR
P9J0440
Lead
<0.44
ug/L
10
1.0
0.44
1
6020B
10/28/19 14:27MMR
P9J0440
Selenium
<0.98
ug/L
10
5.0
0.98
1
6020B
10/28/19 14:27MMR
P9J0440
Silver
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 14:27MMR
P9J0440
Volatile Organic Compounds by GUMS
1, 1, 1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
10/28/19 22:50KDM
P9J0489
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 22:50KDM
P9J0489
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
10/28/19 22:50KDM
P9J0489
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
10/28/19 22:50KDM
P9J0489
1,1-Dichloroethane
<0.29
ug/L
5
0.50
0.29
1
8260D
10/28/19 22:50KDM
P9J0489
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
10/28/19 22:50KDM
P9J0489
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
10/28/19 22:50KDM
P9J0489
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
10/28/19 22:50KDM
P9J0489
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
10/28/19 22:50KDM
P9J0489
1,2-Dichlorobenzene
0.45
J ug/L
5
0.50
0.28
1
8260D
10/28/19 22:50KDM
P9J0489
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
10/28/19 22:50KDM
P9J0489
1,2-Dichloropropane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 22:50KDM
P9J0489
1,4-Dichlorobenzene
3.4
ug/L
1
0.50
0.42
1
8260D
10/28/19 22:50KDM
P9J0489
Acetone
8.0
ug/L
100
5.0
0.70
1
8260D
10/28/19 22:50 KDM
P9J0489
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
10/28/19 22:50KDM
P9J0489
Benzene
0.89
ug/L
1
0.50
0.34
1
8260D
10/28/19 22:50 KDM
P9J0489
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
10/28/19 22:50KDM
P9J0489
Bromodichloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 22:50KDM
P9J0489
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
10/28/19 22:50KDM
P9J0489
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
10/28/19 22:50KDM
P9J0489
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
10/28/19 22:50KDM
P9J0489
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
10/28/19 22:50KDM
P9J0489
Chlorobenzene
5.3
ug/L
3
0.50
0.34
1
8260D
10/28/19 22:50KDM
P9J0489
Chloroethane
0.85
ug/L
10
0.50
0.43
1
8260D
10/28/19 22:50KDM
P9J0489
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
10/28/19 22:50KDM
P9J0489
Chloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 22:50KDM
P9J0489
cis-1,2-Dichloroethylene
0.67
ug/L
5
0.50
0.40
1
8260D
10/28/19 22:50KDM
P9J0489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 24

PRISMLaboratory Report
Full -Service Analytical &
Environmental Solutions 10/31/2019
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill Client Sample ID: MW-03 OLD
Attn: Alec Macbeth Prism Sample ID: 9100306-03
231 Haywood Street Prism Work Order: 9100306
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/17/19 13:44
Time Submitted: 10/18/19 08:20
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
10/28/19 22:50KDM
P9J0489
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
10/28/19 22:50KDM
P9J0489
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
10/28/19 22:50KDM
P9J0489
Ethylbenzene
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 22:50KDM
P9J0489
m,p-Xylenes
<0.73
ug/L
NE
1.0
0.73
1
8260D
10/28/19 22:50KDM
P9J0489
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
10/28/19 22:50KDM
P9J0489
Methyl Ethyl Ketone (2-Butanone)
<0.78
ug/L
100
5.0
0.78
1
8260D
10/28/19 22:50KDM
P9J0489
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
10/28/19 22:50KDM
P9J0489
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
10/28/19 22:50KDM
P9J0489
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1
8260D
10/28/19 22:50KDM
P9J0489
o-Xylene
<0.40
ug/L
NE
0.50
0.40
1
8260D
10/28/19 22:50KDM
P9J0489
Styrene
<0.26
ug/L
1
0.50
0.26
1
8260D
10/28/19 22:50KDM
P9J0489
Tetrachloroethylene
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 22:50KDM
P9J0489
Tetrahydrofuran
<0.68
ug/L
NE
10
0.68
1
8260D
10/28/19 22:50KDM
P9J0489
Toluene
<0.35
ug/L
1
0.50
0.35
1
8260D
10/28/19 22:50KDM
P9J0489
trans- 1,2-Dichloroethylene
<0.27
ug/L
5
0.50
0.27
1
8260D
10/28/19 22:50KDM
P9J0489
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1
8260D
10/28/19 22:50KDM
P9J0489
trans- 1,4-Dich loro-2-butene
<0.22
ug/L
100
10
0.22
1
8260D
10/28/19 22:50KDM
P9J0489
Trichloroethylene
<0.46
ug/L
1
0.50
0.46
1
8260D
10/28/19 22:50KDM
P9J0489
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1
8260D
10/28/19 22:50KDM
P9J0489
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1
8260D
10/28/19 22:50KDM
P9J0489
Vinyl chloride
<0.41
ug/L
1
0.50
0.41
1
8260D
10/28/19 22:50KDM
P9J0489
Xylenes, total
<1.1
ug/L
5
1.5
1.1
1
8260D
10/28/19 22:50KDM
P9J0489
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
96 %
80-124
Dibromofluoromethane
109 % 75-129
Toluene-d8
98 %
77-123
Volatile Organic Compounds by GUMS SIM
1,4-Dioxane
<0.14
ug/L
10
2.0
0.14
1
8260D SIM
10/21/19 20:04TBL
P9J0332
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 24

Laboratory Report
Full -Service
Analytical &
,.PRISM Environmental
LABORATORIES INC.
Solutions
10/31/2019
Anchor QEA of North Carolina, PLLC
Project: Madison Closed Landfill
Client Sample ID:
MW-04 OLD
Attn: Alec Macbeth
Prism Sample ID:
9100306-04
231 Haywood Street
Prism Work Order: 9100306
Asheville, NC 28801
Sample Matrix: Water
Time Collected: 10/17/19 12:38
Time Submitted:
10/18/19 08:20
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Total Metals
Mercury
<0.034
ug/L
0.2
0.20
0.034
1
7470A
10/29/19 16:06JAB
P9J0493
Arsenic
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 14:34MMR
P9J0440
Barium
720
ug/L
100
10
3.2
1
6020B
10/28/19 14:34MMR
P9J0440
Cadmium
<0.22
ug/L
1
1.0
0.22
1
6020B
10/28/19 14:34MMR
P9J0440
Chromium
<0.90
ug/L
10
3.0
0.90
1
6020B
10/28/19 14:34MMR
P9J0440
Lead
<0.44
ug/L
10
1.0
0.44
1
6020B
10/28/19 14:34MMR
P9J0440
Selenium
<0.98
ug/L
10
5.0
0.98
1
6020B
10/28/19 14:34MMR
P9J0440
Silver
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 14:34MMR
P9J0440
Volatile Organic Compounds by GUMS
1, 1, 1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
10/28/19 23:23KDM
P9J0489
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 23:23KDM
P9J0489
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
10/28/19 23:23KDM
P9J0489
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
10/28/19 23:23KDM
P9J0489
1,1-Dichloroethane
<0.29
ug/L
5
0.50
0.29
1
8260D
10/28/19 23:23KDM
P9J0489
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
10/28/19 23:23KDM
P9J0489
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
10/28/19 23:23KDM
P9J0489
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
10/28/19 23:23KDM
P9J0489
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
10/28/19 23:23KDM
P9J0489
1,2-Dichlorobenzene
<0.28
ug/L
5
0.50
0.28
1
8260D
10/28/19 23:23KDM
P9J0489
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
10/28/19 23:23KDM
P9J0489
1,2-Dichloropropane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 23:23KDM
P9J0489
1,4-Dichlorobenzene
1.2
ug/L
1
0.50
0.42
1
8260D
10/28/19 23:23KDM
P9J0489
Acetone
18
ug/L
100
5.0
0.70
1
8260D
10/28/19 23:23KDM
P9J0489
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
10/28/19 23:23KDM
P9J0489
Benzene
<0.34
ug/L
1
0.50
0.34
1
8260D
10/28/19 23:23KDM
P9J0489
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
10/28/19 23:23KDM
P9J0489
Bromodichloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 23:23KDM
P9J0489
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
10/28/19 23:23KDM
P9J0489
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
10/28/19 23:23KDM
P9J0489
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
10/28/19 23:23KDM
P9J0489
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
10/28/19 23:23KDM
P9J0489
Chlorobenzene
2.4
ug/L
3
0.50
0.34
1
8260D
10/28/19 23:23KDM
P9J0489
Chloroethane
0.87
ug/L
10
0.50
0.43
1
8260D
10/28/19 23:23KDM
P9J0489
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
10/28/19 23:23KDM
P9J0489
Chloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 23:23KDM
P9J0489
cis- 1,2-Dichloroethylene
<0.40
ug/L
5
0.50
0.40
1
8260D
10/28/19 23:23KDM
P9J0489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 24

PRISMLaboratory Report
Full -Service Analytical &
Environmental Solutions 10/31/2019
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill Client Sample ID: MW-04 OLD
Attn: Alec Macbeth Prism Sample ID: 9100306-04
231 Haywood Street Prism Work Order: 9100306
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/17/19 12:38
Time Submitted: 10/18/19 08:20
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
10/28/19 23:23KDM
P9J0489
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
10/28/19 23:23KDM
P9J0489
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
10/28/19 23:23KDM
P9J0489
Ethylbenzene
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 23:23KDM
P9J0489
m,p-Xylenes
<0.73
ug/L
NE
1.0
0.73
1
8260D
10/28/19 23:23KDM
P9J0489
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
10/28/19 23:23KDM
P9J0489
Methyl Ethyl Ketone (2-Butanone)
<0.78
ug/L
100
5.0
0.78
1
8260D
10/28/19 23:23KDM
P9J0489
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
10/28/19 23:23KDM
P9J0489
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
10/28/19 23:23KDM
P9J0489
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1
8260D
10/28/19 23:23KDM
P9J0489
o-Xylene
0.45 J
ug/L
NE
0.50
0.40
1
8260D
10/28/19 23:23KDM
P9J0489
Styrene
<0.26
ug/L
1
0.50
0.26
1
8260D
10/28/19 23:23KDM
P9J0489
Tetrachloroethylene
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 23:23KDM
P9J0489
Tetrahydrofuran
<0.68
ug/L
NE
10
0.68
1
8260D
10/28/19 23:23KDM
P9J0489
Toluene
<0.35
ug/L
1
0.50
0.35
1
8260D
10/28/19 23:23KDM
P9J0489
trans- 1,2-Dichloroethylene
<0.27
ug/L
5
0.50
0.27
1
8260D
10/28/19 23:23KDM
P9J0489
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1
8260D
10/28/19 23:23KDM
P9J0489
trans- 1,4-Dich loro-2-butene
<0.22
ug/L
100
10
0.22
1
8260D
10/28/19 23:23KDM
P9J0489
Trichloroethylene
<0.46
ug/L
1
0.50
0.46
1
8260D
10/28/19 23:23KDM
P9J0489
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1
8260D
10/28/19 23:23KDM
P9J0489
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1
8260D
10/28/19 23:23KDM
P9J0489
Vinyl chloride
<0.41
ug/L
1
0.50
0.41
1
8260D
10/28/19 23:23KDM
P9J0489
Xylenes, total
1.1 J
ug/L
5
1.5
1.1
1
8260D
10/28/19 23:23KDM
P9J0489
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
98 %
80-124
Dibromofluoromethane
108 % 75-129
Toluene-d8
97 %
77-123
Volatile Organic Compounds by GUMS SIM
1,4-Dioxane
1.0 J
ug/L
10
2.0
0.14
1
8260D SIM
10/21/19 20:29TBL
P9J0332
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 24

�Full-Service Analytical
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
10/31 /2019
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Madison Closed Landfill
Sample Matrix: Water
Client Sample ID: BG Spring OLD
Prism Sample ID: 9100306-05
Prism Work Order: 9100306
Time Collected: 10/17/19 15:31
Time Submitted: 10/18/19 08:20
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Total Metals
Mercury
<0.034
ug/L
0.2
0.20
0.034
1
7470A
10/29/19 16:09JAB
P9J0493
Arsenic
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 14:40MMR
P9J0440
Barium
130
ug/L
100
10
3.2
1
6020B
10/28/19 14:40MMR
P9J0440
Cadmium
<0.22
ug/L
1
1.0
0.22
1
6020B
10/28/19 14:40MMR
P9J0440
Chromium
2.5 J
ug/L
10
3.0
0.90
1
6020B
10/28/19 14:40MMR
P9J0440
Lead
0.49 J
ug/L
10
1.0
0.44
1
6020B
10/28/19 14:40MMR
P9J0440
Selenium
<0.98
ug/L
10
5.0
0.98
1
6020B
10/28/19 14:40MMR
P9J0440
Silver
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 14:40MMR
P9J0440
Volatile Organic Compounds by GUMS
1, 1, 1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
10/28/19 23:57KDM
P9J0489
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 23:57KDM
P9J0489
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
10/28/19 23:57KDM
P9J0489
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
10/28/19 23:57KDM
P9J0489
1,1-Dichloroethane
<0.29
ug/L
5
0.50
0.29
1
8260D
10/28/19 23:57KDM
P9J0489
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
10/28/19 23:57KDM
P9J0489
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
10/28/19 23:57KDM
P9J0489
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
10/28/19 23:57KDM
P9J0489
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
10/28/19 23:57KDM
P9J0489
1,2-Dichlorobenzene
<0.28
ug/L
5
0.50
0.28
1
8260D
10/28/19 23:57KDM
P9J0489
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
10/28/19 23:57KDM
P9J0489
1,2-Dichloropropane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 23:57KDM
P9J0489
1,4-Dichlorobenzene
<0.42
ug/L
1
0.50
0.42
1
8260D
10/28/19 23:57KDM
P9J0489
Acetone
6.5
ug/L
100
5.0
0.70
1
8260D
10/28/19 23:57KDM
P9J0489
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
10/28/19 23:57KDM
P9J0489
Benzene
<0.34
ug/L
1
0.50
0.34
1
8260D
10/28/19 23:57KDM
P9J0489
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
10/28/19 23:57KDM
P9J0489
Bromodichloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 23:57KDM
P9J0489
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
10/28/19 23:57KDM
P9J0489
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
10/28/19 23:57KDM
P9J0489
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
10/28/19 23:57KDM
P9J0489
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
10/28/19 23:57KDM
P9J0489
Chlorobenzene
<0.34
ug/L
3
0.50
0.34
1
8260D
10/28/19 23:57KDM
P9J0489
Chloroethane
<0.43
ug/L
10
0.50
0.43
1
8260D
10/28/19 23:57KDM
P9J0489
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
10/28/19 23:57KDM
P9J0489
Chloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 23:57KDM
P9J0489
cis- 1,2-Dichloroethylene
<0.40
ug/L
5
0.50
0.40
1
8260D
10/28/19 23:57KDM
P9J0489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 24

PRISMLaboratory Report
Full -Service Analytical &
Environmental Solutions 10/31/2019
LABORATORIES INC.
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill Client Sample ID: BG Spring OLD
Attn: Alec Macbeth Prism Sample ID: 9100306-05
231 Haywood Street Prism Work Order: 9100306
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/17/19 15:31
Time Submitted: 10/18/19 08:20
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
10/28/19 23:57KDM
P9J0489
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
10/28/19 23:57KDM
P9J0489
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
10/28/19 23:57KDM
P9J0489
Ethylbenzene
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 23:57KDM
P9J0489
m,p-Xylenes
<0.73
ug/L
NE
1.0
0.73
1
8260D
10/28/19 23:57KDM
P9J0489
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
10/28/19 23:57KDM
P9J0489
Methyl Ethyl Ketone (2-Butanone)
<0.78
ug/L
100
5.0
0.78
1
8260D
10/28/19 23:57KDM
P9J0489
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
10/28/19 23:57KDM
P9J0489
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
10/28/19 23:57KDM
P9J0489
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1
8260D
10/28/19 23:57KDM
P9J0489
o-Xylene
<0.40
ug/L
NE
0.50
0.40
1
8260D
10/28/19 23:57KDM
P9J0489
Styrene
<0.26
ug/L
1
0.50
0.26
1
8260D
10/28/19 23:57KDM
P9J0489
Tetrachloroethylene
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 23:57KDM
P9J0489
Tetrahydrofuran
<0.68
ug/L
NE
10
0.68
1
8260D
10/28/19 23:57KDM
P9J0489
Toluene
<0.35
ug/L
1
0.50
0.35
1
8260D
10/28/19 23:57KDM
P9J0489
trans- 1,2-Dichloroethylene
<0.27
ug/L
5
0.50
0.27
1
8260D
10/28/19 23:57KDM
P9J0489
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1
8260D
10/28/19 23:57KDM
P9J0489
trans- 1,4-Dich loro-2-butene
<0.22
ug/L
100
10
0.22
1
8260D
10/28/19 23:57KDM
P9J0489
Trichloroethylene
<0.46
ug/L
1
0.50
0.46
1
8260D
10/28/19 23:57KDM
P9J0489
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1
8260D
10/28/19 23:57KDM
P9J0489
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1
8260D
10/28/19 23:57KDM
P9J0489
Vinyl chloride
<0.41
ug/L
1
0.50
0.41
1
8260D
10/28/19 23:57KDM
P9J0489
Xylenes, total
<1.1
ug/L
5
1.5
1.1
1
8260D
10/28/19 23:57KDM
P9J0489
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
98 %
80-124
Dibromofluoromethane
107 % 75-129
Toluene-d8
97 %
77-123
Volatile Organic Compounds by GUMS SIM
1,4-Dioxane
<0.14
ug/L
10
2.0
0.14
1
8260D SIM
10/21/19 20:54TBL
P9J0332
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 24

�Full-Service Analytical s
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
10/31 /2019
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Madison Closed Landfill
Sample Matrix: Water
Client Sample ID: Trip Blank
Prism Sample ID: 9100306-06
Prism Work Order: 9100306
Time Collected: 10/17/19 00:00
Time Submitted: 10/18/19 08:20
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GUMS
1, 1, 1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
10/28/19 20:OOKDM
P9J0489
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 20:OOKDM
P9J0489
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
10/28/19 20:OOKDM
P9J0489
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
10/28/19 20:OOKDM
P9J0489
1,1-Dichloroethane
<0.29
ug/L
5
0.50
0.29
1
8260D
10/28/19 20:OOKDM
P9J0489
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
10/28/19 20:OOKDM
P9J0489
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
10/28/19 20:OOKDM
P9J0489
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
10/28/19 20:OOKDM
P9J0489
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
10/28/19 20:OOKDM
P9J0489
1,2-Dichlorobenzene
<0.28
ug/L
5
0.50
0.28
1
8260D
10/28/19 20:OOKDM
P9J0489
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
10/28/19 20:OOKDM
P9J0489
1,2-Dichloropropane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 20:OOKDM
P9J0489
1,4-Dichlorobenzene
<0.42
ug/L
1
0.50
0.42
1
8260D
10/28/19 20:OOKDM
P9J0489
Acetone
3.6 J
ug/L
100
5.0
0.70
1
8260D
10/28/19 20:00 KDM
P9J0489
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
10/28/19 20:OOKDM
P9J0489
Benzene
<0.34
ug/L
1
0.50
0.34
1
8260D
10/28/19 20:OOKDM
P9J0489
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
10/28/19 20:OOKDM
P9J0489
Bromodichloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 20:OOKDM
P9J0489
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
10/28/19 20:OOKDM
P9J0489
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
10/28/19 20:OOKDM
P9J0489
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
10/28/19 20:OOKDM
P9J0489
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
10/28/19 20:OOKDM
P9J0489
Chlorobenzene
<0.34
ug/L
3
0.50
0.34
1
8260D
10/28/19 20:OOKDM
P9J0489
Chloroethane
<0.43
ug/L
10
0.50
0.43
1
8260D
10/28/19 20:OOKDM
P9J0489
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
10/28/19 20:OOKDM
P9J0489
Chloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 20:OOKDM
P9J0489
cis- 1,2-Dichloroethylene
<0.40
ug/L
5
0.50
0.40
1
8260D
10/28/19 20:OOKDM
P9J0489
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
10/28/19 20:OOKDM
P9J0489
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
10/28/19 20:OOKDM
P9J0489
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
10/28/19 20:OOKDM
P9J0489
Ethylbenzene
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 20:OOKDM
P9J0489
m,p-Xylenes
<0.73
ug/L
NE
1.0
0.73
1
8260D
10/28/19 20:OOKDM
P9J0489
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
10/28/19 20:OOKDM
P9J0489
Methyl Ethyl Ketone (2-Butanone)
<0.78
ug/L
100
5.0
0.78
1
8260D
10/28/19 20:OOKDM
P9J0489
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
10/28/19 20:OOKDM
P9J0489
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
10/28/19 20:OOKDM
P9J0489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 24

Laboratory Report
Full -Service Analytical &
,.PRISM
LABORATORIES INC.
Environmental Solutions
10/31/2019
Anchor QEA of North Carolina,
PLLC
Project: Madison Closed
Landfill
Client Sample ID: Trip Blank
Attn: Alec Macbeth
Prism Sample ID: 9100306-06
231 Haywood Street
Prism Work Order: 9100306
Asheville, NC 28801
Sample Matrix: Water
Time Collected: 10/17/19 00:00
Time Submitted: 10/18/19 08:20
Parameter
Result
Units
SWSL
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1 8260D 10/28/19 20:OOKDM
P9JO489
o-Xylene
<0.40
ug/L
NE
0.50
0.40
1 8260D 10/28/19 20:OOKDM
P9J0489
Styrene
<0.26
ug/L
1
0.50
0.26
1 8260D 10/28/19 20:OOKDM
P9JO489
Tetrachloroethylene
<0.31
ug/L
1
0.50
0.31
1 8260D 10/28/19 20:OOKDM
P9J0489
Tetrahydrofuran
<0.68
ug/L
NE
10
0.68
1 8260D 10/28/19 20:OOKDM
P9JO489
Toluene
<0.35
ug/L
1
0.50
0.35
1 8260D 10/28/19 20:OOKDM
P9J0489
trans- 1,2-Dichloroethylene
<0.27
ug/L
5
0.50
0.27
1 8260D 10/28/19 20:OOKDM
P9JO489
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1 8260D 10/28/19 20:OOKDM
P9J0489
trans- 1,4-Dichloro-2-butene
<0.22
ug/L
100
10
0.22
1 8260D 10/28/19 20:OOKDM
P9JO489
Trichloroethylene
<0.46
ug/L
1
0.50
0.46
1 8260D 10/28/19 20:OOKDM
P9J0489
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1 8260D 10/28/19 20:OOKDM
P9JO489
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1 8260D 10/28/19 20:00KDM
P9J0489
Vinyl chloride
<0.41
ug/L
1
0.50
0.41
1 8260D 10/28/19 20:OOKDM
P9JO489
Xylenes, total
<1.1
ug/L
5
1.5
1.1
1 8260D 10/28/19 20:00KDM
P9J0489
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
97 % 80-124
Dibromofluoromethane
108 % 75-129
Toluene-d8
99 % 77-123
Volatile Organic Compounds by GC/MS SIM
1,4-Dioxane
<0.14
ug/L
10
2.0
0.14
1 8260D SIM 10/21/19 18:23TBL
P9JO332
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 16 of 24

Full -Service Analytical &
14LANKO�TORIES�
S M Environmental Solutions
INC.
Level II QC Report
10/31/19
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Prism Work Order: 9100306
Time Submitted: 10/18/2019 8:20:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9J0489 - 5030B
Blank (P9J0489-BLK1)
Prepared & Analyzed: 10/28/19
1,1,1,2-Tetrachloroethane
BRL
0.50
ug/L
1,1,1-Trichloroethane
BRL
0.50
ug/L
1,1,2,2-Tetrachloroethane
BRL
0.50
ug/L
1,1,2-Trichloroethane
BRL
0.50
ug/L
1,1-Dichloroethane
BRL
0.50
ug/L
1,1-Dichloroethylene
BRL
0.50
ug/L
1,2,3-Trichloropropane
BRL
1.0
ug/L
1,2-Dibromo-3-chloropropane
BRL
2.0
ug/L
1,2-Dibromoethane
BRL
0.50
ug/L
1,2-Dichlorobenzene
BRL
0.50
ug/L
1,2-Dichloroethane
BRL
0.50
ug/L
1,2-Dichloropropane
BRL
0.50
ug/L
1,4-Dichlorobenzene
BRL
0.50
ug/L
Acetone
BRL
5.0
ug/L
Acrylonitrile
BRL
20
ug/L
Benzene
BRL
0.50
ug/L
Bromochloromethane
BRL
2.0
ug/L
Bromodichloromethane
BRL
0.50
ug/L
Bromoform
BRL
1.0
ug/L
Bromomethane
BRL
1.0
ug/L
Carbon disulfide
BRL
5.0
ug/L
Carbon Tetrachloride
BRL
2.0
ug/L
Chlorobenzene
BRL
0.50
ug/L
Chloroethane
BRL
0.50
ug/L
Chloroform
BRL
0.50
ug/L
Chloromethane
BRL
0.50
ug/L
cis-1,2-Dichloroethylene
BRL
0.50
ug/L
cis-1,3-Dichloropropylene
BRL
0.50
ug/L
Dibromochloromethane
BRL
0.50
ug/L
Dibromomethane
BRL
2.0
ug/L
Ethylbenzene
BRL
0.50
ug/L
m,p-Xylenes
BRL
1.0
ug/L
Methyl Butyl Ketone (2-Hexanone)
BRL
5.0
ug/L
Methyl Ethyl Ketone (2-Butanone)
BRL
5.0
ug/L
Methyl Iodide
BRL
5.0
ug/L
Methyl Isobutyl Ketone
BRL
5.0
ug/L
Methylene Chloride
BRL
1.0
ug/L
o-Xylene
BRL
0.50
ug/L
Styrene
BRL
0.50
ug/L
Tetrachloroethylene
BRL
0.50
ug/L
Tetrahydrofuran
BRL
10
ug/L
Toluene
BRL
0.50
ug/L
trans- 1,2-Dichloroethylene
BRL
0.50
ug/L
trans- 1,3-Dichloropropylene
BRL
0.50
ug/L
trans-1,4-Dichloro-2-butene
BRL
10
ug/L
Trichloroethylene
BRL
0.50
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 17 of 24

PR I S M Full -Service Analytical Environmental Solutions
LABCFATCRIES, NC.
Level II QC Report
10/31/19
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill Prism Work Order: 9100306
Attn: Alec Macbeth Time Submitted: 10/18/2019 8:20:OOAM
231 Haywood Street
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9JO489 - 5030B
Blank (P9J0489-131LK1)
Prepared & Analyzed: 10/28/19
Trichlorofluoromethane
BRL
0.50
ug/L
Vinyl acetate
BRL
2.0
ug/L
Vinyl chloride
BRL
0.50
ug/L
Xylenes, total
BRL
1.5
ug/L
Surrogate:4-Bromofluorobenzene
49.0
ug/L
50.00
98
80-124
Surrogate: Dibromofluoromethane
53.2
ug/L
50.00
106
75-129
Surrogate: Toluene-d8
48.8
ug/L
50.00
98
77-123
LCS (P9J0489-BSI)
Prepared &Analyzed: 10/28/19
1,1,1,2-Tetrachloroethane
19.9
0.50
ug/L
20.00
99
79-134
1,1,1-Trichloroethane
21.0
0.50
ug/L
20.00
105
75-136
1,1,2,2-Tetrachloroethane
20.4
0.50
ug/L
20.00
102
62-127
1,1,2-Trichloroethane
19.5
0.50
ug/L
20.00
98
70-140
1,1-Dichloroethane
20.8
0.50
ug/L
20.00
104
78-130
1,1-Dichloroethylene
21.7
0.50
ug/L
20.00
109
70-154
1,2,3-Trichloropropane
21.2
1.0
ug/L
20.00
106
71-127
1,2-Dibromo-3-chloropropane
20.0
2.0
ug/L
20.00
100
63-134
1,2-Dibromoethane
20.6
0.50
ug/L
20.00
103
77-135
1,2-Dichlorobenzene
19.1
0.50
ug/L
20.00
96
78-128
1,2-Dichloroethane
19.1
0.50
ug/L
20.00
95
68-131
1,2-Dichloropropane
19.5
0.50
ug/L
20.00
97
77-130
1,4-Dichlorobenzene
19.0
0.50
ug/L
20.00
95
75-126
Acetone
40.6
5.0
ug/L
40.00
102
40-166
Acrylonitrile
38.2
20
ug/L
40.00
95
81-127
Benzene
20.4
0.50
ug/L
20.00
102
77-128
Bromochloromethane
21.4
2.0
ug/L
20.00
107
78-135
Bromodichloromethane
20.3
0.50
ug/L
20.00
102
76-138
Bromoform
21.8
1.0
ug/L
20.00
109
71-135
Bromomethane
17.0
1.0
ug/L
20.00
85
41-168
Carbon disulfide
24.1
5.0
ug/L
20.00
120
59-135
Carbon Tetrachloride
22.0
2.0
ug/L
20.00
110
72-142
Chlorobenzene
19.6
0.50
ug/L
20.00
98
78-119
Chloroethane
20.6
0.50
ug/L
20.00
103
57-142
Chloroform
20.1
0.50
ug/L
20.00
101
77-130
Chloromethane
18.9
0.50
ug/L
20.00
94
47-145
cis-1,2-Dichloroethylene
19.6
0.50
ug/L
20.00
98
76-141
cis-1,3-Dichloropropylene
21.4
0.50
ug/L
20.00
107
65-140
Dibromochloromethane
20.8
0.50
ug/L
20.00
104
75-134
Dibromomethane
21.2
2.0
ug/L
20.00
106
76-138
Ethylbenzene
20.2
0.50
ug/L
20.00
101
80-127
m,p-Xylenes
40.6
1.0
ug/L
40.00
102
77-133
Methyl Butyl Ketone (2-Hexanone)
18.4
5.0
ug/L
20.00
92
64-137
Methyl Ethyl Ketone (2-Butanone)
19.4
5.0
ug/L
20.00
97
71-134
Methyl Iodide
14.8
5.0
ug/L
20.00
74
70-130
Methyl Isobutyl Ketone
20.0
5.0
ug/L
20.00
100
69-134
Methylene Chloride
19.4
1.0
ug/L
20.00
97
73-131
o-Xylene
18.8
0.50
ug/L
20.00
94
78-128
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 of 24

PR I S M Full -Service Analytical Environmental Solutions
LABCFATCRIES, NC.
Level II QC Report
10/31/19
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill Prism Work Order: 9100306
Attn: Alec Macbeth Time Submitted: 10/18/2019 8:20:OOAM
231 Haywood Street
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9JO489 - 5030B
LCS (P9J0489-BSI)
Prepared &Analyzed: 10/28/19
Styrene
20.0
0.50
ug/L
20.00
100
78-129
Tetrachloroethylene
21.3
0.50
ug/L
20.00
106
80-129
Tetrahydrofuran
20.1
10
ug/L
20.00
100
70-130
Toluene
19.9
0.50
ug/L
20.00
100
76-131
trans- 1,2-Dichloroethylene
20.1
0.50
ug/L
20.00
100
76-135
trans- 1,3-Dichloropropylene
21.6
0.50
ug/L
20.00
108
67-140
trans-1,4-Dichloro-2-butene
19.0
10
ug/L
20.00
95
70-130
Trichloroethylene
20.2
0.50
ug/L
20.00
101
77-133
Trichlorofluoromethane
24.0
0.50
ug/L
20.00
120
62-148
Vinyl acetate
20.9
2.0
ug/L
20.00
104
34-167
Vinyl chloride
23.4
0.50
ug/L
20.00
117
57-141
Xylenes, total
59.4
1.5
ug/L
60.00
99
77-133
Surrogate:4-Bromofluorobenzene
47.4
ug/L
50.00
95
80-124
Surrogate: Dibromofluoromethane
51.7
ug/L
50.00
103
75-129
Surrogate: Toluene-d8
49.3
ug/L
50.00
99
77-123
LCS Dup (P9J0489-BSDI)
Prepared &Analyzed: 10/28/19
1,1,1,2-Tetrachloroethane
19.2
0.50
ug/L
20.00
96
79-134
3
20
1,1,1-Trichloroethane
20.5
0.50
ug/L
20.00
102
75-136
2
20
1,1,2,2-Tetrachloroethane
20.3
0.50
ug/L
20.00
102
62-127
0.2
20
1,1,2-Trichloroethane
20.5
0.50
ug/L
20.00
102
70-140
5
20
1,1-Dichloroethane
20.3
0.50
ug/L
20.00
101
78-130
3
20
1,1-Dichloroethylene
20.9
0.50
ug/L
20.00
104
70-154
4
20
1,2,3-Trichloropropane
20.4
1.0
ug/L
20.00
102
71-127
4
20
1,2-Dibromo-3-chloropropane
21.9
2.0
ug/L
20.00
109
63-134
9
20
1,2-Dibromoethane
20.9
0.50
ug/L
20.00
104
77-135
2
20
1,2-Dichlorobenzene
18.4
0.50
ug/L
20.00
92
78-128
4
20
1,2-Dichloroethane
19.5
0.50
ug/L
20.00
98
68-131
2
20
1,2-Dichloropropane
19.6
0.50
ug/L
20.00
98
77-130
0.6
20
1,4-Dichlorobenzene
18.5
0.50
ug/L
20.00
92
75-126
3
20
Acetone
41.8
5.0
ug/L
40.00
105
40-166
3
20
Acrylonitrile
39.4
20
ug/L
40.00
98
81-127
3
20
Benzene
19.7
0.50
ug/L
20.00
99
77-128
3
20
Bromochloromethane
21.4
2.0
ug/L
20.00
107
78-135
0.09
20
Bromodichloromethane
20.2
0.50
ug/L
20.00
101
76-138
0.5
20
Bromoform
22.6
1.0
ug/L
20.00
113
71-135
4
20
Bromomethane
16.6
1.0
ug/L
20.00
83
41-168
2
20
Carbon disulfide
23.1
5.0
ug/L
20.00
115
59-135
4
20
Carbon Tetrachloride
21.8
2.0
ug/L
20.00
109
72-142
1
20
Chlorobenzene
18.8
0.50
ug/L
20.00
94
78-119
4
20
Chloroethane
19.4
0.50
ug/L
20.00
97
57-142
6
20
Chloroform
19.6
0.50
ug/L
20.00
98
77-130
3
20
Chloromethane
18.2
0.50
ug/L
20.00
91
47-145
3
20
cis-1,2-Dichloroethylene
19.2
0.50
ug/L
20.00
96
76-141
2
20
cis-1,3-Dichloropropylene
21.4
0.50
ug/L
20.00
107
65-140
0.05
20
Dibromochloromethane
20.7
0.50
ug/L
20.00
103
75-134
0.3
20
Dibromomethane
21.2
2.0
ug/L
20.00
106
76-138
0.3
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
10/31/19
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Prism Work Order: 9100306
Time Submitted: 10/18/2019 8:20:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9JO489 - 5030B
LCS Dup (P9J0489-BSD1)
Prepared &Analyzed: 10/28/19
Ethylbenzene
19.6
0.50
ug/L
20.00
98
80-127
3
20
m,p-Xylenes
39.0
1.0
ug/L
40.00
97
77-133
4
20
Methyl Butyl Ketone (2-Hexanone)
18.6
5.0
ug/L
20.00
93
64-137
1
20
Methyl Ethyl Ketone (2-Butanone)
20.3
5.0
ug/L
20.00
101
71-134
5
20
Methyl Iodide
15.4
5.0
ug/L
20.00
77
70-130
4
20
Methyl Isobutyl Ketone
20.5
5.0
ug/L
20.00
103
69-134
2
20
Methylene Chloride
18.8
1.0
ug/L
20.00
94
73-131
3
20
o-Xylene
18.3
0.50
ug/L
20.00
92
78-128
2
20
Styrene
19.4
0.50
ug/L
20.00
97
78-129
3
20
Tetrachloroethylene
20.5
0.50
ug/L
20.00
103
80-129
4
20
Tetrahydrofuran
19.6
10
ug/L
20.00
98
70-130
2
20
Toluene
19.2
0.50
ug/L
20.00
96
76-131
4
20
trans-1,2-Dichloroethylene
19.0
0.50
ug/L
20.00
95
76-135
5
20
trans-1,3-Dichloropropylene
21.4
0.50
ug/L
20.00
107
67-140
1
20
trans-1,4-Dichloro-2-butene
18.1
10
ug/L
20.00
91
70-130
5
20
Trichloroethylene
19.2
0.50
ug/L
20.00
96
77-133
5
20
Trichlorofluoromethane
23.0
0.50
ug/L
20.00
115
62-148
4
20
Vinyl acetate
22.2
2.0
ug/L
20.00
ill
34-167
6
20
Vinyl chloride
22.2
0.50
ug/L
20.00
ill
57-141
5
20
Xylenes, total
57.3
1.5
ug/L
60.00
96
77-133
4
20
Surrogate:4-Bromofluorobenzene
48.4
ug/L
50.00
97
80-124
Surrogate: Dibromofluoromethane
52.1
ug/L
50.00
104
75-129
Surrogate: Toluene-d8
48.9
ug/L
50.00
98
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
10/31/19
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Volatile Organic Compounds by GC/MS SIM - Quality Control
Reporting
Analyte Result Limit Units
Prism Work Order: 9100306
Time Submitted: 10/18/2019 8:20:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P9JO332 - 5030B
Blank (P9J0332-BLK1) Prepared &Analyzed: 10/21/19
1,4-Dioxane BRL 2.0 ug/L
LCS (P9J0332-BS1) Prepared &Analyzed: 10/21/19
1,4-Dioxane 50.2 2.0 ug/L 50.00 100 55-145
LCS Dup (P9J0332-BSD1) Prepared &Analyzed: 10/21/19
1,4-Dioxane 50.4 2.0 ug/L 50.00 101 55-145 0.6 30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
10/31/19
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Total Metals - Quality Control
Prism Work Order: 9100306
Time Submitted: 10/18/2019 8:20:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9JO440 - 3005A
Blank (P9J0440-BLK1)
Prepared: 10/25/19 Analyzed: 10/28/19
Arsenic
BRL
1.0
ug/L
Barium
BRL
10
ug/L
Cadmium
BRL
1.0
ug/L
Chromium
BRL
3.0
ug/L
Lead
BRL
1.0
ug/L
Selenium
BRL
5.0
ug/L
Silver
BRL
1.0
ug/L
LCS (P9J0440-BS1)
Prepared: 10/25/19 Analyzed: 10/28/19
Arsenic
100
1.0
ug/L
100.0 100 80-120
Barium
106
10
ug/L
100.0 106 80-120
Cadmium
101
1.0
ug/L
100.0 101 80-120
Chromium
100
3.0
ug/L
100.0 100 80-120
Lead
101
1.0
ug/L
100.0 101 80-120
Selenium
104
5.0
ug/L
100.0 104 80-120
Silver
100
1.0
ug/L
100.0 100 80-120
Batch P9J0493 - 7470A
Blank (P9J0493-BLK1) Prepared & Analyzed: 10/29/19
Mercury BRL 0.20 ug/L
LCS (P9J0493-BS1) Prepared &Analyzed: 10/29/19
Mercury 10.0 0.20 ug/L 9.375 107 80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
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Sample Extraction Data
Prep Method: 3005A
Lab Number
Batch
Initial
Final
Date/Time
9100306-01
P9J0440
50
mL
50 mL
10/25/19
8:44
9100306-02
P9J0440
50
mL
50 mL
10/25/19
8:44
9100306-03
P9J0440
50
mL
50 mL
10/25/19
8:44
9100306-04
P9J0440
50
mL
50 mL
10/25/19
8:44
9100306-05
P9J0440
50
mL
50 mL
10/25/19
8:44
Prep Method: 7470A
Lab Number
Batch
Initial
Final
Date/Time
9100306-01
P9J0493
20
mL
30 mL
10/29/19
9:18
9100306-02
P9J0493
20
mL
30 mL
10/29/19
9:18
9100306-03
P9J0493
20
mL
30 mL
10/29/19
9:18
9100306-04
P9J0493
20
mL
30 mL
10/29/19
9:18
9100306-05
P9J0493
20
mL
30 mL
10/29/19
9:18
Prep Method: 5030B
Lab Number
Batch
Initial
Final
Date/Time
9100306-01
P9J0489
10
mL
10 mL
10/28/19
9:44
9100306-02
P9J0489
10
mL
10 mL
10/28/19
9:44
9100306-03
P9J0489
10
mL
10 mL
10/28/19
9:44
9100306-04
P9J0489
10
mL
10 mL
10/28/19
9:44
9100306-05
P9J0489
10
mL
10 mL
10/28/19
9:44
9100306-06
P9J0489
10
mL
10 mL
10/28/19
9:44
Prep Method: 5030E
Lab Number
Batch
Initial
Final
Date/Time
9100306-01
P9J0332
5
mL
5 mL
10/21/19
8:21
9100306-02
P9J0332
5
mL
5 mL
10/21/19
8:21
9100306-03
P9J0332
5
mL
5 mL
10/21/19
8:21
9100306-04
P9J0332
5
mL
5 mL
10/21/19
8:21
9100306-05
P9J0332
5
mL
5 mL
10/21/19
8:21
9100306-06
P9J0332
5
mL
5 mL
10/21/19
8:21
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 of 24

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24 of 24

LP R I S M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Anchor QEA of North Carolina, PLLC
Alec Macbeth
231 Haywood Street
Asheville, NC 28801
NC Certification No. 402
NC Drinking Water Cert No. 37735
SC Certification No. 99012
Project: Madison Closed Landfill
Lab Submittal Date: 10/18/2019
Prism Work Order: 9100304
Case Narrative
11/4/19 15:40
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones Reviewed By Robbi A. Jones
President/Project Manager President/Project Manager
Data Qualifiers Key Reference:
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 16

Sample Receipt Summary
Full -Service Analytical R
S
fflyaR I M Environmental Solutions
11 /04/2019
LABORATORIES, INC.
Prism Work Order: 9100304
Client Sample ID Lab Sample ID Matrix
Date/Time Sampled Date/Time Received
SW-02 OLD 9100304-01 Water
10/17/19 14:55 10/18/19 8:20
Trip Blank 9100304-02 Water
10/17/19 0:00 10/18/19 8:20
Samples were received in good condition at 2.9 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 2 of 16

Summary of Detections
PRISM
Full -Service Analytical &
/r
Environmental Solutions
11/04/201 S
LABORATOR
Prism Work Order: 9100304
Prism ID
Client ID
Parameter
Method Result Units
9100304-01
SW-02 OLD
Hardness
SM2340 C 56000 ug/L
9100304-01
SW-02 OLD
Barium
6020B 46 ug/L
9100304-01
SW-02 OLD
Acetone
8260D 6.0 ug/L
9100304-02
Trip Blank
Acetone
8260D 4.0 J ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 16

PRISM Laboratory Report
Full -Service Analytical &
Environmental Solutions 11/04/2019
LABORATORIES, INC.
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill Client Sample ID: SW-02 OLD
Attn: Alec Macbeth Prism Sample ID: 9100304-01
231 Haywood Street Prism Work Order: 9100304
Asheville, NC 28801 Sample Matrix: Water Time Collected: 10/17/19 14:55
Time Submitted: 10/18/19 08:20
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
General Chemistry Parameters
Hardness
56000
ug/L
5000
570
1
SM2340 C
10/28/19 13:50 BMS
P9J0482
Total Metals
Mercury
<0.034
ug/L
0.2
0.20
0.034
1
7470A
10/29/19 15:5WAB
P9J0493
Arsenic
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 13:47MMR
P9J0440
Barium
46
ug/L
100
10
3.2
1
6020B
10/28/19 13:47MMR
P9J0440
Cadmium
<0.22
ug/L
1
1.0
0.22
1
6020B
10/28/19 13:47MMR
P9J0440
Chromium
<0.90
ug/L
10
3.0
0.90
1
6020B
10/28/19 13:47MMR
P9J0440
Lead
<0.44
ug/L
10
1.0
0.44
1
6020B
10/28/19 13:47MMR
P9J0440
Selenium
<0.98
ug/L
10
5.0
0.98
1
6020B
10/28/19 13:47MMR
P9J0440
Silver
<0.34
ug/L
10
1.0
0.34
1
6020B
10/28/19 13:47MMR
P9J0440
Volatile Organic Compounds by GUMS
1,1,1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
10/28/19 20:34KDM
P9J0489
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 20:34KDM
P9J0489
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
10/28/19 20:34KDM
P9J0489
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
10/28/19 20:34KDM
P9J0489
1,1-Dichloroethane
<0.29
ug/L
5
0.50
0.29
1
8260D
10/28/19 20:34KDM
P9J0489
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
10/28/19 20:34KDM
P9J0489
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
10/28/19 20:34KDM
P9J0489
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
10/28/19 20:34KDM
P9J0489
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
10/28/19 20:34KDM
P9J0489
1,2-Dichlorobenzene
<0.28
ug/L
5
0.50
0.28
1
8260D
10/28/19 20:34KDM
P9J0489
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
10/28/19 20:34KDM
P9J0489
1,2-Dichloropropane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 20:34KDM
P9J0489
1,4-Dichlorobenzene
<0.42
ug/L
1
0.50
0.42
1
8260D
10/28/19 20:34KDM
P9J0489
Acetone
6.0
ug/L
100
5.0
0.70
1
8260D
10/28/19 20:34KDM
P9J0489
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
10/28/19 20:34KDM
P9J0489
Benzene
<0.34
ug/L
1
0.50
0.34
1
8260D
10/28/19 20:34KDM
P9J0489
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
10/28/19 20:34KDM
P9J0489
Bromodichloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 20:34KDM
P9J0489
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
10/28/19 20:34KDM
P9J0489
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
10/28/19 20:34KDM
P9J0489
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
10/28/19 20:34KDM
P9J0489
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
10/28/19 20:34KDM
P9J0489
Chlorobenzene
<0.34
ug/L
3
0.50
0.34
1
8260D
10/28/19 20:34KDM
P9J0489
Chloroethane
<0.43
ug/L
10
0.50
0.43
1
8260D
10/28/19 20:34KDM
P9J0489
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
10/28/19 20:34KDM
P9J0489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 4 of 16

Laboratory Report
Full -Service Analytical &
P R S M
Environmental Solutions
LABORATORIES INC.
11/04/2019
Anchor QEA of North Carolina, PLLC
Project: Madison Closed
Landfill
Client
Sample ID:
SW-02 OLD
Attn: Alec Macbeth
Prism
Sample ID:
9100304-01
231 Haywood Street
Prism
Work Order:
9100304
Asheville, NC 28801
Sample Matrix: Water
Time
Collected: 10/17/19 14:55
Time
Submitted: 10/18/19
08:20
Parameter
Result
Units
SWSL
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Chloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 20:34KDM
P9J0489
cis- 1,2-Dichloroethylene
<0.40
ug/L
5
0.50
0.40
1
8260D
10/28/19 20:34KDM
P9J0489
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
10/28/19 20:34KDM
P9J0489
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
10/28/19 20:34KDM
P9J0489
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
10/28/19 20:34KDM
P9J0489
Ethylbenzene
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 20:34KDM
P9J0489
m,p-Xylenes
<0.73
ug/L
NE
1.0
0.73
1
8260D
10/28/19 20:34KDM
P9J0489
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
10/28/19 20:34KDM
P9J0489
Methyl Ethyl Ketone (2-Butanone)
<0.78
ug/L
100
5.0
0.78
1
8260D
10/28/19 20:34KDM
P9J0489
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
10/28/19 20:34KDM
P9J0489
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
10/28/19 20:34KDM
P9J0489
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1
8260D
10/28/19 20:34KDM
P9J0489
o-Xylene
<0.40
ug/L
NE
0.50
0.40
1
8260D
10/28/19 20:34KDM
P9J0489
Styrene
<0.26
ug/L
1
0.50
0.26
1
8260D
10/28/19 20:34KDM
P9J0489
Tetrachloroethylene
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 20:34KDM
P9J0489
Tetrahydrofuran
<0.68
ug/L
NE
10
0.68
1
8260D
10/28/19 20:34KDM
P9J0489
Toluene
<0.35
ug/L
1
0.50
0.35
1
8260D
10/28/19 20:34KDM
P9J0489
trans- 1,2-Dichloroethylene
<0.27
ug/L
5
0.50
0.27
1
8260D
10/28/19 20:34KDM
P9J0489
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1
8260D
10/28/19 20:34KDM
P9J0489
trans- 1,4-Dichloro-2-butene
<0.22
ug/L
100
10
0.22
1
8260D
10/28/19 20:34KDM
P9J0489
Trichloroethylene
<0.46
ug/L
1
0.50
0.46
1
8260D
10/28/19 20:34KDM
P9J0489
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1
8260D
10/28/19 20:34KDM
P9J0489
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1
8260D
10/28/19 20:34KDM
P9J0489
Vinyl chloride
<0.41
ug/L
1
0.50
0.41
1
8260D
10/28/19 20:34KDM
P9J0489
Xylenes, total
<1.1
ug/L
5
1.5
1.1
1
8260D
10/28/19 20:34KDM
P9J0489
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
97 % 80-124
Dibromofluoromethane
108 % 75-129
Toluene-d8
99 % 77-123
Volatile Organic Compounds by GUMS SIM
1,4-Dioxane
<0.14
ug/L
10
2.0
0.14
1
8260D SIM
10/21/19 18:48TBL
P9J0332
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 16

�Full-Service Analytical s
P R I S M
Environmental Solutions
LABORATORIES INC.
Laboratory Report
11 /04/2019
Anchor QEA of North Carolina, PLLC
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Project: Madison Closed Landfill
Sample Matrix: Water
Client Sample ID: Trip Blank
Prism Sample ID: 9100304-02
Prism Work Order: 9100304
Time Collected: 10/17/19 00:00
Time Submitted: 10/18/19 08:20
Parameter Result Units SWSL Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GUMS
1, 1, 1,2-Tetrachloroethane
<0.35
ug/L
5
0.50
0.35
1
8260D
10/28/19 18:53KDM
P9J0489
1, 1, 1 -Trichloroethane
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 18:53KDM
P9J0489
1,1,2,2-Tetrachloroethane
<0.34
ug/L
3
0.50
0.34
1
8260D
10/28/19 18:53KDM
P9J0489
1,1,2-Trichloroethane
<0.42
ug/L
1
0.50
0.42
1
8260D
10/28/19 18:53KDM
P9J0489
1,1-Dichloroethane
<0.29
ug/L
5
0.50
0.29
1
8260D
10/28/19 18:53KDM
P9J0489
1,1-Dichloroethylene
<0.35
ug/L
5
0.50
0.35
1
8260D
10/28/19 18:53KDM
P9J0489
1,2,3-Trichloropropane
<0.34
ug/L
1
1.0
0.34
1
8260D
10/28/19 18:53KDM
P9J0489
1,2-Dibromo-3-chloropropane
<0.59
ug/L
13
2.0
0.59
1
8260D
10/28/19 18:53KDM
P9J0489
1,2-Dibromoethane
<0.37
ug/L
1
0.50
0.37
1
8260D
10/28/19 18:53KDM
P9J0489
1,2-Dichlorobenzene
<0.28
ug/L
5
0.50
0.28
1
8260D
10/28/19 18:53KDM
P9J0489
1,2-Dichloroethane
<0.41
ug/L
1
0.50
0.41
1
8260D
10/28/19 18:53KDM
P9J0489
1,2-Dichloropropane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 18:53KDM
P9J0489
1,4-Dichlorobenzene
<0.42
ug/L
1
0.50
0.42
1
8260D
10/28/19 18:53KDM
P9J0489
Acetone
4.0 J
ug/L
100
5.0
0.70
1
8260D
10/28/19 18:53KDM
P9J0489
Acrylonitrile
<0.85
ug/L
200
20
0.85
1
8260D
10/28/19 18:53KDM
P9J0489
Benzene
<0.34
ug/L
1
0.50
0.34
1
8260D
10/28/19 18:53KDM
P9J0489
Bromochloromethane
<0.53
ug/L
3
2.0
0.53
1
8260D
10/28/19 18:53KDM
P9J0489
Bromodichloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 18:53KDM
P9J0489
Bromoform
<0.26
ug/L
3
1.0
0.26
1
8260D
10/28/19 18:53KDM
P9J0489
Bromomethane
<0.48
ug/L
10
1.0
0.48
1
8260D
10/28/19 18:53KDM
P9J0489
Carbon disulfide
<0.36
ug/L
100
5.0
0.36
1
8260D
10/28/19 18:53KDM
P9J0489
Carbon Tetrachloride
<0.55
ug/L
1
2.0
0.55
1
8260D
10/28/19 18:53KDM
P9J0489
Chlorobenzene
<0.34
ug/L
3
0.50
0.34
1
8260D
10/28/19 18:53KDM
P9J0489
Chloroethane
<0.43
ug/L
10
0.50
0.43
1
8260D
10/28/19 18:53KDM
P9J0489
Chloroform
<0.48
ug/L
5
0.50
0.48
1
8260D
10/28/19 18:53KDM
P9J0489
Chloromethane
<0.29
ug/L
1
0.50
0.29
1
8260D
10/28/19 18:53KDM
P9J0489
cis- 1,2-Dichloroethylene
<0.40
ug/L
5
0.50
0.40
1
8260D
10/28/19 18:53KDM
P9J0489
cis- 1,3-Dichloropropylene
<0.36
ug/L
1
0.50
0.36
1
8260D
10/28/19 18:53KDM
P9J0489
Dibromochloromethane
<0.42
ug/L
3
0.50
0.42
1
8260D
10/28/19 18:53KDM
P9J0489
Dibromomethane
<0.54
ug/L
10
2.0
0.54
1
8260D
10/28/19 18:53KDM
P9J0489
Ethylbenzene
<0.31
ug/L
1
0.50
0.31
1
8260D
10/28/19 18:53KDM
P9J0489
m,p-Xylenes
<0.73
ug/L
NE
1.0
0.73
1
8260D
10/28/19 18:53KDM
P9J0489
Methyl Butyl Ketone (2-Hexanone)
<0.29
ug/L
50
5.0
0.29
1
8260D
10/28/19 18:53KDM
P9J0489
Methyl Ethyl Ketone (2-Butanone)
<0.78
ug/L
100
5.0
0.78
1
8260D
10/28/19 18:53KDM
P9J0489
Methyl Iodide
<0.41
ug/L
10
5.0
0.41
1
8260D
10/28/19 18:53KDM
P9J0489
Methyl Isobutyl Ketone
<0.40
ug/L
100
5.0
0.40
1
8260D
10/28/19 18:53KDM
P9J0489
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 16

Laboratory Report
P R S M
Full -Service Analytical &
LABORATORIES INC.
Environmental Solutions
11/04/2019
Anchor QEA of North Carolina,
PLLC
Project: Madison Closed
Landfill
Client Sample ID: Trip Blank
Attn: Alec Macbeth
Prism Sample ID: 9100304-02
231 Haywood Street
Prism Work Order: 9100304
Asheville, NC 28801
Sample Matrix: Water
Time Collected: 10/17/19 00:00
Time Submitted: 10/18/19 08:20
Parameter
Result
Units
SWSL
Report
MDL
Dilution Method Analysis Analyst
Batch
Limit
Factor Date/Time
ID
Methylene Chloride
<0.40
ug/L
1
1.0
0.40
1 8260D 10/28/19 18:53KDM
P9J0489
o-Xylene
<0.40
ug/L
NE
0.50
0.40
1 8260D 10/28/19 18:53KDM
P9J0489
Styrene
<0.26
ug/L
1
0.50
0.26
1 8260D 10/28/19 18:53KDM
P9J0489
Tetrachloroethylene
<0.31
ug/L
1
0.50
0.31
1 8260D 10/28/19 18:53KDM
P9J0489
Tetrahydrofuran
<0.68
ug/L
NE
10
0.68
1 8260D 10/28/19 18:53KDM
P9J0489
Toluene
<0.35
ug/L
1
0.50
0.35
1 8260D 10/28/19 18:53KDM
P9J0489
trans- 1,2-Dichloroethylene
<0.27
ug/L
5
0.50
0.27
1 8260D 10/28/19 18:53KDM
P9J0489
trans- 1,3-Dichloropropylene
<0.49
ug/L
1
0.50
0.49
1 8260D 10/28/19 18:53KDM
P9J0489
trans- 1,4-Dichloro-2-butene
<0.22
ug/L
100
10
0.22
1 8260D 10/28/19 18:53KDM
P9J0489
Trichloroethylene
<0.46
ug/L
1
0.50
0.46
1 8260D 10/28/19 18:53KDM
P9J0489
Trichlorofluoromethane
<0.24
ug/L
1
0.50
0.24
1 8260D 10/28/19 18:53KDM
P9J0489
Vinyl acetate
<0.26
ug/L
50
2.0
0.26
1 8260D 10/28/19 18:53KDM
P9J0489
Vinyl chloride
<0.41
ug/L
1
0.50
0.41
1 8260D 10/28/19 18:53KDM
P9J0489
Xylenes, total
<1.1
ug/L
5
1.5
1.1
1 8260D 10/28/19 18:53KDM
P9J0489
Surrogate
Recovery Control Limits
4-Bromofluorobenzene
100 % 80-124
Dibromofluoromethane
107 % 75-129
Toluene-d8
98 % 77-123
Volatile Organic Compounds by GC/MS SIM
1,4-Dioxane
<0.14
ug/L
10
2.0
0.14
1 8260D SIM 10/21/19 17:58TBL
P9J0332
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 7 of 16

Full -Service Analytical &
14LANKO�TORIES�
S M Environmental Solutions
INC.
Level II QC Report
11/4/19
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Prism Work Order: 9100304
Time Submitted: 10/18/2019 8:20:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9J0489 - 5030B
Blank (P9J0489-BLK1)
Prepared & Analyzed: 10/28/19
1,1,1,2-Tetrachloroethane
BRL
0.50
ug/L
1,1,1-Trichloroethane
BRL
0.50
ug/L
1,1,2,2-Tetrachloroethane
BRL
0.50
ug/L
1,1,2-Trichloroethane
BRL
0.50
ug/L
1,1-Dichloroethane
BRL
0.50
ug/L
1,1-Dichloroethylene
BRL
0.50
ug/L
1,2,3-Trichloropropane
BRL
1.0
ug/L
1,2-Dibromo-3-chloropropane
BRL
2.0
ug/L
1,2-Dibromoethane
BRL
0.50
ug/L
1,2-Dichlorobenzene
BRL
0.50
ug/L
1,2-Dichloroethane
BRL
0.50
ug/L
1,2-Dichloropropane
BRL
0.50
ug/L
1,4-Dichlorobenzene
BRL
0.50
ug/L
Acetone
BRL
5.0
ug/L
Acrylonitrile
BRL
20
ug/L
Benzene
BRL
0.50
ug/L
Bromochloromethane
BRL
2.0
ug/L
Bromodichloromethane
BRL
0.50
ug/L
Bromoform
BRL
1.0
ug/L
Bromomethane
BRL
1.0
ug/L
Carbon disulfide
BRL
5.0
ug/L
Carbon Tetrachloride
BRL
2.0
ug/L
Chlorobenzene
BRL
0.50
ug/L
Chloroethane
BRL
0.50
ug/L
Chloroform
BRL
0.50
ug/L
Chloromethane
BRL
0.50
ug/L
cis-1,2-Dichloroethylene
BRL
0.50
ug/L
cis-1,3-Dichloropropylene
BRL
0.50
ug/L
Dibromochloromethane
BRL
0.50
ug/L
Dibromomethane
BRL
2.0
ug/L
Ethylbenzene
BRL
0.50
ug/L
m,p-Xylenes
BRL
1.0
ug/L
Methyl Butyl Ketone (2-Hexanone)
BRL
5.0
ug/L
Methyl Ethyl Ketone (2-Butanone)
BRL
5.0
ug/L
Methyl Iodide
BRL
5.0
ug/L
Methyl Isobutyl Ketone
BRL
5.0
ug/L
Methylene Chloride
BRL
1.0
ug/L
o-Xylene
BRL
0.50
ug/L
Styrene
BRL
0.50
ug/L
Tetrachloroethylene
BRL
0.50
ug/L
Tetrahydrofuran
BRL
10
ug/L
Toluene
BRL
0.50
ug/L
trans- 1,2-Dichloroethylene
BRL
0.50
ug/L
trans- 1,3-Dichloropropylene
BRL
0.50
ug/L
trans-1,4-Dichloro-2-butene
BRL
10
ug/L
Trichloroethylene
BRL
0.50
ug/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 8 of 16

PR I S M Full -Service Analytical Environmental Solutions
LABCFATCRIES, NC.
Level II QC Report
11/4/19
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill Prism Work Order: 9100304
Attn: Alec Macbeth Time Submitted: 10/18/2019 8:20:OOAM
231 Haywood Street
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9JO489 - 5030B
Blank (P9J0489-131LK1)
Prepared & Analyzed: 10/28/19
Trichlorofluoromethane
BRL
0.50
ug/L
Vinyl acetate
BRL
2.0
ug/L
Vinyl chloride
BRL
0.50
ug/L
Xylenes, total
BRL
1.5
ug/L
Surrogate:4-Bromofluorobenzene
49.0
ug/L
50.00
98
80-124
Surrogate: Dibromofluoromethane
53.2
ug/L
50.00
106
75-129
Surrogate: Toluene-d8
48.8
ug/L
50.00
98
77-123
LCS (P9J0489-BSI)
Prepared &Analyzed: 10/28/19
1,1,1,2-Tetrachloroethane
19.9
0.50
ug/L
20.00
99
79-134
1,1,1-Trichloroethane
21.0
0.50
ug/L
20.00
105
75-136
1,1,2,2-Tetrachloroethane
20.4
0.50
ug/L
20.00
102
62-127
1,1,2-Trichloroethane
19.5
0.50
ug/L
20.00
98
70-140
1,1-Dichloroethane
20.8
0.50
ug/L
20.00
104
78-130
1,1-Dichloroethylene
21.7
0.50
ug/L
20.00
109
70-154
1,2,3-Trichloropropane
21.2
1.0
ug/L
20.00
106
71-127
1,2-Dibromo-3-chloropropane
20.0
2.0
ug/L
20.00
100
63-134
1,2-Dibromoethane
20.6
0.50
ug/L
20.00
103
77-135
1,2-Dichlorobenzene
19.1
0.50
ug/L
20.00
96
78-128
1,2-Dichloroethane
19.1
0.50
ug/L
20.00
95
68-131
1,2-Dichloropropane
19.5
0.50
ug/L
20.00
97
77-130
1,4-Dichlorobenzene
19.0
0.50
ug/L
20.00
95
75-126
Acetone
40.6
5.0
ug/L
40.00
102
40-166
Acrylonitrile
38.2
20
ug/L
40.00
95
81-127
Benzene
20.4
0.50
ug/L
20.00
102
77-128
Bromochloromethane
21.4
2.0
ug/L
20.00
107
78-135
Bromodichloromethane
20.3
0.50
ug/L
20.00
102
76-138
Bromoform
21.8
1.0
ug/L
20.00
109
71-135
Bromomethane
17.0
1.0
ug/L
20.00
85
41-168
Carbon disulfide
24.1
5.0
ug/L
20.00
120
59-135
Carbon Tetrachloride
22.0
2.0
ug/L
20.00
110
72-142
Chlorobenzene
19.6
0.50
ug/L
20.00
98
78-119
Chloroethane
20.6
0.50
ug/L
20.00
103
57-142
Chloroform
20.1
0.50
ug/L
20.00
101
77-130
Chloromethane
18.9
0.50
ug/L
20.00
94
47-145
cis-1,2-Dichloroethylene
19.6
0.50
ug/L
20.00
98
76-141
cis-1,3-Dichloropropylene
21.4
0.50
ug/L
20.00
107
65-140
Dibromochloromethane
20.8
0.50
ug/L
20.00
104
75-134
Dibromomethane
21.2
2.0
ug/L
20.00
106
76-138
Ethylbenzene
20.2
0.50
ug/L
20.00
101
80-127
m,p-Xylenes
40.6
1.0
ug/L
40.00
102
77-133
Methyl Butyl Ketone (2-Hexanone)
18.4
5.0
ug/L
20.00
92
64-137
Methyl Ethyl Ketone (2-Butanone)
19.4
5.0
ug/L
20.00
97
71-134
Methyl Iodide
14.8
5.0
ug/L
20.00
74
70-130
Methyl Isobutyl Ketone
20.0
5.0
ug/L
20.00
100
69-134
Methylene Chloride
19.4
1.0
ug/L
20.00
97
73-131
o-Xylene
18.8
0.50
ug/L
20.00
94
78-128
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 16

PR I S M Full -Service Analytical Environmental Solutions
LABCFATCRIES, NC.
Level II QC Report
11/4/19
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill Prism Work Order: 9100304
Attn: Alec Macbeth Time Submitted: 10/18/2019 8:20:OOAM
231 Haywood Street
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9JO489 - 5030B
LCS (P9J0489-BSI)
Prepared &Analyzed: 10/28/19
Styrene
20.0
0.50
ug/L
20.00
100
78-129
Tetrachloroethylene
21.3
0.50
ug/L
20.00
106
80-129
Tetrahydrofuran
20.1
10
ug/L
20.00
100
70-130
Toluene
19.9
0.50
ug/L
20.00
100
76-131
trans- 1,2-Dichloroethylene
20.1
0.50
ug/L
20.00
100
76-135
trans- 1,3-Dichloropropylene
21.6
0.50
ug/L
20.00
108
67-140
trans-1,4-Dichloro-2-butene
19.0
10
ug/L
20.00
95
70-130
Trichloroethylene
20.2
0.50
ug/L
20.00
101
77-133
Trichlorofluoromethane
24.0
0.50
ug/L
20.00
120
62-148
Vinyl acetate
20.9
2.0
ug/L
20.00
104
34-167
Vinyl chloride
23.4
0.50
ug/L
20.00
117
57-141
Xylenes, total
59.4
1.5
ug/L
60.00
99
77-133
Surrogate:4-Bromofluorobenzene
47.4
ug/L
50.00
95
80-124
Surrogate: Dibromofluoromethane
51.7
ug/L
50.00
103
75-129
Surrogate: Toluene-d8
49.3
ug/L
50.00
99
77-123
LCS Dup (P9J0489-BSDI)
Prepared &Analyzed: 10/28/19
1,1,1,2-Tetrachloroethane
19.2
0.50
ug/L
20.00
96
79-134
3
20
1,1,1-Trichloroethane
20.5
0.50
ug/L
20.00
102
75-136
2
20
1,1,2,2-Tetrachloroethane
20.3
0.50
ug/L
20.00
102
62-127
0.2
20
1,1,2-Trichloroethane
20.5
0.50
ug/L
20.00
102
70-140
5
20
1,1-Dichloroethane
20.3
0.50
ug/L
20.00
101
78-130
3
20
1,1-Dichloroethylene
20.9
0.50
ug/L
20.00
104
70-154
4
20
1,2,3-Trichloropropane
20.4
1.0
ug/L
20.00
102
71-127
4
20
1,2-Dibromo-3-chloropropane
21.9
2.0
ug/L
20.00
109
63-134
9
20
1,2-Dibromoethane
20.9
0.50
ug/L
20.00
104
77-135
2
20
1,2-Dichlorobenzene
18.4
0.50
ug/L
20.00
92
78-128
4
20
1,2-Dichloroethane
19.5
0.50
ug/L
20.00
98
68-131
2
20
1,2-Dichloropropane
19.6
0.50
ug/L
20.00
98
77-130
0.6
20
1,4-Dichlorobenzene
18.5
0.50
ug/L
20.00
92
75-126
3
20
Acetone
41.8
5.0
ug/L
40.00
105
40-166
3
20
Acrylonitrile
39.4
20
ug/L
40.00
98
81-127
3
20
Benzene
19.7
0.50
ug/L
20.00
99
77-128
3
20
Bromochloromethane
21.4
2.0
ug/L
20.00
107
78-135
0.09
20
Bromodichloromethane
20.2
0.50
ug/L
20.00
101
76-138
0.5
20
Bromoform
22.6
1.0
ug/L
20.00
113
71-135
4
20
Bromomethane
16.6
1.0
ug/L
20.00
83
41-168
2
20
Carbon disulfide
23.1
5.0
ug/L
20.00
115
59-135
4
20
Carbon Tetrachloride
21.8
2.0
ug/L
20.00
109
72-142
1
20
Chlorobenzene
18.8
0.50
ug/L
20.00
94
78-119
4
20
Chloroethane
19.4
0.50
ug/L
20.00
97
57-142
6
20
Chloroform
19.6
0.50
ug/L
20.00
98
77-130
3
20
Chloromethane
18.2
0.50
ug/L
20.00
91
47-145
3
20
cis-1,2-Dichloroethylene
19.2
0.50
ug/L
20.00
96
76-141
2
20
cis-1,3-Dichloropropylene
21.4
0.50
ug/L
20.00
107
65-140
0.05
20
Dibromochloromethane
20.7
0.50
ug/L
20.00
103
75-134
0.3
20
Dibromomethane
21.2
2.0
ug/L
20.00
106
76-138
0.3
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 16

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/4/19
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Volatile Organic Compounds by GC/MS - Quality Control
Prism Work Order: 9100304
Time Submitted: 10/18/2019 8:20:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9JO489 - 5030B
LCS Dup (P9J0489-BSD1)
Prepared &Analyzed: 10/28/19
Ethylbenzene
19.6
0.50
ug/L
20.00
98
80-127
3
20
m,p-Xylenes
39.0
1.0
ug/L
40.00
97
77-133
4
20
Methyl Butyl Ketone (2-Hexanone)
18.6
5.0
ug/L
20.00
93
64-137
1
20
Methyl Ethyl Ketone (2-Butanone)
20.3
5.0
ug/L
20.00
101
71-134
5
20
Methyl Iodide
15.4
5.0
ug/L
20.00
77
70-130
4
20
Methyl Isobutyl Ketone
20.5
5.0
ug/L
20.00
103
69-134
2
20
Methylene Chloride
18.8
1.0
ug/L
20.00
94
73-131
3
20
o-Xylene
18.3
0.50
ug/L
20.00
92
78-128
2
20
Styrene
19.4
0.50
ug/L
20.00
97
78-129
3
20
Tetrachloroethylene
20.5
0.50
ug/L
20.00
103
80-129
4
20
Tetrahydrofuran
19.6
10
ug/L
20.00
98
70-130
2
20
Toluene
19.2
0.50
ug/L
20.00
96
76-131
4
20
trans-1,2-Dichloroethylene
19.0
0.50
ug/L
20.00
95
76-135
5
20
trans-1,3-Dichloropropylene
21.4
0.50
ug/L
20.00
107
67-140
1
20
trans-1,4-Dichloro-2-butene
18.1
10
ug/L
20.00
91
70-130
5
20
Trichloroethylene
19.2
0.50
ug/L
20.00
96
77-133
5
20
Trichlorofluoromethane
23.0
0.50
ug/L
20.00
115
62-148
4
20
Vinyl acetate
22.2
2.0
ug/L
20.00
ill
34-167
6
20
Vinyl chloride
22.2
0.50
ug/L
20.00
ill
57-141
5
20
Xylenes, total
57.3
1.5
ug/L
60.00
96
77-133
4
20
Surrogate:4-Bromofluorobenzene
48.4
ug/L
50.00
97
80-124
Surrogate: Dibromofluoromethane
52.1
ug/L
50.00
104
75-129
Surrogate: Toluene-d8
48.9
ug/L
50.00
98
77-123
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 16

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/4/19
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Volatile Organic Compounds by GC/MS SIM - Quality Control
Prism Work Order: 9100304
Time Submitted: 10/18/2019 8:20:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9JO332 - 5030B
Blank (P9J0332-BLK1)
Prepared &Analyzed: 10/21/19
1,4-Dioxane
BRL 2.0 ug/L
LCS (P9J0332-BS1)
Prepared &Analyzed: 10/21/19
1,4-Dioxane
50.2 2.0 ug/L
50.00 100 55-145
LCS Dup (P9J0332-BSD1)
Prepared &Analyzed: 10/21/19
1,4-Dioxane
50.4 2.0 ug/L
50.00 101 55-145 0.6 30
Matrix Spike (P9J0332-MS1)
Source: 9100304-02
Prepared & Analyzed: 10/21/19
1,4-Dioxane
49.6 2.0 ug/L
50.00 BRL 99 55-145
Matrix Spike Dup (P9J0332-MSD1)
Source: 9100304-02
Prepared &Analyzed: 10/21/19
1,4-Dioxane
49.5 2.0 ug/L
50.00 BRL 99 55-145 0.3 30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 of 16

Level II QC Report
P R I IS M Full -Service Analytical 11/4/19
Environmental Solutions
. LABORATORIES, INC.
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill Prism Work Order: 9100304
Attn: Alec Macbeth Time Submitted: 10/18/2019 8:20:OOAM
231 Haywood Street
Asheville, NC 28801
Total Metals - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9J0440 - 3005A
Blank (P9J0440-BLK1)
Prepared: 10/25/19 Analyzed: 10/28/19
Arsenic
BRL
1.0
ug/L
Barium
BRL
10
ug/L
Cadmium
BRL
1.0
ug/L
Chromium
BRL
3.0
ug/L
Lead
BRL
1.0
ug/L
Selenium
BRL
5.0
ug/L
Silver
BRL
1.0
ug/L
LCS (P9J0440-BS1)
Prepared: 10/25/19 Analyzed: 10/28/19
Arsenic
100
1.0
ug/L
100.0 100 80-120
Barium
106
10
ug/L
100.0 106 80-120
Cadmium
101
1.0
ug/L
100.0 101 80-120
Chromium
100
3.0
ug/L
100.0 100 80-120
Lead
101
1.0
ug/L
100.0 101 80-120
Selenium
104
5.0
ug/L
100.0 104 80-120
Silver
100
1.0
ug/L
100.0 100 80-120
Matrix Spike (P9J0440-MS1)
Source: 9100304-01
Prepared: 10/25/19 Analyzed: 10/28/19
Arsenic
98.8
1.0
ug/L
100.0 BRL 99 75-125
Barium
147
10
ug/L
100.0 46.1 101 75-125
Cadmium
103
1.0
ug/L
100.0 BRL 103 75-125
Chromium
99.3
3.0
ug/L
100.0 BRL 99 75-125
Lead
101
1.0
ug/L
100.0 BRL 101 75-125
Selenium
101
5.0
ug/L
100.0 BRL 101 75-125
Silver
101
1.0
ug/L
100.0 BRL 101 75-125
Matrix Spike Dup (P9J0440-MSD1)
Source: 9100304-01
Prepared: 10/25/19 Analyzed: 10/28/19
Arsenic
101
1.0
ug/L
100.0 BRL 101 75-125
2
20
Barium
148
10
ug/L
100.0 46.1 102 75-125
0.7
20
Cadmium
103
1.0
ug/L
100.0 BRL 103 75-125
0.3
20
Chromium
94.5
3.0
ug/L
100.0 BRL 94 75-125
5
20
Lead
99.3
1.0
ug/L
100.0 BRL 99 75-125
1
20
Selenium
99.1
5.0
ug/L
100.0 BRL 99 75-125
1
20
Silver
101
1.0
ug/L
100.0 BRL 101 75-125
0.2
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 of 16

P R I IS M Full -Service Analytical
Environmental Solutions
. LABORATORIES, INC.
Level II QC Report
11/4/19
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill
Attn: Alec Macbeth
231 Haywood Street
Asheville, NC 28801
Total Metals - Quality Control
Prism Work Order: 9100304
Time Submitted: 10/18/2019 8:20:OOAM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9J0440 - 3005A
Post Spike (P9J0440-PS1)
Source: 9100304-01
Prepared: 10/25/19 Analyzed: 10/28/19
Arsenic
100
ug/L
100.0 0.146 100
80-120
Barium
145
ug/L
100.0 46.1 99
80-120
Cadmium
102
ug/L
100.0 0.00700 102
80-120
Chromium
99.8
ug/L
100.0 0.397 99
80-120
Lead
99.3
ug/L
100.0 0.133 99
80-120
Selenium
101
ug/L
100.0 0.467 101
80-120
Silver
100
ug/L
100.0 0.0110 100
80-120
Batch P9J0493 - 7470A
Blank (P9J0493-BLK1)
Prepared & Analyzed: 10/29/19
Mercury
BRL
0.20 ug/L
LCS (P9J0493-BS1)
Prepared &Analyzed: 10/29/19
Mercury
10.0
0.20 ug/L
9.375 107
80-120
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 of 16

Level II QC Report
P R I IS M Full -Service Analytical 11/4/19
Environmental Solutions
. LABORATORIES, INC.
Anchor QEA of North Carolina, PLLC Project: Madison Closed Landfill Prism Work Order: 9100304
Attn: Alec Macbeth Time Submitted: 10/18/2019 8:20:OOAM
231 Haywood Street
Asheville, NC 28801
General Chemistry Parameters - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9JO482 - NO PREP
Blank (P9J0482-BLK1)
Prepared & Analyzed: 10/28/19
Hardness
BRL 5000 ug/L
LCS (P9J0482-BS1)
Prepared &Analyzed: 10/28/19
Hardness
50000 5000 ug/L
50000 100 90-110
Sample Extraction Data
Prep Method: 3005A
Lab Number Batch
Initial Final
Date/Time
9100304-01 P9J0440 50 mL 50 mL 10/25/19 8:44
Prep Method: 7470A
Lab Number Batch Initial Final Date/Time
9100304-01 P9J0493 20 mL 30 mL 10/29/19 9:18
Prep Method: 5030E
Lab Number Batch Initial Final Date/Time
9100304-01
P9J0489
10
mL
10 mL
10/28/19 9:44
9100304-02
P9J0489
10
mL
10 mL
10/28/19 9:44
Prep Method: 5030E
Lab Number
Batch
Initial
Final
Date/Time
9100304-01
P9J0332
5
mL
5 mL
10/21/19 8:21
9100304-02
P9J0332
5
mL
5 mL
10/21/19 8:21
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 of 16

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