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HomeMy WebLinkAboutMO-9523_40959_CA_IAR_20191105_Risk Assessment ReportRISK ASSESSMENT REPORT Former Moore Residence Hall University of North Carolina at Charlotte Charlotte, Mecklenburg County, North Carolina November 5, 2019 Terracon Project No. 71177348 Prepared for: University of North Carolina at Charlotte Charlotte, North Carolina Prepared by: Terracon Consultants, Inc. Charlotte, North Carolina November 5, 2019 Ms. Elizabeth G. Frere, MUD, PLA Project Manager UNC Charlotte I Facilities Management/Capital Projects 9201 University City Blvd. Charlotte, NC 28223 Email: efrere(a_uncc.edu RE: Risk Assessment Report Former Moore Residence Hall University of North Carolina at Charlotte Charlotte, Mecklenburg County, North Carolina Terracon Project No. 71177348 Dear Ms. Frere: Irerracon Terracon Consultants, Inc. (Terracon) is pleased to submit our Risk Assessment Report to UNC- Charlotte Facilities Management as a result of the discovery of petroleum impacted soils during demolition activities conducted at the above referenced building located on the UNC-Charlotte campus. The Risk Assessment Report presents data from recent field activities conducted at the site including the collection of soil samples and screening of impacted soils during excavation activities in September and October 2019. Terracon has conducted the risk assessment activities in general accordance with a Supplemental Contract between UNC-Charlotte and Terracon dated September 26, 2019 for risk -based sampling and reporting associated with Residence Hall Phase XV1. Terracon appreciates this opportunity to provide our environmental engineering services to UNC- Charlotte. If you have any questions or require additional information, please do not hesitate to contact McKhenzy Welch at (704) 509-1777. Sincerely, Terracon Consultants, Inc. McKhenzy Welch, CPESC Christopher L. Corbitt, PG Staff Scientist Senior Geologist Attachements Terracon Consultants, Inc. 2701 Westport Road Charlotte, NC 28208 P (704) 509 1777 F (704) 509 1888 terracon.com TABLE OF CONTENTS Irerracon 1.0 SITE DESCRIPTION.......................................................................................................1 1.1 Standard of Care..................................................................................................1 1.2 Additional Scope Limitations................................................................................2 1.3 Reliance...............................................................................................................2 2.0 FIELD ACTIVITIES.............................................................................................................2 2.1 Soil Sampling Activities........................................................................................2 3.0 ANALYTICAL RESULTS....................................................................................................3 4.0 CONCLUSIONS AND RECOMMENDATIONS...................................................................4 Figures Figure 1 — Site Location Map Figure 2 — Site Diagram Figure 3 — Boring Locations and Analyses Table Table 1 — Summary of Soil Analytical Results Appendices APPENDIX A — FIELD NOTES APPENDIX B — ANALYTICAL REPORT AND CHAIN OF CUSTODY Soil Sample Analytical Reports — Pace Analytical and Prism Laboratories APPENDIX C — DISPOSAL MANIFEST APPENDIX D — PHOTO PAGE Irerracon RISK ASSESSMENT REPORT UNC-CHARLOTTE MOORE HALL SANFORD HALL LANE CHARLOTTE, NORTH CAROLINA Terracon Project No. 71177348 November 5, 2019 1.0 SITE DESCRIPTION The former Moore Residence Hall site is comprised of approximately 1.56 acres of the 671.72- acre main campus of UNC-Charlotte (UNCC) located in northeast Charlotte, Mecklenburg County, North Carolina. The on -site building was formerly utilized as student housing on the UNC- Charlotte campus but was recently demolished. The former location of the Moore Hall building is depicted on Figures 1 and 2. As requested by UNCC on August 27, 2019, Terracon mobilized to the site to identify and confirm the presence of petroleum impacted soils discovered during demolition activities at the former Moore Residence Hall building. While at the site, Terracon utilized a hand-held photo -ionization detector (PID) to screen potentially impacted soils discovered near the southeastern corner of the former building during grading operations. PID screening values of volatile vapors originating from selected soils ranged from 134 parts per million (ppm) in the southern sidewall to 219 ppm in the eastern sidewall of the excavation. It is Terracon's understanding that UNC-Charlotte contracted with Summit Engineering (Summit) to provide the soil profile sampling and manage the removal and disposal of the petroleum impacted soils. The soil profile analysis of the soils planned for removal indicated total petroleum hydrocarbons (TPH) diesel range organics (DRO) were detected at 580 milligrams per kilogram (mg/kg) which is well above the North Carolina Department of Environmental Quality (NCDEQ) regulatory action level. According to UNC-Charlotte documentation, approximately 174.23 tons of impacted soils were transported to the Republic Landfill in Concord, North Carolina for disposal in September 2019. Following removal of the impacted soils by Summit, Terracon was contracted by UNCC to provide regulatory guidance and proceed to closure of the release incident. UNCC and Terracon were not able to identify the source of the release of petroleum constituents. Soil disposal manifests are included in Appendix C. 1.1 Standard of Care Terracon's services were performed in a manner consistent with generally accepted practices of the profession undertaken in similar studies in the same geographical area during the same time. Terracon makes no warranties, either expressed or implied, regarding the findings, conclusions, or recommendations. Please note that Terracon does not warrant the work of laboratories, regulatory agencies, or other third parties supplying information used in the preparation of the Responsive ■ Resourceful ■ Reliable 1 Risk Site Assessment Letter Report Irerracon Former Moore Residence Hall Charlotte, NC November 5, 2019 Terracon Project No. 71177348 report. The services were performed in accordance with the scope of work authorized by our client, as reflected in our proposal and were not conducted in accordance with ASTM E1903-11. 1.2 Additional Scope Limitations Findings, conclusions, and recommendations resulting from these services are based upon information derived from the on -site activities and other services performed under this scope of work; such information is subject to change over time. Certain indicators of the presence of hazardous substances, petroleum products, or other constituents may have been latent, inaccessible, unobservable, non -detectable, or not present during these services; thus, we cannot represent the site is free of hazardous substances, toxic materials, petroleum products, or other latent conditions beyond those identified during this investigation. Subsurface conditions may vary from those encountered at specific borings or wells or during other surveys, tests, assessments, investigations, or exploratory services. The data, interpretations, findings, and our recommendations are based solely upon data obtained at the time and within the scope of these services. 1.3 Reliance This report has been prepared for the exclusive use of the UNCC. Any authorization for use or reliance by another party (except a governmental entity having jurisdiction over the site) is prohibited without the expressed written authorization of the UNCC and Terracon. Any unauthorized distribution or reuse is at UNCC's sole risk. Reliance by authorized parties will be subject to the terms, conditions, and limitations stated in the Supplemental Contract between UNC-Charlotte and Terracon dated September 26, 2019 for risk -based sampling and reporting associated with Residence Hall Phase XVI and the report. 2.0 FIELD ACTIVITIES Terracon conducted the field work in accordance with a health and safety plan developed specifically for this project. Work was performed using United States Environmental Protection Agency (USEPA) Level D work attire consisting of a hard hat, safety vest, safety glasses, protective gloves and protective boots. 2.1 Soil Sampling Activities On October 1, 2019 after the impacted soils had been removed, Terracon personnel manually advanced two hand auger borings (SSW and ESW) approximately 0.5 feet into the southern and eastern sidewalls of the excavation. The side wall samples were collected about 3.5 feet above the bottom of the excavation. The BOTTOM sample was collected with the hand auger at a depth of approximately of 1 foot below the floor of the excavation. At the time of sampling, groundwater seepage was encountered during advancement of the BOTTOM boring. Terracon notified Ms. Responsive ■ Resourceful ■ Reliable 2 Risk Site Assessment Letter Report Irerracon Former Moore Residence Hall Charlotte, NC November 5, 2019 Terracon Project No. 71177348 Trudy Beverly at NCDEQ regarding the presence of groundwater in the excavation. Ms. Beverly indicated a groundwater sample would not be required due to the site conditions being unsafe for track mounted drill rig to access and install a temporary groundwater monitoring well in the impacted soil area. Soils collected from each boring were screened in the field using a PID. PID screening values ranged from 0.0 ppm in samples SSW and BOTTOM to 121.5 ppm in sample ESW. A confirmation soil sample was collected from each of the three borings. A Boring Locations and Analyses map showing the approximate locations of the soil borings is included as Figure 3. Field notes are provided in Appendix A while photographs of the field activities are provided in Appendix D. The soil samples were placed in laboratory supplied glassware, labeled and placed within an ice - packed cooler pending transport to Pace Analytical Services in Huntersville, North Carolina for laboratory analysis of TPH gasoline -range organics (TPH-GRO) by EPA Method 8015/5030 and TPH-DRO by EPA Method 8015/3545/3550, volatile organic compounds (VOCs) by EPA Method 8260B, and semi -volatile organic compounds (SVOCs) by EPA Method 8270D. Chain -of -custody documentation accompanied the samples to the laboratory, 3.0 ANALYTICAL RESULTS The analytical results for soil samples collected on August 27, 2019 (Summit Engineering) and October 1, 2019 (Terracon Consultants) are discussed below. Soil Profile Sampling by Summit Engineering (August 27, 2019) TPH-DRO was detected in soil sample S-1 at 580 mg/kg above the regulatory action level of 100 mg/kg. TPH-GRO was detected in soil sample S-1 at 99 mg/kg above the regulatory action level of 50 mg/kg. Naphthalene was detected at 0.20 J mg/kg which is slightly above the Soil to Water Maximum Soil Contaminant Concentration (MSCC). The remaining petroleum constituents were detected in soil sample S-1 at concentrations below their respective MSCCs. Risk Assessment Sampling (October 1, 2019) Petroleum constituent concentrations detected in soil sample ESW (eastern sidewall) are below their respective MSCCs. No petroleum constituents were detected in soil samples BOTTOM or SSW (southern sidewall) above the laboratory method detection limits. Acetone was detected in samples ESW and SSW below its MSCC. Acetone is considered to be a laboratory artifact, not representative of the release at the site. Responsive ■ Resourceful ■ Reliable 3 Risk Site Assessment Letter Report Irerracon Former Moore Residence Hall Charlotte, NC November 5, 2019 Terracon Project No. 71177348 Soil analytical results are summarized in Table 1 and are depicted on Figure 3. The laboratory analytical reports for Summit (Prism Laboratories) and Terracon (Pace Analytical) and chain -of - custody records are provided in Appendix B. 4.0 CONCLUSIONS AND RECOMMENDATIONS Based on the scope of services described in this report and subject to the limitations described herein, Terracon provides the following conclusions. No petroleum constituents were detected above their respective MSCCs in the soil samples. The impacted soils discovered at the site appear to have been effectively removed during excavation activities. O Groundwater seepage was encountered in the excavation; however, due to site conditions, Terracon was unable to obtain a groundwater sample. O Contiguous properties are developed as student housing for UNC-Charlotte. O Well receptor information did not identify water -supply wells within a 1,500-ft radius of the source area. Surrounding properties are connected to municipal water supplies. The nearest surface water body is an unnamed tributary of Toby Creek located approximately 220 feet the north of the release area. None of the detected constituents exceeded the 2B surface water standards. O The site currently meets the NCDEQ criteria for Low Risk status. Based on the findings of our assessment activities, the following comments and recommendations are provided for the site. Terracon petitions the NCDEQ for regulatory closure of the release incident with a No Further Action letter in accordance with the Guidelines. Responsive ■ Resourceful ■ Reliable 4 FIGURES WE � \N`k T A v f M 4 q, f pr: % t d m ih, Al� V "'J ',Balk er % 3 fill 1:2 A t & J� p' APPROXIM ATES Z7 4. SITE BOUNDARY V 7F 'z t �'K W N . . . . . . . . . . . . r S It Sm 73JL� rti t "A N j 7 '/ . ; Z _A' J.\1 "_' 41� ; tilt Project Manager: Project No. SITE LOCATION MAP Figure MAW 71177348 Drawn by: MAW Scale: .,=2,000, 1rerracon UNC-Charlotte Moore Hall Checked by: CLC File Name: Moore Hall 2701 Westport Road Sanford Hall Lane Approved by: Date: Charlotte, Mecklenburg County, North Carolina CLC November 2019 Charlotte, NC 28208-3608 1 . SOUTH VILLAGE CROSSING Y 4 = MOORE HALL � I O LL a� denotes approximate site boundary r SAAJFORD HALL r *4< UNC CHARLOTTE HOUSING & RESIDENCE LIFE t^ Project Manager: Project No. MAW 71177348 SITE DIAGRAM FI Figure g Drawn by: ScNOT Irerracon UNC- Charlotte Moore Hall MAW TOSCALE DIAGRAM IS FOR GENERAL LOCATION ONLY, Checked by: File Name: Sanford Hall Lane AND IS NOT INTENDED FOR CONSTRUCTION CLC Moore Hall 2701 Westport Road Charlotte, Mecklenburg County, North Carolina PURPOSES pprovedby: CLC Date: Charlotte, NC October 2019 LLI Z Q J J J Q 2 0 LL Sample ID: ESW Soil Sample 8260 — Acetone: 0.034J mg/kg sec -Butyl benzene: 0.0025J mg/kg 4-Methyl-2-pentanone (MIBK): 0.0058J mg/kg 1,2,4-Trimethylbenzene: 0.002J mg/kg EPH — Aliphatics (C09-C18): 69.9 mg/kg Aromatic (C11-C22): 11.2 mg/kg VPH — Adjusted C9-C12 Aliphatics: 6.0 mg/kg Aliphatic (C09-C12): 8.1mg/kg - � •"f dd Sample ID: BOTTOM NO ANALYTES DETECTED F-- , I I I I T I I I , 1 , Oil --') fib, N it DIAGRAM IS FOR GENERAL LOCATION ONLY, AND IS NOT INTENDED FOR CONSTRUCTION PURPOSES • __— Fes" . w. r' I ' Sample ID: SSW ' Soil Sample 8260 — Acetone: 0.0417J mg/kg denotes approximate known p impactedsoil 1 denotes soil boring location Project Manager: Project No. Mnw BORING LOCATIONS AND ANALYSES Figure MAW71177148 Drawn by: Scale: NOT T°SCALE erracon lr UNC-Charlotte Moore Hall Checked by: CLC File Name: 2701 Waatport Road Sanford Hall Lane K VVV Approved by: CLC Dale:Octob., 2019 Charlotte, NC Charlotte, Mecklenburg County, North Carolina TABLE Table 1 Summary of Soil Analytical Results UNCC Moore Hall Charlotte, North Carolina Terracon Project: 71177348 Analytical Method 8260 EPH VPH Contaminant of Concern Y C � Ci _ N N U N U co rn Depth m U U rn 0 (feet BGS or o T Sam p le within c c :rz co a) M I.D. Date Collected PID (ppm) sidewall) 4 E co a U) CO a n �� o Q Q QQ a SSW 10/1/2019 0.0 j 0.5 0.0417J <0.0016 <0.0028 <0.0015 <11.2 <11.2 <2.2 <2.2 ESW 10/1/2019 121.5 0.5 0.034J 0.0025J 0.0058J 0.002J 69.9 11.2 6 8.1 BOTTOM 10/1/2019 0.0 1 <0.0071 <0.0016 <0.0028 1 <0.0015 <11.9 <11.9 <2.3 <2.3 NC Regulatory Action Level (mg/kg) Soil -to -Water Maximum Contaminant Concentration 24 3.3 0.4 8.5 540 31 540 540 (mg/kg) Residential Soil Cleanup Levels (mg/kg) 1 14,000 1 626 1 1200 1 782 1 1500 1 469 1 1500 1 1,500 Industrial/Commerical Cleanup Levels (mg/kg) 1 360,0001 16,350 1 32,000 1 20,440 1 40,000 1 12,264 1 40,000 1 40,000 Bold Font = Exceeds Soil -to -Water MSCCs Yellow Shading = Exceeds Residential MSCCs Gray Shading = Exceeds Industrial/Commercial MSCCs J = Indicates an estimated value that is above the Method Detection Limit and below the Method Reporting Limit. NE = Standard not established APPENDIX A - FIELD NOTES vwx � Ir -ell 6n X, r,, (ZWq 11� A7.Y-41 a is.�& C rrr � f � aA6F.c;t�n yzu ej,,'4 5ea7!v- (6v(!;) G g��p,ccle,7 r. d fiyr c c �� r4' 4U1111 sc r { e5- 5d�� Im 1 cGe�,<ICC 1-M) c4,-seC(.56;f� 1 f -f-A'1d �o+ do 61, APPENDIX B - ANALYTICAL REPORT AND CHAIN OF CUSTODY Soil Sample Analytical Reports — Pace Analytical and Prism Laboratories aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 October 08, 2019 McKhenzy Welch Terracon 2701 Westport Rd Charlotte, NC 28208 RE: Project: UNCC MOOR HALL Pace Project No.: 92447655 Dear McKhenzy Welch: Enclosed are the analytical results for sample(s) received by the laboratory on October 01, 2019. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, p Taylor Ezell taylor.ezell@pacelabs.com (704)875-9092 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 CERTIFICATIONS Project: UNCC MOOR HALL Pace Project No.: 92447655 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 South Carolina Certification #: 99006001 Louisiana/NELAP Certification # LA170028 Florida/NELAP Certification #: E87627 North Carolina Drinking Water Certification #: 37706 Kentucky UST Certification #: 84 North Carolina Field Services Certification #: 5342 Virginia/VELAP Certification #: 460221 North Carolina Wastewater Certification #: 12 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 44 aceAnalytical —pacelabsxom Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE SUMMARY Project: UNCC MOOR HALL Pace Project No.: 92447655 Lab ID Sample ID Matrix Date Collected Date Received 92447655001 SSW Solid 10/01/1911:45 10/01/1912:33 92447655002 ESW Solid 10/01/1911:17 10/01/1912:33 92447655003 BOTTOM Solid 10/01/1911:30 10/01/1912:33 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: Pace Project No.: UNCC MOOR HALL 92447655 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92447655001 SSW MADEP EPH SEM 7 PASI-C MADEP VPH LMB 6 PASI-C EPA 8270E BPJ 75 PASI-C EPA 8260D CL 70 PASI-C ASTM D2974-87 KDF 1 PASI-C 92447655002 ESW MADEP EPH SEM 7 PASI-C MADEP VPH LMB 6 PASI-C EPA 8270E BPJ 75 PASI-C EPA 8260D CL 70 PASI-C ASTM D2974-87 KDF 1 PASI-C 92447655003 BOTTOM MADEP EPH SEM 7 PASI-C MADEP VPH LMB 6 PASI-C EPA 8270E BPJ 75 PASI-C EPA 8260D CL 70 PASI-C ASTM D2974-87 KDF 1 PASI-C REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SUMMARY OF DETECTION Project: Pace Project No.: UNCC MOOR HALL 92447655 Lab Sample ID Client Sample ID Method Parameters Result Units Report Limit Analyzed Qualifiers 92447655001 SSW EPA 8260D Acetone 41.7J ug/kg 75.0 10/07/19 20:02 ASTM D2974-87 Percent Moisture 10.7 % 0.10 10/01/19 14:36 92447655002 ESW MADEP EPH Aliphatic (C09-C18) 69.9 mg/kg 22.0 10/08/19 12:27 N2 MADEP EPH Aromatic (C11-C22) 11.2 mg/kg 11.0 10/07/19 20:45 N2 MADEP VPH Aliphatic (C09-C12) 8.1 mg/kg 2.1 10/02/19 17:32 N2 MADEP VPH Aliphatic(C09-C12) Adjusted 6.0 mg/kg 2.1 10/02/19 17:32 N2 EPA 8260D Acetone 34.OJ ug/kg 75.5 10/08/19 13:29 EPA 8260D sec-Butylbenzene 2.5J ug/kg 3.8 10/08/19 13:29 EPA 8260D 4-Methyl-2-pentanone (MIBK) 5.8J ug/kg 37.7 10/08/19 13:29 EPA 8260D 1,2,4-Trimethylbenzene 2.OJ ug/kg 3.8 10/08/19 13:29 B,v1 ASTM D2974-87 Percent Moisture 9.2 % 0.10 10/01/19 14:36 92447655003 BOTTOM ASTM D2974-87 Percent Moisture 16.0 % 0.10 10/01/19 14:36 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: UNCC MOOR HALL Pace Project No.: 92447655 Method: MADEP EPH Description: MADEP EPH NC Soil Client: Terracon - Charlotte, NC Date: October 08, 2019 General Information: 3 samples were analyzed for MADEP EPH. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with MADEP EPH with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: UNCC MOOR HALL Pace Project No.: 92447655 Method: MADEP VPH Description: VPH NC Soil Client: Terracon - Charlotte, NC Date: October 08, 2019 General Information: 3 samples were analyzed for MADEP VPH. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with MADEP VPH with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 44 aceAnalytical _pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: UNCC MOOR HALL Pace Project No.: 92447655 Method: EPA 8270E Description: 8270E MSSV Microwave Client: Terracon - Charlotte, NC Date: October 08, 2019 General Information: 3 samples were analyzed for EPA 8270E. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 3546 with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Internal Standards: All internal standards were within QC limits with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 PROJECT NARRATIVE Project: UNCC MOOR HALL Pace Project No.: 92447655 Method: EPA 8260D Description: 8260D/5035A Volatile Organics Client: Terracon - Charlotte, NC Date: October 08, 2019 General Information: 3 samples were analyzed for EPA 8260D. All samples were received in acceptable condition with any exceptions noted below or on the chain -of custody and/or the sample condition upon receipt form (SCUR) attached at the end of this report. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 5035A with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Internal Standards: All internal standards were within QC limits with any exceptions noted below. Surrogates: All surrogates were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. QC Batch: 502304 B: Analyte was detected in the associated method blank. • BLANK for HBN 502304 [MSV/5644 (Lab ID: 2700586) • 1,2,4-Trimethylbenzene Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: This data package has been reviewed for quality and completeness and is approved for release. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UNCC MOOR HALL Pace Project No.: 92447655 Sample: SSW Lab ID: 92447655001 Collected: 10/01/19 11:45 Received: 10/01/19 12:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual MADEP EPH NC Soil Analytical Method: MADEP EPH Preparation Method: MADEP EPH Aliphatic (C09-C18) ND mg/kg 11.2 11.2 1 10/03/19 09:50 10/07/19 20:17 N2 Aliphatic (C19-C36) ND mg/kg 11.2 11.2 1 10/03/19 09:50 10/07/19 20:17 N2 Aromatic (C11-C22) ND mg/kg 11.2 11.2 1 10/03/19 09:50 10/07/19 20:17 N2 Surrogates Nonatriacontane (S) 61 % 40-140 1 10/03/19 09:50 10/07/19 20:17 7194-86-7 o-Terphenyl (S) 67 % 40-140 1 10/03/19 09:50 10/07/19 20:17 84-15-1 2-Fluorobiphenyl (S) 91 % 40-140 1 10/03/19 09:50 10/07/19 20:17 321-60-8 2-Bromonaphthalene (S) 92 % 40-140 1 10/03/19 09:50 10/07/19 20:17 580-13-2 VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH Aliphatic (C05-CO8) ND mg/kg 2.2 2.2 1 10/02/19 14:49 10/02/19 16:33 N2 Aliphatic (C09-C12) ND mg/kg 2.2 2.2 1 10/02/19 14:49 10/02/19 16:33 N2 Aliphatic(C09-C12)Adjusted ND mg/kg 2.2 2.2 1 10/02/19 14:49 10/02/19 16:33 N2 Aromatic (C09-C10) ND mg/kg 2.2 2.2 1 10/02/19 14:49 10/02/19 16:33 N2 Surrogates 4-Bromofluorobenzene (FID) (S) 85 % 70-130 1 10/02/19 14:49 10/02/19 16:33 460-00-4 4-Bromofluorobenzene (PID) (S) 87 % 70-130 1 10/02/19 14:49 10/02/19 16:33 460-00-4 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Acenaphthene ND ug/kg 369 95.1 1 10/03/19 09:52 10/07/19 17:44 83-32-9 Acenaphthylene ND ug/kg 369 87.4 1 10/03/19 09:52 10/07/19 17:44 208-96-8 Aniline ND ug/kg 369 83.0 1 10/03/19 09:52 10/07/19 17:44 62-53-3 Anthracene ND ug/kg 369 95.8 1 10/03/19 09:52 10/07/19 17:44 120-12-7 Benzo(a)anthracene ND ug/kg 369 118 1 10/03/19 09:52 10/07/19 17:44 56-55-3 Benzo(a)pyrene ND ug/kg 369 160 1 10/03/19 09:52 10/07/19 17:44 50-32-8 Benzo(b)fluoranthene ND ug/kg 369 149 1 10/03/19 09:52 10/07/19 17:44 205-99-2 Benzo(g,h,i)perylene ND ug/kg 369 144 1 10/03/19 09:52 10/07/19 17:44 191-24-2 Benzo(k)fluoranthene ND ug/kg 369 156 1 10/03/19 09:52 10/07/19 17:44 207-08-9 Benzoic Acid ND ug/kg 1850 399 1 10/03/19 09:52 10/07/19 17:44 65-85-0 v1 Benzyl alcohol ND ug/kg 739 196 1 10/03/19 09:52 10/07/19 17:44 100-51-6 v1 4-Bromophenylphenyl ether ND ug/kg 369 97.0 1 10/03/19 09:52 10/07/19 17:44 101-55-3 Butylbenzylphthalate ND ug/kg 369 98.4 1 10/03/19 09:52 10/07/19 17:44 85-68-7 4-Chloro-3-methyl phenol ND ug/kg 739 225 1 10/03/19 09:52 10/07/19 17:44 59-50-7 4-Chloroaniline ND ug/kg 1850 226 1 10/03/19 09:52 10/07/19 17:44 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 369 98.6 1 10/03/19 09:52 10/07/19 17:44 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 369 78.5 1 10/03/19 09:52 10/07/19 17:44 111-44-4 2-Chloronaphthalene ND ug/kg 369 82.3 1 10/03/19 09:52 10/07/19 17:44 91-58-7 2-Chlorophenol ND ug/kg 369 86.0 1 10/03/19 09:52 10/07/19 17:44 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 369 96.0 1 10/03/19 09:52 10/07/19 17:44 7005-72-3 Chrysene ND ug/kg 369 107 1 10/03/19 09:52 10/07/19 17:44 218-01-9 Dibenz(a,h)anthracene ND ug/kg 369 148 1 10/03/19 09:52 10/07/19 17:44 53-70-3 Dibenzofuran ND ug/kg 369 92.4 1 10/03/19 09:52 10/07/19 17:44 132-64-9 1,2-Dichlorobenzene ND ug/kg 369 79.9 1 10/03/19 09:52 10/07/19 17:44 95-50-1 1,3-Dichlorobenzene ND ug/kg 369 83.2 1 10/03/19 09:52 10/07/19 17:44 541-73-1 1,4-Dichlorobenzene ND ug/kg 369 81.3 1 10/03/19 09:52 10/07/19 17:44 106-46-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UNCC MOOR HALL Pace Project No.: 92447655 Sample: SSW Lab ID: 92447655001 Collected: 10/01/19 11:45 Received: 10/01/19 12:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 3,3'-Dichlorobenzidine ND ug/kg 1850 258 1 10/03/19 09:52 10/07/19 17:44 91-94-1 2,4-Dichlorophenol ND ug/kg 369 122 1 10/03/19 09:52 10/07/19 17:44 120-83-2 Diethylphthalate ND ug/kg 369 80.2 1 10/03/19 09:52 10/07/19 17:44 84-66-2 2,4-Dimethylphenol ND ug/kg 369 92.0 1 10/03/19 09:52 10/07/19 17:44 105-67-9 Dimethylphthalate ND ug/kg 369 83.5 1 10/03/19 09:52 10/07/19 17:44 131-11-3 Di-n-butylphthalate ND ug/kg 369 91.1 1 10/03/19 09:52 10/07/19 17:44 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 739 596 1 10/03/19 09:52 10/07/19 17:44 534-52-1 2,4-Dinitrophenol ND ug/kg 1850 1180 1 10/03/19 09:52 10/07/19 17:44 51-28-5 2,4-Dinitrotoluene ND ug/kg 369 97.9 1 10/03/19 09:52 10/07/19 17:44 121-14-2 2,6-Dinitrotoluene ND ug/kg 369 96.6 1 10/03/19 09:52 10/07/19 17:44 606-20-2 Di-n-octylphthalate ND ug/kg 369 210 1 10/03/19 09:52 10/07/19 17:44 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 369 121 1 10/03/19 09:52 10/07/19 17:44 117-81-7 Fluoranthene ND ug/kg 369 112 1 10/03/19 09:52 10/07/19 17:44 206-44-0 Fluorene ND ug/kg 369 98.9 1 10/03/19 09:52 10/07/19 17:44 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 369 89.8 1 10/03/19 09:52 10/07/19 17:44 87-68-3 Hexachlorobenzene ND ug/kg 369 93.8 1 10/03/19 09:52 10/07/19 17:44 118-74-1 Hexachlorocyclopentadiene ND ug/kg 369 148 1 10/03/19 09:52 10/07/19 17:44 77-47-4 Hexachloroethane ND ug/kg 369 84.2 1 10/03/19 09:52 10/07/19 17:44 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 369 169 1 10/03/19 09:52 10/07/19 17:44 193-39-5 Isophorone ND ug/kg 369 80.3 1 10/03/19 09:52 10/07/19 17:44 78-59-1 1-Methylnaphthalene ND ug/kg 369 98.4 1 10/03/19 09:52 10/07/19 17:44 90-12-0 2-Methylnaphthalene ND ug/kg 369 94.0 1 10/03/19 09:52 10/07/19 17:44 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 369 81.8 1 10/03/19 09:52 10/07/19 17:44 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 369 92.9 1 10/03/19 09:52 10/07/19 17:44 15831-10-4 Naphthalene ND ug/kg 369 88.4 1 10/03/19 09:52 10/07/19 17:44 91-20-3 2-Nitroaniline ND ug/kg 1850 186 1 10/03/19 09:52 10/07/19 17:44 88-74-4 3-Nitroaniline ND ug/kg 1850 196 1 10/03/19 09:52 10/07/19 17:44 99-09-2 4-Nitroaniline ND ug/kg 739 182 1 10/03/19 09:52 10/07/19 17:44 100-01-6 Nitrobenzene ND ug/kg 369 88.2 1 10/03/19 09:52 10/07/19 17:44 98-95-3 2-Nitrophenol ND ug/kg 369 114 1 10/03/19 09:52 10/07/19 17:44 88-75-5 4-Nitrophenol ND ug/kg 1850 589 1 10/03/19 09:52 10/07/19 17:44 100-02-7 N-Nitrosodimethylamine ND ug/kg 369 104 1 10/03/19 09:52 10/07/19 17:44 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 369 103 1 10/03/19 09:52 10/07/19 17:44 621-64-7 N-Nitrosodiphenylamine ND ug/kg 369 94.3 1 10/03/19 09:52 10/07/19 17:44 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 369 103 1 10/03/19 09:52 10/07/19 17:44 108-60-1 Pentachlorophenol ND ug/kg 1850 169 1 10/03/19 09:52 10/07/19 17:44 87-86-5 Phenanthrene ND ug/kg 369 93.0 1 10/03/19 09:52 10/07/19 17:44 85-01-8 Phenol ND ug/kg 369 88.2 1 10/03/19 09:52 10/07/19 17:44 108-95-2 Pyrene ND ug/kg 369 102 1 10/03/19 09:52 10/07/19 17:44 129-00-0 Pyridine ND ug/kg 369 93.5 1 10/03/19 09:52 10/07/19 17:44 110-86-1 1,2,4-Trichlorobenzene ND ug/kg 369 84.6 1 10/03/19 09:52 10/07/19 17:44 120-82-1 2,4,5-Trichlorophenol ND ug/kg 369 96.0 1 10/03/19 09:52 10/07/19 17:44 95-95-4 2,4,6-Trichlorophenol ND ug/kg 369 92.8 1 10/03/19 09:52 10/07/19 17:44 88-06-2 Surrogates Nitrobenzene-d5 (S) 61 % 23-110 1 10/03/19 09:52 10/07/19 17:44 4165-60-0 REPORT OF LABORATORY ANALYSIS v1 v1 This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 44 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UNCC MOOR HALL Pace Project No.: 92447655 Sample: SSW Lab ID: 92447655001 Collected: 10/01/19 11:45 Received: 10/01/19 12:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Surrogates 2-Fluorobiphenyl (S) 52 % 30-110 1 10/03/19 09:52 10/07/19 17:44 321-60-8 Terphenyl-d14 (S) 49 % 28-110 1 10/03/19 09:52 10/07/19 17:44 1718-51-0 Phenol-d6 (S) 56 % 22-110 1 10/03/19 09:52 10/07/19 17:44 13127-88-3 2-Fluorophenol (S) 57 % 13-110 1 10/03/19 09:52 10/07/19 17:44 367-12-4 2,4,6-Tribromophenol (S) 58 % 27-110 1 10/03/19 09:52 10/07/19 17:44 118-79-6 8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A Acetone 41.7J ug/kg 75.0 7.1 1 10/04/19 15:16 10/07/19 20:02 67-64-1 Benzene ND ug/kg 3.8 0.67 1 10/04/19 15:16 10/07/19 20:02 71-43-2 Bromobenzene ND ug/kg 3.8 1.0 1 10/04/19 15:16 10/07/19 20:02 108-86-1 Bromochloromethane ND ug/kg 3.8 0.92 1 10/04/19 15:16 10/07/19 20:02 74-97-5 Bromodichloromethane ND ug/kg 3.8 0.73 1 10/04/19 15:16 10/07/19 20:02 75-27-4 Bromoform ND ug/kg 3.8 1.8 1 10/04/19 15:16 10/07/19 20:02 75-25-2 Bromomethane ND ug/kg 7.5 1.8 1 10/04/19 15:16 10/07/19 20:02 74-83-9 2-Butanone (MEK) ND ug/kg 75.0 8.9 1 10/04/19 15:16 10/07/19 20:02 78-93-3 n-Butylbenzene ND ug/kg 3.8 2.1 1 10/04/19 15:16 10/07/19 20:02 104-51-8 sec-Butylbenzene ND ug/kg 3.8 1.6 1 10/04/19 15:16 10/07/19 20:02 135-98-8 tert-Butyl benzene ND ug/kg 3.8 1.3 1 10/04/19 15:16 10/07/19 20:02 98-06-6 Carbon tetrachloride ND ug/kg 3.8 0.72 1 10/04/19 15:16 10/07/19 20:02 56-23-5 Chlorobenzene ND ug/kg 3.8 0.73 1 10/04/19 15:16 10/07/19 20:02 108-90-7 Chloroethane ND ug/kg 7.5 1.6 1 10/04/19 15:16 10/07/19 20:02 75-00-3 Chloroform ND ug/kg 3.8 0.80 1 10/04/19 15:16 10/07/19 20:02 67-66-3 Chloromethane ND ug/kg 7.5 2.5 1 10/04/19 15:16 10/07/19 20:02 74-87-3 2-Chlorotoluene ND ug/kg 3.8 1.1 1 10/04/19 15:16 10/07/19 20:02 95-49-8 4-Chlorotoluene ND ug/kg 3.8 1.1 1 10/04/19 15:16 10/07/19 20:02 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 3.8 1.9 1 10/04/19 15:16 10/07/19 20:02 96-12-8 Dibromochloromethane ND ug/kg 3.8 1.9 1 10/04/19 15:16 10/07/19 20:02 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 3.8 0.84 1 10/04/19 15:16 10/07/19 20:02 106-93-4 Dibromomethane ND ug/kg 3.8 1.1 1 10/04/19 15:16 10/07/19 20:02 74-95-3 1,2-Dichlorobenzene ND ug/kg 3.8 1.3 1 10/04/19 15:16 10/07/19 20:02 95-50-1 1,3-Dichlorobenzene ND ug/kg 3.8 1.3 1 10/04/19 15:16 10/07/19 20:02 541-73-1 1,4-Dichlorobenzene ND ug/kg 3.8 1.3 1 10/04/19 15:16 10/07/19 20:02 106-46-7 Dichlorodifluoromethane ND ug/kg 7.5 3.1 1 10/04/19 15:16 10/07/19 20:02 75-71-8 1,1-Dichloroethane ND ug/kg 3.8 0.55 1 10/04/19 15:16 10/07/19 20:02 75-34-3 1,2-Dichloroethane ND ug/kg 3.8 0.75 1 10/04/19 15:16 10/07/19 20:02 107-06-2 1,1-Dichloroethene ND ug/kg 3.8 0.87 1 10/04/19 15:16 10/07/19 20:02 75-35-4 cis-1,2-Dichloroethene ND ug/kg 3.8 0.65 1 10/04/19 15:16 10/07/19 20:02 156-59-2 trans-1,2-Dichloroethene ND ug/kg 3.8 0.74 1 10/04/19 15:16 10/07/19 20:02 156-60-5 1,2-Dichloropropane ND ug/kg 3.8 1.4 1 10/04/19 15:16 10/07/19 20:02 78-87-5 1,3-Dichloropropane ND ug/kg 3.8 1.4 1 10/04/19 15:16 10/07/19 20:02 142-28-9 2,2-Dichloropropane ND ug/kg 3.8 0.37 1 10/04/19 15:16 10/07/19 20:02 594-20-7 1,1-Dichloropropene ND ug/kg 3.8 1.6 1 10/04/19 15:16 10/07/19 20:02 563-58-6 cis-1,3-Dichloropropene ND ug/kg 3.8 1.7 1 10/04/19 15:16 10/07/19 20:02 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 3.8 0.66 1 10/04/19 15:16 10/07/19 20:02 10061-02-6 REPORT OF LABORATORY ANALYSIS v1 v1 v1 This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 44 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UNCC MOOR HALL Pace Project No.: 92447655 Sample: SSW Lab ID: 92447655001 Collected: 10/01/19 11:45 Received: 10/01/19 12:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A Volatile Organics Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Analytical Method: EPA 8260D Preparation Method: EPA 5035A ND ug/kg 3.8 2.1 1 10/04/19 15:16 10/07/19 20:02 108-20-3 ND ug/kg 3.8 0.80 1 10/04/19 15:16 10/07/19 20:02 100-41-4 ND ug/kg 3.8 1.9 1 10/04/19 15:16 10/07/19 20:02 87-68-3 ND ug/kg 37.5 3.9 1 10/04/19 15:16 10/07/19 20:02 591-78-6 ND ug/kg 3.8 1.1 1 10/04/19 15:16 10/07/19 20:02 98-82-8 ND ug/kg 3.8 1.8 1 10/04/19 15:16 10/07/19 20:02 99-87-6 ND ug/kg 15.0 4.4 1 10/04/19 15:16 10/07/19 20:02 75-09-2 ND ug/kg 37.5 2.8 1 10/04/19 15:16 10/07/19 20:02 108-10-1 ND ug/kg 3.8 2.1 1 10/04/19 15:16 10/07/19 20:02 1634-04-4 ND ug/kg 3.8 3.2 1 10/04/19 15:16 10/07/19 20:02 91-20-3 ND ug/kg 3.8 1.3 1 10/04/19 15:16 10/07/19 20:02 103-65-1 ND ug/kg 3.8 1.1 1 10/04/19 15:16 10/07/19 20:02 100-42-5 ND ug/kg 3.8 0.92 1 10/04/19 15:16 10/07/19 20:02 630-20-6 ND ug/kg 3.8 1.3 1 10/04/19 15:16 10/07/19 20:02 79-34-5 ND ug/kg 3.8 1.2 1 10/04/19 15:16 10/07/19 20:02 127-18-4 ND ug/kg 3.8 1.2 1 10/04/19 15:16 10/07/19 20:02 108-88-3 ND ug/kg 3.8 2.7 1 10/04/19 15:16 10/07/19 20:02 87-61-6 ND ug/kg 3.8 2.0 1 10/04/19 15:16 10/07/19 20:02 120-82-1 ND ug/kg 3.8 0.65 1 10/04/19 15:16 10/07/19 20:02 71-55-6 ND ug/kg 3.8 0.85 1 10/04/19 15:16 10/07/19 20:02 79-00-5 ND ug/kg 3.8 0.98 1 10/04/19 15:16 10/07/19 20:02 79-01-6 ND ug/kg 3.8 0.89 1 10/04/19 15:16 10/07/19 20:02 75-69-4 ND ug/kg 3.8 1.3 1 10/04/19 15:16 10/07/19 20:02 96-18-4 ND ug/kg 3.8 1.5 1 10/04/19 15:16 10/07/19 20:02 95-63-6 ND ug/kg 3.8 1.3 1 10/04/19 15:16 10/07/19 20:02 108-67-8 ND ug/kg 37.5 12.2 1 10/04/19 15:16 10/07/19 20:02 108-05-4 IK ND ug/kg 7.5 1.4 1 10/04/19 15:16 10/07/19 20:02 75-01-4 ND ug/kg 7.5 2.6 1 10/04/19 15:16 10/07/19 20:02 1330-20-7 ND ug/kg 7.5 1.8 1 10/04/19 15:16 10/07/19 20:02 179601-23-1 ND ug/kg 3.8 0.88 1 10/04/19 15:16 10/07/19 20:02 95-47-6 104 % 70-130 1 10/04/19 15:16 10/07/19 20:02 2037-26-5 102 % 70-130 1 10/04/19 15:16 10/07/19 20:02 460-00-4 99 % 70-132 1 10/04/19 15:16 10/07/19 20:02 17060-07-0 Analytical Method: ASTM D2974-87 10.7 % 0.10 0.10 1 REPORT OF LABORATORY ANALYSIS 10/01/19 14:36 This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 44 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UNCC MOOR HALL Pace Project No.: 92447655 Sample: ESW Lab ID: 92447655002 Collected: 10/01/19 11:17 Received: 10/01/19 12:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual MADEP EPH NC Soil Analytical Method: MADEP EPH Preparation Method: MADEP EPH Aliphatic (C09-C18) 69.9 mg/kg 22.0 22.0 2 10/03/19 09:50 10/08/19 12:27 N2 Aliphatic (C19-C36) ND mg/kg 22.0 22.0 2 10/03/19 09:50 10/08/19 12:27 N2 Aromatic (C11-C22) 11.2 mg/kg 11.0 11.0 1 10/03/19 09:50 10/07/19 20:45 N2 Surrogates Nonatriacontane (S) 61 % 40-140 2 10/03/19 09:50 10/08/19 12:27 7194-86-7 o-Terphenyl (S) 75 % 40-140 1 10/03/19 09:50 10/07/19 20:45 84-15-1 2-Fluorobiphenyl (S) 110 % 40-140 1 10/03/19 09:50 10/07/19 20:45 321-60-8 2-Bromonaphthalene (S) 117 % 40-140 1 10/03/19 09:50 10/07/19 20:45 580-13-2 VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH Aliphatic (C05-CO8) ND mg/kg 2.1 2.1 1 10/02/19 14:49 10/02/19 17:32 N2 Aliphatic (C09-C12) 8.1 mg/kg 2.1 2.1 1 10/02/19 14:49 10/02/19 17:32 N2 Aliphatic(C09-C12) Adjusted 6.0 mg/kg 2.1 2.1 1 10/02/19 14:49 10/02/19 17:32 N2 Aromatic (C09-C10) ND mg/kg 2.1 2.1 1 10/02/19 14:49 10/02/19 17:32 N2 Surrogates 4-Bromofluorobenzene (FID) (S) 103 % 70-130 1 10/02/19 14:49 10/02/19 17:32 460-00-4 4-Bromofluorobenzene (PID) (S) 88 % 70-130 1 10/02/19 14:49 10/02/19 17:32 460-00-4 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Acenaphthene ND ug/kg 364 93.5 1 10/03/19 09:52 10/07/19 18:13 83-32-9 Acenaphthylene ND ug/kg 364 86.1 1 10/03/19 09:52 10/07/19 18:13 208-96-8 Aniline ND ug/kg 364 81.6 1 10/03/19 09:52 10/07/19 18:13 62-53-3 Anthracene ND ug/kg 364 94.3 1 10/03/19 09:52 10/07/19 18:13 120-12-7 Benzo(a)anthracene ND ug/kg 364 116 1 10/03/19 09:52 10/07/19 18:13 56-55-3 Benzo(a)pyrene ND ug/kg 364 158 1 10/03/19 09:52 10/07/19 18:13 50-32-8 Benzo(b)fluoranthene ND ug/kg 364 147 1 10/03/19 09:52 10/07/19 18:13 205-99-2 Benzo(g,h,i)perylene ND ug/kg 364 142 1 10/03/19 09:52 10/07/19 18:13 191-24-2 Benzo(k)fluoranthene ND ug/kg 364 153 1 10/03/19 09:52 10/07/19 18:13 207-08-9 Benzoic Acid ND ug/kg 1820 392 1 10/03/19 09:52 10/07/19 18:13 65-85-0 v1 Benzyl alcohol ND ug/kg 727 193 1 10/03/19 09:52 10/07/19 18:13 100-51-6 v1 4-Bromophenylphenyl ether ND ug/kg 364 95.4 1 10/03/19 09:52 10/07/19 18:13 101-55-3 Butylbenzylphthalate ND ug/kg 364 96.9 1 10/03/19 09:52 10/07/19 18:13 85-68-7 4-Chloro-3-methyl phenol ND ug/kg 727 221 1 10/03/19 09:52 10/07/19 18:13 59-50-7 4-Chloroaniline ND ug/kg 1820 223 1 10/03/19 09:52 10/07/19 18:13 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 364 97.1 1 10/03/19 09:52 10/07/19 18:13 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 364 77.2 1 10/03/19 09:52 10/07/19 18:13 111-44-4 2-Chloronaphthalene ND ug/kg 364 81.0 1 10/03/19 09:52 10/07/19 18:13 91-58-7 2-Chlorophenol ND ug/kg 364 84.6 1 10/03/19 09:52 10/07/19 18:13 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 364 94.4 1 10/03/19 09:52 10/07/19 18:13 7005-72-3 Chrysene ND ug/kg 364 106 1 10/03/19 09:52 10/07/19 18:13 218-01-9 Dibenz(a,h)anthracene ND ug/kg 364 145 1 10/03/19 09:52 10/07/19 18:13 53-70-3 Dibenzofuran ND ug/kg 364 90.9 1 10/03/19 09:52 10/07/19 18:13 132-64-9 1,2-Dichlorobenzene ND ug/kg 364 78.7 1 10/03/19 09:52 10/07/19 18:13 95-50-1 1,3-Dichlorobenzene ND ug/kg 364 81.9 1 10/03/19 09:52 10/07/19 18:13 541-73-1 1,4-Dichlorobenzene ND ug/kg 364 80.0 1 10/03/19 09:52 10/07/19 18:13 106-46-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UNCC MOOR HALL Pace Project No.: 92447655 Sample: ESW Lab ID: 92447655002 Collected: 10/01/19 11:17 Received: 10/01/19 12:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 3,3'-Dichlorobenzidine ND ug/kg 1820 253 1 10/03/19 09:52 10/07/19 18:13 91-94-1 2,4-Dichlorophenol ND ug/kg 364 120 1 10/03/19 09:52 10/07/19 18:13 120-83-2 Diethylphthalate ND ug/kg 364 78.9 1 10/03/19 09:52 10/07/19 18:13 84-66-2 2,4-Dimethylphenol ND ug/kg 364 90.6 1 10/03/19 09:52 10/07/19 18:13 105-67-9 Dimethylphthalate ND ug/kg 364 82.2 1 10/03/19 09:52 10/07/19 18:13 131-11-3 Di-n-butylphthalate ND ug/kg 364 89.7 1 10/03/19 09:52 10/07/19 18:13 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 727 586 1 10/03/19 09:52 10/07/19 18:13 534-52-1 2,4-Dinitrophenol ND ug/kg 1820 1160 1 10/03/19 09:52 10/07/19 18:13 51-28-5 2,4-Dinitrotoluene ND ug/kg 364 96.3 1 10/03/19 09:52 10/07/19 18:13 121-14-2 2,6-Dinitrotoluene ND ug/kg 364 95.1 1 10/03/19 09:52 10/07/19 18:13 606-20-2 Di-n-octylphthalate ND ug/kg 364 207 1 10/03/19 09:52 10/07/19 18:13 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 364 119 1 10/03/19 09:52 10/07/19 18:13 117-81-7 Fluoranthene ND ug/kg 364 110 1 10/03/19 09:52 10/07/19 18:13 206-44-0 Fluorene ND ug/kg 364 97.3 1 10/03/19 09:52 10/07/19 18:13 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 364 88.4 1 10/03/19 09:52 10/07/19 18:13 87-68-3 Hexachlorobenzene ND ug/kg 364 92.3 1 10/03/19 09:52 10/07/19 18:13 118-74-1 Hexachlorocyclopentadiene ND ug/kg 364 145 1 10/03/19 09:52 10/07/19 18:13 77-47-4 Hexachloroethane ND ug/kg 364 82.9 1 10/03/19 09:52 10/07/19 18:13 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 364 166 1 10/03/19 09:52 10/07/19 18:13 193-39-5 Isophorone ND ug/kg 364 79.0 1 10/03/19 09:52 10/07/19 18:13 78-59-1 1-Methylnaphthalene ND ug/kg 364 96.9 1 10/03/19 09:52 10/07/19 18:13 90-12-0 2-Methylnaphthalene ND ug/kg 364 92.6 1 10/03/19 09:52 10/07/19 18:13 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 364 80.5 1 10/03/19 09:52 10/07/19 18:13 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 364 91.5 1 10/03/19 09:52 10/07/19 18:13 15831-10-4 Naphthalene ND ug/kg 364 87.0 1 10/03/19 09:52 10/07/19 18:13 91-20-3 2-Nitroaniline ND ug/kg 1820 183 1 10/03/19 09:52 10/07/19 18:13 88-74-4 3-Nitroaniline ND ug/kg 1820 193 1 10/03/19 09:52 10/07/19 18:13 99-09-2 4-Nitroaniline ND ug/kg 727 180 1 10/03/19 09:52 10/07/19 18:13 100-01-6 Nitrobenzene ND ug/kg 364 86.8 1 10/03/19 09:52 10/07/19 18:13 98-95-3 2-Nitrophenol ND ug/kg 364 112 1 10/03/19 09:52 10/07/19 18:13 88-75-5 4-Nitrophenol ND ug/kg 1820 580 1 10/03/19 09:52 10/07/19 18:13 100-02-7 N-Nitrosodimethylamine ND ug/kg 364 102 1 10/03/19 09:52 10/07/19 18:13 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 364 102 1 10/03/19 09:52 10/07/19 18:13 621-64-7 N-Nitrosodiphenylamine ND ug/kg 364 92.8 1 10/03/19 09:52 10/07/19 18:13 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 364 101 1 10/03/19 09:52 10/07/19 18:13 108-60-1 Pentachlorophenol ND ug/kg 1820 166 1 10/03/19 09:52 10/07/19 18:13 87-86-5 Phenanthrene ND ug/kg 364 91.6 1 10/03/19 09:52 10/07/19 18:13 85-01-8 Phenol ND ug/kg 364 86.8 1 10/03/19 09:52 10/07/19 18:13 108-95-2 Pyrene ND ug/kg 364 100 1 10/03/19 09:52 10/07/19 18:13 129-00-0 Pyridine ND ug/kg 364 92.0 1 10/03/19 09:52 10/07/19 18:13 110-86-1 1,2,4-Trichlorobenzene ND ug/kg 364 83.3 1 10/03/19 09:52 10/07/19 18:13 120-82-1 2,4,5-Trichlorophenol ND ug/kg 364 94.4 1 10/03/19 09:52 10/07/19 18:13 95-95-4 2,4,6-Trichlorophenol ND ug/kg 364 91.3 1 10/03/19 09:52 10/07/19 18:13 88-06-2 Surrogates Nitrobenzene-d5 (S) 68 % 23-110 1 10/03/19 09:52 10/07/19 18:13 4165-60-0 REPORT OF LABORATORY ANALYSIS v1 v1 This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 44 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UNCC MOOR HALL Pace Project No.: 92447655 Sample: ESW Lab ID: 92447655002 Collected: 10/01/19 11:17 Received: 10/01/19 12:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Surrogates 2-Fluorobiphenyl (S) 69 % 30-110 1 10/03/19 09:52 10/07/19 18:13 321-60-8 Terphenyl-d14 (S) 65 % 28-110 1 10/03/19 09:52 10/07/19 18:13 1718-51-0 Phenol-d6 (S) 66 % 22-110 1 10/03/19 09:52 10/07/19 18:13 13127-88-3 2-Fluorophenol (S) 64 % 13-110 1 10/03/19 09:52 10/07/19 18:13 367-12-4 2,4,6-Tribromophenol (S) 78 % 27-110 1 10/03/19 09:52 10/07/19 18:13 118-79-6 8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A Acetone 34.OJ ug/kg 75.5 7.1 1 10/08/19 13:22 10/08/19 13:29 67-64-1 Benzene ND ug/kg 3.8 0.68 1 10/08/19 13:22 10/08/19 13:29 71-43-2 Bromobenzene ND ug/kg 3.8 1.0 1 10/08/19 13:22 10/08/19 13:29 108-86-1 Bromochloromethane ND ug/kg 3.8 0.93 1 10/08/19 13:22 10/08/19 13:29 74-97-5 Bromodichloromethane ND ug/kg 3.8 0.74 1 10/08/19 13:22 10/08/19 13:29 75-27-4 Bromoform ND ug/kg 3.8 1.8 1 10/08/19 13:22 10/08/19 13:29 75-25-2 Bromomethane ND ug/kg 7.5 1.8 1 10/08/19 13:22 10/08/19 13:29 74-83-9 2-Butanone (MEK) ND ug/kg 75.5 9.0 1 10/08/19 13:22 10/08/19 13:29 78-93-3 n-Butylbenzene ND ug/kg 3.8 2.1 1 10/08/19 13:22 10/08/19 13:29 104-51-8 sec-Butylbenzene 2.5J ug/kg 3.8 1.6 1 10/08/19 13:22 10/08/19 13:29 135-98-8 tert-Butyl benzene ND ug/kg 3.8 1.3 1 10/08/19 13:22 10/08/19 13:29 98-06-6 Carbon tetrachloride ND ug/kg 3.8 0.72 1 10/08/19 13:22 10/08/19 13:29 56-23-5 Chlorobenzene ND ug/kg 3.8 0.73 1 10/08/19 13:22 10/08/19 13:29 108-90-7 Chloroethane ND ug/kg 7.5 1.6 1 10/08/19 13:22 10/08/19 13:29 75-00-3 Chloroform ND ug/kg 3.8 0.80 1 10/08/19 13:22 10/08/19 13:29 67-66-3 Chloromethane ND ug/kg 7.5 2.5 1 10/08/19 13:22 10/08/19 13:29 74-87-3 2-Chlorotoluene ND ug/kg 3.8 1.1 1 10/08/19 13:22 10/08/19 13:29 95-49-8 4-Chlorotoluene ND ug/kg 3.8 1.1 1 10/08/19 13:22 10/08/19 13:29 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 3.8 1.9 1 10/08/19 13:22 10/08/19 13:29 96-12-8 Dibromochloromethane ND ug/kg 3.8 1.9 1 10/08/19 13:22 10/08/19 13:29 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 3.8 0.85 1 10/08/19 13:22 10/08/19 13:29 106-93-4 Dibromomethane ND ug/kg 3.8 1.1 1 10/08/19 13:22 10/08/19 13:29 74-95-3 1,2-Dichlorobenzene ND ug/kg 3.8 1.3 1 10/08/19 13:22 10/08/19 13:29 95-50-1 1,3-Dichlorobenzene ND ug/kg 3.8 1.3 1 10/08/19 13:22 10/08/19 13:29 541-73-1 1,4-Dichlorobenzene ND ug/kg 3.8 1.3 1 10/08/19 13:22 10/08/19 13:29 106-46-7 Dichlorodifluoromethane ND ug/kg 7.5 3.1 1 10/08/19 13:22 10/08/19 13:29 75-71-8 1,1-Dichloroethane ND ug/kg 3.8 0.55 1 10/08/19 13:22 10/08/19 13:29 75-34-3 1,2-Dichloroethane ND ug/kg 3.8 0.75 1 10/08/19 13:22 10/08/19 13:29 107-06-2 1,1-Dichloroethene ND ug/kg 3.8 0.88 1 10/08/19 13:22 10/08/19 13:29 75-35-4 cis-1,2-Dichloroethene ND ug/kg 3.8 0.66 1 10/08/19 13:22 10/08/19 13:29 156-59-2 trans-1,2-Dichloroethene ND ug/kg 3.8 0.74 1 10/08/19 13:22 10/08/19 13:29 156-60-5 1,2-Dichloropropane ND ug/kg 3.8 1.4 1 10/08/19 13:22 10/08/19 13:29 78-87-5 1,3-Dichloropropane ND ug/kg 3.8 1.4 1 10/08/19 13:22 10/08/19 13:29 142-28-9 2,2-Dichloropropane ND ug/kg 3.8 0.37 1 10/08/19 13:22 10/08/19 13:29 594-20-7 1,1-Dichloropropene ND ug/kg 3.8 1.6 1 10/08/19 13:22 10/08/19 13:29 563-58-6 cis-1,3-Dichloropropene ND ug/kg 3.8 1.7 1 10/08/19 13:22 10/08/19 13:29 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 3.8 0.66 1 10/08/19 13:22 10/08/19 13:29 10061-02-6 REPORT OF LABORATORY ANALYSIS v1 This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 44 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UNCC MOOR HALL Pace Project No.: 92447655 Sample: ESW Lab ID: 92447655002 Collected: 10/01/19 11:17 Received: 10/01/19 12:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A Volatile Organics Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Analytical Method: EPA 8260D Preparation Method: EPA 5035A ND ug/kg 3.8 2.2 1 10/08/1913:22 10/08/1913:29 108-20-3 ND ug/kg 3.8 0.80 1 10/08/1913:22 10/08/1913:29 100-41-4 ND ug/kg 3.8 1.9 1 10/08/1913:22 10/08/1913:29 87-68-3 ND ug/kg 37.7 3.9 1 10/08/1913:22 10/08/1913:29 591-78-6 ND ug/kg 3.8 1.1 1 10/08/1913:22 10/08/1913:29 98-82-8 ND ug/kg 3.8 1.8 1 10/08/1913:22 10/08/1913:29 99-87-6 ND ug/kg 15.1 4.5 1 10/08/1913:22 10/08/1913:29 75-09-2 5.8J ug/kg 37.7 2.8 1 10/08/1913:22 10/08/1913:29 108-10-1 ND ug/kg 3.8 2.2 1 10/08/1913:22 10/08/1913:29 1634-04-4 ND ug/kg 3.8 3.2 1 10/08/1913:22 10/08/1913:29 91-20-3 ND ug/kg 3.8 1.3 1 10/08/1913:22 10/08/1913:29 103-65-1 ND ug/kg 3.8 1.1 1 10/08/1913:22 10/08/1913:29 100-42-5 ND ug/kg 3.8 0.93 1 10/08/1913:22 10/08/1913:29 630-20-6 ND ug/kg 3.8 1.3 1 10/08/1913:22 10/08/1913:29 79-34-5 ND ug/kg 3.8 1.2 1 10/08/1913:22 10/08/1913:29 127-18-4 ND ug/kg 3.8 1.2 1 10/08/1913:22 10/08/1913:29 108-88-3 ND ug/kg 3.8 2.7 1 10/08/1913:22 10/08/1913:29 87-61-6 ND ug/kg 3.8 2.0 1 10/08/1913:22 10/08/1913:29 120-82-1 ND ug/kg 3.8 0.66 1 10/08/1913:22 10/08/1913:29 71-55-6 ND ug/kg 3.8 0.85 1 10/08/1913:22 10/08/1913:29 79-00-5 ND ug/kg 3.8 0.98 1 10/08/1913:22 10/08/1913:29 79-01-6 ND ug/kg 3.8 0.89 1 10/08/1913:22 10/08/1913:29 75-69-4 ND ug/kg 3.8 1.3 1 10/08/1913:22 10/08/1913:29 96-18-4 2.OJ ug/kg 3.8 1.5 1 10/08/1913:22 10/08/1913:29 95-63-6 ND ug/kg 3.8 1.3 1 10/08/1913:22 10/08/1913:29 108-67-8 ND ug/kg 37.7 12.3 1 10/08/1913:22 10/08/1913:29 108-05-4 ND ug/kg 7.5 1.4 1 10/08/1913:22 10/08/1913:29 75-01-4 ND ug/kg 7.5 2.6 1 10/08/1913:22 10/08/1913:29 1330-20-7 ND ug/kg 7.5 1.8 1 10/08/1913:22 10/08/1913:29 179601-23-1 ND ug/kg 3.8 0.88 1 10/08/1913:22 10/08/1913:29 95-47-6 ill % 70-130 1 10/08/19 13:22 10/08/19 13:29 2037-26-5 108 % 70-130 1 10/08/1913:22 10/08/1913:29 460-00-4 109 % 70-132 1 10/08/1913:22 10/08/1913:29 17060-07-0 Analytical Method: ASTM D2974-87 9.2 % 0.10 0.10 1 REPORT OF LABORATORY ANALYSIS 10/01/19 14:36 B,vl IK This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UNCC MOOR HALL Pace Project No.: 92447655 Sample: BOTTOM Lab ID: 92447655003 Collected: 10/01/19 11:30 Received: 10/01/19 12:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual MADEP EPH NC Soil Analytical Method: MADEP EPH Preparation Method: MADEP EPH Aliphatic (C09-C18) ND mg/kg 11.9 11.9 1 10/03/19 09:50 10/07/19 21:12 N2 Aliphatic (C19-C36) ND mg/kg 11.9 11.9 1 10/03/19 09:50 10/07/19 21:12 N2 Aromatic (C11-C22) ND mg/kg 11.9 11.9 1 10/03/19 09:50 10/07/19 21:12 N2 Surrogates Nonatriacontane (S) 67 % 40-140 1 10/03/19 09:50 10/07/19 21:12 7194-86-7 o-Terphenyl (S) 76 % 40-140 1 10/03/19 09:50 10/07/19 21:12 84-15-1 2-Fluorobiphenyl (S) 91 % 40-140 1 10/03/19 09:50 10/07/19 21:12 321-60-8 2-Bromonaphthalene (S) 92 % 40-140 1 10/03/19 09:50 10/07/19 21:12 580-13-2 VPH NC Soil Analytical Method: MADEP VPH Preparation Method: MADEP VPH Aliphatic (C05-CO8) ND mg/kg 2.3 2.3 1 10/02/19 14:49 10/02/19 17:03 N2 Aliphatic (C09-C12) ND mg/kg 2.3 2.3 1 10/02/19 14:49 10/02/19 17:03 N2 Aliphatic(C09-C12)Adjusted ND mg/kg 2.3 2.3 1 10/02/19 14:49 10/02/19 17:03 N2 Aromatic (C09-C10) ND mg/kg 2.3 2.3 1 10/02/19 14:49 10/02/19 17:03 N2 Surrogates 4-Bromofluorobenzene (FID) (S) 84 % 70-130 1 10/02/19 14:49 10/02/19 17:03 460-00-4 4-Bromofluorobenzene (PID) (S) 86 % 70-130 1 10/02/19 14:49 10/02/19 17:03 460-00-4 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Acenaphthene ND ug/kg 393 101 1 10/03/19 09:52 10/07/19 18:43 83-32-9 Acenaphthylene ND ug/kg 393 93.0 1 10/03/19 09:52 10/07/19 18:43 208-96-8 Aniline ND ug/kg 393 88.2 1 10/03/19 09:52 10/07/19 18:43 62-53-3 Anthracene ND ug/kg 393 102 1 10/03/19 09:52 10/07/19 18:43 120-12-7 Benzo(a)anthracene ND ug/kg 393 125 1 10/03/19 09:52 10/07/19 18:43 56-55-3 Benzo(a)pyrene ND ug/kg 393 170 1 10/03/19 09:52 10/07/19 18:43 50-32-8 Benzo(b)fluoranthene ND ug/kg 393 158 1 10/03/19 09:52 10/07/19 18:43 205-99-2 Benzo(g,h,i)perylene ND ug/kg 393 154 1 10/03/19 09:52 10/07/19 18:43 191-24-2 Benzo(k)fluoranthene ND ug/kg 393 166 1 10/03/19 09:52 10/07/19 18:43 207-08-9 Benzoic Acid ND ug/kg 1960 424 1 10/03/19 09:52 10/07/19 18:43 65-85-0 v1 Benzyl alcohol ND ug/kg 786 208 1 10/03/19 09:52 10/07/19 18:43 100-51-6 v1 4-Bromophenylphenyl ether ND ug/kg 393 103 1 10/03/19 09:52 10/07/19 18:43 101-55-3 Butylbenzylphthalate ND ug/kg 393 105 1 10/03/19 09:52 10/07/19 18:43 85-68-7 4-Chloro-3-methyl phenol ND ug/kg 786 239 1 10/03/19 09:52 10/07/19 18:43 59-50-7 4-Chloroaniline ND ug/kg 1960 241 1 10/03/19 09:52 10/07/19 18:43 106-47-8 bis(2-Chloroethoxy)methane ND ug/kg 393 105 1 10/03/19 09:52 10/07/19 18:43 111-91-1 bis(2-Chloroethyl) ether ND ug/kg 393 83.5 1 10/03/19 09:52 10/07/19 18:43 111-44-4 2-Chloronaphthalene ND ug/kg 393 87.5 1 10/03/19 09:52 10/07/19 18:43 91-58-7 2-Chlorophenol ND ug/kg 393 91.5 1 10/03/19 09:52 10/07/19 18:43 95-57-8 4-Chlorophenylphenyl ether ND ug/kg 393 102 1 10/03/19 09:52 10/07/19 18:43 7005-72-3 Chrysene ND ug/kg 393 114 1 10/03/19 09:52 10/07/19 18:43 218-01-9 Dibenz(a,h)anthracene ND ug/kg 393 157 1 10/03/19 09:52 10/07/19 18:43 53-70-3 Dibenzofuran ND ug/kg 393 98.2 1 10/03/19 09:52 10/07/19 18:43 132-64-9 1,2-Dichlorobenzene ND ug/kg 393 85.0 1 10/03/19 09:52 10/07/19 18:43 95-50-1 1,3-Dichlorobenzene ND ug/kg 393 88.5 1 10/03/19 09:52 10/07/19 18:43 541-73-1 1,4-Dichlorobenzene ND ug/kg 393 86.5 1 10/03/19 09:52 10/07/19 18:43 106-46-7 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UNCC MOOR HALL Pace Project No.: 92447655 Sample: BOTTOM Lab ID: 92447655003 Collected: 10/01/19 11:30 Received: 10/01/19 12:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 3,3'-Dichlorobenzidine ND ug/kg 1960 274 1 10/03/19 09:52 10/07/19 18:43 91-94-1 2,4-Dichlorophenol ND ug/kg 393 130 1 10/03/19 09:52 10/07/19 18:43 120-83-2 Diethylphthalate ND ug/kg 393 85.3 1 10/03/19 09:52 10/07/19 18:43 84-66-2 2,4-Dimethylphenol ND ug/kg 393 97.9 1 10/03/19 09:52 10/07/19 18:43 105-67-9 Dimethylphthalate ND ug/kg 393 88.8 1 10/03/19 09:52 10/07/19 18:43 131-11-3 Di-n-butylphthalate ND ug/kg 393 96.9 1 10/03/19 09:52 10/07/19 18:43 84-74-2 4,6-Dinitro-2-methyl phenol ND ug/kg 786 634 1 10/03/19 09:52 10/07/19 18:43 534-52-1 2,4-Dinitrophenol ND ug/kg 1960 1260 1 10/03/19 09:52 10/07/19 18:43 51-28-5 2,4-Dinitrotoluene ND ug/kg 393 104 1 10/03/19 09:52 10/07/19 18:43 121-14-2 2,6-Dinitrotoluene ND ug/kg 393 103 1 10/03/19 09:52 10/07/19 18:43 606-20-2 Di-n-octylphthalate ND ug/kg 393 224 1 10/03/19 09:52 10/07/19 18:43 117-84-0 bis(2- Ethyl hexyl)phthalate ND ug/kg 393 129 1 10/03/19 09:52 10/07/19 18:43 117-81-7 Fluoranthene ND ug/kg 393 119 1 10/03/19 09:52 10/07/19 18:43 206-44-0 Fluorene ND ug/kg 393 105 1 10/03/19 09:52 10/07/19 18:43 86-73-7 Hexachloro-1,3-butadiene ND ug/kg 393 95.5 1 10/03/19 09:52 10/07/19 18:43 87-68-3 Hexachlorobenzene ND ug/kg 393 99.8 1 10/03/19 09:52 10/07/19 18:43 118-74-1 Hexachlorocyclopentadiene ND ug/kg 393 157 1 10/03/19 09:52 10/07/19 18:43 77-47-4 Hexachloroethane ND ug/kg 393 89.6 1 10/03/19 09:52 10/07/19 18:43 67-72-1 Indeno(1,2,3-cd)pyrene ND ug/kg 393 180 1 10/03/19 09:52 10/07/19 18:43 193-39-5 Isophorone ND ug/kg 393 85.4 1 10/03/19 09:52 10/07/19 18:43 78-59-1 1-Methylnaphthalene ND ug/kg 393 105 1 10/03/19 09:52 10/07/19 18:43 90-12-0 2-Methylnaphthalene ND ug/kg 393 100 1 10/03/19 09:52 10/07/19 18:43 91-57-6 2-Methylphenol(o-Cresol) ND ug/kg 393 87.1 1 10/03/19 09:52 10/07/19 18:43 95-48-7 3&4-Methyl phenol (m&p Cresol) ND ug/kg 393 98.8 1 10/03/19 09:52 10/07/19 18:43 15831-10-4 Naphthalene ND ug/kg 393 94.1 1 10/03/19 09:52 10/07/19 18:43 91-20-3 2-Nitroaniline ND ug/kg 1960 198 1 10/03/19 09:52 10/07/19 18:43 88-74-4 3-Nitroaniline ND ug/kg 1960 208 1 10/03/19 09:52 10/07/19 18:43 99-09-2 4-Nitroaniline ND ug/kg 786 194 1 10/03/19 09:52 10/07/19 18:43 100-01-6 Nitrobenzene ND ug/kg 393 93.8 1 10/03/19 09:52 10/07/19 18:43 98-95-3 2-Nitrophenol ND ug/kg 393 121 1 10/03/19 09:52 10/07/19 18:43 88-75-5 4-Nitrophenol ND ug/kg 1960 626 1 10/03/19 09:52 10/07/19 18:43 100-02-7 N-Nitrosodimethylamine ND ug/kg 393 ill 1 10/03/19 09:52 10/07/19 18:43 62-75-9 N-Nitroso-di-n-propylamine ND ug/kg 393 110 1 10/03/19 09:52 10/07/19 18:43 621-64-7 N-Nitrosodiphenylamine ND ug/kg 393 100 1 10/03/19 09:52 10/07/19 18:43 86-30-6 2,2'-Oxybis(1-chloropropane) ND ug/kg 393 109 1 10/03/19 09:52 10/07/19 18:43 108-60-1 Pentachlorophenol ND ug/kg 1960 180 1 10/03/19 09:52 10/07/19 18:43 87-86-5 Phenanthrene ND ug/kg 393 99.0 1 10/03/19 09:52 10/07/19 18:43 85-01-8 Phenol ND ug/kg 393 93.8 1 10/03/19 09:52 10/07/19 18:43 108-95-2 Pyrene ND ug/kg 393 108 1 10/03/19 09:52 10/07/19 18:43 129-00-0 Pyridine ND ug/kg 393 99.4 1 10/03/19 09:52 10/07/19 18:43 110-86-1 1,2,4-Trichlorobenzene ND ug/kg 393 90.0 1 10/03/19 09:52 10/07/19 18:43 120-82-1 2,4,5-Trichlorophenol ND ug/kg 393 102 1 10/03/19 09:52 10/07/19 18:43 95-95-4 2,4,6-Trichlorophenol ND ug/kg 393 98.7 1 10/03/19 09:52 10/07/19 18:43 88-06-2 Surrogates Nitrobenzene-d5 (S) 55 % 23-110 1 10/03/19 09:52 10/07/19 18:43 4165-60-0 REPORT OF LABORATORY ANALYSIS vl vl This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 44 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UNCC MOOR HALL Pace Project No.: 92447655 Sample: BOTTOM Lab ID: 92447655003 Collected: 10/01/19 11:30 Received: 10/01/19 12:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8270E MSSV Microwave Analytical Method: EPA 8270E Preparation Method: EPA 3546 Surrogates 2-Fluorobiphenyl (S) 40 % 30-110 1 10/03/19 09:52 10/07/19 18:43 321-60-8 Terphenyl-d14 (S) 44 % 28-110 1 10/03/19 09:52 10/07/19 18:43 1718-51-0 Phenol-d6 (S) 51 % 22-110 1 10/03/19 09:52 10/07/19 18:43 13127-88-3 2-Fluorophenol (S) 53 % 13-110 1 10/03/19 09:52 10/07/19 18:43 367-12-4 2,4,6-Tribromophenol (S) 64 % 27-110 1 10/03/19 09:52 10/07/19 18:43 118-79-6 8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A Acetone ND ug/kg 75.2 7.1 1 10/04/19 15:16 10/07/19 20:26 67-64-1 Benzene ND ug/kg 3.8 0.67 1 10/04/19 15:16 10/07/19 20:26 71-43-2 Bromobenzene ND ug/kg 3.8 1.0 1 10/04/19 15:16 10/07/19 20:26 108-86-1 Bromochloromethane ND ug/kg 3.8 0.92 1 10/04/19 15:16 10/07/19 20:26 74-97-5 Bromodichloromethane ND ug/kg 3.8 0.74 1 10/04/19 15:16 10/07/19 20:26 75-27-4 Bromoform ND ug/kg 3.8 1.8 1 10/04/19 15:16 10/07/19 20:26 75-25-2 Bromomethane ND ug/kg 7.5 1.8 1 10/04/19 15:16 10/07/19 20:26 74-83-9 2-Butanone (MEK) ND ug/kg 75.2 8.9 1 10/04/19 15:16 10/07/19 20:26 78-93-3 n-Butylbenzene ND ug/kg 3.8 2.1 1 10/04/19 15:16 10/07/19 20:26 104-51-8 sec-Butylbenzene ND ug/kg 3.8 1.6 1 10/04/19 15:16 10/07/19 20:26 135-98-8 tert-Butyl benzene ND ug/kg 3.8 1.3 1 10/04/19 15:16 10/07/19 20:26 98-06-6 Carbon tetrachloride ND ug/kg 3.8 0.72 1 10/04/19 15:16 10/07/19 20:26 56-23-5 Chlorobenzene ND ug/kg 3.8 0.73 1 10/04/19 15:16 10/07/19 20:26 108-90-7 Chloroethane ND ug/kg 7.5 1.6 1 10/04/19 15:16 10/07/19 20:26 75-00-3 Chloroform ND ug/kg 3.8 0.80 1 10/04/19 15:16 10/07/19 20:26 67-66-3 Chloromethane ND ug/kg 7.5 2.5 1 10/04/19 15:16 10/07/19 20:26 74-87-3 2-Chlorotoluene ND ug/kg 3.8 1.1 1 10/04/19 15:16 10/07/19 20:26 95-49-8 4-Chlorotoluene ND ug/kg 3.8 1.1 1 10/04/19 15:16 10/07/19 20:26 106-43-4 1,2-Dibromo-3-chloropropane ND ug/kg 3.8 1.9 1 10/04/19 15:16 10/07/19 20:26 96-12-8 Dibromochloromethane ND ug/kg 3.8 1.9 1 10/04/19 15:16 10/07/19 20:26 124-48-1 1,2-Dibromoethane (EDB) ND ug/kg 3.8 0.84 1 10/04/19 15:16 10/07/19 20:26 106-93-4 Dibromomethane ND ug/kg 3.8 1.1 1 10/04/19 15:16 10/07/19 20:26 74-95-3 1,2-Dichlorobenzene ND ug/kg 3.8 1.3 1 10/04/19 15:16 10/07/19 20:26 95-50-1 1,3-Dichlorobenzene ND ug/kg 3.8 1.3 1 10/04/19 15:16 10/07/19 20:26 541-73-1 1,4-Dichlorobenzene ND ug/kg 3.8 1.3 1 10/04/19 15:16 10/07/19 20:26 106-46-7 Dichlorodifluoromethane ND ug/kg 7.5 3.1 1 10/04/19 15:16 10/07/19 20:26 75-71-8 1,1-Dichloroethane ND ug/kg 3.8 0.55 1 10/04/19 15:16 10/07/19 20:26 75-34-3 1,2-Dichloroethane ND ug/kg 3.8 0.75 1 10/04/19 15:16 10/07/19 20:26 107-06-2 1,1-Dichloroethene ND ug/kg 3.8 0.87 1 10/04/19 15:16 10/07/19 20:26 75-35-4 cis-1,2-Dichloroethene ND ug/kg 3.8 0.65 1 10/04/19 15:16 10/07/19 20:26 156-59-2 trans-1,2-Dichloroethene ND ug/kg 3.8 0.74 1 10/04/19 15:16 10/07/19 20:26 156-60-5 1,2-Dichloropropane ND ug/kg 3.8 1.4 1 10/04/19 15:16 10/07/19 20:26 78-87-5 1,3-Dichloropropane ND ug/kg 3.8 1.4 1 10/04/19 15:16 10/07/19 20:26 142-28-9 2,2-Dichloropropane ND ug/kg 3.8 0.37 1 10/04/19 15:16 10/07/19 20:26 594-20-7 1,1-Dichloropropene ND ug/kg 3.8 1.6 1 10/04/19 15:16 10/07/19 20:26 563-58-6 cis-1,3-Dichloropropene ND ug/kg 3.8 1.7 1 10/04/19 15:16 10/07/19 20:26 10061-01-5 trans- 1,3-Dichloropropene ND ug/kg 3.8 0.66 1 10/04/19 15:16 10/07/19 20:26 10061-02-6 REPORT OF LABORATORY ANALYSIS v1 v1 v1 This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 44 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: UNCC MOOR HALL Pace Project No.: 92447655 Sample: BOTTOM Lab ID: 92447655003 Collected: 10/01/19 11:30 Received: 10/01/19 12:33 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual 8260D/5035A Volatile Organics Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone Isopropylbenzene (Cumene) p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIBK) Methyl-tert-butyl ether Naphthalene n-Propylbenzene Styrene 1,1,1,2-Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1,1,1-Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates Toluene-d8 (S) 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Percent Moisture Percent Moisture Analytical Method: EPA 8260D Preparation Method: EPA 5035A ND ug/kg 3.8 2.2 1 10/04/19 15:16 10/07/19 20:26 108-20-3 ND ug/kg 3.8 0.80 1 10/04/19 15:16 10/07/19 20:26 100-41-4 ND ug/kg 3.8 1.9 1 10/04/19 15:16 10/07/19 20:26 87-68-3 ND ug/kg 37.6 3.9 1 10/04/19 15:16 10/07/19 20:26 591-78-6 ND ug/kg 3.8 1.1 1 10/04/19 15:16 10/07/19 20:26 98-82-8 ND ug/kg 3.8 1.8 1 10/04/19 15:16 10/07/19 20:26 99-87-6 ND ug/kg 15.0 4.4 1 10/04/19 15:16 10/07/19 20:26 75-09-2 ND ug/kg 37.6 2.8 1 10/04/19 15:16 10/07/19 20:26 108-10-1 ND ug/kg 3.8 2.2 1 10/04/19 15:16 10/07/19 20:26 1634-04-4 ND ug/kg 3.8 3.2 1 10/04/19 15:16 10/07/19 20:26 91-20-3 ND ug/kg 3.8 1.3 1 10/04/19 15:16 10/07/19 20:26 103-65-1 ND ug/kg 3.8 1.1 1 10/04/19 15:16 10/07/19 20:26 100-42-5 ND ug/kg 3.8 0.92 1 10/04/19 15:16 10/07/19 20:26 630-20-6 ND ug/kg 3.8 1.3 1 10/04/19 15:16 10/07/19 20:26 79-34-5 ND ug/kg 3.8 1.2 1 10/04/19 15:16 10/07/19 20:26 127-18-4 ND ug/kg 3.8 1.2 1 10/04/19 15:16 10/07/19 20:26 108-88-3 ND ug/kg 3.8 2.7 1 10/04/19 15:16 10/07/19 20:26 87-61-6 ND ug/kg 3.8 2.0 1 10/04/19 15:16 10/07/19 20:26 120-82-1 ND ug/kg 3.8 0.65 1 10/04/19 15:16 10/07/19 20:26 71-55-6 ND ug/kg 3.8 0.85 1 10/04/19 15:16 10/07/19 20:26 79-00-5 ND ug/kg 3.8 0.98 1 10/04/19 15:16 10/07/19 20:26 79-01-6 ND ug/kg 3.8 0.89 1 10/04/19 15:16 10/07/19 20:26 75-69-4 ND ug/kg 3.8 1.3 1 10/04/19 15:16 10/07/19 20:26 96-18-4 ND ug/kg 3.8 1.5 1 10/04/19 15:16 10/07/19 20:26 95-63-6 ND ug/kg 3.8 1.3 1 10/04/19 15:16 10/07/19 20:26 108-67-8 ND ug/kg 37.6 12.3 1 10/04/19 15:16 10/07/19 20:26 108-05-4 IK ND ug/kg 7.5 1.4 1 10/04/19 15:16 10/07/19 20:26 75-01-4 ND ug/kg 7.5 2.6 1 10/04/19 15:16 10/07/19 20:26 1330-20-7 ND ug/kg 7.5 1.8 1 10/04/19 15:16 10/07/19 20:26 179601-23-1 ND ug/kg 3.8 0.88 1 10/04/19 15:16 10/07/19 20:26 95-47-6 105 % 70-130 1 10/04/19 15:16 10/07/19 20:26 2037-26-5 99 % 70-130 1 10/04/19 15:16 10/07/19 20:26 460-00-4 95 % 70-132 1 10/04/19 15:16 10/07/19 20:26 17060-07-0 Analytical Method: ASTM D2974-87 16.0 % 0.10 0.10 1 REPORT OF LABORATORY ANALYSIS 10/01/19 14:36 This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UNCC MOOR HALL Pace Project No.: 92447655 QC Batch: 501245 Analysis Method: MADEP VPH QC Batch Method: MADEP VPH Analysis Description: VPH NC Soil Associated Lab Samples: 92447655001, 92447655002, 92447655003 METHOD BLANK: 2695829 Matrix: Solid Associated Lab Samples: 92447655001, 92447655002, 92447655003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Aliphatic (C05-008) mg/kg ND 2.5 2.5 10/02/19 16:03 N2 Aliphatic (C09-C12) mg/kg ND 2.5 2.5 10/02/19 16:03 N2 Aromatic (C09-C10) mg/kg ND 2.5 2.5 10/02/19 16:03 N2 4-Bromofluorobenzene (FID) (S) % 89 70-130 10/02/19 16:03 4-Bromofluorobenzene (PID) (S) % 90 70-130 10/02/19 16:03 LABORATORY CONTROL SAMPLE & LCSD: 2695830 2695831 Spike LCS LCSD LCS LCSD % Rec Max Parameter Units Conc. Result Result % Rec % Rec Limits RPD RPD Qualifiers Aliphatic (C05-CO8) mg/kg 15.1 15.3 14.8 102 98 70-130 3 25 N2 Aliphatic (C09-C12) mg/kg 15.1 15.0 14.4 100 96 30-130 4 25 N2 Aromatic (C09-C10) mg/kg 5 5.0 4.8 99 95 70-130 5 25 N2 4-Bromofluorobenzene (FID) (S) % 99 90 70-130 4-Bromofluorobenzene (PID) (S) % 100 91 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 44 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UNCC MOOR HALL Pace Project No.: 92447655 QC Batch: 501807 Analysis Method: EPA 8260D QC Batch Method: EPA 5035A Analysis Description: 8260D MSV 5035A Volatile Organics Associated Lab Samples: 92447655001, 92447655003 METHOD BLANK: 2698410 Associated Lab Samples: 92447655001, 92447655003 Parameter Units Matrix: Blank Result Solid Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 1.2 10/07/19 12:47 1,1,1-Trichloroethane ug/kg ND 5.0 0.87 10/07/19 12:47 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 1.7 10/07/19 12:47 1,1,2-Trichloroethane ug/kg ND 5.0 1.1 10/07/19 12:47 1,1-Dichloroethane ug/kg ND 5.0 0.74 10/07/19 12:47 1,1-Dichloroethene ug/kg ND 5.0 1.2 10/07/19 12:47 1,1-Dichloropropene ug/kg ND 5.0 2.1 10/07/19 12:47 1,2,3-Trichlorobenzene ug/kg ND 5.0 3.6 10/07/19 12:47 1,2,3-Trichloropropane ug/kg ND 5.0 1.7 10/07/19 12:47 1,2,4-Trichlorobenzene ug/kg ND 5.0 2.6 10/07/19 12:47 1,2,4-Trimethylbenzene ug/kg ND 5.0 2.0 10/07/19 12:47 1,2-Dibromo-3-chloropropane ug/kg ND 5.0 2.5 10/07/19 12:47 1,2-Dibromoethane (EDB) ug/kg ND 5.0 1.1 10/07/19 12:47 1,2-Dichlorobenzene ug/kg ND 5.0 1.8 10/07/19 12:47 1,2-Dichloroethane ug/kg ND 5.0 1.0 10/07/19 12:47 1,2-Dichloropropane ug/kg ND 5.0 1.9 10/07/19 12:47 1,3,5-Trimethylbenzene ug/kg ND 5.0 1.7 10/07/19 12:47 1,3-Dichlorobenzene ug/kg ND 5.0 1.8 10/07/19 12:47 1,3-Dichloropropane ug/kg ND 5.0 1.9 10/07/19 12:47 1,4-Dichlorobenzene ug/kg ND 5.0 1.7 10/07/19 12:47 2,2-Dichloropropane ug/kg ND 5.0 0.49 10/07/19 12:47 2-Butanone (MEK) ug/kg ND 100 11.9 10/07/19 12:47 2-Chlorotoluene ug/kg ND 5.0 1.5 10/07/19 12:47 2-Hexanone ug/kg ND 50.0 5.2 10/07/19 12:47 4-Chlorotoluene ug/kg ND 5.0 1.5 10/07/19 12:47 4-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 3.7 10/07/19 12:47 Acetone ug/kg ND 100 9.4 10/07/19 12:47 Benzene ug/kg ND 5.0 0.90 10/07/19 12:47 Bromobenzene ug/kg ND 5.0 1.4 10/07/19 12:47 Bromochloromethane ug/kg ND 5.0 1.2 10/07/19 12:47 Bromodichloromethane ug/kg ND 5.0 0.98 10/07/19 12:47 Bromoform ug/kg ND 5.0 2.4 10/07/19 12:47 Bromomethane ug/kg ND 10.0 2.4 10/07/19 12:47 Carbon tetrachloride ug/kg ND 5.0 0.96 10/07/19 12:47 Chlorobenzene ug/kg ND 5.0 0.97 10/07/19 12:47 Chloroethane ug/kg ND 10.0 2.1 10/07/19 12:47 Chloroform ug/kg ND 5.0 1.1 10/07/19 12:47 Chloromethane ug/kg ND 10.0 3.3 10/07/19 12:47 cis-1,2-Dichloroethene ug/kg ND 5.0 0.87 10/07/19 12:47 cis-1,3-Dichloropropene ug/kg ND 5.0 2.3 10/07/19 12:47 Dibromochloromethane ug/kg ND 5.0 2.5 10/07/19 12:47 v1 v1 v1 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 44 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UNCC MOOR HALL Pace Project No.: 92447655 METHOD BLANK: 2698410 Associated Lab Samples: 92447655001, 92447655003 Parameter Units Matrix: Blank Result Solid Reporting Limit MDL Analyzed Dibromomethane ug/kg ND 5.0 1.5 10/07/19 12:47 Dichlorodifluoromethane ug/kg ND 10.0 4.1 10/07/19 12:47 Diisopropyl ether ug/kg ND 5.0 2.9 10/07/19 12:47 Ethylbenzene ug/kg ND 5.0 1.1 10/07/19 12:47 Hexachloro-1,3-butadiene ug/kg ND 5.0 2.5 10/07/19 12:47 Isopropylbenzene (Cumene) ug/kg ND 5.0 1.4 10/07/19 12:47 m&p-Xylene ug/kg ND 10.0 2.4 10/07/19 12:47 Methyl-tert-butyl ether ug/kg ND 5.0 2.9 10/07/19 12:47 Methylene Chloride ug/kg ND 20.0 5.9 10/07/19 12:47 n-Butylbenzene ug/kg ND 5.0 2.8 10/07/19 12:47 n-Propylbenzene ug/kg ND 5.0 1.7 10/07/19 12:47 Naphthalene ug/kg ND 5.0 4.2 10/07/19 12:47 o-Xylene ug/kg ND 5.0 1.2 10/07/19 12:47 p-Isopropyltoluene ug/kg ND 5.0 2.4 10/07/19 12:47 sec-Butylbenzene ug/kg ND 5.0 2.1 10/07/19 12:47 Styrene ug/kg ND 5.0 1.5 10/07/19 12:47 tert-Butyl benzene ug/kg ND 5.0 1.7 10/07/19 12:47 Tetrachloroethene ug/kg ND 5.0 1.6 10/07/19 12:47 Toluene ug/kg ND 5.0 1.6 10/07/19 12:47 trans-1,2-Dichloroethene ug/kg ND 5.0 0.98 10/07/19 12:47 trans- 1,3-Dichloropropene ug/kg ND 5.0 0.88 10/07/19 12:47 Trichloroethene ug/kg ND 5.0 1.3 10/07/19 12:47 Trichlorofluoromethane ug/kg ND 5.0 1.2 10/07/19 12:47 Vinyl acetate ug/kg ND 50.0 16.3 10/07/19 12:47 Vinyl chloride ug/kg ND 10.0 1.9 10/07/19 12:47 Xylene (Total) ug/kg ND 10.0 3.5 10/07/19 12:47 1,2-Dichloroethane-d4 (S) % 105 70-132 10/07/19 12:47 4-Bromofluorobenzene (S) % 102 70-130 10/07/19 12:47 Toluene-d8 (S) % 105 70-130 10/07/19 12:47 IK Qualifiers LABORATORY CONTROL SAMPLE: 2698411 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/kg 50 53.1 106 70-130 1,1,1-Trichloroethane ug/kg 50 49.6 99 70-130 1,1,2,2-Tetrachloroethane ug/kg 50 55.6 111 55-130 1,1,2-Trichloroethane ug/kg 50 50.8 102 70-130 1,1-Dichloroethane ug/kg 50 50.3 101 68-130 1,1-Dichloroethene ug/kg 50 51.2 102 70-130 1,1-Dichloropropene ug/kg 50 51.7 103 70-130 1,2,3-Trichlorobenzene ug/kg 50 53.5 107 70-130 1,2,3-Trichloropropane ug/kg 50 57.5 115 70-130 1,2,4-Trichlorobenzene ug/kg 50 51.5 103 70-130 1,2,4-Trimethylbenzene ug/kg 50 53.7 107 69-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 44 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UNCC MOOR HALL Pace Project No.: 92447655 LABORATORY CONTROL SAMPLE: Parameter 2698411 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,2-Dibromo-3-chloropropane ug/kg 50 68.6 137 57-141 v1 1,2-Dibromoethane (EDB) ug/kg 50 53.6 107 70-130 1,2-Dichlorobenzene ug/kg 50 50.9 102 70-130 1,2-Dichloroethane ug/kg 50 48.8 98 70-130 1,2-Dichloropropane ug/kg 50 50.1 100 70-130 1,3,5-Trimethylbenzene ug/kg 50 51.6 103 70-130 1,3-Dichlorobenzene ug/kg 50 50.8 102 70-130 1,3-Dichloropropane ug/kg 50 56.1 112 70-130 1,4-Dichlorobenzene ug/kg 50 49.9 100 70-130 2,2-Dichloropropane ug/kg 50 50.5 101 70-130 2-Butanone (MEK) ug/kg 100 107 107 60-130 2-Chlorotoluene ug/kg 50 50.7 101 70-130 2-Hexanone ug/kg 100 118 118 70-132 4-Chlorotoluene ug/kg 50 51.4 103 70-130 4-Methyl-2-pentanone (MIBK) ug/kg 100 108 108 69-130 Acetone ug/kg 100 112 112 49-148 Benzene ug/kg 50 50.2 100 70-130 Bromobenzene ug/kg 50 52.3 105 70-130 Bromochloromethane ug/kg 50 48.6 97 70-130 Bromodichloromethane ug/kg 50 52.4 105 70-130 Bromoform ug/kg 50 61.5 123 68-136 v1 Bromomethane ug/kg 50 56.3 113 60-140 Carbon tetrachloride ug/kg 50 48.9 98 70-130 Chlorobenzene ug/kg 50 50.1 100 70-130 Chloroethane ug/kg 50 65.2 130 51-147 v1 Chloroform ug/kg 50 49.3 99 70-130 Chloromethane ug/kg 50 53.2 106 48-130 cis-1,2-Dichloroethene ug/kg 50 48.8 98 70-130 cis-1,3-Dichloropropene ug/kg 50 53.4 107 70-130 Dibromochloromethane ug/kg 50 57.2 114 70-130 Dibromomethane ug/kg 50 49.2 98 70-130 Dichlorodifluoromethane ug/kg 50 55.9 112 49-130 Diisopropyl ether ug/kg 50 49.9 100 66-130 Ethylbenzene ug/kg 50 51.2 102 70-130 Hexachloro-1,3-butadiene ug/kg 50 53.5 107 70-130 Isopropylbenzene (Cumene) ug/kg 50 51.3 103 70-130 m&p-Xylene ug/kg 100 102 102 70-130 Methyl-tert-butyl ether ug/kg 50 51.7 103 70-130 Methylene Chloride ug/kg 50 44.7 89 50-137 n-Butylbenzene ug/kg 50 52.4 105 70-130 n-Propylbenzene ug/kg 50 53.1 106 70-130 Naphthalene ug/kg 50 55.6 111 70-131 o-Xylene ug/kg 50 50.9 102 70-130 p-Isopropyltoluene ug/kg 50 52.8 106 70-130 sec-Butylbenzene ug/kg 50 54.0 108 70-130 Styrene ug/kg 50 51.1 102 70-130 tert-Butyl benzene ug/kg 50 46.4 93 69-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 44 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UNCC MOOR HALL Pace Project No.: 92447655 LABORATORY CONTROL SAMPLE: Parameter 2698411 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Tetrachloroethene ug/kg 50 48.4 97 56-130 Toluene ug/kg 50 45.6 91 70-130 trans-1,2-Dichloroethene ug/kg 50 47.8 96 70-130 trans- 1,3-Dichloropropene ug/kg 50 52.5 105 70-130 Trichloroethene ug/kg 50 49.5 99 70-141 Trichlorofluoromethane ug/kg 50 59.4 119 67-130 Vinyl acetate ug/kg 100 94.8 95 10-136 IK Vinyl chloride ug/kg 50 53.9 108 67-130 Xylene (Total) ug/kg 150 153 102 70-130 1,2-Dichloroethane-d4 (S) % 115 70-132 4-Bromofluorobenzene (S) % 96 70-130 Toluene-d8 (S) % 96 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2698412 MS 92447247035 Spike Parameter Units Result Conc. MSD Spike Conc. 2698413 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 1,1,1,2-Tetrachloroethane ug/kg ND 23.7 23.7 24.6 24.2 104 102 52-133 2 30 1,1,1-Trichloroethane ug/kg ND 23.7 23.7 26.7 24.1 113 102 49-137 10 30 1,1,2,2-Tetrachloroethane ug/kg ND 23.7 23.7 24.9 24.1 105 102 39-150 3 30 1,1,2-Trichloroethane ug/kg ND 23.7 23.7 23.6 22.9 100 97 48-140 3 30 1,1-Dichloroethane ug/kg ND 23.7 23.7 27.4 24.8 116 105 46-135 10 30 1,1-Dichloroethene ug/kg ND 23.7 23.7 27.2 26.8 115 113 38-149 1 30 1,1-Dichloropropene ug/kg ND 23.7 23.7 26.1 23.4 110 99 41-140 11 30 1,2,3-Trichlorobenzene ug/kg ND 23.7 23.7 23.0 22.4 97 95 10-158 3 30 1,2,3-Trichloropropane ug/kg ND 23.7 23.7 27.1 25.9 114 109 33-157 5 30 1,2,4-Trichlorobenzene ug/kg ND 23.7 23.7 23.4 23.1 99 98 10-155 1 30 1,2,4-Trimethyl benzene ug/kg ND 23.7 23.7 27.9 26.4 118 111 24-154 6 30 1,2-Dibromo-3- ug/kg ND 23.7 23.7 25.3 24.0 107 101 33-158 5 30 v1 chloropropane 1,2-Dibromoethane (EDB) ug/kg ND 23.7 23.7 24.4 24.2 103 102 40-136 1 30 1,2-Dichlorobenzene ug/kg ND 23.7 23.7 25.7 25.5 109 108 27-146 1 30 1,2-Dichloroethane ug/kg ND 23.7 23.7 24.7 22.4 104 95 49-140 10 30 1,2-Dichloropropane ug/kg ND 23.7 23.7 24.9 23.2 105 98 44-143 7 30 1,3,5-Trimethyl benzene ug/kg ND 23.7 23.7 27.7 27.0 117 114 40-144 3 30 1,3-Dichlorobenzene ug/kg ND 23.7 23.7 26.7 26.1 113 110 33-140 2 30 1,3-Dichloropropane ug/kg ND 23.7 23.7 26.5 24.7 112 104 47-147 7 30 1,4-Dichlorobenzene ug/kg ND 23.7 23.7 27.1 26.3 115 111 35-139 3 30 2,2-Dichloropropane ug/kg ND 23.7 23.7 26.7 25.4 113 108 41-140 5 30 2-Butanone (MEK) ug/kg ND 47.3 47.3 46.3J 40.2J 98 85 10-181 30 2-Chlorotoluene ug/kg ND 23.7 23.7 28.6 27.0 121 114 38-147 6 30 2-Hexanone ug/kg ND 47.3 47.3 47.2J 45.8J 100 97 18-169 30 4-Chlorotoluene ug/kg ND 23.7 23.7 28.2 27.2 119 115 36-145 4 30 4-Methyl-2-pentanone ug/kg ND 47.3 47.3 44.2J 45.2J 93 96 16-175 30 (MIBK) Acetone ug/kg ND 47.3 47.3 51.2J 48.OJ 108 101 10-200 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result Date: 10/08/2019 05:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 26 of 44 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UNCC MOOR HALL Pace Project No.: 92447655 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2698412 MS 92447247035 Spike Parameter Units Result Conc. MSD Spike Conc. 2698413 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual Benzene ug/kg ND 23.7 23.7 26.0 24.7 110 104 46-136 5 30 Bromobenzene ug/kg ND 23.7 23.7 27.8 26.8 117 113 38-149 3 30 Bromochloromethane ug/kg ND 23.7 23.7 25.4 24.2 107 102 44-142 5 30 Bromodichloromethane ug/kg ND 23.7 23.7 24.4 24.0 103 101 41-140 2 30 Bromoform ug/kg ND 23.7 23.7 23.9 23.1 101 97 34-145 3 30 v1 Bromomethane ug/kg ND 23.7 23.7 30.7 28.6 130 121 14-162 7 30 Carbon tetrachloride ug/kg ND 23.7 23.7 25.2 24.7 106 104 44-141 2 30 Chlorobenzene ug/kg ND 23.7 23.7 26.1 25.1 110 106 39-141 4 30 Chloroethane ug/kg ND 23.7 23.7 35.6 33.6 150 142 10-182 6 30 v1 Chloroform ug/kg ND 23.7 23.7 24.9 22.9 105 97 45-140 8 30 Chloromethane ug/kg ND 23.7 23.7 29.8 27.9 126 118 19-149 7 30 v1 cis-1,2-Dichloroethene ug/kg ND 23.7 23.7 26.2 24.5 111 104 38-150 7 30 cis-1,3-Dichloropropene ug/kg ND 23.7 23.7 24.7 23.5 104 99 30-144 5 30 Dibromochloromethane ug/kg ND 23.7 23.7 25.0 22.5 106 95 36-145 10 30 Dibromomethane ug/kg ND 23.7 23.7 24.1 23.2 102 98 41-145 4 30 Dichlorodifluoromethane ug/kg ND 23.7 23.7 32.4 29.8 137 126 16-146 9 30 Diisopropyl ether ug/kg ND 23.7 23.7 23.8 23.6 101 100 41-143 1 30 Ethylbenzene ug/kg ND 23.7 23.7 29.1 26.2 123 111 35-144 10 30 Hexachloro-1,3-butadiene ug/kg ND 23.7 23.7 24.8 25.0 105 106 10-160 1 30 Isopropylbenzene ug/kg ND 23.7 23.7 29.7 26.6 125 113 30-152 11 30 (Cumene) m&p-Xylene ug/kg ND 47.3 47.3 60.3 53.4 127 113 33-145 12 30 Methyl-tert-butyl ether ug/kg ND 23.7 23.7 22.7 21.7 96 92 49-140 4 30 Methylene Chloride ug/kg ND 23.7 23.7 25.6 23.3J 108 98 10-174 30 n-Butylbenzene ug/kg ND 23.7 23.7 27.8 27.7 118 117 10-160 1 30 n-Propylbenzene ug/kg ND 23.7 23.7 30.5 28.8 129 122 24-159 6 30 Naphthalene ug/kg ND 23.7 23.7 23.5 22.8 99 96 10-171 3 30 o-Xylene ug/kg ND 23.7 23.7 28.3 26.5 120 112 31-150 7 30 p-Isopropyltoluene ug/kg ND 23.7 23.7 28.7 27.6 121 117 21-154 4 30 sec-Butylbenzene ug/kg ND 23.7 23.7 29.8 28.9 126 122 19-159 3 30 Styrene ug/kg ND 23.7 23.7 27.6 25.2 117 106 15-152 9 30 tert-Butylbenzene ug/kg ND 23.7 23.7 26.1 25.4 110 107 31-141 3 30 Tetrachloroethene ug/kg ND 23.7 23.7 25.8 24.5 109 104 19-141 5 30 Toluene ug/kg ND 23.7 23.7 24.4 24.5 103 104 31-146 1 30 trans-1,2-Dichloroethene ug/kg ND 23.7 23.7 28.2 24.8 119 105 28-157 13 30 trans-1,3-Dichloropropene ug/kg ND 23.7 23.7 23.5 22.6 99 96 25-146 4 30 Trichloroethene ug/kg ND 23.7 23.7 24.9 23.8 105 101 34-149 5 30 Trichlorofluoromethane ug/kg ND 23.7 23.7 33.5 30.8 142 130 10-167 8 30 Vinyl acetate ug/kg ND 47.3 47.3 35.6J 33.7J 75 71 10-200 30 IK Vinyl chloride ug/kg ND 23.7 23.7 30.2 28.4 127 120 36-155 6 30 Xylene (Total) ug/kg ND 71 71 88.6 80.0 125 113 29-148 10 30 1,2-Dichloroethane-d4 (S) % 108 103 70-132 4-Bromofluorobenzene (S) % 103 96 70-130 Toluene-d8 (S) % 97 103 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 44 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UNCC MOOR HALL Pace Project No.: 92447655 QC Batch: 502304 Analysis Method: EPA 8260D QC Batch Method: EPA 5035A Analysis Description: 8260D MSV 5035A Volatile Organics Associated Lab Samples: 92447655002 METHOD BLANK: 2700586 Associated Lab Samples: 92447655002 Parameter Units Matrix: Blank Result Solid Reporting Limit MDL Analyzed 1,1,1,2-Tetrachloroethane ug/kg ND 5.0 1.2 10/08/19 13:04 1,1,1-Trichloroethane ug/kg ND 5.0 0.87 10/08/19 13:04 1,1,2,2-Tetrachloroethane ug/kg ND 5.0 1.7 10/08/19 13:04 1,1,2-Trichloroethane ug/kg ND 5.0 1.1 10/08/19 13:04 1,1-Dichloroethane ug/kg ND 5.0 0.74 10/08/19 13:04 1,1-Dichloroethene ug/kg ND 5.0 1.2 10/08/19 13:04 1,1-Dichloropropene ug/kg ND 5.0 2.1 10/08/19 13:04 1,2,3-Trichlorobenzene ug/kg ND 5.0 3.6 10/08/19 13:04 1,2,3-Trichloropropane ug/kg ND 5.0 1.7 10/08/19 13:04 1,2,4-Trichlorobenzene ug/kg ND 5.0 2.6 10/08/19 13:04 1,2,4-Trimethylbenzene ug/kg 3.1J 5.0 2.0 10/08/19 13:04 1,2-Dibromo-3-chloropropane ug/kg ND 5.0 2.5 10/08/19 13:04 1,2-Dibromoethane (EDB) ug/kg ND 5.0 1.1 10/08/19 13:04 1,2-Dichlorobenzene ug/kg ND 5.0 1.8 10/08/19 13:04 1,2-Dichloroethane ug/kg ND 5.0 1.0 10/08/19 13:04 1,2-Dichloropropane ug/kg ND 5.0 1.9 10/08/19 13:04 1,3,5-Trimethylbenzene ug/kg ND 5.0 1.7 10/08/19 13:04 1,3-Dichlorobenzene ug/kg ND 5.0 1.8 10/08/19 13:04 1,3-Dichloropropane ug/kg ND 5.0 1.9 10/08/19 13:04 1,4-Dichlorobenzene ug/kg ND 5.0 1.7 10/08/19 13:04 2,2-Dichloropropane ug/kg ND 5.0 0.49 10/08/19 13:04 2-Butanone (MEK) ug/kg ND 100 11.9 10/08/19 13:04 2-Chlorotoluene ug/kg ND 5.0 1.5 10/08/19 13:04 2-Hexanone ug/kg ND 50.0 5.2 10/08/19 13:04 4-Chlorotoluene ug/kg ND 5.0 1.5 10/08/19 13:04 4-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 3.7 10/08/19 13:04 Acetone ug/kg ND 100 9.4 10/08/19 13:04 Benzene ug/kg ND 5.0 0.90 10/08/19 13:04 Bromobenzene ug/kg ND 5.0 1.4 10/08/19 13:04 Bromochloromethane ug/kg ND 5.0 1.2 10/08/19 13:04 Bromodichloromethane ug/kg ND 5.0 0.98 10/08/19 13:04 Bromoform ug/kg ND 5.0 2.4 10/08/19 13:04 Bromomethane ug/kg ND 10.0 2.4 10/08/19 13:04 Carbon tetrachloride ug/kg ND 5.0 0.96 10/08/19 13:04 Chlorobenzene ug/kg ND 5.0 0.97 10/08/19 13:04 Chloroethane ug/kg ND 10.0 2.1 10/08/19 13:04 Chloroform ug/kg ND 5.0 1.1 10/08/19 13:04 Chloromethane ug/kg ND 10.0 3.3 10/08/19 13:04 cis-1,2-Dichloroethene ug/kg ND 5.0 0.87 10/08/19 13:04 cis-1,3-Dichloropropene ug/kg ND 5.0 2.3 10/08/19 13:04 Dibromochloromethane ug/kg ND 5.0 2.5 10/08/19 13:04 v1 v1 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 44 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UNCC MOOR HALL Pace Project No.: 92447655 METHOD BLANK: 2700586 Associated Lab Samples: 92447655002 Parameter Units Matrix: Blank Result Solid Reporting Limit MDL Analyzed Dibromomethane ug/kg ND 5.0 1.5 10/08/19 13:04 Dichlorodifluoromethane ug/kg ND 10.0 4.1 10/08/19 13:04 Diisopropyl ether ug/kg ND 5.0 2.9 10/08/19 13:04 Ethylbenzene ug/kg ND 5.0 1.1 10/08/19 13:04 Hexachloro-1,3-butadiene ug/kg ND 5.0 2.5 10/08/19 13:04 Isopropylbenzene (Cumene) ug/kg ND 5.0 1.4 10/08/19 13:04 m&p-Xylene ug/kg ND 10.0 2.4 10/08/19 13:04 Methyl-tert-butyl ether ug/kg ND 5.0 2.9 10/08/19 13:04 Methylene Chloride ug/kg ND 20.0 5.9 10/08/19 13:04 n-Butylbenzene ug/kg ND 5.0 2.8 10/08/19 13:04 n-Propylbenzene ug/kg ND 5.0 1.7 10/08/19 13:04 Naphthalene ug/kg ND 5.0 4.2 10/08/19 13:04 o-Xylene ug/kg ND 5.0 1.2 10/08/19 13:04 p-Isopropyltoluene ug/kg ND 5.0 2.4 10/08/19 13:04 sec-Butylbenzene ug/kg ND 5.0 2.1 10/08/19 13:04 Styrene ug/kg ND 5.0 1.5 10/08/19 13:04 tert-Butyl benzene ug/kg ND 5.0 1.7 10/08/19 13:04 Tetrachloroethene ug/kg ND 5.0 1.6 10/08/19 13:04 Toluene ug/kg ND 5.0 1.6 10/08/19 13:04 trans-1,2-Dichloroethene ug/kg ND 5.0 0.98 10/08/19 13:04 trans- 1,3-Dichloropropene ug/kg ND 5.0 0.88 10/08/19 13:04 Trichloroethene ug/kg ND 5.0 1.3 10/08/19 13:04 Trichlorofluoromethane ug/kg ND 5.0 1.2 10/08/19 13:04 Vinyl acetate ug/kg ND 50.0 16.3 10/08/19 13:04 Vinyl chloride ug/kg ND 10.0 1.9 10/08/19 13:04 Xylene (Total) ug/kg ND 10.0 3.5 10/08/19 13:04 1,2-Dichloroethane-d4 (S) % 95 70-132 10/08/19 13:04 4-Bromofluorobenzene (S) % 103 70-130 10/08/19 13:04 Toluene-d8 (S) % 106 70-130 10/08/19 13:04 IK Qualifiers LABORATORY CONTROL SAMPLE: Parameter 2700587 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/kg 50 52.8 106 70-130 1,1,1-Trichloroethane ug/kg 50 47.9 96 70-130 1,1,2,2-Tetrachloroethane ug/kg 50 54.7 109 55-130 1,1,2-Trichloroethane ug/kg 50 52.1 104 70-130 1,1-Dichloroethane ug/kg 50 49.9 100 68-130 1,1-Dichloroethene ug/kg 50 51.4 103 70-130 1,1-Dichloropropene ug/kg 50 51.7 103 70-130 1,2,3-Trichlorobenzene ug/kg 50 55.9 112 70-130 1,2,3-Trichloropropane ug/kg 50 57.8 116 70-130 1,2,4-Trichlorobenzene ug/kg 50 53.2 106 70-130 1,2,4-Trimethylbenzene ug/kg 50 58.2 116 69-130 v1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 44 aceAnalytical -pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UNCC MOOR HALL Pace Project No.: 92447655 LABORATORY CONTROL SAMPLE: Parameter 2700587 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 1,2-Dibromo-3-chloropropane ug/kg 50 64.5 129 57-141 1,2-Dibromoethane (EDB) ug/kg 50 55.8 112 70-130 1,2-Dichlorobenzene ug/kg 50 53.1 106 70-130 1,2-Dichloroethane ug/kg 50 47.1 94 70-130 1,2-Dichloropropane ug/kg 50 51.6 103 70-130 1,3,5-Trimethylbenzene ug/kg 50 54.1 108 70-130 1,3-Dichlorobenzene ug/kg 50 52.3 105 70-130 1,3-Dichloropropane ug/kg 50 58.0 116 70-130 1,4-Dichlorobenzene ug/kg 50 52.6 105 70-130 2,2-Dichloropropane ug/kg 50 48.7 97 70-130 2-Butanone (MEK) ug/kg 100 115 115 60-130 2-Chlorotoluene ug/kg 50 51.7 103 70-130 2-Hexanone ug/kg 100 121 121 70-132 4-Chlorotoluene ug/kg 50 52.9 106 70-130 4-Methyl-2-pentanone (MIBK) ug/kg 100 110 110 69-130 Acetone ug/kg 100 115 115 49-148 Benzene ug/kg 50 51.4 103 70-130 Bromobenzene ug/kg 50 53.6 107 70-130 Bromochloromethane ug/kg 50 50.7 101 70-130 Bromodichloromethane ug/kg 50 49.8 100 70-130 Bromoform ug/kg 50 54.4 109 68-136 Bromomethane ug/kg 50 50.7 101 60-140 Carbon tetrachloride ug/kg 50 46.1 92 70-130 Chlorobenzene ug/kg 50 50.5 101 70-130 Chloroethane ug/kg 50 58.8 118 51-147 v1 Chloroform ug/kg 50 47.7 95 70-130 Chloromethane ug/kg 50 51.7 103 48-130 cis-1,2-Dichloroethene ug/kg 50 48.6 97 70-130 cis-1,3-Dichloropropene ug/kg 50 53.9 108 70-130 Dibromochloromethane ug/kg 50 54.5 109 70-130 Dibromomethane ug/kg 50 50.2 100 70-130 Dichlorodifluoromethane ug/kg 50 49.7 99 49-130 Diisopropyl ether ug/kg 50 52.8 106 66-130 Ethylbenzene ug/kg 50 52.3 105 70-130 Hexachloro-1,3-butadiene ug/kg 50 54.2 108 70-130 Isopropylbenzene (Cumene) ug/kg 50 52.9 106 70-130 m&p-Xylene ug/kg 100 106 106 70-130 Methyl-tert-butyl ether ug/kg 50 53.8 108 70-130 Methylene Chloride ug/kg 50 44.4 89 50-137 n-Butylbenzene ug/kg 50 55.5 111 70-130 n-Propylbenzene ug/kg 50 55.2 110 70-130 Naphthalene ug/kg 50 60.9 122 70-131 o-Xylene ug/kg 50 53.2 106 70-130 p-Isopropyltoluene ug/kg 50 55.3 111 70-130 sec-Butylbenzene ug/kg 50 56.1 112 70-130 Styrene ug/kg 50 52.6 105 70-130 tert-Butyl benzene ug/kg 50 48.3 97 69-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UNCC MOOR HALL Pace Project No.: 92447655 LABORATORY CONTROL SAMPLE: Parameter 2700587 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Tetrachloroethene ug/kg 50 50.1 100 56-130 Toluene ug/kg 50 46.8 94 70-130 trans-1,2-Dichloroethene ug/kg 50 49.0 98 70-130 trans- 1,3-Dichloropropene ug/kg 50 52.2 104 70-130 Trichloroethene ug/kg 50 51.7 103 70-141 Trichlorofluoromethane ug/kg 50 52.1 104 67-130 Vinyl acetate ug/kg 100 91.4 91 10-136 IK Vinyl chloride ug/kg 50 52.6 105 67-130 Xylene (Total) ug/kg 150 160 106 70-130 1,2-Dichloroethane-d4 (S) % 107 70-132 4-Bromofluorobenzene (S) % 98 70-130 Toluene-d8 (S) % 95 70-130 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2700588 MS 92447960002 Spike Parameter Units Result Conc. MSD Spike Conc. 2700589 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual 1,1,1,2-Tetrachloroethane ug/kg ND 811 811 748 757 92 93 52-133 1 30 1,1,1-Trichloroethane ug/kg ND 811 811 830 829 102 102 49-137 0 30 1,1,2,2-Tetrachloroethane ug/kg ND 811 811 872 898 108 111 39-150 3 30 1,1,2-Trichloroethane ug/kg ND 811 811 846 867 104 107 48-140 2 30 1,1-Dichloroethane ug/kg ND 811 811 854 886 105 109 46-135 4 30 1,1-Dichloroethene ug/kg ND 811 811 418 453 52 56 38-149 8 30 1,1-Dichloropropene ug/kg ND 811 811 831 836 102 103 41-140 1 30 1,2,3-Trichlorobenzene ug/kg ND 811 811 875 904 108 112 10-158 3 30 1,2,3-Trichooropropane ug/kg ND 811 811 896 909 110 112 33-157 1 30 1,2,4-Trichlorobenzene ug/kg ND 811 811 918 911 113 112 10-155 1 30 1,2,4-Trimethyl benzene ug/kg ND 811 811 930 929 106 106 24-154 0 30 v1 1,2-Dibromo-3- ug/kg ND 811 811 806 824 99 102 33-158 2 30 chloropropane 1,2-Dibromoethane (EDB) ug/kg ND 811 811 822 867 101 107 40-136 5 30 1,2-Dichlorobenzene ug/kg ND 811 811 873 892 108 110 27-146 2 30 1,2-Dichloroethane ug/kg ND 811 811 838 864 103 107 49-140 3 30 1,2-Dichloropropane ug/kg ND 811 811 853 895 105 110 44-143 5 30 1,3,5-Trimethyl benzene ug/kg ND 811 811 841 867 104 107 40-144 3 30 1,3-Dichlorobenzene ug/kg ND 811 811 844 861 104 106 33-140 2 30 1,3-Dichloropropane ug/kg ND 811 811 908 907 112 112 47-147 0 30 1,4-Dichlorobenzene ug/kg ND 811 811 844 891 104 110 35-139 5 30 2,2-Dichloropropane ug/kg ND 811 811 838 856 103 106 41-140 2 30 2-Butanone (MEK) ug/kg ND 1620 1620 1740J 1790J 107 111 10-181 30 2-Chlorotoluene ug/kg ND 811 811 834 878 103 108 38-147 5 30 2-Hexanone ug/kg ND 1620 1620 1470J 1520J 91 93 18-169 30 4-Chlorotoluene ug/kg ND 811 811 852 885 105 109 36-145 4 30 4-Methyl-2-pentanone ug/kg ND 1620 1620 1700J 1690J 105 104 16-175 30 (MIBK) Acetone ug/kg ND 1620 1620 11901 1420J 73 88 10-200 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result Date: 10/08/2019 05:11 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 31 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UNCC MOOR HALL Pace Project No.: 92447655 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2700588 MS 92447960002 Spike Parameter Units Result Conc. MSD Spike Conc. 2700589 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Max RPD Qual Benzene ug/kg ND 811 811 869 900 107 111 46-136 3 30 Bromobenzene ug/kg ND 811 811 851 899 105 111 38-149 5 30 Bromochloromethane ug/kg ND 811 811 869 881 107 109 44-142 1 30 Bromodichloromethane ug/kg ND 811 811 768 787 95 97 41-140 2 30 Bromoform ug/kg ND 811 811 672 667 83 82 34-145 1 30 Bromomethane ug/kg ND 811 811 842 870 104 107 14-162 3 30 Carbon tetrachloride ug/kg ND 811 811 715 732 88 90 44-141 2 30 Chlorobenzene ug/kg ND 811 811 814 854 100 105 39-141 5 30 Chloroethane ug/kg ND 811 811 523 554 64 68 10-182 6 30 v1 Chloroform ug/kg ND 811 811 842 867 104 107 45-140 3 30 Chloromethane ug/kg ND 811 811 952 934 117 115 19-149 2 30 cis-1,2-Dichloroethene ug/kg ND 811 811 885 879 109 108 38-150 1 30 cis-1,3-Dichloropropene ug/kg ND 811 811 840 857 104 106 30-144 2 30 Dibromochloromethane ug/kg ND 811 811 720 721 89 89 36-145 0 30 Dibromomethane ug/kg ND 811 811 820 842 101 104 41-145 3 30 Dichlorodifluoromethane ug/kg ND 811 811 863 896 106 110 16-146 4 30 Diisopropyl ether ug/kg ND 811 811 789 811 97 100 41-143 3 30 Ethylbenzene ug/kg ND 811 811 861 886 106 109 35-144 3 30 Hexachloro-1,3-butadiene ug/kg ND 811 811 840 897 104 111 10-160 7 30 Isopropylbenzene ug/kg ND 811 811 850 889 105 110 30-152 4 30 (Cumene) m&p-Xylene ug/kg ND 1620 1620 1770 1830 104 109 33-145 4 30 Methyl-tert-butyl ether ug/kg ND 811 811 852 786 105 97 49-140 8 30 Methylene Chloride ug/kg ND 811 811 847 856 105 106 10-174 1 30 n-Butylbenzene ug/kg ND 811 811 880 911 109 112 10-160 3 30 n-Propylbenzene ug/kg ND 811 811 868 903 107 111 24-159 4 30 Naphthalene ug/kg ND 811 811 948 990 107 112 10-171 4 30 o-Xylene ug/kg 48.5J 811 811 895 927 104 108 31-150 3 30 p-Isopropyltoluene ug/kg ND 811 811 876 916 108 113 21-154 5 30 sec-Butylbenzene ug/kg ND 811 811 889 929 110 115 19-159 4 30 Styrene ug/kg ND 811 811 855 874 105 108 15-152 2 30 tert-Butylbenzene ug/kg ND 811 811 760 793 94 98 31-141 4 30 Tetrachloroethene ug/kg ND 811 811 778 792 96 98 19-141 2 30 Toluene ug/kg ND 811 811 804 849 93 98 31-146 5 30 trans-1,2-Dichloroethene ug/kg ND 811 811 830 912 102 112 28-157 9 30 trans-1,3-Dichloropropene ug/kg ND 811 811 803 813 99 100 25-146 1 30 Trichloroethene ug/kg 1700 811 811 2820 2620 138 113 34-149 7 30 Trichlorofluoromethane ug/kg ND 811 811 392 391 48 48 10-167 0 30 Vinyl acetate ug/kg ND 1620 1620 19001 1890J 117 116 10-200 30 IK Vinyl chloride ug/kg ND 811 811 898 932 111 115 36-155 4 30 Xylene (Total) ug/kg ND 2430 2430 2660 2760 109 113 29-148 4 30 1,2-Dichloroethane-d4 (S) % 115 113 70-132 4-Bromofluorobenzene (S) % 99 100 70-130 Toluene-d8 (S) % 100 99 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UNCC MOOR HALL Pace Project No.: 92447655 QC Batch: 501380 Analysis Method: EPA 8270E QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave Associated Lab Samples: 92447655001, 92447655002, 92447655003 METHOD BLANK: 2696483 Matrix: Solid Associated Lab Samples: 92447655001, 92447655002, 92447655003 Blank Reporting Parameter Units Result Limit MDL Analyzed 1,2,4-Trichlorobenzene ug/kg ND 330 75.6 10/07/19 13:27 1,2-Dichlorobenzene ug/kg ND 330 71.4 10/07/19 13:27 1,3-Dichlorobenzene ug/kg ND 330 74.3 10/07/19 13:27 1,4-Dichlorobenzene ug/kg ND 330 72.6 10/07/19 13:27 1-Methylnaphthalene ug/kg ND 330 87.9 10/07/19 13:27 2,2'-Oxybis(1-chloropropane) ug/kg ND 330 91.7 10/07/19 13:27 2,4,5-Trichlorophenol ug/kg ND 330 85.7 10/07/19 13:27 2,4,6-Trichlorophenol ug/kg ND 330 82.9 10/07/19 13:27 2,4-Dichlorophenol ug/kg ND 330 109 10/07/19 13:27 2,4-Dimethylphenol ug/kg ND 330 82.2 10/07/19 13:27 2,4-Dinitrophenol ug/kg ND 1650 1050 10/07/19 13:27 2,4-Dinitrotoluene ug/kg ND 330 87.4 10/07/19 13:27 2,6-Dinitrotoluene ug/kg ND 330 86.3 10/07/19 13:27 2-Chloronaphthalene ug/kg ND 330 73.5 10/07/19 13:27 2-Chlorophenol ug/kg ND 330 76.8 10/07/19 13:27 2-Methylnaphthalene ug/kg ND 330 84.0 10/07/19 13:27 2-Methylphenol(o-Cresol) ug/kg ND 330 73.1 10/07/19 13:27 2-Nitroaniline ug/kg ND 1650 166 10/07/19 13:27 2-Nitrophenol ug/kg ND 330 102 10/07/19 13:27 3&4-Methyl phenol (m&p Cresol) ug/kg ND 330 83.0 10/07/19 13:27 3,3'-Dichlorobenzidine ug/kg ND 1650 230 10/07/19 13:27 3-Nitroaniline ug/kg ND 1650 175 10/07/19 13:27 4,6-Dinitro-2-methyl phenol ug/kg ND 660 532 10/07/19 13:27 4-Bromophenylphenyl ether ug/kg ND 330 86.6 10/07/19 13:27 4-ChIoro-3-methyl phenol ug/kg ND 660 201 10/07/19 13:27 4-Chloroaniline ug/kg ND 1650 202 10/07/19 13:27 4-Chlorophenylphenyl ether ug/kg ND 330 85.7 10/07/19 13:27 4-Nitroaniline ug/kg ND 660 163 10/07/19 13:27 4-Nitrophenol ug/kg ND 1650 526 10/07/19 13:27 Acenaphthene ug/kg ND 330 84.9 10/07/19 13:27 Acenaphthylene ug/kg ND 330 78.1 10/07/19 13:27 Aniline ug/kg ND 330 74.1 10/07/19 13:27 Anthracene ug/kg ND 330 85.6 10/07/19 13:27 Benzo(a)anthracene ug/kg ND 330 105 10/07/19 13:27 Benzo(a)pyrene ug/kg ND 330 143 10/07/19 13:27 Benzo(b)fluoranthene ug/kg ND 330 133 10/07/19 13:27 Benzo(g,h,i)perylene ug/kg ND 330 129 10/07/19 13:27 Benzo(k)fluoranthene ug/kg ND 330 139 10/07/19 13:27 Benzoic Acid ug/kg ND 1650 356 10/07/19 13:27 v2 Benzyl alcohol ug/kg ND 660 175 10/07/19 13:27 bis(2-Chloroethoxy)methane ug/kg ND 330 88.1 10/07/19 13:27 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UNCC MOOR HALL Pace Project No.: 92447655 METHOD BLANK: 2696483 Matrix: Associated Lab Samples: 92447655001, 92447655002, 92447655003 Blank Parameter Units Result Solid Reporting Limit MDL Analyzed bis(2-Chloroethyl) ether ug/kg ND 330 70.1 10/07/19 13:27 bis(2-Ethylhexyl)phthalate ug/kg ND 330 108 10/07/19 13:27 Butylbenzylphthalate ug/kg ND 330 87.9 10/07/19 13:27 Chrysene ug/kg ND 330 95.8 10/07/19 13:27 Di-n-butylphthalate ug/kg ND 330 81.4 10/07/19 13:27 Di-n-octylphthalate ug/kg ND 330 188 10/07/19 13:27 Dibenz(a,h)anthracene ug/kg ND 330 132 10/07/19 13:27 Dibenzofuran ug/kg ND 330 82.5 10/07/19 13:27 Diethylphthalate ug/kg ND 330 71.6 10/07/19 13:27 Dimethylphthalate ug/kg ND 330 74.6 10/07/19 13:27 Fluoranthene ug/kg ND 330 99.7 10/07/19 13:27 Fluorene ug/kg ND 330 88.3 10/07/19 13:27 Hexachloro-1,3-butadiene ug/kg ND 330 80.2 10/07/19 13:27 Hexachlorobenzene ug/kg ND 330 83.8 10/07/19 13:27 Hexachlorocyclopentadiene ug/kg ND 330 132 10/07/19 13:27 Hexachloroethane ug/kg ND 330 75.2 10/07/19 13:27 Indeno(1,2,3-cd)pyrene ug/kg ND 330 151 10/07/19 13:27 Isophorone ug/kg ND 330 71.7 10/07/19 13:27 N-Nitroso-di-n-propylamine ug/kg ND 330 92.4 10/07/19 13:27 N-Nitrosodimethylamine ug/kg ND 330 92.8 10/07/19 13:27 N-Nitrosodiphenylamine ug/kg ND 330 84.2 10/07/19 13:27 Naphthalene ug/kg ND 330 79.0 10/07/19 13:27 Nitrobenzene ug/kg ND 330 78.8 10/07/19 13:27 Pentachlorophenol ug/kg ND 1650 151 10/07/19 13:27 Phenanthrene ug/kg ND 330 83.1 10/07/19 13:27 Phenol ug/kg ND 330 78.8 10/07/19 13:27 Pyrene ug/kg ND 330 90.8 10/07/19 13:27 Pyridine ug/kg ND 330 83.5 10/07/19 13:27 2,4,6-Tribromophenol (S) % 75 27-110 10/07/19 13:27 2-Fluorobiphenyl (S) % 70 30-110 10/07/19 13:27 2-Fluorophenol (S) % 70 13-110 10/07/19 13:27 Nitrobenzene-d5 (S) % 62 23-110 10/07/19 13:27 Phenol-d6 (S) % 68 22-110 10/07/19 13:27 Terphenyl-d14 (S) % 71 28-110 10/07/19 13:27 v2 Qualifiers LABORATORY CONTROL SAMPLE: 2696484 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/kg 1670 1250 75 52-130 1,2-Dichlorobenzene ug/kg 1670 1250 75 51-130 1,3-Dichlorobenzene ug/kg 1670 1240 74 50-130 1,4-Dichlorobenzene ug/kg 1670 1240 74 49-130 1-Methylnaphthalene ug/kg 1670 1280 77 55-130 2,2'-Oxybis(1-chloropropane) ug/kg 1670 1230 74 30-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UNCC MOOR HALL Pace Project No.: 92447655 LABORATORY CONTROL SAMPLE: Parameter 2696484 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers 2,4,5-Trichlorophenol ug/kg 1670 1230 74 55-130 2,4,6-Trichlorophenol ug/kg 1670 1280 77 57-130 2,4-Dichlorophenol ug/kg 1670 1260 76 56-130 2,4-Dimethylphenol ug/kg 1670 1290 78 51-130 2,4-Dinitrophenol ug/kg 8330 7040 85 27-133 2,4-Dinitrotoluene ug/kg 1670 1180 71 61-130 2,6-Dinitrotoluene ug/kg 1670 1300 78 60-130 2-Chloronaphthalene ug/kg 1670 1290 77 52-130 2-Chlorophenol ug/kg 1670 1320 79 54-130 2-Methylnaphthalene ug/kg 1670 1300 78 54-130 2-Methylphenol(o-Cresol) ug/kg 1670 1240 75 51-130 2-Nitroaniline ug/kg 3330 2160 65 51-130 2-Nitrophenol ug/kg 1670 1470 88 49-130 3&4-Methyl phenol (m&p Cresol) ug/kg 1670 1260 76 11-163 3,3'-Dichlorobenzidine ug/kg 3330 2370 71 10-132 3-Nitroaniline ug/kg 3330 2230 67 55-130 4,6-Dinitro-2-methyl phenol ug/kg 3330 3600 108 47-142 4-Bromophenylphenyl ether ug/kg 1670 1470 88 59-130 4-ChIoro-3-methyl phenol ug/kg 3330 2350 70 55-130 4-Chloroaniline ug/kg 3330 2470 74 54-130 4-Chlorophenylphenyl ether ug/kg 1670 1190 71 58-130 4-Nitroaniline ug/kg 3330 2230 67 54-130 4-Nitrophenol ug/kg 8330 4280 51 48-130 Acenaphthene ug/kg 1670 1310 79 60-130 Acenaphthylene ug/kg 1670 1430 86 60-130 Aniline ug/kg 1670 1090 65 43-130 Anthracene ug/kg 1670 1420 85 63-130 Benzo(a)anthracene ug/kg 1670 1500 90 59-130 Benzo(a)pyrene ug/kg 1670 1510 91 57-130 Benzo(b)fluoranthene ug/kg 1670 1450 87 54-130 Benzo(g,h,i)perylene ug/kg 1670 1570 94 59-130 Benzo(k)fluoranthene ug/kg 1670 1540 92 54-130 Benzoic Acid ug/kg 8330 4680 56 19-130 v2 Benzyl alcohol ug/kg 3330 2470 74 50-130 bis(2-Chloroethoxy)methane ug/kg 1670 1290 77 54-130 bis(2-Chloroethyl) ether ug/kg 1670 1350 81 48-130 bis(2-Ethylhexyl)phthalate ug/kg 1670 1500 90 45-134 Butylbenzylphthalate ug/kg 1670 1510 91 46-138 Chrysene ug/kg 1670 1460 88 58-130 Di-n-butylphthalate ug/kg 1670 1370 82 60-130 Di-n-octylphthalate ug/kg 1670 1560 94 53-130 Dibenz(a,h)anthracene ug/kg 1670 1580 95 59-130 Dibenzofuran ug/kg 1670 1240 75 60-130 Diethylphthalate ug/kg 1670 1110 67 60-130 Dimethylphthalate ug/kg 1670 1220 73 60-130 Fluoranthene ug/kg 1670 1360 81 65-130 Fluorene ug/kg 1670 1210 73 63-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UNCC MOOR HALL Pace Project No.: 92447655 LABORATORY CONTROL SAMPLE: Parameter 2696484 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Hexachloro-1,3-butadiene ug/kg 1670 1150 69 46-130 Hexachlorobenzene ug/kg 1670 1330 80 58-130 Hexachlorocyclopentadiene ug/kg 1670 1490 90 23-130 Hexachloroethane ug/kg 1670 1190 71 47-130 Indeno(1,2,3-cd)pyrene ug/kg 1670 1510 90 60-130 Isophorone ug/kg 1670 1170 70 49-130 N-Nitroso-di-n-propylamine ug/kg 1670 1130 68 47-130 v2 N-Nitrosodimethylamine ug/kg 1670 1230 74 45-130 N-Nitrosodiphenylamine ug/kg 1670 1480 89 59-130 Naphthalene ug/kg 1670 1370 82 55-130 Nitrobenzene ug/kg 1670 1140 68 49-130 Pentachlorophenol ug/kg 3330 2810 84 10-132 Phenanthrene ug/kg 1670 1480 89 62-130 Phenol ug/kg 1670 1280 77 46-130 Pyrene ug/kg 1670 1610 97 53-130 Pyridine ug/kg 1670 1040 62 37-130 2,4,6-Tribromophenol (S) % 92 27-110 2-Fluorobiphenyl (S) % 78 30-110 2-Fluorophenol(S) % 77 13-110 Nitrobenzene-d5(S) % 69 23-110 Phenol-d6 (S) % 71 22-110 Terphenyl-d14 (S) % 83 28-110 MATRIX SPIKE SAMPLE: Parameter 2696485 Units 92447080001 Result Spike Conc. MS Result MS % Rec % Rec Limits Qualifiers 1,2,4-Trichlorobenzene ug/kg ND 2010 980 49 18-130 1,2-Dichlorobenzene ug/kg ND 2010 1010 50 14-130 1,3-Dichlorobenzene ug/kg ND 2010 985 49 12-130 1,4-Dichlorobenzene ug/kg ND 2010 987 49 10-130 1-Methylnaphthalene ug/kg ND 2010 1070 53 12-130 2,2'-Oxybis(1-chloropropane) ug/kg ND 2010 992 50 10-130 2,4,5-Trichlorophenol ug/kg ND 2010 1110 56 13-130 2,4,6-Trichlorophenol ug/kg ND 2010 1140 57 17-130 2,4-Dichlorophenol ug/kg ND 2010 1060 53 10-130 2,4-Dimethylphenol ug/kg ND 2010 1070 53 10-130 2,4-Dinitrophenol ug/kg ND 10000 6500 65 10-130 2,4-Dinitrotoluene ug/kg ND 2010 1150 57 24-130 2,6-Dinitrotoluene ug/kg ND 2010 1230 62 23-130 2-Chloronaphthalene ug/kg ND 2010 1060 53 19-130 2-Chlorophenol ug/kg ND 2010 1070 53 10-130 2-Methylnaphthalene ug/kg ND 2010 1070 54 18-130 2-Methylphenol(o-Cresol) ug/kg ND 2010 1050 53 10-130 2-Nitroaniline ug/kg ND 4000 2030 51 17-130 2-Nitrophenol ug/kg ND 2010 1180 59 10-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UNCC MOOR HALL Pace Project No.: 92447655 MATRIX SPIKE SAMPLE: 2696485 92447080001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers 3&4-Methyl phenol (m&p Cresol) ug/kg ND 2010 1070 54 10-130 3,3'-Dichlorobenzidine ug/kg ND 4000 2240 56 10-130 3-Nitroaniline ug/kg ND 4000 2250 56 24-130 4,6-Dinitro-2-methyl phenol ug/kg ND 4000 3400 85 10-152 4-Bromophenylphenyl ether ug/kg ND 2010 1300 65 29-130 4-Chloro-3-methylphenol ug/kg ND 4000 2170 54 17-130 4-Chloroaniline ug/kg ND 4000 2180 54 14-130 4-Chlorophenylphenyl ether ug/kg ND 2010 1070 53 25-130 4-Nitroaniline ug/kg ND 4000 2210 55 22-130 4-Nitrophenol ug/kg ND 10000 4100 41 10-130 Acenaphthene ug/kg ND 2010 1150 57 20-130 Acenaphthylene ug/kg ND 2010 1270 63 25-130 Aniline ug/kg ND 2010 917 46 10-130 Anthracene ug/kg ND 2010 1300 65 29-130 Benzo(a)anthracene ug/kg ND 2010 1320 66 19-130 Benzo(a)pyrene ug/kg ND 2010 1330 66 12-130 Benzo(b)fluoranthene ug/kg ND 2010 1250 62 14-130 Benzo(g,h,i)perylene ug/kg ND 2010 1300 65 10-130 Benzo(k)fluoranthene ug/kg ND 2010 1370 68 14-130 Benzoic Acid ug/kg ND 10000 2430 24 10-130 v2 Benzyl alcohol ug/kg ND 4000 2080 52 13-130 bis(2-Chloroethoxy)methane ug/kg ND 2010 1030 52 16-130 bis(2-Chloroethyl) ether ug/kg ND 2010 1090 54 11-130 bis(2-Ethylhexyl)phthalate ug/kg ND 2010 1330 66 21-130 Butylbenzylphthalate ug/kg ND 2010 1360 68 23-130 Chrysene ug/kg ND 2010 1300 65 22-130 Di-n-butylphthalate ug/kg ND 2010 1220 61 30-130 Di-n-octylphthalate ug/kg ND 2010 1330 66 23-142 Dibenz(a,h)anthracene ug/kg ND 2010 1330 66 10-130 Dibenzofuran ug/kg ND 2010 1120 56 24-130 Diethylphthalate ug/kg ND 2010 1060 53 26-130 Dimethylphthalate ug/kg ND 2010 1160 58 22-130 Fluoranthene ug/kg ND 2010 1220 61 33-130 Fluorene ug/kg ND 2010 1110 56 22-130 Hexachloro-1,3-butadiene ug/kg ND 2010 825 41 13-130 Hexachlorobenzene ug/kg ND 2010 1190 59 29-130 Hexachlorocyclopentadiene ug/kg ND 2010 1010 50 10-130 Hexachloroethane ug/kg ND 2010 896 45 10-130 Indeno(1,2,3-cd)pyrene ug/kg ND 2010 1260 63 10-130 Isophorone ug/kg ND 2010 1010 50 13-130 N-Nitroso-di-n-propylamine ug/kg ND 2010 986 49 12-130 v2 N-Nitrosodimethylamine ug/kg ND 2010 966 48 11-130 N-Nitrosodiphenylamine ug/kg ND 2010 1380 69 15-130 Naphthalene ug/kg ND 2010 1110 56 15-130 Nitrobenzene ug/kg ND 2010 904 45 12-130 Pentachlorophenol ug/kg ND 4000 2620 65 10-130 Phenanthrene ug/kg ND 2010 1360 68 27-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UNCC MOOR HALL Pace Project No.: 92447655 MATRIX SPIKE SAMPLE: Parameter 2696485 Units 92447080001 Result Spike Conc. MS MS Result % Rec % Rec Limits Qualifiers Phenol ug/kg ND 2010 1050 52 10-130 Pyrene ug/kg ND 2010 1480 74 19-130 Pyridine ug/kg ND 2010 777 39 10-130 2,4,6-Tribromophenol (S) % 71 27-110 2-Fluorobiphenyl (S) % 52 30-110 2-Fluorophenol(S) % 51 13-110 Nitrobenzene-d5 (S) % 46 23-110 Phenol-d6 (S) % 49 22-110 Terphenyl-d14 (S) % 63 28-110 SAMPLE DUPLICATE: 2696486 Parameter Units 92447080001 Result Dup Result RPD Max RPD Qualifiers 1,2,4-Trichlorobenzene ug/kg ND ND 30 1,2-Dichlorobenzene ug/kg ND ND 30 1,3-Dichlorobenzene ug/kg ND ND 30 1,4-Dichlorobenzene ug/kg ND ND 30 1-Methylnaphthalene ug/kg ND ND 30 2,2'-Oxybis(1-chloropropane) ug/kg ND ND 30 v1 2,4,5-Trichlorophenol ug/kg ND ND 30 2,4,6-Trichlorophenol ug/kg ND ND 30 2,4-Dichlorophenol ug/kg ND ND 30 2,4-Dimethylphenol ug/kg ND ND 30 2,4-Dinitrophenol ug/kg ND ND 30 2,4-Dinitrotoluene ug/kg ND ND 30 2,6-Dinitrotoluene ug/kg ND ND 30 2-Chloronaphthalene ug/kg ND ND 30 2-Chlorophenol ug/kg ND ND 30 2-Methylnaphthalene ug/kg ND ND 30 2-Methylphenol(o-Cresol) ug/kg ND ND 30 2-Nitroaniline ug/kg ND ND 30 2-Nitrophenol ug/kg ND ND 30 3&4-Methyl phenol (m&p Cresol) ug/kg ND ND 30 3,3'-Dichlorobenzidine ug/kg ND ND 30 3-Nitroaniline ug/kg ND ND 30 4,6-Dinitro-2-methyl phenol ug/kg ND ND 30 4-Bromophenylphenyl ether ug/kg ND ND 30 4-ChIoro-3-methyl phenol ug/kg ND ND 30 4-Chloroaniline ug/kg ND ND 30 4-Chlorophenylphenyl ether ug/kg ND ND 30 4-Nitroaniline ug/kg ND ND 30 4-Nitrophenol ug/kg ND ND 30 Acenaphthene ug/kg ND ND 30 Acenaphthylene ug/kg ND ND 30 Aniline ug/kg ND ND 30 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 38 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: UNCC MOOR HALL Pace Project No.: 92447655 SAMPLE DUPLICATE: 2696486 Parameter Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl alcohol bis(2-Chloroethoxy)methane bis(2-Chloroethyl) ether bis(2-Ethylhexyl)phthalate Butylbenzylphthalate Chrysene Di-n-butylphthalate Di-n-octylphthalate Dibenz(a,h)anthracene Dibenzofuran Diethylphthalate Dimethylphthalate Fluoranthene Fluorene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-cd)pyrene Isophorone N-Nitroso-di-n-propylamine N-Nitrosodimethylamine N-Nitrosodiphenylamine Naphthalene Nitrobenzene Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine 2,4,6-Tribromophenol (S) 2-Fluorobiphenyl (S) 2-Fluorophenol(S) Nitrobenzene-d5 (S) Phenol-d6 (S) Terphenyl-d14 (S) QUALITY CONTROL DATA Units 92447080001 Dup Result Result ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND ug/kg ND % 57 % 55 % 57 % 49 % 55 % 55 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 59 40 38 39 38 53 Max RPD RPD 30 30 30 30 30 30 30 30 30 30 30 v1 30 v1 30 30 30 v1 30 30 30 30 30 30 30 30 30 v2 30 30 30 30 30 30 30 30 30 30 30 30 30 Qualifiers Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UNCC MOOR HALL Pace Project No.: 92447655 QC Batch: 501379 Analysis Method: MADEP EPH QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Soil Associated Lab Samples: 92447655001, 92447655002, 92447655003 METHOD BLANK: 2696480 Matrix: Solid Associated Lab Samples: 92447655001, 92447655002, 92447655003 Blank Reporting Parameter Units Result Limit MDL Analyzed Qualifiers Aliphatic (C09-C18) mg/kg ND 10.0 10.0 10/03/19 16:14 N2 Aliphatic (C19-C36) mg/kg ND 10.0 10.0 10/03/19 16:14 N2 Aromatic (C11-C22) mg/kg ND 10.0 10.0 10/03/19 16:14 N2 2-Bromonaphthalene (S) % 103 40-140 10/03/19 16:14 2-Fluorobiphenyl (S) % 104 40-140 10/03/19 16:14 Nonatriacontane (S) % 73 40-140 10/03/19 16:14 o-Terphenyl (S) % 82 40-140 10/03/19 16:14 LABORATORY CONTROL SAMPLE & LCSD: Parameter 2696481 Units Spike Conc. 2696482 LCS LCSD Result Result LCS LCSD % Rec % Rec % Rec Max Limits RPD RPD Qualifiers Aliphatic (C09-C18) mg/kg 10 ND ND 49 52 40-140 50 N2 Aliphatic (C19-C36) mg/kg 13.3 ND ND 65 66 40-140 50 N2 Aromatic (C11-C22) mg/kg 28.3 22.5 21.0 79 74 40-140 7 50 N2 2-Bromonaphthalene (S) % 105 85 40-140 2-Fluorobiphenyl (S) % 105 88 40-140 Nonatriacontane (S) % 67 63 40-140 o-Terphenyl(S) % 88 83 40-140 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 40 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: UNCC MOOR HALL Pace Project No.: 92447655 QC Batch: 500976 Analysis Method: ASTM D2974-87 QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture Associated Lab Samples: 92447655001, 92447655002, 92447655003 SAMPLE DUPLICATE: 2694765 92446155002 Dup Max Parameter Units Result Result RPD RPD Qualifiers Percent Moisture % 90.0 89.8 0 25 SAMPLE DUPLICATE: 2694772 92447655003 Dup Max Parameter Units Result Result RPD RPD Qualifiers Percent Moisture % 16.0 14.8 8 25 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: UNCC MOOR HALL Pace Project No.: 92447655 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. LABORATORIES PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS B Analyte was detected in the associated method blank. IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be considered an estimated value. N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request. v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the associated samples may have a high bias. v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 44 aceAnalytical —pacelabs.com Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: UNCC MOOR HALL 92447655 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92447655001 SSW MADEP EPH 501379 MADEP EPH 501703 92447655002 ESW MADEP EPH 501379 MADEP EPH 501703 92447655003 BOTTOM MADEP EPH 501379 MADEP EPH 501703 92447655001 SSW MADEP VPH 501245 MADEP VPH 501275 92447655002 ESW MADEP VPH 501245 MADEP VPH 501275 92447655003 BOTTOM MADEP VPH 501245 MADEP VPH 501275 92447655001 SSW EPA 3546 501380 EPA 8270E 502038 92447655002 ESW EPA 3546 501380 EPA 8270E 502038 92447655003 BOTTOM EPA 3546 501380 EPA 8270E 502038 92447655001 SSW EPA 5035A 501807 EPA 8260D 501826 92447655002 ESW EPA 5035A 502304 EPA 8260D 502318 92447655003 BOTTOM EPA 5035A 501807 EPA 8260D 501826 92447655001 SSW ASTM D2974-87 500976 92447655002 ESW ASTM D2974-87 500976 92447655003 BOTTOM ASTM D2974-87 500976 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/08/2019 05:11 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 44 v u m a u l b U u `\ �C �,QQ2QQ�`QQq Z2�ZZaz Z2 lam, a a G Z Z Z `. O` u t 41 C (R- u 4 v i N o u 1a a a ❑ m m E" E m acm m yv -.G, " H O H C R F� tj v> + a aro H m �� _m m �., m Nrornu o•Wrovoo u v c ro„ a m a x a s E v v w E ro u N a u N ro a N W 7 E E a o a o E , U - H 4 Nh Ory C1 a N a-.ci U Nsi NM+ro+ Z v O H d, L O a o o f- F U U U U I 'O Wv U dl o U of a. Qf 7 H y 34 'U Q o J E 4' d E N N E N N ,-{ jj U VumU°wcn�v3lo wu a cWq mz a,roj � J 7 � d t} O Z u m p a O In v c ' u 'o FT u a N N V F Z > 7 z a a a � � ( kmt > % ❑ a E �. E E E S O a x fcc 6✓ J VI J V1 G F C 0 > V dr O Z N F. aj � �• � U q v 'yl E ^ o o cr V - IX E > a u q o 0 u F -d i z o a � u U i a ❑ 2 O Q � c Q C d, O Ip o " o m E wcn u cn vU `5 ]` oc o. t o F o m W t F EE t O T Q = V U o � Of U v O q 0 F a z a Z O V E- i � C s fp -- # d, u O v � o 7 v3 4 cf � m n a .F 2 w U _0 v � L p _ y R v u. m L5 } q } ? O -- Q- O U p p T N aj t7 � o E m a u 4 m CL C7 Ip Y N � u n N v C c O O � n v x — O o p V) E -a a x Y n u O d 2 m O a a u r Z C a O z Z dl C C T O c V E Q E U C] lOn O U U T > v N 9 n > N N di V O C �. E E -E `m L m O ❑ x .n D a N C U N C Ln � c c C a E E n � a v E L L O U T K t4 of a LPRISM Full -Service Analytical & Environmental Solutions LABORATORIES, INC. Summit Engineering (Charlotte) Michael Zavislak P.O. Box 7384 Charlotte, NC 28241 NC Certification No. 402 NC Drinking Water Cert No. 37735 SC Certification No. 99012 Project: UNCC Lab Submittal Date: 08/27/2019 Prism Work Order: 9080388 Case Narrative 8/29/19 11:51 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Narrative Notes: Samples were received on wet ice at a temperature of 26.2degrees C; however, samples were submitted to the laboratory within 45 minutes of sample collection. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Robbi A. Jones President/Project Manager Data Qualifiers Key Reference: Reviewed By Robbi A. Jones President/Project Manager J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag). L Parameter reported with possible low bias. LCS recovery below the QC limit. L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken. U Not Detected at the MDL MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 1 of 21 �Full -Service R I IS M Service Analytical Environmental Solutions -LABORATORIES, INC. Sample Receipt Summary 08/29/2019 Prism Work Order: 9080388 Client Sample ID Lab Sample ID Matrix Date/Time Sampled Date/Time Received S-1 9080388-01 Solid 08/27/19 15:00 08/27/19 15:45 Samples were received at 26.2 degrees C. See case narrative for further information. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 2 of 21 Full -Service Analytical & PRISMSummary Environmental Solutions LABORATORIES, INC. of Detections 08/29/2019 Prism Work Order: 9080388 Prism ID Client ID Parameter Method Result Units 9080388-01 S-1 Diesel Range Organics "8015C 580 mg/kg dry 9080388-01 S-1 Gasoline Range Organics '8015C 99 mg/kg dry 9080388-01 S-1 2-Methylnaphthalene 8270E 0.92 mg/kg dry 9080388-01 S-1 Fluorene 8270E 0.10 J mg/kg dry 9080388-01 S-1 Naphthalene 8270E 0.20 J mg/kg dry 9080388-01 S-1 1,2,4-Trimethylbenzene 8260D 0.0032 J mg/kg dry 9080388-01 S-1 1,3,5-Trimethylbenzene 8260D 0.0059 mg/kg dry 9080388-01 S-1 4-Isopropyltoluene 8260D 0.016 mg/kg dry 9080388-01 S-1 Acetone 8260D 0.029 mg/kg dry 9080388-01 S-1 I sopropyl benzene (Cumene) 8260D 0.0049 mg/kg dry 9080388-01 S-1 Naphthalene 8260D 0.032 mg/kg dry 9080388-01 S-1 n-Butylbenzene 8260D 0.034 mg/kg dry 9080388-01 S-1 n-Propylbenzene 8260D 0.0070 mg/kg dry 9080388-01 S-1 sec -Butyl benzene 8260D 0.036 mg/kg dry 9080388-01 S-1 tert-Butylbenzene 8260D 0.012 mg/kg dry This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 3 of 21 PRISM Full -Service Analytical & Laboratory Report Environmental Solutions 08/29/2019 & I LABORATORIES, INC. Summit Engineering (Charlotte) Project: UNCC Client Sample ID: S-1 Attn: Michael Zavislak Prism Sample ID: 9080388-01 P.O. Box 7384 Prism Work Order: 9080388 Charlotte, NC 28241 Sample Matrix: Solid Time Collected: 08/27/19 15:00 Time Submitted: 08/27/19 15:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Diesel Range Organics by GC/FID Diesel Range Organics 580 mg/kg dry 85 28 10 *8015C 8/28/19 13:50 ZRC P9H0463 Surrogate Recovery Control Limits o-Terphenyl 53 % 31-123 Gasoline Range Organics by GC/FID Gasoline Range Organics 99 mg/kg dry 4.9 1.3 50 *8015C 8/28/19 10:45 TBL P9H0451 Surrogate Recovery Control Limits a,a,a-Trifluorotoluene 127 % 50-137 General Chemistry Parameters % Solids 82.3 % by 0.100 0.100 1 *SM2540 G 8128/19 13:30 EDV P9H0461 Weight Semivolatile Organic Compounds by GC/MS 1,2,4-Trichlorobenzene 0.14 U mg/kg dry 0.80 0.14 1 8270E 8/28/19 14:05 JMV P91-10462 1,2-Dichlorobenzene 0.13 U mg/kg dry 0.80 0.13 1 8270E 8/28/19 14:05 JMV P91-10462 1,3-Dichlorobenzene 0.12 U mg/kg dry 0.80 0.12 1 8270E 8/28/19 14:05 JMV P91-10462 1,4-Dichlorobenzene 0.13 U mg/kg dry 0.40 0.13 1 8270E 8/28/19 14:05 JMV P91-10462 2,4,5-Trichlorophenol 0.17 U mg/kg dry 0.80 0.17 1 8270E 8/28/19 14:05 JMV P91-10462 2,4,6-Trichlorophenol 0.19 U mg/kg dry 0.80 0.19 1 8270E 8/28/19 14:05 JMV P91-10462 2,4-Dichlorophenol 0.16 U mg/kg dry 0.80 0.16 1 8270E 8/28/19 14:05 JMV P91-10462 2,4-Dimethylphenol 0.17 U mg/kg dry 0.40 0.17 1 8270E 8/28/19 14:05 JMV P91-10462 2,4-Dinitrophenol 0.47 U mg/kg dry 1.8 0.47 1 8270E 8/28/19 14:05 JMV P91-10462 2,4-Dinitrotoluene 0.21 U mg/kg dry 0.80 0.21 1 8270E 8/28/19 14:05 JMV P91-10462 2,6-Dinitrotoluene 0.21 U mg/kg dry 0.80 0.21 1 8270E 8/28/19 14:05 JMV P91-10462 2-Chloronaphthalene 0.19 U mg/kg dry 0.80 0.19 1 8270E 8/28/19 14:05 JMV P91-10462 2-Chlorophenol 0.15 U mg/kg dry 0.80 0.15 1 8270E 8/28/19 14:05 JMV P91-10462 2-Methyl naphthalene 0.92 mg/kg dry 0.80 0.015 1 8270E 8/28/19 14:05 JMV P9H0462 2-Methylphenol 0.15 U mg/kg dry 0.80 0.15 1 8270E 8/28/19 14:05 JMV P91-10462 2-Nitroaniline 0.17 U mg/kg dry 0.80 0.17 1 8270E 8/28/19 14:05 JMV P91-10462 2-Nitrophenol 0.13 U mg/kg dry 0.80 0.13 1 8270E 8/28/19 14:05 JMV P91-10462 3,3'-Dichlorobenzidine 0.16 U mg/kg dry 0.80 0.16 1 8270E 8/28/19 14:05 JMV P91-10462 3/4-Methyl phenol 0.17 U mg/kg dry 0.80 0.17 1 8270E 8/28/19 14:05 JMV P91-10462 3-Nitroaniline 0.15 U mg/kg dry 0.80 0.15 1 8270E 8/28/19 14:05 JMV P91-10462 4,6-Dinitro-2-methylphenol 0.44 U mg/kg dry 1.8 0.44 1 8270E 8/28/19 14:05 JMV P91-10462 4-Bromophenyl phenyl ether 0.19 U mg/kg dry 0.80 0.19 1 8270E 8/28/19 14:05 JMV P91-10462 4-Chloro-3-methylphenol 0.15 U mg/kg dry 0.80 0.15 1 8270E 8/28/19 14:05 JMV P91-10462 4-Chloroaniline 0.097 U mg/kg dry 0.40 0.097 1 8270E 8/28/19 14:05 JMV P91-10462 4-Chlorophenyl phenyl ether 0.24 U mg/kg dry 1.2 0.24 1 8270E 8/28/19 14:05 JMV P91-10462 4-Nitroaniline 0.12 U mg/kg dry 0.40 0.12 1 8270E 8/28/19 14:05 JMV P91-10462 4-Nitrophenol 0.20 U mg/kg dry 0.80 0.20 1 8270E 8/28/19 14:05 JMV P91-10462 Acenaphthene 0.018 U mg/kg dry 0.80 0.018 1 8270E 8/28/19 14:05 JMV P91-10462 Acenaphthylene 0.016 U mg/kg dry 0.80 0.016 1 8270E 8/28/19 14:05 JMV P91-10462 Aniline 0.20 U mg/kg dry 0.80 0.20 1 8270E 8/28/19 14:05 JMV P91-10462 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 4 of 21 P R I S M Full -Service Analytical 8 Laboratory Report � Environmental Solutions 08/29/2019 LABORATORIES, INC. Summit Engineering (Charlotte) Project: UNCC Client Sample ID: S-1 Attn: Michael Zavislak Prism Sample ID: 9080388-01 P.O. Box 7384 Prism Work Order: 9080388 Charlotte, NC 28241 Sample Matrix: Solid Time Collected: 08/27/19 15:00 Time Submitted: 08/27/19 15:45 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/Time Batch ID Anthracene 0.0088 U mg/kg dry 0.80 0.0088 1 8270E 8/28/19 14:05 JMV P91-10462 Azobenzene 0.17 U mg/kg dry 0.80 0.17 1 8270E 8/28/19 14:05 JMV P91-10462 Benzo(a)anthracene 0.0096 U mg/kg dry 0.80 0.0096 1 8270E 8/28/19 14:05 JMV P91-10462 Benzo(a)pyrene 0.0071 U mg/kg dry 0.80 0.0071 1 8270E 8/28/19 14:05 JMV P91-10462 Benzo(b)fluoranthene 0.0074 U mg/kg dry 0.80 0.0074 1 8270E 8128/19 14:05 JMV P91-10462 Benzo(g,h,i)perylene 0.0079 U mg/kg dry 0.80 0.0079 1 8270E 8/28/19 14:05 JMV P91-10462 Benzo(k)fluoranthene 0.0085 U mg/kg dry 0.80 0.0085 1 8270E 8/28/19 14:05 JMV P91-10462 Benzoic Acid 0.66 U mg/kg dry 2.4 0.66 1 8270E 8/28/19 14:05 JMV P91-10462 Benzyl alcohol 0.15 U mg/kg dry 0.80 0.15 1 8270E 8/28/19 14:05 JMV P91-10462 bis(2-Chloroethoxy)methane 0.15 U mg/kg dry 0.80 0.15 1 8270E 8/28/19 14:05 JMV P91-10462 Bis(2-Chloroethyl)ether 0.13 U mg/kg dry 0.80 0.13 1 8270E 8/28/19 14:05 JMV P91-10462 Bis(2-chloroisopropyl)ether 0.14 U mg/kg dry 0.40 0.14 1 8270E 8/28/19 14:05 JMV P91-10462 Bis(2-Ethylhexyl)phthalate 0.18 U mg/kg dry 0.80 0.18 1 8270E 8/28/19 14:05 JMV P91-10462 Butyl benzyl phthalate 0.14 U mg/kg dry 0.40 0.14 1 8270E 8/28/19 14:05 JMV P91-10462 Chrysene 0.0094 U mg/kg dry 0.80 0.0094 1 8270E 8/28/19 14:05 JMV P91-10462 Dibenzo(a,h)anthracene 0.023 U mg/kg dry 0.80 0.023 1 8270E 8/28/19 14:05 JMV P91-10462 Dibenzofuran 0.22 U mg/kg dry 0.80 0.22 1 8270E 8128/19 14:05 JMV P91-10462 Diethyl phthalate 0.21 U mg/kg dry 0.80 0.21 1 8270E 8/28/19 14:05 JMV P91-10462 Dimethyl phthalate 0.19 U mg/kg dry 0.80 0.19 1 8270E 8/28/19 14:05 JMV P91-10462 Di-n-butyl phthalate 0.20 U mg/kg dry 0.80 0.20 1 8270E 8/28/19 14:05 JMV P91-10462 Di-n-octyl phthalate 0.21 U mg/kg dry 0.40 0.21 1 8270E 8/28/19 14:05 JMV P91-10462 Fluoranthene 0.0091 U mg/kg dry 0.80 0.0091 1 8270E 8/28/19 14:05 JMV P91-10462 Fluorene 0.10 J mg/kg dry 0.80 0.014 1 8270E 8/28/19 14:05 JMV P9H0462 Hexachlorobenzene 0.18 U mg/kg dry 0.80 0.18 1 8270E 8/28/19 14:05 JMV P91-10462 Hexachlorobutadiene 0.18 U mg/kg dry 0.80 0.18 1 8270E 8/28/19 14:05 JMV P91-10462 Hexachlorocyclopentadiene 0.27 U mg/kg dry 0.80 0.27 1 8270E 8/28/19 14:05 JMV P91-10462 Hexachloroethane 0.13 U mg/kg dry 0.80 0.13 1 8270E 8/28/19 14:05 JMV P91-10462 Indeno(1,2,3-cd)pyrene 0.023 U mg/kg dry 0.80 0.023 1 8270E 8/28/19 14:05 JMV P91-10462 Isophorone 0.17 U mg/kg dry 0.80 0.17 1 8270E 8/28/19 14:05 JMV P91-10462 Naphthalene 0.20 J mg/kg dry 0.80 0.017 1 8270E 8/28/19 14:05 JMV P9H0462 Nitrobenzene 0.17 U mg/kg dry 0.40 0.17 1 8270E 8/28/19 14:05 JMV P91-10462 N-Nitroso-di-n-propylamine 0.18 U mg/kg dry 0.80 0.18 1 8270E 8/28/19 14:05 JMV P91-10462 N-Nitrosodiphenylamine 0.22 U mg/kg dry 0.80 0.22 1 8270E 8/28/19 14:05 JMV P91-10462 Pentachlorophenol 0.51 U mg/kg dry 1.2 0.51 1 8270E 8/28/19 14:05 JMV P91-10462 Phenanthrene 0.0087 U mg/kg dry 0.80 0.0087 1 8270E 8/28/19 14:05 JMV P91-10462 Phenol 0.13 U mg/kg dry 0.80 0.13 1 8270E 8/28/19 14:05 JMV P91-10462 Pyrene 0.012 U mg/kg dry 0.80 0.012 1 8270E 8/28/19 14:05 JMV P91-10462 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 64 % 39-132 2-Fluorobiphenyl 66 % 44-115 2-Fluorophenol 67 % 35-115 Nitrobenzene-d5 50 % 37-122 Phenol-d5 62 % 34-121 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 5 of 21 Laboratory Report Full -Service P R S M Analytical & Environmental LABORATORIES INC. Solutions 08/29/2019 Summit Engineering (Charlotte) Project: UNCC Client Sample ID: S-1 Attn: Michael Zavislak Prism Sample ID: 9080388-01 P.O. Box 7384 Prism Work Order: 9080388 Charlotte, NC 28241 Sample Matrix: Solid Time Collected: 08/27/19 15:00 Time Submitted: 08/27/19 15:45 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Terphenyl-d14 63 % 54-127 Volatile Organic Compounds by GUMS 1,1,1,2-Tetrachloroethane 0.00053 U mg/kg dry 0.0044 0.00053 1 8260D 8/29/19 3:56 JLB P91-10480 1,1,1-Trichloroethane 0.00064 U mg/kg dry 0.0044 0.00064 1 8260D 8/29/19 3:56 JLB P91-10480 1,1,2,2-Tetrachloroethane 0.00032 U mg/kg dry 0.0044 0.00032 1 8260D 8/29/19 3:56 JLB P91-10480 1,1,2-Trichloroethane 0.00047 U mg/kg dry 0.0044 0.00047 1 8260D 8/29/19 3:56 JLB P91-10480 1,1-Dichloroethane 0.00079 U mg/kg dry 0.0044 0.00079 1 8260D 8/29/19 3:56 JLB P91-10480 1,1-Dichloroethylene 0.00080 U mg/kg dry 0.0044 0.00080 1 8260D 8/29/19 3:56 JLB P91-10480 1,1-Dichloropropylene 0.00067 U mg/kg dry 0.0044 0.00067 1 8260D 8/29/19 3:56 JLB P91-10480 1,2,3-Trichlorobenzene 0.00062 U mg/kg dry 0.0087 0.00062 1 8260D 8/29/19 3:56 JLB P91-10480 1,2,3-Trichloropropane 0.00050 U mg/kg dry 0.0044 0.00050 1 8260D 8/29/19 3:56 JLB P91-10480 1,2,4-Trichlorobenzene 0.00042 U mg/kg dry 0.0087 0.00042 1 8260D 8/29/19 3:56 JLB P91-10480 1,2,4-Trimethylbenzene 0.0032 J mg/kg dry 0.0044 0.00046 1 8260D 8/29/19 3:56 JLB P9H0480 1,2-Dibromoethane 0.00039 U mg/kg dry 0.0044 0.00039 1 8260D 8/29/19 3:56 JLB P91-10480 1,2-Dichlorobenzene 0.00049 U mg/kg dry 0.0044 0.00049 1 8260D 8/29/19 3:56 JLB P91-10480 1,2-Dichloroethane 0.00052 U mg/kg dry 0.0044 0.00052 1 8260D 8/29/19 3:56 JLB P91-10480 1,2-Dichloropropane 0.00066 U mg/kg dry 0.0044 0.00066 1 8260D 8/29/19 3:56 JLB P91-10480 1,3,5-Trimethylbenzene 0.0059 mg/kg dry 0.0044 0.00055 1 8260D 8/29/19 3:56 JLB P9H0480 1,3-Dichlorobenzene 0.00054 U mg/kg dry 0.0044 0.00054 1 8260D 8/29/19 3:56 JLB P91-10480 1,3-Dichloropropane 0.00036 U mg/kg dry 0.0044 0.00036 1 8260D 8/29/19 3:56 JLB P91-10480 1,4-Dichlorobenzene 0.00055 U mg/kg dry 0.0044 0.00055 1 8260D 8/29/19 3:56 JLB P91-10480 2,2-Dichloropropane 0.00054 U mg/kg dry 0.0044 0.00054 1 8260D 8/29/19 3:56 JLB P91-10480 2-Chlorotoluene 0.00058 U mg/kg dry 0.0044 0.00058 1 8260D 8/29/19 3:56 JLB P91-10480 4-Chlorotoluene 0.00050 U mg/kg dry 0.0044 0.00050 1 8260D 8/29/19 3:56 JLB P91-10480 4-Isopropyltoluene 0.016 mg/kg dry 0.0044 0.0011 1 8260D 8/29/19 3:56 JLB P9H0480 Acetone 0.029 mg/kg dry 0.017 0.0011 1 8260D 8/29/19 3:56 JLB P9H0480 Benzene 0.00068 U mg/kg dry 0.0044 0.00068 1 8260D 8/29/19 3:56 JLB P91-10480 Bromobenzene 0.00060 U mg/kg dry 0.0044 0.00060 1 8260D 8/29/19 3:56 JLB P91-10480 Bromochloromethane 0.00072 U mg/kg dry 0.0044 0.00072 1 8260D 8/29/19 3:56 JLB P91-10480 Bromodichloromethane 0.00041 U mg/kg dry 0.0044 0.00041 1 8260D 8/29/19 3:56 JLB P91-10480 Bromoform 0.00034 U mg/kg dry 0.0044 0.00034 1 8260D 8/29/19 3:56 JLB P91-10480 Bromomethane 0.0021 U mg/kg dry 0.0087 0.0021 1 8260D 8/29/19 3:56 JLB P91-10480 Carbon Tetrachloride 0.00086 U mg/kg dry 0.0044 0.00086 1 8260D 8/29/19 3:56 JLB P91-10480 Chlorobenzene 0.00068 U mg/kg dry 0.0044 0.00068 1 8260D 8/29/19 3:56 JLB P91-10480 Chloroethane 0.00083 U mg/kg dry 0.0087 0.00083 1 8260D 8/29/19 3:56 JLB P91-10480 Chloroform 0.00053 U mg/kg dry 0.0044 0.00053 1 8260D 8/29/19 3:56 JLB P91-10480 Chloromethane 0.0013 U mg/kg dry 0.0087 0.0013 1 8260D 8/29/19 3:56 JLB P91-10480 cis-1,2-Dichloroethylene 0.00069 U mg/kg dry 0.0044 0.00069 1 8260D 8/29/19 3:56 JLB P91-10480 cis-1,3-Dichloropropylene 0.00043 U mg/kg dry 0.0044 0.00043 1 8260D 8/29/19 3:56 JLB P91-10480 Dibromochloromethane 0.00029 U mg/kg dry 0.0044 0.00029 1 8260D 8/29/19 3:56 JLB P91-10480 Dichlorodifluoromethane 0.0012 U mg/kg dry 0.0087 0.0012 1 8260D 8/29/19 3:56 JLB P91-10480 Ethylbenzene 0.00066 U mg/kg dry 0.0044 0.00066 1 8260D 8/29/19 3:56 JLB P91-10480 Isopropyl Ether 0.00064 U mg/kg dry 0.0044 0.00064 1 8260D 8/29/19 3:56 JLB P91-10480 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 6 of 21 P R S M Laboratory Report Full -Service Analytical & Environmental Solutions 08/29/2019 LABORATORIES INC. Summit Engineering (Charlotte) Project: UNCC Client Sample ID: S-1 Attn: Michael Zavislak Prism Sample ID: 9080388-01 P.O. Box 7384 Prism Work Order: 9080388 Charlotte, NC 28241 Sample Matrix: Solid Time Collected: 08/27/19 15:00 Time Submitted: 08/27/19 15:45 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Date/Time Analyst Batch ID Isopropyl benzene (Cumene) 0.0049 mg/kg dry 0.0044 0.00051 1 8260D 8/29/19 3:56 JLB P9H0480 m,p-Xylenes 0.0011 U mg/kg dry 0.0087 0.0011 1 8260D 8/29/19 3:56 JLB P91-10480 Methyl Butyl Ketone (2-Hexanone) 0.00030 U mg/kg dry 0.017 0.00030 1 8260D 8/29/19 3:56 JLB P91-10480 Methyl Ethyl Ketone (2-Butanone) 0.0010 U mg/kg dry 0.017 0.0010 1 8260D 8/29/19 3:56 JLB P91-10480 Methyl Isobutyl Ketone 0.00036 U mg/kg dry 0.017 0.00036 1 8260D 8/29/19 3:56 JLB P91-10480 Methylene Chloride 0.00071 U mg/kg dry 0.0044 0.00071 1 8260D 8/29/19 3:56 JLB P91-10480 Methyl-tert-Butyl Ether 0.00061 U mg/kg dry 0.0044 0.00061 1 8260D 8/29/19 3:56 JLB P91-10480 Naphthalene 0.032 mg/kg dry 0.0087 0.00044 1 8260D 8/29/19 3:56 JLB P9H0480 n-Butylbenzene 0.034 mg/kg dry 0.0044 0.00041 1 8260D 8129/19 3:56 JLB P9H0480 n-Propylbenzene 0.0070 mg/kg dry 0.0044 0.00063 1 8260D 8/29/19 3:56 JLB P9H0480 o-Xylene 0.00046 U mg/kg dry 0.0044 0.00046 1 8260D 8/29/19 3:56 JLB P91-10480 sec-Butylbenzene 0.036 mg/kg dry 0.0044 0.00047 1 8260D 8/29/19 3:56 JLB P9H0480 Styrene 0.00042 U mg/kg dry 0.0044 0.00042 1 8260D 8/29/19 3:56 JLB P91-10480 tert-Butylbenzene 0.012 mg/kg dry 0.0044 0.00052 1 8260D 8/29/19 3:56 JLB P9H0480 Tetrachloroethylene 0.00079 U mg/kg dry 0.0044 0.00079 1 8260D 8/29/19 3:56 JLB P91-10480 Toluene 0.00069 U mg/kg dry 0.0044 0.00069 1 8260D 8/29/19 3:56 JLB P91-10480 trans-1,2-Dichloroethylene 0.00083 U mg/kg dry 0.0044 0.00083 1 8260D 8/29/19 3:56 JLB P91-10480 trans- 1,3-Dichloropropylene 0.00037 U mg/kg dry 0.0044 0.00037 1 8260D 8/29/19 3:56 JLB P91-10480 Trichloroethylene 0.00085 U mg/kg dry 0.0044 0.00085 1 8260D 8/29/19 3:56 JLB P91-10480 Trichlorofluoromethane 0.0012 U mg/kg dry 0.0087 0.0012 1 8260D 8/29/19 3:56 JLB P91-10480 Vinyl acetate 0.00047 U mg/kg dry 0.0087 0.00047 1 8260D 8/29/19 3:56 JLB P91-10480 Vinyl chloride 0.00086 U mg/kg dry 0.0087 0.00086 1 8260D 8/29/19 3:56 JLB P91-10480 Xylenes, total 0.0016 U mg/kg dry 0.013 0.0016 1 8260D 8/29/19 3:56 JLB P91-10480 Surrogate Recovery Control Limits 4-Bromofluorobenzene 96 % 70-130 Dibromofluoromethane 99 % 84-123 Toluene-d8 114 % 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 7 of 21 ,ot P R I IS M EService Analytical s Environmental Solutions LABORATORIES, INC. Level II QC Report 8/29/19 Summit Engineering (Charlotte) Project: UNCC Attn: Michael Zavislak P.O. Box 7384 Charlotte, NC 28241 Volatile Organic Compounds by GC/MS - Quality Control Prism Work Order: 9080388 Time Submitted: 8/27/2019 3:45:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9HO480 - 5035 Blank (P9H0480-BLK1) Prepared: 08/28/19 Analyzed: 08/29/19 1,1,1,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,1-Trichloroethane BRL 0.0050 mg/kg wet 1,1,2,2-Tetrachloroethane BRL 0.0050 mg/kg wet 1,1,2-Trichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethane BRL 0.0050 mg/kg wet 1,1-Dichloroethylene BRL 0.0050 mg/kg wet 1,1-Dichloropropylene BRL 0.0050 mg/kg wet 1,2,3-Trichlorobenzene BRL 0.010 mg/kg wet 1,2,3-Trichloropropane BRL 0.0050 mg/kg wet 1,2,4-Trichlorobenzene BRL 0.010 mg/kg wet 1,2,4-Trimethyl benzene BRL 0.0050 mg/kg wet 1,2-Dibromoethane BRL 0.0050 mg/kg wet 1,2-Dichlorobenzene BRL 0.0050 mg/kg wet 1,2-Dichloroethane BRL 0.0050 mg/kg wet 1,2-Dichloropropane BRL 0.0050 mg/kg wet 1,3,5-Trimethyl benzene BRL 0.0050 mg/kg wet 1,3-Dichlorobenzene BRL 0.0050 mg/kg wet 1,3-Dichloropropane BRL 0.0050 mg/kg wet 1,4-Dichlorobenzene BRL 0.0050 mg/kg wet 2,2-Dichloropropane BRL 0.0050 mg/kg wet 2-Chlorotoluene BRL 0.0050 mg/kg wet 4-Chlorotoluene BRL 0.0050 mg/kg wet 4-Isopropyltoluene BRL 0.0050 mg/kg wet Acetone BRL 0.020 mg/kg wet Benzene BRL 0.0050 mg/kg wet Bromobenzene BRL 0.0050 mg/kg wet Bromochloromethane BRL 0.0050 mg/kg wet Bromodichloromethane BRL 0.0050 mg/kg wet Bromoform BRL 0.0050 mg/kg wet Bromomethane BRL 0.010 mg/kg wet Carbon Tetrachloride BRL 0.0050 mg/kg wet Chlorobenzene BRL 0.0050 mg/kg wet Chloroethane BRL 0.010 mg/kg wet Chloroform BRL 0.0050 mg/kg wet Chloromethane BRL 0.010 mg/kg wet cis-1,2-Dichloroethylene BRL 0.0050 mg/kg wet cis-1,3-Dichloropropylene BRL 0.0050 mg/kg wet Dibromochloromethane BRL 0.0050 mg/kg wet Dichlorodifluoromethane BRL 0.010 mg/kg wet Ethylbenzene BRL 0.0050 mg/kg wet Isopropyl Ether BRL 0.0050 mg/kg wet Isopropylbenzene (Cumene) BRL 0.0050 mg/kg wet m,p-Xylenes BRL 0.010 mg/kg wet Methyl Butyl Ketone (2-Hexanone) BRL 0.020 mg/kg wet Methyl Ethyl Ketone (2-Butanone) BRL 0.020 mg/kg wet Methyl Isobutyl Ketone BRL 0.020 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 8 of 21 P R I S M Full -Service Analytical s Environmental Solutions LABOFATORIEs NC. Level II QC Report 8/29/19 Summit Engineering (Charlotte) Project: UNCC Attn: Michael Zavislak P.O. Box 7384 Charlotte, NC 28241 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P9HO480 - 5035 Reporting Result Limit Units Prism Work Order: 9080388 Time Submitted: 8/27/2019 3:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P9H0480-BLK1) Prepared: 08/28/19 Analyzed: 08/29/19 Methylene Chloride BRL 0.0050 mg/kg wet Methyl-tert-Butyl Ether BRL 0.0050 mg/kg wet Naphthalene BRL 0.010 mg/kg wet n-Butylbenzene BRL 0.0050 mg/kg wet n-Propylbenzene BRL 0.0050 mg/kg wet o-Xylene BRL 0.0050 mg/kg wet sec-Butylbenzene BRL 0.0050 mg/kg wet Styrene BRL 0.0050 mg/kg wet tert-Butyl benzene BRL 0.0050 mg/kg wet Tetrachloroethylene BRL 0.0050 mg/kg wet Toluene BRL 0.0050 mg/kg wet trans- 1,2-Dichloroethylene BRL 0.0050 mg/kg wet trans- 1,3-Dichloropropylene BRL 0.0050 mg/kg wet Trichloroethylene BRL 0.0050 mg/kg wet Trichlorofluoromethane BRL 0.010 mg/kg wet Vinyl acetate BRL 0.010 mg/kg wet Vinyl chloride BRL 0.010 mg/kg wet Xylenes, total BRL 0.015 mg/kg wet Surrogate:4-Bromofluorobenzene 49.7 ug/L 50.00 99 70-130 Surrogate: Dibromofluoromethane 51.6 ug/L 50.00 103 84-123 Surrogate: Toluene-d8 51.1 ug/L 50.00 102 76-129 LCS (P9HO480-BS1) Prepared: 08/28/19 Analyzed: 08/29/19 1,1,1,2-Tetrachloroethane 0.0520 0.0050 mg/kg wet 0.05000 104 72-115 1, 1,1 -Trichloroethane 0.0463 0.0050 mg/kg wet 0.05000 93 67-131 1,1,2,2-Tetrachloroethane 0.0492 0.0050 mg/kg wet 0.05000 98 56-126 1,1,2-Trichloroethane 0.0503 0.0050 mg/kg wet 0.05000 101 70-133 1,1-Dichloroethane 0.0490 0.0050 mg/kg wet 0.05000 98 74-127 1,1-Dichloroethylene 0.0453 0.0050 mg/kg wet 0.05000 91 67-149 1, 1 -Dichloropropylene 0.0472 0.0050 mg/kg wet 0.05000 94 71-130 1,2,3-Trichlorobenzene 0.0521 0.010 mg/kg wet 0.05000 104 68-130 1,2,3-Trichloropropane 0.0509 0.0050 mg/kg wet 0.05000 102 60-137 1,2,4-Trichlorobenzene 0.0492 0.010 mg/kg wet 0.05000 98 66-125 1,2,4-Trimethylbenzene 0.0481 0.0050 mg/kg wet 0.05000 96 69-129 1,2-Dibromoethane 0.0512 0.0050 mg/kg wet 0.05000 102 70-132 1,2-Dichlorobenzene 0.0498 0.0050 mg/kg wet 0.05000 100 72-123 1,2-Dichloroethane 0.0482 0.0050 mg/kg wet 0.05000 96 68-128 1,2-Dichloropropane 0.0495 0.0050 mg/kg wet 0.05000 99 73-130 1,3,5-Trimethylbenzene 0.0479 0.0050 mg/kg wet 0.05000 96 69-128 1,3-Dichlorobenzene 0.0489 0.0050 mg/kg wet 0.05000 98 71-120 1,3-Dichloropropane 0.0511 0.0050 mg/kg wet 0.05000 102 75-124 1,4-Dichlorobenzene 0.0491 0.0050 mg/kg wet 0.05000 98 71-123 2,2-Dichloropropane 0.0462 0.0050 mg/kg wet 0.05000 92 50-142 2-Chlorotoluene 0.0488 0.0050 mg/kg wet 0.05000 98 67-124 4-Chlorotoluene 0.0486 0.0050 mg/kg wet 0.05000 97 71-126 4-Isopropyltoluene 0.0492 0.0050 mg/kg wet 0.05000 98 68-129 Acetone 0.0969 0.020 mg/kg wet 0.1000 97 29-198 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 9 of 21 P R I S M Full -Service Analytical s Environmental Solutions LABOFATORIEs NC. Level II QC Report 8/29/19 Summit Engineering (Charlotte) Project: UNCC Attn: Michael Zavislak P.O. Box 7384 Charlotte, NC 28241 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P9HO480 - 5035 Reporting Result Limit Units Prism Work Order: 9080388 Time Submitted: 8/27/2019 3:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P91-10480-13SI) Prepared: 08/28/19 Analyzed: 08/29/19 Benzene 0.0480 0.0050 mg/kg wet 0.05000 96 74-127 Bromobenzene 0.0496 0.0050 mg/kg wet 0.05000 99 73-125 Bromochloromethane 0.0489 0.0050 mg/kg wet 0.05000 98 72-134 Bromodichloromethane 0.0484 0.0050 mg/kg wet 0.05000 97 75-122 Bromoform 0.0528 0.0050 mg/kg wet 0.05000 106 66-135 Bromomethane 0.0569 0.010 mg/kg wet 0.05000 114 20-180 Carbon Tetrachloride 0.0467 0.0050 mg/kg wet 0.05000 93 64-143 Chlorobenzene 0.0491 0.0050 mg/kg wet 0.05000 98 74-118 Chloroethane 0.0412 0.010 mg/kg wet 0.05000 82 33-149 Chloroform 0.0478 0.0050 mg/kg wet 0.05000 96 73-127 Chloromethane 0.0426 0.010 mg/kg wet 0.05000 85 45-143 cis-1,2-Dichloroethylene 0.0471 0.0050 mg/kg wet 0.05000 94 76-134 cis-1,3-Dichloropropylene 0.0486 0.0050 mg/kg wet 0.05000 97 71-125 Dibromochloromethane 0.0515 0.0050 mg/kg wet 0.05000 103 73-122 Dichlorodifluoromethane 0.0477 0.010 mg/kg wet 0.05000 95 26-146 Ethylbenzene 0.0492 0.0050 mg/kg wet 0.05000 98 74-128 Isopropyl Ether 0.0463 0.0050 mg/kg wet 0.05000 93 59-159 Isopropylbenzene (Cumene) 0.0492 0.0050 mg/kg wet 0.05000 98 68-126 m,p-Xylenes 0.0990 0.010 mg/kg wet 0.1000 99 75-124 Methyl Butyl Ketone (2-Hexanone) 0.0500 0.020 mg/kg wet 0.05000 100 61-157 Methyl Ethyl Ketone (2-Butanone) 0.0472 0.020 mg/kg wet 0.05000 94 63-149 Methyl Isobutyl Ketone 0.0481 0.020 mg/kg wet 0.05000 96 57-162 Methylene Chloride 0.0468 0.0050 mg/kg wet 0.05000 94 74-129 Methyl-tert-Butyl Ether 0.0511 0.0050 mg/kg wet 0.05000 102 70-130 Naphthalene 0.0510 0.010 mg/kg wet 0.05000 102 57-157 n-Butylbenzene 0.0484 0.0050 mg/kg wet 0.05000 97 65-135 n-Propylbenzene 0.0487 0.0050 mg/kg wet 0.05000 97 67-130 o-Xylene 0.0488 0.0050 mg/kg wet 0.05000 97 74-126 sec-Butylbenzene 0.0484 0.0050 mg/kg wet 0.05000 97 66-131 Styrene 0.0504 0.0050 mg/kg wet 0.05000 101 77-121 tert-Butyl benzene 0.0490 0.0050 mg/kg wet 0.05000 98 67-132 Tetrachloroethylene 0.0481 0.0050 mg/kg wet 0.05000 96 68-130 Toluene 0.0478 0.0050 mg/kg wet 0.05000 96 71-129 trans- 1,2-Dichloroethylene 0.0461 0.0050 mg/kg wet 0.05000 92 73-132 trans- 1,3-Dichloropropylene 0.0502 0.0050 mg/kg wet 0.05000 100 68-123 Trichloroethylene 0.0472 0.0050 mg/kg wet 0.05000 94 75-133 Trichlorofluoromethane 0.0420 0.010 mg/kg wet 0.05000 84 44-146 Vinyl acetate 0.0476 0.010 mg/kg wet 0.05000 95 85-161 Vinyl chloride 0.0466 0.010 mg/kg wet 0.05000 93 48-147 Xylenes, total 0.148 0.015 mg/kg wet 0.1500 98 74-126 Surrogate:4-Bromofluorobenzene 50.2 ug/L 50.00 100 70-130 Surrogate: Dibromofluoromethane 49.6 ug/L 50.00 99 84-123 Surrogate: Toluene-d8 49.9 ug/L 50.00 100 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 10 of 21 P R I S M Full -Service Analytical s Environmental Solutions LABOFATORIEs NC. Level II QC Report 8/29/19 Summit Engineering (Charlotte) Project: UNCC Attn: Michael Zavislak P.O. Box 7384 Charlotte, NC 28241 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P9HO480 - 5035 Reporting Result Limit Units Prism Work Order: 9080388 Time Submitted: 8/27/2019 3:45:OOPM Spike Source Level Result %REC %REC RPD Limits RPD Limit Notes LCS Dup (P9HO480-BSD1) Prepared: 08/28/19 Analyzed: 08/29/19 1,1,1,2-Tetrachloroethane 0.0537 0.0050 mg/kg wet 0.05000 107 72-115 3 20 1, 1,1 -Trichloroethane 0.0465 0.0050 mg/kg wet 0.05000 93 67-131 0.5 20 1,1,2,2-Tetrachloroethane 0.0526 0.0050 mg/kg wet 0.05000 105 56-126 7 20 1,1,2-Trichloroethane 0.0525 0.0050 mg/kg wet 0.05000 105 70-133 4 20 1,1-Dichloroethane 0.0496 0.0050 mg/kg wet 0.05000 99 74-127 1 20 1,1-Dichloroethylene 0.0458 0.0050 mg/kg wet 0.05000 92 67-149 1 20 1, 1 -Dichloropropylene 0.0479 0.0050 mg/kg wet 0.05000 96 71-130 1 20 1,2,3-Trichlorobenzene 0.0545 0.010 mg/kg wet 0.05000 109 68-130 5 20 1,2,3-Trichloropropane 0.0549 0.0050 mg/kg wet 0.05000 110 60-137 8 20 1,2,4-Trichlorobenzene 0.0510 0.010 mg/kg wet 0.05000 102 66-125 4 20 1,2,4-Trimethylbenzene 0.0484 0.0050 mg/kg wet 0.05000 97 69-129 0.7 20 1,2-Dibromoethane 0.0535 0.0050 mg/kg wet 0.05000 107 70-132 4 20 1,2-Dichlorobenzene 0.0511 0.0050 mg/kg wet 0.05000 102 72-123 2 20 1,2-Dichloroethane 0.0507 0.0050 mg/kg wet 0.05000 101 68-128 5 20 1,2-Dichloropropane 0.0505 0.0050 mg/kg wet 0.05000 101 73-130 2 20 1,3,5-Trimethylbenzene 0.0486 0.0050 mg/kg wet 0.05000 97 69-128 1 20 1,3-Dichlorobenzene 0.0501 0.0050 mg/kg wet 0.05000 100 71-120 2 20 1,3-Dichloropropane 0.0533 0.0050 mg/kg wet 0.05000 107 75-124 4 20 1,4-Dichlorobenzene 0.0501 0.0050 mg/kg wet 0.05000 100 71-123 2 20 2,2-Dichloropropane 0.0463 0.0050 mg/kg wet 0.05000 93 50-142 0.3 20 2-Chlorotoluene 0.0495 0.0050 mg/kg wet 0.05000 99 67-124 1 20 4-Chlorotoluene 0.0492 0.0050 mg/kg wet 0.05000 98 71-126 1 20 4-Isopropyltoluene 0.0493 0.0050 mg/kg wet 0.05000 99 68-129 0.2 20 Acetone 0.107 0.020 mg/kg wet 0.1000 107 29-198 10 20 Benzene 0.0488 0.0050 mg/kg wet 0.05000 98 74-127 2 20 Bromobenzene 0.0512 0.0050 mg/kg wet 0.05000 102 73-125 3 20 Bromochloromethane 0.0509 0.0050 mg/kg wet 0.05000 102 72-134 4 20 Bromodichloromethane 0.0500 0.0050 mg/kg wet 0.05000 100 75-122 3 20 Bromoform 0.0555 0.0050 mg/kg wet 0.05000 111 66-135 5 20 Bromomethane 0.0586 0.010 mg/kg wet 0.05000 117 20-180 3 20 Carbon Tetrachloride 0.0470 0.0050 mg/kg wet 0.05000 94 64-143 0.7 20 Chlorobenzene 0.0497 0.0050 mg/kg wet 0.05000 99 74-118 1 20 Chloroethane 0.0417 0.010 mg/kg wet 0.05000 83 33-149 1 20 Chloroform 0.0489 0.0050 mg/kg wet 0.05000 98 73-127 2 20 Chloromethane 0.0425 0.010 mg/kg wet 0.05000 85 45-143 0.2 20 cis-1,2-Dichloroethylene 0.0484 0.0050 mg/kg wet 0.05000 97 76-134 3 20 cis-1,3-Dichloropropylene 0.0507 0.0050 mg/kg wet 0.05000 101 71-125 4 20 Dibromochloromethane 0.0533 0.0050 mg/kg wet 0.05000 107 73-122 3 20 Dichlorodifluoromethane 0.0478 0.010 mg/kg wet 0.05000 96 26-146 0.2 20 Ethylbenzene 0.0494 0.0050 mg/kg wet 0.05000 99 74-128 0.5 20 Isopropyl Ether 0.0480 0.0050 mg/kg wet 0.05000 96 59-159 3 20 Isopropylbenzene (Cumene) 0.0494 0.0050 mg/kg wet 0.05000 99 68-126 0.4 20 m,p-Xylenes 0.0999 0.010 mg/kg wet 0.1000 100 75-124 0.9 20 Methyl Butyl Ketone (2-Hexanone) 0.0552 0.020 mg/kg wet 0.05000 110 61-157 10 20 Methyl Ethyl Ketone (2-Butanone) 0.0522 0.020 mg/kg wet 0.05000 104 63-149 10 20 Methyl Isobutyl Ketone 0.0529 0.020 mg/kg wet 0.05000 106 57-162 9 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 11 of 21 P R I IS M Full -Service Analytical Environmental Solutions . LABORATORIES, INC. Level II QC Report 8/29/19 Summit Engineering (Charlotte) Project: UNCC Attn: Michael Zavislak P.O. Box 7384 Charlotte, NC 28241 Volatile Organic Compounds by GC/MS - Quality Control Analyte Batch P9HO480 - 5035 Reporting Result Limit Units Prism Work Order: 9080388 Time Submitted: 8/27/2019 3:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (P9H0480-BSD1) Prepared: 08/28/19 Analyzed: 08/29/19 Methylene Chloride 0.0479 0.0050 mg/kg wet 0.05000 96 74-129 2 20 Methyl-tert-Butyl Ether 0.0543 0.0050 mg/kg wet 0.05000 109 70-130 6 20 Naphthalene 0.0549 0.010 mg/kg wet 0.05000 110 57-157 7 20 n-Butylbenzene 0.0483 0.0050 mg/kg wet 0.05000 97 65-135 0.2 20 n-Propylbenzene 0.0491 0.0050 mg/kg wet 0.05000 98 67-130 0.9 20 o-Xylene 0.0494 0.0050 mg/kg wet 0.05000 99 74-126 1 20 sec-Butylbenzene 0.0486 0.0050 mg/kg wet 0.05000 97 66-131 0.5 20 Styrene 0.0510 0.0050 mg/kg wet 0.05000 102 77-121 1 20 tert-Butylbenzene 0.0493 0.0050 mg/kg wet 0.05000 99 67-132 0.7 20 Tetrachloroethylene 0.0480 0.0050 mg/kg wet 0.05000 96 68-130 0.1 20 Toluene 0.0482 0.0050 mg/kg wet 0.05000 96 71-129 1 20 trans-1,2-Dichloroethylene 0.0465 0.0050 mg/kg wet 0.05000 93 73-132 0.8 20 trans-1,3-Dichloropropylene 0.0524 0.0050 mg/kg wet 0.05000 105 68-123 4 20 Trichloroethylene 0.0477 0.0050 mg/kg wet 0.05000 95 75-133 1 20 Trichlorofluoromethane 0.0421 0.010 mg/kg wet 0.05000 84 44-146 0.2 20 Vinyl acetate 0.0518 0.010 mg/kg wet 0.05000 104 85-161 8 20 Vinyl chloride 0.0468 0.010 mg/kg wet 0.05000 94 48-147 0.3 20 Xylenes, total 0.149 0.015 mg/kg wet 0.1500 100 74-126 1 20 Surrogate:4-Bromofluorobenzene 49.7 ug/L 50.00 99 70-130 Surrogate: Dibromofluoromethane 50.9 ug/L 50.00 102 84-123 Surrogate: Toluene-d8 49.7 ug/L 50.00 99 76-129 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 12 of 21 P R I IS M Full -Service Analytical Environmental Solutions . LABORATORIES, INC. Level II QC Report 8/29/19 Summit Engineering (Charlotte) Project: UNCC Attn: Michael Zavislak P.O. Box 7384 Charlotte, NC 28241 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P9HO462 - 3546 Reporting Result Limit Units Prism Work Order: 9080388 Time Submitted: 8/27/2019 3:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes Blank (P9H0462-BLK1) Prepared & Analyzed: 08/28/19 1,2,4-Trichlorobenzene BRL 0.66 mg/kg wet 1,2-Dichlorobenzene BRL 0.66 mg/kg wet 1,3-Dichlorobenzene BRL 0.66 mg/kg wet 1,4-Dichlorobenzene BRL 0.33 mg/kg wet 2,4,5-Trichlorophenol BRL 0.66 mg/kg wet 2,4,6-Trichlorophenol BRL 0.66 mg/kg wet 2,4-Dichlorophenol BRL 0.66 mg/kg wet 2,4-Dimethylphenol BRL 0.33 mg/kg wet 2,4-Dinitrophenol BRL 1.5 mg/kg wet 2,4-Dinitrotoluene BRL 0.66 mg/kg wet 2,6-Dinitrotoluene BRL 0.66 mg/kg wet 2-Chloronaphthalene BRL 0.66 mg/kg wet 2-Chlorophenol BRL 0.66 mg/kg wet 2-Methyl naphthalene BRL 0.66 mg/kg wet 2-Methylphenol BRL 0.66 mg/kg wet 2-Nitroaniline BRL 0.66 mg/kg wet 2-Nitrophenol BRL 0.66 mg/kg wet 3,3'-Dichlorobenzidine BRL 0.66 mg/kg wet 3/4-Methyl phenol BRL 0.66 mg/kg wet 3-Nitroaniline BRL 0.66 mg/kg wet 4,6-Dinitro-2-methylphenol BRL 1.5 mg/kg wet 4-Bromophenyl phenyl ether BRL 0.66 mg/kg wet 4-Chloro-3-methylphenol BRL 0.66 mg/kg wet 4-Chloroaniline BRL 0.33 mg/kg wet 4-Chlorophenyl phenyl ether BRL 1.0 mg/kg wet 4-Nitroaniline BRL 0.33 mg/kg wet 4-Nitrophenol BRL 0.66 mg/kg wet Acenaphthene BRL 0.66 mg/kg wet Acenaphthylene BRL 0.66 mg/kg wet Aniline BRL 0.66 mg/kg wet Anthracene BRL 0.66 mg/kg wet Azobenzene BRL 0.66 mg/kg wet Benzo(a)anthracene BRL 0.66 mg/kg wet Benzo(a)pyrene BRL 0.66 mg/kg wet Benzo(b)fluoranthene BRL 0.66 mg/kg wet Benzo(g,h,i)perylene BRL 0.66 mg/kg wet Benzo(k)fluoranthene BRL 0.66 mg/kg wet Benzoic Acid BRL 2.0 mg/kg wet Benzyl alcohol BRL 0.66 mg/kg wet bis(2-Chloroethoxy)methane BRL 0.66 mg/kg wet Bis(2-Chloroethyl)ether BRL 0.66 mg/kg wet Bis(2-chloroisopropyl)ether BRL 0.33 mg/kg wet Bis(2-Ethylhexyl)phthalate BRL 0.66 mg/kg wet Butyl benzyl phthalate BRL 0.33 mg/kg wet Chrysene BRL 0.66 mg/kg wet Dibenzo(a,h)anthracene BRL 0.66 mg/kg wet This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 13 of 21 P R I IS M Full -Service Analytical Environmental Solutions . LABORATORIES, INC. Level II QC Report 8/29/19 Summit Engineering (Charlotte) Project: UNCC Attn: Michael Zavislak P.O. Box 7384 Charlotte, NC 28241 Semivolatile Organic Compounds by GC/MS - Quality Control Prism Work Order: 9080388 Time Submitted: 8/27/2019 3:45:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9HO462 - 3546 Blank (P9H0462-BLK1) Prepared & Analyzed: 08/28/19 Dibenzofuran BRL 0.66 mg/kg wet Diethyl phthalate BRL 0.66 mg/kg wet Dimethyl phthalate BRL 0.66 mg/kg wet Di-n-butyl phthalate BRL 0.66 mg/kg wet Di-n-octyl phthalate BRL 0.33 mg/kg wet Fluoranthene BRL 0.66 mg/kg wet Fluorene BRL 0.66 mg/kg wet Hexachlorobenzene BRL 0.66 mg/kg wet Hexachlorobutadiene BRL 0.66 mg/kg wet Hexachlorocyclopentadiene BRL 0.66 mg/kg wet Hexachloroethane BRL 0.66 mg/kg wet Indeno(1,2,3-cd)pyrene BRL 0.66 mg/kg wet Isophorone BRL 0.66 mg/kg wet Naphthalene BRL 0.66 mg/kg wet Nitrobenzene BRL 0.33 mg/kg wet N-Nitroso-di-n-propylamine BRL 0.66 mg/kg wet N-Nitrosodiphenylamine BRL 0.66 mg/kg wet Pentachlorophenol BRL 1.0 mg/kg wet Phenanthrene BRL 0.66 mg/kg wet Phenol BRL 0.66 mg/kg wet Pyrene BRL 0.66 mg/kg wet Surrogate: 2,4,6-Tribromophenol 1.95 mg/kg wet 3.333 59 39-132 Surrogate: 2-Fluorobiphenyl 1.05 mg/kg wet 1.667 63 44-115 Surrogate: 2-Fluorophenol 2.12 mg/kg wet 3.333 64 35-115 Surrogate: Nitrobenzene-d5 0.976 mg/kg wet 1.667 59 37-122 Surrogate: Phenol-d5 1.99 mg/kg wet 3.333 60 34-121 Surrogate: Terphenyl-d14 1.11 mg/kg wet 1.667 66 54-127 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 14 of 21 P R I IS M Full -Service Analytical Environmental Solutions . LABORATORIES, INC. Level II QC Report 8/29/19 Summit Engineering (Charlotte) Project: UNCC Attn: Michael Zavislak P.O. Box 7384 Charlotte, NC 28241 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P9HO462 - 3546 Reporting Result Limit Units Prism Work Order: 9080388 Time Submitted: 8/27/2019 3:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P9H0462-BSI) Prepared &Analyzed: 08/28/19 1,2,4-Trichlorobenzene 0.932 0.66 mg/kg wet 1.667 56 34-118 1,2-Dichlorobenzene 0.919 0.66 mg/kg wet 1.667 55 33-117 1,3-Dichlorobenzene 0.868 0.66 mg/kg wet 1.667 52 30-115 1,4-Dichlorobenzene 0.893 0.33 mg/kg wet 1.667 54 31-115 2,4,5-Trichlorophenol 1.17 0.66 mg/kg wet 1.667 70 41-124 2,4,6-Trichlorophenol 1.17 0.66 mg/kg wet 1.667 70 39-126 2,4-Dichlorophenol 1.08 0.66 mg/kg wet 1.667 65 40-122 2,4-Dimethylphenol 1.21 0.33 mg/kg wet 1.667 72 30-127 2,4-Dinitrophenol 0.431 1.5 mg/kg wet 1.667 26 27-129 L, J 2,4-Dinitrotoluene 1.26 0.66 mg/kg wet 1.667 76 48-126 2,6-Dinitrotoluene 1.28 0.66 mg/kg wet 1.667 77 46-124 2-Chloronaphthalene 1.11 0.66 mg/kg wet 1.667 66 41-114 2-Chlorophenol 1.06 0.66 mg/kg wet 1.667 64 34-121 2-Methyl naphthalene 0.955 0.66 mg/kg wet 1.667 57 38-122 2-Methylphenol 1.07 0.66 mg/kg wet 1.667 64 32-122 2-Nitroaniline 1.06 0.66 mg/kg wet 1.667 64 44-127 2-Nitrophenol 0.964 0.66 mg/kg wet 1.667 58 36-123 3,3'-Dichlorobenzidine 1.20 0.66 mg/kg wet 1.667 72 22-121 3/4-Methyl phenol 1.07 0.66 mg/kg wet 1.667 64 34-119 3-Nitroaniline 1.01 0.66 mg/kg wet 1.667 60 33-119 4,6-Dinitro-2-methylphenol 0.968 1.5 mg/kg wet 1.667 58 29-132 J 4-Bromophenyl phenyl ether 1.20 0.66 mg/kg wet 1.667 72 46-124 4-Chloro-3-methylphenol 1.15 0.66 mg/kg wet 1.667 69 45-122 4-Chloroaniline 0.889 0.33 mg/kg wet 1.667 53 17-106 4-Chlorophenyl phenyl ether 1.17 1.0 mg/kg wet 1.667 70 45-121 4-Nitroaniline 1.05 0.33 mg/kg wet 1.667 63 63-147 4-Nitrophenol 1.32 0.66 mg/kg wet 1.667 79 30-132 Acenaphthene 1.11 0.66 mg/kg wet 1.667 67 40-123 Acenaphthylene 1.12 0.66 mg/kg wet 1.667 67 32-132 Aniline 0.924 0.66 mg/kg wet 1.667 55 12-197 Anthracene 1.21 0.66 mg/kg wet 1.667 73 47-123 Azobenzene 0.982 0.66 mg/kg wet 1.667 59 39-125 Benzo(a)anthracene 1.18 0.66 mg/kg wet 1.667 71 49-126 Benzo(a)pyrene 1.19 0.66 mg/kg wet 1.667 71 45-129 Benzo(b)fluoranthene 1.19 0.66 mg/kg wet 1.667 72 45-132 Benzo(g,hJ)perylene 1.23 0.66 mg/kg wet 1.667 74 43-134 Benzo(k)fluoranthene 1.18 0.66 mg/kg wet 1.667 71 47-132 Benzoic Acid BRL 2.0 mg/kg wet 1.667 10-83 L Benzyl alcohol 1.19 0.66 mg/kg wet 1.667 71 29-122 bis(2-Chloroethoxy)methane 0.954 0.66 mg/kg wet 1.667 57 36-121 Bis(2-Chloroethyl)ether 1.05 0.66 mg/kg wet 1.667 63 31-120 Bis(2-chloroisopropyl)ether 0.932 0.33 mg/kg wet 1.667 56 33-131 Bis(2-Ethylhexyl)phthalate 1.18 0.66 mg/kg wet 1.667 71 51-133 Butyl benzyl phthalate 1.13 0.33 mg/kg wet 1.667 68 48-132 Chrysene 1.14 0.66 mg/kg wet 1.667 68 50-124 Dibenzo(a,h)anthracene 0.993 0.66 mg/kg wet 1.667 60 45-134 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 15 of 21 P R I IS M Full -Service Analytical Environmental Solutions . LABORATORIES, INC. Level II QC Report 8/29/19 Summit Engineering (Charlotte) Project: UNCC Attn: Michael Zavislak P.O. Box 7384 Charlotte, NC 28241 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P9HO462 - 3546 Reporting Result Limit Units Prism Work Order: 9080388 Time Submitted: 8/27/2019 3:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS (P9H0462-BSI) Prepared &Analyzed: 08/28/19 Dibenzofuran 1.08 0.66 mg/kg wet 1.667 65 44-120 Diethyl phthalate 1.15 0.66 mg/kg wet 1.667 69 50-124 Dimethyl phthalate 1.11 0.66 mg/kg wet 1.667 67 48-124 Di-n-butyl phthalate 1.16 0.66 mg/kg wet 1.667 70 51-128 Di-n-octyl phthalate 1.20 0.33 mg/kg wet 1.667 72 45-140 Fluoranthene 1.22 0.66 mg/kg wet 1.667 73 50-127 Fluorene 1.19 0.66 mg/kg wet 1.667 71 43-125 Hexachlorobenzene 1.15 0.66 mg/kg wet 1.667 69 45-122 Hexachlorobutadiene 0.980 0.66 mg/kg wet 1.667 59 32-123 Hexachlorocyclopentadiene 0.908 0.66 mg/kg wet 1.667 54 32-117 Hexachloroethane 0.859 0.66 mg/kg wet 1.667 52 28-117 Indeno(1,2,3-cd)pyrene 1.40 0.66 mg/kg wet 1.667 84 45-133 Isophorone 1.02 0.66 mg/kg wet 1.667 61 30-122 Naphthalene 0.898 0.66 mg/kg wet 1.667 54 35-123 Nitrobenzene 0.917 0.33 mg/kg wet 1.667 55 34-122 N-Nitroso-di-n-propylamine 1.08 0.66 mg/kg wet 1.667 65 36-120 N-Nitrosodiphenylamine 1.42 0.66 mg/kg wet 1.667 85 38-127 Pentachlorophenol 0.853 1.0 mg/kg wet 1.667 51 25-133 J Phenanthrene 1.19 0.66 mg/kg wet 1.667 72 50-121 Phenol 1.06 0.66 mg/kg wet 1.667 64 34-121 Pyrene 1.18 0.66 mg/kg wet 1.667 71 47-127 Surrogate: 2,4,6-Tribromophenol 2.43 mg/kg wet 3.333 73 39-132 Surrogate: 2-Fluorobiphenyl 1.08 mg/kg wet 1.667 65 44-115 Surrogate: 2-Fluorophenol 2.07 mg/kg wet 3.333 62 35-115 Surrogate: Nitrobenzene-d5 0.903 mg/kg wet 1.667 54 37-122 Surrogate: Phenol-d5 2.00 mg/kg wet 3.333 60 34-121 Surrogate: Terphenyl-d14 1.11 mg/kg wet 1.667 66 54-127 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 16 of 21 P R I IS M Full -Service Analytical Environmental Solutions . LABORATORIES, INC. Level II QC Report 8/29/19 Summit Engineering (Charlotte) Project: UNCC Attn: Michael Zavislak P.O. Box 7384 Charlotte, NC 28241 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P9HO462 - 3546 Reporting Result Limit Units Prism Work Order: 9080388 Time Submitted: 8/27/2019 3:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (P9HO462-BSD1) Prepared & Analyzed: 08/28/19 1,2,4-Trichlorobenzene 0.916 0.66 mg/kg wet 1.667 55 34-118 2 20 1,2-Dichlorobenzene 0.916 0.66 mg/kg wet 1.667 55 33-117 0.4 20 1,3-Dichlorobenzene 0.892 0.66 mg/kg wet 1.667 53 30-115 3 20 1,4-Dichlorobenzene 0.908 0.33 mg/kg wet 1.667 54 31-115 2 20 2,4,5-Trichlorophenol 1.10 0.66 mg/kg wet 1.667 66 41-124 7 20 2,4,6-Trichlorophenol 1.11 0.66 mg/kg wet 1.667 66 39-126 5 20 2,4-Dichlorophenol 1.08 0.66 mg/kg wet 1.667 65 40-122 0.6 20 2,4-Dimethylphenol 1.15 0.33 mg/kg wet 1.667 69 30-127 5 20 2,4-Dinitrophenol 0.406 1.5 mg/kg wet 1.667 24 27-129 6 20 L, J 2,4-Dinitrotoluene 1.19 0.66 mg/kg wet 1.667 71 48-126 6 20 2,6-Dinitrotoluene 1.24 0.66 mg/kg wet 1.667 75 46-124 3 20 2-Chloronaphthalene 1.06 0.66 mg/kg wet 1.667 63 41-114 5 20 2-Chlorophenol 1.05 0.66 mg/kg wet 1.667 63 34-121 1 20 2-Methyl naphthalene 0.940 0.66 mg/kg wet 1.667 56 38-122 2 20 2-Methylphenol 1.05 0.66 mg/kg wet 1.667 63 32-122 2 20 2-Nitroaniline 0.987 0.66 mg/kg wet 1.667 59 44-127 7 20 2-Nitrophenol 0.948 0.66 mg/kg wet 1.667 57 36-123 2 20 3,3'-Dichlorobenzidine 1.13 0.66 mg/kg wet 1.667 68 22-121 6 20 3/4-Methyl phenol 1.02 0.66 mg/kg wet 1.667 61 34-119 4 20 3-Nitroaniline 0.927 0.66 mg/kg wet 1.667 56 33-119 8 20 4,6-Dinitro-2-methylphenol 0.899 1.5 mg/kg wet 1.667 54 29-132 7 20 J 4-Bromophenyl phenyl ether 1.09 0.66 mg/kg wet 1.667 65 46-124 10 20 4-Chloro-3-methylphenol 1.08 0.66 mg/kg wet 1.667 65 45-122 6 20 4-Chloroaniline 0.834 0.33 mg/kg wet 1.667 50 17-106 6 20 4-Chlorophenyl phenyl ether 1.10 1.0 mg/kg wet 1.667 66 45-121 6 20 4-Nitroaniline 0.958 0.33 mg/kg wet 1.667 57 63-147 9 20 L2 4-Nitrophenol 1.25 0.66 mg/kg wet 1.667 75 30-132 5 20 Acenaphthene 1.04 0.66 mg/kg wet 1.667 62 40-123 7 20 Acenaphthylene 1.05 0.66 mg/kg wet 1.667 63 32-132 6 20 Aniline 0.931 0.66 mg/kg wet 1.667 56 12-197 0.7 20 Anthracene 1.13 0.66 mg/kg wet 1.667 68 47-123 7 20 Azobenzene 0.897 0.66 mg/kg wet 1.667 54 39-125 9 20 Benzo(a)anthracene 1.08 0.66 mg/kg wet 1.667 65 49-126 9 20 Benzo(a)pyrene 1.12 0.66 mg/kg wet 1.667 67 45-129 6 20 Benzo(b)fluoranthene 1.14 0.66 mg/kg wet 1.667 68 45-132 5 20 Benzo(g,hJ)perylene 1.14 0.66 mg/kg wet 1.667 69 43-134 8 20 Benzo(k)fluoranthene 1.08 0.66 mg/kg wet 1.667 65 47-132 9 20 Benzoic Acid BRL 2.0 mg/kg wet 1.667 10-83 20 L Benzyl alcohol 1.13 0.66 mg/kg wet 1.667 68 29-122 5 20 bis(2-Chloroethoxy)methane 0.950 0.66 mg/kg wet 1.667 57 36-121 0.4 20 Bis(2-Chloroethyl)ether 1.00 0.66 mg/kg wet 1.667 60 31-120 4 20 Bis(2-chloroisopropyl)ether 0.911 0.33 mg/kg wet 1.667 55 33-131 2 20 Bis(2-Ethylhexyl)phthalate 1.08 0.66 mg/kg wet 1.667 64 51-133 9 20 Butyl benzyl phthalate 1.03 0.33 mg/kg wet 1.667 62 48-132 10 20 Chrysene 1.03 0.66 mg/kg wet 1.667 62 50-124 10 20 Dibenzo(a,h)anthracene 0.912 0.66 mg/kg wet 1.667 55 45-134 8 20 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 17 of 21 P R I IS M Full -Service Analytical Environmental Solutions . LABORATORIES, INC. Level II QC Report 8/29/19 Summit Engineering (Charlotte) Project: UNCC Attn: Michael Zavislak P.O. Box 7384 Charlotte, NC 28241 Semivolatile Organic Compounds by GC/MS - Quality Control Analyte Batch P9HO462 - 3546 Reporting Result Limit Units Prism Work Order: 9080388 Time Submitted: 8/27/2019 3:45:OOPM Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes LCS Dup (P9H0462-BSD1) Prepared & Analyzed: 08/28/19 Dibenzofuran 1.02 0.66 mg/kg wet 1.667 61 44-120 6 20 Diethyl phthalate 1.07 0.66 mg/kg wet 1.667 64 50-124 7 20 Dimethyl phthalate 1.05 0.66 mg/kg wet 1.667 63 48-124 5 20 Di-n-butyl phthalate 1.07 0.66 mg/kg wet 1.667 64 51-128 8 20 Di-n-octyl phthalate 1.11 0.33 mg/kg wet 1.667 67 45-140 8 20 Fluoranthene 1.12 0.66 mg/kg wet 1.667 67 50-127 8 20 Fluorene 1.11 0.66 mg/kg wet 1.667 67 43-125 7 20 Hexachlorobenzene 1.05 0.66 mg/kg wet 1.667 63 45-122 9 20 Hexachlorobutadiene 0.981 0.66 mg/kg wet 1.667 59 32-123 0.1 20 Hexachlorocyclopentadiene 0.822 0.66 mg/kg wet 1.667 49 32-117 10 20 Hexachloroethane 0.886 0.66 mg/kg wet 1.667 53 28-117 3 20 Indeno(1,2,3-cd)pyrene 1.30 0.66 mg/kg wet 1.667 78 45-133 8 20 Isophorone 0.977 0.66 mg/kg wet 1.667 59 30-122 4 20 Naphthalene 0.896 0.66 mg/kg wet 1.667 54 35-123 0.2 20 Nitrobenzene 0.907 0.33 mg/kg wet 1.667 54 34-122 1 20 N-Nitroso-di-n-propylamine 1.06 0.66 mg/kg wet 1.667 63 36-120 2 20 N-Nitrosodiphenylamine 1.33 0.66 mg/kg wet 1.667 80 38-127 7 20 Pentachlorophenol 0.762 1.0 mg/kg wet 1.667 46 25-133 11 20 J Phenanthrene 1.09 0.66 mg/kg wet 1.667 66 50-121 9 20 Phenol 1.04 0.66 mg/kg wet 1.667 63 34-121 2 20 Pyrene 1.07 0.66 mg/kg wet 1.667 64 47-127 10 20 Surrogate: 2,4,6-Tribromophenol 2.27 mg/kg wet 3.333 68 39-132 Surrogate: 2-Fluorobiphenyl 1.02 mg/kg wet 1.667 61 44-115 Surrogate: 2-Fluorophenol 2.05 mg/kg wet 3.333 61 35-115 Surrogate: Nitrobenzene-d5 0.892 mg/kg wet 1.667 54 37-122 Surrogate: Phenol-d5 1.92 mg/kg wet 3.333 58 34-121 Surrogate: Terphenyl-d14 1.00 mg/kg wet 1.667 60 54-127 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 18 of 21 P R I IS M Full -Service Analytical Environmental Solutions . LABORATORIES, INC. Level II QC Report 8/29/19 Summit Engineering (Charlotte) Project: UNCC Attn: Michael Zavislak P.O. Box 7384 Charlotte, NC 28241 Gasoline Range Organics by GC/FID - Quality Control Prism Work Order: 9080388 Time Submitted: 8/27/2019 3:45:OOPM Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9HO451 - 5030B Blank (P9H0451-BLK1) Prepared &Analyzed: 08/27/19 Gasoline Range Organics BRL 5.0 mg/kg wet Surrogate: a,a,a-Trifluorotoluene 5.25 mg/kg wet 5.000 105 50-137 LCS (P9H0451-BSI) Prepared &Analyzed: 08/27/19 Gasoline Range Organics 51.1 5.0 mg/kg wet 50.00 102 41-138 Surrogate: a,a,a-Trifluorotoluene 5.85 mg/kg wet 5.000 117 50-137 LCS Dup (P9HO451-BSD1) Prepared & Analyzed: 08/27/19 Gasoline Range Organics 50.1 5.0 mg/kg wet 50.00 100 41-138 2 20 Surrogate: a,a,a-Trifluorotoluene 5.75 mg/kg wet 5.000 115 50-137 Matrix Spike (P9H0451-MSI) Source: 9080388-01 Prepared: 08/27/19 Analyzed: 08/28/19 Gasoline Range Organics 135 6.1 mg/kg dry 60.75 98.7 60 41-138 Surrogate: a,a,a-Trifluorotoluene 6.80 mg/kg dry 6.075 112 50-137 Matrix Spike Dup (P9H0451-MSD1) Source: 9080388-01 Prepared: 08/27/19 Analyzed: 08/28/19 Gasoline Range Organics 128 6.1 mg/kg dry 60.75 98.7 48 41-138 6 34 Surrogate: a,a,a-Trifluorotoluene 6.32 mg/kg dry 6.075 104 50-137 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 19 of 21 Level II QC Report P R I IS M Full -Service Analytical 8/29/19 Environmental Solutions . LABORATORIES, INC. Summit Engineering (Charlotte) Project: UNCC Prism Work Order: 9080388 Attn: Michael Zavislak Time Submitted: 8/27/2019 3:45:OOPM P.O. Box 7384 Charlotte, NC 28241 Diesel Range Organics by GC/FID - Quality Control Reporting Spike Source %REC RPD Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes Batch P9HO463 - 3546 Blank (P9H0463-BLK1) Prepared & Analyzed: 08/28/19 Diesel Range Organics BRL 7.0 mg/kg wet Surrogate: o-Terphenyl 0.747 mg/kg wet 1.333 56 31-123 LCS (P91-10463-13SI) Prepared &Analyzed: 08/28/19 Diesel Range Organics 43.9 7.0 mg/kg wet 66.67 66 46-126 Surrogate: o-Terphenyl 0.763 mg/kg wet 1.333 57 31-123 LCS Dup (P9HO463-BSD1) Prepared & Analyzed: 08/28/19 Diesel Range Organics 42.6 7.0 mg/kg wet 66.67 64 46-126 3 20 Surrogate: o-Terphenyl 0.723 mg/kg wet 1.333 54 31-123 Sample Extraction Data Prep Method: 3546 Lab Number Batch Initial Final Date/Time 9080388-01 P91­10463 30.08 g 1 mL 08/28/19 8:35 Prep Method: 5030E Lab Number Batch Initial Final Date/Time 9080388-01 P91­10451 6.16 mL 5 mL 08/28/19 9:06 Prep Method: Solids, Dry Weight Lab Number Batch Initial Final Date/Time 9080388-01 P9H0461 30 g 30 g 08/28/19 7:30 Prep Method: 3546 Lab Number Batch Initial Final Date/Time 9080388-01 P91­10462 30.11 g 1 mL 08/28/19 8:35 Prep Method: 5035 Lab Number Batch Initial Final Date/Time 9080388-01 P91­10480 6.97 g 5 mL 08/28/19 12:00 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. 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No Fee's 3575 CENTRE CIR FORT MILL, SC 29715 Contract:50101913580 Generator:UNC Charlotte SITE TICKET # CELL W EIGHMASTER DATEMME IN DATE/TIME OUT VEHICLE EHG55255 CONTAINER 30YD-OT REFERENCE 5025248 BILL OF LADING SCALE IN GROSS WEIGHT 60,620 ET�WEIGHT INBOUND TARE OUT TARE WEIGHT 34,660 ET INVOICE CITY. I UNIT DESCRIPTION RATE EXTENSION TAX TOTAL 30.00 YO Tracking QTY 12.98 to SW-CONT SOIL-ALT DAILY Origin:MECKLENBURG 100% COVER HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE • WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW A SET FROM THE SCALE HOUSE. THANK YOU. The undersigned individual signing this document on behalf of Customer acknowledges that he or she has read and understands the terms and conditions on the reverse side and that he or she has the authority to sign this document on behalf of the customer. TENDERED CHANGE CHECK# RS-F042UPR (07/12) SIGNATURE ( SITE BFI/CMS LANDFILL 704-782-2004 105 MOREHEAD RD CONCORD, NC 28025 100600 SUMMIT ECS, INC. No Fee's 3575 CENTRE CIR FORT MILL, SC 29715 Contract:50101913580 Generator:UNC Charlotte SITE TICKET # CELL WEIGHMASTER DATEITIME IN DATEMME OUT VEHICLE CONTAINS REFERENCE 5025245 BILL OF LADING SCALE IN GROSS WEIGHT 65,540 ET TONS 15.31 INBOUND TARE OUT TARE WEIGHT 34,920 ET WEIGHT 30,620 INVOICE CITY. I UNIT DESCRIPTION RATE EXTENSION ` TAX TOTAL 30. 0 YD Tracking QTY 15. 1 to SW-CONT SOIL-ALT DAILY Origin:MECKLENBURG 100% COVER HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE • WHILE IN THE LANDFILL. IF YOU DO'NOT HAVE THESE ITEMS YOU MAY BORROW A SET FROM THE SCALE HOUSE. THANK YOU. The undersigned individual signing this document on behalf of Customer acknowledges that he or she has read and understands the terms and conditions on the reverse side and that he or she has the authority to sign this document on behalf of the customer. TENDERED CHANGE CHECK# RS-F042UPR (07112) SIGNATURE SITE BFI/CMS LANDFILL 704-782-2004 5105 MOREHEAD RD CONCORD, NC 28025 CUSTOMER 100600 SUMMIT ECS, INC. No Fee's 3575 CENTRE CIR FORT MILL, SC 29715 Contract:50101913580 Generator:UNC Charlotte TICKET # CELL DATEMME IN m I DATE/TIME OUT VEHICLE Q Q , CONTAINER' 17 / �Q , � 5025247 BILL OF LADING SCALE IN GROSS WEIGHT 70,080 NET TONS 18_09 INBOUND TARE OUT TARE WEIGHT I'l.90G NET WEIGHT 3'.12n INVOICE CITY. UNIT DESCRIPTION RATE XT EXTENSION '' TAX TOTAL 30.00 YD Tracking QTY 18.09 to SW-CONT SOIL-ALT DAILY Origin:MECKLENBURG 100% COVER HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE • WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW TENDERED A SET FROM THE SCALE HOUSE. THANK YOU. The undersigned individual signing this document on behalf of Customer acknowledges that he or she has read and understands the terms and conditions CHANGE on the reverse side and that he or she has the authority to sign this document on behalf of the customer. CHECK# RS-F042UPR (07/12) SIGNATURE BPI/CMS LANDFILL 704-782-2004 5105 IMOREHEAD RD CONCORD, NC 28025 CUSTOMER 100600 SUMMIT ECS, INC. No Fee's 3575 CENTRE CIR FORT MILL, SC 29715 Contract:50101913580 Generator:UNC Charlotte SITE TICKET # CELL WEIGHMASTER DATEMMEIN DATEMME OUT VEHICLE eha75321 CONTAINER REFERENCE 5025246 BILL OF LADING SCALE IN GROSS WEIGHT 65,36 NET TONS 15.53 INBOUND TARE OUT TARE WEIGHT 34,30 NET WEIGHT 31,060 INVOICE OTY. I UNIT DESCRIPTION RATE EXTENSION TAX TOTAL 30.00 YD Tracking QTY 15.53 to SW-CONT SOIL-ALT DAILY Origin:MECKLENBURG 100% COVER HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW A SET FROM THE SCALE HOUSE. THANK YOU. The undersigned individual signing this document on behalf of Customer acknowledges that he or she has read and understands the terms and conditions on the reverse side and that he or she has the authority to sign this document on behalf of the customer. TENDERED CHANGE CHECK# RS-F042UPR (07/12) SIGNATURE SITE BFI/CMS LANDFILL 704-782-2004 5105 MOREHEAD RD CONCORD, NC 28025 100600 SUMMIT ECS, INC. No Fee's 3575 CENTRE CIR FORT MILL, SC 29715 Contract:50101913580 Generator:UNC Charlotte SITE Y6 TICKET # 1683677 CELL 4916646 WEIGHMASTER DATEMME IN DATEITIME OUT VEHICLE eh 75321 CONTAINER 30YD-OT REFERENCE 5025243 BILL OF LADING SCALE IN GROSS WEIGHT 68,620 NET TONS 17.16 INBOUND TARE OUT TARE WEIGHT NET WEIGHT 34,300 34,320 INVOICE OTY. UNIT DESCRIP770N RATE EXTENSION '' TAX TOTAL 30.(0 YD Tracking QTY 17.36 to SW-CONT SOIL-ALT DAILY Origin:MECKLENBURG 100% COVER HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW A SET FROM THE SCALE HOUSE. THANK YOU. The undersigned individual signing this document on behalf of Customer acknowledges that he or she has read and understands the terms and conditions on the reverse side and that he or she has the authority to sign this document on behalf of the customer. TENDERED CHANGE CHECK# RS-FO42UPR (07/12) SIGNATURE BFI/CMS LANDFILL 704-782-2004 5105 MOREHEAD RD CONCORD, NC 28025 t f CUSTOMER SUMMIT ECS, INC. No Fee's 3575 CENTRE CIR FORT MILL, SC 29715 Contract:50101913580 Generator:UNC Charlotte SCALE IN GROSS WEIGHT 66,760 TARE OUT TARE WEIGHT 34,920 NET TONS NET WEIGHT SITEY6 TICKET # 1683638 CELL 4916646 WEIGHMASTER Quanta S . DATEITIME IN 9/ 17 / 19 12:33 pm DATEITIMEa9917/19 12:33 pr VEHICLE ehg75321 CONTAINER ehg3 REFERENCE 5025244 BILL OF LADING INBOUND 15.92 31,840 INVOICE OTY. UNIT DESCRIPTION RATE EXTENSION TAX TOTAL 3 0 YD Tracking QTY 15.92 to SW-CONT SOIL-ALT DAILY Origin:MECKLENBURG 100% COVER L_HJARHATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW A SET FROM THE SCALE HOUSE. THANK YOU. TENDERED The undersigned individual signing this document on behalf of Customer acknowledges that he or she has read and understands the terms and conditions CHANGE on the reverse side and that he or she has the authority to sign this document on behalf of the customer. CHECK# RS-F042UPR (07/12) SIGNATURE SITE BFI/CMS LANDFILL 704-782-2004 5105 k10REHEAD RD CONCORD, NC 28025 100600 SUMMIT ECS, INC. No Fee's 3575 CENTRE CIR FORT MILL, SC 29715 Contract:50101913580 Generator:UNC Charlotte 'SITE, TICKET # CELL WEIGHMASTER GWEN G.DATE/TIME DATE/TIME IN OUT VEHICLE aff CONTAINER"!:"'! 9 ` REFERENCE 5029391 BILL OF LADING J SCALE IN GROSS WEIGHT 66,600 NET TONS 16.15 INBOUND ` TARE OUT TARE WEIGHT 34.300 NET WEIGHT 32.300 INVOICE CITY. i UNIT DESCRIPTION RATE EXTENSION i TAX TOTAL 30.00 YD Tracking QTY 16.15 to SW-CONT SOIL-ALT DAILY Origin:MECKLENBURG 100% COVER HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE • WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW A SET FROM THE SCALE HOUSE. THANK YOU. The undersigned individual signing this document on behalf of Customer acknowledges that he or she has read and understands the terms and conditions on the reverse side and that he or she has the authority to sign this document on behalf of the customer. TENDERED CHANGE CHECK# RS-F042UPR (07/12) SIGNATURE SITE BFI/CMS LANDFILL 704-782-2004 5105 MOREHEAD RD CONCORD, NC 28025 CUSTOMER SUMMIT ECS', INC. No Fee's 3575 CENTRE CIR FORT MILL, SC 29715 Contract:50101913580 Generator:UNC Charlotte SCALE IN GROSS WEIGHT 64,060 TARE OUT TARE WEIGHT 34,180 NET TONS 14.94 NET WEIGHT 29,880 SITE�,6 TICKET# 1683569 CELL 4916646 WEIGHMASTER Quanta S. DATEITIME IN 9 / 17 / 19 10 : 2 9 am DATEITIME077 / 19 10 : 2 9 ar VEHICLE ehg75321 CONTAINER RS003 REFERENCE 5029392 BILL OF LADING INBOUND INVOICE OTY.r UNIT DESCRIPTION RATE EXTENSION TAX TOTAL 30. 0 YD Tracking QTY 14. 4 to SW-CONT SOIL-ALT DAILY Origin:MECKLENBURG 1000 COVER HARIb HATS JND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW • A SET FROM THE SCALE HOUSE. THANK YOU. TENDERED The undersigned individual signing this document on behalf of Customer acknowledges that he or she has read and understands the terms and conditions CHANGE on the reverse side and that he or she has the authority to sign this document on behalf of the customer. CHECK# RS-F042UPR (07/12) SIGNATURE SITE BFI/CMS LANDFILL 704-782-2004 5105 MOREHEAD RD CONCORD, NC 28025 SUMMIT ECS, INC. No Fee's 3575 CENTRE CIR FORT MILL, SC 29715 Contract:50101913580 Generator:UNC Charlotte SCALE IN GROSS WEIGHT 70,060 TARE OUT TARE WEIGHT 34,480 SITEY6 TICKET# 1683304 CELL 4916646 WEIGHMASTER Quanta S. DATEMME IN 9 / 16 / 19 12 :15 pm DATE/TIME5)PI6 / 19 12 : 15 pI VEHICLE ehg75321 CONTAINER RS004 REFERENCE 5029393 BILL OF LADING INBOUND NET TONS 17.79 NET WEIGHT 35,580 INVOICE CITY. UNIT DESCRIPTION RATE EXTENSION TAX TOTAL 40.00 YD Tracking QTY 17.79 to SW-CONT SOIL-ALT DAILY Origin:MECKLENBURG 100% COVER HARI HATS IND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW A SET FROM THE SCALE HOUSE. THANK YOU. TENDERED The undersigned individual signing this document on behalf of Customer acknowledges that he or she has read and understands the terms and conditions CHANGE on the reverse side and that he or she has the authority to sign this document on behalf of the customer. CHECK# RS-F042UPR (07/12) SIGNATURE CELL BFI/CMS LANDFILL 704-782-2004 5105 MOREHEAD RD CONCORD, NC 28025 100600 DATEMME IN - - - DATE/TIME OUT SUMMIT ECS, INC. No Fee's VEHICLE CONTAINER 3575 CENTRE CIR FORT MILL, SC 29715 REFERENCE 5029394 Contract : 50101913580 BILL OF LADING Generator:UNC Charlotte SCALE IN GROSS WEIGHT 70,720 ET TONS 18.21 INBOUND TARE OUT TARE WEIGHT 34,300 NET WEIGHT 36,420 INVOICE OTY. UNIT cDESCRIPTION RATE EXTENSION TAX TOTAL 30.00 YD Tracking QTY 18.21 to SW-CONT SOIL-ALT DAILY Origin:MECKLENBURG 100% COVER HARD HATS AND SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW A SET FROM THE SCALE HOUSE. THANK YOU. TENDERED The undersigned individual signing this document on behalf of Customer acknowledges that he or she has read and understands the terms and conditions CHANGE on the reverse side and that he or she has the authority to sign this document on behalf of the customer. CHECK# RS-FO42UPR (07/12) SIGNATURE BFI/CMS LANDFILL,,704-782-2004 5105_MOREHEAD RD CONCORD, NC 28025 CUSTOMER lUUbUU SUMMIT ECS, INC. No Fee's 3575 CENTRE CIR FORT MILL, SC 29715 Contract:50101913580 Generator:UNC Charlotte SCALE IN GROSS WEIGHT 58,640 TARE OUT TARE WEIGHT 34,340 NET TONS NET WEIGHT SITEY6 TICKETn 1683229 CELL 4916646 WEIGHMASTER Quanta S. DATE/TIME IN 9 / 16 / 19 9 : 4 9 am DATE/TIMEff6 / 19 9 : 4 9 ar VEHICLE ehg75321 CONTAINER ehgl7 REFERENCE 5029395 BILL OF LADING TNROTTNn 12.15 24,300 INVOICE QTY. UNIT DESCRIPTION RATE EXTENSION TAX TOTAL 30.00 YD Tracking QTY 12.15 to SW-CONT SOIL-ALT DAILY Origin:MECKLENBURG 1000 COVER HARI HATS LD SAFETY VEST ARE REQUIRED WHEN EXITING YOUR VEHICLE WHILE IN THE LANDFILL. IF YOU DO NOT HAVE THESE ITEMS YOU MAY BORROW • A SET FROM THE SCALE HOUSE. THANK YOU. TENDERED The undersigned individual signing this document on behalf of Customer acknowledges that he or she has read and understands the terms and conditions CHANGE on the reverse side and that he or she has the authority to sign this document on behalf of the customer. CHECK# RS-F042UPR (07/12) SIGNATURE APPENDIX D - PHOTO PAGE Project No. 71177348 lrerracon Date Photos Taken: August 27, September 19, and September 30, 2019 Consulting Engineers & Scientists Photo 1 View of the impacted soil location in the southwest portion of the building area discovered during demolition work on August 27, 2019. Ri i� VOW LAY ,4. � ' TV VA �Y Il i Photo 2 View of to impacted and stained soils within the southeastern portion of the demolished building Sanford Hall Lane — Charlotte, North Carolina Project No. 71177348 lrerracon Date Photos Taken: August 27, September 19, and September 30, 2019 Consulting Engineers & Scientists M l v^: i WNIP-W, " \ -sti „. Photo 3 View of the stockpiled impacted soils discovered in the southeastern portion of the demolished building. Photo 4 View of the impacted soil removed and stockpiled on August 27, 2019. Sanford Hall Lane - Charlotte, North Carolina Project No. 71177348 lrerracon Date Photos Taken: August 27, September 19, and September 30, 2019 Consulting Engineers & Scientists Photo 5 View of the stained soils and smear zone following the demolition of the on -site building on September 19, 2019; looking southeast. Photo 6 View of the stained soils and smear zone following the demolition of the on -site building on September 19, 2019; looking south. Sanford Hall Lane — Charlotte, North Carolina Project No. 71177348 lrerracon Date Photos Taken: August 27, September 19, and September 30, 2019 Consulting Engineers & Scientists Photo 7 View of the site following demolition activities; looking southwest on September 30, 2019. Sanford Hall Lane - Charlotte, North Carolina Beverly, Trudy From: Beverly, Trudy Sent: Tuesday, November 12, 2019 1:41 PM To: Welch, McKhenzy A Cc: Elizabeth Frere; Corbitt, Chris L. Subject: RE: [External] UNCC Moore Hall Risk Assessment Report Received. Thanks McKhenzy. Trudy Q.�..,d,,-D - kparLn n[olyGmn-onm L314w Trudy Beverly, L.G. Hydrogeologist, Division of Waste Management North Carolina Department of Environmental Quality UST Section, Mooresville Regional Office 704.235.2182 (Office) Trudy.13everlykncdenn gov Email correspondence to and from this address is subject to the North Carolina Public Records Law and may be disclosed to third parties. Office Mailing Address: 610 East Center Avenue, Suite 301 Mooresville, NC 28115 Branch's Underground Storage Tanks Website Address: https://deg.nc.gov/about/divisions/waste-management/ust Branch's Above Ground Storage Tanks Website Address: hit2s://deq.nc.gov/about/divisions/waste-management/ust/ast-program INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES: httos://dea.ne. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-mans File Review Procedures: httns: //dea.ne. gov/about/divisions/waste-manaizement/ust/file-review-nrocedures#mooresville-regional-office ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche): hops://edocs.deq.nc. gov/WasteManagement/Search.aspxx Document Submittal & UST File Names for Laserfiche Policies: htips:Hfiles.nc. gov/ncdeq/Waste%20Mana,gemenUD WMIUST/Corrective%2OActionBlectronic%2ODocument%2OSubmittal%2OMemo%2OUpdate.pdf ht!Rs:Hfiles.nc. gov/ncdeq/Waste%20Management/DWM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche.docx From: Welch, McKhenzy A[mailto:Mckhenzy.Welch@terracon.com] Sent: Tuesday, November 12, 2019 1:28 PM To: Beverly, Trudy <trudy.beverly@ncdenr.gov> Cc: Elizabeth Frere <efrere@uncc.edu>; Corbitt, Chris L. <Chris.Corbitt@terracon.com> Subject: [External] UNCC Moore Hall Risk Assessment Report i*�**F External email. Do not click links or open attachments unless you verify. Send all suspicious email as an attachment to report.spam@nc.gov Attached is the Moore Hall Risk Assessment report. Contact me with any questions or comments. Hope all is well. McKhenzy Welch, CPESC Terracon Consultants, Inc P 980-938-7436 1 M 704-430-3174 Terracon provides environmental, facilities, geotechnical, and materials consulting engineering services delivered with responsiveness, resourcefulness, and reliability. Private and confidential as detailed here (www.terracon.com/disclaimer). If you cannot access the hyperlink, please e-mail sender.