MO-9531_49066_CA_20-DAY_20191209_20-Day Report, Draft NRP, and Receptor Discussion

HEATING OIL UST CLOSURE REPORT
TIM COLLINS PROPERTY, INCIDENT NO. 40966
2640 SHENANDOAH AVENUE
CHARLOTTE, MECKLENBURG COUNTY, NORTH CAROLINA 28205
ATC PROJECT 199TCP1901
UST NO. MO-9531
Prepared for:
Lanier Site Services
12825 Downs Circle
Pineville, North Carolina 28134
DECEMBER 9, 2019
Prepared by:
ATC Associates of North Carolina, P.C.
7606 Whitehall Executive Center Drive, Suite 800
Charlotte, North Carolina
I, AI Quarles , a Professional Geologist for ATC Associates of
North Carolina, P.C., do certify that the information contained in
this report is correct and accurate to the best of my knowledge.
ATC Associates of North Carolina, P.C. is licensed to practice
engineering and geology in North Carolina. The certification
number of the company or corporation is C-1598 for engineering
and C-294 for geology.

;ETC
December 9, 2019
Mr. Eric Lanier
Lanier Site Services
12825 Downs Circle
Pineville, North Carolina 28134
Subject: Heating Oil UST Closure Report
Tim Collins Property, Incident No. 40966
2640 Shenandoah Avenue
Charlotte, Mecklenburg County, North Carolina 28205
ATC Project 199TCP1901
UST No. MO-9531
Dear Mr. Lanier:
ATC Associates of North Carolina, P.C.
7606 Whitehall Executive Center Drive, Suite 800
Charlotte, North Carolina 28273
704-529-3200
www.atcassociates.com
ATC Group Services, LLC (ATC), submits this Letter Report to Lanier Site Services (Lanier) for
environmental services related to the referenced site. The services were conducted in accordance with
ATC Proposal 199TCP1901 dated November 6, 2019, and Change Order #1 dated November 22, 2019.
Background
The Tim Collins Property is a residential property located at 2640 Shenandoah Avenue, Charlotte, in
Mecklenburg County, North Carolina and is identified by Mecklenburg County as Parcel ID 12710225.
The location of the site is indicated on a Mecklenburg County Topographic Map (Figure 1). The location
of the UST is indicated on a Mecklenburg County aerial (Figure 2). Surrounding properties and nearby
incidents are indicated Figure 3, obtained from the Mecklenburg County Well Information website. As
indicated on Figure 3, there are no reported water supply wells located within 1,500 feet of the source
area, and a surface water body (Briar Creek) is located approximately 400 feet southeast of the source
area.
The property is owned by Tim Collins, 2640 Shenandoah Avenue, Charlotte, 28205. The residence was
constructed in 1948, and used an approximate 650-gallon heating oil underground storage tank (UST)
for on -site heating purposes. The installation date and dates of operation for the UST are unknown. The
UST is considered a non -regulated, non-commercial petroleum UST by the North Carolina Department
of Environmental Quality (NCDEQ). Table 1 and Table 2 summarize information about the UST system,
release history, and owner/operator information. The property is currently in bankruptcy proceedings,
and Lanier was contracted by the bankruptcy trustee to conduct the UST removal activities.
UST Closure and Initial Soil Sampling
On October 29, 2019, Lanier contracted with Haz-Mat Environmental Services of Charlotte, North
Carolina, to remove 476 gallons of petroleum contact water from the UST and dispose of the removed
fluids. A copy of the waste manifest is included in Appendix A.
On November 8, 2019, ATC collected two soil samples from beneath the UST, after removal by Lanier.
The UST was approximately 7 feet in length and 4 feet in diameter (approximately 650 gallons), and
was observed to have multiple corrosion holes at the base of the UST. Since the length of the UST was
greater than 6 feet, two soil samples were collected for laboratory analysis.

Heating Oil UST Closure Report
Tim Collins Property (Incident No. 49066), Charlotte, NC
ATC Project No. 199TCP1901
December 9, 2019
;ETC
ATC submitted the two soil samples (SS-1 and SS-2) to Pace Analytical Services, LLC, Huntersville,
North Carolina, for the analysis of Total Petroleum Hydrocarbon (TPH) for Gasoline Range Organics
(GRO) and Diesel Range Organics (DRO) using EPA Method 8015B. The concentrations of TPH-DRO
were 166 milligrams per kilogram (mg/kg) for sample SS-1 and 5,010 mg/kg for sample SS-2, compared
to the NCDEQ's Action Level of 100 mg/kg. (Table 3) The concentration of TPH-DRO in sample SS-1
was approximately 3.3 percent of the concentration in sample SS-2. Due to the exceedance of the
Action Level, ATC recommended and Lanier approved, the analysis of sample SS-2 of the "Risk -Based
Rule" parameters: volatile organic compounds or VOCs (EPA Method 8260), semi -volatile organic
compounds or SVOCs (EPA Method 8270), volatile petroleum hydrocarbons (MADEP Method VPH),
and extractable petroleum hydrocarbons (MADEP Method EPH). The results indicated several
exceedances of the Soil -to -Groundwater Maximum Soil Contaminant Concentrations (MSCCs) and
three compounds (1-Methyl naphthalene, Aliphatics C9-C18, and Aromatics C9-C22) exceeded the
Residential MSCCs. Analytical results are summarized in Table 3. A copy of the laboratory report is
included in Appendix B.
Soil Excavation and Soil Sampling
Based on the exceedances of the Residential MSCCs, soils were excavated on November 26, 2019 in
an attempt to remove the soil impacted at levels exceeding the Residential MSCCs. On November 26,
2019, ATC observed the soil excavation by Lanier. Excavated soils were screened based on observed
odors or discoloration, and photoionization detector (PID) readings. The soils were segregated as
"clean" overburden and as "impacted" soil, based on the apparent absence or presence of petroleum
impact from the field screening. The "clean" overburden soil was set aside for use as backfill. The
"impacted" soil was loaded directly into dump trucks and disposed off -site at a permitted facility. The
"clean" overburden soil extended to a depth of approximately four feet. Soils below four feet appeared
to be impacted, based on visual and olfactory observations, and PID readings. The excavation was
ceased based on the vertical limit of the excavation equipment. Four truck loads (20.78 tons) were
transported for disposal at a permitted facility: Environmental Soils, Lattimore, North Carolina. Copies
of the waste manifests are included in Appendix A.
The approximate dimensions of the excavation were 8 to 9 feet deep, 9 feet wide, and 10 feet long.
ATC collected soil samples from the sidewalls and base of the excavation. Groundwater was not
encountered at the base of the excavation.
ATC collected soil samples from the base of the excavation and each of the four side walls, SE-1
through SE-5, respectively. On November 27, 2019, ATC delivered the soil samples to Prism
Laboratories, Inc., in Charlotte, North Carolina, for laboratory analysis of the "Risk -Based Rule"
parameters. The results indicated exceedances of the Soil -to -Groundwater MSCCs in each of the
samples, and exceedances of the Residential MSCCs in samples SE-1, SE-3, SE-4 and SE-5. The
parameters with exceedances of the Residential MSCCs included Aliphatics C9-C18 range and
Aromatics C9-C22 range. Analytical results are summarized in Table 3.
On December 3, 2019, ATC submitted a 24-Hour Release and UST Leak Reporting Form (UST-61) to
NCDEQ, and the NCDEQ established Incident 40966 to the release.
Notice of Residual Petroleum, Public Notification, and Notice of No Further Action
Concurrent with this reporting, ATC is preparing a Notice of Residual Petroleum (NORP), alternate
version, with soil and groundwater restrictions. A draft NORP will be submitted to NCDEQ for approval
prior to submitting the final signed/notarized NORP to NCDEQ. The NCDEQ-signed/notarized NORP
2

Heating Oil UST Closure Report
Tim Collins Property (Incident No. 49066), Charlotte, NC
ATC Project No. 199TCP1901
December 9, 2019
ETC
will be filed with the Mecklenburg County Register of Deeds. ATC will also conduct public notification
of the Conditional Notice of No Further Action (NFA), expected to be issued by the NCDEQ following
receipt of this report. ATC anticipated that a final NFA will be issued following submittal of documentation
of the public notification.
Closing
If you have any questions concerning this submittal, please contact ATC at your convenience at (704)
529-3200.
Sincerely,
ATC Group Services, LLC
Erin E. Greene
Project Manager
FIGURES
Figure 1:
Figure 2:
Figure 3:
TABLES
Table 1:
Table 2:
Table 3:
APPENDICES
Appendix A:
Appendix B:
Topographic Map
Sample Location Map
Well Information Map
UST System and Release Information
UST Owner/Operator Information
Soil Analytical Results
Laboratory
Waste Disposal Documentation
Reports
w f'PP
• -
t
cc: Ms. Trudy Beverly, NCDEQ, DWM, UST Section, Mooresville Regional Office

Heating Oil UST Closure Report
Tim Collins Property (Incident No. 49066), Charlotte, NC
ATC Project No. 199TCP1901
December 9, 2019
FIGURES
;ETC

F } Fy
?6. 65b -
** Vi , I.FJ Ii
\ 61 `
YO ;.�.
q�e
00
• ��
2640 Shenandoah Ave
Parcel ID 12710225
Deed Book/Pages: 30084/64-66
0 0.005)_01•70:_02YN
y
1
Map Scale: As Shown
7606 Whitehall Executive Center
Iff Drive, Suite 800
AVA
Iff kTc Charlotte, North Carolina
[phone]
SOURCE: Mecklenburg County POLARIS
December 3, 2019
� +,
-441;%j
FIGURE 1.
TOPOGRAPHIC MAP
Tim Collins Property, Incident # 40966
2640 Shenandoah Avenue
Charlotte, North Carolina 28205
ATC Project No. 199TCP1901

_-+
2640 Shenandoah Ave
Parcel ID 12710225
Deed Book/Pages: 30084/64-66
Approximate UST
Excavation
1 Aerial Map Scale: 1 inch -- 30 feet
All locations and distances are approximate,
and are not based on a site survey.
kTc7606 Whitehall Executive Center
Drive, Suite 800
Charlotte, North Carolina
704 529-3200
SOURCE: Mecklenburg County POLARIS
December 3, 2019
q4%
SE-3 �J
Close-up of Excavation
Scale: 1 inch — 10 feet
® SOIL SAMPLING LOCATION
FIGURE 2.
SAMPLE LOCATION MAP
Tim Collins Property, Incident # 40966
2640 Shenandoah Avenue
Charlotte, North Carolina 28205
ATC Project No. 199TCP1901

F
PrIgLz Wens
ARive
InBC['ye
Rermenem Abandoned
+
Ternporery Abandoned
Unknown
1
Public wolfs
* �rens�ens
7606 Whitehall Executive Center
Iff Drive, Suite 800
AVA
kTc Charlotte, North Carolina
[phone]
SOURCE: Mecklenburg County Well Information System
December 3, 2019
Monkorin Wells
♦
Aas ve
,�
I�a,e4ivr
�a'r„enerYt Aba�dcrtcd
1
1emporaty Abandoned
SIF, rsued
FIGURE 3.
WELL INFORMATION MAP
Tim Collins Property, Incident # 40966
2640 Shenandoah Avenue
Charlotte, North Carolina 28205
ATC Project No. 199TCP1901

Heating Oil UST Closure Report
Tim Collins Property (Incident No. 49066), Charlotte, NC
ATC Project No. 199TCP1901
December 9, 2019
TABLES
;ETC

TABLE 1
UST SYSTEM AND RELEASE INFORMATION
TIM COLLINS PROPERTY
2640 Shenandoah Avenue
Charlotte, North Carolina
NCDEQ Incident #40966
Capacity Was Release
UST ID Number Contents (gallons) Date Tank Installed Status of UST With UST System (Y/N;
1 I No. 2 Heating 600 I Approximately 1948 Removed I Y
Oil 11/8/19
Incident Material Date of Description of Release
Number Released Release
40966 I No. 2 Heating UnknownlUSTase discovered upon removal of home heating oil

TABLE 2
UST OWNER/OPERATOR INFORMATION
TIM COLLINS PROPERTY
2640 Shenandoah Avenue
Charlotte, North Carolina
NCDEQ Incident #40966
UST ID Number 1
Facility ID Number
N/A
Name of Owner
Dates of Operation
(mm/dd/yy to mm/dd/yy)
Tim Collins
1948 to 11/8/19
Street Address
2633 Shenandoah Avenue
City
State
Zip
ITelephone Number
Charlotte
INC
28205
jUnknown
Name of Operator
Dates of Operation
(mm/dd/yy to mm/dd/yy)
Tim Collins
11948 to 11/8/19
Street Address
2633 Shenandoah Avenue
City
I State
jZip
ITelephone Number
Charlotte
INC
128205
jUnknown

TABLE 3
SOIL ANALYTICAL RESULTS
TIM COLLINS PROPERTY
2640 Shenandoah Avenue
Charlotte, North Carolina
NCDEQ Incident #40966
Analytical Method
EPA 8015C
EPA 8260
EPA 8270
MADEP VPH/EPH
N
d
N
=
=
N
c
d
=
N
d
d
C
d
=
Op
CV
=
_
_
_
C1
=
C
10 V
N
d
C
N
w
C
=
N
d
N
Na
N
C
N
C N
W
C
N
d
Q
N
3
C
lC
t
f0
y
r-
N
t
L
_
i
U
Cn
Sample
Sample
Sample
t�
R ._
=
._
c
_
d
=
d
N
=
H
m
=
d
m
M
m
m=
s d
�,
a Y
o
L
s
t
�,
.r
°'
°'
=
L
s
a
s
Q
w
=
U
U
U
Depth
R
m
N
s
m
w
>.
>,
>. E
m
c
°�
°�
a
E
E
R
R
s
=
m
y
w
y
ID
Date
(ft-bgs)
m a�
_ rn
m
H
=
s
a
�,
•,
'
a
N
.
s
E
E
Q
E
>,
o
3
c
�'
c
�`
s
a
R
T
a
°
w
ayi O
o 0
t
m
R
3
M�
m
m
O U
L
>,
L
i
C
o
LL
i
L
10
a=i
L
m
lC
R
_
y
w
X
Z
m
1=
o
i
d
M
H
H
W
C
m
U
i
a
m
m
Z
a
Q
o_
E
4)
fq
w
N
N
4
�
a
=
N
Q
Q
Q
Q
o
Q
N
M
NCDEQ Action Level
100
50
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
MSCC - Soil -to -Water
NA
NA
0.0056
4.3
4.9
4.6
0.16
4.30
3.3
3.4
1.7
0.4
NE
8.5
8.3
0.12
0.4
0.02
1.7
47
0.004
3.6
0.16
56
270
68
540
#
31
MSCC - Residential
NA
NA
18
1,200
1,560
3,129
313
626
626
626
1,560
1,200
NE
782
782
100
22
49
626
620
20
63
313
469
469
939
1,500
31,000
469
MSCC - Industrial/Commercial
NA
NA
164
32,000
40,000
81,760
8,176
16,350
16,350
16,350
40,880
32,000
NE
20,440
20,440
4,000
570
440
16,350
16,400
100
1,635
8,176
12,264
12,264
24,528
40,000
810,000
12,264
SS-1
11/08/19
6
166
3.1J
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
---
SS-2
11/08/19
6
5,010
41.6
<0.0772
<0.139
1.85
6.43
9.85
3.61
<0.182
<0.145
1.65
1.220J
<0.307
17.5
<0.144
<0.207
<0.203
<0.282
<0.144
4.84
32.3
49.2
11.4
11
1.290J
28.1
3,444
<1,170
1,684
SE-1
11/26/19
8.5
---
---
0.27 J
0.78
7.3
30
8.9
5.2
5.7
0.35
3.7
<0.024
<0.043
31
10
3.8
0.37 J
0.15 J
7.0
2.9
19
31
7.1 J
5.8
0.36 J
62
760
180
700
SE-2
11/26/19
8
---
---
0.11 J
0.45
6.1
26
11
4.7
5.0
0.33
3.1
<0.024
<0.042
31
8.5
3.3
0.24 J
<0.089
5.9
1.6
7.6
13
3.0
3.0
0.26 J
60
164
6.3 J
150
SE-3
11/26/19
8
---
---
<0.038
0.12 J
0.6
2.3
3.7
0.63
0.57
<0.029
0.37
<0.020
<0.035
4.1
1.1
0.43
<0.12
<0.074
0.77
1.8
9.3
15
4.3
3.8
0.48 J
7.1 J
820
240
687
SE-4
11/26/19
8
---
---
<0.00087
<0.00089
0.0011 J
0.0043 J
0.0020 J
<0.00052
0.00075 J
<0.00066
<0.00065
<0.00046
0.0011 J
0.0027 J
0.00099 J
<0.0014
<0.0027
<0.0017
0.000921
<0.014
<0.012
<0.015
<0.017
<0.0085
<0.011
<3.5
1,213
360
770
SE-5
11/26/19
8
- -
---
0.0096
0.058
0.32
7.9
0.19
0.14
0.20
0.013
0.17
<0.00044
<0.00077
12
3.7
0.12
<0.0026
<0.0016
2.5
1.1
4.9
7.5
1.8
2.2
0.22 J
8.0 J
2,120
540
1,282
Notes:
Concentrations presented in milligrams per kilogram (mg/kg)
ft-bgs = feet below ground surface
NA = Not Applicable
NE = No Established
--- = Not Analyzed
<Value = Not Detected above laboratory reporting limit.
J = Estimated value between method detection limit and laboratory reporting limit
Constituents not shown were reported below method detection limits in all samples. Refer to laboratory report for reporting and method detection limits.
Maximum Soil Contaminant Concentrations (MSCCs) defined in Table 1, Version 1 - 2016_11-03, "Guidelines for Site Checks, Tank Closure, and Initial Response and Abatement'
Concentrations in BOLD equal to or exceed the Soil -to -Groundwater MSCC
Concentrations in BOLD equal to or exceed the Residential MSCC
# = Health based level >100%

Heating Oil UST Closure Report
Tim Collins Property (Incident No. 49066), Charlotte, NC
ATC Project No. 199TCP1901
December 9, 2019
;ETC
APPENDIX A: WASTE DISPOSAL DOCUMENTATION

. . . . . . . . . . . . .
SwFF
H.AZ-MAT
ENVIRONMENTAL SERVICES
P.O. BOX 37392 - CHARLOTTE, N.C. 28237
[phone]
FAX [phone]
NON -HAZARDOUS SPECIAL WASTE
Sectioth L GEIIEi'4AT--ORcc-ia.cowkteauofseci i,
GENERATO WORK CONTRACTED BY
T08,01uns em To (it diffaroW. from ir.foariation at left)
NAME
ORIGINATING ADDRESS
MAILING AD ES _NC 28205...
Sri otte.
CITY s STATE— ZIP
��Im�o tiff
Manifest No. 88710
P.O. No.
---
19-5911
Job No. ^rA-1 It
.7JI-il I
Lanier Site Service-
W&E
ADDREfl 12_825_N�m_s Circle. C
meville _N
C!Ty STATE
Eric Lanier
PHONE NO. PHONE NO.
_98G-'104J031-3 1152
CONTACTNAME 2664029 CONTACT NAME
UEi-[B�ZffDIr-riquids T] n I
DES. OF WASTE:
NO. Type Units QL:an'Jty
''
S�ctioSection11. ' INV-0.10E'INFORMATON ION GALLS DRUMS -
DESCRIPTION
QUANTITY
LINE TOTAL
1. PEE_ MOLEUM CONTACTINATER
2, OFF -SPEC LIGHT OIL, DIESEL OR GAS
ssI
3. NON -HAZARDOUS LIQUIDS
4. SEDIMENT OR SOLIDS'
5. 55-GALLON DRUM REMOVED -SOLID OR EMPTY
6. 55-GALLON DRUM REMOVED -LIQUID
-----------
7.
9.
10, ARRIVALTIME: 5R611 DEPARTURETIME-
GENERATOR's CERTIFICATION: I 'horeby certify that the above named materlialis not a hazardous waste as dermed by 40 CFR Part 261 or any applicable state law, has been properly
described, classred and packaged, and is in proper condition for transportation accordIng to applicable regulations. GawatorlCustomer Shall reirnbuse t-AZ-,%4AT its reasonable expenses
and charges for handling, anafi zing, loading, preparing, transporting, storing or caring for nonconforming or off spec waste, including costs of decontamination and cleaning of equipment.
Generator must notify HAZZ-MAT of any charges to the waste stream prior to sNprrent.
Generator Authorized AgeW Name Slgrwure
I Se&ioti ITL_ '- "..TRANSPORI'MR
TRARSPORTERT
AT
ENVIRONMENTAL SERVICES
P.O. Q0y_%73924CEiARLO 8237
Driver Name,'Title_ j
Phone No....c. Truck No.
�-Iazardous Waste Trans.mrler Penrnils
EPA NCD048 61370
c.
D::vtt Sig
n 0010
Site Name: Haz-Mat Envfronrnen*af Services
Physical Address: 210 Dalton Avenue
Charlotte, N,C. 28206
f. Ad&ass
g. Driver Name I 7tle
h. Phore No. 1. Truck No.
j. -rar.sporter 11 Perm:: Ncs.
IN000001
a. Phone No. 104-332-560L Q
b, Mailing Address: P.O. Box 37392
Charlotte, N.C. 28237
c: D.screpancy Indication Space
his is to oI M all.rontamrdousmate ial vmvmd 'cm above location has mer recOwd and -A be ddosed: of h ao=darm yiith wplim& iocat, stage and t&J- regulations h It* t" -arx— ") Pmollcun- p-AIcts
-CMUD sanitation sew-- a —.;Ztt]UP#5,r,':2.(3)6.udci-sf,omirea!ni systems are hau'.ed 1,-, E.P.A. apprcved fa6'.itiesfor p..-oper disposal. Manifest aid ce�rtilii:ate �.fdisposal are or. rile.
.hen into the r sy=
,,firstoL0,4 ' andprmdWshcu?
(4) Our treatrI system operates on a fi�� 114ven days.
SIGNA7jRE OF FACILITYAGENT �A DATE
I MONTH lu IDAY
_ORIGINAL '-'ANALTS.:). - YELLOW -DISPOSER - PINK-'STT.S.D. - GOLD -GENERATOR

Environmental Soils Inc.
PO Box 295 - Lattimore, NC 28089
Phone [phone] - Fax [phone]
Non -Hazardous Waste Manifest #
Date ---- Load Number
(numbered sequentially as trucks axe dispatched}
ENnROM MENTALCONSUL TAIVT. ATC Associates of North Carolina, P.C.
Contact: Erin Greene Phone: [phone] Fax: [phone]
GENE&4TOR. Lanier Site Services
Address: 12825 Downs Circle, Pineville, NC 28134
Contact: Eric Lanier
County: _ Mecklenburg
Phone: 704-587­3022
WASTE ORIGEVATIONPOLVT-Complete Address. 2640 Shenandoah Ave, Charlotte, NC 28205
DESTEVATIOM Environmental Soils Inc. 910 Crowdy Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina,
Facility Signature:
Signature: l Date:
Company Name "itle,-
White/Facility Canary/Invoice of Pink/Carrier

Environmental 6oids Inc.
PO Box 295 - Lattimore, NC 28089
Phone [phone] - Fax [phone]
Non -Hazardous Waste Manifest #
Date 0 �­ Load Number
(numbered sequentially as trucks are dispatched)
EAWRON EATML CONS, T _LT ATC Associates of North Carolina, P.C.
,ffT
Contact.- Erin Greene
Phone: [phone] Fax: [phone]
GENERATOR. —Lanier Site Services
Address. 12825 Downs Circle, Pineville, NC A28134
Contact: Eric Lanier
WASTF ORIGINATTONPOINT Comr)lete Addre
County: Mecklenburg
Phone: [phone]
2640 Shenandoah Ave, Charlotte, NC 28205
Class &Type of Contaminate in soil — Petroleum, Heating Oil
SOURCE OFCOATTAMIN,4TION.- (ex. UST or other Source) HeatingOlIUST
DESTINATION.- Environmental Soils Inc. 910 Cro,,Ndy Rd, Shelby, NC 28150 Dedicated Land Application
Site Permit #SR0300038
1 certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina.
A
Facility Signature: l J ate:
Signature:
Date:
Company Name Eli Title:
White/Facility Canary/Invoice Goldenrod/Generator Pink/Carrier

Environmental Soils Inc.
PO Box 295 - Lattimore, NC 28089
Phone [phone] - Fax [phone]
Non -Hazardous Waste Manifest #
Date I I -2-w —19 Load Number
Class &Type of Contaminate in soil Petroleum, Heating it
SOURCE OF CONE4MINATIOX (ex. UST or other source) —Heating Oil UST
TWANSPORTER- —/— e? "
Contact. 1--r t-C Z --'V1 I
Phone:
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and I hereby -receive this material for delivery to the
facility designate.
Carrier Signature: Date:
P 51 q6'q
TRUCK #: TAG #: VOLUME:
TRUCK DRIVER SIGNATURE: DATE:
.BEST' ION.- Environmental Soils Inc. 910 Crowdy Rd, Shelby, NC 28150 Dedicated ,and Application
Site Permit #SR0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina.
Facility Signature: Date:
Signature: —
Company Name
I /
Date: 11-L 6j,7
White/Facility
Canary/Invoice Goldenrod/Generator Pink/Carrier

Environmental Soils Inc.
PO Boy: 295 - Lattimore, NC 2,80
Phone [phone] - Fax [phone]
Non-HazardousaWaste Manifest
Date _ Load Number
(numbered sequentially as trucks are dispatched)
pAWj?nV&jpjXT,rATAFr, ATC Associatesof North Carolina, P.C.
k—ounty: Mecklenburg___
Phone: [phone]
2640 Shenandoah Ave, Charlotte, NC 28205
:lass &Type of Contarninate ire soil Petroleum, Heating Oil
SOURCE FCO �'. ON. (ex. UST or other source) Heating Oil UST
GENERATORS . '.� . " a OF WASTE CONSTITUENTS.- In lieu ofsubmitting anabif ital data(methods
240 and 0 ver5ingthat the waste in question does not contain organic constituents other than those which would
c
normally a , eaar° in analysis aa�'� irginpetroleui o residue, lam suhmitting this Cent cafe of Waste
Constituents. Icertify that lamfamiliar with the source try`"contamination of the soil a ndjur Cher^ certio the source, to
the best o ' a hnowledge, contains no contaminants nts ther° than that listed above.
TR,INSPORTER:
Contact; a ' _ Phone: �q o
As the carrier, I certify that the materials described above being shipped under this non -hazardous materials
manifest are properly classified, packaged, labeled, secured, and are in proper condition for transport in commerce
under the applicable regulations governing transportation, and c e, ceive this material for delivery to the
facility designate.---�---� — re
Carrier Signature: - .mate. - TRUCK DRIVER SIGNATURE:Z!�2-1 DATE: --� f —,Q V-
ION. Environmental Sails Inc. /10 Crowdy Rd, Shelby, NC 23150 Dedicated Land Application:
Site Permit #S 0300038
I certify that the carrier has delivered the materials described above to this facility, and I hereby accept this material
for treatment and/or disposal in a manner that has been authorized by the Sate of North Carolina.
Facility Signature. � . Date.
g - _ r
Si nat�rem F Date:
Company Name Title:
White/Facility Canary/Invoice Goldenrod/Generator Pink/Carrier

Heating Oil UST Closure Report
Tim Collins Property (Incident No. 49066), Charlotte, NC
ATC Project No. 199TCP1901
December 9, 2019
APPENDIX B: LABORATORY REPORTS
;ETC

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
November 19, 2019
Erin Greene
ATC Group
7606 Whitehall Executive Cente
Suite 800
Charlotte, NC 28273
RE: Project: HO UST
Pace Project No.: 92452986
Dear Erin Greene:
Enclosed are the analytical results for sample(s) received by the laboratory on November 08, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely, p
Taylor Ezell
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: HO UST
Pace Project No.: 92452986
Pace Analytical Services Charlotte
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 31

leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE SUMMARY
Project: HO UST
Pace Project No.: 92452986
Lab ID
Sample ID
Matrix
Date Collected
Date Received
92452986001
92452986002
SS-1
SS-2
Solid
Solid
11/08/1911:20
11/08/1911:25
11/08/1913:10
11/08/1913:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 31

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
HO UST
92452986
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92452986001
SS-1
EPA 8015C Modified
BAJ
2
PASI-C
EPA 8015C Modified
LMB
2
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92452986002
SS-2
EPA 8015C Modified
BAJ
2
PASI-C
MADEP EPH
BAJ
7
PASI-C
EPA 8015C Modified
LMB
2
PASI-C
MADEP VPH
LMB
6
PASI-C
EPA 8270E
BPJ
75
PASI-C
EPA 8260D
SAS
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
REPORT OF LABORATORY ANALYSIS
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leAnalyiical
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9800 Kincey Ave. Suite 100
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ANALYTICAL RESULTS
Project: HO UST
Pace Project No.: 92452986
Sample: SS-1 Lab ID: 92452986001 Collected: 11/08/19 11:20 Received: 11/08/19 13:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8015 GCS THC-Diesel
Diesel Range Organics(C10-
C28)
Surrogates
n-Pentacosane (S)
Gasoline Range Organics
Gas Range Organics (C6-C10)
Surrogates
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
166 mg/kg 6.4 2.9 1 11/08/19 21:13 11/11/19 15:56
69 % 33-129
1 11/08/19 21:13
11/11/19 15:56 629-99-2
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030E
3.1J mg/kg 7.6
1.4 1 11/09/19 13:00
11/10/19 00:15
100 % 63-130
1 11/09/19 13:00
11/10/19 00:15 460-00-4
Analytical Method: ASTM D2974-87
21.4 % 0.10
0.10 1
11/08/1917:53
Sample: SS-2 Lab ID: 92452986002 Collected: 11/08/19 11:25 Received: 11/08/19 13:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8015 GCS THC-Diesel
Diesel Range Organics(C10
C28)
Surrogates
n-Pentacosane (S)
�J_1e7=1»]:1"41&T71
Aliphatic (C09-C18)
Aliphatic (C19-C36)
Aromatic (C11-C22)
Surrogates
Nonatriacontane (S)
o-Terphenyl(S)
2-Fluorobiphenyl (S)
2-Bromonaphthalene (S)
Gasoline Range Organics
Gas Range Organics (C6-C10)
Surrogates
4-Bromofluorobenzene (S)
VPH NC Soil
Aliphatic (C05-CO8)
Aliphatic (C09-C12)
Aliphatic(C09-C12) Adjusted
Aromatic (C09-C10)
Date: 11/19/2019 03:45 PM
Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
5010 mg/kg 117 53.8 20 11/08/19 21:13 11/11/19 17:59
ill
%
33-129
20
11/08/19 21:13
11/11/19 17:59
629-99-2
Analytical
Method: MADEP EPH Preparation Method: MADEP EPH
3030
mg/kg
1170
1170
100
11/16/1916:18
11/19/1911:45
N2
<1170
mg/kg
1170
1170
100
11/16/1916:18
11/19/1911:45
N2
1460
mg/kg
234
234
20
11/16/1916:18
11/19/1911:45
N2
0
%
40-140
100
11/16/1916:18
11/19/1911:45
7194-86-7
S4
0
%
40-140
20
11/16/1916:18
11/19/1911:45
84-15-1
S4
0
%
40-140
20
11/16/1916:18
11/19/1911:45
321-60-8
S4
0
%
40-140
20
11/16/1916:18
11/19/1911:45
580-13-2
S4
Analytical
Method: EPA 8015C Modified Preparation Method: EPA 5030E
41.6
mg/kg
7.1
1.4
1
11/09/19 13:00
11/10/19 00:43
145
%
63-130
1
11/09/19 13:00
11/10/19 00:43
460-00-4
S5
Analytical
Method: MADEP VPH Preparation Method: MADEP VPH
28.1
mg/kg
2.3
2.3
1
11/13/1913:47
11/13/1916:56
N2
414
mg/kg
2.3
2.3
1
11/13/1913:47
11/13/1916:56
N2
190
mg/kg
2.3
2.3
1
11/13/1913:47
11/13/1916:56
N2
224
mg/kg
2.3
2.3
1
11/13/1913:47
11/13/1916:56
N2
REPORT OF LABORATORY ANALYSIS
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leAnalyiical
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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: HO UST
Pace Project No.: 92452986
Sample: SS-2
Lab ID:
92452986002
Collected:
11/08/19
11:25
Received: 11/08/19 13:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
PQL
MDL
DF
Prepared
Analyzed
CAS No. Qual
VPH NC Soil
Analytical Method: MADEP VPH Preparation Method: MADEP VPH
Surrogates
4-Bromofluorobenzene (FID) (S)
171
%
70-130
1
11/13/19 13:47
11/13/19 16:56
460-00-4 S5
4-Bromofluorobenzene (PID) (S)
114
%
70-130
1
11/13/19 13:47
11/13/19 16:56
460-00-4
8270E MSSV Microwave
Analytical
Method: EPA 8270E Preparation Method:
EPA 3546
Acenaphthene
<1010
ug/kg
3920
1010
10
11/13/19 16:01
11/14/19 17:09
83-32-9
Acenaphthylene
<929
ug/kg
3920
929
10
11/13/19 16:01
11/14/19 17:09
208-96-8
Aniline
<881
ug/kg
3920
881
10
11/13/19 16:01
11/14/19 17:09
62-53-3
Anthracene
<1020
ug/kg
3920
1020
10
11/13/19 16:01
11/14/19 17:09
120-12-7
Benzo(a)anthracene
<1250
ug/kg
3920
1250
10
11/13/19 16:01
11/14/19 17:09
56-55-3
Benzo(a)pyrene
<1700
ug/kg
3920
1700
10
11/13/19 16:01
11/14/19 17:09
50-32-8
Benzo(b)fluoranthene
<1580
ug/kg
3920
1580
10
11/13/19 16:01
11/14/19 17:09
205-99-2
Benzo(g,h,i)perylene
<1530
ug/kg
3920
1530
10
11/13/19 16:01
11/14/19 17:09
191-24-2
Benzo(k)fluoranthene
<1650
ug/kg
3920
1650
10
11/13/19 16:01
11/14/19 17:09
207-08-9
Benzoic Acid
<4230
ug/kg
19600
4230
10
11/13/19 16:01
11/14/19 17:09
65-85-0
Benzyl alcohol
<2080
ug/kg
7850
2080
10
11/13/19 16:01
11/14/19 17:09
100-51-6
4-Bromophenylphenyl ether
<1030
ug/kg
3920
1030
10
11/13/19 16:01
11/14/19 17:09
101-55-3
Butylbenzylphthalate
<1050
ug/kg
3920
1050
10
11/13/19 16:01
11/14/19 17:09
85-68-7
4-Chloro-3-methyl phenol
<2390
ug/kg
7850
2390
10
11/13/19 16:01
11/14/19 17:09
59-50-7
4-Chloroaniline
<2400
ug/kg
19600
2400
10
11/13/19 16:01
11/14/19 17:09
106-47-8
bis(2-Chloroethoxy)methane
<1050
ug/kg
3920
1050
10
11/13/19 16:01
11/14/19 17:09
111-91-1
bis(2-Chloroethyl) ether
<834
ug/kg
3920
834
10
11/13/19 16:01
11/14/19 17:09
111-44-4
2-Chloronaphthalene
<874
ug/kg
3920
874
10
11/13/19 16:01
11/14/19 17:09
91-58-7
2-Chlorophenol
<913
ug/kg
3920
913
10
11/13/19 16:01
11/14/19 17:09
95-57-8
4-Chlorophenylphenyl ether
<1020
ug/kg
3920
1020
10
11/13/19 16:01
11/14/19 17:09
7005-72-3
Chrysene
<1140
ug/kg
3920
1140
10
11/13/19 16:01
11/14/19 17:09
218-01-9
Dibenz(a,h)anthracene
<1570
ug/kg
3920
1570
10
11/13/19 16:01
11/14/19 17:09
53-70-3
Dibenzofuran
<981
ug/kg
3920
981
10
11/13/19 16:01
11/14/19 17:09
132-64-9
1,2-Dichlorobenzene
<849
ug/kg
3920
849
10
11/13/19 16:01
11/14/19 17:09
95-50-1
1,3-Dichlorobenzene
<884
ug/kg
3920
884
10
11/13/19 16:01
11/14/19 17:09
541-73-1
1,4-Dichlorobenzene
<863
ug/kg
3920
863
10
11/13/19 16:01
11/14/19 17:09
106-46-7
3,3'-Dichlorobenzidine
<2740
ug/kg
19600
2740
10
11/13/19 16:01
11/14/19 17:09
91-94-1
2,4-Dichlorophenol
<1300
ug/kg
3920
1300
10
11/13/19 16:01
11/14/19 17:09
120-83-2
Diethylphthalate
<852
ug/kg
3920
852
10
11/13/19 16:01
11/14/19 17:09
84-66-2
2,4-Dimethylphenol
<978
ug/kg
3920
978
10
11/13/19 16:01
11/14/19 17:09
105-67-9
Dimethylphthalate
<887
ug/kg
3920
887
10
11/13/19 16:01
11/14/19 17:09
131-11-3
Di-n-butylphthalate
<968
ug/kg
3920
968
10
11/13/19 16:01
11/14/19 17:09
84-74-2
4,6-Dinitro-2-methyl phenol
<6330
ug/kg
7850
6330
10
11/13/19 16:01
11/14/19 17:09
534-52-1
2,4-Dinitrophenol
<12500
ug/kg
19600
12500
10
11/13/19 16:01
11/14/19 17:09
51-28-5
2,4-Dinitrotoluene
<1040
ug/kg
3920
1040
10
11/13/19 16:01
11/14/19 17:09
121-14-2
2,6-Dinitrotoluene
<1030
ug/kg
3920
1030
10
11/13/19 16:01
11/14/19 17:09
606-20-2
Di-n-octylphthalate
<2240
ug/kg
3920
2240
10
11/13/19 16:01
11/14/19 17:09
117-84-0
bis(2- Ethyl hexyl)phthalate
<1280
ug/kg
3920
1280
10
11/13/19 16:01
11/14/19 17:09
117-81-7
Fluoranthene
<1190
ug/kg
3920
1190
10
11/13/19 16:01
11/14/19 17:09
206-44-0
Fluorene
4840
ug/kg
3920
1050
10
11/13/19 16:01
11/14/19 17:09
86-73-7
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: HO UST
Pace Project No.: 92452986
Sample: SS-2
Lab ID:
92452986002
Collected:
11/08/19
11:25
Received: 11/08/19 13:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
PQL
MDL
DF
Prepared
Analyzed
CAS No.
Qual
8270E MSSV Microwave
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Hexachloro-1,3-butadiene
<954
ug/kg
3920
954
10
11/13/19 16:01
11/14/19 17:09
87-68-3
Hexachlorobenzene
<997
ug/kg
3920
997
10
11/13/19 16:01
11/14/19 17:09
118-74-1
Hexachlorocyclopentadiene
<1570
ug/kg
3920
1570
10
11/13/19 16:01
11/14/19 17:09
77-47-4
Hexachloroethane
<894
ug/kg
3920
894
10
11/13/19 16:01
11/14/19 17:09
67-72-1
Indeno(1,2,3-cd)pyrene
<1800
ug/kg
3920
1800
10
11/13/19 16:01
11/14/19 17:09
193-39-5
Isophorone
<853
ug/kg
3920
853
10
11/13/19 16:01
11/14/19 17:09
78-59-1
1-Methylnaphthalene
32300
ug/kg
3920
1050
10
11/13/19 16:01
11/14/19 17:09
90-12-0
2-Methylnaphthalene
49200
ug/kg
7850
2000
20
11/13/19 16:01
11/15/1912:28
91-57-6
2-Methylphenol(o-Cresol)
<869
ug/kg
3920
869
10
11/13/19 16:01
11/14/19 17:09
95-48-7
3&4-Methyl phenol (m&p Cresol)
<987
ug/kg
3920
987
10
11/13/19 16:01
11/14/19 17:09
15831-10-4
Naphthalene
11400
ug/kg
3920
940
10
11/13/19 16:01
11/14/19 17:09
91-20-3
2-Nitroaniline
<1970
ug/kg
19600
1970
10
11/13/19 16:01
11/14/19 17:09
88-74-4
3-Nitroaniline
<2080
ug/kg
19600
2080
10
11/13/19 16:01
11/14/19 17:09
99-09-2
4-Nitroaniline
<1940
ug/kg
7850
1940
10
11/13/19 16:01
11/14/19 17:09
100-01-6
Nitrobenzene
<937
ug/kg
3920
937
10
11/13/19 16:01
11/14/19 17:09
98-95-3
2-Nitrophenol
<1210
ug/kg
3920
1210
10
11/13/19 16:01
11/14/19 17:09
88-75-5
4-Nitrophenol
<6260
ug/kg
19600
6260
10
11/13/19 16:01
11/14/19 17:09
100-02-7
N-Nitrosodimethylamine
<1100
ug/kg
3920
1100
10
11/13/19 16:01
11/14/19 17:09
62-75-9
N-Nitroso-di-n-propylamine
<1100
ug/kg
3920
1100
10
11/13/19 16:01
11/14/19 17:09
621-64-7
N-Nitrosodiphenylamine
<1000
ug/kg
3920
1000
10
11/13/19 16:01
11/14/19 17:09
86-30-6
2,2'-Oxybis(1-chloropropane)
<1090
ug/kg
3920
1090
10
11/13/19 16:01
11/14/19 17:09
108-60-1
Pentachlorophenol
<1800
ug/kg
19600
1800
10
11/13/19 16:01
11/14/19 17:09
87-86-5
Phenanthrene
11000
ug/kg
3920
988
10
11/13/19 16:01
11/14/19 17:09
85-01-8
Phenol
<937
ug/kg
3920
937
10
11/13/19 16:01
11/14/19 17:09
108-95-2
Pyrene
1290J
ug/kg
3920
1080
10
11/13/19 16:01
11/14/19 17:09
129-00-0
Pyridine
<993
ug/kg
3920
993
10
11/13/19 16:01
11/14/19 17:09
110-86-1
1,2,4-Trichlorobenzene
<899
ug/kg
3920
899
10
11/13/19 16:01
11/14/19 17:09
120-82-1
2,4,5-Trichlorophenol
<1020
ug/kg
3920
1020
10
11/13/19 16:01
11/14/19 17:09
95-95-4
2,4,6-Trichlorophenol
<986
ug/kg
3920
986
10
11/13/19 16:01
11/14/19 17:09
88-06-2
Surrogates
Nitrobenzene-d5 (S)
0
%
23-110
10
11/13/19 16:01
11/14/19 17:09
4165-60-0
D3,S4
2-Fluorobiphenyl (S)
0
%
30-110
10
11/13/19 16:01
11/14/19 17:09
321-60-8
S4
Terphenyl-d14 (S)
0
%
28-110
10
11/13/19 16:01
11/14/19 17:09
1718-51-0
S4
Phenol-d6 (S)
0
%
22-110
10
11/13/19 16:01
11/14/19 17:09
13127-88-3
S4
2-Fluorophenol (S)
0
%
13-110
10
11/13/19 16:01
11/14/19 17:09
367-12-4
S4
2,4,6-Tribromophenol (S)
0
%
27-110
10
11/13/19 16:01
11/14/19 17:09
118-79-6
S4
8260D/5035A Volatile Organics
Analytical
Method: EPA 8260D Preparation Method:
EPA 5035A
Acetone
<812
ug/kg
8610
812
100
11/13/1911:18
11/13/1919:45
67-64-1
Benzene
<77.2
ug/kg
430
77.2
100
11/13/1911:18
11/13/1919:45
71-43-2
Bromobenzene
<117
ug/kg
430
117
100
11/13/1911:18
11/13/1919:45
108-86-1
Bromochloromethane
<106
ug/kg
430
106
100
11/13/1911:18
11/13/1919:45
74-97-5
Bromodichloromethane
<84.2
ug/kg
430
84.2
100
11/13/1911:18
11/13/1919:45
75-27-4
Bromoform
<210
ug/kg
430
210
100
11/13/1911:18
11/13/1919:45
75-25-2
Bromomethane
<203
ug/kg
861
203
100
11/13/1911:18
11/13/1919:45
74-83-9
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: HO UST
Pace Project No.: 92452986
Sample: SS-2 Lab ID: 92452986002 Collected: 11/08/19 11:25 Received: 11/08/19 13:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
8260D/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
2-Butanone (MEK)
<1020
ug/kg
8610
1020
100
11/13/19 11:18
11/13/19 19:45
78-93-3
n-Butylbenzene
3610
ug/kg
430
243
100
11/13/19 11:18
11/13/19 19:45
104-51-8
sec-Butylbenzene
<182
ug/kg
430
182
100
11/13/19 11:18
11/13/19 19:45
135-98-8
tert-Butyl benzene
<145
ug/kg
430
145
100
11/13/19 11:18
11/13/19 19:45
98-06-6
Carbon tetrachloride
<82.4
ug/kg
430
82.4
100
11/13/19 11:18
11/13/19 19:45
56-23-5
Chlorobenzene
<83.3
ug/kg
430
83.3
100
11/13/19 11:18
11/13/19 19:45
108-90-7
Chloroethane
<180
ug/kg
861
180
100
11/13/19 11:18
11/13/19 19:45
75-00-3
Chloroform
<91.2
ug/kg
430
91.2
100
11/13/19 11:18
11/13/19 19:45
67-66-3
Chloromethane
<282
ug/kg
861
282
100
11/13/19 11:18
11/13/19 19:45
74-87-3
2-Chlorotoluene
<131
ug/kg
430
131
100
11/13/19 11:18
11/13/19 19:45
95-49-8
4-Chlorotoluene
<129
ug/kg
430
129
100
11/13/19 11:18
11/13/19 19:45
106-43-4
1,2-Dibromo-3-chloropropane
<219
ug/kg
430
219
100
11/13/19 11:18
11/13/19 19:45
96-12-8
Dibromochloromethane
<215
ug/kg
430
215
100
11/13/19 11:18
11/13/19 19:45
124-48-1
1,2-Dibromoethane (EDB)
<96.4
ug/kg
430
96.4
100
11/13/19 11:18
11/13/19 19:45
106-93-4
Dibromomethane
<128
ug/kg
430
128
100
11/13/19 11:18
11/13/19 19:45
74-95-3
1,2-Dichlorobenzene
<151
ug/kg
430
151
100
11/13/19 11:18
11/13/19 19:45
95-50-1
1,3-Dichlorobenzene
<153
ug/kg
430
153
100
11/13/19 11:18
11/13/19 19:45
541-73-1
1,4-Dichlorobenzene
<149
ug/kg
430
149
100
11/13/19 11:18
11/13/19 19:45
106-46-7
Dichlorodifluoromethane
<354
ug/kg
861
354
100
11/13/19 11:18
11/13/19 19:45
75-71-8
1,1-Dichloroethane
<63.2
ug/kg
430
63.2
100
11/13/19 11:18
11/13/19 19:45
75-34-3
1,2-Dichloroethane
<86.1
ug/kg
430
86.1
100
11/13/19 11:18
11/13/19 19:45
107-06-2
1,1-Dichloroethene
<99.8
ug/kg
430
99.8
100
11/13/19 11:18
11/13/19 19:45
75-35-4
cis-1,2-Dichloroethene
<74.7
ug/kg
430
74.7
100
11/13/19 11:18
11/13/19 19:45
156-59-2
trans-1,2-Dichloroethene
<84.4
ug/kg
430
84.4
100
11/13/19 11:18
11/13/19 19:45
156-60-5
1,2-Dichloropropane
<162
ug/kg
430
162
100
11/13/19 11:18
11/13/19 19:45
78-87-5
1,3-Dichloropropane
<163
ug/kg
430
163
100
11/13/19 11:18
11/13/19 19:45
142-28-9
2,2-Dichloropropane
<42.5
ug/kg
430
42.5
100
11/13/19 11:18
11/13/19 19:45
594-20-7
1,1-Dichloropropene
<182
ug/kg
430
182
100
11/13/19 11:18
11/13/19 19:45
563-58-6
cis-1,3-Dichloropropene
<195
ug/kg
430
195
100
11/13/19 11:18
11/13/19 19:45
10061-01-5
trans- 1,3-Dichloropropene
<75.3
ug/kg
430
75.3
100
11/13/19 11:18
11/13/19 19:45
10061-02-6
Diisopropyl ether
<246
ug/kg
430
246
100
11/13/19 11:18
11/13/19 19:45
108-20-3
Ethylbenzene
1850
ug/kg
430
91.2
100
11/13/19 11:18
11/13/19 19:45
100-41-4
Hexachloro-1,3-butadiene
<213
ug/kg
430
213
100
11/13/19 11:18
11/13/19 19:45
87-68-3
2-Hexanone
<446
ug/kg
4300
446
100
11/13/19 11:18
11/13/19 19:45
591-78-6
Isopropylbenzene (Cumene)
1650
ug/kg
430
125
100
11/13/19 11:18
11/13/19 19:45
98-82-8
p-Isopropyltoluene
<207
ug/kg
430
207
100
11/13/19 11:18
11/13/19 19:45
99-87-6
Methylene Chloride
<509
ug/kg
1720
509
100
11/13/19 11:18
11/13/19 19:45
75-09-2
4-Methyl-2-pentanone (MIBK)
1220J
ug/kg
4300
321
100
11/13/19 11:18
11/13/19 19:45
108-10-1
Methyl-tert-butyl ether
<246
ug/kg
430
246
100
11/13/19 11:18
11/13/19 19:45
1634-04-4
Naphthalene
9850
ug/kg
430
366
100
11/13/19 11:18
11/13/19 19:45
91-20-3
n-Propylbenzene
<144
ug/kg
430
144
100
11/13/19 11:18
11/13/19 19:45
103-65-1
Styrene
<127
ug/kg
430
127
100
11/13/19 11:18
11/13/19 19:45
100-42-5
1,1,1,2-Tetrachloroethane
<106
ug/kg
430
106
100
11/13/19 11:18
11/13/19 19:45
630-20-6
1,1,2,2-Tetrachloroethane
<149
ug/kg
430
149
100
11/13/19 11:18
11/13/19 19:45
79-34-5
Tetrachloroethene
<136
ug/kg
430
136
100
11/13/19 11:18
11/13/19 19:45
127-18-4
REPORT OF LABORATORY ANALYSIS
v2
IK
IK
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ANALYTICAL RESULTS
Project: HO UST
Pace Project No.: 92452986
Sample: SS-2 Lab ID: 92452986002 Collected: 11/08/19 11:25 Received: 11/08/19 13:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
8260D/5035A Volatile Organics
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 11/19/2019 03:45 PM
Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
<139
ug/kg
430
139
100
11/13/1911:18
11/13/1919:45
108-88-3
<307
ug/kg
430
307
100
11/13/1911:18
11/13/1919:45
87-61-6
<228
ug/kg
430
228
100
11/13/1911:18
11/13/1919:45
120-82-1
<74.9
ug/kg
430
74.9
100
11/13/1911:18
11/13/1919:45
71-55-6
<97.2
ug/kg
430
97.2
100
11/13/1911:18
11/13/1919:45
79-00-5
<112
ug/kg
430
112
100
11/13/1911:18
11/13/1919:45
79-01-6
<102
ug/kg
430
102
100
11/13/1911:18
11/13/1919:45
75-69-4
<145
ug/kg
430
145
100
11/13/1911:18
11/13/1919:45
96-18-4
17500
ug/kg
861
336
200
11/13/1911:18
11/14/1911:58
95-63-6
<144
ug/kg
430
144
100
11/13/1911:18
11/13/1919:45
108-67-8
<1400
ug/kg
4300
1400
100
11/13/1911:18
11/13/1919:45
108-05-4
<164
ug/kg
861
164
100
11/13/1911:18
11/13/1919:45
75-01-4
6430
ug/kg
861
301
100
11/13/1911:18
11/13/1919:45
1330-20-7
5640
ug/kg
861
203
100
11/13/1911:18
11/13/1919:45
179601-23-1
790
ug/kg
430
101
100
11/13/1911:18
11/13/1919:45
95-47-6
123
%
70-130
100
11/13/1911:18
11/13/1919:45
2037-26-5
105
%
70-130
100
11/13/1911:18
11/13/1919:45
460-00-4
89
%
70-132
100
11/13/1911:18
11/13/1919:45
17060-07-0
Analytical Method: ASTM D2974-87
15.9 % 0.10 0.10 1 11/08/1917:53
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 9 of 31

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QUALITY CONTROL DATA
Project: HO UST
Pace Project No.: 92452986
QC Batch: 508638 Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 5030E Analysis Description: Gasoline Range Organics
Associated Lab Samples: 92452986001, 92452986002
METHOD BLANK: 2730445 Matrix: Solid
Associated Lab Samples: 92452986001, 92452986002
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Gas Range Organics (C6-C10) mg/kg <1.1 6.0 1.1 11/09/19 16:07
4-Bromofluorobenzene (S) % 94 63-130 11/09/19 16:07
LABORATORY CONTROL SAMPLE:
2730446
Spike
LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
50
53.2
106
70-130
4-Bromofluorobenzene (S)
%
86
63-130
MATRIX SPIKE SAMPLE:
2730448
92452978012
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND
52.3
62.8
119
40-155
4-Bromofluorobenzene (S)
%
95
63-130
SAMPLE DUPLICATE: 2730447
92452978011
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND
<1.2
30
4-Bromofluorobenzene (S)
%
97
92
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11 /19/2019 03:45 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 31

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HO UST
Pace Project No.: 92452986
QC Batch: 509289 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Soil
Associated Lab Samples: 92452986002
METHOD BLANK: 2733199
Associated Lab Samples: 92452986002
Parameter
Aliphatic (C05-008)
Aliphatic (C09-C12)
Aromatic (C09-C10)
4-Bromofluorobenzene (FID) (S)
4-Bromofluorobenzene (PID) (S)
Matrix: Solid
Units
Blank
Result
Reporting
Limit
MDL Analyzed Qualifiers
mg/kg
<2.5
2.5
2.5 11/13/1914:58 N2
mg/kg
<2.5
2.5
2.5 11/13/1914:58 N2
mg/kg
<2.5
2.5
2.5 11/13/1914:58 N2
%
93
70-130
11/13/1914:58
%
94
70-130
11/13/1914:58
LABORATORY CONTROL SAMPLE & LCSD:
2733200
2733201
Spike
LCS LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-CO8)
mg/kg
14.9
13.5 13.6
91
91
70-130 0 25 N2
Aliphatic (C09-C12)
mg/kg
14.9
14.9 15.1
100
101
30-130 1 25 N2
Aromatic (C09-C10)
mg/kg
5
5.0 5.0
100
100
70-130 0 25 N2
4-Bromofluorobenzene (FID) (S)
%
97
100
70-130
4-Bromofluorobenzene (PID) (S)
%
97
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2019 03:45 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 31

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Huntersville, NC 28078
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QUALITY CONTROL DATA
Project: HO UST
Pace Project No.: 92452986
QC Batch: 509224 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A Analysis Description: 8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92452986002
METHOD BLANK: 2732927
Associated Lab Samples: 92452986002
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/kg
<1.2
5.0
1.2
11/13/19 12:31
1,1,1-Trichloroethane
ug/kg
<0.87
5.0
0.87
11/13/19 12:31
1,1,2,2-Tetrachloroethane
ug/kg
<1.7
5.0
1.7
11/13/19 12:31
1,1,2-Trichloroethane
ug/kg
<1.1
5.0
1.1
11/13/19 12:31
1,1-Dichloroethane
ug/kg
<0.74
5.0
0.74
11/13/19 12:31
1,1-Dichloroethene
ug/kg
<1.2
5.0
1.2
11/13/19 12:31
1,1-Dichloropropene
ug/kg
<2.1
5.0
2.1
11/13/19 12:31
1,2,3-Trichlorobenzene
ug/kg
<3.6
5.0
3.6
11/13/19 12:31
1,2,3-Trichloropropane
ug/kg
<1.7
5.0
1.7
11/13/19 12:31
1,2,4-Trichlorobenzene
ug/kg
<2.6
5.0
2.6
11/13/19 12:31
1,2,4-Trimethylbenzene
ug/kg
<2.0
5.0
2.0
11/13/19 12:31
1,2-Dibromo-3-chloropropane
ug/kg
<2.5
5.0
2.5
11/13/19 12:31
1,2-Dibromoethane (EDB)
ug/kg
<1.1
5.0
1.1
11/13/19 12:31
1,2-Dichlorobenzene
ug/kg
<1.8
5.0
1.8
11/13/19 12:31
1,2-Dichloroethane
ug/kg
<1.0
5.0
1.0
11/13/19 12:31
1,2-Dichloropropane
ug/kg
<1.9
5.0
1.9
11/13/19 12:31
1,3,5-Trimethylbenzene
ug/kg
<1.7
5.0
1.7
11/13/19 12:31
1,3-Dichlorobenzene
ug/kg
<1.8
5.0
1.8
11/13/19 12:31
1,3-Dichloropropane
ug/kg
<1.9
5.0
1.9
11/13/19 12:31
1,4-Dichlorobenzene
ug/kg
<1.7
5.0
1.7
11/13/19 12:31
2,2-Dichloropropane
ug/kg
<0.49
5.0
0.49
11/13/19 12:31
2-Butanone (MEK)
ug/kg
<11.9
100
11.9
11/13/19 12:31
2-Chlorotoluene
ug/kg
<1.5
5.0
1.5
11/13/19 12:31
2-Hexanone
ug/kg
<5.2
50.0
5.2
11/13/19 12:31
4-Chlorotoluene
ug/kg
<1.5
5.0
1.5
11/13/19 12:31
4-Methyl-2-pentanone (MIBK)
ug/kg
<3.7
50.0
3.7
11/13/19 12:31
Acetone
ug/kg
22.5J
100
9.4
11/13/19 12:31
Benzene
ug/kg
<0.90
5.0
0.90
11/13/19 12:31
Bromobenzene
ug/kg
<1.4
5.0
1.4
11/13/19 12:31
Bromochloromethane
ug/kg
<1.2
5.0
1.2
11/13/19 12:31
Bromodichloromethane
ug/kg
<0.98
5.0
0.98
11/13/19 12:31
Bromoform
ug/kg
<2.4
5.0
2.4
11/13/19 12:31
Bromomethane
ug/kg
<2.4
10.0
2.4
11/13/19 12:31
Carbon tetrachloride
ug/kg
<0.96
5.0
0.96
11/13/19 12:31
Chlorobenzene
ug/kg
<0.97
5.0
0.97
11/13/19 12:31
Chloroethane
ug/kg
<2.1
10.0
2.1
11/13/19 12:31
Chloroform
ug/kg
<1.1
5.0
1.1
11/13/19 12:31
Chloromethane
ug/kg
<3.3
10.0
3.3
11/13/19 12:31
cis-1,2-Dichloroethene
ug/kg
<0.87
5.0
0.87
11/13/19 12:31
cis-1,3-Dichloropropene
ug/kg
<2.3
5.0
2.3
11/13/19 12:31
Dibromochloromethane
ug/kg
<2.5
5.0
2.5
11/13/19 12:31
IK
v2
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2019 03:45 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HO UST
Pace Project No.: 92452986
METHOD BLANK: 2732927
Associated Lab Samples: 92452986002
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
Dibromomethane
ug/kg
<1.5
5.0
1.5
11/13/19 12:31
Dichlorodifluoromethane
ug/kg
<4.1
10.0
4.1
11/13/19 12:31
Diisopropyl ether
ug/kg
<2.9
5.0
2.9
11/13/19 12:31
Ethylbenzene
ug/kg
<1.1
5.0
1.1
11/13/19 12:31
Hexachloro-1,3-butadiene
ug/kg
<2.5
5.0
2.5
11/13/19 12:31
Isopropylbenzene (Cumene)
ug/kg
<1.4
5.0
1.4
11/13/19 12:31
m&p-Xylene
ug/kg
<2.4
10.0
2.4
11/13/19 12:31
Methyl-tert-butyl ether
ug/kg
<2.9
5.0
2.9
11/13/19 12:31
Methylene Chloride
ug/kg
<5.9
20.0
5.9
11/13/19 12:31
n-Butylbenzene
ug/kg
<2.8
5.0
2.8
11/13/19 12:31
n-Propylbenzene
ug/kg
<1.7
5.0
1.7
11/13/19 12:31
Naphthalene
ug/kg
<4.2
5.0
4.2
11/13/19 12:31
o-Xylene
ug/kg
<1.2
5.0
1.2
11/13/19 12:31
p-Isopropyltoluene
ug/kg
<2.4
5.0
2.4
11/13/19 12:31
sec-Butylbenzene
ug/kg
<2.1
5.0
2.1
11/13/19 12:31
Styrene
ug/kg
<1.5
5.0
1.5
11/13/19 12:31
tert-Butyl benzene
ug/kg
<1.7
5.0
1.7
11/13/19 12:31
Tetrachloroethene
ug/kg
<1.6
5.0
1.6
11/13/19 12:31
Toluene
ug/kg
<1.6
5.0
1.6
11/13/19 12:31
trans-1,2-Dichloroethene
ug/kg
<0.98
5.0
0.98
11/13/19 12:31
trans- 1,3-Dichloropropene
ug/kg
<0.88
5.0
0.88
11/13/19 12:31
Trichloroethene
ug/kg
<1.3
5.0
1.3
11/13/19 12:31
Trichlorofluoromethane
ug/kg
<1.2
5.0
1.2
11/13/19 12:31
Vinyl acetate
ug/kg
<16.3
50.0
16.3
11/13/19 12:31
Vinyl chloride
ug/kg
<1.9
10.0
1.9
11/13/19 12:31
Xylene (Total)
ug/kg
<3.5
10.0
3.5
11/13/19 12:31
1,2-Dichloroethane-d4 (S)
%
83
70-132
11/13/19 12:31
4-Bromofluorobenzene (S)
%
96
70-130
11/13/19 12:31
Toluene-d8 (S)
%
105
70-130
11/13/19 12:31
IK
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2732928
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
50
47.4
95
70-130
1,1,1-Trichloroethane
ug/kg
50
54.2
108
70-130
1,1,2,2-Tetrachloroethane
ug/kg
50
45.6
91
55-130
1,1,2-Trichloroethane
ug/kg
50
45.8
92
70-130
1,1-Dichloroethane
ug/kg
50
49.8
100
68-130
1,1-Dichloroethene
ug/kg
50
55.8
112
70-130
1,1-Dichloropropene
ug/kg
50
48.3
97
70-130IK
1,2,3-Trichlorobenzene
ug/kg
50
47.6
95
70-130
1,2,3-Trichloropropane
ug/kg
50
45.8
92
70-130
1,2,4-Trichlorobenzene
ug/kg
50
49.6
99
70-130
1,2,4-Trimethylbenzene
ug/kg
50
45.4
91
69-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2019 03:45 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HO UST
Pace Project No.: 92452986
LABORATORY CONTROL SAMPLE:
Parameter
2732928
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2-Dibromo-3-chloropropane
ug/kg
50
43.0
86
57-141
1,2-Dibromoethane (EDB)
ug/kg
50
45.8
92
70-130
1,2-Dichlorobenzene
ug/kg
50
47.1
94
70-130
1,2-Dichloroethane
ug/kg
50
43.3
87
70-130
1,2-Dichloropropane
ug/kg
50
47.5
95
70-130
1,3,5-Trimethylbenzene
ug/kg
50
46.2
92
70-130
1,3-Dichlorobenzene
ug/kg
50
49.7
99
70-130
1,3-Dichloropropane
ug/kg
50
38.9
78
70-130 v3
1,4-Dichlorobenzene
ug/kg
50
47.6
95
70-130
2,2-Dichloropropane
ug/kg
50
51.0
102
70-130
2-Butanone (MEK)
ug/kg
100
86.7J
87
60-130
2-Chlorotoluene
ug/kg
50
48.5
97
70-130
2-Hexanone
ug/kg
100
88.7
89
70-132
4-Chlorotoluene
ug/kg
50
48.0
96
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
100
86.3
86
69-130
Acetone
ug/kg
100
90AJ
90
49-148
Benzene
ug/kg
50
49.9
100
70-130
Bromobenzene
ug/kg
50
49.2
98
70-130
Bromochloromethane
ug/kg
50
48.1
96
70-130
Bromodichloromethane
ug/kg
50
47.4
95
70-130
Bromoform
ug/kg
50
45.4
91
68-136
Bromomethane
ug/kg
50
55.4
111
60-140
Carbon tetrachloride
ug/kg
50
59.1
118
70-130
Chlorobenzene
ug/kg
50
48.0
96
70-130
Chloroethane
ug/kg
50
53.6
107
51-147
Chloroform
ug/kg
50
42.4
85
70-130
Chloromethane
ug/kg
50
49.0
98
48-130
cis-1,2-Dichloroethene
ug/kg
50
49.7
99
70-130
cis-1,3-Dichloropropene
ug/kg
50
48.8
98
70-130
Dibromochloromethane
ug/kg
50
39.7
79
70-130
Dibromomethane
ug/kg
50
47.1
94
70-130
Dichlorodifluoromethane
ug/kg
50
55.3
111
49-130
Diisopropyl ether
ug/kg
50
49.7
99
66-130
Ethylbenzene
ug/kg
50
48.7
97
70-130
Hexachloro-1,3-butadiene
ug/kg
50
53.2
106
70-130
Isopropylbenzene (Cumene)
ug/kg
50
51.3
103
70-130
m&p-Xylene
ug/kg
100
99.1
99
70-130
Methyl-tert-butyl ether
ug/kg
50
42.5
85
70-130 IK
Methylene Chloride
ug/kg
50
50.7
101
50-137
n-Butylbenzene
ug/kg
50
48.5
97
70-130
n-Propylbenzene
ug/kg
50
49.1
98
70-130
Naphthalene
ug/kg
50
48.8
98
70-131
o-Xylene
ug/kg
50
47.8
96
70-130
p-Isopropyltoluene
ug/kg
50
47.7
95
70-130
sec-Butylbenzene
ug/kg
50
49.6
99
70-130
Styrene
ug/kg
50
47.5
95
70-130
tert-Butyl benzene
ug/kg
50
48.2
96
69-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2019 03:45 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 31

leAnalyiical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HO UST
Pace Project No.: 92452986
LABORATORY CONTROL SAMPLE:
Parameter
2732928
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Tetrachloroethene
ug/kg
50
53.0
106
56-130
Toluene
ug/kg
50
48.3
97
70-130
trans-1,2-Dichloroethene
ug/kg
50
53.2
106
70-130
trans- 1,3-Dichloropropene
ug/kg
50
46.3
93
70-130
Trichloroethene
ug/kg
50
50.1
100
70-141
Trichlorofluoromethane
ug/kg
50
55.4
111
67-130
Vinyl acetate
ug/kg
100
81.8
82
10-136
Vinyl chloride
ug/kg
50
59.1
118
67-130
Xylene (Total)
ug/kg
150
147
98
70-130
1,2-Dichloroethane-d4 (S)
%
96
70-132
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
98
70-130
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2732929
MS
92452990002 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2732930
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
Max
RPD Qual
1,1,1,2-Tetrachloroethane
ug/kg
ND
6400
6400
8240
7580
129
118
52-133
8
30
1,1,1-Trichloroethane
ug/kg
ND
6400
6400
7770
7660
121
120
49-137
1
30
1,1,2,2-Tetrachloroethane
ug/kg
ND
6400
6400
8380
7810
131
122
39-150
7
30
1,1,2-Trichloroethane
ug/kg
ND
6400
6400
7370
7410
115
116
48-140
1
30
1,1-Dichloroethane
ug/kg
ND
6400
6400
7680
7770
120
121
46-135
1
30
1,1-Dichloroethene
ug/kg
ND
6400
6400
7890
8000
123
125
38-149
1
30
1,1-Dichloropropene
ug/kg
ND
6400
6400
8790
8640
137
135
41-140
2
30
1,2,3-Trichlorobenzene
ug/kg
ND
6400
6400
9180
8390
143
131
10-158
9
30
1,2,3-Trichooropropane
ug/kg
ND
6400
6400
7870
7000
123
109
33-157
12
30
1,2,4-Trichlorobenzene
ug/kg
ND
6400
6400
8700
8300
136
130
10-155
5
30
1,2,4-Trimethyl benzene
ug/kg
81800
6400
6400
96000
89100
221
113
24-154
7
30 E,M1
1,2-Dibromo-3-
ug/kg
ND
6400
6400
8110
7660
127
120
33-158
6
30
chloropropane
1,2-Dibromoethane (EDB)
ug/kg
ND
6400
6400
8330
7800
130
122
40-136
7
30
1,2-Dichlorobenzene
ug/kg
ND
6400
6400
7910
7610
124
119
27-146
4
30
1,2-Dichloroethane
ug/kg
ND
6400
6400
7430
7410
116
116
49-140
0
30
1,2-Dichloropropane
ug/kg
ND
6400
6400
8290
8030
129
125
44-143
3
30
1,3,5-Trimethyl benzene
ug/kg
ND
6400
6400
12700
12300
199
193
40-144
3
30 M1
1,3-Dichlorobenzene
ug/kg
ND
6400
6400
8010
7820
125
122
33-140
2
30
1,3-Dichloropropane
ug/kg
ND
6400
6400
8250
8040
129
126
47-147
3
30
1,4-Dichlorobenzene
ug/kg
ND
6400
6400
7780
7560
122
118
35-139
3
30
2,2-Dichloropropane
ug/kg
ND
6400
6400
8240
7680
129
120
41-140
7
30
2-Butanone (MEK)
ug/kg
ND
12800
12800
27300J
23900J
213
187
10-181
30 M1
2-Chlorotoluene
ug/kg
ND
6400
6400
11200
11000
176
172
38-147
2
30 M1
2-Hexanone
ug/kg
ND
12800
12800
16800
16900
132
132
18-169
0
30
4-Chlorotoluene
ug/kg
ND
6400
6400
7780
7490
122
117
36-145
4
30
4-Methyl-2-pentanone
ug/kg
ND
12800
12800
23500
21200
165
147
16-175
10
30
(MIBK)
Acetone
ug/kg
ND
12800
12800
19700J
14800J
154
116
10-200
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
Date: 11/19/2019 03:45 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HO UST
Pace Project No.: 92452986
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 2732929
2732930
MS
MSD
92452990002
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
Benzene
ug/kg
ND
6400
6400
9270
9010
122
118
46-136
3
30
Bromobenzene
ug/kg
ND
6400
6400
8080
7790
126
122
38-149
4
30
Bromochloromethane
ug/kg
ND
6400
6400
7570
7400
118
116
44-142
2
30
Bromodichloromethane
ug/kg
ND
6400
6400
7610
7450
119
116
41-140
2
30
Bromoform
ug/kg
ND
6400
6400
7580
7060
118
110
34-145
7
30
Bromomethane
ug/kg
ND
6400
6400
10200
10100
159
157
14-162
1
30
Carbon tetrachloride
ug/kg
ND
6400
6400
7960
7630
124
119
44-141
4
30
Chlorobenzene
ug/kg
ND
6400
6400
7740
7480
121
117
39-141
4
30
Chloroethane
ug/kg
ND
6400
6400
7880
8240
123
129
10-182
4
30
Chloroform
ug/kg
ND
6400
6400
8160
8290
128
129
45-140
1
30
Chloromethane
ug/kg
ND
6400
6400
7580
7270
118
114
19-149
4
30
cis-1,2-Dichloroethene
ug/kg
ND
6400
6400
7590
7670
119
120
38-150
1
30
cis-1,3-Dichloropropene
ug/kg
ND
6400
6400
8150
7930
127
124
30-144
3
30
Dibromochloromethane
ug/kg
ND
6400
6400
7590
7300
119
114
36-145
4
30
Dibromomethane
ug/kg
ND
6400
6400
7200
7280
113
114
41-145
1
30
Dichlorodifluoromethane
ug/kg
ND
6400
6400
8010
7820
125
122
16-146
2
30
Diisopropyl ether
ug/kg
ND
6400
6400
7920
7670
124
120
41-143
3
30
Ethylbenzene
ug/kg
34800
6400
6400
42300
39700
117
76
35-144
6
30
Hexachloro-1,3-butadiene
ug/kg
ND
6400
6400
8490
8120
133
127
10-160
5
30
Isopropylbenzene
ug/kg
3870
6400
6400
11700
11100
122
113
30-152
5
30
(Cumene)
m&p-Xylene
ug/kg
52400
12800
12800
68200
64700
123
96
33-145
5
30
Methyl-tert-butyl ether
ug/kg
ND
6400
6400
7870
7620
123
119
49-140
3
30
Methylene Chloride
ug/kg
ND
6400
6400
6880
6960
108
109
10-174
1
30
n-Butylbenzene
ug/kg
3530
6400
6400
12500
12000
140
132
10-160
4
30
n-Propylbenzene
ug/kg
12800
6400
6400
20800
20000
125
112
24-159
4
30
Naphthalene
ug/kg
12100
6400
6400
21900
20800
154
136
10-171
5
30
o-Xylene
ug/kg
ND
6400
6400
8760
8610
122
119
31-150
2
30
p-Isopropyltoluene
ug/kg
ND
6400
6400
9740
9170
152
143
21-154
6
30
sec-Butylbenzene
ug/kg
ND
6400
6400
8860
8670
138
135
19-159
2
30
Styrene
ug/kg
ND
6400
6400
7950
7540
124
118
15-152
5
30
tert-Butylbenzene
ug/kg
ND
6400
6400
7100
6970
111
109
31-141
2
30
Tetrachloroethene
ug/kg
ND
6400
6400
7860
7470
123
117
19-141
5
30
Toluene
ug/kg
1610
6400
6400
8940
8690
114
111
31-146
3
30
trans-1,2-Dichloroethene
ug/kg
ND
6400
6400
7810
7830
122
122
28-157
0
30
trans-1,3-Dichloropropene
ug/kg
ND
6400
6400
7820
7710
122
121
25-146
1
30
Trichloroethene
ug/kg
ND
6400
6400
7990
7690
125
120
34-149
4
30
Trichlorofluoromethane
ug/kg
ND
6400
6400
7740
7940
121
124
10-167
3
30
Vinyl acetate
ug/kg
ND
12800
12800
18000
15300J
140
119
10-200
30 v1
Vinyl chloride
ug/kg
ND
6400
6400
8630
8720
135
136
36-155
1
30
Xylene (Total)
ug/kg
52400
19200
19200
76900
73300
128
109
29-148
5
30
1,2-Dichloroethane-d4 (S)
%
102
102
70-132
4-Bromofluorobenzene (S)
%
103
101
70-130
Toluene-d8 (S)
%
97
97
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2019 03:45 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HO UST
Pace Project No.: 92452986
QC Batch: 508576 Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 3546 Analysis Description: 8015 Solid GCSV
Associated Lab Samples: 92452986001, 92452986002
METHOD BLANK: 2730261 Matrix: Solid
Associated Lab Samples: 92452986001, 92452986002
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Diesel Range Organics(C10-C28) mg/kg <2.3 5.0 2.3 11/11/19 10:52
n-Pentacosane (S) % 77 33-129 11/11/19 10:52
LABORATORY CONTROL SAMPLE:
2730262
Spike
LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
66.2
46.0
69
43-130
n-Pentacosane (S)
%
66
33-129
MATRIX SPIKE SAMPLE:
2730266
92453048001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
3040 76.4
3630
767
10-130 M1
n-Pentacosane(S)
%
110
33-129
SAMPLE DUPLICATE: 2730267
92453047001
Dup
Max
Parameter
Units
Result
Result
RPD
RPD
Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
ND
<2.8
30
n-Pentacosane (S)
%
54
61
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2019 03:45 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HO UST
Pace Project No.: 92452986
QC Batch: 509329 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E Solid MSSV Microwave
Associated Lab Samples: 92452986002
METHOD BLANK: 2733527
Associated Lab Samples: 92452986002
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
1,2,4-Trichlorobenzene
ug/kg
<74.4
325
74.4
11/14/19 11:38
1,2-Dichlorobenzene
ug/kg
<70.2
325
70.2
11/14/19 11:38
1,3-Dichlorobenzene
ug/kg
<73.1
325
73.1
11/14/19 11:38
1,4-Dichlorobenzene
ug/kg
<71.4
325
71.4
11/14/19 11:38
1-Methylnaphthalene
ug/kg
<86.5
325
86.5
11/14/19 11:38
2,2'-Oxybis(1-chloropropane)
ug/kg
<90.2
325
90.2
11/14/19 11:38
2,4,5-Trichlorophenol
ug/kg
<84.3
325
84.3
11/14/19 11:38
2,4,6-Trichlorophenol
ug/kg
<81.5
325
81.5
11/14/19 11:38
2,4-Dichlorophenol
ug/kg
<107
325
107
11/14/19 11:38
2,4-Dimethylphenol
ug/kg
<80.9
325
80.9
11/14/19 11:38
2,4-Din itrophenol
ug/kg
<1040
1620
1040
11/14/19 11:38
2,4-Dinitrotoluene
ug/kg
<86.0
325
86.0
11/14/19 11:38
2,6-Dinitrotoluene
ug/kg
<84.9
325
84.9
11/14/19 11:38
2-Chloronaphthalene
ug/kg
<72.3
325
72.3
11/14/19 11:38
2-Chlorophenol
ug/kg
<75.5
325
75.5
11/14/19 11:38
2-Methylnaphthalene
ug/kg
<82.6
325
82.6
11/14/19 11:38
2-Methylphenol(o-Cresol)
ug/kg
<71.9
325
71.9
11/14/19 11:38
2-Nitroaniline
ug/kg
<163
1620
163
11/14/19 11:38
2-Nitrophenol
ug/kg
<100
325
100
11/14/19 11:38
3&4-Methyl phenol (m&p Cresol)
ug/kg
<81.6
325
81.6
11/14/19 11:38
3,3'-Dichlorobenzidine
ug/kg
<226
1620
226
11/14/19 11:38
3-Nitroaniline
ug/kg
<172
1620
172
11/14/19 11:38
4,6-Dinitro-2-methyl phenol
ug/kg
<523
649
523
11/14/19 11:38
4-Bromophenylphenyl ether
ug/kg
<85.2
325
85.2
11/14/19 11:38
4-ChIoro-3-methyl phenol
ug/kg
<198
649
198
11/14/19 11:38
4-Chloroaniline
ug/kg
<199
1620
199
11/14/19 11:38
4-Chlorophenylphenyl ether
ug/kg
<84.3
325
84.3
11/14/19 11:38
4-Nitroaniline
ug/kg
<160
649
160
11/14/19 11:38
4-Nitrophenol
ug/kg
<517
1620
517
11/14/19 11:38
Acenaphthene
ug/kg
<83.5
325
83.5
11/14/19 11:38
Acenaphthylene
ug/kg
<76.8
325
76.8
11/14/19 11:38
Aniline
ug/kg
<72.9
325
72.9
11/14/19 11:38
Anthracene
ug/kg
<84.2
325
84.2
11/14/19 11:38
Benzo(a)anthracene
ug/kg
<103
325
103
11/14/19 11:38
Benzo(a)pyrene
ug/kg
<141
325
141
11/14/19 11:38
Benzo(b)fluoranthene
ug/kg
<131
325
131
11/14/19 11:38
Benzo(g,h,i)perylene
ug/kg
<127
325
127
11/14/19 11:38
Benzo(k)fluoranthene
ug/kg
<137
325
137
11/14/19 11:38
Benzoic Acid
ug/kg
<350
1620
350
11/14/19 11:38
Benzyl alcohol
ug/kg
<172
649
172
11/14/19 11:38
bis(2-Chloroethoxy)methane
ug/kg
<86.7
325
86.7
11/14/19 11:38
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2019 03:45 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HO UST
Pace Project No.: 92452986
METHOD BLANK: 2733527
Associated Lab Samples: 92452986002
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
MDL
Analyzed
bis(2-Chloroethyl) ether
ug/kg
<69.0
325
69.0
11/14/19 11:38
bis(2-Ethylhexyl)phthalate
ug/kg
<106
325
106
11/14/19 11:38
Butylbenzylphthalate
ug/kg
<86.5
325
86.5
11/14/19 11:38
Chrysene
ug/kg
<94.2
325
94.2
11/14/19 11:38
Di-n-butylphthalate
ug/kg
<80.1
325
80.1
11/14/19 11:38
Di-n-octylphthalate
ug/kg
<185
325
185
11/14/19 11:38
Dibenz(a,h)anthracene
ug/kg
<130
325
130
11/14/19 11:38
Dibenzofuran
ug/kg
<81.1
325
81.1
11/14/19 11:38
Diethylphthalate
ug/kg
<70.4
325
70.4
11/14/19 11:38
Dimethylphthalate
ug/kg
<73.4
325
73.4
11/14/19 11:38
Fluoranthene
ug/kg
<98.1
325
98.1
11/14/19 11:38
Fluorene
ug/kg
<86.9
325
86.9
11/14/19 11:38
Hexachloro-1,3-butadiene
ug/kg
<78.9
325
78.9
11/14/19 11:38
Hexachlorobenzene
ug/kg
<82.4
325
82.4
11/14/19 11:38
Hexachlorocyclopentadiene
ug/kg
<130
325
130
11/14/19 11:38
Hexachloroethane
ug/kg
<74.0
325
74.0
11/14/19 11:38
Indeno(1,2,3-cd)pyrene
ug/kg
<149
325
149
11/14/19 11:38
Isophorone
ug/kg
<70.5
325
70.5
11/14/19 11:38
N-Nitroso-di-n-propylamine
ug/kg
<90.9
325
90.9
11/14/19 11:38
N-Nitrosodimethylamine
ug/kg
<91.3
325
91.3
11/14/19 11:38
N-Nitrosodiphenylamine
ug/kg
<82.8
325
82.8
11/14/19 11:38
Naphthalene
ug/kg
<77.7
325
77.7
11/14/19 11:38
Nitrobenzene
ug/kg
<77.5
325
77.5
11/14/19 11:38
Pentachlorophenol
ug/kg
<149
1620
149
11/14/19 11:38
Phenanthrene
ug/kg
<81.7
325
81.7
11/14/19 11:38
Phenol
ug/kg
<77.5
325
77.5
11/14/19 11:38
Pyrene
ug/kg
<89.3
325
89.3
11/14/19 11:38
Pyridine
ug/kg
<82.1
325
82.1
11/14/19 11:38
2,4,6-Tribromophenol (S)
%
69
27-110
11/14/19 11:38
2-Fluorobiphenyl (S)
%
68
30-110
11/14/19 11:38
2-Fluorophenol (S)
%
65
13-110
11/14/19 11:38
Nitrobenzene-d5 (S)
%
66
23-110
11/14/19 11:38
Phenol-d6 (S)
%
65
22-110
11/14/19 11:38
Terphenyl-d14 (S)
%
80
28-110
11/14/19 11:38
Qualifiers
LABORATORY CONTROL SAMPLE:
2733528
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1690
1220
72
52-130
1,2-Dichlorobenzene
ug/kg
1690
1230
73
51-130
1,3-Dichlorobenzene
ug/kg
1690
1210
72
50-130
1,4-Dichlorobenzene
ug/kg
1690
1250
74
49-130
1-Methylnaphthalene
ug/kg
1690
1220
72
55-130
2,2'-Oxybis(1-chloropropane)
ug/kg
1690
1150
68
30-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2019 03:45 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HO UST
Pace Project No.: 92452986
LABORATORY CONTROL SAMPLE:
Parameter
2733528
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,4,5-Trichlorophenol
ug/kg
1690
1250
74
55-130
2,4,6-Trichlorophenol
ug/kg
1690
1280
76
57-130
2,4-Dichlorophenol
ug/kg
1690
1220
72
56-130
2,4-Dimethylphenol
ug/kg
1690
1250
74
51-130
2,4-Dinitrophenol
ug/kg
8450
5680
67
27-133
2,4-Dinitrotoluene
ug/kg
1690
1350
80
61-130
2,6-Dinitrotoluene
ug/kg
1690
1320
78
60-130
2-Chloronaphthalene
ug/kg
1690
1270
75
52-130
2-Chlorophenol
ug/kg
1690
1260
75
54-130
2-Methylnaphthalene
ug/kg
1690
1230
73
54-130
2-Methylphenol(o-Cresol)
ug/kg
1690
1200
71
51-130
2-Nitroaniline
ug/kg
3380
2720
80
51-130
2-Nitrophenol
ug/kg
1690
1170
69
49-130
3&4-Methyl phenol (m&p Cresol)
ug/kg
1690
1210
72
11-163
3,3'-Dichlorobenzidine
ug/kg
3380
1760
52
10-132
3-Nitroaniline
ug/kg
3380
2160
64
55-130
4,6-Dinitro-2-methyl phenol
ug/kg
3380
2890
86
47-142
4-Bromophenylphenyl ether
ug/kg
1690
1310
78
59-130
4-ChIoro-3-methyl phenol
ug/kg
3380
2550
75
55-130
4-Chloroaniline
ug/kg
3380
2320
69
54-130
4-Chlorophenylphenyl ether
ug/kg
1690
1290
76
58-130
4-Nitroaniline
ug/kg
3380
2450
73
54-130
4-Nitrophenol
ug/kg
8450
6550
78
48-130
Acenaphthene
ug/kg
1690
1330
79
60-130
Acenaphthylene
ug/kg
1690
1440
85
60-130
Aniline
ug/kg
1690
1100
65
43-130
Anthracene
ug/kg
1690
1440
85
63-130
Benzo(a)anthracene
ug/kg
1690
1400
83
59-130
Benzo(a)pyrene
ug/kg
1690
1450
86
57-130
Benzo(b)fluoranthene
ug/kg
1690
1390
82
54-130
Benzo(g,h,i)perylene
ug/kg
1690
1460
87
59-130
Benzo(k)fluoranthene
ug/kg
1690
1420
84
54-130
Benzoic Acid
ug/kg
8450
4000
47
19-130
Benzyl alcohol
ug/kg
3380
2250
66
50-130
bis(2-Chloroethoxy)methane
ug/kg
1690
1180
70
54-130
bis(2-Chloroethyl) ether
ug/kg
1690
1270
75
48-130
bis(2-Ethylhexyl)phthalate
ug/kg
1690
1280
76
45-134
Butylbenzylphthalate
ug/kg
1690
1290
76
46-138
Chrysene
ug/kg
1690
1310
78
58-130
Di-n-butylphthalate
ug/kg
1690
1270
75
60-130
Di-n-octylphthalate
ug/kg
1690
1300
77
53-130
Dibenz(a,h)anthracene
ug/kg
1690
1460
87
59-130
Dibenzofuran
ug/kg
1690
1300
77
60-130
Diethylphthalate
ug/kg
1690
1320
78
60-130
Dimethylphthalate
ug/kg
1690
1290
77
60-130
Fluoranthene
ug/kg
1690
1360
80
65-130
Fluorene
ug/kg
1690
1380
82
63-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2019 03:45 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HO UST
Pace Project No.: 92452986
LABORATORY CONTROL SAMPLE:
2733528
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Hexachloro-1,3-butadiene
ug/kg
1690
1180
70
46-130
Hexachlorobenzene
ug/kg
1690
1320
78
58-130
Hexachlorocyclopentadiene
ug/kg
1690
1280
76
23-130
Hexachloroethane
ug/kg
1690
1210
72
47-130
Indeno(1,2,3-cd)pyrene
ug/kg
1690
1460
87
60-130
Isophorone
ug/kg
1690
1250
74
49-130
N-Nitroso-di-n-propylamine
ug/kg
1690
1310
78
47-130
N-Nitrosodimethylamine
ug/kg
1690
1290
76
45-130
N-Nitrosodiphenylamine
ug/kg
1690
1310
77
59-130
Naphthalene
ug/kg
1690
1260
75
55-130
Nitrobenzene
ug/kg
1690
1230
73
49-130
Pentachlorophenol
ug/kg
3380
2170
64
10-132
Phenanthrene
ug/kg
1690
1370
81
62-130
Phenol
ug/kg
1690
1320
78
46-130
Pyrene
ug/kg
1690
1380
81
53-130
Pyridine
ug/kg
1690
914
54
37-130
2,4,6-Tribromophenol (S)
%
85
27-110
2-Fluorobiphenyl (S)
%
76
30-110
2-Fluorophenol(S)
%
76
13-110
Nitrobenzene-d5(S)
%
74
23-110
Phenol-d6 (S)
%
79
22-110
Terphenyl-d14 (S)
%
80
28-110
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 2733529
2733530
MS
MSD
92452841003
Spike
Spike
MS
MSD
MS MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD
RPD Qual
1,2,4-Trichoorobenzene
ug/kg
ND
2030
2060
1410
1460
69
70
18-130
4
30
1,2-Dichlorobenzene
ug/kg
ND
2030
2060
1370
1350
67
65
14-130
1
30
1,3-Dichlorobenzene
ug/kg
ND
2030
2060
1380
1400
68
67
12-130
1
30
1,4-Dichlorobenzene
ug/kg
ND
2030
2060
1420
1370
70
66
10-130
4
30
1-Methyl naphthalene
ug/kg
ND
2030
2060
1360
1410
67
68
12-130
3
30
2,2'-Oxybis(1-
ug/kg
ND
2030
2060
1290
1320
64
64
10-130
2
30
chloropropane)
2,4,5-Trichlorophenol
ug/kg
ND
2030
2060
225J
340J
11
16
13-130
30 M1
2,4,6-Trichlorophenol
ug/kg
ND
2030
2060
<101
103J
3
5
17-130
30 M1
2,4-Dichlorophenol
ug/kg
ND
2030
2060
432
577
21
28
10-130
29
30
2,4-Dimethylphenol
ug/kg
ND
2030
2060
1310
1390
64
67
10-130
6
30
2,4-Dinitrophenol
ug/kg
ND
10200
10300
<1280
<1310
0
0
10-130
30 M1
2,4-Dinitrotoluene
ug/kg
ND
2030
2060
1390
1460
69
71
24-130
5
30
2,6-Dinitrotoluene
ug/kg
ND
2030
2060
1470
1600
73
77
23-130
8
30
2-Chloronaphthalene
ug/kg
ND
2030
2060
1400
1420
69
68
19-130
2
30
2-Chlorophenol
ug/kg
ND
2030
2060
465
607
23
29
10-130
27
30
2-Methyl naphthalene
ug/kg
ND
2030
2060
1380
1430
68
69
18-130
4
30
2-Methyl phenol(o-Cresol)
ug/kg
ND
2030
2060
1230
1280
60
62
10-130
4
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2019 03:45 PM without the written consent of Pace Analytical Services, LLC.
Page 21 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HO UST
Pace Project No.: 92452986
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 2733529
2733530
MS
MSD
92452841003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
2-Nitroaniline
ug/kg
ND
4060
4140
3100
3160
76
76
17-130
2
30
2-Nitrophenol
ug/kg
ND
2030
2060
381J
499
19
24
10-130
30
3&4-Methylphenol(m&p
ug/kg
ND
2030
2060
1170
1200
58
58
10-130
2
30
Cresol)
3,3'-Dichlorobenzidine
ug/kg
ND
4060
4140
2220
2500
55
60
10-130
12
30
3-Nitroaniline
ug/kg
ND
4060
4140
2460
2530
61
61
24-130
3
30
4,6-Dinitro-2-methylphenol
ug/kg
ND
4060
4140
<648
<661
0
0
10-152
30 M1
4-Bromophenylphenyl ether
ug/kg
ND
2030
2060
1330
1440
66
70
29-130
8
30
4-Chloro-3-methylphenol
ug/kg
ND
4060
4140
2400
2600
59
63
17-130
8
30
4-Chloroaniline
ug/kg
ND
4060
4140
19901
2300
49
56
14-130
30
4-Chlorophenylphenyl ether
ug/kg
ND
2030
2060
1320
1420
65
68
25-130
7
30
4-Nitroaniline
ug/kg
ND
4060
4140
2920
2990
72
72
22-130
3
30
4-Nitrophenol
ug/kg
ND
10200
10300
<640
<654
1
1
10-130
30 M1
Acenaphthene
ug/kg
ND
2030
2060
1410
1470
69
71
20-130
4
30
Acenaphthylene
ug/kg
ND
2030
2060
1540
1610
76
78
25-130
4
30
Aniline
ug/kg
ND
2030
2060
1170
1170
58
57
10-130
0
30
Anthracene
ug/kg
ND
2030
2060
1470
1580
73
76
29-130
7
30
Benzo(a)anth race ne
ug/kg
ND
2030
2060
1360
1460
67
70
19-130
7
30
Benzo(a)pyrene
ug/kg
ND
2030
2060
1360
1470
67
71
12-130
8
30
Benzo(b)fluoranthene
ug/kg
ND
2030
2060
1290
1450
63
70
14-130
12
30
Benzo(g,h,i)perylene
ug/kg
ND
2030
2060
1360
1490
67
72
10-130
9
30
Benzo(k)fluoranthene
ug/kg
ND
2030
2060
1300
1430
64
69
14-130
9
30
Benzoic Acid
ug/kg
ND
10200
10300
<433
<442
0
0
10-130
30 M1
Benzyl alcohol
ug/kg
ND
4060
4140
2350
2450
58
59
13-130
4
30
bis(2-
ug/kg
ND
2030
2060
1330
1390
65
67
16-130
5
30
Chloroethoxy)methane
bis(2-Chloroethyl) ether
ug/kg
ND
2030
2060
1350
1400
67
67
11-130
3
30
bis(2- Ethyl hexyl)phthalate
ug/kg
ND
2030
2060
1200
1340
59
65
21-130
11
30
Butylbenzylphthalate
ug/kg
ND
2030
2060
1220
1330
60
64
23-130
8
30
Chrysene
ug/kg
ND
2030
2060
1310
1410
65
68
22-130
7
30
Di-n-butylphthalate
ug/kg
ND
2030
2060
1210
1370
60
66
30-130
12
30
Di-n-octylphthalate
ug/kg
ND
2030
2060
1240
1380
61
67
23-142
11
30
Dibenz(a,h)anthracene
ug/kg
ND
2030
2060
1350
1540
66
74
10-130
13
30
Dibenzofuran
ug/kg
ND
2030
2060
1330
1410
66
68
24-130
6
30
Diethylphthalate
ug/kg
ND
2030
2060
1440
1480
71
72
26-130
3
30
Dimethylphthalate
ug/kg
ND
2030
2060
1410
1470
70
71
22-130
4
30
Fluoranthene
ug/kg
ND
2030
2060
1330
1490
65
72
33-130
11
30
Fluorene
ug/kg
ND
2030
2060
1460
1510
72
73
22-130
3
30
Hexachloro-1,3-butadiene
ug/kg
ND
2030
2060
1350
1360
67
66
13-130
1
30
Hexachlorobenzene
ug/kg
ND
2030
2060
1370
1460
67
70
29-130
6
30
Hexachlorocyclopentadiene
ug/kg
ND
2030
2060
1190
1320
58
64
10-130
10
30
Hexachloroethane
ug/kg
ND
2030
2060
1350
1390
66
67
10-130
3
30
Indeno(1,2,3-cd)pyrene
ug/kg
ND
2030
2060
1350
1470
67
71
10-130
8
30
Isophorone
ug/kg
ND
2030
2060
1360
1420
67
69
13-130
5
30
N-Nitroso-di-n-propylamine
ug/kg
ND
2030
2060
1400
1440
69
70
12-130
3
30
N-Nitrosodimethylamine
ug/kg
ND
2030
2060
1340
1320
66
64
11-130
2
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2019 03:45 PM without the written consent of Pace Analytical Services, LLC.
Page 22 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HO UST
Pace Project No.: 92452986
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 2733529
2733530
MS
MSD
92452841003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qual
N-Nitrosodiphenylamine
ug/kg
ND
2030
2060
1470
1530
73
74
15-130
4
30
Naphthalene
ug/kg
ND
2030
2060
1450
1510
71
73
15-130
4
30
Nitrobenzene
ug/kg
ND
2030
2060
1420
1470
70
71
12-130
3
30
Pentachlorophenol
ug/kg
ND
4060
4140
<184
<188
0
0
10-130
30 M1
Phenanthrene
ug/kg
ND
2030
2060
1410
1510
69
73
27-130
7
30
Phenol
ug/kg
ND
2030
2060
895
992
44
48
10-130
10
30
Pyrene
ug/kg
ND
2030
2060
1390
1500
68
72
19-130
7
30
Pyridine
ug/kg
ND
2030
2060
1220
1130
60
54
10-130
8
30
2,4,6-Tribromophenol (S)
%
9
14
27-110
S2
2-Fluorobiphenyl (S)
%
63
64
30-110
2-Fluorophenol (S)
%
11
18
13-110
SO
Nitrobenzene-d5(S)
%
69
70
23-110
Phenol-d6 (S)
%
42
46
22-110
Terphenyl-d14 (S)
%
64
69
28-110
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2019 03:45 PM without the written consent of Pace Analytical Services, LLC.
Page 23 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HO UST
Pace Project No.: 92452986
QC Batch: 509971 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Soil
Associated Lab Samples: 92452986002
METHOD BLANK: 2736776
Matrix:
Solid
Associated Lab Samples: 92452986002
Blank
Reporting
Parameter
Units
Result
Limit
MDL Analyzed Qualifiers
Aliphatic (C09-C18)
mg/kg
<9.9
9.9
9.9 11/18/19 16:07 N2
Aliphatic (C19-C36)
mg/kg
<9.9
9.9
9.9 11/18/19 16:07 N2
Aromatic (C11-C22)
mg/kg
<9.9
9.9
9.9 11/18/19 16:07 N2
2-Bromonaphthalene (S)
%
98
40-140
11/18/19 16:07
2-Fluorobiphenyl (S)
%
104
40-140
11/18/19 16:07
Nonatriacontane (S)
%
71
40-140
11/18/19 16:07
o-Terphenyl (S)
%
82
40-140
11/18/19 16:07
LABORATORY CONTROL SAMPLE & LCSD:
2736777
2736778
Spike
LCS
LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C09-C18)
mg/kg
10
<10.0
<10.1
46
50
40-140 50 N2
Aliphatic (C19-C36)
mg/kg
13.4
<10.0
<10.1
70
68
40-140 50 N2
Aromatic (C11-C22)
mg/kg
28.4
22.9
21.5
80
75
40-140 6 50 N2
2-Bromonaphthalene (S)
%
81
81
40-140
2-Fluorobiphenyl (S)
%
98
107
40-140
Nonatriacontane (S)
%
75
66
40-140
o-Terphenyl(S)
%
93
85
40-140
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2736779
2736780
MS
MSD
92453338001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD RPD Qual
Aliphatic (C09-C18)
mg/kg
ND
30.4
31.1
<30.5
<31.0
23
32
40-140
50 M1,N2
Aliphatic (C19-C36)
mg/kg
ND
40.6
41.2
<30.5
<31.0
58
63
40-140
50 N2
Aromatic (C11-C22)
mg/kg
ND
86.4
87.6
49.1
63.7
54
70
40-140
26 50 N2
2-Bromonaphthalene (S)
%
45
40
40-140
2-Fluorobiphenyl (S)
%
87
99
40-140
Nonatriacontane (S)
%
61
66
40-140
o-Terphenyl(S)
%
63
76
40-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2019 03:45 PM without the written consent of Pace Analytical Services, LLC.
Page 24 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: HO UST
Pace Project No.: 92452986
QC Batch: 508535 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92452986001, 92452986002
SAMPLE DUPLICATE: 2729896
92452974001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 26.1 27.1 4 25
SAMPLE DUPLICATE: 2730171
92453047001 Dup Max
Parameter Units Result Result RPD RPD Qualifiers
Percent Moisture % 16.9 18.4 8 25
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2019 03:45 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 31

Pace Analytical Services, LLC
lac,
Analyilcal ® 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: HO UST
Pace Project No.: 92452986
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
E Analyte concentration exceeded the calibration range. The reported result is estimated.
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
SO Surrogate recovery outside laboratory control limits.
S2 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re -analysis).
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2019 03:45 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: HO UST
Pace Project No.: 92452986
ANALYTE QUALIFIERS
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /19/2019 03:45 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 31

leAnalyiical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
HO UST
92452986
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92452986001
SS-1
EPA 3546
508576
EPA 8015C Modified
508695
92452986002
SS-2
EPA 3546
508576
EPA 8015C Modified
508695
92452986002
SS-2
MADEP EPH
509971
MADEP EPH
510288
92452986001
SS-1
EPA 5030B
508638
EPA 8015C Modified
508751
92452986002
SS-2
EPA 5030B
508638
EPA 8015C Modified
508751
92452986002
SS-2
MADEP VPH
509289
MADEP VPH
509845
92452986002
SS-2
EPA 3546
509329
EPA 8270E
509512
92452986002
SS-2
EPA 5035A
509224
EPA 8260D
509252
92452986001
SS-1
ASTM D2974-87
508535
92452986002
SS-2
ASTM D2974-87
508535
Date: 11/19/2019 03:45 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 28 of 31

Document Name:
Document Revised: February 7, 2018
m
5a1CeAna1XJCa1
Sample Canditlon U on Recei t(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS-033-Rev.06
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[:] Greenwood ❑ Huntersville Ralelgh❑ Mechanicsville[]
ConditionSample Client Name: WO# : 92452986
_—Up-on-Receipt. PrCourier: [-]Fed Ex �'}i-c) ©UPS❑USPS` ❑CI Qnoject
III � I
❑ Commercial ❑Pace ❑Other: 92452986
Custody Seal Present? ❑yes QNo Seals Intact? Des ONo
Date/Initials Person Examining Canlenis: ��
Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑None ©-'Other
Thermometer:
IR Gun ID: �2TO58 Type of Ice: 01et ❑Blue
Cooler Temp ('Cl: !/! Correction Factor: Add/Subtract (°C) O.O°C
Cooler Temp Corrected ('C):
USDA Regulated Sall { N/A, water sample]
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
nYPs r lr3n
Biological�Tssue Frozen?
[-]None ❑Yes QNo ❑NIA
Temp should be above freezing to VC
❑Samples out of temp criteria. Samples an ice, cooling process
hasbegun
Did samples originate from a foreign source (internationally,
Including Hawaii and Puerto RicoP FlYes FlNo
Comments/Discrepancy:
Chain of Custody Present?
®Yes
[]NO
❑NIA
1.
-Samples Arrived within Hold Time?
ElYes
(:]No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
[]Yes
[36
❑N/A
3.
Rush Turn Around Time Requested?
es
❑No
❑N/A
4.
Sufficient Volume?
Yes
[]No
JjNJA
5.
Correct Containers Used?
-Pace Con'. ainers Used?
Y
Yes
❑Na
[-]No
❑N/A
[]N/A
5.
Containers Intact?
❑Ygs
[]No
❑N/A
7.
_
Dissolved analysis: Samples Field Filtered?
❑Yes
❑Nc
0<
B.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix: �-
Eves
ONo
[]N/A
9.
Headspace in VOA Vials (>S-6mm)?
❑Yes
[Na
N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
[--]Yes
Yes
L3Na
�No
❑N/A
N/A
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICAT(ON/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Field Data Required? ❑Yes (-,INO
Date: I�
Date:
Page 29 of 31

5 aceAnalyfical „
Document Name:
Sample Condition Upon Recelpt(SOUR)
Document Revised: February 7, 2018
Page 1 of 2
Document No.:
Issuing Authority:
F•CAR•CS-033-Rev,06
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions, VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, t_LHg
**Bottom half of box is to list number of bottle
Project i w®# : 92452986
Due Date: 11/15/19
PM: PTE
CLIENT: 92-ATC
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date pnaeervation adjusted
Time preservation
adjusted
Amount of Preservative
added
Lot ii
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this Form will beaeritto the North Carolina DEHNR Certification Office (r.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 30 of 31

A
m
m
o b
n w N
tom`
ITEM #
d
m a
3
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Page 31 of 31

Case Narrative
PRISM Full -Service Analytical &
Environmental Solutions
`,. LABORATORIES, INC.
ATC Group Services, LLC
Al Quarles
7606 Whitehall Executive Center Drive, Suite 800
Charlotte, NC 28273
NC Certification No. 402
NC Drinking Water Cent No. 37735
SC Certification No. 99012
Project: Tim Collins Property
Lab Submittal Date: 11/27/2019
Prism Work Order: 9110453
12/4/19 16:06
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
a,j
Angela D. Overcash
VP Laboratory Services
Data Qualifiers Key Reference:
Reviewed By Terri W. Cole For Angela D. Overcash
Project Manager
D RPD value outside of the control limits.
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J-Flag).
L2 LCSD recovery outside of the QC limits. LCS recovery within the limits. No further action taken.
SR Surrogate recovery outside the QC limits.
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 1 of 56

Receipt Summary
Full -Service Analytical R
PRISMSample
Environmental Solutions
12/04/2019
LABORATORIES INC.
Prism Work Order: 9110453
Client Sample ID
Lab Sample ID
Matrix
Date/Time Sampled Date/Time Received
SE-1
9110453-01
Soil
11/26/19 16:25 11/27/19 10:00
SE-2
9110453-02
Soil
11/26/19 16:35 11/27/19 10:00
SE-3
9110453-03
Soil
11/26/19 16:45 11/27/19 10:00
SE-4
9110453-04
Soil
11/26/19 16:55 11/27/19 10:00
SE-5
9110453-05
Soil
11/26/19 17:05 11/27/19 10:00
Samples were received in good condition at 2.6 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 2 of 56

P R I S M Full Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Summary of Detections
12/04/2019
Prism Work Order: 9110453
Prism ID
Client ID
Parameter
Method
Result
Units
9110453-01
SE-1
C9-Cl8 Aliphatics
MADEP EPH
580
mg/kg dry
9110453-01
SE-1
C19-C36 Aliphatics
MADEP EPH
180
mg/kg dry
9110453-01
SE-1
C11-C22 Aromatics
MADEP EPH
400
mg/kg dry
9110453-01
SE-1
1-Methylnaphthalene
8270E
19
mg/kg dry
9110453-01
SE-1
2-Methylnaphthalene
8270E
31
mg/kg dry
9110453-01
SE-1
Fluorene
8270E
2.9
mg/kg dry
9110453-01
SE-1
Naphthalene
8270E
7.1
J
mg/kg dry
9110453-01
SE-1
Phenanthrene
8270E
5.8
mg/kg dry
9110453-01
SE-1
Pyrene
8270E
0.36
J
mg/kg dry
9110453-01
SE-1
1,2,4-Trimethylbenzene
8260D
31
mg/kg dry
9110453-01
SE-1
1,3,5-Trimethylbenzene
8260D
10
mg/kg dry
9110453-01
SE-1
4-Isopropyltoluene
8260D
3.8
mg/kg dry
9110453-01
SE-1
Benzene
8260D
0.27
J
mg/kg dry
9110453-01
SE-1
Bromomethane
8260D
0.37
J
mg/kg dry
9110453-01
SE-1
Chloromethane
8260D
0.15
J
mg/kg dry
9110453-01
SE-1
Ethylbenzene
8260D
7.3
mg/kg dry
9110453-01
SE-1
Isopropyl benzene (Cumene)
8260D
3.7
mg/kg dry
9110453-01
SE-1
m,p-Xylenes
8260D
19
mg/kg dry
9110453-01
SE-1
Naphthalene
8260D
8.9
mg/kg dry
9110453-01
SE-1
n-Butylbenzene
8260D
5.2
mg/kg dry
9110453-01
SE-1
n-Propylbenzene
8260D
7.0
mg/kg dry
9110453-01
SE-1
o-Xylene
8260D
10
mg/kg dry
9110453-01
SE-1
sec -Butyl benzene
8260D
5.7
mg/kg dry
9110453-01
SE-1
tert-Butylbenzene
8260D
0.35
mg/kg dry
9110453-01
SE-1
Toluene
8260D
0.78
mg/kg dry
9110453-01
SE-1
Xylenes, total
8260D
30
mg/kg dry
9110453-01
SE-1
C5-C8 Aliphatics
MADEP VPH
62
mg/kg dry
9110453-01
SE-1
C9-Cl2 Aliphatics
MADEP VPH
180
mg/kg dry
9110453-01
SE-1
C9-Cl0 Aromatics
MADEP VPH
300
mg/kg dry
9110453-02
SE-2
C9-Cl8 Aliphatics
MADEP EPH
14
J
mg/kg dry
9110453-02
SE-2
C19-C36 Aliphatics
MADEP EPH
6.3
J
mg/kg dry
9110453-02
SE-2
1-Methylnaphthalene
8270E
7.6
mg/kg dry
9110453-02
SE-2
2-Methylnaphthalene
8270E
13
mg/kg dry
9110453-02
SE-2
Fluorene
8270E
1.6
mg/kg dry
9110453-02
SE-2
Naphthalene
8270E
3.0
mg/kg dry
9110453-02
SE-2
Phenanthrene
8270E
3.0
mg/kg dry
9110453-02
SE-2
Pyrene
8270E
0.26
J
mg/kg dry
9110453-02
SE-2
1,2,4-Trimethylbenzene
8260D
31
mg/kg dry
9110453-02
SE-2
1,3,5-Trimethylbenzene
8260D
8.5
mg/kg dry
9110453-02
SE-2
4-Isopropyltoluene
8260D
3.3
mg/kg dry
9110453-02
SE-2
Benzene
8260D
0.11
J
mg/kg dry
9110453-02
SE-2
Bromomethane
8260D
0.24
.1
mg/kg dry
9110453-02
SE-2
Ethylbenzene
8260D
6.1
mg/kg dry
9110453-02
SE-2
Isopropyl benzene (Cumene)
8260D
3.1
mg/kg dry
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 3 of 56

/,GA1P-R I S M Full -Service Analytical
Environmental Solutions
LABORATORIES, ING
Summary of Detections
12/04/2019
Prism Work Order: 9110453
Prism ID
Client ID
Parameter
Method
Result
Units
9110453-02
SE-2
m,p-Xylenes
8260D
17
mg/kg dry
9110453-02
SE-2
Naphthalene
8260D
11
mg/kg dry
9110453-02
SE-2
n-Butylbenzene
8260D
4.7
mg/kg dry
9110453-02
SE-2
n-Propylbenzene
8260D
5.9
mg/kg dry
9110453-02
SE-2
o-Xylene
8260D
8.5
mg/kg dry
9110453-02
SE-2
sec -Butyl benzene
8260D
5.0
mg/kg dry
9110453-02
SE-2
tert-Butylbenzene
8260D
0.33
mg/kg dry
9110453-02
SE-2
Toluene
8260D
0.45
mg/kg dry
9110453-02
SE-2
Xylenes, total
8260D
26
mg/kg dry
9110453-02
SE-2
C5-C8 Aliphatics
MADEP VPH
60
mg/kg dry
9110453-02
SE-2
C9-C12 Aliphatics
MADEP VPH
150
mg/kg dry
9110453-02
SE-2
C9-C10 Aromatics
MADEP VPH
300
mg/kg dry
9110453-03
SE-3
C9-Cl8 Aliphatics
MADEP EPH
720
mg/kg dry
9110453-03
SE-3
C19-C36 Aliphatics
MADEP EPH
240
mg/kg dry
9110453-03
SE-3
C11-C22 Aromatics
MADEP EPH
620
mg/kg dry
9110453-03
SE-3
1-Methylnaphthalene
8270E
9.3
mg/kg dry
9110453-03
SE-3
2-Methylnaphthalene
8270E
15
mg/kg dry
9110453-03
SE-3
Fluorene
8270E
1.8
mg/kg dry
9110453-03
SE-3
Naphthalene
8270E
4.3
mg/kg dry
9110453-03
SE-3
Phenanthrene
8270E
3.8
mg/kg dry
9110453-03
SE-3
Pyrene
8270E
0.48
J
mg/kg dry
9110453-03
SE-3
1,2,4-Trimethyl benzene
8260D
4.1
mg/kg dry
9110453-03
SE-3
1,3,5-Trimethylbenzene
8260D
1.1
mg/kg dry
9110453-03
SE-3
4-Isopropyltoluene
8260D
0.43
mg/kg dry
9110453-03
SE-3
Ethylbenzene
8260D
0.60
mg/kg dry
9110453-03
SE-3
Isopropyl benzene (Cumene)
8260D
0.37
mg/kg dry
9110453-03
SE-3
m,p-Xylenes
8260D
1.7
mg/kg dry
9110453-03
SE-3
Naphthalene
8260D
3.7
mg/kg dry
9110453-03
SE-3
n-Butylbenzene
8260D
0.63
mg/kg dry
9110453-03
SE-3
n-Propylbenzene
8260D
0.77
mg/kg dry
9110453-03
SE-3
o-Xylene
8260D
0.68
mg/kg dry
9110453-03
SE-3
sec -Butyl benzene
8260D
0.57
mg/kg dry
9110453-03
SE-3
Toluene
8260D
0.12
J
mg/kg dry
9110453-03
SE-3
Xylenes, total
8260D
2.3
mg/kg dry
9110453-03
SE-3
C5-C8 Aliphatics
MADEP VPH
7.1
J
mg/kg dry
9110453-03
SE-3
C9-C12 Aliphatics
MADEP VPH
100
mg/kg dry
9110453-03
SE-3
C9-Cl0 Aromatics
MADEP VPH
67
mg/kg dry
9110453-04
SE-4
C9-Cl8 Aliphatics
MADEP EPH
1200
mg/kg dry
9110453-04
SE-4
C19-C36 Aliphatics
MADEP EPH
360
mg/kg dry
9110453-04
SE-4
C11-C22 Aromatics
MADEP EPH
770
mg/kg dry
9110453-04
SE-4
1,2,3-Trichlorobenzene
8260D
0.0011
.1
mg/kg dry
9110453-04
SE-4
1,2,4-Trimethylbenzene
8260D
0.0027
J
mg/kg dry
9110453-04
SE-4
1,3,5-Trimethylbenzene
8260D
0.00099
J
mg/kg dry
9110453-04
SE-4
Ethylbenzene
8260D
0.0011
J
mg/kg dry
9110453-04
SE-4
m,p-Xylenes
8260D
0.0026
J
mg/kg dry
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 4 of 56

/,GA1P-R I S M Full -Service Analytical
Environmental Solutions
LABORATORIES, ING
Summary of Detections
12/04/2019
Prism Work Order: 9110453
Prism ID
Client ID
Parameter
Method
Result
Units
9110453-04
SE-4
Naphthalene
8260D
0.0020
J
mg/kg dry
9110453-04
SE-4
n-Propylbenzene
8260D
0.00092
J
mg/kg dry
9110453-04
SE-4
o-Xylene
8260D
0.0017
J
mg/kg dry
9110453-04
SE-4
sec -Butyl benzene
8260D
0.00075
J
mg/kg dry
9110453-04
SE-4
Xylenes, total
8260D
0.0043
J
mg/kg dry
9110453-04
SE-4
C9-C12 Aliphatics
MADEP VPH
13
J
mg/kg dry
9110453-05
SE-5
C9-C18 Aliphatics
MADEP EPH
2O00
mg/kg dry
9110453-05
SE-5
C19-C36 Aliphatics
MADEP EPH
540
mg/kg dry
9110453-05
SE-5
C11-C22 Aromatics
MADEP EPH
1200
mg/kg dry
9110453-05
SE-5
1-Methylnaphthalene
8270E
4.9
mg/kg dry
9110453-05
SE-5
2-Methylnaphthalene
8270E
7.5
mg/kg dry
9110453-05
SE-5
Fluorene
8270E
1.1
mg/kg dry
9110453-05
SE-5
Naphthalene
8270E
1.8
mg/kg dry
9110453-05
SE-5
Phenanthrene
8270E
2.2
mg/kg dry
9110453-05
SE-5
Pyrene
8270E
0.22
J
mg/kg dry
9110453-05
SE-5
4-Isopropyltoluene
8260D
0.12
mg/kg dry
9110453-05
SE-5
Benzene
8260D
0.0096
mg/kg dry
9110453-05
SE-5
Ethylbenzene
8260D
0.32
mg/kg dry
9110453-05
SE-5
Isopropyl benzene (Cumene)
8260D
0.17
mg/kg dry
9110453-05
SE-5
Naphthalene
8260D
0.19
mg/kg dry
9110453-05
SE-5
n-Butylbenzene
8260D
0.14
mg/kg dry
9110453-05
SE-5
sec -Butyl benzene
8260D
0.20
mg/kg dry
9110453-05
SE-5
tert-Butylbenzene
8260D
0.013
mg/kg dry
9110453-05
SE-5
Toluene
8260D
0.058
mg/kg dry
9110453-05
SE-5
1,2,4-Trimethylbenzene
8260D
12000
ug/kg dry
9110453-05
SE-5
1,3,5-Trimethylbenzene
8260D
3700
ug/kg dry
9110453-05
SE-5
m,p-Xylenes
8260D
5400
ug/kg dry
9110453-05
SE-5
n-Propylbenzene
8260D
2500
ug/kg dry
9110453-05
SE-5
o-Xylene
8260D
2600
ug/kg dry
9110453-05
SE-5
Xylenes, total
8260D
7900
ug/kg dry
9110453-05
SE-5
C5-C8 Aliphatics
MADEP VPH
8.0
J
mg/kg dry
9110453-05
SE-5
C9-C12 Aliphatics
MADEP VPH
120
mg/kg dry
9110453-05
SE-5
C9-Cl0 Aromatics
MADEP VPH
82
mg/kg dry
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 5 of 56

/PRISM Full -Service Analytical s
Environmental Solutions
LABORATORIES INC.
Laboratory Report
12/04/2019
ATC Group Services, LLC
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Project: Tim Collins Property
Sample Matrix: Soil
Client Sample ID: SE-1
Prism Sample ID: 9110453-01
Prism Work Order: 9110453
Time Collected: 11/26/19 16:25
Time Submitted: 11/27/19 10:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics 580 mg/kg dry 28 1.4 1 MADEP EPH 1214/19 2:27 ZRC P9K0497
C19-C36 Aliphatics 180 mg/kg dry 28 4.8 1 MADEP EPH 12/4/19 2:27 ZRC P9K0497
C11-C22 Aromatics 400 mg/kg dry 28 7.7 1 MADEP EPH 12/4/19 2:27 ZRC P91K0497
Surrogate
Recovery
Control Limits
1-Chlorooctadecane
126 %
40-140
o-Terphenyl
150 %
40-140 SR
2-Fluorobiphenyl
92 %
40-140
2-Bromonaphthalene
90 %
40-140
General Chemistry Parameters
% Solids
88.3
% by
0.100
0.100
1
SM2540 G
12/3/19 8:14
EDV
P91-0025
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.75
0.13
1
8270E
12/3/19 11:20
JMV
P91-0017
1,2-Dichlorobenzene
BRL
mg/kg dry
0.75
0.12
1
8270E
12/3/19 11:20
JMV
P91-0017
1,3-Dichlorobenzene
BRL
mg/kg dry
0.75
0.11
1
8270E
12/3/19 11:20
JMV
P91-0017
1,4-Dichlorobenzene
BRL
mg/kg dry
0.37
0.12
1
8270E
12/3/19 11:20
JMV
P91-0017
1-Methyl naphthalene
19
mg/kg dry
7.5
0.11
10
8270E
1213/19 13:14
JMV
P91-0017
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.75
0.16
1
8270E
12/3/19 11:20
JMV
P91-0017
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.75
0.18
1
8270E
12/3/19 11:20
JMV
P91-0017
2,4-Dichlorophenol
BRL
mg/kg dry
0.75
0.15
1
8270E
12/3/19 11:20
JMV
P91-0017
2,4-Dimethylphenol
BRL
mg/kg dry
0.37
0.16
1
8270E
12/3/19 11:20
JMV
P91-0017
2,4-Dinitrophenol
BRL
mg/kg dry
1.7
0.44
1
8270E
12/3/19 11:20
JMV
P91-0017
2,4-Dinitrotoluene
BRL
mg/kg dry
0.75
0.20
1
8270E
12/3/19 11:20
JMV
P91-0017
2,6-Dinitrotoluene
BRL
mg/kg dry
0.75
0.19
1
8270E
12/3/19 11:20
JMV
P91-0017
2-Chloronaphthalene
BRL
mg/kg dry
0.75
0.18
1
8270E
12/3/19 11:20
JMV
P91-0017
2-Chlorophenol
BRL
mg/kg dry
0.75
0.14
1
8270E
12/3/19 11:20
JMV
P91-0017
2-Methyl naphthalene
31
mg/kg dry
7.5
0.14
10
8270E
12/3/19 13:14
JMV
P91-0017
2-Methylphenol
BRL
mg/kg dry
0.75
0.14
1
8270E
12/3/19 11:20
JMV
P91-0017
2-Nitrophenol
BRL
mg/kg dry
0.75
0.12
1
8270E
12/3/19 11:20
JMV
P91-0017
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.75
0.15
1
8270E
12/3/19 11:20
JMV
P91-0017
3/4-Methyl phenol
BRL
mg/kg dry
0.75
0.16
1
8270E
12/3/19 11:20
JMV
P91-0017
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.7
0.41
1
8270E
12/3/19 11:20
JMV
P91-0017
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.75
0.18
1
8270E
12/3/19 11:20
JMV
P91-0017
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.75
0.14
1
8270E
12/3/19 11:20
JMV
P91-0017
4-Chloroaniline
BRL
mg/kg dry
0.37
0.091
1
8270E
12/3/19 11:20
JMV
P91-0017
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.1
0.23
1
8270E
12/3/19 11:20
JMV
P91-0017
4-Nitrophenol
BRL
mg/kg dry
0.75
0.18
1
8270E
12/3/19 11:20
JMV
P91-0017
Acenaphthene
BRL
mg/kg dry
0.75
0.017
1
8270E
12/3/19 11:20
JMV
P91-0017
Acenaphthylene
BRL
mg/kg dry
0.75
0.015
1
8270E
12/3/19 11:20
JMV
P91-0017
Anthracene
BRL
mg/kg dry
0.75
0.0083
1
8270E
12/3/19 11:20
JMV
P91-0017
Azobenzene
BRL
mg/kg dry
0.75
0.16
1
8270E
12/3/19 11:20
JMV
P91-0017
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 56

Full -Service Analytical &
PRISMLaboratory
Environmental Solutions
LABORATORIES INC.
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273 Sample Matrix: Soil
Report
12/04/2019
Client Sample ID: SE-1
Prism Sample ID: 9110453-01
Prism Work Order: 9110453
Time Collected: 11/26/19 16:25
Time Submitted: 11/27/19 10:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Benzo(a)anthracene
BRL
mg/kg dry
0.75
0.0089
1
8270E
12/3/19 11:20
JMV
P91-0017
Benzo(a)pyrene
BRL
mg/kg dry
0.75
0.0067
1
8270E
12/3/19 11:20
JMV
P91-0017
Benzo(b)fluoranthene
BRL
mg/kg dry
0.75
0.0069
1
8270E
12/3/19 11:20
JMV
P91-0017
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.75
0.0074
1
8270E
12/3/19 11:20
JMV
P91-0017
Benzo(k)fluoranthene
BRL
mg/kg dry
0.75
0.0079
1
8270E
12/3/19 11:20
JMV
P91-0017
Benzoic Acid
BRL
mg/kg dry
2.3
0.62
1
8270E
12/3/19 11:20
JMV
P91-0017
Benzyl alcohol
BRL
mg/kg dry
0.75
0.14
1
8270E
12/3/19 11:20
JMV
P91-0017
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.75
0.14
1
8270E
12/3/19 11:20
JMV
P91-0017
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.75
0.12
1
8270E
12/3/19 11:20
JMV
P91-0017
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.37
0.13
1
8270E
12/3/19 11:20
JMV
P91-0017
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.75
0.17
1
8270E
12/3/19 11:20
JMV
P91-0017
Butyl benzyl phthalate
BRL
mg/kg dry
0.37
0.13
1
8270E
12/3/19 11:20
JMV
P91-0017
Chrysene
BRL
mg/kg dry
0.75
0.0088
1
8270E
12/3/19 11:20
JMV
P91-0017
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.75
0.022
1
8270E
12/3/19 11:20
JMV
P91-0017
Dibenzofuran
BRL
mg/kg dry
0.75
0.20
1
8270E
12/3/19 11:20
JMV
P91-0017
Diethyl phthalate
BRL
mg/kg dry
0.75
0.19
1
8270E
12/3/19 11:20
JMV
P91-0017
Dimethyl phthalate
BRL
mg/kg dry
0.75
0.18
1
8270E
12/3/19 11:20
JMV
P91-0017
Di-n-butyl phthalate
BRL
mg/kg dry
0.75
0.19
1
8270E
12/3/19 11:20
JMV
P91-0017
Di-n-octyl phthalate
BRL
mg/kg dry
0.37
0.19
1
8270E
12/3/19 11:20
JMV
P91-0017
Fluoranthene
BRL
mg/kg dry
0.75
0.0085
1
8270E
12/3/19 11:20
JMV
P91-0017
Fluorene
2.9
mg/kg dry
0.75
0.013
1
8270E
12/3/19 11:20
JMV
P91-0017
Hexachlorobenzene
BRL
mg/kg dry
0.75
0.16
1
8270E
12/3/19 11:20
JMV
P91-0017
Hexachlorobutadiene
BRL
mg/kg dry
0.75
0.17
1
8270E
12/3/19 11:20
JMV
P91-0017
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.75
0.26
1
8270E
12/3/19 11:20
JMV
P91-0017
Hexachloroethane
BRL
mg/kg dry
0.75
0.12
1
8270E
12/3/19 11:20
JMV
P91-0017
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.75
0.021
1
8270E
12/3/19 11:20
JMV
P91-0017
Isophorone
BRL
mg/kg dry
0.75
0.16
1
8270E
12/3/19 11:20
JMV
P91-0017
Naphthalene
7.1 J
mg/kg dry
7.5
0.16
10
8270E
1213/19 13:14
JMV
P91-0017
Nitrobenzene
BRL
mg/kg dry
0.37
0.16
1
8270E
12/3/19 11:20
JMV
P91-0017
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.75
0.17
1
8270E
12/3/19 11:20
JMV
P91-0017
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.75
0.20
1
8270E
12/3/19 11:20
JMV
P91-0017
Pentachlorophenol
BRL
mg/kg dry
1.1
0.48
1
8270E
12/3/19 11:20
JMV
P91-0017
Phenanthrene
5.8
mg/kg dry
0.75
0.0082
1
8270E
12/3/19 11:20
JMV
P91-0017
Phenol
BRL
mg/kg dry
0.75
0.12
1
8270E
12/3/19 11:20
JMV
P91-0017
Pyrene
0.36 J
mg/kg dry
0.75
0.011
1
8270E
12/3/19 11:20
JMV
P91-0017
Pyridine
BRL
mg/kg dry
0.37
0.071
1
8270E
12/3/19 11:20
JMV
P91-0017
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
90 %
39-132
2-Fluorobiphenyl
86 %
44-115
2-Fluorophenol
72 %
35-115
Nitrobenzene-d5
171 %
37-122
SR
Phenol-d5
70 %
34-121
Terphenyl-d14
65 %
54-127
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 7 of 56

/PRISM Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
12/04/2019
ATC Group Services, LLC
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Project: Tim Collins Property
Sample Matrix: Soil
Client Sample ID: SE-1
Prism Sample ID: 9110453-01
Prism Work Order: 9110453
Time Collected: 11/26/19 16:25
Time Submitted: 11/27/19 10:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS (Medium Level)
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.30
0.037
50
8260D
12/3/19 14:13
JLB
P91-0061
1,1,1-Trichloroethane
BRL
mg/kg dry
0.30
0.044
50
8260D
12/3/19 14:13
JLB
P91-0061
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.30
0.022
50
8260D
12/3/19 14:13
JLB
P91-0061
1,1,2-Trichloroethane
BRL
mg/kg dry
0.30
0.032
50
8260D
12/3/19 14:13
JLB
P91-0061
1,1-Dichloroethane
BRL
mg/kg dry
0.30
0.054
50
8260D
12/3/19 14:13
JLB
P91-0061
1,1-Dichloroethylene
BRL
mg/kg dry
0.30
0.055
50
8260D
12/3/19 14:13
JLB
P91-0061
1,1-Dichloropropylene
BRL
mg/kg dry
0.30
0.046
50
8260D
12/3/19 14:13
JLB
P91-0061
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.60
0.043
50
8260D
12/3/19 14:13
JLB
P91-0061
1,2,3-Trichloropropane
BRL
mg/kg dry
0.30
0.034
50
8260D
12/3/19 14:13
JLB
P91-0061
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.60
0.029
50
8260D
12/3/19 14:13
JLB
P91-0061
1,2,4-Trimethylbenzene
31
mg/kg dry
3.0
0.32
500
8260D
1212/19 17:59
JLB
P91-0061
1,2-Dibromoethane
BRL
mg/kg dry
0.30
0.027
50
8260D
12/3/19 14:13
JLB
P91-0061
1,2-Dichlorobenzene
BRL
mg/kg dry
0.30
0.033
50
8260D
12/3/19 14:13
JLB
P91-0061
1,2-Dichloroethane
BRL
mg/kg dry
0.30
0.036
50
8260D
12/3/19 14:13
JLB
P91-0061
1,2-Dichloropropane
BRL
mg/kg dry
0.30
0.045
50
8260D
12/3/19 14:13
JLB
P91-0061
1,3,5-Trimethylbenzene
10
mg/kg dry
0.30
0.038
50
8260D
1213/19 14:13
JLB
P91-0061
1,3-Dichlorobenzene
BRL
mg/kg dry
0.30
0.037
50
8260D
12/3/19 14:13
JLB
P91-0061
1,3-Dichloropropane
BRL
mg/kg dry
0.30
0.025
50
8260D
12/3/19 14:13
JLB
P91-0061
1,4-Dichlorobenzene
BRL
mg/kg dry
0.30
0.038
50
8260D
12/3/19 14:13
JLB
P91-0061
2,2-Dichloropropane
BRL
mg/kg dry
0.30
0.037
50
8260D
12/3/19 14:13
JLB
P91-0061
2-Chlorotoluene
BRL
mg/kg dry
0.30
0.040
50
8260D
12/3/19 14:13
JLB
P91-0061
4-Chlorotoluene
BRL
mg/kg dry
0.30
0.034
50
8260D
12/3/19 14:13
JLB
P91-0061
4-Isopropyltoluene
3.8
mg/kg dry
0.30
0.075
50
8260D
12/3/19 14:13
JLB
P91-0061
Acetone
BRL
mg/kg dry
1.2
0.077
50
8260D
12/3/19 14:13
JLB
P91-0061
Benzene
0.27 J
mg/kg dry
0.30
0.047
50
8260D
1213/19 14:13
JLB
P91-0061
Bromobenzene
BRL
mg/kg dry
0.30
0.042
50
8260D
12/3/19 14:13
JLB
P91-0061
Bromochloromethane
BRL
mg/kg dry
0.30
0.049
50
8260D
12/3/19 14:13
JLB
P91-0061
Bromodichloromethane
BRL
mg/kg dry
0.30
0.028
50
8260D
12/3/19 14:13
JLB
P91-0061
Bromoform
BRL
mg/kg dry
0.30
0.023
50
8260D
12/3/19 14:13
JLB
P91-0061
Bromomethane
0.37 J
mg/kg dry
0.60
0.15
50
8260D
12/3/19 14:13
JLB
P91-0061
Carbon Tetrachloride
BRL
mg/kg dry
0.30
0.059
50
8260D
12/3/19 14:13
JLB
P91-0061
Chlorobenzene
BRL
mg/kg dry
0.30
0.047
50
8260D
12/3/19 14:13
JLB
P91-0061
Chloroethane
BRL
mg/kg dry
0.60
0.057
50
8260D
12/3/19 14:13
JLB
P91-0061
Chloroform
BRL
mg/kg dry
0.30
0.037
50
8260D
12/3/19 14:13
JLB
P91-0061
Chloromethane
0.15 J
mg/kg dry
0.60
0.091
50
8260D
12/3/19 14:13
JLB
P91-0061
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.30
0.047
50
8260D
12/3/19 14:13
JLB
P91-0061
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.30
0.030
50
8260D
12/3/19 14:13
JLB
P91-0061
Dibromochloromethane
BRL
mg/kg dry
0.30
0.020
50
8260D
12/3/19 14:13
JLB
P91-0061
Dichlorodifluoromethane
BRL
mg/kg dry
0.60
0.085
50
8260D
12/3/19 14:13
JLB
P91-0061
Ethylbenzene
7.3
mg/kg dry
0.30
0.045
50
8260D
12/3/19 14:13
JLB
P91-0061
Isopropyl Ether
BRL
mg/kg dry
0.30
0.044
50
8260D
12/3/19 14:13
JLB
P91-0061
Isopropyl benzene (Cumene)
3.7
mg/kg dry
0.30
0.035
50
8260D
12/3/19 14:13
JLB
P91-0061
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 56

PRISMLaboratory Report
Full -Service Analytical &
Environmental Solutions 12/04/2019
LABORATORIES INC.
ATC Group Services, LLC Project: Tim Collins Property Client Sample ID: SE-1
Attn: Al Quarles Prism Sample ID: 9110453-01
7606 Whitehall Executive Center Drive, Suite Prism Work Order: 9110453
Charlotte, NC 28273 Sample Matrix: Soil Time Collected: 11/26/19 16:25
Time Submitted: 11/27/19 10:00
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
m,p-Xylenes
19
mg/kg dry
0.60
0.077
50
8260D
12/3/19 14:13
JLB
P91-0061
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
1.2
0.021
50
8260D
12/3/19 14:13
JLB
P91-0061
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
1.2
0.070
50
8260D
12/3/19 14:13
JLB
P91-0061
Methyl Isobutyl Ketone
BRL
mg/kg dry
1.2
0.024
50
8260D
12/3/19 14:13
JLB
P91-0061
Methylene Chloride
BRL
mg/kg dry
0.30
0.049
50
8260D
12/3/19 14:13
JLB
P91-0061
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.30
0.042
50
8260D
12/3/19 14:13
JLB
P91-0061
Naphthalene
8.9
mg/kg dry
0.60
0.030
50
8260D
12/3/19 14:13
JLB
P91-0061
n-Butylbenzene
5.2
mg/kg dry
0.30
0.028
50
8260D
1213/19 14:13
JLB
P91-0061
n-Propylbenzene
7.0
mg/kg dry
0.30
0.043
50
8260D
12/3/19 14:13
JLB
P91-0061
o-Xylene
10
mg/kg dry
0.30
0.032
50
8260D
12/3/19 14:13
JLB
1391-0061
sec-Butylbenzene
5.7
mg/kg dry
0.30
0.032
50
8260D
12/3/19 14:13
JLB
P91-0061
Styrene
BRL
mg/kg dry
0.30
0.029
50
8260D
12/3/19 14:13
JLB
P91-0061
tert-Butylbenzene
0.35
mg/kg dry
0.30
0.036
50
8260D
12/3/19 14:13
JLB
P91-0061
Tetrachloroethylene
BRL
mg/kg dry
0.30
0.054
50
8260D
12/3/19 14:13
JLB
P91-0061
Toluene
0.78
mg/kg dry
0.30
0.048
50
8260D
1213/19 14:13
JLB
P91-0061
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.30
0.057
50
8260D
12/3/19 14:13
JLB
P91-0061
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.30
0.026
50
8260D
12/3/19 14:13
JLB
P91-0061
Trichloroethylene
BRL
mg/kg dry
0.30
0.058
50
8260D
12/3/19 14:13
JLB
P91-0061
Trichlorofluoromethane
BRL
mg/kg dry
0.60
0.081
50
8260D
12/3/19 14:13
JLB
P91-0061
Vinyl acetate
BRL
mg/kg dry
0.60
0.033
50
8260D
12/3/19 14:13
JLB
P91-0061
Vinyl chloride
BRL
mg/kg dry
0.60
0.059
50
8260D
12/3/19 14:13
JLB
P91-0061
Xylenes, total
30
mg/kg dry
0.90
0.11
50
8260D
12/3/19 14:13
JLB
P91-0061
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
95 %
70-130
Dibromofluoromethane
90 %
70-130
Toluene-d8
100 %
70-130
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8 Aliphatics
62
mg/kg dry
17
3.5
100
MADEP VPH 12/2/19 12:56
TBL
P91-0004
C9-C12 Aliphatics
180
mg/kg dry
17
1.5
100
MADEP VPH 12/2/19 12:56
TBL
P91-0004
C9-C10 Aromatics
300
mg/kg dry
17
1.6
100
MADEP VPH 1212/19 12:56
TBL
P91-0004
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
83 %
70-130
2,5-Dibromotoluene (FID)
80 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 9 of 56

/PRISM Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
12/04/2019
ATC Group Services, LLC
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Project: Tim Collins Property
Sample Matrix: Soil
Client Sample ID: SE-2
Prism Sample ID: 9110453-02
Prism Work Order: 9110453
Time Collected: 11/26/19 16:35
Time Submitted: 11/27/19 10:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics 14 J mg/kg dry 29 1.5 1 MADEP EPH 1214/19 3:03 ZRC P9K0497
C19-C36 Aliphatics 6.3 J mg/kg dry 29 4.9 1 MADEP EPH 12/4/19 3:03 ZRC P91<0497
C11-C22 Aromatics BRL mg/kg dry 29 8.0 1 MADEP EPH 12/4/19 3:03 ZRC P9K0497
Surrogate Recovery Control Limits
1-Chlorooctadecane
72 %
40-140
o-Terphenyl
88 %
40-140
2-Fluorobiphenyl
81 %
40-140
2-Bromonaphthalene
94 %
40-140
General Chemistry Parameters
% Solids
85.7
% by
0.100
0.100
1
SM2540 G
12/3/19 8:14
EDV
P91-0025
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.77
0.14
1
8270E
12/3/19 11:43
JMV
P91-0017
1,2-Dichlorobenzene
BRL
mg/kg dry
0.77
0.12
1
8270E
12/3/19 11:43
JMV
P91-0017
1,3-Dichlorobenzene
BRL
mg/kg dry
0.77
0.11
1
8270E
12/3/19 11:43
JMV
P91-0017
1,4-Dichlorobenzene
BRL
mg/kg dry
0.38
0.12
1
8270E
12/3/19 11:43
JMV
P91-0017
1-Methyl naphthalene
7.6
mg/kg dry
0.77
0.012
1
8270E
12/3/19 11:43
JMV
P91-0017
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.77
0.16
1
8270E
12/3/19 11:43
JMV
P91-0017
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.77
0.19
1
8270E
12/3/19 11:43
JMV
P91-0017
2,4-Dichlorophenol
BRL
mg/kg dry
0.77
0.15
1
8270E
12/3/19 11:43
JMV
P91-0017
2,4-Dimethylphenol
BRL
mg/kg dry
0.38
0.16
1
8270E
12/3/19 11:43
JMV
P91-0017
2,4-Dinitrophenol
BRL
mg/kg dry
1.7
0.45
1
8270E
12/3/19 11:43
JMV
P91-0017
2,4-Dinitrotoluene
BRL
mg/kg dry
0.77
0.20
1
8270E
12/3/19 11:43
JMV
P91-0017
2,6-Dinitrotoluene
BRL
mg/kg dry
0.77
0.20
1
8270E
12/3/19 11:43
JMV
P91-0017
2-Chloronaphthalene
BRL
mg/kg dry
0.77
0.19
1
8270E
12/3/19 11:43
JMV
P91-0017
2-Chlorophenol
BRL
mg/kg dry
0.77
0.15
1
8270E
12/3/19 11:43
JMV
P91-0017
2-Methyl naphthalene
13
mg/kg dry
3.8
0.074
5
8270E
12/3/19 13:37
JMV
P91-0017
2-Methylphenol
BRL
mg/kg dry
0.77
0.15
1
8270E
12/3/19 11:43
JMV
P91-0017
2-Nitrophenol
BRL
mg/kg dry
0.77
0.13
1
8270E
12/3/19 11:43
JMV
P91-0017
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.77
0.15
1
8270E
12/3/19 11:43
JMV
P91-0017
3/4-Methyl phenol
BRL
mg/kg dry
0.77
0.17
1
8270E
12/3/19 11:43
JMV
P91-0017
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.7
0.42
1
8270E
12/3/19 11:43
JMV
P91-0017
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.77
0.18
1
8270E
12/3/19 11:43
JMV
P91-0017
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.77
0.15
1
8270E
12/3/19 11:43
JMV
P91-0017
4-Chloroaniline
BRL
mg/kg dry
0.38
0.093
1
8270E
12/3/19 11:43
JMV
P91-0017
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.2
0.23
1
8270E
12/3/19 11:43
JMV
P91-0017
4-Nitrophenol
BRL
mg/kg dry
0.77
0.19
1
8270E
12/3/19 11:43
JMV
P91-0017
Acenaphthene
BRL
mg/kg dry
0.77
0.018
1
8270E
12/3/19 11:43
JMV
P91-0017
Acenaphthylene
BRL
mg/kg dry
0.77
0.015
1
8270E
12/3/19 11:43
JMV
P91-0017
Anthracene
BRL
mg/kg dry
0.77
0.0085
1
8270E
12/3/19 11:43
JMV
P91-0017
Azobenzene
BRL
mg/kg dry
0.77
0.16
1
8270E
12/3/19 11:43
JMV
P91-0017
Benzo(a)anthracene
BRL
mg/kg dry
0.77
0.0092
1
8270E
12/3/19 11:43
JMV
P91-0017
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 56

Report
Full -Service
Analytical &
PRISMLaboratory
Environmental Solutions
LABORATORIES INC.
12/04/2019
ATC Group Services, LLC
Project: Tim Collins Property
Client Sample ID: SE-2
Attn: Al Quarles
Prism Sample ID: 9110453-02
7606 Whitehall Executive Center Drive, Suite
Prism Work Order:
9110453
Charlotte, NC 28273
Sample Matrix: Soil
Time Collected:
11/26/19 16:35
Time Submitted:
11/27/19 10:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.77
0.0068
1
8270E
12/3/19 11:43
JMV
P91-0017
Benzo(b)fluoranthene
BRL
mg/kg dry
0.77
0.0071
1
8270E
12/3/19 11:43
JMV
P91-0017
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.77
0.0075
1
8270E
12/3/19 11:43
JMV
P91-0017
Benzo(k)fluoranthene
BRL
mg/kg dry
0.77
0.0081
1
8270E
12/3/19 11:43
JMV
P91-0017
Benzoic Acid
BRL
mg/kg dry
2.3
0.64
1
8270E
12/3/19 11:43
JMV
P91-0017
Benzyl alcohol
BRL
mg/kg dry
0.77
0.14
1
8270E
12/3/19 11:43
JMV
P91-0017
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.77
0.15
1
8270E
12/3/19 11:43
JMV
P91-0017
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.77
0.12
1
8270E
12/3/19 11:43
JMV
P91-0017
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.38
0.14
1
8270E
12/3/19 11:43
JMV
P91-0017
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.77
0.17
1
8270E
12/3/19 11:43
JMV
P91-0017
Butyl benzyl phthalate
BRL
mg/kg dry
0.38
0.13
1
8270E
12/3/19 11:43
JMV
P91-0017
Chrysene
BRL
mg/kg dry
0.77
0.0090
1
8270E
12/3/19 11:43
JMV
P91-0017
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.77
0.022
1
8270E
12/3/19 11:43
JMV
P91-0017
Dibenzofuran
BRL
mg/kg dry
0.77
0.21
1
8270E
12/3/19 11:43
JMV
P91-0017
Diethyl phthalate
BRL
mg/kg dry
0.77
0.20
1
8270E
12/3/19 11:43
JMV
P91-0017
Dimethyl phthalate
BRL
mg/kg dry
0.77
0.18
1
8270E
12/3/19 11:43
JMV
P91-0017
Di-n-butyl phthalate
BRL
mg/kg dry
0.77
0.19
1
8270E
12/3/19 11:43
JMV
P91-0017
Di-n-octyl phthalate
BRL
mg/kg dry
0.38
0.20
1
8270E
12/3/19 11:43
JMV
P91-0017
Fluoranthene
BRL
mg/kg dry
0.77
0.0087
1
8270E
12/3/19 11:43
JMV
P91-0017
Fluorene
1.6
mg/kg dry
0.77
0.013
1
8270E
12/3/19 11:43
JMV
P91-0017
Hexachlorobenzene
BRL
mg/kg dry
0.77
0.17
1
8270E
12/3/19 11:43
JMV
P91-0017
Hexachlorobutadiene
BRL
mg/kg dry
0.77
0.17
1
8270E
12/3/19 11:43
JMV
P91-0017
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.77
0.26
1
8270E
12/3/19 11:43
JMV
P91-0017
Hexachloroethane
BRL
mg/kg dry
0.77
0.12
1
8270E
12/3/19 11:43
JMV
P91-0017
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.77
0.022
1
8270E
12/3/19 11:43
JMV
P91-0017
Isophorone
BRL
mg/kg dry
0.77
0.16
1
8270E
12/3/19 11:43
JMV
P91-0017
Naphthalene
3.0
mg/kg dry
0.77
0.016
1
8270E
1213/19 11:43
JMV
P91-0017
Nitrobenzene
BRL
mg/kg dry
0.38
0.16
1
8270E
12/3/19 11:43
JMV
P91-0017
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.77
0.18
1
8270E
12/3/19 11:43
JMV
P91-0017
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.77
0.21
1
8270E
12/3/19 11:43
JMV
P91-0017
Pentachlorophenol
BRL
mg/kg dry
1.2
0.49
1
8270E
12/3/19 11:43
JMV
P91-0017
Phenanthrene
3.0
mg/kg dry
0.77
0.0083
1
8270E
1213/19 11:43
JMV
P91-0017
Phenol
BRL
mg/kg dry
0.77
0.13
1
8270E
12/3/19 11:43
JMV
P91-0017
Pyrene
0.26 J
mg/kg dry
0.77
0.011
1
8270E
1213/19 11:43
JMV
P91-0017
Pyridine
BRL
mg/kg dry
0.38
0.073
1
8270E
12/3/19 11:43
JMV
P91-0017
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
74 %
39-132
2-Fluorobiphenyl
83 %
44-115
2-Fluorophenol
76 %
35-115
Nitrobenzene-d5
90 %
37-122
Phenol-d5
72 %
34-121
Terphenyl-d14
63 %
54-127
Volatile Organic Compounds by GC/MS
(Medium Level)
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 11 of 56

Full -Service Analytical &
PRISMLaboratory
Environmental Solutions
LABORATORIES INC.
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273 Sample Matrix: Soil
Report
12/04/2019
Client Sample ID: SE-2
Prism Sample ID: 9110453-02
Prism Work Order: 9110453
Time Collected: 11/26/19 16:35
Time Submitted: 11/27/19 10:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.29
0.036
50
8260D
12/3/19 14:43
JLB
P91-0061
1,1,1-Trichloroethane
BRL
mg/kg dry
0.29
0.043
50
8260D
12/3/19 14:43
JLB
P91-0061
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.29
0.021
50
8260D
12/3/19 14:43
JLB
P91-0061
1,1,2-Trichloroethane
BRL
mg/kg dry
0.29
0.032
50
8260D
12/3/19 14:43
JLB
P91-0061
1,1-Dichloroethane
BRL
mg/kg dry
0.29
0.053
50
8260D
12/3/19 14:43
JLB
P91-0061
1,1-Dichloroethylene
BRL
mg/kg dry
0.29
0.054
50
8260D
12/3/19 14:43
JLB
P91-0061
1,1-Dichloropropylene
BRL
mg/kg dry
0.29
0.045
50
8260D
12/3/19 14:43
JLB
P91-0061
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.58
0.042
50
8260D
12/3/19 14:43
JLB
P91-0061
1,2,3-Trichloropropane
BRL
mg/kg dry
0.29
0.033
50
8260D
12/3/19 14:43
JLB
P91-0061
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.58
0.028
50
8260D
12/3/19 14:43
JLB
P91-0061
1,2,4-Trimethylbenzene
31
mg/kg dry
2.9
0.31
500
8260D
12/2/19 18:27
JLB
P91-0061
1,2-Dibromoethane
BRL
mg/kg dry
0.29
0.026
50
8260D
12/3/19 14:43
JLB
P91-0061
1,2-Dichlorobenzene
BRL
mg/kg dry
0.29
0.033
50
8260D
12/3/19 14:43
JLB
P91-0061
1,2-Dichloroethane
BRL
mg/kg dry
0.29
0.035
50
8260D
12/3/19 14:43
JLB
P91-0061
1,2-Dichloropropane
BRL
mg/kg dry
0.29
0.044
50
8260D
12/3/19 14:43
JLB
P91-0061
1,3,5-Trimethylbenzene
8.5
mg/kg dry
0.29
0.037
50
8260D
1213/19 14:43
JLB
P91-0061
1,3-Dichlorobenzene
BRL
mg/kg dry
0.29
0.036
50
8260D
12/3/19 14:43
JLB
P91-0061
1,3-Dichloropropane
BRL
mg/kg dry
0.29
0.024
50
8260D
12/3/19 14:43
JLB
P91-0061
1,4-Dichlorobenzene
BRL
mg/kg dry
0.29
0.037
50
8260D
12/3/19 14:43
JLB
P91-0061
2,2-Dichloropropane
BRL
mg/kg dry
0.29
0.036
50
8260D
12/3/19 14:43
JLB
P91-0061
2-Chlorotoluene
BRL
mg/kg dry
0.29
0.039
50
8260D
12/3/19 14:43
JLB
P91-0061
4-Chlorotoluene
BRL
mg/kg dry
0.29
0.033
50
8260D
12/3/19 14:43
JLB
P91-0061
4-Isopropyltoluene
3.3
mg/kg dry
0.29
0.074
50
8260D
12/3/19 14:43
JLB
P91-0061
Acetone
BRL
mg/kg dry
1.2
0.075
50
8260D
12/3/19 14:43
JLB
P91-0061
Benzene
0.11 J
mg/kg dry
0.29
0.046
50
8260D
12/3/19 14:43
JLB
P91-0061
Bromobenzene
BRL
mg/kg dry
0.29
0.041
50
8260D
12/3/19 14:43
JLB
P91-0061
Bromochloromethane
BRL
mg/kg dry
0.29
0.048
50
8260D
12/3/19 14:43
JLB
P91-0061
Bromodichloromethane
BRL
mg/kg dry
0.29
0.028
50
8260D
12/3/19 14:43
JLB
P91-0061
Bromoform
BRL
mg/kg dry
0.29
0.023
50
8260D
12/3/19 14:43
JLB
P91-0061
Bromomethane
0.24 J
mg/kg dry
0.58
0.14
50
8260D
12/3/19 14:43
JLB
P91-0061
Carbon Tetrachloride
BRL
mg/kg dry
0.29
0.058
50
8260D
12/3/19 14:43
JLB
P91-0061
Chlorobenzene
BRL
mg/kg dry
0.29
0.046
50
8260D
12/3/19 14:43
JLB
P91-0061
Chloroethane
BRL
mg/kg dry
0.58
0.056
50
8260D
12/3/19 14:43
JLB
P91-0061
Chloroform
BRL
mg/kg dry
0.29
0.036
50
8260D
12/3/19 14:43
JLB
P91-0061
Chloromethane
BRL
mg/kg dry
0.58
0.089
50
8260D
12/3/19 14:43
JLB
P91-0061
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.29
0.046
50
8260D
12/3/19 14:43
JLB
P91-0061
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.29
0.029
50
8260D
12/3/19 14:43
JLB
P91-0061
Dibromochloromethane
BRL
mg/kg dry
0.29
0.020
50
8260D
12/3/19 14:43
JLB
P91-0061
Dichlorodifluoromethane
BRL
mg/kg dry
0.58
0.082
50
8260D
12/3/19 14:43
JLB
P91-0061
Ethylbenzene
6.1
mg/kg dry
0.29
0.044
50
8260D
12/3/19 14:43
JLB
P91-0061
Isopropyl Ether
BRL
mg/kg dry
0.29
0.043
50
8260D
12/3/19 14:43
JLB
P91-0061
Isopropyl benzene (Cumene)
3.1
mg/kg dry
0.29
0.034
50
8260D
12/3/19 14:43
JLB
P91-0061
m,p-Xylenes
17
mg/kg dry
0.58
0.075
50
8260D
12/3/19 14:43
JLB
P91-0061
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 12 0f 56

PRISMLaboratory Report
Full -Service Analytical &
Environmental Solutions 12/04/2019
LABORATORIES INC.
ATC Group Services, LLC Project: Tim Collins Property Client Sample ID: SE-2
Attn: Al Quarles Prism Sample ID: 9110453-02
7606 Whitehall Executive Center Drive, Suite Prism Work Order: 9110453
Charlotte, NC 28273 Sample Matrix: Soil Time Collected: 11/26/19 16:35
Time Submitted: 11/27/19 10:00
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
1.2
0.020
50
8260D
12/3/19 14:43
JLB
P91-0061
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
1.2
0.068
50
8260D
12/3/19 14:43
JLB
P91-0061
Methyl Isobutyl Ketone
BRL
mg/kg dry
1.2
0.024
50
8260D
12/3/19 14:43
JLB
P91-0061
Methylene Chloride
BRL
mg/kg dry
0.29
0.047
50
8260D
12/3/19 14:43
JLB
P91-0061
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.29
0.041
50
8260D
12/3/19 14:43
JLB
P91-0061
Naphthalene
11
mg/kg dry
0.58
0.030
50
8260D
12/3/19 14:43
JLB
P91-0061
n-Butylbenzene
4.7
mg/kg dry
0.29
0.027
50
8260D
12/3/19 14:43
JLB
P91-0061
n-Propylbenzene
5.9
mg/kg dry
0.29
0.042
50
8260D
1213/19 14:43
JLB
P91-0061
o-Xylene
8.5
mg/kg dry
0.29
0.031
50
8260D
12/3/19 14:43
JLB
P91-0061
sec-Butylbenzene
5.0
mg/kg dry
0.29
0.032
50
8260D
12/3/19 14:43
JLB
P91-0061
Styrene
BRL
mg/kg dry
0.29
0.028
50
8260D
12/3/19 14:43
JLB
P91-0061
tert-Butylbenzene
0.33
mg/kg dry
0.29
0.035
50
8260D
12/3/19 14:43
JLB
P91-0061
Tetrachloroethylene
BRL
mg/kg dry
0.29
0.053
50
8260D
12/3/19 14:43
JLB
P91-0061
Toluene
0.45
mg/kg dry
0.29
0.047
50
8260D
12/3/19 14:43
JLB
P91-0061
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.29
0.056
50
8260D
12/3/19 14:43
JLB
P91-0061
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.29
0.025
50
8260D
12/3/19 14:43
JLB
P91-0061
Trichloroethylene
BRL
mg/kg dry
0.29
0.057
50
8260D
12/3/19 14:43
JLB
P91-0061
Trichlorofluoromethane
BRL
mg/kg dry
0.58
0.079
50
8260D
12/3/19 14:43
JLB
P91-0061
Vinyl acetate
BRL
mg/kg dry
0.58
0.032
50
8260D
12/3/19 14:43
JLB
P91-0061
Vinyl chloride
BRL
mg/kg dry
0.58
0.058
50
8260D
12/3/19 14:43
JLB
P91-0061
Xylenes, total
26
mg/kg dry
0.88
0.11
50
8260D
12/3/19 14:43
JLB
P91-0061
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
90 %
70-130
Dibromofluoromethane
90 %
70-130
Toluene-d8
100 %
70-130
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8 Aliphatics
60
mg/kg dry
15
2.9
100
MADEP VPH 12/2/19 13:55
TBL
P91-0004
C9-C12 Aliphatics
150
mg/kg dry
15
1.3
100
MADEP VPH 12/2/19 13:55
TBL
P91-0004
C9-C10 Aromatics
300
mg/kg dry
15
1.4
100
MADEP VPH 12/2/19 13:55
TBL
P91-0004
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
73 %
70-130
2,5-Dibromotoluene (FID)
70 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 13 0f 56

/PRISM Full -Service Analytical s
Environmental Solutions
LABORATORIES INC.
Laboratory Report
12/04/2019
ATC Group Services, LLC
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Project: Tim Collins Property
Sample Matrix: Soil
Client Sample ID: SE-3
Prism Sample ID: 9110453-03
Prism Work Order: 9110453
Time Collected: 11/26/19 16:45
Time Submitted: 11/27/19 10:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics 720 mg/kg dry 31 1.6 1 MADEP EPH 1214/19 3:40 ZRC P9K0497
C19-C36 Aliphatics 240 mg/kg dry 31 5.2 1 MADEP EPH 12/4/19 3:40 ZRC P9K0497
C11-C22 Aromatics 620 mg/kg dry 31 8.5 1 MADEP EPH 12/4/19 3:40 ZRC P91K0497
Surrogate Recovery Control Limits
1-Chlorooctadecane
138 %
40-140
o-Terphenyl
140 %
40-140
2-Fluorobiphenyl
104 %
40-140
2-Bromonaphthalene
100 %
40-140
General Chemistry Parameters
% Solids
80.5
% by
0.100
0.100
1
SM2540 G
12/3/19 8:14
EDV
P91-0025
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.82
0.15
1
8270E
12/3/19 12:06
JMV
P91-0017
1,2-Dichlorobenzene
BRL
mg/kg dry
0.82
0.13
1
8270E
12/3/19 12:06
JMV
P91-0017
1,3-Dichlorobenzene
BRL
mg/kg dry
0.82
0.12
1
8270E
12/3/19 12:06
JMV
P91-0017
1,4-Dichlorobenzene
BRL
mg/kg dry
0.41
0.13
1
8270E
12/3/19 12:06
JMV
P91-0017
1-Methyl naphthalene
9.3
mg/kg dry
4.1
0.063
5
8270E
1213/19 14:00
JMV
P91-0017
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.82
0.17
1
8270E
12/3/19 12:06
JMV
P91-0017
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.82
0.20
1
8270E
12/3/19 12:06
JMV
P91-0017
2,4-Dichlorophenol
BRL
mg/kg dry
0.82
0.16
1
8270E
12/3/19 12:06
JMV
P91-0017
2,4-Dimethylphenol
BRL
mg/kg dry
0.41
0.17
1
8270E
12/3/19 12:06
JMV
P91-0017
2,4-Dinitrophenol
BRL
mg/kg dry
1.9
0.48
1
8270E
12/3/19 12:06
JMV
P91-0017
2,4-Dinitrotoluene
BRL
mg/kg dry
0.82
0.22
1
8270E
12/3/19 12:06
JMV
P91-0017
2,6-Dinitrotoluene
BRL
mg/kg dry
0.82
0.21
1
8270E
12/3/19 12:06
JMV
P91-0017
2-Chloronaphthalene
BRL
mg/kg dry
0.82
0.20
1
8270E
12/3/19 12:06
JMV
P91-0017
2-Chlorophenol
BRL
mg/kg dry
0.82
0.16
1
8270E
12/3/19 12:06
JMV
P91-0017
2-Methyl naphthalene
15
mg/kg dry
4.1
0.079
5
8270E
12/3/19 14:00
JMV
P91-0017
2-Methylphenol
BRL
mg/kg dry
0.82
0.16
1
8270E
12/3/19 12:06
JMV
P91-0017
2-Nitrophenol
BRL
mg/kg dry
0.82
0.14
1
8270E
12/3/19 12:06
JMV
P91-0017
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.82
0.16
1
8270E
12/3/19 12:06
JMV
P91-0017
3/4-Methyl phenol
BRL
mg/kg dry
0.82
0.18
1
8270E
12/3/19 12:06
JMV
P91-0017
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.9
0.45
1
8270E
12/3/19 12:06
JMV
P91-0017
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.82
0.19
1
8270E
12/3/19 12:06
JMV
P91-0017
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.82
0.16
1
8270E
12/3/19 12:06
JMV
P91-0017
4-Chloroaniline
BRL
mg/kg dry
0.41
0.099
1
8270E
12/3/19 12:06
JMV
P91-0017
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.2
0.25
1
8270E
12/3/19 12:06
JMV
P91-0017
4-Nitrophenol
BRL
mg/kg dry
0.82
0.20
1
8270E
12/3/19 12:06
JMV
P91-0017
Acenaphthene
BRL
mg/kg dry
0.82
0.019
1
8270E
12/3/19 12:06
JMV
P91-0017
Acenaphthylene
BRL
mg/kg dry
0.82
0.016
1
8270E
12/3/19 12:06
JMV
P91-0017
Anthracene
BRL
mg/kg dry
0.82
0.0090
1
8270E
12/3/19 12:06
JMV
P91-0017
Azobenzene
BRL
mg/kg dry
0.82
0.17
1
8270E
12/3/19 12:06
JMV
P91-0017
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 14 0f 56

Full -Service Analytical &
PRISMLaboratory
Environmental Solutions
LABORATORIES INC.
ATC Group Services, LLC
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Project: Tim Collins Property
Sample Matrix: Soil
Report
12/04/2019
Client Sample ID: SE-3
Prism Sample ID: 9110453-03
Prism Work Order: 9110453
Time Collected: 11/26/19 16:45
Time Submitted: 11/27/19 10:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Benzo(a)anthracene
BRL
mg/kg dry
0.82
0.0098
1
8270E
12/3/19 12:06
JMV
P91-0017
Benzo(a)pyrene
BRL
mg/kg dry
0.82
0.0073
1
8270E
12/3/19 12:06
JMV
P91-0017
Benzo(b)fluoranthene
BRL
mg/kg dry
0.82
0.0076
1
8270E
12/3/19 12:06
JMV
P91-0017
Benzo(g,hJ)perylene
BRL
mg/kg dry
0.82
0.0081
1
8270E
12/3/19 12:06
JMV
P91-0017
Benzo(k)fluoranthene
BRL
mg/kg dry
0.82
0.0087
1
8270E
12/3/19 12:06
JMV
P91-0017
Benzoic Acid
BRL
mg/kg dry
2.5
0.68
1
8270E
12/3/19 12:06
JMV
P91-0017
Benzyl alcohol
BRL
mg/kg dry
0.82
0.15
1
8270E
12/3/19 12:06
JMV
P91-0017
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.82
0.16
1
8270E
12/3/19 12:06
JMV
P91-0017
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.82
0.13
1
8270E
12/3/19 12:06
JMV
P91-0017
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.41
0.15
1
8270E
12/3/19 12:06
JMV
P91-0017
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.82
0.18
1
8270E
12/3/19 12:06
JMV
P91-0017
Butyl benzyl phthalate
BRL
mg/kg dry
0.41
0.14
1
8270E
12/3/19 12:06
JMV
P91-0017
Chrysene
BRL
mg/kg dry
0.82
0.0097
1
8270E
12/3/19 12:06
JMV
P91-0017
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.82
0.024
1
8270E
12/3/19 12:06
JMV
P91-0017
Dibenzofuran
BRL
mg/kg dry
0.82
0.22
1
8270E
12/3/19 12:06
JMV
P91-0017
Diethyl phthalate
BRL
mg/kg dry
0.82
0.21
1
8270E
12/3/19 12:06
JMV
P91-0017
Dimethyl phthalate
BRL
mg/kg dry
0.82
0.20
1
8270E
12/3/19 12:06
JMV
P91-0017
Di-n-butyl phthalate
BRL
mg/kg dry
0.82
0.20
1
8270E
12/3/19 12:06
JMV
P91-0017
Di-n-octyl phthalate
BRL
mg/kg dry
0.41
0.21
1
8270E
12/3/19 12:06
JMV
P91-0017
Fluoranthene
BRL
mg/kg dry
0.82
0.0093
1
8270E
12/3/19 12:06
JMV
P91-0017
Fluorene
1.8
mg/kg dry
0.82
0.014
1
8270E
12/3/19 12:06
JMV
P91-0017
Hexachlorobenzene
BRL
mg/kg dry
0.82
0.18
1
8270E
12/3/19 12:06
JMV
P91-0017
Hexachlorobutadiene
BRL
mg/kg dry
0.82
0.18
1
8270E
12/3/19 12:06
JMV
P91-0017
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.82
0.28
1
8270E
12/3/19 12:06
JMV
P91-0017
Hexachloroethane
BRL
mg/kg dry
0.82
0.13
1
8270E
12/3/19 12:06
JMV
P91-0017
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.82
0.023
1
8270E
12/3/19 12:06
JMV
P91-0017
Isophorone
BRL
mg/kg dry
0.82
0.18
1
8270E
12/3/19 12:06
JMV
P91-0017
Naphthalene
4.3
mg/kg dry
0.82
0.017
1
8270E
1213/19 12:06
JMV
P91-0017
Nitrobenzene
BRL
mg/kg dry
0.41
0.17
1
8270E
12/3/19 12:06
JMV
P91-0017
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.82
0.19
1
8270E
12/3/19 12:06
JMV
P91-0017
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.82
0.22
1
8270E
12/3/19 12:06
JMV
P91-0017
Pentachlorophenol
BRL
mg/kg dry
1.2
0.52
1
8270E
12/3/19 12:06
JMV
P91-0017
Phenanthrene
3.8
mg/kg dry
0.82
0.0089
1
8270E
12/3/19 12:06
JMV
P91-0017
Phenol
BRL
mg/kg dry
0.82
0.13
1
8270E
12/3/19 12:06
JMV
P91-0017
Pyrene
0.48
J mg/kg dry
0.82
0.012
1
8270E
1213/19 12:06
JMV
P91-0017
Pyridine
BRL
mg/kg dry
0.41
0.078
1
8270E
12/3/19 12:06
JMV
P91-0017
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
75 %
39-132
2-Fluorobiphenyl
82 %
44-115
2-Fluorophenol
74 %
35-115
Nitrobenzene-d5
93 %
37-122
Phenol-d5
70 %
34-121
Terphenyl-d14
64 %
54-127
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 15 0f 56

/PRISM Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
12/04/2019
ATC Group Services, LLC
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Project: Tim Collins Property
Sample Matrix: Soil
Client Sample ID: SE-3
Prism Sample ID: 9110453-03
Prism Work Order: 9110453
Time Collected: 11/26/19 16:45
Time Submitted: 11/27/19 10:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GC/MS (Medium Level)
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.24
0.030
50
8260D
12/2/19 17:04
JLB
P91-0044
1,1,1-Trichloroethane
BRL
mg/kg dry
0.24
0.036
50
8260D
12/2/19 17:04
JLB
P91-0044
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.24
0.018
50
8260D
12/2/19 17:04
JLB
P91-0044
1,1,2-Trichloroethane
BRL
mg/kg dry
0.24
0.026
50
8260D
12/2/19 17:04
JLB
P91-0044
1,1-Dichloroethane
BRL
mg/kg dry
0.24
0.044
50
8260D
12/2/19 17:04
JLB
P91-0044
1,1-Dichloroethylene
BRL
mg/kg dry
0.24
0.045
50
8260D
12/2/19 17:04
JLB
P91-0044
1,1-Dichloropropylene
BRL
mg/kg dry
0.24
0.038
50
8260D
12/2/19 17:04
JLB
P91-0044
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.49
0.035
50
8260D
12/2/19 17:04
JLB
P91-0044
1,2,3-Trichloropropane
BRL
mg/kg dry
0.24
0.028
50
8260D
12/2/19 17:04
JLB
P91-0044
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.49
0.023
50
8260D
12/2/19 17:04
JLB
P91-0044
1,2,4-Trimethylbenzene
4.1
mg/kg dry
0.24
0.026
50
8260D
1212/19 17:04
JLB
P91-0044
1,2-Dibromoethane
BRL
mg/kg dry
0.24
0.022
50
8260D
12/2/19 17:04
JLB
P91-0044
1,2-Dichlorobenzene
BRL
mg/kg dry
0.24
0.027
50
8260D
12/2/19 17:04
JLB
P91-0044
1,2-Dichloroethane
BRL
mg/kg dry
0.24
0.029
50
8260D
12/2/19 17:04
JLB
P91-0044
1,2-Dichloropropane
BRL
mg/kg dry
0.24
0.037
50
8260D
12/2/19 17:04
JLB
P91-0044
1,3,5-Trimethylbenzene
1.1
mg/kg dry
0.24
0.031
50
8260D
1212/19 17:04
JLB
P91-0044
1,3-Dichlorobenzene
BRL
mg/kg dry
0.24
0.030
50
8260D
12/2/19 17:04
JLB
P91-0044
1,3-Dichloropropane
BRL
mg/kg dry
0.24
0.020
50
8260D
12/2/19 17:04
JLB
P91-0044
1,4-Dichlorobenzene
BRL
mg/kg dry
0.24
0.031
50
8260D
12/2/19 17:04
JLB
P91-0044
2,2-Dichloropropane
BRL
mg/kg dry
0.24
0.030
50
8260D
12/2/19 17:04
JLB
P91-0044
2-Chlorotoluene
BRL
mg/kg dry
0.24
0.033
50
8260D
12/2/19 17:04
JLB
P91-0044
4-Chlorotoluene
BRL
mg/kg dry
0.24
0.028
50
8260D
12/2/19 17:04
JLB
P91-0044
4-Isopropyltoluene
0.43
mg/kg dry
0.24
0.062
50
8260D
12/2/19 17:04
JLB
P91-0044
Acetone
BRL
mg/kg dry
0.98
0.062
50
8260D
12/2/19 17:04
JLB
P91-0044
Benzene
BRL
mg/kg dry
0.24
0.038
50
8260D
12/2/19 17:04
JLB
P91-0044
Bromobenzene
BRL
mg/kg dry
0.24
0.034
50
8260D
12/2/19 17:04
JLB
P91-0044
Bromochloromethane
BRL
mg/kg dry
0.24
0.040
50
8260D
12/2/19 17:04
JLB
P91-0044
Bromodichloromethane
BRL
mg/kg dry
0.24
0.023
50
8260D
12/2/19 17:04
JLB
P91-0044
Bromoform
BRL
mg/kg dry
0.24
0.019
50
8260D
12/2/19 17:04
JLB
P91-0044
Bromomethane
BRL
mg/kg dry
0.49
0.12
50
8260D
12/2/19 17:04
JLB
P91-0044
Carbon Tetrachloride
BRL
mg/kg dry
0.24
0.048
50
8260D
12/2/19 17:04
JLB
P91-0044
Chlorobenzene
BRL
mg/kg dry
0.24
0.038
50
8260D
12/2/19 17:04
JLB
P91-0044
Chloroethane
BRL
mg/kg dry
0.49
0.047
50
8260D
12/2/19 17:04
JLB
P91-0044
Chloroform
BRL
mg/kg dry
0.24
0.030
50
8260D
12/2/19 17:04
JLB
P91-0044
Chloromethane
BRL
mg/kg dry
0.49
0.074
50
8260D
12/2/19 17:04
JLB
P91-0044
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.24
0.038
50
8260D
12/2/19 17:04
JLB
P91-0044
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.24
0.024
50
8260D
12/2/19 17:04
JLB
P91-0044
Dibromochloromethane
BRL
mg/kg dry
0.24
0.016
50
8260D
12/2/19 17:04
JLB
P91-0044
Dichlorodifluoromethane
BRL
mg/kg dry
0.49
0.069
50
8260D
12/2/19 17:04
JLB
P91-0044
Ethylbenzene
0.60
mg/kg dry
0.24
0.037
50
8260D
12/2/19 17:04
JLB
P91-0044
Isopropyl Ether
BRL
mg/kg dry
0.24
0.036
50
8260D
12/2/19 17:04
JLB
P91-0044
Isopropyl benzene (Cumene)
0.37
mg/kg dry
0.24
0.028
50
8260D
12/2/19 17:04
JLB
P91-0044
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 16 0f 56

/PRISM Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
12/04/2019
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273 Sample Matrix: Soil
Client Sample ID: SE-3
Prism Sample ID: 9110453-03
Prism Work Order: 9110453
Time Collected: 11/26/19 16:45
Time Submitted: 11/27/19 10:00
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
m,p-Xylenes
1.7
mg/kg dry
0.49
0.063
50
8260D
12/2/19 17:04
JLB
P91-0044
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.98
0.017
50
8260D
12/2/19 17:04
JLB
P91-0044
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.98
0.057
50
8260D
12/2/19 17:04
JLB
P91-0044
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.98
0.020
50
8260D
12/2/19 17:04
JLB
P91-0044
Methylene Chloride
BRL
mg/kg dry
0.24
0.040
50
8260D
12/2/19 17:04
JLB
P91-0044
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.24
0.034
50
8260D
12/2/19 17:04
JLB
P91-0044
Naphthalene
3.7
mg/kg dry
0.49
0.025
50
8260D
12/2/19 17:04
JLB
P91-0044
n-Butylbenzene
0.63
mg/kg dry
0.24
0.023
50
8260D
1212/19 17:04
JLB
P91-0044
n-Propylbenzene
0.77
mg/kg dry
0.24
0.035
50
8260D
12/2/19 17:04
JLB
P91-0044
o-Xylene
0.68
mg/kg dry
0.24
0.026
50
8260D
12/2/19 17:04
JLB
P91-0044
sec-Butylbenzene
0.57
mg/kg dry
0.24
0.026
50
8260D
12/2/19 17:04
JLB
P91-0044
Styrene
BRL
mg/kg dry
0.24
0.024
50
8260D
12/2/19 17:04
JLB
P91-0044
tert-Butylbenzene
BRL
mg/kg dry
0.24
0.029
50
8260D
12/2/19 17:04
JLB
P91-0044
Tetrachloroethylene
BRL
mg/kg dry
0.24
0.044
50
8260D
12/2/19 17:04
JLB
P91-0044
Toluene
0.12 J
mg/kg dry
0.24
0.039
50
8260D
12/2/19 17:04
JLB
P91-0044
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.24
0.047
50
8260D
12/2/19 17:04
JLB
P91-0044
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.24
0.021
50
8260D
12/2/19 17:04
JLB
P91-0044
Trichloroethylene
BRL
mg/kg dry
0.24
0.047
50
8260D
12/2/19 17:04
JLB
P91-0044
Trichlorofluoromethane
BRL
mg/kg dry
0.49
0.066
50
8260D
12/2/19 17:04
JLB
P91-0044
Vinyl acetate
BRL
mg/kg dry
0.49
0.027
50
8260D
12/2/19 17:04
JLB
P91-0044
Vinyl chloride
BRL
mg/kg dry
0.49
0.048
50
8260D
12/2/19 17:04
JLB
P91-0044
Xylenes, total
2.3
mg/kg dry
0.73
0.088
50
8260D
12/2/19 17:04
JLB
P91-0044
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
97 %
70-130
Dibromofluoromethane
91 %
70-130
Toluene-d8
96 %
70-130
Volatile Petroleum Hydrocarbons
by GC/PID/FID
C5-C8 Aliphatics
7.1 J
mg/kg dry
16
3.1
100
MADEP VPH 11/27/19 19:17
TBL
P9K0496
C9-C12 Aliphatics
100
mg/kg dry
16
1.4
100
MADEP VPH 11/27/19 19:17
TBL
P91<0496
C9-C10 Aromatics
67
mg/kg dry
16
1.5
100
MADEP VPH 11/27/19 19:17
TBL
P91<0496
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
87 %
70-130
2,5-Dibromotoluene (FID)
102 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 17 of 56

/PRISM Full -Service Analytical s
Environmental Solutions
LABORATORIES INC.
Laboratory Report
12/04/2019
ATC Group Services, LLC
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Project: Tim Collins Property
Sample Matrix: Soil
Client Sample ID: SE-4
Prism Sample ID: 9110453-04
Prism Work Order: 9110453
Time Collected: 11/26/19 16:55
Time Submitted: 11/27/19 10:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics 1200 mg/kg dry 30 1.5 1 MADEP EPH 1214/19 4:16 ZRC P9K0497
C19-C36 Aliphatics 360 mg/kg dry 30 5.0 1 MADEP EPH 12/4/19 4:16 ZRC P9K0497
C11-C22 Aromatics 770 mg/kg dry 30 8.1 1 MADEP EPH 12/4/19 4:16 ZRC P91K0497
Surrogate Recovery Control Limits
1-Chlorooctadecane
120 %
40-140
o-Terphenyl
136 %
40-140
2-Fluorobiphenyl
108 %
40-140
2-Bromonaphthalene
99 %
40-140
General Chemistry Parameters
% Solids
84.1
% by
0.100
0.100
1
SM2540 G
12/3/19 8:14
EDV
P91-0025
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.78
0.14
1
8270E
12/3/19 12:29
JMV
P91-0017
1,2-Dichlorobenzene
BRL
mg/kg dry
0.78
0.13
1
8270E
12/3/19 12:29
JMV
P91-0017
1,3-Dichlorobenzene
BRL
mg/kg dry
0.78
0.12
1
8270E
12/3/19 12:29
JMV
P91-0017
1,4-Dichlorobenzene
BRL
mg/kg dry
0.39
0.12
1
8270E
12/3/19 12:29
JMV
P91-0017
1-Methyl naphthalene
BRL
mg/kg dry
0.78
0.012
1
8270E
12/3/19 12:29
JMV
P91-0017
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.78
0.17
1
8270E
12/3/19 12:29
JMV
P91-0017
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.78
0.19
1
8270E
12/3/19 12:29
JMV
P91-0017
2,4-Dichlorophenol
BRL
mg/kg dry
0.78
0.15
1
8270E
12/3/19 12:29
JMV
P91-0017
2,4-Dimethylphenol
BRL
mg/kg dry
0.39
0.16
1
8270E
12/3/19 12:29
JMV
P91-0017
2,4-Dinitrophenol
BRL
mg/kg dry
1.8
0.46
1
8270E
12/3/19 12:29
JMV
P91-0017
2,4-Dinitrotoluene
BRL
mg/kg dry
0.78
0.21
1
8270E
12/3/19 12:29
JMV
P91-0017
2,6-Dinitrotoluene
BRL
mg/kg dry
0.78
0.20
1
8270E
12/3/19 12:29
JMV
P91-0017
2-Chloronaphthalene
BRL
mg/kg dry
0.78
0.19
1
8270E
12/3/19 12:29
JMV
P91-0017
2-Chlorophenol
BRL
mg/kg dry
0.78
0.15
1
8270E
12/3/19 12:29
JMV
P91-0017
2-Methyl naphthalene
BRL
mg/kg dry
0.78
0.015
1
8270E
12/3/19 12:29
JMV
P91-0017
2-Methylphenol
BRL
mg/kg dry
0.78
0.15
1
8270E
12/3/19 12:29
JMV
P91-0017
2-Nitrophenol
BRL
mg/kg dry
0.78
0.13
1
8270E
12/3/19 12:29
JMV
P91-0017
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.78
0.16
1
8270E
12/3/19 12:29
JMV
P91-0017
3/4-Methyl phenol
BRL
mg/kg dry
0.78
0.17
1
8270E
12/3/19 12:29
JMV
P91-0017
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.8
0.43
1
8270E
12/3/19 12:29
JMV
P91-0017
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.78
0.18
1
8270E
12/3/19 12:29
JMV
P91-0017
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.78
0.15
1
8270E
12/3/19 12:29
JMV
P91-0017
4-Chloroaniline
BRL
mg/kg dry
0.39
0.095
1
8270E
12/3/19 12:29
JMV
P91-0017
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.2
0.24
1
8270E
12/3/19 12:29
JMV
P91-0017
4-Nitrophenol
BRL
mg/kg dry
0.78
0.19
1
8270E
12/3/19 12:29
JMV
P91-0017
Acenaphthene
BRL
mg/kg dry
0.78
0.018
1
8270E
12/3/19 12:29
JMV
P91-0017
Acenaphthylene
BRL
mg/kg dry
0.78
0.015
1
8270E
12/3/19 12:29
JMV
P91-0017
Anthracene
BRL
mg/kg dry
0.78
0.0087
1
8270E
12/3/19 12:29
JMV
P91-0017
Azobenzene
BRL
mg/kg dry
0.78
0.17
1
8270E
12/3/19 12:29
JMV
P91-0017
Benzo(a)anthracene
BRL
mg/kg dry
0.78
0.0094
1
8270E
12/3/19 12:29
JMV
P91-0017
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 18 0f 56

Report
Full -Service Analytical &
PRISMLaboratory
Environmental Solutions
LABORATORIES INC.
12/04/2019
ATC Group Services, LLC
Project: Tim Collins Property
Client Sample ID: SE-4
Attn: Al Quarles
Prism Sample ID: 9110453-04
7606 Whitehall Executive Center Drive, Suite
Prism Work Order:
9110453
Charlotte, NC 28273
Sample Matrix: Soil
Time Collected:
11/26/19 16:55
Time Submitted:
11/27/19 10:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Benzo(a)pyrene
BRL
mg/kg dry
0.78
0.0070
1
8270E
12/3/19 12:29
JMV
P91-0017
Benzo(b)fluoranthene
BRL
mg/kg dry
0.78
0.0072
1
8270E
12/3/19 12:29
JMV
P91-0017
Benzo(g,h,i)perylene
BRL
mg/kg dry
0.78
0.0077
1
8270E
12/3/19 12:29
JMV
P91-0017
Benzo(k)fluoranthene
BRL
mg/kg dry
0.78
0.0083
1
8270E
12/3/19 12:29
JMV
P91-0017
Benzoic Acid
BRL
mg/kg dry
2.4
0.65
1
8270E
12/3/19 12:29
JMV
P91-0017
Benzyl alcohol
BRL
mg/kg dry
0.78
0.15
1
8270E
12/3/19 12:29
JMV
P91-0017
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.78
0.15
1
8270E
12/3/19 12:29
JMV
P91-0017
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.78
0.13
1
8270E
12/3/19 12:29
JMV
P91-0017
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.39
0.14
1
8270E
12/3/19 12:29
JMV
P91-0017
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.78
0.18
1
8270E
12/3/19 12:29
JMV
P91-0017
Butyl benzyl phthalate
BRL
mg/kg dry
0.39
0.14
1
8270E
12/3/19 12:29
JMV
P91-0017
Chrysene
BRL
mg/kg dry
0.78
0.0093
1
8270E
12/3/19 12:29
JMV
P91-0017
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.78
0.023
1
8270E
12/3/19 12:29
JMV
P91-0017
Dibenzofuran
BRL
mg/kg dry
0.78
0.21
1
8270E
12/3/19 12:29
JMV
P91-0017
Diethyl phthalate
BRL
mg/kg dry
0.78
0.20
1
8270E
12/3/19 12:29
JMV
P91-0017
Dimethyl phthalate
BRL
mg/kg dry
0.78
0.19
1
8270E
12/3/19 12:29
JMV
P91-0017
Di-n-butyl phthalate
BRL
mg/kg dry
0.78
0.19
1
8270E
12/3/19 12:29
JMV
P91-0017
Di-n-octyl phthalate
BRL
mg/kg dry
0.39
0.20
1
8270E
12/3/19 12:29
JMV
P91-0017
Fluoranthene
BRL
mg/kg dry
0.78
0.0089
1
8270E
12/3/19 12:29
JMV
P91-0017
Fluorene
BRL
mg/kg dry
0.78
0.014
1
8270E
12/3/19 12:29
JMV
P91-0017
Hexachlorobenzene
BRL
mg/kg dry
0.78
0.17
1
8270E
12/3/19 12:29
JMV
P91-0017
Hexachlorobutadiene
BRL
mg/kg dry
0.78
0.18
1
8270E
12/3/19 12:29
JMV
P91-0017
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.78
0.27
1
8270E
12/3/19 12:29
JMV
P91-0017
Hexachloroethane
BRL
mg/kg dry
0.78
0.12
1
8270E
12/3/19 12:29
JMV
P91-0017
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.78
0.022
1
8270E
12/3/19 12:29
JMV
P91-0017
Isophorone
BRL
mg/kg dry
0.78
0.17
1
8270E
12/3/19 12:29
JMV
P91-0017
Naphthalene
BRL
mg/kg dry
0.78
0.017
1
8270E
12/3/19 12:29
JMV
P91-0017
Nitrobenzene
BRL
mg/kg dry
0.39
0.17
1
8270E
12/3/19 12:29
JMV
P91-0017
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.78
0.18
1
8270E
12/3/19 12:29
JMV
P91-0017
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.78
0.21
1
8270E
12/3/19 12:29
JMV
P91-0017
Pentachlorophenol
BRL
mg/kg dry
1.2
0.50
1
8270E
12/3/19 12:29
JMV
P91-0017
Phenanthrene
BRL
mg/kg dry
0.78
0.0085
1
8270E
12/3/19 12:29
JMV
P91-0017
Phenol
BRL
mg/kg dry
0.78
0.13
1
8270E
12/3/19 12:29
JMV
P91-0017
Pyrene
BRL
mg/kg dry
0.78
0.011
1
8270E
12/3/19 12:29
JMV
P91-0017
Pyridine
BRL
mg/kg dry
0.39
0.075
1
8270E
12/3/19 12:29
JMV
P91-0017
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
81 %
39-132
2-Fluorobiphenyl
75 %
44-115
2-Fluorophenol
73 %
35-115
Nitrobenzene-d5
64 %
37-122
Phenol-d5
72 %
34-121
Terphenyl-d14
71 %
54-127
Volatile Organic Compounds by GC/MS
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 19 of 56

Full -Service Analytical &
PRISMLaboratory
Environmental Solutions
LABORATORIES INC.
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273 Sample Matrix: Soil
Report
12/04/2019
Client Sample ID: SE-4
Prism Sample ID: 9110453-04
Prism Work Order: 9110453
Time Collected: 11/26/19 16:55
Time Submitted: 11/27/19 10:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0056
0.00068
1
8260D
12/3/19 13:13
JLB
P91-0050
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0056
0.00082
1
8260D
12/3/19 13:13
JLB
P91-0050
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0056
0.00041
1
8260D
12/3/19 13:13
JLB
P91-0050
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0056
0.00060
1
8260D
12/3/19 13:13
JLB
P91-0050
1,1-Dichloroethane
BRL
mg/kg dry
0.0056
0.0010
1
8260D
12/3/19 13:13
JLB
P91-0050
1,1-Dichloroethylene
BRL
mg/kg dry
0.0056
0.0010
1
8260D
12/3/19 13:13
JLB
P91-0050
1,1-Dichloropropylene
BRL
mg/kg dry
0.0056
0.00086
1
8260D
12/3/19 13:13
JLB
P91-0050
1,2,3-Trichlorobenzene
0.0011 J
mg/kg dry
0.011
0.00080
1
8260D
12/3/19 13:13
JLB
P91-0050
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0056
0.00063
1
8260D
12/3/19 13:13
JLB
P91-0050
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00053
1
8260D
12/3/19 13:13
JLB
P91-0050
1,2,4-Trimethylbenzene
0.0027 J
mg/kg dry
0.0056
0.00059
1
8260D
12/3/19 13:13
JLB
P91-0050
1,2-Dibromoethane
BRL
mg/kg dry
0.0056
0.00050
1
8260D
12/3/19 13:13
JLB
P91-0050
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0056
0.00062
1
8260D
12/3/19 13:13
JLB
P91-0050
1,2-Dichloroethane
BRL
mg/kg dry
0.0056
0.00066
1
8260D
12/3/19 13:13
JLB
P91-0050
1,2-Dichloropropane
BRL
mg/kg dry
0.0056
0.00084
1
8260D
12/3/19 13:13
JLB
P91-0050
1,3,5-Trimethylbenzene
0.00099 J
mg/kg dry
0.0056
0.00070
1
8260D
12/3/19 13:13
JLB
P91-0050
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0056
0.00069
1
8260D
12/3/19 13:13
JLB
P91-0050
1,3-Dichloropropane
BRL
mg/kg dry
0.0056
0.00047
1
8260D
12/3/19 13:13
JLB
P91-0050
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0056
0.00071
1
8260D
12/3/19 13:13
JLB
P91-0050
2,2-Dichloropropane
BRL
mg/kg dry
0.0056
0.00070
1
8260D
12/3/19 13:13
JLB
P91-0050
2-Chlorotoluene
BRL
mg/kg dry
0.0056
0.00075
1
8260D
12/3/19 13:13
JLB
P91-0050
4-Chlorotoluene
BRL
mg/kg dry
0.0056
0.00064
1
8260D
12/3/19 13:13
JLB
P91-0050
4-Isopropyltoluene
BRL
mg/kg dry
0.0056
0.0014
1
8260D
12/3/19 13:13
JLB
P91-0050
Acetone
BRL
mg/kg dry
0.022
0.0014
1
8260D
12/3/19 13:13
JLB
P91-0050
Benzene
BRL
mg/kg dry
0.0056
0.00087
1
8260D
12/3/19 13:13
JLB
P91-0050
Bromobenzene
BRL
mg/kg dry
0.0056
0.00078
1
8260D
12/3/19 13:13
JLB
P91-0050
Bromochloromethane
BRL
mg/kg dry
0.0056
0.00092
1
8260D
12/3/19 13:13
JLB
P91-0050
Bromodichloromethane
BRL
mg/kg dry
0.0056
0.00053
1
8260D
12/3/19 13:13
JLB
P91-0050
Bromoform
BRL
mg/kg dry
0.0056
0.00043
1
8260D
12/3/19 13:13
JLB
P91-0050
Bromomethane
BRL
mg/kg dry
0.011
0.0027
1
8260D
12/3/19 13:13
JLB
P91-0050
Carbon Tetrachloride
BRL
mg/kg dry
0.0056
0.0011
1
8260D
12/3/19 13:13
JLB
P91-0050
Chlorobenzene
BRL
mg/kg dry
0.0056
0.00087
1
8260D
12/3/19 13:13
JLB
P91-0050
Chloroethane
BRL
mg/kg dry
0.011
0.0011
1
8260D
12/3/19 13:13
JLB
P91-0050
Chloroform
BRL
mg/kg dry
0.0056
0.00068
1
8260D
12/3/19 13:13
JLB
P91-0050
Chloromethane
BRL
mg/kg dry
0.011
0.0017
1
8260D
12/3/19 13:13
JLB
P91-0050
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0056
0.00088
1
8260D
12/3/19 13:13
JLB
P91-0050
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0056
0.00055
1
8260D
12/3/19 13:13
JLB
P91-0050
Dibromochloromethane
BRL
mg/kg dry
0.0056
0.00037
1
8260D
12/3/19 13:13
JLB
P91-0050
Dichlorodifluoromethane
BRL
mg/kg dry
0.011
0.0016
1
8260D
12/3/19 13:13
JLB
P91-0050
Ethylbenzene
0.0011 J
mg/kg dry
0.0056
0.00084
1
8260D
12/3/19 13:13
JLB
P91-0050
Isopropyl Ether
BRL
mg/kg dry
0.0056
0.00082
1
8260D
12/3/19 13:13
JLB
P91-0050
Isopropylbenzene (Cumene)
BRL
mg/kg dry
0.0056
0.00065
1
8260D
12/3/19 13:13
JLB
P91-0050
m,p-Xylenes
0.0026 J
mg/kg dry
0.011
0.0014
1
8260D
12/3/19 13:13
JLB
P91-0050
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 20 0f 56

/PRISM Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
12/04/2019
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273 Sample Matrix: Soil
Client Sample ID: SE-4
Prism Sample ID: 9110453-04
Prism Work Order: 9110453
Time Collected: 11/26/19 16:55
Time Submitted: 11/27/19 10:00
Parameter
Result
Units
Report
MDL Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.022
0.00039
1
8260D
12/3/19 13:13
JLB
P91-0050
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.022
0.0013
1
8260D
12/3/19 13:13
JLB
P91-0050
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.022
0.00046
1
8260D
12/3/19 13:13
JLB
P91-0050
Methylene Chloride
BRL
mg/kg dry
0.0056
0.00090
1
8260D
12/3/19 13:13
JLB
P91-0050
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0056
0.00078
1
8260D
12/3/19 13:13
JLB
P91-0050
Naphthalene
0.0020 J
mg/kg dry
0.011
0.00056
1
8260D
12/3/19 13:13
JLB
P91-0050
n-Butylbenzene
BRL
mg/kg dry
0.0056
0.00052
1
8260D
12/3/19 13:13
JLB
P91-0050
n-Propylbenzene
0.00092 J
mg/kg dry
0.0056
0.00081
1
8260D
12/3/19 13:13
JLB
P91-0050
o-Xylene
0.0017 J
mg/kg dry
0.0056
0.00059
1
8260D
12/3/19 13:13
JLB
P91-0050
sec-Butylbenzene
0.00075 J
mg/kg dry
0.0056
0.00060
1
8260D
1213/19 13:13
JLB
P91-0050
Styrene
BRL
mg/kg dry
0.0056
0.00054
1
8260D
12/3/19 13:13
JLB
P91-0050
tert-Butylbenzene
BRL
mg/kg dry
0.0056
0.00066
1
8260D
12/3/19 13:13
JLB
P91-0050
Tetrachloroethylene
BRL
mg/kg dry
0.0056
0.0010
1
8260D
12/3/19 13:13
JLB
P91-0050
Toluene
BRL
mg/kg dry
0.0056
0.00089
1
8260D
12/3/19 13:13
JLB
P91-0050
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0056
0.0011
1
8260D
12/3/19 13:13
JLB
P91-0050
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0056
0.00048
1
8260D
12/3/19 13:13
JLB
P91-0050
Trichloroethylene
BRL
mg/kg dry
0.0056
0.0011
1
8260D
12/3/19 13:13
JLB
P91-0050
Trichlorofluoromethane
BRL
mg/kg dry
0.011
0.0015
1
8260D
12/3/19 13:13
JLB
P91-0050
Vinyl acetate
BRL
mg/kg dry
0.011
0.00061
1
8260D
12/3/19 13:13
JLB
P91-0050
Vinyl chloride
BRL
mg/kg dry
0.011
0.0011
1
8260D
12/3/19 13:13
JLB
P91-0050
Xylenes, total
0.0043 J
mg/kg dry
0.017
0.0020
1
8260D
12/3/19 13:13
JLB
P91-0050
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
99 %
70-130
Dibromofluoromethane
98 %
84-123
Toluene-d8
93 %
76-129
Volatile Petroleum Hydrocarbons by GC/PID/FID
C5-C8 Aliphatics
BRL
mg/kg dry
18
3.5
100
MADEP VPH 11/27/19 20:44
TBL
P9K0496
C9-C12 Aliphatics
13 J
mg/kg dry
18
1.6
100
MADEP VPH 11/27/19 20:44
TBL
P9K0496
C9-Cl0 Aromatics
BRL
mg/kg dry
18
1.7
100
MADEP VPH 11/27/19 20:44
TBL
P9K0496
Surrogate
Recovery
Control Limits
2,5-Dibromotoluene (PID)
92 %
70-130
2,5-Dibromotoluene
(FID)
107 %
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 21 of 56

/PRISM Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
12/04/2019
ATC Group Services, LLC
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Project: Tim Collins Property
Sample Matrix: Soil
Client Sample ID: SE-5
Prism Sample ID: 9110453-05
Prism Work Order: 9110453
Time Collected: 11/26/19 17:05
Time Submitted: 11/27/19 10:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Extractable Petroleum Hydrocarbons by GC/FID
C9-C18 Aliphatics 2000
mg/kg dry 140 7.2 5 MADEP EPH 1214/19 8:10 ZRC P9K0497
C19-C36 Aliphatics 540
mg/kg dry 29 4.8 1 MADEP EPH 12/4/19 4:53 ZRC P9K0497
C11-C22 Aromatics 1200
mg/kg dry 29 7.8 1 MADEP EPH 12/4/19 4:53 ZRC P91K0497
Surrogate Recovery Control Limits
1-Chlorooctadecane
135 %
40-140
o-Terphenyl
136 %
40-140
2-Fluorobiphenyl
119 %
40-140
2-Bromonaphthalene
96 %
40-140
General Chemistry Parameters
% Solids
87.2
% by
0.100
0.100
1
SM2540 G
12/3/19 8:14
EDV
P91-0025
Weight
Semivolatile Organic Compounds by GC/MS
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.76
0.13
1
8270E
12/3/19 12:51
JMV
P91-0017
1,2-Dichlorobenzene
BRL
mg/kg dry
0.76
0.12
1
8270E
12/3/19 12:51
JMV
P91-0017
1,3-Dichlorobenzene
BRL
mg/kg dry
0.76
0.11
1
8270E
12/3/19 12:51
JMV
P91-0017
1,4-Dichlorobenzene
BRL
mg/kg dry
0.38
0.12
1
8270E
12/3/19 12:51
JMV
P91-0017
1-Methyl naphthalene
4.9
mg/kg dry
0.76
0.012
1
8270E
1213/19 12:51
JMV
P91-0017
2,4,5-Trichlorophenol
BRL
mg/kg dry
0.76
0.16
1
8270E
12/3/19 12:51
JMV
P91-0017
2,4,6-Trichlorophenol
BRL
mg/kg dry
0.76
0.18
1
8270E
12/3/19 12:51
JMV
P91-0017
2,4-Dichlorophenol
BRL
mg/kg dry
0.76
0.15
1
8270E
12/3/19 12:51
JMV
P91-0017
2,4-Dimethylphenol
BRL
mg/kg dry
0.38
0.16
1
8270E
12/3/19 12:51
JMV
P91-0017
2,4-Dinitrophenol
BRL
mg/kg dry
1.7
0.44
1
8270E
12/3/19 12:51
JMV
P91-0017
2,4-Dinitrotoluene
BRL
mg/kg dry
0.76
0.20
1
8270E
12/3/19 12:51
JMV
P91-0017
2,6-Dinitrotoluene
BRL
mg/kg dry
0.76
0.20
1
8270E
12/3/19 12:51
JMV
P91-0017
2-Chloronaphthalene
BRL
mg/kg dry
0.76
0.18
1
8270E
12/3/19 12:51
JMV
P91-0017
2-Chlorophenol
BRL
mg/kg dry
0.76
0.14
1
8270E
12/3/19 12:51
JMV
P91-0017
2-Methyl naphthalene
7.5
mg/kg dry
0.76
0.015
1
8270E
12/3/19 12:51
JMV
P91-0017
2-Methylphenol
BRL
mg/kg dry
0.76
0.14
1
8270E
12/3/19 12:51
JMV
P91-0017
2-Nitrophenol
BRL
mg/kg dry
0.76
0.13
1
8270E
12/3/19 12:51
JMV
P91-0017
3,3'-Dichlorobenzidine
BRL
mg/kg dry
0.76
0.15
1
8270E
12/3/19 12:51
JMV
P91-0017
3/4-Methyl phenol
BRL
mg/kg dry
0.76
0.16
1
8270E
12/3/19 12:51
JMV
P91-0017
4,6-Dinitro-2-methylphenol
BRL
mg/kg dry
1.7
0.42
1
8270E
12/3/19 12:51
JMV
P91-0017
4-Bromophenyl phenyl ether
BRL
mg/kg dry
0.76
0.18
1
8270E
12/3/19 12:51
JMV
P91-0017
4-Chloro-3-methylphenol
BRL
mg/kg dry
0.76
0.14
1
8270E
12/3/19 12:51
JMV
P91-0017
4-Chloroaniline
BRL
mg/kg dry
0.38
0.092
1
8270E
12/3/19 12:51
JMV
P91-0017
4-Chlorophenyl phenyl ether
BRL
mg/kg dry
1.1
0.23
1
8270E
12/3/19 12:51
JMV
P91-0017
4-Nitrophenol
BRL
mg/kg dry
0.76
0.19
1
8270E
12/3/19 12:51
JMV
P91-0017
Acenaphthene
BRL
mg/kg dry
0.76
0.017
1
8270E
12/3/19 12:51
JMV
P91-0017
Acenaphthylene
BRL
mg/kg dry
0.76
0.015
1
8270E
12/3/19 12:51
JMV
P91-0017
Anthracene
BRL
mg/kg dry
0.76
0.0084
1
8270E
12/3/19 12:51
JMV
P91-0017
Azobenzene
BRL
mg/kg dry
0.76
0.16
1
8270E
12/3/19 12:51
JMV
P91-0017
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 22 0f 56

Full -Service Analytical &
PRISMLaboratory
Environmental Solutions
LABORATORIES INC.
ATC Group Services, LLC
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Project: Tim Collins Property
Sample Matrix: Soil
Report
12/04/2019
Client Sample ID: SE-5
Prism Sample ID: 9110453-05
Prism Work Order: 9110453
Time Collected: 11/26/19 17:05
Time Submitted: 11/27/19 10:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis
Analyst
Batch
Limit
Factor
Date/Time
ID
Benzo(a)anthracene
BRL
mg/kg dry
0.76
0.0091
1
8270E
12/3/19 12:51
JMV
P91-0017
Benzo(a)pyrene
BRL
mg/kg dry
0.76
0.0068
1
8270E
12/3/19 12:51
JMV
P91-0017
Benzo(b)fluoranthene
BRL
mg/kg dry
0.76
0.0070
1
8270E
12/3/19 12:51
JMV
P91-0017
Benzo(g,hJ)perylene
BRL
mg/kg dry
0.76
0.0075
1
8270E
12/3/19 12:51
JMV
P91-0017
Benzo(k)fluoranthene
BRL
mg/kg dry
0.76
0.0080
1
8270E
12/3/19 12:51
JMV
P91-0017
Benzoic Acid
BRL
mg/kg dry
2.3
0.63
1
8270E
12/3/19 12:51
JMV
P91-0017
Benzyl alcohol
BRL
mg/kg dry
0.76
0.14
1
8270E
12/3/19 12:51
JMV
P91-0017
bis(2-Chloroethoxy)methane
BRL
mg/kg dry
0.76
0.14
1
8270E
12/3/19 12:51
JMV
P91-0017
Bis(2-Chloroethyl)ether
BRL
mg/kg dry
0.76
0.12
1
8270E
12/3/19 12:51
JMV
P91-0017
Bis(2-chloroisopropyl)ether
BRL
mg/kg dry
0.38
0.14
1
8270E
12/3/19 12:51
JMV
P91-0017
Bis(2-Ethylhexyl)phthalate
BRL
mg/kg dry
0.76
0.17
1
8270E
12/3/19 12:51
JMV
P91-0017
Butyl benzyl phthalate
BRL
mg/kg dry
0.38
0.13
1
8270E
12/3/19 12:51
JMV
P91-0017
Chrysene
BRL
mg/kg dry
0.76
0.0089
1
8270E
12/3/19 12:51
JMV
P91-0017
Dibenzo(a,h)anthracene
BRL
mg/kg dry
0.76
0.022
1
8270E
12/3/19 12:51
JMV
P91-0017
Dibenzofuran
BRL
mg/kg dry
0.76
0.20
1
8270E
12/3/19 12:51
JMV
P91-0017
Diethyl phthalate
BRL
mg/kg dry
0.76
0.19
1
8270E
12/3/19 12:51
JMV
P91-0017
Dimethyl phthalate
BRL
mg/kg dry
0.76
0.18
1
8270E
12/3/19 12:51
JMV
P91-0017
Di-n-butyl phthalate
BRL
mg/kg dry
0.76
0.19
1
8270E
12/3/19 12:51
JMV
P91-0017
Di-n-octyl phthalate
BRL
mg/kg dry
0.38
0.20
1
8270E
12/3/19 12:51
JMV
P91-0017
Fluoranthene
BRL
mg/kg dry
0.76
0.0086
1
8270E
12/3/19 12:51
JMV
P91-0017
Fluorene
1.1
mg/kg dry
0.76
0.013
1
8270E
12/3/19 12:51
JMV
P91-0017
Hexachlorobenzene
BRL
mg/kg dry
0.76
0.17
1
8270E
12/3/19 12:51
JMV
P91-0017
Hexachlorobutadiene
BRL
mg/kg dry
0.76
0.17
1
8270E
12/3/19 12:51
JMV
P91-0017
Hexachlorocyclopentadiene
BRL
mg/kg dry
0.76
0.26
1
8270E
12/3/19 12:51
JMV
P91-0017
Hexachloroethane
BRL
mg/kg dry
0.76
0.12
1
8270E
12/3/19 12:51
JMV
P91-0017
Indeno(1,2,3-cd)pyrene
BRL
mg/kg dry
0.76
0.021
1
8270E
12/3/19 12:51
JMV
P91-0017
Isophorone
BRL
mg/kg dry
0.76
0.16
1
8270E
12/3/19 12:51
JMV
P91-0017
Naphthalene
1.8
mg/kg dry
0.76
0.016
1
8270E
1213/19 12:51
JMV
P91-0017
Nitrobenzene
BRL
mg/kg dry
0.38
0.16
1
8270E
12/3/19 12:51
JMV
P91-0017
N-Nitroso-di-n-propylamine
BRL
mg/kg dry
0.76
0.17
1
8270E
12/3/19 12:51
JMV
P91-0017
N-Nitrosodiphenylamine
BRL
mg/kg dry
0.76
0.21
1
8270E
12/3/19 12:51
JMV
P91-0017
Pentachlorophenol
BRL
mg/kg dry
1.1
0.48
1
8270E
12/3/19 12:51
JMV
P91-0017
Phenanthrene
2.2
mg/kg dry
0.76
0.0083
1
8270E
12/3/19 12:51
JMV
P91-0017
Phenol
BRL
mg/kg dry
0.76
0.12
1
8270E
12/3/19 12:51
JMV
P91-0017
Pyrene
0.22
J mg/kg dry
0.76
0.011
1
8270E
1213/19 12:51
JMV
P91-0017
Pyridine
BRL
mg/kg dry
0.38
0.072
1
8270E
12/3/19 12:51
JMV
P91-0017
Surrogate
Recovery
Control Limits
2,4,6-Tribromophenol
72 %
39-132
2-Fluorobiphenyl
78 %
44-115
2-Fluorophenol
72 %
35-115
Nitrobenzene-d5
75 %
37-122
Phenol-d5
69 %
34-121
Terphenyl-d14
66 %
54-127
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 23 0f 56

/PRISM Full -Service Analytical Environmental Solutions
LABORATORIES INC.
Laboratory Report
12/04/2019
ATC Group Services, LLC
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Project: Tim Collins Property
Sample Matrix: Soil
Client Sample ID: SE-5
Prism Sample ID: 9110453-05
Prism Work Order: 9110453
Time Collected: 11/26/19 17:05
Time Submitted: 11/27/19 10:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Volatile Organic Compounds by GUMS
1,1,1,2-Tetrachloroethane
BRL
mg/kg dry
0.0054
0.00066
1
8260D
12/2/19 13:49
JLB
P91-0043
1,1,1-Trichloroethane
BRL
mg/kg dry
0.0054
0.00079
1
8260D
12/2/19 13:49
JLB
P91-0043
1,1,2,2-Tetrachloroethane
BRL
mg/kg dry
0.0054
0.00039
1
8260D
12/2/19 13:49
JLB
P91-0043
1,1,2-Trichloroethane
BRL
mg/kg dry
0.0054
0.00058
1
8260D
12/2/19 13:49
JLB
P91-0043
1,1-Dichloroethane
BRL
mg/kg dry
0.0054
0.00097
1
8260D
12/2/19 13:49
JLB
P91-0043
1,1-Dichloroethylene
BRL
mg/kg dry
0.0054
0.00099
1
8260D
12/2/19 13:49
JLB
P91-0043
1,1-Dichloropropylene
BRL
mg/kg dry
0.0054
0.00083
1
8260D
12/2/19 13:49
JLB
P91-0043
1,2,3-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00077
1
8260D
12/2/19 13:49
JLB
P91-0043
1,2,3-Trichloropropane
BRL
mg/kg dry
0.0054
0.00061
1
8260D
12/2/19 13:49
JLB
P91-0043
1,2,4-Trichlorobenzene
BRL
mg/kg dry
0.011
0.00052
1
8260D
12/2/19 13:49
JLB
P91-0043
1,2,4-Trimethyl benzene
See 8260ML
mg/kg dry
0.0054
0.00057
1
8260D
12/2/19 13:49
JLB
P91-0043
1,2-Dibromoethane
BRL
mg/kg dry
0.0054
0.00048
1
8260D
12/2/19 13:49
JLB
P91-0043
1,2-Dichlorobenzene
BRL
mg/kg dry
0.0054
0.00060
1
8260D
12/2/19 13:49
JLB
P91-0043
1,2-Dichloroethane
BRL
mg/kg dry
0.0054
0.00064
1
8260D
12/2/19 13:49
JLB
P91-0043
1,2-Dichloropropane
BRL
mg/kg dry
0.0054
0.00081
1
8260D
12/2/19 13:49
JLB
P91-0043
1,3,5-Trimethyl benzene
See 8260ML
mg/kg dry
0.0054
0.00068
1
8260D
12/2/19 13:49
JLB
P91-0043
1,3-Dichlorobenzene
BRL
mg/kg dry
0.0054
0.00067
1
8260D
12/2/19 13:49
JLB
P91-0043
1,3-Dichloropropane
BRL
mg/kg dry
0.0054
0.00045
1
8260D
12/2/19 13:49
JLB
P91-0043
1,4-Dichlorobenzene
BRL
mg/kg dry
0.0054
0.00068
1
8260D
12/2/19 13:49
JLB
P91-0043
2,2-Dichloropropane
BRL
mg/kg dry
0.0054
0.00067
1
8260D
12/2/19 13:49
JLB
P91-0043
2-Chlorotoluene
BRL
mg/kg dry
0.0054
0.00072
1
8260D
12/2/19 13:49
JLB
P91-0043
4-Chlorotoluene
BRL
mg/kg dry
0.0054
0.00062
1
8260D
12/2/19 13:49
JLB
P91-0043
4-Isopropyltoluene
0.12
mg/kg dry
0.0054
0.0014
1
8260D
12/2/19 13:49
JLB
P91-0043
Acetone
BRL
mg/kg dry
0.022
0.0014
1
8260D
12/2/19 13:49
JLB
P91-0043
Benzene
0.0096
mg/kg dry
0.0054
0.00084
1
8260D
12/2/19 13:49
JLB
P91-0043
Bromobenzene
BRL
mg/kg dry
0.0054
0.00075
1
8260D
12/2/19 13:49
JLB
P91-0043
Bromochloromethane
BRL
mg/kg dry
0.0054
0.00089
1
8260D
12/2/19 13:49
JLB
P91-0043
Bromodichloromethane
BRL
mg/kg dry
0.0054
0.00051
1
8260D
12/2/19 13:49
JLB
P91-0043
Bromoform
BRL
mg/kg dry
0.0054
0.00042
1
8260D
12/2/19 13:49
JLB
P91-0043
Bromomethane
BRL
mg/kg dry
0.011
0.0026
1
8260D
12/2/19 13:49
JLB
P91-0043
Carbon Tetrachloride
BRL
mg/kg dry
0.0054
0.0011
1
8260D
12/2/19 13:49
JLB
P91-0043
Chlorobenzene
BRL
mg/kg dry
0.0054
0.00084
1
8260D
12/2/19 13:49
JLB
P91-0043
Chloroethane
BRL
mg/kg dry
0.011
0.0010
1
8260D
12/2/19 13:49
JLB
P91-0043
Chloroform
BRL
mg/kg dry
0.0054
0.00066
1
8260D
12/2/19 13:49
JLB
P91-0043
Chloromethane
BRL
mg/kg dry
0.011
0.0016
1
8260D
12/2/19 13:49
JLB
P91-0043
cis-1,2-Dichloroethylene
BRL
mg/kg dry
0.0054
0.00085
1
8260D
12/2/19 13:49
JLB
P91-0043
cis-1,3-Dichloropropylene
BRL
mg/kg dry
0.0054
0.00053
1
8260D
12/2/19 13:49
JLB
P91-0043
Dibromochloromethane
BRL
mg/kg dry
0.0054
0.00036
1
8260D
12/2/19 13:49
JLB
P91-0043
Dichlorodifluoromethane
BRL
mg/kg dry
0.011
0.0015
1
8260D
12/2/19 13:49
JLB
P91-0043
Ethylbenzene
0.32
mg/kg dry
0.0054
0.00081
1
8260D
12/2/19 13:49
JLB
P91-0043
Isopropyl Ether
BRL
mg/kg dry
0.0054
0.00079
1
8260D
12/2/19 13:49
JLB
P91-0043
Isopropyl benzene (Cumene)
0.17
mg/kg dry
0.0054
0.00063
1
8260D
12/2/19 13:49
JLB
P91-0043
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 24 0f 56

PRISMLaboratory Report
Full -Service Analytical &
Environmental Solutions 12/04/2019
LABORATORIES INC.
ATC Group Services, LLC Project: Tim Collins Property Client Sample ID: SE-5
Attn: Al Quarles Prism Sample ID: 9110453-05
7606 Whitehall Executive Center Drive, Suite Prism Work Order: 9110453
Charlotte, NC 28273 Sample Matrix: Soil Time Collected: 11/26/19 17:05
Time Submitted: 11/27/19 10:00
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
m,p-Xylenes
See 8260ML
mg/kg dry
0.011
0.0014
1
8260D
12/2/19 13:49
JLB
P91-0043
Methyl Butyl Ketone (2-Hexanone)
BRL
mg/kg dry
0.022
0.00037
1
8260D
12/2/19 13:49
JLB
P91-0043
Methyl Ethyl Ketone (2-Butanone)
BRL
mg/kg dry
0.022
0.0013
1
8260D
12/2/19 13:49
JLB
P91-0043
Methyl Isobutyl Ketone
BRL
mg/kg dry
0.022
0.00044
1
8260D
12/2/19 13:49
JLB
P91-0043
Methylene Chloride
BRL
mg/kg dry
0.0054
0.00087
1
8260D
12/2/19 13:49
JLB
P91-0043
Methyl-tert-Butyl Ether
BRL
mg/kg dry
0.0054
0.00076
1
8260D
12/2/19 13:49
JLB
P91-0043
Naphthalene
0.19
mg/kg dry
0.011
0.00055
1
8260D
12/2/19 13:49
JLB
P91-0043
n-Butylbenzene
0.14
mg/kg dry
0.0054
0.00051
1
8260D
12/2/19 13:49
JLB
P91-0043
n-Propylbenzene
See 8260ML
mg/kg dry
0.0054
0.00078
1
8260D
12/2/19 13:49
JLB
P91-0043
o-Xylene
See 8260ML
mg/kg dry
0.0054
0.00057
1
8260D
12/2/19 13:49
JLB
P91-0043
sec-Butylbenzene
0.20
mg/kg dry
0.0054
0.00058
1
8260D
12/2/19 13:49
JLB
P91-0043
Styrene
BRL
mg/kg dry
0.0054
0.00052
1
8260D
12/2/19 13:49
JLB
P91-0043
tert-Butylbenzene
0.013
mg/kg dry
0.0054
0.00064
1
8260D
12/2/19 13:49
JLB
P91-0043
Tetrachloroethylene
BRL
mg/kg dry
0.0054
0.00098
1
8260D
12/2/19 13:49
JLB
P91-0043
Toluene
0.058
mg/kg dry
0.0054
0.00086
1
8260D
1212/19 13:49
JLB
P91-0043
trans-1,2-Dichloroethylene
BRL
mg/kg dry
0.0054
0.0010
1
8260D
12/2/19 13:49
JLB
P91-0043
trans-1,3-Dichloropropylene
BRL
mg/kg dry
0.0054
0.00046
1
8260D
12/2/19 13:49
JLB
P91-0043
Trichloroethylene
BRL
mg/kg dry
0.0054
0.0010
1
8260D
12/2/19 13:49
JLB
P91-0043
Trichlorofluoromethane
BRL
mg/kg dry
0.011
0.0015
1
8260D
12/2/19 13:49
JLB
P91-0043
Vinyl acetate
BRL
mg/kg dry
0.011
0.00059
1
8260D
12/2/19 13:49
JLB
P91-0043
Vinyl chloride
BRL
mg/kg dry
0.011
0.0011
1
8260D
12/2/19 13:49
JLB
P91-0043
Xylenes, total
See 8260ML
mg/kg dry
0.016
0.0019
1
8260D
12/2/19 13:49
JLB
P91-0043
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
98 %
70-130
Dibromofluoromethane
85 %
84-123
Toluene-d8
95 %
76-129
Volatile Organic Compounds by GUMS (Medium Level)
1,2,4-Trimethylbenzene
12000
ug/kg dry
3000
320
500
8260D
12/2/19 15:40
JLB
P91-0044
1,3,5-Trimethylbenzene
3700
ug/kg dry
300
37
50
8260D
12/2/19 15:12
JLB
P91-0044
m,p-Xylenes
5400
ug/kg dry
600
76
50
8260D
12/2/19 15:12
JLB
P91-0044
n-Propylbenzene
2500
ug/kg dry
300
43
50
8260D
1212/19 15:12
JLB
P91-0044
o-Xylene
2600
ug/kg dry
300
32
50
8260D
12/2/19 15:12
JLB
P91-0044
Xylenes, total
7900
ug/kg dry
890
110
50
8260D
12/2/19 15:12
JLB
P91-0044
Surrogate
Recovery
Control Limits
4-Bromofluorobenzene
99 %
70-130
Dibromofluoromethane
93 %
70-130
Toluene-d8
96 %
70-130
Volatile Petroleum Hydrocarbons by GC/PID/FID
C5-C8 Aliphatics
8.0 J
mg/kg dry
17
3.5
100
MADEP VPH 11/27/19 21:14
TBL
P9K0496
C9-C12 Aliphatics
120
mg/kg dry
17
1.5
100
MADEP VPH 11/27/19 21:14
TBL
P9K0496
C9-C10 Aromatics
82
mg/kg dry
17
1.6
100
MADEP VPH 11/27/19 21:14
TBL
P9K0496
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 25 0f 56

/PRISM Full -Service Analytical Environmental Solutions
LABORATORIES INC.
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273 Sample Matrix: Soil
Laboratory Report
12/04/2019
Client Sample ID: SE-5
Prism Sample ID: 9110453-05
Prism Work Order: 9110453
Time Collected: 11/26/19 17:05
Time Submitted: 11/27/19 10:00
Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch
Limit Factor Date/Time ID
Surrogate
Recovery Control Limits
2,5-Dibromotoluene (PID) 92 % 70-130
2,5-Dibromotoluene (FID) 109 % 70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 26 of 56

/r E
P R I IS M Service Analytical
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch MOM - 5035
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9L0043-BLK1)
Prepared &Analyzed: 12/02/19
1,1,1,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,1-Trichloroethane
BRL
0.0050
mg/kg wet
1,1,2,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,2-Trichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethylene
BRL
0.0050
mg/kg wet
1,1-Dichloropropylene
BRL
0.0050
mg/kg wet
1,2,3-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,3-Trichloropropane
BRL
0.0050
mg/kg wet
1,2,4-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,4-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,2-Dibromoethane
BRL
0.0050
mg/kg wet
1,2-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,2-Dichloroethane
BRL
0.0050
mg/kg wet
1,2-Dichloropropane
BRL
0.0050
mg/kg wet
1,3,5-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,3-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,3-Dichloropropane
BRL
0.0050
mg/kg wet
1,4-Dichlorobenzene
BRL
0.0050
mg/kg wet
2,2-Dichloropropane
BRL
0.0050
mg/kg wet
2-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Isopropyltoluene
BRL
0.0050
mg/kg wet
Acetone
BRL
0.020
mg/kg wet
Benzene
BRL
0.0050
mg/kg wet
Bromobenzene
BRL
0.0050
mg/kg wet
Bromochloromethane
BRL
0.0050
mg/kg wet
Bromodichloromethane
BRL
0.0050
mg/kg wet
Bromoform
BRL
0.0050
mg/kg wet
Bromomethane
BRL
0.010
mg/kg wet
Carbon Tetrachloride
BRL
0.0050
mg/kg wet
Chlorobenzene
BRL
0.0050
mg/kg wet
Chloroethane
BRL
0.010
mg/kg wet
Chloroform
BRL
0.0050
mg/kg wet
Chloromethane
BRL
0.010
mg/kg wet
cis-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
cis-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Dibromochloromethane
BRL
0.0050
mg/kg wet
Dichlorodifluoromethane
BRL
0.010
mg/kg wet
Ethylbenzene
BRL
0.0050
mg/kg wet
Isopropyl Ether
BRL
0.0050
mg/kg wet
Isopropylbenzene (Cumene)
BRL
0.0050
mg/kg wet
m,p-Xylenes
BRL
0.010
mg/kg wet
Methyl Butyl Ketone (2-Hexanone)
BRL
0.020
mg/kg wet
Methyl Ethyl Ketone (2-Butanone)
BRL
0.020
mg/kg wet
Methyl Isobutyl Ketone
BRL
0.020
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 27 0f 56

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P911-0043 - 5035
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9L0043-BLK1)
Prepared &Analyzed: 12/02/19
Methylene Chloride
BRL
0.0050
mg/kg wet
Methyl-tert-Butyl Ether
BRL
0.0050
mg/kg wet
Naphthalene
BRL
0.010
mg/kg wet
n-Butylbenzene
BRL
0.0050
mg/kg wet
n-Propylbenzene
BRL
0.0050
mg/kg wet
o-Xylene
BRL
0.0050
mg/kg wet
sec-Butylbenzene
BRL
0.0050
mg/kg wet
Styrene
BRL
0.0050
mg/kg wet
tert-Butyl benzene
BRL
0.0050
mg/kg wet
Tetrachloroethylene
BRL
0.0050
mg/kg wet
Toluene
BRL
0.0050
mg/kg wet
trans- 1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
trans- 1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Trichloroethylene
BRL
0.0050
mg/kg wet
Trichlorofluoromethane
BRL
0.010
mg/kg wet
Vinyl acetate
BRL
0.010
mg/kg wet
Vinyl chloride
BRL
0.010
mg/kg wet
Xylenes, total
BRL
0.015
mg/kg wet
Surrogate:4-Bromofluorobenzene
50.3
ug/L
50.00 101 70-130
Surrogate: Dibromofluoromethane
48.8
ug/L
50.00 98 84-123
Surrogate: Toluene-d8
47.8
ug/L
50.00 96 76-129
LCS (P9L0043-BS1)
Prepared
&Analyzed: 12/02/19
1,1,1,2-Tetrachloroethane
0.0457
0.0050
mg/kg wet
0.05000
91
72-115
1,1,1-Trichloroethane
0.0495
0.0050
mg/kg wet
0.05000
99
67-131
1,1,2,2-Tetrachloroethane
0.0429
0.0050
mg/kg wet
0.05000
86
56-126
1,1,2-Trichloroethane
0.0444
0.0050
mg/kg wet
0.05000
89
70-133
1,1-Dichloroethane
0.0491
0.0050
mg/kg wet
0.05000
98
74-127
1,1-Dichloroethylene
0.0476
0.0050
mg/kg wet
0.05000
95
67-149
1, 1 -Dichloropropylene
0.0508
0.0050
mg/kg wet
0.05000
102
71-130
1,2,3-Trichlorobenzene
0.0428
0.010
mg/kg wet
0.05000
86
68-130
1,2,3-Trichloropropane
0.0432
0.0050
mg/kg wet
0.05000
86
60-137
1,2,4-Trichlorobenzene
0.0428
0.010
mg/kg wet
0.05000
86
66-125
1,2,4-Trimethylbenzene
0.0437
0.0050
mg/kg wet
0.05000
87
69-129
1,2-Dibromoethane
0.0452
0.0050
mg/kg wet
0.05000
90
70-132
1,2-Dichlorobenzene
0.0417
0.0050
mg/kg wet
0.05000
83
72-123
1,2-Dichloroethane
0.0445
0.0050
mg/kg wet
0.05000
89
68-128
1,2-Dichloropropane
0.0489
0.0050
mg/kg wet
0.05000
98
73-130
1,3,5-Trimethylbenzene
0.0437
0.0050
mg/kg wet
0.05000
87
69-128
1,3-Dichlorobenzene
0.0415
0.0050
mg/kg wet
0.05000
83
71-120
1,3-Dichloropropane
0.0457
0.0050
mg/kg wet
0.05000
91
75-124
1,4-Dichlorobenzene
0.0410
0.0050
mg/kg wet
0.05000
82
71-123
2,2-Dichloropropane
0.0518
0.0050
mg/kg wet
0.05000
104
50-142
2-Chlorotoluene
0.0424
0.0050
mg/kg wet
0.05000
85
67-124
4-Chlorotoluene
0.0425
0.0050
mg/kg wet
0.05000
85
71-126
4-Isopropyltoluene
0.0451
0.0050
mg/kg wet
0.05000
90
68-129
Acetone
0.0931
0.020
mg/kg wet
0.1000
93
29-198
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 28 0 56

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P911-0043 - 5035
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P9L0043-BS1)
Prepared &Analyzed: 12/02/19
Benzene
0.0482
0.0050
mg/kg wet
0.05000
96
74-127
Bromobenzene
0.0424
0.0050
mg/kg wet
0.05000
85
73-125
Bromochloromethane
0.0457
0.0050
mg/kg wet
0.05000
91
72-134
Bromodichloromethane
0.0488
0.0050
mg/kg wet
0.05000
98
75-122
Bromoform
0.0486
0.0050
mg/kg wet
0.05000
97
66-135
Bromomethane
0.0439
0.010
mg/kg wet
0.05000
88
20-180
Carbon Tetrachloride
0.0499
0.0050
mg/kg wet
0.05000
100
64-143
Chlorobenzene
0.0440
0.0050
mg/kg wet
0.05000
88
74-118
Chloroethane
0.0486
0.010
mg/kg wet
0.05000
97
33-149
Chloroform
0.0483
0.0050
mg/kg wet
0.05000
97
73-127
Chloromethane
0.0508
0.010
mg/kg wet
0.05000
102
45-143
cis-1,2-Dichloroethylene
0.0463
0.0050
mg/kg wet
0.05000
93
76-134
cis-1,3-Dichloropropylene
0.0519
0.0050
mg/kg wet
0.05000
104
71-125
Dibromochloromethane
0.0456
0.0050
mg/kg wet
0.05000
91
73-122
Dichlorodifluoromethane
0.0390
0.010
mg/kg wet
0.05000
78
26-146
Ethylbenzene
0.0462
0.0050
mg/kg wet
0.05000
92
74-128
Isopropyl Ether
0.0485
0.0050
mg/kg wet
0.05000
97
59-159
Isopropylbenzene (Cumene)
0.0453
0.0050
mg/kg wet
0.05000
91
68-126
m,p-Xylenes
0.0935
0.010
mg/kg wet
0.1000
94
75-124
Methyl Butyl Ketone (2-Hexanone)
0.0491
0.020
mg/kg wet
0.05000
98
61-157
Methyl Ethyl Ketone (2-Butanone)
0.0481
0.020
mg/kg wet
0.05000
96
63-149
Methyl Isobutyl Ketone
0.0507
0.020
mg/kg wet
0.05000
101
57-162
Methylene Chloride
0.0451
0.0050
mg/kg wet
0.05000
90
74-129
Methyl-tert-Butyl Ether
0.0500
0.0050
mg/kg wet
0.05000
100
70-130
Naphthalene
0.0439
0.010
mg/kg wet
0.05000
88
57-157
n-Butylbenzene
0.0453
0.0050
mg/kg wet
0.05000
91
65-135
n-Propylbenzene
0.0439
0.0050
mg/kg wet
0.05000
88
67-130
o-Xylene
0.0460
0.0050
mg/kg wet
0.05000
92
74-126
sec-Butylbenzene
0.0448
0.0050
mg/kg wet
0.05000
90
66-131
Styrene
0.0477
0.0050
mg/kg wet
0.05000
95
77-121
tert-Butyl benzene
0.0447
0.0050
mg/kg wet
0.05000
89
67-132
Tetrachloroethylene
0.0500
0.0050
mg/kg wet
0.05000
100
68-130
Toluene
0.0481
0.0050
mg/kg wet
0.05000
96
71-129
trans- 1,2-Dichloroethylene
0.0470
0.0050
mg/kg wet
0.05000
94
73-132
trans- 1,3-Dichloropropylene
0.0519
0.0050
mg/kg wet
0.05000
104
68-123
Trichloroethylene
0.0474
0.0050
mg/kg wet
0.05000
95
75-133
Trichlorofluoromethane
0.0461
0.010
mg/kg wet
0.05000
92
44-146
Vinyl acetate
0.0558
0.010
mg/kg wet
0.05000
112
85-161
Vinyl chloride
0.0489
0.010
mg/kg wet
0.05000
98
48-147
Xylenes, total
0.139
0.015
mg/kg wet
0.1500
93
74-126
Surrogate:4-Bromofluorobenzene
49.0
ug/L
50.00
98
70-130
Surrogate: Dibromofluoromethane
48.4
ug/L
50.00
97
84-123
Surrogate: Toluene-d8
47.6
ug/L
50.00
95
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 29 0 56

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P911-0043 - 5035
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS Dup (P911-0043-13SD1)
Prepared &Analyzed: 12/02/19
1,1,1,2-Tetrachloroethane
0.0456
0.0050
mg/kg wet
0.05000
91
72-115
0.2
20
1,1,1-Trichloroethane
0.0480
0.0050
mg/kg wet
0.05000
96
67-131
3
20
1,1,2,2-Tetrachloroethane
0.0441
0.0050
mg/kg wet
0.05000
88
56-126
3
20
1,1,2-Trichloroethane
0.0457
0.0050
mg/kg wet
0.05000
91
70-133
3
20
1,1-Dichloroethane
0.0477
0.0050
mg/kg wet
0.05000
95
74-127
3
20
1,1-Dichloroethylene
0.0458
0.0050
mg/kg wet
0.05000
92
67-149
4
20
1, 1 -Dichloropropylene
0.0486
0.0050
mg/kg wet
0.05000
97
71-130
4
20
1,2,3-Trichlorobenzene
0.0432
0.010
mg/kg wet
0.05000
86
68-130
1
20
1,2,3-Trichloropropane
0.0450
0.0050
mg/kg wet
0.05000
90
60-137
4
20
1,2,4-Trichlorobenzene
0.0429
0.010
mg/kg wet
0.05000
86
66-125
0.2
20
1,2,4-Trimethylbenzene
0.0428
0.0050
mg/kg wet
0.05000
86
69-129
2
20
1,2-Dibromoethane
0.0461
0.0050
mg/kg wet
0.05000
92
70-132
2
20
1,2-Dichlorobenzene
0.0414
0.0050
mg/kg wet
0.05000
83
72-123
0.8
20
1,2-Dichloroethane
0.0448
0.0050
mg/kg wet
0.05000
90
68-128
0.6
20
1,2-Dichloropropane
0.0486
0.0050
mg/kg wet
0.05000
97
73-130
0.7
20
1,3,5-Trimethylbenzene
0.0426
0.0050
mg/kg wet
0.05000
85
69-128
3
20
1,3-Dichlorobenzene
0.0409
0.0050
mg/kg wet
0.05000
82
71-120
1
20
1,3-Dichloropropane
0.0469
0.0050
mg/kg wet
0.05000
94
75-124
3
20
1,4-Dichlorobenzene
0.0406
0.0050
mg/kg wet
0.05000
81
71-123
1
20
2,2-Dichloropropane
0.0491
0.0050
mg/kg wet
0.05000
98
50-142
5
20
2-Chlorotoluene
0.0413
0.0050
mg/kg wet
0.05000
83
67-124
3
20
4-Chlorotoluene
0.0415
0.0050
mg/kg wet
0.05000
83
71-126
2
20
4-Isopropyltoluene
0.0437
0.0050
mg/kg wet
0.05000
87
68-129
3
20
Acetone
0.0975
0.020
mg/kg wet
0.1000
97
29-198
5
20
Benzene
0.0467
0.0050
mg/kg wet
0.05000
93
74-127
3
20
Bromobenzene
0.0420
0.0050
mg/kg wet
0.05000
84
73-125
1
20
Bromochloromethane
0.0471
0.0050
mg/kg wet
0.05000
94
72-134
3
20
Bromodichloromethane
0.0485
0.0050
mg/kg wet
0.05000
97
75-122
0.7
20
Bromoform
0.0504
0.0050
mg/kg wet
0.05000
101
66-135
4
20
Bromomethane
0.0463
0.010
mg/kg wet
0.05000
93
20-180
5
20
Carbon Tetrachloride
0.0473
0.0050
mg/kg wet
0.05000
95
64-143
5
20
Chlorobenzene
0.0431
0.0050
mg/kg wet
0.05000
86
74-118
2
20
Chloroethane
0.0466
0.010
mg/kg wet
0.05000
93
33-149
4
20
Chloroform
0.0473
0.0050
mg/kg wet
0.05000
95
73-127
2
20
Chloromethane
0.0381
0.010
mg/kg wet
0.05000
76
45-143
29
20 D
cis-1,2-Dichloroethylene
0.0461
0.0050
mg/kg wet
0.05000
92
76-134
0.4
20
cis-1,3-Dichloropropylene
0.0514
0.0050
mg/kg wet
0.05000
103
71-125
1
20
Dibromochloromethane
0.0467
0.0050
mg/kg wet
0.05000
93
73-122
2
20
Dichlorodifluoromethane
0.0374
0.010
mg/kg wet
0.05000
75
26-146
4
20
Ethylbenzene
0.0450
0.0050
mg/kg wet
0.05000
90
74-128
3
20
Isopropyl Ether
0.0480
0.0050
mg/kg wet
0.05000
96
59-159
0.9
20
Isopropylbenzene (Cumene)
0.0441
0.0050
mg/kg wet
0.05000
88
68-126
3
20
m,p-Xylenes
0.0911
0.010
mg/kg wet
0.1000
91
75-124
3
20
Methyl Butyl Ketone (2-Hexanone)
0.0526
0.020
mg/kg wet
0.05000
105
61-157
7
20
Methyl Ethyl Ketone (2-Butanone)
0.0506
0.020
mg/kg wet
0.05000
101
63-149
5
20
Methyl Isobutyl Ketone
0.0539
0.020
mg/kg wet
0.05000
108
57-162
6
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 30 0 56

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9L0043 - 5035
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS Dup (1391-0043-BS131)
Prepared &Analyzed: 12/02/19
Methylene Chloride
0.0444
0.0050
mg/kg wet
0.05000
89
74-129
2
20
Methyl-tert-Butyl Ether
0.0510
0.0050
mg/kg wet
0.05000
102
70-130
2
20
Naphthalene
0.0459
0.010
mg/kg wet
0.05000
92
57-157
4
20
n-Butylbenzene
0.0438
0.0050
mg/kg wet
0.05000
88
65-135
3
20
n-Propylbenzene
0.0422
0.0050
mg/kg wet
0.05000
84
67-130
4
20
o-Xylene
0.0453
0.0050
mg/kg wet
0.05000
91
74-126
1
20
sec-Butylbenzene
0.0435
0.0050
mg/kg wet
0.05000
87
66-131
3
20
Styrene
0.0474
0.0050
mg/kg wet
0.05000
95
77-121
0.8
20
tert-Butylbenzene
0.0435
0.0050
mg/kg wet
0.05000
87
67-132
3
20
Tetrachloroethylene
0.0486
0.0050
mg/kg wet
0.05000
97
68-130
3
20
Toluene
0.0469
0.0050
mg/kg wet
0.05000
94
71-129
3
20
trans-1,2-Dichloroethylene
0.0457
0.0050
mg/kg wet
0.05000
91
73-132
3
20
trans- 1,3-Dichloropropylene
0.0519
0.0050
mg/kg wet
0.05000
104
68-123
0.06
20
Trichloroethylene
0.0458
0.0050
mg/kg wet
0.05000
92
75-133
3
20
Trichlorofluoromethane
0.0441
0.010
mg/kg wet
0.05000
88
44-146
4
20
Vinyl acetate
0.0560
0.010
mg/kg wet
0.05000
112
85-161
0.4
20
Vinyl chloride
0.0465
0.010
mg/kg wet
0.05000
93
48-147
5
20
Xylenes, total
0.136
0.015
mg/kg wet
0.1500
91
74-126
2
20
Surrogate:4-Bromofluorobenzene
49.2
ug/L
50.00
98
70-130
Surrogate: Dibromofluoromethane
47.9
ug/L
50.00
96
84-123
Surrogate: Toluene-d8
48.0
ug/L
50.00
96
76-129
Batch P9L0050 - 5035
Blank (11391_0050-BLK1)
Prepared & Analyzed: 12/03/19
1,1,1,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,1-Trichloroethane
BRL
0.0050
mg/kg wet
1,1,2,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,2-Trichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethylene
BRL
0.0050
mg/kg wet
1,1-Dichloropropylene
BRL
0.0050
mg/kg wet
1,2,3-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,3-Trichloropropane
BRL
0.0050
mg/kg wet
1,2,4-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,4-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,2-Dibromoethane
BRL
0.0050
mg/kg wet
1,2-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,2-Dichloroethane
BRL
0.0050
mg/kg wet
1,2-Dichloropropane
BRL
0.0050
mg/kg wet
1,3,5-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,3-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,3-Dichloropropane
BRL
0.0050
mg/kg wet
1,4-Dichlorobenzene
BRL
0.0050
mg/kg wet
2,2-Dichloropropane
BRL
0.0050
mg/kg wet
2-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Chlorotoluene
BRL
0.0050
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 31 0f 56

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9L0050 - 5035
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (11291_0050-BLK1)
Prepared & Analyzed: 12/03/19
4-Isopropyltoluene
BRL
0.0050
mg/kg wet
Acetone
BRL
0.020
mg/kg wet
Benzene
BRL
0.0050
mg/kg wet
Bromobenzene
BRL
0.0050
mg/kg wet
Bromochloromethane
BRL
0.0050
mg/kg wet
Bromodichloromethane
BRL
0.0050
mg/kg wet
Bromoform
BRL
0.0050
mg/kg wet
Bromomethane
BRL
0.010
mg/kg wet
Carbon Tetrachloride
BRL
0.0050
mg/kg wet
Chlorobenzene
BRL
0.0050
mg/kg wet
Chloroethane
BRL
0.010
mg/kg wet
Chloroform
BRL
0.0050
mg/kg wet
Chloromethane
BRL
0.010
mg/kg wet
cis-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
cis-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Dibromochloromethane
BRL
0.0050
mg/kg wet
Dichlorodifluoromethane
BRL
0.010
mg/kg wet
Ethylbenzene
BRL
0.0050
mg/kg wet
Isopropyl Ether
BRL
0.0050
mg/kg wet
Isopropylbenzene (Cumene)
BRL
0.0050
mg/kg wet
m,p-Xylenes
BRL
0.010
mg/kg wet
Methyl Butyl Ketone (2-Hexanone)
BRL
0.020
mg/kg wet
Methyl Ethyl Ketone (2-Butanone)
BRL
0.020
mg/kg wet
Methyl Isobutyl Ketone
BRL
0.020
mg/kg wet
Methylene Chloride
BRL
0.0050
mg/kg wet
Methyl-tert-Butyl Ether
BRL
0.0050
mg/kg wet
Naphthalene
BRL
0.010
mg/kg wet
n-Butylbenzene
BRL
0.0050
mg/kg wet
n-Propylbenzene
BRL
0.0050
mg/kg wet
o-Xylene
BRL
0.0050
mg/kg wet
sec-Butylbenzene
BRL
0.0050
mg/kg wet
Styrene
BRL
0.0050
mg/kg wet
tert-Butylbenzene
BRL
0.0050
mg/kg wet
Tetrachloroethylene
BRL
0.0050
mg/kg wet
Toluene
BRL
0.0050
mg/kg wet
trans-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
trans-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Trichloroethylene
BRL
0.0050
mg/kg wet
Trichlorofluoromethane
BRL
0.010
mg/kg wet
Vinyl acetate
BRL
0.010
mg/kg wet
Vinyl chloride
BRL
0.010
mg/kg wet
Xylenes, total
BRL
0.015
mg/kg wet
Surrogate:4-Bromofluorobenzene
51.2
ug/L
50.00 102 70-130
Surrogate: Dibromofluoromethane
48.8
ug/L
50.00 98 84-123
Surrogate: Toluene-d8
47.1
ug/L
50.00 94 76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 32 0f 56

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P911-0050 - 5035
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P9L0050-BS1)
Prepared &Analyzed: 12/03/19
1,1,1,2-Tetrachloroethane
0.0478
0.0050
mg/kg wet
0.05000
96
72-115
1,1,1-Trichloroethane
0.0518
0.0050
mg/kg wet
0.05000
104
67-131
1,1,2,2-Tetrachloroethane
0.0422
0.0050
mg/kg wet
0.05000
84
56-126
1,1,2-Trichloroethane
0.0461
0.0050
mg/kg wet
0.05000
92
70-133
1,1-Dichloroethane
0.0500
0.0050
mg/kg wet
0.05000
100
74-127
1,1-Dichloroethylene
0.0487
0.0050
mg/kg wet
0.05000
97
67-149
1, 1 -Dichloropropylene
0.0532
0.0050
mg/kg wet
0.05000
106
71-130
1,2,3-Trichlorobenzene
0.0458
0.010
mg/kg wet
0.05000
92
68-130
1,2,3-Trichloropropane
0.0433
0.0050
mg/kg wet
0.05000
87
60-137
1,2,4-Trichlorobenzene
0.0478
0.010
mg/kg wet
0.05000
96
66-125
1,2,4-Trimethylbenzene
0.0467
0.0050
mg/kg wet
0.05000
93
69-129
1,2-Dibromoethane
0.0470
0.0050
mg/kg wet
0.05000
94
70-132
1,2-Dichlorobenzene
0.0443
0.0050
mg/kg wet
0.05000
89
72-123
1,2-Dichloroethane
0.0446
0.0050
mg/kg wet
0.05000
89
68-128
1,2-Dichloropropane
0.0496
0.0050
mg/kg wet
0.05000
99
73-130
1,3,5-Trimethylbenzene
0.0468
0.0050
mg/kg wet
0.05000
94
69-128
1,3-Dichlorobenzene
0.0450
0.0050
mg/kg wet
0.05000
90
71-120
1,3-Dichloropropane
0.0472
0.0050
mg/kg wet
0.05000
94
75-124
1,4-Dichlorobenzene
0.0442
0.0050
mg/kg wet
0.05000
88
71-123
2,2-Dichloropropane
0.0526
0.0050
mg/kg wet
0.05000
105
50-142
2-Chlorotoluene
0.0448
0.0050
mg/kg wet
0.05000
90
67-124
4-Chlorotoluene
0.0449
0.0050
mg/kg wet
0.05000
90
71-126
4-Isopropyltoluene
0.0486
0.0050
mg/kg wet
0.05000
97
68-129
Acetone
0.0873
0.020
mg/kg wet
0.1000
87
29-198
Benzene
0.0493
0.0050
mg/kg wet
0.05000
99
74-127
Bromobenzene
0.0439
0.0050
mg/kg wet
0.05000
88
73-125
Bromochloromethane
0.0491
0.0050
mg/kg wet
0.05000
98
72-134
Bromodichloromethane
0.0496
0.0050
mg/kg wet
0.05000
99
75-122
Bromoform
0.0509
0.0050
mg/kg wet
0.05000
102
66-135
Bromomethane
0.0440
0.010
mg/kg wet
0.05000
88
20-180
Carbon Tetrachloride
0.0529
0.0050
mg/kg wet
0.05000
106
64-143
Chlorobenzene
0.0465
0.0050
mg/kg wet
0.05000
93
74-118
Chloroethane
0.0483
0.010
mg/kg wet
0.05000
97
33-149
Chloroform
0.0500
0.0050
mg/kg wet
0.05000
100
73-127
Chloromethane
0.0489
0.010
mg/kg wet
0.05000
98
45-143
cis-1,2-Dichloroethylene
0.0475
0.0050
mg/kg wet
0.05000
95
76-134
cis-1,3-Dichloropropylene
0.0530
0.0050
mg/kg wet
0.05000
106
71-125
Dibromochloromethane
0.0478
0.0050
mg/kg wet
0.05000
96
73-122
Dichlorodifluoromethane
0.0371
0.010
mg/kg wet
0.05000
74
26-146
Ethylbenzene
0.0491
0.0050
mg/kg wet
0.05000
98
74-128
Isopropyl Ether
0.0482
0.0050
mg/kg wet
0.05000
96
59-159
Isopropylbenzene (Cumene)
0.0484
0.0050
mg/kg wet
0.05000
97
68-126
m,p-Xylenes
0.0998
0.010
mg/kg wet
0.1000
100
75-124
Methyl Butyl Ketone (2-Hexanone)
0.0468
0.020
mg/kg wet
0.05000
94
61-157
Methyl Ethyl Ketone (2-Butanone)
0.0446
0.020
mg/kg wet
0.05000
89
63-149
Methyl Isobutyl Ketone
0.0482
0.020
mg/kg wet
0.05000
96
57-162
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 33 0 56

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P911-0050 - 5035
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P911-0050-BS1)
Prepared &Analyzed: 12/03/19
Methylene Chloride
0.0441
0.0050
mg/kg wet
0.05000
88
74-129
Methyl-tert-Butyl Ether
0.0510
0.0050
mg/kg wet
0.05000
102
70-130
Naphthalene
0.0466
0.010
mg/kg wet
0.05000
93
57-157
n-Butylbenzene
0.0484
0.0050
mg/kg wet
0.05000
97
65-135
n-Propylbenzene
0.0461
0.0050
mg/kg wet
0.05000
92
67-130
o-Xylene
0.0493
0.0050
mg/kg wet
0.05000
99
74-126
sec-Butylbenzene
0.0483
0.0050
mg/kg wet
0.05000
97
66-131
Styrene
0.0514
0.0050
mg/kg wet
0.05000
103
77-121
tert-Butyl benzene
0.0482
0.0050
mg/kg wet
0.05000
96
67-132
Tetrachloroethylene
0.0542
0.0050
mg/kg wet
0.05000
108
68-130
Toluene
0.0505
0.0050
mg/kg wet
0.05000
101
71-129
trans- 1,2-Dichloroethylene
0.0486
0.0050
mg/kg wet
0.05000
97
73-132
trans- 1,3-Dichloropropylene
0.0522
0.0050
mg/kg wet
0.05000
104
68-123
Trichloroethylene
0.0507
0.0050
mg/kg wet
0.05000
101
75-133
Trichlorofluoromethane
0.0468
0.010
mg/kg wet
0.05000
94
44-146
Vinyl acetate
0.0534
0.010
mg/kg wet
0.05000
107
85-161
Vinyl chloride
0.0480
0.010
mg/kg wet
0.05000
96
48-147
Xylenes, total
0.149
0.015
mg/kg wet
0.1500
99
74-126
Surrogate:4-Bromofluorobenzene
49.7
ug/L
50.00
99
70-130
Surrogate: Dibromofluoromethane
47.0
ug/L
50.00
94
84-123
Surrogate: Toluene-d8
47.3
ug/L
50.00
95
76-129
LCS Dup (P9L0050-BSD1)
Prepared &Analyzed: 12/03/19
1,1,1,2-Tetrachloroethane
0.0491
0.0050
mg/kg wet
0.05000
98
72-115
3
20
1,1,1-Trichloroethane
0.0518
0.0050
mg/kg wet
0.05000
104
67-131
0.1
20
1,1,2,2-Tetrachloroethane
0.0431
0.0050
mg/kg wet
0.05000
86
56-126
2
20
1,1,2-Trichloroethane
0.0472
0.0050
mg/kg wet
0.05000
94
70-133
2
20
1,1-Dichloroethane
0.0502
0.0050
mg/kg wet
0.05000
100
74-127
0.4
20
1,1-Dichloroethylene
0.0486
0.0050
mg/kg wet
0.05000
97
67-149
0.08
20
1, 1 -Dichloropropylene
0.0525
0.0050
mg/kg wet
0.05000
105
71-130
1
20
1,2,3-Trichlorobenzene
0.0470
0.010
mg/kg wet
0.05000
94
68-130
3
20
1,2,3-Trichloropropane
0.0436
0.0050
mg/kg wet
0.05000
87
60-137
0.6
20
1,2,4-Trichlorobenzene
0.0480
0.010
mg/kg wet
0.05000
96
66-125
0.5
20
1,2,4-Trimethylbenzene
0.0469
0.0050
mg/kg wet
0.05000
94
69-129
0.4
20
1,2-Dibromoethane
0.0477
0.0050
mg/kg wet
0.05000
95
70-132
1
20
1,2-Dichlorobenzene
0.0453
0.0050
mg/kg wet
0.05000
91
72-123
2
20
1,2-Dichloroethane
0.0463
0.0050
mg/kg wet
0.05000
93
68-128
4
20
1,2-Dichloropropane
0.0508
0.0050
mg/kg wet
0.05000
102
73-130
2
20
1,3,5-Trimethylbenzene
0.0466
0.0050
mg/kg wet
0.05000
93
69-128
0.3
20
1,3-Dichlorobenzene
0.0454
0.0050
mg/kg wet
0.05000
91
71-120
0.9
20
1,3-Dichloropropane
0.0481
0.0050
mg/kg wet
0.05000
96
75-124
2
20
1,4-Dichlorobenzene
0.0447
0.0050
mg/kg wet
0.05000
89
71-123
1
20
2,2-Dichloropropane
0.0534
0.0050
mg/kg wet
0.05000
107
50-142
2
20
2-Chlorotoluene
0.0452
0.0050
mg/kg wet
0.05000
90
67-124
0.8
20
4-Chlorotoluene
0.0448
0.0050
mg/kg wet
0.05000
90
71-126
0.1
20
4-Isopropyltoluene
0.0484
0.0050
mg/kg wet
0.05000
97
68-129
0.5
20
Acetone
0.0839
0.020
mg/kg wet
0.1000
84
29-198
4
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 34 0 56

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P911-0050 - 5035
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS Dup (13911-0050-13SD1)
Prepared &Analyzed: 12/03/19
Benzene
0.0497
0.0050
mg/kg wet
0.05000
99
74-127
0.8
20
Bromobenzene
0.0446
0.0050
mg/kg wet
0.05000
89
73-125
2
20
Bromochloromethane
0.0505
0.0050
mg/kg wet
0.05000
101
72-134
3
20
Bromodichloromethane
0.0507
0.0050
mg/kg wet
0.05000
101
75-122
2
20
Bromoform
0.0518
0.0050
mg/kg wet
0.05000
104
66-135
2
20
Bromomethane
0.0453
0.010
mg/kg wet
0.05000
91
20-180
3
20
Carbon Tetrachloride
0.0516
0.0050
mg/kg wet
0.05000
103
64-143
3
20
Chlorobenzene
0.0471
0.0050
mg/kg wet
0.05000
94
74-118
1
20
Chloroethane
0.0476
0.010
mg/kg wet
0.05000
95
33-149
1
20
Chloroform
0.0506
0.0050
mg/kg wet
0.05000
101
73-127
1
20
Chloromethane
0.0477
0.010
mg/kg wet
0.05000
95
45-143
3
20
cis-1,2-Dichloroethylene
0.0485
0.0050
mg/kg wet
0.05000
97
76-134
2
20
cis-1,3-Dichloropropylene
0.0546
0.0050
mg/kg wet
0.05000
109
71-125
3
20
Dibromochloromethane
0.0495
0.0050
mg/kg wet
0.05000
99
73-122
3
20
Dichlorodifluoromethane
0.0370
0.010
mg/kg wet
0.05000
74
26-146
0.4
20
Ethylbenzene
0.0491
0.0050
mg/kg wet
0.05000
98
74-128
0.08
20
Isopropyl Ether
0.0495
0.0050
mg/kg wet
0.05000
99
59-159
3
20
Isopropylbenzene (Cumene)
0.0482
0.0050
mg/kg wet
0.05000
96
68-126
0.4
20
m,p-Xylenes
0.0989
0.010
mg/kg wet
0.1000
99
75-124
0.9
20
Methyl Butyl Ketone (2-Hexanone)
0.0464
0.020
mg/kg wet
0.05000
93
61-157
0.7
20
Methyl Ethyl Ketone (2-Butanone)
0.0430
0.020
mg/kg wet
0.05000
86
63-149
4
20
Methyl Isobutyl Ketone
0.0483
0.020
mg/kg wet
0.05000
97
57-162
0.06
20
Methylene Chloride
0.0452
0.0050
mg/kg wet
0.05000
90
74-129
2
20
Methyl-tert-Butyl Ether
0.0529
0.0050
mg/kg wet
0.05000
106
70-130
4
20
Naphthalene
0.0470
0.010
mg/kg wet
0.05000
94
57-157
0.7
20
n-Butylbenzene
0.0475
0.0050
mg/kg wet
0.05000
95
65-135
2
20
n-Propylbenzene
0.0457
0.0050
mg/kg wet
0.05000
91
67-130
0.8
20
o-Xylene
0.0495
0.0050
mg/kg wet
0.05000
99
74-126
0.4
20
sec-Butylbenzene
0.0475
0.0050
mg/kg wet
0.05000
95
66-131
2
20
Styrene
0.0518
0.0050
mg/kg wet
0.05000
104
77-121
0.6
20
tert-Butyl benzene
0.0480
0.0050
mg/kg wet
0.05000
96
67-132
0.3
20
Tetrachloroethylene
0.0540
0.0050
mg/kg wet
0.05000
108
68-130
0.4
20
Toluene
0.0508
0.0050
mg/kg wet
0.05000
102
71-129
0.6
20
trans- 1,2-Dichloroethylene
0.0483
0.0050
mg/kg wet
0.05000
97
73-132
0.7
20
trans- 1,3-Dichloropropylene
0.0543
0.0050
mg/kg wet
0.05000
109
68-123
4
20
Trichloroethylene
0.0504
0.0050
mg/kg wet
0.05000
101
75-133
0.6
20
Trichlorofluoromethane
0.0459
0.010
mg/kg wet
0.05000
92
44-146
2
20
Vinyl acetate
0.0555
0.010
mg/kg wet
0.05000
ill
85-161
4
20
Vinyl chloride
0.0467
0.010
mg/kg wet
0.05000
93
48-147
3
20
Xylenes, total
0.148
0.015
mg/kg wet
0.1500
99
74-126
0.5
20
Surrogate:4-Bromofluorobenzene
50.0
ug/L
50.00
100
70-130
Surrogate: Dibromofluoromethane
47.8
ug/L
50.00
96
84-123
Surrogate: Toluene-d8
46.9
ug/L
50.00
94
76-129
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 35 0 56

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control
Analyte
Batch P9L0044 - 5035
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9L0044-BLK1)
Prepared & Analyzed: 12/02/19
1,1,1,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,1-Trichloroethane
BRL
0.0050
mg/kg wet
1,1,2,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,2-Trichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethylene
BRL
0.0050
mg/kg wet
1,1-Dichloropropylene
BRL
0.0050
mg/kg wet
1,2,3-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,3-Trichloropropane
BRL
0.0050
mg/kg wet
1,2,4-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,4-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,2,4-Trimethyl benzene
BRL
5.0
ug/kg wet
1,2-Dibromoethane
BRL
0.0050
mg/kg wet
1,2-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,2-Dichloroethane
BRL
0.0050
mg/kg wet
1,2-Dichloropropane
BRL
0.0050
mg/kg wet
1,3,5-Trimethyl benzene
BRL
5.0
ug/kg wet
1,3,5-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,3-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,3-Dichloropropane
BRL
0.0050
mg/kg wet
1,4-Dichlorobenzene
BRL
0.0050
mg/kg wet
2,2-Dichloropropane
BRL
0.0050
mg/kg wet
2-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Isopropyltoluene
BRL
0.0050
mg/kg wet
Acetone
BRL
0.020
mg/kg wet
Benzene
BRL
0.0050
mg/kg wet
Bromobenzene
BRL
0.0050
mg/kg wet
Bromochloromethane
BRL
0.0050
mg/kg wet
Bromodichloromethane
BRL
0.0050
mg/kg wet
Bromoform
BRL
0.0050
mg/kg wet
Bromomethane
BRL
0.010
mg/kg wet
Carbon Tetrachloride
BRL
0.0050
mg/kg wet
Chlorobenzene
BRL
0.0050
mg/kg wet
Chloroethane
BRL
0.010
mg/kg wet
Chloroform
BRL
0.0050
mg/kg wet
Chloromethane
BRL
0.010
mg/kg wet
cis-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
cis-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Dibromochloromethane
BRL
0.0050
mg/kg wet
Dichlorodifluoromethane
BRL
0.010
mg/kg wet
Ethylbenzene
BRL
0.0050
mg/kg wet
Ethylbenzene
BRL
5.0
ug/kg wet
Isopropyl Ether
BRL
0.0050
mg/kg wet
Isopropylbenzene (Cumene)
BRL
0.0050
mg/kg wet
m,p-Xylenes
BRL
0.010
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 36 0f 56

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control
Analyte
Batch P9L0044 - 5035
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9L0044-BLK1)
Prepared &Analyzed: 12/02/19
m,p-Xylenes
BRL
10
ug/kg wet
Methyl Butyl Ketone (2-Hexanone)
BRL
0.020
mg/kg wet
Methyl Ethyl Ketone (2-Butanone)
BRL
0.020
mg/kg wet
Methyl Isobutyl Ketone
BRL
0.020
mg/kg wet
Methylene Chloride
BRL
0.0050
mg/kg wet
Methyl-tert-Butyl Ether
BRL
0.0050
mg/kg wet
Naphthalene
BRL
0.010
mg/kg wet
n-Butylbenzene
BRL
0.0050
mg/kg wet
n-Propylbenzene
BRL
0.0050
mg/kg wet
n-Propylbenzene
BRL
5.0
ug/kg wet
o-Xylene
BRL
0.0050
mg/kg wet
o-Xylene
BRL
5.0
ug/kg wet
sec-Butylbenzene
BRL
0.0050
mg/kg wet
Styrene
BRL
0.0050
mg/kg wet
tert-Butylbenzene
BRL
0.0050
mg/kg wet
Tetrachloroethylene
BRL
0.0050
mg/kg wet
Toluene
BRL
0.0050
mg/kg wet
Toluene
BRL
5.0
ug/kg wet
trans-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
trans-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Trichloroethylene
BRL
0.0050
mg/kg wet
Trichlorofluoromethane
BRL
0.010
mg/kg wet
Vinyl acetate
BRL
0.010
mg/kg wet
Vinyl chloride
BRL
0.010
mg/kg wet
Xylenes, total
BRL
15
ug/kg wet
Xylenes, total
BRL
0.015
mg/kg wet
Surrogate:4-Bromofluorobenzene
50.3
ug/L
50.00
101 70-130
Surrogate:4-Bromofluorobenzene
50.3
ug/L
50.00
101 70-130
Surrogate: Dibromofluoromethane
48.8
ug/L
50.00
98 70-130
Surrogate: Dibromofluoromethane
48.8
ug/L
50.00
98 70-130
Surrogate: Toluene-d8
47.8
ug/L
50.00
96 70-130
Surrogate: Toluene-d8
47.8
ug/L
50.00
96 70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 37 of 56

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control
Analyte
Batch P911-0044 - 5035
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P9L0044-BS1)
Prepared &Analyzed: 12/02/19
1,1,1,2-Tetrachloroethane
0.0457
0.0050
mg/kg wet
0.05000
91
72-115
1,1,1-Trichloroethane
0.0495
0.0050
mg/kg wet
0.05000
99
72-123
1,1,2,2-Tetrachloroethane
0.0429
0.0050
mg/kg wet
0.05000
86
62-127
1,1,2-Trichloroethane
0.0444
0.0050
mg/kg wet
0.05000
89
73-123
1,1-Dichloroethane
0.0491
0.0050
mg/kg wet
0.05000
98
73-119
1,1-Dichloroethylene
0.0476
0.0050
mg/kg wet
0.05000
95
59-157
1, 1 -Dichloropropylene
0.0508
0.0050
mg/kg wet
0.05000
102
70-129
1,2,3-Trichlorobenzene
0.0428
0.010
mg/kg wet
0.05000
86
59-133
1,2,3-Trichloropropane
0.0432
0.0050
mg/kg wet
0.05000
86
52-137
1,2,4-Trichlorobenzene
0.0428
0.010
mg/kg wet
0.05000
86
66-123
1,2,4-Trimethylbenzene
0.0437
0.0050
mg/kg wet
0.05000
87
69-126
1,2,4-Trimethylbenzene
43.7
5.0
ug/kg wet
50.00
87
69-126
1,2-Dibromoethane
0.0452
0.0050
mg/kg wet
0.05000
90
69-127
1,2-Dichlorobenzene
0.0417
0.0050
mg/kg wet
0.05000
83
70-121
1,2-Dichloroethane
0.0445
0.0050
mg/kg wet
0.05000
89
69-125
1,2-Dichloropropane
0.0489
0.0050
mg/kg wet
0.05000
98
75-124
1,3,5-Trimethylbenzene
0.0437
0.0050
mg/kg wet
0.05000
87
69-124
1,3,5-Trimethylbenzene
43.7
5.0
ug/kg wet
50.00
87
69-124
1,3-Dichlorobenzene
0.0415
0.0050
mg/kg wet
0.05000
83
70-121
1,3-Dichloropropane
0.0457
0.0050
mg/kg wet
0.05000
91
70-124
1,4-Dichlorobenzene
0.0410
0.0050
mg/kg wet
0.05000
82
71-119
2,2-Dichloropropane
0.0518
0.0050
mg/kg wet
0.05000
104
46-154
2-Chlorotoluene
0.0424
0.0050
mg/kg wet
0.05000
85
70-121
4-Chlorotoluene
0.0425
0.0050
mg/kg wet
0.05000
85
72-126
4-Isopropyltoluene
0.0451
0.0050
mg/kg wet
0.05000
90
71-126
Acetone
0.0931
0.020
mg/kg wet
0.1000
93
12-196
Benzene
0.0482
0.0050
mg/kg wet
0.05000
96
74-123
Bromobenzene
0.0424
0.0050
mg/kg wet
0.05000
85
66-122
Bromochloromethane
0.0457
0.0050
mg/kg wet
0.05000
91
73-128
Bromodichloromethane
0.0488
0.0050
mg/kg wet
0.05000
98
76-123
Bromoform
0.0486
0.0050
mg/kg wet
0.05000
97
71-124
Bromomethane
0.0439
0.010
mg/kg wet
0.05000
88
56-145
Carbon Tetrachloride
0.0499
0.0050
mg/kg wet
0.05000
100
67-140
Chlorobenzene
0.0440
0.0050
mg/kg wet
0.05000
88
74-121
Chloroethane
0.0486
0.010
mg/kg wet
0.05000
97
64-142
Chloroform
0.0483
0.0050
mg/kg wet
0.05000
97
75-125
Chloromethane
0.0508
0.010
mg/kg wet
0.05000
102
54-132
cis-1,2-Dichloroethylene
0.0463
0.0050
mg/kg wet
0.05000
93
68-132
cis-1,3-Dichloropropylene
0.0519
0.0050
mg/kg wet
0.05000
104
75-128
Dibromochloromethane
0.0456
0.0050
mg/kg wet
0.05000
91
71-121
Dichlorodifluoromethane
0.0390
0.010
mg/kg wet
0.05000
78
39-178
Ethylbenzene
46.2
5.0
ug/kg wet
50.00
92
69-125
Ethylbenzene
0.0462
0.0050
mg/kg wet
0.05000
92
69-125
Isopropyl Ether
0.0485
0.0050
mg/kg wet
0.05000
97
77-123
Isopropylbenzene (Cumene)
0.0453
0.0050
mg/kg wet
0.05000
91
68-129
m,p-Xylenes
93.5
10
ug/kg wet
100.0
94
64-125
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 38 0 56

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property Prism Work Order: 9110453
Attn: Al Quarles Time Submitted: 11/27/2019 10:00:OOAM
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P911-0044 - 5035
LCS (P91-0044-BS1)
Prepared &Analyzed: 12/02/19
m,p-Xylenes
0.0935
0.010
mg/kg wet
0.1000
94
64-125
Methyl Butyl Ketone (2-Hexanone)
0.0491
0.020
mg/kg wet
0.05000
98
54-139
Methyl Ethyl Ketone (2-Butanone)
0.0481
0.020
mg/kg wet
0.05000
96
34-165
Methyl Isobutyl Ketone
0.0507
0.020
mg/kg wet
0.05000
101
63-130
Methylene Chloride
0.0451
0.0050
mg/kg wet
0.05000
90
65-135
Methyl-tert-Butyl Ether
0.0500
0.0050
mg/kg wet
0.05000
100
62-123
Naphthalene
0.0439
0.010
mg/kg wet
0.05000
88
58-129
n-Butylbenzene
0.0453
0.0050
mg/kg wet
0.05000
91
71-126
n-Propylbenzene
43.9
5.0
ug/kg wet
50.00
88
68-128
n-Propylbenzene
0.0439
0.0050
mg/kg wet
0.05000
88
68-128
o-Xylene
46.0
5.0
ug/kg wet
50.00
92
69-121
o-Xylene
0.0460
0.0050
mg/kg wet
0.05000
92
69-121
sec-Butylbenzene
0.0448
0.0050
mg/kg wet
0.05000
90
71-128
Styrene
0.0477
0.0050
mg/kg wet
0.05000
95
67-129
tert-Butyl benzene
0.0447
0.0050
mg/kg wet
0.05000
89
71-126
Tetrachloroethylene
0.0500
0.0050
mg/kg wet
0.05000
100
71-124
Toluene
0.0481
0.0050
mg/kg wet
0.05000
96
74-122
Toluene
48.1
5.0
ug/kg wet
50.00
96
74-122
trans- 1,2-Dichloroethylene
0.0470
0.0050
mg/kg wet
0.05000
94
69-129
trans- 1,3-Dichloropropylene
0.0519
0.0050
mg/kg wet
0.05000
104
74-127
Trichloroethylene
0.0474
0.0050
mg/kg wet
0.05000
95
68-133
Trichlorofluoromethane
0.0461
0.010
mg/kg wet
0.05000
92
60-138
Vinyl acetate
0.0558
0.010
mg/kg wet
0.05000
112
14-179
Vinyl chloride
0.0489
0.010
mg/kg wet
0.05000
98
69-135
Xylenes, total
139
15
ug/kg wet
150.0
93
74-126
Xylenes, total
0.139
0.015
mg/kg wet
0.1500
93
74-126
Surrogate:4-Bromofluorobenzene
49.0
ug/L
50.00
98
70-130
Surrogate:4-Bromofluorobenzene
49.0
ug/L
50.00
98
70-130
Surrogate: Dibromofluoromethane
48.4
ug/L
50.00
97
70-130
Surrogate: Dibromofluoromethane
48.4
ug/L
50.00
97
70-130
Surrogate: Toluene-d8
47.6
ug/L
50.00
95
70-130
Surrogate: Toluene-d8
47.6
ug/L
50.00
95
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 39 0 56

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control
Analyte
Batch P911-0044 - 5035
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS Dup (P91-0044-13SD1)
Prepared &Analyzed: 12/02/19
1,1,1,2-Tetrachloroethane
0.0456
0.0050
mg/kg wet
0.05000
91
72-115
0.2
20
1,1,1-Trichloroethane
0.0480
0.0050
mg/kg wet
0.05000
96
72-123
3
20
1,1,2,2-Tetrachloroethane
0.0441
0.0050
mg/kg wet
0.05000
88
62-127
3
20
1,1,2-Trichloroethane
0.0457
0.0050
mg/kg wet
0.05000
91
73-123
3
20
1,1-Dichloroethane
0.0477
0.0050
mg/kg wet
0.05000
95
73-119
3
20
1,1-Dichloroethylene
0.0458
0.0050
mg/kg wet
0.05000
92
59-157
4
20
1, 1 -Dichloropropylene
0.0486
0.0050
mg/kg wet
0.05000
97
70-129
4
20
1,2,3-Trichlorobenzene
0.0432
0.010
mg/kg wet
0.05000
86
59-133
1
20
1,2,3-Trichloropropane
0.0450
0.0050
mg/kg wet
0.05000
90
52-137
4
20
1,2,4-Trichlorobenzene
0.0429
0.010
mg/kg wet
0.05000
86
66-123
0.2
20
1,2,4-Trimethylbenzene
42.8
5.0
ug/kg wet
50.00
86
69-126
2
20
1,2,4-Trimethylbenzene
0.0428
0.0050
mg/kg wet
0.05000
86
69-126
2
20
1,2-Dibromoethane
0.0461
0.0050
mg/kg wet
0.05000
92
69-127
2
20
1,2-Dichlorobenzene
0.0414
0.0050
mg/kg wet
0.05000
83
70-121
0.8
20
1,2-Dichloroethane
0.0448
0.0050
mg/kg wet
0.05000
90
69-125
0.6
20
1,2-Dichloropropane
0.0486
0.0050
mg/kg wet
0.05000
97
75-124
0.7
20
1,3,5-Trimethylbenzene
42.6
5.0
ug/kg wet
50.00
85
69-124
3
20
1,3,5-Trimethylbenzene
0.0426
0.0050
mg/kg wet
0.05000
85
69-124
3
20
1,3-Dichlorobenzene
0.0409
0.0050
mg/kg wet
0.05000
82
70-121
1
20
1,3-Dichloropropane
0.0469
0.0050
mg/kg wet
0.05000
94
70-124
3
20
1,4-Dichlorobenzene
0.0406
0.0050
mg/kg wet
0.05000
81
71-119
1
20
2,2-Dichloropropane
0.0491
0.0050
mg/kg wet
0.05000
98
46-154
5
20
2-Chlorotoluene
0.0413
0.0050
mg/kg wet
0.05000
83
70-121
3
20
4-Chlorotoluene
0.0415
0.0050
mg/kg wet
0.05000
83
72-126
2
20
4-Isopropyltoluene
0.0437
0.0050
mg/kg wet
0.05000
87
71-126
3
20
Acetone
0.0975
0.020
mg/kg wet
0.1000
97
12-196
5
20
Benzene
0.0467
0.0050
mg/kg wet
0.05000
93
74-123
3
20
Bromobenzene
0.0420
0.0050
mg/kg wet
0.05000
84
66-122
1
20
Bromochloromethane
0.0471
0.0050
mg/kg wet
0.05000
94
73-128
3
20
Bromodichloromethane
0.0485
0.0050
mg/kg wet
0.05000
97
76-123
0.7
20
Bromoform
0.0504
0.0050
mg/kg wet
0.05000
101
71-124
4
20
Bromomethane
0.0463
0.010
mg/kg wet
0.05000
93
56-145
5
20
Carbon Tetrachloride
0.0473
0.0050
mg/kg wet
0.05000
95
67-140
5
20
Chlorobenzene
0.0431
0.0050
mg/kg wet
0.05000
86
74-121
2
20
Chloroethane
0.0466
0.010
mg/kg wet
0.05000
93
64-142
4
20
Chloroform
0.0473
0.0050
mg/kg wet
0.05000
95
75-125
2
20
Chloromethane
0.0381
0.010
mg/kg wet
0.05000
76
54-132
29
20 D
cis-1,2-Dichloroethylene
0.0461
0.0050
mg/kg wet
0.05000
92
68-132
0.4
20
cis-1,3-Dichloropropylene
0.0514
0.0050
mg/kg wet
0.05000
103
75-128
1
20
Dibromochloromethane
0.0467
0.0050
mg/kg wet
0.05000
93
71-121
2
20
Dichlorodifluoromethane
0.0374
0.010
mg/kg wet
0.05000
75
39-178
4
20
Ethylbenzene
45.0
5.0
ug/kg wet
50.00
90
69-125
3
20
Ethylbenzene
0.0450
0.0050
mg/kg wet
0.05000
90
69-125
3
20
Isopropyl Ether
0.0480
0.0050
mg/kg wet
0.05000
96
77-123
0.9
20
Isopropylbenzene (Cumene)
0.0441
0.0050
mg/kg wet
0.05000
88
68-129
3
20
m,p-Xylenes
91.1
10
ug/kg wet
100.0
91
64-125
3
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, INC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 40 0 56

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control
Analyte
Batch P911-0044 - 5035
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS Dup (P9L0044-BSD1)
Prepared &Analyzed: 12/02/19
m,p-Xylenes
0.0911
0.010
mg/kg wet
0.1000
91
64-125
3
20
Methyl Butyl Ketone (2-Hexanone)
0.0526
0.020
mg/kg wet
0.05000
105
54-139
7
20
Methyl Ethyl Ketone (2-Butanone)
0.0506
0.020
mg/kg wet
0.05000
101
34-165
5
20
Methyl Isobutyl Ketone
0.0539
0.020
mg/kg wet
0.05000
108
63-130
6
20
Methylene Chloride
0.0444
0.0050
mg/kg wet
0.05000
89
65-135
2
20
Methyl-tert-Butyl Ether
0.0510
0.0050
mg/kg wet
0.05000
102
62-123
2
20
Naphthalene
0.0459
0.010
mg/kg wet
0.05000
92
58-129
4
20
n-Butylbenzene
0.0438
0.0050
mg/kg wet
0.05000
88
71-126
3
20
n-Propylbenzene
42.2
5.0
ug/kg wet
50.00
84
68-128
4
20
n-Propylbenzene
0.0422
0.0050
mg/kg wet
0.05000
84
68-128
4
20
o-Xylene
45.3
5.0
ug/kg wet
50.00
91
69-121
1
20
o-Xylene
0.0453
0.0050
mg/kg wet
0.05000
91
69-121
1
20
sec-Butylbenzene
0.0435
0.0050
mg/kg wet
0.05000
87
71-128
3
20
Styrene
0.0474
0.0050
mg/kg wet
0.05000
95
67-129
0.8
20
tert-Butyl benzene
0.0435
0.0050
mg/kg wet
0.05000
87
71-126
3
20
Tetrachloroethylene
0.0486
0.0050
mg/kg wet
0.05000
97
71-124
3
20
Toluene
46.9
5.0
ug/kg wet
50.00
94
74-122
3
20
Toluene
0.0469
0.0050
mg/kg wet
0.05000
94
74-122
3
20
trans- 1,2-Dichloroethylene
0.0457
0.0050
mg/kg wet
0.05000
91
69-129
3
20
trans- 1,3-Dichloropropylene
0.0519
0.0050
mg/kg wet
0.05000
104
74-127
0.06
20
Trichloroethylene
0.0458
0.0050
mg/kg wet
0.05000
92
68-133
3
20
Trichlorofluoromethane
0.0441
0.010
mg/kg wet
0.05000
88
60-138
4
20
Vinyl acetate
0.0560
0.010
mg/kg wet
0.05000
112
14-179
0.4
20
Vinyl chloride
0.0465
0.010
mg/kg wet
0.05000
93
69-135
5
20
Xylenes, total
136
15
ug/kg wet
150.0
91
74-126
2
200
Xylenes, total
0.136
0.015
mg/kg wet
0.1500
91
74-126
2
200
Surrogate:4-Bromofluorobenzene
49.2
ug/L
50.00
98
70-130
Surrogate:4-Bromofluorobenzene
49.2
ug/L
50.00
98
70-130
Surrogate: Dibromofluoromethane
47.9
ug/L
50.00
96
70-130
Surrogate: Dibromofluoromethane
47.9
ug/L
50.00
96
70-130
Surrogate: Toluene-d8
48.0
ug/L
50.00
96
70-130
Surrogate: Toluene-d8
48.0
ug/L
50.00
96
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 41 0 56

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control
Analyte
Batch P9L0061 - 5035
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9L0061-BLK1)
Prepared &Analyzed: 12/03/19
1,1,1,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,1-Trichloroethane
BRL
0.0050
mg/kg wet
1,1,2,2-Tetrachloroethane
BRL
0.0050
mg/kg wet
1,1,2-Trichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethane
BRL
0.0050
mg/kg wet
1,1-Dichloroethylene
BRL
0.0050
mg/kg wet
1,1-Dichloropropylene
BRL
0.0050
mg/kg wet
1,2,3-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,3-Trichloropropane
BRL
0.0050
mg/kg wet
1,2,4-Trichlorobenzene
BRL
0.010
mg/kg wet
1,2,4-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,2-Dibromoethane
BRL
0.0050
mg/kg wet
1,2-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,2-Dichloroethane
BRL
0.0050
mg/kg wet
1,2-Dichloropropane
BRL
0.0050
mg/kg wet
1,3,5-Trimethyl benzene
BRL
0.0050
mg/kg wet
1,3-Dichlorobenzene
BRL
0.0050
mg/kg wet
1,3-Dichloropropane
BRL
0.0050
mg/kg wet
1,4-Dichlorobenzene
BRL
0.0050
mg/kg wet
2,2-Dichloropropane
BRL
0.0050
mg/kg wet
2-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Chlorotoluene
BRL
0.0050
mg/kg wet
4-Isopropyltoluene
BRL
0.0050
mg/kg wet
Acetone
BRL
0.020
mg/kg wet
Benzene
BRL
0.0050
mg/kg wet
Bromobenzene
BRL
0.0050
mg/kg wet
Bromochloromethane
BRL
0.0050
mg/kg wet
Bromodichloromethane
BRL
0.0050
mg/kg wet
Bromoform
BRL
0.0050
mg/kg wet
Bromomethane
BRL
0.010
mg/kg wet
Carbon Tetrachloride
BRL
0.0050
mg/kg wet
Chlorobenzene
BRL
0.0050
mg/kg wet
Chloroethane
BRL
0.010
mg/kg wet
Chloroform
BRL
0.0050
mg/kg wet
Chloromethane
BRL
0.010
mg/kg wet
cis-1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
cis-1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Dibromochloromethane
BRL
0.0050
mg/kg wet
Dichlorodifluoromethane
BRL
0.010
mg/kg wet
Ethylbenzene
BRL
0.0050
mg/kg wet
Isopropyl Ether
BRL
0.0050
mg/kg wet
Isopropylbenzene (Cumene)
BRL
0.0050
mg/kg wet
m,p-Xylenes
BRL
0.010
mg/kg wet
Methyl Butyl Ketone (2-Hexanone)
BRL
0.020
mg/kg wet
Methyl Ethyl Ketone (2-Butanone)
BRL
0.020
mg/kg wet
Methyl Isobutyl Ketone
BRL
0.020
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 42 0f 56

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control
Analyte
Batch P911-0061 - 5035
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (1291-0061-BLK1)
Prepared &Analyzed: 12/03/19
Methylene Chloride
BRL
0.0050
mg/kg wet
Methyl-tert-Butyl Ether
BRL
0.0050
mg/kg wet
Naphthalene
BRL
0.010
mg/kg wet
n-Butylbenzene
BRL
0.0050
mg/kg wet
n-Propylbenzene
BRL
0.0050
mg/kg wet
o-Xylene
BRL
0.0050
mg/kg wet
sec-Butylbenzene
BRL
0.0050
mg/kg wet
Styrene
BRL
0.0050
mg/kg wet
tert-Butyl benzene
BRL
0.0050
mg/kg wet
Tetrachloroethylene
BRL
0.0050
mg/kg wet
Toluene
BRL
0.0050
mg/kg wet
trans- 1,2-Dichloroethylene
BRL
0.0050
mg/kg wet
trans- 1,3-Dichloropropylene
BRL
0.0050
mg/kg wet
Trichloroethylene
BRL
0.0050
mg/kg wet
Trichlorofluoromethane
BRL
0.010
mg/kg wet
Vinyl acetate
BRL
0.010
mg/kg wet
Vinyl chloride
BRL
0.010
mg/kg wet
Xylenes, total
BRL
0.015
mg/kg wet
Surrogate:4-Bromofluorobenzene
51.2
ug/L
50.00
102
70-130
Surrogate: Dibromofluoromethane
48.8
ug/L
50.00
98
70-130
Surrogate: Toluene-d8
47.1
ug/L
50.00
94
70-130
LCS (1391-0061-BS1)
Prepared &Analyzed:
12/03/19
1,1,1,2-Tetrachloroethane
0.0478
0.0050
mg/kg wet
0.05000
96
72-115
1,1,1-Trichloroethane
0.0518
0.0050
mg/kg wet
0.05000
104
72-123
1,1,2,2-Tetrachloroethane
0.0422
0.0050
mg/kg wet
0.05000
84
62-127
1,1,2-Trichloroethane
0.0461
0.0050
mg/kg wet
0.05000
92
73-123
1,1-Dichloroethane
0.0500
0.0050
mg/kg wet
0.05000
100
73-119
1,1-Dichloroethylene
0.0487
0.0050
mg/kg wet
0.05000
97
59-157
1, 1 -Dichloropropylene
0.0532
0.0050
mg/kg wet
0.05000
106
70-129
1,2,3-Trichlorobenzene
0.0458
0.010
mg/kg wet
0.05000
92
59-133
1,2,3-Trichloropropane
0.0433
0.0050
mg/kg wet
0.05000
87
52-137
1,2,4-Trichlorobenzene
0.0478
0.010
mg/kg wet
0.05000
96
66-123
1,2,4-Trimethylbenzene
0.0467
0.0050
mg/kg wet
0.05000
93
69-126
1,2-Dibromoethane
0.0470
0.0050
mg/kg wet
0.05000
94
69-127
1,2-Dichlorobenzene
0.0443
0.0050
mg/kg wet
0.05000
89
70-121
1,2-Dichloroethane
0.0446
0.0050
mg/kg wet
0.05000
89
69-125
1,2-Dichloropropane
0.0496
0.0050
mg/kg wet
0.05000
99
75-124
1,3,5-Trimethylbenzene
0.0468
0.0050
mg/kg wet
0.05000
94
69-124
1,3-Dichlorobenzene
0.0450
0.0050
mg/kg wet
0.05000
90
70-121
1,3-Dichloropropane
0.0472
0.0050
mg/kg wet
0.05000
94
70-124
1,4-Dichlorobenzene
0.0442
0.0050
mg/kg wet
0.05000
88
71-119
2,2-Dichloropropane
0.0526
0.0050
mg/kg wet
0.05000
105
46-154
2-Chlorotoluene
0.0448
0.0050
mg/kg wet
0.05000
90
70-121
4-Chlorotoluene
0.0449
0.0050
mg/kg wet
0.05000
90
72-126
4-Isopropyltoluene
0.0486
0.0050
mg/kg wet
0.05000
97
71-126
Acetone
0.0873
0.020
mg/kg wet
0.1000
87
12-196
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 43 0 56

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control
Analyte
Batch P911-0061 - 5035
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P9L0061-BS1)
Prepared &Analyzed: 12/03/19
Benzene
0.0493
0.0050
mg/kg wet
0.05000
99
74-123
Bromobenzene
0.0439
0.0050
mg/kg wet
0.05000
88
66-122
Bromochloromethane
0.0491
0.0050
mg/kg wet
0.05000
98
73-128
Bromodichloromethane
0.0496
0.0050
mg/kg wet
0.05000
99
76-123
Bromoform
0.0509
0.0050
mg/kg wet
0.05000
102
71-124
Bromomethane
0.0440
0.010
mg/kg wet
0.05000
88
56-145
Carbon Tetrachloride
0.0529
0.0050
mg/kg wet
0.05000
106
67-140
Chlorobenzene
0.0465
0.0050
mg/kg wet
0.05000
93
74-121
Chloroethane
0.0483
0.010
mg/kg wet
0.05000
97
64-142
Chloroform
0.0500
0.0050
mg/kg wet
0.05000
100
75-125
Chloromethane
0.0489
0.010
mg/kg wet
0.05000
98
54-132
cis-1,2-Dichloroethylene
0.0475
0.0050
mg/kg wet
0.05000
95
68-132
cis-1,3-Dichloropropylene
0.0530
0.0050
mg/kg wet
0.05000
106
75-128
Dibromochloromethane
0.0478
0.0050
mg/kg wet
0.05000
96
71-121
Dichlorodifluoromethane
0.0371
0.010
mg/kg wet
0.05000
74
39-178
Ethylbenzene
0.0491
0.0050
mg/kg wet
0.05000
98
69-125
Isopropyl Ether
0.0482
0.0050
mg/kg wet
0.05000
96
77-123
Isopropylbenzene (Cumene)
0.0484
0.0050
mg/kg wet
0.05000
97
68-129
m,p-Xylenes
0.0998
0.010
mg/kg wet
0.1000
100
64-125
Methyl Butyl Ketone (2-Hexanone)
0.0468
0.020
mg/kg wet
0.05000
94
54-139
Methyl Ethyl Ketone (2-Butanone)
0.0446
0.020
mg/kg wet
0.05000
89
34-165
Methyl Isobutyl Ketone
0.0482
0.020
mg/kg wet
0.05000
96
63-130
Methylene Chloride
0.0441
0.0050
mg/kg wet
0.05000
88
65-135
Methyl-tert-Butyl Ether
0.0510
0.0050
mg/kg wet
0.05000
102
62-123
Naphthalene
0.0466
0.010
mg/kg wet
0.05000
93
58-129
n-Butylbenzene
0.0484
0.0050
mg/kg wet
0.05000
97
71-126
n-Propylbenzene
0.0461
0.0050
mg/kg wet
0.05000
92
68-128
o-Xylene
0.0493
0.0050
mg/kg wet
0.05000
99
69-121
sec-Butylbenzene
0.0483
0.0050
mg/kg wet
0.05000
97
71-128
Styrene
0.0514
0.0050
mg/kg wet
0.05000
103
67-129
tert-Butyl benzene
0.0482
0.0050
mg/kg wet
0.05000
96
71-126
Tetrachloroethylene
0.0542
0.0050
mg/kg wet
0.05000
108
71-124
Toluene
0.0505
0.0050
mg/kg wet
0.05000
101
74-122
trans- 1,2-Dichloroethylene
0.0486
0.0050
mg/kg wet
0.05000
97
69-129
trans- 1,3-Dichloropropylene
0.0522
0.0050
mg/kg wet
0.05000
104
74-127
Trichloroethylene
0.0507
0.0050
mg/kg wet
0.05000
101
68-133
Trichlorofluoromethane
0.0468
0.010
mg/kg wet
0.05000
94
60-138
Vinyl acetate
0.0534
0.010
mg/kg wet
0.05000
107
14-179
Vinyl chloride
0.0480
0.010
mg/kg wet
0.05000
96
69-135
Xylenes, total
0.149
0.015
mg/kg wet
0.1500
99
74-126
Surrogate:4-Bromofluorobenzene
49.7
ug/L
50.00
99
70-130
Surrogate: Dibromofluoromethane
47.0
ug/L
50.00
94
70-130
Surrogate: Toluene-d8
47.3
ug/L
50.00
95
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 44 0 56

P R I IS M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control
Analyte
Batch P911-0061 - 5035
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS Dup (P91-0061-113SD1)
Prepared &Analyzed: 12/03/19
1,1,1,2-Tetrachloroethane
0.0491
0.0050
mg/kg wet
0.05000
98
72-115
3 20
1,1,1-Trichloroethane
0.0518
0.0050
mg/kg wet
0.05000
104
72-123
0.1 20
1,1,2,2-Tetrachloroethane
0.0431
0.0050
mg/kg wet
0.05000
86
62-127
2 20
1,1,2-Trichloroethane
0.0472
0.0050
mg/kg wet
0.05000
94
73-123
2 20
1,1-Dichloroethane
0.0502
0.0050
mg/kg wet
0.05000
100
73-119
0.4 20
1,1-Dichloroethylene
0.0486
0.0050
mg/kg wet
0.05000
97
59-157
0.08 20
1, 1 -Dichloropropylene
0.0525
0.0050
mg/kg wet
0.05000
105
70-129
1 20
1,2,3-Trichlorobenzene
0.0470
0.010
mg/kg wet
0.05000
94
59-133
3 20
1,2,3-Trichloropropane
0.0436
0.0050
mg/kg wet
0.05000
87
52-137
0.6 20
1,2,4-Trichlorobenzene
0.0480
0.010
mg/kg wet
0.05000
96
66-123
0.5 20
1,2,4-Trimethylbenzene
0.0469
0.0050
mg/kg wet
0.05000
94
69-126
0.4 20
1,2-Dibromoethane
0.0477
0.0050
mg/kg wet
0.05000
95
69-127
1 20
1,2-Dichlorobenzene
0.0453
0.0050
mg/kg wet
0.05000
91
70-121
2 20
1,2-Dichloroethane
0.0463
0.0050
mg/kg wet
0.05000
93
69-125
4 20
1,2-Dichloropropane
0.0508
0.0050
mg/kg wet
0.05000
102
75-124
2 20
1,3,5-Trimethylbenzene
0.0466
0.0050
mg/kg wet
0.05000
93
69-124
0.3 20
1,3-Dichlorobenzene
0.0454
0.0050
mg/kg wet
0.05000
91
70-121
0.9 20
1,3-Dichloropropane
0.0481
0.0050
mg/kg wet
0.05000
96
70-124
2 20
1,4-Dichlorobenzene
0.0447
0.0050
mg/kg wet
0.05000
89
71-119
1 20
2,2-Dichloropropane
0.0534
0.0050
mg/kg wet
0.05000
107
46-154
2 20
2-Chlorotoluene
0.0452
0.0050
mg/kg wet
0.05000
90
70-121
0.8 20
4-Chlorotoluene
0.0448
0.0050
mg/kg wet
0.05000
90
72-126
0.1 20
4-Isopropyltoluene
0.0484
0.0050
mg/kg wet
0.05000
97
71-126
0.5 20
Acetone
0.0839
0.020
mg/kg wet
0.1000
84
12-196
4 20
Benzene
0.0497
0.0050
mg/kg wet
0.05000
99
74-123
0.8 20
Bromobenzene
0.0446
0.0050
mg/kg wet
0.05000
89
66-122
2 20
Bromochloromethane
0.0505
0.0050
mg/kg wet
0.05000
101
73-128
3 20
Bromodichloromethane
0.0507
0.0050
mg/kg wet
0.05000
101
76-123
2 20
Bromoform
0.0518
0.0050
mg/kg wet
0.05000
104
71-124
2 20
Bromomethane
0.0453
0.010
mg/kg wet
0.05000
91
56-145
3 20
Carbon Tetrachloride
0.0516
0.0050
mg/kg wet
0.05000
103
67-140
3 20
Chlorobenzene
0.0471
0.0050
mg/kg wet
0.05000
94
74-121
1 20
Chloroethane
0.0476
0.010
mg/kg wet
0.05000
95
64-142
1 20
Chloroform
0.0506
0.0050
mg/kg wet
0.05000
101
75-125
1 20
Chloromethane
0.0477
0.010
mg/kg wet
0.05000
95
54-132
3 20
cis-1,2-Dichloroethylene
0.0485
0.0050
mg/kg wet
0.05000
97
68-132
2 20
cis-1,3-Dichloropropylene
0.0546
0.0050
mg/kg wet
0.05000
109
75-128
3 20
Dibromochloromethane
0.0495
0.0050
mg/kg wet
0.05000
99
71-121
3 20
Dichlorodifluoromethane
0.0370
0.010
mg/kg wet
0.05000
74
39-178
0.4 20
Ethylbenzene
0.0491
0.0050
mg/kg wet
0.05000
98
69-125
0.08 20
Isopropyl Ether
0.0495
0.0050
mg/kg wet
0.05000
99
77-123
3 20
Isopropylbenzene (Cumene)
0.0482
0.0050
mg/kg wet
0.05000
96
68-129
0.4 20
m,p-Xylenes
0.0989
0.010
mg/kg wet
0.1000
99
64-125
0.9 20
Methyl Butyl Ketone (2-Hexanone)
0.0464
0.020
mg/kg wet
0.05000
93
54-139
0.7 20
Methyl Ethyl Ketone (2-Butanone)
0.0430
0.020
mg/kg wet
0.05000
86
34-165
4 20
Methyl Isobutyl Ketone
0.0483
0.020
mg/kg wet
0.05000
97
63-130
0.06 20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 45 0 56

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Organic Compounds by GC/MS (Medium Level) - Quality Control
Reporting
Analyte Result Limit Units
Batch P9L0061 - 5035
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS Dup (P91-0061-BSD1)
Prepared &Analyzed: 12/03/19
Methylene Chloride
0.0452
0.0050
mg/kg wet
0.05000
90
65-135
2
20
Methyl-tert-Butyl Ether
0.0529
0.0050
mg/kg wet
0.05000
106
62-123
4
20
Naphthalene
0.0470
0.010
mg/kg wet
0.05000
94
58-129
0.7
20
n-Butylbenzene
0.0475
0.0050
mg/kg wet
0.05000
95
71-126
2
20
n-Propylbenzene
0.0457
0.0050
mg/kg wet
0.05000
91
68-128
0.8
20
o-Xylene
0.0495
0.0050
mg/kg wet
0.05000
99
69-121
0.4
20
sec-Butylbenzene
0.0475
0.0050
mg/kg wet
0.05000
95
71-128
2
20
Styrene
0.0518
0.0050
mg/kg wet
0.05000
104
67-129
0.6
20
tert-Butylbenzene
0.0480
0.0050
mg/kg wet
0.05000
96
71-126
0.3
20
Tetrachloroethylene
0.0540
0.0050
mg/kg wet
0.05000
108
71-124
0.4
20
Toluene
0.0508
0.0050
mg/kg wet
0.05000
102
74-122
0.6
20
trans-1,2-Dichloroethylene
0.0483
0.0050
mg/kg wet
0.05000
97
69-129
0.7
20
trans- 1,3-Dichloropropylene
0.0543
0.0050
mg/kg wet
0.05000
109
74-127
4
20
Trichloroethylene
0.0504
0.0050
mg/kg wet
0.05000
101
68-133
0.6
20
Trichlorofluoromethane
0.0459
0.010
mg/kg wet
0.05000
92
60-138
2
20
Vinyl acetate
0.0555
0.010
mg/kg wet
0.05000
ill
14-179
4
20
Vinyl chloride
0.0467
0.010
mg/kg wet
0.05000
93
69-135
3
20
Xylenes, total
0.148
0.015
mg/kg wet
0.1500
99
74-126
0.5
200
Surrogate:4-Bromofluorobenzene
50.0
ug/L
50.00
100
70-130
Surrogate: Dibromofluoromethane
47.8
ug/L
50.00
96
70-130
Surrogate: Toluene-d8
46.9
ug/L
50.00
94
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 46 0f 56

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9L0017 - 3546
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9L0017-BLK1)
Prepared: 12/02/19 Analyzed: 12/03/19
1,2,4-Trichlorobenzene
BRL
0.66
mg/kg wet
1,2-Dichlorobenzene
BRL
0.66
mg/kg wet
1,3-Dichlorobenzene
BRL
0.66
mg/kg wet
1,4-Dichlorobenzene
BRL
0.33
mg/kg wet
1-Methyl naphthalene
BRL
0.66
mg/kg wet
2,4,5-Trichlorophenol
BRL
0.66
mg/kg wet
2,4,6-Trichlorophenol
BRL
0.66
mg/kg wet
2,4-Dichlorophenol
BRL
0.66
mg/kg wet
2,4-Dimethylphenol
BRL
0.33
mg/kg wet
2,4-Dinitrophenol
BRL
1.5
mg/kg wet
2,4-Dinitrotoluene
BRL
0.66
mg/kg wet
2,6-Dinitrotoluene
BRL
0.66
mg/kg wet
2-Chloronaphthalene
BRL
0.66
mg/kg wet
2-Chlorophenol
BRL
0.66
mg/kg wet
2-Methyl naphthalene
BRL
0.66
mg/kg wet
2-Methylphenol
BRL
0.66
mg/kg wet
2-Nitrophenol
BRL
0.66
mg/kg wet
3,3'-Dichlorobenzidine
BRL
0.66
mg/kg wet
3/4-Methyl phenol
BRL
0.66
mg/kg wet
4,6-Dinitro-2-methylphenol
BRL
1.5
mg/kg wet
4-Bromophenyl phenyl ether
BRL
0.66
mg/kg wet
4-Chloro-3-methylphenol
BRL
0.66
mg/kg wet
4-Chloroaniline
BRL
0.33
mg/kg wet
4-Chlorophenyl phenyl ether
BRL
1.0
mg/kg wet
4-Nitrophenol
BRL
0.66
mg/kg wet
Acenaphthene
BRL
0.66
mg/kg wet
Acenaphthylene
BRL
0.66
mg/kg wet
Anthracene
BRL
0.66
mg/kg wet
Azobenzene
BRL
0.66
mg/kg wet
Benzo(a)anthracene
BRL
0.66
mg/kg wet
Benzo(a)pyrene
BRL
0.66
mg/kg wet
Benzo(b)fluoranthene
BRL
0.66
mg/kg wet
Benzo(g,h,i)perylene
BRL
0.66
mg/kg wet
Benzo(k)fluoranthene
BRL
0.66
mg/kg wet
Benzoic Acid
BRL
2.0
mg/kg wet
Benzyl alcohol
BRL
0.66
mg/kg wet
bis(2-Chloroethoxy)methane
BRL
0.66
mg/kg wet
Bis(2-Chloroethyl)ether
BRL
0.66
mg/kg wet
Bis(2-chloroisopropyl)ether
BRL
0.33
mg/kg wet
Bis(2-Ethylhexyl)phthalate
BRL
0.66
mg/kg wet
Butyl benzyl phthalate
BRL
0.33
mg/kg wet
Chrysene
BRL
0.66
mg/kg wet
Dibenzo(a,h)anthracene
BRL
0.66
mg/kg wet
Dibenzofuran
BRL
0.66
mg/kg wet
Diethyl phthalate
BRL
0.66
mg/kg wet
Dimethyl phthalate
BRL
0.66
mg/kg wet
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 47 0f 56

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9L0017 - 3546
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9L0017-BLK1)
Prepared: 12/02/19 Analyzed: 12/03/19
Di-n-butyl phthalate
BRL
0.66
mg/kg wet
Di-n-octyl phthalate
BRL
0.33
mg/kg wet
Fluoranthene
BRL
0.66
mg/kg wet
Fluorene
BRL
0.66
mg/kg wet
Hexachlorobenzene
BRL
0.66
mg/kg wet
Hexachlorobutadiene
BRL
0.66
mg/kg wet
Hexachlorocyclopentadiene
BRL
0.66
mg/kg wet
Hexachloroethane
BRL
0.66
mg/kg wet
Indeno(1,2,3-cd)pyrene
BRL
0.66
mg/kg wet
Isophorone
BRL
0.66
mg/kg wet
Naphthalene
BRL
0.66
mg/kg wet
Nitrobenzene
BRL
0.33
mg/kg wet
N-Nitroso-di-n-propylamine
BRL
0.66
mg/kg wet
N-Nitrosodiphenylamine
BRL
0.66
mg/kg wet
Pentachlorophenol
BRL
1.0
mg/kg wet
Phenanthrene
BRL
0.66
mg/kg wet
Phenol
BRL
0.66
mg/kg wet
Pyrene
BRL
0.66
mg/kg wet
Pyridine
BRL
0.33
mg/kg wet
Surrogate: 2,4,6-Tribromophenol
3.33
mg/kg wet
3.330
100
39-132
Surrogate: 2-Fluorobiphenyl
1.52
mg/kg wet
1.665
91
44-115
Surrogate: 2-Fluorophenol
3.20
mg/kg wet
3.330
96
35-115
Surrogate: Nitrobenzene-d5
1.38
mg/kg wet
1.665
83
37-122
Surrogate: Phenol-d5
3.07
mg/kg wet
3.330
92
34-121
Surrogate: Terphenyl-d14
1.44
mg/kg wet
1.665
87
54-127
LCS (P91-0017-BS1)
Prepared: 12/02/19 Analyzed: 12/03/19
1,2,4-Trichlorobenzene
1.22
0.66
mg/kg wet
1.664
73
34-118
1,2-Dichlorobenzene
1.28
0.66
mg/kg wet
1.664
77
33-117
1,3-Dichlorobenzene
1.25
0.66
mg/kg wet
1.664
75
30-115
1,4-Dichlorobenzene
1.25
0.33
mg/kg wet
1.664
75
31-115
1-Methyl naphthalene
1.31
0.66
mg/kg wet
1.664
79
40-119
2,4,5-Trichlorophenol
1.50
0.66
mg/kg wet
1.664
90
62-124
2,4,6-Trichlorophenol
1.53
0.66
mg/kg wet
1.664
92
39-126
2,4-Dichlorophenol
1.31
0.66
mg/kg wet
1.664
78
40-122
2,4-Dimethylphenol
1.46
0.33
mg/kg wet
1.664
88
30-127
2,4-Dinitrophenol
1.12
1.5
mg/kg wet
1.664
67
27-129 J
2,4-Dinitrotoluene
1.50
0.66
mg/kg wet
1.664
90
48-126
2,6-Dinitrotoluene
1.56
0.66
mg/kg wet
1.664
94
46-124
2-Chloronaphthalene
1.38
0.66
mg/kg wet
1.664
83
41-114
2-Chlorophenol
1.43
0.66
mg/kg wet
1.664
86
34-121
2-Methyl naphthalene
1.28
0.66
mg/kg wet
1.664
77
38-122
2-Methylphenol
1.47
0.66
mg/kg wet
1.664
88
32-122
2-Nitrophenol
1.28
0.66
mg/kg wet
1.664
77
36-123
3,3'-Dichlorobenzidine
1.37
0.66
mg/kg wet
1.664
82
22-121
3/4-Methyl phenol
1.34
0.66
mg/kg wet
1.664
80
34-119
4,6-Dinitro-2-methylphenol
1.53
1.5
mg/kg wet
1.664
92
29-132
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 48 0f 56

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9L0017 - 3546
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P9L0017-BS1)
Prepared: 12/02/19 Analyzed: 12/03/19
4-Bromophenyl phenyl ether
1.43
0.66
mg/kg wet
1.664
86
46-124
4-Chloro-3-methylphenol
1.36
0.66
mg/kg wet
1.664
82
45-122
4-Chloroaniline
1.07
0.33
mg/kg wet
1.664
64
17-106
4-Chlorophenyl phenyl ether
1.40
1.0
mg/kg wet
1.664
84
45-121
4-Nitrophenol
1.61
0.66
mg/kg wet
1.664
97
30-132
Acenaphthene
1.48
0.66
mg/kg wet
1.664
89
40-123
Acenaphthylene
1.55
0.66
mg/kg wet
1.664
93
32-132
Anthracene
1.48
0.66
mg/kg wet
1.664
89
47-123
Azobenzene
1.50
0.66
mg/kg wet
1.664
90
39-125
Benzo(a)anthracene
1.38
0.66
mg/kg wet
1.664
83
49-126
Benzo(a)pyrene
1.55
0.66
mg/kg wet
1.664
93
45-129
Benzo(b)fluoranthene
1.46
0.66
mg/kg wet
1.664
88
45-132
Benzo(g,h,i)perylene
1.48
0.66
mg/kg wet
1.664
89
43-134
Benzo(k)fluoranthene
1.55
0.66
mg/kg wet
1.664
93
47-132
Benzoic Acid
0.676
2.0
mg/kg wet
1.664
41
10-83
Benzyl alcohol
1.43
0.66
mg/kg wet
1.664
86
29-122
bis(2-Chloroethoxy)methane
1.19
0.66
mg/kg wet
1.664
71
36-121
Bis(2-Chloroethyl)ether
1.30
0.66
mg/kg wet
1.664
78
31-120
Bis(2-chloroisopropyl)ether
1.24
0.33
mg/kg wet
1.664
74
33-131
Bis(2-Ethylhexyl)phthalate
1.46
0.66
mg/kg wet
1.664
87
51-133
Butyl benzyl phthalate
1.47
0.33
mg/kg wet
1.664
88
48-132
Chrysene
1.44
0.66
mg/kg wet
1.664
87
50-124
Dibenzo(a,h)anthracene
0.756
0.66
mg/kg wet
1.664
45
45-134
Dibenzofuran
1.43
0.66
mg/kg wet
1.664
86
44-120
Diethyl phthalate
1.44
0.66
mg/kg wet
1.664
86
50-124
Dimethyl phthalate
1.42
0.66
mg/kg wet
1.664
86
48-124
Di-n-butyl phthalate
1.53
0.66
mg/kg wet
1.664
92
51-128
Di-n-octyl phthalate
1.53
0.33
mg/kg wet
1.664
92
45-140
Fluoranthene
1.50
0.66
mg/kg wet
1.664
90
50-127
Fluorene
1.47
0.66
mg/kg wet
1.664
88
43-125
Hexachlorobenzene
1.47
0.66
mg/kg wet
1.664
88
45-122
Hexachlorobutadiene
1.29
0.66
mg/kg wet
1.664
78
32-123
Hexachlorocyclopentadiene
1.30
0.66
mg/kg wet
1.664
78
32-117
Hexachloroethane
1.20
0.66
mg/kg wet
1.664
72
28-117
Indeno(1,2,3-cd)pyrene
1.40
0.66
mg/kg wet
1.664
84
45-133
Isophorone
1.03
0.66
mg/kg wet
1.664
62
30-122
Naphthalene
1.20
0.66
mg/kg wet
1.664
72
35-123
Nitrobenzene
1.11
0.33
mg/kg wet
1.664
67
34-122
N-Nitroso-di-n-propylamine
1.42
0.66
mg/kg wet
1.664
85
36-120
N-Nitrosodiphenylamine
1.79
0.66
mg/kg wet
1.664
108
38-127
Pentachlorophenol
1.72
1.0
mg/kg wet
1.664
104
25-133
Phenanthrene
1.46
0.66
mg/kg wet
1.664
88
50-121
Phenol
1.52
0.66
mg/kg wet
1.664
91
34-121
Pyrene
1.50
0.66
mg/kg wet
1.664
90
47-127
Pyridine
0.923
0.33
mg/kg wet
1.664
55
10-60
Surrogate: 2,4,6-Tribromophenol
3.18
mg/kg wet
3.328
96
39-132
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 49 0f 56

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Semivolatile Organic Compounds by GC/MS - Quality Control
Analyte
Batch P9L0017 - 3546
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P9L0017-BS1)
Prepared: 12/02/19 Analyzed: 12/03/19
Surrogate: 2-Fluorobiphenyl
1.31
mg/kg wet
1.664
79
44-115
Surrogate: 2-Fluorophenol
2.82
mg/kg wet
3.328
85
35-115
Surrogate: Nitrobenzene-d5
1.10
mg/kg wet
1.664
66
37-122
Surrogate: Phenol-d5
2.65
mg/kg wet
3.328
80
34-121
Surrogate: Terphenyl-d14
1.34
mg/kg wet
1.664
80
54-127
LCS Dup (P9L0017-BSD1)
Prepared: 12/02/19 Analyzed: 12/03/19
1,2,4-Trichlorobenzene
1.19
0.66
mg/kg wet
1.664
72
34-118
2
20
1,2-Dichlorobenzene
1.25
0.66
mg/kg wet
1.664
75
33-117
3
20
1,3-Dichlorobenzene
1.20
0.66
mg/kg wet
1.664
72
30-115
4
20
1,4-Dichlorobenzene
1.21
0.33
mg/kg wet
1.664
73
31-115
4
20
1-Methyl naphthalene
1.30
0.66
mg/kg wet
1.664
78
40-119
1
20
2,4,5-Trichlorophenol
1.44
0.66
mg/kg wet
1.664
87
62-124
4
20
2,4,6-Trichlorophenol
1.46
0.66
mg/kg wet
1.664
88
39-126
5
20
2,4-Dichlorophenol
1.28
0.66
mg/kg wet
1.664
77
40-122
2
20
2,4-Dimethylphenol
1.42
0.33
mg/kg wet
1.664
85
30-127
3
20
2,4-Dinitrophenol
1.03
1.5
mg/kg wet
1.664
62
27-129
8
20 J
2,4-Dinitrotoluene
1.42
0.66
mg/kg wet
1.664
85
48-126
6
20
2,6-Dinitrotoluene
1.45
0.66
mg/kg wet
1.664
87
46-124
7
20
2-Chloronaphthalene
1.36
0.66
mg/kg wet
1.664
81
41-114
2
20
2-Chlorophenol
1.38
0.66
mg/kg wet
1.664
83
34-121
4
20
2-Methyl naphthalene
1.26
0.66
mg/kg wet
1.664
76
38-122
1
20
2-Methylphenol
1.43
0.66
mg/kg wet
1.664
86
32-122
3
20
2-Nitrophenol
1.25
0.66
mg/kg wet
1.664
75
36-123
3
20
3,3'-Dichlorobenzidine
1.34
0.66
mg/kg wet
1.664
80
22-121
2
20
3/4-Methyl phenol
1.29
0.66
mg/kg wet
1.664
77
34-119
4
20
4,6-Dinitro-2-methylphenol
1.47
1.5
mg/kg wet
1.664
88
29-132
4
20 J
4-Bromophenyl phenyl ether
1.40
0.66
mg/kg wet
1.664
84
46-124
2
20
4-Chloro-3-methylphenol
1.31
0.66
mg/kg wet
1.664
79
45-122
4
20
4-Chloroaniline
1.04
0.33
mg/kg wet
1.664
63
17-106
2
20
4-Chlorophenyl phenyl ether
1.35
1.0
mg/kg wet
1.664
81
45-121
4
20
4-Nitrophenol
1.50
0.66
mg/kg wet
1.664
90
30-132
7
20
Acenaphthene
1.39
0.66
mg/kg wet
1.664
84
40-123
6
20
Acenaphthylene
1.48
0.66
mg/kg wet
1.664
89
32-132
5
20
Anthracene
1.42
0.66
mg/kg wet
1.664
85
47-123
4
20
Azobenzene
1.43
0.66
mg/kg wet
1.664
86
39-125
5
20
Benzo(a)anthracene
1.29
0.66
mg/kg wet
1.664
78
49-126
7
20
Benzo(a)pyrene
1.46
0.66
mg/kg wet
1.664
87
45-129
6
20
Benzo(b)fluoranthene
1.38
0.66
mg/kg wet
1.664
83
45-132
6
20
Benzo(g,h,i)perylene
1.39
0.66
mg/kg wet
1.664
84
43-134
6
20
Benzo(k)fluoranthene
1.46
0.66
mg/kg wet
1.664
88
47-132
6
20
Benzoic Acid
0.689
2.0
mg/kg wet
1.664
41
10-83
2
20 J
Benzyl alcohol
1.38
0.66
mg/kg wet
1.664
83
29-122
3
20
bis(2-Chloroethoxy)methane
1.15
0.66
mg/kg wet
1.664
69
36-121
3
20
Bis(2-Chloroethyl)ether
1.21
0.66
mg/kg wet
1.664
73
31-120
7
20
Bis(2-chloroisopropyl)ether
1.19
0.33
mg/kg wet
1.664
71
33-131
4
20
Bis(2-Ethylhexyl)phthalate
1.38
0.66
mg/kg wet
1.664
83
51-133
5
20
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 50 0f 56

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property Prism Work Order: 9110453
Attn: Al Quarles Time Submitted: 11/27/2019 10:00:OOAM
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P9L0017 - 3546
LCS Dup (P9L0017-BSD1)
Prepared: 12/02/19 Analyzed: 12/03/19
Butyl benzyl phthalate
1.36
0.33
mg/kg wet
1.664
82
48-132
8
20
Chrysene
1.34
0.66
mg/kg wet
1.664
80
50-124
7
20
Dibenzo(a,h)anthracene
0.655
0.66
mg/kg wet
1.664
39
45-134
14
20 L2, J
Dibenzofuran
1.36
0.66
mg/kg wet
1.664
82
44-120
5
20
Diethyl phthalate
1.34
0.66
mg/kg wet
1.664
81
50-124
7
20
Dimethyl phthalate
1.35
0.66
mg/kg wet
1.664
81
48-124
5
20
Di-n-butyl phthalate
1.47
0.66
mg/kg wet
1.664
89
51-128
4
20
Di-n-octyl phthalate
1.42
0.33
mg/kg wet
1.664
85
45-140
7
20
Fluoranthene
1.45
0.66
mg/kg wet
1.664
87
50-127
3
20
Fluorene
1.39
0.66
mg/kg wet
1.664
83
43-125
6
20
Hexachlorobenzene
1.41
0.66
mg/kg wet
1.664
84
45-122
4
20
Hexachlorobutadiene
1.26
0.66
mg/kg wet
1.664
76
32-123
2
20
Hexachlorocyclopentadiene
1.26
0.66
mg/kg wet
1.664
76
32-117
3
20
Hexachloroethane
1.16
0.66
mg/kg wet
1.664
70
28-117
3
20
Indeno(1,2,3-cd)pyrene
1.32
0.66
mg/kg wet
1.664
79
45-133
6
20
Isophorone
1.00
0.66
mg/kg wet
1.664
60
30-122
2
20
Naphthalene
1.17
0.66
mg/kg wet
1.664
70
35-123
3
20
Nitrobenzene
1.09
0.33
mg/kg wet
1.664
65
34-122
2
20
N-Nitroso-di-n-propylamine
1.37
0.66
mg/kg wet
1.664
82
36-120
4
20
N-Nitrosodiphenylamine
1.70
0.66
mg/kg wet
1.664
102
38-127
5
20
Pentachlorophenol
1.65
1.0
mg/kg wet
1.664
99
25-133
5
20
Phenanthrene
1.41
0.66
mg/kg wet
1.664
85
50-121
4
20
Phenol
1.43
0.66
mg/kg wet
1.664
86
34-121
6
20
Pyrene
1.40
0.66
mg/kg wet
1.664
84
47-127
7
20
Pyridine
0.908
0.33
mg/kg wet
1.664
55
10-60
2
20
Surrogate: 2,4,6-Tribromophenol
3.04
mg/kg wet
3.329
91
39-132
Surrogate: 2-Fluorobiphenyl
1.26
mg/kg wet
1.664
76
44-115
Surrogate: 2-Fluorophenol
2.77
mg/kg wet
3.329
83
35-115
Surrogate: Nitrobenzene-d5
1.08
mg/kg wet
1.664
65
37-122
Surrogate: Phenol-d5
2.58
mg/kg wet
3.329
78
34-121
Surrogate: Terphenyl-d14
1.25
mg/kg wet
1.664
75
54-127
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 51 0f 56

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control
Analyte
Batch P9K0496 - MADEP VPH (S
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9K0496-BLK1)
Prepared &Analyzed: 11/27/19
C5-C8 Aliphatics
BRL
5.0
mg/kg wet
C9-C12 Aliphatics
BRL
5.0
mg/kg wet
C9-Cl0 Aromatics
BRL
5.0
mg/kg wet
Surrogate: 2,5-Dibromotoluene (PID)
9140
ug/L
10000 91
70-130
Surrogate: 2,5-Dibromotoluene (FID)
10800
ug/L
10000 108
70-130
LCS (P9K0496-BSI)
Prepared &Analyzed: 11/27/19
C5-C8 Aliphatics
33.5
5.0
mg/kg wet
32.00 105
70-130
C9-Cl0 Aromatics
9.88
5.0
mg/kg wet
10.67 93
70-130
C9-C12 Aliphatic
33.4
5.0
mg/kg wet
32.00 105
70-130
Surrogate: 2,5-Dibromotoluene (PID)
9050
ug/L
10000 91
70-130
Surrogate: 2,5-Dibromotoluene (FID)
10700
ug/L
10000 107
70-130
LCS Dup (P9K0496-BSD1)
Prepared & Analyzed: 11/27/19
C5-C8 Aliphatics
34.3
5.0
mg/kg wet
32.00 107
70-130 2 50
C9-Cl0 Aromatics
9.22
5.0
mg/kg wet
10.67 86
70-130 7 50
C9-C12 Aliphatic
32.4
5.0
mg/kg wet
32.00 101
70-130 3 50
Surrogate: 2,5-Dibromotoluene (PID)
8940
ug/L
10000 89
70-130
Surrogate: 2,5-Dibromotoluene (FID)
10600
ug/L
10000 106
70-130
Batch P9L0004 - MADEP VPH (S)
Blank (P9L0004-BLK1)
Prepared & Analyzed: 12/02/19
C5-C8 Aliphatics
BRL
5.0
mg/kg wet
C9-C12 Aliphatics
BRL
5.0
mg/kg wet
C9-Cl0 Aromatics
BRL
5.0
mg/kg wet
Surrogate: 2,5-Dibromotoluene (PID)
10400
ug/L
10000 104
70-130
Surrogate: 2,5-Dibromotoluene (FID)
11200
ug/L
10000 112
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 52 0f 56

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Volatile Petroleum Hydrocarbons by GC/PID/FID - Quality Control
Reporting
Analyte Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Batch P9L0004 - MADEP VPH (S)
LCS (P9L0004-BS1)
Prepared &Analyzed: 12/02/19
C5-C8 Aliphatics
24.9
5.0
mg/kg wet
32.00 78
70-130
C9-Cl0 Aromatics
10.8
5.0
mg/kg wet
10.67 101
70-130
C9-C12 Aliphatic
31.5
5.0
mg/kg wet
32.00 98
70-130
Surrogate: 2,5-Dibromotoluene (PID)
10300
ug/L
10000 103
70-130
Surrogate: 2,5-Dibromotoluene (FID)
11200
ug/L
10000 112
70-130
LCS Dup (P9L0004-BSD1)
Prepared &Analyzed: 12/02/19
C5-C8 Aliphatics
25.1
5.0
mg/kg wet
32.00 78
70-130 0.7 50
C9-Cl0 Aromatics
10.5
5.0
mg/kg wet
10.67 98
70-130 3 50
C9-C12 Aliphatic
31.3
5.0
mg/kg wet
32.00 98
70-130 0.4 50
Surrogate: 2,5-Dibromotoluene (PID)
10500
ug/L
10000 105
70-130
Surrogate: 2,5-Dibromotoluene (FID)
11400
ug/L
10000 114
70-130
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 53 0f 56

P R 1 S M Full -Service Analytical s
Environmental Solutions
LABORATOR,
Level II QC Report
12/4/19
ATC Group Services, LLC Project: Tim Collins Property
Attn: Al Quarles
7606 Whitehall Executive Center Drive, Suite
Charlotte, NC 28273
Extractable Petroleum Hydrocarbons by GC/FID - Quality Control
Analyte
Batch P9K0497 - 3546
Reporting
Result Limit Units
Prism Work Order: 9110453
Time Submitted: 11/27/2019 10:00:OOAM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
Blank (P9K0497-BLK1)
Prepared: 11/27/19 Analyzed: 12/03/19
C9-Cl8 Aliphatics
BRL
25
mg/kg wet
C19-C36 Aliphatics
BRL
25
mg/kg wet
C11-C22 Aromatics
BRL
25
mg/kg wet
Surrogate: 1-Chlorooctadecane
1.12
mg/kg wet
1.998
56
40-140
Surrogate: o-Terphenyl
1.54
mg/kg wet
1.998
77
40-140
Surrogate: 2-Fluorobiphenyl
3.32
mg/kg wet
3.996
83
40-140
Surrogate: 2-Bromonaphthalene
3.44
mg/kg wet
3.996
86
40-140
LCS (P9K0497-BS1)
Prepared: 11/27/19 Analyzed: 12/03/19
C9-C18 Aliphatics
30.3
25
mg/kg wet
59.94
51
40-140
C19-C36 Aliphatics
58.4
25
mg/kg wet
79.92
73
40-140
C1 1-C22 Aromatics
267
25
mg/kg wet
339.7
79
40-140
Surrogate: 1-Chlorooctadecane
1.22
mg/kg wet
1.998
61
40-140
Surrogate: o-Terphenyl
1.48
mg/kg wet
1.998
74
40-140
Surrogate: 2-Fluorobiphenyl
3.17
mg/kg wet
3.996
79
40-140
Surrogate: 2-Bromonaphthalene
3.53
mg/kg wet
3.996
88
40-140
LCS Dup (P9K0497-BSD1)
Prepared: 11/27/19 Analyzed: 12/03/19
C9-C18 Aliphatics
30.5
25
mg/kg wet
59.52
51
40-140 0.8 50
C19-C36 Aliphatics
57.0
25
mg/kg wet
79.37
72
40-140 2 50
C11-C22 Aromatics
272
25
mg/kg wet
337.3
81
40-140 2 50
Surrogate: 1-Chlorooctadecane
1.27
mg/kg wet
1.984
64
40-140
Surrogate: o-Terphenyl
1.50
mg/kg wet
1.984
75
40-140
Surrogate: 2-Fluorobiphenyl
3.30
mg/kg wet
3.968
83
40-140
Surrogate: 2-Bromonaphthalene
3.64
mg/kg wet
3.968
92
40-140
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 54 of 56

Sample Extraction Data
Prep Method: 3546
Lab Number
Batch
Initial
Final
Date/Time
9110453-01
1391<0497
10
g 2 mL
11/27/19 14:30
9110453-02
P9K0497
10
g 2 mL
11/27/19 14:30
9110453-03
P91<0497
10
g 2 mL
11/27/19 14:30
9110453-04
P91<0497
10
g 2 mL
11/27/19 14:30
9110453-05
P91<0497
10
g 2 mL
11/27/19 14:30
9110453-05
P9K0497
10
g 2 mL
11/27/19 14:30
Prep Method: Solids, Dry Weight
Lab Number
Batch
Initial
Final
Date/Time
9110453-01
P91-0025
30
g 30 g
12/02/19 14:56
9110453-02
P91-0025
30
g 30 g
12/02/19 14:56
9110453-03
P91-0025
30
g 30 g
12/02/19 14:56
9110453-04
1391-0025
30
g 30 g
12/02/19 14:56
9110453-05
1391-0025
30
g 30 g
12/02/19 14:56
Prep Method: 3546
Lab Number
Batch
Initial
Final
DatelTime
9110453-01
P91-0017
30
g 1 mL
12/02/19 12:00
9110453-01
P91-0017
30
g 1 mL
12/02/19 12:00
9110453-02
1391-0017
30.2
g 1 mL
12/02/19 12:00
9110453-02
1391-0017
30.2
g 1 mL
12/02/19 12:00
9110453-03
1391-0017
30.07
g 1 mL
12/02/19 12:00
9110453-03
1391-0017
30.07
g 1 mL
12/02/19 12:00
9110453-04
P91-0017
30.05
g 1 mL
12/02/19 12:00
9110453-05
P91-0017
30.01
g 1 mL
12/02/19 12:00
Prep Method: 5035
Lab Number
Batch
Initial
Final
Date/Time
9110453-04
1391-0050
5.32
g 5 mL
12/03/19 10:00
9110453-05
1391-0043
5.31
g 5 mL
12/02/19 10:00
Prep Method: 5035
Lab Number
Batch
Initial
Final
Date/Time
9110453-01
1391-0061
4.72
g 5 mL
12/02/19 10:00
9110453-01
1391-0061
4.72
g 5 mL
12/02/19 10:00
9110453-02
1391-0061
4.99
g 5 mL
12/02/19 10:00
9110453-02
1391-0061
4.99
g 5 mL
12/02/19 10:00
9110453-03
P91-0044
6.35
g 5 mL
12/02/19 9:30
9110453-05
P91-0044
4.81
g 5 mL
12/02/19 9:30
9110453-05
P91-0044
4.81
g 5 mL
12/02/19 9:30
Prep Method: MADEP VPH (S)
Lab Number
Batch
Initial
Final
Date/Time
9110453-01
P91-0004
4.86
g 16 mL
12/02/19 8:24
9110453-02
P91-0004
5.9
g 16 mL
12/02/19 8:24
9110453-03
P91<0496
5.94
g 16 mL
11/27/19 11:14
9110453-04
P91<0496
5.01
g 16 mL
11/27/19 11:14
9110453-05
P91<0496
4.92
g 16 mL
11/27/19 11:14
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook
Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 55 0f 56

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L� Page 56 of 56

NOTICE OF RESIDUAL PETROLEUM
Tim Collins Property, Mecklenburg County, North Carolina
2640 Shenandoah Ave, Charlotte, North Carolina, 28205
Mecklenburg County Register of Deeds, Book 30084, Pages 64-66
The property that is the subject of this Notice (hereinafter referred to as the "Site")
contains residual petroleum and is an Underground Storage Tank (UST) incident under North
Carolina's Statutes and Regulations, which consist of N.C.G.S. 143-215.94 and regulations adopted
thereunder. This Notice is part of a remedial action for the Site that has been approved by the
Secretary (or his/her delegate) of the North Carolina Department of Environment Quality (or its
successor in function), as authorized by N.C.G.S. Section 143B-279.9 and 143B-279.11. The North
Carolina Department of Environment Quality shall hereinafter be referred to as "DEQ".
NOTICE
Petroleum product was released and/or discharged at the Site. Petroleum constituents remain
on the site, but are not a danger to public health and the environment, provided that the
restrictions described herein, and any other measures required by DEQ pursuant to N.C.G.S.
Sections 14313-279.9 and 143B-279.11, are strictly complied with. This "Notice of Residual
Petroleum" is composed of a description of the property, the location of the residual petroleum, and the
land use restrictions on the Site. The Notice has been approved and notarized by DEQ pursuant to
N.C.G.S. Sections 143B-279.9 and 143B-279.11 and has/shall be recorded at the
Mecklenburg Register of Deeds' office Book , Page
Any map or plat required by DEQ has been/shall be recorded at the Mecklenburg County
Register of Deeds' office Book , Page , and has been/shall be incorporated into the Notice by
this reference.
Source Property
Tim Collins of 2633 Shenandoah Avenue, Charlotte, North Carolina 28205 is the owner in fee
simple of all or a portion of the Site, which is located in the County of Mecklenburg, State of North
Carolina, and is known and legally described as:
MAIL TO (after filing):
Tim Collins, 2633 Shenandoah Avenue, Charlotte, North Carolina 28205
Revised February 7, 2019

Being all of Lot 11 and part ofLot 12 in Block 32 of CHANTILLY, as same is shown on a map
thereof recorded in Map Book 230, Page 249 of the Mecklenburg County Public Registry, being
more particularly described as follows:
BEGINNING at an existing iron pipe in the southerly margin of the right-of-way of Shenandoah
Avenue, said point marking the common corner of Lots 10 and 11, and running thence with the
dividing line between said Lots 10 and 11, S 33-46-35 W 149.91 feet to an existing iron pipe in
the northerly margin of a 12.5 foot alleyway; thence with the said margin of said alleyway S 56-
09-17 E 59.94 feet to an existing iron pipe in the southerly margin of said Lot 12; thence N 33-47-
57 E 150.06 feet to a point in the southerly margin of the right-of-way of said Shenandoah
Avenue; thence with said right-of-way N 56-18 W 60.0 feet to an existing iron pipe, the point or
place of BEGINNING, all as shown on plat of survey dated May 10,1988, prepared by Richard
Boyd Brooks, Registered Surveyor.
For protection of public health and the environment, the following land use restrictions required
by N.C.G.S. Section 143B-279.9(b) shall apply to all of the above -described real property. These
restrictions shall continue in effect as long as residual petroleum remains on the site in excess of
unrestricted use standards and cannot be amended or cancelled unless and until the Mecklenburg County
Register of Deed receives and records the written concurrence of the Secretary (or his/her delegate) of
DEQ (or its successor in function).
PERPETUAL LAND USE RESTRICTIONS
Soil: Soil containing residual petroleum above applicable regulatory standards) remains on
the site in the area identified in Figure 1, Attachment A. No soil shall be excavated or
disturbed within 3 feet of the area identified in Figure 1, Attachment A except to
remediate the soil in accordance with all applicable state and federal statutes,
regulations and guidelines.
Groundwater: Groundwater from the site is prohibited from use as a water supply. Water supply wells
of any kind shall not be installed or operated on the site.
ENFORCEMENT
The above land use restriction(s) shall be enforced by any owner, operator, or other party
responsible for the Site. The above land use restriction(s) may also be enforced by DEQ through any of
the remedies provided by law or by means of a civil action, and may also be enforced by any unit of local
government having jurisdiction over any part of the Site. Any attempt to cancel this Notice without the
approval of DEQ (or its successor in function) shall be subject to enforcement by DEQ to the full extent
of the law. Failure by any party required or authorized to enforce any of the above restriction(s) shall in
no event be deemed a waiver of the right to do so thereafter as to the same violation or as to one occurring
prior or subsequent thereto.
Revised February 7, 2019
2

IN WITNESS WHEREOF, Tim Collins has caused this Notice to be executed pursuant to
N.C.G.S. Sections 14313-279.9 and 14313-279.11, this day of 92019.
LIM
Signatory's name typed or printed:
COUNTY
(Name of county in which acknowledgment was taken)
(signature of responsible party, attorney or other agent if there is one)
(title of agent for responsible party if there is one)
I certify that the following person(s) personally appeared before me this day, each acknowledging to me
that he or she signed the foregoing document:
Date:
(Official Seal)
expires:
(signature of Notary Public)
printed or typed name of Notary Public)
Notary Public
My commission
Revised February 7, 2019

Approved for the purposes of N.C.G.S. 143B-279.11
(signature of Regional Supervisor)
Regional Supervisor
(printed name of Regional Supervisor)
Regional Office
UST Section
Division of Waste Management
Department of Environment Quality
NORTH CAROLINA
COUNTY
(Name of county in which acknowledgment was taken)
I certify that the following person(s) personally appeared before me this day, each acknowledging to me
that he or she signed the foregoing document: (full printed name of Regional Supervisor)
Date:
(Official Seal)
expires:
(signature of Notary Public)
printed or typed name of Notary Public)
Notary Public
My commission
Revised February 7, 2019
4

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SE-3
Close-up of Excavation
Scale: 1 inch — 10 feet
1 Aerial Map Scale: 1 inch -- 30 feet
All locations and distances are approximate,
and are not based on a site survey. SOIL SAMPLING LOCATION
7606 Whitehall Executive Center
Iff Drive, Suite 800
AwAkTc Charlotte, North Carolina
AV [phone]
SOURCE: Mecklenburg County POLARIS
FIGURE 1, ATTACHMENT A.
SAMPLE LOCATION MAP
Tim Collins Property, Incident # 40966
2640 Shenandoah Avenue
Charlotte, North Carolina 28205
ATC Project No. 199TCP1901

Beverly, Trudy
From: Al Quarles <[e-mail]>
Sent: Tuesday, December 10, 2019 9:48 AM
To: Beverly, Trudy
Cc: Erin Greene
Subject: RE: [External] Tim Collins Property #40966 20Day Report and Draft NORP
not click links or open attachments unless you verify. Send all suspicious email as an
[e-mail]
Thank you.
Al Quarles I SENIOR PROJECT MANAGER I ATC Group Services LLC
Office + 1 704 529 3200 1 Direct [phone] Mobile + 1 803 984 6764
ETC
7606 Whitehall Executive Center Drive Suite 800 1 Charlotte, NC 28273
al.quarles(a)atcas.com I www.atcciroupservices.com
This email and its attachments may contain confidential and/or privileged information for the sole use of the intended recipient(s). If
you are not the intended recipient, any use, distribution or copying of the information contained in this email and its attachments is
strictly prohibited. If you have received this email in error, please notify the sender by replying to this message and immediately
delete and destroy any copies of this email and any attachments. The views or opinions expressed are the author's own and may not
reflect the views or opinions of ATC.
From: Beverly, Trudy <[e-mail]>
Sent: Tuesday, December 10, 2019 9:47 AM
To: Al Quarles <[e-mail]>
Cc: Erin Greene <[e-mail]>
Subject: RE: [External] Tim Collins Property #40966 20Day Report and Draft NORP
The Hart & Hickman survey is sufficient to cover the Tim Collins Property.
Trudy
From: Al Quarles [mailto:[e-mail]]
Sent: Tuesday, December 10, 2019 9:36 AM
To: Beverly, Trudy <[e-mail]>
Cc: Erin Greene <[e-mail]>
Subject: [External] Tim Collins Property #40966 20Day Report and Draft NORP

toe rnal email. Do not click links or open attachments unless you verify. Send all suspicious email as an
Wchment [e-mail]
Trudy,
Are you asking that we need to go out for this site to look for water supply wells within 150 feet, of that the
information from the H&H report is sufficient for our site?
Thanks,
Al
Al Quarles I SENIOR PROJECT MANAGER I ATC Group Services LLC
Office + 1 704 529 3200 1 Direct [phone] Mobile + 1 803 984 6764
Ar
■kTc
7606 Whitehall Executive Center Drive Suite 800 1 Charlotte, NC 28273
al.quarles(o)atcgs.com I www.atcaroupservices.com
This email and its attachments may contain confidential and/or privileged information for the sole use of the intended recipient(s). If
you are not the intended recipient, any use, distribution or copying of the information contained in this email and its attachments is
strictly prohibited. If you have received this email in error, please notify the sender by replying to this message and immediately
delete and destroy any copies of this email and any attachments. The views or opinions expressed are the author's own and may not
reflect the views or opinions of ATC.
From: Beverly, Trudy <[e-mail]>
Sent: Tuesday, December 10, 2019 9:03 AM
To: Al Quarles <[e-mail]>
Cc: Erin Greene <[e-mail]>
Subject: RE: [External] Tim Collins Property #40966 20Day Report and Draft NORP
The 2018 Hart & Hickman survey for incident #8603 looks good to cover this incident. You or your staff should
be looking for water supply wells within 150' of home heating oil ust releases in the field and be willing certify
that information with a seal from a licensed NC geologist of professional engineer from your company or
contractor. The Mecklenburg County well information website is a good resource. But, there are many wells
that were installed prior to their records.
I did not see any changes for the draft Notice of Residual Petroleum. The signed and notarized original Notice
can be mailed to the office for my review and Ron's signature. The Conditional NFA letter will be issued after
the Notice has been reviewed, signed, and notarized by the UST Section.
Thanks,
Trudy

Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
Moll,
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy.Beverly(ic ,ncdenr. gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
From: Al Quarles [mailto:[e-mail]]
Sent: Tuesday, December 10, 2019 8:29 AM
To: Beverly, Trudy <[e-mail]>
Cc: Erin Greene <[e-mail]>
Subject: [External] Tim Collins Property #40966 20Day Report and Draft NORP
no External email. Do not click links or open attachments unless you verify. Send all suspicious email as an
chment to [e-mail]
Trudy,
We have not conducted a survey of the area for water supply wells. Two other UST incidents are in proximity,
and both indicated no water supply wells within 1,000 feet of those source areas, and our site is located within
1,000 feet of both of those sites, one to the NW and one to the SE. If this will be needed, please let us know.
Thanks,
Al
Al Quarles I SENIOR PROJECT MANAGER I ATC Group Services LLC
Office + 1 704 529 3200 1 Direct [phone] Mobile + 1 803 984 6764
jrk
A
7606 Whitehall Executive Center Drive Suite 800 1 Charlotte, NC 28273
[e-mail] I www.atcgroupservices.com
This email and its attachments may contain confidential and/or privileged information for the sole use of the intended recipient(s). If
you are not the intended recipient, any use, distribution or copying of the information contained in this email and its attachments is
strictly prohibited. If you have received this email in error, please notify the sender by replying to this message and immediately
delete and destroy any copies of this email and any attachments. The views or opinions expressed are the author's own and may not
reflect the views or opinions of ATC.
From: Beverly, Trudy <[e-mail]>
Sent: Tuesday, December 10, 2019 7:18 AM
To: Al Quarles <[e-mail]>

Cc: Erin Greene <[e-mail]>
Subject: RE: [External] Tim Collins Property #40966 20Day Report and Draft NORP
Good Morning Al,
The report states that your receptor information was gathered from the Mecklenburg County Well Information
website. Did you have staff conduct a ground or car survey for wells within 150' of the release?
Thanks,
Trudy
e D- I E Q
'.a
.. iimen[o7~6,r.Yronmendt 6urar
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy.BeverlyL&ncdenr.gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: https:Hdeq.nc.Rov/about/divisions/waste-manavement/ust
Branch's Above Ground Storage Tanks Website Address: https://deq.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httns://deo.nc. gov/about/divisions/waste-mana gcmcnt/waste-management-rules-data/waste-management-gis-mans
File Review Procedures:
https://deq.nc. gov/about/divisions/waste-managemcnt/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
https://deq.nc.gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
https:Hfiles.ne.gov/ncdeq/Waste°/`2OManagement/DWM/UST/Corrective%2OAction/Electronic%2ODocument%20Submittal%2OMemo%2OUpdate.pdf
https://files. nc. gov/ncdeq/Waste°/`2OMana,gement/D WM/UST/Corrective%2OAction/UST%20file%20names%20for%2OLaserfiche. docx
From: Al Quarles [mailto:[e-mail]]
Sent: Monday, December 9, 2019 4:49 PM
To: Beverly, Trudy <[e-mail]>
Cc: Erin Greene <[e-mail]>
Subject: [External] Tim Collins Property #40966 20Day Report and Draft NORP
External email. Do not click links or open attachments unless you verify. Send all suspi
attachment to re ort.s am
Trudy,
See attached. We will mail the paper copy of the report and CD tomorrow. Can you review the draft NORP and
let me know if that is acceptable. I did remove the items of the NORP that do not apply (e.g., other portions of
the property or other properties affected, and the filing of a plat). I printed the figure to B&W and everything is
legible.
If the NORP is acceptable, we will have the RP sign and notarize the form and mail the original to you.
Thank you,

Al
Al Quarles I SENIOR PROJECT MANAGER I ATC Group Services LLC
Office + 1 704 529 3200 1 Direct [phone] Mobile + 1 803 984 6764
AV
jr
IrAT
7606 Whitehall Executive Center Drive Suite 800 1 Charlotte, NC 28273
al.quarles(a)atcas.com I www.atcciroupservices.com
This email and its attachments may contain confidential and/or privileged information for the sole use of the intended recipient(s). If
you are not the intended recipient, any use, distribution or copying of the information contained in this email and its attachments is
strictly prohibited. If you have received this email in error, please notify the sender by replying to this message and immediately
delete and destroy any copies of this email and any attachments. The views or opinions expressed are the author's own and may not
reflect the views or opinions of ATC.
From: Beverly, Trudy <[e-mail]>
Sent: Thursday, December 5, 2019 3:36 PM
To: Al Quarles <[e-mail]>
Cc: Erin Greene <[e-mail]>
Subject: RE: [External] UST-61 for 2640 Shenandoah Ave, Charlotte non-reg/non-comm heating oil UST - Tim
Collins Property #40966
Al,
Below is the name and site id information for home heating oil ust release at 2640 Shenandoah Ave., Charlotte.
Tim Collins Property
UST Number = MO-9531
Incident # = 40966
Trudy
From: Beverly, Trudy
Sent: Wednesday, December 4, 2019 11:51 AM
To: Al Quarles <[e-mail]>
Cc: Erin Greene <[e-mail]>
Subject: RE: [External] UST-61 for 2640 Shenandoah Ave, Charlotte non-reg/non-comm heating oil UST
Hey Al,
I haven't had a chance to add the site to the database yet. The name will be Tim Collins Property.
Thanks,
Trudy
From: Beverly, Trudy <[e-mail]>
Sent: Tuesday, December 3, 2019 7:50 AM
To: Al Quarles <[e-mail]>
Cc: Erin Greene <[e-mail]>
Subject: RE: [External] UST-61 for 2640 Shenandoah Ave, Charlotte non-reg/non-comm heating oil UST

Received. Thanks Al.
Have a great day,
Trudy
D�. E
RM f H QV"
Trudy Beverly, L.G.
Hydrogeologist, Division of Waste Management
North Carolina Department of Environmental Quality
UST Section, Mooresville Regional Office
704.235.2182 (Office)
Trudy. B ev erly(a),ncdenr. gov
Email correspondence to and from this address is subject to the
North Carolina Public Records Law and may be disclosed to third parties.
Office Mailing Address:
610 East Center Avenue, Suite 301
Mooresville, NC 28115
Branch's Underground Storage Tanks Website Address: hops://deg.nc.gov/about/divisions/waste-management/ust
Branch's Above Ground Storage Tanks Website Address: httqps://deg.nc.gov/about/divisions/waste-management/ust/ast-program
INTERACTIVE MAPS WITH DWM SITES AND PERMITTED FACILITIES:
httos://deu.nc. gov/about/divisions/waste-management/waste-management-rules-data/waste-management-gis-mans
File Review Procedures:
hops://deg.nc. gov/about/divisions/waste-manaaement/ust/file-review-procedures#mooresville-regional-office
ONLINE ACCESS TO UST SECTION DOCUMENTS (Laserfiche):
https://deq.nc.gov/about/divisions/waste-management/laserfiche
Document Submittal & UST File Names for Laserfiche Policies:
htips:Hfiles.nc. gov/ncdeq/Waste%20Management/DWMfUST/Corrective%2OAction/Electronic%2ODocument%2OSubmittal%2OMemo%2OUpdate.pdf
ht!Rs:Hfiles.nc. gov/ncdeg/Waste%20Management/DWM/UST/Corrective%2OAction/UST%2Ofile%20names%20for%2OLaserfiche.docx
From: Al Quarles [mailto:[e-mail]]
Sent: Tuesday, December 3, 2019 7:38 AM
To: Beverly, Trudy <[e-mail]>
Cc: Erin Greene <[e-mail]>
Subject: [External] UST-61 for 2640 Shenandoah Ave, Charlotte non-reg/non-comm heating oil UST
External email. Do not click links or open attachments unless you verify. Send all suspicious email as an
Kvibment to [e-mail]
Trudy,
See attached UST-61 Form (24-Hour Release and UST Leak Reporting Form) for the site you and I discussed
yesterday. Maps of the site location and soil sample locations are included along with the results of the initial
closure samples, collected on 11/8/2019. We are awaiting the results of over -excavation samples collected on
11/ 26/2019, and will follow-up with a letter report of the UST removal activities, and Notice of Residual
Petroleum if needed for a Notice of No Further Action.
If you have any questions, please contact us at your convenience.
Thank you,
a

Al Quarles I SENIOR PROJECT MANAGER I ATC Group Services LLC
Office + 1 704 529 3200 1 Direct [phone] Mobile + 1 803 984 6764
ATC
7606 Whitehall Executive Center Drive Suite 800 1 Charlotte, NC 28273
al.quarlesPatcgs.com I www.atcgroupservices.com
This email and its attachments may contain confidential and/or privileged information for the sole use of the intended recipient(s). If
you are not the intended recipient, any use, distribution or copying of the information contained in this email and its attachments is
strictly prohibited. If you have received this email in error, please notify the sender by replying to this message and immediately
delete and destroy any copies of this email and any attachments. The views or opinions expressed are the author's own and may not
reflect the views or opinions of ATC.