MO-7444_36096_CA_IAR_20191119_Initial Abatement Action Abatement Report Diesel Pump #20

I`
APEX
November 19, 2019
Ms. Trudy Beverly
Division of Waste Management
Mooresville Regional Office
Department of Environmental Quality
610 East Center Avenue, Suite 301
Mooresville, North Carolina 28115
RE: Initial Abatement Action Report
Pilot Travel Center #56
2825 Lane Street, Kannapolis, North Carolina
Groundwater Incident Number: 36096
Risk Classification: High
Dear Ms. Beverly:
Enclosed please find one copy of the Initial Abatement Action Report completed by Apex
Companies, LLC on behalf of Pilot Travel Centers, LLC for the referenced site. If you have any
questions regarding the enclosed material, or if additional material is required, please feel free to
contact me at [phone].
Sincerely,
e 7/
1z -��
Robert S. Wagner
Program Manager
Enclosure
cc: Mr. Joey Cupp, Pilot Flying J
WATER RESOURCES • ENVIRONMENTAL SERVICES • INDUSTRIAL HYGIENE • SAFETY
Apex Companies, LLC • 7724 Garland Circl
e

Prepared By:
i`
APEX
INITIAL ABATEMENT ACTION
REPORT
Pilot Station #56
2825 Lane Street
Kannapolis, North Carolina
Groundwater Incident Number: 36096
Risk Classification: High
Facility ID 0-011084
Submitted To:
Ms. Trudy Beverly
Division of Waste Management
610 East Center Avenue, Suite 301
Mooresville, North Carolina 28115
Prepared For:
Mr. Joey Cupp
Pilot Fling J
5508 Lonas Road
Knoxville, Tennessee 37939
Prepared By:
Apex Companies, LLC
7742 Garland Circle
Roanoke, Virginia 24019
November 19, 2019
Apex Project No.: 768490-030
Reviewed By:
Reviewed By:
Donald R. Smith, Jr. Robert S. Wagner Scott S. Huismann
Project Manager Program Manager North Carolina PE #23779
WATER RESOURCES • ENVIRONMENTAL SERVICES • INDUSTRIAL HYGIENE • SAFETY • AIR QUALITY • SUSTAINABILITY AND CLIMATE CHANGE
Apex Companies, LLC • 7724 Garland Circle • Roanoke, VA 24019
T 540.563.4920 • F 540.563.4921 • apexcos.com

TABLE OF CONTENTS
A.
SITE INFORMATION..................................................................................................... 1
B.
SITE HISTORY AND CHARACTERIZATION.......................................................... 3
C.
SITE CHECK REPORT...................................................................................................4
D.
UST CLOSURE REPORT................................................................................................4
E.
NAPL INVESTIGATION AND FREE PRODUCT RECOVERY REPORT .............4
F.
GROUNDWATER AND SURFACE WATER INVESTIGATION .............................4
G.
INITIAL RESPONSE AND ABATEMENT ACTION..................................................7
H.
EXCAVATION OF CONTAMINATED SOIL..............................................................7
I.
CONCLUSIONS AND RECOMMENDATIONS...........................................................7
List of Tables
Table 1.
UST Owner and Operator Information
Table 2.
Current and Historical UST Information
Table 3.
Groundwater Elevation Data
Table 4.
Summary of Soil Analytical Results
Table 5.
Soil VPHIEPH Worksheet
Figure 1. Site Location Map
Figure 2. Site Map
List of Figures
List of Appendices
Appendix A Site Check Report
Appendix B Soil Boring Log and Monitoring Well Completion Diagram
Appendix C Laboratory Certificate of Analysis and Chain -of -Custody Records
IAA Report i November 19, 2019
Pilot #56

A. SITE INFORMATION
1. Site Identification
• Date of Report: November 18, 2019
• Facility Identification Number: 0-011084
• Incident Number: 36096
• Site Risk/Priority Rank: High
• Site Name: Pilot Station #56 (site)
• Site Street Address: 2825 Lane Street, Kannapolis, Cabarrus County, North
Carolina.
• Geographical Data Point: Store Building
Google Earth Pro
• Latitude 350 29' 53.20" N and Longitude -800 33' 39.54"W
A site location map is included as Figure 1 to this report.
2. Information about Contacts Associated with the Underground Storage Tank
(UST) System
• UST Owner: Pilot Travel Centers, LLC
5508 Lonas Drive, Knoxville, TN 37909
Phone: [phone]
• UST Operator: Pilot Travel Centers, LLC
5508 Lonas Drive, Knoxville, TN 37909
Phone: [phone]
• Property Owner: Pilot Travel Centers, LLC
5508 Lonas Drive, Knoxville, TN 37909
• Property Occupant: Pilot Travel Centers, LLC
2825 Lane Street, Kannapolis, North Carolina
• Consultant/Contractor: Apex Companies, LLC
7724 Garland Circle, Roanoke, Virginia 24019
Phone: [phone] Facsimile: 540-563-4921
• Analytical Laboratory: Pace National #375
12065 Lebanon Road, Mount Juliet, TN 37122
Phone: [phone]
3. Information about the Release
• Date Discovered: August 20, 2019
• Estimated Quantity of Release: Unknown
• Cause of Release: Fuel weep under diesel dispenser #20.
• Source of Release: Diesel dispenser #20.
• Size and Contents of UST System(s) from which release occurred: See Table
2.
IAA Report 1 November 19, 2019
Pilot #56

4. Certification (The title page must display the seal and signature of the certifying P.E.
or L.G. and the name and certification number of the company or corporation [See
15A NCAC 2L .0103(e).[)
I, Scott S. Huismarm a rofessional Engineer icensed Geologist (circle one) for Maryland Apex
Engineering, PC, an affiliate o S.
LLC, do certify that the information contained in
this report is correct and accurate to the best of my knowledge.
(Please Affix Seal and Signature) <%A CAR
EAL
237 9
=
i►�ig310 :_ -
PC, an affiliate of Apex Companies, LLC, is licensed to practice
one or both) in North Carolina The certification number of the
is C-3073
IAA Report November 18, 2019
Pilot #56

B. SITE HISTORY AND CHARACTERIZATION
1. Provide UST Owner and Operator Information
See Table 1.
2. Provide UST Information
See Table 2.
3. Provide Non -UST Information
In a review of the North Carolina Department of Environmental Quality (NCDEQ), it
was learned that a surface spill occurred at the property on February 8, 2012 due to a
third -parry truck releasing approximately 75 gallons of diesel fuel in the parking lot
due to a damaged fuel tank. The release was contained to the parking lot/asphalt and
cleaned up by emergency response contractors. A 24-Hour Release Form was
submitted to NCDEQ and the incident was issued AST Incident #91187. No further
activities were required by NCDEQ.
4. Provide Description of Release and Relationship to Historical Releases
The release was discovered on August 20, 2019 during compliance inspection for the
facility. A fuel weep was observed beneath diesel dispenser #20. The estimated
quantity of product released is unknown, but minimal since the leak detection
methods for the facility did not detect an issue.
The referenced facility has reportedly been a retail fuel outlet since at least 1984.
From 1966 to 1972, the site was owned and operated by Humble Oil Company. In
1972, retail fuel operations and property ownership was transferred to Exxon
Corporation due to a name change. In 1984, the property was the site of a Starvin
Marvin and at some point in time; Speedway America took over operations until
October 26, 2001 when Pilot Travel Centers, LLC (Pilot) purchased the property.
During May 1994, underground storage tank (UST) closure activities were conducted
in which seven USTs were removed from the property. It was also noted at that time
that two 12,000-gallon USTs were removed from service in 1991. A release was
noted during these activities and UST incident #6379 was assigned. Following
active remediation activities in 1998, the incident was closed by NCDEQ.
In April 2006, prior to well abandonment activities for wells associated with UST
incident #6379, free product (gasoline) was gauged in two on -site monitoring wells.
The source of free product was determined to be a leaking product line. NCDEQ
considered the presence of free product to be an indication of a new release and UST
incident #36096 was assigned.
IAA Report November 19, 2019
Pilot #56

Since 2006, several phases of assessment have been performed. The site was ranked
"high risk" due to the presence of water supply wells within 1,000 feet of the source
area. An active remediation system (air sparge/soil vapor extraction (AS/SVE)) was
placed into operation at the site on April 18, 2012 and is currently active.
5. Provide a Brief Description of Site Characteristics
The subject property consists of one convenience store building and petroleum
fueling equipment. The subject property and surrounding area are fairly level. The
subject property is located in a commercial, residential, and industrial area. Public
water is supplied to the property and area; however, water supply wells are present
within 1,000 feet of the property as reported by others in reports on file at the
NCDEQ Mooresville Regional Office. A topographic map and site map are attached
as Figures 1 and 2, respectively.
6. Summarize Initial Abatement Actions to Date
Refer to Site Check Report provided as Appendix A.
C. SITE CHECK REPORT
Refer to Site Check Report provided as Appendix A.
D. UST CLOSURE REPORT
UST closure was not conducted during this phase.
E. NAPL INVESTIGATION AND FREE PRODUCT RECOVERY REPORT
NAPL was not detected during this phase.
F. GROUNDWATER AND SURFACE WATER INVESTIGATION
1. Soil Boring Activities
Apex performed a subsurface investigation at the site on October 23, 2019 to assess the
presence or absence of petroleum compounds in soil in response to the diesel fuel weep at
dispenser #20. During the investigation, one soil boring was drilled and converted to
monitoring well MW-AL The soil boring location was selected based on the proximity to
dispenser #20 and existing site monitoring wells. Prior to advancement of the soil boring,
Apex conducted a ground penetrating radar (GPR) survey of the DEQ-approved area
proposed for soil boring and monitoring well installation. The GPR survey was conducted to
IAA Report ' November 19, 2019
Pilot #56

assist with identifying private utilities that are not marked in accordance with standard One
Call Utility protocol. Apex also utilized vacuum extraction soft dig techniques to physically
clear the boring to a depth of five feet.
Soil borings SB-1 was drilled using a track -mounted Geoprobe drill rig equipped with
continuous -flight, hollow -stem augers with an internal diameter (I.D.) of 4.25 inches.
Hollow -stem auger drilling methods were utilized to collect split -spoon soil samples and to
facilitate monitoring well construction upon completion of the borings. Two-inch diameter,
24-inch long split -spoon samplers were used to collect subsurface soil samples at five-foot
minimum intervals during drilling. Drilling and split -spoon sampling were conducted in
accordance with ASTM-D-1586-87 protocol. Contact downhole drilling equipment (hollow -
stem augers, drill rods) was decontaminated prior to drilling using a steam cleaner with a
design discharge of 180°F. Sampling equipment was decontaminated between each sample
interval using a phosphate -free detergent solution and water rinse. The boring was advanced
to a depth of 30 feet. Disposable latex gloves were used during all phases of sample
collection. A soil boring log is included as Appendix B. Drill cuttings generated during soil
boring activities were placed in 55-gallon steel drums. The monitoring well location is
depicted on Figure 2.
2. Groundwater Monitoring Well Construction
Apex completed soil boring SB-1 as monitoring well MW-A1. The monitoring well location
is depicted on Figure 2. The groundwater monitoring well was installed to a depth of 30 feet
to collect groundwater samples, perform aquifer testing, and to monitor for the presence of
free -phase petroleum product accumulation. The groundwater monitoring well was
constructed of two-inch I.D. schedule 40 PVC casing and 0.010-inch factory -slotted well
screen. All screen and casing was flush -threaded and equipped with "O" rings to prevent
leakage at j oints. End caps for the screened intervals consisted of threaded well points. The
well is equipped with an expansion -type locking well cap. The well annulus was filled with
washed, #2 quartz filter sand. Apex brought the sand pack up to approximately one foot
above the top of the screened interval. A pelletized bentonite seal was placed above the sand
filter pack and hydrated with potable water. The remainder of the annulus was completed
with neat portland grout and a flush -mount protective well cover cemented at the ground
surface. A monitoring well construction diagram is included on the boring logs provided as
Appendix B. The well was developed by the North Carolina licensed well driller at the
completion of monitoring well construction.
3. Hydrogeology
Apex completed one soil boring at the site as groundwater monitoring well. A mark placed
on the top of each well casing was used as a reference point for surveying and recording
groundwater elevations. Apex used a SolinstTM electronic interface probe to measure the
depth to groundwater and investigate for the presence of free -phase petroleum product prior
to purging and sampling. During this phase, another well was identified on the western side
of the diesel fueling island adjacent to dispenser #20. This well was labeled MW-A2 by
Apex staff. Later it was confirmed as air sparge well AS-8 associated with the existing
IAA Report November 19, 2019
Pilot #56

remediation system. A summary of the results of the groundwater elevation data from
October 23, 2019 are presented in Table 3. Free -phase petroleum product was not detected
in either of the monitoring wells during this phase. Based on historical reports for the site,
shallow groundwater flow at the site is to the northwest.
4. Vapor -Phase
Headspace analyses of soil samples collected during advancement of the soil boring was
conducted using an Industrial Scientific VX 500 photoionization detector (PID) calibrated to
100 parts per million (ppm) isobutylene. This instrument is capable of detecting volatile
organic compound (VOC) vapors, typically associated with petroleum fuels, ranging
between 0.1 ppm and 5,000 ppm. Headspace monitoring of the equilibrated soil samples
collected during soil boring advancement yielded VOC vapor concentrations ranging from
below 0.1 ppm to 573 ppm at a depth of 30 feet. Headspace values of each interval are also
included on the boring log provided as Appendix B.
5. Adsorbed -Phase
During drilling of the monitoring well, soil samples were retained for laboratory analyses
based on headspace values, field observations and drill cuttings, boring location, and depth
of sample. The sample was labeled and stored on ice pending delivery to Pace National
(Pace) in Mount Juliet, Tennessee for volatile organic compound (VOC) analysis via method
8260B, semi -volatile organics (SVOC) analysis via method 8270D, MADEP volatile
petroleum hydrocarbons (VPH) analysis via U.S. EPA SW-846 method 5035, and
extractable petroleum hydrocarbon (EPH) analysis via U.S. EPA SW-846 method 3550B.
Strict sample security and chain -of -custody documentation were observed during all phases
of transport. Adsorbed -phase analytical results yielded VPH and EPH concentrations above
the NCDEQ Soil -to -Water Maximum Contaminant Concentrations, but below their
respective Residential soil cleanup levels. All VOC and SVOC concentrations were below
their respective NCDEQ Soil -to -Water Maximum Contaminant Concentrations. VOC and
SVOC analytical results as compared to NCDEQ cleanup levels are presented in Table 4.
The VPH and EPH MADEP soil worksheet is provided as Table 5. The soil laboratory
Certificate of Analysis and chain -of -custody records are provided in Appendix C.
6. Dissolved -Phase
On October 23, 2019, Apex personnel collected groundwater samples from monitoring wells
MW-Al and MW-A2/AS-8. Prior to sampling, Apex purged all monitoring wells to collect
samples representative of aquifer conditions. Each monitoring well was purged until a
minimum of three well volumes had been displaced. Groundwater samples were collected
using dedicated, disposable high -density polyethylene bailers and were transferred directly
into the appropriate sample containers. Clean, disposable latex gloves were used during all
phases of sample collection. The samples were labeled and stored on ice pending delivery to
Pace for analysis. The groundwater samples were submitted for VOC, SVOC, and MADEP
VPH and EPH analysis. Analytical results did not yield petroleum compounds above
laboratory method detection limits in either of the monitoring wells. Strict sample security
IAA Report ° November 19, 2019
Pilot #56

and chain -of -custody documentation were observed during all phases of transport. The
laboratory Certificate of Analysis and chain -of -custody records are provided as Appendix C.
G. INITIAL RESPONSE AND ABATEMENT ACTION
Refer to Site Check Report provided as Appendix A.
H. EXCAVTION OF CONTAMINATED SOIL
Soil excavation did not occur during this phase.
I. CONCLUSION AND RECOMMENDATION
Apex has completed IAA Report activities in accordance with NCDEQ-directives at
the Pilot 56 facility in Kannapolis, Cabarrus County, North Carolina. Adsorbed -phase
analytical results yielded VPH and EPH concentrations above the NCDEQ Soil -to -Water
Maximum Contaminant Concentrations, but below their respective Residential soil cleanup
levels. All VOC and SVOC concentrations were below their respective NCDEQ Soil -to -
Water Maximum Contaminant Concentrations. Dissolved -phase analytical results did not
yield petroleum compounds above laboratory method detection limits in either of the
monitoring wells. Based on the data collected and presented during this phase, Apex
recommend no further action regarding the release at dispenser #20. This report of findings,
prepared in accordance with the NCDEQ approved scope of work, is being delivered to Ms.
Trudy Beverly of NCDEQ on behalf of Pilot.
IAA Report November 19, 2019
Pilot #56

TABLES

TABLE 1
UST OWNER AND OPERATOR INFORMATION
PILOT TRAVEL CENTERS 056
2825 LANE STREET
KANNAPOLIS, CABARRUS COUNTY, NORTH CAROLINA
Revision Date: 11/12/19 Incident Number and Name: 36096 Pilot #56
UST ID Number
All
Facility ID Number
00-0-0000011084
Owner Name (and Contact)
Dates of Operation (mm/dd/yy to mm/dd/yy)
Pilot Travel Centers, LLC
2001 to Present
Street Address
5508 Lonas Road
City
State
Zip
Telephone Number
Knoxville
TN
37909
865-474-3106
Operator Name (and Contact)
Dates of Operation (mm/dd/yy to mm/dd/yy)
Same as above
Street Address
City
State
Zip
Telephone Number

Table 2.
Current and Historical UST Information
Description
Was release
UST ID
Current/Last
Previous
Capacity
Construction
Tank
of Associated
Date Tank
Status of
associated
Number
Contents *
Contents *
(in gallons)
Details **
Dimensions
Piping and
Installed
UST ***
with the UST
Pumps
System?
1
Kerosene
Unknown
3000
Steel,
UNK
steel, single
1983
Removed
Yes
Single wall
wall piping
1994
2
Premium
Unknown
8000
Steel,
UNK
steel, single
1983
Removed
Yes
Unleaded
Single Wall
wall piping
1994
3,4
Reg.
Unknown
12000
Steel,
UNK
steel, single
1983
Removed
Yes
Unleaded
(each)
Single Wall
wall piping
1994
*out ofservice
in Oct 1991
5
Diesel
Unknown
20000
Steel,
UNK
steel, single
1983
Removed
yes
Single Wall
wall piping
1994
6
Oil/Water
3000
Steel,
UNK
steel, single
1983
Removed
yes
separator
Single Wall
wall piping
1994
G
Mid grade
Unknown
10000
Steel,
UNK
steel, single
03/03/92
Removed
no
unleaded
Single Wall
wall piping
1994
H
Reg
Unknown
15000
Steel,
UNK
steel, single
03/03/92
Removed
no
unleaded
Single Wall
wall piping
1994
A
Auto
Kerosene
4000
Steel,
UNK
steel, single
06/30/94
Currently
Unknown
Diesel
Single Wall
wall piping
Operational
B
Unleaded
Unleaded
10000
Steel,
UNK
steel, single
06/30/94
Currently
Unknown
Gasoline
Gasoline
Single Wall
wall piping
Operational

Table 2 (Cont'd.)
Current and Historical UST Information
Description
Was release
UST ID
Current/Last
Previous
Capacity
Construction
Tank
of Associated
Date Tank
Status of
associated
Number
Contents *
Contents *
(in gallons)
Details **
Dimensions
Piping and
Installed
UST ***
with the UST
Pumps
System?
C
Unleaded
Unleaded
15000
Steel,
UNK
steel, single
06/30/94
Currently
Unknown
Gasoline
Gasoline
Single Wall
wall piping
Operational
D
Diesel
Diesel
20000
Steel,
UNK
steel, single
06/30/94
Currently
Unknown
Single Wall
wall piping
Operational
E
Diesel
Diesel
20000
Steel,
UNK
steel, single
06/30/94
Currently
Unknown
Single Wall
wall piping
Operational
F
Used Oil
Used Oil
4000
Steel,
UNK
steel, single
06/30/94
Currently
Unknown
Single Wall
wall piping
Operational

Table 3.
Groundwater Elevation Data
October 23, 2019
Monitoring/ Air
Date
Well Casing
Well Depth
Screened
Depth to
Sparge Well
Installed
Diameter
(feet)
Interval
Water
Location
(inches)
(feet)
feet
MW-Al
Oct-2019
2
30
10-30
20.21
MW-A2/AS-8
Dec-2011
2
44
42-44
20.85
' Top of casing elevation based on assumed site datum from Concord USGS map of 740.00 feet.

Table 4.
Summary of Soil Analytical Results
Parameter'
SB-1
(30 feet)
Industrial/
Commercial
MSCCs
( m)
Soil -to -Water
Maximum
Concentration
(PPTL
sec-Butylbenzene (mg/kg)'
0.0197
16,350
3.3
2-Butanone (MEK) (mg/kg)
0.0307
245,280
16
Acenaphthene (mg/kg)3
0.0343
24,00
8.2
Naphthalene (mg/kg)
0.0344
8,176
0.16
Phenanthrene (mg/kg)
0.167
12,264
56
Pyrene (mg/kg)
0.0631
12,264
270
' Only parameters with detectable hits are listed.
2 VOC analysis by U.S. EPA method 826013, reported in milligrams per kilogram (mg/kg).
3 Semi-VOCs analysis by U.S. EPA method 8270D, reported in milligrams per kilogram (mg/kg).

Table 5.
Soil VPH and EPH Worksheet
Laboratory
Final VPH
Residential
Industrial/
Soil -to -
Boring
Contaminant
Analytical
Hydrocarbon
Analytical Hydrocarbon
Results
and/or EPH
MSCC
Commercial
Groundwater
Location
Method
Fraction Ranges
Fractions
Concentration
Concentration
(mg/kg)L=g)
C
MSCC
(mg/kg)
(m /k)
(mg/kg)
C5-C8 Aliphatics
C5-C8 Aliphatics
VPH
<5.00
<5.00
939
24,528
68
C9-C 18
C9-C 12 Aliphatics
VPH
12.5
MADEP
Aliphatics
p
61.6
1,500
40,000
540
C9-C18 Aliphatics
EPH
49.1
SB-1
Gasoline and
VPH' and
C19-C36
C19-C36 Aliphatics
EPH
18.7
18.7
31,000
810,000
Considered
(30 feet)
Diesel Fuel
MADEP
EPH'
Aliphatics
Immobile
C9-C22
C9-C 10 Aromatics
VPH
6.17
Aromatics
56.37
469
12,264
31
C11-C22 Aromatics
EPH
50.2
' VPH analysis by method MADEP 5030B, reported in milligrams per kilogram (mg/kg).
2 EPH analysis by method MADEP 3510C, reported in milligrams per kilogram (mg/kg).

FIGURES

FIGURE I
Site Location Map
Former Pilot #56
2825 Lane Street
Kannapolis, Cabarrus County, North Carolina
�5 ' ._,T', f�f-_-'y -+ ''�i ~l j� lJ .•4. +' _ w
Tea ilef
cask �K f£ _ :✓ 'y Jam`' J f ,l 1� _•
�' � — _F _'�L - f �%, 7 .�4 _ _f - '�' • y ,'S• 5_ { Y r—� —�=�_—_=_34 _— 1
`'^■'t'C -t�J'
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low
`� ` � !a_.* i � v l __ . 5�-.,--•}r r.'y r r. i. ll. r '-.� ^` �-,� ��' ; i f .- _-�`y '
Flo Y
F * � ram.■ ■ M 652 ' l Di Ct1QI1
':� � 1 'Ct _ — � • ` ! ems' ' . • �`'� �i - I ,� , .
{ ,
3' aye -j\J Keiser CR*
er`
) _ 4
1 '' t 7
5 l W04
..
,.1`
of rIC RIP
r.s - -� _.s—, �si`�,� / 7 �3�. •�,'J
0" �l ?�'+fJ� i ti. • �{�'r ILIYE� ' 1•R"'' l' -.f� f-5 7 ' l
-�Ch
•5,■ •.,I ti � �'.� ��6.5' f tom+ " ,� � I ��_i �"� .o�. ��.i � � � - l�
7724 Garland Circle CONCORD, NORTH CAROLINA Project: IAA Report '
Roanoke, VA 24019
Telephone: [phone] Client: Pilot Flying J
Source: U.S.G.S. Topographic Map of the
Concord Quadrangle, North Carolina, �y
7.5 Minute Series (1991) Apex Job #: 768490.030 Latitude:
Scale: 1:24,000 Contour Interval: 10 Feet
Vertical Datum: National Geodetic Longitude:
'3.20N
� Vertical Datum 1929 Date: November 2019 Longitude:
Horizontal Datum: North American Datum1927 -080e 33' 39.54" W

•
DIESEL FUEL
DISPENSER ISLkND
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DR.: DRY
DATE: Nov. 2019
IAA
Report
Incident #31
CK.: CLC
APPD.: RSW
SCALE:
APEX PROJ. NO.: 76M90.030
www.apexcos.com
220441
PAVED
GRASS
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Monitoring Well Location Map
Pilot Station #56
APEX
2825 Lane Street
Kannapolis, North Carolina
7724 Garland Circle
Roanoke, VA24019
Phone:[phone]
FIGURE No. 2
A

APPENDIX A
Site Check Report

A L
AV C
X4T
ENVIRONMENTAL - AEOTECHNICAi
BUILURNG SCIENCES • MATERIALS TESTING
September 3, 2019
Mr. Jack Stutts, UST Inspector
North Carolina Department of Environmental Quality
Division of Waste Management — UST Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646
Ms. Trudy Beverly, L.G.
North Carolina Department of Environmental Quality
Division of Waste Management — UST Section
Mooresville Regional Office
610 East Center Avenue, Suite 301
Mooresville, North Carolina 28115
Re: Site Check Report
Pilot Travel Centers 056
2825 Lane Street
Kannapolis, Cabarrus County, North Carolina
NCDEQ Facility ID #00-0-0000011084
609A Piner Road., Suite 115
Wilmington, North Carolina 28409
Telephone [phone]
Fax [phone]
www.atcgroupservices.com
Dear Mr. Stutts and Ms. Beverly:
ATC Associates of North Carolina, LLC (ATC), on behalf of Pilot Travel Centers, LLC, is submitting this Site
Check Report for the referenced facility.
If you have any questions or require additional information, please contact our office at [phone].
Sincerely,
ATC Associates of North Carolina, LLC
qylljx�
Maureen Jackson, P.G.
Senior Project Manager
cc: Pilot Travel Centers, LLC
/A-FWL�
Max Burmeister
Program Manager

SITE CHECK REPORT
PILOT TRAVEL CENTERS 056
2825 Lane Street
Kannapolis, Cabarrus County, North Carolina
NCDEQ Facility ID #00-0-0000011084

Pilot Travel Centers 056
NCDEO Facility ID 9004MMI 1094
September 3. 2019
Site Check Remit
Site Check Report
A. Site Information
1. Site Identification
Daze of Report: OS120119
Facility ID #: 00-0-0000011084 UST Incident N 36096(Oneoina Remndistion)
Site Name: Pilot Travel Centers 056
Site Street Address: 2825 lane Street
City/Town: Kannaoolis Zip Code: 28081 County: Call —
Description of Geographical Data Point: C-store Building
Location Method: Gooale Earth
Latitude: 35029'53.20" N Longitude 80033'39.54"
Information About Contacts
UST Owner and Operator. Pilot Travel Comm LLC
Address: 5508 Lonas Road Knoxville, Tennessee 37909 Tel: [phone]
Property Owner: Pilot Travel CentersLLC
Address: 5508 Lonas Road Knoxville, Tennessee 37909
Property Occupant Pilot Travel Centers 056
Address: 2825 Lane Street Known lis. North Carolina 28081
ConsulnndConmactor. ATC Associates of North Carolina, P.C.
Address: 609A Piner Road. Suite 115 Wilminmon. North Carolina 28409 Tel: [phone]
Analytical Laboratory: Pace Analytical Cen h: 375
Address: 12065 Lebanon Road Mt. Juliet. Tennessee 37122 Tel: [phone]
3. Information About Release
Date Discovered: August 20. 2019
Estimated Quantity of Release: Unknown
Cause of Release: Fuel wcep under diesel dispenser N20
Some of Release: Diesel Dispenser 420
Sim and Contents of UST System: See Table 2
Complete and Include In reW*JFJF M*1)� q`gh H in the order listed.
1. Maureen A. Jackson of pri e . Geologist ircle one) fur ATC Associates of
North Carolina. P.C. do is report is correct and accurate to the
best of my knowledge. ' ��•„ -_
(Please Affix Seal and Si ULO�
FN .:^ (:ns
A. 3:
A01
TC Associates of North Carolina. pi"ol) licensedu)prectic eolugylengineerin 2ireleoneorland)in
North Carolina The certification number of the company or corpora
ATC Associates of Noah Camellia

Pilot Travel Centers 056
NCDEQ Facility ID #00-0-0000011084
B. Site History
1. Provide UST Owner and Operator Information
See Table 1.
2. Provide UST Information
See Table 2.
3. Provide Non -UST Information
September 3, 2019
Site Check Report
In a review of the North Carolina Department of Environmental Quality (NCDEQ), it was
learned that a surface spill occurred at the property on February 8, 2012 due to a third party
truck releasing approximately 75 gallons of diesel fuel in the parking lot due to a damaged fuel
tank. The release was contained to the parking lot/asphalt and cleaned up by emergency
response contractors. A 24-Hour Release Form was submitted to NCDEQ and the incident was
issued AST Incident #91187. No further activities were required by NCDEQ.
4. Describe relation of location of current UST system to historical UST releases.
The referenced facility has reportedly been a retail fuel outlet since at least 1984. From 1966 to
1972, the site was owned and operated by Humble Oil Company. In 1972, retail fuel operations
and property ownership was transferred to Exxon Corporation due to a name change. In 1984,
the property was the site of a Starvin Marvin and at some point in time; Speedway America
took over operations until October 26, 2001 when Pilot Travel Centers, LLC purchased the
property.
During May 1994, underground storage tank (UST) closure activities were conducted in which
seven USTs were removed from the property. It was also noted at that time that two
12,000-gallon USTs were removed from service in 1991. A release was noted during these
activities and UST incident #6379 was assigned. Following active remediation activities in
1998, the incident was closed by NCDEQ.
In April 2006, prior to well abandonment activities for wells associated with UST incident
#6379, free product (gasoline) was gauged in two on -site monitoring wells. The source of free
product was determined to be a leaking product line. NCDEQ considered the presence of free
product to be an indication of a new release and UST incident #36096 was assigned.
Since 2006, several phases of assessment have been performed. The site was ranked "high
risk" due to the presence of water supply wells within 1,000 feet of the source area. An active
remediation system (air sparge/soil vapor extraction (AS/SVE)) was placed into operation at the
site on April 18, 2012 and is currently active.
ATC Associates of North Carolina

Pilot Travel Centers 056
NCDEQ Facility ID #00-0-0000011084
5. Provide a Brief Description of Site Characteristics
September 3, 2019
Site Check Report
The subject property consists of one convenience store building and petroleum fueling
equipment. The subject property and surrounding area are fairly level. The subject property is
located in a commercial, residential, and industrial area. Public water is supplied to the
property and area; however, water supply wells are present within 1,000 feet of the property as
reported by others in reports on file at the NCDEQ Mooresville Regional Office. A
topographic map and site map are attached as Figures I and 2, respectively.
C. Site Check Procedures
1. UST System Testing
On June 5, 2019, during a NCDEQ UST compliance inspection, liquid was noted in the
contaminant sump under diesel dispenser #20. On June 5, 2019, a Notice of Violation (NOV)
was issued to Pilot Travel Centers (Pilot) for these noted conditions. A UST-17B UST
Suspected Release 7-Day Notice was submitted. On June 14, 2019, SPATCO personnel
repaired a loose entry boot. Following the repair, the containment sump was hydrostatically
tested and passed. A UST-6D/23A Triennial UST Spill Bucket Integrity Testing form was
submitted to NCDEQ on June 14, 2019. On August 20, 2019, upon receipt of the laboratory
analytical results, ATC personnel submitted a UST-61 24-Hour Release and UST Leak
Reporting Form to NCDEQ.
Copies of the referenced notifications are provided in Attachment I.
2. Site Check Procedure
On August 9, 2019, ATC personnel contracted with Dewberry to air knife a soil boring adjacent
to diesel dispenser #20. The soil boring for SB-1 was air knifed to 5 feet below ground surface
(bgs). Groundwater was not encountered in the soil boring. ATC personnel collected a soil
sample at the termination depth for laboratory analysis. The location of the soil sample is
provided on Figure 2.
3. Soil Excavation Activities
Soil excavation was not performed as part of this site check.
D. Site Investigation
1. Field Screening
Soil sample SB-1 was screened with a photoionization detector (PID). The respective PID
reading is provided on Table 3.
2. Soil Sampling Information
Soil sample SB-1 was collected at an approximate depth of 5 feet bgs. The soil encountered at
the respective sampling depth was noted to be gray to green sandy silt with a strong petroleum
odor. Groundwater was not encountered during site check activities.
The soil sample was shipped to a N.C. certified laboratory in a chilled cooler following proper
chain -of -custody procedures. Soil sample SB-1 was requested to be analyzed by Total
ATC Associates of North Carolina

Pilot Travel Centers 056
NCDEQ Facility ID #00-0-0000011084
September 3, 2019
Site Check Report
Petroleum Hydrocarbons (TPH) — Gasoline Range Organics and TPH — Diesel Range Organics
(TPH-DRO).
3. Groundwater and Surface Sampling Information
Groundwater samples and surface water samples were not collected.
4. Quality Control Measures
The soil sample was placed in laboratory provided jars and vials. The sample was immediately
placed on ice and contained in a cooler during transportation. The sample was then transported
by courier under a chain -of -custody to the laboratory for analysis.
5. Investigation Results
Laboratory analytical results of the soil sample detected a TPH-DRO concentration above its
established State Action Level. The results are shown in Table 3. A copy of the laboratory
report and chain -of -custody documents are provided in Attachment IT
E. Conclusion and Recommendations
Laboratory analytical results of the soil sample detected a TPH-DRO concentration above its
established State Action Level. Based on the soil analytical data, it appears a release of
petroleum has occurred from diesel dispenser #20.
F. Figures
Figure 1 — Topographic Map
Figure 2 — Site Map
G. Tables
Table 1 — UST Owner and Operator Information
Table 2 — UST/AST System Information
Table 3 — Soil Analytical Results
H. Attachments
I — Notifications and Testing Results
II — Soil Laboratory Report and Chain -of -Custody Documents
ATC Associates of North Carolina

FIGURES

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TABLES

TABLE I
UST OWNER AND OPERATOR INFORMATION
PILOT TRAVEL CENTERS 056
2825 LANE STREET
KANNAPOLIS, CABARRUS COUNTY, NORTH CAROLINA
Revision Date: 8/20/2019 Incident Number and Name: Pilot Travel Centers 056
UST ID Number
All
Facility ID Number 00-0-0000011084
Name of Owner
Dates of Operation (MM/DD/YY to MM/DD/YY)
Pilot Travel Centers, LLC
2001 to Present
Street Address
5508 Lonas Road
City
I State
Zip
ITelephone Number
Knoxville
ITN
37909
865-474-3106
Name of Operator
Dates of Operation (MM/DD/YY to MM/DD/YY)
As Above
Street Address
City
I State
Izip
ITelephone Number

TABLE 2
UST/AST SYSTEM INFORMATION
PILOT TRAVEL CENTERS 056
2825 LANE STREET
KANNAPOLIS, CABARRUS COUNTY, NORTH CAROLINA
Revision Date: 8 20 2019 Incident Number and Name: Pilot Travel Centers 056
UST ID Numberl
Current/Last
Contents
Previous
I Contents
Capacity
(gallons)
Construction
Details
Tank
Dimensions
Description of
Associated
Piping and
Pumps
Date Tank
Installed
Status of UST
Was Release
Associates with
the UST System?
1
Gasoline
None
15,000
Unknown
STiP3
FRP
Unknown
Active
Unknown
2
Gasoline
None
10,000
Unknown
STiP3
FRP
Unknown
Active
Unknown
3
Auto Diesel
None
5,000
Unknown
STiP3
FRP
Unknown
Active
Unknown
4
Diesel
None
20,000
Unknown
STiP3
FRP
Unknown
Active
Unknown
5
L
Diesel
None
20,000
Unknown
STiP3
FRP
Unknown
Active
Unknown
r
Description of
Associated
Was Release
Current/Last
Previous
Capacity
Construction
Tank
Piping and
Date Tank
Associates with
AST ID Number
Contents
Contents
(gallons)
Details
Dimensions
Pumps
Installed
Status of AST
the AST System?
None associated with this site

TABLE 3
SOIL ANALYTICAL RESULTS
PILOT TRAVEL CENTERS 056
2825 LANE STREET
KANNAPOLIS, CABARRUS COUNTY, NORTH CAROLINA
Analytical Method
EPA Method 8015
PID
A
Reading
x
x
Sample
Depth feet
m
Date Sampled
Cam-
H
SB-1
5
452.5
8/9/2019
48.7
4,890
State Action Level
50
100
Notes:
1. Concentrations reported in milligrams per kilogram (mg/kg).
2. Bold type denotes concentration exceed the State Action Level.

ATTACHMENT

UST.61
24-Hour Release and UST Leak Reporting Form.
For Releases This loan should be CNnolelPA aM submJlb la the UST SediunsregiDu"Oh'ce lollovnng a known w suspetletl release from
eo undergaund soage lank DST) syvlem. This tom+ is noosed tO be submetee Within2a hours of discovery of a known a
In NC so
release
(DWM USE ONLYt
IwJUenl# Reek(l4j,4U)_
SUSlaeded 2011lemmaew9 IYIN) Y
Confirmed GW Conlaminsul tym-F
Fatlllly ID Numher 00L-00b001 ION
pale leak Discovered
Recelvetl On Recalveb By _
Reported by lc/ncleowy Phone. Faxes Report
Confirmed Sal Cwtamvavor 1( nk) N.
SamPles Taken>(YINt Y
�gI30/19
CPTMNOhCammarcian
ReWiNon+egulaed'+ Ree
Reglw
Free ptodlCYMI N I(YPssualectisbael
Try[Itnass
INCIDENT DESCRIPTION
IMdent Name
Pilot Tnval Cantata O50
AJtlress' U25 Laos Street
County- Csbxrrus
Clly?avn' ➢ Cotle-
Wnnvpolls F - 280tlt
Rajlonal OOke (time One): Rankles Mowesvll* arseze.
Refth, Washington Wllmntlan. Wins
Lathkal Cewl ewnO 3%029-5310"N LOnBllude laws .). W33'3954"W
Obviincd by:
❑�
BneflY deecribesuspededamnMneb reloaee;/llKlutlin9Ouf mflimiledro nxule of crease, Cafe almlwe. amoum
OITJeaae em0enf
a//TP YCI mSel)(erida nflan Ml(IaIT BS [DIMY[{ed,i e(E ie once (pa
Iv❑1TppagaPhm cep
a ento.Y envy ¢a resu o •mr exmpew me x yeas 0 ese spacer a a asa lee set
yyGlSAddtess malcninB
Doubt
❑UnNnaVRI
Describe location:
h#e tleterlN aTPli-pRO a'xlue(nc'emJ aflM1e Sek Anioo L<eel of 100 msea. These gctivifies were
conducted es per the Notice a Vfa(adon doled Jones, 2019. A She Check Report is being peepard.
HOW RELEASE WAS DISCOVERED (Raease code)
(atecxael
QReleuse adecllon Eeulptnunl or Methods QVuueYOda QGroundwater Contamination
QWdtq UST ClosonvRemoval ❑Weler N Tank QSulhoe Water Oonlaminallon
❑Property Trensler QWalw Bupplyweh Contaminator
SOURCE OF
CONTAMINATION
Source of Release
Cause of Release
Type of Release Product Type Released
fched Mfflry®Ux)
(Check vnmery sconce)
(Cwter ate) (C/recx Primary Pmtlua NPe reeesM)
❑Tank
[]SP10
Iprenaeum awOnevDleseb ❑DxrseWes at
❑Plpin9
❑Over011
11NOn-PeboleJm `t Kerosene Blend
PisPenser
❑Corrosion
Bath ❑-eating Oil ❑ Vegetable Od 100%
❑ SUPnartible TurGre Pump
❑Pleysicamechanlral
El other Pelmlevm ElEll) -E20
❑Delsery Problem
Damage
Location Praducts E]ebt -Eas
El Sol, so"❑Other
❑ Install Probem
(Check one)MBUIa
�EBS-E9g
[:law
QOlhw
ko
�FacllilY ryanl® LlEthand 10o4n
❑Unknown
�UMnown
❑Paesder10e ❑amet omerv[e
❑ EOt -EgB
Depmfrora remaeean rekmrse
D.rmeau wesarcadw revere
QgM1er
aumnlp
t Municipal 2. Millbury 3, UnNnuwPrivaten .Fed9al 0. gwnry 1. stale
Oowadon Tow
'. Public Sarviw 2: Agdoullual S. Rasdenbal <. EducatiaaRNlg. S. Indoors B. Cancer' T. Mining
UST Fann 61 MINIM
Pape IaI.

IMPACT ON DRINKING WATER SUPPLIES
Winer Supply Wells AOemetl9 I. Y® 2 No 3 V
Number of Water Supply Wells Arcan0
Water SUWIY Welt CW"Inahed: llltdutle Users NamK, Atltlrea eS BM FMare NumOers. AMach Btlo"rfimel.SXeef 11 neresSnrYl
1_
2
3.
UST SYSTEM OWNER
UST OwnerfCompany
Pilot Travel Centers, LLC
Pam a cmtmm Addmes
Keith Cllrlmn, Environmental Project Mounter 550E Lunn Rend
city
Sale Lp Cede
Tek'beenNumber
Knoxville
TN 3P309
lfl -07 d106
UST SYSTEM OPERATOR
LIST OperermlCanpsnY
Aceene
Pilot Travel Cenlae. LL(:
5500 Lenea Revd
C�ly Stele
by Coee
Teepnene Number
Knoxville TN
17909
0 "741J106
LANDOWNER AT LOCATION OF UST INCIDENT
largowner
Address
Pilot Travel Cermon. LLC
551111 Linn Rand
OIN
SWte
Lp COEo
relepnone rvumber
Knoxville
1]909
86L47i-31116
Draw Sketch of Area (showing two major road Intersections) or Attach Map
See attached site map
Pathan Radical bra ent M. Jnekeen
I CSa"InY ATG\nacho orNC(on behalf of Pilot)
Telepaone Number 919_ W I-Jtl'IJ
TiatPC/Sr.Project Manager
Addma 609.k Pinar Rd. Suite ilS Wilmington. NC 384A)9
Owe y2WE019
Peen i of 3
Talk minim
theO
Talk ®m the pinkthat ztotm the protect and ¢mthe coM1e.opnrnandSenateobura renksyaem
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contreer; the rabmerslbk lurhtha punde occuutamemN
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during pnduct roven but
to a me fitnome al ofthemouting cadwimlht sourc relaraltkandwrtlillxl
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rosy Fri nth m Lase
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Overml She when her overfill moment a, overfill; meyawrr r the fill Pipeaut pick or when mes9ale tots to Shut arm medlspenher)
Pkymi or MaMmN Manager a¢ fw ran type, ofpbyvrel rx mrtnanlcnl anmagr. recent cormsam leg. ptmnum of who Or ptpmy, have thing, beck M
ortmun and range that archanged d' t
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UST-17B UST Suspected Release 7 Day Notice KC
Q�
➢ This form must be used to report to DEQ, within 7 days of discovery, the investigation results for a Suspected Release from any of the following:
a) Failed or inconclusive leak detection or tightness test results. This includes positive test results, such as "Increase", which indicates the level in the
UST system has increased more than 0.2 gph.
b) Unusual operating conditions which can include, but are not limited to, the erratic behavior of dispensing equipment; the unexplained presence of
water in the tank; the presence of fuel in containment sumps or interstitial spaces; or the degradation of any equipment or element of an underground
storage tank system to the point where that equipment or element can not reasonably be expected to perform its intended function.
c) Internal inspection results such as, perforations, corrosion holes, weld failures, or other similar defects that indicate a release could have occurred.
➢ If you have more than four UST systems to report suspected release investigations, then attach additional sheets of the UST-17B form.
➢ Please submit this form along with the supporting documentation to:
NCDEQ/DWM, UST Section
1646 Mail Service Center
Raleigh, North Carolina 27699-1646
OR
Fax to [phone] OR UST.PermitsCaLncdenr.gov
I. UST OWNER II. UST FACILITY
Name: : Name: Facility ID
P, �nZ— 005 c�
Address: Address:
v
City: State: Zip: City: County:
�� c71 4S INr— 2 2tpq �w,r. v.c� 0 1 t S C_0 Jc�v'1 U S
Person Reporting: Title of Pin Reporting: Telephone Number:
1 rL�.s. s icA, v,(74 5—leg. yLl7'r
III. INVESTIGATION RESULTS
Tank Number / Size:
Product Stored:��. '
Reason for Suspected
Release Investigation
(Check all that apply):
You must attach the
supporting documentation
specified in the footnote for
the reason(s) selected.
❑ Data entry error'
❑ Dispensing fuel while
test is being conducted 2
❑ Faulty equipment 3
❑ Incorrect stick or meter
reading '
❑ Incorrect tank chart °
❑ Internal Inspection 5
❑ Meter not calibrated 6
❑ Other (Attach
explanation)'
❑ Tank/Dispenser
containment sump
contains liquid 7
❑ Tilted tank 6
❑ Unknown'
' Conduct a tank and/or line tightness test and attach the results, along with all of the supporting data sheets for the test method, to this form for submittal.
The summary page listing the results by itself is not acceptable. If the tightness test results are fail, then you must repair or replace your UST system and
conduct a site check in accordance with 15A NCAC 2N .0603.
2 Provide sales receipts or other comparable documentation that shows fuel was being dispensed from the UST during the test.
3 Provide invoices (with a description of the work completed) or other documentation that shows the equipment has been repaired.
4 Correct your leak detection results using the correct tank chart and submit copies with this form.
5 Repair the UST in accordance with the manufacturer's instructions or a national standard (e.g., PEI API 1631) and conduct a site check in accordance with
15A NCAC 2N .0603. If the UST is not repaired, then it must be permanently closed in accordance with the latest version of the UST Sections Guidelines
for Tank Closure.
❑ Data entry error'
❑ Dispensing fuel while
test is being conducted 2
❑ Faulty equipment 3
❑ Incorrect stick or meter
reading'
❑ Incorrect tank chart °
❑ Internal Inspection 5
❑ Meter not calibrated 6
❑ Other (Attach
explanation)'
KTank/Dispenser
containment sump
contains liquid'
❑ Tilted tank 6
❑ Unknown'
❑ Data entry error'
❑ Dispensing fuel while
test is being conducted 2
❑ Faulty equipment 3
❑ Incorrect stick or meter
reading'
❑ Incorrect tank chart °
❑ Internal Inspection 5
❑ Meter not calibrated 6
❑ Other (Attach
explanation)'
❑ Tank/Dispenser
containment sump
contains liquid 7
❑ Tilted tank 6
❑ Unknown'
❑ Data entry error'
❑ Dispensing fuel while
test is being conducted 2
❑ Faulty equipment 3
❑ Incorrect stick or meter
reading'
❑ Incorrect tank chart °
❑ Internal Inspection 5
❑ Meter not calibrated 6
❑ Other (Attach
explanation)'
❑ Tank/Dispenser
containment sump
contains liquid'
❑ Tilted tank 6
❑ Unknown'
6 Correct your leak detection results using the amount your meter was adjusted following calibration and submit copies of the meter calibration and leak
detection results with this form.
' Conduct a tightness test (e.g., hydrostatic test) of the sump and submit the test result along with this form. If the test results are fail, then you must repair
or replace the containment sump and conduct a site check in accordance with 15A NCAC 2N .0603.
6 Submit documentation from your UST equipment contractor explaining how they determined the UST was tilted. Correct your leak detection results using a
tank chart adjusted for the tilt and submit with this form.
Note: Tank, piping, spill bucket and containment sump replacements must be done in accordance with 15A NCAC 2N .0900
UST-17B Revised 10/2016 http://www.wastenotnc.org/web/wm/

�11
UST-6Fif23B Triennial UST Containment Sump 1 UDC Integrity Testing E
Full height hydrostatic or vacuum test mow— v
If any periodic test fails, a suspected release report must be submitted on a UST-17A form, UST Suspected Release 24 Hour Notice. The suspected
release must be investigated, in accordance with 15A NCAC 2N .0603, and defective equipment repaired or replaced in accordance with 15A NCAC
2N .0404/.0900. Results of the investigation must be submitted on a UST-17B form, UST Suspected Release 7 Day Notice.
Containment sumps installed on or after 11/1/2007 that are not monitored continuously for releases using vacuum, pressure, or hydrostatic interstitial
monitoring methods and all other containment sumps installed prior to 11/1/2007 that are used for interstitial monitoring shall be tightness tested at
installation and every three (3) years thereafter in accordance with the manufacturer's written guidelines, PEI/RP100 "Recommended Practices for
Installation of Underground Liquid Storage Systems" and/or PEI/RP1200 "Recommended Practices for the Testing and Verification of Spill, Overfill,
Leak Detection and Secondary Containment Equipment at UST Facilities."
If a UDC / containment sump fails a periodic tightness test, the sump must be replaced or repaired by the manufacturer, or the manufacturer's
authorized representative in accordance with the manufacturer's specifications, or in accordance with a code of practice developed by a nationally
recognized association.
UST FACILITY
O Operator Name R
OT 51.4
Facility Street Address F;
Z$2� L-C -t 'Sit —
TESTING CONTRACTOR INFORMATION
Company Name rnone E-mail Address
of law, that the testing data provided on this form documents the UST system equipment was tested in accordance with the
nes and the applicable national industry standaisted in 15A NCAC 2N .0406 and/or 15A NCAC 2N .0900.
ity Name
�, at 5(
I certify, under
manufacturer's
e of person conducting test
person conducting test Test Date
Identify UDC/sump (By
Dispenser No. or Tank Number,ispenser,
❑Dispenser
❑Dispenser
Tank Size, Stored Product, e.g.
❑Tank
❑Tank
❑Tank
#1 10k Regular STP, Disp 112,
#; LISP ZO
#
#:
etc.
Transition sumps should be listed above as "TS-XX" (with XX= sump ID#)
Sump Material
❑ FRP
❑ FRP
❑ FRP
Plastic
❑ Plastic
❑ Plastic
Test Type
Hydrostatic
❑ Hydrostatic
❑ Hydrostatic
❑ Vacuum
❑ Vacuum
1 ❑ Vacuum
Indicate units for all measurements sump?Eland debris removed from i _
TcxYes No
Visual inspection (No cracks,
loose parts or separation of the XPass ❑ Fail
containment sump}
Sump Depth in inches I i s"
Height from sump bottom to top
of highest penetration or sump i
sidewall seam in inches
Wait time between applying
vacuum/water and start of test 3c) tr\1d1
Begin i End Test Time
(minimum test time: 1 hour) IC 1 I 1151
Begin i End values (inches) 16 rr i 6 A
[]Dispenser
❑Tank
❑ FRP
❑ Plastic
❑ Hydrostatic
❑ Vacuum
❑Dispenser
❑Tank
❑ FRP
❑ Plastic
❑ Hydrostatic
❑ Vacuum
❑Dispenser
❑Tank
❑ FRP
❑ Plastic
❑ Hydrostatic
❑ Vacuum
❑ Yes ❑ No I ❑ Yes ❑ No I ❑ Yes ❑ No I ❑ Yes ❑ No I ❑ Yes ❑ No
❑ Pass ❑ Fail I ❑ Pass ❑ Fail 1 ❑ Pass ❑ Fail I ❑ Pass ❑ Fail I ❑ Pass ❑ Fail
Pass/Fail criteria: Must pass visual inspection. Hydrostatic: Water level drop of 1/8 inch or more fails the test; Vacuum: No change in vacuum
Test Result Pass El Fall El Pass Elail ❑Pass ❑Fail ❑ Pass ❑ Fail ❑ Pass ❑ Fail ❑ Pass ❑ Fail
Comments— (include information on repairs made prior to testing, and recommended follow-up for failed tests)
Date next Containment Sump/UDC integrity test due (required every 3 years)
NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY, DIVISION OF WASTE MANAGEMENT, UST SECTION
1646 MAIL SERVICE CENTER, RALEIGH, NC 27699-1646 PHONE [phone] FAX [phone] http://www.wastenotne.ora
2/2019

M
+� A
-SPATCB
E N E A C Y S O L U T 1 0 W&
Site Information
Service #9712049 PO #19124880-6040919
PILOT TRUCK STOP # 56 Customer #54770
2825 LANE STREET
KANNAPOLIS,NC 28083
United States
Work Performed by Travis Furr
Arrived on site checked in with mod. Pulled up to fp 20 to run a hydrostatic test on the entry boots.
Opens the bottom door and found liquid in the pan I use the compliance trailer to pump out 10 gallons.
I was able to inspect the entry boots and found one completely open I was able to tighten the boot
back to the piping. I filled a 5 gallons bucket up with water and filled the diesel pan on fp 20 to the top
of the entry boot I took measurements of the liquid test started at 10:51 and at 11:51 the test was done
and check my measurements and it was the same the hydrostatic test pass. I pumped the water that I
put in the pan out.
Time On Site
Time Arrived: 6/14/19, 8:45 AM
Time Departed: 6/14/19, 10:30 AM
Total Time on Site: 1 Hours 45 Minutes
Follow up Required?
No followup required.
Customer Signature
Savannah Crainshaw
6/14/19,12:10 PM

ATTACHMENT II

l
ceAnalytical ANALYTICAL REPORT
National Center for Testing & Innovation August 19, 2019
FTC
FS
ATC Group Services - NC Pilot I
Sample Delivery Group: L1127728 4Cn
Samples Received: 08/10/2019 FSr
Project Number: 56-605-13
6
Description: Pilot 56 Qc
7GI
Report To: Maureen Jackson
609A Piner Road Suite 115 rAl
Wilmington, NC 28409
FSC
Entire Report Reviewed By
Jeff Carr
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
a
V
41
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TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
1
Fn
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FS
SB-1 L1127728-01
5
[Cn]
Qc: Quality Control Summary
6
Total Solids by Method 2540 G-2011
6
Fr
Volatile Organic Compounds (GC) by Method 8015D/GRO
7
Semi -Volatile Organic Compounds (GC) by Method 8015C
8
RC
Gl: Glossary of Terms
9
F
Al: Accreditations & Locations
10
Sc: Sample Chain of Custody
11
rAl
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DATE/TIME: PAGE:
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SAMPLE SUMMARY ONE LAB. NATIONWIDE.
Collected by Collected date/time Received date/time
S13-1 L1127728-01 Solid Austen Rubenstein 08/09/1911:15 08/10/19 09:00 C
P
Method
Batch Dilution Preparation Analysis
date/time date/time
Analyst Location
Total Solids by Method 2540 G-2011
WG1330214
1 08/19/19 09:52
08/19/19 09:58 KBC
Mt. Juliet, TN
Volatile Organic Compounds (GC) by Method 8015D/GRO
WG1330422
25 08/09/1911:15
08/17/1919:09 ACG
Mt. Juliet, TN
Semi -Volatile Organic Compounds (GC) by Method 8015C
WG1329660
20 08/16/1916:01
08/19/19 01:57 KME
Mt. Juliet, TN
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
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56-605-13
L1127728
08/19/19 17:16
PAGE:
3 of 11
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CASE NARRATIVE
ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the FP1
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FTChave been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FSS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
FSr
6
QC
GI
Jeff Carr FAI
Project Manager
FSC
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SB-1
Collected date/time: 08/09/19 11:15
Total Solids by Method 2540 G-2011
SAMPLE RESULTS - 01
L1127728
Result Qualifier Dilution Analysis Batch
Analyte % date / time
Total Solids 85.2 1 08/19/2019 09:58 WG1330214
Volatile Organic Compounds (GC) by Method 8015D/GRO
Result (dry) Qualifier MDL (dry) RDL (dry)
Dilution Analysis Batch
Analyte
mg/kg
mg/kg mg/kg
date/time
TPH (GC/FID) Low Fraction
48.7
0.636 2.94
25 08/17/201919:09 WG1330422
(S)
a, a, a- Trifluorotoluene(FID)
91.7
77.0-120
081771201919:09 WG1330422
Semi -Volatile Organic Compounds
(GC) by Method 8015C
Result (dry) Qualifier MDL (dry) RDL (dry) Dilution Analysis Batch
Analyte mg/kg mg/kg mg/kg date/time
TPH (GC/FID) High Fraction 4890
(S) o-Terphenyl 0.000
18.1 93.9 20 08/19/2019 01:57 WG1329660
J7 18.0-148 0811912019 01:57 WG1329660
ONE LAB. NATIONWIDE.
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WG1330214
Total Solids by Method 2540 G-2011
Method Blank (MB)
(MB) R3441897-1 08/19/19 09:58
MB Result MB Qualifier MB MDL
Analyte % %
Total Solids 0.000
L1127738-01 Original Sample (OS) • Duplicate (DUP)
MB RDL
(OS) L1127738-01 08/19/19 09:58 • (DUP) R3441897-3 08/19/19 09:58
Original Result DUP Result Dilution DUP RPD
Analyte % % _ %
Total Solids 82.4 82.5 1 0.113
Laboratory Control Sample (LCS)
(LCS) R3441897-2 08/19/19 09:58
Spike Amount LCS Result LCS Rec.
Analyte % %_ %
Total Solids 50.0 50.0 100
QUALITY CONTROL SUMMARY
L1127728-01
DUP Qualifier DUP RPD
Limits
10
Rec. Limits LCS Qualifier
o/
85.0-115
ONE LAB. NATIONWIDE.
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WG1330422
Volatile Organic Compounds (GC) by Method 8015D/GRO
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1127728-01
(MB) R3441600-2 08/17/1912:43
MB Result MB Qualifier MB MDL
MB RDL
Analyte
mg/kg mg/kg
mg/kg
TPH (GC/FID) Low Fraction
0.0256 J 0.0217
0.100
(S)
o, o, o-Trifluorotoluene(FID)
93.7
77.0-120
Laboratory Control Sample (LCS)
(LCS) R3441600-1 08/17/1911:18
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg % %
TPH (GC/FID) Low Fraction 5.50 5.59 102 72.0-127
(S) 104 77.0-120
a, a, a- Trifluorotoluene(FID)
L1127738-14 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1127738-14 08/17/19 20:31 • (MS) R3441600-3 08/17/19 20:51 • (MSD) R3441600-4 08/17/19 21:12
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Analyte mg/kg mg/kg mg/kg mg/kg % %
TPH (GC/FID) Low Fraction 5.50 0.988 112 109 76.1 74.4
(S) 102 101
a, a, a- Trifluorotoluene(FID)
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
26.5 10.0-151 2.26
77.0-120
ONE LAB. NATIONWIDE.
RPD Limits
28
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WG1329660
Semi -Volatile Organic Compounds (GC) by Method 8015C
Method Blank (MB)
(MB) R3441376-1 08/16/19 23:22
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
TPH (GC/FID) High Fraction U 0.769 4.00
(S) o-Terpheny/ 64.0 18.0-148
Laboratory Control Sample (LCS)
I
QUALITY CONTROL SUMMARY
L1127728-01
(LCS) R3441376-2 08/16/19 23:35
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg % %
TPH (GC/FID) High Fraction 50.0 27.6 55.2 50.0-150
(S) o-Terpheny/ 67.1 18.0-148
ONE LAB. NATIONWIDE.
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GLOSSARY OF TERMS
ONE LAB. NATIONWIDE.
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
(dry) Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL Method Detection Limit.
MDL (dry) Method Detection Limit.
RDL Reported Detection Limit.
RDL (dry) Reported Detection Limit.
Rec. Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty Confidence level of 2 sigma.
(Radiochemistry)
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier Description
J The identification of the analyte is acceptable; the reported value is an estimate.
J7 Surrogate recovery cannot be used for control limit evaluation due to dilution.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
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ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National.
State Accreditations
Alabama
40660
Nebraska
NE-OS-15-05
Alaska
17-026
_
Nevada
TN-03-2002-34
Arizona
AZO612
New Hampshire
2975
Arkansas
88-0469
NewJersey_NELAP
TNO02
California
2932
New Mexico
n/a
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina'
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky76
90010
South Carolina
84004
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' 4
2006
Louisiana'
LA180010
Texas
T104704245-18-15
Maine
TN0002
Texas'
LABO152
Maryland
324
Utah
TN00003
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
460132
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
9980939910
Montana
CERT0086
Wyoming
A21LA
Third Party
Federal Accreditations
A21LA — ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A21LA — ISO 17025 5
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
' Drinking Water 'Underground Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable
Our Locations
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
FP
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PROJECT: SDG: DATE/TIME: PAGE:
56-605-13 L1127728 08/19/19 17:16 10 of 11

ATC Group Services • NC Pilot
609A Pour Road Suite 115
svwmwanvuon'.
aarlody MayuOb ^"
SSW Lava Dr.
xnox*Re. TN 37909
muaCp4. eNeler.l-
Wdminrton, NC I9a09
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APPENDIX B
Soil Boring Log and
Monitoring Well Construction Diagram

Start Date: 10/23/19 Hole Diameter: 4.25 inches Top of Casing Elevation:
Complete Date: 10/23/19 Casing Diameter: 2 inches Total Depth: 30 feet
Well Cap: Locking Expansion Drilling Company: Carolina Soil investigation Remarks: SB-1 30 foot submitted for laboratory analysis
Security Box: Flush -Mount Drilling Method: Hollow -stem Auger
DR: DRY
Nm2019
ReI fort
436096
r \/
/� I — L /�
APEX
R—oke, V vm 24019
[phone]
owumxo.n�e
Cx-:
APP'D.:
ISoil
Boring Log
Pilot #56
Kannapolis, North Carolina
SCAT F: NA
APExrRa. No.: 763490-030
www.apexcos.com
orswvaxc xurneea
nEv
er
owe
Soil Boring l/Monitoring Well MW-Al
O
s ..
a
Sample
ID
op
c
•„
e a
a a°
:;
o
s
J
Geologic Description
Well Diagram
(1' to 30')
Ground
Surface
5
10
15
------------------------------------
20
25
30
-------
Asphalt surface cover.
- 0-5': Brown- to gray Fill material, small- to
medium rock fragments, minimal moisture, 10.0'
slight petro odor. Schedule
40 PVC
5-10': Brown sandy loam, minimal rock
fragments, minimal moisture, slight petro
odor.
10-15': Brown sandy loam, minimal rock
fragments, slight moisture, slight petro
odor.
(20.0') 0.010
Slotted PVC
-15-20': Brown clay loam, minimal rock fragments,
slight moisture, slight petro odor.
-20.21': Equilibrated groundwater level.
- 20-25': Light Brown clay loam, minimal rock
fragments, slight moisture, petro odor.
- 25-30': Dark Brown clay loam, minimal rock
fragments, slight moisture, petro odor.
- 30': Boring terminated.
Boring converted to MW-Al.
Grout
Bentonite
g
10
15
(21.0') #2
Quartz Sand
20
25
30
SB-15
----
-----
-------
--
-------
----- ------
-
--
---
SB-1-10
----
-----
0.0 ------
-----
-----
--------
----
-----
-----
--------------
SB-1-15
----
----
0.0
----- ______=
---
SB-1-20
34.2
V
--------
----
-----
-----
-------
SB-1.25
--------
-
326
_______
----- ______=
-------
----
-----
-----
-------------
SB-130
----
-----
573
-----
t—
Geologist: Page 1 of 1

APPENDIX C
Laboratory Certificate of Analysis
and
Chain -of -Custody

aceAnalytical o ANALYTICAL REPORT
National Center for Testing & Innovation November 04, 2019
• #r
Pilot Apex Environmental
Sample Delivery Group: L1153593
Samples Received: 10/24/2019
Project Number: PILOT 56
Description: Pilot 56
Report To: Robert Wagner
7724 Garland Circle
Roanoke, VA 24019
Entire Report Reviewed By:
Pam Langford
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
4
V -
16
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental PILOT 56 L1153593 11/04/1919:55 1 of 22

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
1
Fn
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FS
MW-A2 L1153593-01
5
[Cn]
Qc: Quality Control Summary
8
Volatile Petroleum Hydrocarbons by Method MADEPV
8
Fr
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
9
TPH by Method MADEPE
13
RC
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
14
F
GI: Glossary of Terms
19
Al: Accreditations & Locations
20
rAl
Sc: Sample Chain of Custody
21
FSC
ACCOUNT: PROJECT: SDG:
DATE/TIME: PAGE:
Pilot Apex Environmental PILOT 56 L1153593
11/04/1919:55 2 of 22

MW-A2 L1153593-01 GW
SAMPLE
SUMMARY
Collected by
Evan Everson
Collected date/time
10/23/1916:15
ONE LAB. NATIONWIDE.
Received date/time
10/24/19 08:45
FP1
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
FTC
Volatile Petroleum Hydrocarbons by Method MADEPV
WG1371722
1 10/30/19 00:44
10/30/19 00:44
ACG
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
WG1374034
1 11/02/1914:10
11/02/1914:10
HJF
Mt. Juliet, TN
TPH by Method MADEPE
WG1371908
1.02 10/29/1917:39
10/31/1911:53
KME
Mt. Juliet, TN
TPH by Method MADEPE
WG1371908
1.02 10/29/1917:39
10/31/1912:15
KME
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
WG1371001
1 10/28/1917:01
10/29/19 03:29
LEA
Mt. Juliet, TN
[Cn]
FSr
RC
F,
FAI
FSC
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Pilot Apex Environmental
PILOT 56
L1153593
11/04/1919:55
3 of 22

CASE NARRATIVE
ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
Pam Langford
Project Manager
FP1
FTC
FSS
FSr
6
QC
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental PILOT 56 L1153593 11/04/1919:55 4 of 22

MW-A2 SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE.
Collected date/time: 10/23/19 16:15 L1153593
Volatile Petroleum Hydrocarbons by Method MADEPV
Result Qualifier RDL Dilution
Analyte mg/I mg/I
Unadjusted C5-C8 Aliphatics ND 0.100 1
Unadjusted C9-C12 Aliphatics ND 0.100 1
Unadjusted C9-C10 Aromatics ND 0.100 1
Total VPH ND 0.100 1
(S) 2,5-Dibromotoluene(FID) 101 70.0-130
(S)2,5-Dibromotoluene(PID) 99.6 70.0-130
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
Analysis
date / time
10/30/2019 00:44
10/30/2019 00:44
10/30/2019 00:44
10/30/2019 00:44
1013012019 00:44
101301201900:44
Batch
WG1371722
WG1371722
WG1371722
WG1371722
WG1371722
WG1371722
u
FTc
F
rCn
Result
Qualifier RDL Dilution
Analysis
Batch
Analyte
mg/I
mg/I
date / time
6QC
Acetone
ND
0.0500 1
11/02/201914:10
WG1374034
Acrolein
ND
0.0500 1
11/02/201914:10
WG1374034
Acrylonitrile
ND
0.0100 1
11/02/201914:10
WG1374034
GI
Benzene
ND
0.00100 1
11/02/201914:10
WG1374034
Bromobenzene
ND
0.00100 1
11/02/201914:10
WG1374034
FAI
Bromodichloromethane
0.00802
0.00100 1
11/02/201914:10
WG1374034
Bromoform
ND
0.00100 1
11/02/201914:10
WG1374034
Bromomethane
ND
0.00500 1
11/02/201914:10
WG1374034
FSC
n-Butylbenzene
ND
0.00100 1
11/02/201914:10
WG1374034
sec -Butyl benzene
ND
0.00100 1
11/02/201914:10
WG1374034
tert-Butylbenzene
ND
0.00100 1
11/02/201914:10
WG1374034
Carbon tetrachloride
ND
0.00100 1
11/02/201914:10
WG1374034
Chlorobenzene
ND
0.00100 1
11/02/201914:10
WG1374034
Chlorodibromomethane
0.00135
0.00100 1
11/02/201914:10
WG1374034
Chloroethane
ND
0.00500 1
11/02/201914:10
WG1374034
Chloroform
0.0385
0.00500 1
11/02/201914:10
WG1374034
Chloromethane
ND
0.00250 1
11/02/201914:10
WG1374034
2-Chlorotoluene
ND
0.00100 1
11/02/201914:10
WG1374034
4-Chlorotoluene
ND
0.00100 1
11/02/201914:10
WG1374034
1,2-Dibromo-3-Chloropropane
ND
0.00500 1
11/02/201914:10
WG1374034
1,2-Dibromoethane
ND
0.00100 1
11/02/201914:10
WG1374034
Dibromomethane
ND
0.00100 1
11/02/201914:10
WG1374034
1,2-Dichlorobenzene
ND
0.00100 1
11/02/201914:10
WG1374034
1,3-Dichlorobenzene
ND
0.00100 1
11/02/201914:10
WG1374034
1,4-Dichlorobenzene
ND
0.00100 1
11/02/201914:10
WG1374034
Dichlorodifluoromethane
ND
0.00500 1
11/02/201914:10
WG1374034
1,1-Dichloroethane
ND
0.00100 1
11/02/201914:10
WG1374034
1,2-Dichloroethane
ND
0.00100 1
11/02/201914:10
WG1374034
1,1-Dichloroethene
ND
0.00100 1
11/02/201914:10
WG1374034
cis-1,2-Dichloroethene
ND
0.00100 1
11/02/201914:10
WG1374034
trans-1,2-Dichloroethene
ND
0.00100 1
11/02/201914:10
WG1374034
1,2-Dichloropropane
ND
0.00100 1
11/02/201914:10
WG1374034
1,1-Dichloropropene
ND
0.00100 1
11/02/201914:10
WG1374034
1,3-Dichloropropane
ND
0.00100 1
11/02/201914:10
WG1374034
2,2-Dichloropropane
ND
0.00100 1
11/02/201914:10
WG1374034
Di -isopropyl ether
ND
0.00100 1
11/02/201914:10
WG1374034
Ethylbenzene
ND
0.00100 1
11/02/201914:10
WG1374034
Hexachloro-1,3-butadiene
ND
0.00100 1
11/02/201914:10
WG1374034
Isopropylbenzene
ND
0.00100 1
11/02/201914:10
WG1374034
p-Isopropyltoluene
ND
0.00100 1
11/02/201914:10
WG1374034
2-Butanone (MEK)
ND
0.0100 1
11/02/201914:10
WG1374034
Methylene Chloride
ND
0.00500 1
11/02/201914:10
WG1374034
4-Methyl-2-pentanone (MIBK)
ND
0.0100 1
11/02/201914:10
WG1374034
Methyl tert-butyl ether
ND
0.00100 1
11/02/201914:10
WG1374034
Naphthalene
ND
0.00500 1
11/02/201914:10
WG1374034
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Pilot Apex Environmental
PILOT 56
L1153593
11/04/1919:55
5 of 22

MW-A2 SAMPLE RESULTS - 01
Collected date/time: 10/23/19 16:15 L1153593
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
ONE LAB. NATIONWIDE.
Analyte
n-Propylbenzene
Styrene
1,1,1, 2-Tetra c h I o ro et h an e
1,1,2,2-TetrachIoroetha ne
Tetrachloroethene
Toluene
1,2,3-Trichlorobe nzene
1,2,4-Trichlorobenzene
1,1,1-Trich Io roetha ne
1,1,2-Trich I oroetha n e
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Tri methyl ben zen e
1,3,5-Trim ethyl benzene
Vinyl chloride
o-Xylene
m&p-Xylenes
(S) Toluene-d8
(S) 4-Bromof/uorobenzene
(S) 1,2-Dich/oroethone-d4
Result
Qualifier RDL
Dilution Analysis
mg/I
mg/I
date / time
ND
0.00100
1 11/02/201914:10
ND
0.00100
1 11/02/201914:10
ND
0.00100
1 11/02/201914:10
ND
0.00100
1 11/02/201914:10
ND
0.00100
1 11/02/201914:10
ND
0.00100
1 11/02/201914:10
ND
0.00100
1 11/02/201914:10
ND
0.00100
1 11/02/201914:10
ND
0.00100
1 11/02/201914:10
ND
0.00100
1 11/02/201914:10
ND
0.00100
1 11/02/201914:10
ND
0.00500
1 11/02/201914:10
ND
0.00250
1 11/02/201914:10
ND
0.00100
1 11/02/201914:10
ND
0.00100
1 11/02/201914:10
ND
0.00100
1 11/02/201914:10
ND
0.00100
1 11/02/201914:10
ND
0.00200
1 11/02/201914:10
93.0
80.0-120
111021201914:10
92.2
77.0-126
111021201914:10
88.9
70.0-130
111021201914:10
TPH by Method MADEPE
Result
Qualifier RDL
Analyte
mg/I
mg/I
Unadjusted C9-C18 Aliphatics
ND
0.102
Unadjusted C19-06 Aliphatics
ND
0.102
Unadjusted C11-C22 Aromatics
ND
0.102
Unadjusted Total Petroleum
ND
0.102
Hydrocarbons
(S) o-Terphenyl
65.0
40.0-140
(S)1-Chloro-octadecane
69.9
40.0-140
(S) 2-Fluorobipheny/
79.7
40.0-140
(S) 2-Bromonaphtha/ene
74.1
40.0-140
Dilution Analysis
date / time
Batch
WG1374034
WG1374034
WG1374034
WG1374034
WG1374034
WG1374034
WG1374034
WG1374034
WG1374034
WG1374034
WG1374034
WG1374034
WG1374034
WG1374034
WG1374034
WG1374034
WG1374034
WG1374034
WG1374034
WG1374034
WG1374034
Batch
1.02
10/31/201911:53
WG1371908
1.02
10/31/201911:53
WG1371908
1.02
10/31/201912:15
WG1371908
1.02
10/31/201911:53
WG1371908
1013112019 12:15
WG1371908
101311201911.53
WG1371908
1013112019 12:15
WG1371908
1013112019 12:15
WG1371908
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result
Qualifier RDL
Dilution Analysis
Batch
Analyte
mg/I
mg/I
date / time
Acenaphthene
ND
0.00100
1 10/29/2019 03:29
WG1371001
Acenaphthylene
ND
0.00100
1 10/29/2019 03:29
WG1371001
Anthracene
ND
0.00100
1 10/29/2019 03:29
WG1371001
Benzidine
ND
0.0100
1 10/29/2019 03:29
WG1371001
Benzo(a)anth race ne
ND
0.00100
1 10/29/2019 03:29
WG1371001
Benzo(b)fluoranthene
ND
0.00100
1 10/29/2019 03:29
WG1371001
Benzo(k)fuoranthene
ND
0.00100
1 10/29/2019 03:29
WG1371001
Benzo(g,h,i)perylene
ND
0.00100
1 10/29/2019 03:29
WG1371001
Benzo(a)pyrene
ND
0.00100
1 10/29/2019 03:29
WG1371001
Bis(2-chlorethoxy)methane
ND
0.0100
1 10/29/2019 03:29
WG1371001
Bis(2-chloroethyl)ether
ND
0.0100
1 10/29/2019 03:29
WG1371001
Bis(2-chloroisopropyl)ether
ND
0.0100
1 10/29/2019 03:29
WG1371001
4-Bromophenyl-phenylether
ND
0.0100
1 10/29/2019 03:29
WG1371001
2-Chloronaphthalene
ND
0.00100
1 10/29/2019 03:29
WG1371001
4-Chlorophenyl-phenylether
ND
0.0100
1 10/29/2019 03:29
WG1371001
Chrysene
ND
0.00100
1 10/29/2019 03:29
WG1371001
Dibenz(a,h)anthracene
ND
0.00100
1 10/29/2019 03:29
WG1371001
3,3-Dichlorobenzidine
ND
0.0100
1 10/29/2019 03:29
WG1371001
Cp
FTc
FSS
4
Cn
Fc
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental PILOT 56 L1153593 11/04/1919:55 6 of 22

ONE LAB. NATIONWIDE.
MW-A2 SAMPLE RESULTS - 01
Collected date/time: 10/23/19 16:15 L1153593
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result
Qualifier RDL
Dilution Analysis
Batch
Analyte
mg/I
mg/I
date / time
2,4-Dinitrotoluene
ND
0.0100
1 10/29/2019 03:29
WG1371001
2,6-Dinitrotoluene
ND
0.0100
1 10/29/2019 03:29
WG1371001
Fluoranthene
ND
0.00100
1 10/29/2019 03:29
WG1371001
Fluorene
ND
0.00100
1 10/29/2019 03:29
WG1371001
Hexachlorobenzene
ND
0.00100
1 10/29/2019 03:29
WG1371001
Hexachloro-1,3-butadiene
ND
0.0100
1 10/29/2019 03:29
WG1371001
Hexachlorocyclopentadiene
ND
0.0100
1 10/29/2019 03:29
WG1371001
Hexachloroethane
ND
0.0100
1 10/29/2019 03:29
WG1371001
Indeno(1,2,3-cd)pyrene
ND
0.00100
1 10/29/2019 03:29
WG1371001
Isophorone
ND
0.0100
1 10/29/2019 03:29
WG1371001
Naphthalene
ND
0.00100
1 10/29/2019 03:29
WG1371001
Nitrobenzene
ND
0.0100
1 10/29/2019 03:29
WG1371001
n-Nitrosodimethyla mine
ND
0.0100
1 10/29/2019 03:29
WG1371001
n-Nitrosodiphenyla mine
ND
0.0100
1 10/29/2019 03:29
WG1371001
n-Nitrosodi-n-propylamine
ND
0.0100
1 10/29/2019 03:29
WG1371001
Phenanthrene
ND
0.00100
1 10/29/2019 03:29
WG1371001
Benzylbutyl phthalate
ND
0.00300
1 10/29/2019 03:29
WG1371001
Bis(2-ethylhexyl)phthalate
ND
0.00300
1 10/29/2019 03:29
WG1371001
Di-n-butyl phthalate
ND
0.00300
1 10/29/2019 03:29
WG1371001
Diethyl phthalate
ND
0.00300
1 10/29/2019 03:29
WG1371001
Dimethyl phthalate
ND
0.00300
1 10/29/2019 03:29
WG1371001
Di-n-octyl phthalate
ND
0.00300
1 10/29/2019 03:29
WG1371001
Pyrene
ND
0.00100
1 10/29/2019 03:29
WG1371001
1,2,4-Trichlorobenzene
ND
0.0100
1 10/29/2019 03:29
WG1371001
4-ChIoro-3-methyl phenol
ND
0.0100
1 10/29/2019 03:29
WG1371001
2-Chorophenol
ND
0.0100
1 10/29/2019 03:29
WG1371001
2,4-Dichlorophenol
ND
0.0100
1 10/29/2019 03:29
WG1371001
2,4-Dimethylphenol
ND
0.0100
1 10/29/2019 03:29
WG1371001
4,6-Dinitro-2-methylphenol
ND
0.0100
1 10/29/2019 03:29
WG1371001
2,4-Dinitrophenol
ND
0.0100
1 10/29/2019 03:29
WG1371001
2-Nitrophenol
ND
0.0100
1 10/29/2019 03:29
WG1371001
4-Nitrophenol
ND
0.0100
1 10/29/2019 03:29
WG1371001
Pentachlorophenol
ND
0.0100
1 10/29/2019 03:29
WG1371001
Phenol
ND
0.0100
1 10/29/2019 03:29
WG1371001
2,4,6-Trichlorophenol
ND
0.0100
1 10/29/2019 03:29
WG1371001
1,2-Diphenylhydrazine
ND
0.0100
1 10/29/2019 03:29
WG1371001
(S) 2-Fluorophenol
31.8
10.0-120
1012912019 03:29
WG1371001
(S) Phenol-d5
19.3
8.00-424
1012912019 03:29
WG1371001
(S) Nitrobenzene-d5
41.7
15.0-314
1012912019 03:29
WG1371001
(S) 2-F/uorobipheny/
55.3
22.0-127
1012912019 03:29
WG1371001
(S)2,4,6-Tribromopheno/
58.0
10.0-153
1012912019 03:29
WG1371001
(S) p-Terphenyl-d14
84.4
29.0-141
1012912019 03:29
WG1371001
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 - TENTATIVELY IDENTIFIED COMPOUNDS
Result Qualifier RDL Dilution Analysis Batch CAS #
Analyte mg/I mg/I date / time
Dodecanoic Acid 0.0591 J N 0.000 1 10/29/2019 03:29 WG1371001 000143-07-7
Octadecanoic Acid 0.0264 J N 0.000 1 10/29/2019 03:29 WG1371001 000057-11-4
Unknown-01 0.00403 J N 0.000 1 10/29/2019 03:29 WG1371001 000870-63-3
Unknown-02 0.00402 J N 0.000 1 10/29/2019 03:29 WG1371001 077862-13-6
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds. Therefore, not all TICS are identified and quantitated using individual standards. TIC
listings are prepared utilizing a computerized library search routine of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist. Quantitation is
accomplished by relative peak area of the TIC compared to that of the nearest internal standard from the total ion chromatogram. TICs are identified and quantitated only if the peak area is
10% or more of that of the nearest internal standard.
FP
FTC
FS
Fn
FC]
F
FAI
FSC
ACCOUNT:
Pilot Apex Environmental
PROJECT: SDG: DATE/TIME: PAGE:
PILOT 56 L1153593 11/04/1919:55 7 of 22

WG1371722
Volatile Petroleum Hydrocarbons by Method MADEPV
Method Blank (MB)
QUALITY
CONTROL SUMMARY
L1153593-01
ONE LAB. NATIONWIDE.
FP1(MB)
R3468263-3 10/29/19 21:53
MB Result MB Qualifier MB MDL
MB RDL
Analyte mg/I mg/I
mg/I
FTc
Unadjusted C5-C8 Aliphatics U 0.0333
0.100
Unadjusted C9-C12 Aliphatics U 0.0333
0.100
FSS
Unadjusted C9-C10 Aromatics U 0.0333
0.100
Total VPH U 0.0333
0.100
(S)2,5-Dibromotoluene(FID) 85.1
70.0-130
rCn
(S)2,5-Dibromotoluene(PID) 86.7
70.0-130
rs—r
Laboratory Control Sample (LCS) • Laboratory Control Sample
Duplicate (LCSD)
(LCS) R3468263-1 10/29/1919:45 • (LCSD) R3468263-2 10/29/19 20:17
M
Spike Amount LCS Result LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits LCS Qualifier LCSD Qualifier
RPD
RPD Limits
Analyte mg/I mg/I mg/I
%
%
%
%
%
7
GI
Unadjusted C5-C8 Aliphatics 1.20 1.22 1.23
102
103
70.0-130
0.816
25
Unadjusted C9-C12 Aliphatics 1.40 1.53 1.55
109
ill
70.0-130
1.30
25
FAI
Unadjusted C9-C10 Aromatics 0.200 0.204 0.208
102
104
70.0-130
1.94
25
Total VPH 2.80 2.95 2.99
105
107
70.0-130
1.35
25
(S)2,5-Dibromotoluene(FID)
97.7
98.9
70.0-130
[Sc(S)2,5-Dibromoto/uene(PID)
97.4
98.1
70.0-130
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental PILOT 56 L1153593 11/04/1919:55 8 of 22

WG1374034 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 620OB-2011 L1153593-01
Method Blank (MB)
(MB) R3467950-3 11/02/1911:31
MB Result MB Qualifier
Analyte mg/I
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec -Butyl benzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
2,2-Dichloropropane
Di -isopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene
p-Isopropyltoluene
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MB MDL
mg/I
0.0100
0.00887
0.00187
0.000331
0.000352
0.000380
0.000469
0.000866
0.000361
0.000365
0.000399
0.000379
0.000348
0.000327
0.000453
0.000324
0.000276
0.000375
0.000351
0.00133
0.000381
0.000346
0.000349
0.000220
0.000274
0.000551
0.000259
0.000361
0.000398
0.000260
0.000396
0.000306
0.000352
0.000366
0.000321
0.000320
0.000384
0.000256
0.000326
0.000350
MB RDL
mg/I
0.0500
0.0500
0.0100
0.00100
0.00100
0.00100
0.00100
0.00500
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
0.00500
0.00500
0.00250
0.00100
0.00100
0.00500
0.00100
0.00100
0.00100
0.00100
0.00100
0.00500
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental PILOT 56 L1153593 11/04/1919:55 9 of 22

WG1374034 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 620OB-2011 L1153593-01
Method Blank (MB)
(MB) R3467950-3 11/02/1911:31
MB Result
Analyte mg/I
2-Butanone (MEK)
U
Methylene Chloride
U
4-Methyl-2-pentanone (MIBK)
U
Methyl tert-butyl ether
U
Naphthalene
U
n-Propylbenzene
U
Styrene
U
1,1,1,2-Tetrachloroethane
U
1,1,2,2-Tetrachloroethane
U
Tetrachloroethene
U
Toluene
U
1,2,3-Trichlorobenzene
U
1,2,4-Trichlorobenzene
U
1,1,1-Trichloroethane
U
1,1,2-Trichloroethane
U
Trichloroethene
U
Trichlorofluoromethane
U
1,2,3-Trichloropropane
U
1,2,4-Trimethylbenzene
U
1,3,5-Trimethyl benzene
U
Vinyl chloride
U
o-Xylene
U
m&p-Xylenes
U
(S) Toluene-d8
95.1
(S) 4-Bromof/uorobenzene
91.8
(S) 1,2-Dich/oroethane-d4
92.6
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.00393
0.0100
0.00100
0.00500
0.00214
0.0100
0.000367
0.00100
0.00100
0.00500
0.000349
0.00100
0.000307
0.00100
0.000385
0.00100
0.000130
0.00100
0.000372
0.00100
0.000412
0.00100
0.000230
0.00100
0.000355
0.00100
0.000319
0.00100
0.000383
0.00100
0.000398
0.00100
0.00120
0.00500
0.000807
0.00250
0.000373
0.00100
0.000387
0.00100
0.000259
0.00100
0.000341
0.00100
0.000719
0.00200
80.0-120
77.0-126
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3467950-1 11/02/19 10:32 • (LCSD) R3467950-2 11/02/1910:52
Spike Amount
LCS Result
LCSD Result
Analyte
mg/I
mg/I
mg/I
Acetone
0.0250
0.0327
0.0292
Acrolein
0.0250
0.0263
0.0238
Acrylonitrile
0.0250
0.0256
0.0234
Benzene
0.00500
0.00445
0.00413
Bromobenzene
0.00500
0.00463
0.00436
Bromodichloromethane
0.00500
0.00463
0.00412
Bromoform
0.00500
0.00461
0.00427
ACCOUNT:
Pilot Apex Environmental
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
131
117
19.0-160
11.3
27
105
95.2
10.0-160
9.98
26
102
93.6
55.0-149
8.98
20
89.0
82.6
70.0-123
7.46
20
92.6
87.2
73.0-121
6.01
20
92.6
82.4
75.0-120
11.7
20
92.2
85.4
68.0-132
7.66
20
PROJECT:
SDG:
DATE/TIME: PAGE:
PILOT 56
L1153593
11/04/1919:55 10 of 22
FP1
FTc
FSS
4
Cn
FSr
�GI
FAI
[Sc

WG1374034 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 620OB-2011 L1153593-01
ONE LAB. NATIONWIDE.
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3467950-1 11/02/19 10:32 • (LCSD) R3467950-2 11/02/1910:52
Spike Amount
LCS Result
LCSD Result
Analyte
mg/I
mg/I
mg/I
Bromomethane
0.00500
0.00488
0.00412
n-Butylbenzene
0.00500
0.00458
0.00434
sec -Butyl benzene
0.00500
0.00443
0.00421
tert-Butylbenzene
0.00500
0.00447
0.00416
Carbon tetrachloride
0.00500
0.00417
0.00387
Chlorobenzene
0.00500
0.00470
0.00441
Chlorodibromomethane
0.00500
0.00467
0.00430
Chloroethane
0.00500
0.00436
0.00385
Chloroform
0.00500
0.00449
0.00420
Chloromethane
0.00500
0.00424
0.00374
2-Chlorotoluene
0.00500
0.00462
0.00451
4-Chlorotoluene
0.00500
0.00455
0.00446
1,2-Dibromo-3-Chloropropane
0.00500
0.00435
0.00402
1,2-Dibromoethane
0.00500
0.00471
0.00443
Dibromomethane
0.00500
0.00497
0.00438
1,2-Dichlorobenzene
0.00500
0.00461
0.00441
1,3-Dichlorobenzene
0.00500
0.00462
0.00442
1,4-Dichlorobenzene
0.00500
0.00450
0.00445
Dichlorodifluoromethane
0.00500
0.00454
0.00428
1,1-Dichloroethane
0.00500
0.00475
0.00431
1,2-Dichloroethane
0.00500
0.00455
0.00441
1,1-Dichloroethene
0.00500
0.00447
0.00419
cis-1,2-Dichloroethene
0.00500
0.00488
0.00444
trans-1,2-Dichloroethene
0.00500
0.00452
0.00427
1,2-Dichloropropane
0.00500
0.00493
0.00430
1,1-Dichloropropene
0.00500
0.00433
0.00409
1,3-Dichloropropane
0.00500
0.00480
0.00446
2,2-Dichloropropane
0.00500
0.00444
0.00422
Di -isopropyl ether
0.00500
0.00489
0.00448
Ethylbenzene
0.00500
0.00448
0.00432
Hexachloro-1,3-butadiene
0.00500
0.00459
0.00476
Isopropylbenzene
0.00500
0.00439
0.00415
p-Isopropyltoluene
0.00500
0.00452
0.00422
2-Butanone (MEK)
0.0250
0.0280
0.0253
Methylene Chloride
0.00500
0.00492
0.00438
4-Methyl-2-pentanone (MIBK)
0.0250
0.0236
0.0216
Methyl tert-butyl ether
0.00500
0.00474
0.00432
Naphthalene
0.00500
0.00397
0.00405
n-Propylbenzene
0.00500
0.00449
0.00432
Styrene
0.00500
0.00468
0.00446
ACCOUNT:
Pilot Apex Environmental
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
97.6
82.4
10.0-160
16.9
25
91.6
86.8
73.0-125
5.38
20
88.6
84.2
75.0-125
5.09
20
89.4
83.2
76.0-124
7.18
20
83.4
77.4
68.0-126
7.46
20
94.0
88.2
80.0-121
6.37
20
93.4
86.0
77.0-125
8.25
20
87.2
77.0
47.0-150
12.4
20
89.8
84.0
73.0-120
6.67
20
84.8
74.8
41.0-142
12.5
20
92.4
90.2
76.0-123
2.41
20
91.0
89.2
75.0-122
2.00
20
87.0
80.4
58.0-134
7.89
20
94.2
88.6
80.0-122
6.13
20
99.4
87.6
80.0-120
12.6
20
92.2
88.2
79.0-121
4.43
20
92.4
88.4
79.0-120
4.42
20
90.0
89.0
79.0-120
1.12
20
90.8
85.6
51.0-149
5.90
20
95.0
86.2
70.0-126
9.71
20
91.0
88.2
70.0-128
3.13
20
89.4
83.8
71.0-124
6.47
20
97.6
88.8
73.0-120
9.44
20
90.4
85.4
73.0-120
5.69
20
98.6
86.0
77.0-125
13.7
20
86.6
81.8
74.0-126
5.70
20
96.0
89.2
80.0-120
7.34
20
88.8
84.4
58.0-130
5.08
20
97.8
89.6
58.0-138
8.75
20
89.6
86.4
79.0-123
3.64
20
91.8
95.2
54.0-138
3.64
20
87.8
83.0
76.0-127
5.62
20
90.4
84.4
76.0-125
6.86
20
112
101
44.0-160
10.1
20
98.4
87.6
67.0-120
11.6
20
94.4
86.4
68.0-142
8.85
20
94.8
86.4
68.0-125
9.27
20
79.4
81.0
54.0-135
2.00
20
89.8
86.4
77.0-124
3.86
20
93.6
89.2
73.0-130
4.81
20
PROJECT:
SDG:
DATE/TIME: PAGE:
PILOT 56
L1153593
11/04/1919:55 11 of 22
FP1
FTC
FSS
[Cn]
FSr
�GI
FAI
FSC

WG1374034 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 620OB-2011 L1153593-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
ONE LAB. NATIONWIDE.
(LCS) R3467950-1 11/02/19 10:32 • (LCSD) R3467950-2 11/02/1910:52
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte mg/I
mg/I
mg/I
%
%
%
%
%
1,1,1,2-Tetrachloroethane 0.00500
0.00456
0.00431
91.2
86.2
75.0-125
5.64
20
1,1,2,2-Tetrachloroethane 0.00500
0.00460
0.00432
92.0
86.4
65.0-130
6.28
20
Tetrachloroethene 0.00500
0.00438
0.00411
87.6
82.2
72.0-132
6.36
20
Toluene 0.00500
0.00442
0.00410
88.4
82.0
79.0-120
7.51
20
1,2,3-Trichlorobenzene 0.00500
0.00410
0.00415
82.0
83.0
50.0-138
1.21
20
1,2,4-Trichlorobenzene 0.00500
0.00405
0.00415
81.0
83.0
57.0-137
2.44
20
1,1,1-Trichloroethane 0.00500
0.00466
0.00439
93.2
87.8
73.0-124
5.97
20
1,1,2-Trichloroethane 0.00500
0.00464
0.00425
92.8
85.0
80.0-120
8.77
20
Trichloroethene 0.00500
0.00470
0.00434
94.0
86.8
78.0-124
7.96
20
Trichlorofluoromethane 0.00500
0.00432
0.00402
86.4
80.4
59.0-147
7.19
20
1,2,3-Trichloropropane 0.00500
0.00474
0.00435
94.8
87.0
73.0-130
8.58
20
1,2,4-Trimethylbenzene 0.00500
0.00467
0.00446
93.4
89.2
76.0-121
4.60
20
1,3,5-Trimethyl benzene 0.00500
0.00458
0.00432
91.6
86.4
76.0-122
5.84
20
Vinyl chloride 0.00500
0.00405
0.00377
81.0
75.4
67.0-131
7.16
20
o-Xylene 0.00500
0.00429
0.00410
85.8
82.0
80.0-122
4.53
20
m&p-Xylenes 0.0100
0.00878
0.00847
87.8
84.7
80.0-122
3.59
20
(S) Toluene-d8
90.5
92.9
80.0-120
(S) 4-Bromofluorobenzene
92.8
91.3
77.0-126
(S) 1,2-Dich/oroethane-d4
93.3
93.1
70.0-130
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Pilot Apex Environmental
PILOT 56
L1153593
11/04/1919:55 12 of 22
FP1
FTC
FSS
4
Cn
FSr
�GI
FAI
FSC

WG1371908
TPH by Method MADEPE
Method Blank (MB)
(MB) R3466999-1 10/31/19 09:38
MB Result
Analyte
mg/I
Unadjusted C9-C18 Aliphatics
0.0377
Unadjusted C19-06 Aliphatics
U
(S)1-Chloro-octadecane
75.5
Method Blank (MB)
(MB) R3466999-4 10/31/1910:48
MB Result
Analyte
mg/I
Unadjusted C11-C22 Aromatics
U
(S) o-Terpheny/
70.1
(S) 2-F/uorobipheny/
77.0
(S) 2-Bromonophtha/ene
71.1
QUALITY CONTROL SUMMARY
L1153593-01
MB Qualifier MB MDL
MB RDL
mg/I
mg/I
J 0.0333
0.100
0.0333
0.100
40.0-140
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.0333 0.100
40.0-140
40.0-140
40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3466999-2 10/31/1910:05 • (LCSD) R3466999-3 10/31/1910:26
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
%
%
%
%
%
Unadjusted C9-C18 Aliphatics
0.600
0.300
0.310
50.0
51.7
40.0-140
3.28
25
Unadjusted C19-C36 Aliphatics
0.800
0.576
0.654
72.0
81.8
40.0-140
12.7
25
(S)1-Chloro-octadecane
71.5
77.5
40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3466999-5 10/31/1911:10 • (LCSD) R3466999-6 10/31/1911:32
Spike Amount LCS Result
LCSD Result LCS Rec.
LCSD Rec.
Rec. Limits LCS Qualifier LCSD Qualifier RPD
Analyte mg/I mg/I
mg/I %
%
% %
Unadjusted C11-C22 Aromatics 1.70 1.08
1.18 63.5
69.4
40.0-140 8.85
(S) o-Terpheny/
69.6
75.3
40.0-140
(S) 2-Fluorobiphenyl
79.1
73.6
40.0-140
(S) 2-Bromonaphtha/ene
76.6
72.2
40.0-140
RPD Limits
25
ONE LAB. NATIONWIDE.
FP1
FTc
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental PILOT 56 L1153593 11/04/1919:55 13 of 22

WG1371001 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1153593-01
Method Blank (MB)
(MB) R3466166-2 10/29/19 02:13
MB Result MB Qualifier
Analyte mg/I
Acenaphthene
Acenaphthylene
Anthracene
Azobenzene
Benzidine
Benzo(a)anth race ne
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(g,h,i)perylene
Benzo(a)pyrene
Bis(2-chlorethoxy)methane
B is(2-ch loroethyl)eth er
Bis(2-chloroisopropyl)ether
4-Bromophenyl-phenylether
2-Chloronaphthalene
4-Chlorophenyl-phenylether
Chrysene
Dibenz(a,h)anthracene
3,3-Dichlorobenzidine
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachlorocyclopentadiene
Hexachloroethane
I nd eno(1,2,3-cd) pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodimethyla mine
n-Nitrosodiphenyla mine
n-N itros o d i-n-p ro pyl a m i n e
Phenanthrene
Benzylbutyl phthalate
B is(2-ethyl h exyl)phtha I ate
Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MB MDL
mg/I
0.000316
0.000309
0.000291
0.000318
0.00432
0.0000975
0.0000896
0.000355
0.000161
0.000340
0.000329
0.00162
0.000445
0.000335
0.000330
0.000303
0.000332
0.000279
0.00202
0.00165
0.000279
0.000310
0.000323
0.000341
0.000329
0.00233
0.000365
0.000279
0.000272
0.000372
0.000367
0.00126
0.00119
0.000403
0.000366
0.000275
0.000709
0.000266
0.000282
0.000283
MB RDL
mg/I
0.00100
0.00100
0.00100
0.0100
0.0100
0.00100
0.00100
0.00100
0.00100
0.00100
0.0100
0.0100
0.0100
0.0100
0.00100
0.0100
0.00100
0.00100
0.0100
0.0100
0.0100
0.00100
0.00100
0.00100
0.0100
0.0100
0.0100
0.00100
0.0100
0.00100
0.0100
0.0100
0.0100
0.0100
0.00100
0.00300
0.00300
0.00300
0.00300
0.00300
FP1
FTC
FSS
[Cn]
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental PILOT 56 L1153593 11/04/1919:55 14 of 22

WG1371001
Semi Volatile Organic Compounds
Method Blank (MB)
(GC/MS) by Method 625.1
QUALITY CONTROL SUMMARY
L1153593-01
ONE LAB. NATIONWIDE.
FP1(MB)
R3466166-2 10/29/19 02:13
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
FTC
Di-n-octyl phthalate U
0.000278
0.00300
Pyrene U
0.000330
0.00100
FSS
1,2,4-Trichlorobenzene U
0.000355
0.0100
4-ChIoro-3-methyl phenol U
0.000263
0.0100
2-Chorophenol U
0.000283
0.0100
rCn
2,4-Dichlorophenol U
0.000284
0.0100
2,4-Dimethylphenol U
0.000624
0.0100
FSr
4,6-Dinitro-2-methylphenol U
0.00262
0.0100
2,4-Dinitrophenol U
0.00325
0.0100
2-Nitrophenol U
0.000320
0.0100
4-Nitrophenol U
0.00201
0.0100
Pentachlorophenol U
0.000313
0.0100
7G1
Phenol U
0.000334
0.0100
2,4,6-Trichlorophenol U
0.000297
0.0100
(S) Nitrobenzene-d5 37.3
15.0-314
FAI
(S) 2-F/uorobipheny/ 51.1
22.0-127
(S) p-Terphenyl-d14 82.9
29.0-141
FSC
(S) Phenol-d5 20.2
8.00-424
(S) 2-Fluorophenol 33.0
10.0-120
(S)2,4,6-Tribromopheno/ 48.5
10.0-153
Laboratory Control Sample (LCS)
(LCS) R3466166-1 10/29/19 01:52
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
%
%
Acenaphthene 0.0500
0.0391
78.2
47.0-145
Acenaphthylene 0.0500
0.0404
80.8
33.0-145
Anthracene 0.0500
0.0396
79.2
27.0-133
Azobenzene 0.0500
0.0420
84.0
37.0-125
Benzidine 0.100
0.0242
24.2
1.00-120
Benzo(a)anth race ne 0.0500
0.0398
79.6
33.0-143
Benzo(b)fluoranthene 0.0500
0.0436
87.2
24.0-159
Benzo(k)fluoranthene 0.0500
0.0429
85.8
11.0-162
Benzo(g,h,i)perylene 0.0500
0.0462
92.4
1.00-219
Benzo(a)pyrene 0.0500
0.0420
84.0
17.0-163
Bis(2-chlorethoxy)methane 0.0500
0.0327
65.4
1.00-219
Bis(2-chloroethyl)ether 0.0500
0.0318
63.6
33.0-185
Bis(2-chloroisopropyl)ether 0.0500
0.0318
63.6
36.0-166
ACCOUNT:
PROJECT: SDG:
DATE/TIME: PAGE:
Pilot Apex Environmental
PILOT 56 L1153593
11/04/1919:55 15 of 22

WG1371001 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1153593-01
Laboratory Control Sample (LCS)
(LCS) R3466166-1 10/29/19 01:52
Spike Amount
Analyte
mg/I
4-Bromophenyl-phenylether
0.0500
2-Chloronaphthalene
0.0500
4-Chlorophenyl-phenylether
0.0500
Chrysene
0.0500
Dibenz(a,h)anth racene
0.0500
3,3-Dichlorobenzidine
0.100
2,4-Dinitrotoluene
0.0500
2,6-Dinitrotoluene
0.0500
Fluoranthene
0.0500
Fluorene
0.0500
Hexachlorobenzene
0.0500
Hexachloro-1,3-butadiene
0.0500
Hexachlorocyclopentadiene
0.0500
Hexachloroethane
0.0500
Indeno(1,2,3-cd)pyrene
0.0500
Isophorone
0.0500
Naphthalene
0.0500
Nitrobenzene
0.0500
n-Nitrosodimethyla mine
0.0500
n-Nitrosodiphenyla mine
0.0500
n-Nitrosodi-n-propylamine
0.0500
Phenanthrene
0.0500
Benzylbutyl phthalate
0.0500
Bis(2-ethylhexyl)phthalate
0.0500
Di-n-butyl phthalate
0.0500
Diethyl phthalate
0.0500
Dimethyl phthalate
0.0500
Di-n-octyl phthalate
0.0500
Pyrene
0.0500
1,2,4-Trichlorobenzene
0.0500
4-Ch I oro-3-m ethyl phenol
0.0500
2-Chlorophenol
0.0500
2,4-Dichlorophenol
0.0500
2,4-Dimethylphenol
0.0500
4,6-Di n itro-2-methyl phen of
0.0500
2,4-Dinitrophenol
0.0500
2-Nitrophenol
0.0500
4-Nitrophenol
0.0500
Pentachlorophenol
0.0500
Phenol
0.0500
ACCOUNT:
Pilot Apex Environmental
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
mg/I
%
%
0.0402
80.4
53.0-127
0.0374
74.8
60.0-120
0.0436
87.2
25.0-158
0.0403
80.6
17.0-168
0.0454
90.8
1.00-227
0.0870
87.0
1.00-262
0.0488
97.6
39.0-139
0.0450
90.0
50.0-158
0.0409
81.8
26.0-137
0.0424
84.8
59.0-121
0.0401
80.2
1.00-152
0.0299
59.8
24.0-120
0.0296
59.2
10.0-120
0.0289
57.8
40.0-120
0.0437
87.4
1.00-171
0.0338
67.6
21.0-196
0.0303
60.6
21.0-133
0.0308
61.6
35.0-180
0.0219
43.8
10.0-120
0.0403
80.6
44.0-120
0.0348
69.6
1.00-230
0.0391
78.2
54.0-120
0.0406
81.2
1.00-152
0.0405
81.0
8.00-158
0.0426
85.2
1.00-120
0.0454
90.8
1.00-120
0.0441
88.2
1.00-120
0.0395
79.0
4.00-146
0.0387
77.4
52.0-120
0.0301
60.2
44.0-142
0.0360
72.0
22.0-147
0.0315
63.0
23.0-134
0.0333
66.6
39.0-135
0.0324
64.8
32.0-120
0.0475
95.0
1.00-181
0.0594
119
1.00-191
0.0351
70.2
29.0-182
0.0230
46.0
1.00-132
0.0483
96.6
14.0-176
0.0157
31.4
5.00-120
PROJECT: SDG: DATE/TIME: PAGE:
PILOT 56 L1153593 11/04/1919:55 16 of 22
FP1
FTc
FSS
4
Cn
FSr
�GI
FAI
FSC

WG1371001 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1153593-01
Laboratory Control Sample (LCS)
(LCS) R3466166-1 10/29/19 01:52
Spike Amount LCS Result
Analyte mg/I mg/I
2,4,6-Trichlorophenol
(S) Nitrobenzene-d5
(S) 2-F/uorobiphenyl
(S) p-Terphenyl-d14
(S) Phenol-d5
(S) 2-Fluorophenol
(S) 2,4,6-Tribromophenol
0.0500 0.0417
LCS Rec.
Rec. Limits LCS Qualifier
83.4
37.0-144
52.4
15.0-314
77.2
22.0-127
80.3
29.0-141
30.4
8.00-424
48.6
10.0-120
83.0
10.0-153
L1153432-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1153432-01 10/29/19 03:17 • (MS) R3466166-3 10/29/19 03:38 • (MSD) R3466166-4 10/29/19 03:59
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
Bis(2-chlorethoxy)methane
0.0500
U
0.0297
0.0302
59.4
60.4
Bis(2-chloroethyl)ether
0.0500
U
0.0294
0.0285
58.8
57.0
Bis(2-chloroisopropyl)ether
0.0500
U
0.0286
0.0286
57.2
57.2
4-Bromophenyl-phenylether
0.0500
U
0.0384
0.0399
76.8
79.8
4-Chlorophenyl-phenylether
0.0500
U
0.0394
0.0421
78.8
84.2
3,3-Dichlorobenzidine
0.100
U
0.0902
0.0945
90.2
94.5
2,4-Dinitrotoluene
0.0500
U
0.0473
0.0490
94.6
98.0
2,6-Dinitrotoluene
0.0500
U
0.0427
0.0453
85.4
90.6
Hexachloro-1,3-butadiene
0.0500
U
0.0281
0.0273
56.2
54.6
Hexachlorocyclopentadiene
0.0500
U
0.0286
0.0287
57.2
57.4
Hexachloroethane
0.0500
U
0.0265
0.0253
53.0
50.6
Isophorone
0.0500
U
0.0312
0.0319
62.4
63.8
Nitrobenzene
0.0500
U
0.0287
0.0288
57.4
57.6
n-Nitrosodiphenyla mine
0.0500
U
0.0390
0.0407
78.0
81.4
n-Nitrosodi-n-propylamine
0.0500
U
0.0316
0.0323
63.2
64.6
Benzylbutyl phthalate
0.0500
U
0.0425
0.0429
85.0
85.8
Bis(2-ethylhexyl)phthalate
0.0500
U
0.0413
0.0416
82.6
83.2
Di-n-butyl phthalate
0.0500
U
0.0426
0.0439
85.2
87.8
Diethyl phthalate
0.0500
U
0.0445
0.0462
89.0
92.4
Dimethyl phthalate
0.0500
U
0.0430
0.0445
86.0
89.0
Di-n-octyl phthalate
0.0500
U
0.0405
0.0408
81.0
81.6
4-ChIoro-3-methyl phenol
0.0500
U
0.0332
0.0342
66.4
68.4
2-Chorophenol
0.0500
U
0.0286
0.0281
57.2
56.2
2,4-Dichlorophenol
0.0500
U
0.0307
0.0309
61.4
61.8
2,4-Dimethylphenol
0.0500
U
0.0301
0.0305
60.2
61.0
4,6-Dinitro-2-methylphenol
0.0500
U
0.0463
0.0502
92.6
100
ACCOUNT: PROJECT:
Pilot Apex Environmental PILOT 56
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 33.0-184
1.67
54
1 12.0-158
3.11
108
1 36.0-166
0.000
76
1 53.0-127
3.83
43
1 25.0-158
6.63
61
1 1.00-262
4.66
108
1 39.0-139
3.53
42
1 50.0-158
5.91
48
1 24.0-120
2.89
62
1 10.0-146
0.349
34
1 40.0-120
4.63
52
1 21.0-196
2.22
93
1 35.0-180
0.348
62
1 16.0-160
4.27
28
1 1.00-230
2.19
87
1 1.00-152
0.937
60
1 8.00-158
0.724
82
1 1.00-120
3.01
47
1 1.00-120
3.75
100
1 1.00-120
3.43
183
1 4.00-146
0.738
69
1 22.0-147
2.97
73
1 23.0-134
1.76
61
1 39.0-135
0.649
50
1 32.0-120
1.32
58
1 1.00-181
8.08
203
SDG:
DATE/TIME:
PAGE:
L1153593
11/04/1919:55
17 of 22
FP1
FTc
FSS
[Cn]
FSr
�GI
FAI
[Sc

WG1371001 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1153593-01
ONE LAB. NATIONWIDE.
L1153432-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1153432-01 10/29/19 03:17 • (MS) R3466166-3 10/29/19 03:38 • (MSD) R3466166-4 10/29/19 03:59
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
2,4-Dinitrophenol
0.0500
U
0.0576
0.0640
115
128
2-Nitrophenol
0.0500
U
0.0320
0.0331
64.0
66.2
4-Nitrophenol
0.0500
U
0.0215
0.0225
43.0
45.0
Pentachlorophenol
0.0500
U
0.0468
0.0516
93.6
103
Phenol
0.0500
U
0.0139
0.0137
27.8
27.4
Acenaphthene
0.0500
U
0.0354
0.0375
70.8
75.0
2,4,6-Trichlorophenol
0.0500
U
0.0393
0.0412
78.6
82.4
Acenaphthylene
0.0500
U
0.0370
0.0385
74.0
77.0
Anthracene
0.0500
U
0.0378
0.0397
75.6
79.4
Azobenzene
0.0500
U
0.0398
0.0423
79.6
84.6
Benzidine
0.100
U
0.0629
0.0573
62.9
57.3
Benzo(a)anth race ne
0.0500
U
0.0403
0.0417
80.6
83.4
Benzo(b)fluoranthene
0.0500
U
0.0423
0.0439
84.6
87.8
Benzo(k)fluoranthene
0.0500
U
0.0431
0.0441
86.2
88.2
Benzo(g,h,i)perylene
0.0500
U
0.0458
0.0467
91.6
93.4
Benzo(a)pyrene
0.0500
U
0.0421
0.0428
84.2
85.6
2-Chloronaphthalene
0.0500
U
0.0340
0.0348
68.0
69.6
Chrysene
0.0500
U
0.0401
0.0419
80.2
83.8
Dibenz(a,h)anthracene
0.0500
U
0.0448
0.0455
89.6
91.0
Fluoranthene
0.0500
U
0.0398
0.0424
79.6
84.8
Fluorene
0.0500
U
0.0393
0.0419
78.6
83.8
Hexachlorobenzene
0.0500
U
0.0386
0.0402
77.2
80.4
Indeno(1,2,3-cd)pyrene
0.0500
U
0.0439
0.0451
87.8
90.2
Naphthalene
0.0500
U
0.0277
0.0279
55.4
55.8
n-Nitrosodimethyla mine
0.0500
U
0.0200
0.0199
40.0
39.8
Phenanthrene
0.0500
U
0.0375
0.0395
75.0
79.0
Pyrene
0.0500
U
0.0396
0.0406
79.2
81.2
1,2,4-Trichlorobenzene
0.0500
U
0.0278
0.0275
55.6
55.0
(S) Nitrobenzene-d5
44.3
46.0
(S) 2-F/uorobipheny/
70.5
71.0
(S) p-Terphenyl-d14
82.7
83.8
(S) Phenol-d5
27.4
27.3
(S) 2-Fluorophenol
43.7
42.3
(S)2,4,6-Tribromopheno/
77.0
84.5
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1.00-191
29.0-182
1.00-132
14.0-176
5.00-120
47.0-145
37.0-144
33.0-145
27.0-133
18.0-156
1.00-120
33.0-143
24.0-159
11.0-162
1.00-219
17.0-163
60.0-120
17.0-168
1.00-227
26.0-137
59.0-121
1.00-152
1.00-171
21.0-133
10.0-120
54.0-120
52.0-120
44.0-142
15.0-314
22.0-127
29.0-141
8.00-424
10.0-120
10.0-153
10.5
3.38
4.55
9.76
1.45
5.76
4.72
3.97
4.90
6.09
9.32
3.41
3.71
2.29
1.95
1.65
2.33
4.39
1.55
6.33
6.40
4.06
2.70
0.719
0.501
5.19
2.49
1.08
RPD Limits
132
55
131
86
64
48
58
74
66
34
40
53
71
63
97
72
24
87
126
66
38
55
99
65
40
39
49
50
FP1
FTc
FSS
[Cn]
FSr
�GI
FAI
[Sc
ACCOUNT: PROJECT: SDG:
Pilot Apex Environmental PILOT 56 L1153593
DATE/TIME:
11/04/1919:55
PAGE:
18 of 22

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE.
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
CP
IP
FTC
FSS
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
[Cn]
RDL
Reported Detection Limit.
Rec.
Recovery.
FSr
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
6
QC
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
a
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
FSC
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
J
The identification of the analyte is acceptable; the reported value is an estimate.
N
The analyte is tentatively identified and the associated numerical value may not be consistent with the actual
concentration present in the sample.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental
PILOT 56 L1153593 11/04/1919:55 19 of 22

ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z
Tc
State Accreditations
f—�
Alabama
40660
Nebraska _
NE-OS-15-05
SS
Alaska
17-026
Nevada
TN-03-2002-34
Arizona
AZO612
New Hampshire
2975
Arkansas
88-0469
New Jersey_NELAP
TNO02
C n
California
2932
New Mexico
n/a
Colorado
TN00003
New York
11742
s
Connecticut
PH-0197
North Carolina
Env375
Sr
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina'
41
Georgia'
923
North Dakota
R-140
RC
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
G
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky76
90010
South Carolina
84004
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' 4
2006
Louisiana'
LA180010
Texas
T104704245-18-15
[SC
Maine
TN0002
Texas'
LABO152
Maryland
324
Utah
Massachusetts
M-TNO03
Vermont
Michigan
9958
Virginia
Minnesota
047-999-395
Washington
Mississippi
TN00003
West Virginia
Missouri
340
Wisconsin
Montana
CERT0086
Wyoming
Third Party
Federal Accreditations
A21LA — ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
A21LA — ISO 17025 5
1461.02
DOD
Canada
1461.01
USDA
EPA—Crypto
TN00003
' Drinking Water 'Underground
Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
TN00003
VT2006
460132
C847
233
9980939910
A2LA
100789
1461.01
P330-15-00234
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
WA
ME
MT NO
OR MN
T ID t WI NY
SD
WY MI
NV
t NE IA OH PA
T f IL Ills WV
vA
UT T
CA�� T
KS MO KY
N
NM O� AR SC
T MS AL`7GA
T TX * LA
T
AK
q FL
wo HI
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental PILOT 56 L1153593 11/04/1919:55 20 of 22

CHAIN -OF -CUSTODY Analytical Request Document
paceAnaivtical
Chain -of -Custody is a LEGAL DOCUMENT - Complete all relevent fields
paw
Billing Information
5508 Lonl[5 Rdl
ess:
27-0Lk r l_ .A C, ,. i WJ Kwxvitic, TN
Phone: 3yo - T(, 3 _'li Site/Facility lD p:
Email:
Cd
L[' Purchase Order q:
_W, _6fY Quote It
Date Required:
To:
_ rAJ1 Rai ED—
ollection Info/Address:
Pt1DAF"r-Ktnv-QIv-6()
County/City: Time Zone Collected:
/ K"n( OI 1Yj [ I PT ( ] MT [ I CT [J] ET
Compliance Monitoring?
I I yes I I No
DW PWS 10 k:
DW Location Code:
"YesI No
Sample Disposal: Rush: Field Filtered (if applicablep.
I I Dispose as appropriate I I Return
1,11I Archive. I I Same Day I ] Next Day / I I yes [ I No
I I Hold: [ 12 Day ( 1.3 Day I ] 4 Day [J] S Day
( Expedite Charges Apply) Analysis:
"Matrix Codes (Insert in Matrix box below): Drinking Water (D W ), Ground Water (G W ), Wastewater (W W ),
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT)
Customer Sample lD
CO°rP/ Colle'I'd(or=EodCI
Matrix' Grab Compositestart)
Com
Customer Remarks/ Special Co nditions/Pn'.'' ( Ha+arus
� erhP - � • I °c
:elir1puBhed bVCompany: (Signature) T
(Signature)
ype of Ice Used: Wet Blue Dry None
3ckmg MetCrlal Used:
sample(s) screened (<Soo cpm): Y N NA
Recejyed by/Company (Signature)
t (000 15�
LAB USE ONLY- Affix Workorder/Login Label Here or List Pace W orkorder Number or
MTJL Log -in Number Here
ALL SHADED AREAS are for LAB USE ONLY
>reservative Type " ILab Project Manager:
•' Preservative Types: Ill nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate,
(6) methanol, 0) sodium bisulfate, (8) sodium Nlosulfate, (9) hexane, (A) ascorbic acid, (B) ammonium sulfate,
(Q ammonium hydroxide. Ud TSP. IUl Unoreserved. (01 Other
a
HT HOLDS PRESENT (<72 hours): Y N N/A
Tracking g: 2410405
Custody Seals Present/Intact 4PN NA
Custody Signatures Present 4VN NA
Collector Signature Present 11N NA
Bottles intact
%N NA
Correct Bottles
.{N NA
Sufficient Volume
N NA
Samples Received on Ice
Y N NA
VOA - Headspace Acceptable
V N NA
USDA Regulated Soils
Y N ➢Rf
Samples in Holding Time
Ir N NA
Residual Chlorine Present
Y N KA
Cl Strips:
Sample pH Acceptable
Y N NA
pH Strips:
Sulfide Present
Y N )rA
Lead Acetate Strips: _
Iff-I-MIM AUM
Lab Sample J[ �Comments
A105
pies received via:
FEDEX UPS Client Courier Pace Courier
Date/Time: I MTJL LAB USE ONLY
Lab Sample Temperature Info:
Temp Blank Received Y N NA
Therm IDg: _11 "N
Cooler 1 Temp Upon Receipt:
oC
Cooler 1 Therm Corr. Factor _x_oC
Cooler 1 Corrected Temp: _a,3_oc
Comments'.
PAD SCREEN: <0.5 mMr
Trip Blank Received. Y N NA
HCL McOH TSP Other
Non Conform nce(s): Page:
YES / of: /

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aceAnalytical o ANALYTICAL REPORT
National Center for Testing & Innovation November 08, 2019
• #r
Pilot Apex Environmental
Sample Delivery Group: L1153643
Samples Received: 10/24/2019
Project Number:
Description: Pilot 56
Report To: Robert Wagner
7724 Garland Circle
Roanoke, VA 24019
Entire Report Reviewed By:
Pam Langford
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
4
V -
16
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 1 of 40

TABLE OF CONTENTS
ONE LAB. NATIONWIDE.
Cp: Cover Page
Tc: Table of Contents
Ss: Sample Summary
Cn: Case Narrative
Sr: Sample Results
MW-Al L1153643-01
SB-1 L1153643-02
Qc: Quality Control Summary
Total Solids by Method 2540 G-2011
Volatile Petroleum Hydrocarbons by Method MADEPV
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
Volatile Organic Compounds (GC/MS) by Method 8260D
TPH by Method MADEPE
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
GI: Glossary of Terms
Al: Accreditations & Locations
Sc: Sample Chain of Custody
1
2
3
4
5
5
8
12
12
13
15
19
24
27
32
38
39
40
Fn
FS
[Cn]
FS-r
RC
F,
rAl
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 2 of 40

SAMPLE SUMMARY ONE LAB. NATIONWIDE.
Collected by Collected date/time Received date/time
MW-Al L1153643-01 GW Evan Everson 10/23/1915:50 10/24/1908:45 C
P
Method
Volatile Petroleum Hydrocarbons by Method MADEPV
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
TPH by Method MADEPE
TPH by Method MADEPE
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
S13-1 L1153643-02 Solid
Batch Dilution Preparation Analysis Analyst Location
date/time date/time
WG1374871
1 11/06/19 02:36
11/06/19 02:36
BMB
Mt. Juliet, TN
WG1374390
1 11/04/19 01:14
11/04/19 01:14
JSD
Mt. Juliet, TN
WG1371908
1 10/29/1917:39
11/01/1915:25
SHG
Mt. Juliet, TN
WG1371908
1 10/29/1917:39
11/01/1916:40
SHG
Mt. Juliet, TN
WG1371001
1 10/28/1917:01
10/29/19 02:08
LEA
Mt. Juliet, TN
Collected by
Collected date/time
Received date/time
Evan Everson
10/23/19 12:05
10/24/19 08:45
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
Total Solids by Method 2540 G-2011
WG1372541
1 10/31/1911:13
10/31/1911:23
KDW
Mt. Juliet, TN
Volatile Petroleum Hydrocarbons by Method MADEPV
WG1370282
1 10/23/1912:05
10/27/19 02:13
HJF
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1374670
1 10/23/1912:05
11/04/1913:29
ACG
Mt. Juliet, TN
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1375172
1 10/23/1912:05
11/05/1916:01
ACG
Mt. Juliet, TN
TPH by Method MADEPE
WG1372377
1 10/30/1912:00
11/03/19 02:43
KME
Mt. Juliet, TN
TPH by Method MADEPE
WG1372377
1 10/30/1912:00
11/03/19 08:09
KME
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG1370556
1 10/27/1918:34
10/28/19 01:47
AO
Mt. Juliet, TN
FTC
M
[Cn]
FSr
RC
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 3 of 40

CASE NARRATIVE
ONE LAB. NATIONWIDE.
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
Pam Langford
Project Manager
FP1
FTC
FSS
FSr
6
QC
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 4 of 40

SAMPLE RESULTS - 01
L1153643
ONE LAB. NATIONWIDE.
M W-A1
Collected date/time: 10/23/19 15:50
Additional Information
Result Units
Analyte
pH (On Site) 6.73 su
Temperature (on -site) 21.6 Deg C
Volatile Petroleum Hydrocarbons by Method MADEPV
Result
Qualifier RDL Dilution
Analysis
Batch
Analyte
mg/I
_ mg/I
date / time
Unadjusted C5-C8 Aliphatics
ND
0.100 1
11/06/2019 02:36
WG1374871
Unadjusted C9-C12 Aliphatics
ND
0.100 1
11/06/2019 02:36
WG1374871
Unadjusted C9-C10 Aromatics
ND
0.100 1
11/06/2019 02:36
WG1374871
Total VPH
ND
0.100 1
11/06/2019 02:36
WG1374871
(S) 2,5-Dibromotoluene(FID)
108
70.0-130
1110612019 02:36
WG1374871
(S) 2,5-Dibromotoluene(PID)
97.3
70.0-130
1110612019 02:36
WG1374871
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
Result
Qualifier RDL Dilution
Analysis
Batch
Analyte
mg/I
mg/I
date / time
Acetone
ND
0.0500 1
11/04/2019 01:14
WG1374390
Acrolein
ND
0.0500 1
11/04/2019 01:14
WG1374390
Acrylonitrile
ND
0.0100 1
11/04/2019 01:14
WG1374390
Benzene
ND
0.00100 1
11/04/2019 01:14
WG1374390
Bromobenzene
ND
0.00100 1
11/04/2019 01:14
WG1374390
Bromodichloromethane
ND
0.00100 1
11/04/2019 01:14
WG1374390
Bromoform
ND
0.00100 1
11/04/2019 01:14
WG1374390
Bromomethane
ND
J4 0.00500 1
11/04/2019 01:14
WG1374390
n-Butylbenzene
ND
0.00100 1
11/04/2019 01:14
WG1374390
sec -Butyl benzene
ND
0.00100 1
11/04/2019 01:14
WG1374390
tert-Butylbenzene
ND
0.00100 1
11/04/2019 01:14
WG1374390
Carbon tetrachloride
ND
0.00100 1
11/04/2019 01:14
WG1374390
Chlorobenzene
ND
0.00100 1
11/04/2019 01:14
WG1374390
Chlorodibromomethane
ND
0.00100 1
11/04/2019 01:14
WG1374390
Chloroethane
ND
0.00500 1
11/04/2019 01:14
WG1374390
Chloroform
ND
0.00500 1
11/04/2019 01:14
WG1374390
Chloromethane
ND
0.00250 1
11/04/2019 01:14
WG1374390
2-Chlorotoluene
ND
0.00100 1
11/04/2019 01:14
WG1374390
4-Chlorotoluene
ND
0.00100 1
11/04/2019 01:14
WG1374390
1,2-Dibromo-3-Chloropropane
ND
0.00500 1
11/04/2019 01:14
WG1374390
1,2-Dibromoethane
ND
0.00100 1
11/04/2019 01:14
WG1374390
Dibromomethane
ND
0.00100 1
11/04/2019 01:14
WG1374390
1,2-Dichlorobenzene
ND
0.00100 1
11/04/2019 01:14
WG1374390
1,3-Dichlorobenzene
ND
0.00100 1
11/04/2019 01:14
WG1374390
1,4-Dichlorobenzene
ND
0.00100 1
11/04/2019 01:14
WG1374390
Dichlorodifluoromethane
ND
0.00500 1
11/04/2019 01:14
WG1374390
1,1-Dichloroethane
ND
0.00100 1
11/04/2019 01:14
WG1374390
1,2-Dichloroethane
ND
0.00100 1
11/04/2019 01:14
WG1374390
1,1-Dichloroethene
ND
0.00100 1
11/04/2019 01:14
WG1374390
cis-1,2-Dichloroethene
ND
0.00100 1
11/04/2019 01:14
WG1374390
trans-1,2-Dichloroethene
ND
0.00100 1
11/04/2019 01:14
WG1374390
1,2-Dichloropropane
ND
0.00100 1
11/04/2019 01:14
WG1374390
1,1-Dichloropropene
ND
0.00100 1
11/04/2019 01:14
WG1374390
1,3-Dichloropropane
ND
0.00100 1
11/04/2019 01:14
WG1374390
2,2-Dichloropropane
ND
0.00100 1
11/04/2019 01:14
WG1374390
Di -isopropyl ether
ND
0.00100 1
11/04/2019 01:14
WG1374390
Ethylbenzene
ND
0.00100 1
11/04/2019 01:14
WG1374390
Hexachloro-1,3-butadiene
ND
0.00100 1
11/04/2019 01:14
WG1374390
IsoorODVlbenzene
ND
0.00100 1
11/04/2019 01:14
WG1374390
FP1
FTc
FSS
4
Cn
Fc
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 5 of 40

MW-Al SAMPLE RESULTS - 01
Collected date/time: 10/23/19 15:50 L1153643
Volatile Organic Compounds (GC/MS) by Method 620OB-2011
ONE LAB. NATIONWIDE.
Analyte
p-Isopropyltoluene
2-Butanone (MEK)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1, 2-Tet ra c h l o ro et h a n e
1,1,2,2-Tetrachloroetha ne
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Tri ch to roetha ne
1,1,2-Trich I oroetha n e
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Tri methyl ben zen e
1,3,5-Trim ethyl benzene
Vinyl chloride
o-Xylene
m&p-Xylenes
(S) Toluene-d8
(S) 4-Bromofluorobenzene
(S) 1,2-Dich/oroethone-d4
TPH by Method MADEPE
Analyte
Unadjusted C9-C18 Aliphatics
Unadjusted C19-C36 Aliphatics
Unadjusted C11-C22 Aromatics
Unadjusted Total Petroleum
Hydrocarbons
(S) o-Terphenyl
(S)1-Chloro-octadecane
(S) 2-F/uorobiphenyl
(S) 2-Bromonaphtha/ene
Result
Qualifier RDL
Dilution Analysis
mg/I
mg/I
date / time
ND
0.00100
1 11/04/2019 01:14
ND
0.0100
1 11/04/2019 01:14
ND
0.00500
1 11/04/2019 01:14
ND
0.0100
1 11/04/2019 01:14
ND
0.00100
1 11/04/2019 01:14
ND
0.00500
1 11/04/2019 01:14
ND
0.00100
1 11/04/2019 01:14
ND
0.00100
1 11/04/2019 01:14
ND
0.00100
1 11/04/2019 01:14
ND
0.00100
1 11/04/2019 01:14
ND
0.00100
1 11/04/2019 01:14
ND
0.00100
1 11/04/2019 01:14
ND
0.00100
1 11/04/2019 01:14
ND
0.00100
1 11/04/2019 01:14
ND
0.00100
1 11/04/2019 01:14
ND
0.00100
1 11/04/2019 01:14
ND
0.00100
1 11/04/2019 01:14
ND
0.00500
1 11/04/2019 01:14
ND
0.00250
1 11/04/2019 01:14
ND
0.00100
1 11/04/2019 01:14
ND
0.00100
1 11/04/2019 01:14
ND
0.00100
1 11/04/2019 01:14
ND
0.00100
1 11/04/2019 01:14
ND
0.00200
1 11/04/2019 01:14
109
80.0-120
1110412019 01:14
108
77.0-126
1110412019 01:14
105
70.0-130
1110412019 01:14
Result
Qualifier RDL
Dilution Analysis
mg/I
mg/I
date / time
ND
0.100
1 11/01/201915:25
ND
0.100
1 11/01/201915:25
ND
0.100
1 11/01/201916:40
ND
0.100
1 11/01/201915:25
69.5
40.0-140
111011201916.'40
63.8
40.0-140
11101120191525
84.7
40.0-140
111011201916:40
80.7
40.0-140
111011201916.'40
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Batch
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
WG1374390
Batch
WG1371908
WG1371908
WG1371908
WG1371908
WG1371908
WG1371908
WG1371908
WG1371908
Result
Qualifier RDL
Dilution Analysis
Batch
Analyte
mg/I
mg/I
date / time
Acenaphthene
ND
0.00100
1 10/29/2019 02:08
WG1371001
Acenaphthylene
ND
0.00100
1 10/29/2019 02:08
WG1371001
Anthracene
ND
0.00100
1 10/29/2019 02:08
WG1371001
Benzidine
ND
0.0100
1 10/29/2019 02:08
WG1371001
Benzo(a)anth race ne
ND
0.00100
1 10/29/2019 02:08
WG1371001
Benzo(b)fluoranthene
ND
0.00100
1 10/29/2019 02:08
WG1371001
Benzo(k)fuoranthene
ND
0.00100
1 10/29/2019 02:08
WG1371001
Benzo(g,h,i)perylene
ND
0.00100
1 10/29/2019 02:08
WG1371001
Benzo(a)pyrene
ND
0.00100
1 10/29/2019 02:08
WG1371001
Bis(2-chlorethoxy)methane
ND
0.0100
1 10/29/2019 02:08
WG1371001
Bis(2-chloroethyl)ether
ND
0.0100
1 10/29/2019 02:08
WG1371001
Bis(2-chloroisopropyl)ether
ND
0.0100
1 10/29/2019 02:08
WG1371001
Cp
FTc
FSS
4
Cn
Fc
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 6 of 40

ONE LAB. NATIONWIDE.
MW-Al SAMPLE RESULTS - 01
Collected date/time: 10/23/19 15:50 L1153643
Semi Volatile Organic Compounds (GC/MS) by Method 625.1
Result
Qualifier RDL
Dilution Analysis
Batch
Analyte
mg/I
mg/I
date / time
4-Bromophenyl-phenylether
ND
0.0100
1 10/29/2019 02:08
WG1371001
2-Chloronaphthalene
ND
0.00100
1 10/29/2019 02:08
WG1371001
4-Chlorophenyl-phenylether
ND
0.0100
1 10/29/2019 02:08
WG1371001
Chrysene
ND
0.00100
1 10/29/2019 02:08
WG1371001
Dibenz(a,h)anthracene
ND
0.00100
1 10/29/2019 02:08
WG1371001
3,3-Dichlorobenzidine
ND
0.0100
1 10/29/2019 02:08
WG1371001
2,4-Dinitrotoluene
ND
0.0100
1 10/29/2019 02:08
WG1371001
2,6-Dinitrotoluene
ND
0.0100
1 10/29/2019 02:08
WG1371001
Fluoranthene
ND
0.00100
1 10/29/2019 02:08
WG1371001
Fluorene
ND
0.00100
1 10/29/2019 02:08
WG1371001
Hexachlorobenzene
ND
0.00100
1 10/29/2019 02:08
WG1371001
Hexachloro-1,3-butadiene
ND
0.0100
1 10/29/2019 02:08
WG1371001
Hexachlorocyclopentadiene
ND
0.0100
1 10/29/2019 02:08
WG1371001
Hexachloroethane
ND
0.0100
1 10/29/2019 02:08
WG1371001
Indeno(1,2,3-cd)pyrene
ND
0.00100
1 10/29/2019 02:08
WG1371001
Isophorone
ND
0.0100
1 10/29/2019 02:08
WG1371001
Naphthalene
ND
0.00100
1 10/29/2019 02:08
WG1371001
Nitrobenzene
ND
0.0100
1 10/29/2019 02:08
WG1371001
n-Nitrosodimethyla mine
ND
0.0100
1 10/29/2019 02:08
WG1371001
n-Nitrosodiphenyla mine
ND
0.0100
1 10/29/2019 02:08
WG1371001
n-Nitrosodi-n-propylamine
ND
0.0100
1 10/29/2019 02:08
WG1371001
Phenanthrene
ND
0.00100
1 10/29/2019 02:08
WG1371001
Benzylbutyl phthalate
ND
0.00300
1 10/29/2019 02:08
WG1371001
Bis(2-ethylhexyl)phthalate
ND
0.00300
1 10/29/2019 02:08
WG1371001
Di-n-butyl phthalate
ND
0.00300
1 10/29/2019 02:08
WG1371001
Diethyl phthalate
ND
0.00300
1 10/29/2019 02:08
WG1371001
Dimethyl phthalate
ND
0.00300
1 10/29/2019 02:08
WG1371001
Di-n-octyl phthalate
ND
0.00300
1 10/29/2019 02:08
WG1371001
Pyrene
ND
0.00100
1 10/29/2019 02:08
WG1371001
1,2,4-Trichlorobenzene
ND
0.0100
1 10/29/2019 02:08
WG1371001
4-ChIoro-3-methyl phenol
ND
0.0100
1 10/29/2019 02:08
WG1371001
2-Chlorophenol
ND
0.0100
1 10/29/2019 02:08
WG1371001
2,4-Dichlorophenol
ND
0.0100
1 10/29/2019 02:08
WG1371001
2,4-Dimethylphenol
ND
0.0100
1 10/29/2019 02:08
WG1371001
4,6-Dinitro-2-methylphenol
ND
0.0100
1 10/29/2019 02:08
WG1371001
2,4-Dinitrophenol
ND
0.0100
1 10/29/2019 02:08
WG1371001
2-Nitrophenol
ND
0.0100
1 10/29/2019 02:08
WG1371001
4-Nitrophenol
ND
0.0100
1 10/29/2019 02:08
WG1371001
Pentachlorophenol
ND
0.0100
1 10/29/2019 02:08
WG1371001
Phenol
ND
0.0100
1 10/29/2019 02:08
WG1371001
2,4,6-Trichlorophenol
ND
0.0100
1 10/29/2019 02:08
WG1371001
(S) 2-F/uorophenol
30.1
10.0-120
1012912019 02:08
WG1371001
(S) Phenol-d5
17.8
8.00-424
1012912019 02:08
WG1371001
(S) Nitrobenzene-d5
36.8
15.0-314
1012912019 02:08
WG1371001
(S) 2-Fluorobiphenyl
46.0
22.0-127
1012912019 02:08
WG1371001
(S)2,4,6-Tribromopheno/
49.4
10.0-153
1012912019 02:08
WG1371001
(S) p-Terphenyl-d14
76.4
29.0-141
1012912019 02:08
WG1371001
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 - TENTATIVELY IDENTIFIED COMPOUNDS
Result Qualifier RDL Dilution Analysis Batch CAS #
Analyte mg/I mg/I date / time
Unknown-01 0.00480 J N 0.000 1 10/29/2019 02:08 WG1371001 031396-33-5
Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds. Therefore, not all TICS are identified and quantitated using individual standards. TIC
listings are prepared utilizing a computerized library search routine of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist. Quantitation is
accomplished by relative peak area of the TIC compared to that of the nearest internal standard from the total ion chromatogram. TICs are identified and quantitated only if the peak area is
10% or more of that of the nearest internal standard.
FP
FTC
FS
Fn
N
FC]
F
FAI
FSC
ACCOUNT:
Pilot Apex Environmental
PROJECT: SDG: DATE/TIME: PAGE:
L1153643 11/08/19 14:17 7 of 40

SAMPLE RESULTS - 02
L1153643
ONE LAB. NATIONWIDE.
SB-1
Collected date/time: 10/23/19 12:05
Additional Information
Result
Analyte
pH (On Site) 6.73
Temperature (on -site) 21.6
Total Solids by Method 2540 G-2011
Units
su
Deg C
Result Qualifier Dilution Analysis Batch
Analyte % date / time
Total Solids 88.9 1 10/31/201911:23 WG1372541
Volatile Petroleum Hydrocarbons by Method MADEPV
Result
Qualifier RDL Dilution
Analysis
Batch
Analyte
mg/kg
mg/kg
date / time
Unadjusted C5-C8 Aliphatics
ND
5.00 1
10/27/2019 02:13
WG1370282
Unadjusted C9-C12 Aliphatics
12.5
5.00 1
10/27/2019 02:13
WG1370282
Unadjusted C9-C10 Aromatics
6.17
5.00 1
10/27/2019 02:13
WG1370282
Total VPH
18.7
5.00 1
10/27/2019 02:13
WG1370282
(S) 2,5-Dibromotoluene(FID)
109
70.0-130
1012712019 02:13
WG1370282
(S) 2,5-Dibromotoluene(PID)
81.7
70.0-130
1012712019 02:13
WG1370282
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Analyte
mg/kg
Acetone
ND
Acrylonitrile
ND
Benzene
ND
Bromobenzene
ND
Bromodichloromethane
ND
Bromoform
ND
Bromomethane
ND
n-Butylbenzene
ND
sec -Butyl benzene
0.0197
tert-Butylbenzene
ND
Carbon tetrachloride
ND
Chlorobenzene
ND
Chlorodibromomethane
ND
Chloroethane
ND
Chloroform
ND
Chloromethane
ND
2-Chlorotoluene
ND
4-Chlorotoluene
ND
1,2-Dibromo-3-Chloropropane
ND
1,2-Dibromoethane
ND
Dibromomethane
ND
1,2-Dichlorobenzene
ND
1,3-Dichlorobenzene
ND
1,4-Dichlorobenzene
ND
Dichlorodifluoromethane
ND
1,1-Dichloroethane
ND
1,2-Dichloroethane
ND
1,1-Dichloroethene
ND
cis-1,2-Dichloroethene
ND
trans-1,2-Dichloroethene
ND
1,2-Dichloropropane
ND
1,1-Dichloropropene
ND
1,3-Dichloropropane
ND
ACCOUNT:
Pilot Apex Environmental
Qualifier RDL Dilution Analysis Batch
mg/kg date / time
0.0250 1
11/04/2019 13:29
WG1374670
0.0125 1
11/04/2019 13:29
WG1374670
0.00100 1
11/04/2019 13:29
WG1374670
0.0125 1
11/04/2019 13:29
WG1374670
0.00250 1
11/04/2019 13:29
WG1374670
0.0250 1
11/04/2019 13:29
WG1374670
0.0125 1
11/04/2019 13:29
WG1374670
0.0125 1
11/04/2019 13:29
WG1374670
0.0125 1
11/04/2019 13:29
WG1374670
0.00500 1
11/04/2019 13:29
WG1374670
0.00500 1
11/04/2019 13:29
WG1374670
0.00250 1
11/04/2019 13:29
WG1374670
0.00250 1
11/04/2019 13:29
WG1374670
0.00500 1
11/04/2019 13:29
WG1374670
0.00250 1
11/04/2019 13:29
WG1374670
0.0125 1
11/04/2019 13:29
WG1374670
0.00250 1
11/04/2019 13:29
WG1374670
0.00500 1
11/04/2019 13:29
WG1374670
0.0250 1
11/04/2019 13:29
WG1374670
0.00250 1
11/04/2019 13:29
WG1374670
0.00500 1
11/04/2019 13:29
WG1374670
0.00500 1
11/04/2019 13:29
WG1374670
0.00500 1
11/04/2019 13:29
WG1374670
0.00500 1
11/04/2019 13:29
WG1374670
0.00250 1
11/04/2019 13:29
WG1374670
0.00250 1
11/04/2019 13:29
WG1374670
0.00250 1
11/04/2019 13:29
WG1374670
0.00250 1
11/04/2019 13:29
WG1374670
0.00250 1
11/04/2019 13:29
WG1374670
0.00500 1
11/04/2019 13:29
WG1374670
0.00500 1
11/04/2019 13:29
WG1374670
0.00250 1
11/04/2019 13:29
WG1374670
0.00500 1
11/04/2019 13:29
WG1374670
PROJECT: SDG:
L1153643
FP1
FTC
FSS
4
Cn
Fc
F
FAI
FSC
DATE/TIME: PAGE:
11/08/19 14:17 8 of 40

ONE LAB. NATIONWIDE.
SB-1 SAMPLE RESULTS - 02
Collected date/time: 10/23/19 12:05 L1153643
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL
Dilution Analysis
Batch
Analyte
mg/kg
mg/kg
date / time
cis-1,3-Dichloropropene
ND
0.00250
1 11/04/201913:29
WG1374670
trans-1,3-Dichloropropene
ND
0.00500
1 11/04/201913:29
WG1374670
2,2-Dichloropropane
ND
0.00250
1 11/04/201913:29
WG1374670
Di -isopropyl ether
ND
0.00100
1 11/04/201913:29
WG1374670
Ethylbenzene
ND
0.00250
1 11/04/201913:29
WG1374670
Hexachloro-1,3-butadiene
ND
0.0250
1 11/04/201913:29
WG1374670
Isopropylbenzene
ND
0.00250
1 11/04/201913:29
WG1374670
p-Isopropyltoluene
ND
0.00500
1 11/04/201913:29
WG1374670
2-Butanone (MEK)
0.0307
B 0.0250
1 11/04/201913:29
WG1374670
Methylene Chloride
ND
0.0250
1 11/04/201913:29
WG1374670
4-Methyl-2-pentanone (MIBK)
ND
0.0250
1 11/04/201913:29
WG1374670
Methyl tert-butyl ether
ND
0.00100
1 11/04/201913:29
WG1374670
Naphthalene
ND
0.0125
1 11/04/201913:29
WG1374670
n-Propylbenzene
ND
0.00500
1 11/04/201913:29
WG1374670
Styrene
ND
0.0125
1 11/04/201913:29
WG1374670
1,1,1,2-Tetrachloroethane
ND
0.00250
1 11/04/201913:29
WG1374670
1,1,2,2-Tetrachloroethane
ND
0.00250
1 11/04/201913:29
WG1374670
1,1,2-Trichlorotrifluoroethane
ND
0.00250
1 11/04/201913:29
WG1374670
Tetrachloroethene
ND
0.00250
1 11/04/201913:29
WG1374670
Toluene
ND
0.00500
1 11/04/201913:29
WG1374670
1,2,3-Trichlorobenzene
ND
0.00250
1 11/05/201916:01
WG1375172
1,2,4-Trichlorobenzene
ND
0.0125
1 11/04/201913:29
WG1374670
1,1,1-Trichloroethane
ND
0.00250
1 11/04/201913:29
WG1374670
1,1,2-Trichloroethane
ND
0.00250
1 11/04/201913:29
WG1374670
Trichloroethene
ND
0.00100
1 11/04/201913:29
WG1374670
Trichlorofluoromethane
ND
0.00250
1 11/04/201913:29
WG1374670
1,2,3-Trichloropropane
ND
0.0125
1 11/04/201913:29
WG1374670
1,2,4-Trimethylbenzene
ND
0.00500
1 11/04/201913:29
WG1374670
1,2,3-Trimethyl benzene
ND
0.00500
1 11/04/201913:29
WG1374670
1,3,5-Trimethyl benzene
ND
0.00500
1 11/04/201913:29
WG1374670
Vinyl chloride
ND
0.00250
1 11/04/201913:29
WG1374670
Xylenes, Total
ND
0.00650
1 11/04/201913:29
WG1374670
(S) Toluene-d8
113
75.0-131
111041201913:29
WG1374670
(S) Toluene-d8
104
75.0-131
111051201916:01
WG1375172
(S) 4-Bromof/uorobenzene
115
67.0-138
111041201913:29
WG1374670
(S) 4-Bromofluorobenzene
102
67.0-138
111051201916:01
WG1375172
(S)1,2-Dich/oroethone-d4
91.4
70.0-130
111041201913:29
WG1374670
(S)1,2-Dich/oroethone-d4
91.2
70.0-130
111051201916:01
WG1375172
TPH by Method MADEPE
Analyte
Unadjusted C9-C18 Aliphatics
Unadjusted C19-C36 Aliphatics
Unadjusted C11-C22 Aromatics
Unadjusted Total Petroleum
Hydrocarbons
(S) o-Terphenyl
(S)1-Chloro-octadecane
(S) 2-F/uorobiphenyl
(S) 2-Bromonaphtha/ene
Result
Qualifier RDL
Dilution Analysis
mg/kg
mg/kg
date / time
49.1
6.50
1 11/03/2019 02:43
18.7
6.50
1 11/03/2019 02:43
50.2
6.50
1 11/03/2019 08:09
118
6.50
1 11/03/2019 08:09
82.0
40.0-140
1110312019 08:09
67.7
40.0-140
1110312019 02:43
106
40.0-140
1110312019 08:09
108
40.0-140
1110312019 08:09
Batch
WG1372377
WG1372377
WG1372377
WG1372377
WG1372377
WG1372377
WG1372377
WG1372377
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 9 of 40

S B-1 SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE.
Collected date/time: 10/23/19 12:05 L1153643
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result
Qualifier RDL Dilution
Analysis
Batch
I Cl7
Analyte
mg/kg
mg/kg
date / time
u
1,4-Dichlorobenzene
ND
0.333 1
10/28/2019 01:47
WG1370556
FTc
Acenaphthene
0.0343
0.0333 1
10/28/2019 01:47
WG1370556
Acenaphthylene
ND
0.0333 1
10/28/2019 01:47
WG1370556
Anthracene
ND
0.0333 1
10/28/2019 01:47
WG1370556
FS
Benzidine
ND
0.333 1
10/28/2019 01:47
WG1370556
Benzo(a)anth race ne
ND
0.0333 1
10/28/2019 01:47
WG1370556
[Cn]
Benzo(b)fluoranthene
ND
0.0333 1
10/28/2019 01:47
WG1370556
Benzo(k)fluoranthene
ND
0.0333 1
10/28/2019 01:47
WG1370556
Benzo(g,h,i)perylene
ND
0.0333 1
10/28/2019 01:47
WG1370556
Benzo(a)pyrene
ND
0.0333 1
10/28/2019 01:47
WG1370556
Bis(2-chlorethoxy)methane
ND
0.333 1
10/28/2019 01:47
WG1370556
FC]
Bis(2-chloroethyl)ether
ND
0.333 1
10/28/2019 01:47
WG1370556
Bis(2-chloroisopropyl)ether
ND
0.333 1
10/28/2019 01:47
WG1370556
4-Bromophenyl-phenylether
ND
0.333 1
10/28/2019 01:47
WG1370556
ql
2-Chloronaphthalene
ND
0.0333 1
10/28/2019 01:47
WG1370556
4-Chlorophenyl-phenylether
ND
0.333 1
10/28/2019 01:47
WG1370556
FAI
Chrysene
ND
0.0333 1
10/28/2019 01:47
WG1370556
Dibenz(a,h)anth racene
ND
0.0333 1
10/28/2019 01:47
WG1370556
3,3-Dichlorobenzidine
ND
0.333 1
10/28/2019 01:47
WG1370556
FSC
2,4-Dinitrotoluene
ND
0.333 1
10/28/2019 01:47
WG1370556
2,6-Dinitrotoluene
ND
0.333 1
10/28/2019 01:47
WG1370556
Fluoranthene
ND
0.0333 1
10/28/2019 01:47
WG1370556
Fluorene
ND
0.0333 1
10/28/2019 01:47
WG1370556
Hexachlorobenzene
ND
0.333 1
10/28/2019 01:47
WG1370556
Hexachloro-1,3-butadiene
ND
0.333 1
10/28/2019 01:47
WG1370556
Hexachlorocyclopentadiene
ND
0.333 1
10/28/2019 01:47
WG1370556
Hexachloroethane
ND
0.333 1
10/28/2019 01:47
WG1370556
Indeno(1,2,3-cd)pyrene
ND
0.0333 1
10/28/2019 01:47
WG1370556
Isophorone
ND
0.333 1
10/28/2019 01:47
WG1370556
Naphthalene
0.0344
B 0.0333 1
10/28/2019 01:47
WG1370556
Nitrobenzene
ND
0.333 1
10/28/2019 01:47
WG1370556
n-Nitrosodimethyla mine
ND
0.333 1
10/28/2019 01:47
WG1370556
n-Nitrosodiphenyla mine
ND
0.333 1
10/28/2019 01:47
WG1370556
n-Nitrosodi-n-propylamine
ND
0.333 1
10/28/2019 01:47
WG1370556
Phenanthrene
0.167
0.0333 1
10/28/2019 01:47
WG1370556
Benzylbutyl phthalate
ND
0.333 1
10/28/2019 01:47
WG1370556
Bis(2-ethylhexyl)phthalate
ND
0.333 1
10/28/2019 01:47
WG1370556
Di-n-butyl phthalate
ND
0.333 1
10/28/2019 01:47
WG1370556
Diethyl phthalate
ND
0.333 1
10/28/2019 01:47
WG1370556
Dimethyl phthalate
ND
0.333 1
10/28/2019 01:47
WG1370556
Di-n-octyl phthalate
ND
0.333 1
10/28/2019 01:47
WG1370556
Pyrene
0.0631
0.0333 1
10/28/2019 01:47
WG1370556
1,2,4-Trichlorobenzene
ND
0.333 1
10/28/2019 01:47
WG1370556
4-ChIoro-3-methyl phenol
ND
0.333 1
10/28/2019 01:47
WG1370556
2-Chlorophenol
ND
0.333 1
10/28/2019 01:47
WG1370556
2,4-Dichlorophenol
ND
0.333 1
10/28/2019 01:47
WG1370556
2,4-Dimethylphenol
ND
0.333 1
10/28/2019 01:47
WG1370556
4,6-Dinitro-2-methylphenol
ND
0.333 1
10/28/2019 01:47
WG1370556
2,4-Dinitrophenol
ND
0.333 1
10/28/2019 01:47
WG1370556
2-Nitrophenol
ND
0.333 1
10/28/2019 01:47
WG1370556
4-Nitrophenol
ND
0.333 1
10/28/2019 01:47
WG1370556
Pentachlorophenol
ND
0.333 1
10/28/2019 01:47
WG1370556
Phenol
ND
0.333 1
10/28/2019 01:47
WG1370556
2,4,6-Trichlorophenol
ND
0.333 1
10/28/2019 01:47
WG1370556
1,2-Dichlorobenzene
ND
0.333 1
10/28/2019 01:47
WG1370556
1,3-Dichlorobenzene
ND
0.333 1
10/28/2019 01:47
WG1370556
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Pilot Apex Environmental
L1153643
11/08/19 14:17
10 of 40

ONE LAB. NATIONWIDE.
SB-1 SAMPLE RESULTS - 02
Collected date/time: 10/23/19 12:05 L1153643
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Analyte
Result
mg/kg
Qualifier RDL
mg/kg
(S) 2-F/uorophenol
74.2
12.0-120
(S) Phenol-d5
60.9
10.0-120
(S) Nitrobenzene-d5
39.4
10.0-122
(S) 2-F/uorobipheny/
70.9
15.0-120
(S)2,4,6-Tribromopheno/
80.3
10.0-127
(S) p-Terphenyl-d14
74.6
10.0-120
Dilution Analysis
Batch
date / time
1012812019 01:47
WG1370556
1012812019 01:47
WG1370556
1012812019 01:47
WG1370556
1012812019 01.47
WG1370556
1012812019 01:47
WG1370556
1012812019 01.47
WG1370556
FP
FTc
FS
Fn
Fc
F,
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 11 of 40

WG1372541 QUALITY CONTROL SUMMARY
Total Solids by Method 2540 G-2011 L1153643-02
Method Blank (MB)
(MB) R3467398-1 10/31/1911:23
MB Result MB Qualifier MB MDL MB RDL
Analyte % % %
Total Solids 0.00100
L1153653-03 Original Sample (OS) • Duplicate (DUP)
(OS) L1153653-03 10/31/1911:23 • (DUP) R3467398-3 10/31/1911:23
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte % % % %
Total Solids 88.2 87.3 1 1.06 10
Laboratory Control Sample (LCS)
(LCS) R3467398-2 10/31/1911:23
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte % %_ % %
Total Solids 50.0 50.0 100 85.0-115
ONE LAB. NATIONWIDE.
— I
Cp
FTc
FSS
4
— Cn
FSr
— �GI
FAI
[Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 12 of 40

WG1370282
QUALITY
CONTROL SUMMARY
ONE LAB. NATIONWIDE.
Volatile Petroleum Hydrocarbons by Method MADEPV
L1153643-02
Method Blank (MB)
FP1(MB)
R3466512-3 10/26/19 23:30
MB Result MB Qualifier MB MDL
MB RDL
z
Analyte mg/kg mg/kg
mg/kg
TC
Unadjusted C5-C8 Aliphatics U 1.67
5.00
Unadjusted C9-C12 Aliphatics U 1.67
5.00
FSS
Unadjusted C9-C10 Aromatics U 1.67
5.00
Total VPH U 1.67
5.00
(S)2,5-Dibromotoluene(FID) 99.6
70.0-130
rCn
(S)2,5-Dibromotoluene(PID) 79.2
70.0-130
FSr
Laboratory Control Sample (LCS) • Laboratory Control Sample
Duplicate (LCSD)
(LCS) R3466512-1 10/26/19 21:18 • (LCSD) R3466512-2 10/26/19 21:51
M
Spike Amount LCS Result LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits LCS Qualifier LCSD Qualifier
RPD
RPD Limits
Analyte mg/kg mg/kg mg/kg
%
%
%
%
%
GI
Unadjusted C5-C8 Aliphatics 60.0 56.2 56.1
93.7
93.5
70.0-130
0.178
25
Unadjusted C9-C12 Aliphatics 70.0 67.4 67.1
96.3
95.9
70.0-130
0.446
25
FAI
Unadjusted C9-C10 Aromatics 10.0 7.68 7.66
76.8
76.6
70.0-130
0.261
25
Total VPH 140 131 131
93.6
93.6
70.0-130
0.000
25
(S)2,5-Dibromotoluene(FID)
104
104
70.0-130
[Sc(S)2,5-Dibromoto/uene(PID)
83.3
83.9
70.0-130
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 13 of 40

WG1374871
Volatile Petroleum Hydrocarbons by Method MADEPV
Method Blank (MB)
QUALITY
CONTROL SUMMARY
L1153643-01
ONE LAB. NATIONWIDE.
FP1(MB)
R3469776-3 11/06/19 01:43
MB Result MB Qualifier MB MDL
MB RDL
Analyte mg/I mg/I
mg/I
FTc
Unadjusted C5-C8 Aliphatics U 0.0333
0.100
Unadjusted C9-C12 Aliphatics U 0.0333
0.100
FSS
Unadjusted C9-C10 Aromatics U 0.0333
0.100
Total VPH U 0.0333
0.100
(S)2,5-Dibromotoluene(FID) 85.1
70.0-130
rCn
(S)2,5-Dibromotoluene(PID) 85.2
70.0-130
rs—r
Laboratory Control Sample (LCS) • Laboratory Control Sample
Duplicate (LCSD)
(LCS) R3469776-1 11/05/19 23:35 • (LCSD) R3469776-2 11/06/19 00:07
M
Spike Amount LCS Result LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits LCS Qualifier LCSD Qualifier
RPD
RPD Limits
Analyte mg/I mg/I mg/I
%
%
%
%
%
7
GI
Unadjusted C5-C8 Aliphatics 1.20 1.23 1.23
103
103
70.0-130
0.000
25
Unadjusted C9-C12 Aliphatics 1.40 1.53 1.54
109
110
70.0-130
0.651
25
FAI
Unadjusted C9-C10 Aromatics 0.200 0.207 0.207
104
104
70.0-130
0.000
25
Total VPH 2.80 2.97 2.98
106
106
70.0-130
0.336
25
(S)2,5-Dibromotoluene(FID)
101
97.4
70.0-130
[Sc(S)2,5-Dibromoto/uene(PID)
99.6
96.6
70.0-130
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 14 of 40

WG1374390 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 620OB-2011 L1153643-01
Method Blank (MB)
(MB) R3468708-3 11/04/19 00:30
MB Result MB Qualifier
Analyte mg/I
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec -Butyl benzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
2,2-Dichloropropane
Di -isopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene
p-Isopropyltoluene
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MB MDL
mg/I
0.0100
0.00887
0.00187
0.000331
0.000352
0.000380
0.000469
0.000866
0.000361
0.000365
0.000399
0.000379
0.000348
0.000327
0.000453
0.000324
0.000276
0.000375
0.000351
0.00133
0.000381
0.000346
0.000349
0.000220
0.000274
0.000551
0.000259
0.000361
0.000398
0.000260
0.000396
0.000306
0.000352
0.000366
0.000321
0.000320
0.000384
0.000256
0.000326
0.000350
MB RDL
mg/I
0.0500
0.0500
0.0100
0.00100
0.00100
0.00100
0.00100
0.00500
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
0.00500
0.00500
0.00250
0.00100
0.00100
0.00500
0.00100
0.00100
0.00100
0.00100
0.00100
0.00500
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
0.00100
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 15 of 40

WG1374390 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 620OB-2011 L1153643-01
Method Blank (MB)
(MB) R3468708-3 11/04/19 00:30
MB Result
Analyte
mg/I
2-Butanone (MEK)
U
Methylene Chloride
U
4-Methyl-2-pentanone (MIBK)
U
Methyl tert-butyl ether
U
Naphthalene
U
n-Propylbenzene
U
Styrene
U
1,1,1,2-Tetrachloroethane
U
1,1,2,2-Tetrachloroethane
U
Tetrachloroethene
U
Toluene
U
1,2,3-Trichlorobenzene
U
1,2,4-Trichlorobenzene
U
1,1,1-Trichloroethane
U
1,1,2-Trichloroethane
U
Trichloroethene
U
Trichlorofluoromethane
U
1,2,3-Trichloropropane
U
1,2,4-Trimethylbenzene
U
1,3,5-Trimethyl benzene
U
Vinyl chloride
U
o-Xylene
U
m&p-Xylenes
U
(S) Toluene-d8
109
(S) 4-Bromof/uorobenzene
104
(S)1,2-Dich/oroethane-d4
105
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.00393
0.0100
0.00100
0.00500
0.00214
0.0100
0.000367
0.00100
0.00100
0.00500
0.000349
0.00100
0.000307
0.00100
0.000385
0.00100
0.000130
0.00100
0.000372
0.00100
0.000412
0.00100
0.000230
0.00100
0.000355
0.00100
0.000319
0.00100
0.000383
0.00100
0.000398
0.00100
0.00120
0.00500
0.000807
0.00250
0.000373
0.00100
0.000387
0.00100
0.000259
0.00100
0.000341
0.00100
0.000719
0.00200
80.0-120
77.0-126
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3468708-1 11/03/19 23:18 • (LCSD) R3468708-2 11/03/19 23:42
Spike Amount
LCS Result
LCSD Result
Analyte
mg/I
mg/I
mg/I
Acetone
0.0250
0.0266
0.0278
Acrolein
0.0250
0.0259
0.0252
Acrylonitrile
0.0250
0.0234
0.0232
Benzene
0.00500
0.00455
0.00484
Bromobenzene
0.00500
0.00482
0.00470
Bromodichloromethane
0.00500
0.00476
0.00483
Bromoform
0.00500
0.00444
0.00460
ACCOUNT:
Pilot Apex Environmental
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
106
ill
19.0-160
4.41
27
104
101
10.0-160
2.74
26
93.6
92.8
55.0-149
0.858
20
91.0
96.8
70.0-123
6.18
20
96.4
94.0
73.0-121
2.52
20
95.2
96.6
75.0-120
1.46
20
88.8
92.0
68.0-132
3.54
20
PROJECT:
SDG:
DATE/TIME: PAGE:
L1153643
11/08/19 14:17 16 of 40
FP1
FTc
FSS
4
Cn
FSr
�GI
FAI
[Sc

WG1374390 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 620OB-2011 L1153643-01
ONE LAB. NATIONWIDE.
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3468708-1 11/03/19 23:18 • (LCSD) R3468708-2 11/03/19 23:42
Spike Amount
LCS Result
LCSD Result
Analyte
mg/I
mg/I
mg/I
Bromomethane
0.00500
0.00844
0.00820
n-Butylbenzene
0.00500
0.00452
0.00463
sec -Butyl benzene
0.00500
0.00477
0.00466
tert-Butylbenzene
0.00500
0.00463
0.00466
Carbon tetrachloride
0.00500
0.00364
0.00424
Chlorobenzene
0.00500
0.00493
0.00516
Chlorodibromomethane
0.00500
0.00438
0.00449
Chloroethane
0.00500
0.00535
0.00574
Chloroform
0.00500
0.00480
0.00496
Chloromethane
0.00500
0.00620
0.00624
2-Chlorotoluene
0.00500
0.00469
0.00467
4-Chlorotoluene
0.00500
0.00473
0.00468
1,2-Dibromo-3-Chloropropane
0.00500
0.00414
0.00404
1,2-Dibromoethane
0.00500
0.00471
0.00496
Dibromomethane
0.00500
0.00504
0.00497
1,2-Dichlorobenzene
0.00500
0.00477
0.00500
1,3-Dichlorobenzene
0.00500
0.00474
0.00491
1,4-Dichlorobenzene
0.00500
0.00474
0.00499
Dichlorodifluoromethane
0.00500
0.00520
0.00521
1,1-Dichloroethane
0.00500
0.00450
0.00486
1,2-Dichloroethane
0.00500
0.00499
0.00511
1,1-Dichloroethene
0.00500
0.00505
0.00528
cis-1,2-Dichloroethene
0.00500
0.00460
0.00478
trans-1,2-Dichloroethene
0.00500
0.00461
0.00487
1,2-Dichloropropane
0.00500
0.00469
0.00476
1,1-Dichloropropene
0.00500
0.00469
0.00497
1,3-Dichloropropane
0.00500
0.00474
0.00493
2,2-Dichloropropane
0.00500
0.00505
0.00498
Di -isopropyl ether
0.00500
0.00445
0.00456
Ethylbenzene
0.00500
0.00475
0.00500
Hexachloro-1,3-butadiene
0.00500
0.00452
0.00496
Isopropylbenzene
0.00500
0.00460
0.00492
p-Isopropyltoluene
0.00500
0.00456
0.00466
2-Butanone (MEK)
0.0250
0.0230
0.0234
Methylene Chloride
0.00500
0.00548
0.00558
4-Methyl-2-pentanone (MIBK)
0.0250
0.0245
0.0242
Methyl tert-butyl ether
0.00500
0.00473
0.00481
Naphthalene
0.00500
0.00388
0.00388
n-Propylbenzene
0.00500
0.00472
0.00469
Styrene
0.00500
0.00460
0.00481
ACCOUNT:
Pilot Apex Environmental
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
169
164
10.0-160
J4 J4 2.88
25
90.4
92.6
73.0-125
2.40
20
95.4
93.2
75.0-125
2.33
20
92.6
93.2
76.0-124
0.646
20
72.8
84.8
68.0-126
15.2
20
98.6
103
80.0-121
4.56
20
87.6
89.8
77.0-125
2.48
20
107
115
47.0-150
7.03
20
96.0
99.2
73.0-120
3.28
20
124
125
41.0-142
0.643
20
93.8
93.4
76.0-123
0.427
20
94.6
93.6
75.0-122
1.06
20
82.8
80.8
58.0-134
2.44
20
94.2
99.2
80.0-122
5.17
20
101
99.4
80.0-120
1.40
20
95.4
100
79.0-121
4.71
20
94.8
98.2
79.0-120
3.52
20
94.8
99.8
79.0-120
5.14
20
104
104
51.0-149
0.192
20
90.0
97.2
70.0-126
7.69
20
99.8
102
70.0-128
2.38
20
101
106
71.0-124
4.45
20
92.0
95.6
73.0-120
3.84
20
92.2
97.4
73.0-120
5.49
20
93.8
95.2
77.0-125
1.48
20
93.8
99.4
74.0-126
5.80
20
94.8
98.6
80.0-120
3.93
20
101
99.6
58.0-130
1.40
20
89.0
91.2
58.0-138
2.44
20
95.0
100
79.0-123
5.13
20
90.4
99.2
54.0-138
9.28
20
92.0
98.4
76.0-127
6.72
20
91.2
93.2
76.0-125
2.17
20
92.0
93.6
44.0-160
1.72
20
110
112
67.0-120
1.81
20
98.0
96.8
68.0-142
1.23
20
94.6
96.2
68.0-125
1.68
20
77.6
77.6
54.0-135
0.000
20
94.4
93.8
77.0-124
0.638
20
92.0
96.2
73.0-130
4.46
20
PROJECT:
SDG:
DATE/TIME: PAGE:
L1153643
11/08/19 14:17 17 of 40
FP1
FTC
FSS
[Cn]
FSr
�GI
FAI
FSC

WG1374390 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 620OB-2011 L1153643-01
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3468708-1 11/03/19 23:18 • (LCSD) R3468708-2 11/03/19 23:42
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
%
%
%
%
%
1,1,1,2-Tetrachloroethane
0.00500
0.00469
0.00483
93.8
96.6
75.0-125
2.94
20
1,1,2,2-Tetrachloroethane
0.00500
0.00517
0.00488
103
97.6
65.0-130
5.77
20
Tetrachloroethene
0.00500
0.00499
0.00534
99.8
107
72.0-132
6.78
20
Toluene
0.00500
0.00480
0.00502
96.0
100
79.0-120
4.48
20
1,2,3-Trichlorobenzene
0.00500
0.00369
0.00370
73.8
74.0
50.0-138
0.271
20
1,2,4-Trichlorobenzene
0.00500
0.00374
0.00376
74.8
75.2
57.0-137
0.533
20
1,1,1-Trichloroethane
0.00500
0.00446
0.00472
89.2
94.4
73.0-124
5.66
20
1,1,2-Trichloroethane
0.00500
0.00482
0.00522
96.4
104
80.0-120
7.97
20
Trichloroethene
0.00500
0.00479
0.00452
95.8
90.4
78.0-124
5.80
20
Trichlorofluoromethane
0.00500
0.00554
0.00556
ill
ill
59.0-147
0.360
20
1,2,3-Trichloropropane
0.00500
0.00501
0.00483
100
96.6
73.0-130
3.66
20
1,2,4-Trimethylbenzene
0.00500
0.00455
0.00456
91.0
91.2
76.0-121
0.220
20
1,3,5-Trimethyl benzene
0.00500
0.00472
0.00463
94.4
92.6
76.0-122
1.93
20
Vinyl chloride
0.00500
0.00488
0.00516
97.6
103
67.0-131
5.58
20
o-Xylene
0.00500
0.00480
0.00492
96.0
98.4
80.0-122
2.47
20
m&p-Xylenes
0.0100
0.00937
0.00991
93.7
99.1
80.0-122
5.60
20
(S) Toluene-d8
107
110
80.0-120
(S) 4-Bromofluorobenzene
104
108
77.0-126
(S)1,2-Dich/oroethane-d4
105
107
70.0-130
ONE LAB. NATIONWIDE.
FP1
FTC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 18 of 40

WG1374670 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1153643-02
Method Blank (MB)
(MB) R3468455-2 11/04/19 08:58
MB Result MB Qualifier
Analyte mg/kg
Acetone
Acrylonitrile
Benzene
Bromobenzene
Bromodichloromethane
Bromoform
Bromomethane
n-Butylbenzene
sec -Butyl benzene
tert-Butylbenzene
Carbon tetrachloride
Chlorobenzene
Chlorodibromomethane
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
1,2-Dibromo-3-Chloropropane
1,2-Dibromoethane
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,1-Dichloropropene
1,3-Dichloropropane
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
2,2-Dichloropropane
Di -isopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
MB MDL
mg/kg
0.0137
0.00190
0.000400
0.00105
0.000788
0.00598
0.00370
0.00384
0.00253
0.00155
0.00108
0.000573
0.000450
0.00108
0.000415
0.00139
0.000920
0.00113
0.00510
0.000525
0.00100
0.00145
0.00170
0.00197
0.000818
0.000575
0.000475
0.000500
0.000690
0.00143
0.00127
0.000700
0.00175
0.000678
0.00153
0.000793
0.000350
0.000530
0.0127
0.000863
MB RDL
mg/kg
0.0250
0.0125
0.00100
0.0125
0.00250
0.0250
0.0125
0.0125
0.0125
0.00500
0.00500
0.00250
0.00250
0.00500
0.00250
0.0125
0.00250
0.00500
0.0250
0.00250
0.00500
0.00500
0.00500
0.00500
0.00250
0.00250
0.00250
0.00250
0.00250
0.00500
0.00500
0.00250
0.00500
0.00250
0.00500
0.00250
0.00100
0.00250
0.0250
0.00250
FP1
FTC
FSS
[Cn]
FSr
�GI
FAI
FSC
ACCOUNT:
Pilot Apex Environmental
PROJECT: SDG: DATE/TIME: PAGE:
L1153643 11/08/19 14:17 19 of 40

WG1374670 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1153643-02
Method Blank (MB)
(MB) R3468455-2 11/04/19 08:58
MB Result
Analyte
mg/kg
p-Isopropyltoluene
U
2-Butanone (MEK)
0.0482
Methylene Chloride
0.00697
4-Methyl-2-pentanone (MIBK)
U
Methyl tert-butyl ether
U
Naphthalene
U
n-Propylbenzene
U
Styrene
U
1,1,1,2-Tetrachloroethane
U
1,1,2,2-Tetrachloroethane
U
Tetrachloroethene
U
Toluene
U
1,1,2-Trichlorotrifluoroethane
U
1,2,4-Trichlorobenzene
U
1,1,1-Trichloroethane
U
1,1,2-Trichloroethane
U
Trichloroethene
U
Trichlorofluoromethane
U
1,2,3-Trichloropropane
U
1,2,3-Trimethyl benzene
U
1,2,4-Trimethylbenzene
U
1,3,5-Trimethyl benzene
U
Vinyl chloride
U
Xylenes, Total
U
(S) Toluene-d8
113
(S) 4-Bromofluorobenzene
107
(S) 1,2-Dich/oroethone-d4
91.4
MB Qualifier MB MDL
mg/kg
MB RDL
mg/kg
0.00233
0.00500
0.0125
0.0250
J 0.00664
0.0250
0.0100
0.0250
0.000295
0.00100
0.00312
0.0125
0.00118
0.00500
0.00273
0.0125
0.000500
0.00250
0.000390
0.00250
0.000700
0.00250
0.00125
0.00500
0.000675
0.00250
0.00482
0.0125
0.000275
0.00250
0.000883
0.00250
0.000400
0.00100
0.000500
0.00250
0.00510
0.0125
0.00115
0.00500
0.00116
0.00500
0.00108
0.00500
0.000683
0.00250
0.00478
0.00650
Laboratory Control Sample (LCS)
75.0-131
67.0-138
70.0-130
(LCS) R3468455-1 11/04/19 07:55
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/kg
mg/kg
%
%
Acetone 0.625
0.482
77.1
10.0-160
Acrylonitrile 0.625
0.675
108
45.0-153
Benzene 0.125
0.133
106
70.0-123
Bromobenzene 0.125
0.126
101
73.0-121
Bromodichloromethane 0.125
0.122
97.6
73.0-121
Bromoform 0.125
0.119
95.2
64.0-132
ACCOUNT:
PROJECT:
Pilot Apex Environmental
SDG: DATE/TIME: PAGE:
L1153643 11/08/19 14:17 20 of 40
FP1
FTC
FSS
4
Cn
FSr
�GI
FAI
FSC

WG1374670
QUALITY CONTROL
SUMMARY
ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS)
by Method 8260D
L1153643-02
Laboratory Control Sample (LCS)
FP1(LCS)
R3468455-1 11/04/19 07:55
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/kg
mg/kg
%
%
FTC
Bromomethane 0.125
0.111
88.8
56.0-147
n-Butylbenzene 0.125
0.139
111
68.0-135
FSS
sec -Butyl benzene 0.125
0.147
118
74.0-130
tert-Butylbenzene 0.125
0.145
116
75.0-127
Carbon tetrachloride 0.125
0.127
102
66.0-128
[Cn]
Chlorobenzene 0.125
0.137
110
76.0-128
Chlorodibromomethane 0.125
0.129
103
74.0-127
FSr
Chloroethane 0.125
0.109
87.2
61.0-134
Chloroform 0.125
0.129
103
72.0-123
Chloromethane 0.125
0.127
102
51.0-138
2-Chlorotoluene 0.125
0.136
109
75.0-124
4-Chlorotoluene 0.125
0.136
109
75.0-124
7G1
1,2-Dibromo-3-Chloropropane 0.125
0.113
90.4
59.0-130
1,2-Dibromoethane 0.125
0.142
114
74.0-128
Dibromomethane 0.125
0.134
107
75.0-122
FAI
1,2-Dichlorobenzene 0.125
0.140
112
76.0-124
1,3-Dichlorobenzene 0.125
0.145
116
76.0-125
FSC
1,4-Dichlorobenzene 0.125
0.139
111
77.0-121
Dichlorodifluoromethane 0.125
0.143
114
43.0-156
1,1-Dichloroethane 0.125
0.139
111
70.0-127
1,2-Dichloroethane 0.125
0.118
94.4
65.0-131
1,1-Dichloroethene 0.125
0.139
111
65.0-131
cis-1,2-Dichloroethene 0.125
0.125
100
73.0-125
trans-1,2-Dichloroethene 0.125
0.132
106
71.0-125
1,2-Dichloropropane 0.125
0.135
108
74.0-125
1,1-Dichloropropene 0.125
0.134
107
73.0-125
1,3-Dichloropropane 0.125
0.145
116
80.0-125
cis-1,3-Dichloropropene 0.125
0.128
102
76.0-127
trans-1,3-Dichloropropene 0.125
0.129
103
73.0-127
2,2-Dichloropropane 0.125
0.122
97.6
59.0-135
Di -isopropyl ether 0.125
0.139
111
60.0-136
Ethylbenzene 0.125
0.139
111
74.0-126
Hexachloro-1,3-butadiene 0.125
0.152
122
57.0-150
Isopropylbenzene 0.125
0.146
117
72.0-127
p-Isopropyltoluene 0.125
0.144
115
72.0-133
2-Butanone(MEK) 0.625
0.675
108
30.0-160
Methylene Chloride 0.125
0.132
106
68.0-123
4-Methyl-2-pentanone (MIBK) 0.625
0.688
110
56.0-143
Methyl tert-butyl ether 0.125
0.133
106
66.0-132
Naphthalene 0.125
0.132
106
59.0-130
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Pilot Apex Environmental
L1153643
11/08/19 14:17 21 of 40

WG1374670 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Volatile Organic Compounds (GC/MS) by Method 8260D L1153643-02
Laboratory Control Sample (LCS)
(LCS) R3468455-1 11/04/19 07:55
Spike Amount
Analyte
mg/kg
n-Propylbenzene
0.125
Styrene
0.125
1,1,1,2-Tetrachloroethane
0.125
1,1,2,2-Tetrachloroethane
0.125
Tetrachloroethene
0.125
Toluene
0.125
1,1,2-Trichlorotrifluoroethane
0.125
1,2,4-Trichlorobenzene
0.125
1,1,1-Trichloroethane
0.125
1,1,2-Trichloroethane
0.125
Trichloroethene
0.125
Trichlorofluoromethane
0.125
1,2,3-Trichloropropane
0.125
1,2,3-Trimethyl benzene
0.125
1,2,4-Trimethylbenzene
0.125
1,3,5-Trimethyl benzene
0.125
Vinyl chloride
0.125
Xylenes, Total
0.375
(S) Toluene-d8
(S) 4-Bromof/uorobenzene
(S) 1,2-Dich/oroethane-d4
LCS Result
mg/kg
0.138
0.139
0.139
0.130
0.146
0.135
0.138
0.158
0.133
0.146
0.145
0.137
0.137
0.138
0.139
0.137
0.126
0.419
LCS Rec
110
104
117
108
110
126
106
117
116
110
110
110
110
101
112
ill
108
94.9
Rec. Limits LCS Qualifier
74.0-126
72.0-127
74.0-129
68.0-128
70.0-136
75.0-121
61.0-139
62.0-137
69.0-126
78.0-123
76.0-126
61.0-142
67.0-129
74.0-124
70.0-126
73.0-127
63.0-134
72.0-127
75.0-131
67.0-138
70.0-130
FP1
FTC
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 22 of 40

WG1375172
Volatile Organic Compounds (GC/MS) by Method 8260D
Method Blank (MB)
QUALITY CONTROL SUMMARY
L1153643-02
ONE LAB. NATIONWIDE.
(MB) R3468671-2 11/05/1912:30
MB Result MB Qualifier
MB MDL
MB RDL
Analyte mg/kg
mg/kg
mg/kg
1,2,3-Trichlorobenzene U
0.000625
0.00250
(S) Toluene-d8 105
75.0-131
(S) 4-Bromofluorobenzene 92.8
67.0-138
(S) 1,2-Dich/oroethane-d4 94.4
70.0-130
Laboratory Control Sample (LCS)
(LCS) R3468671-1 11/05/1911:33
Spike Amount LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg
%
%
1,2,3-Trichlorobenzene 0.125 0.115
92.0
59.0-139
(S) Toluene-d8
100
75.0-131
(S) 4-Bromofluorobenzene
93.8
67.0-138
(S)1,2-Dich/oroethane-d4
97.8
70.0-130
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental
L1153643 11/08/19 14:17 23 of 40
FP1
FTC
FSS
4
Cn
FSr
�GI
FAI
FSC

WG1371908
TPH by Method MADEPE
Method Blank (MB)
(MB) R3466999-1 10/31/19 09:38
MB Result
Analyte
mg/I
Unadjusted C9-C18 Aliphatics
0.0377
Unadjusted C19-06 Aliphatics
U
(S)1-Chloro-octadecane
75.5
Method Blank (MB)
(MB) R3466999-4 10/31/1910:48
MB Result
Analyte
mg/I
Unadjusted C11-C22 Aromatics
U
(S) o-Terpheny/
70.1
(S) 2-F/uorobipheny/
77.0
(S) 2-Bromonophtha/ene
71.1
QUALITY CONTROL SUMMARY
L1153643-01
MB Qualifier MB MDL
MB RDL
mg/I
mg/I
J 0.0333
0.100
0.0333
0.100
40.0-140
MB Qualifier MB MDL MB RDL
mg/I mg/I
0.0333 0.100
40.0-140
40.0-140
40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3466999-2 10/31/1910:05 • (LCSD) R3466999-3 10/31/1910:26
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
%
%
%
%
%
Unadjusted C9-C18 Aliphatics
0.600
0.300
0.310
50.0
51.7
40.0-140
3.28
25
Unadjusted C19-C36 Aliphatics
0.800
0.576
0.654
72.0
81.8
40.0-140
12.7
25
(S)1-Chloro-octadecane
71.5
77.5
40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3466999-5 10/31/1911:10 • (LCSD) R3466999-6 10/31/1911:32
Spike Amount LCS Result
LCSD Result LCS Rec.
LCSD Rec.
Rec. Limits LCS Qualifier LCSD Qualifier RPD
Analyte mg/I mg/I
mg/I %
%
% %
Unadjusted C11-C22 Aromatics 1.70 1.08
1.18 63.5
69.4
40.0-140 8.85
(S) o-Terpheny/
69.6
75.3
40.0-140
(S) 2-Fluorobiphenyl
79.1
73.6
40.0-140
(S) 2-Bromonaphtha/ene
76.6
72.2
40.0-140
RPD Limits
25
ONE LAB. NATIONWIDE.
FP1
FTc
FSS
4
Cn
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 24 of 40

WG1372377
TPH by Method MADEPE
Method Blank (MB)
(MB) R3467948-1 11/03/19 00:49
MB Result
Analyte
mg/kg
Unadjusted C9-C18 Aliphatics
4.12
Unadjusted C19-06 Aliphatics
U
Unadjusted Total Petroleum
4.12
Hydrocarbons
(S)1-Chloro-octadecane
53.6
Method Blank (MB)
(MB) R3467948-6 11/03/19 01:55
MB Result
Analyte mg/kg
MB Qualifier MB MDL
mg/kg
J 2.17
2.17
J 2.17
■
QUALITY CONTROL SUMMARY
L1153643-02
MB RDL
mg/kg
6.50
6.50
6.50
40.0-140
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
Unadjusted C11-C22 Aromatics
U
2.17 6.50
Unadjusted Total Petroleum
U
2.17 6.50
Hydrocarbons
(S) o-Terphenyl
58.5
40.0-140
(S) 2-F/uorobipheny/
99.2
40.0-140
(S) 2-Bromonaphthalene
94.2
40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3467948-2 11/03/19 01:11 • (LCSD) R3467948-4 11/03/19 01:33
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte
mg/kg
mg/kg
mg/kg
%
%
%
%
%
Unadjusted C9-C18 Aliphatics
39.9
23.4
21.6
58.6
54.1
40.0-140
8.00
25
Unadjusted C19-06 Aliphatics
53.2
28.1
25.1
52.8
47.2
40.0-140
11.3
25
(S)1-Chloro-octadecane
57.0
51.1
40.0-140
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3467948-3 11/03/19 01:16 • (LCSD) R3467948-5 11/03/19 01:38
Spike Amount LCS Result LCSD Result LCS Rec.
Analyte mg/kg mg/kg mg/kg %
Unadjusted C11-C22 Aromatics 113 75.8 87.8 67.1
(S) o-Terpheny/ 69.5
(S) 2-F/uorobipheny/ 105
(S) 2-Bromonaphthalene 100
LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
77.7 40.0-140 14.7 25
79.5 40.0-140
101 40.0-140
95.9 40.0-140
ONE LAB. NATIONWIDE.
ACCOUNT:
Pilot Apex Environmental
PROJECT: SDG: DATE/TIME: PAGE:
L1153643 11/08/19 14:17 25 of 40

WG1372377 QUALITY CONTROL SUMMARY
TPH by Method MADEPE L1153643-02
L1152553-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE.
(OS) L1152553-02 11/03/1916:08 • (MS) R3467948-7 11/03/1916:29 • (MSD) R3467948-8 11/03/1916:51
Spike Amount
(dry)
Original Result
(dry)
MS Result (dry)
MSD Result
(dry)
MS Rec. MSD Rec.
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte
mg/kg
mg/kg
mg/kg
mg/kg
% %
% % %
Unadjusted C9-C18 Aliphatics
44.4
U
35.0
38.4
78.9 86.5
1 40.0-140 9.09 50
Unadjusted C19-C36 Aliphatics
59.2
U
89.1
96.2
151 163
1 40.0-140 J5 J5 7.68 50
(S)1-Chloro-octodecane
66.7 69.7
40.0-140
L1152553-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1152553-02 11/03/1916:08 • (MS) R3467948-10 11/03/1917:35 • (MSD) R3467948-9 11/03/1917:13
Spike Amount
(dry)
Original Result
(dry)
MS Result (dry) MSD Result
(dry)
MS Rec.
MSD Rec.
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte
mg/kg
mg/kg
mg/kg mg/kg
%
%
% % %
Unadjusted C11-C22 Aromatics
126
U
137 120
109
95.6
1 40.0-140 13.0 50
(S) o-Terpheny/
77.1
64.7
40.0-140
(S) 2-Fluorobipheny/
105
79.7
40.0-140
(S) 2-Bromonaphtha/ene
100
76.3
40.0-140
FP1
FTc
FSS
4
Cn
FSr
�GI
FAI
[Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 26 of 40

WG1371001
QUALITY CONTROL
SUMMARY
ONE LAB. NATIONWIDE.
Semi Volatile Organic Compounds
(GC/MS) by Method 625.1
L1153643-01
Method Blank (MB)
FP1(MB)
R3466166-2 10/29/19 02:13
MB Result
MB Qualifier MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
FTC
Acenaphthene U
0.000316
0.00100
Acenaphthylene U
0.000309
0.00100
FSS
Anthracene U
0.000291
0.00100
Benzidine U
0.00432
0.0100
Benzo(a)anthracene U
0.0000975
0.00100
rCn
Benzo(b)fluoranthene U
0.0000896
0.00100
Benzo(k)fluoranthene U
0.000355
0.00100
FSr
Benzo(g,h,i)perylene U
0.000161
0.00100
Benzo(a)pyrene U
0.000340
0.00100
Bis(2-chlorethoxy)methane U
0.000329
0.0100
Bis(2-chloroethyl)ether U
0.00162
0.0100
Bis(2-chloroisopropyl)ether U
0.000445
0.0100
7G�
4-Bromophenyl-phenylether U
0.000335
0.0100
2-Chloronaphthalene U
0.000330
0.00100
4-Chlorophenyl-phenylether U
0.000303
0.0100
FAI
Chrysene U
0.000332
0.00100
Dibenz(a,h)anthracene U
0.000279
0.00100
FSC
3,3-Dichlorobenzidine U
0.00202
0.0100
2,4-Dinitrotoluene U
0.00165
0.0100
2,6-Dinitrotoluene U
0.000279
0.0100
Fluoranthene U
0.000310
0.00100
Fluorene U
0.000323
0.00100
Hexachlorobenzene U
0.000341
0.00100
Hexachloro-1,3-butadiene U
0.000329
0.0100
Hexachlorocyclopentadiene U
0.00233
0.0100
Hexachloroethane U
0.000365
0.0100
Indeno(1,2,3-cd)pyrene U
0.000279
0.00100
Isophorone U
0.000272
0.0100
Naphthalene U
0.000372
0.00100
Nitrobenzene U
0.000367
0.0100
n-Nitrosodimethyla mine U
0.00126
0.0100
n-Nitrosodiphenylamine U
0.00119
0.0100
n-Nitrosodi-n-propylamine U
0.000403
0.0100
Phenanthrene U
0.000366
0.00100
Benzylbutyl phthalate U
0.000275
0.00300
Bis(2-ethylhexyl)phthalate U
0.000709
0.00300
Di-n-butyl phthalate U
0.000266
0.00300
Diethyl phthalate U
0.000282
0.00300
Dimethyl phthalate U
0.000283
0.00300
Di-n-octyl phthalate U
0.000278
0.00300
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Pilot Apex Environmental
L1153643
11/08/19 14:17 27 of 40

WG1371001
Semi Volatile Organic Compounds
Method Blank (MB)
(GC/MS) by Method 625.1
QUALITY CONTROL SUMMARY
L1153643-01
ONE LAB. NATIONWIDE.
FP1(MB)
R3466166-2 10/29/19 02:13
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
FTC
Pyrene U
0.000330
0.00100
1,2,4-Trichlorobenzene U
0.000355
0.0100
FSS
4-ChIoro-3-methyl phenol U
0.000263
0.0100
2-Chlorophenol U
0.000283
0.0100
2,4-Dichlorophenol U
0.000284
0.0100
rCn
2,4-Dimethylphenol U
0.000624
0.0100
4,6-Dinitro-2-methylphenol U
0.00262
0.0100
FSr
2,4-Dinitrophenol U
0.00325
0.0100
2-Nitrophenol U
0.000320
0.0100
4-Nitrophenol U
0.00201
0.0100
Pentachlorophenol U
0.000313
0.0100
Phenol U
0.000334
0.0100
GI
2,4,6-Trichlorophenol U
0.000297
0.0100
(S) Nitrobenzene-d5 37.3
15.0-314
(S) 2-Fluorobiphenyl 51.1
22.0-127
FAI
(S) p-Terphenyl-d14 82.9
29.0-141
(S) Phenol-d5 20.2
8.00-424
FSC
(S) 2-F/uorophenol 33.0
10.0-120
(S)2,4,6-Tribromopheno/ 48.5
10.0-153
Laboratory Control Sample (LCS)
(LCS) R3466166-1 10/29/19 01:52
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
%
%
Acenaphthene 0.0500
0.0391
78.2
47.0-145
Acenaphthylene 0.0500
0.0404
80.8
33.0-145
Anthracene 0.0500
0.0396
79.2
27.0-133
Benzidine 0.100
0.0242
24.2
1.00-120
Benzo(a)anth race ne 0.0500
0.0398
79.6
33.0-143
Benzo(b)fluoranthene 0.0500
0.0436
87.2
24.0-159
Benzo(k)fluoranthene 0.0500
0.0429
85.8
11.0-162
Benzo(g,h,i)perylene 0.0500
0.0462
92.4
1.00-219
Benzo(a)pyrene 0.0500
0.0420
84.0
17.0-163
Bis(2-chlorethoxy)methane 0.0500
0.0327
65.4
1.00-219
Bis(2-chloroethyl)ether 0.0500
0.0318
63.6
33.0-185
Bis(2-chloroisopropyl)ether 0.0500
0.0318
63.6
36.0-166
4-Bromophenyl-phenylether 0.0500
0.0402
80.4
53.0-127
2-Chloronaphthalene 0.0500
0.0374
74.8
60.0-120
ACCOUNT:
PROJECT: SDG:
DATE/TIME: PAGE:
Pilot Apex Environmental
L1153643
11/08/19 14:17 28 of 40

WG1371001
QUALITY CONTROL
SUMMARY
ONE LAB. NATIONWIDE.
Semi Volatile Organic Compounds
(GC/MS) by
Method 625.1
L1153643-01
Laboratory Control Sample (LCS)
FP1(LCS)
R3466166-1 10/29/19 01:52
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
%
% _
z
TC
4-Chlorophenyl-phenylether 0.0500
0.0436
87.2
25.0-158
Chrysene 0.0500
0.0403
80.6
17.0-168
FSS
Dibenz(a,h)anthracene 0.0500
0.0454
90.8
1.00-227
3,3-Dichlorobenzidine 0.100
0.0870
87.0
1.00-262
2,4-Dinitrotoluene 0.0500
0.0488
97.6
39.0-139
rCn
2,6-Dinitrotoluene 0.0500
0.0450
90.0
50.0-158
Fluoranthene 0.0500
0.0409
81.8
26.0-137
FSr
Fluorene 0.0500
0.0424
84.8
59.0-121
Hexachlorobenzene 0.0500
0.0401
80.2
1.00-152
Hexachloro-1,3-butadiene 0.0500
0.0299
59.8
24.0-120
Hexachlorocyclopentadiene 0.0500
0.0296
59.2
10.0-120
Hexachloroethane 0.0500
0.0289
57.8
40.0-120
7G1
Indeno(1,2,3-cd)pyrene 0.0500
0.0437
87.4
1.00-171
Isophorone 0.0500
0.0338
67.6
21.0-196
Naphthalene 0.0500
0.0303
60.6
21.0-133
FAI
Nitrobenzene 0.0500
0.0308
61.6
35.0-180
n-Nitrosodimethyla mine 0.0500
0.0219
43.8
10.0-120
FSC
n-Nitrosodiphenylamine 0.0500
0.0403
80.6
44.0-120
n-Nitrosodi-n-propylamine 0.0500
0.0348
69.6
1.00-230
Phenanthrene 0.0500
0.0391
78.2
54.0-120
Benzylbutyl phthalate 0.0500
0.0406
81.2
1.00-152
Bis(2-ethylhexyl)phthalate 0.0500
0.0405
81.0
8.00-158
Di-n-butyl phthalate 0.0500
0.0426
85.2
1.00-120
Diethyl phthalate 0.0500
0.0454
90.8
1.00-120
Dimethyl phthalate 0.0500
0.0441
88.2
1.00-120
Di-n-octyl phthalate 0.0500
0.0395
79.0
4.00-146
Pyrene 0.0500
0.0387
77.4
52.0-120
1,2,4-Trichlorobenzene 0.0500
0.0301
60.2
44.0-142
4-Chloro-3-methylphenol 0.0500
0.0360
72.0
22.0-147
2-Chlorophenol 0.0500
0.0315
63.0
23.0-134
2,4-Dichlorophenol 0.0500
0.0333
66.6
39.0-135
2,4-Dimethylphenol 0.0500
0.0324
64.8
32.0-120
4,6-Dinitro-2-methylphenol 0.0500
0.0475
95.0
1.00-181
2,4-Dinitrophenol 0.0500
0.0594
119
1.00-191
2-Nitrophenol 0.0500
0.0351
70.2
29.0-182
4-Nitrophenol 0.0500
0.0230
46.0
1.00-132
Pentachlorophenol 0.0500
0.0483
96.6
14.0-176
Phenol 0.0500
0.0157
31.4
5.00-120
2,4,6-Trichlorophenol 0.0500
0.0417
83.4
37.0-144
(S) Nitrobenzene-d5
52.4
15.0-314
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Pilot Apex Environmental
L1153643
11/08/19 14:17 29 of 40

WG1371001 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1153643-01
Laboratory Control Sample (LCS)
(LCS) R3466166-1 10/29/19 01:52
Spike Amount LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I mg/I
%
%
(S) 2-Fluorobipheny/
77.2
22.0-127
(S) p-Terphenyl-d14
80.3
29.0-141
(S) Phenol-d5
30.4
8.00-424
(S) 2-F/uorophenol
48.6
10.0-120
(S) 2,4,6-Tribromopheno/
83.0
10.0-153
L1153432-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1153432-01 10/29/19 03:17 • (MS) R3466166-3 10/29/19 03:38 • (MSD) R3466166-4 10/29/19 03:59
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
Bis(2-chlorethoxy)methane
0.0500
U
0.0297
0.0302
59.4
60.4
Bis(2-chloroethyl)ether
0.0500
U
0.0294
0.0285
58.8
57.0
Bis(2-chloroisopropyl)ether
0.0500
U
0.0286
0.0286
57.2
57.2
4-Bromophenyl-phenylether
0.0500
U
0.0384
0.0399
76.8
79.8
4-Chlorophenyl-phenylether
0.0500
U
0.0394
0.0421
78.8
84.2
3,3-Dichlorobenzidine
0.100
U
0.0902
0.0945
90.2
94.5
2,4-Dinitrotoluene
0.0500
U
0.0473
0.0490
94.6
98.0
2,6-Dinitrotoluene
0.0500
U
0.0427
0.0453
85.4
90.6
Hexachloro-1,3-butadiene
0.0500
U
0.0281
0.0273
56.2
54.6
Hexachlorocyclopentadiene
0.0500
U
0.0286
0.0287
57.2
57.4
Hexachloroethane
0.0500
U
0.0265
0.0253
53.0
50.6
Isophorone
0.0500
U
0.0312
0.0319
62.4
63.8
Nitrobenzene
0.0500
U
0.0287
0.0288
57.4
57.6
n-Nitrosodiphenyla mine
0.0500
U
0.0390
0.0407
78.0
81.4
n-Nitrosodi-n-propylamine
0.0500
U
0.0316
0.0323
63.2
64.6
Benzylbutyl phthalate
0.0500
U
0.0425
0.0429
85.0
85.8
Bis(2-ethylhexyl)phthalate
0.0500
U
0.0413
0.0416
82.6
83.2
Di-n-butyl phthalate
0.0500
U
0.0426
0.0439
85.2
87.8
Diethyl phthalate
0.0500
U
0.0445
0.0462
89.0
92.4
Dimethyl phthalate
0.0500
U
0.0430
0.0445
86.0
89.0
Di-n-octyl phthalate
0.0500
U
0.0405
0.0408
81.0
81.6
4-ChIoro-3-methyl phenol
0.0500
U
0.0332
0.0342
66.4
68.4
2-Chlorophenol
0.0500
U
0.0286
0.0281
57.2
56.2
2,4-Dichlorophenol
0.0500
U
0.0307
0.0309
61.4
61.8
2,4-Dimethylphenol
0.0500
U
0.0301
0.0305
60.2
61.0
4,6-Dinitro-2-methylphenol
0.0500
U
0.0463
0.0502
92.6
100
2,4-Dinitrophenol
0.0500
U
0.0576
0.0640
115
128
2-Nitrophenol
0.0500
U
0.0320
0.0331
64.0
66.2
Dilution Rec. Limits MS Qualifier MSD Qualifier
33.V-Ib4
12.0-158
36.0-166
53.0-127
25.0-158
1.00-262
39.0-139
50.0-158
24.0-120
10.0-146
40.0-120
21.0-196
35.0-180
16.0-160
1.00-230
1.00-152
8.00-158
1.00-120
1.00-120
1.00-120
4.00-146
22.0-147
23.0-134
39.0-135
32.0-120
1.00-181
1.00-191
29.0-182
RPD
RPD Limits
1.67
54
3.11
108
0.000
76
3.83
43
6.63
61
4.66
108
3.53
42
5.91
48
2.89
62
0.349
34
4.63
52
2.22
93
0.348
62
4.27
28
2.19
87
0.937
60
0.724
82
3.01
47
3.75
100
3.43
183
0.738
69
2.97
73
1.76
61
0.649
50
1.32
58
8.08
203
10.5
132
3.38
55
FP1
FTc
FSS
[Cn]
s
Sr
�GI
FAI
[Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 30 of 40

WG1371001 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1153643-01
ONE LAB. NATIONWIDE.
L1153432-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1153432-01 10/29/19 03:17 • (MS) R3466166-3 10/29/19 03:38 • (MSD) R3466166-4 10/29/19 03:59
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
4-Nitrophenol
0.0500
U
0.0215
0.0225
43.0
45.0
Pentachlorophenol
0.0500
U
0.0468
0.0516
93.6
103
Phenol
0.0500
U
0.0139
0.0137
27.8
27.4
Acenaphthene
0.0500
U
0.0354
0.0375
70.8
75.0
2,4,6-Trichlorophenol
0.0500
U
0.0393
0.0412
78.6
82.4
Acenaphthylene
0.0500
U
0.0370
0.0385
74.0
77.0
Anthracene
0.0500
U
0.0378
0.0397
75.6
79.4
Benzidine
0.100
U
0.0629
0.0573
62.9
57.3
Benzo(a)anth race ne
0.0500
U
0.0403
0.0417
80.6
83.4
Benzo(b)fluoranthene
0.0500
U
0.0423
0.0439
84.6
87.8
Benzo(k)fluoranthene
0.0500
U
0.0431
0.0441
86.2
88.2
Benzo(g,h,i)perylene
0.0500
U
0.0458
0.0467
91.6
93.4
Benzo(a)pyrene
0.0500
U
0.0421
0.0428
84.2
85.6
2-Chloronaphthalene
0.0500
U
0.0340
0.0348
68.0
69.6
Chrysene
0.0500
U
0.0401
0.0419
80.2
83.8
Dibenz(a,h)anthracene
0.0500
U
0.0448
0.0455
89.6
91.0
Fluoranthene
0.0500
U
0.0398
0.0424
79.6
84.8
Fluorene
0.0500
U
0.0393
0.0419
78.6
83.8
Hexachlorobenzene
0.0500
U
0.0386
0.0402
77.2
80.4
Indeno(1,2,3-cd)pyrene
0.0500
U
0.0439
0.0451
87.8
90.2
Naphthalene
0.0500
U
0.0277
0.0279
55.4
55.8
n-Nitrosodimethyla mine
0.0500
U
0.0200
0.0199
40.0
39.8
Phenanthrene
0.0500
U
0.0375
0.0395
75.0
79.0
Pyrene
0.0500
U
0.0396
0.0406
79.2
81.2
1,2,4-Trichlorobenzene
0.0500
U
0.0278
0.0275
55.6
55.0
(S) Nitrobenzene-d5
44.3
46.0
(S) 2-Fluorobiphenyl
70.5
71.0
(S) p-Terphenyl-d14
82.7
83.8
(S) Phenol-d5
27.4
27.3
(S) 2-F/uorophenol
43.7
42.3
(S) 2,4,6- Tribromophenol
77.0
84.5
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 1.00-132
4.55
131
1 14.0-176
9.76
86
1 5.00-120
1.45
64
1 47.0-145
5.76
48
1 37.0-144
4.72
58
1 33.0-145
3.97
74
1 27.0-133
4.90
66
1 1.00-120
9.32
40
1 33.0-143
3.41
53
1 24.0-159
3.71
71
1 11.0-162
2.29
63
1 1.00-219
1.95
97
1 17.0-163
1.65
72
1 60.0-120
2.33
24
1 17.0-168
4.39
87
1 1.00-227
1.55
126
1 26.0-137
6.33
66
1 59.0-121
6.40
38
1 1.00-152
4.06
55
1 1.00-171
2.70
99
1 21.0-133
0.719
65
1 10.0-120
0.501
40
1 54.0-120
5.19
39
1 52.0-120
2.49
49
1 44.0-142
1.08
50
15.0-314
22.0-127
29.0-141
8.00-424
10.0-120
10.0-153
FP1
FTc
FSS
[Cn]
FSr
�GI
FAI
[Sc
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 31 of 40

WG1370556 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1153643-02
Method Blank (MB)
(MB) R3465685-2 10/28/19 00:16
MB Result MB Qualifier
Analyte mg/kg
Acenaphthene
U
Acenaphthylene
U
Anthracene
U
Benzidine
U
Benzo(a)anth race ne
U
Benzo(b)fluoranthene
U
Benzo(k)fluoranthene
U
Benzo(g,h,i)perylene
U
Benzo(a)pyrene
U
Bis(2-chlorethoxy)methane
U
Bis(2-chloroethyl)ether
U
Bis(2-chloroisopropyl)ether
U
4-Bromophenyl-phenylether
U
2-Chloronaphthalene
U
4-Chlorophenyl-phenylether
U
Chrysene
U
Dibenz(a,h)anthracene
U
1,2-Dichlorobenzene
U
1,3-Dichlorobenzene
U
1,4-Dichlorobenzene
U
3,3-Dichlorobenzidine
U
2,4-Dinitrotoluene
U
2,6-Dinitrotoluene
U
Fluoranthene
U
Fluorene
U
Hexachlorobenzene
U
Hexachloro-1,3-butadiene
U
Hexachlorocyclopentadiene
U
Hexachloroethane
U
Indeno(1,2,3-cd)pyrene
U
Isophorone
U
Naphthalene
0.00945
Nitrobenzene
U
n-Nitrosodimethyla mine
U
n-Nitrosodiphenyla mine
U
n-Nitrosodi-n-propylamine
U
Phenanthrene
U
Benzylbutyl phthalate
U
Bis(2-ethylhexyl)phthalate
U
Di-n-butyl phthalate
U
J
MB MDL MB RDL
mg/kg mg/kg
0.00642 0.0333
0.00671 0.0333
0.00632 0.0333
0.0637 0.333
0.00428 0.0333
0.00695 0.0333
0.00582 0.0333
0.00721 0.0333
0.00548 0.0333
0.00770 0.333
0.00896 0.333
0.00760 0.333
0.0114 0.333
0.00639 0.0333
0.00627 0.333
0.00555 0.0333
0.00821 0.0333
0.00921 0.333
0.0100 0.333
0.0100 0.333
0.0794 0.333
0.00607 0.333
0.00737 0.333
0.00496 0.0333
0.00682 0.0333
0.00856 0.333
0.0100 0.333
0.0587 0.333
0.0134 0.333
0.00772 0.0333
0.00522 0.333
0.00889 0.0333
0.00695 0.333
0.0647 0.333
0.0900 0.333
0.00906 0.333
0.00528 0.0333
0.0103 0.333
0.0120 0.333
0.0109 0.333
FP1
FTC
FSS
[Cn]
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 32 of 40

WG1370556
QUALITY CONTROL SUMMARY
ONE LAB. NATIONWIDE.
Semi Volatile Organic Compounds
(GC/MS) by
Method 8270E
L1153643-02
Method Blank (MB)
FP1(MB)
R3465685-2 10/28/19 00:16
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/kg
mg/kg
mg/kg
z
TC
Diethyl phthalate U
0.00691
0.333
Dimethyl phthalate U
0.00540
0.333
FSS
Di-n-octyl phthalate U
0.00907
0.333
Pyrene U
0.0123
0.0333
1,2,4-Trichlorobenzene U
0.00876
0.333
rCn
4-ChIoro-3-methyl phenol U
0.00477
0.333
2-Chorophenol U
0.00831
0.333
FSr
2,4-Dichlorophenol U
0.00746
0.333
2,4-Dimethylphenol U
0.0471
0.333
4,6-Dinitro-2-methylphenol U
0.124
0.333
2,4-Dinitrophenol U
0.0980
0.333
2-Nitrophenol U
0.0130
0.333
GI
4-Nitrophenol U
0.0525
0.333
Pentachlorophenol U
0.0480
0.333
Phenol U
0.00695
0.333
FAI
2,4,6-Trichlorophenol U
0.00779
0.333
(S) Nitrobenzene-d5 65.5
10.0-122
FSC
(S)2-F/uorobipheny/ 70.6
15.0-120
(S) p-Terphenyl-d14 76.0
10.0-120
(S) Phenol-d5 57.5
10.0-120
(S) 2-Fluorophenol 70.7
12.0-120
(S)2,4,6-Tribromopheno/ 74.8
10.0-127
Laboratory Control Sample (LCS)
(LCS) R3465685-1 10/27/19 23:54
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/kg
mg/kg
%
%
Acenaphthene 0.666
0.399
59.9
38.0-120
Acenaphthylene 0.666
0.448
67.3
40.0-120
Anthracene 0.666
0.427
64.1
42.0-120
Benzidine 1.33
0.206
15.5
10.0-120
Benzo(a)anth race ne 0.666
0.498
74.8
44.0-120
Benzo(b)fluoranthene 0.666
0.462
69.4
43.0-120
Benzo(k)fluoranthene 0.666
0.446
67.0
44.0-120
Benzo(g,h,i)perylene 0.666
0.440
66.1
43.0-120
Benzo(a)pyrene 0.666
0.465
69.8
45.0-120
Bis(2-chlorethoxy)methane 0.666
0.350
52.6
20.0-120
Bis(2-chloroethyl)ether 0.666
0.339
50.9
16.0-120
ACCOUNT:
PROJECT: SDG:
DATE/TIME: PAGE:
Pilot Apex Environmental
L1153643
11/08/19 14:17 33 of 40

WG1370556 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE.
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1153643-02
Laboratory Control Sample (LCS)
(LCS) R3465685-1 10/27/19 23:54
Spike Amount
Analyte ma/ka
Bis(2-chloroisopropyl)ether
4-Bromophenyl-phenylether
2-Chloronaphthalene
4-Chlorophenyl-phenylether
Chrysene
Dibenz(a,h)anthracene
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
3,3-Dichlorobenzidine
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Fluoranthene
Fluorene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachlorocyclopentadiene
Hexachloroethane
I nd eno(1,2,3-cd) pyrene
Isophorone
Naphthalene
Nitrobenzene
n-Nitrosodimethyla mine
n-Nitrosodiphenyla mine
n-N itros o d i-n-p ro pyl a m i n e
Phenanthrene
Benzylbutyl phthalate
B is(2-ethyl h exyl)phtha I ate
Di-n-butyl phthalate
Diethyl phthalate
Dimethyl phthalate
Di-n-octyl phthalate
Pyrene
1,2,4-Trichlorobenzene
4-Ch I oro-3-m ethyl phenol
2-Chlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
4,6-Di n itro-2-methyl phen of
2,4-Dinitrophenol
V.bbb
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
1.33
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
0.666
LCS Result
mg/kg
0.342
0.433
0.418
0.448
0.436
0.445
0.370
0.358
0.361
1.09
0.531
0.471
0.445
0.424
0.432
0.455
0.460
0.329
0.486
0.360
0.393
0.350
0.243
0.421
0.312
0.409
0.531
0.522
0.472
0.465
0.460
0.543
0.447
0.425
0.416
0.399
0.463
0.375
0.393
0.308
LCS Rec.
51.4
65.0
62.8
67.3
65.5
66.8
55.6
53.8
54.2
82.0
79.7
70.7
66.8
63.7
64.9
68.3
69.1
49.4
73.0
54.1
59.0
52.6
36.5
63.2
46.8
61.4
79.7
78.4
70.9
69.8
69.1
81.5
67.1
63.8
62.5
59.9
69.5
56.3
59.0
46.2
Rec. Limits LCS Qualifier
23.0-120
40.0-120
35.0-120
40.0-120
43.0-120
44.0-120
32.0-120
30.0-120
31.0-120
28.0-120
45.0-120
42.0-120
44.0-120
41.0-120
39.0-120
15.0-120
15.0-120
17.0-120
45.0-120
23.0-120
18.0-120
17.0-120
10.0-125
40.0-120
26.0-120
42.0-120
40.0-120
41.0-120
43.0-120
43.0-120
43.0-120
40.0-120
41.0-120
17.0-120
28.0-120
28.0-120
25.0-120
15.0-120
16.0-120
10.0-120
FP1
FTc
FSS
[Cn]
FSr
�GI
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 34 of 40

WG1370556 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1153643-02
Laboratory Control Sample (LCS)
(LCS) R3465685-1 10/27/19 23:54
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/kg
mg/kg
%
%
2-Nitrophenol
0.666
0.459
68.9
20.0-120
4-Nitrophenol
0.666
0.459
68.9
27.0-120
Pentachlorophenol
0.666
0.451
67.7
29.0-120
Phenol
0.666
0.345
51.8
28.0-120
2,4,6-Trichlorophenol
0.666
0.500
75.1
37.0-120
(S) Nitrobenzene-d5
53.5
10.0-122
(S) 2-F/uorobipheny/
62.5
15.0-120
(S) p-Terphenyl-d14
67.6
10.0-120
(S) Phenol-d5
53.9
10.0-120
(S) 2-Fluorophenol
64.6
12.0-120
(S) 2,4,6-Tribromopheno/
71.5
10.0-127
L1152026-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE.
(OS) L1152026-07 10/28/19 00:39 • (MS) R3465685-3 10/28/19 01:02 • (MSD) R3465685-4 10/28/19 01:24
Spike Amount
Original Result
MS Result (dry)
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
(dry)
(dry)
(dry)
Analyte
mg/kg
mg/kg
mg/kg
mg/kg
%
%
%
%
%
Acenaphthene
0.911
U
0.465
0.432
51.1
47.6
1 18.0-120
7.34
32
Acenaphthylene
0.911
U
0.512
0.476
56.2
52.4
1 25.0-120
7.22
32
Anthracene
0.911
U
0.505
0.466
55.4
51.4
1 22.0-120
7.91
29
Benzidine
1.82
U
0.737
0.628
40.4
34.7
1 10.0-120
15.9
40
Benzo(a)anth race ne
0.911
U
0.564
0.523
61.9
57.6
1 25.0-120
7.58
29
Benzo(b)fluoranthene
0.911
U
0.514
0.481
56.5
53.0
1 19.0-122
6.61
31
Benzo(k)fluoranthene
0.911
U
0.492
0.455
54.1
50.2
1 23.0-120
7.81
30
Benzo(g,h,i)perylene
0.911
U
0.507
0.458
55.7
50.5
1 10.0-120
10.2
33
Benzo(a)pyrene
0.911
U
0.523
0.488
57.4
53.8
1 24.0-120
6.78
30
Bis(2-chIorethoxy)methane
0.911
U
0.388
0.390
42.6
42.9
1 10.0-120
0.353
34
Bis(2-chIoroethyl) ether
0.911
U
0.377
0.376
41.4
41.4
1 10.0-120
0.364
40
Bis(2-chIoroisopropyl)ether
0.911
U
0.370
0.365
40.7
40.2
1 10.0-120
1.49
40
4-Bromophenyl-phenylether
0.911
U
0.507
0.470
55.7
51.8
1 27.0-120
7.57
30
2-Chloronaphthalene
0.911
U
0.468
0.435
51.4
47.9
1 20.0-120
7.29
32
4-C h I o ro p h e nyl -p h e nyl et h e r
0.911
U
0.528
0.497
58.0
54.7
1 24.0-120
6.16
29
Chrysene
0.911
U
0.492
0.453
54.1
49.8
1 21.0-120
8.42
29
Dibenz(a,h)anth racene
0.911
U
0.501
0.462
55.0
50.9
1 10.0-120
7.98
32
1,2-Dichlorobenzene
0.911
U
0.403
0.387
44.3
42.6
1 10.0-120
4.17
38
1,3-Dichlorobenzene
0.911
U
0.391
0.373
42.9
41.1
1 10.0-120
4.67
40
1,4-Dichlorobenzene
0.911
U
0.388
0.362
42.6
39.9
1 10.0-120
6.95
39
3,3-DIchIorobenzidine
1.82
U
1.34
1.24
73.6
68.5
1 10.0-120
7.97
34
2,4-Dinitrotoluene
0.911
U
0.610
0.577
67.0
63.6
1 30.0-120
5.54
31
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
Pilot Apex
Environmental
L1153643
11/08/19 14:17
35 of 40
FP1
FTc
FSS
[Cn]
FSr
�GI
FAI
[Sc

WG1370556 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1153643-02
ONE LAB. NATIONWIDE.
L1152026-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1152026-07 10/28/19 00:39 • (MS) R3465685-3 10/28/19 01:02 • (MSD) R3465685-4 10/28/19 01:24
Spike Amount
Original Result
MS Result (dry)
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
(dry)
(dry)
(dry)
Analyte
mg/kg
mg/kg
mg/kg
mg/kg
%
%
%
2,6-Dinitrotoluene
0.911
U
0.556
0.524
61.0
57.7
1 25.0-120
Fluoranthene
0.911
U
0.503
0.468
55.3
51.5
1 18.0-126
Fluorene
0.911
U
0.505
0.466
55.4
51.4
1 25.0-120
Hexachlorobenzene
0.911
U
0.513
0.469
56.3
51.7
1 27.0-120
HexachIoro-1,3-butadiene
0.911
U
0.477
0.457
52.4
50.3
1 10.0-120
H exa c h I o rocyc I o p e nta d I e n e
0.911
U
0.228
0.166
25.0
18.3
1 10.0-120
Hexachloroethane
0.911
U
0.357
0.324
39.2
35.6
1 10.0-120
Indeno(1,2,3-cd)pyre ne
0.911
U
0.538
0.506
59.0
55.7
1 10.0-120
Isophorone
0.911
U
0.405
0.407
44.4
44.9
1 13.0-120
Naphthalene
0.911
U
0.428
0.432
47.0
47.6
1 10.0-120
Nitrobenzene
0.911
U
0.374
0.374
41.1
41.2
1 10.0-120
n-Nitrosod1methylamIne
0.911
U
0.289
0.295
31.8
32.5
1 10.0-127
n-NitrosodIphenylamIne
0.911
U
0.494
0.462
54.2
50.9
1 17.0-120
n-NitrosodI-n-propylamIne
0.911
U
0.350
0.351
38.4
38.7
1 10.0-120
Phenanthrene
0.911
U
0.475
0.442
52.1
48.6
1 17.0-120
Benzylbutyl phthalate
0.911
U
0.580
0.549
63.7
60.4
1 23.0-120
Bis(2-ethylhexyl)phthalate
0.911
U
0.583
0.535
64.0
58.9
1 17.0-126
Di-n-butyl phthalate
0.911
U
0.524
0.484
57.5
53.3
1 30.0-120
Diethyl phthalate
0.911
U
0.547
0.517
60.1
56.9
1 26.0-120
Dimethyl phthalate
0.911
U
0.534
0.516
58.6
56.8
1 25.0-120
Di-n-octyl phthalate
0.911
U
0.616
0.575
67.6
63.3
1 21.0-123
Pyrene
0.911
U
0.527
0.487
57.8
53.6
1 16.0-121
1,2,4-Trichlorobenzene
0.911
U
0.453
0.442
49.7
48.6
1 12.0-120
4-ChIoro-3-methyl phenol
0.911
U
0.524
0.513
57.5
56.5
1 15.0-120
2-Chlorophenol
0.911
U
0.447
0.455
49.1
50.2
1 15.0-120
2,4-Dichlorophenol
0.911
U
0.564
0.540
61.9
59.5
1 20.0-120
2,4-Dimethylphenol
0.911
U
0.469
0.468
51.5
51.5
1 10.0-120
4,6-Dinitro-2-methylphenol
0.911
U
0.571
0.535
62.7
58.9
1 10.0-120
2,4-Dinitrophenol
0.911
U
0.543
0.509
59.6
56.0
1 10.0-121
2-Nitrophenol
0.911
U
0.495
0.451
54.4
49.7
1 12.0-120
4-Nitrophenol
0.911
U
0.528
0.512
58.0
56.3
1 10.0-137
Pentachlorophenol
0.911
U
0.627
0.550
68.8
60.6
1 10.0-160
Phenol
0.911
U
0.447
0.476
49.1
52.4
1 12.0-120
2,4,6-Trichlorophenol
0.911
U
0.588
0.529
64.6
58.3
1 19.0-120
(S) Nitrobenzene-d5
43.7
44.4
10.0-122
(S)2-F/uorobipheny/
50.0
474
15.0-120
(S) p-Terphenyl-d14
56.3
52.3
10.0-120
(S) Phenol-d5
48.0
49.8
10.0-120
(S) 2-F/uorophenol
54.5
55.7
12.0-120
MS Qualifier MSD Qualifier RPD RPD Limits
5.84 31
7.34 32
7.91 30
8.94 28
4.41 38
31.4 40
9.68 40
6.04 32
0.676 34
0.957 35
0.000 36
1.88 40
6.60 29
0.391 37
7.19 31
5.59 30
8.59 30
7.89 29
5.67 28
3.40 29
6.91 29
7.85 32
2.45 37
2.12 30
1.82 37
4.22 31
0.293 33
6.45 39
6.52 40
9.28 39
3.17 32
13.1 31
6.24 38
10.6 32
FP1
FTc
FSS
H
FSr
�GI
$AI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 36 of 40

WG1370556 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1153643-02
L1152026-07 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
ONE LAB. NATIONWIDE.
(OS) L1152026-07 10/28/19 00:39 • (MS) R3465685-3 10/28/19 01:02 • (MSD) R3465685-4 10/28/19 01:24
Spike Amount
Original Result
MS Result (dry) MSD Result MS Rec. MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
(dry)
(dry)
(dry)
Analyte mg/kg
mg/kg
mg/kg mg/kg % %
%
% %
(S)2,4,6-Tribromophenol
63.4 54.2
10.0-127
ACCOUNT:
PROJECT:
SDG:
DATE/TIME: PAGE:
Pilot Apex Environmental
L1153643
11/08/19 14:17 37 of 40
FP1
FTc
FSS
4
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
ONE LAB. NATIONWIDE.
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
CP
IP
FTC
FSS
(dry)
Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils].
MDL
Method Detection Limit.
[Cn]
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Fr
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Fc
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
FC
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
B
The same analyte is found in the associated blank.
J
The identification of the analyte is acceptable; the reported value is an estimate.
J4
The associated batch QC was outside the established quality control range for accuracy.
J5
The sample matrix interfered with the ability to make any accurate determination; spike value is high.
N
The analyte is tentatively identified and the associated numerical value may not be consistent with the actual
concentration present in the sample.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental
L1153643 11/08/19 14:17 38 of 40

ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE.
Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as
accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network
laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1
turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE.
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z
Tc
State Accreditations
f—�
Alabama
40660
Nebraska _
NE-OS-15-05
SS
Alaska
17-026
Nevada
TN-03-2002-34
Arizona
AZO612
New Hampshire
2975
Arkansas
88-0469
New Jersey_NELAP
TNO02
C n
California
2932
New Mexico
n/a
Colorado
TN00003
New York
11742
s
Connecticut
PH-0197
North Carolina
Env375
Sr
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina'
41
Georgia'
923
North Dakota
R-140
RC
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
G
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky76
90010
South Carolina
84004
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' 4
2006
Louisiana'
LA180010
Texas
T104704245-18-15
[SC
Maine
TN0002
Texas'
LABO152
Maryland
324
Utah
Massachusetts
M-TNO03
Vermont
Michigan
9958
Virginia
Minnesota
047-999-395
Washington
Mississippi
TN00003
West Virginia
Missouri
340
Wisconsin
Montana
CERT0086
Wyoming
Third Party
Federal Accreditations
A21LA — ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
A21LA — ISO 17025 5
1461.02
DOD
Canada
1461.01
USDA
EPA—Crypto
TN00003
' Drinking Water 'Underground
Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold
6 Wastewater n/a Accreditation not applicable
Our Locations
TN00003
VT2006
460132
C847
233
9980939910
A2LA
100789
1461.01
P330-15-00234
Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact
our main office. Pace National performs all testing at our central laboratory.
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
Pilot Apex Environmental L1153643 11/08/19 14:17 39 of 40

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