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MO-9520_40956_CA_SCH_20191101_Diesel Shear Valve Weep
peedway Speedway LLC Speedway Office P.O. Box 1500 Springfield, OH 45501 Telephone 937-864-3000 November 1, 2019 Ms. Ron Taraban NCDEQ, UST Section Mooresville Regional Office 610 East Center Avenue, Suite 301 Mooresville, North Carolina 28115 Re: Site Check Report Speedway #7984 2401 S. Cannon Boulevard Kannapolis, Cabarrus County, NC Incident Number: N/A GRI Project Number: 5194 Dear Mr. Taraban, Please find enclosed the referenced report for the above mentioned site. If you have any questions, please do not hesitate to contact Joanna Alley, E.I.T. and/or Nicole Long with Geological Resources, Inc. at 704-845- 4010. Sincerely, Speedway, LLC. vvo-� A 4� Charles Chiara Environmental Representative Enclosure An Equal Opportunity Employer 0 Geological Resources, Inc. Site Check Report Speedway #7984 2401 South Cannon Blvd. Kannapolis, Cabarrus County North Carolina Facility ID Number: 0-031744 Incident Number: N/A GRI Project Number: 5194 Prepared for: Charles Chiara Speedway, LLC 500 Speedway Drive Enon, Ohio 45323 November 1, 2019 Joanna Alley, E.I.T. Project Manager Nicole Long Project Manager 3502 Hayes Road • Monroe, North Carolina 28110 113 West Firetower Road, Suite G • Winterville, North Carolina 28590 Phone (704) 845-4010 • (888) 870-4133 • Fax (704) 845-4012 EXECUTIVE SUMMARY The Speedway #7984 site is located at 2401 South Cannon Blvd. in Kannapolis, Cabarrus County, North Carolina. The property operates as a petroleum retail facility and convenience store. The site is covered by concrete and grass. There are three 10,000-gallon gasoline and one 8,000-gallon diesel USTs currently in use at the site with five associated dispenser islands. A past release has be documented at the site as incident 36648 in October 2007. The site was determined to be low risk and the incident was closed with a Notice of Residual Petroleum (NRP) for soil in September 2009. On August 13, 2019, during annual compliance inspections, a weeping shear valve associated with diesel dispenser island 9/10 was discovered. Therefore a site check was required by the NCDEQ. Repairs were conducted on August 14, 2019. On September 3, 2019, GRI conducted a site check in the area of dispenser island 9/10. One soil boring was advanced to approximately 3 feet below ground surface (bgs) adjacent to dispenser island 9/10. A soil sample was collected. The soil boring was continued to 40 feet bgs and was completed as monitoring well MW-1. As part of the site check activities, a ground water sample was collected from MW-1 on September 3, 2019. Due to high sediment content in the sample, EDB analyses could not be performed. Well MW-1 was resampled on September 13, 2019 for EDB analyses. The Maximum Allowable Concentration was below the concentration of MTBE reported in groundwater sample MW-1. Based on the presence of a past incident that was classified as low risk and closed with a NRP for soils, GRI recommends a deed restriction NRP be completed for groundwater and a no further action be issued. Prepared by: Geological Resources, Inc. Site Check Report Prepared on: November 1, 2019 40 Speedway #7984 Project Manager: Joanna Alley, E.I.T. Geo. .ine..-,i- GRI Project No. 5194 SITE INFORMATION 1. Site Identification Speedway #7984 (Facility ID 0-031744) Incident Number N/A— Risk Ranking Undetermined Location of Source Area: 2401 South Cannon Blvd. Kannapolis, NC 27533 Cabarrus County 35.461878°N, 80.608600°W (Topographical Map) 2. Information about Contacts Associated with the Leaking UST System UST/AST Owner Speedway, LLC (Table 1) 500 Speedway Drive Enon, OH 45323 cachiara@speedway.com 919-516-8069 UST/AST Operator Speedway, LLC 500 Speedway Drive Enon, OH 45323 cachiara@speedway. corn 919-516-8069 3. Information about Release Property Owner Williams Properties II, LLC 539 South Main Street Findlay, OH 45840 Email Unknown Phone No. Unknown Property Occupant Speedway, LLC 500 Speedway Drive Enon, OH 45323 cachiara@speedway.com 919-516-8069 Release was discovered on September 24, 2019 Consultant/Contractor Geological Resources, Inc. 3502 Hayes Road Monroe, NC 28110 jra@geologicalresourcesinc.com 704-845-4010 Analytical Laboratory Pace Analytical 12065 Lebanon Road Mt. Juliet, TN 37122 State Certification No. 375 615-758-5858 An unknown amount of product was released from the weeping shear valve at dispenser Island 9/10 Three 10,000-gallon gasoline USTs and one 8,000-gallon diesel UST are in use at the site Certification: I, Randy AA�trF}��i;�aflGjed Geologist for Geological Resources, Inc., do certify that the information containeepnp k i,.refaWr st.Ci' ect and accurate to the best of my knowledge. 4vSi AL 12b2 i Geological'°!F�'%4t1AiApl�jc'`s licensed to practice geology and engineering in North Carolina. The 9 certification numfie�'?;''o"f the corporation are C-127 and C-2727, respectively. Prepared by: Geological Resources, Inc. Site Check Report Prepared on: November 1, 2019 G� Speedway #7984 Project Manager: Joanna Alley, E.I.T. �,,,,�,,,,GRI Project No. 5194 TABLE OF CONTENTS A. SITE HISTORY AND CHARACTERIZATION........................................................................1 B. SITE CHECK PROCEDURES..............................................................................................2 C. SITE INVESTIGATION......................................................................................................3 D. SUMMARY AND CONCLUSIONS.....................................................................................4 E. LIMITATIONS..................................................................................................................4 FIGURES Figure 1: Site Location Map Figure 2: Site Map Figure 3: Soil Quality Map Figure 4: Ground Water Quality Map TABLES Table 1: UST Owner/Operator Information Table 2: UST System Information Table 3: Well Construction and Gauging Information Table 4: Summary of Soil Sample Analytical Results Table 5: Summary of Ground Water Sample Analytical Results APPENDICES Appendix A: UST Suspected Release 24 Hour Notice Form (UST-17A) Appendix B: UST Suspected Release 7 Day Notice Form (UST-17B) Appendix C: 24-Hour Release and UST Leak Reporting Form (UST-61) Appendix D: Subsurface Log and Well Construction Record Appendix E: Laboratory Analytical Report Prepared by: Geological Resources, Inc. Site Check Report Prepared on: November 1, 2019 Speedway #7984 Project Manager: Joanna Alley, E.I.T. �Q,,g1Ci1ReSOUCeS GRI Project No. 5194 A. SITE HISTORY AND CHARACTERIZATION 1. UST Owner and Operator Information: In accordance with the Site Check Report guidelines, the underground storage tank (UST) owner and operator information has been summarized in the attached Table 1. 2. UST System Information: In accordance with the Site Check Report guidelines, the UST system information has been summarized in the attached Table 2. There are three 10,000-gallon gasoline and one 8,000-gallon diesel USTs currently in use at the site with four associated gasoline and one diesel dispenser islands. The dispensers are located in the front of store building. There are approximately 170 feet of product piping from the tanks to the dispenser islands. The NCDEQ Registered Tank Report lists an 8,000 kerosene UST, this UST is currently used for diesel. A copy of the NCDEQ Registered Tank Report is shown below: NCDEQ Registered Tank Report Facility Id 00-0-000D031744 Facility Name SPEEDWAY47984 d ess 2401 SOUTH CANNON BLVD. City KANNAPOLIS ® NC Caunty Caharrus ®28082 Longitude -80.60836 Latitude 35.46202 Tank Information ank Owner SPEEDWAY LLC dress 5DOSPEEDWAY DRIVE �ENON State OH ® 5323-1026 Tank Id Product Name 1CdPdL4 I Installation DaF erm Close Date ank Construdion JPiplps Construction INLffill Protedion ISPIll Protection rdrik Status I Gasoline, Gas Mix IODDO 7/10/1990 Single Wail Steel Single Wail FRP Ball Float Valve Catchment Basin Current 7 Gasoline, Gas Mix 10000 7/10/199C Single Wall Steel Single Wall FRP Bail Float Valve Catchment Basin Current 3 Gasoline, Gas Mix 100D0 7JI011990 Single Wail Steel Single Wall FAP Ball Float Valve Catchment Basin Current 4 Kerosene, Kero Mix 8000 W1011990 Single Wall Steel Single Wall FRP UI Float Valve Catchment Basin Current 3. Non -UST Information: There are currently no above ground petroleum storage tanks (ASTs) and no known ASTs formerly at the site. 4. Comprehensive Description of the Release: Annual compliance inspections were completed on August 13, 2019. During the inspection a weeping shear valve associated with diesel dispenser island 9/10 was discovered. The leaking component was repaired on August 14, 2019. Copies of the UST Suspected Release 24 Hour Notice (UST-17A) form and the USTSuspected Release 7 Day Notice (UST-1713) form are included as AppendicesA and B, respectively. A site check was required according to the North Carolina Department of Environmental Quality (NCDEQ). On September 3, 2019, one soil boring was advanced approximately 3 feet below ground surface (bgs) adjacent to dispenser Island 9/10. This boring was completed as monitoring well MW-1. A soil and groundwater sample were collected and sent for laboratory testing. Prepared by: Geological Resources, Inc. Site Check Report Prepared on: November 1, 2019 40 Speedway #7984 Project Manager: Joanna Alley, E.I.T. Geo.*.inrso.—,i- GRI Project No. 5194 1 Upon receipt of the laboratory analytical results on September 24, 2019, a release was confirmed at the site. A copy of the UST-61 Form has been included as Appendix C. 5. Description of the Site Characteristics: The Speedway #7984 site is located at 2401 South Cannon Blvd. in Kannapolis, Cabarrus County, North Carolina. (Figure 1). The property operates as a petroleum retail facility and convenience store. The site is covered by concrete and grass. There are three 10,000-gallon gasoline and one 8,000-gallon diesel USTs currently in use at the site with four associated gasoline and one diesel dispenser islands. The surrounding properties are commercial and residential. A past release has be documented at the site as incident 36648 in October 2007, the site was determined to be low risk and the incident was closed with a Notice of Residual petroleum (NRP) for soil in September 2009. A Site Map has been included as Figure 2. B. SITE CHECK PROCEDURES 1. Results of Tank and Line Tightness Testing: On August 13, 2019, a weeping shear valve associated with diesel dispenser island 9/10 was reported. The component was repaired on August 14, 2019. No testing was required upon repair. 2. Summary of Site Check Procedure: GRI performed a site check on September 3, 2019, that included the instillation of one monitoring well, collection of one soil sample and one groundwater sample. A soil boring was advanced to a depth of approximately 3 feet bgs adjacent to dispenser island 9/10, and a soil sample was collected. The soil boring was continued to a total depth of 40 feet bgs and was completed as monitoring well MW-1 with a 25-foot screened interval set to bracket the water table at the time of installation. A subsurface log and well construction record is provided as Appendix D. Well construction and gauging information is presented in Table 3. A photo of the newly installed monitoring well is shown below: 3. Soil Excavation Activities: No soil excavation activities were conducted. Prepared by: Geological Resources, Inc. Site Check Report Prepared on: November 1, 2019 40 Speedway #7984 Project Manager: Joanna Alley, E.I.T. Geo. .ine..-,i- GRI Project No. 5194 C. SITE INVESTIGATION 1. Field Screening: Soil sample (MW-1(2.5)) collected on September 3, 2019, was not screened with a photo ionization detector (PID) for volatile organic compounds (VOCs). 2. Soil Sampling Information: Soil sample (MW-1(2.5)) was collected on September 3, 2019, and submitted for laboratory analyses of total petroleum hydrocarbons (TPH) gasoline -range organics (GRO) by EPA Method 8015D and BTEX by EPA Method 8260E and for TPH-diesel range organics (DRO) by EPA Method 8015C. All of the reported contaminant concentrations were below the applicable standards. No free product was noted at the site. A soil quality map is presented as Figure 3. A summary of soil sample analytical results is presented in Table 4. The laboratory analytical report is provided as Appendix E. A summary of the soil sampling data from the September 2019 site check activities is show below: 0 L Q-� c M c d y c d a c OC f6 OC a C N C N N N T Q. a) COG1 a C .N N H 3 ) X H £ y m H L H � 0 W H RAL(mg/kg) 50 100 NE NE NE NE Soil to Water MCC (mg/kg) NE NE 0.0056 4.3 4.9 4.6 Residential SCLs (mg/kg) NE NE 18 1,200 1,560 3,129 MW-1(2.5) 2.5 <0.113 <4.54 <0.00128 0.00781 <0.00321 <0.00833 3. Ground Water and Surface Water Sampling Information: A ground water sample was collected from monitoring well MW-1 on September 3, 2019, and submitted for analysis of VOC+oxygenates by EPA Method 6200B, SVOCs by EPA 625.1, EDB by EPA Method 504.1, lead by EPA Method 6010 and VPH and EPH by the MADEP Methods. EDB was resampled on September 13, 2019 due to high suspended solids in the first sample. The Maximum Allowable Concentrations (MACs) as specified in T15A NCAC 2L.0202 were below the concentration of MTBE reported in the ground water sample collected from monitoring well MW-1. A ground water quality map is presented as Figure 4. A summary of ground water sample analytical results is presented in Table S. The laboratory analytical report is provided as Appendix E. A summary of the ground water sampling data from the September 2019 site check activities is show below: Contaminant of 4% N N N Concern 4 a`, C 4) ) 4) m f6 C m 0 t X ~ �' C Well ID W Z MAC (mg/1) 1 600 600 500 20 6 GCL (mg/1) 5,000 260,000 84,500 85,500 20,000 6,000 MW-1 <1.0 <1.0 <1.0 <3.0 54.5 <5.0 Prepared by: Geological Resources, Inc. �� Prepared on: November 1, 2019 Project Manager: Joanna Alley, E.I.T. Geo. .ine..0 ,i- Site Check Report Speedway #7984 GRI Project No. 5194 3 4. Quality -Control Measures: Clean, disposable nitrile gloves were used for the collection of the soil samples. The samples were collected in laboratory supplied containers and shipped to the laboratory in a cooler following proper chain -of -custody procedures. D. SUMMARY AND CONCLUSIONS • The site is commercial and surrounding properties are commercial and residential. A past incident had occurred at the site and closed with an NRP. • On August 13, 2019, a weeping shear valve associated with diesel dispenser 9/10 was reported. The component was repaired on August 14, 2019. • A site check was conducted on September 3, 2019, to determine if a petroleum release had occurred. • One soil boring (MW-1) was advanced to approximately 3 feet bgs, adjacent to dispenser island 9/10. A soil sample was collected and send for laboratory analysis. All of the reported contaminant concentrations were below the applicable standards. • Soil boring MW-1 was continued to 40 feet bgs and was completed as a monitoring well. • A ground water sample was collected from MW-1 on September 3, 2019. The MAC was below the concentration of MTBE reported in MW-1. • Based on the presence of a past incident that was classified as low risk and closed with a NRP for soils, GRI recommends a deed restriction NRP be completed for groundwater and a no further action be issued. E. LIMITATIONS This report has been prepared for the exclusive use of Speedway, LLC and the NCDEQ for the specific application to the referenced site in Cabarrus County, North Carolina. The assessment was conducted based on the scope of work and level of effort specified by the NCDEQ and with resources adequate only for that scope of work. Our findings have been developed in accordance with generally accepted standards of geology and hydrogeology practices in the State of North Carolina, available information, and our professional judgment. No other warranty is expressed or implied. The data that are presented in this report are indicative of conditions that existed at the precise locations sampled and at the time the samples were collected. In addition, the data obtained from samples would be interpreted as being meaningful with respect to parameters indicated in the laboratory report. No additional information can logically be inferred from these data. Prepared by: Geological Resources, Inc. �� Prepared on: November 1, 2019 Project Manager: Joanna Alley, E.I.T. Geo. .ine..0 ,i- Site Check Report Speedway #7984 GRI Project No. 5194 4 FIGURES r 'h -/A 17 e4 Li= Z I R 7 % L Ail Im x. % If I. f Ph 711 Figure I Site Location Speedway #7984 J MIN 2401 S. Cannon Blvd. 4�4A Kannapolis, Cabarrus County, NC Incident No. Pending 0 500 M GRI Project No. 5194 C 2000 FIT I Date:10/13/19 Location: 35.461831'N 80.608600'W I LEGEND — - - — - - — SUBJECT PROPERTY BOUNDARY LINE — — — — — — — UNDERGROUND STORAGE TANK — E — E — OVERHEAD ELECTRIC LINE —�—�— UNDERGROUND ELECTRIC LINE —w— UNDERGROUND WATER LINE UNDERGROUND STORM SEWER LINE PRODUCT PIPING LINE ® SUBSURFACE ANOMALY LIGHT POLE UTILITY/POWER POLE Q FUEL DISPENSER FIRE HYDRANT �O SIGN TYPE II MONITORING WELL Note: 1. This Site Map is based on data from the Carbarrus County, NC GIS Office. 2. This site was not professionally surveyed, site features and utilities are approximate. Ld LLJ Of pa n�n—n Shed GRASS m I �GRASS� II IUSTI I I I 1 �,ASI(V Speedway —tLI � T,JI LI _JII LII _JI �0-I—Ga/ 8000 Diesel UST �SPHAL!�, c � I11I �GRAVEL� I I Fuel nopy I I � 0❑ II f 1 � 1 I I s s / c-► SPHAL!�- -a 9 A �$I�_� i �/ GRASS �GRASS� SS9 . as « — as m I ^ II � m m SOUTH CANNON BLVD O SITE MAP 0 15 30 60 Speedway #7984 2401 S. Cannon Blvd, Incident No. Pending Kannapolis, Cabarrus County, ( IN FEET ) GRI Project No. 5194 NC Geo%g/co/ Resources, Inc. 1 inch = 30 ft Date: 10/29/19 Drawn by. JRA I Figure: 2 LEGEND — - - — - - — SUBJECT PROPERTY BOUNDARY LINE — — — — — — — UNDERGROUND STORAGE TANK — E — E — OVERHEAD ELECTRIC LINE —�—�— UNDERGROUND ELECTRIC LINE —w— UNDERGROUND WATER LINE UNDERGROUND STORM SEWER LINE PRODUCT PIPING LINE ® SUBSURFACE ANOMALY LIGHT POLE UTILITY/POWER POLE Q FUEL DISPENSER FIRE HYDRANT CEO SIGN TYPE II MONITORING WELL o a ) N CC Oo r- N a d a U' y m _ 0. r- N y 3 �, X c v m s ( N W W H Q RAL(mg/kg) 50 100 NE NE NE NE Soil to Water MCC NE NE 0.0056 4.3 4.9 4.6 Residential SCLs NE NE 18 1,200 1,560 3,129 MW-1 2.5' 2.5 1 <0.113 1 <4.54 <0.00128 0.00781 <0.00321 <0.00833 Shed m I II II II1 F II IUST1 110,ASIN .m. i 1 Spee dway JL LLJ LLJQ 0 Fuelnopy� I 11I 11I 1 1 ,0 m � / 1 � I m c m m I m II m � m SOUTH CANNON BLVD r t� 0 15 30 60 SOIL QUALITY MAP (09/03/19) Speedway #7984 2401 S. Cannon Blvd, Incident No. Pending Kannapolis, Caborrus County, ( IN FEET ) GRI Project No. 5194 NC Geological Resources, Inc. 1 inch = 30 ft Date: 10/29/19 Drawn by. JRA I Figure: 3 LEGEND — - - — - - — SUBJECT PROPERTY BOUNDARY LINE — — — — — — — UNDERGROUND STORAGE TANK — E — E — OVERHEAD ELECTRIC LINE —�—�— UNDERGROUND ELECTRIC LINE ww UNDERGROUND WATER LINE UNDERGROUND STORM SEWER LINE PRODUCT PIPING LINE ® SUBSURFACE ANOMALY LIGHT POLE UTILITY/POWER POLE Q FUEL DISPENSER FIRE HYDRANT �O SIGN TYPE II MONITORING WELL Contaminant of Concern a� W v C cu m � N W y X W m s s m Well s W z ID MAC (µg/1) 1 600 600 500 20 6 G C L /I 5,000 260,000 84,500 85,500 20,000 6,000 MW-1 <1.0 <1.0 <1.0 <3.0 54.5 <5.0 Shed m I II II I F ' I II IUSTI 1 I I 1 1 I I 11 0,ASIN I I 1 T—t n .m . i 1 1 Speedway I i I I � I I1 1 L �a I L J� m - / m I T I LLJ = /y LLJ Z , Q 1 0 I I Fuelnopy m � / 1 � I m c m m I m II m � m SOUTH CANNON BLVD r t� 0 15 30 60 GROUND WATER QUALITY MAP (09/03/19) Speedway #7984 2401 S. Cannon Blvd, Incident No. Pending Kannapolis, Caborrus County, ( IN FEET ) GRI Project No. 5194 NC Geological Resources, Inc. 1 inch = 30 ft Date: 10/29/19 Drawn by. JRA I Figure: 4 TABLES TABLE 1 UST OWNER/OPERATOR INFORMATION SPEEDWAY #7984 (INCIDENT NO. N/A) UST ID Number 1-4 Facility ID Number 0-031744 Name of Owner or Operator Dates of Ownership / Operation Owner or Operator? Speedway, LLC. 01/01/2016 - Current Owner/Operator Address Telephone Number 500 Speedway Drive, Enon, Ohio 45323 1-937-863-6507 UST ID Number 1-4 Facility ID Number 0-031744 Name of Owner or Operator Dates of Ownership / Operation Owner or Operator? WilcoHess, LLC. 04/02/2001 - 01/01/2016 Owner/Operator Address Telephone Number 5446 University Parkway, Winston-Salem, NC 27105-1366 1-800-642-0945 UST ID Number 1-4 Facility ID Number 0-031744 Name of Owner or Operator Dates of Ownership / Operation Owner or Operator? A.T. Williams Oil Company 07/10/1990 - 04/02/2001 Owner/Operator Address Telephone Number 5446 University Parkway, Winston-Salem, NC 27105-1366 Unknown Page 1 of 1 TABLE 2 UST SYSTEM INFORMATION SPEEDWAY #7984 (INCIDENT NO. N/A) Date: 10 11 19 Facility ID #: 0-031744 Description of Was Release UST Current Associated Status Associated ID or Most Previous Capacity Date Construction Tank Product Piping of with UST Recent Contents (gallons) Installed Details Dimensions System? No. and UST Contents Pumps (Yes / No) 1 Gasoline NA 10,000 07/10/1990 Single Wall Steel 8' x 26' 8" Single Wall FRP Current No 2 Gasoline NA 10,000 07/10/1990 Single Wall Steel 8' x 26' 8" Single Wall FRP Current No 3 Gasoline NA 10,000 07/10/1990 Single Wall Steel 8' x 26' 8" Single Wall FRP Current No 4 Diesel Kerosene 8,000 07/10/1990 Single Wall Steel 8' x 21' 4" Single Wall FRP Current Yes Page 1 of 1 TABLE 3 SUMMARY OF SOIL SAMPLE ANALYTICAL RESULTS SPEEDWAY #7984 (INCIDENT NO. N/A) Date: 10 11 19 Facility ID #: 0-031744 5030/ 3550/ Analytical Method 4 EPA Method 8260B 8015D 8015C alli v t +� CL ao °' C d N 01 a d N _N > fl. O V Q m H N H N X N wE ca E= N a� coco s G N p w H RAL (mg/kg) 50 100 NE NE NE NE Soil to Water MCC (mg/kg) NE NE 0.0056 4.3 4.9 4.6 Residential SCLs (mg/kg) NE NE 18 1,200 1,560 3,129 MW-1(2.5') 1 09/03/19 1 2.5 <0.113 <4.54 <0.00128 0.00781 <0.00321 <0.00833 Notes: • Results reported in mg/kg (milligrams per kilograms) • ft-BGS: feet below ground surface. • RAL: Regulatory Action Level. • MCCs: Maximum Contaminant Concentrations (soils). • SCLs: Soil Cleanup Levels. • < : Less than the method detection limit specified in the laboratory report • Concentrations in bold face type indicate the soil -to -water MCCs were below the reported concentrations. • Concentrations in italic type indicate the residential SCLs were below the reported concentrations. • NE: Not Established • NR: Not Requested. Page 1 of 1 TABLE 4 WELL CONSTRUCTION AND GAUGING INFORMATION SPEEDWAY #7984 (INCIDENT NO. N/A) Date: 10 11 19 Facility ID # : 0-031744 Date Water Well Screened Top of Depth to Date Bottom Free Product Ground Level Casing Interval Casing Water from Well ID Installed of Well Thickness Water Comments Measured Depth (x to y ft. Elevation Top of Casing (m/dd/yy) (ft. BGS) (ft.) Elevation (ft.) (m/dd/yy) (ft. BGS) BGS) (ft.) (feet) MW-1 09/03/19 09/03/19 20 20-40 40 100.00 19.64 --- 80.36 09/13/19 19.92 --- 80.08 Notes: • Elevation relative to an arbitrary datum of 100 feet. • ft BGS : feet below ground surface. • NM : Not measured. Page 1 of 1 TABLE 5 SUMMARY OF GROUND WATER SAMPLE ANALYTICAL RESULTS SPEEDWAY#7984 (INCIDENT NO. N/A) Date: 10 03 19 Facility ID # : 0-031744 Analytical Method EPA EPA 6200E EPA 6010 MADEP VPH MADEP EPH 504.1 Contaminant of Concern U N G1 O1 of m GJ f6 G1 o m -a U t CL S a E c 3 S a C. +-+ 3 Y 0 N 3 ~ M E d a a a Q a Well Date Sampled m X a = —' 00 o � n N ID (mm/dd/yy) c0 z � U U U v U v U v Q, U r, ,s N Ln V V V V U U ri MAC (µg/1) 1 600 600 500 20 6 0.02 15 400 700 200 700 10,000 200 GCL (µg/1) 5,000 260,000 84,500 85,500 20,000 6,000 50 15,000 NE NE NE NE NE NE 09/03/19 <1.0 <1.0 <1.0 <3.0 54.5 <5.0 NA <5.0 <100 <100 <100 <100 <100 <100 MW-1 09/13/19 NR NR NR NR NR NR <0.0100 NR NR NR NR NR NR NR Notes: • Results reported in micrograms per liter W/1). • MAC: Maximum Allowable Concentration as specified in T15A NCAC 2L.0202. • < : Less than the method detection limit specified in the laboratory report. • GCL: Gross contamination level. • Concentrations in bold face type indicate the MAC was below the reported concentration. • J: Estimated value. • NA: Not analyzed due to high suspended solids, resampled 09/13/19. • NE: Not established. • NR: Not requested. • Refer to laboratory report for other detectable concentrations which did not exceed the MACs. Page 1 of 1 APPENDICES Appendix A UST Suspected Release 24 Hour Notice Form (UST-17A) UST-17A UST Suspected Release 24 our Notice ND Pary Do not use this form to report a 24 hour notice of a Pollution Incident. You must use form UST-61, 24 Hour Release and UST Leak Reporting Form. ➢ This form must be used to report to DEQ, within 24 hours of discovery, a Suspected Release from any of the following: a) Failed or inconclusive lea detection or tightness test results. This includes positive test results, such as "Increase", which indicates the level in the UST system has increased more than 0.2 gph. b) Unusual operating conditions which can include, but are not limited to: the erratic behavior of dispensing equipment; the unexplained presence of water in the tank; the presence of fuel in containment sumps or interstitial spaces; or the degradation of any equipment or element of an underground storage tank system to the point where that equipment or element can not reasonably be expected to perform its intended function. c) Internal inspection results such as, perforations, corrosion holes, weld failures, or other similar defects that indicate a release could have occurred. ➢ If you have more than four UST systems to report suspected releases, then attach additional sheets of the UST-17A form. You only need to list the UST systems at your site that have suspected releases. ➢ Within 7 days of discovery, submit a UST-17B form to document the response activities taken to investigate the suspected release. ➢ Please submit this form to: NCDEQ/DWM, UST Section 1646 Mail Service Center Raleigh, North Carolina 27699-1646 OR Fax to (919) 715-1117 OR UST.Permits(o)ncdenr.gov I. UST OWNER Name: Speedway, LLC Address: 500 Speedway Drive Enon Joanna Alley, E.I.T III. UST INFORMATION Tank Number / Size: Product Stored: Location and/or source of suspected release: (check all that apply) Leak detection method or other observation that indicates a suspected release. (e.g., ATG, SIR, visual contamination, fuel in sump, etc.): Failed/Inconclusive date or date that leak detection method suspected release discovered: I . COMMENTS II. UST FACILIT Name: Speedway #7984 Address: 2401 S. Cannon Blvd OH 1 45323 1 Kannapolis Project Manager (GRI) 4 / 8000 Diesel ❑ Tank ❑ Piping ❑ Tank Sump ® Dispenser Sump ❑ Spill Bucket ❑ Internal Inspection ❑ Other (Explain in comments) Compliance Testing 8/ 13/2019 ❑ Tank ❑ Piping ❑ Tank Sump ❑ Dispenser Sump ❑ Spill Bucket ❑ Internal Inspection ❑ Other (Explain in comments) i eiepnone Numoer: (704) 845-4010 ❑ Tank ❑ Piping ❑ Tank Sump ❑ Dispenser Sump ❑ Spill Bucket ❑ Internal Inspection ❑ Other (Explain in comments) Facility ID: 0-031744 County: Cabarrus I / ❑ Tank ❑ Piping ❑ Tank Sump ❑ Dispenser Sump ❑ Spill Bucket ❑ Internal Inspection ❑ Other (Explain in comments) During a NCDEQ compliance inspection on 8/13/19, a weep above the shear valve was noted at diesel dispenser 9/10. UST-17A Revised 10/2015 http://www.wastenotnc.org/web/wm/ Appendix B UST Suspected Release 7 Day Notice Form (UST-17B) UST-1713 UST Suspected Release 7 Day Notice KC This form must be used to report to DEQ, within 7 days of discovery, the investigation results for a Suspected Release from any of the following: a) Failed or inconclusive leak detection or tightness test results. This includes positive test results, such as "Increase", which indicates the level in the UST system has increased more than 0.2 gph. b) Unusual operating conditions which can include, but are not limited to, the erratic behavior of dispensing equipment; the unexplained presence of water in the tank; the presence of fuel in containment sumps or interstitial spaces; or the degradation of any equipment or element of an underground storage tank system to the point where that equipment or element can not reasonably be expected to perform its intended function. c) Internal inspection results such as, perforations, corrosion holes, weld failures, or other similar defects that indicate a release could have occurred. ➢ If you have more than four UST systems to report suspected release investigations, then attach additional sheets of the UST-17B form. ➢ Please submit this form along with the supporting documentation to: NCDEQ/DWM, UST Section 1646 Mail Service Center Raleigh, North Carolina 27699-1646 OR Fax to (919) 715-1117 OR UST. Perm its(@ncdenr.gov I. UST OWNER II. UST FACILIT Name: Speedway, LLC Name: Speedway #7984 Facility ID: 0-031744 Address: 500 Speedway Drive Address: 2401 S. Cannon Blvd City: Enon State: Ohio Zip: 45323 City: Kannapolis County: Cabarrus Person Reporting: Joanna Alley (GRI) Title of Person Reporting: Project Manager Telephone Number: (704) 845-4010 III. IN ESTIGATION RESULTS Tank Number / Size: 1 4 / 8,000 Product Stored: Reason for Suspected Release Investigation (Check all that apply): You must attach the supporting documentation specified in the footnote for the reason(s) selected. Diesel ❑ Data entry error' ❑ Data entry error' ❑ Data entry error' ❑ Data entry error' ❑ Dispensing fuel while ❑ Dispensing fuel while ❑ Dispensing fuel while ❑ Dispensing fuel while test is being conducted 2 test is being conducted 2 test is being conducted 2 test is being conducted 2 ❑ Faulty equipment 3 ❑ Incorrect stick or meter reading' ❑ Incorrect tank chart 4 ❑ Internal Inspection 5 ❑ Meter not calibrated ❑ Other (Attach explanation)' ® Tank/Dispenser containment sump contains liquid 7 ❑ Tilted tank 8 ❑ Unknown' ❑ Faulty equipment 3 ❑ Incorrect stick or meter reading' ❑ Incorrect tank chart 4 ❑ Internal Inspection 5 ❑ Meter not calibrated ❑ Other (Attach explanation)' ❑ Tank/Dispenser containment sump contains liquid 7 ❑ Tilted tank 8 ❑ Unknown' ❑ Faulty equipment 3 ❑ Faulty equipment 3 ❑ Incorrect stick or meter ❑ Incorrect stick or meter reading' reading' ❑ Incorrect tank chart 4 ❑ Internal Inspection 5 ❑ Meter not calibrated ❑ Other (Attach explanation)' ❑ Tank/Dispenser containment sump contains liquid 7 ❑ Tilted tank 8 ❑ Unknown' ❑ Incorrect tank chart 4 ❑ Internal Inspection 5 ❑ Meter not calibrated ❑ Other (Attach explanation)' ❑ Tank/Dispenser containment sump contains liquid 7 ❑ Tilted tank 8 ❑ Unknown' Conduct a tank and/or line tightness test and attach the results, along with all of the supporting data sheets for the test method, to this form for submittal. The summary page listing the results by itself is not acceptable. If the tightness test results are fail, then you must repair or replace your UST system and conduct a site check in accordance with 15A NCAC 2N .0603. 2 Provide sales receipts or other comparable documentation that shows fuel was being dispensed from the UST during the test. 3 Provide invoices (with a description of the work completed) or other documentation that shows the equipment has been repaired. 4 Correct your leak detection results using the correct tank chart and submit copies with this form. 5 Repair the UST in accordance with the manufacturer's instructions or a national standard (e.g., PEI API 1631) and conduct a site check in accordance with 15A NCAC 2N .0603. If the UST is not repaired, then it must be permanently closed in accordance with the latest version of the UST Sections Guidelines for Tank Closure. 6 Correct your leak detection results using the amount your meter was adjusted following calibration and submit copies of the meter calibration and leak detection results with this form. Conduct a tightness test (e.g., hydrostatic test) of the sump and submit the test result along with this form. If the test results are fail, then you must repair or replace the containment sump and conduct a site check in accordance with 15A NCAC 2N .0603. 8 Submit documentation from your UST equipment contractor explaining how they determined the UST was tilted. Correct your leak detection results using a tank chart adjusted for the tilt and submit with this form. Note: Tan , piping, spill buc et and containment sump replacements must be done in accordance with 15A NCAC 2N .0900 UST-17B Revised 10/2015 http://www.wastenotnc.org/web/wm/ Appendix C 24-Hour Release and UST Leak Reporting Form (UST-61) UST-61 24-Hour Release and UST Leak Reporting Form. For Releases This form should be completed and submitted to the UST Section's regional office following a known or suspected release from an underground storage tank (UST) system. This form is required to be submitted within 24 hours of discovery of a known or in NC suspected release (DWM USE ONLY) Suspected Contamination? (Y/N) Facility ID Number Incident # Risk (H,I,L,U) Confirmed GW Contamination? (Y/N) Date Leak Discovered Received On Received By Confirmed Soil Contamination ?(Y/N) Comm/Non-Commercial? Reported by (circle one): Phone, Fax or Report Samples Taken?(Y/N) Reg/Non-regulated? Region Free Product? (Y/N) If Yes, State Greatest Thickness INCIDENT DESCRIPTION Incident Name: Speedway #7984 Address: 2401 S. Cannon Blvd County: Cabarrus City/Town: Kannapolls Zip Code:28083 Regional Office (circle one): Asheville, Mooresville, Fayetteville, Raleigh, Washington, Wilmington, Winston-Salem Latitude (decimal degrees): 35.461879 Longitude (decimal degrees) :-80.608675 Obtained by: ❑ GPS Briefly describe suspected or confirmed release: (including but not limited to: nature of release, date of release, amount of release, amount of free product present and recovery efforts, initial responses conducted, impacts to receptors) ❑Topographic map ❑GIS Address matching ®Other ❑ Unknown USe��beg stered Tank Report On August 13, 2019, during annual compliance inspections, a weeping shear valve associated with diesel dispenser island 9/10 was discovered. On September 3, 2019, GRI conducted a site check in the area of dispenser island 9/10. Upon receipt of the analytical results, a release was confirmed at the site. HOW RELEASE WAS DISCOVERED (Release code) (Check one) ©Release Detection Equipment or Methods ❑Visual/Odor ❑Groundwater Contamination ❑During UST Closure/Removal ❑Water in Tank ❑Surface Water Contamination ❑Property Transfer ❑Water Supply Well Contamination ❑Other (specify) SOURCE OF CONTAMINATION Source of Release Cause of Release Type of Release Product Type Released (Check primary source) (Check primary cause) (Check one) (Check primary product type released) ❑ Tank ❑ Spill ❑ Petroleum ❑ Gasoline/ Diesel/ ❑ Diesel/Veg. Oil ❑ Piping ❑ Overfill ❑ Non -Petroleum Kerosene Blend Heating Oil ❑ Vegetable Oil 100% ❑❑ Dispenser ❑Corrosion Both ❑ Other Petroleum E10 - E20 ❑ ❑ ❑ Submersible Turbine Pump Physical/Mechanical Products Location ❑ E21 E84 Damage - ❑ Delivery Problem (Check one) Metals ❑ ❑ Install Problem ❑ E85 - E99 ❑ Spill Bucket Other [-]Facility ❑ Other Inorganics ❑ [:]Ethanol 100% ❑ Other ❑ Other Organics ❑ Unknown ❑Residence ❑ E01 - E09 ❑ Unknown ❑Other Definitions resented on reverse Definitions presented on reverse Ownership 1. Municipal 2. Military 3. Unknown 4. Private 5. Federal 6. County 7. State Operation Type 1. Public Service 2. Agricultural 3. Residential 4. Education/Relig. 5. Industrial 6. Commercial 7. Mining UST Form 61 (02/19) Page 1 of 2 IMPACT ON DRINKING WATER SUPPLIES Water Supply Wells Affected? 1. Yes 2. No 3. Unknown Number of Water Supply Wells Affected Water Supply Wells Contaminated: 1. 2. 3. (Include Users Names, Addresses and Phone Numbers. Attach additional sheet if necessary) UST Owner/Company UST SYSTEM OWNER Point of Contact Address City State Zip Code Telephone Number UST SYSTEM OPERATOR UST Operator/Company Address City State Zip Code Telephone Number LANDOWNER AT LOCATION OF UST INCIDENT Landowner Address City State Zip Code Telephone Number Draw Sketch of Area (showing two major road intersections) or Attach Map Person Reporting Incident Company Telephone Number Title Address Date UST Form 61 (02/19) Page 2 of 2 Definitions of Sources Tank: means the tank that stores the product and is part of the underground storage tank system Piping: means the piping and connectors running from the tank or submersible turbine pump to the dispenser or other end -use equipment (Vent, vapor recovery, or fill lines are excluded.) Dispenser: includes the dispenser and the equipment used to connect the dispenser to the piping (e.g., a release from a suction pump or from components located above the shear valve) Submersible Turbine Pump (STP) Area includes the submersible turbine pump head (typically located in the tank sump), the line leak detector, and the piping that connects the submersible turbine pump to the tank Delivery Problem: identifies releases that occurred during product delivery to the tank. (Typical causes associated with this source are spills and overfills.) Other: serves as the option to use when the release source is known but does not fit into one of the preceding categories (e.g., for releases from vent lines, vapor recovery lines, and fill lines) Unknown: identifies releases for which the source has not been determined Definitions of Causes Spill: use this cause when a spill occurs (e.g., when the delivery hose is disconnected from the tank fill pipe or when the nozzle is removed from the dispenser) Overfill: use when an overfill occurs (e.g., overfills may occur from the fill pipe at the tank or when the nozzle fails to shut off at the dispenser) Physical or Mechanical Damage: use for all types of physical or mechanical damage, except corrosion (e.g., puncture of tank or piping, loose fittings, broken components, and components that have changed dimension) Corrosion: use when a metal tank, piping, or other component has a release due to corrosion (e.g., for steel, corrosion takes the form of rust) Installation Problem: use when the problem is determined to have occurred specifically because the UST system was not installed properly Other: use this option when the cause is known but does not fit into one of the preceding categories (e.g., putting regulated substances into monitoring wells) Unknown: use when the cause has not been determined Appendix D Subsurface Log and Well Construction Record WELL CONSTRUCTION RECORD This form can be used for single or multiple wells For Internal Use ONLY: 1. Well Contractor Information: Justin Radford Well Contractor Name 3270-A NC Well Contractor Certification Number Geological Resources, Inc. Company Name 2. Well Construction Permit #: List all applicable well permits (i.e. County, State, Variance, Injection, etc) 3. Well Use (check well use): Water Supply Well: ❑Agricultural ❑Geothermal (Heating/Cooling Supply) ❑ lndustrial/Commercial ❑ Irrigation Non -Water Supply Well: El Aquifer Recharge El Aquifer Storage and Recovery ❑Aquifer Test ❑Experimental Technology ❑Geothermal (Closed Loop) ❑Geothermal (Heating/Cooling ❑Municipal/Public El Residential Water Supply (single) ❑Residential Water Supply (shared) El Groundwater Remediation ❑ Salinity Barrier ❑ Stormwater Drainage ❑Subsidence Control ❑Tracer ❑Other (explain under #21 F 4. Date Well(s) Completed: 9/3/1 9 Well ID# MW-1 5a. Well Location: Speedway #7984 0-00031744 Facility/Owner Name Facility ID# (if applicable) 2401 South Cannon Blvd, Kannapolis, NC Physical Address, City, and Zip Cabarrus 56221609240000 County Parcel Identification No. (PIN) 5b. Latitude and Longitude in degrees/minutes/seconds or decimal degrees: (if well field, one lat/long is sufficient) 35.461831 N 80.608600 W 6. Is (are) the well(s): ❑] Permanent or ❑Temporary 7. Is this a repair to an existing well: ❑Yes or ONo If this is a repair, fill out known well construction information and explain the nature of the repair under #21 remarks section or on the back of this form. 8. Number of wells constructed: 1 For multiple injection or non -water supply wells ONLY with the same construction, you can submit one form. 9. Total well depth below land surface: 40 (ft.) For multiple wells list all depths if different (example- 3@200' and 2@100') 10. Static water level below top of casing: 19.9 (ft.) If water level is above casing, use "+" 11. Borehole diameter: 5 (in.) 12. Well construction method: Rotary Air Hammer (i.e. auger, rotary, cable, direct push, etc.) 14. WATER ZONES FROM TO DESCRIPTION 20 ft 40 ft Weather rock ft. ft. 15. OUTER CASING for multi -cased wells OR LINER if applicable) FROM TO DIAMETER THICKNESSr MATERIAL ft. ft. I in. 16. INNER CASING OR TUBING eother at closed -loop) FROM TO DIAMETER THICKNESS MATERIAL 0 ft• 15 ft• 2 '"' SCh 40 PVC ft fL in. 17. SCREEN FROM TO DIAMETER SLOT SIZE THICKNESS MATERIAL 15 ft' 40 ft' 2 in. 0.010 Sch 40 PVC ft. ft. in. 18. GROUT FROM TO MATERIAL EMPLACEMENT METHOD & AMOUNT 0 ft. 11 ft. grout pour 11 IL 13 ft. bentonite pour rt. rt. 19. SAND/GRAVEL PACK (if applicable) FROM TO MATERIAL EMPLACEMENT METHOD 13 fL 40 ft #2 Gravel Pour rt. rt. 20. DRILLING LOG attach additional sheets if necessary) FROM TO DESCRIPTION (color, hardness, soil/rock type, grain size, etc.) 0 ft. 0.5 ft. Gravel 0.5 ft. 2.5 ft. Gray to brown clay 2.5 ft. 40 ft. Greenish brown weathered rock rt. ft. rt. ft. ft. ft. rt. rL 21. REMARKS 22. Certification: Signature of Certified Well Contractor 10/31 /19 Date By signing this form, I hereby certify that the well(s) was (were) constructed in accordance with 15A NCAC 02C .0100 or 15A NCAC 02C .0200 Well Construction Standards and that a copy of this record has been provided to the well owner. 23. Site diagram or additional well details: You may use the back of this page to provide additional well site details or well construction details. You may also attach additional pages if necessary. SUBMITTAL INSTUCTIONS 24a. For All Wells: Submit this form within 30 days of completion of well construction to the following: Division of Water Resources, Information Processing Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617 24b. For Iniection Wells ONLY: In addition to sending the form to the address in 24a above, also submit a copy of this form within 30 days of completion of well construction to the following: Division of Water Resources, Underground Injection Control Program, FOR WATER SUPPLY WELLS ONLY: 1636 Mail Service Center, Raleigh, NC 27699-1636 13a. Yield m Method of test: 24c. For Water Supply & Injection Wells: (gP ) Also submit one copy of this form within 30 days of completion of 13b. Disinfection type: Amount: well construction to the county health department of the county where constructed. Form GW-1 North Carolina Department of Environment and Natural Resources - Division of Water Resources Revised August 2013 Geological Resources, Inc. Phone: (704) 845-4010 2301-F Crown Point Executive Drive Fax: (704) 845-4012 Charlotte, NC 28227 SUBSURFACE LOG Project Speedway #7984 Address 241 South Cannon Blvd., Kannapolis, Cabarrus County, North Carolina Boring Number MW-1 Date Drilled 09/03/19 Sample Method Grab Drilling Method 5" Dia Air Rotary Completion Details Total Well Depth 40', riser 0-15', screened 15'-40'. 2" diameter well. Driller Justin Radford Log By Corey Buchanan Lab Sample PID Depth Sample Interval(ft) ppm LITHOLOGY 0 - 0.2' Asphalt 0 0.2' - 0.5' Gravel MW-1(2.5) 2.5 0.5' - 2.5' Gray to Brown Clay 3 2.5' - 40' Greenish brown weathered rock 6 9 12 15 18 21 24 27 30 33 Wet @ 35' 36 39 Well set at 40 ft. 42 45 APPENDIX E Laboratory Analytical Report aceAnalytical o ANALYTICAL REPORT National Center for Testing & Innovation September 24, 2019 • #r Geological Resources- NC Speedway Sample Delivery Group: L1140647 Samples Received: 09/18/2019 Project Number: 5194 Description: Speedway 7984 Site: 7984 Report To: Ms. Nicole Long 3502 Hayes Rd. Charlotte, NC 28110 Entire Report Reviewed By iLlc� T. Alan Harvill Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received. 4 V — 16 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1140647 09/24/19 09:43 1 of 11 TABLE OF CONTENTS ONE LAB. NATIONWIDE. Cp: Cover Page Tc: Table of Contents Ss: Sample Summary Cn: Case Narrative Sr: Sample Results MW-1 L1140647-01 Qc: Quality Control Summary EDB / DBCP by Method 504.1 GI: Glossary of Terms Al: Accreditations & Locations Sc: Sample Chain of Custody 2 3 4 5 5 6 6 7 8 9 CID ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1140647 09/24/19 09:43 2 of 11 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected date/time Received date/time MW-1 L1140647-01 GW Alex Lin 09/13/19 09:42 09/18/19 08:45 C P Method EDB / DBCP by Method 504.1 Batch Dilution Preparation Analysis Analyst Location date/time date/time WG1349298 1 09/20/19 09:16 09/20/19 21:26 HMH Mt. Juliet, TN FTC M [Cn] FSr RC F, FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1140647 09/24/19 09:43 3 of 11 CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the FP1 appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FTChave been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FSS knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. FSr 6 QC r �GI iz T. Alan Harvill FAI Project Manager FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1140647 09/24/19 09:43 4 of 11 SAMPLE RESULTS - 01 L1140647 ONE LAB. NATIONWIDE. MW-1 Collected date/time: 09/13/19 09:42 EDB / DBCP by Method 504.1 Analyte Ethylene Dibromide Result ug/I ND Qualifier RDL ug/I 0.0100 Dilution Analysis date / time 1 09/20/2019 21:26 Batch WG1349298 FP1 FTC FSS 4 Cn FC 7G1 FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1140647 09/24/19 09:43 5 of 11 WG1349298 QUALITY CONTROL SUMMARY EDB / DBCP by Method 504.1 L1140647-01 Method Blank (MB) (MB) R3453537-1 09/20/1919:37 MB Result MB Qualifier MB MDL MB RDL Analyte ug/I ug/I ug/I Ethylene Dibromide U 0.00240 0.0100 L1140992-01 Original Sample (OS) • Duplicate (DUP) (OS) L1140992-01 09/20/19 20:26 • (DUP) R3453537-3 09/20/19 20:14 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte ug/I ug/I _ % % Ethylene Dibromide ND 0.000 1.02 0.000 20 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3453537-4 09/20/19 22:26 • (LCSD) R3453537-5 09/21/19 00:52 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte _ ug/I ug/I ug/I % % % % % Ethylene Dibromide 0.250 0.237 0.238 94.8 95.2 70.0-130 0.421 20 L1140992-04 Original Sample (OS) • Matrix Spike (MS) (OS) L1140992-04 09/20/19 20:01 • (MS) R3453537-2 09/20/1919:49 Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier Analyte ug/I ug/I ug/I % % Ethylene Dibromide 0.101 ND 0.0959 95.0 1.01 70.0-130 ONE LAB. NATIONWIDE. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1140647 09/24/19 09:43 6 of 11 GLOSSARY OF TERMS ONE LAB. NATIONWIDE. Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit. Rec. Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry) Confidence level of 2 sigma. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description The remainder of this page intentionally left blank, there are no qualifiers applied to this SDG. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1140647 09/24/19 09:43 7 of 11 FP1 FTC FSS [Cn] FSr FC-1 FAI E ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1 turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z Tc State Accreditations f—� Alabama 40660 Nebraska _ NE-OS-15-05 SS Alaska 17-026 Nevada TN-03-2002-34 Arizona AZO612 New Hampshire 2975 Arkansas 88-0469 New Jersey_NELAP TNO02 C n California 2932 New Mexico n/a Colorado TN00003 New York 11742 s Connecticut PH-0197 North Carolina Env375 Sr Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina' 41 Georgia' 923 North Dakota R-140 RC Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 G Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky76 90010 South Carolina 84004 Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee' 4 2006 Louisiana' LA180010 Texas T104704245-18-15 [SC Maine TN0002 Texas' LABO152 Maryland 324 Utah Massachusetts M-TNO03 Vermont Michigan 9958 Virginia Minnesota 047-999-395 Washington Mississippi TN00003 West Virginia Missouri 340 Wisconsin Montana CERT0086 Wyoming Third Party Federal Accreditations A21LA — ISO 17025 1461.01 AIHA-LAP,LLC EMLAP A21LA — ISO 17025 5 1461.02 DOD Canada 1461.01 USDA EPA—Crypto TN00003 ' Drinking Water 'Underground Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable Our Locations TN00003 VT2006 460132 C847 233 9980939910 A2LA 100789 1461.01 P330-15-00234 Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory. WA MT NO OR MN T I❑ SD ITO WI NY WY MI NV T NE IA OH T PA T f IL Ills WY vA UT T CA�� T KS MO KY W 11110 � NM O� AR N Sc T MS A`7L GA T TX * LA T AK T T q FL wo HI ACCOUNT: PROJECT: SDG: DATE/TIME: Geological Resources- NC Speedway 5194 L1140647 09/24/19 09:43 ME PAGE: 8 of 11 f (Geological Resources- NC Speedway 3502 Hayes Rd. Charlotte, NC 28110 RePort[o'. MS. Ni[OIB Long Billing Information. Mr. Charles Chiara Phk PO Box 1510 `hk Springfield, OH 45500 anal Container or servo ive ':hairs of Custody Page of , ce nalytical' N,n�,nioa�w m, M��aa, Lebanon Rd a mountJuliet, rN 3n22 Phore.6157SS 5856 f Phone: eoo-167 56s9 Fac61s-Ira 5959 Q- F12065 O 2 to 2 U O O g ul Lair I i Emma To nml@geologicalresourcesinc.com; jra@geologicalresourcesinc.com; Project Descriptlon. Speedway 7984 City/State Collected: Please Circle: PT MT CrT F' , SDG It Phone: 704-845-4010 Client Project a Sj CI /L Fax: �I Lab Project M GEORESSSA-7984 Table If Coll ted by( riot): I � � Sire/Facility ID 4 —I �q � P.O. a Acctnum: GEORESSSA Templa[e:T155686 Prelogin:P729669 PM: 364 • T. Alan Hamill p� Pg: Collected by ' nature � /� Immediately / Packed on Ice N VjL/ Rush? (Lab MUST Be Notifics) Quote k Same Day _Five Day I _ Next Day :A _ 5 Day (Ronly) Date Results Needed _Two Day _ 10 Day(Rad Onlyl No. _Three Day of Shipped via: Fed EX Ground Sample ID Comp/Grab Matrix' Depth Date Time nVs Remarks sample Pllab only) GW rl� q 13 dq(4� 3 X I 1 i Rerl Sample Receipt Checklist pH Temp -oc seal Present/Intact: _NP _N "Nalatrix SS - Soil AIR - Air F- Filter GW- nun water - icassay WW- WdSleWatef OW - Drinking Water OT - Other Flow Other — Bottles arrive Intact: t/x _N Correct bottles used: N Sufficient volute sent: _N VOA Zero Headspaac+--Caheliq;ls]Selicab]e —N Preservation Con e c t/Checked: Y, N RAD Screen <0.5 mR/hr: _N Samples returned via: UPS FedEx _Courier y^ l �r n Tracking# .-}�'� /.� / (/ Relinq h b (Signa[ur Date. Time'. Received by: (SignaW re) Trip Blank Received: Yes/ HCL / Tell Relinquished by :(Signature) Date: Time: Received by (Signature) Temp Bottles Received: If preservation required by Login: Date/Time Relinquished by:(Signature) Date: Time. Received for lab by; (Signature) Date: Time: / �/ • 8", il� Hold: Conditio%{ NCF / Oi7 Page 1 of 1 Chain -of -Custody -Record COC ID # 00051834 9 [TURN AROUND TIME TANDARD Speedway Project Information Speedway Store #: C210007984 Address: 2401 S Cannon Blvd City: Kannapolis Phone #: Speedway Proj. Mgr: Charles Chiara AFE #: 190192 Facility ID 0000031744 State: NC Fax #: **INVOICE TO SPEEDWAY** Work Order #: 1103786264 Lab Information Lab: Pace Analytical Services (TN) Consultant: Geological Resources, Inc. - Monroe, NC Project Mgr: Nicole Long Address: 3502 Hayes Road, Monroe, NC 28110 Phone #: Fax #: Sampler: Alex Lin Shipped: FedExp Tracking #: 120357752248 Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks MW-1 09/13/2019 09:42am W 1 VOA NA2S203 EDB 504.1 NC Task Code 280 504.1 Relinquished by: Date Time Received by: Date Time Relinquished by: Date Time Received by laboratory: Date Time Special Reporting Requirements: Lab Notes: Temp Speedway LLC. 1/1 https://www.speedway-ids.com Chain of Custody Analysis to be Performed COC ID # 51834 Analysis Name: EDB 504.1 NC Task Code 280 ( Water ) Analysis Description / Method: EDB by 504.1 / 504.1 Container Type / Preservative: VOA / NA2S203 Analytes: 1,2-Dibromoethane ug/L Chain -of -Custody -Record Printed: 11 /03/2019 Speedway LLC. 1/1 https://www.speedway-ids.com aceAnalytical o ANALYTICAL REPORT National Center for Testing & Innovation September 24, 2019 • #r Geological Resources- NC Speedway Sample Delivery Group: L1135637 Samples Received: 09/04/2019 Project Number: 5194 Description: Speedway 7984 Site: 7984 Report To: Ms. Nicole Long 3502 Hayes Rd. Charlotte, NC 28110 Entire Report Reviewed By iLzlc�' T. Alan Harvill Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received. 4 V — 16 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 1 of 39 TABLE OF CONTENTS ONE LAB. NATIONWIDE. Cp: Cover Page Tc: Table of Contents Ss: Sample Summary Cn: Case Narrative Sr: Sample Results MW-1 (2.5') L1135637-01 MW-1 L1135637-02 Qc: Quality Control Summary Total Solids by Method 2540 G-2011 Metals (ICP) by Method 6010D Volatile Petroleum Hydrocarbons by Method MADEPV Volatile Organic Compounds (GC) by Method 8015D/GRO Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011 Volatile Organic Compounds (GC/MS) by Method 8260D Semi -Volatile Organic Compounds (GC) by Method 8015C TPH by Method MADEPE Semi Volatile Organic Compounds (GC/MS) by Method 625.1 GI: Glossary of Terms Al: Accreditations & Locations Sc: Sample Chain of Custody 1 2 3 4 5 5 6 10 10 11 12 13 14 15 23 24 25 26 31 32 33 Fn FS [Cn] FS-r RC F, rAl FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 2 of 39 SAMPLE SUMMARY ONE LAB. NATIONWIDE. Collected by Collected date/time Received date/time MW-1 (2.5') L1135637-01 Solid Corey N. Buchanan 09/03/1912:11 09/04/1908:45 FP1 Method Batch Dilution Preparation Analysis Analyst Location date/time date/time FTC Total Solids by Method 2540 G-2011 WG1343147 1 09/11/1914:22 09/11/1914:34 KDW Mt. Juliet, TN Volatile Organic Compounds (GC) by Method 8015D/GRO WG1342410 1 09/03/1912:11 09/09/1917:19 BMB Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 8260D WG1342266 1.13 09/03/1912:11 09/09/1914:31 JAH Mt. Juliet, TN Semi -Volatile Organic Compounds (GC) by Method 8015C WG1341417 1 09/06/19 21:31 09/07/1918:57 KME Mt. Juliet, TN 4 Cn Collected by Collected date/time Received date/time MW-1 L1135637-02 GW Corey N. Buchanan 09/03/1915:57 09/04/19 08:45 FSr Method Batch Dilution Preparation Analysis Analyst Location date/time date/time 6QC Metals (ICP) by Method 6010D WG1340429 1 09/05/1915:05 09/06/19 09:21 TRB Mt. Juliet, TN Volatile Petroleum Hydrocarbons by Method MADEPV WG1342188 1 09/09/19 09:04 09/09/19 09:04 ACG Mt. Juliet, TN Volatile Organic Compounds (GC/MS) by Method 6200E-1997 WG1345539 1 09/13/1917:39 09/13/1917:39 ADM Mt. Juliet, TN GI Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011 WG1345376 1 09/13/1916:41 09/13/1916:41 JHH Mt. Juliet, TN TPH by Method MADEPE WG1341347 1 09/06/1911:57 09/10/1915:43 SHG Mt. Juliet, TN FAI TPH by Method MADEPE WG1341347 1 09/06/1911:57 09/10/19 21:26 SHG Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 625.1 WG1340629 1 09/06/19 08:22 09/09/1916:03 LEA Mt. Juliet, TN FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 3 of 39 CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the FP1 appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FTc have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FSS knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. FSr 6 QC r �GI iz T. Alan Harvill rAl Project Manager Project Narrative FSC Due to multiple preparation procedures, calculated analytes are not reported in the quality control samples for EPH and VPH Methods. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 4 of 39 SAMPLE RESULTS - 01 L1135637 ONE LAB. NATIONWIDE. MW-1 (2.5') Collected date/time: 09/03/19 12:11 Total Solids by Method 2540 G-2011 Result Qualifier Dilution Analysis Batch Analyte % date / time Total Solids 88.1 1 09/11/201914:34 WG1343147 Volatile Organic Compounds (GC) by Method 8015D/GRO Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) Low Fraction ND 0.113 1 09/09/201917:19 WG1342410 (S) a, a, a-Trifluorotoluene(FID) 98.3 77.0-120 091091201917:19 WG1342410 Volatile Organic Compounds (GC/MS) by Method 8260D Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time Benzene ND 0.00128 1.13 09/09/201914:31 WG1342266 Toluene 0.00781 0.00641 1.13 09/09/201914:31 WG1342266 Ethylbenzene ND 0.00321 1.13 09/09/201914:31 WG1342266 Total Xylenes ND 0.00833 1.13 09/09/201914:31 WG1342266 (S) Toluene-d8 104 75.0-131 0910912019 14:31 WG1342266 (S)4-Bromof/uorobenzene 104 67.0-138 091091201914:31 WG1342266 (S)1,2-Dichloroethone-d4 110 70.0-130 091091201914:31 WG1342266 Semi -Volatile Organic Compounds (GC) by Method 8015C Result (dry) Qualifier RDL (dry) Dilution Analysis Batch Analyte mg/kg mg/kg date / time TPH (GC/FID) High Fraction ND 4.54 1 09/07/201918:57 WG1341417 (S) o-Terpheny/ 84.9 18.0-148 091071201918:57 WG1341417 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 5 of 39 M W-1 SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE. Collected date/time: 09/03/19 15:57 L1135637 Metals (ICP) by Method 6010D Analyte Lead Result Qualifier RDL ug/I ug/I ND 5.00 Volatile Petroleum Hydrocarbons by Method MADEPV Dilution Analysis Batch date / time 1 09/06/2019 09:21 WG1340429 Result Qualifier RDL Dilution Analysis Analyte ug/I ug/I date / time Unadjusted C5-C8 Aliphatics ND 100 1 09/09/2019 09:04 Unadjusted C9-C12 Aliphatics ND 100 1 09/09/2019 09:04 Unadjusted C9-C10 Aromatics ND 100 1 09/09/2019 09:04 Adjusted C5-C8 Aliphatics ND J 100 1 09/09/2019 09:04 Adjusted C9-C12 Aliphatics ND 100 1 09/09/2019 09:04 Total VPH ND 200 1 09/09/2019 09:04 Total Purgeable Hydrocarbons C5-C12 ND 200 1 09/09/2019 09:04 (S) 2,5-Dibromotoluene(FID) 93.2 70.0-130 0910912019 09:04 (S) 2,5-Dibromotoluene(PID) 94.7 70.0-130 0910912019 09:04 Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011 Result Qualifier RDL Dilution Analysis Analyte ug/I ug/I date / time 1,1,1,2-Tetrachloroethane ND 1.00 1 09/13/201916:41 1,1,1-Trichloroethane ND 1.00 1 09/13/201916:41 1,1,2,2-Tetrachloroethane ND 1.00 1 09/13/201916:41 1,1,2-Trichloroethane ND 1.00 1 09/13/201916:41 1,1-Dichloroethane ND 1.00 1 09/13/201916:41 1,1-Dichloroethene ND 1.00 1 09/13/201916:41 1,1-Dichloropropene ND 1.00 1 09/13/201916:41 1,2,3-Trichlorobe nzene ND 1.00 1 09/13/201916:41 1,2,3-Trichloropropane ND 2.50 1 09/13/201916:41 1,2,3-Trimethyl benzene ND 1.00 1 09/13/201916:41 1,2,4-Trichlorobenzene ND 1.00 1 09/13/201916:41 1,2,4-Trimethylbenzene ND 1.00 1 09/13/201916:41 1,2-Dibromo-3-Chloropropane ND 5.00 1 09/13/201916:41 1,2-Dibromoethane ND 1.00 1 09/13/201916:41 1,2-Dichlorobenzene ND 1.00 1 09/13/201916:41 1,2-Dichloroethane ND 1.00 1 09/13/201916:41 1,2-Dichloropropane ND 1.00 1 09/13/201916:41 1,3,5-Trimethyl benzene ND 1.00 1 09/13/201916:41 1,3-Dichlorobenzene ND 1.00 1 09/13/201916:41 1,3-Dichloropropane ND 1.00 1 09/13/201916:41 1,4-Dichlorobenzene ND 1.00 1 09/13/201916:41 2,2-Dichloropropane ND 1.00 1 09/13/201916:41 Benzene ND 1.00 1 09/13/201916:41 Bromobenzene ND 1.00 1 09/13/201916:41 Bromochloromethane ND J4 1.00 1 09/13/201916:41 Bromodichloromethane ND 1.00 1 09/13/201916:41 Bromoform ND 1.00 1 09/13/201916:41 Carbon tetrachloride ND 1.00 1 09/13/201916:41 Chlorobenzene ND 1.00 1 09/13/201916:41 Chloroethane ND 5.00 1 09/13/201916:41 Chloroform ND 5.00 1 09/13/201916:41 Chlorodibromomethane ND 1.00 1 09/13/201916:41 Dichlorodifluoromethane ND 5.00 1 09/13/201916:41 Di -isopropyl ether 1.22 1.00 1 09/13/201916:41 Ethanol ND 100 1 09/13/201916:41 Ethylbenzene ND 1.00 1 09/13/201916:41 Hexachloro-1,3-butadiene ND 1.00 1 09/13/201916:41 Batch WG1342188 WG1342188 WG1342188 WG1342188 WG1342188 WG1342188 WG1342188 WG1342188 WG1342188 Batch WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 WG1345376 FP1 FTc FSS 4 Cn Rc F ql FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 6 of 39 M W-1 SAMPLE RESULTS - 02 Collected date/time: 09/03/19 15:57 L1135637 Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011 ONE LAB. NATIONWIDE. Result Qualifier RDL Dilution Analysis Batch FP1 Analyte ug/I ug/I date / time Isopropylbenzene ND 1.00 1 09/13/201916:41 WG1345376 FTc Bromomethane ND 5.00 1 09/13/201916:41 WG1345376 Chloromethane ND 2.50 1 09/13/201916:41 WG1345376 Methyl tert-butyl ether 54.5 1.00 1 09/13/201916:41 WG1345376 FSS Dibromomethane ND 1.00 1 09/13/201916:41 WG1345376 Methylene Chloride ND 5.00 1 09/13/201916:41 WG1345376 rCn Naphthalene ND 5.00 1 09/13/201916:41 WG1345376 Styrene ND 1.00 1 09/13/201916:41 WG1345376 Tetrachloroethene ND 1.00 1 09/13/201916:41 WG1345376 Toluene ND 1.00 1 09/13/201916:41 WG1345376 Trichloroethene ND 1.00 1 09/13/201916:41 WG1345376 Fc Trichlorofluoromethane ND 5.00 1 09/13/201916:41 WG1345376 Vinyl chloride ND J4 1.00 1 09/13/201916:41 WG1345376 Total Xylenes ND 3.00 1 09/13/201916:41 WG1345376 GI cis-1,2-Dichloroethene ND 1.00 1 09/13/201916:41 WG1345376 cis-1,3-Dichloropropene ND 1.00 1 09/13/201916:41 WG1345376 FAI n-Butylbenzene ND 1.00 1 09/13/201916:41 WG1345376 n-Propylbenzene ND 1.00 1 09/13/201916:41 WG1345376 2-Chlorotoluene ND 1.00 1 09/13/201916:41 WG1345376 FSC p-Isopropyltoluene ND 1.00 1 09/13/201916:41 WG1345376 4-Chlorotoluene ND 1.00 1 09/13/201916:41 WG1345376 sec -Butyl benzene ND 1.00 1 09/13/201916:41 WG1345376 tert-Butylbenzene ND 1.00 1 09/13/201916:41 WG1345376 trans-1,2-Dichloroethene ND J4 1.00 1 09/13/201916:41 WG1345376 trans-1,3-Dichloropropene ND 1.00 1 09/13/201916:41 WG1345376 Ethyl tert-butyl ether ND 1.00 1 09/13/201916:41 WG1345376 t-Amyl Alcohol ND 50.0 1 09/13/201916:41 WG1345376 tert-Butyl alcohol 8.54 5.00 1 09/13/201916:41 WG1345376 tert-Amyl Methyl Ether 5.29 1.00 1 09/13/201916:41 WG1345376 Tert-Amyl Ethyl Ether ND 1.00 1 09/13/201916:41 WG1345376 tert-Butyl Formate ND 20.0 1 09/13/201917:39 WG1345539 (S) Toluene-d8 98.2 80.0-120 091131201916.41 WG1345376 (S) Toluene-d8 102 80.0-120 09113120191739 WG1345539 (S 1,2-Dich/oroethane-d4 97.0 70.0-130 0911312019 16.41 WG1345376 (S 1,2-Dich/oroethane-d4 96.6 70.0-130 09113120191739 WG1345539 (S)4-Bromofluorobenzene 97.7 77.0-126 091131201916.41 WG1345376 (S) 4-Bromofluorobenzene 93.3 77.0-126 09113120191739 WG1345539 TPH by Method MADEPE Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time Unadjusted C9-C18 Aliphatics ND 100 1 09/10/201915:43 WG1341347 Unadjusted C19-C36 Aliphatics ND 100 1 09/10/201915:43 WG1341347 Unadjusted C11-C22 Aromatics ND 100 1 09/10/2019 21:26 WG1341347 Unadjusted Total Petroleum ND 100 1 09/10/2019 21:26 WG1341347 Hydrocarbons Adjusted C11-C22 Aromatics ND 100 1 09/10/2019 21:26 WG1341347 Adjusted Total Petroleum Hydrocarbons ND 100 1 09/10/2019 21:26 WG1341347 (S) o-Terphenyl 64.7 40.0-140 0911012019 21.26 WG1341347 (S)1-Chloro-octadecone 42.9 40.0-140 091101201915.43 WG1341347 (S) 2-F/uorobipheny/ 83.1 40.0-140 0911012019 21.26 WG1341347 (S) 2-Bromonaphtha/ene 77.5 40.0-140 0911012019 21:26 WG1341347 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 7 of 39 M W-1 SAMPLE RESULTS - 02 ONE LAB. NATIONWIDE. Collected date/time: 09/03/19 15:57 L1135637 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 Result Qualifier RDL Dilution Analysis Batch I Cl7 Analyte ug/I ug/I date / time u 1-Methylnaphthalene ND 1.00 1 09/09/201916:03 WG1340629 FTc 2,4,6-Trichlorophenol ND 10.0 1 09/09/201916:03 WG1340629 2,4-Dichlorophenol ND 10.0 1 09/09/201916:03 WG1340629 2,4-Dimethylphenol ND 10.0 1 09/09/201916:03 WG1340629 FS 2,4-Dinitrophenol ND 50.0 1 09/09/201916:03 WG1340629 2,4-Dinitrotoluene ND 10.0 1 09/09/201916:03 WG1340629 [Cn] 2,6-Dinitrotoluene ND 10.0 1 09/09/201916:03 WG1340629 2-Chloronaphthalene ND 1.00 1 09/09/201916:03 WG1340629 2-Chlorophenol ND 10.0 1 09/09/201916:03 WG1340629 2-Methylnaphthalene ND 1.00 1 09/09/201916:03 WG1340629 2-Methylphenol ND 10.0 1 09/09/201916:03 WG1340629 6 QC 2-Nitrophenol ND 10.0 1 09/09/201916:03 WG1340629 3,3-Dichlorobenzidine ND 10.0 1 09/09/201916:03 WG1340629 3&4-Methyl Phenol ND 10.0 1 09/09/201916:03 WG1340629 F ql 4,6-Dinitro-2-methylphenol ND 10.0 1 09/09/201916:03 WG1340629 4-Bromophenyl-phenylether ND 10.0 1 09/09/201916:03 WG1340629 FAI 4-ChIoro-3-methyl phenol ND 10.0 1 09/09/201916:03 WG1340629 4-Chloroaniline ND 10.0 1 09/09/201916:03 WG1340629 4-Chlorophenyl-phenylether ND 10.0 1 09/09/201916:03 WG1340629 FSC 4-Nitrophenol ND 10.0 1 09/09/201916:03 WG1340629 Acenaphthene ND 1.00 1 09/09/201916:03 WG1340629 Acenaphthylene ND 1.00 1 09/09/201916:03 WG1340629 Anthracene ND 1.00 1 09/09/201916:03 WG1340629 Benzo(a)anth race ne ND 1.00 1 09/09/201916:03 WG1340629 Benzo(a)pyrene ND 1.00 1 09/09/201916:03 WG1340629 Benzo(b)fluoranthene ND 1.00 1 09/09/201916:03 WG1340629 Benzo(g,h,i)perylene ND 1.00 1 09/09/201916:03 WG1340629 Benzo(k)fluoranthene ND 1.00 1 09/09/201916:03 WG1340629 Benzoic acid ND 10.0 1 09/09/201916:03 WG1340629 Bis(2-chlorethoxy)methane ND 10.0 1 09/09/201916:03 WG1340629 Bis(2-chloroisopropyl)ether ND 10.0 1 09/09/201916:03 WG1340629 Bis(2-ethylhexyl)phthalate ND 3.00 1 09/09/201916:03 WG1340629 Benzylbutyl phthalate ND 3.00 1 09/09/201916:03 WG1340629 Chrysene ND 1.00 1 09/09/201916:03 WG1340629 Di-n-butyl phthalate 4.83 J4 3.00 1 09/09/201916:03 WG1340629 Di-n-octyl phthalate ND 3.00 1 09/09/201916:03 WG1340629 Dibenz(a,h)anthracene ND 1.00 1 09/09/201916:03 WG1340629 Dibenzofuran ND 10.0 1 09/09/201916:03 WG1340629 Diethyl phthalate ND 3.00 1 09/09/201916:03 WG1340629 Dimethyl phthalate ND 3.00 1 09/09/201916:03 WG1340629 Fluoranthene ND 1.00 1 09/09/201916:03 WG1340629 Fluorene ND 1.00 1 09/09/201916:03 WG1340629 Hexachlorobenzene ND 1.00 1 09/09/201916:03 WG1340629 Hexachloro-1,3-butadiene ND 10.0 1 09/09/201916:03 WG1340629 Hexachlorocyclopentadiene ND 10.0 1 09/09/201916:03 WG1340629 Hexachloroethane ND 10.0 1 09/09/201916:03 WG1340629 Indeno(1,2,3-cd)pyrene ND 1.00 1 09/09/201916:03 WG1340629 Isophorone ND 10.0 1 09/09/201916:03 WG1340629 n-Nitrosodi-n-propylamine ND 10.0 1 09/09/201916:03 WG1340629 n-Nitrosodiphenyla mine ND 10.0 1 09/09/201916:03 WG1340629 Naphthalene ND 1.00 1 09/09/201916:03 WG1340629 Nitrobenzene ND 10.0 1 09/09/201916:03 WG1340629 Pentachlorophenol ND 10.0 1 09/09/201916:03 WG1340629 Phenanthrene ND 1.00 1 09/09/201916:03 WG1340629 Phenol ND 10.0 1 09/09/201916:03 WG1340629 Pyrene ND 1.00 1 09/09/201916:03 WG1340629 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 8 of 39 ONE LAB. NATIONWIDE. MW-1 SAMPLE RESULTS - 02 Collected date/time: 09/03/19 15:57 L1135637 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time (S) 2-F/uorophenol 28.2 10.0-120 091091201916.03 WG1340629 (S) Phenol-d5 19.4 8.00-424 091091201916.03 WG1340629 (S) Nitrobenzene-d5 42.6 15.0-314 091091201916.03 WG1340629 (S) 2-F/uorobipheny/ 45.0 22.0-127 091091201916.03 WG1340629 (S)2,4,6-Tribromopheno/ 66.0 10.0-153 091091201916.03 WG1340629 (S) p-Terphenyl-d14 80.6 29.0-141 091091201916.03 WG1340629 Semi Volatile Organic Compounds (GC/MS) by Method 625.1 - TENTATIVELY IDENTIFIED COMPOUNDS Result Qualifier RDL Dilution Analysis Batch CAS # Analyte ug/I ug/I date / time Unknown-03 38.4 J N 0.000 1 09/09/201916:03 WG1340629 000096-49-1 Unknown-01 32.6 J N 0.000 1 09/09/201916:03 WG1340629 000105-58-8 Unknown-02 14.2 J N 0.000 1 09/09/201916:03 WG1340629 000111-76-2 Nonanoic Acid 14.0 J N 0.000 1 09/09/201916:03 WG1340629 000112-05-0 Octanoic Acid 8.88 J N 0.000 1 09/09/201916:03 WG1340629 000124-07-2 Unknown-10 6.94 J N 0.000 1 09/09/201916:03 WG1340629 027554-26-3 Cyclotrisiloxane, Hexamethyl- 6.54 J N 0.000 1 09/09/201916:03 WG1340629 000541-05-9 Unknown-08 5.85 J N 0.000 1 09/09/201916:03 WG1340629 025154-52-3 Unknown-07 4.81 J N 0.000 1 09/09/201916:03 WG1340629 000104-40-5 1,2-Benzenedicarboxylic Acid, Buty 4.72 J N 0.000 1 09/09/201916:03 WG1340629 017851-53-5 Tentatively Identified compounds (TIC) refers to substances not present in the list of target compounds. Therefore, not all TICS are identified and quantitated using individual standards. TIC listings are prepared utilizing a computerized library search routine of electron impact mass spectral data and evaluation of the relevant data by a mass spectral data specialist. Quantitation is accomplished by relative peak area of the TIC compared to that of the nearest internal standard from the total ion chromatogram. TICs are identified and quantitated only if the peak area is 10% or more of that of the nearest internal standard. FP FTC FSS Fn N Rc F FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 9 of 39 WG1343147 Total Solids by Method 2540 G-2011 Method Blank (MB) (MB) R3449740-1 09/11/1914:34 MB Result MB Qualifier MB MDL Analyte % % Total Solids 0.00100 L1135623-01 Original Sample (OS) • Duplicate (DUP) MB RDL (OS) L1135623-01 09/11/1914:34 • (DUP) R3449740-3 09/11/1914:34 Original Result DUP Result Dilution DUP RPD Analyte % % % Total Solids 11.9 12.0 1 0.198 Laboratory Control Sample (LCS) QUALITY CONTROL SUMMARY L1135637-01 DUP Qualifier DUP RPD Limits 10 (LCS) R3449740-2 09/11/1914:34 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte % % % % Total Solids 50.0 49.9 99.9 85.0-115 ONE LAB. NATIONWIDE. — I Cp FTc FSS 4 — Cn FSr — �GI FAI [Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 10 of 39 WG1340429 Metals (ICP) by Method 6010D Method Blank (MB) (MB) R3447829-1 09/06/19 07:58 MB Result Analyte ug/I Lead 1.98 MB Qualifier MB MDL MB RDL ug/I ug/1 J 1.90 5.00 QUALITY CONTROL SUMMARY L1135637-02 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3447829-2 09/06/19 08:00 • (LCSD) R3447829-3 09/06/19 08:03 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/I ug/I ug/I % % % % % Lead 1000 997 1010 99.7 101 80.0-120 1.47 20 L1135013-32 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1135013-32 09/06/19 08:06 • (MS) R3447829-5 09/06/19 08:12 • (MSD) R3447829-6 09/06/19 08:14 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte ug/I ug/I ug/I ug/I % % Lead 1000 2.74 1010 1020 100 101 Dilution Rec. Limits MS Qualifier MSD Qualifier RPD 1 75.0-125 1.11 ONE LAB. NATIONWIDE. RPD Limits 20 - I Cp FTc FSS 4 — Cn FSr — 7G1 — $AI [Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 11 of 39 WG1342188 Volatile Petroleum Hydrocarbons by Method MADEPV Method Blank (MB) (MB) R3449149-3 09/08/1914:15 MB Result Analyte ug/I Unadjusted C5-C8 Aliphatics U Unadjusted C9-C12 Aliphatics U Unadjusted C9-C10 Aromatics U Adjusted C5-C8 Aliphatics U Adjusted C9-C12 Aliphatics U Total VPH U Total Purgeable Hydrocarbons 76.2 C5-C12 (S)2,5-Dibromotoluene(FID) 94.2 (S)2,5-Dibromotoluene(PID) 96.6 MB Qualifier MB MDL MB RDL ug/I ug/I QUALITY CONTROL SUMMARY L1135637-02 33.3 100 33.3 100 33.3 100 33.3 100 33.3 100 66.7 200 J 66.7 200 70.0-130 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3449149-1 09/08/1910:19 • (LCSD) R3449149-2 09/08/1910:50 Spike Amount LCS Result LCSD Result LCS Rec. Analyte ug/I ug/I ug/I % Unadjusted C5-C8 Aliphatics 1200 1330 1330 ill Unadjusted C9-C12 Aliphatics 1400 1390 1400 99.0 Unadjusted C9-C10 Aromatics 200 194 195 96.8 Total VPH 2800 2910 2920 104 Total Purgeable Hydrocarbons 2800 3080 3090 110 C5-C12 (S) 2,5-Dibromotoluene(FID) 101 (S) 2,5-Dibromotoluene(P/D) 101 LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD ill 70.0-130 0.0810 99.6 70.0-130 0.647 97.4 70.0-130 0.643 104 70.0-130 0.0343 110 70.0-130 0.443 105 70.0-130 105 70.0-130 RPD Limits 50 50 50 50 Z ONE LAB. NATIONWIDE. FP1 FTc FSS 4 Cn FSr 7G1 FAI [Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 12 of 39 WG1342410 Volatile Organic Compounds (GC) by Method 8015D/GRO Method Blank (MB) QUALITY CONTROL SUMMARY L1135637-01 ONE LAB. NATIONWIDE. (MB) R3449197-3 09/09/1911:37 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg TPH (GC/FID) Low Fraction U 0.0217 0.100 (S) 100 o, o, o-Trifluorotoluene(FID) 77.0-120 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3449197-1 09/09/1910:25 • (LCSD) R3449197-2 09/09/1910:49 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg % % % % % TPH (GC/FID) Low Fraction 5.50 4.47 4.30 81.4 78.1 72.0-127 4.06 20 (S) a, a, a- Trifluorotoluene(FID) 102 102 77.0-120 L1135783-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1135783-02 09/09/1918:07 • (MS) R3449197-4 09/09/19 20:55 • (MSD) R3449197-5 09/09/19 21:19 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mg/kg mg/kg mg/kg mg/kg % % TPH (GC/FID) Low Fraction 5.50 ND 68.0 54.0 49.5 39.2 (S) 108 106 a, a, a- Trifluorotoluene(FID) Dilution Rec. Limits MS Qualifier MSD Qualifier RPD 25 10.0-151 23.0 77.0-120 RPD Limits 28 FP1 FTC FSS H 5 Sr �GI FAI [SC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 13 of 39 WG1345539 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 620OB-1997 L1135637-02 Method Blank (MB) (MB) R3450656-3 09/13/1911:14 MB Result Analyte ug/I tert-Butyl formate U (S) Toluene-d8 ill (S) 4-Bromofluorobenzene 98.1 (S)1,2-Dich/oroethane-d4 110 MB Qualifier MB MDL MB RDL ug/I ug/I 3.30 20.0 80.0-120 77.0-126 70.0-130 Laboratory Control Sample (LCS) (LCS) R3450656-2 09/13/1910:09 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte ug/I ug/I % % tert-Butyl Formate 100 139 139 10.0-160 (S) Toluene-d8 104 80.0-120 (S) 4-Bromofluorobenzene 92.1 77.0-126 (S)1,2-Dich/oroethane-d4 112 70.0-130 ONE LAB. NATIONWIDE. FP1 FTC FSS 4 Cn FSr 7G1 FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 14 of 39 WG1345376 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011 L1135637-02 ONE LAB. NATIONWIDE. Method Blank (MB) (MB) R3450551-3 09/13/1914:00 MB Result Analyte ug/I MB Qualifier MB MDL MB RDL ug/I ug/I Benzene U 0.331 1.00 Bromobenzene U 0.352 1.00 Bromodichloromethane U 0.380 1.00 Bromochloromethane U 0.520 1.00 Bromoform U 0.469 1.00 Bromomethane U 0.866 5.00 n-Butylbenzene U 0.361 1.00 sec -Butyl benzene U 0.365 1.00 tert-Butylbenzene U 0.399 1.00 Carbon tetrachloride U 0.379 1.00 Chlorobenzene U 0.348 1.00 Chlorodibromomethane U 0.327 1.00 Chloroethane U 0.453 5.00 Chloroform U 0.324 5.00 Chloromethane U 0.276 2.50 2-Chlorotoluene U 0.375 1.00 4-Chlorotoluene U 0.351 1.00 1,2-Dibromo-3-Chloropropane U 1.33 5.00 1,2-Dibromoethane U 0.381 1.00 Dibromomethane U 0.346 1.00 1,2-Dichlorobenzene U 0.349 1.00 1,3-Dichlorobenzene U 0.220 1.00 1,4-Dichlorobenzene U 0.274 1.00 Dichlorodifluoromethane U 0.551 5.00 1,1-Dichloroethane U 0.259 1.00 1,2-Dichloroethane U 0.361 1.00 1,1-Dichloroethene U 0.398 1.00 cis-1,2-Dichloroethene U 0.260 1.00 trans-1,2-Dichloroethene U 0.396 1.00 1,2-Dichloropropane U 0.306 1.00 1,1-Dichloropropene U 0.352 1.00 1,3-Dichloropropane U 0.366 1.00 cis-1,3-Dichloropropene U 0.419 1.00 trans-1,3-Dichloropropene U 0.419 1.00 2,2-Dichloropropane U 0.321 1.00 Di -isopropyl ether U 0.320 1.00 Ethylbenzene U 0.384 1.00 Ethanol U 42.0 100 Hexachloro-1,3-butadiene U 0.256 1.00 Isopropylbenzene U 0.326 1.00 ACCOUNT: Geological Resources- NC Speedway PROJECT: SDG: DATE/TIME: PAGE: 5194 L1135637 09/24/19 09:49 15 of 39 FP1 FTC FSS [Cn] FSr 7G1 FAI FSC WG1345376 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011 L1135637-02 ONE LAB. NATIONWIDE. Method Blank (MB) (MB) R3450551-3 09/13/1914:00 MB Result Analyte ug/I p-Isopropyltoluene U Methylene Chloride U Methyl tert-butyl ether U Naphthalene U n-Propylbenzene U Styrene U 1,1,1,2-Tetrachloroethane U 1,1,2,2-Tetrachloroethane U Tetrachloroethene U Toluene U 1,2,3-Trichlorobenzene U 1,2,4-Trichlorobenzene U 1,1,1-Trichloroethane U 1,1,2-Trichloroethane U Trichloroethene U Trichlorofluoromethane U 1,2,3-Trichloropropane U 1,2,3-Trimethylbenzene U 1,2,4-Trimethylbenzene U 1,3,5-Trimethyl benzene U Vinyl chloride U Xylenes, Total U tert-Amyl Methyl Ether U Ethyl tert-butyl ether U tert-Butyl alcohol U t-Amyl Alcohol U Tert-Amyl Ethyl Ether U (S) Toluene-d8 100 (S) 4-Bromof/uorobenzene 101 (S) 1,2-Dich/oroethane-d4 97.3 Method Blank (MB) MB Qualifier MB MDL MB RDL ug/I ug/I 0.350 1.00 1.00 5.00 0.367 1.00 1.00 5.00 0.349 1.00 0.307 1.00 0.385 1.00 0.130 1.00 0.372 1.00 0.412 1.00 0.230 1.00 0.355 1.00 0.319 1.00 0.383 1.00 0.398 1.00 1.20 5.00 0.807 2.50 0.355 1.00 0.373 1.00 0.387 1.00 0.259 1.00 1.06 3.00 0.260 1.00 0.270 1.00 2.40 5.00 4.90 50.0 0.401 1.00 80.0-120 77.0-126 70.0-130 (MB) R3450551-3 09/13/1914:00 MB Result MB Qualifier MB MDL MB RDL Analyte ug/1 ug/I ug/I Bromobenzene U 0.352 1.00 Benzene U 0.331 1.00 Bromodichloromethane U 0.380 1.00 ACCOUNT: Geological Resources- NC Speedway PROJECT: SDG: DATE/TIME: PAGE: 5194 L1135637 09/24/19 09:49 16 of 39 FP1 FTC FSS 4 Cn FSr 7G1 FAI FSC WG1345376 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011 L1135637-02 ONE LAB. NATIONWIDE. Method Blank (MB) (MB) R3450551-3 09/13/1914:00 MB Result Analyte ug/I Bromochloromethane U Bromoform U Bromomethane U n-Butylbenzene U sec -Butyl benzene U tert-Butylbenzene U Carbon tetrachloride U Chlorobenzene U Chlorodibromomethane U Chloroethane U Chloroform U Chloromethane U 2-Chlorotoluene U 4-Chlorotoluene U 1,2-Dibromo-3-Chloropropane U Dibromomethane U 1,2-Dichlorobenzene U 1,2-Dibromoethane U 1,3-Dichlorobenzene U 1,4-Dichlorobenzene U Dichlorodifluoromethane U 1,1-Dichloroethane U 1,1-Dichloroethene U cis-1,2-Dichloroethene U 1,2-Dichloroethane U trans-1,2-Dichloroethene U 1,2-Dichloropropane U 1,1-Dichloropropene U 1,3-Dichloropropane U cis-1,3-Dichloropropene U trans-1,3-Dichloropropene U 2,2-Dichloropropane U Di -isopropyl ether U Ethanol U Ethylbenzene U Hexachloro-1,3-butadiene U p-Isopropyltoluene U Isopropylbenzene U Methylene Chloride U Methyl tert-butyl ether U MB Qualifier MB MDL ug/I 0.520 0.469 0.866 0.361 0.365 0.399 0.379 0.348 0.327 0.453 0.324 0.276 0.375 0.351 1.33 0.346 0.349 0.381 0.220 0.274 0.551 0.259 0.398 0.260 0.361 0.396 0.306 0.352 0.366 0.419 0.419 0.321 0.320 42.0 0.384 0.256 0.350 0.326 1.00 0.367 MB RDL ug/I 1.00 1.00 5.00 1.00 1.00 1.00 1.00 1.00 1.00 5.00 5.00 2.50 1.00 1.00 5.00 1.00 1.00 1.00 1.00 1.00 5.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 100 1.00 1.00 1.00 1.00 5.00 1.00 FP1 FTC FSS [Cn] FSr 7G1 FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 17 of 39 WG1345376 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011 L1135637-02 Method Blank (MB) Cp (MB) R3450551-3 09/13/1914:00 MB Result MB Qualifier MB MDL MB RDL z Analyte ug/I ug/I ug/I TC n-Propylbenzene U 0.349 1.00 Styrene U 0.307 1.00 E 1,1,1,2-Tetrachloroethane U 0.385 1.00 Naphthalene U 1.00 5.00 1,1,2,2-Tetrachloroethane U 0.130 1.00 FCn Tetrachloroethene U 0.372 1.00 1,2,3-Trichlorobenzene U 0.230 1.00 E 1,2,4-Trichlorobenzene U 0.355 1.00 1,1,1-Trichloroethane U 0.319 1.00 1,1,2-Trichloroethane U 0.383 1.00 ce Toluene U 0.412 1.00 Trichloroethene U 0.398 1.00 FG I Trichlorofluoromethane U 1.20 5.00 1,2,3-Trichloropropane U 0.807 2.50 1,2,3-Trimethylbenzene U 0.355 1.00 FAI Vinyl chloride U 0.259 1.00 1,2,4-Trimethylbenzene U 0.373 1.00 E 1,3,5-Trimethylbenzene U 0.387 1.00 tert-Amyl Methyl Ether U 0.260 1.00 Ethyl tert-butyl ether U 0.270 1.00 tert-Butyl alcohol U 2.40 5.00 Xylenes, Total U 1.06 3.00 t-Amyl Alcohol U 4.90 50.0 Tert-Amyl Ethyl Ether U 0.401 1.00 (S) Toluene-d8 100 80.0-120 (S) 4-Bromofluorobenzene 101 77.0-126 (S) 1,2-Dich/oroethone-d4 97.3 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3450551-1 09/13/1912:58 • (LCSD) R3450551-2 09/13/1913:19 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/I ug/I ug/I % % % % % Benzene 25.0 27.2 25.9 109 104 70.0-123 4.92 20 Bromobenzene 25.0 23.8 22.3 95.3 89.3 73.0-121 6.52 20 Bromodichloromethane 25.0 28.4 26.9 113 108 75.0-120 5.14 20 Bromochloromethane 25.0 30.8 30.0 123 120 76.0-122 J4 2.60 20 Bromoform 25.0 25.7 24.5 103 98.1 68.0-132 4.70 20 Bromomethane 25.0 34.6 31.8 138 127 10.0-160 8.26 25 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 18 of 39 WG1345376 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011 L1135637-02 ONE LAB. NATIONWIDE. Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3450551-1 09/13/1912:58 • (LCSD) R3450551-2 09/13/1913:19 Spike Amount LCS Result LCSD Result Analyte ug/I ug/I ug/I n-Butylbenzene 25.0 28.4 26.0 sec -Butyl benzene 25.0 27.8 25.5 tert-Butylbenzene 25.0 28.6 26.2 Carbon tetrachloride 25.0 30.7 29.1 Chlorobenzene 25.0 27.4 26.8 Chlorodibromomethane 25.0 25.7 24.9 Chloroethane 25.0 31.0 27.9 Chloroform 25.0 27.2 26.6 Chloromethane 25.0 28.3 26.5 2-Chlorotoluene 25.0 28.2 25.7 4-Chlorotoluene 25.0 28.7 26.5 1,2-Dibromo-3-Chloropropane 25.0 26.2 25.6 1,2-Dibromoethane 25.0 25.5 24.9 Dibromomethane 25.0 28.3 27.0 1,2-Dichlorobenzene 25.0 27.6 26.4 1,3-Dichlorobenzene 25.0 28.5 27.1 1,4-Dichlorobenzene 25.0 27.2 25.8 Dichlorodifluoromethane 25.0 35.2 33.5 1,1-Dichloroethane 25.0 29.8 28.1 1,2-Dichloroethane 25.0 27.5 25.7 1,1-Dichloroethene 25.0 30.3 28.9 cis-1,2-Dichloroethene 25.0 29.7 28.1 trans-1,2-Dichloroethene 25.0 30.3 28.5 1,2-Dichloropropane 25.0 27.8 26.2 1,1-Dichloropropene 25.0 30.0 28.2 1,3-Dichloropropane 25.0 26.8 26.1 cis-1,3-Dichloropropene 25.0 27.8 26.8 trans-1,3-Dichloropropene 25.0 25.9 25.2 2,2-Dichloropropane 25.0 24.8 25.2 Di -isopropyl ether 25.0 26.1 25.1 Ethylbenzene 25.0 25.8 25.0 Hexachloro-1,3-butadiene 25.0 27.3 25.8 Isopropylbenzene 25.0 26.7 25.5 p-Isopropyltoluene 25.0 27.6 26.2 Methylene Chloride 25.0 26.3 24.7 Methyl tert-butyl ether 25.0 26.9 25.8 Naphthalene 25.0 26.8 24.8 n-Propylbenzene 25.0 28.9 27.1 Styrene 25.0 26.6 25.7 1,1,1,2-Tetrachloroethane 25.0 25.2 24.8 ACCOUNT: Geological Resources- NC Speedway LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 113 104 73.0-125 8.65 20 111 102 75.0-125 8.45 20 114 105 76.0-124 8.68 20 123 116 68.0-126 5.58 20 109 107 80.0-121 2.08 20 103 99.4 77.0-125 3.48 20 124 111 47.0-150 10.8 20 109 107 73.0-120 1.90 20 113 106 41.0-142 6.33 20 113 103 76.0-123 9.23 20 115 106 75.0-122 8.22 20 105 102 58.0-134 2.29 20 102 99.5 80.0-122 2.54 20 113 108 80.0-120 4.84 20 110 105 79.0-121 4.60 20 114 109 79.0-120 4.83 20 109 103 79.0-120 5.26 20 141 134 51.0-149 4.84 20 119 112 70.0-126 5.86 20 110 103 70.0-128 6.49 20 121 115 71.0-124 4.97 20 119 112 73.0-120 5.65 20 121 114 73.0-120 J4 6.10 20 111 105 77.0-125 6.10 20 120 113 74.0-126 6.13 20 107 104 80.0-120 2.75 20 111 107 80.0-123 3.83 20 104 101 78.0-124 2.88 20 99.2 101 58.0-130 1.43 20 104 101 58.0-138 3.76 20 103 100 79.0-123 3.32 20 109 103 54.0-138 5.45 20 107 102 76.0-127 4.49 20 110 105 76.0-125 5.20 20 105 98.8 67.0-120 6.23 20 108 103 68.0-125 4.35 20 107 99.1 54.0-135 7.87 20 116 108 77.0-124 6.71 20 106 103 73.0-130 3.36 20 101 99.2 75.0-125 1.71 20 PROJECT: SDG: DATE/TIME: PAGE: 5194 L1135637 09/24/19 09:49 19 of 39 FP1 FTC FSS [Cn] FSr 7G1 FAI FSC WG1345376 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011 L1135637-02 ONE LAB. NATIONWIDE. Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3450551-1 09/13/1912:58 • (LCSD) R3450551-2 09/13/1913:19 Spike Amount LCS Result LCSD Result Analyte ug/I ug/I ug/I 1,1,2,2-Tetrachloroethane 25.0 27.7 26.5 Tetrachloroethene 25.0 26.9 26.7 Toluene 25.0 24.3 23.6 1,2,3-Trichlorobenzene 25.0 27.5 25.9 1,2,4-Trichlorobenzene 25.0 27.4 26.0 1,1,1-Trichloroethane 25.0 29.8 28.8 1,1,2-Trichloroethane 25.0 25.4 25.1 Trichloroethene 25.0 29.3 27.9 Trichlorofluoromethane 25.0 27.0 25.5 1,2,3-Trichloropropane 25.0 27.3 26.0 1,2,3-Trimethyl benzene 25.0 28.5 26.1 1,2,4-Trimethylbenzene 25.0 27.1 26.0 1,3,5-Trimethyl benzene 25.0 27.5 24.7 Vinyl chloride 25.0 33.5 31.2 Xylenes, Total 75.0 78.3 76.4 Tert-Amyl Ethyl Ether 25.0 27.2 26.4 ethanol 1250 1420 1320 tert-Butyl alcohol 125 140 132 (S) Toluene-d8 (S) 4-Bromof/uorobenzene (S) 1,2-Dich/oroethane-d4 LCS Rec. LCSD Rec. Rec. Limits ill 106 65.0-130 108 107 72.0-132 97.2 94.4 79.0-120 110 104 50.0-138 110 104 57.0-137 119 115 73.0-124 102 101 80.0-120 117 ill 78.0-124 108 102 59.0-147 109 104 73.0-130 114 104 77.0-120 108 104 76.0-121 110 98.7 76.0-122 134 125 67.0-131 104 102 79.0-123 109 105 70.0-130 114 105 10.0-160 112 106 27.0-160 90.0 90.1 80.0-120 95.5 93.1 77.0-126 110 106 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3450551-1 09/13/1912:58 • (LCSD) R3450551-2 09/13/1913:19 Spike Amount LCS Result LCSD Result Analyte ug/I ug/I ug/I Bromobenzene 25.0 23.8 22.3 Bromodichloromethane 25.0 28.4 26.9 Bromochloromethane 25.0 30.8 30.0 Bromoform 25.0 25.7 24.5 Bromomethane 25.0 34.6 31.8 n-Butylbenzene 25.0 28.4 26.0 sec -Butyl benzene 25.0 27.8 25.5 tert-Butylbenzene 25.0 28.6 26.2 Carbon tetrachloride 25.0 30.7 29.1 Chlorobenzene 25.0 27.4 26.8 Chlorodibromomethane 25.0 25.7 24.9 Chloroethane 25.0 31.0 27.9 ACCOUNT: Geological Resources- NC Speedway LCS Qualifier J4 LCSD Qualifier RPD 4.61 0.771 2.97 6.09 5.19 3.48 1.14 4.85 5.64 4.81 8.65 4.33 10.7 7.07 2.46 3.11 7.45 5.66 RPD Limits 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 30 30 LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 95.3 89.3 73.0-121 6.52 20 113 108 75.0-120 5.14 20 123 120 76.0-122 J4 2.60 20 103 98.1 68.0-132 4.70 20 138 127 10.0-160 8.26 25 113 104 73.0-125 8.65 20 ill 102 75.0-125 8.45 20 114 105 76.0-124 8.68 20 123 116 68.0-126 5.58 20 109 107 80.0-121 2.08 20 103 99.4 77.0-125 3.48 20 124 ill 47.0-150 10.8 20 PROJECT: SDG: DATE/TIME: PAGE: 5194 L1135637 09/24/19 09:49 20 of 39 FP1 FTC FSS [Cn] FSr 7G1 FAI FSC WG1345376 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011 L1135637-02 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) Cp (LCS) R3450551-1 09/13/1912:58 • (LCSD) R3450551-2 09/13/1913:19 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits z Analyte ug/I ug/I ug/I % % % % % TC Chloroform 25.0 27.2 26.6 109 107 73.0-120 1.90 20 Chloromethane 25.0 28.3 26.5 113 106 41.0-142 6.33 20 E 2-Chlorotoluene 25.0 28.2 25.7 113 103 76.0-123 9.23 20 4-Chlorotoluene 25.0 28.7 26.5 115 106 75.0-122 8.22 20 1,2-Dibromo-3-Chloropropane 25.0 26.2 25.6 105 102 58.0-134 2.29 20 FC n Benzene 25.0 27.2 25.9 109 104 70.0-123 4.92 20 Dibromomethane 25.0 28.3 27.0 113 108 80.0-120 4.84 20 E 1,2-Dichlorobenzene 25.0 27.6 26.4 110 105 79.0-121 4.60 20 1,3-Dichlorobenzene 25.0 28.5 27.1 114 109 79.0-120 4.83 20 1,4-Dichlorobenzene 25.0 27.2 25.8 109 103 79.0-120 5.26 20 ce Dichlorodifluoromethane 25.0 35.2 33.5 141 134 51.0-149 4.84 20 1,1-Dichloroethane 25.0 29.8 28.1 119 112 70.0-126 5.86 20 FG I 1,1-Dichloroethene 25.0 30.3 28.9 121 115 71.0-124 4.97 20 cis-1,2-Dichloroethene 25.0 29.7 28.1 119 112 73.0-120 5.65 20 trans-1,2-Dichloroethene 25.0 30.3 28.5 121 114 73.0-120 J4 6.10 20 FAI 1,2-Dichloropropane 25.0 27.8 26.2 111 105 77.0-125 6.10 20 1,1-Dichloropropene 25.0 30.0 28.2 120 113 74.0-126 6.13 20 E 1,3-Dichloropropane 25.0 26.8 26.1 107 104 80.0-120 2.75 20 cis-1,3-Dichloropropene 25.0 27.8 26.8 111 107 80.0-123 3.83 20 trans-1,3-Dichloropropene 25.0 25.9 25.2 104 101 78.0-124 2.88 20 2,2-Dichloropropane 25.0 24.8 25.2 99.2 101 58.0-130 1.43 20 Di -isopropyl ether 25.0 26.1 25.1 104 101 58.0-138 3.76 20 1,2-Dibromoethane 25.0 25.5 24.9 102 99.5 80.0-122 2.54 20 Hexachloro-1,3-butadiene 25.0 27.3 25.8 109 103 54.0-138 5.45 20 p-Isopropyltoluene 25.0 27.6 26.2 110 105 76.0-125 5.20 20 1,2-Dichloroethane 25.0 27.5 25.7 110 103 70.0-128 6.49 20 Methylene Chloride 25.0 26.3 24.7 105 98.8 67.0-120 6.23 20 n-Propylbenzene 25.0 28.9 27.1 116 108 77.0-124 6.71 20 Styrene 25.0 26.6 25.7 106 103 73.0-130 3.36 20 1,1,1,2-Tetrachloroethane 25.0 25.2 24.8 101 99.2 75.0-125 1.71 20 1,1,2,2-Tetrachloroethane 25.0 27.7 26.5 111 106 65.0-130 4.61 20 Ethylbenzene 25.0 25.8 25.0 103 100 79.0-123 3.32 20 Tetrachloroethene 25.0 26.9 26.7 108 107 72.0-132 0.771 20 1,2,3-Trichlorobenzene 25.0 27.5 25.9 110 104 50.0-138 6.09 20 1,2,4-Trichlorobenzene 25.0 27.4 26.0 110 104 57.0-137 5.19 20 1,1,1-Trichloroethane 25.0 29.8 28.8 119 115 73.0-124 3.48 20 1,1,2-Trichloroethane 25.0 25.4 25.1 102 101 80.0-120 1.14 20 Isopropylbenzene 25.0 26.7 25.5 107 102 76.0-127 4.49 20 Trichloroethene 25.0 29.3 27.9 117 111 78.0-124 4.85 20 Trichlorofluoromethane 25.0 27.0 25.5 108 102 59.0-147 5.64 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 21 of 39 WG1345376 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 620OB-1997/620OB-2011 L1135637-02 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3450551-1 09/13/1912:58 • (LCSD) R3450551-2 09/13/1913:19 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier Analyte ug/I ug/I ug/I % % % 1,2,3-Trichloropropane 25.0 27.3 26.0 109 104 73.0-130 1,2,3-Trimethyl benzene 25.0 28.5 26.1 114 104 77.0-120 Methyl tert-butyl ether 25.0 26.9 25.8 108 103 68.0-125 Vinyl chloride 25.0 33.5 31.2 134 125 67.0-131 J4 Naphthalene 25.0 26.8 24.8 107 99.1 54.0-135 tert-Butyl alcohol 125 140 132 112 106 27.0-160 Toluene 25.0 24.3 23.6 97.2 94.4 79.0-120 1,2,4-Trimethylbenzene 25.0 27.1 26.0 108 104 76.0-121 1,3,5-Trimethyl benzene 25.0 27.5 24.7 110 98.7 76.0-122 Xylenes, Total 75.0 78.3 76.4 104 102 79.0-123 Tert-Amyl Ethyl Ether 25.0 27.2 26.4 109 105 70.0-130 ethanol 1250 1420 1320 114 105 10.0-160 (S) Toluene-d8 90.0 90.1 80.0-120 (S) 4-Bromof/uorobenzene 95.5 93.1 77.0-126 (S)1,2-Dich/oroethane-d4 110 106 70.0-130 LCSD Qualifier RPD RPD Limits 4.81 20 8.65 20 4.35 20 7.07 20 7.87 20 5.66 30 2.97 20 4.33 20 10.7 20 2.46 20 3.11 20 7.45 30 ONE LAB. NATIONWIDE. FP1 FTC FSS 4 Cn FSr 7G1 FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 22 of 39 WG1342266 Volatile Organic Compounds (GC/MS) by Method 8260D Method Blank (MB) QUALITY CONTROL SUMMARY L1135637-01 ONE LAB. NATIONWIDE. (MB) R3448962-3 09/09/1910:18 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Benzene U 0.000400 0.00100 Ethylbenzene U 0.000530 0.00250 Toluene U 0.00125 0.00500 Xylenes, Total U 0.00478 0.00650 (S) Toluene-d8 107 75.0-131 (S) 4-Bromof/uorobenzene 109 67.0-138 (S)1,2-Dich/oroethone-d4 108 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3448962-1 09/09/19 09:02 • (LCSD) R3448962-2 09/09/19 09:21 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg % % % % % Benzene 0.125 0.110 0.111 87.8 88.9 70.0-123 1.22 20 Ethylbenzene 0.125 0.111 0.113 88.5 90.2 74.0-126 1.92 20 Toluene 0.125 0.116 0.115 92.8 91.6 75.0-121 1.33 20 Xylenes, Total 0.375 0.346 0.347 92.3 92.5 72.0-127 0.289 20 (S) Toluene-d8 103 102 75.0-131 (S) 4-Bromofluorobenzene 101 102 67.0-138 (S)1,2-Dich/oroethone-d4 118 115 70.0-130 FP1 FTc FSS 4 Cn FSr �GI FAI [Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 23 of 39 WG1341417 Semi -Volatile Organic Compounds (GC) by Method 8015C Method Blank (MB) (MB) R3448246-1 09/07/1913:37 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg TPH (GC/FID) High Fraction U 0.769 4.00 (S) o-Terpheny/ 84.1 18.0-148 Laboratory Control Sample (LCS) QUALITY CONTROL SUMMARY L1135637-01 (LCS) R3448246-2 09/07/1913:49 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/kg mg/kg % % TPH (GC/FID) High Fraction 50.0 38.5 77.0 50.0-150 (S) o-Terpheny/ 90.1 18.0-148 L1135533-14 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1135533-14 09/07/1916:24 • (MS) R3448246-3 09/07/1916:37 • (MSD) R3448246-4 09/07/1916:50 Spike Amount Original Result MS Result (dry) MSD Result MS Rec. MSD Rec. (dry) (dry) (dry) Analyte mg/kg mg/kg mg/kg mg/kg % % TPH (GC/FID) High Fraction 71.0 6.54 50.2 56.9 61.6 71.0 (S) o-Terpheny/ 65.0 82.4 Dilution Rec. Limits MS Qualifier MSD Qualifier RPD 1 50.0-150 12.5 18.0-148 ONE LAB. NATIONWIDE. RPD Limits 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 24 of 39 WG1341347 QUALITY CONTROL SUMMARY TPH by Method MADEPE L1135637-02 Method Blank (MB) (MB) R3449425-1 09/10/19 11:37 MB Result MB Qualifier MB MDL MB RDL Analyte ug/I ug/I ug/I Unadjusted C9-C18 Aliphatics U 33.0 100 Unadjusted C19-06 Aliphatics U 33.0 100 (S)1-Chloro-octadecane 77.8 40.0-140 Method Blank (MB) (MB) R3449425-4 09/10/1912:42 MB Result MB Qualifier MB MDL MB RDL Analyte ug/I ug/I ug/I Unadjusted C11-C22 Aromatics U 33.0 100 (S) o-Terpheny/ 76.1 40.0-140 (S) 2-F/uorobipheny/ 80.1 40.0-140 (S) 2-Bromonophtha/ene 74.9 40.0-140 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3449425-2 09/10/1911:59 • (LCSD) R3449425-3 09/10/1912:21 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/I ug/I ug/I % % % % % Unadjusted C9-C18 Aliphatics 600 307 272 51.2 45.3 40.0-140 12.1 25 Unadjusted C19-C36 Aliphatics 800 682 657 85.3 82.1 40.0-140 3.73 25 (S)1-Chloro-octadecane 70.6 70.9 40.0-140 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3449425-5 09/10/1913:04 • (LCSD) R3449425-6 09/10/1913:26 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD Analyte ug/I ug/I ug/I % % % % Unadjusted C11-C22 Aromatics 1700 1420 1320 83.5 77.6 40.0-140 7.30 (S) o-Terpheny/ 80.5 75.6 40.0-140 (S)2-Fluorobiphenyl 87.9 82.9 40.0-140 (S) 2-Bromonaphtho/ene 82.7 78.1 40.0-140 RPD Limits 25 ONE LAB. NATIONWIDE. FP1 FTc FSS 4 Cn FSr 7G1 FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 25 of 39 WG1340629 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1135637-02 Method Blank (MB) (MB) R3448360-2 09/07/1911:11 MB Result Analyte ug/I MB Qualifier MB MDL MB RDL ug/I ug/I Acenaphthene U 0.316 1.00 Acenaphthylene U 0.309 1.00 Anthracene U 0.291 1.00 Benzo(a)anth race ne U 0.0975 1.00 Benzo(b)fluoranthene U 0.0896 1.00 Benzo(k)fluoranthene U 0.355 1.00 Benzo(g,h,i)perylene U 0.161 1.00 Benzo(a)pyrene U 0.340 1.00 Bis(2-chlorethoxy)methane U 0.329 10.0 Bis(2-chloroisopropyl)ether U 0.445 10.0 4-Bromophenyl-phenylether U 0.335 10.0 2-Chloronaphthalene U 0.330 1.00 4-Chlorophenyl-phenylether U 0.303 10.0 Chrysene U 0.332 1.00 Dibenz(a,h)anthracene U 0.279 1.00 3,3-Dichlorobenzidine U 2.02 10.0 2,4-Dinitrotoluene U 1.65 10.0 2,6-Dinitrotoluene U 0.279 10.0 Fluoranthene U 0.310 1.00 Fluorene U 0.323 1.00 Hexachlorobenzene U 0.341 1.00 Hexachloro-1,3-butadiene U 0.329 10.0 Hexachlorocyclopentadiene U 2.33 10.0 Hexachloroethane U 0.365 10.0 Indeno(1,2,3-cd)pyrene U 0.279 1.00 Isophorone U 0.272 10.0 Naphthalene U 0.372 1.00 Nitrobenzene U 0.367 10.0 n-Nitrosodiphenyla mine U 1.19 10.0 n-Nitrosodi-n-propylamine U 0.403 10.0 Phenanthrene U 0.366 1.00 Benzylbutyl phthalate U 0.275 3.00 Bis(2-ethylhexyl)phthalate U 0.709 3.00 Di-n-butyl phthalate U 0.266 3.00 Diethyl phthalate U 0.282 3.00 Dimethyl phthalate U 0.283 3.00 Di-n-octyl phthalate U 0.278 3.00 Pyrene U 0.330 1.00 Benzoic Acid U 4.40 10.0 4-Chloroaniline U 0.382 10.0 ACCOUNT: Geological Resources- NC Speedway PROJECT: SDG: DATE/TIME: PAGE: 5194 L1135637 09/24/19 09:49 26 of 39 FP1 FTC FSS [Cn] FSr 7G1 FAI FSC WG1340629 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1135637-02 Method Blank (MB) (MB) R3448360-2 09/07/1911:11 MB Result Analyte ug/I 4-ChIoro-3-methyl phenol U 2-Chorophenol U 2-Nitrophenol U 4-Nitrophenol U Pentachlorophenol U Phenol U 2,4,6-Trichlorophenol U Dibenzofuran U 2,4-Dichlorophenol U 2,4-Dimethylphenol U 4,6-Dinitro-2-methylphenol U 2,4-Dinitrophenol U 2-Methylnaphthalene U 2-Methylphenol U 3&4-Methyl Phenol U 1-Methylnaphthalene U (S) Nitrobenzene-d5 65.9 (S) 2-F/uorobipheny/ 75.4 (S) p-Terphenyl-d14 102 (S) Phenol-d5 19.3 (S) 2-Fluorophenol 32.8 (S)2,4,6-Tribromopheno/ 55.0 MB Qualifier MB MDL MB RDL ug/I ug/I Laboratory Control Sample (LCS) 0.263 10.0 0.283 10.0 0.320 10.0 2.01 10.0 0.313 10.0 0.334 10.0 0.297 10.0 0.380 10.0 0.284 10.0 0.624 10.0 2.66 10.0 3.25 50.0 0.311 1.00 3.12 10.0 0.266 10.0 0.332 1.00 15.0-314 22.0-127 29.0-141 8.00-424 10.0-120 10.0-153 (LCS) R3448360-1 09/07/1910:50 Spike Amount LCS Result LCS Rec. Analyte ug/I ug/I % Acenaphthene 50.0 43.8 87.6 Acenaphthylene 50.0 44.2 88.4 Anthracene 50.0 51.5 103 Benzo(a)anth race ne 50.0 53.3 107 Benzo(b)fluoranthene 50.0 54.1 108 Benzo(k)fluoranthene 50.0 52.7 105 Benzo(g,h,i)perylene 50.0 49.2 98.4 Benzo(a)pyrene 50.0 53.2 106 Bis(2-chlorethoxy)methane 50.0 38.2 76.4 Bis(2-chloroisopropyl)ether 50.0 39.9 79.8 4-Bromophenyl-phenylether 50.0 54.7 109 Rec. Limits LCS Qualifier 47.0-145 33.0-145 27.0-133 33.0-143 24.0-159 11.0-162 1.00-219 17.0-163 1.00-219 36.0-166 53.0-127 FP1 FTC FSS 4 Cn FSr 7G1 FAI FSC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 27 of 39 WG1340629 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1135637-02 Laboratory Control Sample (LCS) (LCS) R3448360-1 09/07/1910:50 Spike Amount Analyte ug/I 2-Chloronaphthalene 50.0 4-Chlorophenyl-phenylether 50.0 Chrysene 50.0 Dibenz(a,h)anthracene 50.0 3,3-Dichlorobenzidine 100 2,4-Dinitrotoluene 50.0 2,6-Dinitrotoluene 50.0 Fluoranthene 50.0 Fluorene 50.0 Hexachlorobenzene 50.0 Hexachloro-1,3-butadiene 50.0 Hexachlorocyclopentadiene 50.0 Hexachloroethane 50.0 Indeno(1,2,3-cd)pyrene 50.0 Isophorone 50.0 Naphthalene 50.0 Nitrobenzene 50.0 n-Nitrosodiphenyla mine 50.0 n-Nitrosodi-n-propylamine 50.0 Phenanthrene 50.0 Benzylbutyl phthalate 50.0 Bis(2-ethylhexyl)phthalate 50.0 Di-n-butyl phthalate 50.0 Diethyl phthalate 50.0 Dimethyl phthalate 50.0 Di-n-octyl phthalate 50.0 Pyrene 50.0 Benzoic Acid 100 4-Chloroaniline 50.0 4-Ch I oro-3-m ethyl phenol 50.0 2-Chlorophenol 50.0 Dibenzofuran 50.0 2,4-Dichlorophenol 50.0 2,4-Dimethylphenol 50.0 4,6-Di n itro-2-methyl phen of 50.0 2,4-Dinitrophenol 50.0 2-Methylnaphthalene 50.0 2-Methylphenol 50.0 3&4-Methyl Phenol 50.0 2-Nitrophenol 50.0 LCS Result ug/I 41.8 48.1 53.0 49.5 92.3 54.3 50.6 55.8 48.3 51.6 37.8 24.1 40.3 49.3 39.2 34.7 37.0 50.1 43.3 51.5 63.0 62.5 61.6 53.7 50.0 60.9 55.4 18.7 32.4 40.8 34.3 44.3 38.2 34.5 57.0 48.9 36.8 28.9 31.0 40.0 LCS Rec 83.6 96.2 106 99.0 92.3 109 101 112 96.6 103 75.6 48.2 80.6 98.6 78.4 69.4 74.0 100 86.6 103 126 125 123 107 100 122 18.7 64.8 81.6 68.6 88.6 76.4 69.0 114 97.8 73.6 57.8 62.0 80.0 Rec. Limits LCS Qualifier 60.0-120 25.0-158 17.0-168 1.00-227 1.00-262 39.0-139 50.0-158 26.0-137 59.0-121 1.00-152 24.0-120 10.0-120 40.0-120 1.00-171 21.0-196 21.0-133 35.0-180 44.0-120 1.00-230 54.0-120 1.00-152 8.00-158 1.00-120 1.00-120 1.00-120 4.00-146 52.0-120 10.0-120 23.0-120 22.0-147 23.0-134 42.0-120 39.0-135 32.0-120 1.00-181 1.00-191 35.0-120 26.0-120 27.0-120 29.0-182 J4 FP1 FTC FSS 4 Cn FSr 7G1 FAI FSC ACCOUNT: Geological Resources- NC Speedway PROJECT: SDG: DATE/TIME: PAGE: 5194 L1135637 09/24/19 09:49 28 of 39 WG1340629 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1135637-02 Laboratory Control Sample (LCS) (LCS) R3448360-1 09/07/1910:50 Spike Amount Analyte ug/I 4-Nitrophenol 50.0 Pentachlorophenol 50.0 Phenol 50.0 2,4,6-Trichlorophenol 50.0 1-Methyl naphthalene 50.0 (S) Nitrobenzene-d5 (S) 2-F/uorobiphenyl (S) p-Terphenyl-d14 (S) Phenol-d5 (S) 2-Fluorophenol (S) 2,4,6-Tribromophenol LCS Result ua/1 L3.1 35.5 16.2 45.6 38.3 LCS Rec. 46.2 71.0 32.4 91.2 76.6 63.8 80.9 109 22.9 37.7 91.5 Rec. Limits LCS Qualifier 1.00-132 14.0-176 5.00-120 37.0-144 33.0-120 15.0-314 22.0-127 29.0-141 8.00-424 10.0-120 10.0-153 L1136O17-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1136017-04 09/07/1914:44 • (MS) R3448360-3 09/07/1915:05 • (MSD) R3448360-4 09/07/1915:27 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte ug/I ug/I ug/I ug/I % % Acenaphthene 50.0 U 40.0 41.2 80.0 82.4 Acenaphthylene 50.0 U 40.7 41.8 81.4 83.6 Anthracene 50.0 U 48.1 47.8 96.2 95.6 Benzo(a)anth race ne 50.0 U 50.2 49.3 100 98.6 Benzo(b)fluoranthene 50.0 U 50.7 50.0 101 100 Benzo(k)fluoranthene 50.0 U 50.3 49.3 101 98.6 Benzo(g,h,i)perylene 50.0 U 44.3 44.0 88.6 88.0 Benzo(a)pyrene 50.0 U 49.6 47.2 99.2 94.4 Bis(2-chlorethoxy)methane 50.0 U 36.7 36.9 73.4 73.8 Bis(2-chloroisopropyl)ether 50.0 U 40.0 40.4 80.0 80.8 4-Bromophenyl-phenylether 50.0 U 51.1 51.2 102 102 2-Chloronaphthalene 50.0 U 40.1 40.2 80.2 80.4 4-Chlorophenyl-phenylether 50.0 U 44.3 45.2 88.6 90.4 Chrysene 50.0 U 50.6 48.9 101 97.8 Dibenz(a,h)anthracene 50.0 U 45.8 45.4 91.6 90.8 3,3-Dichlorobenzidine 100 U 71.0 61.3 71.0 61.3 2,4-Dinitrotoluene 50.0 U 50.8 51.9 102 104 2,6-Dinitrotoluene 50.0 U 46.7 47.8 93.4 95.6 Fluoranthene 50.0 U 51.5 51.0 103 102 Fluorene 50.0 U 44.0 44.3 88.0 88.6 Hexachlorobenzene 50.0 U 48.0 47.8 96.0 95.6 Hexachloro-1,3-butadiene 50.0 U 37.4 36.1 74.8 72.2 Dilution Rec. Limits 47.0-145 33.0-145 27.0-133 33.0-143 24.0-159 11.0-162 1.00-219 17.0-163 33.0-184 36.0-166 53.0-127 60.0-120 25.0-158 17.0-168 1.00-227 1.00-262 39.0-139 50.0-158 26.0-137 59.0-121 1.00-152 24.0-120 MS Qualifier MSD Qualifier RPD /.tlo 2.67 0.626 1.81 1.39 2.01 0.680 4.96 0.543 0.995 0.195 0.249 2.01 3.42 0.877 14.7 2.14 2.33 0.976 0.680 0.418 3.54 RPD Limits 48 74 66 53 71 63 97 72 54 76 43 24 61 87 126 108 42 48 66 38 55 62 FP1 FTc FSS [Cn] FSr 7G1 FAI [Sc ACCOUNT: PROJECT: Geological Resources- NC Speedway 5194 SDG: L1135637 DATE/TIME: 09/24/19 09:49 PAGE: 29 of 39 WG1340629 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 625.1 L1135637-02 ONE LAB. NATIONWIDE. L1136O17-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1136017-04 09/07/1914:44 • (MS) R3448360-3 09/07/1915:05 • (MSD) R3448360-4 09/07/1915:27 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte ug/I ug/I ug/I ug/I % % Hexachlorocyclopentadiene 50.0 U 21.3 21.8 42.6 43.6 Hexachloroethane 50.0 U 40.4 40.1 80.8 80.2 Indeno(1,2,3-cd)pyrene 50.0 U 45.3 44.5 90.6 89.0 Isophorone 50.0 U 38.1 38.6 76.2 77.2 Naphthalene 50.0 U 33.7 33.6 67.4 67.2 Nitrobenzene 50.0 U 36.5 36.3 73.0 72.6 n-Nitrosodiphenyla mine 50.0 U 47.1 46.5 94.2 93.0 n-Nitrosodi-n-propylamine 50.0 U 43.3 43.6 86.6 87.2 Phenanthrene 50.0 U 48.3 48.5 96.6 97.0 Benzylbutyl phthalate 50.0 U 62.4 61.9 125 124 Bis(2-ethylhexyl)phthalate 50.0 U 61.4 61.1 123 122 Di-n-butyl phthalate 50.0 0.364 58.8 58.8 117 117 Diethyl phthalate 50.0 U 50.0 50.8 100 102 Dimethyl phthalate 50.0 U 46.5 47.3 93.0 94.6 Di-n-octyl phthalate 50.0 U 62.7 60.6 125 121 Pyrene 50.0 U 53.3 53.0 107 106 Benzoic Acid 100 U 33.0 36.8 33.0 36.8 4-Chloroaniline 50.0 U 31.3 28.8 62.6 57.6 4-ChIoro-3-methyl phenol 50.0 U 38.7 38.9 77.4 77.8 2-Chlorophenol 50.0 U 33.2 31.5 66.4 63.0 Dibenzofuran 50.0 U 41.6 42.0 83.2 84.0 2,4-Dichlorophenol 50.0 U 36.6 36.7 73.2 73.4 2,4-Dimethylphenol 50.0 U 32.8 32.4 65.6 64.8 4,6-Dinitro-2-methylphenol 50.0 U 53.1 54.5 106 109 2,4-Dinitrophenol 50.0 U 47.4 49.6 94.8 99.2 2-Methylnaphthalene 50.0 U 35.7 35.9 71.4 71.8 2-Methylphenol 50.0 U 28.5 26.3 57.0 52.6 3&4-Methyl Phenol 50.0 U 30.5 28.4 61.0 56.8 2-Nitrophenol 50.0 U 40.0 40.7 80.0 81.4 4-Nitrophenol 50.0 U 20.5 21.0 41.0 42.0 Pentachlorophenol 50.0 U 44.3 44.9 88.6 89.8 Phenol 50.0 U 15.6 13.7 31.2 27.4 2,4,6-Trichlorophenol 50.0 U 44.0 44.6 88.0 89.2 1-Methyl naphthalene 50.0 U 36.5 37.4 73.0 74.8 (S) Nitrobenzene-d5 64.8 63.6 (S) 2-F/uorobipheny/ 75.8 77.6 (S) p-Terphenyl-d14 108 106 (S) Phenol-d5 23.2 20.8 (S) 2-F/uorophenol 35.9 32.0 (S) 2,4,6-Tribromopheno/ 96.0 100 ACCOUNT: PROJECT: Geological Resources- NC Speedway 5194 Dilution Rec. Limits MS Qualifier MSD Qualifier RPD 10.0-146 40.0-120 1.00-171 21.0-196 21.0-133 35.0-180 16.0-160 1.00-230 54.0-120 1.00-152 8.00-158 1.00-120 1.00-120 1.00-120 4.00-146 52.0-120 10.0-120 10.0-137 22.0-147 23.0-134 17.0-150 39.0-135 32.0-120 1.00-181 1.00-191 13.0-142 14.0-120 13.0-124 29.0-182 1.00-132 14.0-176 5.00-120 37.0-144 33.0-120 15.0-314 22.0-127 29.0-141 8.00-424 10.0-120 10.0-153 SDG: L1135637 2.32 0.745 1.78 1.30 0.297 0.549 1.28 0.690 0.413 0.805 0.490 0.000 1.59 1.71 3.41 0.564 10.9 8.32 0.515 5.26 0.957 0.273 1.23 2.60 4.54 0.559 8.03 7.13 1.73 2.41 1.35 13.0 1.35 2.44 DATE/TIME: 09/24/19 09:49 RPD Limits 34 52 99 93 65 62 28 87 39 60 82 47 100 183 69 49 40 33 73 61 27 50 58 203 132 29 29 26 55 131 86 64 58 23 PAGE: 30 of 39 FP1 FTc FSS [Cn] FSr �GI FAI FSC GLOSSARY OF TERMS ONE LAB. NATIONWIDE. Guide to Reading and Understanding Your Laboratory Report FP1 The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and if you have additional questions please contact your project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, FTC Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions FSS (dry) Results are reported based on the dry weight of the sample. [this will only be present on a dry report basis for soils]. MDL Method Detection Limit. [Cn] ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit. Fr RDL (dry) Reported Detection Limit. Rec. Recovery. RPD Relative Percent Difference. s QC SDG Sample Delivery Group. Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes E reported. If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the F laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry) Confidence level of 2 sigma. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section of the report includes the results of the laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the samples from the time of collection until delivery to the laboratory for analysis. This section of your report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description J The identification of the analyte is acceptable; the reported value is an estimate. J4 The associated batch QC was outside the established quality control range for accuracy. N The analyte is tentatively identified and the associated numerical value may not be consistent with the actual concentration present in the sample. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 31 of 39 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. Pace National is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our one location design is the design of our laboratory campus. The model is conducive to accelerated productivity, decreasing FP1 turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace National. Z Tc State Accreditations f—� Alabama 40660 Nebraska _ NE-OS-15-05 SS Alaska 17-026 Nevada TN-03-2002-34 Arizona AZO612 New Hampshire 2975 Arkansas 88-0469 New Jersey_NELAP TNO02 C n California 2932 New Mexico n/a Colorado TN00003 New York 11742 s Connecticut PH-0197 North Carolina Env375 Sr Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina' 41 Georgia' 923 North Dakota R-140 RC Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 G Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky76 90010 South Carolina 84004 Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee' 4 2006 Louisiana' LA180010 Texas T104704245-18-15 [SC Maine TN0002 Texas' LABO152 Maryland 324 Utah Massachusetts M-TNO03 Vermont Michigan 9958 Virginia Minnesota 047-999-395 Washington Mississippi TN00003 West Virginia Missouri 340 Wisconsin Montana CERT0086 Wyoming Third Party Federal Accreditations A21LA — ISO 17025 1461.01 AIHA-LAP,LLC EMLAP A21LA — ISO 17025 5 1461.02 DOD Canada 1461.01 USDA EPA—Crypto TN00003 ' Drinking Water 'Underground Storage Tanks 3 Aquatic Toxicity 4 Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable Our Locations TN00003 VT2006 460132 C847 233 9980939910 A2LA 100789 1461.01 P330-15-00234 Pace National has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. If you would like assistance from one of our support offices, please contact our main office. Pace National performs all testing at our central laboratory. WA MT NO OR MN T I❑ SD ITO WI NY WY MI NV T NE IA OH T PA T f IL Ills WY vA UT T CA�� T KS MO KY W 11110 � NM O� AR N Sc T MS A`7L GA T TX * LA T AK T T q FL wo HI ACCOUNT: PROJECT: SDG: DATE/TIME: Geological Resources- NC Speedway 5194 L1135637 09/24/19 09:49 ME PAGE: 32 of 39 ----- Geological Resources- NC Speedway 3502 Hayes Rd. Charlotte, NC 28110 Billing Information: Mr. Cares ara Prey Charles ChiChk PO Box 1510 Springfield, OH 45500 Analvfiis / ontain r / Pr"ervativa, Chain of Custody Page of_ �eMal uIYpofral' Ne1Mv�Gnlr rM T• lnrvrveM1m �nMou1LebanoJuliet,TN31132 ❑� '❑� Phone 615 758 5858 Fax 615758-5859 , Fax 615 ]58 5859 a v N a n _ Z Q O ay U 'i ry ID tu Cl. Z V U O N p of O rn Z _ a = E N 'u_ CO o r ro Z u E O O 0t.n > to u = _ a -6 E -CC Q w > to ac m u = Q E o ID > u = Q O > 0 o to > x a N O = Z o Z O x m W > Report to Ms. Nicole Long Email To nml@geologicalresourcesinc.com; jra@geologicalresourcesinc.com; Project i Description Speedway 7984 City/State I<4y 41aa� I L.. '� Collected: -1 (`„s(tN: Auk, Please Circle. PT MT CT ET SDG # S B1 % 7 Acctnum: GEORESSSA Template.T154741 Prelogin: P725452 11314-T. Alan Hamill Phone:704-845-4010 Fax: Client Project # 1 G1.j �1 1 1 ab Project It GEORESSSA-7984 Collected by (print): (Af u1 Site/Facility ID # --�qQ , W� P.D. N V_ E Q E O Q = C- > Collected by (signature): j(��,�,� ,1�I.� ��l w`Uy`I/� Immediately Packed on Ice N_ Y Rush? (Lab NiBe Notified) Quote# Same Day Five Day _ _Next Day _SOay (Rod Only) Date Results Needed _Two Day _ 10 Day (Rod Only( No, _ Three Day of shipped via: Fe EX Ground Sample ID Comp/Grab Matrix' Depth OWQ, ntr5 aemar4: sample a(lab °niyl °P (fit Ank C7rut1 Gw o 9-3-IL X SS 7.5 ` 5 X X ' GW Al / 14 X X X X X X • Matrix: SS -soil AIR -Air F- Filter GW- Groundwater B- Bioassay WW- WasteWaler DW- Drinking Water OT Other entafks; RM SCREM'45 ffMW PH Temp Flow Other sarnple Receipt Checklist CDC Seal Present/Intact: _NP tg�`_N COC Signed/Accurate: 1L' N Bottles arrive intact: CX. N Correct bottles used: x N Sufficient volume sent: vN y If Applicable VOAPre Zero Readspace:N Preservation Correct/Checked: _N PAD Screen <0.5 alN — Samples returned via: Trackingu _UPS _Fed Ex _Courier �,S �S�,a� �'J/\1 lli LL S W f Relinqui ed by : (Signature) /� ✓ Relinquish V: (Signature( Date: �3jly Date. Time: Received (� Time: Received by. (Signature! - 420t b (Signature) Trip Blank R d: Yes No g�rye ( j na eoH v TER Temp: Bottles Reled If preservation required by Login: Date/Time Relinquished by :(Signature) Date: Time: Receiv d orla by:(Sigatu Date:Time. l at/�C Hold ition: OK Page 1 of 2 Chain -of -Custody -Record COC ID # 00051770 9 [TURN AROUND TIME TANDARD Speedway Project Information Speedway Store #: C210007984 Address: 2401 S Cannon Blvd City: Kannapolis Phone #: Speedway Proj. Mgr: Charles Chiara AFE #: 190192 Facility ID 0000031744 State: NC Fax #: **INVOICE TO SPEEDWAY** Work Order #: 1103786264 Lab Information Lab: Pace Analytical Services (TN) Consultant: Geological Resources, Inc. - Monroe, NC Project Mgr: Nicole Long Address: 3502 Hayes Road, Monroe, NC 28110 Phone #: Fax #: Sampler: Corey Buchanan Shipped: FedExp Tracking #: 12035774366 Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks MW-1 09/03/2019 03:57pm W 5 1 LG HCL U&A MADEP EPH TC #342 MADEP El VOA HCL BTEX by 6200B NC task code 2 6200B VOA HCL TAEE-Oxygenate 6200B VOA HCL U&A MADEP VPH TC #341 MADEP VI 1 LAG COOL 625 10 TICS NC Task Code 301 625 250 ML HNO3 Lead 6010 6010 VOA HCL 4 Oxygenates + Ethanol TC 240 6200B VOA HCL TBF-Oxygenate- TC #240 6200B MW-1 (2.5') 09/03/2019 12:11 pm S 3 VOA MEOH/NAHS BTEX Only 8260D 4 OZ COOL Total Solids 2540 G 8 OZ JAR COOL TPH-DRO 8015 4 OZ MEOH TPH-GRO 8015 Relinquished by: Date Time Received by: Date Time Relinquished by: Date Time Received by laboratory: Date Time Special Reporting Requirements: Lab Notes: Temp Speedway LLC. 112 https://www.speedway-ids.com Page 2 of 2 Chain -of -Custody -Record COC ID # 00051770 9 [TURN AROUND TIME TANDARD Speedway Project Information Speedway Store #: C210007984 Address: 2401 S Cannon Blvd City: Kannapolis Phone #: Speedway Proj. Mgr: Charles Chiara AFE #: 190192 Facility ID 0000031744 State: NC Fax #: **INVOICE TO SPEEDWAY** Work Order #: 1103786264 Lab Information Lab: Pace Analytical Services (TN) Consultant: Geological Resources, Inc. - Monroe, NC Project Mgr: Nicole Long Address: 3502 Hayes Road, Monroe, NC 28110 Phone #: Fax #: Sampler: Corey Buchanan Shipped: FedExp Tracking #: 12035774366 Sample ID Date/Time Sampled Matrix Count Container Type Preservative Analysis to be Performed Method Remarks Relinquished by: Date Time Received by: Date Time Relinquished by: Date Time Received by laboratory: Date Time Special Reporting Requirements: Lab Notes: Temp Speedway LLC. 212 https://www.speedway-ids.com Chain of Custody Analysis to be Performed COC ID # 51770 Analysis Name: 4 Oxygenates + Ethanol TC 240 ( Water ) Analysis Description / Method: 4 Oxygenates + Ethanol TC 240 / 6200B Container Type / Preservative: VOA / HCL Analytes: Ethanol ug/L, Ethyl tert-butyl ether ug/L, t-Butyl alcohol ug/L, tert-Amyl alcohol ug/L, tert-Amyl methyl ether ug/L Analysis Name: 625 10 TICS NC Task Code 301 ( Water ) Analysis Description / Method: 625 10 TICS / 625 Container Type / Preservative: 1 LAG / COOL Chain -of -Custody -Record Printed: 11 /09/2019 Analytes: 1-Methyl naphthalene ug/L, 2,4,6-Trichlorophenol ug/L, 2,4-Dichlorophenol ug/L, 2,4-Di methyl phenol ug/L, 2,4-Dinitrophenol ug/L, 2,4-Dinitrotoluene ug/L, 2,6-Dinitrotoluene ug/L, 2-Chloronaphthalene ug/L, 2-Chlorophenol ug/L, 2-Methylnaphthalene ug/L, 2-Methylphenol ug/L, 2-Nitrophenol ug/L, 3,3'-Dichlorobenzidine ug/L, 3- & 4-Methylphenol ug/L, 4,6-Dinitro-o-cresol ug/L, 4-Bromophenyl phenyl ether ug/L, 4-Chloro-3-methylphenol ug/L, 4-Chloroaniline ug/L, 4-Chlorophenyl phenyl ether ug/L, 4-Nitrophenol ug/L, Acenaphthene ug/L, Acenaphthylene ug/L, Anthracene ug/L, Benzo(a)anthracene ug/L, Benzo(a)pyrene ug/L, Benzo(b)fluoranthene ug/L, Benzo(g,h,l)perylene ug/L, Benzo(k)fuoranthene ug/L, Benzoic acid ug/L, Bis(2-chloroethoxy)methane ug/L, Bis(2-ch loroisopropyl )ether ug/L, Bis(2-ethylhexyl)phthalate ug/L, Butyl benzyl phthalate ug/L, Chrysene ug/L, Di-n-butyl phthalate ug/L, Di-n-octyl phthalate ug/L, Dibenzo(a,h)anthracene ug/L, Dibenzofuran ug/L, Diethyl phthalate ug/L, Dimethyl phthalate ug/L, Fluoranthene ug/L, Fluorene ug/L, Hexachlorobenzene ug/L, Hexachlorobutadiene ug/L, Hexachlorocyclopentadiene ug/L, Hexachloroethane ug/L, Indeno(1,2,3-cd)pyrene ug/L, Isophorone ug/L, N-Nitroso-di-n-propylamine ug/L, N-Nitrosodiphenylamine ug/L, Naphthalene ug/L, Nitrobenzene ug/L, Pentachlorophenol ug/L, Phenanthrene ug/L, Phenol ug/L, Pyrene ug/L Analysis Name: BTEX Only (Soil) Analysis Description / Method: BTEX Only / 8260D Container Type / Preservative: VOA / MEOH/NAHSO4 Analytes: Benzene mg/Kg, Ethylbenzene mg/Kg, Toluene mg/Kg, Total Xylenes mg/Kg Analysis Name: BTEX by 6200B NC task code 272 ( Water ) Speedway LLC. 114 https:Ilwww.speedway-ids.com Chain of Custody Analysis to be Performed COC ID # 51770 Analysis Description / Method: 6200B / 6200B Container Type / Preservative: VOA / HCL Chain -of -Custody -Record Printed: 11 /09/2019 Analytes: 1,1,1,2-Tetrachloroethane ug/L, 1,1,1-Trichloroethane ug/L, 1,1,2,2-Tetrachloroethane ug/L, 1,1,2-Trichloroethane ug/L, 1,1-Dichloroethane ug/L, 1,1-Dichloroethylene ug/L, 1,1-Dichloropropene ug/L, 1,2,3-Trichlorobenzene ug/L, 1,2,3-Trichloropropane ug/L, 1,2,3-Trimethylbenzene ug/L, 1,2,4-Trichlorobenzene ug/L, 1,2,4-Trimethylbenzene ug/L, 1,2-Dibromo-3-chloropropane ug/L, 1,2-Dibromoethane ug/L, 1,2-Dichlorobenzene ug/L, 1,2-Dichloroethane ug/L, 1,2-Dichloropropane ug/L, 1,3,5-Trimethyl benzene ug/L, 1,3-Dichlorobenzene ug/L, 1,3-Dichloropropane ug/L, 1,4-Dichlorobenzene ug/L, 2,2-Dichloropropane ug/L, Benzene ug/L, Bromobenzene ug/L, Bromochloromethane ug/L, Bromodichloromethane ug/L, Bromoform ug/L, Carbon tetrachloride ug/L, Chlorobenzene ug/L, Chloroethane ug/L, Chloroform ug/L, Dibromochloromethane ug/L, Dichlorodifluoromethane ug/L, Diisopropyl ether ug/L, Ethylbenzene ug/L, Hexachlorobutadiene ug/L, Isopropyl benzene ug/L, Methyl bromide ug/L, Methyl chloride ug/L, Methyl tert butyl ether ug/L, Methylene bromide ug/L, Methylene chloride ug/L, Naphthalene ug/L, Styrene ug/L, Tetrachloroethyllene ug/L, Toluene ug/L, Trichloroethylene ug/L, Trichlorofluoromethane ug/L, Vinyl chloride ug/L, Xylene ug/L, cis-1,2-Dichloroethylene ug/L, cis-1,3-Dichloropropene ug/L, n-Butylbenzene ug/L, n-Propylbenzene ug/L, o-Chlorotoluene ug/L, p-Isopropyltoluene ug/L, p-chlorotoluene ug/L, sec -Butyl benzene ug/L, tert-Butylbenzene ug/L, trans-1,2-Dichloroethylene ug/L, trans- 1,3-Dichloropropene ug/L Analysis Name: Lead 6010 ( Water ) Analysis Description / Method: Lead 6010 / 6010 Container Type / Preservative: 250 ML / HNO3 Analytes: Lead ug/L Analysis Name: TAEE-Oxygenate ( Water ) Analysis Description / Method: TAEE-Oxygenate / 6200B Container Type / Preservative: VOA / HCL Analytes: TERT-AMYL ETHYL ETHER ug/L Analysis Name: TBF-Oxygenate- TC #240 ( Water ) Analysis Description / Method: TBF-Oxygenate- TC #240 / 6200B Speedway LLC. 214 https:Ilwww.speedway-ids.com Chain of Custody Analysis to be Performed COC ID # 51770 Container Type / Preservative: VOA / HCL Analytes: tert-Butyl formate ug/L Chain -of -Custody -Record Printed: 11 /09/2019 Analysis Name: TPH-DRO ( Soil ) Analysis Description / Method: DRO 3550/8015B NC TC#360 / 8015 Container Type / Preservative: 8 OZ JAR / COOL Analytes: Diesel Range Organics mg/Kg Analysis Name: TPH-GRO (Soil) Analysis Description / Method: GRO 5030/8015B NC TC#350 / 8015 Container Type / Preservative: 4 OZ / MEOH Analytes: Gasoline Range Organics mg/Kg Analysis Name: Total Solids ( Soil ) Analysis Description / Method: Total Solids / 2540 G Container Type / Preservative: 4 OZ / COOL Analytes: Solids,Total % Analysis Name: U&A MADEP EPH TC #342 ( Water ) Analysis Description / Method: U&A MADEP EPH TC #342 / MADEP EPH Container Type / Preservative: 1 LG / HCL Analytes: Adjusted Total Petroleum hydrocarbon ug/L, C11-C22 Aromatics ug/L, C11-C22 aromatics (unadjusted) ug/L, Unadjusted C19-C36 Aliphatics ug/L, Unadjusted C9-C18 Aliphatics ug/L, Unadjusted Total Petroleum hydrocarbon ug/L Analysis Name: U&A MADEP VPH TC #341 ( Water ) Speedway LLC. 314 https:Ilwww.speedway-ids.com Chain of Custody Analysis to be Performed COC ID # 51770 Analysis Description / Method: U&A MADEP VPH TC #341 / MADEP VPH Container Type / Preservative: VOA / HCL Chain -of -Custody -Record Printed: 11 /09/2019 Analytes: C5-C8 Aliphatics ug/L, C5-C8 aliphatics (unadjusted) ug/L, C9-C10 aromatics (unadjusted) ug/L, C9-C12 Aliphatics ug/L, C9-C12 aliphatics (unadjusted) ug/L, Total Purgeable Hydrocarbons ug/L, Total VPH ug/L Speedway LLC. 414 https:Ilwww.speedway-ids.com