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HomeMy WebLinkAbout4101_Guilford_CityofHighPoint_Riverdale_MSLWF_GW_FID1377052_20191114Environmental CQmpkance and Remediatron Babb & Associates, PA. November 14, 2019 Mr. Joe Ghiold, Project Manager Ms. Jackie Drummond, Hydrogeologist NC Division of Waste Management 1646 Mail Service Center Raleigh, North Carolina 27699-1646 Re: 2019 Annual Water Quality Monitoring Report Former Seaboard Chemical/Riverdale Drive Landfill Site Jamestown, North Carolina EPA ID No. NCD 071 574 164 NC DEQ Landfill Permit No. 41-04 Dear Joe and Jackie: Please find attached the 2019 Annual Water Quality Monitoring Report for the former Seaboard Chemical/Riverdale Drive Landfill Site in Jamestown, North Carolina. If there are any questions or comments regarding this report, please contact the undersigned at (919) 605-4719. Respectfully, Babb & Associates, P.A. �4C• �ct CrP Gary D. Babb, P.G. President Enclosure Cc: Mr. Robby Stone Mr. Terry Houk Mr. Ed Gunderson Mr. Craig Coslette • 0H 111111 to,"""' ,,.•� vk C A fq o,.,,, rz: SEALS i 488 q. ••.......-....... ,��•,f 111,11111���tN L FiF�15E QhjY❑Paper Report ❑Electronic Data - Email CD (data loaded: Yes / No Doc/Event #: NC DENR I IEnvironmental Monitoring Division of Waste Management - Solid Waste Reporting Form Notice: This form and any information attached to it are 'Public Records" as defined in NC General Statute 132-1. As such, these documents are available for inspection and examination by any person upon request (NC General Statute 132-6). Instructions: Prepare one form for each individually monitored unit. Please type or print legibly. Attach a notification table with values that attain or exceed NC 2L groundwater standards or NC 2B surface water standards. The notification must include a preliminary analysis of the cause and significance of each value. (e.g. naturally occurring, off -site source, pre-existing condition, etc.). Attach a notification table of any groundwater or surface water values that equal or exceed the reporting limits. Attach a notification table of any methane gas values that attain or exceed explosive gas levels. This includes any structures on or nearby the facility (NCAC 13B .1629 (4)(a)(i). Send the original signed and sealed form, any tables, and Electronic Data Deliverable to: Compliance Unit, NCDENR-DWM, Solid Waste Section, 1646 Mail Service Center, Raleigh, NC 27699-1646. $SId rite Moth%#rit�i 'Rath„(bin�tn#vrrnatio i. ; Name of entity submitting data (laboratory, consultant, facility owner): Babb & Associates, P.A. Contact for questions about data formatting. Include data preparer's name, telephone number and E-mail address: Name: Gary D. Babb Phone: (919) 605-4719 E-mail: gdbabb@gmail.com NC Landfill Rule: Actual sampling dates (e.g., Facility name: Facility Address: Facility Permit # (.0500 or .1600) October 20-24, 2006) Closed Riverdale Drive Landfill SR 1145 41-04 .0500 Sept. 11 - 19, 2019 High Point, NC Environmental Status: (Check all that apply) Initial/Background Monitoring Detection Monitoring Assessment Monitoring of data submitted: (Check all that apply) Groundwater monitoring data from monitoring wells Methane gas monitoring data Groundwater monitoring data from private water supply wells X Corrective action data (specify) Leachate monitoring data ❑ Surface water monitoring data Other(specify) 0 Corrective Action Annual Water Quality Monitoring Notification attached? No. No groundwater or surface water standards were exceeded. X Yes, a notification of values exceeding a groundwater or surface water standard is attached. It includes a list of groundwater and surface water monitoring points, dates, analytical values, NC 2L groundwater standard, NC 2B surface water standard or NC Solid Waste GWPS and preliminary analysis of the cause and significance of any concentration. Yes, a notification of values exceeding an explosive methane gas limit is attached. It includes the methane monitoring points, dates, sample values and explosive methane gas limits. Ceitifica`#I�ot� , :� E To the best of my knowledge, the information reported and statements made on this data submittal and attachments are true and correct. Furthermore, I have attached complete notification of any sampling values meeting or exceeding groundwater standards or explosive gas levels, and a preliminary analysis of the cause and significance of concentrations exceeding groundwater standards. I am aware that there are significant penalties for making any false statement, representation, or certification including the possibility of a fine and imprisonment. Gary D. Babb Licensed Geologist (919) 605-4719 FacilityRe r ntative Na (Prin Title (Area Code) Telephone Number October 10, 2019 Affix NC Licensed/ Professional Geologist Seal Signaturq / Date Babb & Associates, P.A., 5506 Bradford Pear Ct., Raleigh, NC 27606-1379 Facility Representative Address NC PE Firm License Number (if applicable effective May 1, 2009) Revised 6/2009 #,M,� ��i N.............. `' �0Q-'\GENSF✓�'�. V :2- JL t47 488 ..OLQ ` ,.. YD•g % ��,iau i 1."W,% Water Quality Monitoring Report Former Seaboard Chemical/Riverdale Drive Landfill 5899 Riverdale Drive Jamestown, North Carolina Permit No. 41-01 NCD 071 574 164 Prepared for: Seaboard Group II and City of High Point High Point, NC Prepared by: Babb & Associates, P.A. 5506 Bradford Pear Court Raleigh, North Carolina 27606 Gary D. Babb, Licensed Geologist September 2019 .:'�C A ••. H_..........R p''•• zt SEAL 488 ...... O 0 Babb & Associates, P.A. Table of Contents 1.0 Introduction 1.1 Site Information 1.2 Site Geology 1.3 Site Hydrogeology 2.0 Water Quality Monitoring Program 2.1 Groundwater Monitoring Network 2.2 Surface Water Monitoring Network 3.0 Water Quality Sample Collection 3.1 Field Sample Procedures 3.2 Field Quality Assurance 3.3 Sample Delivery/Chain-of-Custody 4.0 Laboratory Analysis 5.0 Hydrogeological Conditions 6.0 Laboratory Analytical Results 6.1 Groundwater Analytical Results 6.2 Surface Water Analytical Results 6.3 Quality Control Samples 7.0 Conclusions Figure 1 Site Location Map Figure 2 Groundwater Potentiometric Map Figure 3 1,2-Dichloroethane Isoconcentration Map Figure 4 Vinyl Chloride Isoconcentration Map Figure 5 Chlorobenzene Isoconcentration Map Figure 6 1,4-Dioxane Isoconcentration Map Figure 7 Total Volatile Organic Compound Isoconcentration Map Table 1 Monitoring Well Construction/Groundwater Elevations Table 2 Groundwater VOC Concentrations Table 3 Surface Water VOC Concentrations Table 4 Field Parameters Table 5 Monitoring Well Lat/Long and Elevations Appendix A ENCO Laboratory Analytical Report 1 6 8 10 11 12 17 1.0 Introduction 1.1 Site Information The former Seaboard Chemical/Riverdale Drive Landfill Site (the Site) is located approximately five miles east-southeast of High Point, NC near the intersection of Riverdale Drive and Interstate 85 (Figure 1). The Site consists of two properties, the facility where the former Seaboard Chemical Corporation (Seaboard) conducted operations and the closed municipal Riverdale Drive Landfill (Landfill), as shown on Figure 2. The former Seaboard Facility is located at 5899 Riverdale Drive, Jamestown, NC and consists of approximately 13 acres. Between 1974 and 1989, Seaboard operated solvent recovery and fuel blending processes at the facility. The corporation declared bankruptcy in 1989 and was not able to fund the cost of performing the necessary site closure and remediation. Removal activities were conducted during 1990 and 1992 to remove all remaining waste materials and certain tanks and equipment from the former Seaboard Facility. The removal was conducted by Seaboard Group I which was formed by parties that may have used the services of Seaboard in the past. The adjacent Landfill, a closed unlined municipal solid waste facility, consists of approximately 150 acres and bounds the former Seaboard Facility on two sides. The Landfill was operated from the 1950's until October 1993. The Landfill was permitted by the North Carolina DEQ Solid Waste Section in 1979. During Landfill operations, sections of the two tributary streams that cross the landfill property were piped and solid waste was used to fill the drainage valleys. The two streams are referred to as the Southern Intermittent Stream and the Northern Intermittent Stream. During filling of the Southern Intermittent Stream valley, a leachate collection system was installed adjacent to the stream channel to collect leachate migrating from the overlying solid waste. In Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report September 2019 Page 1 1989, a leachate collection system was added to control surface seeps (leachate leaks) along the slopes of the Landfill. From approximately 1966 to 1970, Landfill operations also included the disposal and open burning of spent solvents in shallow pits located just north of the former Landfill scale house (Figure 2). Periodically, these burn pits were cleaned of residue that accumulated in a mound to the south of the burn pits. Presently, this mound consists of approximately 600 cubic yards of contaminated residue capped by a synthetic liner and is referred to as the "soil residue mound". The Landfill is now capped and maintained under an approved post -closure plan. Seaboard Group II was formed in 1994 and entered into an agreement with the City of High Point (the City) to jointly perform a remedial investigation and prepare a baseline risk assessment and feasibility study for the Site, including both the former Seaboard Facility and closed Landfill properties. The Seaboard Group II and the City then entered into an Administrative Order on Consent (AOC) dated January 30, 1996 with NC DEQ to perform the remedial investigation. The feasibility study was conducted under a separate AOC dated July 22, 1997. Remedial investigations conducted at the Site have documented the presence of chlorinated and non -chlorinated volatile organic compounds (VOCs) in soils, leachate, groundwater, and surface water. The results from the remedial investigation indicate that the VOC-affected groundwater had migrated toward Randleman Lake, which adjoins the Site along the northern and eastern property boundary of the Landfill. The Randleman Lake was created by the impoundment of the Deep River in 2006 by the Randleman Lake Dam, which is located approximately 11.5 miles downstream of the Site. The Remedial Recommendation Document (February 2005) presented a remedial strategy for the impacted media at the Site based on the results of the remedial investigation, baseline risk assessment, and feasibility study. The remedial design consisted of groundwater extraction and treatment in combination with institutional controls including site access control, recorded land use restrictions, and restriction of water Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report September 2019 Page 2 supply well construction. The groundwater and surface water monitoring program is designed to evaluate the effectiveness of the remedy. The Remedial Recommendation Document was conditionally approved by the NC DEQ in September 2005. Seaboard Group II and the City entered into a Remedial Action Settlement Agreement (RASA) with NC DEQ on December 29, 2008. The RASA provides for the design and implementation of the approved remedial action program for the Site as well as completion and reporting of annual groundwater and surface water monitoring activities. 1.2 Site Geology The Site is located in the central Piedmont Physiographic Province in the northern portion of the Carolina Slate Belt. Granite is the predominant rock type in the area and outcrops are observed along the creeks and within the Site. The geology of the Site consists of fractured granitic gneiss which has been intruded by mafic dikes. The mafic dikes are generally oriented N20°E and are sub -vertical, dipping to both the northwest and the southeast. The mafic dikes generally do not occur as single massive tabular bodies but normally occur as a swarm of thinner tabular and/or irregular dikes within larger fracture zones within the granitic gneiss. The thickness of individual mafic dikes ranges from less than one foot to more than 30 feet. Smaller mafic dikes that are not associated with fracture zones are disseminated throughout the granitic gneiss. Several prominent geologic structures have been identified and mapped at the Site, including these significant geologic features: Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report September 2019 Page 3 Southern Intermittent Stream Fault — N80°E oriented fracture zone/fault that parallels the Southern Intermittent Stream. Based on an on -site outcrop measurement and fracture orientation data from the PW-31) core, the fracture zone is believed to dip 43' to the south; Seaboard Dike — N20°E oriented mafic dike that extends from the Seaboard Facility to the vicinity of monitoring well PW-13I and north of the Deep River; PW-5D Dike/Fault — N200E oriented diabase dike/fault that extends northward from the east side of the Seaboard Facility near PW-8S to the vicinity of monitoring well PW-5D north of the Deep River. The PW-51) Fault has an inferred connection with the Southern Intermittent Stream Fault beneath the Landfill; Regional Fault/Dike — major regional fault/mafic dike that extends N20°E near PW-6I/6D and extends north of the Deep River; and Deep River Fault — southward -dipping fault that forms the east -west segment of the Deep River. Based on an on -site outcrop measurement and fracture orientation data from the PW-5D core, the fracture zone is believed to dip 50' to the south. 1.3 Site Hydrogeology The Site hydrogeology is characteristic of the regional piedmont aquifer system and consists of three aquifer units: the saprolite and partially weathered rock (PWR) aquifer, shallow bedrock aquifer, and deep bedrock aquifer. The saprolite/PWR aquifer is the uppermost aquifer across much of the Site, but is locally absent where the water table occurs below the top of bedrock. The thickness of the saprolite/PWR aquifer, where present, is generally less than 20 feet but extends to depths of 90 feet in limited areas Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report September 2019 Page 4 (PW-13I). The shallow bedrock aquifer extends from the top of competent bedrock to a depth where groundwater flow becomes limited due to the lack of open fractures. The base of the shallow bedrock zone at the Site is variable but generally believed to occur at depths of 200 to 400 feet. The deep bedrock aquifer extends downward from the base of the shallow bedrock aquifer and is characterized by low permeability and limited groundwater flow. The primary zone of groundwater movement at the Site is considered to occur within the saprolite/PWR and shallow bedrock aquifer zones. The saprolite/PWR and shallow bedrock aquifers are hydraulically connected. The potentiometric surface of shallow groundwater in the saprolite/PWR aquifer is generally a subdued replica of the original topography of the Site. The saprolite/PWR aquifer is locally absent where the water table occurs below the top of bedrock (generally beneath the topographic highs). Groundwater flow within the shallow bedrock aquifer is primarily through fractures in the bedrock and is strongly controlled by subsurface geologic structures such as faults, fracture zones, and mafic dikes. Based on the results of two constant rate discharge tests conducted in August and September 1997, the calculated bulk hydraulic conductivity values at the Site range from 0.5 to 3 feet/day (ft/d) in the saprolite/PWR aquifer zone and 0.1 to 0.6 ft/d in the shallow bedrock aquifer zone. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report September 2019 Page 5 2.0 Water Quality Monitoring Program The water quality monitoring network at the Site is evaluated on an annual basis. The locations of the groundwater and surface water samples collected during the annual monitoring event are shown on the attached Figure 2. The primary objectives of the annual groundwater and surface water monitoring program are: • Monitor VOC concentrations and migration of the VOC-affected groundwater; • Monitor groundwater elevations, hydraulic gradients and flow directions; • Monitor surface water quality in Randleman Lake, Northern Intermittent Stream, and Southern Intermittent Stream to assess impacts from groundwater discharge. The 2019 annual groundwater and surface water monitoring activities were conducted at the Site during the period of September 11 — 19, 2019. Groundwater level gauging was conducted at the monitoring wells to be sampled to evaluate groundwater flow patterns at the Site (Figure 2). Surface water sampling was conducted at nine surface water stations which included; four stations along Randleman Lake (SW-6, SW-7, SW-DRP-2, and SW-DRP-11), three stations on the Southern Intermittent Stream (SW-3, SW-4, and SW-5), and two monitoring stations on the Northern Intermittent Stream (SW-1 and SW-2). 2.1 Groundwater Monitoring Network The existing groundwater monitoring network consists of 25 monitoring wells which have been selected to evaluate the lateral and vertical extent of the contaminant plume as well as the effectiveness of the groundwater extraction system. The 25 monitoring wells sampled for subsequent laboratory analysis include: Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report September 2019 Page 6 MW-1 (background) MW-3C MW-6 MW-10 MW-1 2A MW-12B MW-12D MW-15A OW-DR2 OW-LFS2 PW-31) PW-4I PW-5D PW-6I PW-61) PW-10I PW-1 OD PW-12I PW-13I PW-14D PW-15D PW-16D PW-18 PW-SF1 W-4A Monitoring well construction information and groundwater elevations for the monitoring wells at the Site are provided on Table 1. 2.2 Surface Water Monitoring Network The current surface water monitoring network consists of nine monitoring stations as shown on Figure 2. The surface water monitoring stations are located along the Northern Intermittent Stream, Southern Intermittent Stream, and on Randleman Lake. The nine surface water stations sampled for the water quality monitoring program include: SW-1 SW-3 SW-5 SW-7 SW-DRP-11 SW-2 SW-4 SW-6 SW-DRP-2 * The surface water samples collected from the Randleman Lake are collected at two discrete depths, 1' below the surface and l' above the bottom of the lake. Seaboard Chemical/Riverdale Drive Landfill September 2019 Water Quality Monitoring Report Page 7 3.0 Water Quality Sample Collection Samples of groundwater and surface water were collected in accordance with the approved Annual Monitoring Plan — 2010 dated March 17, 2010. A brief description of the sample collection procedure is provided below. The 2019 annual groundwater and surface water monitoring activities were conducted at the Site during the period of September 11 — 19, 2019. 3.1 Field Sample Procedures Prior to groundwater sampling, water levels were obtained from each well using an electric water level meter capable of measuring the depth to water to the nearest 0.01 feet. This information was later used to determine the elevation of the water table in each monitoring well relative to surveyed datum (Table 1). The depth to water in each well was also used to determine the volume of standing water in the well casing. This information allowed for the purging of a minimum of three casing volumes from each well prior to sample collection to assure a fresh groundwater sample was collected. New nitrile gloves were worn by sampling personnel and each well was purged and sampled with a decontaminated submersible pump or a new disposable bailer. After purging of the monitoring wells, samples were collected in the following order: • VOCs and 1,4-dioxane • Field parameters (pH, conductivity, and temperature) The samples were collected directly in the laboratory -supplied containers which had been pre -filled with the appropriate preservative. No filtering of the samples was performed either in the field or laboratory. After collection, the samples were placed in a cooler on ice for overnight shipment to the analytical laboratory. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report September 2019 Page 8 Surface water samples were collected directly into the laboratory -supplied containers as grab samples. Sampling personnel wore new disposable nitrile gloves for each surface water sample collected. The surface water samples collected from the four stations along the Randleman Lake were collected at two discrete intervals: a shallow sample collected one foot below the surface, and a deeper sample collected one foot above the bottom of the Lake. The Randleman Lake water samples were collected using a stainless steel discrete -interval Kemmerer water sampler. The actual depths of the shallow and deeper Randleman Lake surface water samples are provided in Table 4. As with the groundwater samples, these samples were stored in a cooler on ice prior to overnight delivery to the analytical laboratory. 3.2 Field Quality Assurance Two trip blank samples were prepared by the analytical laboratory and accompanied the sample shipments until receipt by the laboratory. The trip blank samples were analyzed for VOCs. Temperature blanks were also provided with the sample shipments to assure the proper temperature was maintained until delivery to the analytical laboratory. 3.3 Sample Delivery/Chain of Custody All groundwater and surface water samples were stored in coolers on ice immediately after collection. Individual sample containers for each monitoring well or surface water sample were placed in zip lock plastic bags to reduce the potential for cross contamination between sample locations. Chain -of -Custody control documents were prepared and shipped with each cooler. Custody seals were also used for each cooler to maintain sample integrity until delivery to the analytical laboratory. The sample coolers were shipped via Federal Express for next morning delivery to the analytical laboratory. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report September 2019 Page 9 4.0 Laboratory Analysis The groundwater and surface water samples were analyzed for VOCs by EPA Method 8260D and 1,4-dioxane by EPA Method 8260C SIM. The laboratory performing the water quality analysis is Environmental Conservation Laboratories, Inc. (ENCO) of Cary, North Carolina, which is a NC Certified Laboratory. Internal quality control samples, including matrix spikes/matrix spike duplicates, were performed by ENCO for each set of samples. The ENCO laboratory reports, including internal quality control samples, are provided with this report in Appendix A. Field parameters (pH, specific conductivity, and temperature) were also measured by the sampling personnel for each groundwater and surface water sample using calibrated meters. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report September 2019 Page 10 5.0 Hydrogeological Conditions The depth to groundwater was measured in the 25 compliance monitoring wells during the September 2019 monitoring event. The groundwater elevations were calculated relative to the surveyed measuring point (top of casing) for each monitoring well. A groundwater potentiometric map is provided as Figure 2. This potentiometric map primarily represents groundwater flow in the bedrock aquifer. The groundwater depths and elevation data for the Site are summarized in Table 1. In the bedrock aquifer, the general groundwater flow direction across the Site is northeastward toward Randleman Lake. The vertical hydraulic gradient in the shallow bedrock aquifer, as measured between monitoring wells MW-3C and OW-DR2 during the September 2019 monitoring event, was 0.007 feet/feet upward. An Extraction Rate/Capture Zone Test was conducted by ERM NC, PC in August 2002. This test used well PW-DR1 as the primary extraction point to determine the potential capture zone using various pumping rates. The results of this test indicated pumping at a relatively low rate of 10 - 20 gallons per minute from PW-DR1 effectively contains the contaminant plume. A pumping rate of 13 — 14 gallons per minute from PW-DR1 during operation of the system has demonstrated a drawdown of approximately 24 feet which creates an effective capture zone. The filling of Randleman Lake began in 2006 and the lake level reached normal pool elevation (682 feet msl) in 2008. Consistent with prior gauging events, and confirmed with the data collected during the September 2019 monitoring event, groundwater levels at monitoring wells located adjacent to the lake have risen 10 - 12 feet as compared to pre -lake water level conditions. Inland from the lake, groundwater levels at wells located on the western portion of the Site have risen approximately 4 feet due to the lake impoundment. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report September 2019 Page 11 6.0 Laboratory Analytical Results The complete analytical results for the samples collected during the period of September 11 — 19, 2019 were received from the laboratory on October 7, 2019. A summary of the analytical results are provided for groundwater (Table 2), surface water (Table 3), and field parameters (Table 4). 6.1 Groundwater Analytical Results The analytical results for selected groundwater contaminants collected during the September 2019 monitoring event are shown in a series of figures. Groundwater quality maps representing the bedrock aquifer are provided for 1,2-dichloroethane (Figure 3), vinyl chloride (Figure 4), chlorobenzene (Figure 5), 1,4-dioxane (Figure 6), and total VOCs (Figure 7). The historical groundwater analytical results for specific VOCs, including the 2019 data, are summarized in Table 2 and the ENCO laboratory reports are provided in Appendix A. Measurements of pH, temperature, and specific conductance as determined in the field during sample collection are provided in Table 4. Additional monitoring well information including the latitude/longitude of each well location is provided in Table 5. The main mass of VOC impacted groundwater generally extends northeastward across the Site to the Randleman Lake basin. As shown on Figure 7, the most elevated levels of VOCs are present in the vicinity of the northeast corner of the Seaboard Facility near the location of three former surface impoundments. Prior to their closure and capping between 1984 and 1986, the area of the former impoundments served as a primary source area of VOC releases to the groundwater at the Seaboard Facility. Additionally, elevated VOC concentrations in groundwater are also present in the area of the soil residue mound, a contaminant source area located at the Landfill which has also been closed and capped. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report September 2019 Page 12 VOCs were detected in a limited area across Randleman Lake to the northeast of the Site. Concentrations of VOCs and/or 1,4-dioxane at levels above the North Carolina 2L Groundwater Quality Standards were detected at off -site bedrock monitoring wells PW- 14D, PW-15D, and PW-16D. These bedrock monitoring wells are located on the north side of the Randleman Lake basin from the Site. The extent of the VOC contaminant plume on the north side of Randleman Lake appears to be limited primarily to property encompassed by the Lake's buffer zone, which is maintained and regulated by the Piedmont Triad Regional Water Authority (PTRWA). Please note that a sample was not collected from monitoring well PW-18 during this monitoring event. Monitoring well PW-18 is located on the Crutchfield property on the north side of Randleman Lake from the Site. After numerous attempts to contact the property owner (written and verbal), permission to access the PW-18 location was not granted. Additional measures to gain permission to sample the well during the 2020 monitoring event will be undertaken, which may include sending requests by certified mail. Overall, the September 2019 groundwater analytical results and the general distribution of VOCs in the Site's groundwater are consistent with the historical groundwater quality monitoring results. 6.2 Surface Water Analytical Results Surface water sampling was conducted at the Southern Intermittent Stream, Northern Intermittent Stream, and at various locations and depths in Randleman Lake. The surface water results for VOCs and 1,4-dioxane are summarized in Table 3 and the ENCO laboratory report is provided in Appendix A. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report September 2019 Page 13 Randleman Lake The Randleman Lake surface water sampling stations include: • SW-6 — Upstream and background sample location for the Site, • SW-DRP-2 — Adjacent to the Site near Lift Station 1 and PW-DR1, • SW-7 — Downstream of the Site at the I-85 bridge, and • SW-DRP-11 —Downstream (—I mile) at Richland Creek confluence. The laboratory analytical data indicated no VOCs or 1,4-dioxane concentrations above the laboratory quantitation limits in any of Randleman Lake surface water samples. The locations of the surface water monitoring stations are shown on Figure 2 and a summary of the Randleman Lake surface water analytical results are provided in Table 3. Based on field observations during the September 2019 monitoring activities, the Randleman Lake was approximately one-half foot below normal pool elevation of 682 feet msl. Southern Intermittent Stream The Southern Intermittent Stream surface water sampling stations include: • SW-5 — Upstream of Seaboard Facility and downstream of City MRF, • SW-3 — Downstream of Seaboard Facility and upstream of Landfill, and • SW- 4 — Downstream of both Seaboard Facility and Landfill. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report September 2019 Page 14 The compound 1,4-dioxane was reported in all three of the Southern Intermittent Stream surface water monitoring stations. The upstream surface water monitoring station (SW-5) reported a 1,4-dioxane concentration of 5.8 ug/l. Both of the downstream surface water monitoring stations on the Southern Intermittent Stream, SW-3 and SW-4, reported detectable 1,4-dioxane concentrations of 1.7 ug/1 and 1,800 ug/l, respectively. No other Site VOCs were reported above the laboratory reporting limits in the samples collected from surface water monitoring stations SW-3 or SW-5. In addition to the reported concentration of 1,4-dioxane in the sample collected from surface water monitoring station SW-4, several Site VOCs were also reported in this sample. A summary of the analytical data for the Southern Intermittent Stream samples is provided in Table 3. Northern Intermittent Stream The Northern Intermittent Stream surface water sampling stations include: • SW-1 Surface Water Station —Upstream of the Landfill, and • SW-2 Surface Water Station — Downstream of the Landfill. The flow path of the Northern Intermittent Stream was re-routed in 2011 and no longer passes through a pipe beneath the Landfill. Due to a limited watershed area, these two surface water monitoring stations are typically dry except during periods of heavy rainfall. Both surface water monitoring stations for the Northern Intermittent Stream were dry during the September 2019 monitoring event. A summary of the laboratory analytical results for September 2019 monitoring event is provided on Table 3. A copy of the ENCO laboratory analytical report for the surface water samples is provided with Appendix A. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report September 2019 Page 15 6.3 Quality Control Samples Two trip blanks were submitted and analyzed for quality assurance purposes. No VOCs were detected at a concentration equaling or exceeding its laboratory quantitation limit in either of the trip blanks. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report September 2019 Page 16 7.0 Conclusions The major findings of the annual groundwater and surface water monitoring activities for September 2019 monitoring event at the Site include the following: • The overall groundwater flow pattern (Figure 2) at the Site continues to be toward Randleman Lake on both sides of the Lake basin. Pumping of the extraction well PW-DR1 over the past year indicates a significant capture zone for monitoring wells along the northern section of the Landfill adjacent to Randleman Lake. The observed capture zone also extends to the bedrock wells on the north side of Randleman Lake. The capture zone can be maintained by pumping extraction well PW-DR1 at a rate of approximately 10 - 15 gallons per minute. An operational extraction rate of 13 — 14 gallons per minute from PW-DR1 during this monitoring period has demonstrated a drawdown of approximately 24 feet which creates an effective capture zone. • During the September 2019 monitoring event, concentrations of 1,4-dioxane above the laboratory method detection limit of 1.2 ug/l were reported at six of the nine surface water monitoring locations. This sampling event occurred during a period of extremely low surface water flow due to an extended period without significant rainfall. Only two of the surface water samples (SW-4 and SW-5) exceeded the laboratory quantitation limit of 2.0 ug/l. The laboratory analytical data indicated no 1,4-dioxane concentrations above the laboratory quantitation limit of 2.0 ug/l in any of the Randleman Lake surface water samples. Two of the locations (SW-1 and SW-2) were dry and not sampled. As summarized on Table 3 of this report, detectable concentrations of 1,4-dioxane in the surface water samples, including the SW-6 upstream background sample, exceeded the NC Protective Value for 1,4-dioxane of 0.35 ug/l. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report September 2019 Page 17 • Based on the September 2019 monitoring results and historical data, the main VOC plume extends from the former Seaboard Facility and City Landfill soil residue mound through the Southern Intermittent Stream valley northeastward to Randleman Lake. The VOCs and/or 1,4-dioxane detected on the north side of the lake across from the Site in monitoring wells PW-14D, PW-15D, and PW-16D represents the northern extent of the VOC plume. Based on historical groundwater analytical results, the northern extent of Site VOCs in the groundwater north of Randleman Lake is likely restricted to the Piedmont Triad Regional Water Authority regulated buffer. • The September 2019 monitoring data indicated that groundwater levels at monitoring wells located adjacent to the Randleman Lake have risen approximately 10 to 12 feet compared to pre -lake water level conditions. Inland from the lake, the 2019 groundwater levels at wells located on the western portion of the Site are approximately 4 feet higher compared to pre -lake water level conditions. • Overall, the September 2019 groundwater monitoring results are generally consistent with historical monitoring data. The geometry and migration of VOC- affected groundwater at the Site have not been substantially altered by the filling of Randleman Lake to normal pool. Pumping of extraction well PW-DR1 at a rate of 13 - 14 gallons per minute has demonstrated a significant capture zone created by the drawdown on both sides of Randleman Lake. Seaboard Chemical/Riverdale Drive Landfill Water Quality Monitoring Report September 2019 Page 18 FIGURES TIRE: Site Location leap Seaboard/Riverdale LF Site Jamestown, North Carolina Babb & Associates, P.A. MGM W. W"..• PAWECT NO. Figure 1 1 "= 8000' CHECKM ■r. AU*W or- WE G. Babb 2/10/11 . SW-2�SW-6 LOCATED AT UPSTREAM PW-18 SIDE OF KI VETT DRIVE BRIDGE A _-. --- I' II ,l ------ ow Nis, �. RW-Nls .� . M 2.6sA W 2D RIVERDALE DRIVE LANDFILL 90.96 I \ *PW-19 / II 1, PW-14D i PW679.91 W , s I � / I I J7I 1598.62 - - I PW 15 *w ;ss 679,20 Y v. . . PN �� SW OR 2 W 78.3s D ,, — I. 7 \\\ \\\ FORMER BURN 681.41 . III MW-1 , i i PITS AREA / ! 7 687.3 1�I - OW RZ MW-4 111 9 I \ f e MW 3B 675.63 \ _/`e 785.88 i 1 i j---_ OW-DR4 MW 3A wA r w , 6 � \� RECOVERY Alsce v �Ho�sr 1 M W— 3 C �, `, W`•��I'i -� _ 1� A -683.76 L) \ T i - .. `� 678,85 R) THE�N� -,. TENCl _\ RW-SIS1 /N RMITTENT '` --- \� •\ •�_ ., MAGARAGNC -� GARAGE MW-17 Y W 3A Ir i MRF-1 _SOIL SIDUE� W 15 A UND 741.75 �. p M / e \ MATERIAL 1 , �� I RECYCLING W- 21 � II FACILITY j R SIS2 .17 RW-s—IS1 \-sw-s i -LFS2 . 1. . vT 4A 8 \6 .25 S/W6 G w 1-5 \\ eMW_ 1\ -/ 5'ul0N INrERMW�IT20NT _ _Ea OW'SIS2 w 4 W-3D �go \\ \\ \I s?s8 �Pw V MRF-2 �___ -� g OW-SF1 �� MW 8e HOUSE 711, 1 00 eW 18 W-5 _ q // I �) y (� I OF 1 94�w✓-78 _.. P VV y'.�l'?C W 0 PRAYER �_— 4YM-7A ' 682 73� 81.6 PW-10D\\; I 651.56 o IIi / I _W-2s JW-29 II 710 Y RIVERDALE DRIVE LANDFILL 1� \ . J1 �20 II \. . i FORMERSEABOARD L- I ` I I \ CHEMICAL I CORPORA PON Q RIVERDACE ORII/E o a .1 M I II SW—dRP-11 LOG TE / P\ V 1 21 J DOWNSTREAM A 727 65 EAST SIDE ONFL UENCE Wl ` -' S -7 PW-17 m /' wASiERATER o / / REAMEN r CHLAND CREE PLANT W— 6 \ SCALE IN FEET I 0 75 150 300 oBASE MAP FROM BBL REMEDIAL INVESTIGATION LEGEND FIGURE o REPORT, MARCH 1999. g MONITORING WELL (SAPROLITE/PWR) SEPTEMBER 2019 GROUNDWATER POTENTIOMETRIC MAP N WELLS TO BE SAMPLED SHOWN ® RECOVERY WELL (SAPROLITE/SB) GROUNDWATER AND SURFACE WATER SAMPLE LOCATIONS N ENLARGED TYPE & FORMER SEABOARD CHEMICAL/RIVERDALE DRIVE LF ,nn A SURFACE WATER MONITORING STATION Babb & Associates, P.A. JAMESTOWN, NORTH CAROLINA FORMER BURN mw—1 (BQL) PITS AREA HOUSE or PRAMR —SOIL RESIDUE MOUND MW-15A* (BOL) MA RVAL M FACILITY 0 LREC'= FVRMER -W-480ARD OVMVrIL CORPORATON BASE MAP FROM BBL REMEDIAL INVESTIGATION REPORT, MARCH 1999. CITr' MAINTENANCE GARAGE NOTE: WELLS TO BE SAMPLED SHOWN IN ENLARGED TYPE .z MW_12A,,_ (B.) mw—l(zp_jL_ MW-1 26-- PW-18 -Ito 720, . . . . . PW-14D PW-16 ..... ...... . . . . . . . . . . . . . . . . . . . . . . . . PW-15# . . . . . . . . . . . . . . . (BQL) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . PW-6D . . . . . . . . . . . . . . . . . . . . . . . . . . . .. .. . . W— 61 (4.7) \ . . . . . . . . . . . . . . . .. .. . (2.9) . . . . . . . . . . . . . . . EAST SIDE WASIEWA IER 7R&4 WEN PLANT M W— +6� LEGEND MONITORING WELL (BEDROCK) RECOVERY WELL (SAPROLITE/SB) (64.6) CONCENTRATION IN PPB C NCE�TIONS GREATER THAN 1'� 00 60tN CONCENTRATIONS G EATER THAN 100 Ug CON E IONS GREATER THAN 10 u L_ SCALE IN FEET 0 75 150 300 *PW-18 I M W-12,A (BQL) Y M W BQL) (BQL) MW-12 -------- (BQL) / /� PW-14D PW-16� \ (BQL) (,.3) . LEGEND ((( MONITORING WELL (BEDROCK) ECOVERY WELL (SAPROLITE/SB) . . . _ _ . . . . _ _ _ PW-15 . . . . i.`� ��ss2 C NCENTRAPON IN PPB (BQL) / \ / // PW�6D 0 C NCE TIONS GREATER THAN M W-1 \ FORMER BURN — — — _ / W— 6I ,(2S) PITS AREA /' _ ._ . /� (5.3) // I \ I 5 0 u (BQL) { / 131 OW— R2 ;---- // 0 CONCENTRATIONS G EATER THAN / WAY 10 ug/L M W �, a Q (5s) OW=DR3 a(gy) \ MArNrENANCE1'`� / GARAGE HOUSE PRAM SOIL RESIDUE MOUND MW-15A* (BQL) a MAIM& RECYCITMG FACILITY o CNaW AL COMPORAWN I RI BASE MAP FROM BBL REMEDIAL INVESTIGATION REPORT. MARCH 1999. OW—LFS2 m (BQL) .� W D / I / y. P fn JFF 1 \ MW— 0 . \— \ (3.7 (BQL) . RIVERDALE DRIVE LANDFILL . --- I PW—(10D I I I I � I{ PWW-121 \ SME (BQL) IYAS7M7ER TREATMENT PUNT N SCALE IN FEET 75 150 300 740 —730 /760� IWMAL RECYVUNO FACILITY BASE MAP FROM BBL REMEDIAL INVESTIGATION REPORT, MARCH 1999. �i MW-12A (6.2) 2P.LA (10) MW-12 (BOL` / FORMER BURN P175 AREA L \ 1 HOUSE ream S> VON aTr MAINTENANCE GARAGE PW+--121 (BOL) j / \ PW-14Dy�yy� PW /1/4 \ (1.4) T / (22) \ EAST WE WASTEWAMR TREATMENT PLANT RIVERDALE DRIVE LANDFILL 720 �720 ��730 PWL6D ; l / W-61// (120) (13) / / lI I I S2 (3 z \— MW5) 0. . (2.6) . . . . PW-10D (BOL) „ l 11 11 j! i MW _6 —740 LEGEND MONITORING WELL (BEDROCK) ® ECOVERY WELL (SAPROLITE/SB) (662) CONCENTRATION IN PPB CONCENTRATIONS GREATER THAN 1,000 ug/L 0 CONCENTRATIONS GREATER THAN 100 ug/L CONCENT TIONS GREATER THAN 10 ug/L L� G 0 SCALE IN FEET 75 150 300 PW-18 I •.c - 7 Q MW 1 M W�' W�L12 I I � I I /1 I �� FORMER M W—BURN / \ I I 1 * I PITS AREA ( 8OL) I I 1 I � Y WAY o I ....................... GITr MAINTENANCE I GARAGE 730 /760� 730 740 i / I L PW-14D� f� BASE MAP FROM BBL REMEDIAL INVESTIGATION REPORT. MARCH 1999. PW-18 720 ,10 �720 730 / / \ 740 _ ✓'W�P N \ \ .I- LEGEND �Dl MONITORING WELL (BEDROCK) W61 (9(ss2) OONC�ION PPB (148) � C NC 7TR IONS EATER THAN V.Y.1 0,000 ug/L I I� CONCENTRATIONS GREATER THAN 1,000 u g/L R3 I I NJ CONCERATION�REATER THAN I I 1-00 uq/L ,I 1 CON^ RATIONS EATER THAN 'j v OW—LFS2 \ \ Z (213) \ \. .rn . �— MW) 0\\. . (292 PW-10D (soy) I ,I SCALE IN FEET \\ % / 0 75 150 300 MW6�......\ll /� BASE MAP FROM BBL REMEDIAL INVESTIGATION REPORT. MARCH 1999. TABLES TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 1 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-1 57.71 47.71-57.71 743.98-733.98 789.40 791.69 11/14/2000 27.28 764.41 9/4/2001 27.99 763.70 9/17/2002 29.55 762.14 9/11/2003 23.86 767.83 8/16/2004 25.70 765.99 12/19/2005 25.55 766.14 8/21/2006 25.97 765.72 9/24/2007 26.33 765.36 2/23/2009 25.35 766.14 3/29/2010 24.89 765.72 11/1/2011 27.69 764.00 11/16/2012 27.23 764.46 12/9/2013 28.36 763.33 12/8/2014 28.54 763.15 New Survey 788.85 790.46 10/26/2015 27.99 763.47 11/14/2016 27.50 762.96 10/11/2017 28.43 762.03 11/1/2018 29.70 760.76 9/10/2019 24.78 765.68 MW-2A 19 4-19 709.9-694.9 711.80 713.90 11/14/2000 13.46 700.44 9/4/2001 17.43 696.47 9/17/2002 10.25 703.65 9/11/2003 10.60 703.30 8/16/2004 7.83 706.07 8/21 /2006 13.04 700.86 9/24/2007 14.17 699.73 2/23/2009 10.67 703.23 3/29/2010 6.11 707.79 11/1/2011 8.18 705.72 11/16/2012 12.90 701.00 MW-26 30 30 681.0 711.00 712.57 11/14/2000 12.78 699.79 9/4/2001 13.01 699.56 9/17/2002 10.61 701.96 9/11/2003 10.62 701.95 8/16/2004 7.75 704.82 8/21 /2006 12.25 700.32 9/24/2007 14.64 697.93 2/23/2009 10.35 702.22 3/29/2010 6.05 706.52 11/1/2011 9.16 703.41 1 /16/2012 12.21 700.36 MW-2C 48 28-48 685.56-665.56 711.40 713.56 11/14/2000 16.12 697.44 9/4/2001 14.02 699.54 9/17/2002 18.41 695.15 9/11/2003 12.78 700.78 8/16/2004 14.80 698.76 12/19/2005 NM NM 8/21 /2006 17.53 696.03 9/24/2007 16.86 696.70 2/23/2009 14.25 699.31 3/29/2010 10.97 702.59 11/1/2011 14.55 699.01 11/16/2012 15.82 697.74 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 2 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-3A 27 12-27 682.4-667.4 692.74 694.40 11/14/2000 19.62 674.78 9/4/2001 21.03 673.37 9/17/2002 20.22 674.18 9/11/2003 16.74 677.66 8/16/2004 18.60 675.80 12/19/2005 18.54 675.86 8/21/2006 20.32 674.08 9/24/2007 17.18 677.22 2/23/2009 11.00 683.40 3/29/2010 10.92 683.48 11 /1 /2011 12.34 682.06 11/16/2012 11.87 682.53 MW-36 38.83 28.83-38.83 664.76-654.76 692.32 693.59 11/14/2000 19.46 674.13 9/4/2001 21.00 672.59 9/17/2002 20.00 673.59 9/11/2003 16.32 677.27 8/16/2004 NM NM 12/19/2005 18.81 674.78 8/21/2006 20.33 673.26 9/24/2007 16.59 677.00 2/23/2009 8.48 685.11 3/29/2010 8.04 685.55 11 /1 /2011 11.27 682.32 11/16/2012 11.00 682.59 MW-3C 57 47-57 647.22-637.22 691.90 694.22 11/14/2000 19.51 674.71 9/4/2001 21.12 673.10 8/19/2002 20.57 673.65 9/16/2002 20.00 674.22 9/11/2003 16.47 677.75 8/16/2004 18.46 675.13 12/19/2005 18.96 674.63 8/21/2006 20.56 673.03 9/24/2007 16.50 677.72 2/23/2009 10.15 683.44 3/29/2010 7.86 685.73 11 /1 /2011 10.33 683.89 11/16/2012 10.88 683.34 12/11/2013 10.54 683.68 12/11/2014 20.74 673.48 New Survey 692.50 692.74 10/27/2015 17.68 675.06 11/14/2016 9.90 682.84 10/9/2017 20.46 672.28 11 /2/2018 18.31 674.43 9/11/2019 18.00 674.74 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 3 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-4 30 20-30 664.72-654.72 683.20 684.72 11/14/2000 12.22 672.50 9/4/2001 14.18 670.54 9/ 16/2002 12.71 672.01 9/11/2003 10.62 674.10 8/16/2004 11.91 672.81 12/19/2005 17.55 667.17 8/21/2006 NM NM 9/24/2007 13.22 671.50 New TOC elevation 683.87 687.29 2/23/2009 8.02 679.27 3/29/2010 6.25 681.04 11/1/2011 6.48 680.81 11/16/2012 7.01 680.28 MW-5 30 20-30 664.4-654.4 682.00 684.40 11/14/2000 12.89 671.51 9/4/2001 14.69 669.71 9/ 16/2002 13.81 670.59 9/11/2003 9.23 675.17 8/16/2004 12.05 672.35 12/19/2005 16.59 667.81 8/21/2006 NM NM 9/24/2007 13.98 670.42 New TOC elevation; survey data pending 2/23/2009 5.82 NA 3/29/2010 4.63 NA 11/1/2011 6.18 NA 11/16/2012 6.61 NA MW-6 110 100-110 661.73-651.73 759.60 761.73 11/14/2000 65.92 695.81 9/4/2001 66.49 695.24 9/17/2002 67.21 694.52 9/11/2003 59.32 702.41 8/16/2004 63.47 698.26 12/19/2005 65.83 695.90 8/21/2006 66.46 695.27 9/24/2007 67.11 694.62 2/23/2009 62.58 699.15 3/29/2010 60.55 701.18 11/1/2011 64.36 697.37 11/16/2012 64.60 697.13 12/11/2013 64.88 696.85 12/12/2014 65.80 695.93 New Survey 759.74 761.47 10/30/2015 64.89 696.58 11/17/2016 64.38 697.09 10/10/2017 65.03 696.44 11 /2/2018 61.20 700.27 9/12/2019 62.28 699.19 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 4 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-7A 35 15-35 726.64-706.64 739.42 741.64 11/14/2000 31.10 710.54 9/4/2001 32.34 709.30 9/17/2002 35.73 705.91 9/11/2003 22.61 719.03 8/16/2004 29.02 712.62 12/19/2005 31.13 710.51 8/21 /2006 31.19 710.45 9/24/2007 30.55 711.09 2/23/2009 28.23 713.41 3/29/2010 23.65 717.99 11/1/2011 30.61 711.03 11/16/2012 30.60 711.04 MW-713 68 58-68 682.16-672.16 738.50 740.16 11/14/2000 33.90 706.26 9/4/2001 33.15 707.01 9/17/2002 38.12 702.04 9/11/2003 24.53 715.63 8/16/2004 31.80 708.36 12/19/2005 33.74 706.42 8/21 /2006 33.36 706.80 9/24/2007 33.31 706.85 2/23/2009 30.18 709.98 3/29/2010 25.67 714.49 11/1/2011 27.93 712.23 11/16/2012 30.00 710.16 MW-8 33 13-33 721.16-701.16 731.80 734.16 11/14/2000 >30.70 - 9/4/2001 >30.70 9/17/2002 >30.70 - 9/11/2003 20.49 719.67 8/16/2004 28.35 711.81 12/19/2005 20.22 719.94 8/21 /2006 30.81 709.35 9/24/2007 32.89 701.27 2/23/2009 26.39 713.77 3/29/2010 20.51 719.65 11/1/2011 28.85 705.31 11/16/2012 30.96 703.20 MW-9 32 12-32 676.95-656.95 685.95 688.95 11/14/2000 12.36 9/4/2001 13.53 675.42 9/16/2002 13.48 675.47 9/11/2003 8.15 680.80 8/16/2004 10.78 678.17 12/19/2005 11.43 677.52 8/21 /2006 21.35 667.60 9/24/2007 NM NM 2/23/2009 5.37 683.58 3/29/2010 4.22 684.73 11/1/2011 5.97 682.98 11/16/2012 6.26 682.69 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 5 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-10 28 8-28 687.62-667.62 693.60 695.62 11/14/2000 16.91 678.71 9/4/2001 18.61 677.01 9/16/2002 17.64 677.98 9/11/2003 13.78 681.84 8/16/2004 15.06 680.56 12/19/2005 14.47 681.15 8/21 /2006 16.80 678.82 9/24/2007 17.29 678.33 2/23/2009 11.92 683.70 3/29/2010 10.57 685.05 11 /1 /2011 12.96 682.66 11/16/2012 13.18 682.44 12/10/2013 12.97 682.65 12/10/2014 13.97 681.65 New Survey 693.24 695.01 10/26/2015 12.59 682.42 11/14/2016 12.86 682.15 10/9/2017 12.95 682.06 10/31 /2018 11.53 683.48 9/10/2019 13.40 681.61 MW-11 68 53-68 695.42-680.42 746.26 748.42 11/14/2000 38.24 710.18 9/4/2001 38.50 709.92 8/19/2002 41.06 707.36 9/16/2002 40.65 707.77 9/11/2003 28.97 719.45 8/16/2004 36.81 711.61 12/19/2005 38.51 709.91 8/21 /2006 32.91 715.51 9/24/2007 37.29 711.13 2/23/2009 28.91 719.51 3/29/2010 26.02 722.40 11/1/2011 31.13 717.29 11/16/2012 34.87 713.55 MW-12A 20 5-20 688.96-673.96 691.12 693.96 11/14/2000 15.66 678.30 9/4/2001 15.87 678.09 9/16/2002 15.62 678.34 9/11/2003 11.08 682.88 8/16/2004 14.15 679.81 12/19/2005 11.31 682.65 8/21 /2006 14.67 679.29 9/24/2007 13.92 680.04 2/23/2009 11.11 682.85 3/29/2010 9.99 683.97 11 /1 /2011 9.26 684.70 11/16/2012 11.13 682.83 12/10/2013 9.07 684.89 12/11/2014 11.58 682.38 New Survey 690.21 693.07 10/27/2015 11.15 681.92 11 /14/2016 11.01 682.06 10/9/2017 10.98 682.09 11/1/2018 10.19 682.88 9/ 10/2019 10.41 682.66 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 6 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-12B 58 48-58 647-637 691.70 695.00 11/14/2000 16.49 678.51 9/4/2001 16.92 678.08 9/16/2002 16.65 678.35 9/11/2003 12.72 682.28 8/16/2004 15.03 679.97 12/19/2005 14.12 680.88 8/21/2006 NM NM 9/24/2007 NM NM 2/23/2009 10.95 684.05 3/29/2010 NM NM 11/1/2011 10.25 684.75 11/16/2012 10.81 684.19 12/10/2013 11.55 683.45 12/11/2014 11.65 683.35 New Survey 690.75 693.86 10/27/2015 10.67 683.19 11/14/2016 10.23 683.63 10/ 10/2017 11.21 682.65 11 /1 /2018 10.22 683.64 9/11/2019 10.76 683.10 MW-12D 202 187-202 507.93-492.93 691.81 694.93 11/14/2000 >101.50 <593 9/4/2001 48.12 646.81 9/16/2002 47.59 647.34 9/11/2003 46.06 648.87 8/16/2004 NM NM 12/19/2005 20.80 674.13 8/21/2006 NM NM 9/24/2007 14.24 680.69 2/23/2009 9.43 685.50 3/29/2010 12.62 682.31 11/1/2011 13.88 681.05 11/16/2012 43.06 651.87 12/10/2013 25.34 669.59 12/11/2014 43.02 651.91 New Survey 691.19 694.21 10/29/2015 21.96 672.25 11/18/2016 24.12 670.09 10/11/2017 53.41 640.80 11 /1 /2018 26.84 667.37 9/12/2019 3.25 690.96 MW-14 35 20-35 746.22-731.22 763.80 766.22 11/14/2000 28.42 737.80 9/4/2001 29.33 736.89 9/17/2002 NM NM 9/11/2003 25.38 740.84 8/16/2004 26.16 740.06 8/21/2006 27.98 738.24 2/23/2009 27.27 738.95 3/29/2010 25.71 740.51 11/1/2011 27.86 738.36 11/16/2012 27.61 738.61 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 7 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MW-15A 34 19-34 731.34-746.34 762.5 765.34 9/4/2001 26.70 738.64 9/17/2002 21.40 743.94 9/11/2003 NM NM 8/16/2004 22.72 742.62 12/19/2005 24.31 741.03 8/21/2006 NM NM 2/23/2009 15.21 750.13 3/29/2010 22.06 743.28 11/1/2011 25.19 740.15 11/16/2012 24.75 740.59 12/10/2013 24.69 740.65 12/8/2014 25.64 739.70 New Survey 762.57 764.33 10/27/2015 24.46 739.87 11/14/2016 27.01 737.32 10/11/2017 27.90 736.43 10/31/2018 22.72 741.61 9/10/2019 22.58 741.75 MW-16 45 30-45 749.13-734.13 779.00 779.13 11/14/2000 34.18 744.95 9/4/2001 NM NM 9/17/2002 NM NM 9/11/2003 NM NM 8/16/2004 NM NM 12/19/2005 NM NM 8/21/2006 NM NM 2/23/2009 NM NM 11/16/2012 NM NM MW-17 (WSW-1) 250 230-250 12/19/2005 68.09 8/21/2006 NM NM 2/23/2009 66.04 3/29/2010 64.30 11 /1 /2011 66.88 11/16/2012 67.34 NM MRF-1 43.5 28.5-43.5 723.31-708.31 752.10 751.81 11/14/2000 8.45 743.36 9/4/2001 8.48 743.33 9/17/2002 8.56 743.25 9/11/2003 7.40 744.41 8/16/2004 7.59 744.22 12/19/2005 7.63 744.18 8/21/2006 8.25 743.56 9/24/2007 8.87 742.94 2/23/2009 7.56 744.25 3/29/2010 7.55 744.26 11 /1 /2011 8.01 743.80 11/16/2012 7.98 743.83 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 8 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) MRF-2 41.5 26.5-41.5 724.23-709.23 751.00 750.73 11/14/2000 26.06 724.67 9/4/2001 26.18 724.55 9/17/2002 26.10 724.63 9/11/2003 24.28 726.45 8/16/2004 24.10 726.63 12/19/2005 24.35 726.38 8/21/2006 25.69 725.04 9/24/2007 25.69 725.04 2/23/2009 25.22 725.51 3/29/2010 24.73 726.00 11/1/2011 25.18 725.55 11/16/2012 25.30 725.43 OW-DR1 165 49-165 648.95-532.95 695.39 697.95 11/14/2000 23.21 674.74 9/4/2001 24.72 673.23 9/16/2002 23.80 674.15 9/11/2003 20.21 677.74 8/16/2004 22.23 675.72 12/19/2005 22.91 675.04 8/21/2006 24.40 673.55 9/24/2007 20.16 677.79 2/23/2009 13.77 684.18 3/29/2010 11.42 686.53 11 /1 /2011 13.95 684.00 11/16/2012 14.64 683.31 OW-DR2 186 176-186 518.4-508.4 692.61 694.40 11/14/2000 19.72 674.68 9/4/2001 21.33 673.07 8/19/2002 20.75 673.65 9/16/2002 20.25 674.15 9/11/2003 16.60 677.80 8/16/2004 18.62 675.78 12/19/2005 19.34 675.06 8/21/2006 20.79 673.61 9/24/2007 16.52 677.88 2/23/2009 10.13 684.27 3/29/2010 7.97 686.43 11 /1 /2011 10.32 684.08 11/16/2012 10.90 683.50 12/10/2013 10.55 683.85 12/12/2014 27.31 667.09 New Survey 692.22 695.87 10/30/2015 13.53 682.34 11/18/2016 14.28 681.59 10/ 10/2017 16.31 679.56 11 /2/2018 19.59 676.28 9/11/2019 20.24 675.63 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 9 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) OW-DR3 160 77-160 626.52-543.52 703.52 704.75 8/19/2002 30.79 663.61 9/16/2002 30.40 664.00 9/11/2003 27.80 666.60 8/16/2004 29.02 665.38 12/19/2005 30.29 664.11 8/21 /2006 31.17 663.23 9/24/2007 26.32 678.43 2/23/2009 20.17 684.58 3/29/2010 18.61 686.14 11/1/2011 20.45 684.30 11/16/2012 20.75 684.00 12/10/2013 20.99 683.76 OW-DR4 165 45 - 165 667.70-547.70 712.70 713.85 8/19/2002 40.15 673.70 9/16/2002 39.72 674.13 9/11/2003 36.25 677.60 8/16/2004 38.23 675.62 12/19/2005 38.91 674.94 8/21 /2006 40.34 673.51 9/24/2007 35.99 677.86 2/23/2009 29.64 684.21 3/29/2010 22.30 691.55 11/1/2011 29.83 684.02 11/16/2012 30.30 683.55 OW-DR5 40 20-40 12/19/2005 10.50 -- 2/23/2009 NM 3/29/2010 NM 11/1/2011 NM 11/16/2012 NM NM OW-NIS1 40 25-40 12/19/2005 10.91 2/23/2009 8.40 3/29/2010 7.59 11/1/2011 6.40 11/16/2012 7.54 OW-SIS1 39 20-39 12/19/2005 24.05 8/21 /2006 24.08 9/24/2007 23.89 2/23/2009 20.89 3/29/2010 17.69 11/1/2011 22.98 11/16/2012 22.99 OW-SIS2 40 20-40 12/19/2005 5.32 2/23/2009 4.32 3/29/2010 3.29 11/1/2011 3.74 11/16/2012 7.63 OW-SIS3 45 15-45 12/19/2005 5.80 2/23/2009 5.67 3/29/2010 3.61 11/1/2011 5.22 11/16/2012 7.00 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 10 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) OW-SF1 120 95-120 638.15-613.15 731.06 731.06 12/19/2005 26.15 704.91 8/21/2006 26.00 705.06 9/24/2007 25.84 705.22 2/23/2009 23.03 708.03 3/29/2010 18.64 712.42 11/1/2011 25.39 705.67 11/16/2012 25.22 705.84 OW-SF2 120 80-120 651.05-611.05 728.87 731.05 8/21/2006 NM NM 9/24/2007 20.44 710.61 2/23/2009 18.47 -- 3/29/2010 14.27 716.78 11/1/2011 20.46 710.59 11/16/2012 20.68 710.37 OW-LFS1 50 30-50 698.74 12/19/2005 17.15 681.59 2/23/2009 14.45 684.29 3/29/2010 13.28 685.46 11/1/2011 14.90 683.84 11/16/2012 15.88 682.86 OW-LFS2 50 30-50 700.08 12/19/2005 21.97 678.11 2/23/2009 15.81 684.27 3/29/2010 14.66 685.42 11/1/2011 16.34 683.74 11/16/2012 16.61 683.47 12/11/2013 16.82 683.26 12/12/2014 17.44 682.64 New Survey 696.69 699.45 10/26/2015 16.48 682.97 11/14/2016 20.12 679.33 10/9/2017 25.57 673.88 10/31/2018 38.96 660.49 9/12/2019 17.20 682.25 PW-DR1 185 38-185 657.21-510.21 693.62 695.21 11/14/2000 20.51 674.70 9/4/2001 21.90 673.31 8/19/2002 21.48 673.73 9/16/2002 21.02 674.19 9/11 /2003 17.51 677.70 8/16/2004 19.55 675.66 12/19/2005 NM -- 8/21/2006 NM 9/24/2007 NM 2/23/2009 NM 3/29/2010 NM 11/1/2011 NM 11/16/2012 NM TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 11 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-SF1 120 95-120 638.15-613.15 732.14 733.15 8/21/2006 25.98 707.17 9/24/2007 25.60 707.55 2/23/2009 22.96 710.19 3/29/2010 18.62 714.53 11 /1 /2011 25.31 707.84 11/16/2012 25.50 707.64 12/9/2013 21.00 712.15 12/8/2014 26.65 706.50 New Survey 731.13 732.19 10/27/2015 26.78 705.41 11/17/2016 24.45 707.74 10/11/2017 28.21 703.98 10/31 /2018 22.17 710.02 9/10/2019 20.50 711.69 PW-SIS1 39 19-39 695.21 8/16/2004 NM -- 12/19/2005 12.20 683.01 8/21/2006 13.95 681.26 9/24/2007 15.43 679.78 2/23/2009 12.73 682.48 3/29/2010 11.31 683.90 11 /1 /2011 13.01 682.20 11/16/2012 13.63 681.58 PW-1D 81.5 66.5-81.5 717.18-702.18 781.90 783.68 11/14/2000 54.92 728.76 9/4/2001 54.60 729.08 9/17/2002 54.65 729.03 9/11/2003 47.49 736.19 8/16/2004 NM -- 12/19/2005 51.82 731.86 8/21/2006 NM -- 2/23/2009 49.60 734.08 3/29/2010 47.86 735.82 11 /1 /2011 50.18 733.50 11/16/2012 50.30 733.38 PW-2D 101 80-100 700.55-680.55 778.80 780.55 11/14/2000 45.43 735.12 9/4/2001 45.16 735.39 9/17/2002 NM -- 9/11/2003 NM -- 8/16/2004 43.45 737.10 12/19/2005 43.94 736.61 8/21/2006 42.75 737.80 9/24/2007 44.20 736.35 2/23/2009 41.43 739.12 3/29/2010 39.30 741.25 11 /1 /2011 42.62 737.93 11/16/2012 42.20 738.35 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 12 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-3D 209.5 179.5-209.5 578.84-548.84 756.60 758.34 11/14/2000 56.60 701.74 9/4/2001 NM -- 9/16/2002 58.62 699.72 9/11/2003 NM -- 8/16/2004 55.55 702.79 12/19/2005 NM -- 8/21/2006 56.75 701.59 2/23/2009 50.02 708.32 3/29/2010 48.12 710.22 11 /1 /2011 50.52 707.82 11/16/2012 47.90 710.44 12/17/2013 48.81 709.53 12/11/2014 49.51 708.83 New Survey 737.63 738.60 10/29/2015 48.91 689.69 11/16/2016 52.42 686.18 10/11/2017 43.99 694.61 11 /2/2018 50.71 687.89 9/11/2019 52.02 686.58 PW-41 122 112-122 625.67-615.67 735.17 737.67 11/14/2000 43.39 694.28 9/4/2001 44.73 692.94 9/17/2002 45.94 691.73 9/11/2003 36.04 701.63 8/16/2004 42.31 695.36 12/19/2005 43.27 694.40 8/21 /2006 43.11 712.03 2/23/2009 39.35 698.32 3/29/2010 35.56 719.58 11 /1 /2011 41.23 696.44 11/16/2012 41.49 696.18 12/17/2013 42.03 695.64 12/8/2014 42.62 695.05 New Survey 732.04 737.59 10/29/2015 42.10 695.49 Corrected elevation after well repair. Removed 2.59' of casing. 735.00 11/17/2016 40.78 694.22 10/11/2017 43.80 691.20 11 /2/2018 34.04 700.96 9/11/2019 35.52 699.48 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 13 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-5D 306.5 272-282 425.87-415.87 695.07 697.87 11/14/2000 23.52 674.35 9/4/2001 24.04 673.83 8/19/2002 24.54 673.33 9/16/2002 23.86 674.01 9/11/2003 20.37 677.50 8/16/2004 22.45 675.42 12/19/2005 23.21 674.66 8/21 /2006 24.68 673.19 9/24/2007 20.31 677.56 2/23/2009 13.85 684.02 3/29/2010 10.85 687.02 11 /1 /2011 13.98 683.89 11/16/2012 12.92 684.95 12/16/2013 10.54 687.33 12/11/2014 21.86 676.01 New Survey 693.96 696.27 10/30/2015 13.80 682.47 11/18/2016 13.73 682.54 10/ 10/2017 17.41 678.86 11 /2/2018 17.31 678.96 9/11/2019 17.42 678.85 PW-61 76 65-76 619.19-608.19 682.27 684.19 11/14/2000 11.80 672.39 9/4/2001 13.98 670.21 8/ 19/2002 12.81 671.38 9/16/2002 12.35 671.84 9/11/2003 11.20 672.99 8/16/2004 12.00 672.19 12/19/2005 16.14 668.05 8/21/2006 NM -- 9/24/007 NM -- New TOC elevation 693.57 696.15 2/23/2009 14.75 681.40 3/29/2010 11.76 684.39 11/1/2011 13.98 682.17 11/16/2012 14.26 669.93 12/16/2013 14.29 681.86 New well 12/10/2014 17.43 679.98 New Survey 100 90-100 695.12 697.41 10/27/2015 16.15 681.26 11/17/2016 16.54 680.87 10/10/2017 17.38 680.03 11/1/2018 15.47 681.94 9/12/2019 16.00 681.41 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 14 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-6D 275 260-275 424.77-409.77 682.22 684.77 11/14/2000 11.01 673.76 9/4/2001 12.58 672.19 8/19/2002 12.07 672.70 9/16/2002 11.57 673.20 9/11/2003 7.87 676.90 8/16/2004 9.95 674.82 12/19/2005 13.24 671.53 8/21/2006 NM -- 9/24/2007 NM -- New TOC elevation 691.53 696.33 3/12/2009 13.05 683.28 3/29/2010 11.84 684.49 11 /1 /2011 13.34 682.99 11/16/2012 14.03 682.30 12/16/2013 NA NA New well 12/10/2014 23.56 673.23 New Survey 300 270-300 695.02 696.79 10/30/2015 14.53 682.26 11/17/2016 15.02 681.77 10/10/2017 21.65 675.14 11 /1 /2018 17.33 679.46 9/12/2019 18.44 678.35 PW-71 101 90-100 594.92-584.92 683.42 684.92 11/14/2000 12.90 672.02 9/4/2001 14.58 670.34 6/ 16/2002 12.81 672.11 8/19/2002 13.28 671.64 9/ 16/2002 12.81 672.11 9/11/2003 11.69 673.23 8/16/2004 12.92 672.00 12/19/2005 11.41 673.51 8/21 /2006 14.38 670.54 9/24/2007 9.11 675.81 New TOC elevation; survey data pending 2/23/2009 2.34 NA 3/29/2010 1.89 NA 11/1/2011 1.85 NA 11/16/2012 2.99 NA PW-8S 48 35-45 728.13-718.13 761.23 763.13 11/14/2000 42.30 720.83 9/4/2001 45.10 718.03 9/17/2002 47.33 715.80 9/11/2003 38.95 724.18 8/16/2004 40.70 722.43 12/19/2005 42.80 720.33 8/21 /2006 43.39 719.74 9/24/2007 44.57 718.56 2/23/2009 41.66 721.47 3/29/2010 27.22 735.91 11 /1 /2011 40.58 722.55 11/16/2012 40.96 722.17 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 15 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-91 100 80-100 619.07-599.07 698.07 699.07 11/14/2000 21.80 677.27 9/4/2001 22.95 676.12 9/16/2002 22.74 676.33 9/11/2003 18.04 681.03 8/16/2004 20.50 678.57 12/19/2005 20.79 678.28 8/21 /2006 11.75 687.32 9/24/2007 21.14 677.93 2/23/2009 14.18 684.89 3/29/2010 13.50 685.57 11 /1 /2011 14.61 684.46 11/16/2012 15.18 683.89 PW-101 100 80-100 616.44-596.44 695.34 696.44 11/14/2000 17.24 679.20 9/4/2001 19.08 677.36 9/16/2002 18.30 678.14 9/11/2003 14.57 681.87 8/16/2004 16.05 680.39 12/19/2005 15.53 680.91 8/21 /2006 17.68 678.76 9/24/2007 17.44 679.00 2/23/2009 12.06 684.38 3/29/2010 10.62 685.82 11/1/2011 12.32 684.12 11/16/2012 13.37 683.07 12/11/2013 13.10 683.34 12/ 10/2014 14.21 682.23 New Survey 694.63 695.97 10/29/2015 12.43 683.54 11/17/2016 13.46 682.51 10/9/2017 14.19 681.78 11 /1 /2018 11.68 684.29 9/12/2019 13.20 682.77 PW-10D 200 185-200 512.75-497.75 695.48 697.96 11/14/2000 >101.50 - 9/4/2001 39.20 658.76 9/16/2002 46.45 651.51 9/11/2003 NM NM 8/16/2004 48.04 649.92 12/19/2005 29.01 668.95 8/21 /2006 32.60 665.36 9/24/2007 18.42 679.54 2/23/2009 14.51 683.45 3/29/2010 26.38 671.58 11 /1 /2011 17.01 680.95 11/16/2012 43.21 654.75 12/11/2013 42.25 655.71 12/10/2014 34.50 663.46 New Survey 695.13 697.26 11/3/2015 35.32 661.94 11/17/2016 25.33 671.93 10/10/2017 49.55 647.71 10/31 /2018 26.28 670.98 9/12/2019 45.70 651.56 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 16 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-111 90 75-90 710.45-695.45 784.38 785.45 11/14/2000 57.55 727.90 9/4/2001 58.00 727.45 9/17/2002 58.77 726.68 9/11/2003 53.81 731.64 8/16/2004 56.23 729.22 12/19/2005 56.65 728.80 8/21 /2006 56.73 728.72 9/24/2007 57.25 728.20 2/23/2009 55.90 729.55 3/29/2010 52.60 732.85 11 /1 /2011 55.01 730.44 11/16/2012 54.90 730.55 PW-121 105 90-105 660.54-645.54 748.07 750.54 11/14/2000 29.09 721.45 9/4/2001 32.36 718.18 2/16/2002 36.25 714.29 9/16/2002 36.25 714.29 9/11/2003 26.18 724.36 8/16/2004 27.41 723.13 12/19/2005 29.55 720.99 8/23/2006 30.15 720.39 9/24/2007 28.55 721.99 2/23/2009 28.93 721.61 3/29/2010 24.62 725.92 11/1/2011 28.18 722.36 11/16/2012 27.73 722.81 12/16/2013 28.17 722.37 12/12/2014 28.70 721.84 New Survey 746.99 749.48 10/30/2015 28.82 720.66 11/21/2016 35.73 713.75 10/11/2017 28.55 720.93 11/6/2018 29.51 719.97 9/11/2019 21.83 727.65 PW-131 250 235-250 504.9-489.9 736.58 739.90 11/14/2000 67.65 672.25 9/4/2001 69.68 670.22 8/19/2002 68.50 671.40 9/17/2002 68.12 671.78 9/11/2003 66.59 673.31 8/16/2004 67.52 672.38 12/19/2005 68.51 671.39 8/21/2006 69.64 670.26 9/24/2007 64.70 675.20 2/23/2009 57.31 682.59 3/29/2010 54.65 685.25 11 /1 /2011 57.33 682.57 11/16/2012 58.05 681.85 12/16/2013 57.20 682.70 12/12/2014 59.52 680.38 New Survey 736.23 739.01 10/26/2015 37.69 701.32 11/18/2016 58.24 680.77 10/11/2017 58.97 680.04 10/31/2018 57.15 681.86 9/11/2019 51.68 687.33 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 17 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-14D 198.8 183.8-198.8 505.33-490.33 686.38 689.13 10/31/2000 16.24 672.89 12/20/2000 > 150 - 9/5/2001 76.98 612.15 9/17/2002 64.16 624.97 9/11/2003 6.51 682.62 8/16/2004 56.01 633.12 12/19/2005 67.27 621.86 8/21/2006 37.29 651.84 9/24/2007 62.45 626.68 3/11/2009 37.90 651.23 3/29/2010 29.41 659.72 11/1/2011 17.63 671.50 11/16/2012 32.37 656.76 12/12/2013 56.60 632.53 12/9/2014 63.29 625.84 New Survey 685.27 686.50 11/3/2015 72.59 613.91 11/16/2016 46.02 640.48 10/12/2017 9.42 677.08 11 /5/2018 39.62 646.88 9/17/2019 87.88 598.62 PW-14S 21.5 11.5-21.5 677.09-667.09 685.96 688.59 10/30/2000 13.19 675.40 12/20/2000 13.47 675.12 9/5/2001 14.28 674.31 9/17/2002 14.55 674.04 9/11/2003 14.92 673.67 8/16/2004 10.26 678.33 12/19/2005 11.54 677.05 8/21 /2006 13.45 675.14 3/11/2009 4.34 684.25 3/29/2010 2.13 686.46 11/1/2011 4.27 684.32 11/16/2012 5.30 683.29 PW-15D 163.5 153.5-163.5 533.93-523.93 684.85 687.43 10/31/2000 13.25 674.18 12/20/2000 13.32 674.11 9/5/2001 14.79 672.64 9/17/2002 13.81 673.62 9/11/2003 10.13 677.30 8/16/2004 12.24 675.19 12/19/2005 13.03 674.40 8/21 /2006 15.80 671.63 9/24/2007 9.93 677.50 3/11/2009 3.20 684.23 3/29/2010 2.02 685.41 11/1/2011 3.25 684.18 11/16/2012 4.39 683.04 12/12/2013 4.50 682.93 12/9/2014 8.14 679.29 New Survey 684.05 685.80 10/28/2015 4.11 681.69 11/15/2016 4.54 681.26 10/12/2017 10.15 675.65 11 /5/2018 4.95 680.85 9/17/2019 6.60 679.20 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 18 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-15S 21.5 11.5-21.5 676.71-666.71 685.88 688.21 10/30/2000 14.87 673.34 12/20/2000 14.91 673.30 9/5/2001 16.26 671.95 9/17/2002 15.42 672.79 9/11/2003 11.61 676.60 8/16/2004 13.89 674.32 12/19/2005 14.14 674.07 8/21 /2006 14.32 673.89 9/24/2007 9.75 678.46 3/11/2009 4.65 683.56 3/29/2010 3.09 685.12 11/1/2011 4.58 683.63 11/16/2012 5.89 682.32 PW-16D 179 169-179 515.98-505.98 681.46 684.98 10/31/2000 10.94 674.04 12/20/2000 10.95 674.03 9/5/2001 12.43 672.55 9/17/2002 11.51 673.47 9/11/2003 7.88 677.10 8/16/2004 9.91 675.07 12/19/2005 10.80 674.18 8/21 /2006 12.09 672.89 9/24/2007 11.21 673.77 New TOC elevation; survey data pending 3/11/2009 4.38 NA 3/29/2010 3.23 NA 11/1/2011 4.45 NA 11/16/2012 5.65 NA 12/12/2013 5.22 NA 12/9/2014 7.10 NA New Survey 684.07 686.68 10/28/2015 4.84 681.84 11/15/2016 5.31 681.37 10/12/2017 8.89 677.79 11 /5/2018 4.70 681.98 9/17/2019 6.77 679.91 PW-16S 12.5 5.5-12.5 677.67-670.67 680.97 683.17 10/30/2000 8.00 675.17 12/20/2000 7.39 675.78 9/5/2001 9.82 673.35 9/17/2002 9.65 673.52 9/11/2003 6.56 676.61 8/16/2004 6.79 676.38 12/19/2005 6.21 676.96 8/21 /2006 8.44 674.73 9/24/2007 11.83 671.34 New TOC elevation; survey data pending 3/11/2009 4.93 NA 3/29/2010 4.10 NA 11/1/2011 4.64 NA 11/16/2012 5.96 NA TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 19 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) PW-17 100 85 - 100 686.0 - 671.0 771.0 774.7 11/14/2000 43.25 731.45 12/20/2000 43.96 730.74 9/5/2001 45.55 729.15 9/16/2002 49.34 725.36 9/11/2003 37.64 737.06 8/16/2004 39.42 735.28 12/19/2005 21.09 753.61 8/21 /2006 43.19 731.51 9/24/2007 42.02 732.68 2/23/2009 42.50 732.20 3/29/2010 38.20 736.50 11/1/2011 43.50 731.20 11/16/2012 42.40 732.30 PW-18 225 210 - 225 525.4 - 510.4 735.4 737.8 11/9/2000 110.06 627.74 12/7/2000 57.23 680.57 12/14/2000 57.28 680.52 12/20/2000 57.27 680.53 9/5/2001 58.50 679.30 9/17/2002 NM NM 9/11/2003 86.31? Suspect data 8/16/2004 53.18 684.62 12/19/2005 NM NM 8/21 /2006 39.32 698.48 9/24/2007 34.56 703.24 3/11/2009 37.43 700.37 3/29/2010 30.22 707.58 11/1/2011 36.15 701.65 11/16/2012 35.04 702.76 12/12/2013 34.75 703.05 12/9/2014 33.80 704.00 New Survey 734.02 736.44 10/26/2015 36.68 699.76 11/15/2016 30.73 705.71 10/16/2017 33.24 703.20 11 /7/2018 32.70 703.74 NM PW-19 260 235-250 516.6 - 501.6 751.6 754.1 11/5/2001 75.70 678.40 9/17/2002 60.16 693.94 9/11/2003 94.56? Suspect data 9/11/2003 52.75 701.35 8/16/2004 53.18 700.92 12/19/2005 54.11 699.99 8/21 /2006 54.50 699.60 9/24/007 54.15 699.95 2/25/2009 52.18 701.92 3/29/2010 50.65 703.45 11/1/2011 NM 11/16/2012 NM TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 20 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) W-1 64.7 53.7-64.7 719.05-708.05 772.20 772.75 11/14/2000 42.08 730.67 9/4/2001 24.12 748.63 9/17/2002 48.07 724.68 9/11/2003 36.39 736.36 8/16/2004 38.00 734.75 12/19/2005 40.78 731.97 8/21 /2006 41.87 730.88 2/23/2009 41.63 731.12 3/29/2010 37.13 735.62 11/1/2011 41.53 731.22 11/16/2012 41.00 731.75 W-2 35 23-35 703-691 723.30 726.00 11/14/2000 16.51 709.49 9/4/2001 17.33 708.67 9/17/2002 18.35 707.65 9/11/2003 12.62 713.38 8/16/2004 14.05 711.95 8/21 /2006 18.56 707.44 9/224/07 16.30 709.70 2/23/2009 15.54 710.46 3/29/2010 14.75 711.25 11 /1 /2011 16.43 709.57 11/16/2012 18.10 707.90 W-4 19 9-19 703.64-693.64 710.30 712.64 11/14/2000 9.49 703.15 9/4/2001 9.84 702.80 9/17/2002 8.57 704.07 9/11/2003 6.71 705.93 8/16/2004 6.28 706.36 12/19/2005 7.74 704.90 8/21 /2006 9.09 703.55 9/24/2007 9.94 702.70 2/23/2009 6.22 706.42 3/29/2010 5.80 706.84 11 /1 /2011 6.69 705.95 11/16/2012 9.35 703.29 W-4A 38.5 28.5-38.5 684.75-674.75 712.00 713.25 11/14/2000 9.77 703.48 9/4/2001 10.12 703.13 9/17/2002 9.00 704.25 9/11/2003 7.58 705.67 8/16/2004 6.87 706.38 12/19/2005 6.91 706.34 8/21 /2006 9.49 703.76 9/24/2007 10.08 703.17 2/23/2009 6.92 706.33 3/29/2010 5.83 707.42 11 /1 /2011 6.82 706.43 11/16/2012 9.57 703.68 12/17/2013 7.39 705.86 12./8/2014 14.76 698.49 New Survey 709.86 712.64 10/27/2015 9.93 702.71 11/16/2016 11.07 701.57 10/11/2017 12.93 699.71 10/31 /2018 6.72 705.92 9/11/2019 17.60 695.04 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 21 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) W-413 50 52.7 711.70 713.93 11/14/2000 10.71 703.22 9/4/2001 11.11 702.82 9/17/2002 10.27 703.66 9/11/2003 NM NM 8/16/2004 7.90 706.03 12/19/2005 7.79 706.14 8/21 /2006 10.59 703.34 9/24/2007 11.00 702.93 2/23/2009 6.50 707.43 3/29/2010 5.78 708.15 11/1/2011 7.58 706.35 11/16/2012 10.50 703.43 W-5 60 50-60 702.06-692.06 750.86 752.06 11/14/2000 32.28 719.78 9/4/2001 33.84 718.22 9/17/2002 38.61 713.45 9/11/2003 26.85 725.21 8/16/2004 29.64 722.42 12/19/2005 32.30 719.76 8/21 /2006 33.11 718.95 9/24/2007 32.50 719.56 2/23/2009 31.97 720.09 3/29/2010 27.64 724.42 11/1/2011 32.63 719.43 11/16/2012 32.35 719.71 W-6 57 42-57 701.8-686.8 742.17 743.80 11/14/2000 30.43 713.37 9/4/2001 31.59 712.21 9/17/2002 35.47 708.33 9/11/2003 22.78 721.02 8/16/2004 27.95 715.85 12/19/2005 30.36 713.44 8/21 /2006 30.81 712.99 9/24/2007 29.86 713.94 2/23/2009 28.53 715.27 3/29/2010 24.32 719.48 11/1/2011 30.13 713.67 11/16/2012 30.15 713.65 W-6A 90 80-90 664.9-654.9 742.91 744.90 11/14/2000 32.45 712.45 9/4/2001 33.70 711.20 9/17/2002 36.67 708.23 9/11/2003 24.62 720.28 8/16/2004 30.20 714.70 12/19/2005 32.51 712.39 8/21 /2006 32.85 712.05 9/24/2007 32.15 712.75 2/23/2009 30.39 714.51 3/29/2010 26.17 718.73 11/1/2011 32.99 711.91 11/16/2012 33.17 711.73 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 22 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) W-613 35 20-35 724.39-709.39 743.13 744.39 11/14/2000 29.75 714.64 9/4/2001 30.98 713.41 9/17/2002 33.71 710.68 9/11/2003 22.34 722.05 8/16/2004 27.00 717.39 12/19/2005 29.44 714.95 8/21/2006 29.97 714.42 9/24/2007 28.86 715.53 2/23/2009 27.99 716.40 3/29/2010 23.70 720.69 11/1/2011 28.03 716.36 11/16/2012 27.33 717.06 W-12 60 50-60 685.84-675.84 734.14 735.84 12/19/2005 21.65 714.19 8/21/2006 NM NM 9/24/2007 20.96 714.88 2/23/2009 19.83 716.01 3/29/2010 15.45 720.39 11/1/2011 21.26 714.58 11/16/2012 21.30 714.54 W-12A 25 10-25 725.74-710.74 733.62 735.74 12/19/2005 21.61 714.13 8/21/2006 NM NM 9/24/2007 NM NM 2/23/2009 20.19 715.55 3/29/2010 15.93 719.81 11/1/2011 21.71 714.03 11/16/2012 21.50 714.24 W-13 20 10-20 744.4-734.7 752.40 754.70 11/14/2000 DRY -- 9/4/2001 DRY 9/17/2002 DRY -- 9/11/2003 24.25 730.45 8/16/2004 14.30 740.40 8/21/2006 DRY -- 2/23/2009 35.97 718.73 3/29/2010 4.30 750.40 11/1/2011 18.61 736.09 11/16/2012 dry W-14 23 8-23 715.9-700.9 721.3 723.90 12/19/2005 16.68 707.22 8/21/2006 NM NM 9/24/2007 13.32 710.58 2/23/2009 3.52 720.38 3/29/2010 2.56 721.34 11/1/2011 11.72 712.18 11/16/2012 12.52 711.38 W-15 55 35-55 727.36-707.36 760.0 762.36 8/21/2006 NM NM 2/23/2009 NM NM 3/29/2010 NM NM 11/1/2011 40.96 721.40 11/16/2012 40.27 722.09 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 23 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) W-16 38 28-38 714.01-704.01 739.8 742.01 9/17/2002 29.73 712.28 9/11/2003 NM NM 8/16/2004 NM NM 8/21/2006 NM NM 2/23/2009 22.53 719.48 3/29/2010 18.42 723.59 11/1/2011 23.69 718.32 11/16/2012 23.62 718.39 W-17 20.5 23 687.44 708.4 710.44 12/19/2005 6.97 703.47 8/21/2006 9.40 701.04 9/24/2007 11.00 699.44 2/23/2009 7.80 702.64 3/29/2010 4.62 705.82 11/1/2011 9.86 700.58 11/16/2012 10.20 700.24 W-18 41.5 31.5-41.5 722.21-712.21 751.4 753.71 12/19/2005 35.01 718.70 8/21/2006 36.45 717.26 9/24/2007 37.10 716.61 2/23/2009 36.08 717.63 3/29/2010 33.81 719.90 11/1/2011 36.69 717.02 11/16/2012 37.55 716.16 W-19 40 30-40 717.33-707.33 744.3 747.33 8/21/2006 NM NM 9/24/2007 29.14 718.19 2/23/2009 28.75 718.58 3/29/2010 24.68 722.65 11/1/2011 29.22 718.11 11/16/2012 29.00 718.33 W-20 10 5-10 712.24-707.24 715.14 717.24 12/19/2005 5.14 712.10 8/21/2006 6.65 710.59 9/24/2007 7.10 710.14 2/23/2009 4.59 712.65 3/29/2010 4.05 713.19 11/1/2011 7.01 710.23 11/16/2012 7.61 709.63 W-21 33.4 33.4 684.78 716.00 718.18 11/14/2000 15.73 702.45 9/4/2001 16.41 701.77 9/17/2002 17.15 701.03 9/11/2003 14.00 704.18 8/16/2004 14.94 703.24 12/19/2005 14.18 704.00 8/21/2006 15.59 702.59 9/24/2007 15.91 702.27 2/23/2009 14.60 703.58 3/29/2010 9.48 708.70 11/1/2011 15.02 703.16 11/16/2012 15.70 702.48 TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 24 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) W-23A 75 65-75 707.66-697.66 770.18 772.66 11/14/2000 41.41 731.25 9/4/2001 42.91 729.75 9/17/2002 45.30 727.36 9/11/2003 31.29 741.37 8/16/2004 38.17 734.49 12/19/2005 42.06 730.60 8/21/2006 40.94 731.72 9/24/2007 42.30 730.36 2/23/2009 40.10 732.56 3/29/2010 36.44 736.22 11/1/2011 41.74 730.92 11/16/2012 41.65 731.01 W-23B 55 40-55 731.89-716.89 769.60 771.89 11/14/2000 41.00 730.89 9/4/2001 42.37 729.52 9/17/2002 44.54 727.35 9/11/2003 31.29 740.60 8/16/2004 37.45 734.44 12/19/2005 41.29 730.60 8/21/2006 40.42 731.47 9/24/2007 42.57 729.32 2/23/2009 39.55 732.34 3/29/2010 35.74 736.15 11/1/2011 41.01 730.88 11/16/2012 41.40 730.49 W-24 60 45-60 721.14-706.14 765.80 766.14 11/14/2000 40.45 725.69 9/4/2001 42.61 723.53 9/17/2002 NM -- 9/11/2003 NM 8/16/2004 NM 12/19/2005 NM 8/21/2006 NM 2/23/2009 NM 3/29/2010 NM 11/1/2011 NM 11/16/2012 NM NM W-25 58 43-58 727.27-712.27 770.80 770.27 11/14/2000 40.58 729.69 9/4/2001 42.47 727.80 9/17/2002 46.25 724.02 9/11/2003 35.75 734.52 8/16/2004 NM NM 12/19/2005 NM NM 8/21/2006 NM NM 2/23/2009 NM NM 3/29/2010 NM NM 11/1/2011 NM NM 11/16/2012 NM NM TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 25 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) W-26 53 38-53 721.65-706.65 759.20 759.65 11/14/2000 NM NM 9/4/2001 NM NM 9/17/2002 40.62 719.03 9/11/2003 NM NM 8/16/2004 NM NM 8/21/2006 NM NM 2/23/2009 NM NM 3/29/2010 NM NM 11/1/2011 NM NM 11/16/2012 NM NM W-27 58.5 43.5-58.5 721.7-706.7 765.50 765.20 11/14/2000 39.86 725.34 9/4/2001 41.37 723.83 9/17/02 NM NM 9/11/2003 NM NM 8/16/2004 NM NM 8/21/2006 NM NM 2/23/2009 NM NM 3/29/2010 NM NM 11/1/2011 39.05 726.15 11/16/2012 37.61 727.59 W-29 49.5 34.5-49.5 715.69-700.69 750.74 750.19 11/14/2000 28.22 721.97 9/4/2001 29.68 720.51 9/17/2002 28.01 722.18 9/11/2003 NM NM 8/16/2004 NM NM 8/21/2006 NM NM 2/23/2009 NM NM 3/29/2010 NM NM 11/1/2011 NM NM 11/16/2012 NM NM W-30 53 38-53 722.77-707.77 761.00 760.77 11/14/2000 34.47 726.30 9/4/2001 36.59 724.18 9/17/2002 40.16 720.61 9/11/2003 30.37 730.40 8/16/2004 NM NM 12/19/2005 NM NM 8/21/2006 34.92 725.85 9/24/2007 33.67 727.10 2/23/2009 32.79 727.98 3/29/2010 28.64 732.13 11/1/2011 33.73 727.04 11/16/2012 33.58 727.19 RW-NIS1 40 20-40 12/19/2005 10.51 -- 2/23/2009 9.43 -- 3/29/2010 8.72 -- 11/1/2011 3.79 -- 11/16/2012 5.57 RW-SIS1 50 30-50 12/19/2005 11.59 2/23/2009 NM -- 3/29/2010 NM -- 11/1/2011 NM -- 11/16/2012 NM TABLE 1 GROUND WATER ELEVATION DATA SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE JAMESTOWN, NORTH CAROLINA Page 26 of 26 TOP OF GROUND TOTAL SCREENED INTERVAL GROUND CASING DEPTH TO WATER Depth Elevation MONITOR DEPTH ELEVATION ELEVATION GAUGING WATER ELEVATION WELL I.D. (feet BGL) (feet BGL) (feet MSL) (feet MSL) (feet MSL) DATE (feet BTOC) (feet MSL) RW-SIS2 40 20-40 12/19/2005 6.48 2/23/2009 7.47 -- 3/29/2010 6.98 -- 11/1/2011 6.11 -- 11/16/2012 8.84 RW-SIS3 40 20-40 713.60 12/19/2005 6.67 706.93 2/23/2009 5.15 708.45 3/29/2010 4.05 709.55 11/1/2011 4.82 708.78 11/16/2012 5.43 708.17 RW-SIS4 45 1545 713.16 12/19/2005 4.38 708.78 2/23/2009 9.99 703.17 3/29/2010 2.51 710.65 11/1/2011 4.27 708.89 11/16/2012 4.00 709.16 RW-SIS5 12/19/2005 9.22 -- 2/23/2009 9.22 3/29/2010 5.50 11/1/2011 9.56 11/16/2012 8.50 RW-SIS6 12/19/2005 5.28 2/23/2009 6.15 3/29/2010 4.70 11/1/2011 5.73 -- 11/16/2012 6.70 RW-LFS1 50 30-50 696.44 12/19/2005 14.71 681.73 2/23/2009 12.09 684.35 3/29/2010 10.97 685.47 11/1/2011 11.88 684.56 11/16/2012 11.74 684.70 RW-LFS2 50 30-50 697.48 12/19/2005 19.39 678.09 2/23/2009 13.16 684.32 3/29/2010 12.05 685.43 11/1/2011 13.49 683.99 11/16/2012 12.96 684.52 NM = Not measured BGL = Below ground level MSL = Mean sea level BTOC = Below top of well casing TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 1 of 14 VOLATILE ORGANIC COMPOUNDS (ug/L) i i 0 c> y su °1 y Sample i i N b o ^' CD ^' Sample I.D. Date �. �. b 0 q 0 b 0 a 3 3 n n n 3 b c, m c, o S n S S S S i (D O S O S 3 F n S S_ n S 3 O O O O O O A y p O S p O `G fD O O O 3 S O O O O Do n a a 0 0 0 OO N CD fD (D . O O O n (D O S M M O M fD (D O (DD (D S _ M <S O S -a x N S S N S O O 0 2) 3 0) 3 a) 3 (D 3 a) 3 a) 3 a) 3 O 3 (D 3 CL CND 3 a) 3 c) 3 CD 3 CD 3 M CD 3 M 3 fD 3 CD 3 O. m n fp CD CD fD fD fD fD fD M fD M fD fD fD fD fD fD CD M fD CD fD to NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 MW-1 1/28/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3/5/2009 17 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 15.3 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.1 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 3/31/2010 0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11/2/2011 0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <3.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 11/20/2012 54 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 54.4 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 1/21/2013 ND <2.0 12/9/2013 ND <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 ND 12/8/2014 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/26/2015 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 11/14/2016 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/11/2017 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 11/1/2018 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 9/10/2019 ND <1 <1 <1 <1 <1 I <1 <2 I <20 <1 <1 I <1 <1 <1 <1 <1 <1 <1 <1 <1 I <1 <1 <1 <3 I ND MW-2A 1/24/1997 4 4 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND MW-2C 1/24/1997 620 160 ND 260 98.0 30.0 ND ND ND 7 J ND 3 J 10 J ND ND ND ND 6 J ND ND 13.0 31.0 ND 2.0 7/15/1998 600 ND 100 290 D 140 ND ND ND ND 5.0 ND ND ND ND ND ND ND 6.0 ND ND 9.0 50.0 ND ND 2/24/2009 102 <1.0 <1.0 41.1 <1.0 2.8 <1.0 49 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.8 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 4.9 <2.0 ND MW-3A 8/6/1996 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1/29/1997 24 ND ND ND ND ND ND ND ND 3 J ND 15 ND ND ND ND ND ND ND ND ND ND ND 6 MW-3B 7/15/1998 139 ND ND ND ND ND ND 120 J ND 3 J 14 2 J ND ND ND ND ND ND ND ND ND ND ND 9/26/2000 186 <5 <5 <5 <5 <5 <5 160 NA <5 26 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 139 <5 <5 <5 <5 <5 <5 126 <10 <5 12.6 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND MW-3C 8/6/1996 273 11 ND 150 31 5.0 ND ND 6 37 ND ND ND ND 2 J 4J ND ND 14 13 ND ND 1/28/1997 197 6 ND 92 21 3.0 ND ND ND ND 41 14 ND NA ND 1 J ND ND ND 9 10.0 ND ND 9/26/2000 138 <5 <5 41 7.2 <5 <5 <100 NA <5 32 <10 <5 21 <5 <5 <5 37 <5 <5 <10 <10 ND 9/5/2001 178 <5 <5 22.6 <5 <5 <5 117 <10 <5 24.2 <10 <5 14.6 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/18/2002 152 <5 <5 18.4 <5 <5 <5 94.6 <10 <5 27.3 <10 <5 12 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2003 103 <5 <5 <5 <5 <5 <5 90 <10 <5 13.4 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/17/2004 132 <5 <5 19.4 <5 <5 <5 71 <10 <5 30.0 <10 <5 12.4 <5 <5 <5 <5 <5 <5 <10 <5 ND 2/27/2009 589 <1.0 <1.0 104 20.3 4.4 <1.0 160 <5.0 3.0 <1.0 151 32.7 <1.0 <1.0 70.1 <1.0 <1.0 1.9 <1.0 <1.0 2.5 39.4 <2.0 ND 3/30/2010 863 <1.0 <1.0 161 32.4 6.31 <1.0 186 <5.0 3.92 <1.0 249 45.7 <1.0 <1.0 108 <1.0 4.87 1.71 <1.0 <1.0 2.71 61 ND ND 11/1/2011 1,861 29.1 <0.5 396 144 14 <0.5 80 <0.5 9.94 <0.5 459 192 <0.5 <0.5 364 <0.5 <0.5 3.09 <0.5 1.15 8.74 157 <0.5 3.26 11 /20/2012 1,798 28.5 <0.5 361 106 <0.5 <0.5 268 <0.5 8.73 <0.5 386 150 <0.5 <0.5 314 <0.5 4.30 3.83 1.26 1.40 8.36 146 0.7 10.31 12/11/2013 2,268 18.6 <5 383 107 15 <5 549 <50 9 <5 559 137 <5 <5 318 <5 <5 <5 <5 <5 <5 173 <5 ND 12/11/2014 2,051 100 <1 290 170 <1 <1 311 <5.0 12 17.0 330 60 <1 <1 620 <1 <1 <1 <1 <1 11 130 <3 ND 10/27/2015 1,262 66 <1 210 100 <1 <1 308 >50 10 <1 350 40 <1 <1 410 <1 <1 <1 <1 <1 9.4 J 67 <30 ND 11/14/2016 872 67 <10 94 56 <10 <10 190 <10 5.4 J 12.0 150 <10 <10 <10 270 <10 <10 <10 <10 <10 6.0 27 <30 ND 10/10/2017 402 15 <1 57 22 1.8 <1 120 <20 2.2 <1 49 6.2 J <1 <1 100 <1 <1 0.81 J <1 0.73 J 2.0 31 <3 1.70 11/2/2018 414 6 <1 54 30 1.9 <1 110 <20 3.2 <1 66 6.3 <1 <1 110 <1 <1 0.62 J <1 0.61 J 2.3 22 <3 2.60 9/11/2019 288 <10 <10 41 17 <10 <10 94 <200 <10 <10 50 <10 <10 <10 72 <10 <10 <10 <10 <10 <10 14 <30 ND MW-4 1/27/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND MW-5 2/24/2009 19 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 18.6 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 2 of 14 n v; Sample iv N b p N CD N Sample I.D. �. �. b q b F 3 n n v 3 ,� �, v x Date 0 0 0 0 0 3- n 3 c, m 0 c, 0 _<, � S S 3- 3- S 0 0 3- n O S S S S_ 3' 3 (DD O O O O O O O A y p O S O O K fD O O O 3 S C) 0 0 O' 0 0 0 W 0 a 0 0 a n 0 0 /� ♦/ N fD N .. fD .. (D O a O O (D O 3 S O 3 (DD O M O 3 S fOD a O_ fOD .. fOD .. S_ : C O S S S S S -a x .r N O N S O S S N O S C S S O O O 0 D) 3 D) 3 N 3 M 3 D) 3 D) 3 D) 3 O 3 (D 3 0: fD 3 N 3 D) 3 fD 3 fD 3 a CD 3 M 3 fD 3 M 3 3 O. Iv 0 fp fD CD fD M fD fD fD M fD M fD fD fD fD fD CD M M fD M (D U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 MW-6 1/27/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND NA ND ND ND ND ND ND ND ND ND 9/26/2000 ND <5 <5 <5 <5 <5 <5 <100 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 40 <5 <5 <5 <5 <5 <5 40.2 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 24 <5 <5 <5 <5 <5 <5 24.4 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/22/2003 16 <5 <5 <5 <5 <5 <5 15.8 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/18/2004 14 <5 <5 <5 <5 <5 <5 13.8 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/3/2009 75 <1.0 <1.0 5.9 <1.0 <1.0 <1.0 36.8 16.2 <1.0 <1.0 1.0 <1.0 <1.0 <1.0 6.3 <1.0 2.4 2.9 <1.0 <1.0 1.6 2.0 <2.0 ND 3/30/2010 73 <1.0 <1.0 7.99 <1.0 <1.0 <1.0 47.9 <5.0 <1.0 <1.0 1.21 <1.0 <1.0 <1.0 7.47 <1.0 2.51 1.86 <1.0 <1.0 1.44 2.13 ND ND 11/1/2011 57 <0.5 <0.5 12.9 1.84 <0.5 <0.5 18.0 <0.5 <0.5 <0.5 3.86 2.58 <0.5 <0.5 11 <0.5 <0.5 0.52 <0.5 <0.5 1.92 3.66 <0.5 0.63 11/19/2012 58 <0.5 <0.5 13.2 <0.5 <0.5 <0.5 19.7 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 14 <0.5 <0.5 1.86 <0.5 0.68 2.46 4.87 <0.5 0.76 12/11/2013 48 <5 <5 13.8 <5 <5 <5 12.3 <50 <5 <5 6.50 <5 <5 <5 16 <5 <5 <5 <5 <5 <5 <5 <10 ND 12/12/2014 101 <1 <1 13 0.47 J <1 <1 58.4 <5 0.96 J <1 2.2 3.8 <1 <1 14 <1 <1 1.9 <1 0.65 J 1.7 4.7 <3 1.2 10/30/2015 69 <1 <1 10 <1 <1 <1 44.8 <5 0.63 J <1 2.0 J 2.2 J <1 <1 8.3 <1 <1 0.99 J <1 <1 1.2 3.2 <3 1.5 11/17/2016 90 <1 <1 12 <1 <1 <1 59 <20 0.74 J <1 1.9 J 2.1 J <1 <1 11 <1 <1 1.6 <1 0.56 J 1.6 3.2 <3 1.4 10/10/2017 53 <1 <1 7 <1 <1 <1 34 <20 15 J <1 1.7 J <1 <1 <1 6 <1 <1 <1 <1 <1 4.2 2.0 <3 ND 11/2/2018 118 <1 <1 12 <1 <1 <1 82 <20 0.63 J <1 2.7 2.1 <1 <1 13 <1 <1 0.79 J <1 0.54 J 1.1 3.3 <3 1.6 9/12/2019 67 <1 <1 5.4 <1 <1 <1 29 27.0 0.45 J <1 <1 <1 <1 <1 4.2 <1 <1 <1 <1 <1 <1 1.1 <3 ND MW-7B 3/3/2009 244,324 2,630 <100X 25,800 10,100 9,760 <100X 28,900 12,000 <100X <100X 39,500 2,450 <100X <100X 36,100 181 48,100 522 6,020 <100X 251 15,800 1,740 4,470 MW-8 1/28/1997 119 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2 J 96 4.0 3/5/2009 47 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 10.8 15.2 6.6 <1.0 10.8 <1.0 <1.0 <1.0 <1.0 <1.0 3.3 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND MW-9 1/28/1997 1 ND ND ND ND ND ND ND ND 1 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND DUP-1 (MW-9) 1/28/1997 2 ND ND ND ND ND ND ND ND 2 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND 2/26/2009 182 <1.0 <1.0 1.5 <1.0 <1.0 <1.0 168 6.0 <1.0 <1.0 2.7 2.0 <1.0 <1.0 2.1 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND MW-10 1/27/1997 126 ND ND 6 ND ND ND 120 ND 2 J ND ND ND ND ND ND ND ND 1 J ND ND ND 7/14/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9/26/2000 258 <5 <5 7.6 <5 <5 <5 250 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 335 <5 <5 <5 <5 <5 <5 335 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 234 <5 <5 <5 <5 <5 <5 234 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 221 <5 <5 <5 <5 <5 <5 221 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/19/2004 198 <5 <5 <5 <5 <5 <5 198 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/6/2009 176 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 162 6.4 1.1 <1.0 4.1 <1.0 <1.0 <1.0 <1.0 <1.0 2.2 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 3/29/2010 184 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 166 10.6 <1.0 <1.0 3.82 1.26 <1.0 <1.0 <1.0 <1.0 2.31 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11/1/2011 56 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 47 <0.5 <0.5 <0.5 3.99 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 6.45 11/19/2012 148 <5 74 <5 <5 <5 <5 74.4 <50 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 ND 12/10/2013 33 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 28.1 <5 <0.5 <0.5 2.27 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 2.7 12/10/2014 137 <1 <1 <1 <1 <1 <1 133 <5 <1 <1 2.6 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 1.2 10/26/2015 104 <1 <1 <1 <1 <1 <1 103 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 1.1 11/14/2016 130 <1 <1 <1 <1 <1 <1 130 <20 0.78 J <1 2.8 J <1 <1 <1 0.41 J <1 <1 <1 <1 <1 <1 <1 <3 ND 10/10/2017 150 <1 <1 <1 <1 <1 <1 150 <20 <1 <1 <1 1.8 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/31/2018 160 <1 <1 <1 <1 <1 <1 160 <20 <1 <1 0.93 J 1.1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 9/10/2019 74 <1 <1 <1 <1 <1 <1 72 <20 <1 <1 1.5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND MW-11 1/23/1997 84 5 J ND 4 J 3 J ND ND ND ND 4 J 9 ND ND NA 10 ND ND ND ND ND ND 2 J 47 9/28/2000 298 <5 <5 <5 <5 <5 <5 270 NA 8.6 12 <10 <5 <5 <5 7.7 <5 <5 <5 <5 <10 <10 ND 9/10/2001 314 <5 <5 <5 <5 <5 <5 288 <10 10.6 15.3 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/18/2002 434 <5 <5 <5 <5 <5 <5 283 <10 11.1 13.7 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 126 9/19/2003 118 <5 <5 <5 <5 <5 <5 94.2 <10 7.4 16.8 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/17/2004 120 <5 <5 <5 <5 <5 <5 94.1 <10 11.5 14.4 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/4/2009 74 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 39.8 11.6 5.4 <1.0 15.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.7 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 3 of 14 n v; Sample iv N b p N CDN Sample I.D. Date �. �. b 0 q 0 b 0 F 3 n 3- n n 3 v c, m 3 v c, o S n S 3- 3- 3- p 3- O 3- S F n n O O O O O O 3A y p O S O O K fD O O O S C) 0 0 O' o o n W n a ' ' a n ' 0 /� ♦/ N CD C N .. fD .. K CD ,. fD ,. O O �p O 3 S M 3 (D O M fD 3 S fOD a O_ fOD fOD S O S S S S S -a x .r N O N S O S S N O S C S S O O O 0 D) 3 D) 3 N 3 M 3 D) 3 D) 3 D) 3 O 3 (D 3 CL fD 3 N 3 D) 3 fD 3 fD 3 a CD 3 M 3 fD 3 CD 3 3 O. m n fp fD CD fD M fD fD CD I M fD M fD fD fD fD I fD CD CD M fD M (D 1 U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 MW-12A 1/23/1997 11 2 J ND ND 3 J ND ND ND ND 2 J ND ND ND ND ND ND 2 J ND 2 J ND ND ND 7/10/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/30/2000 ND <5 <5 <5 <5 <5 <5 <100 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 12 <5 <5 <5 <5 <5 <5 <10 12.3 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/20/2002 27 <5 <5 <5 <5 <5 <5 11.7 14.9 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 28 <5 <5 <5 <5 <5 <5 11.9 15.6 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/18/2004 44 <5 <5 <5 <5 <5 <5 <10 43.7 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/6/2009 40 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 38.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.9 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 4/1/2010 6 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.50 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.09 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11 /2/2011 38 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 29.0 <5 <0.5 <0.5 8.04 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.61 11/19/2012 203 <5 <5 <5 <5 <5 <5 203 <50 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 ND 12/10/2013 210 <5 <5 <5 <5 <5 <5 210 <50 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 ND 12/11/2014 226 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 210 8.3 <1.0 <1.0 5.6 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <3 1.7 10/27/2015 213 <1 <1 <1 <1 <1 <1 200 <5 <1 <1 11 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 2.2 11/14/2016 207 <1 <1 <1 <1 <1 <1 200 19 J <1 <1 5.9 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 1.5 10/10/2017 273 <1 <1 <1 <1 <1 <1 260 <20 <1 <1 11 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 1.7 11/1/2018 93 <1 <1 <1 <1 <1 <1 79 <20 <1 <1 11 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 2.9 9/10/2019 189 <1 <1 <1 <1 <1 <1 180 16 J <1 <1 6.2 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 2.9 MW-12B 1/23/1997 16 6 ND 2 J ND ND ND ND ND ND 8.0 ND ND ND ND ND ND ND ND ND ND ND 7/10/1998 11 ND ND ND ND ND ND ND ND ND 11 ND ND ND ND ND ND ND ND ND ND ND 9/28/2000 567 <5 <5 <5 <5 <5 <5 510 <5 18 <10 <5 11.0 <5 28 <5 <5 <5 <5 <10 <10 ND 9/6/2001 371 <5 <5 <5 <5 <5 <5 359 <10 <5 12 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/20/2002 221 <5 <5 <5 <5 <5 <5 211 <10 <5 10.2 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 262 <5 <5 <5 <5 <5 <5 250 <10 <5 12.4 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/18/2004 196 <5 <5 <5 <5 <5 <5 182 <10 <5 13.7 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/4/2009 224 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 199 17.6 <1.0 <1.0 5.8 <1.0 <1.0 <1.0 <1.0 <1.0 1.5 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 4/9/2010 191 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 176 12.6 <1.0 <1.0 2.50 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11 /2/2011 62 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 43 <5 <0.5 <0.5 13.0 <0.5 <0.5 <0.5 3.6 <0.5 <0.5 <0.5 <0.5 <0.5 1.5 <0.5 <0.5 1.1 11/19/2012 69 <10 <10 <10 <10 <10 <10 68.5 <100 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 ND 12/10/2013 83 <5 <5 <5 <5 <5 <5 71.4 <50 <5 <5 11.3 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 ND 12/11/2014 158 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 132 6.3 0.64 J <1.0 12.0 <1.0 <1.0 <1.0 3.4 <1.0 <1.0 <1.0 <1.0 <1.0 0.73 J <1.0 <3 4.2 10/27/2015 123 <1 <1 <1 <1 <1 <1 117 <5 <1 <1 4.7 <1 <1 <1 1.1 J <1 <1 <1 <1 <1 <1 <1 <3 ND 11/14/2016 164 <1 <1 <1 <1 <1 <1 150 <20 0.5 J <1 11.0 <1 <1 <1 2.7 J <1 <1 <1 <1 <1 0.58 J <1 <3 3.4 10/10/2017 181 <1 <1 <1 <1 <1 <1 170 <20 0.94 J <1 8.3 <1 <1 <1 2.3 J <1 <1 <1 <1 <1 0.61 J <1 <3 2.7 11/1/2018 112 <1 <1 <1 <1 <1 <1 95 <20 0.51 J <1 11 <1 <1 <1 2.7 <1 <1 <1 <1 <1 <1 <1 <3 3.1 9/11/2019 133 <1 <1 <1 <1 <1 <1 120 <20 0.48 J <1 10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 3.1 MW-12D 9/10/1998 ND ND ND ND ND ND ND ND ND ND ND NA NA ND ND ND NA ND ND ND ND 9/29/2000 132 <5 <5 <5 <5 <5 <5 120 NA <5 <5 <10 <5 <5 <5 12 <5 <5 <5 <5 <10 <10 ND 9/12/2001 54 <5 <5 <5 <5 <5 <5 14.4 39.6 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/20/2002 31 <5 <5 <5 <5 <5 <5 <10 21.9 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 9.5 10/22/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/5/2009 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 4/1/2010 6 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.58 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.15 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11/3/2011 11 <0.5 <0.5 0.99 <0.5 <0.5 <0.5 3.0 <5 <0.5 <0.5 2.22 <0.5 <0.5 <0.5 1.42 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 11/23/2012 79 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 77.6 <5 <0.5 <0.5 1.30 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 12/12/2013 ND <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 12/11/2014 1740 41 2.2 29 41 770 <1.0 5.3 5.3 12 6.3 480 <1.0 <1.0 <1.0 5 <1.0 66 47 32 <1.0 180 2.2 7.1 8.6 10/25/2015 ND <1 <1 <1 <1 <1 <1 4.29 J <5 <1 <1 1.1 J <1 <1 <1 0.49 J <1 <1 <1 <1 <1 0.56 J <1 <3 ND 11/18/2016 ND <1 <1 0.48 J 0.41 J <1 <1 4.9 J <20 <1 <1 0.76 J <1 <1 <1 0.79 J <1 <1 <1 <1 <1 <1 <1 <3 ND 10/11/2017 8 <1 <1 <1 <1 <1 <1 8.2 J <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 11/1/2018 16 <1 <1 0.82 J 1.4 <1 <1 7.2 <20 <1 <1 0.95 J <1 <1 <1 4.1 <1 <1 <1 <1 <1 1.8 1.5 <3 ND 9/11/2019 4 <10 <10 <10 <10 <10 <10 3.7 <200 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <30 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 4 of 14 �'71_ n v; Sample iv N b p N 3 CD N Sample I.D. Date �. �. b 0 q 0 b 0 � 3 n 3- n n 3 v c, m ,� �, v c, x � 0 S 0 S 3- 3- S 0 0 3- n O S S 0 S S_ 0 3' _<, 3 (DD O O O O O O O 3A y p O S O O K fD O O O 3 S 0 0 O' 0 0 0 W 0 a 0 0 a n 0 0 /� ♦/ N CD N .. fD .. (D O a O O M O 3 S O 3 (DD O M O 3 S fOD a O_ fOD a M fOD =r S_ - C O S D) S D) S N S M S D) -a D) x D) .+ O N (D O N fD S N O S D) S fD N fD O S CD C M S fD S M O 3 O O 0 3 3 3 3 3 3 3 3 3 0: 3 3 3 3 3 a 3 3 3 3 O. m n fA fD CD fD M fD fD M CD fD M fD fD fD fD fD CD CD M fD M (D U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 MW-14 8/6/1996 147 ND ND ND ND ND ND ND ND ND 140 ND ND ND ND ND ND ND ND 7 J ND ND 1/29/1997 2,118 ND ND 1 J ND ND ND 1,700 J ND 2 J ND 180 ND ND ND ND ND ND ND ND 3 J 7 J 1 J 46 MW-15A 1/30/1997 2,266 ND ND ND ND ND ND 1,700 ND 9 J ND 520 ND ND ND ND ND ND ND ND ND ND ND 37.0 9/5/2001 3,157 <5 <5 <5 <5 <5 <5 2,640 <10 <5 517 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/18/2002 2,140 <5 <5 <5 <5 <5 <5 1,500 <10 <5 635 <10 <5 5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/17/2003 2,424 <25 <25 <25 <25 <25 <25 1,910 <50 <25 514 <50 <25 <25 <25 <25 <25 <25 <25 <25 <50 <25 ND 8/18/2004 3,209 <25 <25 <25 <25 <25 <25 2,720 <50 <25 489 <50 <25 <25 <25 <25 <25 <25 <25 <25 <50 <25 ND 3/6/2009 2,238 <1.0 <1.0 <1.0 <1.0 <1.0 1.2 1,900 <5.0 <1.0 <1.0 335 <1.0 <1.0 <1.0 1.8 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 3/31/2010 1,211 <1.0 <1.0 <1.0 <1.0 <1.0 1.26 1,170 <5.0 <1.0 <1.0 32.7 <1.0 <1.0 <1.0 7.48 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11/2/2011 940 <0.5 <0.5 <0.5 <0.5 <0.5 1.23 480 <5 1.27 <0.5 430 <0.5 <0.5 <0.5 1.64 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.92 14.96 11/19/2012 2,324 <10 <10 <10 <10 <10 <10 1,920 <100 <10 <10 404 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 <10 ND 12/10/2013 3,308 <5 <5 <5 <5 <5 <5 2,950 <50 <5 <5 350 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 8.2 12/9/2014 2,405 <5 <5 <5 <5 <5 <5 1,970 <25 <5 <5 430 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <15 4.6 10/27/2015 2,159 <5 <5 <5 <5 <5 <5 1,740 <25 <5 <5 410 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <15 9.0 11/14/2016 2,334 <1 <1 <1 <1 <1 1.4 2,200 <20 0.49 J <1 110 <1 <1 <1 5.3 <1 <1 <1 <1 <1 0.45 J 0.93 J <3 17.3 10/11/2017 2,734 <1 <1 <1 <1 <1 1.8 2,600 <20 0.51 J <1 110 <1 <1 <1 5.8 <1 <1 <1 <1 <1 0.43 J 0.69 J <3 16.1 10/31/2018 1,796 <1 <1 <1 <1 <1 0.42 J 1,600 <20 0.67J <1 190 <1 <1 <1 0.45J <1 <1 <1 <1 <1 <1 <1 <3 6.2 9/10/2019 1,590 <5 <5 <5 <5 <5 <5 1,400 <100 <5 <5 190 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <15 ND MW-15B 1/30/1997 330 ND ND ND ND ND ND 210 J ND 1 J ND 110 ND ND ND ND ND ND ND ND ND ND ND 9.0 MW-16 1/21/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND MW-17 3/5/2009 305 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 258 30.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 5.8 <1.0 <1.0 1.7 <1.0 <1.0 5.9 3.2 <2.0 ND MRF-1 1/21/1997 63 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 63.0 ND ND ND 7/13/1998 53 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 53.0 ND ND ND 2/24/2009 65 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 28.3 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 6.9 <1.0 <1.0 <1.0 <1.0 <1.0 29.9 <1.0 <2.0 ND MRF-2 1/21/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND OW-NIS1 3/10/2009 214 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 180 9.9 <1.0 <1.0 20.6 <1.0 <1.0 <1.0 <1.0 <1.0 3.4 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND OW-DR1 9/28/2000 26,291 360 <5 4,300 1,000 150 <5 2,900 150 6,600 3,300 <5 4,100 33 310 18 420 26 14 2,400 210 ND OW-DR2 7/21/1998 11,612 400 J 1,500 D 480 J ND 3,400 J ND 150 2,900 D 1,100 D ND 40 J 460 J 22 ND 250 J 910 9/26/2000 25,240 460 <5 4,200 1,400 220 <5 4,900 NA 170 5,600 1,300 <5 3,500 25 120 19 260 77 28 2,800 161 ND 9/10/2001 27,394 695 <5 4,950 1,330 208 <5 3,450 <10 145 5,980 1,380 <5 5,700 27 107 36 271 11.3 27.8 2,880 196 ND 2/27/2009 25,306 1,230 7.3 3,550 1,580 141 1.3 4,180 46.8 113 <1.0 5,380 1,030 4.3 41.4 6,320 21.1 41.4 47.2 201 17.4 29.5 1,190 120 13.6 3/30/2010 24,982 1,330 <1.0 3,330 1,790 123 <5.0 3,910 <5.0 127 <1.0 5,510 1,090 <1.0 <1.0 6,400 <1.0 <1.0 <1.0 182 <1.0 <1.0 1,190 ND ND 11/1/2011 22,265 1,910 <25 3,000 2,050 121 <25 990 <250 101 <25 4,130 2,350 <25 <25 6,290 <25 <25 <25 153 <25 <25 1,100 38 32.0 11/23/2012 19,775 1,620 <50 2,230 1,430 <50 <50 2,180 <500 <50 <50 4,810 1,760 <50 <50 4,650 <50 <50 <50 177 <50 <50 918 <50 ND 12/11/2013 24,766 1,920 <50 2,730 1,920 120 <50 3,130 <500 154 <50 4,800 1,890 <50 <50 6,600 <50 <50 <50 172 <50 <50 1,330 <100 ND 12/12/2014 6,977 11 <100 19 15 3 <100 2,160 <5 1.1 1.8 4,500 <1.0 <1.0 <1.0 45 <100 <1.0 <100 160 <1.0 <100 13 48 ND 10/30/2015 12,595 720 <20 1,300 800 71 <20 1,630 <100 79 <20 3,400 480 <20 <20 3,200 <20 <20 24 95 14 J 22 750 24 J ND 11/18/2016 11,740 830 <20 1,300 860 150 <20 1,800 <400 65 <20 2,800 340 8.8 J <20 2,800 9.4 J <20 19 J 65 12 J 20 710 21 J ND 10/10/2017 4,103 100 <5 590 290 48 <5 990 <50 23 <100 920 45 <5 <5 840 <5 <5 5.9 5.4 4.7 J 5.4 240 4.5 J ND 11/2/2018 1,882 20 <10 250 110 16 <10 560 <200 8.9 J <10 380 13 <10 <10 430 <10 <10 <10 <10 <10 <10 94 <30 ND 9/11/2019 1,178 12 <5 200 84 11 <5 250 <100 7 <5 260 12 <5 <5 290 <5 <5 <5 <5 <5 <5 52 <15 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 5 of 14 �'71_ n v; Sample N N b 0 N N Sample I.D. Date �. �. b 0 q 0 b 0 F 3 n 3- n n 3 v c, m 3 ,� v c, 0 S 0 S 3- 3- 3- p 3- O 3- S F 0 S S_ 0 3' 3 O O O O O O 3A y 0 O S O O K fD O O O S C) 0 0 O' 0 0 0 W 0 a 0 0 a n 0 0 /� ♦/ N :D N .. fD .. (D O a O O M O 3 S O 3 (DD O M O 3 S fOD a O_ fOD .+ fOD .' S_ : C O S S S S S -a K .r N O N S O S S N O S C S S O O O 0 C) 3 D) 3 N 3 M 3 a) 3 a) 3 D) 3 O 3 M 3 0: N 3 N 3 D) 3 N 3 M 3 a CD 3 M 3 N 3 M 3 3 O. m n fp (D CD I M M N I N CD I M M fD I M M M fD I M CD fD M N M MU) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 OW-DR3 9/20/2002 3,989 <5 <5 221 <5 15.4 <5 1,050 <10 11.3 1,840 778 <5 8.9 <5 29.5 <5 <5 <5 <5 35.3 <5 ND 9/19/2003 2,815 <5 <5 201 <5 14.7 <5 690 <10 6.1 1,390 455 <5 11.1 <5 12 <5 <5 <5 <5 35.5 <5 ND 8/24/2004 4,403 <50 <50 452 <50 <50 <50 1,260 <100 <50 1,910 675 <50 <50 <50 <50 <50 <50 <50 <50 106 <50 ND 10/12/2004 3,438 <5 <5 353 <5 14.2 <5 916 <10 6.9 1,480 553 <5 26.2 <5 11.5 <5 <5 <5 <5 77.1 <5 ND 3/4/2009 2,184 <1.0 <1.0 251 5.3 25.1 <1.0 552 <5.0 3.3 <1.0 984 267 <1.0 5.8 38.7 <1.0 5.0 1.3 2.4 <1.0 2.6 40.6 <2.0 ND 11/26/2012 2,352 <0.5 <0.5 226 J 14.7 23.3 <0.5 471 <5 <0.5 <0.5 1,020 359 <0.5 <0.5 73.4 <0.5 5.5 2.06 2.16 1.21 6.55 92.8 0.61 279.57 12/10/2013 2,757 <5 <5 374 43.6 26.4 <5 793 <50 <5 <5 1,060 249 <5 <5 112.0 <5 <5 <5 <5 <5 7.70 85.3 <10 6.30 OW-DR4 9/23/2002 20,502 1,860 <5 4,320 2,010 226 <5 1,570 <10 121 323 282 <5 7,630 5.4 27.6 55.3 27.3 11.7 66.1 1,880 86.7 ND 9/22/2003 22,030 1,350 <50 4,850 1,860 181 <50 2,200 <100 107 562 311 <50 8,960 <50 <50 <50 <50 <50 65.4 1,530 53.5 ND 8/24/2004 20,516 1,840 <250 4,630 2,100 298 <250 1,480 <500 <250 608 <250 <250 7,880 <250 <250 <250 <250 <250 <250 1,680 <250 ND 10/12/2004 9,067 810 <5 3,110 1,230 167 <5 2,190 <10 77 353 <10 <5 <5 <5 <5 35.3 <5 18.8 39.3 987 50.0 ND 10/20/2004 20,733 1,700 <250 4,480 2,240 <250 <250 2,120 <500 <250 522 <500 <250 8,030 <250 <250 <250 <250 <250 <250 1,590 51.0 ND 2/25/2009 15,223 1,490 6.2 2,570 1,510 156 <1.0 1,300 56.0 96.4 <1.0 659 127 7.1 3.9 6,350 4.3 <1.0 44.9 12.9 17.7 96.3 677 38.5 ND OW-SIS-1 8/17/2004 9,885 1,770 6.0 768 1,580 201 <5 811 <10 95 111 <10 18.3 3,150 <5 160 215 <5 <5 774 213 12.8 ND 3/9/2009 16,834 2,820 11.6 1,280 2,950 256 <10.OX 1,360 107 180 <10.OX 179 54.1 29.6 <10.OX 5,200 <10.OX 146 412 <10.OX <10.OX 1,540 288 20.9 ND OW-SIS-2 2/24/2009 3,111 79.8 <1.0 579 277 26 <1.0 418 17.8 38.2 <1.0 29 14.8 <1.0 <1.0 1,030 4.9 356 3.8 36.1 2.1 3.9 167 28.2 ND OW-SIS-3 3/4/2009 41,840 9,110 14.4 4,320 4,640 172 2.7 2,540 158 167 <1.0 147 23.5 34.9 <1.0 13,600 46.2 3,330 103 132 72.6 1,620 1,400 207 ND OW -SR 3/9/2009 57,440 2,920 48.4 4,980 5,530 1,860 <10.OX 6,670 242 89.6 <10.OX 2,160 1,840 194 <10.OX 20,400 15.7 680 437 618 40.2 1,290 7,240 185 ND OW-LFS-1 2/26/2009 782 <1.0 <1.0 1.5 <1.0 <1.0 <1.0 723 12.8 4.5 <1.0 1 20.8 12.0 <1.0 <1.0 4.3 2.4 <1.0 <1.0 1.1 <1.0 <1.0 <1.0 <2.0 ND OW-LFS-2 2/26/2009 363 <1.0 <1.0 1.9 <1.0 <1.0 <1.0 329 9.0 2.4 <1.0 9.4 3.5 <1.0 <1.0 7.1 <1.0 <1.0 <1.0 <1.0 <1.0 1.1 <1.0 <2.0 ND 3/30/2010 281 <1.0 <1.0 2.33 <1.0 <1.0 <1.0 251 <5.0 2.17 <1.0 9.92 2.74 <1.0 <1.0 11.8 <1.0 <1.0 <1.0 <1.0 <1.0 1.15 <1.0 ND ND 11/1/2011 110 <0.5 <0.5 3.23 <0.5 <0.5 <0.5 65 <5 4.52 <0.5 10.1 1.90 <0.5 <0.5 20.7 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.3 <0.5 3.5 11/19/2012 276 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 274 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 2.12 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 12/11/2013 421 <5 <5 <5 <5 <5 <5 391 <50 <5 <5 <5 <5 <5 <5 29.6 <5 <5 <5 <5 <5 <5 <5 <10 ND 12/12/2014 306 <1.0 <1.0 1.9 <1.0 <1.0 <1.0 255 8.1 6.2 <1.0 15 3.8 <1.0 <1.0 12 <1.0 <1.0 <1.0 0.48 J <1.0 0.54 J 1.7 0.75 J 3.7 10/26/2015 285 <1.0 <1.0 1.8 J <1.0 <1.0 <1.0 253 <5 4.5 <1.0 11 <1.0 <1.0 <1.0 13 <1.0 <1.0 <1.0 <1.0 <1.0 0.93 J <1.0 0.45 J 3.4 11/14/2016 276 <1.0 <1.0 1.2 J <1.0 <1.0 <1.0 250 12 J 2.4 <1.0 11 0.76 J <1.0 <1.0 9 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <3 3.2 10/10/2017 248 <1 <1 1.1 J <1 <1 <1 240 <20 1.4 <1 4.6 1.5 J <1 <1 4.6 J <1 <1 <1 <1 <1 <1 <3 0.50 J 2.0 10/31/2018 404 <1 <1 <1 <1 <1 <1 360 <20 32.0 <1 9.3 1.3 <1 <1 0.80 J <1 <1 <1 <1 <1 <1 <1 <3 1.2 9/12/2019 213 <1 <1 0.8 J <1 <1 <1 210 <20 0.48 J <1 3.1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND PW-1 D 1/24/1997 659 ND ND 1 J 1 J ND ND 530 J ND ND 7 ND ND ND ND ND ND ND ND ND 120 ND ND ND 7/15/1998 110 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 110 ND ND ND PW-2D 2/7/1997 28 ND ND 10 ND ND ND ND 10 J ND ND ND 4 J ND ND ND 4 J ND ND ND ND ND ND ND 7/18/1998 11 ND ND 9 ND ND ND ND ND ND ND ND ND ND ND ND 2 J ND ND ND ND ND ND ND 2/26/2009 21 <1.0 <1.0 1.3 <1.0 <1.0 <1.0 1 19.5 <5.0 <1.0 I <1.0 <1.0 I <1.0 I <1.0 I <1.0 <1.0 I <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 6 of 14 �'71_ n v; Sample N N b 0 N N Sample I.D. �. �. b q b F 3 n n v 3 ,� v Date 0 0 0 0 0 3- n 3 c, m F 0 c, 0 S S 3- 3- 3- p 3- O 3- S S S_ 3' 3 Q O O O O O O A y p O S O O K fD O O O 3 S C) 0 0 O' 0 0 0 W 0 a 0 0 a n 0 0 /� ♦/ N fD N .. fD .. (D O a O O M O 3 3 O 3 (DD O M O 3 S fOD a O_ fOD .. fOD .. 3- : C O S S S S S -a K .r N O N S O S S N O S C S S O O O 0 D) 3 D) 3 N 3 M 3 a) 3 a) 3 D) 3 O 3 M 3 0: N 3 N 3 D) 3 N 3 M 3 a CD 3 M 3 N 3 M 3 3 a m 0 fp (D CD I M M N I N M M M fD I M M M N M CD CD M N M N 1 U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 - PW-3D 2/7/1997 42,680 4,100 ND 370 J 790 15,000 ND ND ND 260 J ND 16,000 ND ND ND ND 1,300 990 740 ND 3,600 ND ND 160 7/17/1998 21,462 ND 650 D ND 520 J 8,100 D ND ND ND 160 ND 8,600 3 J 2 J ND 13 680 610 D ND ND 2,000 D 54.0 49.0 21.0 4/9/2010 22,149 <1.0 <1.0 393 82.5 8,840 <1.0 39.8 18.4 5.46 <1.0 174 <1.0 <1.0 <1.0 36.1 <1.0 99.1 137.0 7.72 <1.0 419 11.6 ND ND 11/3/2011 damaged 11/27/2012 8,532 54 <50 293 203 4,830 <50 55 <500 <50 <50 2,150 <50 <50 <50 54.0 <50 <50 222 82 <50 589 <50 <50 ND 12/17/2013 27,696 993 9.0 491 1,180 12,800 <5 19.5 <50 137 <5 7,250 <5 <5 <5 59.4 <5 979 723 338 <5 2,540 58.4 12.3 106.5 12/11/2014 73,348 1,500 <200 610 2,800 14,000 <200 67.6 <100 310 240 32,000 <200 <200 <200 100 <200 1,100 8,900 1,300 <200 9,300 150 180 790 10/29/2015 67,602 2,300 <200 660 2,100 17,000 <200 112 <1000 350 <200 32,000 <200 <200 <200 380 86 J 1,000 3,300 1,400 <200 7,000 120 J >600 160 J 11/16/2016 45,170 970 <100 400 870 20,000 <100 120 <2000 190 <100 16,000 <100 <100 <100 110 <100 1,100 1,300 610 <100 3,500 <100 <300 470 J 10/11/2017 70,050 1,700 <200 730 2,000 20,000 <200 180 <4000 330 <200 31,000 <200 <200 <200 280 <200 1,700 3,700 1,200 <200 7,100 120 J 130 760 J 11/2/2018 61,400 1,600 <200 660 2,000 17,000 <200 170 <4000 320 <200 27,000 <200 <200 <200 510 <200 1,400 3,100 1,100 <200 6,100 130 J 100 J 1101 9/11/2019 31,290 860 <200 480 1,100 14,000 <200 140 <200 190 J <200 11,000 <200 <200 <200 350 <200 1,300 620 470 <200 <200 <200 <600 780 J PW-41 1/29/1997 1,086 19.0 ND 440 19.0 280 ND ND ND 3 J 210 101 ND ND ND 4 J 4 J ND 7 J 100 4 J ND 7/13/1998 1,012 ND ND 240 D 26 J 200 D ND ND ND 3 J 110 J ND ND 140 J ND ND 101 2 J ND 11 J 130 DJ ND 140 9/26/2000 1,063 37.0 <5 290 28.0 200 <5 <100 <5 160 <10 <5 190 <5 <5 8 <5 <5 30 120 <10 ND 9/12/2001 1,532 47.8 <5 378 49.2 256 <5 108 <10 <5 211 <10 <5 277 <5 <5 30.6 <5 <5 47.4 127 <5 ND 9/19/2002 1,861 55.8 <15 451 64 306 <15 156 <30 <15 253 <30 <15 336 <15 <15 33.7 <15 <15 53.1 152 <15 ND 10/22/2003 1,781 95.3 <5 340 84 247 <5 232 <10 <5 228 <10 <5 361 <5 <5 18.7 <5 <5 27.5 147 <5 ND 8/26/2004 1,997 78.1 <20 359 78.9 409 <20 215 <40 <20 266 <40 <20 357 <20 <20 39.9 <20 <20 50.6 143 <20 ND 3/5/2009 1,441 45.2 <2.OX 227 66.5 192 <2.OX 204 15.4 <2.OX <2.OX 172 6.4 <2.OX <2.OX 288 <2.OX <2.OX 51.4 <2.OX <2.OX 67.2 106 <4.OX ND 4/2/2010 1,143 <1.0 <1.0 220 38.8 178 <1.0 224 8.12 2.32 <1.0 132 3.78 <1.0 <1.0 195 <1.0 3.19 21.3 <1.0 <1.0 28.5 87.6 ND ND 11/2/2011 1,077 456 <5 8.84 48.7 101 <5 44 <50 <5 <5 74.2 <5 <5 <5 204 <5 <5 17.3 <5 <5 118 4.99 <5 ND 11/20/2012 1,086 28.9 <0.5 122 65.5 135 <0.5 175 <50 <5 <5 84.3 <5 <5 <5 276 <5 <5 30 <5 <5 87.8 81.3 <5 ND 12/17/2013 1,276 62.2 <5 134 67.1 139 <5 143 <50 <5 <5 82.4 <5 <5 <5 406 <5 <5 9.4 <5 <5 110 123 <10 ND 12/8/2014 864 35 <5 73 48 87 <5 196 <25 <5 <5 63 3.1 J <5 <5 210 <5 <5 28 <5 <5 74 50 <15 ND 10/29/2015 942 33 <2 75 43 55 <2 206 <10 2.0 <2 88 <2 <2 <2 240 <2 <2 44 <2 1.3 J 95 57 <6 3.9 11/17/2016 933 59 <2 75 51 74 <2 210 <40 2.0 <2 71 <2 <2 <2 230 <2 <2 31 <2 1.5 J 80 47 <6 3.3 10/11/2017 906 46 <2 72 42 49 <2 240 <40 2.0 <2 77 3.5 J <2 <2 230 <2 <2 30 <2 1.7 J 70 45 <6 2.9 11/2/2018 853 46 <2 57 42 36 <2 220 <40 1.6 J <2 78 2.8 <2 <2 230 <2 <2 26 <2 1.3 J 64 46 <6 2.7 9/11/2019 720 32 <5 69 37 36 <5 200 <100 <5 <5 60 <5 <5 <5 230 <5 <5 13 <5 <5 <5 43 <15 ND PW-5D 1/30/1997 426 ND ND 20.0 ND 2.0 ND ND 76.0 2 J 140 33.0 8.0 NA ND 26 ND 10 ND ND 18 ND 91 7/14/1998 6,293 96 J ND 550 D ND 38.0 ND 1,300 ND 61 J 3,800 ND ND 22.0 19 J ND 9 J 260 D 3 J 5 J ND 99 J 31 9/26/2000 13,327 360 <5 2,400 500 150 <5 2,300 110 4,300 220 <5 1,600 21 6.3 17 180 31 28 1,000 104 ND 9/10/2001 13,445 437 <5 2,310 534 168 <5 1,680 <10 90.6 4,110 156 <5 2,280 19.3 11.1 31.7 205 6.6 30.8 1,270 105 ND 9/23/2002 14,201 552 <5 2,500 694 211 <5 1,920 <10 90.1 3,460 190 <5 2,900 16.9 6 27.6 169 7.5 26.2 1,330 101 ND 9/19/2003 753 <5 <5 57.6 <5 <5 <5 412 110.0 <5 164 <10 <5 9 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/18/2004 12,945 534 <5 2,360 757 177 <5 1,260 <10 78.0 3,240 <10 <5 2,980 15.6 <5 32.1 131 <5 15.7 1,280 85 ND 10/12/2004 6,457 166 <5 842 235 57.4 <5 2,420 33.4 31.6 1,240 <10 <5 921 5.7 <5 9.5 44.0 <5 5.8 417 28.4 ND 2/27/2009 14,465 638 5.7 1,900 885 178 <1.0 2,390 36.4 83.4 <1.0 3,110 119 3.5 22.8 4,120 14.8 <1.0 38.3 131 12.1 26.4 672 78.7 ND 3/30/2010 12,428 481 <20.0 1,760 771 102 <20.0 2,170 <100 71.4 <20 3,070 210 <20.0 <20.0 3,040 <20.0 <20.0 <20.0 109 <20.0 <20.0 644 ND ND 11/3/2011 11,290 895 <50 1,760 925 103 <50 580 <500 <50 <50 2,440 488 <50 <50 3,450 <50 <50 <50 <50 <50 <50 649 <50 ND 11/23/2012 11,845 792 <5 1,290 896 109 <5 1,710 <50 51.9 <5 2,000 302 <5 <5 3,850 <5 <5 21.5 101 <5 22.2 602 49.8 47.6 12/16/2013 19,821 1,550 <5 2,200 2,200 181 <5 3,760 <50 121 <5 2,960 509 7.2 <5 5,300 <5 <5 <5 <5 29.7 <5 920 57.6 25.5 12/10/2014 18,168 860 <100 1,800 1,700 340 <100 1,740 <100 100 120 5,200 350 <100 <100 4,400 <100 <100 100 <100 160 <100 1,000 58 240 10/30/2015 7,514 280 <20 870 490 61 <20 1,390 <100 46 <20 2,000 52 <20 <20 1,900 <20 <20 14 J 45 8.8 J 9.2 J 380 13 J ND 11/18/2016 11,941 830 <50 1,400 960 190 <50 1,600 <1000 65 <50 3,000 240 <50 <50 2,900 <50 <50 28 J 66 <50 28 J 690 22 J ND 10/10/2017 4,536 120 <10 640 300 57 <10 1,100 <200 23 <10 830 36 <10 <10 1,200 <10 <10 5.0 J 4.0 J <10 5.1 J 230 4.1 J ND 11/2/2018 2,010 20 <10 280 110 15 <10 560 <200 11 <10 450 14 <10 <10 440 <10 <10 <10 <10 <10 <10 110 <30 ND 9/11/2019 940 7 <5 170 55 8 <5 240 <100 4.4 J <5 220 <5 <5 <5 180 <5 <5 <5 <5 <5 <5 56 <15 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 7 of 14 n v; Sample iv N b p N CD N Sample I.D. �. �. b q b F 3 n n v 3 v Date 0 0 0 0 0 3- n 3 c, m F 0 c, 0 S S 3- 3- 3- p 3- O 3- S S S_ 3' 3 O O O O O O 3A y p O S O O K fD O O O S C) 0 0 O' 0 0 0 W 0 a 0 0 a n 0 0 /� ♦/ N CD N .. fD .. (D O a O O (D O 3 S O 3 (DD O M O 3 S fOD a O_ fOD .. fOD .. S_ : C O S S S S S -a x .r N O N S O S S N O S C S S O O O 0 D) 3 D) 3 N 3 M 3 a) 3 a) 3 D) 3 O 3 (D 3 0: fD 3 N 3 D) 3 fD 3 fD 3 a CD 3 M 3 fD 3 M 3 3 O. m n fp fD CD fD M fD fD CD M fD M fD fD fD fD fD CD M M fD M (D U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 PW-6D 7/21/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/2/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/12/2001 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/20/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/25/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/18/2009 3.8 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.8 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 3/31/2010 31.3 <1.0 <1.0 4.9 <1.0 <1.0 <1.0 5.70 <5.0 <1.0 <1.0 15.5 <1.0 <1.0 <1.0 3.24 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.0 ND ND 11/3/2011 damaged 11/21/2012 damaged 12/10/2013 damaged new well 12/10/2014 266 3.2 <1 41 16 <1 <1 43.2 <5 1.7 <1 90 <1 <1 <1 48 <1 <1 0.53J 1.1 <1 <1 20.0 1.5 ND 10/30/2015 116 2.7 <1 20 8.6 <1 <1 8.85 J <5 0.9 J <1 46 3.0 J <1 <1 31 <1 <1 <1 <1 <1 <1 7.9 <3 ND 11/17/2016 935 14.0 <5 140 59.0 5.2 <5 190 <100 5.4 <5 260 12.0 <5 <5 210 <5 <5 <5 <5 <5 <5 39 <15 ND 12/28/2016 13 NA NA NA NA NA NA 13 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 2/1/2017 600 NA NA NA NA NA NA 600 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA 10/10/2017 1,626 19.0 <2 270 95 12.0 <2 450 <40 7.3 <2 320 20.0 <2 <2 370 <2 <2 1.5 <2 1.4 J 1.4 J 61 <6 ND 11/1/2018 996 7.4 <2 130 50 6.5 <2 320 <40 2.7 <2 230 6.1 <2 <2 210 <2 <2 1.3 <2 <2 1.1 J 31 <6 ND 9/12/2019 392 4.5 <1 120 42 4.7 <1 100 <20 1.4 <1 120 7.0 <1 <1 150 <1 0.84 J 0.84 J <1 1.6 <1 25 <3 ND PW-61 1/28/1997 33 ND ND 11 ND 1 J ND ND ND ND 14 4 J ND ND 1 J ND ND ND 2 J ND ND ND 7/14/1998 46 ND ND 10 ND ND ND ND ND ND 14 4 J ND 5 ND ND 5 ND ND 3 J ND ND 5 9/26/2000 29 <5 <5 12 <5 <5 <5 <100 <5 8.4 <10 <5 8.3 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/12/2001 28 <5 <5 10.7 <5 <5 <5 <10 <10 <5 7.2 <10 <5 9.9 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 31 <5 <5 12.2 <5 <5 <5 <10 <10 <5 9.0 <10 <5 9.8 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/20/2003 47 <5 <5 12.1 <5 <5 <5 11.6 <10 <5 9.9 <10 <5 13 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/25/2004 42 <5 <5 10.6 <5 <5 <5 11.7 <10 <5 6.2 <10 <5 13.0 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/4/2009 8.2 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.0 <1.0 2.4 <1.0 3.8 <1.0 <1.0 <1.0 <2.0 ND 3/31/2010 143.1 <1.0 <1.0 32 1.63 3.47 <1.0 22.5 <5.0 <1.0 <1.0 35.7 10.3 <1.0 <1.0 25.2 <1.0 <1.0 1.56 <1.0 <1.0 2.81 7.88 ND ND 11/3/2011 damaged 11/21/2012 damaged 12/10/2013 damaged new well 12/10/2014 115 0.41 J <1 26 2.2 <1 <1 47.9 <5 <1 <1 2.2 <1 <1 <1 24 <1 1.1 0.7 J 0.7 J <1 1.1 3.3 4.8 1.9 10/27/2015 98 <1 <1 20 1.1 J 3 <1 46.7 <5 <1 <1 7.6 <1 <1 <1 18 <1 <1 0.74 J <1 <1 1.4 <1 <3 1.1 11/17/2016 132 <1 <1 19 1.1 J 11 <1 56 <20 0.47 J <1 21 <1 <1 <1 18 <1 0.53 J 1.0 <1 <1 2.5 3.6 <3 3.89 J 10/10/2017 148 <1 <1 25 0.92 J 3.6 <1 71 <20 0.52 J <1 19 <1 <1 <1 25 <1 <1 0.42 J <1 <1 1.1 3.0 <3 1.4 11/1/2018 128 <1 <1 17 1.1 3.2 0.4 J 60 <20 0.58 J <1 14 <1 <1 <1 24 <1 <1 0.8 J <1 <1 1.7 4.7 <3 1.8 9/12/2019 148 <1 <1 19 1.0 2.9 <1 79 <20 0.74 J <1 13 <1 <1 <1 26 <1 <1 0.42 J <1 <1 <1 5.3 <3 1.8 PW-71 2/6/1997 11 ND ND 2 J ND ND ND ND 7 J ND 1 J ND ND ND ND ND ND ND 1 J ND ND ND 7/17/1998 443 86 ND 16 37 23 ND ND ND 2 J 77 ND ND 50 ND ND 65 9 ND 21 4 J 3 J 50 9/28/2000 99 <5 <5 9.2 15 7.2 <5 <100 NA <5 18 <10 <5 36 <5 14 <5 <5 <5 <5 <10 <10 ND 9/12/2001 158 <5 <5 <5 <5 <5 <5 150 <10 <5 8.1 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/20/2002 139 <5 <5 <5 <5 <5 <5 126 <10 <5 7.7 <10 <5 5 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/22/2003 161 <5 <5 <5 <5 <5 <5 144 <10 <5 9.8 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 6.8 8/25/2004 199 <5 <5 <5 <5 <5 <5 191 <10 <5 8.4 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/4/2009 75 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 50.5 6.8 <1.0 <1.0 11.8 <1.0 <1.0 <1.0 2.6 <1.0 <1.0 <1.0 <1.0 <1.0 1.4 <1.0 1.8 ND PW-8S 1/28/1997 670 ND ND ND ND ND ND ND 670 J ND ND ND ND ND ND ND ND ND ND ND ND ND 7/13/1998 17 ND ND ND ND ND ND ND ND ND ND ND ND 7 ND ND ND ND ND ND ND ND 10 9/27/2000 7.7 <5 <5 <5 <5 <5 <5 <100 <5 <5 <10 <5 7.7 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 37 <5 <5 <5 <5 <5 <5 14.5 <10 <5 6.1 <10 <5 8.1 <5 <5 <5 <5 <5 <5 <10 <5 8.7 9/17/2003 180 <5 <5 <5 <5 <5 <5 <10 163 <5 11.3 <10 <5 6.0 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/17/2004 7.7 <5 <5 <5 <5 <5 <5 <10 <10 <5 7.7 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/3/2009 53 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 41.3 <1.0 <1.0 9.2 <1.0 <1.0 <1.0 2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 8 of 14 n v; Sample iv N b p N CD N Sample I.D. �. �. b q b F 3 n n v 3 v Date 0 0 0 0 0 3- n 3 c, m F 0 c, 0 S S 3- 3- 3- p 3- O 3- S S S_ 3' 3 O O O O O O 3A y p O S O O K fD O O O S C) 0 0 O' 0 0 0 W 0 a 0 0 a n 0 0 /� ♦/ N CD N .. fD .. (D O a O O (D O 3 S O 3 (DD O M O 3 S fOD a O_ fOD .. fOD .. S_ : C O S S S S S -a x .r N O N S O S S N O S C S S O O O 0 D) 3 D) 3 N 3 M 3 a) 3 a) 3 D) 3 O 3 (D 3 0: fD 3 N 3 D) 3 fD 3 fD 3 a CD 3 M 3 fD 3 M 3 3 O. m n fp fD CD fD M fD I fD M M fD M fD fD fD fD fD CD CD M fD M (D U) NC 2L Standard NE 200 6 7 0.4 0.6 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 PW-91 1/30/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 7/17/1998 50 ND ND ND ND ND ND LND 50 J ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3/12/2009 97 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND PW-10D 9/10/1998 15.0 ND ND 6.0 ND ND ND ND ND ND ND 9 J NA NA NA ND ND ND ND ND ND ND 9/26/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/12/2001 11 <5 <5 <5 <5 <5 <5 10.8 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 10.4 <5 <5 <5 <5 <5 <5 <10 10.4 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/17/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 2/26/2009 31 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.6 <1.0 <1.0 <1.0 <2.0 29.0 3/29/2010 2 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.37 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11/1/2011 2 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <3.0 <5 <0.5 <0.5 1.56 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.72 <0.5 <0.5 <0.5 <0.5 ND 11 /21 /2012 ND <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 12/11/2013 ND <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 ND 12/10/2014 ND <1 <1 <1 <1 <1 <1 1.7 J <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 1.8 J ND 11/3/2015 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 11/17/2016 15 1.5 <1 2.3 J 4.9 J <1 <1 <1 <20 <1 <1 2.6 J <1 <1 <1 7.8 <1 <1 0.60 J 0.49 J <1 2.4 3.3 <3 ND 10/10/2017 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/31/2018 20 0.96 J <1 1.6 2.3 <1 <1 <2 <20 <1 <1 1.1 <1 <1 <1 8.6 <1 <1 <1 0.5 J <1 2.7 3.2 <3 ND 9/12/2019 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND PW-101 1/27/1997 7.0 ND ND 6 ND ND ND ND ND ND ND ND ND ND 1 J ND ND ND ND ND ND ND 7/10/1998 8.0 ND ND 8 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 9/26/2000 14 <5 <5 14 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/11/2001 44 <5 <5 12.9 <5 <5 <5 31.4 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 39 <5 <5 <5 <5 <5 <5 14.7 24.6 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/18/2003 126 <5 <5 17 <5 <5 <5 109 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/17/2004 83 <5 <5 16.7 <5 <5 <5 61.3 <10 <5 <5 <10 <5 5.0 <5 <5 <5 <5 <5 <5 <10 <5 ND 3/12/2009 150 <1.0 <1.0 12.7 <1.0 <1.0 <1.0 115 13.8 <1.0 <1.0 <1.0 1.5 <1.0 <1.0 5.2 <1.0 1.1 <1.0 <1.0 <1.0 1.1 <1.0 <2.0 ND 3/29/2010 229 <1.0 <1.0 12.6 <1.0 <1.0 <1.0 206 <5.0 <1.0 <1.0 1.38 1.96 <1.0 <1.0 4.86 <1.0 1.49 <1.0 <1.0 <1.0 <1.0 1.14 ND ND 11/1/2011 78 <0.5 <0.5 21.7 1.65 <0.5 <0.5 36 <5 <0.5 <0.5 1.95 3.73 <0.5 <0.5 8.64 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 3.18 <0.5 1.45 11/19/2012 440 220 <5 25.9 <5 <5 <5 183 <50 <5 <5 <5 <5 <5 <5 11.4 <5 <5 <5 <5 <5 <5 <5 <5 ND 12/11/2013 276 <5 <5 19.5 <5 <5 <5 249 <50 <5 <5 <5 <5 <5 <5 7.7 <5 <5 <5 <5 <5 <5 <5 <10 ND 12/10/2014 243 <1 <1 18 0.55 J <1 <1 205 <5 0.45 J <1 2.3 5.1 <1 <1 6.2 <1 <1 <1 <1 <1 <1 4.4 <3 1.6 10/29/2015 22 <1 <1 16 <1 <1 <1 222 <5 0.57 J <1 2.7 J 3.3 J <1 <1 4.2 J <1 <1 <1 <1 <1 <1 3.9 <3 2.3 11/17/2016 270 <1 <1 18 0.41 J <1 <1 240 <20 0.85 J <1 3.0 2.6 J <1 <1 5.2 <1 <1 <1 <1 0.45 J <1 4.1 <3 2.93 J 10/10/2017 226 <1 <1 5.7 <1 <1 <1 220 <20 <1 <1 <1 <1 <1 <1 1.4 J <1 <1 <1 <1 <1 <1 0.51 J <3 0.44 J 11/1/2018 319 <1 <1 13 <1 <1 <1 290 <20 0.96 J <1 2.5 3.7 <1 <1 4.2 <1 <1 <1 <1 <1 <1 3.4 <3 2.0 9/12/2019 292 <1 <1 12 <1 <1 <1 260 <20 1.0 <1 2.6 <1 <1 5.9 4.2 <1 <1 <1 <1 <1 <1 3.7 <3 2.4 PW-111 7/22/1997 458 ND ND ND ND ND 81 ND ND ND ND ND ND ND ND ND ND ND 450 ND ND ND 7/16/1998 354 ND ND ND ND ND ND ND ND ND ND ND ND 47 ND ND ND ND ND 260 D ND ND 47 9/29/2000 156 <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 26 <5 <5 <5 <5 <5 130 <10 <10 ND 9/11/2001 254 <5 <5 <5 <5 <5 <5 14.3 <10 <5 <5 <10 <5 34.8 <5 <5 <5 <5 <5 205 <10 <5 ND 9/18/2002 274 <5 <5 <5 <5 <5 <5 22.3 <10 <5 <5 <10 <5 38.1 <5 <5 <5 <5 <5 214 <10 <5 ND 9/23/2003 516 <10 <10 <10 <10 <10 <10 50.3 <20 <10 <10 <20 <10 87.3 <10 <10 <10 <10 <10 378 <20 <10 ND 8/25/2004 365 <10 <10 21.5 <10 <10 <10 31.3 <20 <10 <10 <20 <10 82.7 <10 <10 <10 <10 <10 229 <20 <10 ND 3/5/2009 224 <1.0 <1.0 <1.0 <1.0 <1.0 1.7 13.2 8.4 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 36.2 <1.0 2.5 <1.0 <1.0 <1.0 162 <1.0 <5.0 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 9 of 14 n v; Sample iv N b p N CD N Sample I.D. �. �. b q b � 3 n n v 3 ,� �, v x Date 0 0 0 0 0 3- n 3 c, m 0 c, 0 _<, � S S 3- 3- S 0 0 3- n O S S S S_ 3' 3 (DD O O O O O O O 3A y p O S O O K fD O O O 3 S C) 0 0 O' 0 0 0 W 0 a 0 0 a n 0 0 /� ♦/ N CD N .. fD .. K CD ,. fD ,. O O M O 3 S M 3 (D O M fD 3 S fOD a O_ fOD a fOD .. S_ : C O S S S S S -a x .r N O N S O S S N O S C S S O O O 0 D) 3 D) 3 N 3 M 3 a) 3 a) 3 D) 3 O 3 (D 3 0: fD 3 N 3 c) 3 fD 3 fD 3 a M 3 M 3 fD 3 CD 3 3 CL m n fp fD CD fD CD fD fD CD I M fD M fD fD fD fD fD CD M M fD M (D U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 PW-121 7/22/1997 8.0 ND ND ND ND ND ND ND 6 J ND ND ND ND ND 2 J ND ND ND ND ND ND ND 7/16/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/2/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/12/2001 1.0 <5 <5 <5 <5 <5 <5 1.0 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/22/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/17/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 9/27/2007 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/3/2009 6.7 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 6.7 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 3/31/2010 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11/2/2011 1 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <3.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.69 <0.5 <0.5 <0.5 <0.5 ND 11/20/2012 9 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 8.55 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 1.22 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 1/21/2013 ND <2.0 12/17/2013 ND <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 ND 12/12/2014 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/30/2015 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 1.3 J <1 <1 <1 0.70 J <1 <1 <1 <1 <1 <1 <1 <3 ND 11/21/2016 ND <1 <1 <1 <1 <1 <1 <1 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 10/11/2017 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 11/6/2018 ND <1 <1 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND 9/11/2019 ND <1 <1 <1 <1 <1 <1 1.2 J <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 ND PW-131 7/22/1998 295 16/14 NA 77/76 35/26 ND/ND NA ND/ND ND/ND 2 J/2 J 6/6 ND/4 J NA ND/ND 3 J / 2 J 8/8 NA 4 J / 4 J 34/36 ND/ND 110/110 9/29/2000 754 27 <5 240 120 12 <5 <100 NA 8.2 11.0 11.0 <5 220 <5 <5 <5 <5 5.4 6.2 93 <10 ND 9/12/2001 892 16.4 <5 275 89.0 14.1 <5 70.9 <10 7.8 10.4 10.9 <5 305 <5 <5 <5 <5 <5 5.2 87.6 <5 ND 9/20/2002 799 <15 <15 243 67.4 <15 <15 128 <30 <15 <15 <30 <15 270 <15 <15 <15 <15 <15 <15 91 <15 ND 9/23/2003 1,027 11.7 <10 321 92.2 14.3 <10 118 <20 <10 21.7 <20 <10 358 <10 <10 <10 <10 <10 <10 90.4 <10 ND 8/25/2004 1,285 <5 <5 353 116 22.2 <5 166 <10 10.7 47.0 13.4 <5 405 <5 <5 5.6 <5 <5 8.4 138 <5 ND 3/4/2009 520 <1.0 <1.0 175 39.3 8.9 <1.0 78.0 <5.0 5.6 <1.0 18.1 4.1 <1.0 <1.0 133 <1.0 <1.0 1.8 <1.0 <1.0 2.6 53.9 <2.0 ND 3/31/2010 581 <1.0 <1.0 192 41.6 8.8 <1.0 92.4 <5.0 4.96 <1.0 14.5 3.66 <1.0 <1.0 158 <1.0 <1.0 1.07 <1.0 <1.0 2.08 62 ND ND 11/3/2011 784 6.18 <0.5 214 121 11.8 <0.5 27.0 <5 8.05 <0.5 31.4 7.27 <0.5 <0.5 243 <0.5 <0.5 <0.5 <0.5 <0.5 6.26 107 <0.5 0.87 11 /23/2012 779 2.10 <0.5 137 58.5 <0.5 <0.5 332 <5 2.21 <0.5 23.1 4.98 <0.5 <0.5 147 <0.5 <0.5 1.64 <0.5 <0.5 3.26 62.1 <0.5 5.21 12/16/2013 743 <5 <5 197 56.3 11.0 <5 139 <50 <5 <5 <5 <5 <5 <5 236 <5 <5 <5 <5 <5 <5 104 <10 ND 12/12/2014 564 <2 <2 150 53 11.0 <2 91.6 <10 4.0 <2 22 <2 <2 <2 160 <2 <2 1.5 <2 <2 2.8 69 <6 2.1 10/26/2015 419 <1 <1 120 28 4.6 <1 88.6 <5 3.2 <1 18 2.0 J <1 <1 110 <1 <1 1.2 <1 <1 2.1 41 <3 2.2 11/18/2016 433 <1 <1 120 34 5.0 <1 89 <20 2.9 <1 17 1.6 J <1 <1 120 <1 <1 1.3 <1 <1 2.3 40 <3 1.9 10/11/2017 350 <1 <1 100 20 4.8 <1 88 <20 2.5 <1 11 1.7 J <1 <1 80 <1 <1 0.83 J <1 <1 1.6 40 <3 1.9 10/31/2018 322 <1 <1 82 20 4.1 <1 81 <20 2.3 <1 12 1.3 <1 <1 84 <1 <1 0.86 J <1 <1 1.7 32 <3 1.5 9/11/2019 282 <1 <1 94 18 3.6 <1 44 <20 2.4 <1 8.9 1.4 <1 <1 72 <1 <1 0.72 J <1 0.44 J <1 38 <3 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 10of14 �'71_ n v; Sample N N b 0 N N Sample I.D. �. �. b q b � 3 n n v 3 ,� �, v x Date 0 0 0 0 0 3- n 3 c, m 0 c, 0 _<, S S 3- 3- 3- p 3- O S S S S_ 3' 3 O O O O O O 3A y 0 O S O O K fD O O O S C) 0 0 O' 0 0 0 W 0 a 0 0 a n 0 0 /� ♦/ N :D N .. fD .. (D O a O O M O 3 3 O 3 (DD O M O 3 S fOD a O_ .+ .' 3 : C O S -a x .+ N O N S O S S N O S C S S O O O 0 C) 3 D) 3 a) 3 M 3 a) 3 a) 3 a) 3 O 3 M 3 0: N 3 N 3 D) 3 N 3 M 3 a CD 3 M 3 N 3 M 3 3 a m n fp (D CD N M N N M CD M M M M M N M CD CD M N M N U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 PW-14D 7/22/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/31/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/10/2001 81 <5 <5 <5 <5 <5 <5 <10 73.1 <5 <5 <10 <5 <5 <5 7.6 <5 <5 <5 <5 <10 <5 ND 9/17/2003 71 <5 <5 <5 <5 <5 <5 <10 70.7 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/17/2004 25 <5 <5 <5 <5 <5 <5 <10 25.2 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 16 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <2/<2 16.3/18.1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <1/<1 <2/<2 ND 7/26/2007 13 <1 <1 <1 <1 <1 <1 <2 12.6 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/11/2009 14 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 13.4 <1.0 <1.0 1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 3/31/2010 21 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 21.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11 /7/2011 23 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <3.0 13.6 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 9.2 11/27/2012 40 <0.5 <0.5 1.1 <0.5 <0.5 <0.5 35.4 <5 <0.5 <0.5 1.72 <0.5 <0.5 <0.5 2.18 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 ND 12/12/2013 690 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 690 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <1 ND 12/9/2014 236 8.9 <1 25 17 <1 <1 28.7 16.0 1.9 1.2 75.0 6.9 <1 <1 44 <1 <1 0.41 J 1.1 <1 <1 10 2.9 J ND 11/3/2015 10 0.53 J <1 4.2 J 1.0 J <1 <1 8.33 J 8.5 J <1 <1 4.0 <1 <1 <1 5.9 <1 <1 <1 <1 <1 <1 <1 <3 ND 11/16/2016 9 0.64 J <1 3.1 J 0.96 J <1 <1 7.6 J <20 <1 <1 4.4 <1 <1 <1 5 <1 <1 <1 <1 <1 <1 0.89 J <3 ND 10/12/2017 972 5.9 <1 100 24 0.63 J <1 640 <20 1.7 <1 83.0 4.7 J <1 <1 110 <1 <1 0.87 J <1 <1 0.59 J 7.8 <3 ND 11/5/2018 153 <1 <1 0.91 J <1 <1 <1 2.4 <20 0.71 J <1 1.5 <1 <1 <1 1.6 7.7 <1 <1 23 <1 <1 <1 59 ND 9/17/2019 19 <1 <1 0.55 J <1 <1 <1 <1 10 J <1 <1 1.4 <1 <1 <1 0.89 J 1.6 <1 <1 5.2 <1 <1 <1 11 ND PW-14S 7/23/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/30/2000 ND <5 <5 <5 <5 <5 <5 <100 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/19/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 7/28/2007 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/10/2009 28 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 28.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND PW-15D 7/21/1998 841 ND 150 ND 8 320 J ND ND 14.0 220 D 75.0 3 J ND 3 J 38.0 ND 10.0 10/31/2000 9,042 46.0 <5 710 57 19 <5 1,800 NA 73.0 5,100 690 <5 220 <5 68.0 <5 25.0 5.4 6.5 200 22.0 ND 9/6/2001 12,582 <5 <5 1,150 <5 <5 <5 3,650 <10 <5 5,930 813 <5 653 <5 <5 <5 <5 <5 <5 386 <5 ND 9/16/2003 2,467 24.0 <5 349 78.2 14.1 <5 622 <10 <10 728 162 <5 352 <5 20.1 <5 <5 <5 <5 118 <5 ND 8/19/2004 507 <5 <5 105 19.7 <5 <5 126 <10 <10 107 27.0 <5 104 <5 <5 <5 <5 <5 <5 17.8 <5 ND 8/29/2006 8,571 234 <10 1,450 507 65.2 <10 1,650 <50 57.3 1,910 200 <10 1,920 <10 16.9 10.1 <10 <10 <10 550 <20 ND 9/26/2007 1.8 <1 <1 1.8 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/11/2009 11,715 426 3.6 1,840 740 83.6 <1.0 1,990 37.1 69.3 <1.0 2,890 254 1.7 <1.0 2,530 1.9 7.4 20.2 31.6 8.4 7.1 713 52.2 7.4 3/30/2010 14,028 466 3.37 2,120 876 83.0 <1.0 2,230 40.1 82.1 <1.0 3,660 273 1.65 <1.0 3,360 <1.0 8.21 15.9 19.1 9.47 8.0 772 ND ND 11/7/2011 196 10.1 <5 39.4 <5 <5 <5 8 <50 <5 <5 61.9 <5 <5 <5 58.4 <5 <5 <5 <5 <5 <5 18.5 <5 ND 11/26/2012 6,608 424 1.89 1,160 612 64.6 0.59 1,180 <5 73.9 <0.5 812 J 351 <0.5 <0.5 2,070 6.56 7.23 12.0 53.2 12.0 7.48 483 37.5 50.63 12/12/2013 11,775 591 <5 1,440 593 70.5 <5 1,770 <50 67.3 88.4 2,920 536 <5 <5 2,920 <5 <5 <5 51.8 <5 <5 676 32.7 18.2 12/9/2014 12,358 520 <50 1,400 920 82.0 <50 1,930 <250 66.0 <50 3,600 470 <50 <50 2,700 <50 <50 <50 23.0 <50 <50 670 <150 ND 10/28/2015 4,734 68 <50 570 220 <50 <50 1,280 <250 28.0 <50 1,300 <50 <50 96 1,000 <50 <50 <50 <50 <50 <50 200 <150 ND 11/15/2016 3,812 63 <10 430 170 24 <10 1,300 <200 16.0 <10 910 99 <10 <10 690 <10 <10 <10 <10 <10 <10 110 <30 ND 10/12/2017 1,321 12 <1 200 66 7.9 <1 510 <20 4.2 <1 190 12 <1 <1 280 <1 <1 1.5 J <1 1.1 J 1.0 J 39 <3 ND 11/5/2018 572 3.1 <2 81 27 2.2 <2 240 <40 1.1 J <2 79 5.3 <2 <2 120 <2 <2 1.2 J <2 1.1 J <2 11 <6 ND 9/17/2019 176 <5 <5 30 8.9 <5 <5 91 <100 <5 <5 7.4 <5 <5 <5 39 <5 <5 <5 <5 <5 <5 <5 <15 ND PW-15S 7/21/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/30/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 11 <5 <5 <5 <5 <5 <5 11.0 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 25 <5 <5 <5 <5 <5 <5 24.6 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/19/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 9/25/2007 1.5 <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 1.5 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/11/2009 78 <1.0 <1.0 18.6 4.8 <1.0 <1.0 6.6 13.4 <1.0 <1.0 <1.0 4.5 <1.0 <1.0 26.5 <1.0 3.9 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 11 of 14 n v; Sample N N b 0 N N Sample I.D. Date �. �. b 0 q 0 b 0 F 3 n 3- n n 3 v c, m 3 ,� v c, 0 S 0 S 3- 3- 3- p 3- O S S F 0 S S_ 0 3' 3 O O O O O O 3A y 0 O S O O K fD O O O S C) 0 0 O' 0 0 0 W 0 a 0 0 a n 0 0 /� ♦/ N :D N .. fD .. K CD ,. fD ,. O O M O 3 S M 3 (D O M fD 3 S fOD a O_ fOD .* fOD ,+ S_ 1 < O S S S 3 S -a x .r N O N S O S S N O S C S S O O O 0 C) 3 D) 3 N 3 M 3 a) 3 a) 3 a) 3 O 3 M 3 0: N 3 N 3 D) 3 N 3 M 3 a CD 3 M 3 N 3 CD 3 3 O. m n fp (D CD M M N I N M M M fD I M M M M M CD CD M N M M U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 - PW-16D 7/22/1998 786 ND 130 ND 6.0 87.0 ND 7.0 380 140 ND 3 J ND 6.0 16.0 ND 11.0 11/2/2000 1,610 <120 <120 210 <120 <120 <120 <2,500 <120 1,400 <250 <120 <120 <120 <120 <120 <120 <120 <120 <250 <250 ND 9/6/2001 4,184 10.6 <5 355 12.3 8.9 <5 788 <10 29.3 2,580 250 <5 71.5 <5 22.7 <5 <5 <5 <5 55.2 <5 ND 9/17/2003 4,324 <100 <100 501 <100 <100 <100 858 <200 <100 2,680 <200 <100 285 <100 <100 <100 <100 <100 <100 <200 <100 ND 8/19/2004 2,722 <50 <50 353 <50 <50 <50 729 <100 <50 1,200 119 <50 215 <50 <50 <50 <50 <50 <50 106 <50 ND 8/29/2006 4,357 71.8 <10 732 178 31.5 <10 889 <50 31.1 1,370 78 <10 709 <10 <10 <10 <10 <10 <10 266 <20 ND 9/25/2007 5,130 <20 <20 844 247 36.5 <20 882 <100 36.8 1,700 75.5 <20 957 <20 <20 <20 <20 <20 <20 351 <40 ND 3/11/2009 6,570 110 1.5 1,160 372 50.5 <1.0 890 15.9 42.6 <1.0 1,950 93.5 <1.0 <1.0 1,400 <1.0 4.9 11.1 3.4 4.2 4.5 442 10.5 3.3 3/30/2010 6,295 88.2 <1.0 1,180 329 48.2 <1.0 1,080 27.2 39.9 <1.0 1,780 80.8 <1.0 <1.0 1,240 <1.0 4.85 4.97 1.50 3.03 3.59 384 ND ND 11/7/2011 7,345 232.0 <5 1,380 732 62.5 <5 260 <50 55.9 <5 1,770 405 <5 <5 1,740 <5 <5 <5 <5 <5 11.7 655 7.9 8.0 11/26/2012 7,820 165 1.01 1,090 543 50.4 0.52 1,260 <5 48.7 <0.5 2,100 229 <0.5 <0.5 1,680 <0.5 4.57 8.59 3.30 6.72 5.5 601 <0.5 23.1 12/12/2013 7,988 251 <5 1,360 688 65.9 <5 1,330 <50 55.2 37 1,870 245 <5 <5 1,700 <5 <5 <5 <5 <5 <5 368 5.7 12.0 12/9/2014 6,745 180 <20 920 490 60 <20 1,150 <100 36 <20 1,900 150 <20 <20 1,500 <20 <20 9.2 <20 <20 <20 350 <60 ND 10/28/2015 3,527 51 <20 480 190 18 <20 772 <100 22 <20 1,000 44 <20 <20 790 <20 <20 <20 <20 <20 <20 160 <60 ND 11/15/2016 2,461 46 <10 390 180 23 <10 650 <200 12 <10 520 <10 <10 <10 540 <10 <10 3.2 J <10 <10 2.1 J 100 <30 ND 10/12/2017 4 <1 <1 1.5 J 0.47 J <1 <1 3.9 J 13 J <1 <1 2.4 J <1 <1 <1 2.5 J <1 <1 <1 <1 <1 <1 0.66 J <3 ND 11/29/2017 2,284 21 <5 340 76 16 <5 870 <100 14 <5 490 14 <5 <5 370 <5 <5 2.4 J <5 <5 <5 73 <15 ND 11/5/2018 195 1.5 <1 40 12 0.96 J <1 84 <20 <1 <1 2.3 <1 <1 <1 53 <1 <1 <1 <1 <1 0.46 J 1.8 <3 ND 9/17/2019 99 0.51 J <1 20 4.5 <1 <1 28 <20 0.45 J <1 22 3.3 <1 <1 20 <1 <1 <1 <1 <1 <1 1.3 <3 ND PW-16S 7/22/1998 ND ND NA ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 10/30/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/6/2001 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/17/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/19/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 6.5 <1 <1 <1 <1 <1 <1 <2 6.5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 9/26/2007 ND <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND PW-17 11/3/2000 160 <5 <5 <5 <5 <5 <5 160 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 12/20/2000 ND <5/<2 <5/<2 <5/<2 <5/<2 <5/NA <5/<10 <100/<100 NA/<100 <5/<2 <5/<10 <10/<10 <5/<2 <5/<2 <5/<2 <5/<10 <5/<2 <5/<2 <5/<2 <5/<2 <10/<2 <10/<5 ND 9/12/2001 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/22/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/25/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 8.8 <1 <1 <1 <1 <1 <1 <2 8.8 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 9/27/2007 6.3 <1 <1 <1 <1 <1 <1 <2 6.3 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/5/2009 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 12 of 14 n v; Sample N N b o CDN Sample I.D. �. �. b q b F 3 n n v 3 v Date 0 0 0 0 0 3- n c, m F 0 a 0 S S 3- 3- 3- p 3- O 3- S S S_ 3' 3 Q O O O O O O A y p O S O O K fD O O O 3 S v 0 0 O' 0 0 'a 0 W 0 a a 0 0 0 m N m C N .. fD .. (D O a O _ O (D O 3 S O 3 (D O M O 3 S fOD a O_ fOD .. fOD .. S_ : C O S S S S S -a x .r N O N S O S S N O S C S S O O O 0 Cl 3 D) 3 N 3 m 3 C) 3 C) 3 d 3 O 3 (D 3 0: fD 3 N 3 D) 3 fD 3 (D 3 a CD 3 M 3 fD 3 M 3 3 O. Iv 0 fp fD CD fD M fD I fD CD I M fD fD I fD fD fD fD fD CD M M fD M (D U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 PW-18 11/7/2000 19 <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 19.0 <5 <5 <10 <10 ND 12/20/2000 ND <5/<2 <5/<2 <5/<2 <5/<2 <5/NA <5/<10 <100/<100 NA/<100 <5/<2 <5/<10 <10/<10 <5/<2 <5/<2 <5/<2 <5/<10 <5/<2 <5/<2 <5/<2 <5/<2 <10/<2 <10/<5 ND 9/11/2001 24 <5 <5 <5 <5 <5 <5 <10 24.3 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 204 <5 <5 <5 <5 <5 <5 <10 195 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 8.9 ND 8/19/2004 149 <5 <5 <5 <5 <5 <5 22.8 119 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 6.8 ND 10/1/2004 27 <5 <5 <5 <5 <5 <5 <10 27.4 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 264 <1 <1 <1 <1 <1 <1 <2 151 <1 <1 <1 < <1 1.7 <1 <1 1.2 <1 <1 <1 16.3 93.8 9/26/2007 194 <1 <1 <1 <1 <1 <1 <2 108 <1 <1 <1 < <1 1.3 <1 <1 1.2 <1 <1 <1 12.0 71.1 3/12/2009 203 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 125 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.1 3.5 <1.0 <1.0 <1.0 <1.0 <1.0 9.8 63.7 3/31/2010 86 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 85.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 1.26 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND 11 /7/2011 143 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <3.0 92.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 2.94 48.43 11 /26/2012 91 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 36.0 30.8 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.86 <0.5 <0.5 0.6 <0.5 <0.5 <0.5 6.73 24.5 1/21/2013 ND <2.0 12/12/2013 31 <5 <5 <5 <5 <5 <0.5 5.05 <50 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <5 <10 25.6 2/25/2014 ND <2 12/9/2014 96 <1 <1 <1 <1 <1 <1 9.17 55 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 1 <1 <1 <1 6 30.7 1/29/2015 58 <1 <1 <1 <1 <1 <1 <2 35 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 4.9 18 10/26/2015 ND <1 <1 <1 <1 <1 <1 <2 40 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 0.65 J <1 <1 <1 1.2 J 19 11/15/2016 ND <10 <10 <10 <10 <10 <10 <10 <200 <10 <10 <10 <10 8.3 J <10 <10 <10 <10 <10 <10 <10 <10 <10 <30 ND 10/16/2017 ND <1 <1 <1 <1 <1 <1 <2 20 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 6.7 J 11/7/20018 35 <1 <1 0.65 J 0.91 J <1 <1 <2 20 <1 <1 0.42 J <1 <1 <1 2.8 <1 <1 <1 <1 <1 1.3 <1 0.58 J 7.3 1/10/2019 24 J <1 <1 0.65 J <1 <1 <1 <2 17 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 1.3 J 5.2 J 9/17/2019 Not Sampled PW-19 11/6/2001 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/19/2002 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/16/2003 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/18/2004 98 <5 <5 <5 <5 <5 <5 97.8 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/1/2004 ND <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 8/29/2006 3.7 <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 3.7 9/27/2007 5.0 <1 <1 <1 <1 <1 <1 <2 5.0 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <2 ND 3/11/2009 91 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 87.3 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.8 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND 1/29/2015 <1 <1 <1 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 0.57 J <1 <3 ND PW-DR-1 9/8/2004 248 <5 <5 10.7 <5 <5 <5 164 <10 <5 40.2 16.6 <5 16.4 <5 <5 <5 <5 <5 <5 <5 <5 ND 9/23/2004 268 <5 <5 5.6 <5 <5 <5 209 <10 <5 31.3 13.6 <5 8.3 <5 <5 <5 <5 <5 <5 <10 <5 ND 10/8/2004 249 <5 <5 5.6 <5 <5 <5 213 <10 <5 30.8 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 2/25/2009 1,848 54.4 <1.0 213 98.8 7.7 <1.0 579 7.5 11.8 <1.0 400 58.3 <1.0 <1.0 314 2.2 <1.0 3.5 23.8 1.2 1.3 <1.0 71.2 ND PW-SIS1 8/25/2004 12,848 201 <5 3,370 765 223 <5 2,500 <10 69.5 39.0 <10 <5 5,060 <5 110 49.9 <5 <5 69.8 376 15.1 ND 3/9/2009 9,940 473 3.7 1,990 1,310 139 1.4 1,230 37.7 97.4 <1.0 68.1 38.8 3.7 <1.0 3,510 1 <1.0 6.0 121 3.2 49.0 263 555 39.9 ND W-1 1/29/1997 3 ND ND ND ND ND ND ND ND ND ND ND 3 J NA ND ND ND ND ND ND ND ND ND 9/27/2000 ND <5 <5 <5 <5 <5 <5 <100 NA <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <10 ND 9/10/2001 <5 <5 <5 <5 <5 <5 12.4 <10 <5 <5 <10 <5 <5 <5 <5 8.4 <5 <5 <5 <10 <5 ND 9/18/2002 20 <5 <5 <5 <5 <5 <5 11.5 <10 <5 <5 <10 <5 <5 <5 <5 8.2 <5 <5 <5 <10 <5 ND 9/17/2003 86 <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 76.4 <5 <5 9.7 <10 <5 ND 8/17/2004 43 <5 <5 <5 <5 <5 <5 <10 <10 <5 <5 <10 <5 <5 <5 <5 33.7 <5 <5 9.3 <10 <5 ND 3/3/2009 25 <1.0 <1.0 <1.0 3.3 <1.0 <1.0 <2.0 7.7 <1.0 <1.0 <1.0 <1.0 1.1 <1.0 <1.0 <1.0 <1.0 11.1 <1.0 <1.0 1.9 <1.0 <2.0 ND W-2 1/30/1997 87,240 30,000 ND 12,000 11,000 960 J ND ND 2,200 J 410 J ND ND 1,500 J ND ND ND 20,000 970 J 1,200 ND 1,200 5,300 500 J ND DUP-3(W-2) 1/28/1997 79,260 27,000 ND 11,000 9,500 930 J ND ND 2,300 J 410 J ND ND 1,400 J ND ND ND 19,000 910 1 1,200 ND 1,100 4,300 210 J ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 13 of 14 �'71_ n v; Sample N N b 0 N 3 N Sample I.D. Date �. �. b 0 q 0 b 0 � n 3- n n 3 v c, m ,� �, v c, x 0 S 0 S 3- 3- 3- p 3- O S S 0 0 _<, Q O O O O O O 3A y p O S O O K fD O O O 7 S C) 0 0 O' 0 0 0 W 0 a 0 0 a n 0 0 /� ♦/ N fD N .. fD .. (D O a O O M O 3 S O 3 (DD O M W 3 S fOD a O_ fOD fOD S O S D) S D) S N S fD S O -a O K D) .r O N M O N N S N O S D) S N N M O S CD C M S N S M O 3 O O 0 3 3 3 3 3 3 3 3 3 0: 3 3 3 3 3 a 3 3 3 3 CL m 0 fp (D CD I M M N N CD M M M M M M M M CD CD M N M M U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 - W-4 2/6/1997 1,624 47.0 ND 640 86.0 23 J ND ND 6 J 30.0 8 J 35 J ND NA 7 J ND ND 7 J ND ND 280 5 J 450 9/27/2000 525 14.0 <5 200 57.0 8.4 <5 <100 NA 8.7 <5 <10 <5 170 <5 <5 <5 <5 6.7 <5 60.0 <10 ND 9/10/2001 49 <5 32.7 <5 <5 <5 <5 16.5 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/17/2002 18 <5 <5 <5 <5 <5 <5 18.2 <10 <5 <5 <10 <5 <5 <5 <5 <5 <5 <5 <5 <10 <5 ND 9/17/2003 694 27.9 <5 135 56.9 10.9 <5 162 <10 <5 <5 <10 <5 248 <5 <5 <5 <5 <5 8.1 45.2 <5 ND 8/17/2004 3,157 136 <10 432 331 35.2 <10 547 <20 17.0 14.5 <20 <10 1,010 <10 <10 13.0 <10 <10 10.4 91.2 <10 ND W-4A 1/28/1997 75,370 13,000 ND 11,000 5,700 540 ND ND ND 890 J ND ND ND NA ND 39,000 ND 1,300 ND ND 2,600 280 J 1,060 9/27/2000 15,940 380 <5 4,300 1,500 160 <5 2,100 NA 230 67 50 <5 4,500 12.0 1,300 38.0 57 260 42.0 870 66.0 8.3 9/10/2001 37,215 619 <5 10,400 3,560 316 <5 2,770 <10 <5 125 111 <5 12,400 40.4 4,350 52.6 126 19.3 43.8 2,100 169 13.1 9/17/2002 31,439 515 <5 9,120 2,490 207 <5 1,950 <10 273 105 95.7 <5 10,500 24.4 3,570 38.5 59.4 10.9 28.5 2,330 122 ND 9/17/2003 5,351 83 <5 1,350 544 68.1 <5 1,090 <10 73 29.1 18.5 <5 1,740 <5 <5 16.8 15.1 <5 16 286 22.4 ND 8/17/2004 19,357 <100 <100 5,390 2,070 182 <100 1,870 <200 225 111 <100 <100 7,330 <100 831 <100 <100 <100 <100 1,230 118 ND 2/27/2009 6,307 73.4 <1.0 1,240 541 57.9 <1.0 942 13.4 98.4 <1.0 67.4 163 <1.0 3.3 2,260 7.3 78.8 8.3 11.3 6.5 12 686 36.8 ND 3/31/2010 10,920 401 <1.0 1,880 995 73.6 1.19 1,010 32.7 129 <1.0 91.9 238 <1.0 1.98 3,590 16.1 918 43.5 72.5 6.26 89 1,330 ND ND 11/2/2011 41,390 216 <50 5,340 3,750 363 <50 520 <500 861 <50 469 7,290 <50 <50 10,300 <50 1,130 <50 307 <50 83 11,000 281 ND 11/19/2012 4,144 28.7 <0.5 335 296 21.9 <0.5 1,600 <5 65.3 3.77 30 241 <0.5 0.95 693 3.28 155 1.48 16 2.87 4.27 622 20.11 3.74 12/17/2013 59,696 513 <50 7,580 3,260 318 <50 1,270 <500 843 <50 332 6,790 <50 <50 14,400 <50 15,300 <50 249 <50 <50 8,580 261 ND 12/8/2014 37,661 430 <100 4,700 2,700 360 <100 2,100 <100 560 <100 270 3,600 <100 <100 8,800 <100 6,300 <100 220 41 140 7,000 220 220 10/27/2015 8,952 270 <100 1,400 640 <100 <100 962 <500 210 <100 110 540 <100 <100 2,500 <100 <100 <100 120 <100 76 J 2,200 <300 ND 11/16/2016 9,410 380 <100 2,000 690 67 <100 660 <2000 260 <100 140 560 <100 <100 2,400 <100 220 <100 72 J <100 92 J 2,100 <300 ND 10/11/2017 2,832 24 <10 440 190 36 <10 630 <200 40 <10 39 66 <10 <10 570 <10 <10 4.3 J <10 <10 5.3 780 12 ND 10/31/2018 1,400 33 <5 260 110 7.6 <5 210 <100 14 <5 11 30 <5 <5 500 <5 <5 3.4 J <5 2.4 J 28 190 <15 ND 9/11/2019 435 12 <1 83 33 2.8 <1 54 <20 7.5 <1 4.4 13 <1 <1 130 <1 0.45 J 0.81 J <1 1.3 6 88 <3 ND W-4B 2/4/1997 117,470 20,000 ND 13,000 8,700 810 J ND ND 4,500 J 1,200 J ND ND ND ND ND ND 61,000 550 J 2,800 ND ND 4,200 710 J ND W-5 8/7/1996 467,000 110,000 ND 27,000 21,000 ND ND 19,000 2,100 J 1,700 9,400 J ND ND ND 140,000 6,900 13,000 ND ND 36,000 3,900 J 77,000 2/24/1997 415,300 98,000 ND 26,000 19,000 2,000 ND ND 34,000 2,200 J 1,800 9,100 J ND ND 1,100 J 130,000 5,600 15,000 ND 24,000 33,000 5,200 9,300 10/30/2000 402,208 95,000 91.0 22,000 31,000 1,100 17.0 24,000 NA 1,000 1,200 2,200 190 72,000 760 100,000 3,500 8,900 340 11,000 25,000 2,540 370 9/10/2001 378,680 144,000 <5 14,000 33,300 <5 <5 13,800 <10 <5 <5 <10 <5 53,900 <5 63,200 7,710 9,270 <5 27,000 12,500 <5 ND 9/19/2002 672,790 121,000 <5,000 45,400 122,000 <5,000 <5,000 14,300 <10,000 7,780 11,100 <10,000 <5,000 74,300 5,880 93,100 28,900 35,300 <5,000 38,300 39,500 28,400 7,530 9/17/2003 367,940 135,000 <5,000 9,220 31,800 <5,000 <5,000 11,300 <10,000 <5,000 <5,000 <10,000 <5,000 56,400 <5,000 81,900 6,340 7,580 <5,000 28,400 <10,000 <5,000 ND 8/18/2004 375,700 177,000 <5000 5,290 36,600 <5000 <5,000 4,110 <10,000 <5,000 <5,000 <10,000 <5,000 41,400 <5,000 48,900 10,800 10,400 <5,000 41,200 <10,000 <5,000 ND 3/3/2009 170,238 66,700 75.8 3,720 15,500 289 <50.OX 1,860 1,380 1,420 <50 1,000 111 121 <50.OX 30,800 <50.OX 10,900 3,700 3,400 70.0 25,900 1,040 1,940 311.0 W-6 2/5/1997 123,360 23,000 ND 14,000 8,500 20,000 ND ND 3,400 J ND ND 15,000 ND ND ND ND 260 J 19,000 2,700 3,000 ND 2,400 5,100 1,400 2,800 DUP-1 (W-6 8/7/1996 143,900 27,000 ND 16,000 10,000 23,000 ND 2,800 ND ND 18,000 ND ND ND ND ND 21,000 6,200 3,300 ND 4,000 6,500 1,600 4,500 W-6A 2/5/1997 739,000 10,000 ND 65,000 16,000 48,000 ND ND 150,000 ND 21,000 ND ND ND ND 310,000 3,200 J 12,000 ND ND 6,800 J ND 97,000 9/28/2000 838,040 31,000 280 69,000 24,000 71,000 <5 81,000 <5 17,000 940 160 100,000 550 410,000 3,200 14,000 660 3,100 9,900 1,950 300 W-6B 2/5/1997 238,400 59,000 ND 23,000 14,000 19,000 ND ND 14,000 ND ND 18,000 ND ND ND ND 55,000 4,700 5,700 ND 11,000 1,000 J 1,000 J 13,000 W-13A 1/31/1997 1,688 66.0 ND 230 110 6 J ND 990 120 ND ND ND 5J ND ND ND 27.0 90 ND ND 30 14J ND ND W-18 2/3/1997 6,781 500 ND 820 930 960 ND ND ND ND ND ND ND 71 J ND ND 610 1,500 ND ND 930 460 ND ND 3/5/2009 9,932 60.0 3 741 396 17.4 <1.0 1,350 19.5 9.9 7.2 4.4 11.7 77.9 <1.0 4,050 <1.0 7.2 490 <1.0 13.5 1,850 819 3.8 ND W-20 1/31/1997 19.0 4 J ND 4 J 4 J ND ND ND ND ND ND ND ND ND ND ND ND 5 ND ND 2 J ND ND ND TABLE 2 GROUND WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Page 14of14 �'71_ n v; Sample N N b o N N Sample I.D. �. �. b q b � 3 n n v 3 ,� �, v x Date 0 n 0 0 0 3- n c, m n a n _< -4 S S 3- 3- S C p 3- n O S S S S_ 3' 3 N O O O O O O O A y p O S O O K fD O O O 3 S C) 0 0 O' o o n W n rr ' ' a n ' 0 /� ♦/ N fD N a fD .. (D O a O O M O 3 3 O 3 (DD O M O 3 S fOD a O_ fOD .. fOD .. 3- : C O S S S S S -a X .r N O N S O S S N O S C S S O O O 0 D) 3 D) 3 N 3 fD 3 a) 3 a) 3 D) 3 O 3 (D 3 CL fD 3 N 3 D) 3 fD 3 fD 3 a CD 3 M 3 fD 3 M 3 3 a m 0 fp fD CD fD M fD I fD CD M fD M fD fD fD fD I fD CD CD M fD M (D U) NC 2L Standard NE 200 6 7 0.4 0.6 3 6000 1 0.3 50 3,000 70 3 70 600 5 0.7 600 100 3 0.03 500 W-21 1/31/1997 1,232 340 ND 130 210 110 ND 240 J ND ND ND 18 J 3 J ND ND 3 J 47.0 ND ND 54.0 77.0 ND ND 9/28/2000 1,494 190 <5 120 140 74.0 <5 520 NA <5 <5 <10 <5 220 <5 <5 97.0 <5 <5 73.0 60.0 <10 ND 9/10/2001 1,336 129 <5 101 140 57.8 <5 407 <10 <5 <5 <10 <5 271 <5 <5 116 <5 <5 72.7 41.4 <5 ND 9/17/2002 1,775 127 <5 188 163 36.2 <5 458 <10 5.2 <5 <10 <5 498 <5 <5 102 <5 <5 98.0 100 <5 ND 9/17/2003 1,890 106 <5 140 151 44.6 <5 743 <10 <5 <5 <10 <5 384 <5 <5 140 <5 <5 105 76.7 <5 ND 8/17/2004 1,761 71.2 <10 114 124 47.4 <10 821 <20 <10 <10 <20 <10 333 <10 <10 95.2 <10 <10 81.5 73.5 <10 ND 9/24/2009 3,701 313 1.2 1 518 390 38.9 1 <1.0 678 16.0 12.6 <1.0 1 9.8 4.9 5.3 1 <1.0 1,210 1 <1.0 <1.0 108 <1.0 1 3.3 170 222 <2.0 ND W-23A 1/30/1997 4,600 ND ND ND ND ND ND ND 4,600 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 7/17/1998 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 3/4/2009 115 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 106 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.4 <1.0 <1.0 3.1 <1.0 <1.0 2.6 <1.0 <2.0 ND W-23B 1/22/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND W-24 1/31/1997 2,109 200 ND 190 330 ND ND ND ND ND ND ND ND 11 J ND ND 54 440 ND ND 710 160 14 J ND UP-2 (W-2 1/31/1997 1,921 180 ND 180 310 ND ND ND ND ND ND ND ND 10 J ND ND 49 400 ND ND 630 150 12 J ND 7/16/1998 1,943 ND 100 J 160 240 D ND ND ND ND 3 J ND ND ND 8 ND ND 12 520 D ND ND 690 D 190 20.0 ND W-25 8/7/1996 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 1/27/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND W-29 2/5/1997 1,688,000 120,000 ND 7,400 J 29,000 580,000 ND ND 240,000 ND ND 49,000 ND ND ND ND 290,000 13,000 J 10,000 J ND 150,000 ND ND 230,000 BD-1 3/29/2010 235 <1.0 <1.0 14.7 <1.0 <1.0 <5.0 208 <5.0 <1.0 <1.0 1.74 2.28 <1.0 <1.0 5.72 <1.0 1.48 <1.0 <1.0 <1.0 <1.0 1.34 ND ND DUP-02 3/31/2010 148 <1.0 <1.0 31.0 1.60 3.45 <1.0 28.6 <5.0 <1.0 <1.0 35.4 9.90 <1.0 <1.0 24.1 <1.0 2.00 1.55 <1.0 <1.0 2.87 7.67 ND ND LCHT-COMP 3/30/2010 904 <2.0 <2.0 82.2 34.4 8.87 <2.0 416 32.4 8.00 <2.0 136 24.7 <2.0 <2.0 95.8 2.60 5.09 <2.0 6.24 <2.0 6.69 44.9 ND ND PW-SF1 4/2/2010 11,985 <2.0 <2.0 114 <2.0 <2.0 <2.0 8,410 247 20 <2.0 1,190 1,340 <2.0 <2.0 2.4 11 175 <2.0 447 4 <2.0 25 ND ND 11/3/2011 34,627 1,840 32.6 2,990 3,670 1,240 <5 1,300 57.2 32.5 <5 1,450 1,580 250 <5 13,100 <5 251 211 1,070 23.3 1,410 3,920 54.0 145.7 11/20/2012 8,577 136 <50 480 5.7 135 <50 4,310 <500 <50 <50 298 <50 <50 <50 2,230 <50 <50 <50 110 <50 123 749 <50 ND 12/9/2013 46,400 1,250 <50 3,700 6,190 1,060 <50 3,940 <500 <50 <50 1,710 1,130 276 19,900 <50 <50 <50 700 <50 1,470 4,920 <100 154 12/8/2014 43,302 1,100 <200 3,500 4,200 1,300 <200 3,510 <1000 <200 <200 2,000 1,200 200 <200 19,000 <200 <200 320 680 <200 1,700 4,500 <600 92 10/27/2015 41,479 1,100 <100 3,200 3,600 780 <100 3,550 <500 <100 <100 2,100 790 160 <100 18,000 <100 <100 420 800 <100 2,200 4,700 <300 79 J 11/17/2016 48,530 1,800 <500 4,400 4,900 780 <500 3,600 <10000 <500 <500 2,200 450 J 280 J <500 22,000 <500 <500 660 690 <500 2,800 4,700 <1500 ND 10/11/2017 43,254 1,300 <100 3,900 4,000 880 <100 3,600 <2000 <100 <100 1,900 340 180 <100 19,000 <100 <100 650 530 <100 2,900 4,000 43 J 74 10/30/2018 40,063 1,200 <100 3,400 3,600 660 <100 2,800 <2000 <100 <100 2,100 <100 110 <100 18,000 <100 <100 680 660 <100 3,100 3,600 45 J 63 J 9/10/2019 43,240 3,100 <200 3,500 4,100 600 <200 3,200 <4000 <200 <200 1,800 <200 120 <200 20,000 <200 160 830 530 <200 2,900 2,400 <600 ND EB-1 4/2/2010 19 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 15.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 3.15 <1.0 <1.0 <1.0 <1.0 <1.0 ND ND FB-1 4/2/2010 25 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 1 21.4 <1.0 <1.0 I <1.0 <1.0 <1.0 I <1.0 <1.0 <1.0 3.55 <1.0 I <1.0 <1.0 <1.0 I <1.0 ND ND Crutchfield (potable well 12/1/1998' ND <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA <2.0 <0.5 <0.5 <0.5 <2.0 <0.5 <2.0 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 NA <0.5 ND 3/11/2009 2.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 2.5 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND ug/l = micrograms per liter J = Estimated value B = Analyte detected in associated method blank as well as sample ND = Not detected NA = Not Analyzed 1 - Sample collected and analyzed by North Carolina Division of Waste Management Bold type indicates value exceeds NC 2L ground water standard Values separated by slash 0 indicate split sample results NC 2L Standard = North Carolina 2L ground water quality standard TABLE 3 Pagel of 3 SURFACE WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL SITE c c c 0 �_ s x Sample Sample Date o s 0 s 0 s 00 0 0 0 'o n 1P m s o 0 0 - m W Descri [ion p o o 'o 0 o D 0 3 o z 'o T o s >• >• 0 3 $ 0 - 0 = 0 m x .o1p. 0 m .. a p 1D a 0 o (ug/1) (ug/1) u /I a /I a /I u /I u /I (ug/1) (ug/1) u /I u /I u /1) (ug/1) (u°/I) (u /I u /I u /I _ u /I u /I NC 2B Ste. WS-IV 2500 6700 330 0.38 0.35 2000 1.19 130 12 NE 330 2.6 0.7 11 140 2.5 0.025 670 20,000 Northern Intermittent Stream SW-1 4/30/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 11/2/2000 <5 <5 <5 <5 <100 NA <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <10 ND 9/14/2001 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/02 Dry _ _ _ _ __ __ __ _ ND __ __ __ __ __ _ _ __ __ 9/16/2003 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/23/2004 c5 c5 c5 c5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 Dry - - -- - -- -- -- - - -- 8/29/2006 Dry _-- 9/27/2007 Dry _-- 5/13/2009 Dry -- - -- - -- -- -- - 12/13/2013 Dry 12/8/2014 Dry-- 10/22/2015 Dry-- 11/17/2016 Dry-- 2/1/2017 Dry-- 10/13/2017 Dry-- 11/29/2017 Dry-- 11/7/2018 <1 c1 <1 <1 12 <20 <i <1 c1 c1 <1 <1 <1 <1 <1 <1 c1 <3 <5 1/10/2019 <1 c1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 9/18/2019 Drry SW-2 4/30/1997 ND ND ND ND ND ND 3J S ND ND ND ND ND ND ND ND ND ND ND 7/15/1998 ND ND ND ND ND ND 6 12 ND ND ND ND ND ND ND ND ND ND ND 11/2/2000 <5 c5 <5 <5 420 NA <5 10 <10 ND <5 <5 <5 <5 <5 <5 <10 c10 ND 9/14/2001 <5 c5 <5 <5 353 <10 <5 7.6 c10 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 c5 <5 <5 258 c10 <5 7.7 c10 ND <5 <5 <5 <5 <5 <5 <10 <5 c10 11/26/2002 NA NA NA NA 293 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 c5 c5 c5 c5 305 c10 c5 9.6 c10 ND c5 c5 c5 c5 c5 c5 c10 c5 c10 11/16/2004 <5 <5 <5 <5 233 <10 <5 8.7 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 <5 <5 <5 <5 64 14.7 <5 6.2 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/29/2006 <1 <1 <1 <1 218 <5 <1 9.1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND Split(8270) 8/29/2006 NA NA NA NA 390 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/27/2007 <1 <1 <1 <1 176 <5 <1 9.4 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND 5/13/2009 <i <1 <1 ,1 17.1 7.1 <1 3.8 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <5 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 11/3/2011 <0.5 <0.5 <0.5 <0.5 6.2 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 11/20/2012 Dry -- - - -- - - -- -- 12/13/2013 Dry _ _ _ 12/8/2014 Dry - - - -- -- p8i7u6 -- - - -- -- - - -- - - -- -- 10/22/2015 Dry -- - - -- - - -- -- 11/17/2016 Dry _ _ _ 2/1/2017 Dry -- - - -- - - -- -- 10/13/2017 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 11/29/2017 Dry - -- - - -- - - -- -- 11/7/2018 <i <1 <1 <1 22 <20 <1 <i <1 <1 <i <1 <1 <1 <1 <1 <1 <3 <5 1/10/2019 <1 <1 <1 <1 15 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 9/18/2019 Dry Southern Intermittent Sti SW-3 4/30/1997 66 73 33 6 ND ND 3" ND 51 ND ND 110 4J 41 ND 21 19 ND ND 7/15/1998 ND 5 ND ND NA ND ND ND ND ND 4J ND ND ND ND ND ND ND ND 11/2/2000 24 38 14 c5 600 B NA c5 c5 c10 ND 45 10 c5 c5 c5 c5 c10 c10 ND 9/14/2001 <5 <5 c5 <5 281 c10 c5 c5 c10 ND c5 c5 c5 c5 c5 c5 <10 <5 ND 9/24/2002 <5 14.6 5.1 <5 69.7 c10 <5 <5 c10 ND 17.0 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA 151 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/16/2003 13 42.4 16.8 <5 202 c10 <5 <5 c10 ND 50.4 7.2 c5 c5 <5 c5 <10 <5 <10 8/23/2004 c5 13.3 <5 <5 546 c10 c5 8.7 16.4 ND 6.9 <5 c5 c5 <5 <5 <10 <5 c10 8/25/2004 c5 31.7 9 <5 115 c10 c5 <5 c10 ND 33.6 <5 c5 <5 <5 <5 <10 <5 <10 12/20/2005 39.1 96.3 50 <5 26.3 c10 c5 c5 c10 ND 182 111 c5 c5 <5 c5 20.7 <5 c10 8/29/2006 11.8 59.3 24 3.5 327 <5 c1 c1 3.2 ND 88.6 5.2 1.1 c1 <1 1.7 7.4 <2 ND 9/27/2007 Dry - -- -- - - -- - - -- -- 5/13/2009 32.3 84.1 52.4 4.1 144 10.2 2.5 1.4 10.5 c1 178 7.6 2.1 <1.0 c1.0 7.8 28.5 <1 <5 4/1/2010 21.7 52.6 36.6 <1.0 66.9 8.01 1.69 1.01 11.2 <1.0 127 51 1.32 <1.0 c1.0 5.58 23.7 ND c5.0 11/3/2011 20.6 37.3 24 1.58 38 c5 c0.5 c0.5 19.9 <0.5 76.5 4.79 <0.5 <0.5 c0.5 10.6 25 c0.5 <5 11/20/2012 27.1 50.7 29.3 <0.5 115 c5 c0.5 0.62 19 <0.5 105 1.31 2.62 <0.5 0.58 14 23.2 c0.5 <5 12/11/2013 28.7 26.6 33.2 0.74 10 <5 1.83 0.73 10.4 <0.5 85.1 c0.5 1.4 <0.5 0.75 14.6 18.8 c0.5 <5 12/8/2014 8.2 22 10 <1 96.8 c5 <1 c1 8.8 c1 42 15 1.2 c1 <1 4.8 11 <3 <5 10/22/2015 27 81 37 2.7 104 c5 0.88 J ci 24 c1 140 81 4.8 c1 0.87 J 19 28 c3 c5 11/17/2016 <1 c1 <1 <1 16 28 J <1 <1 c1 c1 0.44 J <1 c1 c1 <1 c1 <1 c3 c5 2/1/2017 NA NA NA NA 12 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 10/13/2017 <1 c1 <1 <1 9.7J c20 <1 <1 c1 c1 <1 <1 <1 <1 <1 <1 <1 <3 <5 11/29/2017 NA NA NA NA 15 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 11/7/2018 <1 1.2 c1 c1 13 c20 <1 <1 c1 c1 2.3 <1 c1 <1 <1 c1 c1 <3 <5 9/18/2019 ci <1 c1 c1 1.7 c20 ci ci c1 c1 <1 <1 <1 <1 <1 <1 <1 <3 <1 SW-4 4/30/1997 4J/5J 30/34 3J/3J 3J/4J NDMD 12JI23J 1J/iJ 62169 15J/16J ND NDMD 10111 ND/ND NDMD ND/ND NDMD 8J/9J ND/ND ND/ND 7/20/1998 ND 16 ND 4J NA ND ND 77 36 ND ND ND ND ND ND ND ND ND ND 11/2/2000 c c c c 1100NA c5 48 34 ND c5 c5 c5 c5 <5 <5 10 <10 ND 9/14/0 5 5 5 5 806 c10 5 16.5 <10 ND 5 5 5 5 ccc1201 5 5 0 <5 ND 9/24/2002 <5 c5 <5 <5 480 c10 <5 19.3 c10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA 448 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 <5 7.7 <5 <5 118 11 <5 12.2 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 c10 8/25/2004 <5 c5 c5 <5 592 c10 <5 38.0 18.2 ND <5 <5 Ic5 <5 <5 <10 <5 c10 12/20/2005 6.4 24.9 7.3 <5 172 17.3 <5 22.4 c10 ND 36.5 5.8 c5 c5 <5 I <10 <5 c10 8/29/2006 <1 1.2 c1 <1 1040 <5 <1 9.5 8.1 ND <1 <1 c1 <1 <1 <1 c1 <2 ND Split(8270) 8/29/2006 NA NA NA NA 1200 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/27/2007 <1 c1 <1 c1 24.1 <5 ci ci c1 ND ci ci c1 c1 ci c1 c1 c2 ND 5/13/2009 ci c1 c1 c1 8.4 8.4 ci ci c1 1.7 ci ci c1 c1 ci c1 c1 c1 <5 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 c1.0 c1.0 <1.0 <1.0 <1.0 <1.0 <1.0 c1.0 <1.0 <1.0 ND <5.0 11/3/2011 72 443 126 32.6 110 10.6 14.2 358 141 <0.5 440 1.21 3.24 0.74 c0.5 13.5 371 4.93 <5 11/20/2012 <0.5 2.1 c0.5 c0.5 22.7 c5 c0.5 5.9 c0.5 <0.5 1.56 c0.5 c0.5 <0.5 c0.5 <0.5 <0.5 c0.5 <5 12I13/2013 <0.5 <0.5 c0.5 c0.5 c2.0 c5 c0.5 c0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 c0.5 <0.5 <0.5 c0.5 <5 12/8/2014 ci c1 c1 c1 3.3 <5 <1 <1 c1 c1 c1 <1 <1 <1 ci c1 c1 c3 c5 10/22/2015 ci c1 c1 <1 4.1 J <5 ci 0.82 J c1 c1 ci <1 c1 <1 ci c1 c1 c3 c5 11/21/2016 <1 <1 <1 <1 18 <10 ci 1.3J 0.70J c1 <1 <1 c1 <1 <1 <1 <1 <3 <5 2/1/2017 NA NA NA NA <2.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 10/13/2017 86 710 280 63 1700 c200 20 840 120 <10 1100 c10 6.7 J 4.8 J 4.3 J 4.1 J 1000 9.1 <0 11/29/2017 120 770 370 58 1500 c200 24 950 65 <10 1400 c10 15 6.7 4.1 22 970 14 <50 11/7/2018 <1 25 13 2.5 48 120 <1 23 2.4 <1 40 <1 <1 <1 <1 <1 45 <3 <5 9/18/2019 51 400 120 34 1800 c200 <10 820 250 <10 540 1 c10 4.4 4.9 J 7.1 J 420 7.7 J <0 TABLE 3 Page 2 of 3 SURFACE WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL SITE x Sample s s s 0 0 n 1P m s 0 Descri [ion Sample Date o 0 0 'o 00 0 'o o 'o 0 - m W p o o W 0 o 0 D 3 0 3 � 0 $ z o - T 0 o s g > W 1 A 0 > e � a a 1D o 0 (u /I) (u /I u /I a' (a/I N3 u /I u /I u /I u /I u /I u /I u /I u /I ua/I a /I u /I (a/I u /I u /I u /I NC 2B Std. S.IV) 2500 6700 330 0.38 0.35 2000 1.19 130 12 NE 330 2.6 0.7 11 140 2.5 0.025 670 20,000 SW-5 4/30/1997 ND ND ND ND ND 8J ND ND ND ND ND ND ND ND ND ND ND ND ND 11/2/2000 15 <5 <5 <5 <100 NA <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <10 ND 9/14/2001 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/16/2003 <5 <5 <5 <5 12.4 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/25/2004 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/29/2006 <1 <1 <1 <1 <2 51.7 <1 <1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND 9/27/2007 <1 <1 <1 <1 <2 <5 <1 <1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND 5/13/2009 8.7 8.6 6.4 <1 25.4 5.3 <1 <1 <1 <1 39.4 <1 3.3 <1 <1 9.0 8.2 <1 <5 4/1/2010 11.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 11 /3/2011 <0.5 <0.5 <0.5 <0.5 <3.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 11/20/2012 <0.5 <0.5 <0.5 <0.5 6.97 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 12/16/2013 <0.5 <0.5 <0.5 <0.5 13.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 10.5 12/8/2014 <1 <1 <1 <1 2.26 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 10/22/2015 <1 <1 <1 <1 1.8 J <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 11/17/2016 <1 <1 <1 <1 3.1 J <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 2/1/2017 NA NA NA NA 8.3 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 10/1312017 <1 <1 <1 <1 14.0 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 11/29/2017 NA NA NA NA 8.6 NA NA NA NA NA NA NA NA NA NA NA NA NA NA 11/7/2018 <1 <1 <1 <1 23.0 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 9/18/2019 1 <1 <1 <1 I <1 5.8 <20 1 <1 <i I <1 I <1 0.63 J <1 <1 <1 <1 <1 0.46 J <3 <5 Randleman Lake (rorrn.riy m. D-p Ri-) SW-6 5/1/1997 ND ND ND ND ND 6J ND ND ND ND ND ND ND ND ND ND ND ND ND 11/2/2000 <5 <5 <5 <5 <100 NA <5 <5 <10 ND <5 15 <5 <5 <5 <5 110 <10 ND 9/14/2001 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 15 <5 <5 <5 <5 <10 15 ND 9/24/2002 <5 <5 <5 <5 11.5 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 110 15 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/16/2003 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND 15 15 <5 <5 <5 <5 110 15 <10 8/25/2004 c5 <5 c5 <5 133 <10 <5 <5 c10 ND <5 <5 c5 <5 <5 <5 <10 15 <10 12/20/2005 <5 <5 <5 <5 11.4 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/29/2006 It c1 <1 <1 <2 <5 It It <1 ND It <1 c1 <1 It <1 <1 <2 ND Split(8270) 8/29/2006 NA NA NA NA <3.3 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/27/2007 <1 <1 <1 <1 <2 <5 <1 <1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND Upper 2/25/2009 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND Mid 2/25/2009 <11.0 <1.0 1.0 <1 1.0 <1 < < 1.0 <1<1 1.0 1.0 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND Mid 5/13/2009 .0 1.0 .0 .0 2.0 5.0 .0 .0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5 Upper 5/13/2009 <1.0 <1.0 <1.0 <1.0 <2.0 8.1 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <5 Surface 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Bottom 4/1/2010 <1.0 <1.0 <1.0 <1.0 4.02 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Surface 11/3/2011 <0.5 <0.5 <0.5 <0.5 <3.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Surface 11/21/2012 <0.5 <0.5 <0.5 <0.5 3.73 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Bottom 11/21/2012 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Surface 12/13/2013 <0.5 <0.5 <0.5 <0.5 9.29 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Bottom 12/13/2013 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Surface 12/15/2014 <1 <1 <1 <1 <2 <5 <1 <i <1 <1 <1 <i <1 <1 <1 <1 <1 <3 <5 Bottom 12/15/2014 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 10/22/2015 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 10/22/2015 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 11/21/2016 <1 <1 <1 <1 <2 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 11/21/2016 <1 <1 <1 <1 <2 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 2/1/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 2/1120,7 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 10/1312017 <i <1 <1 <1 13.0 <20 <i <i <1 <1 <i <i <1 <1 <i <1 <1 <3 <5 Bottom 10/13/2017 <i <1 <1 <1 14.0 <20 <i <i <1 <1 <i <i <1 <1 <i <1 <1 <3 <5 Surface 11/29/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 11/29/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 11/7/2018 <i <1 <1 <1 <2 <20 <i <i <1 <1 <i <i <1 <1 <i <1 <1 <3 <5 Bottom 11/7/2018 <1 <1 <1 <1 <2 <20 <1 <1 11 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 9/18/2019 <1 <1 <1 <1 1.6 J <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 9/18/2019 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 SW-7 5/2/1997 ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND ND 11/3/2000 <5 <5 <5 <5 <100 NA <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <10 ND 9/13/2001 <5 <5 <5 <5 40.5 <10 <5 <5 23 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/23/2004 c5 c5 c5 c5 c10 <10 c5 c5 <10 ND c5 c5 <5 <5 c5 <5 c10 c5 <10 12120/2005 <5 <5 <5 <5 <10 10.7 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/29/2006 <1 c1 <1 <1 4.3 <5 ci 2 <1 ND ci ci <1 <1 <1 <1 <1 <2 ND 9-27-200 It <1 <1 <1 23.2 5.0 It 2 <1 ND <1 <1 <1 <1 It <1 <1 <2 ND Upper 2/25/2009 c11.0 c11..0 c11..0 c11.0 c2.0 c5.0 c11.0 c11.0 <11.0 ND <11.0 <11.0 <11.0 c11.0 c1.0 c10 c1.0 c2.0 ND Mid 22009 /25/ 0 0 0 0 20 50 0 0 0 ND 10 0 0 0 10 1.0 10 20 ND Mid 5/13/2009 <1.0 <10 <10 <1.0 <2.0 5.3 <1.0 c1.0 c1.0 <1.0 <1.0 <1.0 <1.0 <1.0 c1.0 <1.0 <1.0 c1.0 <5 Upper 5/13/2009 c1.0 c1.0 c1.0 c1.0 c2.0 7.0 <1.0 c1.0 c1.0 <1.0 <1.0 <1.0 <1.0 <1.0 c1.0 <1.0 <1.0 c1.0 <5 Surface 4/1/2010 c1.0 c1.0 c1.0 c1.0 c2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 c1.0 <1.0 <1.0 ND c5.0 Bottom 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 c1.0 <1.0 <1.0 ND c5.0 Surface 11/3/2011 c0.5 c0.5 <0.5 c0.5 <3.0 c5 c0.5 c0.5 c0.5 c0.5 c0.5 <0.5 <0.5 c0.5 c0.5 c0.5 c0.5 c0.5 <5 Surface 11/21/2012 c0.5 c0.5 0.88 c0.5 9.10 c5 c0.5 1.11 c0.5 c0.5 c0.5 c0.5 c0.5 c0.5 c0.5 c0.5 c0.5 c0.5 c0.5 Bottom 11/21/2012 c0.5 c0.5 c0.5 c0.5 9.88 c5 c0.5 0.94 c0.5 <0.5 <0.5 c0.5 c0.5 <0.5 c0.5 <0.5 <0.5 c0.5 c0.5 Surface 12I13/2013 c0.5 c0.5 c0.5 c0.5 c2.0 c5 c0.5 c0.5 c0.5 <0.5 <0.5 c0.5 c0.5 <0.5 c0.5 <0.5 <0.5 c0.5 <5 Bottom 12/13/2013 <0.5 <0.5 <0.5 <0.5 <2.0 c5 <0.5 c0.5 c0.5 <0.5 <0.5 c0.5 c0.5 <0.5 c0.5 <0.5 <0.5 c0.5 <5 Surface 12/15/2014 ci c1 c1 <1 2.38 c5 ci 1.3 <1 <1 0.42 J It <1 <1 It <1 <1 13 <5 Bottom 12/15/2014 It c1 c1 <1 c2 <5 It 1.3 c1 <1 It It c1 <1 It <1 <1 13 <5 Surface 10/21015 ci c1 c1 c1 1.43 J c5 ci ci <1 <1 c1 ci c1 <1 <i <1 <1 c3 c5 Bottom 10/22/2015 ci c1 c1 <i 1.60 J c5 ci ci <1 <1 ci ci c1 <1 <i <1 <1 c3 c5 Surface 11/21/2016 It c1 c1 <1 27 c10 <1 It c1 c1 It It c1 c1 It <1 <1 <3 <5 Bottom 11/21/2016 <1 c1 c1 <1 28 c10 <1 <1 c1 c1 <1 <1 c1 c1 <1 <1 <1 <3 <5 Bottom 12,28/20,6 NA NA NA NA 10 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 2/1/2017 NA NA NA NA c2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 2/1/2017 NA NA NA NA c2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 10/13/2017 ci 11 11 11 26.0 c20 ci ci c1 c1 ci ci c1 c1 ci c1 <1 <3 <5 Bottom 10/13/2017 <1 c1 c1 <1 20.0 c20 It It c1 c1 It It c1 c1 <1 c1 <1 <3 <5 Surface 11129/2017 NA NA NA NA 8.9 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 11,29/2017 NA NA NA NA 9.1 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 11/1/2018 ci c1 c1 c1 c2 c20 ci ci <1 <1 ci <i <1 <1 ci <1 <1 c3 c5 Bottom 11/7/2018 <1 c1 c1 c1 c2 c20 ci ci <1 <1 ci <1 c1 <1 ci <1 <1 c3 c5 Surface 9/18/2019 ci c1 c1 c1 c2 c20 <1 <1 <1 <1 ci 11 c1 <1 c1 <1 <1 <3 <5 Bottom 9/18/2019 ci c1 c1 c1 c2 c20 <1 <1 <1 <1 ci 11 c1 <1 <1 <1 <1 <3 <5 TABLE 3 SURFACE WATER ANALYTICAL RESULTS - VOCs SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL SITE Page 3 of 3 c c c n �_ s x Sample m 0 Description Sample Date o 0 0 'o 0o o 'o o 0 'o 0 m c g o 0 o 3. 0 3 z o 0 o m s x q Ir y m > o ar a 1D a o o u/I ull u/l ull ull u/I u/I u/I u/I ull u/I u/I ua/I u/I u/I Ull u/l u/I u/I NC 26 Std. WS-IV 2500 6700 330 0.38 0.35 2000 1.19 130 12 NE 330 2.6 0.7 11 140 2.5 0.025 670 20,000 SW-DRP-2 11/3/2000 15 <5 <5 <5 <100 NA <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <10 ND EAST 9/14/2001 <5 6.3 <5 <5 15.3 <10 <5 5.8 <10 ND 5.7 <5 <5 <5 <5 <5 <10 <5 ND WEST 9/14/2001 <5 29.5 <5 <5 42.8 <10 <5 61.5 30.5 ND 26.4 <5 <5 <5 <5 <5 21.7 <5 ND 9/24/2002 6.6 47.0 11.8 <5 39.2 <10 <5 62.3 20.5 ND 60.3 <5 <5 <5 <5 <5 28.1 <5 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/23/2004 <5 <5 7.1 <5 145 <10 5.4 189 48.6 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 14.2 80.3 33.8 <5 82.1 <10 <5 66.4 17.7 ND 140 <5 <5 <5 <5 <5 36.1 <5 <10 8/29/2006 <1 2 <1 <1 <2 <5 <1 <1 <1 ND 3.1 <1 <1 <1 <1 <1 <1 <2 ND Split(8270) 8/29/2006 NA NA NA NA <3 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/27/2007 <1 <1 <1 <1 23.3 <5 <1 2 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND Upper 2/25/2009 <1.0 <1.0 3.0 1.9 <2.0 8.0 <1.0 1.4 <1.0 ND 7.5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND Mid 2/25/2009 <11.0 <11.0 <11.0 <1.0 <2.0 9.2 <1.0 <11.0 <11.0 ND <1.0 <1.0 <1.0 1.4 <1.0 <1.0 <1.0 <2.0 ND Mid 5/13/2009 .0 .0 .0 1.0 2.0 8.6 .0 .0 .0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5 Upper 5/13/2009 <1.0 <1.0 <1.0 <1.0 <2.0 6.9 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5 Surface 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Bottom 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Surface 11/21/2012 <0.5 <0.5 <0.5 <0.5 7.27 <5 <0.5 2.75 <0.5 <0.5 1.19 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Bottom 11/21/2012 <0.5 1.86 1.4 <0.5 11.4 <5 <0.5 6.26 6.36 <0.5 2.26 <0.5 <0.5 <0.5 <0.5 <0.5 2.54 <0.5 <0.5 Surface 12/13/2013 <0.5 <0.5 <0.5 <0.5 <2.0 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Bottom 12/13/2013 <0.5 <0.5 IS <0.5 <2.0 <5 <0.5 <0.5 <0.5 IS <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <5 Surface 12/15/2014 <1 <1 <1 <1 1.2 J <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 12/15/2014 <1 <1 <1 <1 1.62 J <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 10/2212015 <1 <1 <1 <1 3.02 J <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 10/2212015 <1 <1 <1 <1 3.11 J <5 <1 0.47 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 11/21/2016 <1 <1 <1 <1 18 <10 <1 1.3J 0.59J <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 11/21/2016 <1 <1 <1 <1 18 <10 <1 1.3J <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 12128/2016 NA NA NA NA 7.2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 2/1/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 2/1/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 10/13/2017 <1 <1 <1 <1 19.0 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 10/13/2017 <1 <1 <1 <1 21.0 <20 <1 0.53 J <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 11/29/2017 NA NA NA NA 3.4 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 11/29/2017 NA NA NA NA 3.4 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 11,7120111 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 11/7/2018 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 9/18/2019 <1 <1 <1 <1 1.4 J <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 9/8/2019 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 SW-DRP-4 11/2/2000 <5 <5 <5 <5 <100 NA <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <10 ND EAST 9/14/2001 <5 9.1 <5 <5 44 <10 <5 101 51.5 ND 8 <5 <5 <5 <5 <5 <10 <5 ND WEST 9/14/2001 <5 8.5 <5 <5 30.2 <10 <5 69.4 33.3 ND 7.4 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/24/2004 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12/20/2005 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/29/2006 <1 <1 <1 <1 <2 <5 <1 <1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND 9/27/2007 <1 <1 <1 <1 24.9 <5 <1 <1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND SW-DRP-10 11/2/2000 <5 7.5 <5 <5 <100 NA <5 14 17 ND 5.7 <5 <5 <5 <5 <5 <10 <10 ND EAST 9/13/2001 <5 6 <5 <5 43.8 <10 <5 14.4 27.7 ND <5 <5 <5 <5 <5 <5 <10 <5 ND WEST 9/13/2001 <5 6.3 <5 <5 43.5 <10 <5 19.2 30.9 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 12.6 <10 <5 7.2 7.5 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/23/2004 <5 <5 <5 <5 12 <10 <5 9.1 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12120/2005 <5 <5 <5 <5 <10 <10 <5 <10 <10 ND <5 <5 <5 <5 <5 <5 <10 c5 <10 8/29/2006 <1 <1 <1 <1 4.1 <5 <1 2.9 1.1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND 9/27/2007 <1 <1 <1 <1 22.4 <5 <1 <1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND SW-DRP-11 11/2/2000 <5 <5 <5 <5 <100 NA <5 <5 <10 ND <5 <5 <5 <5 <5 <5 c10 <10 ND 9/13/2001 <5 <5 <5 <5 10.2 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 ND 9/24/2002 <5 <5 <5 <5 109 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 50 FT UPSTREAM 11/26/2002 NA NA NA NA <10 NA NA NA NA ND NA NA NA NA NA NA NA NA NA 9/15/2003 <5 <5 <5 <5 53.5 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/23/2004 <5 <5 <5 <5 20.4 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 12120/2005 <5 <5 <5 <5 <10 <10 <5 <5 <10 ND <5 <5 <5 <5 <5 <5 <10 <5 <10 8/29/2006 <1 <1 <1 <1 3.5 5.2 <1 1.1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND 9/27/2007 <1 <1 <1 <1 17.9 <5 <1 <1 <1 ND <1 <1 <1 <1 <1 <1 <1 <2 ND Upper 2/25/2009 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND Mid 2/25/2009 <11.0 <11.0 <11.0 <11.0 <2.0 <5.0 <11.0 <11.0 <11.0 ND <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 ND Mid 5/13/2009 .0 .0 0 0 20 104 0 0 0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5 Upper 5/13/2009 <1.0 <1.0 <1.0 <1.0 <2.0 <5 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <2.0 <5 Surface 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <5.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Bottom 4/1/2010 <1.0 <1.0 <1.0 <1.0 <2.0 <10 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 <1.0 ND <5.0 Surface 11/21/2012 <0.5 <0.5 <0.5 <0.5 10.2 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Bottom 11/21/2012 <0.5 <0.5 <0.5 <0.5 9.93 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Surface 12/16/2013 <0.5 <0.5 <0.5 <0.5 <0.5 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Bottom 12/16/2013 <0.5 <0.5 <0.5 <0.5 14.4 <5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 Surface 12/11014 <1 <1 <1 <1 1.55 J <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 12/15/2014 <1 <1 <1 <1 1.53 J <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 10/22/2015 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 10/22/2015 <1 <1 <1 <1 <2 <5 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 11/21/2016 <1 <1 <1 <1 19 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 11/21/2016 <1 <1 <1 <1 17 <10 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 2/1/2017 NA NA NA NA <2 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 2/1120,7 NA NA NA NA 1.4J NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 10/13/2017 <1 <1 <1 <1 31.0 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 10/13/2017 <1 <1 <1 <1 31.0 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 11/29/2017 NA NA NA NA 20.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Bottom 11/29/2017 NA NA NA NA 20.0 NA NA NA NA NA NA NA NA NA NA NA NA NA NA Surface 11/7/2018 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 11/7/2018 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Surface 9/18/2019 <1 <1 <1 <1 1.3 J <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 Bottom 9/18/2019 <1 <1 <1 <1 <2 <20 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <1 <3 <5 ugn = mwrograms per urer = J= Estimated mine NE = Not Established B = Analyte detected in method blank as well as sample NA = Not Analyzed Bold type indiestes aalue exceeds NC 2B surface water quality standard (WS-IV) NC 2B Std. (INS -IV) = North Carolina 2B surface water quality standard far Class WS-IV waters Values separated by slash 0 indicates split sample results TABLE 4 Page 1 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Date Temperature (degrees Celsius) pH (Std. Units) Dissolved Oxygen (mg/1) Conductivity (US/Cm) Sample Identification jo Ground Water MRF-1 2/24/2009 17.0 6.1 900 MW-1 3/5/2009 14.8 3.9 194 3/31/2010 16.5 6.6 2840 11/2/2011 14.2 8.2 9.7 228 11/20/2012 13.6 9.4 3.5 458 12/9/2013 13.5 12.0 3.6 3 12/8/2014 12.1 7.8 4.6 352 10/26/2015 13.7 8.0 3.5 0 11/14/2016 14.5 7.3 3.4 287 10/11/2017 19.9 7.2 4.7 262 11/1/2018 17.8 8.1 10.5 324 9/10/2019 22.8 6.6 585 MW-2C 2/24/2009 14.4 6.6 688 MW-3B 9/26/2000 15.7 6.2 2000 9/5/2001 17.8 6.4 1930 MW-3C 9/26/2000 15.4 6.3 1520 9/5/2001 17.6 6.5 1570 9/18/2002 16.9 6.8 1820 8/17/2004 18.2 6.6 1461 2/27/2009 15.7 6.4 686 3/30/2010 17.5 7.7 2370 11/1/2011 16.4 7.8 8.3 971 11/20/2012 14.8 7.9 2.9 648 12/11/2013 11.1 6.9 19.5 4 12/11/2014 15.7 6.7 4.4 1915 10/27/2015 15.3 6.5 1.9 1284 11/14/2016 17.2 7.3 2.7 1221 10/10/2017 23.9 6.2 4.2 1096 11/2/2018 17.3 6.8 3.3 1123 9/11/2019 31.1 6.5 1555 MW-5 2/24/2009 10.5 5.2 544 MW-6 9/26/2000 15.3 6.0 559 9/6/2001 17.5 6.2 472 9/19/2002 18.1 6.5 538 8/18/2004 -- -- -- 3/3/2009 14.6 7.5 900 3/30/2010 17.4 6.9 2730 11/1/2011 17.6 8.9 7.3 40 11/19/2012 20.6 7.3 2.9 1036 12/11/2013 11.3 6.5 11.7 113 12/12/2014 14.7 6.6 3.2 1163 10/30/2015 16.0 7.1 1.3 719 11/17/2016 20.1 6.5 1.7 751 10/10/2017 22.0 7.6 3.6 692 11/2/2018 19.5 6.6 4.6 993 9/12/2019 26.7 6.9 1245 MW-7B 3/3/2009 16.2 5.9 4220 MW-8 3/5/2009 16.9 5.1 990 MW-9 9/26/2000 14.9 5.8 1.17 2/26/2009 12.4 8.0 1840 MW-10 9/26/2000 15.4 6.3 2.51 9/6/2001 16.0 6.3 2480 9/19/2002 16.1 6.7 2740 9/16/2003 17.0 6.7 1940 8/17/2004 16.0 6.4 2200 3/6/2009 14.9 6.2 932 3/29/2010 16.6 8.8 4510 11/1/2011 16.9 7.1 9.4 1058 11/19/2012 15.8 7.4 2.0 154 12/10/2013 12.8 6.5 7.9 302 12/10/2014 13.1 6.5 4.1 257 10/26/2015 15.9 7.0 1.8 1523 11/14/2016 16.6 6.7 2.3 1194 10/10/2017 20.2 6.0 3.9 905 10/31/2018 17.6 6.8 3.6 1591 9/10/2019 24.5 6.2 31 TABLE 4 Page 2 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date pH (Std. Units) (degrees Celsius) Oxygen (mg/1) (US/cm) Sample Identification MW-11 9/28/2000 17.2 6.5 5950 9/10/2001 17.3 6.7 5860 9/18/2002 16.5 7.0 5350 8/17/2004 -- -- -- 3/4/2009 14.0 6.8 2990 MW-12A 9/28/2000 17.9 6.2 747 10/30/2000 17.7 6.4 899 9/6/2001 18.7 6.5 506 9/20/2002 18.8 6.4 766 9/16/2003 21.3 6.6 521 8/18/2004 23.0 7.0 425 3/6/2009 12.1 5.0 150 4/1/2010 17.0 7.4 6660 11/2/2011 10.9 9.6 1.1 1601 11/19/2012 15.8 7.7 2.8 539 12/10/2013 12.3 6.8 7.7 317 12/11/2014 14.1 6.8 4.6 564 10/27/2015 14.7 6.8 1.6 1948 11/14/2016 16.4 7.5 3.1 1530 10/10/2017 22.2 6.4 4.4 1558 11/1/2018 18.2 6.1 1.7 1720 9/10/2019 26.7 6.5 1500 MW-12B 9/28/2000 16.9 6.2 2620 9/6/2001 17.7 6.4 2570 9/20/2002 18.1 6.3 2930 9/16/2003 18.3 6.7 2500 8/18/2004 -- -- -- 3/4/2009 11.9 7.8 2990 4/9/2010 16.6 6.2 412 11/2/2011 16.4 9.0 2.7 1418 11/19/2012 15.0 7.4 2.8 39 12/10/2013 14.8 6.4 18.5 295 12/11/2014 14.3 6.5 3.5 868 10/27/2015 14.0 6.5 1.7 1475 11/14/2016 15.3 6.6 2.9 1682 10/10/2017 22.4 6.5 3.5 1699 11/1/2018 22.1 6.7 7.8 990 9/11/2019 25.0 6.5 1695 MW-12D 9/29/2000 15.8 6.8 1110 9/12/2001 16.2 7.8 949 9/20/2002 19.5 7.6 520 3/5/2009 13.4 11.9 208 4/1/2010 19.6 9.6 91100 11/2/2011 11.2 8.4 11.5 293 11/23/2012 18.0 9.1 1.9 27 12/11/2013 12.8 7.9 18.8 379 12/11/2014 17.3 7.7 6.0 609 10/25/2015 19.3 6.7 1.8 1210 11/18/2016 14.8 8.3 3.7 358 10/11/2017 20.5 7.3 6.2 382 11/1/2018 22.2 8.7 4.7 412 9/12/2019 21.0 7.1 275 MW-15A 9/5/2001 17.5 6.3 942 9/18/2002 15.8 6.7 1150 9/17/2003 15.8 5.9 932 8/18/2004 -- -- -- 3/6/2009 15.1 6.3 427 3/31/2010 17.7 7.7 4940 11/2/2011 14.7 7.8 7.8 265 11/19/2012 14.8 7.6 2.7 237 12/10/2013 14.9 6.1 6.9 873 12/8/2014 11.6 6.6 4.9 768 10/27/2015 14.7 6.6 1.8 478 11/14/2016 14.1 6.6 2.8 760 10/11/2017 22.9 6.6 4.7 739 10/31/2018 16.3 6.8 11.2 246 9/10/2019 24.8 6.6 1515 MW-16 MW-17 3/5/2009 18.7 10.0 357 OW-DR1 9/27/2000 19.0 6.3 2120 TABLE 4 Page 3 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date pH (Std. Units) (degrees Celsius) Oxygen (mg/1) (US/cm) Sample Identification OW-DR2 9/26/2000 16.0 6.3 1850 9/10/2001 15.6 6.5 1900 2/27/2009 16.2 9.9 1760 3/30/2010 17.1 8.2 4960 11/1/2011 17.0 8.4 6.3 1060 11/23/2012 14.7 7.7 1.9 789 12/11/2013 13.2 8.4 2.9 837 12/12/2014 14.4 7.0 3.1 1918 10/30/2015 12.7 9.7 0.9 1388 11/18/2016 17.0 6.9 1.0 987 10/10/2017 20.6 6.4 3.3 1500 11/2/2018 17.1 7.6 0.8 1600 9/11/2019 23.3 7.6 900 OW-DR3 9/20/2002 16.7 6.3 2520 8/24/2004 17.6 6.7 643 3/4/2009 12.7 3.7 2460 11/26/2012 17.5 6.1 2.5 1713 12/10/2013 13.7 6.3 4.1 254 OW-DR4 9/23/2002 17.9 6.6 1720 8/24/2004 17.5 6.3 1288 2/25/2009 17.5 6.2 762 OW-LFS1 2/26/2009 15.2 6.0 3730 OW-LFS2 2/26/2009 14.5 5.4 3100 3/30/2010 17.3 8.2 9990 11/1/2011 16.9 7.7 6.2 141 11/19/2012 17.4 7.6 2.7 367 12/11/2013 12.2 6.4 8.4 668 12/12/2014 14.7 6.5 4.6 1722 10/26/2015 16.2 6.6 2.2 1302 11/14/2016 18.9 6.5 2.5 2036 10/10/2017 21.6 6.5 4.5 2093 10/31/2018 17.9 6.6 9.5 1403 9/12/2019 20.2 6.7 830 OW-NIS1 3/10/2009 20.3 4.4 2650 OW-SF1 3/9/2009 18.0 3.8 802 OW-SIS1 8/17/2004 16.2 5.8 656.4 3/9/2009 18.0 4.2 579 OW-SIS2 2/24/2009 16.0 6.1 155 OW-SIS3 3/4/2009 13.6 6.0 392 PW-2D 3/3/2009 15.2 7.8 1930 PW-3D 11/27/2012 9.3 10.0 5.0 375 12/17/2013 8.6 12.7 18.7 128 12/11/2014 14.1 8.6 1.8 572 10/25/2015 18.8 6.3 0.6 397 11/16/2016 18.1 8.5 3.7 358 10/11/2017 21.4 7.5 1.7 377 11/2/2018 19.1 7.5 1.5 457 9/11/2019 23.6 8.0 762 PW-41 9/28/2000 21.8 6.3 2010 9/11/2001 19.7 6.4 1710 9/19/2002 20.8 6.5 1890 8/23/2004 20.4 3.1 1719 3/5/2009 17.5 4.4 2160 4/2/2010 16.6 7.6 1860 11/2/2011 24.4 8.0 0.2 1017 11/20/2012 18.9 7.2 2.0 920 12/17/2013 12.1 6.7 19.6 807 12/8/2014 13.9 6.3 1.5 1516 10/29/2015 20.5 6.8 0.8 1675 11/17/2016 21.1 6.0 1.6 1399 10/11/2017 22.7 6.4 1.5 857 11/2/2018 21.5 6.5 1.9 1686 9/11/2019 24.2 6.4 1857 TABLE 4 Page 4 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date pH (Std. Units) (degrees Celsius) Oxygen (mg/1) (US/cm) Sample Identification PW-5D 9/26/2000 15.8 6.4 1620 9/10/2001 16.0 6.7 1590 9/23/2002 16.3 6.8 1610 8/18/2004 16.5 6.4 1293 3/27/2009 16.3 6.3 797 3/30/2010 17.2 8.4 1690 11/3/2011 17.3 8.4 8.3 1044 11/23/2012 15.8 8.2 1.9 790 12/16/2013 10.4 6.8 18.3 995 12/11/2014 14.9 7.0 2.8 1609 10/30/2015 15.8 7.8 1.3 955 11/18/2016 15.3 6.9 1.1 927 10/10/2017 20.3 6.8 2.4 1335 11/2/2018 17.6 7.8 2.9 1658 9/11/2019 25.6 7.6 920 PW-6D 10/2/2000 16.5 7.7 320 9/12/2001 15.4 8.0 472 9/19/2002 15.9 8.1 356 8/25/2004 15.7 7.9 276 3/18/2009 16.7 7.3 363 3/31/2010 17.4 7.4 408 New Well 12/10/2014 13.1 8.2 4.6 564 10/30/2015 20.5 8.2 1.2 263 11/17/2016 17.6 7.7 1.4 410 10/10/2017 19.0 7.3 4.3 1100 11/1/2018 16.6 7.6 7.1 918 9/12/2019 25.2 7.5 904 PW-61 10/2/2000 15.9 6.2 573 9/12/2001 14.5 6.2 816 9/19/2002 15.3 6.3 631 8/25/2004 15.1 6.3 544 3/4/2009 13.5 6.2 404 3/31/2010 17.9 6.0 1020 New Well 12/10/2014 11.0 7.6 3.5 1521 10/27/2015 14.7 6.7 1.5 1201 11/17/2016 14.6 6.8 1.9 1155 10/10/2017 22.1 6.4 3.6 1178 11/1/2018 17.3 6.5 0.7 1157 9/12/2019 21.8 6.0 1517 PW-71 9/28/2000 19.3 6.9 2230 9/12/2001 16.6 6.6 3190 9/20/2002 16.2 6.7 3250 8/20/2004 19.6 6.6 2666 3/4/2009 13.8 5.2 3010 PW-8S 9/27/2000 15.5 6.3 1130 9/6/2001 19.0 6.5 1040 9/17/2003 17.4 6.2 2080 8/17/2004 20.0 6.3 1628 3/3/2009 14.1 9.7 1670 PW-91 9/27/2000 19.2 7.0 1860 3/12/2009 19.0 5.4 1410 PW-10D 9/26/2000 15.1 8.3 703 9/11/2001 15.5 6.9 769 9/18/2002 19.8 9.8 354 8/17/2004 18.0 9.3 235 3/29/2010 18.1 9.9 920 11/1/2011 19.3 7.7 6.8 53 11/21/2012 14.3 12.8 4.7 103 12/11/2013 13.3 12.0 4.6 120 12/10/2014 13.6 9.8 4.6 342 11/3/2015 17.7 7.1 2.7 1225 11/17/2016 17.5 9.9 2.1 259 10/10/2017 21.3 7.3 4.6 285 10/31/2018 23.3 9.9 4.9 250 9/12/2019 24.9 9.9 298 TABLE 4 Page 5 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date pH (Std. Units) (degrees Celsius) Oxygen (mg/1) (US/cm) Sample Identification PW-101 9/26/2000 16.7 6.1 787 9/11/2001 15.6 6.2 1080 9/18/2002 16.0 6.4 1210 8/17/2004 15.9 6.3 1192 3/12/2009 16.5 3.7 2110 3/29/2010 15.6 7.7 3960 11/1/2011 17.4 7.9 6.1 1123 11/19/2012 15.0 7.3 1.9 1693 12/11/2013 11.9 6.5 7.2 973 12/10/2014 14.3 6.4 2.7 214 10/29/2015 19.7 8.1 2.5 1356 11/17/2016 17.3 6.2 1.7 1529 10/10/2017 22.5 6.9 2.8 930 11/1/2018 16.3 7.3 11.8 62 9/12/2019 22.2 6.2 2000 PW-111 9/29/2000 16.3 6.9 649 9/11/2001 17.2 7.2 722 9/18/2002 19.1 8.1 618 8/25/2004 19.1 7.8 294 3/5/2009 16.1 1 5.2 929 PW-121 10/2/2000 23.1 7.1 659 9/11/2001 15.9 6.5 554 9/19/2002 17.6 6.7 689 8/17/2004 17.3 5.8 525 8/22/2006 16.9 5.5 90 3/3/2009 13.9 6.1 752 3/31/2010 17.0 6.4 634 11/2/2011 21.3 8.9 1.5 47 11/20/2012 16.3 8.1 3.4 152 12/17/2013 11.8 7.0 8.8 160 12/12/2014 11.7 7.1 9.2 880 10/30/2015 15.8 7.2 2.9 650 11/21/2016 16.1 6.7 2.7 597 10/11/2017 21.3 6.5 8.9 660 11/6/2018 19.1 7.2 3.4 816 9/11/2019 25.5 6.3 1022 PW-131 9/29/2000 17.5 6.7 1100 9/12/2001 18.3 6.9 937 9/20/2002 18.4 7.2 999 9/23/2003 17.8 6.3 890 8/25/2004 17.8 7.0 896 3/4/2009 16.5 6.7 483 3/31/2010 18.5 8.1 1640 11/3/2011 12.1 9.5 6.3 780 11/23/2012 19.2 8.4 1.7 1323 12/16/2013 13.1 6.8 8.7 319 12/12/2014 17.5 6.9 2.9 1450 10/26/2015 16.9 6.9 1.0 1701 11/18/2016 18.0 6.9 1.3 976 10/11/2017 19.8 6.8 3.0 791 10/31/2018 17.7 7.1 10.1 1003 9/11/2019 24.7 6.9 1247 PW-14D 10/31/2000 23.0 12.2 6.91 9/10/2001 19.3 12.7 6,720 8/19/2004 19.2 12.2 4941 8/22/2006 20.5 12.8 613 3/11/2009 18.9 9.7 6400 3/31/2010 16.0 12.0 6640 11/7/2011 14.8 9.6 7.5 1253 11/27/2012 13.3 12.7 2.8 1776 12/12/2013 9.5 7.0 2.6 629 12/9/2014 16.8 12.1 5.2 381 11/3/2015 18.1 9.1 1.7 340 11/16/2016 15.6 13.1 2.0 3999 10/12/2017 18.8 6.9 5.1 612 11/5/2018 19.2 12.7 2.0 4246 9/17/2019 26.0 12.5 365 PW-14S 10/30/2000 17.7 6.0 130 9/6/2001 17.8 6.3 185 8/19/2004 16.8 5.9 95 8/22/2006 16.8 5.1 185 3/10/2009 15.7 4.0 68 TABLE 4 Page 6 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date pH (Std. Units) (degrees Celsius) Oxygen (mg/1) (US/cm) Sample Identification PW-15D 10/31/2000 15.5 6.8 1.46 9/6/2001 16.8 6.7 1.68 9/16/2003 16.3 7.5 730 8/19/2004 -- -- -- 8/23/2006 16.0 6.3 1.6 3/11/2009 19.0 4.0 79 3/30/2010 15.9 6.2 1950 11/7/2011 11.1 6.3 8.1 95 11/26/2012 17.3 6.3 1.1 1204 12/12/2013 9.4 6.9 7.0 727 12/9/2014 16.1 7.0 2.8 1628 10/28/2015 18.7 7.1 1.0 966 11/15/2016 17.3 7.8 2.4 867 10/12/2017 18.1 6.9 2.8 738 11/5/2018 15.9 7.5 0.7 1360 9/17/2019 21.1 7.2 920 PW-15S 10/30/2000 16.7 6.4 467 9/6/2001 16.3 7.2 648 8/19/2004 -- -- -- 8/23/2006 17.9 6.5 604 3/11/2009 17.6 1 4.5 432 PW-16D 11/2/2000 17.1 7.4 85.7 9/6/2001 15.7 7.3 96 8/19/2004 16.5 7.2 845 8/23/2006 15.8 6.7 125 3/11/2009 19.1 3.8 633 3/30/2010 15.4 6.6 1280 11/7/2011 16.8 8.2 6.1 460 11/26/2012 19.8 6.8 1.6 926 12/12/2013 8.4 7.8 9.7 365 12/9/2014 15.2 7.7 2.9 1327 10/28/2015 18.6 7.1 0.8 815 11/15/2016 18.0 8.4 1.7 709 10/12/2017 18.8 7.8 3.2 1364 11/5/2018 16.3 7.4 2.4 619 9/12/2019 22.5 7.2 689 PW-16S 10/30/2000 17.4 6.3 347 9/6/2001 17.6 6.3 499 8/19/2004 17.2 6.3 291 8/23/2006 18.6 6.8 416 PW-17 11/3/2000 18.8 6.4 44.4 9/12/2001 18.3 6.5 364 9/18/2002 16.8 6.6 424 8/19/2004 17.3 6.6 447 3/5/2009 15.9 7.4 242 PW-18 11/3/2000 15.6 10.3 44.2 9/10/2001 17.3 11.2 853 9/16/2003 16.8 12.9 9040 8/19/2004 -- -- -- 8/22/2006 18.5 13.1 121 3/11/2009 20.3 8.7 1310 3/31 /2010 17.7 12.2 12200 11/8/2011 7.7 6.1 9.6 954 11/26/2012 15.1 12.0 3.1 393 12/12/2013 10.6 12.5 8.7 66 12/9/2014 14.1 12.2 7.6 1134 10/26/2015 15.5 12.7 4.3 1102 11/15/2016 17.2 13.5 7.3 3999 10/16/2017 16.7 12.8 7.9 1217 11/7/2018 17.5 12.7 4.8 1210 9/17/2019 Not Sampled PW-19 11/6/2001 15.3 7.2 268 9/18/2002 18.6 7.5 387 9/16/2003 11.8 8.9 483 8/17/2004 16.2 7.8 450 3/10/2009 17.1 9.2 299 PW-DR1 2/25/2009 13.6 6.2 1950 PW-SIS1 8/19/2004 15.7 6.8 536 3/9/2009 17.2 5.8 210 TABLE 4 Page 7 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date pH (Std. Units) (degrees Celsius) Oxygen (mg/1) (US/cm) Sample Identification PW-SF1 4/2/2010 17.6 8.8 3960 11/3/2011 18.6 8.7 3.4 896 11/20/2012 14.9 7.6 1.8 147 12/9/2013 14.9 6.8 11.3 39 12/8/2014 14.5 6.7 3.4 1272 10/27/2015 14.1 6.8 3.1 1656 11/17/2016 15.9 6.9 1.6 845 10/11/2017 18.3 6.4 3.3 819 10/31/2018 17.2 6.4 0.5 392 9/10/2019 24.6 6.0 218 RW-LFS1 2/26/2009 14.8 6.0 3010 RW-LFS2 2/26/2009 15.7 6.2 2460 RW-NIS1 3/6/2009 15.0 5.1 3190 RW-SIS2 3/9/2009 17.7 3.8 160 RW-SIS3 3/4/2009 15.6 6.0 681 RW-SIS4 3/4/2009 12.7 6.1 97 RW-SIS5 3/4/2009 12.5 6.7 425 RW-SIS6 3/4/2009 15.2 6.3 322 W-1 9/27/2000 16.2 6.5 330 9/10/2001 17.5 6.6 296 9/18/2002 17.1 6.6 307 9/17/2003 17.6 6.3 448 8/17/2004 17.1 6.8 390 3/3/2009 16.4 6.9 484 W-4 9/27/2000 14.9 6.5 267 9/10/2001 16.0 6.6 263 9/17/2002 18.4 6.9 342 9/17/2003 16.5 6.1 290 8/17/2004 18.4 6.0 248 W-4A 9/27/2000 14.7 6.5 612 9/10/2001 15.1 6.5 773 9/14/2002 15.5 6.4 653 9/17/2003 14.5 6.1 434 8/17/2004 15.5 6.4 475 2/27/2009 18.6 6.2 223 3/31/2010 15.6 7.6 52100 11/2/2011 14.7 9.0 1.0 695 11/19/2012 14.5 7.6 3.4 32 12/17/2013 10.8 6.5 9.5 546 12/8/2014 12.5 6.6 4.2 1006 10/27/2015 14.3 6.7 1.8 234 11/16/2016 16.3 7.6 1.3 356 10/11/2017 21.9 6.6 4.1 383 10/31/2018 17.3 6.6 10.0 13 9/11/2019 23.2 7.1 337 W-5 9/27/2000 15.7 6.4 2530 10/30/2000 15.3 6.3 2580 9/10/2001 15.9 6.4 2170 9/18/2002 16.1 6.9 2060 8/18/2004 -- -- -- 3/3/2009 14.1 6.3 556 W-6A 9/28/2000 17.1 5.9 4950 W-18 3/5/2009 14.6 6.1 361 W-21 9/28/2000 14.3 6.0 343 9/10/2001 14.8 6.6 310 9/17/2002 15.5 6.7 342 9/17/2003 14.9 6.1 360 8/17/2004 16.8 6.5 292 2/24/2009 13.4 6.6 900 W-23A 3/4/2009 11.8 6.4 426 W-24 3/5/2009 TABLE 4 Page 8 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Date Temperature (degrees Celsius) pH (Std. Units) Dissolved Oxygen (mg/1) Conductivity (US/Cm) Sample Identification Surface Water SW-1 6.7 175 11/2/2000 10.4 9/14/2001 20.1 6.4 153 9/24/2002 Dry -- -- 9/16/2003 19.9 6.8 119 8/23/2004 20.2 7.4 59 10/22/2015 Dry 11/21/2016 Dry 10/13/2017 Dry 11/7/2018 12.8 7.9 6.7 177 9/18/2019 Dry SW-2 11/2/2000 16.6 7.2 2070 9/14/2001 21.2 7.1 1640 9/24/2002 20.9 5.8 1870 9/15/2003 21.8 7.2 2160 8/23/2004 24.8 7.3 98 8/22/2006 20.8 7.0 226 4/1/2010 15.3 7.5 103 11/3/2011 14.3 8.4 378 11/20/2012 Dry 12/11/2013 Dry 12/8/2014 Dry 10/22/2015 Dry 11/21/2016 Dry 10/13/2017 21.7 7.8 5.3 112 11/7/2018 14.7 7.7 7.1 251 9/18/2019 Dry SW-3 11/2/2000 11.0 8.0 359 9/14/2001 20.1 7.3 199 9/24/2002 19.3 6.7 3450 9/16/2003 19.7 7.3 244 8/25/2004 23.1 8.1 133 8/22/2006 23.2 7.5 480 4/1/2010 15.6 7.6 6850 11/3/2011 10.6 8.9 11.1 261 11/20/2012 11.1 9.1 6.0 35 12/11/2013 5.5 9.0 1.6 144 12/8/2014 10.2 8.4 16.2 108 10/22/2015 16.6 7.5 4.8 224 11/17/2016 12.7 7.7 2.2 1577 10/13/2017 19.1 7.4 2.2 246 11/7/2018 19.2 7.9 6.6 298 9/18/2019 21.8 7.7 323 SW-3A 8/25/2004 21.9 8.1 126 SW-3B 8/25/2004 21.9 7.7 123 SW-4 11/2/2000 12.8 6.9 964 9/14/2001 19.9 7.2 771 9/15/2003 25.0 7.5 473 8/25/2004 22.9 7.5 452 8/22/2006 22.2 7.3 112 4/1/2010 14.9 7.7 102 11/3/2011 14.5 7.7 6.1 671 11/20/2012 11.5 9.1 5.6 22 12/13/2013 4.2 8.8 9.5 1 12/8/2014 7.2 8.3 17.4 147 10/22/2015 15.8 8.4 4.8 0 11/21/2016 9.8 8.1 4.0 206 10/13/2017 19.9 6.3 8.8 878 11/7/2018 19.5 8.1 6.3 252 9/18/2019 21.2 6.5 1285 TABLE 4 Page 9 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date pH (Std. Units) (degrees Celsius) Oxygen (mg/1) (US/cm) Sample Identification SW-5 11/2/2000 14.7 6.9 415 9/14/2001 19.7 6.7 295 9/24/2002 19.7 6.7 295 9/16/2003 20.6 7.0 300 8/25/2004 21.1 7.5 168 8/22/2006 22.2 7.5 540 4/1/2010 17.1 7.4 6760 11/3/2011 11.9 9.6 9.9 212 11/20/2012 11.5 9.1 5.6 22 12/16/2013 8.7 8.5 9.7 78 12/8/2014 7.7 10.1 11.0 229 10/22/2015 16.3 7.3 4.9 199 11/17/2016 10.2 7.8 4.8 320 10/13/2017 19.0 7.4 9.2 314 11/7/2018 14.9 7.8 6.1 217 9/18/2019 22.0 9.1 311 SW-6 11/2/2000 11.4 7.5 215 9/14/2001 22.4 6.9 133 9/24/2002 22.4 7.5 168 9/16/2003 21.5 7.4 117 8/25/2004 26.4 8.2 82 8/22/2006 25.7 7.7 168 4/1/2010 14.3 8.3 103 11/3/2011 14.5 10.3 6.8 326 shallow-1' 11/21/2012 8.1 9.0 5.4 8 deep-8.5' 11/21/2012 8.7 9.3 5.2 79 shallow - 1' 12/13/2013 5.2 8.2 9.8 45 deep - 11' 12/13/2013 5.6 8.3 9.5 26 shallow - 1' 12/15/2014 9.0 8.6 13.9 212 deep - 8.6' 12/15/2014 9.1 8.7 13.3 279 shallow - 1' 10/22/2015 21.6 7.5 3.9 127 deep - 8.6' 10/22/2015 20.3 7.4 4.1 97 shallow-1' 11/21/2016 12.2 8.0 4.4 154 deep-8.5' 11/21/2016 11.9 7.9 4.2 151 shallow - 1' 10/13/2017 22.5 9.4 13.6 303 deep - 10.2' 10/13/2017 22.0 9.2 13.3 293 shallow - 1' 11/7/2018 18.1 9.9 7.3 197 deep - 11.0' 11/7/2018 17.8 9.5 7.3 100 shallow - 1' 9/18/2019 24.4 8.1 177 deep - 10' 9/18/2019 24.6 8.6 163 SW-7 11/3/2000 9.0 6.3 319 9/13/2001 20.3 6.8 220 9/24/2002 21.8 6.6 263 9/15/2003 23.8 7.0 156 8/23/2004 25.5 7.2 85 4/1/2010 13.4 7.4 103 11/3/2011 11.8 9.0 13.3 84 shallow-1' 11/21/2012 10.5 9.1 6.4 58 deep -11.5' 11/21/2012 10.7 9.0 6.8 319 shallow - 1' 12/13/2013 6.6 8.2 9.1 18 deep - 13' 12/13/2013 6.4 8.2 9.6 4 shallow - 1' 12/15/2014 10.5 8.6 13.4 186 deep - 12.3' 12/15/2014 11.1 8.4 13.8 179 shallow - 1' 10/22/2015 18.6 8.6 5.4 75 deep - 12.1' 10/22/2015 18.3 8.6 5.5 64 shallow-1' 11/21/2016 10.5 8.0 4.4 262 deep -12' 11/21/2016 9.7 9.2 5.7 276 shallow - 1' 10/13/2017 23.3 8.6 13.8 338 deep - 13.0' 10/13/2017 22.3 8.3 13.5 318 shallow - 1' 11/7/2018 17.8 8.7 6.9 82 deep - 16.0' 11/7/2018 17.8 8.7 6.4 80 shallow - 1' 9/18/2019 26.2 8.5 216 deep - 19.5' 9/18/2019 24.7 8.2 169 TABLE 4 Page 10 of 10 FIELD PARAMETER DATA - GROUND WATER AND SURFACE WATER SEABOARD CHEMICALIRIVERDALE DRIVE LANDFILL JAMESTOWN, NORTH CAROLINA Temperature Dissolved Conductivity Date pH (Std. Units) (degrees Celsius) Oxygen (mg/1) (US/cm) Sample Identification SW-DRP-2 11/3/2000 13.5 6.5 1870 East 9/14/2001 20.3 7.0 224 West 9/14/2001 20.5 6.9 239 9/15/2003 23.1 7.1 150 8/23/2004 22.0 3.7 386 4/1/2010 14.1 7.8 102 11/3/2011 11.5 8.8 10.9 140 shallow-1' 11/21/2012 10.2 8.9 5.9 43 deep -12.5' 11/21/2012 9.9 9.1 5.6 67 shallow - 1' 12/13/2013 5.8 8.2 9.4 10 deep - 10' 12/13/2013 5.7 6.9 9.9 28 shallow - 1' 12/15/2014 10.2 8.7 16.5 176 deep - 12.3' 12/15/2014 10.2 8.5 16.3 176 shallow - 1' 10/22/2015 15.9 8.1 6.3 0 deep - 12.3' 10/22/2015 16.0 8.1 6.4 0 shallow-1' 11/21/2016 9.7 8.1 3.7 203 deep -12' 11/21/2016 9.6 7.9 6.6 206 shallow - 1' 10/13/2017 23.3 8.5 16.5 324 deep - 14.2' 10/13/2017 21.7 8.6 16.3 334 shallow - 1' 11/7/2018 18.9 9.1 6.7 97 deep - 12.0' 11/7/2018 17.9 8.8 6.5 83 shallow - 1' 9/18/2019 24.8 7.7 300 deep -10' 9/18/2019 25.0 8.3 159 SW-DRP-4 11/3/2000 13.1 6.3 544 East 9/14/2001 18.8 6.1 286 West 9/14/2001 17.7 6.8 237 9/15/2003 23.4 7.1 182 SW-DRP-10 11/2/2000 12.6 6.9 306 East 9/13/2001 21.9 7.6 214 West 9/13/2001 21.4 7.2 215 9/15/2003 23.5 7.1 154 SW-DRP-11 11/2/2000 16.5 6.4 559 9/13/2001 20.4 6.4 343 9/24/2002 23.6 6.3 527 9/15/2003 25.4 6.8 357 8/23/2004 15.7 7.9 276 4/1/2010 14.0 7.3 104 11/3/2011 13.5 9.1 12.2 58 shallow-1' 11/21/2012 9.2 11.0 8.2 27 deep -9' 11/21/2012 10.3 9.3 8.3 26 shallow - 1' 12/16/2013 5.6 8.5 9.7 1 deep - 12' 12/16/2013 5.4 8.7 9.2 34 shallow - 1' 12/15/2014 7.5 8.9 16.4 164 deep - 11.6' 12/15/2014 9.3 8.8 16.9 198 shallow - 1' 10/22/2015 18.4 7.9 5.6 0 deep - 11.7' 10/22/2015 18.0 7.6 6.0 0 shallow-1' 11/21/2016 11.0 8.2 7.0 362 deep -12' 11/21/2016 11.2 8.2 2.7 398 shallow - 1' 10/13/2017 23.0 7.7 16.4 357 deep - 12.5' 10/13/2017 21.9 7.9 16.7 342 shallow - 1' 11/7/2018 17.9 8.7 6.4 87 deep - 11.5' 11/7/2018 17.8 8.9 6.7 167 shallow - 1' 9/18/2019 26.8 8.3 230 deep - 5' 9/18/2019 28.6 7.7 224 SWT-40 East @ 1' ^ 9/13/2001 21.9 7.0 219 East @ 3.25' ^ 9/13/2001 22.0 7.0 219 West @ 0.5' ^ 9/13/2001 21.8 7.0 217 SWT-50 East @ 1' ^ 9/13/2001 21.0 7.5 217 East @ 3' ^ 9/13/2001 22.1 7.0 216 West @ 1' ^ 9/13/2001 21.6 7.0 216 SWT-70 East 9/13/2001 22.0 7.1 216 West 9/13/2001 20.8 7.2 216 RCP-1 11/2/2000 15.3 6.6 277 RCP-2 11/2/2000 15.4 6.6 248 TABLE 5 MONITORING WELL LATITUDE/LONGITUDE, DEPTHS AND ELEVATIONS SEABOARD CHEMICAL/RIVERDALE DRIVE LANDFILL SITE Facility Name Seaboard Chemical/Riverdale Drive Landfill EPA ID Number NCD 071 574 164 Well ID Type Well Use Northing Easting Reference Source of Information TOC Elevation Well Depth MW-1 well monitoring 801318.45 1729231.88 state plane coord Jamestown Engineering 790.46 57.7 MW-3C well monitoring 801265.20 1731350.08 state plane coord Jamestown Engineering 692.74 57 MW-6 well monitoring 799702.65 1731990.93 state plane coord Jamestown Engineering 761.47 110 MW-10 well monitoring 800464.20 1732378.92 state plane coord Jamestown Engineering 695.01 28 MW-12A well monitoring 801788.63 1730912.94 state plane coord Jamestown Engineering 693.07 20 MW-12B well monitoring 801780.30 1730911.77 state plane coord Jamestown Engineering 693.86 58 MW-12D well monitoring 801770.20 1730908.12 state plane coord Jamestown Engineering 694.21 202 MW-15A well monitoring 800903.23 1730181.46 state plane coord Jamestown Engineering 764.33 34 OW-DR2 well monitoring 801266.66 1731357.68 state plane coord Jamestown Engineering 695.87 186 OW-DR3 well monitoring 801185.56 1731735.15 state plane coord Jamestown Engineering 702.93 160 OW-LFS-2 well monitoring 800674.15 1732093.91 state plane coord Jamestown Engineering 699.45 50 PW-3D well monitoring 800603.04 1730831.13 state plane coord Jamestown Engineering 738.60 209.5 PW-41 well monitoring 800545.88 1731099.56 state plane coord Jamestown Engineering 735.00 ** 122 PW-5D well monitoring 801164.35 1731363.53 state plane coord Jamestown Engineering 696.27 306.5 PW-6D well monitoring 801425.12 1732032.71 state plane coord Jamestown Engineering 696.79 275 PW-61 well monitoring 801415.38 1732022.44 state plane coord Jamestown Engineering 697.41 75 PW-10D well monitoring 800446.73 1732384.15 state plane coord Jamestown Engineering 697.26 200 PW-101 well monitoring 800456.28 1732373.34 state plane coord Jamestown Engineering 695.97 100 PW-121 well monitoring 799844.10 1730816.38 state plane coord Jamestown Engineering 749.48 105 PW-131 well monitoring 801310.27 1730977.69 state plane coord Jamestown Engineering 739.01 250 PW-14D well monitoring 801653.66 1731389.41 state plane coord Jamestown Engineering 686.50 * 198.8 PW-15D well monitoring 801544.36 1731748.91 state plane coord Jamestown Engineering 685.80 163.5 PW-16D well monitoring 801711.36 1732067.64 state plane coord Jamestown Engineering 686.68 179 W-4A well monitoring 1800667.98 11730625.66 state plane coord iJamestown Engineering 1712.64 138.5 I * Elevation corrected for repairs performed on PW-14D during October 2015 monitoring event. ** Elevation corrected for repairs performed on PW-41 during November 2016 monitoring event. APPENDIX A Laboratory Report 2�SENCO Laboratories 9g Accurate. Timely. Respousive. luuavative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Monday, October 7, 2019 Babb & Associates (BA024) Attn: Gary Babb 5506 Bradford Pear Court Raleigh, NC 27606 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Seaboard/Riverdale Landfill ENCO Workorder(s): CC16053 Dear Gary Babb, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Thursday, September 19, 2019. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Bill Scott Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 ofJ2 PROJECT NARRATIVE Date: October 7, 2019 Client: Babb & Associates (BA024) Project: Seaboard/Riverdale Landfill Lab ID: CC16053 Overview (� �Eo www.encolabs.com Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in the QC Remarks section below. Quality Control Samples No Comments Quality Control Remarks No Comments Other Comments In some instances, confirmation rereuns were required for 1,4-dioxane SIM analyses. Some of those reruns were beyond the 14 day holding times. In those cases both sets of data have been reported. Results were appropriately qualified. The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of the report. Released By: Environmental Conservation Laboratories, Inc. Bill Scott Project Manager FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 2 of 52 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 4401-PW15D Lab ID: CC16053-OIRE1 Sampled: 09/17/19 14:00 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 10/01/19 09/26/19 00:00 09/26/19 14:50 EPA 8260D EPA 503013_MS 10/01/19 09/26/19 13:30 09/27/19 06:51 Client ID: 4401-SW3 Lab ID: CC16053-02 Sampled: 09/18/19 09:15 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 10/02/19 09/26/19 08:42 09/26/19 19:56 EPA 8260D EPA 503013_MS 10/02/19 09/27/19 15:48 09/28/19 03:51 Client ID: 4401-SW3 Lab ID: CC16053-02RE1 Sampled: 09/18/19 09:15 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 10/02/19 10/02/19 14:07 10/03/19 03:28 Client ID: 4401-SW4 Lab ID: CC16053-03RE1 Sampled: 09/18/19 09:40 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 10/02/19 09/27/19 09:49 09/28/19 00:07 EPA 8260D EPA 5030B_MIS 10/02/19 09/30/19 14:35 10/01/19 04:24 Client ID: 4401-SW4 Lab ID: CC16053-03RE2 Sampled: 09/18/19 09:40 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 10/02/19 10/04/19 00:00 10/04/19 12:47 Client ID: 4401-SW5 Lab ID: CC16053-04 Sampled: 09/18/19 08:40 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 10/02/19 09/26/19 08:42 09/26/19 20:59 EPA 8260D EPA 503013_MS 10/02/19 09/27/19 15:48 09/28/19 05:03 Client ID: 4401-SW5 Lab ID: CC16053-04RE1 Sampled: 09/18/19 08:40 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 10/02/19 10/02/19 14:07 10/03/19 04:06 Client ID: 4401-SW6Surface Lab ID: CC16053-05 Sampled: 09/18/19 10:10 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 10/02/19 09/26/19 08:42 09/26/19 21:30 EPA 8260D EPA 503013_MS 10/02/19 09/27/19 15:48 09/28/19 05:38 Client ID: 4401-SW6Surface Lab ID: CC16053-05RE1 Sampled: 09/18/19 10:10 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 10/02/19 10/02/19 14:07 10/03/19 04:45 Client ID: 4401-SW6Bottom Lab ID: CC16053-06 Sampled: 09/18/19 10:15 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 10/02/19 09/26/19 08:42 09/26/19 22:01 EPA 8260D EPA 503013_MS 10/02/19 09/30/19 14:35 09/30/19 19:11 Client ID: 4401-SW6Bottom Lab ID: CC16053-06RE1 Sampled: 09/18/19 10:15 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 10/02/19 10/02/19 14:07 10/03/19 05:23 Client ID: 4401-SW7Surface Lab ID: CC16053-07 Sampled: 09/18/19 11:50 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 10/02/19 09/25/19 14:04 09/26/19 00:18 EPA 8260D EPA 5030B_MIS 10/02/19 09/30/19 14:35 09/30/19 19:48 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 3 Of 52 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 4401-SW7Surface Lab ID: CC16053-07RE1 Sampled: 09/18/19 11:50 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MIS 10/02/19 10/02/19 14:07 10/03/19 06:01 Client ID: 4401-SW7Bottom Lab ID: CC16053-08 Sampled: 09/18/19 11:55 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 10/02/19 09/25/19 14:04 09/26/19 00:49 EPA 8260D EPA 503013_MS 10/02/19 09/30/19 14:35 09/30/19 20:25 Client ID: 4401-SW7Bottom Lab ID: CC16053-08RE1 Sampled: 09/18/19 11:55 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 10/02/19 10/03/19 15:18 10/04/19 03:03 Client ID: 4401-SWDRP2Surface Lab ID: CC16053-09 Sampled: 09/18/19 11:15 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 10/02/19 09/25/19 14:04 09/26/19 01:20 EPA 8260D EPA 503013_MS 10/02/19 09/30/19 14:35 09/30/19 21:01 Client ID: 4401-SWDRP2Surface Lab ID: CC16053-09RE1 Sampled: 09/18/19 11:15 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 10/02/19 10/03/19 15:18 10/04/19 03:39 Client ID: 4401-SWDRP2Bottom Lab ID: CC16053-10 Sampled: 09/18/19 11:20 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 10/02/19 09/25/19 14:04 09/26/19 01:52 EPA 8260D EPA 503013_MS 10/02/19 09/30/19 14:35 09/30/19 21:37 Client ID: 4401-SWDRP2Bottom Lab ID: CC16053-IOREI Sampled: 09/18/19 11:20 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 10/02/19 10/03/19 15:18 10/04/19 04:15 Client ID: 4401-SWDRPllSurface Lab ID: CC16053-11 Sampled: 09/18/19 12:30 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 10/02/19 09/25/19 14:04 09/26/19 02:23 EPA 8260D EPA 5030B_MS 10/02/19 09/30/19 14:35 09/30/19 22:15 Client ID: 4401-SWDRPllSurface Lab ID: CC16053-11RE1 Sampled: 09/18/19 12:30 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MIS 10/02/19 10/03/19 15:18 10/04/19 04:51 Client ID: 4401-SWDRP11Bottom Lab ID: CC16053-12 Sampled: 09/18/19 12:35 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 10/02/19 09/25/19 14:04 09/26/19 02:54 EPA 8260D EPA 503013_MS 10/02/19 09/27/19 13:56 09/27/19 14:36 Client ID: 4401-PW16D Lab ID: CC16053-13RE1 Sampled: 09/17/19 11:15 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 10/01/19 09/26/19 13:30 09/27/19 07:22 EPA 8260D EPA 503013_MS 10/01/19 09/27/19 13:56 09/27/19 15:10 Client ID: 4401-PW14D Lab ID: CC16053-14 Sampled: 09/17/19 15:30 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 10/01/19 09/25/19 14:04 09/26/19 03:56 Client ID: 4401-PW14D Lab ID: CC16053-14RE1 Sampled: 09/17/19 15:30 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 10/01/19 09/27/19 13:56 09/27/19 15:45 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 4 Of 52 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 4401-TripBlank Lab ID: CC16053-15 Sampled: 09/17/19 11:15 Received: 09/19/19 09:30 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 10/01/19 EPA 8260D EPA 503013_MS 10/01/19 09/25/19 14:04 09/25/19 21:11 09/25/19 14:09 09/26/19 00:46 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 5 Of 52 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 4401-PW15D Lab ID: CC16053-01RE3 Anala Results Flag MDL POLL Units Method Notes 1,1-Dichloroethane 30 D 0.65 5.0 ug/L EPA 8260D 1,1-Dichloroethene 8.9 D 1.0 5.0 ug/L EPA 8260D 1,4-Dioxane 91 D 6.0 10 ug/L EPA 8260D Chlorobenzene 7.4 D 0.85 5.0 ug/L EPA 8260D cis-1.2-Dichloroethene 39 D 0.75 5.0 ua/L EPA 8260D I Client ID: 4401-SW3 Lab ID: CC16053-02 Anala Results Flag MDL POLL Units Method Notes 1,4-Dioxane 1.7 J 1.2 2.0 ug/L EPA 8260D QI-02 Client ID: 4401-SW3 Lab ID: CC16053-02RE1 Anala Results Flag MDL POLL Units Method Notes 1,4-Dioxane 1.6 J 1.2 2.0 ug/L EPA 8260D Q-01 Client ID: 4401-SW4 Lab ID: CC16053-03RE1 Anala Results Flag MDL POLL Units Method Notes 1,1,1-Trichloroethane 51 D 1.2 10 ug/L EPA 8260D 1,1-Dichloroethane 400 D 1.3 10 ug/L EPA 8260D 1,1-Dichloroethene 120 D 2.1 10 ug/L EPA 8260D 1,2-Dichlorobenzene 4.7 JD 1.9 10 ug/L EPA 8260D 1,2-Dichloroethane 34 D 2.1 10 ug/L EPA 8260D 1,4-Dioxane 1800 D 60 100 ug/L EPA 8260D J-05,J-06 Chlorobenzene 820 D 1.7 10 ug/L EPA 8260D Chloroethane 250 D 2.3 10 ug/L EPA 8260D cis-1,2-Dichloroethene 540 D 1.5 10 ug/L EPA 8260D o-Xylene 7.7 JD 0.65 10 ug/L EPA 8260D Tetrachloroethene 4.4 JD 1.7 10 ug/L EPA 8260D Toluene 4.9 JD 1.4 10 ug/L EPA 8260D trans-1,2-Dichloroethene 7.1 JD 2.1 10 ug/L EPA 8260D Vinyl chloride 420 D 3.2 10 ug/L EPA 8260D Xylenes (Total) 7.7 JD 4.5 30 ug/L EPA 8260D Client ID: 4401-SW4 Lab ID: CC16053-03RE2 Anala Results Flag MDL POLL Units Method Notes 1,4-Dioxane 1500 D 60 100 ug/L EPA 8260D Q-01 Client ID: 4401-SW5 Lab ID: CC16053-04 Anala Results Flag MDL POLL Units Method Notes 1,4-Dioxane 5.8 1.2 2.0 ug/L EPA 8260D QI-02 cis-1,2-Dichloroethene 0.63 J 0.15 1.0 ug/L EPA 8260D Vinyl chloride 0.46 J 0.32 1.0 ug/L EPA 8260D Client ID: 4401-SW5 Lab ID: CC16053-04RE3 Anala Results Flag MDL POLL Units Method Notes 1.4-Dioxane 2.4 1.2 2.0 uo/L EPA 8260D 0-01 Client ID: 4401-SMSurface Lab ID: CC16053-05 Anala Results Flag MDL POLL Units Method Notes 1,4-Dioxane 1.6 J 1.2 2.0 ug/L EPA 8260D QI-02 Client ID: 4401-SWDRP2Surface Lab ID: CC16053-09 Anala Results Flag MDL POLL Units Method Notes 1,4-Dioxane 1.4 J 1.2 2.0 ug/L EPA 8260D J-05,J-06 Client ID: 4401-SWDRP11Surface Lab ID: CC16053-11 Anala Results Flag MDL POLL Units Method Notes 1,4-Dioxane 1.3 J 1.2 2.0 ug/L EPA 8260D J-05, J-06 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 6 Of 52 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 4401-PW16D Lab ID: CC16053-13RE3 Anala Results Flag MDL POLL Units Method Notes 1,1,1-Trichloroethane 0.51 1 0.12 1.0 ug/L EPA 8260D 1,1-Dichloroethane 20 0.13 1.0 ug/L EPA 8260D 1,1-Dichloroethene 4.5 0.21 1.0 ug/L EPA 8260D 1,4-Dioxane 28 1.2 2.0 ug/L EPA 8260D Benzene 0.45 1 0.15 1.0 ug/L EPA 8260D Chlorobenzene 22 0.17 1.0 ug/L EPA 8260D Chloroethane 3.3 0.23 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 20 0.15 1.0 ug/L EPA 8260D Vinyl chloride 1.3 0.32 1.0 ug/L EPA 8260D Client ID: 4401-PW14D Lab ID: CC16053-14 Anala Results Flag MDL POLL Units Method Notes 1,1-Dichloroethane 0.55 1 0.13 1.0 ug/L EPA 8260D Acetone 10 1 10 20 ug/L EPA 8260D Chlorobenzene 1.4 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 0.89 1 0.15 1.0 ug/L EPA 8260D Ethylbenzene 1.6 0.13 1.0 ug/L EPA 8260D m,p-Xylenes 7.4 0.17 2.0 ug/L EPA 8260D o-Xylene 3.7 0.065 1.0 ug/L EPA 8260D Toluene 5.2 0.14 1.0 ug/L EPA 8260D Xylenes (Total) 11 0.45 3.0 ug/L EPA 8260D Client ID: 4401-PW14D Lab ID: CC16053-14RE3 Anala Results Flag MDL POLL Units Method Notes 1,4-Dioxane 1.3 1 1.2 2.0 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 7 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW15D Lab Sample ID:CC16053-01 Received: 09/19/19 09:30 Matrix: Water Sampled:09/17/19 14:00 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.85 UD ug/L 5 0.85 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF 1,1,1-Trichloroethane [71-55-6]^ 0.60 UD ug/L 5 0.60 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 1.4 UD ug/L 5 1.4 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF 1,1,2-Trichloroethane [79-00-5]^ 0.70 UD ug/L 5 0.70 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF 1,1-Dichloroethane [75-34-3]^ 30 D ug/L 5 0.65 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF 1,1-Dichloroethene [75-35-4]^ 8.9 D ug/L 5 1.0 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF 1,2,3-Trichloropropane [96-18-4]^ 1.2 UD ug/L 5 1.2 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 2.4 UD ug/L 5 2.4 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF 1,2-Dibromoethane [106-93-4]^ 3.3 UD ug/L 5 3.3 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF 1,2-Dichlorobenzene [95-50-1]^ 0.95 UD ug/L 5 0.95 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF 1,2-Dichloroethane [107-06-2]^ 1.0 UD ug/L 5 1.0 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF 1,2-Dichloropropane [78-87-5]^ 0.50 UD ug/L 5 0.50 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF 1,4-Dichlorobenzene [106-46-7]^ 0.95 UD ug/L 5 0.95 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF 2-Butanone [78-93-3]^ 6.5 UD ug/L 5 6.5 25 9I26038 EPA 8260D 09/27/19 06:51 REF 2-Hexanone [591-78-6]^ 4.4 UD ug/L 5 4.4 25 9I26038 EPA 8260D 09/27/19 06:51 REF 4-Methyl-2-pentanone [108-10-1]^ 5.5 UD ug/L 5 5.5 25 9I26038 EPA 8260D 09/27/19 06:51 REF Acetone [67-64-1]^ 50 UD ug/L 5 50 100 9I26038 EPA 8260D 09/27/19 06:51 REF Acrylonitrile [107-13-1]^ 18 UD ug/L 5 18 50 9I26038 EPA 8260D 09/27/19 06:51 REF Benzene [71-43-2]^ 0.75 UD ug/L 5 0.75 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF Bromochloromethane [74-97-5]^ 2.4 UD ug/L 5 2.4 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF Bromodichloromethane [75-27-4]^ 0.85 UD ug/L 5 0.85 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF Bromoform [75-25-2]^ 1.1 UD ug/L 5 1.1 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF Bromomethane [74-83-9]^ 0.70 UD ug/L 5 0.70 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF Carbon disulfide [75-15-0]^ 7.5 UD ug/L 5 7.5 25 9I26038 EPA 8260D 09/27/19 06:51 REF Carbon tetrachloride [56-23-5]^ 0.85 UD ug/L 5 0.85 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF Chlorobenzene [108-90-7]^ 7.4 D ug/L 5 0.85 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF Chloroethane [75-00-3]^ 1.2 UD ug/L 5 1.2 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF Chloroform [67-66-3]^ 0.90 UD ug/L 5 0.90 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF Chloromethane [74-87-3]^ 0.65 UD ug/L 5 0.65 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF cis- 1,2-Dichloroethene [156-59-2]^ 39 D ug/L 5 0.75 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF cis- 1,3-Dichloropropene [10061-01-5]^ 1.0 UD ug/L 5 1.0 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF Dibromochloromethane [124-48-1]^ 0.85 UD ug/L 5 0.85 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF Dibromomethane [74-95-3]^ 1.4 UD ug/L 5 1.4 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF Ethylbenzene [100-41-4]^ 0.65 UD ug/L 5 0.65 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF Iodomethane [74-88-4]^ 8.5 UD ug/L 5 8.5 25 9I26038 EPA 8260D 09/27/19 06:51 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.85 UD ug/L 5 0.85 10 9I26038 EPA 8260D 09/27/19 06:51 REF Methylene chloride [75-09-2]^ 1.2 UD ug/L 5 1.2 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF o-Xylene [95-47-6]^ 0.32 UD ug/L 5 0.32 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF Styrene [100-42-5]^ 0.55 UD ug/L 5 0.55 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF Tetrachloroethene [127-18-4]^ 0.85 UD ug/L 5 0.85 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF Toluene [108-88-3]^ 0.70 UD ug/L 5 0.70 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF trans-1,2-Dichloroethene [156-60-5]^ 1.0 UD ug/L 5 1.0 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.75 UD ug/L 5 0.75 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 3.5 UD ug/L 5 3.5 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF Trichloroethene [79-01-6]^ 0.75 UD ug/L 5 0.75 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF Trichlorofluoromethane [75-69-4]^ 1.2 UD ug/L 5 1.2 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF Vinyl acetate [108-05-4]^ 4.8 UD ug/L 5 4.8 25 9I26038 EPA 8260D 09/27/19 06:51 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 8 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW15D Lab Sample ID:CC16053-01 Received: 09/19/19 09:30 Matrix: Water Sampled:09/17/19 14:00 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 1.6 UD ug/L 5 1.6 5.0 9I26038 EPA 8260D 09/27/19 06:51 REF Xylenes (Total) [1330-20-7]1 2.2 UD ug/L 5 2.2 15 9I26038 EPA 8260D 09/27/19 06:51 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 44 1 50.0 88 % 53-136 9126036 EPA 8260D 09127119 06:51 REF Dlbromofluoromethane 46 1 50.0 91 % 67-129 9126036 EPA 6260D 09127119 06:51 REF Toluene-d8 38 1 50.0 75 % 59-134 9126036 EPA 6260D 09127119 06:51 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte ICAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 91 D ug/L 5 6.0 10 9I26041 EPA 8260D 09/26/19 14:50 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 5.0 1 5.00 100 % 75-125 9126041 EPA 8260D 09126119 14:50 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 9 Of 52 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW3 Lab Sample ID:CC16053-02 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 09:15 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I26008 EPA 8260D 09/26/19 19:56 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 9I26008 EPA 8260D 09/26/19 19:56 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I26008 EPA 8260D 09/26/19 19:56 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I26008 EPA 8260D 09/26/19 19:56 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I26008 EPA 8260D 09/26/19 19:56 REF Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I26008 EPA 8260D 09/26/19 19:56 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I26008 EPA 8260D 09/26/19 19:56 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I26008 EPA 8260D 09/26/19 19:56 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I26008 EPA 8260D 09/26/19 19:56 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 10 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW3 Lab Sample ID:CC16053-02 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 09:15 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9I26008 EPA 8260D 09/26/19 19:56 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I26008 EPA 8260D 09/26/19 19:56 REF Surrogates Results DF Snike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 44 1 50.0 88 % 53-136 9126006 EPA 8260D 09126119 19:56 REF Dlbromofluoromethane 45 1 50.0 90 % 67-129 9126006 EPA 6260D 09126119 19:56 REF Toluene-d8 37 1 50.0 74 % 59-134 9126008 EPA 6260D 09126119 19:56 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte ICAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes 1,4-Dioxane [123-91-1]^ 1.7 1 ug/L 1 1.2 2.0 9I27039 EPA 8260D 09/28/19 03:51 KKW QI-02 1,4-Dioxane [123-91-1]^ 1.6 1 ug/L 1 1.2 2.0 9102042 EPA 8260D 10/03/19 03:28 KKW Q-01 Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-& 5.6 1 5.00 111 % 75-125 9127039 EPA 8260D 09128119 03:51 KKW Qr-02 Toluene-& 5.0 1 5.00 100 % 75-125 9JO2042 EPA 8260D 10103119 03:28 KKW Q-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 11 of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW4 Lab Sample ID:CC16053-03 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 09:40 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 1.7 UD ug/L 10 1.7 10 9I27013 EPA 8260D 09/28/19 00:07 REF 1,1,1-Trichloroethane [71-55-6]^ 51 D ug/L 10 1.2 10 9I27013 EPA 8260D 09/28/19 00:07 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 2.8 UD ug/L 10 2.8 10 9I27013 EPA 8260D 09/28/19 00:07 REF 1,1,2-Trichloroethane [79-00-5]^ 1.4 UD ug/L 10 1.4 10 9I27013 EPA 8260D 09/28/19 00:07 REF 1,1-Dichloroethane [75-34-3]^ 400 D ug/L 10 1.3 10 9I27013 EPA 8260D 09/28/19 00:07 REF 1,1-Dichloroethene [75-35-4]^ 120 D ug/L 10 2.1 10 9I27013 EPA 8260D 09/28/19 00:07 REF 1,2,3-Trichloropropane [96-18-4]^ 2.3 UD ug/L 10 2.3 10 9I27013 EPA 8260D 09/28/19 00:07 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 4.8 UD ug/L 10 4.8 10 9I27013 EPA 8260D 09/28/19 00:07 REF 1,2-Dibromoethane [106-93-4]^ 6.6 UD ug/L 10 6.6 10 9I27013 EPA 8260D 09/28/19 00:07 REF 1,2-Dichlorobenzene [95-50-1]^ 4.7 ]D ug/L 10 1.9 10 9I27013 EPA 8260D 09/28/19 00:07 REF 1,2-Dichloroethane [107-06-2]^ 34 D ug/L 10 2.1 10 9I27013 EPA 8260D 09/28/19 00:07 REF 1,2-Dichloropropane [78-87-5]^ 1.0 UD ug/L 10 1.0 10 9I27013 EPA 8260D 09/28/19 00:07 REF 1,4-Dichlorobenzene [106-46-7]^ 1.9 UD ug/L 10 1.9 10 9I27013 EPA 8260D 09/28/19 00:07 REF 2-Butanone [78-93-3]^ 13 UD ug/L 10 13 50 9I27013 EPA 8260D 09/28/19 00:07 REF 2-Hexanone [591-78-6]^ 8.8 UD ug/L 10 8.8 50 9I27013 EPA 8260D 09/28/19 00:07 REF 4-Methyl-2-pentanone [108-10-1]^ 11 UD ug/L 10 11 50 9I27013 EPA 8260D 09/28/19 00:07 REF Acetone[67-64-1]^ 100 UD ug/L 10 100 200 9I27013 EPA 8260D 09/28/19 00:07 REF Acrylonitrile [107-13-1]^ 35 UD ug/L 10 35 100 9I27013 EPA 8260D 09/28/19 00:07 REF Benzene [71-43-2]^ 1.5 UD ug/L 10 1.5 10 9I27013 EPA 8260D 09/28/19 00:07 REF Bromochloromethane [74-97-5]^ 4.8 UD ug/L 10 4.8 10 9I27013 EPA 8260D 09/28/19 00:07 REF Bromodichloromethane [75-27-4]^ 1.7 UD ug/L 10 1.7 10 9I27013 EPA 8260D 09/28/19 00:07 REF Bromoform [75-25-2]^ 2.2 UD ug/L 10 2.2 10 9I27013 EPA 8260D 09/28/19 00:07 REF Bromomethane [74-83-9]^ 1.4 UD ug/L 10 1.4 10 9I27013 EPA 8260D 09/28/19 00:07 REF Carbon disulfide [75-15-0]^ 15 UD ug/L 10 15 50 9I27013 EPA 8260D 09/28/19 00:07 REF Carbon tetrachloride [56-23-5]^ 1.7 UD ug/L 10 1.7 10 9I27013 EPA 8260D 09/28/19 00:07 REF Chlorobenzene [108-90-7]^ 820 D ug/L 10 1.7 10 9I27013 EPA 8260D 09/28/19 00:07 REF Chloroethane [75-00-3]^ 250 D ug/L 10 2.3 10 9I27013 EPA 8260D 09/28/19 00:07 REF Chloroform [67-66-3]^ 1.8 UD ug/L 10 1.8 10 9I27013 EPA 8260D 09/28/19 00:07 REF Chloromethane [74-87-3]^ 1.3 UD ug/L 10 1.3 10 9I27013 EPA 8260D 09/28/19 00:07 REF cis- 1,2-Dichloroethene [156-59-2]^ 540 D ug/L 10 1.5 10 9I27013 EPA 8260D 09/28/19 00:07 REF cis- 1,3-Dichloropropene [10061-01-5]^ 2.0 UD ug/L 10 2.0 10 9I27013 EPA 8260D 09/28/19 00:07 REF Dibromochloromethane [124-48-1]^ 1.7 UD ug/L 10 1.7 10 9I27013 EPA 8260D 09/28/19 00:07 REF Dibromomethane [74-95-3]^ 2.7 UD ug/L 10 2.7 10 9I27013 EPA 8260D 09/28/19 00:07 REF Ethylbenzene [100-41-4]^ 1.3 UD ug/L 10 1.3 10 9I27013 EPA 8260D 09/28/19 00:07 REF Iodomethane [74-88-4]^ 17 UD ug/L 10 17 50 9I27013 EPA 8260D 09/28/19 00:07 REF m,p-Xylenes [108-38-3/106-42-3]^ 1.7 UD ug/L 10 1.7 20 9I27013 EPA 8260D 09/28/19 00:07 REF Methylene chloride [75-09-2]^ 2.3 UD ug/L 10 2.3 10 9I27013 EPA 8260D 09/28/19 00:07 REF o-Xylene [95-47-6]^ 7.7 ]D ug/L 10 0.65 10 9I27013 EPA 8260D 09/28/19 00:07 REF Styrene [100-42-5]^ 1.1 UD ug/L 10 1.1 10 9I27013 EPA 8260D 09/28/19 00:07 REF Tetrachloroethene [127-18-4]^ 4.4 ]D ug/L 10 1.7 10 9I27013 EPA 8260D 09/28/19 00:07 REF Toluene [108-88-3]^ 4.9 ]D ug/L 10 1.4 10 9I27013 EPA 8260D 09/28/19 00:07 REF trans- 1,2-Dichloroethene [156-60-5]^ 7.1 ]D ug/L 10 2.1 10 9I27013 EPA 8260D 09/28/19 00:07 REF trans-1,3-Dichloropropene [10061-02-6]^ 1.5 UD ug/L 10 1.5 10 9I27013 EPA 8260D 09/28/19 00:07 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 7.0 UD ug/L 10 7.0 10 9I27013 EPA 8260D 09/28/19 00:07 REF Trichloroethene [79-01-6]^ 1.5 UD ug/L 10 1.5 10 9I27013 EPA 8260D 09/28/19 00:07 REF Trichlorofluoromethane [75-69-4]^ 2.4 UD ug/L 10 2.4 10 9I27013 EPA 8260D 09/28/19 00:07 REF Vinyl acetate [108-05-4]^ 9.5 UD ug/L 10 9.5 50 9I27013 EPA 8260D 09/28/19 00:07 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 12 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW4 Lab Sample ID:CC16053-03 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 09:40 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]^ 420 D ug/L 10 3.2 10 9I27013 EPA 8260D 09/28/19 00:07 REF Xylenes(Total)[1330-20-7]^ 7.7 JD ug/L 10 4.5 30 9I27013 EPA 8260D 09/28/19 00:07 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 44 1 50.0 88 % 53-136 9127013 EPA 8260D 09128119 00:07 REF Dlbromofluoromethane 45 1 50.0 90 % 67-129 9127013 EPA 6260D 09128119 00:07 REF Toluene-d8 37 1 50.0 73 % 59-134 9127013 EPA 6260D 09128119 00:07 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1800 D ug/L 50 60 100 9I30043 EPA 8260D 10/01/19 04:24 KKW 1-05, J-06 1,4-Dioxane [123-91-1]^ 1500 D ug/L 50 60 100 9104030 EPA 8260D 10/04/19 12:47 KKW Q-01 Surrogates Results DF SSqike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 5.7 1 5.00 114 % 75-125 9130043 EPA 8260D 10101119 04:24 KKW Toluene-d8 5.2 1 5.00 104 % 75-125 9JO4030 EPA 8260D 10104119 12:47 KKW Q-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 13 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW5 Lab Sample ID:CC16053-04 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 08:40 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF 1,1-Dichloroethane [75-34-3]1 0.13 U ug/L 1 0.13 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF 1,1-Dichloroethene [75-35-4]1 0.21 U ug/L 1 0.21 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF 1,2,3-Trichloropropane [96-18-4]1 0.23 U ug/L 1 0.23 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF 1,2-Dibromoethane [106-93-4]1 0.66 U ug/L 1 0.66 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF 1,2-Dichloroethane [107-06-2]1 0.21 U ug/L 1 0.21 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF 1,2-Dichloropropane [78-87-5]1 0.10 U ug/L 1 0.10 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF 1,4-Dichlorobenzene [106-46-7]1 0.19 U ug/L 1 0.19 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I26008 EPA 8260D 09/26/19 20:59 REF 2-Hexanone [591-78-6]1 0.88 U ug/L 1 0.88 5.0 9I26008 EPA 8260D 09/26/19 20:59 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I26008 EPA 8260D 09/26/19 20:59 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I26008 EPA 8260D 09/26/19 20:59 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I26008 EPA 8260D 09/26/19 20:59 REF Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I26008 EPA 8260D 09/26/19 20:59 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF cis- 1,2-Dichloroethene [156-59-2]^ 0.63 J ug/L 1 0.15 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I26008 EPA 8260D 09/26/19 20:59 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I26008 EPA 8260D 09/26/19 20:59 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I26008 EPA 8260D 09/26/19 20:59 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 14 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW5 Lab Sample ID:CC16053-04 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 08:40 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]^ 0.46 J ug/L 1 0.32 1.0 9I26008 EPA 8260D 09/26/19 20:59 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I26008 EPA 8260D 09/26/19 20:59 REF Surrogates Results DF Snike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 43 1 50.0 86 % 53-136 9126006 EPA 8260D 09126119 20:59 REF Dlbromofluoromethane 45 1 50.0 90 % 67-129 9126006 EPA 6260D 09126119 20:59 REF Toluene-d8 37 1 50.0 74 % 59-134 9126008 EPA 6260D 09126119 20:59 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes 1,4-Dioxane [123-91-1]^ 5.8 ug/L 1 1.2 2.0 9I27039 EPA 8260D 09/28/19 05:03 KKW QI-02 1,4-Dioxane [123-91-1]^ 2.4 ug/L 1 1.2 2.0 9102042 EPA 8260D 10/03/19 04:06 KKW Q-01 Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-& 5.2 1 5.00 104 % 75-125 9127039 EPA 8260D 09128119 05:03 KKW Qr-02 Toluene-& 5.0 1 5.00 100 % 75-125 9JO2042 EPA 8260D 10103119 04:06 KKW Q-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 15 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW6Surface Lab Sample ID:CC16053-05 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 10: 10 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF 1,1-Dichloroethane [75-34-3]1 0.13 U ug/L 1 0.13 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF 1,1-Dichloroethene [75-35-4]1 0.21 U ug/L 1 0.21 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF 1,2,3-Trichloropropane [96-18-4]1 0.23 U ug/L 1 0.23 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF 1,2-Dibromoethane [106-93-4]1 0.66 U ug/L 1 0.66 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF 1,2-Dichloroethane [107-06-2]1 0.21 U ug/L 1 0.21 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF 1,2-Dichloropropane [78-87-5]1 0.10 U ug/L 1 0.10 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF 1,4-Dichlorobenzene [106-46-7]1 0.19 U ug/L 1 0.19 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I26008 EPA 8260D 09/26/19 21:30 REF 2-Hexanone [591-78-6]1 0.88 U ug/L 1 0.88 5.0 9I26008 EPA 8260D 09/26/19 21:30 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I26008 EPA 8260D 09/26/19 21:30 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I26008 EPA 8260D 09/26/19 21:30 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I26008 EPA 8260D 09/26/19 21:30 REF Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I26008 EPA 8260D 09/26/19 21:30 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF cis- 1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I26008 EPA 8260D 09/26/19 21:30 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I26008 EPA 8260D 09/26/19 21:30 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I26008 EPA 8260D 09/26/19 21:30 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 16 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW6Surface Lab Sample ID:CC16053-05 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 10:10 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9I26008 EPA 8260D 09/26/19 21:30 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I26008 EPA 8260D 09/26/19 21:30 REF Surrogates Results DF Snike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 43 1 50.0 87 % 53-136 9126006 EPA 8260D 09126119 21:30 REF Dlbromofluoromethane 45 1 50.0 91 % 67-129 9126006 EPA 6260D 09126119 21:30 REF Toluene-d8 37 1 50.0 74 % 59-134 9126008 EPA 6260D 09126119 2130 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes 1,4-Dioxane [123-91-1]^ 1.6 J ug/L 1 1.2 2.0 9I27039 EPA 8260D 09/28/19 05:38 KKW QI-02 1,4-Dioxane [123-91-1]^ 1.2 U ug/L 1 1.2 2.0 9JO2042 EPA 8260D 10/03/19 04:45 KKW Q-01 Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-& 5.4 1 5.00 109 % 75-125 9127039 EPA 8260D 09128119 0538 KKW Qr-02 Toluene-& 5.5 1 5.00 110 % 75-125 9JO2042 EPA 8260D 10103119 04:45 KKW Q-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 17 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW6Bottom Lab Sample ID:CC16053-06 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 10:15 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF 1,1-Dichloroethane [75-34-3]1 0.13 U ug/L 1 0.13 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF 1,1-Dichloroethene [75-35-4]1 0.21 U ug/L 1 0.21 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF 1,2,3-Trichloropropane [96-18-4]1 0.23 U ug/L 1 0.23 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF 1,2-Dibromoethane [106-93-4]1 0.66 U ug/L 1 0.66 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF 1,2-Dichloroethane [107-06-2]1 0.21 U ug/L 1 0.21 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF 1,2-Dichloropropane [78-87-5]1 0.10 U ug/L 1 0.10 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF 1,4-Dichlorobenzene [106-46-7]1 0.19 U ug/L 1 0.19 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I26008 EPA 8260D 09/26/19 22:01 REF 2-Hexanone [591-78-6]1 0.88 U ug/L 1 0.88 5.0 9I26008 EPA 8260D 09/26/19 22:01 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I26008 EPA 8260D 09/26/19 22:01 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I26008 EPA 8260D 09/26/19 22:01 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I26008 EPA 8260D 09/26/19 22:01 REF Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I26008 EPA 8260D 09/26/19 22:01 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF cis- 1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I26008 EPA 8260D 09/26/19 22:01 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I26008 EPA 8260D 09/26/19 22:01 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I26008 EPA 8260D 09/26/19 22:01 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 18 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW6Bottom Lab Sample ID:CC16053-06 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 10:15 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9I26008 EPA 8260D 09/26/19 22:01 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I26008 EPA 8260D 09/26/19 22:01 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 44 1 50.0 88 % 53-136 9126006 EPA 8260D 09126119 22:01 REF Dlbromofluoromethane 45 1 50.0 91 % 67-129 9126006 EPA 6260D 09126119 22:01 REF Toluene-d8 37 1 50.0 74 % 59-134 9126008 EPA 6260D 09126119 22:01 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.2 U ug/L 1 1.2 2.0 9I30043 EPA 8260D 09/30/19 19:11 KKW 1-05, J-06 1,4-Dioxane [123-91-1]^ 1.2 U ug/L 1 1.2 2.0 9302042 EPA 8260D 10/03/19 05:23 KKW Q-01 Surrogates Results DF SSqike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 4.5 1 5.00 90 % 75-125 9130043 EPA 8260D 09130119 19:11 KKW Toluene-d8 5.4 1 5.00 108 % 75-125 9JO2042 EPA 8260D 10103119 05:23 KKW Q-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 19 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW7Surface Lab Sample ID:CC16053-07 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 11:50 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF 1,1-Dichloroethane [75-34-3]1 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF 1,1-Dichloroethene [75-35-4]1 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF 1,2,3-Trichloropropane [96-18-4]1 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF 1,2-Dibromoethane [106-93-4]1 0.66 U ug/L 1 0.66 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF 1,2-Dichloroethane [107-06-2]1 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF 1,2-Dichloropropane [78-87-5]1 0.10 U ug/L 1 0.10 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF 1,4-Dichlorobenzene [106-46-7]1 0.19 U ug/L 1 0.19 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I25045 EPA 8260D 09/26/19 00:18 REF 2-Hexanone [591-78-6]1 0.88 U ug/L 1 0.88 5.0 9I25045 EPA 8260D 09/26/19 00:18 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I25045 EPA 8260D 09/26/19 00:18 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I25045 EPA 8260D 09/26/19 00:18 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I25045 EPA 8260D 09/26/19 00:18 REF Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I25045 EPA 8260D 09/26/19 00:18 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF cis- 1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I25045 EPA 8260D 09/26/19 00:18 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I25045 EPA 8260D 09/26/19 00:18 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I25045 EPA 8260D 09/26/19 00:18 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 20 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW7Surface Lab Sample ID:CC16053-07 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 11:50 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9I25045 EPA 8260D 09/26/19 00:18 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I25045 EPA 8260D 09/26/19 00:18 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 44 1 50.0 89 % 53-136 9125045 EPA 8260D 09126119 00:18 REF Dlbromofluoromethane 45 1 50.0 89 % 67-129 9125045 EPA 6260D 09126119 00:18 REF Toluene-d8 37 1 50.0 74 % 59-134 9125045 EPA 6260D 09126119 00:16 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.2 U ug/L 1 1.2 2.0 9I30043 EPA 8260D 09/30/19 19:48 KKW 1-05, J-06 1,4-Dioxane [123-91-1]^ 1.2 U ug/L 1 1.2 2.0 9302042 EPA 8260D 10/03/19 06:01 KKW Q-01 Surrogates Results DF SSqike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 4.4 1 5.00 87 % 75-125 9130043 EPA 8260D 09130119 19:48 KKW Toluene-d8 5.3 1 5.00 106 % 75-125 9JO2042 EPA 8260D 10103119 06:01 KKW Q-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 21 of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW7Bottom Lab Sample ID:CC16053-08 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 11:55 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF 1,1-Dichloroethane [75-34-3]1 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF 1,1-Dichloroethene [75-35-4]1 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF 1,2,3-Trichloropropane [96-18-4]1 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF 1,2-Dibromoethane [106-93-4]1 0.66 U ug/L 1 0.66 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF 1,2-Dichloroethane [107-06-2]1 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF 1,2-Dichloropropane [78-87-5]1 0.10 U ug/L 1 0.10 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF 1,4-Dichlorobenzene [106-46-7]1 0.19 U ug/L 1 0.19 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I25045 EPA 8260D 09/26/19 00:49 REF 2-Hexanone [591-78-6]1 0.88 U ug/L 1 0.88 5.0 9I25045 EPA 8260D 09/26/19 00:49 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I25045 EPA 8260D 09/26/19 00:49 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I25045 EPA 8260D 09/26/19 00:49 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I25045 EPA 8260D 09/26/19 00:49 REF Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I25045 EPA 8260D 09/26/19 00:49 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF cis- 1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I25045 EPA 8260D 09/26/19 00:49 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I25045 EPA 8260D 09/26/19 00:49 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I25045 EPA 8260D 09/26/19 00:49 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 22 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SW7Bottom Lab Sample ID:CC16053-08 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 11:55 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9I25045 EPA 8260D 09/26/19 00:49 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I25045 EPA 8260D 09/26/19 00:49 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 44 1 50.0 88 % 53-136 9125045 EPA 8260D 09126119 00:49 REF Dlbromofluoromethane 44 1 50.0 89 % 67-129 9125045 EPA 6260D 09126119 00:49 REF Toluene-d8 37 1 50.0 75 % 59-134 9125045 EPA 6260D 09126119 00:49 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.2 U ug/L 1 1.2 2.0 9I30043 EPA 8260D 09/30/19 20:25 KKW 1-05, J-06 1,4-Dioxane [123-91-1]^ 1.2 U ug/L 1 1.2 2.0 9303063 EPA 8260D 10/04/19 03:03 KKW Q-01 Surrogates Results DF SSqike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 4.4 1 5.00 89 % 75-125 9130043 EPA 8260D 09130119 20:25 KKW Toluene-d8 5.0 1 5.00 101 % 75-125 9JO3063 EPA 8260D 10104119 03:03 KKW Q-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 23 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SWDRP2Surface Lab Sample ID:CC16053-09 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 11:15 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF 1,1-Dichloroethane [75-34-3]1 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF 1,1-Dichloroethene [75-35-4]1 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF 1,2,3-Trichloropropane [96-18-4]1 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF 1,2-Dibromoethane [106-93-4]1 0.66 U ug/L 1 0.66 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF 1,2-Dichloroethane [107-06-2]1 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF 1,2-Dichloropropane [78-87-5]1 0.10 U ug/L 1 0.10 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF 1,4-Dichlorobenzene [106-46-7]1 0.19 U ug/L 1 0.19 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I25045 EPA 8260D 09/26/19 01:20 REF 2-Hexanone [591-78-6]1 0.88 U ug/L 1 0.88 5.0 9I25045 EPA 8260D 09/26/19 01:20 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I25045 EPA 8260D 09/26/19 01:20 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I25045 EPA 8260D 09/26/19 01:20 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I25045 EPA 8260D 09/26/19 01:20 REF Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I25045 EPA 8260D 09/26/19 01:20 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF cis- 1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I25045 EPA 8260D 09/26/19 01:20 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I25045 EPA 8260D 09/26/19 01:20 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I25045 EPA 8260D 09/26/19 01:20 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 24 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SWDRP2Surface Lab Sample ID:CC16053-09 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 11:15 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9I25045 EPA 8260D 09/26/19 01:20 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I25045 EPA 8260D 09/26/19 01:20 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 46 1 50.0 92 % 53-136 9125045 EPA 8260D 09126119 01:20 REF Dlbromofluoromethane 44 1 50.0 89 % 67-129 9125045 EPA 6260D 09126119 01:20 REF Toluene-d8 36 1 50.0 73 % 59-134 9125045 EPA 6260D 09126119 01:20 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte ICAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.4 J ug/L 1 1.2 2.0 9I30043 EPA 8260D 09/30/19 21:01 KKW 1-05, J-06 1,4-Dioxane [123-91-1]^ 1.2 U ug/L 1 1.2 2.0 9303063 EPA 8260D 10/04/19 03:39 KKW Q-01 Surrogates Results DF SSqike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 4.7 1 5.00 95 % 75-125 9130043 EPA 8260D 09130119 21:01 KKW Toluene-d8 5.6 1 5.00 113 % 75-125 9JO3063 EPA 8260D 10104119 03:39 KKW Q-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 25 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 440 1 -SWDRP2 Bottom Lab Sample ID:CC16053-10 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 11:20 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF 1,1-Dichloroethane [75-34-3]1 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF 1,1-Dichloroethene [75-35-4]1 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF 1,2,3-Trichloropropane [96-18-4]1 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF 1,2-Dibromoethane [106-93-4]1 0.66 U ug/L 1 0.66 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF 1,2-Dichloroethane [107-06-2]1 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF 1,2-Dichloropropane [78-87-5]1 0.10 U ug/L 1 0.10 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF 1,4-Dichlorobenzene [106-46-7]1 0.19 U ug/L 1 0.19 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I25045 EPA 8260D 09/26/19 01:52 REF 2-Hexanone [591-78-6]1 0.88 U ug/L 1 0.88 5.0 9I25045 EPA 8260D 09/26/19 01:52 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I25045 EPA 8260D 09/26/19 01:52 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I25045 EPA 8260D 09/26/19 01:52 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I25045 EPA 8260D 09/26/19 01:52 REF Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I25045 EPA 8260D 09/26/19 01:52 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF cis- 1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I25045 EPA 8260D 09/26/19 01:52 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I25045 EPA 8260D 09/26/19 01:52 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I25045 EPA 8260D 09/26/19 01:52 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 26 of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 440 1 -SWDRP2 Bottom Lab Sample ID:CC16053-10 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 11:20 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9I25045 EPA 8260D 09/26/19 01:52 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I25045 EPA 8260D 09/26/19 01:52 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 46 1 50.0 91 % 53-136 9125045 EPA 8260D 09126119 01:52 REF Dlbromofluoromethane 44 1 50.0 88 % 67-129 9125045 EPA 6260D 09126119 01:52 REF Toluene-d8 36 1 50.0 73 % 59-134 9125045 EPA 6260D 09126119 01:52 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.2 U ug/L 1 1.2 2.0 9I30043 EPA 8260D 09/30/19 21:37 KKW 1-05, J-06 1,4-Dioxane [123-91-1]^ 1.2 U ug/L 1 1.2 2.0 9303063 EPA 8260D 10/04/19 04:15 KKW Q-01 Surrogates Results DF SSqike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 4.7 1 5.00 95 % 75-125 9130043 EPA 8260D 09130119 21:37 KKW Toluene-d8 5.1 1 5.00 103 % 75-125 9JO3063 EPA 8260D 10104119 04:15 KKW Q-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 27 of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SWDRP11Surface Lab Sample ID:CC16053-11 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 12:30 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF 1,1-Dichloroethane [75-34-3]1 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF 1,1-Dichloroethene [75-35-4]1 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF 1,2,3-Trichloropropane [96-18-4]1 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF 1,2-Dibromoethane [106-93-4]1 0.66 U ug/L 1 0.66 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF 1,2-Dichloroethane [107-06-2]1 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF 1,2-Dichloropropane [78-87-5]1 0.10 U ug/L 1 0.10 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF 1,4-Dichlorobenzene [106-46-7]1 0.19 U ug/L 1 0.19 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I25045 EPA 8260D 09/26/19 02:23 REF 2-Hexanone [591-78-6]1 0.88 U ug/L 1 0.88 5.0 9I25045 EPA 8260D 09/26/19 02:23 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I25045 EPA 8260D 09/26/19 02:23 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I25045 EPA 8260D 09/26/19 02:23 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I25045 EPA 8260D 09/26/19 02:23 REF Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I25045 EPA 8260D 09/26/19 02:23 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF cis- 1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I25045 EPA 8260D 09/26/19 02:23 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I25045 EPA 8260D 09/26/19 02:23 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I25045 EPA 8260D 09/26/19 02:23 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 28 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SWDRPllSurface Lab Sample ID:CC16053-11 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 12:30 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9I25045 EPA 8260D 09/26/19 02:23 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I25045 EPA 8260D 09/26/19 02:23 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 45 1 50.0 89 % 53-136 9125045 EPA 8260D 09126119 02:23 REF Dlbromofluoromethane 45 1 50.0 90 % 67-129 9125045 EPA 6260D 09126119 02:23 REF Toluene-d8 37 1 50.0 73 % 59-134 9125045 EPA 6260D 09126119 02:23 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte ICAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.3 J ug/L 1 1.2 2.0 9I30043 EPA 8260D 09/30/19 22:15 KKW 1-05, J-06 1,4-Dioxane [123-91-1]^ 1.2 U ug/L 1 1.2 2.0 9303063 EPA 8260D 10/04/19 04:51 KKW Q-01 Surrogates Results DF SSqike Lv/ % Rec % Rec Limits Batch Method Analyzed ffy Notes Toluene-d8 5.1 1 5.00 103 % 75-125 9130043 EPA 8260D 09130119 22:15 KKW Toluene-d8 5.2 1 5.00 104 % 75-125 9JO3063 EPA 8260D 10104119 04:51 KKW Q-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 29 of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SWDRP11Bottom Lab Sample ID:CC16053-12 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 12:35 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF 1,1-Dichloroethane [75-34-3]1 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF 1,1-Dichloroethene [75-35-4]1 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF 1,2,3-Trichloropropane [96-18-4]1 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF 1,2-Dibromoethane [106-93-4]1 0.66 U ug/L 1 0.66 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF 1,2-Dichloroethane [107-06-2]1 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF 1,2-Dichloropropane [78-87-5]1 0.10 U ug/L 1 0.10 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF 1,4-Dichlorobenzene [106-46-7]1 0.19 U ug/L 1 0.19 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I25045 EPA 8260D 09/26/19 02:54 REF 2-Hexanone [591-78-6]1 0.88 U ug/L 1 0.88 5.0 9I25045 EPA 8260D 09/26/19 02:54 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I25045 EPA 8260D 09/26/19 02:54 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I25045 EPA 8260D 09/26/19 02:54 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I25045 EPA 8260D 09/26/19 02:54 REF Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I25045 EPA 8260D 09/26/19 02:54 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF cis- 1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I25045 EPA 8260D 09/26/19 02:54 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I25045 EPA 8260D 09/26/19 02:54 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I25045 EPA 8260D 09/26/19 02:54 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 30 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-SWDRPllBottom Lab Sample ID:CC16053-12 Received: 09/19/19 09:30 Matrix: Water Sampled:09/18/19 12:35 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9I25045 EPA 8260D 09/26/19 02:54 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I25045 EPA 8260D 09/26/19 02:54 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 44 1 50.0 89 % 53-136 9125045 EPA 8260D 09126119 02:54 REF Dlbromofluoromethane 44 1 50.0 89 % 67-129 9125045 EPA 6260D 09126119 02:54 REF Toluene-d8 37 1 50.0 74 % 59-134 9125045 EPA 6260D 09126119 02:54 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.2 U ug/L 1 1.2 2.0 9I27029 EPA 8260D 09/27/19 14:36 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-& 5.5 1 5.00 110 % 75-125 9127029 EPA 8260D 0912711914:36 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 31 of 52 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW16D Lab Sample ID:CC16053-13 Received: 09/19/19 09:30 Matrix: Water Sampled:09/17/19 11:15 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF 1,1,1-Trichloroethane [71-55-6]A 0.51 1 ug/L 1 0.12 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF 1,1-Dichloroethane [75-34-3]A 20 ug/L 1 0.13 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF 1,1-Dichloroethene [75-35-4]A 4.5 ug/L 1 0.21 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I26038 EPA 8260D 09/27/19 07:22 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 9I26038 EPA 8260D 09/27/19 07:22 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I26038 EPA 8260D 09/27/19 07:22 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I26038 EPA 8260D 09/27/19 07:22 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I26038 EPA 8260D 09/27/19 07:22 REF Benzene [71-43-2]A 0.45 J ug/L 1 0.15 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I26038 EPA 8260D 09/27/19 07:22 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF Chlorobenzene [108-90-7]^ 22 ug/L 1 0.17 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF Chloroethane [75-00-3]^ 3.3 ug/L 1 0.23 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF cis-1,2-Dichloroethene [156-59-2]^ 20 ug/L 1 0.15 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I26038 EPA 8260D 09/27/19 07:22 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I26038 EPA 8260D 09/27/19 07:22 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I26038 EPA 8260D 09/27/19 07:22 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 32 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW16D Lab Sample ID:CC16053-13 Received: 09/19/19 09:30 Matrix: Water Sampled:09/17/19 11:15 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]^ 1.3 ug/L 1 0.32 1.0 9I26038 EPA 8260D 09/27/19 07:22 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I26038 EPA 8260D 09/27/19 07:22 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 43 1 50.0 86 % 53-136 9126036 EPA 8260D 09127119 07:22 REF Dlbromofluoromethane 45 1 50.0 91 % 67-129 9126036 EPA 6260D 09127119 07:22 REF Toluene-d8 38 1 50.0 75 % 59-134 9126036 EPA 6260D 09127119 07:22 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 28 ug/L 1 1.2 2.0 9I27029 EPA 8260D 09/27/19 15:10 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 4.9 1 5.00 98 % 75-125 9127029 EPA 8260D 0912711915:10 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 33 of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW14D Lab Sample ID:CC16053-14 Received: 09/19/19 09:30 Matrix: Water Sampled:09/17/19 15:30 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF 1,1-Dichloroethane [75-34-3]A 0.55 1 ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I25045 EPA 8260D 09/26/19 03:56 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 9I25045 EPA 8260D 09/26/19 03:56 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I25045 EPA 8260D 09/26/19 03:56 REF Acetone [67-64-1]A 10 1 ug/L 1 10 20 9I25045 EPA 8260D 09/26/19 03:56 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I25045 EPA 8260D 09/26/19 03:56 REF Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I25045 EPA 8260D 09/26/19 03:56 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF Chlorobenzene [108-90-7]A 1.4 ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF cis- 1,2-Dichloroethene [156-59-2]A 0.89 J ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF Ethylbenzene [100-41-4]A 1.6 ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I25045 EPA 8260D 09/26/19 03:56 REF m,p-Xylenes [108-38-3/106-42-3] A 7.4 ug/L 1 0.17 2.0 9I25045 EPA 8260D 09/26/19 03:56 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF o-Xylene [95-47-6]A 3.7 ug/L 1 0.065 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF Toluene [108-88-3]A 5.2 ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I25045 EPA 8260D 09/26/19 03:56 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 34 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW14D Lab Sample ID:CC16053-14 Received: 09/19/19 09:30 Matrix: Water Sampled:09/17/19 15:30 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9I25045 EPA 8260D 09/26/19 03:56 REF Xylenes(Total)[1330-20-7]^ 11 ug/L 1 0.45 3.0 9I25045 EPA 8260D 09/26/19 03:56 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 44 1 50.0 88 % 53-136 9125045 EPA 8260D 09126119 03:56 REF Dlbromofluoromethane 45 1 50.0 91 % 67-129 9125045 EPA 6260D 09126119 03:56 REF Toluene-d8 37 1 50.0 74 % 59-134 9125045 EPA 6260D 09126119 03:56 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte ICAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.3 1 ug/L 1 1.2 2.0 9I27029 EPA 8260D 09/27/19 15:45 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 5.1 1 5.00 103 % 75-125 9127029 EPA 8260D 0912711915:45 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 35 of 52 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-Trip Blank Lab Sample ID:CC16053-15 Received: 09/19/19 09:30 Matrix: Water Sampled:09/17/19 11:15 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By:ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I25045 EPA 8260D 09/25/19 21:11 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 9I25045 EPA 8260D 09/25/19 21:11 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I25045 EPA 8260D 09/25/19 21:11 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I25045 EPA 8260D 09/25/19 21:11 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I25045 EPA 8260D 09/25/19 21:11 REF Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I25045 EPA 8260D 09/25/19 21:11 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF Chlorobenzene[108-90-7]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I25045 EPA 8260D 09/25/19 21:11 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I25045 EPA 8260D 09/25/19 21:11 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I25045 EPA 8260D 09/25/19 21:11 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 36 Of 52 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-TripBlank Lab Sample ID:CC16053-15 Received: 09/19/19 09:30 Matrix: Water Sampled:09/17/19 11:15 Work Order: CC16053 Project: Seaboard/Riverdale Landfill Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9I25045 EPA 8260D 09/25/19 21:11 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I25045 EPA 8260D 09/25/19 21:11 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 44 1 50.0 89 % 53-136 9125045 EPA 8260D 09125119 21:11 REF Dlbromofluoromethane 44 1 50.0 87 % 67-129 9125045 EPA 6260D 09125119 21:11 REF Toluene-d8 37 1 50.0 74 % 59-134 9125045 EPA 6260D 09125119 21:11 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.2 U ug/L 1 1.2 2.0 9I25047 EPA 8260D 09/26/19 00:46 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-& 4.9 1 5.00 98 % 75-125 9125047 EPA 8260D 09126119 00:46 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 37 Of 52 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9125045 - EPA 5030E MS Blank (9I25045-BLK1) Prepared: 09/25/2019 14:04 Analyzed: 09/25/2019 19:38 Analvte Result Flaa POL Units 1, 1, 1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC Level Result %REC Limits RPD RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 38 Of 52 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9125045 - EPA 50308 MS - Continued Blank (9I25045-BLKI) Continued Prepared: 09/25/2019 14:04 Analyzed: 09/25/2019 19:38 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 43 ug/L 50.0 87 53-136 Dibromofluoromethane 44 ug/L 50.0 88 67-129 Toluene-d8 37 ug/L 50.0 74 59-134 LCS (9I25045-BS1) Prepared: 09/25/2019 14:04 Analyzed: 09/25/2019 17:33 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 17 1.0 ug/L 20.0 85 75-133 Benzene 18 1.0 ug/L 20.0 91 80-134 Chlorobenzene 18 1.0 ug/L 20.0 89 80-120 Toluene 18 1.0 ug/L 20.0 88 71-120 Trichloroethene 16 1.0 ug/L 20.0 82 74-120 4-Bromofluorobenzene 45 ug/L 50.0 89 53-136 Dibromofluoromethane 43 ug/L 50.0 86 67-129 Toluene-d8 37 ug/L 50.0 74 59-134 Matrix Spike (9I25045-MS1) Prepared: 09/25/2019 14:04 Analyzed: 09/25/2019 18:04 Source: CC16075-10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 16 1.0 ug/L 20.0 0.21 U 82 75-133 Benzene 18 1.0 ug/L 20.0 0.15 U 90 80-134 Chlorobenzene 17 1.0 ug/L 20.0 0.17 U 84 80-120 Toluene 18 1.0 ug/L 20.0 0.14 U 89 71-120 Trichloroethene 16 1.0 ug/L 20.0 0.15 U 78 74-120 4-Bromofluorobenzene 45 ug/L 50.0 90 53-136 Dibromofluoromethane 43 ug/L 50.0 86 67-129 Toluene-d8 37 ug/L 50.0 74 59-134 Matrix Spike Dup (9I25045-MSD1) Prepared: 09/25/2019 14:04 Analyzed: 09/25/2019 18:35 Source: CC16075-10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 15 1.0 ug/L 20.0 0.21 U 77 75-133 6 20 Benzene 18 1.0 ug/L 20.0 0.15 U 89 80-134 2 17 Chlorobenzene 17 1.0 ug/L 20.0 0.17 U 84 80-120 0.4 16 Toluene 17 1.0 ug/L 20.0 0.14 U 83 71-120 6 17 Trichloroethene 16 1.0 ug/L 20.0 0.15 U 78 74-120 0.3 22 4-Bromofluorobenzene 44 ug/L 50.0 88 53-136 Dibromofluoromethane 43 ug/L 50.0 66 67-129 Toluene-d8 37 ug/L 50.0 75 59-134 Batch 9I26008 - EPA 5030E MS Blank (9I26008-BLK3) Prepared: 09/26/2019 08:42 Analyzed: 09/26/2019 14:12 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 39 Of 52 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9126008 - EPA 50308 MS - Continued Blank (9I26008-BLKI) Continued Prepared: 09/26/2019 08:42 Analyzed: 09/26/2019 14:12 Analvte Result Flaa POL Units 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene Dibromofluoromethane FINAL 42 u9/L 50.0 65 53-136 44 u9/L 50.0 67 67-129 This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 40 Of 52 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9I26008 - EPA 50308 MS - Continued Blank (9I26008-BLKI) Continued Prepared: 09/26/2019 08:42 Analyzed: 09/26/2019 14:12 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Toluene-d8 37 u9/L 50.0 74 59-134 LCS (9I26008-BSI) Prepared: 09/26/2019 08:42 Analyzed: 09/26/2019 11:05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 16 1.0 ug/L 20.0 79 75-133 Benzene 18 1.0 ug/L 20.0 90 80-134 Chlorobenzene 17 1.0 ug/L 20.0 85 80-120 Toluene 18 1.0 ug/L 20.0 89 71-120 Trichloroethene 16 1.0 ug/L 20.0 80 74-120 4-Bromofluorobenzene 45 u9/L 50.0 89 53-136 Dibromofluoromethane 43 u9/L 50.0 85 67-129 Toluene-d8 37 u9/L 50.0 74 59-134 Matrix Spike (9I26008-MS1) Prepared: 09/26/2019 08:42 Analyzed: 09/26/2019 11:36 Source: CC15257-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 9.0 1.0 ug/L 20.0 0.21 U 45 75-133 QM-07 Benzene 13 1.0 ug/L 20.0 3.3 46 80-134 QM-07 Chlorobenzene 9.2 1.0 ug/L 20.0 0.17 U 46 80-120 QM-07 Toluene 9.2 1.0 ug/L 20.0 0.14 U 46 71-120 QM-07 Trichloroethene 8.5 1.0 ug/L 20.0 0.15 U 42 74-120 QM-07 4-Bromofluorobenzene 45 u9/L 50.0 91 53-136 Dibromofluoromethane 43 u9/L 50.0 66 67-129 Toluene-d8 37 u9/L 50.0 73 59-134 Matrix Spike Dup (9I26008-MSD1) Prepared: 09/26/2019 08:42 Analyzed: 09/26/2019 12:07 Source: CCI5257-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 6.7 1.0 ug/L 20.0 0.21 U 34 75-133 28 20 QM-11, QM-07 Benzene 9.9 1.0 ug/L 20.0 3.3 33 80-134 23 17 QM-11, QM-07 Chlorobenzene 6.6 1.0 ug/L 20.0 0.17 U 33 80-120 33 16 QM-07, QM-11 Toluene 6.5 1.0 ug/L 20.0 0.14 U 33 71-120 34 17 QM-07, QM-11 Trichloroethene 6.1 1.0 ug/L 20.0 0.15 U 30 74-120 33 22 QM-11, QM-07 4-Bromofluorobenzene 44 u9/L 50.0 89 53-136 Dibromofluoromethane 43 u9/L 50.0 86 67-129 Toluene-d8 37 u9/L 50.0 74 59-134 Batch 9I26038 - EPA 5030E MS Blank (9I26038-BLK3) Prepared: 09/26/2019 13:30 Analyzed: 09/27/2019 02:11 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 41 of 52 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9126038 - EPA 50308 MS - Continued Blank (9I26038-BLKI) Continued Prepared: 09/26/2019 13:30 Analyzed: 09/27/2019 02:11 Analvte Result Flaa POL Units 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene FINAL 43 ug/L 50.0 66 53-136 This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 42 Of 52 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9126038 - EPA 50308 MS - Continued Blank (9I26038-BLKI) Continued Prepared: 09/26/2019 13:30 Analyzed: 09/27/2019 02:11 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Dibromofluoromethane 44 U91L 50.0 88 67-129 Toluene-& 37 U91L 50.0 74 59-134 LCS (9I26038-BS1) Prepared: 09/26/2019 13:30 Analyzed: 09/27/2019 00:06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 17 1.0 ug/L 20.0 86 75-133 Benzene 19 1.0 ug/L 20.0 96 80-134 Chlorobenzene 19 1.0 ug/L 20.0 93 80-120 Toluene 19 1.0 ug/L 20.0 96 71-120 Trichloroethene 18 1.0 ug/L 20.0 91 74-120 4-Bromofluorobenzene 45 U91L 50.0 89 53-136 Dibromofluoromethane 43 U91L 50.0 86 67-129 Toluene-d8 36 U91L 50.0 72 59-134 Matrix Spike (9I26038-MS1) Prepared: 09/26/2019 13:30 Analyzed: 09/27/2019 00:37 Source: CC16420-05 Spike Source %REC RPD Analvte Result Flao POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 18 1.0 ug/L 20.0 0.21 U 91 75-133 Benzene 20 1.0 ug/L 20.0 0.15 U 98 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 93 80-120 Toluene 18 1.0 ug/L 20.0 0.14 U 92 71-120 Trichloroethene 19 1.0 ug/L 20.0 0.15 U 93 74-120 4-Bromofluorobenzene 45 U91L 50.0 91 53-136 Dibromofluoromethane 43 U91L 50.0 86 67-129 Toluene-d8 38 U91L 50.0 75 59-134 Matrix Spike Dup (9I26038-MSD1) Prepared: 09/26/2019 13:30 Analyzed: 09/27/2019 01:08 Source: CC16420-05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 17 1.0 ug/L 20.0 0.21 U 84 75-133 8 20 Benzene 19 1.0 ug/L 20.0 0.15 U 94 80-134 5 17 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 88 80-120 6 16 Toluene 18 1.0 ug/L 20.0 0.14 U 88 71-120 4 17 Trichloroethene 17 1.0 ug/L 20.0 0.15 U 87 74-120 6 22 4-Bromofluorobenzene 44 U91L 50.0 88 53-136 Dibromofluoromethane 43 U91L 50.0 86 67-129 Toluene-d8 37 u9/L 50.0 75 59-134 Batch 9I27013 - EPA 50305 MS Blank (9I27013-BLK3) Prepared: 09/27/2019 09:49 Analyzed: 09/27/2019 15:47 Spike Source %REC Analvte Result Flaa Q Units Level Result %REC Limits 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L RPD RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full Page 43 of 52 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9127013 - EPA 50308 MS - Continued Blank (9I27013-BLKi) Continued Prepared: 09/27/2019 09:49 Analyzed: 09/27/2019 15:47 Analvte Result Flaa POL Units 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 43 u91L 50.0 87 53-136 Dibromofluoromethane 45 u9/L 50.0 69 67-129 Toluene-d8 36 u9/L 50.0 75 59-134 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 44 of 52 0Nk"q09 www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9127013 - EPA 5030E MS - Continued LCS (9I27013-BSI) Prepared: 09/27/2019 09:49 Analyzed: 09/27/2019 13:42 Spike Source %REC RPD Analvte Result Flau POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 17 1.0 ug/L 20.0 86 75-133 Benzene 19 1.0 ug/L 20.0 96 80-134 Chlorobenzene 18 1.0 ug/L 20.0 90 80-120 Toluene 18 1.0 ug/L 20.0 92 71-120 Trichloroethene 17 1.0 ug/L 20.0 86 74-120 4-8romofluorobenzene 43 u9/L 50.0 87 53-136 Dibromofluoromethane 43 u9/L 50.0 86 67-129 Toluene-& 37 u91L 50.0 75 59-134 Matrix Spike (9I27013-MS1) Prepared: 09/27/2019 09:49 Analyzed: 09/27/2019 14:13 Source: CC16420-06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limi RPD Limit Notes 1,1-Dichloroethene 17 1.0 ug/L 20.0 0.21 U 85 75-133 Benzene 19 1.0 ug/L 20.0 0.15 U 94 80-134 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 90 80-120 Toluene 17 1.0 ug/L 20.0 0.14 U 87 71-120 Trichloroethene 16 1.0 ug/L 20.0 0.15 U 82 74-120 4-8romofluorobenzene 44 u9/L 50.0 89 53-136 Dibromofluoromethane 44 u9/L 50.0 88 67-129 Toluene-& 37 u9/L 50.0 75 59-134 Matrix Spike Dup (9I27013-MSD1) Prepared: 09/27/2019 09:49 Analyzed: 09/27/2019 14:45 Source: CC16420-06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 18 1.0 ug/L 20.0 0.21 U 91 75-133 7 20 Benzene 21 1.0 ug/L 20.0 0.15 U 104 80-134 10 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 96 80-120 7 16 Toluene 19 1.0 ug/L 20.0 0.14 U 97 71-120 11 17 Trichloroethene 18 1.0 ug/L 20.0 0.15 U 91 74-120 10 22 4-Bromofluorobenzene 43 u9/L 50.0 86 53-136 Dibromofluoromethane 43 u9/L 50.0 87 67-129 Toluene-d8 38 u91L 50.0 76 59-134 Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch 9125035 - EPA 50308 MS Blank (9I25035-BLK1) Prepared: 09/25/2019 00:00 Analyzed: 09/25/2019 10:54 Spike Source %REC RPD Analvte Result Flao POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 1.2 U 2.0 ug/L Toluene-d8 5.5 u9/L 5.00 111 75-125 LCS (9I25035-BS1) Prepared: 09/25/2019 00:00 Analyzed: 09/25/2019 09:47 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limi RPD Limit Notes 1,4-Dioxane 25 2.0 ug/L 25.0 101 80-133 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 45 Of 52 0Nk"q09 www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch 9125035 - EPA 5030E MS - Continued LCS (9I25035-BSI) Continued Prepared: 09/25/2019 00:00 Analyzed: 09/25/2019 09:47 Spike Source %REC RPD Analvte Result Flao POL Units Level Result %REC Limits RPD Limit Notes Toluene-& 4.9 u9/L 5.00 98 75-125 LCS Dup (9I25035-BSD1) Prepared: 09/25/2019 00:00 Analyzed: 09/25/2019 10:20 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 28 2.0 ug/L 25.0 113 80-133 11 19 QM-10 Toluene-& 4.2 u9/L 5.00 83 75-125 QM-10 Batch 9125047 - EPA 50306 MS Blank (9I25047-BLKI) Prepared: 09/25/2019 14:09 Analyzed: 09/25/2019 23:33 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 1.2 U 2.0 ug/L Toluene-& 5.6 u9/L 5.00 113 75-125 LCS (9I25047-BSI) Prepared: 09/25/2019 14:09 Analyzed: 09/25/2019 22:20 Spike Source %REC RPD Analvte Result Flau POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 24 2.0 ug/L 25.0 95 80-133 Toluene-d8 4.8 u9/L 5.00 97 75-125 LCS Dup (9I25047-BSD1) Prepared: 09/25/2019 14:09 Analyzed: 09/25/2019 22:57 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 24 2.0 ug/L 25.0 95 80-133 0.5 19 QM-10 Toluene-& 5.0 u9/L 5.00 100 75-125 QM-10 Batch 9126041 - EPA 5030B MS Blank (9I26041-BLKI) Prepared: 09/26/2019 00:00 Analyzed: 09/26/2019 11:59 Spike Source %REC RPD Analvte Result Flao POL Knits Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 1.2 U 2.0 ug/L Toluene-d8 4.8 u9/L 5.00 97 75-125 LCS (9I26041-BS1) Prepared: 09/26/2019 00:00 Analyzed: 09/26/2019 10:52 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Mlina Notes 1,4-Dioxane 23 2.0 ug/L 25.0 93 80-133 Toluene-& 5.0 u9/L 5,00 99 75-125 LCS Dup (9I26041-BSD1) Prepared: 09/26/2019 00:00 Analyzed: 09/26/2019 11:25 Spike Source %REC RPD Analvte Result Flao POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 27 2.0 ug/L 25.0 108 80-133 16 19 QM-10 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 46 of 0Nk"q09 www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch 9126041 - EPA 5030E MS - Continued LCS Dup (9I26041-BSDI) Continued Prepared: 09/26/2019 00:00 Analyzed: 09/26/2019 11:25 Spike Source %REC RPD Analvte Result Flao POL Units Level Result %REC Limits RPD Limit Notes Toluene-& 5.5 u9/L 5.00 109 75-125 QM-10 Batch 9127029 - EPA 5030E MS Blank (9I27029-BLKI) Prepared: 09/27/2019 00:00 Analyzed: 09/27/2019 13:30 Spike Source a/o REC RPD Analvte Result Flaa POL Uni Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 1.2 U 2.0 ug/L Toluene-d8 5.7 u9/L 5.00 114 75-125 LCS (9I27029-BS1) Prepared: 09/27/2019 00:00 Analyzed: 09/27/2019 12:25 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 26 2.0 ug/L 25.0 103 80-133 Toluene-& 5.1 u9/L 5.00 102 75-125 LCS Dup (9I27029-BSD1) Prepared: 09/27/2019 00:00 Analyzed: 09/27/2019 12:57 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 27 2.0 ug/L 25.0 109 80-133 5 19 QM-10 Toluene-d8 5.5 u9/L 5.00 110 75-125 QM-10 Batch 9JO2042 - EPA 5030E MS Blank (9302042-BLK3) Prepared: 10/02/2019 14:07 Analyzed: 10/03/2019 01:32 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 1.2 U 2.0 ug/L Toluene-& 5.4 u9/L 5.00 108 75-125 LCS (9102042-BSI) Prepared: 10/02/2019 14:07 Analyzed: 10/02/2019 23:02 Spike Source %REC RPD Analvte Result Flaa POL Knits Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 24 2.0 ug/L 25.0 96 80-133 Toluene-d8 5.3 u9/L 5.00 105 75-125 Matrix Spike (9302042-MS1) Prepared: 10/02/2019 14:07 Analyzed: 10/02/2019 23:39 Source: AC06689-02 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Mlina Notes 1,4-Dioxane 24 2.0 ug/L 25.0 1.2 U 96 80-133 Toluene-& 5.4 u9/L 5,00 109 75-125 Matrix Spike Dup (9102042-MSD1) Prepared: 10/02/2019 14:07 Analyzed: 10/03/2019 00:17 Source: AC06689-02 Spike Source %REC RPD Analvte Result Flao POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 25 2.0 ug/L 25.0 1.2 U 100 80-133 4 19 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 47 Of 5Z 0Nk"q09 www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch 9JO2042 - EPA 5030B MS - Continued Matrix Spike Dup (9302042-MSDI) Continued Prepared: 10/02/2019 14:07 Analyzed: 10/03/2019 00:17 Source: AC06689-02 Spike Source %REC RPD Analvte Result Flao POL Units Level Result %REC Limits RPD Limit Notes Toluene-& 6.1 u9/L 5,00 123 75-125 Batch 9JO3063 - EPA 5030E MS Blank (9303063-BLK3) Prepared: 10/03/2019 15:18 Analyzed: 10/04/2019 00:04 Spike Source %REC RPD Analvte Result Flaa POL Uni Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 1.2 U 2.0 ug/L Toluene-d8 4.8 u9/L 5.00 97 75-125 LCS (9J03063-BS1) Prepared: 10/03/2019 15:18 Analyzed: 10/03/2019 21:39 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 28 2.0 ug/L 25.0 111 80-133 Toluene-& 5.5 u9/L 5.00 110 75-125 Matrix Spike (9303063-MS1) Prepared: 10/03/2019 15:18 Analyzed: 10/03/2019 22:15 Source: AC06736-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 21 2.0 ug/L 25.0 1.2 U 83 80-133 Toluene-& 4.9 u91L 5.00 98 75-125 Matrix Spike Dup (9303063-MSD1) Prepared: 10/03/2019 15:18 Analyzed: 10/03/2019 22:52 Source: AC06736-01 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 23 2.0 ug/L 25.0 1.2 U 91 80-133 9 19 Toluene-& 5.1 u91L 5.00 101 75-125 Batch 9JO4030 - EPA 5030B MS Blank (9104030-BLK3) Prepared: 10/04/2019 00:00 Analyzed: 10/04/2019 11:39 Spike Source %REC RPD Analvte Result Flaa POL Knits Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 1.2 U 2.0 ug/L Toluene-d8 5.0 u9/L 5.00 100 75-125 LCS (9J04030-BSI) Prepared: 10/04/2019 00:00 Analyzed: 10/04/2019 10:03 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Mlina Notes 1,4-Dioxane 25 2.0 ug/L 25.0 100 80-133 Toluene-& 5.0 u9/L 5,00 101 75-125 LCS Dup (9104030-BSD1) Prepared: 10/04/2019 00:00 Analyzed: 10/04/2019 12:12 Spike Source %REC RPD Analvte Result Flao POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 21 2.0 ug/L 25.0 84 80-133 17 19 QM-10 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 48 Of 5Z (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch 9JO4030 - EPA 5030E MS - Continued LCS Dup (9304030-BSD3) Continued Prepared: 10/04/2019 00:00 Analyzed: 10/04/2019 12:12 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes Toluene-d8 5.2 ug/L 5.00 104 75-125 QM-10 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 49 Of 52 (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. 3-05 Result may be biased low. Associated calibration verification standard did not meet the minimum control limit. 3-06 The associated laboratory control sample exhibited low bias; the reported result should be considered to be a minimum estimate. Q-01 Analysis performed outside of method - specified holding time. QI-02 Internal standard outside acceptance limits. Samples results are considered estimated. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QM-10 LCS/LCSD were analyzed in place of MS/MSD. QM-11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits. QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there is no impact. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 50 of 52 E 0 cc 2 0_ 9 LU v a c m v � L] � LLoU� 0r Z U U) W_ Q 0 OaY cc �mN a Z 3 LL 0s%� H LJ 010 QW O O Y a cc LLJ 0 U z o a — a � Z d N y 0ro� Z —� o LLL 2 o c Ccl Q m. C Cc 41 co 7 rn 9 C E O ro a�i F- LU 0. C a Y T CL E E� E m E eki a Q Uc m a Q E 7 c a o � c � m o U a = N K N Z O y C � d M m p m Z c En N m L o Q U m m m } m m m N_ o n m w O m U l J a E U N a � c oa rIQ H m o � o �o 01 V41S 009L9'PeAuWX9 009L8'009U x X X X X X x x x X v U m n V 4 � > i0 m F U o a„y � 7 Z N� Z � C S U ��[j��j r � $ � �('�� � � Q m cU�y� y c � •v � � � �' cc cc cl men en E a c• Cr (z ► v V' C.P N O i M o m E m ❑ rn m o w c� Q .co co ❑ ❑ ° mil co C a7 CC] 'sn 4 1 m ? !� ? Ln LO (D 1-- 1-- 7 a o E� nQi /� V! z 1 �3J� v/ ,3„ �// co�/J � uJ �?/�' v/ �3/��/�� �// WI �3/� wf �/� UJ z a im r ,'�, 4 41 Page 51 of 52 q� NNE r!1 Ul w -p cd _ F a c Q o {� a _ Y c Cn L1J i _❑ E E m cIr ❑ ❑ m Z C�11 o J a m V Q Q � 9 � U a o U � 0 UO � m 'v v m N � x y C Z Q1 m m a m 2 � r � 3 o a U m © = o o n c o = � cai W a U E E E O ` d 01 WIS ❑09Ze'PePuswx 009L9'009L8 x X x x x K x `e V C Yo m a m CO CO "t `t .1 to w U � m q � 'N O a o m � m V m m m v o n�m E U v ❑�Ad o tF1 a '' nn c o h ! h1 M 4 M s ¢ ¢ 0 n aV 3i. w m zi E � N obi p1 v ~ F- r y Z ci (~,� V _ � � �► m vi d m C7 `J` o G ao .� U �. =' m o a� �° - a oa m N- � U N r m O r r Y Y Y 1 ` - a v U 0 5 m mm E a f Page 52 o2 U Q U12 H 2�SENCO Laboratories 9g Accurate. Timely. Respousive. luuavative. 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, October 18, 2019 Babb & Associates (BA024) Attn: Gary Babb 5506 Bradford Pear Court Raleigh, NC 27606 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Seaboard/Riverdale Landfill ENCO Workorder(s): CC14233 Dear Gary Babb, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Friday, September 13, 2019. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative if applicable. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Bill Scott Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 1 of 74 PROJECT NARRATIVE Client: Babb & Associates (BA024) Project: Seaboard/Riverdale Landfill Lab ID: CC14233-Rev Overview (� �Eo www.encolabs.com This report is an amendment to the original report dated 09/26/19. This report has been revised due to samples MW-12D and W-4A being reported at over diluted analyses. The samples were re -analyzed at correct dilutions. Both sets of data have been reported and qualified appropriately. Environmental Conservation Laboratories, Inc. (ENCO) analyzed all submitted samples in accordance with the methods referenced in the laboratory report. Any particular difficulties encountered during sample handling by ENCO are discussed in the QC Remarks section below. Quality Control Samples No Comments Quality Control Remarks No Comments Other Comments 1,4-dioxane containers for sample PW-SF1 contained air bubbles larger than 6mm in diamter. The analytical data presented in this report are consistent with the methods as referenced in the analytical report. Any exceptions or deviations are noted in the QC remarks section of this narrative or in the Flags/Notes and Definitions section of the report. Released By: Environmental Conservation Laboratories, Inc. Bill Scott Project Manager FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 2 of 74 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 4401-MW3 Lab ID: CC14233-01 Sampled: 09/10/19 11:10 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MIS 09/24/19 09/16/19 12:10 09/17/19 15:38 EPA 8260D EPA 503013_MS 09/24/19 09/19/19 00:00 09/19/19 15:26 Client ID: 4401-MW3C Lab ID: CC14233-02 Sampled: 09/11/19 11:00 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 09/25/19 09/18/19 10:13 09/18/19 17:00 EPA 8260D EPA 503013_MS 09/25/19 09/20/19 00:00 09/20/19 15:25 Client ID: 4401-MW6 Lab ID: CC14233-03 Sampled: 09/12/19 11:00 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 09/26/19 09/18/19 10:13 09/18/19 17:31 EPA 8260D EPA 5030B_MS 09/26/19 09/19/19 00:00 09/19/19 16:02 Client ID: 4401-MW10 Lab ID: CC14233-04 Sampled: 09/10/19 14:20 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 09/24/19 09/16/19 12:10 09/17/19 16:09 EPA 8260D EPA 503013_MS 09/24/19 09/19/19 00:00 09/19/19 16:38 Client ID: 4401-MW12A Lab ID: CC14233-05 Sampled: 09/10/19 15:00 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 09/24/19 09/16/19 12:10 09/17/19 16:41 EPA 8260D EPA 503013_MS 09/24/19 09/19/19 00:00 09/19/19 17:15 Client ID: 4401-MW12B Lab ID: CC14233-06 Sampled: 09/11/19 14:30 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(sl Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 09/25/19 09/18/19 10:13 09/18/19 18:02 EPA 8260D EPA 5030B_MS 09/25/19 09/19/19 00:00 09/19/19 17:51 Client ID: 4401-MW12D Lab ID: CC14233-07 Sampled: 09/12/19 08:45 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 09/26/19 09/18/19 10:13 09/18/19 18:34 EPA 8260D EPA 503013_MS 09/26/19 09/20/19 00:00 09/20/19 16:02 Client ID: 4401-MW12D Lab ID: CC14233-07RE1 Sampled: 09/12/19 08:45 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 09/26/19 09/18/19 10:13 10/16/19 07:58 Client ID: 4401-MW15A Lab ID: CC14233-08 Sampled: 09/10/19 13:15 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 09/24/19 09/16/19 12:10 09/17/19 17:12 EPA 8260D EPA 503013_MS 09/24/19 09/19/19 00:00 09/19/19 18:27 Client ID: 4401-OWDR2 Lab ID: CC14233-09RE1 Sampled: 09/11/19 14:45 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 09/25/19 09/18/19 10:13 09/18/19 19:05 EPA 8260D EPA 5030B_MIS 09/25/19 09/20/19 00:00 09/20/19 12:23 Client ID: 4401-OWLFS2 Lab ID: CC14233-10 Sampled: 09/12/19 08:30 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 09/26/19 09/18/19 10:13 09/18/19 19:36 EPA 8260D EPA 503013_MS 09/26/19 09/20/19 00:00 09/20/19 16:39 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 3 Of 74 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 4401-PW3D Lab ID: CC14233-11 Sampled: 09/11/19 09:50 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 09/25/19 09/16/19 12:10 09/17/19 18:14 EPA 8260D EPA 503013_MS 09/25/19 09/19/19 00:00 09/19/19 19:42 Client ID: 4401-PW4I Lab ID: CC14233-12 Sampled: 09/11/19 10:00 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 09/25/19 09/20/19 00:00 09/20/19 17:16 Client ID: 4401-PW4I Lab ID: CC14233-12RE1 Sampled: 09/11/19 10:00 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(-.) EPA 8260D EPA 503013_MS 09/25/19 09/18/19 10:13 09/18/19 20:07 Client ID: 4401-PWSD Lab ID: CC14233-13 Sampled: 09/11/19 15:00 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 09/25/19 09/20/19 00:00 09/20/19 17:53 Client ID: 4401-PWSD Lab ID: CC14233-13RE1 Sampled: 09/11/19 15:00 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 09/25/19 09/20/19 12:27 09/20/19 19:40 Client ID: 4401-PW6I Lab ID: CC14233-14 Sampled: 09/12/19 10:45 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 09/26/19 09/18/19 10:13 09/18/19 21:09 EPA 8260D EPA 503013_MS 09/26/19 09/20/19 14:35 09/21/19 00:35 Client ID: 4401-PW6D Lab ID: CC14233-15 Sampled: 09/12/19 10:00 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 09/26/19 09/18/19 10:13 09/18/19 21:40 Client ID: 4401-PW6D Lab ID: CC14233-15RE1 Sampled: 09/12/19 10:00 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 09/26/19 09/23/19 00:00 09/23/19 13:02 Client ID: 4401-PWSOI Lab ID: CC14233-16 Sampled: 09/12/19 11:30 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 09/26/19 09/18/19 10:13 09/18/19 22:11 EPA 8260D EPA 503013_MS 09/26/19 09/20/19 00:00 09/20/19 18:29 Client ID: 4401-PW10D Lab ID: CC14233-17 Sampled: 09/12/19 10:00 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 5030B_MS 09/26/19 09/18/19 10:13 09/18/19 22:43 EPA 8260D EPA 5030B_MS 09/26/19 09/20/19 14:35 09/21/19 01:49 Client ID: 4401-PW12I Lab ID: CC14233-18 Sampled: 09/11/19 11:30 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 09/25/19 09/18/19 10:13 09/18/19 23:14 EPA 8260D EPA 503013_MS 09/25/19 09/20/19 00:00 09/20/19 19:05 Client ID: 4401-PW13I Lab ID: CC14233-19 Sampled: 09/11/19 11:45 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 09/25/19 09/18/19 10:13 09/18/19 23:45 EPA 8260D EPA 503013_MS 09/25/19 09/20/19 00:00 09/20/19 19:41 Client ID: 4401-W4A Lab ID: CC14233-20 Sampled: 09/11/19 09:30 Received: 09/13/19 12:35 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 8260D EPA 503013_MS 09/25/19 09/18/19 10:13 09/19/19 00:16 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 4 Of 74 (� �Eo www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: 4401-W4A Lab ID: CC14233-20RE1 Sampled: 09/11/19 09:30 Received: 09/13/19 12:35 Parameter EPA 8260D Preparation EPA 5030B_MS Hold Date/Time(s) 09/25/19 Prep Date/Time(s) 09/23/19 00:00 Analysis Date/Time(s) 09/23/19 13:37 Client ID: 4401-W4A Lab ID: CC14233-20RE2 Sampled: 09/11/19 09:30 Received: 09/13/19 12:35 Parameter EPA 8260D Preparation EPA 5030B_MS Hold Date/Time(s) 09/25/19 Prep Date/Time(s) 10/16/19 11:10 Analysis Date/Time(s) 10/16/19 17:16 Client ID: 4401-PWSF1 Lab ID: CC14233-21 Sampled: 09/10/19 13:30 Received: 09/13/19 12:35 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 09/24/19 Prep Date/Time(s) 09/19/19 00:00 Analysis Date/Time(s) 09/19/19 20:19 Client ID: 4401-PWSF1 Lab ID: CC14233-21RE2 Sampled: 09/10/19 13:30 Received: 09/13/19 12:35 Parameter EPA 8260D Preparation EPA 503013_MS Hold Date/Time(s) 09/24/19 Prep Date/Time(s) 09/20/19 13:44 Analysis Date/Time(s) 09/24/19 19:09 Client ID: 4401-TripBlank Lab ID: CC14233-22 Sampled: 09/10/19 11:10 Received: 09/13/19 12:35 Parameter EPA 8260D EPA 8260D Preparation EPA 503013_MS EPA 5030B_MS Hold Date/Time(sl 09/24/19 09/24/19 Prep Date/Time(s) 09/16/19 12:10 09/19/19 00:00 Analysis Date/Time(s) 09/17/19 15:07 09/19/19 20:56 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page) Of 74 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 4401-MW3C Lab ID: CC14233-02 Anala Results Flag MDL POLL Units Method Notes 1,1-Dichloroethane 41 D 1.3 10 ug/L EPA 8260D 1,1-Dichloroethene 17 D 2.1 10 ug/L EPA 8260D 1,4-Dioxane 94 D 12 20 ug/L EPA 8260D Chlorobenzene 50 D 1.7 10 ug/L EPA 8260D cis-1,2-Dichloroethene 72 D 1.5 10 ug/L EPA 8260D Vinyl chloride 14 D 3.2 10 ug/L EPA 8260D Client ID: 4401-MW6 Lab ID: CC14233-03 Anala Results Flag MDL POLL Units Method Notes 1,1-Dichloroethane 5.4 0.13 1.0 ug/L EPA 8260D 1,4-Dioxane 29 1.2 2.0 ug/L EPA 8260D Acetone 27 10 20 ug/L EPA 8260D Benzene 0.45 1 0.15 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 4.2 0.15 1.0 ug/L EPA 8260D Vinyl chloride 1.1 0.32 1.0 ug/L EPA 8260D Client ID: 4401-MW10 Lab ID: CC14233-04 Anala Results Flag MDL POLL Units Method Notes 1,4-Dioxane 72 D 6.0 10 ug/L EPA 8260D Chlorobenzene 1.5 0.17 1.0 ug/L EPA 8260D Client ID: 4401-MW12A Lab ID: CC14233-05 Anala Results Flag MDL POLL Units Method Notes 1,4-Dichlorobenzene 2.9 0.19 1.0 ug/L EPA 8260D 1,4-Dioxane 180 D 12 20 ug/L EPA 8260D Acetone 16 1 10 20 ug/L EPA 8260D Chlorobenzene 6.2 0.17 1.0 ug/L EPA 8260D Client ID: 4401-MW12B Lab ID: CC14233-06 Anala Results Flag MDL POLL Units Method Notes 1,4-Dichlorobenzene 3.1 0.19 1.0 ug/L EPA 8260D 1,4-Dioxane 120 D 6.0 10 ug/L EPA 8260D Benzene 0.48 1 0.15 1.0 ug/L EPA 8260D Chlorobenzene 10 0.17 1.0 ug/L EPA 8260D Client ID: 4401-MW12D Lab ID: CC14233-07 Anala Results Flag MDL POLL Units Method Notes 1,4-Dioxane 3.7 1.2 2.0 ug/L EPA 8260D Client ID: 4401-MW15A Lab ID: CC14233-08 Anala Results Flag MDL POLL Units Method Notes 1,4-Dioxane 1400 D 120 200 ug/L EPA 8260D Chlorobenzene 190 D 0.85 5.0 ug/L EPA 8260D Client ID: 4401-OWDR2 Lab ID: CC14233-09RE1 Anala Results Flag MDL POLL Units Method Notes 1,1,1-Trichloroethane 12 D 0.60 5.0 ug/L EPA 8260D 1,1-Dichloroethane 200 D 0.65 5.0 ug/L EPA 8260D 1,1-Dichloroethene 84 D 1.0 5.0 ug/L EPA 8260D 1,2-Dichloroethane 11 D 1.0 5.0 ug/L EPA 8260D 1,4-Dioxane 250 D 6.0 10 ug/L EPA 8260D Benzene 6.5 D 0.75 5.0 ug/L EPA 8260D Chlorobenzene 260 D 0.85 5.0 ug/L EPA 8260D Chloroethane 12 D 1.2 5.0 ug/L EPA 8260D cis-1,2-Dichloroethene 290 D 0.75 5.0 ug/L EPA 8260D Vinyl chloride 52 D 1.6 5.0 ug/L EPA 8260D Client ID: 4401-OWLFS2 Lab ID: CC14233-10 Anala Results Flag MDL POLL Units Method Notes 1,1-Dichloroethane 0.80 1 0.13 1.0 ug/L EPA 8260D 1,4-Dioxane 210 D 6.0 10 ug/L EPA 8260D Benzene 0.48 1 0.15 1.0 ug/L EPA 8260D Chlorobenzene 3.1 0.17 1.0 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 6 Of 74 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 4401-PW3D Lab ID: CC14233-11 Anala Results Flag MDL POLL Units Method Notes 1,1,1-Trichloroethane 860 D 24 200 ug/L EPA 8260D 1,1-Dichloroethane 480 D 26 200 ug/L EPA 8260D 1,1-Dichloroethene 1100 D 42 200 ug/L EPA 8260D 1,2-Dichloroethane 14000 D 42 200 ug/L EPA 8260D 1,4-Dioxane 140 D 6.0 10 ug/L EPA 8260D 2-Butanone 560 ID 260 1000 ug/L EPA 8260D 4-Methyl-2-pentanone 220 ID 220 1000 ug/L EPA 8260D Benzene 190 ID 30 200 ug/L EPA 8260D Chlorobenzene 11000 D 34 200 ug/L EPA 8260D cis-1,2-Dichloroethene 350 D 30 200 ug/L EPA 8260D Methylene chloride 1300 D 46 200 ug/L EPA 8260D Tetrachloroethene 620 D 34 200 ug/L EPA 8260D Toluene 470 D 28 200 ua/L EPA 8260D I Client ID: 4401-PW4I Lab ID: CC14233-12 Anala Results Flag MDL POLL Units Method Notes 1,4-Dioxane 200 D 6.0 10 ug/L EPA 8260D Client ID: 4401-PW4I Lab ID: CC14233-12RE3 Anala Results Flag MDL POLL Units Method Notes 1,1,1-Trichloroethane 32 D 0.60 5.0 ug/L EPA 8260D 1,1-Dichloroethane 69 D 0.65 5.0 ug/L EPA 8260D 1,1-Dichloroethene 37 D 1.0 5.0 ug/L EPA 8260D 1,2-Dichloroethane 36 D 1.0 5.0 ug/L EPA 8260D Chlorobenzene 60 D 0.85 5.0 ug/L EPA 8260D cis-1,2-Dichloroethene 230 D 0.75 5.0 ug/L EPA 8260D Tetrachloroethene 13 D 0.85 5.0 ug/L EPA 8260D Vinyl chloride 43 D 1.6 5.0 ug/L EPA 8260D Client ID: 4401-PW5D Lab ID: CC14233-13 Anala Results Flag MDL POLL Units Method Notes 1,4-Dioxane 240 D 60 100 ug/L EPA 8260D Client ID: 4401-PW5D Lab ID: CC14233-13RE1 Anala Results Flag MDL POLL Units Method Notes 1,1,1-Trichloroethane 6.5 D 0.60 5.0 ug/L EPA 8260D 1,1-Dichloroethane 170 D 0.65 5.0 ug/L EPA 8260D 1,1-Dichloroethene 55 D 1.0 5.0 ug/L EPA 8260D 1,2-Dichloroethane 8.0 D 1.0 5.0 ug/L EPA 8260D Benzene 4.4 ID 0.75 5.0 ug/L EPA 8260D Chlorobenzene 220 D 0.85 5.0 ug/L EPA 8260D cis-1,2-Dichloroethene 180 D 0.75 5.0 ug/L EPA 8260D Vinyl chloride 56 D 1.6 5.0 ug/L EPA 8260D Client ID: 4401-PW6I Lab ID: CC14233-14 Anala Results Flag MDL POLL Units Method Notes 1,1-Dichloroethane 19 0.13 1.0 ug/L EPA 8260D 1,1-Dichloroethene 1.0 0.21 1.0 ug/L EPA 8260D 1,2-Dichloroethane 2.9 0.21 1.0 ug/L EPA 8260D 1,4-Dichlorobenzene 1.8 0.19 1.0 ug/L EPA 8260D 1,4-Dioxane 79 1.2 2.0 ug/L EPA 8260D Benzene 0.74 1 0.15 1.0 ug/L EPA 8260D Chlorobenzene 13 0.17 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 26 0.15 1.0 ug/L EPA 8260D Tetrachloroethene 0.42 1 0.17 1.0 ug/L EPA 8260D Vinyl chloride 5.3 0.32 1.0 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 7 Of 74 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 4401-PW6D Lab ID: CC14233-15 Anala Results Flag MDL POLL Units Method Notes 1,1,1-Trichloroethane 4.5 0.12 1.0 ug/L EPA 8260D 1,1-Dichloroethane 120 0.13 1.0 ug/L EPA 8260D 1,1-Dichloroethene 42 0.21 1.0 ug/L EPA 8260D 1,2-Dichloroethane 4.7 0.21 1.0 ug/L EPA 8260D Benzene 1.4 0.15 1.0 ug/L EPA 8260D Chlorobenzene 120 0.17 1.0 ug/L EPA 8260D Chloroethane 7.0 0.23 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 150 0.15 1.0 ug/L EPA 8260D Methylene chloride 0.84 1 0.23 1.0 ug/L EPA 8260D Tetrachloroethene 0.84 1 0.17 1.0 ug/L EPA 8260D trans-1,2-Dichloroethene 1.6 0.21 1.0 ug/L EPA 8260D Vinyl chloride 25 0.32 1.0 ug/L EPA 8260D Client ID: 4401-PW6D Lab ID: CC14233-15RE3 Anala Results Flag MDL POLL Units Method Notes 1,4-Dioxane 100 D 6.0 10 ug/L EPA 8260D Client ID: 4401-PW10I Lab ID: CC14233-16 Anala Results Flag MDL POLL Units Method Notes 1,1-Dichloroethane 12 0.13 1.0 ug/L EPA 8260D 1,4-Dichlorobenzene 2.4 0.19 1.0 ug/L EPA 8260D 1,4-Dioxane 260 D 6.0 10 ug/L EPA 8260D Benzene 1.0 0.15 1.0 ug/L EPA 8260D Chlorobenzene 2.6 0.17 1.0 ug/L EPA 8260D Chloroethane 5.9 0.23 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 4.2 0.15 1.0 ug/L EPA 8260D Vinyl chloride 3.7 0.32 1.0 ug/L EPA 8260D Client ID: 4401-PW12I Lab ID: CC14233-18 Anala Results Flag MDL POLL Units Method Notes 1,4-Dioxane 1.2 1 1.2 2.0 ug/L EPA 8260D Client ID: 4401-PW13I Lab ID: CC14233-19 Anala Results Flag MDL POLL Units Method Notes 1,1-Dichloroethane 94 0.13 1.0 ug/L EPA 8260D 1,1-Dichloroethene 18 0.21 1.0 ug/L EPA 8260D 1,2-Dichloroethane 3.6 0.21 1.0 ug/L EPA 8260D 1,4-Dioxane 44 1.2 2.0 ug/L EPA 8260D Benzene 2.4 0.15 1.0 ug/L EPA 8260D Chlorobenzene 8.9 0.17 1.0 ug/L EPA 8260D Chloroethane 1.4 0.23 1.0 ug/L EPA 8260D cis-1,2-Dichloroethene 72 0.15 1.0 ug/L EPA 8260D Tetrachloroethene 0.72 1 0.17 1.0 ug/L EPA 8260D trans-1,2-Dichloroethene 0.44 1 0.21 1.0 ug/L EPA 8260D Vinvl chloride 38 0.32 1.0 ua/L EPA 8260D I Client ID: 4401-W4A Lab ID: CC14233-20RE1 Anala Results Flag MDL POLL Units Method Notes 1,4-Dioxane 54 D 6.0 10 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 8 Of 74 (� �Eo www.encolabs.com SAMPLE DETECTION SUMMARY Client ID: 4401-W4A Lab ID: CC14233-20RE2 Anala Results Flag MDL POLL Units Method Notes 1,1,1-Trichloroethane 12 0.12 1.0 ug/L EPA 8260D Q-01 1,1-Dichloroethane 83 0.13 1.0 ug/L EPA 8260D Q-01 1,1-Dichloroethene 33 0.21 1.0 ug/L EPA 8260D Q-01 1,2-Dichloroethane 2.8 0.21 1.0 ug/L EPA 8260D Q-01 Benzene 7.5 0.15 1.0 ug/L EPA 8260D Q-01 Chlorobenzene 4.4 0.17 1.0 ug/L EPA 8260D Q-01 Chloroethane 13 0.23 1.0 ug/L EPA 8260D Q-01 cis-1,2-Dichloroethene 130 0.15 1.0 ug/L EPA 8260D Q-01 Methylene chloride 0.45 1 0.23 1.0 ug/L EPA 8260D Q-01 Tetrachloroethene 0.81 1 0.17 1.0 ug/L EPA 8260D Q-01 trans-1,2-Dichloroethene 1.3 0.21 1.0 ug/L EPA 8260D Q-01 Trichloroethene 6.0 0.15 1.0 ug/L EPA 8260D Q-01 Vinvl chloride 88 0.32 1.0 ua/L EPA 8260D 0-01 I Client ID: 4401-PWSF3 Lab ID: CC14233-21 Anala Results Flag MDL POLL Units Method Notes 1,4-Dioxane 3200 D 120 200 ug/L EPA 8260D Client ID: 4401-PWSF3 Lab ID: CC14233-21RE2 Anala Results Flag MDL POLL Units Method Notes 1,1,1-Trichloroethane 3100 D 24 200 ug/L EPA 8260D 1,1-Dichloroethane 3500 D 26 200 ug/L EPA 8260D 1,1-Dichloroethene 4100 D 42 200 ug/L EPA 8260D 1,2-Dichloroethane 600 D 42 200 ug/L EPA 8260D Chlorobenzene 1800 D 34 200 ug/L EPA 8260D Chloroform 120 ID 36 200 ug/L EPA 8260D cis-1,2-Dichloroethene 20000 D 30 200 ug/L EPA 8260D Methylene chloride 160 ID 46 200 ug/L EPA 8260D Tetrachloroethene 830 D 34 200 ug/L EPA 8260D Toluene 530 D 28 200 ug/L EPA 8260D Trichloroethene 2900 D 30 200 ug/L EPA 8260D Vinyl chloride 2400 D 64 200 ug/L EPA 8260D FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 9 Of 74 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW1 Lab Sample ID:CC14233-01 Received: 09/13/19 12:35 Matrix: Water Sampled:09/10/19 11:10 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I16024 EPA 8260D 09/17/19 15:38 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 9I16024 EPA 8260D 09/17/19 15:38 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I16024 EPA 8260D 09/17/19 15:38 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I16024 EPA 8260D 09/17/19 15:38 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I16024 EPA 8260D 09/17/19 15:38 REF Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I16024 EPA 8260D 09/17/19 15:38 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I16024 EPA 8260D 09/17/19 15:38 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I16024 EPA 8260D 09/17/19 15:38 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF QV-01 Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I16024 EPA 8260D 09/17/19 15:38 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 10 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW1 Lab Sample ID:CC14233-01 Received: 09/13/19 12:35 Matrix: Water Sampled:09/10/19 11:10 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9I16024 EPA 8260D 09/17/19 15:38 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I16024 EPA 8260D 09/17/19 15:38 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 45 1 50.0 91 % 53-136 9116024 EPA 8260D 09117119 15:38 REF Dlbromofluoromethane 46 1 50.0 93 % 67-129 9116024 EPA 6260D 091171191528 REF Toluene-d8 38 1 50.0 77 % 59-134 9116024 EPA 6260D 091171191538 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes 1,4-Dioxane [123-91-1]^ 1.2 U ug/L 1 1.2 2.0 9I19040 EPA 8260D 09/19/19 15:26 MJH Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-& 4.9 1 5.00 99 % 75-125 9119040 EPA 8260D 0911.9119 15:26 MJH FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 11 of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW3C Lab Sample ID:CC14233-02 Received: 09/13/19 12:35 Matrix: Water Sampled:09/11/19 11:00 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 1.7 UD ug/L 10 1.7 10 9I18027 EPA 8260D 09/18/19 17:00 REF 1,1,1-Trichloroethane [71-55-6]^ 1.2 UD ug/L 10 1.2 10 9I18027 EPA 8260D 09/18/19 17:00 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 2.8 UD ug/L 10 2.8 10 9I18027 EPA 8260D 09/18/19 17:00 REF 1,1,2-Trichloroethane [79-00-5]^ 1.4 UD ug/L 10 1.4 10 9I18027 EPA 8260D 09/18/19 17:00 REF 1,1-Dichloroethane [75-34-3]^ 41 D ug/L 10 1.3 10 9I18027 EPA 8260D 09/18/19 17:00 REF 1,1-Dichloroethene [75-35-4]^ 17 D ug/L 10 2.1 10 9I18027 EPA 8260D 09/18/19 17:00 REF 1,2,3-Trichloropropane [96-18-4]^ 2.3 UD ug/L 10 2.3 10 9I18027 EPA 8260D 09/18/19 17:00 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 4.8 UD ug/L 10 4.8 10 9I18027 EPA 8260D 09/18/19 17:00 REF 1,2-Dibromoethane [106-93-4]^ 6.6 UD ug/L 10 6.6 10 9I18027 EPA 8260D 09/18/19 17:00 REF 1,2-Dichlorobenzene [95-50-1]^ 1.9 UD ug/L 10 1.9 10 9I18027 EPA 8260D 09/18/19 17:00 REF 1,2-Dichloroethane [107-06-2]^ 2.1 UD ug/L 10 2.1 10 9I18027 EPA 8260D 09/18/19 17:00 REF 1,2-Dichloropropane [78-87-5]^ 1.0 UD ug/L 10 1.0 10 9I18027 EPA 8260D 09/18/19 17:00 REF 1,4-Dichlorobenzene [106-46-7]^ 1.9 UD ug/L 10 1.9 10 9I18027 EPA 8260D 09/18/19 17:00 REF 2-Butanone [78-93-3]^ 13 UD ug/L 10 13 50 9I18027 EPA 8260D 09/18/19 17:00 REF 2-Hexanone [591-78-6]^ 8.8 UD ug/L 10 8.8 50 9I18027 EPA 8260D 09/18/19 17:00 REF 4-Methyl-2-pentanone [108-10-1]^ 11 UD ug/L 10 11 50 9I18027 EPA 8260D 09/18/19 17:00 REF Acetone [67-64-1]^ 100 UD ug/L 10 100 200 9I18027 EPA 8260D 09/18/19 17:00 REF Acrylonitrile [107-13-1]^ 35 UD ug/L 10 35 100 9I18027 EPA 8260D 09/18/19 17:00 REF Benzene [71-43-2]^ 1.5 UD ug/L 10 1.5 10 9I18027 EPA 8260D 09/18/19 17:00 REF Bromochloromethane [74-97-5]^ 4.8 UD ug/L 10 4.8 10 9I18027 EPA 8260D 09/18/19 17:00 REF Bromodichloromethane [75-27-4]^ 1.7 UD ug/L 10 1.7 10 9I18027 EPA 8260D 09/18/19 17:00 REF Bromoform [75-25-2]^ 2.2 UD ug/L 10 2.2 10 9I18027 EPA 8260D 09/18/19 17:00 REF Bromomethane [74-83-9]^ 1.4 UD ug/L 10 1.4 10 9I18027 EPA 8260D 09/18/19 17:00 REF Carbon disulfide [75-15-0]^ 15 UD ug/L 10 15 50 9I18027 EPA 8260D 09/18/19 17:00 REF Carbon tetrachloride [56-23-5]^ 1.7 UD ug/L 10 1.7 10 9I18027 EPA 8260D 09/18/19 17:00 REF Chlorobenzene [108-90-7]^ 50 D ug/L 10 1.7 10 9I18027 EPA 8260D 09/18/19 17:00 REF Chloroethane [75-00-3]^ 2.3 UD ug/L 10 2.3 10 9I18027 EPA 8260D 09/18/19 17:00 REF Chloroform [67-66-3]^ 1.8 UD ug/L 10 1.8 10 9I18027 EPA 8260D 09/18/19 17:00 REF Chloromethane [74-87-3]^ 1.3 UD ug/L 10 1.3 10 9I18027 EPA 8260D 09/18/19 17:00 REF cis- 1,2-Dichloroethene [156-59-2]^ 72 D ug/L 10 1.5 10 9I18027 EPA 8260D 09/18/19 17:00 REF cis- 1,3-Dichloropropene [10061-01-5]^ 2.0 UD ug/L 10 2.0 10 9I18027 EPA 8260D 09/18/19 17:00 REF Dibromochloromethane [124-48-1]^ 1.7 UD ug/L 10 1.7 10 9I18027 EPA 8260D 09/18/19 17:00 REF Dibromomethane [74-95-3]^ 2.7 UD ug/L 10 2.7 10 9I18027 EPA 8260D 09/18/19 17:00 REF Ethylbenzene [100-41-4]^ 1.3 UD ug/L 10 1.3 10 9I18027 EPA 8260D 09/18/19 17:00 REF Iodomethane [74-88-4]^ 17 UD ug/L 10 17 50 9I18027 EPA 8260D 09/18/19 17:00 REF m,p-Xylenes [108-38-3/106-42-3]^ 1.7 UD ug/L 10 1.7 20 9I18027 EPA 8260D 09/18/19 17:00 REF Methylene chloride [75-09-2]^ 2.3 UD ug/L 10 2.3 10 9I18027 EPA 8260D 09/18/19 17:00 REF o-Xylene [95-47-6]^ 0.65 UD ug/L 10 0.65 10 9I18027 EPA 8260D 09/18/19 17:00 REF Styrene [100-42-5]^ 1.1 UD ug/L 10 1.1 10 9I18027 EPA 8260D 09/18/19 17:00 REF Tetrachloroethene [127-18-4]^ 1.7 UD ug/L 10 1.7 10 9I18027 EPA 8260D 09/18/19 17:00 REF Toluene [108-88-3]^ 1.4 UD ug/L 10 1.4 10 9I18027 EPA 8260D 09/18/19 17:00 REF trans-1,2-Dichloroethene [156-60-5]^ 2.1 UD ug/L 10 2.1 10 9I18027 EPA 8260D 09/18/19 17:00 REF trans-1,3-Dichloropropene [10061-02-6]^ 1.5 UD ug/L 10 1.5 10 9I18027 EPA 8260D 09/18/19 17:00 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 7.0 UD ug/L 10 7.0 10 9I18027 EPA 8260D 09/18/19 17:00 REF Trichloroethene [79-01-6]^ 1.5 UD ug/L 10 1.5 10 9I18027 EPA 8260D 09/18/19 17:00 REF Trichlorofluoromethane [75-69-4]^ 2.4 UD ug/L 10 2.4 10 9I18027 EPA 8260D 09/18/19 17:00 REF Vinyl acetate [108-05-4]^ 9.5 UD ug/L 10 9.5 50 9I18027 EPA 8260D 09/18/19 17:00 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 12 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW3C Lab Sample ID:CC14233-02 Received: 09/13/19 12:35 Matrix: Water Sampled:09/11/19 11:00 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]^ 14 D ug/L 10 3.2 10 9I18027 EPA 8260D 09/18/19 17:00 REF Xylenes(Total)[1330-20-7]^ 4.5 UD ug/L 10 4.5 30 9I18027 EPA 8260D 09/18/19 17:00 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 45 1 50.0 90 % 53-136 9118027 EPA 8260D 09118119 17:00 REF Dlbromofluoromethane 45 1 50.0 91 % 67-129 9116027 EPA 6260D 09118119 17:00 REF Toluene-d8 39 1 50.0 77 % 59-134 9118027 EPA 6260D 09118119 17:00 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 94 D ug/L 10 12 20 9I20040 EPA 8260D 09/20/19 15:25 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 5.6 1 5.00 113 % 75-125 9120040 EPA 8260D 0912011915:25 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 13 Of 74 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW6 Lab Sample ID:CC14233-03 Received: 09/13/19 12:35 Matrix: Water Sampled:09/12/19 11:00 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF 1,1-Dichloroethane [75-34-3]A 5.4 ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I18027 EPA 8260D 09/18/19 17:31 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 9I18027 EPA 8260D 09/18/19 17:31 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I18027 EPA 8260D 09/18/19 17:31 REF Acetone [67-64-1]A 27 ug/L 1 10 20 9I18027 EPA 8260D 09/18/19 17:31 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I18027 EPA 8260D 09/18/19 17:31 REF Benzene [71-43-2]A 0.45 J ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I18027 EPA 8260D 09/18/19 17:31 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF cis-1,2-Dichloroethene [156-59-2]^ 4.2 ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I18027 EPA 8260D 09/18/19 17:31 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I18027 EPA 8260D 09/18/19 17:31 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I18027 EPA 8260D 09/18/19 17:31 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 14 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW6 Lab Sample ID:CC14233-03 Received: 09/13/19 12:35 Matrix: Water Sampled:09/12/19 11:00 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]^ 1.1 ug/L 1 0.32 1.0 9I18027 EPA 8260D 09/18/19 17:31 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I18027 EPA 8260D 09/18/19 17:31 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 47 1 50.0 93 % 53-136 9118027 EPA 8260D 09118119 1731 REF Dlbromofluoromethane 46 1 50.0 92 % 67-129 9116027 EPA 6260D 09118119 1731 REF Toluene-d8 38 1 50.0 76 % 59-134 9118027 EPA 6260D 09118119 1731 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 29 ug/L 1 1.2 2.0 9I19040 EPA 8260D 09/19/19 16:02 MJH Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 5.3 1 5.00 107 % 75-125 9119040 EPA 8260D 0911911916:02 MJH FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 15 Of 74 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW10 Lab Sample ID:CC14233-04 Received: 09/13/19 12:35 Matrix: Water Sampled:09/10/19 14:20 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I16024 EPA 8260D 09/17/19 16:09 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 9I16024 EPA 8260D 09/17/19 16:09 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I16024 EPA 8260D 09/17/19 16:09 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I16024 EPA 8260D 09/17/19 16:09 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I16024 EPA 8260D 09/17/19 16:09 REF Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I16024 EPA 8260D 09/17/19 16:09 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF Chlorobenzene [108-90-7]^ 1.5 ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I16024 EPA 8260D 09/17/19 16:09 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I16024 EPA 8260D 09/17/19 16:09 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF QV-01 Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I16024 EPA 8260D 09/17/19 16:09 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 16 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW10 Lab Sample ID:CC14233-04 Received: 09/13/19 12:35 Matrix: Water Sampled:09/10/19 14:20 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9I16024 EPA 8260D 09/17/19 16:09 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I16024 EPA 8260D 09/17/19 16:09 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 46 1 50.0 93 % 53-136 9116024 EPA 8260D 09117119 16:09 REF Dlbromofluoromethane 46 1 50.0 92 % 67-129 9116024 EPA 6260D 0911711916:09 REF Toluene-d8 39 1 50.0 77 % 59-134 9116024 EPA 6260D 0911711916:09 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte ICAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 72 D ug/L 5 6.0 10 9I19040 EPA 8260D 09/19/19 16:38 MJH Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 5.1 1 5.00 103 % 75-125 9119040 EPA 8260D 091191191638 MJH FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 17 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW12A Lab Sample ID:CC14233-05 Received: 09/13/19 12:35 Matrix: Water Sampled:09/10/19 15:00 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF 1,1-Dichloroethane [75-34-3]1 0.13 U ug/L 1 0.13 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF 1,1-Dichloroethene [75-35-4]1 0.21 U ug/L 1 0.21 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF 1,2,3-Trichloropropane [96-18-4]1 0.23 U ug/L 1 0.23 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF 1,2-Dibromoethane [106-93-4]1 0.66 U ug/L 1 0.66 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF 1,2-Dichloroethane [107-06-2]1 0.21 U ug/L 1 0.21 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF 1,2-Dichloropropane [78-87-5]1 0.10 U ug/L 1 0.10 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF 1,4-Dichlorobenzene [306-46-7]A 2.9 ug/L 1 0.19 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I16024 EPA 8260D 09/17/19 16:41 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 9I16024 EPA 8260D 09/17/19 16:41 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I16024 EPA 8260D 09/17/19 16:41 REF Acetone [67-64-1]A 16 J ug/L 1 10 20 9I16024 EPA 8260D 09/17/19 16:41 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I16024 EPA 8260D 09/17/19 16:41 REF Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I16024 EPA 8260D 09/17/19 16:41 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF Chlorobenzene [108-90-7]A 6.2 ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF cis- 1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF cis- 1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I16024 EPA 8260D 09/17/19 16:41 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I16024 EPA 8260D 09/17/19 16:41 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF QV-01 Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I16024 EPA 8260D 09/17/19 16:41 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 18 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW12A Lab Sample ID:CC14233-05 Received: 09/13/19 12:35 Matrix: Water Sampled:09/10/19 15:00 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9I16024 EPA 8260D 09/17/19 16:41 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I16024 EPA 8260D 09/17/19 16:41 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 45 1 50.0 91 % 53-136 9116024 EPA 8260D 09117119 16:41 REF Dlbromofluoromethane 47 1 50.0 93 % 67-129 9116024 EPA 6260D 0911711916:41 REF Toluene-d8 39 1 50.0 78 % 59-134 9116024 EPA 6260D 0911711916:41 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte ICAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes 1,4-Dioxane [123-91-1]^ 180 D ug/L 10 12 20 9I19040 EPA 8260D 09/19/19 17:15 MJH Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 5.2 1 5.00 105 % 75-125 9119040 EPA 8260D 0911911917:15 MJH FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 19 Of 74 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW12B Lab Sample ID:CC14233-06 Received: 09/13/19 12:35 Matrix: Water Sampled:09/11/19 14:30 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF 1,4-Dichlorobenzene [106-46-7]A 3.1 ug/L 1 0.19 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I18027 EPA 8260D 09/18/19 18:02 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 9I18027 EPA 8260D 09/18/19 18:02 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I18027 EPA 8260D 09/18/19 18:02 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I18027 EPA 8260D 09/18/19 18:02 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I18027 EPA 8260D 09/18/19 18:02 REF Benzene [71-43-2]A 0.48 J ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I18027 EPA 8260D 09/18/19 18:02 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF Chlorobenzene [108-90-7]A 10 ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I18027 EPA 8260D 09/18/19 18:02 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I18027 EPA 8260D 09/18/19 18:02 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I18027 EPA 8260D 09/18/19 18:02 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 20 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW12B Lab Sample ID:CC14233-06 Received: 09/13/19 12:35 Matrix: Water Sampled:09/11/19 14:30 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9I18027 EPA 8260D 09/18/19 18:02 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I18027 EPA 8260D 09/18/19 18:02 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 46 1 50.0 92 % 53-136 9118027 EPA 8260D 09118119 16:02 REF Dlbromofluoromethane 46 1 50.0 92 % 67-129 9116027 EPA 6260D 09118119 16:02 REF Toluene-d8 38 1 50.0 76 % 59-134 9118027 EPA 6260D 09118119 18:02 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte ICAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes 1,4-Dioxane [123-91-1]^ 120 D ug/L 5 6.0 10 9I19040 EPA 8260D 09/19/19 17:51 MJH Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 5.0 1 5.00 100 % 75-125 9119040 EPA 8260D 0911911917:51 MJH FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 21 of 74 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW12D Lab Sample ID:CC14233-07 Received: 09/13/19 12:35 Matrix: Water Sampled:09/12/19 08:45 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 1.7 UD ug/L 10 1.7 10 9I18027 EPA 8260D 09/18/19 18:34 REF 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 1,1,1-Trichloroethane [71-55-6]^ 1.2 UD ug/L 10 1.2 10 9I18027 EPA 8260D 09/18/19 18:34 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 1,1,2,2-Tetrachloroethane [79-34-5]^ 2.8 UD ug/L 10 2.8 10 9I18027 EPA 8260D 09/18/19 18:34 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 1,1,2-Trichloroethane [79-00-5]^ 1.4 UD ug/L 10 1.4 10 9I18027 EPA 8260D 09/18/19 18:34 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 1,1-Dichloroethane [75-34-3]^ 1.3 UD ug/L 10 1.3 10 9I18027 EPA 8260D 09/18/19 18:34 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 1,1-Dichloroethene [75-35-4]^ 2.1 UD ug/L 10 2.1 10 9I18027 EPA 8260D 09/18/19 18:34 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 1,2,3-Trichloropropane [96-18-4]^ 2.3 UD ug/L 10 2.3 10 9I18027 EPA 8260D 09/18/19 18:34 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 1,2-Dibromo-3-chloropropane [96-12-8]^ 4.8 UD ug/L 10 4.8 10 9I18027 EPA 8260D 09/18/19 18:34 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 1,2-Dibromoethane [106-93-4]^ 6.6 UD ug/L 10 6.6 10 9I18027 EPA 8260D 09/18/19 18:34 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 1,2-Dichlorobenzene [95-50-1]^ 1.9 UD ug/L 10 1.9 10 9I18027 EPA 8260D 09/18/19 18:34 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 1,2-Dichloroethane [107-06-2]^ 2.1 UD ug/L 10 2.1 10 9I18027 EPA 8260D 09/18/19 18:34 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 1,2-Dichloropropane [78-87-5]^ 1.0 UD ug/L 10 1.0 10 9I18027 EPA 8260D 09/18/19 18:34 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 1,4-Dichlorobenzene [106-46-7]^ 1.9 UD ug/L 10 1.9 10 9I18027 EPA 8260D 09/18/19 18:34 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 2-Butanone [78-93-3]^ 13 UD ug/L 10 13 50 9I18027 EPA 8260D 09/18/19 18:34 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 2-Hexanone [591-78-6]^ 8.8 UD ug/L 10 8.8 50 9I18027 EPA 8260D 09/18/19 18:34 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 4-Methyl-2-pentanone [108-10-1]^ 11 UD ug/L 10 11 50 9I18027 EPA 8260D 09/18/19 18:34 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Acetone [67-64-1]^ 100 UD ug/L 10 100 200 9I18027 EPA 8260D 09/18/19 18:34 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Acrylonitrile [107-13-1]^ 35 UD ug/L 10 35 100 9I18027 EPA 8260D 09/18/19 18:34 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Benzene [71-43-2]^ 1.5 UD ug/L 10 1.5 10 9I18027 EPA 8260D 09/18/19 18:34 REF Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Bromochloromethane [74-97-5]^ 4.8 UD ug/L 10 4.8 10 9I18027 EPA 8260D 09/18/19 18:34 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Bromodichloromethane [75-27-4]^ 1.7 UD ug/L 10 1.7 10 9I18027 EPA 8260D 09/18/19 18:34 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Bromoform [75-25-2]^ 2.2 UD ug/L 10 2.2 10 9I18027 EPA 8260D 09/18/19 18:34 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Bromomethane [74-83-9]^ 1.4 UD ug/L 10 1.4 10 9I18027 EPA 8260D 09/18/19 18:34 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Carbon disulfide [75-15-0]^ 15 UD ug/L 10 15 50 9I18027 EPA 8260D 09/18/19 18:34 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 22 Of 74 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW12D Lab Sample ID:CC14233-07 Received: 09/13/19 12:35 Matrix: Water Sampled:09/12/19 08:45 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Carbon tetrachloride [56-23-5]^ 1.7 UD ug/L 10 1.7 10 9I18027 EPA 8260D 09/18/19 18:34 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Chlorobenzene [108-90-7]^ 1.7 UD ug/L 10 1.7 10 9I18027 EPA 8260D 09/18/19 18:34 REF Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Chloroethane [75-00-3]^ 2.3 UD ug/L 10 2.3 10 9I18027 EPA 8260D 09/18/19 18:34 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Chloroform [67-66-3]^ 1.8 UD ug/L 10 1.8 10 9I18027 EPA 8260D 09/18/19 18:34 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Chloromethane [74-87-3]^ 1.3 UD ug/L 10 1.3 10 9I18027 EPA 8260D 09/18/19 18:34 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 cis-1,2-Dichloroethene [156-59-2]^ 1.5 UD ug/L 10 1.5 10 9I18027 EPA 8260D 09/18/19 18:34 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 cis-1,3-Dichloropropene [10061-01-5]^ 2.0 UD ug/L 10 2.0 10 9I18027 EPA 8260D 09/18/19 18:34 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Dibromochloromethane [124-48-1]^ 1.7 UD ug/L 10 1.7 10 9I18027 EPA 8260D 09/18/19 18:34 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Dibromomethane [74-95-3]^ 2.7 UD ug/L 10 2.7 10 9I18027 EPA 8260D 09/18/19 18:34 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Ethylbenzene [100-41-4]^ 1.3 UD ug/L 10 1.3 10 9I18027 EPA 8260D 09/18/19 18:34 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Iodomethane[74-88-4]^ 17 UD ug/L 10 17 50 9I18027 EPA 8260D 09/18/19 18:34 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 m,p-Xylenes [108-38-3/106-42-3]^ 1.7 UD ug/L 10 1.7 20 9I18027 EPA 8260D 09/18/19 18:34 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Methylene chloride [75-09-2]^ 2.3 UD ug/L 10 2.3 10 9I18027 EPA 8260D 09/18/19 18:34 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 o-Xylene [95-47-6]^ 0.65 UD ug/L 10 0.65 10 9I18027 EPA 8260D 09/18/19 18:34 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Styrene [100-42-5]^ 1.1 UD ug/L 10 1.1 10 9I18027 EPA 8260D 09/18/19 18:34 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Tetrachloroethene [127-18-4]^ 1.7 UD ug/L 10 1.7 10 9I18027 EPA 8260D 09/18/19 18:34 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Toluene [108-88-3]^ 1.4 UD ug/L 10 1.4 10 9I18027 EPA 8260D 09/18/19 18:34 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 trans-1,2-Dichloroethene [156-60-5]^ 2.1 UD ug/L 10 2.1 10 9I18027 EPA 8260D 09/18/19 18:34 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 trans-1,3-Dichloropropene [10061-02-6]^ 1.5 UD ug/L 10 1.5 10 9I18027 EPA 8260D 09/18/19 18:34 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 trans-1,4-Dichloro-2-butene [110-57-6]^ 7.0 UD ug/L 10 7.0 10 9I18027 EPA 8260D 09/18/19 18:34 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Trichloroethene [79-01-6]^ 1.5 UD ug/L 10 1.5 10 9I18027 EPA 8260D 09/18/19 18:34 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Trichlorofluoromethane [75-69-4]^ 2.4 UD ug/L 10 2.4 10 9I18027 EPA 8260D 09/18/19 18:34 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Vinyl acetate [108-05-4]^ 9.5 UD ug/L 10 9.5 50 9I18027 EPA 8260D 09/18/19 18:34 REF QV-01 Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01, QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Pag@ 23 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW12D Lab Sample ID:CC14233-07 Received: 09/13/19 12:35 Matrix: Water Sampled:09/12/19 08:45 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 3.2 UD ug/L 10 3.2 10 9I18027 EPA 8260D 09/18/19 18:34 REF Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Xylenes(Total)[1330-20-7]^ 4.5 UD ug/L 10 4.5 30 9I18027 EPA 8260D 09/18/19 18:34 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9315032 EPA 8260D 10/16/19 07:58 REF Q-01 Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes 4-Bromofluorobenzene 47 1 50.0 94 % 53-136 9118027 EPA 8260D 09118119 18:34 REF 4-Bromofluorobenzene 44 1 50.0 87 % 53-136 9715032 EPA 6260D 10116119 07:58 REF Q-01 Dibromofluoromethane 46 1 50.0 92 % 67-129 9116027 EPA 6260D 09118119 1624 REF Dibromofluoromethane 46 1 50.0 93 % 67-129 9715032 EPA 6260D 10116119 07:58 REF Q-01 Toluene-d8 38 1 50.0 75 % 59-134 9116027 EPA 8260D 09118119 1624 REF Toluene-d8 38 1 50.0 75 % 59-134 9715032 EPA 8260D 10116119 07:58 REF Q-01 Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte ICAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 3.7 ug/L 1 1.2 2.0 9I20040 EPA 8260D 09/20/19 16:02 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-& 4.9 1 5.00 98 % 75-125 9120040 EPA 6260D 09120119 16:02 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 24 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW15A Lab Sample ID:CC14233-08 Received: 09/13/19 12:35 Matrix: Water Sampled:09/10/19 13:15 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.85 UD ug/L 5 0.85 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF 1,1,1-Trichloroethane [71-55-6]^ 0.60 UD ug/L 5 0.60 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 1.4 UD ug/L 5 1.4 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF 1,1,2-Trichloroethane [79-00-5]^ 0.70 UD ug/L 5 0.70 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF 1,1-Dichloroethane [75-34-3]1 0.65 UD ug/L 5 0.65 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF 1,1-Dichloroethene [75-35-4]1 1.0 UD ug/L 5 1.0 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF 1,2,3-Trichloropropane [96-18-4]1 1.2 UD ug/L 5 1.2 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 2.4 UD ug/L 5 2.4 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF 1,2-Dibromoethane [106-93-4]1 3.3 UD ug/L 5 3.3 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF 1,2-Dichlorobenzene [95-50-1]^ 0.95 UD ug/L 5 0.95 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF 1,2-Dichloroethane [107-06-2]1 1.0 UD ug/L 5 1.0 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF 1,2-Dichloropropane [78-87-5]1 0.50 UD ug/L 5 0.50 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF 1,4-Dichlorobenzene [106-46-7]1 0.95 UD ug/L 5 0.95 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF 2-Butanone [78-93-3]^ 6.5 UD ug/L 5 6.5 25 9I16024 EPA 8260D 09/17/19 17:12 REF 2-Hexanone [591-78-6]1 4.4 UD ug/L 5 4.4 25 9I16024 EPA 8260D 09/17/19 17:12 REF 4-Methyl-2-pentanone [108-10-1]^ 5.5 UD ug/L 5 5.5 25 9I16024 EPA 8260D 09/17/19 17:12 REF Acetone [67-64-1]^ 50 UD ug/L 5 50 100 9I16024 EPA 8260D 09/17/19 17:12 REF Acrylonitrile [107-13-1]^ 18 UD ug/L 5 18 50 9I16024 EPA 8260D 09/17/19 17:12 REF Benzene [71-43-2]^ 0.75 UD ug/L 5 0.75 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF Bromochloromethane [74-97-5]^ 2.4 UD ug/L 5 2.4 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF Bromodichloromethane [75-27-4]^ 0.85 UD ug/L 5 0.85 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF Bromoform [75-25-2]^ 1.1 UD ug/L 5 1.1 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF Bromomethane [74-83-9]^ 0.70 UD ug/L 5 0.70 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF Carbon disulfide [75-15-0]^ 7.5 UD ug/L 5 7.5 25 9I16024 EPA 8260D 09/17/19 17:12 REF Carbon tetrachloride [56-23-5]^ 0.85 UD ug/L 5 0.85 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF Chlorobenzene [108-90-7]^ 190 D ug/L 5 0.85 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF Chloroethane [75-00-3]^ 1.2 UD ug/L 5 1.2 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF Chloroform [67-66-3]^ 0.90 UD ug/L 5 0.90 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF Chloromethane [74-87-3]^ 0.65 UD ug/L 5 0.65 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF cis- 1,2-Dichloroethene [156-59-2]^ 0.75 UD ug/L 5 0.75 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF cis- 1,3-Dichloropropene [10061-01-5]^ 1.0 UD ug/L 5 1.0 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF Dibromochloromethane [124-48-1]^ 0.85 UD ug/L 5 0.85 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF Dibromomethane [74-95-3]^ 1.4 UD ug/L 5 1.4 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF Ethylbenzene [100-41-4]^ 0.65 UD ug/L 5 0.65 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF Iodomethane [74-88-4]^ 8.5 UD ug/L 5 8.5 25 9I16024 EPA 8260D 09/17/19 17:12 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.85 UD ug/L 5 0.85 10 9I16024 EPA 8260D 09/17/19 17:12 REF Methylene chloride [75-09-2]^ 1.2 UD ug/L 5 1.2 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF o-Xylene [95-47-6]^ 0.32 UD ug/L 5 0.32 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF Styrene [100-42-5]^ 0.55 UD ug/L 5 0.55 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF Tetrachloroethene [127-18-4]^ 0.85 UD ug/L 5 0.85 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF Toluene [108-88-3]^ 0.70 UD ug/L 5 0.70 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF trans-1,2-Dichloroethene [156-60-5]^ 1.0 UD ug/L 5 1.0 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.75 UD ug/L 5 0.75 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 3.5 UD ug/L 5 3.5 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF QV-01 Trichloroethene [79-01-6]^ 0.75 UD ug/L 5 0.75 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF Trichlorofluoromethane [75-69-4]^ 1.2 UD ug/L 5 1.2 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF Vinyl acetate [108-05-4]^ 4.8 UD ug/L 5 4.8 25 9I16024 EPA 8260D 09/17/19 17:12 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 25 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-MW15A Lab Sample ID:CC14233-08 Received: 09/13/19 12:35 Matrix: Water Sampled:09/10/19 13:15 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 1.6 UD ug/L 5 1.6 5.0 9I16024 EPA 8260D 09/17/19 17:12 REF Xylenes(Total)[1330-20-7]^ 2.2 UD ug/L 5 2.2 15 9I16024 EPA 8260D 09/17/19 17:12 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 45 1 50.0 89 % 53-136 9116024 EPA 8260D 09117119 17:12 REF Dlbromofluoromethane 46 1 50.0 92 % 67-129 9116024 EPA 6260D 0911711917:12 REF Toluene-d8 39 1 50.0 77 % 59-134 9116024 EPA 6260D 0911711917:12 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte ICAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1400 D ug/L 100 120 200 9I19040 EPA 8260D 09/19/19 18:27 MJH Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 4.6 1 5.00 92 % 75-125 9119040 EPA 8260D 0911911918:27 MJH FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 26 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-OWDR2 Lab Sample ID:CC14233-09 Received: 09/13/19 12:35 Matrix: Water Sampled:09/11/19 14:45 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.85 UD ug/L 5 0.85 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF 1,1,1-Trichloroethane [71-55-6]^ 12 D ug/L 5 0.60 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 1.4 UD ug/L 5 1.4 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF 1,1,2-Trichloroethane [79-00-5]^ 0.70 UD ug/L 5 0.70 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF 1,1-Dichloroethane [75-34-3]^ 200 D ug/L 5 0.65 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF 1,1-Dichloroethene [75-35-4]^ 84 D ug/L 5 1.0 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF 1,2,3-Trichloropropane [96-18-4]^ 1.2 UD ug/L 5 1.2 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 2.4 UD ug/L 5 2.4 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF 1,2-Dibromoethane [106-93-4]^ 3.3 UD ug/L 5 3.3 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF 1,2-Dichlorobenzene [95-50-1]^ 0.95 UD ug/L 5 0.95 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF 1,2-Dichloroethane [107-06-2]^ 11 D ug/L 5 1.0 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF 1,2-Dichloropropane [78-87-5]^ 0.50 UD ug/L 5 0.50 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF 1,4-Dichlorobenzene [106-46-7]^ 0.95 UD ug/L 5 0.95 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF 2-Butanone [78-93-3]^ 6.5 UD ug/L 5 6.5 25 9I18027 EPA 8260D 09/18/19 19:05 REF 2-Hexanone [591-78-6]^ 4.4 UD ug/L 5 4.4 25 9I18027 EPA 8260D 09/18/19 19:05 REF 4-Methyl-2-pentanone [108-10-1]^ 5.5 UD ug/L 5 5.5 25 9I18027 EPA 8260D 09/18/19 19:05 REF Acetone [67-64-1]^ 50 UD ug/L 5 50 100 9I18027 EPA 8260D 09/18/19 19:05 REF Acrylonitrile [107-13-1]^ 18 UD ug/L 5 18 50 9I18027 EPA 8260D 09/18/19 19:05 REF Benzene [71-43-2]^ 6.5 D ug/L 5 0.75 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF Bromochloromethane [74-97-5]^ 2.4 UD ug/L 5 2.4 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF Bromodichloromethane [75-27-4]^ 0.85 UD ug/L 5 0.85 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF Bromoform [75-25-2]^ 1.1 UD ug/L 5 1.1 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF Bromomethane [74-83-9]^ 0.70 UD ug/L 5 0.70 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF Carbon disulfide [75-15-0]^ 7.5 UD ug/L 5 7.5 25 9I18027 EPA 8260D 09/18/19 19:05 REF Carbon tetrachloride [56-23-5]^ 0.85 UD ug/L 5 0.85 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF Chlorobenzene [108-90-7]^ 260 D ug/L 5 0.85 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF Chloroethane [75-00-3]^ 12 D ug/L 5 1.2 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF Chloroform [67-66-3]^ 0.90 UD ug/L 5 0.90 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF Chloromethane [74-87-3]^ 0.65 UD ug/L 5 0.65 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF cis- 1,2-Dichloroethene [156-59-2]^ 290 D ug/L 5 0.75 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF cis- 1,3-Dichloropropene [10061-01-5]^ 1.0 UD ug/L 5 1.0 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF Dibromochloromethane [124-48-1]^ 0.85 UD ug/L 5 0.85 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF Dibromomethane [74-95-3]^ 1.4 UD ug/L 5 1.4 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF Ethylbenzene [100-41-4]^ 0.65 UD ug/L 5 0.65 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF Iodomethane [74-88-4]^ 8.5 UD ug/L 5 8.5 25 9I18027 EPA 8260D 09/18/19 19:05 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.85 UD ug/L 5 0.85 10 9I18027 EPA 8260D 09/18/19 19:05 REF Methylene chloride [75-09-2]^ 1.2 UD ug/L 5 1.2 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF o-Xylene [95-47-6]^ 0.32 UD ug/L 5 0.32 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF Styrene [100-42-5]^ 0.55 UD ug/L 5 0.55 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF Tetrachloroethene [127-18-4]^ 0.85 UD ug/L 5 0.85 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF Toluene [108-88-3]^ 0.70 UD ug/L 5 0.70 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF trans-1,2-Dichloroethene [156-60-5]^ 1.0 UD ug/L 5 1.0 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.75 UD ug/L 5 0.75 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 3.5 UD ug/L 5 3.5 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF Trichloroethene [79-01-6]^ 0.75 UD ug/L 5 0.75 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF Trichlorofluoromethane [75-69-4]^ 1.2 UD ug/L 5 1.2 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF Vinyl acetate [108-05-4]^ 4.8 UD ug/L 5 4.8 25 9I18027 EPA 8260D 09/18/19 19:05 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 27 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-OWDR2 Lab Sample ID:CC14233-09 Received: 09/13/19 12:35 Matrix: Water Sampled:09/11/19 14:45 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]^ 52 D ug/L 5 1.6 5.0 9I18027 EPA 8260D 09/18/19 19:05 REF Xylenes(Total)[1330-20-7]^ 2.2 UD ug/L 5 2.2 15 9I18027 EPA 8260D 09/18/19 19:05 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 45 1 50.0 91 % 53-136 9118027 EPA 8260D 09118119 19:05 REF Dlbromofluoromethane 46 1 50.0 91 % 67-129 9116027 EPA 6260D 09118119 19:05 REF Toluene-d8 38 1 50.0 76 % 59-134 9118027 EPA 6260D 09118119 19:05 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte fCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 250 D ug/L 5 6.0 10 9I20040 EPA 8260D 09/20/19 12:23 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 4.8 1 5.00 96 % 75-125 9120040 EPA 8260D 0912011912:23 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 28 Of 74 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-OWLFS2 Lab Sample ID:CC14233-10 Received: 09/13/19 12:35 Matrix: Water Sampled:09/12/19 08:30 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF 1,1-Dichloroethane [75-34-3]A 0.80 1 ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I18027 EPA 8260D 09/18/19 19:36 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 9I18027 EPA 8260D 09/18/19 19:36 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I18027 EPA 8260D 09/18/19 19:36 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I18027 EPA 8260D 09/18/19 19:36 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I18027 EPA 8260D 09/18/19 19:36 REF Benzene [71-43-2]A 0.48 J ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I18027 EPA 8260D 09/18/19 19:36 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF Chlorobenzene [108-90-7]A 3.1 ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I18027 EPA 8260D 09/18/19 19:36 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I18027 EPA 8260D 09/18/19 19:36 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I18027 EPA 8260D 09/18/19 19:36 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 29 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-OWLFS2 Lab Sample ID:CC14233-10 Received: 09/13/19 12:35 Matrix: Water Sampled:09/12/19 08:30 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9I18027 EPA 8260D 09/18/19 19:36 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I18027 EPA 8260D 09/18/19 19:36 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 47 1 50.0 95 % 53-136 9118027 EPA 8260D 09118119 19:36 REF Dlbromofluoromethane 46 1 50.0 91 % 67-129 9116027 EPA 6260D 09118119 1926 REF Toluene-d8 38 1 50.0 76 % 59-134 9118027 EPA 6260D 09118119 1936 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte ICAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 210 D ug/L 5 6.0 10 9I20040 EPA 8260D 09/20/19 16:39 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 4.9 1 5.00 97 % 75-125 9120040 EPA 8260D 09120119 1639 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 30 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW3D Lab Sample ID:CC14233-11 Received: 09/13/19 12:35 Matrix: Water Sampled:09/11/19 09:50 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 34 UD ug/L 200 34 200 9I16024 EPA 8260D 09/17/19 18:14 REF 1,1,1-Trichloroethane [71-55-6]^ 860 D ug/L 200 24 200 9I16024 EPA 8260D 09/17/19 18:14 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 56 UD ug/L 200 56 200 9I16024 EPA 8260D 09/17/19 18:14 REF 1,1,2-Trichloroethane [79-00-5]^ 28 UD ug/L 200 28 200 9I16024 EPA 8260D 09/17/19 18:14 REF 1,1-Dichloroethane [75-34-3]^ 480 D ug/L 200 26 200 9I16024 EPA 8260D 09/17/19 18:14 REF 1,1-Dichloroethene [75-35-4]^ 1100 D ug/L 200 42 200 9I16024 EPA 8260D 09/17/19 18:14 REF 1,2,3-Trichloropropane [96-18-4]^ 46 UD ug/L 200 46 200 9I16024 EPA 8260D 09/17/19 18:14 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 96 UD ug/L 200 96 200 9I16024 EPA 8260D 09/17/19 18:14 REF 1,2-Dibromoethane [106-93-4]^ 130 UD ug/L 200 130 200 9I16024 EPA 8260D 09/17/19 18:14 REF 1,2-Dichlorobenzene [95-50-1]^ 38 UD ug/L 200 38 200 9I16024 EPA 8260D 09/17/19 18:14 REF 1,2-Dichloroethane [107-06-2]^ 14000 D ug/L 200 42 200 9I16024 EPA 8260D 09/17/19 18:14 REF 1,2-Dichloropropane [78-87-5]^ 20 UD ug/L 200 20 200 9I16024 EPA 8260D 09/17/19 18:14 REF 1,4-Dichlorobenzene [106-46-7]^ 38 UD ug/L 200 38 200 9I16024 EPA 8260D 09/17/19 18:14 REF 2-Butanone [78-93-3]^ 560 ]D ug/L 200 260 1000 9I16024 EPA 8260D 09/17/19 18:14 REF 2-Hexanone [591-78-6]^ 180 UD ug/L 200 180 1000 9I16024 EPA 8260D 09/17/19 18:14 REF 4-Methyl-2-pentanone [108-10-1]^ 220 ]D ug/L 200 220 1000 9I16024 EPA 8260D 09/17/19 18:14 REF Acetone [67-64-1]^ 2000 UD ug/L 200 2000 4000 9I16024 EPA 8260D 09/17/19 18:14 REF Acrylonitrile [107-13-1]^ 700 UD ug/L 200 700 2000 9I16024 EPA 8260D 09/17/19 18:14 REF Benzene [71-43-2]^ 190 ]D ug/L 200 30 200 9I16024 EPA 8260D 09/17/19 18:14 REF Bromochloromethane [74-97-5]^ 96 UD ug/L 200 96 200 9I16024 EPA 8260D 09/17/19 18:14 REF Bromodichloromethane [75-27-4]^ 34 UD ug/L 200 34 200 9I16024 EPA 8260D 09/17/19 18:14 REF Bromoform [75-25-2]^ 44 UD ug/L 200 44 200 9I16024 EPA 8260D 09/17/19 18:14 REF Bromomethane [74-83-9]^ 28 UD ug/L 200 28 200 9I16024 EPA 8260D 09/17/19 18:14 REF Carbon disulfide [75-15-0]^ 300 UD ug/L 200 300 1000 9I16024 EPA 8260D 09/17/19 18:14 REF Carbon tetrachloride [56-23-5]^ 34 UD ug/L 200 34 200 9I16024 EPA 8260D 09/17/19 18:14 REF Chlorobenzene [308-90-7]^ 11000 D ug/L 200 34 200 9I16024 EPA 8260D 09/17/19 18:14 REF Chloroethane [75-00-3]^ 46 UD ug/L 200 46 200 9I16024 EPA 8260D 09/17/19 18:14 REF Chloroform [67-66-3]^ 36 UD ug/L 200 36 200 9I16024 EPA 8260D 09/17/19 18:14 REF Chloromethane [74-87-3]^ 26 UD ug/L 200 26 200 9I16024 EPA 8260D 09/17/19 18:14 REF cis- 1,2-Dichloroethene [156-59-2]^ 350 D ug/L 200 30 200 9I16024 EPA 8260D 09/17/19 18:14 REF cis- 1,3-Dichloropropene [10061-01-5]^ 40 UD ug/L 200 40 200 9I16024 EPA 8260D 09/17/19 18:14 REF Dibromochloromethane [124-48-1]^ 34 UD ug/L 200 34 200 9I16024 EPA 8260D 09/17/19 18:14 REF Dibromomethane [74-95-3]^ 54 UD ug/L 200 54 200 9I16024 EPA 8260D 09/17/19 18:14 REF Ethylbenzene [100-41-4]^ 26 UD ug/L 200 26 200 9I16024 EPA 8260D 09/17/19 18:14 REF Iodomethane[74-88-4]^ 340 UD ug/L 200 340 1000 9I16024 EPA 8260D 09/17/19 18:14 REF m,p-Xylenes [108-38-3/106-42-3]^ 34 UD ug/L 200 34 400 9I16024 EPA 8260D 09/17/19 18:14 REF Methylene chloride [75-09-2]^ 1300 D ug/L 200 46 200 9I16024 EPA 8260D 09/17/19 18:14 REF o-Xylene [95-47-6]^ 13 UD ug/L 200 13 200 9I16024 EPA 8260D 09/17/19 18:14 REF Styrene [100-42-5]^ 22 UD ug/L 200 22 200 9I16024 EPA 8260D 09/17/19 18:14 REF Tetrachloroethene [127-18-4]^ 620 D ug/L 200 34 200 9I16024 EPA 8260D 09/17/19 18:14 REF Toluene [108-88-3]^ 470 D ug/L 200 28 200 9I16024 EPA 8260D 09/17/19 18:14 REF trans-1,2-Dichloroethene [156-60-5]^ 42 UD ug/L 200 42 200 9I16024 EPA 8260D 09/17/19 18:14 REF trans-1,3-Dichloropropene [10061-02-6]^ 30 UD ug/L 200 30 200 9I16024 EPA 8260D 09/17/19 18:14 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 140 UD ug/L 200 140 200 9I16024 EPA 8260D 09/17/19 18:14 REF QV-01 Trichloroethene [79-01-6]^ 30 UD ug/L 200 30 200 9I16024 EPA 8260D 09/17/19 18:14 REF Trichlorofluoromethane [75-69-4]^ 48 UD ug/L 200 48 200 9I16024 EPA 8260D 09/17/19 18:14 REF Vinyl acetate [108-05-4]^ 190 UD ug/L 200 190 1000 9I16024 EPA 8260D 09/17/19 18:14 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 31 of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW3D Lab Sample ID:CC14233-11 Received: 09/13/19 12:35 Matrix: Water Sampled:09/11/19 09:50 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 64 UD ug/L 200 64 200 9I16024 EPA 8260D 09/17/19 18:14 REF Xylenes(Total)[1330-20-7]^ 90 UD ug/L 200 90 600 9I16024 EPA 8260D 09/17/19 18:14 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 46 1 50.0 92 % 53-136 9116024 EPA 8260D 09117119 16:14 REF Dlbromofluoromethane 46 1 50.0 92 % 67-129 9116024 EPA 6260D 0911711916:14 REF Toluene-d8 39 1 50.0 77 % 59-134 9116024 EPA 6260D 0911711918:14 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte ICAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 140 D ug/L 5 6.0 10 9I19040 EPA 8260D 09/19/19 19:42 MJH Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 4.7 1 5.00 94 % 75-125 9119040 EPA 8260D 0911911919:42 MJH FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 32 of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW4I Lab Sample ID:CC14233-12 Received: 09/13/19 12:35 Matrix: Water Sampled:09/11/19 10:00 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.85 UD ug/L 5 0.85 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF 1,1,1-Trichloroethane [71-55-6]^ 32 D ug/L 5 0.60 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 1.4 UD ug/L 5 1.4 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF 1,1,2-Trichloroethane [79-00-5]^ 0.70 UD ug/L 5 0.70 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF 1,1-Dichloroethane [75-34-3]^ 69 D ug/L 5 0.65 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF 1,1-Dichloroethene [75-35-4]^ 37 D ug/L 5 1.0 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF 1,2,3-Trichloropropane [96-18-4]^ 1.2 UD ug/L 5 1.2 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 2.4 UD ug/L 5 2.4 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF 1,2-Dibromoethane [106-93-4]^ 3.3 UD ug/L 5 3.3 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF 1,2-Dichlorobenzene [95-50-1]^ 0.95 UD ug/L 5 0.95 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF 1,2-Dichloroethane [107-06-2]^ 36 D ug/L 5 1.0 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF 1,2-Dichloropropane [78-87-5]^ 0.50 UD ug/L 5 0.50 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF 1,4-Dichlorobenzene [106-46-7]^ 0.95 UD ug/L 5 0.95 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF 2-Butanone [78-93-3]^ 6.5 UD ug/L 5 6.5 25 9I18027 EPA 8260D 09/18/19 20:07 REF 2-Hexanone [591-78-6]^ 4.4 UD ug/L 5 4.4 25 9I18027 EPA 8260D 09/18/19 20:07 REF 4-Methyl-2-pentanone [108-10-1]^ 5.5 UD ug/L 5 5.5 25 9I18027 EPA 8260D 09/18/19 20:07 REF Acetone [67-64-1]^ 50 UD ug/L 5 50 100 9I18027 EPA 8260D 09/18/19 20:07 REF Acrylonitrile [107-13-1]^ 18 UD ug/L 5 18 50 9I18027 EPA 8260D 09/18/19 20:07 REF Benzene [71-43-2]^ 0.75 UD ug/L 5 0.75 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF Bromochloromethane [74-97-5]^ 2.4 UD ug/L 5 2.4 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF Bromodichloromethane [75-27-4]^ 0.85 UD ug/L 5 0.85 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF Bromoform [75-25-2]^ 1.1 UD ug/L 5 1.1 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF Bromomethane [74-83-9]^ 0.70 UD ug/L 5 0.70 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF Carbon disulfide [75-15-0]^ 7.5 UD ug/L 5 7.5 25 9I18027 EPA 8260D 09/18/19 20:07 REF Carbon tetrachloride [56-23-5]^ 0.85 UD ug/L 5 0.85 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF Chlorobenzene [108-90-7]^ 60 D ug/L 5 0.85 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF Chloroethane [75-00-3]^ 1.2 UD ug/L 5 1.2 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF Chloroform [67-66-3]^ 0.90 UD ug/L 5 0.90 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF Chloromethane [74-87-3]^ 0.65 UD ug/L 5 0.65 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF cis- 1,2-Dichloroethene [156-59-2]^ 230 D ug/L 5 0.75 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF cis- 1,3-Dichloropropene [10061-01-5]^ 1.0 UD ug/L 5 1.0 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF Dibromochloromethane [124-48-1]^ 0.85 UD ug/L 5 0.85 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF Dibromomethane [74-95-3]^ 1.4 UD ug/L 5 1.4 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF Ethylbenzene [100-41-4]^ 0.65 UD ug/L 5 0.65 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF Iodomethane [74-88-4]^ 8.5 UD ug/L 5 8.5 25 9I18027 EPA 8260D 09/18/19 20:07 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.85 UD ug/L 5 0.85 10 9I18027 EPA 8260D 09/18/19 20:07 REF Methylene chloride [75-09-2]^ 1.2 UD ug/L 5 1.2 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF o-Xylene [95-47-6]^ 0.32 UD ug/L 5 0.32 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF Styrene [100-42-5]^ 0.55 UD ug/L 5 0.55 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF Tetrachloroethene [127-18-4]^ 13 D ug/L 5 0.85 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF Toluene [108-88-3]^ 0.70 UD ug/L 5 0.70 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF trans-1,2-Dichloroethene [156-60-5]^ 1.0 UD ug/L 5 1.0 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.75 UD ug/L 5 0.75 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 3.5 UD ug/L 5 3.5 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF Trichloroethene [79-01-6]^ 0.75 UD ug/L 5 0.75 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF Trichlorofluoromethane [75-69-4]^ 1.2 UD ug/L 5 1.2 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF Vinyl acetate [108-05-4]^ 4.8 UD ug/L 5 4.8 25 9I18027 EPA 8260D 09/18/19 20:07 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 33 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW4I Lab Sample ID:CC14233-12 Received: 09/13/19 12:35 Matrix: Water Sampled:09/11/19 10:00 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]^ 43 D ug/L 5 1.6 5.0 9I18027 EPA 8260D 09/18/19 20:07 REF Xylenes(Total)[1330-20-7]^ 2.2 UD ug/L 5 2.2 15 9I18027 EPA 8260D 09/18/19 20:07 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 46 1 50.0 92 % 53-136 9118027 EPA 8260D 09118119 20:07 REF Dlbromofluoromethane 47 1 50.0 94 % 67-129 9116027 EPA 6260D 09118119 20:07 REF Toluene-d8 39 1 50.0 77 % 59-134 9118027 EPA 6260D 09118119 20:07 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 200 D ug/L 5 6.0 10 9I20040 EPA 8260D 09/20/19 17:16 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 5.1 1 5.00 102 % 75-125 9120040 EPA 8260D 09120119 17:16 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 34 of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW5D Lab Sample ID:CC14233-13 Received: 09/13/19 12:35 Matrix: Water Sampled:09/11/19 15:00 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.85 UD ug/L 5 0.85 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF 1,1,1-Trichloroethane [71-55-6]^ 6.5 D ug/L 5 0.60 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 1.4 UD ug/L 5 1.4 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF 1,1,2-Trichloroethane [79-00-5]^ 0.70 UD ug/L 5 0.70 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF 1,1-Dichloroethane [75-34-3]^ 170 D ug/L 5 0.65 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF 1,1-Dichloroethene [75-35-4]^ 55 D ug/L 5 1.0 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF 1,2,3-Trichloropropane [96-18-4]^ 1.2 UD ug/L 5 1.2 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 2.4 UD ug/L 5 2.4 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF 1,2-Dibromoethane [106-93-4]^ 3.3 UD ug/L 5 3.3 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF 1,2-Dichlorobenzene [95-50-1]^ 0.95 UD ug/L 5 0.95 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF 1,2-Dichloroethane [107-06-2]^ 8.0 D ug/L 5 1.0 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF 1,2-Dichloropropane [78-87-5]^ 0.50 UD ug/L 5 0.50 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF 1,4-Dichlorobenzene [106-46-7]^ 0.95 UD ug/L 5 0.95 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF 2-Butanone [78-93-3]^ 6.5 UD ug/L 5 6.5 25 9I20019 EPA 8260D 09/20/19 19:40 REF QV-01 2-Hexanone [591-78-6]^ 4.4 UD ug/L 5 4.4 25 9I20019 EPA 8260D 09/20/19 19:40 REF 4-Methyl-2-pentanone [108-10-1]^ 5.5 UD ug/L 5 5.5 25 9I20019 EPA 8260D 09/20/19 19:40 REF QV-01 Acetone [67-64-1]^ 50 UD ug/L 5 50 100 9I20019 EPA 8260D 09/20/19 19:40 REF QV-01 Acrylonitrile [107-13-1]^ 18 UD ug/L 5 18 50 9I20019 EPA 8260D 09/20/19 19:40 REF QV-01 Benzene [71-43-2]^ 4.4 ]D ug/L 5 0.75 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF Bromochloromethane [74-97-5]^ 2.4 UD ug/L 5 2.4 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF Bromodichloromethane [75-27-4]^ 0.85 UD ug/L 5 0.85 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF Bromoform [75-25-2]^ 1.1 UD ug/L 5 1.1 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF Bromomethane [74-83-9]^ 0.70 UD ug/L 5 0.70 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF QV-01 Carbon disulfide [75-15-0]^ 7.5 UD ug/L 5 7.5 25 9I20019 EPA 8260D 09/20/19 19:40 REF Carbon tetrachloride [56-23-5]^ 0.85 UD ug/L 5 0.85 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF Chlorobenzene [308-90-7]^ 220 D ug/L 5 0.85 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF Chloroethane [75-00-3]^ 1.2 UD ug/L 5 1.2 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF QV-01 Chloroform [67-66-3]^ 0.90 UD ug/L 5 0.90 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF Chloromethane [74-87-3]^ 0.65 UD ug/L 5 0.65 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF cis- 1,2-Dichloroethene [156-59-2]^ 180 D ug/L 5 0.75 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF cis- 1,3-Dichloropropene [10061-01-5]^ 1.0 UD ug/L 5 1.0 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF Dibromochloromethane [124-48-1]^ 0.85 UD ug/L 5 0.85 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF Dibromomethane [74-95-3]^ 1.4 UD ug/L 5 1.4 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF Ethylbenzene [100-41-4]^ 0.65 UD ug/L 5 0.65 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF Iodomethane [74-88-4]^ 8.5 UD ug/L 5 8.5 25 9I20019 EPA 8260D 09/20/19 19:40 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.85 UD ug/L 5 0.85 10 9I20019 EPA 8260D 09/20/19 19:40 REF Methylene chloride [75-09-2]^ 1.2 UD ug/L 5 1.2 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF o-Xylene [95-47-6]^ 0.32 UD ug/L 5 0.32 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF Styrene [100-42-5]^ 0.55 UD ug/L 5 0.55 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF Tetrachloroethene [127-18-4]^ 0.85 UD ug/L 5 0.85 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF Toluene [108-88-3]^ 0.70 UD ug/L 5 0.70 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF trans-1,2-Dichloroethene [156-60-5]^ 1.0 UD ug/L 5 1.0 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.75 UD ug/L 5 0.75 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 3.5 UD ug/L 5 3.5 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF QV-01 Trichloroethene [79-01-6]^ 0.75 UD ug/L 5 0.75 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF Trichlorofluoromethane [75-69-4]^ 1.2 UD ug/L 5 1.2 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF QV-01 Vinyl acetate [108-05-4]^ 4.8 UD ug/L 5 4.8 25 9I20019 EPA 8260D 09/20/19 19:40 REF QL-02, QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 35 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW5D Lab Sample ID:CC14233-13 Received: 09/13/19 12:35 Matrix: Water Sampled:09/11/19 15:00 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]^ 56 D ug/L 5 1.6 5.0 9I20019 EPA 8260D 09/20/19 19:40 REF Xylenes(Total)[1330-20-7]^ 2.2 UD ug/L 5 2.2 15 9I20019 EPA 8260D 09/20/19 19:40 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 46 1 50.0 92 % 53-136 9120019 EPA 8260D 09120119 19:40 REF Dlbromofluoromethane 47 1 50.0 95 % 67-129 9120019 EPA 6260D 09120119 19:40 REF Toluene-d8 38 1 50.0 77 % 59-134 9120019 EPA 6260D 09120119 19:40 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 240 D ug/L 50 60 100 9I20040 EPA 8260D 09/20/19 17:53 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 4.7 1 5.00 94 % 75-125 9120040 EPA 8260D 09120119 17:53 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 36 of 74 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW6I Lab Sample ID:CC14233-14 Received: 09/13/19 12:35 Matrix: Water Sampled:09/12/19 10:45 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF 1,1-Dichloroethane [75-34-3]A 19 ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF 1,1-Dichloroethene [75-35-4]A 1.0 ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF 1,2-Dichloroethane [107-06-2]A 2.9 ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF 1,4-Dichlorobenzene [106-46-7]A 1.8 ug/L 1 0.19 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I18027 EPA 8260D 09/18/19 21:09 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 9I18027 EPA 8260D 09/18/19 21:09 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I18027 EPA 8260D 09/18/19 21:09 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I18027 EPA 8260D 09/18/19 21:09 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I18027 EPA 8260D 09/18/19 21:09 REF Benzene [71-43-2]A 0.74 J ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I18027 EPA 8260D 09/18/19 21:09 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF Chlorobenzene [108-90-7]A 13 ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF cis-1,2-Dichloroethene [156-59-2]^ 26 ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I18027 EPA 8260D 09/18/19 21:09 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I18027 EPA 8260D 09/18/19 21:09 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF Tetrachloroethene [127-18-4]A 0.42 J ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I18027 EPA 8260D 09/18/19 21:09 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 37 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW6I Lab Sample ID:CC14233-14 Received: 09/13/19 12:35 Matrix: Water Sampled:09/12/19 10:45 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]^ 5.3 ug/L 1 0.32 1.0 9I18027 EPA 8260D 09/18/19 21:09 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I18027 EPA 8260D 09/18/19 21:09 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 46 1 50.0 92 % 53-136 9118027 EPA 8260D 09118119 21:09 REF Dlbromofluoromethane 46 1 50.0 93 % 67-129 9116027 EPA 6260D 09118119 21:09 REF Toluene-d8 39 1 50.0 77 % 59-134 9118027 EPA 6260D 09118119 21:09 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 79 ug/L 1 1.2 2.0 9I20043 EPA 8260D 09/21/19 00:35 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 5.6 1 5.00 111 % 75-125 9120043 EPA 8260D 09121119 0035 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 38 of 74 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW6D Lab Sample ID:CC14233-15 Received: 09/13/19 12:35 Matrix: Water Sampled:09/12/19 10:00 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF 1,1,1-Trichloroethane [71-55-6]A 4.5 ug/L 1 0.12 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF 1,1-Dichloroethane [75-34-3]A 120 ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF 1,1-Dichloroethene [75-35-4]A 42 ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF 1,2-Dichloroethane [107-06-2]A 4.7 ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I18027 EPA 8260D 09/18/19 21:40 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 9I18027 EPA 8260D 09/18/19 21:40 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I18027 EPA 8260D 09/18/19 21:40 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I18027 EPA 8260D 09/18/19 21:40 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I18027 EPA 8260D 09/18/19 21:40 REF Benzene [71-43-2]A 1.4 ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I18027 EPA 8260D 09/18/19 21:40 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF Chlorobenzene [108-90-7]^ 120 ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF Chloroethane [75-00-3]^ 7.0 ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF cis-1,2-Dichloroethene [156-59-2]^ 150 ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I18027 EPA 8260D 09/18/19 21:40 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I18027 EPA 8260D 09/18/19 21:40 REF Methylene chloride [75-09-2]A 0.84 J ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF Tetrachloroethene [127-18-4]A 0.84 J ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF trans-1,2-Dichloroethene [156-60-5]A 1.6 ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I18027 EPA 8260D 09/18/19 21:40 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 39 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW6D Lab Sample ID:CC14233-15 Received: 09/13/19 12:35 Matrix: Water Sampled:09/12/19 10:00 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]^ 25 ug/L 1 0.32 1.0 9I18027 EPA 8260D 09/18/19 21:40 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I18027 EPA 8260D 09/18/19 21:40 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 45 1 50.0 90 % 53-136 9118027 EPA 8260D 09118119 21:40 REF Dlbromofluoromethane 46 1 50.0 93 % 67-129 9116027 EPA 6260D 09118119 21:40 REF Toluene-d8 38 1 50.0 76 % 59-134 9118027 EPA 6260D 09118119 21:40 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 100 D ug/L 5 6.0 10 9I23034 EPA 8260D 09/23/19 13:02 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 5.2 1 5.00 103 % 75-125 9123034 EPA 8260D 0912311913:02 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 40 of 74 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW10I Lab Sample ID:CC14233-16 Received: 09/13/19 12:35 Matrix: Water Sampled:09/12/19 11:30 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF 1,1-Dichloroethane [75-34-3]A 12 ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF 1,4-Dichlorobenzene [106-46-7]A 2.4 ug/L 1 0.19 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I18027 EPA 8260D 09/18/19 22:11 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 9I18027 EPA 8260D 09/18/19 22:11 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I18027 EPA 8260D 09/18/19 22:11 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I18027 EPA 8260D 09/18/19 22:11 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I18027 EPA 8260D 09/18/19 22:11 REF Benzene [71-43-2]A 1.0 ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I18027 EPA 8260D 09/18/19 22:11 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF Chlorobenzene [108-90-7]^ 2.6 ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF Chloroethane [75-00-3]^ 5.9 ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF cis-1,2-Dichloroethene [156-59-2]^ 4.2 ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I18027 EPA 8260D 09/18/19 22:11 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I18027 EPA 8260D 09/18/19 22:11 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I18027 EPA 8260D 09/18/19 22:11 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 41 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW10I Lab Sample ID:CC14233-16 Received: 09/13/19 12:35 Matrix: Water Sampled:09/12/19 11:30 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]^ 3.7 ug/L 1 0.32 1.0 9I18027 EPA 8260D 09/18/19 22:11 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I18027 EPA 8260D 09/18/19 22:11 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 46 1 50.0 93 % 53-136 9118027 EPA 8260D 09118119 22:11 REF Dlbromofluoromethane 47 1 50.0 93 % 67-129 9116027 EPA 6260D 09118119 22:11 REF Toluene-d8 38 1 50.0 76 % 59-134 9118027 EPA 6260D 09118119 22:11 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 260 D ug/L 5 6.0 10 9I20040 EPA 8260D 09/20/19 18:29 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 5.1 1 5.00 101 % 75-125 9120040 EPA 8260D 09120119 18:29 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 42 of 74 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW10D Lab Sample ID:CC14233-17 Received: 09/13/19 12:35 Matrix: Water Sampled:09/12/19 10:00 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I18027 EPA 8260D 09/18/19 22:43 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 9I18027 EPA 8260D 09/18/19 22:43 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I18027 EPA 8260D 09/18/19 22:43 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I18027 EPA 8260D 09/18/19 22:43 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I18027 EPA 8260D 09/18/19 22:43 REF Benzene[71-43-2]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I18027 EPA 8260D 09/18/19 22:43 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I18027 EPA 8260D 09/18/19 22:43 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I18027 EPA 8260D 09/18/19 22:43 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I18027 EPA 8260D 09/18/19 22:43 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 43 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW10D Lab Sample ID:CC14233-17 Received: 09/13/19 12:35 Matrix: Water Sampled:09/12/19 10:00 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9I18027 EPA 8260D 09/18/19 22:43 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I18027 EPA 8260D 09/18/19 22:43 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 45 1 50.0 90 % 53-136 9118027 EPA 8260D 09118119 22:43 REF Dlbromofluoromethane 48 1 50.0 95 % 67-129 9116027 EPA 6260D 09118119 22:43 REF Toluene-d8 39 1 50.0 77 % 59-134 9118027 EPA 6260D 09118119 22:43 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.2 U ug/L 1 1.2 2.0 9I20043 EPA 8260D 09/21/19 01:49 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-& 4.9 1 5.00 98 % 75-125 9120043 EPA 8260D 09121119 01:49 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 44 of 74 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW12I Lab Sample ID:CC14233-18 Received: 09/13/19 12:35 Matrix: Water Sampled:09/11/19 11:30 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I18027 EPA 8260D 09/18/19 23:14 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 9I18027 EPA 8260D 09/18/19 23:14 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I18027 EPA 8260D 09/18/19 23:14 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I18027 EPA 8260D 09/18/19 23:14 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I18027 EPA 8260D 09/18/19 23:14 REF Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I18027 EPA 8260D 09/18/19 23:14 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I18027 EPA 8260D 09/18/19 23:14 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I18027 EPA 8260D 09/18/19 23:14 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I18027 EPA 8260D 09/18/19 23:14 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 45 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW12I Lab Sample ID:CC14233-18 Received: 09/13/19 12:35 Matrix: Water Sampled:09/11/19 11:30 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9I18027 EPA 8260D 09/18/19 23:14 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I18027 EPA 8260D 09/18/19 23:14 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 46 1 50.0 91 % 53-136 9118027 EPA 8260D 09118119 23:14 REF Dlbromofluoromethane 48 1 50.0 95 % 67-129 9116027 EPA 6260D 09118119 23:14 REF Toluene-d8 38 1 50.0 77 % 59-134 9118027 EPA 6260D 09118119 23:14 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte ICAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.2 1 ug/L 1 1.2 2.0 9I20040 EPA 8260D 09/20/19 19:05 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 5.1 1 5.00 101 % 75-125 9120040 EPA 8260D 09120119 19:05 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 46 of 74 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW13I Lab Sample ID:CC14233-19 Received: 09/13/19 12:35 Matrix: Water Sampled:09/11/19 11:45 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF 1,1-Dichloroethane [75-34-3]A 94 ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF 1,1-Dichloroethene [75-35-4]A 18 ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF 1,2-Dichloroethane [107-06-2]A 3.6 ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I18027 EPA 8260D 09/18/19 23:45 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 9I18027 EPA 8260D 09/18/19 23:45 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I18027 EPA 8260D 09/18/19 23:45 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I18027 EPA 8260D 09/18/19 23:45 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I18027 EPA 8260D 09/18/19 23:45 REF Benzene [71-43-2]A 2.4 ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I18027 EPA 8260D 09/18/19 23:45 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF Chlorobenzene [108-90-7]^ 8.9 ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF Chloroethane [75-00-3]^ 1.4 ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF cis-1,2-Dichloroethene [156-59-2]^ 72 ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I18027 EPA 8260D 09/18/19 23:45 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I18027 EPA 8260D 09/18/19 23:45 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF Tetrachloroethene [127-18-4]A 0.72 J ug/L 1 0.17 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF trans-1,2-Dichloroethene [156-60-5]A 0.44 J ug/L 1 0.21 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I18027 EPA 8260D 09/18/19 23:45 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 47 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PW13I Lab Sample ID:CC14233-19 Received: 09/13/19 12:35 Matrix: Water Sampled:09/11/19 11:45 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]^ 38 ug/L 1 0.32 1.0 9I18027 EPA 8260D 09/18/19 23:45 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I18027 EPA 8260D 09/18/19 23:45 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 46 1 50.0 92 % 53-136 9118027 EPA 8260D 09118119 23:45 REF Dlbromofluoromethane 46 1 50.0 93 % 67-129 9116027 EPA 6260D 09118119 23:45 REF Toluene-d8 38 1 50.0 75 % 59-134 9118027 EPA 6260D 09118119 23:45 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 44 ug/L 1 1.2 2.0 9I20040 EPA 8260D 09/20/19 19:41 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 5.1 1 5.00 102 % 75-125 9120040 EPA 8260D 09120119 19:41 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 48 of 74 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-W4A Lab Sample ID:CC14233-20 Received: 09/13/19 12:35 Matrix: Water Sampled:09/11/19 09:30 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]A 34 UD ug/L 200 34 200 9I18027 EPA 8260D 09/19/19 00:16 REF 1,1,1,2-Tetrachloroethane [630-20-6]A 0.17 U ug/L 1 0.17 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 1,1,1-Trichloroethane [71-55-6]A 24 UD ug/L 200 24 200 9I18027 EPA 8260D 09/19/19 00:16 REF 1,1,1-Trichloroethane [71-55-6]A 12 ug/L 1 0.12 1.0 9116023 EPA 8260D 10/16/19 17:16 REF Q-01 1,1,2,2-Tetrachloroethane [79-34-5]A 56 UD ug/L 200 56 200 9I18027 EPA 8260D 09/19/19 00:16 REF 1,1,2,2-Tetrachloroethane [79-34-5]A 0.28 U ug/L 1 0.28 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 1,1,2-Trichloroethane [79-00-5]A 28 UD ug/L 200 28 200 9I18027 EPA 8260D 09/19/19 00:16 REF 1,1,2-Trichloroethane [79-00-5]A 0.14 U ug/L 1 0.14 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 1,1-Dichloroethane [75-34-3]A 26 UD ug/L 200 26 200 9I18027 EPA 8260D 09/19/19 00:16 REF 1,1-Dichloroethane [75-34-3]A 83 ug/L 1 0.13 1.0 9116023 EPA 8260D 10/16/19 17:16 REF Q-01 1,1-Dichloroethene [75-35-4]A 42 UD ug/L 200 42 200 9I18027 EPA 8260D 09/19/19 00:16 REF 1,1-Dichloroethene [75-35-4]A 33 ug/L 1 0.21 1.0 9116023 EPA 8260D 10/16/19 17:16 REF Q-01 1,2,3-Trichloropropane [96-18-4]A 46 UD ug/L 200 46 200 9I18027 EPA 8260D 09/19/19 00:16 REF 1,2,3-Trichloropropane [96-18-4]A 0.23 U ug/L 1 0.23 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 1,2-Dibromo-3-chloropropane [96-12-8]A 96 UD ug/L 200 96 200 9I18027 EPA 8260D 09/19/19 00:16 REF 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 1,2-Dibromoethane[106-93-4]A 130 UD ug/L 200 130 200 9I18027 EPA 8260D 09/19/19 00:16 REF 1,2-Dibromoethane [106-93-4]A 0.66 U ug/L 1 0.66 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 1,2-Dichlorobenzene [95-50-1]A 38 UD ug/L 200 38 200 9I18027 EPA 8260D 09/19/19 00:16 REF 1,2-Dichlorobenzene [95-50-1]A 0.19 U ug/L 1 0.19 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 1,2-Dichloroethane [107-06-2]A 42 UD ug/L 200 42 200 9I18027 EPA 8260D 09/19/19 00:16 REF 1,2-Dichloroethane [107-06-2]A 2.8 ug/L 1 0.21 1.0 9116023 EPA 8260D 10/16/19 17:16 REF Q-01 1,2-Dichloropropane [78-87-5]A 20 UD ug/L 200 20 200 9I18027 EPA 8260D 09/19/19 00:16 REF 1,2-Dichloropropane [78-87-5]A 0.10 U ug/L 1 0.10 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 1,4-Dichlorobenzene [106-46-7]A 38 UD ug/L 200 38 200 9I18027 EPA 8260D 09/19/19 00:16 REF 1,4-Dichlorobenzene [106-46-7]A 0.19 U ug/L 1 0.19 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 2-Butanone [78-93-3]A 260 UD ug/L 200 260 1000 9I18027 EPA 8260D 09/19/19 00:16 REF 2-Butanone [78-93-3]A 1.3 U ug/L 1 1.3 5.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 2-Hexanone [591-78-6]A 180 UD ug/L 200 180 1000 9I18027 EPA 8260D 09/19/19 00:16 REF 2-Hexanone [591-78-6]A 0.88 U ug/L 1 0.88 5.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 4-Methyl-2-pentanone [108-10-1]A 220 UD ug/L 200 220 1000 9I18027 EPA 8260D 09/19/19 00:16 REF 4-Methyl-2-pentanone [108-10-1]A 1.1 U ug/L 1 1.1 5.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 Acetone [67-64-1]A 2000 UD ug/L 200 2000 4000 9I18027 EPA 8260D 09/19/19 00:16 REF Acetone [67-64-1]A 10 U ug/L 1 10 20 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 Acrylonitrile [107-13-1]A 700 UD ug/L 200 700 2000 9I18027 EPA 8260D 09/19/19 00:16 REF Acrylonitrile [107-13-1]A 3.5 U ug/L 1 3.5 10 9316023 EPA 8260D 10/16/19 17:16 REF QV-01, Q-01 Benzene[71-43-2]A 30 UD ug/L 200 30 200 9I18027 EPA 8260D 09/19/19 00:16 REF Benzene [71-43-2]A 7.5 ug/L 1 0.15 1.0 9116023 EPA 8260D 10/16/19 17:16 REF Q-01 Bromochloromethane [74-97-5]A 96 UD ug/L 200 96 200 9I18027 EPA 8260D 09/19/19 00:16 REF Bromochloromethane [74-97-5]A 0.48 U ug/L 1 0.48 1.0 9116023 EPA 8260D 10/16/19 17:16 REF Q-01 Bromodichloromethane [75-27-4]A 34 UD ug/L 200 34 200 9I18027 EPA 8260D 09/19/19 00:16 REF Bromodichloromethane [75-27-4]A 0.17 U ug/L 1 0.17 1.0 9116023 EPA 8260D 10/16/19 17:16 REF Q-01 Bromoform [75-25-2]A 44 UD ug/L 200 44 200 9I18027 EPA 8260D 09/19/19 00:16 REF Bromoform [75-25-2]A 0.22 U ug/L 1 0.22 1.0 9116023 EPA 8260D 10/16/19 17:16 REF Q-01 Bromomethane[74-83-9]A 28 UD ug/L 200 28 200 9I18027 EPA 8260D 09/19/19 00:16 REF Bromomethane [74-83-9]A 0.14 U ug/L 1 0.14 1.0 9116023 EPA 8260D 10/16/19 17:16 REF Q-01 Carbon disulfide [75-15-0]A 300 UD ug/L 200 300 1000 9I18027 EPA 8260D 09/19/19 00:16 REF FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 49 Of 74 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-W4A Lab Sample ID:CC14233-20 Received: 09/13/19 12:35 Matrix: Water Sampled:09/11/19 09:30 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 Carbon tetrachloride [56-23-5]^ 34 UD ug/L 200 34 200 9I18027 EPA 8260D 09/19/19 00:16 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 Chlorobenzene[108-90-7]^ 34 UD ug/L 200 34 200 9I18027 EPA 8260D 09/19/19 00:16 REF Chlorobenzene [108-90-7]^ 4.4 ug/L 1 0.17 1.0 9116023 EPA 8260D 10/16/19 17:16 REF Q-01 Chloroethane [75-00-3]^ 46 UD ug/L 200 46 200 9I18027 EPA 8260D 09/19/19 00:16 REF Chloroethane [75-00-3]^ 13 ug/L 1 0.23 1.0 9116023 EPA 8260D 10/16/19 17:16 REF Q-01 Chloroform [67-66-3]^ 36 UD ug/L 200 36 200 9I18027 EPA 8260D 09/19/19 00:16 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 Chloromethane [74-87-3]^ 26 UD ug/L 200 26 200 9I18027 EPA 8260D 09/19/19 00:16 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 cis-1,2-Dichloroethene [156-59-2]^ 30 UD ug/L 200 30 200 9I18027 EPA 8260D 09/19/19 00:16 REF cis-1,2-Dichloroethene [156-59-2]^ 130 ug/L 1 0.15 1.0 9116023 EPA 8260D 10/16/19 17:16 REF Q-01 cis-1,3-Dichloropropene [10061-01-5]^ 40 UD ug/L 200 40 200 9I18027 EPA 8260D 09/19/19 00:16 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 Dibromochloromethane [124-48-1]^ 34 UD ug/L 200 34 200 9I18027 EPA 8260D 09/19/19 00:16 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 Dibromomethane [74-95-3]^ 54 UD ug/L 200 54 200 9I18027 EPA 8260D 09/19/19 00:16 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 Ethylbenzene[100-41-4]^ 26 UD ug/L 200 26 200 9I18027 EPA 8260D 09/19/19 00:16 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 Iodomethane[74-88-4]^ 340 UD ug/L 200 340 1000 9I18027 EPA 8260D 09/19/19 00:16 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 m,p-Xylenes[108-38-3/106-42-3]^ 34 UD ug/L 200 34 400 9I18027 EPA 8260D 09/19/19 00:16 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 Methylene chloride [75-09-2]^ 46 UD ug/L 200 46 200 9I18027 EPA 8260D 09/19/19 00:16 REF Methylene chloride [75-09-2]^ 0.45 1 ug/L 1 0.23 1.0 9116023 EPA 8260D 10/16/19 17:16 REF Q-01 o-Xylene [95-47-6]^ 13 UD ug/L 200 13 200 9I18027 EPA 8260D 09/19/19 00:16 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 Styrene[100-42-5]^ 22 UD ug/L 200 22 200 9I18027 EPA 8260D 09/19/19 00:16 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 Tetrachloroethene [127-18-4]^ 34 UD ug/L 200 34 200 9I18027 EPA 8260D 09/19/19 00:16 REF Tetrachloroethene [127-18-4]^ 0.81 1 ug/L 1 0.17 1.0 9116023 EPA 8260D 10/16/19 17:16 REF Q-01 Toluene [108-88-3]^ 28 UD ug/L 200 28 200 9I18027 EPA 8260D 09/19/19 00:16 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 trans-1,2-Dichloroethene [156-60-5]^ 42 UD ug/L 200 42 200 9I18027 EPA 8260D 09/19/19 00:16 REF trans-1,2-Dichloroethene [156-60-5]^ 1.3 ug/L 1 0.21 1.0 9116023 EPA 8260D 10/16/19 17:16 REF Q-01 trans-1,3-Dichloropropene [10061-02-6]^ 30 UD ug/L 200 30 200 9I18027 EPA 8260D 09/19/19 00:16 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 trans-1,4-Dichloro-2-butene [110-57-6]^ 140 UD ug/L 200 140 200 9I18027 EPA 8260D 09/19/19 00:16 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 Trichloroethene [79-01-6]^ 30 UD ug/L 200 30 200 9I18027 EPA 8260D 09/19/19 00:16 REF Trichloroethene [79-01-6]^ 6.0 ug/L 1 0.15 1.0 9116023 EPA 8260D 10/16/19 17:16 REF Q-01 Trichlorofluoromethane [75-69-4]^ 48 UD ug/L 200 48 200 9I18027 EPA 8260D 09/19/19 00:16 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 Vinyl acetate [108-05-4]^ 190 UD ug/L 200 190 1000 9I18027 EPA 8260D 09/19/19 00:16 REF QV-01 Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9316023 EPA 8260D 10/16/19 17:16 REF QV-01, Q-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Pag@ 50 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-W4A Lab Sample ID:CC14233-20 Received: 09/13/19 12:35 Matrix: Water Sampled:09/11/19 09:30 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 64 UD ug/L 200 64 200 9I18027 EPA 8260D 09/19/19 00:16 REF Vinyl chloride [75-01-4]^ 88 ug/L 1 0.32 1.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 Xylenes(Total)[1330-20-7]^ 90 UD ug/L 200 90 600 9I18027 EPA 8260D 09/19/19 00:16 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9316023 EPA 8260D 10/16/19 17:16 REF Q-01 Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 47 1 50.0 94 % 53-136 9118027 EPA 8260D 09119119 00:16 REF 4-Bromofluorobenzene 44 1 50.0 87 % 53-136 9716023 EPA 6260D 10116119 17:16 REF Q-01 Dibromofluoromethane 47 1 50.0 94 % 67-129 9116027 EPA 6260D 09119119 00:16 REF Dibromofluoromethane 47 1 50.0 94 % 67-129 9716023 EPA 6260D 10116119 17:16 REF Q-01 Toluene-d8 38 1 50.0 75 % 59-134 9116027 EPA 8260D 09119119 00:16 REF Toluene-d8 37 1 50.0 75 % 59-134 9716023 EPA 8260D 10116119 17:16 REF Q-01 Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte ICAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 54 D ug/L 5 6.0 10 9I23034 EPA 8260D 09/23/19 13:37 KKW Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-& 4.9 1 5.00 98 % 75-125 9123034 EPA 6260D 091231191337 KKW FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 51 of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PWSF1 Lab Sample ID:CC14233-21 Received: 09/13/19 12:35 Matrix: Water Sampled:09/10/19 13:30 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte ICAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 34 UD ug/L 200 34 200 9I20024 EPA 8260D 09/24/19 19:09 REF 1,1,1-Trichloroethane [71-55-6]A 3100 D ug/L 200 24 200 9I20024 EPA 8260D 09/24/19 19:09 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 56 UD ug/L 200 56 200 9I20024 EPA 8260D 09/24/19 19:09 REF 1,1,2-Trichloroethane [79-00-5]^ 28 UD ug/L 200 28 200 9I20024 EPA 8260D 09/24/19 19:09 REF 1,1-Dichloroethane [75-34-3]A 3500 D ug/L 200 26 200 9I20024 EPA 8260D 09/24/19 19:09 REF 1,1-Dichloroethene [75-35-4]A 4100 D ug/L 200 42 200 9I20024 EPA 8260D 09/24/19 19:09 REF 1,2,3-Trichloropropane [96-18-4]^ 46 UD ug/L 200 46 200 9I20024 EPA 8260D 09/24/19 19:09 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 96 UD ug/L 200 96 200 9I20024 EPA 8260D 09/24/19 19:09 REF 1,2-Dibromoethane[106-93-4]^ 130 UD ug/L 200 130 200 9I20024 EPA 8260D 09/24/19 19:09 REF 1,2-Dichlorobenzene [95-50-1]^ 38 UD ug/L 200 38 200 9I20024 EPA 8260D 09/24/19 19:09 REF 1,2-Dichloroethane [107-06-2]A 600 D ug/L 200 42 200 9I20024 EPA 8260D 09/24/19 19:09 REF 1,2-Dichloropropane [78-87-5]^ 20 UD ug/L 200 20 200 9I20024 EPA 8260D 09/24/19 19:09 REF 1,4-Dichlorobenzene [106-46-7]^ 38 UD ug/L 200 38 200 9I20024 EPA 8260D 09/24/19 19:09 REF 2-Butanone [78-93-3]^ 260 UD ug/L 200 260 1000 9I20024 EPA 8260D 09/24/19 19:09 REF 2-Hexanone [591-78-6]^ 180 UD ug/L 200 180 1000 9I20024 EPA 8260D 09/24/19 19:09 REF 4-Methyl-2-pentanone[108-10-1]^ 220 UD ug/L 200 220 1000 9I20024 EPA 8260D 09/24/19 19:09 REF Acetone[67-64-1]^ 2000 UD ug/L 200 2000 4000 9I20024 EPA 8260D 09/24/19 19:09 REF Acrylonitrile [107-13-1]^ 700 UD ug/L 200 700 2000 9I20024 EPA 8260D 09/24/19 19:09 REF Benzene [71-43-2]^ 30 UD ug/L 200 30 200 9I20024 EPA 8260D 09/24/19 19:09 REF Bromochloromethane [74-97-5]^ 96 UD ug/L 200 96 200 9I20024 EPA 8260D 09/24/19 19:09 REF Bromodichloromethane [75-27-4]^ 34 UD ug/L 200 34 200 9I20024 EPA 8260D 09/24/19 19:09 REF Bromoform [75-25-2]^ 44 UD ug/L 200 44 200 9I20024 EPA 8260D 09/24/19 19:09 REF Bromomethane [74-83-9]^ 28 UD ug/L 200 28 200 9I20024 EPA 8260D 09/24/19 19:09 REF Carbon disulfide [75-15-0]^ 300 UD ug/L 200 300 1000 9I20024 EPA 8260D 09/24/19 19:09 REF Carbon tetrachloride [56-23-5]^ 34 UD ug/L 200 34 200 9I20024 EPA 8260D 09/24/19 19:09 REF Chlorobenzene [308-90-7]A 1800 D ug/L 200 34 200 9I20024 EPA 8260D 09/24/19 19:09 REF Chloroethane [75-00-3]^ 46 UD ug/L 200 46 200 9I20024 EPA 8260D 09/24/19 19:09 REF Chloroform [67-66-3]A 120 ]D ug/L 200 36 200 9I20024 EPA 8260D 09/24/19 19:09 REF Chloromethane [74-87-3]^ 26 UD ug/L 200 26 200 9I20024 EPA 8260D 09/24/19 19:09 REF cis- 1,2-Dichloroethene [156-59-2]A 20000 D ug/L 200 30 200 9I20024 EPA 8260D 09/24/19 19:09 REF cis- 1,3-Dichloropropene [10061-01-5]^ 40 UD ug/L 200 40 200 9I20024 EPA 8260D 09/24/19 19:09 REF Dibromochloromethane [124-48-1]^ 34 UD ug/L 200 34 200 9I20024 EPA 8260D 09/24/19 19:09 REF Dibromomethane [74-95-3]^ 54 UD ug/L 200 54 200 9I20024 EPA 8260D 09/24/19 19:09 REF Ethylbenzene [100-41-4]^ 26 UD ug/L 200 26 200 9I20024 EPA 8260D 09/24/19 19:09 REF Iodomethane[74-88-4]^ 340 UD ug/L 200 340 1000 9I20024 EPA 8260D 09/24/19 19:09 REF m,p-Xylenes [108-38-3/106-42-3]^ 34 UD ug/L 200 34 400 9I20024 EPA 8260D 09/24/19 19:09 REF Methylene chloride [75-09-2]A 160 ]D ug/L 200 46 200 9I20024 EPA 8260D 09/24/19 19:09 REF o-Xylene [95-47-6]^ 13 UD ug/L 200 13 200 9I20024 EPA 8260D 09/24/19 19:09 REF Styrene [100-42-5]^ 22 UD ug/L 200 22 200 9I20024 EPA 8260D 09/24/19 19:09 REF Tetrachloroethene [127-18-4]A 830 D ug/L 200 34 200 9I20024 EPA 8260D 09/24/19 19:09 REF Toluene [108-88-3]A 530 D ug/L 200 28 200 9I20024 EPA 8260D 09/24/19 19:09 REF trans-1,2-Dichloroethene [156-60-5]^ 42 UD ug/L 200 42 200 9I20024 EPA 8260D 09/24/19 19:09 REF trans-1,3-Dichloropropene [10061-02-6]^ 30 UD ug/L 200 30 200 9I20024 EPA 8260D 09/24/19 19:09 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 140 UD ug/L 200 140 200 9I20024 EPA 8260D 09/24/19 19:09 REF Trichloroethene [79-01-6]A 2900 D ug/L 200 30 200 9I20024 EPA 8260D 09/24/19 19:09 REF Trichlorofluoromethane [75-69-4]^ 48 UD ug/L 200 48 200 9I20024 EPA 8260D 09/24/19 19:09 REF Vinyl acetate [108-05-4]^ 190 UD ug/L 200 190 1000 9I20024 EPA 8260D 09/24/19 19:09 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 52 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-PWSF1 Lab Sample ID:CC14233-21 Received: 09/13/19 12:35 Matrix: Water Sampled:09/10/19 13:30 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: Ronald Barron Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]^ 2400 D ug/L 200 64 200 9I20024 EPA 8260D 09/24/19 19:09 REF Xylenes (Total) [1330-20-7]^ 90 UD ug/L 200 90 600 9I20024 EPA 8260D 09/24/19 19:09 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 43 1 50.0 86 % 53-136 9120024 EPA 8260D 09124119 19:09 REF Dlbromofluoromethane 42 1 50.0 85 % 67-129 9120024 EPA 6260D 09124119 19:09 REF Toluene-d8 36 1 50.0 73 % 59-134 9120024 EPA 6260D 09124119 19:09 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes 1,4-Dioxane [123-91-1]^ 3200 D ug/L 100 120 200 9I19040 EPA 8260D 09/19/19 20:19 MJH Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed " Notes Toluene-& 4.8 1 5.00 97 % 75-125 9119040 EPA 8260D 0911.9119 20:19 MJH FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 53 of 74 0Nk"q09 www.encolabs.com ANALYTICAL RESULTS Description: 4401-Trip Blank Lab Sample ID:CC14233-22 Received: 09/13/19 12:35 Matrix: Water Sampled:09/10/19 11:10 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By:ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF 1,1,1-Trichloroethane [71-55-6]^ 0.12 U ug/L 1 0.12 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF 1,1,2,2-Tetrachloroethane [79-34-5]^ 0.28 U ug/L 1 0.28 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF 1,1,2-Trichloroethane [79-00-5]^ 0.14 U ug/L 1 0.14 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF 1,1-Dichloroethane [75-34-3]^ 0.13 U ug/L 1 0.13 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF 1,1-Dichloroethene [75-35-4]^ 0.21 U ug/L 1 0.21 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF 1,2,3-Trichloropropane [96-18-4]^ 0.23 U ug/L 1 0.23 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF 1,2-Dibromoethane [106-93-4]^ 0.66 U ug/L 1 0.66 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF 1,2-Dichlorobenzene [95-50-1]^ 0.19 U ug/L 1 0.19 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF 1,2-Dichloroethane [107-06-2]^ 0.21 U ug/L 1 0.21 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF 1,2-Dichloropropane [78-87-5]^ 0.10 U ug/L 1 0.10 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF 1,4-Dichlorobenzene [106-46-7]^ 0.19 U ug/L 1 0.19 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF 2-Butanone [78-93-3]^ 1.3 U ug/L 1 1.3 5.0 9I16024 EPA 8260D 09/17/19 15:07 REF 2-Hexanone [591-78-6]^ 0.88 U ug/L 1 0.88 5.0 9I16024 EPA 8260D 09/17/19 15:07 REF 4-Methyl-2-pentanone [108-10-1]^ 1.1 U ug/L 1 1.1 5.0 9I16024 EPA 8260D 09/17/19 15:07 REF Acetone [67-64-1]^ 10 U ug/L 1 10 20 9I16024 EPA 8260D 09/17/19 15:07 REF Acrylonitrile [107-13-1]^ 3.5 U ug/L 1 3.5 10 9I16024 EPA 8260D 09/17/19 15:07 REF Benzene [71-43-2]^ 0.15 U ug/L 1 0.15 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF Bromochloromethane [74-97-5]^ 0.48 U ug/L 1 0.48 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF Bromodichloromethane [75-27-4]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF Bromoform [75-25-2]^ 0.22 U ug/L 1 0.22 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF Bromomethane [74-83-9]^ 0.14 U ug/L 1 0.14 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF Carbon disulfide [75-15-0]^ 1.5 U ug/L 1 1.5 5.0 9I16024 EPA 8260D 09/17/19 15:07 REF Carbon tetrachloride [56-23-5]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF Chlorobenzene [108-90-7]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF Chloroethane [75-00-3]^ 0.23 U ug/L 1 0.23 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF Chloroform [67-66-3]^ 0.18 U ug/L 1 0.18 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF Chloromethane [74-87-3]^ 0.13 U ug/L 1 0.13 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF cis-1,2-Dichloroethene [156-59-2]^ 0.15 U ug/L 1 0.15 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF cis-1,3-Dichloropropene [10061-01-5]^ 0.20 U ug/L 1 0.20 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF Dibromochloromethane [124-48-1]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF Dibromomethane [74-95-3]^ 0.27 U ug/L 1 0.27 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF Ethylbenzene [100-41-4]^ 0.13 U ug/L 1 0.13 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF Iodomethane [74-88-4]^ 1.7 U ug/L 1 1.7 5.0 9I16024 EPA 8260D 09/17/19 15:07 REF m,p-Xylenes [108-38-3/106-42-3]^ 0.17 U ug/L 1 0.17 2.0 9I16024 EPA 8260D 09/17/19 15:07 REF Methylene chloride [75-09-2]^ 0.23 U ug/L 1 0.23 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF o-Xylene [95-47-6]^ 0.065 U ug/L 1 0.065 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF Styrene [100-42-5]^ 0.11 U ug/L 1 0.11 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF Tetrachloroethene [127-18-4]^ 0.17 U ug/L 1 0.17 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF Toluene [108-88-3]^ 0.14 U ug/L 1 0.14 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF trans-1,2-Dichloroethene [156-60-5]^ 0.21 U ug/L 1 0.21 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF trans-1,3-Dichloropropene [10061-02-6]^ 0.15 U ug/L 1 0.15 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF trans-1,4-Dichloro-2-butene [110-57-6]^ 0.70 U ug/L 1 0.70 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF QV-01 Trichloroethene [79-01-6]^ 0.15 U ug/L 1 0.15 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF Trichlorofluoromethane [75-69-4]^ 0.24 U ug/L 1 0.24 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF Vinyl acetate [108-05-4]^ 0.95 U ug/L 1 0.95 5.0 9I16024 EPA 8260D 09/17/19 15:07 REF QV-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 54 Of 74 (� �Eo www.encolabs.com ANALYTICAL RESULTS Description: 4401-TripBlank Lab Sample ID:CC14233-22 Received: 09/13/19 12:35 Matrix: Water Sampled:09/10/19 11:10 Work Order: CC14233 Project: Seaboard/Riverdale Landfill Sampled By: ENCO Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte MAS Numberl Results Flag Units DF MDL P L Batch Method Analyzed By Notes Vinyl chloride [75-01-4]1 0.32 U ug/L 1 0.32 1.0 9I16024 EPA 8260D 09/17/19 15:07 REF Xylenes(Total)[1330-20-7]^ 0.45 U ug/L 1 0.45 3.0 9I16024 EPA 8260D 09/17/19 15:07 REF Surrogates Results DF Soike Lv/ % Rec % Rec Limits Batch Method Ana/vzed ffy Notes 4-Bromofluorobenzene 46 1 50.0 91 % 53-136 9116024 EPA 8260D 09117119 15:07 REF Dlbromofluoromethane 46 1 50.0 91 % 67-129 9116024 EPA 6260D 0911711915:07 REF Toluene-d8 38 1 50.0 75 % 59-134 9116024 EPA 6260D 0911711915:07 REF Volatile Organic Compounds by GCMS SIM Isotope Dilution ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Ay Notes 1,4-Dioxane [123-91-1]^ 1.2 U ug/L 1 1.2 2.0 9I19040 EPA 8260D 09/19/19 20:56 MJH Surrogates Results DF So/ke Lv/ % Rec % Rec Limits Batch Method Ana/vzed By Notes Toluene-& 5.1 1 5.00 103 % 75-125 9119040 EPA 8260D 09119119 20:56 MJH FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 55 Of 74 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9116024 - EPA 5030E MS Blank (9I16024-BLK1) Prepared: 09/16/2019 12:10 Analyzed: 09/17/2019 13:33 Analvte Result Flaa POL Units 1, 1, 1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC Level Result %REC Limits RPD RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 56 Of 74 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9116024 - EPA 50308 MS - Continued Blank (9I16024-BLKi) Continued Prepared: 09/16/2019 12:10 Analyzed: 09/17/2019 13:33 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 45 ug/L 50.0 91 53-136 Dibromofluoromethane 45 ug/L 50.0 91 67-129 Toluene-d8 36 ug/L 50.0 76 59-134 LCS (9I16024-BS1) Prepared: 09/16/2019 12:10 Analyzed: 09/17/2019 11:28 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 98 75-133 Benzene 21 1.0 ug/L 20.0 105 80-134 Chlorobenzene 20 1.0 ug/L 20.0 100 80-120 Toluene 20 1.0 ug/L 20.0 101 71-120 Trichloroethene 18 1.0 ug/L 20.0 91 74-120 4-Bromofluorobenzene 46 ug/L 50.0 96 53-136 Dibromofluoromethane 44 ug/L 50.0 88 67-129 Toluene-d8 38 ug/L 50.0 76 59-134 Matrix Spike (9I16024-MS1) Prepared: 09/16/2019 12:10 Analyzed: 09/17/2019 11:59 Source: CC15352-10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 23 1.0 ug/L 20.0 0.21 U 115 75-133 Benzene 22 1.0 ug/L 20.0 0.15 U 112 80-134 Chlorobenzene 22 1.0 ug/L 20.0 0.17 U 108 80-120 Toluene 21 1.0 ug/L 20.0 0.14 U 107 71-120 Trichloroethene 19 1.0 ug/L 20.0 0.15 U 97 74-120 4-Bromofluorobenzene 49 ug/L 50.0 97 53-136 Dibromofluoromethane 45 ug/L 50.0 91 67-129 Toluene-d8 39 ug/L 50.0 77 59-134 Matrix Spike Dup (9I16024-MSD1) Prepared: 09/16/2019 12:10 Analyzed: 09/17/2019 12:31 Source: CC15352-10 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 0.21 U 94 75-133 20 20 Benzene 20 1.0 ug/L 20.0 0.15 U 98 80-134 13 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 94 80-120 13 16 Toluene 19 1.0 ug/L 20.0 0.14 U 96 71-120 11 17 Trichloroethene 16 1.0 ug/L 20.0 0.15 U 82 74-120 17 22 4-Bromofluorobenzene 46 ug/L 50.0 95 53-136 Dibromofluoromethane 45 ug/L 50.0 90 67-129 Toluene-d8 38 ug/L 50.0 76 59-134 Batch 9118027 - EPA 5030E MS Blank (9I18027-BLK3) Prepared: 09/18/2019 10:13 Analyzed: 09/18/2019 15:21 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 57 Of 74 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9118027 - EPA 50308 MS - Continued Blank (9I18027-BLKi) Continued Prepared: 09/18/2019 10:13 Analyzed: 09/18/2019 15:21 Analvte Result Flaa POL Units 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene Dibromofluoromethane FINAL 46 u9/L 50.0 93 53-136 45 u9/L 50.0 91 67-129 This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 58 Of 74 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9118027 - EPA 50308 MS - Continued Blank (9I18027-BLKi) Continued Prepared: 09/18/2019 10:13 Analyzed: 09/18/2019 15:21 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Toluene-d8 38 u91L 50.0 76 59-134 LCS (9I18027-BSI) Prepared: 09/18/2019 10:13 Analyzed: 09/18/2019 13:16 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 97 75-133 Benzene 20 1.0 ug/L 20.0 102 80-134 Chlorobenzene 19 1.0 ug/L 20.0 97 80-120 Toluene 20 1.0 ug/L 20.0 100 71-120 Trichloroethene 17 1.0 ug/L 20.0 87 74-120 4-Bromofluorobenzene 46 u91L 50.0 92 53-136 Dibromofluoromethane 45 u91L 50.0 91 67-129 Toluene-d8 38 u91L 50.0 77 59-134 Matrix Spike (9I18027-MS1) Prepared: 09/18/2019 10:13 Analyzed: 09/18/2019 13:48 Source: CC15675-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 0.21 U 96 75-133 Benzene 20 1.0 ug/L 20.0 0.15 U 100 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 97 80-120 Toluene 20 1.0 ug/L 20.0 0.14 U 98 71-120 Trichloroethene 17 1.0 ug/L 20.0 0.15 U 85 74-120 4-Bromofluorobenzene 47 u91L 50.0 93 53-136 Dibromofluoromethane 46 u91L 50.0 91 67-129 Toluene-d8 38 u91L 50.0 77 59-134 Matrix Spike Dup (9I18027-MSD1) Prepared: 09/18/2019 10:13 Analyzed: 09/18/2019 14:19 Source: CCI5675-07 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 17 1.0 ug/L 20.0 0.21 U 84 75-133 14 20 Benzene 18 1.0 ug/L 20.0 0.15 U 90 80-134 10 17 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 89 80-120 8 16 Toluene 18 1.0 ug/L 20.0 0.14 U 88 71-120 11 17 Trichloroethene 15 1.0 ug/L 20.0 0.15 U 76 74-120 12 22 4-Bromofluorobenzene 46 u91L 50.0 93 53-136 Dibromofluoromethane 45 u9/L 50.0 90 67-129 Toluene-d8 39 u91L 50.0 77 59-134 Batch 9120019 - EPA 5030E MS Blank (9I20019-BLK1) Prepared: 09/20/2019 12:27 Analyzed: 09/20/2019 17:04 Spike Source %REC Analvte Result Flaq POL Units Level Result %REC Limits 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L RPD RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full Page 59 of 74 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9120019 - EPA 50308 MS - Continued Blank (9I20019-BLKi) Continued Prepared: 09/20/2019 12:27 Analyzed: 09/20/2019 17:04 Analvte Result Flaa POL Units 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 46 u9/L 50.0 92 53-136 Dibromofluoromethane 48 u91L 50.0 96 67-129 Toluene-d8 38 u9/L 50.0 77 59-134 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 60 Of 74 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9120019 - EPA 50308 MS - Continued LCS (9I20019-BS1) Prepared: 09/20/2019 12:27 Analyzed: 09/20/2019 14:59 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 99 75-133 Benzene 20 1.0 ug/L 20.0 98 80-134 Chlorobenzene 18 1.0 ug/L 20.0 91 80-120 Toluene 18 1.0 ug/L 20.0 92 71-120 Trichloroethene 16 1.0 ug/L 20.0 82 74-120 4-Bromofluorobenzene 47 ug/L 50.0 94 53-136 Dibromofluoromethane 47 u9/L 50.0 95 67-129 Toluene-d8 38 u91L 50.0 77 59-134 Matrix Spike (9I20019-MS1) Prepared: 09/20/2019 12:27 Analyzed: 09/20/2019 15:30 Source: CC16075-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 21 1.0 ug/L 20.0 0.21 U 103 75-133 Benzene 20 1.0 ug/L 20.0 0.15 U 102 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 93 80-120 Toluene 18 1.0 ug/L 20.0 0.14 U 91 71-120 Trichloroethene 17 1.0 ug/L 20.0 0.15 U 86 74-120 4-Bromofluorobenzene 46 u91L 50.0 92 53-136 Dibromofluoromethane 48 u91L 50.0 97 67-129 Toluene-d8 39 u9/L 50.0 78 59-134 Matrix Spike Dup (9I20019-MSD1) Prepared: 09/20/2019 12:27 Analyzed: 09/20/2019 16:02 Source: CC16075-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 21 1.0 ug/L 20.0 0.21 U 103 75-133 0.2 20 Benzene 20 1.0 ug/L 20.0 0.15 U 100 80-134 2 17 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 94 80-120 0.4 16 Toluene 18 1.0 ug/L 20.0 0.14 U 92 71-120 0.4 17 Trichloroethene 17 1.0 ug/L 20.0 0.15 U 83 74-120 3 22 4-Bromofluorobenzene 46 u91L 50.0 95 53-136 Dibromofluoromethane 47 u9/L 50.0 94 67-129 Toluene-d8 39 u91L 50.0 78 59-134 Batch 9I20024 - EPA 50305 MS Blank (9I20024-BLK3) Prepared: 09/20/2019 13:44 Analyzed: 09/24/2019 17:35 Analvte Result Flaq POL Units 1, 1, 1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 61 of 74 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9I20024 - EPA 50308 MS - Continued Blank (9I20024-BLKI) Continued Prepared: 09/20/2019 13:44 Analyzed: 09/24/2019 17:35 Analvte Result Flaq POL Units 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromof/uorobenzene 44 u91L 50.0 88 53-136 Dibromof/uoromethane 43 u91L 50.0 86 67-129 Toluene-d8 37 u91L 50.0 74 59-134 LCS (9I20024-BS1) Prepared: 09/20/2019 13:44 Analyzed: 09/24/2019 15:30 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 15 1.0 ug/L 20.0 77 75-133 Benzene 18 1.0 ug/L 20.0 91 80-134 Chlorobenzene 18 1.0 ug/L 20.0 89 80-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 62 Of 74 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9I20024 - EPA 50308 MS - Continued LCS (9I20024-BS3) Continued Prepared: 09/20/2019 13:44 Analyzed: 09/24/2019 15:30 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Toluene 18 1.0 ug/L 20.0 88 71-120 Trichloroethene 17 1.0 ug/L 20.0 85 74-120 4-Bromofluorobenzene 44 ug/L 50.0 86 53-136 Dibromofluoromethane 41 u91L 50.0 83 67-129 Toluene-d8 37 u91L 50.0 75 59-134 Matrix Spike (9I20024-MS1) Prepared: 09/20/2019 13:44 Analyzed: 09/24/2019 16:01 Source: CC16075-04 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 15 1.0 ug/L 20.0 0.21 U 77 75-133 Benzene 18 1.0 ug/L 20.0 0.15 U 90 80-134 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 88 80-120 Toluene 17 1.0 ug/L 20.0 0.14 U 86 71-120 Trichloroethene 18 1.0 ug/L 20.0 0.15 U 88 74-120 4-Bromofluorobenzene 44 u91L 50.0 87 53-136 Dibromofluoromethane 42 u91L 50.0 84 67-129 Toluene-d8 37 u91L 50.0 75 59-134 Matrix Spike Dup (9I20024-MSD1) Prepared: 09/20/2019 13:44 Analyzed: 09/24/2019 16:32 Source: CC16075-04 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 16 1.0 ug/L 20.0 0.21 U 79 75-133 3 20 Benzene 19 1.0 ug/L 20.0 0.15 U 94 80-134 3 17 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 91 80-120 3 16 Toluene 18 1.0 ug/L 20.0 0.14 U 90 71-120 4 17 Trichloroethene 18 1.0 ug/L 20.0 0.15 U 92 74-120 5 22 4-Bromofluorobenzene 45 u91L 50.0 69 53-136 Dibromofluoromethane 42 u91L 50.0 84 67-129 Toluene-d8 37 u91L 50.0 75 59-134 Batch 9.714030 - EPA 5030B MS Blank (9314030-BLK3) Prepared: 10/14/2019 13:59 Analyzed: 10/15/2019 05:05 Analvte 1,1,1,2-Tetrachloroethane 1,1,1-Trichloroethane 1,1, 2,2-Tetrachloroethane 1,1,2-Trichloroethane 1,1-Dich loroethane 1,1-Dichloroethene 1,2,3-Trichloropropane 1,2-Di bromo-3-ch loropropane 1,2-Dibromoethane 1,2-Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane 1,4-Dichlorobenzene FINAL Spike Source %REC Result Flaq POL Units Level Result %REC Limits 0.17 U 1.0 ug/L 0.12 U 1.0 ug/L 0.28 U 1.0 ug/L 0.14 U 1.0 ug/L 0.13 U 1.0 ug/L 0.21 U 1.0 ug/L 0.23 U 1.0 ug/L 0.48 U 1.0 ug/L 0.66 U 1.0 ug/L 0.19 U 1.0 ug/L 0.21 U 1.0 ug/L 0.10 U 1.0 ug/L 0.19 U 1.0 ug/L This report relates only to the sample as received by the laboratory, and may only be reproduced in full. RPD RPD Limit Notes Page 63 of 74 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9J14030 - EPA 5030E MS - Continued Blank (9314030-BLK3) Continued Prepared: 10/14/2019 13:59 Analyzed: 10/15/2019 05:05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L 4-Bromof/uorobenzene 50 u91L 50.0 100 53-136 Dibromof/uoromethane 46 u91L 50.0 92 67-129 Toluene-d8 39 u91L 50.0 79 59-134 LCS (9314030-BS1) Prepared: 10/14/2019 13:59 Analyzed: 10/15/2019 02:55 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 100 75-133 Benzene 21 1.0 ug/L 20.0 106 80-134 Chlorobenzene 16 1.0 ug/L 20.0 81 80-120 Toluene 17 1.0 ug/L 20.0 87 71-120 Trichloroethene 20 1.0 ug/L 20.0 98 74-120 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 64 Of 74 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9J14030 - EPA 5030E MS - Continued LCS (9314030-BS3) Continued Prepared: 10/14/2019 13:59 Analyzed: 10/15/2019 02:55 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 48 ug/L 50.0 97 53-136 Dibromofluoromethane 46 ug/L 50.0 92 67-129 Toluene-d8 41 ug/L 50.0 82 59-134 Matrix Spike (9314030-MS1) Prepared: 10/14/2019 13:59 Analyzed: 10/15/2019 03:27 Source: CC17406-05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 0.21 U 102 75-133 Benzene 22 1.0 ug/L 20.0 0.15 U 110 80-134 Chlorobenzene 17 1.0 ug/L 20.0 0.17 U 84 80-120 Toluene 18 1.0 ug/L 20.0 0.14 U 88 71-120 Trichloroethene 21 1.0 ug/L 20.0 0.15 U 105 74-120 4-Bromofluorobenzene 46 ug/L 50.0 97 53-136 Dibromofluoromethane 44 ug/L 50.0 88 67-129 Toluene-d8 41 ug/L 50.0 81 59-134 Matrix Spike Dup (9314030-MSD1) Prepared: 10/14/2019 13:59 Analyzed: 10/15/2019 04:00 Source: CC17406-05 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 0.21 U 102 75-133 0.2 20 Benzene 23 1.0 ug/L 20.0 0.15 U 115 80-134 4 17 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 90 80-120 6 16 Toluene 19 1.0 ug/L 20.0 0.14 U 94 71-120 6 17 Trichloroethene 21 1.0 ug/L 20.0 0.15 U 103 74-120 2 22 4-Bromofluorobenzene 48 ug/L 50.0 95 53-136 Dibromofluoromethane 44 ug/L 50.0 88 67-129 Toluene-d8 40 ug/L 50.0 61 59-134 Batch 9J15032 - EPA 5030E MS Blank (9315032-BLK3) Prepared: 10/15/2019 15:00 Analyzed: 10/16/2019 08:29 Analvte Result Flaq POL Units 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 65 Of 74 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9J15032 - EPA 5030E MS - Continued Blank (9315032-BLK3) Continued Prepared: 10/15/2019 15:00 Analyzed: 10/16/2019 08:29 Analvte Result Flaa POL Units 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes 4-Bromofluorobenzene 46 u91L 50.0 91 53-136 Dibromofluoromethane 48 u9/L 50.0 95 67-129 Toluene-d8 37 u9/L 50.0 74 59-134 LCS (9315032-BSI) Prepared: 10/15/2019 15:00 Analyzed: 10/15/2019 21:33 Spike Source %REC RPD Analvte Result Flaa CQ Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 96 75-133 Benzene 21 1.0 ug/L 20.0 105 80-134 Chlorobenzene 19 1.0 ug/L 20.0 95 80-120 Toluene 19 1.0 ug/L 20.0 95 71-120 Trichloroethene 20 1.0 ug/L 20.0 98 74-120 4-Bromofluorobenzene 44 u9/L 50.0 69 53-136 Dibromofluoromethane 44 u91L 50.0 89 67-129 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 66 Of 74 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9J15032 - EPA 5030E MS - Continued LCS (9115032-BS3) Continued Prepared: 10/15/2019 15:00 Analyzed: 10/15/2019 21:33 Spike Source %REC RPD Analvte Result Flaq Q Units Level Result %REC Limits RPD Limit Notes Toluene-d8 37 u91L 50.0 75 59-134 Matrix Spike (9315032-MS1) Prepared: 10/15/2019 15:00 Analyzed: 10/15/2019 22:05 Source: CC17406-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 18 1.0 ug/L 20.0 0.21 U 89 75-133 Benzene 20 1.0 ug/L 20.0 0.15 U 98 80-134 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 90 80-120 Toluene 17 1.0 ug/L 20.0 0.14 U 87 71-120 Trichloroethene 18 1.0 ug/L 20.0 0.15 U 89 74-120 4-Bromofluorobenzene 45 u9/L 50.0 89 53-136 Dibromofluoromethane 44 u91L 50.0 89 67-129 Toluene-d8 38 u9/L 50.0 75 59-134 Matrix Spike Dup (9715032-MSD1) Prepared: 10/15/2019 15:00 Analyzed: 10/15/2019 22:36 111 Source: CC17406-09 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 18 1.0 ug/L 20.0 0.21 U 90 75-133 0.6 20 Benzene 20 1.0 ug/L 20.0 0.15 U 101 80-134 3 17 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 90 80-120 0.06 16 Toluene 18 1.0 ug/L 20.0 0.14 U 89 71-120 2 17 Trichloroethene 18 1.0 ug/L 20.0 0.15 U 92 74-120 3 22 4-Bromofluorobenzene 45 u91L 50.0 90 53-136 Dibromofluoromethane 45 u9/L 50.0 69 67-129 Toluene-d8 38 u91L 50.0 76 59-134 Batch 9J16023 -EPA 5030B MS Blank (9116023-BLK3) Prepared: 10/16/2019 11:10 Analyzed: 10/16/2019 15:42 Analvte Result Flaq POL Units 1,1,1,2-Tetrachloroethane 0.17 U 1.0 ug/L 1,1,1-Trichloroethane 0.12 U 1.0 ug/L 1,1,2,2-Tetrachloroethane 0.28 U 1.0 ug/L 1,1,2-Trichloroethane 0.14 U 1.0 ug/L 1,1-Dichloroethane 0.13 U 1.0 ug/L 1,1-Dichloroethene 0.21 U 1.0 ug/L 1,2,3-Trichloropropane 0.23 U 1.0 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 1.0 ug/L 1,2-Dibromoethane 0.66 U 1.0 ug/L 1,2-Dichlorobenzene 0.19 U 1.0 ug/L 1,2-Dichloroethane 0.21 U 1.0 ug/L 1,2-Dichloropropane 0.10 U 1.0 ug/L 1,4-Dichlorobenzene 0.19 U 1.0 ug/L 2-Butanone 1.3 U 5.0 ug/L 2-Hexanone 0.88 U 5.0 ug/L 4-Methyl-2-pentanone 1.1 U 5.0 ug/L Acetone 10 U 20 ug/L Spike Source %REC Level Result %REC Limits RPD RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 67 Of 74 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9.716023 - EPA 5030E MS - Continued Blank (9116023-BLK3) Continued Prepared: 10/16/2019 11:10 Analyzed: 10/16/2019 15:42 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes Acrylonitrile 3.5 U 10 ug/L Benzene 0.15 U 1.0 ug/L Bromochloromethane 0.48 U 1.0 ug/L Bromodichloromethane 0.17 U 1.0 ug/L Bromoform 0.22 U 1.0 ug/L Bromomethane 0.14 U 1.0 ug/L Carbon disulfide 1.5 U 5.0 ug/L Carbon tetrachloride 0.17 U 1.0 ug/L Chlorobenzene 0.17 U 1.0 ug/L Chloroethane 0.23 U 1.0 ug/L Chloroform 0.18 U 1.0 ug/L Chloromethane 0.13 U 1.0 ug/L cis- 1,2-Dichloroethene 0.15 U 1.0 ug/L cis- 1,3-Dichloropropene 0.20 U 1.0 ug/L Dibromochloromethane 0.17 U 1.0 ug/L Dibromomethane 0.27 U 1.0 ug/L Ethylbenzene 0.13 U 1.0 ug/L Iodomethane 1.7 U 5.0 ug/L m,p-Xylenes 0.17 U 2.0 ug/L Methylene chloride 0.23 U 1.0 ug/L o-Xylene 0.065 U 1.0 ug/L Styrene 0.11 U 1.0 ug/L Tetrachloroethene 0.17 U 1.0 ug/L Toluene 0.14 U 1.0 ug/L trans-1,2-Dichloroethene 0.21 U 1.0 ug/L trans-1,3-Dichloropropene 0.15 U 1.0 ug/L trans-1,4-Dichloro-2-butene 0.70 U 1.0 ug/L Trichloroethene 0.15 U 1.0 ug/L Trichlorofluoromethane 0.24 U 1.0 ug/L Vinyl acetate 0.95 U 5.0 ug/L Vinyl chloride 0.32 U 1.0 ug/L Xylenes (Total) 0.45 U 3.0 ug/L 4-Bromofluorobenzene 45 u9/L 50.0 69 53-136 Dibromofluoromethane 48 u9/L 50.0 96 67-129 Toluene-d8 37 u91L 50.0 75 59-134 LCS (9316023-BS1) Prepared: 10/16/2019 11:10 Analyzed: 10/16/2019 13:36 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 100 75-133 Benzene 21 1.0 ug/L 20.0 107 80-134 Chlorobenzene 19 1.0 ug/L 20.0 96 80-120 Toluene 19 1.0 ug/L 20.0 96 71-120 Trichloroethene 19 1.0 ug/L 20.0 97 74-120 4-Bromofluorobenzene 45 u91L 50.0 91 53-136 Dibromofluoromethane 45 u91L 50.0 90 67-129 Toluene-d8 37 u9/L 50.0 75 59-134 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 68 Of 74 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 9.716023 - EPA 5030E MS - Continued Matrix Spike (9316023-MS3) Prepared: 10/16/2019 11:10 Analyzed: 10/16/2019 14:08 Source: CC17564-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 1.0 ug/L 20.0 0.21 U 102 75-133 Benzene 22 1.0 ug/L 20.0 0.15 U 108 80-134 Chlorobenzene 19 1.0 ug/L 20.0 0.17 U 96 80-120 Toluene 19 1.0 ug/L 20.0 0.14 U 94 71-120 Trichloroethene 20 1.0 ug/L 20.0 0.15 U 98 74-120 4-Bromofluorobenzene 45 ug/L 50.0 90 53-136 Dibromofluoromethane 45 u91L 50.0 91 67-129 Toluene-d8 38 u91L 50.0 75 59-134 Matrix Spike Dup (9316023-MSD1) Prepared: 10/16/2019 11:10 Analyzed: 10/16/2019 14:39 Source: CC17564-02 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 19 1.0 ug/L 20.0 0.21 U 94 75-133 9 20 Benzene 20 1.0 ug/L 20.0 0.15 U 102 80-134 6 17 Chlorobenzene 18 1.0 ug/L 20.0 0.17 U 92 80-120 4 16 Toluene 18 1.0 ug/L 20.0 0.14 U 92 71-120 2 17 Trichloroethene 18 1.0 ug/L 20.0 0.15 U 92 74-120 7 22 4-Bromofluorobenzene 45 u91L 50.0 89 53-136 Dibromofluoromethane 46 u91L 50.0 92 67-129 Toluene-d8 38 u91L 50.0 76 59-134 Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch 9119040 - EPA 5030E MS Blank (9I19040-BLK1) Prepared: 09/19/2019 00:00 Analyzed: 09/19/2019 11:23 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 1.2 U 2.0 ug/L Toluene-d8 4.9 u91L 5.00 98 75-125 LCS (9I19040-BS1) Prepared: 09/19/2019 00:00 Analyzed: 09/19/2019 10:49 Spike Source %REC RPD Analvte Result Fh Q Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 25 2.0 ug/L 25.0 99 80-133 Toluene-d8 4.8 u91L 5.00 97 75-125 LCS Dup (9I19040-BSD1) Prepared: 09/19/2019 00:00 Analyzed: 09/19/2019 11:57 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 23 2.0 ug/L 25.0 90 80-133 9 19 QM-10 Toluene-& 4.5 u91L 5.00 91 75-125 QM-10 Batch 9I20040 - EPA 50308 MS FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 69 Of 74 0Nk"q09 www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch 9120040 - EPA 5030E MS - Continued Blank (9I20040-BLKi) Prepared: 09/20/2019 00:00 Analyzed: 09/20/2019 10:41 Spike Source %REC RPD Analvte Result Flao POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 1.2 U 2.0 ug/L Toluene-& 4.5 u9/L 5.00 91 75-125 LCS (9I20040-BS1) Prepared: 09/20/2019 00:00 Analyzed: 09/20/2019 10:06 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limi RPD Limit Notes 1,4-Dioxane 25 2.0 ug/L 25.0 100 80-133 Toluene-& 4.8 u9/L 5.00 95 75-125 LCS Dup (9I20040-BSD1) Prepared: 09/20/2019 00:00 Analyzed: 09/20/2019 11:16 Spike Source %REC RPD Analvte Result Flan POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 23 2.0 ug/L 25.0 93 80-133 7 19 QM-10 Toluene-& 4.5 u9/L 5.00 91 75-125 QM-10 Batch 9120043 - EPA 5030E MS Blank (9I20043-BLKi) Prepared: 09/20/2019 14:35 Analyzed: 09/20/2019 23:22 Spike Source %REC RPD Analvte Result Flaa POL Uni Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 1.2 U 2.0 ug/L Toluene-d8 5.2 u9/L 5.00 105 75-125 LCS (9I20043-BS1) Prepared: 09/20/2019 14:35 Analyzed: 09/20/2019 22:09 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 26 2.0 ug/L 25.0 105 80-133 Toluene-& 5.1 u9/L 5.00 102 75-125 LCS Dup (9I20043-BSD1) Prepared: 09/20/2019 14:35 Analyzed: 09/20/2019 22:45 Spike Source %REC RPD Analvte Result Flaa POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 23 2.0 ug/L 25.0 92 80-133 13 19 QM-10 Toluene-d8 4.9 u9/L 5.00 98 75-125 QM-10 Batch 9123034 - EPA 5030E MS Blank (9I23034-BLKi) Prepared: 09/23/2019 00:00 Analyzed: 09/23/2019 10:43 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 1.2 U 2.0 ug/L Toluene-& 5.1 u9/L 5.00 102 75-125 LCS (9I23034-BSI) Prepared: 09/23/2019 00:00 Analyzed: 09/23/2019 09:37 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. F Page 70 Of 74 (� �Eo www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS SIM Isotope Dilution - Quality Control Batch 9I23034 - EPA 50308 MS - Continued LCS (9I23034-BS3) Continued Prepared: 09/23/2019 00:00 Analyzed: 09/23/2019 09:37 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 22 2.0 ug/L 25.0 88 80-133 Toluene-d8 4.5 u9/L 5.00 91 75-125 LCS Dup (9I23034-BSD1) Prepared: 09/23/2019 00:00 Analyzed: 09/23/2019 11:16 Spike Source %REC RPD Analvte Result Flaq POL Units Level Result %REC Limits RPD Limit Notes 1,4-Dioxane 23 2.0 ug/L 25.0 92 80-133 5 19 QM-10 Toluene-d8 5.1 u9/L 5.00 102 75-125 QM-10 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 71 of 74 (� �Eo www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. The PQL presented is the laboratory MRL. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. [CALC] Calculated analyte - MDL/MRL reported to the highest reporting limit of the component analyses. Q-01 Analysis performed outside of method - specified holding time. QL-02 The associated laboratory control sample exhibited high bias; since the result is ND, there is no impact. QM-10 LCS/LCSD were analyzed in place of MS/MSD. QV-01 The associated continuing calibration verification standard exhibited high bias; since the result is ND, there is no impact. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. 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