22004_Witherspoon Nursery_RRPT_20180404

April 4, 2018
Mr. Chris Howlett
Beacon Properties & Investments
16122 Morehead Drive
Chapel Hill, North Carolina 27517
Re: Soil Excavation Activities — Witherspoon Roses Property
Heating Oil Aboveground Storage Tank
3312 Watkins Road
Durham, Durham County, North Carolina
ATC Project No. BEACONAST
Dear Mr. Howlett:
:kTc
ENVIRONMENTAL • GEOTECHNICAL
BUILDING SCIENCES • MATERIALS TESTING
ATC Associates of North Carolina, P.C. (ATC) has prepared this letter report regarding soil
excavation activities conducted at the Witherspoon Roses property at 3312 Watkins Road in
Durham, Durham County, North Carolina.
BACKGROUND
The property has historically operated as a rose landscaping business and garden supply shop since
1979. In September 2017, Terracon conducted a Phase II Limited Site Investigation for the property.
During these activities, a soil sample was collected from the area of an on -site heating oil
aboveground storage tank (AST). Laboratory analytical results of the soil sample detected Total
Petroleum Hydrocarbon (TPH) — Diesel Range Organics (DRO) at a concentration of 270 milligrams
per kilogram (mg/kg), which is above the North Carolina Department of Environmental Quality
(NCDEQ) Action Level of 100 mg/kg.
SOIL EXCAVATION ACTIVITIES
On March 5, 2018, ATC contracted with Eastern Environmental Management (EEM) of Rocky
Mount, North Carolina to assist with the excavation of petroleum -impacted soil in proximity to the
280-gallon heating oil aboveground storage tank (AST) (labeled AST-3). The heating oil AST was
transported from the property for proper disposal on March 5, 2018. Prior to its removal,
approximately 68 gallons of heating oil were removed from the AST. The approximate location of
the heating oil AST is provided in Attachment I. A copy of the pump out manifest and AST
disposal manifest are provided in Attachment II
On March 5, 2018, EEM and ATC personnel excavated approximately six tons of
petroleum -impacted soil from the area of AST-3. The AST-3 excavated area measured
approximately seven to nine feet in length, seven to nine feet in width, and approximately four feet in
depth. The soil was mainly tan to light gray sand with fine to medium gravel to approximately three
feet below ground surface (bgs). Groundwater was not encountered during excavation activities.
Excavated soils were placed directly into a dump truck and disposed of at Soil Resources, LLC in
Pinetops, North Carolina. The soil excavation area, as well as pictures of excavation activities,
are provided in Attachment I. The waste manifest for the soil is included in Attachment II.
ATC personnel performed confirmatory soil sampling prior to backfilling the excavated area of
AST-3. One soil sample was collected the bottom of the excavation and from each sidewall by
ATC Associates of North
Carolina, P.C.
609A Piner Road, Suite115
Wilmington, NC 28409
USA
Phone: [phone]
Fax: [phone]
www.atcqs.com

W
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ENVIRONMENTAL • GEOTECHNICAL
3UILOING SCIENCES - MATERIALS TESTING
April 4, 2019
Page 2 of 2
hand using clean nitrile gloves between each sampling location. The soil samples were labeled
according to their location. These samples were collected to determine the effectiveness of the soil
excavation activities. The locations of the confirmatory soil samples are depicted on Attachment
I.
All samples were collected in laboratory -supplied containers and shipped on ice to Colt -test
Analytical Laboratory (Con -test) located in East Longmeadow, Massachusetts. Confirmation soil
samples collected from excavation area AST-3 utilized Environmental Protection Agency (EPA)
Method 8260 and EPA Method 8270. It should be noted one soil sample, AST-3 North ( 1 -2) also
was analyzed by Total Petroleum Hydrocarbons (TPH) -- Gasoline Range Organics (GRO) and
Diesel Range Organics (DRO) and TCLP Metals for soil disposal purposes.
Based on the laboratory analytical results utilizing EPA Method 8260 and EPA Method 8270, target
compound concentrations were not detected above Soil -to -Groundwater (STGW) Maximum
Contaminant Concentrations (MSCCs) in the soil samples collected from the AST-3 excavation
area. Target compound concentration detected above the laboratory method detection limit, but
below the STGW-MSCCs, are presented in Attachment III. A copy of the laboratory reports and
chains -of -custody documents are provided in Attachment IV.
Following completion of excavation activities, the excavated area was backfilled with clean fill
material that was obtained from another portion of the property.
CONCLUSIONS
Based on the above activities and subsequent laboratory results, it appears heating oil -impacted soil
have been effectively removed from the area of the former heating oil AST and no other activities
are warranted at this time.
If you have any questions or require additional information, please contact our office at (919)
871-0999.
Sincerely,
ATC Associates of North Carolina, P.C.
Maureen Jackson, P
Senior Project Mangy
N.C. Licensed Geol
*0A GAR04
5zCoF
yy F� A
�Hflip 11 Mllfy��
Benjamin V. Wilson, P.E.
Principle Geotechnical Engineer

Attachment I

609A Piner Road, Suite 115
N4LTc Wilmington, North Carolina 28409
ENVIRONMENTAL • GEOTEGHNIUL [phone]
BUILDING SCIENCES - MATERIALS TESTING
Project No. DATE: PM:
BEACONAST 0311412018 Maureen Jackson
r
�ardt�on�
•� Y
Xp
Figure 1: Soil Excavation Area
Witherspoon Roses Fi-ogei-ty
3312 Watkins Road
Durham, Durham County, North Carolina

(Irl
•.
� .IU,I/11/f
Fill
F�WI
<� +1
IL
• ANY
.. �� !
+k.......1,
NEj P11
.,
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_
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16
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Photo 3: View of AST-3 Excavation Backfilled
Photo 4: Source location of backfill material (looking west)
Witherspoon Roses Property
3312 Watkins Road
Durham, North Carolina
ATC Project No. BEACONAST

Attachment II

Eastern Environmental ManagemenU
P.O. Box 4030 - Rocky Mount, NC 27803
Office [phone] (24 Hrs.) - Fax [phone]
www,eastern-environmental.com
NON -HAZARDOUS Generator's US EPA ID No.
Manifest
2. Page
11.
WASTE MANIFEST
Document No.
of
3. Generator's Name and Mailing Address fj -�
Contact:
4. Generator's Phone
5. Transporter 1 Company Name 6. US EPA ID Number
A. State Transporter's ID
600308640
EASTERN ENVIRONMENTAL MANAGEMENT NCR00146456
B. Transporter 1 Phone
252-443-2224
7. Transporter 2 Company Name S. US EPA ID Number
C. State Transporter's I❑
D. Transporter 2 Phone
9. Designate Facility Name and Site Address 10. US EPA ID Number
E. State Facility's ID
SCII K6(461"l
(� {1 ���"
i' .f1 Y
F.Facility's Phone
11. WASTE DESCRIPTION
12. Containers
13,
14,
No. Type
Quantlit
Unit
WtNol.
a.
E
N
b.
R
A
T
c.
O
R
d.
e.
f.
15. Special Handling Instructions and Additional Information
16, GENERATOR'S CERTIFICATION' I hereby certify that the contents of this shipment are fully and accurately described and are in all respects in
proper condition for transport. The materials described on this manifest are not subjectto federal hazardous waste regulations.
Date
edlTyd me
t(1k
5i n ur
�144
Month Day Year
fil t�V
IL I + Y
T
17. Trans rter 1 Acknowledgment of Receipt of Matefial
Date
A
s
Printed/Typed Na a Sig
- lid;G
Month Clay Year
7
!i
p18.
R
Transporter 2 Acknowledgment of Receipt of Materials
Date
Printed/Typed Name
Signature
Month Day Year
E
R
P
19. Discrepancy Indication Space
A
C
I
L
20. Faaccility_Owner or Operator: Certification of receipt of the waste materials covered b this
cept as noted in item 19.
I
F�J
p
Date
T
Printe yp Name
Signa
Month Day Year
Y
t, dy Z
I `Y )v

Soil Resources, LLC
Physical Address:
402 Orchard Road
Pinetops, NC
Office: 252-904-2457
Mailing Address:
PO Box 4005
Rocky Mount, NC 27803
Fax: [phone]
Soil Resources, LLC is operating under the State of North Carolina Contaminated Soil
Disposal Permit # SR-0002, hereby acknowledges the receipt of 11.64 tans of soil
contaminated with petroleum hydrocarbons and will properly execute the disposal
of this soil in the prescribed manner set forth by the North Carolina Department of
Environment and Natural Resources, Division of Waste Management, and in
accordance with the requirements of SR-0002.
Company:
Generator:
Transporter:
Date(s) Received:
Eastern Environmental Management
PO Box 4030
Rocky Mount, NC 27803
Witherspoon Property
3312 Watkins Rd
Durham, NC
Eastern Environmental Management, LLC
PO Box 4030
Rocky Mount, NC 27803
11/07/12 [E-06191]
Soil Resources, LLC
By-
C�jl C. S

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cl

Eastern Environmental Management
P.O. Box 4030 • Rocky Mount, NC 27803
Office [phone] (24 Hrs.) • Fax [phone]
www.eastern-environmental.com
NON -HAZARDOUS
1. Generator's US EPA ID No.
Manifest
2. Page
WASTE MANIFEST
Document
No.
of
3. Generator's Name and Mailing Address {-��!61c,V1 5 e Oy
Contact:
4. Generator's Phone t Fief"�
5. Transporter 1 Company Name 6. US EPA ID Number
A. State Transporter's ID
600308640
EASTERN ENVIRONMENTAL MANAGEMENT NCR000146456
B. Transporter 1 Phone [phone]
7, Transporter 2 Company Name 8. US EPA ID Number
C. State Transporter's ID
D. Transporter 2 Phone
9, Desi Hated Facility Name and Site Address 10. US EPA ID Number
E. State Facility's ID
rty CTF r, 3
F. Facility's Phone
/LA�r ��
t L'U�
L-S 1---
11. WASTE bESCRIPTION
12. Containers
13.
14.
No.
Type
Quantlit
Wt Unit
a.
-
�-
N
b.
E
R
A
T
c.
R
d.
e.
f.
15. Special Handling Instructions and Additional Information
16. GENERATOR'S CERTIFICATION: I hereby certify thatthe contents of this shipment are fully and accurately described and are in all respects in
proper condition for transport. The materials described on this manifest are not subject to federal hazardous aste regulations.
Date
PjF,i . Inted�Ty d ame
yE
n ur
Month
3
Day Yea
�
ri 36, zv. s
TT
17. Transporter 1 Acknowledgment of Receipt of Material
Date
Pri d yped Na a
Signet
41
Month
Day Year
P
f
1'4
o
R
18. Transporter 2 Ac Oow led gment of Receipt of Materials
Date
PrintedlTyped Name
Signature
Month
Day Year
E
R
F
19. Discrepancy Indication Space
A
C
I
L
2�cility Owner or Operator; Certification of receipt of the waste materials cn�e d this m i e , xcept as noted in item 19.
1
//�
Date
YPrue
ype Name
Sign
M th
Day Year
�.J7 I
I I

Eastern Environmental Management
P.O. Box 4030 ■ Rocky Mount, NC 27803
Office [phone] (24 Hrs.) • Fax [phone]
www.eastem-environmeiital.com
NON -HAZARDOUS
I. Generator's US EPA ID Na.
Manifest
2. Page
WASTE MANIFEST
Document No.
of
3. Generator's Name and Mailing Address s o.FqKil, f
Contact:
4. Generator's Phone
5. Transporter 1 Company Name S. US EPA ID Number
A. State Transporter's ID
600308640
EASTERN ENVIRONMENTAL MANAGEMENT NCR000146456
B. Transporter 1 Phone [phone]
7. Transporter 2 Company Name S. US EPA ID Number
C. State Transporter's I❑
D. Transporter 2 Phone
9. ❑ signated Facility !Name and Site Address 10. US EPA ID Number
E. State Facility's ID
�1A
va ei, L�
{ f S7 S A A-"
F. Facility's Phone
1-k-r _ �Y A/C 000iV6 (1J L
S-Z -Q1 ; -
11. WASTE hESCRIPTION
12. Containers
13.
14.
No.
Type
Total
Quantity
Unit
Wt.Nol,
a.
E
I
E G-rr1
T ll
N
b.
E
R
A
T
c-
O
R
d.
e.
f.
15. Special Handling Instructions and Additional Information
16. GENERATOR'S CERTIFICATION: I hereby certity that the contents of this shipment are fully and accurately described and are in all respects in
proper condition for transport. The materials described on this manifest are not subjeet to federal hazardous waste regulations.
Date
PrintedlTyped Name
Month
❑ay. Year
/f
C Lt ,�i; �%� �c :� ism• .h'�. s
VUA4_
a
s of �
TR
17. Transporter 1 Acknowledgment of Recei f Material f
Date
N
Pr' tggl/Typed Nye
5i to
Month
Day Year
O18.
Trans orter 2 Acknowledgment of Receipt of Materials
Date
PrintedlTyped Name
Signature
Month
Day Year
E
R
F
19. Discrepancy Indication Space
A
C
I
U
20. Facjlity Ownewor Operator: Certification of receipt of the waste materials y anifest, except as noted in item 19.
W J�
I
GC
Date
T
Printe yp aame
Si r
Month
❑ate_
Y
f�
(�"U r 1
Q

Eastern Environmental Management, LLC
P.O. Box 4030
Rocky Mount, NC 27803
Office [phone] (24 Hrs.)
Fax [phone]
www.eastem-environmental.com
Certipeate of disposal
Generator: Witherspoon Roses Property
3312 Watkins RD
Durham, NC
Material Accepted:
1- TT (s)- (68-gal.) — Non -hazardous Material -
Petroleum Contact Water
1-DM (s)- (280) — AST fuel oil tank
Disposal Method:
Waste water treatment
Recycle
Eastern Environmental Management LLC. Accepted the above materials on 03/05/2018
Eastern Environmental Management LLC has accepted custody of the above referenced non -hazardous
material. This material has been determined to be non -hazardous by a material profile, generator
knowledge, and/%finalytical data provided to Eastern Environmental Management, LLC.
JoV ny Egdnes, CEO.

Attachment III

Table 1
Soil Excavation Confirmation Laboratory Results
Witherspoon Roses Property
3312 Watkins Road
Durham, North Carolina
ATC Project No. BEACONAST
EPA METHOD
ANALTYICAL METHOD
8270
Sample
Sample ID
Date
PID
Depth
.�
Sampled
(ppm)
(feet)
;
d
G�
U
�
U
AST-3 Floor
3/5/2018
0.8
3
<0.43
<1.3
AST-3 North (1-2)
3/5/2018
2.9
1-2
<0.41
0.45J
AST-3 North (3-4)
3/5/2018
0.0
3-4
<0.40
<1.2
AST-3 South
3/5/2018
0.0
1-2
<0.42
<1.2
AST-3 West
3/5/2018
0.0
1-2
<0.40
<1.2
AST-3 East
3/5/2018
1.2
1-2
<0.43
<1.3
Soil -to -Groundwater MSCCs
NE
120
Notes:
1. Concentrations reported in milligrams per kilogram (mg/kg).
2. "<" = not detected at or above the laboratory detection limit.
3. NE denotes Soil -to -Groundwater MSCC has not been established.
4. J value denotes concentration estimated by the laboratory.
5. MSCC denotes Maximum Soil Contaminant Concentration

Attachment IV

con-test
46%
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
March 13, 2018
Maureen Jackson
ATC Group Services LLC - Raleigh NC
2725 East Millbrook Road, Ste 121
Raleigh, NC 27604
Project Location: 3312 Watkins Rd
Client Job Number:
Project Number: [none]
Laboratory Work Order Number: 18CO324
Enclosed are results of analyses for samples received by the laboratory on March 6, 2018. If you have any questions concerning
this report, please feel free to contact me.
Sincerely,
�Suwj �{. vxu
Kerry K. McGee
Project Manager
Page 1 of 94

Table of Contents
Table of Contents
Sample Summary
Hits Only Report
Case Narrative
Sample Results
18C0324-01
18C0324-02
18C0324-03
18C0324-04
18C0324-05
18C0324-06
18C0324-07
18C0324-08
18C0324-09
18C0324-10
18C0324-11
Sample Preparation Information
QC Data
Volatile Organic Compounds by GC/MS
B 198462
Semivolatile Organic Compounds by GUMS
B 198559
Petroleum Hydrocarbons Analyses
B198557
B198651
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
4
5
7
11
11
16
21
26
31
36
41
48
53
58
63
68
70
70
70
75
75
83
83
83
84
Page 2 of 94

Table of Contents
Table of Contents (continued)
B 198433
TCLP - Metals Analyses
B 198629
B 198633
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
84
85
85
85
86
87
91
Page 3 of 94

Table of Contents
icon -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
ATC Group Services LLC - Raleigh NC
2725 East Millbrook Road, Ste 121 REPORT DATE: 3/13/2018
Raleigh, NC 27604 PURCHASE ORDER NUMBER:
ATTN: Maureen Jackson
PROJECT NUMBER: [none]
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 18CO324
The results of analyses performed on the following samples submitted to the CON -TEST Analytical Laboratory are found in this report
PROJECT LOCATION: 3312 Watkins Rd
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
AST-1 Floor 18C0324-01 Soil SM 254OG
SW-846 8260B
SW-846 8270D
AST -I South 18CO324-02 Soil SM 2540G
SW-846 8260B
SW-846 8270D
AST-1 North 18C0324-03 Soil SM 254OG
SW-846 8260B
SW-846 8270D
AST-1 West 18C0324-04 Soil SM 2540G
SW-846 8260B
SW-846 8270D
AST-1 East 18C0324-05 Soil SM 254OG
SW-846 8260B
SW-846 8270D
AST-3 Floor 18C0324-06 Soil SM 2540G
SW-846 8260B
SW-846 8270D
AST-3 North (1-2) 18CO324-07 Soil SM 2540G
SW-846 601OC-D
SW-846 7470A
SW-846 8015C
SW-846 8260B
SW-846 8270D
AST-3 North (3-4) 18C0324-08 Soil SM 254OG
SW-846 8260B
SW-846 8270D
AST-3 South 18C0324-09 Soil SM 2540G
SW-846 8260B
SW-846 8270D
AST-3 West 18CO324-10 Soil SM 254OG
SW-846 8260B
SW-846 8270D
AST-3 East 18CO324-11 Soil SM 2540G
SW-846 8260B
SW-846 8270D
Page 4 of 94

con-testo
ANALYTICAL LABORATORY
Table of Contents
Client ID: AST-1 Floor
Analyte
Butylbenzylphthalate
% Solids
Client ID: AST-1 South
Analyte
% Solids
Client ID: AST-1 North
Analyte
Benzoic Acid
% Solids
Client ID: AST-1 West
Analyte
% Solids
Client ID: AST-1 East
Analyte
% Solids
Client ID: AST-3 Floor
Analyte
% Solids
Client ID: AST-3 North (1-2)
Analyte
Benzoic Acid
Diesel Range Organics
% Solids
Barium
Lead
Mercury
Client ID: AST-3 North (3-4)
Analyte
% Solids
Client ID: AST-3 South
Analyte
% Solids
Client ID: AST-3 West
Analyte
% Solids
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
EXECUTIVE SUMMARY
Lab ID:
18C0324-01
Results/Qual
DL
RL
Units
Method
0.12 J
0 093
039
mg/Kg dry
SW-846 8270D
87.0
% Wt
SM 2540G
Lab ID:
18CO324-02
Results/Qual
DL
RL
Units
Method
85.4
% Wt
SM 2540G
Lab ID:
18CO324-03
Results/Qual
DL
RL
Units
Method
0.27 J
021
12
mg/Kg dry
SW-846 8270D
85.4
% Wt
SM 2540G
Lab ID:
18CO324-04
Results/Qual
DL
RL
Units
Method
88.6
% Wt
SM 2540G
Lab ID:
18C0324-05
Results/Qual
DL
RL
Units
Method
84.5
% Wt
SM 2540G
Lab ID:
18C0324-06
Results/Qual
DL
RL
Units
Method
78.4
% Wt
SM 2540G
Lab ID:
18CO324-07
Results/Qual
DL
RL
Units
Method
0.45 1
022
12
mg/Kg dry
SW-846 8270D
1600
23
100
mg/Kg dry
SW-846 8015C
82.3
% Wt
SM 2540G
0.22
00053
0 050
mg/L
SW-846 601OC-D
0.14
00044
0 010
mg/L
SW-846 601OC-D
0.000059 J
0000034
000010
mg/L
SW-846 7470A
Lab ID:
18CO324-08
Results/Qual
DL
RL
Units
Method
84.2
% Wt
SM 2540G
Lab ID:
18CO324-09
Results/Qual
DL
RL
Units
Method
81.5
% Wt
SM 2540G
Lab ID:
18CO324-10
Results/Qual
DL
RL
Units
Method
85.8
% Wt
SM 2540G
Page 5 of 94

con-testo
ANALYTICAL LABORATORY
Table of Contents
Client ID: AST-3 East
Analyte
% Solids
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Lab ID: 18C0324-11
Results/Qual DL RL Units Method
78.3 % Wt SM 2540G
Con -Test does not accept liability for the consequences of any actions taken solely on the basis of the information provided in the Executive Summary
section of this report. Users must review this report in its entirety to determine data usability and assessment.
Page 6 of 94

con-test
46%
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CASE NARRATIVE SUMMARY
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report
Page 7 of 94

Table of Contents
icon -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
SW-846 6010C-D
Qualifications:
L-02
Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits Data validation is not
affected since all results are 'hot detected" for associated samples in this batch and bias is on the high side
Analyte & Samples(s) Qualified:
Selenium
18C0324-07 AST-3 North (1-2)], B198629-BS1, B198629-BSDI
SW-846 8260B
Qualifications:
L 04
Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits Reported value for this
compound is likely to be biased on the low side
Analyte & Samples(s) Qualified
Chloromethane
18C0324-01 AST-1 Floor], 18C0324-02[AST-1 South], 18C0324-03[AST-1 North], 18C0324-04[AST-1 West], 18C0324-05[AST-1 East], 18C0324-06[AST-3 Floor],
18C0324-07 AST-3 North (1-2)], 18C0324-08[AST-3 North (3-4)], 18C0324-09[AST-3 South], 18C0324-10[AST-3 West], 18C0324-II[AST-3 East], B198462-BLKI,
B198462-BS1, B198462-BSD1
SW-846 8270D
Qualifications:
L-07
Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but the other is within limits RPD
between the two LFB/LCS results is within method specified criteria
Analyte & Samples(s) Qualified:
Pyridine
B 198559-BS 1
MS-09
Matrix spike recovery and/or matrix spike duplicate recovery outside of control limits Possibility of sample matrix effects that lead to a low
bias for reported result or non -homogeneous sample aliquots cannot be eliminated
Analyte & Samples(s) Qualified:
3,3-Dichlorobenzidfne
18C0324-07[AST-3 North (1-2)], B198559-MSI, B198559-MSDI
4-Chloroaniline
18C0324-07[AST-3 North (1-2)], B198559-MSI, B198559-MSDI
4-Nitroaniline
18C0324-07[AST-3 North (1-2)], B198559-MSI, B198559-MSDI
Aniline
18C0324-07[AST-3 North (1-2)], B198559-MSI, B198559-MSDI
Benzidine
18C0324-07[AST-3 North (1-2)], B198559-MSI, B198559-MSDI
Pyridine
18C0324-07[AST-3 North (1-2)], B198559-MSI, B198559-MSDI
MS-22
Either matrix spike or MS duplicate is outside of control limits, but the other is within limits RPD between the two MS/MSD results is
within method specified criteria
Analyte & Samples(s) Qualified:
3-Nitroaniline
B198559-MSI
R-06
Matrix spike duplicate RPD is outside of control limits Reduced precision is anticipated for reported result for this compound in this sample
Analyte & Samples(s) Qualified:
4-Chloroaniline
18C0324-07[AST-3 North (1-2)], B198559-MS1, B198559-MSDI
Page 8 of 94

con-testo
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
V-04
Initial calibration did not meet method specifications Compound was calibrated using a response factor where %RSD is outside of method
specified criteria Reported result is estimated
Analyte & Samples(s) Qualified:
Benzidine
18C0324-01 AST-1 Floor], 18C0324-02[AST-1 South], 18C0324-03[AST-1 North], 18C0324-04[AST-1 West], 18C0324-05[AST-1 East], 18C0324-06[AST-3 Floor],
18C0324-07 AST-3 North (1-2)], 18C0324-08[AST-3 North (3-4)], 18C0324-09[AST-3 South], 18C0324-10[AST-3 West], 18C0324-11[AST-3 East], B198559-BLKI,
13198559-13SI, B198559-BSDI, B198559-MS1, B198559-MSD1
V-05
Continuing calibration did not meet method specifications and was biased on the low side for this compound Reported result is estimated
Analyte & Samples(s) Qualified:
Aniline
18C0324-01 AST-1 Floor], 18C0324-02[AST-1 South], 18C0324-03[AST-1 North], 18C0324-04[AST-1 West], 18C0324-05[AST-1 East], 18C0324-06[AST-3 Floor],
18C0324-07 AST-3 North (1-2)], 18C0324-08[AST-3 North (3-4)], 18C0324-09[AST-3 South], 18C0324-10[AST-3 West], 18C0324-11[AST-3 East], B198559-BLKI,
13198559-13SI, B198559-BSDI, B198559-MS1, B198559-MSDI
Benzidine
18C0324-01 AST-1 Floor], 18C0324-02[AST-1 South], 18C0324-03[AST-1 North], 18C0324-04[AST-1 West], 18C0324-05[AST-1 East], 18C0324-06[AST-3 Floor],
18C0324-07 AST-3 North (1-2)], 18C0324-08[AST-3 North (3-4)], 18C0324-09[AST-3 South], 18C0324-10[AST-3 West], 18C0324-11[AST-3 East], B198559-BLKI,
B198559-BSI, B198559-BSDI, B198559-MS1, B198559-MSD1
Pyridine
18C0324-01 AST-1 Floor], 18C0324-02[AST-1 South], 18C0324-03[AST-1 North], 18C0324-04[AST-1 West], 18C0324-05[AST-1 East], 18C0324-06[AST-3 Floor],
18C0324-07 AST-3 North (1-2)], 18C0324-08[AST-3 North (3-4)], 18C0324-09[AST-3 South], 18C0324-10[AST-3 West], 18C0324-I1[AST-3 East], B198559-BLKI,
B198559-BS1, B198559-BSD1, B198559-MS1, B198559-MSD1
V-16
Response factor is less than method specified minimum acceptable value Reduced precision and accuracy may be associated with reported
result
Analyte & Samples(s) Qualified:
Pentachloronitrobenzene
18C0324-01 AST-1 Floor], 18C0324-02[AST-1 South], 18C0324-03[AST-1 North], 18C0324-04[AST-1 West], 18C0324-05[AST-1 East], 18C0324-06[AST-3 Floor],
18C0324-07 AST-3 North (1-2)], 18C0324-08[AST-3 North (3-4)], 18C0324-09[AST-3 South], 18C0324-10[AST-3 West], 18C0324-I1[AST-3 East], B198559-BLKI,
B198559-BS1. B198559-BSD1. B198559-MS1. B198559-MSD1
V-20
Continuing calibration did not meet method specifications and was biased on the high side Data validation is not affected since sample result
was "not detected" for this compound
Analyte & Samples(s) Qualified:
2-Nitroaniline
18C0324-01 AST-1 Floor], 18C0324-02[AST-1 South], 18C0324-03[AST-1 North], 18C0324-04[AST-1 West], 18C0324-05[AST-1 East], 18C0324-06[AST-3 Floor],
18C0324-07 AST-3 North (1-2)], 18C0324-08[AST-3 North (3-4)], 18C0324-09[AST-3 South], 18C0324-10[AST-3 West], 18C0324-11[AST-3 East], B198559-BLKI,
B198559-BS1, B198559-BSD1, B198559-MS1, B198559-MSD1
4-Nitrophenol
18C0324-01 AST-1 Floor], 18C0324-02[AST-1 South], 18C0324-03[AST-1 North], 18C0324-04[AST-1 West], 18C0324-05[AST-1 East], 18C0324-06[AST-3 Floor],
18C0324-07 AST-3 North (1-2)], 18C0324-08[AST-3 North (3-4)], 18C0324-09[AST-3 South], 18C0324-IO[AST-3 West], 18C0324-I1[AST-3 East], B198559-BLKI,
B198559-BS1, B198559-BSD1, B198559-MS1, B198559-MSD1
N-Nitrosodimethylamine
18C0324-01 AST-1 Floor], 18C0324-02[AST-1 South], 18C0324-03[AST-1 North], 18C0324-04[AST-1 West], 18C0324-05[AST-1 East], 18C0324-06[AST-3 Floor],
18C0324-07 AST-3 North (1-2)], 18C0324-08[AST-3 North (3-4)], 18C0324-09[AST-3 South], 18C0324-10[AST-3 West], 18C0324-11[AST-3 East], B198559-BLKI,
B198559-BS1, B198559-BSD1, B198559-MS1, B198559-MSD1
V-34
Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this compound Reported result is
estimated
Analyte & Samples(s) Qualified:
4-Chloroaniline
B198559-BLKI, 13198559-13SI, B198559-BSDI, B198559-MSI
Page 9 of 94

con-testo
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
SW-846 601OC/D SW-846 602OA/B
For NC, Metals methods SW-846 6010D and SW-846 6020B are followed, and for all other states methods SW-846 6010C and SW-846 6020A are followed
SW-846 8015C
Gasoline Range Organics (2-Methylpentane through 1,2,4-Trimethylbenzene) is quantitated against a calibration made with an unleaded gasoline composite standard
Diesel Range Organics (C 10-C28) is quantitated against a calibration made with a #2 fuel oil standard
The results of analyses reported only relate to samples submitted to the Con -Test Analytical Laboratory for testing
I certify that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete
4't� VWWL"�(_�
Lisa A Worthington
Project Manager
Page 10 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 Floor Sampled: 3/5/2018 10:15
Sample ID: 18C0324-01
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
0 083
0 019
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Acrylonitrile
ND
00050
00021
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
tert-Amyl Methyl Ether (TAME)
ND
000083
000058
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Benzene
ND
00017
000058
mg/Kg dry
1
SW 846 8260B
3/8/18
3/8/18 8:03
MFF
Bromobenzene
ND
00017
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Bromochloromethane
ND
00017
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Bromodichloromethane
ND
00017
000050
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Bromoform
ND
00017
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Bromomethane
ND
00083
00035
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
2-Butanone (MEK)
ND
0 033
0 015
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
tert-Butyl Alcohol (TBA)
ND
0 033
0 017
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
n-Butylbenzene
ND
00017
000058
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
sec-Butylbenzene
ND
00017
000083
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
tert-Butylbenzene
ND
00017
000075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
000083
000050
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Carbon Disulfide
ND
00050
00036
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Carbon Tetrachloride
ND
00017
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Chlorobenzene
ND
00017
000058
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Chlorodibromomethane
ND
00017
000058
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Chloroethane
ND
0 017
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Chloroform
ND
00033
000058
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Chloromethane
ND
00083
00053
mg/Kg dry
1 L-04
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
2-Chlorotoluene
ND
00017
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
4-Chlorotoluene
ND
00017
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
00017
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1,2-Dibromoethane (EDB)
ND
00017
000083
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Dibromomethane
ND
00017
000050
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1,2-Dichlorobenzene
ND
00017
000058
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1,3-Dichlorobenzene
ND
00017
000058
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1,4-Dichlorobenzene
ND
00017
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
trans-1,4-Dichloro-2-butene
ND
00033
00017
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Dichlorodifluoromethane (Freon 12)
ND
0 017
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1,1-Dichloroethane
ND
00017
000058
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1,2-Dichloroethane
ND
00017
00011
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1,1-Dichloroethylene
ND
00033
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
cis-1,2-Dichloroethylene
ND
00017
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
trans-1,2-Dichloroethylene
ND
00017
000075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1,2-Dichloropropane
ND
00017
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1,3-Dichloropropane
ND
000083
000058
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
2,2-Dichloropropane
ND
00017
000075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1, 1 -Dichloropropene
ND
00017
000075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
cis-1,3-Dichloropropene
ND
000083
000058
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
trans-1,3-Dichloropropene
ND
000083
000058
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Diethyl Ether
ND
0 017
00015
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Page 11 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 Floor Sampled: 3/5/2018 10:15
Samnle ID: 18C0324-01
Samnle Matrix: Soil
Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPE)
ND
000083
000050
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1,4-Dioxane
ND
0 083
0 048
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Ethanol
ND
0 17
0 033
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Ethylbenzene
ND
00017
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Hexachlorobutadiene
ND
00017
000083
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8 03
MFF
2-Hexanone (MBK)
ND
0 017
00090
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Isopropylbenzene (Cumene)
ND
00017
000058
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
p-Isopropyholuene (p-Cymene)
ND
00017
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Methyl tert-Butyl Ether (MTBE)
ND
00033
000075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Methylene Chloride
ND
0 017
00059
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
4-Methyl-2-pentanone (MIBK)
ND
0 017
00063
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Naphthalene
ND
00033
000058
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
n-Propylbenzene
ND
00017
000058
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Styrene
ND
00017
000050
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1, 1, 1,2-Tetrachloroethane
ND
00017
00015
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1,1,2,2-Tetrachloroethane
ND
000083
000075
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Tetrachloroethylene
ND
00017
00011
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Tetrahydrofman
ND
00083
00018
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Toluene
ND
00017
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1,2,3-Trichlorobenzene
ND
00017
000050
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1,2,4-Trichlorobenzene
ND
00017
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1,3,5-Trichlorobenzene
ND
00017
000058
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1, 1, 1 -Trichloroethane
ND
00017
000083
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1,1,2-Trichloroethane
ND
00017
000099
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Trichloroethylene
ND
00017
000083
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Trichlorofluoromethane (Freon 11)
ND
00083
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1,2,3-Trichloropropane
ND
00017
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1, 1,2-Trichloro- 1,2,2-trifluoroethane
ND
00083
000075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
(Freon 113)
1,2,4-Trimethylbenzene
ND
00017
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
1,3,5-Trimethylbenzene
ND
00017
000050
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Vinyl Chloride
ND
00083
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
m+p Xylene
ND
00033
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
o-Xylene
ND
00017
000058
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:03
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
100
70-130
3/8/18 8:03
Toluene-d8
102
70-130
3/8/18 8:03
4-Bromofluorobenzene
102
70-130
3/8/18 8:03
Page 12 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 Floor Sampled: 3/5/2018 10:15
Samnle ID: 18C0324-01
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
0 19
0 058
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Acenaphthylene
ND
0 19
0 065
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Acetophenone
ND
039
0 077
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Aniline
ND
039
Oil
mg/Kg dry
1
V 05
SW 846 8270D
3/9/18
3/12/18 13:06
BGL
Anthracene
ND
0 19
0 056
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Benzidine
ND
076
049
mg/Kg dry
1
V-04, V-05
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Benzo(a)anthracene
ND
0 19
0 052
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Benzo(a)pyrene
ND
0 19
0 061
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Benzo(b)fluoranthene
ND
0 19
0 055
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Benzo(g,h,i)perylene
ND
0 19
0 086
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Benzo(k)fluoranthene
ND
0 19
0 061
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Benzoic Acid
ND
1 1
021
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Bis(2-chloroethoxy)methane
ND
039
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Bis(2-chloroethyl)ether
ND
039
0 077
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Bis(2-chloroisopropyl)ether
ND
039
0 084
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Bis(2-Ethylhexyl)phthalate
ND
039
0 15
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
4-Bromophenylphenylether
ND
039
0 065
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Butylbenzylphthalate
0 12
039
0 093
mg/Kg dry
I
J
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Carbazole
ND
0 19
0 050
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
4-Chloroaniline
ND
076
0 089
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
4-Chloro-3-methylphenol
ND
076
0 084
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
2-Chloronaphthalene
ND
039
0 073
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
2-Chlorophenol
ND
039
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
4-Chlorophenylphenylether
ND
039
0 065
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Chrysene
ND
0 19
0 061
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Dibenz(a,h)anthracene
ND
0 19
0 12
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Dibenzofman
ND
039
0 068
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Di-n-butylphthalate
ND
039
0 085
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
1,2-Dichlorobenzene
ND
039
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
1,3-Dichlorobenzene
ND
039
0 066
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
1,4-Dichlorobenzene
ND
039
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
3,3-Dichlorobenzidine
ND
0 19
0 060
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
2,4-Dichlorophenol
ND
039
0 066
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Diethylphthalate
ND
039
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
2,4-Dimethylphenol
ND
039
0 072
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Dimethylphthalate
ND
039
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
4,6-Dinitro-2-methylphenol
ND
039
037
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
2,4-Dinitrophenol
ND
076
022
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
2,4-Dinitrotoluene
ND
039
0 063
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
2,6-Dinitrotoluene
ND
039
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Di-n-octylphthalate
ND
039
020
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
1,2-Diphenylhydrazine (as Azobenzene)
ND
039
0 063
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Fluoranthene
ND
0 19
0 064
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Flumene
ND
0 19
0 063
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Page 13 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 Floor Sampled: 3/5/2018 10:15
Samnle ID: 18C0324-01
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
039
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Hexachlorobutadiene
ND
039
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Hexachlorocyclopentadiene
ND
039
0 082
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Hexachloroethane
ND
039
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Indeno(1,2,3-cd)pyrene
ND
0 19
0 14
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13 06
BGL
Isophorone
ND
039
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
1-Methylnaphthalene
ND
0 19
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
2-Methylnaphthalene
ND
0 19
0 068
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
2-Methylphenol
ND
039
0 097
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
3/4-Methylphenol
ND
039
0 12
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Naphthalene
ND
0 19
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
2-Nitroaniline
ND
039
0 065
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
3-Nitroaniline
ND
039
0 056
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
4-Nitroaniline
ND
039
0 065
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Nitrobenzene
ND
039
0 073
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
2-Nitrophenol
ND
039
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
4-Nitrophenol
ND
076
0 085
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
N-Nitrosodimethylamine
ND
039
025
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
N-Nitrosodiphenylamine
ND
039
0 080
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
N-Nitrosodi-n-propylamine
ND
039
0 080
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Pentachloronitrobenzene
ND
039
0 093
mg/Kg dry
1
V-16
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Pentachlorophenol
ND
039
0 094
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Phenanthrene
ND
0 19
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Phenol
ND
039
0 066
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Pyrene
ND
0 19
0 064
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Pyridine
ND
039
0 063
mg/Kg dry
1
V-05
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
1,2,4,5-Tetrachlorobenzene
ND
039
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
1,2,4-Trichlorobenzene
ND
039
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
2,4,5-Trichlorophenol
ND
039
0 088
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
2,4,6-Trichlorophenol
ND
039
0 065
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:06
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
569
30-130
3/12/18 13:06
Phenol-d6
575
30-130
3/12/18 13:06
Nitrobenzene-d5
790
30-130
3/12/18 13:06
2-Fluorobiphenyl
740
30-130
3/12/18 13:06
2,4,6-Tribromophenol
796
30-130
3/12/18 13:06
p-Terphenyl-dl4
809
30-130
3/12/18 13:06
Page 14 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 Floor Sampled: 3/5/2018 10:15
Samnle ID: 18C0324-01
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 870 % Wt 1
SM 2540G 3/8/18 3/8/18 19:26 DMP
Page 15 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 South Sampled: 3/5/2018 10:20
Sample ID: 18C0324-02
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
0 091
0 021
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Acrylonitrile
ND
00054
00023
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
tert-Amyl Methyl Ether (TAME)
ND
000091
000064
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Benzene
ND
00018
000064
mg/Kg dry
1
SW 846 8260B
3/8/18
3/8/18 8:30
MFF
Bromobenzene
ND
00018
000073
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Bromochloromethane
ND
00018
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Bromodichloromethane
ND
00018
000054
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Bromoform
ND
00018
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Bromomethane
ND
00091
00038
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
2-Butanone (MEK)
ND
0 036
0 016
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
tert-Butyl Alcohol (TBA)
ND
0 036
0 019
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
n-Butylbenzene
ND
00018
000064
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
sec-Butylbenzene
ND
00018
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
tert-Butylbenzene
ND
00018
000082
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
000091
000054
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Carbon Disulfide
ND
00054
00039
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Carbon Tetrachloride
ND
00018
000073
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Chlorobenzene
ND
00018
000064
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Chlorodibromomethane
ND
00018
000064
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Chloroethane
ND
0 018
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Chloroform
ND
00036
000064
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Chloromethane
ND
00091
00058
mg/Kg dry
1 L-04
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
2-Chlorotoluene
ND
00018
000073
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
4-Chlorotoluene
ND
00018
000073
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
00018
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1,2-Dibromoethane (EDB)
ND
00018
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Dibromomethane
ND
00018
000054
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1,2-Dichlorobenzene
ND
00018
000064
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1,3-Dichlorobenzene
ND
00018
000064
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1,4-Dichlorobenzene
ND
00018
000073
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
trans-1,4-Dichloro-2-butene
ND
00036
00019
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Dichlorodifluoromethane (Freon 12)
ND
0 018
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1,1-Dichloroethane
ND
00018
000064
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1,2-Dichloroethane
ND
00018
00012
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1,1-Dichloroethylene
ND
00036
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
cis-1,2-Dichloroethylene
ND
00018
000073
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
trans-1,2-Dichloroethylene
ND
00018
000082
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1,2-Dichloropropane
ND
00018
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1,3-Dichloropropane
ND
000091
000064
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
2,2-Dichloropropane
ND
00018
000082
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1, 1 -Dichloropropene
ND
00018
000082
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
cis-1,3-Dichloropropene
ND
000091
000064
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
trans-1,3-Dichloropropene
ND
000091
000064
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Diethyl Ether
ND
0 018
00016
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Page 16 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 South Sampled: 3/5/2018 10:20
Samnle ID: 18C0324-02
Samnle Matrix: Soil
Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPE)
ND
000091
000054
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1,4-Dioxane
ND
0 091
0 052
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Ethanol
ND
0 18
0 036
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Ethylbenzene
ND
00018
000073
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Hexachlorobutadiene
ND
00018
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 830
MFF
2-Hexanone (MBK)
ND
0 018
00099
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Isopropylbenzene (Cumene)
ND
00018
000064
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
p-Isopropyltoluene (p-Cymene)
ND
00018
000073
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Methyl tert-Butyl Ether (MTBE)
ND
00036
000082
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Methylene Chloride
ND
0 018
00064
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
4-Methyl-2-pentanone (MIBK)
ND
0 018
00069
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Naphthalene
ND
00036
000064
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
n-Propylbenzene
ND
00018
000064
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Styrene
ND
00018
000054
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1, 1, 1,2-Tetrachloroethane
ND
00018
00016
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1,1,2,2-Tetrachloroethane
ND
000091
000082
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Tetrachloroethylene
ND
00018
00012
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Tetrahydrofman
ND
00091
00020
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Toluene
ND
00018
000073
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1,2,3-Trichlorobenzene
ND
00018
000054
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1,2,4-Trichlorobenzene
ND
00018
000073
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1,3,5-Trichlorobenzene
ND
00018
000064
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1, 1, 1 -Trichloroethane
ND
00018
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1,1,2-Trichloroethane
ND
00018
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Trichloroethylene
ND
00018
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Trichlorofluoromethane (Freon 11)
ND
00091
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1,2,3-Trichloropropane
ND
00018
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1, 1,2-Trichloro- 1,2,2-trifluoroethane
ND
00091
000082
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
(Freon 113)
1,2,4-Trimethylbenzene
ND
00018
000073
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
1,3,5-Trimethylbenzene
ND
00018
000054
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Vinyl Chloride
ND
00091
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
m+p Xylene
ND
00036
00015
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
o-Xylene
ND
00018
000064
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:30
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
100
70-130
3/8/18 8:30
Toluene-d8
982
70-130
3/8/18 8:30
4-Bromofluorobenzene
100
70-130
3/8/18 8:30
Page 17 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 South Sampled: 3/5/2018 10:20
Samnle ID: 18C0324-02
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
020
0 060
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Acenaphthylene
ND
020
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Acetophenone
ND
040
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Aniline
ND
040
Oil
mg/Kg dry
1 V 05
SW 846 8270D
3/9/18
3/12/18 13:30
BGL
Anthracene
ND
020
0 057
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Benzidine
ND
077
050
mg/Kg dry
1 V-04, V-05
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Benzo(a)anthracene
ND
020
0 053
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Benzo(a)pyrene
ND
020
0 062
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Benzo(b)fluoranthene
ND
020
0 056
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Benzo(g,h,i)perylene
ND
020
0 088
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Benzo(k)fluoranthene
ND
020
0 062
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Benzoic Acid
ND
12
021
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Bis(2-chloroethoxy)methane
ND
040
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Bis(2-chloroethyl)ether
ND
040
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Bis(2-chloroisopropyl)ether
ND
040
0 085
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Bis(2-Ethylhexyl)phthalate
ND
040
0 15
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
4-Bromophenylphenylether
ND
040
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Butylbenzylphthalate
ND
040
0 095
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Carbazole
ND
020
0 052
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
4-Chloroaniline
ND
077
0 091
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
4-Chloro-3-methylphenol
ND
077
0 085
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
2-Chloronaphthalene
ND
040
0 075
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
2-Chlorophenol
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
4-Chlorophenylphenylether
ND
040
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Chrysene
ND
020
0 062
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Dibenz(a,h)anthracene
ND
020
0 12
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Dibenzofman
ND
040
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Di-n-butylphthalate
ND
040
0 087
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
1,2-Dichlorobenzene
ND
040
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
1,3-Dichlorobenzene
ND
040
0 068
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
1,4-Dichlorobenzene
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
3,3-Dichlorobenzidine
ND
020
0 061
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
2,4-Dichlorophenol
ND
040
0 068
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Diethylphthalate
ND
040
0 071
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
2,4-Dimethylphenol
ND
040
0 074
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Dimethylphthalate
ND
040
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
4,6-Dinitro-2-methylphenol
ND
040
038
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
2,4-Dinitrophenol
ND
077
023
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
2,4-Dinitrotoluene
ND
040
0 064
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
2,6-Dinitrotoluene
ND
040
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Di-n-octylphthalate
ND
040
021
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
1,2-Diphenylhydrazine (as Azobenzene)
ND
040
0 064
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Fluoranthene
ND
020
0 066
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Flumene
ND
020
0 064
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Page 18 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 South Sampled: 3/5/2018 10:20
Samnle ID: 18C0324-02
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
040
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Hexachlorobutadiene
ND
040
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Hexachlorocyclopentadiene
ND
040
0 084
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Hexachloroethane
ND
040
0 080
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Indeno(1,2,3-cd)pyrene
ND
020
0 14
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13 30
BGL
Isophorone
ND
040
0 077
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
1-Methylnaphthalene
ND
020
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
2-Methylnaphthalene
ND
020
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
2-Methylphenol
ND
040
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
3/4-Methylphenol
ND
040
0 13
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Naphthalene
ND
020
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
2-Nitroaniline
ND
040
0 067
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
3-Nitroaniline
ND
040
0 057
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
4-Nitroaniline
ND
040
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Nitrobenzene
ND
040
0 075
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
2-Nitrophenol
ND
040
Oil
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
4-Nitrophenol
ND
077
0 087
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
N-Nitrosodimethylamine
ND
040
025
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
N-Nitrosodiphenylamine
ND
040
0 082
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
N-Nitrosodi-n-propylamine
ND
040
0 082
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Pentachloronitrobenzene
ND
040
0 095
mg/Kg dry
1
V-16
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Pentachlorophenol
ND
040
0 096
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Phenanthrene
ND
020
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Phenol
ND
040
0 068
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Pyrene
ND
020
0 066
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Pyridine
ND
040
0 064
mg/Kg dry
1
V-05
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
1,2,4,5-Tetrachlorobenzene
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
1,2,4-Trichlorobenzene
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
2,4,5-Trichlorophenol
ND
040
0 090
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
2,4,6-Trichlorophenol
ND
040
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:30
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
54 7
30-130
3/12/18 13:30
Phenol-d6
534
30-130
3/12/18 13:30
Nitrobenzene-d5
769
30-130
3/12/18 13:30
2-Fluorobiphenyl
675
30-130
3/12/18 13:30
2,4,6-Tribromophenol
671
30-130
3/12/18 13:30
p-Terphenyl-dl4
71 1
30-130
3/12/18 13:30
Page 19 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 South Sampled: 3/5/2018 10:20
Samnle ID: 18C0324-02
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 854 % Wt 1
SM 2540G 3/8/18 3/8/18 19:27 DMP
Page 20 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 North Sampled: 3/5/2018 10:25
Sample ID: 18C0324-03
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
0 098
0 023
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Acrylonitrile
ND
00059
00024
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
tert-Amyl Methyl Ether (TAME)
ND
000098
000068
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Benzene
ND
00020
000068
mg/Kg dry
1
SW 846 8260B
3/8/18
3/8/18 8:57
MFF
Bromobenzene
ND
00020
000078
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Bromochloromethane
ND
00020
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Bromodichloromethane
ND
00020
000059
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Bromoform
ND
00020
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Bromomethane
ND
00098
00041
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
2-Butanone (MEK)
ND
0 039
0 017
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
tert-Butyl Alcohol (TBA)
ND
0 039
0 020
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
n-Butylbenzene
ND
00020
000068
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
sec-Butylbenzene
ND
00020
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
tert-Butylbenzene
ND
00020
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
000098
000059
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Carbon Disulfide
ND
00059
00042
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Carbon Tetrachloride
ND
00020
000078
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Chlorobenzene
ND
00020
000068
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Chlorodibromomethane
ND
00020
000068
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Chloroethane
ND
0 020
00015
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Chloroform
ND
00039
000068
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Chloromethane
ND
00098
00063
mg/Kg dry
1 L-04
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
2-Chlorotoluene
ND
00020
000078
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
4-Chlorotoluene
ND
00020
000078
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
00020
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1,2-Dibromoethane (EDB)
ND
00020
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Dibromomethane
ND
00020
000059
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1,2-Dichlorobenzene
ND
00020
000068
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1,3-Dichlorobenzene
ND
00020
000068
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1,4-Dichlorobenzene
ND
00020
000078
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
trans-1,4-Dichloro-2-butene
ND
00039
00021
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Dichlorodifluoromethane (Freon 12)
ND
0 020
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1,1-Dichloroethane
ND
00020
000068
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1,2-Dichloroethane
ND
00020
00013
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1,1-Dichloroethylene
ND
00039
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
cis-1,2-Dichloroethylene
ND
00020
000078
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
trans-1,2-Dichloroethylene
ND
00020
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1,2-Dichloropropane
ND
00020
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1,3-Dichloropropane
ND
000098
000068
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
2,2-Dichloropropane
ND
00020
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1, 1 -Dichloropropene
ND
00020
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
cis-1,3-Dichloropropene
ND
000098
000068
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
trans-1,3-Dichloropropene
ND
000098
000068
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Diethyl Ether
ND
0 020
00018
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Page 21 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 North Sampled: 3/5/2018 10:25
Samnle ID: 18C0324-03
Samnle Matrix: Soil
Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPE)
ND
0 00098
0 00059
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1,4-Dioxane
ND
0 098
0 056
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Ethanol
ND
020
0 039
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Ethylbenzene
ND
00020
000078
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Hexachlorobutadiene
ND
00020
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8 57
MFF
2-Hexanone (MBK)
ND
0 020
0 011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Isopropylbenzene (Cumene)
ND
00020
000068
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
p-Isopropyltoluene (p-Cymene)
ND
00020
000078
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Methyl tert-Butyl Ether (MTBE)
ND
00039
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Methylene Chloride
ND
0 020
00069
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
4-Methyl-2-pentanone (MIBK)
ND
0 020
00074
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Naphthalene
ND
00039
000068
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
n-Propylbenzene
ND
00020
000068
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Styrene
ND
00020
000059
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1, 1, 1,2-Tetrachloroethane
ND
00020
00018
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1,1,2,2-Tetrachloroethane
ND
000098
000088
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Tetrachloroethylene
ND
00020
00013
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Tetrahydrofman
ND
00098
00022
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Toluene
ND
00020
000078
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1,2,3-Trichlorobenzene
ND
00020
000059
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1,2,4-Trichlorobenzene
ND
00020
000078
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1,3,5-Trichlorobenzene
ND
00020
000068
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1, 1, 1 -Trichloroethane
ND
00020
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1,1,2-Trichloroethane
ND
00020
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Trichloroethylene
ND
00020
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Trichlorofluoromethane (Freon 11)
ND
00098
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1,2,3-Trichloropropane
ND
00020
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1, 1,2-Trichloro- 1,2,2-trifluoroethane
ND
00098
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
(Freon 113)
1,2,4-Trimethylbenzene
ND
00020
000078
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
1,3,5-Trimethylbenzene
ND
00020
000059
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Vinyl Chloride
ND
00098
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
m+p Xylene
ND
00039
00017
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
o-Xylene
ND
00020
000068
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 8:57
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
991
70-130
3/8/18 8:57
Toluene-d8
100
70-130
3/8/18 8:57
4-Bromofluorobenzene
102
70-130
3/8/18 8:57
Page 22 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 North Sampled: 3/5/2018 10:25
Samnle ID: 18C0324-03
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
020
0 060
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Acenaphthylene
ND
020
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Acetophenone
ND
040
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Aniline
ND
040
Oil
mg/Kg dry
1
V 05
SW 846 8270D
3/9/18
3/12/18 13:53
BGL
Anthracene
ND
020
0 057
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Benzidine
ND
077
050
mg/Kg dry
1
V-04, V-05
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Benzo(a)anthracene
ND
020
0 053
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Benzo(a)pyrene
ND
020
0 062
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Benzo(b)fluoranthene
ND
020
0 056
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Benzo(g,h,i)perylene
ND
020
0 088
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Benzo(k)fluoranthene
ND
020
0 062
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Benzoic Acid
027
12
021
mg/Kg dry
1
J
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Bis(2-chloroethoxy)methane
ND
040
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Bis(2-chloroethyl)ether
ND
040
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Bis(2-chloroisopropyl)ether
ND
040
0 085
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Bis(2-Ethylhexyl)phthalate
ND
040
0 15
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
4-Bromophenylphenylether
ND
040
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Butylbenzylphthalate
ND
040
0 095
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Carbazole
ND
020
0 052
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
4-Chloroaniline
ND
077
0 091
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
4-Chloro-3-methylphenol
ND
077
0 085
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
2-Chloronaphthalene
ND
040
0 075
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
2-Chlorophenol
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
4-Chlorophenylphenylether
ND
040
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Chrysene
ND
020
0 062
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Dibenz(a,h)anthracene
ND
020
0 12
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Dibenzofman
ND
040
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Di-n-butylphthalate
ND
040
0 087
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
1,2-Dichlorobenzene
ND
040
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
1,3-Dichlorobenzene
ND
040
0 068
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
1,4-Dichlorobenzene
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
3,3-Dichlorobenzidine
ND
020
0 061
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
2,4-Dichlorophenol
ND
040
0 068
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Diethylphthalate
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
2,4-Dimethylphenol
ND
040
0 074
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Dimethylphthalate
ND
040
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
4,6-Dinitro-2-methylphenol
ND
040
038
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
2,4-Dinitrophenol
ND
077
023
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
2,4-Dinitrotoluene
ND
040
0 064
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
2,6-Dinitrotoluene
ND
040
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Di-n-octylphthalate
ND
040
021
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
1,2-Diphenylhydrazine (as Azobenzene)
ND
040
0 064
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Fluoranthene
ND
020
0 066
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Flumene
ND
020
0 064
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Page 23 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 North Sampled: 3/5/2018 10:25
Samnle ID: 18C0324-03
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
040
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Hexachlorobutadiene
ND
040
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Hexachlorocyclopentadiene
ND
040
0 084
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Hexachloroethane
ND
040
0 080
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Indeno(1,2,3-cd)pyrene
ND
020
0 14
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13 53
BGL
Isophorone
ND
040
0 077
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
1-Methylnaphthalene
ND
020
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
2-Methylnaphthalene
ND
020
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
2-Methylphenol
ND
040
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
3/4-Methylphenol
ND
040
0 13
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Naphthalene
ND
020
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
2-Nitroaniline
ND
040
0 067
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
3-Nitroaniline
ND
040
0 057
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
4-Nitroaniline
ND
040
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Nitrobenzene
ND
040
0 075
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
2-Nitrophenol
ND
040
Oil
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
4-Nitrophenol
ND
077
0 087
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
N-Nitrosodimethylamine
ND
040
025
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
N-Nitrosodiphenylamine
ND
040
0 082
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
N-Nitrosodi-n-propylamine
ND
040
0 082
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Pentachloronitrobenzene
ND
040
0 095
mg/Kg dry
1
V-16
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Pentachlorophenol
ND
040
0 096
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Phenanthrene
ND
020
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Phenol
ND
040
0 068
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Pyrene
ND
020
0 066
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Pyridine
ND
040
0 064
mg/Kg dry
1
V-05
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
1,2,4,5-Tetrachlorobenzene
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
1,2,4-Trichlorobenzene
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
2,4,5-Trichlorophenol
ND
040
0 090
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
2,4,6-Trichlorophenol
ND
040
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 13:53
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
593
30-130
3/12/18 13:53
Phenol-d6
598
30-130
3/12/18 13:53
Nitrobenzene-d5
821
30-130
3/12/18 13:53
2-Fluorobiphenyl
766
30-130
3/12/18 13:53
2,4,6-Tribromophenol
80 9
30-130
3/12/18 13:53
p-Terphenyl-dl4
844
30-130
3/12/18 13:53
Page 24 of 94

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 North Sampled: 3/5/2018 10:25
Samnle ID: 18C0324-03
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 854 % Wt 1
SM 2540G 3/8/18 3/8/18 19:27 DMP
Page 25 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 West Sampled: 3/5/2018 10:30
Sample ID: 18C0324-04
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
Oil
0 026
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Acrylonitrile
ND
00065
00027
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
tert-Amyl Methyl Ether (TAME)
ND
00011
000076
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Benzene
ND
00022
000076
mg/Kg dry
1
SW 846 8260B
3/8/18
3/8/18 9:25
MFF
Bromobenzene
ND
00022
000087
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Bromochloromethane
ND
00022
00015
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Bromodichloromethane
ND
00022
000065
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Bromoform
ND
00022
00015
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Bromomethane
ND
0 011
00046
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
2-Butanone (MEK)
ND
0 044
0 019
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
tert-Butyl Alcohol (TBA)
ND
0 044
0 023
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
n-Butylbenzene
ND
00022
000076
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
sec-Butylbenzene
ND
00022
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
tert-Butylbenzene
ND
00022
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
00011
000065
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Carbon Disulfide
ND
00065
00047
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Carbon Tetrachloride
ND
00022
000087
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Chlorobenzene
ND
00022
000076
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Chlorodibromomethane
ND
00022
000076
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Chloroethane
ND
0 022
00016
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Chloroform
ND
00044
000076
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Chloromethane
ND
0 011
00070
mg/Kg dry
1 L-04
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
2-Chlorotoluene
ND
00022
000087
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
4-Chlorotoluene
ND
00022
000087
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
00022
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1,2-Dibromoethane (EDB)
ND
00022
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Dibromomethane
ND
00022
000065
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1,2-Dichlorobenzene
ND
00022
000076
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1,3-Dichlorobenzene
ND
00022
000076
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1,4-Dichlorobenzene
ND
00022
000087
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
trans-1,4-Dichloro-2-butene
ND
00044
00023
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Dichlorodifluoromethane (Freon 12)
ND
0 022
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1,1-Dichloroethane
ND
00022
000076
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1,2-Dichloroethane
ND
00022
00014
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1,1-Dichloroethylene
ND
00044
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
cis-1,2-Dichloroethylene
ND
00022
000087
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
trans-1,2-Dichloroethylene
ND
00022
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1,2-Dichloropropane
ND
00022
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1,3-Dichloropropane
ND
00011
000076
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
2,2-Dichloropropane
ND
00022
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1, 1 -Dichloropropene
ND
00022
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
cis-1,3-Dichloropropene
ND
00011
000076
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
trans-1,3-Dichloropropene
ND
00011
000076
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Diethyl Ether
ND
0 022
00020
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Page 26 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 West Sampled: 3/5/2018 10:30
Samnle ID: 18C0324-04
Samnle Matrix: Soil
Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPE)
ND
00011
000065
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1,4-Dioxane
ND
Oil
0 063
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Ethanol
ND
022
0 044
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Ethylbenzene
ND
00022
000087
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Hexachlorobutadiene
ND
00022
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 925
MFF
2-Hexanone (MBK)
ND
0 022
0 012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Isopropylbenzene (Cumene)
ND
00022
000076
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
p-Isopropyholuene (p-Cymene)
ND
00022
000087
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Methyl tert-Butyl Ether (MTBE)
ND
00044
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Methylene Chloride
ND
0 022
00077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
4-Methyl-2-pentanone (MIBK)
ND
0 022
00083
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Naphthalene
ND
00044
000076
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
n-Propylbenzene
ND
00022
000076
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Styrene
ND
00022
000065
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1, 1, 1,2-Tetrachloroethane
ND
00022
00020
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1,1,2,2-Tetrachloroethane
ND
00011
000098
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Tetrachloroethylene
ND
00022
00014
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Tetrahydrofman
ND
0 011
00024
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Toluene
ND
00022
000087
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1,2,3-Trichlorobenzene
ND
00022
000065
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1,2,4-Trichlorobenzene
ND
00022
000087
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1,3,5-Trichlorobenzene
ND
00022
000076
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1, 1, 1 -Trichloroethane
ND
00022
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1,1,2-Trichloroethane
ND
00022
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Trichloroethylene
ND
00022
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Trichlorofluoromethane (Freon 11)
ND
0 011
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1,2,3-Trichloropropane
ND
00022
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1, 1,2-Trichloro- 1,2,2-trifluoroethane
ND
0 011
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
(Freon 113)
1,2,4-Trimethylbenzene
ND
00022
000087
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
1,3,5-Trimethylbenzene
ND
00022
000065
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Vinyl Chloride
ND
0 011
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
m+p Xylene
ND
00044
00019
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
o-Xylene
ND
00022
000076
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:25
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
982
70-130
3/8/18 9:25
Toluene-d8
101
70-130
3/8/18 9:25
4-Bromofluorobenzene
102
70-130
3/8/18 9:25
Page 27 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 West Sampled: 3/5/2018 10:30
Samnle ID: 18C0324-04
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
0 19
0 057
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Acenaphthylene
ND
0 19
0 064
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Acetophenone
ND
038
0 075
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Aniline
ND
038
Oil
mg/Kg dry
1 V 05
SW 846 8270D
3/9/18
3/12/18 14:16
BGL
Anthracene
ND
0 19
0 055
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Benzidine
ND
074
047
mg/Kg dry
1 V-04, V-05
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Benzo(a)anthracene
ND
0 19
0 050
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Benzo(a)pyrene
ND
0 19
0 059
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Benzo(b)fluoranthene
ND
0 19
0 054
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Benzo(g,h,i)perylene
ND
0 19
0 084
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Benzo(k)fluoranthene
ND
0 19
0 059
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Benzoic Acid
ND
1 1
020
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Bis(2-chloroethoxy)methane
ND
038
0 073
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Bis(2-chloroethyl)ether
ND
038
0 075
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Bis(2-chloroisopropyl)ether
ND
038
0 082
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Bis(2-Ethylhexyl)phthalate
ND
038
0 15
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
4-Bromophenylphenylether
ND
038
0 064
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Butylbenzylphthalate
ND
038
0 091
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Carbazole
ND
0 19
0 049
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
4-Chloroaniline
ND
074
0 087
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
4-Chloro-3-methylphenol
ND
074
0 082
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
2-Chloronaphthalene
ND
038
0 072
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
2-Chlorophenol
ND
038
0 068
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
4-Chlorophenylphenylether
ND
038
0 064
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Chrysene
ND
0 19
0 059
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Dibenz(a,h)anthracene
ND
0 19
0 12
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Dibenzofman
ND
038
0 066
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Di-n-butylphthalate
ND
038
0 083
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
1,2-Dichlorobenzene
ND
038
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
1,3-Dichlorobenzene
ND
038
0 065
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
1,4-Dichlorobenzene
ND
038
0 068
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
3,3-Dichlorobenzidine
ND
0 19
0 058
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
2,4-Dichlorophenol
ND
038
0 065
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Diethylphthalate
ND
038
0 068
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
2,4-Dimethylphenol
ND
038
0 070
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Dimethylphthalate
ND
038
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
4,6-Dinitro-2-methylphenol
ND
038
036
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
2,4-Dinitrophenol
ND
074
022
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
2,4-Dinitrotoluene
ND
038
0 061
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
2,6-Dinitrotoluene
ND
038
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Di-n-octylphthalate
ND
038
020
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
1,2-Diphenylhydrazine (as Azobenzene)
ND
038
0 061
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Fluoranthene
ND
0 19
0 063
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Flumene
ND
0 19
0 061
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Page 28 of 94

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 West Sampled: 3/5/2018 10:30
Samnle ID: 18C0324-04
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
038
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Hexachlorobutadiene
ND
038
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Hexachlorocyclopentadiene
ND
038
0 080
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Hexachloroethane
ND
038
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Indeno(1,2,3-cd)pyrene
ND
0 19
0 14
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14 16
BGL
Isophorone
ND
038
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
1-Methylnaphthalene
ND
0 19
0 073
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
2-Methylnaphthalene
ND
0 19
0 066
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
2-Methylphenol
ND
038
0 095
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
3/4-Methylphenol
ND
038
0 12
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Naphthalene
ND
0 19
0 097
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
2-Nitroaniline
ND
038
0 064
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
3-Nitroaniline
ND
038
0 055
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
4-Nitroaniline
ND
038
0 064
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Nitrobenzene
ND
038
0 072
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
2-Nitrophenol
ND
038
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
4-Nitrophenol
ND
074
0 083
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
N-Nitrosodimethylamine
ND
038
024
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
N-Nitrosodiphenylamine
ND
038
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
N-Nitrosodi-n-propylamine
ND
038
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Pentachloronitrobenzene
ND
038
0 091
mg/Kg dry
1
V-16
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Pentachlorophenol
ND
038
0 092
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Phenanthrene
ND
0 19
0 098
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Phenol
ND
038
0 065
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Pyrene
ND
0 19
0 063
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Pyridine
ND
038
0 061
mg/Kg dry
1
V-05
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
1,2,4,5-Tetrachlorobenzene
ND
038
0 068
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
1,2,4-Trichlorobenzene
ND
038
0 068
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
2,4,5-Trichlorophenol
ND
038
0 086
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
2,4,6-Trichlorophenol
ND
038
0 064
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:16
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
596
30-130
3/12/18 14:16
Phenol-d6
608
30-130
3/12/18 14:16
Nitrobenzene-d5
869
30-130
3/12/18 14:16
2-Fluorobiphenyl
814
30-130
3/12/18 14:16
2,4,6-Tribromophenol
84 6
30-130
3/12/18 14:16
p-Terphenyl-dl4
88 8
30-130
3/12/18 14:16
Page 29 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 West Sampled: 3/5/2018 10:30
Samnle ID: 18C0324-04
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 886 % Wt 1
SM 2540G 3/8/18 3/8/18 19:27 DMP
Page 30 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 East Sampled: 3/5/2018 10:35
Sample ID: 18C0324-05
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
0 10
0 024
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Acrylonitrile
ND
00062
00026
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
tert-Amyl Methyl Ether (TAME)
ND
00010
000072
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Benzene
ND
00021
000072
mg/Kg dry
1
SW 846 8260B
3/8/18
3/8/18 9:52
MFF
Bromobenzene
ND
00021
000082
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Bromochloromethane
ND
00021
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Bromodichloromethane
ND
00021
000062
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Bromoform
ND
00021
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Bromomethane
ND
0 010
00043
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
2-Butanone (MEK)
ND
0 041
0 018
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
tert-Butyl Alcohol (TBA)
ND
0 041
0 021
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
n-Butylbenzene
ND
00021
000072
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
sec-Butylbenzene
ND
00021
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
tert-Butylbenzene
ND
00021
000092
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
00010
000062
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Carbon Disulfide
ND
00062
00044
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Carbon Tetrachloride
ND
00021
000082
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Chlorobenzene
ND
00021
000072
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Chlorodibromomethane
ND
00021
000072
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Chloroethane
ND
0 021
00015
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Chloroform
ND
00041
000072
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Chloromethane
ND
0 010
00066
mg/Kg dry
1 L-04
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
2-Chlorotoluene
ND
00021
000082
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
4-Chlorotoluene
ND
00021
000082
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
00021
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1,2-Dibromoethane (EDB)
ND
00021
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Dibromomethane
ND
00021
000062
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1,2-Dichlorobenzene
ND
00021
000072
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1,3-Dichlorobenzene
ND
00021
000072
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1,4-Dichlorobenzene
ND
00021
000082
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
trans-1,4-Dichloro-2-butene
ND
00041
00022
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Dichlorodifluoromethane (Freon 12)
ND
0 021
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1,1-Dichloroethane
ND
00021
000072
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1,2-Dichloroethane
ND
00021
00013
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1,1-Dichloroethylene
ND
00041
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
cis-1,2-Dichloroethylene
ND
00021
000082
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
trans-1,2-Dichloroethylene
ND
00021
000092
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1,2-Dichloropropane
ND
00021
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1,3-Dichloropropane
ND
00010
000072
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
2,2-Dichloropropane
ND
00021
000092
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1, 1 -Dichloropropene
ND
00021
000092
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
cis-1,3-Dichloropropene
ND
00010
000072
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
trans-1,3-Dichloropropene
ND
00010
000072
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Diethyl Ether
ND
0 021
00018
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Page 31 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 East Sampled: 3/5/2018 10:35
Samnle ID: 18C0324-05
Samnle Matrix: Soil
Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPE)
ND
00010
000062
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1,4-Dioxane
ND
0 10
0 059
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Ethanol
ND
021
0 041
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Ethylbenzene
ND
00021
000082
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Hexachlorobutadiene
ND
00021
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 952
MFF
2-Hexanone (MBK)
ND
0 021
0 011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Isopropylbenzene (Cumene)
ND
00021
000072
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
p-Isopropyholuene (p-Cymene)
ND
00021
000082
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Methyl tert-Butyl Ether (MTBE)
ND
00041
000092
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Methylene Chloride
ND
0 021
00073
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
4-Methyl-2-pentanone (MIBK)
ND
0 021
00078
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Naphthalene
ND
00041
000072
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
n-Propylbenzene
ND
00021
000072
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Styrene
ND
00021
000062
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1, 1, 1,2-Tetrachloroethane
ND
00021
00018
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1,1,2,2-Tetrachloroethane
ND
00010
000092
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Tetrachloroethylene
ND
00021
00013
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Tetrahydrofman
ND
0 010
00023
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Toluene
ND
00021
000082
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1,2,3-Trichlorobenzene
ND
00021
000062
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1,2,4-Trichlorobenzene
ND
00021
000082
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1,3,5-Trichlorobenzene
ND
00021
000072
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1, 1, 1 -Trichloroethane
ND
00021
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1,1,2-Trichloroethane
ND
00021
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Trichloroethylene
ND
00021
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Trichlorofluoromethane (Freon 11)
ND
0 010
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1,2,3-Trichloropropane
ND
00021
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1, 1,2-Trichloro- 1,2,2-trifluoroethane
ND
0 010
000092
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
(Freon 113)
1,2,4-Trimethylbenzene
ND
00021
000082
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
1,3,5-Trimethylbenzene
ND
00021
000062
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Vinyl Chloride
ND
0 010
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
m+p Xylene
ND
00041
00017
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
o-Xylene
ND
00021
000072
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 9:52
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
992
70-130
3/8/18 9:52
Toluene-d8
994
70-130
3/8/18 9:52
4-Bromofluorobenzene
101
70-130
3/8/18 9:52
Page 32 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 East Sampled: 3/5/2018 10:35
Samnle ID: 18C0324-05
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
020
0 060
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Acenaphthylene
ND
020
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Acetophenone
ND
040
0 079
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Aniline
ND
040
Oil
mg/Kg dry
1 V 05
SW 846 8270D
3/9/18
3/12/18 14:38
BGL
Anthracene
ND
020
0 058
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Benzidine
ND
078
050
mg/Kg dry
1 V-04, V-05
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Benzo(a)anthracene
ND
020
0 053
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Benzo(a)pyrene
ND
020
0 063
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Benzo(b)fluoranthene
ND
020
0 057
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Benzo(g,h,i)perylene
ND
020
0 089
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Benzo(k)fluoranthene
ND
020
0 063
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Benzoic Acid
ND
12
021
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Bis(2-chloroethoxy)methane
ND
040
0 077
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Bis(2-chloroethyl)ether
ND
040
0 079
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Bis(2-chloroisopropyl)ether
ND
040
0 086
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Bis(2-Ethylhexyl)phthalate
ND
040
0 16
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
4-Bromophenylphenylether
ND
040
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Butylbenzylphthalate
ND
040
0 096
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Carbazole
ND
020
0 052
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
4-Chloroaniline
ND
078
0 092
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
4-Chloro-3-methylphenol
ND
078
0 086
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
2-Chloronaphthalene
ND
040
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
2-Chlorophenol
ND
040
0 072
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
4-Chlorophenylphenylether
ND
040
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Chrysene
ND
020
0 063
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Dibenz(a,h)anthracene
ND
020
0 12
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Dibenzofman
ND
040
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Di-n-butylphthalate
ND
040
0 088
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
1,2-Dichlorobenzene
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
1,3-Dichlorobenzene
ND
040
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
1,4-Dichlorobenzene
ND
040
0 072
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
3,3-Dichlorobenzidine
ND
020
0 062
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
2,4-Dichlorophenol
ND
040
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Diethylphthalate
ND
040
0 072
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
2,4-Dimethylphenol
ND
040
0 075
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Dimethylphthalate
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
4,6-Dinitro-2-methylphenol
ND
040
038
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
2,4-Dinitrophenol
ND
078
023
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
2,4-Dinitrotoluene
ND
040
0 065
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
2,6-Dinitrotoluene
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Di-n-octylphthalate
ND
040
021
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
1,2-Diphenylhydrazine (as Azobenzene)
ND
040
0 065
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Fluoranthene
ND
020
0 066
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Flumene
ND
020
0 065
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Page 33 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 East Sampled: 3/5/2018 10:35
Samnle ID: 18C0324-05
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Hexachlorobutadiene
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Hexachlorocyclopentadiene
ND
040
0 085
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Hexachloroethane
ND
040
0 080
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Indeno(1,2,3-cd)pyrene
ND
020
0 14
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14 38
BGL
Isophorone
ND
040
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
1-Methylnaphthalene
ND
020
0 077
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
2-Methylnaphthalene
ND
020
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
2-Methylphenol
ND
040
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
3/4-Methylphenol
ND
040
0 13
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Naphthalene
ND
020
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
2-Nitroaniline
ND
040
0 067
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
3-Nitroaniline
ND
040
0 058
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
4-Nitroaniline
ND
040
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Nitrobenzene
ND
040
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
2-Nitrophenol
ND
040
Oil
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
4-Nitrophenol
ND
078
0 088
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
N-Nitrosodimethylamine
ND
040
025
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
N-Nitrosodiphenylamine
ND
040
0 083
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
N-Nitrosodi-n-propylamine
ND
040
0 083
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Pentachloronitrobenzene
ND
040
0 096
mg/Kg dry
1
V-16
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Pentachlorophenol
ND
040
0 097
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Phenanthrene
ND
020
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Phenol
ND
040
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Pyrene
ND
020
0 066
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Pyridine
ND
040
0 065
mg/Kg dry
1
V-05
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
1,2,4,5-Tetrachlorobenzene
ND
040
0 072
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
1,2,4-Trichlorobenzene
ND
040
0 072
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
2,4,5-Trichlorophenol
ND
040
0 091
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
2,4,6-Trichlorophenol
ND
040
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 14:38
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
609
30-130
3/12/18 14:38
Phenol-d6
606
30-130
3/12/18 14:38
Nitrobenzene-d5
865
30-130
3/12/18 14:38
2-Fluorobiphenyl
784
30-130
3/12/18 14:38
2,4,6-Tribromophenol
796
30-130
3/12/18 14:38
p-Terphenyl-dl4
824
30-130
3/12/18 14:38
Page 34 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-1 East Sampled: 3/5/2018 10:35
Samnle ID: 18C0324-05
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 845 % Wt 1
SM 2540G 3/8/18 3/8/18 19:27 DMP
Page 35 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 Floor Sampled: 3/5/2018 11:00
Sample ID: 18C0324-06
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
0 12
0 029
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Acrylonitrile
ND
00073
00031
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
tert-Amyl Methyl Ether (TAME)
ND
00012
000085
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Benzene
ND
00024
000085
mg/Kg dry
1
SW 846 8260B
3/8/18
3/8/18 10:21
MFF
Bromobenzene
ND
00024
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Bromochloromethane
ND
00024
00017
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Bromodichloromethane
ND
00024
000073
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Bromoform
ND
00024
00017
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Bromomethane
ND
0 012
00051
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
2-Butanone (MEK)
ND
0 049
0 021
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
tert-Butyl Alcohol (TBA)
ND
0 049
0 026
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
n-Butylbenzene
ND
00024
000085
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
sec-Butylbenzene
ND
00024
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
tert-Butylbenzene
ND
00024
00011
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
00012
000073
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Carbon Disulfide
ND
00073
00053
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Carbon Tetrachloride
ND
00024
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Chlorobenzene
ND
00024
000085
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Chlorodibromomethane
ND
00024
000085
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Chloroethane
ND
0 024
00018
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Chloroform
ND
00049
000085
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Chloromethane
ND
0 012
00078
mg/Kg dry
1 L-04
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
2-Chlorotoluene
ND
00024
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
4-Chlorotoluene
ND
00024
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
00024
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1,2-Dibromoethane (EDB)
ND
00024
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Dibromomethane
ND
00024
000073
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1,2-Dichlorobenzene
ND
00024
000085
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1,3-Dichlorobenzene
ND
00024
000085
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1,4-Dichlorobenzene
ND
00024
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
trans-1,4-Dichloro-2-butene
ND
00049
00026
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Dichlorodifluoromethane (Freon 12)
ND
0 024
00016
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1,1-Dichloroethane
ND
00024
000085
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1,2-Dichloroethane
ND
00024
00016
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1,1-Dichloroethylene
ND
00049
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
cis-1,2-Dichloroethylene
ND
00024
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
trans-1,2-Dichloroethylene
ND
00024
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1,2-Dichloropropane
ND
00024
00016
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1,3-Dichloropropane
ND
00012
000085
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
2,2-Dichloropropane
ND
00024
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1, 1 -Dichloropropene
ND
00024
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
cis-1,3-Dichloropropene
ND
00012
000085
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
trans-1,3-Dichloropropene
ND
00012
000085
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Diethyl Ether
ND
0 024
00022
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Page 36 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 Floor Sampled: 3/5/2018 11:00
Samnle ID: 18C0324-06
Samnle Matrix: Soil
Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPS)
ND
00012
000073
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1,4-Dioxane
ND
0 12
0 070
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Ethanol
ND
024
0 049
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Ethylbenzene
ND
00024
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Hexachlorobutadiene
ND
00024
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 1021
MFF
2-Hexanone (MBK)
ND
0 024
0 013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Isopropylbenzene (Cumene)
ND
00024
000085
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
p-Isopropyholuene (p-Cymene)
ND
00024
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Methyl tert-Butyl Ether (MTBE)
ND
00049
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Methylene Chloride
ND
0 024
00087
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
4-Methyl-2-pentanone (MIBK)
ND
0 024
00093
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Naphthalene
ND
00049
000085
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
n-Propylbenzene
ND
00024
000085
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Styrene
ND
00024
000073
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1, 1, 1,2-Tetrachloroethane
ND
00024
00022
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1,1,2,2-Tetrachloroethane
ND
00012
00011
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Tetrachloroethylene
ND
00024
00016
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Tetrahydrofman
ND
0 012
00027
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Toluene
ND
00024
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1,2,3-Trichlorobenzene
ND
00024
000073
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1,2,4-Trichlorobenzene
ND
00024
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1,3,5-Trichlorobenzene
ND
00024
000085
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1, 1, 1 -Trichloroethane
ND
00024
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1,1,2-Trichloroethane
ND
00024
00015
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Trichloroethylene
ND
00024
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Trichlorofluoromethane (Freon 11)
ND
0 012
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1,2,3-Trichloropropane
ND
00024
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1, 1,2-Trichloro- 1,2,2-trifluoroethane
ND
0 012
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
(Freon 113)
1,2,4-Trimethylbenzene
ND
00024
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
1,3,5-Trimethylbenzene
ND
00024
000073
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Vinyl Chloride
ND
0 012
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
m+p Xylene
ND
00049
00021
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
o-Xylene
ND
00024
000085
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:21
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
100
70-130
3/8/18 10:21
Toluene-d8
978
70-130
3/8/18 10:21
4-Bromofluorobenzenc
102
70-130
3/8/18 10:21
Page 37 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 Floor Sampled: 3/5/2018 11:00
Samnle ID: 18C0324-06
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
022
0 065
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Acenaphthylene
ND
022
0 073
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Acetophenone
ND
043
0 085
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Aniline
ND
043
0 12
mg/Kg dry
1 V 05
SW 846 8270D
3/9/18
3/12/18 15:01
BGL
Anthracene
ND
022
0 062
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Benzidine
ND
0 84
054
mg/Kg dry
1 V-04, V-05
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Benzo(a)anthracene
ND
022
0 057
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Benzo(a)pyrene
ND
022
0 068
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Benzo(b)fluoranthene
ND
022
0 061
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Benzo(g,h,i)perylene
ND
022
0 096
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Benzo(k)fluoranthene
ND
022
0 068
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Benzoic Acid
ND
13
023
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Bis(2-chloroethoxy)methane
ND
043
0 083
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Bis(2-chloroethyl)ether
ND
043
0 085
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Bis(2-chloroisopropyl)ether
ND
043
0 093
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Bis(2-Ethylhexyl)phthalate
ND
043
0 17
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
4-Bromophenylphenylether
ND
043
0 073
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Butylbenzylphthalate
ND
043
0 10
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Carbazole
ND
022
0 056
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
4-Chloroaniline
ND
0 84
0 099
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
4-Chloro-3-methylphenol
ND
0 84
0 093
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
2-Chloronaphthalene
ND
043
0 082
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
2-Chlorophenol
ND
043
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
4-Chlorophenylphenylether
ND
043
0 073
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Chrysene
ND
022
0 068
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Dibenz(a,h)anthracene
ND
022
0 13
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Dibenzofman
ND
043
0 075
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Di-n-butylphthalate
ND
043
0 094
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
1,2-Dichlorobenzene
ND
043
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
1,3-Dichlorobenzene
ND
043
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
1,4-Dichlorobenzene
ND
043
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
3,3-Dichlorobenzidine
ND
022
0 066
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
2,4-Dichlorophenol
ND
043
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Diethylphthalate
ND
043
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
2,4-Dimethylphenol
ND
043
0 080
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Dimethylphthalate
ND
043
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
4,6-Dinitro-2-methylphenol
ND
043
041
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
2,4-Dinitrophenol
ND
0 84
025
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
2,4-Dinitrotoluene
ND
043
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
2,6-Dinitrotoluene
ND
043
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Di-n-octylphthalate
ND
043
023
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
1,2-Diphenylhydrazine (as Azobenzene)
ND
043
0 070
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Fluoranthene
ND
022
0 071
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Flumene
ND
022
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Page 38 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 Floor Sampled: 3/5/2018 11:00
Samnle ID: 18C0324-06
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
043
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Hexachlorobutadiene
ND
043
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Hexachlorocyclopentadiene
ND
043
0 092
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Hexachloroethane
ND
043
0 087
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Indeno(1,2,3-cd)pyrene
ND
022
0 16
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15 01
BGL
Isophorone
ND
043
0 084
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
1-Methylnaphthalene
ND
022
0 083
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
2-Methylnaphthalene
ND
022
0 075
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
2-Methylphenol
ND
043
Oil
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
3/4-Methylphenol
ND
043
0 14
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Naphthalene
ND
022
Oil
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
2-Nitroaniline
ND
043
0 073
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
3-Nitroaniline
ND
043
0 062
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
4-Nitroaniline
ND
043
0 073
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Nitrobenzene
ND
043
0 082
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
2-Nitrophenol
ND
043
Oil
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
4-Nitrophenol
ND
0 84
0 094
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
N-Nitrosodimethylamine
ND
043
027
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
N-Nitrosodiphenylamine
ND
043
0 089
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
N-Nitrosodi-n-propylamine
ND
043
0 089
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Pentachloronitrobenzene
ND
043
0 10
mg/Kg dry
1
V-16
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Pentachlorophenol
ND
043
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Phenanthrene
ND
022
Oil
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Phenol
ND
043
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Pyrene
ND
022
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Pyridine
ND
043
0 070
mg/Kg dry
1
V-05
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
1,2,4,5-Tetrachlorobenzene
ND
043
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
1,2,4-Trichlorobenzene
ND
043
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
2,4,5-Trichlorophenol
ND
043
0 098
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
2,4,6-Trichlorophenol
ND
043
0 073
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:01
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
636
30-130
3/12/18 15:01
Phenol-d6
63 6
30-130
3/12/18 15:01
Nitrobenzene-d5
949
30-130
3/12/18 15:01
2-Fluorobiphenyl
78 5
30-130
3/12/18 15:01
2,4,6-Tribromophenol
82 8
30-130
3/12/18 15:01
p-Terphenyl-dl4
84 8
30-130
3/12/18 15:01
Page 39 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 Floor Sampled: 3/5/2018 11:00
Samnle ID: 18C0324-06
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 784 % Wt 1
SM 2540G 3/8/18 3/8/18 19:27 DMP
Page 40 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 North (1-2) Sampled: 3/5/2018 11:15
Sample ID: 18C0324-07
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
Oil
0 026
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Acrylonitrile
ND
00066
00028
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
tert-Amyl Methyl Ether (TAME)
ND
00011
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Benzene
ND
00022
000077
mg/Kg dry
1
SW 846 8260B
3/8/18
3/8/18 10:48
MFF
Bromobenzene
ND
00022
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Bromochloromethane
ND
00022
00015
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Bromodichloromethane
ND
00022
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Bromoform
ND
00022
00015
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Bromomethane
ND
0 011
00046
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
2-Butanone (MEK)
ND
0 044
0 019
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
tert-Butyl Alcohol (TBA)
ND
0 044
0 023
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
n-Butylbenzene
ND
00022
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
sec-Butylbenzene
ND
00022
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
tert-Butylbenzene
ND
00022
000099
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
00011
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Carbon Disulfide
ND
00066
00047
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Carbon Tetrachloride
ND
00022
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Chlorobenzene
ND
00022
000077
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Chlorodibromomethane
ND
00022
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Chloroethane
ND
0 022
00017
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Chloroform
ND
00044
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Chloromethane
ND
0 011
00071
mg/Kg dry
1 L-04
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
2-Chlorotoluene
ND
00022
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
4-Chlorotoluene
ND
00022
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
00022
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1,2-Dibromoethane (EDB)
ND
00022
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Dibromomethane
ND
00022
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1,2-Dichlorobenzene
ND
00022
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1,3-Dichlorobenzene
ND
00022
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1,4-Dichlorobenzene
ND
00022
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
trans-1,4-Dichloro-2-butene
ND
00044
00023
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Dichlorodifluoromethane (Freon 12)
ND
0 022
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1,1-Dichloroethane
ND
00022
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1,2-Dichloroethane
ND
00022
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1,1-Dichloroethylene
ND
00044
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
cis-1,2-Dichloroethylene
ND
00022
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
trans-1,2-Dichloroethylene
ND
00022
000099
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1,2-Dichloropropane
ND
00022
00014
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1,3-Dichloropropane
ND
00011
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
2,2-Dichloropropane
ND
00022
000099
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1, 1 -Dichloropropene
ND
00022
000099
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
cis-1,3-Dichloropropene
ND
00011
000077
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
trans-1,3-Dichloropropene
ND
00011
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Diethyl Ether
ND
0 022
00020
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Page 41 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 North (1-2) Sampled: 3/5/2018 11:15
Samnle ID: 18C0324-07
Samnle Matrix: Soil
Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPE)
ND
00011
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1,4-Dioxane
ND
Oil
0 063
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Ethanol
ND
022
0 044
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Ethylbenzene
ND
00022
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Hexachlorobutadiene
ND
00022
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 1048
MFF
2-Hexanone (MBK)
ND
0 022
0 012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Isopropylbenzene (Cumene)
ND
00022
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
p-Isopropyltoluene (p-Cymene)
ND
00022
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Methyl tert-Butyl Ether (MTBE)
ND
00044
000099
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Methylene Chloride
ND
0 022
00078
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
4-Methyl-2-pentanone (MIBK)
ND
0 022
00084
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Naphthalene
ND
00044
000077
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
n-Propylbenzene
ND
00022
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Styrene
ND
00022
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1, 1, 1,2-Tetrachloroethane
ND
00022
00020
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1,1,2,2-Tetrachloroethane
ND
00011
000099
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Tetrachloroethylene
ND
00022
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Tetrahydrofman
ND
0 011
00024
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Toluene
ND
00022
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1,2,3-Trichlorobenzene
ND
00022
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1,2,4-Trichlorobenzene
ND
00022
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1,3,5-Trichlorobenzene
ND
00022
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1, 1, 1 -Trichloroethane
ND
00022
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1,1,2-Trichloroethane
ND
00022
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Trichloroethylene
ND
00022
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Trichlorofluoromethane (Freon 11)
ND
0 011
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1,2,3-Trichloropropane
ND
00022
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1, 1,2-Trichloro- 1,2,2-trifluoroethane
ND
0 011
000099
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
(Freon 113)
1,2,4-Trimethylbenzene
ND
00022
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
1,3,5-Trimethylbenzene
ND
00022
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Vinyl Chloride
ND
0 011
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
m+p Xylene
ND
00044
00019
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
o-Xylene
ND
00022
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 10:48
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
100
70-130
3/8/18 10:48
Toluene-d8
990
70-130
3/8/18 10:48
4-Bromofluorobenzenc
998
70-130
3/8/18 10:48
Page 42 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 North (1-2) Sampled: 3/5/2018 11:15
Samnle ID: 18C0324-07
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
021
0 062
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Acenaphthylene
ND
021
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Acetophenone
ND
041
0 081
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Aniline
ND
041
0 12
mg/Kg dry
1
MS 09, V 05
SW 846 8270D
3/9/18
3/12/18 15:24
BGL
Anthracene
ND
021
0 060
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Benzidine
ND
080
0 52
mg/Kg dry
1
MS-09, V-04, V-05
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Benzo(a)anthracene
ND
021
0 055
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Benzo(a)pyrene
ND
021
0 064
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Benzo(b)fluoranthene
ND
021
0 058
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Benzo(g,h,i)perylene
ND
021
0 091
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Benzo(k)fluoranthene
ND
021
0 064
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Benzoic Acid
045
12
022
mg/Kg dry
1
J
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Bis(2-chloroethoxy)methane
ND
041
0 079
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Bis(2-chloroethyl)ether
ND
041
0 081
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Bis(2-chloroisopropyl)ether
ND
041
0 089
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Bis(2-Ethylhexyl)phthalate
ND
041
0 16
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
4-Bromophenylphenylether
ND
041
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Butylbenzylphthalate
ND
041
0 098
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Carbazole
ND
021
0 053
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
4-Chloroaniline
ND
0 80
0 095
mg/Kg dry
1
MS-09, R-06
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
4-Chloro-3-methylphenol
ND
0 80
0 089
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
2-Chloronaphthalene
ND
041
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
2-Chlorophenol
ND
041
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
4-Chlorophenylphenylether
ND
041
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Chrysene
ND
021
0 064
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Dibenz(a,h)anthracene
ND
021
0 13
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Dibenzofman
ND
041
0 072
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Di-n-butylphthalate
ND
041
0 090
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
1,2-Dichlorobenzene
ND
041
0 073
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
1,3-Dichlorobenzene
ND
041
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
1,4-Dichlorobenzene
ND
041
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
3,3-Dichlorobenzidine
ND
021
0 063
mg/Kg dry
1
MS-09
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
2,4-Dichlorophenol
ND
041
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Diethylphthalate
ND
041
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
2,4-Dimethylphenol
ND
041
0 077
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Dimethylphthalate
ND
041
0 073
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
4,6-Dinitro-2-methylphenol
ND
041
039
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
2,4-Dinitrophenol
ND
080
024
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
2,4-Dinitrotoluene
ND
041
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
2,6-Dinitrotoluene
ND
041
0 073
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Di-n-octylphthalate
ND
041
022
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
1,2-Diphenylhydrazine (as Azobenzene)
ND
041
0 067
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Fluoranthene
ND
021
0 068
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Flumene
ND
021
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Page 43 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 North (1-2) Sampled: 3/5/2018 11:15
Samnle ID: 18C0324-07
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
041
0 073
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Hexachlorobutadiene
ND
041
0 073
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Hexachlorocyclopentadiene
ND
041
0 087
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Hexachloroethane
ND
041
0 083
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Indeno(1,2,3-cd)pyrene
ND
021
0 15
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15 24
BGL
Isophorone
ND
041
0 080
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
1-Methylnaphthalene
ND
021
0 079
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
2-Methylnaphthalene
ND
021
0 072
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
2-Methylphenol
ND
041
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
3/4-Methylphenol
ND
041
0 13
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Naphthalene
ND
021
Oil
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
2-Nitroaniline
ND
041
0 069
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
3-Nitroaniline
ND
041
0 060
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
4-Nitroaniline
ND
041
0 069
mg/Kg dry
1
MS-09
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Nitrobenzene
ND
041
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
2-Nitrophenol
ND
041
Oil
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
4-Nitrophenol
ND
080
0 090
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
N-Nitrosodimethylamine
ND
041
026
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
N-Nitrosodiphenylamine
ND
041
0 085
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
N-Nitrosodi-n-propylamine
ND
041
0 085
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Pentachloronitrobenzene
ND
041
0 098
mg/Kg dry
1
V-16
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Pentachlorophenol
ND
041
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Phenanthrene
ND
021
Oil
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Phenol
ND
041
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Pyrene
ND
021
0 068
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Pyridine
ND
041
0 067
mg/Kg dry
1
MS-09, V-05
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
1,2,4,5-Tetrachlorobenzene
ND
041
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
1,2,4-Trichlorobenzene
ND
041
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
2,4,5-Trichlorophenol
ND
041
0 094
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
2,4,6-Trichlorophenol
ND
041
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:24
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
53 8
30-130
3/12/18 15:24
Phenol-d6
534
30-130
3/12/18 15:24
Nitrobenzene-d5
795
30-130
3/12/18 15:24
2-Fluorobiphenyl
656
30-130
3/12/18 15:24
2,4,6-Tribromophenol
774
30-130
3/12/18 15:24
p-Terphenyl-dl4
85 7
30-130
3/12/18 15:24
Page 44 of 94

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con-testo
CP
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 North (1-2) Sampled: 3/5/2018 11:15
Samnle ID: 18C0324-07
Samnle Matrix: Soil
Petroleum Hydrocarbons Analyses
Date Date/Time
Analyte Results RL DL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
Gasoline Range Organics (GRO) ND 12 12 mg/Kg dry 1 SW-846 8015C 3/12/18 3/12/18 17:01 EEH
Diesel Range Organics 1600 100 23 mg/Kg dry 10 SW-846 8015C 3/9/18 3/11/18 18:45 PJG
Surrogates % Recovery Recovery Limits Flag/Qual
1-Chloro-3-fluorobenzene 104 70-130 3/12/18 17:01
o-Terphenyl 718 40-140 3/11/18 18:45
Page 45 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 North (1-2) Sampled: 3/5/2018 11:15
Samnle ID: 18C0324-07
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 823 % Wt 1
SM 2540G 3/8/18 3/8/18 19:16 DMP
Page 46 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
Project Location: 3312 Watkins Rd
Date Received: 3/6/2018
Field Sample #: AST-3 North (1-2)
Samnle ID: 18C0324-07
Samnle Matrix: Soil
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Description:
Sampled: 3/5/2018 11:15
Work Order:
18C0324
TCLP - Metals Analyses
Date
Date/Time
Analyte
Results
RL DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Arsenic
ND
0 010 00080
mg/L
1
SW-846 601OC-D
3/12/18
3/12/18 18:41
QNW
Mercury
0 000059 0 00010 0 000034
mg/L
1 J
SW-846 7470A
3/12/18
3/12/18 11:59
EJB
Barium
022
0 050 00053
mg/L
1
SW-846 601OC-D
3/12/18
3/12/18 18:41
QNW
Cadmium
ND
00040 000090
mg/L
1
SW 846 6010C D
3/12/18
3/12/18 18:41
QNW
Chromium
ND
0 010 00061
mg/L
1
SW-846 601OC-D
3/12/18
3/12/18 18:41
QNW
Lead
0 14
0 010 00044
mg/L
1
SW-846 601OC-D
3/12/18
3/12/18 18:41
QNW
Selenium
ND
0 050 0 034
mg/L
1 L-02
SW-846 601OC-D
3/12/18
3/12/18 18:41
QNW
Silver
ND
00050 00049
mg/L
1
SW-846 601OC-D
3/12/18
3/13/18 13:12
QNW
Page 47 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 North (3-4) Sampled: 3/5/2018 11:35
Sample ID: 18C0324-08
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
0 13
0 030
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Acrylonitrile
ND
00078
00033
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
tert-Amyl Methyl Ether (TAME)
ND
00013
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Benzene
ND
00026
000091
mg/Kg dry
1
SW 846 8260B
3/8/18
3/8/18 11:17
MFF
Bromobenzene
ND
00026
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Bromochloromethane
ND
00026
00018
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Bromodichloromethane
ND
00026
000078
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Bromoform
ND
00026
00018
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Bromomethane
ND
0 013
00055
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
2-Butanone (MEK)
ND
0 052
0 023
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
tert-Butyl Alcohol (TBA)
ND
0 052
0 027
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
n-Butylbenzene
ND
00026
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
sec-Butylbenzene
ND
00026
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
tert-Butylbenzene
ND
00026
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
00013
000078
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Carbon Disulfide
ND
00078
00056
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Carbon Tetrachloride
ND
00026
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Chlorobenzene
ND
00026
000091
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Chlorodibromomethane
ND
00026
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Chloroethane
ND
0 026
00020
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Chloroform
ND
00052
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Chloromethane
ND
0 013
00083
mg/Kg dry
1 L-04
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
2-Chlorotoluene
ND
00026
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
4-Chlorotoluene
ND
00026
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
00026
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1,2-Dibromoethane (EDB)
ND
00026
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Dibromomethane
ND
00026
000078
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1,2-Dichlorobenzene
ND
00026
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1,3-Dichlorobenzene
ND
00026
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1,4-Dichlorobenzene
ND
00026
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
trans-1,4-Dichloro-2-butene
ND
00052
00027
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Dichlorodifluoromethane (Freon 12)
ND
0 026
00017
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1,1-Dichloroethane
ND
00026
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1,2-Dichloroethane
ND
00026
00017
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1,1-Dichloroethylene
ND
00052
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
cis-1,2-Dichloroethylene
ND
00026
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
trans-1,2-Dichloroethylene
ND
00026
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1,2-Dichloropropane
ND
00026
00017
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1,3-Dichloropropane
ND
00013
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
2,2-Dichloropropane
ND
00026
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1, 1 -Dichloropropene
ND
00026
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
cis-1,3-Dichloropropene
ND
00013
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
trans-1,3-Dichloropropene
ND
00013
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Diethyl Ether
ND
0 026
00023
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Page 48 of 94

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 North (3-4) Sampled: 3/5/2018 11:35
Samnle ID: 18C0324-08
Samnle Matrix: Soil
Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPE)
ND
00013
000078
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1,4-Dioxane
ND
0 13
0 075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Ethanol
ND
026
0 052
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Ethylbenzene
ND
00026
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Hexachlorobutadiene
ND
00026
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11 17
MFF
2-Hexanone (MBK)
ND
0 026
0 014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Isopropylbenzene (Cumene)
ND
00026
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
p-Isopropyltoluene (p-Cymene)
ND
00026
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Methyl tert-Butyl Ether (MTBE)
ND
00052
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Methylene Chloride
ND
0 026
00092
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
4-Methyl-2-pentanone (MIBK)
ND
0 026
00099
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Naphthalene
ND
00052
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
n-Propylbenzene
ND
00026
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Styrene
ND
00026
000078
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1, 1, 1,2-Tetrachloroethane
ND
00026
00023
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1,1,2,2-Tetrachloroethane
ND
00013
00012
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Tetrachloroethylene
ND
00026
00017
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Tetrahydrofman
ND
0 013
00029
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Toluene
ND
00026
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1,2,3-Trichlorobenzene
ND
00026
000078
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1,2,4-Trichlorobenzene
ND
00026
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1,3,5-Trichlorobenzene
ND
00026
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1, 1, 1 -Trichloroethane
ND
00026
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1,1,2-Trichloroethane
ND
00026
00016
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Trichloroethylene
ND
00026
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Trichlorofluoromethane (Freon 11)
ND
0 013
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1,2,3-Trichloropropane
ND
00026
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1, 1,2-Trichloro- 1,2,2-trifluoroethane
ND
0 013
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
(Freon 113)
1,2,4-Trimethylbenzene
ND
00026
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
1,3,5-Trimethylbenzene
ND
00026
000078
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Vinyl Chloride
ND
0 013
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
m+p Xylene
ND
00052
00022
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
o-Xylene
ND
00026
000091
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:17
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
98 5
70-130
3/8/18 11:17
Toluene-d8
990
70-130
3/8/18 11:17
4-Bromofluorobenzenc
100
70-130
3/8/18 11:17
Page 49 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 North (3-4) Sampled: 3/5/2018 11:35
Samnle ID: 18C0324-08
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
020
0 060
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Acenaphthylene
ND
020
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Acetophenone
ND
040
0 079
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Aniline
ND
040
Oil
mg/Kg dry
1 V 05
SW 846 8270D
3/9/18
3/12/18 15:46
BGL
Anthracene
ND
020
0 058
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Benzidine
ND
078
0 50
mg/Kg dry
1 V-04, V-05
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Benzo(a)anthracene
ND
020
0 053
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Benzo(a)pyrene
ND
020
0 063
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Benzo(b)fluoranthene
ND
020
0 057
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Benzo(g,h,i)perylene
ND
020
0 089
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Benzo(k)fluoranthene
ND
020
0 063
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Benzoic Acid
ND
12
021
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Bis(2-chloroethoxy)methane
ND
040
0 077
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Bis(2-chloroethyl)ether
ND
040
0 079
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Bis(2-chloroisopropyl)ether
ND
040
0 086
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Bis(2-Ethylhexyl)phthalate
ND
040
0 16
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
4-Bromophenylphenylether
ND
040
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Butylbenzylphthalate
ND
040
0 096
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Carbazole
ND
020
0 052
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
4-Chloroaniline
ND
078
0 092
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
4-Chloro-3-methylphenol
ND
078
0 086
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
2-Chloronaphthalene
ND
040
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
2-Chlorophenol
ND
040
0 072
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
4-Chlorophenylphenylether
ND
040
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Chrysene
ND
020
0 063
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Dibenz(a,h)anthracene
ND
020
0 12
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Dibenzofman
ND
040
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Di-n-butylphthalate
ND
040
0 088
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
1,2-Dichlorobenzene
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
1,3-Dichlorobenzene
ND
040
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
1,4-Dichlorobenzene
ND
040
0 072
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
3,3-Dichlorobenzidine
ND
020
0 062
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
2,4-Dichlorophenol
ND
040
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Diethylphthalate
ND
040
0 072
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
2,4-Dimethylphenol
ND
040
0 075
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Dimethylphthalate
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
4,6-Dinitro-2-methylphenol
ND
040
038
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
2,4-Dinitrophenol
ND
078
023
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
2,4-Dinitrotoluene
ND
040
0 065
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
2,6-Dinitrotoluene
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Di-n-octylphthalate
ND
040
021
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
1,2-Diphenylhydrazine (as Azobenzene)
ND
040
0 065
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Fluoranthene
ND
020
0 066
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Flumene
ND
020
0 065
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Page 50 of 94

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 North (3-4) Sampled: 3/5/2018 11:35
Samnle ID: 18C0324-08
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Hexachlorobutadiene
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Hexachlorocyclopentadiene
ND
040
0 085
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Hexachloroethane
ND
040
0 080
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Indeno(1,2,3-cd)pyrene
ND
020
0 14
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15 46
BGL
Isophorone
ND
040
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
1-Methylnaphthalene
ND
020
0 077
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
2-Methylnaphthalene
ND
020
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
2-Methylphenol
ND
040
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
3/4-Methylphenol
ND
040
0 13
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Naphthalene
ND
020
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
2-Nitroaniline
ND
040
0 067
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
3-Nitroaniline
ND
040
0 058
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
4-Nitroaniline
ND
040
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Nitrobenzene
ND
040
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
2-Nitrophenol
ND
040
Oil
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
4-Nitrophenol
ND
078
0 088
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
N-Nitrosodimethylamine
ND
040
025
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
N-Nitrosodiphenylamine
ND
040
0 083
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
N-Nitrosodi-n-propylamine
ND
040
0 083
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Pentachloronitrobenzene
ND
040
0 096
mg/Kg dry
1
V-16
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Pentachlorophenol
ND
040
0 097
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Phenanthrene
ND
020
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Phenol
ND
040
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Pyrene
ND
020
0 066
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Pyridine
ND
040
0 065
mg/Kg dry
1
V-05
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
1,2,4,5-Tetrachlorobenzene
ND
040
0 072
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
1,2,4-Trichlorobenzene
ND
040
0 072
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
2,4,5-Trichlorophenol
ND
040
0 091
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
2,4,6-Trichlorophenol
ND
040
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 15:46
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
614
30-130
3/12/18 15:46
Phenol-d6
610
30-130
3/12/18 15:46
Nitrobenzene-d5
843
30-130
3/12/18 15:46
2-Fluorobiphenyl
812
30-130
3/12/18 15:46
2,4,6-Tribromophenol
824
30-130
3/12/18 15:46
p-Terphenyl-dl4
928
30-130
3/12/18 15:46
Page 51 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 North (3-4) Sampled: 3/5/2018 11:35
Samnle ID: 18C0324-08
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 842 % Wt 1
SM 2540G 3/8/18 3/8/18 19:17 DMP
Page 52 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 South Sampled: 3/5/2018 11:20
Sample ID: 18C0324-09
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
Oil
0 026
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Acrylonitrile
ND
00066
00028
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
tert-Amyl Methyl Ether (TAME)
ND
00011
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Benzene
ND
00022
000077
mg/Kg dry
1
SW 846 8260B
3/8/18
3/8/18 11:46
MFF
Bromobenzene
ND
00022
000089
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Bromochloromethane
ND
00022
00015
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Bromodichloromethane
ND
00022
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Bromoform
ND
00022
00015
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Bromomethane
ND
0 011
00046
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
2-Butanone (MEK)
ND
0 044
0 019
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
tert-Butyl Alcohol (TBA)
ND
0 044
0 023
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
n-Butylbenzene
ND
00022
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
sec-Butylbenzene
ND
00022
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
tert-Butylbenzene
ND
00022
00010
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
00011
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Carbon Disulfide
ND
00066
00048
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Carbon Tetrachloride
ND
00022
000089
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Chlorobenzene
ND
00022
000077
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Chlorodibromomethane
ND
00022
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Chloroethane
ND
0 022
00017
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Chloroform
ND
00044
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Chloromethane
ND
0 011
00071
mg/Kg dry
1 L-04
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
2-Chlorotoluene
ND
00022
000089
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
4-Chlorotoluene
ND
00022
000089
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
00022
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1,2-Dibromoethane (EDB)
ND
00022
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Dibromomethane
ND
00022
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1,2-Dichlorobenzene
ND
00022
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1,3-Dichlorobenzene
ND
00022
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1,4-Dichlorobenzene
ND
00022
000089
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
trans-1,4-Dichloro-2-butene
ND
00044
00023
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Dichlorodifluoromethane (Freon 12)
ND
0 022
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1,1-Dichloroethane
ND
00022
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1,2-Dichloroethane
ND
00022
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1,1-Dichloroethylene
ND
00044
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
cis-1,2-Dichloroethylene
ND
00022
000089
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
trans-1,2-Dichloroethylene
ND
00022
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1,2-Dichloropropane
ND
00022
00014
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1,3-Dichloropropane
ND
00011
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
2,2-Dichloropropane
ND
00022
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1, 1 -Dichloropropene
ND
00022
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
cis-1,3-Dichloropropene
ND
00011
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
trans-1,3-Dichloropropene
ND
00011
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Diethyl Ether
ND
0 022
00020
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Page 53 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 South Sampled: 3/5/2018 11:20
Samnle ID: 18C0324-09
Samnle Matrix: Soil
Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPE)
ND
00011
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1,4-Dioxane
ND
Oil
0 064
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Ethanol
ND
022
0 044
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Ethylbenzene
ND
00022
000089
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Hexachlorobutadiene
ND
00022
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 1146
MFF
2-Hexanone (MBK)
ND
0 022
0 012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Isopropylbenzene (Cumene)
ND
00022
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
p-Isopropyltoluene (p-Cymene)
ND
00022
000089
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Methyl tert-Butyl Ether (MTBE)
ND
00044
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Methylene Chloride
ND
0 022
00079
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
4-Methyl-2-pentanone (MIBK)
ND
0 022
00084
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Naphthalene
ND
00044
000077
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
n-Propylbenzene
ND
00022
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Styrene
ND
00022
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1, 1, 1,2-Tetrachloroethane
ND
00022
00020
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1,1,2,2-Tetrachloroethane
ND
00011
00010
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Tetrachloroethylene
ND
00022
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Tetrahydrofman
ND
0 011
00024
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Toluene
ND
00022
000089
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1,2,3-Trichlorobenzene
ND
00022
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1,2,4-Trichlorobenzene
ND
00022
000089
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1,3,5-Trichlorobenzene
ND
00022
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1, 1, 1 -Trichloroethane
ND
00022
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1,1,2-Trichloroethane
ND
00022
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Trichloroethylene
ND
00022
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Trichlorofluoromethane (Freon 11)
ND
0 011
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1,2,3-Trichloropropane
ND
00022
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1, 1,2-Trichloro- 1,2,2-trifluoroethane
ND
0 011
00010
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
(Freon 113)
1,2,4-Trimethylbenzene
ND
00022
000089
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
1,3,5-Trimethylbenzene
ND
00022
000066
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Vinyl Chloride
ND
0 011
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
m+p Xylene
ND
00044
00019
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
o-Xylene
ND
00022
000077
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 11:46
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
975
70-130
3/8/18 11:46
Toluene-d8
992
70-130
3/8/18 11:46
4-Bromofluorobenzenc
102
70-130
3/8/18 11:46
Page 54 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 South Sampled: 3/5/2018 11:20
Samnle ID: 18C0324-09
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
021
0 063
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Acenaphthylene
ND
021
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Acetophenone
ND
042
0 082
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Aniline
ND
042
0 12
mg/Kg dry
1 V 05
SW 846 8270D
3/9/18
3/12/18 16:09
BGL
Anthracene
ND
021
0 060
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Benzidine
ND
0 81
052
mg/Kg dry
1 V-04, V-05
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Benzo(a)anthracene
ND
021
0 055
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Benzo(a)pyrene
ND
021
0 065
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Benzo(b)fluoranthene
ND
021
0 059
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Benzo(g,h,i)perylene
ND
021
0 092
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Benzo(k)fluoranthene
ND
021
0 065
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Benzoic Acid
ND
12
022
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Bis(2-chloroethoxy)methane
ND
042
0 080
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Bis(2-chloroethyl)ether
ND
042
0 082
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Bis(2-chloroisopropyl)ether
ND
042
0 090
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Bis(2-Ethylhexyl)phthalate
ND
042
0 16
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
4-Bromophenylphenylether
ND
042
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Butylbenzylphthalate
ND
042
0 099
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Carbazole
ND
021
0 054
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
4-Chloroaniline
ND
0 81
0 096
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
4-Chloro-3-methylphenol
ND
0 81
0 090
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
2-Chloronaphthalene
ND
042
0 079
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
2-Chlorophenol
ND
042
0 075
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
4-Chlorophenylphenylether
ND
042
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Chrysene
ND
021
0 065
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Dibenz(a,h)anthracene
ND
021
0 13
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Dibenzofman
ND
042
0 072
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Di-n-butylphthalate
ND
042
0 091
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
1,2-Dichlorobenzene
ND
042
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
1,3-Dichlorobenzene
ND
042
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
1,4-Dichlorobenzene
ND
042
0 075
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
3,3-Dichlorobenzidine
ND
021
0 064
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
2,4-Dichlorophenol
ND
042
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Diethylphthalate
ND
042
0 075
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
2,4-Dimethylphenol
ND
042
0 077
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Dimethylphthalate
ND
042
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
4,6-Dinitro-2-methylphenol
ND
042
040
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
2,4-Dinitrophenol
ND
0 81
024
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
2,4-Dinitrotoluene
ND
042
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
2,6-Dinitrotoluene
ND
042
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Di-n-octylphthalate
ND
042
022
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
1,2-Diphenylhydrazine (as Azobenzene)
ND
042
0 067
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Fluoranthene
ND
021
0 069
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Flumene
ND
021
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Page 55 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 South Sampled: 3/5/2018 11:20
Samnle ID: 18C0324-09
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
042
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Hexachlorobutadiene
ND
042
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Hexachlorocyclopentadiene
ND
042
0 088
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Hexachloroethane
ND
042
0 083
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Indeno(1,2,3-cd)pyrene
ND
021
0 15
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16 09
BGL
Isophorone
ND
042
0 081
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
1-Methylnaphthalene
ND
021
0 080
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
2-Methylnaphthalene
ND
021
0 072
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
2-Methylphenol
ND
042
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
3/4-Methylphenol
ND
042
0 13
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Naphthalene
ND
021
Oil
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
2-Nitroaniline
ND
042
0 070
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
3-Nitroaniline
ND
042
0 060
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
4-Nitroaniline
ND
042
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Nitrobenzene
ND
042
0 079
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
2-Nitrophenol
ND
042
Oil
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
4-Nitrophenol
ND
0 81
0 091
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
N-Nitrosodimethylamine
ND
042
026
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
N-Nitrosodiphenylamine
ND
042
0 086
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
N-Nitrosodi-n-propylamine
ND
042
0 086
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Pentachloronitrobenzene
ND
042
0 099
mg/Kg dry
1
V-16
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Pentachlorophenol
ND
042
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Phenanthrene
ND
021
Oil
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Phenol
ND
042
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Pyrene
ND
021
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Pyridine
ND
042
0 067
mg/Kg dry
1
V-05
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
1,2,4,5-Tetrachlorobenzene
ND
042
0 075
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
1,2,4-Trichlorobenzene
ND
042
0 075
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
2,4,5-Trichlorophenol
ND
042
0 094
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
2,4,6-Trichlorophenol
ND
042
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:09
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
604
30-130
3/12/18 16:09
Phenol-d6
620
30-130
3/12/18 16:09
Nitrobenzene-d5
893
30-130
3/12/18 16:09
2-Fluorobiphenyl
85 2
30-130
3/12/18 16:09
2,4,6-Tribromophenol
881
30-130
3/12/18 16:09
p-Terphenyl-dl4
926
30-130
3/12/18 16:09
Page 56 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 South Sampled: 3/5/2018 11:20
Samnle ID: 18C0324-09
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 815 % Wt 1
SM 2540G 3/8/18 3/8/18 19:17 DMP
Page 57 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 West Sampled: 3/5/2018 11:25
Sample ID: 18C0324-10
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
0 098
0 023
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Acrylonitrile
ND
00059
00025
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
tert-Amyl Methyl Ether (TAME)
ND
000098
000069
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Benzene
ND
00020
000069
mg/Kg dry
1
SW 846 8260B
3/8/18
3/8/18 12:14
MFF
Bromobenzene
ND
00020
000079
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Bromochloromethane
ND
00020
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Bromodichloromethane
ND
00020
000059
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Bromoform
ND
00020
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Bromomethane
ND
00098
00041
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
2-Butanone (MEK)
ND
0 039
0 017
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
tert-Butyl Alcohol (TBA)
ND
0 039
0 021
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
n-Butylbenzene
ND
00020
000069
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
sec-Butylbenzene
ND
00020
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
tert-Butylbenzene
ND
00020
000088
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
000098
000059
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Carbon Disulfide
ND
00059
00042
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Carbon Tetrachloride
ND
00020
000079
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Chlorobenzene
ND
00020
000069
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Chlorodibromomethane
ND
00020
000069
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Chloroethane
ND
0 020
00015
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Chloroform
ND
00039
000069
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Chloromethane
ND
00098
00063
mg/Kg dry
1 L-04
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
2-Chlorotoluene
ND
00020
000079
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
4-Chlorotoluene
ND
00020
000079
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
00020
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1,2-Dibromoethane (EDB)
ND
00020
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Dibromomethane
ND
00020
000059
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1,2-Dichlorobenzene
ND
00020
000069
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1,3-Dichlorobenzene
ND
00020
000069
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1,4-Dichlorobenzene
ND
00020
000079
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
trans-1,4-Dichloro-2-butene
ND
00039
00021
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Dichlorodifluoromethane (Freon 12)
ND
0 020
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1,1-Dichloroethane
ND
00020
000069
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1,2-Dichloroethane
ND
00020
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1,1-Dichloroethylene
ND
00039
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
cis-1,2-Dichloroethylene
ND
00020
000079
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
trans-1,2-Dichloroethylene
ND
00020
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1,2-Dichloropropane
ND
00020
00013
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1,3-Dichloropropane
ND
000098
000069
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
2,2-Dichloropropane
ND
00020
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1, 1 -Dichloropropene
ND
00020
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
cis-1,3-Dichloropropene
ND
000098
000069
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
trans-1,3-Dichloropropene
ND
000098
000069
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Diethyl Ether
ND
0 020
00018
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Page 58 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 West Sampled: 3/5/2018 11:25
Samnle ID: 18C0324-10
Samnle Matrix: Soil
Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPE)
ND
0 00098
0 00059
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1,4-Dioxane
ND
0 098
0 057
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Ethanol
ND
020
0 039
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Ethylbenzene
ND
00020
000079
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Hexachlorobutadiene
ND
00020
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12 14
MFF
2-Hexanone (MBK)
ND
0 020
0 011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Isopropylbenzene (Cumene)
ND
00020
000069
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
p-Isopropyholuene (p-Cymene)
ND
00020
000079
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Methyl tert-Butyl Ether (MTBE)
ND
00039
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Methylene Chloride
ND
0 020
00070
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
4-Methyl-2-pentanone (MIBK)
ND
0 020
00075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Naphthalene
ND
00039
000069
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
n-Propylbenzene
ND
00020
000069
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Styrene
ND
00020
000059
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1, 1, 1,2-Tetrachloroethane
ND
00020
00018
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1,1,2,2-Tetrachloroethane
ND
000098
000088
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Tetrachloroethylene
ND
00020
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Tetrahydrofman
ND
00098
00022
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Toluene
ND
00020
000079
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1,2,3-Trichlorobenzene
ND
00020
000059
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1,2,4-Trichlorobenzene
ND
00020
000079
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1,3,5-Trichlorobenzene
ND
00020
000069
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1, 1, 1 -Trichloroethane
ND
00020
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1,1,2-Trichloroethane
ND
00020
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Trichloroethylene
ND
00020
000098
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Trichlorofluoromethane (Freon 11)
ND
00098
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1,2,3-Trichloropropane
ND
00020
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1, 1,2-Trichloro- 1,2,2-trifluoroethane
ND
00098
000088
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
(Freon 113)
1,2,4-Trimethylbenzene
ND
00020
000079
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
1,3,5-Trimethylbenzene
ND
00020
000059
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Vinyl Chloride
ND
00098
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
m+p Xylene
ND
00039
00017
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
o-Xylene
ND
00020
000069
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:14
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
995
70-130
3/8/18 12:14
Toluene-d8
101
70-130
3/8/18 12:14
4-Bromofluorobenzenc
101
70-130
3/8/18 12:14
Page 59 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 West Sampled: 3/5/2018 11:25
Samnle ID: 18C0324-10
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
020
0 059
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Acenaphthylene
ND
020
0 066
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Acetophenone
ND
040
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Aniline
ND
040
Oil
mg/Kg dry
1 V 05
SW 846 8270D
3/9/18
3/12/18 16:34
BGL
Anthracene
ND
020
0 057
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Benzidine
ND
077
049
mg/Kg dry
1 V-04, V-05
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Benzo(a)anthracene
ND
020
0 052
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Benzo(a)pyrene
ND
020
0 062
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Benzo(b)fluoranthene
ND
020
0 056
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Benzo(g,h,i)perylene
ND
020
0 087
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Benzo(k)fluoranthene
ND
020
0 062
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Benzoic Acid
ND
12
021
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Bis(2-chloroethoxy)methane
ND
040
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Bis(2-chloroethyl)ether
ND
040
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Bis(2-chloroisopropyl)ether
ND
040
0 085
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Bis(2-Ethylhexyl)phthalate
ND
040
0 15
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
4-Bromophenylphenylether
ND
040
0 066
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Butylbenzylphthalate
ND
040
0 094
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Carbazole
ND
020
0 051
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
4-Chloroaniline
ND
077
0 091
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
4-Chloro-3-methylphenol
ND
077
0 085
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
2-Chloronaphthalene
ND
040
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
2-Chlorophenol
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
4-Chlorophenylphenylether
ND
040
0 066
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Chrysene
ND
020
0 062
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Dibenz(a,h)anthracene
ND
020
0 12
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Dibenzofman
ND
040
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Di-n-butylphthalate
ND
040
0 086
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
1,2-Dichlorobenzene
ND
040
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
1,3-Dichlorobenzene
ND
040
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
1,4-Dichlorobenzene
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
3,3-Dichlorobenzidine
ND
020
0 060
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
2,4-Dichlorophenol
ND
040
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Diethylphthalate
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
2,4-Dimethylphenol
ND
040
0 073
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Dimethylphthalate
ND
040
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
4,6-Dinitro-2-methylphenol
ND
040
038
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
2,4-Dinitrophenol
ND
077
023
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
2,4-Dinitrotoluene
ND
040
0 064
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
2,6-Dinitrotoluene
ND
040
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Di-n-octylphthalate
ND
040
021
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
1,2-Diphenylhydrazine (as Azobenzene)
ND
040
0 064
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Fluoranthene
ND
020
0 065
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Flumene
ND
020
0 064
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Page 60 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 West Sampled: 3/5/2018 11:25
Samnle ID: 18C0324-10
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
040
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Hexachlorobutadiene
ND
040
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Hexachlorocyclopentadiene
ND
040
0 084
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Hexachloroethane
ND
040
0 079
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Indeno(1,2,3-cd)pyrene
ND
020
0 14
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16 34
BGL
Isophorone
ND
040
0 077
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
1-Methylnaphthalene
ND
020
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
2-Methylnaphthalene
ND
020
0 069
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
2-Methylphenol
ND
040
0 099
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
3/4-Methylphenol
ND
040
0 13
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Naphthalene
ND
020
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
2-Nitroaniline
ND
040
0 066
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
3-Nitroaniline
ND
040
0 057
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
4-Nitroaniline
ND
040
0 066
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Nitrobenzene
ND
040
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
2-Nitrophenol
ND
040
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
4-Nitrophenol
ND
077
0 086
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
N-Nitrosodimethylamine
ND
040
025
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
N-Nitrosodiphenylamine
ND
040
0 081
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
N-Nitrosodi-n-propylamine
ND
040
0 081
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Pentachloronitrobenzene
ND
040
0 094
mg/Kg dry
1
V-16
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Pentachlorophenol
ND
040
0 095
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Phenanthrene
ND
020
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Phenol
ND
040
0 067
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Pyrene
ND
020
0 065
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Pyridine
ND
040
0 064
mg/Kg dry
1
V-05
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
1,2,4,5-Tetrachlorobenzene
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
1,2,4-Trichlorobenzene
ND
040
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
2,4,5-Trichlorophenol
ND
040
0 089
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
2,4,6-Trichlorophenol
ND
040
0 066
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:34
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
65 3
30-130
3/12/18 16:34
Phenol-d6
653
30-130
3/12/18 16:34
Nitrobenzene-d5
919
30-130
3/12/18 16:34
2-Fluorobiphenyl
86 7
30-130
3/12/18 16:34
2,4,6-Tribromophenol
870
30-130
3/12/18 16:34
p-Terphenyl-dl4
964
30-130
3/12/18 16:34
Page 61 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 West Sampled: 3/5/2018 11:25
Samnle ID: 18C0324-10
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 858 % Wt 1
SM 2540G 3/8/18 3/8/18 19:18 DMP
Page 62 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 East Sampled: 3/5/2018 11:30
Sample ID: 18C0324-11
Samnle Matrix: Soil
Analyte
Results
RL
Volatile Organic Compounds by GC/MS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acetone
ND
Oil
0 025
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Acrylonitrile
ND
00064
00027
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
tert-Amyl Methyl Ether (TAME)
ND
00011
000075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Benzene
ND
00021
000075
mg/Kg dry
1
SW 846 8260B
3/8/18
3/8/18 12:41
MFF
Bromobenzene
ND
00021
000086
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Bromochloromethane
ND
00021
00015
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Bromodichloromethane
ND
00021
000064
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Bromoform
ND
00021
00015
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Bromomethane
ND
0 011
00045
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
2-Butanone (MEK)
ND
0 043
0 019
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
tert-Butyl Alcohol (TBA)
ND
0 043
0 022
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
n-Butylbenzene
ND
00021
000075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
sec-Butylbenzene
ND
00021
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
tert-Butylbenzene
ND
00021
000096
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
tert-Butyl Ethyl Ether (TBEE)
ND
00011
000064
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Carbon Disulfide
ND
00064
00046
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Carbon Tetrachloride
ND
00021
000086
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Chlorobenzene
ND
00021
000075
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Chlorodibromomethane
ND
00021
000075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Chloroethane
ND
0 021
00016
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Chloroform
ND
00043
000075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Chloromethane
ND
0 011
00069
mg/Kg dry
1 L-04
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
2-Chlorotoluene
ND
00021
000086
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
4-Chlorotoluene
ND
00021
000086
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1,2-Dibromo-3-chloropropane (DBCP)
ND
00021
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1,2-Dibromoethane (EDB)
ND
00021
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Dibromomethane
ND
00021
000064
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1,2-Dichlorobenzene
ND
00021
000075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1,3-Dichlorobenzene
ND
00021
000075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1,4-Dichlorobenzene
ND
00021
000086
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
trans-1,4-Dichloro-2-butene
ND
00043
00023
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Dichlorodifluoromethane (Freon 12)
ND
0 021
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1,1-Dichloroethane
ND
00021
000075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1,2-Dichloroethane
ND
00021
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1,1-Dichloroethylene
ND
00043
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
cis-1,2-Dichloroethylene
ND
00021
000086
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
trans-1,2-Dichloroethylene
ND
00021
000096
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1,2-Dichloropropane
ND
00021
00014
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1,3-Dichloropropane
ND
00011
000075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
2,2-Dichloropropane
ND
00021
000096
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1, 1 -Dichloropropene
ND
00021
000096
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
cis-1,3-Dichloropropene
ND
00011
000075
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
trans-1,3-Dichloropropene
ND
00011
000075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Diethyl Ether
ND
0 021
00019
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Page 63 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 East Sampled: 3/5/2018 11:30
Samnle ID: 18C0324-11
Samnle Matrix: Soil
Volatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
Diisopropyl Ether (DIPE)
ND
00011
000064
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1,4-Dioxane
ND
Oil
0 062
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Ethanol
ND
021
0 043
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Ethylbenzene
ND
00021
000086
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Hexachlorobutadiene
ND
00021
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 1241
MFF
2-Hexanone (MBK)
ND
0 021
0 012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Isopropylbenzene (Cumene)
ND
00021
000075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
p-Isopropyholuene (p-Cymene)
ND
00021
000086
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Methyl tert-Butyl Ether (MTBE)
ND
00043
000096
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Methylene Chloride
ND
0 021
00076
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
4-Methyl-2-pentanone (MIBK)
ND
0 021
00081
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Naphthalene
ND
00043
000075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
n-Propylbenzene
ND
00021
000075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Styrene
ND
00021
000064
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1, 1, 1,2-Tetrachloroethane
ND
00021
00019
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1,1,2,2-Tetrachloroethane
ND
00011
000096
mg/Kg dry
I
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Tetrachloroethylene
ND
00021
00014
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Tetrahydrofman
ND
0 011
00024
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Toluene
ND
00021
000086
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1,2,3-Trichlorobenzene
ND
00021
000064
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1,2,4-Trichlorobenzene
ND
00021
000086
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1,3,5-Trichlorobenzene
ND
00021
000075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1, 1, 1 -Trichloroethane
ND
00021
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1,1,2-Trichloroethane
ND
00021
00013
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Trichloroethylene
ND
00021
00011
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Trichlorofluoromethane (Freon 11)
ND
0 011
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1,2,3-Trichloropropane
ND
00021
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1, 1,2-Trichloro- 1,2,2-trifluoroethane
ND
0 011
000096
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
(Freon 113)
1,2,4-Trimethylbenzene
ND
00021
000086
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
1,3,5-Trimethylbenzene
ND
00021
000064
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Vinyl Chloride
ND
0 011
00012
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
m+p Xylene
ND
00043
00018
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
o-Xylene
ND
00021
000075
mg/Kg dry
1
SW-846 8260B
3/8/18
3/8/18 12:41
MFF
Surrogates
% Recovery
Recovery Limits
Flag/Qual
1,2-Dichloroethane-d4
101
70-130
3/8/18 12:41
Toluene-d8
100
70-130
3/8/18 12:41
4-Bromofluorobenzenc
102
70-130
3/8/18 12:41
Page 64 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 East Sampled: 3/5/2018 11:30
Samnle ID: 18C0324-11
Samnle Matrix: Soil
Analyte
Results
RL
Semivolatile Organic Compounds by GUMS
DL Units Dilution Flag/Qual
Method
Date
Prepared
Date/Time
Analyzed
Analyst
Acenaphthene
ND
022
0 065
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Acenaphthylene
ND
022
0 073
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Acetophenone
ND
043
0 085
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Aniline
ND
043
0 12
mg/Kg dry
1 V 05
SW 846 8270D
3/9/18
3/12/18 16:56
BGL
Anthracene
ND
022
0 062
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Benzidine
ND
0 84
054
mg/Kg dry
1 V-04, V-05
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Benzo(a)anthracene
ND
022
0 057
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Benzo(a)pyrene
ND
022
0 068
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Benzo(b)fluoranthene
ND
022
0 061
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Benzo(g,h,i)perylene
ND
022
0 096
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Benzo(k)fluoranthene
ND
022
0 068
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Benzoic Acid
ND
13
023
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Bis(2-chloroethoxy)methane
ND
043
0 083
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Bis(2-chloroethyl)ether
ND
043
0 085
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Bis(2-chloroisopropyl)ether
ND
043
0 093
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Bis(2-Ethylhexyl)phthalate
ND
043
0 17
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
4-Bromophenylphenylether
ND
043
0 073
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Butylbenzylphthalate
ND
043
0 10
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Carbazole
ND
022
0 056
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
4-Chloroaniline
ND
0 84
0 099
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
4-Chloro-3-methylphenol
ND
0 84
0 093
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
2-Chloronaphthalene
ND
043
0 082
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
2-Chlorophenol
ND
043
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
4-Chlorophenylphenylether
ND
043
0 073
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Chrysene
ND
022
0 068
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Dibenz(a,h)anthracene
ND
022
0 13
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Dibenzofman
ND
043
0 075
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Di-n-butylphthalate
ND
043
0 094
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
1,2-Dichlorobenzene
ND
043
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
1,3-Dichlorobenzene
ND
043
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
1,4-Dichlorobenzene
ND
043
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
3,3-Dichlorobenzidine
ND
022
0 066
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
2,4-Dichlorophenol
ND
043
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Diethylphthalate
ND
043
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
2,4-Dimethylphenol
ND
043
0 080
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Dimethylphthalate
ND
043
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
4,6-Dinitro-2-methylphenol
ND
043
041
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
2,4-Dinitrophenol
ND
0 84
025
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
2,4-Dinitrotoluene
ND
043
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
2,6-Dinitrotoluene
ND
043
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Di-n-octylphthalate
ND
043
023
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
1,2-Diphenylhydrazine (as Azobenzene)
ND
043
0 070
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Fluoranthene
ND
022
0 071
mg/Kg dry
I
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Flumene
ND
022
0 070
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Page 65 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 East Sampled: 3/5/2018 11:30
Samnle ID: 18C0324-11
Samnle Matrix: Soil
Semivolatile Organic Compounds by GUMS
Date
Date/Time
Analyte
Results
RL
DL
Units
Dilution
Flag/Qual
Method
Prepared
Analyzed
Analyst
Hexachlorobenzene
ND
043
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Hexachlorobutadiene
ND
043
0 076
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Hexachlorocyclopentadiene
ND
043
0 092
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Hexachloroethane
ND
043
0 087
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Indeno(1,2,3-cd)pyrene
ND
022
0 16
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16 56
BGL
Isophorone
ND
043
0 084
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
1-Methylnaphthalene
ND
022
0 083
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
2-Methylnaphthalene
ND
022
0 075
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
2-Methylphenol
ND
043
Oil
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
3/4-Methylphenol
ND
043
0 14
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Naphthalene
ND
022
Oil
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
2-Nitroaniline
ND
043
0 073
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
3-Nitroaniline
ND
043
0 062
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
4-Nitroaniline
ND
043
0 073
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Nitrobenzene
ND
043
0 082
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
2-Nitrophenol
ND
043
Oil
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
4-Nitrophenol
ND
0 84
0 094
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
N-Nitrosodimethylamine
ND
043
027
mg/Kg dry
1
V-20
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
N-Nitrosodiphenylamine
ND
043
0 089
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
N-Nitrosodi-n-propylamine
ND
043
0 089
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Pentachloronitrobenzene
ND
043
0 10
mg/Kg dry
1
V-16
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Pentachlorophenol
ND
043
0 10
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Phenanthrene
ND
022
Oil
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Phenol
ND
043
0 074
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Pyrene
ND
022
0 071
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Pyridine
ND
043
0 070
mg/Kg dry
1
V-05
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
1,2,4,5-Tetrachlorobenzene
ND
043
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
1,2,4-Trichlorobenzene
ND
043
0 078
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
2,4,5-Trichlorophenol
ND
043
0 098
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
2,4,6-Trichlorophenol
ND
043
0 073
mg/Kg dry
1
SW-846 8270D
3/9/18
3/12/18 16:56
BGL
Surrogates
% Recovery
Recovery Limits
Flag/Qual
2-Fluorophenol
645
30-130
3/12/18 16:56
Phenol-d6
645
30-130
3/12/18 16:56
Nitrobenzene-d5
841
30-130
3/12/18 16:56
2-Fluorobiphenyl
78 1
30-130
3/12/18 16:56
2,4,6-Tribromophenol
85 2
30-130
3/12/18 16:56
p-Terphenyl-dl4
875
30-130
3/12/18 16:56
Page 66 of 94

Table of Contents
ion -test°
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: 3312 Watkins Rd Sample Description: Work Order: 18C0324
Date Received: 3/6/2018
Field Sample #: AST-3 East Sampled: 3/5/2018 11:30
Samnle ID: 18C0324-11
Samnle Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date Date/Time
Analyte Results RL Units Dilution Flag/Qual Method Prepared Analyzed Analyst
% Solids 783 % Wt 1
SM 2540G 3/8/18 3/8/18 19:18 DMP
Page 67 of 94

Table of Contents
con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: % Solids-SM 2540G
Lab Number [Field ID]
Batch
Date
18C0324-01 [AST-1 Floor]
B198433
03/08/18
18C0324-02 [AST-1 South]
B198433
03/08/18
18C0324-03 [AST-1 North]
B198433
03/08/18
18C0324-04 [AST-1 West]
B198433
03/08/18
18C0324-05 [AST-1 East]
B198433
03/08/18
18C0324-06 [AST-3 Floor]
B198433
03/08/18
18C0324-07 [AST-3 North (1-2)]
B198433
03/08/18
18C0324-08 [AST-3 North (3-4)]
B198433
03/08/18
18C0324-09 [AST-3 South]
B198433
03/08/18
18C0324-10 [AST-3 West]
B198433
03/08/18
18C0324-11 [AST-3 East]
B198433
03/08/18
Prep Method: SW-846 3010A-SW-846 6010C-D
Leachates were extracted on 3/8/2018 per SW-846 1311 in Batch B198451
Lab Number [Field ID]
Batch
Initial [mL]
Final [mL]
Date
18C0324-07 [AST-3 North (1-2)]
B198629
500
500
03/12/18
Prep Method: SW-846 7470A Prep-SW-846 7470A
Leachates were extracted on 3/8/2018 per SW-846 1311 in Batch B198451
Lab Number [Field ID]
Batch
Initial [mL]
Final [mL]
Date
18C0324 07 [AST 3 North (1 2)]
B198633
600
600
03/12/18
Prep Meth d SW 846 3546 SW 846 8015C
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
18C0324-07 [AST-3 North (1-2)]
B198557
30 1
100
03/09/18
Prep Method: SW-846 5035/5030B-SW-846 8015C
Lab Number [Field ID]
Batch
Initial [g]
Final JmLl
Date
18C0324-07 [AST-3 North (1-2)]
B198651
590
600
03/12/18
Prep Method: SW-846 5035-SW-846 8260B
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
18C0324-01 [AST-1 Floor]
B198462
693
too
03/08/18
18C0324-02 [AST-1 South]
B198462
645
100
03/08/18
18C0324-03 [AST-1 North]
B198462
599
100
03/08/18
18C0324-04 [AST-1 West]
B198462
5 17
100
03/08/18
18C0324-05 [AST-1 East]
B198462
577
100
03/08/18
18C0324-06 [AST-3 Floor]
B 198462
522
100
03/08/18
18C0324-07 [AST-3 North (1-2)]
B198462
551
100
03/08/18
18C0324-08 [AST-3 North (3-4)]
B198462
456
too
03/08/18
18C0324-09 [AST-3 South]
B198462
554
100
03/08/18
18C0324-10 [AST-3 West]
B198462
593
100
03/08/18
18C0324-11 [AST-3 East]
B198462
596
100
03/08/18
Page 68 of 94

Table of Contents
con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
Prep Method: SW-846 3546-SW-846 8270D
Lab Number [Field ID] Batch Initial [g] Final [mL] Date
18C0324-01 [AST-1 Floor]
B198559
30 1
100
03/09/18
18C0324-02 [AST-1 South]
B198559
300
100
03/09/18
18C0324-03 [AST-1 North]
B198559
300
too
03/09/18
18C0324-04 [AST-1 West]
B198559
303
100
03/09/18
18C0324-05 [AST-1 East]
B198559
300
100
03/09/18
18C0324-06 [AST-3 Floor]
B198559
300
100
03/09/18
18C0324-07 [AST-3 North (1-2)]
B198559
300
100
03/09/18
18C0324-08 [AST-3 North (3-4)]
B198559
30 1
100
03/09/18
18C0324-09 [AST-3 South]
B198559
300
100
03/09/18
18C0324-10 [AST-3 West]
B198559
30 1
100
03/09/18
18C0324-11 [AST-3 East]
B198559
30 1
too
03/09/18
Page 69 of 94

Table of Contents
con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B198462 - SW-846 5035
Blank (B198462-BLK1) Prepared & Analyzed: 03/08/18
Acetone
ND
010
mg/Kg wet
Acrylonitrile
ND
00060
mg/Kg wet
tert-Amyl Methyl Ether (TAME)
ND
00010
mg/Kg wet
Benzene
ND
00020
mg/Kg wet
Bromobenzene
ND
00020
mg/Kg wet
Bromochloromethane
ND
00020
mg/Kg wet
Bromodichloromethane
ND
00020
mg/Kg wet
Bromoform
ND
00020
mg/Kg wet
Bromomethane
ND
0 010
mg/Kg wet
2-Butanone (MEK)
ND
0 040
mg/Kg wet
tert-Butyl Alcohol (TBA)
ND
0 040
mg/Kg wet
n-Butylbenzene
ND
00020
mg/Kg wet
sec-Butylbenzene
ND
00020
mg/Kg wet
tert-Butylbenzene
ND
00020
mg/Kg wet
tert-Butyl Ethyl Ether (TBEE)
ND
00010
mg/Kg wet
Carbon Disulfide
ND
00060
mg/Kg wet
Carbon Tetrachloride
ND
00020
mg/Kg wet
Chlorobenzene
ND
00020
mg/Kg wet
Chlorodibromomethane
ND
00010
mg/Kg wet
Chloroethane
ND
0 020
mg/Kg wet
Chloroform
ND
00040
mg/Kg wet
Chloromethane
ND
0 010
mg/Kg wet
2-Chlorotoluene
ND
00020
mg/Kg wet
4-Chlorotoluene
ND
00020
mg/Kg wet
1,2-Dibromo-3-chloropropane (DBCP)
ND
00020
mg/Kg wet
1,2-Dibromoethane (EDB)
ND
00010
mg/Kg wet
Dibromomethane
ND
00020
mg/Kg wet
1,2-Dichlorobenzene
ND
00020
mg/Kg wet
1,3-Dichlorobenzene
ND
00020
mg/Kg wet
1,4-Dichlorobenzene
ND
00020
mg/Kg wet
trans-1,4-Dichloro-2-butene
ND
00040
mg/Kg wet
Dichlorodifluoromethane (Freon 12)
ND
0 020
mg/Kg wet
1,1-Dichloroethane
ND
00020
mg/Kg wet
1,2-Dichloroethane
ND
00020
mg/Kg wet
1,1-Dichloroethylene
ND
00040
mg/Kg wet
cis-1,2-Dichloroethylene
ND
00020
mg/Kg wet
trans-1,2-Dichloroethylene
ND
00020
mg/Kg wet
1,2-Dichloropropane
ND
00020
mg/Kg wet
1,3-Dichloropropane
ND
00010
mg/Kg wet
2,2-Dichloropropane
ND
00020
mg/Kg wet
1, 1 -Dichloropropene
ND
00020
mg/Kg wet
cis-1,3-Dichloropropene
ND
00010
mg/Kg wet
trans-1,3-Dichloropropene
ND
00010
mg/Kg wet
Diethyl Ether
ND
0 020
mg/Kg wet
Diisopropyl Ether (DIPE)
ND
00010
mg/Kg wet
1,4-Dioxane
ND
0 10
mg/Kg wet
Ethanol
ND
020
mg/Kg wet
Ethylbenzene
ND
00020
mg/Kg wet
Hexachlorobutadiene
ND
00020
mg/Kg wet
2-Hexanone (MBK)
ND
0 020
mg/Kg wet
Isopropylbenzene (Cumene)
ND
00020
mg/Kg wet
p-Isopropyltoluene (p-Cymene)
ND
00020
mg/Kg wet
L-04
Page 70 of 94

Table of Contents
con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
knalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B198462 - SW-846 5035
Blank (B198462-BLK1)
Prepared & Analyzed:03/08/18
Methyl tert-Butyl Ether (MTBE)
ND
00040
mg/Kg wet
Methylene Chloride
ND
0 020
mg/Kg wet
4-Methyl-2-pentanone (MIBK)
ND
0 020
mg/Kg wet
Naphthalene
ND
00040
mg/Kg wet
n-Propylbenzene
ND
00020
mg/Kg wet
Styrene
ND
00020
mg/Kg wet
1, 1, 1,2-Tetrachloroethane
ND
00020
mg/Kg wet
1,1,2,2-Tetrachloroethane
ND
00010
mg/Kg wet
Tetrachloroethylene
ND
00020
mg/Kg wet
Tetrahydrofuran
ND
0 010
mg/Kg wet
Toluene
ND
00020
mg/Kg wet
1,2,3-Trichlorobenzene
ND
00020
mg/Kg wet
1,2,4-Trichlorobenzene
ND
00020
mg/Kg wet
1,3,5-Trichlorobenzene
ND
00020
mg/Kg wet
1, 1, 1 -Trichloroethane
ND
00020
mg/Kg wet
1,1,2-Trichloroethane
ND
00020
mg/Kg wet
Trichloroethylene
ND
00020
mg/Kg wet
Trichlorofluoromethane (Freon 11)
ND
0 010
mg/Kg wet
1,2,3-Trichloropropane
ND
00020
mg/Kg wet
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
ND
0 010
mg/Kg wet
113)
1,2,4-Trimethylbenzene
ND
00020
mg/Kg wet
1,3,5-Trimethylbenzene
ND
00020
mg/Kg wet
Vinyl Chloride
ND
0 010
mg/Kg wet
m+p Xylene
ND
00040
mg/Kg wet
o-Xylene
ND
00020
mg/Kg wet
Surrogate: 1,2-Dichloroethane-d4
0.0489
mg/Kg wet
00500 978 70-130
Surrogate: Toluene-d8
0.0488
mg/Kg wet
00500 976 70-130
Surrogate: 4-Bromofluorobenzene
0.0502
mg/Kg wet
00500 100 70-130
LCS (B198462-BS1)
Prepared & Analyzed: 03/08/18
Acetone
0 182
010
mg/Kg wet
0200
912
70-160
t
Acrylonitrile
00205
00060
mg/Kg wet
00200
103
70-130
tert-Amyl Methyl Ether (TAME)
00180
00010
mg/Kg wet
00200
899
70-130
Benzene
00178
00020
mg/Kg wet
00200
889
70-130
Bromobenzene
00193
00020
mg/Kg wet
00200
965
70-130
Bromochloromethane
00202
00020
mg/Kg wet
00200
101
70-130
Bromodichloromethane
00183
00020
mg/Kg wet
00200
915
70-130
Bromoform
00203
00020
mg/Kg wet
00200
102
70-130
Bromomethane
000892
0 010
mg/Kg wet
00200
446
40-130
1 t
2-Butanone (MEK)
0 215
0 040
mg/Kg wet
0200
107
70-160
f
tert-Butyl Alcohol (TBA)
0200
0 040
mg/Kg wet
0200
100
40-130
t
n-Butylbenzene
00193
00020
mg/Kg wet
00200
966
70-130
sec-Butylbenzene
00188
00020
mg/Kg wet
00200
940
70-130
tert-Butylbenzene
00178
00020
mg/Kg wet
00200
891
70-160
tert-Butyl Ethyl Ether (TBEE)
00180
00010
mg/Kg wet
00200
902
70-130
Carbon Disulfide
00168
00060
mg/Kg wet
00200
841
70-130
Carbon Tetrachloride
00193
00020
mg/Kg wet
00200
965
70-130
Chlorobenzene
00190
00020
mg/Kg wet
00200
948
70-130
Chlorodibromomethane
00211
00010
mg/Kg wet
00200
105
70-130
Chloroethane
00158
0 020
mg/Kg wet
00200
78 8
70-130
J
Chloroform
00180
00040
mg/Kg wet
00200
901
70-130
Chloromethane
00138
0 010
mg/Kg wet
00200
69.0
* 70-130
L-04
Page 71 of 94

con-testo
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
P.nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B198462 - SW-846 5035
LCS (B198462-BSI)
Prepared & Analyzed: 03/08/18
2-Chlorotoluene
00190
00020
mg/Kg wet
00200
95 1
70-130
4-Chlorotoluene
00198
00020
mg/Kg wet
00200
988
70-130
1,2-Dibromo-3-chloropropane (DBCP)
00198
00020
mg/Kg wet
00200
989
70-130
1,2-Dibromoethane (EDB)
00202
00010
mg/Kg wet
00200
101
70-130
Dibromomethane
00204
00020
mg/Kg wet
00200
102
70-130
1,2-Dichlorobenzene
00191
00020
mg/Kg wet
00200
957
70-130
1,3-Dichlorobenzene
00194
00020
mg/Kg wet
00200
972
70-130
1,4-Dichlorobenzene
00186
00020
mg/Kg wet
00200
929
70-130
trans-1,4-Dichloro-2-butene
00212
00040
mg/Kg wet
00200
106
70-130
Dichlorodifluoromethane (Freon 12)
000922
0 020
mg/Kg wet
00200
461
40-160
J t
1, 1 -Dichloroethane
00190
00020
mg/Kg wet
00200
952
70-130
1,2-Dichloroethane
00192
00020
mg/Kg wet
00200
958
70-130
1,1-Dichloroethylene
00168
00040
mg/Kg wet
00200
839
70-130
cis-1,2-Dichloroethylene
00195
00020
mg/Kg wet
00200
976
70-130
trans-1,2-Dichloroethylene
00182
00020
mg/Kg wet
00200
91 1
70-130
1,2-Dichloropropane
00179
00020
mg/Kg wet
00200
893
70-130
1,3-Dichloropropane
00192
00010
mg/Kg wet
00200
962
70-130
2,2-Dichloropropane
00192
00020
mg/Kg wet
00200
959
70-130
1,1-Dichloropropene
00174
00020
mg/Kg wet
00200
870
70-130
cis-1,3-Dichloropropene
00183
00010
mg/Kg wet
00200
916
70-130
trans-1,3-Dichloropropene
00209
00010
mg/Kg wet
00200
104
70-130
Diethyl Ether
00204
0 020
mg/Kg wet
00200
102
70-130
Diisopropyl Ether (DIPE)
00195
00010
mg/Kg wet
00200
977
70-130
1,4-Dioxane
0 217
010
mg/Kg wet
0200
108
40-160
t
Ethanol
0 183
020
mg/Kg wet
0200
914
40-160
J
Ethylbenzene
00184
00020
mg/Kg wet
00200
920
70-130
Hexachlorobutadiene
00181
00020
mg/Kg wet
00200
903
70-160
2-Hexanone (MBK)
0 219
0 020
mg/Kg wet
0200
110
70-160
t
Isopropylbenzene (Cumene)
00213
00020
mg/Kg wet
00200
106
70-130
p-Isopropyholuene (p-Cymene)
00189
00020
mg/Kg wet
00200
944
70-130
Methyl tert-Butyl Ether (MTBE)
00199
00040
mg/Kg wet
00200
994
70-130
Methylene Chloride
00197
0 020
mg/Kg wet
00200
985
40-160
J t
4-Methyl-2-pentanone (MIBK)
0 218
0 020
mg/Kg wet
0200
109
70-160
t
Naphthalene
00176
00040
mg/Kg wet
00200
881
40-130
t
n-Propylbenzene
00193
00020
mg/Kg wet
00200
964
70-130
Styrene
00200
00020
mg/Kg wet
00200
998
70-130
1, 1, 1,2-Tetrachloroethane
00201
00020
mg/Kg wet
00200
100
70-130
1,1,2,2-Tetrachloroethane
00210
00010
mg/Kg wet
00200
105
70-130
Tetrachloroethylene
00195
00020
mg/Kg wet
00200
974
70-130
Tetrahydroforan
00177
0 010
mg/Kg wet
00200
88 3
70-130
Toluene
00186
00020
mg/Kg wet
00200
93 1
70-130
1,2,3-Trichlorobenzene
00179
00020
mg/Kg wet
00200
896
70-130
1,2,4-Trichlorobenzene
00181
00020
mg/Kg wet
00200
905
70-130
1,3,5-Trichlorobenzene
00181
00020
mg/Kg wet
00200
903
70-130
1, 1, 1 -Trichloroethane
00177
00020
mg/Kg wet
00200
884
70-130
1,1,2-Trichloroethane
00204
00020
mg/Kg wet
00200
102
70-130
Trichloroethylene
00179
00020
mg/Kg wet
00200
893
70-130
Trichlorofluoromethane (Freon 11)
00167
0 010
mg/Kg wet
00200
834
70-130
1,2,3-Trichloropropane
00214
00020
mg/Kg wet
00200
107
70-130
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
00170
0 010
mg/Kg wet
00200
85 0
70-130
113)
1,2,4-Trimethylbenzene
00179
00020
mg/Kg wet
00200
895
70-130
Page 72 of 94

Table of Contents
con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
knalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B198462 - SW-846 5035
LCS (B198462-BSI)
Prepared & Analyzed: 03/08/18
1,3,5-Trimethylbenzene
00197
0 0020
mg/Kg wet
00200
985
70-130
Vinyl Chloride
00143
0 010
mg/Kg wet
00200
716
40-130
t
m+p Xylene
00358
00040
mg/Kg wet
00400
896
70-130
o-Xylene
00189
00020
mg/Kg wet
00200
945
70-130
Surrogate: 1,2-Dichloroethane-d4
0.0492
mg/Kg wet
00500
984
70-130
Surrogate: Toluene-d8
0.0494
mg/Kg wet
00500
988
70-130
Surrogate: 4-Bromofluorobenzene
0.0518
mg/Kg wet
00500
104
70-130
LCS Dup (B198462-BSD1)
Prepared & Analyzed: 03/08/18
Acetone
0 184
010
mg/Kg wet
0200
919
70-160
0 798
25
t
Acrylonitrile
00210
00060
mg/Kg wet
00200
105
70-130
231
25
tert-Amyl Methyl Ether (TAME)
00189
00010
mg/Kg wet
00200
947
70-130
520
25
Benzene
00184
00020
mg/Kg wet
00200
918
70-130
321
25
Bromobenzene
00204
00020
mg/Kg wet
00200
102
70-130
554
25
Bromochloromethane
00226
00020
mg/Kg wet
00200
113
70-130
113
25
Bromodichloromethane
00196
00020
mg/Kg wet
00200
979
70-130
676
25
Bromoform
00216
00020
mg/Kg wet
00200
108
70-130
5 82
25
Bromomethane
000994
0 010
mg/Kg wet
00200
497
40-130
10 8
25
1 t
2-Butanone (MEK)
0 218
0 040
mg/Kg wet
0200
109
70-160
141
25
f
tert-Butyl Alcohol (TBA)
0 216
0 040
mg/Kg wet
0200
108
40-130
777
25
t
n-Butylbenzene
00202
00020
mg/Kg wet
00200
101
70-130
4 65
25
sec-Butylbenzene
00202
00020
mg/Kg wet
00200
101
70-130
6 98
25
tert-Butylbenzene
00187
00020
mg/Kg wet
00200
937
70-160
503
25
t
tert-Butyl Ethyl Ether (TBEE)
00185
00010
mg/Kg wet
00200
927
70-130
2 73
25
Carbon Disulfide
00169
00060
mg/Kg wet
00200
845
70-130
0 474
25
Carbon Tetrachloride
00195
00020
mg/Kg wet
00200
977
70-130
124
25
Chlorobenzene
00200
00020
mg/Kg wet
00200
100
70-130
544
25
Chlorodibromomethane
00220
00010
mg/Kg wet
00200
110
70-130
4 09
25
Chloroethane
00160
0 020
mg/Kg wet
00200
800
70-130
151
25
1
Chloroform
00180
00040
mg/Kg wet
00200
900
70-130
0 111
25
Chloromethane
00140
0 010
mg/Kg wet
00200
698
* 70-130
1 15
25
L-04
2-Chlorotoluene
00191
00020
mg/Kg wet
00200
956
70-130
0 524
25
4-Chlorotoluene
00203
00020
mg/Kg wet
00200
101
70-130
250
25
1,2-Dibromo-3-chloropropane (DBCP)
00217
00020
mg/Kg wet
00200
108
70-130
9 07
25
1,2-Dibromoethane (EDB)
00211
00010
mg/Kg wet
00200
106
70-130
445
25
Dibromomethane
00215
00020
mg/Kg wet
00200
107
70-130
497
25
1,2-Dichlorobenzene
00207
00020
mg/Kg wet
00200
104
70-130
8 02
25
1,3-Dichlorobenzene
00207
00020
mg/Kg wet
00200
104
70-130
647
25
1,4-Dichlorobenzene
00196
00020
mg/Kg wet
00200
981
70-130
545
25
trans-1,4-Dichloro-2-butene
00225
00040
mg/Kg wet
00200
113
70-130
622
25
Dichlorodifluoromethane (Freon 12)
000936
0 020
mg/Kg wet
00200
468
40-160
151
25
1 t
1,1-Dichloroethane
00191
00020
mg/Kg wet
00200
956
70-130
0 419
25
1,2-Dichloroethane
00196
00020
mg/Kg wet
00200
980
70-130
227
25
1,1-Dichloroethylene
00175
00040
mg/Kg wet
00200
875
70-130
420
25
cis-1,2-Dichloroethylene
00198
00020
mg/Kg wet
00200
991
70-130
153
25
trans-1,2-Dichloroethylene
00188
00020
mg/Kg wet
00200
939
70-130
3 03
25
1,2-Dichloropropane
00191
00020
mg/Kg wet
00200
957
70-130
692
25
1,3-Dichloropropane
00207
00010
mg/Kg wet
00200
103
70-130
721
25
2,2-Dichloropropane
00195
00020
mg/Kg wet
00200
975
70-130
165
25
1,1-Dichloropropene
00185
00020
mg/Kg wet
00200
924
70-130
6 02
25
cis-1,3-Dichloropropene
00191
00010
mg/Kg wet
00200
957
70-130
438
25
trans-1,3-Dichloropropene
00215
00010
mg/Kg wet
00200
108
70-130
3 02
25
Page 73 of 94

Table of Contents
con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Volatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B198462 - SW-846 5035
LCS Dup (B198462-BSD1) Prepared & Analyzed: 03/08/18
Diethyl Ether
00189
0 020
mg/Kg wet
00200
945
70-130
773
25
J
Diisopropyl Ether (DIPE)
00197
00010
mg/Kg wet
00200
987
70-130
102
25
1,4-Dioxane
0 211
010
mg/Kg wet
0200
106
40-160
248
50
t $
Ethanol
0 172
020
mg/Kg wet
0200
86 1
40-160
595
25
J
Ethylbenzene
00195
00020
mg/Kg wet
00200
973
70-130
560
25
Hexachlorobutadiene
00207
00020
mg/Kg wet
00200
104
70-160
137
25
2-Hexanone (MBK)
0 232
0 020
mg/Kg wet
0200
116
70-160
568
25
$
Isopropylbenzene (Cumene)
00216
00020
mg/Kg wet
00200
108
70-130
149
25
p-Isopropyltoluene (p-Cymene)
00197
00020
mg/Kg wet
00200
986
70-130
435
25
Methyl tert-Butyl Ether (MTBE)
00196
00040
mg/Kg wet
00200
978
70-130
162
25
Methylene Chloride
00190
0 020
mg/Kg wet
00200
95 1
40-160
3 51
25
J t
4-Methyl-2-pentanone (MIBK)
0 228
0 020
mg/Kg wet
0200
114
70-160
462
25
t
Naphthalene
00192
00040
mg/Kg wet
00200
961
40-130
869
25
$
n-Propylbenzene
00197
00020
mg/Kg wet
00200
985
70-130
2 15
25
Styrene
00201
00020
mg/Kg wet
00200
101
70-130
0 898
25
1, 1, 1,2-Tetrachloroethane
00208
00020
mg/Kg wet
00200
104
70-130
3 72
25
1,1,2,2-Tetrachloroethane
00222
00010
mg/Kg wet
00200
ill
70-130
538
25
Tetrachloroethylene
00206
00020
mg/Kg wet
00200
103
70-130
5 69
25
Tetrahydrofuran
00207
0 010
mg/Kg wet
00200
104
70-130
15 9
25
Toluene
00194
00020
mg/Kg wet
00200
972
70-130
431
25
1,2,3-Trichlorobenzene
00194
00020
mg/Kg wet
00200
969
70-130
7 83
25
1,2,4-Trichlorobenzene
00199
00020
mg/Kg wet
00200
996
70-130
957
25
1,3,5-Trichlorobenzene
00198
00020
mg/Kg wet
00200
989
70-130
9 09
25
1, 1, 1 -Trichloroethane
00178
00020
mg/Kg wet
00200
891
70-130
0 789
25
1,1,2-Trichloroethane
00206
00020
mg/Kg wet
00200
103
70-130
0 780
25
Trichloroethylene
00183
00020
mg/Kg wet
00200
913
70-130
221
25
Trichlorofluoromethane (Freon 11)
00174
0 010
mg/Kg wet
00200
868
70-130
400
25
1,2,3-Trichloropropane
00232
00020
mg/Kg wet
00200
116
70-130
7 97
25
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon
00168
0 010
mg/Kg wet
00200
83 8
70-130
142
25
113)
1,2,4-Trimethylbenzene
00191
00020
mg/Kg wet
00200
957
70-130
670
25
1,3,5-Trimethylbenzene
00201
00020
mg/Kg wet
00200
100
70-130
191
25
Vinyl Chloride
00145
0 010
mg/Kg wet
00200
725
40-130
125
25
t
m+p Xylene
00394
00040
mg/Kg wet
00400
986
70-130
957
25
o-Xylene
00198
00020
mg/Kg wet
00200
992
70-130
485
25
Surrogate: 1,2-Dichloroethane-d4
0.0497
mg/Kg wet
00500
994
70-130
Surrogate: Toluene-d8
0.0495
mg/Kg wet
00500
991
70-130
Surrogate: 4-Bromofluorobenzene
0.0505
mg/Kg wet
00500
101
70-130
Page 74 of 94

Table of Contents
con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B198559 - SW-846 3546
Blank (B198559-BLK1) Prepared: 03/09/18 Analyzed: 03/12/18
Acenaphthene
ND
017
mg/Kg wet
Acenaphthylene
ND
017
mg/Kg wet
Acetophenone
ND
034
mg/Kg wet
Aniline
ND
034
mg/Kg wet
Anthracene
ND
017
mg/Kg wet
Benzidine
ND
066
mg/Kg wet
Benzo(a)anthracene
ND
017
mg/Kg wet
Benzo(a)pyrene
ND
017
mg/Kg wet
Benzo(b)fluoranthene
ND
017
mg/Kg wet
Benzo(g,h,i)perylene
ND
017
mg/Kg wet
Benzo(k)fluoranthene
ND
017
mg/Kg wet
Benzoic Acid
ND
10
mg/Kg wet
Bis(2-chloroethoxy)methane
ND
034
mg/Kg wet
Bis(2-chloroethyl)ether
ND
034
mg/Kg wet
Bis(2-chloroisopropyl)ether
ND
034
mg/Kg wet
Bis(2-Ethylhexyl)phthalate
ND
034
mg/Kg wet
4-13romophenylphenylether
ND
034
mg/Kg wet
Butylbenzylphthalate
ND
034
mg/Kg wet
Carbazole
ND
017
mg/Kg wet
4-Chloroaniline
ND
066
mg/Kg wet
4-Chloro-3-methylphenol
ND
066
mg/Kg wet
2-Chloronaphthalene
ND
034
mg/Kg wet
2-Chlorophenol
ND
034
mg/Kg wet
4-Chlorophenylphenylether
ND
034
mg/Kg wet
Chrysene
ND
017
mg/Kg wet
Dibenz(a,h)anthracene
ND
017
mg/Kg wet
Dibenzofuran
ND
034
mg/Kg wet
Di-n-butylphthalate
ND
034
mg/Kg wet
1,2-Dichlorobenzene
ND
034
mg/Kg wet
1,3-Dichlorobenzene
ND
034
mg/Kg wet
1,4-Dichlorobenzene
ND
034
mg/Kg wet
3,3-Dichlorobenzidine
ND
017
mg/Kg wet
2,4-Dichlorophenol
ND
034
mg/Kg wet
Diethylphthalate
ND
034
mg/Kg wet
2,4-Dimethylphenol
ND
034
mg/Kg wet
Dimethylphthalate
ND
034
mg/Kg wet
4,6-Dinitro-2-methylphenol
ND
034
mg/Kg wet
2,4-Dinitrophenol
ND
066
mg/Kg wet
2,4-Dinitrotoluene
ND
034
mg/Kg wet
2,6-Dinitrotoluene
ND
034
mg/Kg wet
Di-n-octylphthalate
ND
034
mg/Kg wet
1,2-Diphenylhydrazine (as Azobenzene)
ND
034
mg/Kg wet
Fluoranthene
ND
017
mg/Kg wet
Fluorene
ND
017
mg/Kg wet
Hexachlorobenzene
ND
034
mg/Kg wet
Hexachlorobutadiene
ND
034
mg/Kg wet
Hexachlorocyclopentadiene
ND
034
mg/Kg wet
Hexachloroethane
ND
034
mg/Kg wet
Indeno(1,2,3-cd)pyrene
ND
017
mg/Kg wet
Isophorone
ND
034
mg/Kg wet
1-Methylnaphthalene
ND
0 17
mg/Kg wet
2-Methylnaphthalene
ND
0 17
mg/Kg wet
V-05
V-04, V-05
V-34
Page 75 of 94

Table of Contents
con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B198559 - SW-846 3546
Blank (B198559-BLK1)
Prepared: 03/09/18 Analyzed: 03/12/18
2-Methylphenol
ND
034
mg/Kg wet
3/4-Methylphenol
ND
034
mg/Kg wet
Naphthalene
ND
017
mg/Kg wet
2-Nitroaniline
ND
034
mg/Kg wet
V-20
3-Nitroaniline
ND
034
mg/Kg wet
4-Nitroaniline
ND
034
mg/Kg wet
Nitrobenzene
ND
034
mg/Kg wet
2-Nitrophenol
ND
034
mg/Kg wet
4-Nitrophenol
ND
066
mg/Kg wet
V-20
N-Nitrosodimethylamine
ND
034
mg/Kg wet
V-20
N-Nitrosodiphenylamine
ND
034
mg/Kg wet
N-Nitrosodi-n-propylamine
ND
034
mg/Kg wet
Pentachloronitrobenzene
ND
034
mg/Kg wet
V-16
Pentachlorophenol
ND
034
mg/Kg wet
Phenanthrene
ND
017
mg/Kg wet
Phenol
ND
034
mg/Kg wet
Pyrene
ND
017
mg/Kg wet
Pyridine
ND
034
mg/Kg wet
V-05
1,2,4,5-Tetrachlorobenzene
ND
034
mg/Kg wet
1,2,4-Trichlorobenzene
ND
034
mg/Kg wet
2,4,5-Trichlorophenol
ND
034
mg/Kg wet
2,4,6-Trichlorophenol
ND
034
mg/Kg wet
Surrogate: 2-Fluorophenol
3.71
mg/Kg wet
667
556
30-130
Surrogate: Phenol-d6
3.75
mg/Kg wet
667
562
30-130
Surrogate: Nitrobenzene-d5
2.55
mg/Kg wet
333
766
30-130
Surrogate: 2-Fluorobiphenyl
2.24
mg/Kg wet
333
672
30-130
Surrogate: 2,4,6-Tribromophenol
4.60
mg/Kg wet
667
689
30-130
Surrogate: p-Terphenyl-dl4
2.26
mg/Kg wet
333
679
30-130
LCS (B198559-BSI)
Prepared: 03/09/18 Analyzed: 03/12/18
Acenaphthene
0 963
017
mg/Kg wet
167
578
40-140
Acenaphthylene
0 997
017
mg/Kg wet
167
598
40-140
Acetophenone
0 897
034
mg/Kg wet
167
53 8
40-140
Aniline
0 676
034
mg/Kg wet
167
406
10-140
V-05 t
Anthracene
0 917
017
mg/Kg wet
167
550
40-140
Benzidine
143
066
mg/Kg wet
167
86 1
40-140
V-04, V-05
Benzo(a)anthracene
0 990
017
mg/Kg wet
167
594
40-140
Benzo(a)pyrene
101
017
mg/Kg wet
167
607
40-140
Benzo(b)fluoranthene
0 964
017
mg/Kg wet
167
578
40-140
Benzo(g,h,i)perylene
104
017
mg/Kg wet
167
621
40-140
Benzo(k)fluoranthene
0 989
017
mg/Kg wet
167
593
40-140
Benzoic Acid
0 517
10
mg/Kg wet
167
310
30-130
J
Bis(2-chloroethoxy)methane
106
034
mg/Kg wet
167
633
40-140
Bis(2-chloroethyl)ether
0 829
034
mg/Kg wet
167
498
40-140
Bis(2-chloroisopropyl)ether
0 941
034
mg/Kg wet
167
565
40-140
Bis(2-Ethylhexyl)phthalate
123
034
mg/Kg wet
167
736
40-140
4-Bromophenylphenylether
101
034
mg/Kg wet
167
607
40-140
Butylbenzylphthalate
1 19
034
mg/Kg wet
167
714
40-140
Carbazole
0 961
017
mg/Kg wet
167
576
40-140
4-Chloroaniline
0 744
066
mg/Kg wet
167
446
10-140
V-34
4-Chloro-3-methylphenol
1 13
066
mg/Kg wet
167
677
30-130
2-Chloronaphthalene
0 872
034
mg/Kg wet
167
523
40-140
Page 76 of 94

Table of Contents
con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
malyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B198559 - SW-846 3546
LCS (B198559-BSI)
Prepared: 03/09/18 Analyzed: 03/12/18
2-Chlorophenol
0 768
034
mg/Kg wet
167
461
30-130
4-Chlorophenylphenylether
105
034
mg/Kg wet
167
630
40-140
Chrysene
0 984
017
mg/Kg wet
167
590
40-140
Dibenz(a,h)anthracene
102
017
mg/Kg wet
167
613
40-140
Dibenzofuran
1 10
034
mg/Kg wet
167
659
40-140
Di-n-butylphthalate
110
034
mg/Kg wet
167
661
40-140
1,2-Dichlorobenzene
0 724
034
mg/Kg wet
167
434
40-140
1,3-Dichlorobenzene
0 709
034
mg/Kg wet
167
425
40-140
1,4-Dichlorobenzene
0 700
034
mg/Kg wet
167
420
40-140
3,3-Dichlorobenzidine
0 827
017
mg/Kg wet
167
496
20-140
t
2,4-Dichlorophenol
0 891
034
mg/Kg wet
167
535
30-130
Diethylphthalate
1 18
034
mg/Kg wet
167
709
40-140
2,4-Dimethylphenol
0 981
034
mg/Kg wet
167
589
30-130
Dimethylphthalate
106
034
mg/Kg wet
167
633
40-140
4,6-Dinitro-2-methylphenol
0 754
034
mg/Kg wet
167
452
30-130
2,4-Dinitrophenol
0 604
066
mg/Kg wet
167
362
30-130
1
2,4-Dinitrotoluene
0 986
034
mg/Kg wet
167
591
40-140
2,6-Dinitrotoluene
102
034
mg/Kg wet
167
61 1
40-140
Di-n-octylphthalate
120
034
mg/Kg wet
167
718
40-140
1,2-Diphenylhydrazine (as Azobenzene)
122
034
mg/Kg wet
167
733
40-140
Fluoranthene
0 949
017
mg/Kg wet
167
570
40-140
Fluorene
102
017
mg/Kg wet
167
611
40-140
Hexachlorobenzene
0 908
034
mg/Kg wet
167
545
40-140
Hexachlorobutadiene
0 966
034
mg/Kg wet
167
579
40-140
Hexachlorocyclopentadiene
0 815
034
mg/Kg wet
167
489
40-140
Hexachloroethane
0 813
034
mg/Kg wet
167
488
40-140
Indeno(1,2,3-cd)pyrene
101
017
mg/Kg wet
167
606
40-140
Isophorone
1 11
034
mg/Kg wet
167
668
40-140
1-Methylnaphthalene
0 934
0 17
mg/Kg wet
167
560
40-140
2-Methylnaphthalene
0 928
0 17
mg/Kg wet
167
557
40-140
2-Methylphenol
0 853
034
mg/Kg wet
167
512
30-130
3/4-Methylphenol
0 939
034
mg/Kg wet
167
563
30-130
Naphthalene
0 841
0 17
mg/Kg wet
167
505
40-140
2-Nitroaniline
132
034
mg/Kg wet
167
789
40-140
V-20
3-Nitroaniline
0 904
034
mg/Kg wet
167
543
30-140
f
4-Nitroaniline
0 989
034
mg/Kg wet
167
593
40-140
Nitrobenzene
104
034
mg/Kg wet
167
624
40-140
2-Nitrophenol
0 839
034
mg/Kg wet
167
503
30-130
4-Nitrophenol
123
066
mg/Kg wet
167
738
30-130
V-20
N-Nitrosodimethylamine
0 972
034
mg/Kg wet
167
583
40-140
V-20
N-Nitrosodiphenylamine
126
034
mg/Kg wet
167
753
40-140
N-Nitrosodi-n-propylamine
0 982
034
mg/Kg wet
167
58 9
40-140
Pentachloronitrobenzene
0 954
034
mg/Kg wet
167
572
40-140
V-16
Pentachlorophenol
0 815
034
mg/Kg wet
167
48 9
30-130
Phenanthrene
0 920
0 17
mg/Kg wet
167
552
40-140
Phenol
0 785
034
mg/Kg wet
167
471
30-130
Pyrene
0 993
0 17
mg/Kg wet
167
596
40-140
Pyridine
0 491
034
mg/Kg wet
167
29.4 *
30-140
L-07, V-05 t
1,2,4,5-Tetrachlorobenzene
104
034
mg/Kg wet
167
625
40-140
1,2,4-Trichlorobenzene
0 855
034
mg/Kg wet
167
513
40-140
2,4,5-Trichlorophenol
1 10
034
mg/Kg wet
167
661
30-130
2,4,6-Trichlorophenol
109
034
mg/Kg wet
167
65 1
30-130
Page 77 of 94

Table of Contents
con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B198559 - SW-846 3546
LCS (B198559-BSI)
Prepared: 03/09/18 Analyzed: 03/12/18
Surrogate: 2-Fluorophenol
3.23
mg/Kg wet
667
484
30-130
Surrogate: Phenol-d6
3.44
mg/Kg wet
667
516
30-130
Surrogate: Nitrobenzene-d5
2.30
mg/Kg wet
333
689
30-130
Surrogate: 2-Fluorobiphenyl
2.33
mg/Kg wet
333
698
30-130
Surrogate: 2,4,6-Tribromophenol
4.74
mg/Kg wet
667
71 1
30-130
Surrogate: p-Terphenyl-dl4
2.20
mg/Kg wet
333
661
30-130
LCS Dup (B198559-BSD1)
Prepared: 03/09/18 Analyzed: 03/12/18
Acenaphthene
0 973
017
mg/Kg wet
167
584
40-140
0 998
30
Acenaphthylene
0 989
017
mg/Kg wet
167
593
40-140
0 873
30
Acetophenone
101
034
mg/Kg wet
167
607
40-140
120
30
Aniline
0 686
034
mg/Kg wet
167
412
10-140
152
50
V-05 f #
Anthracene
0 949
017
mg/Kg wet
167
569
40-140
343
30
Benzidine
145
066
mg/Kg wet
167
871
40-140
1 18
30
V-04, V-05
Benzo(a)anthracene
102
017
mg/Kg wet
167
613
40-140
311
30
Benzo(a)pyrene
0 989
017
mg/Kg wet
167
594
40-140
230
30
Benzo(b)fluoranthene
100
017
mg/Kg wet
167
600
40-140
370
30
Benzo(g,h,i)perylene
106
017
mg/Kg wet
167
638
40-140
273
30
Benzo(k)fluoranthene
0 998
017
mg/Kg wet
167
599
40-140
0 906
30
Benzoic Acid
0 523
10
mg/Kg wet
167
314
30-130
122
50
J $
Bis(2-chloroethoxy)methane
1 13
034
mg/Kg wet
167
678
40-140
677
30
Bis(2-chloroethyl)ether
0 938
034
mg/Kg wet
167
563
40-140
123
30
Bis(2-chloroisopropyl)ether
105
034
mg/Kg wet
167
628
40-140
106
30
Bis(2-Ethylhexyl)phthalate
1 17
034
mg/Kg wet
167
702
40-140
465
30
4-Bromophenylphenylether
107
034
mg/Kg wet
167
642
40-140
557
30
Butylbenzylphthalate
1 17
034
mg/Kg wet
167
699
40-140
212
30
Carbazole
0 959
017
mg/Kg wet
167
576
40-140
0 139
30
4-Chloroaniline
0 656
066
mg/Kg wet
167
394
10-140
125
30
V-34, J t
4-Chloro-3-methylphenol
1 13
066
mg/Kg wet
167
677
30-130
00295
30
2-Chloronaphthalene
0 816
034
mg/Kg wet
167
489
40-140
668
30
2-Chlorophenol
0 878
034
mg/Kg wet
167
527
30-130
134
30
4-Chlorophenylphenylether
109
034
mg/Kg wet
167
652
40-140
343
30
Chrysene
0 980
017
mg/Kg wet
167
58 8
40-140
0 407
30
Dibenz(a,h)anthracene
1 13
017
mg/Kg wet
167
677
40-140
998
30
Dibenzofuran
108
034
mg/Kg wet
167
648
40-140
162
30
Di-n-butylphthalate
1 11
034
mg/Kg wet
167
665
40-140
0 633
30
1,2-Dichlorobenzene
0 830
034
mg/Kg wet
167
498
40-140
13 7
30
1,3-Dichlorobenzene
0 812
034
mg/Kg wet
167
487
40-140
136
30
1,4-Dichlorobenzene
0 809
034
mg/Kg wet
167
486
40-140
144
30
3,3-Dichlorobenzidine
0 694
017
mg/Kg wet
167
417
20-140
174
50
t #
2,4-Dichlorophenol
0 959
034
mg/Kg wet
167
575
30-130
735
30
Diethylphthalate
1 14
034
mg/Kg wet
167
683
40-140
3 65
30
2,4-Dimethylphenol
0 928
034
mg/Kg wet
167
557
30-130
555
30
Dimethylphthalate
105
034
mg/Kg wet
167
632
40-140
00948
30
4,6-Dinitro-2-methylphenol
0 773
034
mg/Kg wet
167
464
30-130
258
30
2,4-Dinitrophenol
0 574
066
mg/Kg wet
167
344
30-130
5 10
30
1
2,4-Dinitrotoluene
0 942
034
mg/Kg wet
167
565
40-140
453
30
2,6-Dinitrotoluene
101
034
mg/Kg wet
167
606
40-140
0 920
30
Di-n-octylphthalate
1 16
034
mg/Kg wet
167
699
40-140
271
30
1,2-Diphenylhydrazine (as Azobenzene)
123
034
mg/Kg wet
167
735
40-140
0 382
30
Fluoranthene
0 954
017
mg/Kg wet
167
572
40-140
0 490
30
Fluorene
100
017
mg/Kg wet
167
600
40-140
178
30
Page 78 of 94

Table of Contents
con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
.nalyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B198559 - SW-846 3546
LCS Dup (B198559-BSD1)
Prepared: 03/09/18 Analyzed: 03/12/18
Hexachlorobenzene
0 978
034
mg/Kg wet
167
587
40-140
749
30
Hexachlorobutadiene
108
034
mg/Kg wet
167
646
40-140
109
30
Hexachlorocyclopentadiene
0 838
034
mg/Kg wet
167
515
40-140
5 14
30
Hexachloroethane
0 947
034
mg/Kg wet
167
568
40-140
152
30
Indeno(1,2,3-cd)pyrene
108
017
mg/Kg wet
167
650
40-140
713
30
Isophorone
118
034
mg/Kg wet
167
709
40-140
6 04
30
1-Methylnaphthalene
0 972
0 17
mg/Kg wet
167
583
40-140
406
30
2-Methylnaphthalene
0 969
0 17
mg/Kg wet
167
58 2
40-140
439
30
2-Methylphenol
0 938
034
mg/Kg wet
167
563
30-130
949
30
3/4-Methylphenol
0987
034
mg/Kg wet
167
592
30-130
5 02
30
Naphthalene
0 906
0 17
mg/Kg wet
167
543
40-140
740
30
2-Nitroaniline
125
034
mg/Kg wet
167
75 1
40-140
4 91
30
V-20
3-Nitroaniline
0 823
034
mg/Kg wet
167
494
30-140
938
30
f
4-Nitroaniline
0 952
034
mg/Kg wet
167
57 1
40-140
3 81
30
Nitrobenzene
1 12
034
mg/Kg wet
167
670
40-140
7 14
30
2-Nitrophenol
0 900
034
mg/Kg wet
167
540
30-130
7 06
30
4-Nitrophenol
125
066
mg/Kg wet
167
74 7
30-130
124
50
V-20
N-Nitrosodimethylamine
107
034
mg/Kg wet
167
644
40-140
997
30
V-20
N-Nitrosodiphenylamine
129
034
mg/Kg wet
167
774
40-140
2 65
30
N-Nitrosodi-n-propylamine
107
034
mg/Kg wet
167
642
40-140
867
30
Pentachloronitrobenzene
0 964
034
mg/Kg wet
167
579
40-140
108
30
V-16
Pentachlorophenol
0 819
034
mg/Kg wet
167
491
30-130
0 531
30
Phenanthrene
0 940
0 17
mg/Kg wet
167
564
40-140
222
30
Phenol
0 884
034
mg/Kg wet
167
530
30-130
119
30
Pyrene
100
0 17
mg/Kg wet
167
601
40-140
0 969
30
Pyridine
0 562
034
mg/Kg wet
167
337
30-140
13 6
30
V-05 t
1,2,4,5-Tetrachlorobenzene
108
034
mg/Kg wet
167
650
40-140
3 92
30
1,2,4-Trichlorobenzene
0 922
034
mg/Kg wet
167
553
40-140
758
30
2,4,5-Trichlorophenol
106
034
mg/Kg wet
167
635
30-130
4 14
30
2,4,6-Trichlorophenol
107
034
mg/Kg wet
167
642
30-130
139
30
Surrogate: 2-Fluorophenol
3.75
mg/Kg wet
667
562
30-130
Surrogate: Phenol-d6
3.88
mg/Kg wet
667
58 2
30-130
Surrogate: Nitrobenzene-d5
2.46
mg/Kg wet
333
739
30-130
Surrogate: 2-Fluorobiphenyl
2.37
mg/Kg wet
333
712
30-130
Surrogate: 2,4,6-Tribromophenol
4.70
mg/Kg wet
667
706
30-130
Surrogate: p-Terphenyl-dl4
2.28
mg/Kg wet
333
68 3
30-130
Matrix Spike (B198559-MSI)
Source: 18CO324-07
Prepared: 03/09/18 Analyzed: 03/12/18
Acenaphthene
108
021
mg/Kg dry
2 02
ND
53 1
40-140
Acenaphthylene
1 12
021
mg/Kg dry
202
ND
552
40-140
Acetophenone
1 12
041
mg/Kg dry
202
ND
552
40-140
Aniline
00506
041
mg/Kg dry
2 02
ND
2.50 *
40-140
MS-09, V-05, J
Anthracene
1 10
021
mg/Kg dry
202
ND
542
40-140
Benzidine
00142
080
mg/Kg dry
202
ND
0.700 *
40-140
MS-09, V-04,
V-05,J
Benzo(a)anthracene
1 14
021
mg/Kg dry
202
ND
564
40-140
Benzo(a)pyrene
1 10
021
mg/Kg dry
2 02
ND
543
40-140
Benzo(b)fluoranthene
109
021
mg/Kg dry
2 02
ND
53 8
40-140
Benzo(g,h,i)perylene
120
021
mg/Kg dry
202
ND
592
40-140
Benzo(k)fluoranthene
1 14
021
mg/Kg dry
2 02
ND
564
40-140
Benzoic Acid
160
12
mg/Kg dry
2 02
0 451
569
40-140
Bis(2-chloroethoxy)methane
128
041
mg/Kg dry
202
ND
633
40-140
Bis(2-chloroethyl)ether
106
041
mg/Kg dry
2 02
ND
523
40-140
Page 79 of 94

Table of Contents
con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
malyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B198559 - SW-846 3546
Matrix Spike (B198559-MSI)
Source: 18CO324-07
Prepared: 03/09/18 Analyzed: 03/12/18
Bis(2-chloroisopropyl)ether
121
041
mg/Kg dry
202
ND
598
40-140
Bis(2-Ethylhexyl)phthalate
157
041
mg/Kg dry
202
ND
777
40-140
4-Bromophenylphenylether
110
041
mg/Kg dry
202
ND
543
40-140
Butylbenzylphthalate
155
041
mg/Kg dry
202
ND
766
40-140
Carbazole
120
021
mg/Kg dry
202
ND
59 1
40-140
4-Chloroaniline
0 210
080
mg/Kg dry
202
ND
10.4 *
40-140
MS-09, R-06,
V-34, J
4-Chloro-3-methylphenol
137
080
mg/Kg dry
202
ND
676
30-130
2-Chloronaphthalene
0 896
041
mg/Kg dry
202
ND
443
40-140
2-Chlorophenol
0 977
041
mg/Kg dry
202
ND
483
30-130
4-Chlorophenylphenylether
130
041
mg/Kg dry
202
ND
641
40-140
Chrysene
114
021
mg/Kg dry
202
ND
564
40-140
Dibenz(a,h)anthracene
121
021
mg/Kg dry
202
ND
598
40-140
Dibenzofuran
119
041
mg/Kg dry
202
ND
590
40-140
Di-n-butylphthalate
134
041
mg/Kg dry
202
ND
662
40-140
1,2-Dichlorobenzene
0 883
041
mg/Kg dry
202
ND
436
40-140
1,3-Dichlorobenzene
0 832
041
mg/Kg dry
202
ND
41 1
40-140
1,4-Dichlorobenzene
0 838
041
mg/Kg dry
202
ND
414
40-140
3,3-Dichlorobenzidine
000648
021
mg/Kg dry
202
ND
0.320 *
40-140
MS-09, J
2,4-Dichlorophenol
108
041
mg/Kg dry
202
ND
533
30-130
Diethylphthalate
142
041
mg/Kg dry
202
ND
699
40-140
2,4-Dimethylphenol
107
041
mg/Kg dry
202
ND
53 1
30-130
Dimethylphthalate
1 17
041
mg/Kg dry
202
ND
577
40-140
4,6-Dinitro-2-methylphenol
0 843
041
mg/Kg dry
202
ND
417
30-130
2,4-Dinitrophenol
108
080
mg/Kg dry
202
ND
532
30-130
2,4-Dinitrotoluene
122
041
mg/Kg dry
202
ND
601
40-140
2,6-Dinitrotoluene
1 16
041
mg/Kg dry
202
ND
575
40-140
Di-n-octylphthalate
156
041
mg/Kg dry
202
ND
769
40-140
1,2-Diphenylhydrazine (as Azobenzene)
123
041
mg/Kg dry
202
ND
606
40-140
Fluoranthene
1 17
021
mg/Kg dry
202
ND
580
40-140
Fluorene
123
021
mg/Kg dry
202
ND
607
40-140
Hexachlorobenzene
107
041
mg/Kg dry
202
ND
527
40-140
Hexachlorobutadiene
128
041
mg/Kg dry
202
ND
633
40-140
Hexachlorocyclopentadiene
0 904
041
mg/Kg dry
202
ND
447
30-130
Hexachloroethane
0 994
041
mg/Kg dry
202
ND
491
40-140
Indeno(1,2,3-cd)pyrene
1 16
021
mg/Kg dry
202
ND
575
40-140
Isophorone
137
041
mg/Kg dry
202
ND
678
40-140
1-Methylnaphthalene
1 16
021
mg/Kg dry
202
ND
573
40-140
2-Methylnaphthalene
1 14
021
mg/Kg dry
202
ND
562
40-140
2-Methylphenol
104
041
mg/Kg dry
202
ND
512
30-130
3/4-Methylphenol
109
041
mg/Kg dry
202
ND
537
30-130
Naphthalene
106
021
mg/Kg dry
202
ND
522
40-140
2-Nitroaniline
134
041
mg/Kg dry
202
ND
664
40-140
V-20
3-Nitroaniline
0 724
041
mg/Kg dry
202
ND
358 *
40-140
MS-22
4-Nitroaniline
0 685
041
mg/Kg dry
202
ND
339 *
40-140
MS-09
Nitrobenzene
131
041
mg/Kg dry
202
ND
645
40-140
2-Nitrophenol
107
041
mg/Kg dry
202
ND
529
30-130
4-Nitrophenol
145
080
mg/Kg dry
202
ND
715
30-130
V-20
N-Nitrosodimethylamine
1 13
041
mg/Kg dry
202
ND
559
40-140
V-20
N-Nitrosodiphenylamine
134
041
mg/Kg dry
202
ND
662
40-140
N-Nitrosodi-n-propylamine
121
041
mg/Kg dry
202
ND
597
40-140
Pentachloronitrobenzene
1 18
041
mg/Kg dry
202
ND
583
40-140
V-16
Pentachlorophenol
1 10
041
mg/Kg dry
202
ND
545
30-130
Page 80 of 94

Table of Contents
con-testo
ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
malyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B198559 - SW-846 3546
Matrix Spike (B198559-MS1)
Source: 18CO324-07
Prepared: 03/09/18 Analyzed: 03/12/18
Phenanthrene
107
021
mg/Kg dry
202
ND
529
40-140
Phenol
100
041
mg/Kg dry
202
ND
496
30-130
Pyrene
135
021
mg/Kg dry
202
ND
669
40-140
Pyridine
00158
041
mg/Kg dry
202
ND
0.780 *
40-140
MS-09, V-05, J
1,2,4,5-Tetrachlorobenzene
110
041
mg/Kg dry
202
ND
543
40-140
1,2,4-Trichlorobenzene
104
041
mg/Kg dry
202
ND
513
40-140
2,4,5-Trichlorophenol
112
041
mg/Kg dry
202
ND
554
30-130
2,4,6-Trichlorophenol
1 11
041
mg/Kg dry
202
ND
550
30-130
Surrogate: 2-Fluorophenol
4.05
mg/Kg dry
8 10
501
30-130
Surrogate: Phenol-d6
4.26
mg/Kg dry
810
527
30-130
Surrogate: Nitrobenzene-d5
2.89
mg/Kg dry
405
713
30-130
Surrogate: 2-Fluorobiphenyl
2.34
mg/Kg dry
405
578
30-130
Surrogate: 2,4,6-Tribromophenol
5.89
mg/Kg dry
8 10
728
30-130
Surrogate: p-Terphenyl-d14
3.00
mg/Kg dry
405
740
30-130
Matrix Spike Dup (B198559-MSD1)
Source: 18CO324-07
Prepared: 03/09/18 Analyzed: 03/12/18
Acenaphthene
108
021
mg/Kg dry
202
ND
537
40-140
0 753
30
Acenaphthylene
1 12
021
mg/Kg dry
202
ND
557
40-140
0 533
30
Acetophenone
109
041
mg/Kg dry
202
ND
540
40-140
249
30
Aniline
00504
041
mg/Kg dry
202
ND
2.50 *
40-140
30
MS-09, V-05, J
Anthracene
107
021
mg/Kg dry
202
ND
533
40-140
201
30
Benzidine
00291
080
mg/Kg dry
202
ND
1.44 *
40-140
30
MS-09, V-04,
V-05,J
Benzo(a)anthracene
1 15
021
mg/Kg dry
202
ND
57 1
40-140
0 865
30
Benzo(a)pyrene
1 17
021
mg/Kg dry
202
ND
581
40-140
654
30
Benzo(b)fluoranthene
1 11
021
mg/Kg dry
202
ND
55 1
40-140
220
30
Benzo(g,h,i)perylene
1 14
021
mg/Kg dry
202
ND
564
40-140
5 18
30
Benzo(k)fluoranthene
1 19
021
mg/Kg dry
202
ND
58 8
40-140
384
30
Benzoic Acid
167
12
mg/Kg dry
202
0 451
605
40-140
421
30
Bis(2-chloroethoxy)methane
128
041
mg/Kg dry
202
ND
635
40-140
00172
30
Bis(2-chloroethyl)ether
101
041
mg/Kg dry
202
ND
502
40-140
443
30
Bis(2-chloroisopropyl)ether
1 14
041
mg/Kg dry
202
ND
565
40-140
604
30
Bis(2-Ethylhexyl)phthalate
161
041
mg/Kg dry
202
ND
799
40-140
246
30
4-Bromophenylphenylether
1 17
041
mg/Kg dry
202
ND
578
40-140
577
30
Butylbenzylphthalate
158
041
mg/Kg dry
202
ND
782
40-140
181
30
Carbazole
1 18
021
mg/Kg dry
202
ND
583
40-140
173
30
4-Chloroaniline
0 154
080
mg/Kg dry
202
ND
7.62 *
40-140
30.8
* 30
MS-09, R-06, J
4-Chloro-3-methylphenol
129
080
mg/Kg dry
202
ND
641
30-130
559
30
2-Chloronaphthalene
0 897
041
mg/Kg dry
202
ND
445
40-140
0 118
30
2-Chlorophenol
0 953
041
mg/Kg dry
202
ND
473
30-130
247
30
4-Chlorophenylphenylether
134
041
mg/Kg dry
202
ND
665
40-140
328
30
Chrysene
1 14
021
mg/Kg dry
202
ND
564
40-140
0 333
30
Dibenz(a,h)anthracene
1 15
021
mg/Kg dry
202
ND
569
40-140
527
30
Dibenzofuran
121
041
mg/Kg dry
202
ND
601
40-140
148
30
Di-n-butylphthalate
133
041
mg/Kg dry
202
ND
661
40-140
0 454
30
1,2-Dichlorobenzene
0 839
041
mg/Kg dry
202
ND
416
40-140
5 12
30
1,3-Dichlorobenzene
0 826
041
mg/Kg dry
202
ND
409
40-140
0 772
30
1,4-Dichlorobenzene
0 831
041
mg/Kg dry
202
ND
412
40-140
0 914
30
3,3-Dichlorobenzidine
000565
021
mg/Kg dry
202
ND
0.280 *
40-140
30
MS-09.. J
2,4-Dichlorophenol
109
041
mg/Kg dry
202
ND
542
30-130
142
30
Diethylphthalate
138
041
mg/Kg dry
202
ND
682
40-140
282
30
2,4-Dimethylphenol
103
041
mg/Kg dry
202
ND
51 1
30-130
406
30
Dimethylphthalate
123
041
mg/Kg dry
202
ND
608
40-140
490
30
Page 81 of 94

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Semivolatile Organic Compounds by GC/MS - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B198559 - SW-846 3546
Matrix Spike Dup (B198559-MSD1) Source: 18CO324-07 Prepared: 03/09/18 Analyzed: 03/12/18
4,6-Dinitro-2-methylphenol
0 800
041
mg/Kg dry
202
ND
396
30-130
530
30
2,4-Dinitrophenol
114
080
mg/Kg dry
202
ND
567
30-130
600
30
2,4-Dinitrotoluene
138
041
mg/Kg dry
202
ND
683
40-140
126
30
2,6-Dinitrotoluene
120
041
mg/Kg dry
202
ND
596
40-140
325
30
Di-n-octylphthalate
156
041
mg/Kg dry
202
ND
773
40-140
0 290
30
1,2-Diphenylhydrazine (as Azobenzene)
110
041
mg/Kg dry
202
ND
547
40-140
106
30
Fluoranthene
1 14
021
mg/Kg dry
202
ND
563
40-140
3 34
30
Fluorene
128
021
mg/Kg dry
202
ND
634
40-140
399
30
Hexachlorobenzene
102
041
mg/Kg dry
202
ND
506
40-140
432
30
Hexachlorobutadiene
127
041
mg/Kg dry
202
ND
630
40-140
0 745
30
Hexachlorocyclopentadiene
0 822
041
mg/Kg dry
202
ND
407
30-130
956
30
Hexachloroethane
0 993
041
mg/Kg dry
202
ND
492
40-140
0 129
30
Indeno(1,2,3-cd)pyrene
1 19
021
mg/Kg dry
202
ND
58 8
40-140
180
30
Isophorone
133
041
mg/Kg dry
202
ND
658
40-140
3 33
30
1-Methylnaphthalene
1 12
021
mg/Kg dry
202
ND
557
40-140
324
30
2-Methylnaphthalene
1 10
021
mg/Kg dry
202
ND
545
40-140
340
30
2-Methylphenol
0 979
041
mg/Kg dry
202
ND
485
30-130
567
30
3/4-Methylphenol
106
041
mg/Kg dry
202
ND
523
30-130
294
30
Naphthalene
106
021
mg/Kg dry
202
ND
524
40-140
00114
30
2-Nitroaniline
143
041
mg/Kg dry
202
ND
708
40-140
609
30
V-20
3-Nitroaniline
0 831
041
mg/Kg dry
202
ND
412
40-140
138
30
4-Nitroaniline
0 600
041
mg/Kg dry
202
ND
29.7 *
40-140
133
30
MS-09
Nitrobenzene
127
041
mg/Kg dry
202
ND
630
40-140
265
30
2-Nitrophenol
106
041
mg/Kg dry
202
ND
523
30-130
140
30
4-Nitrophenol
163
080
mg/Kg dry
202
ND
806
30-130
116
30
V-20
N-Nitrosodimethylamine
1 11
041
mg/Kg dry
202
ND
552
40-140
145
30
V-20
N-Nitrosodiphenylamine
126
041
mg/Kg dry
202
ND
623
40-140
643
30
N-Nitrosodi-n-propylamine
1 15
041
mg/Kg dry
202
ND
570
40-140
5 10
30
Pentachloronitrobenzene
109
041
mg/Kg dry
202
ND
542
40-140
755
30
V-16
Pentachlorophenol
105
041
mg/Kg dry
202
ND
520
30-130
503
30
Phenanthrene
106
021
mg/Kg dry
202
ND
523
40-140
155
30
Phenol
0 964
041
mg/Kg dry
202
ND
478
30-130
403
30
Pyrene
142
021
mg/Kg dry
202
ND
705
40-140
491
30
Pyridine
000444
041
mg/Kg dry
202
ND
0.220 *
40-140
30
MS-09, V-05, J
1,2,4,5-Tetrachlorobenzene
1 10
041
mg/Kg dry
202
ND
545
40-140
0 145
30
1,2,4-Trichlorobenzene
107
041
mg/Kg dry
202
ND
530
40-140
300
30
2,4,5-Trichlorophenol
1 14
041
mg/Kg dry
202
ND
566
30-130
174
30
2,4,6-Trichlorophenol
1 15
041
mg/Kg dry
202
ND
570
30-130
3 35
30
Surrogate: 2-Fluorophenol
3.94
mg/Kg dry
807
488
30-130
Surrogate: Phenol-d6
4.11
mg/Kg dry
807
510
30-130
Surrogate: Nitrobenzene-d5
2.90
mg/Kg dry
404
719
30-130
Surrogate: 2-Fluorobiphenyl
2.35
mg/Kg dry
404
58 1
30-130
Surrogate: 2,4,6-Tribromophenol
6.00
mg/Kg dry
807
743
30-130
Surrogate: p-Terphenyl-d14
3.26
mg/Kg dry
404
808
30-130
Page 82 of 94

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Petroleum Hydrocarbons Analyses - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B198557 - SW-846 3546
Blank (B198557-BLK1)
Prepared: 03/09/18 Analyzed: 03/11/18
Diesel Range Organics
ND
8 3
mg/Kg wet
Surrogate: o-Terphenyl
LCS (B198557-BS1)
3.37
mg/Kg wet
333 101
Prepared: 03/09/18 Analyzed: 03/11/18
40-140
Diesel Range Organics
285
83
mg/Kg wet
33 3 854
40-140
Surrogate: o-Terphenyl
LCS Dup (B198557-BSDI)
3.40
mg/Kg wet
333 102
Prepared: 03/09/18 Analyzed: 03/11/18
40-140
Diesel Range Organics
274
83
mg/Kg wet
33 3 823
40-140 3 75
Surrogate: o-Terphenyl
Batch B198651 - SW-846 5035/5030B
3.27
mg/Kg wet
333 981
40-140
Blank (B198651-BLK1)
Prepared & Analyzed: 03/12/18
Gasoline Range Organics (GRO)
ND
10
mg/Kg wet
Surrogate: 1-Chloro-3-fluorobenzene
LCS (B198651-BSI)
16.4
µg/L
150 109
Prepared & Analyzed: 03/12/18
70-130
Gasoline Range Organics (GRO)
0 250
0 010
mg/Kg wet
0 250 100
80-120
Surrogate: 1-Chloro-3-fluorobenzene
LCS Dup (B198651-BSD1)
19.2
µg/L
150 128
Prepared & Analyzed: 03/12/18
70-130
Gasoline Range Organics (GRO)
0 263
0 010
mg/Kg wet
0 250 105
80-120 484 30
Surrogate: 1-Chloro-3-fluorobenzene
16.1
µg/L
150 107
70-130
Page 83 of 94

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B198433 - % Solids
Blank (B198433-BLK1)
Prepared: 03/08/18 Analyzed: 03/09/18
% Solids
Blank (B198433-BLK2)
000
% Wt
Prepared: 03/08/18 Analyzed: 03/09/18
% Solids
Blank (B198433-BLK3)
000
% Wt
Prepared: 03/08/18 Analyzed: 03/09/18
% Solids
Blank (B198433-BLK4)
000
% Wt
Prepared: 03/08/18 Analyzed: 03/09/18
% Solids
Blank (B198433-BLK5)
000
% Wt
Prepared: 03/08/18 Analyzed: 03/09/18
% Solids
Duplicate (B198433-DUPB)
000
Source: 18CO324-01
% Wt
Prepared & Analyzed: 03/08/18
% Solids
863
% Wt
870 0 865 20
Page 84 of 94

Table of Contents
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ANALYTICAL LABORATORY
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
TCLP - Metals Analyses - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B198629 - SW-846 3010A
Blank (B198629-BLK1)
Prepared & Analyzed: 03/12/18
Arsenic
ND
0 010
mg/L
Barium
ND
0 050
mg/L
Cadmium
ND
00040
mg/L
Chromium
ND
0 010
mg/L
Lead
ND
0 010
mg/L
Selenium
ND
0 050
mg/L
Silver
ND
00050
mg/L
LCS (B198629-BS1)
Prepared & Analyzed: 03/12/18
Arsenic
0 557
0 010
mg/L
0 500 ill
80-120
Barium
0 513
0 050
mg/L
0 500 103
80-120
Cadmium
0 543
00040
mg/L
0 500 109
80-120
Chromium
0 508
0 010
mg/L
0 500 102
80-120
Lead
0 486
0 010
mg/L
0 500 973
80-120
Selenium
0 635
0 050
mg/L
0 500 127
* 80-120
L-02
Silver
0 552
00050
mg/L
0 500 110
80-120
LCS Dup (B198629-BSDI)
Prepared & Analyzed: 03/12/18
Arsenic
0 567
0 010
mg/L
0 500 113
80-120
190
20
Barium
0 523
0 050
mg/L
0 500 105
80-120
197
20
Cadmium
0 555
00040
mg/L
0 500 ill
80-120
2 15
20
Chromium
0 518
0 010
mg/L
0 500 104
80-120
190
20
Lead
0 494
0 010
mg/L
0 500 98 8
80-120
155
20
Selenium
0 665
0 050
mg/L
0 500 133
* 80-120
455
20 L-02
Silver
0 543
00050
mg/L
0 500 109
80-120
170
20
Batch B198633 - SW-846 7470A Prep
Blank (B198633-BLK1)
Prepared & Analyzed: 03/12/18
Mercury
0000045
000010
mg/L
J
LCS (B198633-BS1)
Prepared & Analyzed: 03/12/18
Mercury
000197
000010
mg/L
000200 985
80-120
LCS Dup (B198633-BSD1)
Prepared & Analyzed: 03/12/18
Mercury
000199
000010
mg/L
000200 993
80-120
0 779
20
Page 85 of 94

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ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
* QC result is outside of established limits
fi Wide recovery limits established for difficult compound
$ Wide RPD limits established for difficult compound
# Data exceeded client recommended or regulatory level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded
No results have been blank subtracted unless specified in the case narrative section
J Detected but below the Reporting Limit (lowest calibration standard); therefore, result is an estimated
concentration (CLP J-Flag)
L-02 Laboratory fortified blank/laboratory control sample recovery and duplicate recoveries outside of control limits
Data validation is not affected since all results are "not detected" for associated samples in this batch and bias is
on the high side
L-04 Laboratory fortified blank/laboratory control sample recovery and duplicate recovery are outside of control limits
Reported value for this compound is likely to be biased on the low side
L-07 Either laboratory fortified blank/laboratory control sample or duplicate recovery is outside of control limits, but
the other is within limits RPD between the two LFB/LCS results is within method specified criteria
MS-09 Matrix spike recovery and/or matrix spike duplicate recovery outside of control limits Possibility of sample
matrix effects that lead to a low bias for reported result or non -homogeneous sample aliquots cannot be
eliminated
MS-22 Either matrix spike or MS duplicate is outside of control limits, but the other is within limits RPD between the
two MS/MSD results is within method specified criteria
R-06 Matrix spike duplicate RPD is outside of control limits Reduced precision is anticipated for reported result for
this compound in this sample
V-04 Initial calibration did not meet method specifications Compound was calibrated using a response factor where
%RSD is outside of method specified criteria Reported result is estimated
V-05 Continuing calibration did not meet method specifications and was biased on the low side for this compound
Reported result is estimated
V-16 Response factor is less than method specified minimum acceptable value Reduced precision and accuracy may
be associated with reported result
V-20 Continuing calibration did not meet method specifications and was biased on the high side Data validation is nol
affected since sample result was "not detected" for this compound
V-34 Initial calibration verification (ICV) did not meet method specifications and was biased on the low side for this
compound Reported result is estimated
Page 86 of 94

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ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
Certifications
SW-846 6010C-D in Water
Arsenic
NY,CT,NC,ME,NH,VA
Barium
NY,CT,ME,NC,NH,VA
Cadmium
NY,CT,ME,NC,NH,VA
Chromium
NY,CT,ME,NC,NH,VA
Lead
NY,CT,ME,NC,NH,VA
Selenium
CT,ME,NCNH,NY,VA
Silver
CT,ME,NCNH,NY,VA
SW-846 7470A in Water
Mercury
CT,ME,NCNH,NY,VA
SW-846 801 SC in Soil
Gasoline Range Organics (GRO)
NY,VA,NH,NC
Diesel Range Organics
NY,VA,NH,NC
SW-846 8260B in Soil
Acetone
NC
Acrylonitrile
NC
tert-Amyl Methyl Ether (TAME)
NC
Benzene
NC
Bromobenzene
NC
Bromochloromethane
NC
Bromodichloromethane
NC
Bromoform
NC
Bromomethane
NC
2-Butanone (MEK)
NC
tert-Butyl Alcohol (TBA)
NC
n-Butylbenzene
NC
sec-Butylbenzene
NC
tert-Butylbenzene
NC
tert-Butyl Ethyl Ether (TBEE)
NC
Carbon Disulfide
NC
Carbon Tetrachloride
NC
Chlorobenzene
NC
Chlorodibromomethane
NC
Chloroethane
NC
Chloroform
NC
Chloromethane
NC
2-Chlorotoluene
NC
4-Chlorotoluene
NC
1,2-Dibromo-3-chloropropane (DBCP)
NC
1,2-Dibromoethane (EDB)
NC
Dibromomethane
NC
1,2-Dichlorobenzene
NC
1,3-Dichlorobenzene
NC
1,4-Dichlorobenzene
NC
trans-1,4-Dichloro-2-butene
NC
Dichlorodifluoromethane (Freon 12)
NC
1,1-Dichloroethane
NC
Page 87 of 94

con-testo
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
SW-846 8260B in Soil
1,2-Dichloroethane
1,1-Dichloroethylene
cis-1,2-Dichloroethylene
trans- l,2-Dichloro ethylene
1,2-Dichloropropane
1,3-Dichloropropane
2,2 Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Diethyl Ether
Diisopropyl Ether (DIPE)
1,4-Dioxane
Ethylbenzene
Hexachlorobutadiene
2-Hexanone (MBK)
Isopropylbenzene (Cumene)
p-Isopropyltoluene (p-Cymene)
Methyl tert-Butyl Ether (MTBE)
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Naphthalene
n-Propylbenzene
Styrene
1, 1, 1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethylene
Tetrahydrofuran
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,3,5-Trichlorobenzene
1, 1, 1 -Trichloroethane
1, 1,2 -Trichloroethane
Trichloroethylene
Trichlorofluoromethane (Freon 11)
1,2,3-Trichloropropane
1, 1,2-Trichloro- 1,2,2-trifluoroethane (Freon 113)
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl Chloride
m+p Xylene
o-Xylene
SW-846 8270D in Soil
Acenaphthene
Acenaphthylene
Certifications
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
NC
CT,NY,NH,ME,NC,VA
CT,NY,NH,ME,NC,VA
Page 88 of 94

con-testo
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte
Certifications
SW-846 8270D in Soil
Acetophenone
NY,NH,ME,NC,VA
Aniline
NY,NH,ME,NC,VA
Anthracene
CT,NY,NH,ME,NC,VA
Benzidine
CT,NY,NKNM,NC,VA
Benzo(a)anthracene
CT,NY,NH,ME,NC,VA
Benzo(a)pyrene
CT,NY,NH,ME,NC,VA
Benzo(b)fluoranthene
CT,NY,NH,ME,NC,VA
Benzo(g,h,i)perylene
CT,NY,NH,ME,NC,VA
Benzo(k)fluoranthene
CT,NY,NH,ME,NC,VA
Benzoic Acid
NY,NH,ME,NC,VA
Bis(2-chloroethoxy)methane
CT,NY,NH,ME,NC,VA
Bis(2-chloroethyl)ether
CT,NY,NH,ME,NC,VA
Bis(2-chloroisopropyl)ether
CT,NY,NH,ME,NC,VA
Bis(2-Ethylhexyl)phthalate
CT,NY,NH,ME,NC,VA
4-Bromophenylphenylether
CT,NY,NH,ME,NC,VA
Butylbenzylphthalate
CT,NY,NH,ME,NC,VA
Carbazole
NC
4-Chloroaniline
CT,NY,NH,ME,NC,VA
4-Chloro-3-methylphenol
CT,NY,NH,ME,NC,VA
2-Chloronaphthalene
CT,NY,NH,NC,VA
2-Chlorophenol
CT,NY,NH,ME,NC,VA
4-Chlorophenylphenylether
CT,NY,NH,ME,NC,VA
Chrysene
CT,NY,NH,ME,NC,VA
Dibenz(a,h)anthracene
CT,NY,NH,ME,NC,VA
Dibenzofuran
CT,NY,NH,ME,NC,VA
Di-n-butylphthalate
CT,NY,NH,ME,NC,VA
1,2-Dichlorobenzene
NY,NH,ME,NC,VA
1,3-Dichlorobenzene
NY,NH,ME,NC,VA
1,4-Dichlorobenzene
NY,NH,ME,NC,VA
3,3-Dichlorobenzidine
CT,NY,NH,ME,NC,VA
2,4-Dichlorophenol
CT,NY,NH,ME,NC,VA
Diethylphthalate
CT,NY,NH,ME,NC,VA
2,4-Dimethylphenol
CT,NY,NH,ME,NC,VA
Dimethylphthalate
CT,NY,NH,ME,NC,VA
4,6-Dinitro-2-methylphenol
CT,NY,NH,ME,NC,VA
2,4-Dinitrophenol
CT,NY,NH,ME,NC,VA
2,4-Dinitrotoluene
CT,NY,NH,ME,NC,VA
2,6-Dinitrotoluene
CT,NY,NH,ME,NC,VA
Di-n-octylphthalate
CT,NY,NH,ME,NC,VA
1,2-Diphenylhydrazine (as Azobenzene)
NY,NH,ME,NC,VA
Fluoranthene
CT,NY,NH,ME,NC,VA
Fluorene
NY,NH,ME,NC,VA
Hexachlorobenzene
CT,NY,NH,ME,NC,VA
Hexachlorobutadiene
CT,NY,NH,ME,NC,VA
Hexachlorocyclopentadiene
CT,NY,NH,ME,NC,VA
Hexachloroethane
CT,NY,NH,ME,NC,VA
Indeno(1,2,3-cd)pyrene
CT,NY,NH,ME,NC,VA
Page 89 of 94

con-testo
ANALYTICAL LABORATORY
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
SW-846 8270D in Soil
Isophorone
CT,NY,NH,ME,NC,VA
1-Methylnaphthalene
NC
2-Methylnaphthalene
CT,NY,NH,ME,NC,VA
2-Methylphenol
CT,NY,NH,ME,NC,VA
3/4-Methylphenol
CT,NY,NH,ME,NC,VA
Naphthalene
CT,NY,NH,ME,NC,VA
2 Nitroaniline
CT,NY,NH,ME,NC,VA
3-Nitroaniline
CT,NY,NH,ME,NC,VA
4-Nitroaniline
CT,NY,NH,ME,NC,VA
Nitrobenzene
CT,NY,NH,ME,NC,VA
2-Nitrophenol
CT,NY,NH,ME,NC,VA
4-Nitrophenol
CT,NY,NH,ME,NC,VA
N-Nitrosodimethylamine
CT,NY,NH,ME,NC,VA
N-Nitrosodiphenylamine
CT,NY,NH,ME,NC,VA
N-Nitrosodi-n-propylamine
CT,NY,NH,ME,NC,VA
Pentachloronitrobenzene
NY,NC
Pentachlorophenol
CT,NY,NH,ME,NC,VA
Phenanthrene
CT,NY,NH,ME,NC,VA
Phenol
CT,NY,NH,ME,NC,VA
Pyrene
CT,NY,NH,ME,NC,VA
Pyridine
CT,NY,NH,ME,NC,VA
1,2,4,5-Tetrachlorobenzene
NY,NC
1,2,4-Trichlorobenzene
CT,NY,NH,ME,NC,VA
2,4,5-Trichlorophenol
CT,NY,NH,ME,NC,VA
2,4,6-Trichlorophenol
CT,NY,NH,ME,NC,VA
2-Fluorophenol
NC
The CON -TEST Environmental Laboratory operates under the
following certifications and accreditation:
Code Description
Number
Expires
AIHA AIHA-LAP, LLC - ISO17025:2005
100033
03/l/2020
MA Massachusetts DEP
M-MA100
06/30/2018
CT Connecticut Department of Publilc Health
PH-0567
09/30/2019
NY New York State Department of Health
10899 NELAP
04/1/2018
NH-S New Hampshire Environmental Lab
2516 NELAP
02/5/2019
RI Rhode Island Department of Health
LA000112
12/30/2018
NC North Carolina Div of Water Quality
652
12/31/2018
NJ New Jersey DEP
MA007 NELAP
06/30/2018
FL Florida Department of Health
E871027 NELAP
06/30/2018
VT Vermont Department of Health Lead Laboratory
LL015036
07/30/2018
ME State of Maine
2011028
06/9/2019
VA Commonwealth of Virginia
460217
12/14/2018
NH-P New Hampshire Environmental Lab
2557 NELAP
09/6/2018
VT-DW Vermont Department of Health Drinking Water
VT-255716
06/12/2018
NC-DW North Carolina Department of Health
25703
07/31/2018
Page 90 of 94

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Page 92 of 94

3171201 &
Track your package or shipment with FedEx Trooping
Table of Contents
V. C_'' .�
IMPORTANTt
FedEx is closely monitoring the Minter storms across the U.S. Learn Mori
Raleigh, NC US Delivered EAST LONGMEADOW, MA € -S
Signed Ia r b},: J, OE 7A7 RA S
Travel history
s DateMme
Activity
Location
3fU7l2015
-Wednesday
1Q:49 am
Delivered
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On FedExvehiclefordelivery
t�74PPDRLCCL=.�T
8,15am
At local FedExtactilty
V'NO3UKLMKR;.(.T
8:24 am
At destination 5ori facility
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Departcd FedEx (oration
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1,07 am
Arrivod nt Fed Cox location
1'4DjAhN?oLjs, IN
w N06)20 i 8
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4:22 pm
Picked up
ruaE16H. hr,
3,02 pm
Shlprnent information sent to FedEx
Shipment racts
Tracking Number
r7173449G441
Service
FedEx Prior -sty Overnight
Weight
36.6 lhs i 16.6 kgs
Dimensions
24xl4xl4 in.
Delivered To
ShippingR6('Biong
Total pieces
1
Total shipment weight. 35.6 IM 116,6 kgs
Terms
Third Party
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Paokaging
Your Packaging
Spec ia€ handling
DeliverWeekday, Additional
Standard
3107l2018 by 10:30 am
section
Handling Surcharge
transit
OUR cOMP&NV
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Our PorifoG4
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Page 93 of 94

Table of Contents
s:MMLE-Est I
...........
L❑gin Sample Receipt Checklist - (Rejection Criteria Listing - Using Acceptance Policy) Any False
Statement will be brought: to the attention of the Client - State True or False
Client _ __e�
Deceived By
Bate ' I � 1.(._ , Time f L)f 7
How were the samples In Cooler + No Cooler On Ice l No Ice
received? Direct from Sampling Ambient Melted Ice
By Gun # K- 7 Actual Temp
Were samples within
Temperature? 2-6'C
By !sank #
Actual 'Temp -
Was Custody Seal Intact?
I VYr-
Were Samples Tampered with? j�
Was COC Relinquished ?
-T—
Does Chain Agree With Samples? -f —
Are there broken/leaking/loose caps
an any samples?
7
Is CCC in ink/ Legible? i
Were samples received within holding tame? i
Did COC include all Client
Analysis Sampler Name
pertinent information? Project
T.,
ID's -- Collection Dates/Times
Are Sample labels tilled out and legible?
Are there Lab to Filters?
Who was notified?
Are there Rushes?
Who was notified?
Are there Short Holds?
�_
Who was notified?
Is there enough Volume?"
Is there Headspace where applicable?
i -
MSfMSD? ,
Proper Media/Containers Used?
Is splitting sales required?
Were trip blanks received?
On COG?
Do all samples have the proper pH?
h p�-
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comments:
Page 94 of 94 1