MO-4617_15621_CA_LSA_20191015_Limited Site Assessment

Nova
Group
October 15, 2019
Tige Darner
Tar Heel Capital Corp No. 2
166 Southgate Drive
Boone, NC 28607
RE: PHASE II LIMITED SITE ASSESSMENT
AL'S AUTO / HARRISBURG PHILLIPS 66
4960 NC HWY 49
HARRISBURG, NORTH CAROLINA 28075
DEQ INCIDENT # 15621
AMA PiR(iJECT NO.119-5100
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W I - UN
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Nova Group GBC (Nova) is pleased to present this Limited Site Assessment (LSA) for the
referenced location (Site). The objective of this LSA was to evaluate the shallow soils and
groundwater on the Property and perform a receptor survey to determine if there was
anntaminatinn on site from former petroleum sales. Based on the results of this
investigation, there is minor dissolved shallow groundwater contamination below gross
contaminant levels, and the soil contamination documented is below residential standards
and only one location with one analyte exceeds the soil to groundwater concentrations.
Thank you for choosing Nova to assist you with this project If you have any questions, please
Luftacta at 704 258-5196.
Sincerely,
NOVA CONSULTING GROUP, INC.
`,% ✓.., ems'-�;e..%lam!/
Mike Minett
Vice President
Licensed Geologist
442 SOUTH MAIN ST. STE #i 7, DAVIDSON SAC 2803b

PHASE II LIMITED SITE ASSESSMENT
AL'S AUTO / HARRISBURG
4960 NC HWY 49
HARRISBURG, NC 28075
OCTOBER 15, 2019
NOVA PROJECT NO. J19-5100
NCDEQ INCIDENT # 15621
PREPARED FOR:
TRUDY BEVERLY, L.G.
NCDEQ MOORESVILLE REGIONAL OFFICE
610 EAST CENTER AVENUE
MOORESVILLE, NC 28115
PREPARED BY:
NOVA GROUP GBC
442 SOUTH MAIN ST. STE # 7,
DAVIDSON NC 28036
[phone]
ask, Nova
70, Croup

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70NIC , s,
Executive Summary
Nova prepared a Phase I Environmental Site Assessment for the Property that included the following
recognized environmental conditions (RECs) " Law Engineering (LAW) conducted soil sampling in August
1990 and installed eight soil borings around the former UST excavations. Three samples were above the
total petroleum hydrocarbon (TPH) action level (at that time) of 10 mg/Kg. One sample collected at B-3
was 290 mg/Kg in the gasoline range.
Another sampling round, conducted by LAW dated November 9, 1990, indicated that contaminated soils
had been removed to a depth of 14 feet below land surface (BLS). Confirmation soil sampling did
not identify soil samples with TPH concentrations above the action limit of 10 mg/Kg. LAW also had two
composite samples from the removed soils that were over the 10 mg/Kg threshold. LAW segregated the
soils after the excavation and did not provide details of the fate of the removed soils, or whether
segregated soils (with a photoionization detector [PID]) were placed back into the excavation. The tanks
were reportedly removed in 1989.
An NOV issued by the North Carolina Department of Environment and Natural Resources (NCDENR,
predecessor to the NCDEQ) and dated April 24, 1992, responded to a site inspection showing
contaminated soil on the ground behind the garage at the Property. "
On August 20, 1996, NCDENR sent a letter stating that the site was now listed as an E ranking for
contaminated soils remaining under the former gasoline and kerosene tanks, (following the November
1990 report), but that a no Notice of Violation (NOV) or Notice of Regulatory Requirement (NORR) was
issued due to a new law using risk -based rule implemented. This is an open incident and a REC to the
Property.
Based on the two areas (former tank pit) and former waste oil tank surficial staining, a Phase II was
conducted by Nova. The Phase II documented a groundwater impact by the former diesel dispenser
location of 237 micrograms per liter ( Ug/L) benzene in the groundwater near the former diesel
dispenser; at 2.2 Ug/L benzene in the groundwater near the former waste oil tank; and non -detect
benzene in a downgradient area of the ASTs. In the area around the former diesel dispenser there was
also soil contamination documented at 16' bls (180 ppm TPH DRO and 1340 TPH GRO). This area was
either within the aquifer, or at the capillary fringe.
Nova reviewed the documents available on the DEQ Laserfiche website and produced the following
conclusions:
Site Name: Harrisburg Texaco or Harrisburg 76. Site Address: Listed as 143 Hwy 49, Harrisburg
Site Owner / Operator: Horace Hart. Facility ID: 0-004568 Incident Number 15621
These relate to the operation and removal of four underground storage tanks. There were several
"Notices of Violation" issued by DENR for contaminated soils remaining.
The Site had several storage tanks that were removed in the early 1990's. There were at least
two reports that documented releases, and contaminated soils remaining on the Property.
Nova did not review any documents that provided groundwater information. In 1992, DENR
sent a letter to Mr. Hart stating that the risk priority on the Site was E and that further
remediation timeframes were suspended. This means that Mr. Hart (now deceased) is the
PHASE II LIMITED SITE ASSESSMENT i AUS AUTO/HARRISBURG
PAGE i PROJECT NO. J19-5100

-00L J
responsible party for the onsite petroleum contamination, and possible off -site migration of
dissolved petroleum groundwater contamination.
In August 2019, Nova mobilized to the Site to install and sample three temporary monitoring
wells, TMW-1, TMW-2, and TMW-3 near the northern site boundary. Following that
sampling and analysis, Nova returned again and installed two source wells (gasoline and
diesel USTs), labelled MW-1 and MW-2, and one upgradient well MW-3; measured
groundwater elevation and submitted soil and groundwater samples for analysis.
This report includes the data generated by Nova, historic site documentation, and a receptor
survey conducted by Nova.
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TABLE OF CONTENTS
1.0 INTRODUCTION.......................................................................................................... 1
1.1
Background.........................................................................................................................1
1.2
Scope of Services................................................................................................................1
2.0 FIELD ACTIVITIES........................................................................................................ 2
2.1
Monitoring Well Locations..................................................................................................2
2.2
Monitoring Well Installation Procedures............................................................................2
2.3
Field Screening....................................................................................................................3
2.4
Soil Laboratory Analyses.....................................................................................................3
2.5
Groundwater Laboratory Analyses.....................................................................................3
3.0 RESULTS.....................................................................................................................5
3.1 Geology and Site Conditions...............................................................................................5
3.2 Potentiometric Surface.......................................................................................................5
3.3 Field Screening....................................................................................................................5
3.4 Chemical Analyses...............................................................................................................5
4.0 RECEPTOR SURVEY..................................................................................................... 7
5.0 DISCUSSION............................................................................................................... 9
6.0 SOIL MANAGEMENT PLAN........................................................................................ 10
7.0 CONCLUSIONS AND RECOMMENDATIONS................................................................ 11
TABLES
1. Groundwater MADEP Results
2. Identified Water Wells
FIGURES
1. Site Location Plan
2. Boring Location Plan
3. Historic Boring Location Plan
4. Potentiometric Elevations
5. Topographic Map
6. Dissolved Benzene Groundwater Concentrations
7. Dissolved Naphthalene Groundwater Concentrations
8. City Water Line Plan
9. Site Receptor Plan
APPENDICES
A.
Photo Log
B.
Soil Boring Logs
C.
Analytical Summary Tables
D.
Laboratory Analytical Data
E.
Receptor Survey
F.
LSA Questionnaire
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4106 Nova
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1.1 Background
Nova has conducted three rounds of sampling and analysis on the Site since June 2019. The latest data
generated was in September 2019. This report has been prepared to provide North Carolina Department
of Environmental Quality (DEQ) with sufficient information to rank the Site, ideally with a no further
action by the filing of a notice of residual petroleum (NRP) with groundwater use restricted.
1.2 Scope of Services
The environmental services that Nova provided for this project included:
• Clear unmarked utilities in the boring locations.
• An initial round of seven soil borings, and collection of groundwater samples from three
locations (GW-A, GW-B, and GW-C) in June 2019.
• Install three soil borings to and converted them to temporary monitoring wells (TMW-
1, TMW-2 and TMW-3) in August 2019.
• Install three permanent groundwater monitoring wells (MW-1, MW-2, and MW-3) and
collect soil and groundwater samples (September 2019).
• Perform a walking reconnaissance within 500' radius, and a vehicular survey to 1500'
radius to identify potential well locations.
• Measure the elevation of the three permanent monitoring wells, and three temporary
monitoring wells, and measure depth to groundwater in those wells (September 2019).
• Send out well survey letters to property owners within 1,000 feet radius from the
contaminant source area.
• Map the location of all addresses within 1500 feet radius, and determine that municipal
water is universally available, and required to be hooked up.
• Preparation of this report. A Site Location Plan is included as Figure 1.
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4106 Nova
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2.1 Monitoring Well Locations
Nova completed three temporary monitoring wells (labeled TMW-1. TMW-2 and TMW-2) at
the Site on August 5, 2019. The three wells were installed as follows:
• Temporary Monitoring Well TMW-1 was located downgradient (east) of the former
diesel dispenser and SB-3.
• Temporary Monitoring Well TMW-2 was located downgradient (east) of the S13-1 and
the service bays.
• Temporary Monitoring Well TMW-3 was located downgradient (east) of the former and
current waste oil UST/ASTs and SB-1.
Nova completed three permanent monitoring wells (labeled MW-1, MW-2, and MW-3) at the
site on September 6, 2019. The three wells were installed as follows:
• Monitoring well MW-1 was installed in the area of the former diesel tank / dispenser;
• Monitoring well MW-2 was installed in the area of the former gasoline underground
storage tanks; and
• Monitoring well MW-3 was installed in an upgradient location to the two source wells.
A map depicting the soil boring locations (including the July 2019 soil borings) is included as
Figure 2. A map showing the former UST and historic sampling (circa 1990) locations is
included as Figure 3.
2.2 Monitoring Well Installation Procedures
The soil borings were completed using a truck mounted Geoprobe® Model 6250 Hydraulic
push probe. A Geoprobe® Macro -Core sampler was used to collect the soil samples from the
borings at continuous four -foot intervals to a depth of up to 20 feet below land surface (bls).
The Macro -Core sampler consists of a 3.25-inch outside diameter, 48-inch long nickel -plated
alloy -steel sampling tube that is continuously filled with soil as it is pushed and/or hammered
to the termination depth of the borings.
The 1 inch diameter temporary wells were installed with 10 feet of .010' screen, and finished
to above grade with solid riser. Well pack gravel was used to one foot above the screen level,
and the boring filled with hydrated bentonite to surface. The wells were marked, and flagged,
locked, and placed within used auto tires to protect them.
The 1 inch diameter permanent wells were installed with 10 feet of .010' screen, and finished
to 3" below grade with solid riser. Well pack gravel was used to one foot above the screen level,
PHASE II LIMITED SITE ASSESSMENT 2 AL'S AUTO/HARRISBURG
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4106 Nova
7A! Group
and the boring filled with hydrated bentonite to 18" below grade, and finished with grout,
locking well plugs, and a manhole. The wells were marked, and locked.
An environmental scientist recorded a physical description of the soils encountered at each
boring location on a field -boring log. A Photo Log is included as Appendix A. The boring logs
are included as Appendix B.
2.3 Field Screening
The Nova environmental scientist also screened the soil samples collected during the
completion of the soil borings for indications of contamination. The soil samples were
evaluated for the presence of unusual odors and staining. Additionally, the soil samples were
screened for the presence of organic vapors using an MicroFID photoionization detector (PID).
The PID was equipped with a 10.2 eV lamp and was calibrated to an isobutylene standard prior
to being used at the Site. The soil samples were screened utilizing the headspace field analysis
technique.
The headspace technique consists of half -filling a quart sized zip -lock bag with a soil sample
and quickly sealing the bag. Headspace development proceeds for at least 10 minutes. The bag
is shaken vigorously for 15 seconds, at both the beginning and the end of the headspace
development period. After headspace development, the bag is opened slightly and the PID
probe is inserted to one-half the headspace depth. The highest reading observed on the PID is
then recorded.
2.4 Soil Laboratory Analyses
The soil samples (June data) were placed in laboratory -supplied containers, stored in a cooler,
and transported to Pace Analytical Inc., in Huntersville, North Carolina using chain -of -custody
procedures. Pace Analytical is certified to analyze samples collected in the State of North
Carolina. The soil samples were chemically analyzed for the presence and concentration of
Total Petroleum Hydrocarbon (TPH) diesel range organics (DRO) compounds, and gasoline
range organics (GRO) compounds, and PCBs in two of the samples. One sample was also
analyzed for volatiles and semivolatiles by EPA methods 8260 / 8270.
The soil samples (September data) from seemingly contaminated profiles were collected from
Monitoring wells MW-1 and MW-2. Monitoring well MW-1 had an approximately eight feet
vertical profile of seemingly contaminated soils (two samples), while MW-2 was clean fill to 14'
bls and only one sample was collected below that. The three soil samples were analyzed for
volatiles and semivolatiles by EPA methods 8260 / 8270. No samples were collected from MW-
3 (upgradient well) as there were no field indictors of contamination. Summary tables of soil
and groundwater analytical data is included in Appendix C.
2.5 Groundwater Laboratory Analyses
Groundwater samples were collected from four locations in the initial (June data) sampling
event. The groundwater samples were placed in laboratory -supplied containers, stored in a
cooler, and transported to Pace Analytical Inc., in Huntersville, North Carolina using chain -of -
PHASE II LIMITED SITE ASSESSMENT 3 AL'S AUTO/HARRISBURG
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4106 Nova
1At Group
custody procedures. Pace Analytical is certified to analyze samples collected in the State of
North Carolina. The four groundwater samples were analyzed for volatiles and semivolatiles by
EPA methods 8260 / 8270. The laboratory data for the three rounds of Nova sampling is
included as Appendix D.
Groundwater samples were collected from the three temporary monitoring well locations
(August 2019 data). The groundwater samples were placed in laboratory -supplied containers,
stored in a cooler, and transported to Pace Analytical Inc., in Huntersville, North Carolina using
chain -of -custody procedures. Pace Analytical is certified to analyze samples collected in the
State of North Carolina. The three groundwater samples were analyzed for volatiles and
semivolatiles by EPA methods 8260 / 8270, and MADEP EPH/VPH, and total lead.
Groundwater samples (September 2019 data) were collected from the three permanent
monitoring wells (September data) using the same procedures. The samples were analyzed for
EPA methods 8260 / 8270. The laboratory data is included as Appendix D.
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4106 Nova
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3.1 Geology and Site Conditions
Soil boring logs with descriptions of the encountered materials and water level information are
contained in Appendix B. Also shown are the PID results. There was no staining or odor in
TMW-1. The soils from TMW-2 and TMW-3, MW-1 and MW-2 all exhibited apparent staining
and petroleum odor.
3.2 Potentiometric Surface
Nova returned to the site on September 19, 2019 to measure the rim elevations on the
temporary and permanent monitoring wells, and depth to water in the same wells.
An arbitrary height of 100 feet was established for MW-2 north rim elevation, and the other
wells were assigned their elevations with respect to MW-2. An interface probe was used to
measure depth to water in the wells. The depth to water was subtracted from the rim elevation,
and the groundwater elevation was determined. The data was mapped and shown on Figure 4.
Surface water drains on the north side of Hwy 49 to the Rocky River. The area to the south of
Hwy 49 drains to Back Creek. A topographic map of the area is included as Figure S.
3.3 Field Screening
Field screening of the soil samples collected from the six soil borings in June indicated PID
results below 5 ppm and are generally considered background.
Field screening of the soil samples collected from the three permanent monitoring wells in June
measured the highest PID readings near or below the capillary fringe (1580 ppm) in SB-1 / MW-
1 at a depth of 18 feet. Groundwater later came up in the well to a depth of 16 feet.
In SB-2 / MW-2 there was a PID response of 7 at 10 feet, then 0 at 15 feet, and 75 at 17 feet in
the capillary fringe.
There were no PID detections in SB-3 / MW-3. Soil boring logs including PID screening results
are contained in Appendix B.
3.4 Chemical Analyses
The soil analytical data is summarized in Tables 1 and 2. The only analyte specific exceedance
of soil -to -water data occurred in MW-1 for 1-Methyl Naphthalene. There were no exceedances
of residential standards for soils. The data is included in Appendix C.
The chemical detections for groundwater using MADEP analysis is shown below.
PHASE II LIMITED SITE ASSESSMENT 5 AL'S AUTO/HARRISBURG
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4106 Nova
7A! Group
Table 1
MADEP Groundwater Analytical Results
Parameter
Units
TMW-1
TMW-2
TMW-3
NCAC 2L
Aliphatic C05-008
u /L
BDL
147
6600
400
Aliphatic (C09-C12)
ug/L
BDL
1270
3390
700
Aliphatic C09-C18
u /L
BDL
163
236
700
Ali hatic C09-C12 Adjusted
u /L
BDL
502
1920
700
Aromatic (C09-C10)
ug/L
BDL
768
1480
200
Aromatic C11-C22
u /L
BDL
223
278
200
Analyte specific groundwater data is contained in Table 3, Appendix C. There were no
exceedances of the gross contaminant levels (GCLs) in the data generated. In the volatile range,
xylenes were the highest concentration measured at 26,700 micrograms per liter (ug/L) in MW-
A. Benzene was the highest ratio of concentration to MCL with a concentration of 2,380 in MW-
2 compared to an MCL of 1 (and a GCL of 5,000).
Naphthalene exceedances were in the 200 ug/L range in MW-1 and MW-2, with a highest
concentration measured in GW-B at 756 ug/L. It should be noted that cross -gradient wells
TMW-2 and TMW-3 did not have benzene concentrations above the MCL, and were only slightly
above the MCL for naphthalene, at 12.3 and 10.5 ug/L respectively.
A figure was prepared showing dissolved groundwater benzene concentrations, which is
included as Figure 6. A similar map (figure 7) was prepared for naphthalene.
PHASE II LIMITED SITE ASSESSMENT 6 AL'S AUTO/HARRISBURG
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4106 Nova
7A! Group
Nova contacted the Cabarrus County Health Department to determine if there were any
registered water wells in the area. Mr. Troutman responded with an email capturing the data.
Nova reviewed that data (included in Appendix E) and determined that none were within 1500
feet of the site.
Nova also obtained a map from Mr. Troutman showing the municipal water supply lines in the
area of the Site. Mr. Troutman stated that everyone in the town of Harrisburg is required to
connect to city water and sewer, and those became available in the area in the 1950's and
1960's. The water lines are shown Figure 8.
Nova researched property ownership on MyCabarrus.com (GIS platform) and produced a map
showing the property parcels within 1500 feet of the site and numbered those parcels. The
numbers coincide to the spreadsheet showing the location of the residence or business, and the
name and address of the property owners. This information is contained in the Receptor Survey
Appendix. A map showing the Nova assigned number to each parcel, and the radius information
is included in Figure 9. The table showing the results of the survey is included in the Receptor
Survey Appendix E.
Registered letters were sent to every parcel within a 1,000-foot radius to ask whether there
were water wells on their respective parcels. Copies of the letters are contained in Appendix E.
There were ninety-four separate parcels within a 1,000-foot radius. It should be noted that the
parcels on the south side of Highway 49 are in a separate watershed that drains to the south
towards Back Creek. The parcels to the north of Highway 49 drain to the north towards the
Rocky River. Of the 94 requests for information, Nova received 40 responses, and an additional
10 letters returned. The returned letters were originally sent to the Property owner (as shown
in the Harrisburg GIS system) and once returned; they were resent to the Property address, but
there were no responses.
The receptor survey determined that the closest water well is an irrigation well at
approximately 325 feet down -gradient from the contaminant source area. There were several
other wells identified within the 1,000-foot radius. The wells identified are as follows:
Table 2
Identified Water Wells From Well Survey
Distance
from
Nova
contaminant
Map #
Location
Owner
Use
source
Gradient
18
205 MORRIS DR
LONG ALFARD L
Used for irrigation
325'
Down
HARRISBURG NC 28075
/ swimming pool
27
138 PLAZA DR
LOVE MIKE
irrigation
500,
Down
HARRISBURG NC 28075
DELVERT
31
218 PLAZA DR
BOOTH GEORGE
Irrigation, and
700'
Down
HARRISBURG NC 28075
A
general use
PHASE II LIMITED SITE ASSESSMENT 7 AL'S AUTO/HARRISBURG
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4106 Nova
7A! Group
Table 2
Identified Water Wells From Well Survey
51
125 OAKLEY DR
WARD JANE F
Well is not used,
450'
Up, and separate
HARRISBURG NC 28075
but not properly
watershed
abandoned
57
126 OAKLEY DR
LEWIS RICKARD A
City water, but has
550'
Up, and separate
HARRISBURG NC 28075
an 180' well used
watershed
for garden only.
Also connected to
118 Oakley (same
parcel)
88
216 PARALLEL DR
BAKER CHARLIE F
Irrigation, and
950'
Down gradient
HARRISBURG NC 28075
general use
24
313 Morris Drive,
Joe Martin
Irrigation and car
1,000' +
Down gradient
Harrisburg NC 28075
washing
PHASE II LIMITED SITE ASSESSMENT 8 AL'S AUTO/HARRISBURG
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4106 Nava
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The data shows no detectable impact to groundwater at TMW-1, GW-13 and GW-C at cross to
down -gradient locations for the analytes tested. The upgradient well (MW-3) also had no
detectable impact to shallow groundwater for the analytes tested.
The MADEP EPH and VPH analyses are considered by many to be duplicative to the analyte
specific values previously discussed. There are no Gross Contaminant Levels, and the analytical
results were typically within an order of magnitude (i.e. 1OX) of the North Carolina
groundwater standard as listed under 15A NCAC 2L .O2O2(2L).
The benzene to xylene ratios showing an order of magnitude ratio xylene enrichment in MW-1
and MW-2, i.e. 200 ug/L benzene in MW-1 to 5,710 total xylenes in the same sample to two
orders of magnitude in the sample collected from MW-13 (237 benzene to 21,700 ug/L xylenes).
This is indicative of a weathered gasoline degradation.
Lead was tested in TMW-1,2, and 3 with the sample analyzed from TMW-3 was 20.8 ug/L for
lead and TMW-2 was 10.4 which is above the 2L standard of 15 ug/L. No lead was detected in
TMW-1.
The only specific analyte that exceed 21, standards in TMW-2 analysis was for naphthalene,
which was detected at 36.3 ug/L which is above the 2L standard of 6.0.
The sample analyzed from TMW-3 had two detections above 21, standards. The highest
exceedance was 20.8 ug/L for lead which is above the 2L standard of 15ug/L followed by
naphthalene detection at 14.9 ug/L.
There are also naphthalene exceedances that vary when viewed as a volatile or semi -volatile
organic compound. In general, monitoring wells MW-1 and MW-2 appear to be a naphthalene
source with concentrations in the 200 ug/L range when measured in the volatile range. The
semi -volatile range concentrations were in the 60 to 80 ug/L range.
There appears to be a small co -mingled groundwater dissolved contaminant plume that is being
enriched with residual soils at or near the water table.
The receptor survey shows the entire area hooked up to the municipal water supply, as
required. There are some remaining irrigation wells, likely from the time before municipal
water was available. The nearest irrigation well is over 325 feet away. Considering the
contaminant plume appears to be predominantly on the Site, Nova considers it very unlikely
that the off -site wells would be contaminated.
PHASE II LIMITED SITE ASSESSMENT 9 AL'S AUTO/HARRISBURG
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4106 Nova
7A! Croup
The site is currently below grade approximately four feet at the current building footprint. The
plan is to raze the building and fill that area of the site to grade. The current documented soil
contamination is below the residential standards and will have at least ten feet of clean soil
above any impacted soils discovered to date.
The prospective developer plans to do some source removal / remediation on a voluntary basis.
We currently envision the demolition of the building and other structures on the Property
followed by:
1. Removal of the pavement, and current slab foundation.
2. Overburden soils will be excavated in the areas of Monitoring wells MW-1, and MW-2,
and TMW-2 and TMW-3 to a depth of between 8 and 14' bls.
3. Any stained or soils with an odor will remain in place until Nova is on site to field screen
the soils.
4. Once the overburden is removed, Nova will be on site for additional removal of
potentially impacted soils.
5. The soils will be screened with a PID and excavated to a depth to intersect the water
table.
6. The contaminated soils will be stockpiled, and properly disposed as petroleum
contaminated.
7. Nova anticipates removal of up to 300 tons of potentially contaminated soil in three
areas. The open excavations will be treated with Regenesis Petrofix, or other oxidation
compound to improve biodegradation. If required, Nova will obtain a 5I injection
permit.
8. Nova anticipates up to 2,000 pounds of soil amendments (Regenesis) to address residual
contamination in the capillary fringe and shallow groundwater.
9. The excavated areas will be backfilled to existing grade.
10. The overburden soils will be used as fill in other areas of the site. These soils will be
used above the water table, and with at least two feet of new fill above them.
11.Once the above is accomplished, development will proceed as a normal construction
project.
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04 Nova
7a! Group
Nova concludes that there is residual contamination in soils and groundwater that resulted
from former site use.
The site is slated for redevelopment as a fast food restaurant, if the site can be closed with a No
Further Action, and will accept a Notice of Residual Petroleum for groundwater use.
PHASE II LIMITED SITE ASSESSMENT 11 AL'S AUTO/HARRISBURG
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SB-6
O
O
S13-5 / GW-C
F SB-1 /
GW-A
■
61tss. ��
MW-2 / S13-2
S B-4
Former
N Dispenser MW-3
Island
W E
S _
(Not to Scale) T
Boring Location Plan (June 2019- September 2019)
4960 NC Hwy 49
Harrisburg, NC
NOVA PROJECT No. J19-5100
(DITMW
TM
*SB-2 (2 sam es)
MW-1 / SB
O T
SB-3 / GW-B
-1
diesel dispenser
location
LEGEND
= Property Boundary
0 = Soil Boring (June 2019)
Q= Former UST Location
2019
�Lt Nova
GroupFigure 2

LM-10E k QZ dL AJI-D
5 ? D ;1Fif-TE- -FAA-I�.
r
0000r/ --p -B I or
B-3 O
r'111 Xi-T
N
W E
S
(Not to Scale)
Historic Boring Location Plan
Previous Environmental Assessment (by others)
i-WDEZGE DLJ LD
IOE TAJV
2
�vL Nova 019
7 � Group Figure 3

N I
W E
S
ASrs
rn r
S13-7 / GW-D
O
Fo( met
Truck office
O
-5 / GW-C
i SB-1
O
G W-A
O O SB
MW-1
P83.80'
&'f5 83.80'
r,
S13-3 / GW-B
SB
�P-
84.201 -----
84.401 -------------------- 84 57'
MW-3
84.57' = groundwater
elevation in feet
Scale as shown 0
Potentiometric Elevations (September 2019)
4960 NC Hwy 49
Harrisburg, NC
NOVA PROJECT No. J19-5100
i
TMW-3I 83.42'
,3.60'
TMW[2 83.84'
-1 84.07'
LEGEND
= Property Boundary
' = diesel dispenser
= Soil Boring (June 2019)
= Former UST Location
Temporary Monitoring Well (August
2019)
2019
Nova
�� G rou p Figure 4

BE
op
N
W E
S
(Not to Scale)
Topographic Map
4960 NC Hwy 49
Harrisburg, NC
NOVA PROJECT No. J19-5100
tuo
L
_16
H a rrisbu rr ~ t49
3 OAS
� � f
�- 0 • - {
LEGEND
= Property Boundary
4&W* Nova 2019
*,%! Group
Figure 5

GW-D
BDL
GW-C
TMW-3
O
ff) B BDL
0
Bni
N 14.9
B 2.2
X 3.8
100
N 8.4 Q -B-1 / GW-A
4.2 \
TMW-2
500
� B BDL
B 208
N 36.3
245
X 3.8
Existing Building
1000
X 5, 10
(shown as Service
WMW-1
-2
TNT-1
Station in Figure 3)
2000
-B
O
BDL
2,380
B 23
N 213
N 7 6
X14,300
X .700
B = benzene
N = naphthatlene
N X = total xylenes
All concentrations in Ug/L.
W 4, E
S
Scale as shown 0
50'
Groundwater Data / Benzene Concentration in Ug/L
4960 NC Hwy 49
Harrisburg, NC
NOVA PROJECT No. J19-5100
MW-3
BDL
* Note: MW-1, 2,3 data from 9/19;
TMW-1,2,3 data from 8/19
GW-A, B,C data from 6/19.
2019
'AYIL. Nova
GroupFigure 6

Existing Building
(shown as Service
Station in Figure 3)
B = benzene
N = naphthatlene (as SVOC)
N X = total xylenes
All concentrations in Ug/L.
W E
S
Scale as shown 0
GW-D
* BDL
GW-C TMW-3
O B BDL
BDL N 10.5
B22 X3.8
N 8.4 ' B-1 / GW-A
6 X TMW-2
4.2
Approx location of B-2 circa
1992 — 770 mg/kg tph dro @
16' bls
50'
Groundwater Data / Naphthalene Concentration in Ug/L
4960 NC Hwy 49
Harrisburg, NC
NOVA PROJECT No. J19-5100
380
53.
X14,30
B 78 B BDL
O N 78 100 N 36.3
X5,710 X3.8
MW-1 i 0
T -1
• / BDL
0 23
0 N 234
X 26,700
MW-3
BDL
* Note: MW-1, 2,3 data from 9/19;
TMW-1,2,3 data from 8/19
GW-A, B,C data from 6/19.
2019
L Nova
47^r G ro u p
Figure 7

1500' LEI 1000'
11,
N
of
W E
FM s 011vir
D
cae-as
0 1 .nnn'
UK
500'
f�
TOM
Park
FO 1
5
Harrisburg Land Use Plan
Blue lines show water mains, smaller blue lines show water latterals.
Pink shading is Back Creek watershed LEGEND
Blue shading is Hambry Branch watershed =Property Boundary
City Water Line Plan
4960 NC Hwy 49
Harrisburg, NC
NOVA PROJECT No. J19-5100
2
Nova 019
�r` G ro u p Figure 8

1 1500' 1
■
v
RON
N
W 1W E
Scale - as shown
0
1,000'
LEGEND
S
= Property Boundary
= water well
Site Receptor Plan
2019
4960 NC Hwy 49
9.�
Nova
Harrisburg, NC
7 r�
G ro u p
NOVA PROJECT No. J19-5100
Figure 9

1 1500' 1
W40113rr-DR
0
10001,
-1 1
E]
Zoning Districts
dr Cr1
{` C:-
I-1
1-2
QI
PID
PUD
RE
Copied from:
RL
Official Zoning Map of the RM_i
Town of Harrisburg, North Carolina RM-z
N AaAmer4edTWnugft CVmbera.201a
W E
S
(Not to Scale)
Site Zoning Plan
4960 NC Hwy 49
Harrisburg, NC
NOVA PROJECT No. J19-5100
LEGEND
= Property Boundary
RV
RC
FDPO
Conditional Districts
a� Nova 2019
7�r G ro u p
Figure 10

106 Nova
*ONV Group
1. View of TMW-1 location to the east, with SB-3 in
3. View to the north along Property Line from right of way.
5. Location of TMW-2 (drill rig) with TMW-1 in the
foreground. View is to the north.
Former Phillips 66 / Harrisburg LSA
4960 Hwy 49, Harrisburg NC
2. View to the south along Property Line
4. Soil Boring profile for TMW-1.
6. View of probable soil staining in soil boring TMW-2
profile.
Date of Photographs June 5, August 5, September 16, and September 19, 2019
Limited Site Assessment
Nova Project No. J19-5100

Nova
Group
7. View to the northeast of TMW-3 location. TMW-2 is to
the right.
Former Phillips 66 / Harrisburg LSA
4960 Hwy 49, Harrisburg NC
8. View of stained soils at the capillary fringe (TMW-2).
9. View of MW-2 location 10. View of stained soils at MW-1 location
I
J
11. Setting pad for MW-2. 12. View of MW-2 from MW-1 location.
Date of Photographs June 5, August 5, September 16, and September 19, 2019 2
Limited Site Assessment Nova Project No. J19-5100

106 Nova
Group
13. Location of MW-3
15. View to the east with MW-2 to the right, and MW-1 in
the background.
Former Phillips 66 / Harrisburg LSA
4960 Hwy 49, Harrisburg NC
14. Survey transit setup to measure rim elevations.
16. View of adjacent property and SB-7 / GW-D down
gradient well.
Date of Photographs June 5, August 5, September 16, and September 19, 2019 3
Limited Site Assessment Nova Project No. J19-5100

TWA& Nova
LOG OF BORING SB-1/ MW-1
AWW Group
(Page 1 of 1)
Phillips 66 LSA
Date
September 16, 2019
Weather : Clear - 70 F
4690 Highway 49,
Drilling Company
: Regional Probing
Harrisburg, North Carolina
Hole Diameter
Drilling Method
Sampling Method
: 2.25-inches
: Geoprobe 6712DT
: Macro Core 5
PID : Mini Rae 3000
PID Lamp : 10.6 eV
Logged By : M. Minett
J19-5100
Limited Subsurface Investigation
u_
n
a-
E
U
U
S
Q
U
D
Q
0-
0
s a
1
2-
3-
4—
SM
0.2
5-
6-
7—
DESCRIPTION
SILTY SAND Fill, loose
8 3.4
SILTY SAND, red, tight
9—
9'
SM
10
11
12
8.0
13
SL
14
14'
15
16
17
SANDY SAPROLITE, brown -tan,
Weathered Rock with SAND, tan
18 Rock 1580
19 402
CLAY, green, moist, petroleum odor, visible staining
20 CL
21 LS-1
END OF BORING - REFUSAL
a�
a>
J
�5 REMARKS
>m
Groundwater
Encountered
Temp: MW-1

TWA& Nova
LOG OF BORING SB-2/ MW-2
lW1w Group
(Page 1 of 1)
Phillips 66 LSA
Date
September 16, 2019
Weather : Clear - 70 F
4690 Highway 49,
Drilling Company
: Regional Probing
Harrisburg, North Carolina
Hole Diameter
Drilling Method
Sampling Method
: 2.25-inches
: Geoprobe 6712DT
: Macro Core 5
PID : Mini Rae 3000
PID Lamp : 10.6 eV
Logged By : M. Minett
J19-5100
Limited Subsurface Investigation
Li Q
E
- M
U)
CL
0 J
1
2
3
4
5
6
7
8
9
10
11
12
13
14 14'
15
16
17
18
19
20
21
22
U �
S Q
0- U Q
< � o
(D > 0-
SM I 0
SM
DESCRIPTION
SILTY SAND Fill, red -to -tan
7
SILTY SAND, brown
0
CL 1 75
CLAY, green, wet, petroleum odor, visible staining
END OF BORING
a�
a>
J
a, REMARKS
>m
Groundwater
Encountered
Temp: MW-2

TWA& Nova
LOG OF BORING SB-3/ MW-3
lW1w Group
(Page 1 of 1)
Phillips 66 LSA
Date
September 16, 2019
Weather : Clear - 70 F
4690 Highway 49,
Drilling Company
: Regional Probing
Harrisburg, North Carolina
Hole Diameter
Drilling Method
Sampling Method
: 2.25-inches
: Geoprobe 6712DT
: Macro Core 5
PID : Mini Rae 3000
PID Lamp : 10.6 eV
Logged By : M. Minett
J19-5100
Limited Subsurface Investigation
u_
a-
E
U
E
>
C
Un
=
Q
�
Q
DESCRIPTION
�
REMARKS
CL
0
J
CO
D
o
0-
0
sa
Asphalt
ON
Concrete
1
SILTY SAND Fill, dark red
2
3
0
4
SM
5-
6-
7-
8—
SILTY SAND SAPROLITE, tan to red
9
10
11
SL
12
13
14'
0
14
CLAY, tan to red, wet
15
Groundwater
Encountered
16
17
CL
18
19
20
21
END OF BORING
Temp: MW-3

-JOill"I""i"i Nova
LOG OF BORING TMW-1
'OV^ Ci ro u p
(Page 1 of 1)
Phillips 66 LSA
Date
August 5, 2019
Weather
: Overcast — 75 F
4690 Highway 49,
Drilling Company
: Regional Probing
Harrisburg, North Carolina
Hole Diameter
Drilling Method
Sampling Method
: 2.25-inches
: Geoprobe 6712DT
: Macro Core 5
PID
PID Lamp
Logged By
: Mini Rae 3000
: 10.6 eV
: M. Minett
J19-5100
Limited Subsurface Investigation
u-
a
E
U
E
>>
x
Un
=
Q
�
Q
DESCRIPTION
�
REMARKS
CL
0
J
C0
o
0-
0-
Grass, topsoil
SILTY SAND Fill, brown
1
2
SM
3
4
5
SILTY SAND, red -to -brown
6
7
SM
8
9
10
SANDY SAPROLITE, brown -to -tan
11
12
GC
13
14
CLAY, dark green -to -black, moist
15
CL
16
Groundwater
Partial) Weathered Rock, tan -to -brown
Y
Encountered
17
Rock
18
SANDY SILT, brown
19
SP
20
ROCK
21
END OF BORING - REFUSAL
Temp: TMW-1

-JOill"I""i"i Nova
LOG OF BORING TMW-2
'OV^ Ci ro u p
(Page 1 of 1)
Phillips 66 LSA
Date
August 5, 2019
Weather
: Overcast — 75 F
4690 Highway 49,
Drilling Company
: Regional Probing
Harrisburg, North Carolina
Hole Diameter
Drilling Method
Sampling Method
: 2.25-inches
: Geoprobe 6712DT
: Macro Core 5
PID
PID Lamp
Logged By
: Mini Rae 3000
: 10.6 eV
: M. Minett
J19-5100
Limited Subsurface Investigation
u_
a-
E
U
n
Un
S
Q
U)
Q
DESCRIPTION
0
J
0
0-
0-
Grass, topsoil
SILTY SAND Fill with gravel, brown
1
j
I
2-
I
3-
4-
5—
j
SM
6
I
I
7
I
I
8
9
10
SILTY SAND, tan -to -brown
11
12
13
SM
14
15
16
SILTY SAND, grey, staining, hydrocarbon odor
17
18
19
20
SM
21
22
23
24
25
END OF BORING
a�
a>
J
�5 REMARKS
>m
Groundwater
Encountered
Temp: TMW-2

-JOill"I""i"i Nova
LOG OF BORING TMW-3
'OV^ Ci ro u p
(Page 1 of 1)
Phillips 66 LSA
Date
August 5, 2019
Weather
: Overcast — 75 F
4690 Highway 49,
Drilling Company
: Regional Probing
Harrisburg, North Carolina
Hole Diameter
Drilling Method
Sampling Method
: 2.25-inches
: Geoprobe 6712DT
: Macro Core 5
PID
PID Lamp
Logged By
: Mini Rae 3000
: 10.6 eV
: M. Minett
J19-5100
Limited Subsurface Investigation
u_
n
a-
E
07
U
S
Q
U
Q
d
0
...............
1
SM
2
3
4
5
6
7
8
SM
9
10
11
12
13
14
SP
15
16
17
DESCRIPTION
Grass, topsoil
SILTY SAND, brown
SILTY SAND FILL with gravel, brown
SANDY SILT, green, staining, hydrocarbon odor
ROCK, dry
END OF BORING- REFUSAL
a�
a>
J
�5 REMARKS
>m
Groundwater
Encountered
Temp: TMW-3

s
Sample ID Units Benzene Eth (benzene Isopropylbenzen4
p-Isopropyltoluene Meth I-tert-but I ether Naphthalene c-Bu Ibenze n-Pro
(benzene I Toluene I 1,2,4-Trimeth (benzene 1,3,5-Trimeth (benzene X lene Total
m& -X lene I o-X lene hloroanal 1-Meth Ina hthalene 2-Meth Ina hthalene Na hthalene
9/24/2019
MW-1
ug/L
208
1480
BDL
11.3
BDL
245
BDL
BDL
211
BDL
BDL
5710
3870
1840
BDL
9.9
18.4
78.1
N/a
9/24/2019
MW-2
ug/L
2380
3940
BDL
BDL
90.5
213
BDL
BDL
396
BDL
BDL
14300
12100
2230
BDL
4.1
8.0
63.0
N/a
9/29/2019
MW-3
ug/L
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
N/a
8/5/2019
TMW-1
ug/L
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
8/5/2019
TMW-2
ug/L
BDL
32.4
14
BDL
BDL
12.3
BDL
42.3
BDL
194
43.4
46
46
BDL
BDL
BDL
BDL
BDL
10
8/5/2019
TMW-3
ug/L
BDL
52.1
51.3
BDL
BDL
10.5
16.8
155
BDL
8.8
BDL
BDL
3.8
BDL
BDL
BDL
BDL
14.9
20.8
6/6/2019
GW-A
ug/L
2.2
24.7
BDL
BDL
1.8
8.4
BDL
BDL
BDL
BDL
BDL
4.2
4.2
BDL
BDL
BDL
BDL
BDL
N/a
6/6/2019
GW-B
ug/L
237
5350
BDL
BDL
BDL
756
BDL
BDL
615
BDL
BDL
26700
19100
7590
67.5
33.9
69
234
N/a
6/6/2019
GW-C
ug/L
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
N/a
6/6/2019
GW-D
ug/L
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
BDL
N/a
NCAC 2L
1
600
70
25
20
6
70
70
600
400
400
500
500
500
1
30
6
GCL
5000
84500
25000
11700
20000
6000
8500
30000
260000
28500
25000
85500
85500
85500
1000
12500
6000
625
14

lacieAnalXical"
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
August 12, 2019
Mike Minett
Nova Consulting Group, Inc.
442 South Main Street
Suite #7
Davidson, NC 28036
RE: Project: J 19-5100
Pace Project No.: 92439904
Dear Mike Minett:
Enclosed are the analytical results for sample(s) received by the laboratory on August 05, 2019. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: J19-5100
Pace Project No.: 92439904
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/NELAP Certification # LA170028
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
J19-5100
92439904
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92439904001
TMW-1
MADEP EPH
SEM
7
PASI-C
MADEP VPH
LMB
6
PASI-C
EPA 601 OD
IDS
1
PASI-A
EPA 625.1
PKS
63
PASI-C
SM 6200B
GAW
63
PASI-C
92439904002
TMW-2
MADEP EPH
SEM
7
PASI-C
MADEP VPH
LMB
6
PASI-C
EPA 601 OD
DS
1
PASI-A
EPA 625.1
PKS
68
PASI-C
SM 6200B
GAW
63
PASI-C
92439904003
TMW-3
MADEP EPH
SEM
7
PASI-C
MADEP VPH
LMB
6
PASI-C
EPA 601 OD
IDS
1
PASI-A
EPA 625.1
PKS
68
PASI-C
SM 6200B
GAW
63
PASI-C
92439904004
TB
SM 6200B
GAW
63
PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92439904
Sample: TMW-1 Lab ID: 92439904001 Collected: 08/05/19 13:10 Received: 08/05/19 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)
ND
ug/L
250
1
08/07/19 20:11
08/08/19 16:30
N2
Aliphatic (C19-C36)
ND
ug/L
250
1
08/07/19 20:11
08/08/19 16:30
N2
Aromatic (C11-C22)
ND
ug/L
250
1
08/07/19 20:11
08/08/19 16:30
N2
Surrogates
Nonatriacontane (S)
80
%
40-140
1
08/07/19 20:11
08/08/19 16:30
7194-86-7
o-Terphenyl (S)
91
%
40-140
1
08/07/19 20:11
08/08/19 16:30
84-15-1
2-Fluorobiphenyl (S)
97
%
40-140
1
08/07/19 20:11
08/08/19 16:30
321-60-8
2-Bromonaphthalene (S)
97
%
40-140
1
08/07/19 20:11
08/08/19 16:30
580-13-2
VPH NC Water
Analytical Method:
MADEP VPH
Aliphatic (C05-CO8)
ND
ug/L
50.0
1
08/06/19 13:52
N2
Aliphatic (C09-C12)
ND
ug/L
50.0
1
08/06/19 13:52
N2
Aliphatic(C09-C12) Adjusted
ND
ug/L
50.0
1
08/06/19 13:52
N2
Aromatic (C09-C10)
ND
ug/L
50.0
1
08/06/19 13:52
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
92
%
70-130
1
08/06/19 13:52
460-00-4
4-Bromofluorobenzene (PID) (S)
91
%
70-130
1
08/06/19 13:52
460-00-4
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Lead
ND
ug/L
5.0
1
08/11/19 10:01
08/12/19 00:12
7439-92-1
625 RVE
Analytical Method: EPA 625.1
Preparation Method:
EPA
625.1
Acenaphthene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
83-32-9
Acenaphthylene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
208-96-8
Anthracene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 18:51
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
7005-72-3
Chrysene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
25.0
1
08/08/19 18:04
08/09/19 18:51
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
120-83-2
Diethylphthalate
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 18:51
105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
84-74-2
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 08/12/2019 04:51 PM
without
the written consent of Pace Analytical Services,
LLC.
Page 4 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: J19-5100
Pace Project No.: 92439904
Sample: TMW-1
Parameters
ANALYTICAL RESULTS
Lab ID: 92439904001 Collected: 08/05/19 13:10 Received: 08/05/19 14:10 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 RVE Analytical Method: EPA 625.1 Preparation Method: EPA 625.1
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
1
08/08/19 18:04
08/09/19 18:51
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
08/08/19 18:04
08/09/19 18:51
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
117-81-7
Fluoranthene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
206-44-0
Fluorene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 18:51
77-47-4
Hexachloroethane
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
193-39-5
Isophorone
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 18:51
78-59-1
Naphthalene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
91-20-3
Nitrobenzene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
88-75-5
4-Nitrophenol
ND
ug/L
50.0
1
08/08/19 18:04
08/09/19 18:51
100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 18:51
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
108-60-1
Pentachlorophenol
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 18:51
87-86-5
Phenanthrene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
85-01-8
Phenol
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
108-95-2
Pyrene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 18:51
120-82-1
2,4,6-TrichIorophenol
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 18:51
88-06-2
Surrogates
Nitrobenzene-d5 (S)
31
%
10-120
1
08/08/19 18:04
08/09/19 18:51
4165-60-0
2-Fluorobiphenyl (S)
28
%
15-120
1
08/08/19 18:04
08/09/19 18:51
321-60-8
Terphenyl-d14 (S)
73
%
11-131
1
08/08/19 18:04
08/09/19 18:51
1718-51-0
Phenol-d6 (S)
18
%
10-120
1
08/08/19 18:04
08/09/19 18:51
13127-88-3
2-Fluorophenol (S)
24
%
10-120
1
08/08/19 18:04
08/09/19 18:51
367-12-4
2,4,6-Tribromophenol (S)
39
%
10-137
1
08/08/19 18:04
08/09/19 18:51
118-79-6
Tentatively Identified Compounds
Hexanoic acid, 2-ethyl-
11.2J
ug/L
1
08/08/19 18:04
08/09/19 18:51
149-57-5
Octanoic Acid
9.2J
ug/L
1
08/08/19 18:04
08/09/19 18:51
124-07-2
Nonanoic acid
6.3J
ug/L
1
08/08/19 18:04
08/09/19 18:51
112-05-0
Unknown
9.1J
ug/L
1
08/08/19 18:04
08/09/19 18:51
Phenol, 4-(1,1-dimethylp
13.6J
ug/L
1
08/08/19 18:04
08/09/19 18:51
80-46-6
6200B MSV
Analytical Method:
SM 6200B
Benzene
ND
ug/L
0.50
1
08/07/19 03:57
71-43-2
Bromobenzene
ND
ug/L
0.50
1
08/07/19 03:57
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
08/07/19 03:57
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
08/07/19 03:57
75-27-4
REPORT OF LABORATORY ANALYSIS
N
N
N
N
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 38

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92439904
Sample: TMW-1 Lab ID: 92439904001 Collected: 08/05/19 13:10 Received: 08/05/19 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method: SM 6200B
Bromoform
ND
ug/L
0.50
1
08/07/19 03:57
75-25-2
Bromomethane
ND
ug/L
5.0
1
08/07/19 03:57
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
08/07/19 03:57
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
08/07/19 03:57
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
08/07/19 03:57
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
08/07/19 03:57
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
08/07/19 03:57
108-90-7
Chloroethane
ND
ug/L
1.0
1
08/07/19 03:57
75-00-3
Chloroform
ND
ug/L
5.0
1
08/07/19 03:57
67-66-3
Chloromethane
ND
ug/L
1.0
1
08/07/19 03:57
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
08/07/19 03:57
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
08/07/19 03:57
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
08/07/19 03:57
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
08/07/19 03:57
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
08/07/19 03:57
106-93-4
Dibromomethane
ND
ug/L
0.50
1
08/07/19 03:57
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
08/07/19 03:57
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
08/07/19 03:57
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
08/07/19 03:57
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
08/07/19 03:57
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
08/07/19 03:57
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
08/07/19 03:57
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
08/07/19 03:57
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
08/07/19 03:57
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
08/07/19 03:57
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
08/07/19 03:57
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
08/07/19 03:57
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
08/07/19 03:57
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
08/07/19 03:57
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
08/07/19 03:57
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
08/07/19 03:57
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
08/07/19 03:57
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
08/07/19 03:57
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
08/07/19 03:57
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
08/07/19 03:57
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
08/07/19 03:57
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
08/07/19 03:57
1634-04-4
Naphthalene
ND
ug/L
2.0
1
08/07/19 03:57
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
08/07/19 03:57
103-65-1
Styrene
ND
ug/L
0.50
1
08/07/19 03:57
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
08/07/19 03:57
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
08/07/19 03:57
79-34-5
Tetrachloroethene
ND
ug/L
0.50
1
08/07/19 03:57
127-18-4
Toluene
ND
ug/L
0.50
1
08/07/19 03:57
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
08/07/19 03:57
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
08/07/19 03:57
120-82-1
1,1,1-Trichloroethane
ND
ug/L
0.50
1
08/07/19 03:57
71-55-6
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM
without
the written consent
of Pace Analytical Services, LLC.
Page 6 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92439904
Sample: TMW-1
Lab ID: 92439904001 Collected: 08/05/19 13:10
Received: 08/05/19 14:10 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
6200B MSV
Analytical Method:
SM 6200B
1,1,2-Trichloroethane
ND
ug/L
0.50
1
08/07/19 03:57
79-00-5
Trichloroethene
ND
ug/L
0.50
1
08/07/19 03:57
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
08/07/19 03:57
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
08/07/19 03:57
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
08/07/19 03:57
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
08/07/19 03:57
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
08/07/19 03:57
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
08/07/19 03:57
179601-23-1
o-Xylene
ND
ug/L
0.50
1
08/07/19 03:57
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
97
%
70-130
1
08/07/19 03:57
17060-07-0
4-Bromofluorobenzene (S)
95
%
70-130
1
08/07/19 03:57
460-00-4
Toluene-d8 (S)
101
%
70-130
1
08/07/19 03:57
2037-26-5
Date: 08/12/2019 04:51 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92439904
Sample: TMW-2 Lab ID: 92439904002 Collected: 08/05/19 12:50 Received: 08/05/19 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)
163
ug/L
98.0
1
08/07/19 20:11
08/08/19 16:58
N2
Aliphatic (C19-C36)
ND
ug/L
98.0
1
08/07/19 20:11
08/08/19 16:58
N2
Aromatic (C11-C22)
223
ug/L
98.0
1
08/07/19 20:11
08/08/19 16:58
N2
Surrogates
Nonatriacontane (S)
76
%
40-140
1
08/07/19 20:11
08/08/19 16:58
7194-86-7
o-Terphenyl (S)
86
%
40-140
1
08/07/19 20:11
08/08/19 16:58
84-15-1
2-Fluorobiphenyl (S)
90
%
40-140
1
08/07/19 20:11
08/08/19 16:58
321-60-8
2-Bromonaphthalene (S)
90
%
40-140
1
08/07/19 20:11
08/08/19 16:58
580-13-2
VPH NC Water
Analytical Method:
MADEP VPH
Aliphatic (C05-CO8)
147
ug/L
50.0
1
08/06/19 14:22
N2
Aliphatic (C09-C12)
1270
ug/L
50.0
1
08/06/19 14:22
N2
Aliphatic(C09-C12) Adjusted
502
ug/L
50.0
1
08/06/19 14:22
N2
Aromatic (C09-C10)
768
ug/L
50.0
1
08/06/19 14:22
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
87
%
70-130
1
08/06/19 14:22
460-00-4
4-Bromofluorobenzene (PID) (S)
89
%
70-130
1
08/06/19 14:22
460-00-4
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Lead
10.4
ug/L
5.0
1
08/11/19 10:01
08/12/19 00:15
7439-92-1
625 RVE
Analytical Method: EPA 625.1
Preparation Method:
EPA
625.1
Acenaphthene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
83-32-9
Acenaphthylene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
208-96-8
Anthracene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 19:16
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
7005-72-3
Chrysene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
25.0
1
08/08/19 18:04
08/09/19 19:16
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
120-83-2
Diethylphthalate
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 19:16
105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
84-74-2
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 08/12/2019 04:51 PM
without
the written consent of Pace Analytical Services,
LLC.
Page 8 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92439904
Sample: TMW-2
Lab ID: 92439904002 Collected: 08/05/19
12:50
Received: 08/05/19 14:10 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
625 RVE
Analytical Method:
EPA 625.1
Preparation Method: EPA 625.1
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
1
08/08/19 18:04
08/09/19 19:16
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
08/08/19 18:04
08/09/19 19:16
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
117-81-7
Fluoranthene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
206-44-0
Fluorene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 19:16
77-47-4
Hexachloroethane
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
193-39-5
Isophorone
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 19:16
78-59-1
Naphthalene
36.3
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
91-20-3
Nitrobenzene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
88-75-5
4-Nitrophenol
ND
ug/L
50.0
1
08/08/19 18:04
08/09/19 19:16
100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 19:16
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
108-60-1
Pentachlorophenol
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 19:16
87-86-5
Phenanthrene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
85-01-8
Phenol
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
108-95-2
Pyrene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:16
120-82-1
2,4,6-TrichIorophenol
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 19:16
88-06-2
Surrogates
Nitrobenzene-d5 (S)
63
%
10-120
1
08/08/19 18:04
08/09/19 19:16
4165-60-0
2-Fluorobiphenyl (S)
61
%
15-120
1
08/08/19 18:04
08/09/19 19:16
321-60-8
Terphenyl-d14 (S)
73
%
11-131
1
08/08/19 18:04
08/09/19 19:16
1718-51-0
Phenol-d6 (S)
30
%
10-120
1
08/08/19 18:04
08/09/19 19:16
13127-88-3
2-Fluorophenol (S)
46
%
10-120
1
08/08/19 18:04
08/09/19 19:16
367-12-4
2,4,6-Tribromophenol (S)
72
%
10-137
1
08/08/19 18:04
08/09/19 19:16
118-79-6
Tentatively Identified Compounds
Ethylbenzene
106J
ug/L
1
08/08/19 18:04
08/09/19 19:16
100-41-4
N
Benzene, (1-methylethyl)
50.1J
ug/L
1
08/08/19 18:04
08/09/19 19:16
98-82-8
N
Benzene, propyl-
154J
ug/L
1
08/08/19 18:04
08/09/19 19:16
103-65-1
N
Benzene, 1-ethyl-2-methy
106J
ug/L
1
08/08/19 18:04
08/09/19 19:16
611-14-3
N
Benzene, 1-ethyl-2-methy
233J
ug/L
1
08/08/19 18:04
08/09/19 19:16
611-14-3
N
1,2,4-Trimethylbenzene
215J
ug/L
1
08/08/19 18:04
08/09/19 19:16
95-36-3
N
Indane
89.91
ug/L
1
08/08/19 18:04
08/09/19 19:16
496-11-7
N
Benzene, 2-ethyl-1,4-dim
41.5J
ug/L
1
08/08/19 18:04
08/09/19 19:16
1758-88-9
N
Benzene, 1,2,4,5-tetrame
18.51
ug/L
1
08/08/19 18:04
08/09/19 19:16
95-93-2
N
1 H-Indene, 2,3-dihydro-5
23.6J
ug/L
1
08/08/19 18:04
08/09/19 19:16
874-35-1
N
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92439904
Sample: TMW-2 Lab ID: 92439904002 Collected: 08/05/19 12:50 Received: 08/05/19 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method: SM 6200B
Benzene
ND
ug/L
0.50
1
08/07/19 04:15
71-43-2
Bromobenzene
ND
ug/L
0.50
1
08/07/19 04:15
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
08/07/19 04:15
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
08/07/19 04:15
75-27-4
Bromoform
ND
ug/L
0.50
1
08/07/19 04:15
75-25-2
Bromomethane
ND
ug/L
5.0
1
08/07/19 04:15
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
08/07/19 04:15
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
08/07/19 04:15
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
08/07/19 04:15
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
08/07/19 04:15
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
08/07/19 04:15
108-90-7
Chloroethane
ND
ug/L
1.0
1
08/07/19 04:15
75-00-3
Chloroform
ND
ug/L
5.0
1
08/07/19 04:15
67-66-3
Chloromethane
ND
ug/L
1.0
1
08/07/19 04:15
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
08/07/19 04:15
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
08/07/19 04:15
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
08/07/19 04:15
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
08/07/19 04:15
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
08/07/19 04:15
106-93-4
Dibromomethane
ND
ug/L
0.50
1
08/07/19 04:15
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
08/07/19 04:15
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
08/07/19 04:15
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
08/07/19 04:15
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
08/07/19 04:15
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
08/07/19 04:15
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
08/07/19 04:15
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
08/07/19 04:15
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
08/07/19 04:15
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
08/07/19 04:15
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
08/07/19 04:15
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
08/07/19 04:15
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
08/07/19 04:15
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
08/07/19 04:15
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
08/07/19 04:15
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
08/07/19 04:15
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
08/07/19 04:15
108-20-3
Ethylbenzene
32.4
ug/L
0.50
1
08/07/19 04:15
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
08/07/19 04:15
87-68-3
Isopropylbenzene (Cumene)
14.0
ug/L
0.50
1
08/07/19 04:15
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
08/07/19 04:15
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
08/07/19 04:15
1634-04-4
Naphthalene
12.3
ug/L
2.0
1
08/07/19 04:15
91-20-3
n-Propylbenzene
42.3
ug/L
0.50
1
08/07/19 04:15
103-65-1
Styrene
ND
ug/L
0.50
1
08/07/19 04:15
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
08/07/19 04:15
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
08/07/19 04:15
79-34-5
Tetrachloroethene
ND
ug/L
0.50
1
08/07/19 04:15
127-18-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC.
Page 10 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92439904
Sample: TMW-2 Lab ID: 92439904002 Collected: 08/05/19 12:50 Received: 08/05/19 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 08/12/2019 04:51 PM
Analytical Method: SM 6200B
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
194
ug/L
43.4
ug/L
ND
ug/L
46.0
ug/L
ND
ug/L
97 %
95 %
103 %
0.50
1
08/07/19 04:15
108-88-3
2.0
1
08/07/19 04:15
87-61-6
2.0
1
08/07/19 04:15
120-82-1
0.50
1
08/07/19 04:15
71-55-6
0.50
1
08/07/19 04:15
79-00-5
0.50
1
08/07/19 04:15
79-01-6
1.0
1
08/07/19 04:15
75-69-4
0.50
1
08/07/19 04:15
96-18-4
0.50
1
08/07/19 04:15
95-63-6
0.50
1
08/07/19 04:15
108-67-8
1.0
1
08/07/19 04:15
75-01-4
1.0
1
08/07/19 04:15
179601-23-1
0.50
1
08/07/19 04:15
95-47-6
70-130
1
08/07/19 04:15
17060-07-0
70-130
1
08/07/19 04:15
460-00-4
70-130
1
08/07/19 04:15
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92439904
Sample: TMW-3 Lab ID: 92439904003 Collected: 08/05/19 13:30 Received: 08/05/19 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MADEP EPH NC Water Analytical Method: MADEP EPH Preparation Method: MADEP EPH
Aliphatic (C09-C18)
236
ug/L
99.0
1
08/07/19 20:11
08/08/19 17:26
N2
Aliphatic (C19-C36)
ND
ug/L
99.0
1
08/07/19 20:11
08/08/19 17:26
N2
Aromatic (C11-C22)
278
ug/L
99.0
1
08/07/19 20:11
08/08/19 17:26
N2
Surrogates
Nonatriacontane (S)
70
%
40-140
1
08/07/19 20:11
08/08/19 17:26
7194-86-7
o-Terphenyl (S)
99
%
40-140
1
08/07/19 20:11
08/08/19 17:26
84-15-1
2-Fluorobiphenyl (S)
105
%
40-140
1
08/07/19 20:11
08/08/19 17:26
321-60-8
2-Bromonaphthalene (S)
106
%
40-140
1
08/07/19 20:11
08/08/19 17:26
580-13-2
VPH NC Water
Analytical Method:
MADEP VPH
Aliphatic (C05-CO8)
6600
ug/L
50.0
1
08/06/19 14:51
N2
Aliphatic (C09-C12)
3390
ug/L
50.0
1
08/06/19 14:51
N2
Aliphatic(C09-C12) Adjusted
1920
ug/L
50.0
1
08/06/19 14:51
N2
Aromatic (C09-C10)
1480
ug/L
50.0
1
08/06/19 14:51
N2
Surrogates
4-Bromofluorobenzene (FID) (S)
167
%
70-130
1
08/06/19 14:51
460-00-4
S5
4-Bromofluorobenzene (PID) (S)
108
%
70-130
1
08/06/19 14:51
460-00-4
6010 MET ICP Analytical Method: EPA 6010D Preparation Method: EPA 3010A
Lead
20.8
ug/L
5.0
1
08/11/19 10:01
08/12/19 00:25
7439-92-1
625 RVE
Analytical Method: EPA 625.1
Preparation Method:
EPA
625.1
Acenaphthene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
83-32-9
Acenaphthylene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
208-96-8
Anthracene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
120-12-7
Benzo(a)anthracene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
56-55-3
Benzo(a)pyrene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
50-32-8
Benzo(b)fluoranthene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
191-24-2
Benzo(k)fluoranthene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
101-55-3
Butylbenzylphthalate
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
85-68-7
4-Chloro-3-methyl phenol
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 19:42
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
111-44-4
2-Chloronaphthalene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
91-58-7
2-Chlorophenol
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
7005-72-3
Chrysene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
53-70-3
3,3'-Dichlorobenzidine
ND
ug/L
25.0
1
08/08/19 18:04
08/09/19 19:42
91-94-1
2,4-Dichlorophenol
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
120-83-2
Diethylphthalate
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 19:42
105-67-9
Dimethylphthalate
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
131-11-3
Di-n-butylphthalate
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
84-74-2
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 08/12/2019 04:51 PM
without
the written consent of Pace Analytical Services,
LLC.
Page 12 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92439904
Sample: TMW-3
Lab ID: 92439904003 Collected: 08/05/19
13:30
Received: 08/05/19 14:10 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
625 RVE
Analytical Method:
EPA 625.1
Preparation Method: EPA 625.1
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
1
08/08/19 18:04
08/09/19 19:42
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
08/08/19 18:04
08/09/19 19:42
51-28-5
2,4-Dinitrotoluene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
121-14-2
2,6-Dinitrotoluene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
606-20-2
Di-n-octylphthalate
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
117-81-7
Fluoranthene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
206-44-0
Fluorene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
87-68-3
Hexachlorobenzene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 19:42
77-47-4
Hexachloroethane
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
193-39-5
Isophorone
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 19:42
78-59-1
Naphthalene
10.5
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
91-20-3
Nitrobenzene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
98-95-3
2-Nitrophenol
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
88-75-5
4-Nitrophenol
ND
ug/L
50.0
1
08/08/19 18:04
08/09/19 19:42
100-02-7
N-Nitrosodimethylamine
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 19:42
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
108-60-1
Pentachlorophenol
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 19:42
87-86-5
Phenanthrene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
85-01-8
Phenol
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
108-95-2
Pyrene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
5.0
1
08/08/19 18:04
08/09/19 19:42
120-82-1
2,4,6-TrichIorophenol
ND
ug/L
10.0
1
08/08/19 18:04
08/09/19 19:42
88-06-2
Surrogates
Nitrobenzene-d5 (S)
80
%
10-120
1
08/08/19 18:04
08/09/19 19:42
4165-60-0
2-Fluorobiphenyl (S)
76
%
15-120
1
08/08/19 18:04
08/09/19 19:42
321-60-8
Terphenyl-d14 (S)
106
%
11-131
1
08/08/19 18:04
08/09/19 19:42
1718-51-0
Phenol-d6 (S)
30
%
10-120
1
08/08/19 18:04
08/09/19 19:42
13127-88-3
2-Fluorophenol (S)
43
%
10-120
1
08/08/19 18:04
08/09/19 19:42
367-12-4
2,4,6-Tribromophenol (S)
99
%
10-137
1
08/08/19 18:04
08/09/19 19:42
118-79-6
Tentatively Identified Compounds
Pentane, 2,3,3-trimethyl
69.6J
ug/L
1
08/08/19 18:04
08/09/19 19:42
560-21-4
N
Heptane, 3-methyl-
62.7J
ug/L
1
08/08/19 18:04
08/09/19 19:42
589-81-1
N
Unknown
69.9J
ug/L
1
08/08/19 18:04
08/09/19 19:42
Octane, 3-methyl-
104J
ug/L
1
08/08/19 18:04
08/09/19 19:42
2216-33-3
N
Benzene, propyl-
97.2J
ug/L
1
08/08/19 18:04
08/09/19 19:42
103-65-1
N
Unknown
122J
ug/L
1
08/08/19 18:04
08/09/19 19:42
Indane
68.1J
ug/L
1
08/08/19 18:04
08/09/19 19:42
496-11-7
N
Benzene, 1,3-diethyl-
63.3J
ug/L
1
08/08/19 18:04
08/09/19 19:42
141-93-5
N
1 H-Indene, 2,3-dihydro-4
22.8J
ug/L
1
08/08/19 18:04
08/09/19 19:42
824-22-6
N
2,3-Dihydro-1-methylinde
40.9J
ug/L
1
08/08/19 18:04
08/09/19 19:42
27133-93-3
N
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92439904
Sample: TMW-3 Lab ID: 92439904003 Collected: 08/05/19 13:30 Received: 08/05/19 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method: SM 6200B
Benzene
ND
ug/L
0.50
1
08/07/19 04:33
71-43-2
Bromobenzene
ND
ug/L
0.50
1
08/07/19 04:33
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
08/07/19 04:33
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
08/07/19 04:33
75-27-4
Bromoform
ND
ug/L
0.50
1
08/07/19 04:33
75-25-2
Bromomethane
ND
ug/L
5.0
1
08/07/19 04:33
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
08/07/19 04:33
104-51-8
sec-Butylbenzene
16.8
ug/L
0.50
1
08/07/19 04:33
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
08/07/19 04:33
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
08/07/19 04:33
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
08/07/19 04:33
108-90-7
Chloroethane
ND
ug/L
1.0
1
08/07/19 04:33
75-00-3
Chloroform
ND
ug/L
5.0
1
08/07/19 04:33
67-66-3
Chloromethane
ND
ug/L
1.0
1
08/07/19 04:33
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
08/07/19 04:33
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
08/07/19 04:33
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
08/07/19 04:33
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
08/07/19 04:33
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
08/07/19 04:33
106-93-4
Dibromomethane
ND
ug/L
0.50
1
08/07/19 04:33
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
08/07/19 04:33
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
08/07/19 04:33
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
08/07/19 04:33
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
08/07/19 04:33
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
08/07/19 04:33
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
08/07/19 04:33
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
08/07/19 04:33
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
08/07/19 04:33
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
08/07/19 04:33
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
08/07/19 04:33
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
08/07/19 04:33
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
08/07/19 04:33
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
08/07/19 04:33
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
08/07/19 04:33
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
08/07/19 04:33
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
08/07/19 04:33
108-20-3
Ethylbenzene
52.1
ug/L
0.50
1
08/07/19 04:33
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
08/07/19 04:33
87-68-3
Isopropylbenzene (Cumene)
51.3
ug/L
0.50
1
08/07/19 04:33
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
08/07/19 04:33
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
08/07/19 04:33
1634-04-4
Naphthalene
14.9
ug/L
2.0
1
08/07/19 04:33
91-20-3
n-Propylbenzene
155
ug/L
0.50
1
08/07/19 04:33
103-65-1
Styrene
ND
ug/L
0.50
1
08/07/19 04:33
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
08/07/19 04:33
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
08/07/19 04:33
79-34-5
Tetrachloroethene
ND
ug/L
0.50
1
08/07/19 04:33
127-18-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92439904
Sample: TMW-3 Lab ID: 92439904003 Collected: 08/05/19 13:30 Received: 08/05/19 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 08/12/2019 04:51 PM
Analytical Method: SM 6200B
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
8.8
ug/L
ND
ug/L
ND
ug/L
3.8
ug/L
ND
ug/L
99 %
98 %
93 %
0.50
1
08/07/19 04:33
108-88-3
2.0
1
08/07/19 04:33
87-61-6
2.0
1
08/07/19 04:33
120-82-1
0.50
1
08/07/19 04:33
71-55-6
0.50
1
08/07/19 04:33
79-00-5
0.50
1
08/07/19 04:33
79-01-6
1.0
1
08/07/19 04:33
75-69-4
0.50
1
08/07/19 04:33
96-18-4
0.50
1
08/07/19 04:33
95-63-6
0.50
1
08/07/19 04:33
108-67-8
1.0
1
08/07/19 04:33
75-01-4
1.0
1
08/07/19 04:33
179601-23-1
0.50
1
08/07/19 04:33
95-47-6
70-130
1
08/07/19 04:33
17060-07-0
70-130
1
08/07/19 04:33
460-00-4
70-130
1
08/07/19 04:33
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 15 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92439904
Sample: TB Lab ID: 92439904004 Collected: 08/05/19 00:00 Received: 08/05/19 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method: SM 6200B
Benzene
ND
ug/L
0.50
1
08/07/19 15:31
71-43-2
Bromobenzene
ND
ug/L
0.50
1
08/07/19 15:31
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
08/07/19 15:31
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
08/07/19 15:31
75-27-4
Bromoform
ND
ug/L
0.50
1
08/07/19 15:31
75-25-2
Bromomethane
ND
ug/L
5.0
1
08/07/19 15:31
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
08/07/19 15:31
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
08/07/19 15:31
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
08/07/19 15:31
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
08/07/19 15:31
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
08/07/19 15:31
108-90-7
Chloroethane
ND
ug/L
1.0
1
08/07/19 15:31
75-00-3
Chloroform
ND
ug/L
5.0
1
08/07/19 15:31
67-66-3
Chloromethane
ND
ug/L
1.0
1
08/07/19 15:31
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
08/07/19 15:31
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
08/07/19 15:31
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
08/07/19 15:31
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
08/07/19 15:31
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
08/07/19 15:31
106-93-4
Dibromomethane
ND
ug/L
0.50
1
08/07/19 15:31
74-95-3
1,2-Dichlorobenzene
ND
ug/L
0.50
1
08/07/19 15:31
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
1
08/07/19 15:31
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
1
08/07/19 15:31
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
08/07/19 15:31
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
08/07/19 15:31
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
08/07/19 15:31
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
08/07/19 15:31
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
08/07/19 15:31
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
08/07/19 15:31
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
08/07/19 15:31
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
08/07/19 15:31
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
08/07/19 15:31
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
08/07/19 15:31
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
1
08/07/19 15:31
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
08/07/19 15:31
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
08/07/19 15:31
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
08/07/19 15:31
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
08/07/19 15:31
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
08/07/19 15:31
98-82-8
Methylene Chloride
16.4
ug/L
2.0
1
08/07/19 15:31
75-09-2 C9
Methyl-tert-butyl ether
ND
ug/L
0.50
1
08/07/19 15:31
1634-04-4
Naphthalene
ND
ug/L
2.0
1
08/07/19 15:31
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
08/07/19 15:31
103-65-1
Styrene
ND
ug/L
0.50
1
08/07/19 15:31
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
1
08/07/19 15:31
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
0.50
1
08/07/19 15:31
79-34-5
Tetrachloroethene
ND
ug/L
0.50
1
08/07/19 15:31
127-18-4
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM
without
the written consent
of Pace Analytical Services, LLC.
Page 16 of 38

aceAnalXical
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ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92439904
Sample: TB Lab ID: 92439904004 Collected: 08/05/19 00:00 Received: 08/05/19 14:10 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o-Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 08/12/2019 04:51 PM
Analytical Method: SM 6200B
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
93 %
95 %
100 %
0.50
1
08/07/19 15:31
108-88-3
2.0
1
08/07/19 15:31
87-61-6
2.0
1
08/07/19 15:31
120-82-1
0.50
1
08/07/19 15:31
71-55-6
0.50
1
08/07/19 15:31
79-00-5
0.50
1
08/07/19 15:31
79-01-6
1.0
1
08/07/19 15:31
75-69-4
0.50
1
08/07/19 15:31
96-18-4
0.50
1
08/07/19 15:31
95-63-6
0.50
1
08/07/19 15:31
108-67-8
1.0
1
08/07/19 15:31
75-01-4
1.0
1
08/07/19 15:31
179601-23-1
0.50
1
08/07/19 15:31
95-47-6
70-130
1
08/07/19 15:31
17060-07-0
70-130
1
08/07/19 15:31
460-00-4
70-130
1
08/07/19 15:31
2037-26-5
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 17 of 38

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9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92439904
QC Batch: 490578 Analysis Method: MADEP VPH
QC Batch Method: MADEP VPH Analysis Description: VPH NC Water
Associated Lab Samples: 92439904001, 92439904002, 92439904003
METHOD BLANK: 2646390
Matrix:
Water
Associated Lab Samples: 92439904001, 92439904002, 92439904003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aliphatic (C05-008)
ug/L
ND
50.0
08/06/19 13:22 N2
Aliphatic (C09-C12)
ug/L
ND
50.0
08/06/19 13:22 N2
Aromatic (C09-C10)
ug/L
ND
50.0
08/06/19 13:22 N2
4-Bromofluorobenzene (FID) (S)
%
91
70-130
08/06/19 13:22
4-Bromofluorobenzene (PID) (S)
%
92
70-130
08/06/19 13:22
LABORATORY CONTROL SAMPLE & LCSD:
2646391
2646392
Spike
LCS
LCSD
LCS
LCSD
% Rec Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits RPD RPD Qualifiers
Aliphatic (C05-CO8)
ug/L
300
294
295
98
98
70-130 0 25 N2
Aliphatic (C09-C12)
ug/L
300
304
314
101
105
30-130 3 25 N2
Aromatic (C09-C10)
ug/L
100
94.9
98.9
95
99
70-130 4 25 N2
4-Bromofluorobenzene (FID) (S)
%
98
102
70-130
4-Bromofluorobenzene (PID) (S)
%
97
102
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 38

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92439904
QC Batch: 491593
Analysis Method: EPA 6010D
QC Batch Method: EPA 3010A
Analysis Description: 6010 MET
Associated Lab Samples: 92439904001, 92439904002,
92439904003
METHOD BLANK: 2651232
Matrix: Water
Associated Lab Samples: 92439904001, 92439904002,
92439904003
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Lead ug/L
ND 5.0
08/11/19 23:18
LABORATORY CONTROL SAMPLE: 2651233
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Lead ug/L
500 490
98 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2651234 2651235
MS MSD
92440149001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Lead ug/L
500 500 515
514 103 103 75-125 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 38

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92439904
QC Batch: 490614 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Associated Lab Samples: 92439904001, 92439904002, 92439904003
METHOD BLANK: 2646532 Matrix:
Associated Lab Samples: 92439904001, 92439904002, 92439904003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
08/07/19 02:26
1,1,1-Trichloroethane
ug/L
ND
0.50
08/07/19 02:26
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
08/07/19 02:26
1,1,2-Trichloroethane
ug/L
ND
0.50
08/07/19 02:26
1,1-Dichloroethane
ug/L
ND
0.50
08/07/19 02:26
1,1-Dichloroethene
ug/L
ND
0.50
08/07/19 02:26
1,1-Dichloropropene
ug/L
ND
0.50
08/07/19 02:26
1,2,3-Trichlorobenzene
ug/L
ND
2.0
08/07/19 02:26
1,2,3-Trichloropropane
ug/L
ND
0.50
08/07/19 02:26
1,2,4-Trichlorobenzene
ug/L
ND
2.0
08/07/19 02:26
1,2,4-Trimethylbenzene
ug/L
ND
0.50
08/07/19 02:26
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
08/07/19 02:26
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
08/07/19 02:26
1,2-Dichlorobenzene
ug/L
ND
0.50
08/07/19 02:26
1,2-Dichloroethane
ug/L
ND
0.50
08/07/19 02:26
1,2-Dichloropropane
ug/L
ND
0.50
08/07/19 02:26
1,3,5-Trimethylbenzene
ug/L
ND
0.50
08/07/19 02:26
1,3-Dichlorobenzene
ug/L
ND
0.50
08/07/19 02:26
1,3-Dichloropropane
ug/L
ND
0.50
08/07/19 02:26
1,4-Dichlorobenzene
ug/L
ND
0.50
08/07/19 02:26
2,2-Dichloropropane
ug/L
ND
0.50
08/07/19 02:26
2-Chlorotoluene
ug/L
ND
0.50
08/07/19 02:26
4-Chlorotoluene
ug/L
ND
0.50
08/07/19 02:26
Benzene
ug/L
ND
0.50
08/07/19 02:26
Bromobenzene
ug/L
ND
0.50
08/07/19 02:26
Bromochloromethane
ug/L
ND
0.50
08/07/19 02:26
Bromodichloromethane
ug/L
ND
0.50
08/07/19 02:26
Bromoform
ug/L
ND
0.50
08/07/19 02:26
Bromomethane
ug/L
ND
5.0
08/07/19 02:26
Carbon tetrachloride
ug/L
ND
0.50
08/07/19 02:26
Chlorobenzene
ug/L
ND
0.50
08/07/19 02:26
Chloroethane
ug/L
ND
1.0
08/07/19 02:26
Chloroform
ug/L
ND
5.0
08/07/19 02:26
Chloromethane
ug/L
ND
1.0
08/07/19 02:26
cis-1,2-Dichloroethene
ug/L
ND
0.50
08/07/19 02:26
cis-1,3-Dichloropropene
ug/L
ND
0.50
08/07/19 02:26
Dibromochloromethane
ug/L
ND
0.50
08/07/19 02:26
Dibromomethane
ug/L
ND
0.50
08/07/19 02:26
Dichlorodifluoromethane
ug/L
ND
0.50
08/07/19 02:26
Diisopropyl ether
ug/L
ND
0.50
08/07/19 02:26
Ethylbenzene
ug/L
ND
0.50
08/07/19 02:26
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 38

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92439904
METHOD BLANK: 2646532 Matrix:
Associated Lab Samples: 92439904001, 92439904002, 92439904003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
2.0
08/07/19 02:26
Isopropylbenzene (Cumene)
ug/L
ND
0.50
08/07/19 02:26
m&p-Xylene
ug/L
ND
1.0
08/07/19 02:26
Methyl-tert-butyl ether
ug/L
ND
0.50
08/07/19 02:26
Methylene Chloride
ug/L
ND
2.0
08/07/19 02:26
n-Butylbenzene
ug/L
ND
0.50
08/07/19 02:26
n-Propylbenzene
ug/L
ND
0.50
08/07/19 02:26
Naphthalene
ug/L
ND
2.0
08/07/19 02:26
o-Xylene
ug/L
ND
0.50
08/07/19 02:26
sec-Butylbenzene
ug/L
ND
0.50
08/07/19 02:26
Styrene
ug/L
ND
0.50
08/07/19 02:26
tert-Butyl benzene
ug/L
ND
0.50
08/07/19 02:26
Tetrachloroethene
ug/L
ND
0.50
08/07/19 02:26
Toluene
ug/L
ND
0.50
08/07/19 02:26
trans-1,2-Dichloroethene
ug/L
ND
0.50
08/07/19 02:26
trans- 1,3-Dichloropropene
ug/L
ND
0.50
08/07/19 02:26
Trichloroethene
ug/L
ND
0.50
08/07/19 02:26
Trichlorofluoromethane
ug/L
ND
1.0
08/07/19 02:26
Vinyl chloride
ug/L
ND
1.0
08/07/19 02:26
1,2-Dichloroethane-d4 (S)
%
94
70-130
08/07/19 02:26
4-Bromofluorobenzene (S)
%
97
70-130
08/07/19 02:26
Toluene-d8 (S)
%
96
70-130
08/07/19 02:26
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2646533
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
49.0
98
60-140
1,1,1-Trichloroethane
ug/L
50
43.2
86
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
47.7
95
60-140
1,1,2-Trichloroethane
ug/L
50
48.4
97
60-140
1,1-Dichloroethane
ug/L
50
42.1
84
60-140
1,1-Dichloroethene
ug/L
50
43.1
86
60-140
1,1-Dichloropropene
ug/L
50
45.1
90
60-140
1,2,3-Trichlorobenzene
ug/L
50
60.2
120
60-140
1,2,3-Trichloropropane
ug/L
50
48.5
97
60-140
1,2,4-Trichlorobenzene
ug/L
50
53.1
106
60-140
1,2,4-Trimethylbenzene
ug/L
50
44.4
89
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
55.4
111
60-140
1,2-Dibromoethane (EDB)
ug/L
50
50.3
101
60-140
1,2-Dichlorobenzene
ug/L
50
47.0
94
60-140
1,2-Dichloroethane
ug/L
50
46.1
92
60-140
1,2-Dichloropropane
ug/L
50
45.1
90
60-140
1,3,5-Trimethylbenzene
ug/L
50
44.6
89
60-140
1,3-Dichlorobenzene
ug/L
50
46.3
93
60-140
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 38

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92439904
LABORATORY CONTROL SAMPLE:
Parameter
2646533
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichloropropane
ug/L
50
48.7
97
60-140
1,4-Dichlorobenzene
ug/L
50
45.7
91
60-140
2,2-Dichloropropane
ug/L
50
38.2
76
60-140
2-Chlorotoluene
ug/L
50
43.9
88
60-140
4-Chlorotoluene
ug/L
50
44.4
89
60-140
Benzene
ug/L
50
45.0
90
60-140
Bromobenzene
ug/L
50
45.9
92
60-140
Bromochloromethane
ug/L
50
44.6
89
60-140
Bromodichloromethane
ug/L
50
49.2
98
60-140
Bromoform
ug/L
50
53.6
107
60-140
Bromomethane
ug/L
50
42.0
84
60-140
Carbon tetrachloride
ug/L
50
44.8
90
60-140
Chlorobenzene
ug/L
50
45.2
90
60-140
Chloroethane
ug/L
50
41.7
83
60-140
Chloroform
ug/L
50
42.2
84
60-140
Chloromethane
ug/L
50
45.0
90
60-140
cis-1,2-Dichloroethene
ug/L
50
42.1
84
60-140
cis-1,3-Dichloropropene
ug/L
50
48.9
98
60-140
Dibromochloromethane
ug/L
50
50.7
101
60-140
Dibromomethane
ug/L
50
52.1
104
60-140
Dichlorodifluoromethane
ug/L
50
46.4
93
60-140
Diisopropyl ether
ug/L
50
43.3
87
60-140
Ethylbenzene
ug/L
50
45.7
91
60-140
Hexachloro-1,3-butadiene
ug/L
50
47.4
95
60-140
Isopropylbenzene (Cumene)
ug/L
50
46.1
92
60-140
m&p-Xylene
ug/L
100
92.0
92
60-140
Methyl-tert-butyl ether
ug/L
50
44.9
90
60-140
Methylene Chloride
ug/L
50
41.4
83
60-140
n-Butylbenzene
ug/L
50
43.3
87
60-140
n-Propylbenzene
ug/L
50
44.7
89
60-140
Naphthalene
ug/L
50
57.3
115
60-140
o-Xylene
ug/L
50
46.5
93
60-140
sec-Butylbenzene
ug/L
50
46.0
92
60-140
Styrene
ug/L
50
47.5
95
60-140
tert-Butyl benzene
ug/L
50
39.4
79
60-140
Tetrachloroethene
ug/L
50
45.7
91
60-140
Toluene
ug/L
50
44.7
89
60-140
trans-1,2-Dichloroethene
ug/L
50
42.8
86
60-140
trans- 1,3-Dichloropropene
ug/L
50
49.3
99
60-140
Trichloroethene
ug/L
50
45.1
90
60-140
Trichlorofluoromethane
ug/L
50
45.7
91
60-140
Vinyl chloride
ug/L
50
48.7
97
60-140
1,2-Dichloroethane-d4 (S)
%
92
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
98
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 38

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92439904
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2646534
2646535
MS
MSD
92439316001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
2000
2000
1980
1930
99
97
60-140
2
1,1,1-Trichloroethane
ug/L
ND
2000
2000
1980
1960
99
98
60-140
1
1,1,2,2-Tetrachloroethane
ug/L
ND
2000
2000
1900
1820
95
91
60-140
4
1,1,2-Trichloroethane
ug/L
ND
2000
2000
1920
1890
96
94
60-140
2
1,1-Dichloroethane
ug/L
ND
2000
2000
1920
1860
96
93
60-140
3
1,1-Dichloroethene
ug/L
ND
2000
2000
2090
2000
104
100
60-140
4
1,1-Dichloropropene
ug/L
ND
2000
2000
2060
2010
103
100
60-140
2
1,2,3-Trichlorobenzene
ug/L
ND
2000
2000
2280
2150
114
108
60-140
6
1,2,3-Trichloropropane
ug/L
ND
2000
2000
1900
1880
95
94
60-140
1
1,2,4-Trichlorobenzene
ug/L
ND
2000
2000
2070
1970
104
99
60-140
5
1,2,4-Trimethylbenzene
ug/L
ND
2000
2000
2010
ND
101
0
60-140
M1
1,2-Dibromo-3-chloropropane
ug/L
ND
2000
2000
2010
1990
100
99
60-140
1
1,2-Dibromoethane (EDB)
ug/L
ND
2000
2000
2030
1910
102
96
60-140
6
1,2-Dichlorobenzene
ug/L
ND
2000
2000
1890
1860
94
93
60-140
1
1,2-Dichloroethane
ug/L
ND
2000
2000
1980
1820
99
91
60-140
8
1,2-Dichloropropane
ug/L
ND
2000
2000
1870
1820
93
91
60-140
3
1,3,5-Trimethylbenzene
ug/L
ND
2000
2000
1920
1880
96
94
60-140
2
1,3-Dichlorobenzene
ug/L
ND
2000
2000
1890
1870
94
94
60-140
1
1,3-Dichloropropane
ug/L
ND
2000
2000
1970
1940
98
97
60-140
1
1,4-Dichlorobenzene
ug/L
ND
2000
2000
1870
1860
94
93
60-140
1
2,2-Dichloropropane
ug/L
ND
2000
2000
1550
1550
77
78
60-140
0
2-Chlorotoluene
ug/L
ND
2000
2000
1900
1880
95
94
60-140
1
4-Chlorotoluene
ug/L
ND
2000
2000
1900
1860
95
93
60-140
2
Benzene
ug/L
ND
2000
2000
1960
1920
98
96
60-140
2
Bromobenzene
ug/L
ND
2000
2000
1930
1920
97
96
60-140
0
Bromochloromethane
ug/L
ND
2000
2000
1900
1880
95
94
60-140
1
Bromodichloromethane
ug/L
ND
2000
2000
1970
2050
99
102
60-140
4
Bromoform
ug/L
ND
2000
2000
1930
1910
96
95
60-140
1
Bromomethane
ug/L
ND
2000
2000
1280
1280
46
46
60-140
0 M1
Carbon tetrachloride
ug/L
ND
2000
2000
1980
1940
99
97
60-140
2
Chlorobenzene
ug/L
ND
2000
2000
1940
1890
97
94
60-140
3
Chloroethane
ug/L
ND
2000
2000
2380
2180
119
109
60-140
9
Chloroform
ug/L
ND
2000
2000
1840
1870
92
93
60-140
2
Chloromethane
ug/L
ND
2000
2000
2150
2030
107
101
60-140
6
cis-1,2-Dichloroethene
ug/L
ND
2000
2000
1880
1820
94
91
60-140
3
cis-1,3-Dichloropropene
ug/L
ND
2000
2000
1950
1920
98
96
60-140
1
Dibromochloromethane
ug/L
ND
2000
2000
1920
1910
96
95
60-140
1
Dibromomethane
ug/L
ND
2000
2000
2180
2050
109
102
60-140
6
Dichlorodifluoromethane
ug/L
ND
2000
2000
2190
2210
110
110
60-140
1
Diisopropyl ether
ug/L
ND
2000
2000
1830
1800
92
90
60-140
2
Ethylbenzene
ug/L
ND
2000
2000
1970
1920
99
96
60-140
3
Hexachloro-1,3-butadiene
ug/L
ND
2000
2000
1900
1850
95
92
60-140
3
Isopropylbenzene (Cumene)
ug/L
ND
2000
2000
1980
1940
99
97
60-140
2
m&p-Xylene
ug/L
ND
4000
4000
3980
3840
100
96
60-140
4
Methyl-tert-butyl ether
ug/L
ND
2000
2000
1890
1850
94
92
60-140
2
Methylene Chloride
ug/L
ND
2000
2000
1860
1800
93
90
60-140
3
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92439904
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2646534
2646535
MS
MSD
92439316001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
ND
2000
2000
1800
1800
90
90
60-140
0
n-Propylbenzene
ug/L
ND
2000
2000
1950
1930
97
97
60-140
1
Naphthalene
ug/L
ND
2000
2000
2630
2210
131
111
60-140
17
o-Xylene
ug/L
ND
2000
2000
1990
1910
100
96
60-140
4
sec-Butylbenzene
ug/L
ND
2000
2000
2010
1980
100
99
60-140
1
Styrene
ug/L
ND
2000
2000
1940
1900
97
95
60-140
2
tert-Butyl benzene
ug/L
ND
2000
2000
1710
1670
86
84
60-140
2
Tetrachloroethene
ug/L
ND
2000
2000
2040
1950
102
98
60-140
4
Toluene
ug/L
8510
2000
2000
10100
9990
81
74
60-140
1
trans-1,2-Dichloroethene
ug/L
ND
2000
2000
1950
1930
98
96
60-140
1
trans- 1,3-Dichloropropene
ug/L
ND
2000
2000
1940
1870
97
94
60-140
4
Trichloroethene
ug/L
ND
2000
2000
1980
1960
99
98
60-140
1
Trichlorofluoromethane
ug/L
ND
2000
2000
2330
2230
116
111
60-140
4
Vinyl chloride
ug/L
ND
2000
2000
2310
2260
115
113
60-140
2
1,2-Dichloroethane-d4 (S)
%
94
97
70-130
4-Bromofluorobenzene (S)
%
100
97
70-130
Toluene-d8(S)
%
101
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92439904
QC Batch: 490874 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Associated Lab Samples: 92439904004
METHOD BLANK: 2647662
Associated Lab Samples: 92439904004
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
08/07/19 14:54
1,1,1-Trichloroethane
ug/L
ND
0.50
08/07/19 14:54
1,1,2,2-Tetrachloroethane
ug/L
ND
0.50
08/07/19 14:54
1,1,2-Trichloroethane
ug/L
ND
0.50
08/07/19 14:54
1,1-Dichloroethane
ug/L
ND
0.50
08/07/19 14:54
1,1-Dichloroethene
ug/L
ND
0.50
08/07/19 14:54
1,1-Dichloropropene
ug/L
ND
0.50
08/07/19 14:54
1,2,3-Trichlorobenzene
ug/L
ND
2.0
08/07/19 14:54
1,2,3-Trichloropropane
ug/L
ND
0.50
08/07/19 14:54
1,2,4-Trichlorobenzene
ug/L
ND
2.0
08/07/19 14:54
1,2,4-Trimethylbenzene
ug/L
ND
0.50
08/07/19 14:54
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
08/07/19 14:54
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
08/07/19 14:54
1,2-Dichlorobenzene
ug/L
ND
0.50
08/07/19 14:54
1,2-Dichloroethane
ug/L
ND
0.50
08/07/19 14:54
1,2-Dichloropropane
ug/L
ND
0.50
08/07/19 14:54
1,3,5-Trimethylbenzene
ug/L
ND
0.50
08/07/19 14:54
1,3-Dichlorobenzene
ug/L
ND
0.50
08/07/19 14:54
1,3-Dichloropropane
ug/L
ND
0.50
08/07/19 14:54
1,4-Dichlorobenzene
ug/L
ND
0.50
08/07/19 14:54
2,2-Dichloropropane
ug/L
ND
0.50
08/07/19 14:54
2-Chlorotoluene
ug/L
ND
0.50
08/07/19 14:54
4-Chlorotoluene
ug/L
ND
0.50
08/07/19 14:54
Benzene
ug/L
ND
0.50
08/07/19 14:54
Bromobenzene
ug/L
ND
0.50
08/07/19 14:54
Bromochloromethane
ug/L
ND
0.50
08/07/19 14:54
Bromodichloromethane
ug/L
ND
0.50
08/07/19 14:54
Bromoform
ug/L
ND
0.50
08/07/19 14:54
Bromomethane
ug/L
ND
5.0
08/07/19 14:54
Carbon tetrachloride
ug/L
ND
0.50
08/07/19 14:54
Chlorobenzene
ug/L
ND
0.50
08/07/19 14:54
Chloroethane
ug/L
ND
1.0
08/07/19 14:54
Chloroform
ug/L
ND
5.0
08/07/19 14:54
Chloromethane
ug/L
ND
1.0
08/07/19 14:54
cis-1,2-Dichloroethene
ug/L
ND
0.50
08/07/19 14:54
cis-1,3-Dichloropropene
ug/L
ND
0.50
08/07/19 14:54
Dibromochloromethane
ug/L
ND
0.50
08/07/19 14:54
Dibromomethane
ug/L
ND
0.50
08/07/19 14:54
Dichlorodifluoromethane
ug/L
ND
0.50
08/07/19 14:54
Diisopropyl ether
ug/L
ND
0.50
08/07/19 14:54
Ethylbenzene
ug/L
ND
0.50
08/07/19 14:54
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92439904
METHOD BLANK: 2647662
Associated Lab Samples: 92439904004
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
2.0
08/07/19 14:54
Isopropylbenzene (Cumene)
ug/L
ND
0.50
08/07/19 14:54
m&p-Xylene
ug/L
ND
1.0
08/07/19 14:54
Methyl-tert-butyl ether
ug/L
ND
0.50
08/07/19 14:54
Methylene Chloride
ug/L
ND
2.0
08/07/19 14:54
n-Butylbenzene
ug/L
ND
0.50
08/07/19 14:54
n-Propylbenzene
ug/L
ND
0.50
08/07/19 14:54
Naphthalene
ug/L
ND
2.0
08/07/19 14:54
o-Xylene
ug/L
ND
0.50
08/07/19 14:54
sec-Butylbenzene
ug/L
ND
0.50
08/07/19 14:54
Styrene
ug/L
ND
0.50
08/07/19 14:54
tert-Butyl benzene
ug/L
ND
0.50
08/07/19 14:54
Tetrachloroethene
ug/L
ND
0.50
08/07/19 14:54
Toluene
ug/L
ND
0.50
08/07/19 14:54
trans-1,2-Dichloroethene
ug/L
ND
0.50
08/07/19 14:54
trans- 1,3-Dichloropropene
ug/L
ND
0.50
08/07/19 14:54
Trichloroethene
ug/L
ND
0.50
08/07/19 14:54
Trichlorofluoromethane
ug/L
ND
1.0
08/07/19 14:54
Vinyl chloride
ug/L
ND
1.0
08/07/19 14:54
1,2-Dichloroethane-d4 (S)
%
94
70-130
08/07/19 14:54
4-Bromofluorobenzene (S)
%
95
70-130
08/07/19 14:54
Toluene-d8 (S)
%
100
70-130
08/07/19 14:54
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2647663
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
48.0
96
60-140
1,1,1-Trichloroethane
ug/L
50
46.4
93
60-140
1,1,2,2-Tetrachloroethane
ug/L
50
47.4
95
60-140
1,1,2-Trichloroethane
ug/L
50
47.6
95
60-140
1,1-Dichloroethane
ug/L
50
44.0
88
60-140
1,1-Dichloroethene
ug/L
50
45.7
91
60-140
1,1-Dichloropropene
ug/L
50
47.6
95
60-140
1,2,3-Trichlorobenzene
ug/L
50
60.0
120
60-140
1,2,3-Trichloropropane
ug/L
50
47.1
94
60-140
1,2,4-Trichlorobenzene
ug/L
50
53.9
108
60-140
1,2,4-Trimethylbenzene
ug/L
50
44.1
88
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
54.1
108
60-140
1,2-Dibromoethane (EDB)
ug/L
50
49.6
99
60-140
1,2-Dichlorobenzene
ug/L
50
46.2
92
60-140
1,2-Dichloroethane
ug/L
50
46.7
93
60-140
1,2-Dichloropropane
ug/L
50
43.9
88
60-140
1,3,5-Trimethylbenzene
ug/L
50
44.7
89
60-140
1,3-Dichlorobenzene
ug/L
50
45.8
92
60-140
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92439904
LABORATORY CONTROL SAMPLE:
Parameter
2647663
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichloropropane
ug/L
50
47.7
95
60-140
1,4-Dichlorobenzene
ug/L
50
45.1
90
60-140
2,2-Dichloropropane
ug/L
50
46.2
92
60-140
2-Chlorotoluene
ug/L
50
44.1
88
60-140
4-Chlorotoluene
ug/L
50
44.2
88
60-140
Benzene
ug/L
50
45.8
92
60-140
Bromobenzene
ug/L
50
45.6
91
60-140
Bromochloromethane
ug/L
50
46.8
94
60-140
Bromodichloromethane
ug/L
50
50.4
101
60-140
Bromoform
ug/L
50
51.6
103
60-140
Bromomethane
ug/L
50
39.8
80
60-140
Carbon tetrachloride
ug/L
50
46.4
93
60-140
Chlorobenzene
ug/L
50
45.3
91
60-140
Chloroethane
ug/L
50
45.5
91
60-140
Chloroform
ug/L
50
43.6
87
60-140
Chloromethane
ug/L
50
44.8
90
60-140
cis-1,2-Dichloroethene
ug/L
50
43.4
87
60-140
cis-1,3-Dichloropropene
ug/L
50
50.0
100
60-140
Dibromochloromethane
ug/L
50
48.4
97
60-140
Dibromomethane
ug/L
50
51.2
102
60-140
Dichlorodifluoromethane
ug/L
50
52.5
105
60-140
Diisopropyl ether
ug/L
50
44.5
89
60-140
Ethylbenzene
ug/L
50
46.1
92
60-140
Hexachloro-1,3-butadiene
ug/L
50
49.2
98
60-140
Isopropylbenzene (Cumene)
ug/L
50
47.0
94
60-140
m&p-Xylene
ug/L
100
92.8
93
60-140
Methyl-tert-butyl ether
ug/L
50
45.9
92
60-140
Methylene Chloride
ug/L
50
42.2
84
60-140
n-Butylbenzene
ug/L
50
44.5
89
60-140
n-Propylbenzene
ug/L
50
44.9
90
60-140
Naphthalene
ug/L
50
58.4
117
60-140
o-Xylene
ug/L
50
46.8
94
60-140
sec-Butylbenzene
ug/L
50
46.2
92
60-140
Styrene
ug/L
50
47.1
94
60-140
tert-Butyl benzene
ug/L
50
39.6
79
60-140
Tetrachloroethene
ug/L
50
47.4
95
60-140
Toluene
ug/L
50
46.0
92
60-140
trans-1,2-Dichloroethene
ug/L
50
44.4
89
60-140
trans- 1,3-Dichloropropene
ug/L
50
50.3
101
60-140
Trichloroethene
ug/L
50
46.7
93
60-140
Trichlorofluoromethane
ug/L
50
50.1
100
60-140
Vinyl chloride
ug/L
50
51.9
104
60-140
1,2-Dichloroethane-d4 (S)
%
93
70-130
4-Bromofluorobenzene (S)
%
100
70-130
Toluene-d8 (S)
%
98
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92439904
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2647664
2647665
MS
MSD
92439768001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
50
50
46.5
45.8
93
92
60-140
1
1,1,1-Trichloroethane
ug/L
ND
50
50
47.3
49.6
95
99
60-140
5
1,1,2,2-Tetrachloroethane
ug/L
ND
50
50
44.4
44.3
89
89
60-140
0
1,1,2-Trichloroethane
ug/L
ND
50
50
42.9
42.9
86
86
60-140
0
1,1-Dichloroethane
ug/L
ND
50
50
46.8
47.8
94
96
60-140
2
1,1-Dichloroethene
ug/L
ND
50
50
51.2
51.1
102
102
60-140
0
1,1-Dichloropropene
ug/L
ND
50
50
49.9
49.4
100
99
60-140
1
1,2,3-Trichlorobenzene
ug/L
ND
50
50
38.1
40.3
76
81
60-140
6
1,2,3-Trichloropropane
ug/L
ND
50
50
48.1
47.5
96
95
60-140
1
1,2,4-Trichlorobenzene
ug/L
ND
50
50
39.8
43.2
80
86
60-140
8
1,2,4-Trimethylbenzene
ug/L
400
50
50
392
403
-16
5
60-140
3 M1
1,2-Dibromo-3-chloropropane
ug/L
ND
50
50
48.1
50.8
96
102
60-140
5
1,2-Dibromoethane (EDB)
ug/L
ND
50
50
48.4
46.8
97
94
60-140
3
1,2-Dichlorobenzene
ug/L
ND
50
50
43.5
45.3
87
91
60-140
4
1,2-Dichloroethane
ug/L
ND
50
50
43.2
43.2
86
86
60-140
0
1,2-Dichloropropane
ug/L
ND
50
50
46.2
45.4
92
91
60-140
2
1,3,5-Trimethylbenzene
ug/L
82.8
50
50
118
122
70
78
60-140
3
1,3-Dichlorobenzene
ug/L
ND
50
50
45.2
45.8
90
92
60-140
1
1,3-Dichloropropane
ug/L
ND
50
50
47.0
44.9
94
90
60-140
5
1,4-Dichlorobenzene
ug/L
ND
50
50
44.2
45.5
88
91
60-140
3
2,2-Dichloropropane
ug/L
ND
50
50
40.6
41.4
81
83
60-140
2
2-Chlorotoluene
ug/L
ND
50
50
63.2
55.3
126
111
60-140
13
4-Chlorotoluene
ug/L
ND
50
50
45.1
44.3
90
89
60-140
2
Benzene
ug/L
111
50
50
156
155
90
89
60-140
0
Bromobenzene
ug/L
ND
50
50
46.7
47.0
93
94
60-140
1
Bromochloromethane
ug/L
ND
50
50
43.8
45.8
88
92
60-140
4
Bromodichloromethane
ug/L
ND
50
50
47.6
46.8
95
94
60-140
2
Bromoform
ug/L
ND
50
50
45.7
45.6
91
91
60-140
0
Bromomethane
ug/L
ND
50
50
33.2
36.3
66
73
60-140
9
Carbon tetrachloride
ug/L
ND
50
50
48.6
48.1
97
96
60-140
1
Chlorobenzene
ug/L
ND
50
50
46.5
47.0
93
94
60-140
1
Chloroethane
ug/L
ND
50
50
72.2
65.8
144
132
60-140
9 M1
Chloroform
ug/L
ND
50
50
46.0
45.6
92
91
60-140
1
Chloromethane
ug/L
ND
50
50
54.6
53.8
109
108
60-140
1
cis-1,2-Dichloroethene
ug/L
ND
50
50
44.9
45.8
90
92
60-140
2
cis-1,3-Dichloropropene
ug/L
ND
50
50
46.6
46.3
93
93
60-140
1
Dibromochloromethane
ug/L
ND
50
50
44.4
45.2
89
90
60-140
2
Dibromomethane
ug/L
ND
50
50
48.9
50.7
98
101
60-140
4
Dichlorodifluoromethane
ug/L
ND
50
50
57.0
57.8
114
116
60-140
1
Diisopropyl ether
ug/L
ND
50
50
48.4
49.1
97
98
60-140
1
Ethylbenzene
ug/L
58.9
50
50
102
103
86
88
60-140
1
Hexachloro-1,3-butadiene
ug/L
ND
50
50
39.8
41.0
80
82
60-140
3
Isopropylbenzene(Cumene)
ug/L
12.5
50
50
57.5
58.0
90
91
60-140
1
m&p-Xylene
ug/L
175
100
100
255
255
80
80
60-140
0
Methyl-tert-butyl ether
ug/L
219
50
50
260
259
82
81
60-140
0
Methylene Chloride
ug/L
ND
50
50
44.5
45.4
89
91
60-140
2
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92439904
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2647664
2647665
MS
MSD
92439768001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
n-Butylbenzene
ug/L
ND
50
50
64.9
68.9
130
138
60-140
6
n-Propylbenzene
ug/L
35.3
50
50
75.1
77.3
80
84
60-140
3
Naphthalene
ug/L
117
50
50
127
142
19
51
60-140
12 M1
o-Xylene
ug/L
40.7
50
50
84.0
85.3
86
89
60-140
2
sec-Butylbenzene
ug/L
ND
50
50
50.1
51.2
100
102
60-140
2
Styrene
ug/L
ND
50
50
45.9
47.2
92
94
60-140
3
tert-Butyl benzene
ug/L
ND
50
50
40.1
41.3
80
83
60-140
3
Tetrachloroethene
ug/L
ND
50
50
50.9
50.3
102
101
60-140
1
Toluene
ug/L
14.3
50
50
59.9
59.8
91
91
60-140
0
trans-1,2-Dichloroethene
ug/L
ND
50
50
47.8
48.5
96
97
60-140
1
trans- 1,3-Dichloropropene
ug/L
ND
50
50
43.1
44.5
86
89
60-140
3
Trichloroethene
ug/L
ND
50
50
50.2
48.2
100
96
60-140
4
Trichlorofluoromethane
ug/L
ND
50
50
57.1
57.2
114
114
60-140
0
Vinyl chloride
ug/L
ND
50
50
59.2
59.4
118
119
60-140
0
1,2-Dichloroethane-d4 (S)
%
87
89
70-130
4-Bromofluorobenzene (S)
%
97
96
70-130
Toluene-d8(S)
%
99
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC.
Page 29 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92439904
QC Batch: 491345 Analysis Method: EPA 625.1
QC Batch Method: EPA 625.1 Analysis Description: 625 MSS
Associated Lab Samples: 92439904001, 92439904002, 92439904003
METHOD BLANK: 2650028 Matrix:
Associated Lab Samples: 92439904001, 92439904002, 92439904003
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
5.0
08/09/19 13:36
2,2'-Oxybis(1-chloropropane)
ug/L
ND
5.0
08/09/19 13:36
2,4,6-Trichlorophenol
ug/L
ND
10.0
08/09/19 13:36
2,4-Dichlorophenol
ug/L
ND
5.0
08/09/19 13:36
2,4-Dimethylphenol
ug/L
ND
10.0
08/09/19 13:36
2,4-Dinitrophenol
ug/L
ND
50.0
08/09/19 13:36
2,4-Dinitrotoluene
ug/L
ND
5.0
08/09/19 13:36
2,6-Dinitrotoluene
ug/L
ND
5.0
08/09/19 13:36
2-Chloronaphthalene
ug/L
ND
5.0
08/09/19 13:36
2-Chlorophenol
ug/L
ND
5.0
08/09/19 13:36
2-Nitrophenol
ug/L
ND
5.0
08/09/19 13:36
3,3'-Dichlorobenzidine
ug/L
ND
25.0
08/09/19 13:36
4,6-Dinitro-2-methyl phenol
ug/L
ND
20.0
08/09/19 13:36
4-Bromophenylphenyl ether
ug/L
ND
5.0
08/09/19 13:36
4-Chloro-3-methylphenol
ug/L
ND
5.0
08/09/19 13:36
4-Chlorophenylphenyl ether
ug/L
ND
5.0
08/09/19 13:36
4-Nitrophenol
ug/L
ND
50.0
08/09/19 13:36
Acenaphthene
ug/L
ND
5.0
08/09/19 13:36
Acenaphthylene
ug/L
ND
5.0
08/09/19 13:36
Anthracene
ug/L
ND
5.0
08/09/19 13:36
Benzo(a)anthracene
ug/L
ND
5.0
08/09/19 13:36
Benzo(a)pyrene
ug/L
ND
5.0
08/09/19 13:36
Benzo(b)fluoranthene
ug/L
ND
5.0
08/09/19 13:36
Benzo(g,h,i)perylene
ug/L
ND
5.0
08/09/19 13:36
Benzo(k)fluoranthene
ug/L
ND
5.0
08/09/19 13:36
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
08/09/19 13:36
bis(2-Chloroethyl) ether
ug/L
ND
5.0
08/09/19 13:36
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
08/09/19 13:36
Butylbenzylphthalate
ug/L
ND
5.0
08/09/19 13:36
Chrysene
ug/L
ND
5.0
08/09/19 13:36
Di-n-butylphthalate
ug/L
ND
5.0
08/09/19 13:36
Di-n-octylphthalate
ug/L
ND
5.0
08/09/19 13:36
Dibenz(a,h)anthracene
ug/L
ND
5.0
08/09/19 13:36
Diethylphthalate
ug/L
ND
5.0
08/09/19 13:36
Dimethylphthalate
ug/L
ND
5.0
08/09/19 13:36
Fluoranthene
ug/L
ND
5.0
08/09/19 13:36
Fluorene
ug/L
ND
5.0
08/09/19 13:36
Hexachloro-1,3-butadiene
ug/L
ND
5.0
08/09/19 13:36
Hexachlorobenzene
ug/L
ND
5.0
08/09/19 13:36
Hexachlorocyclopentadiene
ug/L
ND
10.0
08/09/19 13:36
Hexachloroethane
ug/L
ND
5.0
08/09/19 13:36
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92439904
METHOD BLANK: 2650028
Matrix:
Water
Associated Lab Samples: 92439904001, 92439904002, 92439904003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
08/09/19 13:36
Isophorone
ug/L
ND
10.0
08/09/19 13:36
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
08/09/19 13:36
N-Nitrosodimethylamine
ug/L
ND
5.0
08/09/19 13:36
N-Nitrosodiphenylamine
ug/L
ND
10.0
08/09/19 13:36
Naphthalene
ug/L
ND
5.0
08/09/19 13:36
Nitrobenzene
ug/L
ND
5.0
08/09/19 13:36
Pentachlorophenol
ug/L
ND
10.0
08/09/19 13:36
Phenanthrene
ug/L
ND
5.0
08/09/19 13:36
Phenol
ug/L
ND
5.0
08/09/19 13:36
Pyrene
ug/L
ND
5.0
08/09/19 13:36
2,4,6-Tribromophenol (S)
%
79
10-137
08/09/19 13:36
2-Fluorobiphenyl (S)
%
68
15-120
08/09/19 13:36
2-Fluorophenol (S)
%
62
10-120
08/09/19 13:36
Nitrobenzene-d5 (S)
%
73
10-120
08/09/19 13:36
Phenol-d6 (S)
%
44
10-120
08/09/19 13:36
Terphenyl-d14 (S)
%
100
11-131
08/09/19 13:36
LABORATORY CONTROL SAMPLE & LCSD:
2650029
2650030
Spike
LCS
LCSD
LCS LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec % Rec
Limits RPD
RPD Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
36.3
37.4
73 75
44-142
3 30
2,2'-Oxybis(1-chloropropane)
ug/L
50
41.0
42.5
82 85
36-166
3 30
2,4,6-Trichlorophenol
ug/L
50
38.7
41.1
77 82
37-144
6 30
2,4-Dichlorophenol
ug/L
50
38.4
41.1
77 82
1-191
7 30
2,4-Dimethylphenol
ug/L
50
37.4
39.0
75 78
32-119
4 30
2,4-Dinitrophenol
ug/L
250
223
227
89 91
1-181
2 30
2,4-Dinitrotoluene
ug/L
50
42.0
41.9
84 84
39-139
0 30
2,6-Dinitrotoluene
ug/L
50
40.7
42.4
81 85
50-158
4 30
2-Chloronaphthalene
ug/L
50
34.3
35.4
69 71
60-118
3 30
2-Chlorophenol
ug/L
50
37.5
39.9
75 80
23-134
6 30
2-Nitrophenol
ug/L
50
39.1
41.8
78 84
29-182
7 30
3,3'-Dichlorobenzidine
ug/L
100
87.9
92.6
88 93
1-262
5 30
4,6-Dinitro-2-methyl phenol
ug/L
100
97.8
103
98 103
1-181
6 30
4-Bromophenylphenyl ether
ug/L
50
44.1
47.1
88 94
53-127
7 30
4-ChIoro-3-methyl phenol
ug/L
100
81.8
85.4
82 85
22-147
4 30
4-Chlorophenylphenyl ether
ug/L
50
41.3
42.7
83 85
25-158
3 30
4-Nitrophenol
ug/L
250
162
161
65 64
1-132
1 30
Acenaphthene
ug/L
50
39.6
41.0
79 82
47-145
4 30
Acenaphthylene
ug/L
50
40.3
42.2
81 84
33-145
5 30
Anthracene
ug/L
50
47.1
49.4
94 99
1-166
5 30
Benzo(a)anthracene
ug/L
50
49.3
53.3
99 107
33-143
8 30
Benzo(a)pyrene
ug/L
50
49.2
52.3
98 105
17-163
6 30
Benzo(b)fluoranthene
ug/L
50
48.6
52.3
97 105
24-159
7 30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92439904
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
2650029
Units
Spike
Conc.
2650030
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec
Limits
RPD
Max
RPD Qualifiers
Benzo(g,h,i)perylene
ug/L
50
48.7
51.0
97
102
1-219
5
30
Benzo(k)fluoranthene
ug/L
50
48.9
52.9
98
106
11-162
8
30
bis(2-Chloroethoxy)methane
ug/L
50
39.6
42.0
79
84
33-184
6
30
bis(2-Chloroethyl) ether
ug/L
50
39.1
42.6
78
85
12-158
8
30
bis(2-Ethylhexyl)phthalate
ug/L
50
51.4
54.6
103
109
8-158
6
30
Butylbenzylphthalate
ug/L
50
49.2
53.9
98
108
1-152
9
30
Chrysene
ug/L
50
50.1
54.2
100
108
17-168
8
30
Di-n-butylphthalate
ug/L
50
51.1
51.2
102
102
1-118
0
30
Di-n-octylphthalate
ug/L
50
52.4
55.2
105
110
4-146
5
30
Dibenz(a,h)anthracene
ug/L
50
49.4
51.5
99
103
1-227
4
30
Diethylphthalate
ug/L
50
43.1
44.5
86
89
1-114
3
30
Dimethylphthalate
ug/L
50
42.6
43.8
85
88
1-112
3
30
Fluoranthene
ug/L
50
50.3
51.7
101
103
26-137
3
30
Fluorene
ug/L
50
42.1
43.0
84
86
59-121
2
30
Hexachloro-1,3-butadiene
ug/L
50
36.5
36.7
73
73
24-116
1
30
Hexachlorobenzene
ug/L
50
39.3
41.2
79
82
1-152
5
30
Hexachlorocyclopentadiene
ug/L
50
34.8
35.6
70
71
25-150
2
30
Hexachloroethane
ug/L
50
36.0
35.4
72
71
40-113
2
30
Indeno(1,2,3-cd)pyrene
ug/L
50
49.2
51.7
98
103
1-171
5
30
Isophorone
ug/L
50
36.2
38.6
72
77
21-196
6
30
N-Nitroso-di-n-propylamine
ug/L
50
40.3
43.5
81
87
1-230
8
30
N-Nitrosodimethylamine
ug/L
50
35.5
38.4
71
77
25-150
8
30
N-Nitrosodiphenylamine
ug/L
50
45.7
47.1
91
94
25-150
3
30
Naphthalene
ug/L
50
42.0
43.5
84
87
21-133
4
30
Nitrobenzene
ug/L
50
36.2
38.4
72
77
35-180
6
30
Pentachlorophenol
ug/L
100
99.5
101
100
101
14-176
1
30
Phenanthrene
ug/L
50
46.3
48.1
93
96
54-120
4
30
Phenol
ug/L
50
26.3
27.6
53
55
5-112
5
30
Pyrene
ug/L
50
48.3
52.9
97
106
52-115
9
30
2,4,6-Tribromophenol (S)
%
102
93
10-137
2-Fluorobiphenyl (S)
%
79
73
15-120
2-Fluorophenol(S)
%
69
65
10-120
Nitrobenzene-d5(S)
%
80
77
10-120
Phenol-d6 (S)
%
54
50
10-120
Terphenyl-d14(S)
%
97
95
11-131
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC.
Page 32 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92439904
QC Batch: 491000 Analysis Method: MADEP EPH
QC Batch Method: MADEP EPH Analysis Description: MADEP EPH NC Water
Associated Lab Samples: 92439904001, 92439904002, 92439904003
METHOD BLANK: 2648299
Matrix:
Water
Associated Lab Samples:
92439904001, 92439904002, 92439904003
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aliphatic (C09-C18)
ug/L
ND
100
08/08/19 15:07 N2
Aliphatic (C19-C36)
ug/L
ND
100
08/08/19 15:07 N2
Aromatic (C11-C22)
ug/L
ND
100
08/08/19 15:07 N2
2-Bromonaphthalene (S)
%
105
40-140
08/08/19 15:07
2-Fluorobiphenyl (S)
%
106
40-140
08/08/19 15:07
Nonatriacontane (S)
%
58
40-140
08/08/19 15:07
o-Terphenyl (S)
%
87
40-140
08/08/19 15:07
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
2648300
Units
Spike
Conc.
2648301
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec Max
Limits RPD RPD Qualifiers
Aliphatic (C09-C18)
ug/L
300
196
217
65
72
40-140 10 50 N2
Aliphatic (C19-C36)
ug/L
400
262
290
66
73
40-140 10 50 N2
Aromatic (C11-C22)
ug/L
850
773
764
91
90
40-140 1 50 N2
2-Bromonaphthalene (S)
%
98
90
40-140
2-Fluorobiphenyl (S)
%
100
100
40-140
Nonatriacontane (S)
%
69
71
40-140
o-Terphenyl(S)
%
99
95
40-140
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC.
Page 33 of 38

Pace Analytical Services, LLC
aceAnalXical� 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: J19-5100
Pace Project No.: 92439904
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
C9 Common Laboratory Contaminant.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N The reported TIC has an 85% or higher match on a mass spectral library search.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
S5 Surrogate recovery outside control limits due to matrix interferences (not confirmed by re -analysis).
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 38

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
J19-5100
Pace Project No.:
92439904
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92439904001
TMW-1
MADEP EPH
491000
MADEP EPH
491163
92439904002
TMW-2
MADEP EPH
491000
MADEP EPH
491163
92439904003
TMW-3
MADEP EPH
491000
MADEP EPH
491163
92439904001
TMW-1
MADEP VPH
490578
92439904002
TMW-2
MADEP VPH
490578
92439904003
TMW-3
MADEP VPH
490578
92439904001
TMW-1
EPA 3010A
491593
EPA 6010D
491649
92439904002
TMW-2
EPA 3010A
491593
EPA 6010D
491649
92439904003
TMW-3
EPA 3010A
491593
EPA 6010D
491649
92439904001
TMW-1
EPA 625.1
491345
EPA 625.1
491445
92439904002
TMW-2
EPA 625.1
491345
EPA 625.1
491445
92439904003
TMW-3
EPA 625.1
491345
EPA 625.1
491445
92439904001
TMW-1
SM 6200E
490614
92439904002
TMW-2
SM 6200E
490614
92439904003
TMW-3
SM 6200E
490614
92439904004
TB
SM 6200B
490874
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/12/2019 04:51 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 38

Document Name: Document Revised: February 7, 2018
Condition Upon Receipt(SCUR) Page 1 of 2
Document No.: Issuing Authority:
F-CAR43-033-Rev.06 Pace Carolinas Qualitv Office
Asheville ❑ Eden❑ Greenwood ❑ Fluntersville ❑ Raleigh[] Mechanicsville[]
ConditionSample Client Name: W0# : 92439904
Upon Receipt ,Project fs: II I �I� II III1I 1 I l l� l III
Courier: ❑Fed Ex [-]UPS [—]LISPS } ❑Client
❑ Commercial QPace. ❑other: 92439904
ril,.
Custody Seal Present? []Yes []NO Seals Intact? ❑Yes ❑No
Date/Initials Person Examining Contents:
Packing MatiMal: []Bubble Wrap []Bubble Bags ❑None ❑ Other
Therrrtameter:
❑ra Gunl rp: 92TO48 . Type of Ice: ❑wet ❑slue
Coaler Temp Correction Factor: Add/Subtract ('C) 0.0
Cooler Temp Corrected ('C): '
USDA Regulated Soil (❑ N/A, water sample)
Did sarriples.originate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
DYes ❑No
Biological Tissue Frozen?
[]Yes[]No[]N/A❑None
Tempshould be above freezing to 6'C
❑Samples out of temp criteria. Samples an ice, cooling process
hasbegurs
Did samples originate from a foreign source (internationally,
n 1—r-14-1i —d Pn rm A1rn17 MY— 1-lnln
Corhments/Discrepancy: _
Cfialn of Custody Present?
❑Yes
❑No
❑NIA
1.
Samples Arrived within FlDld Time?
❑Yes
[]No
❑N/A
2.
Short Hold. Time Analysis 102 hr.)?
❑Yes
❑Na
❑NJA
3.
Rush Turn Around Time Requested?
❑Yes
[]NO
❑N/A
4.
Sufficient Volume?
❑Yes
[]No
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
Des
❑Yes
[]No
[]No
❑N/A
❑N/A
6.
Containers Intact?
❑Yes
[:]No
❑NJA
7.
DISSOIved analysis: Samples Field Filtered?
❑Yes
❑Na
[]NIA
8.
Sample labels Match CDC?
-Includes Date/Time/ID/Analysis Matrix: I '
❑Yes
❑No
❑N/A
9.
Headspace in VOA Vials (>5-6rmm)?
❑Yes
[]No
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
.❑Yes
--.[]Yes
[]No
[-]No
[-I NIA
[I N/A
11.
COMMENTS/SAMPLE DOCREPANCY Field Data Required? ❑Yes [—]No
Lot ID ofmlitcontainers:
CLIENT NOT IFICAVC)N/RESOLUTION
Person contacted:
Project Manager SCURF Review: d_6
Project Manager SRF Review:
Date/Tlme:
Date:
ghl /a
Date:
Page 36 of 38

m Sample Condition Upon Receipt{SCUR) rage i os z
CeAf1dIytICal Document No.: Issuing Authority:
F-CAR-CS-033-Rev.06 Pace Carolinas Quality Office
*Check rnarlc top half of box If pH and/or dechlorination is Project# I92439904
verified and within the acceptance range for preservation WO
samples. Due pate: 08/12/19
CLIENT:
Exceptions: VOA, CDliform, TOC, Oil and Grease, CRO/8015 {water) DOC, LLHk N
"Bottom half of box is to list number of bottle CLIENTT : 92-Nova NC
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Sample ID Type of Preservative pH upon receipt 4ate preservation adjusted Tune preservation Amount Of Preservative Lot q
adjusted I added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will heientta the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Page 37 of 38

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Page 38 of 38

lacieAnalXical"
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
September 24, 2019
Mike Minett
Nova Consulting Group, Inc.
442 South Main Street
Suite #7
Davidson, NC 28036
RE: Project: J 19-5100
Pace Project No.: 92445717
Dear Mike Minett:
Enclosed are the analytical results for sample(s) received by the laboratory on September 16, 2019.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: J19-5100
Pace Project No.: 92445717
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
J19-5100
92445717
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92445717001
S13-1 9'
EPA 8270E
PKS
21
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92445717002
S13-1 14'
EPA 8270E
PKS
21
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92445717003
S13-2 14'
EPA 8270E
PKS
21
PASI-C
EPA 8260D
CL
70
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92445717004
MW-1
EPA 8270E by SIM
PKS
21
PASI-C
EPA 8260D
DLK
63
PASI-C
92445717005
MW-2
EPA 8270E by SIM
PKS
21
PASI-C
EPA 8260D
DLK
63
PASI-C
92445717006
MW-3
EPA 8270E by SIM
PKS
21
PASI-C
EPA 8260D
DLK
63
PASI-C
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC. Page 3 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92445717
Sample: SB-1 9'
Lab ID: 92445717001
Collected: 09/16/19
11:25
Received: 09/16/19 14:40 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270E MSSV MW PAH by SIM
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Acenaphthene
ND
ug/kg
12.6
1
09/18/19 10:45
09/19/19 12:16
83-32-9
Acenaphthylene
ND
ug/kg
12.6
1
09/18/19 10:45
09/19/19 12:16
208-96-8
Anthracene
ND
ug/kg
12.6
1
09/18/19 10:45
09/19/19 12:16
120-12-7
Benzo(a)anthracene
ND
ug/kg
12.6
1
09/18/19 10:45
09/19/19 12:16
56-55-3
Benzo(a)pyrene
ND
ug/kg
12.6
1
09/18/19 10:45
09/19/19 12:16
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
12.6
1
09/18/19 10:45
09/19/19 12:16
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
12.6
1
09/18/19 10:45
09/19/19 12:16
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
12.6
1
09/18/19 10:45
09/19/19 12:16
207-08-9
Chrysene
ND
ug/kg
12.6
1
09/18/19 10:45
09/19/19 12:16
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
12.6
1
09/18/19 10:45
09/19/19 12:16
53-70-3
Fluoranthene
ND
ug/kg
12.6
1
09/18/19 10:45
09/19/19 12:16
206-44-0
Fluorene
ND
ug/kg
12.6
1
09/18/19 10:45
09/19/19 12:16
86-73-7
Indeno(1,2,3-cd)pyrene
ND
ug/kg
12.6
1
09/18/19 10:45
09/19/19 12:16
193-39-5
1-Methylnaphthalene
ND
ug/kg
12.6
1
09/18/19 10:45
09/19/19 12:16
90-12-0
2-Methylnaphthalene
ND
ug/kg
12.6
1
09/18/19 10:45
09/19/19 12:16
91-57-6
Naphthalene
ND
ug/kg
12.6
1
09/18/19 10:45
09/19/19 12:16
91-20-3
Phenanthrene
ND
ug/kg
12.6
1
09/18/19 10:45
09/19/19 12:16
85-01-8
Pyrene
ND
ug/kg
12.6
1
09/18/19 10:45
09/19/19 12:16
129-00-0
Surrogates
2-Fluorobiphenyl (S)
69
%
10-110
1
09/18/19 10:45
09/19/19 12:16
321-60-8
Nitrobenzene-d5 (S)
69
%
10-128
1
09/18/19 10:45
09/19/19 12:16
4165-60-0
Terphenyl-d14 (S)
82
%
39-119
1
09/18/19 10:45
09/19/19 12:16
1718-51-0
826013/5035A Volatile Organics
Analytical Method: EPA 8260D Preparation Method:
EPA 5035A
Acetone
ND
ug/kg
98.2
1
09/21/19 11:49
09/21/19 16:01
67-64-1
Benzene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
71-43-2
Bromobenzene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
108-86-1
Bromochloromethane
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
74-97-5
Bromodichloromethane
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
75-27-4
Bromoform
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
75-25-2
Bromomethane
ND
ug/kg
9.8
1
09/21/19 11:49
09/21/19 16:01
74-83-9 v2
2-Butanone (MEK)
ND
ug/kg
98.2
1
09/21/19 11:49
09/21/19 16:01
78-93-3
n-Butylbenzene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
104-51-8
sec-Butylbenzene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
135-98-8
tert-Butyl benzene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
98-06-6
Carbon tetrachloride
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
56-23-5
Chlorobenzene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
108-90-7
Chloroethane
ND
ug/kg
9.8
1
09/21/19 11:49
09/21/19 16:01
75-00-3 v2
Chloroform
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
67-66-3
Chloromethane
ND
ug/kg
9.8
1
09/21/19 11:49
09/21/19 16:01
74-87-3 L1,v2
2-Chlorotoluene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
95-49-8
4-Chlorotoluene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
96-12-8
Dibromochloromethane
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
106-93-4
Dibromomethane
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
74-95-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92445717
Sample: S13-1 9'
Lab ID: 92445717001
Collected: 09/16/19
11:25
Received: 09/16/19 14:40 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
8260D/5035A Volatile Organics
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
1,2-Dichlorobenzene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
106-46-7
Dichlorodifluoromethane
ND
ug/kg
9.8
1
09/21/19 11:49
09/21/19 16:01
75-71-8
L1,v2
1,1-Dichloroethane
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
75-34-3
1,2-Dichloroethane
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
107-06-2
1,1-Dichloroethene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
156-60-5
1,2-Dichloropropane
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
78-87-5
1,3-Dichloropropane
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
142-28-9
2,2-Dichloropropane
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
594-20-7
1,1-Dichloropropene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
10061-02-6
Diisopropyl ether
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
108-20-3
Ethylbenzene
15.7
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
87-68-3
2-Hexanone
ND
ug/kg
49.1
1
09/21/19 11:49
09/21/19 16:01
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
98-82-8
p-Isopropyltoluene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
99-87-6
Methylene Chloride
ND
ug/kg
19.6
1
09/21/19 11:49
09/21/19 16:01
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
49.1
1
09/21/19 11:49
09/21/19 16:01
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
1634-04-4
Naphthalene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
91-20-3
n-Propylbenzene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
103-65-1
Styrene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
79-34-5
Tetrachloroethene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
127-18-4
Toluene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
79-00-5
Trichloroethene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
79-01-6
Trichlorofluoromethane
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
75-69-4
L1,v2
1,2,3-Trichloropropane
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
108-67-8
Vinyl acetate
ND
ug/kg
49.1
1
09/21/19 11:49
09/21/19 16:01
108-05-4
L1
Vinyl chloride
ND
ug/kg
9.8
1
09/21/19 11:49
09/21/19 16:01
75-01-4
L1,v2
Xylene (Total)
ND
ug/kg
9.8
1
09/21/19 11:49
09/21/19 16:01
1330-20-7
m&p-Xylene
ND
ug/kg
9.8
1
09/21/19 11:49
09/21/19 16:01
179601-23-1
o-Xylene
ND
ug/kg
4.9
1
09/21/19 11:49
09/21/19 16:01
95-47-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92445717
Sample: S13-1 9' Lab ID: 92445717001 Collected: 09/16/19 11:25 Received: 09/16/19 14:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
826013/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 09/24/2019 04:23 PM
107 %
103 %
97 %
Analytical Method: ASTM D2974-87
20.1 %
70-130 1 09/21/1911:49 09/21/1916:01 2037-26-5
70-130 1 09/21/1911:49 09/21/1916:01 460-00-4
70-132 1 09/21/1911:49 09/21/1916:01 17060-07-0
0.10 1 09/16/19 16:49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92445717
Sample: SB-1 14'
Lab ID: 92445717002
Collected: 09/16/19
11:30
Received: 09/16/19 14:40 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent
moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270E MSSV MW PAH by SIM
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Acenaphthene
ND
ug/kg
11.5
1
09/18/19 10:45
09/19/19 12:37
83-32-9
Acenaphthylene
ND
ug/kg
11.5
1
09/18/19 10:45
09/19/19 12:37
208-96-8
Anthracene
ND
ug/kg
11.5
1
09/18/19 10:45
09/19/19 12:37
120-12-7
Benzo(a)anthracene
ND
ug/kg
11.5
1
09/18/19 10:45
09/19/19 12:37
56-55-3
Benzo(a)pyrene
ND
ug/kg
11.5
1
09/18/19 10:45
09/19/19 12:37
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
11.5
1
09/18/19 10:45
09/19/19 12:37
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
11.5
1
09/18/19 10:45
09/19/19 12:37
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
11.5
1
09/18/19 10:45
09/19/19 12:37
207-08-9
Chrysene
ND
ug/kg
11.5
1
09/18/19 10:45
09/19/19 12:37
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
11.5
1
09/18/19 10:45
09/19/19 12:37
53-70-3
Fluoranthene
ND
ug/kg
11.5
1
09/18/19 10:45
09/19/19 12:37
206-44-0
Fluorene
ND
ug/kg
11.5
1
09/18/19 10:45
09/19/19 12:37
86-73-7
Indeno(1,2,3-cd)pyrene
ND
ug/kg
11.5
1
09/18/19 10:45
09/19/19 12:37
193-39-5
1-Methylnaphthalene
116
ug/kg
11.5
1
09/18/19 10:45
09/19/19 12:37
90-12-0
2-Methylnaphthalene
262
ug/kg
11.5
1
09/18/19 10:45
09/19/19 12:37
91-57-6
Naphthalene
82.5
ug/kg
11.5
1
09/18/19 10:45
09/19/19 12:37
91-20-3
Phenanthrene
ND
ug/kg
11.5
1
09/18/19 10:45
09/19/19 12:37
85-01-8
Pyrene
ND
ug/kg
11.5
1
09/18/19 10:45
09/19/19 12:37
129-00-0
Surrogates
2-Fluorobiphenyl (S)
60
%
10-110
1
09/18/19 10:45
09/19/19 12:37
321-60-8
Nitrobenzene-d5 (S)
74
%
10-128
1
09/18/19 10:45
09/19/19 12:37
4165-60-0
Terphenyl-d14 (S)
72
%
39-119
1
09/18/19 10:45
09/19/19 12:37
1718-51-0
826013/5035A Volatile Organics
Analytical Method: EPA 8260D
Preparation Method:
EPA 5035A
Acetone
ND
ug/kg
117
1
09/21/19 11:49
09/21/19 16:26
67-64-1
Benzene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
71-43-2
Bromobenzene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
108-86-1
Bromochloromethane
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
74-97-5
Bromodichloromethane
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
75-27-4
Bromoform
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
75-25-2
Bromomethane
ND
ug/kg
11.7
1
09/21/19 11:49
09/21/19 16:26
74-83-9 v2
2-Butanone (MEK)
ND
ug/kg
117
1
09/21/19 11:49
09/21/19 16:26
78-93-3
n-Butylbenzene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
104-51-8
sec-Butylbenzene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
135-98-8
tert-Butyl benzene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
98-06-6
Carbon tetrachloride
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
56-23-5
Chlorobenzene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
108-90-7
Chloroethane
ND
ug/kg
11.7
1
09/21/19 11:49
09/21/19 16:26
75-00-3 v2
Chloroform
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
67-66-3
Chloromethane
ND
ug/kg
11.7
1
09/21/19 11:49
09/21/19 16:26
74-87-3 L1,v2
2-Chlorotoluene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
95-49-8
4-Chlorotoluene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
96-12-8
Dibromochloromethane
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
106-93-4
Dibromomethane
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
74-95-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92445717
Sample: S13-1 14'
Lab ID: 92445717002
Collected: 09/16/19
11:30
Received: 09/16/19 14:40 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent
moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
8260D/5035A Volatile Organics
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
1,2-Dichlorobenzene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
106-46-7
Dichlorodifluoromethane
ND
ug/kg
11.7
1
09/21/19 11:49
09/21/19 16:26
75-71-8
L1,v2
1,1-Dichloroethane
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
75-34-3
1,2-Dichloroethane
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
107-06-2
1,1-Dichloroethene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
156-60-5
1,2-Dichloropropane
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
78-87-5
1,3-Dichloropropane
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
142-28-9
2,2-Dichloropropane
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
594-20-7
1,1-Dichloropropene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
10061-02-6
Diisopropyl ether
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
108-20-3
Ethylbenzene
16.0
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
87-68-3
2-Hexanone
ND
ug/kg
58.5
1
09/21/19 11:49
09/21/19 16:26
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
98-82-8
p-Isopropyltoluene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
99-87-6
Methylene Chloride
ND
ug/kg
23.4
1
09/21/19 11:49
09/21/19 16:26
75-09-2
v2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
58.5
1
09/21/19 11:49
09/21/19 16:26
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
1634-04-4
Naphthalene
8.8
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
91-20-3
n-Propylbenzene
9.1
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
103-65-1
Styrene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
79-34-5
Tetrachloroethene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
127-18-4
Toluene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
79-00-5
Trichloroethene
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
79-01-6
Trichlorofluoromethane
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
75-69-4
L1,v2
1,2,3-Trichloropropane
ND
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
96-18-4
1,2,4-Trimethylbenzene
39.1
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
95-63-6
1,3,5-Trimethylbenzene
12.4
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
108-67-8
Vinyl acetate
ND
ug/kg
58.5
1
09/21/19 11:49
09/21/19 16:26
108-05-4
L1
Vinyl chloride
ND
ug/kg
11.7
1
09/21/19 11:49
09/21/19 16:26
75-01-4
L1,v2
Xylene (Total)
36.9
ug/kg
11.7
1
09/21/19 11:49
09/21/19 16:26
1330-20-7
m&p-Xylene
29.0
ug/kg
11.7
1
09/21/19 11:49
09/21/19 16:26
179601-23-1
o-Xylene
7.9
ug/kg
5.8
1
09/21/19 11:49
09/21/19 16:26
95-47-6
REPORT OF LABORATORY ANALYSIS
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Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 46

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ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92445717
Sample: S13-1 14' Lab ID: 92445717002 Collected: 09/16/19 11:30 Received: 09/16/19 14:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
826013/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 09/24/2019 04:23 PM
106 %
99 %
86 %
Analytical Method: ASTM D2974-87
11.5 %
70-130 1 09/21/1911:49 09/21/1916:26 2037-26-5
70-130 1 09/21/1911:49 09/21/1916:26 460-00-4
70-132 1 09/21/1911:49 09/21/1916:26 17060-07-0
0.10 1 09/16/19 16:49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 46

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9800 Kincey Ave. Suite 100
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ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92445717
Sample: SB-2 14'
Lab ID: 92445717003
Collected: 09/16/19
12:00
Received: 09/16/19 14:40 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent
moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270E MSSV MW PAH by SIM
Analytical Method: EPA 8270E Preparation Method: EPA 3546
Acenaphthene
ND
ug/kg
13.8
1
09/18/19 10:45
09/19/19 12:58
83-32-9
Acenaphthylene
ND
ug/kg
13.8
1
09/18/19 10:45
09/19/19 12:58
208-96-8
Anthracene
ND
ug/kg
13.8
1
09/18/19 10:45
09/19/19 12:58
120-12-7
Benzo(a)anthracene
ND
ug/kg
13.8
1
09/18/19 10:45
09/19/19 12:58
56-55-3
Benzo(a)pyrene
ND
ug/kg
13.8
1
09/18/19 10:45
09/19/19 12:58
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
13.8
1
09/18/19 10:45
09/19/19 12:58
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
13.8
1
09/18/19 10:45
09/19/19 12:58
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
13.8
1
09/18/19 10:45
09/19/19 12:58
207-08-9
Chrysene
ND
ug/kg
13.8
1
09/18/19 10:45
09/19/19 12:58
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
13.8
1
09/18/19 10:45
09/19/19 12:58
53-70-3
Fluoranthene
ND
ug/kg
13.8
1
09/18/19 10:45
09/19/19 12:58
206-44-0
Fluorene
ND
ug/kg
13.8
1
09/18/19 10:45
09/19/19 12:58
86-73-7
Indeno(1,2,3-cd)pyrene
ND
ug/kg
13.8
1
09/18/19 10:45
09/19/19 12:58
193-39-5
1-Methylnaphthalene
ND
ug/kg
13.8
1
09/18/19 10:45
09/19/19 12:58
90-12-0
2-Methylnaphthalene
ND
ug/kg
13.8
1
09/18/19 10:45
09/19/19 12:58
91-57-6
Naphthalene
ND
ug/kg
13.8
1
09/18/19 10:45
09/19/19 12:58
91-20-3
Phenanthrene
ND
ug/kg
13.8
1
09/18/19 10:45
09/19/19 12:58
85-01-8
Pyrene
ND
ug/kg
13.8
1
09/18/19 10:45
09/19/19 12:58
129-00-0
Surrogates
2-Fluorobiphenyl (S)
64
%
10-110
1
09/18/19 10:45
09/19/19 12:58
321-60-8
Nitrobenzene-d5 (S)
66
%
10-128
1
09/18/19 10:45
09/19/19 12:58
4165-60-0
Terphenyl-d14 (S)
84
%
39-119
1
09/18/19 10:45
09/19/19 12:58
1718-51-0
826013/5035A Volatile Organics
Analytical Method: EPA 8260D
Preparation Method:
EPA 5035A
Acetone
ND
ug/kg
121
1
09/21/19 11:49
09/21/19 16:51
67-64-1
Benzene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
71-43-2
Bromobenzene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
108-86-1
Bromochloromethane
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
74-97-5
Bromodichloromethane
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
75-27-4
Bromoform
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
75-25-2
Bromomethane
ND
ug/kg
12.1
1
09/21/19 11:49
09/21/19 16:51
74-83-9 v2
2-Butanone (MEK)
ND
ug/kg
121
1
09/21/19 11:49
09/21/19 16:51
78-93-3
n-Butylbenzene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
104-51-8
sec-Butylbenzene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
135-98-8
tert-Butyl benzene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
98-06-6
Carbon tetrachloride
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
56-23-5
Chlorobenzene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
108-90-7
Chloroethane
ND
ug/kg
12.1
1
09/21/19 11:49
09/21/19 16:51
75-00-3 v2
Chloroform
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
67-66-3
Chloromethane
ND
ug/kg
12.1
1
09/21/19 11:49
09/21/19 16:51
74-87-3 L1,v2
2-Chlorotoluene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
95-49-8
4-Chlorotoluene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
96-12-8
Dibromochloromethane
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
106-93-4
Dibromomethane
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
74-95-3
REPORT OF LABORATORY ANALYSIS
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Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 46

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ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92445717
Sample: S13-2 14'
Lab ID: 92445717003
Collected: 09/16/19
12:00
Received: 09/16/19 14:40 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent
moisture, sample size and any dilutions.
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
8260D/5035A Volatile Organics
Analytical Method: EPA 8260D Preparation Method: EPA 5035A
1,2-Dichlorobenzene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
106-46-7
Dichlorodifluoromethane
ND
ug/kg
12.1
1
09/21/19 11:49
09/21/19 16:51
75-71-8
L1,v2
1,1-Dichloroethane
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
75-34-3
1,2-Dichloroethane
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
107-06-2
1,1-Dichloroethene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
75-35-4
cis-1,2-Dichloroethene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
156-59-2
trans-1,2-Dichloroethene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
156-60-5
1,2-Dichloropropane
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
78-87-5
1,3-Dichloropropane
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
142-28-9
2,2-Dichloropropane
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
594-20-7
1,1-Dichloropropene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
563-58-6
cis-1,3-Dichloropropene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
10061-02-6
Diisopropyl ether
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
108-20-3
Ethylbenzene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
100-41-4
Hexachloro-1,3-butadiene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
87-68-3
2-Hexanone
ND
ug/kg
60.7
1
09/21/19 11:49
09/21/19 16:51
591-78-6
Isopropylbenzene (Cumene)
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
98-82-8
p-Isopropyltoluene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
99-87-6
Methylene Chloride
ND
ug/kg
24.3
1
09/21/19 11:49
09/21/19 16:51
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/kg
60.7
1
09/21/19 11:49
09/21/19 16:51
108-10-1
Methyl-tert-butyl ether
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
1634-04-4
Naphthalene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
91-20-3
n-Propylbenzene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
103-65-1
Styrene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
79-34-5
Tetrachloroethene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
127-18-4
Toluene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
108-88-3
1,2,3-Trichlorobenzene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
87-61-6
1,2,4-Trichlorobenzene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
120-82-1
1,1,1-Trichloroethane
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
71-55-6
1,1,2-Trichloroethane
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
79-00-5
Trichloroethene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
79-01-6
Trichlorofluoromethane
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
75-69-4
L1,v2
1,2,3-Trichloropropane
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
96-18-4
1,2,4-Trimethylbenzene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
95-63-6
1,3,5-Trimethylbenzene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
108-67-8
Vinyl acetate
ND
ug/kg
60.7
1
09/21/19 11:49
09/21/19 16:51
108-05-4
L1
Vinyl chloride
ND
ug/kg
12.1
1
09/21/19 11:49
09/21/19 16:51
75-01-4
L1,v2
Xylene (Total)
ND
ug/kg
12.1
1
09/21/19 11:49
09/21/19 16:51
1330-20-7
m&p-Xylene
ND
ug/kg
12.1
1
09/21/19 11:49
09/21/19 16:51
179601-23-1
o-Xylene
ND
ug/kg
6.1
1
09/21/19 11:49
09/21/19 16:51
95-47-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 46

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92445717
Sample: S13-2 14' Lab ID: 92445717003 Collected: 09/16/19 12:00 Received: 09/16/19 14:40 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
826013/5035A Volatile Organics Analytical Method: EPA 8260D Preparation Method: EPA 5035A
Surrogates
Toluene-d8 (S)
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Percent Moisture
Percent Moisture
Date: 09/24/2019 04:23 PM
106 %
102 %
95 %
Analytical Method: ASTM D2974-87
28.0 %
70-130 1 09/21/1911:49 09/21/1916:51 2037-26-5
70-130 1 09/21/1911:49 09/21/1916:51 460-00-4
70-132 1 09/21/1911:49 09/21/1916:51 17060-07-0
0.10 1 09/16/19 16:49
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 12 of 46

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92445717
Sample: MW-1
Lab ID: 92445717004 Collected:
09/16/19
12:55
Received: 09/16/19 14:40 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270E Low Volume PAH SIM
Analytical Method:
EPA 8270E by SIM Preparation Method:
EPA 3511
Acenaphthene
ND
ug/L
0.50
1
09/23/19 16:08
09/23/19 19:00
83-32-9
Acenaphthylene
ND
ug/L
0.50
1
09/23/19 16:08
09/23/19 19:00
208-96-8
Anthracene
ND
ug/L
0.050
1
09/23/19 16:08
09/23/19 19:00
120-12-7
Benzo(a)anthracene
ND
ug/L
0.050
1
09/23/19 16:08
09/23/19 19:00
56-55-3
Benzo(a)pyrene
ND
ug/L
0.10
1
09/23/19 16:08
09/23/19 19:00
50-32-8
Benzo(b)fluoranthene
ND
ug/L
0.050
1
09/23/19 16:08
09/23/19 19:00
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
0.20
1
09/23/19 16:08
09/23/19 19:00
191-24-2
Benzo(k)fluoranthene
ND
ug/L
0.20
1
09/23/19 16:08
09/23/19 19:00
207-08-9
Chrysene
ND
ug/L
0.10
1
09/23/19 16:08
09/23/19 19:00
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
0.15
1
09/23/19 16:08
09/23/19 19:00
53-70-3
Fluoranthene
ND
ug/L
0.30
1
09/23/19 16:08
09/23/19 19:00
206-44-0
Fluorene
ND
ug/L
0.31
1
09/23/19 16:08
09/23/19 19:00
86-73-7
Indeno(1,2,3-cd)pyrene
ND
ug/L
0.050
1
09/23/19 16:08
09/23/19 19:00
193-39-5
1-Methylnaphthalene
9.9
ug/L
0.80
1
09/23/19 16:08
09/23/19 19:00
90-12-0
2-Methylnaphthalene
18.4
ug/L
0.80
1
09/23/19 16:08
09/23/19 19:00
91-57-6
Naphthalene
78.1
ug/L
7.5
5
09/23/19 16:08
09/23/19 20:48
91-20-3
Phenanthrene
ND
ug/L
0.20
1
09/23/19 16:08
09/23/19 19:00
85-01-8
Pyrene
ND
ug/L
0.10
1
09/23/19 16:08
09/23/19 19:00
129-00-0
Surrogates
Nitrobenzene-d5 (S)
85
%
57-164
1
09/23/19 16:08
09/23/19 19:00
4165-60-0
2-Fluorobiphenyl (S)
93
%
45-150
1
09/23/19 16:08
09/23/19 19:00
321-60-8
Terphenyl-d14 (S)
111
%
38-153
1
09/23/19 16:08
09/23/19 19:00
1718-51-0
8260D MSV Low Level
Analytical Method:
EPA 8260D
Acetone
ND
ug/L
250
10
09/23/19 19:21
67-64-1
Benzene
208
ug/L
10.0
10
09/23/19 19:21
71-43-2
Bromobenzene
ND
ug/L
10.0
10
09/23/19 19:21
108-86-1
Bromochloromethane
ND
ug/L
10.0
10
09/23/19 19:21
74-97-5
Bromodichloromethane
ND
ug/L
10.0
10
09/23/19 19:21
75-27-4
Bromoform
ND
ug/L
10.0
10
09/23/19 19:21
75-25-2
Bromomethane
ND
ug/L
20.0
10
09/23/19 19:21
74-83-9
2-Butanone (MEK)
ND
ug/L
50.0
10
09/23/19 19:21
78-93-3
Carbon tetrachloride
ND
ug/L
10.0
10
09/23/19 19:21
56-23-5
Chlorobenzene
ND
ug/L
10.0
10
09/23/19 19:21
108-90-7
Chloroethane
ND
ug/L
10.0
10
09/23/19 19:21
75-00-3
Chloroform
ND
ug/L
50.0
10
09/23/19 19:21
67-66-3
Chloromethane
ND
ug/L
10.0
10
09/23/19 19:21
74-87-3
2-Chlorotoluene
ND
ug/L
10.0
10
09/23/19 19:21
95-49-8
4-Chlorotoluene
ND
ug/L
10.0
10
09/23/19 19:21
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
50.0
10
09/23/19 19:21
96-12-8
Dibromochloromethane
ND
ug/L
10.0
10
09/23/19 19:21
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
10.0
10
09/23/19 19:21
106-93-4
Dibromomethane
ND
ug/L
10.0
10
09/23/19 19:21
74-95-3
1,2-Dichlorobenzene
ND
ug/L
10.0
10
09/23/19 19:21
95-50-1
1,3-Dichlorobenzene
ND
ug/L
10.0
10
09/23/19 19:21
541-73-1
1,4-Dichlorobenzene
ND
ug/L
10.0
10
09/23/19 19:21
106-46-7
Dichlorodifluoromethane
ND
ug/L
10.0
10
09/23/19 19:21
75-71-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 46

aceAnalXical
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Pace Analytical Services, LLC
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ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92445717
Sample: MW-1 Lab ID: 92445717004 Collected: 09/16/19 12:55 Received: 09/16/19 14:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/24/2019 04:23 PM
Analytical Method: EPA 8260D
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
1480
ug/L
ND
ug/L
ND
ug/L
11.3
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
245
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
211
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
5710
ug/L
3870
ug/L
1840
ug/L
99 %
83 %
120 %
10.0
10
09/23/19 19:21
75-34-3
10.0
10
09/23/19 19:21
107-06-2
10.0
10
09/23/19 19:21
75-35-4
10.0
10
09/23/19 19:21
156-59-2
10.0
10
09/23/19 19:21
156-60-5
10.0
10
09/23/19 19:21
78-87-5
10.0
10
09/23/19 19:21
142-28-9
10.0
10
09/23/19 19:21
594-20-7
10.0
10
09/23/19 19:21
563-58-6
10.0
10
09/23/19 19:21
10061-01-5
10.0
10
09/23/19 19:21
10061-02-6
10.0
10
09/23/19 19:21
108-20-3
10.0
10
09/23/19 19:21
100-41-4
10.0
10
09/23/19 19:21
87-68-3
50.0
10
09/23/19 19:21
591-78-6
10.0
10
09/23/19 19:21
99-87-6
50.0
10
09/23/19 19:21
75-09-2
50.0
10
09/23/19 19:21
108-10-1
10.0
10
09/23/19 19:21
1634-04-4
10.0
10
09/23/19 19:21
91-20-3
10.0
10
09/23/19 19:21
100-42-5
10.0
10
09/23/19 19:21
630-20-6
10.0
10
09/23/19 19:21
79-34-5
10.0
10
09/23/19 19:21
127-18-4
10.0
10
09/23/19 19:21
108-88-3
10.0
10
09/23/19 19:21
87-61-6
10.0
10
09/23/19 19:21
120-82-1
10.0
10
09/23/19 19:21
71-55-6
10.0
10
09/23/19 19:21
79-00-5
10.0
10
09/23/19 19:21
79-01-6
10.0
10
09/23/19 19:21
75-69-4
10.0
10
09/23/19 19:21
96-18-4
20.0
10
09/23/19 19:21
108-05-4
10.0
10
09/23/19 19:21
75-01-4
10.0
10
09/23/19 19:21
1330-20-7
20.0
10
09/23/19 19:21
179601-23-1
10.0
10
09/23/19 19:21
95-47-6
70-130 10
70-130 10
70-130 10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
09/23/19 19:21 460-00-4
09/23/19 19:21 17060-07-0
09/23/19 19:21 2037-26-5
Page 14 of 46

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92445717
Sample: MW-2
Lab ID: 92445717005 Collected:
09/16/19
13:35
Received: 09/16/19 14:40 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270E Low Volume PAH SIM
Analytical Method:
EPA 8270E by SIM Preparation Method:
EPA 3511
Acenaphthene
ND
ug/L
0.50
1
09/23/19 16:08
09/23/19 19:22
83-32-9
Acenaphthylene
ND
ug/L
0.50
1
09/23/19 16:08
09/23/19 19:22
208-96-8
Anthracene
ND
ug/L
0.050
1
09/23/19 16:08
09/23/19 19:22
120-12-7
Benzo(a)anthracene
ND
ug/L
0.050
1
09/23/19 16:08
09/23/19 19:22
56-55-3
Benzo(a)pyrene
ND
ug/L
0.10
1
09/23/19 16:08
09/23/19 19:22
50-32-8
Benzo(b)fluoranthene
ND
ug/L
0.050
1
09/23/19 16:08
09/23/19 19:22
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
0.20
1
09/23/19 16:08
09/23/19 19:22
191-24-2
Benzo(k)fluoranthene
ND
ug/L
0.20
1
09/23/19 16:08
09/23/19 19:22
207-08-9
Chrysene
ND
ug/L
0.10
1
09/23/19 16:08
09/23/19 19:22
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
0.15
1
09/23/19 16:08
09/23/19 19:22
53-70-3
Fluoranthene
ND
ug/L
0.30
1
09/23/19 16:08
09/23/19 19:22
206-44-0
Fluorene
ND
ug/L
0.31
1
09/23/19 16:08
09/23/19 19:22
86-73-7
Indeno(1,2,3-cd)pyrene
ND
ug/L
0.050
1
09/23/19 16:08
09/23/19 19:22
193-39-5
1-Methylnaphthalene
4.1
ug/L
0.80
1
09/23/19 16:08
09/23/19 19:22
90-12-0
2-Methylnaphthalene
8.0
ug/L
0.80
1
09/23/19 16:08
09/23/19 19:22
91-57-6
Naphthalene
63.0
ug/L
7.5
5
09/23/19 16:08
09/23/19 21:09
91-20-3
Phenanthrene
ND
ug/L
0.20
1
09/23/19 16:08
09/23/19 19:22
85-01-8
Pyrene
ND
ug/L
0.10
1
09/23/19 16:08
09/23/19 19:22
129-00-0
Surrogates
Nitrobenzene-d5 (S)
149
%
57-164
1
09/23/19 16:08
09/23/19 19:22
4165-60-0
2-Fluorobiphenyl (S)
97
%
45-150
1
09/23/19 16:08
09/23/19 19:22
321-60-8
Terphenyl-d14 (S)
114
%
38-153
1
09/23/19 16:08
09/23/19 19:22
1718-51-0
8260D MSV Low Level
Analytical Method:
EPA 8260D
Acetone
ND
ug/L
1250
50
09/23/19 19:40
67-64-1
Benzene
2380
ug/L
50.0
50
09/23/19 19:40
71-43-2
Bromobenzene
ND
ug/L
50.0
50
09/23/19 19:40
108-86-1
Bromochloromethane
ND
ug/L
50.0
50
09/23/19 19:40
74-97-5
Bromodichloromethane
ND
ug/L
50.0
50
09/23/19 19:40
75-27-4
Bromoform
ND
ug/L
50.0
50
09/23/19 19:40
75-25-2
Bromomethane
ND
ug/L
100
50
09/23/19 19:40
74-83-9
2-Butanone (MEK)
ND
ug/L
250
50
09/23/19 19:40
78-93-3
Carbon tetrachloride
ND
ug/L
50.0
50
09/23/19 19:40
56-23-5
Chlorobenzene
ND
ug/L
50.0
50
09/23/19 19:40
108-90-7
Chloroethane
ND
ug/L
50.0
50
09/23/19 19:40
75-00-3
Chloroform
ND
ug/L
250
50
09/23/19 19:40
67-66-3
Chloromethane
ND
ug/L
50.0
50
09/23/19 19:40
74-87-3
2-Chlorotoluene
ND
ug/L
50.0
50
09/23/19 19:40
95-49-8
4-Chlorotoluene
ND
ug/L
50.0
50
09/23/19 19:40
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
250
50
09/23/19 19:40
96-12-8
Dibromochloromethane
ND
ug/L
50.0
50
09/23/19 19:40
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
50.0
50
09/23/19 19:40
106-93-4
Dibromomethane
ND
ug/L
50.0
50
09/23/19 19:40
74-95-3
1,2-Dichlorobenzene
ND
ug/L
50.0
50
09/23/19 19:40
95-50-1
1,3-Dichlorobenzene
ND
ug/L
50.0
50
09/23/19 19:40
541-73-1
1,4-Dichlorobenzene
ND
ug/L
50.0
50
09/23/19 19:40
106-46-7
Dichlorodifluoromethane
ND
ug/L
50.0
50
09/23/19 19:40
75-71-8
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 46

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92445717
Sample: MW-2 Lab ID: 92445717005 Collected: 09/16/19 13:35 Received: 09/16/19 14:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/24/2019 04:23 PM
Analytical Method: EPA 8260D
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
3940
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
90.5
ug/L
213
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
396
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
14300
ug/L
12100
ug/L
2230
ug/L
100 %
83 %
117 %
50.0
50
09/23/1919:40
75-34-3
50.0
50
09/23/1919:40
107-06-2
50.0
50
09/23/1919:40
75-35-4
50.0
50
09/23/1919:40
156-59-2
50.0
50
09/23/1919:40
156-60-5
50.0
50
09/23/1919:40
78-87-5
50.0
50
09/23/1919:40
142-28-9
50.0
50
09/23/1919:40
594-20-7
50.0
50
09/23/1919:40
563-58-6
50.0
50
09/23/1919:40
10061-01-5
50.0
50
09/23/1919:40
10061-02-6
50.0
50
09/23/1919:40
108-20-3
50.0
50
09/23/1919:40
100-41-4
50.0
50
09/23/1919:40
87-68-3
250
50
09/23/1919:40
591-78-6
50.0
50
09/23/1919:40
99-87-6
250
50
09/23/1919:40
75-09-2
250
50
09/23/1919:40
108-10-1
50.0
50
09/23/1919:40
1634-04-4
50.0
50
09/23/1919:40
91-20-3
50.0
50
09/23/1919:40
100-42-5
50.0
50
09/23/1919:40
630-20-6
50.0
50
09/23/1919:40
79-34-5
50.0
50
09/23/1919:40
127-18-4
50.0
50
09/23/1919:40
108-88-3
50.0
50
09/23/1919:40
87-61-6
50.0
50
09/23/1919:40
120-82-1
50.0
50
09/23/1919:40
71-55-6
50.0
50
09/23/1919:40
79-00-5
50.0
50
09/23/1919:40
79-01-6
50.0
50
09/23/1919:40
75-69-4
50.0
50
09/23/1919:40
96-18-4
100
50
09/23/1919:40
108-05-4
50.0
50
09/23/1919:40
75-01-4
50.0
50
09/23/1919:40
1330-20-7
100
50
09/23/1919:40
179601-23-1
50.0
50
09/23/1919:40
95-47-6
70-130 50
70-130 50
70-130 50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
09/23/1919:40 460-00-4
09/23/19 19:40 17060-07-0
09/23/1919:40 2037-26-5
Page 16 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92445717
Sample: MW-3 Lab ID: 92445717006 Collected: 09/16/19 14:20 Received: 09/16/19 14:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270E Low Volume PAH SIM Analytical Method: EPA 8270E by SIM Preparation Method: EPA 3511
Acenaphthene
ND
ug/L
0.50
1
09/23/19 16:08
09/23/19 19:43
83-32-9
Acenaphthylene
ND
ug/L
0.50
1
09/23/19 16:08
09/23/19 19:43
208-96-8
Anthracene
ND
ug/L
0.050
1
09/23/19 16:08
09/23/19 19:43
120-12-7
Benzo(a)anthracene
ND
ug/L
0.050
1
09/23/19 16:08
09/23/19 19:43
56-55-3
Benzo(a)pyrene
ND
ug/L
0.10
1
09/23/19 16:08
09/23/19 19:43
50-32-8
Benzo(b)fluoranthene
ND
ug/L
0.050
1
09/23/19 16:08
09/23/19 19:43
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
0.20
1
09/23/19 16:08
09/23/19 19:43
191-24-2
Benzo(k)fluoranthene
ND
ug/L
0.20
1
09/23/19 16:08
09/23/19 19:43
207-08-9
Chrysene
ND
ug/L
0.10
1
09/23/19 16:08
09/23/19 19:43
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
0.15
1
09/23/19 16:08
09/23/19 19:43
53-70-3
Fluoranthene
ND
ug/L
0.30
1
09/23/19 16:08
09/23/19 19:43
206-44-0
Fluorene
ND
ug/L
0.31
1
09/23/19 16:08
09/23/19 19:43
86-73-7
Indeno(1,2,3-cd)pyrene
ND
ug/L
0.050
1
09/23/19 16:08
09/23/19 19:43
193-39-5
1-Methylnaphthalene
ND
ug/L
0.80
1
09/23/19 16:08
09/23/19 19:43
90-12-0
2-Methylnaphthalene
ND
ug/L
0.80
1
09/23/19 16:08
09/23/19 19:43
91-57-6
Naphthalene
ND
ug/L
1.5
1
09/23/19 16:08
09/23/19 19:43
91-20-3
Phenanthrene
ND
ug/L
0.20
1
09/23/19 16:08
09/23/19 19:43
85-01-8
Pyrene
ND
ug/L
0.10
1
09/23/19 16:08
09/23/19 19:43
129-00-0
Surrogates
Nitrobenzene-d5 (S)
95
%
57-164
1
09/23/19 16:08
09/23/19 19:43
4165-60-0
2-Fluorobiphenyl (S)
88
%
45-150
1
09/23/19 16:08
09/23/19 19:43
321-60-8
Terphenyl-d14 (S)
98
%
38-153
1
09/23/19 16:08
09/23/19 19:43
1718-51-0
8260D MSV Low Level Analytical Method: EPA 8260D
Acetone
ND
ug/L
25.0
1
09/24/19 14:01
67-64-1
Benzene
ND
ug/L
1.0
1
09/24/19 14:01
71-43-2
Bromobenzene
ND
ug/L
1.0
1
09/24/19 14:01
108-86-1
Bromochloromethane
ND
ug/L
1.0
1
09/24/19 14:01
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
09/24/19 14:01
75-27-4
Bromoform
ND
ug/L
1.0
1
09/24/19 14:01
75-25-2
Bromomethane
ND
ug/L
2.0
1
09/24/19 14:01
74-83-9 v2
2-Butanone (MEK)
ND
ug/L
5.0
1
09/24/19 14:01
78-93-3
Carbon tetrachloride
ND
ug/L
1.0
1
09/24/19 14:01
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
09/24/19 14:01
108-90-7
Chloroethane
ND
ug/L
1.0
1
09/24/19 14:01
75-00-3
Chloroform
ND
ug/L
5.0
1
09/24/19 14:01
67-66-3
Chloromethane
ND
ug/L
1.0
1
09/24/19 14:01
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
1
09/24/19 14:01
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
1
09/24/19 14:01
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
09/24/19 14:01
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
09/24/19 14:01
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
1.0
1
09/24/19 14:01
106-93-4
Dibromomethane
ND
ug/L
1.0
1
09/24/19 14:01
74-95-3
1,2-Dichlorobenzene
ND
ug/L
1.0
1
09/24/19 14:01
95-50-1
1,3-Dichlorobenzene
ND
ug/L
1.0
1
09/24/19 14:01
541-73-1
1,4-Dichlorobenzene
ND
ug/L
1.0
1
09/24/19 14:01
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
1
09/24/19 14:01
75-71-8
REPORT OF LABORATORY ANALYSIS
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Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 46

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ANALYTICAL RESULTS
Project: J19-5100
Pace Project No.: 92445717
Sample: MW-3 Lab ID: 92445717006 Collected: 09/16/19 14:20 Received: 09/16/19 14:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 09/24/2019 04:23 PM
Analytical Method: EPA 8260D
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
108 %
85 %
110 %
1.0
1
09/24/19 14:01
75-34-3
1.0
1
09/24/19 14:01
107-06-2
1.0
1
09/24/19 14:01
75-35-4
1.0
1
09/24/19 14:01
156-59-2
1.0
1
09/24/19 14:01
156-60-5
1.0
1
09/24/19 14:01
78-87-5
1.0
1
09/24/19 14:01
142-28-9
1.0
1
09/24/19 14:01
594-20-7
1.0
1
09/24/19 14:01
563-58-6
1.0
1
09/24/19 14:01
10061-01-5
1.0
1
09/24/19 14:01
10061-02-6
1.0
1
09/24/19 14:01
108-20-3
1.0
1
09/24/19 14:01
100-41-4
1.0
1
09/24/19 14:01
87-68-3
5.0
1
09/24/19 14:01
591-78-6
1.0
1
09/24/19 14:01
99-87-6
5.0
1
09/24/19 14:01
75-09-2
5.0
1
09/24/19 14:01
108-10-1
1.0
1
09/24/19 14:01
1634-04-4
1.0
1
09/24/19 14:01
91-20-3
1.0
1
09/24/19 14:01
100-42-5
1.0
1
09/24/19 14:01
630-20-6
1.0
1
09/24/19 14:01
79-34-5
1.0
1
09/24/19 14:01
127-18-4
1.0
1
09/24/19 14:01
108-88-3
1.0
1
09/24/19 14:01
87-61-6
1.0
1
09/24/19 14:01
120-82-1
1.0
1
09/24/19 14:01
71-55-6
1.0
1
09/24/19 14:01
79-00-5
1.0
1
09/24/19 14:01
79-01-6
1.0
1
09/24/19 14:01
75-69-4
1.0
1
09/24/19 14:01
96-18-4
2.0
1
09/24/19 14:01
108-05-4
1.0
1
09/24/19 14:01
75-01-4
1.0
1
09/24/19 14:01
1330-20-7
2.0
1
09/24/19 14:01
179601-23-1
1.0
1
09/24/19 14:01
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
09/24/19 14:01 460-00-4
09/24/19 14:01 17060-07-0
09/24/19 14:01 2037-26-5
Page 18 of 46

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QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
QC Batch: 499141 Analysis Method: EPA 8260D
QC Batch Method: EPA 5035A Analysis Description: 8260D MSV 5035A Volatile Organics
Associated Lab Samples: 92445717001, 92445717002, 92445717003
METHOD BLANK: 2686540 Matrix:
Associated Lab Samples: 92445717001, 92445717002, 92445717003
Blank
Parameter Units Result
Solid
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/kg
ND
5.0
09/21/19 12:14
1,1,1-Trichloroethane
ug/kg
ND
5.0
09/21/19 12:14
1,1,2,2-Tetrachloroethane
ug/kg
ND
5.0
09/21/19 12:14
1,1,2-Trichloroethane
ug/kg
ND
5.0
09/21/19 12:14
1,1-Dichloroethane
ug/kg
ND
5.0
09/21/19 12:14
1,1-Dichloroethene
ug/kg
ND
5.0
09/21/19 12:14
1,1-Dichloropropene
ug/kg
ND
5.0
09/21/19 12:14
1,2,3-Trichlorobenzene
ug/kg
ND
5.0
09/21/19 12:14
1,2,3-Trichloropropane
ug/kg
ND
5.0
09/21/19 12:14
1,2,4-Trichlorobenzene
ug/kg
ND
5.0
09/21/19 12:14
1,2,4-Trimethylbenzene
ug/kg
ND
5.0
09/21/19 12:14
1,2-Dibromo-3-chloropropane
ug/kg
ND
5.0
09/21/19 12:14
1,2-Dibromoethane (EDB)
ug/kg
ND
5.0
09/21/19 12:14
1,2-Dichlorobenzene
ug/kg
ND
5.0
09/21/19 12:14
1,2-Dichloroethane
ug/kg
ND
5.0
09/21/19 12:14
1,2-Dichloropropane
ug/kg
ND
5.0
09/21/19 12:14
1,3,5-Trimethylbenzene
ug/kg
ND
5.0
09/21/19 12:14
1,3-Dichlorobenzene
ug/kg
ND
5.0
09/21/19 12:14
1,3-Dichloropropane
ug/kg
ND
5.0
09/21/19 12:14
1,4-Dichlorobenzene
ug/kg
ND
5.0
09/21/19 12:14
2,2-Dichloropropane
ug/kg
ND
5.0
09/21/19 12:14
2-Butanone (MEK)
ug/kg
ND
100
09/21/19 12:14
2-Chlorotoluene
ug/kg
ND
5.0
09/21/19 12:14
2-Hexanone
ug/kg
ND
50.0
09/21/19 12:14
4-Chlorotoluene
ug/kg
ND
5.0
09/21/19 12:14
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
50.0
09/21/19 12:14
Acetone
ug/kg
ND
100
09/21/19 12:14
Benzene
ug/kg
ND
5.0
09/21/19 12:14
Bromobenzene
ug/kg
ND
5.0
09/21/19 12:14
Bromochloromethane
ug/kg
ND
5.0
09/21/19 12:14
Bromodichloromethane
ug/kg
ND
5.0
09/21/19 12:14
Bromoform
ug/kg
ND
5.0
09/21/19 12:14
Bromomethane
ug/kg
ND
10.0
09/21/19 12:14
Carbon tetrachloride
ug/kg
ND
5.0
09/21/19 12:14
Chlorobenzene
ug/kg
ND
5.0
09/21/19 12:14
Chloroethane
ug/kg
ND
10.0
09/21/19 12:14
Chloroform
ug/kg
ND
5.0
09/21/19 12:14
Chloromethane
ug/kg
ND
10.0
09/21/19 12:14
cis-1,2-Dichloroethene
ug/kg
ND
5.0
09/21/19 12:14
cis-1,3-Dichloropropene
ug/kg
ND
5.0
09/21/19 12:14
Dibromochloromethane
ug/kg
ND
5.0
09/21/19 12:14
v1
v1
v1
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 46

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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
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QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
METHOD BLANK: 2686540 Matrix:
Associated Lab Samples: 92445717001, 92445717002, 92445717003
Blank
Parameter Units Result
Solid
Reporting
Limit
Analyzed
Dibromomethane
ug/kg
ND
5.0
09/21/19 12:14
Dichlorodifluoromethane
ug/kg
ND
10.0
09/21/19 12:14
Diisopropyl ether
ug/kg
ND
5.0
09/21/19 12:14
Ethylbenzene
ug/kg
ND
5.0
09/21/19 12:14
Hexachloro-1,3-butadiene
ug/kg
ND
5.0
09/21/19 12:14
Isopropylbenzene (Cumene)
ug/kg
ND
5.0
09/21/19 12:14
m&p-Xylene
ug/kg
ND
10.0
09/21/19 12:14
Methyl-tert-butyl ether
ug/kg
ND
5.0
09/21/19 12:14
Methylene Chloride
ug/kg
ND
20.0
09/21/19 12:14
n-Butylbenzene
ug/kg
ND
5.0
09/21/19 12:14
n-Propylbenzene
ug/kg
ND
5.0
09/21/19 12:14
Naphthalene
ug/kg
ND
5.0
09/21/19 12:14
o-Xylene
ug/kg
ND
5.0
09/21/19 12:14
p-Isopropyltoluene
ug/kg
ND
5.0
09/21/19 12:14
sec-Butylbenzene
ug/kg
ND
5.0
09/21/19 12:14
Styrene
ug/kg
ND
5.0
09/21/19 12:14
tert-Butyl benzene
ug/kg
ND
5.0
09/21/19 12:14
Tetrachloroethene
ug/kg
ND
5.0
09/21/19 12:14
Toluene
ug/kg
ND
5.0
09/21/19 12:14
trans-1,2-Dichloroethene
ug/kg
ND
5.0
09/21/19 12:14
trans- 1,3-Dichloropropene
ug/kg
ND
5.0
09/21/19 12:14
Trichloroethene
ug/kg
ND
5.0
09/21/19 12:14
Trichlorofluoromethane
ug/kg
ND
5.0
09/21/19 12:14
Vinyl acetate
ug/kg
ND
50.0
09/21/19 12:14
Vinyl chloride
ug/kg
ND
10.0
09/21/19 12:14
Xylene (Total)
ug/kg
ND
10.0
09/21/19 12:14
1,2-Dichloroethane-d4 (S)
%
93
70-132
09/21/19 12:14
4-Bromofluorobenzene (S)
%
104
70-130
09/21/19 12:14
Toluene-d8 (S)
%
105
70-130
09/21/19 12:14
v1
v1
v1
Qualifiers
LABORATORY CONTROL SAMPLE:
2686541
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
50
53.0
106
70-130
1,1,1-Trichloroethane
ug/kg
50
57.2
114
70-130
1,1,2,2-Tetrachloroethane
ug/kg
50
47.8
96
55-130
1,1,2-Trichloroethane
ug/kg
50
52.9
106
70-130
1,1-Dichloroethane
ug/kg
50
55.4
111
68-130
1,1-Dichloroethene
ug/kg
50
59.8
120
70-130
1,1-Dichloropropene
ug/kg
50
59.8
120
70-130
1,2,3-Trichlorobenzene
ug/kg
50
49.6
99
70-130
1,2,3-Trichloropropane
ug/kg
50
48.4
97
70-130
1,2,4-Trichlorobenzene
ug/kg
50
48.0
96
70-130
1,2,4-Trimethylbenzene
ug/kg
50
49.9
100
69-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 46

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Pace Analytical Services, LLC
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QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
LABORATORY CONTROL SAMPLE:
Parameter
2686541
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,2-Dibromo-3-chloropropane
ug/kg
50
47.6
95
57-141
1,2-Dibromoethane (EDB)
ug/kg
50
51.1
102
70-130
1,2-Dichlorobenzene
ug/kg
50
48.7
97
70-130
1,2-Dichloroethane
ug/kg
50
52.7
105
70-130
1,2-Dichloropropane
ug/kg
50
55.3
111
70-130
1,3,5-Trimethylbenzene
ug/kg
50
50.2
100
70-130
1,3-Dichlorobenzene
ug/kg
50
49.1
98
70-130
1,3-Dichloropropane
ug/kg
50
53.0
106
70-130
1,4-Dichlorobenzene
ug/kg
50
48.8
98
70-130
2,2-Dichloropropane
ug/kg
50
57.6
115
70-130
2-Butanone (MEK)
ug/kg
100
115
115
60-130
2-Chlorotoluene
ug/kg
50
48.9
98
70-130
2-Hexanone
ug/kg
100
97.6
98
70-132
4-Chlorotoluene
ug/kg
50
49.2
98
70-130
4-Methyl-2-pentanone (MIBK)
ug/kg
100
99.4
99
69-130
Acetone
ug/kg
100
115
115
49-148
Benzene
ug/kg
50
56.6
113
70-130
Bromobenzene
ug/kg
50
51.3
103
70-130
Bromochloromethane
ug/kg
50
54.4
109
70-130
Bromodichloromethane
ug/kg
50
53.9
108
70-130
Bromoform
ug/kg
50
49.0
98
68-136
Bromomethane
ug/kg
50
70.0
140
60-140 F3,v1
Carbon tetrachloride
ug/kg
50
53.1
106
70-130
Chlorobenzene
ug/kg
50
49.8
100
70-130
Chloroethane
ug/kg
50
68.6
137
51-147 v1
Chloroform
ug/kg
50
56.9
114
70-130
Chloromethane
ug/kg
50
87.0
174
48-130 F3,L1,v1
cis-1,2-Dichloroethene
ug/kg
50
54.4
109
70-130
cis-1,3-Dichloropropene
ug/kg
50
57.7
115
70-130
Dibromochloromethane
ug/kg
50
50.5
101
70-130
Dibromomethane
ug/kg
50
51.3
103
70-130
Dichlorodifluoromethane
ug/kg
50
156
311
49-130 F3,IK,L1,v1
Diisopropyl ether
ug/kg
50
59.2
118
66-130
Ethylbenzene
ug/kg
50
50.9
102
70-130
Hexachloro-1,3-butadiene
ug/kg
50
47.5
95
70-130
Isopropylbenzene (Cumene)
ug/kg
50
51.3
103
70-130
m&p-Xylene
ug/kg
100
102
102
70-130
Methyl-tert-butyl ether
ug/kg
50
55.5
111
70-130
Methylene Chloride
ug/kg
50
49.3
99
50-137
n-Butylbenzene
ug/kg
50
47.7
95
70-130
n-Propylbenzene
ug/kg
50
50.7
101
70-130
Naphthalene
ug/kg
50
47.6
95
70-131
o-Xylene
ug/kg
50
51.7
103
70-130
p-Isopropyltoluene
ug/kg
50
50.3
101
70-130
sec-Butylbenzene
ug/kg
50
52.0
104
70-130
Styrene
ug/kg
50
50.0
100
70-130
tert-Butyl benzene
ug/kg
50
45.5
91
69-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 46

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: J19-5100
Pace Project No.: 92445717
LABORATORY CONTROL SAMPLE: 2686541
Parameter
QUALITY CONTROL DATA
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
Tetrachloroethene
ug/kg
50
50.1
100
56-130
Toluene
ug/kg
50
52.6
105
70-130
trans-1,2-Dichloroethene
ug/kg
50
57.9
116
70-130
trans- 1,3-Dichloropropene
ug/kg
50
54.7
109
70-130
Trichloroethene
ug/kg
50
57.6
115
70-141
Trichlorofluoromethane
ug/kg
50
71.8
144
67-130 L1,v1
Vinyl acetate
ug/kg
100
149
149
10-136 L1
Vinyl chloride
ug/kg
50
72.4
145
67-130 F3,L1,v1
Xylene (Total)
ug/kg
150
154
103
70-130
1,2-Dichloroethane-d4 (S)
%
99
70-132
4-Bromofluorobenzene (S)
%
97
70-130
Toluene-d8 (S)
%
98
70-130
MATRIX SPIKE SAMPLE:
Parameter
2687239
Units
92445872002
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/kg
ND
22.4
20.4
91
52-133
1,1,1-Trichloroethane
ug/kg
ND
22.4
22.1
99
49-137
1,1,2,2-Tetrachloroethane
ug/kg
ND
22.4
19.9
89
39-150
1,1,2-Trichloroethane
ug/kg
ND
22.4
20.2
90
48-140
1,1-Dichloroethane
ug/kg
ND
22.4
22.4
100
46-135
1,1-Dichloroethene
ug/kg
ND
22.4
24.8
110
38-149
1,1-Dichloropropene
ug/kg
ND
22.4
21.6
96
41-140
1,2,3-Trichlorobenzene
ug/kg
ND
22.4
19.9
89
10-158
1,2,3-Trichloropropane
ug/kg
ND
22.4
21.8
97
33-157
1,2,4-Trichlorobenzene
ug/kg
ND
22.4
19.4
86
10-155
1,2,4-Trimethylbenzene
ug/kg
ND
22.4
22.0
89
24-154
1,2-Dibromo-3-chloropropane
ug/kg
ND
22.4
20.0
89
33-158
1,2-Dibromoethane (EDB)
ug/kg
ND
22.4
19.9
89
40-136
1,2-Dichlorobenzene
ug/kg
ND
22.4
19.8
88
27-146
1,2-Dichloroethane
ug/kg
ND
22.4
20.6
92
49-140
1,2-Dichloropropane
ug/kg
ND
22.4
20.7
92
44-143
1,3,5-Trimethylbenzene
ug/kg
ND
22.4
20.9
93
40-144
1,3-Dichlorobenzene
ug/kg
ND
22.4
20.0
89
33-140
1,3-Dichloropropane
ug/kg
ND
22.4
20.1
90
47-147
1,4-Dichlorobenzene
ug/kg
ND
22.4
19.8
88
35-139
2,2-Dichloropropane
ug/kg
ND
22.4
23.1
103
41-140
2-Butanone (MEK)
ug/kg
ND
44.9
33.9J
76
10-181
2-Chlorotoluene
ug/kg
ND
22.4
19.6
88
38-147
2-Hexanone
ug/kg
ND
44.9
42.5J
95
18-169
4-Chlorotoluene
ug/kg
ND
22.4
19.9
89
36-145
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
44.9
41.5J
92
16-175
Acetone
ug/kg
ND
44.9
39.5J
88
10-200
Benzene
ug/kg
ND
22.4
22.8
102
46-136
Bromobenzene
ug/kg
ND
22.4
20.4
91
38-149
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 46

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
MATRIX SPIKE SAMPLE:
2687239
92445872002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Bromochloromethane
ug/kg
ND
22.4
20.7
92
44-142
Bromodichloromethane
ug/kg
ND
22.4
21.6
96
41-140
Bromoform
ug/kg
ND
22.4
19.8
88
34-145
Bromomethane
ug/kg
ND
22.4
26.8
120
14-162
Carbon tetrachloride
ug/kg
ND
22.4
22.2
99
44-141
Chlorobenzene
ug/kg
ND
22.4
20.5
91
39-141
Chloroethane
ug/kg
ND
22.4
25.4
113
10-182
Chloroform
ug/kg
ND
22.4
21.2
94
45-140
Chloromethane
ug/kg
ND
22.4
23.4
104
19-149
cis-1,2-Dichloroethene
ug/kg
ND
22.4
21.6
96
38-150
cis-1,3-Dichloropropene
ug/kg
ND
22.4
21.0
94
30-144
Dibromochloromethane
ug/kg
ND
22.4
19.2
86
36-145
Dibromomethane
ug/kg
ND
22.4
21.0
94
41-145
Dichlorodifluoromethane
ug/kg
ND
22.4
24.2
108
16-146
Diisopropyl ether
ug/kg
ND
22.4
21.1
94
41-143
Ethylbenzene
ug/kg
2.5J
22.4
22.7
90
35-144
Hexachloro-1,3-butadiene
ug/kg
ND
22.4
20.2
90
10-160
Isopropylbenzene (Cumene)
ug/kg
ND
22.4
21.5
96
30-152
m&p-Xylene
ug/kg
8.5J
44.9
49.3
91
33-145
Methyl-tert-butyl ether
ug/kg
ND
22.4
22.0
98
49-140
Methylene Chloride
ug/kg
ND
22.4
ND
21
10-174
n-Butylbenzene
ug/kg
ND
22.4
20.4
91
10-160
n-Propylbenzene
ug/kg
ND
22.4
21.1
94
24-159
Naphthalene
ug/kg
ND
22.4
20.2
90
10-171
o-Xylene
ug/kg
3.2J
22.4
23.5
90
31-150
p-Isopropyltoluene
ug/kg
ND
22.4
20.3
91
21-154
sec-Butylbenzene
ug/kg
ND
22.4
21.4
96
19-159
Styrene
ug/kg
ND
22.4
20.3
91
15-152
tert-Butyl benzene
ug/kg
ND
22.4
18.4
82
31-141
Tetrachloroethene
ug/kg
ND
22.4
20.3
90
19-141
Toluene
ug/kg
14.2
22.4
30.0
70
31-146
trans-1,2-Dichloroethene
ug/kg
ND
22.4
22.0
98
28-157
trans- 1,3-Dichloropropene
ug/kg
ND
22.4
20.3
91
25-146
Trichloroethene
ug/kg
ND
22.4
21.4
95
34-149
Trichlorofluoromethane
ug/kg
ND
22.4
24.2
108
10-167
Vinyl acetate
ug/kg
ND
44.9
29.2J
65
10-200
Vinyl chloride
ug/kg
ND
22.4
23.4
104
36-155
Xylene (Total)
ug/kg
ND
67.3
72.8
108
29-148
1,2-Dichloroethane-d4 (S)
%
104
70-132
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8(S)
%
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 46

aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
SAMPLE DUPLICATE: 2687238
Parameter
Units
92445872001
Result
Dup
Result
1,1,1,2-Tetrachloroethane
ug/kg
ND
ND
1,1,1-Trichloroethane
ug/kg
ND
ND
1,1,2,2-Tetrachloroethane
ug/kg
ND
ND
1,1,2-Trichloroethane
ug/kg
ND
ND
1,1-Dichloroethane
ug/kg
ND
ND
1,1-Dichloroethene
ug/kg
ND
ND
1,1-Dichloropropene
ug/kg
ND
ND
1,2,3-Trichlorobenzene
ug/kg
ND
ND
1,2,3-Trichloropropane
ug/kg
ND
ND
1,2,4-Trichlorobenzene
ug/kg
ND
ND
1,2,4-Trimethylbenzene
ug/kg
ND
2.6J
1,2-Dibromo-3-chloropropane
ug/kg
ND
ND
1,2-Dibromoethane (EDB)
ug/kg
ND
ND
1,2-Dichlorobenzene
ug/kg
ND
ND
1,2-Dichloroethane
ug/kg
ND
ND
1,2-Dichloropropane
ug/kg
ND
ND
1,3,5-Trimethylbenzene
ug/kg
ND
ND
1,3-Dichlorobenzene
ug/kg
ND
ND
1,3-Dichloropropane
ug/kg
ND
ND
1,4-Dichlorobenzene
ug/kg
ND
ND
2,2-Dichloropropane
ug/kg
ND
ND
2-Butanone (MEK)
ug/kg
ND
ND
2-Chlorotoluene
ug/kg
ND
ND
2-Hexanone
ug/kg
ND
ND
4-Chlorotoluene
ug/kg
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/kg
ND
ND
Acetone
ug/kg
ND
ND
Benzene
ug/kg
ND
ND
Bromobenzene
ug/kg
ND
ND
Bromochloromethane
ug/kg
ND
ND
Bromodichloromethane
ug/kg
ND
ND
Bromoform
ug/kg
ND
ND
Bromomethane
ug/kg
ND
ND
Carbon tetrachloride
ug/kg
ND
ND
Chlorobenzene
ug/kg
ND
ND
Chloroethane
ug/kg
ND
ND
Chloroform
ug/kg
ND
ND
Chloromethane
ug/kg
ND
ND
cis-1,2-Dichloroethene
ug/kg
ND
ND
cis-1,3-Dichloropropene
ug/kg
ND
ND
Dibromochloromethane
ug/kg
ND
ND
Dibromomethane
ug/kg
ND
ND
Dichlorodifluoromethane
ug/kg
ND
ND
Diisopropyl ether
ug/kg
ND
ND
Ethylbenzene
ug/kg
1.2J
1.6J
Hexachloro-1,3-butadiene
ug/kg
ND
ND
Isopropylbenzene (Cumene)
ug/kg
ND
ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
SAMPLE DUPLICATE: 2687238
Parameter
Units
92445872001
Result
Dup
Result
m&p-Xylene
ug/kg
3.9J
7.5J
Methyl-tert-butyl ether
ug/kg
ND
ND
Methylene Chloride
ug/kg
ND
ND
n-Butylbenzene
ug/kg
ND
ND
n-Propylbenzene
ug/kg
ND
ND
Naphthalene
ug/kg
ND
ND
o-Xylene
ug/kg
1.6J
2.5J
p-Isopropyltoluene
ug/kg
ND
ND
sec-Butylbenzene
ug/kg
ND
ND
Styrene
ug/kg
ND
ND
tert-Butyl benzene
ug/kg
ND
ND
Tetrachloroethene
ug/kg
ND
ND
Toluene
ug/kg
6.0
9.5
trans-1,2-Dichloroethene
ug/kg
ND
ND
trans- 1,3-Dichloropropene
ug/kg
ND
ND
Trichloroethene
ug/kg
ND
ND
Trichlorofluoromethane
ug/kg
ND
ND
Vinyl acetate
ug/kg
ND
ND
Vinyl chloride
ug/kg
ND
ND
Xylene (Total)
ug/kg
ND
ND
1,2-Dichloroethane-d4 (S)
%
95
95
4-Bromofluorobenzene (S)
%
101
103
Toluene-d8 (S)
%
108
106
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC.
Page 25 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
QC Batch: 499269 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level
Associated Lab Samples: 92445717004, 92445717005
METHOD BLANK: 2686854
Associated Lab Samples: 92445717004, 92445717005
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
09/23/19 13:53
1,1,1-Trichloroethane
ug/L
ND
1.0
09/23/19 13:53
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
09/23/19 13:53
1,1,2-Trichloroethane
ug/L
ND
1.0
09/23/19 13:53
1,1-Dichloroethane
ug/L
ND
1.0
09/23/19 13:53
1,1-Dichloroethene
ug/L
ND
1.0
09/23/19 13:53
1,1-Dichloropropene
ug/L
ND
1.0
09/23/19 13:53
1,2,3-Trichlorobenzene
ug/L
ND
1.0
09/23/19 13:53
1,2,3-Trichloropropane
ug/L
ND
1.0
09/23/19 13:53
1,2,4-Trichlorobenzene
ug/L
ND
1.0
09/23/19 13:53
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
09/23/19 13:53
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
09/23/19 13:53
1,2-Dichlorobenzene
ug/L
ND
1.0
09/23/19 13:53
1,2-Dichloroethane
ug/L
ND
1.0
09/23/19 13:53
1,2-Dichloropropane
ug/L
ND
1.0
09/23/19 13:53
1,3-Dichlorobenzene
ug/L
ND
1.0
09/23/19 13:53
1,3-Dichloropropane
ug/L
ND
1.0
09/23/19 13:53
1,4-Dichlorobenzene
ug/L
ND
1.0
09/23/19 13:53
2,2-Dichloropropane
ug/L
ND
1.0
09/23/19 13:53
2-Butanone (MEK)
ug/L
ND
5.0
09/23/19 13:53
2-Chlorotoluene
ug/L
ND
1.0
09/23/19 13:53
2-Hexanone
ug/L
ND
5.0
09/23/19 13:53
4-Chlorotoluene
ug/L
ND
1.0
09/23/19 13:53
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
09/23/19 13:53
Acetone
ug/L
ND
25.0
09/23/19 13:53
Benzene
ug/L
ND
1.0
09/23/19 13:53
Bromobenzene
ug/L
ND
1.0
09/23/19 13:53
Bromochloromethane
ug/L
ND
1.0
09/23/19 13:53
Bromodichloromethane
ug/L
ND
1.0
09/23/19 13:53
Bromoform
ug/L
ND
1.0
09/23/19 13:53
Bromomethane
ug/L
ND
2.0
09/23/19 13:53
Carbon tetrachloride
ug/L
ND
1.0
09/23/19 13:53
Chlorobenzene
ug/L
ND
1.0
09/23/19 13:53
Chloroethane
ug/L
ND
1.0
09/23/19 13:53
Chloroform
ug/L
ND
5.0
09/23/19 13:53
Chloromethane
ug/L
ND
1.0
09/23/19 13:53
cis-1,2-Dichloroethene
ug/L
ND
1.0
09/23/19 13:53
cis-1,3-Dichloropropene
ug/L
ND
1.0
09/23/19 13:53
Dibromochloromethane
ug/L
ND
1.0
09/23/19 13:53
Dibromomethane
ug/L
ND
1.0
09/23/19 13:53
Dichlorodifluoromethane
ug/L
ND
1.0
09/23/19 13:53
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
METHOD BLANK: 2686854
Associated Lab Samples: 92445717004, 92445717005
Parameter Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Diisopropyl ether
ug/L
ND
1.0
09/23/19 13:53
Ethylbenzene
ug/L
ND
1.0
09/23/19 13:53
Hexachloro-1,3-butadiene
ug/L
ND
1.0
09/23/19 13:53
m&p-Xylene
ug/L
ND
2.0
09/23/19 13:53
Methyl-tert-butyl ether
ug/L
ND
1.0
09/23/19 13:53
Methylene Chloride
ug/L
ND
5.0
09/23/19 13:53
Naphthalene
ug/L
ND
1.0
09/23/19 13:53
o-Xylene
ug/L
ND
1.0
09/23/19 13:53
p-Isopropyltoluene
ug/L
ND
1.0
09/23/19 13:53
Styrene
ug/L
ND
1.0
09/23/19 13:53
Tetrachloroethene
ug/L
ND
1.0
09/23/19 13:53
Toluene
ug/L
ND
1.0
09/23/19 13:53
trans-1,2-Dichloroethene
ug/L
ND
1.0
09/23/19 13:53
trans- 1,3-Dichloropropene
ug/L
ND
1.0
09/23/19 13:53
Trichloroethene
ug/L
ND
1.0
09/23/19 13:53
Trichlorofluoromethane
ug/L
ND
1.0
09/23/19 13:53
Vinyl acetate
ug/L
ND
2.0
09/23/19 13:53
Vinyl chloride
ug/L
ND
1.0
09/23/19 13:53
Xylene (Total)
ug/L
ND
1.0
09/23/19 13:53
1,2-Dichloroethane-d4 (S)
%
87
70-130
09/23/19 13:53
4-Bromofluorobenzene (S)
%
108
70-130
09/23/19 13:53
Toluene-d8 (S)
%
111
70-130
09/23/19 13:53
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2686855
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
48.4
97
70-130
1,1,1-Trichloroethane
ug/L
50
49.6
99
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
46.7
93
70-130
1,1,2-Trichloroethane
ug/L
50
48.0
96
70-130
1,1-Dichloroethane
ug/L
50
50.1
100
70-130
1,1-Dichloroethene
ug/L
50
49.7
99
70-130
1,1-Dichloropropene
ug/L
50
51.8
104
70-130
1,2,3-Trichlorobenzene
ug/L
50
47.2
94
70-130
1,2,3-Trichloropropane
ug/L
50
50.0
100
70-130
1,2,4-Trichlorobenzene
ug/L
50
45.7
91
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
46.9
94
70-130
1,2-Dibromoethane (EDB)
ug/L
50
48.0
96
70-130
1,2-Dichlorobenzene
ug/L
50
45.0
90
70-130
1,2-Dichloroethane
ug/L
50
48.7
97
70-130
1,2-Dichloropropane
ug/L
50
50.3
101
70-130
1,3-Dichlorobenzene
ug/L
50
45.6
91
70-130
1,3-Dichloropropane
ug/L
50
49.6
99
70-131
1,4-Dichlorobenzene
ug/L
50
44.9
90
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
LABORATORY CONTROL SAMPLE:
Parameter
2686855
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,2-Dichloropropane
ug/L
50
54.7
109
69-130
2-Butanone (MEK)
ug/L
100
99.6
100
64-135
2-Chlorotoluene
ug/L
50
45.8
92
70-130
2-Hexanone
ug/L
100
83.7
84
66-135
4-Chlorotoluene
ug/L
50
45.5
91
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
86.3
86
70-130
Acetone
ug/L
100
104
104
61-157
Benzene
ug/L
50
48.9
98
70-130
Bromobenzene
ug/L
50
44.7
89
70-130
Bromochloromethane
ug/L
50
47.9
96
70-130
Bromodichloromethane
ug/L
50
50.0
100
70-130
Bromoform
ug/L
50
48.0
96
70-130
Bromomethane
ug/L
50
44.6
89
38-130
Carbon tetrachloride
ug/L
50
48.3
97
70-130
Chlorobenzene
ug/L
50
45.2
90
70-130
Chloroethane
ug/L
50
43.4
87
37-142
Chloroform
ug/L
50
48.5
97
70-130
Chloromethane
ug/L
50
45.8
92
48-130
cis-1,2-Dichloroethene
ug/L
50
49.2
98
70-130
cis-1,3-Dichloropropene
ug/L
50
54.6
109
70-130
Dibromochloromethane
ug/L
50
48.1
96
70-130
Dibromomethane
ug/L
50
47.7
95
70-130
Dichlorodifluoromethane
ug/L
50
50.2
100
53-134
Diisopropyl ether
ug/L
50
50.1
100
70-135
Ethylbenzene
ug/L
50
46.0
92
70-130
Hexachloro-1,3-butadiene
ug/L
50
45.6
91
68-132
m&p-Xylene
ug/L
100
111
111
70-130
Methyl-tert-butyl ether
ug/L
50
54.2
108
70-130
Methylene Chloride
ug/L
50
49.5
99
67-132
Naphthalene
ug/L
50
46.6
93
70-130
o-Xylene
ug/L
50
47.3
95
70-131
p-Isopropyltoluene
ug/L
50
47.2
94
70-130
Styrene
ug/L
50
46.2
92
70-130
Tetrachloroethene
ug/L
50
45.9
92
69-130
Toluene
ug/L
50
44.8
90
70-130
trans-1,2-Dichloroethene
ug/L
50
50.8
102
70-130
trans- 1,3-Dichloropropene
ug/L
50
51.9
104
70-130
Trichloroethene
ug/L
50
48.7
97
70-130
Trichlorofluoromethane
ug/L
50
48.3
97
63-130
Vinyl acetate
ug/L
100
104
104
55-143
Vinyl chloride
ug/L
50
48.7
97
70-131
Xylene (Total)
ug/L
150
159
106
70-130
1,2-Dichloroethane-d4 (S)
%
106
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8 (S)
%
99
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
MATRIX SPIKE SAMPLE:
2686857
92446007001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
20
19.1
96
73-134
1,1,1-Trichloroethane
ug/L
ND
20
20.8
104
82-143
1,1,2,2-Tetrachloroethane
ug/L
ND
20
19.9
99
70-136
1,1,2-Trichloroethane
ug/L
ND
20
19.6
98
70-135
1,1-Dichloroethane
ug/L
ND
20
21.1
106
70-139
1,1-Dichloroethene
ug/L
ND
20
21.0
105
70-154
1,1-Dichloropropene
ug/L
ND
20
21.3
107
70-149
1,2,3-Trichlorobenzene
ug/L
ND
20
19.6
98
70-135
1,2,3-Trichloropropane
ug/L
ND
20
19.9
100
71-137
1,2,4-Trichlorobenzene
ug/L
ND
20
18.4
92
73-140
1,2-Dibromo-3-chloropropane
ug/L
ND
20
18.5
93
65-134
1,2-Dibromoethane (EDB)
ug/L
ND
20
19.2
96
70-137
1,2-Dichlorobenzene
ug/L
ND
20
18.9
95
70-133
1,2-Dichloroethane
ug/L
ND
20
20.3
101
70-137
1,2-Dichloropropane
ug/L
ND
20
20.8
104
70-140
1,3-Dichlorobenzene
ug/L
ND
20
19.3
97
70-135
1,3-Dichloropropane
ug/L
ND
20
20.2
101
70-143
1,4-Dichlorobenzene
ug/L
ND
20
19.2
96
70-133
2,2-Dichloropropane
ug/L
ND
20
22.0
110
61-148
2-Butanone (MEK)
ug/L
ND
40
41.1
97
60-139
2-Chlorotoluene
ug/L
ND
20
19.5
98
70-144
2-Hexanone
ug/L
ND
40
36.0
90
65-138
4-Chlorotoluene
ug/L
ND
20
19.7
99
70-137
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
37.2
93
65-135
Acetone
ug/L
ND
40
47.7
119
60-148
Benzene
ug/L
50.2
20
73.4
116
70-151
Bromobenzene
ug/L
ND
20
19.4
97
70-136
Bromochloromethane
ug/L
ND
20
20.4
102
70-141
Bromodichloromethane
ug/L
ND
20
20.9
105
70-138
Bromoform
ug/L
ND
20
18.5
93
63-130
Bromomethane
ug/L
ND
20
20.4
102
15-152
Carbon tetrachloride
ug/L
ND
20
20.6
103
70-143
Chlorobenzene
ug/L
ND
20
19.3
97
70-138
Chloroethane
ug/L
ND
20
20.1
101
52-163
Chloroform
ug/L
ND
20
19.9
100
70-139
Chloromethane
ug/L
ND
20
18.9
95
41-139
cis-1,2-Dichloroethene
ug/L
ND
20
20.3
102
70-141
cis-1,3-Dichloropropene
ug/L
ND
20
22.0
110
70-137
Dibromochloromethane
ug/L
ND
20
19.2
96
70-134
Dibromomethane
ug/L
ND
20
20.1
101
70-138
Dichlorodifluoromethane
ug/L
ND
20
21.5
108
47-155
Diisopropyl ether
ug/L
ND
20
19.3
96
63-144
Ethylbenzene
ug/L
6.9
20
27.4
102
66-153
Hexachloro-1,3-butadiene
ug/L
ND
20
18.3
91
65-149
m&p-Xylene
ug/L
26.1
40
77.0
127
69-152
Methyl-tert-butyl ether
ug/L
ND
20
19.9
100
54-156
Methylene Chloride
ug/L
ND
20
19.5
97
42-159
Results presented on
this page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
MATRIX SPIKE SAMPLE:
Parameter
2686857
Units
92446007001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Naphthalene
ug/L
7.2
20
27.3
100
61-148
o-Xylene
ug/L
71.2
20
91.3
100
70-148
p-Isopropyltoluene
ug/L
ND
20
20.2
101
70-146
Styrene
ug/L
ND
20
19.8
99
70-135
Tetrachloroethene
ug/L
ND
20
19.6
98
59-143
Toluene
ug/L
14.5
20
34.6
100
59-148
trans-1,2-Dichloroethene
ug/L
ND
20
20.9
105
70-146
trans- 1,3-Dichloropropene
ug/L
ND
20
20.8
104
70-135
Trichloroethene
ug/L
ND
20
20.8
104
70-147
Trichlorofluoromethane
ug/L
ND
20
21.1
106
70-148
Vinyl acetate
ug/L
ND
40
36.8
92
49-151
Vinyl chloride
ug/L
ND
20
21.1
106
70-156
Xylene (Total)
ug/L
97.3
60
168
118
63-158
1,2-Dichloroethane-d4 (S)
%
111
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene-d8(S)
%
102
70-130
SAMPLE DUPLICATE: 2686856
Parameter
Units
92445029001
Result
Dup
Result RPD Qualifiers
1,1,1,2-Tetrachloroethane
ug/L
ND
ND
1,1,1-Trichloroethane
ug/L
ND
ND
1,1,2,2-Tetrachloroethane
ug/L
ND
ND
1,1,2-Trichloroethane
ug/L
ND
ND
1,1-Dichloroethane
ug/L
ND
ND
1,1-Dichloroethene
ug/L
ND
ND
1,1-Dichloropropene
ug/L
ND
ND
1,2,3-Trichlorobenzene
ug/L
ND
ND
1,2,3-Trichloropropane
ug/L
ND
ND
1,2,4-Trichlorobenzene
ug/L
ND
ND
1,2-Dibromo-3-chloropropane
ug/L
ND
ND
1,2-Dibromoethane (EDB)
ug/L
ND
ND
1,2-Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
1,3-Dichlorobenzene
ug/L
ND
ND
1,3-Dichloropropane
ug/L
ND
ND
1,4-Dichlorobenzene
ug/L
ND
ND
2,2-Dichloropropane
ug/L
ND
ND
2-Butanone (MEK)
ug/L
ND
3AJ
2-Chlorotoluene
ug/L
ND
ND
2-Hexanone
ug/L
ND
ND
4-Chlorotoluene
ug/L
ND
ND
4-Methyl-2-pentanone (MIBK)
ug/L
ND
ND
Acetone
ug/L
89.8
35.6 86 D6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC.
Page 30 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
SAMPLE DUPLICATE: 2686856
Parameter
Units
92445029001
Result
Benzene
ug/L
ND
Bromobenzene
ug/L
ND
Bromochloromethane
ug/L
ND
Bromodichloromethane
ug/L
2.0
Bromoform
ug/L
ND
Bromomethane
ug/L
ND
Carbon tetrachloride
ug/L
ND
Chlorobenzene
ug/L
ND
Chloroethane
ug/L
ND
Chloroform
ug/L
11.0
Chloromethane
ug/L
ND
cis-1,2-Dichloroethene
ug/L
ND
cis-1,3-Dichloropropene
ug/L
ND
Dibromochloromethane
ug/L
ND
Dibromomethane
ug/L
ND
Dichlorodifluoromethane
ug/L
ND
Diisopropyl ether
ug/L
ND
Ethylbenzene
ug/L
ND
Hexachloro-1,3-butadiene
ug/L
ND
m&p-Xylene
ug/L
ND
Methyl-tert-butyl ether
ug/L
ND
Methylene Chloride
ug/L
ND
Naphthalene
ug/L
ND
o-Xylene
ug/L
ND
p-Isopropyltoluene
ug/L
ND
Styrene
ug/L
ND
Tetrachloroethene
ug/L
ND
Toluene
ug/L
ND
trans-1,2-Dichloroethene
ug/L
ND
trans- 1,3-Dichloropropene
ug/L
ND
Trichloroethene
ug/L
ND
Trichlorofluoromethane
ug/L
ND
Vinyl acetate
ug/L
ND
Vinyl chloride
ug/L
ND
Xylene (Total)
ug/L
ND
1,2-Dichloroethane-d4 (S)
%
85
4-Bromofluorobenzene (S)
%
104
Toluene-d8 (S)
%
111
Dup
Result RPD Qualifiers
ND
ND
ND
1.9
ND
ND
ND
ND
ND
11.0
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
87
109
111
3
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC.
Page 31 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
QC Batch: 499512 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level
Associated Lab Samples: 92445717006
METHOD BLANK: 2687961
Associated Lab Samples: 92445717006
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
09/24/19 13:06
1,1,1-Trichloroethane
ug/L
ND
1.0
09/24/19 13:06
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
09/24/19 13:06
1,1,2-Trichloroethane
ug/L
ND
1.0
09/24/19 13:06
1,1-Dichloroethane
ug/L
ND
1.0
09/24/19 13:06
1,1-Dichloroethene
ug/L
ND
1.0
09/24/19 13:06
1,1-Dichloropropene
ug/L
ND
1.0
09/24/19 13:06
1,2,3-Trichlorobenzene
ug/L
ND
1.0
09/24/19 13:06
1,2,3-Trichloropropane
ug/L
ND
1.0
09/24/19 13:06
1,2,4-Trichlorobenzene
ug/L
ND
1.0
09/24/19 13:06
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
09/24/19 13:06
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
09/24/19 13:06
1,2-Dichlorobenzene
ug/L
ND
1.0
09/24/19 13:06
1,2-Dichloroethane
ug/L
ND
1.0
09/24/19 13:06
1,2-Dichloropropane
ug/L
ND
1.0
09/24/19 13:06
1,3-Dichlorobenzene
ug/L
ND
1.0
09/24/19 13:06
1,3-Dichloropropane
ug/L
ND
1.0
09/24/19 13:06
1,4-Dichlorobenzene
ug/L
ND
1.0
09/24/19 13:06
2,2-Dichloropropane
ug/L
ND
1.0
09/24/19 13:06
2-Butanone (MEK)
ug/L
ND
5.0
09/24/19 13:06
2-Chlorotoluene
ug/L
ND
1.0
09/24/19 13:06
2-Hexanone
ug/L
ND
5.0
09/24/19 13:06
4-Chlorotoluene
ug/L
ND
1.0
09/24/19 13:06
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
09/24/19 13:06
Acetone
ug/L
ND
25.0
09/24/19 13:06
Benzene
ug/L
ND
1.0
09/24/19 13:06
Bromobenzene
ug/L
ND
1.0
09/24/19 13:06
Bromochloromethane
ug/L
ND
1.0
09/24/19 13:06
Bromodichloromethane
ug/L
ND
1.0
09/24/19 13:06
Bromoform
ug/L
ND
1.0
09/24/19 13:06
Bromomethane
ug/L
ND
2.0
09/24/19 13:06 v2
Carbon tetrachloride
ug/L
ND
1.0
09/24/19 13:06
Chlorobenzene
ug/L
ND
1.0
09/24/19 13:06
Chloroethane
ug/L
ND
1.0
09/24/19 13:06
Chloroform
ug/L
ND
5.0
09/24/19 13:06
Chloromethane
ug/L
ND
1.0
09/24/19 13:06
cis-1,2-Dichloroethene
ug/L
ND
1.0
09/24/19 13:06
cis-1,3-Dichloropropene
ug/L
ND
1.0
09/24/19 13:06
Dibromochloromethane
ug/L
ND
1.0
09/24/19 13:06
Dibromomethane
ug/L
ND
1.0
09/24/19 13:06
Dichlorodifluoromethane
ug/L
ND
1.0
09/24/19 13:06
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
METHOD BLANK: 2687961
Associated Lab Samples: 92445717006
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Diisopropyl ether
ug/L
ND
1.0
09/24/19 13:06
Ethylbenzene
ug/L
ND
1.0
09/24/19 13:06
Hexachloro-1,3-butadiene
ug/L
ND
1.0
09/24/19 13:06
m&p-Xylene
ug/L
ND
2.0
09/24/19 13:06
Methyl-tert-butyl ether
ug/L
ND
1.0
09/24/19 13:06
Methylene Chloride
ug/L
ND
5.0
09/24/19 13:06
Naphthalene
ug/L
ND
1.0
09/24/19 13:06
o-Xylene
ug/L
ND
1.0
09/24/19 13:06
p-Isopropyltoluene
ug/L
ND
1.0
09/24/19 13:06
Styrene
ug/L
ND
1.0
09/24/19 13:06
Tetrachloroethene
ug/L
ND
1.0
09/24/19 13:06
Toluene
ug/L
ND
1.0
09/24/19 13:06
trans-1,2-Dichloroethene
ug/L
ND
1.0
09/24/19 13:06
trans- 1,3-Dichloropropene
ug/L
ND
1.0
09/24/19 13:06
Trichloroethene
ug/L
ND
1.0
09/24/19 13:06
Trichlorofluoromethane
ug/L
ND
1.0
09/24/19 13:06
Vinyl acetate
ug/L
ND
2.0
09/24/19 13:06
Vinyl chloride
ug/L
ND
1.0
09/24/19 13:06
Xylene (Total)
ug/L
ND
1.0
09/24/19 13:06
1,2-Dichloroethane-d4 (S)
%
85
70-130
09/24/19 13:06
4-Bromofluorobenzene (S)
%
108
70-130
09/24/19 13:06
Toluene-d8 (S)
%
111
70-130
09/24/19 13:06
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2687962
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
47.9
96
70-130
1,1,1-Trichloroethane
ug/L
50
49.0
98
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
49.2
98
70-130
1,1,2-Trichloroethane
ug/L
50
49.3
99
70-130
1,1-Dichloroethane
ug/L
50
50.5
101
70-130
1,1-Dichloroethene
ug/L
50
50.0
100
70-130
1,1-Dichloropropene
ug/L
50
51.3
103
70-130
1,2,3-Trichlorobenzene
ug/L
50
48.5
97
70-130
1,2,3-Trichloropropane
ug/L
50
39.0
78
70-130
1,2,4-Trichlorobenzene
ug/L
50
47.6
95
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
48.0
96
70-130
1,2-Dibromoethane (EDB)
ug/L
50
49.3
99
70-130
1,2-Dichlorobenzene
ug/L
50
46.2
92
70-130
1,2-Dichloroethane
ug/L
50
49.3
99
70-130
1,2-Dichloropropane
ug/L
50
51.6
103
70-130
1,3-Dichlorobenzene
ug/L
50
46.1
92
70-130
1,3-Dichloropropane
ug/L
50
51.8
104
70-131
1,4-Dichlorobenzene
ug/L
50
46.4
93
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: J19-5100
Pace Project No.: 92445717
LABORATORY CONTROL SAMPLE: 2687962
Parameter
QUALITY CONTROL DATA
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
2,2-Dichloropropane
ug/L
50
53.2
106
69-130
2-Butanone (MEK)
ug/L
100
108
108
64-135
2-Chlorotoluene
ug/L
50
47.4
95
70-130
2-Hexanone
ug/L
100
93.8
94
66-135
4-Chlorotoluene
ug/L
50
47.3
95
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
92.8
93
70-130
Acetone
ug/L
100
118
118
61-157
Benzene
ug/L
50
50.3
101
70-130
Bromobenzene
ug/L
50
47.0
94
70-130
Bromochloromethane
ug/L
50
50.3
101
70-130lK
Bromodichloromethane
ug/L
50
50.2
100
70-130
Bromoform
ug/L
50
47.6
95
70-130
Bromomethane
ug/L
50
36.5
73
38-1301K,v3
Carbon tetrachloride
ug/L
50
47.5
95
70-130
Chlorobenzene
ug/L
50
46.3
93
70-130
Chloroethane
ug/L
50
45.1
90
37-142 IK
Chloroform
ug/L
50
47.7
95
70-130
Chloromethane
ug/L
50
46.8
94
48-130
cis-1,2-Dichloroethene
ug/L
50
49.7
99
70-130
cis-1,3-Dichloropropene
ug/L
50
54.6
109
70-130
Dibromochloromethane
ug/L
50
48.8
98
70-130
Dibromomethane
ug/L
50
47.7
95
70-130
Dichlorodifluoromethane
ug/L
50
50.5
101
53-134
Diisopropyl ether
ug/L
50
52.2
104
70-135
Ethylbenzene
ug/L
50
46.7
93
70-130
Hexachloro-1,3-butadiene
ug/L
50
47.9
96
68-132
m&p-Xylene
ug/L
100
94.2
94
70-130
Methyl-tert-butyl ether
ug/L
50
54.3
109
70-130
Methylene Chloride
ug/L
50
47.3
95
67-132
Naphthalene
ug/L
50
49.4
99
70-130
o-Xylene
ug/L
50
47.3
95
70-131
p-Isopropyltoluene
ug/L
50
48.8
98
70-130
Styrene
ug/L
50
47.0
94
70-130
Tetrachloroethene
ug/L
50
46.3
93
69-130
Toluene
ug/L
50
45.6
91
70-130
trans-1,2-Dichloroethene
ug/L
50
51.0
102
70-130
trans- 1,3-Dichloropropene
ug/L
50
52.2
104
70-130
Trichloroethene
ug/L
50
50.3
101
70-130
Trichlorofluoromethane
ug/L
50
48.0
96
63-130
Vinyl acetate
ug/L
100
109
109
55-143
Vinyl chloride
ug/L
50
50.0
100
70-131
Xylene (Total)
ug/L
150
142
94
70-130
1,2-Dichloroethane-d4 (S)
%
104
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene-d8 (S)
%
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2687963
2687964
MS
MSD
92446205022
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
15.5
16.1
77
80
73-134
4
1,1,1-Trichloroethane
ug/L
ND
20
20
16.8
17.1
84
85
82-143
2
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
16.1
16.8
80
84
70-136
5
1,1,2-Trichloroethane
ug/L
ND
20
20
15.9
16.6
80
83
70-135
4
1,1-Dichloroethane
ug/L
ND
20
20
18.7
18.7
94
93
70-139
0
1,1-Dichloroethene
ug/L
ND
20
20
19.4
19.5
97
98
70-154
1
1,1-Dichloropropene
ug/L
ND
20
20
16.2
16.3
81
82
70-149
1
1,2,3-Trichlorobenzene
ug/L
ND
20
20
16.2
16.3
81
81
70-135
1
1,2,3-Trichloropropane
ug/L
ND
20
20
16.4
12.9
82
65
71-137
24 M1
1,2,4-Trichlorobenzene
ug/L
ND
20
20
16.2
16.1
81
80
73-140
1
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
14.9
15.6
74
78
65-134
5
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
15.3
16.4
77
82
70-137
7
1,2-Dichlorobenzene
ug/L
ND
20
20
16.6
16.2
83
81
70-133
2
1,2-Dichloroethane
ug/L
ND
20
20
16.6
16.6
83
83
70-137
0
1,2-Dichloropropane
ug/L
ND
20
20
17.3
17.8
87
89
70-140
3
1,3-Dichlorobenzene
ug/L
ND
20
20
17.1
16.6
85
83
70-135
3
1,3-Dichloropropane
ug/L
ND
20
20
15.9
16.5
80
82
70-143
4
1,4-Dichlorobenzene
ug/L
ND
20
20
16.5
16.4
83
82
70-133
1
2,2-Dichloropropane
ug/L
ND
20
20
18.4
18.6
92
93
61-148
1
2-Butanone (MEK)
ug/L
ND
40
40
29.2
31.1
73
78
60-139
6
2-Chlorotoluene
ug/L
ND
20
20
17.2
17.1
86
85
70-144
1
2-Hexanone
ug/L
ND
40
40
29.8
31.5
74
79
65-138
6
4-Chlorotoluene
ug/L
ND
20
20
17.3
17.1
87
85
70-137
2
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
30.3
31.7
76
79
65-135
5
Acetone
ug/L
ND
40
40
36.2
39.3
91
98
60-148
8
Benzene
ug/L
ND
20
20
17.7
17.7
88
88
70-151
0
Bromobenzene
ug/L
ND
20
20
16.6
16.4
83
82
70-136
1
Bromochloromethane
ug/L
ND
20
20
18.5
18.6
93
93
70-141
0
Bromodichloromethane
ug/L
0.52J
20
20
17.5
18.0
85
88
70-138
3
Bromoform
ug/L
ND
20
20
14.5
15.6
72
78
63-130
7
Bromomethane
ug/L
ND
20
20
17.6
16.7
88
83
15-152
5 v3
Carbon tetrachloride
ug/L
ND
20
20
17.0
17.3
85
86
70-143
2
Chlorobenzene
ug/L
ND
20
20
17.0
17.1
85
85
70-138
0
Chloroethane
ug/L
ND
20
20
19.4
19.1
97
95
52-163
2
Chloroform
ug/L
4.7J
20
20
22.5
22.0
89
86
70-139
2
Chloromethane
ug/L
ND
20
20
17.3
17.6
87
88
41-139
1
cis-1,2-Dichloroethene
ug/L
ND
20
20
17.9
18.0
90
90
70-141
0
cis-1,3-Dichloropropene
ug/L
ND
20
20
17.1
17.6
86
88
70-137
3
Dibromochloromethane
ug/L
ND
20
20
14.8
15.5
74
77
70-134
4
Dibromomethane
ug/L
ND
20
20
16.9
17.5
85
87
70-138
3
Dichlorodifluoromethane
ug/L
ND
20
20
18.3
18.0
91
90
47-155
1
Diisopropyl ether
ug/L
ND
20
20
16.1
16.2
81
81
63-144
0
Ethylbenzene
ug/L
ND
20
20
17.2
17.4
86
87
66-153
1
Hexachloro-1,3-butadiene
ug/L
ND
20
20
16.7
16.0
84
80
65-149
4
m&p-Xylene
ug/L
ND
40
40
35.9
36.9
90
92
69-152
3
Methyl-tert-butyl ether
ug/L
ND
20
20
14.9
15.4
75
77
54-156
3
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2687963
2687964
MS
MSD
92446205022
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Methylene Chloride
ug/L
ND
20
20
17.7
17.6
89
88
42-159
1
Naphthalene
ug/L
ND
20
20
16.5
16.3
82
82
61-148
1
o-Xylene
ug/L
ND
20
20
17.5
18.0
87
90
70-148
3
p-Isopropyltoluene
ug/L
ND
20
20
17.9
17.5
90
87
70-146
3
Styrene
ug/L
ND
20
20
17.3
17.9
87
90
70-135
4
Tetrachloroethene
ug/L
ND
20
20
16.1
16.3
81
81
59-143
1
Toluene
ug/L
ND
20
20
17.5
17.8
87
89
59-148
2
trans-1,2-Dichloroethene
ug/L
ND
20
20
18.6
18.5
93
92
70-146
0
trans- 1,3-Dichloropropene
ug/L
ND
20
20
16.4
17.3
82
87
70-135
5
Trichloroethene
ug/L
ND
20
20
16.6
16.8
83
84
70-147
1
Trichlorofluoromethane
ug/L
ND
20
20
18.3
18.3
91
91
70-148
0
Vinyl acetate
ug/L
ND
40
40
28.1
28.6
70
72
49-151
2
Vinyl chloride
ug/L
ND
20
20
19.2
19.1
96
95
70-156
1
Xylene (Total)
ug/L
ND
60
60
53.4
54.9
89
92
63-158
3
1,2-Dichloroethane-d4 (S)
%
101
104
70-130
4-Bromofluorobenzene (S)
%
102
105
70-130
Toluene-d8(S)
%
104
104
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
QC Batch: 498453 Analysis Method: EPA 8270E
QC Batch Method: EPA 3546 Analysis Description: 8270E MSSV PAH by SIM
Associated Lab Samples: 92445717001, 92445717002, 92445717003
METHOD BLANK: 2683257 Matrix:
Associated Lab Samples: 92445717001, 92445717002, 92445717003
Blank
Parameter Units Result
Solid
Reporting
Limit
Analyzed
1-Methylnaphthalene
ug/kg
ND
9.9
09/19/19 08:49
2-Methylnaphthalene
ug/kg
ND
9.9
09/19/19 08:49
Acenaphthene
ug/kg
ND
9.9
09/19/19 08:49
Acenaphthylene
ug/kg
ND
9.9
09/19/19 08:49
Anthracene
ug/kg
ND
9.9
09/19/19 08:49
Benzo(a)anthracene
ug/kg
ND
9.9
09/19/19 08:49
Benzo(a)pyrene
ug/kg
ND
9.9
09/19/19 08:49
Benzo(b)fluoranthene
ug/kg
ND
9.9
09/19/19 08:49
Benzo(g,h,i)perylene
ug/kg
ND
9.9
09/19/19 08:49
Benzo(k)fluoranthene
ug/kg
ND
9.9
09/19/19 08:49
Chrysene
ug/kg
ND
9.9
09/19/19 08:49
Dibenz(a,h)anthracene
ug/kg
ND
9.9
09/19/19 08:49
Fluoranthene
ug/kg
ND
9.9
09/19/19 08:49
Fluorene
ug/kg
ND
9.9
09/19/19 08:49
Indeno(1,2,3-cd)pyrene
ug/kg
ND
9.9
09/19/19 08:49
Naphthalene
ug/kg
ND
9.9
09/19/19 08:49
Phenanthrene
ug/kg
ND
9.9
09/19/19 08:49
Pyrene
ug/kg
ND
9.9
09/19/19 08:49
2-Fluorobiphenyl (S)
%
77
10-110
09/19/19 08:49
Nitrobenzene-d5 (S)
%
73
10-128
09/19/19 08:49
Terphenyl-d14 (S)
%
84
39-119
09/19/19 08:49
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2683258
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1-Methylnaphthalene
ug/kg
33.2
29.2
88
44-130
2-Methylnaphthalene
ug/kg
33.2
30.9
93
41-134
Acenaphthene
ug/kg
33.2
29.2
88
52-123
Acenaphthylene
ug/kg
33.2
27.8
84
49-116
Anthracene
ug/kg
33.2
29.6
89
41-133
Benzo(a)anthracene
ug/kg
33.2
29.7
89
56-130
Benzo(a)pyrene
ug/kg
33.2
25.5
77
51-136
Benzo(b)fluoranthene
ug/kg
33.2
30.3
91
37-149
Benzo(g,h,i)perylene
ug/kg
33.2
29.5
89
39-127
Benzo(k)fluoranthene
ug/kg
33.2
31.1
94
45-139
Chrysene
ug/kg
33.2
29.7
89
59-127
Dibenz(a,h)anthracene
ug/kg
33.2
29.8
90
37-139
Fluoranthene
ug/kg
33.2
30.1
91
53-132
Fluorene
ug/kg
33.2
28.8
87
45-127
Indeno(1,2,3-cd)pyrene
ug/kg
33.2
29.7
89
35-145
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 37 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
LABORATORY CONTROL SAMPLE:
2683258
Spike
LCS LCS
% Rec
Parameter
Units
Conc.
Result % Rec
Limits
Naphthalene
ug/kg
33.2
27.8 84
45-123
Phenanthrene
ug/kg
33.2
29.7 90
50-125
Pyrene
ug/kg
33.2
30.6 92
52-132
2-Fluorobiphenyl (S)
%
84
10-110
Nitrobenzene-d5 (S)
%
79
10-128
Terphenyl-d14 (S)
%
85
39-119
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2683259
MS
92445548004 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
2683260
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1-Methylnaphthalene
ug/kg
0.0043J
45.5
45.3
40.8
37.9
80
74
50-150
7
mg/kg
2-Methylnaphthalene
ug/kg
0.0079J
45.5
45.3
50.6
46.6
94
86
50-150
8
mg/kg
Acenaphthene
ug/kg
0.014
45.5
45.3
65.8
56.7
114
94
50-150
15
mg/kg
Acenaphthylene
ug/kg
0.00191
45.5
45.3
39.0
34.5
82
72
50-150
12
mg/kg
Anthracene
ug/kg
0.048
45.5
45.3
131
123
183
166
50-150
6 M1
mg/kg
Benzo(a)anthracene
ug/kg
0.054
45.5
45.3
166
143
247
198
50-150
15 M1
mg/kg
Benzo(a)pyrene
ug/kg
0.035
45.5
45.3
122
112
191
171
50-150
8 M1
mg/kg
Benzo(b)fluoranthene
ug/kg
0.048
45.5
45.3
160
146
246
218
50-150
9 M1
mg/kg
Benzo(g,h,i)perylene
ug/kg
0.022
45.5
45.3
81.4
72.5
131
112
50-150
12
mg/kg
Benzo(k)fluoranthene
ug/kg
0.025
45.5
45.3
77.4
72.4
116
106
50-150
7
mg/kg
Chrysene
ug/kg
0.043
45.5
45.3
144
122
222
176
50-150
16 M1
mg/kg
Dibenz(a,h)anthracene
ug/kg
0.0057J
45.5
45.3
44.8
41.9
86
80
50-150
7
mg/kg
Fluoranthene
ug/kg
0.12
45.5
45.3
332
277
465
347
50-150
18 M1
mg/kg
Fluorene
ug/kg
0.022
45.5
45.3
96.3
75.9
162
118
50-150
24 M1
mg/kg
Indeno(1,2,3-cd)pyrene
ug/kg
0.019
45.5
45.3
79.6
71.2
134
117
50-150
11
mg/kg
Naphthalene
ug/kg
0.016
45.5
45.3
56.2
62.2
88
102
50-150
10
mg/kg
Phenanthrene
ug/kg
0.16
45.5
45.3
442
361
612
437
50-150
20 M1
mg/kg
Pyrene
ug/kg
0.090
45.5
45.3
247
215
346
277
50-150
14 M1
mg/kg
2-Fluorobiphenyl (S)
%
71
66
10-110
Nitrobenzene-d5(S)
%
65
64
10-128
Terphenyl-d14(S)
%
89
79
39-119
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC.
Page 38 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
QC Batch: 499304 Analysis Method: EPA 8270E by SIM
QC Batch Method: EPA 3511 Analysis Description: 8270E 3511 Low Volume PAH SIM
Associated Lab Samples: 92445717004, 92445717005, 92445717006
METHOD BLANK: 2687123 Matrix:
Associated Lab Samples: 92445717004, 92445717005, 92445717006
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed Qualifiers
1-Methylnaphthalene
ug/L
ND
0.80
09/23/19 16:27
2-Methylnaphthalene
ug/L
ND
0.80
09/23/19 16:27
Acenaphthene
ug/L
ND
0.50
09/23/19 16:27
Acenaphthylene
ug/L
ND
0.50
09/23/19 16:27
Anthracene
ug/L
ND
0.050
09/23/19 16:27
Benzo(a)anthracene
ug/L
ND
0.050
09/23/19 16:27
Benzo(a)pyrene
ug/L
ND
0.10
09/23/19 16:27
Benzo(b)fluoranthene
ug/L
ND
0.050
09/23/19 16:27
Benzo(g,h,i)perylene
ug/L
ND
0.20
09/23/19 16:27
Benzo(k)fluoranthene
ug/L
ND
0.20
09/23/19 16:27
Chrysene
ug/L
ND
0.10
09/23/19 16:27
Dibenz(a,h)anthracene
ug/L
ND
0.15
09/23/19 16:27
Fluoranthene
ug/L
ND
0.30
09/23/19 16:27
Fluorene
ug/L
ND
0.31
09/23/19 16:27
Indeno(1,2,3-cd)pyrene
ug/L
ND
0.050
09/23/19 16:27
Naphthalene
ug/L
ND
1.5
09/23/19 16:27
Phenanthrene
ug/L
ND
0.20
09/23/19 16:27
Pyrene
ug/L
ND
0.10
09/23/19 16:27
2-Fluorobiphenyl (S)
%
99
45-150
09/23/19 16:27
Nitrobenzene-d5 (S)
%
108
57-164
09/23/19 16:27
Terphenyl-d14 (S)
%
111
38-153
09/23/19 16:27
LABORATORY CONTROL SAMPLE:
Parameter
2687124
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1-Methylnaphthalene
ug/L
2.5
3.1
123
47-152
2-Methylnaphthalene
ug/L
2.5
3.4
134
45-155
Acenaphthene
ug/L
2.5
3.2
126
52-160
Acenaphthylene
ug/L
2.5
3.2
129
52-163
Anthracene
ug/L
2.5
3.6
144
57-169
Benzo(a)anthracene
ug/L
2.5
3.5
139
48-164
Benzo(a)pyrene
ug/L
2.5
3.4
138
49-165
Benzo(b)fluoranthene
ug/L
2.5
3.5
141
42-177
Benzo(g,h,i)perylene
ug/L
2.5
3.3
131
35-160
Benzo(k)fluoranthene
ug/L
2.5
3.4
138
39-179
Chrysene
ug/L
2.5
3.6
145
54-166
Dibenz(a,h)anthracene
ug/L
2.5
3.3
134
30-176
Fluoranthene
ug/L
2.5
3.6
144
45-175
Fluorene
ug/L
2.5
3.3
132
53-165
Indeno(1,2,3-cd)pyrene
ug/L
2.5
3.3
133
35-181
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
LABORATORY CONTROL SAMPLE:
2687124
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
Naphthalene
ug/L
2.5
3.2
128
34-174
Phenanthrene
ug/L
2.5
3.5
140
48-166
Pyrene
ug/L
2.5
3.6
146
52-169
2-Fluorobiphenyl (S)
%
110
45-150
Nitrobenzene-d5 (S)
%
123
57-164
Terphenyl-d14 (S)
%
120
38-153
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2687125
2687126
MS
MSD
92432161005
Spike
Spike
MS
MSD
MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec % Rec
Limits
RPD Qual
1-Methylnaphthalene
ug/L
ND
2.5
2.5
3.4
3.0
109
93
70-130
12
2-Methylnaphthalene
ug/L
0.91
2.5
2.5
3.9
3.4
118
100
70-130
12
Acenaphthene
ug/L
2.6
2.5
2.5
5.4
4.9
113
92
70-130
10
Acenaphthylene
ug/L
ND
2.5
2.5
2.9
2.6
115
103
70-130
11
Anthracene
ug/L
ND
2.5
2.5
3.6
3.3
145
132
70-130
9 M1
Benzo(a)anthracene
ug/L
ND
2.5
2.5
3.1
2.8
124
111
70-130
11
Benzo(a)pyrene
ug/L
ND
2.5
2.5
3.0
2.6
118
106
70-130
11
Benzo(b)fluoranthene
ug/L
ND
2.5
2.5
3.0
2.8
119
111
70-130
7
Benzo(g,h,i)perylene
ug/L
ND
2.5
2.5
2.7
2.5
110
101
70-130
9
Benzo(k)fluoranthene
ug/L
ND
2.5
2.5
3.0
2.7
122
108
70-130
12
Chrysene
ug/L
ND
2.5
2.5
3.2
2.9
127
116
70-130
9
Dibenz(a,h)anthracene
ug/L
ND
2.5
2.5
2.8
2.6
111
103
70-130
7
Fluoranthene
ug/L
ND
2.5
2.5
3.4
3.0
128
115
70-130
10
Fluorene
ug/L
1.6
2.5
2.5
4.6
4.2
120
101
70-130
10
Indeno(1,2,3-cd)pyrene
ug/L
ND
2.5
2.5
2.8
2.6
112
103
70-130
9
Naphthalene
ug/L
5.1
2.5
2.5
8.0
7.1
114
77
70-130
12
Phenanthrene
ug/L
2.4
2.5
2.5
5.5
4.9
124
102
70-130
10
Pyrene
ug/L
ND
2.5
2.5
3.3
3.0
132
119
70-130
11 M1
2-Fluorobiphenyl (S)
%
104
92
45-150
Nitrobenzene-d5 (S)
%
109
96
57-164
Terphenyl-d14 (S)
%
112
102
38-153
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC.
Page 40 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: J19-5100
Pace Project No.: 92445717
QC Batch: 498078 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92445717001, 92445717002, 92445717003
SAMPLE DUPLICATE: 2681829
92445594001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 27.5 24.0 14
SAMPLE DUPLICATE: 2681919
92445717003 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 28.0 28.6 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: J19-5100
Pace Project No.: 92445717
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
F3 The recovery of the second source standard used to verify the initial calibration curve for this analyte is outside the
laboratory's control limits. The result is estimated.
IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should
be considered an estimated value.
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
v1 The continuing calibration verification was above the method acceptance limit. Any detection for the analyte in the
associated samples may have a high bias.
v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the
associated samples and the sensitivity of the instrument was verified with a reporting limit check standard.
v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the
associated samples may have low bias.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 46

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
J19-5100
92445717
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92445717001
SB-1 9'
EPA 3546
498453
EPA 8270E
498672
92445717002
SB-1 14'
EPA 3546
498453
EPA 8270E
498672
92445717003
SB-2 14'
EPA 3546
498453
EPA 8270E
498672
92445717004
MWA
EPA 3511
499304
EPA 8270E by SIM
499369
92445717005
MW-2
EPA 3511
499304
EPA 8270E by SIM
499369
92445717006
MW-3
EPA 3511
499304
EPA 8270E by SIM
499369
92445717001
SB-1 9'
EPA 5035A
499141
EPA 8260D
499149
92445717002
SB-1 14'
EPA 5035A
499141
EPA 8260D
499149
92445717003
SB-2 14'
EPA 5035A
499141
EPA 8260D
499149
92445717004
MWA
EPA 8260D
499269
92445717005
MW-2
EPA 8260D
499269
92445717006
MW-3
EPA 8260D
499512
92445717001
SB-1 9'
ASTM D2974-87
498078
92445717002
SB-1 14'
ASTM D2974-87
498078
92445717003
SB-2 14'
ASTM D2974-87
498078
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/24/2019 04:23 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 46

Document Name:
Docurnent Revised: February 7, 2018
r�r m
=ARaIACaf
Sample Condition Upon Receipt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F•CAR•CS-033-Rev.O6
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑
Client dame:
11 'I
Custody Seal Present? []Yes ❑No Seals Intact? ❑Yes
Huntersville ❑ Raleigh[] Mechanicsville[]
WO#:92445717
Project #,
924457f
ONO
Date/initials Person Examining Contents: '
Packing Material: []Bubble Wrap []Bubble Bags []None ❑ Other Biological Tissue Frozen?
Thermometer: [Yes []No❑N/A
❑ IR Gun ID: 92TO49 Type of 1[e: ❑Wet ❑slue ❑None
Tempshould he above freezing to VC
Cooler Temp Corrected (°C): ❑Sarnples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Solt (❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (Check maps)? Did samples criginatefrom a Foreign source (internationally,
FlyPs nNo including Hawaii and Puerto Rico)? nYes nNo
Comments/Discrepancy:
Chain of Custody Present?
[]Yes
❑No
❑N/A
1,
Samples Arrived within Hold Time?
[]Yes
❑Na
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
[-]Yes
ONO
[]N/A
3.
Rush Turn Around Time Requested?
El Yes
❑No
❑N/A
4.
Sufficient Volume?
❑Yes
❑No
❑N/A
S.
Correct Containers Used?
Pace Cortainers Used?
❑Yes
❑Yes
[:]No
❑two
❑N/A
FJN/A
6.
j�antaner�ntact.I
--- ❑les
❑Nb
❑NIA
7, - — ---
Dissolved analysis: Samples Field Filtered?
❑Yes
❑Iwo
❑N/A
8.
Sample Labels Match COC?
-Includes Date/Tirr,e/ID/Analysis Matrix:
❑Yes
❑No
[]NIA
9.
ea space In VOA Vials ,> mm
Yes
Nc
Trip BiankNesent?
Trip 8lankCustody Seals Present?
[]Yes
❑Yes
[-]No
❑No
[]NIA
❑N(A
COMMENTS/SAMPLE DISCREPANCY Field Data Required? Dyes ❑N...
CLIENT NOTIFICATION/RESOLUTION
Person
Project Manager SCURF Review: P m b
v-DProject Manager SRF Review: 1 1 I t r
Lot ID of split containers:
Date: l
Date:
Page 44 of 46

aceAnaly MI-
Document Name:
Sample Condition Upon RecelptjSCURi
Document Revised: February 7, 2018
Page I of 2
Document No,:
issuing Authority,
F-CAR-CS-033-Rev.05
Pace Carolinas Quality Office
"Check mark top half of box if pH and/or dechiorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coilform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
"Bottom half of box is to list number of bottle
Project # WQ# : 92445717
PM: AMB Due Date: 09/24/19
CLIENT: 92-Nova NC
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pH Adjustment Log for Preserved Samples
Sample ID
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pH upon receipt
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added
Lot p
Note: Whenever there is a discrepancy affecting North Carolina comp Ilarice samples, a copy or this form wui Des Ent to the North Carolina uknNrs Cerdkauon urnce ii.e.
out of hold, tncorrect preservative, out oftemp, Incorrect containers.
Page 45 of 46

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Page 46 of 46

lacieAnalXical"
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
June 06, 2019
Mike Minett
Nova Consulting Group, Inc.
442 South Main Street
Suite #7
Davidson, NC 28036
RE: Project: SB/GW
Pace Project No.: 92430807
Dear Mike Minett:
Enclosed are the analytical results for sample(s) received by the laboratory between May 29, 2019
and May 30, 2019. The results relate only to the samples included in this report. Results reported
herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality
Assurance Manual, where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
A*a-
LrU
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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CERTIFICATIONS
Project: SB/GW
Pace Project No.: 92430807
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Florida/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
SB/GW
92430807
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92430807001
S13-1 14'
EPA 8015C Modified
BAJ
2
PASI-C
EPA 8015C Modified
LMB
2
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92430807002
S13-2 12'
EPA 8015C Modified
BAJ
2
PASI-C
EPA 8082A
SEM
8
PASI-C
EPA 8015C Modified
LMB
2
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92430807003
S13-4 10'
EPA 8015C Modified
BAJ
2
PASI-C
EPA 8015C Modified
LMB
2
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92430807004
S13-5 14'
EPA 8015C Modified
BAJ
2
PASI-C
EPA 8015C Modified
LMB
2
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92430807005
S13-6 9'
EPA 8015C Modified
BAJ
2
PASI-C
EPA 8015C Modified
LMB
2
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92430807006
S13-7 9
EPA 8015C Modified
BAJ
2
PASI-C
EPA 8015C Modified
LMB
2
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92430807007
S13-1 6'
EPA 8015C Modified
BAJ
2
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92430807008
S13-2 20'
EPA 8270D
PKS
74
PASI-C
ASTM D2974-87
KDF
1
PASI-C
92430807009
GW-A
EPA 8270D
PKS
74
PASI-C
EPA 8260E
DLK
63
PASI-C
92430807010
GW-B
EPA 8270D
PKS
74
PASI-C
EPA 8260E
CL
63
PASI-C
92430807011
GW-C
EPA 8270D
PKS
74
PASI-C
EPA 8260E
DLK
63
PASI-C
92430807012
GW-D
EPA 8270D
PKS
74
PASI-C
EPA 8260E
DLK
63
PASI-C
92430807013
S13-3 16'
EPA 8015C Modified
BAJ
2
PASI-C
EPA 8082A
SEM
8
PASI-C
EPA 8015C Modified
LMB
2
PASI-C
ASTM D2974-87
KDF
1
PASI-C
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ANALYTICAL RESULTS
Project: SB/GW
Pace Project No.: 92430807
Sample: S13-1 14' Lab ID: 92430807001 Collected: 05/28/19 14:58 Received: 05/29/19 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Diesel Range Organics(C10-C28)
ND mg/kg 7.6 1 05/29/19 16:14
06/01/19 14:14
Surrogates
n-Pentacosane (S)
62 % 33-129 1 05/29/19 16:14
06/01/19 14:14 629-99-2
Gasoline Range Organics
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Gas Range Organics (C6-C10)
ND mg/kg 15.7 1 05/29/19 16:48
05/30/19 05:45
Surrogates
4-Bromofluorobenzene (S)
115 % 63-130 1 05/29/19 16:48
05/30/19 05:45 460-00-4
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
34.7 % 0.10 1
05/29/19 16:31
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: SB/GW
Pace Project No.: 92430807
Sample: S13-2 12' Lab ID: 92430807002 Collected: 05/28/19 15:53 Received: 05/29/19 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Diesel Range Organics(C10-C28)
ND
mg/kg
7.4
1
05/29/19 16:14
06/01/19 14:14
Surrogates
n-Pentacosane (S)
58
%
33-129
1
05/29/19 16:14
06/01/19 14:14
629-99-2
8082 GCS PCB
Analytical Method:
EPA 8082A Preparation Method:
EPA 3546
PCB-1016 (Aroclor 1016)
ND
ug/kg
49.0
1
06/03/19 09:14
06/03/19 15:39
12674-11-2
PCB-1221 (Aroclor 1221)
ND
ug/kg
49.0
1
06/03/19 09:14
06/03/19 15:39
11104-28-2
PCB-1232 (Aroclor 1232)
ND
ug/kg
49.0
1
06/03/19 09:14
06/03/19 15:39
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/kg
49.0
1
06/03/19 09:14
06/03/19 15:39
53469-21-9
PCB-1248 (Aroclor 1248)
ND
ug/kg
49.0
1
06/03/19 09:14
06/03/19 15:39
12672-29-6
PCB-1254 (Aroclor 1254)
ND
ug/kg
49.0
1
06/03/19 09:14
06/03/19 15:39
11097-69-1
PCB-1260 (Aroclor 1260)
ND
ug/kg
49.0
1
06/03/19 09:14
06/03/19 15:39
11096-82-5
Surrogates
Decachlorobiphenyl (S)
36
%
10-130
1
06/03/19 09:14
06/03/19 15:39
2051-24-3
Gasoline Range Organics
Analytical Method: EPA 8015C Modified
Preparation
Method: EPA 5030B
Gas Range Organics (C6-C10)
10.7
mg/kg
10.0
1
05/29/19 16:48
05/30/19 06:15
Surrogates
4-Bromofluorobenzene (S)
ill
%
63-130
1
05/29/19 16:48
05/30/19 06:15
460-00-4
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
33.0
%
0.10
1
05/29/19 16:31
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: SB/GW
Pace Project No.: 92430807
Sample: S13-4 10' Lab ID: 92430807003 Collected: 05/29/19 09:00 Received: 05/29/19 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Diesel Range Organics(C10-C28)
ND mg/kg 6.2 1 05/29/19 16:14
06/01/19 14:38
Surrogates
n-Pentacosane (S)
63 % 33-129 1 05/29/19 16:14
06/01/19 14:38 629-99-2
Gasoline Range Organics
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Gas Range Organics (C6-C10)
ND mg/kg 7.1 1 05/29/19 16:48
05/30/19 06:43
Surrogates
4-Bromofluorobenzene (S)
104 % 63-130 1 05/29/19 16:48
05/30/19 06:43 460-00-4
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
20.1 % 0.10 1
05/29/19 16:31
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: SB/GW
Pace Project No.: 92430807
Sample: S13-5 14' Lab ID: 92430807004 Collected: 05/29/19 10:11 Received: 05/29/19 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Diesel Range Organics(C10-C28)
ND mg/kg 6.3 1 05/29/19 16:14
06/01/19 14:38
Surrogates
n-Pentacosane (S)
52 % 33-129 1 05/29/19 16:14
06/01/19 14:38 629-99-2
Gasoline Range Organics
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Gas Range Organics (C6-C10)
ND mg/kg 6.8 1 05/29/19 16:48
05/30/19 07:11
Surrogates
4-Bromofluorobenzene (S)
102 % 63-130 1 05/29/19 16:48
05/30/19 07:11 460-00-4
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
22.3 % 0.10 1
05/29/19 16:31
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: SB/GW
Pace Project No.: 92430807
Sample: S13-6 9' Lab ID: 92430807005 Collected: 05/29/19 11:10 Received: 05/29/19 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Diesel Range Organics(C10-C28)
ND mg/kg 5.7 1 05/29/19 16:14
06/01/19 15:03
Surrogates
n-Pentacosane (S)
63 % 33-129 1 05/29/19 16:14
06/01/19 15:03 629-99-2
Gasoline Range Organics
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Gas Range Organics (C6-C10)
ND mg/kg 7.1 1 05/29/19 16:48
05/30/19 07:39
Surrogates
4-Bromofluorobenzene (S)
102 % 63-130 1 05/29/19 16:48
05/30/19 07:39 460-00-4
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
11.3 % 0.10 1
05/29/19 16:31
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: SB/GW
Pace Project No.: 92430807
Sample: S13-7 9 Lab ID: 92430807006 Collected: 05/29/19 11:37 Received: 05/29/19 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Diesel Range Organics(C10-C28)
ND mg/kg 6.0 1 05/29/19 16:14
06/01/19 15:03
Surrogates
n-Pentacosane (S)
55 % 33-129 1 05/29/19 16:14
06/01/19 15:03 629-99-2
Gasoline Range Organics
Analytical Method: EPA 8015C Modified Preparation Method: EPA 5030B
Gas Range Organics (C6-C10)
ND mg/kg 7.7 1 05/29/19 16:48
05/30/19 08:07
Surrogates
4-Bromofluorobenzene (S)
102 % 63-130 1 05/29/19 16:48
05/30/19 08:07 460-00-4
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
15.5 % 0.10 1
05/29/19 16:31
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: SB/GW
Pace Project No.: 92430807
Sample: S13-1 6' Lab ID: 92430807007 Collected: 05/28/19 14:48 Received: 05/29/19 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
Diesel Range Organics(C10-C28) 7.4 mg/kg 6.8 1 05/29/19 16:14 06/01/19 15:28
Surrogates
n-Pentacosane (S) 66 % 33-129 1 05/29/19 16:14 06/01/19 15:28 629-99-2
Percent Moisture Analytical Method: ASTM D2974-87
Percent Moisture 27.1 % 0.10 1 05/29/19 17:16
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: SB/GW
Pace Project No.: 92430807
Sample: S13-2 20' Lab ID: 92430807008 Collected: 05/28/19 16:00 Received: 05/29/19 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave Analytical Method: EPA 8270D Preparation Method: EPA 3546
Acenaphthene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
83-32-9
Acenaphthylene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
208-96-8
Aniline
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
62-53-3
Anthracene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
120-12-7
Benzo(a)anthracene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
56-55-3
Benzo(a)pyrene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
50-32-8
Benzo(b)fluoranthene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
205-99-2
Benzo(g,h,i)perylene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
191-24-2
Benzo(k)fluoranthene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
207-08-9
Benzoic Acid
ND
ug/kg
2320
1
05/30/19 12:03
05/31/19 14:51
65-85-0
Benzyl alcohol
ND
ug/kg
929
1
05/30/19 12:03
05/31/19 14:51
100-51-6
4-Bromophenylphenyl ether
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
101-55-3
Butylbenzylphthalate
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
85-68-7
4-Chloro-3-methyl phenol
ND
ug/kg
929
1
05/30/19 12:03
05/31/19 14:51
59-50-7
4-Chloroaniline
ND
ug/kg
2320
1
05/30/19 12:03
05/31/19 14:51
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
111-91-1
bis(2-Chloroethyl) ether
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
111-44-4
2-Chloronaphthalene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
91-58-7
2-Chlorophenol
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
95-57-8
4-Chlorophenylphenyl ether
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
7005-72-3
Chrysene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
218-01-9
Dibenz(a,h)anthracene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
53-70-3
Dibenzofuran
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
132-64-9
1,2-Dichlorobenzene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
95-50-1
1,3-Dichlorobenzene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
541-73-1
1,4-Dichlorobenzene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
106-46-7
3,3'-Dichlorobenzidine
ND
ug/kg
2320
1
05/30/19 12:03
05/31/19 14:51
91-94-1
2,4-Dichlorophenol
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
120-83-2
Diethylphthalate
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
84-66-2
2,4-Dimethylphenol
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
105-67-9
Dimethylphthalate
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
131-11-3
Di-n-butylphthalate
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/kg
929
1
05/30/19 12:03
05/31/19 14:51
534-52-1
2,4-Dinitrophenol
ND
ug/kg
2320
1
05/30/19 12:03
05/31/19 14:51
51-28-5
2,4-Dinitrotoluene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
121-14-2
2,6-Dinitrotoluene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
606-20-2
Di-n-octylphthalate
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
117-81-7
Fluoranthene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
206-44-0
Fluorene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
86-73-7
Hexachloro-1,3-butadiene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
87-68-3
Hexachlorobenzene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
118-74-1
Hexachlorocyclopentadiene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
77-47-4
Hexachloroethane
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
193-39-5
Isophorone
ND
ug/kg
464
1
05/30/19 12:03
05/31/19 14:51
78-59-1
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: SB/GW
Pace Project No.: 92430807
Sample: S13-2 20' Lab ID: 92430807008 Collected: 05/28/19 16:00 Received: 05/29/19 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 MSSV Microwave
1-Methylnaphthalene
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methyl phenol (m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitrosodimethylamine
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
2,2'-Oxybis(1-chloropropane)
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
1,2,4-Trichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Surrogates
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Percent Moisture
Percent Moisture
Analytical Method: EPA 8270D Preparation Method: EPA 3546
ND
ug/kg
464
1
05/30/1912:03
05/31/1914:51
90-12-0
ND
ug/kg
464
1
05/30/1912:03
05/31/1914:51
91-57-6
ND
ug/kg
464
1
05/30/1912:03
05/31/1914:51
95-48-7
ND
ug/kg
464
1
05/30/1912:03
05/31/1914:51
15831-10-4
ND
ug/kg
464
1
05/30/1912:03
05/31/1914:51
91-20-3
ND
ug/kg
2320
1
05/30/1912:03
05/31/1914:51
88-74-4
ND
ug/kg
2320
1
05/30/1912:03
05/31/1914:51
99-09-2
ND
ug/kg
929
1
05/30/1912:03
05/31/1914:51
100-01-6
ND
ug/kg
464
1
05/30/1912:03
05/31/1914:51
98-95-3
ND
ug/kg
464
1
05/30/1912:03
05/31/1914:51
88-75-5
ND
ug/kg
2320
1
05/30/1912:03
05/31/1914:51
100-02-7
ND
ug/kg
464
1
05/30/1912:03
05/31/1914:51
62-75-9
ND
ug/kg
464
1
05/30/1912:03
05/31/1914:51
621-64-7
ND
ug/kg
464
1
05/30/1912:03
05/31/1914:51
86-30-6
ND
ug/kg
464
1
05/30/1912:03
05/31/1914:51
108-60-1
ND
mg/kg
2.3
1
05/30/1912:03
05/31/1914:51
87-86-5
ND
ug/kg
464
1
05/30/1912:03
05/31/1914:51
85-01-8
ND
ug/kg
464
1
05/30/1912:03
05/31/1914:51
108-95-2
ND
ug/kg
464
1
05/30/1912:03
05/31/1914:51
129-00-0
ND
ug/kg
464
1
05/30/1912:03
05/31/1914:51
120-82-1
ND
ug/kg
464
1
05/30/1912:03
05/31/1914:51
95-95-4
ND
ug/kg
464
1
05/30/1912:03
05/31/1914:51
88-06-2
60
%
23-110
1
05/30/1912:03
05/31/1914:51
4165-60-0
33
%
30-110
1
05/30/1912:03
05/31/1914:51
321-60-8
21
%
28-110
1
05/30/1912:03
05/31/1914:51
1718-51-0 SO
61
%
22-110
1
05/30/1912:03
05/31/1914:51
13127-88-3
66
%
13-110
1
05/30/1912:03
05/31/1914:51
367-12-4
49
%
27-110
1
05/30/1912:03
05/31/1914:51
118-79-6
Analytical Method: ASTM D2974-87
29.4 % 0.10 1
REPORT OF LABORATORY ANALYSIS
05/29/19 17:16
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SB/GW
Pace Project No.: 92430807
Sample: GW-A
Lab ID: 92430807009
Collected: 05/28/19
15:11
Received: 05/29/19 12:30 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270 RVE
Analytical Method:
EPA 8270D
Preparation Method: EPA 3510C
Acenaphthene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
83-32-9
Acenaphthylene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
208-96-8
Aniline
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
62-53-3
Anthracene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
120-12-7
Benzo(a)anthracene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
56-55-3
Benzo(a)pyrene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
50-32-8
Benzo(b)fluoranthene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
191-24-2
Benzo(k)fluoranthene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
207-08-9
Benzoic Acid
ND
ug/L
50.0
1
05/30/19 12:31
05/30/19 16:07
65-85-0 L2
Benzyl alcohol
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 16:07
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
101-55-3
Butylbenzylphthalate
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 16:07
59-50-7
4-Chloroaniline
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 16:07
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
111-44-4
2-Chloronaphthalene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
91-58-7
2-Chlorophenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
7005-72-3
Chrysene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
53-70-3
Dibenzofuran
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
132-64-9
1,2-Dichlorobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
95-50-1
1,3-Dichlorobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
541-73-1
1,4-Dichlorobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 16:07
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
120-83-2
Diethylphthalate
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
105-67-9
Dimethylphthalate
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 16:07
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
05/30/19 12:31
05/30/19 16:07
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
121-14-2
2,6-Dinitrotoluene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
606-20-2
Di-n-octylphthalate
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
1
05/30/19 12:31
05/30/19 16:07
117-81-7
Fluoranthene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
206-44-0
Fluorene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
87-68-3
Hexachlorobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
77-47-4
Hexachloroethane
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
193-39-5
Isophorone
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
78-59-1
1-Methylnaphthalene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
90-12-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SB/GW
Pace Project No.: 92430807
Sample: GW-A
Parameters
ANALYTICAL RESULTS
Lab ID: 92430807009 Collected: 05/28/19 15:11 Received: 05/29/19 12:30 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 RVE Analytical Method: EPA 8270D Preparation Method: EPA 3510C
2-Methylnaphthalene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
15831-10-4
Naphthalene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
91-20-3
2-Nitroaniline
ND
ug/L
50.0
1
05/30/19 12:31
05/30/19 16:07
88-74-4
3-Nitroaniline
ND
ug/L
50.0
1
05/30/19 12:31
05/30/19 16:07
99-09-2
4-Nitroaniline
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 16:07
100-01-6
Nitrobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
98-95-3
2-Nitrophenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
88-75-5
4-Nitrophenol
ND
ug/L
50.0
1
05/30/19 12:31
05/30/19 16:07
100-02-7
N-Nitrosodimethylamine
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
108-60-1
Pentachlorophenol
ND
ug/L
25.0
1
05/30/19 12:31
05/30/19 16:07
87-86-5
Phenanthrene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
85-01-8
Phenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
108-95-2
Pyrene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
120-82-1
2,4,5-Trichlorophenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
95-95-4
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:07
88-06-2
Surrogates
Nitrobenzene-d5 (S)
65
%
13-130
1
05/30/19 12:31
05/30/19 16:07
4165-60-0
2-Fluorobiphenyl (S)
58
%
13-130
1
05/30/19 12:31
05/30/19 16:07
321-60-8
Terphenyl-d14 (S)
67
%
25-130
1
05/30/19 12:31
05/30/19 16:07
1718-51-0
Phenol-d6 (S)
38
%
10-130
1
05/30/19 12:31
05/30/19 16:07
13127-88-3
2-Fluorophenol (S)
52
%
10-130
1
05/30/19 12:31
05/30/19 16:07
367-12-4
2,4,6-Tribromophenol (S)
76
%
10-137
1
05/30/19 12:31
05/30/19 16:07
118-79-6
8260 MSV Low Level
Analytical Method:
EPA 8260E
Acetone
ND
ug/L
25.0
1
05/31/19 06:27
67-64-1
Benzene
2.2
ug/L
1.0
1
05/31/19 06:27
71-43-2
Bromobenzene
ND
ug/L
1.0
1
05/31/19 06:27
108-86-1
Bromochloromethane
ND
ug/L
1.0
1
05/31/19 06:27
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
05/31/19 06:27
75-27-4
Bromoform
ND
ug/L
1.0
1
05/31/19 06:27
75-25-2
Bromomethane
ND
ug/L
2.0
1
05/31/19 06:27
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
05/31/19 06:27
78-93-3
Carbon tetrachloride
ND
ug/L
1.0
1
05/31/19 06:27
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
05/31/19 06:27
108-90-7
Chloroethane
ND
ug/L
1.0
1
05/31/19 06:27
75-00-3
Chloroform
ND
ug/L
5.0
1
05/31/19 06:27
67-66-3
Chloromethane
ND
ug/L
1.0
1
05/31/19 06:27
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
1
05/31/19 06:27
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
1
05/31/19 06:27
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
05/31/19 06:27
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
05/31/19 06:27
124-48-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SB/GW
Pace Project No.: 92430807
Sample: GW-A Lab ID: 92430807009 Collected: 05/28/19 15:11 Received: 05/29/19 12:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/06/2019 04:56 PM
Analytical Method: EPA 8260E
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
24.7
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
1.8
ug/L
8.4
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
4.2
ug/L
4.2
ug/L
ND
ug/L
101 %
102 %
103 %
1.0
1
05/31/19 06:27
106-93-4
1.0
1
05/31/19 06:27
74-95-3
1.0
1
05/31/19 06:27
95-50-1
1.0
1
05/31/19 06:27
541-73-1
1.0
1
05/31/19 06:27
106-46-7
1.0
1
05/31/19 06:27
75-71-8
1.0
1
05/31/19 06:27
75-34-3
1.0
1
05/31/19 06:27
107-06-2
1.0
1
05/31/19 06:27
75-35-4
1.0
1
05/31/19 06:27
156-59-2
1.0
1
05/31/19 06:27
156-60-5
1.0
1
05/31/19 06:27
78-87-5
1.0
1
05/31/19 06:27
142-28-9
1.0
1
05/31/19 06:27
594-20-7
1.0
1
05/31/19 06:27
563-58-6
1.0
1
05/31/19 06:27
10061-01-5
1.0
1
05/31/19 06:27
10061-02-6
1.0
1
05/31/19 06:27
108-20-3
1.0
1
05/31/19 06:27
100-41-4
1.0
1
05/31/19 06:27
87-68-3
5.0
1
05/31/19 06:27
591-78-6
1.0
1
05/31/19 06:27
99-87-6
5.0
1
05/31/19 06:27
75-09-2
5.0
1
05/31/19 06:27
108-10-1
1.0
1
05/31/19 06:27
1634-04-4
1.0
1
05/31/19 06:27
91-20-3
1.0
1
05/31/19 06:27
100-42-5
1.0
1
05/31/19 06:27
630-20-6
1.0
1
05/31/19 06:27
79-34-5
1.0
1
05/31/19 06:27
127-18-4
1.0
1
05/31/19 06:27
108-88-3
1.0
1
05/31/19 06:27
87-61-6
1.0
1
05/31/19 06:27
120-82-1
1.0
1
05/31/19 06:27
71-55-6
1.0
1
05/31/19 06:27
79-00-5
1.0
1
05/31/19 06:27
79-01-6
1.0
1
05/31/19 06:27
75-69-4
1.0
1
05/31/19 06:27
96-18-4
2.0
1
05/31/19 06:27
108-05-4
1.0
1
05/31/19 06:27
75-01-4
1.0
1
05/31/19 06:27
1330-20-7
2.0
1
05/31/19 06:27
179601-23-1
1.0
1
05/31/19 06:27
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
05/31/19 06:27 460-00-4
05/31/19 06:27 17060-07-0
05/31/19 06:27 2037-26-5
Page 15 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SB/GW
Pace Project No.: 92430807
Sample: GW-B
Lab ID: 92430807010
Collected: 05/28/19
17:00
Received: 05/29/19 12:30 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270 RVE
Analytical Method:
EPA 8270D
Preparation Method: EPA 3510C
Acenaphthene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
83-32-9
Acenaphthylene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
208-96-8
Aniline
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
62-53-3
Anthracene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
120-12-7
Benzo(a)anthracene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
56-55-3
Benzo(a)pyrene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
50-32-8
Benzo(b)fluoranthene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
191-24-2
Benzo(k)fluoranthene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
207-08-9
Benzoic Acid
ND
ug/L
50.0
1
05/30/19 12:31
05/30/19 16:58
65-85-0 L2
Benzyl alcohol
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 16:58
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
101-55-3
Butylbenzylphthalate
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 16:58
59-50-7
4-Chloroaniline
67.5
ug/L
20.0
1
05/30/19 12:31
05/30/19 16:58
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
111-44-4
2-Chloronaphthalene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
91-58-7
2-Chlorophenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
7005-72-3
Chrysene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
53-70-3
Dibenzofuran
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
132-64-9
1,2-Dichlorobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
95-50-1
1,3-Dichlorobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
541-73-1
1,4-Dichlorobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 16:58
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
120-83-2
Diethylphthalate
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
105-67-9
Dimethylphthalate
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 16:58
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
05/30/19 12:31
05/30/19 16:58
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
121-14-2
2,6-Dinitrotoluene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
606-20-2
Di-n-octylphthalate
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
1
05/30/19 12:31
05/30/19 16:58
117-81-7
Fluoranthene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
206-44-0
Fluorene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
87-68-3
Hexachlorobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
77-47-4
Hexachloroethane
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
193-39-5
Isophorone
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
78-59-1
1-Methylnaphthalene
33.9
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
90-12-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SB/GW
Pace Project No.: 92430807
Sample: GW-B
Lab ID: 92430807010 Collected:
05/28/19
17:00
Received: 05/29/19 12:30 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270 RVE
Analytical Method:
EPA 8270D
Preparation Method: EPA 3510C
2-Methylnaphthalene
69.0
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
15831-10-4
Naphthalene
234
ug/L
20.0
2
05/30/19 12:31
05/31/1918:08
91-20-3
2-Nitroaniline
ND
ug/L
50.0
1
05/30/19 12:31
05/30/19 16:58
88-74-4
3-Nitroaniline
ND
ug/L
50.0
1
05/30/19 12:31
05/30/19 16:58
99-09-2
4-Nitroaniline
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 16:58
100-01-6
Nitrobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
98-95-3
2-Nitrophenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
88-75-5
4-Nitrophenol
ND
ug/L
50.0
1
05/30/19 12:31
05/30/19 16:58
100-02-7
N-Nitrosodimethylamine
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
108-60-1
Pentachlorophenol
ND
ug/L
25.0
1
05/30/19 12:31
05/30/19 16:58
87-86-5
Phenanthrene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
85-01-8
Phenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
108-95-2
Pyrene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
120-82-1
2,4,5-Trichlorophenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
95-95-4
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 16:58
88-06-2
Surrogates
Nitrobenzene-d5 (S)
48
%
13-130
1
05/30/19 12:31
05/30/19 16:58
4165-60-0
2-Fluorobiphenyl (S)
46
%
13-130
1
05/30/19 12:31
05/30/19 16:58
321-60-8
Terphenyl-d14 (S)
71
%
25-130
1
05/30/19 12:31
05/30/19 16:58
1718-51-0
Phenol-d6 (S)
31
%
10-130
1
05/30/19 12:31
05/30/19 16:58
13127-88-3
2-Fluorophenol (S)
37
%
10-130
1
05/30/19 12:31
05/30/19 16:58
367-12-4
2,4,6-Tribromophenol (S)
60
%
10-137
1
05/30/19 12:31
05/30/19 16:58
118-79-6
8260 MSV Low Level
Analytical Method:
EPA 8260E
Acetone
ND
ug/L
2500
100
06/05/19 17:42
67-64-1 HS
Benzene
237
ug/L
100
100
06/05/19 17:42
71-43-2
Bromobenzene
ND
ug/L
100
100
06/05/19 17:42
108-86-1
Bromochloromethane
ND
ug/L
100
100
06/05/19 17:42
74-97-5
Bromodichloromethane
ND
ug/L
100
100
06/05/19 17:42
75-27-4
Bromoform
ND
ug/L
100
100
06/05/19 17:42
75-25-2
Bromomethane
ND
ug/L
200
100
06/05/19 17:42
74-83-9 L1
2-Butanone (MEK)
ND
ug/L
500
100
06/05/19 17:42
78-93-3
Carbon tetrachloride
ND
ug/L
100
100
06/05/19 17:42
56-23-5
Chlorobenzene
ND
ug/L
100
100
06/05/19 17:42
108-90-7
Chloroethane
ND
ug/L
100
100
06/05/19 17:42
75-00-3
Chloroform
ND
ug/L
500
100
06/05/19 17:42
67-66-3
Chloromethane
ND
ug/L
100
100
06/05/19 17:42
74-87-3
2-Chlorotoluene
ND
ug/L
100
100
06/05/19 17:42
95-49-8
4-Chlorotoluene
ND
ug/L
100
100
06/05/19 17:42
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
500
100
06/05/19 17:42
96-12-8
Dibromochloromethane
ND
ug/L
100
100
06/05/19 17:42
124-48-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SB/GW
Pace Project No.: 92430807
Sample: GW-B
Lab ID: 92430807010 Collected:
05/28/19
17:00
Received: 05/29/19 12:30 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared Analyzed
CAS No.
Qual
8260 MSV Low Level
Analytical Method:
EPA 8260E
1,2-Dibromoethane (EDB)
ND
ug/L
100
100
06/05/19 17:42
106-93-4
Dibromomethane
ND
ug/L
100
100
06/05/19 17:42
74-95-3
1,2-Dichlorobenzene
ND
ug/L
100
100
06/05/19 17:42
95-50-1
1,3-Dichlorobenzene
ND
ug/L
100
100
06/05/19 17:42
541-73-1
1,4-Dichlorobenzene
ND
ug/L
100
100
06/05/19 17:42
106-46-7
Dichlorodifluoromethane
ND
ug/L
100
100
06/05/19 17:42
75-71-8
1,1-Dichloroethane
ND
ug/L
100
100
06/05/19 17:42
75-34-3
1,2-Dichloroethane
ND
ug/L
100
100
06/05/19 17:42
107-06-2
1,1-Dichloroethene
ND
ug/L
100
100
06/05/19 17:42
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
100
100
06/05/19 17:42
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
100
100
06/05/19 17:42
156-60-5
1,2-Dichloropropane
ND
ug/L
100
100
06/05/19 17:42
78-87-5
1,3-Dichloropropane
ND
ug/L
100
100
06/05/19 17:42
142-28-9
2,2-Dichloropropane
ND
ug/L
100
100
06/05/19 17:42
594-20-7
1,1-Dichloropropene
ND
ug/L
100
100
06/05/19 17:42
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
100
100
06/05/19 17:42
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
100
100
06/05/19 17:42
10061-02-6
Diisopropyl ether
ND
ug/L
100
100
06/05/19 17:42
108-20-3
Ethylbenzene
5350
ug/L
100
100
06/05/19 17:42
100-41-4
M1
Hexachloro-1,3-butadiene
ND
ug/L
100
100
06/05/19 17:42
87-68-3
2-Hexanone
ND
ug/L
500
100
06/05/19 17:42
591-78-6
p-Isopropyltoluene
ND
ug/L
100
100
06/05/19 17:42
99-87-6
Methylene Chloride
ND
ug/L
500
100
06/05/19 17:42
75-09-2
4-Methyl-2-pentanone (MIBK)
ND
ug/L
500
100
06/05/19 17:42
108-10-1
Methyl-tert-butyl ether
ND
ug/L
100
100
06/05/19 17:42
1634-04-4
Naphthalene
756
ug/L
100
100
06/05/19 17:42
91-20-3
Styrene
ND
ug/L
100
100
06/05/19 17:42
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
100
100
06/05/19 17:42
630-20-6
1,1,2,2-Tetrachloroethane
ND
ug/L
100
100
06/05/19 17:42
79-34-5
Tetrachloroethene
ND
ug/L
100
100
06/05/19 17:42
127-18-4
Toluene
615
ug/L
100
100
06/05/19 17:42
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
100
100
06/05/19 17:42
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
100
100
06/05/19 17:42
120-82-1
1,1,1-Trichloroethane
ND
ug/L
100
100
06/05/19 17:42
71-55-6
1,1,2-Trichloroethane
ND
ug/L
100
100
06/05/19 17:42
79-00-5
Trichloroethene
ND
ug/L
100
100
06/05/19 17:42
79-01-6
Trichlorofluoromethane
ND
ug/L
100
100
06/05/19 17:42
75-69-4
1,2,3-Trichloropropane
ND
ug/L
100
100
06/05/19 17:42
96-18-4
Vinyl acetate
ND
ug/L
200
100
06/05/19 17:42
108-05-4
Vinyl chloride
ND
ug/L
100
100
06/05/19 17:42
75-01-4
Xylene (Total)
26700
ug/L
100
100
06/05/19 17:42
1330-20-7
MS
m&p-Xylene
19100
ug/L
200
100
06/05/19 17:42
179601-23-1
M1
o-Xylene
7590
ug/L
100
100
06/05/19 17:42
95-47-6
M1
Surrogates
4-Bromofluorobenzene (S)
100
%
70-130
100
06/05/19 17:42
460-00-4
1,2-Dichloroethane-d4 (S)
98
%
70-130
100
06/05/19 17:42
17060-07-0
Toluene-d8 (S)
100
%
70-130
100
06/05/19 17:42
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SB/GW
Pace Project No.: 92430807
Sample: GW-C
Lab ID: 92430807011
Collected: 05/29/19
10:32
Received: 05/29/19 12:30 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270 RVE
Analytical Method:
EPA 8270D Preparation Method: EPA 3510C
Acenaphthene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
83-32-9
Acenaphthylene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
208-96-8
Aniline
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
62-53-3
Anthracene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
120-12-7
Benzo(a)anthracene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
56-55-3
Benzo(a)pyrene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
50-32-8
Benzo(b)fluoranthene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
191-24-2
Benzo(k)fluoranthene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
207-08-9
Benzoic Acid
ND
ug/L
50.0
1
05/30/19 12:31
05/30/19 17:24
65-85-0 L2
Benzyl alcohol
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 17:24
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
101-55-3
Butylbenzylphthalate
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 17:24
59-50-7
4-Chloroaniline
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 17:24
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
111-44-4
2-Chloronaphthalene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
91-58-7
2-Chlorophenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
7005-72-3
Chrysene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
53-70-3
Dibenzofuran
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
132-64-9
1,2-Dichlorobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
95-50-1
1,3-Dichlorobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
541-73-1
1,4-Dichlorobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 17:24
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
120-83-2
Diethylphthalate
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
105-67-9
Dimethylphthalate
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 17:24
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
05/30/19 12:31
05/30/19 17:24
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
121-14-2
2,6-Dinitrotoluene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
606-20-2
Di-n-octylphthalate
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
1
05/30/19 12:31
05/30/19 17:24
117-81-7
Fluoranthene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
206-44-0
Fluorene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
87-68-3
Hexachlorobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
77-47-4
Hexachloroethane
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
193-39-5
Isophorone
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
78-59-1
1-Methylnaphthalene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
90-12-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SB/GW
Pace Project No.: 92430807
Sample: GW-C
Parameters
ANALYTICAL RESULTS
Lab ID: 92430807011 Collected: 05/29/19 10:32 Received: 05/29/19 12:30 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 RVE Analytical Method: EPA 8270D Preparation Method: EPA 3510C
2-Methylnaphthalene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
15831-10-4
Naphthalene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
91-20-3
2-Nitroaniline
ND
ug/L
50.0
1
05/30/19 12:31
05/30/19 17:24
88-74-4
3-Nitroaniline
ND
ug/L
50.0
1
05/30/19 12:31
05/30/19 17:24
99-09-2
4-Nitroaniline
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 17:24
100-01-6
Nitrobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
98-95-3
2-Nitrophenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
88-75-5
4-Nitrophenol
ND
ug/L
50.0
1
05/30/19 12:31
05/30/19 17:24
100-02-7
N-Nitrosodimethylamine
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
108-60-1
Pentachlorophenol
ND
ug/L
25.0
1
05/30/19 12:31
05/30/19 17:24
87-86-5
Phenanthrene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
85-01-8
Phenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
108-95-2
Pyrene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
120-82-1
2,4,5-Trichlorophenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
95-95-4
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:24
88-06-2
Surrogates
Nitrobenzene-d5 (S)
59
%
13-130
1
05/30/19 12:31
05/30/19 17:24
4165-60-0
2-Fluorobiphenyl (S)
51
%
13-130
1
05/30/19 12:31
05/30/19 17:24
321-60-8
Terphenyl-d14 (S)
76
%
25-130
1
05/30/19 12:31
05/30/19 17:24
1718-51-0
Phenol-d6 (S)
33
%
10-130
1
05/30/19 12:31
05/30/19 17:24
13127-88-3
2-Fluorophenol (S)
22
%
10-130
1
05/30/19 12:31
05/30/19 17:24
367-12-4
2,4,6-Tribromophenol (S)
35
%
10-137
1
05/30/19 12:31
05/30/19 17:24
118-79-6
8260 MSV Low Level
Analytical Method:
EPA 8260E
Acetone
ND
ug/L
25.0
1
05/31/19 07:20
67-64-1
Benzene
ND
ug/L
1.0
1
05/31/19 07:20
71-43-2
Bromobenzene
ND
ug/L
1.0
1
05/31/19 07:20
108-86-1
Bromochloromethane
ND
ug/L
1.0
1
05/31/19 07:20
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
05/31/19 07:20
75-27-4
Bromoform
ND
ug/L
1.0
1
05/31/19 07:20
75-25-2
Bromomethane
ND
ug/L
2.0
1
05/31/19 07:20
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
05/31/19 07:20
78-93-3
Carbon tetrachloride
ND
ug/L
1.0
1
05/31/19 07:20
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
05/31/19 07:20
108-90-7
Chloroethane
ND
ug/L
1.0
1
05/31/19 07:20
75-00-3
Chloroform
ND
ug/L
5.0
1
05/31/19 07:20
67-66-3
Chloromethane
ND
ug/L
1.0
1
05/31/19 07:20
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
1
05/31/19 07:20
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
1
05/31/19 07:20
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
05/31/19 07:20
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
05/31/19 07:20
124-48-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SB/GW
Pace Project No.: 92430807
Sample: GW-C Lab ID: 92430807011 Collected: 05/29/19 10:32 Received: 05/29/19 12:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/06/2019 04:56 PM
Analytical Method: EPA 8260E
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
100 %
103 %
103 %
1.0
1
05/31/19 07:20
106-93-4
1.0
1
05/31/19 07:20
74-95-3
1.0
1
05/31/19 07:20
95-50-1
1.0
1
05/31/19 07:20
541-73-1
1.0
1
05/31/19 07:20
106-46-7
1.0
1
05/31/19 07:20
75-71-8
1.0
1
05/31/19 07:20
75-34-3
1.0
1
05/31/19 07:20
107-06-2
1.0
1
05/31/19 07:20
75-35-4
1.0
1
05/31/19 07:20
156-59-2
1.0
1
05/31/19 07:20
156-60-5
1.0
1
05/31/19 07:20
78-87-5
1.0
1
05/31/19 07:20
142-28-9
1.0
1
05/31/19 07:20
594-20-7
1.0
1
05/31/19 07:20
563-58-6
1.0
1
05/31/19 07:20
10061-01-5
1.0
1
05/31/19 07:20
10061-02-6
1.0
1
05/31/19 07:20
108-20-3
1.0
1
05/31/19 07:20
100-41-4
1.0
1
05/31/19 07:20
87-68-3
5.0
1
05/31/19 07:20
591-78-6
1.0
1
05/31/19 07:20
99-87-6
5.0
1
05/31/19 07:20
75-09-2
5.0
1
05/31/19 07:20
108-10-1
1.0
1
05/31/19 07:20
1634-04-4
1.0
1
05/31/19 07:20
91-20-3
1.0
1
05/31/19 07:20
100-42-5
1.0
1
05/31/19 07:20
630-20-6
1.0
1
05/31/19 07:20
79-34-5
1.0
1
05/31/19 07:20
127-18-4
1.0
1
05/31/19 07:20
108-88-3
1.0
1
05/31/19 07:20
87-61-6
1.0
1
05/31/19 07:20
120-82-1
1.0
1
05/31/19 07:20
71-55-6
1.0
1
05/31/19 07:20
79-00-5
1.0
1
05/31/19 07:20
79-01-6
1.0
1
05/31/19 07:20
75-69-4
1.0
1
05/31/19 07:20
96-18-4
2.0
1
05/31/19 07:20
108-05-4
1.0
1
05/31/19 07:20
75-01-4
1.0
1
05/31/19 07:20
1330-20-7
2.0
1
05/31/19 07:20
179601-23-1
1.0
1
05/31/19 07:20
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
05/31/19 07:20 460-00-4
05/31/19 07:20 17060-07-0
05/31/19 07:20 2037-26-5
Page 21 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: SB/GW
Pace Project No.: 92430807
Sample: GW-D
Lab ID: 92430807012
Collected: 05/29/19
11:48
Received: 05/29/19 12:30 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
8270 RVE
Analytical Method:
EPA 8270D
Preparation Method: EPA 3510C
Acenaphthene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
83-32-9
Acenaphthylene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
208-96-8
Aniline
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
62-53-3
Anthracene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
120-12-7
Benzo(a)anthracene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
56-55-3
Benzo(a)pyrene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
50-32-8
Benzo(b)fluoranthene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
191-24-2
Benzo(k)fluoranthene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
207-08-9
Benzoic Acid
ND
ug/L
50.0
1
05/30/19 12:31
05/30/19 17:49
65-85-0 L2
Benzyl alcohol
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 17:49
100-51-6
4-Bromophenylphenyl ether
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
101-55-3
Butylbenzylphthalate
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
85-68-7
4-ChIoro-3-methyl phenol
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 17:49
59-50-7
4-Chloroaniline
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 17:49
106-47-8
bis(2-Chloroethoxy)methane
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
111-44-4
2-Chloronaphthalene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
91-58-7
2-Chlorophenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
7005-72-3
Chrysene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
53-70-3
Dibenzofuran
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
132-64-9
1,2-Dichlorobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
95-50-1
1,3-Dichlorobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
541-73-1
1,4-Dichlorobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
106-46-7
3,3'-Dichlorobenzidine
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 17:49
91-94-1
2,4-Dichlorophenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
120-83-2
Diethylphthalate
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
84-66-2
2,4-Dimethylphenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
105-67-9
Dimethylphthalate
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
131-11-3
Di-n-butylphthalate
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
84-74-2
4,6-Dinitro-2-methyl phenol
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 17:49
534-52-1
2,4-Dinitrophenol
ND
ug/L
50.0
1
05/30/19 12:31
05/30/19 17:49
51-28-5
2,4-Dinitrotoluene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
121-14-2
2,6-Dinitrotoluene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
606-20-2
Di-n-octylphthalate
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
117-84-0
bis(2- Ethyl hexyl)phthalate
ND
ug/L
6.0
1
05/30/19 12:31
05/30/19 17:49
117-81-7
Fluoranthene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
206-44-0
Fluorene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
87-68-3
Hexachlorobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
77-47-4
Hexachloroethane
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
193-39-5
Isophorone
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
78-59-1
1-Methylnaphthalene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
90-12-0
REPORT OF LABORATORY ANALYSIS
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Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 63

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Project: SB/GW
Pace Project No.: 92430807
Sample: GW-D
Parameters
ANALYTICAL RESULTS
Lab ID: 92430807012 Collected: 05/29/19 11:48 Received: 05/29/19 12:30 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8270 RVE Analytical Method: EPA 8270D Preparation Method: EPA 3510C
2-Methylnaphthalene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
91-57-6
2-Methylphenol(o-Cresol)
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
95-48-7
3&4-Methyl phenol (m&p Cresol)
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
15831-10-4
Naphthalene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
91-20-3
2-Nitroaniline
ND
ug/L
50.0
1
05/30/19 12:31
05/30/19 17:49
88-74-4
3-Nitroaniline
ND
ug/L
50.0
1
05/30/19 12:31
05/30/19 17:49
99-09-2
4-Nitroaniline
ND
ug/L
20.0
1
05/30/19 12:31
05/30/19 17:49
100-01-6
Nitrobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
98-95-3
2-Nitrophenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
88-75-5
4-Nitrophenol
ND
ug/L
50.0
1
05/30/19 12:31
05/30/19 17:49
100-02-7
N-Nitrosodimethylamine
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
108-60-1
Pentachlorophenol
ND
ug/L
25.0
1
05/30/19 12:31
05/30/19 17:49
87-86-5
Phenanthrene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
85-01-8
Phenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
108-95-2
Pyrene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
120-82-1
2,4,5-Trichlorophenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
95-95-4
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
05/30/19 12:31
05/30/19 17:49
88-06-2
Surrogates
Nitrobenzene-d5 (S)
73
%
13-130
1
05/30/19 12:31
05/30/19 17:49
4165-60-0
2-Fluorobiphenyl (S)
69
%
13-130
1
05/30/19 12:31
05/30/19 17:49
321-60-8
Terphenyl-d14 (S)
72
%
25-130
1
05/30/19 12:31
05/30/19 17:49
1718-51-0
Phenol-d6 (S)
41
%
10-130
1
05/30/19 12:31
05/30/19 17:49
13127-88-3
2-Fluorophenol (S)
57
%
10-130
1
05/30/19 12:31
05/30/19 17:49
367-12-4
2,4,6-Tribromophenol (S)
66
%
10-137
1
05/30/19 12:31
05/30/19 17:49
118-79-6
8260 MSV Low Level
Analytical Method:
EPA 8260E
Acetone
ND
ug/L
25.0
1
05/31/19 07:02
67-64-1
Benzene
ND
ug/L
1.0
1
05/31/19 07:02
71-43-2
Bromobenzene
ND
ug/L
1.0
1
05/31/19 07:02
108-86-1
Bromochloromethane
ND
ug/L
1.0
1
05/31/19 07:02
74-97-5
Bromodichloromethane
ND
ug/L
1.0
1
05/31/19 07:02
75-27-4
Bromoform
ND
ug/L
1.0
1
05/31/19 07:02
75-25-2
Bromomethane
ND
ug/L
2.0
1
05/31/19 07:02
74-83-9
2-Butanone (MEK)
ND
ug/L
5.0
1
05/31/19 07:02
78-93-3
Carbon tetrachloride
ND
ug/L
1.0
1
05/31/19 07:02
56-23-5
Chlorobenzene
ND
ug/L
1.0
1
05/31/19 07:02
108-90-7
Chloroethane
ND
ug/L
1.0
1
05/31/19 07:02
75-00-3
Chloroform
ND
ug/L
5.0
1
05/31/19 07:02
67-66-3
Chloromethane
ND
ug/L
1.0
1
05/31/19 07:02
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
1
05/31/19 07:02
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
1
05/31/19 07:02
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
5.0
1
05/31/19 07:02
96-12-8
Dibromochloromethane
ND
ug/L
1.0
1
05/31/19 07:02
124-48-1
REPORT OF LABORATORY ANALYSIS
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Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 63

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ANALYTICAL RESULTS
Project: SB/GW
Pace Project No.: 92430807
Sample: GW-D Lab ID: 92430807012 Collected: 05/29/19 11:48 Received: 05/29/19 12:30 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260 MSV Low Level
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
2-Hexanone
p-Isopropyltoluene
Methylene Chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
Vinyl acetate
Vinyl chloride
Xylene (Total)
m&p-Xylene
o-Xylene
Surrogates
4-Bromofluorobenzene (S)
1,2-Dichloroethane-d4 (S)
Toluene-d8 (S)
Date: 06/06/2019 04:56 PM
Analytical Method: EPA 8260E
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
100 %
103 %
100 %
1.0
1
05/31/19 07:02
106-93-4
1.0
1
05/31/19 07:02
74-95-3
1.0
1
05/31/19 07:02
95-50-1
1.0
1
05/31/19 07:02
541-73-1
1.0
1
05/31/19 07:02
106-46-7
1.0
1
05/31/19 07:02
75-71-8
1.0
1
05/31/19 07:02
75-34-3
1.0
1
05/31/19 07:02
107-06-2
1.0
1
05/31/19 07:02
75-35-4
1.0
1
05/31/19 07:02
156-59-2
1.0
1
05/31/19 07:02
156-60-5
1.0
1
05/31/19 07:02
78-87-5
1.0
1
05/31/19 07:02
142-28-9
1.0
1
05/31/19 07:02
594-20-7
1.0
1
05/31/19 07:02
563-58-6
1.0
1
05/31/19 07:02
10061-01-5
1.0
1
05/31/19 07:02
10061-02-6
1.0
1
05/31/19 07:02
108-20-3
1.0
1
05/31/19 07:02
100-41-4
1.0
1
05/31/19 07:02
87-68-3
5.0
1
05/31/19 07:02
591-78-6
1.0
1
05/31/19 07:02
99-87-6
5.0
1
05/31/19 07:02
75-09-2
5.0
1
05/31/19 07:02
108-10-1
1.0
1
05/31/19 07:02
1634-04-4
1.0
1
05/31/19 07:02
91-20-3
1.0
1
05/31/19 07:02
100-42-5
1.0
1
05/31/19 07:02
630-20-6
1.0
1
05/31/19 07:02
79-34-5
1.0
1
05/31/19 07:02
127-18-4
1.0
1
05/31/19 07:02
108-88-3
1.0
1
05/31/19 07:02
87-61-6
1.0
1
05/31/19 07:02
120-82-1
1.0
1
05/31/19 07:02
71-55-6
1.0
1
05/31/19 07:02
79-00-5
1.0
1
05/31/19 07:02
79-01-6
1.0
1
05/31/19 07:02
75-69-4
1.0
1
05/31/19 07:02
96-18-4
2.0
1
05/31/19 07:02
108-05-4
1.0
1
05/31/19 07:02
75-01-4
1.0
1
05/31/19 07:02
1330-20-7
2.0
1
05/31/19 07:02
179601-23-1
1.0
1
05/31/19 07:02
95-47-6
70-130 1
70-130 1
70-130 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
05/31/19 07:02 460-00-4 HS
05/31/19 07:02 17060-07-0
05/31/19 07:02 2037-26-5
Page 24 of 63

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ANALYTICAL RESULTS
Project: SB/GW
Pace Project No.: 92430807
Sample: S13-3 16' Lab ID: 92430807013 Collected: 05/29/19 16:32 Received: 05/30/19 12:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8015 GCS THC-Diesel
Diesel Range Organics(C10-C28)
Surrogates
n-Pentacosane (S)
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Surrogates
Decachlorobiphenyl (S)
Gasoline Range Organics
Gas Range Organics (C6-C10)
Surrogates
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
Date: 06/06/2019 04:56 PM
Analytical Method: EPA 8015C Modified Preparation Method: EPA 3546
180
mg/kg
5.4
1
06/03/19 09:56
06/04/19 14:07
75
%
33-129
1
06/03/19 09:56
06/04/19 14:07
629-99-2
Analytical Method:
EPA 8082A Preparation Method:
EPA 3546
ND
ug/kg
36.8
1
06/03/19 09:14
06/03/19 16:00
12674-11-2
ND
ug/kg
36.8
1
06/03/19 09:14
06/03/19 16:00
11104-28-2
ND
ug/kg
36.8
1
06/03/19 09:14
06/03/19 16:00
11141-16-5
ND
ug/kg
36.8
1
06/03/19 09:14
06/03/19 16:00
53469-21-9
ND
ug/kg
36.8
1
06/03/19 09:14
06/03/19 16:00
12672-29-6
ND
ug/kg
36.8
1
06/03/19 09:14
06/03/19 16:00
11097-69-1
ND
ug/kg
36.8
1
06/03/19 09:14
06/03/19 16:00
11096-82-5
73
%
10-130
1
06/03/19 09:14
06/03/19 16:00
2051-24-3
Analytical Method: EPA 8015C Modified
Preparation
Method: EPA 5030B
1340
mg/kg
25.9
4
05/31/1913:02
05/31/1919:46
120
%
63-130
4
05/31/1913:02
05/31/1919:46
460-00-4
Analytical Method: ASTM D2974-87
8.9
%
0.10
1
05/31 /19 13:54
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 25 of 63

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QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
QC Batch: 478023 Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 5030E Analysis Description: Gasoline Range Organics
Associated Lab Samples: 92430807001, 92430807002, 92430807003, 92430807004, 92430807005, 92430807006
METHOD BLANK: 2588119 Matrix: Solid
Associated Lab Samples: 92430807001, 92430807002, 92430807003, 92430807004, 92430807005, 92430807006
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Gas Range Organics (C6-C10) mg/kg ND 6.0 05/30/19 03:18
4-Bromofluorobenzene (S) % 116 63-130 05/30/19 03:18
LABORATORY CONTROL SAMPLE: 2588120
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Gas Range Organics (C6-C10) mg/kg 49.9 53.7 108 70-130
4-Bromofluorobenzene (S) % 113 63-130
MATRIX SPIKE SAMPLE:
Parameter
2588122
Units
92430807006
Result
Spike MS
Conc. Result
MS % Rec
% Rec Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND
64.3 72.9
112 40-155
4-Bromofluorobenzene (S)
%
101 63-130
SAMPLE DUPLICATE: 2588121
92430508001
Dup
Parameter
Units
Result
Result RPD
Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND
ND
4-Bromofluorobenzene (S)
%
103
114
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC.
Page 26 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
QC Batch: 478460 Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 5030E Analysis Description: Gasoline Range Organics
Associated Lab Samples: 92430807013
METHOD BLANK: 2590022 Matrix: Solid
Associated Lab Samples: 92430807013
Blank Reporting
Parameter Units Result Limit Analyzed
Gas Range Organics (C6-C10) mg/kg ND 6.0 05/31/19 13:00
4-Bromofluorobenzene (S) % 111 63-130 05/31/19 13:00
Qualifiers
LABORATORY CONTROL SAMPLE:
2590023
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Gas Range Organics (C6-C10)
mg/kg
49.9 57.4
115
70-130
4-Bromofluorobenzene (S)
%
106
63-130
MATRIX SPIKE SAMPLE:
2590025
92431099001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Gas Range Organics (C6-C10)
mg/kg
ND 56.2
75.0
124
40-155
4-Bromofluorobenzene (S)
%
122
63-130
SAMPLE DUPLICATE: 2590024
Parameter
Gas Range Organics (C6-C10)
4-Bromofluorobenzene (S)
92430947001 Dup
Units Result Result
mg/kg ND ND
112 124
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
QC Batch: 478294 Analysis Method: EPA 8260B
QC Batch Method: EPA 8260E Analysis Description: 8260 MSV Low Level
Associated Lab Samples: 92430807009, 92430807011, 92430807012
METHOD BLANK: 2589474 Matrix:
Associated Lab Samples: 92430807009, 92430807011, 92430807012
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
05/31/19 01:41
1,1,1-Trichloroethane
ug/L
ND
1.0
05/31/19 01:41
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
05/31/19 01:41
1,1,2-Trichloroethane
ug/L
ND
1.0
05/31/19 01:41
1,1-Dichloroethane
ug/L
ND
1.0
05/31/19 01:41
1,1-Dichloroethene
ug/L
ND
1.0
05/31/19 01:41
1,1-Dichloropropene
ug/L
ND
1.0
05/31/19 01:41
1,2,3-Trichlorobenzene
ug/L
ND
1.0
05/31/19 01:41
1,2,3-Trichloropropane
ug/L
ND
1.0
05/31/19 01:41
1,2,4-Trichlorobenzene
ug/L
ND
1.0
05/31/19 01:41
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
05/31/19 01:41
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
05/31/19 01:41
1,2-Dichlorobenzene
ug/L
ND
1.0
05/31/19 01:41
1,2-Dichloroethane
ug/L
ND
1.0
05/31/19 01:41
1,2-Dichloropropane
ug/L
ND
1.0
05/31/19 01:41
1,3-Dichlorobenzene
ug/L
ND
1.0
05/31/19 01:41
1,3-Dichloropropane
ug/L
ND
1.0
05/31/19 01:41
1,4-Dichlorobenzene
ug/L
ND
1.0
05/31/19 01:41
2,2-Dichloropropane
ug/L
ND
1.0
05/31/19 01:41
2-Butanone (MEK)
ug/L
ND
5.0
05/31/19 01:41
2-Chlorotoluene
ug/L
ND
1.0
05/31/19 01:41
2-Hexanone
ug/L
ND
5.0
05/31/19 01:41
4-Chlorotoluene
ug/L
ND
1.0
05/31/19 01:41
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
05/31/19 01:41
Acetone
ug/L
ND
25.0
05/31/19 01:41
Benzene
ug/L
ND
1.0
05/31/19 01:41
Bromobenzene
ug/L
ND
1.0
05/31/19 01:41
Bromochloromethane
ug/L
ND
1.0
05/31/19 01:41
Bromodichloromethane
ug/L
ND
1.0
05/31/19 01:41
Bromoform
ug/L
ND
1.0
05/31/19 01:41
Bromomethane
ug/L
ND
2.0
05/31/19 01:41
Carbon tetrachloride
ug/L
ND
1.0
05/31/19 01:41
Chlorobenzene
ug/L
ND
1.0
05/31/19 01:41
Chloroethane
ug/L
ND
1.0
05/31/19 01:41
Chloroform
ug/L
ND
5.0
05/31/19 01:41
Chloromethane
ug/L
ND
1.0
05/31/19 01:41
cis-1,2-Dichloroethene
ug/L
ND
1.0
05/31/19 01:41
cis-1,3-Dichloropropene
ug/L
ND
1.0
05/31/19 01:41
Dibromochloromethane
ug/L
ND
1.0
05/31/19 01:41
Dibromomethane
ug/L
ND
1.0
05/31/19 01:41
Dichlorodifluoromethane
ug/L
ND
1.0
05/31/19 01:41
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
METHOD BLANK: 2589474 Matrix:
Associated Lab Samples: 92430807009, 92430807011, 92430807012
Blank
Parameter Units Result
Water
Reporting
Limit
Analyzed
Diisopropyl ether
ug/L
ND
1.0
05/31/19 01:41
Ethylbenzene
ug/L
ND
1.0
05/31/19 01:41
Hexachloro-1,3-butadiene
ug/L
ND
1.0
05/31/19 01:41
m&p-Xylene
ug/L
ND
2.0
05/31/19 01:41
Methyl-tert-butyl ether
ug/L
ND
1.0
05/31/19 01:41
Methylene Chloride
ug/L
ND
5.0
05/31/19 01:41
Naphthalene
ug/L
ND
1.0
05/31/19 01:41
o-Xylene
ug/L
ND
1.0
05/31/19 01:41
p-Isopropyltoluene
ug/L
ND
1.0
05/31/19 01:41
Styrene
ug/L
ND
1.0
05/31/19 01:41
Tetrachloroethene
ug/L
ND
1.0
05/31/19 01:41
Toluene
ug/L
ND
1.0
05/31/19 01:41
trans-1,2-Dichloroethene
ug/L
ND
1.0
05/31/19 01:41
trans- 1,3-Dichloropropene
ug/L
ND
1.0
05/31/19 01:41
Trichloroethene
ug/L
ND
1.0
05/31/19 01:41
Trichlorofluoromethane
ug/L
ND
1.0
05/31/19 01:41
Vinyl acetate
ug/L
ND
2.0
05/31/19 01:41
Vinyl chloride
ug/L
ND
1.0
05/31/19 01:41
Xylene (Total)
ug/L
ND
1.0
05/31/19 01:41
1,2-Dichloroethane-d4 (S)
%
99
70-130
05/31/19 01:41
4-Bromofluorobenzene (S)
%
100
70-130
05/31/19 01:41
Toluene-d8 (S)
%
100
70-130
05/31/19 01:41
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2589475
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
53.5
107
70-130
1,1,1-Trichloroethane
ug/L
50
50.9
102
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
49.4
99
70-130
1,1,2-Trichloroethane
ug/L
50
51.1
102
70-130
1,1-Dichloroethane
ug/L
50
51.4
103
70-130
1,1-Dichloroethene
ug/L
50
54.3
109
70-130
1,1-Dichloropropene
ug/L
50
47.8
96
70-130
1,2,3-Trichlorobenzene
ug/L
50
51.9
104
70-130
1,2,3-Trichloropropane
ug/L
50
50.0
100
70-130
1,2,4-Trichlorobenzene
ug/L
50
50.5
101
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
51.3
103
70-130
1,2-Dibromoethane (EDB)
ug/L
50
50.6
101
70-130
1,2-Dichlorobenzene
ug/L
50
47.5
95
70-130
1,2-Dichloroethane
ug/L
50
54.2
108
70-130
1,2-Dichloropropane
ug/L
50
49.2
98
70-130
1,3-Dichlorobenzene
ug/L
50
48.0
96
70-130
1,3-Dichloropropane
ug/L
50
50.0
100
70-131
1,4-Dichlorobenzene
ug/L
50
48.0
96
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
LABORATORY CONTROL SAMPLE:
Parameter
2589475
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
2,2-Dichloropropane
ug/L
50
51.3
103
69-130
2-Butanone (MEK)
ug/L
100
104
104
64-135
2-Chlorotoluene
ug/L
50
47.4
95
70-130
2-Hexanone
ug/L
100
103
103
66-135
4-Chlorotoluene
ug/L
50
47.4
95
70-130
4-Methyl-2-pentanone (MIBK)
ug/L
100
102
102
70-130
Acetone
ug/L
100
115
115
61-157
Benzene
ug/L
50
50.4
101
70-130
Bromobenzene
ug/L
50
50.4
101
70-130
Bromochloromethane
ug/L
50
59.8
120
70-130
Bromodichloromethane
ug/L
50
49.3
99
70-130
Bromoform
ug/L
50
50.4
101
70-130
Bromomethane
ug/L
50
45.2
90
38-130
Carbon tetrachloride
ug/L
50
47.6
95
70-130
Chlorobenzene
ug/L
50
48.2
96
70-130
Chloroethane
ug/L
50
45.9
92
37-142
Chloroform
ug/L
50
49.6
99
70-130
Chloromethane
ug/L
50
46.9
94
48-130
cis-1,2-Dichloroethene
ug/L
50
51.1
102
70-130
cis-1,3-Dichloropropene
ug/L
50
52.1
104
70-130
Dibromochloromethane
ug/L
50
51.0
102
70-130
Dibromomethane
ug/L
50
49.9
100
70-130
Dichlorodifluoromethane
ug/L
50
48.7
97
53-134
Diisopropyl ether
ug/L
50
52.2
104
70-135
Ethylbenzene
ug/L
50
49.3
99
70-130
Hexachloro-1,3-butadiene
ug/L
50
52.4
105
68-132
m&p-Xylene
ug/L
100
97.9
98
70-130
Methyl-tert-butyl ether
ug/L
50
51.6
103
70-130
Methylene Chloride
ug/L
50
56.1
112
67-132
Naphthalene
ug/L
50
51.3
103
70-130
o-Xylene
ug/L
50
48.2
96
70-130
p-Isopropyltoluene
ug/L
50
48.9
98
70-130
Styrene
ug/L
50
49.0
98
70-130
Tetrachloroethene
ug/L
50
48.6
97
69-130
Toluene
ug/L
50
48.8
98
70-130
trans-1,2-Dichloroethene
ug/L
50
54.2
108
70-130
trans- 1,3-Dichloropropene
ug/L
50
51.7
103
70-130
Trichloroethene
ug/L
50
49.9
100
70-130
Trichlorofluoromethane
ug/L
50
45.0
90
63-130
Vinyl acetate
ug/L
100
108
108
55-143
Vinyl chloride
ug/L
50
51.2
102
70-131
Xylene (Total)
ug/L
150
146
97
70-130
1,2-Dichloroethane-d4 (S)
%
96
70-130
4-Bromofluorobenzene (S)
%
98
70-130
Toluene-d8 (S)
%
98
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 30 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2589476 2589477
MS MSD
92430807011 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
20
20
20.9
20.4
105
102
73-134 3
1,1,1-Trichloroethane
ug/L
ND
20
20
20.6
21.0
103
105
82-143 2
1,1,2,2-Tetrachloroethane
ug/L
ND
20
20
19.5
18.9
97
95
70-136 3
1,1,2-Trichloroethane
ug/L
ND
20
20
20.2
20.1
101
101
70-135 0
1,1-Dichloroethane
ug/L
ND
20
20
20.2
20.5
101
102
70-139 1
1,1-Dichloroethene
ug/L
ND
20
20
21.4
21.7
107
108
70-154 1
1,1-Dichloropropene
ug/L
ND
20
20
19.7
19.7
98
98
70-149 0
1,2,3-Trichlorobenzene
ug/L
ND
20
20
19.5
19.8
98
99
70-135 1
1,2,3-Trichloropropane
ug/L
ND
20
20
19.8
19.1
99
96
71-137 4
1,2,4-Trichlorobenzene
ug/L
ND
20
20
18.8
19.0
94
95
73-140 1
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
18.3
17.5
91
87
65-134 5
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
20.2
19.5
101
98
70-137 3
1,2-Dichlorobenzene
ug/L
ND
20
20
19.1
19.2
95
96
70-133 1
1,2-Dichloroethane
ug/L
ND
20
20
20.8
21.0
104
105
70-137 1
1,2-Dichloropropane
ug/L
ND
20
20
19.6
20.2
98
101
70-140 3
1,3-Dichlorobenzene
ug/L
ND
20
20
18.7
18.8
93
94
70-135 1
1,3-Dichloropropane
ug/L
ND
20
20
20.2
19.7
101
99
70-143 2
1,4-Dichlorobenzene
ug/L
ND
20
20
18.8
18.6
94
93
70-133 1
2,2-Dichloropropane
ug/L
ND
20
20
16.1
16.0
81
80
61-148 0
2-Butanone (MEK)
ug/L
ND
40
40
40.2
39.4
101
99
60-139 2
2-Chlorotoluene
ug/L
ND
20
20
18.8
18.8
94
94
70-144 0
2-Hexanone
ug/L
ND
40
40
39.5
37.8
99
95
65-138 4
4-Chlorotoluene
ug/L
ND
20
20
18.8
18.9
94
94
70-137 0
4-Methyl-2-pentanone (MIBK)
ug/L
ND
40
40
39.5
38.1
99
95
65-135 4
Acetone
ug/L
ND
40
40
46.9
47.3
117
118
60-148 1
Benzene
ug/L
ND
20
20
20.6
20.8
103
104
70-151 1
Bromobenzene
ug/L
ND
20
20
19.8
20.1
99
100
70-136 2
Bromochloromethane
ug/L
ND
20
20
23.7
23.8
119
119
70-141 0
Bromodichloromethane
ug/L
ND
20
20
19.4
19.7
97
98
70-138 1
Bromoform
ug/L
ND
20
20
17.7
17.2
89
86
63-130 3
Bromomethane
ug/L
ND
20
20
14.3
14.0
72
70
15-152 2
Carbon tetrachloride
ug/L
ND
20
20
20.1
20.0
100
100
70-143 0
Chlorobenzene
ug/L
ND
20
20
19.6
19.0
98
95
70-138 3
Chloroethane
ug/L
ND
20
20
20.1
21.9
100
110
52-163 9
Chloroform
ug/L
ND
20
20
20.7
20.4
103
102
70-139 1
Chloromethane
ug/L
ND
20
20
17.4
18.3
87
91
41-139 5
cis-1,2-Dichloroethene
ug/L
ND
20
20
20.1
20.4
101
102
70-141 1
cis-1,3-Dichloropropene
ug/L
ND
20
20
18.6
19.0
93
95
70-137 2
Dibromochloromethane
ug/L
ND
20
20
18.4
18.1
92
91
70-134 2
Dibromomethane
ug/L
ND
20
20
19.8
20.0
99
100
70-138 1
Dichlorodifluoromethane
ug/L
ND
20
20
19.2
19.0
96
95
47-155 1
Diisopropyl ether
ug/L
ND
20
20
19.5
20.3
98
102
63-144 4
Ethylbenzene
ug/L
ND
20
20
21.1
20.6
101
99
66-153 3
Hexachloro-1,3-butadiene
ug/L
ND
20
20
19.2
19.2
96
96
65-149 0
m&p-Xylene
ug/L
ND
40
40
40.6
40.1
99
98
69-152 1
Methyl-tert-butyl ether
ug/L
ND
20
20
19.8
20.7
99
103
54-156 4
Results presented on this page are in the units indicated
by the "Units"
column
except where
an alternate unit
is presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 31 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2589476
2589477
MS
MSD
92430807011
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Methylene Chloride
ug/L
ND
20
20
21.3
21.6
106
108
42-159
1
Naphthalene
ug/L
ND
20
20
20.0
19.1
100
96
61-148
5
o-Xylene
ug/L
ND
20
20
20.4
19.9
102
100
70-148
2
p-Isopropyltoluene
ug/L
ND
20
20
19.5
19.5
98
98
70-146
0
Styrene
ug/L
ND
20
20
19.2
19.6
96
98
70-135
2
Tetrachloroethene
ug/L
ND
20
20
19.8
19.1
99
95
59-143
4
Toluene
ug/L
ND
20
20
20.3
20.0
101
100
59-148
1
trans-1,2-Dichloroethene
ug/L
ND
20
20
20.7
20.5
103
103
70-146
1
trans- 1,3-Dichloropropene
ug/L
ND
20
20
18.7
18.9
93
94
70-135
1
Trichloroethene
ug/L
ND
20
20
20.7
20.2
103
101
70-147
2
Trichlorofluoromethane
ug/L
ND
20
20
19.9
20.4
99
102
70-148
2
Vinyl acetate
ug/L
ND
40
40
26.4
26.1
66
65
49-151
1
Vinyl chloride
ug/L
ND
20
20
20.5
20.7
102
104
70-156
1
Xylene (Total)
ug/L
ND
60
60
61.0
60.0
102
100
63-158
2
1,2-Dichloroethane-d4 (S)
%
96
96
70-130
4-Bromofluorobenzene (S)
%
101
99
70-130
Toluene-d8(S)
%
99
99
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 32 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
QC Batch: 479165 Analysis Method: EPA 8260B
QC Batch Method: EPA 8260E Analysis Description: 8260 MSV Low Level
Associated Lab Samples: 92430807010
METHOD BLANK: 2593249
Associated Lab Samples: 92430807010
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
1.0
06/05/19 17:25
1,1,1-Trichloroethane
ug/L
ND
1.0
06/05/19 17:25
1,1,2,2-Tetrachloroethane
ug/L
ND
1.0
06/05/19 17:25
1,1,2-Trichloroethane
ug/L
ND
1.0
06/05/19 17:25
1,1-Dichloroethane
ug/L
ND
1.0
06/05/19 17:25
1,1-Dichloroethene
ug/L
ND
1.0
06/05/19 17:25
1,1-Dichloropropene
ug/L
ND
1.0
06/05/19 17:25
1,2,3-Trichlorobenzene
ug/L
ND
1.0
06/05/19 17:25
1,2,3-Trichloropropane
ug/L
ND
1.0
06/05/19 17:25
1,2,4-Trichlorobenzene
ug/L
ND
1.0
06/05/19 17:25
1,2-Dibromo-3-chloropropane
ug/L
ND
5.0
06/05/19 17:25
1,2-Dibromoethane (EDB)
ug/L
ND
1.0
06/05/19 17:25
1,2-Dichlorobenzene
ug/L
ND
1.0
06/05/19 17:25
1,2-Dichloroethane
ug/L
ND
1.0
06/05/19 17:25
1,2-Dichloropropane
ug/L
ND
1.0
06/05/19 17:25
1,3-Dichlorobenzene
ug/L
ND
1.0
06/05/19 17:25
1,3-Dichloropropane
ug/L
ND
1.0
06/05/19 17:25
1,4-Dichlorobenzene
ug/L
ND
1.0
06/05/19 17:25
2,2-Dichloropropane
ug/L
ND
1.0
06/05/19 17:25
2-Butanone (MEK)
ug/L
ND
5.0
06/05/19 17:25
2-Chlorotoluene
ug/L
ND
1.0
06/05/19 17:25
2-Hexanone
ug/L
ND
5.0
06/05/19 17:25
4-Chlorotoluene
ug/L
ND
1.0
06/05/19 17:25
4-Methyl-2-pentanone (MIBK)
ug/L
ND
5.0
06/05/19 17:25
Acetone
ug/L
ND
25.0
06/05/19 17:25
Benzene
ug/L
ND
1.0
06/05/19 17:25
Bromobenzene
ug/L
ND
1.0
06/05/19 17:25
Bromochloromethane
ug/L
ND
1.0
06/05/19 17:25
Bromodichloromethane
ug/L
ND
1.0
06/05/19 17:25
Bromoform
ug/L
ND
1.0
06/05/19 17:25
Bromomethane
ug/L
ND
2.0
06/05/19 17:25
Carbon tetrachloride
ug/L
ND
1.0
06/05/19 17:25
Chlorobenzene
ug/L
ND
1.0
06/05/19 17:25
Chloroethane
ug/L
ND
1.0
06/05/19 17:25
Chloroform
ug/L
ND
5.0
06/05/19 17:25
Chloromethane
ug/L
ND
1.0
06/05/19 17:25
cis-1,2-Dichloroethene
ug/L
ND
1.0
06/05/19 17:25
cis-1,3-Dichloropropene
ug/L
ND
1.0
06/05/19 17:25
Dibromochloromethane
ug/L
ND
1.0
06/05/19 17:25
Dibromomethane
ug/L
ND
1.0
06/05/19 17:25
Dichlorodifluoromethane
ug/L
ND
1.0
06/05/19 17:25
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 33 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
METHOD BLANK: 2593249
Associated Lab Samples: 92430807010
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Diisopropyl ether
ug/L
ND
1.0
06/05/19 17:25
Ethylbenzene
ug/L
ND
1.0
06/05/19 17:25
Hexachloro-1,3-butadiene
ug/L
ND
1.0
06/05/19 17:25
m&p-Xylene
ug/L
ND
2.0
06/05/19 17:25
Methyl-tert-butyl ether
ug/L
ND
1.0
06/05/19 17:25
Methylene Chloride
ug/L
ND
5.0
06/05/19 17:25
Naphthalene
ug/L
ND
1.0
06/05/19 17:25
o-Xylene
ug/L
ND
1.0
06/05/19 17:25
p-Isopropyltoluene
ug/L
ND
1.0
06/05/19 17:25
Styrene
ug/L
ND
1.0
06/05/19 17:25
Tetrachloroethene
ug/L
ND
1.0
06/05/19 17:25
Toluene
ug/L
ND
1.0
06/05/19 17:25
trans-1,2-Dichloroethene
ug/L
ND
1.0
06/05/19 17:25
trans- 1,3-Dichloropropene
ug/L
ND
1.0
06/05/19 17:25
Trichloroethene
ug/L
ND
1.0
06/05/19 17:25
Trichlorofluoromethane
ug/L
ND
1.0
06/05/19 17:25
Vinyl acetate
ug/L
ND
2.0
06/05/19 17:25
Vinyl chloride
ug/L
ND
1.0
06/05/19 17:25
Xylene (Total)
ug/L
ND
1.0
06/05/19 17:25
1,2-Dichloroethane-d4 (S)
%
98
70-130
06/05/19 17:25
4-Bromofluorobenzene (S)
%
101
70-130
06/05/19 17:25
Toluene-d8 (S)
%
100
70-130
06/05/19 17:25
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2593250
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2-Tetrachloroethane
ug/L
50
48.8
98
70-130
1,1,1-Trichloroethane
ug/L
50
44.7
89
70-130
1,1,2,2-Tetrachloroethane
ug/L
50
43.8
88
70-130
1,1,2-Trichloroethane
ug/L
50
45.2
90
70-130
1,1-Dichloroethane
ug/L
50
45.4
91
70-130
1,1-Dichloroethene
ug/L
50
47.3
95
70-130
1,1-Dichloropropene
ug/L
50
42.3
85
70-130
1,2,3-Trichlorobenzene
ug/L
50
49.0
98
70-130
1,2,3-Trichloropropane
ug/L
50
46.2
92
70-130
1,2,4-Trichlorobenzene
ug/L
50
47.7
95
70-130
1,2-Dibromo-3-chloropropane
ug/L
50
50.1
100
70-130
1,2-Dibromoethane (EDB)
ug/L
50
46.1
92
70-130
1,2-Dichlorobenzene
ug/L
50
45.3
91
70-130
1,2-Dichloroethane
ug/L
50
42.5
85
70-130
1,2-Dichloropropane
ug/L
50
44.3
89
70-130
1,3-Dichlorobenzene
ug/L
50
44.6
89
70-130
1,3-Dichloropropane
ug/L
50
45.3
91
70-131
1,4-Dichlorobenzene
ug/L
50
44.2
88
70-130
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
LABORATORY CONTROL SAMPLE:
Parameter
2593250
Units
Spike
Conc.
2,2-Dichloropropane
ug/L
50
2-Butanone (MEK)
ug/L
100
2-Chlorotoluene
ug/L
50
2-Hexanone
ug/L
100
4-Chlorotoluene
ug/L
50
4-Methyl-2-pentanone (MIBK)
ug/L
100
Acetone
ug/L
100
Benzene
ug/L
50
Bromobenzene
ug/L
50
Bromochloromethane
ug/L
50
Bromodichloromethane
ug/L
50
Bromoform
ug/L
50
Bromomethane
ug/L
50
Carbon tetrachloride
ug/L
50
Chlorobenzene
ug/L
50
Chloroethane
ug/L
50
Chloroform
ug/L
50
Chloromethane
ug/L
50
cis-1,2-Dichloroethene
ug/L
50
cis-1,3-Dichloropropene
ug/L
50
Dibromochloromethane
ug/L
50
Dibromomethane
ug/L
50
Dichlorodifluoromethane
ug/L
50
Diisopropyl ether
ug/L
50
Ethylbenzene
ug/L
50
Hexachloro-1,3-butadiene
ug/L
50
m&p-Xylene
ug/L
100
Methyl-tert-butyl ether
ug/L
50
Methylene Chloride
ug/L
50
Naphthalene
ug/L
50
o-Xylene
ug/L
50
p-Isopropyltoluene
ug/L
50
Styrene
ug/L
50
Tetrachloroethene
ug/L
50
Toluene
ug/L
50
trans-1,2-Dichloroethene
ug/L
50
trans- 1,3-Dichloropropene
ug/L
50
Trichloroethene
ug/L
50
Trichlorofluoromethane
ug/L
50
Vinyl acetate
ug/L
100
Vinyl chloride
ug/L
50
Xylene (Total)
ug/L
150
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene-d8 (S)
%
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
46.3
93
69-130
89.0
89
64-135
44.8
90
70-130
97.0
97
66-135
45.1
90
70-130
92.5
93
70-130
108
108
61-157
44.6
89
70-130
46.2
92
70-130
42.9
86
70-130
46.4
93
70-130
48.6
97
70-130
71.1
142
38-130 L1
46.0
92
70-130
43.1
86
70-130
57.6
115
37-142
43.4
87
70-130
49.4
99
48-130
44.7
89
70-130
47.2
94
70-130
47.6
95
70-130
43.9
88
70-130
54.3
109
53-134
45.8
92
70-135
45.0
90
70-130
48.7
97
68-132
89.7
90
70-130
45.6
91
70-130
42.4
85
67-132
47.3
95
70-130
45.5
91
70-130
46.5
93
70-130
44.8
90
70-130
45.2
90
69-130
43.0
86
70-130
45.1
90
70-130
47.2
94
70-130
44.9
90
70-130
49.8
100
63-130
99.9
100
55-143
51.6
103
70-131
135
90
70-130
100
70-130
102
70-130
100
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 35 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2593251
2593252
MS
MSD
92430807010
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
1,1,1,2-Tetrachloroethane
ug/L
ND
2000
2000
2150
2150
107
108
73-134
0
1,1,1-Trichloroethane
ug/L
ND
2000
2000
2240
2210
112
111
82-143
1
1,1,2,2-Tetrachloroethane
ug/L
ND
2000
2000
1980
1970
99
98
70-136
1
1,1,2-Trichloroethane
ug/L
ND
2000
2000
2080
2070
104
103
70-135
1
1,1-Dichloroethane
ug/L
ND
2000
2000
2240
2210
112
111
70-139
1
1,1-Dichloroethene
ug/L
ND
2000
2000
2380
2370
119
119
70-154
0
1,1-Dichloropropene
ug/L
ND
2000
2000
2150
2110
108
106
70-149
2
1,2,3-Trichlorobenzene
ug/L
ND
2000
2000
2250
2150
113
108
70-135
5
1,2,3-Trichloropropane
ug/L
ND
2000
2000
2180
2120
109
106
71-137
3
1,2,4-Trichlorobenzene
ug/L
ND
2000
2000
2090
2140
104
107
73-140
2
1,2-Dibromo-3-chloropropane
ug/L
ND
2000
2000
2160
2090
108
104
65-134
3
1,2-Dibromoethane (EDB)
ug/L
ND
2000
2000
2110
2050
105
102
70-137
3
1,2-Dichlorobenzene
ug/L
ND
2000
2000
2090
2080
105
104
70-133
0
1,2-Dichloroethane
ug/L
ND
2000
2000
2010
2000
101
100
70-137
1
1,2-Dichloropropane
ug/L
ND
2000
2000
2150
2170
108
109
70-140
1
1,3-Dichlorobenzene
ug/L
ND
2000
2000
2150
2090
108
104
70-135
3
1,3-Dichloropropane
ug/L
ND
2000
2000
2080
2070
104
104
70-143
1
1,4-Dichlorobenzene
ug/L
ND
2000
2000
2150
2070
107
103
70-133
4
2,2-Dichloropropane
ug/L
ND
2000
2000
2250
2230
113
112
61-148
1
2-Butanone (MEK)
ug/L
ND
4000
4000
4030
3790
101
95
60-139
6
2-Chlorotoluene
ug/L
ND
2000
2000
2360
2340
118
117
70-144
1
2-Hexanone
ug/L
ND
4000
4000
4170
4100
104
103
65-138
2
4-Chlorotoluene
ug/L
ND
2000
2000
2170
2140
109
107
70-137
2
4-Methyl-2-pentanone (MIBK)
ug/L
ND
4000
4000
4200
4100
102
100
65-135
3
Acetone
ug/L
ND
4000
4000
4190
4190
105
105
60-148
0
Benzene
ug/L
237
2000
2000
2430
2400
110
108
70-151
1
Bromobenzene
ug/L
ND
2000
2000
2120
2190
106
109
70-136
3
Bromochloromethane
ug/L
ND
2000
2000
2130
2040
107
102
70-141
4
Bromodichloromethane
ug/L
ND
2000
2000
2160
2210
108
110
70-138
2
Bromoform
ug/L
ND
2000
2000
1910
1900
95
95
63-130
0
Bromomethane
ug/L
ND
2000
2000
1790
1790
89
90
15-152
0
Carbon tetrachloride
ug/L
ND
2000
2000
2210
2160
110
108
70-143
2
Chlorobenzene
ug/L
ND
2000
2000
2110
2100
106
105
70-138
1
Chloroethane
ug/L
ND
2000
2000
2520
2350
126
118
52-163
7
Chloroform
ug/L
ND
2000
2000
2190
2200
109
110
70-139
0
Chloromethane
ug/L
ND
2000
2000
2110
2180
106
109
41-139
3
cis-1,2-Dichloroethene
ug/L
ND
2000
2000
2230
2180
111
109
70-141
2
cis-1,3-Dichloropropene
ug/L
ND
2000
2000
2210
2090
111
105
70-137
6
Dibromochloromethane
ug/L
ND
2000
2000
2010
1990
101
99
70-134
1
Dibromomethane
ug/L
ND
2000
2000
2030
2000
101
100
70-138
1
Dichlorodifluoromethane
ug/L
ND
2000
2000
2190
2170
110
108
47-155
1
Diisopropyl ether
ug/L
ND
2000
2000
2180
2180
109
109
63-144
0
Ethylbenzene
ug/L
5350
2000
2000
6690
6650
67
65
66-153
1 M1
Hexachloro-1,3-butadiene
ug/L
ND
2000
2000
2060
2120
103
106
65-149
3
m&p-Xylene
ug/L
19100
4000
4000
19700
19700
14
15
69-152
0 M1
Methyl-tert-butyl ether
ug/L
ND
2000
2000
2160
2090
108
104
54-156
4
Results presented on this page are in
the units indicated by the
"Units" column except where
an alternate unit is presented
to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 36 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
2593251
2593252
MS
MSD
92430807010
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Methylene Chloride
ug/L
ND
2000
2000
2230
2190
112
110
42-159
2
Naphthalene
ug/L
756
2000
2000
2800
2740
102
99
61-148
2
o-Xylene
ug/L
7590
2000
2000
8520
8500
47
46
70-148
0 M1
p-Isopropyltoluene
ug/L
ND
2000
2000
2300
2280
115
114
70-146
1
Styrene
ug/L
ND
2000
2000
2120
2140
106
107
70-135
1
Tetrachloroethene
ug/L
ND
2000
2000
2110
2170
106
108
59-143
2
Toluene
ug/L
615
2000
2000
2610
2620
100
100
59-148
1
trans-1,2-Dichloroethene
ug/L
ND
2000
2000
2240
2250
112
112
70-146
0
trans- 1,3-Dichloropropene
ug/L
ND
2000
2000
2020
2050
101
102
70-135
1
Trichloroethene
ug/L
ND
2000
2000
2090
2120
105
106
70-147
1
Trichlorofluoromethane
ug/L
ND
2000
2000
2290
2340
114
117
70-148
2
Vinyl acetate
ug/L
ND
4000
4000
4550
4510
114
113
49-151
1
Vinyl chloride
ug/L
ND
2000
2000
2380
2330
119
116
70-156
2
Xylene(Total)
ug/L
26700
6000
6000
28200
28200
25
25
63-158
0 MS
1,2-Dichloroethane-d4 (S)
%
101
99
70-130
4-Bromofluorobenzene (S)
%
101
97
70-130
Toluene-d8(S)
%
101
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC.
Page 37 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
QC Batch: 477980 Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 3546 Analysis Description: 8015 Solid GCSV
Associated Lab Samples: 92430807001, 92430807002, 92430807003, 92430807004, 92430807005, 92430807006, 92430807007
METHOD BLANK: 2587783 Matrix: Solid
Associated Lab Samples: 92430807001, 92430807002, 92430807003, 92430807004, 92430807005, 92430807006, 92430807007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Diesel Range Organics(C10-C28) mg/kg ND 5.1 06/01/19 10:34
n-Pentacosane (S) % 61 33-129 06/01/19 10:34
LABORATORY CONTROL SAMPLE: 2587784
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Diesel Range Organics(C10-C28) mg/kg 67.3 50.9 76 43-130
n-Pentacosane (S) % 65 33-129
MATRIX SPIKE SAMPLE:
Parameter
2587785
Units
92430734011
Result
Spike MS MS
Conc. Result % Rec
% Rec
Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
6.9
70.3 55.6 69
10-130
n-Pentacosane(S)
%
55
33-129
SAMPLE DUPLICATE: 2587792
92430796001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
1100
901 20
n-Pentacosane(S)
%
168
317 S2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC.
Page 38 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
QC Batch: 478681 Analysis Method: EPA 8015C Modified
QC Batch Method: EPA 3546 Analysis Description: 8015 Solid GCSV
Associated Lab Samples: 92430807013
METHOD BLANK: 2591077 Matrix: Solid
Associated Lab Samples: 92430807013
Blank Reporting
Parameter Units Result Limit Analyzed
Diesel Range Organics(C10-C28) mg/kg ND 5.0 06/04/19 11:17
n-Pentacosane (S) % 89 33-129 06/04/19 11:17
Qualifiers
LABORATORY CONTROL SAMPLE:
2591078
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
66.4 55.9
84
43-130
n-Pentacosane (S)
%
83
33-129
MATRIX SPIKE SAMPLE:
2591079
92430734015 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Diesel Range Organics(C10-C28)
mg/kg
ND 69.5
35.3
49 10-130
n-Pentacosane(S)
%
49 33-129
SAMPLE DUPLICATE: 2591080
Parameter
Diesel Range Organics(C10-C28)
n-Pentacosane (S)
92430734015 Dup
Units Result Result
mg/kg ND ND
% 75 81
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 39 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
QC Batch: 478680 Analysis Method: EPA 8082A
QC Batch Method: EPA 3546 Analysis Description: 8082 GCS PCB
Associated Lab Samples: 92430807002, 92430807013
METHOD BLANK: 2591075
Matrix:
Solid
Associated Lab Samples:
92430807002, 92430807013
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
PCB-1016 (Aroclor 1016)
ug/kg
ND
33.3
06/03/19 19:08
PCB-1221 (Aroclor 1221)
ug/kg
ND
33.3
06/03/19 19:08
PCB-1232 (Aroclor 1232)
ug/kg
ND
33.3
06/03/19 19:08
PCB-1242 (Aroclor 1242)
ug/kg
ND
33.3
06/03/19 19:08
PCB-1248 (Aroclor 1248)
ug/kg
ND
33.3
06/03/19 19:08
PCB-1254 (Aroclor 1254)
ug/kg
ND
33.3
06/03/19 19:08
PCB-1260 (Aroclor 1260)
ug/kg
ND
33.3
06/03/19 19:08
Decachlorobiphenyl (S)
%
93
10-130
06/03/19 19:08
LABORATORY CONTROL SAMPLE:
2591076
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
PCB-1016 (Aroclor 1016)
ug/kg
164
125 76 35-130
PCB-1260 (Aroclor 1260)
ug/kg
164
140 85 46-130
Decachlorobiphenyl (S)
%
87 10-130
MATRIX SPIKE SAMPLE:
Parameter
2591090
Units
92430807013
Result
Spike MS
Conc. Result
MS
% Rec
% Rec
Limits Qualifiers
PCB-1016 (Aroclor 1016)
ug/kg
ND
184 116
63
10-130
PCB-1260 (Aroclor 1260)
ug/kg
ND
184 127
69
10-130
Decachlorobiphenyl (S)
%
75
10-130
SAMPLE DUPLICATE: 2591091
92430508001
Dup
Parameter
Units
Result
Result RPD
Qualifiers
PCB-1016 (Aroclor 1016)
ug/kg
ND
ND
PCB-1221 (Aroclor 1221)
ug/kg
ND
ND
PCB-1232 (Aroclor 1232)
ug/kg
ND
ND
PCB-1242 (Aroclor 1242)
ug/kg
ND
ND
PCB-1248 (Aroclor 1248)
ug/kg
ND
ND
PCB-1254 (Aroclor 1254)
ug/kg
ND
ND
PCB-1260 (Aroclor 1260)
ug/kg
ND
ND
Decachlorobiphenyl (S)
%
31
41
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC.
Page 40 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
QC Batch: 478179 Analysis Method: EPA 8270D
QC Batch Method: EPA 3546 Analysis Description: 8270 Solid MSSV Microwave
Associated Lab Samples: 92430807008
METHOD BLANK: 2588722
Associated Lab Samples: 92430807008
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
1,2,4-Trichlorobenzene
ug/kg
ND
327
05/31/19 13:09
1,2-Dichlorobenzene
ug/kg
ND
327
05/31/19 13:09
1,3-Dichlorobenzene
ug/kg
ND
327
05/31/19 13:09
1,4-Dichlorobenzene
ug/kg
ND
327
05/31/19 13:09
1-Methylnaphthalene
ug/kg
ND
327
05/31/19 13:09
2,2'-Oxybis(1-chloropropane)
ug/kg
ND
327
05/31/19 13:09
2,4,5-Trichlorophenol
ug/kg
ND
327
05/31/19 13:09
2,4,6-Trichlorophenol
ug/kg
ND
327
05/31/19 13:09
2,4-Dichlorophenol
ug/kg
ND
327
05/31/19 13:09
2,4-Dimethylphenol
ug/kg
ND
327
05/31/19 13:09
2,4-Dinitrophenol
ug/kg
ND
1630
05/31/19 13:09
2,4-Dinitrotoluene
ug/kg
ND
327
05/31/19 13:09
2,6-Dinitrotoluene
ug/kg
ND
327
05/31/19 13:09
2-Chloronaphthalene
ug/kg
ND
327
05/31/19 13:09
2-Chlorophenol
ug/kg
ND
327
05/31/19 13:09
2-Methylnaphthalene
ug/kg
ND
327
05/31/19 13:09
2-Methylphenol(o-Cresol)
ug/kg
ND
327
05/31/19 13:09
2-Nitroaniline
ug/kg
ND
1630
05/31/19 13:09
2-Nitrophenol
ug/kg
ND
327
05/31/19 13:09
3&4-Methyl phenol (m&p Cresol)
ug/kg
ND
327
05/31/19 13:09
3,3'-Dichlorobenzidine
ug/kg
ND
1630
05/31/19 13:09
3-Nitroaniline
ug/kg
ND
1630
05/31/19 13:09
4,6-Dinitro-2-methyl phenol
ug/kg
ND
653
05/31/19 13:09
4-Bromophenylphenyl ether
ug/kg
ND
327
05/31/19 13:09
4-ChIoro-3-methyl phenol
ug/kg
ND
653
05/31/19 13:09
4-Chloroaniline
ug/kg
ND
1630
05/31/19 13:09
4-Chlorophenylphenyl ether
ug/kg
ND
327
05/31/19 13:09
4-Nitroaniline
ug/kg
ND
653
05/31/19 13:09
4-Nitrophenol
ug/kg
ND
1630
05/31/19 13:09
Acenaphthene
ug/kg
ND
327
05/31/19 13:09
Acenaphthylene
ug/kg
ND
327
05/31/19 13:09
Aniline
ug/kg
ND
327
05/31/19 13:09
Anthracene
ug/kg
ND
327
05/31/19 13:09
Benzo(a)anthracene
ug/kg
ND
327
05/31/19 13:09
Benzo(a)pyrene
ug/kg
ND
327
05/31/19 13:09
Benzo(b)fluoranthene
ug/kg
ND
327
05/31/19 13:09
Benzo(g,h,i)perylene
ug/kg
ND
327
05/31/19 13:09
Benzo(k)fluoranthene
ug/kg
ND
327
05/31/19 13:09
Benzoic Acid
ug/kg
ND
1630
05/31/19 13:09
Benzyl alcohol
ug/kg
ND
653
05/31/19 13:09
bis(2-Chloroethoxy)methane
ug/kg
ND
327
05/31/19 13:09
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
METHOD BLANK: 2588722
Associated Lab Samples: 92430807008
Parameter
Units
Matrix:
Blank
Result
Solid
Reporting
Limit
Analyzed
bis(2-Chloroethyl) ether
ug/kg
ND
327
05/31/19 13:09
bis(2-Ethylhexyl)phthalate
ug/kg
ND
327
05/31/19 13:09
Butylbenzylphthalate
ug/kg
ND
327
05/31/19 13:09
Chrysene
ug/kg
ND
327
05/31/19 13:09
Di-n-butylphthalate
ug/kg
ND
327
05/31/19 13:09
Di-n-octylphthalate
ug/kg
ND
327
05/31/19 13:09
Dibenz(a,h)anthracene
ug/kg
ND
327
05/31/19 13:09
Dibenzofuran
ug/kg
ND
327
05/31/19 13:09
Diethylphthalate
ug/kg
ND
327
05/31/19 13:09
Dimethylphthalate
ug/kg
ND
327
05/31/19 13:09
Fluoranthene
ug/kg
ND
327
05/31/19 13:09
Fluorene
ug/kg
ND
327
05/31/19 13:09
Hexachloro-1,3-butadiene
ug/kg
ND
327
05/31/19 13:09
Hexachlorobenzene
ug/kg
ND
327
05/31/19 13:09
Hexachlorocyclopentadiene
ug/kg
ND
327
05/31/19 13:09
Hexachloroethane
ug/kg
ND
327
05/31/19 13:09
Indeno(1,2,3-cd)pyrene
ug/kg
ND
327
05/31/19 13:09
Isophorone
ug/kg
ND
327
05/31/19 13:09
N-Nitroso-di-n-propylamine
ug/kg
ND
327
05/31/19 13:09
N-Nitrosodimethylamine
ug/kg
ND
327
05/31/19 13:09
N-Nitrosodiphenylamine
ug/kg
ND
327
05/31/19 13:09
Naphthalene
ug/kg
ND
327
05/31/19 13:09
Nitrobenzene
ug/kg
ND
327
05/31/19 13:09
Pentachlorophenol
mg/kg
ND
1.6
05/31/19 13:09
Phenanthrene
ug/kg
ND
327
05/31/19 13:09
Phenol
ug/kg
ND
327
05/31/19 13:09
Pyrene
ug/kg
ND
327
05/31/19 13:09
2,4,6-Tribromophenol (S)
%
73
27-110
05/31/19 13:09
2-Fluorobiphenyl (S)
%
78
30-110
05/31/19 13:09
2-Fluorophenol(S)
%
79
13-110
05/31/19 13:09
Nitrobenzene-d5 (S)
%
78
23-110
05/31/19 13:09
Phenol-d6 (S)
%
75
22-110
05/31/19 13:09
Terphenyl-d14 (S)
%
86
28-110
05/31/19 13:09
Qualifiers
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
2588723
Units
Spike
Conc.
2588724
LCS LCSD
Result Result
LCS
% Rec
LCSD
% Rec
% Rec
Limits
RPD
Max
RPD Qualifiers
1,2,4-Trichlorobenzene
ug/kg
1660
1350
1210
81
74
52-130
11
30
1,2-Dichlorobenzene
ug/kg
1660
1350
1160
81
71
51-130
15
30
1,3-Dichlorobenzene
ug/kg
1660
1320
1200
80
73
50-130
10
30
1,4-Dichlorobenzene
ug/kg
1660
1310
1230
79
75
49-130
7
30
1-Methylnaphthalene
ug/kg
1660
1390
1250
84
76
55-130
11
30
2,2'-Oxybis(1-chloropropane)
ug/kg
1660
1460
1310
88
80
30-130
11
30
2,4,5-Trichlorophenol
ug/kg
1660
1390
1260
84
77
55-130
10
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 42 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
LABORATORY CONTROL SAMPLE & LCSD:
2588723
2588724
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
2,4,6-TrichIorophenol
ug/kg
1660
1420
1310
86
80
57-130
8
30
2,4-DichIorophenol
ug/kg
1660
1370
1230
83
75
56-130
11
30
2,4-Dimethylphenol
ug/kg
1660
1400
1270
84
77
51-130
10
30
2,4-Dinitrophenol
ug/kg
8310
7300
6690
88
82
27-133
9
30
2,4-Dinitrotoluene
ug/kg
1660
1310
1240
79
75
61-130
6
30
2,6-Dinitrotoluene
ug/kg
1660
1370
1290
83
79
60-130
6
30
2-Chloronaphthalene
ug/kg
1660
1360
1250
82
76
52-130
9
30
2-Chlorophenol
ug/kg
1660
1440
1290
87
79
54-130
11
30
2-Methylnaphthalene
ug/kg
1660
1430
1280
86
78
54-130
11
30
2-Methylphenol(o-Cresol)
ug/kg
1660
1420
1290
86
78
51-130
10
30
2-Nitroaniline
ug/kg
3320
2780
2560
84
78
51-130
8
30
2-Nitrophenol
ug/kg
1660
1440
1270
87
78
49-130
12
30
3&4-Methyl phenol (m&p Cresol)
ug/kg
1660
1370
1250
82
77
11-163
9
30
3,3'-Dichlorobenzidine
ug/kg
3320
2400
2280
72
70
10-132
5
30
3-Nitroaniline
ug/kg
3320
2510
2340
75
71
55-130
7
30
4,6-Dinitro-2-methyl phenol
ug/kg
3320
2960
2740
89
84
47-142
8
30
4-Bromophenylphenyl ether
ug/kg
1660
1250
1160
75
70
59-130
8
30
4-Chloro-3-methylphenol
ug/kg
3320
2790
2520
84
77
55-130
10
30
4-Chloroaniline
ug/kg
3320
2710
2460
82
75
54-130
10
30
4-Chlorophenylphenyl ether
ug/kg
1660
1380
1220
83
74
58-130
13
30
4-Nitroaniline
ug/kg
3320
2650
2510
80
76
54-130
6
30
4-Nitrophenol
ug/kg
8310
6520
6180
78
75
48-130
5
30
Acenaphthene
ug/kg
1660
1440
1290
87
79
60-130
11
30
Acenaphthylene
ug/kg
1660
1480
1290
89
79
60-130
14
30
Aniline
ug/kg
1660
1270
1130
77
69
43-130
12
30
Anthracene
ug/kg
1660
1420
1270
86
78
63-130
11
30
Benzo(a)anthracene
ug/kg
1660
1500
1380
90
84
59-130
8
30
Benzo(a)pyrene
ug/kg
1660
1450
1310
88
80
57-130
11
30
Benzo(b)fluoranthene
ug/kg
1660
1430
1310
86
80
54-130
8
30
Benzo(g,h,i)perylene
ug/kg
1660
1410
1260
85
77
59-130
11
30
Benzo(k)fluoranthene
ug/kg
1660
1410
1310
85
80
54-130
7
30
Benzoic Acid
ug/kg
8310
5830
5310
70
65
19-130
9
30
Benzyl alcohol
ug/kg
3320
2790
2440
84
75
50-130
13
30
bis(2-Chloroethoxy)methane
ug/kg
1660
1360
1220
82
74
54-130
11
30
bis(2-Chloroethyl) ether
ug/kg
1660
1330
1200
80
73
48-130
10
30
bis(2-Ethylhexyl)phthalate
ug/kg
1660
1400
1300
84
79
45-134
8
30
Butylbenzylphthalate
ug/kg
1660
1420
1320
85
81
46-138
7
30
Ch rysene
ug/kg
1660
1390
1310
84
80
58-130
6
30
Di-n-butylphthalate
ug/kg
1660
1320
1200
79
73
60-130
9
30
Di-n-octylphthalate
ug/kg
1660
1390
1300
84
79
53-130
7
30
Dibenz(a,h)anthracene
ug/kg
1660
1430
1290
86
79
59-130
10
30
Dibenzofuran
ug/kg
1660
1370
1250
83
76
60-130
9
30
Diethylphthalate
ug/kg
1660
1360
1260
82
77
60-130
7
30
Dimethylphthalate
ug/kg
1660
1380
1260
83
77
60-130
9
30
Fluoranthene
ug/kg
1660
1450
1320
87
81
65-130
9
30
Fluorene
ug/kg
1660
1390
1240
84
75
63-130
12
30
Hexachloro-1,3-butadiene
ug/kg
1660
1380
1240
83
75
46-130
11
30
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 43 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
LABORATORY CONTROL SAMPLE & LCSD:
2588723
2588724
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
Hexachlorobenzene
ug/kg
1660
1250
1120
75
68
58-130
11
30
Hexachlorocyclopentadiene
ug/kg
1660
1330
1180
80
72
23-130
12
30
Hexachloroethane
ug/kg
1660
1320
1170
79
71
47-130
12
30
Indeno(1,2,3-cd)pyrene
ug/kg
1660
1420
1300
86
79
60-130
9
30
Isophorone
ug/kg
1660
1310
1170
79
72
49-130
11
30
N-Nitroso-di-n-propylamine
ug/kg
1660
1290
1140
77
70
47-130
12
30
N-Nitrosodimethylamine
ug/kg
1660
1350
1220
81
75
45-130
10
30
N-Nitrosodiphenylamine
ug/kg
1660
1360
1260
82
77
59-130
8
30
Naphthalene
ug/kg
1660
1430
1310
86
80
55-130
9
30
Nitrobenzene
ug/kg
1660
1320
1200
80
73
49-130
9
30
Pentachlorophenol
mg/kg
3.3
2.3
2.0
69
62
10-132
12
30
Phenanthrene
ug/kg
1660
1400
1230
84
75
62-130
13
30
Phenol
ug/kg
1660
1400
1250
84
76
46-130
12
30
Pyrene
ug/kg
1660
1540
1450
93
88
53-130
6
30
2,4,6-Tribromophenol (S)
%
70
64
27-110
2-Fluorobiphenyl (S)
%
76
69
30-110
2-Fluorophenol(S)
%
83
74
13-110
Nitrobenzene-d5(S)
%
80
71
23-110
Phenol-d6 (S)
%
81
72
22-110
Terphenyl-d14(S)
%
79
73
28-110
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 44 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
QC Batch: 478153 Analysis Method: EPA 8270D
QC Batch Method: EPA 3510C Analysis Description: 8270 Water MSSV RVE
Associated Lab Samples: 92430807009, 92430807010, 92430807011, 92430807012
METHOD BLANK: 2588581 Matrix: Water
Associated Lab Samples: 92430807009, 92430807010, 92430807011, 92430807012
Blank Reporting
Parameter Units Result Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
10.0
05/30/19 15:05
1,2-Dichlorobenzene
ug/L
ND
10.0
05/30/19 15:05
1,3-Dichlorobenzene
ug/L
ND
10.0
05/30/19 15:05
1,4-Dichlorobenzene
ug/L
ND
10.0
05/30/19 15:05
1-Methylnaphthalene
ug/L
ND
10.0
05/30/19 15:05
2,2'-Oxybis(1-chloropropane)
ug/L
ND
10.0
05/30/19 15:05
2,4,5-Trichlorophenol
ug/L
ND
10.0
05/30/19 15:05
2,4,6-Trichlorophenol
ug/L
ND
10.0
05/30/19 15:05
2,4-Dichlorophenol
ug/L
ND
10.0
05/30/19 15:05
2,4-Dimethylphenol
ug/L
ND
10.0
05/30/19 15:05
2,4-Dinitrophenol
ug/L
ND
50.0
05/30/19 15:05
2,4-Dinitrotoluene
ug/L
ND
10.0
05/30/19 15:05
2,6-Dinitrotoluene
ug/L
ND
10.0
05/30/19 15:05
2-Chloronaphthalene
ug/L
ND
10.0
05/30/19 15:05
2-Chlorophenol
ug/L
ND
10.0
05/30/19 15:05
2-Methylnaphthalene
ug/L
ND
10.0
05/30/19 15:05
2-Methylphenol(o-Cresol)
ug/L
ND
10.0
05/30/19 15:05
2-Nitroaniline
ug/L
ND
50.0
05/30/19 15:05
2-Nitrophenol
ug/L
ND
10.0
05/30/19 15:05
3&4-Methyl phenol (m&p Cresol)
ug/L
ND
10.0
05/30/19 15:05
3,3'-Dichlorobenzidine
ug/L
ND
20.0
05/30/19 15:05
3-Nitroaniline
ug/L
ND
50.0
05/30/19 15:05
4,6-Dinitro-2-methyl phenol
ug/L
ND
20.0
05/30/19 15:05
4-Bromophenylphenyl ether
ug/L
ND
10.0
05/30/19 15:05
4-ChIoro-3-methyl phenol
ug/L
ND
20.0
05/30/19 15:05
4-Chloroaniline
ug/L
ND
20.0
05/30/19 15:05
4-Chlorophenylphenyl ether
ug/L
ND
10.0
05/30/19 15:05
4-Nitroaniline
ug/L
ND
20.0
05/30/19 15:05
4-Nitrophenol
ug/L
ND
50.0
05/30/19 15:05
Acenaphthene
ug/L
ND
10.0
05/30/19 15:05
Acenaphthylene
ug/L
ND
10.0
05/30/19 15:05
Aniline
ug/L
ND
10.0
05/30/19 15:05
Anthracene
ug/L
ND
10.0
05/30/19 15:05
Benzo(a)anthracene
ug/L
ND
10.0
05/30/19 15:05
Benzo(a)pyrene
ug/L
ND
10.0
05/30/19 15:05
Benzo(b)fluoranthene
ug/L
ND
10.0
05/30/19 15:05
Benzo(g,h,i)perylene
ug/L
ND
10.0
05/30/19 15:05
Benzo(k)fluoranthene
ug/L
ND
10.0
05/30/19 15:05
Benzoic Acid
ug/L
ND
50.0
05/30/19 15:05
Benzyl alcohol
ug/L
ND
20.0
05/30/19 15:05
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
05/30/19 15:05
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 45 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
METHOD BLANK: 2588581 Matrix: Water
Associated Lab Samples: 92430807009, 92430807010, 92430807011, 92430807012
Blank Reporting
Parameter Units Result Limit
Analyzed
bis(2-Chloroethyl) ether
ug/L
ND
10.0
05/30/19 15:05
bis(2-Ethylhexyl)phthalate
ug/L
ND
6.0
05/30/19 15:05
Butylbenzylphthalate
ug/L
ND
10.0
05/30/19 15:05
Chrysene
ug/L
ND
10.0
05/30/19 15:05
Di-n-butylphthalate
ug/L
ND
10.0
05/30/19 15:05
Di-n-octylphthalate
ug/L
ND
10.0
05/30/19 15:05
Dibenz(a,h)anthracene
ug/L
ND
10.0
05/30/19 15:05
Dibenzofuran
ug/L
ND
10.0
05/30/19 15:05
Diethylphthalate
ug/L
ND
10.0
05/30/19 15:05
Dimethylphthalate
ug/L
ND
10.0
05/30/19 15:05
Fluoranthene
ug/L
ND
10.0
05/30/19 15:05
Fluorene
ug/L
ND
10.0
05/30/19 15:05
Hexachloro-1,3-butadiene
ug/L
ND
10.0
05/30/19 15:05
Hexachlorobenzene
ug/L
ND
10.0
05/30/19 15:05
Hexachlorocyclopentadiene
ug/L
ND
10.0
05/30/19 15:05
Hexachloroethane
ug/L
ND
10.0
05/30/19 15:05
Indeno(1,2,3-cd)pyrene
ug/L
ND
10.0
05/30/19 15:05
Isophorone
ug/L
ND
10.0
05/30/19 15:05
N-Nitroso-di-n-propylamine
ug/L
ND
10.0
05/30/19 15:05
N-Nitrosodimethylamine
ug/L
ND
10.0
05/30/19 15:05
N-Nitrosodiphenylamine
ug/L
ND
10.0
05/30/19 15:05
Naphthalene
ug/L
ND
10.0
05/30/19 15:05
Nitrobenzene
ug/L
ND
10.0
05/30/19 15:05
Pentachlorophenol
ug/L
ND
25.0
05/30/19 15:05
Phenanthrene
ug/L
ND
10.0
05/30/19 15:05
Phenol
ug/L
ND
10.0
05/30/19 15:05
Pyrene
ug/L
ND
10.0
05/30/19 15:05
2,4,6-Tribromophenol (S)
%
89
10-137
05/30/19 15:05
2-Fluorobiphenyl (S)
%
78
13-130
05/30/19 15:05
2-Fluorophenol (S)
%
63
10-130
05/30/19 15:05
Nitrobenzene-d5 (S)
%
81
13-130
05/30/19 15:05
Phenol-d6 (S)
%
46
10-130
05/30/19 15:05
Terphenyl-d14 (S)
%
87
25-130
05/30/19 15:05
Qualifiers
LABORATORY CONTROL SAMPLE:
2588582
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
50
23.1
46
30-130
1,2-Dichlorobenzene
ug/L
50
25.3
51
30-130
1,3-Dichlorobenzene
ug/L
50
24.7
49
20-130
1,4-Dichlorobenzene
ug/L
50
25.0
50
30-130
1-Methylnaphthalene
ug/L
50
27.6
55
30-130
2,2'-Oxybis(1-chloropropane)
ug/L
50
22.3
45
20-130
2,4,5-Trichlorophenol
ug/L
50
28.8
58
40-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 46 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
LABORATORY CONTROL SAMPLE:
Parameter
2588582
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
2,4,6-TrichIorophenol
ug/L
50
29.2
58
40-130
2,4-DichIorophenol
ug/L
50
27.8
56
31-130
2,4-Dimethylphenol
ug/L
50
29.0
58
30-130
2,4-Dinitrophenol
ug/L
250
157
63
30-130
2,4-Dinitrotoluene
ug/L
50
39.8
80
49-130
2,6-Dinitrotoluene
ug/L
50
33.0
66
50-130
2-Chloronaphthalene
ug/L
50
24.8
50
30-130
2-Chlorophenol
ug/L
50
28.7
57
30-130
2-Methylnaphthalene
ug/L
50
27.9
56
30-130
2-Methylphenol(o-Cresol)
ug/L
50
30.0
60
30-130
2-Nitroaniline
ug/L
100
57.8
58
40-130
2-Nitrophenol
ug/L
50
27.1
54
20-130
3&4-Methyl phenol (m&p Cresol)
ug/L
50
24.7
49
20-130
3,3'-Dichlorobenzidine
ug/L
100
82.2
82
10-150
3-Nitroaniline
ug/L
100
76.1
76
40-130
4,6-Dinitro-2-methyl phenol
ug/L
100
84.7
85
40-130
4-Bromophenylphenyl ether
ug/L
50
32.3
65
30-130
4-Chloro-3-methylphenol
ug/L
100
57.9
58
30-130
4-Chloroaniline
ug/L
100
56.1
56
20-130
4-Chlorophenylphenyl ether
ug/L
50
29.1
58
20-130
4-Nitroaniline
ug/L
100
89.9
90
40-130
4-Nitrophenol
ug/L
250
128
51
10-130
Acenaphthene
ug/L
50
28.8
58
30-130
Acenaphthylene
ug/L
50
29.4
59
30-130
Aniline
ug/L
50
25.3
51
20-130
Anthracene
ug/L
50
41.8
84
50-130
Benzo(a)anthracene
ug/L
50
46.4
93
50-130
Benzo(a)pyrene
ug/L
50
45.7
91
50-130
Benzo(b)fluoranthene
ug/L
50
45.0
90
50-130
Benzo(g,h,i)perylene
ug/L
50
47.7
95
50-130
Benzo(k)fluoranthene
ug/L
50
45.4
91
50-130
Benzoic Acid
ug/L
250
ND
7
10-130 L2
Benzyl alcohol
ug/L
100
46.4
46
20-130
bis(2-Chloroethoxy)methane
ug/L
50
26.0
52
30-130
bis(2-Chloroethyl) ether
ug/L
50
27.2
54
30-130
bis(2-Ethylhexyl)phthalate
ug/L
50
44.5
89
50-130
Butylbenzylphthalate
ug/L
50
28.8
58
50-150
Chrysene
ug/L
50
42.1
84
50-130
Di-n-butylphthalate
ug/L
50
44.5
89
50-130
Di-n-octylphthalate
ug/L
50
45.5
91
50-130
Dibenz(a,h)anthracene
ug/L
50
47.6
95
40-130
Dibenzofuran
ug/L
50
28.4
57
40-130
Diethylphthalate
ug/L
50
39.6
79
40-130
Dimethylphthalate
ug/L
50
33.9
68
40-130
Fluoranthene
ug/L
50
48.6
97
30-130
Fluorene
ug/L
50
31.9
64
20-130
Hexachloro-1,3-butadiene
ug/L
50
22.7
45
10-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 47 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
LABORATORY CONTROL SAMPLE:
Parameter
2588582
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Hexachlorobenzene
ug/L
50
34.1
68
30-130
Hexachlorocyclopentadiene
ug/L
50
17.9
36
10-150
Hexachloroethane
ug/L
50
23.3
47
10-130
Indeno(1,2,3-cd)pyrene
ug/L
50
48.7
97
40-130
Isophorone
ug/L
50
26.5
53
30-130
N-Nitroso-di-n-propylamine
ug/L
50
26.8
54
30-130
N-Nitrosodimethylamine
ug/L
50
22.7
45
10-130
N-Nitrosodiphenylamine
ug/L
50
35.3
71
30-130
Naphthalene
ug/L
50
27.8
56
20-130
Nitrobenzene
ug/L
50
25.1
50
20-130
Pentachlorophenol
ug/L
100
77.7
78
10-140
Phenanthrene
ug/L
50
41.2
82
50-130
Phenol
ug/L
50
17.9
36
10-130
Pyrene
ug/L
50
44.1
88
50-130
2,4,6-Tribromophenol (S)
%
81
10-137
2-Fluorobiphenyl (S)
%
55
13-130
2-Fluorophenol (S)
%
45
10-130
Nitrobenzene-d5 (S)
%
56
13-130
Phenol-d6 (S)
%
33
10-130
Terphenyl-d14 (S)
%
85
25-130
MATRIX SPIKE SAMPLE:
Parameter
2588583
Units
92430807009
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,2,4-Trichlorobenzene
ug/L
ND
50
23.3
47
30-130
1,2-Dichlorobenzene
ug/L
ND
50
25.0
50
30-130
1,3-Dichlorobenzene
ug/L
ND
50
23.9
48
20-130
1,4-Dichlorobenzene
ug/L
ND
50
24.4
49
30-130
1-Methylnaphthalene
ug/L
ND
50
29.0
55
30-130
2,2'-Oxybis(1-chloropropane)
ug/L
ND
50
22.2
44
20-130
2,4,5-Trichlorophenol
ug/L
ND
50
29.3
59
40-130
2,4,6-Trichlorophenol
ug/L
ND
50
29.0
58
40-130
2,4-Dichlorophenol
ug/L
ND
50
29.3
59
31-130
2,4-Dimethylphenol
ug/L
ND
50
29.8
60
30-130
2,4-Dinitrophenol
ug/L
ND
250
187
75
30-130
2,4-Dinitrotoluene
ug/L
ND
50
39.3
79
49-130
2,6-Dinitrotoluene
ug/L
ND
50
33.0
66
50-130
2-Chloronaphthalene
ug/L
ND
50
24.6
49
30-130
2-Chlorophenol
ug/L
ND
50
28.8
58
30-130
2-Methylnaphthalene
ug/L
ND
50
29.7
55
30-130
2-Methylphenol(o-Cresol)
ug/L
ND
50
31.0
62
30-130
2-Nitroaniline
ug/L
ND
100
58.7
59
40-130
2-Nitrophenol
ug/L
ND
50
28.2
56
20-130
3&4-Methyl phenol (m&p Cresol)
ug/L
ND
50
25.5
51
20-130
3,3'-Dichlorobenzidine
ug/L
ND
100
75.0
75
10-150
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 48 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
MATRIX SPIKE SAMPLE:
2588583
92430807009
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
3-Nitroaniline
ug/L
ND
100
73.0
73
40-130
4,6-Dinitro-2-methyl phenol
ug/L
ND
100
86.4
86
40-130
4-Bromophenylphenyl ether
ug/L
ND
50
33.0
66
30-130
4-Chloro-3-methylphenol
ug/L
ND
100
60.4
60
30-130
4-Chloroaniline
ug/L
ND
100
55.7
56
20-130
4-Chlorophenylphenyl ether
ug/L
ND
50
28.8
58
20-130
4-Nitroaniline
ug/L
ND
100
85.7
86
40-130
4-Nitrophenol
ug/L
ND
250
137
55
10-130
Acenaphthene
ug/L
ND
50
28.5
57
30-130
Acenaphthylene
ug/L
ND
50
29.1
58
30-130
Aniline
ug/L
ND
50
24.5
49
20-130
Anthracene
ug/L
ND
50
41.8
84
50-130
Benzo(a)anthracene
ug/L
ND
50
45.2
90
50-130
Benzo(a)pyrene
ug/L
ND
50
45.8
92
50-130
Benzo(b)fluoranthene
ug/L
ND
50
45.5
91
50-130
Benzo(g,h,i)perylene
ug/L
ND
50
46.4
93
50-130
Benzo(k)fluoranthene
ug/L
ND
50
45.2
90
50-130
Benzoic Acid
ug/L
ND
250
74.2
30
10-130
Benzyl alcohol
ug/L
ND
100
49.3
49
20-130
bis(2-Chloroethoxy)methane
ug/L
ND
50
27.5
55
30-130
bis(2-Chloroethyl) ether
ug/L
ND
50
27.2
54
30-130
bis(2-Ethylhexyl)phthalate
ug/L
ND
50
43.9
88
50-130
Butylbenzylphthalate
ug/L
ND
50
26.5
53
50-150
Chrysene
ug/L
ND
50
40.7
81
50-130
Di-n-butylphthalate
ug/L
ND
50
44.1
88
50-130
Di-n-octylphthalate
ug/L
ND
50
44.4
89
50-130
Dibenz(a,h)anthracene
ug/L
ND
50
46.2
92
40-130
Dibenzofuran
ug/L
ND
50
28.0
56
40-130
Diethylphthalate
ug/L
ND
50
50.0
84
40-130
Dimethylphthalate
ug/L
ND
50
33.4
67
40-130
Fluoranthene
ug/L
ND
50
47.6
95
30-130
Fluorene
ug/L
ND
50
31.7
63
20-130
Hexachloro-1,3-butadiene
ug/L
ND
50
22.8
46
10-130
Hexachlorobenzene
ug/L
ND
50
33.7
67
30-130
Hexachlorocyclopentadiene
ug/L
ND
50
18.2
36
10-150
Hexachloroethane
ug/L
ND
50
22.9
46
10-130
Indeno(1,2,3-cd)pyrene
ug/L
ND
50
47.5
95
40-130
Isophorone
ug/L
ND
50
27.2
54
30-130
N-Nitroso-di-n-propylamine
ug/L
ND
50
26.8
54
30-130
N-Nitrosodimethylamine
ug/L
ND
50
24.1
48
10-130
N-Nitrosodiphenylamine
ug/L
ND
50
35.6
71
30-130
Naphthalene
ug/L
ND
50
31.4
53
20-130
Nitrobenzene
ug/L
ND
50
26.2
52
20-130
Pentachlorophenol
ug/L
ND
100
79.3
79
10-140
Phenanthrene
ug/L
ND
50
40.8
82
50-130
Phenol
ug/L
ND
50
19.7
39
10-130
Pyrene
ug/L
ND
50
43.9
88
50-130
Results presented on
this page are in the units indicated
by the "Units" column except where
an alternate unit is
presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalXical
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Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: SB/GW
Pace Project No.: 92430807
MATRIX SPIKE SAMPLE:
Parameter
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
QUALITY CONTROL DATA
2588583
Units
92430807009 Spike MS MS
Result Conc. Result % Rec
% Rec
Limits
%
83
10-137
%
51
13-130
%
46
10-130
%
55
13-130
%
35
10-130
%
81
25-130
SAMPLE DUPLICATE: 2588587
Parameter
Units
92430900001
Result
Dup
Result
1,2,4-Trichlorobenzene
ug/L
ND
ND
1,2-Dichlorobenzene
ug/L
ND
ND
1,3-Dichlorobenzene
ug/L
ND
ND
1,4-Dichlorobenzene
ug/L
ND
ND
1-Methylnaphthalene
ug/L
ND
ND
2,2'-Oxybis(1-chloropropane)
ug/L
ND
ND
2,4,5-Trichlorophenol
ug/L
ND
ND
2,4,6-Trichlorophenol
ug/L
ND
ND
2,4-Dichlorophenol
ug/L
ND
ND
2,4-Dimethylphenol
ug/L
ND
ND
2,4-Dinitrophenol
ug/L
ND
ND
2,4-Dinitrotoluene
ug/L
ND
ND
2,6-Dinitrotoluene
ug/L
ND
ND
2-Chloronaphthalene
ug/L
ND
ND
2-Chlorophenol
ug/L
ND
ND
2-Methylnaphthalene
ug/L
ND
ND
2-Methylphenol(o-Cresol)
ug/L
ND
ND
2-Nitroaniline
ug/L
ND
ND
2-Nitrophenol
ug/L
ND
ND
3&4-Methyl phenol (m&p Cresol)
ug/L
ND
ND
3,3'-Dichlorobenzidine
ug/L
ND
ND
3-Nitroaniline
ug/L
ND
ND
4,6-Dinitro-2-methyl phenol
ug/L
ND
ND
4-Bromophenylphenyl ether
ug/L
ND
ND
4-ChIoro-3-methyl phenol
ug/L
ND
ND
4-Chloroaniline
ug/L
ND
ND
4-Chlorophenylphenyl ether
ug/L
ND
ND
4-Nitroaniline
ug/L
ND
ND
4-Nitrophenol
ug/L
ND
ND
Acenaphthene
ug/L
ND
ND
Acenaphthylene
ug/L
ND
ND
Aniline
ug/L
ND
ND
Anthracene
ug/L
ND
ND
Benzo(a)anthracene
ug/L
ND
ND
Benzo(a)pyrene
ug/L
ND
ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
Qualifiers
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aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
SAMPLE DUPLICATE: 2588587
Parameter
Units
92430900001
Result
Dup
Result
RPD Qualifiers
Benzo(b)fluoranthene
ug/L
ND
ND
Benzo(g,h,i)perylene
ug/L
ND
ND
Benzo(k)fluoranthene
ug/L
ND
ND
Benzoic Acid
ug/L
ND
ND
Benzyl alcohol
ug/L
ND
ND
bis(2-Chloroethoxy)methane
ug/L
ND
ND
bis(2-Chloroethyl) ether
ug/L
ND
ND
bis(2-Ethylhexyl)phthalate
ug/L
ND
ND
Butylbenzylphthalate
ug/L
ND
ND
Chrysene
ug/L
ND
ND
Di-n-butylphthalate
ug/L
ND
ND
Di-n-octylphthalate
ug/L
ND
ND
Dibenz(a,h)anthracene
ug/L
ND
ND
Dibenzofuran
ug/L
ND
ND
Diethylphthalate
ug/L
ND
ND
Dimethylphthalate
ug/L
ND
ND
Fluoranthene
ug/L
ND
ND
Fluorene
ug/L
ND
ND
Hexachloro-1,3-butadiene
ug/L
ND
ND
Hexachlorobenzene
ug/L
ND
ND
Hexachlorocyclopentadiene
ug/L
ND
ND
Hexachloroethane
ug/L
ND
ND
Indeno(1,2,3-cd)pyrene
ug/L
ND
ND
Isophorone
ug/L
ND
ND
N-Nitroso-di-n-propylamine
ug/L
ND
ND
N-Nitrosodimethylamine
ug/L
ND
ND
N-Nitrosodiphenylamine
ug/L
ND
ND
Naphthalene
ug/L
ND
ND
Nitrobenzene
ug/L
ND
ND
Pentachlorophenol
ug/L
ND
ND
Phenanthrene
ug/L
ND
ND
Phenol
ug/L
ND
ND
Pyrene
ug/L
ND
ND
2,4,6-Tribromophenol (S)
%
0
0
S4
2-Fluorobiphenyl (S)
%
0
0
S4
2-Fluorophenol (S)
%
0
0
S4
Nitrobenzene-d5 (S)
%
0
0
D3,P3,S4
Phenol-d6 (S)
%
0
0
S4
Terphenyl-d14 (S)
%
0
0
S4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 51 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
QC Batch: 477998 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92430807001, 92430807002, 92430807003, 92430807004, 92430807005, 92430807006
SAMPLE DUPLICATE: 2587899
92430812010 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 13.2 15.8 18
SAMPLE DUPLICATE: 2587900
92430807006 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 15.5 15.9 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 52 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
QC Batch: 478034 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92430807007, 92430807008
SAMPLE DUPLICATE: 2588171
92430895001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 6.7 6.9 2
SAMPLE DUPLICATE: 2588172
92430880003 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 27.3 27.6 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 53 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: SB/GW
Pace Project No.: 92430807
QC Batch: 478469 Analysis Method: ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92430807013
SAMPLE DUPLICATE: 2590066
92430752005 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 7.6 5.6 30 D6
SAMPLE DUPLICATE: 2590067
92431047001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 58.9 60.4 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 54 of 63

Pace Analytical Services, LLC
aceAnalXical� 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pacelabs.com [phone]
QUALIFIERS
Project: SB/GW
Pace Project No.: 92430807
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
WORKORDER QUALIFIERS
WO: 92430807
Ill Samples requiring thermal preservation were received outside of recommended temperature limits of 0-6 degrees
Celsius.
ANALYTE QUALIFIERS
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
HS Results are from sample aliquot taken from VOA vial with headspace (air bubble greater than 6 mm diameter).
L1 Analyte recovery in the laboratory control sample (LCS) was above QC limits. Results for this analyte in associated
samples may be biased high.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
MS Analyte recovery in the matrix spike was outside QC limits for one or more of the constituent analytes used in the
calculated result.
P3 Sample extract could not be concentrated to the routine final volume, resulting in elevated reporting limits.
REPORT OF LABORATORY ANALYSIS
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aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: SB/GW
Pace Project No.: 92430807
ANALYTE QUALIFIERS
SO Surrogate recovery outside laboratory control limits.
S2 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re -analysis).
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
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Date: 06/06/2019 04:56 PM without the written consent of Pace Analytical Services, LLC. Page 56 of 63

aceAnalXical
www.pacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
SB/GW
92430807
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92430807001
SB-1 14'
EPA 3546
477980
EPA 8015C
Modified
478352
92430807002
SB-2 12'
EPA 3546
477980
EPA 8015C
Modified
478352
92430807003
SB-4 10'
EPA 3546
477980
EPA 8015C
Modified
478352
92430807004
SB-5 14'
EPA 3546
477980
EPA 8015C
Modified
478352
92430807005
SB-6 9'
EPA 3546
477980
EPA 8015C
Modified
478352
92430807006
SB-7 9
EPA 3546
477980
EPA 8015C
Modified
478352
92430807007
SB-1 6'
EPA 3546
477980
EPA 8015C
Modified
478352
92430807013
SB-3 16'
EPA 3546
478681
EPA 8015C
Modified
478891
92430807002
SB-2 12'
EPA 3546
478680
EPA 8082A
478748
92430807013
SB-3 16'
EPA 3546
478680
EPA 8082A
478748
92430807001
SB-1 14'
EPA 5030B
478023
EPA 8015C
Modified
478036
92430807002
SB-2 12'
EPA 5030B
478023
EPA 8015C
Modified
478036
92430807003
SB-4 10'
EPA 5030B
478023
EPA 8015C
Modified
478036
92430807004
SB-5 14'
EPA 5030B
478023
EPA 8015C
Modified
478036
92430807005
SB-6 9'
EPA 5030B
478023
EPA 8015C
Modified
478036
92430807006
SB-7 9
EPA 5030B
478023
EPA 8015C
Modified
478036
92430807013
SB-3 16'
EPA 5030B
478460
EPA 8015C
Modified
478468
92430807008
SB-2 20'
EPA 3546
478179
EPA 8270D
478376
92430807009
GW-A
EPA 3510C
478153
EPA 8270D
478238
92430807010
GW-B
EPA 3510C
478153
EPA 8270D
478238
92430807011
GW-C
EPA 3510C
478153
EPA 8270D
478238
92430807012
GW-D
EPA 3510C
478153
EPA 8270D
478238
92430807009
GW-A
EPA 8260B
478294
92430807010
GW-B
EPA 8260B
479165
92430807011
GW-C
EPA 8260B
478294
92430807012
GW-D
EPA 8260B
478294
92430807001
SB-1 14'
ASTM D2974-87
477998
92430807002
SB-2 12'
ASTM D2974-87
477998
92430807003
SB-4 10'
ASTM D2974-87
477998
92430807004
SB-5 14'
ASTM D2974-87
477998
92430807005
SB-6 9'
ASTM D2974-87
477998
92430807006
SB-7 9
ASTM D2974-87
477998
92430807007
SB-1 6'
ASTM D2974-87
478034
92430807008
SB-2 20'
ASTM D2974-87
478034
92430807013
SB-3 16'
ASTM D2974-87
478469
Date: 06/06/2019 04:56 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 57 of 63

Analytical
Document Name:
Condition Upon Recei
Document No.:
F-CAR-CS-033-Rev.06
Document Revised: February i, Luis
Page I of 2
Issuing Authority:
Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville < Raleigh❑ Mechanicsville[]
�a
Sample -Condition
raett #
Client Name: WO# : 92430507
,, _LN
�j
Courier: ❑Fe Ex ❑UPS E]USPS
lient
❑ Commercial []Pace []Other:— 92430807
Custody Seal Present? []yes ,�KNO Seals Intact? ❑Yes �nNo ��� �•�-,< r
a Date/Initials Person Examining Contents:
Peeking Material: ❑Bubble Wrap )�aubble Bags ❑None ❑ Other BiologicalTissuepozen?
,� ❑Yes ❑No ❑kA
Ther-M-9peter: 92 Q�B Type of Ice: . h(w.E ❑Blue ❑None
�❑IR Gun ICJ;
Cooler Temp ('C): IC
_ Correction Factor: Add/Subtract (°C) 0.0
Tempshould be above freezing to VC
Cooler Temp Corrected ('C): I ❑samples out of temp criteria. Samples on ice, cooling process
has begun
USDARegulatcd5oil (❑ N/A, water sample)
Did samples ptigigate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
ain of Custody Present?
Samples Arrived within Hold Time?
short Hold.Tirne Analysis (e72 hr.)'
Rush Turn Around Time Requestec
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissolved analysis: Samples Field Filtered?
Sample Labels Match CCIC?
-includes
Headspace in VOA Vials
Trip Blank Present?
blank Cvstodv Seals Present?
COMMENTS/SAMPLE DISCREPANCY
)L
[:]No
[]N/A
i.
[]NO
❑N/A
2.
No
❑N/A
3.
❑Na
[]N/A
4.
[]No
❑N/A
S.
[]No
[]N/A
6.
7.
&o ❑N/A ! 9.
❑NO
[]No
Did samples originate from a foreign source
including Hawaii and Puerto RICO? [:]Yes
Carrrments/Discrepancy
Field Data Required? ❑Yes []NO
Cot ID of split containers:
CLIENT
IlNOT IFICATION/RESOLUTION
J'n
Person contacted: _ffl�' 'x✓"4 Date/Tlrne: �T r Ir�"'x ✓ J" w��
Project Manager SCURF Review: ! ! r f 1i Date: J— �'n� (1
Project Manager SRF Review: 7 Date: `J[
'Znrr-�� Ict --� �y S axy- i �w� War,
S�� . (i 1 n j� , 1 r S p �r,r��y�. W4,
Oi +A CAC �+� (1 � "1 Y \� �V'( y' `' '� � C Page 58 of 63

Document Name:
Condition Upon Receil
Document No.:
F-CAR-CS-633-Rev.06
document Kevisea: rearuary r, duio
Page 1 of 2
Issuing Authority:
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is Project #
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8075 (water) DOC, LLHg
"Bottom half of box is to list riumber of bottle
WO#:92430807
PM: AMB Due Date: 06/05/19
CLIENT: 92-Nova NC
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Sample ID
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pH upon receipt
Date preservation adjusted
Time preservatlon
adjusted
Amount of Preservative
added
Lot d
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNA Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect conta+hers.
Page 59 of 63

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Page 60 of 63

Document Name: Document Revised: February 7, 2a1is
Sample Condition Upon Receipt(SCUR) Page 1 of 2
Document No.: Issuing Authority:
F-CAR-05.033-Rev.06 Pace Carolinas Quality Office
laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville Raleigh[] Mechanicsville❑
Sample• Client Name: WO# : 92430907
Upon Receipt Project # PM: pMB Due Dade: 0B/ms/1
Courier: ❑Fed Ex [—]UPS USPS ' ❑Client CLIENT, 92-Nova NC
❑ Commercial QPace ❑Other:
Custody Seal Present? ❑Yes ❑N10 Seals intact? ❑Yes QNo J 1r > f I
Pate/Initials Person Examining Contents:
Packing Material: ❑Bubble Wrap ❑Bubble Bags []None ❑ Other Biological Tissue Frozen?
Thermometer: []yes []NO ❑N/A
01R Gun 10:
92TQ48 Type of he: .❑Net ❑Blue []None
Cooler Temp (°C): Correction Factor: Add/Subtract (°C) 0.0
Temp should be above freezing to fi°C
Cooler Temp Corrected {'C): []Samples aut of ternp criteria. Samples on ice, cooling process
hasbegun
USDA Regulated Sail {❑ N/A, water sample)
Did samples origin� to in a quarantine zone within the United States: CA, NY, or SC icheck maps]? Did samples originate from a Foreign source linternat�nally,
[]Yes ONa including Hawaii and Puerto Rlcol? Des [INo
Chain of Custody Present?
Samples Arrived within Hold Time? .
Short Hold.Time Analysis [<72 hr.]?
Rush Turn Around Time Requested?
Sufficient Volume?
Correct Containers Used?
-Pace Containers Used?
Containers Intact?
Dissoived analysis: Samples Field Filtered?
Sample Labels Match COC?
-Ihclu&s. Date/Time/ID/Analysis
Headspace in VOA Vials [>5-6mm]?
Trip Blank Present?
Trip Blank Custody Seals Present?
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
❑No ❑N/A 1.
QNa ❑N/A 2.
QNo
❑N/A
3.
ElN.
❑N/A
4.
[]NO
[I N/A
5.
[]No
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�.
04es ❑No ❑N/A 7.
❑Yes ❑No ❑NIA B.
[]Yes []No ❑N/A 9.
❑Yes []No_-. DN/A I14,
❑Yes AND ❑N/A 1 11.
Date/Time:
Project Manager SCURF Review: affi,�)
Project Manager SRF Revlew: O I f `c)
Field Data Required? ❑Yes ❑No
Lot lD of split containers:
Date:
Date: :5—
Page 61 of 63

Document Name:
Sample Condition Upon Rec
Document No.:
Document nevisea: renroary /, cuia
Page 2 of 2
Issuing Authority:
Pace Carolinas Quality Office
*Check mark top half of box if pH and/or dechlorination is
verified and within the acceptance range for preservation
samples.
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box is to list number of bottle
Project # WQ# : 92430807
PM: pMg Due Date: 06/05/19
CLIENT: 92-Nova NC
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Sample ID Type of Preservative PH upon receipt I Date preservation adJusted Time preservotlon Amount of Preservative Lat ff
adjusted I added
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will 6esent to the North Carolina DEHNR Certification Office
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Page 62 of 63

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Page 63 of 63

4WD► Nova
* Group
4960 Hwy 49 Well Survey Data Table, October, 2019
NCDEQ Incident 15621 Nova Project J19-5100
map
ID #
Property Physical Adress
Property owner
received response
1
4934 NC HWY 49 S HARRISBURG NC 28075
MCINNIS DONALD A & WIFE SHERI
2
4900 NC HWY 49 S HARRISBURG NC 28075
GREENE ELMER R JR
returned (twice) not deliverable as
adressed
3
4850 NC HWY 49 S HARRISBURG NC 28075
ROCK POINT LLC
no well
4
120 MORRIS DR HARRISBURG NC 28075
MASHBURN/ZSAMBEKY & ROGERS
5
5040 NC HWY 49 S HARRISBURG NC 28075
SIBLEY FAMILY LLC
6
118 MORRIS DR HARRISBURG NC 28075
STAFFORD HOWARD C & SUSAN H &
re urne not deliverable as
adressed
715088
NC HWY 49 S HARRISBURG NC 28075
COUCHELL INVESTMENT COMPANY LLC
no well
8
6561 MOREHEAD RD HARRISBURG NC 28075
LE BACH MAI
9
6549 MOREHEAD RD HARRISBURG NC 28075
N E HIMEBAUGH REALTY LLC
10
6515 MOREHEAD RD HARRISBURG NC 28075
HARRISBURG BAPTIST CHURCH
no well
11
109 MORRIS DR HARRISBURG NC 28075
SINER ERIN LEE
returned not deliverable as
adressed
12
113 MORRIS DR HARRISBURG NC 28075
MERA INVESTMENTS LLC
13
117 MORRIS DR HARRISBURG NC 28075
HUDGENS WANDA H
no well
14
121 MORRIS DR HARRISBURG NC 28075
THOMPSON TOMMY E
returned (twice) not deliverable as
adressed
15
125 MORRIS DR HARRISBURG NC 28075
OLD TOWNE DEVELOPMENT Corp
re urne wice MTUerl—verable as
adressed
16
129 MORRIS DR HARRISBURG NC 28075
LAMBERT ARNOLD E
17
201 MORRIS DR HARRISBURG NC 28075
OLD TOWNE DEVELOPMENT Corp
returned (twice) not deliverable as
adressed
18
205 MORRIS DR HARRISBURG NC 28075
LONG ALFARD L
yes, usecl Tor irrigation 7 swimming
pool
19,209
MORRIS DR HARRISBURG NC 28075
CANUP MELVIN F
20
211 MORRIS DR HARRISBURG NC 28075
CANUP FREDIA I LF EST
21
215 MORRIS DR HARRISBURG NC 28075
HATLEY ROY E
no well
22
201 PATRICIA AVE HARRISBURG NC 28075
RUFF S EUGENE
23
202 PATRICIA AVE HARRISBURG NC 28075
STRUBE PAUL F & SARAH GAILIWF
no well
24
313 MORRIS DR HARRISBURG NC 28075
MARTIN JOE R
yes, used Tor irrigation ancl was ing
cars
25
130 PLAZA DR HARRISBURG NC 28075
HAMPTON ROBERT ALLEN
no well
26
132 PLAZA DR HARRISBURG NC 28075
LOVE MIKE DELVERT
27
138 PLAZA DR HARRISBURG NC 28075
LOVE MIKE DELVERT
yes, used for irrigation
28
210 PLAZA DR HARRISBURG NC 28075
MCCONNELL JEREMIAH S
29
1 212 PLAZA DR HARRISBURG NC 28075
HERRERA SEBASTIANA
no well
30
214 PLAZA DR HARRISBURG NC 28075
RATCLIFF RICHARD D JR
no well / phone message
31
218 PLAZA DR HARRISBURG NC 28075
BOOTH GEORGE A
water well on site
32
222 PLAZA DR HARRISBURG NC 28075
RICE LISA A
33
213 PATRICIA AVE HARRISBURG NC 28075
STRICKHOUSER VIRGINIA W
34
1 302 PLAZA DR HARRISBURG NC 28075
SPRINGS KELLY M
35
304 PLAZA DR HARRISBURG NC 28075
LITTLE CLARENCE F
no well
36
308 PLAZA DR HARRISBURG NC 28075
MATTERN LAWRENCE DOUGLAS JR
37
5041 NC HWY 49 S HARRISBURG NC 28075
O & G LEASING LLC
returned (twice) not deliverable as
adressed
38
4935 NC HWY 49 S HARRISBURG NC 28075
KILLIAN PLAZA LLC
no well
39
4909 NC HWY 49 S HARRISBURG NC 28075
HARRISBURG MEDICAL ASSOCIATES
no well
5214875
NC HWY 49 S HARRISBURG NC 28075
HARRISBURG PRESBYTERIAN CHURCH
Ino well

4WD► Nova
* Group
4960 Hwy 49 Well Survey Data Table, October, 2019
NCDEQ Incident 15621 Nova Project J19-5100
map
ID #
Property Physical Adress
Property owner
received response
414863
NC HWY 49 S HARRISBURG NC 28075
O & G LEASING LLC
returned (twice) not deliverable as
adressed
42
5125 NC HWY 49 S HARRISBURG NC 28075
LANDAZ LLC A NC LLC
no well
43
110 SIMS PKWY HARRISBURG NC 28075
PHARR ELIZA
44
116 SIMS PKWY HARRISBURG NC 28075
OAK GROVE MISSIONARY BAPTIST
45
5075 NC HWY 49 S HARRISBURG NC 28075
HARRISBURG NC HOLDINGS LLC
no well
46
105 OAKLEY DR HARRISBURG NC 28075
STAUB TERESITA M
47
101 OAKLEY DR HARRISBURG NC 28075
LAGANA LOUIS P
48
107 OAKLEY DR HARRISBURG NC 28075
JOENICK LLC
49
111 OAKLEY DR HARRISBURG NC 28075
DELANEY PETER M
no well
50
115 OAKLEY DR HARRISBURG NC 28075
DELANEY PETER M
no well
51
125 OAKLEY DR HARRISBURG NC 28075
WARD JANE F
water well / not operational
52,207
OAKLEY DR HARRISBURG NC 28075
HARRISBURG PRESBYTERIAN CHURCH
no well
53
6740 HARRIS DEPOT RD HARRISBURG NC 28
HARRISBURG PRESBYTERIAN CHURCH
no well
54
214 OAKLEY DR HARRISBURG NC 28075
LEONARD ROBERT B
nwell
55
208 OAKLEY DR HARRISBURG NC 28075
WRIGHT MARGOT M LF EST
56
202 OAKLEY DR HARRISBURG NC 28075
DA MCDONALD LLC
no well
57
126 OAKLEY DR HARRISBURG NC 28075
LEWIS RICKARD A
City water, but has an 180'well use
for garden only. Also connected to
118 Oakley
58
112 OAKLEY DR HARRISBURG NC 28075
OTERI ANDREA B
returned ice not deliverable as
adressed
59
208 HENDERSON CIR HARRISBURG NC 28075
TOLBERT BRIAN M
60
214 HENDERSON CIR HARRISBURG NC 28075
LITTLE PHILLIP A
61
213HENDERSON CIR HARRISBURG NC 28075
CAUDLE WILSON H
62
320 HENDERSON CIR HARRISBURG NC 28075
LEE GAYLE MORRIS
no well
63
330 HENDERSON CIR HARRISBURG NC 28075
CIUCEVICH PATRICK JOSEPH
64
333 PARK PL HARRISBURG NC 28075
HANNA PATRICIA A
65
337 PARK PL HARRISBURG NC 28075
SWAIN ROGER ALLEN TR
66,341
PARK PL HARRISBURG NC 28075
FRYE JUDY A
no well
67
4800 NC HWY 49 S HARRISBURG NC 28075
VW REBOUND 1 LLC
returned not deliverable as
adressed
68
unadressed parcel 55075693030000, Morris
Drive Harrisburg NC
Rocky River LLC
no well
69
4720 NC HWY 49 S HARRISBURG NC 28075
CHARLOTTE METRO FEDERAL CREDIT UNION
70
Unadressed parcel 55076643400000 hwy 49, Hari
WOODFIELD HOLDINGS LLC
714725
NC HWY 49 S HARRISBURG NC 28075
FIRST CHARTER REAL ESTATE
72
120 PLAZA DR HARRISBURG NC 28075
HAMMOCK AMY E
no well
73
124 PLAZA DR HARRISBURG NC 28075
HUSTER KENNETH H
no well
74,128
PLAZA DR HARRISBURG NC 28075
OLLILA JOHN R & MARGIE M
no well
75
120 PARALLEL DR HARRISBURG NC 28075
CURRIE TONY MILES
76
124 PARALLEL DR HARRISBURG NC 28075
BLAND CHADD M
77
123 PLAZA DR HARRISBURG NC 28075
STOWERS G LANIER
returned not deliverable as
adressed
78
129 PLAZA DR HARRISBURG NC 28075
BLACKWELDER KENNETH W
no well
79
133 PLAZA DR HARRISBURG NC 28075
REED JOHN S JR
80
137 PLAZA DR HARRISBURG NC 28075
INORRIS EDDIE WAYNE

4WD► Nova
JP** Group
4960 Hwy 49 Well Survey Data Table, October, 2019
NCDEQ Incident 15621 Nova Project J19-5100
map
ID #
Property Physical Adress
Property owner
received response
81
203 PLAZA DR HARRISBURG NC 28075
BUSTLE BENJAMIN SHANE
no well
82
209 PLAZA DR HARRISBURG NC 28075
THREATT PAUL E JR
83
215 PLAZA DR HARRISBURG NC 28075
JERRELL HELMS
no well
84
217 PLAZA DR HARRISBURG NC 28075
RICE BARBARA S
85
305 PATRICIA AVE HARRISBURG NC 28075
SIDES JOE KENT
86
212 PARALLEL DR HARRISBURG NC 28075
TORRENCE SANDY J
87
214 PARALLEL DR HARRISBURG NC 28075
TORRENCE ROBIN G
88
216 PARALLEL DR HARRISBURG NC 28075
BAKER CHARLIE F
yes
89
226PARALLEL DR HARRISBURG NC 28075
RATCLIFF RICHARD III
no well / phone message
90
230 PARALLEL DR HARRISBURG NC 28075
KIKER PAM J
91
232 PARALLEL DR HARRISBURG NC 28075
HATLEY PATSY DIANNE
no well
92
234 PARALLEL DR HARRISBURG NC 28075
WALTERS HARVEY A
93,319
PATRICIA AVE HARRISBURG NC 28075
LITTLE PHILLIP A
9416570
MOREHEAD RD HARRISBURG NC 28075
HARRISBURG PRESBYTERIAN CHURCH
no well

RECEPTOR SURVEY - CERTIFIED MAIL RECEIPTS
0 to 500 foot Radius from Property Boundaries
CERTIFIEDU.S. Postal Service'" i
MAILO RECEIPT
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�5enrro 220 Branchview Dr SE
SireerariifA Concord, NC 28025
�,ry, Stete' Re: 120 Morris Dr, Harrisburg, NC 28075 4

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a Signal Mountain, TN 37377 _-
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$ 3362 Smith Farm RD
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Matthews, NC 28104
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�iiy 3Yare;zi Re: 5088 NC Hwy 49 �, Harrisburg, NC 28075 7
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$ 230 Union St
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$ PO Box 393
Sent To
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6 OLD TOWNE DEVELOPMENT CARP
Sent To 8312 Caldwell Rd
Harrisburg, NC 28075
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$ 11501 Winners Cir
Sent To
9 Charlotte, NC 28215
1 Sira3et and'Apt: J
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$ 121 Morris Dr -
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HAMPTON RDBERT ALLEN
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1 s7r�ei eriifApr:1
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112015 PSN 7530-02-DOO-9047
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$ 210 Plaza Dr
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C1 STAUB TERESITA M © JOENICK LLC
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4324 Granite Ridge Rd
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137 Plaza Dr
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r-1 OLLILA JOHN R & MARGIF M
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209 Plaza Dr
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iet aird Apr-
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2593 Live Oak Dr SW
�' Suppply, NC 28462 ---0f� Re: 201 Patricia Ave, Harrisburg, NC 28075 22 ------

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$ 4600 Annette Dr
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$
850 Sleepy Hollow Rd
Sent To
Midland, NC 28107
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PostalPS Form 3800, April 2015 PSN
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208 Henderson Cir
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341 Park PI
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EZI 9 FIRST CHARTEL ESTATE
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Mike Minett
From: David M Troutman <[e-mail]>
Sent: Friday, July 19, 2019 11:30 AM
To: Mike Minett
Subject: this is everything with a Harrisburg mailing address -NONE are actully in the city
Follow Up Flag: Follow up
Flag Status: Flagged
52
07-0022
Arica Rucker
9265 Robinson Church Rd.
Harrisburg
55
07-0332 W
Ben J. Howie
9814 Hickory Ridge Rd.
Harrisburg
1910
08-00,40
Justin Cook
11123 Hickory Ridge Rd
Harrisburg
229
03-0074
Theodore Suggs
10579 Hickory Ridge Rd
Harrisburg
246
OS-0134
Vince Powell
9593 Morningside Circle
Harrisburg
270
94-0294
Stacy Chaffin
4035 Oak Hollow Lane
Harrisburg
297
02-0272
Whitley Construction LLC.
9700 Reedy Lane
Harrisburg
344
05-0119
Larry Wilcox
7220 Pharr Mill Road
Harrisburg
395
10-007S R
James M. Little
9812Chestnut Hills Drive
Harrisburg
410
10-0(Y99
Julia Mason
8787 Rocky River Road
Harrisburg
429
08-0217R
George R. Powell
2412 Timber Ridge Road
Harrisburg
477
83-0689A
Patrick Keen
8835 Lazy Ridge Lane
Harrisburg
479
11-0129W
Jennifer McMillan
10490 Hickory Ridge Road
Harrisburg
561
12-0155
Vince &Staci Powell
8346 Pompano Road
Harrisburg
585
13-0054
Andrew Coore
Lower Rocky River Road
Harrisburg
605
13-0153W
Bryan S. Reece
12125 Lower Rocky River Road
Harrisburg
518
13-0188
Lucy Caldwell
8970 Robinson Church Road
Harrisburg
621
11-0106P
Eric Hampton
10075 Hickory Ridge Road
Harrisburg
539
14-0003W
AGA Italia, LLC
5470 Hudspeth Dairy Road
Harrisburg
562
14-0054
Hwy 49 Landfill Inc.
1840 Mulberry Road
Harrisburg
573
12-0118
Rebecca Lancaster
3520 Mckees Court
Harrisburg
703
13-0157
Jonathan Kiser
11801 Gatewood Road
Harrisburg
776
12-0065
Cleave K. Carr
2655 Timber Ridge Road
Harrisburg
791
15-0178
Christopher Duff ell
9725 Reedy Lane
Harrisburg
804
15-0216
Samuel C. Johnson
2521 Grady Harris Road
Harrisburg
825
1.5-0157
Kelly Marris
4133 Nonia Drive
Harrisburg
898
15-02,50W
James & Rebecca Watson
7541 Paul Linker Place
Harrisburg
905
16-0119
Cody & Morgan Johnson
2597 Grady Harris Sr. Rd.
Harrisburg
947
14-0204
Deborah Carano
9600 Reedy Ln.
Harrisburg
1011
17-0145
Alberto Sandoval
2659 Grady Harris SR Road
Harrisburg
1022
18-0041
Mayada Idlibi
3505 Mckees Court
Harrisburg
1023
18-00,42
Mayada Idlibi
3505 Mckees Court
Harrisburg
1091
13-0167
Jerry Davis
11771 Lower Rocky River Road
Harrisburg
1116
19-0033
Hoawrd Cress
7507 Robinson Church Road
Harrisburg
1121
19.0119
Kirkpatrick Carr
8355 Rocky River Road
Harrisburg
462
11-0039p
Joshua Goodman
7535 Robinson Church Road
Harrisburg NC
SSQ
1Q_fY171;1n0
Crnff RorrLdA —Al; ']1Fth Ct r QQ AYlnAmnC3 I n
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1

From: Mike Minett [mailto:[e-mail]]
Sent: Friday, July 19, 2019 10:14 AM
To: David M Troutman
Subject: Permitted drinking water wells in Harrisburg
CAUTION: This email originated from outside of the organization. Do not click links or open attachments unless you recognize the
sender and know the content is safe.
Hi David,
Thanks for returning my call. Please use this as a request for your listing of permitted drinking water wells in Harrisburg.
Thanks, and try to stay cool this weekend!
Mike Minett
VP - Client Manager I Nova Group, GBC
442 South Main Street, Suite 7
Davidson, NC 28036
❑ [phone] J ❑ [e-mail]
❑ www.novagroupgbc.com
Connect:
Inspired Solutions by Novo Group
DISCLAIMER: Email correspondence to and from this address may be subject to North Carolina public records law and/or
may be confidential under HIPAA regulations.
"CONFIDENTIALITY NOTICE: The information contained in this electronic mail is confidential information intended only
for the use of the entity or individual to whom it is addressed. If the reader of this message is not the intended recipient,
you are hereby notified that any dissemination, distribution, retransmission, or copying of this message is strictly
prohibited. If you have received this message in error, please notify me immediately by reply transmission. Thank You.

Limited Site Assessment Report Appendix A
Report Formats
Limited Site Assessment Risk Classification and Land Use Form
Part I — Groundwater/Surface WaterNapor Impacts
High Risk
1. Has the release contaminated any water supply well including any well used for non -drinking purposes?
YES®
2. Is a water supply well used for drinking water located within 1,000 feet of the source area of the release?
YESAQ
3. Is a water supply well not used for drinking water (e.g., irrigation, washing cars, industrial cooling water
filling swimming pools) located within 250 feet of the source area of the release? YESQ
4. Does groundwater within 500 feet of the source area of the release have the potential for future use (there
no other source of water supply other than the groundwater)? YE9W
5. Do vapors from the release pose a threat of explosion because of accumulation of the vapors in a confined
space or pose any other serious threat to public health, public safety or the environment? YESO
If yes, describe.
6. Are there any other factors that would cause the release to pose an imminent danger to public health, public
safety, or the environment? YES&
If yes, describe.
Intermediate Risk
7. Is a surface water body located within 500 feet of the source area of the release?
YES,�O
If YES, does the maximum groundwater contaminant concentration exceed the surface water quality
standards and criteria found in 15A NCAC 2B .0200 by a factor of 10? YES/NO
8. Is the source area of the release located within a approved or planned wellhead protection area as defined in 42
USC 300h-7(e)? YESO
If yes, describe.
9. Is the release located in the Coastal Plain physiographic region as designated on a map entitled "Geology
North Carolina" published by the Department in 1985? YERW
If YES, is the source area of the release located in an area in which there is recharge to an unconfined or
semi -confined deeper aquifer that is being used or may be used as a source of drinking water? YES/NO
If YES, describe.
10. Do the levels of groundwater contamination for any contaminant exceed the gross contamination levels (S e
Table 2.) established by the Department? YE6
Part II - Land Use
Property Containing Source Area of Release
The questions below pertain to the property containing the source area of the release.
1. Does the property contain one or more primary or secondary residences (permanent or temporary)?
YESQ
Describe.

Limited Site Assessment Report Appendix A
Report Formats
2. Does the property contain a school, daycare center, hospital, playground, park, recreation area, church,
nursing home, or other place of public assembly? YES4
Describe.
3. Does the property contain a commercial (e.g., retail, warehouse, office/business space, etc.) or industrial
(e.g., manufacturing, utilities, industrial research and development, chemical/petroleum bulk storag tc.)
enterprise, an inactive commercial or industrial enterprise, or is the land undeveloped? kEy�j NO
Describe.
The Property is currently used for light automotive repair, and automobile inspection. It was formerly a gas
station.
4. Do children visit the property?
Explain. Children of the auto repair / car inspection business visit the Property.
a/NO
Is access to the property reliably restricted consistent with its use (e.g., by fences, security personnel or
both)? YE5O
Explain.
No. The contaminated soil is under pavement. There are no fences surrounding the Property.
5. Do pavement, buildings, or other structures cap the contaminated soil? ®E /NO
Describe.
The soil contamination remaining appears to be residual. The site has undergone some initial remedial
action, with a general removal of impacted soils to between 8 and 12 feet bls. The impacted soils tested,
were near the capillary fringe, and were below soil -to -groundwater standards, with one exception, (1-
Methylnaphthalene) at 14' bls in MW-1.
If yes, what mechanisms are in place or can be put into place to ensure that the contaminated soil will
remain capped in the foreseeable future?
The site is slated for redevelopment with a restaurant. It will be a
filled site, essentially bringing the grade up to current street level (approximately four feet). There is also
some source removal / remediation planned.
6. What is the zoning status of the property?
Commercial
7. Is the use of the property likely to change in the next 20 years?
Explain. The prospective developer plans to build a Wendy's Restaurant.
Property Surrounding Source Area of Release
The questions below pertain to the area within 1,500 feet of the source area of the release (excludes property
containing source area of the release):
1. What is the distance from the source area of the release to the nearest primary or secondary residence
(permanent or temporary)? Approximately 225 feet.

Limited Site Assessment Report Appendix A
Report Formats
2. What is the distance from the source area of the release to the nearest school, daycare center, hospital,
playground, park, recreation area, church, nursing home or other place of public assembly?
Approximately 500 feet.
3. What is the zoning status of properties in the surrounding area? _C-1 Light Commercial and Office
District on both sides of Hwy 49, RM-1 Residential, medium
density north of Morris Drive and south of Oakley Drive. There is some CUO-1 Office /
Institutional District south of Hwy 49.
Briefly characterize the use and activities of the land in the surrounding area. Highway business,
office, and food along Hwy 49, with single family residential to the north, and south.
F. Receptor Information
Determine and describe all potential receptors, including those in the categories listed below. Compile this
information in a table entitled Public and Private Water Supply Well and Other Receptor Information (Complete Table
B-5 from the Guidelines, Appendix B.) in which an identification code is assigned to each potential receptor. Indicate
the locations of each potential receptor, using the identification code, on a potential receptor map. Use information
from all available sources and from site investigations.
1. Water Supply Wells
Determine and describe the location, use, and ownership of public and private water supply wells in the area
within 1,500 feet of the source of the release. Compile this information in Table B-5 and indicate the well locations
on the potential receptor map. Note whether well users are also served by a municipal water supply. Refer to the
instructions for a water supply well survey in Section 2.4 of the Guidelines.
2. Public Water Supplies
Determine the existence and availability of public water supplies within 1,500 feet of the source area of the
release. Compile this information in Table B-5 and indicate the locations of the nearest public water lines and
the source(s) of the public water supply on the potential receptor map.
3. Surface Water
Identify all surface water bodies (e.g., ditch, pond, stream, lake, river) located within 1,500 feet of the source
area of the release and indicate distance from source of release in Table B-5 and indicate locations on the
potential receptor map.
4. Wellhead Protection Areas
Indicate whether or not the UST release source area is located within an approved wellhead protection area.
Refer to Section 2.4 of the Guidelines for instructions on how to access the list of currently approved wellhead
protection plans and generate a map of UST and wellhead protection area locations. List any identified wellhead
protection area in Table B-5 by PWS ID number and PWS system name and show the wellhead protection area
on the potential receptor map. To document performance of the wellhead protection area investigation append
to the potential receptor map a copy of the map generated using ArcIMS Viewer to show 1) the UST location,
2) the wellhead protection area, and 3) community wells.
5. Deep Aquifers in the Coastal Plain Physiographic Region
Indicate if the source area of the release is located in an area in which there is recharge to an unconfined or semi -
confined deeper aquifer and indicate if that aquifer is being used or may be used as a source of drinking water,
referring to Section 2.4 of the Guidelines. Based on a review of scientific literature on the regional hydrogeology
and well construction records and lithologic logs for deeper wells in the area, identify and describe the deep
aquifers underlying the release. Include information on the depth of the deep aquifer in relation to the surficial
saturated zone, the lithology and hydraulic conductivity of the strata between the surficial aquifer and the deeper
aquifer, and the difference in groundwater head between the surficial aquifer and the deeper aquifer. Discuss the

Limited Site Assessment Report Appendix A
Report Formats
local and regional usage of the deep aquifer and the draw down from major pumping influences. Also, specify
the distance from the source area of the release to major discharge areas, such as streams and rivers. Cite all
sources and references used for this discussion.
Note: This requirement only pertains to releases in the Coastal Plain physiographic region as designated on a
map entitled "Geologic Map of North Carolina "published by the Department in 1985. This map can be
obtained for a fee from the North Carolina Geologic Survey, 1612 MSC, Raleigh, NC 27699-1612 or at
hlt 2://nc-maps.store.yahoo.net.
Subsurface Structures
Describe subsurface features, including sewers, utility lines, conduits, basements, vaults, septic tanks, drain
fields, etc., referring to Section 2.4 of the Guidelines. Compile this information in Table B-5 and indicate the
locations on the potential receptor map. Discuss the risk of explosion due to the accumulation of vapors in
confined space and the threat to public health, public safety or the environment posed by vapors in the
subsurface features.
G. Land Use
1. Property Owners and Occupants
Determine the names and addresses of property owners and occupants within or contiguous to the area
containing contamination and all property owners and occupants within or contiguous to the area where the
contamination is expected to migrate. Compile this information in Table B-6 from the Guidelines, Appendix B,
and indicate the property locations on the land use map.
2. Sensitive Land Use Features
List features sensitive to impact from the release (schools, daycare centers, nursing homes, hospitals, playgrounds,
parks and recreation areas, churches, camps and other places of assembly) and show the zoning status of the area
within 1500' of the source of the release. Compile this information in Table 13-10 from the Guidelines, Appendix
B, and indicate the feature locations on the land use map.