MO-9370_40822_CA_IAR_201809027_ Initial Abatement Report

0 PAR
ENVIRONMENTAL
Risk Well Managed
September 27, 2018
Ms. Trudy Beverly
NCDEQ, Division of Waste Management, UST Section
610 East Center Avenue, Suite 301
Mooresville, North Carolina, 28115
Re: Initial Abatement Action Report
Siblings, LLC
Ms. Wendy Sweet
234 Johnson Street
Rock Hill, South Carolina 28731
Incident No. 40822
Dear Ms. Beverly:
North Carolina
301 McCullough Dr. Suite 400,
Charlotte, NC 28262
f: 877.884.6775
t: 704.782.0555
On behalf of the owner for the subject property, PM Environmental, Inc. (PM) is submitting the
attached Initial Abatement Action Report. Please contact me at 704-782-0555 should you have
any questions or comments concerning this submittal.
Sincerely,
PM Environmental, Inc.
Donald D. Warren.
Regional Manager/Senior Consultant
Attachment
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INITIAL ABATEMENT ACTION REPORT
411 Woodvale Place I Charlotte, North Carolina
PM Project Number 15-4305-0002
Prepared for:
Siblings, LLC
234 Johnson Street
Rock Hill, South Carolina 28731
Prepared by:
PM Environmental, Inc.
301 McCullough Drive, Suite 400
Charlotte, North Carolina 28262
www,pmenvxorn

PAII
ENVIRONMENTAL
Risk Well Managed
INITIAL ABATEMENT ACTION REPORT
FOR
Siblings, LLC Property
411 Woodvale Place
Charlotte, Mecklenburg County, North Carolina
North Carolina
301 McCullough Dr. Suite 400,
Charlotte, NC 28262
f: 877.884.6775
t: 704.782.0555
Facility I.D. Number: N/A
Incident Number: 40822
Risk Classification: Pending
Latitude: 35' 14' 14.93" North Longitude: 80° 51' 50.15" West
August 28, 2018
PREPARED FOR:
Siblings, LLC
Ms. Wendy Sweet
234 Johnson Street
Rock Hill, South Carolina 28731
704-400-9481
CONSULTANT:
PM Environmental, Inc.
301 McCullough Drive, Suite 400
Charlotte, North Carolina 28216
704-782-0555
PM Project No. 15-4305-0-0002
INCIDENT INFORMATION:
In April 2018, during the removal of one 550-gallon fuel oil UST, hydrocarbon affected soil were
detected. Hydrocarbon affected soils were confirmed from a sample obtained on May 4, 2018.
The soil sample revealed TPH-DRO at a concentration of 3,680 mg/kg.
9"� 0
1�i all5iD
Donald D. Warren John W. Hargraves, P.G.
Regional Manager Regional Manager/Senior Geologist
ALABAMA FLORIDA ILLINOIS MICHIGAN MISSISSIPPI NEW JERSEY NORTH CAROLINA OHIO I TENNESSEE I WWW.PMENV.COM
Q U A L I TY - S E R V I C E S 0 L U TI 0 N S

Initial Abatement Action Report for the Siblings, LLC Residence
Located at 411 Woodvale Place, Charlotte, North Carolina
PM Environmental, Inc., Project No. 15-4305-0-0002; August 28, 2018
A. Site Information
1. Site Identification
Date of Report: August 28, 2018
Facility ID#:
N/A
UST Incident#:
40822
Site Name:
Siblings, LLC Property
Site Street Address: 411 Woodvale Place
Nearest City/Town:
Charlotte, North Carolina
Zip Code:
28208
County:
Mecklenburg
Latitude:
35.14'14.93" North Longitude:
2. Contact Information
UST Owner:
Address:
Phone:
UST Operator:
Property Owner:
Property Owner Address:
Property Owner Phone:
Property Occupant:
Consultant/Contractor:
Address:
Analytical Laboratory:
Address:
State Certification:
Phone:
3. Release Information
80.51'50.15" West
Siblings, LLC (Attn: Ms. Wendy Sweet)
234 Johnston Street, Rock Hill, South Carolina 28731
704-400-9481
N/A
Siblings, LLC (Attn: Ms. Wendy Sweet)
234 Johnston Street, Rock Hill, South Carolina 28731
704-400-9481
Performance Ford
PM Environmental, Inc.
301 McCullough Drive, Suite 400, Charlotte, North Carolina 28216
SGS Accutest
4405 Vinland Road, Suite C-15
Orlando, Florida 32811
573
407-425-6700
Date Discovered: May 2018
Estimated Quantity of Release: Unknown
Cause of Release: In May 2018, soil samples confirmed subsurface hydrocarbon -affected soil
post the removal of the fuel oil UST. The release timing and quantity are not known.
Source of Release: UST
Size and Contents of UST System(s) from which the release occurred: One 550-gallon
petroleum UST.
PM Environmental, Inc.
Page 1

Initial Abatement Action Report for the Siblings, LLC Residence
Located at 411 Woodvale Place, Charlotte, North Carolina
PM Environmental, Inc., Project No. 15-4305-0-0002; August 28, 2018
4. Report Certification
I, John. W. Hargraves, a Licensed Geologist for PM Environmental, Inc., do certify that the
information contained in this report is correct and accurate to the best of my knowledge.
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John W. Hargraves, P.G. ""®�.�c%•°•�o��iG��`'
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Regional Manager/Senior Geo�b�c}'t.,,,
PM Environmental, Inc.
Page 2

Initial Abatement Action Report for the Siblings, LLC Residence
Located at 411 Woodvale Place, Charlotte, North Carolina
PM Environmental, Inc., Project No. 15-4305-0-0002; August 28, 2018
B. Executive Summary
The subject property consists of one parcel totaling approximately 0.145 acres located at 411
Woodvale Place in Charlotte, Mecklenburg County, North Carolina (Parcel ID No. 07107412).
This property includes a single parcel and is currently undeveloped. The property location is
illustrated on Figure 1.
The adjacent and surrounding properties are primarily residential and Woodvale Place fronts the
subject property to the north, beyond which are residential properties. The adjoining properties
to the south, west and east are also residential properties. The subject property layout and
adjoining properties are illustrated on Figure 2.
In April 2018 during the demolition of the former onsite residence, one estimated 550-gallon fuel
oil underground storage tank (UST) was removed from the central portion of the subject lot.
The UST was removed from the ground by the demolition contractor. Prior to removal of the
UST, 450-gallons of petroleum contact water (PCW) was removed from the tank and
transported off -site for disposal. During the UST removal olfactory indications of hydrocarbon
affected soil in the vicinity of the UST were detected.
On May 4, 2018, PM was contracted to collect a soil sample from the hydrocarbon affected soils
in the area of the former UST location. One soil sample (TP-1) was collected at the
approximate depth of the former basin bottom. The soil sample was submitted for laboratory
analysis of Total Petroleum Hydrocarbons — Gasoline Range Organics (TPH-GRO), Total
Petroleum Hydrocarbons — Diesel Range Organics (TPH-DRO). Review of the soil analytical
results indicated TPH-DRO at concentrations of TPH-DRO 3,680 milligrams per kilograms
(mg/kg) exceeding the North Carolina Department of Environmental Quality (NCDEQ) reporting
limit of 100 mg/kg.
Based on the results of the May 2018 sampling results, the property owner contacted the
NCDEQ notifying them of the release, which prompted a Notice of Regulatory Requirement
(NORR) issued by NCDEQ dated July 6, 2018. The NORR issued a requirement for Initial
Abatement Action (IAA) to be completed. Additionally, the NCDEQ assigned an incident
number (40822) for the release.
On August 7, 2018, PM performed the oversight of approximately 66.99 tons of hydrocarbon
affected soils from the former UST basin. The excavated soil was transported to Environmental
Soils, Inc. of Lattimore, North Carolina. Five subsurface confirmation soil samples (OE-1
through OE-5) were obtained from native material from the tank basin sidewalls and base
following the soil excavation. Each of the confirmation soil samples were submitted for
laboratory analysis of volatile organic compounds (VOCs), semi -volatile organic compounds
(SVOCs), and Massachusetts Department of Environmental Protection Volatile Petroleum
Hydrocarbons and Extractable Petroleum Hydrocarbons (MADEP VPH/EPH).
A review of the analysis from the confirmation soil samples obtained from the former tank basin
revealed EPH Aromatic fraction C-11-C22 at a concentration of 28.9 milligrams per kilograms
(mg/kg) in sample OE-1 collected at the base of the excavation. The detected concentration of
C-11-C22 is below the NCDEQ most stringent soil to groundwater Maximum Soil Contaminant
Concentration (MSCC) of 31 mg/kg. No additional target analytes were detected in any of the
confirmation samples exceeding the laboratory MRLs.
PM Environmental, Inc.
Page 3

Initial Abatement Action Report for the Siblings, LLC Residence
Located at 411 Woodvale Place, Charlotte, North Carolina
PM Environmental, Inc., Project No. 15-4305-0-0002; August 28, 2018
Based on the over excavation, removal of hydrocarbon affected soils and results of confirmation
sampling results, PM recommends this incident be closed and the site granted no further action
(NFA) in accordance with the NCDEQ UST Section guidelines.
PM Environmental, Inc.
Page 4

Initial Abatement Action Report for the Siblings, LLC Residence
Located at 411 Woodvale Place, Charlotte, North Carolina
PM Environmental, Inc., Project No. 15-4305-0-0002; August 28, 2018
C. Table of Contents
A.
Site Information..................................................................................................................................... I
1. Site Identification.....................................................................................................................1
2. Contact Information.................................................................................................................1
3. Release Information................................................................................................................1
4. Report Certification..................................................................................................................2
B.
Executive Summary.............................................................................................................................3
C.
Table of Contents.................................................................................................................................5
D.
Site History and Characterization......................................................................................................6
E.
Site Check Report (Not Applicable to this Investigation)...............................................................7
F.
UST Closure Report.............................................................................................................................7
G.
Initial Response and Abatement Action...........................................................................................7
H.
Groundwater and Surface Water Investigation...............................................................................7
I.
Excavation of Contaminated Soil........................................................................................................7
J.
Recommendations................................................................................................................................9
FIGURES
Figure 1
Figure 2
Figure 3
TABLES
Table 1
Table 2
Table 3
APPENDICES
Property Location Map
Site Plan
Site Plan with Sample Locations and Analytical Results
Site History — Release Information
Site History — Property Owner and Responsible Party Information
Summary of Soil Analytical Results — TPH, VOCs, SVOCs, VPH and EPH
Appendix A Disposal Manifests for Soil and Liquids
Appendix B Laboratory Reports — Pace Analytical, LLC
Appendix C Chain of Custody for Soil Samples
Appendix D Photographic Log
PM Environmental, Inc.
Page 5

Initial Abatement Action Report for the Siblings, LLC Residence
Located at 411 Woodvale Place, Charlotte, North Carolina
PM Environmental, Inc., Project No. 15-4305-0-0002; August 28, 2018
D. Site History and Characterization
UST system details:
UST
Capacity
Was Release
ID#
Product
(gallons)
Date Installed
Date Removed
Assoc. with UST
System
Petroleum
1
(records
550
Unknown
April, 2018
Yes
unavailable
UST Owner/Operator information:
UST
Name of Owner/
Dates of
Owner or
Telephone
ID#
Operator
Ownership/
Operator
Address
Number
Operation
Information
Property
234 Johnston
1
Siblings, LLC.
Not
Owner
Street, Rock Hill,
704-400-9481
Available
SC 28713
The subject property consists of one parcel totaling approximately 0.145 acres located at 411
Woodvale Place in Charlotte, Mecklenburg County, North Carolina (Parcel ID No. 07107412).
This property includes a single parcel and is currently undeveloped. The property location is
illustrated on Figure 1.
The adjacent and surrounding properties are primarily residential and Woodvale Place fronts the
subject property to the north, beyond which are residential properties. The adjoining properties
to the south, west and east are also residential properties. The subject property layout and
adjoining properties are illustrated on Figure 2.
In April 2018 during the demolition of the former onsite residence, one estimated 550-gallon fuel
oil underground storage tank (UST) was removed from the central portion of the subject lot.
The UST was removed from the ground by the demolition contractor. Prior to removal of the
UST, 450-gallons of petroleum Contact Water (PCW) was removed from the tank and
transported off -site for disposal During the UST removal olfactory indications of hydrocarbon
affected soil in the vicinity of the UST were detected.
On May 4, 2018, PM was contracted to collect a soil sample from the hydrocarbon affected soils
in the area of the former UST location. One soil sample (TP-1) was collected at the
approximate depth of the former basin bottom. The soil sample was submitted for laboratory
analysis of Total Petroleum Hydrocarbons — Gasoline Range Organics (TPH-GRO), Total
Petroleum Hydrocarbons — Diesel Range Organics (TPH-DRO). Review of the soil analytical
results indicated TPH-DRO at concentrations of TPH-DRO 3,680 milligrams per kilograms
(mg/kg) exceeding the North Carolina Department of Environmental Quality (NCDEQ) reporting
limit of 100 mg/kg.
Based on the results of the May 2018 sampling results, the property owner contacted the
NCDEQ notifying them of the release, which prompted a Notice of Regulatory Requirement
(NORR) issued by NCDEQ dated July 6, 2018. The NORR issued a requirement for Initial
PM Environmental, Inc.
Page 6

Initial Abatement Action Report for the Siblings, LLC Residence
Located at 411 Woodvale Place, Charlotte, North Carolina
PM Environmental, Inc., Project No. 15-4305-0-0002; August 28, 2018
Abatement Action (IAA) to be completed. Additionally, the NCDEQ assigned an incident
number (40822) for the release.
On August 7, 2018, PM performed the oversight of approximately 66.99 tons of hydrocarbon
affected soils from the former UST basin. The excavated soil was transported to Environmental
Soils, Inc. of Lattimore, North Carolina.
E. Site Check Report (Not Applicable to this Investigation)
F. UST Closure Report
In April, 2018 during demolition of the former onsite residence, one fuel oil UST was identified
and removed from the central portion of the subject property. Prior to removal of the UST, 450-
gallons of PCW was removed from the tank and transported off -site for disposal. During the
UST removal olfactory indications of hydrocarbon affected soil in the vicinity of the UST were
detected.
The UST was estimated to have a capacity of 550-gallons, measured 3.5 feet in diameter and
seven feet in length. Additional information pertaining to the date of installation, use, or
contents of the UST is unknown. The location of the tank is illustrated on Figure 2.
The overburden soil was removed with an excavator and stockpiled. The top of the tank was
encountered approximately two -feet below the ground surface. Tank measurements were:
• Diameter: 3.5 feet.
• Length: 7.0 feet.
• Capacity: 550 gallons.
• Construction: Steel.
Soil excavation and subsurface sampling are discussed in Section I.
G. Initial Response and Abatement Action
On August 7, 2018, PM performed the oversight during the excavation and disposal of
approximately 66.99 tons of hydrocarbon affected soil from the former UST basin.
H. Groundwater and Surface Water Investigation
Groundwater was not encountered during this Initial Abatement investigation. Surface water
was not addressed during this investigation.
I. Excavation of Contaminated Soil
Excavation and Sampling:
On August 7', 2018, PM performed the oversight of Elite Environmental Services, Inc. (Elite),
utilize an excavator to remove subsurface soil, including hydrocarbon affected soil, from the
former UST basin. The final excavation dimensions of the basin, located near the central
portion of the subject property, are as follows:
PM Environmental, Inc.
Page 7

Initial Abatement Action Report for the Siblings, LLC Residence
Located at 411 Woodvale Place, Charlotte, North Carolina
PM Environmental, Inc., Project No. 15-4305-0-0002; August 28, 2018
• Excavation Length (east -west): 14 feet.
• Excavation Width (north -south): 16 feet.
• Excavation Depth (bgs): 8 feet.
Soil was excavated approximately 1.5 to 2.5 feet laterally and approximately 2.0 feet vertically
from the former tank location, and directly loaded into dump trucks. The excavated soil
consisted primarily of silt and clay fill with a hydrocarbon odor. Overburden soil which did not
exhibit hydrocarbon odors or photoionization detector (PID) readings were stock piled onsite.
Five soil samples were collected from the sidewalls and base of the soil excavation (OE-1
through OE-5). The soil sample locations are illustrated on Figure 3.
Each of the soil samples were placed into laboratory containers, labeled, and transported to
Prism Laboratories, Inc. of Charlotte, North Carolina (a North Carolina certified laboratory)
under chain of custody procedures. The samples were analyzed for MADEP VPH / EPH,
volatile organic compounds (VOCs) per EPA Method 8260, and semi -volatile organic
compounds (SVOCs) per EPA Method 8270.
Following the soil excavation the basin was left open pending the results of the confirmation
samples.
Approximately 66.99 tons of hydrocarbon affected soil were removed from the former UST
basin. The excavated soil was transported to Environmental Soils, Inc. in Lattimore, North
Carolina for disposal. Soil disposal manifests are included in Appendix A.
Analvtical Results:
Soil samples were obtained from the excavated basin sidewalls and basin floor, examined, and
scanned with a photoionization detector (PID). The sample identifications, locations, and PID
results were as follows:
• OE-1, basin bottom, 8 ft. bgs, 0.0 ppm (PID).
• OE-2, west side wall, 5 ft. bgs, 0.0 ppm (PID).
• OE-3, south side wall, 5 ft. bgs, 0.0 ppm (PID).
• OE-4, east side wall, 5 ft. bgs, 0.0 ppm (PID).
• OE-5, north side wall, 5 ft. bgs, 0.0 ppm (PID).
Reference: ppm refers to parts -per -million; bgs refers to below ground surface.
A review of the analysis from the confirmation soil samples obtained from the former tank basin
revealed EPH Aromatic fraction C-11-C22 at a concentration of 28.9 milligrams per kilograms
(mg/kg) in sample OE-1 collected at the base of the excavation. The detected concentration of
C-11-C22 is below the NCDEQ most stringent soil to groundwater MSCC of 31 mg/kg. No
additional target analytes were detected in any of the confirmation samples exceeding the
laboratory MRLs.
The analytical results are summarized in Table B-3 and illustrated on Figure 3
PM Environmental, Inc.
Page 8

Initial Abatement Action Report for the Siblings, LLC Residence
Located at 411 Woodvale Place, Charlotte, North Carolina
PM Environmental, Inc., Project No. 15-4305-0-0002; August 28, 2018
The Soil to Groundwater MSCC criteria is used as the guideline for limiting the over -excavation
of soil in a UST basin. The analytical results indicated that the sidewall excavation was
completed within this guideline.
The analytical results are summarized in Table 3 along with the criteria used by the NCDEQ,
Division of Waste Management — UST Section. The laboratory analytical report and chain of
custody is provided in Appendix C.
J. Recommendations
Based on the over excavation, removal of hydrocarbon affected soils and results of confirmation
sampling results, PM recommends this incident be closed and the site granted no further action
(NFA) in accordance with the NCDEQ UST Section guidelines.
If you have any questions related to this document, please contact our Charlotte, North Carolina
office at 704-782-0555.
Sincerely,
PM ENVIRONMENTAL, INC.
Donald D. Warren
Regional Manager
John W. Hargraves, P.G.
Regional Manager/Senior Geologist
PM Environmental, Inc.
Page 9

Figures
Environmental
PM Ca & Engineering
ENVIRONMENTAL Services

MECKLENBURG COUNTY
SCALE 1:24,000
1 MILE
1/2 MILE
0
1 MILE
FIGURE 1
PROPERTY VICINITY MAP
USGS, 7.5 MINUTE SERIES
CHARLOTTE EAST, NC QUADRANGLE, 1967. PHOTO REVISED 1988.
Environmental
PROJ:
RESIDENTIAL PROPERTY
THIS IS NOT A LEGAL
SURVEY
DRN BY: CS
DATEg/23/2018
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VERIFY SCALE
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CHARLOTTE, NC
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FILE NAME:
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Environmental
pxq& Engineering
ENVIRONMENTAL Services
FIGURE 2
GENERALIZED DIAGRAM OF THE SUBJECT
PROPERTY AND ADJOINING PROPERTIES
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RESIDENTIAL PROPERTY
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CHARLOTTE, NC
RESIDENTIAL
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FIGURE 3
_ —
EXCAVATION SAMPLE LOCATION MAP
PROJ:
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411 WOODVALE PLACE
CHARLOTTE, NC
RESIDENTIAL
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SURVEY CS 8/23/2018
VERIFY SCALE CHKD BY: SCALE:
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Tables
Environmental
PM & Engineering
ENVIRONMENTAL Services

Table 1: Site History — UST/AST System and Other Release Information
Revision Date: Incident Number and Name: 40822/Siblings, LLC
Description
Was release
Date
Status
UST ID
Current/Last
Previous
Capacity
Construction
Tank
of Associated
associated
Tank
o***
Number
Contents*
Contents*
(in gallons)
Details **
Dimensions
Piping and
With the UST
Installed
UST
Pumps
System?
Remove
1
Steel
3.5'x 7'
Unknown
Unknown
April,
Yes
Petroleum
Petroleum
Approx. 550
2018
AST ID
Number
Current/Last
Contents*
Previous
Contents*
Capacity
(in gallons)
Construction
Details **
Tank
Dimensions
Description
of Associated
Piping and
Pumps
Date
Tank
Installed
Status
o ***
AST
Was release
associated
With the AST
System?
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
N/A
Incident
Number
Material
Released
Date of
Release
Description of Release
40822
Fuel Oil
Unknown —
A release of petroleum was suspected during UST removal in April 2018. Sample results
(suspected)
Discovered
confirmed a release which prompted the release notification.
on 10/1
* Gasoline (unleaded or leaded), diesel, used oil, waste oil, aviation fuel, etc., or pesticides, non -halogenated or halogenated solvents, etc.
** Fiberglass (single- or double -walled), steel (single- or double -walled), steel with FRP (single- or double -walled), steel with liner, other, unknown.
*** Currently operational, not in use or temporarily closed (specify date), permanently closed in place (specify date), permanently closed by removal
(specify date).

Table 2: Site History — UST/AST Owner/Operator and Other Responsible Party
Information
Revision Date:
Incident Number and Name: 40822/Siblings, LLC
UST ID Number
1
Facility ID Number: N/A
Name of Owner: Siblings, LLC
Dates of Operation: Unknown to Unknown
(mm/dd/yy to mm/dd.yy)
Street Address
234 Johnston Street
City
State
Zip
Telephone Number
Rock Hill
SC
28731
704-400-9481
Name of Operator
Date of Operation
(mm/dd/yy to mm/dd/yy)
Unknown
Unknown to Unknown
Street Address
411 Woodvale Place
City
State
Zip
Telephone Number
Charlotte
NC
28208
704-400-9481
Incident Number
40822
Name of Other Responsible Party
Date of Operation
(mm/dd/yy to mm/dd/yy)
Same as Owner
Street Address
City
State
Zip
Telephone Number
Add additional records for all owners, operators and responsible parties as necessary

TABLE 3
SUMMARY OF SOIL ANALYTICAL RESULTS
Siblings, LLC PROPERTY
TPH-DRO, ALIPHATICS/AROMATICS, VOCS, AND SVOCS
411 WOODVALE PLACE IN CHARLOTTE, NORTH CAROLINA
PM PROJECT # 15-4305-0-0002
NCDEQ INCIDENT NO. 40822
TOTAL PETROELUM HYDROCARBONS
o0
00
coN
DIESEL RANGE ORGANICS (TPH-DRO),
U
O
ALIPHATICS / AROMATICS, VOLATILE
U
U
U
o
Oj
U
O
p
ORGANIC COMPOUNDS (VOCs), AND
0
o
a)ICU
u
=
SEMI VOLATILE ORGANIC COMPOUNDS
n
E
~
0
Q
0
Q
a
(SVOCs). UNITS: (mg/kg)
Q
Q
°
Q
Q
Q
Chemical Abstract Service Number
(CAS#)
NA
NA
NA
NA
108-88-3
67-64-1
Various
Various
NA
Sample
Sample ID
Sample Date
Depth
MADEP VPH and EPH
VOCs
SVOCs
TPH
(bgTP-1
5/4/2018
5.0
NA
NA
NA
NA
NA
NA
NA
NA
3,680
OE-1
8/7/2018
8.0
BRL
BRL
3.82J
28.9
BRL
3.22J
BRL
BRL
NA
OE-2
8/7/2018
5.0
BRL
BRL
BRL
8.7J
BRL
2.63J
BRL
BRL
NA
OE-3
8/7/2018
5.0
BRL
BRL
3.55J
1 8.11J
BRL
3.52J
I BRL
BRL
NA
OE-4
8/7/2018
5.0
BRL
BRL
5.24J
8.5J
BRL
2.68J
BRL
BRL
NA
OE-5
8/7/2018
5.0
BRL
BRL
4.49J
7.05J
BRL
4.35J
BRL
BRL
NA
North Carolina Department of Environmental Quality, Division of Waste ManagementSoil, UST Section (NCDEQ UST)
Soil Criteria
TPH
NA
NA
NA
NA
NA
NA
NA
NA 100
Soil to Groundwater MSCC
68
540
IMMOBILE
31
4.3
24
Various
Various NA
Residential MSCC
939
1,500
31,000
469
1,200
14,000
Various
Various NA
Industrial/Commercial MSCC
24,528
40,000
810,000
12,264
32,000
360,000
Various
Various NA
Applicable Criterion/RBSL Exceeded
BOLD
Value Exceeds Applicable Criterion/RBSL
bgs
Below Ground Surface (feet)
BRL
Below the Laboratory Reporting Limit
NA
Not Applicable/Not Analyzed
NE
Not Established
TPH Total Petroleum Hydrocarbons
MADEP Massechusetts Department of Environmental Protection
J Estimated value above the laboratory method detecion limit (MDL) but below the Reporting Limit

Appendix A
Environmental
OPM & Engineering
ENVIRONMENTAL Services

����
ENVIRONMENTAL
,.
LOCATION
HAZ~�pT
ENVIRONMEN A LO�E� NEC. 28237
P.O.BOX3739�7� 332-56Q�
FAX �704) 375-7183
Manifest No•
__8 0 5._.� 5-
p,p. No, _
Job No•
�� a
RDOUS SPECIAL WASTE ''"
NON-HAZA
GENERATOR ���.��r�t,-r��,ro1'�t��t,��>��,►, I'flt.� �. �� ���c�,�
WORK CONTRp,CTED BY %�} %���.I�j�4- ' •'� � I
Bill To (If different from Information at left) �_ t(,. �J'`
rtG1NATING ADDRESS �' � � W"�+� `•
Att_I ADDRESS
;I'iY STATE
PHONE NO
1. PETROLEUM CONTACT WATER
2. OFF -SPEC LIGHT OIL : DIESEL OR GAS
3. NON -HAZARDOUS LIQUIDS
4. SEDIMENT OR SOLIDS
5. 55-GALLON DRUM REMOVED - SOLID OR EMPTY
&. 55-GALLON DRUM REMOVED -LIQUID
7.
A
ARRIVAL TIME: DEPARIURETIME:
22 �• Nw +,
NAM � - - Q I
ADDRESS Ai �j�_ ZIP _ " j � O
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ZIP ____----
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PHONE NO. 1
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CONTACT NAME r-f--•f �� �
GENERATOfi`5 CERTIFICATION: !hereby certify that theitio�n for Vansporta6onaaccording to applicablearegulationsnGeneratorlC stomer shlall reimbursellHAZ-MATets reasonable expenses
��: classified and packaged, and is in proper cond
and Charges for handling, analyzing, bading, preparing, transporting, storing or caring for nonconforming or ott spec waste, including costs of decontamination and cleaning of egwpment.
Generator must rlo[ HAZ-MAT of an changes to the waste stream prior to shipment. � %
S� c, K e J`4�L SUN fi,-.-.� Signature _ � - , __ _
Generator A^.;th'Jnzed Agen Name
713ANSiK2RTER IGenrrs�,n a�mpMe oJ, �CnnaMu�er I.�vnPlcre ru:
T•I2�,Ai4SPORTtiR rr n� Ir,•hn�
Sectic�i� III.• T TRANSPORTER II
HqZ�—MAT e. Name
ENVIRONMENTAL SERVICES f. Address --
p.p. BOX 37392 • CHARLOI-fE, N.C. 28237 ��
----"'—• /' g. Driver Name 1 Title
a paver Name%Tltie r_�_j i. Truck No.
c. Truck No h. Phone No.
b. Phone #o I Transporter II Permit Nos.
�yar8rxrs Waste Transporter Permits /� �"--
c -'� �•-,-'-'— �71) CERTIFICATE OF DISPOSAL
SAC"ILiTY I?v'FOR�
a. Phone Na. P 0=�_392
�CCt�aEi �� � 28237
��ttVtrOn�.�-r!��.�� b. Mailing Address. � tte N C
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?.� staff axl federal regulatsor�s n f� tub 9epera4on,
A er>d wi be d d n arx��'� �, G>en 11o�s a �soA'ed ar tiotatgn system 1<x P
reae►+ed pH a�els, ro r disposal, Manifest and certificate of disposal are on 81e.
5--• �n � ,�pers are��et� aruled to E.PA appro+ed faollties for p (�e
p�q 17A! # �fya/ for U1e � �p Q�,,,f�fi2. j31 S11�s`fro,,m�� wltivn seven days. _�-----_ DA , YEAR _
ff63 iR u� rirtld i+r,�..." r be P"�-"'__,-,___ �--- DATE MONTH_________-- _..
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f plgpO5ER •RINK • 1ST T.S.O.
f� •

Appendix B
Environmental
OPM & Engineering
ENVIRONMENTAL Services

ffm
Orlando, FL
The results set forth herein are provided by SGS North America Inc. a-Hl ydcopy 2. 0
Automated Report
Technical Report for
PM Environmental
Residential Property; Charlotte, NC
15-4305-0-0002
SGS Job Number: FA56562
Sampling Date: 08/07/ 18
Report to:
PM Environmental
8320 University Executive Park Dr Suite 106
Charlotte, NC 28262
warren(dbmenv. com
ATTN: Don Warren
Total number of pages in report: 69
Ac Fp
Test results contained within this data package meet the requirements Caitlin Brice, M. S.
of the National Environmental Laboratory Accreditation Program General Manager
and/or state specific certification programs as applicable.
Client Service contact: Muna Mohammed 407-425-6700
Certifications: FL(E83510), LA(03051), KS(E-10327), IL(200063), NC(573), NJ(FL002), NY(12022), SC(96038001)
DoD ELAP(ANAB L2229), AZ(AZ0806), CA(2937), TX(T104704404), PA(68-03573), VA(460177),
AK, AR, IA, KY, MA, MS, ND, NH, NV, OK, OR, UT, WA, WV
This report shall not be reproduced, except in its entirety, without the written approval of SGS.
Test results relate only to samples analyzed.
SGS North America Inc. • 4405 Vineland Road • Suite C-15 • Orlando, FL 32811 • tel: [phone] • fax: [phone]
SGS is the sole authority for authorizing edits or modifications to this document. Please share your ideas about
Unauthorized modification of this report is strictly prohibited. how we can serve you better at:
Review standard terms at: http://www.sgs.com/en/terms-and-conditions [e-mail]
1 of 69
FA56562

Sections:
Table of Contents
-I-
Section1: Sample Summary...................................................................................................
3
Section2: Summary of Hits....................................................................................................
4
Section3: Sample Results........................................................................................................
5
3.1: FA56562-1: OE-1.........................................................................................................
6
3.2: FA56562-2: OE-2.........................................................................................................
13
3.3: FA56562-3: OE-3.........................................................................................................
20
3.4: FA56562-4: OE-4.........................................................................................................
27
3.5: FA56562-5: OE-5.........................................................................................................
34
Section4: Misc. Forms............................................................................................................
41
4.1: Chain of Custody...........................................................................................................
42
Section5: MS Volatiles - QC Data Summaries.....................................................................
44
5.1: Method Blank Summary................................................................................................
45
5.2: Blank Spike Summary...................................................................................................
48
5.3: Matrix Spike/Matrix Spike Duplicate Summary...........................................................
51
Section 6: MS Semi-volatiles - QC Data Summaries............................................................
54
6.1: Method Blank Summary................................................................................................
55
6.2: Blank Spike Summary...................................................................................................
57
6.3: Matrix Spike/Matrix Spike Duplicate Summary...........................................................
59
Section 7: GC Volatiles - QC Data Summaries.....................................................................
61
7.1: Method Blank Summary................................................................................................
62
7.2: Blank Spike/Blank Spike Duplicate Summary..............................................................
63
7.3: Matrix Spike Summary..................................................................................................
64
7ADuplicate Summary.......................................................................................................
65
Section 8: GC/LC Semi-volatiles - QC Data Summaries.....................................................
66
8.1: Method Blank Summary................................................................................................
67
8.2: Blank Spike/Blank Spike Duplicate Summary..............................................................
68
8.3: Duplicate Summary.......................................................................................................
69
W,

SGS North America Inc.
Sample Summary
PM Environmental
Residential Property; Charlotte, NC
Project No: 15-4305-0-0002
Job No: FA56562
Sample Collected Matrix Client
Number Date Time By Received Code Type Sample I D
FA56562-1 08/07/18 12:00 DW 08/09/18 SO Soil OE-1
FA56562-2 08/07/18 12:30 DW 08/09/18 SO Soil OE-2
FA56562-3 08/07/18 12:45 DW 08/09/18 SO Soil OE-3
FA56562-4 08/07/18 13:00 DW 08/09/18 SO Soil OE-4
FA56562-5 08/07/18 13:15 DW 08/09/18 SO Soil OE-5
Soil samples reported on a dry weight basis unless otherwise indicated on result page.
6 3 of 69
FA56562

Summary of Hits
Job Number: FA56562
Account: PM Environmental
Project: Residential Property; Charlotte, NC
Collected: 08/07/ 18
Lab Sample ID Client Sample ID Result/
Analyte Qual RL MDL Units Method
Page 1 of 1
FA56562-1 OE-1
Acetone a
3.22 JB
4.6
0.91
mg/kg
SW846 8260B
C11-C22 Aromatics (Unadj.)
28.9
13
5.3
mg/kg
MADEP EPH REV 1.1
C 19-C36 Aliphatics
3.82 J
13
3.3
mg/kg
MADEP EPH REV 1.1
FA56562-2 OE-2
Acetone a
2.63 JB
3.7
0.74
mg/kg
SW846 8260B
C11-C22 Aromatics (Unadj.)
8.70 J
12
4.7
mg/kg
MADEP EPH REV 1.1
FA56562-3 OE-3
Acetone a
3.52 JB
4.9
0.97
mg/kg
SW846 8260B
C11-C22 Aromatics (Unadj.)
8.11 J
12
4.8
mg/kg
MADEP EPH REV 1.1
C 19-C36 Aliphatics
3.55 J
12
3.0
mg/kg
MADEP EPH REV 1.1
FA56562-4 OE-4
Acetone a
2.68 JB
4.1
0.83
mg/kg
SW846 8260B
Toluene a
0.236 J
0.41
0.083
mg/kg
SW846 8260B
C11-C22 Aromatics (Unadj.)
8.50 J
13
5.2
mg/kg
MADEP EPH REV 1.1
C 19-C36 Aliphatics
5.24 J
13
3.2
mg/kg
MADEP EPH REV 1.1
FA56562-5 OE-5
Acetone a
4.35 JB
5.8
1.2
mg/kg
SW846 8260B
Toluene a
0.433 J
0.58
0.12
mg/kg
SW846 8260B
C11-C22 Aromatics (Unadj.)
7.05 J
13
5.4
mg/kg
MADEP EPH REV 1.1
C 19-C36 Aliphatics
4.49 J
13
3.4
mg/kg
MADEP EPH REV 1.1
(a) Dilution required due to matrix interference (sample foamed). Suspected laboratory contaminant.
6 4of69
FA56562

i
SG$f
Orlando, FL im
Section 3
Sample Results
Report of Analysis
6 5of69
FA56562

SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:
OE-1
Lab Sample ID:
FA56562-1 Date Sampled: 08/07/18
Matrix:
SO - Soil Date Received: 08/09/ 18
Method:
SW846 8260B Percent Solids: 74.7
Project:
Residential Property; Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 3C1453.D 1 08/14/18 17:47 SP n/a n/a V3C61
Run #2
Initial Weight Final Volume Methanol Aliquot
Run # 1 4.51 g 5.0 ml 100 ul
Run #2
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units
67-64-1
Acetone b
3.22
4.6
0.91
mg/kg
71-43-2
Benzene
ND
0.46
0.11
mg/kg
108-86-1
Bromobenzene
ND
0.46
0.091
mg/kg
74-97-5
Bromochloromethane
ND
0.46
0.13
mg/kg
75-27-4
Bromodichloromethane
ND
0.46
0.091
mg/kg
75-25-2
Bromoform
ND
0.46
0.091
mg/kg
78-93-3
2-Butanone (MEK)
ND
2.3
0.66
mg/kg
104-51-8
n-Butylbenzene
ND
0.46
0.091
mg/kg
135-98-8
sec-Butylbenzene
ND
0.46
0.091
mg/kg
98-06-6
tert-Butylbenzene
ND
0.46
0.091
mg/kg
56-23-5
Carbon Tetrachloride °
ND
0.46
0.093
mg/kg
108-90-7
Chlorobenzene
ND
0.46
0.091
mg/kg
75-00-3
Chloroethanec
ND
0.46
0.18
mg/kg
67-66-3
Chloroform
ND
0.46
0.12
mg/kg
95-49-8
o-Chlorotoluene
ND
0.46
0.091
mg/kg
106-43-4
p-Chlorotoluene
ND
0.46
0.091
mg/kg
124-48-1
Dibromochloromethane
ND
0.46
0.091
mg/kg
106-93-4
1,2-Dibromoethane
ND
0.46
0.091
mg/kg
75-71-8
Dichlorodifluoromethane
ND
0.46
0.18
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.46
0.091
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.46
0.091
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.46
0.10
mg/kg
75-34-3
1, 1 -Dichloroethane
ND
0.46
0.16
mg/kg
107-06-2
1,2-Dichloroethane
ND
0.46
0.091
mg/kg
75-35-4
1, 1 -Dichloroethylene
ND
0.46
0.091
mg/kg
156-59-2
cis-1,2-Dichloroethylene
ND
0.46
0.13
mg/kg
156-60-5
trans-1,2-Dichloroethylene
ND
0.46
0.091
mg/kg
78-87-5
1,2-Dichloropropane
ND
0.46
0.091
mg/kg
142-28-9
1,3-Dichloropropane
ND
0.46
0.091
mg/kg
594-20-7
2,2-Dichloropropane
ND
0.46
0.091
mg/kg
563-58-6
1, 1 -Dichloropropene
ND
0.46
0.093
mg/kg
10061-01-5
cis- 1, 3-Dichloropropene
ND
0.46
0.091
mg/kg
"
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
01
6 of 69
FA56562

SGS North America Inc.
Report of Analysis
Page 2 of 3
Client Sample ID:
OE-1
Lab Sample ID:
FA56562-1 Date Sampled: 08/07/18
Matrix:
SO - Soil Date Received: 08/09/ 18
Method:
SW846 8260B Percent Solids: 74.7
Project:
Residential Property; Charlotte, NC
VOA List for NC, May 2012
CAS No.
Compound
Result
RL
MDL
Units Q
10061-02-6
trans- 1, 3-Dichloropropene
ND
0.46
0.091
mg/kg
108-20-3
Di -Isopropyl Ether
ND
0.46
0.21
mg/kg
64-17-5
Ethyl Alcohol
ND
36
6.8
mg/kg
100-41-4
Ethylbenzene
ND
0.46
0.091
mg/kg
591-78-6
2-Hexanone
ND
2.3
0.68
mg/kg
98-82-8
Isopropylbenzene
ND
0.46
0.091
mg/kg
99-87-6
p-Isopropyltoluene
ND
0.46
0.091
mg/kg
74-83-9
Methyl Bromide
ND
0.46
0.18
mg/kg
74-87-3
Methyl Chloride
ND
0.46
0.18
mg/kg
75-09-2
Methylene Chloride
ND
0.91
0.36
mg/kg
108-10-1
4-Methyl-2-pentanone (MIBK) ND
2.3
0.68
mg/kg
1634-04-4
Methyl Tert Butyl Ether
ND
0.46
0.091
mg/kg
91-20-3
Naphthalene
ND
0.46
0.18
mg/kg
103-65-1
n-Propylbenzene
ND
0.46
0.091
mg/kg
100-42-5
Styrene
ND
0.46
0.091
mg/kg
630-20-6
1, 1, 1,2-Tetrachloroethane
ND
0.46
0.094
mg/kg
79-34-5
1,1,2,2-Tetrachloroethane
ND
0.46
0.091
mg/kg
127-18-4
Tetrachloroethylene
ND
0.46
0.12
mg/kg
108-88-3
Toluene
ND
0.46
0.091
mg/kg
87-61-6
1,2,3-Trichlorobenzene
ND
0.46
0.13
mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
0.46
0.091
mg/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
0.46
0.091
mg/kg
79-00-5
1, 1, 2-Trichloroethane
ND
0.46
0.091
mg/kg
79-01-6
Trichloroethylene
ND
0.46
0.091
mg/kg
75-69-4
Trichlorofluoromethane
ND
0.46
0.18
mg/kg
96-18-4
1,2,3-Trichloropropane
ND
0.46
0.11
mg/kg
95-63-6
1,2,4-Trimethylbenzene
ND
0.46
0.091
mg/kg
108-67-8
1,3,5-Trimethylbenzene
ND
0.46
0.091
mg/kg
108-05-4
Vinyl Acetate
ND
2.3
1.5
mg/kg
75-01-4
Vinyl Chloride
ND
0.46
0.091
mg/kg
m,p-Xylene
ND
0.91
0.10
mg/kg
95-47-6
o-Xylene
ND
0.46
0.091
mg/kg
1330-20-7
Xylene (total)
ND
1.4
0.19
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
111%
75-124%
17060-07-0
1,2-Dichloroethane-D4
109%
72-135%
2037-26-5
Toluene-D8
107%
75-126%
460-00-4
4-Bromofluorobenzene
99%
71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
01
7 of 69
FA56562

SGS North America Inc.
Report of Analysis
Page 3 of 3 L
Client Sample ID:
OE-1
Lab Sample ID:
FA56562-1 Date Sampled: 08/07/18
Matrix:
SO - Soil Date Received: 08/09/ 18
Method:
SW846 8260B Percent Solids: 74.7
Project:
Residential Property; Charlotte, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
(a) Dilution required due to matrix interference (sample foamed).
(b) Suspected laboratory contaminant.
(c) Associated CCV outside of control limits high, sample was ND.
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
6 8 of 69
FA56562

SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID: OE-1
Lab Sample ID: FA56562-1 Date Sampled: 08/07/18
Matrix: SO - Soil Date Received: 08/09/ 18
Method: SW846 8270D SW846 3550C Percent Solids: 74.7
Project: Residential Property; Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 9I002129.1) 1 08/16/18 22:09 MV 08/14/18 12:15 OP71335 S9173
Run #2
Initial Weight Final Volume
Run #1 30.1 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No. Compound Result RL MDL Units
65-85-0
Benzoic Acid
ND
1.1
0.22
mg/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
0.22
0.025
mg/kg
95-57-8
2-Chlorophenol
ND
0.22
0.027
mg/kg
120-83-2
2,4-Dichlorophenol
ND
0.22
0.026
mg/kg
105-67-9
2,4-Dimethylphenol
ND
0.22
0.059
mg/kg
51-28-5
2,4-Dinitrophenol
ND
1.1
0.22
mg/kg
534-52-1
4,6-Dinitro-o-cresol
ND
0.44
0.089
mg/kg
95-48-7
2-Methylphenol
ND
0.22
0.027
mg/kg
3&4-Methylphenol
ND
0.22
0.037
mg/kg
88-75-5
2-Nitrophenol
ND
0.22
0.024
mg/kg
100-02-7
4-Nitrophenol
ND
1.1
0.22
mg/kg
87-86-5
Pentachlorophenol
ND
1.1
0.22
mg/kg
108-95-2
Phenol
ND
0.22
0.022
mg/kg
88-06-2
2,4,6-Trichlorophenol
ND
0.22
0.026
mg/kg
83-32-9
Acenaphthene
ND
0.22
0.024
mg/kg
208-96-8
Acenaphthylene
ND
0.22
0.022
mg/kg
120-12-7
Anthracene
ND
0.22
0.025
mg/kg
56-55-3
Benzo(a)anthracene
ND
0.22
0.022
mg/kg
50-32-8
Benzo(a)pyrene
ND
0.22
0.026
mg/kg
205-99-2
Benzo(b)fluoranthene
ND
0.22
0.024
mg/kg
191-24-2
Benzo(g,h,i)perylene
ND
0.22
0.023
mg/kg
207-08-9
Benzo(k)fluoranthene
ND
0.22
0.029
mg/kg
100-51-6
Benzyl Alcohol
ND
0.22
0.022
mg/kg
101-55-3
4-Bromophenyl phenyl ether
ND
0.22
0.023
mg/kg
85-68-7
Butyl benzyl phthalate
ND
0.22
0.044
mg/kg
106-47-8
4-Chloroaniline
ND
0.22
0.056
mg/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
0.22
0.022
mg/kg
111-44-4
bis(2-Chloroethyl)ether
ND
0.22
0.026
mg/kg
108-60-1
2,2'-Oxybis(1-chloropropane)
ND
0.22
0.028
mg/kg
91-58-7
2-Chloronaphthalene
ND
0.22
0.022
mg/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.22
0.022
mg/kg
218-01-9
Chrysene
ND
0.22
0.023
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
01
9 of 69
FA56562

SGS North America Inc.
Report of Analysis
Client Sample ID: OE-1
Lab Sample ID: FA56562-1 Date Sampled: 08/07/18
Matrix: SO - Soil Date Received: 08/09/ 18
Method: SW846 8270D SW846 3550C Percent Solids: 74.7
Project: Residential Property; Charlotte, NC
ABN List for NC, May 2012
CAS No.
Compound
Result
RL
MDL
Units Q
53-70-3
Dibenzo(a,h)anthracene
ND
0.22
0.028
mg/kg
132-64-9
Dibenzofaran
ND
0.22
0.022
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.22
0.022
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.22
0.024
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.22
0.030
mg/kg
91-94-1
3,3'-Dichlorobenzidine
ND
0.22
0.053
mg/kg
84-66-2
Diethyl Phthalate
ND
0.44
0.044
mg/kg
131-11-3
Dimethyl Phthalate
ND
0.22
0.044
mg/kg
117-84-0
Di-n-octyl Phthalate
ND
0.22
0.044
mg/kg
84-74-2
Di-n-butyl Phthalate
ND
0.44
0.089
mg/kg
122-66-7
1,2-Diphenylhydrazine
ND
0.22
0.022
mg/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
0.44
0.044
mg/kg
206-44-0
Fluoranthene
ND
0.22
0.022
mg/kg
86-73-7
Fluorene
ND
0.22
0.024
mg/kg
118-74-1
Hexachlorobenzene
ND
0.22
0.023
mg/kg
87-68-3
Hexachlorobutadiene
ND
0.22
0.023
mg/kg
77-47-4
Hexachlorocyclopentadiene
ND
0.22
0.044
mg/kg
67-72-1
Hexachloroethane
ND
0.22
0.026
mg/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.22
0.027
mg/kg
78-59-1
Isophorone
ND
0.22
0.022
mg/kg
90-12-0
1-Methylnaphthalene
ND
0.22
0.022
mg/kg
91-57-6
2-Methylnaphthalene
ND
0.22
0.022
mg/kg
91-20-3
Naphthalene
ND
0.22
0.022
mg/kg
98-95-3
Nitrobenzene
ND
0.22
0.022
mg/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
0.22
0.022
mg/kg
86-30-6
N-Nitrosodiphenylamine
ND
0.22
0.024
mg/kg
85-01-8
Phenanthrene
ND
0.22
0.022
mg/kg
129-00-0
Pyrene
ND
0.22
0.026
mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
0.22
0.026
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
71%
40-102%
4165-62-2
Phenol-d5
75%
41-100%
118-79-6
2,4,6-Tribromophenol
76%
42-108%
4165-60-0
Nitrobenzene-d5
62%
40-105%
321-60-8
2-Fluorobiphenyl
80%
43-107%
1718-51-0
Terphenyl-dl4
94%
45-119%
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
01
10 of 69
FA56562

SGS North America Inc.
Report of Analysis Page 1 of 1 s
Client Sample ID: OE-1
Lab Sample ID: FA56562-1 Date Sampled: 08/07/18
Matrix: SO - Soil Date Received: 08/09/ 18
Method: MADEP VPH REV 1.1 Percent Solids: 74.7
Project: Residential Property; Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 UU025483.D 1 08/15/18 22:02 NM n/a n/a GUU1319
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 4.75 g 5.1 ml 100 ul
Run #2
MADEP VPH List
CAS No.
Compound
Result
RL
MDL Units Q
C5- C8 Aliphatics (Unadj.)
ND
8.9
3.1 mg/kg
C9- C12 Aliphatics (Unadj.)
ND
8.9
3.1 mg/kg
C9- C10 Aromatics (Unadj.)
ND
8.9
3.1 mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
460-00-4
BFB
119%
70-130%
460-00-4
BFB
113%
70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 11 of 69
FA56562

SGS North America Inc.
Report of Analysis
Client Sample ID: OE-1
Lab Sample ID: FA56562-1 Date Sampled: 08/07/18
Matrix: SO - Soil Date Received: 08/09/ 18
Method: MADEP EPH REV 1.1 SW846 3546 Percent Solids: 74.7
Project: Residential Property; Charlotte, NC
Page 1 of 1 j
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN023227.13 1 08/15/18 19:05 NJ 08/13/18 09:30 OP71311 GNN1137
Run #2
Initial Weight Final Volume
Run # 1 20.3 g 2.0 ml
Run #2
MAEPH List
CAS No.
Compound
Result
RL
MDL Units Q
C11-C22 Aromatics (Unadj.)
28.9
13
5.3 mg/kg
C9-C18 Aliphatics
ND
13
3.3 mg/kg
C19-C36 Aliphatics
3.82
13
3.3 mg/kg J
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
3386-33-2
1-Chlorooctadecane
80%
40-140%
580-13-2
2-Bromonaphthalene
100%
40-140%
84-15-1
o-Terphenyl
86%
40-140%
321-60-8
2-Fluorobiphenyl
85%
40-140%
ND = Not detected MDL = Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
�1%6 12 of 69
FA56562

SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:
OE-2
Lab Sample ID:
FA56562-2 Date Sampled: 08/07/ 18
Matrix:
SO - Soil Date Received: 08/09/ 18
Method:
SW846 8260B Percent Solids: 83.9
Project:
Residential Property; Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 3C1454.D 1 08/14/18 18:11 SP n/a n/a V3C61
Run #2
Initial Weight Final Volume Methanol Aliquot
Run # 1 4.66 g 5.0 ml 100 ul
Run #2
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units
67-64-1
Acetone b
2.63
3.7
0.74
mg/kg
71-43-2
Benzene
ND
0.37
0.090
mg/kg
108-86-1
Bromobenzene
ND
0.37
0.074
mg/kg
74-97-5
Bromochloromethane
ND
0.37
0.11
mg/kg
75-27-4
Bromodichloromethane
ND
0.37
0.074
mg/kg
75-25-2
Bromoform
ND
0.37
0.074
mg/kg
78-93-3
2-Butanone (MEK)
ND
1.8
0.53
mg/kg
104-51-8
n-Butylbenzene
ND
0.37
0.074
mg/kg
135-98-8
sec-Butylbenzene
ND
0.37
0.074
mg/kg
98-06-6
tert-Butylbenzene
ND
0.37
0.074
mg/kg
56-23-5
Carbon Tetrachloride °
ND
0.37
0.075
mg/kg
108-90-7
Chlorobenzene
ND
0.37
0.074
mg/kg
75-00-3
Chloroethane c
ND
0.37
0.15
mg/kg
67-66-3
Chloroform
ND
0.37
0.098
mg/kg
95-49-8
o-Chlorotoluene
ND
0.37
0.074
mg/kg
106-43-4
p-Chlorotoluene
ND
0.37
0.074
mg/kg
124-48-1
Dibromochloromethane
ND
0.37
0.074
mg/kg
106-93-4
1,2-Dibromoethane
ND
0.37
0.074
mg/kg
75-71-8
Dichlorodifluoromethane
ND
0.37
0.15
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.37
0.074
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.37
0.074
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.37
0.085
mg/kg
75-34-3
1, 1 -Dichloroethane
ND
0.37
0.13
mg/kg
107-06-2
1,2-Dichloroethane
ND
0.37
0.074
mg/kg
75-35-4
1, 1 -Dichloroethylene
ND
0.37
0.074
mg/kg
156-59-2
cis-1,2-Dichloroethylene
ND
0.37
0.10
mg/kg
156-60-5
trans-1,2-Dichloroethylene
ND
0.37
0.074
mg/kg
78-87-5
1,2-Dichloropropane
ND
0.37
0.074
mg/kg
142-28-9
1,3-Dichloropropane
ND
0.37
0.074
mg/kg
594-20-7
2,2-Dichloropropane
ND
0.37
0.074
mg/kg
563-58-6
1, 1 -Dichloropropene
ND
0.37
0.075
mg/kg
10061-01-5
cis- 1, 3-Dichloropropene
ND
0.37
0.074
mg/kg
"
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 13 of 69
FA56562

SGS North America Inc.
Report of Analysis
Page 2 of 3
Client Sample ID:
OE-2
Lab Sample ID:
FA56562-2 Date Sampled: 08/07/ 18
Matrix:
SO - Soil Date Received: 08/09/ 18
Method:
SW846 8260B Percent Solids: 83.9
Project:
Residential Property; Charlotte, NC
VOA List for NC, May 2012
CAS No.
Compound
Result
RL
MDL
Units Q
10061-02-6
trans- 1, 3-Dichloropropene
ND
0.37
0.074
mg/kg
108-20-3
Di -Isopropyl Ether
ND
0.37
0.17
mg/kg
64-17-5
Ethyl Alcohol
ND
29
5.5
mg/kg
100-41-4
Ethylbenzene
ND
0.37
0.074
mg/kg
591-78-6
2-Hexanone
ND
1.8
0.55
mg/kg
98-82-8
Isopropylbenzene
ND
0.37
0.074
mg/kg
99-87-6
p-Isopropyltoluene
ND
0.37
0.074
mg/kg
74-83-9
Methyl Bromide
ND
0.37
0.15
mg/kg
74-87-3
Methyl Chloride
ND
0.37
0.15
mg/kg
75-09-2
Methylene Chloride
ND
0.74
0.29
mg/kg
108-10-1
4-Methyl-2-pentanone (MIBK) ND
1.8
0.55
mg/kg
1634-04-4
Methyl Tert Butyl Ether
ND
0.37
0.074
mg/kg
91-20-3
Naphthalene
ND
0.37
0.15
mg/kg
103-65-1
n-Propylbenzene
ND
0.37
0.074
mg/kg
100-42-5
Styrene
ND
0.37
0.074
mg/kg
630-20-6
1, 1, 1,2-Tetrachloroethane
ND
0.37
0.076
mg/kg
79-34-5
1,1,2,2-Tetrachloroethane
ND
0.37
0.074
mg/kg
127-18-4
Tetrachloroethylene
ND
0.37
0.094
mg/kg
108-88-3
Toluene
ND
0.37
0.074
mg/kg
87-61-6
1,2,3-Trichlorobenzene
ND
0.37
0.10
mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
0.37
0.074
mg/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
0.37
0.074
mg/kg
79-00-5
1, 1, 2-Trichloroethane
ND
0.37
0.074
mg/kg
79-01-6
Trichloroethylene
ND
0.37
0.074
mg/kg
75-69-4
Trichlorofluoromethane
ND
0.37
0.15
mg/kg
96-18-4
1,2,3-Trichloropropane
ND
0.37
0.092
mg/kg
95-63-6
1,2,4-Trimethylbenzene
ND
0.37
0.074
mg/kg
108-67-8
1,3,5-Trimethylbenzene
ND
0.37
0.074
mg/kg
108-05-4
Vinyl Acetate
ND
1.8
1.2
mg/kg
75-01-4
Vinyl Chloride
ND
0.37
0.074
mg/kg
m,p-Xylene
ND
0.74
0.081
mg/kg
95-47-6
o-Xylene
ND
0.37
0.074
mg/kg
1330-20-7
Xylene (total)
ND
1.1
0.15
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
112%
75-124%
17060-07-0
1,2-Dichloroethane-D4
108%
72-135%
2037-26-5
Toluene-D8
110%
75-126%
460-00-4
4-Bromofluorobenzene
94%
71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
01
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SGS North America Inc.
Report of Analysis
Page 3 of 3 N
Client Sample ID:
OE-2
Lab Sample ID:
FA56562-2 Date Sampled: 08/07/ 18
Matrix:
SO - Soil Date Received: 08/09/ 18
Method:
SW846 8260B Percent Solids: 83.9
Project:
Residential Property; Charlotte, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
(a) Dilution required due to matrix interference (sample foamed).
(b) Suspected laboratory contaminant.
(c) Associated CCV outside of control limits high, sample was ND.
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
6 15 of 69
FA56562

SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID: OE-2
Lab Sample ID: FA56562-2 Date Sampled: 08/07/ 18
Matrix: SO - Soil Date Received: 08/09/ 18
Method: SW846 8270D SW846 3550C Percent Solids: 83.9
Project: Residential Property; Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 9I002130.1) 1 08/16/18 22:36 MV 08/14/18 12:15 OP71335 S9173
Run #2
Initial Weight Final Volume
Run #1 30.0 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No. Compound Result RL MDL Units
65-85-0
Benzoic Acid
ND
0.99
0.20
mg/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
0.20
0.022
mg/kg
95-57-8
2-Chlorophenol
ND
0.20
0.024
mg/kg
120-83-2
2,4-Dichlorophenol
ND
0.20
0.023
mg/kg
105-67-9
2,4-Dimethylphenol
ND
0.20
0.053
mg/kg
51-28-5
2,4-Dinitrophenol
ND
0.99
0.20
mg/kg
534-52-1
4,6-Dinitro-o-cresol
ND
0.40
0.079
mg/kg
95-48-7
2-Methylphenol
ND
0.20
0.024
mg/kg
3&4-Methylphenol
ND
0.20
0.033
mg/kg
88-75-5
2-Nitrophenol
ND
0.20
0.022
mg/kg
100-02-7
4-Nitrophenol
ND
0.99
0.20
mg/kg
87-86-5
Pentachlorophenol
ND
0.99
0.20
mg/kg
108-95-2
Phenol
ND
0.20
0.020
mg/kg
88-06-2
2,4,6-Trichlorophenol
ND
0.20
0.023
mg/kg
83-32-9
Acenaphthene
ND
0.20
0.021
mg/kg
208-96-8
Acenaphthylene
ND
0.20
0.020
mg/kg
120-12-7
Anthracene
ND
0.20
0.022
mg/kg
56-55-3
Benzo(a)anthracene
ND
0.20
0.020
mg/kg
50-32-8
Benzo(a)pyrene
ND
0.20
0.023
mg/kg
205-99-2
Benzo(b)fluoranthene
ND
0.20
0.022
mg/kg
191-24-2
Benzo(g,h,i)perylene
ND
0.20
0.021
mg/kg
207-08-9
Benzo(k)fluoranthene
ND
0.20
0.026
mg/kg
100-51-6
Benzyl Alcohol
ND
0.20
0.020
mg/kg
101-55-3
4-Bromophenyl phenyl ether
ND
0.20
0.021
mg/kg
85-68-7
Butyl benzyl phthalate
ND
0.20
0.040
mg/kg
106-47-8
4-Chloroaniline
ND
0.20
0.050
mg/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
0.20
0.020
mg/kg
111-44-4
bis(2-Chloroethyl)ether
ND
0.20
0.023
mg/kg
108-60-1
2,2'-Oxybis(1-chloropropane)
ND
0.20
0.025
mg/kg
91-58-7
2-Chloronaphthalene
ND
0.20
0.020
mg/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.20
0.020
mg/kg
218-01-9
Chrysene
ND
0.20
0.020
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
01
16 of 69
FA56562

SGS North America Inc.
Report of Analysis
Client Sample ID: OE-2
Lab Sample ID: FA56562-2 Date Sampled: 08/07/ 18
Matrix: SO - Soil Date Received: 08/09/ 18
Method: SW846 8270D SW846 3550C Percent Solids: 83.9
Project: Residential Property; Charlotte, NC
ABN List for NC, May 2012
CAS No.
Compound
Result
RL
MDL
Units Q
53-70-3
Dibenzo(a,h)anthracene
ND
0.20
0.025
mg/kg
132-64-9
Dibenzofaran
ND
0.20
0.020
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.20
0.020
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.20
0.021
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.20
0.026
mg/kg
91-94-1
3,3'-Dichlorobenzidine
ND
0.20
0.047
mg/kg
84-66-2
Diethyl Phthalate
ND
0.40
0.040
mg/kg
131-11-3
Dimethyl Phthalate
ND
0.20
0.040
mg/kg
117-84-0
Di-n-octyl Phthalate
ND
0.20
0.040
mg/kg
84-74-2
Di-n-butyl Phthalate
ND
0.40
0.079
mg/kg
122-66-7
1,2-Diphenylhydrazine
ND
0.20
0.020
mg/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
0.40
0.040
mg/kg
206-44-0
Fluoranthene
ND
0.20
0.020
mg/kg
86-73-7
Fluorene
ND
0.20
0.021
mg/kg
118-74-1
Hexachlorobenzene
ND
0.20
0.020
mg/kg
87-68-3
Hexachlorobutadiene
ND
0.20
0.020
mg/kg
77-47-4
Hexachlorocyclopentadiene
ND
0.20
0.040
mg/kg
67-72-1
Hexachloroethane
ND
0.20
0.023
mg/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.20
0.024
mg/kg
78-59-1
Isophorone
ND
0.20
0.020
mg/kg
90-12-0
1-Methylnaphthalene
ND
0.20
0.020
mg/kg
91-57-6
2-Methylnaphthalene
ND
0.20
0.020
mg/kg
91-20-3
Naphthalene
ND
0.20
0.020
mg/kg
98-95-3
Nitrobenzene
ND
0.20
0.020
mg/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
0.20
0.020
mg/kg
86-30-6
N-Nitrosodiphenylamine
ND
0.20
0.021
mg/kg
85-01-8
Phenanthrene
ND
0.20
0.020
mg/kg
129-00-0
Pyrene
ND
0.20
0.023
mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
0.20
0.023
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
69%
40-102%
4165-62-2
Phenol-d5
73%
41-100%
118-79-6
2,4,6-Tribromophenol
73%
42-108%
4165-60-0
Nitrobenzene-d5
59%
40-105%
321-60-8
2-Fluorobiphenyl
77%
43-107%
1718-51-0
Terphenyl-dl4
92%
45-119%
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
01
17 of 69
FA56562

SGS North America Inc.
Report of Analysis Page 1 of 1 N
Client Sample ID: OE-2
Lab Sample ID: FA56562-2 Date Sampled: 08/07/ 18
Matrix: SO - Soil Date Received: 08/09/ 18
Method: MADEP VPH REV 1.1 Percent Solids: 83.9
Project: Residential Property; Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 UU025484.D 1 08/15/18 22:33 NM n/a n/a GUU1319
Run #2
Initial Weight Final Volume Methanol Aliquot
Run # 1 4.10 g 5.1 ml 100 ul
Run #2
MADEP VPH List
CAS No.
Compound
Result
RL
MDL Units Q
C5- C8 Aliphatics (Unadj.)
ND
8.4
2.9 mg/kg
C9- C12 Aliphatics (Unadj.)
ND
8.4
2.9 mg/kg
C9- C10 Aromatics (Unadj.)
ND
8.4
2.9 mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
460-00-4
BFB
120%
70-130%
460-00-4
BFB
115%
70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 18 of 69
FA56562

SGS North America Inc.
Report of Analysis
Client Sample ID: OE-2
Lab Sample ID: FA56562-2 Date Sampled: 08/07/ 18
Matrix: SO - Soil Date Received: 08/09/ 18
Method: MADEP EPH REV 1.1 SW846 3546 Percent Solids: 83.9
Project: Residential Property; Charlotte, NC
Page 1 of 1 N
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN023228.13 1 08/15/18 19:37 NJ 08/13/18 09:30 OP71311 GNN1137
Run #2
Initial Weight Final Volume
Run # 1 20.5 g 2.0 ml
Run #2
MAEPH List
CAS No.
Compound
Result
RL
MDL Units Q
C11-C22 Aromatics (Unadj.)
8.70
12
4.7 mg/kg J
C9-C18 Aliphatics
ND
12
2.9 mg/kg
C19-C36 Aliphatics
ND
12
2.9 mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
3386-33-2
1-Chlorooctadecane
71%
40-140%
580-13-2
2-Bromonaphthalene
70%
40-140%
84-15-1
o-Terphenyl
76%
40-140%
321-60-8
2-Fluorobiphenyl
58%
40-140%
ND = Not detected MDL = Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
6 19 of 69
FA56562

SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:
OE-3
Lab Sample ID:
FA56562-3 Date Sampled: 08/07/ 18
Matrix:
SO - Soil Date Received: 08/09/ 18
Method:
SW846 8260B Percent Solids: 80.6
Project:
Residential Property; Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 3C1455.D 1 08/14/18 18:34 SP n/a n/a V3C61
Run #2
Initial Weight Final Volume Methanol Aliquot
Run # 1 3.63 g 5.0 ml 100 ul
Run #2
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units
67-64-1
Acetone b
3.52
4.9
0.97
mg/kg
71-43-2
Benzene
ND
0.49
0.12
mg/kg
108-86-1
Bromobenzene
ND
0.49
0.097
mg/kg
74-97-5
Bromochloromethane
ND
0.49
0.14
mg/kg
75-27-4
Bromodichloromethane
ND
0.49
0.097
mg/kg
75-25-2
Bromoform
ND
0.49
0.097
mg/kg
78-93-3
2-Butanone (MEK)
ND
2.4
0.71
mg/kg
104-51-8
n-Butylbenzene
ND
0.49
0.097
mg/kg
135-98-8
sec-Butylbenzene
ND
0.49
0.097
mg/kg
98-06-6
tert-Butylbenzene
ND
0.49
0.097
mg/kg
56-23-5
Carbon Tetrachloride °
ND
0.49
0.099
mg/kg
108-90-7
Chlorobenzene
ND
0.49
0.097
mg/kg
75-00-3
Chloroethanec
ND
0.49
0.19
mg/kg
67-66-3
Chloroform
ND
0.49
0.13
mg/kg
95-49-8
o-Chlorotoluene
ND
0.49
0.097
mg/kg
106-43-4
p-Chlorotoluene
ND
0.49
0.097
mg/kg
124-48-1
Dibromochloromethane
ND
0.49
0.097
mg/kg
106-93-4
1,2-Dibromoethane
ND
0.49
0.097
mg/kg
75-71-8
Dichlorodifluoromethane
ND
0.49
0.19
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.49
0.097
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.49
0.097
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.49
0.11
mg/kg
75-34-3
1, 1 -Dichloroethane
ND
0.49
0.17
mg/kg
107-06-2
1,2-Dichloroethane
ND
0.49
0.097
mg/kg
75-35-4
1, 1 -Dichloroethylene
ND
0.49
0.097
mg/kg
156-59-2
cis-1,2-Dichloroethylene
ND
0.49
0.13
mg/kg
156-60-5
trans-1,2-Dichloroethylene
ND
0.49
0.097
mg/kg
78-87-5
1,2-Dichloropropane
ND
0.49
0.097
mg/kg
142-28-9
1,3-Dichloropropane
ND
0.49
0.097
mg/kg
594-20-7
2,2-Dichloropropane
ND
0.49
0.097
mg/kg
563-58-6
1, 1 -Dichloropropene
ND
0.49
0.099
mg/kg
10061-01-5
cis- 1, 3-Dichloropropene
ND
0.49
0.097
mg/kg
"
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 20 of 69
FA56562

SGS North America Inc.
Report of Analysis
Page 2 of 3
Client Sample ID:
OE-3
Lab Sample ID:
FA56562-3 Date Sampled: 08/07/ 18
Matrix:
SO - Soil Date Received: 08/09/ 18
Method:
SW846 8260B Percent Solids: 80.6
Project:
Residential Property; Charlotte, NC
VOA List for NC, May 2012
CAS No.
Compound
Result
RL
MDL
Units Q
10061-02-6
trans- 1, 3-Dichloropropene
ND
0.49
0.097
mg/kg
108-20-3
Di -Isopropyl Ether
ND
0.49
0.23
mg/kg
64-17-5
Ethyl Alcohol
ND
39
7.3
mg/kg
100-41-4
Ethylbenzene
ND
0.49
0.097
mg/kg
591-78-6
2-Hexanone
ND
2.4
0.73
mg/kg
98-82-8
Isopropylbenzene
ND
0.49
0.097
mg/kg
99-87-6
p-Isopropyltoluene
ND
0.49
0.097
mg/kg
74-83-9
Methyl Bromide
ND
0.49
0.19
mg/kg
74-87-3
Methyl Chloride
ND
0.49
0.19
mg/kg
75-09-2
Methylene Chloride
ND
0.97
0.39
mg/kg
108-10-1
4-Methyl-2-pentanone (MIBK) ND
2.4
0.73
mg/kg
1634-04-4
Methyl Tert Butyl Ether
ND
0.49
0.097
mg/kg
91-20-3
Naphthalene
ND
0.49
0.19
mg/kg
103-65-1
n-Propylbenzene
ND
0.49
0.097
mg/kg
100-42-5
Styrene
ND
0.49
0.097
mg/kg
630-20-6
1, 1, 1,2-Tetrachloroethane
ND
0.49
0.10
mg/kg
79-34-5
1,1,2,2-Tetrachloroethane
ND
0.49
0.097
mg/kg
127-18-4
Tetrachloroethylene
ND
0.49
0.12
mg/kg
108-88-3
Toluene
ND
0.49
0.097
mg/kg
87-61-6
1,2,3-Trichlorobenzene
ND
0.49
0.14
mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
0.49
0.097
mg/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
0.49
0.097
mg/kg
79-00-5
1, 1, 2-Trichloroethane
ND
0.49
0.097
mg/kg
79-01-6
Trichloroethylene
ND
0.49
0.097
mg/kg
75-69-4
Trichlorofluoromethane
ND
0.49
0.19
mg/kg
96-18-4
1,2,3-Trichloropropane
ND
0.49
0.12
mg/kg
95-63-6
1,2,4-Trimethylbenzene
ND
0.49
0.097
mg/kg
108-67-8
1,3,5-Trimethylbenzene
ND
0.49
0.097
mg/kg
108-05-4
Vinyl Acetate
ND
2.4
1.6
mg/kg
75-01-4
Vinyl Chloride
ND
0.49
0.097
mg/kg
m,p-Xylene
ND
0.97
0.11
mg/kg
95-47-6
o-Xylene
ND
0.49
0.097
mg/kg
1330-20-7
Xylene (total)
ND
1.5
0.20
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
110%
75-124%
17060-07-0
1,2-Dichloroethane-D4
109%
72-135%
2037-26-5
Toluene-D8
106%
75-126%
460-00-4
4-Bromofluorobenzene
95%
71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
01
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FA56562

SGS North America Inc.
Report of Analysis
Page 3 of 3 w
Client Sample ID:
OE-3
Lab Sample ID:
FA56562-3 Date Sampled: 08/07/ 18
Matrix:
SO - Soil Date Received: 08/09/ 18
Method:
SW846 8260B Percent Solids: 80.6
Project:
Residential Property; Charlotte, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
(a) Dilution required due to matrix interference (sample foamed).
(b) Suspected laboratory contaminant.
(c) Associated CCV outside of control limits high, sample was ND.
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
6 22 of 69
FA56562

SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID: OE-3
Lab Sample ID: FA56562-3 Date Sampled: 08/07/ 18
Matrix: SO - Soil Date Received: 08/09/ 18
Method: SW846 8270D SW846 3550C Percent Solids: 80.6
Project: Residential Property; Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 91002131.D 1 08/16/18 23:03 MV 08/14/18 12:15 OP71335 S9173
Run #2
Initial Weight Final Volume
Run #1 30.3 g 1.0 ml
Run #2
ABN List for NC, May 2012
CAS No. Compound Result RL MDL Units
65-85-0
Benzoic Acid
ND
1.0
0.20
mg/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
0.20
0.023
mg/kg
95-57-8
2-Chlorophenol
ND
0.20
0.025
mg/kg
120-83-2
2,4-Dichlorophenol
ND
0.20
0.024
mg/kg
105-67-9
2,4-Dimethylphenol
ND
0.20
0.054
mg/kg
51-28-5
2,4-Dinitrophenol
ND
1.0
0.20
mg/kg
534-52-1
4,6-Dinitro-o-cresol
ND
0.41
0.082
mg/kg
95-48-7
2-Methylphenol
ND
0.20
0.025
mg/kg
3&4-Methylphenol
ND
0.20
0.034
mg/kg
88-75-5
2-Nitrophenol
ND
0.20
0.022
mg/kg
100-02-7
4-Nitrophenol
ND
1.0
0.20
mg/kg
87-86-5
Pentachlorophenol
ND
1.0
0.20
mg/kg
108-95-2
Phenol
ND
0.20
0.020
mg/kg
88-06-2
2,4,6-Trichlorophenol
ND
0.20
0.024
mg/kg
83-32-9
Acenaphthene
ND
0.20
0.022
mg/kg
208-96-8
Acenaphthylene
ND
0.20
0.020
mg/kg
120-12-7
Anthracene
ND
0.20
0.023
mg/kg
56-55-3
Benzo(a)anthracene
ND
0.20
0.020
mg/kg
50-32-8
Benzo(a)pyrene
ND
0.20
0.024
mg/kg
205-99-2
Benzo(b)fluoranthene
ND
0.20
0.022
mg/kg
191-24-2
Benzo(g,h,i)perylene
ND
0.20
0.021
mg/kg
207-08-9
Benzo(k)fluoranthene
ND
0.20
0.027
mg/kg
100-51-6
Benzyl Alcohol
ND
0.20
0.020
mg/kg
101-55-3
4-Bromophenyl phenyl ether
ND
0.20
0.021
mg/kg
85-68-7
Butyl benzyl phthalate
ND
0.20
0.041
mg/kg
106-47-8
4-Chloroaniline
ND
0.20
0.052
mg/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
0.20
0.020
mg/kg
111-44-4
bis(2-Chloroethyl)ether
ND
0.20
0.024
mg/kg
108-60-1
2,2'-Oxybis(1-chloropropane)
ND
0.20
0.026
mg/kg
91-58-7
2-Chloronaphthalene
ND
0.20
0.020
mg/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.20
0.020
mg/kg
218-01-9
Chrysene
ND
0.20
0.021
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
01
23 of 69
FA56562

SGS North America Inc.
Report of Analysis
Client Sample ID: OE-3
Lab Sample ID: FA56562-3 Date Sampled: 08/07/ 18
Matrix: SO - Soil Date Received: 08/09/ 18
Method: SW846 8270D SW846 3550C Percent Solids: 80.6
Project: Residential Property; Charlotte, NC
ABN List for NC, May 2012
CAS No.
Compound
Result
RL
MDL
Units Q
53-70-3
Dibenzo(a,h)anthracene
ND
0.20
0.026
mg/kg
132-64-9
Dibenzofaran
ND
0.20
0.020
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.20
0.020
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.20
0.022
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.20
0.027
mg/kg
91-94-1
3,3'-Dichlorobenzidine
ND
0.20
0.049
mg/kg
84-66-2
Diethyl Phthalate
ND
0.41
0.041
mg/kg
131-11-3
Dimethyl Phthalate
ND
0.20
0.041
mg/kg
117-84-0
Di-n-octyl Phthalate
ND
0.20
0.041
mg/kg
84-74-2
Di-n-butyl Phthalate
ND
0.41
0.082
mg/kg
122-66-7
1,2-Diphenylhydrazine
ND
0.20
0.020
mg/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
0.41
0.041
mg/kg
206-44-0
Fluoranthene
ND
0.20
0.020
mg/kg
86-73-7
Fluorene
ND
0.20
0.022
mg/kg
118-74-1
Hexachlorobenzene
ND
0.20
0.021
mg/kg
87-68-3
Hexachlorobutadiene
ND
0.20
0.021
mg/kg
77-47-4
Hexachlorocyclopentadiene
ND
0.20
0.041
mg/kg
67-72-1
Hexachloroethane
ND
0.20
0.024
mg/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.20
0.025
mg/kg
78-59-1
Isophorone
ND
0.20
0.020
mg/kg
90-12-0
1-Methylnaphthalene
ND
0.20
0.020
mg/kg
91-57-6
2-Methylnaphthalene
ND
0.20
0.020
mg/kg
91-20-3
Naphthalene
ND
0.20
0.020
mg/kg
98-95-3
Nitrobenzene
ND
0.20
0.020
mg/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
0.20
0.020
mg/kg
86-30-6
N-Nitrosodiphenylamine
ND
0.20
0.022
mg/kg
85-01-8
Phenanthrene
ND
0.20
0.020
mg/kg
129-00-0
Pyrene
ND
0.20
0.024
mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
0.20
0.024
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
66%
40-102%
4165-62-2
Phenol-d5
70%
41-100%
118-79-6
2,4,6-Tribromophenol
71%
42-108%
4165-60-0
Nitrobenzene-d5
57%
40-105%
321-60-8
2-Fluorobiphenyl
75%
43-107%
1718-51-0
Terphenyl-dl4
89%
45-119%
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
01
24 of 69
FA56562

SGS North America Inc.
Report of Analysis Page 1 of 1 w
Client Sample ID: OE-3
Lab Sample ID: FA56562-3 Date Sampled: 08/07/ 18
Matrix: SO - Soil Date Received: 08/09/ 18
Method: MADEP VPH REV 1.1 Percent Solids: 80.6
Project: Residential Property; Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 UU025485.D 1 08/15/18 23:04 NM n/a n/a GUU1319
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 4.37 g 5.1 ml 100 ul
Run #2
MADEP VPH List
CAS No. Compound
Result
RL
MDL Units Q
C5- C8 Aliphatics (Unadj.)
ND
8.4
3.0 mg/kg
C9- C12 Aliphatics (Unadj.)
ND
8.4
3.0 mg/kg
C9- C10 Aromatics (Unadj.)
ND
8.4
3.0 mg/kg
CAS No. Surrogate Recoveries
Run# 1
Run# 2
Limits
460-00-4 BFB
134% a
70-130%
460-00-4 BFB
129%
70-130%
(a) Outside control limits; however, sample
is ND.
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
�1%6 25 of 69
FA56562

SGS North America Inc.
Report of Analysis
Client Sample ID: OE-3
Lab Sample ID: FA56562-3 Date Sampled: 08/07/ 18
Matrix: SO - Soil Date Received: 08/09/ 18
Method: MADEP EPH REV 1.1 SW846 3546 Percent Solids: 80.6
Project: Residential Property; Charlotte, NC
Page 1 of 1 w
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN023229.13 1 08/15/18 20:08 NJ 08/13/18 09:30 OP71311 GNN1137
Run #2
Initial Weight Final Volume
Run # 1 20.5 g 2.0 ml
Run #2
MAEPH List
CAS No.
Compound
Result
RL
MDL Units Q
C11-C22 Aromatics (Unadj.)
8.11
12
4.8 mg/kg J
C9-C18 Aliphatics
ND
12
3.0 mg/kg
C19-C36 Aliphatics
3.55
12
3.0 mg/kg J
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
3386-33-2
1-Chlorooctadecane
74%
40-140%
580-13-2
2-Bromonaphthalene
71%
40-140%
84-15-1
o-Terphenyl
73%
40-140%
321-60-8
2-Fluorobiphenyl
60%
40-140%
ND = Not detected MDL = Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
6 26 of 69
FA56562

SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:
OE-4
Lab Sample ID:
FA56562-4 Date Sampled: 08/07/ 18
Matrix:
SO - Soil Date Received: 08/09/ 18
Method:
SW846 8260B Percent Solids: 75.8
Project:
Residential Property; Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 3C1456.D 1 08/14/18 18:58 SP n/a n/a V3C61
Run #2
Initial Weight Final Volume Methanol Aliquot
Run # 1 4.94 g 5.0 ml 100 ul
Run #2
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units
67-64-1
Acetone b
2.68
4.1
0.83
mg/kg
71-43-2
Benzene
ND
0.41
0.10
mg/kg
108-86-1
Bromobenzene
ND
0.41
0.083
mg/kg
74-97-5
Bromochloromethane
ND
0.41
0.12
mg/kg
75-27-4
Bromodichloromethane
ND
0.41
0.083
mg/kg
75-25-2
Bromoform
ND
0.41
0.083
mg/kg
78-93-3
2-Butanone (MEK)
ND
2.1
0.60
mg/kg
104-51-8
n-Butylbenzene
ND
0.41
0.083
mg/kg
135-98-8
sec-Butylbenzene
ND
0.41
0.083
mg/kg
98-06-6
tert-Butylbenzene
ND
0.41
0.083
mg/kg
56-23-5
Carbon Tetrachloride °
ND
0.41
0.084
mg/kg
108-90-7
Chlorobenzene
ND
0.41
0.083
mg/kg
75-00-3
Chloroethanec
ND
0.41
0.17
mg/kg
67-66-3
Chloroform
ND
0.41
0.11
mg/kg
95-49-8
o-Chlorotoluene
ND
0.41
0.083
mg/kg
106-43-4
p-Chlorotoluene
ND
0.41
0.083
mg/kg
124-48-1
Dibromochloromethane
ND
0.41
0.083
mg/kg
106-93-4
1,2-Dibromoethane
ND
0.41
0.083
mg/kg
75-71-8
Dichlorodifluoromethane
ND
0.41
0.17
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.41
0.083
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.41
0.083
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.41
0.095
mg/kg
75-34-3
1, 1 -Dichloroethane
ND
0.41
0.15
mg/kg
107-06-2
1,2-Dichloroethane
ND
0.41
0.083
mg/kg
75-35-4
1, 1 -Dichloroethylene
ND
0.41
0.083
mg/kg
156-59-2
cis-1,2-Dichloroethylene
ND
0.41
0.11
mg/kg
156-60-5
trans-1,2-Dichloroethylene
ND
0.41
0.083
mg/kg
78-87-5
1,2-Dichloropropane
ND
0.41
0.083
mg/kg
142-28-9
1,3-Dichloropropane
ND
0.41
0.083
mg/kg
594-20-7
2,2-Dichloropropane
ND
0.41
0.083
mg/kg
563-58-6
1, 1 -Dichloropropene
ND
0.41
0.084
mg/kg
10061-01-5
cis- 1, 3-Dichloropropene
ND
0.41
0.083
mg/kg
"
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 27 of 69
FA56562

SGS North America Inc.
Report of Analysis
Page 2 of 3
Client Sample ID:
OE-4
Lab Sample ID:
FA56562-4 Date Sampled: 08/07/ 18
Matrix:
SO - Soil Date Received: 08/09/ 18
Method:
SW846 8260B Percent Solids: 75.8
Project:
Residential Property; Charlotte, NC
VOA List for NC, May 2012
CAS No.
Compound
Result
RL
MDL
Units Q
10061-02-6
trans- 1, 3-Dichloropropene
ND
0.41
0.083
mg/kg
108-20-3
Di -Isopropyl Ether
ND
0.41
0.19
mg/kg
64-17-5
Ethyl Alcohol
ND
33
6.2
mg/kg
100-41-4
Ethylbenzene
ND
0.41
0.083
mg/kg
591-78-6
2-Hexanone
ND
2.1
0.62
mg/kg
98-82-8
Isopropylbenzene
ND
0.41
0.083
mg/kg
99-87-6
p-Isopropyltoluene
ND
0.41
0.083
mg/kg
74-83-9
Methyl Bromide
ND
0.41
0.17
mg/kg
74-87-3
Methyl Chloride
ND
0.41
0.17
mg/kg
75-09-2
Methylene Chloride
ND
0.83
0.33
mg/kg
108-10-1
4-Methyl-2-pentanone (MIBK) ND
2.1
0.62
mg/kg
1634-04-4
Methyl Tert Butyl Ether
ND
0.41
0.083
mg/kg
91-20-3
Naphthalene
ND
0.41
0.17
mg/kg
103-65-1
n-Propylbenzene
ND
0.41
0.083
mg/kg
100-42-5
Styrene
ND
0.41
0.083
mg/kg
630-20-6
1, 1, 1,2-Tetrachloroethane
ND
0.41
0.085
mg/kg
79-34-5
1,1,2,2-Tetrachloroethane
ND
0.41
0.083
mg/kg
127-18-4
Tetrachloroethylene
ND
0.41
0.11
mg/kg
108-88-3
Toluene b
0.236
0.41
0.083
mg/kg J
87-61-6
1,2,3-Trichlorobenzene
ND
0.41
0.12
mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
0.41
0.083
mg/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
0.41
0.083
mg/kg
79-00-5
1, 1, 2-Trichloroethane
ND
0.41
0.083
mg/kg
79-01-6
Trichloroethylene
ND
0.41
0.083
mg/kg
75-69-4
Trichlorofluoromethane
ND
0.41
0.17
mg/kg
96-18-4
1,2,3-Trichloropropane
ND
0.41
0.10
mg/kg
95-63-6
1,2,4-Trimethylbenzene
ND
0.41
0.083
mg/kg
108-67-8
1,3,5-Trimethylbenzene
ND
0.41
0.083
mg/kg
108-05-4
Vinyl Acetate
ND
2.1
1.4
mg/kg
75-01-4
Vinyl Chloride
ND
0.41
0.083
mg/kg
m,p-Xylene
ND
0.83
0.091
mg/kg
95-47-6
o-Xylene
ND
0.41
0.083
mg/kg
1330-20-7
Xylene (total)
ND
1.2
0.17
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
103%
75-124%
17060-07-0
1,2-Dichloroethane-D4
108%
72-135%
2037-26-5
Toluene-D8
108%
75-126%
460-00-4
4-Bromofluorobenzene
98%
71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
01
28 of 69
FA56562

SGS North America Inc.
Report of Analysis
Page 3 of 3
Client Sample ID:
OE-4
Lab Sample ID:
FA56562-4 Date Sampled: 08/07/ 18
Matrix:
SO - Soil Date Received: 08/09/ 18
Method:
SW846 8260B Percent Solids: 75.8
Project:
Residential Property; Charlotte, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
(a) Dilution required due to matrix interference (sample foamed).
(b) Suspected laboratory contaminant.
(c) Associated CCV outside of control limits high, sample was ND.
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
6 29 of 69
FA56562

SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID: OE-4
Lab Sample ID: FA56562-4 Date Sampled: 08/07/ 18
Matrix: SO - Soil Date Received: 08/09/ 18
Method: SW846 8270D SW846 3550C Percent Solids: 75.8
Project: Residential Property; Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 91002149.D 1 08/17/18 16:28 MV 08/14/18 12:15 OP71335 S9174
Run #2
Initial Weight Final Volume
Run#1 30.2g 1.0ml
Run #2
ABN List for NC, May 2012
CAS No. Compound Result RL MDL Units
65-85-0
Benzoic Acid
ND
1.1
0.22
mg/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
0.22
0.025
mg/kg
95-57-8
2-Chlorophenol
ND
0.22
0.027
mg/kg
120-83-2
2,4-Dichlorophenol
ND
0.22
0.025
mg/kg
105-67-9
2,4-Dimethylphenol
ND
0.22
0.058
mg/kg
51-28-5
2,4-Dinitrophenol
ND
1.1
0.22
mg/kg
534-52-1
4,6-Dinitro-o-cresol
ND
0.44
0.087
mg/kg
95-48-7
2-Methylphenol
ND
0.22
0.026
mg/kg
3&4-Methylphenol
ND
0.22
0.036
mg/kg
88-75-5
2-Nitrophenol
ND
0.22
0.024
mg/kg
100-02-7
4-Nitrophenol
ND
1.1
0.22
mg/kg
87-86-5
Pentachlorophenol
ND
1.1
0.22
mg/kg
108-95-2
Phenol
ND
0.22
0.022
mg/kg
88-06-2
2,4,6-Trichlorophenol
ND
0.22
0.025
mg/kg
83-32-9
Acenaphthene
ND
0.22
0.023
mg/kg
208-96-8
Acenaphthylene
ND
0.22
0.022
mg/kg
120-12-7
Anthracene
ND
0.22
0.024
mg/kg
56-55-3
Benzo(a)anthracene
ND
0.22
0.022
mg/kg
50-32-8
Benzo(a)pyrene
ND
0.22
0.026
mg/kg
205-99-2
Benzo(b)fluoranthene
ND
0.22
0.024
mg/kg
191-24-2
Benzo(g,h,i)perylene
ND
0.22
0.023
mg/kg
207-08-9
Benzo(k)fluoranthene
ND
0.22
0.029
mg/kg
100-51-6
Benzyl Alcohol
ND
0.22
0.022
mg/kg
101-55-3
4-Bromophenyl phenyl ether
ND
0.22
0.023
mg/kg
85-68-7
Butyl benzyl phthalate
ND
0.22
0.044
mg/kg
106-47-8
4-Chloroaniline
ND
0.22
0.055
mg/kg
111-91-1
bis(2-Chloroethoxy)methane a
ND
0.22
0.022
mg/kg
111-44-4
bis(2-Chloroethyl)ether
ND
0.22
0.025
mg/kg
108-60-1
2,2'-Oxybis(1-chloropropane)
ND
0.22
0.027
mg/kg
91-58-7
2-Chloronaphthalene
ND
0.22
0.022
mg/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.22
0.022
mg/kg
218-01-9
Chrysene
ND
0.22
0.022
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
01
30 of 69
FA56562

SGS North America Inc.
Report of Analysis
Client Sample ID: OE-4
Lab Sample ID: FA56562-4 Date Sampled: 08/07/ 18
Matrix: SO - Soil Date Received: 08/09/ 18
Method: SW846 8270D SW846 3550C Percent Solids: 75.8
Project: Residential Property; Charlotte, NC
ABN List for NC, May 2012
CAS No.
Compound
Result
RL
MDL
Units Q
53-70-3
Dibenzo(a,h)anthracene
ND
0.22
0.027
mg/kg
132-64-9
Dibenzofaran
ND
0.22
0.022
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.22
0.022
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.22
0.024
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.22
0.029
mg/kg
91-94-1
3,3'-Dichlorobenzidine
ND
0.22
0.052
mg/kg
84-66-2
Diethyl Phthalate
ND
0.44
0.044
mg/kg
131-11-3
Dimethyl Phthalate
ND
0.22
0.044
mg/kg
117-84-0
Di-n-octyl Phthalate
ND
0.22
0.044
mg/kg
84-74-2
Di-n-butyl Phthalate
ND
0.44
0.087
mg/kg
122-66-7
1,2-Diphenylhydrazine
ND
0.22
0.022
mg/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
0.44
0.044
mg/kg
206-44-0
Fluoranthene
ND
0.22
0.022
mg/kg
86-73-7
Fluorene
ND
0.22
0.023
mg/kg
118-74-1
Hexachlorobenzene
ND
0.22
0.022
mg/kg
87-68-3
Hexachlorobutadiene
ND
0.22
0.022
mg/kg
77-47-4
Hexachlorocyclopentadiene
ND
0.22
0.044
mg/kg
67-72-1
Hexachloroethane
ND
0.22
0.026
mg/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.22
0.027
mg/kg
78-59-1
Isophorone
ND
0.22
0.022
mg/kg
90-12-0
1-Methylnaphthalene
ND
0.22
0.022
mg/kg
91-57-6
2-Methylnaphthalene
ND
0.22
0.022
mg/kg
91-20-3
Naphthalene
ND
0.22
0.022
mg/kg
98-95-3
Nitrobenzene
ND
0.22
0.022
mg/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
0.22
0.022
mg/kg
86-30-6
N-Nitrosodiphenylamine
ND
0.22
0.024
mg/kg
85-01-8
Phenanthrene
ND
0.22
0.022
mg/kg
129-00-0
Pyrene
ND
0.22
0.025
mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
0.22
0.026
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
69%
40-102%
4165-62-2
Phenol-d5
74%
41-100%
118-79-6
2,4,6-Tribromophenol
80%
42-108%
4165-60-0
Nitrobenzene-d5
68%
40-105%
321-60-8
2-Fluorobiphenyl
68%
43-107%
1718-51-0
Terphenyl-dl4
81%
45-119%
(a) Associated CCV outside control limits high. Sample was ND.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
01
31 of 69
FA56562

SGS North America Inc.
Report of Analysis Page 1 of 1 P
Client Sample ID: OE-4
Lab Sample ID: FA56562-4 Date Sampled: 08/07/ 18
Matrix: SO - Soil Date Received: 08/09/ 18
Method: MADEP VPH REV 1.1 Percent Solids: 75.8
Project: Residential Property; Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 UU025486.D 1 08/15/18 23:34 NM n/a n/a GUU1319
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 4.52 g 5.1 ml 100 ul
Run #2
MADEP VPH List
CAS No.
Compound
Result
RL
MDL Units Q
C5- C8 Aliphatics (Unadj.)
ND
9.0
3.2 mg/kg
C9- C12 Aliphatics (Unadj.)
ND
9.0
3.2 mg/kg
C9- C10 Aromatics (Unadj.)
ND
9.0
3.2 mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
460-00-4
BFB
127%
70-130%
460-00-4
BFB
122%
70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
� 32 of 69
FA56562

SGS North America Inc.
Report of Analysis
Client Sample ID: OE-4
Lab Sample ID: FA56562-4 Date Sampled: 08/07/ 18
Matrix: SO - Soil Date Received: 08/09/ 18
Method: MADEP EPH REV 1.1 SW846 3546 Percent Solids: 75.8
Project: Residential Property; Charlotte, NC
Page 1 of 1 P
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN023230.13 1 08/15/18 20:40 NJ 08/13/18 09:30 OP71311 GNN1137
Run #2
Initial Weight Final Volume
Run # 1 20.3 g 2.0 ml
Run #2
MAEPH List
CAS No.
Compound
Result
RL
MDL Units Q
C11-C22 Aromatics (Unadj.)
8.50
13
5.2 mg/kg J
C9-C18 Aliphatics
ND
13
3.2 mg/kg
C19-C36 Aliphatics
5.24
13
3.2 mg/kg J
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
3386-33-2
1-Chlorooctadecane
61%
40-140%
580-13-2
2-Bromonaphthalene
76%
40-140%
84-15-1
o-Terphenyl
73%
40-140%
321-60-8
2-Fluorobiphenyl
64%
40-140%
ND = Not detected MDL = Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
�I 33 of 69
FA56562

SGS North America Inc.
Report of Analysis Page 1 of 3
Client Sample ID:
OE-5
Lab Sample ID:
FA56562-5 Date Sampled: 08/07/ 18
Matrix:
SO - Soil Date Received: 08/09/ 18
Method:
SW846 8260B Percent Solids: 73.2
Project:
Residential Property; Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 a 3C1457.D 1 08/14/18 19:21 SP n/a n/a V3C61
Run #2
Initial Weight Final Volume Methanol Aliquot
Run #1 3.52 g 5.0 ml 100 ul
Run #2
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units
67-64-1
Acetone b
4.35
5.8
1.2
mg/kg
71-43-2
Benzene
ND
0.58
0.14
mg/kg
108-86-1
Bromobenzene
ND
0.58
0.12
mg/kg
74-97-5
Bromochloromethane
ND
0.58
0.17
mg/kg
75-27-4
Bromodichloromethane
ND
0.58
0.12
mg/kg
75-25-2
Bromoform
ND
0.58
0.12
mg/kg
78-93-3
2-Butanone (MEK)
ND
2.9
0.84
mg/kg
104-51-8
n-Butylbenzene
ND
0.58
0.12
mg/kg
135-98-8
sec-Butylbenzene
ND
0.58
0.12
mg/kg
98-06-6
tert-Butylbenzene
ND
0.58
0.12
mg/kg
56-23-5
Carbon Tetrachloride °
ND
0.58
0.12
mg/kg
108-90-7
Chlorobenzene
ND
0.58
0.12
mg/kg
75-00-3
Chloroethane c
ND
0.58
0.23
mg/kg
67-66-3
Chloroform
ND
0.58
0.15
mg/kg
95-49-8
o-Chlorotoluene
ND
0.58
0.12
mg/kg
106-43-4
p-Chlorotoluene
ND
0.58
0.12
mg/kg
124-48-1
Dibromochloromethane
ND
0.58
0.12
mg/kg
106-93-4
1,2-Dibromoethane
ND
0.58
0.12
mg/kg
75-71-8
Dichlorodifluoromethane
ND
0.58
0.23
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.58
0.12
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.58
0.12
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.58
0.13
mg/kg
75-34-3
1, 1 -Dichloroethane
ND
0.58
0.20
mg/kg
107-06-2
1,2-Dichloroethane
ND
0.58
0.12
mg/kg
75-35-4
1, 1 -Dichloroethylene
ND
0.58
0.12
mg/kg
156-59-2
cis-1,2-Dichloroethylene
ND
0.58
0.16
mg/kg
156-60-5
trans-1,2-Dichloroethylene
ND
0.58
0.12
mg/kg
78-87-5
1,2-Dichloropropane
ND
0.58
0.12
mg/kg
142-28-9
1,3-Dichloropropane
ND
0.58
0.12
mg/kg
594-20-7
2,2-Dichloropropane
ND
0.58
0.12
mg/kg
563-58-6
1, 1 -Dichloropropene
ND
0.58
0.12
mg/kg
10061-01-5
cis- 1, 3-Dichloropropene
ND
0.58
0.12
mg/kg
"
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 34 of 69
FA56562

SGS North America Inc.
Report of Analysis
Page 2 of 3
Client Sample ID:
OE-5
Lab Sample ID:
FA56562-5 Date Sampled: 08/07/ 18
Matrix:
SO - Soil Date Received: 08/09/ 18
Method:
SW846 8260B Percent Solids: 73.2
Project:
Residential Property; Charlotte, NC
VOA List for NC, May 2012
CAS No.
Compound
Result
RL
MDL
Units Q
10061-02-6
trans- 1, 3-Dichloropropene
ND
0.58
0.12
mg/kg
108-20-3
Di -Isopropyl Ether
ND
0.58
0.27
mg/kg
64-17-5
Ethyl Alcohol
ND
46
8.6
mg/kg
100-41-4
Ethylbenzene
ND
0.58
0.12
mg/kg
591-78-6
2-Hexanone
ND
2.9
0.86
mg/kg
98-82-8
Isopropylbenzene
ND
0.58
0.12
mg/kg
99-87-6
p-Isopropyltoluene
ND
0.58
0.12
mg/kg
74-83-9
Methyl Bromide
ND
0.58
0.23
mg/kg
74-87-3
Methyl Chloride
ND
0.58
0.23
mg/kg
75-09-2
Methylene Chloride
ND
1.2
0.46
mg/kg
108-10-1
4-Methyl-2-pentanone (MIBK) ND
2.9
0.86
mg/kg
1634-04-4
Methyl Tert Butyl Ether
ND
0.58
0.12
mg/kg
91-20-3
Naphthalene
ND
0.58
0.23
mg/kg
103-65-1
n-Propylbenzene
ND
0.58
0.12
mg/kg
100-42-5
Styrene
ND
0.58
0.12
mg/kg
630-20-6
1, 1, 1,2-Tetrachloroethane
ND
0.58
0.12
mg/kg
79-34-5
1,1,2,2-Tetrachloroethane
ND
0.58
0.12
mg/kg
127-18-4
Tetrachloroethylene
ND
0.58
0.15
mg/kg
108-88-3
Toluene b
0.433
0.58
0.12
mg/kg J
87-61-6
1,2,3-Trichlorobenzene
ND
0.58
0.16
mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
0.58
0.12
mg/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
0.58
0.12
mg/kg
79-00-5
1, 1, 2-Trichloroethane
ND
0.58
0.12
mg/kg
79-01-6
Trichloroethylene
ND
0.58
0.12
mg/kg
75-69-4
Trichlorofluoromethane
ND
0.58
0.23
mg/kg
96-18-4
1,2,3-Trichloropropane
ND
0.58
0.14
mg/kg
95-63-6
1,2,4-Trimethylbenzene
ND
0.58
0.12
mg/kg
108-67-8
1,3,5-Trimethylbenzene
ND
0.58
0.12
mg/kg
108-05-4
Vinyl Acetate
ND
2.9
1.9
mg/kg
75-01-4
Vinyl Chloride
ND
0.58
0.12
mg/kg
m,p-Xylene
ND
1.2
0.13
mg/kg
95-47-6
o-Xylene
ND
0.58
0.12
mg/kg
1330-20-7
Xylene (total)
ND
1.7
0.24
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
1868-53-7
Dibromofluoromethane
110%
75-124%
17060-07-0
1,2-Dichloroethane-D4
112%
72-135%
2037-26-5
Toluene-D8
104%
75-126%
460-00-4
4-Bromofluorobenzene
99%
71-133%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
01
35 of 69
FA56562

SGS North America Inc.
Report of Analysis
Page 3 of 3 P
Client Sample ID:
OE-5
Lab Sample ID:
FA56562-5 Date Sampled: 08/07/ 18
Matrix:
SO - Soil Date Received: 08/09/ 18
Method:
SW846 8260B Percent Solids: 73.2
Project:
Residential Property; Charlotte, NC
VOA List for NC, May 2012
CAS No. Compound Result RL MDL Units Q
(a) Dilution required due to matrix interference (sample foamed).
(b) Suspected laboratory contaminant.
(c) Associated CCV outside of control limits high, sample was ND.
ND
= Not detected MDL = Method Detection Limit
J =
Indicates an estimated value
RL
= Reporting Limit
B =
Indicates analyte found in associated method blank
E =
Indicates value exceeds calibration range
N
= Indicates presumptive evidence of a compound
6 36 of 69
FA56562

SGS North America Inc.
Report of Analysis Page 1 of 2
Client Sample ID: OE-5
Lab Sample ID: FA56562-5 Date Sampled: 08/07/ 18
Matrix: SO - Soil Date Received: 08/09/ 18
Method: SW846 8270D SW846 3550C Percent Solids: 73.2
Project: Residential Property; Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 9I002150.1) 1 08/17/18 16:57 MV 08/14/18 12:15 OP71335 S9174
Run #2
Initial Weight Final Volume
Run#1 30.2g 1.0ml
Run #2
ABN List for NC, May 2012
CAS No. Compound Result RL MDL Units
65-85-0
Benzoic Acid
ND
1.1
0.23
mg/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
0.23
0.026
mg/kg
95-57-8
2-Chlorophenol
ND
0.23
0.028
mg/kg
120-83-2
2,4-Dichlorophenol
ND
0.23
0.026
mg/kg
105-67-9
2,4-Dimethylphenol
ND
0.23
0.060
mg/kg
51-28-5
2,4-Dinitrophenol
ND
1.1
0.23
mg/kg
534-52-1
4,6-Dinitro-o-cresol
ND
0.45
0.090
mg/kg
95-48-7
2-Methylphenol
ND
0.23
0.027
mg/kg
3&4-Methylphenol
ND
0.23
0.037
mg/kg
88-75-5
2-Nitrophenol
ND
0.23
0.025
mg/kg
100-02-7
4-Nitrophenol
ND
1.1
0.23
mg/kg
87-86-5
Pentachlorophenol
ND
1.1
0.23
mg/kg
108-95-2
Phenol
ND
0.23
0.023
mg/kg
88-06-2
2,4,6-Trichlorophenol
ND
0.23
0.026
mg/kg
83-32-9
Acenaphthene
ND
0.23
0.024
mg/kg
208-96-8
Acenaphthylene
ND
0.23
0.023
mg/kg
120-12-7
Anthracene
ND
0.23
0.025
mg/kg
56-55-3
Benzo(a)anthracene
ND
0.23
0.023
mg/kg
50-32-8
Benzo(a)pyrene
ND
0.23
0.027
mg/kg
205-99-2
Benzo(b)fluoranthene
ND
0.23
0.025
mg/kg
191-24-2
Benzo(g,h,i)perylene
ND
0.23
0.023
mg/kg
207-08-9
Benzo(k)fluoranthene
ND
0.23
0.030
mg/kg
100-51-6
Benzyl Alcohol
ND
0.23
0.023
mg/kg
101-55-3
4-Bromophenyl phenyl ether
ND
0.23
0.023
mg/kg
85-68-7
Butyl benzyl phthalate
ND
0.23
0.045
mg/kg
106-47-8
4-Chloroaniline
ND
0.23
0.057
mg/kg
111-91-1
bis(2-Chloroethoxy)methane a
ND
0.23
0.023
mg/kg
111-44-4
bis(2-Chloroethyl)ether
ND
0.23
0.026
mg/kg
108-60-1
2,2'-Oxybis(1-chloropropane)
ND
0.23
0.028
mg/kg
91-58-7
2-Chloronaphthalene
ND
0.23
0.023
mg/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
0.23
0.023
mg/kg
218-01-9
Chrysene
ND
0.23
0.023
mg/kg
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
01
37 of 69
FA56562

SGS North America Inc.
Report of Analysis
Client Sample ID: OE-5
Lab Sample ID: FA56562-5 Date Sampled: 08/07/ 18
Matrix: SO - Soil Date Received: 08/09/ 18
Method: SW846 8270D SW846 3550C Percent Solids: 73.2
Project: Residential Property; Charlotte, NC
ABN List for NC, May 2012
CAS No.
Compound
Result
RL
MDL
Units Q
53-70-3
Dibenzo(a,h)anthracene
ND
0.23
0.028
mg/kg
132-64-9
Dibenzofaran
ND
0.23
0.023
mg/kg
95-50-1
1,2-Dichlorobenzene
ND
0.23
0.023
mg/kg
541-73-1
1,3-Dichlorobenzene
ND
0.23
0.024
mg/kg
106-46-7
1,4-Dichlorobenzene
ND
0.23
0.030
mg/kg
91-94-1
3,3'-Dichlorobenzidine
ND
0.23
0.054
mg/kg
84-66-2
Diethyl Phthalate
ND
0.45
0.045
mg/kg
131-11-3
Dimethyl Phthalate
ND
0.23
0.045
mg/kg
117-84-0
Di-n-octyl Phthalate
ND
0.23
0.045
mg/kg
84-74-2
Di-n-butyl Phthalate
ND
0.45
0.090
mg/kg
122-66-7
1,2-Diphenylhydrazine
ND
0.23
0.023
mg/kg
117-81-7
bis(2-Ethylhexyl)phthalate
ND
0.45
0.045
mg/kg
206-44-0
Fluoranthene
ND
0.23
0.023
mg/kg
86-73-7
Fluorene
ND
0.23
0.024
mg/kg
118-74-1
Hexachlorobenzene
ND
0.23
0.023
mg/kg
87-68-3
Hexachlorobutadiene
ND
0.23
0.023
mg/kg
77-47-4
Hexachlorocyclopentadiene
ND
0.23
0.045
mg/kg
67-72-1
Hexachloroethane
ND
0.23
0.027
mg/kg
193-39-5
Indeno(1,2,3-cd)pyrene
ND
0.23
0.028
mg/kg
78-59-1
Isophorone
ND
0.23
0.023
mg/kg
90-12-0
1-Methylnaphthalene
ND
0.23
0.023
mg/kg
91-57-6
2-Methylnaphthalene
ND
0.23
0.023
mg/kg
91-20-3
Naphthalene
ND
0.23
0.023
mg/kg
98-95-3
Nitrobenzene
ND
0.23
0.023
mg/kg
621-64-7
N-Nitrosodi-n-propylamine
ND
0.23
0.023
mg/kg
86-30-6
N-Nitrosodiphenylamine
ND
0.23
0.024
mg/kg
85-01-8
Phenanthrene
ND
0.23
0.023
mg/kg
129-00-0
Pyrene
ND
0.23
0.026
mg/kg
120-82-1
1,2,4-Trichlorobenzene
ND
0.23
0.027
mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
367-12-4
2-Fluorophenol
62%
40-102%
4165-62-2
Phenol-d5
65%
41-100%
118-79-6
2,4,6-Tribromophenol
69%
42-108%
4165-60-0
Nitrobenzene-d5
63%
40-105%
321-60-8
2-Fluorobiphenyl
64%
43-107%
1718-51-0
Terphenyl-dl4
70%
45-119%
(a) Associated CCV outside control limits high. Sample was ND.
Page 2 of 2
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
01
38 of 69
FA56562

SGS North America Inc.
Report of Analysis Page 1 of 1 P
Client Sample ID: OE-5
Lab Sample ID: FA56562-5 Date Sampled: 08/07/ 18
Matrix: SO - Soil Date Received: 08/09/ 18
Method: MADEP VPH REV 1.1 Percent Solids: 73.2
Project: Residential Property; Charlotte, NC
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 UU025487.D 1 08/16/18 00:05 NM n/a n/a GUU1319
Run #2
Initial Weight Final Volume Methanol Aliquot
Run # 1 4.03 g 5.1 ml 100 ul
Run #2
MADEP VPH List
CAS No.
Compound
Result
RL
MDL Units Q
C5- C8 Aliphatics (Unadj.)
ND
10
3.7 mg/kg
C9- C12 Aliphatics (Unadj.)
ND
10
3.7 mg/kg
C9- C10 Aromatics (Unadj.)
ND
10
3.7 mg/kg
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
460-00-4
BFB
125%
70-130%
460-00-4
BFB
120%
70-130%
ND = Not detected MDL = Method Detection Limit J = Indicates an estimated value
RL = Reporting Limit B = Indicates analyte found in associated method blank
E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound
6 39 of 69
FA56562

SGS North America Inc.
Report of Analysis
Client Sample ID: OE-5
Lab Sample ID: FA56562-5 Date Sampled: 08/07/ 18
Matrix: SO - Soil Date Received: 08/09/ 18
Method: MADEP EPH REV 1.1 SW846 3546 Percent Solids: 73.2
Project: Residential Property; Charlotte, NC
Page 1 of 1 P
File ID DF Analyzed By Prep Date Prep Batch Analytical Batch
Run #1 NN023231.13 1 08/15/18 21:11 NJ 08/13/18 09:30 OP71311 GNN1137
Run #2
Initial Weight Final Volume
Run # 1 20.3 g 2.0 ml
Run #2
MAEPH List
CAS No.
Compound
Result
RL
MDL Units Q
C11-C22 Aromatics (Unadj.)
7.05
13
5.4 mg/kg J
C9-C18 Aliphatics
ND
13
3.4 mg/kg
C19-C36 Aliphatics
4.49
13
3.4 mg/kg J
CAS No.
Surrogate Recoveries
Run# 1
Run# 2
Limits
3386-33-2
1-Chlorooctadecane
69%
40-140%
580-13-2
2-Bromonaphthalene
73%
40-140%
84-15-1
o-Terphenyl
71%
40-140%
321-60-8
2-Fluorobiphenyl
62%
40-140%
ND = Not detected MDL = Method Detection Limit
RL = Reporting Limit
E = Indicates value exceeds calibration range
J = Indicates an estimated value
B = Indicates analyte found in associated method blank
N = Indicates presumptive evidence of a compound
6 40 of 69
FA56562

ffm
Orlando, FL
Misc. Forms
Custody Documents and Other Forms
Includes the following where applicable:
• Chain of Custody
Section 4
6 41 of 69
FA56562

. IA Accutest Laboratories Southeast
� ACCLJTEST
Chain of Custody
4405 Vineland Road, Suite C-15 Orlando, 32911
*ST#'5IIiiiv b
Accutest JOB # PA( —OFF
LABORATORIES TEL. [phone] • FAX: [phone]"707
www.accu(est.com
CCuteSt u0te
Clant /Reporting Information r . . .r::m.,..+..a ..:.: Pro ect Information �' „, : u, . „,, ::.... �.. ".,
.. . .. ...:.
... .. �r" Analytical
Information
Z,:
".,•.3
Matdx Codes
Company Name
Project Name: /
e HC ! B
`9
r
V�r
DW . Drinking Water
GW - Ground Water
W W Water
SW - Surface Water
SO -Solt
SL - - soll
udge
OI
LIG •Other Liquid
AIR -Air
SOW OtWi eeolltl
P
USE 2ULY
Address
Street
, [
of a State fUG Zi
//
city CH.a r' e, Slate ti G
Project Contac G /K --mail
Project # 3OS - CS -006 Z
Phone#
Fax #
Sampler(s) Names) (Printed) C tK
Client Purchase order #
S- 3�s 6 -G as z
ACCat¢st
Sampleest
Field ID / Point of Collection
SAMPLEe
MATRI%
TOTpLN
dF
rnl
_ ilo8
tg
T 3
3gLAB
_ 7
S
- Sx
x
k
l3cb
k
k
UL-S"
r
X
X
X
XX
c...;.
TURNAROUND TIME Business Des
.„.?:
+., ,ar;4
Data
Deliverable
Information
.
.?.
,. ;..:
`r.�
:.�
Comments)
Remarks
❑ 10 Days Standard Approved By: / Rush Code
❑ 7 Day RUSH
® 5 Day RUSH
❑ 3Day EMERGENCY
❑ 2 Day EMERGENCY
❑ 1 Day EMERGENCY _
❑ OTHER
Emergency or Rush T/A Data Available VIA Email or Lablink
❑ COMMERCIAL "A" (RESULTS ONLY)
❑ COMMERCIAL "B" (RESULTS � V V I m ;
j;9L' `0iJ t^
REDT1 (EPA jt��3)r. QU--Ei� ^ft
DR
�FULT1(EPALALEVEL 4)��� �� 2�2Jd
EDD'S J
Sam
Ie C tnr must b documented
below
each time sam les change Possession,
in luding c uri r deliv.
Reli quished by mpler:
Da;/m
Receive4L$p: Refinqui
y :
Date TimeJ;Recerve
ecei d B
Re Inquishe by/
5 (
Da a Time:
`1(i)
R y:
6 7
Relinquished by:
Date Timed
By:
8
Lab use only: Custody Seal in Place: Y N Temp Blank Provided: Y N Preserved where Applicable: Y N Total At of Coolers: Cooler Temperature (s) Celsius:
FA56562: Chain of Custody
Page 1 of 2
P,
6 42 of 69
FA56562

SGS Sample Receipt Summary
Job Number: FA56562 Client: PM ENV Project: RES PROP
Date / Time Received: 8/9/2018 9:00:00 AM Delivery Method: FX Airbill Vs:
Therm ID: IR 1; Therm CIF: 0.1: # of Coolers: 1
Cooler Temps (Raw Measured) °C: Cooler 1: (2.0);
Cooler Temps (Corrected) °C: Cooler 1: (2.1);
Cooler Information
Y or
N
Sample Information
1. Custody Seals Present
❑d
❑
1. Sample labels present on bottles
2. Custody Seals Intact
2
❑
2. Samples preserved properly
3. Temp criteria achieved
❑d
❑
3. Sufficient volume/containers recvd for analysis:
4. Cooler temp verification
IR Gun
4. Condition of sample
5. Cooler media
Ice(Bag)
5. Sample recvd within HT
Trip Blank Information
1. Trip Blank present / cooler
2. Trip Blank listed on COC
3. Type Of TB Received
Y
or
N
N/A
❑
o
❑
❑
❑d
❑
W
❑
or
S
❑
N/A
❑d
Misc. Information
Number of Encores: 25-Gram 5-Gram
Test Strip Lot #s: pH 0-3 230315
Residual Chlorine Test Strip Lot #:
Comments
SM0Rev. Date OS/24/17 Technician: HEATHERW
Rev. D
6. Dates/Times/IDs on COC match Sample Label
7. VOCs have headspace
8. Bottles received for unspecified tests
9. Compositing instructions clear
10. Voa Soil Kits/Jars received past 48hrs?
11. % Solids Jar received?
12. Residual Chlorine Present?
Number of 5035 Field Kits:
pH 10-12 219813A
Y or
N
N/A
2
❑
❑d
❑
o
❑
Intact
o
❑
o
❑
❑
❑d
❑
❑
o
❑
❑
❑d
❑
❑
❑/
❑
❑
o
Number of Lab Filtered Metals:
Other: (Specify)
Date: 8/9/2018 9:00:00 AM Reviewer: Date:
FA56562: Chain of Custody
Page 2 of 2
� 43 of 69
FA56562

Orlando, FL
MS Volatiles
QC Data Summaries
60
i
Section 5
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
6 44 of 69
FA56562

Method Blank Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 1 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
V3C61-MB
3C1452.D
1
08/14/18
SP
n/a
n/a
V3C61
The QC reported here applies to the following samples: Method: SW846 8260B
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
CAS No. Compound
Result RL MDL Units Q
67-64-1
Acetone
36.3
50
10
ug/kg J
71-43-2
Benzene
ND
5.0
1.2
ug/kg
108-86-1
Bromobenzene
ND
5.0
1.0
ug/kg
74-97-5
Bromochloromethane
ND
5.0
1.5
ug/kg
75-27-4
Bromodichloromethane
ND
5.0
1.0
ug/kg
75-25-2
Bromoform
ND
5.0
1.0
ug/kg
78-93-3
2-Butanone (MEK)
ND
25
7.3
ug/kg
104-51-8
n-Butylbenzene
ND
5.0
1.0
ug/kg
135-98-8
sec-Butylbenzene
ND
5.0
1.0
ug/kg
98-06-6
tert-Butylbenzene
ND
5.0
1.0
ug/kg
56-23-5
Carbon Tetrachloride
ND
5.0
1.0
ug/kg
108-90-7
Chlorobenzene
ND
5.0
1.0
ug/kg
75-00-3
Chloroethane
ND
5.0
2.0
ug/kg
67-66-3
Chloroform
ND
5.0
1.3
ug/kg
95-49-8
o-Chlorotoluene
ND
5.0
1.0
ug/kg
106-43-4
p-Chlorotoluene
ND
5.0
1.0
ug/kg
124-48-1
Dibromochloromethane
ND
5.0
1.0
ug/kg
106-93-4
1,2-Dibromoethane
ND
5.0
1.0
ug/kg
75-71-8
Dichlorodifluoromethane
ND
5.0
2.0
ug/kg
95-50-1
1,2-Dichlorobenzene
ND
5.0
1.0
ug/kg
541-73-1
1,3-Dichlorobenzene
ND
5.0
1.0
ug/kg
106-46-7
1,4-Dichlorobenzene
ND
5.0
1.2
ug/kg
75-34-3
1, 1 -Dichloroethane
ND
5.0
1.8
ug/kg
107-06-2
1,2-Dichloroethane
ND
5.0
1.0
ug/kg
75-35-4
1, 1 -Dichloroethylene
ND
5.0
1.0
ug/kg
156-59-2
cis- 1, 2-Dichloroethylene
ND
5.0
1.4
ug/kg
156-60-5
trans- 1, 2-Dichloroethylene
ND
5.0
1.0
ug/kg
78-87-5
1,2-Dichloropropane
ND
5.0
1.0
ug/kg
142-28-9
1,3-Dichloropropane
ND
5.0
1.0
ug/kg
594-20-7
2,2-Dichloropropane
ND
5.0
1.0
ug/kg
563-58-6
1, 1 -Dichloropropene
ND
5.0
1.0
ug/kg
10061-01-5 cis- 1, 3-Dichloropropene
ND
5.0
1.0
ug/kg
10061-02-6 trans- 1, 3-Dichloropropene
ND
5.0
1.0
ug/kg
108-20-3
Di -Isopropyl Ether
ND
5.0
2.3
ug/kg
64-17-5
Ethyl Alcohol
ND
400
75
ug/kg
100-41-4
Ethlbenzene
ND
5.0
1.0
ug/kg
6 45 of 69
FA56562

Method Blank Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 2 of 3
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
73C61-MB
3C1452.D
1
08/14/18
SP
n/a
n/a
V3C61
The QC reported here applies to the following samples: Method: SW846 8260B
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
CAS No. Compound Result RL MDL Units Q
591-78-6
2-Hexanone
ND
25
7.5
ug/kg
98-82-8
Isopropylbenzene
ND
5.0
1.0
ug/kg
99-87-6
p-Isopropyltoluene
ND
5.0
1.0
ug/kg
74-83-9
Methyl Bromide
ND
5.0
2.0
ug/kg
74-87-3
Methyl Chloride
ND
5.0
2.0
ug/kg
75-09-2
Methylene Chloride
ND
10
4.0
ug/kg
108-10-1
4-Methyl-2-pentanone (MIBK) ND
25
7.5
ug/kg
1634-04-4
Methyl Tert Butyl Ether
ND
5.0
1.0
ug/kg
91-20-3
Naphthalene
ND
5.0
2.0
ug/kg
103-65-1
n-Propylbenzene
ND
5.0
1.0
ug/kg
100-42-5
Styrene
ND
5.0
1.0
ug/kg
630-20-6
1, 1, 1, 2-Tetrachloroethane
ND
5.0
1.0
ug/kg
79-34-5
1,1,2,2-Tetrachloroethane
ND
5.0
1.0
ug/kg
127-18-4
Tetrachloroethylene
ND
5.0
1.3
ug/kg
108-88-3
Toluene
ND
5.0
1.0
ug/kg
87-61-6
1,2,3-Trichlorobenzene
ND
5.0
1.4
ug/kg
120-82-1
1,2,4-Trichlorobenzene
ND
5.0
1.0
ug/kg
71-55-6
1, 1, 1 -Trichloroethane
ND
5.0
1.0
ug/kg
79-00-5
1,1,2-Trichloroethane
ND
5.0
1.0
ug/kg
79-01-6
Trichloroethylene
ND
5.0
1.0
ug/kg
75-69-4
Trichlorofluoromethane
ND
5.0
2.0
ug/kg
96-18-4
1, 2,3 -Trichloropropane
ND
5.0
1.3
ug/kg
95-63-6
1,2,4-Trimethylbenzene
ND
5.0
1.0
ug/kg
108-67-8
1,3,5-Trimethylbenzene
ND
5.0
1.0
ug/kg
108-05-4
Vinyl Acetate
ND
25
16
ug/kg
75-01-4
Vinyl Chloride
ND
5.0
1.0
ug/kg
m,p-Xylene
ND
10
1.1
ug/kg
95-47-6
o-Xylene
ND
5.0
1.0
ug/kg
1330-20-7
Xylene (total)
ND
15
2.1
ug/kg
CAS No.
Surrogate Recoveries
Limits
1868-53-7
Dibromofluoromethane
112%
75-124%
17060-07-0
1,2-Dichloroethane-D4
112%
72-135%
2037-26-5
Toluene-D8
103%
75-126%
6 46 of 69
FA56562

Method Blank Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 3 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
V3C61-MB
3C1452.D
1
08/14/18
SP
n/a
n/a
V3C61
The QC reported here applies to the following samples: Method: SW846 8260B
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
CAS No. Surrogate Recoveries Limits
460-00-4 4-Bromofluorobenzene 99% 71-133%
6 47 of 69
FA56562

Blank Spike Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 1 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
V3C61-BS
3C1448.D
1
08/14/18
SP
n/a
n/a
V3C61
The QC reported here applies to the following samples: Method: SW846 8260B
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
CAS No. Compound
Spike BSP BSP
ug/kg ug/kg % Limits
67-64-1
Acetone
250
294
118
61-152
71-43-2
Benzene
50
48.6
97
76-126
108-86-1
Bromobenzene
50
48.8
98
76-122
74-97-5
Bromochloromethane
50
48.4
97
77-120
75-27-4
Bromodichloromethane
50
53.0
106
74-130
75-25-2
Bromoform
50
58.0
116
76-127
78-93-3
2-Butanone (MEK)
250
227
91
75-137
104-51-8
n-Butylbenzene
50
45.5
91
71-128
135-98-8
sec-Butylbenzene
50
49.6
99
79-135
98-06-6
tert-Butylbenzene
50
41.1
82
77-133
56-23-5
Carbon Tetrachloride
50
54.9
110
78-133
108-90-7
Chlorobenzene
50
49.9
100
81-129
75-00-3
Chloroethane
50
64.3
129
68-133
67-66-3
Chloroform
50
50.7
101
72-123
95-49-8
o-Chlorotoluene
50
47.2
94
77-129
106-43-4
p-Chlorotoluene
50
48.9
98
80-134
124-48-1
Dibromochloromethane
50
57.5
115
76-127
106-93-4
1,2-Dibromoethane
50
50.4
101
77-126
75-71-8
Dichlorodifluoromethane
50
37.4
75
68-168
95-50-1
1,2-Dichlorobenzene
50
48.6
97
80-129
541-73-1
1,3-Dichlorobenzene
50
48.5
97
81-129
106-46-7
1,4-Dichlorobenzene
50
48.5
97
76-130
75-34-3
1, 1 -Dichloroethane
50
57.6
115
73-125
107-06-2
1,2-Dichloroethane
50
48.0
96
74-128
75-35-4
1, 1 -Dichloroethylene
50
54.0
108
81-136
156-59-2
cis- 1, 2-Dichloroethylene
50
47.2
94
74-126
156-60-5
trans- 1, 2-Dichloroethylene
50
52.4
105
70-127
78-87-5
1,2-Dichloropropane
50
50.7
101
74-125
142-28-9
1,3-Dichloropropane
50
47.9
96
76-122
594-20-7
2,2-Dichloropropane
50
48.3
97
77-133
563-58-6
1, 1 -Dichloropropene
50
45.7
91
75-130
10061-01-5 cis- 1, 3-Dichloropropene
50
51.2
102
80-123
10061-02-6 trans- 1, 3-Dichloropropene
50
53.1
106
75-131
108-20-3
Di -Isopropyl Ether
50
52.9
106
75-122
64-17-5
Ethyl Alcohol
1000
1050
105
53-154
100-41-4
Ethlbenzene
50
50.1
100
77-123
* = Outside of Control Limits.
6 48 of 69
FA56562

Blank Spike Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 2 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
V3C61-BS
3C1448.D
1
08/14/18
SP
n/a
n/a
V3C61
The QC reported here applies to the following samples: Method: SW846 8260B
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
CAS No. Compound
Spike BSP BSP
ug/kg ug/kg % Limits
591-78-6
2-Hexanone
250
244
98
72-133
98-82-8
Isopropylbenzene
50
53.9
108
80-136
99-87-6
p-Isopropyltoluene
50
41.5
83
77-131
74-83-9
Methyl Bromide
50
56.0
112
65-139
74-87-3
Methyl Chloride
50
46.1
92
71-144
75-09-2
Methylene Chloride
50
56.3
113
74-137
108-10-1
4-Methyl-2-pentanone (MIBK) 250
253
101
76-132
1634-04-4
Methyl Tert Butyl Ether
50
52.2
104
77-120
91-20-3
Naphthalene
50
42.4
85
79-129
103-65-1
n-Propylbenzene
50
48.6
97
80-135
100-42-5
Styrene
50
53.1
106
78-125
630-20-6
1, 1, 1, 2-Tetrachloroethane
50
57.4
115
78-126
79-34-5
1,1,2,2-Tetrachloroethane
50
49.5
99
71-126
127-18-4
Tetrachloroethylene
50
47.5
95
79-130
108-88-3
Toluene
50
47.1
94
76-124
87-61-6
1,2,3-Trichlorobenzene
50
41.6
83
77-128
120-82-1
1,2,4-Trichlorobenzene
50
45.5
91
78-130
71-55-6
1, 1, 1 -Trichloroethane
50
49.6
99
70-129
79-00-5
1,1,2-Trichloroethane
50
51.6
103
74-124
79-01-6
Trichloroethylene
50
48.5
97
75-128
75-69-4
Trichlorofluoromethane
50
54.3
109
73-145
96-18-4
1, 2,3 -Trichloropropane
50
42.5
85
74-127
95-63-6
1,2,4-Trimethylbenzene
50
42.5
85
74-123
108-67-8
1,3,5-Trimethylbenzene
50
48.9
98
73-122
108-05-4
Vinyl Acetate
250
220
88
48-164
75-01-4
Vinyl Chloride
50
48.0
96
76-141
m,p-Xylene
100
109
109
80-128
95-47-6
o-Xylene
50
50.9
102
80-132
1330-20-7
Xylene (total)
150
160
107
80-129
CAS No.
Surrogate Recoveries
BSP
Limits
1868-53-7
Dibromofluoromethane
102%
75-124%
17060-07-0
1,2-Dichloroethane-D4
95%
72-135%
2037-26-5
Toluene-D8
94%
75-126%
* = Outside of Control Limits.
6 49 of 69
FA56562

Blank Spike Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 3 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
V3C61-BS
3C1448.D
1
08/14/18
SP
n/a
n/a
V3C61
The QC reported here applies to the following samples: Method: SW846 8260B
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
CAS No. Surrogate Recoveries BSP Limits
460-00-4 4-Bromofluorobenzene 87% 71-133%
* = Outside of Control Limits.
6 50 of 69
FA56562

Matrix Spike/Matrix Spike Duplicate Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 1 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA56587-2MS
3C1469.D
1
08/15/18
SP
n/a
n/a
V3C61
FA56587-2MSD
3C1470.D
1
08/15/18
SP
n/a
n/a
V3C61
FA56587-2
3C1459.D
1
08/14/18
SP
n/a
n/a
V3C61
The QC reported here applies to the following samples:
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
CAS No. Compound
FA56587-2 Spike MS MS
ug/kg Q ug/kg ug/kg %
Method: SW846 8260B
Spike MSD MSD Limits
ug/kg ug/kg % RPD Rec/RPD
67-64-1
Acetone
54 U
305
274
90
301
261
87
5
61-152/27
71-43-2
Benzene
5.4 U
60.9
43.5
71*
60.2
44.6
74*
2
76-126/26
108-86-1
Bromobenzene
5.4 U
60.9
42.2
69*
60.2
42.8
71*
1
76-122/32
74-97-5
Bromochloromethane
5.4 U
60.9
46.7
77
60.2
46.1
77
1
77-120/24
75-27-4
Bromodichloromethane
5.4 U
60.9
45.0
74
60.2
47.5
79
5
74-130/25
75-25-2
Bromoform
5.4 U
60.9
49.8
82
60.2
50.4
84
1
76-127/26
78-93-3
2-Butanone(MEK)
27 U
305
203
67*
301
194
64*
5
75-137/25
104-51-8
n-Butylbenzene
5.4 U
60.9
35.6
58*
60.2
37.0
61*
4
71-128/35
135-98-8
sec-Butylbenzene
5.4 U
60.9
39.7
65*
60.2
41.2
68*
4
79-135/34
98-06-6
tert-Butylbenzene
5.4 U
60.9
35.2
58*
60.2
37.3
62*
6
77-133/34
56-23-5
Carbon Tetrachloride
5.4 U
60.9
40.6
67*
60.2
46.9
78
14
78-133/29
108-90-7
Chlorobenzene
5.4 U
60.9
44.7
73*
60.2
47.4
79*
6
81-129/29
75-00-3
Chloroethane
5.4 U
60.9
53.6
88
60.2
54.0
90
1
68-133/29
67-66-3
Chloroform
5.4 U
60.9
47.0
77
60.2
47.2
78
0
72-123/26
95-49-8
o-Chlorotoluene
5.4 U
60.9
41.1
67*
60.2
43.2
72*
5
77-129/33
106-43-4
p-Chlorotoluene
5.4 U
60.9
42.1
69*
60.2
44.3
74*
5
80-134/33
124-48-1
Dibromochloromethane
5.4 U
60.9
45.0
74*
60.2
48.7
81
8
76-127/27
106-93-4
1,2-Dibromoethane
5.4 U
60.9
43.9
72*
60.2
46.9
78
7
77-126/26
75-71-8
Dichlorodifluoromethane
5.4 U
60.9
23.9
39*
60.2
23.5
39*
2
68-168/29
95-50-1
1,2-Dichlorobenzene
5.4 U
60.9
41.4
68*
60.2
42.8
71*
3
80-129/32
541-73-1
1,3-Dichlorobenzene
5.4 U
60.9
42.0
69*
60.2
43.6
72*
4
81-129/33
106-46-7
1,4-Dichlorobenzene
5.4 U
60.9
42.2
69*
60.2
44.3
74*
5
76-130/32
75-34-3
1, 1 -Dichloroethane
5.4 U
60.9
52.5
86
60.2
52.1
87
1
73-125/27
107-06-2
1,2-Dichloroethane
5.4 U
60.9
47.3
78
60.2
46.8
78
1
74-128/23
75-35-4
1, 1 -Dichloroethylene
5.4 U
60.9
47.3
78*
60.2
48.1
80*
2
81-136/28
156-59-2
cis- 1, 2-Dichloroethylene
5.4 U
60.9
46.6
77
60.2
46.7
78
0
74-126/26
156-60-5
trans- 1, 2-Dichloroethylene
5.4 U
60.9
48.1
79
60.2
49.4
82
3
70-127/27
78-87-5
1,2-Dichloropropane
5.4 U
60.9
47.8
78
60.2
48.5
81
1
74-125/25
142-28-9
1,3-Dichloropropane
5.4 U
60.9
44.4
73*
60.2
45.2
75*
2
76-122/26
594-20-7
2,2-Dichloropropane
5.4 U
60.9
40.8
67*
60.2
39.4
65*
3
77-133/28
563-58-6
1, 1 -Dichloropropene
5.4 U
60.9
40.4
66*
60.2
41.4
69*
2
75-130/28
10061-01-5 cis- 1, 3-Dichloropropene
5.4 U
60.9
43.4
71*
60.2
45.1
75*
4
80-123/26
10061-02-6 trans-1,3-Dichloropropene
5.4 U
60.9
46.2
76
60.2
48.2
80
4
75-131/28
108-20-3
Di -Isopropyl Ether
5.4 U
60.9
52.0
85
60.2
51.0
85
2
75-122/25
64-17-5
Ethyl Alcohol
430 U
1220
1520
125
1200
1580
131
4
53-154/42
100-41-4
Ethlbenzene
5.4 U
60.9
46.4
76*
60.2
49.0
81
5
77-123/31
* = Outside of Control Limits.
01
51 of 69
FA56562

Matrix Spike/Matrix Spike Duplicate Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 2 of 3
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA56587-2MS
3C1469.D
1
08/15/18
SP
n/a
n/a
V3C61
FA56587-2MSD
3C1470.D
1
08/15/18
SP
n/a
n/a
V3C61
FA56587-2
3C1459.D
1
08/14/18
SP
n/a
n/a
V3C61
The QC reported here applies to the following samples:
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
CAS No. Compound
FA56587-2 Spike MS MS
ug/kg Q ug/kg ug/kg %
Method: SW846 8260B
Spike MSD MSD Limits
ug/kg ug/kg % RPD Rec/RPD
591-78-6
2-Hexanone
27 U
305
214
70*
301
200
66*
7
72-133/26
98-82-8
Isopropylbenzene
5.4 U
60.9
46.9
77*
60.2
49.5
82
5
80-136/32
99-87-6
p-Isopropyltoluene
5.4 U
60.9
34.1
56*
60.2
36.6
61*
7
77-131/34
74-83-9
Methyl Bromide
5.4 U
60.9
49.9
82
60.2
51.3
85
3
65-139/31
74-87-3
Methyl Chloride
5.4 U
60.9
43.1
71
60.2
43.4
72
1
71-144/27
75-09-2
Methylene Chloride
11 U
60.9
53.8
88
60.2
52.4
87
3
74-137/28
108-10-1
4-Methyl-2-pentanone (MIBK) 27 U
305
231
76
301
221
73*
4
76-132/26
1634-04-4
Methyl Tert Butyl Ether
5.4 U
60.9
51.4
84
60.2
49.4
82
4
77-120/24
91-20-3
Naphthalene
5.4 U
60.9
33.3
55*
60.2
35.6
59*
7
79-129/33
103-65-1
n-Propylbenzene
5.4 U
60.9
41.9
69*
60.2
44.0
73*
5
80-135/33
100-42-5
Styrene
5.4 U
60.9
46.2
76*
60.2
49.2
82
6
78-125/30
630-20-6
1, 1, 1, 2-Tetrachloroethane
5.4 U
60.9
50.0
82
60.2
49.8
83
0
78-126/27
79-34-5
1,1,2,2-Tetrachloroethane
5.4 U
60.9
43.8
72
60.2
42.7
71
3
71-126/30
127-18-4
Tetrachloroethylene
5.4 U
60.9
47.4
78*
60.2
51.4
85
8
79-130/31
108-88-3
Toluene
5.4 U
60.9
45.3
74*
60.2
47.8
79
5
76-124/30
87-61-6
1,2,3-Trichlorobenzene
5.4 U
60.9
28.7
47*
60.2
33.1
55*
14
77-128/35
120-82-1
1,2,4-Trichlorobenzene
5.4 U
60.9
33.9
56*
60.2
36.7
61*
8
78-130/34
71-55-6
1, 1, 1 -Trichloroethane
5.4 U
60.9
41.0
67*
60.2
42.9
71
5
70-129/27
79-00-5
1,1,2-Trichloroethane
5.4 U
60.9
48.2
79
60.2
49.1
82
2
74-124/28
79-01-6
Trichloroethylene
5.4 U
60.9
43.8
72*
60.2
45.3
75
3
75-128/27
75-69-4
Trichlorofluoromethane
5.4 U
60.9
36.8
60*
60.2
37.7
63*
2
73-145/31
96-18-4
1,2,3-Trichloropropane
5.4 U
60.9
39.4
65*
60.2
39.7
66*
1
74-127/27
95-63-6
1,2,4-Trimethylbenzene
5.4 U
60.9
37.4
61*
60.2
38.2
63*
2
74-123/34
108-67-8
1,3,5-Trimethylbenzene
5.4 U
60.9
42.8
70*
60.2
44.5
74
4
73-122/33
108-05-4
Vinyl Acetate
27 U
305
ND
0*
301
ND
0*
ne
48-164/37
75-01-4
Vinyl Chloride
5.4 U
60.9
40.2
66*
60.2
41.7
69*
4
76-141/27
m,p-Xylene
11 U
122
97.8
80
120
102
85
4
80-128/30
95-47-6
o-Xylene
5.4 U
60.9
46.9
77*
60.2
49.4
82
5
80-132/30
1330-20-7
Xylene (total)
16 U
183
145
79*
181
152
84
5
80-129/30
CAS No.
Surrogate Recoveries
MS
MSD
FA56587-2
Limits
1868-53-7
Dibromofluoromethane
100%
99%
111%
75-124%
17060-07-0
1,2-Dichloroethane-D4
98%
95%
122%
72-135%
2037-26-5
Toluene-D8
98%
104%
105%
75-126%
* = Outside of Control Limits.
6 52 of 69
FA56562

Matrix Spike/Matrix Spike Duplicate Summary Page 3 of 3
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA56587-2MS
3C1469.D
1
08/15/18
SP
n/a
n/a
V3C61
FA56587-2MSD
3C1470.D
1
08/15/18
SP
n/a
n/a
V3C61
FA56587-2
3C1459.D
1
08/14/18
SP
n/a
n/a
V3C61
The QC reported here applies to the following samples:
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
CAS No. Surrogate Recoveries MS MSD FA56587-2 Limits
460-00-4 4-Bromofluorobenzene 94% 94% 105% 71-133%
* = Outside of Control Limits.
Method: SW846 8260B
6 53 of 69
FA56562

Orlando, FL
MS Semi-volatiles
QC Data Summaries
:10
i
Section 6
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
0
6 54 of 69
FA56562

Method Blank Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
DP71335-MB
X062045.D
1
08/16/18
MV
08/14/18
OP71335
SX2574
The QC reported here applies to the following samples: Method: SW846 8270D
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
CAS No. Compound
Result RL MDL Units Q
65-85-0
Benzoic Acid
ND
830
170
ug/kg
59-50-7
4-Chloro-3-methyl Phenol
ND
170
19
ug/kg
95-57-8
2-Chlorophenol
ND
170
20
ug/kg
120-83-2
2,4-Dichlorophenol
ND
170
19
ug/kg
105-67-9
2,4-Dimethylphenol
ND
170
44
ug/kg
51-28-5
2,4-Dinitrophenol
ND
830
170
ug/kg
534-52-1
4,6-Dinitro-o-cresol
ND
330
67
ug/kg
95-48-7
2-Methylphenol
ND
170
20
ug/kg
3&4-Methylphenol
ND
170
27
ug/kg
88-75-5
2-Nitrophenol
ND
170
18
ug/kg
100-02-7
4-Nitrophenol
ND
830
170
ug/kg
87-86-5
Pentachlorophenol
ND
830
170
ug/kg
108-95-2
Phenol
ND
170
17
ug/kg
88-06-2
2,4,6-Trichlorophenol
ND
170
19
ug/kg
83-32-9
Acenaphthene
ND
170
18
ug/kg
208-96-8
Acenaphthylene
ND
170
17
ug/kg
120-12-7
Anthracene
ND
170
19
ug/kg
56-55-3
Benzo(a)anthracene
ND
170
17
ug/kg
50-32-8
Benzo(a)pyrene
ND
170
20
ug/kg
205-99-2
Benzo(b)fluoranthene
ND
170
18
ug/kg
191-24-2
Benzo(g,h,i)perylene
ND
170
17
ug/kg
207-08-9
Benzo(k)fluoranthene
ND
170
22
ug/kg
100-51-6
Benzyl Alcohol
ND
170
17
ug/kg
101-55-3
4-Bromophenyl phenyl ether
ND
170
17
ug/kg
85-68-7
Butyl benzyl phthalate
ND
170
33
ug/kg
106-47-8
4-Chloroaniline
ND
170
42
ug/kg
111-91-1
bis(2-Chloroethoxy)methane
ND
170
17
ug/kg
111-44-4
bis(2-Chloroethyl)ether
ND
170
19
ug/kg
108-60-1
2,2'-Oxybis(1-chloropropane)
ND
170
21
ug/kg
91-58-7
2-Chloronaphthalene
ND
170
17
ug/kg
7005-72-3
4-Chlorophenyl phenyl ether
ND
170
17
ug/kg
218-01-9
Chrysene
ND
170
17
ug/kg
53-70-3
Dibenzo(a,h)anthracene
ND
170
21
ug/kg
132-64-9
Dibenzofuran
ND
170
17
ug/kg
95-50-1
1,2-Dichlorobenzene
ND
170
17
ug/kg
541-73-1
1,3-Dichlorobenzene
ND
170
18
ug/kg
6 55 of 69
FA56562

Method Blank Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 2 of 2
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
)P71335-MB
X062045.D
1
08/16/18
MV
08/14/18
OP71335
SX2574
The QC reported here applies to the following samples: Method: SW846 8270D
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
CAS No. Compound
106-46-7
1,4-Dichlorobenzene
91-94-1
3, 3'-Dichlorobenzidine
84-66-2
Diethyl Phthalate
131-11-3
Dimethyl Phthalate
117-84-0
Di-n-octyl Phthalate
84-74-2
Di-n-butyl Phthalate
122-66-7
1, 2-Diphenylhydrazine
117-81-7
bis(2-Ethylhexyl)phthalate
206-44-0
Fluoranthene
86-73-7
Fluorene
118-74-1
Hexachlorobenzene
87-68-3
Hexachlorobutadiene
77-47-4
Hexachlorocyclopentadiene
67-72-1
Hexachloroethane
193-39-5
Indeno(1,2,3-cd)pyrene
78-59-1
Isophorone
90-12-0
1-M ethylnaphthalene
91-57-6
2-Methylnaphthalene
91-20-3
Naphthalene
98-95-3
Nitrobenzene
621-64-7
N-Nitrosodi-n-propylamine
86-30-6
N-Nitrosodiphenylamine
85-01-8
Phenanthrene
129-00-0
Pyrene
120-82-1
1,2,4-Trichlorobenzene
CAS No. Surrogate Recoveries
367-12-4 2-Fluorophenol
4165-62-2 Phenol-d5
118-79-6 2,4,6-Tribromophenol
4165-60-0 Nitrobenzene-d5
321-60-8 2-Fluorobiphenyl
1718-51-0 Terphenyl-d14
Result
RL
MDL
Units Q
ND
170
22
ug/kg
ND
170
40
ug/kg
ND
330
33
ug/kg
ND
170
33
ug/kg
ND
170
33
ug/kg
ND
330
67
ug/kg
ND
170
17
ug/kg
ND
330
33
ug/kg
ND
170
17
ug/kg
ND
170
18
ug/kg
ND
170
17
ug/kg
ND
170
17
ug/kg
ND
170
33
ug/kg
ND
170
20
ug/kg
ND
170
20
ug/kg
ND
170
17
ug/kg
ND
170
17
ug/kg
ND
170
17
ug/kg
ND
170
17
ug/kg
ND
170
17
ug/kg
ND
170
17
ug/kg
ND
170
18
ug/kg
ND
170
17
ug/kg
ND
170
19
ug/kg
ND
170
20
ug/kg
Limits
77%
40-102%
82%
41-100%
91%
42-108%
84%
40-105%
79%
43-107%
93%
45-119%
6 56 of 69
FA56562

Blank Spike Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP71335-BS
X062044.D
1
08/16/18
MV
08/14/18
OP71335
SX2574
The QC reported here applies to the following samples:
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
Spike
BSP
BSP
CAS No.
Compound
ug/kg
ug/kg
%
Limits
65-85-0
Benzoic Acid
3330
2680
80
36-118
59-50-7
4-Chloro-3-methyl Phenol
1670
1320
79
52-108
95-57-8
2-Chlorophenol
1670
1330
80
48-104
120-83-2
2,4-Dichlorophenol
1670
1310
79
51-105
105-67-9
2,4-Dimethylphenol
1670
1110
67
43-96
51-28-5
2,4-Dinitrophenol
3330
2600
78
40-119
534-52-1
4,6-Dinitro-o-cresol
3330
3080
92
64-121
95-48-7
2-Methylphenol
1670
1280
77
46-107
3&4-Methylphenol
3330
2620
79
44-111
88-75-5
2-Nitrophenol
1670
1450
87
49-104
100-02-7
4-Nitrophenol
3330
2760
83
56-116
87-86-5
Pentachlorophenol
3330
2270
68
61-114
108-95-2
Phenol
1670
1300
78
45-110
88-06-2
2,4,6-Trichlorophenol
1670
1620
97
56-109
83-32-9
Acenaphthene
1670
1360
82
56-109
208-96-8
Acenaphthylene
1670
1410
85
56-106
120-12-7
Anthracene
1670
1350
81
61-110
56-55-3
Benzo(a)anthracene
1670
1450
87
66-111
50-32-8
Benzo(a)pyrene
1670
1460
88
59-104
205-99-2
Benzo(b)fluoranthene
1670
1520
91
67-113
191-24-2
Benzo(g,h,i)perylene
1670
1480
89
67-113
207-08-9
Benzo(k)fluoranthene
1670
1530
92
67-114
100-51-6
Benzyl Alcohol
1670
1490
89
53-108
101-55-3
4-Bromophenyl phenyl ether
1670
1510
91
62-110
85-68-7
Butyl benzyl phthalate
1670
1530
92
65-113
106-47-8
4-Chloroaniline
1670
1110
67
30-115
111-91-1
bis(2-Chloroethoxy)methane
1670
1090
65
48-105
111-44-4
bis(2-Chloroethyl)ether
1670
1200
72
46-103
108-60-1
2,2'-Oxybis(1-chloropropane)
1670
1220
73
40-110
91-58-7
2-Chloronaphthalene
1670
1300
78
53-106
7005-72-3
4-Chlorophenyl phenyl ether
1670
1410
85
58-106
218-01-9
Chrysene
1670
1440
86
65-112
53-70-3
Dibenzo(a,h)anthracene
1670
1500
90
68-115
132-64-9
Dibenzofuran
1670
1510
91
57-108
95-50-1
1,2-Dichlorobenzene
1670
1130
68
44-102
541-73-1
1,3-Dichlorobenzene
1670
1150
69
42-100
* = Outside of Control Limits.
Method: SW846 8270D
6 57 of 69
FA56562

Blank Spike Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 2 of 2
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
)P71335-BS
X062044.D
1
08/16/18
MV
08/14/18
OP71335
SX2574
The QC reported here applies to the following samples: Method: SW846 8270D
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
Spike
BSP
BSP
CAS No.
Compound
ug/kg
ug/kg
%
Limits
106-46-7
1,4-Dichlorobenzene
1670
1130
68
40-106
84-66-2
Diethyl Phthalate
1670
1400
84
61-109
131-11-3
Dimethyl Phthalate
1670
1400
84
59-108
117-84-0
Di-n-octyl Phthalate
1670
1650
99
64-119
84-74-2
Di-n-butyl Phthalate
1670
1440
86
63-108
122-66-7
1,2-Diphenylhydrazine
1670
1420
85
58-112
117-81-7
bis(2-Ethylhexyl)phthalate
1670
1500
90
64-115
206-44-0
Fluoranthene
1670
1420
85
60-108
86-73-7
Fluorene
1670
1450
87
58-109
118-74-1
Hexachlorobenzene
1670
1470
88
59-111
87-68-3
Hexachlorobutadiene
1670
1100
66
41-108
77-47-4
Hexachlorocyclopentadiene
1670
1250
75
49-110
67-72-1
Hexachloroethane
1670
1120
67
40-105
193-39-5
Indeno(1,2,3-cd)pyrene
1670
1560
94
66-116
78-59-1
Isophorone
1670
1110
67
42-89
90-12-0
1-Methylnaphthalene
1670
1100
66
49-106
91-57-6
2-Methylnaphthalene
1670
1270
76
47-106
91-20-3
Naphthalene
1670
1070
64
44-104
98-95-3
Nitrobenzene
1670
1130
68
43-108
621-64-7
N-Nitrosodi-n-propylamine
1670
1230
74
48-108
86-30-6
N-Nitrosodiphenylamine
1670
1420
85
62-110
85-01-8
Phenanthrene
1670
1450
87
63-111
129-00-0
Pyrene
1670
1540
92
65-115
120-82-1
1,2,4-Trichlorobenzene
1670
1090
65
45-100
CAS No.
Surrogate Recoveries
BSP
Limits
367-12-4
2-Fluorophenol
78%
40-102%
4165-62-2
Phenol-d5
82%
41-100%
118-79-6
2,4,6-Tribromophenol
100%
42-108%
4165-60-0
Nitrobenzene-d5
71%
40-105%
321-60-8
2-Fluorobiphenyl
78%
43-107%
1718-51-0
Terphenyl-d14
92%
45-119%
* = Outside of Control Limits.
6 58 of 69
FA56562

Matrix Spike/Matrix Spike Duplicate Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 1 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP71335-MS
91002147.D
1
08/17/18
MV
08/14/18
OP71335
S9I74
OP71335-MSD
91002148.D
1
08/17/18
MV
08/14/18
OP71335
S9I74
FA56562-3
91002131.D
1
08/16/18
MV
08/14/18
OP71335
S9I73
The QC reported here applies to the following samples:
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
CAS No. Compound
FA56562-3 Spike MS MS
ug/kg Q ug/kg ug/kg %
Method: SW846 8270D
Spike MSD MSD Limits
ug/kg ug/kg % RPD Rec/RPD
65-85-0
Benzoic Acid
ND
4090
2090
51
4110
2000
49
4
36-118/41
59-50-7
4-Chloro-3-methyl Phenol
ND
2050
1550
76
2050
1680
82
8
52-108/21
95-57-8
2-Chlorophenol
ND
2050
1350
66
2050
1460
71
8
48-104/26
120-83-2
2,4-Dichlorophenol
ND
2050
1470
72
2050
1620
79
10
51-105/27
105-67-9
2,4-Dimethylphenol
ND
2050
1320
64
2050
1480
72
11
43-96/23
51-28-5
2,4-Dinitrophenol
ND
4090
3040
74
4110
3150
77
4
40-119/32
534-52-1
4,6-Dinitro-o-cresol
ND
4090
3370
82
4110
3630
88
7
64-121/29
95-48-7
2-Methylphenol
ND
2050
1320
64
2050
1450
71
9
46-107/24
3&4-Methylphenol
ND
4090
2750
67
4110
3020
74
9
44-111/24
88-75-5
2-Nitrophenol
ND
2050
1330
65
2050
1500
73
12
49-104/27
100-02-7
4-Nitrophenol
ND
4090
3420
84
4110
3720
91
8
56-116/23
87-86-5
Pentachlorophenol
ND
4090
2900
71
4110
3040
74
5
61-114/23
108-95-2
Phenol
ND
2050
1360
66
2050
1480
72
8
45-110/24
88-06-2
2,4,6-Trichlorophenol
ND
2050
1590
78
2050
1720
84
8
56-109/25
83-32-9
Acenaphthene
ND
2050
1430
70
2050
1600
78
11
56-109/23
208-96-8
Acenaphthylene
ND
2050
1510
74
2050
1680
82
11
56-106/23
120-12-7
Anthracene
ND
2050
1500
73
2050
1650
80
10
61-110/21
56-55-3
Benzo(a)anthracene
ND
2050
1540
75
2050
1720
84
11
66-111/23
50-32-8
Benzo(a)pyrene
ND
2050
1560
76
2050
1730
84
10
59-104/23
205-99-2
Benzo(b)fluoranthene
ND
2050
1690
83
2050
1840
90
8
67-113/24
191-24-2
Benzo(g,h,i)perylene
ND
2050
1630
80
2050
1850
90
13
67-113/21
207-08-9
Benzo(k)fluoranthene
ND
2050
1580
77
2050
1740
85
10
67-114/22
100-51-6
Benzyl Alcohol
ND
2050
1700
83
2050
1680
82
1
53-108/24
101-55-3
4-Bromophenyl phenyl ether
ND
2050
1570
77
2050
1750
85
11
62-110/21
85-68-7
Butyl benzyl phthalate
ND
2050
1640
80
2050
1800
88
9
65-113/20
106-47-8
4-Chloroaniline
ND
2050
1330
65
2050
1320
64
1
30-115/30
111-91-1
bis(2-Chloroethoxy)methane
ND
2050
1240
61
2050
1360
66
9
48-105/24
111-44-4
bis(2-Chloroethyl)ether
ND
2050
1180
58
2050
1310
64
10
46-103/27
108-60-1
2,2'-Oxybis(1-chloropropane)
ND
2050
1180
58
2050
1320
64
11
40-110/25
91-58-7
2-Chloronaphthalene
ND
2050
1350
66
2050
1520
74
12
53-106/23
7005-72-3
4-Chlorophenyl phenyl ether
ND
2050
1500
73
2050
1640
80
9
58-106/21
218-01-9
Chrysene
ND
2050
1580
77
2050
1780
87
12
65-112/25
53-70-3
Dibenzo(a,h)anthracene
ND
2050
1640
80
2050
1840
90
11
68-115/23
132-64-9
Dibenzofuran
ND
2050
1780
87
2050
1810
88
2
57-108/22
95-50-1
1,2-Dichlorobenzene
ND
2050
1040
51
2050
1190
58
13
44-102/28
541-73-1
1,3-Dichlorobenzene
ND
2050
1030
50
2050
1170
57
13
42-100/30
* = Outside of Control Limits.
01
59 of 69
FA56562

Matrix Spike/Matrix Spike Duplicate Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 2 of 2
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP71335-MS
91002147.D
1
08/17/18
MV
08/14/18
OP71335
S9I74
OP71335-MSD
91002148.D
1
08/17/18
MV
08/14/18
OP71335
S9I74
FA56562-3
91002131.D
1
08/16/18
MV
08/14/18
OP71335
S9I73
The QC reported here applies to the following samples:
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
CAS No. Compound
FA56562-3 Spike MS MS
ug/kg Q ug/kg ug/kg %
Method: SW846 8270D
Spike MSD MSD Limits
ug/kg ug/kg % RPD Rec/RPD
106-46-7
1,4-Dichlorobenzene
ND
2050
1020
50
2050
1160
56
13
40-106/29
84-66-2
Diethyl Phthalate
ND
2050
1600
78
2050
1720
84
7
61-109/20
131-11-3
Dimethyl Phthalate
ND
2050
1560
76
2050
1680
82
7
59-108/20
117-84-0
Di-n-octyl Phthalate
ND
2050
1740
85
2050
1860
91
7
64-119/21
84-74-2
Di-n-butyl Phthalate
ND
2050
1650
81
2050
1830
89
10
63-108/19
122-66-7
1,2-Diphenylhydrazine
ND
2050
1530
75
2050
1680
82
9
58-112/22
117-81-7
bis(2-Ethylhexyl)phthalate
ND
2050
1690
83
2050
1860
91
10
64-115/23
206-44-0
Fluoranthene
ND
2050
1600
78
2050
1800
88
12
60-108/25
86-73-7
Fluorene
ND
2050
1560
76
2050
1700
83
9
58-109/21
118-74-1
Hexachlorobenzene
ND
2050
1510
74
2050
1680
82
11
59-111/21
87-68-3
Hexachlorobutadiene
ND
2050
1120
55
2050
1290
63
14
41-108/27
77-47-4
Hexachlorocyclopentadiene
ND
2050
1170
57
2050
1340
65
14
49-110/31
67-72-1
Hexachloroethane
ND
2050
997
49
2050
1140
55
13
40-105/32
193-39-5
Indeno(1,2,3-cd)pyrene
ND
2050
1670
82
2050
1870
91
11
66-116/22
78-59-1
Isophorone
ND
2050
1290
63
2050
1430
70
10
42-89/22
90-12-0
1-Methylnaphthalene
ND
2050
1210
59
2050
1370
67
12
49-106/26
91-57-6
2-Methylnaphthalene
ND
2050
1620
79
2050
1600
78
1
47-106/27
91-20-3
Naphthalene
ND
2050
1170
57
2050
1340
65
14
44-104/27
98-95-3
Nitrobenzene
ND
2050
1210
59
2050
1380
67
13
43-108/25
621-64-7
N-Nitrosodi-n-propylamine
ND
2050
1280
63
2050
1410
69
10
48-108/27
86-30-6
N-Nitrosodiphenylamine
ND
2050
1550
76
2050
1690
82
9
62-110/21
85-01-8
Phenanthrene
ND
2050
1590
78
2050
1730
84
8
63-111/22
129-00-0
Pyrene
ND
2050
1650
81
2050
1810
88
9
65-115/25
120-82-1
1,2,4-Trichlorobenzene
ND
2050
1130
55
2050
1300
63
14
45-100/26
CAS No.
Surrogate Recoveries
MS
MSD
FA56562-3
Limits
367-12-4
2-Fluorophenol
71%
69%
66%
40-102%
4165-62-2
Phenol-d5
75%
73%
70%
41-100%
118-79-6
2,4,6-Tribromophenol
80%
84%
71%
42-108%
4165-60-0
Nitrobenzene-d5
69%
69%
57%
40-105%
321-60-8
2-Fluorobiphenyl
75%
76%
75%
43-107%
1718-51-0
Terphenyl-d14
82%
86%
89%
45-119%
* = Outside of Control Limits.
6 60 of 69
FA56562

i
SG$
Orlando, FL -me"
Section 7
GC Volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
6 61 of 69
FA56562

Method Blank Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GUU1319-MB
UU025482.D
1
08/15/18
NM
n/a
n/a
GUU1319
The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
CAS No.
Compound
Result
RL MDL
Units Q
C5- C8 Aliphatics (Unadj.)
ND
5100 1800
ug/kg
C9- C12 Aliphatics (Unadj.)
ND
5100 1800
ug/kg
C9- C10 Aromatics (Unadj.)
ND
5100 1800
ug/kg
CAS No.
Surrogate Recoveries
Limits
460-00-4
BFB
106%
70-130%
460-00-4
BFB
101%
70-130%
6 62 of 69
FA56562

Blank Spike/Blank Spike Duplicate Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
GUU1319-BS
UU025480.D
1
08/15/18
NM
n/a
n/a
GUU1319
GUU 1319-BSD
UU025481. D
1
08/ 15/ 18
NM
n/a
n/a
GUU 1319
The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
Spike
BSP
BSP
BSD
BSD
Limits
CAS No.
Compound
ug/kg
ug/kg
%
ug/kg
%
RPD
Rec/RPD
C5- C8 Aliphatics (Unadj.)
12500
13500
108
13000
104
19
70-130/25
C9- C12 Aliphatics (Unadj.)
8320
7420
89
7870
95
10
70-130/25
C9- C10 Aromatics (Unadj.)
4160
4320
104
4410
106
1
70-130/25
CAS No.
Surrogate Recoveries
BSP
BSD
Limits
460-00-4
BFB
99%
99%
70-130%
460-00-4
BFB
96%
96%
70-130%
* = Outside of Control Limits.
6 63 of 69
FA56562

Matrix Spike Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
FA56562-2MS
UU025489.D
1
08/16/18
NM
n/a
n/a
GUU1319
FA56562-2
UU025484.D
1
08/15/18
NM
n/a
n/a
GUU1319
The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
FA56562-2
Spike
MS MS
CAS No.
Compound
ug/kg Q
ug/kg
ug/kg %
Limits
C5- C8 Aliphatics (Unadj.)
ND
41000
24600 60*
70-130
C9- C12 Aliphatics (Unadj.)
ND
34200
11200 33*
70-130
C9- C10 Aromatics (Unadj.)
ND
20500
6730 33*
70-130
CAS No.
Surrogate Recoveries
MS
FA56562-2 Limits
460-00-4
BFB
104%
120%
70-130%
460-00-4
BFB
102%
115%
70-130%
* = Outside of Control Limits.
6 64 of 69
FA56562

Duplicate Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 1 of 1
ample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batcl
A56562-1DUP
UU025488.D
1
08/16/18
NM
n/a
n/a
GUU1319
'A56562-1
UU025483.D
1
08/15/18
NM
n/a
n/a
GUU1319
The QC reported here applies to the following samples: Method: MADEP VPH REV 1.1
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
FA56562-1 DUP
CAS No. Compound ug/kg Q ug/kg Q RPD Limits
C5- C8 Aliphatics (Unadj.) ND ND nc 50
C9- C12 Aliphatics (Unadj.) ND ND nc 50
C9- C10 Aromatics (Unadj.) ND ND nc 50
CAS No. Surrogate Recoveries
460-00-4 BFB
460-00-4 BFB
* = Outside of Control Limits.
DUP FA56562-1 Limits
122% 119% 70-130%
116% 113% 70-130%
P-
6 65 of 69
FA56562

ffm
Orlando, FL
GC/LC Semi-volatiles
QC Data Summaries
Includes the following where applicable:
• Method Blank Summaries
• Blank Spike Summaries
• Matrix Spike and Duplicate Summaries
kJ
i
Section 8
a
6 66 of 69
FA56562

Method Blank Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP71311-MB
NN023215.D
1
08/15/18
NJ
08/13/18
OP71311
GNN1137
The QC reported here applies to the following samples: Method: MADEP EPH REV 1.1
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
oD
CAS No.
Compound
Result
RL MDL
Units Q
C11-C22 Aromatics (Unadj.)
ND
10000 4000
ug/kg
C9-C18 Aliphatics
ND
10000 2500
ug/kg
C19-C36 Aliphatics
ND
10000 2500
ug/kg
CAS No.
Surrogate Recoveries
Limits
3386-33-2
1-Chlorooctadecane
75%
40-140%
580-13-2
2-Bromonaphthalene
65%
40-140%
84-15-1
o-Terphenyl
76%
40-140%
321-60-8
2-Fluorobiphenyl
57%
40-140%
6 67 of 69
FA56562

Blank Spike/Blank Spike Duplicate Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP71311-BS
NN023213.D
1
08/15/18
NJ
08/13/18
OP71311
GNN1137
OP71311-BSD
NN023214.D
1
08/15/18
NJ
08/13/18
OP71311
GNN1137
The QC reported here applies to the following samples: Method: MADEP EPH REV 1.1
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
Spike
BSP
BSP
BSD
BSD
PO
Limits iv
CAS No. Compound
ug/kg
ug/kg
%
ug/kg
%
RPD
Rec/RPD
C11-C22 Aromatics (Unadj.)
85000
71200
84
62900
74
12
40-140/30
C9-C18 Aliphatics
30000
21200
71
17200
57
21
40-140/30
C19-C36 Aliphatics
40000
36200
91
31600
79
14
40-140/30
CAS No. Surrogate Recoveries
BSP
BSD
Limits
3386-33-2 1-Chlorooctadecane
85%
72%
40-140%
580-13-2 2-Bromonaphthalene
90%
89%
40-140%
84-15-1 o-Terphenyl
93%
81%
40-140%
321-60-8 2-Fluorobiphenyl
79%
79%
40-140%
Sample Compound
Col #1
Col #2
Breakthrough
Limit
OP71311-BS 2-Methylnaphthalene
3330
ND
0.0%
5.0
OP71311-BS Naphthalene
3070
ND
0.0%
5.0
OP71311-BSD 2-Methylnaphthalene
2700
ND
0.0%
5.0
OP71311-BSD Naphthalene
2420
ND
0.0%
5.0
* = Outside of Control Limits.
6 68 of 69
FA56562

Duplicate Summary
Job Number: FA56562
Account: PMENCC PM Environmental
Project: Residential Property; Charlotte, NC
Page 1 of 1
Sample
File ID
DF
Analyzed
By
Prep Date
Prep Batch
Analytical Batch
OP71311-DUP
NN023217.D
1
08/15/18
NJ
08/13/18
OP71311
GNN1137
FA56553-2
NN023216.D
1
08/15/18
NJ
08/13/18
OP71311
GNN1137
The QC reported here applies to the following samples: Method: MADEP EPH REV 1.1
FA56562-1, FA56562-2, FA56562-3, FA56562-4, FA56562-5
oD
FA56553-2
DUP
w
CAS No.
Compound
ug/kg Q
ug/kg Q
RPD Limits
C11-C22 Aromatics (Unadj.)
12000 U
ND
nc 30 a
C9-C18 Aliphatics
12000 U
ND
nc 30 a
C19-C36 Aliphatics
3430 J
3730 J
8 30 a
CAS No.
Surrogate Recoveries
DUP
FA56553-2
Limits
3386-33-2
1-Chlorooctadecane
70%
82%
40-140%
580-13-2
2-Bromonaphthalene
86%
81%
40-140%
84-15-1
o-Terphenyl
86%
85%
40-140%
321-60-8
2-Fluorobiphenyl
74%
72%
40-140%
(a) Advisory control limits.
* = Outside of Control Limits.
6 69 of 69
FA56562

Appendix C
Environmental
OPM & Engineering
ENVIRONMENTAL Services

. IA Accutest Laboratories Southeast
� ACCLJTEST
Chain of Custody
4405 Vineland Road, Suite C-15 Orlando, 32911
*ST#'5IIiiiv b
Accutest JOB # PA( —OFF
LABORATORIES TEL. [phone] • FAX: [phone]"707
www.accu(est.com
CCuteSt u0te
Clant /Reporting Information r . . .r::m.,..+..a ..:.: Pro ect Information �' „, : u, . „,, ::.... �.. ".,
.. . .. ...:.
... .. �r" Analytical
Information
Z,:
".,•.3
Matdx Codes
Company Name
Project Name: /
e HC ! B
`9
r
V�r
DW . Drinking Water
GW - Ground Water
W W Water
SW - Surface Water
SO -Solt
SL - - soll
udge
OI
LIG •Other Liquid
AIR -Air
SOW OtWi eeolltl
P
USE 2ULY
Address
Street
, [
of a State fUG Zi
//
city CH.a r' e, Slate ti G
Project Contac G /K --mail
Project # 3OS - CS -006 Z
Phone#
Fax #
Sampler(s) Names) (Printed) C tK
Client Purchase order #
S- 3�s 6 -G as z
ACCat¢st
Sampleest
Field ID / Point of Collection
SAMPLEe
MATRI%
TOTpLN
dF
rnl
_ ilo8
tg
T 3
3gLAB
_ 7
S
- Sx
x
k
l3cb
k
k
UL-S"
r
X
X
X
XX
c...;.
TURNAROUND TIME Business Des
.„.?:
+., ,ar;4
Data
Deliverable
Information
.
.?.
,. ;..:
`r.�
:.�
Comments)
Remarks
❑ 10 Days Standard Approved By: / Rush Code
❑ 7 Day RUSH
® 5 Day RUSH
❑ 3Day EMERGENCY
❑ 2 Day EMERGENCY
❑ 1 Day EMERGENCY _
❑ OTHER
Emergency or Rush T/A Data Available VIA Email or Lablink
❑ COMMERCIAL "A" (RESULTS ONLY)
❑ COMMERCIAL "B" (RESULTS � V V I m ;
j;9L' `0iJ t^
REDT1 (EPA jt��3)r. QU--Ei� ^ft
DR
�FULT1(EPALALEVEL 4)��� �� 2�2Jd
EDD'S J
Sam
Ie C tnr must b documented
below
each time sam les change Possession,
in luding c uri r deliv.
Reli quished by mpler:
Da;/m
Receive4L$p: Refinqui
y :
Date TimeJ;Recerve
ecei d B
Re Inquishe by/
5 (
Da a Time:
`1(i)
R y:
6 7
Relinquished by:
Date Timed
By:
8
Lab use only: Custody Seal in Place: Y N Temp Blank Provided: Y N Preserved where Applicable: Y N Total At of Coolers: Cooler Temperature (s) Celsius:
FA56562: Chain of Custody
Page 1 of 2
P,
6 42 of 69
FA56562

Appendix D
Environmental
OPM & Engineering
ENVIRONMENTAL Services

PAR
Photographs From Site Reconnaissance
PM Project No. 15-4305-0-0002
ENWRONMMAL
Location: 411 Woodvale Place, Charlotte, North Carolina
Photograph 1
ly
k-.
View of Subject Property and stockpiled soil.
r.
y
Photograph 2
II
i
.-I
View of stockpiled soil being loaded into dump
'
truck.

PAR
Photographs From Site Reconnaissance
PM Project No. 15-4305-0-0002
ENWRONMMAL
Location: 411 Woodvale Place, Charlotte, North Carolina
Photograph 3
. r
View of excavated basin.
"IVp
t.
}
Photograph 4
�ti
x
i
{
ff�36
View of Subject Property post excavation.
�2
'.x